9233T_Wake_EastWakeTransfer_CityLeachateSoilSampingReport_FID1756474_20221222

AECOM
December 22, 2022
Ms. Jaclynne Drummond
North Carolina Department of Environmental Quality
Division of Waste Management
Solid Waste Section
2090 U.S. 70 Highway
Swannanoa, North Carolina 28778
RE: Wake County —East Wake Transfer Station
820 Corporation Parkway
Raleigh, Wake County, North Carolina
Solid Waste Permit Number 9233T-TRANSFER-2008
Leachate Release Soil Sampling Report
Dear Ms. Drummond,
AECOM
5438 Wade Park Boulevard, Suite 200
Raleigh, NC 27607
aecom.com
As required by the North Carolina Department of Environmental Quality (NCDEQ), AECOM Technical Services, Inc.
(AECOM), on behalf of the City of Raleigh (CoR), has prepared this Leachate Release Soil Sampling Report for the
East Wake Transfer Station (Site) located in Raleigh, Wake County, North Carolina.
On September 8, 2022, the State of North Carolina, Division of Waste Management Solid Waste Section (SWS)
inspected the Site for compliance with North Carolina Solid Waste Statutes and Rules. The NCDEQ issued a Notice of
Violation (NOV) to the Site on September 20, 2022. The Site was found to be in violation of 15A NCAC 13B .0405 (a)
(10), (b), and (c) and 15A NCAC 13 0.104 (a) through (d). In response, AECOM, on behalf of the CoR, submitted a
Response Plan dated September 2022. Soil sampling was performed in accordance with the Response Plan
approved by the SWS and the Leachate Release Sampling and Analysis Guidelines (SWS, 2021).
Release Incident Pertaining to City of Raleigh
The CoR portion of the Site was found to be in violation of 15A NCAC 13B .0405 (a) (10) for a large amount of
windblown waste throughout the facility and concealed under plastic sheeting in the riprap along the eastern wall of
the transfer station.
The CoR portion of the Site violated 15A NCAC 13B .0405 (c) for improper temporary storage. Leaking rolling bins
containing waste were stored on the soil adjacent to the access road. Also, transfer vehicles waiting to enter the
transfer station tipping floor were leaking leachate, which was running down the access road and accumulating in a
low-lying area of the access road.
The Site was found to be in violation of 15A NCAC 13 0.104 (a) through (d) for improper solid waste storage. Multiple
City of Raleigh plastic rolling garbage bins containing leachate and waste were stored uncovered on a dirt area
adjacent to the facility access road to the south of the transfer station building. The area was covered with waste and
several dark stains.
Soil Sampling Results
On October 20, 2022, AECOM properly disposed of all visible waste material and excavated the top 12 inches of soil
from the approximate area presented in Figure 1. Approximately 340 bank cubic yards (BCY) were removed from the
area a, transported, and disposed at the South Wake County Landfill. After soil removal, AECOM personnel inspected
the cut floor for any remaining stains; no stains were observed. Once the excavation operations were completed,
AECOM personnel subdivided the excavated area into eight (8) approximately equal parts and collected a discrete
sample from the center of each sub -section (Figure 1). A duplicate sample and a background sample were also
collected. The background sample (BG-1) was collected upgradient from leachate-impacted areas, and the duplicate

sample was collected randomly from one of the sub -sections. A total of ten samples (BG-1, DUP-01, SS-1, SS-2, SS-
3, SS-4, SS-5, SS-6, SS-7, and SS-8) were collected. SS-4 sample exhibited a cobalt concentration that was twice the
concentration of all sample locations, including the background location. Therefore, an additional 6 inches
(approximately 22 BCY) of soil were removed from the SS-4 sub -section and disposed at the South Wake Landfill,
and a second sampling was conducted on November 29, 2022 to reconfirm sampling. A summary of soil sample
locations is provided in Table 1, and field notes are provided under Appendix A.
Collected samples were labeled, sealed, and placed on ice in coolers for transportation under chain of custody
protocol to Eurofins (formerly Environmental Conservation Laboratories, Inc.) for analysis of Volatile Organic
Compounds (VOCs) by Test Methods For Evaluating Solid Waste, Physical/Chemical Methods (SW-846) 8260D, 1,4-
dioxane by SW-846 8270E selective ion monitoring (SIM) with isotope dilution (ID), metals by SW-846 6010D,
mercury by SW-846 7471 B, total phosphorus by Environmental Protection Agency (EPA) Method 365.4, sulfate by
SW-846 9056A, nitrate by EPA Method 9056A, and pH by EPA Method 9045D.
Soil analytical results were compared to the NCDEQ Preliminary Soil Remediation Goals (PSRGs) — July 2022 and
the background sample BG-1. Arsenic, cobalt, and total phosphorus were detected above the NCDEQ PSRGs, but not
all exceeded the background sample BG-1. Details of analytes exceedances are summarized below:
Arsenic exceeded the Health -Based Residential PSRG in all nine sample locations, including the background
location. The arsenic background concentration, 2.7 milligrams per kilogram (mg/kg), was exceeded by three
sample locations which included sample locations SS-2, SS-3, and SS-6.
Cobalt exceeded the Protection of Groundwater PSRG in all nine sample locations, including the background
location, and exceeded the Health -Based Residential PSRG in sample location SS-7. The cobalt background
concentration (3.0 mg/kg) was exceeded by seven sample locations which included SS-1, SS-2, SS-3, SS-4, SS-
5, SS-6, and SS-7.
Total phosphorus exceeded the Health -Based PSRG and Protection of Groundwater PSRG in all nine sample
locations, including the background location. However, the total phosphorus background concentration (640
mg/kg) was not exceeded by any sample locations.
A summary of the analytical results is provided in Table 2, and exceedances are shown in Figure 2. The laboratory
analytical data report is provided in Appendix B, and a copy of the NCDEQ PSRGs — July 2022 is provided under
Appendix C.
Conclusions and Recommendations
In response to the NOV dated September 20, 2022, the following corrective measures were taken on leachate
impacted area investigated by the CoR:
• Sanitation operations were moved to the transfer station.
• CoR plastic rolling garbage bins containing leachate and waste were processed through the transfer station.
• Windblown waste was collected and processed through the transfer station.
• 12 inches of topsoil were removed from the leachate-impacted area, and confirmatory soil samples were
collected.
Arsenic, cobalt, and total phosphorus were detected at concentrations exceeding their respective PSRGs in all nine
sample locations, including the background location. The background sample and samples collected from the soil
removal area exhibited similar concentrations indicating that the detected concentrations are naturally occurring.
Additionally, the Metals and Radionuclides Analyses in Soil Cores from Mooresville, North Carolina investigation led
by Dr. Xiaoming Liu (University of North Carolina at Chapel Hill) and Drs. Heather Stapleton and Avner Vengosh
(Duke University) showed that cobalt and arsenic concentrations in soil cores collected from six sites near Mooresville,
North Carolina were higher than that of the background soil in North Carolina but consistent with cobalt and arsenic
concentrations expected in soils overlying Piedmont felsic rocks (Appendix D). Since the Site is located in the
Piedmont providence, the soil could be expected to exhibit higher concentrations of arsenic and cobalt naturally.
Based on the findings, all detected concentrations at the sample locations appear to be naturally occurring or
unrelated to leachate contamination. The analytical results and conclusions indicate that the leachate-impacted area
has been properly addressed in accordance with the response plan, and there are no continued hazards to public
health and safety.
aecom.com

Yours sincerely,
Jonathan Kucera
Senior Engineer/Project Manager
[e-mail]
cc: Megan Tosches, CoR
Stan Joseph, CoR
aecom.com

Tables

Table 1
Soil Sample Summary
East Wake Transfer Station
Facility Permit No. 9233T-TRANSFER-2008
Raleigh, Wake County, North Carolina
Soil Sample Code
BG-1
Sample Date
10/20/22
Sample Location Area
Background location upgradient
from leachate impacted areas
SS-1
10/20/22
Impacted soil located southwest
quadrant of the Site, generally south
of the service road and west of the
southern -most storage building
SS-2
10/20/22
SS-3
10/20/22
SS-4
10/20/22
SS-5
10/20/22
SS-6
10/20/22
SS-7
10/20/22
SS-8
10/20/22
DUP-01
10/20/22
Notes:
1. Total volatile organic compounds were not measured during sample
collection.
2. There were no leachate impacted soils at BG-1 (background location).
Page 1 of 1

Table 2
Detected Soil Constituents
East Wake Transfer Station
Facility Permit No. 9233T-TRANSFER-2008
Raleigh, Wake County, North Carolina
Soil
Health -Based Residential PSRG(1) NA I NA 0.68 3,100 31 1.4 4N
7 630 400 2.3 310 78 4,700 0.31 NG
25,000
NG
NG
Protection of Groundwater PSRG(1) NA
NA
5.80
580
63 3.0
700
270
1
1,200
0.0034
NG
NG
NG
NG
BG-1 (2)
ND
ND
2.7
72
0.34 J 0.26 J
20
18
0.081100
640
<9.4
4.0 J
6.1
84.7
SS-1
10/20/2022
ND
ND
2.7
52
0.41 <0.10
13
11
0.028
50
550 F1
130
<2.1
7.2
95.6
SS-2
10/20/2022
ND
ND
3.7
83
0.70 <0.11
16
17
0.036
53
260
120
<2.7
7.0
76.6
SS-3
10/20/2022
ND
ND
2.8
40 F2
0.62 0.35 J
15
25 F1
0.048
42
230
150
7.8 J
7.2
97.5
SS-4
10/20/2022
ND
ND
2.4
55
0.70
0 552
25
15
0.057
$33
M20
55
180
150
4.6 J
7.4
95.711/29/2022
4
NS
NS
2.3
50
0.44 J
<0.11
17 F1
12
0.024 J
53
NS
NS
NS
NS
NSSS-5
10/20/2022
ND
ND
1.8 J
46
0.33 J
0.12 J
18
6.6
0.2651
320
110
9.0 J
6.4
90.5SS-6
10/20/2022
ND
ND
3.0
83
0.74
0.18 J
14
11
0.021 J
58
260
45
<2.3
5.4
90.210/20/2022
ND
ND
1.9 J
99
0.80
0.21 J
15
12
0.022 J
72
290
<8.6
2.9 J
4.8
93.1
SS-8
10/20/2022
ND
ND
2.5
60
0.52
0.13 J
2.9
8.4
9.8
0.020 J
41
210
22 J
<2.7
4.9
76.7
DUP-01 (5)
10/20/2022
ND
ND
3.2
87
0.87
0.18 J
4.0
17
13
0.023 JB
4.5
30
55
310
<8.8
4.7J
4.8
90.0
nou:s:
This table presents the results of all detected soil target analytes.
(1) North Carolina Department of Environmental Quality Preliminary Soil Remediation Goals (PSRGs) - July 2022
(2) Background Sample
(3) PSRG based on the soluble salts criteria
(4) Reconfirmation sampling after an additional 6" of soil removal
(5) Duplicate sample was collected from location SS-7
< Indicates the result is below the method detection limit.
EPA - Environmental Protection Agency
B - The analyte was detected in the associated method blank.
J - The analytical result is less than the reporting limit but greater than or equal to the method detection limit. The concentration is an appropmate value.
NA - Not applicable
ND - Not detected
NG - No goal established
NS - Not sampled
F2 - MS/MSD Relative Percent Distance exceeds control limits
F1 - MS and/or MSD recovery exceeds control limits
MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not applicable.
SIM - Selective Ion Monitoring
SW-846 - Test Methods for Evaluating Solid Waste, PhysicaUChemical Methods (EPA)
VOC - Volatile organic compounds
Bold Concentration exceeds either the Residential PSRGs or Protection of Groundwater PSRGs.
Boltl Concentration exceeds either the Residential PSRGs or Protection of Groundwater PARGs and BG-1.
Page 1 of 1

Figures
aecom.com

r N
0
0
v I
4
CC
Transfer Trailer
Loading Bay
Transfer Station Building `
r
1
SS0
-1 SSS--2 SSS--3 SSS--4
S0
5 SO6 SS-SS-8 h~
.w
;F Source: E-sri, Maxar, GeoEye, Earthstar Ge•graphics, CNE�S/Airbus DS, USDA, USES, AeroGRID,
IGN, and the GIS User Community
Legend SCALE (FEET) CONFIDENTIAL
FIGURE 1
(BG-1) Background Sample o 100
AS-4 I
AECOM Sample Location (Sampled 10/20/2022; "Sampled 11/29/2022) SOIL REMOVAL AREA
Soil Removal Gridline DRAWNBY: REVIEWED BY AFF-D BY, DATE: P-ECTNO.
NOTES: miI Ir -- -- 12/20/2022 60620631
0 Soil Removal Area 1. SS-4 had second sampling (11/29/22) to reconfirm sampling after
an additional 6" of soil removal. EAST WAKE TRANSFER STATION
2. 12" of top soil were removed. CORPORATION PKWY

n
0
0
v
0
lit
Arsenic
2.7
Cobalt
3 0
Total Phosphorus
640
BG-1
ss-4
Arsenic
2.4
Cobalt
8.1
Total Phosphorus
1 180
SS-3
Arsenic
2.8
Cobalt
4.0
1 Af Y .
All A
Transfer Trailer
Loading Bay
1 �—
Kj
enic 37 t
)all 4.0 SS-1 SS-2 SS-3 SS-4
al Phosphorus 260 Q 0 0 Q
SS1
enic 2.7 SS-5 SS-6 SS-7 SS-8;`'"
salt 3.3 O O O O
0
Legend NOTES: SCALE(FEET) FIGURE 2
1. SS-4 had second sampling (11/29/22) to reconfirm sampling after 0 100
• (BG-1) Background Sample an additional 6" of soil removal.
IS AECOM Sample Location (Sampled 10/20/2022; —Sampled 11/29/2022 2. Only concentrations that exceeded the North Carolina Department of Environmental Quality
P ( P P ) Residential Preliminary Soil Remediation Goals (PSRG) or Protection of Groundwater PSRG (July 2022). SOIL ANALYTICAL RESULTS MAP
Soil Removal Gridline 3. Gray shading indicates exceedance of Background sample concentrations.
5. nits are in milligrams per kilograms. DRnwR ae RemeweDer nPP—D By, D PR.1—No.
U
Leachate Impacted Area investigated by Wake County 6. J - The analytical result is less than the reporting limit but greater than or equal to the method mikealr -- -- 12/20/2022 60620631
detection limit. The concentration is an approximate value.
0 Leachate Impacted Area investigated by the City of Raleigh 7. F1 - MS and/or MSD recovery exceeds control limits. EAST WAKE TRANSFER STATION
8. MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike CORPORATION PKWY
concentration; therefore, control limits are not applicable. fans FI(;H Nr:

Appendix A — Field Notes
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Appendix B — Laboratory Analytical Report
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2�SQ PCCRF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Tuesday, November 8, 2022
CITY OF RALEIGH (CI018)
Attn: Jon Kucera
PO BOX 590
RALEIGH, NC 27602-0590
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: City of Raleigh Soil Sampling Event
ENCO Workorder(s): CF15067
Dear Jon Kucera,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, October 20, 2022.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Daniel G. Harmon For Amanda L. Gaines
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 of 8

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: SS-1
Lab ID: CF15067-01
Sampled: 10/20/22 10:20
Received: 10/20/22 12:40
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 9045D
Same
10/25/22 09:31
10/25/22 09:17
10/25/22 11:38
EPA 9056A
WETS-88 Soil
10/23/22 10/23/22
08:35 10/21/22 08:35
10/21/22 11:33
Leaching
Client ID: SS-2
Lab ID: CF15067-02
Sampled: 10/20/22 10:25
Received: 10/20/22 12:40
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 9045D
Same
10/25/22 09:31
10/25/22 09:17
10/25/22 11:38
EPA 9056A
WETS-88 Soil
10/23/22 10/23/22
08:35 10/21/22 08:35
10/21/22 12:17
Leaching
Client ID: SS-3
Lab ID: CF15067-03
Sampled: 10/20/22 10:30
Received: 10/20/22 12:40
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 9045D
Same
10/25/22 09:31
10/25/22 09:17
10/25/22 11:38
EPA 9056A
WETS-88 Soil
10/23/22 10/23/22
08:35 10/21/22 08:35
10/21/22 12:31
Leaching
Client ID: SS-4
Lab ID: CF15067-04
Sampled: 10/20/22 10:35
Received: 10/20/22 12:40
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 9045D
Same
10/25/22 09:31
10/25/22 09:17
10/25/22 11:38
EPA 9056A
WETS-88 Soil
10/23/22 10/23/22
08:35 10/21/22 08:35
10/21/22 12:46
Leaching
Client ID: SS-5
Lab ID: CF15067-05
Sampled: 10/20/22 10:40
Received: 10/20/22 12:40
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 9045D
Same
10/25/22 09:31
10/25/22 09:17
10/25/22 11:38
EPA 9056A
WETS-88 Soil
10/23/22 10/23/22
08:35 10/21/22 08:35
10/21/22 13:00
Leaching
Client ID: SS-6
Lab ID: CF15067-06
Sampled: 10/20/22 10:45
Received: 10/20/22 12:40
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 9045D
Same
10/25/22 09:31
10/25/22 09:17
10/25/22 11:38
EPA 9056A
WETS-88 Soil
10/23/22 10/23/22
08:35 10/21/22 08:35
10/21/22 13:15
Leaching
Client ID: SS-7
Lab ID: CF15067-07
Sampled: 10/20/22 10:50
Received: 10/20/22 12:40
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 9045D
Same
10/25/22 09:31
10/25/22 09:17
10/25/22 11:38
EPA 9056A
WETS-88 Soil
10/23/22 10/23/22
08:35 10/21/22 08:35
10/21/22 13:58
Leaching
Client ID: SS-8
Lab ID: CF15067-08
Sampled: 10/20/22 10:55
Received: 10/20/22 12:40
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 9045D
Same
10/25/22 09:31
10/25/22 09:17
10/25/22 11:38
EPA 9056A
WETS-88 Soil
10/23/22 10/23/22
08:35 10/21/22 08:35
10/21/22 14:12
Leaching
Client ID: BG-1
Lab ID: CF15067-09
Sampled: 10/20/22 11:10
Received: 10/20/22 12:40
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 9045D
Same
10/25/22 09:31
10/25/22 09:17
10/25/22 11:38
EPA 9056A
WETS-88 Soil
10/23/22 10/23/22
08:35 10/21/22 08:35
10/21/22 14:27
Leaching
Client ID: DUP-01
Lab ID: CF15067-10
Sampled: 10/20/22 08:00
Received: 10/20/22 12:40
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 9045D
Same
10/25/22 09:31
10/25/22 09:17
10/25/22 11:38
EPA 9056A
WETS-88 Soil
10/23/22 10/23/22
08:35 10/21/22 08:35
10/21/22 14:41
Leaching
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 2 Of 8

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SAMPLE DETECTION SUMMARY
Client ID: SS-1
Lab ID:
CF15067-01
Analvte
Results
Flag MDL
PQL
Units
Method
Notes
PH
7.2
1.0
1.0
pH Units
EPA 9045D
Q-02
Temperature for pH (deg. C)
23
pH Units
EPA 9045D
Q-02
Client ID: SS-2
Lab ID:
CF15067-02
Analvte
Results
Flag MDL
PQL
Units
Method
Notes
PH
7.0
1.0
1.0
pH Units
EPA 9045D
Q-02
for pH (deg. C) 23 pH Units EPA 9045D
I Client ID: SS-3 Lab ID: CF15067-03
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Nitrate as N
7.8
J
2.1
10
mg/kg dry
EPA 9056A
PH
7.2
1.0
1.0
pH Units
EPA 9045D
Q-02
Temperature for pH (deg. C)
23
pH Units
EPA 9045D
Q-02
Client ID: SS-4
Lab ID:
CF15067-04
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Nitrate as N
4.6
J
2.1
10
mg/kg dry
EPA 9056A
PH
7.4
1.0
1.0
pH Units
EPA 9045D
Q-02
Temperature for pH (deg. C)
23
pH Units
EPA 9045D
Q-02
Client ID: SS-5
Lab ID:
CF15067-05
Analvte
Results
Flag MDL
PQL
Units
Method
Notes
Nitrate as N
9.0
1 2.3
11
mg/kg dry
EPA 9056A
PH
6.4
1.0
1.0
pH Units
EPA 9045D
Q-02
Temperature for pH (deg. C)
23
pH Units
EPA 9045D
Q-02
Client ID: SS-6
Lab ID:
CF15067-06
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
PH
5.4
1.0
1.0
pH Units
EPA 9045D
Q-02
Temperature for pH (deg. C)
23
pH Units
EPA 9045D
Q-02
Client ID: SS-7
Lab ID:
CF15067-07
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Nitrate as N
2.9
1
2.2
11
mg/kg dry
EPA 9056A
PH
4.8
1.0
1.0
pH Units
EPA 9045D
Q-02
Temperature for pH (deg. C)
23
pH Units
EPA 9045D
Q-02
Client ID: SS-8
Lab ID:
CF15067-08
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
PH
4.9
1.0
1.0
pH Units
EPA 9045D
Q-02
Temperature for pH (deg. C)
23
pH Units
EPA 9045D
Q-02
Client ID: BG-1
Lab ID:
CF15067-09
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Nitrate as N
4.0
J
2.4
12
mg/kg dry
EPA 9056A
PH
6.1
1.0
1.0
pH Units
EPA 9045D
Q-02
Temperature for pH (deg. C)
23
pH Units
EPA 9045D
Q-02
Client ID: DUP-01
Lab ID:
CF15067-10
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Nitrate as N
4.7
J
2.3
11
mg/kg dry
EPA 9056A
PH
4.8
1.0
1.0
pH Units
EPA 9045D
Q-02
Temperature for pH (deg. C)
23
pH Units
EPA 9045D
Q-02
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 Of 8

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ANALYTICAL RESULTS
Description: SS-1 Lab Sample ID:CF15067-01 Received: 10/20/22 12:40
Matrix: Soil Sampled: 10/20/22 10:20 Work Order: CF15067
Project: City of Raleigh Soil Sampling Event Sampled By: CLIENT % Solids: 95.60
Classical Chemistry Parameters
Analyte KAS Numberl Results
Flaa Units
DF
MDL P L Batch
Method
Analyzed
Ay Notes
Nitrate as N [14797-55-8] 2.1
U mg/kg dry
1
2.1 10 2J21007
EPA 9056A
10/21/22 11:33
MSE
pH 7.2
pH Units
1
1.0 1.0 2325006
EPA 9045D
10/25/22 11:38
CB Q-02
Temperature for pH (deg. C] 23
pH Units
1
2325006
EPA 9045D
10/25/22 11:38
CB Q-02
Description: SS-2 Lab Sample ID:CF15067-02 Received: 10/20/22 12:40
Matrix: Soil Sampled: 10/20/22 10:25 Work Order: CF15067
Project: City of Raleigh Soil Sampling Event Sampled By: CLIENT % Solids: 76.60
Classical Chemistry Parameters
Analyte rCAS Numberl Results
Flaa Units DF MDL P L
Batch
Method
Analyzed By Notes
Nitrate as N [14797-55-8] 2.7
U mg/kg dry 1 2.7 13
2321007
EPA 9056A
10/21/22 12:17 MSE
pH 7.0
pH Units 1 1.0 1.0
2325006
EPA 9045D
10/25/22 11:38 CB Q-02
Temperature for pH (deg. C] 23
pH Units 1
2325006
EPA 9045D
10/25/22 11:38 CB Q-02
Description: SS-3
Lab Sample ID:CF15067-03
Received: 10/20/22 12:40
Matrix: Soil
Sampled: 10/20/22 10:30
Work Order: CF15067
Project: City of Raleigh Soil Sampling Event
Sampled By: CLIENT
% Solids: 97.50
lClassical Chemistry Parameters
Analyte rCAS Numberl
Results
Flag Units
DF
MDL P L Batch
Method
Analyzed
—By Notes
Nitrate as N [14797-55-8]
7.8
J mg/kg dry
1
2.1 10 2321007
EPA 9056A
10/21/22 12:31
MSE
pH
7.2
pH Units
1
1.0 1.0 2325006
EPA 9045D
10/25/22 11:38
CB Q-02
Temperature for pH (deg. C]
23
pH Units
1
2325006
EPA 9045D
10/25/22 11:38
CB Q-02
Description: SS-4 Lab Sample ID:CF15067-04 Received: 10/20/22 12:40
Matrix: Soil Sampled: 10/20/22 10:35 Work Order: CF15067
Project: City of Raleigh Soil Sampling Event Sampled By: CLIENT % Solids: 95.70
Classical Chemistry Parameters
Analyte rCAS Numberl Results
Flag Units
DF
MDL P L Batch
Method
Analyzed
By Notes
Nitrate as N [34797-55-8] 4.6
J mg/kg dry
1
2.1 10 2321007
EPA 9056A
10/21/22 12:46
MSE
pH 7.4
pH Units
1
1.0 1.0 2325006
EPA 9045D
10/25/22 11:38
CB Q-02
Temperature for pH (deg. C] 23
pH Units
1
2325006
EPA 9045D
10/25/22 11:38
CB Q-02
Description: SS-5 Lab Sample ID:CF15067-05 Received: 10/20/22 12:40
Matrix: Soil Sampled: 10/20/22 10:40 Work Order: CF15067
Project: City of Raleigh Soil Sampling Event Sampled By: CLIENT a/o Solids: 90.50
Classical Chemistry Parameters
Analyte rCAS Numberl Results
Flag Units
DF
MDL PQL Batch
Method
Analyzed
By Notes
Nitrate as N [14797-55-8] 9.0
J mg/kg dry
1
2.3 11 2121007
EPA 9056A
10/21/22 13:00
MSE
pH 6.4
pH Units
1
1.0 1.0 2125006
EPA 9045D
10/25/22 11:38
CB Q-02
Temperature for pH (deg. C] 23
pH Units
1
2125006
EPA 9045D
10/25/22 11:38
CB Q-02
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 4 Of 8

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ANALYTICAL RESULTS
Description: SS-6 Lab Sample ID:CF15067-06 Received: 10/20/22 12:40
Matrix: Soil Sampled: 10/20/22 10:45 Work Order: CF15067
Project: City of Raleigh Soil Sampling Event Sampled By: CLIENT % Solids: 90.20
Classical Chemistry Parameters
Analyte KAS Numberl Results
Flaa Units
DF
MDL POLL Batch
Method
Analyzed
Ay Notes
Nitrate as N [14797-55-8] 2.3
U mg/kg dry
1
2.3 11 2J21007
EPA 9056A
10/21/22 13:15
MSE
pH 5.4
pH Units
1
1.0 1.0 2325006
EPA 9045D
10/25/22 11:38
CB Q-02
Temperature for pH (deg. C] 23
pH Units
1
2325006
EPA 9045D
10/25/22 11:38
CB Q-02
Description: SS-7 Lab Sample ID:CF15067-07 Received: 10/20/22 12:40
Matrix: Soil Sampled: 10/20/22 10:50 Work Order: CF15067
Project: City of Raleigh Soil Sampling Event Sampled By: CLIENT % Solids: 93.10
Classical Chemistry Parameters
Analyte rCAS Numberl Results
Flaa Units DF MDL P L
Batch
Method
Analyzed By Notes
Nitrate as N [14797-55-8] 2.9
J mg/kg dry 1 2.2 11
2321007
EPA 9056A
10/21/22 13:58 MSE
pH 4.8
pH Units 1 1.0 1.0
2325006
EPA 9045D
10/25/22 11:38 CB Q-02
Temperature for pH (deg. C] 23
pH Units 1
2325006
EPA 9045D
10/25/22 11:38 CB Q-02
Description: SS-8
Lab Sample ID:CF15067-08
Received: 10/20/22 12:40
Matrix: Soil
Sampled: 10/20/22 10:55
Work Order: CF15067
Project: City of Raleigh Soil Sampling Event
Sampled By: CLIENT
% Solids: 76.70
lClassical Chemistry Parameters
Analyte rCAS Numberl
Results
Flag Units
DF
MDL P L Batch
Method
Analyzed
—By Notes
Nitrate as N [14797-55-8]
2.7
U mg/kg dry
1
2.7 13 2321007
EPA 9056A
10/21/22 14:12
MSE
pH
4.9
pH Units
1
1.0 1.0 2325006
EPA 9045D
10/25/22 11:38
CB Q-02
Temperature for pH (deg. C]
23
pH Units
1
2325006
EPA 9045D
10/25/22 11:38
CB Q-02
Description: BG-1 Lab Sample ID:CF15067-09 Received: 10/20/22 12:40
Matrix: Soil Sampled: 10/20/22 11:10 Work Order: CF15067
Project: City of Raleigh Soil Sampling Event Sampled By: CLIENT % Solids: 84.70
Classical Chemistry Parameters
Analyte rCAS Numberl Results
Flag Units
DF
MDL P L Batch
Method
Analyzed
By Notes
Nitrate as N [34797-55-8] 4.0
J mg/kg dry
1
2.4 12 2321007
EPA 9056A
10/21/22 14:27
MSE
pH 6.1
pH Units
1
1.0 1.0 2325006
EPA 9045D
10/25/22 11:38
CB Q-02
Temperature for pH (deg. C] 23
pH Units
1
2325006
EPA 9045D
10/25/22 11:38
CB Q-02
Description: DUP-01 Lab Sample ID:CF15067-10 Received: 10/20/22 12:40
Matrix: Soil Sampled: 10/20/22 08:00 Work Order: CF15067
Project: City of Raleigh Soil Sampling Event Sampled By: CLIENT a/o Solids: 90.00
Classical Chemistry Parameters
Analyte rCAS Numberl Results
Flag Units
DF
MDL PQL Batch
Method
Analyzed
By Notes
Nitrate as N [14797-55-8] 4.7
J mg/kg dry
1
2.3 11 2121007
EPA 9056A
10/21/22 14:41
MSE
pH 4.8
pH Units
1
1.0 1.0 2125006
EPA 9045D
10/25/22 11:38
CB Q-02
Temperature for pH (deg. C] 23
pH Units
1
2125006
EPA 9045D
10/25/22 11:38
CB Q-02
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Pager) Of 8

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QUALITY CONTROL DATA
Classical Chemistry Parameters - Quality Control
Batch 2121007 - WETS-88 Soil Leaching
Blank (2121007-BLK1) Prepared: 10/21/2022 08:35 Analyzed: 10/21/2022 11:04
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes
Nitrate as N 2.0 U 10 mg/kg wet
LCS (2721007-BS3) Prepared: 10/21/2022 08:35 Analyzed: 10/21/2022 11:19
Spike Source O/oREC
RPD
Analvte
Result Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Nitrate as N
51
10
mg/kg wet
50.0 102 80-120
Matrix Spike (2J23007-MS1)
Prepared: 10/21/2022 08:35 Analyzed: 10/21/2022 11:48
Source: CF15067-01
Spike Source O/oREC
RPD
Analvte
Result Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Nitrate as N
20
10
mg/kg dry
20.9 2.1 U 94 80-120
Matrix Spike Dup (2321007-MSD1)
Prepared: 10/21/2022 08:35 Analyzed: 10/21/2022 12:02
Source: CF15067-01
Spike Source O/oREC
RPD
Analvte
Result Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit Notes
Nitrate as N
19
10
mg/kg dry
20.9 2.1 U 91 80-120 3
15
Batch Z725006 - Same
LCS (2325006-BS3) Prepared: 10/25/2022 09:17 Analyzed: 10/25/2022 11:38
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit Notes
pH
7.0
1.0
pH Units
7.00 100 99-101
Duplicate (2125006-DUPI)
Prepared: 10/25/2022 09:17 Analyzed: 10/25/2022 11:38
Source: CF15067-01
Spike Source O/oREC
RPD
Analvte
Result Flaq
POL
Units
Level Result O/oREC Limits RPD
Limit Notes
pH
7.2
1.0
pH Units
7.2 0.6
25
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 6 Of 8

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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
Q-02 Sample received outside of method - specified holding time.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 7 of 8

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a

urofins
Environment Testing
ANALYTICAL REPORT
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-223856-1
Client Project/Site: CF15067
Revision: 1
For:
Environmental Conservation Laboratories
102 Woodwinds Industrial Ct, Suite A
Cary, North Carolina 27511
Attn: Amanda Gaines
Authorized for release by:
111812022 7:52:54 AM
Naomi Flanagan, Project Manager
[phone]
[e-mail]
Designee for
Sheila Hoffman, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI
requirements for accredited parameters, exceptions are noted in this report. This
report may not be reproduced except in full, and with written approval from the
laboratory. For questions please contact the Project Manager at the e-mail address or
telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic
signature is intended to be the legally binding equivalent of a traditionally handwritten
signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: Environmental Conservation Laboratories Sample Summary Job ID: 680-223856-1
Project/Site: CF15067
Lab Sample ID
Client Sample ID
Matrix
Collected
Received
680-223856-1
SS-1
Solid
10/20/22 10:20
10/22/22
07:00
680-223856-2
SS-2
Solid
10/20/22 10:25
10/22/22
07:00
680-223856-3
SS-3
Solid
10/20/22 10:30
10/22/22
07:00
680-223856-4
SS-4
Solid
10/20/22 10:35
10/22/22
07:00
680-223856-5
SS-5
Solid
10/20/22 10:40
10/22/22
07:00
680-223856-6
SS-6
Solid
10/20/22 10:45
10/22/22
07:00
680-223856-7
SS-7
Solid
10/20/22 10:50
10/22/22
07:00
680-223856-8
SS-8
Solid
10/20/22 10:55
10/22/22
07:00
680-223856-9
BG-1
Solid
10/20/22 11:10
10/22/22
07:00
680-223856-10
DUP-01
Solid
10/20/22 08:00
10/22/22
07:00
680-223856-11
Trip Blank
Water
10/20/22 08:00
10/22/22
07:00
680-223856-12
Trip Blank
Water
10/20/22 08:00
10/22/22
07:00
Page 2 of 81 1 )

Method Summary
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
U
Method
Method Description
Protocol
Laboratory
8260D
Volatile Organic Compounds by GC/MS
SW846
EET SAV
8270E SIM ID
Semivolatile Organic Compounds (GC/MS SIM / Isotope Dilution)
SW846
EET SAV
9056A
Anions, Ion Chromatography
SW846
EET SAV
6010D
Metals (ICP)
SW846
EET SAV
7471 B
Mercury (CVAA)
SW846
EET SAV
365.4-1974
Phosphorus, Total
EPA
EET SAV
Moisture
Percent Moisture
EPA
EET SAV
3050B
Preparation, Metals
SW846
EET SAV
3546
Microwave Extraction
SW846
EET SAV
5030C
Purge and Trap
SW846
EET SAV
5035A
Closed System Purge & Trap
SW846
EET SAV
7471 B
Preparation, Mercury
SW846
EET SAV
DI Leach
Deionized Water Leaching Procedure
ASTM
EET SAV
Digestion
Digestion, Hot Block
MCAWW
EET SAV
Protocol References:
ASTM = ASTM International
EPA= US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
Page 3 of 81 11 /8/2022 (Rev. 1)

Definitions/Glossary
Client: Environmental Conservation Laboratories Job ID: 680-223856-1
Project/Site: CF15067
Qualifiers
GC/MS VOA
Qualifier Qualifier Description
*+ LCS and/or LCSD is outside acceptance limits, high biased.
E Result exceeded calibration range.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
HPLC/IC
Qualifier Qualifier Description
F1 MS and/or MSD recovery exceeds control limits.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Metals
Qualifier Qualifier Description
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
B Compound was found in the blank and sample.
F1 MS and/or MSD recovery exceeds control limits.
F2 MS/MSD RPD exceeds control limits
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
General Chemistry
Qualifier Qualifier Description
F1 MS and/or MSD recovery exceeds control limits.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
a Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level'
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
Eurofins Savannah
Page 4 of 81 11/8/2022 (Rev. 1)

Definitions/Glossary
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Glossary (Continued)
Abbreviation These commonly used abbreviations may or may not be present in this report.
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
F
Job ID: 680-223856-1
U
Eurofins Savannah
Page 5 of 81 11 /8/2022 (Rev. 1)

Case Narrative
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-223856-1
Comments
No additional comments.
Job ID: 680-223856-1
Revision
The report being provided is a revision of the original report sent on 11/4/2022. The report (revision 1) is being revised due to: Client wants
analytes removed. Original analyte list not provided.
Receipt
The samples were received on 10/22/2022 7:00 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 1.30 C.
GC/MS VOA
Method 8260D: The laboratory control sample (LCS) for analytical batch 680-748284 recovered outside control limits for the following
analytes: Carbon disulfide. This analyte was biased high in the LCS and was not detected in the associated samples; therefore, the data
have been reported.
Method 8260D: The continuing calibration verification (CCV) associated with batch 680-748284 recovered above the upper control limit for
1, 1 -Dichloroethene, Carbon disulfide, Chloroethane and Methylene Chloride. The samples associated with this CCV were non -detects for
the affected analytes; therefore, the data have been reported.
Method 8260D: The continuing calibration verification (CCV) associated with batch 680-748284 recovered outside acceptance criteria, low
biased, for 2-Butanone (MEK) and Methyl tert-butyl ether. A reporting limit (RL) standard was analyzed, and the target analytes are
detected. Since the associated samples were non -detect for the analyte(s), the data are reported.
Method 8260D: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
analytical batch 680-748284.
Method 8260D: The continuing calibration verification (CCV) associated with batch 680-748517 recovered above the upper control limit for
Acetonitrile, Methacrylonitrile, Methyl methacrylate and Propionitrile. The samples associated with this CCV were non -detects for the
affected analytes; therefore, the data have been reported.
Method 8260D: The continuing calibration verification (CCV) associated with batch 680-748517 recovered above the upper control limit for
1,1,2-Trichloro-1,2,2-trifluoroethane, 3-Chloro-1-propene, 1,1-Dichloroethene, Carbon disulfide, Cyclohexane, Chlorobromomethane,
Methyl acetate and Trichlorofluoromethane. The samples associated with this CCV were non -detects for the affected analytes; therefore,
the data have been reported.
Method 8260D: The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for analytical batch 680-748517
recovered outside control limits for the following analytes: Carbon disulfide. This analyte was biased high in the LCS and was not
detected in the associated samples; therefore, the data have been reported.
Method 8260D: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
preparation batch 680-746886 and analytical batch 680-748517.
Method 8260D: The continuing calibration verification (CCV) associated with batch 680-748537 recovered above the upper control limit for
Dichlorobromomethane, 1,1,1-Trichloroethane, 1,2-Dibromo-3-Chloropropane and Trichlorofluoromethane. The samples associated with
this CCV were non -detects for the affected analytes; therefore, the data have been reported.
Eurofins Savannah
Page 6 of 81 11 /8/2022 (Rev. 1)

Case Narrative
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1 (Continued)
Laboratory: Eurofins Savannah (Continued)
Job ID: 680-223856-1
Method 8260D: The laboratory control sample (LCS) for analytical batch 680-748537 recovered outside control limits for the following
analytes: 1,2-Dibromo-3-Chloropropane and Trichlorofluoromethane. These analytes were biased high in the LCS and were not detected
in the associated samples; therefore, the data have been reported.
Method 8260D: The laboratory control sample duplicate (LCSD) for analytical batch 680-748537 recovered outside control limits for the
following analytes: 1,2-Dibromo-3-Chloropropane, Acetone and Trichlorofluoromethane. These analytes were biased high in the LCSD
and were not detected in the associated samples; therefore, the data have been reported.
Method 8260D: The method blank for preparation batch <PrepBatch> contained Acetone above the reporting limit (RL). None of the
samples associated with this method blank contained the target compound; therefore, re -extraction and/or re -analysis of samples were
not performed.
Method 8260D: The method blank associated with analytical batch 680-748537 contained Styrene greater than one-half the reporting limit
(RL). The samples could not be re -analyzed because not detected. The sample results have been qualified and reported.
Method 8260D: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
analytical batch 680-748537.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
HPLC/IC
Method 9056A: The matrix spike / matrix spike duplicate (MS/MSD) recoveries and precision for preparation batch 680-748171 and
analytical batch 680-748340 were outside control limits. Sample matrix interference and/or non -homogeneity are suspected because the
associated laboratory control sample / laboratory sample control duplicate (LCS/LCSD) precision was within acceptance limits.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Eurofins Savannah
Page 7 of 81 11 /8/2022 (Rev. 1)

Detection Summary
Client: Environmental Conservation Laboratories
Job ID:
680-223856-1
Project/Site: CF15067
Client Sample ID: SS-1
Lab Sample ID: 680-223856-1
Analyte
Result
Qualifier
RL
MDL
Unit
Dil Fac
D
Method
Prep Type
Sulfate
130
21
8.4
mg/Kg
1
*
9056A
Soluble
Arsenic
2.7
2.0
1.2
mg/Kg
1
*
601OD
Total/NA
Barium
52
1.0
0.41
mg/Kg
1
*
6010D
Total/NA
Lead
11
1.0
0.61
mg/Kg
1
*
6010D
Total/NA
Beryllium
0.41
0.40
0.071
mg/Kg
1
*
6010D
Total/NA
Nickel
5.3
4.0
0.91
mg/Kg
1
*
6010D
Total/NA
Vanadium
25
1.0
0.16
mg/Kg
1
*
6010D
Total/NA
Copper
13
2.5
0.50
mg/Kg
1
*
6010D
Total/NA
Zinc
50
2.0
0.58
mg/Kg
1
*
6010D
Total/NA
Cobalt
3.3
1.0
0.33
mg/Kg
1
*
6010D
Total/NA
Mercury
0.028
0.025
0.0079
mg/Kg
1
*
7471 B
Total/NA
Phosphorus
550
F1
51
28
mg/Kg
5
*
365.4-1974
Total/NA
Client Sample ID: SS-2
Lab Sample ID: 680-223856-2
Analyte
Result
Qualifier
RL
MDL
Unit
Dil Fac
D
Method
Prep Type
Sulfate
120
26
10
mg/Kg
1
*
9056A
Soluble
Arsenic
3.7
2.1
1.3
mg/Kg
1
*
601OD
Total/NA
Barium
83
1.1
0.44
mg/Kg
1
*
601OD
Total/NA
Lead
17
1.1
0.65
mg/Kg
1
*
601OD
Total/NA
Beryllium
0.70
0.43
0.076
mg/Kg
1
*
601OD
Total/NA
Nickel
5.8
4.3
0.96
mg/Kg
1
*
601OD
Total/NA
Vanadium
33
1.1
0.17
mg/Kg
1
*
601OD
Total/NA
Copper
16
2.7
0.54
mg/Kg
1
*
601OD
Total/NA
Zinc
53
2.1
0.62
mg/Kg
1
*
601OD
Total/NA
Cobalt
4.0
1.1
0.35
mg/Kg
1
*
601OD
Total/NA
Mercury
0.036
0.030
0.0095
mg/Kg
1
*
7471 B
Total/NA
Phosphorus
260
13
7.0
mg/Kg
1
*
365.4-1974
Total/NA
Client Sample ID: SS-3
Lab Sample ID: 680-223856-3
Analyte
Result
Qualifier
RL
MDL
Unit
Dil Fac
D
Method
Prep Type
Sulfate
150
20
8.2
mg/Kg
1
9056A
Soluble
Arsenic
2.8
2.1
1.2
mg/Kg
1
*
6010D
Total/NA
Barium
40
F2
1.0
0.42
mg/Kg
1
*
6010D
Total/NA
Cadmium
0.35
J
0.51
0.10
mg/Kg
1
*
6010D
Total/NA
Lead
25
F1
1.0
0.63
mg/Kg
1
*
6010D
Total/NA
Beryllium
0.62
0.41
0.073
mg/Kg
1
*
6010D
Total/NA
Nickel
5.7
4.1
0.92
mg/Kg
1
*
6010D
Total/NA
Vanadium
46
1.0
0.16
mg/Kg
1
*
601OD
Total/NA
Copper
15
2.6
0.51
mg/Kg
1
*
601OD
Total/NA
Zinc
42
2.1
0.59
mg/Kg
1
*
601OD
Total/NA
Cobalt
4.0
1.0
0.34
mg/Kg
1
*
601OD
Total/NA
Mercury
0.048
0.025
0.0080
mg/Kg
1
*
7471 B
Total/NA
Phosphorus
230
10
5.6
mg/Kg
1
*
365.4-1974
Total/NA
Client Sample ID: SS-4
Lab Sample ID: 680-223856-4
Analyte
Result
Qualifier
RL
MDL
Unit
Dil Fac
D
Method
Prep Type
Sulfate
150
21
8.3
mg/Kg
1
*
9056A
Soluble
Arsenic
2.4
2.1
1.3
mg/Kg
1
*
6010D
Total/NA
Barium
55
1.0
0.43
mg/Kg
1
*
6010D
Total/NA
This Detection Summary does not include radiochemical test results.
Eurofins Savannah
Page 8 of 81 11/8/2022 (Rev. 1)

Detection Summary
Client: Environmental Conservation Laboratories
Job ID:
680-223856-1
Project/Site: CF15067
Client Sample ID: SS-4 (Continued)
Lab Sample ID: 680-223856-4
Analyte
Result
Qualifier
RL
MDL
Unit
Dil Fac
D
Method
Prep Type
Cadmium
0.52
0.52
0.10
mg/Kg
1
*
601OD
Total/NA '
Lead
15
1.0
0.64
mg/Kg
1
*
601OD
Total/NA
Beryllium
0.70
0.42
0.074
mg/Kg
1
*
6010D
Total/NA
Nickel
11
4.2
0.94
mg/Kg
1
*
6010D
Total/NA
Vanadium
65
1.0
0.17
mg/Kg
1
*
6010D
Total/NA
Copper
25
2.6
0.52
mg/Kg
1
*
6010D
Total/NA
Zinc
55
2.1
0.61
mg/Kg
1
*
6010D
Total/NA
Cobalt
8.1
1.0
0.34
mg/Kg
1
*
6010D
Total/NA
Mercury
0.057
0.025
0.0079
mg/Kg
1
*
7471 B
Total/NA
Phosphorus
180
10
5.6
mg/Kg
1
*
365.4-1974
Total/NA
Client Sample ID: SS-5
Lab Sample ID: 680-223856-5
C
Analyte
Result
Qualifier
RL
MDL
Unit
Dill Fac
D
Method
Prep Type
Sulfate
110
22
8.8
mg/Kg
1
*
9056A
Soluble
Arsenic
1.8
J
2.1
1.3
mg/Kg
1
*
601OD
Total/NA
Barium
46
1.1
0.44
mg/Kg
1
*
601OD
Total/NA
Cadmium
0.12
J
0.53
0.11
mg/Kg
1
*
601OD
Total/NA
Lead
6.6
1.1
0.65
mg/Kg
1
*
601OD
Total/NA
Beryllium
0.33
J
0.42
0.075
mg/Kg
1
*
601OD
Total/NA
Nickel
3.7
J
4.2
0.96
mg/Kg
1
*
601OD
Total/NA
Vanadium
21
1.1
0.17
mg/Kg
1
*
601OD
Total/NA
Copper
18
2.7
0.53
mg/Kg
1
*
601OD
Total/NA
Zinc
51
2.1
0.62
mg/Kg
1
*
601OD
Total/NA
Cobalt
3.3
1.1
0.35
mg/Kg
1
*
601OD
Total/NA
Mercury
0.26
0.027
0.0085
mg/Kg
1
*
7471 B
Total/NA
Phosphorus
320
11
6.0
mg/Kg
1
*
365.4-1974
Total/NA
Client Sample ID: SS-6
Lab Sample ID: 680-223856-6
Analyte
Result
Qualifier
RL
MDL
Unit
Dil Fac
D
Method
Prep Type
Sulfate
45
22
8.8
mg/Kg
1
0
9056A
Soluble
Arsenic
3.0
1.9
1.2
mg/Kg
1
*
6010D
Total/NA
Barium
83
0.97
0.40
mg/Kg
1
*
6010D
Total/NA
Cadmium
0.18
J
0.49
0.097
mg/Kg
1
*
6010D
Total/NA
Lead
11
0.97
0.59
mg/Kg
1
*
6010D
Total/NA
Beryllium
0.74
0.39
0.069
mg/Kg
1
#
6010D
Total/NA
Nickel
3.8
J
3.9
0.87
mg/Kg
1
*
6010D
Total/NA
Vanadium
26
0.97
0.16
mg/Kg
1
*
6010D
Total/NA
Copper
14
2.4
0.49
mg/Kg
1
*
6010D
Total/NA
Zinc
58
1.9
0.56
mg/Kg
1
*
601OD
Total/NA
Cobalt
4.0
0.97
0.32
mg/Kg
1
*
601OD
Total/NA
Mercury
0.021
J
0.027
0.0085
mg/Kg
1
*
7471 B
Total/NA
Phosphorus
260
11
6.1
mg/Kg
1
*
365.4-1974
Total/NA
Client Sample ID: SS-7
Lab Sample ID: 680-223856-7
Analyte
Result
Qualifier
RL
MDL
Unit
Dil Fac
D
Method
Prep Type
Arsenic
1.9
J
2.0
1.2
mg/Kg
1
*
6010D
Total/NA
Barium
99
1.0
0.42
mg/Kg
1
*
6010D
Total/NA
Cadmium
0.21
J
0.51
0.10
mg/Kg
1
*
6010D
Total/NA
Lead
12
1.0
0.62
mg/Kg
1
*
6010D
Total/NA
This Detection Summary does not include radiochemical test results.
Eurofins Savannah
Page 9 of 81 11/8/2022 (Rev. 1)

Detection Summary
Client: Environmental Conservation Laboratories
Job ID:
680-223856-1
Project/Site: CF15067
Client Sample ID: SS-7 (Continued)
Lab Sample ID: 680-223856-7
Analyte
Result
Qualifier
RL
MDL
Unit
Dil Fac
D
Method
Prep Type
Beryllium
0.80
0.41
0.072
mg/Kg
1
*
601OD
Total/NA '
Nickel
3.8
J
4.1
0.91
mg/Kg
1
*
6010D
Total/NA
Vanadium
29
1.0
0.16
mg/Kg
1
*
6010D
Total/NA
Copper
15
2.5
0.51
mg/Kg
1
*
6010D
Total/NA
Zinc
72
2.0
0.59
mg/Kg
1
*
6010D
Total/NA
Cobalt
4.8
1.0
0.33
mg/Kg
1
*
6010D
Total/NA
Mercury
0.022
J
0.023
0.0074
mg/Kg
1
*
7471 B
Total/NA
Phosphorus
290
10
5.7
mg/Kg
1
*
365.4-1974
Total/NA
Client Sample ID: SS-8
Lab Sample ID: 680-223856-8
Analyte
Result
Qualifier
RL
MDL
Unit
Dil Fac
D
Method
Prep Type
C
Sulfate
22
J
26
10
mg/Kg
1
9056A
Soluble
Arsenic
2.5
2.2
1.3
mg/Kg
1
*
601OD
Total/NA
Barium
60
1.1
0.45
mg/Kg
1
*
601OD
Total/NA
Cadmium
0.13
J
0.54
0.11
mg/Kg
1
*
601OD
Total/NA
Lead
9.8
1.1
0.66
mg/Kg
1
*
601OD
Total/NA
Beryllium
0.52
0.43
0.077
mg/Kg
1
*
601OD
Total/NA
Nickel
3.3
J
4.3
0.98
mg/Kg
1
*
601OD
Total/NA
Vanadium
20
1.1
0.17
mg/Kg
1
*
601OD
Total/NA
Copper
8.4
2.7
0.54
mg/Kg
1
*
601OD
Total/NA
Zinc
41
2.2
0.63
mg/Kg
1
*
601OD
Total/NA
Cobalt
2.9
1.1
0.36
mg/Kg
1
*
601OD
Total/NA
Mercury
0.020
J
0.029
0.0093
mg/Kg
1
*
7471 B
Total/NA
Phosphorus
210
13
6.9
mg/Kg
1
*
365.4-1974
Total/NA
Client Sample ID: BG-1
Lab Sample ID: 680-223856-9
Analyte
Result
Qualifier
RL
MDL
Unit
Dil Fac
D
Method
Prep Type
Arsenic
2.7
2.3
1.4
mg/Kg
1
*
601OD
Total/NA
Barium
72
1.2
0.47
mg/Kg
1
*
6010D
Total/NA
Cadmium
0.26
J
0.58
0.12
mg/Kg
1
*
6010D
Total/NA
Lead
18
1.2
0.71
mg/Kg
1
*
6010D
Total/NA
Beryllium
0.34
J
0.46
0.082
mg/Kg
1
*
6010D
Total/NA
Nickel
6.0
4.6
1.0
mg/Kg
1
*
6010D
Total/NA
Vanadium
24
1.2
0.19
mg/Kg
1
*
6010D
Total/NA
Copper
20
2.9
0.58
mg/Kg
1
*
6010D
Total/NA
Zinc
100
2.3
0.67
mg/Kg
1
*
6010D
Total/NA
Cobalt
3.0
1.2
0.38
mg/Kg
1
*
6010D
Total/NA
Mercury
0.081
0.028
0.0089
mg/Kg
1
*
7471 B
Total/NA
Phosphorus
640
57
32
mg/Kg
5
*
365.4-1974
Total/NA
Client Sample ID: DUP-01
Lab Sample ID: 680-223856-10
Analyte
Result
Qualifier
RL
MDL
Unit
Dil Fac
D
Method
Prep Type
Arsenic
3.2
1.9
1.2
mg/Kg
1
*
601OD
Total/NA
Barium
87
0.97
0.40
mg/Kg
1
*
601OD
Total/NA
Cadmium
0.18
J
0.49
0.097
mg/Kg
1
*
601OD
Total/NA
Lead
13
0.97
0.59
mg/Kg
1
*
601OD
Total/NA
Beryllium
0.87
0.39
0.069
mg/Kg
1
*
601OD
Total/NA
Nickel
4.5
3.9
0.88
mg/Kg
1
*
601OD
Total/NA
Vanadium
30
0.97
0.16
mg/Kg
1
*
601OD
Total/NA
This Detection Summary does not include radiochemical test results.
Eurofins Savannah
Page 10 of 81 11/8/2022 (Rev. 1)

Detection Summary
Client: Environmental Conservation Laboratories
Job ID: 680-223856-1
Project/Site: CF15067
Client Sample ID: DUP-01 (Continued)
Lab Sample ID: 680-223856-10
Analyte Result Qualifier
RL
MDL
Unit
Dil Fac D Method Prep Type
Copper 17
2.4
0.49
mg/Kg
1 * 601OD Total/NA '
Zinc 55
1.9
0.57
mg/Kg
1 * 6010D Total/NA
Cobalt 4.0
0.97
0.32
mg/Kg
1 * 6010D Total/NA
Mercury 0.023 J B
0.026
0.0084
mg/Kg
1 * 7471 B Total/NA
Phosphorus 310
11
5.9
mg/Kg
1 * 365.4-1974 Total/NA
Client Sample ID: Trip Blank
Lab Sample ID: 680-223856-11
ENo Detections.
Client Sample ID: Trip Blank
Lab Sample ID: 680-223856-12
INo Detections
This Detection Summary does not include radiochemical test results.
Page 11 of 81
Eurofins Savannah
11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: SS-1 Lab Sample ID: 680-223856-1
Date Collected: 10/20/22 10:20 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 95.6
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
Analyte
Result Qualifier
RL
1,1,1,2-Tetrachloroethane
<1.4
5.4
1,1,1-Trichloroethane
<2.8
5.4
1,1,2-Trichloroethane
<1.6
5.4
1,1-Dichloroethane
<3.1
5.4
1,1-Dichloroethene
<3.9
5.4
1,2,3-Trichlorobenzene
<2.2
5.4
1,2,4-Trichlorobenzene
<2.7
5.4
1,2-Dibromo-3-Chloropropane
<1.7
11
1,2-Dibromoethane
<1.8
5.4
1,2-Dichlorobenzene
<1.8
5.4
1,2-Dichloroethane
<2.5
5.4
1,2-Dichloropropane
<2.8
5.4
1,3-Dichlorobenzene
<2.2
5.4
1,4-Dichlorobenzene
<1.9
5.4
2-Butanone (MEK)
<10
27
2-Hexanone
<21
27
4-Methyl-2-pentanone (MIBK)
<19
27
Acetone
<12
54
Benzene
<2.6
5.4
Bromochloromethane
<2.2
5.4
Bromoform
<2.4
5.4
Bromomethane
<2.6
5.4
Carbon disulfide
<2.3 '+
5.4
Carbon tetrachloride
<2.3
5.4
Chlorobenzene
<1.5
5.4
Chloroethane
<2.4
5.4
Chloroform
<2.2
5.4
Chloromethane
<2.6
5.4
cis-1,2-Dichloroethene
<3.1
5.4
cis-1,3-Dichloropropene
<2.4
5.4
Cyclohexane
<2.5
5.4
Dichlorobromomethane
<2.2
5.4
Dichlorodifluoromethane
<3.5
5.4
Ethylbenzene
<2.3
5.4
Freon 113
<3.1
5.4
Hexachlorobutadiene
<4.4
5.4
Isopropylbenzene
<2.4
5.4
Methyl acetate
<8.8
27
Methyl tert-butyl ether
<2.4
5.4
Methylcyclohexane
<2.2 '+
5.4
Methylene Chloride
<8.7
11
m-Xylene & p-Xylene
<2.4
5.4
o-Xylene
<2.5
5.4
Styrene
<2.1
5.4
Tetrachloroethene
<2.8
5.4
Toluene
<2.8
5.4
trans- 1,2-Dichloroethene
<2.5
5.4
trans- 1,3-Dichloropropene
<2.8
5.4
Trichloroethene
<1.9
5.4
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1.4
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
2.8
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
1.6
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
3.1
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
3.9
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
2.2
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
2.7
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
1.7
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
1.8
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
1.8
ug/Kg
10/25/2212:49
11/03/2210:44
1
2.5
ug/Kg
10/25/2212:49
11/03/2210:44
1
2.8
ug/Kg
10/25/2212:49
11/03/2210:44
1
2.2
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
1.9
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
10
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
21
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
19
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
12
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
2.6
ug/Kg
10/25/2212:49
11/03/2210:44
1
2.2
ug/Kg
10/25/2212:49
11/03/2210:44
1
2.4
ug/Kg
10/25/2212:49
11/03/2210:44
1
2.6
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
2.3
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
2.3
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
1.5
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
2.4
ug/Kg
10/25/2212:49
11/03/2210:44
1
2.2
ug/Kg
10/25/2212:49
11/03/2210:44
1
2.6
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
3.1
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
2.4
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
2.5
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
2.2
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
3.5
ug/Kg
*
10/25/2212:49
11/03/2210:44
1
2.3
ug/Kg
10/25/2212:49
11/03/2210:44
1
3.1
ug/Kg
10/25/2212:49
11/03/2210:44
1
4.4
ug/Kg
10/25/2212:49
11/03/2210:44
1
2.4
ug/Kg
10/25/2212:49
11/03/2210:44
1
8.8
ug/Kg
10/25/2212:49
11/03/2210:44
1
2.4
ug/Kg
10/25/2212:49
11/03/2210:44
1
2.2
ug/Kg
10/25/2212:49
11/03/2210:44
1
8.7
ug/Kg
10/25/2212:49
11/03/2210:44
1
2.4
ug/Kg
10/25/2212:49
11/03/2210:44
1
2.5
ug/Kg
10/25/2212:49
11/03/2210:44
1
2.1
ug/Kg
10/25/2212:49
11/03/2210:44
1
2.8
ug/Kg
10/25/2212:49
11/03/2210:44
1
2.8
ug/Kg
10/25/2212:49
11/03/2210:44
1
2.5
ug/Kg
10/25/2212:49
11/03/2210:44
1
2.8
ug/Kg
10/25/2212:49
11/03/2210:44
1
1.9
ug/Kg
10/25/2212:49
11/03/2210:44
1
Eurofins Savannah
Page 12 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Job ID: 680-223856-1
Project/Site: CF15067
Client Sample ID: SS-1
Lab Sample
ID: 680-223856-1
Date Collected: 10/20/22 10:20
Matrix: Solid
Date Received: 10/22/22 07:00
Percent Solids: 95.6
Method: SW846 8260D - Volatile
Organic Compounds by GC/MS (Continued)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
Trichlorofluoromethane
<3.4
5.4 3.4 ug/Kg
* 10/25/2212:49
11/03/2210:44 1
Vinyl chloride
<3.0
5.4 3.0 ug/Kg
* 10/25/22 12:49
11/03/22 10:44 1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr)
105
65- 130
10125122 12:49
11103122 10:44 1
4-Bromofluorobenzene (Surr)
95
65 - 130
10125122 12:49
11103122 10:44 1
Dibromofluoromethane (Surr)
104
65 - 130
10125122 12:49
11103122 10:44 1
Toluene-d8 (Surr)
99
65 - 130
10/25/22 12:49
11103122 10:44 1
Method: SW846 8270E SIM ID
- Semivolatile Organic Compounds (GC/MS SIM / Isotope
Dilution)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
1,4-Dioxane
<4.1
34 4.1 ug/Kg
* 10/31/2212:25
11/01/2217:16 1
Isotope Dilution
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,4-Dioxane-d8
37
10- 150
10131122 12:25
11101122 17:16 1
Method: SW846 9056A - Anions, Ion Chromatography - Soluble
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Sulfate
130
21
8.4
mg/Kg
#
11/02/2214:21
1
Method: SW846 6010D - Metals (ICP)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Silver
<0.32
1.0
0.32
mg/Kg
10/24/22 15:17
10/26/22 21:16
1
Arsenic
2.7
2.0
1.2
mg/Kg
10/24/22 15:17
10/26/22 21:16
1
Barium
52
1.0
0.41
mg/Kg
10/24/22 15:17
10/26/22 21:16
1
Cadmium
<0.10
0.50
0.10
mg/Kg
10/24/22 15:17
10/26/22 21:16
1
Lead
11
1.0
0.61
mg/Kg
10/24/22 15:17
10/26/22 21:16
1
Selenium
<1.1
2.5
1.1
mg/Kg
10/24/22 15:17
10/26/22 21:16
1
Antimony
<0.88
2.0
0.88
mg/Kg
10/24/22 15:17
10/26/22 21:16
1
Beryllium
0.41
0.40
0.071
mg/Kg
10/24/22 15:17
10/26/22 21:16
1
Thallium
<0.78
2.5
0.78
mg/Kg
10/24/22 15:17
10/26/22 21:16
1
Nickel
5.3
4.0
0.91
mg/Kg
10/24/22 15:17
10/26/22 21:16
1
Vanadium
25
1.0
0.16
mg/Kg
10/24/22 15:17
10/26/22 21:16
1
Copper
13
2.5
0.50
mg/Kg
10/24/22 15:17
10/26/22 21:16
1
Zinc
50
2.0
0.58
mg/Kg
10/24/22 15:17
10/26/22 21:16
1
Cobalt
3.3
1.0
0.33
mg/Kg
10/24/22 15:17
10/26/22 21:16
1
Method: SW846 7471 B - Mercury (CVAA)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Mercury
0.028
0.025
0.0079
mg/Kg
10/28/22 09:19
10/31/22 10:25
1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Phosphorus (EPA 365.4-1974)
550
F1
51
28
mg/Kg
*
10/27/22 17:30
10/28/22 14:10
5
Eurofins Savannah
Page 13 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: SS-2 Lab Sample ID: 680-223856-2
Date Collected: 10/20/22 10:25 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 76.6
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
Analyte
Result Qualifier
RL
1,1,1,2-Tetrachloroethane
<1.8
7.0
1,1,1-Trichloroethane
<3.6
7.0
1,1,2-Trichloroethane
<2.1
7.0
1,1-Dichloroethane
<4.1
7.0
1,1-Dichloroethene
<5.0
7.0
1,2,3-Trichlorobenzene
<2.8
7.0
1,2,4-Trichlorobenzene
<3.5
7.0
1,2-Dibromo-3-Chloropropane
<2.2
14
1,2-Dibromoethane
<2.4
7.0
1,2-Dichlorobenzene
<2.4
7.0
1,2-Dichloroethane
<3.2
7.0
1,2-Dichloropropane
<3.6
7.0
1,3-Dichlorobenzene
<2.8
7.0
1,4-Dichlorobenzene
<2.5
7.0
2-Butanone (MEK)
<13
35
2-Hexanone
<27
35
4-Methyl-2-pentanone (MIBK)
<25
35
Acetone
<15
70
Benzene
<3.4
7.0
Bromochloromethane
<2.8
7.0
Bromoform
<3.1
7.0
Bromomethane
<3.4
7.0
Carbon disulfide
<2.9 `+
7.0
Carbon tetrachloride
<2.9
7.0
Chlorobenzene
<2.0
7.0
Chloroethane
<3.1
7.0
Chloroform
<2.8
7.0
Chloromethane
<3.4
7.0
cis-1,2-Dichloroethene
<4.1
7.0
cis-1,3-Dichloropropene
<3.1
7.0
Cyclohexane
<3.2
7.0
Dichlorobromomethane
<2.8
7.0
Dichlorodifluoromethane
<4.5
7.0
Ethylbenzene
<2.9
7.0
Freon 113
<4.1
7.0
Hexachlorobutadiene
<5.7
7.0
Isopropylbenzene
<3.1
7.0
Methyl acetate
<11
35
Methyl tert-butyl ether
<3.1
7.0
Methylcyclohexane
<2.8 '+
7.0
Methylene Chloride
<11
14
m-Xylene & p-Xylene
<3.1
7.0
o-Xylene
<3.2
7.0
Styrene
<2.7
7.0
Tetrachloroethene
<3.6
7.0
Toluene
<3.6
7.0
trans- 1,2-Dichloroethene
<3.2
7.0
trans- 1,3-Dichloropropene
<3.6
7.0
Trichloroethene
<2.5
7.0
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1.8
ug/Kg
*
10/25/22 12:49
11/03/2211:08
1
3.6
ug/Kg
*
10/25/22 12:49
11/03/2211:08
1
2.1
ug/Kg
*
10/25/22 12:49
11/03/2211:08
1
4.1
ug/Kg
*
10/25/22 12:49
11 /03/22 11:08
1
5.0
ug/Kg
*
10/25/22 12:49
11 /03/22 11:08
1
2.8
ug/Kg
*
10/25/22 12:49
11 /03/22 11:08
1
3.5
ug/Kg
*
10/25/22 12:49
11 /03/22 11:08
1
2.2
ug/Kg
*
10/25/22 12:49
11 /03/22 11:08
1
2.4
ug/Kg
*
10/25/22 12:49
11 /03/22 11:08
1
2.4
ug/Kg
10/25/22 12:49
11 /03/22 11:08
1
3.2
ug/Kg
10/25/22 12:49
11 /03/22 11:08
1
3.6
ug/Kg
10/25/22 12:49
11 /03/22 11:08
1
2.8
ug/Kg
*
10/25/22 12:49
11/03/2211:08
1
2.5
ug/Kg
*
10/25/22 12:49
11/03/2211:08
1
13
ug/Kg
*
10/25/22 12:49
11/03/2211:08
1
27
ug/Kg
*
10/25/22 12:49
11 /03/22 11:08
1
25
ug/Kg
*
10/25/22 12:49
11 /03/22 11:08
1
15
ug/Kg
*
10/25/22 12:49
11 /03/22 11:08
1
3.4
ug/Kg
10/25/22 12:49
11 /03/22 11:08
1
2.8
ug/Kg
10/25/22 12:49
11 /03/22 11:08
1
3.1
ug/Kg
10/25/22 12:49
11 /03/22 11:08
1
3.4
ug/Kg
*
10/25/22 12:49
11 /03/22 11:08
1
2.9
ug/Kg
*
10/25/22 12:49
11 /03/22 11:08
1
2.9
ug/Kg
*
10/25/22 12:49
11 /03/22 11:08
1
2.0
ug/Kg
*
10/25/22 12:49
11 /03/22 11:08
1
3.1
ug/Kg
10/25/22 12:49
11 /03/22 11:08
1
2.8
ug/Kg
10/25/22 12:49
11 /03/22 11:08
1
3.4
ug/Kg
*
10/25/22 12:49
11/03/2211:08
1
4.1
ug/Kg
*
10/25/22 12:49
11/03/2211:08
1
3.1
ug/Kg
*
10/25/22 12:49
11/03/2211:08
1
3.2
ug/Kg
*
10/25/22 12:49
11 /03/22 11:08
1
2.8
ug/Kg
*
10/25/22 12:49
11 /03/22 11:08
1
4.5
ug/Kg
*
10/25/22 12:49
11 /03/22 11:08
1
2.9
ug/Kg
10/25/22 12:49
11 /03/22 11:08
1
4.1
ug/Kg
10/25/22 12:49
11 /03/22 11:08
1
5.7
ug/Kg
10/25/22 12:49
11 /03/22 11:08
1
3.1
ug/Kg
10/25/22 12:49
11 /03/22 11:08
1
11
ug/Kg
10/25/22 12:49
11 /03/22 11:08
1
3.1
ug/Kg
10/25/22 12:49
11 /03/22 11:08
1
2.8
ug/Kg
10/25/22 12:49
11/03/2211:08
1
11
ug/Kg
10/25/22 12:49
11/03/2211:08
1
3.1
ug/Kg
10/25/22 12:49
11/03/2211:08
1
3.2
ug/Kg
10/25/22 12:49
11/03/2211:08
1
2.7
ug/Kg
10/25/22 12:49
11/03/2211:08
1
3.6
ug/Kg
10/25/22 12:49
11/03/2211:08
1
3.6
ug/Kg
10/25/22 12:49
11 /03/22 11:08
1
3.2
ug/Kg
10/25/22 12:49
11 /03/22 11:08
1
3.6
ug/Kg
10/25/22 12:49
11 /03/22 11:08
1
2.5
ug/Kg
10/25/22 12:49
11 /03/22 11:08
1
Eurofins Savannah
Page 14 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Job ID: 680-223856-1
Project/Site: CF15067
Client Sample ID: SS-2
Lab Sample
ID: 680-223856-2
Date Collected: 10/20/22 10:25
Matrix: Solid
Date Received: 10/22/22 07:00
Percent Solids: 76.6
Method: SW846 8260D - Volatile
Organic Compounds by GC/MS (Continued)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
Trichlorofluoromethane
<4.3
7.0 4.3 ug/Kg
* 10/25/2212:49
11/03/2211:08 1
Vinyl chloride
<3.9
7.0 3.9 ug/Kg
* 10/25/22 12:49
11/03/22 11:08 1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr)
103
65- 130
10125122 12:49
11103122 11:08 1
4-Bromofluorobenzene (Surr)
97
65- 130
10125122 12:49
11103122 11:08 1
Dibromofluoromethane (Surr)
103
65 - 130
10125122 12:49
11103122 11:08 1
Toluene-d8 (Surr)
100
65 - 130
10/25/22 12:49
11103122 11:08 1
Method: SW846 8270E SIM ID
- Semivolatile Organic Compounds (GC/MS SIM / Isotope
Dilution)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
1,4-Dioxane
<5.1
42 5.1 ug/Kg
* 10/31/2212:25
11/01/2217:38 1
Isotope Dilution
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,4-Dioxane-d8
49
10- 150
10131122 12:25
11101122 17:38 1
Method: SW846 9056A - Anions, Ion Chromatography - Soluble
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Sulfate
120
26
10
mg/Kg
#
11/02/2215:00
1
Method: SW846 6010D - Metals (ICP)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Silver
<0.34
1.1
0.34
mg/Kg
10/24/22 15:17
10/26/22 21:19
1
Arsenic
3.7
2.1
1.3
mg/Kg
10/24/22 15:17
10/26/22 21:19
1
Barium
83
1.1
0.44
mg/Kg
10/24/22 15:17
10/26/22 21:19
1
Cadmium
<0.11
0.54
0.11
mg/Kg
10/24/22 15:17
10/26/22 21:19
1
Lead
17
1.1
0.65
mg/Kg
10/24/22 15:17
10/26/22 21:19
1
Selenium
<1.2
2.7
1.2
mg/Kg
10/24/22 15:17
10/26/22 21:19
1
Antimony
<0.93
2.1
0.93
mg/Kg
10/24/22 15:17
10/26/22 21:19
1
Beryllium
0.70
0.43
0.076
mg/Kg
10/24/22 15:17
10/26/22 21:19
1
Thallium
<0.83
2.7
0.83
mg/Kg
10/24/22 15:17
10/26/22 21:19
1
Nickel
5.8
4.3
0.96
mg/Kg
10/24/22 15:17
10/26/22 21:19
1
Vanadium
33
1.1
0.17
mg/Kg
10/24/22 15:17
10/26/22 21:19
1
Copper
16
2.7
0.54
mg/Kg
10/24/22 15:17
10/26/22 21:19
1
Zinc
53
2.1
0.62
mg/Kg
10/24/22 15:17
10/26/22 21:19
1
Cobalt
4.0
1.1
0.35
mg/Kg
10/24/22 15:17
10/26/22 21:19
1
Method: SW846 7471 B - Mercury (CVAA)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Mercury
0.036
0.030
0.0095
mg/Kg
10/28/22 09:19
10/31/22 10:28
1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Phosphorus (EPA 365.4-1974)
260
13
7.0
mg/Kg
*
10/27/22 17:30
10/28/22 12:44
1
Eurofins Savannah
Page 15 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: SS-3 Lab Sample ID: 680-223856-3
Date Collected: 10/20/22 10:30 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 97.5
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
Analyte
Result Qualifier
RL
1,1,1,2-Tetrachloroethane
<1.5
5.9
1,1,1-Trichloroethane
<3.1
5.9
1,1,2-Trichloroethane
<1.8
5.9
1,1-Dichloroethane
<3.4
5.9
1,1-Dichloroethene
<4.2
5.9
1,2,3-Trichlorobenzene
<2.3
5.9
1,2,4-Trichlorobenzene
<2.9
5.9
1,2-Dibromo-3-Chloropropane
<1.9
12
1,2-Dibromoethane
<2.0
5.9
1,2-Dichlorobenzene
<2.0
5.9
1,2-Dichloroethane
<2.7
5.9
1,2-Dichloropropane
<3.1
5.9
1,3-Dichlorobenzene
<2.3
5.9
1,4-Dichlorobenzene
<2.1
5.9
2-Butanone (MEK)
<11
29
2-Hexanone
<22
29
4-Methyl-2-pentanone (MIBK)
<21
29
Acetone
<13
59
Benzene
<2.8
5.9
Bromochloromethane
<2.3
5.9
Bromoform
<2.6
5.9
Bromomethane
<2.8
5.9
Carbon disulfide
<2.5 `+
5.9
Carbon tetrachloride
<2.5
5.9
Chlorobenzene
<1.6
5.9
Chloroethane
<2.6
5.9
Chloroform
<2.3
5.9
Chloromethane
<2.8
5.9
cis-1,2-Dichloroethene
<3.4
5.9
cis-1,3-Dichloropropene
<2.6
5.9
Cyclohexane
<2.7
5.9
Dichlorobromomethane
<2.3
5.9
Dichlorodifluoromethane
<3.8
5.9
Ethylbenzene
<2.5
5.9
Freon 113
<3.4
5.9
Hexachlorobutadiene
<4.8
5.9
Isopropylbenzene
<2.6
5.9
Methyl acetate
<9.5
29
Methyl tert-butyl ether
<2.6
5.9
Methylcyclohexane
<2.3 '+
5.9
Methylene Chloride
<9.4
12
m-Xylene & p-Xylene
<2.6
5.9
o-Xylene
<2.7
5.9
Styrene
<2.2
5.9
Tetrachloroethene
<3.1
5.9
Toluene
<3.1
5.9
trans- 1,2-Dichloroethene
<2.7
5.9
trans- 1,3-Dichloropropene
<3.1
5.9
Trichloroethene
<2.1
5.9
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1.5
ug/Kg
*
10/25/22 12:49
11/03/2211:32
1
3.1
ug/Kg
*
10/25/22 12:49
11/03/2211:32
1
1.8
ug/Kg
*
10/25/22 12:49
11/03/2211:32
1
3.4
ug/Kg
*
10/25/22 12:49
11 /03/22 11:32
1
4.2
ug/Kg
*
10/25/22 12:49
11 /03/22 11:32
1
2.3
ug/Kg
*
10/25/22 12:49
11 /03/22 11:32
1
2.9
ug/Kg
*
10/25/22 12:49
11 /03/22 11:32
1
1.9
ug/Kg
*
10/25/22 12:49
11 /03/22 11:32
1
2.0
ug/Kg
*
10/25/22 12:49
11 /03/22 11:32
1
2.0
ug/Kg
10/25/22 12:49
11 /03/22 11:32
1
2.7
ug/Kg
10/25/22 12:49
11 /03/22 11:32
1
3.1
ug/Kg
10/25/22 12:49
11 /03/22 11:32
1
2.3
ug/Kg
*
10/25/22 12:49
11/03/2211:32
1
2.1
ug/Kg
*
10/25/22 12:49
11/03/2211:32
1
11
ug/Kg
*
10/25/22 12:49
11/03/2211:32
1
22
ug/Kg
*
10/25/22 12:49
11 /03/22 11:32
1
21
ug/Kg
*
10/25/22 12:49
11 /03/22 11:32
1
13
ug/Kg
*
10/25/22 12:49
11 /03/22 11:32
1
2.8
ug/Kg
10/25/22 12:49
11 /03/22 11:32
1
2.3
ug/Kg
10/25/22 12:49
11 /03/22 11:32
1
2.6
ug/Kg
10/25/22 12:49
11 /03/22 11:32
1
2.8
ug/Kg
*
10/25/22 12:49
11 /03/22 11:32
1
2.5
ug/Kg
*
10/25/22 12:49
11 /03/22 11:32
1
2.5
ug/Kg
*
10/25/22 12:49
11 /03/22 11:32
1
1.6
ug/Kg
*
10/25/22 12:49
11 /03/22 11:32
1
2.6
ug/Kg
10/25/22 12:49
11 /03/22 11:32
1
2.3
ug/Kg
10/25/22 12:49
11 /03/22 11:32
1
2.8
ug/Kg
*
10/25/22 12:49
11/03/2211:32
1
3.4
ug/Kg
*
10/25/22 12:49
11/03/2211:32
1
2.6
ug/Kg
*
10/25/22 12:49
11/03/2211:32
1
2.7
ug/Kg
*
10/25/22 12:49
11 /03/22 11:32
1
2.3
ug/Kg
*
10/25/22 12:49
11 /03/22 11:32
1
3.8
ug/Kg
*
10/25/22 12:49
11 /03/22 11:32
1
2.5
ug/Kg
10/25/22 12:49
11 /03/22 11:32
1
3.4
ug/Kg
10/25/22 12:49
11 /03/22 11:32
1
4.8
ug/Kg
10/25/22 12:49
11 /03/22 11:32
1
2.6
ug/Kg
10/25/22 12:49
11 /03/22 11:32
1
9.5
ug/Kg
10/25/22 12:49
11 /03/22 11:32
1
2.6
ug/Kg
10/25/22 12:49
11 /03/22 11:32
1
2.3
ug/Kg
10/25/22 12:49
11/03/2211:32
1
9.4
ug/Kg
10/25/22 12:49
11/03/2211:32
1
2.6
ug/Kg
10/25/22 12:49
11/03/2211:32
1
2.7
ug/Kg
10/25/22 12:49
11/03/2211:32
1
2.2
ug/Kg
10/25/22 12:49
11/03/2211:32
1
3.1
ug/Kg
10/25/22 12:49
11/03/2211:32
1
3.1
ug/Kg
10/25/22 12:49
11 /03/22 11:32
1
2.7
ug/Kg
10/25/22 12:49
11 /03/22 11:32
1
3.1
ug/Kg
10/25/22 12:49
11 /03/22 11:32
1
2.1
ug/Kg
10/25/22 12:49
11 /03/22 11:32
1
Eurofins Savannah
Page 16 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Job ID: 680-223856-1
Project/Site: CF15067
Client Sample ID: SS-3
Lab Sample
ID: 680-223856-3
Date Collected: 10/20/22 10:30
Matrix: Solid
Date Received: 10/22/22 07:00
Percent Solids: 97.5
Method: SW846 8260D - Volatile
Organic Compounds by GC/MS (Continued)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
Trichlorofluoromethane
<3.6
5.9 3.6 ug/Kg
* 10/25/22 12:49
11/03/2211:32 1
Vinyl chloride
<3.3
5.9 3.3 ug/Kg
* 10/25/22 12:49
11/03/22 11:32 1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr)
105
65- 130
10125122 12:49
11103122 11:32 1
4-Bromofluorobenzene (Surr)
97
65- 130
10125122 12:49
11103122 11:32 1
Dibromofluoromethane (Surr)
104
65 - 130
10125122 12:49
11103122 11:32 1
Toluene-d8 (Surr)
99
65 - 130
10/25/22 12:49
11103122 11:32 1
Method: SW846 8270E SIM ID
- Semivolatile Organic Compounds (GC/MS SIM / Isotope
Dilution)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
1,4-Dioxane
<4.0
33 4.0 ug/Kg
* 10/31/2212:25
11/01/2218:00 1
Isotope Dilution
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,4-Dioxane-d8
45
10- 150
10131122 12:25
11101122 18:00 1
Method: SW846 9056A - Anions, Ion Chromatography - Soluble
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Sulfate
150
20
8.2
mg/Kg
#
11/02/2215:13
1
Method: SW846 6010D - Metals (ICP)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Silver
<0.33
1.0
0.33
mg/Kg
10/25/22 08:20
10/27/22 22:05
1
Arsenic
2.8
2.1
1.2
mg/Kg
10/25/22 08:20
10/27/22 22:05
1
Barium
40
F2
1.0
0.42
mg/Kg
10/25/22 08:20
10/27/22 22:05
1
Cadmium
0.35
J
0.51
0.10
mg/Kg
10/25/22 08:20
10/27/22 22:05
1
Lead
25
F1
1.0
0.63
mg/Kg
10/25/22 08:20
10/27/22 22:05
1
Selenium
<1.1
F1
2.6
1.1
mg/Kg
10/25/22 08:20
10/27/22 22:05
1
Antimony
<0.89
F1
2.1
0.89
mg/Kg
10/25/22 08:20
10/27/22 22:05
1
Beryllium
0.62
0.41
0.073
mg/Kg
10/25/22 08:20
10/27/22 22:05
1
Thallium
<0.80
2.6
0.80
mg/Kg
10/25/22 08:20
10/27/22 22:05
1
Nickel
5.7
4.1
0.92
mg/Kg
10/25/22 08:20
10/27/22 22:05
1
Vanadium
46
1.0
0.16
mg/Kg
10/25/22 08:20
10/27/22 22:05
1
Copper
15
2.6
0.51
mg/Kg
10/25/22 08:20
10/27/22 22:05
1
Zinc
42
2.1
0.59
mg/Kg
10/25/22 08:20
10/27/22 22:05
1
Cobalt
4.0
1.0
0.34
mg/Kg
10/25/22 08:20
10/27/22 22:05
1
Method: SW846 7471 B - Mercury (CVAA)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Mercury
0.048
0.025
0.0080
mg/Kg
10/28/22 09:19
10/31/22 10:32
1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Phosphorus (EPA 365.4-1974)
230
10
5.6
mg/Kg
*
10/27/22 17:30
10/28/22 12:42
1
Eurofins Savannah
Page 17 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: SS-4 Lab Sample ID: 680-223856-4
Date Collected: 10/20/22 10:35 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 95.7
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
Analyte
Result Qualifier
RL
1,1,1,2-Tetrachloroethane
<2.1
8.0
1,1,1-Trichloroethane
<4.2
8.0
1,1,2-Trichloroethane
<2.4
8.0
1,1-Dichloroethane
<4.7
8.0
1,1-Dichloroethene
<5.8
8.0
1,2,3-Trichlorobenzene
<3.2
8.0
1,2,4-Trichlorobenzene
<4.0
8.0
1,2-Dibromo-3-Chloropropane
<2.6
16
1,2-Dibromoethane
<2.7
8.0
1,2-Dichlorobenzene
<2.7
8.0
1,2-Dichloroethane
<3.7
8.0
1,2-Dichloropropane
<4.2
8.0
1,3-Dichlorobenzene
<3.2
8.0
1,4-Dichlorobenzene
<2.9
8.0
2-Butanone (MEK)
<15
40
2-Hexanone
<31
40
4-Methyl-2-pentanone (MIBK)
<29
40
Acetone
<18
80
Benzene
<3.9
8.0
Bromochloromethane
<3.2
8.0
Bromoform
<3.5
8.0
Bromomethane
<3.9
8.0
Carbon disulfide
<3.4 `+
8.0
Carbon tetrachloride
<3.4
8.0
Chlorobenzene
<2.2
8.0
Chloroethane
<3.5
8.0
Chloroform
<3.2
8.0
Chloromethane
<3.9
8.0
cis-1,2-Dichloroethene
<4.7
8.0
cis-1,3-Dichloropropene
<3.5
8.0
Cyclohexane
<3.7
8.0
Dichlorobromomethane
<3.2
8.0
Dichlorodifluoromethane
<5.1
8.0
Ethylbenzene
<3.4
8.0
Freon 113
<4.7
8.0
Hexachlorobutadiene
<6.6
8.0
Isopropylbenzene
<3.5
8.0
Methyl acetate
<13
40
Methyl tert-butyl ether
<3.5
8.0
Methylcyclohexane
<3.2 *+
8.0
Methylene Chloride
<13
16
m-Xylene & p-Xylene
<3.5
8.0
o-Xylene
<3.7
8.0
Styrene
<3.1
8.0
Tetrachloroethene
<4.2
8.0
Toluene
<4.2
8.0
trans- 1,2-Dichloroethene
<3.7
8.0
trans- 1,3-Dichloropropene
<4.2
8.0
Trichloroethene
<2.9
8.0
MDL
Unit
D
Prepared
Analyzed
Dil Fac
2.1
ug/Kg
*
10/25/22 12:49
11/03/2211:55
1
4.2
ug/Kg
*
10/25/22 12:49
11/03/2211:55
1
2.4
ug/Kg
*
10/25/22 12:49
11/03/2211:55
1
4.7
ug/Kg
*
10/25/22 12:49
11 /03/22 11:55
1
5.8
ug/Kg
*
10/25/22 12:49
11 /03/22 11:55
1
3.2
ug/Kg
*
10/25/22 12:49
11 /03/22 11:55
1
4.0
ug/Kg
*
10/25/22 12:49
11 /03/22 11:55
1
2.6
ug/Kg
*
10/25/22 12:49
11 /03/22 11:55
1
2.7
ug/Kg
*
10/25/22 12:49
11 /03/22 11:55
1
2.7
ug/Kg
10/25/22 12:49
11 /03/22 11:55
1
3.7
ug/Kg
10/25/22 12:49
11 /03/22 11:55
1
4.2
ug/Kg
10/25/22 12:49
11 /03/22 11:55
1
3.2
ug/Kg
*
10/25/22 12:49
11/03/2211:55
1
2.9
ug/Kg
*
10/25/22 12:49
11/03/2211:55
1
15
ug/Kg
*
10/25/22 12:49
11/03/2211:55
1
31
ug/Kg
*
10/25/22 12:49
11 /03/22 11:55
1
29
ug/Kg
*
10/25/22 12:49
11 /03/22 11:55
1
18
ug/Kg
*
10/25/22 12:49
11 /03/22 11:55
1
3.9
ug/Kg
10/25/22 12:49
11 /03/22 11:55
1
3.2
ug/Kg
10/25/22 12:49
11 /03/22 11:55
1
3.5
ug/Kg
10/25/22 12:49
11 /03/22 11:55
1
3.9
ug/Kg
*
10/25/22 12:49
11 /03/22 11:55
1
3.4
ug/Kg
*
10/25/22 12:49
11 /03/22 11:55
1
3.4
ug/Kg
*
10/25/22 12:49
11 /03/22 11:55
1
2.2
ug/Kg
*
10/25/22 12:49
11 /03/22 11:55
1
3.5
ug/Kg
10/25/22 12:49
11 /03/22 11:55
1
3.2
ug/Kg
10/25/22 12:49
11 /03/22 11:55
1
3.9
ug/Kg
*
10/25/22 12:49
11/03/2211:55
1
4.7
ug/Kg
*
10/25/22 12:49
11/03/2211:55
1
3.5
ug/Kg
*
10/25/22 12:49
11/03/2211:55
1
3.7
ug/Kg
*
10/25/22 12:49
11 /03/22 11:55
1
3.2
ug/Kg
*
10/25/22 12:49
11 /03/22 11:55
1
5.1
ug/Kg
*
10/25/22 12:49
11 /03/22 11:55
1
3.4
ug/Kg
10/25/22 12:49
11 /03/22 11:55
1
4.7
ug/Kg
10/25/22 12:49
11 /03/22 11:55
1
6.6
ug/Kg
10/25/22 12:49
11 /03/22 11:55
1
3.5
ug/Kg
10/25/22 12:49
11 /03/22 11:55
1
13
ug/Kg
10/25/22 12:49
11 /03/22 11:55
1
3.5
ug/Kg
10/25/22 12:49
11 /03/22 11:55
1
3.2
ug/Kg
10/25/22 12:49
11/03/2211:55
1
13
ug/Kg
10/25/22 12:49
11/03/2211:55
1
3.5
ug/Kg
10/25/22 12:49
11/03/2211:55
1
3.7
ug/Kg
10/25/22 12:49
11/03/2211:55
1
3.1
ug/Kg
10/25/22 12:49
11/03/2211:55
1
4.2
ug/Kg
10/25/22 12:49
11/03/2211:55
1
4.2
ug/Kg
10/25/22 12:49
11 /03/22 11:55
1
3.7
ug/Kg
10/25/22 12:49
11 /03/22 11:55
1
4.2
ug/Kg
10/25/22 12:49
11 /03/22 11:55
1
2.9
ug/Kg
10/25/22 12:49
11 /03/22 11:55
1
Eurofins Savannah
Page 18 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Job ID: 680-223856-1
Project/Site: CF15067
Client Sample ID: SS-4
Lab Sample
ID: 680-223856-4
Date Collected: 10/20/22 10:35
Matrix: Solid
Date Received: 10/22/22 07:00
Percent Solids: 95.7
Method: SW846 8260D - Volatile
Organic Compounds by GC/MS (Continued)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
Trichlorofluoromethane
<5.0
8.0 5.0 ug/Kg
* 10/25/22 12:49
11/03/2211:55 1
Vinyl chloride
<4.5
8.0 4.5 ug/Kg
* 10/25/22 12:49
11/03/22 11:55 1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr)
105
65- 130
10125122 12:49
11103122 11:55 1
4-Bromofluorobenzene (Surr)
99
65 - 130
10125122 12:49
11103122 11:55 1
Dibromofluoromethane (Surr)
103
65 - 130
10125122 12:49
11103122 11:55 1
Toluene-d8 (Surr)
100
65 - 130
10/25/22 12:49
11103122 11:55 1
Method: SW846 8270E SIM ID
- Semivolatile Organic Compounds (GC/MS SIM / Isotope
Dilution)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
1,4-Dioxane
<4.1
34 4.1 ug/Kg
* 10/31/2212:25
11/01/2218:22 1
Isotope Dilution
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,4-Dioxane-d8
45
10- 150
10131122 12:25
11101122 18:22 1
Method: SW846 9056A - Anions, Ion Chromatography - Soluble
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Sulfate
150
21
8.3
mg/Kg
#
11/02/2215:27
1
Method: SW846 6010D - Metals (ICP)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Silver
<0.33
1.0
0.33
mg/Kg
10/25/22 08:20
10/27/22 22:20
1
Arsenic
2.4
2.1
1.3
mg/Kg
10/25/22 08:20
10/27/22 22:20
1
Barium
55
1.0
0.43
mg/Kg
10/25/22 08:20
10/27/22 22:20
1
Cadmium
0.52
0.52
0.10
mg/Kg
10/25/22 08:20
10/27/22 22:20
1
Lead
15
1.0
0.64
mg/Kg
10/25/22 08:20
10/27/22 22:20
1
Selenium
<1.1
2.6
1.1
mg/Kg
10/25/22 08:20
10/27/22 22:20
1
Antimony
<0.91
2.1
0.91
mg/Kg
10/25/22 08:20
10/27/22 22:20
1
Beryllium
0.70
0.42
0.074
mg/Kg
10/25/22 08:20
10/27/22 22:20
1
Thallium
<0.81
2.6
0.81
mg/Kg
10/25/22 08:20
10/27/22 22:20
1
Nickel
11
4.2
0.94
mg/Kg
10/25/22 08:20
10/27/22 22:20
1
Vanadium
65
1.0
0.17
mg/Kg
10/25/22 08:20
10/27/22 22:20
1
Copper
25
2.6
0.52
mg/Kg
10/25/22 08:20
10/27/22 22:20
1
Zinc
55
2.1
0.61
mg/Kg
10/25/22 08:20
10/27/22 22:20
1
Cobalt
8.1
1.0
0.34
mg/Kg
10/25/22 08:20
10/27/22 22:20
1
Method: SW846 7471 B - Mercury (CVAA)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Mercury
0.057
0.025
0.0079
mg/Kg
10/28/22 09:19
10/31/22 10:35
1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Phosphorus (EPA 365.4-1974)
180
10
5.6
mg/Kg
*
10/27/22 17:30
10/28/22 12:49
1
Eurofins Savannah
Page 19 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: SS-5 Lab Sample ID: 680-223856-5
Date Collected: 10/20/22 10:40 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 90.5
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
Analyte
Result Qualifier
RL
1,1,1,2-Tetrachloroethane
<1.3
5.2
1,1,1-Trichloroethane
<2.7
5.2
1,1,2-Trichloroethane
<1.6
5.2
1,1-Dichloroethane
<3.0
5.2
1,1-Dichloroethene
<3.7
5.2
1,2,3-Trichlorobenzene
<2.1
5.2
1,2,4-Trichlorobenzene
<2.6
5.2
1,2-Dibromo-3-Chloropropane
<1.7
10
1,2-Dibromoethane
<1.8
5.2
1,2-Dichlorobenzene
<1.8
5.2
1,2-Dichloroethane
<2.4
5.2
1,2-Dichloropropane
<2.7
5.2
1,3-Dichlorobenzene
<2.1
5.2
1,4-Dichlorobenzene
<1.9
5.2
2-Butanone (MEK)
<9.6
26
2-Hexanone
<20
26
4-Methyl-2-pentanone (MIBK)
<19
26
Acetone
<11
52
Benzene
<2.5
5.2
Bromochloromethane
<2.1
5.2
Bromoform
<2.3
5.2
Bromomethane
<2.5
5.2
Carbon disulfide
<2.2 `+
5.2
Carbon tetrachloride
<2.2
5.2
Chlorobenzene
<1.5
5.2
Chloroethane
<2.3
5.2
Chloroform
<2.1
5.2
Chloromethane
<2.5
5.2
cis-1,2-Dichloroethene
<3.0
5.2
cis-1,3-Dichloropropene
<2.3
5.2
Cyclohexane
<2.4
5.2
Dichlorobromomethane
<2.1
5.2
Dichlorodifluoromethane
<3.3
5.2
Ethylbenzene
<2.2
5.2
Freon 113
<3.0
5.2
Hexachlorobutadiene
<4.3
5.2
Isopropylbenzene
<2.3
5.2
Methyl acetate
<8.4
26
Methyl tert-butyl ether
<2.3
5.2
Methylcyclohexane
<2.1 *+
5.2
Methylene Chloride
<8.3
10
m-Xylene & p-Xylene
<2.3
5.2
o-Xylene
<2.4
5.2
Styrene
<2.0
5.2
Tetrachloroethene
<2.7
5.2
Toluene
<2.7
5.2
trans- 1,2-Dichloroethene
<2.4
5.2
trans- 1,3-Dichloropropene
<2.7
5.2
Trichloroethene
<1.9
5.2
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1.3
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
2.7
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
1.6
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
3.0
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
3.7
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
2.1
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
2.6
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
1.7
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
1.8
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
1.8
ug/Kg
10/25/2212:49
11/03/2212:19
1
2.4
ug/Kg
10/25/2212:49
11/03/2212:19
1
2.7
ug/Kg
10/25/2212:49
11/03/2212:19
1
2.1
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
1.9
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
9.6
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
20
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
19
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
11
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
2.5
ug/Kg
10/25/2212:49
11/03/2212:19
1
2.1
ug/Kg
10/25/2212:49
11/03/2212:19
1
2.3
ug/Kg
10/25/2212:49
11/03/2212:19
1
2.5
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
2.2
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
2.2
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
1.5
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
2.3
ug/Kg
10/25/2212:49
11/03/2212:19
1
2.1
ug/Kg
10/25/2212:49
11/03/2212:19
1
2.5
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
3.0
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
2.3
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
2.4
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
2.1
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
3.3
ug/Kg
*
10/25/2212:49
11/03/2212:19
1
2.2
ug/Kg
10/25/2212:49
11/03/2212:19
1
3.0
ug/Kg
10/25/2212:49
11/03/2212:19
1
4.3
ug/Kg
10/25/2212:49
11/03/2212:19
1
2.3
ug/Kg
10/25/2212:49
11/03/2212:19
1
8.4
ug/Kg
10/25/2212:49
11/03/2212:19
1
2.3
ug/Kg
10/25/2212:49
11/03/2212:19
1
2.1
ug/Kg
10/25/2212:49
11/03/2212:19
1
8.3
ug/Kg
10/25/2212:49
11/03/2212:19
1
2.3
ug/Kg
10/25/2212:49
11/03/2212:19
1
2.4
ug/Kg
10/25/2212:49
11/03/2212:19
1
2.0
ug/Kg
10/25/2212:49
11/03/2212:19
1
2.7
ug/Kg
10/25/2212:49
11/03/2212:19
1
2.7
ug/Kg
10/25/2212:49
11/03/2212:19
1
2.4
ug/Kg
10/25/2212:49
11/03/2212:19
1
2.7
ug/Kg
10/25/2212:49
11/03/2212:19
1
1.9
ug/Kg
10/25/2212:49
11/03/2212:19
1
Eurofins Savannah
Page 20 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Job ID: 680-223856-1
Project/Site: CF15067
Client Sample ID: SS-5
Lab Sample
ID: 680-223856-5
Date Collected: 10/20/22 10:40
Matrix: Solid
Date Received: 10/22/22 07:00
Percent Solids: 90.5
Method: SW846 8260D - Volatile
Organic Compounds by GC/MS (Continued)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
Trichlorofluoromethane
<3.2
5.2 3.2 ug/Kg
* 10/25/22 12:49
11/03/2212:19 1
Vinyl chloride
<2.9
5.2 2.9 ug/Kg
* 10/25/22 12:49
11/03/22 12:19 1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr)
106
65- 130
10125122 12:49
11103122 12:19 1
4-Bromofluorobenzene (Surr)
99
65 - 130
10125122 12:49
11103122 12:19 1
Dibromofluoromethane (Surr)
103
65 - 130
10125122 12:49
11103122 12:19 1
Toluene-d8 (Surr)
101
65 - 130
10/25/22 12:49
11103122 12:19 1
Method: SW846 8270E SIM ID
- Semivolatile Organic Compounds (GC/MS SIM / Isotope
Dilution)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
1,4-Dioxane
<4.2
34 4.2 ug/Kg
* 10/31/2212:25
11/01/2218:44 1
Isotope Dilution
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,4-Dioxane-d8
52
10- 150
10131122 12:25
11101122 18:44 1
Method: SW846 9056A - Anions, Ion Chromatography - Soluble
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Sulfate
110
22
8.8
mg/Kg
#
11/02/2215:40
1
Method: SW846 6010D - Metals (ICP)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Silver
<0.34
1.1
0.34
mg/Kg
10/25/22 08:20
10/27/22 14:28
1
Arsenic
1.8
J
2.1
1.3
mg/Kg
10/25/22 08:20
10/27/22 14:28
1
Barium
46
1.1
0.44
mg/Kg
10/25/22 08:20
10/27/22 14:28
1
Cadmium
0.12
J
0.53
0.11
mg/Kg
10/25/22 08:20
10/27/22 14:28
1
Lead
6.6
1.1
0.65
mg/Kg
10/25/22 08:20
10/27/22 14:28
1
Selenium
<1.2
2.7
1.2
mg/Kg
10/25/22 08:20
10/27/22 14:28
1
Antimony
<0.92
2.1
0.92
mg/Kg
10/25/22 08:20
10/27/22 14:28
1
Beryllium
0.33
J
0.42
0.075
mg/Kg
10/25/22 08:20
10/27/22 14:28
1
Thallium
<0.83
2.7
0.83
mg/Kg
10/25/22 08:20
10/27/22 14:28
1
Nickel
3.7
J
4.2
0.96
mg/Kg
10/25/22 08:20
10/27/22 14:28
1
Vanadium
21
1.1
0.17
mg/Kg
10/25/22 08:20
10/27/22 14:28
1
Copper
18
2.7
0.53
mg/Kg
10/25/22 08:20
10/27/22 14:28
1
Zinc
51
2.1
0.62
mg/Kg
10/25/22 08:20
10/27/22 14:28
1
Cobalt
3.3
1.1
0.35
mg/Kg
10/25/22 08:20
10/27/22 14:28
1
Method: SW846 7471 B - Mercury (CVAA)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Mercury
0.26
0.027
0.0085
mg/Kg
10/28/22 09:19
10/31/22 10:39
1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Phosphorus (EPA 365.4-1974)
320
11
6.0
mg/Kg
*
10/27/22 17:30
10/28/22 12:46
1
Eurofins Savannah
Page 21 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: SS-6 Lab Sample ID: 680-223856-6
Date Collected: 10/20/22 10:45 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 90.2
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
Analyte
Result Qualifier
RL
1,1,1,2-Tetrachloroethane
<1.4
5.5
1,1,1-Trichloroethane
<2.9
5.5
1,1,2-Trichloroethane
<1.7
5.5
1,1-Dichloroethane
<3.2
5.5
1,1-Dichloroethene
<4.0
5.5
1,2,3-Trichlorobenzene
<2.2
5.5
1,2,4-Trichlorobenzene
<2.8
5.5
1,2-Dibromo-3-Chloropropane
<1.8
11
1,2-Dibromoethane
<1.9
5.5
1,2-Dichlorobenzene
<1.9
5.5
1,2-Dichloroethane
<2.5
5.5
1,2-Dichloropropane
<2.9
5.5
1,3-Dichlorobenzene
<2.2
5.5
1,4-Dichlorobenzene
<2.0
5.5
2-Butanone (MEK)
<10
28
2-Hexanone
<21
28
4-Methyl-2-pentanone (MIBK)
<20
28
Acetone
<12
55
Benzene
<2.7
5.5
Bromochloromethane
<2.2
5.5
Bromoform
<2.4
5.5
Bromomethane
<2.7
5.5
Carbon disulfide
<2.3 `+
5.5
Carbon tetrachloride
<2.3
5.5
Chlorobenzene
<1.5
5.5
Chloroethane
<2.4
5.5
Chloroform
<2.2
5.5
Chloromethane
<2.7
5.5
cis-1,2-Dichloroethene
<3.2
5.5
cis-1,3-Dichloropropene
<2.4
5.5
Cyclohexane
<2.5
5.5
Dichlorobromomethane
<2.2
5.5
Dichlorodifluoromethane
<3.5
5.5
Ethylbenzene
<2.3
5.5
Freon 113
<3.2
5.5
Hexachlorobutadiene
<4.5
5.5
Isopropylbenzene
<2.4
5.5
Methyl acetate
<9.0
28
Methyl tert-butyl ether
<2.4
5.5
Methylcyclohexane
<2.2 '+
5.5
Methylene Chloride
<8.8
11
m-Xylene & p-Xylene
<2.4
5.5
o-Xylene
<2.5
5.5
Styrene
<2.1
5.5
Tetrachloroethene
<2.9
5.5
Toluene
<2.9
5.5
trans- 1,2-Dichloroethene
<2.5
5.5
trans- 1,3-Dichloropropene
<2.9
5.5
Trichloroethene
<2.0
5.5
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1.4
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
2.9
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
1.7
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
3.2
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
4.0
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
2.2
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
2.8
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
1.8
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
1.9
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
1.9
ug/Kg
10/25/2212:49
11/03/2212:43
1
2.5
ug/Kg
10/25/2212:49
11/03/2212:43
1
2.9
ug/Kg
10/25/2212:49
11/03/2212:43
1
2.2
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
2.0
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
10
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
21
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
20
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
12
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
2.7
ug/Kg
10/25/2212:49
11/03/2212:43
1
2.2
ug/Kg
10/25/2212:49
11/03/2212:43
1
2.4
ug/Kg
10/25/2212:49
11/03/2212:43
1
2.7
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
2.3
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
2.3
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
1.5
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
2.4
ug/Kg
10/25/2212:49
11/03/2212:43
1
2.2
ug/Kg
10/25/2212:49
11/03/2212:43
1
2.7
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
3.2
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
2.4
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
2.5
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
2.2
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
3.5
ug/Kg
*
10/25/2212:49
11/03/2212:43
1
2.3
ug/Kg
10/25/2212:49
11/03/2212:43
1
3.2
ug/Kg
10/25/2212:49
11/03/2212:43
1
4.5
ug/Kg
10/25/2212:49
11/03/2212:43
1
2.4
ug/Kg
10/25/2212:49
11/03/2212:43
1
9.0
ug/Kg
10/25/2212:49
11/03/2212:43
1
2.4
ug/Kg
10/25/2212:49
11/03/2212:43
1
2.2
ug/Kg
10/25/2212:49
11/03/2212:43
1
8.8
ug/Kg
10/25/2212:49
11/03/2212:43
1
2.4
ug/Kg
10/25/2212:49
11/03/2212:43
1
2.5
ug/Kg
10/25/2212:49
11/03/2212:43
1
2.1
ug/Kg
10/25/2212:49
11/03/2212:43
1
2.9
ug/Kg
10/25/2212:49
11/03/2212:43
1
2.9
ug/Kg
10/25/2212:49
11/03/2212:43
1
2.5
ug/Kg
10/25/2212:49
11/03/2212:43
1
2.9
ug/Kg
10/25/2212:49
11/03/2212:43
1
2.0
ug/Kg
10/25/2212:49
11/03/2212:43
1
Eurofins Savannah
Page 22 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Job ID: 680-223856-1
Project/Site: CF15067
Client Sample ID: SS-6
Lab Sample
ID: 680-223856-6
Date Collected: 10/20/22 10:45
Matrix: Solid
Date Received: 10/22/22 07:00
Percent Solids: 90.2
Method: SW846 8260D - Volatile
Organic Compounds by GC/MS (Continued)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
Trichlorofluoromethane
<3.4
5.5 3.4 ug/Kg
* 10/25/22 12:49
11/03/2212:43 1
Vinyl chloride
<3.1
5.5 3.1 ug/Kg
* 10/25/22 12:49
11/03/22 12:43 1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr)
106
65- 130
10125122 12:49
11103122 12:43 1
4-Bromofluorobenzene (Surr)
98
65 - 130
10125122 12:49
11103122 12:43 1
Dibromofluoromethane (Surr)
105
65 - 130
10125122 12:49
11103122 12:43 1
Toluene-d8 (Surr)
102
65 - 130
10/25/22 12:49
11103122 12:43 1
Method: SW846 8270E SIM ID
- Semivolatile Organic Compounds (GC/MS SIM / Isotope
Dilution)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
1,4-Dioxane
<4.4
36 4.4 ug/Kg
* 10/31/2212:25
11/01/2219:06 1
Isotope Dilution
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,4-Dioxane-d8
60
10- 150
10131122 12:25
11101122 19:06 1
Method: SW846 9056A - Anions, Ion Chromatography - Soluble
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Sulfate
45
22
8.8
mg/Kg
#
11/02/2215:53
1
Method: SW846 6010D - Metals (ICP)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Silver
<0.31
0.97
0.31
mg/Kg
10/25/22 08:20
10/27/22 14:31
1
Arsenic
3.0
1.9
1.2
mg/Kg
10/25/22 08:20
10/27/22 14:31
1
Barium
83
0.97
0.40
mg/Kg
10/25/22 08:20
10/27/22 14:31
1
Cadmium
0.18
J
0.49
0.097
mg/Kg
10/25/22 08:20
10/27/22 14:31
1
Lead
11
0.97
0.59
mg/Kg
10/25/22 08:20
10/27/22 14:31
1
Selenium
<1.1
2.4
1.1
mg/Kg
10/25/22 08:20
10/27/22 14:31
1
Antimony
<0.85
1.9
0.85
mg/Kg
10/25/22 08:20
10/27/22 14:31
1
Beryllium
0.74
0.39
0.069
mg/Kg
10/25/22 08:20
10/27/22 14:31
1
Thallium
<0.76
2.4
0.76
mg/Kg
10/25/22 08:20
10/27/22 14:31
1
Nickel
3.8
J
3.9
0.87
mg/Kg
10/25/22 08:20
10/27/22 14:31
1
Vanadium
26
0.97
0.16
mg/Kg
10/25/22 08:20
10/27/22 14:31
1
Copper
14
2.4
0.49
mg/Kg
10/25/22 08:20
10/27/22 14:31
1
Zinc
58
1.9
0.56
mg/Kg
10/25/22 08:20
10/27/22 14:31
1
Cobalt
4.0
0.97
0.32
mg/Kg
10/25/22 08:20
10/27/22 14:31
1
Method: SW846 7471 B - Mercury (CVAA)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Mercury
0.021
J
0.027
0.0085
mg/Kg
10/28/22 09:19
10/31/22 10:49
1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Phosphorus (EPA 365.4-1974)
260
11
6.1
mg/Kg
*
10/27/22 17:30
10/28/22 12:46
1
Eurofins Savannah
Page 23 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: SS-7 Lab Sample ID: 680-223856-7
Date Collected: 10/20/22 10:50 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 93.1
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
Analyte
Result Qualifier
RL
1,1,1,2-Tetrachloroethane
<1.5
5.6
1,1,1-Trichloroethane
<2.9
5.6
1,1,2-Trichloroethane
<1.7
5.6
1,1-Dichloroethane
<3.2
5.6
1,1-Dichloroethene
<4.0
5.6
1,2,3-Trichlorobenzene
<2.2
5.6
1,2,4-Trichlorobenzene
<2.8
5.6
1,2-Dibromo-3-Chloropropane
<1.8
11
1,2-Dibromoethane
<1.9
5.6
1,2-Dichlorobenzene
<1.9
5.6
1,2-Dichloroethane
<2.6
5.6
1,2-Dichloropropane
<2.9
5.6
1,3-Dichlorobenzene
<2.2
5.6
1,4-Dichlorobenzene
<2.0
5.6
2-Butanone (MEK)
<10
28
2-Hexanone
<21
28
4-Methyl-2-pentanone (MIBK)
<20
28
Acetone
<12
56
Benzene
<2.7
5.6
Bromochloromethane
<2.2
5.6
Bromoform
<2.5
5.6
Bromomethane
<2.7
5.6
Carbon disulfide
<2.3 `+
5.6
Carbon tetrachloride
<2.3
5.6
Chlorobenzene
<1.6
5.6
Chloroethane
<2.5
5.6
Chloroform
<2.2
5.6
Chloromethane
<2.7
5.6
cis-1,2-Dichloroethene
<3.2
5.6
cis-1,3-Dichloropropene
<2.5
5.6
Cyclohexane
<2.6
5.6
Dichlorobromomethane
<2.2
5.6
Dichlorodifluoromethane
<3.6
5.6
Ethylbenzene
<2.3
5.6
Freon 113
<3.2
5.6
Hexachlorobutadiene
<4.6
5.6
Isopropylbenzene
<2.5
5.6
Methyl acetate
<9.1
28
Methyl tert-butyl ether
<2.5
5.6
Methylcyclohexane
<2.2 '+
5.6
Methylene Chloride
<9.0
11
m-Xylene & p-Xylene
<2.5
5.6
o-Xylene
<2.6
5.6
Styrene
<2.1
5.6
Tetrachloroethene
<2.9
5.6
Toluene
<2.9
5.6
trans- 1,2-Dichloroethene
<2.6
5.6
trans- 1,3-Dichloropropene
<2.9
5.6
Trichloroethene
<2.0
5.6
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1.5
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
2.9
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
1.7
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
3.2
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
4.0
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
2.2
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
2.8
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
1.8
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
1.9
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
1.9
ug/Kg
10/25/2212:49
11/03/2213:07
1
2.6
ug/Kg
10/25/2212:49
11/03/2213:07
1
2.9
ug/Kg
10/25/2212:49
11/03/2213:07
1
2.2
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
2.0
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
10
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
21
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
20
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
12
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
2.7
ug/Kg
10/25/2212:49
11/03/2213:07
1
2.2
ug/Kg
10/25/2212:49
11/03/2213:07
1
2.5
ug/Kg
10/25/2212:49
11/03/2213:07
1
2.7
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
2.3
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
2.3
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
1.6
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
2.5
ug/Kg
10/25/2212:49
11/03/2213:07
1
2.2
ug/Kg
10/25/2212:49
11/03/2213:07
1
2.7
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
3.2
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
2.5
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
2.6
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
2.2
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
3.6
ug/Kg
*
10/25/2212:49
11/03/2213:07
1
2.3
ug/Kg
10/25/2212:49
11/03/2213:07
1
3.2
ug/Kg
10/25/2212:49
11/03/2213:07
1
4.6
ug/Kg
10/25/2212:49
11/03/2213:07
1
2.5
ug/Kg
10/25/2212:49
11/03/2213:07
1
9.1
ug/Kg
10/25/2212:49
11/03/2213:07
1
2.5
ug/Kg
10/25/2212:49
11/03/2213:07
1
2.2
ug/Kg
10/25/2212:49
11/03/2213:07
1
9.0
ug/Kg
10/25/2212:49
11/03/2213:07
1
2.5
ug/Kg
10/25/2212:49
11/03/2213:07
1
2.6
ug/Kg
10/25/2212:49
11/03/2213:07
1
2.1
ug/Kg
10/25/2212:49
11/03/2213:07
1
2.9
ug/Kg
10/25/2212:49
11/03/2213:07
1
2.9
ug/Kg
10/25/2212:49
11/03/2213:07
1
2.6
ug/Kg
10/25/2212:49
11/03/2213:07
1
2.9
ug/Kg
10/25/2212:49
11/03/2213:07
1
2.0
ug/Kg
10/25/2212:49
11/03/2213:07
1
Eurofins Savannah
Page 24 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Job ID: 680-223856-1
Project/Site: CF15067
Client Sample ID: SS-7
Lab Sample
ID: 680-223856-7
Date Collected: 10/20/22 10:50
Matrix: Solid
Date Received: 10/22/22 07:00
Percent Solids: 93.1
Method: SW846 8260D - Volatile
Organic Compounds by GC/MS (Continued)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
Trichlorofluoromethane
<3.5
5.6 3.5 ug/Kg
* 10/25/22 12:49
11/03/2213:07 1
Vinyl chloride
<3.1
5.6 3.1 ug/Kg
* 10/25/22 12:49
11/03/22 13:07 1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr)
105
65- 130
10125122 12:49
11103122 13:07 1
4-Bromofluorobenzene (Surr)
99
65 - 130
10125122 12:49
11103122 13:07 1
Dibromofluoromethane (Surr)
104
65 - 130
10125122 12:49
11103122 13:07 1
Toluene-d8 (Surr)
102
65 - 130
10/25/22 12:49
11103122 13:07 1
Method: SW846 8270E SIM ID
- Semivolatile Organic Compounds (GC/MS SIM / Isotope
Dilution)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
1,4-Dioxane
<4.1
34 4.1 ug/Kg
* 10/31/2212:25
11/01/2219:28 1
Isotope Dilution
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,4-Dioxane-d8
58
10- 150
10131122 12:25
11101122 19:28 1
Method: SW846 9056A - Anions, Ion Chromatography - Soluble
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Sulfate
<8.6
21
8.6
mg/Kg
#
11/02/2216:06
1
Method: SW846 6010D - Metals (ICP)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Silver
<0.32
1.0
0.32
mg/Kg
10/25/22 08:20
10/27/22 14:34
1
Arsenic
1.9
J
2.0
1.2
mg/Kg
10/25/22 08:20
10/27/22 14:34
1
Barium
99
1.0
0.42
mg/Kg
10/25/22 08:20
10/27/22 14:34
1
Cadmium
0.21
J
0.51
0.10
mg/Kg
10/25/22 08:20
10/27/22 14:34
1
Lead
12
1.0
0.62
mg/Kg
10/25/22 08:20
10/27/22 14:34
1
Selenium
<1.1
2.5
1.1
mg/Kg
10/25/22 08:20
10/27/22 14:34
1
Antimony
<0.88
2.0
0.88
mg/Kg
10/25/22 08:20
10/27/22 14:34
1
Beryllium
0.80
0.41
0.072
mg/Kg
10/25/22 08:20
10/27/22 14:34
1
Thallium
<0.79
2.5
0.79
mg/Kg
10/25/22 08:20
10/27/22 14:34
1
Nickel
3.8
J
4.1
0.91
mg/Kg
10/25/22 08:20
10/27/22 14:34
1
Vanadium
29
1.0
0.16
mg/Kg
10/25/22 08:20
10/27/22 14:34
1
Copper
15
2.5
0.51
mg/Kg
10/25/22 08:20
10/27/22 14:34
1
Zinc
72
2.0
0.59
mg/Kg
10/25/22 08:20
10/27/22 14:34
1
Cobalt
4.8
1.0
0.33
mg/Kg
10/25/22 08:20
10/27/22 14:34
1
Method: SW846 7471 B - Mercury (CVAA)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Mercury
0.022
J
0.023
0.0074
mg/Kg
10/28/22 09:19
10/31/22 10:52
1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Phosphorus (EPA 365.4-1974)
290
10
5.7
mg/Kg
*
10/27/22 17:30
10/28/22 12:48
1
Eurofins Savannah
Page 25 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: SS-8 Lab Sample ID: 680-223856-8
Date Collected: 10/20/22 10:55 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 76.7
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
Analyte
Result Qualifier
RL
1,1,1,2-Tetrachloroethane
<1.8
6.7
1,1,1-Trichloroethane
<3.5
6.7
1,1,2-Trichloroethane
<2.0
6.7
1,1-Dichloroethane
<3.9
6.7
1,1-Dichloroethene
<4.8
6.7
1,2,3-Trichlorobenzene
<2.7
6.7
1,2,4-Trichlorobenzene
<3.4
6.7
1,2-Dibromo-3-Chloropropane
<2.2
13
1,2-Dibromoethane
<2.3
6.7
1,2-Dichlorobenzene
<2.3
6.7
1,2-Dichloroethane
<3.1
6.7
1,2-Dichloropropane
<3.5
6.7
1,3-Dichlorobenzene
<2.7
6.7
1,4-Dichlorobenzene
<2.4
6.7
2-Butanone (MEK)
<12
34
2-Hexanone
<26
34
4-Methyl-2-pentanone (MIBK)
<24
34
Acetone
<15
67
Benzene
<3.2
6.7
Bromochloromethane
<2.7
6.7
Bromoform
<3.0
6.7
Bromomethane
<3.2
6.7
Carbon disulfide
<2.8 `+
6.7
Carbon tetrachloride
<2.8
6.7
Chlorobenzene
<1.9
6.7
Chloroethane
<3.0
6.7
Chloroform
<2.7
6.7
Chloromethane
<3.2
6.7
cis-1,2-Dichloroethene
<3.9
6.7
cis-1,3-Dichloropropene
<3.0
6.7
Cyclohexane
<3.1
6.7
Dichlorobromomethane
<2.7
6.7
Dichlorodifluoromethane
<4.3
6.7
Ethylbenzene
<2.8
6.7
Freon 113
<3.9
6.7
Hexachlorobutadiene
<5.5
6.7
Isopropylbenzene
<3.0
6.7
Methyl acetate
<11
34
Methyl tert-butyl ether
<3.0
6.7
Methylcyclohexane
<2.7 *+
6.7
Methylene Chloride
<11
13
m-Xylene & p-Xylene
<3.0
6.7
o-Xylene
<3.1
6.7
Styrene
<2.6
6.7
Tetrachloroethene
<3.5
6.7
Toluene
<3.5
6.7
trans- 1,2-Dichloroethene
<3.1
6.7
trans- 1,3-Dichloropropene
<3.5
6.7
Trichloroethene
<2.4
6.7
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1.8
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
3.5
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
2.0
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
3.9
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
4.8
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
2.7
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
3.4
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
2.2
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
2.3
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
2.3
ug/Kg
10/25/2212:49
11/03/2213:31
1
3.1
ug/Kg
10/25/2212:49
11/03/2213:31
1
3.5
ug/Kg
10/25/2212:49
11/03/2213:31
1
2.7
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
2.4
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
12
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
26
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
24
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
15
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
3.2
ug/Kg
10/25/2212:49
11/03/2213:31
1
2.7
ug/Kg
10/25/2212:49
11/03/2213:31
1
3.0
ug/Kg
10/25/2212:49
11/03/2213:31
1
3.2
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
2.8
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
2.8
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
1.9
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
3.0
ug/Kg
10/25/2212:49
11/03/2213:31
1
2.7
ug/Kg
10/25/2212:49
11/03/2213:31
1
3.2
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
3.9
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
3.0
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
3.1
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
2.7
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
4.3
ug/Kg
*
10/25/2212:49
11/03/2213:31
1
2.8
ug/Kg
10/25/2212:49
11/03/2213:31
1
3.9
ug/Kg
10/25/2212:49
11/03/2213:31
1
5.5
ug/Kg
10/25/2212:49
11/03/2213:31
1
3.0
ug/Kg
10/25/2212:49
11/03/2213:31
1
11
ug/Kg
10/25/2212:49
11/03/2213:31
1
3.0
ug/Kg
10/25/2212:49
11/03/2213:31
1
2.7
ug/Kg
10/25/2212:49
11/03/2213:31
1
11
ug/Kg
10/25/2212:49
11/03/2213:31
1
3.0
ug/Kg
10/25/2212:49
11/03/2213:31
1
3.1
ug/Kg
10/25/2212:49
11/03/2213:31
1
2.6
ug/Kg
10/25/2212:49
11/03/2213:31
1
3.5
ug/Kg
10/25/2212:49
11/03/2213:31
1
3.5
ug/Kg
10/25/2212:49
11/03/2213:31
1
3.1
ug/Kg
10/25/2212:49
11/03/2213:31
1
3.5
ug/Kg
10/25/2212:49
11/03/2213:31
1
2.4
ug/Kg
10/25/2212:49
11/03/2213:31
1
Eurofins Savannah
Page 26 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Job ID: 680-223856-1
Project/Site: CF15067
Client Sample ID: SS-8
Lab Sample
ID: 680-223856-8
Date Collected: 10/20/22 10:55
Matrix: Solid
Date Received: 10/22/22 07:00
Percent Solids: 76.7
Method: SW846 8260D - Volatile
Organic Compounds by GC/MS (Continued)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
Trichlorofluoromethane
<4.2
6.7 4.2 ug/Kg
* 10/25/22 12:49
11/03/2213:31 1
Vinyl chloride
<3.8
6.7 3.8 ug/Kg
* 10/25/22 12:49
11/03/22 13:31 1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr)
105
65- 130
10125122 12:49
11103122 13:31 1
4-Bromofluorobenzene (Surr)
99
65 - 130
10125122 12:49
11103122 13:31 1
Dibromofluoromethane (Surr)
106
65 - 130
10125122 12:49
11103122 13:31 1
Toluene-d8 (Surr)
101
65 - 130
10/25/22 12:49
11103122 13:31 1
Method: SW846 8270E SIM ID
- Semivolatile Organic Compounds (GC/MS SIM / Isotope
Dilution)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
1,4-Dioxane
<4.9
41 4.9 ug/Kg
* 10/31/2212:25
11/01/2219:49 1
Isotope Dilution
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,4-Dioxane-d8
59
10- 150
10131122 12:25
11101122 19:49 1
Method: SW846 9056A - Anions, Ion Chromatography - Soluble
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Sulfate
22
J
26
10
mg/Kg
#
11/02/2216:45
1
Method: SW846 6010D - Metals (ICP)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Silver
<0.35
1.1
0.35
mg/Kg
10/25/22 08:20
10/27/22 14:36
1
Arsenic
2.5
2.2
1.3
mg/Kg
10/25/22 08:20
10/27/22 14:36
1
Barium
60
1.1
0.45
mg/Kg
10/25/22 08:20
10/27/22 14:36
1
Cadmium
0.13
J
0.54
0.11
mg/Kg
10/25/22 08:20
10/27/22 14:36
1
Lead
9.8
1.1
0.66
mg/Kg
10/25/22 08:20
10/27/22 14:36
1
Selenium
<1.2
2.7
1.2
mg/Kg
10/25/22 08:20
10/27/22 14:36
1
Antimony
<0.95
2.2
0.95
mg/Kg
10/25/22 08:20
10/27/22 14:36
1
Beryllium
0.52
0.43
0.077
mg/Kg
10/25/22 08:20
10/27/22 14:36
1
Thallium
<0.85
2.7
0.85
mg/Kg
10/25/22 08:20
10/27/22 14:36
1
Nickel
3.3
J
4.3
0.98
mg/Kg
10/25/22 08:20
10/27/22 14:36
1
Vanadium
20
1.1
0.17
mg/Kg
10/25/22 08:20
10/27/22 14:36
1
Copper
8.4
2.7
0.54
mg/Kg
10/25/22 08:20
10/27/22 14:36
1
Zinc
41
2.2
0.63
mg/Kg
10/25/22 08:20
10/27/22 14:36
1
Cobalt
2.9
1.1
0.36
mg/Kg
10/25/22 08:20
10/27/22 14:36
1
Method: SW846 7471 B - Mercury (CVAA)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Mercury
0.020
J
0.029
0.0093
mg/Kg
10/28/22 09:19
10/31/22 10:56
1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Phosphorus (EPA 365.4-1974)
210
13
6.9
mg/Kg
*
10/28/22 12:28
10/31/22 09:31
1
Eurofins Savannah
Page 27 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: BG-1 Lab Sample ID: 680-223856-9
Date Collected: 10/20/22 11:10 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 84.7
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
Analyte
Result Qualifier
RL
1,1,1,2-Tetrachloroethane
<1.9
7.3
1,1,1-Trichloroethane
<3.8
7.3
1,1,2-Trichloroethane
<2.2
7.3
1,1-Dichloroethane
<4.2
7.3
1,1-Dichloroethene
<5.2
7.3
1,2,3-Trichlorobenzene
<2.9
7.3
1,2,4-Trichlorobenzene
<3.6
7.3
1,2-Dibromo-3-Chloropropane
<2.3
15
1,2-Dibromoethane
<2.5
7.3
1,2-Dichlorobenzene
<2.5
7.3
1,2-Dichloroethane
<3.3
7.3
1,2-Dichloropropane
<3.8
7.3
1,3-Dichlorobenzene
<2.9
7.3
1,4-Dichlorobenzene
<2.6
7.3
2-Butanone (MEK)
<13
36
2-Hexanone
<28
36
4-Methyl-2-pentanone (MIBK)
<26
36
Acetone
<16
73
Benzene
<3.5
7.3
Bromochloromethane
<2.9
7.3
Bromoform
<3.2
7.3
Bromomethane
<3.5
7.3
Carbon disulfide
<3.1 `+
7.3
Carbon tetrachloride
<3.1
7.3
Chlorobenzene
<2.0
7.3
Chloroethane
<3.2
7.3
Chloroform
<2.9
7.3
Chloromethane
<3.5
7.3
cis-1,2-Dichloroethene
<4.2
7.3
cis-1,3-Dichloropropene
<3.2
7.3
Cyclohexane
<3.3
7.3
Dichlorobromomethane
<2.9
7.3
Dichlorodifluoromethane
<4.7
7.3
Ethylbenzene
<3.1
7.3
Freon 113
<4.2
7.3
Hexachlorobutadiene
<6.0
7.3
Isopropylbenzene
<3.2
7.3
Methyl acetate
<12
36
Methyl tert-butyl ether
<3.2
7.3
Methylcyclohexane
<2.9 *+
7.3
Methylene Chloride
<12
15
m-Xylene & p-Xylene
<3.2
7.3
o-Xylene
<3.3
7.3
Styrene
<2.8
7.3
Tetrachloroethene
<3.8
7.3
Toluene
<3.8
7.3
trans- 1,2-Dichloroethene
<3.3
7.3
trans- 1,3-Dichloropropene
<3.8
7.3
Trichloroethene
<2.6
7.3
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1.9
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
3.8
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
2.2
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
4.2
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
5.2
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
2.9
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
3.6
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
2.3
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
2.5
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
2.5
ug/Kg
10/25/2212:49
11/03/2213:55
1
3.3
ug/Kg
10/25/2212:49
11/03/2213:55
1
3.8
ug/Kg
10/25/2212:49
11/03/2213:55
1
2.9
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
2.6
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
13
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
28
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
26
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
16
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
3.5
ug/Kg
10/25/2212:49
11/03/2213:55
1
2.9
ug/Kg
10/25/2212:49
11/03/2213:55
1
3.2
ug/Kg
10/25/2212:49
11/03/2213:55
1
3.5
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
3.1
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
3.1
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
2.0
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
3.2
ug/Kg
10/25/2212:49
11/03/2213:55
1
2.9
ug/Kg
10/25/2212:49
11/03/2213:55
1
3.5
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
4.2
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
3.2
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
3.3
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
2.9
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
4.7
ug/Kg
*
10/25/2212:49
11/03/2213:55
1
3.1
ug/Kg
10/25/2212:49
11/03/2213:55
1
4.2
ug/Kg
10/25/2212:49
11/03/2213:55
1
6.0
ug/Kg
10/25/2212:49
11/03/2213:55
1
3.2
ug/Kg
10/25/2212:49
11/03/2213:55
1
12
ug/Kg
10/25/2212:49
11/03/2213:55
1
3.2
ug/Kg
10/25/2212:49
11/03/2213:55
1
2.9
ug/Kg
10/25/2212:49
11/03/2213:55
1
12
ug/Kg
10/25/2212:49
11/03/2213:55
1
3.2
ug/Kg
10/25/2212:49
11/03/2213:55
1
3.3
ug/Kg
10/25/2212:49
11/03/2213:55
1
2.8
ug/Kg
10/25/2212:49
11/03/2213:55
1
3.8
ug/Kg
10/25/2212:49
11/03/2213:55
1
3.8
ug/Kg
10/25/2212:49
11/03/2213:55
1
3.3
ug/Kg
10/25/2212:49
11/03/2213:55
1
3.8
ug/Kg
10/25/2212:49
11/03/2213:55
1
2.6
ug/Kg
10/25/2212:49
11/03/2213:55
1
Eurofins Savannah
Page 28 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Job ID: 680-223856-1
Project/Site: CF15067
Client Sample ID: BG-1
Lab Sample
ID: 680-223856-9
Date Collected: 10/20/22 11:10
Matrix: Solid
Date Received: 10/22/22 07:00
Percent Solids: 84.7
Method: SW846 8260D - Volatile
Organic Compounds by GC/MS (Continued)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
Trichlorofluoromethane
<4.5
7.3 4.5 ug/Kg
* 10/25/22 12:49
11/03/2213:55 1
Vinyl chloride
<4.1
7.3 4.1 ug/Kg
* 10/25/22 12:49
11/03/22 13:55 1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr)
106
65- 130
10125122 12:49
11103122 13:55 1
4-Bromofluorobenzene (Surr)
103
65 - 130
10125122 12:49
11103122 13:55 1
Dibromofluoromethane (Surr)
105
65 - 130
10125122 12:49
11103122 13:55 1
Toluene-d8 (Surr)
103
65 - 130
10/25/22 12:49
11103122 13:55 1
Method: SW846 8270E SIM ID
- Semivolatile Organic Compounds (GC/MS SIM / Isotope
Dilution)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
1,4-Dioxane
<4.6
38 4.6 ug/Kg
* 10/31/22 12:25
11/01/22 20:12 1
Isotope Dilution
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,4-Dioxane-d8
31
10- 150
10131122 12:25
11101122 20:12 1
Method: SW846 9056A - Anions, Ion Chromatography - Soluble
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Sulfate
<9.4
24
9.4
mg/Kg
#
11/02/2216:58
1
Method: SW846 6010D - Metals (ICP)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Silver
<0.37
1.2
0.37
mg/Kg
10/25/22 08:20
10/27/22 14:39
1
Arsenic
2.7
2.3
1.4
mg/Kg
10/25/22 08:20
10/27/22 14:39
1
Barium
72
1.2
0.47
mg/Kg
10/25/22 08:20
10/27/22 14:39
1
Cadmium
0.26
J
0.58
0.12
mg/Kg
10/25/22 08:20
10/27/22 14:39
1
Lead
18
1.2
0.71
mg/Kg
10/25/22 08:20
10/27/22 14:39
1
Selenium
<1.3
2.9
1.3
mg/Kg
10/25/22 08:20
10/27/22 14:39
1
Antimony
<1.0
2.3
1.0
mg/Kg
10/25/22 08:20
10/27/22 14:39
1
Beryllium
0.34
J
0.46
0.082
mg/Kg
10/25/22 08:20
10/27/22 14:39
1
Thallium
<0.90
2.9
0.90
mg/Kg
10/25/22 08:20
10/27/22 14:39
1
Nickel
6.0
4.6
1.0
mg/Kg
10/25/22 08:20
10/27/22 14:39
1
Vanadium
24
1.2
0.19
mg/Kg
10/25/22 08:20
10/27/22 14:39
1
Copper
20
2.9
0.58
mg/Kg
10/25/22 08:20
10/27/22 14:39
1
Zinc
100
2.3
0.67
mg/Kg
10/25/22 08:20
10/27/22 14:39
1
Cobalt
3.0
1.2
0.38
mg/Kg
10/25/22 08:20
10/27/22 14:39
1
Method: SW846 7471 B - Mercury (CVAA)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Mercury
0.081
0.028
0.0089
mg/Kg
10/28/22 09:19
10/31/22 10:59
1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Phosphorus (EPA 365.4-1974)
640
57
32
mg/Kg
*
10/28/22 12:28
10/31/22 13:18
5
Eurofins Savannah
Page 29 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: DUP-01 Lab Sample ID: 680-223856-10
Date Collected: 10/20/22 08:00 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 90.0
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
Analyte
Result Qualifier
RL
1,1,1,2-Tetrachloroethane
<1.5
5.7
1,1,1-Trichloroethane
<2.9
5.7
1,1,2-Trichloroethane
<1.7
5.7
1,1-Dichloroethane
<3.3
5.7
1,1-Dichloroethene
<4.1
5.7
1,2,3-Trichlorobenzene
<2.3
5.7
1,2,4-Trichlorobenzene
<2.8
5.7
1,2-Dibromo-3-Chloropropane
<1.8
11
1,2-Dibromoethane
<1.9
5.7
1,2-Dichlorobenzene
<1.9
5.7
1,2-Dichloroethane
<2.6
5.7
1,2-Dichloropropane
<2.9
5.7
1,3-Dichlorobenzene
<2.3
5.7
1,4-Dichlorobenzene
<2.0
5.7
2-Butanone (MEK)
<10
28
2-Hexanone
<22
28
4-Methyl-2-pentanone (MIBK)
<20
28
Acetone
<12
57
Benzene
<2.7
5.7
Bromochloromethane
<2.3
5.7
Bromoform
<2.5
5.7
Bromomethane
<2.7
5.7
Carbon disulfide
<2.4 `+
5.7
Carbon tetrachloride
<2.4
5.7
Chlorobenzene
<1.6
5.7
Chloroethane
<2.5
5.7
Chloroform
<2.3
5.7
Chloromethane
<2.7
5.7
cis-1,2-Dichloroethene
<3.3
5.7
cis-1,3-Dichloropropene
<2.5
5.7
Cyclohexane
<2.6
5.7
Dichlorobromomethane
<2.3
5.7
Dichlorodifluoromethane
<3.6
5.7
Ethylbenzene
<2.4
5.7
Freon 113
<3.3
5.7
Hexachlorobutadiene
<4.6
5.7
Isopropylbenzene
<2.5
5.7
Methyl acetate
<9.2
28
Methyl tert-butyl ether
<2.5
5.7
Methylcyclohexane
<2.3 '+
5.7
Methylene Chloride
<9.1
11
m-Xylene & p-Xylene
<2.5
5.7
o-Xylene
<2.6
5.7
Styrene
<2.2
5.7
Tetrachloroethene
<2.9
5.7
Toluene
<2.9
5.7
trans- 1,2-Dichloroethene
<2.6
5.7
trans- 1,3-Dichloropropene
<2.9
5.7
Trichloroethene
<2.0
5.7
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1.5
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
2.9
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
1.7
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
3.3
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
4.1
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
2.3
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
2.8
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
1.8
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
1.9
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
1.9
ug/Kg
10/25/2212:49
11/03/2214:19
1
2.6
ug/Kg
10/25/2212:49
11/03/2214:19
1
2.9
ug/Kg
10/25/2212:49
11/03/2214:19
1
2.3
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
2.0
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
10
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
22
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
20
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
12
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
2.7
ug/Kg
10/25/2212:49
11/03/2214:19
1
2.3
ug/Kg
10/25/2212:49
11/03/2214:19
1
2.5
ug/Kg
10/25/2212:49
11/03/2214:19
1
2.7
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
2.4
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
2.4
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
1.6
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
2.5
ug/Kg
10/25/2212:49
11/03/2214:19
1
2.3
ug/Kg
10/25/2212:49
11/03/2214:19
1
2.7
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
3.3
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
2.5
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
2.6
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
2.3
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
3.6
ug/Kg
*
10/25/2212:49
11/03/2214:19
1
2.4
ug/Kg
10/25/2212:49
11/03/2214:19
1
3.3
ug/Kg
10/25/2212:49
11/03/2214:19
1
4.6
ug/Kg
10/25/2212:49
11/03/2214:19
1
2.5
ug/Kg
10/25/2212:49
11/03/2214:19
1
9.2
ug/Kg
10/25/2212:49
11/03/2214:19
1
2.5
ug/Kg
10/25/2212:49
11/03/2214:19
1
2.3
ug/Kg
10/25/2212:49
11/03/2214:19
1
9.1
ug/Kg
10/25/2212:49
11/03/2214:19
1
2.5
ug/Kg
10/25/2212:49
11/03/2214:19
1
2.6
ug/Kg
10/25/2212:49
11/03/2214:19
1
2.2
ug/Kg
10/25/2212:49
11/03/2214:19
1
2.9
ug/Kg
10/25/2212:49
11/03/2214:19
1
2.9
ug/Kg
10/25/2212:49
11/03/2214:19
1
2.6
ug/Kg
10/25/2212:49
11/03/2214:19
1
2.9
ug/Kg
10/25/2212:49
11/03/2214:19
1
2.0
ug/Kg
10/25/2212:49
11/03/2214:19
1
Eurofins Savannah
Page 30 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Job ID: 680-223856-1
Project/Site: CF15067
Client Sample ID: DUP-01
Lab Sample ID: 680-223856-10
Date Collected: 10/20/22 08:00
Matrix: Solid
Date Received: 10/22/22 07:00
Percent Solids: 90.0
Method: SW846 8260D - Volatile
Organic Compounds by GC/MS (Continued)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
Trichlorofluoromethane
<3.5
5.7 3.5 ug/Kg
* 10/25/22 12:49
11/03/2214:19 1
Vinyl chloride
<3.2
5.7 3.2 ug/Kg
* 10/25/22 12:49
11/03/22 14:19 1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr)
104
65- 130
10125122 12:49
11103122 14:19 1
4-Bromofluorobenzene (Surr)
99
65 - 130
10125122 12:49
11103122 14:19 1
Dibromofluoromethane (Surr)
104
65 - 130
10125122 12:49
11103122 14:19 1
Toluene-d8 (Surr)
103
65 - 130
10/25/22 12:49
11103122 14:19 1
Method: SW846 8270E SIM ID
- Semivolatile Organic Compounds (GC/MS SIM /
Isotope Dilution)
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
1,4-Dioxane
<4.3
35 4.3 ug/Kg
* 10/31/22 12:25
11/01/22 20:34 1
Isotope Dilution
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,4-Dioxane-d8
61
10- 150
10131122 12:25
11101122 20:34 1
Method: SW846 9056A - Anions, Ion Chromatography - Soluble
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Sulfate
<8.8
F1
22
8.8
mg/Kg
#
11/02/2217:24
1
Method: SW846 6010D - Metals (ICP)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Silver
<0.31
0.97
0.31
mg/Kg
10/25/22 08:20
10/27/22 14:42
1
Arsenic
3.2
1.9
1.2
mg/Kg
10/25/22 08:20
10/27/22 14:42
1
Barium
87
0.97
0.40
mg/Kg
10/25/22 08:20
10/27/22 14:42
1
Cadmium
0.18
J
0.49
0.097
mg/Kg
10/25/22 08:20
10/27/22 14:42
1
Lead
13
0.97
0.59
mg/Kg
10/25/22 08:20
10/27/22 14:42
1
Selenium
<1.1
2.4
1.1
mg/Kg
10/25/22 08:20
10/27/22 14:42
1
Antimony
<0.85
1.9
0.85
mg/Kg
10/25/22 08:20
10/27/22 14:42
1
Beryllium
0.87
0.39
0.069
mg/Kg
10/25/22 08:20
10/27/22 14:42
1
Thallium
<0.76
2.4
0.76
mg/Kg
10/25/22 08:20
10/27/22 14:42
1
Nickel
4.5
3.9
0.88
mg/Kg
10/25/22 08:20
10/27/22 14:42
1
Vanadium
30
0.97
0.16
mg/Kg
10/25/22 08:20
10/27/22 14:42
1
Copper
17
2.4
0.49
mg/Kg
10/25/22 08:20
10/27/22 14:42
1
Zinc
55
1.9
0.57
mg/Kg
10/25/22 08:20
10/27/22 14:42
1
Cobalt
4.0
0.97
0.32
mg/Kg
10/25/22 08:20
10/27/22 14:42
1
Method: SW846 7471 B - Mercury (CVAA)
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Mercury
0.023
J B
0.026
0.0084
mg/Kg
10/28/22 10:02
10/31/22 11:09
1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Phosphorus (EPA 365.4-1974)
310
11
5.9
mg/Kg
*
10/28/22 12:28
10/31/22 09:37
1
Eurofins Savannah
Page 31 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: Trip Blank Lab Sample ID: 680-223856-11
Date Collected: 10/20/22 08:00 Matrix: Water
Date Received: 10/22/22 07:00
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
Analyte
Result Qualifier
RL
Chloromethane
<0.54
1.0
Vinyl chloride
<0.40
1.0
Bromomethane
<3.7
5.0
Chloroethane
<4.6
5.0
Trichlorofluoromethane
<0.33
1.0
1,1-Dichloroethene
<0.33
1.0
1,1,2-Trichloro-1,2,2-trifluoroethane
<0.23
1.0
Acetone
<3.7
10
Carbon disulfide
<0.43 `+
2.0
Methyl acetate
<3.2
5.0
Methylene Chloride
<3.2
5.0
trans- 1,2-Dichloroethene
<0.34
1.0
Methyl tert-butyl ether
<0.81
5.0
1,1-Dichloroethane
<0.33
1.0
cis-1,2-Dichloroethene
<0.25
1.0
2-Butanone (MEK)
<6.4
10
Chloroform
<0.27
1.0
1,1,1-Trichloroethane
<0.21
1.0
Cyclohexane
<0.28
1.0
Carbon tetrachloride
<0.30
1.0
Benzene
<0.27
1.0
1,2-Dichloroethane
<0.25
1.0
Trichloroethene
<0.20
1.0
Methylcyclohexane
<0.33
1.0
1,2-Dichloropropene
<0.22
1.0
Dichlorobromomethane
<0.25
1.0
cis-1,3-Dichloropropene
<0.26
1.0
4-Methyl-2-pentanone (MIBK)
<2.7
10
Toluene
<0.25
1.0
trans- 1,3-Dichloropropene
<0.23
1.0
1,1,2-Trichloroethane
<0.32
1.0
Tetrachloroethene
<0.35
0.50
2-Hexanone
<3.2
10
Chlorodibromomethane
<0.39
1.0
Ethylene Dibromide
<0.33
1.0
Chlorobenzene
<0.15
1.0
Ethylbenzene
<0.20
1.0
Xylenes, Total
<0.23
1.0
Styrene
<0.27
1.0
Bromoform
<0.59
1.0
Isopropylbenzene
<0.26
1.0
1,1,2,2-Tetrachloroethane
<0.40
1.0
1,3-Dichlorobenzene
<0.31
1.0
1,4-Dichlorobenzene
<0.31
1.0
1,2-Dichlorobenzene
<0.31
1.0
1,2-Dibromo-3-Chloropropane
<1.8
5.0
1,2,4-Trichlorobenzene
<0.53
5.0
Surrogate
%Recovery Qualifier
Limits
Toluene-d8 (Surr)
104
70 - 130
MDL
Unit
D Prepared Analyzed
Dil Fac
0.54
ug/L
11/02/2214:29
1
0.40
ug/L
11/02/2214:29
1
3.7
ug/L
11/02/2214:29
1
4.6
ug/L
11/02/2214:29
1
0.33
ug/L
11/02/2214:29
1
0.33
ug/L
11/02/2214:29
1
0.23
ug/L
11/02/2214:29
1
3.7
ug/L
11/02/2214:29
1
0.43
ug/L
11/02/2214:29
1
3.2
ug/L
11/02/2214:29
1
3.2
ug/L
11/02/2214:29
1
0.34
ug/L
11/02/2214:29
1
0.81
ug/L
11/02/2214:29
1
0.33
ug/L
11/02/2214:29
1
0.25
ug/L
11/02/2214:29
1
6.4
ug/L
11/02/2214:29
1
0.27
ug/L
11/02/2214:29
1
0.21
ug/L
11/02/2214:29
1
0.28
ug/L
11/02/2214:29
1
0.30
ug/L
11/02/2214:29
1
0.27
ug/L
11/02/2214:29
1
0.25
ug/L
11/02/2214:29
1
0.20
ug/L
11/02/2214:29
1
0.33
ug/L
11/02/2214:29
1
0.22
ug/L
11/02/2214:29
1
0.25
ug/L
11/02/2214:29
1
0.26
ug/L
11/02/2214:29
1
2.7
ug/L
11/02/2214:29
1
0.25
ug/L
11/02/2214:29
1
0.23
ug/L
11/02/2214:29
1
0.32
ug/L
11/02/2214:29
1
0.35
ug/L
11/02/2214:29
1
3.2
ug/L
11/02/2214:29
1
0.39
ug/L
11/03/2215:56
1
0.33
ug/L
11/02/2214:29
1
0.15
ug/L
11/02/2214:29
1
0.20
ug/L
11/02/2214:29
1
0.23
ug/L
11/02/2214:29
1
0.27
ug/L
11/02/2214:29
1
0.59
ug/L
11/02/2214:29
1
0.26
ug/L
11/02/2214:29
1
0.40
ug/L
11/02/2214:29
1
0.31
ug/L
11/02/2214:29
1
0.31
ug/L
11/02/2214:29
1
0.31
ug/L
11/02/2214:29
1
1.8
ug/L
11/02/2214:29
1
0.53
ug/L
11/03/2215:56
1
Prepared Analyzed
Dil Fac
11102122 14:29
1
Eurofins Savannah
Page 32 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: Trip Blank
Lab Sample ID: 680-223856-11
Date Collected: 10/20/22 08:00
Matrix: Water
Date Received: 10/22/22 07:00
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
Toluene-d8 (Surr) 105
70 - 130
11103122 15:56 1
1,2-Dichloroethane-d4 (Surr) 76
60- 124
11102122 14:29 1
1,2-Dichloroethane-d4 (Surr) 103
60- 124
11103122 15:56 1
Dibromofluoromethane (Surr) 97
70- 130
11102122 14:29 1
Dibromofluoromethane (Surr) 118
70 - 130
11103122 15:56 1
4-Bromofluorobenzene (Surr) 97
70- 130
11/02/22 14:29 1
4-Bromofluorobenzene (Surr) 100
70 - 130
11103122 15:56 1 F
Eurofins Savannah
Page 33 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: Trip Blank Lab Sample ID: 680-223856-12
Date Collected: 10/20/22 08:00 Matrix: Water
Date Received: 10/22/22 07:00
Method: SW846 8260D - Volatile Organic Compounds by GC/MS
Analyte
Result Qualifier
RL
Chloromethane
<0.54
1.0
Vinyl chloride
<0.40
1.0
Bromomethane
<3.7
5.0
Chloroethane
<4.6
5.0
Trichlorofluoromethane
<0.33
1.0
1,1-Dichloroethene
<0.33
1.0
1,1,2-Trichloro-1,2,2-trifluoroethane
<0.23
1.0
Acetone
<3.7
10
Carbon disulfide
<0.43 `+
2.0
Methyl acetate
<3.2
5.0
Methylene Chloride
<3.2
5.0
trans- 1,2-Dichloroethene
<0.34
1.0
Methyl tert-butyl ether
<0.81
5.0
1,1-Dichloroethane
<0.33
1.0
cis-1,2-Dichloroethene
<0.25
1.0
2-Butanone (MEK)
<6.4
10
Chloroform
<0.27
1.0
1,1,1-Trichloroethane
<0.21
1.0
Cyclohexane
<0.28
1.0
Carbon tetrachloride
<0.30
1.0
Benzene
<0.27
1.0
1,2-Dichloroethane
<0.25
1.0
Trichloroethene
<0.20
1.0
Methylcyclohexane
<0.33
1.0
1,2-Dichloropropene
<0.22
1.0
Dichlorobromomethane
<0.25
1.0
cis-1,3-Dichloropropene
<0.26
1.0
4-Methyl-2-pentanone (MIBK)
<2.7
10
Toluene
<0.25
1.0
trans- 1,3-Dichloropropene
<0.23
1.0
1,1,2-Trichloroethane
<0.32
1.0
Tetrachloroethene
<0.35
0.50
2-Hexanone
<3.2
10
Chlorodibromomethane
<0.39
1.0
Ethylene Dibromide
<0.33
1.0
Chlorobenzene
<0.15
1.0
Ethylbenzene
<0.20
1.0
Xylenes, Total
<0.23
1.0
Styrene
<0.27
1.0
Bromoform
<0.59
1.0
Isopropylbenzene
<0.26
1.0
1,1,2,2-Tetrachloroethane
<0.40
1.0
1,3-Dichlorobenzene
<0.31
1.0
1,4-Dichlorobenzene
<0.31
1.0
1,2-Dichlorobenzene
<0.31
1.0
1,2-Dibromo-3-Chloropropane
<1.8
5.0
1,2,4-Trichlorobenzene
<0.53
5.0
Surrogate
%Recovery Qualifier
Limits
Toluene-d8 (Surr)
105
70 - 130
MDL
Unit
D Prepared Analyzed
Dil Fac
0.54
ug/L
11/02/2214:48
1
0.40
ug/L
11/02/2214:48
1
3.7
ug/L
11/02/2214:48
1
4.6
ug/L
11/02/2214:48
1
0.33
ug/L
11/02/2214:48
1
0.33
ug/L
11/02/2214:48
1
0.23
ug/L
11/02/2214:48
1
3.7
ug/L
11/02/2214:48
1
0.43
ug/L
11/02/2214:48
1
3.2
ug/L
11/02/2214:48
1
3.2
ug/L
11/02/2214:48
1
0.34
ug/L
11/02/2214:48
1
0.81
ug/L
11/02/2214:48
1
0.33
ug/L
11/02/2214:48
1
0.25
ug/L
11/02/2214:48
1
6.4
ug/L
11/02/2214:48
1
0.27
ug/L
11/02/2214:48
1
0.21
ug/L
11/02/2214:48
1
0.28
ug/L
11/02/2214:48
1
0.30
ug/L
11/02/2214:48
1
0.27
ug/L
11/02/2214:48
1
0.25
ug/L
11/02/2214:48
1
0.20
ug/L
11/02/2214:48
1
0.33
ug/L
11/02/2214:48
1
0.22
ug/L
11/02/2214:48
1
0.25
ug/L
11/02/2214:48
1
0.26
ug/L
11/02/2214:48
1
2.7
ug/L
11/02/2214:48
1
0.25
ug/L
11/02/2214:48
1
0.23
ug/L
11/02/2214:48
1
0.32
ug/L
11/02/2214:48
1
0.35
ug/L
11/02/2214:48
1
3.2
ug/L
11/02/2214:48
1
0.39
ug/L
11/03/2216:17
1
0.33
ug/L
11/02/2214:48
1
0.15
ug/L
11/02/2214:48
1
0.20
ug/L
11/02/2214:48
1
0.23
ug/L
11/02/2214:48
1
0.27
ug/L
11/02/2214:48
1
0.59
ug/L
11/02/2214:48
1
0.26
ug/L
11/02/2214:48
1
0.40
ug/L
11/02/2214:48
1
0.31
ug/L
11/02/2214:48
1
0.31
ug/L
11/02/2214:48
1
0.31
ug/L
11/02/2214:48
1
1.8
ug/L
11/02/2214:48
1
0.53
ug/L
11/03/2216:17
1
Prepared Analyzed
Dil Fac
11102122 14:48
1
Eurofins Savannah
Page 34 of 81 11/8/2022 (Rev. 1)

Client Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: Trip Blank
Lab Sample ID: 680-223856-12
Date Collected: 10/20/22 08:00
Matrix: Water
Date Received: 10/22/22 07:00
Method: SW846 8260D - Volatile Organic Compounds by GC/MS (Continued)
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
Toluene-d8 (Surr) 110
70 - 130
11103122 16:17 1
1,2-Dichloroethane-d4 (Surr) 76
60- 124
11102122 14:48 1
1,2-Dichloroethane-d4 (Surr) 100
60- 124
11103122 16:17 1
Dibromofluoromethane (Surr) 97
70- 130
11102122 14:48 1
Dibromofluoromethane (Surr) 115
70 - 130
11103122 16:17 1
4-Bromofluorobenzene (Surr) 100
70- 130
11/02/22 14:48 1
4-Bromofluorobenzene (Surr) 103
70 - 130
11103122 16:17 1 F
Eurofins Savannah
Page 35 of 81 11/8/2022 (Rev. 1)

Isotope Dilution Summary
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Method: 8270E SIM ID - Semivolatile Organic Compounds (GC/MS SIM / Isotope Dilution)
Matrix: Solid PreD TvDe: Total/NA
Lab Sample ID
680-223856-1
680-223856-1 MS
680-223856-1 MSD
680-223856-2
680-223856-3
680-223856-4
680-223856-5
680-223856-6
680-223856-7
680-223856-8
680-223856-9
680-223856-10
LCS 680-747919/19-A
MB 680-747919/18-A
Surrogate Legend
DXE = 1,4-Dioxane-d8
Client Sample ID
SS-1
SS-1
SS-1
SS-2
SS-3
SS-4
SS-5
SS-6
SS-7
SS-8
BG-1
DUP-01
Lab Control Sample
Method Blank
Percent Isotope Dilution Recovery (Acceptance Limits)
DXE
(10-150)
37
53
39
49
45
45
52
60
58
59
31
61
63
61
0
Page 36 of 81
Eurofins Savannah
11 /8/2022 (Rev. 1)

QC Sample Results
Client: Environmental Conservation Laboratories
Job ID: 680-223856-1
Project/Site: CF15067
Method: 8260D - Volatile Organic Compounds by GUMS
Lab Sample ID: MB 680-748284/9
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 748284
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
1,1-Dichloroethene
<0.33
1.0
0.33
ug/L
11/02/22 14:02
1
1,1-Dichloroethane
<0.33
1.0
0.33
ug/L
11/02/22 14:02
1
1,1,1-Trichloroethane
<0.21
1.0
0.21
ug/L
11/02/22 14:02
1
1,2-Dichloroethane
<0.25
1.0
0.25
ug/L
11/02/22 14:02
1
2-Butanone (MEK)
<6.4
10
6.4
ug/L
11/02/22 14:02
1
1,2-Dichloropropane
<0.22
1.0
0.22
ug/L
11/02/22 14:02
1
1,1,2-Trichloroethane
<0.32
1.0
0.32
ug/L
11/02/22 14:02
1
4-Methyl-2-pentanone (MIBK)
<2.7
10
2.7
ug/L
11/02/22 14:02
1
Acetone
<3.7
10
3.7
ug/L
11/02/22 14:02
1
2-Hexanone
<3.2
10
3.2
ug/L
11/02/22 14:02
1
Ethylene Dibromide
<0.33
1.0
0.33
ug/L
11/02/22 14:02
1
Benzene
<0.27
1.0
0.27
ug/L
11/02/22 14:02
1
Bromoform
<0.59
1.0
0.59
ug/L
11/02/22 14:02
1
Bromomethane
<3.7
5.0
3.7
ug/L
11/02/22 14:02
1
Carbon disulfide
<0.43
2.0
0.43
ug/L
11/02/22 14:02
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.40
ug/L
11/02/22 14:02
1
Carbon tetrachloride
<0.30
1.0
0.30
ug/L
11/02/22 14:02
1
1,3-Dichlorobenzene
<0.31
1.0
0.31
ug/L
11/02/22 14:02
1
Chlorobenzene
<0.15
1.0
0.15
ug/L
11/02/22 14:02
1
1,4-Dichlorobenzene
<0.31
1.0
0.31
ug/L
11/02/22 14:02
1
Chlorodibromomethane
<0.39
1.0
0.39
ug/L
11/02/22 14:02
1
1,2-Dichlorobenzene
<0.31
1.0
0.31
ug/L
11/02/22 14:02
1
Chloroethane
<4.6
5.0
4.6
ug/L
11/02/22 14:02
1
1,2-Dibromo-3-Chloropropane
<1.8
5.0
1.8
ug/L
11/02/22 14:02
1
Chloroform
<0.27
1.0
0.27
ug/L
11/02/22 14:02
1
1,2,4-Trichlorobenzene
1.99 J
5.0
0.53
ug/L
11/02/22 14:02
1
Chloromethane
<0.54
1.0
0.54
ug/L
11/02/22 14:02
1
cis-1,2-Dichloroethene
<0.25
1.0
0.25
ug/L
11/02/22 14:02
1
cis-1,3-Dichloropropene
<0.26
1.0
0.26
ug/L
11/02/22 14:02
1
Cyclohexane
<0.28
1.0
0.28
ug/L
11/02/22 14:02
1
Dichlorobromomethane
<0.25
1.0
0.25
ug/L
11/02/22 14:02
1
Ethylbenzene
<0.20
1.0
0.20
ug/L
11/02/22 14:02
1
1,1,2-Trichloro-1,2,2-trifluoroethane
<0.23
1.0
0.23
ug/L
11/02/22 14:02
1
Isopropylbenzene
<0.26
1.0
0.26
ug/L
11/02/22 14:02
1
Methyl acetate
<3.2
5.0
3.2
ug/L
11/02/22 14:02
1
Methyl tert-butyl ether
<0.81
5.0
0.81
ug/L
11/02/22 14:02
1
Methylcyclohexane
<0.33
1.0
0.33
ug/L
11/02/22 14:02
1
Methylene Chloride
<3.2
5.0
3.2
ug/L
11/02/22 14:02
1
Styrene
<0.27
1.0
0.27
ug/L
11/02/22 14:02
1
Tetrachloroethene
<0.35
0.50
0.35
ug/L
11/02/22 14:02
1
Toluene
<0.25
1.0
0.25
ug/L
11/02/22 14:02
1
trans- 1,2-Dichloroethene
<0.34
1.0
0.34
ug/L
11/02/22 14:02
1
trans- 1,3-Dichloropropene
<0.23
1.0
0.23
ug/L
11/02/22 14:02
1
Trichloroethene
<0.20
1.0
0.20
ug/L
11/02/22 14:02
1
Trichlorofluoromethane
<0.33
1.0
0.33
ug/L
11/02/22 14:02
1
Vinyl chloride
<0.40
1.0
0.40
ug/L
11/02/22 14:02
1
Xylenes, Total
<0.23
1.0
0.23
ug/L
11/02/22 14:02
1
Eurofins Savannah
Page 37 of 81 11/8/2022 (Rev. 1)

QC Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: MB 680-748284/9
Matrix: Water
Analysis Batch: 748284
MB MB
Surrogate %Recovery Qualifier
1,2-Dichloroethane-d4 (Surr)
76
4-Bromofluorobenzene (Surr)
95
Dibromofluoromethane (Surr)
98
Toluene-d8 (Surr)
106
Lab Sample ID: LCS 680-748284/5
Matrix: Water
Analysis Batch: 748284
Analyte
1,1-Dichloroethene
1,1-Dichloroethane
1,1,1-Trichloroethane
1,2-Dichloroethane
2-Butanone (MEK)
1,2-Dichloropropane
1,1,2-Trichloroethane
4-Methyl-2-pentanone (MIBK)
Acetone
2-Hexanone
Ethylene Dibromide
Benzene
Bromoform
Bromomethane
Carbon disulfide
1,1,2,2-Tetrachloroethane
Carbon tetrachloride
1,3-Dichlorobenzene
Chlorobenzene
1,4-Dichlorobenzene
Chlorodibromomethane
1,2-Dichlorobenzene
Chloroethane
1,2-Dibromo-3-Chloropropane
Chloroform
1,2,4-Trichlorobenzene
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Cyclohexane
Dichlorobromomethane
Ethylbenzene
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
Isopropylbenzene
Methyl acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
Job ID: 680-223856-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Limits
Prepared Analyzed
Dil Fac
60 - 124
11102122 14: 02
1
70 - 130
11102122 14: 02
1
70 - 130
11102122 14: 02
1
70 - 130
11102122 14: 02
1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS LCS
%Rec
Added
Result Qualifier
Unit
D %Rec
Limits
50.0
63.4
ug/L
127
70 -130
50.0
56.4
ug/L
113
70 -130
50.0
50.5
ug/L
101
70 -130
50.0
45.8
ug/L
92
70 -130
250
204
ug/L
82
69-120
50.0
52.2
ug/L
104
70 -130
50.0
54.0
ug/L
108
70 -130
250
241
ug/L
96
68-120
250
247
ug/L
99
67-120
250
261
ug/L
105
70-130
50.0
56.3
ug/L
113
70 -130
50.0
53.0
ug/L
106
70 -130
50.0
57.8
ug/L
116
69 -129
50.0
48.4
ug/L
97
28 -192
50.0
65.9 "+
ug/L
132
70 -130
50.0
51.0
ug/L
102
70 -130
50.0
45.0
ug/L
90
70 -130
50.0
52.6
ug/L
105
70 -130
50.0
54.4
ug/L
109
70 -130
50.0
52.2
ug/L
104
70 -130
50.0
46.3
ug/L
93
70 -130
50.0
55.6
ug/L
111
70 -130
50.0
63.8
ug/L
128
31 - 213
50.0
51.8
ug/L
104
70 -130
50.0
54.0
ug/L
108
70 -130
50.0
51.6
ug/L
103
70 -130
50.0
61.2
ug/L
122
59 -127
50.0
52.4
ug/L
105
70 -130
50.0
51.5
ug/L
103
70 -130
50.0
55.0
ug/L
110
23 -175
50.0
50.6
ug/L
101
70 -130
50.0
54.1
ug/L
108
70 -130
50.0
53.9
ug/L
108
63 -141
50.0
57.4
ug/L
115
70 -130
100
94.0
ug/L
94
67 -120
50.0
37.6
ug/L
75
70 -130
50.0
53.4
ug/L
107
70 -130
50.0
63.3
ug/L
127
70 -130
Page 38 of 81
Eurofins Savannah
11 /8/2022 (Rev. 1)

QC Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: LCS 680-748284/5
Matrix: Water
Analysis Batch: 748284
Job ID: 680-223856-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Analyte
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec
Limits
Styrene
50.0
58.8
ug/L
118
70 -130
Tetrachloroethene
50.0
58.6
ug/L
117
70 -130
Toluene
50.0
57.4
ug/L
115
70 -130
trans- 1,2-Dichloroethene
50.0
57.2
ug/L
114
70-130
trans- 1,3-Dichloropropene
50.0
49.2
ug/L
98
70-130
Trichloroethene
50.0
50.8
ug/L
102
70 -130
Trichlorofluoromethane
50.0
51.0 E
ug/L
102
63 -142
Vinyl chloride
50.0
55.1
ug/L
110
66 -129
Xylenes, Total
100
109
ug/L
109
70 -130
Surrogate
1,2-Dichloroethane-d4 (Surr)
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
Toluene-d8 (Surr)
LCS LCS
%Recovery Qualifier
Limits
92
60-124
93
70-130
116
70-130
115
70-130
Lab Sample ID: LCSD 680-748284/6
Matrix: Water
Analysis Batch: 748284
Analyte
Spike
Added
LCSD
Result
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
LCSD %Rec RPD
Qualifier Unit D %Rec Limits RPD Limit
1,1-Dichloroethene
50.0
60.3
ug/L
121
70-130
5
20
1,1-Dichloroethane
50.0
56.1
ug/L
112
70-130
1
30
1,1,1-Trichloroethane
50.0
49.0
ug/L
98
70-130
3
30
1,2-Dichloroethane
50.0
44.9
ug/L
90
70 -130
2
50
2-Butanone (MEK)
250
203
ug/L
81
69 -120
0
30
1,2-Dichloropropane
50.0
50.9
ug/L
102
70 -130
3
20
1,1,2-Trichloroethane
50.0
53.2
ug/L
106
70-130
2
30
4-Methyl-2-pentanone (MIBK)
250
238
ug/L
95
68-120
1
30
Acetone
250
237
ug/L
95
67 -120
4
30
2-Hexanone
250
260
ug/L
104
70-130
1
20
Ethylene Dibromide
50.0
56.1
ug/L
112
70 -130
0
30
Benzene
50.0
51.9
ug/L
104
70-130
2
30
Bromoform
50.0
57.0
ug/L
114
69 -129
1
30
Bromomethane
50.0
47.9
ug/L
96
28 -192
1
30
Carbon disulfide
50.0
62.9
ug/L
126
70 -130
5
30
1,1,2,2-Tetrachloroethane
50.0
52.6
ug/L
105
70-130
3
30
Carbon tetrachloride
50.0
44.7
ug/L
89
70 -130
1
30
1,3-Dichlorobenzene
50.0
52.3
ug/L
105
70 -130
1
30
Chlorobenzene
50.0
53.5
ug/L
107
70 -130
2
30
1,4-Dichlorobenzene
50.0
52.3
ug/L
105
70 -130
0
30
Chlorodibromomethane
50.0
45.7
ug/L
91
70 -130
2
30
1,2-Dichlorobenzene
50.0
53.8
ug/L
108
70 -130
3
30
Chloroethane
50.0
61.5
ug/L
123
31 - 213
4
30
1,2-Dibromo-3-Chloropropane
50.0
50.5
ug/L
101
70-130
3
30
Chloroform
50.0
53.2
ug/L
106
70 -130
2
30
1,2,4-Trichlorobenzene
50.0
49.5
ug/L
99
70 -130
4
30
Chloromethane
50.0
61.7
ug/L
123
59 -127
1
30
Eurofins Savannah
Page 39 of 81 11/8/2022 (Rev. 1)

QC Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: LCSD 680-748284/6
Matrix: Water
Analysis Batch: 748284
Analyte
cis- 1,2-Dichloroethene
cis-1,3-Dichloropropene
Cyclohexane
Dichlorobromomethane
Ethylbenzene
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
Isopropylbenzene
Methyl acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
Styrene
Tetrachloroethene
Toluene
trans- 1,2-Dichloroethene
trans- 1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Xylenes, Total
LCSD LCSD
Surrogate %Recovery Qualifier
1,2-Dichloroethane-d4 (Surr) 91
4-Bromofluorobenzene (Surr) 95
Dibromofluoromethane (Surr) 113
Toluene-d8 (Surr) 114
Lab Sample ID: MB 680-748517/9
Matrix: Solid
Analysis Batch: 748517
Job ID: 680-223856-1
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
LCSD LCSD
%Rec
RPD
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Limit
50.0
51.1
ug1
102
70 -130
3
30
50.0
50.5
ug/L
101
70 -130
2
20
50.0
54.2
ug/L
108
23 -175
2
30
50.0
50.0
ug/L
100
70 -130
1
30
50.0
53.2
ug/L
106
70 -130
2
20
50.0
51.1
ug/L
102
63 -141
5
30
50.0
56.0
ug/L
112
70-130
2
30
100
92.5
ug/L
92
67-120
2
30
50.0
37.5
ug/L
75
70 -130
0
30
50.0
52.6
ug/L
105
70 -130
1
30
50.0
62.5
ug/L
125
70 -130
1
30
50.0
58.0
ug/L
116
70 -130
1
30
50.0
57.7
ug/L
115
70 -130
2
30
50.0
57.2
ug/L
114
70 -130
0
30
50.0
57.2
ug/L
114
70 -130
0
30
50.0
48.9
ug/L
98
70 -130
1
30
50.0
50.1
ug/L
100
70 -130
1
30
50.0
48.7
ug/L
97
63 -142
5
30
50.0
54.7
ug/L
109
66 -129
1
30
100
107
ug/L
107
70-130
2
30
Limits
60-124
70-130
70-130
70-130
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<1.3
5.0
1.3
ug/Kg
11/03/22 10:20
1
1,1-Dichloroethene
<3.6
5.0
3.6
ug/Kg
11/03/22 10:20
1
1,2,3-Trichlorobenzene
<2.0
5.0
2.0
ug/Kg
11/03/22 10:20
1
1,1-Dichloroethane
<2.9
5.0
2.9
ug/Kg
11/03/22 10:20
1
1,1,1-Trichloroethane
<2.6
5.0
2.6
ug/Kg
11/03/22 10:20
1
1,2-Dichloroethane
<2.3
5.0
2.3
ug/Kg
11/03/22 10:20
1
2-Butanone (MEK)
<9.2
25
9.2
ug/Kg
11/03/22 10:20
1
1,2-Dichloropropane
<2.6
5.0
2.6
ug/Kg
11/03/22 10:20
1
1,1,2-Trichloroethane
<1.5
5.0
1.5
ug/Kg
11/03/22 10:20
1
4-Methyl-2-pentanone (MIBK)
<18
25
18
ug/Kg
11/03/22 10:20
1
Acetone
<11
50
11
ug/Kg
11/03/22 10:20
1
2-Hexanone
<19
25
19
ug/Kg
11/03/22 10:20
1
1,2-Dibromoethane
<1.7
5.0
1.7
ug/Kg
11/03/22 10:20
1
Benzene
<2.4
5.0
2.4
ug/Kg
11/03/22 10:20
1
Bromochloromethane
<2.0
5.0
2.0
ug/Kg
11/03/22 10:20
1
Bromoform
<2.2
5.0
2.2
ug/Kg
11/03/22 10:20
1
Page 40 of 81
Eurofins Savannah
11 /8/2022 (Rev. 1)

QC Sample Results
Client: Environmental Conservation Laboratories
Job ID: 680-223856-1
Project/Site: CF15067
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Lab Sample ID: MB 680-748517/9
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 748517
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Bromomethane
<2.4
5.0
2.4
ug/Kg
11/03/22 10:20
1
Carbon disulfide
<2.1
5.0
2.1
ug/Kg
11/03/22 10:20
1
1,1,2,2-Tetrachloroethane
<2.1
5.0
2.1
ug/Kg
11/03/22 10:20
1
Carbon tetrachloride
<2.1
5.0
2.1
ug/Kg
11/03/22 10:20
1
1,3-Dichlorobenzene
<2.0
5.0
2.0
ug/Kg
11/03/22 10:20
1
Chlorobenzene
<1.4
5.0
1.4
ug/Kg
11/03/22 10:20
1
1,4-Dichlorobenzene
<1.8
5.0
1.8
ug/Kg
11/03/22 10:20
1
Chlorodibromomethane
<2.1
5.0
2.1
ug/Kg
11/03/22 10:20
1
1,2-Dichlorobenzene
<1.7
5.0
1.7
ug/Kg
11/03/22 10:20
1
Chloroethane
<2.2
5.0
2.2
ug/Kg
11/03/22 10:20
1
1,2-Dibromo-3-Chloropropane
<1.6
10
1.6
ug/Kg
11/03/22 10:20
1
Chloroform
<2.0
5.0
2.0
ug/Kg
11/03/22 10:20
1
1,2,4-Trichlorobenzene
<2.5
5.0
2.5
ug/Kg
11/03/22 10:20
1
Chloromethane
<2.4
5.0
2.4
ug/Kg
11/03/22 10:20
1
cis-1,2-Dichloroethene
<2.9
5.0
2.9
ug/Kg
11/03/22 10:20
1
cis-1,3-Dichloropropene
<2.2
5.0
2.2
ug/Kg
11/03/22 10:20
1
Cyclohexane
<2.3
5.0
2.3
ug/Kg
11/03/22 10:20
1
Dichlorobromomethane
<2.0
5.0
2.0
ug/Kg
11/03/22 10:20
1
Dichlorodifluoromethane
<3.2
5.0
3.2
ug/Kg
11/03/22 10:20
1
Ethylbenzene
<2.1
5.0
2.1
ug/Kg
11/03/22 10:20
1
Freon 113
<2.9
5.0
2.9
ug/Kg
11/03/22 10:20
1
Hexachlorobutadiene
<4.1
5.0
4.1
ug/Kg
11/03/22 10:20
1
Isopropylbenzene
<2.2
5.0
2.2
ug/Kg
11/03/22 10:20
1
Methyl acetate
<8.1
25
8.1
ug/Kg
11/03/22 10:20
1
Methyl tert-butyl ether
<2.2
5.0
2.2
ug/Kg
11/03/22 10:20
1
Methylcyclohexane
<2.0
5.0
2.0
ug/Kg
11/03/22 10:20
1
Methylene Chloride
<8.0
10
8.0
ug/Kg
11/03/22 10:20
1
m-Xylene & p-Xylene
<2.2
5.0
2.2
ug/Kg
11/03/22 10:20
1
o-Xylene
<2.3
5.0
2.3
ug/Kg
11/03/22 10:20
1
Styrene
<1.9
5.0
1.9
ug/Kg
11/03/22 10:20
1
Tetrachloroethene
<2.6
5.0
2.6
ug/Kg
11/03/22 10:20
1
Toluene
<2.6
5.0
2.6
ug/Kg
11/03/22 10:20
1
trans- l,2-Dichloroethene
<2.3
5.0
2.3
ug/Kg
11/03/22 10:20
1
trans- 1,3-Dichloropropene
<2.6
5.0
2.6
ug/Kg
11/03/22 10:20
1
Trichloroethene
<1.8
5.0
1.8
ug/Kg
11/03/22 10:20
1
Trichlorofluoromethane
<3.1
5.0
3.1
ug/Kg
11/03/22 10:20
1
Vinyl chloride
<2.8
5.0
2.8
ug/Kg
11/03/22 10:20
1
Xylenes, Total
<3.6
10
3.6
ug/Kg
11/03/22 10:20
1
MB MB
Surrogate %Recovery
Qualifier
Limits
Prepared Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
99
65- 130
11103122 10:20
1
4-Bromofluorobenzene (Surr)
93
65 - 130
11103122 10:20
1
Dibromofluoromethane (Surr)
102
65 - 130
11103122 10:20
1
Toluene-d8 (Surr)
98
65 - 130
11103122 10:20
1
Eurofins Savannah
Page 41 of 81 11/8/2022 (Rev. 1)

QC Sample Results
Client: Environmental Conservation Laboratories
Job ID: 680-223856-1
Project/Site: CF15067
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Lab Sample ID: LCS 680-748517/6
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 748517
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
1,1,1,2-Tetrachloroethane
50.0
51.9
ug/Kg
104
70-130
1,1-Dichloroethene
50.0
61.5
ug/Kg
123
69-130
1,1-Dichloropropene
50.0
58.6
ug/Kg
117
70-130
1,2,3-Trichlorobenzene
50.0
52.9
ug/Kg
106
70-130
1,2,3-Trichloropropane
50.0
51.6
ug/Kg
103
64 -130
1,2,4-Trimethylbenzene
50.0
50.8
ug/Kg
102
70 -130
1,1-Dichloroethane
50.0
56.3
ug/Kg
113
70-130
1,1,1-Trichloroethane
50.0
56.8
ug/Kg
114
70-130
1,3,5-Trimethylbenzene
50.0
50.8
ug/Kg
102
70-130
1,3-Dichloropropane
50.0
57.2
ug/Kg
114
54 -150
1,2-Dichloroethane
50.0
57.5
ug/Kg
115
68 -139
1,4-Dioxane
1000
1060
ug/Kg
106
35-150
2,2-Dichloropropane
50.0
56.2
ug/Kg
112
70 -130
2-Butanone (MEK)
250
274
ug/Kg
110
40 -150
1,2-Dichloropropane
50.0
57.3
ug/Kg
115
70 -130
2-Chlorotoluene
50.0
50.1
ug/Kg
100
70 -130
3-Chloropropene
50.0
62.0
ug/Kg
124
66-134
4-Chlorotoluene
50.0
51.4
ug/Kg
103
70 -130
4-Isopropyltoluene
50.0
50.8
ug/Kg
102
70 -130
1,1,2-Trichloroethane
50.0
54.7
ug/Kg
109
56-146
4-Methyl-2-pentanone (MIBK)
250
273
ug/Kg
109
34 -150
Acetone
250
253
ug/Kg
101
10-150
2-Hexanone
250
271
ug/Kg
108
30-150
Acrolein
1000
1080
ug/Kg
108
27 -150
1,2-Dibromoethane
50.0
57.9
ug/Kg
116
48-150
Acrylonitrile
500
560
ug/Kg
112
50 -150
Benzene
50.0
58.1
ug/Kg
116
70-130
Bromobenzene
50.0
52.0
ug/Kg
104
70 -130
Bromochloromethane
50.0
59.1
ug/Kg
118
66 -130
Bromoform
50.0
50.5
ug/Kg
101
68 -130
Bromomethane
50.0
59.8
ug/Kg
120
70 -130
Carbon disulfide
50.0
71.7 "+
ug/Kg
143
70 -130
1,1,2,2-Tetrachloroethane
50.0
50.5
ug/Kg
101
64-130
Carbon tetrachloride
50.0
57.5
ug/Kg
115
70 -130
1,3-Dichlorobenzene
50.0
53.0
ug/Kg
106
70 -130
Chlorobenzene
50.0
51.1
ug/Kg
102
70 -130
1,4-Dichlorobenzene
50.0
52.5
ug/Kg
105
70 -130
Chlorodibromomethane
50.0
56.4
ug/Kg
113
64 -133
1,2-Dichlorobenzene
50.0
53.0
ug/Kg
106
70 -130
Chloroethane
50.0
57.9
ug/Kg
116
70 -130
1,2-Dibromo-3-Chloropropane
50.0
48.7
ug/Kg
97
42 -145
Chloroform
50.0
55.3
ug/Kg
111
70 -130
1,2,4-Trichlorobenzene
50.0
53.3
ug/Kg
107
70 -130
Chloromethane
50.0
56.7
ug/Kg
113
70 -130
cis-1,2-Dichloroethene
50.0
56.8
ug/Kg
114
70 -130
cis-1,3-Dichloropropene
50.0
55.2
ug/Kg
110
70 -130
Cyclohexane
50.0
61.6
ug/Kg
123
70 -130
Dibromomethane
50.0
59.7
ug/Kg
119
59 -142
Eurofins Savannah
Page 42 of 81 11/8/2022 (Rev. 1)

QC Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: LCS 680-748517/6
Matrix: Solid
Analysis Batch: 748517
Job ID: 680-223856-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS
LCS
%Rec
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits
Dichlorobromomethane
50.0
54.8
ug/Kg
110
70 -130
Dichlorodifluoromethane
50.0
58.0
ug/Kg
116
43 -131
Ethyl methacrylate
50.0
55.6
ug/Kg
ill
40 -150
Ethylbenzene
50.0
51.0
ug/Kg
102
70 -130
Freon 113
50.0
60.7
ug/Kg
121
70 -130
Hexachlorobutadiene
50.0
55.6
ug/Kg
111
70 -130
lodomethane
50.0
56.0
ug/Kg
112
65 -138
Isobutyl alcohol
1250
1230
ug/Kg
99
14 -150
Isopropylbenzene
50.0
51.3
ug/Kg
103
70 -130
Methyl acetate
100
127
ug/Kg
127
22 -150
Methyl tert-butyl ether
50.0
57.7
ug/Kg
115
70 -130
Methylcyclohexane
50.0
58.6
,+
ug/Kg
117
69 -110
Methylene Chloride
50.0
59.3
ug/Kg
119
54 -149
m-Xylene & p-Xylene
50.0
51.0
ug/Kg
102
70 -130
Naphthalene
50.0
51.7
ug/Kg
103
46 -150
n-Butylbenzene
50.0
51.1
ug/Kg
102
70 -130
N-Propylbenzene
50.0
50.8
ug/Kg
102
70-130
o-Xylene
50.0
50.3
ug/Kg
101
70 -130
sec- Butylbenzene
50.0
50.6
ug/Kg
101
69 -142
Styrene
50.0
52.0
ug/Kg
104
70 -130
tert-Butylbenzene
50.0
50.6
ug/Kg
101
67 -145
Tetrachloroethene
50.0
58.9
ug/Kg
118
70 -130
Tetrahydrofuran
100
102
ug/Kg
102
15 -150
Toluene
50.0
57.4
ug/Kg
115
70 -130
trans- 1,2-Dichloroethene
50.0
57.7
ug/Kg
115
67-130
trans- 1,3-Dichloropropene
50.0
56.7
ug/Kg
113
54 -150
trans- 1,4-Dichloro-2-butene
50.0
51.9
ug/Kg
104
54 -150
Trichloroethene
50.0
57.0
ug/Kg
114
70 -130
Trichlorofluoromethane
50.0
60.5
ug/Kg
121
70 -130
Vinyl acetate
100
101
ug/Kg
101
53 -150
Vinyl chloride
50.0
58.6
ug/Kg
117
70 -130
Xylenes, Total
100
101
ug/Kg
101
70 -130
LCS LCS
Surrogate
%Recovery Qualifier
Limits
1,2-Dichloroethane-d4 (Surr)
118
65- 130
4-Bromofluorobenzene (Surr)
107
65 - 130
Dibromofluoromethane (Surr)
115
65 - 130
Toluene-d8 (Surr)
102
65 - 130
Lab Sample ID: LCSD 680-748517/7
Client Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 748517
Spike
LCSD
LCSD
%Rec RPD
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits RPD Limit
1,1,1,2-Tetrachloroethane
50.0
52.7
ug/Kg
105
70-130 2 30
1,1-Dichloroethene
50.0
61.4
ug/Kg
123
69-130 0 50
1,1-Dichloropropene
50.0
56.8
ug/Kg
114
70-130 3 30
1,2,3-Trichlorobenzene
50.0
54.2
ug/Kg
108
70-130 2 30
Eurofins Savannah
Page 43 of 81 11/8/2022 (Rev. 1)

QC Sample Results
Client: Environmental Conservation Laboratories
Job ID:
680-223856-1
Project/Site: CF15067
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Lab Sample ID: LCSD 680-748517/7
Client Sample ID: Lab Control
Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 748517
Spike
LCSD
LCSD
%Rec
RPD
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
RPD
Limit
1,2,3-Trichloropropane
50.0
53.2
ug/Kg
106
64 -130
3
30
1,2,4-Trimethylbenzene
50.0
48.5
ug/Kg
97
70 -130
5
30
1,1-Dichloroethane
50.0
57.8
ug/Kg
116
70-130
3
30
1,1,1-Trichloroethane
50.0
55.9
ug/Kg
112
70-130
2
30
1,3,5-Trimethylbenzene
50.0
48.7
ug/Kg
97
70-130
4
30
1,3-Dichloropropane
50.0
59.3
ug/Kg
119
54 -150
4
30
1,2-Dichloroethane
50.0
60.0
ug/Kg
120
68 -139
4
30
1,4-Dioxane
1000
1140
ug/Kg
114
35-150
7
30
2,2-Dichloropropane
50.0
56.5
ug/Kg
113
70 -130
1
30
2-Butanone (MEK)
250
291
ug/Kg
116
40 -150
6
30
1,2-Dichloropropane
50.0
58.2
ug/Kg
116
70 -130
2
30
2-Chlorotoluene
50.0
48.1
ug/Kg
96
70 -130
4
30
3-Chloropropene
50.0
61.0
ug/Kg
122
66-134
2
30
4-Chlorotoluene
50.0
50.3
ug/Kg
101
70 -130
2
30
4-Isopropyltoluene
50.0
49.5
ug/Kg
99
70 -130
3
30
1,1,2-Trichloroethane
50.0
57.1
ug/Kg
114
56-146
4
30
4-Methyl-2-pentanone (MIBK)
250
294
ug/Kg
118
34 -150
7
30
Acetone
250
267
ug/Kg
107
10-150
5
50
2-Hexanone
250
288
ug/Kg
115
30-150
6
30
Acrolein
1000
1150
ug/Kg
115
27 -150
6
30
1,2-Dibromoethane
50.0
60.3
ug/Kg
121
48-150
4
30
Acrylonitrile
500
597
ug/Kg
119
50 -150
7
30
Benzene
50.0
58.8
ug/Kg
118
70-130
1
30
Bromobenzene
50.0
51.7
ug/Kg
103
70-130
1
30
Bromochloromethane
50.0
62.4
ug/Kg
125
66 -130
5
30
Bromoform
50.0
52.1
ug/Kg
104
68 -130
3
30
Bromomethane
50.0
61.8
ug/Kg
124
70 -130
3
30
Carbon disulfide
50.0
71.5
'+ ug/Kg
143
70 -130
0
30
1,1,2,2-Tetrachloroethane
50.0
52.6
ug/Kg
105
64-130
4
30
Carbon tetrachloride
50.0
57.0
ug/Kg
114
70 -130
1
30
1,3-Dichlorobenzene
50.0
53.9
ug/Kg
108
70 -130
2
30
Chlorobenzene
50.0
51.0
ug/Kg
102
70 -130
0
30
1,4-Dichlorobenzene
50.0
53.4
ug/Kg
107
70 -130
2
30
Chlorodibromomethane
50.0
57.9
ug/Kg
116
64 -133
3
30
1,2-Dichlorobenzene
50.0
54.6
ug/Kg
109
70 -130
3
30
Chloroethane
50.0
59.9
ug/Kg
120
70 -130
3
30
1,2-Dibromo-3-Chloropropane
50.0
53.8
ug/Kg
108
42 -145
10
30
Chloroform
50.0
57.2
ug/Kg
114
70 -130
3
30
1,2,4-Trichlorobenzene
50.0
54.7
ug/Kg
109
70 -130
3
30
Chloromethane
50.0
59.5
ug/Kg
119
70 -130
5
30
cis-1,2-Dichloroethene
50.0
58.6
ug/Kg
117
70 -130
3
30
cis-1,3-Dichloropropene
50.0
56.6
ug/Kg
113
70 -130
2
30
Cyclohexane
50.0
60.3
ug/Kg
121
70 -130
2
30
Dibromomethane
50.0
61.8
ug/Kg
124
59 -142
4
30
Dichlorobromomethane
50.0
56.9
ug/Kg
114
70 -130
4
30
Dichlorodifluoromethane
50.0
60.1
ug/Kg
120
43 -131
4
30
Ethyl methacrylate
50.0
58.7
ug/Kg
117
40 -150
5
30
Ethylbenzene
50.0
49.6
ug/Kg
99
70 -130
3
30
Freon 113
50.0
60.3
ug/Kg
121
70 -130
1
40
Eurofins Savannah
Page 44 of 81 11/8/2022 (Rev. 1)

QC Sample Results
Client: Environmental Conservation Laboratories
Job ID: 680-223856-1
Project/Site: CF15067
Method: 8260D - Volatile Organic Compounds by
GUMS (Continued)
Lab Sample ID: LCSD 680-748517/7
Client Sample ID: Lab Control Sample
Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 748517
Spike
LCSD
LCSD
%Rec
RPD
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits RPD
Limit
Hexachlorobutadiene
50.0
52.6
ug/Kg
105
70 -130
6 30
lodomethane
50.0
57.6
ug/Kg
115
65 -138
3 30
Isobutyl alcohol
1250
1340
ug/Kg
107
14 -150
8 30
Isopropylbenzene
50.0
49.3
ug/Kg
99
70 -130
4 30
Methyl acetate
100
134
ug/Kg
134
22 -150
6 30
Methyl tert-butyl ether
50.0
61.2
ug/Kg
122
70 -130
6 30
Methyl cyclohexane
50.0
58.0
"+
ug/Kg
116
69 -110
1 30
Methylene Chloride
50.0
61.2
ug/Kg
122
54 -149
3 30
m-Xylene & p-Xylene
50.0
49.7
ug/Kg
99
70 -130
3 30
Naphthalene
50.0
55.8
ug/Kg
112
46 -150
8 30
n-Butylbenzene
50.0
48.3
ug/Kg
97
70 -130
6 30
N-Propylbenzene
50.0
48.4
ug/Kg
97
70 -130
5 30
o-Xylene
50.0
49.7
ug/Kg
99
70 -130
1 30
sec-Butylbenzene
50.0
47.3
ug/Kg
95
69 -142
7 30
Styrene
50.0
51.3
ug/Kg
103
70 -130
1 30
tert-Butylbenzene
50.0
48.2
ug/Kg
96
67 -145
5 30
Tetrachloroethene
50.0
56.9
ug/Kg
114
70 -130
4 30
Tetrahydrofuran
100
109
ug/Kg
109
15 -150
7 30
Toluene
50.0
57.3
ug/Kg
115
70 -130
0 30
trans- 1,2-Dichloroethene
50.0
59.8
ug/Kg
120
67-130
4 30
trans- 1,3-Dichloropropene
50.0
58.7
ug/Kg
117
54 -150
3 30
trans- 1,4-Dichloro-2-butene
50.0
53.2
ug/Kg
106
54 -150
2 30
Trichloroethene
50.0
57.2
ug/Kg
114
70 -130
0 30
Trichlorofluoromethane
50.0
63.4
ug/Kg
127
70 -130
5 30
Vinyl acetate
100
106
ug/Kg
106
53 -150
5 30
Vinyl chloride
50.0
61.1
ug/Kg
122
70 -130
4 30
Xylenes, Total
100
99.4
ug/Kg
99
70 -130
2 30
LCSD LCSD
Surrogate %Recovery Qualifier
Limits
1, 2-Dichloroethane-d4 (Surr) 123
65 -130
4-Bromofluorobenzene (Surr) 109
65 -130
Dibromofluoromethane (Surr) 119
65 -130
Toluene-d8 (Surr) 101
65 - 130
Lab Sample ID: MB 680-748537/9
Client Sample ID: Method
Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 748537
MB MB
Analyte Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
1,1-Dichloroethene <0.33
1.0
0.33
ug/L
11/03/22 15:36
1
1,1-Dichloroethane <0.33
1.0
0.33
ug/L
11/03/22 15:36
1
1,1,1-Trichloroethane <0.21
1.0
0.21
ug/L
11/03/22 15:36
1
1,2-Dichloroethane <0.25
1.0
0.25
ug/L
11/03/22 15:36
1
2-Butanone (MEK) <6.4
10
6.4
ug/L
11/03/22 15:36
1
1,2-Dichloropropane <0.22
1.0
0.22
ug/L
11/03/22 15:36
1
1,1,2-Trichloroethane <0.32
1.0
0.32
ug/L
11/03/22 15:36
1
4-Methyl-2-pentanone (MIBK) <2.7
10
2.7
ug/L
11/03/22 15:36
1
Acetone 20.8
10
3.7
ug/L
11/03/22 15:36
1
Eurofins Savannah
Page 45 of 81 11/8/2022 (Rev. 1)

QC Sample Results
Client: Environmental Conservation Laboratories
Job ID: 680-223856-1
Project/Site: CF15067
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Lab Sample ID: MB 680-748537/9
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 748537
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
2-Hexanone
<3.2
10
3.2
ug/L
11/03/22 15:36
1
Ethylene Dibromide
<0.33
1.0
0.33
ug/L
11/03/22 15:36
1
Benzene
<0.27
1.0
0.27
ug/L
11/03/22 15:36
1
Bromoform
<0.59
1.0
0.59
ug/L
11/03/22 15:36
1
Bromomethane
<3.7
5.0
3.7
ug/L
11/03/22 15:36
1
Carbon disulfide
<0.43
2.0
0.43
ug/L
11/03/22 15:36
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.40
ug/L
11/03/22 15:36
1
Carbon tetrachloride
<0.30
1.0
0.30
ug/L
11/03/22 15:36
1
1,3-Dichlorobenzene
<0.31
1.0
0.31
ug/L
11/03/22 15:36
1
Chlorobenzene
<0.15
1.0
0.15
ug/L
11/03/22 15:36
1
1,4-Dichlorobenzene
<0.31
1.0
0.31
ug/L
11/03/22 15:36
1
Chlorodibromomethane
<0.39
1.0
0.39
ug/L
11/03/22 15:36
1
1,2-Dichlorobenzene
<0.31
1.0
0.31
ug/L
11/03/22 15:36
1
Chloroethane
<4.6
5.0
4.6
ug/L
11/03/22 15:36
1
1,2-Dibromo-3-Chloropropane
<1.8
5.0
1.8
ug/L
11/03/22 15:36
1
Chloroform
<0.27
1.0
0.27
ug/L
11/03/22 15:36
1
1,2,4-Trichlorobenzene
<0.53
5.0
0.53
ug/L
11/03/22 15:36
1
Chloromethane
<0.54
1.0
0.54
ug/L
11/03/22 15:36
1
cis-1,2-Dichloroethene
<0.25
1.0
0.25
ug/L
11/03/22 15:36
1
cis-1,3-Dichloropropene
<0.26
1.0
0.26
ug/L
11/03/22 15:36
1
Cyclohexane
<0.28
1.0
0.28
ug/L
11/03/22 15:36
1
Dichlorobromomethane
<0.25
1.0
0.25
ug/L
11/03/22 15:36
1
Ethylbenzene
<0.20
1.0
0.20
ug/L
11/03/22 15:36
1
1,1,2-Trichloro-1,2,2-trifluoroethane
<0.23
1.0
0.23
ug/L
11/03/22 15:36
1
Isopropylbenzene
<0.26
1.0
0.26
ug/L
11/03/22 15:36
1
Methyl acetate
<3.2
5.0
3.2
ug/L
11/03/22 15:36
1
Methyl tert-butyl ether
<0.81
5.0
0.81
ug/L
11/03/22 15:36
1
Methylcyclohexane
<0.33
1.0
0.33
ug/L
11/03/22 15:36
1
Methylene Chloride
<3.2
5.0
3.2
ug/L
11/03/22 15:36
1
Styrene
0.450 J
1.0
0.27
ug/L
11/03/22 15:36
1
Tetrachloroethene
<0.35
0.50
0.35
ug/L
11/03/22 15:36
1
Toluene
<0.25
1.0
0.25
ug/L
11/03/22 15:36
1
trans- l,2-Dichloroethene
<0.34
1.0
0.34
ug/L
11/03/22 15:36
1
trans- 1,3-Dichloropropene
<0.23
1.0
0.23
ug/L
11/03/22 15:36
1
Trichloroethene
<0.20
1.0
0.20
ug/L
11/03/22 15:36
1
Trichlorofluoromethane
<0.33
1.0
0.33
ug/L
11/03/22 15:36
1
Vinyl chloride
<0.40
1.0
0.40
ug/L
11/03/22 15:36
1
Xylenes, Total
<0.23
1.0
0.23
ug/L
11/03/22 15:36
1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
108
60- 124
11103122 15:36
1
4-Bromofluorobenzene (Surr)
99
70 - 130
11103122 15:36
1
Dibromofluoromethane (Surr)
117
70 - 130
11103122 15:36
1
Toluene-d8 (Surr)
109
70 - 130
11103122 15:36
1
Eurofins Savannah
Page 46 of 81 11/8/2022 (Rev. 1)

QC Sample Results
Client: Environmental Conservation Laboratories
Job ID: 680-223856-1
Project/Site: CF15067
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Lab Sample ID: LCS 680-748537/5
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 748537
Spike
LCS LCS
%Rec
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
1,1-Dichloroethene
50.0
58.1
ug/L
116
70-130
1,1-Dichloroethane
50.0
55.5
ug/L
111
70-130
1,1,1-Trichloroethane
50.0
63.9
ug/L
128
70-130
1,2-Dichloroethane
50.0
51.5
ug/L
103
70 -130
2-Butanone (MEK)
250
286
ug/L
114
69 -120
1,2-Dichloropropane
50.0
47.0
ug/L
94
70 -130
1,1,2-Trichloroethane
50.0
52.3
ug/L
105
70-130
4-Methyl-2-pentanone (MIBK)
250
293
ug/L
117
68-120
Acetone
250
259
ug/L
104
67-120
2-Hexanone
250
299
ug/L
120
70-130
Ethylene Dibromide
50.0
61.3
ug/L
123
70 -130
Benzene
50.0
50.4
ug/L
101
70-130
Bromoform
50.0
56.4
ug/L
113
69 -129
Bromomethane
50.0
71.8
ug/L
144
28 -192
Carbon disulfide
50.0
55.2
ug/L
110
70 -130
1,1,2,2-Tetrachloroethane
50.0
48.5
ug/L
97
70-130
Carbon tetrachloride
50.0
56.3
ug/L
113
70 -130
1,3-Dichlorobenzene
50.0
52.4
ug/L
105
70 -130
Chlorobenzene
50.0
52.2
ug/L
104
70 -130
1,4-Dichlorobenzene
50.0
50.2
ug/L
100
70 -130
Chlorodibromomethane
50.0
57.0
ug/L
114
70 -130
1,2-Dichlorobenzene
50.0
50.2
ug/L
100
70 -130
Chloroethane
50.0
55.9
ug/L
112
31 - 213
1,2-Dibromo-3-Chloropropane
50.0
69.8 '+
ug/L
140
70-130
Chloroform
50.0
57.3
ug/L
115
70 -130
1,2,4-Trichlorobenzene
50.0
57.0
ug/L
114
70 -130
Chloromethane
50.0
42.3
ug/L
85
59 -127
cis-1,2-Dichloroethene
50.0
55.0
ug/L
110
70 -130
cis-1,3-Dichloropropene
50.0
58.8
ug/L
118
70 -130
Cyclohexane
50.0
50.8
ug/L
102
23 -175
Dichlorobromomethane
50.0
62.2
ug/L
124
70 -130
Ethylbenzene
50.0
52.4
ug/L
105
70 -130
1,1,2-Trichloro-1,2,2-trifluoroetha
50.0
54.3
ug/L
109
63-141
ne
Isopropylbenzene
50.0
55.8
ug/L
112
70 -130
Methyl acetate
100
110
ug/L
110
67 -120
Methyl tert-butyl ether
50.0
60.2
ug/L
120
70 -130
Methylcyclohexane
50.0
52.0
ug/L
104
70 -130
Methylene Chloride
50.0
50.7
ug/L
101
70 -130
Styrene
50.0
54.0
ug/L
108
70 -130
Tetrachloroethene
50.0
53.1
ug/L
106
70 -130
Toluene
50.0
49.8
ug/L
100
70 -130
trans- 1,2-Dichloroethene
50.0
50.8
ug/L
102
70-130
trans- 1,3-Dichloropropene
50.0
51.9
ug/L
104
70-130
Trichloroethene
50.0
57.9
ug/L
116
70 -130
Trichlorofluoromethane
50.0
84.1+
ug/L
168
63 -142
Vinyl chloride
50.0
49.6
ug/L
99
66 -129
Xylenes, Total
100
106
ug/L
106
70 -130
Eurofins Savannah
Page 47 of 81 11/8/2022 (Rev. 1)

QC Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: LCS 680-748537/5
Matrix: Water
Analysis Batch: 748537
LCS LCS
Surrogate %Recovery Qualifier
1,2-Dichloroethane-d4 (Surr) 117
4-Bromofluorobenzene (Surr) 99
Dibromofluoromethane (Surr) 117
Toluene-d8 (Surr) 115
Lab Sample ID: LCSD 680-74853716
Matrix: Water
Analysis Batch: 748537
Analyte
1,1-Dichloroethene
1,1-Dichloroethane
1,1,1-Trichloroethane
1,2-Dichloroethane
2-Butanone (MEK)
1,2-Dichloropropane
1,1,2-Trichloroethane
4-Methyl-2-pentanone (MIBK)
Acetone
2-Hexanone
Ethylene Dibromide
Benzene
Bromoform
Bromomethane
Carbon disulfide
1,1,2,2-Tetrachloroethane
Carbon tetrachloride
1,3-Dichlorobenzene
Chlorobenzene
1,4-Dichlorobenzene
Chlorodibromomethane
1,2-Dichlorobenzene
Chloroethane
1,2-Dibromo-3-Chloropropane
Chloroform
1,2,4-Trichlorobenzene
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Cyclohexane
Dichlorobromomethane
Ethylbenzene
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
Isopropylbenzene
Methyl acetate
Methyl tert-butyl ether
Methylcyclohexane
Methylene Chloride
Limits
60 - 124
70 - 130
70 - 130
70-130
Job ID: 680-223856-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
LCSD
LCSD
%Rec
RPD
Added
Result
Qualifier
Unit
D %Rec
Limits
RPD
Limit
50.0
58.7
ug/L
117
70 -130
1
20
50.0
56.3
ug/L
113
70 -130
1
30
50.0
62.7
ug/L
125
70 -130
2
30
50.0
52.4
ug/L
105
70 -130
2
50
250
288
ug/L
115
69-120
1
30
50.0
48.7
ug/L
97
70 -130
4
20
50.0
54.0
ug/L
108
70 -130
3
30
250
298
ug/L
119
68-120
2
30
250
302
"+
ug/L
121
67-120
15
30
250
299
ug/L
120
70-130
0
20
50.0
59.1
ug/L
118
70 -130
4
30
50.0
50.9
ug/L
102
70 -130
1
30
50.0
53.0
ug/L
106
69 -129
6
30
50.0
70.6
ug/L
141
28 -192
2
30
50.0
54.5
ug/L
109
70 -130
1
30
50.0
45.8
ug/L
92
70 -130
6
30
50.0
56.9
ug/L
114
70 -130
1
30
50.0
51.4
ug/L
103
70 -130
2
30
50.0
50.6
ug/L
101
70 -130
3
30
50.0
50.6
ug/L
101
70 -130
1
30
50.0
56.5
ug/L
113
70 -130
1
30
50.0
50.0
ug/L
100
70 -130
0
30
50.0
51.2
ug/L
102
31 - 213
9
30
50.0
71.3
.+
ug/L
143
70 -130
2
30
50.0
59.5
ug/L
119
70 -130
4
30
50.0
54.8
ug/L
110
70 -130
4
30
50.0
41.0
ug/L
82
59 -127
3
30
50.0
53.2
ug/L
106
70 -130
3
30
50.0
59.7
ug/L
119
70 -130
2
20
50.0
51.8
ug/L
104
23-175
2
30
50.0
63.4
ug/L
127
70 -130
2
30
50.0
50.2
ug/L
100
70 -130
4
20
50.0
54.5
ug/L
109
63 -141
0
30
50.0
53.5
ug/L
107
70 -130
4
30
100
109
ug/L
109
67-120
1
30
50.0
59.5
ug/L
119
70 -130
1
30
50.0
51.5
ug/L
103
70 -130
1
30
50.0
52.5
ug/L
105
70 -130
4
30
Page 48 of 81
Eurofins Savannah
11 /8/2022 (Rev. 1)

QC Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Lab Sample ID: LCSD 680-748537/6 Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 748537
RPD
Limit
Spike
LCSD LCSD
%Rec
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Styrene
50.0
52.5
ug/L
105
70-130
3
Tetrachloroethene
50.0
50.9
ug/L
102
70 -130
4
Toluene
50.0
51.9
ug/L
104
70 -130
4
trans- 1,2-Dichloroethene
50.0
51.4
ug/L
103
70 -130
1
trans- 1,3-Dichloropropene
50.0
50.6
ug/L
101
70-130
3
Trichloroethene
50.0
60.4
ug/L
121
70-130
4
Trichlorofluoromethane
50.0
84.9 .+
ug/L
170
63-142
1
Vinyl chloride
50.0
50.0
ug/L
100
66-129
1
Xylenes, Total
100
98.9
ug/L
99
70 -130
7
LCSD LCSD
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) ill 60-124
4-Bromofluorobenzene (Surr) 101 70 -130
Dibromofluoromethane (Surr) 116 70-130
Toluene-d8 (Surr) 113 70-130
30
30
30
30
30
30
30
30
30
Method: 8270E SIM ID - Semivolatile Organic Compounds (GC/MS SIM / Isotope Dilution)
Lab Sample ID: MB 680-747919/18-A Client Sample ID: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 748005 Prep Batch: 747919
MB MB
Analyte Result Qualifier
1,4-Dioxane <3.9
MB MB
Isotope Dilution %Recovery Qualifier
1,4-Dioxane-d8 61
Lab Sample ID: LCS 680-747919/19-A
Matrix: Solid
Analysis Batch: 748005
Analyte
1,4-Dioxane
LCS LCS
Isotope Dilution %Recovery Qualifier
1,4-Dioxane-d8 63
FLab Sample ID: 680-223856-1 MS
Matrix: Solid
Analysis Batch: 748005
Analyte
Sample Sample
Result Qualifier
1,4-Dioxane
<4.1
MS MS
Isotope Dilution
%Recovery Qualifier
1,4-Dioxane-d8
53
RL MDL Unit D Prepared Analyzed Dil Fac
32 3.9 ug/Kg 10/31/2212:25 11/01/2215:47 1
Limits Prepared Analyzed Dil Fac
10- 150 10131122 12:25 11101122 15:47 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 747919
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
164 167 ug/Kg 102 70-130
Limits
10-150
Spike MS MS
Added Result Qualifier Unit
167 157 ug/Kg
Limits
10 - 150
Client Sample ID: SS-1
Prep Type: Total/NA
Prep Batch: 747919
%Rec
D %Rec Limits
94
Page 49 of 81
Eurofins Savannah
11/8/2022 (Rev. 1)

QC Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
F
Job ID: 680-223856-1
Method: 8270E SIM ID - Semivolatile Organic Compounds (GC/MS SIM / Isotope Dilution)
(Continued)
Lab Sample ID: 680-223856-1 MSD Client Sample ID: SS-1
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 748005 Prep Batch: 747919
Sample Sample Spike MSD MSD %Rec RPD
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit
1,4-Dioxane <4.1 173 174 ug/Kg r 101 10
MSD MSD
Isotope Dilution %Recovery Qualifier
1,4-Dioxane-d8 39
Method: 9056A - Anions, Ion Chromatogre
Lab Sample ID: MB 680-748171/1-A
Matrix: Solid
Analysis Batch: 748340
MB MB
Analyte Result Qualifier
Sulfate <8.0
Lab Sample ID: LCS 680-748171/2-A
Matrix: Solid
Analysis Batch: 748340
Analyte
Sulfate
Lab Sample ID: LCSD 680-748171/3-A
Matrix: Solid
Analysis Batch: 748340
Analyte
Sulfate
FLab Sample ID: 680-223856-1 MS
Matrix: Solid
Analysis Batch: 748340
Sample Sample
Analyte Result Qualifier
Sulfate 130
FLab Sample ID: 680-223856-1 MSD
Matrix: Solid
Analysis Batch: 748340
Sample Sample
Analyte Result Qualifier
Sulfate 130
Lab Sample ID: 680-223856-10 MS
Matrix: Solid
Analysis Batch: 748340
Sample Sample
Analyte Result Qualifier
Sulfate <8.8 F1
Limits
10-150
)hy
Client Sample ID: Method Blank
Prep Type: Soluble
RL MDL Unit D Prepared Analyzed Dil Fac
20 8.0 mg/Kg 11/02/2213:42 1
Client Sample ID: Lab Control Sample
Prep Type: Soluble
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
99.7 87.7 mg/Kg 88 75 -125
Client Sample ID: Lab Control Sample Dup
Prep Type: Soluble
Spike LCSD LCSD %Rec RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
99.6 85.1 mg/Kg 85 75 -125 3 15
Client Sample ID: SS-1
Prep Type: Soluble
Spike MS MS %Rec
Added Result Qualifier Unit D %Rec Limits
104 247 mg/Kg 109 75-125
Client Sample ID: SS-1
Prep Type: Soluble
Spike MSD MSD %Rec RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
105 245 mg/Kg 106 75-125 1 15
Client Sample ID: DUP-01
Prep Type: Soluble
Spike MS MS %Rec
Added Result Qualifier Unit D %Rec Limits
ill 31.6 F1 mg/Kg 28 75 - 125
Page 50 of 81
Eurofins Savannah
11/8/2022 (Rev. 1)

QC Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Method: 9056A - Anions, Ion Chromatography (Continued)
Lab Sample ID: 680-223856-10 MSD
Matrix: Solid
Analysis Batch: 748340
Sample Sample Spike MSD MSD
Analyte Result Qualifier Added Result Qualifier Unit
Sulfate <8.8 F1 110 34.2 F1 mg/Kg
Method: 6010D - Metals (ICP)
Lab Sample ID: MB 680-746580/1-A
Matrix: Solid
Analysis Batch: 747234
MB MB
Analyte
Result Qualifier
Silver
<0.26
Arsenic
<0.98
Barium
<0.34
Cadmium
<0.082
Lead
<0.50
Selenium
<0.90
Antimony
<0.71
Beryllium
<0.058
Thallium
<0.64
Nickel
<0.74
Vanadium
<0.13
Copper
<0.41
Zinc
<0.48
Cobalt
<0.27
Lab Sample ID: LCS 680-746580/2-A
Matrix: Solid
Analysis Batch: 747234
Analyte
Silver
Arsenic
Barium
Cadmium
Lead
Selenium
Antimony
Beryllium
Thallium
Nickel
Vanadium
Copper
Zinc
Cobalt
Job ID: 680-223856-1
Client Sample ID: DUP-01
Prep Type: Soluble
%Rec RPD C
D %Rec Limits RPD Limit
3:31 75-125 8 15
0
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 746580 F
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
0.82
0.26
mg/Kg
10/24/22 09:55
10/26/22 19:57
1
1.6
0.98
mg/Kg
10/24/22 09:55
10/26/22 19:57
1
0.82
0.34
mg/Kg
10/24/22 09:55
10/26/22 19:57
1
0.41
0.082
mg/Kg
10/24/22 09:55
10/26/22 19:57
1
0.82
0.50
mg/Kg
10/24/22 09:55
10/26/22 19:57
1
2.0
0.90
mg/Kg
10/24/22 09:55
10/26/22 19:57
1
1.6
0.71
mg/Kg
10/24/22 09:55
10/26/22 19:57
1
0.33
0.058
mg/Kg
10/24/22 09:55
10/26/22 19:57
1
2.0
0.64
mg/Kg
10/24/22 09:55
10/26/22 19:57
1
3.3
0.74
mg/Kg
10/24/22 09:55
10/26/22 19:57
1
0.82
0.13
mg/Kg
10/24/22 09:55
10/26/22 19:57
1
2.0
0.41
mg/Kg
10/24/22 09:55
10/26/22 19:57
1
1.6
0.48
mg/Kg
10/24/22 09:55
10/26/22 19:57
1
0.82
0.27
mg/Kg
10/24/22 09:55
10/26/22 19:57
1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 746580
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec
Limits
4.81
4.80
mg/Kg
100
80 -120
9.62
9.65
mg/Kg
100
80 -120
9.62
9.98
mg/Kg
104
80 -120
4.81
4.95
mg/Kg
103
80 -120
48.5
48.1
mg/Kg
99
80 -120
9.63
8.98
mg/Kg
93
80 -120
4.80
5.09
mg/Kg
106
80 -120
4.81
4.93
mg/Kg
102
80 -120
4.81
4.98
mg/Kg
104
80 -120
9.52
10.0
mg/Kg
105
80 -120
9.60
9.65
mg/Kg
101
80 -120
9.62
10.8
mg/Kg
112
80 -120
9.62
9.67
mg/Kg
101
80 -120
4.80
5.04
mg/Kg
105
80 -120
Page 51 of 81
Eurofins Savannah
11 /8/2022 (Rev. 1)

QC Sample Results
Client: Environmental Conservation Laboratories
Job ID: 680-223856-1
Project/Site: CF15067
Method: 6010D - Metals
(ICP) (Continued)
Lab Sample ID: MB 680-746778/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 747484
Prep Batch: 746778
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Silver
<0.30
0.94
0.30
mg/Kg
10/25/22 08:20
10/27/22 21:59 1
Arsenic
<1.1
1.9
1.1
mg/Kg
10/25/22 08:20
10/27/22 21:59 1
Barium
<0.39
0.94
0.39
mg/Kg
10/25/22 08:20
10/27/22 21:59 1
Cadmium
<0.094
0.47
0.094
mg/Kg
10/25/22 08:20
10/27/22 21:59 1
Lead
<0.58
0.94
0.58
mg/Kg
10/25/22 08:20
10/27/22 21:59 1
Selenium
<1.0
2.4
1.0
mg/Kg
10/25/22 08:20
10/27/22 21:59 1
Antimony
<0.82
1.9
0.82
mg/Kg
10/25/22 08:20
10/27/22 21:59 1
Beryllium
<0.067
0.38
0.067
mg/Kg
10/25/22 08:20
10/27/22 21:59 1
Thallium
<0.74
2.4
0.74
mg/Kg
10/25/22 08:20
10/27/22 21:59 1
Nickel
<0.85
3.8
0.85
mg/Kg
10/25/22 08:20
10/27/22 21:59 1
Vanadium
<0.15
0.94
0.15
mg/Kg
10/25/22 08:20
10/27/22 21:59 1
Copper
<0.47
2.4
0.47
mg/Kg
10/25/22 08:20
10/27/22 21:59 1
Zinc
<0.55
1.9
0.55
mg/Kg
10/25/22 08:20
10/27/22 21:59 1
Cobalt
<0.31
0.94
0.31
mg/Kg
10/25/22 08:20
10/27/22 21:59 1
Lab Sample ID: LCS 680-746778/2-A
Client Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 747484
Prep Batch: 746778
Spike
LCS
LCS
%Rec
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits
Silver
4.24
4.07
mg/Kg
96
80 -120
Arsenic
8.47
7.90
mg/Kg
93
80 -120
Barium
8.47
8.50
mg/Kg
100
80-120
Cadmium
4.24
4.14
mg/Kg
98
80 -120
Lead
42.8
40.6
mg/Kg
95
80 -120
Selenium
8.49
7.18
mg/Kg
85
80 -120
Antimony
4.23
3.99
mg/Kg
94
80 -120
Beryllium
4.24
4.21
mg/Kg
99
80 -120
Thallium
4.24
3.98
mg/Kg
94
80-120
Nickel
8.39
8.43
mg/Kg
101
80 -120
Vanadium
8.46
8.28
mg/Kg
98
80 -120
Copper
8.47
9.21
mg/Kg
109
80 -120
Zinc
8.47
8.17
mg/Kg
96
80 -120
Cobalt
4.23
4.41
mg/Kg
104
80 -120
Lab Sample ID: 680-223856-3
MS
Client
Sample ID: SS-3
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 747484
Prep Batch: 746778
Sample Sample
Spike
MS
MS
%Rec
Analyte
Result Qualifier
Added
Result
Qualifier
Unit
D %Rec
Limits
Silver
<0.33
4.75
4.53
mg/Kg
95
75 -125
Arsenic
2.8
9.50
10.1
mg/Kg
77
75 -125
Barium
40 F2
9.50
46.9
4
mg/Kg
67
75-125
Cadmium
0.35 J
4.75
4.62
mg/Kg
90
75 -125
Lead
25 F1
47.9
54.4
F1
mg/Kg
61
75-125
Selenium
<1.1 F1
9.51
6.94
F1
mg/Kg
73
75-125
Antimony
<0.89 F1
4.74
2.96
F1
mg/Kg
62
75-125
Beryllium
0.62
4.75
5.09
mg/Kg
94
75 -125
Thallium
<0.80
4.75
4.51
mg/Kg
95
75-125
Eurofins Savannah
Page 52 of 81 11/8/2022 (Rev. 1)

QC Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Method: 6010D - Metals (ICP) (Continued)
Lab Sample ID: 680-223856-3 MS
Matrix: Solid
Analysis Batch: 747484
Sample Sample
Spike
MS
MS
Analyte Result Qualifier
Added
Result
Qualifier
Unit
D
%Rec
Nickel 5.7
9.40
14.4
mg/Kg
#
93
Vanadium 46
9.48
53.8
4
mg/Kg
82
Copper 15
9.50
24.8
mg/Kg
107
Zinc 42
9.50
43.9
4
mg/Kg
16
Cobalt 4.0
4.74
8.37
mg/Kg
91
Lab Sample ID: 680-223856-3 MSD
Matrix: Solid
Analysis Batch: 747484
Sample
Sample
Analyte
Result
Qualifier
Silver
<0.33
Arsenic
2.8
Barium
40
F2
Cadmium
0.35
J
Lead
25
F1
Selenium
<1.1
F1
Antimony
<0.89
F1
Beryllium
0.62
Thallium
<0.80
Nickel
5.7
Vanadium
46
Copper
15
Zinc
42
Cobalt
4.0
Method: 7471 B -
Mercury (CVAA)
Lab Sample ID: MB 680-747528/12-A
Matrix: Solid
Analysis Batch: 747974
Spike
Added
MSD
Result
MSD
Qualifier
Unit
4.75
4.64
mg/Kg
9.50
10.9
mg/Kg
9.50
58.5
4 F2
mg/Kg
4.75
4.67
mg/Kg
47.9
55.8
F1
mg/Kg
9.51
6.95
F1
mg/Kg
4.74
2.64
F1
mg/Kg
4.75
5.10
mg/Kg
4.75
4.62
mg/Kg
9.40
13.6
mg/Kg
9.48
45.1
4
mg/Kg
9.50
23.1
mg/Kg
9.50
49.6
4
mg/Kg
4.74
8.09
mg/Kg
MB MB
Analyte Result Qualifier RL MDL Unit
Mercury <0.0078 0.025 0.0078 mg/Kg
Lab Sample ID: LCS 680-747528/13-A
Matrix: Solid
Analysis Batch: 747974
Analyte
Mercury
Lab Sample ID: MB 680-747540/1-A
Matrix: Solid
Analysis Batch: 747974
D %Rec
98
85
190
91
64
73
56
94
97
85
-10
89
# 77
# 85
Job ID: 680-223856-1
Client Sample ID: SS-3
Prep Type: Total/NA
Prep Batch: 746778
%Rec
Limits
75-125
75-125
75-125
75-125
75-125
Client Sample
ID:
SS-3
Prep Type:
Total/NA
Prep Batch:
746778
%Rec
RPD
Limits RPD
Limit
75-125
2
20
75-125
7
20
75-125
22
20
75-125
1
20
75-125
3
20
75-125
0
20
75-125
12
20
75-125
0
20
75-125
2
20
75-125
5
20
75-125
18
20
75-125
7
20
75-125
12
20
75-125
3
20
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 747528
D Prepared Analyzed Dil Fac
10/28/22 09:19 10/31 /22 09:27 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 747528
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
0.212 0.221 mg/Kg 105 80 -120
MB MB
Analyte Result Qualifier RL
Mercury 0.00714 J 0.022
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch:747540
MDL Unit D Prepared Analyzed Dil Fac
0.0071 mg/Kg 10/28/2210:02 10/31/2211:03 1
Page 53 of 81
Eurofins Savannah
11 /8/2022 (Rev. 1)

QC Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Method: 7471 B - Mercury (CVAA) (Continued)
Lab Sample ID: LCS 680-747540/2-A
Matrix: Solid
Analysis Batch: 747974
Spike
Analyte
Added
Mercury
0.227
Lab Sample ID: 680-223856-10 MS
Matrix: Solid
Analysis Batch: 747974
Sample
Sample
Spike
Analyte Result
Qualifier
Added
Mercury 0.023
J B
0.105
Lab Sample ID: 680-223856-10 MSD
Matrix: Solid
Analysis Batch: 747974
Sample
Sample
Spike
Analyte Result
Qualifier
Added
Mercury 0.023
J B
0.105
Method: 365.4-1974 - Phosphorus, Total
Lab Sample ID: 680-223856-1 MS
Matrix: Solid
Analysis Batch: 747625
Sample Sample
Analyte Result Qualifier
Phosphorus 550 F1
Lab Sample ID: 680-223856-1 MSD
Matrix: Solid
Analysis Batch: 747625
Sample Sample
Analyte Result Qualifier
Phosphorus 550 F1
Lab Sample ID: MB 680-747587/1-A
Matrix: Solid
Analysis Batch: 748034
MB MB
Analyte Result Qualifier
Phosphorus <4.4
Lab Sample ID: LCS 680-747587/2-A
Matrix: Solid
Analysis Batch: 748034
Analyte
Phosphorus
Job ID: 680-223856-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 747540
LCS LCS %Rec
Result Qualifier Unit D %Rec Limits
0.235 mg/Kg 104 80 - 120
Client Sample ID: DUP-01
Prep Type: Total/NA
Prep Batch: 747540
MS MS %Rec
Result Qualifier Unit D %Rec Limits
0.125 mg/Kg 98 80 -120
Client Sample ID: DUP-01
Prep Type: Total/NA
Prep Batch: 747540
MSD MSD %Rec RPD
Result Qualifier Unit D %Rec Limits RPD Limit
0.123 mg/Kg * 96 80 -120 1 20
Client Sample ID: SS-1
Prep Type: Total/NA
Prep Batch: 747442
Spike MS MS %Rec
Added Result Qualifier Unit D %Rec Limits
207 668 F1 mg/Kg 57 70-130
Client Sample ID: SS-1
Prep Type: Total/NA
Prep Batch: 747442
Spike MSD MSD %Rec RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
203 865 F1 mg/Kg # 156 70-130 26 30
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 747587
RL MDL Unit D Prepared Analyzed Dil Fac
8.0 4.4 mg/Kg 10/28/2212:28 10/31/2213:17 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 747587
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
159 162 mg/Kg 101 70 -130
Page 54 of 81
Eurofins Savannah
11/8/2022 (Rev. 1)

QC Association Summary
Client: Environmental Conservation Laboratories
Project/Site: CF15067
GC/MS VOA
Prep Batch: 746886
Job ID: 680-223856-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-223856-1
SS-1
Total/NA
Solid
5035A
680-223856-2
SS-2
Total/NA
Solid
5035A
680-223856-3
SS-3
Total/NA
Solid
5035A
680-223856-4
SS-4
Total/NA
Solid
5035A
680-223856-5
SS-5
Total/NA
Solid
5035A
680-223856-6
SS-6
Total/NA
Solid
5035A
680-223856-7
SS-7
Total/NA
Solid
5035A
680-223856-8
SS-8
Total/NA
Solid
5035A
680-223856-9
BG-1
Total/NA
Solid
5035A
680-223856-10
DUP-01
Total/NA
Solid
5035A
Analysis Batch: 748284
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-223856-11
Trip Blank
Total/NA
Water
8260D
680-223856-12
Trip Blank
Total/NA
Water
8260D
MB 680-748284/9
Method Blank
Total/NA
Water
8260D
LCS 680-748284/5
Lab Control Sample
Total/NA
Water
8260D
LCSD 680-748284/6
Lab Control Sample Dup
Total/NA
Water
8260D
Analysis Batch: 748517
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-223856-1
SS-1
Total/NA
Solid
8260D
746886
680-223856-2
SS-2
Total/NA
Solid
8260D
746886
680-223856-3
SS-3
Total/NA
Solid
8260D
746886
680-223856-4
SS-4
Total/NA
Solid
8260D
746886
680-223856-5
SS-5
Total/NA
Solid
8260D
746886
680-223856-6
SS-6
Total/NA
Solid
8260D
746886
680-223856-7
SS-7
Total/NA
Solid
8260D
746886
680-223856-8
SS-8
Total/NA
Solid
8260D
746886
680-223856-9
BG-1
Total/NA
Solid
8260D
746886
680-223856-10
DUP-01
Total/NA
Solid
8260D
746886
MB 680-748517/9
Method Blank
Total/NA
Solid
8260D
LCS 680-748517/6
Lab Control Sample
Total/NA
Solid
8260D
LCSD 680-748517/7
Lab Control Sample Dup
Total/NA
Solid
8260D
Analysis Batch: 748537
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-223856-11
Trip Blank
Total/NA
Water
8260D
680-223856-12
Trip Blank
Total/NA
Water
8260D
MB 680-748537/9
Method Blank
Total/NA
Water
8260D
LCS 680-748537/5
Lab Control Sample
Total/NA
Water
8260D
LCSD 680-748537/6
Lab Control Sample Dup
Total/NA
Water
8260D
GUMS Semi VOA
Prep Batch: 747919
Lab Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 3546
Total/NA Solid 3546
Total/NA Solid 3546
Total/NA Solid 3546
Client Sample ID
680-223856-1
SS-1
680-223856-2
SS-2
680-223856-3
SS-3
680-223856-4
SS-4
0
Page 55 of 81
Eurofins Savannah
11 /8/2022 (Rev. 1)

QC Association Summary
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
GC/MS Semi VOA (Continued)
Prep Batch: 747919 (Continued)
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-223856-5 SS-5
Total/NA
Solid
3546
680-223856-6 SS-6
Total/NA
Solid
3546
680-223856-7 SS-7
Total/NA
Solid
3546
680-223856-8 SS-8
Total/NA
Solid
3546
680-223856-9 BG-1
Total/NA
Solid
3546
680-223856-10 DUP-01
Total/NA
Solid
3546
MB 680-747919/18-A Method Blank
Total/NA
Solid
3546
LCS 680-747919/19-A Lab Control Sample
Total/NA
Solid
3546
680-223856-1 MS SS-1
Total/NA
Solid
3546
680-223856-1 MSD SS-1
Total/NA
Solid
3546
Analysis Batch: 748005
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-223856-1
SS-1
Total/NA
Solid
8270E SIM ID
747919
680-223856-2
SS-2
Total/NA
Solid
8270E SIM ID
747919
680-223856-3
SS-3
Total/NA
Solid
8270E SIM ID
747919
680-223856-4
SS-4
Total/NA
Solid
8270E SIM ID
747919
680-223856-5
SS-5
Total/NA
Solid
8270E SIM ID
747919
680-223856-6
SS-6
Total/NA
Solid
8270E SIM ID
747919
680-223856-7
SS-7
Total/NA
Solid
8270E SIM ID
747919
680-223856-8
SS-8
Total/NA
Solid
8270E SIM ID
747919
680-223856-9
BG-1
Total/NA
Solid
8270E SIM ID
747919
680-223856-10
DUP-01
Total/NA
Solid
8270E SIM ID
747919
MB 680-747919/18-A
Method Blank
Total/NA
Solid
8270E SIM ID
747919
LCS 680-747919/19-A
Lab Control Sample
Total/NA
Solid
8270E SIM ID
747919
680-223856-1 MS
SS-1
Total/NA
Solid
8270E SIM ID
747919
680-223856-1 MSD
SS-1
Total/NA
Solid
8270E SIM ID
747919
HPLCAC
Leach Batch: 748171
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-223856-1
SS-1
Soluble
Solid
DI Leach
680-223856-2
SS-2
Soluble
Solid
DI Leach
680-223856-3
SS-3
Soluble
Solid
DI Leach
680-223856-4
SS-4
Soluble
Solid
DI Leach
680-223856-5
SS-5
Soluble
Solid
DI Leach
680-223856-6
SS-6
Soluble
Solid
DI Leach
680-223856-7
SS-7
Soluble
Solid
DI Leach
680-223856-8
SS-8
Soluble
Solid
DI Leach
680-223856-9
BG-1
Soluble
Solid
DI Leach
680-223856-10
DUP-01
Soluble
Solid
DI Leach
MB 680-748171/1-A
Method Blank
Soluble
Solid
DI Leach
LCS 680-748171/2-A
Lab Control Sample
Soluble
Solid
DI Leach
LCSD 680-748171/3-A
Lab Control Sample Dup
Soluble
Solid
DI Leach
680-223856-1 MS
SS-1
Soluble
Solid
DI Leach
680-223856-1 MSD
SS-1
Soluble
Solid
DI Leach
680-223856-10 MS
DUP-01
Soluble
Solid
DI Leach
680-223856-10 MSD
DUP-01
Soluble
Solid
DI Leach
0
Eurofins Savannah
Page 56 of 81 11/8/2022 (Rev. 1)

QC Association Summary
Client: Environmental Conservation Laboratories
Job ID:
680-223856-1
Project/Site: CF15067
HPLC/IC
Analysis Batch: 748340
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-223856-1
SS-1
Soluble
Solid
9056A
748171
680-223856-2
SS-2
Soluble
Solid
9056A
748171
680-223856-3
SS-3
Soluble
Solid
9056A
748171
680-223856-4
SS-4
Soluble
Solid
9056A
748171
680-223856-5
SS-5
Soluble
Solid
9056A
748171
680-223856-6
SS-6
Soluble
Solid
9056A
748171
680-223856-7
SS-7
Soluble
Solid
9056A
748171
680-223856-8
SS-8
Soluble
Solid
9056A
748171
680-223856-9
BG-1
Soluble
Solid
9056A
748171
680-223856-10
DUP-01
Soluble
Solid
9056A
748171
MB 680-748171/1-A
Method Blank
Soluble
Solid
9056A
748171
LCS 680-748171/2-A
Lab Control Sample
Soluble
Solid
9056A
748171
LCSD 680-748171/3-A
Lab Control Sample Dup
Soluble
Solid
9056A
748171
680-223856-1 MS
SS-1
Soluble
Solid
9056A
748171
680-223856-1 MSD
SS-1
Soluble
Solid
9056A
748171
680-223856-10 MS
DUP-01
Soluble
Solid
9056A
748171
680-223856-10 MSD
DUP-01
Soluble
Solid
9056A
748171
Metals
Prep Batch: 746580
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-223856-1
SS-1
Total/NA
Solid
3050B
680-223856-2
SS-2
Total/NA
Solid
3050B
MB 680-746580/1-A
Method Blank
Total/NA
Solid
3050B
LCS 680-746580/2-A
Lab Control Sample
Total/NA
Solid
3050B
Prep Batch: 746778
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-223856-3
SS-3
Total/NA
Solid
3050E
680-223856-4
SS-4
Total/NA
Solid
3050E
680-223856-5
SS-5
Total/NA
Solid
3050E
680-223856-6
SS-6
Total/NA
Solid
3050B
680-223856-7
SS-7
Total/NA
Solid
3050B
680-223856-8
SS-8
Total/NA
Solid
3050B
680-223856-9
BG-1
Total/NA
Solid
3050B
680-223856-10
DUP-01
Total/NA
Solid
3050B
MB 680-746778/1-A
Method Blank
Total/NA
Solid
3050B
LCS 680-746778/2-A
Lab Control Sample
Total/NA
Solid
3050E
680-223856-3 MS
SS-3
Total/NA
Solid
3050E
680-223856-3 MSD
SS-3
Total/NA
Solid
3050E
Analysis Batch: 747234
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-223856-1
SS-1
Total/NA
Solid
6010D
746580
680-223856-2
SS-2
Total/NA
Solid
6010D
746580
MB 680-746580/1-A
Method Blank
Total/NA
Solid
6010D
746580
LCS 680-746580/2-A
Lab Control Sample
Total/NA
Solid
6010D
746580
Eurofins Savannah
Page 57 of 81 11/8/2022 (Rev. 1)

QC Association Summary
Client: Environmental Conservation Laboratories
Job ID:
680-223856-1
Project/Site: CF15067
Metals
Analysis Batch: 747484
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-223856-3
SS-3
Total/NA
Solid
6010D
746778
680-223856-4
SS-4
Total/NA
Solid
6010D
746778
680-223856-5
SS-5
Total/NA
Solid
6010D
746778
680-223856-6
SS-6
Total/NA
Solid
6010D
746778
680-223856-7
SS-7
Total/NA
Solid
6010D
746778
680-223856-8
SS-8
Total/NA
Solid
6010D
746778
680-223856-9
BG-1
Total/NA
Solid
6010D
746778
680-223856-10
DUP-01
Total/NA
Solid
6010D
746778
MB 680-746778/1-A
Method Blank
Total/NA
Solid
6010D
746778
LCS 680-746778/2-A
Lab Control Sample
Total/NA
Solid
6010D
746778
680-223856-3 MS
SS-3
Total/NA
Solid
6010D
746778
680-223856-3 MSD
SS-3
Total/NA
Solid
6010D
746778
Prep Batch: 747528
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-223856-1
SS-1
Total/NA
Solid
7471B
680-223856-2
SS-2
Total/NA
Solid
7471B
680-223856-3
SS-3
Total/NA
Solid
7471B
680-223856-4
SS-4
Total/NA
Solid
7471B
680-223856-5
SS-5
Total/NA
Solid
7471B
680-223856-6
SS-6
Total/NA
Solid
7471B
680-223856-7
SS-7
Total/NA
Solid
7471B
680-223856-8
SS-8
Total/NA
Solid
7471B
680-223856-9
BG-1
Total/NA
Solid
7471B
MB 680-747528/12-A
Method Blank
Total/NA
Solid
7471B
LCS 680-747528/13-A
Lab Control Sample
Total/NA
Solid
7471B
Prep Batch: 747540
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-223856-10
DUP-01
Total/NA
Solid
7471B
MB 680-747540/1-A
Method Blank
Total/NA
Solid
7471B
LCS 680-747540/2-A
Lab Control Sample
Total/NA
Solid
7471B
680-223856-10 MS
DUP-01
Total/NA
Solid
7471B
680-223856-10 MSD
DUP-01
Total/NA
Solid
7471B
Analysis Batch: 747974
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-223856-1
SS-1
Total/NA
Solid
7471B
747528
680-223856-2
SS-2
Total/NA
Solid
7471B
747528
680-223856-3
SS-3
Total/NA
Solid
7471B
747528
680-223856-4
SS-4
Total/NA
Solid
7471B
747528
680-223856-5
SS-5
Total/NA
Solid
7471B
747528
680-223856-6
SS-6
Total/NA
Solid
7471B
747528
680-223856-7
SS-7
Total/NA
Solid
7471B
747528
680-223856-8
SS-8
Total/NA
Solid
7471B
747528
680-223856-9
BG-1
Total/NA
Solid
7471B
747528
680-223856-10
DUP-01
Total/NA
Solid
7471B
747540
MB 680-747528/12-A
Method Blank
Total/NA
Solid
7471B
747528
MB 680-747540/1-A
Method Blank
Total/NA
Solid
7471B
747540
LCS 680-747528/13-A
Lab Control Sample
Total/NA
Solid
7471B
747528
LCS 680-747540/2-A
Lab Control Sample
Total/NA
Solid
7471B
747540
Eurofins Savannah
Page 58 of 81 11/8/2022 (Rev. 1)

QC Association Summary
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Metals (Continued)
Analysis Batch: 747974 (Continued)
Job ID: 680-223856-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-223856-10 MS
680-223856-10 MSD
DUP-01
DUP-01
Total/NA
Total/NA
Solid
Solid
7471B
7471B
747540
747540
General Chem
Prep Batch: 747442
Lab Sample ID
Client Sample ID
680-223856-1
SS-1
680-223856-2
SS-2
680-223856-3
SS-3
680-223856-4
SS-4
680-223856-5
SS-5
680-223856-6
SS-6
680-223856-7
SS-7
680-223856-1 MS
SS-1
680-223856-1 MSD
SS-1
Prep Batch: 747587
Lab Sample ID
Client Sample ID
680-223856-8
SS-8
680-223856-9
BG-1
680-223856-10
DUP-01
MB 680-747587/1-A
Method Blank
LCS 680-747587/2-A
Lab Control Sample
Analysis Batch: 747625
Lab Sample ID
Client Sample ID
680-223856-1
SS-1
680-223856-2
SS-2
680-223856-3
SS-3
680-223856-4
SS-4
680-223856-5
SS-5
680-223856-6
SS-6
680-223856-7
SS-7
680-223856-1 MS
SS-1
680-223856-1 MSD
SS-1
Analysis Batch: 748003
Lab Sample ID
Client Sample ID
680-223856-1
SS-1
680-223856-2
SS-2
680-223856-3
SS-3
680-223856-4
SS-4
680-223856-5
SS-5
680-223856-6
SS-6
680-223856-7
SS-7
680-223856-8
SS-8
680-223856-9
BG-1
680-223856-10
DUP-01
Prep Type
Matrix
Method
Total/NA
Solid
Digestion
Total/NA
Solid
Digestion
Total/NA
Solid
Digestion
Total/NA
Solid
Digestion
Total/NA
Solid
Digestion
Total/NA
Solid
Digestion
Total/NA
Solid
Digestion
Total/NA
Solid
Digestion
Total/NA
Solid
Digestion
Prep Type
Matrix
Method
Total/NA
Solid
Digestion
Total/NA
Solid
Digestion
Total/NA
Solid
Digestion
Total/NA
Solid
Digestion
Total/NA
Solid
Digestion
Prep Batch
U
Prep Batch
Prep Type
Matrix
Method
Prep Batch
Total/NA
Solid
365.4-1974
747442
Total/NA
Solid
365.4-1974
747442
Total/NA
Solid
365.4-1974
747442
Total/NA
Solid
365.4-1974
747442
Total/NA
Solid
365.4-1974
747442
Total/NA
Solid
365.4-1974
747442
Total/NA
Solid
365.4-1974
747442
Total/NA
Solid
365.4-1974
747442
Total/NA
Solid
365.4-1974
747442
Prep Type
Matrix
Method
Prep Batch
Total/NA
Solid
Moisture
Total/NA
Solid
Moisture
Total/NA
Solid
Moisture
Total/NA
Solid
Moisture
Total/NA
Solid
Moisture
Total/NA
Solid
Moisture
Total/NA
Solid
Moisture
Total/NA
Solid
Moisture
Total/NA
Solid
Moisture
Total/NA
Solid
Moisture
Eurofins Savannah
Page 59 of 81 11/8/2022 (Rev. 1)

QC Association Summary
Client: Environmental Conservation Laboratories
Project/Site: CF15067
General Chemistry
Analysis Batch: 748034
Lab Sample ID
Client Sample ID
680-223856-8
SS-8
680-223856-9
BG-1
680-223856-10
DUP-01
MB 680-747587/1-A
Method Blank
LCS 680-747587/2-A
Lab Control Sample
Job ID: 680-223856-1
Prep Type
Matrix
Method
Prep Batch
Total/NA
Solid
365.4-1974
747587
Total/NA
Solid
365.4-1974
747587
Total/NA
Solid
365.4-1974
747587
Total/NA
Solid
365.4-1974
747587
Total/NA
Solid
365.4-1974
747587
0
Eurofins Savannah
Page 60 of 81 11/8/2022 (Rev. 1)

Lab Chronicle
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: SS-1 Lab Sample ID: 680-223856-1
Date Collected: 10/20/22 10:20 Matrix: Solid
Date Received: 10/22/22 07:00
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis Moisture 1 748003 10/31/22 15:32 TD EET SAV
Instrument ID: NOEQUIP
Client Sample ID: SS-1 Lab Sample ID: 680-223856-1
Date Collected: 10/20/22 10:20 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 95.6
Prep Type
Total/NA
Total/NA
Total/NA
Total/NA
Soluble
Soluble
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Batch
Batch
Type
Method
Prep
5035A
Analysis
8260D
Instrument ID: CMSP2
Prep
3546
Analysis
8270E SIM ID
Instrument ID: CMSX
Leach
DILeach
Analysis
9056A
Instrument ID: CICK
Prep
3050B
Analysis
6010D
Instrument ID: ICPH
Prep
7471 B
Analysis
7471 B
Instrument ID: LEEMAN2
Prep
Digestion
Analysis
365.4-1974
Instrument ID: SEAL 2
Dil
Initial
Run Factor
Amount
4.83 g
1
5g
15.32 g
1
1 mL
10.01 g
1
5 mL
0.52 g
1
0.53 g
0.2059 g
5
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst
Lab
5 mL
746886
10/25/22 12:49
FES
EET SAV
5 g
748517
11/03/22 10:44
Y1S
EET SAV
1 mL
747919
10/31/22 12:25
MEW
EET SAV
1 mL
748005
11/01/22 17:16
NED
EET SAV
100 mL
748171
11/01/22 14:20
AF
EET SAV
5 mL
748340
11/02/22 14:21
AF
EET SAV
50 mL
746580
10/24/22 15:17
SY
EET SAV
747234
10/26/22 21:16
BJB
EET SAV
50 mL
747528
10/28/22 09:19
JKL
EET SAV
747974
10/31/22 10:25
JKL
EET SAV
20 mL
747442
10/27/22 17:30
SM
EET SAV
747625
10/28/22 14:10
AS
EET SAV
Client Sample ID: SS-2 Lab Sample ID: 680-223856-2
Date Collected: 10/20/22 10:25 Matrix: Solid
Date Received: 10/22/22 07:00
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis Moisture 1 748003 10/31/22 15:32 TD EET SAV
Instrument ID: NOEQUIP
Client Sample ID: SS-2 Lab Sample ID: 680-223856-2
Date Collected: 10/20/22 10:25 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 76.6
Prep Type
Batch
Type
Batch
Method
Total/NA
Prep
5035A
Total/NA
Analysis
8260D
Instrument ID: CMSP2
Total/NA
Prep
3546
Total/NA
Analysis
8270E SIM ID
Instrument ID: CMSX
Dil
Initial
Run Factor
Amount
4.67 g
1
5g
15.46 g
1
1 mL
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst
Lab
5 mL
746886
10/25/22 12:49
FES
EET SAV
5 g
748517
11/03/22 11:08
Y1S
EET SAV
1 mL
747919
10/31/22 12:25
MEW
EET SAV
1 mL
748005
11/01/22 17:38
NED
EET SAV
Page 61 of 81
Eurofins Savannah
11 /8/2022 (Rev. 1)

Lab Chronicle
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: SS-2 Lab Sample ID: 680-223856-2
Date Collected: 10/20/22 10:25 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 76.6
Prep Type
Soluble
Soluble
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Batch
Batch
Type
Method
Leach
DlLeach
Analysis
9056A
Instrument ID: CICK
Prep
3050B
Analysis
6010D
Instrument ID: ICPH
Prep
7471 B
Analysis
7471 B
Instrument ID: LEEMAN2
Prep
Digestion
Analysis
365.4-1974
Instrument ID: SEAL 2
Dil
Initial
Run Factor
Amount
10.09 g
1
5 mL
0.61 g
1
0.55 g
E
0.2045 g
1
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst
Lab
100 mL
748171
11/01/22 14:20
AF
EET SAV
5 mL
748340
11/02/22 15:00
AF
EET SAV
50 mL
746580
10/24/22 15:17
SY
EET SAV
747234
10/26/22 21:19
BJB
EET SAV
50 mL
747528
10/28/22 09:19
JKL
EET SAV
747974
10/31/22 10:28
JKL
EET SAV
20 mL
747442
10/27/22 17:30
SM
EET SAV
747625
10/28/22 12:44
AS
EET SAV
Client Sample ID: SS-3 Lab Sample ID: 680-223856-3
Date Collected: 10/20/22 10:30 Matrix: Solid
Date Received: 10/22/22 07:00
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis Moisture 1 748003 10/31/22 15:32 TD EET SAV
Instrument ID: NOEQUIP
Client Sample ID: SS-3 Lab Sample ID: 680-223856-3
Date Collected: 10/20/22 10:30 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 97.5
Prep Type
Total/NA
Total/NA
Total/NA
Total/NA
Soluble
Soluble
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Batch
Batch
Type
Method
Prep
5035A
Analysis
8260D
Instrument ID: CMSP2
Prep
3546
Analysis
8270E SIM ID
Instrument ID: CMSX
Leach
DlLeach
Analysis
9056A
Instrument ID: CICK
Prep
3050B
Analysis
6010D
Instrument ID: ICPH
Prep
7471 B
Analysis
7471 B
Instrument ID: LEEMAN2
Prep
Digestion
Analysis
365.4-1974
Instrument ID: SEAL 2
Dil
Initial
Run Factor
Amount
4.37 g
1
5g
15.24 g
1
1 mL
10.03 g
1
5 mL
0.50 g
1
0.51 g
1
0.2002 g
1
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst
Lab
5 mL
746886
10/25/22 12:49
FES
EET SAV
5 g
748517
11/03/22 11:32
Y1S
EET SAV
1 mL
747919
10/31/22 12:25
MEW
EET SAV
1 mL
748005
11/01/22 18:00
NED
EET SAV
100 mL
748171
11/01/22 14:20
AF
EET SAV
5 mL
748340
11/02/22 15:13
AF
EET SAV
50 mL
746778
10/25/22 08:20
SY
EET SAV
747484
10/27/22 22:05
BJB
EET SAV
50 mL
747528
10/28/22 09:19
JKL
EET SAV
747974
10/31/22 10:32
JKL
EET SAV
20 mL
747442
10/27/22 17:30
SM
EET SAV
747625
10/28/22 12:42
AS
EET SAV
Page 62 of 81
Eurofins Savannah
11 /8/2022 (Rev. 1)

Lab Chronicle
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: SS-4 Lab Sample ID: 680-223856-4
Date Collected: 10/20/22 10:35 Matrix: Solid
Date Received: 10/22/22 07:00
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis Moisture 1 748003 10/31/22 15:32 TD EET SAV
Instrument ID: NOEQUIP
Client Sample ID: SS-4 Lab Sample ID: 680-223856-4
Date Collected: 10/20/22 10:35 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 95.7
Prep Type
Total/NA
Total/NA
Total/NA
Total/NA
Soluble
Soluble
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Batch
Batch
Type
Method
Prep
5035A
Analysis
8260D
Instrument ID: CMSP2
Prep
3546
Analysis
8270E SIM ID
Instrument ID: CMSX
Leach
DILeach
Analysis
9056A
Instrument ID: CICK
Prep
3050B
Analysis
6010D
Instrument ID: ICPH
Prep
7471 B
Analysis
7471 B
Instrument ID: LEEMAN2
Prep
Digestion
Analysis
365.4-1974
Instrument ID: SEAL 2
Dil
Initial
Run Factor
Amount
3.25 g
1
5g
15.38 g
1
1 mL
10.08 g
1
5 mL
0.50 g
1
0.53 g
1
0.2039 g
1
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst
Lab
5 mL
746886
10/25/22 12:49
FES
EET SAV
5 g
748517
11/03/22 11:55
Y1S
EET SAV
1 mL
747919
10/31/22 12:25
MEW
EET SAV
1 mL
748005
11/01/22 18:22
NED
EET SAV
100 mL
748171
11/01/22 14:20
AF
EET SAV
5 mL
748340
11/02/22 15:27
AF
EET SAV
50 mL
746778
10/25/22 08:20
SY
EET SAV
747484
10/27/22 22:20
BJB
EET SAV
50 mL
747528
10/28/22 09:19
JKL
EET SAV
747974
10/31/22 10:35
JKL
EET SAV
20 mL
747442
10/27/22 17:30
SM
EET SAV
747625
10/28/22 12:49
AS
EET SAV
Client Sample ID: SS-5 Lab Sample ID: 680-223856-5
Date Collected: 10/20/22 10:40 Matrix: Solid
Date Received: 10/22/22 07:00
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis Moisture 1 748003 10/31/22 15:32 TD EET SAV
Instrument ID: NOEQUIP
Client Sample ID: SS-5 Lab Sample ID: 680-223856-5
Date Collected: 10/20/22 10:40 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 90.5
Prep Type
Batch
Type
Batch
Method
Total/NA
Prep
5035A
Total/NA
Analysis
8260D
Instrument ID: CMSP2
Total/NA
Prep
3546
Total/NA
Analysis
8270E SIM ID
Instrument ID: CMSX
Dil
Initial
Run Factor
Amount
5.32 g
1
5g
15.86 g
1
1 mL
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst
Lab
5 mL
746886
10/25/22 12:49
FES
EET SAV
5 g
748517
11/03/22 12:19
Y1S
EET SAV
1 mL
747919
10/31/22 12:25
MEW
EET SAV
1 mL
748005
11/01/22 18:44
NED
EET SAV
Page 63 of 81
Eurofins Savannah
11 /8/2022 (Rev. 1)

Lab Chronicle
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: SS-5 Lab Sample ID: 680-223856-5
Date Collected: 10/20/22 10:40 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 90.5
Prep Type
Soluble
Soluble
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Batch
Batch
Type
Method
Leach
DlLeach
Analysis
9056A
Instrument ID: CICK
Prep
3050B
Analysis
6010D
Instrument ID: ICPH
Prep
7471 B
Analysis
7471 B
Instrument ID: LEEMAN2
Prep
Digestion
Analysis
365.4-1974
Instrument ID: SEAL 2
Dil
Initial
Run Factor
Amount
10.07 g
1
5 mL
0.52 g
1
0.52 g
E
0.2012 g
1
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst
Lab
100 mL
748171
11/01/22 14:20
AF
EET SAV
5 mL
748340
11/02/22 15:40
AF
EET SAV
50 mL
746778
10/25/22 08:20
SY
EET SAV
747484
10/27/22 14:28
BJB
EET SAV
50 mL
747528
10/28/22 09:19
JKL
EET SAV
747974
10/31/22 10:39
JKL
EET SAV
20 mL
747442
10/27/22 17:30
SM
EET SAV
747625
10/28/22 12:46
AS
EET SAV
Client Sample ID: SS-6 Lab Sample ID: 680-223856-6
Date Collected: 10/20/22 10:45 Matrix: Solid
Date Received: 10/22/22 07:00
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis Moisture 1 748003 10/31/22 15:32 TD EET SAV
Instrument ID: NOEQUIP
Client Sample ID: SS-6 Lab Sample ID: 680-223856-6
Date Collected: 10/20/22 10:45 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 90.2
Prep Type
Total/NA
Total/NA
Total/NA
Total/NA
Soluble
Soluble
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Batch
Batch
Type
Method
Prep
5035A
Analysis
8260D
Instrument ID: CMSP2
Prep
3546
Analysis
8270E SIM ID
Instrument ID: CMSX
Leach
DlLeach
Analysis
9056A
Instrument ID: CICK
Prep
3050B
Analysis
6010D
Instrument ID: ICPH
Prep
7471 B
Analysis
7471 B
Instrument ID: LEEMAN2
Prep
Digestion
Analysis
365.4-1974
Instrument ID: SEAL 2
Dil
Initial
Run Factor
Amount
5.01 g
1
5g
15.28 g
1
1 mL
10.06 g
1
5 mL
0.57 g
1
0.52 g
1
0.2002 g
1
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst
Lab
5 mL
746886
10/25/22 12:49
FES
EET SAV
5 g
748517
11/03/22 12:43
Y1S
EET SAV
1 mL
747919
10/31/22 12:25
MEW
EET SAV
1 mL
748005
11/01/22 19:06
NED
EET SAV
100 mL
748171
11/01/22 14:20
AF
EET SAV
5 mL
748340
11/02/22 15:53
AF
EET SAV
50 mL
746778
10/25/22 08:20
SY
EET SAV
747484
10/27/22 14:31
BJB
EET SAV
50 mL
747528
10/28/22 09:19
JKL
EET SAV
747974
10/31/22 10:49
JKL
EET SAV
20 mL
747442
10/27/22 17:30
SM
EET SAV
747625
10/28/22 12:46
AS
EET SAV
Page 64 of 81
Eurofins Savannah
11 /8/2022 (Rev. 1)

Lab Chronicle
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: SS-7 Lab Sample ID: 680-223856-7
Date Collected: 10/20/22 10:50 Matrix: Solid
Date Received: 10/22/22 07:00
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis Moisture 1 748003 10/31/22 15:32 TD EET SAV
Instrument ID: NOEQUIP
Client Sample ID: SS-7 Lab Sample ID: 680-223856-7
Date Collected: 10/20/22 10:50 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 93.1
Prep Type
Total/NA
Total/NA
Total/NA
Total/NA
Soluble
Soluble
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Batch
Batch
Type
Method
Prep
5035A
Analysis
8260D
Instrument ID: CMSP2
Prep
3546
Analysis
8270E SIM ID
Instrument ID: CMSX
Leach
DILeach
Analysis
9056A
Instrument ID: CICK
Prep
3050B
Analysis
6010D
Instrument ID: ICPH
Prep
7471 B
Analysis
7471 B
Instrument ID: LEEMAN2
Prep
Digestion
Analysis
365.4-1974
Instrument ID: SEAL 2
Dil
Initial
Run Factor
Amount
4.8 g
1
5g
15.71 g
1
1 mL
10.02 g
1
5 mL
0.53 g
1
0.58 g
1
0.2089 g
1
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst
Lab
5 mL
746886
10/25/22 12:49
FES
EET SAV
5 g
748517
11/03/22 13:07
Y1S
EET SAV
1 mL
747919
10/31/22 12:25
MEW
EET SAV
1 mL
748005
11/01/22 19:28
NED
EET SAV
100 mL
748171
11/01/22 14:20
AF
EET SAV
5 mL
748340
11/02/22 16:06
AF
EET SAV
50 mL
746778
10/25/22 08:20
SY
EET SAV
747484
10/27/22 14:34
BJB
EET SAV
50 mL
747528
10/28/22 09:19
JKL
EET SAV
747974
10/31/22 10:52
JKL
EET SAV
20 mL
747442
10/27/22 17:30
SM
EET SAV
747625
10/28/22 12:48
AS
EET SAV
Client Sample ID: SS-8 Lab Sample ID: 680-223856-8
Date Collected: 10/20/22 10:55 Matrix: Solid
Date Received: 10/22/22 07:00
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis Moisture 1 748003 10/31/22 15:32 TD EET SAV
Instrument ID: NOEQUIP
Client Sample ID: SS-8 Lab Sample ID: 680-223856-8
Date Collected: 10/20/22 10:55 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 76.7
Prep Type
Batch
Type
Batch
Method
Total/NA
Prep
5035A
Total/NA
Analysis
8260D
Instrument ID: CMSP2
Total/NA
Prep
3546
Total/NA
Analysis
8270E SIM ID
Instrument ID: CMSX
Dil
Initial
Run Factor
Amount
4.84 g
1
5g
15.85 g
1
1 mL
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst
Lab
5 mL
746886
10/25/22 12:49
FES
EET SAV
5 g
748517
11/03/22 13:31
Y1S
EET SAV
1 mL
747919
10/31/22 12:25
MEW
EET SAV
1 mL
748005
11/01/22 19:49
NED
EET SAV
Page 65 of 81
Eurofins Savannah
11 /8/2022 (Rev. 1)

Lab Chronicle
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: SS-8 Lab Sample ID: 680-223856-8
Date Collected: 10/20/22 10:55 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 76.7
Prep Type
Soluble
Soluble
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Batch
Batch
Type
Method
Leach
DlLeach
Analysis
9056A
Instrument ID: CICK
Prep
3050B
Analysis
6010D
Instrument ID: ICPH
Prep
7471 B
Analysis
7471 B
Instrument ID: LEEMAN2
Prep
Digestion
Analysis
365.4-1974
Instrument ID: SEAL 2
Dil
Initial
Run Factor
Amount
10.08 g
1
5 mL
0.60 g
1
0.56 g
E
0.2083 g
1
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst
Lab
100 mL
748171
11/01/22 14:20
AF
EET SAV
5 mL
748340
11/02/22 16:45
AF
EET SAV
50 mL
746778
10/25/22 08:20
SY
EET SAV
747484
10/27/22 14:36
BJB
EET SAV
50 mL
747528
10/28/22 09:19
JKL
EET SAV
747974
10/31/22 10:56
JKL
EET SAV
20 mL
747587
10/28/22 12:28
SM
EET SAV
748034
10/31/22 09:31
AS
EET SAV
Client Sample ID: BG-1 Lab Sample ID: 680-223856-9
Date Collected: 10/20/22 11:10 Matrix: Solid
Date Received: 10/22/22 07:00
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis Moisture 1 748003 10/31/22 15:32 TD EET SAV
Instrument ID: NOEQUIP
Client Sample ID: BG-1 Lab Sample ID: 680-223856-9
Date Collected: 10/20/22 11:10 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 84.7
Prep Type
Total/NA
Total/NA
Total/NA
Total/NA
Soluble
Soluble
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Total/NA
Batch
Batch
Type
Method
Prep
5035A
Analysis
8260D
Instrument ID: CMSP2
Prep
3546
Analysis
8270E SIM ID
Instrument ID: CMSX
Leach
DlLeach
Analysis
9056A
Instrument ID: CICK
Prep
3050B
Analysis
6010D
Instrument ID: ICPH
Prep
7471 B
Analysis
7471 B
Instrument ID: LEEMAN2
Prep
Digestion
Analysis
365.4-1974
Instrument ID: SEAL 2
Dil
Initial
Run Factor
Amount
4.06 g
1
5g
15.32 g
1
1 mL
10.03 g
1
5 mL
0.51 g
1
0.53 g
li
0.2060 g
5
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst
Lab
5 mL
746886
10/25/22 12:49
FES
EET SAV
5 g
748517
11/03/22 13:55
Y1S
EET SAV
1 mL
747919
10/31/22 12:25
MEW
EET SAV
1 mL
748005
11/01/22 20:12
NED
EET SAV
100 mL
748171
11/01/22 14:20
AF
EET SAV
5 mL
748340
11/02/22 16:58
AF
EET SAV
50 mL
746778
10/25/22 08:20
SY
EET SAV
747484
10/27/22 14:39
BJB
EET SAV
50 mL
747528
10/28/22 09:19
JKL
EET SAV
747974
10/31/22 10:59
JKL
EET SAV
20 mL
747587
10/28/22 12:28
SM
EET SAV
748034
10/31/22 13:18
AS
EET SAV
Page 66 of 81
Eurofins Savannah
11 /8/2022 (Rev. 1)

Lab Chronicle
Client: Environmental Conservation Laboratories
Project/Site: CF15067
Job ID: 680-223856-1
Client Sample ID: DUP-01 Lab Sample ID: 680-223856-10
Date Collected: 10/20/22 08:00 Matrix: Solid
Date Received: 10/22/22 07:00
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis Moisture 1 748003 10/31/22 15:32 TD EET SAV
Instrument ID: NOEQUIP
Client Sample ID: DUP-01 Lab Sample ID: 680-223856-10
Date Collected: 10/20/22 08:00 Matrix: Solid
Date Received: 10/22/22 07:00 Percent Solids: 90.0
Prep Type
Batch Batch
Type Method
Dil
Run Factor
Initial
Amount
Total/NA
Prep 5035A
4.9 g
Total/NA
Analysis 8260D
1
5 g
Instrument ID: CMSP2
Total/NA
Prep 3546
15.66 g
Total/NA
Analysis 8270E SIM ID
1
1 mL
Instrument ID: CMSX
Soluble
Leach DI Leach
10.08 g
Soluble
Analysis 9056A
1
5 mL
Instrument ID: CICK
Total/NA
Prep 3050B
0.57 g
Total/NA
Analysis 6010D
1
Instrument ID: ICPH
Total/NA
Prep 7471 B
0.53 g
Total/NA
Analysis 7471 B
1
Instrument ID: LEEMAN2
Total/NA
Prep Digestion
0.2065 g
Total/NA
Analysis 365.4-1974
1
Instrument ID: SEAL 2
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst
Lab
5 mL
746886
10/25/22 12:49
FES
EET SAV
5 g
748517
11/03/22 14:19
Y1S
EET SAV
1 mL
747919
10/31/22 12:25
MEW
EET SAV
1 mL
748005
11/01/22 20:34
NED
EET SAV
100 mL
748171
11/01/22 14:20
AF
EET SAV
5 mL
748340
11/02/22 17:24
AF
EET SAV
50 mL
746778
10/25/22 08:20
SY
EET SAV
747484
10/27/22 14:42
BJB
EET SAV
50 mL
747540
10/28/22 10:02
JKL
EET SAV
747974
10/31/22 11:09
JKL
EET SAV
20 mL
747587
10/28/22 12:28
SM
EET SAV
748034
10/31/22 09:37
AS
EET SAV
Client Sample ID: Trip Blank
Lab Sample ID: 680-223856-11
Date Collected: 10/20/22 08:00
Matrix: Water
Date Received: 10/22/22 07:00
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260D
1
5 mL
5 mL
748537
11/03/22 15:56
P1C EET SAV
Instrument ID: CMSAD
Total/NA Analysis 8260D
1
5 mL
5 mL
748284
11/02/22 14:29
Y1S EET SAV
Instrument ID: CMSC
Client Sample ID: Trip Blank Lab Sample ID: 680-223856-12
Date Collected: 10/20/22 08:00 Matrix: Water
Date Received: 10/22/22 07:00
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA Analysis 8260D
1
5 mL
5 mL
748537
11/03/22 16:17 P1C EET SAV
Instrument ID: CMSAD
Total/NA Analysis 8260D
1
5 mL
5 mL
748284
11/02/22 14:48 Y1S EET SAV
Instrument ID: CMSC
Page 67 of 81
Eurofins Savannah
11 /8/2022 (Rev. 1)

Lab Chronicle
Client: Environmental Conservation Laboratories Job ID: 680-223856-1
Project/Site: CF15067
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
0
Eurofins Savannah
Page 68 of 81 11/8/2022 (Rev. 1)

SENDING LABORATORY:
ENCO Cary
102-A Woodwinds Industrial Court
Cary, NC 27511
Phone-- 919 467 3090
Fax [phone]
Project Manager Amanda L Gaines
SUBCONTRACT ORDER 1 r'" 1 �✓ �� C
ENCO Cary
CF15067
RECEIVING LABORATORY:
Test America (GA)
5102 LaRoche Avenue
Savannah, GA 31404
Phone .[phone]
Fax -0
Prqlect State of Origin North Carolina
Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments
SS-1 Soil 20-Oct-22 10:20
Analysis late lft #es Ana a) C mnte #5;
8260D fCL SOIv102 4 31-Oct-22 15 00 03-Nov-22 10 20 m
8270E SIM- 1,4-Droxane
31-00-22 15 OU
27-Oct-22 10 20
Antimony 'Iotal EPA 6010D
31-Oct-22 1500
18-Apr-23 1020
Arsenic Total EPA 601OD
31-Oct-22 1500
18-Apt'-23 10 20 `J
Barium Total LPA 6010D
31-Oct-22 15 00
18-Apr-23 1020
Beryllium Total EPA 601OD
31-Oct-22 1500
18-Apr-23 1020
Cadmium Total EPA 6010D
31-Oct-22 15 00
18-Apr-23 1020
('obalt Total EPA 60IOD
31-Oct-22 15 00
18-Apr-23 1020
Copper Total EPA 6010D
31-Oct-22 1500
18-Apr-23 1020 u
Lead Total EPA 601 OD
31-0e t-22 1500
18-Apr-23 1020
Mercury Total P13A 7000 (Upda31-Oct-22
15 00
17-Nov-22 10 20 j%0
Nickel Total EPA 6010D
31-Oct-22 1500
18-Apr-23 10 20 V.,Phosphorus
Total CPA 365 4
31-Oct-22 1500
17-Nov-22 10 2011.5
SeICIMMI Total CPA 6010D
31-Oct-22 15 00
18-Apr-23 10 20,..#5
Silver rotal EPA 6010D
31-Oct-22 1500
18-Apr-23 10 20 9%'S
Sulrate 9056A
31-Oct-22 15 00
17-Nov-22 10 20y/a
t halhum "local FPA 6010D
31-Oct-22 15 00
18-Apr-23 10 20-05
Vanadiuni'lolal EPA 6010D
31-Oct-22 1500
18-Apr-23 10 20 Zf
Zinc Total I- PA 601OD
31-Oct-22 1500
18-Apr-23 10 24.�
( oulauter v Supj)hed
40mIV-1'I+IOmLMeOFI
40mLV-L1+surbar(B)
40mLV-LT+strrhar(C)
(A)
4ozAlar (D)
680-223856 Chain of Custody
I oh I -
Released 13` Date Received B) Date
Page I of 10
Page 69 of 81 11/8/2022 (Rev. 1)

SUBCONTRACT ORDER C
ENCO Cary
CF15067
Sub Lab ID Originating Lab Ill Client Matrix Date Sampled Sample Comments
SS-2 Soil 20-Oct-22 10:25
Analysis
Rae
Expires Analysis Comments
8260D TCL SOM02 4
31-Oct-22 1500
03-Nov-22 10 25
8270E SIM- 1,4-Dtoxane
31-Oct-22 1500
27-Oct-22 1025
Antimony Total EPA 601 OD
31-Oct-22 1500
18-Apr-23 1025
Arsenic Total EPA 601 OD
31-Oct-22 15 00
18-Apr-23 1025
Bartum Total EPA 601 OD
31-Oct-22 15 00
18-Apr-23 1025
Beryllium Total EPA 6010D
31-Oct-22 1500
18-Apr-23 1025
Cadmuim Total EPA6010D
31-Oct-22 15 00
18-Apr-23 1025
Cobalt Tolal EPA 601 OD
31-Oct-22 1500
18-Apr-23 1025
Copper Total EPA 001OD
31-Oct-22 1500
18-Apr-23 1025 m
Lead Total EPA 601 OD
3 1-Oct-22 1500
18-Apr-23 1025
Mercury Iota) LPA 7000 (Upda3
i-00-22 1500
17-Nov-22 1025
Nickel'Total LPA 6010D
31-Oct-22 1500
18-Apr-23 1025
Phosphorus Total EPA 365 4
31-Oct-22 15 00
17-Nov-22 1025
Selenium Total I PA 601 OD
31-Oct-22 1500
18-Apr-23 1025
Scher Total EPA 601OD
31-Oct-22 1500
18-Apr-23 1025
Sulfate 9056A
31-Oct-22 1500
17-Nov-22 1025
Thallium Total EPA 601 OD
31-Oct-22 1500
18-Apr-23 1025
Vanadium Total EPA 601 OD
31-Oct-22 1500
18-Apr-23 1025
Zinc Total EPA 601 OD
31-Oct-22 1500
18-Apr-23 1025
('onrawel s S+y)plled
40mLV-! F+10mLMe0F1 40mLV-I.T+sUrbar (B) 40mLV-LT+sttrbar (C) 4ozA.1ar (D)
e
Released By Date Received By Date
Page 2 of 10
Page 70 of 81 11 /8/2022 (Rev. 1)

SUBCONTRACT ORDER C
ENCO Cary
CF15067
Sub Lab ID Or►ginating Lab ID
Client 117atrix Date Sampled Sample Comments
SS-3
Soil 20-Oct-22 10:30
Analysis
flue
Expires Anal sis Cpmm nts
8260D 1C.1. 50M02 4
31-Oct-22 1500
03-Nov-22 10 30
8270E SIM- 1 4-Deoxane
31-0ct-22 1500
27-Oct-22 1030
Antimony lotal EPA 6010D
31-Oct-22 1500
18-Apr-23 1030
Arsenic Iotul FPA 60IOD
31-Oct-22 1500
18-Apr-23 1030
Barnum Total LPA 601 OD
31-Oct-22 1500
18-Apr-23 1030
Beryllium Total EPA 601 OD
31-Oct-22 1500
18-Apr-23 1030
Cadnmu►n total CPA 601 OD
31-Oct-22 1500
18-Apr-23 1030
Cobalt Total CPA 601 OD
31-Oct-22 1500
18-Apr-23 1030
Copper Total FPA 601OD
II-Oct-22 1500
18-Apr-23 1030
Lead Total F,PA 601OD
31-Oct-22 1500
18-Apr-23 1030
Mercmy'rotal EPA 7000 (Upda3 I -Oct-22 1500
17-Nov-22 1030
N►ckel Total EPA 601 OD
i I -Oct-22 1500
18-Apr-23 1030
Phosphorus Total CPA 365 4
31-Oct-22 1500
17-Nox-22 1030
SelelilUm Total EPA 601OD
31-00-22 1500
18-Apr-23 1030
S►Iver Total EPA 001OD
31-OU-22 1500
18-Apr-23 1030
Sultutc 9056A
31-Oct-22 15 00
17-Nov-22 1030
rhalhum'rotal EPA 601OD
31-Oct-22 1500
18-Apr-23 1030
Vanadium'rotal LPA 601 OD
31-Oct-22 1500
18-Apr-23 1030
7mc Total EPA 6010D
31-Oc1-22 1500
18-Apr-23 1030
Contaune rs ,Supphed
40mLV-L T+IOmLMeOH 40mLV-LT+sttrbar (B) 40mLV-LT+stu•bar (C) 4ozAjar (D)
Released B) Datc Received By Date
Page 3 of 10
Page 71 of 81 11 /8/2022 (Rev. 1)

SUBCONTRACT ORDER
ENCO Cary
CF15067
Sub Lab ID Originating Lab ID
Client 'Matrix Date Sampled Sample Comments
SS-4
Soil 20-Oct-22 10:35
Analysis
Due
Expires Analysis Comments
8260D ICL SOM02 4
31-Oct-22 15 00
03-Nov-22 10 35
8270E SIM- 14-Dioxane
31-Oct-22 1500
27-Oct-22 10 35
Antiniony total 1 PA 6010D
31-Oct-22 1500
18-Apr-23 1035
Arsenic Iotal I PA 6010D
31-Oct-22 1500
18-Api-23 1035
Barium Total PI'A 6010D
31-Oct-22 1500
18-Apr-23 1035
Beryl Iium'lotal LPA 6010D
31-Oct-22 1500
18-Apr-23 1035
(-admiwn'lotal LPA 6010D
31-Oct-22 1500
18-Apr-23 1035
Cobalt total L PA 6010D
31-00-22 1500
18-Apr-23 1035
C opper Total LPA 60101)
31-Oct-22 1500
18-Apr-23 1035
I -cad Iotal EI'A 6010D
31-Oct-22 1500
18-Apr-23 1035
Mercury Total FPA 7000 (Upda31-00-22
1500
17-Nov-22 1035
Nickel Total FPA 6010D
31-0e1-22 1500
18-Apr-23 1035
Phosphorus Total CPA 365 4
31-Oct-22 1500
17-Nov-22 1035
Selenium Iotal EPA 6010D
31-Oc1-22 15 00
18-Apr-23 1035
Silver total L PA 6010D
31-Oc1-22 1500
18-Apr-23 1035
Sulfate 9056A
31-Oct-22 1500
17-Nov-22 1035
Thallium Total EPA 601OD
31-Oct-22 1500
18-Apr-23 1035
Vanadium Total EPA 6010D
31-Oct-22 1500
18-Apr-23 1035
Zinc Total CPA 60101)
31-Oct-22 1500
18-Apr-23 1035
C'onlrnnel s Supplied
40mt V-1 T+IOmL McOli
40mLV-I l'+SUrbar (B)
40tnLV-13+stirbar (C) 4ozAlar (D)
(A)
( Vvz 114 w �� =
Da
Released BY Date Received By Date
Page 72 of 81
Pa e 4 of 10
11 /8/%22 (Rev. 1)

SUBCONTRACT ORDER
ENCO Cary
CF15067
Sub Lab ID Originating Lab ID
Client Matrix Date Sampled Sample Continents
SS-5
Soil 20-Oct-22 10:40
Analysis
Due
Expires Analysis Comments
8260D TCL SOM02 4
31-Oct-22 1500
03-Nov-22 10 40
82701 SIM- 14-Dioxane
31-Oct-22 1500
27-Opt-22 10 40
Antimony Total EPA 6010D
31-Oct-22 1500
18-Apr-23 1040
Arsenic Total EPA 601OD
31-Oct-22 1500
18-Apr-23 1040
Banum total 1 PA 6010D
31-Oct-22 1500
18-Apr-23 1040
Beryihmn Total EPA 601OD
31-Oct-22 1500
18-Apr-23 1040
Cadmium total L PA 6010D
31-Oct-22 1500
18-Apr-23 1040
Cobalt Total EPA 601OD
31-Oct-22 1500
18-Apr-23 1040
Copper Total I PA 6010D
31-Oc1-22 1500
18-Apr-23 1040
Lead local LPA 6010D
31-0o-22 1500
18-Apr-23 1040
Mcmw-) Total I PA 7000 (Upda3 1 -Oct-22 1500
17-Nov-22 1040
Nickel Total EPA 601OD
31-Oct-22 1500
18-Apr-23 1040
Phosphorus'lotal EPA 365 4
31-Oct-22 1500
17-Nov-22 1040
Selenium Total L-PA 6010D
31-Oct-22 1500
18-Apr-23 1040
Snlver'lotal I PA 6010D
31-Oct-22 1500
18-Apr-23 1040
Sulfate 9056A
31-Oct-22 1500
17-Nov-22 1040
Thalhum total LPA 60IOD
31-Oct-22 1500
18-Apr-23 1040
Vanadium Total EPA 6010D
31-Oct-22 1500
18-Apr-23 1040
7me lotal EPA6010D
31-Oct-22 1500
18-Apr-23 1040
C. ontainei s Supplied
40m1,V-LT+I OtnLMeO1-1
40mLV-LT+-,urbar (B)
40mLV-LT+stnrbar (C) 4ozA,lar (D)
(A)
c
Released By Date Received By Date
Page 73 of 81
Page 5 oI 10
11 /8/2022 (Rev. 1)

SURCONTRACT ORDER
ENCO Cary
CF 15067
Sub Lab ID Originating Lab ID
Client Matrix Date Sampled Sample Comments
SS-6
Soil 20-Oct-22 10:45
Analysis
Due
Expires Analysis Comments . .
8260D TCl SOM02 4
31-Oct-22 1500
03-Nov-22 10 45
8270E SIM- 1 4-Dioxane
3 1 -00-22 1500
27-Oct-22 1045
Antimony total CPA 601OD
31-Oct-22 1500
18-Apr-23 1045
Arsenic total t PA 60101)
31-0ct-22 1500
18-Apr-23 1045
Banum Total EPA 601 OD
31-Oct-22 1500
18-Apr-23 1045
Beryllium Total C.PA 601 OD
31-Oct-22 1500
18-Apr-23 1045
Cadmium Total CPA 6010D
31-Oct-22 1500
18-Apr-23 1045
Cobalt Total EPA 60101)
31-Oct-22 1500
18-Apr-23 1045
Copper Total EPA 601OD
31-Oct-22 1500
18-Apr-23 1045
l ead'total E PA 601OD
31-Oct-22 1500
18-Apr-23 1045
Mercup Total EPA 7000 (Upda3 I -Oct-22 1500
17-Nov-22 1045
Nickel Total CPA 601OD
31-Oct-22 1500
18-Apr-23 1045
Phosphorus Total EPA 365 4
31-Oct-22 1500
17-Nov-22 1045
Selenium Total EPA 601OD
31-00-22 1500
18-Apr-23 1045
Silver Iolal 1'PA 60101)
31-Oct-22 1500
18-Apr-23 1045
Sullate 9056A
31-Oct-22 1500
17-Nov-22 1045
Thalhum Total EPA 601 OD
31-Oct-22 1500
18-Apr-23 1045
Vanadium Total LPA 601 OD
31-Oct-22 1500
18-Apr-23 1045
Zinc Total LPA 6010D
31-Oct-22 1500
18-Apr-23 1045
Conlamel s Supplied
40mLV-1 T+l0mLMeOH 40nil V-ur+snrbsr (B) 40mLV-LT+sttrbar (C) 4ozAlar (D)
Released 13y Date Received By Date
Page 74 of 81 11 /0022 (Rev. 1)

SUBCONTRACT ORDER
ENCO Cary
CF15O67
Sub Lab ID Originating Lab ID
Client Matrix Date Sampled Sample Comments
SS-7
Soil 20-00-22 10:50
Analysis
Due
Ax ,ires Analysis Comments
82601) FCI. SOM02 4
31-Oct-22 1500
03-Nov-22 10 50
8270C SIM- 1 4-Dloxane
31-Oct-22 1500
27-Oct-22 1050
Antimony lotal F PA 6010D
31-Oc1-22 15 00
18-Apr-23 1050
Arsenic total L-I'A 6010D
31-Oct-22 15 00
18-Apr-23 1050
l3anum total I PA 601 OD
31-Oct-22 1500
18-Apr-23 1050
I3erj II IUm I otal I PA 6010D
31-Oc1-22 1500
18-Apr-23 1050
C.admILIM Total CPA 6010D
31-Oct-22 1500
18-Apr-23 1050
Cobalt Iolai I PA601OD
31-Oct-22 1500
18-Apr-23 1050
Copper total LPA 601 OD
31-Oct-22 15 00
18-Apr-23 1050
I cad total CPA 60101)
31-00-22 1500
18-Apr-23 1050
Mercury focal LPA 7000 (Upda3 I -Oct-22 1500
17-Nov-22 1050
Nickel Total CPA 601OD
31-Oct-22 1500
18-Apr-23 1050
Phosphorus Total PPA 365 4
31-Oct-22 1500
17-Nov-22 1050
Selenium Total I PA 6010D
3I-Oct-22 1500
18-Apr-23 IO 50
Sliver Total F I'A 601 OD
31-Oc1-22 1500
18-Apr-23 1050
Sul late 9056A
31-Oct-22 1500
17-Nov-22 1050
1 halhum Total EPA 601 OD
31-Oct-22 1500
18-Apr-23 IO 50
Vanadium total EPA6010D
31-Oct-22 1500
18-Apr-23 1050
/Inc total CPA 601 OD
31-Oct-22 1500
18-Api-23 1050
( onlamel s Supplied
40m1 V-17+1 Oml McOI I 40mLV-LT+Stlrbar (13) 40mLV-LT+stirhar (C) 4ozA.lar (D)
(A)
Released lay Date Recened By Date
Page 75 of 81 11 /01022t�(Rev. 1)

SUBCONTRACT ORDER C
ENCO Cary
CF15067
Sub Lab ID Originating Lab ID
Client Matrix Date Sampled Sample Comments
SS-8
Soil 20-Oct-22 10:55
Analysis
Due
Expires Analysis Comments
8260D R 1, SOM02 4
31-Oct-22 1500
03-Nov-22 10 55
8270E SIM- 1 4-Dioxanc
31-Oc1-22 1500
27-Oct-22 10 55
Antunony Total LPA 6010D
31-Oct-22 1500
18-Apr-23 1055
Arsenic Total EPA 6010D
31-OLt-22 1500
18-Apr-23 1055
Barium Total LPA 6010D
31-Oct-22 1500
18-Apr-23 1055
13er)liiLim "total CPA 60101)
31-Oct-22 1500
18-Apr-23 1055
C admaum "total LPA 6010D
31-Oct-22 1500
18-Apr-23 1055
Cobalt Total L PA 601 OD
31-Oct-22 1500
18-Apr-23 1055
Copper Total L PA 6010D
31-Oct-22 1500
18-Apr-23 1055
Lead Total LPA 60101)
31-Oct-22 I> 00
18-Apr-23 10 55
Mercury Total CPA 7000 (Llpda31-00-22
1500
17-Nov-22 1055
Nukel Total El'A 6010D
31-Oct-22 1500
18-Apr-23 1055
Phosphorus Total EPA 365 4
31-Oct-22 1500
17-Nov-22 1055
Sclennun Total t PA 60101)
31-Oct-22 1500
18-Apr-23 1055
Salver "Total L PA 60101.)
31-Oct-22 1500
18-Apr-23 10 55
Sulfate 9056A
31-Oct-22 1500
17-Nov-22 10 55
1 hallium Total EPA 6010D
31-Oct-22 15 00
18-Apr-23 1055
Vanadium Total EPA 6010D
31-Oct-22 1500
18-Apr-23 10 55
Zinc total EPA 6010D
31-Oct-22 1500
18-Apr-23 1055
Conl mei s Supplied
40mLV4LI+IOmLMeOTI
40mLV-Cr+surbar (13)
40ml V-LT+stu•bar (C) 4ozAjar (D)
(A)
Released By Date Received By Date
Page 8 01 10
Page 76 of 81 11 /8/2022 (Rev. 1)

SUBCONTRACT ORDER
ENCO Cary
CF15067
Sub Lab ID Originating Lab ID
Client Mati ix Date Sampled Sample -Comments
l3G- I
Soil 20-Oct-22 11:10
Analysis
Due
Expires Analysis Comments
8260D I CL SOM02 4
31-Oct-22 1500
03-Nov-22 11 10
92701 YM- 14-Dioxane
31-Oct-22 1500
27-Oct-22 I 1 10
Antunony total LPA601OD
3 1 -00-22 1500
18-Apr-23 I 10
AI'SCIM Total t PA 60101)
31-Oct-22 1500
18-Apr-23 I 1 10
Barium 'total FPA 6010D
31-Oct-22 1500
18-Apr-23 I 1 10
Bery1hunl Total FPA 6010D
31-Oct-22 1500
18-Apr-23 11 10
C.ad111iL1111 total FlIA 6010D
31-Oct-22 1500
18-Apr-23 I1 10
Cobalt Total LPA 601OD
31-Oc1-22 1500
18-Apr-23 11 10
C opper Total EPA 6010D
31-Oct -22 1500
18-Apr-23 11 10
Lead total LPA601OD
31-00-22 1500
18-Apr-23 I 10
Mercury Total LPA 7000 (Upda3 I -Oct-22 1500
17-Nov-22 11 10
Nickel Total EPA6010D
31-Oct-22 1500
18-Apr-23 I 1 10
Phosphorus'lotal LPA 365 4
31-Oct-22 1500
17-Nov-22 I 1 10
Selenium total LPA 60101)
31-Oct-22 1500
18-Apr-23 I 1 10
SiIvei Total I-PA601OD
31-Oct-22 1500
18-Apr-23 1110
Sulfate 9056A
31-Opt-22 1500
17-Nov-22 I 1 10
Thalluuo Total EPA 6010D
31-Oct-22 1500
18-Apr-23 1110
Vanadnu» total FPA 6010D
31-Oct-22 1500
18-Apr-23 I 1 10
Zinc Total t 111A 601OD
31-Oct-22 1500
18-Apr-23 I 1 10
C'omamei.s Supplied
40ml. V-L 1+10n1L McOl-1
40mLV-L1+ti1irbar (13)
40mLV-L3+mirbar (C) 4ozA1ar (D)
(A)
F&
c
Released By Date Ruined t3y Date
Page 9 o 110
Page 77 of 81 11/8/2022 (Rev. 1)

SUBCONTRACT ORDER C
ENCO Cary
CF15067
Sub Lab ID Originating Lab ID
Client Matrix Date Sampled Sample Comments
DUP-01
Soil 20-00-22 08:00
Analysis
Due
Expires Analysis Comments
8260D TC.L SOMO2 4
31-Oct-22 1500
03-Nov-22 08 00
82701- SIM- 1,4-Dioxanc
31-Oct-22 1500
27-Oct-22 08 00
Antimony Total L PA 601 OD
31-OL1-22 1500
18-Apr-23 08 00
Arscn1L To(al I PA 60101)
31-0c,1-22 1500
18-Apr-23 08 00
l3anom total I PA 601 OD
31-0c,t-22 1500
18-Apr-23 08 00
Beryllium total 1. PA 60IOD
31-Oct-22 1500
18-Apr-23 08 00
C admium total I PA 601 OD
31-0ct-22 1500
18-Apr-23 08 00
(. obah Total IYA 601 OD
11-0(,t-22 1500
18-Apr-23 08 00
C opper Iola[ FPA 601 OD
31-Oct-22 1500
18-Apr-23 08 00
Lead total EPA 601 OD
31-Oct-22 1500
18-Apr-23 08 00
Mercury Total L PA 7000 (Upda31 Oct-22 1500
17-Nov-22 08 00
Nickel Total EPA 601 OD
31-Oct-22 1500
18-Apr-23 08 00
PhosphoruS Total CPA 365 4
31-Oct-22 1500
17-Nov-22 08 00
Selenium Total EPA 6010D
31 100-22 1500
18-Apr-23 08 00
Silver Total F1'A 601OD
31-Oct-22 1500
18-Apr-23 08 00
Sulfate 9056A
31-00-22 1500
17-Nov-22 08 00
'1'hallMin Total EPA 601OD
31-Oct-22 1500
18-Apr-23 08 00
Vanadium Total CPA 601 OD
31-Oct-22 1500
18-Apr-23 08 00
Zinc Total CPA 601 OD
31-Oct-22 1500
18-Apr-23 08 00
Cnuiamers Supplied
40ml-V-1 T+IOml-Me011 40mLV-1T+stn-bar (B) 40ml V-L'l+stirbar (C) 4ozAjar (D)
(A)
Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments
Trip Blank Water 20-Oct-22 08:00
Anal sis Due Expires Analysis Comments
8260D TC L SOM02 4 31-00-22 15 00 03-Nov-22 08 00
8270L YN4- 14-Dioxanc 31-Oct-22 15 00 27-00-22 08 00
C'owamei % Supplied
40ml V+I ICI (A) 40mLV+HCI (B)
Sub Lab ID Originating Lab ID Client Matrix Date Sampled Sample Comments
Trip Blaul< Water 20-Oct-22 08:00
Analysis One Expires Analysis Comments J
8260D'ICL SOM02 4 31-Oct-22 15 00 03-Nov-22 08 00
92701 SIM- 14-Dioaane 31-Oct-22 15 00 27-Oct-22 08 00
Crmlautei s Supplied
40ni1 V+I-ICI (A) 40ml V+11CI (B)
Re.
ate
Released By Date Received By Date
Page 10 ol' 10
Page 78 of 81 11 /8/2022 (Rev. 1)

i
�yCL
N
cc
4' 1.
� t bt I6 m
( a'. Y
r
U)LU
i i V I
co
y
�.+�
f LU
of isd p I n L
S
US 7 gs} k, I" w
c�
0
LJ
ell
c
It
� ! � s �?:j � � �/ ti � �, � ! � I �, _ �} f � t.r. I � .� � j c 1, •}
w
} 2 I
(. a
c
Page 79 of 81 11/8/2022 (Rev. 1)

Login Sample Receipt Checklist
Client: Environmental Conservation Laboratories Job Number: 680-223856-1
Login Number: 223856
List Number: 1
Creator: Kirkland, Bernard C
Question
List Source: Eurofins Savannah
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True m
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
Eurofins Savannah
Page 80 of 81 11/8/2022 (Rev. 1)

Accreditation/Certification Summary
Client: Environmental Conservation Laboratories Job ID: 680-223856-1
Project/Site: CF15067
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report
Authority Program Identification Number Expiration Date
North Carolina (WW/SW) State 269 12-31-22
Eurofins Savannah
Page 81 of 81 11/8/2022 (Rev. 1)

•
% eurofins
Environment Testing
I ANALYTICAL REPORT C
PREPARED FOR
Attn: Amanda Gaines
Environmental Conservation Laboratories
102 Woodwinds Industrial Ct, Suite A C
Cary, North Carolina 27511
Generated 12/6/2022 4:35:12 PM
4 JOB DESCRIPTION
CR8136
JOB NUMBER
680-226581-1

The test results in this report meet NELAP requirements for parameters for which accreditation is required or available. Any
exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report may not be
reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the person who
signed this report.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project
Manager.
F
Generated
12/6/2022 4:35:12 PM
Authorized for release by
Sheila Hoffman, Project Manager II
Sheila.Hoffman(o-)et.eurofinsus.com
[phone]
Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies
Page 2 of 18 12/6/2022

Method Summary
Client: Environmental Conservation Laboratories
Job ID: 680-226581-1
Project/Site: CF18136
Method Method Description
Protocol
Laboratory
601 OD Metals (ICP)
SW846
EET SAV
7471B Mercury (CVAA)
SW846
EET SAV
Moisture Percent Moisture
EPA
EET SAV
3050B Preparation, Metals
SW846
EET SAV
7471B Preparation, Mercury
SW846
EET SAV
Protocol References:
EPA = US Environmental Protection Agency
SW846 ='Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
Page 3 of 18 12/6/2022

Sample Summary
Client: Environmental Conservation Laboratories
Project/Site: CF18136
Lab Sample ID Client Sample ID Matrix Collected Received
680-226581-1 SS-4 (11/29/22) Solid 11/29/22 16:40 12/01/22 06:30
Job ID: 680-226581-1
Page 4 of 18
Eurofins Savannah
12/6/2022

Definitions/Glossary
Client: Environmental Conservation Laboratories Job ID: 680-226581-1
Project/Site: CF18136
Qualifiers
Metals
Qualifier Qualifier Description
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
F1 MS and/or MSD recovery exceeds control limits.
F2 MS/MSD RPD exceeds control limits
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
c Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
oil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Lever'
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRIES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Savannah
Page 5 of 18 12/6/2022

Case Narrative
Client: Environmental Conservation Laboratories
Project/Site: CF18136
Job ID: 680-226581-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-226581-1
Receipt
The sample was received on 12/1/2022 6:30 AM. Unless otherwise noted below, the sample arrived in good condition, and, where
required, properly preserved and on ice. The temperature of the cooler at receipt time was 1.9°C
Metals
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
General Chemistry
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Job ID: 680-226581-1
Eurofins Savannah
Page 6 of 18 12/6/2022

Detection Summary
Client: Environmental Conservation Laboratories
Project/Site: CF18136
Client Sample ID: SS-4 (11/29/22)
Analyte
Arsenic
Barium
Beryllium
Cobalt
Copper
Lead
Nickel
Vanadium
Zinc
Mercury
F
Job ID: 680-226581-1
Lab Sample ID: 680-226581-1
Result
Qualifier
RL
Unit
Dil Fac
D
Method
Prep Type
2.3
2.3
1.4
mg/Kg
1
*
6010D
Total/NA
50
1.1
0.47
mg/Kg
1
*
6010D
Total/NA
0.44
J
0.46
0.081
mg/Kg
1
*
6010D
Total/NA
4.6
1.1
0.38
mg/Kg
1
*
6010D
Total/NA
17
F1
2.9
0.57
mg/Kg
1
*
6010D
Total/NA
12
1.1
0.70
mg/Kg
1
*
6010D
Total/NA
5.5
4.6
1.0
mg/Kg
1
o
6010D
Total/NA
36
F1
1.1
0.18
mg/Kg
1
o
6010D
Total/NA
53
2.3
0.66
mg/Kg
1
o
6010D
Total/NA
0.024
J
0.028
0.0088
mg/Kg
1
*
7471 B
Total/NA
This Detection Summary does not include radiochemical test results.
Eurofins Savannah
Page 7 of 18 12/6/2022

Client Sample Results
Client: Environmental Conservation Laboratories
Job ID: 680-226581-1
Project/Site: CF18136
Client Sample ID: SS-4 (11/29/22)
Lab Sample ID: 680-226581-1
Date Collected: 11/29/22 16:40
Matrix: Solid
Date Received: 12/01/22 06:30
Percent Solids: 85.7
Method: SW846 6010D - Metals (ICP)
Analyte
Result
Qualifier
RL
Unit
D
Prepared
Analyzed Dil Fac
Antimony
<1.0
F1 F2
2.3
1.0
mg/Kg
*
12/02/22 09:15
12/05/22 13:32 1
Arsenic
2.3
2.3
1.4
mg/Kg
*
12/02/22 09:15
12/05/22 13:32 1
Barium
50
1.1
0.47
mg/Kg
*
12/02/22 09:15
12/05/22 13:32 1
Beryllium
0.44
J
0.46
0.081
mg/Kg
12/02/22 09:15
12/05/22 13:32 1
Cadmium
<0.11
0.57
0.11
mg/Kg
12/02/22 09:15
12/05/22 13:32 1
Cobalt
4.6
1.1
0.38
mg/Kg
12/02/22 09:15
12/05/22 13:32 1
Copper
17
F1
2.9
0.57
mg/Kg
-3:�
12/02/22 09:15
12/05/22 13:32 1
Lead
12
1.1
0.70
mg/Kg
-3:�
12/02/22 09:15
12/05/22 13:32 1
Nickel
5.5
4.6
1.0
mg/Kg
12/02/22 09:15
12/05/22 13:32 1
Selenium
<1.3
2.9
1.3
mg/Kg
12/02/22 09:15
12/05/22 13:32 1
Silver
<0.37
1.1
0.37
mg/Kg
12/02/22 09:15
12/05/22 13:32 1
Thallium
<0.89
2.9
0.89
mg/Kg
12/02/22 09:15
12/05/22 13:32 1
Vanadium
36
F1
1.1
0.18
mg/Kg
o
12/02/22 09:15
12/05/22 13:32 1
Zinc
53
2.3
0.66
mg/Kg
o
12/02/22 09:15
12/05/22 13:32 1
Method: SW846 7471E - Mercury (CVAA)
Analyte
Result
Qualifier
RL
Unit
D
Prepared
Analyzed Dil Fac
Mercury
0.024
J
0.028
0.0088
mg/Kg
*
12/05/2212:44
12/06/2211:02 1
Eurofins Savannah
Page 8 of 18 12/6/2022

QC Sample Results
Client: Environmental Conservation Laboratories
Job ID: 680-226581-1
Project/Site: CF18136
Method: 6010D - Metals (ICP)
Lab Sample ID: MB 680-753301/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 753837
Prep Batch: 753301
MB MB
Analyte
Result Qualifier
RL
Unit
D Prepared
Analyzed Dil Fac
Antimony
<0.74
1.7
0.74
mg/Kg
12/02/22 09:15
12/06/22 10:02 1
Arsenic
<1.0
1.7
1.0
mg/Kg
12/02/22 09:15
12/06/22 10:02 1
Barium
<0.35
0.85
0.35
mg/Kg
12/02/22 09:15
12/06/22 10:02 1
Beryllium
<0.060
0.34
0.060
mg/Kg
12/02/22 09:15
12/06/22 10:02 1
Cadmium
<0.085
0.42
0.085
mg/Kg
12/02/22 09:15
12/06/22 10:02 1
Cobalt
<0.28
0.85
0.28
mg/Kg
12/02/22 09:15
12/06/22 10:02 1
Copper
<0.42
2.1
0.42
mg/Kg
12/02/22 09:15
12/06/22 10:02 1
Lead
<0.52
0.85
0.52
mg/Kg
12/02/22 09:15
12/06/22 10:02 1
Nickel
<0.76
3.4
0.76
mg/Kg
12/02/22 09:15
12/06/22 10:02 1
Selenium
<0.93
2.1
0.93
mg/Kg
12/02/22 09:15
12/06/22 10:02 1
Silver
<0.27
0.85
0.27
mg/Kg
12/02/22 09:15
12/06/22 10:02 1
Thallium
<0.66
2.1
0.66
mg/Kg
12/02/22 09:15
12/06/22 10:02 1
Vanadium
<0.14
0.85
0.14
mg/Kg
12/02/22 09:15
12/06/22 10:02 1
Zinc
<0.49
1.7
0.49
mg/Kg
12/02/22 09:15
12/06/22 10:02 1
Lab Sample ID: LCS 680-753301/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 753837
Prep Batch: 753301
Spike
LCS
LCS
%Rec
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits
Antimony
4.67
4.26
mg/Kg
91
80 - 120
Arsenic
9.35
9.54
mg/Kg
102
80 - 120
Barium
9.35
9.70
mg/Kg
104
80 - 120
Beryllium
4.67
4.63
mg/Kg
99
80 - 120
Cadmium
4.67
4.72
mg/Kg
101
80 - 120
Cobalt
4.67
4.83
mg/Kg
103
80 - 120
Copper
9.35
10.1
mg/Kg
108
80 - 120
Lead
47.1
48.0
mg/Kg
102
80 - 120
Nickel
9.25
9.68
mg/Kg
105
80 - 120
Selenium
14.0
13.6
mg/Kg
97
80 - 120
Silver
4.67
4.42
mg/Kg
95
80 - 120
Thallium
4.67
4.66
mg/Kg
100
80 - 120
Vanadium
9.33
9.44
mg/Kg
101
80 - 120
Zinc
9.35
9.72
mg/Kg
104
80 - 120
Lab Sample ID: 680-226581-1 MS
Client Sample ID: SS-4 (11129/22)
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 753837
Prep Batch: 753301
Sample Sample
Spike
MS
MS
%Rec
Analyte
Result Qualifier
Added
Result
Qualifier
Unit
D %Rec
Limits
Antimony
<1.0 F1 F2
4.98
2.01
F1
mg/Kg
40
75 - 125
Arsenic
2.3
9.98
11.4
mg/Kg
# 92
75 - 125
Barium
50
9.98
57.0
4
mg/Kg
# 73
75 - 125
Beryllium
0.44 J
4.99
5.20
mg/Kg
Ct 96
75 - 125
Cadmium
<0.11
4.99
4.72
mg/Kg
Ct 95
75 - 125
Cobalt
4.6
4.98
9.39
mg/Kg
Ct 96
75 - 125
Copper
17 F1
9.98
27.9
mg/Kg
108
75-125
Lead
12
50.3
58.4
mg/Kg
91
75 - 125
Nickel
5.5
9.88
16.1
mg/Kg
107
75 - 125
Eurofins Savannah
Page 9 of 18 12/6/2022

QC Sample Results
Client: Environmental Conservation Laboratories
Project/Site: CF18136
Method: 6010D - Metals (ICP) (Continued)
Lab Sample ID: 680-226581-1 MS
Matrix: Solid
Analysis Batch: 753837
Sample Sample
Analyte
Result Qualifier
Selenium
<1.3
Silver
<0.37
Thallium
<0.89
Vanadium
36 F1
Zinc
53
Lab Sample ID: 680-226581-1 MSD
Matrix: Solid
Analysis Batch: 753837
Sample
Sample
Analyte Result
Qualifier
Antimony <1.0
F1 F2
Arsenic 2.3
Barium 50
Beryllium 0.44
J
Cadmium <0.11
Cobalt 4.6
Copper 17
F1
Lead 12
Nickel 5.5
Selenium <1.3
Silver <0.37
Thallium <0.89
Vanadium 36
F1
Zinc 53
Method: 7471 B - Mercury (CVAA)
Lab Sample ID: MB 680-753639/12-A
Matrix: Solid
Analysis Batch: 753834
Analyte
Mercury
Lab Sample ID: LCS 680-753639/13-A
Matrix: Solid
Analysis Batch: 753834
Analyte
Mercury
Spike
Added
MS
Result
MS
Qualifier
Unit
15.0
12.8
mg/Kg
4.99
4.39
mg/Kg
4.99
5.01
mg/Kg
9.96
50.7
F1
mg/Kg
9.98
57.0
4
mg/Kg
Spike
MSD
MSD
Added
Result
Qualifier
Unit
5.40
3.69
F1 F2
mg/Kg
10.8
12.0
mg/Kg
10.8
62.1
4
mg/Kg
5.40
5.34
mg/Kg
5.40
4.84
mg/Kg
5.40
9.25
mg/Kg
10.8
24.9
F1
mg/Kg
54.5
60.0
mg/Kg
10.7
14.6
mg/Kg
16.2
13.2
mg/Kg
5.40
4.61
mg/Kg
5.40
5.14
mg/Kg
10.8
44.4
mg/Kg
10.8
61.7
4
mg/Kg
MB MB
Result Qualifier RL Unit
<0.0078 0.025 0.0078 mg/Kg
F
Job ID: 680-226581-1
Client Sample ID: SS-4 (11/29/22)
Prep Type: Total/NA
Prep Batch: 753301
%Rec
D %Rec
Limits
0 85
75-125
88
75.125
�F 101
75.125
i� 152
75.125
� 40
75.125
Client Sample ID: SS-4 (11/29/22)
Prep Type: Total/NA
Prep Batch: 753301
%Rec RPD
D %Rec
Limits RPD Limit
68
75.125 59 20
# 89
75.125 4 20
# 115
75.125 9 20
91
75-125 3 20
90
75-125 2 20
86
75-125 1 20
71
75.125 12 20
87
75.125 3 20
85
75.125 10 20
81
75. 125 3 20
85
75.125 5 20
95
75.125 2 20
81
75.125 13 20
80
75. 125 8 20
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 753639
D Prepared Analyzed Dil Fac
12/05/22 12:44 12/06/22 10:38 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 753639
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
0.231 0.231 mg/Kg 100 80 _ 120
Eurofins Savannah
Page 10 of 18 12/6/2022

Client: Environmental Conservation Laboratories
Project/Site: CF18136
Metals
Prep Batch: 753301
Lab Sample ID
Client Sample ID
680-226581-1
SS-4 (11/29/22)
MB 680-753301/1-A
Method Blank
LCS 680-753301/2-A
Lab Control Sample
680-226581-1 MS
SS-4 (11/29/22)
680-226581-1 MSD
SS-4 (11/29/22)
Prep Batch: 753639
Lab Sample ID
Client Sample ID
680-226581-1
SS-4 (11/29/22)
MB 680-753639/12-A
Method Blank
LCS 680-753639/13-A
Lab Control Sample
Analysis Batch: 753834
Lab Sample ID
Client Sample ID
680-226581-1
SS-4 (11/29/22)
MB 680-753639/12-A
Method Blank
LCS 680-753639/13-A
Lab Control Sample
Analysis Batch: 753837
Lab Sample ID
Client Sample ID
680-226581-1
SS-4 (11/29/22)
MB 680-753301/1-A
Method Blank
LCS 680-753301/2-A
Lab Control Sample
680-226581-1 MS
SS-4 (11/29/22)
680-226581-1 MSD
SS-4 (11/29/22)
General Chemistry
Analysis Batch: 753455
Lab Sample ID
Client Sample ID
680-226581-1
SS-4 (11/29/22)
QC Association Summary C
Job ID: 680-226581-1
Prep Type
Matrix
Method
Prep Batch
Total/NA
Solid
3050B
Total/NA
Solid
3050B
Total/NA
Solid
3050B
Total/NA
Solid
3050B
Total/NA
Solid
3050B
Prep Type
Matrix
Method
Prep Batch i
Total/NA
Solid
7471B
Total/NA
Solid
7471B
Total/NA
Solid
7471B
Prep Type
Matrix
Method
Prep Batch
Total/NA
Solid
7471B
753639
Total/NA
Solid
7471B
753639
Total/NA
Solid
7471B
753639
Prep Type
Matrix
Method
Prep Batch
Total/NA
Solid
6010D
753301
Total/NA
Solid
6010D
753301
Total/NA
Solid
6010D
753301
Total/NA
Solid
6010D
753301
Total/NA
Solid
6010D
753301
Prep Type
Matrix
Method
Prep Batch
Total/NA
Solid
Moisture
Page 11 of 18
Eurofins Savannah
12/6/2022

Lab Chronicle
Client: Environmental Conservation Laboratories
Project/Site: CF18136
Client Sample ID: SS-4 (11/29/22)
Date Collected: 11/29/22 16:40
Date Received: 12/01/22 06:30
Batch Batch Dil Initial
Prep Type Type Method Run Factor Amount
Total/NA Analysis Moisture 1
Instrument ID: NOEQUIP
Client Sample ID: SS-4 (11/29/22)
Date Collected: 11/29/22 16:40
Date Received: 12/01/22 06:30
Batch Batch
Dil
Initial
Prep Type Type Method
Run Factor
Amount
Total/NA Prep 3050B
1.02 g
Total/NA Analysis 6010D
1
Instrument ID: ICPH
Total/NA Prep 7471 B
0.53 g
Total/NA Analysis 7471 B
1
Instrument ID: LEEMAN2
Laboratory References:
EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
F
Job ID: 680-226581-1
Lab Sample ID: 680-226581-1
Matrix: Solid
Final Batch Prepared
Amount Number or Analyzed Analyst Lab
753455 12/03/22 12:13 TD EET SAV
Lab Sample ID: 680-226581-1
Matrix: Solid
Percent Solids: 85.7
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst
Lab
100 mL
753301
12/02/22 09:15
SY
EET SAV
753837
12/05/22 13:32
BJB
EET SAV
50 mL
753639
12/05/22 12:44
JKL
EET SAV
753834
12/06/22 11:02
BCB
EET SAV
Page 12 of 18
Eurofins Savannah
12/6/2022

SUBCONTRACT ORDER
ENCO Cary
CF18136
SENDING LABORATORY:
RECEIVING LABORATORY:
ENCO Cary
Test America (GA)
102-A Woodwinds Industrial Court
5102 LaRoche Avenue
Cary, NC 27511
Savannah, GA 31404
Phone: [phone]
Phone •[phone]
Fax [phone]
Fax: -0
Project Manager- Amanda
L. Gaines
Project State of Origin: North Carolina
Sub Lab ID Originating Lab ID
Client Matrix Date Sampled Sample Comments
C
SS-4 (11/29/22)
Soil 29-Nov-22 16:40
Anal sis
Due
Ex lI,vs, Analysis Comments
Antunony Total EPA 601 OD
09-Dec-22 1500
28-May-23 1640 m
Arsenic Total EPA 6010D
09-Dec-22 15 00
28-May-23 1640 /� ' c
Barium Total EPA 6010D
09-Dec-22 15 00
28-May-23 1640
Beryllium Total EPA 601 OD
09-Dec-22 1500
28-May-23 1640
Cadmium Total EPA 601 OD
09-Dec-22 1500
28-May-23 1640
Cobalt Total EPA 6010D
09-Dec-22 1500
28-May-23 1640
Copper Total EPA 601 OD
09-Dec-22 15 00
28-May-23 1640
Lead Total EPA 6010D
09-Dec-22 1500
28-May-23 1640 J /
t�
Mercury Total EPA 7000 (Upda09-Dec-22
1500
27-Dec-22 16 40
Nickel Total EPA 6010D
09-Dec-22 15 00
28-May-23 1640
Selenium Total EPA 6010D
09-Dec-22 1500
28-May-23 1640
Silver Total EPA 6010D
09-Dec-22 1500
28-May-23 1640
Solids, Dry Weight
09-Dec-22 1500
28-May-23 1640 Auto -Included
Thallium Total EPA 60101)
09-Dec-22 15 00
28-May-23 1640
Vanadium Total EPA 6010D
09-Dec-22 1500
28-May-23 1640
Zinc Total EPA 6010D
09-Dec-22 1500
28-May-23 1640
C ontainei s Suppfied
4ozAlar (A)
4ozAlar (B)
Released By Date Received By
Page 13 of 18
IN-2UIII81�IqChain YIINCIJStIIIVI��'NI�N� _12/6/2022

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0
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12/6/2022
Flage 14 of 16

Login Sample Receipt Checklist
Client: Environmental Conservation Laboratories
Job Number: 680-226581-1
Login Number: 226581
List Number: 1
Creator: Padayao, Abigail
Question
List Source: Eurofins Savannah
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True m
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
Eurofins Savannah
Page 15 of 18 12/6/2022

Accreditation/Certification Summary
Client: Environmental Conservation Laboratories Job ID: 680-226581-1
Project/Site: CF18136
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW) State 269 12-31-22 L
Eurofins Savannah
Page 16 of 18 12/6/2022

Definitions/Glossary
Client: Environmental Conservation Laboratories
Project/Site: CF18136
Qualifiers
Metals
Job ID: 680-226581-1
Qualifier Qualifier Description
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
F1 MS and/or MSD recovery exceeds control limits.
F2 MS/MSD RPD exceeds control limits
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
c Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Lever'
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRIES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Savannah
Page 17 of 18 12/6/2022

Accreditation/Certification Summary
Client: Environmental Conservation Laboratories Job ID: 680-226581-1
Project/Site: CF18136
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW) State 269 12-31-22 L
Eurofins Savannah
Page 18 of 18 12/6/2022

Appendix C — NCDEQ PSRGs (July 2022)
aecom.com

Table 1
Sample Analytical Summary and PSRGs
Chemical Name
CAS #
Residential Health
Based PSRG (mg/kg)
Protection of
Groundwater PSRG
(mg/kg)
SW-846 8260D Volatile Organic Compounds
Acetone
67-64-1
14100
24.6
Acrylonitrile
107-13-1
0.268
0.000282
Benzene
71-43-2
1.22
0.0102
Bromochloromethane
74-97-5
31.8
NE
Bromodichloromethane
75-27-4
0.311
0.00325
Bromoform; Tribromomethane
75-25-2
20.3
0.0212
Carbon disulfide
75-15-0
162
4.12
Carbon tetrachloride
56-23-5
0.691
0.00231
Chlorobenzene
108-90-7
58.3
0.679
Chloroethane; Ethyl chloride
75-00-3
1150
17
Chloroform; Trichloromethane
67-66-3
0.336
0.387
Dibromochloromethane; Chlorodibromomethane
124-48-1
8.28
0.00213
1,2-Dibromo-3-chloropropane; DBCP
96-12-8
0.00559
0.000346
1,2-Dibromoethane; Ethylene dibromide; EDB
106-93-4
0.0383
0.000113
o-Dichlorobenzene; 1,2-Dichlorobenzene
95-50-1
379
0.389
p-Dichlorobenzene; 1,4-Dichlorobenzene
106-46-7
2.78
0.115
trans-1, 4-Dichloro-2-butene
110-57-6
0.00792
1,1-Dichlorethane; Ethylidene chloride
75-34-3
3.77
0.034
1,2-Dichlorethane; Ethylene dichloride
107-06-2
0.492
0.00227
1,1-Dichloroethylene; 1,1-Dichloroethene; Vinylidene chloride
75-35-4
48.1
2.49
cis- 1,2-Dichloroethylene; cis-1,2-Dichloroethene
156-59-2
31.3
0.411
trans-1, 2-Dichloroethylene;trans-1,2-Dichloroethene
156-60-5
14.8
0.625
1,2-Dichloropropane; Propylene dichloride
78-87-5
2.63
0.00398
cis-1,3-Dich lorop rope n e
10061-01-5
1.92
0.00286
tra n s-1,3-Dich lorop rope n e
10061-02-6
1.92
0.00286
1,4-Dioxane*
123-91-1
5.37
0.0123
Ethylbenzene
100-41-4
6.12
13.4
2-Hexanone; Methyl butyl ketone
591-78-6
41.5
0.184
Methyl bromide; Bromomethane
74-83-9
1.45
0.0505
Methyl chloride; Chloromethane
74-87-3
23.5
0.0155
Methylene bromide; Dibromomethane
74-95-3
5.02
0.345
Methylene chloride; Dichloromethane
75-09-2
57.8
0.0255
Methyl ethyl ketone; MEK; 2-Butanone
78-93-3
5540
16.7
Methyl iodide; Idomethane
74-88-4
4-Methyl-2-pentanone; Methyl isobutyl ketone
108-10-1
7040
0.451
Styrene
100-42-5
1250
1.54
1,1,1,2-Tetrach loroeth a ne
630-20-6
2.11
0.00762
1,1,2,2-Tetrach loroeth a ne
79-34-5
0.636
0.00156
Tetrachloroethylene; Tetrachloroethene; Perchloroethylene
127-18-4
17.1
0.00634
Toluene
108-88-3
991
8.3
1,1,1-Trichloroethane; Methylchloroform
71-55-6
1730
1.39
1,1,2-Trichloroethane
79-00-5
0.319
0.00389
Trichloroethylene; Trichloroethene
79-01-6
0.871
0.0214
Trichlorofluoromethane;CFC-11
75-69-4
4690
25.3
1,2,3-Trichloropropane
96-18-4
0.0051
0.0000433
Vinyl acetate
108-05-4
193
0.375
Vinyl chloride
75-01-4
0.0605
0.000205
Xylenes
1330-20-7
122
9.89
SW-846 6010D - Metals
Antimony (Total)
7440-36-0
6.26
0.904
Arsenic (Total)
7440-38-2
0.677
5.84
Barium (Total)
7440-39-3
3130
577
Beryllium (Total)
7440-41-7
31.3
63.2
Cadmium (Total)
7440-43-9
1.43
3.01
Chromium (Total)
7440-47-3
0.306
3.84
Cobalt (Total)
7440-48-4
4.69
0.904
Copper (Total)
7440-50-8
626
704
Lead (Total)
7439-92-1
NE
270
Mercury (Total)
7439-97-6
2.31
1.04
Nickel (Total)
7440-02-0
313
130

Table 1
Sample Analytical Summary and PSRGs
Chemical Name
CAS #
Residential Health
Based PSRG (mg/kg)
Protection of
Groundwater PSRG
(mg/kg)
Selenium (Total)
7782-49-2
78.2
2.08
Silver (Total)
7440-22-4
78.2
3.4
Thallium (Total)
7440-28-0
0.156
0.285
Vanadium (Total)
7440-62-2
78.2
350
Zinc (Total)
7440-66-6
4690
1240
EPA 356.3 - Total Phosphorus
7723-14-0
0.313
0.00343
EPA 300 - Sulfate
14808-79-8
EPA 353.2 - Nitrate
14797-55-8
250001
NE
SM 9045 D - pH
*1,4-Dioxane may need to be analyzed by SW-846 8260D SIM or 8270D SIM in order to achieve applicable detection limits

Appendix D - Metals and Radionuclides Analyses in Soil Cores from Mooresville, North
Carolina (Cobalt and Arsenic Box Plots)
aecom.com

0
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Piedmont soil
Figure 2D: Box plots of arsenic concentrations in soil cores collected from six sites near Mooresville, NC
as compared to arsenic concentrations in top -soil, horizon -A soil, and horizon-C soil across NC reported
in USGS study of soil data (Smith et al., 2013). The range of mean values of arsenic in different Georgia
Piedmont soils (Albright, 2004) is marked. While arsenic concentrations of some soil cores samples are
higher than that of the background soil in NC, they are consistent with arsenic concentration expected in
soils overlying felsic rocks.
33

L
' C
ca a�
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L
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cv -� CL
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o 1-
0 M {n
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0
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as '
m;
V
0 Mean
' V)
U) ' .0 .0 U
� Q. Q C
O
C N
' N'C
0
LO _
1
Sampling sites ; Background NC soils
Figure 8-1: Box plots of arsenic concentrations in soil cores collected from six sites near Mooresville, NC
as compared to lead concentrations in top -soil, horizon -A soil, and horizon-C soil across NC reported in
USGS study of soil data (Smith et al., 2013).
47

r1.
Cd
O
40
Krk
20
10
[C
u
U)
a)
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aa)
o
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a)
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J
T
Background NC soil
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;
'
'
G
o
0
Y
o
D_
G
0
�
Y
(1)
°'
'
o
Piedmont soil
Figure 2J.• Box plots of cobalt concentrations in soil cores collected from six sites near Mooresville, NC
as compared to cobalt concentrations in top -soil, horizon -A soil, and horizon-C soil across NC reported
in USGS study of soil data (Smith et al., 2013). The mean value of cobalt in Georgia Piedmont soils
(Albright, 2004) is marked. While cobalt concentrations of some soil cores samples are higher than that
of the background soil in NC, they are consistent with cobalt concentration expected in soils overlying
felsic rocks.
39

CD
E
C
L
C
t�
C
0
0
Al
40
35
30
25
20
15
10
5
0
C
O C 'a M
E M c
0 E E
Z O L N
� Z 0 LU �
J M CO 70
a
41 J 0 =S
s
Cn Cn
N
N
.N
N
0
O
N
.0+
+
0
a
O
V
C
N
E
�N
.o
0
LO
0
_
=
I95%CJ.
Mean
Sampling sites ; Background NC soils
Figure 8-5: Box plots of cobalt concentrations in soil cores collected from six sites near Mooresville, NC
as compared to lead concentrations in top -soil, horizon -A soil, and horizon-C soil across NC reported in
USGS study of soil data (Smith et al., 2013).
51