6001_Mecklenburg_Harrisburg_MSWLF_Dec22GW_FID1767932_20230118

I pENR USE ONLY: I I ❑Paper Report [:]Electronic Data Email CD (data loaded: Yes / No Doc/Event #:
' NC DENR Environmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Mecklenburg County Solid Waste Services
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Amber R. Grzymski, P.G. Phone: [phone]
E-mail: [e-mail]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Harrisburg Road Landfill 7817 Harrisburg Road, Charlotte 60-01 .0500 December 13-14, 2022
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring QX Detection Monitoring Assessment Monitoring ❑ Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells �X Methane gas monitoring data
Groundwater monitoring data from private water supply wells Corrective action data (specify)
Leachate monitoring data ❑
Surface water monitoring data Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
El Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Amber R. Grzymski, P.G. Project Manager
Fadllty RerJresent i nt Title
01-18-2023
Signature W Date
2145 Suttle Ave, Charlotte, NC 28208
Facility Representative Address
980-314-3855
Telephone Number
Affix NC LicenW0j?8j"_,&%LGeologist Seal
l Fw�u�p!tr s
� A o
:P OHOt 0
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009

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MECKLENBURG COUNTY
Land Use and Environmental Services Agency
Solid Waste Services
January 18, 2023
Jaclynne Drummond
North Carolina Department of Environment
and Natural Resources
Division of Waste Management - Solid Waste Section
2090 US Highway 70
Swannanoa, NC 28778
Subject: Water Quality Monitoring Report December 2022
Harrisburg Road Landfill, Permit 60-01
Dear Ms. Drummond:
Mecklenburg County conducted semi-annual water quality monitoring at the closed
Harrisburg Road Landfill December 13, 2022, in accordance with the approved revised
sample and analysis plan dated May 11, 2004. Samples were collected from five
monitoring wells (HBW-12B, HBW-14, HBW-20, HBW-21, and background well
HBW-28) and three surface -water sampling locations (HB2006, HB2008 and, 1-1132010).
Monitoring wells HBW-17B and HBW-22 were dry during this sampling event.
Laboratory analytical data and field -measured data are included on the electronic data
deliverable (EDD) submittal. A new landfill gas probe (MP-13) was installed between
MP -I I and the property line. A report under a separate cover will be submitted on the
installation of the new probe.
The EDD containing the monitoring data are labeled to reflect the units that are used for
reporting. Detection levels and applicable standards have been included for all sampling
locations. Surface water standards listed are the water quality standards established for
freshwater classification for aquatic life as outlined in 15A NCAC 213 "Classification and
Water Quality Standards Applicable to Surface Waters of North Carolina". Groundwater
standards listed are the standards outlined in 15A NCAC 2L "Classification of Water
Quality Standards applicable to the Groundwaters of North Carolina". If the sample is
reported in parts per billion, then the standard is also reported in parts per billion.
PEOPLE • PRIDE • PROGRESS • PARTNERSHIP
2145 Suttle Ave • Charlotte, NC 28208-5237 • [phone] • FAX [phone]
www.wipeoutwaste.com

Page 2
Surface -water samples:
Barium was detected in HB 2006, HB 2008 and HB 2010 at 27.1 ppb, 20.7 ppb and 49.4
ppb, respectively. No other analytes were detected in the surface water samples. Field -
measured parameters for surface -water samples were within the range of established
standards and are summarized in the table below.
Location
Temperature
PH
Specific
Conductivity
Dissolved
Ox en
HB2006
8.70 C
7.1
190.3 µs/cm
11.52 mg/l
HB2008
9.30 C
7.8
168.1 µs/cm
11.54 mg/l
HB2010
8.30 C
7.4
264.2 µs/cm
10.82 mg/l
Groundwater samples:
No metals were detected above 2L standards. The table below summarizes metals
detections in groundwater samples.
Well ID
Ba
ug/l
Be
ug/l
Cd
ug/1
Cr
ug/l
Co
ug/l
Cu
ug/l
Ni
ug/l
Pb
ug/l
Th
ug/1
Vn
ug/l
Zn
ug/l
HBW12B
32.1
-----
-----
-----
------
-----
-----
-----
------
-----
-----
HBW14
133
-----
-----
-----
-----
40.6
-----
-----
------
-----
-----
HBW17B
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
HBW-20
10.3
-----
-----
-----
-----
-----
-----
-----
------
-----
-----
HBW-21
14.0
-----
-----
-----
-----
-----
-----
-----
------
-----
-----
HBW-22
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
HBW-28*
33.1
-----
-----
-----
-----
33.9
-----
-----
------
-----
-----
2L Std. ug/1
700
4
2.0
10
1
1,000
100
15
0.2
0.3
1,000
Note: Bolded results exceed 2L Standard, *Background Well, NS= No Sample
The following volatile organic compound ("VOC") was detected in the sample collected
fi om well HBW-20:
VOC
I Sample Result u /l
2L Standard u /l
1,1-Dichloroethane
1 1.0
6
The pH was measured to be more acidic than the standard in the samples collected from
HBW-12B, HBW-20, HBW-21, HBW-22 and background monitoring well HBW-28.
Field -measured parameters for groundwater samples are summarized in the following
table:

Page 3
Location
Temperature
pH
Conductivity
HBW12B
14.6 °C
6.4
372.6 µs/cm
HBW14
15.4 °C
6.7
206.2 µs/cm
HBW-20
16.1 °C
6.4
140.3 [is/cm
HBW-21
15.1 °C
6.2
195.0 µs/cm
*HBW-28
16.0 °C
5.1
29.4 Rs/cm.
Note: Bolded results are outside of the 6.5 to 8.5 S.U. range 2L Standard
*Background Well
Please call me at [phone], if you have any questions concerning this report.
Sincerely,
-lip
YR
Fe A
Gr' ° Amber R. Grzymski P.G.
Project Manager
LUESA Solid Waste Services
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Landfill Gas Monitoring Data Form
Facility Name: ,Harrisburg Road Landfill Permit Number: 60-01
Date of Sampling: J12/14/2022 NC Landfill Rule (.0500 or .1600): .0500
Name and Position of Sample Collector: _Amber R. Grzymski, Proiect Manager
Type and Serial Number of Gas Meter: Gem 5000 #G507530
Calibration Date of Gas Meter: 4/l/2022 Date and Time of Field Calibration: 12/14/2022 9:45 AM
Type of Field Calibration Gas (15/15 or 35/50): 35/50
Expiration Date of Field Calibration Gas Canister: April 2027
Pump Rate of Gas Meter: ,120 Seconds _ Ambient Air Temperature: 46 Degrees
Barometric Pressure: 29.37 General Weather Conditions: Cloudy, Calm
Sample ID
Time
% LEL
% CH4
% CO2
% 02
Comments
MP-1
10:00
>100
61.3
38.6
0.1
Methane Extraction System
MP-2
10:05
>100
59.2
31.9
1.9
Methane Extraction System
MP-3
10:11
2
0.1
0.3
20.9
Methane Extraction System
MP-4
10:15
>100
37.8
27.0
7.3
Methane Extraction System
MP-5
10:58
0
0
3.3
17.9
MP-6
10:52
0
0
4.9
16.3
MP-7
11:03
0
0
6.5
15.1
MP-8
11:09
0
0
7.8
13.5
MP-9A
11:14
0
0
1.5
19.4
MP-9B
11:20
0
0
6.5
14.9
MP-11
11:30
>100
32.9
21.1
6.7
MP-12
11:45
0
0
10.3
8.4
MP-13
11:54
2
0.1
0.4
21.0
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and
attachments are true and correct. I am aware that there are significant penalties for making any false
statemejA epresentation, or certification including the possibility of a fine and imprisonment.
SIGN TURE TITLE

60-01 Harrisburg Rd Landfill Methane Probes
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2022 Aerial Photo

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
January 06, 2023
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642459
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on December 13, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Ariel S Fitzgerald
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 21

lacmnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642459
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification M 812
CERTIFICATIONS
South Carolina Certification M 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification M E87627
Kentucky UST Certification M 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification M 460221
North Carolina Certification #: 381
South Carolina Certification M 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642459
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92642459001 6001-HBW21
EPA 6010D
DRB
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
SAS
52
PASI-C
92642459002 6001-HBW12B
EPA 6010D
DRB
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
SAS
52
PASI-C
92642459003 TRIP BLANK
EPA 8260D
SAS
52
PASI-C
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 21

Pace Analytical Services, LLC
ceAnalyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642459
Sample: 6001-HBW21 Lab ID: 92642459001 Collected: 12/13/22 11:45 Received: 12/13/22 14:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
12/27/22 14:40
12/28/22 01:31
7440-38-2
Beryllium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:31
7440-41-7
Barium
14.0
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:31
7440-39-3
Cadmium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:31
7440-43-9
Chromium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:31
7440-47-3
Copper
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:31
7440-50-8
Nickel
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:31
7440-02-0
Silver
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:31
7440-22-4
Lead
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:31
7439-92-1
Antimony
ND
ug/L
50.0
1
12/27/22 14:40
12/28/22 01:31
7440-36-0
Selenium
ND
ug/L
40.0
1
12/27/22 14:40
12/28/22 01:31
7782-49-2
Thallium
ND
ug/L
200
1
12/27/22 14:40
12/28/22 01:31
7440-28-0
Vanadium
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:31
7440-62-2
Zinc
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:31
7440-66-6
Cobalt
ND
ug/L
40.0
1
12/27/22 14:40
12/28/22 01:31
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
12/27/2217:44
01/03/2315:56
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/17/22 02:14
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/17/22 02:14
107-13-1
Benzene
ND
ug/L
1.0
1
12/17/22 02:14
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/17/22 02:14
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/17/22 02:14
75-27-4
Bromoform
ND
ug/L
1.0
1
12/17/22 02:14
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/17/22 02:14
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/17/22 02:14
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/17/22 02:14
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/17/22 02:14
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/17/22 02:14
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/17/22 02:14
75-00-3
Chloroform
ND
ug/L
1.0
1
12/17/22 02:14
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/17/22 02:14
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/17/22 02:14
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/17/22 02:14
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/17/22 02:14
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/17/22 02:14
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/17/22 02:14
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/17/22 02:14
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/17/22 02:14
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/17/22 02:14
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/17/22 02:14
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:53 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642459
Sample: 6001-HBW21 Lab ID: 92642459001 Collected: 12/13/22 11:45 Received: 12/13/22 14:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/17/22 02:14
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/17/22 02:14
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/17/22 02:14
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/17/22 02:14
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/17/22 02:14
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/17/22 02:14
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/17/22 02:14
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/17/22 02:14
591-78-6
lodomethane
ND
ug/L
20.0
1
12/17/22 02:14
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/17/22 02:14
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/17/22 02:14
108-10-1
Styrene
ND
ug/L
1.0
1
12/17/22 02:14
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/17/22 02:14
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/17/22 02:14
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/17/22 02:14
127-18-4
Toluene
ND
ug/L
1.0
1
12/17/22 02:14
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/17/22 02:14
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/17/22 02:14
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/17/22 02:14
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/17/22 02:14
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/17/22 02:14
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/17/22 02:14
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/17/22 02:14
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/17/22 02:14
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/17/22 02:14
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/17/22 02:14
95-47-6
Surrogates
4-Bromofluorobenzene (S)
101
%
70-130
1
12/17/22 02:14
460-00-4
1,2-Dichloroethane-d4 (S)
105
%
70-130
1
12/17/22 02:14
17060-07-0
Toluene-d8 (S)
102
%
70-130
1
12/17/22 02:14
2037-26-5
Date: 01/06/2023 03:53 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 21

Pace Analytical Services, LLC
ceAnalyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642459
Sample: 6001-HBW12B Lab ID: 92642459002 Collected: 12/13/22 12:00 Received: 12/13/22 14:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
12/27/22 14:40
12/28/22 01:36
7440-38-2
Beryllium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:36
7440-41-7
Barium
32.1
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:36
7440-39-3
Cadmium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:36
7440-43-9
Chromium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:36
7440-47-3
Copper
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:36
7440-50-8
Nickel
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:36
7440-02-0
Silver
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:36
7440-22-4
Lead
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:36
7439-92-1
Antimony
ND
ug/L
50.0
1
12/27/22 14:40
12/28/22 01:36
7440-36-0
Selenium
ND
ug/L
40.0
1
12/27/22 14:40
12/28/22 01:36
7782-49-2
Thallium
ND
ug/L
200
1
12/27/22 14:40
12/28/22 01:36
7440-28-0
Vanadium
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:36
7440-62-2
Zinc
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:36
7440-66-6
Cobalt
ND
ug/L
40.0
1
12/27/22 14:40
12/28/22 01:36
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
12/27/2217:44
01/03/2316:02
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/17/22 02:32
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/17/22 02:32
107-13-1
Benzene
ND
ug/L
1.0
1
12/17/22 02:32
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/17/22 02:32
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/17/22 02:32
75-27-4
Bromoform
ND
ug/L
1.0
1
12/17/22 02:32
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/17/22 02:32
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/17/22 02:32
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/17/22 02:32
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/17/22 02:32
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/17/22 02:32
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/17/22 02:32
75-00-3
Chloroform
ND
ug/L
1.0
1
12/17/22 02:32
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/17/22 02:32
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/17/22 02:32
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/17/22 02:32
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/17/22 02:32
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/17/22 02:32
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/17/22 02:32
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/17/22 02:32
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/17/22 02:32
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/17/22 02:32
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/17/22 02:32
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:53 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642459
Sample: 6001-HBW12B Lab ID: 92642459002 Collected: 12/13/22 12:00 Received: 12/13/22 14:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/17/22 02:32
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/17/22 02:32
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/17/22 02:32
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/17/22 02:32
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/17/22 02:32
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/17/22 02:32
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/17/22 02:32
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/17/22 02:32
591-78-6
lodomethane
ND
ug/L
20.0
1
12/17/22 02:32
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/17/22 02:32
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/17/22 02:32
108-10-1
Styrene
ND
ug/L
1.0
1
12/17/22 02:32
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/17/22 02:32
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/17/22 02:32
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/17/22 02:32
127-18-4
Toluene
ND
ug/L
1.0
1
12/17/22 02:32
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/17/22 02:32
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/17/22 02:32
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/17/22 02:32
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/17/22 02:32
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/17/22 02:32
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/17/22 02:32
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/17/22 02:32
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/17/22 02:32
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/17/22 02:32
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/17/22 02:32
95-47-6
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
12/17/22 02:32
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
12/17/22 02:32
17060-07-0
Toluene-d8 (S)
106
%
70-130
1
12/17/22 02:32
2037-26-5
Date: 01/06/2023 03:53 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 21

Pace Analytical Services, LLC
ceAnalyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642459
Sample: TRIP BLANK Lab ID: 92642459003 Collected: 12/13/22 00:00 Received: 12/13/22 14:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/17/22 01:02
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/17/22 01:02
107-13-1
Benzene
ND
ug/L
1.0
1
12/17/22 01:02
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/17/22 01:02
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/17/22 01:02
75-27-4
Bromoform
ND
ug/L
1.0
1
12/17/22 01:02
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/17/22 01:02
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/17/22 01:02
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/17/22 01:02
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/17/22 01:02
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/17/22 01:02
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/17/22 01:02
75-00-3
Chloroform
ND
ug/L
1.0
1
12/17/22 01:02
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/17/22 01:02
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/17/22 01:02
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/17/22 01:02
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/17/22 01:02
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/17/22 01:02
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/17/22 01:02
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/17/22 01:02
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/17/22 01:02
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/17/22 01:02
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/17/22 01:02
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/17/22 01:02
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/17/22 01:02
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/17/22 01:02
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/17/22 01:02
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/17/22 01:02
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/17/22 01:02
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/17/22 01:02
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/17/22 01:02
591-78-6
lodomethane
ND
ug/L
20.0
1
12/17/22 01:02
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/17/22 01:02
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/17/22 01:02
108-10-1
Styrene
ND
ug/L
1.0
1
12/17/22 01:02
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/17/22 01:02
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/17/22 01:02
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/17/22 01:02
127-18-4
Toluene
ND
ug/L
1.0
1
12/17/22 01:02
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/17/22 01:02
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/17/22 01:02
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/17/22 01:02
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/17/22 01:02
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/17/22 01:02
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/17/22 01:02
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/17/22 01:02
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:53 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642459
Sample: TRIP BLANK
Parameters
Lab ID: 92642459003 Collected: 12/13/22 00:00
Results Units Report Limit DF
Received: 12/13/22 14:38 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
12/17/22 01:02
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
12/17/22 01:02
179601-23-1
o-Xylene
ND ug/L
1.0
1
12/17/22 01:02
95-47-6
Surrogates
4-Bromofluorobenzene (S)
100 %
70-130
1
12/17/22 01:02
460-00-4
1,2-Dichloroethane-d4 (S)
102 %
70-130
1
12/17/22 01:02
17060-07-0
Toluene-d8 (S)
108 %
70-130
1
12/17/22 01:02
2037-26-5
Date: 01/06/2023 03:53 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642459
QC Batch: 745958 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 601 OD ATL
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92642459001, 92642459002
METHOD BLANK: 3880043
Associated Lab Samples: 92642459001, 92642459002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Antimony
ug/L
ND
50.0
12/28/22 00:08
Arsenic
ug/L
ND
30.0
12/28/22 00:08
Barium
ug/L
ND
10.0
12/28/22 00:08
Beryllium
ug/L
ND
10.0
12/28/22 00:08
Cadmium
ug/L
ND
10.0
12/28/22 00:08
Chromium
ug/L
ND
10.0
12/28/22 00:08
Cobalt
ug/L
ND
40.0
12/28/22 00:08
Copper
ug/L
ND
20.0
12/28/22 00:08
Lead
ug/L
ND
20.0
12/28/22 00:08
Nickel
ug/L
ND
20.0
12/28/22 00:08
Selenium
ug/L
ND
40.0
12/28/22 00:08
Silver
ug/L
ND
10.0
12/28/22 00:08
Thallium
ug/L
ND
200
12/28/22 00:08
Vanadium
ug/L
ND
20.0
12/28/22 00:08
Zinc
ug/L
ND
20.0
12/28/22 00:08
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3880044
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
1000
1060
106
80-120
Arsenic
ug/L
1000
1070
107
80-120
Barium
ug/L
1000
1040
104
80-120
Beryllium
ug/L
1000
1070
107
80-120
Cadmium
ug/L
1000
1070
107
80-120
Chromium
ug/L
1000
1050
105
80-120
Cobalt
ug/L
1000
1070
107
80-120
Copper
ug/L
1000
1050
105
80-120
Lead
ug/L
1000
1070
107
80-120
Nickel
ug/L
1000
1080
108
80-120
Selenium
ug/L
1000
1070
107
80-120
Silver
ug/L
1000
1020
102
80-120
Thallium
ug/L
1000
1030
103
80-120
Vanadium
ug/L
1000
1120
112
80-120
Zinc
ug/L
1000
1070
107
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:53 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
HARRISBURG RD LANDFILL(PERMIT#
92642459
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3880045
3880046
MS
MSD
92641048001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
1000
1000
1060
1090
105
108
75-125
3
Arsenic
ug/L
ND
1000
1000
1070
1100
107
110
75-125
2
Barium
ug/L
76.5
1000
1000
1120
1140
104
107
75-125
2
Beryllium
ug/L
ND
1000
1000
1070
1100
107
109
75-125
3
Cadmium
ug/L
ND
1000
1000
1070
1090
107
109
75-125
3
Chromium
ug/L
ND
1000
1000
1060
1080
106
108
75-125
1
Cobalt
ug/L
20AJ
1000
1000
1090
1110
107
109
75-125
2
Copper
ug/L
20.OJ
1000
1000
1100
1120
108
110
75-125
2
Lead
ug/L
ND
1000
1000
1070
1100
105
108
75-125
3
Nickel
ug/L
27.0
1000
1000
1100
1120
107
110
75-125
2
Selenium
ug/L
ND
1000
1000
1020
1030
102
103
75-125
1
Silver
ug/L
ND
1000
1000
1040
1050
104
105
75-125
1
Thallium
ug/L
ND
1000
1000
1040
1070
104
107
75-125
2
Vanadium
ug/L
ND
1000
1000
1140
1160
114
116
75-125
2
Zinc
ug/L
13.1 J
1000
1000
1050
1080
103
107
75-125
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:53 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 21

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642459
QC Batch: 746005 Analysis Method: EPA 6020B
QC Batch Method: EPA 3005A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92642459001, 92642459002
METHOD BLANK: 3880266
Matrix:
Water
Associated Lab Samples: 92642459001, 92642459002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
1.0
01/03/2314:31
LABORATORY CONTROL SAMPLE:
3880267
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
100
101
101 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3880268 3880269
MS MSD
92641696001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L 0.18J 100 100 97.3 96.3 97 96 75-125 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:53 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642459
QC Batch: 744044 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92642459001, 92642459002, 92642459003
METHOD BLANK: 3871223 Matrix:
Associated Lab Samples: 92642459001, 92642459002, 92642459003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
12/17/22 00:44
1,1,1-Trichloroethane
ug/L
ND
1.0
12/17/22 00:44
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/17/22 00:44
1,1,2-Trichloroethane
ug/L
ND
1.0
12/17/22 00:44
1,1-Dichloroethane
ug/L
ND
1.0
12/17/22 00:44
1,1-Dichloroethene
ug/L
ND
1.0
12/17/22 00:44
1,2,3-Trichloropropane
ug/L
ND
1.0
12/17/22 00:44
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
12/17/22 00:44
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/17/22 00:44
1,2-Dichlorobenzene
ug/L
ND
1.0
12/17/22 00:44
1,2-Dichloroethane
ug/L
ND
1.0
12/17/22 00:44
1,2-Dichloropropane
ug/L
ND
1.0
12/17/22 00:44
1,4-Dichlorobenzene
ug/L
ND
1.0
12/17/22 00:44
2-Butanone (MEK)
ug/L
ND
5.0
12/17/22 00:44
2-Hexanone
ug/L
ND
5.0
12/17/22 00:44
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/17/22 00:44
Acetone
ug/L
ND
25.0
12/17/22 00:44
Acrylonitrile
ug/L
ND
10.0
12/17/22 00:44
Benzene
ug/L
ND
1.0
12/17/22 00:44
Bromochloromethane
ug/L
ND
1.0
12/17/22 00:44
Bromodichloromethane
ug/L
ND
1.0
12/17/22 00:44
Bromoform
ug/L
ND
1.0
12/17/22 00:44
Bromomethane
ug/L
ND
2.0
12/17/22 00:44
Carbon disulfide
ug/L
ND
2.0
12/17/22 00:44
Carbon tetrachloride
ug/L
ND
1.0
12/17/22 00:44
Chlorobenzene
ug/L
ND
1.0
12/17/22 00:44
Chloroethane
ug/L
ND
1.0
12/17/22 00:44
Chloroform
ug/L
ND
1.0
12/17/22 00:44
Chloromethane
ug/L
ND
1.0
12/17/22 00:44
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/17/22 00:44
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/17/22 00:44
Dibromochloromethane
ug/L
ND
1.0
12/17/22 00:44
Dibromomethane
ug/L
ND
1.0
12/17/22 00:44
Ethylbenzene
ug/L
ND
1.0
12/17/22 00:44
lodomethane
ug/L
ND
20.0
12/17/22 00:44
m&p-Xylene
ug/L
ND
2.0
12/17/22 00:44
Methylene Chloride
ug/L
ND
5.0
12/17/22 00:44
o-Xylene
ug/L
ND
1.0
12/17/22 00:44
Styrene
ug/L
ND
1.0
12/17/22 00:44
Tetrachloroethene
ug/L
ND
1.0
12/17/22 00:44
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:53 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 21

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642459
METHOD BLANK: 3871223 Matrix:
Associated Lab Samples: 92642459001, 92642459002, 92642459003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
Toluene
ug/L
ND
1.0
12/17/22 00:44
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/17/22 00:44
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/17/22 00:44
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
12/17/22 00:44
Trichloroethene
ug/L
ND
1.0
12/17/22 00:44
Trichlorofluoromethane
ug/L
ND
1.0
12/17/22 00:44
Vinyl acetate
ug/L
ND
2.0
12/17/22 00:44
Vinyl chloride
ug/L
ND
1.0
12/17/22 00:44
Xylene (Total)
ug/L
ND
1.0
12/17/22 00:44
1,2-Dichloroethane-d4 (S)
%
106
70-130
12/17/22 00:44
4-Bromofluorobenzene (S)
%
103
70-130
12/17/22 00:44
Toluene-d8 (S)
%
106
70-130
12/17/22 00:44
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3871224
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.0
102
70-130
1,1,1-Trichloroethane
ug/L
50
49.5
99
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
48.3
97
70-130
1,1,2-Trichloroethane
ug/L
50
48.2
96
70-130
1,1-Dichloroethane
ug/L
50
46.1
92
70-130
1,1-Dichloroethene
ug/L
50
47.8
96
70-130
1,2,3-Trichloropropane
ug/L
50
48.6
97
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
52.3
105
70-131
1,2-Dibromoethane (EDB)
ug/L
50
51.9
104
70-130
1,2-Dichlorobenzene
ug/L
50
51.2
102
70-130
1,2-Dichloroethane
ug/L
50
48.3
97
70-130
1,2-Dichloropropane
ug/L
50
49.2
98
70-130
1,4-Dichlorobenzene
ug/L
50
50.2
100
70-130
2-Butanone (MEK)
ug/L
100
103
103
70-134
2-Hexanone
ug/L
100
96.1
96
70-131
4-Methyl-2-pentanone (MIBK)
ug/L
100
95.0
95
70-130
Acetone
ug/L
100
94.0
94
70-133
Acrylonitrile
ug/L
250
230
92
70-130
Benzene
ug/L
50
45.8
92
70-130
Bromochloromethane
ug/L
50
51.3
103
70-130
Bromodichloromethane
ug/L
50
48.8
98
70-130
Bromoform
ug/L
50
49.7
99
70-130
Bromomethane
ug/L
50
41.0
82
45-151
Carbon disulfide
ug/L
50
46.6
93
70-130
Carbon tetrachloride
ug/L
50
48.5
97
70-130
Chlorobenzene
ug/L
50
49.5
99
70-130
Chloroethane
ug/L
50
45.3
91
39-152
Chloroform
ug/L
50
44.7
89
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642459
LABORATORY CONTROL SAMPLE:
Parameter
3871224
Units
Spike LCS
Conc. Result
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
m&p-Xylene
ug/L
100
Methylene Chloride
ug/L
50
o-Xylene
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits
41.4
83
58-130
47.1
94
70-130
50.4
101
70-130
50.2
100
70-130
48.8
98
70-130
48.6
97
70-130
96.3
96
53-141
97.6
98
70-130
44.5
89
66-130
47.4
95
70-130
49.3
99
70-130
48.8
98
70-130
46.3
93
70-130
47.5
95
70-130
49.9
100
70-130
52.1
104
57-185
51.2
102
70-130
40.2
80
62-130
112
112
70-144
42.8
86
62-130
145
97
70-130
101
70-130
96
70-130
97
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3871225
MS
92641898022 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3871226
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
22.7
23.2
113
116
70-141
2
1,1,1-Trichloroethane
ug/L
ND
20
20
23.7
25.5
118
128
70-150
8
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.6
22.4
113
112
69-142
1
1,1,2-Trichloroethane
ug/L
ND
20
20
23.3
22.8
116
114
70-138
2
1,1-Dichloroethane
ug/L
ND
20
20
23.0
23.6
115
118
70-150
3
1,1-Dichloroethene
ug/L
ND
20
20
24.5
25.2
122
126
70-156
3
1,2,3-Trichloropropane
ug/L
ND
20
20
23.0
21.0
115
105
70-140
9
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
24.4
23.7
122
119
68-146
3
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.6
23.6
113
118
70-138
4
1,2-Dichlorobenzene
ug/L
ND
20
20
22.1
22.6
111
113
70-141
2
1,2-Dichloroethane
ug/L
ND
20
20
23.1
23.1
116
115
69-143
0
1,2-Dichloropropane
ug/L
ND
20
20
23.4
23.2
117
116
68-156
1
1,4-Dichlorobenzene
ug/L
ND
20
20
22.0
21.6
110
108
70-142
2
2-Butanone (MEK)
ug/L
ND
40
40
42.7
42.6
107
106
60-157
0 v1
2-Hexanone
ug/L
ND
40
40
44.6
43.9
112
110
68-146
2
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
43.9
42.9
110
107
70-141
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:53 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 21

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642459
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3871225
MS
92641898022 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3871226
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
43.1
45.4
108
114
58-157
5
Acrylonitrile
ug/L
ND
100
100
125
123
125
123
69-147
1
Benzene
ug/L
ND
20
20
22.1
22.1
111
111
70-142
0
Bromochloromethane
ug/L
ND
20
20
23.8
24.5
119
122
70-146
3
Bromodichloromethane
ug/L
ND
20
20
22.8
22.6
114
113
70-139
1
Bromoform
ug/L
ND
20
20
22.7
22.9
113
115
64-140
1
Bromomethane
ug/L
ND
20
20
23.1
22.5
115
112
28-192
3
Carbon disulfide
ug/L
ND
20
20
25.4
26.1
127
130
70-151
3
Carbon tetrachloride
ug/L
ND
20
20
25.2
25.0
126
125
70-148
1
Chlorobenzene
ug/L
ND
20
20
22.9
23.1
115
115
70-141
1
Chloroethane
ug/L
ND
20
20
23.3
24.7
116
124
58-191
6
Chloroform
ug/L
ND
20
20
22.8
23.7
113
118
70-148
4
Chloromethane
ug/L
ND
20
20
22.2
23.1
111
115
43-162
4
cis-1,2-Dichloroethene
ug/L
ND
20
20
22.9
24.6
114
123
68-151
7
cis-1,3-Dichloropropene
ug/L
ND
20
20
23.8
24.0
119
120
70-139
1
Dibromochloromethane
ug/L
ND
20
20
23.0
22.9
115
115
70-144
0
Dibromomethane
ug/L
ND
20
20
23.7
23.0
119
115
70-139
3
Ethylbenzene
ug/L
ND
20
20
23.2
22.9
116
114
70-143
2
lodomethane
ug/L
ND
40
40
41.3
43.7
103
109
35-171
6
m&p-Xylene
ug/L
ND
40
40
46.4
46.2
116
116
70-144
0
Methylene Chloride
ug/L
ND
20
20
21.8
22.2
109
111
62-149
2
o-Xylene
ug/L
ND
20
20
22.3
22.0
111
110
70-145
1
Styrene
ug/L
ND
20
20
22.2
22.0
111
110
70-143
1
Tetrachloroethene
ug/L
ND
20
20
23.2
23.4
116
117
70-145
1
Toluene
ug/L
ND
20
20
22.4
22.0
112
110
70-142
2
trans-1,2-Dichloroethene
ug/L
ND
20
20
24.2
24.9
121
125
70-151
3
trans- 1,3-Dichloropropene
ug/L
ND
20
20
23.7
23.7
119
118
70-139
0
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
22.9
20.7
115
104
51-159
10
Trichloroethene
ug/L
ND
20
20
24.1
24.1
120
120
62-146
0
Trichlorofluoromethane
ug/L
ND
20
20
21.1
22.0
105
110
63-153
4
Vinyl acetate
ug/L
ND
40
40
41.8
43.3
104
108
61-162
4
Vinyl chloride
ug/L
ND
20
20
22.1
23.2
111
116
61-163
5
Xylene (Total)
ug/L
ND
60
60
68.6
68.2
114
114
70-143
1
1,2-Dichloroethane-d4 (S)
%
104
112
70-130
4-Bromofluorobenzene (S)
%
102
101
70-130
Toluene-d8(S)
%
101
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:53 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 21

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QUALIFIERS
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642459
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
REPORT OF LABORATORY ANALYSIS
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[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642459
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92642459001
6001-HBW21
EPA 3010A
745958
EPA6010D
746019
92642459002
6001-HBW12B
EPA 3010A
745958
EPA6010D
746019
92642459001
6001-HBW21
EPA3005A
746005
EPA6020B
746121
92642459002
6001-HBW12B
EPA3005A
746005
EPA6020B
746121
92642459001
6001-HBW21
EPA 8260D
744044
92642459002
6001-HBW12B
EPA 8260D
744044
92642459003
TRIP BLANK
EPA 8260D
744044
Date: 01/06/2023 03:53 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 21

f-iiace „ i_.p—rrl.rrlu ­vriurttvrl upon meceipt
Effective Date: 05/12/202205/12/2022
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Raleigh[] Mechanicsville❑ Atlanta❑ Kernersville❑
Sample Condition Client Name: rWO# . 92642459 '
rrReceipt
1n I Project #:
Courier: MFed Ex ❑UPS ❑U05 ❑Client
❑ Commerciaf ❑Pace j I
❑Other,
926424-9
Custody Seal Present? ❑Yes []No Seals Intact? ❑Yes F No
Packing Material, Bubble Wrap I
❑ p ❑Bubble Bags ❑None ❑ Other
Thermomefer:
IR Gun ID: 91)vToD
Type of ice: L11Net ❑glue
—Correction Factor:
Cooler Temp: O' Add/Subtract {°C}
Cooler Temp Corrected If"-;
USDA Regulated Soil ( N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC
(check maps)? []Yes F1No
Chain of Custody Present?
✓ Yes
❑No
❑N/A
1.
Samples Arrived with in Bold Time?
dYes
❑No
❑N/A
2.
Short Hold Time Analysis (02 hr.)?
❑Yes
0No
❑N/A
3.
Rush Turn Around Time Requested?
Des
[]No
❑N/q
4.
Sufficient Volume?
dYes
❑No
[I N/A
S.
Correct Containers Used?
I�Yes
❑Na
❑N/A
6.
-Pace Containers Used?
❑yes
❑No
❑N/A
Containers Intact?
Yes
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
Des
❑No
[QN/A
d.
Sample Labels Match COC?
❑Yes
❑Na
❑N/A
9.
-Includes Aate/Time/lD/Analysis Matrix:
Headspace in V0A Vials (>5-6mm)? ❑yes I❑No ❑N/A 10.
Trip Blank Present? Ys ❑No ❑ N/A 11.
Trip Blank Custody Seals Present? ❑Yes ❑No ❑N/A
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
_f'roject147anager_SRFReview; --_
Qualtrax ID:69614
Date/Initials Person Examining Contents: {I'�
iS 2
Biological Tissue frozen?
❑Yes [:)No dN/A
❑None
Temp should be above freezing to 6'C
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source (internationally,
including Hawaii and Puerto Rico)? []Yes nNo
Field Data Required? Des ❑No
Lot la of split containers:
Date/Time:
Date:
Date; -- - — —
Page 1 of 2 Page 19 of 21

•� E vgll Et.71G VVlIIiF LI VII WVU1111GLGIt.JI
- ace
Effective Date: 05/12/202205/12/2022
r 9211642459
*Check mark top half of box if pH and/or dechlorination is verified and Project AW: _
within the acceptance range for preservation samples. PM: ASF Due Date: 12/28/22
Exceptions: VOA, Caliform, TOC, Oil and Grease, DRO/$015 (water) DOC, LLHg
CLIENT: 92-MECK CO
*'"Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
3t
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pH Adjustment Log for Preserved Samples
Sample to Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot p
adjusted added
Note: WKLIMYv�Tthere is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina OENR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
QLfaltrax ID: 69614 Page 2 of 2
Page 20 of 21

CHAIN -OF -CUSTODY 1 Analytical Request Document
GE
`- The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Submilting a sample via this chain of custody constitutes acknowledgment and acceptance of the Pace Terms and Conditions found at https://info.pacelabs.comlhubfsfpas-standard-terms.pdf.
tion A Section 8
ce.r..., r
Page 21 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
January 06, 2023
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on December 13, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Ariel S Fitzgerald
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 28

lacmnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92642465001 6001-HB2006
EPA 601OD
DRB
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
SAS
52
PASI-C
92642465002 6001-HB2008
EPA 601OD
DRB
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
SAS
52
PASI-C
92642465003 6001-HB2010
EPA 601OD
DRB
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
SAS
52
PASI-C
92642465004 TRIP BLANK
EPA 8260D
JJK
52
PASI-C
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
Sample: 6001-HB2006 Lab ID: 92642465001 Collected: 12/13/22 12:58 Received: 12/13/22 14:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
12/27/22 14:40
12/28/22 01:40
7440-38-2
Beryllium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:40
7440-41-7
Barium
27.1
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:40
7440-39-3
Cadmium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:40
7440-43-9
Chromium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:40
7440-47-3
Copper
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:40
7440-50-8
Nickel
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:40
7440-02-0
Silver
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:40
7440-22-4
Lead
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:40
7439-92-1
Antimony
ND
ug/L
50.0
1
12/27/22 14:40
12/28/22 01:40
7440-36-0
Selenium
ND
ug/L
40.0
1
12/27/22 14:40
12/28/22 01:40
7782-49-2
Thallium
ND
ug/L
200
1
12/27/22 14:40
12/28/22 01:40
7440-28-0
Vanadium
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:40
7440-62-2
Zinc
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:40
7440-66-6
Cobalt
ND
ug/L
40.0
1
12/27/22 14:40
12/28/22 01:40
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
12/27/2217:44
01/03/2316:08
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/17/22 02:50
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/17/22 02:50
107-13-1
Benzene
ND
ug/L
1.0
1
12/17/22 02:50
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/17/22 02:50
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/17/22 02:50
75-27-4
Bromoform
ND
ug/L
1.0
1
12/17/22 02:50
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/17/22 02:50
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/17/22 02:50
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/17/22 02:50
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/17/22 02:50
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/17/22 02:50
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/17/22 02:50
75-00-3
Chloroform
ND
ug/L
1.0
1
12/17/22 02:50
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/17/22 02:50
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/17/22 02:50
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/17/22 02:50
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/17/22 02:50
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/17/22 02:50
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/17/22 02:50
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/17/22 02:50
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/17/22 02:50
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/17/22 02:50
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/17/22 02:50
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:54 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
Sample: 6001-HB2006 Lab ID: 92642465001 Collected: 12/13/22 12:58 Received: 12/13/22 14:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/17/22 02:50
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/17/22 02:50
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/17/22 02:50
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/17/22 02:50
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/17/22 02:50
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/17/22 02:50
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/17/22 02:50
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/17/22 02:50
591-78-6
lodomethane
ND
ug/L
20.0
1
12/17/22 02:50
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/17/22 02:50
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/17/22 02:50
108-10-1
Styrene
ND
ug/L
1.0
1
12/17/22 02:50
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/17/22 02:50
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/17/22 02:50
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/17/22 02:50
127-18-4
Toluene
ND
ug/L
1.0
1
12/17/22 02:50
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/17/22 02:50
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/17/22 02:50
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/17/22 02:50
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/17/22 02:50
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/17/22 02:50
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/17/22 02:50
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/17/22 02:50
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/17/22 02:50
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/17/22 02:50
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/17/22 02:50
95-47-6
Surrogates
4-Bromofluorobenzene (S)
101
%
70-130
1
12/17/22 02:50
460-00-4
1,2-Dichloroethane-d4 (S)
105
%
70-130
1
12/17/22 02:50
17060-07-0
Toluene-d8(S)
105
%
70-130
1
12/17/22 02:50
2037-26-5
Date: 01/06/2023 03:54 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
Sample: 6001-HB2008 Lab ID: 92642465002 Collected: 12/13/22 13:10 Received: 12/13/22 14:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
12/27/22 14:40
12/28/22 01:45
7440-38-2
Beryllium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:45
7440-41-7
Barium
20.7
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:45
7440-39-3
Cadmium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:45
7440-43-9
Chromium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:45
7440-47-3
Copper
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:45
7440-50-8
Nickel
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:45
7440-02-0
Silver
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:45
7440-22-4
Lead
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:45
7439-92-1
Antimony
ND
ug/L
50.0
1
12/27/22 14:40
12/28/22 01:45
7440-36-0
Selenium
ND
ug/L
40.0
1
12/27/22 14:40
12/28/22 01:45
7782-49-2
Thallium
ND
ug/L
200
1
12/27/22 14:40
12/28/22 01:45
7440-28-0
Vanadium
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:45
7440-62-2
Zinc
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:45
7440-66-6
Cobalt
ND
ug/L
40.0
1
12/27/22 14:40
12/28/22 01:45
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
12/27/2217:44
01/03/2316:14
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/17/22 03:08
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/17/22 03:08
107-13-1
Benzene
ND
ug/L
1.0
1
12/17/22 03:08
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/17/22 03:08
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/17/22 03:08
75-27-4
Bromoform
ND
ug/L
1.0
1
12/17/22 03:08
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/17/22 03:08
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/17/22 03:08
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/17/22 03:08
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/17/22 03:08
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/17/22 03:08
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/17/22 03:08
75-00-3
Chloroform
ND
ug/L
1.0
1
12/17/22 03:08
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/17/22 03:08
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/17/22 03:08
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/17/22 03:08
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/17/22 03:08
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/17/22 03:08
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/17/22 03:08
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/17/22 03:08
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/17/22 03:08
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/17/22 03:08
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/17/22 03:08
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:54 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
Sample: 6001-HB2008 Lab ID: 92642465002 Collected: 12/13/22 13:10 Received: 12/13/22 14:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/17/22 03:08
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/17/22 03:08
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/17/22 03:08
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/17/22 03:08
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/17/22 03:08
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/17/22 03:08
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/17/22 03:08
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/17/22 03:08
591-78-6
lodomethane
ND
ug/L
20.0
1
12/17/22 03:08
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/17/22 03:08
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/17/22 03:08
108-10-1
Styrene
ND
ug/L
1.0
1
12/17/22 03:08
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/17/22 03:08
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/17/22 03:08
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/17/22 03:08
127-18-4
Toluene
ND
ug/L
1.0
1
12/17/22 03:08
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/17/22 03:08
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/17/22 03:08
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/17/22 03:08
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/17/22 03:08
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/17/22 03:08
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/17/22 03:08
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/17/22 03:08
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/17/22 03:08
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/17/22 03:08
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/17/22 03:08
95-47-6
Surrogates
4-Bromofluorobenzene (S)
101
%
70-130
1
12/17/22 03:08
460-00-4
1,2-Dichloroethane-d4 (S)
104
%
70-130
1
12/17/22 03:08
17060-07-0
Toluene-d8 (S)
111
%
70-130
1
12/17/22 03:08
2037-26-5
Date: 01/06/2023 03:54 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
Sample: 6001-HB2010 Lab ID: 92642465003 Collected: 12/13/22 11:00 Received: 12/13/22 14:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
12/27/22 14:40
12/28/22 01:50
7440-38-2
Beryllium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:50
7440-41-7
Barium
49.4
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:50
7440-39-3
Cadmium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:50
7440-43-9
Chromium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:50
7440-47-3
Copper
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:50
7440-50-8
Nickel
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:50
7440-02-0
Silver
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 01:50
7440-22-4
Lead
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:50
7439-92-1
Antimony
ND
ug/L
50.0
1
12/27/22 14:40
12/28/22 01:50
7440-36-0
Selenium
ND
ug/L
40.0
1
12/27/22 14:40
12/28/22 01:50
7782-49-2
Thallium
ND
ug/L
200
1
12/27/22 14:40
12/28/22 01:50
7440-28-0
Vanadium
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:50
7440-62-2
Zinc
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 01:50
7440-66-6
Cobalt
ND
ug/L
40.0
1
12/27/22 14:40
12/28/22 01:50
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
12/27/2217:44
01/03/2316:20
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/17/22 03:26
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/17/22 03:26
107-13-1
Benzene
ND
ug/L
1.0
1
12/17/22 03:26
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/17/22 03:26
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/17/22 03:26
75-27-4
Bromoform
ND
ug/L
1.0
1
12/17/22 03:26
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/17/22 03:26
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/17/22 03:26
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/17/22 03:26
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/17/22 03:26
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/17/22 03:26
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/17/22 03:26
75-00-3
Chloroform
ND
ug/L
1.0
1
12/17/22 03:26
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/17/22 03:26
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/17/22 03:26
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/17/22 03:26
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/17/22 03:26
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/17/22 03:26
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/17/22 03:26
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/17/22 03:26
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/17/22 03:26
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/17/22 03:26
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/17/22 03:26
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:54 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
Sample: 6001-HB2010 Lab ID: 92642465003 Collected: 12/13/22 11:00 Received: 12/13/22 14:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/17/22 03:26
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/17/22 03:26
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/17/22 03:26
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/17/22 03:26
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/17/22 03:26
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/17/22 03:26
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/17/22 03:26
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/17/22 03:26
591-78-6
lodomethane
ND
ug/L
20.0
1
12/17/22 03:26
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/17/22 03:26
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/17/22 03:26
108-10-1
Styrene
ND
ug/L
1.0
1
12/17/22 03:26
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/17/22 03:26
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/17/22 03:26
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/17/22 03:26
127-18-4
Toluene
ND
ug/L
1.0
1
12/17/22 03:26
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/17/22 03:26
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/17/22 03:26
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/17/22 03:26
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/17/22 03:26
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/17/22 03:26
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/17/22 03:26
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/17/22 03:26
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/17/22 03:26
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/17/22 03:26
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/17/22 03:26
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
12/17/22 03:26
460-00-4
1,2-Dichloroethane-d4 (S)
104
%
70-130
1
12/17/22 03:26
17060-07-0
Toluene-d8 (S)
108
%
70-130
1
12/17/22 03:26
2037-26-5
Date: 01/06/2023 03:54 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
Sample: TRIP BLANK
Lab ID: 92642465004 Collected:
12/13/22
00:00
Received: 12/13/22 14:38 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/20/22 01:29
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/20/22 01:29
107-13-1
Benzene
ND
ug/L
1.0
1
12/20/22 01:29
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/20/22 01:29
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/20/22 01:29
75-27-4
Bromoform
ND
ug/L
1.0
1
12/20/22 01:29
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/20/22 01:29
74-83-9 v2
2-Butanone (MEK)
ND
ug/L
5.0
1
12/20/22 01:29
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/20/22 01:29
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/20/22 01:29
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/20/22 01:29
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/20/22 01:29
75-00-3
Chloroform
ND
ug/L
1.0
1
12/20/22 01:29
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/20/22 01:29
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/20/22 01:29
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/20/22 01:29
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/20/22 01:29
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/20/22 01:29
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/20/22 01:29
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/20/22 01:29
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/20/22 01:29
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/20/22 01:29
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/20/22 01:29
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/20/22 01:29
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/20/22 01:29
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/20/22 01:29
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/20/22 01:29
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/20/22 01:29
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/20/22 01:29
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/20/22 01:29
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/20/22 01:29
591-78-6
lodomethane
ND
ug/L
20.0
1
12/20/22 01:29
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
1
12/20/22 01:29
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/20/22 01:29
108-10-1
Styrene
ND
ug/L
1.0
1
12/20/22 01:29
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/20/22 01:29
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/20/22 01:29
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/20/22 01:29
127-18-4
Toluene
ND
ug/L
1.0
1
12/20/22 01:29
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/20/22 01:29
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/20/22 01:29
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/20/22 01:29
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/20/22 01:29
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/20/22 01:29
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/20/22 01:29
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/20/22 01:29
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:54 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 28

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ANALYTICAL RESULTS
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
Sample: TRIP BLANK
Parameters
Lab ID: 92642465004 Collected: 12/13/22 00:00
Results Units Report Limit DF
Received: 12/13/22 14:38 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
12/20/22 01:29
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
12/20/22 01:29
179601-23-1
o-Xylene
ND ug/L
1.0
1
12/20/22 01:29
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99 %
70-130
1
12/20/22 01:29
460-00-4
1,2-Dichloroethane-d4 (S)
98 %
70-130
1
12/20/22 01:29
17060-07-0
Toluene-d8(S)
100 %
70-130
1
12/20/22 01:29
2037-26-5
Date: 01/06/2023 03:54 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 28

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QUALITY CONTROL DATA
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
QC Batch: 745958 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 601 OD ATL
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92642465001, 92642465002, 92642465003
METHOD BLANK: 3880043 Matrix: Water
Associated Lab Samples: 92642465001, 92642465002, 92642465003
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
50.0
12/28/22 00:08
30.0
12/28/22 00:08
10.0
12/28/22 00:08
10.0
12/28/22 00:08
10.0
12/28/22 00:08
10.0
12/28/22 00:08
40.0
12/28/22 00:08
20.0
12/28/22 00:08
20.0
12/28/22 00:08
20.0
12/28/22 00:08
40.0
12/28/22 00:08
10.0
12/28/22 00:08
200
12/28/22 00:08
20.0
12/28/22 00:08
20.0
12/28/22 00:08
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3880044
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
1000
1060
106
80-120
Arsenic
ug/L
1000
1070
107
80-120
Barium
ug/L
1000
1040
104
80-120
Beryllium
ug/L
1000
1070
107
80-120
Cadmium
ug/L
1000
1070
107
80-120
Chromium
ug/L
1000
1050
105
80-120
Cobalt
ug/L
1000
1070
107
80-120
Copper
ug/L
1000
1050
105
80-120
Lead
ug/L
1000
1070
107
80-120
Nickel
ug/L
1000
1080
108
80-120
Selenium
ug/L
1000
1070
107
80-120
Silver
ug/L
1000
1020
102
80-120
Thallium
ug/L
1000
1030
103
80-120
Vanadium
ug/L
1000
1120
112
80-120
Zinc
ug/L
1000
1070
107
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:54 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 28

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QUALITY CONTROL DATA
Project:
Pace Project No.:
HARRISBURG ROAD LANDFILL
92642465
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3880045
3880046
MS
MSD
92641048001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
1000
1000
1060
1090
105
108
75-125
3
Arsenic
ug/L
ND
1000
1000
1070
1100
107
110
75-125
2
Barium
ug/L
76.5
1000
1000
1120
1140
104
107
75-125
2
Beryllium
ug/L
ND
1000
1000
1070
1100
107
109
75-125
3
Cadmium
ug/L
ND
1000
1000
1070
1090
107
109
75-125
3
Chromium
ug/L
ND
1000
1000
1060
1080
106
108
75-125
1
Cobalt
ug/L
20AJ
1000
1000
1090
1110
107
109
75-125
2
Copper
ug/L
20.OJ
1000
1000
1100
1120
108
110
75-125
2
Lead
ug/L
ND
1000
1000
1070
1100
105
108
75-125
3
Nickel
ug/L
27.0
1000
1000
1100
1120
107
110
75-125
2
Selenium
ug/L
ND
1000
1000
1020
1030
102
103
75-125
1
Silver
ug/L
ND
1000
1000
1040
1050
104
105
75-125
1
Thallium
ug/L
ND
1000
1000
1040
1070
104
107
75-125
2
Vanadium
ug/L
ND
1000
1000
1140
1160
114
116
75-125
2
Zinc
ug/L
13.1 J
1000
1000
1050
1080
103
107
75-125
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01 /06/2023 03:54 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 28

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
QC Batch: 746005 Analysis Method: EPA 6020B
QC Batch Method: EPA 3005A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92642465001, 92642465002, 92642465003
METHOD BLANK: 3880266
Matrix:
Water
Associated Lab Samples: 92642465001, 92642465002, 92642465003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
1.0
01/03/2314:31
LABORATORY CONTROL SAMPLE:
3880267
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
100
101
101 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3880268 3880269
MS MSD
92641696001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L 0.18J 100 100 97.3 96.3 97 96 75-125 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01 /06/2023 03:54 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 28

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
QC Batch: 744044 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92642465001, 92642465002, 92642465003
METHOD BLANK: 3871223 Matrix:
Associated Lab Samples: 92642465001, 92642465002, 92642465003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
12/17/22 00:44
1,1,1-Trichloroethane
ug/L
ND
1.0
12/17/22 00:44
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/17/22 00:44
1,1,2-Trichloroethane
ug/L
ND
1.0
12/17/22 00:44
1,1-Dichloroethane
ug/L
ND
1.0
12/17/22 00:44
1,1-Dichloroethene
ug/L
ND
1.0
12/17/22 00:44
1,2,3-Trichloropropane
ug/L
ND
1.0
12/17/22 00:44
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
12/17/22 00:44
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/17/22 00:44
1,2-Dichlorobenzene
ug/L
ND
1.0
12/17/22 00:44
1,2-Dichloroethane
ug/L
ND
1.0
12/17/22 00:44
1,2-Dichloropropane
ug/L
ND
1.0
12/17/22 00:44
1,4-Dichlorobenzene
ug/L
ND
1.0
12/17/22 00:44
2-Butanone (MEK)
ug/L
ND
5.0
12/17/22 00:44
2-Hexanone
ug/L
ND
5.0
12/17/22 00:44
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/17/22 00:44
Acetone
ug/L
ND
25.0
12/17/22 00:44
Acrylonitrile
ug/L
ND
10.0
12/17/22 00:44
Benzene
ug/L
ND
1.0
12/17/22 00:44
Bromochloromethane
ug/L
ND
1.0
12/17/22 00:44
Bromodichloromethane
ug/L
ND
1.0
12/17/22 00:44
Bromoform
ug/L
ND
1.0
12/17/22 00:44
Bromomethane
ug/L
ND
2.0
12/17/22 00:44
Carbon disulfide
ug/L
ND
2.0
12/17/22 00:44
Carbon tetrachloride
ug/L
ND
1.0
12/17/22 00:44
Chlorobenzene
ug/L
ND
1.0
12/17/22 00:44
Chloroethane
ug/L
ND
1.0
12/17/22 00:44
Chloroform
ug/L
ND
1.0
12/17/22 00:44
Chloromethane
ug/L
ND
1.0
12/17/22 00:44
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/17/22 00:44
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/17/22 00:44
Dibromochloromethane
ug/L
ND
1.0
12/17/22 00:44
Dibromomethane
ug/L
ND
1.0
12/17/22 00:44
Ethylbenzene
ug/L
ND
1.0
12/17/22 00:44
lodomethane
ug/L
ND
20.0
12/17/22 00:44
m&p-Xylene
ug/L
ND
2.0
12/17/22 00:44
Methylene Chloride
ug/L
ND
5.0
12/17/22 00:44
o-Xylene
ug/L
ND
1.0
12/17/22 00:44
Styrene
ug/L
ND
1.0
12/17/22 00:44
Tetrachloroethene
ug/L
ND
1.0
12/17/22 00:44
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:54 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 28

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
METHOD BLANK: 3871223 Matrix:
Associated Lab Samples: 92642465001, 92642465002, 92642465003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
Toluene
ug/L
ND
1.0
12/17/22 00:44
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/17/22 00:44
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/17/22 00:44
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
12/17/22 00:44
Trichloroethene
ug/L
ND
1.0
12/17/22 00:44
Trichlorofluoromethane
ug/L
ND
1.0
12/17/22 00:44
Vinyl acetate
ug/L
ND
2.0
12/17/22 00:44
Vinyl chloride
ug/L
ND
1.0
12/17/22 00:44
Xylene (Total)
ug/L
ND
1.0
12/17/22 00:44
1,2-Dichloroethane-d4 (S)
%
106
70-130
12/17/22 00:44
4-Bromofluorobenzene (S)
%
103
70-130
12/17/22 00:44
Toluene-d8 (S)
%
106
70-130
12/17/22 00:44
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3871224
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.0
102
70-130
1,1,1-Trichloroethane
ug/L
50
49.5
99
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
48.3
97
70-130
1,1,2-Trichloroethane
ug/L
50
48.2
96
70-130
1,1-Dichloroethane
ug/L
50
46.1
92
70-130
1,1-Dichloroethene
ug/L
50
47.8
96
70-130
1,2,3-Trichloropropane
ug/L
50
48.6
97
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
52.3
105
70-131
1,2-Dibromoethane (EDB)
ug/L
50
51.9
104
70-130
1,2-Dichlorobenzene
ug/L
50
51.2
102
70-130
1,2-Dichloroethane
ug/L
50
48.3
97
70-130
1,2-Dichloropropane
ug/L
50
49.2
98
70-130
1,4-Dichlorobenzene
ug/L
50
50.2
100
70-130
2-Butanone (MEK)
ug/L
100
103
103
70-134
2-Hexanone
ug/L
100
96.1
96
70-131
4-Methyl-2-pentanone (MIBK)
ug/L
100
95.0
95
70-130
Acetone
ug/L
100
94.0
94
70-133
Acrylonitrile
ug/L
250
230
92
70-130
Benzene
ug/L
50
45.8
92
70-130
Bromochloromethane
ug/L
50
51.3
103
70-130
Bromodichloromethane
ug/L
50
48.8
98
70-130
Bromoform
ug/L
50
49.7
99
70-130
Bromomethane
ug/L
50
41.0
82
45-151
Carbon disulfide
ug/L
50
46.6
93
70-130
Carbon tetrachloride
ug/L
50
48.5
97
70-130
Chlorobenzene
ug/L
50
49.5
99
70-130
Chloroethane
ug/L
50
45.3
91
39-152
Chloroform
ug/L
50
44.7
89
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:54 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 28

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[phone]
QUALITY CONTROL DATA
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
LABORATORY CONTROL SAMPLE:
Parameter
3871224
Units
Spike LCS
Conc. Result
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
m&p-Xylene
ug/L
100
Methylene Chloride
ug/L
50
o-Xylene
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits
41.4
83
58-130
47.1
94
70-130
50.4
101
70-130
50.2
100
70-130
48.8
98
70-130
48.6
97
70-130
96.3
96
53-141
97.6
98
70-130
44.5
89
66-130
47.4
95
70-130
49.3
99
70-130
48.8
98
70-130
46.3
93
70-130
47.5
95
70-130
49.9
100
70-130
52.1
104
57-185
51.2
102
70-130
40.2
80
62-130
112
112
70-144
42.8
86
62-130
145
97
70-130
101
70-130
96
70-130
97
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3871225
MS
92641898022 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3871226
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
22.7
23.2
113
116
70-141
2
1,1,1-Trichloroethane
ug/L
ND
20
20
23.7
25.5
118
128
70-150
8
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.6
22.4
113
112
69-142
1
1,1,2-Trichloroethane
ug/L
ND
20
20
23.3
22.8
116
114
70-138
2
1,1-Dichloroethane
ug/L
ND
20
20
23.0
23.6
115
118
70-150
3
1,1-Dichloroethene
ug/L
ND
20
20
24.5
25.2
122
126
70-156
3
1,2,3-Trichloropropane
ug/L
ND
20
20
23.0
21.0
115
105
70-140
9
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
24.4
23.7
122
119
68-146
3
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.6
23.6
113
118
70-138
4
1,2-Dichlorobenzene
ug/L
ND
20
20
22.1
22.6
111
113
70-141
2
1,2-Dichloroethane
ug/L
ND
20
20
23.1
23.1
116
115
69-143
0
1,2-Dichloropropane
ug/L
ND
20
20
23.4
23.2
117
116
68-156
1
1,4-Dichlorobenzene
ug/L
ND
20
20
22.0
21.6
110
108
70-142
2
2-Butanone (MEK)
ug/L
ND
40
40
42.7
42.6
107
106
60-157
0 v1
2-Hexanone
ug/L
ND
40
40
44.6
43.9
112
110
68-146
2
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
43.9
42.9
110
107
70-141
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:54 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3871225
MS
92641898022 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3871226
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
43.1
45.4
108
114
58-157
5
Acrylonitrile
ug/L
ND
100
100
125
123
125
123
69-147
1
Benzene
ug/L
ND
20
20
22.1
22.1
111
111
70-142
0
Bromochloromethane
ug/L
ND
20
20
23.8
24.5
119
122
70-146
3
Bromodichloromethane
ug/L
ND
20
20
22.8
22.6
114
113
70-139
1
Bromoform
ug/L
ND
20
20
22.7
22.9
113
115
64-140
1
Bromomethane
ug/L
ND
20
20
23.1
22.5
115
112
28-192
3
Carbon disulfide
ug/L
ND
20
20
25.4
26.1
127
130
70-151
3
Carbon tetrachloride
ug/L
ND
20
20
25.2
25.0
126
125
70-148
1
Chlorobenzene
ug/L
ND
20
20
22.9
23.1
115
115
70-141
1
Chloroethane
ug/L
ND
20
20
23.3
24.7
116
124
58-191
6
Chloroform
ug/L
ND
20
20
22.8
23.7
113
118
70-148
4
Chloromethane
ug/L
ND
20
20
22.2
23.1
111
115
43-162
4
cis-1,2-Dichloroethene
ug/L
ND
20
20
22.9
24.6
114
123
68-151
7
cis-1,3-Dichloropropene
ug/L
ND
20
20
23.8
24.0
119
120
70-139
1
Dibromochloromethane
ug/L
ND
20
20
23.0
22.9
115
115
70-144
0
Dibromomethane
ug/L
ND
20
20
23.7
23.0
119
115
70-139
3
Ethylbenzene
ug/L
ND
20
20
23.2
22.9
116
114
70-143
2
lodomethane
ug/L
ND
40
40
41.3
43.7
103
109
35-171
6
m&p-Xylene
ug/L
ND
40
40
46.4
46.2
116
116
70-144
0
Methylene Chloride
ug/L
ND
20
20
21.8
22.2
109
111
62-149
2
o-Xylene
ug/L
ND
20
20
22.3
22.0
111
110
70-145
1
Styrene
ug/L
ND
20
20
22.2
22.0
111
110
70-143
1
Tetrachloroethene
ug/L
ND
20
20
23.2
23.4
116
117
70-145
1
Toluene
ug/L
ND
20
20
22.4
22.0
112
110
70-142
2
trans-1,2-Dichloroethene
ug/L
ND
20
20
24.2
24.9
121
125
70-151
3
trans- 1,3-Dichloropropene
ug/L
ND
20
20
23.7
23.7
119
118
70-139
0
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
22.9
20.7
115
104
51-159
10
Trichloroethene
ug/L
ND
20
20
24.1
24.1
120
120
62-146
0
Trichlorofluoromethane
ug/L
ND
20
20
21.1
22.0
105
110
63-153
4
Vinyl acetate
ug/L
ND
40
40
41.8
43.3
104
108
61-162
4
Vinyl chloride
ug/L
ND
20
20
22.1
23.2
111
116
61-163
5
Xylene (Total)
ug/L
ND
60
60
68.6
68.2
114
114
70-143
1
1,2-Dichloroethane-d4 (S)
%
104
112
70-130
4-Bromofluorobenzene (S)
%
102
101
70-130
Toluene-d8(S)
%
101
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:54 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
QC Batch: 744438 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92642465004
METHOD BLANK: 3872965
Associated Lab Samples: 92642465004
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
12/20/22 01:11
1,1,1-Trichloroethane
ug/L
ND
1.0
12/20/22 01:11
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/20/22 01:11
1,1,2-Trichloroethane
ug/L
ND
1.0
12/20/22 01:11
1,1-Dichloroethane
ug/L
ND
1.0
12/20/22 01:11
1,1-Dichloroethene
ug/L
ND
1.0
12/20/22 01:11
1,2,3-Trichloropropane
ug/L
ND
1.0
12/20/22 01:11
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
12/20/22 01:11
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/20/22 01:11
1,2-Dichlorobenzene
ug/L
ND
1.0
12/20/22 01:11
1,2-Dichloroethane
ug/L
ND
1.0
12/20/22 01:11
1,2-Dichloropropane
ug/L
ND
1.0
12/20/22 01:11
1,4-Dichlorobenzene
ug/L
ND
1.0
12/20/22 01:11
2-Butanone (MEK)
ug/L
ND
5.0
12/20/22 01:11
2-Hexanone
ug/L
ND
5.0
12/20/22 01:11
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/20/22 01:11
Acetone
ug/L
ND
25.0
12/20/22 01:11
Acrylonitrile
ug/L
ND
10.0
12/20/22 01:11
Benzene
ug/L
ND
1.0
12/20/22 01:11
Bromochloromethane
ug/L
ND
1.0
12/20/22 01:11
Bromodichloromethane
ug/L
ND
1.0
12/20/22 01:11
Bromoform
ug/L
ND
1.0
12/20/22 01:11
Bromomethane
ug/L
ND
2.0
12/20/22 01:11
Carbon disulfide
ug/L
ND
2.0
12/20/22 01:11
Carbon tetrachloride
ug/L
ND
1.0
12/20/22 01:11
Chlorobenzene
ug/L
ND
1.0
12/20/22 01:11
Chloroethane
ug/L
ND
1.0
12/20/22 01:11
Chloroform
ug/L
ND
1.0
12/20/22 01:11
Chloromethane
ug/L
ND
1.0
12/20/22 01:11
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/20/22 01:11
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/20/22 01:11
Dibromochloromethane
ug/L
ND
1.0
12/20/22 01:11
Dibromomethane
ug/L
ND
1.0
12/20/22 01:11
Ethylbenzene
ug/L
ND
1.0
12/20/22 01:11
lodomethane
ug/L
ND
20.0
12/20/22 01:11
m&p-Xylene
ug/L
ND
2.0
12/20/22 01:11
Methylene Chloride
ug/L
ND
5.0
12/20/22 01:11
o-Xylene
ug/L
ND
1.0
12/20/22 01:11
Styrene
ug/L
ND
1.0
12/20/22 01:11
Tetrachloroethene
ug/L
ND
1.0
12/20/22 01:11
v2
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:54 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
METHOD BLANK: 3872965
Associated Lab Samples: 92642465004
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed Qualifiers
Toluene
ug/L
ND
1.0
12/20/22 01:11
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/20/22 01:11
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/20/22 01:11
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
12/20/22 01:11
Trichloroethene
ug/L
ND
1.0
12/20/22 01:11
Trichlorofluoromethane
ug/L
ND
1.0
12/20/22 01:11
Vinyl acetate
ug/L
ND
2.0
12/20/22 01:11
Vinyl chloride
ug/L
ND
1.0
12/20/22 01:11
Xylene (Total)
ug/L
ND
1.0
12/20/22 01:11
1,2-Dichloroethane-d4 (S)
%
91
70-130
12/20/22 01:11
4-Bromofluorobenzene (S)
%
99
70-130
12/20/22 01:11
Toluene-d8 (S)
%
95
70-130
12/20/22 01:11
LABORATORY CONTROL SAMPLE:
Parameter
3872966
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
50.3
101
70-130
1,1,1-Trichloroethane
ug/L
50
47.6
95
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
49.2
98
70-130
1,1,2-Trichloroethane
ug/L
50
52.0
104
70-130
1,1-Dichloroethane
ug/L
50
47.6
95
70-130
1,1-Dichloroethene
ug/L
50
45.4
91
70-130
1,2,3-Trichloropropane
ug/L
50
45.2
90
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
54.3
109
70-131
1,2-Dibromoethane (EDB)
ug/L
50
49.9
100
70-130
1,2-Dichlorobenzene
ug/L
50
49.5
99
70-130
1,2-Dichloroethane
ug/L
50
43.4
87
70-130
1,2-Dichloropropane
ug/L
50
52.0
104
70-130
1,4-Dichlorobenzene
ug/L
50
49.3
99
70-130
2-Butanone (MEK)
ug/L
100
98.1
98
70-134
2-Hexanone
ug/L
100
107
107
70-131
4-Methyl-2-pentanone (MIBK)
ug/L
100
109
109
70-130
Acetone
ug/L
100
91.2
91
70-133
Acrylonitrile
ug/L
250
269
108
70-130
Benzene
ug/L
50
45.3
91
70-130
Bromochloromethane
ug/L
50
49.9
100
70-130
Bromodichloromethane
ug/L
50
51.0
102
70-130
Bromoform
ug/L
50
51.9
104
70-130
Bromomethane
ug/L
50
40.5
81
45-151 v3
Carbon disulfide
ug/L
50
45.8
92
70-130
Carbon tetrachloride
ug/L
50
49.6
99
70-130
Chlorobenzene
ug/L
50
48.7
97
70-130
Chloroethane
ug/L
50
49.4
99
39-152
Chloroform
ug/L
50
46.1
92
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:54 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
LABORATORY CONTROL SAMPLE:
3872966
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Chloromethane
ug/L
50
47.2
94
58-130
cis-1,2-Dichloroethene
ug/L
50
48.9
98
70-130
cis-1,3-Dichloropropene
ug/L
50
53.5
107
70-130
Dibromochloromethane
ug/L
50
49.3
99
70-130
Dibromomethane
ug/L
50
52.8
106
70-130
Ethylbenzene
ug/L
50
48.9
98
70-130
lodomethane
ug/L
100
93.3
93
53-141 v3
m&p-Xylene
ug/L
100
99.9
100
70-130
Methylene Chloride
ug/L
50
45.8
92
66-130
o-Xylene
ug/L
50
50.2
100
70-130
Styrene
ug/L
50
52.4
105
70-130
Tetrachloroethene
ug/L
50
45.7
91
70-130
Toluene
ug/L
50
50.3
101
70-130
trans-1,2-Dichloroethene
ug/L
50
48.7
97
70-130
trans- 1,3-Dichloropropene
ug/L
50
53.7
107
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
47.0
94
57-185
Trichloroethene
ug/L
50
50.5
101
70-130
Trichlorofluoromethane
ug/L
50
39.5
79
62-130
Vinyl acetate
ug/L
100
99.2
99
70-144
Vinyl chloride
ug/L
50
47.4
95
62-130
Xylene (Total)
ug/L
150
150
100
70-130
1,2-Dichloroethane-d4 (S)
%
84
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
105
70-130
MATRIX SPIKE SAMPLE:
3872970
92642468002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
27.7
139
70-141
1,1,1-Trichloroethane
ug/L
ND
20
29.6
148
70-150
1,1,2,2-Tetrachloroethane
ug/L
ND
20
25.4
127
69-142
1,1,2-Trichloroethane
ug/L
ND
20
28.2
141
70-138 M1
1,1-Dichloroethane
ug/L
1.0
20
30.7
149
70-150
1,1-Dichloroethene
ug/L
ND
20
31.0
155
70-156
1,2,3-Trichloropropane
ug/L
ND
20
24.8
124
70-140
1,2-Dibromo-3-chloropropane
ug/L
ND
20
26.4
132
68-146
1,2-Dibromoethane (EDB)
ug/L
ND
20
27.0
135
70-138
1,2-Dichlorobenzene
ug/L
ND
20
25.0
125
70-141
1,2-Dichloroethane
ug/L
ND
20
28.4
142
69-143
1,2-Dichloropropane
ug/L
ND
20
28.6
143
68-156
1,4-Dichlorobenzene
ug/L
ND
20
25.0
125
70-142
2-Butanone (MEK)
ug/L
ND
40
55.9
140
60-157
2-Hexanone
ug/L
ND
40
52.6
132
68-146
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
52.4
131
70-141
Acetone
ug/L
ND
40
51.9
128
58-157
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:54 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
MATRIX SPIKE SAMPLE:
3872970
92642468002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Acrylonitrile
ug/L
ND
100
146
146
69-147
Benzene
ug/L
ND
20
27.1
135
70-142
Bromochloromethane
ug/L
ND
20
29.9
149
70-146 M1
Bromodichloromethane
ug/L
ND
20
27.7
139
70-139
Bromoform
ug/L
ND
20
26.9
134
64-140
Bromomethane
ug/L
ND
20
21.5
108
28-192
Carbon disulfide
ug/L
ND
20
29.0
145
70-151
Carbon tetrachloride
ug/L
ND
20
27.5
138
70-148
Chlorobenzene
ug/L
ND
20
26.5
132
70-141
Chloroethane
ug/L
ND
20
27.7
138
58-191
Chloroform
ug/L
ND
20
28.9
143
70-148
Chloromethane
ug/L
ND
20
32.4
162
43-162
cis-1,2-Dichloroethene
ug/L
ND
20
30.5
153
68-151 M1
cis-1,3-Dichloropropene
ug/L
ND
20
28.7
143
70-139 M1
Dibromochloromethane
ug/L
ND
20
27.2
136
70-144
Dibromomethane
ug/L
ND
20
26.8
134
70-139
Ethylbenzene
ug/L
ND
20
26.4
132
70-143
lodomethane
ug/L
ND
40
53.3
133
35-171
m&p-Xylene
ug/L
ND
40
53.7
134
70-144
Methylene Chloride
ug/L
ND
20
28.1
139
62-149
o-Xylene
ug/L
ND
20
25.9
129
70-145
Styrene
ug/L
ND
20
26.6
133
70-143
Tetrachloroethene
ug/L
ND
20
26.0
129
70-145
Toluene
ug/L
ND
20
27.1
136
70-142
trans-1,2-Dichloroethene
ug/L
ND
20
31.3
156
70-151 M1
trans- 1,3-Dichloropropene
ug/L
ND
20
29.4
147
70-139 M1
trans-1,4-Dichloro-2-butene
ug/L
ND
20
26.9
134
51-159
Trichloroethene
ug/L
ND
20
28.7
143
62-146
Trichlorofluoromethane
ug/L
ND
20
26.5
130
63-153
Vinyl acetate
ug/L
ND
40
59.4
149
61-162
Vinyl chloride
ug/L
ND
20
33.3
167
61-163 M1
Xylene (Total)
ug/L
ND
60
79.6
133
70-143
1,2-Dichloroethane-d4 (S)
%
106
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
102
70-130
SAMPLE DUPLICATE: 3872969
92642468001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
1,1,1-Trichloroethane
ug/L
ND
ND
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
1,1,2-Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
ND
ND
1,1-Dichloroethene
ug/L
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:54 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 28

leAnalyiical
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QUALITY CONTROL DATA
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
SAMPLE DUPLICATE: 3872969
Parameter
Units
92642468001
Result
Dup
Result
1,2,3-Trichloropropane
ug/L
ND
ND
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
m&p-Xylene
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
o-Xylene
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
88
102
4-Bromofluorobenzene (S)
%
97
98
Toluene-d8 (S)
%
99
104
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:54 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 28

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: HARRISBURG ROAD LANDFILL
Pace Project No.: 92642465
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:54 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 28

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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
HARRISBURG ROAD LANDFILL
Pace Project No.:
92642465
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92642465001
6001-HB2006
EPA 3010A
745958
EPA6010D
746019
92642465002
6001-HB2008
EPA 3010A
745958
EPA6010D
746019
92642465003
6001-HB2010
EPA 3010A
745958
EPA6010D
746019
92642465001
6001-HB2006
EPA3005A
746005
EPA6020B
746121
92642465002
6001-HB2008
EPA3005A
746005
EPA6020B
746121
92642465003
6001-HB2010
EPA3005A
746005
EPA6020B
746121
92642465001
6001-HB2006
EPA 8260D
744044
92642465002
6001-HB2008
EPA 8260D
744044
92642465003
6001-HB2010
EPA 8260D
744044
92642465004
TRIP BLANK
EPA 8260D
744438
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2023 03:54 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 28

vvrr� 1141C. CtV V-r'ritYl-r7UlVl-tflJt3.3 volt —Sample Condition Upon Receipt
- ace
Effective Date: 051121202205/12/2022
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑' Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville❑
Sample Client Name: r
Upon Receipt Project #: WO# . 92642465
Courier: ❑ ed Ex ❑UPS ❑USA
❑Client❑ Commercial ❑Pace Other:
92�6�424�5� 5
Custody Seal Present? ❑Yes ❑No Seals Intact? ❑Yes QNo L
Packing Material: ❑Bubble wrap ❑Bubble Bags ❑None ❑ Other
Thermometer:
['(IR Gun ID:
Type of Ice: OWet []Blue
Correction Factor:
Cooler Temp: � Add/Subtract (°C)
Cooler Temp Corrected (°C):
USDA Regulated Soil ( dN/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC
(check maps)? [7]yes I-1No
Chain of Custody Present?
Samples Arrived within Hold Time?
Short Hold Time Analysis (02 hr.)?
Rush Turn Around Time Requested?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis: Samples Field Filtered?
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis
Headspace in VOA Vials (>5-6mm)?
Trip Blank Present?
Trip Blank Custody Seals Present?
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
____—PC9jC&tA1anager.SRF Review:. — .. - -
No
Yes
Yes
Yes []No ❑N/A
Yes ❑No nN/A
1.
2.
1
4.
5.
6.
Yes
I_„INo
UN/A
7.
Oyes
❑Na
N/A
8.
Yes
[]No❑N/A
9.
❑Yes
�No
❑N/A
10.
I]Yes
❑No
❑N/A
A1.
aYes
❑No
11N/A
Date/Initials Person Examining Contents:
Biological Tissue Fozen?
❑Yes ❑No I N/A
[]None
Tempshould be above freezing to 6°C
[]Samples out of temp criteria. Samples on ice, cooling process
has begun
Did Samples originate from a foreign source (internationally,
including Hawaii and Puerto Ricol? []yes ❑No
Field Data Required? ❑Yes []NO
Lot ID of split containers:
Date/Tune:
Date,
Date: - - - - — - - -
Qualtrax ID: 69614 Page 1 of 2 Page 26 of 28

Frr I }.IV. CIYv-r-r-tvil-r1uNi-uutsj vu7 Sample Condition Upon Receipt
Effective Date: 05/121202205/12/2022
*Check mark top half of box if pH and/or dechlorination is verified and Project # WO# : 92;642465
within the acceptance range for preservation samples. PM: ASS
Exceptions: VOA, Cal€form, roc, Oil and Grease, DRO/8015 (water) DOC, LLfCI.IEN'
3g Due Date: I21i8/;?2
r: 92-MECK CO
**Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
N
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PH Adjustment Log for Preserved Samples
Sample ID Type of Preservative pit upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot 4
adjusted added
Note: Whenever there is a discrepancy affecting North Carolina compfiance samples, a copy of this form will he sent to the Borth Carolina DENR Certification office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers,
Qualtrax ID; 69614 Page 2 of 2 Page 27 of 28

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Page 28 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
January 04, 2023
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on December 13, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Ariel S Fitzgerald
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 28

lacmnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification M 812
CERTIFICATIONS
South Carolina Certification M 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification M E87627
Kentucky UST Certification M 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification M 460221
North Carolina Certification #: 381
South Carolina Certification M 98011001
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 2 of 28

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[phone]
SAMPLE ANALYTE COUNT
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92642468001 6001-HBW28
EPA 6010D
DRB
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
JJK
52
PASI-C
92642468002 6001-HBW20
EPA 6010D
DRB
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
JJK
52
PASI-C
92642468003 6001-HBW14
EPA 6010D
DRB
15
PASI-GA
EPA6020B
CW1
1
PASI-GA
EPA 8260D
JJK
52
PASI-C
92642468004 TRIP BLANK
EPA 8260D
SAS
52
PASI-C
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 28

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[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
Sample: 6001-HBW28 Lab ID: 92642468001 Collected: 12/13/22 09:50 Received: 12/13/22 14:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
12/27/22 14:40
12/28/22 02:04
7440-38-2
Beryllium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 02:04
7440-41-7
Barium
33.1
ug/L
10.0
1
12/27/22 14:40
12/28/22 02:04
7440-39-3
Cadmium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 02:04
7440-43-9
Chromium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 02:04
7440-47-3
Copper
33.9
ug/L
20.0
1
12/27/22 14:40
12/28/22 02:04
7440-50-8
Nickel
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 02:04
7440-02-0
Silver
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 02:04
7440-22-4
Lead
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 02:04
7439-92-1
Antimony
ND
ug/L
50.0
1
12/27/22 14:40
12/28/22 02:04
7440-36-0
Selenium
ND
ug/L
40.0
1
12/27/22 14:40
12/28/22 02:04
7782-49-2
Thallium
ND
ug/L
200
1
12/27/22 14:40
12/28/22 02:04
7440-28-0
Vanadium
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 02:04
7440-62-2
Zinc
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 02:04
7440-66-6
Cobalt
ND
ug/L
40.0
1
12/27/22 14:40
12/28/22 02:04
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
12/27/2217:44
01/03/2316:25
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/20/22 02:05
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/20/22 02:05
107-13-1
Benzene
ND
ug/L
1.0
1
12/20/22 02:05
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/20/22 02:05
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/20/22 02:05
75-27-4
Bromoform
ND
ug/L
1.0
1
12/20/22 02:05
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/20/22 02:05
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/20/22 02:05
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/20/22 02:05
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/20/22 02:05
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/20/22 02:05
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/20/22 02:05
75-00-3
Chloroform
ND
ug/L
1.0
1
12/20/22 02:05
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/20/22 02:05
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/20/22 02:05
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/20/22 02:05
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/20/22 02:05
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/20/22 02:05
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/20/22 02:05
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/20/22 02:05
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/20/22 02:05
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/20/22 02:05
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/20/22 02:05
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 01 /04/2023 04:28 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
Sample: 6001-HBW28
Lab ID: 92642468001 Collected:
12/13/22
09:50
Received: 12/13/22 14:38 Matrix: Water
Parameters
Results
Units Report
Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/20/22 02:05
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/20/22 02:05
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/20/22 02:05
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/20/22 02:05
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/20/22 02:05
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/20/22 02:05
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/20/22 02:05
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/20/22 02:05
591-78-6
lodomethane
ND
ug/L
20.0
1
12/20/22 02:05
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
1
12/20/22 02:05
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/20/22 02:05
108-10-1
Styrene
ND
ug/L
1.0
1
12/20/22 02:05
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/20/22 02:05
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/20/22 02:05
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/20/22 02:05
127-18-4
Toluene
ND
ug/L
1.0
1
12/20/22 02:05
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/20/22 02:05
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/20/22 02:05
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/20/22 02:05
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/20/22 02:05
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/20/22 02:05
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/20/22 02:05
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/20/22 02:05
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/20/22 02:05
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/20/22 02:05
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/20/22 02:05
95-47-6
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
12/20/22 02:05
460-00-4
1,2-Dichloroethane-d4 (S)
88
%
70-130
1
12/20/22 02:05
17060-07-0
Toluene-d8(S)
99
%
70-130
1
12/20/22 02:05
2037-26-5
Date: 01/04/2023 04:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
Sample: 6001-HBW20
Lab ID: 92642468002 Collected:
12/13/22
10:25
Received: 12/13/22 14:38 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010D ATL ICP
Analytical Method:
EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
12/27/22 14:40
12/28/22 02:09
7440-38-2
Beryllium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 02:09
7440-41-7
Barium
10.3
ug/L
10.0
1
12/27/22 14:40
12/28/22 02:09
7440-39-3
Cadmium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 02:09
7440-43-9
Chromium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 02:09
7440-47-3
Copper
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 02:09
7440-50-8
Nickel
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 02:09
7440-02-0
Silver
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 02:09
7440-22-4
Lead
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 02:09
7439-92-1
Antimony
ND
ug/L
50.0
1
12/27/22 14:40
12/28/22 02:09
7440-36-0
Selenium
ND
ug/L
40.0
1
12/27/22 14:40
12/28/22 02:09
7782-49-2
Thallium
ND
ug/L
200
1
12/27/22 14:40
12/28/22 02:09
7440-28-0
Vanadium
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 02:09
7440-62-2
Zinc
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 02:09
7440-66-6
Cobalt
ND
ug/L
40.0
1
12/27/22 14:40
12/28/22 02:09
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method:
EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
12/27/2217:44
01/03/2316:31
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/20/22 02:23
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/20/22 02:23
107-13-1
Benzene
ND
ug/L
1.0
1
12/20/22 02:23
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/20/22 02:23
74-97-5 M1
Bromodichloromethane
ND
ug/L
1.0
1
12/20/22 02:23
75-27-4
Bromoform
ND
ug/L
1.0
1
12/20/22 02:23
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/20/22 02:23
74-83-9 v2
2-Butanone (MEK)
ND
ug/L
5.0
1
12/20/22 02:23
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/20/22 02:23
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/20/22 02:23
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/20/22 02:23
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/20/22 02:23
75-00-3
Chloroform
ND
ug/L
1.0
1
12/20/22 02:23
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/20/22 02:23
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/20/22 02:23
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/20/22 02:23
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/20/22 02:23
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/20/22 02:23
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/20/22 02:23
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/20/22 02:23
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/20/22 02:23
110-57-6
1,1-Dichloroethane
1.0
ug/L
1.0
1
12/20/22 02:23
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/20/22 02:23
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /04/2023 04:28 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
Sample: 6001-HBW20 Lab ID: 92642468002 Collected: 12/13/22 10:25 Received: 12/13/22 14:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/20/22 02:23
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/20/22 02:23
156-59-2
M1
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/20/22 02:23
156-60-5
M1
1,2-Dichloropropene
ND
ug/L
1.0
1
12/20/22 02:23
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/20/22 02:23
10061-01-5
M1
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/20/22 02:23
10061-02-6
M1
Ethylbenzene
ND
ug/L
1.0
1
12/20/22 02:23
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/20/22 02:23
591-78-6
lodomethane
ND
ug/L
20.0
1
12/20/22 02:23
74-88-4
v2
Methylene Chloride
ND
ug/L
5.0
1
12/20/22 02:23
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/20/22 02:23
108-10-1
Styrene
ND
ug/L
1.0
1
12/20/22 02:23
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/20/22 02:23
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/20/22 02:23
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/20/22 02:23
127-18-4
Toluene
ND
ug/L
1.0
1
12/20/22 02:23
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/20/22 02:23
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/20/22 02:23
79-00-5
M1
Trichloroethene
ND
ug/L
1.0
1
12/20/22 02:23
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/20/22 02:23
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/20/22 02:23
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/20/22 02:23
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/20/22 02:23
75-01-4
M1
Xylene (Total)
ND
ug/L
1.0
1
12/20/22 02:23
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/20/22 02:23
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/20/22 02:23
95-47-6
Surrogates
4-Bromofluorobenzene (S)
101
%
70-130
1
12/20/22 02:23
460-00-4
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
12/20/22 02:23
17060-07-0
Toluene-d8(S)
99
%
70-130
1
12/20/22 02:23
2037-26-5
Date: 01/04/2023 04:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
Sample: 6001-HBW14 Lab ID: 92642468003 Collected: 12/13/22 10:50 Received: 12/13/22 14:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010D ATL ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services - Peachtree Corners, GA
Arsenic
ND
ug/L
30.0
1
12/27/22 14:40
12/28/22 02:14
7440-38-2
Beryllium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 02:14
7440-41-7
Barium
133
ug/L
10.0
1
12/27/22 14:40
12/28/22 02:14
7440-39-3
Cadmium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 02:14
7440-43-9
Chromium
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 02:14
7440-47-3
Copper
40.6
ug/L
20.0
1
12/27/22 14:40
12/28/22 02:14
7440-50-8
Nickel
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 02:14
7440-02-0
Silver
ND
ug/L
10.0
1
12/27/22 14:40
12/28/22 02:14
7440-22-4
Lead
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 02:14
7439-92-1
Antimony
ND
ug/L
50.0
1
12/27/22 14:40
12/28/22 02:14
7440-36-0
Selenium
ND
ug/L
40.0
1
12/27/22 14:40
12/28/22 02:14
7782-49-2
Thallium
ND
ug/L
200
1
12/27/22 14:40
12/28/22 02:14
7440-28-0
Vanadium
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 02:14
7440-62-2
Zinc
ND
ug/L
20.0
1
12/27/22 14:40
12/28/22 02:14
7440-66-6
Cobalt
ND
ug/L
40.0
1
12/27/22 14:40
12/28/22 02:14
7440-48-4
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3005A
Pace Analytical
Services - Peachtree Corners, GA
Thallium
ND
ug/L
1.0
1
12/27/2217:44
01/03/2316:37
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/20/22 02:41
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/20/22 02:41
107-13-1
Benzene
ND
ug/L
1.0
1
12/20/22 02:41
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/20/22 02:41
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/20/22 02:41
75-27-4
Bromoform
ND
ug/L
1.0
1
12/20/22 02:41
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/20/22 02:41
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/20/22 02:41
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/20/22 02:41
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/20/22 02:41
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/20/22 02:41
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/20/22 02:41
75-00-3
Chloroform
ND
ug/L
1.0
1
12/20/22 02:41
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/20/22 02:41
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/20/22 02:41
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/20/22 02:41
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/20/22 02:41
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/20/22 02:41
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/20/22 02:41
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/20/22 02:41
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/20/22 02:41
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/20/22 02:41
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/20/22 02:41
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
This report shall not be reproduced, except in full,
Date: 01 /04/2023 04:28 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
Sample: 6001-HBW14
Lab ID: 92642468003 Collected:
12/13/22
10:50
Received: 12/13/22 14:38 Matrix: Water
Parameters
Results
Units Report
Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/20/22 02:41
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/20/22 02:41
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/20/22 02:41
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/20/22 02:41
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/20/22 02:41
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/20/22 02:41
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/20/22 02:41
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/20/22 02:41
591-78-6
lodomethane
ND
ug/L
20.0
1
12/20/22 02:41
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
1
12/20/22 02:41
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/20/22 02:41
108-10-1
Styrene
ND
ug/L
1.0
1
12/20/22 02:41
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/20/22 02:41
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/20/22 02:41
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/20/22 02:41
127-18-4
Toluene
ND
ug/L
1.0
1
12/20/22 02:41
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/20/22 02:41
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/20/22 02:41
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/20/22 02:41
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/20/22 02:41
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/20/22 02:41
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/20/22 02:41
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/20/22 02:41
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/20/22 02:41
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/20/22 02:41
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/20/22 02:41
95-47-6
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
12/20/22 02:41
460-00-4
1,2-Dichloroethane-d4 (S)
98
%
70-130
1
12/20/22 02:41
17060-07-0
Toluene-d8(S)
100
%
70-130
1
12/20/22 02:41
2037-26-5
Date: 01/04/2023 04:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 28

Pace Analytical Services, LLC
ceAnalyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
Sample: TRIP BLANK Lab ID: 92642468004 Collected: 12/13/22 00:00 Received: 12/13/22 14:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/17/22 01:20
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/17/22 01:20
107-13-1
Benzene
ND
ug/L
1.0
1
12/17/22 01:20
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/17/22 01:20
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/17/22 01:20
75-27-4
Bromoform
ND
ug/L
1.0
1
12/17/22 01:20
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/17/22 01:20
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/17/22 01:20
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/17/22 01:20
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/17/22 01:20
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/17/22 01:20
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/17/22 01:20
75-00-3
Chloroform
ND
ug/L
1.0
1
12/17/22 01:20
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/17/22 01:20
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/17/22 01:20
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/17/22 01:20
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/17/22 01:20
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/17/22 01:20
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/17/22 01:20
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/17/22 01:20
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/17/22 01:20
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/17/22 01:20
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/17/22 01:20
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/17/22 01:20
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/17/22 01:20
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/17/22 01:20
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/17/22 01:20
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/17/22 01:20
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/17/22 01:20
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/17/22 01:20
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/17/22 01:20
591-78-6
lodomethane
ND
ug/L
20.0
1
12/17/22 01:20
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/17/22 01:20
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/17/22 01:20
108-10-1
Styrene
ND
ug/L
1.0
1
12/17/22 01:20
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/17/22 01:20
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/17/22 01:20
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/17/22 01:20
127-18-4
Toluene
ND
ug/L
1.0
1
12/17/22 01:20
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/17/22 01:20
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/17/22 01:20
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/17/22 01:20
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/17/22 01:20
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/17/22 01:20
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/17/22 01:20
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/17/22 01:20
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /04/2023 04:28 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 28

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
Sample: TRIP BLANK
Parameters
Lab ID: 92642468004 Collected: 12/13/22 00:00
Results Units Report Limit DF
Received: 12/13/22 14:38 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
12/17/22 01:20
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
12/17/22 01:20
179601-23-1
o-Xylene
ND ug/L
1.0
1
12/17/22 01:20
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99 %
70-130
1
12/17/22 01:20
460-00-4
1,2-Dichloroethane-d4 (S)
103 %
70-130
1
12/17/22 01:20
17060-07-0
Toluene-d8 (S)
108 %
70-130
1
12/17/22 01:20
2037-26-5
Date: 01/04/2023 04:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
QC Batch: 745958 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 601 OD ATL
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92642468001, 92642468002, 92642468003
METHOD BLANK: 3880043 Matrix: Water
Associated Lab Samples: 92642468001, 92642468002, 92642468003
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
50.0
12/28/22 00:08
30.0
12/28/22 00:08
10.0
12/28/22 00:08
10.0
12/28/22 00:08
10.0
12/28/22 00:08
10.0
12/28/22 00:08
40.0
12/28/22 00:08
20.0
12/28/22 00:08
20.0
12/28/22 00:08
20.0
12/28/22 00:08
40.0
12/28/22 00:08
10.0
12/28/22 00:08
200
12/28/22 00:08
20.0
12/28/22 00:08
20.0
12/28/22 00:08
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3880044
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
1000
1060
106
80-120
Arsenic
ug/L
1000
1070
107
80-120
Barium
ug/L
1000
1040
104
80-120
Beryllium
ug/L
1000
1070
107
80-120
Cadmium
ug/L
1000
1070
107
80-120
Chromium
ug/L
1000
1050
105
80-120
Cobalt
ug/L
1000
1070
107
80-120
Copper
ug/L
1000
1050
105
80-120
Lead
ug/L
1000
1070
107
80-120
Nickel
ug/L
1000
1080
108
80-120
Selenium
ug/L
1000
1070
107
80-120
Silver
ug/L
1000
1020
102
80-120
Thallium
ug/L
1000
1030
103
80-120
Vanadium
ug/L
1000
1120
112
80-120
Zinc
ug/L
1000
1070
107
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /04/2023 04:28 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
HARRISBURG RD LANDFILL(PERMIT#
92642468
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3880045
3880046
MS
MSD
92641048001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
1000
1000
1060
1090
105
108
75-125
3
Arsenic
ug/L
ND
1000
1000
1070
1100
107
110
75-125
2
Barium
ug/L
76.5
1000
1000
1120
1140
104
107
75-125
2
Beryllium
ug/L
ND
1000
1000
1070
1100
107
109
75-125
3
Cadmium
ug/L
ND
1000
1000
1070
1090
107
109
75-125
3
Chromium
ug/L
ND
1000
1000
1060
1080
106
108
75-125
1
Cobalt
ug/L
20AJ
1000
1000
1090
1110
107
109
75-125
2
Copper
ug/L
20.OJ
1000
1000
1100
1120
108
110
75-125
2
Lead
ug/L
ND
1000
1000
1070
1100
105
108
75-125
3
Nickel
ug/L
27.0
1000
1000
1100
1120
107
110
75-125
2
Selenium
ug/L
ND
1000
1000
1020
1030
102
103
75-125
1
Silver
ug/L
ND
1000
1000
1040
1050
104
105
75-125
1
Thallium
ug/L
ND
1000
1000
1040
1070
104
107
75-125
2
Vanadium
ug/L
ND
1000
1000
1140
1160
114
116
75-125
2
Zinc
ug/L
13.1 J
1000
1000
1050
1080
103
107
75-125
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /04/2023 04:28 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 28

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
QC Batch: 746005 Analysis Method: EPA 6020B
QC Batch Method: EPA 3005A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92642468001, 92642468002, 92642468003
METHOD BLANK: 3880266
Matrix:
Water
Associated Lab Samples: 92642468001, 92642468002, 92642468003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
1.0
01/03/2314:31
LABORATORY CONTROL SAMPLE:
3880267
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
100
101
101 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3880268 3880269
MS MSD
92641696001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L 0.18J 100 100 97.3 96.3 97 96 75-125 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /04/2023 04:28 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
QC Batch: 744044 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92642468004
METHOD BLANK: 3871223
Associated Lab Samples: 92642468004
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
12/17/22 00:44
1,1,1-Trichloroethane
ug/L
ND
1.0
12/17/22 00:44
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/17/22 00:44
1,1,2-Trichloroethane
ug/L
ND
1.0
12/17/22 00:44
1,1-Dichloroethane
ug/L
ND
1.0
12/17/22 00:44
1,1-Dichloroethene
ug/L
ND
1.0
12/17/22 00:44
1,2,3-Trichloropropane
ug/L
ND
1.0
12/17/22 00:44
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
12/17/22 00:44
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/17/22 00:44
1,2-Dichlorobenzene
ug/L
ND
1.0
12/17/22 00:44
1,2-Dichloroethane
ug/L
ND
1.0
12/17/22 00:44
1,2-Dichloropropane
ug/L
ND
1.0
12/17/22 00:44
1,4-Dichlorobenzene
ug/L
ND
1.0
12/17/22 00:44
2-Butanone (MEK)
ug/L
ND
5.0
12/17/22 00:44
2-Hexanone
ug/L
ND
5.0
12/17/22 00:44
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/17/22 00:44
Acetone
ug/L
ND
25.0
12/17/22 00:44
Acrylonitrile
ug/L
ND
10.0
12/17/22 00:44
Benzene
ug/L
ND
1.0
12/17/22 00:44
Bromochloromethane
ug/L
ND
1.0
12/17/22 00:44
Bromodichloromethane
ug/L
ND
1.0
12/17/22 00:44
Bromoform
ug/L
ND
1.0
12/17/22 00:44
Bromomethane
ug/L
ND
2.0
12/17/22 00:44
Carbon disulfide
ug/L
ND
2.0
12/17/22 00:44
Carbon tetrachloride
ug/L
ND
1.0
12/17/22 00:44
Chlorobenzene
ug/L
ND
1.0
12/17/22 00:44
Chloroethane
ug/L
ND
1.0
12/17/22 00:44
Chloroform
ug/L
ND
1.0
12/17/22 00:44
Chloromethane
ug/L
ND
1.0
12/17/22 00:44
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/17/22 00:44
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/17/22 00:44
Dibromochloromethane
ug/L
ND
1.0
12/17/22 00:44
Dibromomethane
ug/L
ND
1.0
12/17/22 00:44
Ethylbenzene
ug/L
ND
1.0
12/17/22 00:44
lodomethane
ug/L
ND
20.0
12/17/22 00:44
m&p-Xylene
ug/L
ND
2.0
12/17/22 00:44
Methylene Chloride
ug/L
ND
5.0
12/17/22 00:44
o-Xylene
ug/L
ND
1.0
12/17/22 00:44
Styrene
ug/L
ND
1.0
12/17/22 00:44
Tetrachloroethene
ug/L
ND
1.0
12/17/22 00:44
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /04/2023 04:28 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 28

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
METHOD BLANK: 3871223
Associated Lab Samples: 92642468004
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Toluene
ug/L
ND
1.0
12/17/22 00:44
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/17/22 00:44
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/17/22 00:44
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
12/17/22 00:44
Trichloroethene
ug/L
ND
1.0
12/17/22 00:44
Trichlorofluoromethane
ug/L
ND
1.0
12/17/22 00:44
Vinyl acetate
ug/L
ND
2.0
12/17/22 00:44
Vinyl chloride
ug/L
ND
1.0
12/17/22 00:44
Xylene (Total)
ug/L
ND
1.0
12/17/22 00:44
1,2-Dichloroethane-d4 (S)
%
106
70-130
12/17/22 00:44
4-Bromofluorobenzene (S)
%
103
70-130
12/17/22 00:44
Toluene-d8 (S)
%
106
70-130
12/17/22 00:44
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3871224
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.0
102
70-130
1,1,1-Trichloroethane
ug/L
50
49.5
99
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
48.3
97
70-130
1,1,2-Trichloroethane
ug/L
50
48.2
96
70-130
1,1-Dichloroethane
ug/L
50
46.1
92
70-130
1,1-Dichloroethene
ug/L
50
47.8
96
70-130
1,2,3-Trichloropropane
ug/L
50
48.6
97
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
52.3
105
70-131
1,2-Dibromoethane (EDB)
ug/L
50
51.9
104
70-130
1,2-Dichlorobenzene
ug/L
50
51.2
102
70-130
1,2-Dichloroethane
ug/L
50
48.3
97
70-130
1,2-Dichloropropane
ug/L
50
49.2
98
70-130
1,4-Dichlorobenzene
ug/L
50
50.2
100
70-130
2-Butanone (MEK)
ug/L
100
103
103
70-134
2-Hexanone
ug/L
100
96.1
96
70-131
4-Methyl-2-pentanone (MIBK)
ug/L
100
95.0
95
70-130
Acetone
ug/L
100
94.0
94
70-133
Acrylonitrile
ug/L
250
230
92
70-130
Benzene
ug/L
50
45.8
92
70-130
Bromochloromethane
ug/L
50
51.3
103
70-130
Bromodichloromethane
ug/L
50
48.8
98
70-130
Bromoform
ug/L
50
49.7
99
70-130
Bromomethane
ug/L
50
41.0
82
45-151
Carbon disulfide
ug/L
50
46.6
93
70-130
Carbon tetrachloride
ug/L
50
48.5
97
70-130
Chlorobenzene
ug/L
50
49.5
99
70-130
Chloroethane
ug/L
50
45.3
91
39-152
Chloroform
ug/L
50
44.7
89
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /04/2023 04:28 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 28

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
LABORATORY CONTROL SAMPLE:
Parameter
3871224
Units
Spike LCS
Conc. Result
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
m&p-Xylene
ug/L
100
Methylene Chloride
ug/L
50
o-Xylene
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits
41.4
83
58-130
47.1
94
70-130
50.4
101
70-130
50.2
100
70-130
48.8
98
70-130
48.6
97
70-130
96.3
96
53-141
97.6
98
70-130
44.5
89
66-130
47.4
95
70-130
49.3
99
70-130
48.8
98
70-130
46.3
93
70-130
47.5
95
70-130
49.9
100
70-130
52.1
104
57-185
51.2
102
70-130
40.2
80
62-130
112
112
70-144
42.8
86
62-130
145
97
70-130
101
70-130
96
70-130
97
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3871225
MS
92641898022 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3871226
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
22.7
23.2
113
116
70-141
2
1,1,1-Trichloroethane
ug/L
ND
20
20
23.7
25.5
118
128
70-150
8
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.6
22.4
113
112
69-142
1
1,1,2-Trichloroethane
ug/L
ND
20
20
23.3
22.8
116
114
70-138
2
1,1-Dichloroethane
ug/L
ND
20
20
23.0
23.6
115
118
70-150
3
1,1-Dichloroethene
ug/L
ND
20
20
24.5
25.2
122
126
70-156
3
1,2,3-Trichloropropane
ug/L
ND
20
20
23.0
21.0
115
105
70-140
9
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
24.4
23.7
122
119
68-146
3
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.6
23.6
113
118
70-138
4
1,2-Dichlorobenzene
ug/L
ND
20
20
22.1
22.6
111
113
70-141
2
1,2-Dichloroethane
ug/L
ND
20
20
23.1
23.1
116
115
69-143
0
1,2-Dichloropropane
ug/L
ND
20
20
23.4
23.2
117
116
68-156
1
1,4-Dichlorobenzene
ug/L
ND
20
20
22.0
21.6
110
108
70-142
2
2-Butanone (MEK)
ug/L
ND
40
40
42.7
42.6
107
106
60-157
0 v1
2-Hexanone
ug/L
ND
40
40
44.6
43.9
112
110
68-146
2
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
43.9
42.9
110
107
70-141
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /04/2023 04:28 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3871225
MS
92641898022 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3871226
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
43.1
45.4
108
114
58-157
5
Acrylonitrile
ug/L
ND
100
100
125
123
125
123
69-147
1
Benzene
ug/L
ND
20
20
22.1
22.1
111
111
70-142
0
Bromochloromethane
ug/L
ND
20
20
23.8
24.5
119
122
70-146
3
Bromodichloromethane
ug/L
ND
20
20
22.8
22.6
114
113
70-139
1
Bromoform
ug/L
ND
20
20
22.7
22.9
113
115
64-140
1
Bromomethane
ug/L
ND
20
20
23.1
22.5
115
112
28-192
3
Carbon disulfide
ug/L
ND
20
20
25.4
26.1
127
130
70-151
3
Carbon tetrachloride
ug/L
ND
20
20
25.2
25.0
126
125
70-148
1
Chlorobenzene
ug/L
ND
20
20
22.9
23.1
115
115
70-141
1
Chloroethane
ug/L
ND
20
20
23.3
24.7
116
124
58-191
6
Chloroform
ug/L
ND
20
20
22.8
23.7
113
118
70-148
4
Chloromethane
ug/L
ND
20
20
22.2
23.1
111
115
43-162
4
cis-1,2-Dichloroethene
ug/L
ND
20
20
22.9
24.6
114
123
68-151
7
cis-1,3-Dichloropropene
ug/L
ND
20
20
23.8
24.0
119
120
70-139
1
Dibromochloromethane
ug/L
ND
20
20
23.0
22.9
115
115
70-144
0
Dibromomethane
ug/L
ND
20
20
23.7
23.0
119
115
70-139
3
Ethylbenzene
ug/L
ND
20
20
23.2
22.9
116
114
70-143
2
lodomethane
ug/L
ND
40
40
41.3
43.7
103
109
35-171
6
m&p-Xylene
ug/L
ND
40
40
46.4
46.2
116
116
70-144
0
Methylene Chloride
ug/L
ND
20
20
21.8
22.2
109
111
62-149
2
o-Xylene
ug/L
ND
20
20
22.3
22.0
111
110
70-145
1
Styrene
ug/L
ND
20
20
22.2
22.0
111
110
70-143
1
Tetrachloroethene
ug/L
ND
20
20
23.2
23.4
116
117
70-145
1
Toluene
ug/L
ND
20
20
22.4
22.0
112
110
70-142
2
trans-1,2-Dichloroethene
ug/L
ND
20
20
24.2
24.9
121
125
70-151
3
trans- 1,3-Dichloropropene
ug/L
ND
20
20
23.7
23.7
119
118
70-139
0
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
22.9
20.7
115
104
51-159
10
Trichloroethene
ug/L
ND
20
20
24.1
24.1
120
120
62-146
0
Trichlorofluoromethane
ug/L
ND
20
20
21.1
22.0
105
110
63-153
4
Vinyl acetate
ug/L
ND
40
40
41.8
43.3
104
108
61-162
4
Vinyl chloride
ug/L
ND
20
20
22.1
23.2
111
116
61-163
5
Xylene (Total)
ug/L
ND
60
60
68.6
68.2
114
114
70-143
1
1,2-Dichloroethane-d4 (S)
%
104
112
70-130
4-Bromofluorobenzene (S)
%
102
101
70-130
Toluene-d8(S)
%
101
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /04/2023 04:28 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
QC Batch: 744438 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92642468001, 92642468002, 92642468003
METHOD BLANK: 3872965 Matrix:
Associated Lab Samples: 92642468001, 92642468002, 92642468003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
12/20/22 01:11
1,1,1-Trichloroethane
ug/L
ND
1.0
12/20/22 01:11
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/20/22 01:11
1,1,2-Trichloroethane
ug/L
ND
1.0
12/20/22 01:11
1,1-Dichloroethane
ug/L
ND
1.0
12/20/22 01:11
1,1-Dichloroethene
ug/L
ND
1.0
12/20/22 01:11
1,2,3-Trichloropropane
ug/L
ND
1.0
12/20/22 01:11
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
12/20/22 01:11
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/20/22 01:11
1,2-Dichlorobenzene
ug/L
ND
1.0
12/20/22 01:11
1,2-Dichloroethane
ug/L
ND
1.0
12/20/22 01:11
1,2-Dichloropropane
ug/L
ND
1.0
12/20/22 01:11
1,4-Dichlorobenzene
ug/L
ND
1.0
12/20/22 01:11
2-Butanone (MEK)
ug/L
ND
5.0
12/20/22 01:11
2-Hexanone
ug/L
ND
5.0
12/20/22 01:11
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/20/22 01:11
Acetone
ug/L
ND
25.0
12/20/22 01:11
Acrylonitrile
ug/L
ND
10.0
12/20/22 01:11
Benzene
ug/L
ND
1.0
12/20/22 01:11
Bromochloromethane
ug/L
ND
1.0
12/20/22 01:11
Bromodichloromethane
ug/L
ND
1.0
12/20/22 01:11
Bromoform
ug/L
ND
1.0
12/20/22 01:11
Bromomethane
ug/L
ND
2.0
12/20/22 01:11
Carbon disulfide
ug/L
ND
2.0
12/20/22 01:11
Carbon tetrachloride
ug/L
ND
1.0
12/20/22 01:11
Chlorobenzene
ug/L
ND
1.0
12/20/22 01:11
Chloroethane
ug/L
ND
1.0
12/20/22 01:11
Chloroform
ug/L
ND
1.0
12/20/22 01:11
Chloromethane
ug/L
ND
1.0
12/20/22 01:11
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/20/22 01:11
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/20/22 01:11
Dibromochloromethane
ug/L
ND
1.0
12/20/22 01:11
Dibromomethane
ug/L
ND
1.0
12/20/22 01:11
Ethylbenzene
ug/L
ND
1.0
12/20/22 01:11
lodomethane
ug/L
ND
20.0
12/20/22 01:11
m&p-Xylene
ug/L
ND
2.0
12/20/22 01:11
Methylene Chloride
ug/L
ND
5.0
12/20/22 01:11
o-Xylene
ug/L
ND
1.0
12/20/22 01:11
Styrene
ug/L
ND
1.0
12/20/22 01:11
Tetrachloroethene
ug/L
ND
1.0
12/20/22 01:11
v2
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /04/2023 04:28 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
METHOD BLANK: 3872965 Matrix:
Associated Lab Samples: 92642468001, 92642468002, 92642468003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed Qualifiers
Toluene
ug/L
ND
1.0
12/20/22 01:11
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/20/22 01:11
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/20/22 01:11
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
12/20/22 01:11
Trichloroethene
ug/L
ND
1.0
12/20/22 01:11
Trichlorofluoromethane
ug/L
ND
1.0
12/20/22 01:11
Vinyl acetate
ug/L
ND
2.0
12/20/22 01:11
Vinyl chloride
ug/L
ND
1.0
12/20/22 01:11
Xylene (Total)
ug/L
ND
1.0
12/20/22 01:11
1,2-Dichloroethane-d4 (S)
%
91
70-130
12/20/22 01:11
4-Bromofluorobenzene (S)
%
99
70-130
12/20/22 01:11
Toluene-d8 (S)
%
95
70-130
12/20/22 01:11
LABORATORY CONTROL SAMPLE:
Parameter
3872966
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
50.3
101
70-130
1,1,1-Trichloroethane
ug/L
50
47.6
95
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
49.2
98
70-130
1,1,2-Trichloroethane
ug/L
50
52.0
104
70-130
1,1-Dichloroethane
ug/L
50
47.6
95
70-130
1,1-Dichloroethene
ug/L
50
45.4
91
70-130
1,2,3-Trichloropropane
ug/L
50
45.2
90
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
54.3
109
70-131
1,2-Dibromoethane (EDB)
ug/L
50
49.9
100
70-130
1,2-Dichlorobenzene
ug/L
50
49.5
99
70-130
1,2-Dichloroethane
ug/L
50
43.4
87
70-130
1,2-Dichloropropane
ug/L
50
52.0
104
70-130
1,4-Dichlorobenzene
ug/L
50
49.3
99
70-130
2-Butanone (MEK)
ug/L
100
98.1
98
70-134
2-Hexanone
ug/L
100
107
107
70-131
4-Methyl-2-pentanone (MIBK)
ug/L
100
109
109
70-130
Acetone
ug/L
100
91.2
91
70-133
Acrylonitrile
ug/L
250
269
108
70-130
Benzene
ug/L
50
45.3
91
70-130
Bromochloromethane
ug/L
50
49.9
100
70-130
Bromodichloromethane
ug/L
50
51.0
102
70-130
Bromoform
ug/L
50
51.9
104
70-130
Bromomethane
ug/L
50
40.5
81
45-151 v3
Carbon disulfide
ug/L
50
45.8
92
70-130
Carbon tetrachloride
ug/L
50
49.6
99
70-130
Chlorobenzene
ug/L
50
48.7
97
70-130
Chloroethane
ug/L
50
49.4
99
39-152
Chloroform
ug/L
50
46.1
92
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /04/2023 04:28 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 28

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
LABORATORY CONTROL SAMPLE:
Parameter
3872966
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Chloromethane
ug/L
50
47.2
94
58-130
cis-1,2-Dichloroethene
ug/L
50
48.9
98
70-130
cis-1,3-Dichloropropene
ug/L
50
53.5
107
70-130
Dibromochloromethane
ug/L
50
49.3
99
70-130
Dibromomethane
ug/L
50
52.8
106
70-130
Ethylbenzene
ug/L
50
48.9
98
70-130
lodomethane
ug/L
100
93.3
93
53-141 v3
m&p-Xylene
ug/L
100
99.9
100
70-130
Methylene Chloride
ug/L
50
45.8
92
66-130
o-Xylene
ug/L
50
50.2
100
70-130
Styrene
ug/L
50
52.4
105
70-130
Tetrachloroethene
ug/L
50
45.7
91
70-130
Toluene
ug/L
50
50.3
101
70-130
trans-1,2-Dichloroethene
ug/L
50
48.7
97
70-130
trans- 1,3-Dichloropropene
ug/L
50
53.7
107
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
47.0
94
57-185
Trichloroethene
ug/L
50
50.5
101
70-130
Trichlorofluoromethane
ug/L
50
39.5
79
62-130
Vinyl acetate
ug/L
100
99.2
99
70-144
Vinyl chloride
ug/L
50
47.4
95
62-130
Xylene (Total)
ug/L
150
150
100
70-130
1,2-Dichloroethane-d4 (S)
%
84
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
105
70-130
MATRIX SPIKE SAMPLE:
Parameter
3872970
Units
92642468002
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
27.7
139
70-141
1,1,1-Trichloroethane
ug/L
ND
20
29.6
148
70-150
1,1,2,2-Tetrachloroethane
ug/L
ND
20
25.4
127
69-142
1,1,2-Trichloroethane
ug/L
ND
20
28.2
141
70-138 M1
1,1-Dichloroethane
ug/L
1.0
20
30.7
149
70-150
1,1-Dichloroethene
ug/L
ND
20
31.0
155
70-156
1,2,3-Trichloropropane
ug/L
ND
20
24.8
124
70-140
1,2-Dibromo-3-chloropropane
ug/L
ND
20
26.4
132
68-146
1,2-Dibromoethane (EDB)
ug/L
ND
20
27.0
135
70-138
1,2-Dichlorobenzene
ug/L
ND
20
25.0
125
70-141
1,2-Dichloroethane
ug/L
ND
20
28.4
142
69-143
1,2-Dichloropropane
ug/L
ND
20
28.6
143
68-156
1,4-Dichlorobenzene
ug/L
ND
20
25.0
125
70-142
2-Butanone (MEK)
ug/L
ND
40
55.9
140
60-157
2-Hexanone
ug/L
ND
40
52.6
132
68-146
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
52.4
131
70-141
Acetone
ug/L
ND
40
51.9
128
58-157
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /04/2023 04:28 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 28

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
MATRIX SPIKE SAMPLE:
3872970
92642468002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Acrylonitrile
ug/L
ND
100
146
146
69-147
Benzene
ug/L
ND
20
27.1
135
70-142
Bromochloromethane
ug/L
ND
20
29.9
149
70-146 M1
Bromodichloromethane
ug/L
ND
20
27.7
139
70-139
Bromoform
ug/L
ND
20
26.9
134
64-140
Bromomethane
ug/L
ND
20
21.5
108
28-192
Carbon disulfide
ug/L
ND
20
29.0
145
70-151
Carbon tetrachloride
ug/L
ND
20
27.5
138
70-148
Chlorobenzene
ug/L
ND
20
26.5
132
70-141
Chloroethane
ug/L
ND
20
27.7
138
58-191
Chloroform
ug/L
ND
20
28.9
143
70-148
Chloromethane
ug/L
ND
20
32.4
162
43-162
cis-1,2-Dichloroethene
ug/L
ND
20
30.5
153
68-151 M1
cis-1,3-Dichloropropene
ug/L
ND
20
28.7
143
70-139 M1
Dibromochloromethane
ug/L
ND
20
27.2
136
70-144
Dibromomethane
ug/L
ND
20
26.8
134
70-139
Ethylbenzene
ug/L
ND
20
26.4
132
70-143
lodomethane
ug/L
ND
40
53.3
133
35-171
m&p-Xylene
ug/L
ND
40
53.7
134
70-144
Methylene Chloride
ug/L
ND
20
28.1
139
62-149
o-Xylene
ug/L
ND
20
25.9
129
70-145
Styrene
ug/L
ND
20
26.6
133
70-143
Tetrachloroethene
ug/L
ND
20
26.0
129
70-145
Toluene
ug/L
ND
20
27.1
136
70-142
trans-1,2-Dichloroethene
ug/L
ND
20
31.3
156
70-151 M1
trans- 1,3-Dichloropropene
ug/L
ND
20
29.4
147
70-139 M1
trans-1,4-Dichloro-2-butene
ug/L
ND
20
26.9
134
51-159
Trichloroethene
ug/L
ND
20
28.7
143
62-146
Trichlorofluoromethane
ug/L
ND
20
26.5
130
63-153
Vinyl acetate
ug/L
ND
40
59.4
149
61-162
Vinyl chloride
ug/L
ND
20
33.3
167
61-163 M1
Xylene (Total)
ug/L
ND
60
79.6
133
70-143
1,2-Dichloroethane-d4 (S)
%
106
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
102
70-130
SAMPLE DUPLICATE: 3872969
92642468001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
1,1,1-Trichloroethane
ug/L
ND
ND
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
1,1,2-Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
ND
ND
1,1-Dichloroethene
ug/L
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /04/2023 04:28 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 28

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
SAMPLE DUPLICATE: 3872969
Parameter
Units
92642468001
Result
Dup
Result
1,2,3-Trichloropropane
ug/L
ND
ND
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
m&p-Xylene
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
o-Xylene
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
88
102
4-Bromofluorobenzene (S)
%
97
98
Toluene-d8 (S)
%
99
104
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /04/2023 04:28 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 28

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.: 92642468
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /04/2023 04:28 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 28

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
HARRISBURG RD LANDFILL(PERMIT#
Pace Project No.:
92642468
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92642468001
6001-HBW28
EPA 3010A
745958
EPA6010D
746019
92642468002
6001-HBW20
EPA 3010A
745958
EPA6010D
746019
92642468003
6001-HBW14
EPA 3010A
745958
EPA6010D
746019
92642468001
6001-HBW28
EPA3005A
746005
EPA6020B
746121
92642468002
6001-HBW20
EPA3005A
746005
EPA6020B
746121
92642468003
6001-HBW14
EPA3005A
746005
EPA6020B
746121
92642468001
6001-HBW28
EPA 8260D
744438
92642468002
6001-HBW20
EPA 8260D
744438
92642468003
6001-HBW14
EPA 8260D
744438
92642468004
TRIP BLANK
EPA 8260D
744044
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /04/2023 04:28 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 28

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Effective Date: 05/12/202205/12/2022
Laboratory receiving samples:
Asheville ❑ Eden[:] Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville[] Atlanta❑ Kernersville❑
Sam• ' Condition Client Name: rW41t , 926424�68
" , Project #:
Ntil �' %�^ I t„rr:.
Courier: ❑fed Ex ❑UPS ❑LISPS ❑Client
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❑ Commercial Dace ❑Other
92642,168
I /
Custody Seal Present? ❑Yes QNo Seals Intact? []yes ❑No
Packing Material; ❑Bubble Wrap ❑Bubble Bags ❑None ❑ Other
Thermom! er: !�
LJ IR Gun ID:
Type of ice: [wet ❑glue
Correction Factor:
Cooler Temp: Add/Subtract (°C)
Cooler Temp Corrected (°C):
USDA Regulated Soil ( N/A, water sample)
Did samples originate in a quarantine zone within the United States; CA, IVY, or SC
CO"
.-..,.•If VIrtL�e��ner�srrs r
CLIENT NOTIFICATION/RESOLUTION
Date/Initials Person Examining Contents:
Biological Tissue rozen?
]Yes [:]No❑N/A
❑None
Temp should be above freezing to 6'C
❑5amples out of temp criteria. Samples on ice, cooling process
has begun
Did samnir+snriAinit. Irnm a fn ivn �� • �o ri �e �•; yn..
Lot ID of split containers:
Person contacted: Date/Time:
Project Manager SCURF Review: Date:
_ __Pr4j;<c1_N1anager_5RF Review: Date:
Field Data Required? []Yes ❑No
QLtaltrax ID: 69614 Page 1 of 2 Page 26 of 28

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*Check mark top half of box if pH and/or dechlorination is verified and
within the acceptance range for preservation samples.
Exceptions: VOA, Caiiform, TOC, Oil and Grease, 0110/8015 (water) ❑OC, Wig
"Bottom half of box is to list number of bottles
***Check all unpreserved Nitrates for chlorine
Project# W41t : 92:642416$
PM: ASF Due Date: 12/28/22
CLIENT: 92—MECK CO
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PH Adjustment Log for Preserved Samples
Sample !p Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative !ot #
adjusted added
Note: WhCenever there if a discrepancyaffecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DENR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Qualtrax ID: 69614 Page 2 of 2 Page 27 of 28

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D
A
a
X
X
X
VOCs
m
o
m
to
ro'
c
N
a
a
D
'm
E.
N
a
l
H
=
m
m
b
d
TEMP in C
d
Residual Chlorine (YIN)
y
3
S7
c�
O
w
p
Received on Ice
(YIN)
m
0
O
l
a
n
Custody Sealed
zz
r
Cooler
A
(YIN}
_
`--
z
4�
Samples Intact
(YIN}
jo
m =
�n
Z
71
66
' C ;
N 60
a /c
n 0
O n
O
m ,z
Z
.> c7
CU
m
CD
G (Q
a
fD (D
a �
N r-►
cv
TO
0
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n
3
m 4
Ca
Iv
n
C
W
rD
Page 28 of 28