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Home My WebLink About7407_Pitt_C&DLandfillInc_CDLF_Phase1_Phase2_Dec2021GW_FID1704426_20220809DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA DENR USE ONLY ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #: NC DENR I IEnvironmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): Smith Gardner, Inc. Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Seth C. Rickerts, P.G. E-mail: Seth@smithgardnerinc.com Phone: 919-828-0577 x 135 NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006) C&D Disposal, Inc. 802 Recycling Lane. Greenville, NC 74-07 .0500 December 8-9 & 15-16, 2021 27834 Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring ❑X Detection Monitoring ❑ Assessment Monitoring Corrective Action of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells ❑ Groundwater monitoring data from private water supply wells ❑ Leachate monitoring data El water monitoring data Methane gas monitoring data Corrective action data (specify) Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. ❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Seth C. Rickerts, P.G. Project Geologist 919-828-0577 x 135 64gVWW-tative Name (Print) Title (Area Code) Telephone Number 8/8/zuzz U4WScan G. 21�1cc�s Wk978EA4E6... Date 14 N. Boylan Ave. Raleigh, NC 27603 Facility Representative Address F-1370 NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 Affix NC Licensed/ Professional Geologist Seal Ili PIP .} "G EN EAR- 8//222 2758 CLOG`.X DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA This page intentionally left blank. DocuSign Envelope ID: lE49C9C5-lEA4-40EE-BA46-8A724DF270DA December2021 Groundwater Monitoring Report C6D Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 G 7407- CDLF- 2009 Prepared for: COD Disposal, Inc. 802 Recycling Lane Greenville, North Carolina 27834 August 2022 Prepared by: NC LICAU-00 (ENGINEERING) SMITH+GARONER 14 N. Boylan Avenue, Raleigh NC 276N3 1919.828.0577 PRINTED ON M. RECYCLED PAPER 0 2022 Smith Gardner, Inc. This document is intended for the sole use of the client for which it was prepared and for the purpose agreed on by the client and Smith Gardner, Inc. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA This page intentionally left blank. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA December2021 Groundwater Monitoring Report CGD Disposal, Inc. NC Solid Waste Permit 7407-CDLF-2001 G 7407- CDLF- 2009 Prepared For: CGD Disposal, Inc. Greenville, North Carolina S+G Project No. EJERECYCLING-21-2 DocuSigned by: d�, G- 2,�"5 E M8305CMEME6... Seth C. Rickerts, P.G. Project Geologist N C A p DocuSigned by: Q. Sw,r�f , DB9779EBA711F488.a O4� �iCENS�I`O 7 EA6AJA, .. ��' 8/ 12 22 Joan A, Smyth, P.G. Senior Hydrogeologist UO Loy ram;, August 2022 NCLIC.NO.F-1370 (ENGINEERING) SMITH °-GARDNER 14 N. Boylan Avenue. Raleigh NC 27603 1919.828.0577 DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA This page intentionally left blank. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA CGD Disposal, Inc. NC Solid Waste Permit No. 7407- CDLF- 2001 G 7407- CDLF- 2009 December2021 Groundwater Monitoring Report Table of Contents Page 1.0 INTRODUCTION................................................................................................................... 1 2.0 SITE GEOLOGY.................................................................................................................... 1 3.0 SAMPLING LOCATIONS...................................................................................................... 1 4.0 SAMPLING PROCEDURES.................................................................................................. 2 5.0 FIELD & LABORATORY RESULTS....................................................................................... 2 5.1 Field Results..............................................................................................................2 5.2 Laboratory Analysis................................................................................................... 2 5.3 Laboratory Results....................................................................................................3 5.3.1 Inorganic Constituents..................................................................................3 5.3.2 Organic Constituents....................................................................................4 5.3.3 Surface Water Results..................................................................................4 6.0 GROUNDWATER CHARACTERIZATION............................................................................... 4 7.0 CONCLUSIONS....................................................................................................................4 FIGURE Figure 1 Groundwater Potentiometric Map TABLES Table 1 Groundwater Elevation Table 2 Field Parameters Table 3 Monitoring Results Table 4 Velocity and Conductivity Data APPENDICES Appendix A Well Logs Appendix B Laboratory Analytical Report Appendix C Time Vs. Concentration Graphs CSD Disposal, Inc. December 2021 Groundwater Monitoring Report August 2022 Table of Contents Page i DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA This page intentionally left blank. DocuSign Envelope ID: lE49C9C5-lEA4-40EE-BA46-8A724DF270DA 1.0 INTRODUCTION C&D Disposal, Inc., located at 802 Recycling Lane, Greenville, North Carolina, operates a C&D landfill under Solid Waste Permit #7407- CDLF- 2001 and #7407- CDLF- 2009. The site is currently required to submit semi-annual groundwater monitoring reports to NCDEQ. The facility contains two unlined construction & demolition (C&D) landfill units. Phase 2 is currently active. Phase 1 has ceased accepting waste and is partially closed, with final closure planned for late 2022. The Facility was developed in two non-contiguous footprints, Phases 1 and 2 approximately midway between US 264, i.e., a localized topographic divide, and Grindle Creek. The phases became operational in May 2001 and August 2009, respectively. Phase 1 was the regional repository for flood -damage debris after Hurricane Floyd in 1999. Phase 2 was a staging area, where flood -debris was stored temporarily. Both areas were used for agriculture, and a former railroad corridor traverses the site, including the Phase 2 footprint. This report presents the results from the semi-annual monitoring event conducted June 8-9 & 23-24, 2021 and includes a field procedure summary, laboratory analyses, summary tables and groundwater characterization. 2.0 SITE GEOLOGY Historical literature and available geologic maps indicate that C&D Landfill, Inc. sits within the NC Coastal Plain. The coastal plain is characterized as an eastward thickening wedge of sedimentary layers that alternate between sandy aquifers and aquitard. Information taken from The Geologic Map of North Carolina, 1985 shows that the C&D landfill is underlain by the Yorktown Formation, which is described as "fossiliferous clay with varying amounts of fine-grained sand, silty sand, sandy silt, silty clay, and blueish gray shell material". Groundwater in the upper -most aquifer generally flows through unconsolidated sediments. Recharge occurs generally in the northern portion of the site and is limited on slopes. Groundwater flows generally south where it discharges into tributaries of Grindle Creek. The groundwater potentiometric surface generally reflects a subdued expression of the surface topography. Local conditions are considered typical for the coastal plain region. Ground water depths generally range from 3 ft to 12 ft below ground surface (bgs) across the facility. There are minor seasonal variations in the flow pattern, but overall flow direction is consistent. 3.0 SAMPLING LOCATIONS The groundwater monitoring network consists of eighteen shallow and four deep wells totaling (22) groundwater monitoring wells. MW-1S (upgradient of phase 1); MW-1D, MW-2D, MW-2S, MW-3D, MW-3S and MW-3A, MW-4, MW-5, MW-6, MW-7, and MW-8 (downgradient of phase 1); MW-9A, MW-16, and MW-17 (upgradient of phase II); MW-10, MW-11, MW-12S, MW-13, MW-14D, MW-14S, and MW-15 (downgradient of phase II); the network also includes four surface water CGD Disposal, Inc. December 2021 Groundwater Monitoring Report August 2022 Page 1 DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA locations (SW-1, SW-2, SW-3, and SW-4). MW-5, SW-1, and SW-2 were unable to be sampled by Environment 1 personnel this event. Figure 1 illustrates sampling locations. Available well logs for the groundwater monitoring wells are included in Appendix A. 4.0 SAMPLING PROCEDURES Environment 1 personnel conducted the monitoring network sampling event December 9-10 & 15-16, 2021. Sampling methods followed the protocol outlined in the North Carolina Water Quality Monitoring Guidance Document for Solid Waste Facilities (DENR, DWM) and the approved site Water Quality Monitoring Plan'. The monitoring network includes wells: MW-1s, MW-1d, MW-2s, MW-2d, MW-3A, MW-3s, MW-3d, MW-4, MW-5, MW-6, MW-7, MW-8m NW09a, MW-10, MW-11, MW-12s, MW-13, MW-14s, MW-14d, MW-15, MW-16 and MW-17, as well as surface water monitoring points SW-1 through SW-4. Monitoring wells MW-1s and MW-1d serve as the upgradient background locations for the site. Each well was gauged to determine groundwater depth and then purged three well volumes or until dry. Groundwater depth from this event, as well as other well details are presented in Table 1. Samples were collected by Environment 1, Inc. in laboratory prepared containers for the specified analytical procedures. Groundwater samples and quality control blanks, were properly preserved, placed on ice and transported to the laboratory facility within the specified hold times for each analysis. 5.0 FIELD 0 LABORATORY RESULTS 5.1 Field Results Temperature, pH, turbidity, specific conductance, ORP, and dissolved oxygen were measured in the field at the time of sampling via direct read instruments. Field results from this sampling event are presented in Table 2. All wells exhibited turbidities less than 10 NTUs except for MW-11 (46.1 NTU) and MW-14S (17.6 NTU). 5.2 Laboratory Analysis Ground and surface water samples were transported to Environment 1, Inc., a North Carolina certified laboratory for metals and Appendix I I VOC analysis. Samples were also analyzed for additional C&D inorganics, alkalinity, sulfide, chloride, total dissolved solids and tetrahydrofuran. The laboratory report including the full list of analytes tested for is presented as Appendix B. 1 Water Quality Monitoring Plan Amendment, C&D Landfill, Inc., CDLF (Phases 1 and 2) prepared for C&D Landfill, Inc., by David Garrett and Associates, Revised May 2008. CGD Disposal, Inc. December 2021 Groundwater Monitoring Report August 2022 Page 2 DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA 5.3 Laboratory Results Analytical results were compared to Rule 15A NCAC 2L.0200 (21- Standard) and/or the NC Groundwater Interim Maximum Allowable Concentration. Surface water results were compared with the NCAC 2B Standard for Class C waters (213 Standards). Most constituent concentrations were either below the method detection limit (MDL) or were reported as "J-values". J-values are identified by the laboratory as "estimated values between the MDL and the MRL". 5.3.1 Inor0anic Constituents Six inorganic constituents were reported at concentrations above their 2L Standard this event. • Antimony (MW-14S); • Arsenic (MW-3A, MW-3S, MW-6, MW-7, MW-8, MW-12S, MW-14S, and MW- 16); • Barium (MW-3S and MW-6); • Chromium (MW-3A, MW-3S, MW-6, MW-7, MW-8, MW-10, MW-12S, MW- 14S, and MW-16) • Iron (MW-1 D, MW-1 S, MW-2D, MW-2S, MW-3A, MW-3S, MW-4, MW-5, MW- 6, MW-7, MW-8, MW-9A, MW-11, MW-12S, MW-13, MW-14S, MW-15, MW- 16, and MW-17); and • Manganese (MW-1 S, MW-2S, MW-3A, MW-3S, MW-4, MW-5, MW-6, MW-7, MW-8, MW-9A, MW-10, MW-11, MW-12S, MW-13, MW-14S, MW-15, MW- 16, and MW-17). Two inorganic constituents were reported at concentrations above their GWP standard this event. • Cobalt (MW-1S, MW-3A, MW-3S, MW-6, MW-7, MW-8, MW-10, MW-12S, MW-13, and MW-14S); and • Vanadium (MW-3S, MW-6, MW-12S, MW-14S, MW-15, and MW-16). As MW-1S and MW-1D are upgradient of Phase 1 and MW-17 is upgradient of Phase 2, exceedances in these wells indicate that detected constituents may be due to naturally occurring conditions. Detections are summarized in Table 3. CGD Disposal, Inc. December 2021 Groundwater Monitoring Report August 2022 Page 3 DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA 5.3.2 Organic Constituents Five organic constituents were detected above their 2L Standards during this sampling event. Detections are summarized in Table 3. • 1,2-Dibromoethane (MW-3A); • 1,4-Dioxane (MW-1S, MW-2S, MW-3A, MW-3S, MW-6, MW-7, MW-8, MW- 10, MW-11, MW-12S, MW-13, MW-14S, MW-15, and MW-16); • Benzene (MW-10, MW-12S, and MW-14S); • Naphthalene (MW-6); and • Vinyl Chloride (MW-10, MW-12S, MW-13, MW-14S, and MW-16). 5.3.3 Surface Water Results No inorganic or organic constituents were detected above their NC213 standards in surface water samples collected this event. Surface water detections are provided on Table 3. 6.0 GROUNDWATER CHARACTERIZATION A potentiometric surface map was prepared from groundwater data from the most recent sampling event. The data indicates that groundwater is flowing generally south towards tributaries of Grindle Creek. This is consistent with groundwater flow patterns previously reported for the site. The potentiometric surface map is included as Figure 1. Groundwater flow velocities during the sampling event were calculated using the equation: V = Ki/n where: K = hydraulic conductivity i = groundwater gradient n = porosity Calculated groundwater velocities ranged from 0.00053 ft/day (MW-11) to 0.02320 ft/day (MW- 10) averaging 0.02071 ft/day. Flow velocities and calculated gradients are included in Table 4. 7.0 CONCLUSIONS Analytical results are generally consistent with past sampling events. Iron and manganese were detected in most samples collected this event, including in background wells above their respective NC21- and NCGWP standards. Due to the low turbidity values, and the exceedances noted in upgradient wells, it is likely that some of these inorganic exceedances can be attributed to naturally occurring metals in the soil. CGD Disposal, Inc. December 2021 Groundwater Monitoring Report August 2022 Page 4 DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA 1,4-Dioxane, benzene, and vinyl chloride were detected again in multiple monitoring wells above their NC2L standards this sampling event. Although not exceeding regulatory limits, 1,2- Dichloroethane and 1,2-cis-Dichloroethylene were present in multiple wells this event. The continued presence of these organochlorides as well as vinyl chloride provide some evidence that reductive dichlorination via natural attenuation may be occurring onsite. The exceedance of the hydrocarbon naphthalene is unique to this event. This may be due to laboratory or sampling error and will continue to be monitored. A Corrective Action Plan to address organic exceedances has been submitted to the NCDEQ and is under review. This plan included an evaluation of natural attenuation that indicated that natural attenuation is occurring at the site. Once approved, the plan will be implemented. The next groundwater monitoring event is scheduled for Spring 2022. A report with laboratory analysis will be submitted to NCDEQ in accordance with 15A NCAC 13B .0544. CGD Disposal, Inc. December 2021 Groundwater Monitoring Report August 2022 Page 5 DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA This page intentionally left blank. CGD Disposal, Inc. December 2021 Groundwater Monitoring Report August 2022 Page 6 DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA FIGURES December2021 Groundwater Monitoring Report CEO Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 & 7407- CDLF- 2009 DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA This page intentionally left blank. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA MW-17 TOC= 20.74 DTW= 8.90 GWE= 11.84;, - MW-16r TOC= 19.16 DTW= 9.21 GWE= 9.95 MW-9A= TOC= 20.58 DTW= 6.80 GWE= 13.78 MW-10 MW-15 TOC= 16.61 TOC= 19.67 DTW= 4.41 DTW= 8.93 ` GWE= 12.20 GWE= 10.74 ` MW-145 TGWE= C= 16.60 TW= 8.13 8.47 MW-14D* TOC= 17.45 DTW= 7.00 GWE= 10.IO 4 MW-13 TOC= 20.69 DTW= 10.27 GWE= 10.42 SW-3 5 - MW-12S TOC= 16.18 DTW= 5.56 GWE= 10.62 &iMW-3D* TOC= 22.83 DTW= 13.42 GWE= 9.41 BMW-1D* TOC= 21.14 DTW= 9.55 GWE= 11.59 LEGEND EXISTING 10' CONTOUR s5o - (SEE REFERENCE 2) EXISTING 2' CONTOUR (SEE REFERENCE 2) APPROXIMATE PROPERTY LINE (SEE REFERENCE 1) FLOOD HAZARD AREAS ZONE AE (SEE REFERENCE 3) APPROXIMATE GROUNDWATER SURFACE CONTOUR . SW-1 SURFACEW,4TER MONITORING LOCATION MW-8* INDICATES ELEVATION NOT USED FOR CONTOURING M W-1 A GROUNDWATER MONITORING WELL TOC TOP OF CASING ELEVATION DTW DEPTH TO WATER GWE GROUNDWATER ELEVA77ON MW-1S TOC= 20.91 DTW= 9.32 GWE= 11.59 mom MW-11 TOC= 14.4.9 DTW= 3.74 RO ME= 10.75 MW-8* TOC= 21.21 ' "DTW= 10.10 . GWE= 11.11 ` MW-3S TOC= 23.02 DTW= 12.68 GWE= 10.34011 ` 4C:�"Y" 45 r �- MW-3A TOC= 21.93 DTW= 11.87 GWE= 10.06 MW-4 TOC=18.42 DTW= 7.60 GWE=10.82 NOTES 1. GROUNDWATER DATA COLLECTED BY ENVIRONMENT 1, INC. DECEMBER 2021. REFERENCES 1. PARCEL BOUNDARIES FROM PITT COUNTY GIS DEPARTMENT. 2. FLOOD HAZARD INFORMATION FROM NORTH CAROLINA FLOODPLAIN MAPPING PROGRAM, FEMA FIRM MAP NO. 3720562800L, EFFECTIVE DATE JUNE 19, 2020. 3. AERIAL IMAGERY DATED 2016 FROM PITT COUNTY GIS DEPARTMENT 0 200' 400' AMW-70/1 TOC= 19.40 ' DTW= 8.91 ' GWE= 10.49 /IDTW=29.;6 MW-b TOC= 003 GWE= 10.07 , _ MW-2D* % MW-2S - TOC= 21.80 TOC= 21.44 DTW= 13.14 DTW= 11.57 GWE= 8.66 GWE= 9.87 IF 0 SW-2 'A *1' 1. N co Oo m w w a w z z W 0 (n N Q N Z w w U W U � N CV 0 N C, U Q a L� W Z U CV z o c LAJ [- CV Z c LL. W .. J W W G = ... W � Lo Q o 0 z 0 cm 22 Smith Gardn . Inc. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA This Page Intentionally Left Blank DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA TABLES December 2021 Groundwater Monitoring Report CEO Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 & 7407- CDLF- 2009 DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA This page intentionally left blank. DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA SMITh GARDNER .• - C.; .No V . • D. . Well Well Installation Date Well Diameter (inches) Total Well Depth (ft bgs) Ground Surface Elevation (ft amsl TOC Elevation (ft amsl) Depth toElevation Water (ft) Water Table (ft bgs) Screen Interval (feet bgs) M W-1 D 10/ 13/ 2000 2 33.75 17.4 1 21.14 9.55 11.59 40- 50 M W-1 S 5/ 2/ 2001 2 17.21 17.59 20.91 9.32 11.59 3-13 MW-2D 10/11/2000 2 38.17 17.97 21.8 13.14 8.66 39-49 MW-2S 5/3/2001 2 16.57 18.45 21.44 11.57 9.87 3-13 M W- 3A 8/ 10/ 2009 2 23.44 19.13 21.93 11.87 10.06 5- 20 MW-3D 10/13/2000 2 52.3 19.37 22.83 13.42 9.41 40-50 MW-3S 8/6/2007 2 22.24 19.37 23.02 12.68 10.34 8-18 M W- 4 5/ 3/ 2001 2 15.98 14.83 18.42 7.6 10.82 3-13 MW-5 11/19/2002 2 9.5 14.8 17.9 - - 3-18 M W- 6 5/ 3/ 2001 2 16.65 16.87 20.03 9.96 10.07 3-13 M W- 7 5/ 3/ 2001 2 16.33 16.03 19.4 8.91 10.49 3-13 MW-8 11/5/2002 2 20.26 18.3 21.21 10.1 11.11 3-18 M W- 9A 8/7/2009 2 23.17 17.64 20.58 6.8 13.78 5- 20 M W-10 8/ 6/ 2009 2 22.73 14.16 16.61 4.41 12.20 5- 20 MW-11 8/6/2009 2 23.84 11.60 14.49 3.74 10.75 5-20 MW-12S 8/7/2009 2 22.93 1 13.72 16.18 5.56 10.62 5-20 MW-13 8/7/2009 2 20.68 18.12 20.69 10.27 10.42 5-20 MW-14D 12/17/2002 2 41.92 14.54 17.45 7 10.45 35-40 M W-14S 12/ 18/ 2002 2 23.12 13.9 16.6 8.13 8.47 5- 20 M W-15 12/ 18/ 2002 2 22.14 13.9 19.67 8.93 10.74 5- 20 MW-16 6/16/2017 2 22.73 NA 19.16 9.21 9.95 NA M W-17 12/ 9/ 2002 2 22.25 18.18 20.74 8.9 11.84 5- 20 Note: 1. Well installation, depth, elevations, and screened interval from David Garrett Boring Logs E�.3U Dfe07/2YM MRgeds\Gard&dalvtntoir#2Girrl daNtntairxOFperts\EERLydirr,4.Fd12321F1I2021EERrydirUTaHE&AEx DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA This page intentionally left blank. DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA SMITh GARDNER Ffdd Pawdas Bf.3U DAe07/2YM 7••- .- . • • • d/ Well ID pH (SU) Temperature (OCelsius) Specific Conductivity (uMhos/cm) Dissolved Oxygen ORP (mv) Turbidity (NTU) M W-1 D 7.5 15 360 0.17 107 1.96 M W-1 S 6.6 14 1732 0.93 135 7.02 MW-2D 8.2 13 441 0.63 110 6.07 M W- 2S 6.6 15 1764 0.87 127 7.93 M W- 3A 7 16 2689 0.87 136 7.91 MW-3D 7.8 17 528 0.13 106 5.79 M W- 3S 6.9 17 3703 0.77 138 2.12 MW-4 6.5 13 376.3 0.44 177 8.61 MW-5 - - - - - - MW-6 6.9 15 2641 1.85 156 7.57 M W- 7 6.9 15 2429 0.65 163 6.59 MW-8 7.1 13 3574 1.87 174 8.93 M W- 9A 6.7 17 1014 0.57 123 8.83 MW-10 6.7 15 2497 1.32 146 5.19 M W-11 7.1 17 1020 0.31 129 46.1 MW-12S 6.8 16 4077 0.63 167 3.15 M W-13 6.4 17 1472 0.83 122 8.67 MW-14D 7.8 20 564 0.64 110 2.37 MW-14S 6.8 19 332 1.52 143 17.6 MW-15 6.2 20 1303 0.58 122 6.51 M W-16 6.3 21 1902 1.96 136 7.21 M W-17 6 19 663 1.82 152 5.93 SW-1 - - - - - - SW-2 - - - - - - SW- 3 7.4 7 1148 4.87 139 22.6 SW-4 7.7 9 358 3.73 141 29.9 Note: 1. Field Parameters measured by Environment 1 on December 8-9, 15-16, 2021 2. Bold indicates a turbidity exceeding 10 NTU. 3. MW-5, SW-1, and SW-2 were unable to be sampled this event. [f.T.Tti1u uuf►ZtT,Teililn a��::an\.::Tlli�[Irlfa7�i\rIN.I�I�.::TIIii7CiC3!�'J DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA This page intentionally left blank. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA SMITH GARDNER T2de3 M ntcnrgP,esdts E1ERDydingLa-dll Dae Er8-9,15-16, 2M1 Monitoring Results Station Name Units NC2L NC2B NC2B-P MW-11D MW-1S MW-2D MW-2S MW-3A MW-31D MW-3S MW-4 I MW-6 I MW-7 I MW-8 I MW-9A I MW-10 I MW-11 Sample Date 12/8/2021 12/8/2021 ###### 12/8/2021 12/8/2021 12/8/2021 12/8/2021 12/9/2021 1 12/9/2021 1 12/9/2021 1 12/9/2021 12/15/2021 12/15/2021 12/15/2021 Furans Tetrahydrofuran ug/I I I 1 1 14.8 1 4.77 1 1 9.24 1 13.5 1 1 24.8 1 1 15.2 1 18.1 1 22.4 1 19.7 17.43 Metal s Antimony ug/I 1 0.21 J 0.16J 0.091 0.16J 0.21 J 0.14J 0.04J 0.2J 0.04J 0.06J 0.15J Arsenic ug/I 10 150 0.69 J 5 0.54 J 6.9 18 0.12 J 25 0.62 J 17 28 26 0.54 J 4.6 J 4.9 J Barium ug/I 700 21000 20.5 249 16 190 405 11 771 70.4 713 571 620 141 307 65.5 Beryl I ium ug/I 4 6.5 0.09 J 0.04 J 0.06 J 0.04 J 0.05 J 0.09 J 0.04 J 0.05 J 0.04 J 0.02 J 0.04 J 0.05 J Cadmium ug/I 2 0.111 Chromium ug/I 10 0.2 J 10 0.32 J 4.2 J 12 25 1.5 J 13 12 25 0.99 J 15 1.9 J Cobalt ug/I 1 4 0.05 J 1.6 0.08 J 0.84 J 4.4 0.02 J 3.6 0.15 J 3.3 14 2.7 0.15 J 1.3 0.64 J Copper ug/I 1000 3.1 0.26J 0.89J 0.36J 0.3J 0.22J 0.06J 0.41 J 0.18J 0.191 0.2J 0.15J 0.08J 0.18J 0.11 J Iron ug/I 300 515 3048 395 10649 25332 248 11313 5000 18418 52259 34503 9213 142 18251 Lead ug/I 15 25 0.05J 0.46J 0.15J 2.3J 0.14J 0.06J 0.15J 0.05J 0.06J 0.05J 0.04J 0.05J Manganese ug/I 50 21 183 15 495 827 23 1220 56 765 727 765 479 172 273 Nickel ug/I 100 88 0.24J 3.8J 0.34J Ili 2.2J 0.191 2.9J 0.2J 5.7J 1.91 1.7J 0.32J 1.11 0.91 J Selenium ug/I 20 5 0.21 J 1.91 11 0.85J 1.4J 0.18J 1.11 0.86J 0.84J 0.21 J 1.2J 0.6J Thallium ug/I 2 0.47 0.04 J 0.12 J 0.02 J 0.04 J 0.11 Tin ug/ I 2000 Vanadium ug/I 7 0.34 J 3 0.16 J 2 3 0.111 8 2 10 2 4 1 7 0.95 J Zinc u /I 1 1000 1 81 1 1.4J 1 3.1 J 1 11 0.8J 1.4J 21 1.6J 1.4J 0.8J 1.4J 1.3J 2.4J 5.2J 1.2J Nutrients Nitrite as N m /I I I 1 1 0.22 1 0.1 1 1 0.18 1 1 1 1.09 1 1 0.16 1 0.19 1 0.27 Other 1,2- cis- Dichloroethylene ug/I 70 1,2-Dibromoethane ug/I 0.02 0.04 J 1,2-Dichloroethane ug/I 0.4 37 0.02 J 0.09 J 0.06 J 0.03 J 0.02 J 0.25 0.05 J 1,2-Dichloropropane ug/I 0.6 0.04 J 0.04 J 0.15 J 1,4-Dioxane ug/I 3 70.1 38.5 88.2 147 35.7 19.2 81.5 7.16 8.79 2,4- Dichlorophenoxy Acetic Acid ug/I 70 Acenaphthene ug/I 80 2.85 J 6.24 J 12.94 3.09 J Acetone ug/I 6000 2000 12.2 J 12.6 J 15 J Alkalinity, Total mg/I 356 552 190 680 1020 242 1660 134 1410 1450 1640 170 51 520 Benzene ug/I 1 0.93 J 0.39 J 2.03 Carbon Disulfide ug/I 700 0.36 J Chloride mg/I 15 84 13 79 131 21 230 11 116 101 169 27 73 88 Chlorobenzene ug/I 50 0.32 J Dibenzofuran ug/I 4.91 J Dichlorodifluoromethane ug/I 1000 0.56 J Ethylbenzene ug/I 600 0.26 J Methyl Ethyl Ketone (2-Butanone) ug/I 750000 Naphthalene ug/I 6 95 1.09 J Sulfate mg/I 31.6 326 26 169 257 6.3 99.5 48.8 76.7 39.8 129 306 583 269 Sulfide ug/I 188 J Toluene ug/I 600 11 0.5 J Total Dissolved Solids mg/I 220 1400 310 1100 1600 340 2000 260 1600 1500 2000 620 1700 840 Vinyl chloride ug/I 0.03 0.53 Xylenes u /I 1 500 NOTES: ug/L = micrograms per liter BOLD = Constituent exceeds NCA002L or GWP regulatory limits BaD = Constituent exceeds NCI CO2B or 2B Protection regulatorylimits J = Lab estimated concentration BDL =constituent is below laboratory detection limits NA= Not Analyzed By33 DteM/291M R RgetElGandkdErMrttairrJ, 23xrd&dErWtairgRp3tsi EHbcydirrj4 Fdl M Fdl 2M1 E9R8c}dirgTEde As( DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA SMITH GARDNER T2de3 M ntcnrgP,esdts ElBiDydingLa dull Dae be-8-9,1<r16,2021 Monitoring Results Station Name jUnits I NC21- I NC2B I NC2B-P I MW-11D I MW-12S I MW-13 I MW-14D I MW-14S I MW-15 I MW-16 I MW-17 I SW3 I SW-4 Sample Date 12/ 8/ 2021 12/ 15/ 2021 12/ 15/ 2021 12/ 16/ 2021 12/ 16/ 2021 1 12/ 16/ 2021 12/ 16/ 2021 1 12/ 16/ 2021 12/ 9/ 2021 1 12/ 9/ 2021 Furans Tetrahydrofuran ug/I I I 1 1 14.8 1 59.3 1 11.1 1 70.7 1 3.09 1 4.58 Metal s Antimony ug/1 1 0.29 J 0.09 J 0.06 J 1.1 0.19 J 0.19 J Arsenic ug/I 10 150 0.69 J 57 10 0.5 J 86 6.3 14 1.9 J 3 J 0.5 J Barium ug/I 700 21000 20.5 572 171 8.1 J 557 273 488 75.2 161 66.7 Beryllium ug/I 4 6.5 0.04 J 0.04 J 0.02 J 0.06 J 0.14 J 0.06 J 0.05 J 0.02 J 0.22 J Cadmium ug/I 2 0.06 J 0.06 J Chromium ug/I 10 0.2 J 67 2.9 J 0.15 J 52 8.2 25 1.6 J 7.1 0.66 J Cobalt ug/I 1 4 0.05 J 4.1 1.4 0.04 J 3.5 0.56 J 0.81 J 0.16 J 1.3 1.6 Copper ug/I 1000 3.1 0.26 J 0.14 J 0.32 J 0.31 J 0.24 J 0.69 J 0.26 J 0.24 J 0.31 J 11 Iron ug/I 300 515 1473 27923 26J 6585 21238 45845 2156 Lead ug/I 15 25 0.05 J 0.06 J 0.18 J 0.06 J 0.16 J 0.74 J 0.09 J 0.21 J 0.18 J 0.89 J Manganese ug/I 50 21 415 190 2J 805 248 494 111 Nickel ug/I 100 88 0.24J 4.5J 2.8J 0.35J 4.7J 1.3J 1.8J 0.46J 0.91 0.991 Selenium ug/I 20 5 0.21 J 2.8J 2J 0.3J 2.3J 1.8J 2J 0.61 J 0.46J 0.39J Thallium ug/I 2 0.47 0.09 J 0.28 J 0.06 J Tin ug/I 2000 0.62 J Vanadium ug/I 7 0.34 J 48 4 0.5 J 11 14 14 3 0.95 J 1 Zinc u /I 1 1000 1 81 1 1.4J 1 2.2J 1 14 1 2.3J 1 1.6J 1 60 1 1.6J 1 3.2J 1 3.5J 1 11 Nutrients Nitrite as N m /I I I 1 1 0.22 1 1 1 0.13 1 0.05 Other 1,2- cis- Dichloroethylene ug/1 70 0.42 J 2.2 J 0.64 J 1,2-Dibromoethane ug/I 0.02 1,2-Dichloroethane ug/I 0.4 37 0.18 J 0.16 J 0.14 J 0.13 J 0.02 J 1,2-Dichloropropane ug/I 0.6 0.111 0.05 J 0.05 J 0.06 J 1,4-Dioxane ug/I 3 34.5 9.74 41.9 4.47 61.4 12.3 2,4- Dichlorophenoxy Acetic Acid ug/I 70 1.04 J 3.24 Acenaphthene ug/I 80 Acetone ug/I 6000 2000 17.9 J 22.8 J 9.81 J 28.8 J Alkalinity, Total mg/I 356 1660 584 243 1450 244 664 43 Benzene ug/I 1 2.96 0.91 J 1.63 0.47 J Carbon Disulfide ug/I 700 Chloride mg/I 15 254 59 16 276 53 101 4 Chlorobenzene ug/I 50 Dibenzofuran ug/I Dichl orodifl uorom ethane ug/I 1000 Ethylbenzene ug/I 600 0.22 J 0.62 J 0.38 J Methyl Ethyl Ketone (2-Butanone) ug/I 750000 2.79 J Naphthalene ug/I 6 5.11 J 0.78 J Sulfate mg/I 31.6 21.6 371 304 152 319 334 Sulfide ug/I 209 J Toluene ug/I 600 11 0.58 J 2.06 Total Dissolved Solids mg/I 220 2100 960 300 1400 640 1200 410 Virl chloride ug/I 0.03 2.09 1.74 2.06 0.15 J X lenes ug/I 1 500 1 1 1 1 1.7 J NOTES: ug/L = micrograms per liter BOLD = Constituent exceeds NCA002L or GWP regulatory limits BaD = Constituent exceeds NGI CO2B or 2B Protection regulatorylimits J = Lab estimated concentration BDL =constituent is below laboratory detection limits NA= Not Analyzed By33 DteM/291M M RgetElGandkdErMrttairrJ, 23xrd&dErWtaircJRp3tsi EHbcydirrj4 Fdl M Fdl 2M1 EER8c}dircJTEde As( DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA SMITH GARDNER Ce o :.. M. . . . . I !r -- "m Hydraulic Hydraulic Velocity Effective Weil Conductivity Gradient v Porosity n (feet/day) i (feet/day) M W- 3A 0.805 0.08 0.004 0.03924 MW-10 0.116 0.05 0.010 0.02320 MW-11 0.009 0.04 0.002 0.00053 MW-12S 1 0.322 1 0.06 1 0.004 1 0.01986 Note: 1. Hydraulic conductivity and effective porosityvalues from historical Wood Inc. groundwater monitoring reports 2. Velocity calculated based on the modified Darcyequation: v=(KI)/n W.3j ate07/29M MRgedslGard&daN,tntairr,2C3aniAdErMntcnrgRpotsl EERL)dir#4 Fdl M Fdl MEEFtqdirgIdesAx DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA This page intentionally left blank. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA Appendix A Well Logs December 2021 Groundwater Monitoring Report CEO Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 & 7407- CDLF- 2009 DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA This page intentionally left blank. DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett, P. G., P.E. Boring No. AlfW-I d Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of 2 Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 17.40 �t Equipment CME 750 Drilling Method 3-114" Hollow AugeisNater Level, TOB NA sz Date Started iom2100 Date Ended 10/13/00 Water Level, 24 Hr. 4.8 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 4.8 Comments Plowed field. cool sunny weather Total Depth mo Date of Observation 1omwoo Elegy. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction SAND: Medium dense buff -white, slightly silty, I I I I I I I I I I I I I I I moist 16,00 I I I I I I I I I I I I - - 14.00 I I I I I I I I 1 I I l I I I - - - 3.5 3 i i I i I i S i I 4.0 SAND: Loose, green -gray, silty and clayey, wet 4 SM 5 I I I I I I I I I I -- - 12.00 t I I I I I I I I i S t I I I I I I I I I 7.5 - - 10.00 ' I I ' ' ' —Y SILT: Medium stiff, gray -green, fine sandy and clayey, with heavy shell hash (turritellas) wet, 8.5 2 i i i i ; —_ medium plasticity 1 SM 8.00 i i i i i — 1 I I— I I I I I i I I I I — 6.00 4WV I I I I I I I I I I I S ! S 5 t I I I I I I I I I I — - — 4.00 1 I I I I I I I I t I I I 1 1 I I I I I I — 13.5 3 — I I I I — 4 s I I I I — M L- 1 I I 1 I C L 2,00 1 I I I I — — 0.00 3 I S I I I I 1 I 1 I I I I I I I I I I I I I I I — — — — I I I I 1 I I I I I I 18.5 — 18,5 4 ♦ CLAY: Medium stiff, gray -green, plastic gumbo -2.00 4 clay, moist CL 6 I I I I 1 I I I I I I I I I I I I I I I 4 00 I I I I I I I 1 I I I I I I I I I I I I I I I I I I I I I I I I I I I I I M I I I I I I I 1 I I I I I I I I I I 1 I 23.5 4 I I I 5 I I ' I I ' I CL 7 I I I I I I I I DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett, P. G., P.E. Boring No. A4W--1 d Engineering and Geology Depths in feet, referenced b.g.s. Page 2 of 2 Client and Project CSD Landfill, Inc. (Pitt County) Ground Elevation 17.40 Equipment CME 750 Drilling Method 3-114" Hollow AugelhlVater Level, TOB NA Date Started 10/12/00 Date Ended 10/13/00 Water Level, 24 Hr. 4.8 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 4.8 r.nmmPntG Pinwed field- cool sunnv weather Total DeDth sox Date of Observation 10/16/00 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction -8.00 i i ; i CLAY: Medium stiff, gray -green, plastic gumbo 'ANNULUS GROUTED i f S I I I I I I I 1 I I I I I day, moist -10.00 I I I I I I 1 1 I I I I I I I I I I I I I I I I I I 28.5 3CL I I I I I I I I I I 1 3 -12.00 I I I I 1 I I I I I I I 1 I I I I I I I I 1 I I I 31.5 -14.00 SILTYSAND: Dense, partly cemented, black- - ' ' green speckled, variably clayey, silty, moist, hard — ' layer at 36 to 38 feet, very hard below 45 feet -16.00 I 1 I I I I s -7. -• 33.5 6 22 I I I I ! — SM Bentonite 18 I I I r I I Seal -18.00 I I I 7 I I I I I I I ! t S I I I I I 1 1 I I I I I - - -20.00 3 I 1 f t I I I I I I I I I I I I I I I 1 I I I I I I I I I I I - - 38.5 31 I I I 1 I I I 15 I - SM -22.00 I - 24 I I I I I I I I I I I I I I I 1 I - -24.007. I I I I I I I I I I 1 I - I I I I I I I I 1 1 I l I I I I - Sand Pack I - SM -26.00 1 43.5 501.1— I I ! I I I - I I 1 I I 1 I I I I I 1 I I I 77 0.010" 28.00 i i i i i Slotted I I I 7 I I I I I I Screen -30.00 .JII W I I I i ! I I I I I I I I I I t 48.5 501.5 I I I I I I I I I S 7. SM -32.00 — ' I I I ' I t Boring Terminated at 50 feet DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett, P. G., P.E. Boring No. MW-1 s Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of i Client and Project C8D Landfill, Inc. (Pitt County) Ground Elevation 17.59 Equipment CME 75 Drilling Method 4.11NO ID HSA Water Level, TOB NA sz Date Started 05102/01 Date Ended 05/02/01 Water Level, 24 Hr. NA Drilling Firm Bore & core Logged by David Garrett Stabilized Level 5.59 s Comments Lockino cover with 3.32' stickup Total Depth 13.0 Date of Observation 5/116/01 Elev. SPT Data and Strata Depths. Lithology Description and USCS Code Piez. Construction 1 I I I ! SILTY SAND: Loose, tan -brown, moist [ I I , - Concrete I i I I I pad 16.00 I t I I I • I I I I I SM Bentonite I I I I 1 - Seal 14.00 I I I I I I I I I I I I I I f I I I I I ] i I 1 I - - 12.00— I I I I I I I l } ! I I I I I I I • = - I I I I I I I 3 ! S I I I I I I - - 10.00 I I I I 1 I 8.0 - 0.010" . • . SAND: Loose, tan, fine to medium Slotted 1 Screen I I ! ! $W g.00 ! I 3 I I I I 1 I ! I ! - 6.00 3 5 ! I I I I 1 1 I 1 I I I I I I I I I I I I I I 1 I I I 1 I I I I I I I Boring Terminated at 13 feet DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett, P.G., P.E. Boring No. MW-2d Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of 3 Client and Project C&D Landfill, inc. (Pitt County) Ground Elevation 17.97 Equipment CME 750 Drilling Method 3-718" rotary -mud Water Level, TOB 6.6 a Date Started 1019100 Date Ended 10111100 Water Level, 24 Hr. 7.9 Drilling Firm Bore & core Logged by David Garrett Stabilized Level 7.9 Comments Plowed field. cool sunnv weather Total Degth 70.o Date of Observation 10/16/00 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction F I I I I . ' . • - SAND: Loose, tan -yellow, variably silty sand 16.00 { I I I I I I 1 1 I I I I I I I I I I I I I I I I - I I I I I I I I I I 1 3.5 14.00 3.5 16 ' ' CLAY: Medium stiff, tan range, very sandy, silty, e ; slightly plastic, moist, crumbly CL 8 I i I I i I I i 1 I i I I i I I SM 12.00 I I I l I I I ' I I I I I I I 1 1 I I I I I I I i I 75 i D.00 ' SAND: Medium dense, tan, subangular, f - c well ; graded (boring collapsed at 13.6 feet when casing Bentonite- 8.5 5 i pulled, redrilled with 41l4" hollow stem auger) Cement 6 I f I I I � $p- Grout 8 SM 8.00 I I 1 ! I I I I I I - 6.00 I I I I I I 1 I I I I I I I I I I I I I I I S F E 12.5 - �- -, CLAYEY SILT: Medium stiff, gray -green, fine — sandy, with heavy shell hash (whole turritellas), 13.5 3 — moist, moderately plastic 4 00 3 � I I r I I �— CL- 4 I I I I I ML I I I I 1 t I I I I \— I I I I { I I I I I \- 2.00 I I 1 I \ I I ! I I \ — I I I I I 0.00 i I r I I I I I I 1 1 t I I I \— I I I 1 I 16.5 2 a I I 1 I 2 , I i I i I i I i \— iiL- ML -2.00 3 , I I I I I \— I I 1 I I I I I I I \— I I 1 1 I I I I I I �— I I 1 I I I I I I I \ µ -4.00 I 1 I I I 22.5 CLAY: Medium stiff, gray -green, plastic gumbo I I I I I I I I I I clay, moist 23.5 2 -6.00 2 ' I ' I I I I CL 4 I I I I I DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett, P.G., P.E. Boring No. MW-2d Engineering and Geology Depths in feet, referenced b.g.s. Page 2 of 3 Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 17.97 n Equipment CME 750 Drilling Method 3-7/8" rotarrmud Water Level, TOB 6.6 a Date Started io/woo Date Ended 10/11/00 Water Level, 24 Hr. 7.9 Drilling Firm Bore & core Logged by David Garrett Stabilized Level 7.9 Comments Plowed field. cool sunnv weather Total Depth 70A Date of Observation 1of16/00 Elev. SPT Data and Strata Depths Lithology Description and USCS Code PEez. Construction 1 I I I CLAY: Medium stiff, gray -green, plastic gumbo i f i i i day, moist -8.00 I I I I i I I I I I I I I I I I I I I I -10.00 I I I I I I I I I I I I I I I I f 7 f f 1 28.5 2 I I I I l I I ' I I 2 , I I 1 I I CL 3 I I I I I I I I -12.00 I I I I I I 1 I [ I I I I I I I I I I I I I I l ? i i I I I I I I I I -14.00 I I I I l S i I I I I I I I I I I E S I I I I I I 33.5 _3604 33.5 1 I 1 I 1 I i I i = SILT: Stiff, gray -green, fine sandy, clayey, fi I I I I — - interlayered with sand SM 8 I I I I I — I _- Bentonite — Seal -18.00 7 I I I I I I I I I I - - i 37.0 _ 1 I I I I I , Sand Pack = — SILT: Hard, black -green speckled, clayey, fine ' — sandy, moist, moderately plastic, scattered -20.00 ; I i I i I i I i I — - pelecypod shell hash 38.5 5 ' — ' ' ' — 4 I 1 I I I ML 29 -22.00 I I I I I I I 1 I I I I I I I I 1 I I I - - - - -24 00 I I I I I I I I I I I I I I I I 1 - - = I I I I I I I I I 1 - 0.01 a' - Slotted Screen MIL 43.5 10 26.00 20- 27 I I I I I I I I 1 1 — - -28 00 I I I I I I I I 1 I I I I I I I I I I I I I I I 1 I - = - -30.00 I I I I I I I I I I I I I I I I I I I I 1 I 1 I I _- - — - - 48.5 22 I I I I I I I I I 1 49.038 - 5M Bentonite SAND: Very dense (partly cemented), black -green 501.2 i i i i i speckled, clayey, silty, fine glauconite nodules Seal DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett, P.G., P.E. Boring No. MW-2d Engineering and Geology Depths in feet, referenced b.g.s. Page 3 of 3 Client and Project C&D Landfill, Inc, (Pitt County) Ground Elevation 17.97 Equipment CME 750 Drilling Method 3-7/8" rotary -mud Water Level, TOB 6.6 Date Started iomoo Date Ended 10/11100 Water Level, 24 Hr. 7.9 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 7.9 z Comments Plowed field. cool sunny weather Total Depth 70.o Date of Observation 10M6100 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction SAND: Very dense (partly cemented), black -green 1 I I I I I E I I I I - speckled, clayey, silty, fine glauconite nodules -3-4.00 I 1 I I I I I I I I 53.5 50/ t I i 36.00 i I i - SM -38.00 I I ! I I I - I I I I I I I I I I I I I I I I I r I 1 57.4 - - ' SAND: Medium dense, green -black speckled, 40.00 i i i i i silty, clayey, fine grained, wet 58.5 6 I I I I I I I I F 7 I I I i 8C 7 42.00 I I I I I I I I Boring .• collapsed below50 I r I 61.5 , ' . feet CLAY: Medium stiff to very hard, gray -green, fine -44.00 i i i I I I I I I I r i ! I I I I I I I sandy, silty, moderately plastic 63.5 5 I I I I I I r s I I I I I -46.00 6 I I I ° I I I CL 5 I I I I I I i l I I I I I i I -48 00 I I I I I I I I I I I I I 7 r r ! F I I I I I I i I I i I I -_^•� I I I I I I I I I I I l k t ! I I I 1 I I I I I I 68.5 40 38 ; CL -s7 nn 501.5 I I t r I I Boring Terminated at 70 feet DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett, P. G., P.E. Boring No. MW-2s Engineering and Geology Depths in feet, referenced 6.g.s. Page 1 of i Client and Project C&D Landfill, Inc. (Pitt county) Ground Elevation 1 s.45 Equipment CME 75 Drilling Method 4114" ID HSA Water Level, TOB NA Date Started 05/03/01 Date Ended 05/03/01 Water Level, 24 Hr. NA Drilling Finn Bore & core Logged by David Garrett Stabilized Level 7.91 Comments Locking cover with 2.99' stickup Total Depth 13.o Date of Observation 5116101 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction 18.00 i i i i i - • - SILTY SAND. Loose, tan -brown, moist Concrete I I i I I I I I I I Prdut l I I I I ! I I I I t — SM Bentonite 16.00 I I I ' I I ' ! I I 1 I I .. - Sea[ 14.00 l 3 I I I I 1 I I I I I 1 I I I I I I 1 - 12.00 I I I I I I I I I I I I ' 1 t I - I I I I I I I I I I 7.0 - SAND: Loose, tan, fine to medium, wet I I 1 I I I I 1 i I . ' 0.019, 10.00 I I Slotted 1 I I I I I I ! 1 I I I SVV Screen 6 W00 V 1 t I I I t I I I ! I I I I I I I I I I I I I I I I I I I [ • 6'00 I I I I i i Boring Terminated at 131eet DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett, P. G., P.E. Boring No. M 3d Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of 2 Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 19.37 Equipment CME 750 Drilling Method 4-1v4" Hollow AugaiNater Level, TOB 3.0 Q Date Started 10112l00 Date Ended 10/13/00 Water Level, 24 Hr. 4.5 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 4.5 Comments Plowed field. cool sunnv weather Total Depth 50.0 Date of Observation 10/16/00 Elev, SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction I I r I CLAY: Stiff, bright yellow -orange, fine sandy, silty, 1 I I I S I moist I I I S I 18.00 I 1 I I I I I I I 1 I I I I I I I I I I I i ! i I I I I i I I I I I I I Caved 16.00 3.5 4 + I i i i 4.0 SAND: Medium dense, tan -yellow, silty, trace of 4 I i I i I i I i I CL M 6 I I I I I f day, moist 14.00 I I I I I I I I f i I I I I I I I I 1 i 7.0 ' 12 00 I I SAND: Medium dense, tan -buff, well graded fine I to coarse, wet I I I I 4 S I I I 6.5 4 I I I I I I 10.00 5 * I i I i I i I i SW I I i 3 I I I I I I I I I I 1 1 I I I I 8.00 1 I ! ! I I I I I I I I I I I I I I I I 6.00 I I I 1 I 1 I I I I I I I I I 13.5 2 ' ' 14.0 - I I I I SILT: Stiff, gray -green, fine sandy and clayey, with 4 I M L- 4 I i i I i i — - rr heavy shell hash (tuitellas) wet, medium plastic CL 4.00 I I I I I I I I I I I I I I I I 1 1 1 1 — - - 2,00 I I I I I I I I I I I I I I I I I 1 I I I i 16.5 2 I I I I I 1 I I I I - 0•DD 2 CL 4 I I I I I I 1 I I I I I I I I — - - - -2.00 I I I I I I I I I I I I I 1 I I 1 1 I 1 I I I I r I I I I I I I I I - - - - - -4.00 I i I i 1 i I i I i 23.5 — CLAY: Medium stiff, gray -green, plastic gumbo 23.5 2 5 Gay, moist CL 7 I I I I 1 1 I I I I I DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett, P.G., P.E. Boring No. MW-3d Engineering and Geology Depths in feet, referenced b.g.s. Page 2 of 2 Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 19.37 r `1 Equipment CME 750 Drilling Method 4-114" Hollow AugekWater Level, TOB 3.0 a Date Started 10/12/00 Date Ended 10/13/00 Water Level, 24 Hr. 4.5 Drilling Firm Bore & Core Logged by David Garrett Stabilized Level 4.5 Y Comments Plowed field, cool sunny weather Total Depth 50.0 Date of Observation 10/16/00 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez, Construction _g 00 ' CLAY: Medium stiff, gray -green, plastic gumbo Bentonite- : day, moist Cement I I I I I r i I I I I I Grout -8.00 I I I I I I ! I I I I 27.5 - - SILTYSAND: Medium dense to dense, partly .. cemented, black -green speckled, variably clayey, 28.5 3 - silty, moist, very hard drilling (cemented) below 38 6 * i i i i feet, glauconitic SM -10.00 5 ! 3 1 I I I I I I I I I -- 12.00 F I I I I I 1 I I 1 I I I I I I I I I I I I I I I 77 - - -14.00 I I I I I I I I I I I I I I I I I I I I I I 33.5 5 I I I I I 18 I I I I I I SM 20 I I I ' - - _18.00 I I I I I _ Bentonite I I I I I I I I I I I I I I I I I I I I - Seal -18.00 I I I I I I I I I I I I 1 I 1 I I I I I I I I I I 38.5 15 I I I I I I I 1 1 1 I I 1 I I I - -20.00 501.3 i I I i I I i 1 1 i l r i I I _ - - SM I I I 1 s f I I - .. -22.00 I I I s I I I 1 I l I I - - Sand Pack -24.00 I I 1 I I 1 1 3 F I SM 43.5 501.5 I 1 I I 1 I f 1 I I -28.00 I 1 1 I I I I I 1 ! ! I I I 0.010" I I I I I Slotted 1 1 1 I r I 1 ! 1 1 I I - -- - Screen V W 1 1 I I I I I I I I 3 f I I I I - - 48,gyp .5 2943 1 I 1 I r I I I I 1 1 1 I I I -30.00 1 ! SM 501.5 Boring Terminated at 50 feet DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett, P.G., P.E. Boring No. MW-3s Engineering and Geology Depths in feet, referenced b.g.s- Page 1 of 1 Client and Project CAD Landfill, Inc. (Pitt County) Ground Elevation 19.37 Equipment CME 750 Drilling Method 4-11,V Hollow AugeliNater Level, TOB 3.9 s Date Started 815107 Date Ended 815107 Water Level, 24 Hr. NA Drilling Firm Bore A Core Logged by Aaron Hill Stabilized Level NA Comments Renlaces former MW-9s Total Depth 20.o Date of Observation NA Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction I t ' SILTY CLAY: St'df, bright yellow -orange, fine 1 I I I 1.2 sandy, silty. moist 18.00 1.0 12 + Bentonite- — 16 i i i i — SILTY SAND: Med. dense, brown w! orange ML_ Cement I .. mottle, fine -medium texture CL Grout 21 I I I I I - I I I I I I 33 — Bentonite 16.00 3.5 14 ' i ' i ' i i ' i SAND: Tan, silty, fine texture, moist Seal 11 i i i i i SM- 11 I I I I 1 ML 14.00 I I I I I - 6.0 7 I I i I i I i I i • Sand Pack 11 i i i i 7.1 SM 12.00 11 ; SAND: Medium dense, tan -gray, well graded fine ' to medium texture, wet '• 0.010" 8.5 4 Slotted 4 SW Screen 10.00 4 I I i ! I i I I i I I i I t sM 8 00 I I I 1 1 I I I I I I I I I 7 ! I - I I I I I I I I I I I I r t S 12.9 - I I i I i I i t i CLAYEY SILT: Stiff, gray -green, fine sandy and 6.00 13.5 2 1 _ _ clayey, with heavy shell hash (turritellas) wet, 3 medium plasticity SM 3 I I I S I I 4.00 I I I I I I I I I I \ W I I E I I I I I i I I I I I I I I i t I 2.00 I I I I I \- I I 5 I I 18.5 4 I I ! I I — 5 I \ CL_ 0.� 5 I I F I I I _ Boring Terminated at 20 feet MIL r-111 DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/10/09 Date Ended 08/10/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 21.93 Total Depth 20.0 Boring No. MW-3A Page 1 of 1 Ground Elevation 19.13 Water Level, TOB 5.9 Water Level, 24 Hr. NA Stabilized Level 11.4 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -18 -16 -14 -12 Eli] -8 -6 -4 -2 -0 N = 0 20 40 60 80 100 BPF CLAYEY SAND: Topsoil with roots Bentonite- 1.0 3 1.6 Cement Grout 5 SM 0 - 3' SILTY SAND: Loose orange sli. clayey, fine - medium, trace of roots, sli. moist 3.5 4 - Bentonite Seal 4 -_ sM 3-4' 5 SZ 6.0 7 SM 7 8.5 SAND: Medium dense, tan -buff, 8.5 5 s well graded fine to coarse, SW moist -wet Sand Pack 4-20' 12.9 :. . — �- SILTY CLAY: Stiff, gray -green, 13.5 3 fine sandy, with heavy shell \- hash (turritellas) wet, medium ML- 4 plasticity CL 0.010" Slotted Screen 5 - 20' �- 18.5 2 \- M L- 2 — �— Boring Terminated at 20.0 feet CL 3 DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett, P. G., P.E. Boring No. MW-4 Engineering and Geology Depths in feet, referenced b.g.s. Page i of i Client and Project C&D Landfill, Inc. (Pitt County) Ground Elevation 14.83 Equipment CME 75 Drilling Method 4-114~ ID HSA Water Level, TOB NA s Date Started 05/03/01 Date Ended 05/03/01 Water Level, 24 Hr. NA Drilling Firm sore & core Logged by David Garrett Stabilized Level 3.35 Comments leckinn cover with 3.59'stickuo Total Der)th 13.o Date of Observation wiwo1 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction _ .. - SILTY SAND: Loose, tan -brown, moist Concrete I I I I I .. Pad 14.00 ' ' ' ' ' — I I I I I I I Grout I I 1 I I I - — SM Bentonite I Seal 12.00 I I .. I I I I I I I I 1 I I l I I I — 10.00 I I I I I I I I I 1 1 1 I I I l I I I I — I I I I I I I I 1 I I 6.0 — SAND: Loose, tan, fine to medium, wet i i $.00 I 1 I I I I I ! f I I - - 1 t I 1 t I I 1 I I I 0.010" Slotted 6.00 W Screen I I I i i I I I I I I I I I I • SW 4.00 I I I I I I I I I I I I ! I I - 2.00 I I I I I I Boring Terminated at 13 feet DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett, P. G., P.E. Boring No. MW-5 Engineering and Geology Depths in feet, referenced b.g.s_ Page 1 of 1 Client and Project C&D Landfill, Inc. (Phase 1) Ground Elevation 14,.80 Equipment Mobile 6-53 ATUrilling Method 4-1147 Hollow AugeidVater Level, TOB 3.6 Date Started 11M9102 Date Ended 11/19/02 Water Level, 24 Hr. NA Drilling Firm Bore & core Logged by David Garrett Stabilized Level 3.9 Comments wooded area, cool sunny weatherTotal Depth 20.o Date of Observation 11/27/02 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction SAND: Loose, tan, silty, fine to medium, dry ` Bentonite- I Cement 14.00 i ; i i Grout 1.0 4 4 i i i i SM 6 S I I I I I I Bentonite 2.9 Seal 12.00 i i i i i SAND: Medium dense, tan -buff, medium to 3.5 9 I I I 1 coarse, wet (fluvial) 3V ' I � 14 i i i i SW 10.00 16 I I I I I I I I I I S I 5.6 ' SAND: Loose to medium dense, tan -buff, fine to 6.1) 9 coarse, wet, trace of silt (fluvial) $.00 9 i i i i sM 4 I k I I I I I 3 t I I I I I I 8.1 Sand Pack I CLAYEY SAND: Loose, green -gray, silty, wet, 6.00 8.5 4 3 I . � sampled as distinct sand layers with plastic clay lenses (channel or near -shore deposits) SC 4 I \- I I ! I I \ \- I �- 4'00\- 0.01 a, \- ••• Slotted l I I I I Screen 2•00 3 I I I I 1 13.5 3 I i i i ....... .\- 4 i i i i \-\- SC 0.00 4\-\- i-- * Locking steel cover w! 3 foot \- •\ stickup �, -2.00 I I I I I I I I 1 I \- I I 1 I I I I I I I 18.4 Deep SILTY CLAY: Stiff, gray -green, var. sandy, shell 4.00 18.5 3 i i i i i marine 4 1 i i i i hash, moist, plastic ** CL_ deposits (Yorktown 6 i i i Boring Termat 20 feet CHinated Grp.) DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett, P. G., P.E. Boring No. MW-6 Engineering and Geology Depths in feet, referenced b.g-s. Page 1 of 1 Client and Project C&D Landfill, Inc. (Pitt county) Ground Elevation 16"87 Equipment CME 75 Drilling Method 411,C ID HSA Water Level, TOB NA Date Started 05/03/01 Date Ended 05/03/01 Water Level, 24 Hr. NA Drilling Firm Bore & core Logged by David Garrett Stabilized Level 6.68 Comments Lockina cover with 3.16" stickup Total Depth 13.o Date of Observation 5116/01 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction I SILTY SAND: Loose, tan, moist Concrete pad 16.00 I — I I ! I I I - - Grout I I f I I SM Bentonite — Seal 14.00 I l f I I I I I I I 1 I I I I - 12.00 3 1 I I I I ! I I I . . — I I 1 ! I I I I I 1 6.0 - SAND: Loose, tan, fine to medium, wet I I I I I i 0.00 I I I I I 1 I I ! I • I I I I I 1 I I I I • 0.010" ' Slotted 8.00 i i i r i Screen I 1 1 I I I I I I I F I 1 I I I - SVj b 00 I I I I I I I - 1 I l I I I I I I I - 1 1 I I I I - Boring Terminated at 13 feet 4.00 - DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett, P.G., P.E. Boring No. AM-7 Engineering and Geology Depths in feet, referenced b.g.s. Page 1 of i Client and Project C&D Landfill, Inc. (Pitt county) Ground Elevation 16.03 Equipment CME 75 Drilling Method 4-1►47 ID HSA Water Level, TOB NA s Date Started 05/03/01 Date Ended 05/03/01 Water Level, 24 Hr. NA Drilling Firm sore & core Logged by David Garrett Stabilized Level 5.29 ('nmmAntS Lne-kinn cover with 3.37' stickup Total Depth 13.o Date of Observation 5/16/01 Elev. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction SILTY SAND: Loose, tan, moist Concrete I I I I I •• P I I I I I — Grout 14.00 1 ; r ; I ; I ; I ;77 SM Bentonfte I I I E I I I I I i Seal 12.00 I I I I I I I I I I I I I I I I S 5 1 i - I I I I ! I I I I 5.0 - - I SAND: Loose, tan, fine to medium, wot 10.00 I I S ! t I I I I I I 1 I I I I I 1 I I I I I I I I I 1 I I I I I I I 0.010" I I I I 1 Slotted Screen I SW 6.00 I 1 I I 1 I I 4D0 I 1 I I I I 1 i I I Boring Terminated at 13 feet DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett, P. G., P.E. Boring .No. AM-8 Engineering and Geology Depths in feet, referenced b-g.s. Page 1 of 1 Client and Project CSD Landfill, Inc. (Phase 1) Ground Elevation 18.30 Equipment Mobile 13-53 ATDrilling Method 4-114" Hollow AugeliJVater Level, TOB 7.3 s Date Started 11/18/02 Date Ended 11/18/02 Water Level, 24 Hr. 7.3 Drilling Firm Bore S Core Logged by David Garrett Stabilized Level 7.3 COMMentS wooded area- cool sunny weatherTotal ❑eoth 20.o Date of Observation 11/27/02 Elegy. SPT Data and Strata Depths Lithology Description and USCS Code Piez. Construction 18.00 SAND: Loose, tan, slightly silty, fine to medium, ` Bentonite- ' dry Cement Grout - 2 i i r i SW 16.00 3 I , I I , f I I , I I , I I , I - Bentonite Seal 3.5 3 I s I I I I 14.00 3 i i i i t - SW 4 I I I I I I I I I I I I I 1 f - 6.3 12.00 6.0 4 4 SAND: Medium dense, tan -buff, medium to SW 4 I I I I f I I I :. coarse, wet 10.00 i i i i i 8 4 Sand Pack SAND: Loose to medium dense, tan -buff, fine to 8.5 7 8 I I i I i I i I , ' ' coarse, wet, trace of slit Sw 8.00 I 1 I I I - I I I I I Slotted I I I I 1 Screen 6.00 W I I I I I I I I I I I I 1 1 1 • 13.5 4 I I I 1 I I I - 4.00 4 SW 4 I I 1 I I I Locking I , , , , • steel cover _ wl 3 foot 2.00 I I I : = I stickup I i I I i I 1 i I I s i I i I 17.6 ." SILTY CLAY: Mod. stiff, gray -green, var. sandy, 0.00 i i i heavy shell hash (turritellas) moist, plastic '• CL- " Deep 18.5 3 l• I I I I CH marine deposits 4 I I 1 I I 1 I (Yorktown 6 Boring Terminated at 20 feet Fm.) DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/07/09 Date Ended 08/07/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 20.58 Total Depth 20.0 Boring No. MW-9A Page 1 of 1 Ground Elevation 17.64 Water Level, TOB 3.1 Water Level, 24 Hr. NA Stabilized Level 4.8 Observation Date o8M o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -16 -14 -12 -10 -8 -6 -4 -2 -0 -2 N = 0 20 40 60 80 100 BPF 77 SILTY SAND: FILL with brick 1.0 3 77 and concrete fragments Bentonite- Cement Grout 4 2.1 SM 0-3' 5 XX CLAY: Med. stiff, orange -tan - gray (mottled), fine sandy, very 3.5 10 moist Bentonite Seal 12 CIL 3 - 4' 13 Ir 5.9 SAND: Medium dense, light 6.0 5 ♦ 5 gray -buff, sli. silty, well graded SW- 6 fine to medium, wet SM 85 4 5 SW- 5 SM Sand Pack 4-20' 13.5 4 13.7 _ 4 — SILTY CLAY: Med. stiff, gray- ML- 5 green, sli. fine sandy, with CL �- heavy shell hash (turritellas) 0.010" Slotted — wet, medium plasticity Screen 5 - 20' �- Artesian water press. at 12 feet 18.5 2 \- M L- 2 — Boring Terminated at 20.0 feet CL 3 DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/06/09 Date Ended 08/06/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 16.61 Total Depth 20.0 Boring No. MW-10 Page 1 of 1 Ground Elevation 14.16 Water Level, TOB 2.7 Water Level, 24 Hr. NA Stabilized Level 4.8 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -14 -12 -10 -8 -6 -4 W -0 -2 -4 N = 0 20 40 60 80 100 BPF SILT: Soft, dark brown, fine 1 sandy, organic, very moist Bentonite- 1.0 Cement Grout 1 2.1 ML 0-3' 5 SAND: Med. dense, tan -buff, uniform fine grained, wet t t 3.5 9 Bentonite Seal 13 SP 3-4' 12 Ir 6.0 9 12 7.1 SW 2 8.0 SAND: Loose, tan -buff, sli. silty —_ SILTY CLAY: Soft, gray -green, 8.5 3 sli. fine sandy, with heavy shell 2ML- \ hash (turritellas) wet, distict CL sand and clay layers Sand Pack 4-20' 13.5 3 �- 2 — M L- 3 CL \- 0.010" Slotted Screen 5 - 20' �- 18.5 3 \- M L- 3 — Boring Terminated at 20.0 feet CL 3 DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/06/09 Date Ended 08/06/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 14.49 Total Depth 20.0 Boring No. MW-11 Page 1 of 1 Ground Elevation 11.60 Water Level, TOB 6.1 Water Level, 24 Hr. NA Stabilized Level 3.1 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data M -8 -6 -4 -2 -0 -2 -4 -6 -8 N = 0 20 40 60 80 100 BPF SAND: Loose, dark brown, silty, 2 fine - medium, tr. clay, moist Bentonite- 1.0 Cement Grout 2 SM >0-3' 3 2.9 CLAY: Very soft, green -gray, 3.5 1 silty, fine sandy, w/ turritella Bentonite Seal shell hash, wet ��- 3 - 4' 0 5.5 CLAY: Soft - med. stiff, gray- 6.0 2 Sz 3 green, fine sandy, very silty, ML- 2 with shell hash (turritellas) wet, CL very sandy layer w/ large shell fragments at 9.5 - 10 feet 8.5 4 5 SC- 6 CL Sand Pack 4-20' 13.5 5 5 14.5 MH- $ SILTY CLAY: Med. stiff, gray- CH — green, sli. fine sandy, wet, very 0.010" Slotted plastic Screen 5 - 20' 18.5 5 \- M H- Boring Terminated at 20.0 feet CH DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/07/09 Date Ended 08/07/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 16.18 Total Depth 20.0 Boring No. MW-12S Page 1 of 1 Ground Elevation 13.72 Water Level, TOB 2.1 Water Level, 24 Hr. NA Stabilized Level 5.3 Observation Date o8M o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -12 -10 -8 -6 -4 -2 -0 -2 -4 z. N = 0 20 40 60 80 100 BPF SAND: FILL, Loose, brown, 1.0 1 silty, moist (drilling pad) Bentonite- Cement Grout 2 2 0 SM sz 0 - 3' SAND: Loose, tan -gray. sli. 5 silty, fine -medium, black 3.5 10 decayed organic debris, wet Bentonite Seal 12 SW- 3-4' 13 SM 7W 6.0 5 9 SW 10 SM 8.5 5 Loose, white, clean "sugar sand" 7 9.5 SP 3 10.0 �- SILTY CLAY: Med. stiff, gray- Sand Pack green, sli. fine sandy, moist, w/ 4 - 20' _— shells, very plastic 13.5 3 5 CH \- 0.010" Slotted Screen 5 - 20' �- 18.5 5 \- M H- Boring Terminated at 20.0 feet CH DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment CME 450 Drilling Method 4-1/4" HSA Date Started 08/07/09 Date Ended 08/07/09 Drilling Firm Bore & Core, Inc. Logged by Aaron Hill Comments TOC Elev. 20.69 Total Depth 20.0 Boring No. MW-13 Page 1 of 1 Ground Elevation 18.12 Water Level, TOB 5.1 Water Level, 24 Hr. NA Stabilized Level 8.8 Observation Date o8M o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -18 -16 -14 -12 -10 -8 -6 -4 -2 -0 N = 0 20 40 60 80 100 BPF SILTY SAND: Loose, brown, 1.0 2 fine -medium, w/ clay, roots, dry Bentonite- 3 (perimeter embankment fill) gW_ Cement Grout0 - 3' 3 - SM 3.5 3 4.0 Bentonite Seal CLAYEY SAND: Loose, tan, SC 3 - 4' 5 fine -medium, w/ wood, moist 5.7 - SILTY SAND: Very loose, tan- 6.0 1 1 brown, w/ tr. clay, wood SM 1 _ 8.1 �_ SILTY CLAY: Stiff, green -gray, 8.5 7 9 _— sli. fine sand w/wood Y, ML- 10 C L \_ Sand Pack — 4-20' 12.5 �- �- SILTY CLAY: Stiff, gray -green, 13.5 5 sli. fine sandy, w/ heavy shell 6 — hash (turritellas), moist, very MH- 6 plastic CH \- 0.010" Slotted Screen 5 - 20' �- 18.5 4 \- M H- 5 Boring Terminated at 20.0 feet CH DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment Detrich D-10 Drilling Method 4-1/4" HSA Date Started 12/17/02 Date Ended 12/17/02 Drilling Firm Bore & Core, Inc. Logged by David Garrett Comments TOC Elev. 17.45 Total Depth 40.0 Boring No. MW-14D Page 1 of 2 Ground Elevation 14.54 Water Level, TOB 2.9 Water Level, 24 Hr. 3.0 Stabilized Level 4.0 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -14 -12 -10 -8 -6 -4 -2 -0 W -4 -6 -8 -10 N = 0 20 40 60 80 100 BPF . SILTY SAND: Medium dense 1.0 ♦ tan -brown, fine to medium Convertedfrom 5 SM piezometer 5 B-23d 3.1 3.5 6 SAND: Medium dense, tan, 10 medium to coarse SP 9 6.0 7 10 SW 7 7.9 X. CLAYEY SAND: Medium 8.5 4 • dense, dark gray 3 _I SC 5 12.7 Bentonite- Cement Grout �- SILTY CLAY: Stiff, dark gray, 13.5 4 l \- fine sand layers, shell layers, 0-32' 5 — becomes sandy with shell hash ML- 6 below 28.4 feet CL 18.5 4 * �_ 6 CH 23.5 5 CH 6 DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment Detrich D-10 Drilling Method 4-1/4" HSA Date Started 12/17/02 Date Ended 12/17/02 Drilling Firm Bore & Core, Inc. Logged by David Garrett Comments TOC Elev. 17.45 Total Depth 40.0 Boring No. MW-14D Page 2 of 2 Ground Elevation 14.54 Water Level, TOB 2.9 Water Level, 24 Hr. 3.0 Stabilized Level 4.0 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -12 -14 -16 -18 - 20 - 22 - 24 N = 0 20 40 60 80 100 BPF \- SILTY CLAY: Stiff, dark gray, fine sand layers, shell layers, becomes sandy with shell hash below 28.4 feet 28.5 21 : \- 16 CL Bentonite Seal 32-33' 32.8 �- SAND: Very dense, dark gray, 33.5 50/A silty, glauconitic, shell hash SM Sand Pack 33-40' 0.0101, Slotted Screen 35-40' 29 38.5 50/.5 Boring Terminated at 40.0 feet SM DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA David Garrett and Associates Engineering and Geology Depths in feet, referenced b.g.s. Client and Project C&D Landfill, Inc. (Pitt County) Equipment Detrich D-10 Drilling Method 4-1/4" HSA Date Started 12/18/02 Date Ended 12/18/02 Drilling Firm Bore & Core, Inc. Logged by David Garrett Comments TOC Elev. 16.60 Total Depth 20.0 Boring No. MW-14S Page 1 of 1 Ground Elevation 13.90 Water Level, TOB 3.0 Water Level, 24 Hr. 2.2 Stabilized Level 2.0 Observation Date o8/1 o/o9 Elev. SPT Depth, Value and Plot Strata Depth and Description (USCS) Piezometer Constuction Data -12 -10 -8 -6 -4 -2 -0 -2 -4 -6 N = 0 20 40 60 80 100 BPF SILTY SAND: Medium dense Convertedfrom 1.0 tan -brown, fine to medium piezometer B-23s 5 SM 5 Bentonite- 3.1 _ sz Cement Grout SAND: Medium dense, tan, 3.5 6 0-1' 10 medium to coarse SP Bentonite Seal 9 1-3' 6.0 7 10 SW 7 7.9 X. CLAYEY SAND: Medium 8.5 4 dense, dark gray 3 Sc 5 12.7 Sand Pack 3-20' -- SILTY CLAY: Stiff, dark gray, 13.5 4 l \— fine sand layers, shell layers, 5 — becomes sandy with shell hash ML- 6 below 28.4 feet CL \- 0.010" Slotted Screen 5-20' 18.5 4 \— s ? Boring Terminated at 20.0 feet CH DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA David Garrett, P.G., P.E. MW-15s (OLD B-23s) Engineering and Geology Page 1 of 1 Client and Project CAD Landfill, Inc. (Phase 2) Ground Elevation 13.90 Equipment Detrich 0-10 Drilling Method 3-114" HSA Water Level, TOB 3.0 Date Started 12/18/02 Date Ended 12 I8102 Water Level, 24 Hr. 2.2 Drilling Firm Bare & care, inc. Logged by David Garrett Stabilized Level 1.4 Comments Lagged area, cool sunny weather Total Depth 20.0 Date of Observation 1116103 All deaths are given in feet and referenced b.a.s. Depth and Elev. SPT Value and Plot Soil Description, OVA and USCS Symbol Piezometer Constuction Data -0 - 2 12.00 - 4 10.00 - g 8.00 - 8 6.00 - 10 4.00 - 12 2.00 - 14 0.00 - 16 -2.00 - 18 -4.00 — 20 -6.00 i I l i i i i + � I i i I i i i i i BLANK: No samples taken - please see log fpr &23d Sz Bentonite- Cement Grout Bentonite Seal ' i I I i i Sand Pack 3 ' 0.0101, (} t E F e ! i i Slotted Screen DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA David Garrett, P.G., P.E. MW-17 (OLD B-20) M I I I Engineering and Geology Page I of 1 Client and Project C&D Landfill, Inc. (Phase 2) Ground Elevation 18.18 Equipment Detrich D•10 Drilling Method 3-1/4" NSA Water Level, TOB 3.7" Date Started 12/09/02 Date Ended 12109/02 Water Level, 24 Hr. 3.9 Drilling Firm sore & Core, Inc. Logged by David Garrett Stabilized Level 4.1 Comments Logged area, cool Manny weather Total Depth 20.0 Date of Observation 1115103 All depths are given in feet and referenced b.g.s. Depth and Elev.1. SPT Value and Plot Soil Description, OVA and USCS Symbol Piezometer Constuction Data - a 1 B_oa — 16.00 — 14.00 — 6 12.00 — 8 10.00 — 10 8.00 — 12 6.00 — 14 4.00 — 16 2.00 = 18 0.00 - 20 .. SILTY SAND: Medium Sentonite- ; i dense, dark brown, fine Cement Grout 3 grained SM 5 1 — Bentonite Seal � SAND: Medium dense to dense, tan -brown, SW 19 I i fine to medium 8 14 0i ! i i ! SW 21 ! I 9 12 SW 14 I f � I i Sand Pack 3 SW SAND: Medium dense, [ fine to medium, trace of i { silt E f f� �{ 0.01 01, I I i Slotted Screen 3 a E f ! ! SILTY CLAY: Medium 5 I stiff, trace of shells ML-CL DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA D SOIL CLASSIFICATION P .AND REMARKS T H SEE KEY SYMBOL SHEET FOR EXPLANATION OF (ft) SYMBOLS AND ABBREVIATIONS BELOW. 0 Sandy topsoilirootmat Landfill debris/gravel and sand ------------------------ COASTAL PLAIN: Orange -tan to gray, dry to moist, clayey and silty SAND (SM) C-OAST-AT P-1-Tan--a-a-nd -wh-t-m-ist-to-sa-tur-ate-d- L E SAMPLES PL (%) NM.(%) LL (%) E L I (Rec") G E D T N-COUNT ♦ FINES (%) E V E Y or N N P Rcc%MQD% SPT (bpf) D (ft) T E 6"- 6"- 6"- 6" 10 20 30 40 50 60 70 80 90 100 15.0 5 slightly silty, tine to coarse SAND (SP) with trace rounded 10.0 fine gravel 1 . 10 5.0 15 YORKTOWN FORMATION: Dark gray to gray -green,- 0.0 saturated, silty, fine to medium SAND (SM) with thin (0,1-0.2) lenses and layers of dark gray -green, fat CLAY (CH) 20 Boring terminated at 20.0 feet. -5.0 G n :7 a 3 25 0.0 d .a a a a n 30 15.0 35 -1 1 �- -20.0 40 -1 1 F- -25.0 45 -30.0 CONTRACTOR: Regional Probing Services -Larry Opper LOGGED BY: M. Lear EQUIPMENT: Geoprobe 5410 DRILL METHOD: Direct Push HOLE DIAMETER: 4" WELL: Stickup 2.9' Size 2" CLOSURE METHOD: Installed Monitering Well MW-16. REMARKS: Well developed by purging approximately 3 well volumes via bailer and pump. Static water level measured at 7,45 ft below TOC. 0 10 20 30 40 50 60 70 80 90 100 GEOTECHNICAL BORING RECORD BORING NO.: MW-16 PROJECT: EJE Recycling LOCATION: Greenville, NC DRILLED: June 16, 2017 PROJECT NO.: 6468-17-7070 PAGE 1 OF 1 IEWED BY: amec faster wheeler ► DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA David Garrett, P.G., P.E. Engineering and Geology .,Client and Project C&D Landfill, Inc. (phases 3 and 4) Equipment CIVIE 450 Drilling Method 4 1vvv H$A Date Started 12114101 Date Ended 12/14/01 Drilling Firm Bore & Core, Inc. Logged by David Garrett Comments :.iamg2u aiea5 cioal rarliny weather Total Depth 15.0 All dent :- are ,;:al: ,l__� _s_..__i.td r � � �kl iT.CI pelf l�if�rl'�.��YV`ii N.w.sx OLD B-Is (BG) Page 1 of 1 Ground Elevation 17.19 Water Level, TOE 1.5 Water Level, 24 Hr. 1.4 Stabilized Level 1.6 Date of Observation 12/27/01 Depth and Elegy. SPT Value and Plot Soil Description, OVA and USCS Symbol Piezom2ter Constuction Data 0 r 16.00 2 14.00 4 12.00 6 10.00 8 8.00 10 6.00 12 4.00 14 SAND: Loose, gray- 2 I I I - brown, variably silty, 3 4 moist, trace of clay and a i ! . organics SM I Bentonite- s 6 ' SP- Cement Grout 7 i I SM 2 SILT: Soft, dark bra.,.n, 2 clayey, decayed 2 — organics (channel Bentonite Seal -= deposits) 2 I — 1 I i ML 2 — Sand Pack 0.0101, 2 i I i i - - — ML Slotted Screen DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA Appendix Laboratory Analytical Report December 2021 Groundwater Monitoring Report CEO Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 R 7407- CDLF- 2009 DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA This page intentionally left blank. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA i ET'HNNMW I U kcUPT MAW 114 OAKMONT DRIVE GREENVIL-LE, N.C. 27858 C & D DISPOSAL, INC. MR, JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 Drinking water YD: 37715 wamtowater IL, 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 6003 DATE COLLUCTED: 12/09/21 DATE REPORTED : 07/19/22 RLV'IEWED $Y I HW-4 NW-5 MW-6 NW-7 MW-8 Analysis Method PARAMETERS MDL MRG Date Analyst Code PH (field measurement). Unite 6.5 HISSING 6.9 6.9 7.1 12/09/21 PJC 45DOND-11 Nitrate+Nitrite as N, mg/1 0.04 0.04 --- U MrSSINO 0.16 0.19 0.27 12JI3121 EMD 353.2 R2-93 Alkalinity eta PH 4.5), mg CaCD3/1 1.0 1.0 134 Mr59ING 1410 1450 1640 12/13/21 DNS 2320E-11 Chloride, mg/l 1.0 1.0 11 MISSING 116 101 169 12/13/21 DIJ 4500CLE-11 Cyanide, ug/1 5.0 5.0 --- V mraOINQ --- U --- U --- u 12/13/21 14MM 4500CMS-11 Total nineplved Residue, m9/1 10 10 26C MISSING 1600 2000 12/24/21 JHS D5907-13 Total Dissolved Residue, mg/l 10 10 1500 12/16/Zl JMO D5907-11 Sulfate, mg/1 9.0 5.0 4$ A MISSING 76.7 39.E 129 12/23/21 Las 4500SO42E11 Antimony, ug/1 0.03 1.0 --- 1) MISSING 0.14 J 0.04 J 0.20a 22/21/21 NAB EPA200.0 Arsenio, ug/1 0.D8 5.0 0.62 J MIaaING 17 20 26 12/17/21 NAB BBA200.6 Barium, ug/l 0.04 10.0 70.4 MISSING 713 511 620 12/21/21 NA13 EPA200.6 beryllium, ug/l 0.02 1.0 0.09 J MISSING 0,04 J 0.05 J 0.94 J 12117/21 NAB 13PA200.8 Cadmium, ug/l 0.04 1.0 --- U MISSING --- U ,-- V --- u 12/17/21 NAB EPA200.6 Cobalt, ug/1 0.02 1.0 0.15 J MISSING 3.3 14 2.7 12/17/21 NAB BPA300-$ Total chromium, U7/1 0.12 5.0 1151 MISSING 13 12 25 12/17/21 NAIL EPA200.6 Copper, u9/1 0.04 10.0 0.1E J MISSING 0,19 J 0.20 J 0.15 J 12117/21 NAB 13PA$00.8 Iron, ug/l 4.96 50.0 5000 MISSING 10418 52259 34503 12114/21 LFJ 11PA200.7 Manganese, ug/1 0.31 10.0 56 MISSING 765 727 765 12/24/21 LFJ 8PA200.7 Lead, Ug/l 0.03 5.0 0.151 MISSING 0.05 J 0.06 J 0.05 J 12/111/21 NAB EPA20OLO Mercury, ug/1 4.05 0.20 --- U MISSING --- U --- U --- U 12/22/21 HTM 245.1 R3-94 Nickel, ug/1 0.03 10.0 0.20 J MISSING 5.7 J 1.9 J 1.7 J 12/17/21 NAB EpA200.8 Melenium, ug/1 0.05 10.0 0.10 J HISSING 1.1 J 0.$6 J 0,94 J 12/17/21 NAB EPA200.0 Silver, v0l 0.22 5.0 --- U MISSING --- U --- U ... U 12/17/21 HAD HPA200.8 Thallium, ug/l 0.02 1.0 --- U MISSING --- U 0.10 J --- U 12/17/21 NAB EPA200.6 Tirl, ug/1 0.05 100.0 --- U MISSING --- U --- U 12/21/21 NAB EPA200.8 Tin, ug/l 0.05 100.0 --- U O1/05/22 NAB RFA200.$ Vanadium, ug/l 0.04 1.0 2 MISSING 10 2 4 12/17/21 NAB EPA200.8 Zino, Ug/1 0.17 10.0 1.4 J b9ISSINO 0 A0 1 1.4 a 1.3 J 12/17/21 HAD BPA200.0 sulfide, ug/1 100 1000 --- U HISSING --- U --- U --- U 12/09/21 LFJ 450092D-11 Conduetivlty (at 25o}, uMhos/am 1.0 1.0 376.3 MISSING 2641 2429 3574 12/09/21 PJC 25108-11 Dissolved Oxygen, m9,/1 0.1 0.1 D.44 Mr981NG 1.05 0.65 1.87 12/09/21 PJC 45000G-16 Temperature, °c 13 MISSING 1$ 15 13 12/05/21 P7C 2550E-10 Static Water Love 1, feet 7.60 HISSING 9.96 8.91 10.30 12/09/21 PJC well Depth, feet 15.96 MISSING 16.65 16,33 20.26 12/09/21 PJC ORP, my +177 MISSING +156 4263 +174 12/09/21 PJC 2590E-11 Turbidity 4Field), NTU 1.0 1.0 0.61 MISSING 7.57 6.99 8.93 12/09/21 1'JC 2130b-11 J r 8etimated value between the NDL and MRL, U - Below ALL Quantitation Limits. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA EQW'UTOCf IM(@.r' �, hr-,r',)00 TPOO W Drinking Water IDs 37715 Wa4berrit.8r 1Dt 10 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C_ 27858 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 MR. JIMSON WHITEHURST 802 RECYCLING LANE ANALYST: HYC GREENVILLE, NC 27634 DATE COLLECTED: 12/09/21 DATE EXTRACTED: 12/13/21 y DATE ANALYZED: 12/14/21 REVIEWED BY: _ DATE REPORTED: 07/19/22 PESTICIDES AND PCB' S EPA METHOD 8081E R2(07) NW-4 NW-5 mw-6 NW-7 Hw-8 nARAMBTERS, U9/1 MDL MRL 1, Aldrin 0.029 0.D50 V --- V --- U --- U --- U 2. Alpha-BHC 0.032 0.0S0 -.- U ... U --- U --- U '" U 3. beta-HH¢ 0.031 0.050 --- U --- V --- U t-- it --- U 4, Delta-BHC 0.03D 0.050 --- U --- U -.- U --- U --- U S. 0ttnM&-5P1C (Lindane? 0.032 0.050 --- U - U -_' U .._ U "_. U 6, Chlordane 01320 0.500 --- U --- U ••• U "" U --- U 7, 4,4-DDD 0.051 0.100 ... U --- U --- V --- U --- U B. 4r4-DDE D.04$ 0.100 --- V --- U ... U ___ U U y. 4,4-DDT 0.052 O.1D0 •.. U --- U --- U -"- U U 10, Pieldrin 0.042 0,075 --- U --- U -•- U U --- U 11. EndosuLtan 1 0.056 0.100 --- U --• U U --- U --- U 12, Endpaulfan 11 0.044 0.100 --- D --- U ••• U - U .-• U 13. Hndoevllttl BVIARte 0.072 0.IOU --- V --- U --- V --- V --- U 14. Nnarin 0.051 0.100 -- V --- U ... U --- U --- U 15. Endrin Aldehyde 0.068 0.100 --- V --- U --- U " ' U --- U 15. HeptaOhlor 0,039 0.050 --- U --- U -`- U --- V --- U 17. Heptachlbr Epoxide 0.042 0.075 - 17 --- U --- U --- U -_- U 10. Hethoxychtor 0.530 1.000 --- a --- U --- ❑ --- v --- u 19. P4b'a (ArOC10ZO) D.500 2.000 --- V --- U --- U --- U --- U 20. Toxaphene 0.690 1.500 --- U --- U -- U --- U ❑ a . setimattd value between the Mob and MRL, U - 8410W ALL QUantitation Limixa, DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA �Arofiwm % hmpo m. Nd Drinking Water ID: 37115 Waatawater IDi 10 114 OAKMONT DRIVE GREENVILLE, N,C. 2785H CLIENT- C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE OREENV'ILLE, NC 27834 REVIEWED BY: � f LANDFILL APPENDIX II EPA METHOD 8151A R1(96) PHONE (252) 756-6208 FAX (252) 755-0633 CLIENT ID: 6003 ANALYST: HIC DATE COLLECTED: 12 / 0 9 / 21 DATE EXTRACTED: 12/14/21 DATE ANALYZED: 12/18/21 DATE REPORTED: 07/19/22 taw-4 MW-5 MW-6 NW-7 NW-8 PARAMETERS, ug/l MDL MRL 1. 2,4-D 0.34 2.000 ••• U --- V --- U --- U --- U 2, Dinaeeb 0.54 1.000 --- V --- U --- U -__ U ___ U 3. 2,4,5-TP 0.41 2.000 ••• U -•• U --- U --- 0 U 4, 2,4,5-T 0.47 2.000 --- u --- v --- a --- U --- U J + Estimated value between the MDL and MRL, U • 8e10W ALL QUantitation Limita. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA ERTHhflffflM t D coo TPO t- od Drinking water TDB 37715 4)aff"w0er ;Px 10 114 OAKMONT DRIVE GREENVILLE. N.C. 27856 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC, CLIENT IA: 61303 MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST; HIC GREENVILLE, NC 27834 DATE COLLECTED: 12/09/21 Page: 1 DATE EXTRACTED: 12/10/21 DATE ANALYZED: 12/30/21 REVIEWED BY: DATE REPORTED: 07/19/22 SEMI -VOLATILE ORGANICS EPA METHOD 8270E RG(18) PARAMBURS, u8/1 MDL MkL MN-4 KW-5 MW-6 MW-7 NW-8 1. Acenaphthone 2,56 10.000 --- U U 12,94 --- U 3.09 1 2. Aeenaphthylene 2.60 10.000 - U --- U --- U --- V --- U 3. Anthratana 2.97 10.000 --- U --- 13 •-- U --- V --- U 4. Senro[a)antrhacene 4.16 10.000 U --- U --- U --- U 5. senzo[h]fluvrsntheAe 3,32 l0,Do0 --- U U --- U --- U --- U 6. SenzoCk3flucranthene 4.23 10.000 --- U --- U --- U --- U --- U 7. Benzo(y.h,ilpacylene 2.61 to. Ono --- U --- U --- V --- U --- U U. BenzaCa)pyrene 7,31 1D.000 --- U ... U --- U --- U --- U 9, 4-3romophenyl Phenyl $eher 3.63 10.000 --- U --- U --- U --- U --• U 10. Butyl Benzyl Phthalate 5.7a 10.000 --- U --- U --- U --- U --- ❑ 11, 8ia(2-Chlor0sth0xy) Methane 3.14 10.000 --- U --- U --- U --- D ... U 12, Bi■(2-Chloroethyl) Ether 2.5E 10.000 --- V --- U --- U --- U --- U 13. eie{2-Chloro-1-methylathyl) Ether 2.56 10.000 --- U --- U ... U --- V ... U 14. 2-Chl0ronaphthalene 2.17 10.000 --- U --- U --- U --- U --- U 15. 4-Chloropheny2 Phenyl Ether 2.42 10A00 --- U --- U --- U --- U U 16. Chrysene 4.04 10.000 --- U ••• U --- V --- U .-- V 17, Aibenzo[a,h]anthraCane 2.7E 10.000 --- V --- U ••• U --- U --- U la, Di-N-hutyl Phthalate 3.09 10.000 --- U ki --- U --- U - U 19. Dimethyl Phthalate 3178 10.ODO --- U ••• U --- ❑ --- U --- U 20, Diethyl Phthalate 3.92 10.D00 --- V --- U --- V '"' V " " U 21, 2,4-Dinitrotoluene 3.95 10.000 --- U --- U --- U --- U --- V 22. 2,6-Dinitret0lusne 3.B8 20.DOD --- U --- U --- U --- V --- V 23, Di-M-00tyl Phthalate 2.61 10,000 --- V --- V --- U ___ U ... U 2''4. Si0-(2-$thy1hexy1) phthalate 9.97 15.000 --- V --- U `-- U --- V --- U 25. Fluoranthene 3,92 10.000 --- U --- U --- U --- U --- U 26. FXUordna 2.95 lo.DOO --- V --- U --- U --• U ... U 27. Haxaahlaropcnxene 2.61 10.000 --- U --- U --- U --- U •.. U 2$, Mexachlarocyclopentadiene 4.15 10.000 --- U --- U --- U --- V --- U 29. 1nden0Cl,2,3-Cd)pyrene 2.91 10.000 --- U --- V --- V --- U --- V 30. 100phorone 3.74 10.004 --- U V --- U --- V --- U 31. Hitrobanzene 2,05 1D.000 --- U --- u --- U --- U -•- V 32, N-NiCroaodimethylamina 4.25 10.000 --- V --- V --- U --- U - V 33. N-Nitrasodiphenylamine 3195 l0.000 --- U - U --- U U .. U 34. N-Nitr0sodi-N-Prapylamine 4.06 1D.000 --- U --- U --- U --- U --- V 3g, Phenanthrena 3.24 10,000 --- U --- U --- U --- U ... U 35. Pyreria 1.63 10.000 --- U --- U --- U •-' U --- U 37, 4-Chloro-3-Msthylphenol 3.79 20.000 --- U --- U --- U --- U --- U 30. 2-Chlor0ph6R01 2.75 1D.000 --- U --- V --- U --- U --- U 39, 0-Cresol 3.68 10.000 --- U -- U --- U --- U "-_ U 40. P-Cr4aol 4.12 10.000 --- U --- U --- V --- U --- V 41. 2,4-Dichlorophan0l 5.19 10.000 --- U --- V --- U --- U --- U 42. 2,6-Di0hlorophencl 4.89 10.000 --- V --- U 11 --- U --- U 43. 2,4-Dimsthylphanal 3.21 10,000 --- U --- V --- U --- U --- U 44. 4,6-D1nitr*-2-Methylphano2 4.77 50.000 --- U --- U - - U --- V --- U 45. 2,4-Dinitrophenol 4.37 50,000 --- U --- U --- U ... U U 46. Sthyl M4thanesulfonate 5.26 20.000 --- U --- U --- U --- V " ' U 47, methyl Mathanesulfonate 4,32 1O.oDO --- U --- U --- U ••• U --- U 43. 2-Nitrophennl 3.64 10.000 --- U --- U --- U --- V --- U ,7 r xptimated value between the MDL and MRL, U - 8610W ALL Ouanritatian Limits. DocuSign Envelope ID: lE49C9C5-lEA4-40EE-BA46-8A724DF270DA kRW'uT(031MH(M 1, Drinking wator ID: 37716 114 OAKMONT DRIVE GREENVILLE, N.C_ 27858 CLIENT: C & D DISPOSAL, INC. MR, J=ON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 ANALYST: HIC DATE COLLECTED: 12/09/21 DATE EXTRACTED: 12/10/21 DATE ANALYZED; 12/30/21 REVIEWED BY: DATE REPORTED: 07/19/22 SEMI -VOLATILE ORGANICS EPA METHOD 8270E R6(18) Page: 2 PARAMRT'BRB, u9/1 MDL MAL KW-4 MW-5 NW-6 MW-7 Mw-8 49, 4-Nitrophencl 3.17 $0.000 --- u --- u --- v •-- V --- u 50. Pantachlorophancl 9.33 25,D00 --- V --- U --- u -_- V - V 51, Phenol 1.66 10,000 --- u --- u --- V -•- U •.. V 52. 2,3,4,6-Tatrachlorophenol 3112 10.000 --- u --- u --- U --- u --- u 53. 214,5-Trichlorophanol 4.17 20.000 --- V --- u --- u --- V --- V 54. 2,4,6-Trichlorophonol ],64 10.000 --- u --- u --- V --- U --- u 55. Aoetophenone 2.89 10.000 --- Ti --- U --- u -•- u --- V 56. 2-Acetylsminofluorane 3.98 20.000 --- U --- u --- u --- u u 57. 4-Aminnhiphsnyl 4.22 20.000 --- u - U --- u --- u -- V S0. Dencyl alcohol 4.47 20.000 --- u --- u --- u --- u --- v 59. 4-Ghloroaniline 3.36 20.000 --- u --- U --- u --- u --- V 60. Chlorobenzilata 5.12 10.000 --- V --- V --- v --- u --- v 61. ulallate 2.90 10.000 --- u --- u --- U --- u --- u 62. Dibencaturan 4.20 10.000 --- u --- u 4.91, S --- u --- u 63, 3,31-Dich1probenzidine 4.22 20.000 --- u --- D --- u --- U --- U 64. Dim4thaate 3.96 20.000 --- V --- u --- u --- u --- u 65, P-Dimmehylaminonzobenzene 2.89 10.000 --- u --- u - D --- u --- u 66. 7,12-Din@thylbenztaIant 5.20 10.060 --- u --- V --- u --- u --- u 67, 3,3-pimelhylhenzidine 3.21 10.000 --- u --- V --- u •-- u •-- u 6B. 1,3-Dinitrobancene a,e9 20.000 --- u •-• V --- u --- u --- u 69, ❑ipheAylamine 5.10 10.000 --- V --- u --- u --- u --- V 70. Disullaton 4.28 10,000 --- u _-- 11 --- u --- u --- V 71. 8amphur 3.9E 20.000 --- u --- u --- u --- u --- u 72, Hexaahlarnpropens 4.32 10.000 --- u --- u --- u --- u --- V 73. Is*sarrbla 2.66 ip.000 --- U --- u --- U u ••• U 14, Reppne 2.7E 20.0o0 --- V --- u --- u --- u --- V 75. Mathapyrilana 3.54 100.000 --- u --- u --- V --- u •-• U 16, 3-Nethy iah41pnthrapa 4.21 10.000 --- u --- u --- u --- u --- u 77. 2-Me thy lna¢hthalone 3.79 10.000 --- u --- V --- u --- u --- V 78, mothyl Parathion 4.32 10.000 --- u --- u --- u --- u --- u 79. m-cromol 3.e1 10,000 --- u - V --- u --- u --- u 00. 1,4-Naphthoquinone 4.00 1D.D00 --- u --- V --- u --- u ,-- u 81, 1-N4hthyiantipe 5.61 10,000 --- u --- V --- u --- u --- D B2. 2-Naphthylamine 4.62 10.000 --- u --- U --- u --- u --- u e3, 2-Nitr0aniline 3.61 $0.D00 --- a --- u --- u --- V u B4. 3-Nitroantline 4.81 50.000 --- V --- u --- u --- u --- u $5. 4-Nitroani]line 4,22 20,000 -_- u --- u --- u --- V --- U 86. 5-Nitro-4-Tuluidine 4.01 10.000 --- V --- V --- u --- u --- u e7, N-Nitrosodi-n-butYlamine 3,63 10.000 --- u --- V _-- u --- V --- V 60. N-Nitroeadiethylamine 3.B3 20.000 --- u --- u --- tl --- u --- V 69, N-Nitrosamethylethyl&nine 3,83 10,000 --- V --- u -- u --- u --- V 90. N-Nitroeapiparidine 5.19 20.000 --- u --- u --- u --- u --- u 91. N-Nitroaapyrraiidiae 2.89 10.000 --- u --- V -- u - u - u 92. earathion 3.12 10.000 --- U --- u --- V --- u --- t] 93. Pentechloxabenaene 3.9a 10.000 --- u --- u -- V --- V --- u 94. 2entachloronitrobencene 3.71 20.000 --- u --- U --- 11 --- u --- u 95. phanacetin 4.41 20,000 .-- u --- u --- V 56. 1,4-genaenediemina 2.99 10.0DO --- ❑ --- U --- U --- U --- ll ,7 - Estimated value between the MIX, and MAL, U . below ALL Quantitation Limits. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA I hgmpmmAd Drinking water IDt 37715 wamtewaCer xns 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE CREENVILLE, NC 27634 REVIEWED BY: PRONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 ANALYST: HIC DATE COLLECTED: 12/09/21 Page: 3 DATE EXTRACTED: 12/10/21 DATE ANALYZED: 12/30/21 DATE REPORTED: 07/19/22 SEMI -VOLATILE ORGANIC$ EPA METHOD 8270E R6(18) rARANET$x@, uU/1 MDL MRL Mw-4 KW-5 Mw-6 Mw-7 Mw-@ 97. Phorat! 3186 10.000 --- U --- U --- U --- U --- V 9g, Fronamids 3,69 10.000 --- U --- U --- U --- U --- U 99. safrbl4 4,12 10.000 --- U --- U --- it --- U --- U 100, 1,2,4,5-Tetrach10r0hant0n0 5101 10�000 --- U --- V --- U --- U --- U 101. Thiadnsid 4.62 20.@00 --- U --- U --- U --- u --- v 102. U-T4luidine 4.11 10,000 --- U --- V --- U --- V U 103. 1,3,5-Trinitrobensene 3.98 10.000 --- V --- U --- U --- V --- U 104. C,0,0-Triethy2 Phoephorathioate 3.61 10,000 --- U --- U --- U --- U --- U 105. Rexachlorbethmne 1149 10.004 --- U --- U V ... U --- U 106. iagdrin 3.11 20,000 --- U --- u -- U --- U --- U i ■ Retimated value bitwaen the XDL and MRL, U • aglow ALL Quantitation Limits, DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA EET Hmmmflm� 'd, jw alp colm hdo Drinking water ID: 37725 NAIL.*water In1 14 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR, JilDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY. LANDFILL APPENDIX II HPA METHOD 8260D R4(18) PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 ANALYST., JAP DATE COLLECTED: 12/09/21 Page; 1 DATE REPORTED: 07/19/22 LARAMSTERS, u9I1 Date KD1, Analysed MRL 32/20/21 KW-4 12/20/21 KW-6 12/20%21 kw-7 12/22/21 NW-6 12/20/21 Trip Dlank 1. Chloromethane 0.77 3.000 --- U --_ U --- U U --- U 2. Vinyl Chloride 0.12 0.200 --- U --- U --- U --- U --- U 3, EromoMethane 0.67 10.000 --- U --- U -- U --- U --- U 4, Chlotbetharie 0.48 10,000 --- U .. U --- U --- U --- U 5. TrichloroflUoromethana 0.24 1.000 --- U --- U -•- U --- U --- U 6. 1,1-Didhloroethene 0.11 5.000 --- U --- U --- U --- U --- U 7. Acetone 9.Of 100,000 - U 12,80 J --- U 15.00 a --- U 8. IodOmethane 0126 10.000 --- U --• U --- U .-- U --- U 9, Carbon Disulfide 0.23 100,009 --- U --- V --- U --- U 10. Methylene Chloride 0,64 1.00D --- U --• U --- U --- U --- U 11, trans-1,2-Dichlbrbathene 0.23 5.000 --- tf U --- U --- U --- U 12. lrl-DidhlDYOethane 0�20 5.000 --- V --- U --- U --- U --- U 13. Vinyl A.oetate 0.20 50.000 --- U -•- U V --- U --- U 14. Cie-1,2-Dichloroothtne 0.25 5.000 --- U --- u --- U U --- U 15. 2-DOtan0no 2,21 100.000 --- V U --- U --- U --- U 16, 8romochloromethan• 0.27 a.DD0 --- U --- V --- U --- U --- U 17. Chloroform 0,25 5.000 --- U --- U --- U --- U --- U 10, 1,1.1-Trichloroathans 0.19 1.000 --- U --- U --- V --- U U 19. Carbon Tetrachloride 0104 0.200 ... U --- V --- U --- U --- U 20. Denzone 0,24 1.000 ... U 0.39 17 --- U --- U ••• U 21, 1,2-Dichlorosthane 0.02 0.200 --- U --- U --- U 0.03 J --- U 22. TriChloro*thpne 0.23 1.000 ••. U --- U --- U --- U --- U 23. 1,2-Dichloropropahe D.04 0.200 --- U --- U --- 11 0.04 J --- U 24. DromodLahloromethans D,04 0.200 -•- U --- U --- U --- U -•• U 25. Cim-1,3-Dichlotopropene D.06 0.200 --- U --• U --" U --- U ,-- U 26. 4-Methyl-2-gantanona 1.19 10D,000 --- U --- V --- U --- U --• U 27. Toluene 0.23 1.000 --- U 0.50 4 --- V --- U --- V 28. trano-1,3-Dioh1oropropens 0,04 0.200 --- U --- U --- U --- V --- V 29. 1,1,2-TrichlorCethane 0.03 D.200 U --• U --- U --- U --- V 30. TetrachloxOethens 0,z0 0.200 - U --- lu --- U --- U --- U 31, 2-Hexanone 1.57 5D.000 -,- U --• U --- U --- U --- U 32. 1?ibY4m40h147C0me[hone 0.03 0.200 --• U U --- U --- U --- U 33, 1,2-Dibromoethene 0.03 0.200 --- U -•• U --- U --- V ••. U 34. Chlorbbensene 0.30 3.000 --- U ... U --- U --- U --- U 35, 1,1,1,2-Tetrachloroethane 0.22 2.000 --- U --- U --- U --- U --- U 36. 'Sthylbentene 0.21 1,000 --- U 0.26 J --- U --- U --- U 37, xylenes 0.60 3.000 --- U --- U --- U --• U --- U 38, Dibromomethen• 0.25 10.000 - U ... U --- U --- U --- U 39. atyrane 0.19 2.000 --- U --- U --- U --- U ... U 40. gromoform 0.20 3,000 --- U U --- U --- U --- U 41, 1,1,2,1-Tetrachloroethane 0,63 0.200 --- V --- U --- U --- U ••• U 42. 1,2.3-TriChloropropane 0.09 o.200 --- U --• U --- U ... U --- U 43. 1,4-Dichiorobenzene 0.39 1.0D0 --- U --- U --- U --- U ••• U 44. 1,2.0iohlorobenzene 0.32 5.000 --- U - U U --- V --- U 45, 1,2-Dibx0mo-3-Chl0ropropane O,oT 0.200 --- V --- U --- U --- U --- U 46. Acrylonitrile 2.72 200,000 --- if --- U -•- v --- u --- U 47� trans-1,4•Dichloro-2-6utene 0.42 100.DOD --- U --- U --- V •-- U --- U J - Estimated valise between Cho MDL and MRL, U r Below ALL Quantitation Limits. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA �Rwmoflma rij, kc-'a pufflbd Drihking water IDL 37715 wastewater IDe 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON ihHITZHURST 802 RECYCLING LANE GREENVILLE, NC 27834 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 ANALYST: TAP DATE COLLECTED: 12/09/21 Page: 2 DATE REPORTED: 0 7 / 19 / 2 2 REVIEWED gY: J •, LANDFILL APPENDIX II EPA METHOD 8260D 14 (18) pate Analyzed 12/20/31 12/20/21 12/20/21 12/21/21 12/20/21 MW-4 NW-6 NW-7 my-8 Trip FARAMBTBRA, u9/1 MnL MRL Blank 48. ACrolaie 1.97 4.000 --- V --- V --- u --- V =-- u 49, Allyl Chloride 0.20 20.000 --- V --- A --- V --- V --- u $0. Chlorbpr4n4 0,21 20.000 --- V --- V --- V --- V u 51, 1,3-Diohlorobanzoaa 0.41 5.000 --- it ... tl '-- U --" V --- U $2, DiVhlorodifluoromethane 0,51 5.000 --- u --- U --- V --- rr 53, 1,3-niehloropropane 0.20 1.000 U --- V --- V --- V •__ U 54, 2,2-Diehloropropans 0.17 15.000 --- V --- V -"- u --- u --" U 55. 1,1-Diahloropropen■ 0.22 6.000 --- u --- u --- v --- V --- v 56, Ethyl NOthiCrylatm 0.16 10.000 --- V -- V --' U "-" V --- V 57. Raxaahlorobucadiane 0.10 0.200 --- v ... ❑ --- u 50. Tmobutyl A1Cana1 12.60 100.000 --- tr --- V --- u 59, Methacryloni.tril 1.9; 100.000 --- V --- u --- V --- V -•' u 60. Methyl Methadryl:te 0.25 30.000 --- U --- V --- IF --- V --- u 61. Naphthalene 0.47 6.D00 --- V 95.00 1.09 1 u '-- u 62, prvpionitrila 3.26 15a.D0fl --' u --- u --- U --- 0 ••• u 63. 1,2,4-T1`iahlorobanzene 0.50 14.000 --- u --- U --- V --- u --- V 64. Aaetonitri14 M .29 55.000 --- u --- V --- u --- U --- V 65. Tatrahydrofuran 0.39 1.000 --- U 15.20 18.10 22.40 --- V 96. 1,4-Diaxaria 2.71 3.000 --- U 35,7D 19,20 D1.50 --- V .7 . Entimmted value nrtwaen the MDL and MRL, U • "low ALL QUttntitation Limire. NOTE, EPA METHOD 8260D R4 (I8); MW-6, MW-7 and MW.8 received at pH>2. NOTE: EPA METHOD 8260D R4 (IS); M W 6 rrRlllitl�alene resxdt exCccdcd ius:rnment calibration range. DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA 0 w z to QD S 4)e9n o M M CZ5 n 4 ■ F LA .�_ 0 0 p'4�,� p E 4 m m M w M R P LID u d OR TALCCHLORINE.TCOLLECTION OR ugll AT COLLECTION o �" x TENIPERMFIE,°C ATCOLLECTION -r_ as o e o 9 OF CONTAINERS � Field pH Nitrate+Nitrite 0 'y � 11 Mill€ Alkalinity ` Chloride 0- Cyaziide tj K41:I� :S TDS '••� F €€ € Sulfate > ro , •:,, s: Metals > 'b 5all3 # € Sulfide 'd s Conductivity "d p su :: Temperature Field Parameter EPA 8270E G] i ' $ 8270E Du -+. n 51. : ; EPA 8081B G5 PARAMETE RSITESTS Ch m Cj G7 n m 4 � >"U n rn M 4 4 S Y ad I� 0 W U, DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA r CJ7 m m m d a O N 0 U z CID 10 :x M92�n W to w �o F to � w r � m ��Tryj r, m C ; . r, Q Q ti C3 rt." Y% C/1 w �.5 +{7 G? w Wit" N4 rn Fri "17 ?'c rn r r� Ln Q f '1 41 4] m CTtLOFI1NE, mg/1 LD G L C7 fn OR ll Al' COLLECTIpN OlR ug. ° TEMPERATURE,°C D ATCOLLECTION 4 '7 .ti G' 0 0 # Of CONTAINERS Z 8081B j]IIplICAte € 3 " ''s, 6260A App. II Cr1 4i SG 9260D App, II 2 lam] erg^,fit $260D App, II 3 8260D App. 114 4� 8151A Landfill m m m IWI. do-. } ' #i 8151A Duplicate WE ORP !J7 r � U L �L7 1� PARAMETERS/TESTS a 9 . can T m n c�� z r O rn t.r' $r' ri _ rn rr� � o C cn IN,r G'3 00 0 i 6 f: � D C7 [7j O p 2 b N DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46 s Fn En Lm7 Q 4 c T 0 ur m rr M 0 I -8A724DF270DA - ffi s Ilk Fn m - Q � '" yr m W � p Z � m v d a z t" O n 0 m C7 �* o<r;b � = Zoow a O+ n rJ � .• o m G � M c c• w 1: L 0 C OHS gLl AT COLLECTION ECTION TEMPERATURE, °C O < AT COLLECTION 1 4 P OF CONTAINERS r�7 C Field pH > Nitrate+Nitrite f7 M. Alkalinity Chloride > b Cyanide. `b C+ TDS •a Sulfate` Metals Sulfide `ti r- Conductivity 'a DO > "d Temperature Meld Parameter JEJPA 8270E G} nx,"{ 8270E Dup. 1 > EPA 8081E ( �T PARAMETERS/TFSTS rb ' m m D 9 r rr1 r rn ° IN o Q 2 Ti D )7 s DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA r m cn m DD r 0 c c� 0 C 0 Cn D ¢� D � z (7)92 n m z m z m D�zJ7 v o r I D n C p ,p r- g� O^] a m m mm Q O �J r• J O zo� ED CC)" z� � 0) M) r o o 0-4 W �� v O0 C� C;c J m Y J D D m m m O O m Sri TOTAL CHLORINE, mg/I p m m m OR ug/I AT COLLECTION < < < z n z TEMPERATURE, °C 0 0 0 O < x m { Al- COLLECTION z OF CONTAINERS ( o 8081B Duplicate `'• 8260D App. II 8260D App. II 2 G� 8260D App. II 3 G� n 8260D App. II 4 G� o c 2f 8151A Landfill 8151A Duplicate G� o ORP m z U, U, PARAMETERS/TESTS ' D m �p D m S D = m O Z 2 C7 = r0 fml c� frTl z O DC 0 0) D C7 D Z m O 77 Z n0 _ m r1 zcr) -Cr) z O -ro O x z m � j (a rn -i � D m � - -1 O ` m �� -0 O O O z ) O - m 7 7,) m r D Z N m Z DO G� m ' D l O = m O D m f Z ZO 77 D O � 9 0 C m O w 7Cm.7 z O D D m m D m OZ m D O � O = DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA ERWIN)UMM Ala h(-LPq(wP0 m do 114 OAKMONT DRIVE GREENVILLE, N.G, 27858 C & D DISPOSAL, INC. MR, iTIDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 Drinking Weteg ID: 37115 Wsatewatar ID, 10 PHONE (252) 756-6208 FAX (252) 756-0633 Il)#: 6003 C DATE COLLECTED: 12/09/21 DATE REPORTED : 07/18/22 REVIEWE1D BY: 8w-1 SW-2 SW-3 SW-4 Trip Analysis Method PARhMSTERB HDL MRL Blank Date Analyst gcde PH (field meALNUrement), Units HISSING MISSING 7.4 7.7 12/09/22 PJC 4500AB-11 Antimony, u9/l 0,03 1.0 MISSING 6i7851Nd --- U --- U 12/17121 NAB EPA200,8 Arsenic, uy/1 0.0E 5.0 MISSINU MISSING 3.0 J 0.50I7 12/17/21 NAB RPA200.9 Barium, ug/1 0.04 10.0 MISSING HI,9SING 161 22/20/21 NAB EFA2DD.8 Barium, ug/l 0.04 10.0 56.7 12/17/21 NAE BPA200.8 Beryllium, ug/l 0.02 1.0 MISSING MISSING 0.02 3' 0.22 J 12123121 NAB EPA200.0 Cadmium, u9/1 0.04 1.0 MISSING M199INa --- U .-- U 12/17/21 NAB EPA200.B Cobalt, ug/l 0.02 1.0 MISSING: MISSING 1.3 1.6 12/17/21 NAB EPA200.0 Total Chromium, ug/l 0.12 5.0 MISSING HISSING 7.1 0,66 J 12/17/21 NAB EFA200.8 Capper, ug/1 0.04 10.0 MISSING MISSING 0.31 J I J 12/17/21 NAB HPA200.B Lead, ug/l 0.03 5.0 HIBBING MISSING 0118 J 0,99.I 12/17/21 NAB EPA200.8 Nickel, ug/1 0.03 10.0 MISSING MI8$1NG 0.40 d 0.991 12/17/21 NAB SPA200,6 Selanium, ug/1 0.05 10.0 MISSING HISSING 0.46 S 0.39 J 12/17/21 HAD EPA200.8 Silver, ug/l 0.22 5.0 HISSING MISSING --- U --- U 22/17/21 NAB EPA200.B ThalliUM, u9/1 Q.02 1,0 M198ING MISSING --- U 0.06 d 12/I7/21 NAB EPA2a0-B Vanadium, ug/l 0.04 1.D MISSING MISSINO OAS J 1 12/17/21 HAa EPA200.8 zinc, ug/1 0.17 10.0 MI$BING HISSING 3.55 11 12/11/21 NAB EPA200.8 Conductivity (at 254), uHhoa/cm 1.0 1,0 HIBBING HISSING 1140 358 12/09/22 PSC 2SIDB-11 Diaaolv8d ORYgen, mg/l 0.1 0.1 MISSING HISSING 4.87 3,73 12/09/21 PSC 450000-16 Temperature, 'C HISSING MISSING 7 9 12/09/21 PSC 2550E-10 9260 (dupliCete) HISSING HISSING 0260 (dupliante) HISSING MISSING 4.139 +141 12/D9/21 PSC 2560E-11 ORP, my MISSING MISSING Turbidity (Field), NTV 1.0 1.0 HISSING MISSING 22.60 29.90 la/09/21 PSC 2130e-11 All QC requirements were not mats d DupliCate data not within established limits, d + Estimated value between the MDL and NR1,, u . Below ALL 4uantitstign Limits. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA �RwD fiu@w T, hcuyoo Tn%d 114 OAKMONT DRIVE GREENVILLE. N.C. 27858 Drinking Water IPA 37715 Wastewater ID: 10 PHONE (252) 756-52u8 FAX (252) 756.0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 C MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: JAP GREENVILLE, NC 27834 DATE COLLECTED: 12/09/21 DATE ANALYZED: 12/21/22 DATE REPORTED: 07/18/22 REVIEWED BY: LANDFILL APPENDIX II EPA METHOD 8260D R4(18) ew-3 SW-4 Trip PARAMETERS, ugll MDL MRL Blank 1. ChloromethotSe 0.77 3.000 --- u --- ❑ -"" u vinyl Chloride 0.12 0.200 --- u --- ❑ --- u 3. Bromomethane 0.97 10.000 --- U --- 0 -`" U 4, chloroath*ne 0.49 10.000 --- u --- u --- u 5. TrichloralluOrOtrlfthans 0.24 11000 --` V --- U --- U 6. 1,1-olahloroethene 0.17 5.000 --- u --- U --- u 7. Acetone 9,06 100.000 9,81 J 28,60 1 -` U 6, 14domethan* 0.26 10.000 --- u --- U --- U 9, Carbon 5laulfide 0.23 100,000 --- U --- U --" V 10, Methylene Chloride 0.64 11000 --- u --- ❑ '-" u 11. trans-1,2-Dichloro*thene 0.23 5.000 --- a --- ❑ --` yj 12, 1,1-Dichloraathane 0.20 5.400 --- u --- u --- u 13, Vinyl Acetate 0.20 50.000 --- a ___ a --- u 14. Ci9-1,2-Diahl0r0ethene 0.25 5.000 --- u "-` U --" u 15, 2-8utanone 2,21 200.000 --- u 2.79 S ... u 15. Bromochloromathana 0.27 3.000 --` p --- - u 17, Chloroform 0,25 5.000 --- u --- U --- u 18. 1,1,1-Triphloroethane 0,19 1.000 --- U --- U '-- u is, Carbon Tetrachloride 0.04 0,200 --- U ... U --- U 20. Benzene 0,24 1.000 --- u --- U ... u 21. 1,2-piahloro9thana 0.02 0.200 0.D2 .7 --, u --- U 22. Trichlorofthene 0.23 1,000 --- u --- 0 --- a 23. 1.2-Dichloropropane 0.04 0,200 --- u --- u -'- ❑ 24, Bromodichloromethane 0.04 0,200 --- u --- U U 25. Cis-1,3-Dichloropropene 0,06 0.200 ... ❑ --- V _.. u 25. 4-Methyl-2-P6nt8n4n0 1.19 100.000 --- ❑ --- u -". U 27, TOluane 0,23 1.000 --- a 2.06 --- V 20, trans-lr3-Oichloropropena 0.04 0.200 - - ❑ --- ❑ --` 0 29. 1,1,2-Triphloraethane 0.03 0.200 --- ❑ --- u --- U 30. TetrechlOrOGthena 0,10 0.200 --- u --- U 31. 2-He6enone 1,57 50,000 --- U ... u 32, DibrombOhloremethane 0.03 0.200 --- U _-- D --- 0 13. 1,2-Dibrempethans 0,03 0.200 --- u --- u --- U 34. ChlorObfnt4n* 0,30 3.000 --- u --- u - - U 35. 1,1,1,2-Tetrachloroathane 0.22 1.000 --- u --- u --- ❑ 36, uthylbadzeh* 0.21 1.000 - - u --- u - t1 37. Xylenfv 0,68 5.000 --- u --- ❑ --- v 39. Dibromomethane 0.28 10.000 --- u --- V --- V 39. 13tyrarle 0.19 1.000 --- u -'- u --- U 40. BromOform 0.20 3,000 --- a ._- D -_- U 41. 1,1.1,2-T*tr60hl4ro0thane 0.03 0.200 --- v --- U "'" u 42. 1,2,3-TrichloraprOpan* 0.09 4.200 --- u --- u --- u 43. 1,4-Dichlorobenaene 0.39 1.000 --- u --- u --- U 44. 1,2-Diohlorobfnrehe D.32 5,000 --- u --- U - V 45, 1.2-Dibromo-3-Chloropropane 0.07 0.200 --- U --- u --- u 46, ACXylonitrila 3.72 200.000 --- 0 --- u --- u 47. trans-1,4-Dichlora-2-Bulene 0,42 109.000 --- u '•• ❑ ."- u 40. Aorolsin 1.97 4,000 --• 0 u J . R!*timatsd value between the MDL and MRL, U • Below ALL Quantitation Limits. Page: 1 DocuSign Envelope ID: lE49C9C5-lEA4-40EE-BA46-8A724DF270DA ERWIT(OMIHOMA `l]a 1w�-p9mum0do 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 Drinking Water ID: 37715 Wastowater IDi 10 PHONE (252) 7S6-6208 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT IDI 6003 C MR. JUDSON WHITERURST 802 RECYCLING LANE ANALYST, JAP GREENVILLE, NC 27834 DATE COLLECTED: 12/09/21 DATE ANALYZED: 12/21/22 DATE REPORTED! 07/18/22 REVIEWED BY: LANDFILL APPENDIX IT EPA METHOD B260D R4(18) sw 3 Sw-4 Trip PARAMETERS, u9/l MDL MRL Blank 49. Allyl Chloride 0.20 10.000 --- u --- V - V so. Chloroprene 0.21 20.000 --- D -" u ... V 51. 1,3-bidhlarobenaene 0.42 5.000 --- u --^ V 52. DiohloTodifluoromethane 0.51 S.000 --- U 53. 1,3-Diohlorapropsne 0.22 11000 u --- u '-- V 54, 2,2-Diohlornpropane 0.17 15.000 --- V -- u tl 55. 1,1-Piahloropropene 0,22 5.000 --- U --- u --- u 56, Ethyl mthaorylate 0.16 10.000 --- u --- u - V 57. Hexachlorobutadiene 0.10 0.200 -^- V V - " u so, Ieabptyl Alaah4l 12.00 100.000 --- u --- u -•^ V 55, Methaary10nitei16 1.93 100.000 •-- u -- D --- u 60. Methyl Methadrylate 0.25 30.000 --- u ___ u ... u 61. Naphthalene 0.47 6.a00 ••• u --- V --- u 62. propionitrile 3.26 150,000 --- u --- u -•• u 63. 1,2,4-Trich1orobenxen■ 0.50 10.000 ••• u --- u --- u 69, Avatonitrile 36.29 55,000 --- u --- u --- u 65. TetrahydrOfUran 0.39 1.Ona 4.50 --- u -•" V $6. 1.4-Dioxane 2.71 3.000 12.30 --- u " ' u Page: 2 J . Estimated value betwean the XDL Ani MAb, U . Below ALL 4uanatation LlMite. DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA w cr m 8 r' su o m o � 4 N A b CD {a o (N py t O N W M z G3 co 1-4 c C7 n P . j r vt w r � y. Fco u,rc _ U1 N � 01 m TOTAL CHLORINE, mg/l �i C7 �I '� m OR ugll AT COLLECTION o Q 71=MPERATURE,°C a C r m m m "us ATCOLLECTION v� ur ch vi ci cn C) ) k OF CONTAINERS s; ;,,, , Field PH Y b Metals y ro Mr Conductivity DO Temperature '0 o I*' m Pi $200 Dup. 1 8260 Dup. 2 t n 8260 Dup. 3 }€fl # 8260DUP. 4 t� 8260D App. 11 8260D App. II 2 4� s 8260D App. li 3 4� g w ,. b • , 0.N m Field Parameter ram, PARAMETERSITESTS 2 g G U m o rn as m P z m stir = Q_n o `r, n m DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA kgoo qwmuoad ► - � �. .fir •' `•y 114 OAKMONT DRIVE GREENVILLE. N.C. 27858 C & D DISPOSAL, INC. MR, JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 PARAMBTBRS MDL ME Drinking Water ID, 37715 Wastewater 16a 10 PHONE (252) 756-6208 FAX (252) 756-0633 IA#: 6003 A DATE COLLECTED: 12/08/21 DATE REP0RT9D : 07/18/22 REVIEwZn BY: z Z�- MW-is MW-1D KW-2s KW-2D MW-39 Analysis Method Date Analyst Cade PH (field measurement?, Units 6.5 7.5 6.6 6,2 6.9 12/UB/21 PJC Nitrate+Nitrite as N, mg/l 0.04 D.04 0.10 0.22 0.18 --- U 1.05 12/13/21 BMD Alkalinity (to pH 4.51, mg CaCO3/1 1.0 1.9 552 3,96 6BD 190 1660 12/13/21 DNS Chloride, mg/1 2.0 )..o 84 15 79 13 230 12/11/21 D1i7 Cyanide, ug/l 5.0 5.0 --- U --- U --- U --- U - U 12/13/21 HUM 'total Dissolved Residue, mg/1 10 10 1400 1100 2D00 12/14121 JMS Total Dissolved Residue, mg/l 10 10 220 310 12/09/21 DIJ sulfate, mg/l 5.0 5.0 326 32.6 169 26.0 99.5 12/23/21 LaJ Antimony, ug/1 0.03 1.0 9.21J --- U 0.09 J 12/20/21 HAD Antimony, ug/1 0.03 1.D 0.16 a 0.21 J 12121/21 NAB Arsenio, ug/l 0.08 5.0 5.9 0,69 J 6.9 0.54 J 25 12/17/21 NAB Barium, u7/1 0.04 10.0 249 190 771 12/20/21 NAB Barium, ug/1 0.04 10.0 20.5 12/17/21 NAB Barium, ug/l 0,04 10.0 16.0 12/22/21 HAS Beryllium, ug/1 0.03 1.0 0.09 J ... U 0.06 J 12/21/21 NAB Beryllium, ug/l 0.02 1.0 C.04 J 0.45 J 12/17/21 NA13 Cadmium, ugfl 0.04 1.0 --- U --- U --- U --- u --- u 12/17/21 NA9 cobalt, ug/l 0.02 1.0 1.6 0.05 J 0.84 J 0.00 J 3.6 12/17/21 NAB Total Chromium, u9/1 U.12 5.0 10 0.29 J 4.2 J 0,32 J 25 l2/17/21 NAB copper, ug/1 6.04 10.0 0.99 J 0.24 J 0.30 J 0.36 J 0.411 12117/21 NAB ZrOA, ug/l 4.96 50.0 3046 515 10649 395 11313 12/14/21 [,P,7 Manganeae, ug/l 0.11 10.0 283 21 495 15 1220 12/14/21 LYC Load, Ug/l 0.03 5.0 0.46 J 0.05 J 2.3.7 0.15.7 0.06 J 12/17/21 NAB Mercury, ugfl 0.05 4.20 --- U --- U --- U ... U --- D 12/22/21 MTH Niokel, Ug/l 0.03 1010 a I a J 0.24 J 1.D J 0.34 J 2.9 J 12/27/21 NAB Selenium, ug/l 0.05 10.0 1.9 J 0.21 J 1.0 J --- U 1.4 J 12/17/21 NAB silver, Ug/1 0.22 5.0 --- U ... U --- U -'- U --- U 22/27/21 NAB Thallium, ug/l 0.02 1.0 --- U --- U --- U 0.04 J 0,04 J 12/17/21 NAB Tin, u9/1 0.05 100.0 --- U --- U --- U --- U --- 0 12/21/21 NAB vanadium, ug/l 0,04 1.0 3 0.34 J 2 0.16 J B 12/17/31 NAB Zinc, ug/1 0.17 10.0 3.1 J 1.4 J 0.80 J 11 1.6 a 12/17/21 NAB 8Ulfide, ug/l 10D loon --- V --- U --- U --- U --- U 12/09/21 I.FJ Conductivity (at 25c). uMhoo/cm 1.0 1.0 1733 360 1764 442 3703 12/08/21 FTC pi9aclved Oxygen, mg/l 0.1 0.1 0.93 0.27 0.01 D.63 0.77 12/08/21 PJC Temperature, "C 14 15 15 13 11 12/00/21 PJC static water Level, Poet 9.32 9.55 11.57 13.14 12.68 12foS/21 PJC Well Depth, feet 17.21 33.75 26.57 3E.17 22.24 12/00/21 PJC ❑RP, my +235 +1D7 +127 +110 4139 12/08/21 Pic Turbidity (Pieldl, NTlf 1.0 1.0 7.02 1,96 7.93 6.07 2.12 12/00/21 PJC p . gytimated value between the KDL and MRL, U - Below ALL Quantitation Writo, DocuSign Envelope ID: lE49C9C5-lEA4-40EE-BA46-8A724DF270DA 114 OAKMONT DRIVE GREENVILLE, N-C. 27858 C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27634 Drinking Water IDz 37725 W&dt9w4it6r ID, 10 PHONE (252) 756-6208 FAX (252) 756-4633 iD#: 6003 A PH> 2 DATE COLLECTED: 12/08/21 DATE REPORTED : 07/18/22 REVIEWED BY: MW-311 MW-3A Trip Analysis Method PARAMETERS MDL MRL Blank oat* Analyst code Pk (field measurement), unite 7.R 7.0 12/00/21 PJC 4500H5-11 Nitrate+Nitrite as N, mg/1 0.04 0.04 --- u --- u 12/13f21 HMI} 333.3 R2-93 Alkalinity (to pH 4.5), mg cacc3/1 1A 1.0 242 2030 12/13/21 DNS 2320E-11 Chloride, mg/i 1.0 1.0 21 131 12/13f21 IPIJ 4500CLB-11 Cyanide, ug/1 5.0 5.0 --- U --- U 12/13/21 HUM 4509CNE-11 Total Diraolved segidaa, mq/l 10 10 340 1600 12/09'/81 D19 D5907.13 sulfate, mg/1 $.0 5.0 6.3 257 12/23/21 LFJ 45000042HII Ahtimdriy, Ug/l 0.03 1.0 --- U 0.16 J 12/21/21 NAB EPA20o.9 Arsenic, ug/1 0.08 5.0 0.12 J 19 12/17/21 NAB BPA200.8 Be'eliry, ug/l 0.04 10.0 11.0 12/21/21 NAB EPA20o.B Barium, ug/1 0.04 10.0 405 12/20121 NAB EPA200.9 Bexylltum, ug/l 0.02 1.0 --- U 0.04 J 12/17/21, NAB EPA200.8 cadmium, ug/l 0.04 1.0 0.11 J --- U 12/17121 NAB EPA200.9 Cobalt, ug/l 0.02 1.0 0.02 J 4,4 12117/21 NAB EPA200.0 Total Chromium, ug/1 0,12 5.0 --- U 12 12117/21 NAB 13PA200.0 Copper, ug/l 0.04 10.0 0.06 J 0.22 J 12/17/21 NAB EPA200.$ Iron, ug/1 4.96 50.0 248 25332 12/14/21 LFJ BPA200,7 14anganegs, ug/1 0.31 10.0 23 927 12114/21 LFJ EPA200.7 beat, ug/1 0.03 5.0 --- U 0.14 J 12/17/21 NAB EPA200,B Mercury, ug/l 0.0$ 0.20 --- U --- U 12/22/21 MTM 245.1 R3-94 NiCk01, ug/l 0.03 10.0 0,19 J 2,2 J 12/17/21 NAB SPA200.0 selenium, ug/1 0.05 10.0 --- U 0.85 J 12/17/21 NAB BPA200.9 silver, u$/l 0.22 5.0 --- U --- v 12/17/2), NAB EPA200.8 Thallium, ug/1 0.02 1.0 0.02 J 0.12 J 12/17/21 NAB EPA200.9 Tin, u9/1 0.05 100.0 --- U --- tr 12/21/21 NAB BPA200.6 Vanadiutn, +19/1 0.04 1.0 0.21 J 3 12/17/2l NAB BPA200.9 zinc, ug/l 0.17 10.0 21 1.4 J 12/17/21 NAB SPA200.8 Sulfide, ug/l 100 1000 --- U --- U 12/09/2l LFJ 450082D-11 Conductivity (at 250), uMhoa/am 1.0 1.0 $28 2689 12/00121 PJC 1510E-11 VisBolved 4ky9en, mg/1 0.1 0.1 0.23 0.87 12/08/21 PJC 450000-15 Temperature, ^c 17 16 22/09/21 PJC 2550E-10 Static Water LeVel, feet 13.42 11.87 12/08/21 PJC Well Depth, feet 52.30 23.44 12/00/21 Pic ORP, my +106 +136 22/08/21 PJC 2580E-21 Turbidity (Field), NTU 1.0 1.0 5.79 7.91 12/09/21 PJC 1130E-11 J - Hatimatad vAIIA* bttwesn the MDL and MRL, U - Below ALL Ouentitation LimiLa. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA kowkcffinr-R� % h�@Tpmm' %jo 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: PESTICIDES AND PCBIS EPA METWOn 8 081B R2 (07 ) Drinking water 1Dj 37715 WaOCawtrOr ID4 10 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 A ANALYST, HIC DATE COLLECTED; 12/08/21 Page; 1 DATE EXTRACTED: 12/13/21 DATE ANALYZED: 12/14/21 DATE REPORTED: 07/18/22 PARAMETERS, ug/1 hiDL MRL NW-19 KW-lD Mw-29 MW-2D Mw-30 1. Aldrin 0.029 0.050 --- U --- U --- U --- U --- U 2. A104-BHC 0.032 0.050 --- U ... U --- U --- U --- U 3. Beta-8HC 0.031 0.050 --- U --- u --, V ,-- U --- U 4. Delta-BHC 0.030 0.050 --- U --- U -" U --- U --- U S. 13amma-8HC (Llndane) 0.032 0.050 --- U --- u --- U --- U --- U 5. Chlordane 0.32C 0.500 --- U --- U -- U --- U --- U 7. 4,4-DDD 0.053 0.100 --- U --- u --- U --- V ... U 8. 4,4-DDE 0.04E 0.100 --- U .-- U --- U --- U --- U 9. 4,4-DDT 0.052 0.100 --- U --- V --- U --- U --- U 10. DieIdrid 0.042 0.075 --- U --- t) --- U --- U --- U 11. 8ndoaulfan I 0.056 0.100 -- U --- U --- U --- U --- U 12. Endoaulfan 12 0.046 0.100 --- U - U --- U --- U --- U 13. Hndopulfan Sulfate 0.012 0.100 --- V --- U --- U --- V --- U 14. Endrin a.053 U.100 --- U --- U --- U --- V --- U 15. Endrin Aldahyde 0.068 0.100 --- U --- U - U --- V --- V 16. Haptachlor 0.039 0,050 --- U --- U --- V --- U --- U 17. Heptachlor Epoxide 0.042 0.075 --- V --- U --- U --- V --- U 16, Kethaxychlor 0.530 1.000 --- U --- U --- V --- t) --- U 19. Feb -a (Aroalore) 0.500 2.000 --- U --- U --- U --- V --- U 20. Toxaphene 0.880 1.$00 --- U --- U --" U '"" U --- U J . Eptimated value between the MDL and HRL, U . Below ALL QuantitatiCn 3AM td. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA d EfiwkooRH(M % k 9- mgTO 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPDSAL, INC. MR. IUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY:� PESTICIDES AND PCB'S EPA METHOD 8081E R2(07) Drinkiti# WnEnr mot 301s WoptlwaCar IDs 14 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 A ANALYST: xIC DATE COLLECTED: 12/08/21 Page: 2 DATE EXTRACTED: 12/13/21 DATE ANALYZED: 12/14/21 DATE REPORTED: 07/18/22 PARAMETERS, uU�l HDL MRL mbr-31) mw-3A L. Aldrin 0.022 O.050 --- u --- it 2= Alpha-Bmc 0.032 0.050 ❑ --- U 3. seta -SEC 0.031 0.D50 --- U •-• U 4= Delta-ERC 0.030 0.050 --- U --- U 5. Gamma -EEC (Lindane) 0.032 0.050 --- U --= U 6. Chlordane 0.320 0.500 --- U --- U 1. 4,4-DDD 0.051 0.100 --- U ••• U $, 4,4-DDE 0.049 0.100 --- U --- U 9. 4,4-DDT 0,052 0.100 --- U --- U 10, nieldrin 0.042 DA75 U U 11. hndomullan I 0,05G D.100 --- U --- U 22, Hnd4mµIran YT 0.046 0.100 -•- U --- U 13. Endoaulfan 9uiecte 0.077 0,100 --- U ii 14. Enarin 0,053 0.100 --- U --- U 15, Endrin Aldehyde 0.060 0.100 --- U --- U 16. Heptachlor 0.039 0.050 =-, U --- V 17. Heptachlor Epoxide 0,042 0,075 --- u ^-• U 18. Methoxychlor 0.530 1.000 --- U •-• V 19, Pcb.p (Aroclara) 0,S00 2.099 --- u --- U 20. Toxaphene 0.690 1.500 --= U -•- U d - gatimated value between the MDL and NRL, U - Below ALL ❑uantitation Limits, DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA Drinking water I37715E�UNHEM lu h-Nqu)nm d wastewater IM 10 114 OAKMON`f DRIVE PHONE (252) 756-6208 GREENVILLE, N,C, 27858 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 A MR. JMSON WHITEHURST $02 RECYCLING LANE ANALYST: HIC GREENVILLE, NC 27834 DATE COLLECTED: 12/08/21 Page: 1 DATE EXTRACTED: 12/14/21 ` DATE REPORTED; 07/18/22 REVIEWED BY: � LANDFILL APPENDIX II EPA METHOD 8151A R1(96) Data Analyzed: 12/1-7/21 12/17/21 MW-18 MW-1D PARAMBTURS, ug/l MQG MRL 1. 2,4-D 0,76 2.000 --` V '-- V 2, DiPoseb 0.54 1,000 ... u ... u 3. 2,4,5-TP 0.42 2.000 -_- a --' U 4, 2,4,5-T 0.47 21000 --- u --- u J = Ratimated valUa between the MnL and MRL, U . Below ALL ¢uaR4itation Limits. 12/17/22 I 12/10/21 I 12110/21 idW-2e ` MW-2G 1 nw-38 '-- u --- u --- u - 0 --- u ... u --- u "' u --- 0 DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA EQA' mmbd 114 OAKMONT DRIVE GREENVILLE, N.C_ 27858 CLIENT: C & D DISPOSAL, INC. MR. ,7LiDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY! LANDFILL APPENDIX 11 EPA METHOD 8151A Rl (9 6 ) 'brinkiaQ Water 1A1 37715 wastewater M 10 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 A PH>2 ANALYST: HIC DATE COLLECTED: 12/08/21. DATE EXTRACTED: 12/14/21 DATE REPORTED: 07/18/22 Date Analyzed, 12119/21 12/16/21 Mw-3D MN-3A PARAMETERS, ug/1 MDL MRL 1, 214-D 0.36 2.000 --- u u 2. Dinosob 0.54 1.000 --- u " ' V 3. 2,4,5-TP 0�42 2.D00 --- u --- u 4. 2,4,5-T 0.47 2.000 --- u --' u Page: 2 J . Eatimatad valus between the MDL end MRL, V . Below ALL Quantitation Limits. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA It W66*80;tar IDA i4 :'i ,K%-iC_,N r UHI` r PHONE (252) 756-6208 -girl NVll_LL FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 A MR. JMSODT WHITEHLTRST 802 RECYCLING LANE ANALYST: HIC GREENVILLE, NC 27834 DATE COLLECTED: 12/08/21 Paget 1 DATE EXTRACTED: 12/10/21 f DATE R8VORTED: 07/18/22 REVIEWED BY: I SEMI-VOLATILE ORGANICS EPA METHOD 8270E R6(18) Date Analysed: 12129/21 12/29/21 12/29/21 12/29/22 12/30/21 NW-19 Mw-1b KW-29 HW-2D Kw-39 PARAMHTBRB, L9/1 MDL MRL 1, Acensphthen• 2.66 10.D00 --- U --- u --- V --- u 6.2a J Z. Acenaphthylene 2.60 101000 --- u --- u --- u --- 11 '•• u 3. Anthrkdens 2.97 10.000 --- u --- u --- V --- u --- V J. benzo(a)antrhacene 4.16 10.000 --- V --- u --- t! --- V ••• u $. tenro(bjElmoranthene 3.32 10.000 --- u --- u --- V • V --- u 6. Kenzo[k]flucranthsne 4.21 i0.000 --- V u --- a --- V --- u �. Benaa(g,h,ijperylane 2.61 30.000 --- V --- u --- V --- V --- V @. Benzo [a]pyrena 3,R7 10.000 --- V --- u --- u --- U --- u 9. 4-13romophehyl Bhdnyl ether 2163 10.000 --• u --- V --- V --- u --- u 10. Butyl Eenayl Phthalate 5,79 10,000 --- U --- u --- u --- u --- u 11. ei4j2-Chlarowt314Ry) Methane 3.14 10.000 -- u --- V •-- u --- u U u. Bie(7-Chloroethyi] Sther 2.59 10.000 --- U --- u ___ a --- u --- u 13, Big(2-Chlorb-l-methylethyl) Ether 2.58 10.000 --- V --- u --- u --- u --- u 14. 2-Chloronaphtha38no 2.17 10.D00 --- u -"" V --- u --- V --- u 15, 4-Chlorophenyl Phenyl Ether 3.42 10.000 --- V --- u u 1; " - V 16L Chrysene 4.D4 1D.000 --- U --- V --- u u --- u 17. DibeAxpEa. h]enthraCene 2.70 10,000 •-• V --- u --- u --- u --- u 18. Di-N-Butyl PhthdllatR 3.09 10.000 --- u --- V ... u --- u --- u 19. Dimethyl Phthalate 3.79 10.000 ••. V --- u --- u --- V --- U 20. Diethyl Phthalate 3.92 10.000 --- u --- u --- u --' u --- V 21. 2,4-Dinitrotoluene 3.95 20.000 ••• u --- u --- V --^ V ••- U 22. 2,fi-Dinitrotoluerie 3.88 10.000 --- u --- u --- u -'- u --- u 23. bi-N-QCtyl Phthalate 2.81 10,06D ••• u --- u --' u --- V u 24. Bea-(2-Ithylhoxyl) Rhthalata 9,97 15.000 --- u -_, V --- u --- U --- u 29. PludYY•nthens 3.92 10,000 ••• u U --- u ^-- V ... u 26, Pluorene 2.95 10.000 --- u -^ V --- u --- V --- V 27. Hoxachlorobanaena 2.61 10,000 ••. u "-- u u " - u - u 28, HexaahluroCyelopERtadiene 4.16 10.000 --- u --- V ••• u --- u --- u 29• Ynden4(1,2,3-Cd3pyren■ 2.91 101000 ••• U --- u --- u --- V --- u 30. ieophorons 3.74 10.009 --- u --- V ••• u --• t7 --- u 31• Nitrolwiaane 2.85 10.000 •-• u --- u --- u u u 32, N-NitraeodimethylaRline 4,25 10.000 --- u --- V --- u --' u --- u 31. :P-Hitt444Qiphenylamine 3.95 10.000 --• u - V --- u - V --• u 34. H-Nitroeodi-N•Propylamine 4.06 1D.000 --- V -•^ u --- u '-- u " ' V 35. Phenanthr*ne 3.24 1D.000 --• u --- u __- ❑ --- V --- u 36. Pyrene 3.63 10.000 --- V _.. V -_- V --- u ._. V 37. 4-Chloro-3-Nethylphenol 9.79 20.000 --- ❑ --- V --- u --- u --- u 3e. 2-Chlorophenal 2.75 10.000 --- u --- u --- a --' u --- V 39, 0-Cresol 3.6B 10.000 --- u --- u --- u •-- u --- u 40. P-Cresol 4,12 10.000 --- V --^ u --- u --- u --- U 41, 2,4-Dichlorophenol 5.19 10.00D -•- V --- u - u -^- V --- V 42. 2,6-Dichlurop114D01 4.09 10.0oo --- u ^ u --- u --- V --- u 43. 2,4-Dimethylphenol 3.21 10.000 ••. V --- u --- u --- u --- U 44, 4,6-Dinitr0-8^Methylphenol 4.77 50.000 --- u --- it --- V --- u 45. 2,4-Din1trpphenol 4.37 50.DOD ••• u --- V --- u -- u U 46, Ethyl MethaneojIfo 7ata 5.26 20.009 --- u --- u --- U --- u --- u 47. Methyl Hathanesulforiate 4.92 10,000 -•- u --- u --- u --- u --- u d . 8stimatad value betw4Rn the MDL end NRL, V a Below ALL Quantitation Limits. DocuSign Envelope ID: lE49C9C5-lEA4-40EE-BA46-8A724DF270DA Drinking Water ID, J7715 Waatewater IDt 10 114 OAKMGNT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 27858 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 A MR. JUDSON WHITZHURST 802 RECYCLING LANE ANALYST: HIC GREENVILLE, NC 27834 DATE COLLECTED: 12/08/21 Page: 2 DATE EXTRACTED: 12/10/21 DATE REPORT8D: 137/18/22 REVIEwAn BY: �!/ SEMI -VOLATILE ORGANICS EPA METHOD 8270E R6(18) Date Analyaedi 22/29/21 22/29/21 12/29/21 12/29131 13/30121 MW-l0 NW -ID NW-20 mw-2D MW-39 PARAWMRB, U9/1 MDL MRL to, 2-NitraphwA01 3.64 10.000 --- a --- u --- u --- u 49. 4-Nitrophenol 3.11 50.D00 --- u •-• V ... a --- u --- u 50. PentachloNophenol 5.33 25.000 --- u --- u --- V --- V --- u 51, Phonol 1.$8 10.000 __- u --. u ._. u --- u --- 52. 2,1,4,6-Tetrachl0:rophanol 3.12 10.000 --•• V --, u --- V --- u --- u 53, 2,4,S-Tr1chl0xaphenul 4.17 10.000 --- u --� u '"- tr '"- tt u 54. 2,4,6-Trichloxvph*A0l 3.84 1D.D00 --- V --- V -_. V --- u --- u 55. Acetophanone 2.89 10.000 --- u --- u --' u --- u --- U 66. 2-AOetYleminoflu0Yen4 3.98 20,000 --- u •-- u •-' a •-- V --• u 57, 4-Aminobiphenyl 4.12 20.000 - u --- u --- u --- V - - u 58. Benlyl Alcohol 4.47 20.000 --- V --- u ... u --- u --. u 59. 4-Chloroaniline 3.36 20.000 --- u --- u --- u - u --- u 50. Chlorobenzilate s.12 10.000 --- u --- u ... V --- u ... u 61, niallate 211 9 10.000 --- u ___ u --- u - u --- u 62. Dibenzofuran 4.28 10.000 --- u --- u ... u ..- u --- u 63, 3,3'-Dichlorcbenzidine 4.22 20.000 --- IT --- v u - V -- V 64. Dimethvate 3.9B 2o.000 --- V --- u --- u --- u --- u 65. P-u1methylamincaacbenzene 2.89 10.000 --- a --- tl u --- V V 66. 7,12-nimethylbenz(alanthracesYe 5.29 10.000 --- u --- u --- u --- u --- u 57. l,3-Dimethylbeozidine 3.21 10.009 --- u --- u --- u --- V •-- V 68. 1,3-Dinitrobenzene 2.99 20.000 - -- u - -- u ... u - -- u -•- u 69. ❑iphanylamine 5.1D 50.000 --- u --- u --- u u V 70. Dieulfoton 4.29 10.000 ••. u --- u --- u --- u 71. samphur 3.98 20.000 --- V --- u -.. u .._ V ... U 72. Hexachloropropene 4,31 10.000 --- u --- u --- u --- u --- u 73, IeOsafrole 2.00 10.000 --- V --- V --- u --• u ... u 14. xepono 2.7$ 20.000 --- u --- u --- u --- u --- u 75. Nethapyrilone 3.54 100.000 --- ❑ --- V --- u -•" u ... u 76. 3-Hethylcholanthrehe 4.21 10.000 --- u --- u --- u --- u --- u 77. 2-Methylnaphthalene 3.79 10.000 --- V --- u --- u "'- V " - u 76. Methyl Parathion 4.32 10.06D --- u ... u --- a --' u --- u 79. M-craeol 3.81 10.000 --- u --- u --- u _.. u -.. u go. 1,4=Naphthogainarie 4.00 10.000 ••. u ••• u --- u -'- u --` u al. 1-Naphthy lamine 5.61 10.000 --- u --- u --- u =-- u --- u 82. 2-NaphthyIamino 4.62 10.000 •-- u --- u --- u --' u --- it 83, 2-Nitroaniline 3.61 5o.000 --- u --- V --- u -_- u --- u 04. 3-Nitraeniline 4.81 50.000 --- u --- u --- a --' u --- V 05, 4-Nit104niline 4.22 2D.000 --- u --- V - U -- u .-_ U B6. 5-Nitro-0-Toluidlne 4.01 10,000 --- V --- u ••- u --" V --` u 07, N-Nitrasodi-n-butylamint 3.$3 10.0D0 --- u --- u - u --- u u 08. N-Nttroaodiathylamine 3.83 20.000 ... u -" u .-- u --- li u e9. N-Nitroe0methylethylamine 3.03 10.000 --- u --- u --- V --- U --- ❑ 90. N-Nitronopiperidine 5.19 20.000 ••• u --- u --- u --- u --- u 91. N-Nitroaepyrrolidine 2.09 10.0oo --- u --- a --- U -,- U --- U 92. Parathion 3.12 10,000 ••. V --- u -•• a --- U --- u 93, Pentaahlorobenaene 3.92 10.000 --- u --- u --- ❑ "- u --- u 94. Pentachloronitrobenzene 3.71 201000 --- V --- u ••• V •-- u --- V S . Batimated value between the MDL and MRL. V e Below ALL QUentitation Limits. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA I RAFOIEHM % �EtgTI Td, NO 114 OAKMONT DRIVE GREENVILLE. N.C. 27858 Drinking Water 1Dz 37715 W&Atdwater SDY 10 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT: C & D OTSPOSAL, INC. CLIENT ID: 6003 A MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: HIC GREENVILLE, NC 27834 DATE COLLECTED: 12/08/21 DATE EXTRACTED; 12/10/21 DATE REPORTED: 07/18/22 REVIEWED HY: SEMI -VOLATILE ORGANICS EPA METHOD 9270E R6(18) Pageg 3 PikRAMIETERS, u9/1 Data Analyzads MOL HRL 12/29/21 MW-26 12/29/22 law-iD 12/29/21 MW-29 12129/21 MW-3b 19/30/21 kW-38 95. Phernaoetin 4.41 20.000 --- ❑ --- U --- D --- V --- U 96. 1,4-8.nzrdodiamine 3199 10.000 --- U --- tr --- U --- V --- U 97. Phorate 3.86 10.000 --- U --- U --- U --- U "` D 99. Pronamide 3,69 10.000 --- U --- U --- U --- U --- U 99. SALX4x4 4.12 10.0D6 --- U --- V --- U --- U --- V 100. 1,2,4,8-Tltr&chI*rob*nzena 5101 10,000 --- U --- U --- V --- U --- U 101. Thionaain 4.62 20.000 --- ❑ - ^ U --- U --- U --- U 102. 4-Toluidin* 4.11 101D00 --- U '-` U --- V "' U --- V 103. 1,3,5-Trinitrohenzerie 3.90 10.D00 --- U --- U --- 11 --- V --_ U 104. 0,D,0-Triethyl Phosphorothioate 3.51 101D00 --- U --- ❑ --- U "-- V --- U IDS. Hexeohloroathane 1.49 10.000 --- U --- U --- V --- U --- U 106. Iaodrin 3.11 20.D00 - U --- U --- U _-- ❑ --- V 1 - catimated value between the HDL and MRL, U - Helo-W ALL Uuantitation Limits. DocuSign Envelope ID: lE49C9C5-lEA4-40EE-BA46-8A724DF270DA 114 OAKMONT DnIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR, JUDSON WHITEHURST 802 RECYCLING LANE CREENVILLE, NC 27834 REVIEWED BY: SEMI -VOLATILE' ORGANICS EPA METHOD 8270E R6(18) ,""tt �61 741if WuC•Wster M 10 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 A ANALYST: HIC DATE COLLECTED: 12/08/21 DATE EXTRACTED: 12/10/21 DATE REPORTED: 07/18/22 Date Analyzed; 12/30/21 12/30/21 NW-3D KW-3A PAAAMBTER8, uB/1 MDL MRL 1, ACenaphthene Z,66 10.000 --- Ti 2.85 J 2. Acenaphthylene 2.60 10.000 --- V --- u 3. Anthraaens 2.97 10,000 --- u --- u 4. benzoCal antrhaudne 4.26 10.000 --- u --- u 5. Benzo[b]fluoranthene 3.32 10.000 --- u --- u 6. Benzo[k]fluoranthene 4.23 10.000 '-- u u 7, BenzO[y,h,i)perylens 2.61 10,000 --- u --- u S. Benzo[a3pyrenw 3.27 10.000 V --" u 9, 4-6romophenyl Phenyl Ether 2.63 10.000 --- u --- u 10. Butyl Benzyl Phthalate 5.78 10.000 --- V --- u 11. aie{2-Chloroathoxy) Methane 3.14 20,000 --- u -•• u 12. Bix(2-Chlaroathyl) Ether 2.58 10 u --- u 13. Bie{2-Chloro-l-methy1ethy1) Ether 2.5e 10.000 --- u u 14. 2-Ch3.arcnaphthe.1eRe 2.19 10.000 --- u --- u I$, 4-Chlorophenyl Phenyl Bthir 2,42 1D.900 --- u --- u 16. Chrymene 4.04 1D.000 --- V --- V 17, Dibenza(1,h)anthra0ene 2.75 10.000 --- u --- u 19. Di-N-Butyl Phthalate 3.09 10.000 --- u --- u 19. DimeChyl Phthalate 3.76 10.D00 --- u --- u 20. Diethyl Phthalate 3,92 10.000 --- u --- u 21. 2,4-PiniCrat0luerte 3.95 10.000 --- V '-' V 22, 2,6-Dinitrotcluens 3,88 10.000 --- u --- u 23. Di-N-oatyl Phthalate 2.01 10.000 --- u --- V 24. nit-(2-3thylhexy1) Phthalate 9187 15.000 --- u --- u 25, pluoranthans 3.92 1D.000 --- V •-- u 26. rluorane 2,AS 10.000 --- u --- u 27, xexaahlorobenzene 2.$1 10.000 --- u --- u 28. :1exachlorocyclopentadiene 4.16 10.000 --- u --- u 25. Zndsno[1,2,3-Cd]pyrene 2.91 10,000 --- u --- u 30. Iaophorone 1.74 20.000 --- u --- u 31. Nitrobenzene 2.85 10.000 --- u --- V 32. N-Nitrcmadimsthyldmine 4.25 20,000 --- V --- u 33, N-Nitraeodiphenylamins 3.35 10.000 --- u --- u 34. N-Nitroeodi-N-Pr0py1amin4 4,06 10.000 --- u --- u 35, phananthrane 3.24 10.000 --- u --- u 36. Pyrene 3,63 ID.000 --- u --- u 37, 4-Chloro-3-Nethylphenol 3.79 20.000 --- U --- u 38. 2-Chlorophenol 2.75 10.000 --- u --- u 39. Q-Creeol 3.65 10,000 --- V --- u 40. P-Cresol 4.12 10.40D ..- V --- u 41. 2,4-Dichlorophsnol 5.19 10.000 --- u --• u 42. 2,5-Dichloraphsh4l 4.89 10.000 --- u •-- D 43, 2,4-Dimwthy1phen01 3,21 10.000 u --- u 44. 4,6-1Dinitru-2-N*thylphen01 4.77 50.000 --- u --- u 45. 2,4-Dinitrophenal 4.37 50.000 --- V •• V 45, Ethyl Methah9ev1fQAmt8 5.26 20.000 --- U --- u 41, mathyl Nethaneeuli0d#te 9,42 10.000 --- u --- V Page: 4 J . satimaven vague notween cne mma DocuSign Envelope ID: lE49C9C5-lEA4-40EE-BA46-8A724DF270DA Em"�o�� N@,�,00TP-Q d 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 Drinking Water M 3771$ wastewater to, 10 PHONE �252) 756-6208 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 A MR. _TUDSON WHITEHURS'T 502 RECYCLING LANE ANALYST: HIC GREENVILLE, NC 27834 DATE COLLECTED: 12/08/21 DATE EXTRACTED: 12/10/21 ./ DATE REPORTED: 07/18/22 REVIEWED BY: SEMI --VOLATILE ORGANICS EPA METHOD 8270E R6 f181 PARAMBTURB, U9f1 Date Analyzed, MDL MR:, 12/30/21 14w-3D 12/3D/21 MW-3A 40, 2-Nitrophenol 3.44 10.D00 --- U --- U 49. 4-Nitrophenol 3.17 50,000 --- V I --- U $0, Pentachlorophanol $,33 25.000 ... U V 51. Phaaol 1.85 10.000 --_ p _.. U $2, 2,3,4,6-Tatrachlorophenol 3.12 1D.000 --- U --- U 53. 2,4,5=Trichlcraphsnal 4.17 10,000 --- V --- U 54, 2,4,6-Tr10hl0Y0Vb*n01 1.84 10.D00 --- tt _-- U 55. Acatophenone 2.09 20,000 --- U --- U 54, 2-AOetylamindflU6Ybn4 3.98 20.000 --_ U --- U 51, 4-Aminobighenyl 4.12 20.000 --- U --- V 59, 89ntyl Alcohol 4.47 20.000 --- U --- U 59. 4-Chluroaniline 3.36 20.PDo --- U --- B 60, Chlarobenzilate 5.12 10.000 -- U --- U 61. Diallate 2.98 10.099 --- ❑ --- U 62. DiboRaoturan 4128 10.000 --- V --- U 63. 3,31_Dio]tlo)cobenaidine 4.22 20.000 --- U --- U 64. Dimethpats 3.96 20.000 --- U --- U $5. P-Dimathylamincazohenzone 2.89 10.400 --- U --- U 66. 7,12-Dimethylbenz(41AnthY4kCens 5�26 10.000 --- U --- U 67. 3,3-Dimathylban•tidina 3.21 10.000 --- U --- U 60. 1,3-Dinitrobenzana 2.89 20.000 =_- U --- U $9. Diphenylamin4 $.10 10,000 U --- U 70, Dieultoton 4.28 10 000 -_= U --- U 71, Pamphur 3.90 20,000 --- U --- U 72. xaxachl6YOpYo&OP4 4.31 20.000 --- U --- V 73. 1e0844role 2.08 10.000 --- V --- V 74, Kepone 2.70 20.000 --- U --- U 7S. Mathapyrilene 3.54 100.000 --- V --- U 76, 3-Methylchvlanthrens 4.21 10.000 --- U --- U 77. 2-Methy1naphthalene 3,79 10.000 =-- U --- U 78. Methyl Parathion 4.32 10.000 --- U --- u 79. m-Cresol 3.81 1D.000 --- U --- U 00. 1,4-NAphthoquincne 4.0D 1D.00D •_- U --- U 01, 1-Naphthylami,na 5.61 10.000 --- U --- U 82. 2-Naphthylamine 4.52 10.000 •-- U --- U 83, 2-Nitronnilin4 3.51 50.D00 --- U --- U 04. 3-N1tx0&n1line 4.01 50.000 -- V --- U 85. 4-NStraanil104 4.22 20.000 - U --- U 96, 5-Nitro-0-Toluidiria 4.01 10.000 --- U --- U 07. N-Nitruoodi=n butylemine 3.63 20.000 --- U --- U 98. N-NitrgsodisthylAmintr 3.03 20.000 --- U --- U 89, N-NitrOMOMOthylethylamins 3.83 lQA00 --- U --- U 9D. N-NitrOsopiperidihe 5.19 20.000 --- U _-- U 91. N-Nitroaopyrrolldine 2.89 10.00 --- U --- U 92. parathion 3.12 10.000 --- 11 --- U 93, Pontachlorobenzene 3.92 10,00D --- U --- IT 94. PentOChloronitrobentena 3.71 20.000 --- U --- V Page: 5 J ■ zotimatad value between the MDL and NRL, lI - Below ALL 9uantitatiOA TAMita. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA I�HwIQ�Uum- M I hrr(A0 ffP0 mmUd 114 OAKMONT DRIVE GREENVILLE, N_C_ 27B58 At�"I%i up water Ybr 37715 waatawater ZDi 20 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID; 6003 A MR. JUDSON WHITERURST 802 RECYCLING LANE ANALYST, HIC GREENVILLE, NC 27834 DATE COLLECTED: 12/08/21 DATE EXTRACTED: 12/10/21 DATE REPORTED: 07/18/22 REVIEWED BY: SEMI -VOLATILE ORGANICS EPA METHOD 8270E R6(18) PARAWST&R8. ug/l Date Analyzed: MDL MRL 12/30/21 Mw-3D 12/30/21 KW-3x 95. Phenacatin 4.41 20,000 --- V --- U 96. 1,4-Benzenediamine 2.19 10.000 --- U - V 97. PhorRte 3.a4 10,000 --- V --- U 96, Pronamido 3.69 10.000 --- U --- tt 99. Sairole 4.12 10.000 --- V --- U 100. 1,2,4,5-T8tra0hjorQbenzsne 5.01 20.000 --- U U 101. Thionazin 4.63 20.000 --- v -•- U 102. C-ToIUidin♦ 4.11 1D.000 --- U tl 103. 1,3,5-Txinitrobsnx4bn• 3.99 10.000 --- V --- U 104, 0,0,0-Tristhyl Phgeph4rothioata 1,61 1D.000 --- U --- U 103. Hexachloxasthane 1.49 10.000 --- V --- U 106. leodrin 1.11 20.000 --- U --- u Page: 6 .7 . 8etimsted value between Chs MDL and MRL, U . Below ALL Quantitation Limits• DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA �Rwff ug[ do ��r��U��d D7titkiiki Mki it Xbi 37715 Wastewater M 10 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE. N.C. 27858 FAX (252) 756-0633 CLIENT: C & D D19POSAL, INC. CLIENT ID: 6003 A MR. =SON WHIT8HU'RST 802 RECYCLING LANE ANALYST: JAP GREENVILLE, NC 27834 DATE COLLECTED: 12/08/21 Page: I DATE ANALYZED: 12/20/21 DATE REPORTED: 07/18/22 REVIEWED BY: LANDFILL APPENDIX IT EPA METHOD 8260p R4(18) Mw-13 Mw-ID Mw-29 KW-2D MW-36 p ARAM6TB[i6, u971 MDL MRL 1. ChIaramethena 0.77 3.4aD --- V --- u --- u --- u •-^ u 2, Vinyl Chloride 0.12 0.200 --- u -- V __ u --- u u 3. .9romomethans 0.67 10.000 --- V --- u --- u --- u " ` u 4. Chluroethane 0.49 10.000 --- u --- u --- u --- u --- u 5. Triahloroflu0rumethane 0.24 1.000 --- V --- U '"- V --- u -• U 6. 1,1-Diuhloroothene 0.17 5.000 --- a --- u --' u - - u u 7. Aoetane 9.05 100,000 --- V _.. V -__ u --- u 12.20 S 9, Iodomethant 0.26 10.000 --- u --- u --- u --- U --- u 9. Carbon Disulfide 0.23 100.000 --- V --- u -_- U ___ u ... q 10, Methylana Chloride 0,64 1.000 --- u --- u •-• u -`- u u 11. trans-1.2-Dichloroethens 0.23 5,000 --- V --- U --- u --- u -^- V 12. 1,1-DiChlorosth4ns 0.20 5.0D0 --- u --- u ... u --- V u 13, Vinyl Acetate 0.20 50.000 --- V --- V --- V --- u ••. V 14. Cie-1,1-Dichlorosthene 0.25 5.000 --- u --- u u --- u u 15. 2-Sutanone 2.21 100,000 --- u --^ u --- V --- u •-• u 16. Bromochlurometh4Pe 0.27 3.000 --- u --' u --- u --- 1) -'- u 17. Chloroform 0.25 5,000 -.. u --- u --- U --- u ... u 10. 1,1,1-Tr10hlOr06thane 0.19 1.000 --- V --- u --- u --- V --- u 19, Carbon Tetrachloride 0.04 0.200 ... u ... u --- u --` u --- U 20. Benzene 0.24 1.000 --- U --- u --- u --- u 0.93 J 21. 1,2-Dich2orostharie 0,02 0.200 --- u --- u 0.02 J --- u 0.06 17 22. Trichloroethene 0.23 1.000 --- V --- u --- V --- u --' U 23, 1r2-Dichloropropane 0.04 0.200 --- u --- u ___ u --- u 0.04 1 24. nramodichloromethano 0.04 0.200 ••. V --- u --- u --- V -•- u 25, Cie-1,3-Dichloropropene 0.06 0,200 --- u --- u --- u --- t1 --- u 26, 4-Methyl-2-Pentanone 1.19 100,000 ... V --- u -•- u --• u ... u 27. Toluene 0.23 1.000 --- u --- u --- u --- u --- u 29. trans-113-Dichloropropeno 0,04 0.200 ••. u --- V --- V V .-- u 29. 1,1,a-Triahloroe thans 0.03 0.200 --- u --- u --- u --- u --- u 30• Tetraahiornethene 0.10 0.200 ••• u --- u --- U U V 31, 2-Nexanons 1.57 50.000 --- u --- u --- u --" ll --- u 32. Dibromoahloramethaae 0.03 0.200 --- u --- u ... u V V 33. 1,2-Dibrom0ethane 0.03 0.200 --- u --- u --- u --- V --- u 34. Chlorobenzens 0.30 3.000 --- u --- u •-- V _.. V .-- u 35, X,1,1,2-Tetraahloroethane 0,22 1,009 --- u --- u --- u --- u --- u 36. sthyihenzens 0.22 1.000 --- V --- u -'- V 37. xylanes 0.66 5.000 --- u .__ u -__ u --. u -•• u 30. Dibromemethane 0.29 10.000 --- u --- u -._ V --- V u 39. styrene 0,19 1.000 --- u --- u --- u ___ u _.. u 40. Bromalorm 0.20 3.000 -•- u --- u --- V --- u --- u 41. 1,1,2,2-Tetrachlorouthane 0.03 0.200 --- V --- u --- u --- u -"• u 42, 1,2,3-Trich10r0pY0pan4 0.09 0.200 --- U --- U --- A --- u --- V 43. 1,4-Dichlorobenmans 0.39 1.000 --- u --- u --- a --- u --- u 44. 1,2-Dichlorobenzene 0.32 5.000 ... u --- u --- Ti --- u --- u 45. 1,2-Dibram0-3-Chl0r0Pr0pane 0,07 0.209 --- u -`- u -`- u --- u --- U 46• Acrylonitrile 2.72 200.000 --- V --* V -'- V --- V `-- u 47, trana-1,4-Diahlorc-2-Butene 0.42 100,00C --- u --- u --- u --- u --- u 49. Acralein 1.97 4,000 --- V --- u --- 11 --' v --- u i m Ratimated V41Ue between tlse MDL and MRL, U � Below ALL gUentitation Limita. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA FEW'no fimM % D are 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHZTEHURBT 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: LANDFTLL APPENDIX II EPA METHOD 8260D R4(16) MW-1 PARAMBTE,RS, ugi1 UDL lditL 49, Allyl Chloride 0,20 10.000 so. C111oropronm 0.21 20.000 - 51, 1,3-Dichlorobaaaene 0.41 5.000 - 52. Diohl0rgdi[1u0ramethan0 0.51 5.000 - 53. 1,3-Dichloropropane 0,28 1.000 - 54. 2,2-Di0hloropropana 0.17 15.000 - 55. 1,1-oichloropropone 0122 5.000 - 56. Ethyl MathnCrylata 9.15 10,000 - 57. Hexaohiorobutadiene 0.10 0,200 - 58, 120buty2 Alcohol 12,80 100.000 $9. Hethacrylpnitrile 1.93 100.000 - 60. Methyl MathACry1Ate 0.25 30.000 61, Naphthalene 0.47 6.000 62. propionitril! 3.26 150.000 - 63. 1,2,4-Triehlorobtntana 0.50 10.000 - 64, k4etonitrile 36.29 55.000 65. Tltrahydro[uran 0.39 1.000 4 65, 1,4-Dioxane 2,71 3.000 70 Driallaftsx avatar *1 JiI13 Woffitaxater SD, 10 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 A ANALYST: JAP DATE COLLECTED: 12/08/21 Page: 2 DATE ANALYZED: 12/20/21 DATE REPORTED: 07/18/22 MW-in M7P-as Mw-2n NW-30 .'V ___ V _-- V --- u ___ u - V --- U --- V M-- V --- u - V --- a --- u - -- u U --- a ... u --- D --- V -- u --` t1 " V - - V --- u - V --- u ... V --- U .._ V ._ V •-- u --- V --- V --- u - V --- U --- V --- V --- u - u --- u --- V --- V U -- V -'- U - V --- V --- u -- V ^-- V --- V •-- V V V --- u .__ V --- V - -- v --- a --- d - v ._ U -__ V -_- V --- V --- u 77 14,80 9.24 --- V 24.80 10 --- u 38.50 --- V 147.00 ,7 • getimated valu• between the MDL and XRL, U • Relpw ALL QuantitatiOn Limits, NOTE: EPA METH0D &260D R4 (IS): MW-3S received at pH }2. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA kfiw'k WHOM % k9@00 mudo 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 Drinking Water IAt 37715 waatswater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 A DER. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: TAP GREENVILLE, NC 27834 DATE COLLECTED: 12/08/21 Page: 3 DATE ANALYZED: 12/20/21 DATE REPORTED: 07/18/22 REVIEWHD BY: 'x-- /'X�- LANDFILL APPENDIX II EPA METHOD 8260D R4 (18) PKRAMXT$R9, u$/1 MDL MRL Mw-ID Mli-3A Trip Blank 1. Chlorpmethane 0.77 3.000 --- V --- U --- U 2. Vinyl Chloride 0,12 0.200 - v --- 11 U 3. Bromomethane D.67 3UA00 --- U --- U •-- U 4. Chloroathano 0.48 10.000 - U --- U --- U 5. Trichlorofluoromethane 0.24 1.000 --- U --- V --- U G. 1,1-Dichloroathana 0,17 3.000 --- U --- U --- U 7. Acetone 9.06 100.000 --- U --- U --- U B. ladomathane 0,26 10.000 -- U --- U --- U 9. Carhgn DiBuLfids 0.23 100.000 --- U --- U --- U 10. Hathyleno Chloride 0,84 2.000 --- U --- U --- U 11, trana-1,2-Dichlcroethene 0.23 5.000 --- U --- U --- V 12. 1,1-bichloroathane 0.20 E.000 --- U --- U --- U 13. Vinyl Acetate 0.20 50.000 --- U --- U --- V 14, Cis-1,2-Dichloraethene 0.25 5,000 .-- V --- U --- U 25. 2-Butanone 2.21 100.000 --- V --- U --- U 16. Hrgesgohloromethans 0.27 3,000 --- V --- U --- U 17. Chloroform 0.25 5.000 --- U --- U --- U 18. 1,1,1-TTigh1oraethans D.19 lA 00 --- U --- U --- U 19, Carbon Tetrachloride 0.04 0.200 --- V --- U --- U 20. Ben%ene 0.24 1A00 --- U --- tr --- U 21, 1,2-Dichloroethane 0.02 0.200 --- V O.D9 J --- U 22. Trlehl9Xoethene 0.23 1,008 --- U --- it --- U 23, 1,2-Dich2orcprapane 0.04 0.200 --- U --- V - V 24. Bromodichloromathane 0.04 0.200 ... U --- if --- U 25, Cip-1,3-Dichloropropene 0.06 0.200 --- U --- U --- U 26. 4-methyl-2-Pentanona 1.19 100.000 ... U --- V --- U 27, Tgluene 0.23 1.000 --= U --- U --- U 28. trana-10-niohloropropens O,D4 0,500 --- U --- U --- U 29, 1,1,2-Trichloroethans 0.03 0.200 --- U --- U - U 30. Tatrachlgroathene 0,1D 0,200 --- U --- U --- U 31, 2-Hexanona 1.51 50.00D --- U --- U --- U 32. Dibromo9hloromethans 0.03 01200 --- U --- u --- U 33, 1,2-Dibromosthane 0.03 0.20D --- U 0.04 1 --- U 34. Chlorobenzena 0.30 3.000 --- U 0.12 a --- U 35, 1,1,1,2-Tstraohloro6thmna 0.22 1.00D --- U --- U --- U 36. Bthylbenxena 0.22 1A 00 --- U --- u --- U 37, Xylenes 0.69 5.000 --- V --- U --- U 38. Dibromomethene 0.28 14,000 --- U --- u --- U 39, 6tyrans 0.19 1,000 --- U --- U --- U 40. BrOmolorn 0.20 3.000 --- U --- u --- U 41, 1,1,2,2-Tetrachioroethans 0.03 0.200 -_- V --- U --- U 42. 1,8,3-Trichlgropropana 0.99 D.200 --- U --- l7 --- U 43. 1,4-Dich2crobenmene 0.39 1.000 - V --- U --- U 44. 1,2-Dioh1grobsnmana C.J2 $,000 --- V --- U --- U 45, 2,2-Dibromo-3-Chlorgpropmne 0.07 0.200 --- U --- U --- U 46. ilorylonitrila 2.73 200.000 --- U --- U --- U 47. trans-114-Dichlora-2-Butens 0.42 100.000 -•- U --- U --- V 40. Acrolein 1,97 4.000 --- U ••• U --- U Q a Satimated value between the MDL and HRL, U . Below ALL Quantitation Limits. E491 -40EE--BA46-I8A}j'7`�21141IjDI�F2270DA Docul{ C5-1 EA4kmw ISSiIg�1{nEnvvell�}opI lee IID: I(l ICC91 4J Ll LI 41 lJ L� 4f U LI I� I �.J 4� [J \.:e!b d LL�IIJ Dxinking Water TDc 37715 Waotswater ID1 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 A MR. =SON WHTTHHURST 802 RECYCLING LANE ANALYST: JAP GREENVILLE, NC 27834 DATE COLLECTED: 12/08/21 Page: 4 DATE ANALYZED- 12/20/21 DATE REpORTEDt 07/1$/22 R2VIEWED BY: LANDFILL .APPENDIX. II EPA METHOD 8260D R4(16) mW-3D MW-3A Trip PARAMETER,$. Ug/l MDL MRL Blank 49. Allyl Chloride 0.24 10.000 --- U --- U --- U 50. Chloraprene 0.21 20.000 --- U --- U --- U 51, 1,3-DichlOxghanaene 0.41 S.00o --- U -- U --- U 52. Diehlorodifluoromethahe 0.51 5.000 --- U --- U --- U 53, 1,3-Dichluxopropane 0.2B 1.000 --- U --- U --- U $4, 2,2-Diam oropropane 0.17 15.000 U --' U --- U 55. 2,l-Diehloroprvp6n0 0.22 5.000 --- U --- U --- U 56, Ethyl Methacrylate 0.25 10.000 --- U --- U --- U 57. Haxachlorobutadieno 0.10 0.200 -•- U --- U --' U 59. I9obutyl Alcohol 12.80 100.000 --- U --- U --- U 59. Mathacrylonitrila 1,93 100.000 --- U --- U --- U 60. maehyl Methaerylata 0.25 30.000 --- U --- U --- U 61. maphthalene 0,47 6.000 --- U --- U "" U 62, Propionitril• 3.26 150.000 --- U --- U --- U 63. 1,2,4-Txiohlorob*hz*nG 0150 10.000 --• U --- U " ' U 64. koetonitrile 36.29 55,000 --- U --- U -'- U 65. Tetrahydroluran 0,19 1.000 --- U 13.50 --- U 66, 1,4-Dioxane 2.72 3P000 --- U 05.20 -^ U S w xatimated value between the MDL and MRL, U • Below ALL puantitation Limita, DocuSign Envelope ID: lE49C9C5-lEA4-40EE-BA46-8A724DF270DA M C)%�zn Q 0 M ro CD m ML P z CID 0 4 w° rn U} J ;P. CD A Fn pp• }{ N rn m �y rn w qy m TOTAL CHLORINE, mq/ p m CR ug/I AT COLLECTION cn <• B TEMPERATURE,°C ATCOLLECTION txi 1z: h in ` t`n �n #0F0WAINFRS n7 e G* o a e c o s a-�' In Field p1l W '� Nitrate+Nitrite Alkalinity Chloride 'd Cyanide O P3 IT m m .. "UW 11 TD5 Sulfate Ni eumse: 'sv's€ s:I: .##.€g 3 Metals ro �i € ia. !i €s.. E f Sulfide ro CellductiYlty ro DO ro i:: t ? ' n :s 1. mill lh Temperature ro r Field Parameter 3 5 i EPA 8270E 1� G� 8270E Dap. 1 G� EPA 80813 C] c, PARAMETERSITESTS = O . ca 4 rn �? b7 A 4—] Z n cm7 Fu�r-yl c-j 2 O m m 05 Dj Z rn 4 o m Fn a �jn y Q r M m = fn o 2 C7 In � rrN Q # O 3o_ DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA z a 0 ob n }" Of C rao C ry "C N Q P' VP V5 n� o � V 4 . lv mrcq " Ln TOTAL CHLORIDE, mgll �I �i O �l �l w, m m OR ug/I AT COLLECTION) � a S o O - "`� -- ` TE=MPERATURE,°C AT COLLECTION fn -M G7 � �i7 � �Z #QFCANTAINERS 8081B Duplicate 4� 8260D App. ll 47 # €, 8260D App. II 2 C7 8260D App. 1131-3 47 .. 8151A Landfill Y] { #` 8151A Duplicate F€ ()RP y b e� ;v1 PARAMETERSITESTS z m a ua fir' irk �rY S z DD - m m m z Ln m n m KD Q T a L 0 < m m DocuSign Envelope ID: lE49C9C5-lEA4-40EE-BA46-8A724DF270DA 114 OAKMONT DRIVE GRrzD- 1VILLE. N.C. 27858 C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 Drinking water IDe S7715 Wastewater ID. 10 ID#: 6003 D DATE COLLECTED: 12/16/21 DATE REPORTED : 07/18/22 4 REVIEWED BY: MW-15 pew-16 MW-17 MW-148 MW-14D Ahalyslia Method PARAMETERS MDL MRL Date Analyst Code PH (field meaeuxament). Unite 6.2 6.3 6.0 618 7.9 12/16/21 PJC 4500HB-11 xitrate+Nitrite as N, mg/1 0.04 O.C4 0.05 --- U --- U --- U 0.13 12/21/21 X56 353.2 R2.93 Alkalinity (to pH 4.5), mg C&CO3/1 1.0 1.0 244 664 43 1450 243 12/20/21 D 1 a 233OD-11 chloride, mg/l 1.D 1.0 53 101 q 276 16 12/20/21 CAW 4500CL15-11 cyanide, ug/1 5.0 5.0 --- V .-- U --- U --- V - U 12/20/21 HUM 4500CNE-11 Total Dissolved Residue, mg/1 10 10 $40 1200 410 300 12/21/21 DIJ D$907-13 Total Dissolved Residue, mg/l 10 10 1400 12/23/21 JM5 D5907.13 ""fate, mg/1 5,0 5.0 152 319 334 304 --- U 01/08/22 LFJ 45000042HII Antimony, ug/1 0.03 1.0 0.19 J D.19 J --- U 1.1 0.06 J D2/05/22 NAB $PA200.8 Arsenic, ug/1 0,00 5.0 6.3 14 1.9 J 96 0.56 J 01/05/22 NAB SPA200.0 Barium, ug/l 0.04 10.0 273 499 75.2 557 02/05/22 Barium, ug/1 0.04 10.0 B.S J NAB IEPA200.0 Beryllium, u9/1 0.02 1.0 0.14c 0.06 S D.D5 0 0,06 J 0.02 J 12I22/21 NAB EPA200.9 Cadmium, ug/1 0.04 1,0 a.06 J --- U --- U .-- U 0.06 J 01105/22 NAB BPA200.0 cobalt, ug/1 9.02 1.0 0,56 J 0.02 J 0.16 J 3,5 0.04 J 22/22/21 NAB 51-A200,8 Total Chromium, ug/1 0.12 5.0 8.2 25 1.6 J $2 0.15 J 12/22/21 WAS EPA200.9 Copper, ug/1 0.04 10,0 0.69 J 0.26 J 0.241 0.24 J 0.11 a 12/22/21 NAB SPA200.8 Iron, ug/1 4.96 50.0 2123e 45945 2156 6595 26 J 12/70/21 LFJ 5PA200.7 MangA9450, U911 D.31 1010 248 494 ill 005 2 J 12/20/21 LFJ 6PA200.7 Lead, ug/l 0.03 5,0 0,74 J 0.09 S 0.21 J 0.16 J 0.06 J 12/22/71 NAB 8PA200.8 Mercury, Ug/l 0.05 0.20 --- U --- U --- U --- U --- U 12/22/21 MTM 245.1 R3-94 Mickel, ug/1 0.03 10.0 1,3 J 1.9 J 0.46 U 4.7 J 0.35 J 12/22/21 NAB 5PA200.8 Selenium, ug/l 0.05 1D.0 1.0 J 2,0 J 0.61 J 2.3 J 0.3D J 12/22/21 NAB Erh200.8 Silver, ug/l 0.22 5.0 --- U --- U --- U --- U --- U 22/22/a1 NAB 5PA200.8 Tha1D1Um, u9/1 0.02 1.0 ... U --- U --- U --- U D.28 J 12/22/21 HAD EPA200.0 Tin, ug/1 0.05 100.0 --- U --- U 0.62 J --- U --- V 02/05/22 NAB EPA200.8 vanpolUm, ug/1 0.04 1.0 14 14 3 11 0,50 J 12/22/21 NAB 3PA200.0 Zinc, ug/1 0.17 10.0 60 1.6 J 3.2 s 2.6 J 2.3 J 22/22/21 NAB aPA200.8 Sullide, Ug/l 100 1000 --- U --- U --- U --- U --- V 12/21/21 LFJ 450082D-11 Conductivity (at 254), uMhae/om 1.0 1.0 2303 1902 663 332 564 12116/21 PJC 2$10B-11 Dissolved OXY90n, mg/1 0.1 0.1 0,5g 1,96 1.82 2.52 0.64 12/16/21 FJG 45DDOO.16 Temperatvre, 'C 20 21 19 19 20 12/16/21 YJC 25509-1D Static water Level, feat $.93 9.21 9.90 6.23 7.00 12/16122 PJC Well Depth, feet 22.14 22.73 22.25 23.12 41.92 l2/16/21 FJO ORP, my +122 +136 +152 +143 +110 12/16/21 FJC 1590E-11 Turbidity (Field), NTU 1.D 1.0 6.51 7.21 5.93 17.60 2.37 12/16/21 FJC 213OD-11 All QC regUirements were not meti d Duplicate data not within established limits. Q . Estimated value between the NDL and MRL, U . Be14N ALL 9uantitation Limits. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. KR. JUDSON WHITEHUROT 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED By, PESTICIDES AND PCB'S EPA METHOD 8081E R2(07) Drinking Water Us 37715 wastewater IDs 10 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 5003 D ANALYST: HIC DATE COLLECTED: 12/16/21 DATE EXTRACTED: 1.2/21/21 DATE ANALYZED: 12/21/21 DATE REPORTED: 07/18/22 NW-15 taw-16 KW-17 Mw-148 taw-14D BARAMETBRS, ug/l MDL MRI, J. Aldrin 0.025 0.050 --- V --- u --- u u u 2, Alpha-8HC 0.032 D.650 --- u --- u -_- V _.. u ... V 3, BetA-BHC 0.011 D.050 --- V --" u --- V u u 4, Delta-8HC 0.030 0,050 --- u --- 11 --- u _._ a ... u 5. GAMMA-BHC (Lindane) 0.032 0.05D --- u --- u --- u --- u --- u 6. Chlordane 0.320 0.50O --- u --- u --- It --- u u 7. 4,4-DDD 0.D51 0.100 --- u --- u --- u ---- u ... u 9. 4,4-DDE O.D49 0.100 --- u -•- V --- V 9. 4.4-DDT 0.052 0.100 --- V -- a ... u __- u u 10. Dieldrin 0.041 D.075 --- u --^ u --" u '-- V --- V 11, En11(2eu1E&n 1 0.056 0.100 u --- u --- u - u u 12. Endosulfan 11 0.046 0.100 u --- u --- u --- u --- u 13. Bmdoaulfan @ul�ate 0.072 0.100 --- u --- V ^-- U --- u --- V 14. Hndrin 0.053 0.1D0 --- u --- u --- u --- u --- V 15. Endrin Aldehyde 0.069 0.100 --- u --- V --- u --- u --' V 16. Heptachlor 0.039 9.050 --- V V 17. HaptAchlor 8yoxide 0.042 u --- u .-- u V --- u 18. Methoxychlor 0.930 1.000 -"^ V --- V --- u --- u --- u 19. ecb-s (Aroclata) 0.500 2.000 --- u "'- V --- u u --- u �0. Toxaphan■ 01690 1.500 --- u u --- u -' u - ` u J r Estimated Ve1U0 between the MDL and M , V . Below ALL pUantitotian Limits. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA �mlwoha hmpo cow&W 114 OAKMONT DRIVE GREENVILLE, N,C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JIMSON WHITLHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: A —_ — LANDFILL APPENDIX II EPA METHOD 8151A RI(96) nsinkitiv Wkt■s m 3TUS WAAt8WLt6X IDi 10 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 D ANALYST: T IC DATE COLLECTED; 12/16/21 DATE EXTRACTED: 12/22/21 DAT'9 ANALYZED: 12/24/21 DATE REPORTED: 07/18/22 MW-25 MW-16 MW-17 ecW-149 MW-14D PARAMETHR3, "/1 MDL MRL 1. 2,4-D 4,36 2.000 --- ❑ _... U --- V 3.24 2. Dinoseb 1.54 1.00D -•• U --- U --- V _,_ U _... U 3. 21415-TP 0.42 2.000 •-- U --- V --- U .__ U ... U 4. 2,4,5•T 0.47 2,000 --• U ... U .-_ U --- i7 --- D J . Batimated value between rho MDL and NHL, u . Below ALL 4uantitption Limits. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA Prinking Water Im 37715 Wa/towaver ID: 10 114 ❑AKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 27858 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 D MR. allDSON WHITEHURST 802 RECYCLING LANE ANALYST: HIC GREENVILLE, N'C 27834 DATE COLLECTED: 12/16/21 Paga3: 1 DATE EXTRACTED: 12/20/21 DATE REPORTED: 07/18/22 REVIEWED BY: SEMI -VOLATILE ORGANICS EPA METHOD 9270E R6(18) Date Analytbd 01/20f22 01/20/22 01/21/22 D1/20122 01/20/22 raw-15 Mw-16 mW_ 17 Mw-14s NW-14D P&RhM3T81L9, uD/1 MDL MRL i, Anenaphthans 2.66 10.OD0 --- U 2. AoanaPhthylene 2.50 10A00 --- u --- u --- V --- V U 3, Anthracene 2.97 10.000 ___ U -_- V --" u __. u --- - V 4. Benzo[a]antrhaoene 4.16 10,000 --- u --- U _.. V _"- V --- u 5, aenzo[b]fluoranthane 3.32 10,000 --- V --- U -'- u " _ u 6, 8enzo[k]lluoranthehe 4.23 30.000 --- u --- V --- u ___ a -.. u 7. h,il er lens 2.61 10.000 --- u `-- u --" a --- U 8- Eenzo[e]pyrane 3.27 10.000 --- u """ u "' 9, 4-Bromophanyl Phenyl Ether 2.63 10.000 --- V --- u "-- U u 10. BUtyi $enayl Phthalate 5.78 10,000 --- u --- u ___ V --- u 11, 17Le(a-chloroathoxy) Methane 3.14 10,D00 --- V u - u --" 12, 3ie(2-Chloroethyl) Sther 2.58 10,000 --- u --- V --- U 13, EiY(2-Ch1erm-1-methy1athy2) 8ther 2.50 10.000 --- u --- u -"- u U - U 14. 2-Vhloronaphthelene 2.17 10.000 --- u --- u V _-' u 15. 4-Chlorophenyl Phenyl Ether 2.42 10.00D --- u --- u `-" u tr 16. Uhrysene 4.04 10.000 --- u `-- u --- V -"- V --- 17, Dibens�c[a,hlanthracene 2.7$ 10.000 --- V u --- 1! """ V --- u le. pi-H-Butyl Phthalate 3.09 10,000 --- u --- U --- u --- V 19, oim9thyl Phthalate 3.78 10.000 "-- U -- U - u u u 20, Diethyl Phthalate 3.93 10.000 --- u --- u--- u u --- - V 31, 2,4-Dini,trotcluane 3.95 10.000 --- V --- u --- u --- U --" u 22. 2.6-Vinitrotoluend 3.88 10.000 u -- u 23. Di-N-Cctyl Phthalate 2.B1 10,000 --- u --- u --- U """ U --- V 24. eis-(2_Hthy1hexy1) Phthalate 9.97 15.000 --- u --- u --" V "'- v --- 25. F1U4rantha0e 3192 10.0D0 --" U --' u --- u ___ u --- u 26. Fluorine 2.95 10.000 --- V --- u --- V -"- V -"- u 27. Hexa0h1orobenLehe 2.61 L0.000 --- V - V -"- V ___ a --- u u 20, xexauh10X00yc10pentadiene 4.26 10,000 --- u --- V --- u - ^ u 29. lnden0[1,2,3-CdlPyrans 2.91 10.000 --- u --- u -`- u '-' U --' U 30. lsophorone 3.74 10.00D --- u --- U --- u V --- D 31. Nitrobenzene 2,05 10.000 --- u --- u 32. N-Nitro a4dlmathylamine 4.25 10,000 --- u --- u --- V --- V --- u 13. N-NitrOPadiphenylamine 3,95 10.0D0 --- V --- V --- u - V j- V 34. N-Nitrua001-N-Propylamine 4.06 10.000 --- U ___ u _._ V ___ V - - u 35. Phenahthrens 3.24 10.000 -"- V u --" V "-- a --- u 36. Pyrene 3.63 10.000 -"- u .-- U --- V --- V --- V 37. 4-Chloro-3-NathykPhencl 3.74 20.000 --- U --- u --- u ___ u ... V 38. 2-ChlorophOnOl 2.75 10,000 --- V --- u --- u --- U - u 39. 0-Creap1 3,68 10.000 --- u -- u --- u --- u u 40. P-Cresol 4.12 10,000 --- u --- V --- U --- V 41. 2,4-D10hloropheh0l 5,19 10.000 --- V - " V '-" u 42. 2,6-DichlOrOphanal 4.99 10,000 --" V ___ u ___ V ___ u 43, 2,4-Dimethylphenol 3A 1 10.000 --- U --- V --- V u --- u 44. 4,6-Pinitro-7-Methy1ph6no1 4.77 50.000 --- a -.. u --- u "-" u --- u 45, 2,4-Dinitrcpheno1 4.37 50.000 --- u u --- u " " V V 46, Rthyl Methane60lfonat■ 5,26 20.000 __- u -` tl ___ U -- V u 47. Methyl MOthaneeulLOhata 9.92 10.000 --- U --- V --- u V V iT . Setilnetsd 4a1V,e hetween the MDL and MxL, U . BeloW 4LL 0uahtiteti0n Limits. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA h(_i69100 ff pub" Nd wastewater IDf 10 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE- N.C. 27858 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 D MR. JUDSON WHITEHURST B02 RECYCLING LANE ANALYST, HIC UREENVILLE, NC 27834 DATE COLLECTED: 12/16/21 Page: 2 DATE EXTRACTED. 12/20/21 DATE REPORTED: 07/18/22 REVIEWED HY; SEMI -•VOLATILE ORGANICS EPA METHOD 8270E 126(18) Deta Analysed 01/20122 01/20/22 01/21/22 02/20/22 O1/20/22 NW-15 mw-16 Nw-17 NW-140 KW-14D PARAMETERS, ug/l N0L NRL 42. 2-Nitrophenol 3.64 101000 ••- U --- A --- u --- V .=- U 49, 4-Nitrophenol 3.17 50.000 --- a --' V --` U """ U • ll 50, Pantachlorophanol 5.33 25.D00 --- U --- u --- u --- V -'- V 51, Phenol 1.86 10.000 --- u -'- V - " U --- V •"" u 52, 2,3,4,6-Tetrach3.Orophena1 3,12 1D.000 --- u ... u -,- u -"^ u 53. 2,4,5-Txjchlo3ro1;heno1 4.17 1D.000 --- V --- u - - u - V --- V 54, 2,4,6-Trich3-orophen01 3.84 10,000 --- u --- u ... U ___ u _ u 55. AaetophenunO 2.09 10.00D --- u --- u 56, 2-Acetylaminoflucrano 3.98 90.000 --- V LL-- U --- u --- V --- u 57. 4-Aminobiphenyl 4.12 20.000 --- U ••. 0 --- a --- U ... u 5a. 9anzyl Alcohol 4.47 29.000 --- u --- u --- u SA. 4-Chloroaniline 3.36 20.000 --- V - " u - u 64. chlorobenzilate 5.12 10.000 --- V •-- u --- u --- u --- u 61. Dlallmte 2.98 1D.000 --- u u -- u _-- V __ u 62, Dibonz0fUrAn 4.28 10.000 --- :1 --- U ... U --- Ti --- u 63. 3,31-1)ichlorobenaidine 4.22 20.000 --- A --- u --- u V --- U 64, Dimethoeta 3.98 20,000 --- V --• u ... U --- u _._ u 65. P-Dimethylaminoaxc ben%ene 2.89 10.0D0 --- a --- u --- u 66, 7012-Dimathy1benz[alnnthraoana 5.26 10,000 --^ U - u ••. u --- u _"' u 67. 3,]-Dimethylbenzidine 3.21 10.000 --- u --- u --- a -'" V -•- u 60. 1,3-Dinitrobanzena 2.09 20.000 --- u u •• U --- u --- U 69. Diphenylmmina 5.10 10.000 --- u u 70, Diauli0t0E 4.20 10.000 --- u --- V ... u ___ u - u 72. Famphur 3.98 20.000 ... V --- u --- u --- Ti - u 72, Nexachloroprapane 4.31 10.000 --- u --- V ••- u --- U -- ❑ u 73. Iao&alrole 2.80 10.000 --• u --_ ❑ -•- 0 ___ u - - 74, R4pone 2.70 20.00D --- ❑ --- ❑ --- u --- u --- u 75, Nethapyrilene 3.54 100.000 --- U --- V --- u --' u --- u 76. 3-Methyleholanthrone 4,21 10.000 --- V --- V '-' V --- u - u 11, 2-1dethy2naphthalane 3.79 10.000 --- it --- u --- V --- V --- V 10. Nethyl Para,thi0tl 4.32 10.000 --• U --- a '-- u ••- u __ V 79. m-Cresol 3.81 10.000 --- u -'" It --- V " u - u BO. 1,4-N&phthoquinOne 4.00 10.000 --- u -- u --- u --- u 81. 1-Naphthylamin9 5.61 10.000 --- u --- T1 --- V 82. 2-Nephthylamins 4.63 10.000 --- t1 " • u "-- U "-- u =_- u 93. 2-NitromniIine 3.61 50.000 •-- U --- V U --- U - u 04. 3-Nitroanilins 4.01 50.000 -- V --• U 05, 4-Nitrcanillna 4.22 20.000 --- u --- U --- V --- V --- u 96. 5-Llitxa V-7Pluidifla 4.01 10.000 --- u --- u --- V --- u - V 87. N-Nltraa0di-S-bUtylamine 3,63 10,000 --- u --- u --- V ••- u --' u 89. 14-Nitroeodiethylomine 3.63 20.000 •-- V --- u --- u ••- Ti - u 89. N-Nitroeomsthylethylamina 3.03 10,000 --- u --- V --- Ti """ U - u 90. N-NitroaopiparidiM1O 5.19 20.000 ... V --- u --- 0 •" U u 91. N-Nitro&Opyrrolidine 2.09 20,000 --- u --- V --- U .-- u .•- u 92. Parathion 3,12 20.000 --- V --- U --- 0 - V u 93. Pentachlorobenzene 3,92 10.000 --- U - u __- u """ u ••- U 94. Pentachlorgnitrobeneane 3,71 20.000 --- V --- u --- u --- V --- V .Y - E&tl,mated value between the NDL and HRL, u - Balow ALL quantitation Limit&, DocuSign Envelope ID: lE49C9C5-lEA4-40EE-BA46-8A724DF270DA Drinking Water M 37715 Wastewater ID, 10 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE. N.C. 27858 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 A MR. JUDSON WHITEHURST 602 RECYCLING LANE ANALYST: HIC GREENVILLE, NC 27834 DATE COLLECTED: 12/16/21 Page: 3 DATE EXTRACTED: 12/20/21 REVIEWED BY: DATE REPORTED: 07/18/22 SEMI -VOLATILE ORGANICS EPA METHOD 8270E R6(18) Data Analyses 01/20/22 1 01/20/22 01/21/22 01/2D/22 01/90/22 MW-15 mw-16 NW-17 MW-14D NW-14D PARAMETER'S, U9/1 DML MRI. 98. Phenaeetin 4.41 2D.000 --- u ... u --- U --- v --� 96. 1,4-gari5enediemin9 2.99 10.000 --- u --- U --- u ___ u U 97. Phorate 3.06 1D.004 --- u -•- u '"- u --- V '-' u 98. Prvnamide 3.69 10,000 --- u '-' U 99. Salrole 4.12 30.040 --- u -•• u --- u _-_ V ."" V 100. 1,2,4,5-T*tr44h10rObeBaan6 5.01 30.044 u 101. Thionazin 4,62 20.DD0 --- V -•• V --- u --- V --- u 102, 0-Toluidine 4.11 10.000 --- u --- V — u -- U - u 103. 1,3,5-TxinitrebwnZ*ne 3,0$ 10.000 --- u ••. V --- Ti --- u --- u U 104. 0,0,0-Triathyl Aho*phorothio4ts 3.61 10.000 --- u --- V --- u U --- 1o9, Haxanhloroethane 1.49 10,000 -- V --• V '-' V --- V U 106. lsodxin 3.11 20.000 --- u J - EatiMated value but-een the MDL and MEL, U . Below ALL Quantitation Limita. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA Drinking Water IDI 37715 Wmatewater IDi 10 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 2785E FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID; 6003 D MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST; JAP 6REE'NVILLE, NC 27834 DATE COLLECTED! 12/16/21 Page: 1 DATE ANALYZED: 12/21/21 REVIEWED BY: DATE REPORTED; 07f1$/22 LANDFILL APPENDIX 11 EPA METHOD 8260D R4 (18) MW-15 Mw-16 Nw-17 rmW-145 Mw-14u VARAMETERB, v9/1 mDL MRL 1. Chloromethans 0.77 3.00D --- U --- U --- u --` 2.05 U "-" U 2. Vinyl Chloride D.12 0.200 - ^ U 0.15 a •-• U U 3. bromomethans 0.67 10.060 --- V --- U --- u --- U --- u 4. Chlcroetha6* 0.49 1O.D00 --- V --» U --- V --- U --- - U 5. Trichlowofluarmmethane 0,24 1.000 --- U --- V --- U - U 6. 1,1-Diohlor0*th*ne 0.17 5.000 -•. V --- U --- V _.. U U 9.06 lO0.O00 •^- V --- U --- U 22.00 J-- 7. Acetone U --- V - U --- V e. iodomathans 0,26 10.000 --- v V 9. Carbon Disulfide 0.23 100.000 --- v --- U - D --- V --- U 10, Methylena Chloride 0.64 1.000 -,- U --- 17 --- V --- U --- 11, trans-1,2-Dichlor%thens 0.23 5,00E --- U --- V --- U - U - U U 12. 1,1-Dichlorostheme 0.20 5.000 ••• V --- U --- U - U - 13. Vinyl Aaetata 0.20 50,000 --- U --- U U U U 14. Cia-1,2-Diahloroathen* 0,26 5.000 --- V 0.64 J --- U -_- u -- ❑ 15. 2-Buranone 2.21 200.000 --- U --- U __. V - V V 16. Dramcehlaramethans 0.27 3.000 --- U '-- V " " V """ U V -- ••• U 17, Chloroform 0.25 5.000 --- V " ' U --- U -�- 16, 1,1,1-Txiohloroathane 0.29 1,000 --- V --- U 19. CaYbon Tetrachloride 0.04 0.200 --- U -`" V U 20. Benzene 0.24 1.000 --- U 0.47 J --` U 3,63 ::- U 21. 1,2•Pich2ora*thane 0.02 D.200 --- U 0.13 J --- U 0,14 4 ` II 22. Triahlarcathene 0.23 1.000 _.- U ... U --- U --- V --- V 23. 1,2-iniahlorapropane 0.04 0.200 --- U 0.06 J ... V 0105 J =_` U 24, sromodichlcromathans 0.04 0.200 -- V --- U --- V - U - U 25. Cis-1,3-1)1chlorcp;open6 0.09 0,200 --- V --- V - - U --- U O - U 26. 4-Kethyl-2-Pantmnons 2.19 100,000 --- V -" V --- Ti U V 27. ToluaYie 0.23 1.004 --- U --- V --- V U _` - --- V --- U 2B. tran*-1.3-Dichloropropene 0.04 0.200 --- V--- V --- V 29. 1,1,2-Triahloroethan* 0.03 0.200 --• U --- U --- U --- V __ - U 30. TstrachlpraethaTla 0.10 0.200 --- U --- U --- V --- U U --- --- u 31. 2-8exanon a 1,57 50.DOO ... u - _ u --- u V '- --" U V 32. Dibromaahloromsthans 0.03 01200 --- V -- U -" 33. 1,2-DihroAOOthans 0.03 0.200 --- V --' 34. Chlorobenzsn4 0.3c 3,000 -- V - --hloraethane V 35. 1,1,1,2-T*traa 0.12 1.000 --- U --- V --- U --- u 36. ethylbenaana 0.21 1.000 .__ U 0.30 IT--- U 0.62 IT U 37. Xylenes 0.69 5.000 --- D --- U --- U - --• U U U 39. Dibromomethane 0.20 10.000 --- V --- V --- V U -Y- V 39. Styrene 0.19 1.D00 -,- V --- V -_- `-- V V --- --- U V 40, bramozorm 0.20 31000 --- V U U .__ U 41. 1,1,2,2-T*traahlaroethane 0.03 0.200 --- U --- V --- U --- V 42, 1,2,3-Tr1ch10r0Pr4P4&n■ 0.09 0.200 --- U -- U - _ U `- V U =- - U 43. 1,4-Dich2arobenzens 0,39 1.000 -- U V --- U - --- V V 44, 1.2-DichlorabenZone 0.32 S.ODD --- U --- V •. U V =_' U 45. 1,2-1)ibram0-3-Ch1aropropane 0.07 0.200 --- V --` U _"- U __- V 46. Aarylonitrile 2.72 200.000 --- V... V ��- V--- U --� 47. trans-1,4-D1chloro-2-Butan0 0.42 10O.DOc --- U --- D `-- U --- V --- - V 40, Acrolsin 1.97 4,000 --- U .__ U J estimated value hetween the MDL and mRL, U ■ Selaw ALL Wantit&ti4n Limits. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA ENATUMMM % ho-UATPO wmud 114 OAKMONT DRIVE GREENVILLE, N.C_ 2785 CLIENT; C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 9EVIEWED BY! LANDFILL APPENDIX II EPA METHOD 8260D R4(18) - MW 1 PARAMTSRS, ug/I NDL MRL 49. Allyl Chloride 0,20 10.000 ... V 50. Chloroprena 0.21 MOOD --- V 51. 1,3-Dichlarobanren1 0.11 5.000 --- u 52, DiohlORodifluoromethane 0.51 5.000 --- u 53. 1,3-Aichloroprppan■ 0.28 1.000 --- u 54, 2,2-DiohlaroPrbpane 0.17 15.000 - V $5. 1,1-DichlorOprOPena 0.22 5.000 --- V 56. Bthyl Hethecrylate 0.16 10.000 --- u $7, Hexaohlorobutadiene 0.10 0.200 --- u 58. Iaobutyl A140ho1 12.80 100.D00 --- V 59, 1lethaorylonitrlls 1.91 100.000 --- u 60. Methyl Nethaorylete 0,25 30.000 --- V 61, Naphthalene u.47 6.000 --- U 62. Propionitrile 3,26 150,000 --- u 63. 1,2,4-Trichlorobenmene 0.50 10.000 --- V 64, hcetonitrils 96.29 55,000 -- u 65, Tetrahydrofuran Q.34 1,000 --- V 66, 1,4-Dioxana 1.71 3.000 4,47 Drinking Water ID3 37115 Wastewater lul 10 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ZDt 6003 D ANALYSTt JAP DATE COLLECTED: 12/16/21 Page; 2 DATE AWALYZEDt 12/21/21 DATE REPORTED: 07/18/22 MiV-16 KW-1 Kw -Its mTd-14D --- t1 -_- a --- U ... u u--- a --- U ... V `-- u .-- V --- D --- u --• a --- u .-- u ... V - u --- it - - u _ V - - u - a ... u ... V --- a --- V '"" V U .-_ u --- 11 ... V --- u - u --- u --- D --- V --- V - - u --- u ... V --- u -- u --- u .-- u --' u 0.78 J --- u --- u .._ a --- u --- u --- 9 -•- tT --- V --- V •-- U -'- u --- V `-- u 3.09 --- u 70.70 --- u 61.40 — u 41.99 -"- U J - 8atimaaad velua botWaen the MDL and HRL, V - B610W ALL Quentitation Limits. NOTE: EPA METHOD 8260D R4 (19): MW-l4S received at pH >2. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA I NWJNRMFN `�l� hk-fQ9*q0'owb�-kro-d 114 OAKMONT DHIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY; � LANDrILL APPENDIX II EPA METHOD 6260D R4(18) Vf dike n9 Oatdr 191 3774 Wastswater Ips 16 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 D ANALYST: JAP DATE COLLECTED: 12/16/21 Page: 3 DINE ANALYZED: 12/21/21 DATE REPORTED: 07/18/22 PARAMETERS, U9/1 y7DL MRL Txip Blank 1. Chloromethnns 0.77 3.000 --- U 2. vinyl Chloride 0.22 0.200 --- U 3. Sromomethane 0.61 10.000 --- V 4, Chloroethane 0.48 10.000 --- U S. Trich Iorvfluaromtthen0 0.24 1,000 --- U 6. 1,1-Diehloro*thena 0.11 5.000 -- U 7. AoatOne 9.06 100,000 --- U 8. Iodomethmn0 0.26 10.000 --- U 9. Carbon Disulfide 0.23 100.000 --- U 10. Methylene Chloride 0.64 1.000 ••• U 11. trans-1,2-Dichloroethene 0.23 5.000 --- U 12. 1,1-Dichloroethane- 0.20 5.000 --- U 19. vinyl Acetate 0.20 50,000 - U 14. Cis-1,2-Diohlvx*sthens 0.25 5.000 --- U 15, 2-Butanone 2.21 100.000 -- V 16. Sromochloromsthane 0.27 3.000 --- U 17. Chloroform 0.25 5.000 --- U 18. 1,1,1-Txichloroeth4ne 0.19 1.000 --- 0 19. Carbon Tetrachloride 0.04 0.200 --- U 20. Benaen■ 0.24 2.000 ^-- U 21. 1,2-Diehloroethans 0.02 0.200 --- U 22, Trichlorcethene 0.23 1.000 ••. U 23. 1,2-Diehloropropan■ 0.04 0,200 U 24. Sromadichloromethane 0.04 0.200 --• U 25, Cia-1,3-Dichloropropens 0,06 9.200 --- V 26. 4-Methyl-2-Pentsn0ne 1.19 100.000 --- U 27. TGIUGM49 0.23 1.000 -- V 28. trans-1,3-Dichlor0propens 4.04 0.200 •-- U 20, 1,1,2-Trichloroethane 0.03 0.200 --- V 30. Tetrochloroethene 0.10 0.200 --• U 31. 2-H9x1kriChe 1.57 50.000 --- V 32. Dibromochloromethane 0.03 0.200 •-- U 33. 1,2-Dibrom0ethane 0.03 0,200 --- V 34. Chlorobenzene 0.30 3.000 •-• U 35, 1,2,1,2-Tetraohlorasthene 0.22 11000 -^- U 36. 8thylhenxana 0.21 1.000 ••• V 31, Xylene9 0.60 5.000 -- V 36, Dibromomethane 0.26 10.000 -•• U 39, etyrans 0.19 1.000 -- U 40. 6roMoform 0.20 3.000 -•• U 41, 1,1,2,2-Tstr4Lchloroethane 0.03 0.200 --• U 42. 1,2,3-Trlchlorogropane 0.09 0.200 -•- U 43. 1,4-Diehlorobenaans 0.39 1.000 •-- V 44. 1,2•Pichlorobenseno 0.32 5.000 --• U 45, 1,2-DibraMe-3-Chloropropane 0.07 0,200 --- U 46, Acrylonitrils 2.72 200.300 ••. V 47. trans-1,4-Diohloro-2-BUtene 0.42 100.000 U 40. Acrolein 1.91 4.000 -•- U J . gstimated value between the MDL and NPL, V • Below ALL pUantitatian Limits- DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA 4ma-runuo ai, hd 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, INC. MR_ SUDSON WHiITEHURST 802 RECYCLING LANE GREENVILLE, NC 27634 REVIEWED BY: �' Drinking Water M 37715 Wastewater ID, 10 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 D ANALYST: JAP DATE COLLECTED: 12/16/21 Page: 4 DATE ANALYZED: 12/21/21 DATE REPORTED: 07/18/22 LANDFILL APPENDIX II EPA METHOD 8260D R4(18) Trig pARANOTSR9, ug/1 MDL MRL Blank 49. Allyl Chloride 0,20 �0,000 --- U 50. Chloroprene 0.21 20.000 --- V $1. 1,3-giahlorobantene 0.41 5,000 --- V 52, Diohlorodigluoromethane 0.51 5.000 --- V 63, 1,3-DiahAaropropane 0.26 1.000 54, 2,2-D1ahlor0pr0p5ne 0.17 19.000 --- U 55. 1,1-Didhloropropen• 0.22 5.000 -- U 56. Sthyl Nothadrylate 0.16 101000 " - V 57. Hexachlorobutadiene 0.10 0.200 - - U 59. YsobUtyl Alcohol 12.90 100,000 --- V 59, W4thaorylOSitrile 1.93 100.009 --- U 60, ldethyl NOthacrylat• 0.2S 30.000 --- U 61. Naphthalene 0.47 6.000 --- U 62. @ropionitrils 3.26 150.000 --- U 63. 1,2,4-Trich1or0ba6aene 0.50 10,000 --- U 64. Aaetonittil• 36.29 5S.000 ^-- U 65. Tetrahydr0loran 0,39 1.000 -- V 66. 1,4-Dioxan6 2.71 3.000 •-- V S - 8atinated value between the HDL and KRL, U + Below ALL Quaneitation Limits. DocuSign Envelope ID: lE49C9C5-lEA4-40EE-BA46-8A724DF270DA cn w III z CID ik C'S(La V A Q v r" b L� Z5 ?5 5 � IJ � � b m w ,f "l m TOTAL CHLORINE. mg/l k7 L m OR ug/I AT COLLECTION TEMPERATURE, °C � -1 N ATOMECTION O In cn cr #0FCONTAINERS O o c o c 10 US "I„#,a Field pH � ro Nitrate+Nitrite Y Alkalinity > >I>; IBM Chloride `d Cyanide tv ;:: .:'::: r•h €# i Sulfate > "o l . Metals Sulficle Conductivity Y i € DO "d l Temperature ti Field Parameter 8260 Dup. 2 t�1 G5 ' EPA 8270E G] <� 8274E Dup. 1 > 4] cn n PARAMETERS/TESTS am S CD L L z a m ca LI) o Q y g n M a rn r�r � © tn � { En rn tn 2 ri'i Q 1 zi cmrf N fiS p � m Q C i JmC7 n 0 � d -t b 6q tQ DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA cn' 0 0 m m S� CP OL Cb m g 3 � CpCD n Cr n � 0 m 0 m 0 v s, a W w � m ¢ j@q C ¢ [a Ch N a z CD K) 1�+ Lj 7e1r1 r�> 4 �. l►, cnFn v C all' F 71 w � U C7 p • • Lh m m A TOTAL CHLORINE, mg/1 O OR ugll AT COLLECTION m TEMPERATURE,°C r AnoLLECTION M p t" Q) &' N OF CONTAINERS a, Q ?° EPA 80811# No 8081B Duplicate „L 8260D App. 11 kn 45 8260D App. 1t 2 Gi 8260D App. II 3 G� m m 8260D App. 114 m 8151A Landfill C7 8151A Duplicate c1; cn n PARAMETERSJESTS z = Y �--� ro"' �0 j� m m cr z mo �s�n o o VE �n c �� r _� 1 n o r Q C� 4 f� t� -:b m r�o C7 p tp � � r�r f'7 L" F. C n D d �7 r w 11, DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA kuqoara.Ad 114 OAKMONT DRIVE GREENVILLE. N.C. 27858 C & D DISPOSAL, INC. Ids. JUDSON WHITEHURST 802 RECYCLING LAME GREENVILLE, xc 27834 pARAIJB7BR6 NDL pg (field mebeurement), Units Nitrate+Nitrite as N, mg/1 0.04 Alkalinity (tO pH 4.5), mg CaCO3/1 1.0 Chloride, M911 1.0 Cyanide, uy/1 5.0 Total Dissolved Residue, Rig/1 10 Sulfate, mg/1 5.0 Antimony, 119/1 0.03 Antimony, ug/1 0.03 Arsenic, ug/1 0.09 Arsenic, ug/1 0•a6 Barium, us/1 0.04 Barium, ug/1 0.04 Barium, ug/1 0•D4 Beryllium, u9/1 0102 Beryllium, mg/1 0.02 cadmium, ug/1 0.04 Cadmium, u9/1 0.04 Cobalt, U9/1 0.02 cahalt, ug/l 0,02 Total chromium, ug/1 0.12 Total Chromium, u9/1 0.12 COPPerr u9/1 0.04 Copper, U+ /1 0.04 Tran, ug/l 4.96 Iron, ug/1 4.96 Manganese, ug/1 0.31 Nangeneaa, ug/1 0.32 Lead, wall 0.01 [jead, k%V, 0.03 Mercury, ug/1 0.05 Nickel, ug/1 0.03 Nickel, U9/1 0.01 selenium, ug/1 0.05 selenium, ug/1 0.05 silver, ug/1 0.22 Silver, U9/1 0.22 Thallium, ug/l 0.02 Thallium, 99/l 0,02 Tin, V$/1 0•05 Vanadium, Ug/1 0.04 Vanadium, ug/1 0,04 Ivii-nkitia "Ot*x %6.1 wl* Wastowater ;D, 10 PHONE (252) 756-6208 FAX (252) 756-0633 xD#: 6003 8 DATE COLLECTED: 12/15/21 DATE REPORTED : 07/18/22 l REVIEWED BY: NW -RA NW-10 MW-11 MW-13 MW-12 MRL 0.04 1.0 1.0 5•D 10 5.0 1.0 l,D 5.0 5.0 10.0 10.0 10.D 1.D 1.0 1.0 1.0 1.0 1.0 5.0 5.0 10.0 10.0 50.0 50.0 10.0 10.0 5.0 5.0 0.20 10.0 10.0 10.0 10.0 s.0 5.0 1.0 1.0 140.D 1.0 1.0 6.7 s.7 7,1 6.4 .._ U ... U -.. U ... U 170 51 520 594 27 73 Be S9 --- V •'- U --- U --- U 620 1700 *40 9b0 306 S83 269 371 0,04 7 0.06 J 0.15 1 0.09 a 4. 54 a 4.6 J 4.9 J 10 141 307 171 0.02 S --- U 0.15 IT O. 99 J 0.08 J 9213 479 u u 0.32 0 0.21 J --- u --- u -- U x 0,04 J --- U 1.3 15 D,18 a 142 172 0.04 J 1,1d 1.2 J -- tr -- U ..- U 7 65.5 O,O5J - U 0.64 J 0.11 J 19251 273 0.051 --- 11 0.91 J 0.60 J --- u - U 0.95 a All QC requirementa were not mete d Duplicate data not within eatabliahed limita- 0.04 1 --- U 1.4 a,9J 0,a2J 27923 190 0.194 --- U 2.8,7 2.0 J --- U 0.09 J --- U 4 s Analysis Method Date Analyst Cade b.6 22/15/21 PJC 450ORS-11 --- U 12/20/21 RES 353.2 R2-93 1550 12/20/21 DIJ 2]24B-11 254 12/20/21 LAW 4500CLB-11 --- U 12/26/11 mmm 45DOCNN-13 2100 12/16/21 JME D5907-13 21.6 12/23/21 LF,7 4500SO42811 12/17/21 NAS EPA200.B 0.29 J 02/05/22 NAB EPA200.8 12/17/22 NAB EPA200.8 57 O1/05/22 NAB BPA200.8 12/20/21 NAB MPA200.8 01/05/R$ NAB BPA200.9 S72 12/22121 NAB RPA200.9 12/21/21 NAB B11A200.0 0.C4 J 12/22/21 NAB UPA200.6 12/17/22 NAB SPA200.0 --- v 02/05/22 NAB BPA700,8 12/17/21 NAB EkA20D.0 4,1 12/22/21 NAB aPA200.9 12/17/21 NAB IRPIL200.6 61 12/22/21 NAB BPA204.9 12/17/21 NAB gPA200.6 0.14 J 12/22121 NAS EPA200.6 02/07/22 LF,T EPA200.7 1473 12/20/21 LFJ BPA200.7 01/07122 LF,7 SPA200.7 415 11/20/21 LFJ RPA200.7 12/17/21 NAB BPA200.8 D•06 S 12/22/21 HAD @,PA200.0 -_- U 12/22/21 HTM 245.1 R3-94 12/17/21 HAD RPA200.9 4,$ J 12/22/21 NAB SPA299A 12/17/21 NAB RPA200.0 2.8,7 12/22/21 NAB 3PA200,0 12/17/21 NAB EPA200.8 -- 1J 12/22/21 NAB SPA20D.8 17/17/21 NAB RPA200.8 •-• V 1212212L NAB SPA200.9 --- U 01/0$/22 NAB EPA200.8 12/17/21 NAB SPA200.6 49 12/22/21 NAB EPA200,9 J . Satimated value between the MDL and NBL, U = Below ALL 0uantitatien Limits. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA or�a�� 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 C & D DISPOSAL, INC. MR. O-UDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 PAxAMETPaS zing, ug/l Zino, ug/1 Sulfide, ug/l Conductivity fat 250), uMhce/cm Dissolved Oxygen, mg/1 Temperature, 'C static Water Level, feet Well Depth, East ORP, my Turbidity (Field), NTV MW-PA KDL MRL 0.17 10.0 0.17 10.0 100 1001) --- u 1.0 1.0 1024 0.1 0,1 0.51 17 6.90 23.17 +123 1,0 1.0 8.03 brinking Water XD, 37715 Wastewater YD, 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 6003 s DATE COLLECTED: 12/15/21 DATE REPORTED : 07/18/22 REVIEWED BY: NW-10 MW-11 Hw-13 Mw-12a Analyaie Method Date Analyst Cade 12/17/21 NAB $PA200.9 5.2 J 1.24 14 2.21 12/22/21 NAB 3PA200,8 18B J --- U --- V 20§ a 12/21/21 LFJ 4$0082D-11 2497 1020 1472 4077 12/15/21 PJC 251O9-11 1,12 0.31 0.03 0.0 12/15/21 PJC 450006-16 15 17 17 16 12/15/22 P1C 255OD-10 4.41 3.74 10.27 5.56 12/15/21 PJC 22.73 23.04 20.60 22,91 12/15/21 PJc +146 +129 +122 +167 12/15/21 PJC 25BOD-11 5.19 46.10 8.67 3.15 12/25/21 PJC 21308-ll All 4C requiremento were not not, d DUpli4ata data not within setablinhed limits- 1 . Sakimated value between the KDL and MRL, V - Selbw ALL ouantitatiOn Limits. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA % hcmpo (OT ti' Nd 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, I14C. MR. JUDSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY; FARAMMTHR6, Ug/l 1. Aldrin 2. Alpha-BHC 3. Beta-EHC 4, Delta-BHC S. Gamma-BHC (Lindane) 6. Chlordane 7. 4,4-DDD 0. 4,4-DDE 9, 4r4-DDT 10, aieldrin 11. 8adaaulfan l 12, Endoeullan II 13. &nddaulfan Sulfate 14. Endrin 1S. 6ndein Aldehyde 16. Heptachlor 17, Heptachlor Epoxide 18, M4GhoxychLor 19. pdb-s (aroclors) 20. Toxaphane nrinking water It 37715 Wastewdt4Y IDs 10 PHONE (252') 156-6208 FAX (252) 756-0633 CLIENT ID; 6003 8 ANALYST: ETC DATE COLLECTED; 12/15/21 DATE EXTRACTED: 12/21/21 DATE ANALYZED: 12/21/21 DATE REPORTED: 07/18/22 PESTICIXIES EPA MXTHOD ANT) PCB' 8081B R2(07) S MW-')A MW-10 MW-]1 l6W-13 Dsm-12a HVL ARL U --' U ___ U -.. t7 4.432 0,090 --- U --- U --- U --- U ... U 0.031 0.050 ^- V --- U --- U ___ U 0,030 O.05o --- U --- u --- n --- a --- u 0.032 0,050 --- V -_- V --- U --- U -__ U 0,320 0.500 --- V -- U -- u --- v -- V 0.051 0.100 ••• Ti --' U ___ U ___ V ___ U D.00 0.100 --- V '.- U •-- V --- U 0,052 0.100 --- U -- u - u --- u --- U 0.048 0.075 --- V --- U ••- V-_ V --- U 0.056 0.100 _.. U ___ U --- U --- U __ U 0.046 0.100 --- U '-- V --- V --- U --- U 0.012 0.100 U --- U --- U __. V 0.059 0.100 __- U --- U --- V -Y- U --- U 0.069 0.100 - o --- U --- v --- v -- U 0.039 0.050 -.. V _-- U --- U --- U --- U 0.042 0.075 V __ U -- U 0.530 1.000 --- U -'" V ... U U --- U 0.500 2.000 --- U --- U --- U --- U _ " V 01690 1.500 --- v --- 0 --- U --- 73 --- v J ■ Eatimated valve between the MDL and MRL, ❑ - Below ALL Ouartititatiori Limits. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA ERW'ff(fflFffl0 `dQ kmvup"A(d 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D nISPOSAL, INC. MR. "DSON WHITEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: LANDFILL APPENDIX 11 EPA METHOD 8151A R1(96) DrinRinB water IDS 37715 Waotawater Ivi 10 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 6003 8 ANALYST: xre DATE COLLECTED: 12/15/21 DATE EXTRACTED: 12/22/21 DATE ANALYZED: 12/24/21 DATE REPORTED: 07/18/22 mw-3A yew-10 mW-11 mw-13 mw-12e rARAHRTERS, U911 MDL MRL 1. 2,4-D 0.3d 2.000 --- u --- V --� u 2. Dinooeb 0.54 2.000 --- V --- V •" u V V 3. 2,4,5-TP 4.42 2.000 --- u --- U --- u --- u --- V 4. 2,4,5-T 0.47 2.000 ..- V --- V ... a _._ V ... U J . Estimated vdIUe between the NDL and maL, V . E014w ALL Qvantitation Limits. DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA � % INATPOFMINW01 ENWuL'T@mm(M k-19 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: C & D DISPOSAL, TNC. MR. JUDSON WHITEHURST 802 RECYCLING LANE CREENVILLE, NC 27834 REVIEWED BY: � Drinking Water Ibi 37715 WanteWater ID, 10 PHONE (252) 756.6208 FAX (252) 756.0633 CLIENT ID: 6003 B ANALYST: Hic DATE COLLECTED. 12/15/21 DATE EXTRACTED: 12/20/21 DATE ANALYZED: 01120/22 DATE REPORTED: 07/18/22 SEMI -VOLATILE ORGANICS EPA METHOD 8270E R6(18) Page: 1 N�a-sn Mw to ]sw-11 HW-13 NW-12a PARANETERB, u9/1 HPL HRL 1. Acenaphthene 2.66 10,0D0 u - v --- U - u =-- u a. Acenaphthyl*n• 2,50 10.000 v --- u --- u --- U u 3. AnihraCene 2.97 10,D00 -•• u --- u --- u u -- - u 4. 8anao(a]ant"ACGrIe 4,16 1D.000 --- u --- V -'- u --- V --- u 5. Benao Uiltlporanthena 3.32 10.000 --" U --- u --- u --' u 6. Ransa(k]fluoranthene 4.23 10.000 --- u --- u --- u --- V --- u 7. Sensa[g.h,i]perylsna 2.61 10,000 - " u _._ u _.. u 8, Benzo(a)pyrene 3.27 30.000 --- U --' u --- u .._ u ... u 9. 4-arvmophenyl phenyl Ether 2.53 10.000 U '•• U •-- V --- V 10. Butyl 9enayl Phthalate 5.79 14.D00 --- u --- u -"- V --- u --- - u U 11. Bis(2-chloruethoxy) Hathane 3.14 10.000 u --- V --- V 12, Bie(2-Chlarcethy2l Ether 2.50 10.000 --- u --- V --` u --- V -•- V 13. eis(9-chlDx0-1-methylathyl) $Cher 2.58 10.000 --- V -"' u --- u --- u --- D 14. 2-Chloronaphthalena 2,17 10.000 --- u --- u --` u --- u U 15. 4-Chloraphanyl Phenyl Ither 2.42 10.000 --- u --- u --- u --- u u 16. Chrysens 4.04 10,000 --- U •.. U -"" U u --- 17, Dihanso(a,hianthraaene 2,78 16.0D0 --- U --" U .-- U --- u - --- U u is. D1-N-butyl Phthalats 3.09 10.000 --- u --- V --- V 19, Dimethyl Phthalate 3.79 10.000 --- u --- V --- V -- V --- u 20, Diethyl Phthalate 3.92 10.000 u -'" V --- V --- V ±=- u V 21. 2,4-Dinitrotolusne 3,95 10.000 -�- u --- V --- u --- V - u 22. 2,6-Dinitrotolµans 3.98 10.000 --- u --- u - u --- u --- 23. Di-H-Oatyl Phthalate 2.01 10.000 --- 0 - _ u .. u --- U -- V 24. asa-(2-Hthylhexy1] Phthalata 9.97 15.000 --- u --- u --~ v --- u --- -- ° D 25. Pluoranthene 3.92 10.DDD --- u -`- v --- u --- u u 26. pluorens 2.95 10.000 --- D --- u .-- u __ u --- 27. HexmCh10rohenrana 2.61 10,000 --- u 29, Nexachloraoyclopentadiene 4.16 10.000 --- V --- V --- a .__ u .`. - u V 29. Indmn0[1,2,3-Cdjpyxens 2.91 10.000 --- V `-- V --- u --- U - 30. Zoophorone 3.74 10.000 --- u --- V --` 0 __- p 31. Nitrobenzene 2.05 10.000 --- V -"- u --- u -" u J" D 32. N-Nitraaodimethylamine 4.25 10.000 --- u --- u --• V --- u --- u 33. N-Nitraeodiphenylamine 3.95 10.000 --- u - u --- u --- u -- U 34. N-Nitrosodi-N-Propylamine 4,06 10,000 --- V --- u --- D - D - U 35. Phenanthxene 3,24 1D.0D0 ••- U --- D --- U --- D --- V 36. Pyrons 3.63 10A00 --- u --- u --- u =_ a --- u 37. 4-Chloro-3-14sthylphsnol 3.79 20.000 ••. v _-- u --- u - D u 38. 2-Chlorophenol 2.75 10.000 D --- u -•• u -�- U - --- U 39. 0-cresol 3A0 10.000 ••- u --- U __. u --- u ... u 40. P-Cresol 4.12 10.000 u --- u --- u u -- U 41. 2,4-Dichlerophenol 5.19 10.000 --- u --- V -"' V - u --- i7 42, 2,6-Dichiorophonal 4.65 10,000 --- u 43. 2,4-D1methylphenol 3,21 1D.000 ... V --- u __- u 44, 4,6-Dinitro-2_M6thylphen0l 4.77 50.000 -"- u "-- u --` U 45. 2,4-Dinitrophenol 4.37 50.000 ... u --- u --- D -i- V 46, Butyl Herhanasulfomats 5.26 20.000 -`- u u 47. Hathyl MathaneRulfanate 4.92 10.000 •-- u "" u --- u u 4S, 2-Nitrophanal 3.64 10.000 --- u u -" u `"- V - ,7 . ¢ptimated Value between the MUL and MA L, U - Below ALL Qwantitation Limits. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA P, am. ud Drinking Water FAI 37715 Wastewater M 10 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C, 27858 FAX (252) 756-0633 CLIENT: C & D AZSFOSAL, INC. CLIENT ID: 6003 B MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST. HIC GREENVILLE, NC 27834 DATE COLLECTHDs 12/15/21 Page: 2 DATE EXTRACTED: 12/20/21 DATE ANALYZED: 01/20/22 f DATE REPORTED: 07/18/22 REVIEWED BY: SEMI -VOLATILE ORGANICS EPA METHOD 8270E W18) m-M NW-10 tsW-11 NW-13 mw-120 WARAMBTSR9, ug/l HDL NRL 49, 4-Nitrophsnol 3.17 50.000 --- U --- V --' V --- U ... U 50. Pentaahlarophenal 5.33 25.000 --- In •• U --- U -"- V U 51. Phenol 1.96 10.000 --- V -` 52. 4,6-Metraehlarophenol 1.12 101000 --- V --- S! --- U --- V --- U U 53, 2,4,5-Trichlorcphenol 4.17 10,D00 --- U --- U --- U U -- $4. 2,4,6-Triahloraphenol 3.04 10.000 --- U • V --- U --- U -=- U U 55. A4etophenon• 2.89 10.000 --- U -.-- U --- v --- V - $6. 2-Acetylaminef2uorens 3,$$ 20.000 --- U --- U --- U -- U T- U 57. 4-Aminabiphenyl 4,12 20.00D --- U --- U --- U --- V --- V 59, 9enzyl Alcohol 4.47 MOOD --- U --- U --- U ___ U 59. 4-chicromnilin■ 3.36 20,OD0 --- V -'" U --- V --- U - U U 60. OhlorobanrilatO 5.13 10.000 --- U --- U --' U - V --- $I. Diallato 2.90 10.000 --- U --- u --- U --- V -- --' U V 62. Dibenaofuran 4,28 10.000 --- U --- U --- U --' U U 63. 3,3+-Dichlorobensidine 4,22 20.000 --- U --- U --- U --- U --- 64. almethoate 3.98 30.000 --- U --- U --- U --- U __- U U 65. 4-Dimethylaminoasobennene 2.09 10.000 --- U --- U -^- V --' U --- 66. 7,12-Dimethylben6lalanthraeene 5126 10.OD6 --- V -"" V " " U --- U 67, 3,1-Dimethylbenzidine 3.21 10,000 --- V --- U --- U '-` V 68. 1,3-Dinitrabert6en4 2.09 20,000 --- U --- U --- U -- U - U U 69. PiphmnylAmiD* 5.10 10.000 --- U ___ U •-- V `-- V - 70. Diaulloton 4.28 10.000 --- ❑ V --- U --- V - V U 71. ramphur 3.98 20.000 --- U --- U ^ • V " - V --- 72. Hexaahiaropropane 4.31 10.000 --- u --- if " ' u """ U - V 75, Isooa[r01e 2.88 10.000 --- V --- U 74, Kepone 2,76 20.ODO --- Ti --- U --- U - - U --- V 75, Methapyrilene 3.54 100.000 --- V --- U ... U -_- V - V U. 3-Nethylch4Dlanthre1,a 4.21 10.000 --- V --- U --- U " " V - V 77, 2-Nethylnaphthailene 3.79 10.000 --- V --- V --- U --- U --- U 18, Kethyl Parathion 4.32 10,000 -- V --- V __ U ... V --- U U 79. m-cresol 3.91 10.090 --- U .-- v --- U --- U --- 00. 1,4-NaphthoQuinone 4.00 10.000 --- U --- U •-- U '-' V 01, 1-Naphthylamine 5.61 10.000 --- U --- U -- V 82. a-Naphthylamine 4.62 10•000 - U --' U " ' U ••^ V V U 82. 2-Ni troaniline 3.61 50.000 --- U -- U --- V --- V __- - -'- U 84. 3-Nitraanil41te 4.82 50,000 --- U --- U --- U "-' it U 85. 4-Nitroaniline 4,22 20.000 --- U ❑ --- U --- U --- 86. 5-Nitro-0-TOluidine 4.01 10,000 --- U --- U --- U ••_ tl U $7. N-Nitroaod,i-n-butylamine 3.63 20.000 --- V --^ V -- U --- U --- B8. N-Nitsraa0$1ethYlamine 3.83 8016DO --- U --- U --- V --- U V tl $9, N-l:itraaomethylethylamine 3.63 10.000 --- U -^- U --- V --- U --- 90. N-Nitraaopiparidine 5.29 20.000 --- V '-' U --- U - U - U 91, N-Nitrosopyrrulidine 2.89 10.000 --- U '-- U --- U --- V -- U 92. RarathIAM 3.12 10,000 --- U --- U --- V --" U --- - U V 93. GentachlorobenXens 3.92 ID.000 - U `-- U --- U --- U --- U 94. Pentachlor4nitrobedsene 3.71 20.004 --- U --- U --- U `-- V -'" U 9S. Phenacstin 4,41 20.000 ___ V ..- V _-- U -_- U _- 96. 1,4-ban zoned iamins 2.99 10.000 --- V --- V -`- V --- V J w 6atimatbd value betWeen the NDL and t4R6, U w aelpw ALL Quantitation Limits. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA % 5DICUP(OTHPA 114 OAKMONT DRIVE GREENVILLE. N.C. 2785E CLIENT: C & D DISPOSAL, INC. MR. CUDSON WHTTEHURST 802 RECYCLING LANE GREENVILLE, NC 27834 REVIEWED BY: Drinking Water ID; 31115 waetowatsr IDS 10 PHONE (252) 756-6208 FAX (252) 758-0633 CLIENT ID: 6003 B ANALYST: HIc DATE COLLECTED: 12/15/21 Page: 3 DATE EXTRACTED: 12/20/21 DATE ANALYZED: 01/20/22 DATE REPORTED: 07/18/22 ,OEMI-VOLATILE ORGANICS EPA b9TROD 8270E R6(18) bSW-ar m -1 PARAMSTERS, U9/1 MDL MRL 97. Phorate 1106 20.000 --- V 90, Pronamid• 3.69 10,000 --- U 99. 96expla 4,12 10.000 --- U 100, 1.2.4.5-Tatraahlarodanzone 5.01 10.000 --- U 501, Thionaain 4,62 20.000 --- U 102, 4-Taluldina 4.11 10,p00 --- U 103. 1,3,5-TrinitrcbeRaana 3.98 10.000 --- V 104, 0,04-TriethYl PhosphorothiosLa 3.61 10,000 -- V 105. Hexachlorosthane 1.49 10.000 --- V 106, Iaodrin 3,11 20,000 --- U � a1w-11 Mw-17 MW-1aa U--- U ... U "- U "- U --- U --- V --- tt - U --- U ... V _.- U --- V .... U --- U V.-- U ... U ... U --- U --- U --- U --- U U -" U --- U ... U --- Ti --- V -" tt '_• U ..- U `-- U ._. U .__ U i ■ 8atimated value between the MUL and MRL, U - Below ALL puentitation LimitR, DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA Em'DHAR no,, owvgdo Drinking water ID, 31715 waatewatex ID, 10 114 OAKMONT DRIVE PHONE (252) 756`6208 GREENVILLE. N,C, 27858 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID, 6003 B MR, OTJDSON WHITENURST 802 RECYCLING LANE ANALYST: TAP GREENVILLE, NC 27634 DATE COLLECTED. 12/15/21 Page: 1 DATE ANALYZED: 12/21/21 DATE REPORTED: 07/18/22 REVIEWED BY: _ LANDFILL APPENDIX II EPA METHOD 8260D R4(18) Mw.gA Mw-10 Mw-li :aw-13 now -lee PARAMeT898, ugfl MDL MRL 1. Chloxomethane 0.77 1.000 --- U --- U --- U ••• U 1.74 U 2.09 2. Vinyl Chloride 0,12 0.200 .-- U D.53 --- U 3, aromomethana 0.67 10.0DO --- U --- U --' U - U V 4, ChlarowthOTM 0.48 10.DOD --- V - " U --- U .__ U 5. TriChlprofluoromethane 0.24 1,000 --- U U - U U ... U 6. 1,1-DichlotOathene 0.17 5.000 --- U --- U ... U 7. Acetvn0 9,06 100.000 --" U -•• U ^-^ V --- V 17.90 d S. IOdomethane 0.26 10.000 --- U --- U --" U --- U " - U U 9. Carbon DiNUlfide 0,23 100.000 --- V -•^ U 0.36 J --- U _.. in. Methylene ChlOXide 0.54 1,000 --- U --- U ""- U ••- U 11. trans-1,2-13ichlOrOithene 0.23 5.000 --^ v --- a --- U - U U 12, 1,1-DichloK**tha1'e 0.20 5,000 --- V '^- V --" U --- U --- U 13. Vinyl Acetate 0.20 50.D00 U 2.20 J 0.42 J 14. Cia-1.2-DiChloXoethens 0.25 $,000 --- U -'- U --- 15. 2-ButanOna 2,21 100.000 --- V - " U ""- U --- U V 16. Uromoohloromdthene 0.27 3,004) - - U -- U -- U U --- 17. Chloroform 0.25 5.00D --- U tr --- U 1$, 1,1,1-Triohlvra�kriana 0.19 1.000 --- U --- U --- U --- U 19. Carbon Tetrachloride 0.04 0,200 --- U --^ U --- U --- V --- 2.9fi 0.24 1.000 --- U 2.03 ... U 0.91 J 20. aeneana 21. 1,2-Dichiaroathano 0.02 0,2o0 0.02 d 0.25 0.05 J 0,16 a 0.18 d 22. TCiphloraethene 0.23 1.000 ••• U --- U --" V U U 0,D$ J D.11 c 2;. 1,2-Diohloroprvpane 0,09 0.240 -_- U 0.15 J --- 24. bromodichloromethane 0.04 0.200 "-- U --- V --- U --- U - U - U 25, Cie-1,3-Dichloropropene 0.06 0.200 --- U --- U '.. u --- V 25. 4-Methyl-2-Pantanone 1.19 100.000 --- U --- U '-- U U 0.58 C 21, Toluene 0.23 1.000 --, U - " U -.. U -- "-- U --- U 28. tranD"1,3-Diehlorvpropene 0.04 0.200 --- U --- V --- U 29, 1,1,2-TxiohlorodthAne 0.03 0.200 - U '-- --- U --- U --- V --- U 30. Tatrachlaro*thene 0.10 0.200 U --- U --- U -"- U ... U 31. 2-xexanone 1.57 50.000 --- U --- U --- V -- U U 32. Dibxomochloromethane 0.03 0,200 --- U --- U --- V --" 1J --- 33, 1,2-Dibromoathane 0.03 0.2DO --- U --- U --- U --- U --- U U 34. Chlorobanzene 0.30 3.000 --- U ... U --- U --- U --- U 35. 1,1,1,2-Tetrachloroethane 0.22 1.000 --- V --' U " • U --- U - U "- 0.22 J 36. 6ChyXbenzene 0.22 1.000 --" U ••• U -- U V 1.70 J 37. xylenam 0.68 5.000 V --' U --- U 3D. Dibromomethane 0.29 10,000 --- U --- U =-- U 39. ,9tyrane 0.19 1.000 =_" V U "-- U 40. grbmoform 0.20 3.000 --- U --- U --- U -'" V 41, 1,1,2,2-Tetravhlomaothpae D.03 0.200 --- V --- U -'" U --- V --- U 42. 1,2,3-Trichloropropane 0.03 0.200 a --- U --- U --- a --- V 43. 1,4-Dichlorobonzene 0.39 1.000 --- U --- U --- U --- U - 44, 1,2-Dichloxobenzene 0.32 5.000 - U U U 45. 1,2-Vibrvmo-3-ChloropYOpana 0.07 0.20D --- U --- V --- U "-- U --- ""• U 46, A9rylonitrile 2,72 200.000 " - U --- U --^ U " - V 47. trand-1,4-Dich1oro-2-BUtena 0.42 100,000 --- V --- v --- a --- v -' u U 48, Acrolain i.97 4,000 --- U .. V - U --- U .7 . Retimated value between the MDL and Mkh, U Below ALL QmAntitaCion Limito. DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA �Tm"MNIIAMA `�11 �NCVT 0 Prinking Wat*v ini 37735 Wastewater ID: 10 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 27858 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 H MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: .TAP GREENVILLE, NC 21834 DATE COLLECTED: 12/15/21 VaLge: 2 DATE ANALYZED: 12/21/21 DATE REPORTED: 07/1$/22 REVIEWED BY LANDFILL APPENDIX II ton% mwrrtr^n PiAnn 174f1A1 Mw-4A PARAMRTERS, US/1 MDL MRL 49. Allyl Chloride 0.20 10.000 --- U 5Q, chlaroprone 0.21 20.000 U 51. 1,3-Diohlorobenzene 1.41 5.D00 -- U 52. Diehlorodifluoromethane 0.51 51000 `- U 53. 1,3-Diohlaropropsne 0.20 2.000 --- U 54, 2,2-IIiohloropropane 4.17 15.400 -" U 55. 1,1-Diohloroprapens 0.22 S.ODO """ U 56. Ethyl Methaerylato 0116 10,000 -' U 57, xexachlorobutadiene 0.10 0,200 --- U 59. Imobvty1 Alcohol 12.80 10D.000 -- V 59. Methacry1onitrild 1'B3 1e0.QOD --- U 60, Methyl Mothaerylate 0.25 30.000 --- U 61. Naphthalene 0.47 6.ODO --r T7 62, PropioRitrile 3,26 150.D00 --- U 63. 1,3,4-Tr1chlorobenrana 4,50 10.000 --- U 64. Aoetonitrile 36,29 55.000 --- U 6S• TatrahydrofuraD 0.39 1.000 --- U 66. 1,4-Diaxane 2.71 3.000 - U D3V7-10 MW-11 Nw-13 Mw-12e U U •-- V •-- U ❑ - V U 0.56 'T --- U --- v ___ U -_ U '"- ❑ -__ U --- U ... U --- U ___ U --- U --- U --- U --' U --- U ... U -,- U --- U --- U --- U --- U - V ___ U U --_ y _- U --_ U --- U 5.21 a U --- U' ___ U --- U _.. U .._ U --- U ___ U --- U --_ U __- U ""- V 14.7D 7.43 11.10 39,30 7.16 $.79 9.74 34.90 J - 8otimated value betilean the MDL and MIL, V . Below ALI- Quantitation Limit,. NOTE: EPA METI100 82600 R4 (18), MW-13 rcceivod Bf pH>2. DocuSign Envelope ID: lE49C9C5-lEA4-40EE-BA46-8A724DF270DA �W�JaC� u W `llp il��w-FrWo -bid 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 Drinking Wd ter TD, 17715 WaNtewacer lDI 10 PHONE (252) 756.6208 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC. CLIENT ID: 6003 B DdR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST; JAP GREENVILLE, NC 27834 DATE COLLECTED: 12/15/21 page; 3 DATE ANALYZED: 12/21/21 .� DATE REPORTED: 07/18/22 REVIEWED BY! LANDFILL APPENDIX II EPA METHOD 8260D R4(18) PARAH8rERS, 1.19/1 MDL MRL Trip Blmnk 1. Chloromethan4 0.77 3.000 --- V 2. Vinyl Chloride 0.12 0.200 --- u 3, Bromomethane, 0.67 10.004 --- U 4. Chlarcathane 0.48 10,000 --- V 5. Trichloruf1moromethane 0.24 1.00D ... D 6. 1,1-Dichloraethanm 0.17 5,000 --- D 7. Acetone 9.06 100.400 --- 0 8. lodom•thane 0.26 10,000 --- D 9. Carbon Dibulfide 0.23 100.000 --- u 10, methylene Chloride 0.54 1.000 --- u 21. trans-1,3-Dichlprpethens 0.23 5.000 --- u 12, 1,1-Dichloroethane 0.20 5.000 --^ u 13. Vinyl Acetate 0.20 $0.000 --- V 14, Cie-1,2-Diehloroethen9 0.25 5.000 --- u 15. 2-Butancne 2.21 100.000 --- V 15. Bromochloromathane 0.27 3.000 --- U 17. Chloroform 0.25 5.000 --- U 18. 1,1,1-Trichlaroethano 0.19 1.000 --- D 19. Carbon Tetrachloride 0.04 0.200 --- u 20, Benzene 0.24 1.000 --- u 32, 1,2-Dichlaroathane 0.02 0.200 --- u 22, Trichlorcothene 0.23 2.000 --- u 23, 1,2-DiGhloropropans 0,04 0.200 --- V 24, Bromodichloromethmne 0,04 0.200 --- u 25. Cis,1,3-Dichloroprapene 0,06 0,200 --- u 26, 4-methy2-2-Pentonons 1.19 100.000 --- u 27. Toluene 0.23 1.000 --- u 29, trans-1,3-Dic hloropropeno 0.04 0.300 --- u 29. 1,1,2-Trichloroathaaa 0.03 0.240 --- u 30, Tetrachleroothene 0,10 0.Y00 --- u 32. 2-Hexananm 1.57 50,060 --- u 32. DibramoChlorpmethane 0,03 0.200 --- u 33. 1,2-Pibromosthana 0.03 0,200 --- u 34, Ch1crobent4,n0 0.30 3.000 --- u 35. 1,1,1,2-Tetrachloromthano 0.22 1.000 --- u 36, Sthylbanrei» 0.21 1.000 -- u 37. Xylanes 0.60 5,000 --- 13 30. DibrRmomethane 0,25 10.000 - -- u 39. Styrene 0.19 1.000 --- u 40. sxompform 0.20 3.000 --- u 41. 1.1,2,2-Tot rachloroethano 0.03 0.200 _-- u 42, 1,2,3-Trichloroprepane 0.05 0.200 --- V 43. 1,4-Di01110robenzena 0.39 1,000 --- V 44, 1,2-Dich1crobOnzana 0,32 5.000 -^- u 45. 1,2-Dibroma-3-Chl0rapropan8 0,07 0.200 --- u 46, Acrylonitrile 2.72 200.000 -^- V 47. trans-1,4-Dichloro-2-Butene 0.42 100.060 --- u 4@. AOrolein 1,97 4.000 -- u d r Bstimated ValUe between the NDL and HRL, u . Below AL14 0uantitation Limite. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA r Drinking water IDi 37715 Waatewater IDG 10 114 OAKMONT DRIVE PHONE (252) 756.6208 GREENVILLE, N.C. 27858 FAX (252) 756-0633 CLIENT: C & D DISPOSAL, INC- CLIENT ID: 6003 B MR. JUDSON WHITEHURST 802 RECYCLING LANE ANALYST: JAP GREENVILLE, NC 27834 DATE COLLECTED: 1.2/15/21 Page: 4 DATE ANALYZED. 12/21/21 DATE REPORTED: 07/18/22 REVIEWED BY: , LANDrILL EPA METHOD PARAMETERS, u9/1 APPENDIX II 8260D R4(18) MDL MRL Trig Blank 49. Allyl Chloride 0A 0 10.00D --- u 50. chloroprtne 0.21 20.000 --- U 51. 1,3-Dichlorabenztne 0.41 5.000 --- V 52, DichlorodLPluoromethane 0.51 5.000 --- V 51. 1,3-Dichloropropana 0.28 1.000 u 54. 2,2-nichloroprapdne 0.11 15.000 --- u 55, 1,1-Dichloropropens 0.22 5.000 --- V 56. 8thyl Methacrylotb 0.16 10.000 --- u 57. Haxachlorobutediena 0,10 0.200 •-- V 58. Iacbutyl Alcohol 12.8D 100.000 --- it 59, methacrylonitrile 1193 100.000 --- V 60. Methyl Methacrylatt 0.25 30,000 --- u 51, Naphthalana 0.47 6.009 --- u $2. Propienitrile 3.26 150.000 --- u 63. 1,2,4-Trich2orobenzene 0.50 10.000 --- Ti 64. ACetdnitrile j6.29 55.000 --- 65, Tatrahydrofuran 0.39 1.000 -•• u 66. 1,4-olaxane 2,71 3.000 •-- V 3 ■ aetimatid velus between the HDL and tM L, U . 5t10W ALL Quantitation Limita. DocuSign Envelope ID: 1 E49C9C5-1 EA4-40EE-BA46-8A724DF270DA ch M 2 0 0 m e� a Q P� WUI R =3 q0 m @ Cr 0 C� 4 N N � m cD cD O2 fo �_l z 10 CD N) cr) Fn CA k., vy all- 4� W C5 i rj toc LA m m irns 4s zz 4 .p rn m M mT TOTAL CHLORINE, mg/1 I j� b �I L m m c7 OR ugll AT CDLLI=CTION M M rg TEMPERA7l1RE,"C r ATCOLLECTION rn D _ Z 5 O # OF CONTAINERS cc Field pH � Nitrate+Nitrite V Alkalinity > Chloride v M Q {i`S`i >;.i<:a Cyanide `b+ ks r, g Sulfate metals r'.# x : Conductivity "b DO Temperature � "4 Field Parameter ix k�€ EPA 8270E139% G� 8370E Dup. 1 Li i EPA 8081E 43dri#' c, PARAMETERSITESTS, cy 2 n m [n fA ,�``�I 9 S_ �? t3J D C1 � Z 2 Mn o Z 71 CD ' n �r = _ _' m M m 71 M ri m m �2 rr� q N Gi O t77 ram- 1 m j� rn F� Cy] o DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA ^ ee 10 n G7 U] � W y � a 4n u? m u w 0 cl rO q w o o $ o � w � m� � w w � �A cn sa a z to Ul a rb CD '6 w p a r '•� 1 0 m f7 ' a n mom+ m_ ] S m ram„ {' TOTAL CHLORINE, mgll L L L L C� W m m OR ug/l AT COLLECTION 2 7 (-- n 0 C b TEMPERATURE,^C W ATCOLLECTION rat cn �'' Fn i Q x w ►a #OFCONTAINERS 8081B Duplicate 0 'S ru", ., 82601) APP. II 4� 8260D App. is 2 G� 8260D APP. 113 G u N 11 S." � 8I51A Landfill � G� �' 3. 3 ..;i MIN E $151A Duplicate > G7 m ITI On ORP "0 rn L� = PARAMETERSITESTS i oa 0 LJ LJ LJ C7 as � n CD 4 rn Q C) 99 m G y� LA m D r [!] p 4 r m z C M p z y 4 � DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA This page intentionally left blank. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA Appendix C Time vs. Concentration Graphs December 2021 Groundwater Monitoring Report CEO Disposal, Inc. NC Solid Waste Permit No. 7407-CDLF-2001 & 7407- CDLF- 2009 DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA This page intentionally left blank. DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA 3 2.5 2 m c_ c 0 1.5 v 0 u 1 0.5 0 Jul-09 BE MW-3S Organochlorides Nov-10 Apr-12 Aug-13 Dec-14 May-16 Sep-17 Feb-19 Jun-20 Oct-21 Mar-23 tTetrachloroethene (CAS 127-18-4) tTrichloroethene (CAS 79-01-6) +1,2-Dichloroethane +cis-1,2-Dichloroethene --*--Vinyl chloride DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA HE MW-3A Organochlorides r-23 DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA 1.6 1.4 1.2 1 0 .� 0.8 u° 0.6 0.4 0.0 0 Jul-09 DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA EJE MW-10 Organochlorides -23 DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA 0.8 0.7 0.6 m 0.5 c 0 0 ±• 0.4 w 0 0.3 u 0.2 0.1 0 Jul-09 EJE MW-11 Organochlorides Nov-10 Apr-12 Aug-13 Dec-14 May-16 Sep-17 Feb-19 Jun-20 Oct-21 Mar-23 t Tetrachloroethene (CAS 127-18-4) t Trichloroethene (CAS 79-01-6) t 1,2-Dichloroethane +cis-1,2-Dichloroethene +Vinyl chloride DocuSign Envelope ID: 1E49C9C5-1EA4-40EE-BA46-8A724DF270DA BE MW-12S Organochlorides 9 8 7 6 � 6 \ / 0 4 w 0 u 3 — 2 — — 1 o ' it i — 0 ti • it • • 1 4 • • • i Jul-09 Nov-10 Apr-12 Aug-13 Dec-14 May-16 Sep-17 Feb-19 Jun-20 Oct-21 Mar-23 t Tetrachloroethene (CAS 127-18-4) t Trichloroethene (CAS 79-01-6) t 1,2-Dichloroethane +cis-1,2-Dichloroethene +Vinyl chloride