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HomeMy WebLinkAboutCCB0057_Nash_SwiftCreek_StructuralFill_Nov2021GW_FID1648935_20220310Water Quality Monitoring Report - November 2021 Swift Creek CCB Structural Fill — CCB0057 Battieboro, Nash County North Carolina Chris Means, Project Manager ERM NC, Inc. 303 West Summit Avenue Suite 330 Charlotte, North Carolina 28203 Phone: +1-704-541-8345 D Copyright 2022 by LRM worldwide Group Ltd and f or its affiliates (-ERM'). All rights reserved. No part or this work may he reproduced or transmitted in any form, or by any means, without the prior written permission of ERM 1 ' ENSE° Brian Wilson, P.G. 7 Principal -in -Charge SEAL 2272 '- I.aG�g 5Qa'�` www.erm.com Version. 1.0 Project No.. 0397281 Client: Reuse Technology March 9, 2022 WATER QUALITY MONITORING REPORT — NOVEMBER 2021 Battleboro, Nash County CONTENTS CONTENTS 1. INTRODUCTION AND SITE HISTORY.............................................................................................1 1.1 Introduction...........................................................................................................................................1 1.2 Summary of Site Environmental History and Corrective Action............................................................1 2. CONCEPTUAL SITI MODEL............................................................................................................3 2.1 Hydrogeology........................................................................................................................................3 2.2 Contaminant Fate and Transport..........................................................................................................3 3. WATER QUALITY MONITORING ACTIVITIES................................................................................4 3.1 Objectives.............................................................................................................................................4 3.2 Monitoring Methods..............................................................................................................................5 4. MONITORING RESULTS......................................................................................................6 4.1 Groundwater Monitoring Results..........................................................................................................6 4.2 Surface Water Monitoring Results........................................................................................................8 4.3 Laboratory Data Quality Analysis..........................................................................................................8 5. SUMMARY.........................................................................................................................................9 APPENDIX A HISTORICAL GROUNDWATER AND SURFACE WATER RESULTS APPENDIX B FIELD SHEETS APPENDIX C LABORATORY DATA List of Figures Figure1 Site Location Map.................................................................................................................. Figure 2 Site Map and Monitor Well Locations.................................................................................... Figure 3 Shallow Groundwater Potentiometric Map — November 2021............................................... Figure 4 Groundwater Analyses - Constituents Exceeding 2L Groundwater Standards — November 2021....................................................................................................................................... Figure 5 Groundwater Analyses — Sulfate — Surficial Aquifer.............................................................. Figure 6 Hydrogeologic Profile A-A...................................................................................................... Figure 7 Sulfate Concentrations over Time — Selected Monitor Wells ................................................ List of Tables Table 1 Monitor Well Construction Data Summary ......................... Table 2 Historical Groundwater Elevation Data .............................. Table 3 Groundwater and Surface Water Analytical Event Results Table 4 Groundwater and Surface Water Field Parameter Results 10 10 10 10 10 10 10 11 11 11 11 www.erm.com Version: 1.0 Project No.: 0397281 Client: ReUse Technology January 19, 2022 Page i WATER QUALITY MONITORING REPORT— NOVEMBER 2021 INTRODUCTION AND SITE HISTORY Battleboro, Nash County INTRODUCTION AND SITE HISTORY 1.1 Introduction On behalf of ReUse Technology, Inc. (ReUse), ERM NC, Inc. (ERM) has prepared this Water Quality Monitoring Report to summarize corrective action activities conducted for the Swift Creek Coal Combustion By -Products (CCBs) Structural Fill site (CCB-0057) located along U.S. Highway 301 north of Battleboro, Nash County, North Carolina, (hereafter called the "Site" or "subject property"). Corrective actions have been implemented at the Site to address groundwater quality impacts in accordance with the Corrective Action Plan (CAP) (ERM, February 27, 2015) approved by the North Carolina Department of Environmental Quality (NCDEQ) on March 12, 2015. The corrective actions were implemented in 2017 and included temporary removal of CCB materials to allow raising the floor elevation above the seasonal high groundwater table, placing the CCB materials on the raised floor in a reduced footprint, installation of a synthetic liner (cap) over the limits of the CCBs, and drainage improvements to minimize rainfall infiltration. Groundwater and surface water monitoring activities presented herein are being conducted at the Site to monitor the effectiveness of the previously completed corrective actions. The Site location is shown in Figure 1. A Site map is included as Figure 2. 1.2 Summary of Site Environmental History and Corrective Action The Site consists of a 25-acre property in northeast Nash County bounded by US Highway 301 to the west, Lane Swamp to the north and east, and Swift Creek to the south. The area surrounding the Site is comprised of sparsely populated agricultural land and partially wooded land. In December 1991, the Solid Waste Section approved a proposed plan submitted by ReUse to use CCBs as structural fill material in the development of the 25 acres as a commercial property. In September 1992, ReUse began placement of CCBs as beneficial use fill at the Site. In January 2003, the last shipment of CCBs was accepted at the Site. In March 2003, the Site had been graded, compacted, covered with an 18-inch soil cap and planted with grass seed. In December 2003, Full Circle Solutions, Inc. purchased the business assets of ReUse Technology, Inc., including the Swift Creek Site. According to records of Full Circle Solutions, Inc., a total of approximately 134,000 tons of CCBs were placed at the Site. On November 4, 2004, the Closure Notice was forwarded to the Solid Waste Section. In August 2004, Sherrill Environmental, Inc. reported the results of groundwater monitoring at four newly installed monitoring wells (MW-1 S/MW-1 D, MW-2S/MW-2D) at the Site. Lead and sulfate were detected at concentrations above the respective North Carolina 2L groundwater standards in the shallow groundwater on the east side of the CCB fill. In October 2004, the Solid Waste Section required an assessment by ReUse to determine the extent of the groundwater impact resulting from the placement of CCBs at the Site. In March 2006, a Comprehensive Site Assessment for the Swift Creek Project was submitted to the Solid Waste Section that included the results of an expanded groundwater and surface water assessment. In September 2006, a Compliance Order was issued by the Solid Waste Section to ReUse. In December 2006, pursuant to the Compliance Order, an Assessment Monitoring Plan and a Swift Creek Dewatering Analysis were submitted to the Solid Waste Section. The Assessment Monitoring Plan described a proposed groundwater and surface water monitoring program for the Site. The Swift Creek Dewatering Analysis described a proposed dewatering subsurface drain along the western boundary of the fill along US Highway 301 to remove water from the coal ash fill and lower the local groundwater table to provide a required minimum 1-foot vertical separation between coal ash and seasonal high groundwater elevations. The Assessment Monitoring Plan was approved by the Solid Waste Section in February 2007. The Swift Creek Dewatering Analysis was conditionally approved by the Solid Waste Section in July 2007 based on the performance of the proposed dewatering plan. www.erm.com Version: 1.0 Project No.: 0397281 Client: ReUse Technology January 19, 2022 Page 1 WATER QUALITY MONITORING REPORT— NOVEMBER 2021 INTRODUCTION AND SITE HISTORY Battleboro, Nash County In January 2008, a dewatering subsurface drain was installed consisting of a 6-inch polyvinyl chloride (PVC) drain pipe along the western boundary of the fill along US Highway 301. The drain was designed to lower the local groundwater table to provide a required minimum 1-foot vertical separation between coal ash and seasonal high groundwater elevations. Groundwater collected in the pipe was transmitted by gravity flow to an outfall box located at the north end of the Site at Lane Swamp. The groundwater and surface water monitoring program was initiated at the Site in October 2007 in accordance with the Assessment Monitoring Plan. The program consisted of semi-annual sampling and laboratory analytical testing for metals and sulfates at eight (8) groundwater monitoring well locations and three (3) surface water monitoring locations. Groundwater levels were also measured in the monitoring wells and piezometers in order to evaluate ground water flow direction and determine water levels relative to the CCB fill. The reported results of the groundwater monitoring from 2007 to 2014 confirmed groundwater quality impacts including concentrations of sulfate, arsenic and lead at levels above the respective North Carolina 2L groundwater standards. The monitoring reported no impacts to surface water quality in Lane Swamp or Swift Creek adjacent to the facility. The Division of Waste Management issued a "Warning Notice" to Full Circle Solutions and ReUse dated May 16, 2014. The notice stated that the required groundwater vertical separation between filled CCBs and seasonal high groundwater elevations had not been achieved and exceedances of the North Carolina 2L groundwater standards had been routinely reported. As a result, a "Groundwater Corrective Action Application" was required to be submitted for approval. On behalf of Full Circle Solutions and ReUse, ERM NC, Inc. (ERM) submitted a Corrective Action Application, dated October 16, 2014, to the Division of Waste Management for approval. The Corrective Action Application proposed the construction of a synthetic liner (cap) and drainage improvements as corrective actions to significantly reduce or eliminate rainfall infiltration and leachate generation from the beneficial fill. Two contingency corrective actions also were identified. The Division issued approval in December 2014 and requested the submittal of a detailed Corrective Action Plan (CAP) to the Solid Waste Section. The Corrective Action Plan was submitted in February 2015 and approved by the NCDEQ Solid Waste Section in March 2015. The Corrective Action Plan was designed to raise existing CCBs to above historically high groundwater levels to prevent the leaching of contaminants of concern from the existing CCBs. The CAP included the installation of a protective liner system, cover soil layer, and drainage outlets to prevent infiltration of precipitation into the CCBs to assist in the prevention of leaching. The footprint of the limits of ash was condensed from approximately 10 acres to 5 acres, reducing the effective infiltration area. Implementation of the CAP was delayed approximately one year in 2015-2016 due to a North Carolina Department of Transportation (NCDOT) project to realign US Highway 301, along with bridge replacements across Swift Creek. The corrective measures began on April 24, 2017 and were completed on January 12, 2018. In June 2018, two new monitoring wells, MW-5RS and MW-5RD, were installed as replacements for former upgradient wells MW-5S and MW-5D, which were abandoned in 2015 by the NCDOT as part of the Highway 301 realignment project. The new wells were located hydraulically upgradient (west) of the Site on the west side of Highway 301 (see Figure 2) to monitor background water quality in the surficial aquifer (MW-5RS) and deep aquifer (MW-5RD) zones. The monitoring wells were installed under an NCDOT right-of-way encroachment agreement (E-0420981800025). In accordance with the CAP, a performance monitoring and reporting plan was implemented in 2018 to monitor the effectiveness of the corrective action. The elements of the performance monitoring plan include: ■ Semi-annual groundwater and surface water monitoring and reporting, www.erm.com Version: 1.0 Project No.: 0397281 Client: ReUse Technology January 19, 2022 Page 2 WATER QUALITY MONITORING REPORT— NOVEMBER 2021 CONCEPTUAL SITE MODEL Battleboro, Nash County ■ Quarterly inspection and reporting of the Site for cap structural integrity, erosion control, proper drainage, etc., and ■ Corrective Action Effectiveness Reports prepared every five years to evaluate and document a reduction in contaminant concentrations in groundwater and a stable or decreasing plume extent. 2. CONCEPTUAL SITE MODEL 2.1 Hydrogeology The following updated conceptual site model (CSM) has been developed based on the corrective action and monitoring work performed by ERM, as well as previous site investigation activities performed by others. The Site is located in the Coastal Plain physiographic province of North Carolina. The Site surficial geology consists of alluvial terrace deposits consisting of layers and mixtures of silts, clay, sands and gravels. The alluvial deposits at the Site range in thickness from approximately 8 to 16 feet. The shallow ground water at the Site occurs in the alluvial deposits and is referred to as the surficial or alluvial aquifer. The alluvial aquifer sands are of low to moderate permeability (average hydraulic conductivity 0.67 feet/day). Within the alluvial aquifer zone, a yellowish -brown clay layer was encountered in the majority of the borings for monitoring wells and piezometers installed at the Site. The clay layer of the alluvial aquifer at the Site is approximately 1 to 4 feet thick and has a low permeability (average hydraulic conductivity 0.002 feet/day). The clayey layer behaves as a confining layer or perching layer, which appears to limit the vertical migration of contaminants at the Site. On the west (upgradient) edge of the Site, the clay layer was reported absent in the borings for former wells MW-5S, MW-51D, P-23 and P-24. The alluvial deposits at the Site are underlain by the Yorktown Formation, a regionally extensive marine deposit. The upper Yorktown Formation, consisting typically of greenish -gray, clayey, silty, Shelly, very fine sands, is encountered at the Site from approximately 13 feet below ground surface (bgs) to the maximum depth of investigation of 35 feet bgs, and has a low permeability (average of 0.002 feet/day). No groundwater quality impacts have been detected in monitoring wells completed in the deeper Yorktown aquifer zone. The general groundwater flow pattern at the Site is controlled largely by two groundwater discharge features: Lane Swamp to the north and east, and Swift Creek to the south. Groundwater flow in the area of the Site is generally from west to east with a northeast component of flow toward Lane Swamp at the north end of the Site, and a southeast component of flow toward Swift Creek at the south end of the Site. 2.2 Contaminant Fate and Transport The key features of the CSM for contaminant fate and transport are summarized as follows: ■ The depth to groundwater ranges from the ground surface at the creeks and swamps to more than 6 feet bgs in topographically higher areas (not including the beneficial fill footprint). ■ The regional groundwater flow regime within the surficial (alluvial) aquifer flows west to east, with north and south flow components near Swift Creek and Lane Swamp, which serve as shallow groundwater discharge features. ■ The estimated groundwater velocities at the Site are very low. The historical calculated groundwater velocities are approximately 6 to 27 feet per year for the surficial (alluvial) aquifer and approximately 0.03 feet per year for the deeper Yorktown aquifer. ■ Prior to the 2018 corrective action, seasonal rises of the underlying water table and rainfall infiltration downward through the old soil cap resulted in water infiltration into the coal ash fill. Constituents www.erm.com Version: 1.0 Project No.: 0397281 Client: ReUse Technology January 19, 2022 Page 3 WATER QUALITY MONITORING REPORT— NOVEMBER 2021 WATER QUALITY MONITORING ACTIVITIES Battleboro, Nash County within the coal ash fill were dissolved by the infiltration water and became mobile. The former infiltration mechanism has been mitigated by the corrective action. Once the infiltration water enters the surficial groundwater, it migrates laterally above a clay confining or perching layer within the alluvial aquifer zone towards the groundwater discharge features of Lane Swamp and Swift Creek, which serve to limit the lateral extent of the affected groundwater. The limited lateral extent of the affected groundwater is evident at wells MW-2S and 2D, located approximately 200 feet east of the former perimeter of the beneficial fill, where groundwater concentrations are below 2L groundwater standards. Similarly, there is no evidence of affected groundwater to the west (upgradient) as demonstrated by groundwater monitoring results at current monitoring wells MW-5RS and MW-5RD and former monitoring wells MW-5S and 5D. ■ Based on historical groundwater monitoring results, the groundwater quality impacts at the Site are limited to the surficial aquifer zone. No groundwater quality impacts are detected in the deeper aquifer zone of the Yorktown Formation. The swamps and creeks surrounding the beneficial fill site act as a "natural perimeter drain" and intercept the affected groundwater. Based on the historical surface water monitoring results, there are no surface water quality impacts to Lane Swamp or Swift Creek due to affected groundwater from the Site. 3. WATER QUALITY MONITORING ACTIVITIES 3.1 Objectives Demonstration of effectiveness of the completed remediation is the primary objective of the water quality monitoring program (i.e. remedial performance monitoring). This objective is achieved by monitoring the reduction of the site -specific contaminants of concern (COC) in groundwater, therefore mitigating the potential for surface water quality impacts due to contaminated groundwater migration and discharge to surface water. The applicable preliminary remedial goals for groundwater and surface water are summarized below. www.erm.com Version: 1.0 Project No.: 0397281 Client: ReUse Technology January 19, 2022 Page 4 WATER QUALITY MONITORING REPORT — NOVEMBER 2021 WATER QUALITY MONITORING ACTIVITIES Battleboro, Nash County 1compounds • • NC 2L •. •NC Surface Water 2B Standard Arsenic • 0.01 • 0.15 Barium 0.7 NE Cadmium 0.002 h Chromium (Total) 0.01 h Lead 0.015 0.025 Mercury 0.001 0.000012 Selenium 0.02 0.005 Silver 0.02 0.00006 Sulfate 250 NE pH 6.5-8.5 6.0-9.0 North Carolina 2L Groundwater Quality Standard (April 1, 2013) 2 North Carolina Surface Water Quality Standard for Class C Waters (July 26, 2021) NE = Not Established mg/L = milligrams per liter h = hardness dependent dissolved metal standard Water quality monitoring is conducted in accordance with the NCDEQ-approved Corrective Action Plan (ERM, March 2015). The following sections summarize the groundwater and surface water monitoring activities conducted at the Site during the reporting period. 3.2 Monitoring Methods A water quality monitoring event was conducted at the Site on November 1-2, 2021. Groundwater and surface water samples were collected from the following monitoring wells and surface water locations. Monitoring Wells Surface Water Locations MW-1 S SW-1 MW-1 D SW-2 MW-2S SW-3 MW-2D MW-3 MW-4 MW-5RS MW-5RD MW-6 M W-7 MW-8 Subtotal: 11 Subtotal: 3 The monitoring well and surface water locations are shown on Figure 2. Monitoring well construction details are summarized in Table 1. All monitoring wells were gauged for water levels and then purged and sampled by low -flow purging methods. The surface water samples were collected as grab samples using clean containers. Field parameters (pH, conductivity, temperature, dissolved oxygen and oxidation-reduction potential) were www.erm.com Version: 1.0 Project No.: 0397281 Client: ReUse Technology January 19, 2022 Page 5 WATER QUALITY MONITORING REPORT — NOVEMBER 2021 MONITORING RESULTS Battleboro, Nash County measured for each groundwater and surface water sample by calibrated meters. Well purge logs were completed for each monitoring well to document the stabilization of field parameters prior to sample collection. Well purge logs are provided in Appendix B. The groundwater and surface water samples were placed in laboratory supplied containers and placed on ice. The samples were submitted to North Carolina certified laboratory Pace Analytical Services (Formerly Shealy Environmental Services) (NC329) and were analyzed for eight specific metals, sulfates and total dissolved solids using the analytical methods summarized below: Analytical Methods MethodEPA EPA Method 6010 EPA Method 7470C Compound Arsenic Barium Cadmium Chromium (Total) Lead Selenium Silver Mercury EPA 300.0 Sulfates SM 2540 C Total Dissolved Solids 4. MONITORING RESULTS 4.1 Groundwater Monitoring Results Groundwater monitoring activities were conducted at 11 monitoring wells at the Site. Groundwater depth - to -water gauging and elevation data are presented in Table 2. The groundwater elevations in the surficial aquifer on November 1, 2021 ranged from 89.89 feet above mean sea level (ft MSL) at MW-7 located on the east (downgradient) side of the Site to 93.12 ft MSL at MW-4 located on the west (upgradient) side of the Site. The groundwater elevations are below the base of the CCB fill, which generally ranges from 94 to 99 ft MSL from east to west. A potentiometric surface map for the surficial (alluvial) aquifer zone for the November 2021 monitoring event is presented as Figure 3. Groundwater flow in the surficial aquifer over most of the Site is generally west to east towards Lane Swamp Swift Creek, which serve as groundwater discharge zones. Using the current groundwater elevation data, the hydraulic gradients for the Site were calculated. See summarized table below. Horizontal Hydraulic.• - 01-November-2021 Well Head Head Distance Hydraulic Gradient Designation Elevation Change Change (ft) (ft) (ft) (ft/ft) • � • .1 11 11 / 1/ - .•- Hvdraulic Gradient0.0035 www.erm.com Version: 1.0 Project No.: 0397281 Client: ReUse Technology January 19, 2022 Page 6 WATER QUALITY MONITORING REPORT — NOVEMBER 2021 Battleboro, Nash County MONITORING RESULTS Groundwater seepage velocities were calculated using Darcy's equation, summarized as: Where: V=(Kxi)/ne V = seepage velocity of groundwater in ft/day K = hydraulic conductivity in ft/day i = hydraulic gradient (ft/ft) ne = effective porosity As summarized below, the estimated groundwater seepage velocity in the surficial aquifer zone using a primary porosity range of 10-25% is approximately 3 to 7 feet per year based on the November 2021 hydraulic gradients and the previously calculated mean hydraulic conductivities. Seepage Velocity Range (Surficial Aquifer) = = (0.55) (0.0035) / (0.25) = 7.66E-03 ft/day = (0.55) (0.0035) / (0.10) = 1.91 E-02 ft/day Range 25% 2.80 ft/yr of porosity 10% 6.99 ft/yr Seepage of3to7 The November 2021 groundwater analytical results are summarized in Table 3 for metals, sulfate and total dissolved solids (TDS), and in Table 4 for field parameters. Constituents that exceeded North Carolina 2L groundwater standards are summarized on Figure 4. Laboratory analytical reports for the sampling event are provided in Appendix D. A historical groundwater data summary is provided in Appendix A. For the November 2021 monitoring event, four analytes were detected above their respective North Carolina 2L groundwater standards, as summarized in the following table. www.erm.com Version: 1.0 Project No.: 0397281 Client: ReUse Technology January 19, 2022 Page 7 WATER QUALITY MONITORING REPORT— NOVEMBER 2021 Battleboro, Nash County MONITORING RESULTS Current Maximum Concentrations in Groundwater — November 2021 Arsenic 0.090 0.01 Lead 0.27 0.015 Sulfate 810 250 Total Dissolved Solids 10,000 500 mg/L = milligrams per liter Sulfate, a primary indicator analyte for CCB contaminant releases, was detected in groundwater at concentrations above its 2L standard (250 mg/L) at five of the 11 monitoring wells. The distribution of sulfate concentrations across the Site is depicted in Figure 5. A hydrogeologic profile across the Site, including sulfate concentrations in groundwater, is presented in Figure 6. The highest concentration of sulfate was detected in the groundwater sample collected from monitoring well MW-3 (810 mg/L) located on the southern (locally downgradient) side of the Site. Graphs of sulfate concentrations over time for selected monitoring wells are presented in Figure 7. Since the completion of the corrective action in January 2018, the graphs indicate fluctuating but overall decreasing sulfate concentration trends at MW-3, MW-6, MW-7 and MW-8, where the most elevated sulfate levels have historically been observed. Notably low values of pH were measured in the groundwater samples from MW-6 (3.7), MW-7 (3.7), and MW-8 (3.9). The low pH values at the three wells are consistent with historical monitoring results, and correlate with detections of arsenic and lead, in addition to sulfate, at concentrations above their respective North Carolina 2L groundwater standards at the three wells. There were no exceedances of 2L standards in the two monitoring wells located on the west (upgradient) side of the Site (MW-5RS & MW-5RD). Monitoring well MW-4, located near the southwest limit of the CCB fill area, had only one exceedance (arsenic 0.035 mg/L) during the November 2021 monitoring event. Historically, there have been no detectable levels of arsenic at MW-4 since 2010. On the east side of the Site, sulfate and TDS concentrations exceeded their 2L standards in MW-1 S, which is consistent with historical monitoring results. The only other exceedance of the 2L standards detected in the four monitoring wells located on the east side of the Site (MW-1 D, MW-1 S, MW-2S and MW-21D) was a concentration of TDS in MW-1 D. The elevated TDS concentration at MW-1 D does not appear to be attributable to sulfate or metals, which were not present at elevated levels. 4.2 Surface Water Monitoring Results Consistent with historical monitoring results, all November 2021 surface water monitoring results were below the respective North Carolina 2B surface water standards for samples collected from Swift Creek (SW-1) and Lane Swamp (SW-2 and SW-3). The November 2021 surface water sampling results are summarized in Table 3. Laboratory analytical reports for the surface water samples are provided in Appendix D. Historical surface water data is summarized in Appendix A. 4.3 Laboratory Data Quality Analysis Quality assurance/quality control (QA/QC) samples collected during the November 2021 groundwater sampling activities included one blind duplicate sample collected at MW-1 S. The duplicate and parent www.erm.com Version: 1.0 Project No.: 0397281 Client: ReUse Technology January 19, 2022 Page 8 WATER QUALITY MONITORING REPORT— NOVEMBER 2021 SUMMARY Battleboro, Nash County sample results for MW-1S can be compared in Table 3. The analytical results of the MW-1S and duplicate groundwater samples compare favorably, indicating no analytical discrepancy. 5. SUMMARY Corrective actions have been implemented at the Site to address groundwater quality impacts in accordance with the approved CAP. The corrective actions were completed in January 2018 and included temporary removal of CCB materials to allow raising the floor foundation above the seasonal high groundwater table, placing the CCB materials on the raised floor in a reduced footprint, installation of a synthetic liner (cap) over the limits of the CCBs, and drainage improvements to minimize rainfall infiltration. Groundwater and surface water monitoring activities are being conducted at the Site to monitor the effectiveness of the previously completed corrective actions. The November 2021 water quality monitoring event evaluated groundwater and surface water quality conditions at the Site approximately 3.8 years after the corrective action completion. Since the completion of the corrective action in 2018, the 4 monitoring wells (MW-3, MW-6, MW-7 and MW-8) historically exhibiting the greatest sulfate concentrations in groundwater continue to exhibit overall decreasing trends as shown in Figure 7. The trend of decreasing sulfate concentrations indicates that the corrective action is effectively mitigating the groundwater quality impacts at the Site. The November 2021 surface water quality results continue to demonstrate that there have been no surface water impacts to Swift Creek or Lane Swamp due to discharges of affected groundwater from the Site. In accordance with the CAP, semi-annual water quality monitoring will continue at the Site, with the next monitoring event tentatively planned for March 2022. www.erm.com Version: 1.0 Project No.: 0397281 Client: ReUse Technology January 19, 2022 Page 9 WATER QUALITY MONITORING REPORT — NOVEMBER 2021 SUMMARY Battleboro, Nash County Figures Figure 1 Site Location Map Figure 2 Site Map and Monitoring Well Locations Figure 3 Shallow Groundwater Potentiometric Map — November 2021 Figure 4 Groundwater Analytical Sample Results - Constituents Exceeding 2L Groundwater Standards — November 2021 Figure 5 Groundwater Analytical Sample Resultss —Sulfate —Surf icial Aquifer Figure 6 Hydrogeologic Profile A -A' Figure 7 Sulfate Concentrations over Time — Selected Monitoring Wells www.erm.com Version: 1.0 Project No.: 0397281 Client: ReUse Technology January 19, 2022 Page 10 e ; F •f " k y ! �vl i j{.� r y .r evil IN it 3 1 t_. _ +► w If n rL+],1 � � _ 1''e(yr��jq"y� y- w 'r � �= y __ �., � f � � �. .� � � •►r � -� _ f � � �`��-�+ � � �N► 4 M _ � � } � f� f ti � f �� �_ r4-� _ yam+ ,_ �- �� � � � � •� - - Vim__ M ~ + _ w!w ww _ �, f w w� .+r. w + + • w.s. 'r -rw - w - �'-w �` w •r -lot- w 41 rr s r + J L u' a r • w $ d11 "� i! r1� r rAP n ' Feet ��� ' L� ! y Legend N Figure 1 Q site Site Location Map o 2,000 ReUse Technology, Inc. Swift Creek CCB Structural Fill - CCB0057 LD i Environmental Resources Management Feet Battleboro, Nash County, North Carolina ERM `v` w.erm.com 1:24,000 1 inch = 2,000 feet Source: Copyright:© 2013 National Geoqraphic Society, i-cubed Coordinate System: NAD 1983 StatePlane North Carolina FIPS 3200 Feet »I 1 u � u n i MW-5RS -Al SW-1 �I i �A J'I ;Mw_3 ~MWz1S MW-1D MW-2D M W-7 `6 MW-8 DI 1:2,400 1 inch = 200 feet r 0 100 200 5 7 Feet tq C N 2 A Legend Figure 2 £, Shallow Monitoring Well Q Site Site Plan '. Abandoned Shallow Monitoring Well Topographic Contour (1-ft intervals) Reuse Technology, Inc. Deep Monitoring Well .// Wetland Swift Creek CCB Structural Fill - CCB0057 Abandoned Deep Monitoring Well E% Freshwater Pond Battleboro, Nash County, North Carolina 0 Surface Water Monitoring Location 0 Riverine Environmental Resources Management w o_ www.erm.com ERM Source: Sources: Esri, HERE, Garmin, Intermap, increment P Corp., GEBCO, USGS, FAO, NPS, NRCAN, GeoBase, IGN, Kadaster NL, Ordnance Survev, Esri Japan, METI, Esri China (Hong Konq), (c) OpenStreetMap contributors, and the GIS User Communitv Coordinate Svstem: NAD 1983 StatePlane North Carolina FIPS 3200 Feet Esri, DigitalGlobe, GeoEye, Earthstar Geographies, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the GIS User Community SW-1 � l 1:1,680 1 inch = 140 feet 01 z 0 70 140 7 Feet b, MW-5RS _ --------- MW-51RD 91.49 — 91.22*,Q� 48MW--5D — 1 MW-4— 93.12 M W-3 9124 ` o CO i ►w w-9 MW-1S 90.46* MW-7 89.93 90+50* .90�66 SW-2 MW-8 90.06 Legend Shallow Monitoring Well r--j Site Potentiometric Surface Contour '. Abandoned Shallow Monitoring Well Topographic Contour (1-ft intervals) Apparent Groundwater Flow Direction Deep Monitoring Well Wetland Notes: Groundwater elevation measurements collected 02 Nov 2021. Abandoned Deep Monitoring Well Freshwater Pond 91.49 - Groundwater Elevation in Shallow Monitoring Well 0 Surface Water Monitoring Location Riverine 91.22" - Groundwater Elevation in Deep Monitoring Well (not contoured) Elevations in feet above mean sea level �f MW-6 ); 89.89 A SW-3 Figure 3 Shallow Groundwater Potentiometric Surface ReUse Technology, Inc. Swift Creek CCB Structural Fill - CCB0057 Battleboro, Nash County, North Carolina Environmental Resources Management www.erm.com ERM Coordinate Svstem: NAD 1983 StatePlane North Carolina FIPS 3200 Feet �rce: Esri, DigitalGlobe, GeoEye, Earthstar Geographies, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the GIS User Community e_ MW-5RD None Exceed MW-5RS None Exceed --r . -•- ._ ---- — •- MW-4 11/02/2021 Arsenic 0.035 SW-1 j None Exceed r MW-3 11/02/2021 Sulfate 810 Dissolved Solids. Total 2,700 MW-1 S 11/01/2021 Sulfate 380 Dissolved Solids, Total 6,800 H MW-1 D 11/01/2021 Dissolved Solids. Total 720H ,1 SW-2 None Exceed MW-6 Sulfate Dissolved Solids. Total 790 MW-7 09 1 11/01/2021 Arsenic 0.090 Lead 0.27 Sulfate 700 Dissolved Solids, Total 10,000 1:1,800 1 inch = 150 feet SW-3 N None Exceed D 0 75 150 y c I MMMU Feet - Legend Figure 4 Shallow Monitoring Well Q Site Groundwater Analytical Results - Exceeds Standards E t+tchir: E '. Abandoned Shallow Monitoring Well CCB Structural Fill Boundary Reuse Technology, Inc. ° n Deep Monitoring Well Topographic Contour (1-ft intervals) Notes: Swift Creek CCB Structural Fill - CCB0057 Abandoned Deep Monitoring Well ��/, Wetland Groundwater samples collected 02 Nov 2021. Battleboro, Nash County, North Carolina 0 0 Surface Water Monitoring Location Freshwater Pond 810 - Concentration in Monitoring Well Concentrations in milligrams per liter (mg/L) Environmental Resources Management 0 0 Riverine Only Concentrations that exceed applicable regulatory standards are shown www.:rm.com ERM Source: Sources: Esri, HERE, Garmin, Intermap, increment P Corp., GEBCO, USGS, FAO, NPS, NRCAN, GeoBase, IGN, Kadaster NL, Ordnance Survey, Esri Japan, METI, Esri China (Hong Konq), (c) OpenStreetMap contributors, and the GIS User Communitv Coordinate Svstem: NAD 1983 StatePlane North Carolina FIPS 3200 Feet ce: Esri, DigitalGlobe, GeoEye, Earthstar Geographies, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the GIS User Community tMW=4 SW-1 1 161 MW 810'. 1 b, MW-5RD MW-5RS 6.0 2.8 ci?IMW--5D — 1 Y MW-1S 380fMW 1 D MW-2D \ 1.1 i MW 2S SW-2 1:1,680 1 inch = 140 feet !�\ z 0 70 140 Feet N C N Legend ❑ Shallow MonitoringWell Site Sulfate Isoconcentration Contours trr_n: '. Abandoned Shallow Monitoring Well Topographic Contour (1-ft intervals) Notes: Deep Monitoring Well Wetland Groundwater samples collected 02 Nov 2021. 91.49 - Sulfate Concentration in Monitoring Well Abandoned Deep Monitoring Well E% Freshwater Pond Concentration in milligrams per liter (mg/L) 0 Surface Water Monitoring Location F Riverine BMW-7 700 MW-8 ie610 . "*�� -1-100 +J p MW-6 i� : — c ✓790� N SW-3 Figure 5 Groundwater Analytical Results - Sulfate ReUse Technology, Inc. Swift Creek CCB Structural Fill - CCB0057 Battleboro, Nash County, North Carolina Environmental Resources Management www.erm.com ERM Coordinate Svstem: NAD 1983 StatePlane North Carolina FIPS 3200 Feet ,urce: Esri, DigitalGlobe, GeoEye, Earthstar Geographies, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the GIS User Community 0 u u Notes: 0 o Vertical Exaggeration = 10:1 (90.55) Groundwater Elevation 1 inch = 150 feet 380 Sulfate Concentration (mg/L) ' A A Groundwater Elevation 2021) (November Well Details 150 150 _ Casing ® Screen 140 140 Subsurface Details ♦ h Existing Clay Layer from Boring ♦ �, Logs (Alluvial) 130 ♦ 130 e !I lzu i lzu n CCB Fill 110 110 n '2 Y , El n (93.12) ♦ L 100 n p rn N � ♦ , � �rL M 100 (90.66) 90 25 90 380 9 3 700 so <1.0 610 80 Alluvial Aquifer 0 325 650 Feet 70 Yorktown Aquifer 70 16 n -I 6o L A 1.1 J 60 >I 50 1 1 50 0 100 200 300 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 Fig u re6 , Earthstar Geoqraphics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, Hydrogeologic Profile A -A' ReUse Technology, Inc. Swift Creek CCB Structural Fill - CCB0057 Battleboro, Nash County, North Carolina Environmental Resources Management kb www.erm.com ERM Coordinate System: NAD 1983 StatePlane North Carolina RIPS 3200 Feet FIGURE 7 - SULFATE CONCENTRATIONS OVER TIME SWIFT CREEK CCB FILL SITE 800 700 600 500 n 400 v 300 3 `) 200 100 0 >J�O O'l OV O\ O% O_J /� Y /� V A'J /�N lb nV ^ \ N% ^_J r& /� Y PJ� �eQ &, �° O Sao Y �1 >4a Y PQ >�o Y 1O0 Y ,J� Y PJ�Y 4 > dG- V�°, V Sulfate ......••• Sulfate Concentration Trend MW-3 1200 1000 800 J 600 v N 400 200 0 Oh 00 O� O� O� ,y0 ,y'y y'L ,y3 ,you `yh ti� ti� ti� ti0 ,y0 ,titi O O O O O O O O O O O O O O O O O Sulfate ......••• Sulfate Concentration Trend 1200 1000 800 J bD C 600 v 7- 400 200 0 W® MW-6 (�, 00 O� O� O°� y0 yy yL yS yb yh ti0 ti� ti� ti� ti0 Ly O O O O O O O O O O O O O O O O O 0—Seriesl ......••• Sulfate Concentration Trend FIGURE 7 - SULFATE CONCENTRATIONS OVER TIME SWIFT CREEK CCB FILL SITE 1000 900 800 700 600 on 500 400 2= zv000� 'n 300 200 100 0 Oh O� 01 OR' O� y0 yy yL y3 yA yh 1� 'yA y4' ti0 ti0 by e� e� e� e� e� e� e� e� e� e� O O O O O O O O O O O O O O O O O f Sulfate ......••• Sulfate Concentration Trend MW-8 1200 1000 800 J bD 600 v' m 75 400.... ..........• N Iis1s. 0 OA ow o� do titi titi ti3 ti° ti`' ti° ti� tiw ti° do titi ♦Sulfate ......••• Sulfate Concentration Trend WATER QUALITY MONITORING REPORT — NOVEMBER 2021 Battleboro, Nash County SUMMARY Tables Table 1 Monitoring Well Construction Data Summary Table 2 Historical Groundwater Elevation Data Table 3 Groundwater and Surface Water Analytical Sample Results Table 4 Groundwater and Surface Water Field Parameter Results www.erm.com Version: 1.0 Project No.: 0397281 Client: ReUse Technology January 19, 2022 Page 11 TABLE 1 MONITOR WELL CONSTRUCTION DATA SUMMARY - SWIFT CREEK PROJECT Monitor Well Top of Casing Elev. MW-1 S 99.54 MW-1 D 99.90 MW-2S 94.87 MW-21D 95.22 MW-3 102.15 MW-4 106.06 MW-5S 102.68 MW-51D 102.67 MW-5RS 98.80 MW-5RD 98.57 MW-6 98.41 MW-7 98.63 MW-8 95.42 Ground Surface Elev. 96.8 97.1 92.1 92.2 99.2 104.1 99.7 99.8 TBD TBD 95.0 95.1 92.4 Casing Stick Up 2.7 2.8 2.8 3.0 3.0 2.0 3.0 2.9 Flush Mount Flush Mount 3.4 3.5 KIM Screen Interval 3-13 23-33 6-16 26-36 7-17 8-18 6-16 25-35 8-18 30-35 6-16 6-16 Total Depth (TOC) 15.7 35.7 18.7 39.1 20.0 20.0 17.0 37.9 18.0 37.9 19.4 19.5 19.0 Status Active Active Active Active Active Active Abandoned Abandoned Active Active Active Active Active Piezometer P-1 108.19 105.6 2.6 20-30 32.6 Abandoned P-2 109.53 106.7 2.8 20-30 32.8 Abandoned P-3 106.18 104.4 1.8 18-28 30.0 Abandoned P-4 106.57 104.0 2.6 20-30 32.6 Abandoned P-5 108.39 105.9 2.5 20-30 32.5 Abandoned P-6 109.79 107.5 2.3 20-30 32.3 Abandoned P-7 107.77 105.9 1.9 30-40 41.9 Abandoned P-8 106.53 103.9 2.6 30-40 42.6 Abandoned P-9 103.32 100.9 2.4 20-30 32.4 Abandoned P-10 108.17 106.1 2.1 20-30 32.1 Abandoned P-11 101.88 99.2 2.7 13-23 25.7 Abandoned P-12 107.04 104.0 3.0 6-16 19.0 Abandoned P-13 108.99 105.9 3.1 6-16 19.1 Abandoned P-14 105.38 101.9 3.5 4-14 17.5 Abandoned P-15 103.76 101.0 2.8 4-14 16.8 Abandoned P-16 105.28 102.1 3.2 4-14 17.2 Abandoned P-17 105.31 101.8 3.5 4-14 17.5 Abandoned P-18 111.21 107.5 3.7 5-15 18.7 Abandoned P-19 111.86 108.3 3.6 7-17 20.6 Abandoned P-20 107.00 104.2 2.8 7-17 19.8 Abandoned P-21 104.99 99.5 5.5 4.5-11.5 16.5 Abandoned P-22 103.60 101.8 1.8 17-27 28.8 Abandoned P-23East 109.75 107.1 2.7 9-19 21.8 Abandoned P-24West 103.17 101.1 2.1 3-13 15.3 Abandoned B-1 107.66 105.7 2.0 14-19 21.0 Abandoned TABLE 2 HISTORICAL GROUNDWATER ELEVATION DATA SWIFT CREEK - CCB0057 BATTLEBORO, NORTH CAROLINA Page 1 of 1 Depth Elevation Depth Elevation Depth Elevation Depth Elevation Depth Elevation Depth Elevation Depth Elevation Depth Elevation Depth Elevation Depth Elevation Depth Elevation Depth Elevation Depth Elevation Depth Elevation Gauging Date ft BTOC ft MSL ft BTOC ft MSL ft BTOC ft MSL ft BTOC ft MSL ft BTOC ft MSL ft BTOC ft MSL ft BTOC ft MSL ft BTOC ft MSL ft BTOC ft MSL ft BTOC ft MSL ft BTOC ft MSL ft BTOC ft MSL ft BTOC ft MSL ft BTOC ft MSL Well Identification MWAS MW-1D MW-2S MW-213 MW-3 MW-4 MW-5S MW-5D MW-6 MW-7 MW-8 MW-5RS MW-5RD Lane Swamp TOC Elevation: 99.54 99.90 94.87 95.22 102.15 106.06 102.68 102.67 98.41 98.63 95.42 98.80 98.57 92.25 TOC Stickup (Ft from GL) 2.7 2.8 2.8 6-16 3.0 3.0 2.0 3.0 2.9 25-35 3.4 3.5 3.0 6-16 N/A Screened Interval (Ft BGL) 3-13 23-33 26-36 7-17 8-18 6-16 6-16 6-16 8-18 30-35 N/A Geologic Zone Screened Surficial Surficial Surficial Deep (Yorktown) Surficial Surficial Surficial Deep (Yorktown) Surficial Surficial Surficial Surficial Deep (Yorktown) N/A 12-Jan-2005 8.21 91.33 8.57 91.33 4.72 90.15 4.7 90.52 9.65 92.50 11.24 94.82 6.01 96.67 6.4 96.27 7.17 91.24 7.63 91.00 NM - -- 1-Aug-2006 8.11 91.43 8.28 91.62 NM -- NM -- 9.48 92.67 10.15 95.91 5.86 96.82 5.68 96.99 7.18 91.23 7.74 90.89 NM - -- 6-Sep-2006 8.69 90.85 9.05 90.85 4.83 90.04 4.87 90.35 10.32 91.83 11.41 94.65 6.94 95.74 6.84 95.83 7.74 90.67 8.66 89.97 NM - 4-Apr-2007 7.80 91.74 8.18 91.72 4.4 90.47 4.75 90.47 9.31 92.84 9.96 96.10 6.12 96.56 5.96 96.71 7.28 91.13 7.8 90.83 4.84 90.58 - 21-Aug-2007 10.89 88.65 11.30 88.60 6.77 88.10 6.82 88.40 11.4 90.75 13.28 92.78 9.57 93.11 9.42 93.25 10.8 87.61 10.71 87.92 7.67 87.75 - 21-Oct-2007 11.40 88.14 11.76 88.14 7.31 87.56 7.43 87.79 12.98 89.17 14.06 92.00 10.62 92.06 10.63 92.04 11.9 86.51 11.41 87.22 8.3 87.12 - -- 31-Jan-2008 9.13 90.41 9.42 90.48 4.86 90.01 5.02 90.20 10.7 91.45 14.11 91.95 7.65 95.03 8.11 94.56 8.44 89.97 8.71 89.92 5.57 89.85 -- -- 22-Mar-2008 8.10 91.44 8.44 91.46 4.4 90.47 4.54 90.68 9.18 92.97 13.28 92.78 6.98 95.70 7.34 95.33 7.18 91.23 7.79 90.84 4.78 90.64 -- - 2.51 89.74 9-Apr-2008 9.26 90.28 9.47 90.43 4.58 90.29 5.02 90.20 10.98 91.17 14.82 91.24 10.87 91.81 10.72 91.95 8.92 89.49 9.06 89.57 5.97 89.45 - - 3.1 89.15 17-Jun-2008 9.12 90.42 9.42 90.48 5.03 89.84 5.23 89.99 10.54 91.61 14.05 92.01 8.93 93.75 8.92 93.75 8.36 90.05 9.06 89.57 6.09 89.33 - -- 3.2 89.05 13-Jan-2009 8.22 91.32 8.55 91.35 4.26 90.61 4.46 90.76 9.35 92.80 13.41 92.65 7.16 95.52 7.54 95.13 7.02 91.39 7.6 91.03 4.58 90.84 -- 2.52 89.73 31-Mar-2009 7.60 91.94 7.96 91.94 4.36 90.51 4.38 90.84 6.74 95.41 12.43 93.63 5.98 96.70 6.22 96.45 6.81 91.60 7.2 91.43 4.21 91.21 - 2.5 89.75 23-Jun-2009 8.62 90.92 8.92 90.98 4.41 90.46 4.77 90.45 10.06 92.09 13.86 92.20 9.83 92.85 9.63 93.04 7.72 90.69 8.52 90.11 5.56 89.86 - - 2.9 89.35 30-Sep-2009 8.86 90.68 9.18 90.72 4.64 90.23 5.00 90.22 10.82 91.33 14.7 91.36 10.4 92.28 10.26 92.41 8.08 90.33 8.51 90.12 5.5 89.92 - -- 3.15 89.10 15-Dec-2009 7.54 92.00 NM -- 4.22 90.65 NM -- 8.68 93.47 12.85 93.21 6.3 96.38 NM -- 6.78 91.63 7.13 91.50 4.21 91.21 - - 2.6 89.65 31-Mar-2010 7.37 92.17 7.74 92.16 2.42 92.45 4.46 90.76 8.64 93.51 12.52 93.54 5.8 96.88 6.19 96.48 6.77 91.64 7.93 90.70 3.96 91.46 - 2.14 90.11 29-Jun-2010 9.35 90.19 NM -- 4.94 89.93 NM -- 10.66 91.49 14.62 91.44 9.97 92.71 NM -- 9.21 89.20 9.25 89.38 6.31 89.11 -- 3.35 88.90 28-Sep-2010 9.23 90.31 10.05 89.85 4.8 90.07 5.50 89.72 11.55 90.60 14.8 91.26 10.85 91.83 11.1 91.57 9.11 89.30 8.52 90.11 5.48 89.94 - - 4.1 88.15 13-Dec-2010 8.54 91.00 NM -- 4.36 90.51 NM -- 10.12 92.03 14.02 92.04 8.72 93.96 NM -- 7.37 91.04 7.93 90.70 4.81 90.61 - - 2.02 90.23 28-Mar-2011 8.03 91.51 8.42 91.48 4.35 90.52 4.67 90.55 9.17 92.98 13.32 92.74 7.45 95.23 7.84 94.83 7.25 91.16 7.53 91.10 4.42 91.00 - 2.85 89.40 26-Jun-2011 10.05 89.49 10.35 89.55 6.02 88.85 6.32 88.90 11.23 90.92 14.82 91.24 10.59 92.09 10.43 92.24 9.2 89.21 9.98 88.65 7.04 88.38 -- 2.85 89.40 28-Sep-2011 7.84 91.70 NM -- 4.24 90.63 NM -- 8.9 93.25 13.09 92.97 7.62 95.06 NM -- 7.13 91.28 7.71 90.92 4.83 90.59 -- - 2.2 90.05 18-Dec-2011 8.00 91.54 8.35 91.55 4.32 90.55 4.65 90.57 8.88 93.27 13.1 92.96 7.35 95.33 7.7 94.97 6.98 91.43 7.53 91.10 4.47 90.95 - 1.8 90.45 23-Mar-2012 8.01 91.53 8.35 91.55 4.31 90.56 4.56 90.66 8.89 93.26 13.01 93.05 7.35 95.33 7.66 95.01 7.03 91.38 7.75 90.88 4.8 90.62 -- 1.65 90.60 28-Jun-2012 8.39 91.15 8.72 91.18 4.65 90.22 4.92 90.30 9.4 92.75 13.38 92.68 8.52 94.16 8.54 94.13 7.42 90.99 8.45 90.18 5.63 89.79 -- 1.95 90.30 18-Sep-2012 7.41 92.13 7.86 92.04 4.16 90.71 4.5 90.72 8.21 93.94 12.73 93.33 7.21 95.47 7.45 95.22 6.82 91.59 7.37 91.26 4.51 90.91 - 1.52 90.73 17-Dec-2012 8.04 91.50 8.44 91.46 NM -- NM -- 9.19 92.96 13.36 92.70 8.55 94.13 8.76 93.91 6.82 91.59 7.37 91.26 4.51 90.91 - - 1.45 90.80 26-Mar-2013 7.87 91.67 8.13 91.77 4.23 90.64 4.46 90.76 8.71 93.44 12.84 93.22 7.03 95.65 7.38 95.29 7.08 91.33 7.26 91.37 4.22 91.20 -- 2.05 90.20 12-Apr-2013 8.30 91.24 8.59 91.31 4.31 90.56 4.72 90.50 9.59 92.56 14.13 91.93 8.48 94.20 8.7 93.97 7.47 90.94 7.8 90.83 4.82 90.60 -- 2.85 89.40 25-Jun-2013 8.00 91.54 8.34 91.56 4.18 90.69 4.57 90.65 9.05 93.10 12.97 93.09 6.92 95.76 7.44 95.23 7.05 91.36 7.7 90.93 4.69 90.73 2.45 89.80 26-Sep-2013 8.38 91.16 8.67 91.23 4.32 90.55 4.71 90.51 9.57 92.58 13.65 92.41 9.5 93.18 9.5 93.17 8.75 89.66 8.19 90.44 5.25 90.17 -- - 3.05 89.20 28-Mar-2014 7.74 91.80 8.03 91.87 4.33 90.54 4.54 90.68 8.56 93.59 12.53 93.53 6.68 96.00 7.03 95.64 6.92 91.49 7.23 91.40 4.39 91.03 -- 1.85 90.40 27-Jun-2014 8.43 91.11 8.74 91.16 4.45 90.42 4.8 90.42 9.69 92.46 13.93 92.13 7.78 94.90 8.8 93.87 8.33 90.08 8.54 90.09 5.6 89.82 - 2.95 89.30 26-Sep-2014 7.82 91.72 8.20 91.70 3.91 90.96 4.28 90.94 8.62 93.53 13.81 92.25 6.68 96.00 7.33 95.34 7.1 91.31 7.36 91.27 4.4 91.02 1.95 90.30 17-Dec-2014 7.88 91.66 8.30 91.60 4.22 90.65 4.53 90.69 9.01 93.14 13.71 92.35 7.94 94.74 7.46 95.21 7.24 91.17 7.4 91.23 4.34 91.08 - 2.1 90.15 28-Jun-2018 9.36 90.18 9.55 90.35 4.56 90.31 4.96 90.26 10.35 91.80 11.65 94.41 Abandoned 2015 Abandoned 2015 8.68 89.73 9.12 89.51 5.86 89.56 6.84 91.96 10.52 88.05 22-Jan-2019 8.68 90.86 9.14 90.76 3.8 91.07 4.55 90.67 9.71 92.44 11.24 94.82 Abandoned 2015 Abandoned 2015 7.78 90.63 7.93 90.70 4.93 90.49 6.59 92.21 5.75 92.82 -- 17-Jun-2019 8.90 90.64 10.16 89.74 4.06 90.81 4.56 90.66 10.54 91.61 11.96 94.10 Abandoned 2015 Abandoned 2015 8.19 90.22 8.55 90.08 5.35 90.07 6.98 91.82 8.95 89.62 -- 9-Mar-2020 8.66 90.88 8.99 90.91 3.95 90.92 4.45 90.77 9.74 92.41 11.26 94.80 Abandoned 2015 Abandoned 2015 7.79 90.62 8.08 90.55 4.61 90.81 5.81 92.99 6.01 92.56 -- 9-Nov-2020 8.65 90.89 8.80 91.10 3.73 91.14 4.27 90.95 9.98 92.17 11.56 94.50 Abandoned 2015 Abandoned 2015 7.8 90.61 8.2 90.43 4.89 90.53 5.7 93.10 6.03 92.54 -- -- 25-Mar-2021 8.52 91.02 8.82 91.08 3.8 91.07 4.35 90.87 9.61 92.54 11.3 94.76 Abandoned 2015 Abandoned 2015 7.61 90.80 7.5 91.13 NM NM 5.88 92.92 5.28 93.29 - 1-Nov-2021 8.77 90.77 9.44 90.46 4.21 90.66 4.72 90.50 10.91 91.24 12.94 93.12 Abandoned 2015 Abandoned 2015 8.52 89.89 8.7 89.93 5.36 90.06 7.31 91.49 7.35 91.22 -- NE - Not Established -- = Not Measured BTOC = Below Top of Casing BGL - Below ground level ft MSL = feet above Mean Sea Level TOC Stickup data per Sherrill Environmental, Assessment Montoring Report , Feb 10, 2015 10-7-20 Note: Historical GW elevation values corrected for MW-3 RJRTIDRAFT Swift Creek Tables 2021 11.xisxl2. GW Elevations TABLE 3 GROUNDWATER AND SURFACE WATER ANALYTICAL EVENT RESULTS SWIFT CREEK STRUCTURAL FILL - CCB0057 BATTLEBORO, NORTH CAROLINA Page 1 of 1 Sample Location / ID Date D CD W n a s o o °' a m Z cn m Cn `< cn 0 En Cn ccnn ° o a m NC 2L Groundwater Standard 0.01 0.7 0.002 0.01 0.015 0.001 0.02 0.02 250 500 NC 213 Surface Water Standard 0.15 NE h h 0.025 0.000012 0.005 0.00006 NE NE GROUNDWATER MONITORING WELLS MW-1S 11/1/21 <0.015 <0.025 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 380 6,800 FD-01 (MW-1S) 11/1/21 <0.015 0.27 <0.005 <0.01 0.031 <0.0002 <0.02 <0.01 410 7,000 MW-1D 11/1/21 <0.015 0.027 <0.005 <0.01 <0.010 <0.0002 <0.02 <0.01 16 720 MW-2S 11/1/21 <0.015 0.2 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 <1.0 360 MW-2D 11/1/21 <0.015 0.066 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 1.1 320 MW-3 11/2/21 <0.015 <0.025 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 810 2,700 MW-4 11/2/21 0.025 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 25 230 MW-5RS 11/1/21 <0.015 <0.025 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 2.8 300 MW-5RD 11/1/21 <0.01 <0.025 <0.005 <0.01 <0.01 <0.0002 <0.01 <0.01 6.0 190 MW-6 11/2/21 <0.015 <0.025 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 7,509 MW-7 11/1/21 0.0901 0.13 <0.005 <0.01 <0.0002 <0.02 <0.01 700 10,000 MW-8 11/1/21 0.070 0.089 <0.005 <0.01 0.24 <0.0002 <0.02 <0.01 610 7,300 SURFACE WATER SW-01 11/1/21 <0.01b 0.027 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 2.3 75 SW-02 11/1/21 <0.015 0.048 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 5.3 110 SW-03 11/1/21 <0.015 0.026 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 9.3 82 All concentrations in milligrams per liter (mg/L) unless otherwise noted. --- Not sampled NE - Not established Bold with gray background indicates exceedance of NC Groundwater or Surface Water Standai h = hardness dependent dissolved metal standard DRAFT Swift Creek Tables 2021 11.xlsx/Table 3-Event Data 2021-11 TABLE 4 GROUNDWATER AND SURFACE WATER FIELD PARAMETER RESULTS SWIFT CREEK STRUCTURAL FILL - CCB0057 BATTLEBORO, NORTH CAROLINA Page 1 of 1 Sample Location / ID Date = 3 nCQD m `�-° v v � 3 5 o3c n c a o ? A O of as < 0 p X o cn < v CDa INC 2L Groundwater Standard 6.5 - 8.5 NE NE NE NE NE NC 2B Surface Water Standard 6.0 - 9.0 NE NE 50 NE >5.0 GROUNDWATER MONITORING WELLS MW-1S 11/1/21 5.8 20.2 10,278 4.5 -27 0.31 MW-1D 11/1/21 7.0 20.4 1,205 1.0 -41 0.97 MW-2S 11/1/21 6.9 18.8 684 25.1 -106 0.30 MW-213 11/1/21 7.2 18.3 478 2.6 -91 0.34 MW-3 11/2/21 5.4 19.5 3,831 6.0 48 0.39 MW-4 11/2/21 6.4 22 320 5.9 14 0.29 MW-5RS 11/1/21 7.0 22.8 450 3.1 24 0.47 MW-5RD 11/1/21 7.4 21.6 321 1.5 -45 1.05 MW-6 11/2/21 3.7 20.2 9,522 0.3 231 0.30 MW-7 11/1/21 3.7 20.9 15,392 3.9 205 0.27 MW-8 11/1/21 3.9 19.5 12,230 8.8 235 0.29 SURFACE WATER SW-01 11/1/21 7.3 14.4 77 14 35 8.16 SW-02 11/1/21 6.7 17.1 185 7 -9 2.48 SW-03 11/1/21 6.5 20.7 173 7 35 3.14 NE - Not established NM - Not measured Bold value exceeds applicable pH standard DRAFT Swift Creek Tables 2021 11.xlsx/Table 4-Field Parameters2021-11 WATER QUALITY MONITORING REPORT— NOVEMBER 2021 APPENDIX A HISTORICAL GROUNDWATER AND SURFACE WATER RESULTS November 2021 www.erm.com Version: 1.0 Project No.: 0397281 Client: ReUse Technology January 19, 2022 P:\Projects\0397281 ReUse CAP Implementation Swift Cr.DW\Post Closure Monitoring\2021-11 GWS\Swift Creek Water Quality Monitoring Report DRAFT TW_bpw.docx APPENDIX Al GROUNDWATER ANALYTICAL RESULTS SUMMARY SWIFT CREEK STRUCTURAL FILL - CCB0057 BATTLEBORO, NORTH CAROLINA Sample Location / ID Date D 0' oo °' C' 3 0- D C' D o o C' v 3 r O Q S C 3 C' cn <' mCD cn c N o v ° m 0_ C -O = Q cc m m C' v i3 _ 0 o CL n <' 3 �' Zc 6 Q Z, �' O CD in CD m 3 -'. p' < x0( < 0 (c c0 < r CD Q NC 2L Ground Water Standard (mg/1) 0.01 0.7 0.002 1 0.01 0.015 0.001 0.02 1 0.02 250 500 6.5 - 8.5 NE NE NE NE NE Ju1-04 0.028 0.19 <0.001 <0.01 0.068 <0.0002 <0.01 <0.01 490 MW-IS Dec-05 0.02 0.17 <0.001 <0.01 0.042 <0.0002 <0.01 <0.01 608 Oct-06 0.012 0.472 <0.001 <0.01 0.052 0.00064 <0.01 <0.01 740 May-07 <0.01 0.458 <0.001 <0.01 <0.010 0.00047 <0.01 <0.01 420 Nov-07 <0.01 0.529 <0.001 <0.01 0.031 0.00089 <0.01 <0.01 520 Jun-08 <0.01 0.619 <0.001 <0.01 0.011 0.00051 <0.01 <0.01 470 Jan-09 <0.01 0.416 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 210 Jun-09 <0.01 0.412 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 220 Dec-09 <0.01 0.256 0.001 <0.01 <0.010 <0.0002 0.022 <0.01 160 Jun-10 0.012 0.691 0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 280 Dec-10 <0.01 0.599 0.003 <0.01 <0.010 <0.0002 <0.01 <0.01 400 Jun-11 <0.10 0.475 <0.01 <0.10 <0.10 <0.00028 <0.10 <0.10 590 Dec-11 <0.050 0.422 <0.005 <0.050 <0.050 <0.0002 <0.050 <0.050 170 Jun-12 <0.01 0.419 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 150 Dec-12 0.018 0.567 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 180 Jun-13 <0.01 0.174 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 75 Dec-13 <0.01 0.163 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 99 Jun-14 <0.01 0.25 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 110 Dec-14 <0.01 0.408 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 310 Jun-18 <0.015 0.24 <0.005 <0.030 <0.01 <0.0002 <0.02 <0.01 320 8,100 5.8 27.0 14,679 5 47 0.18 Jan-19 <0.015 0.27 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 270 4,700 6.0 6.4 4,305 7 4 0.53 Jun-19 <0.015 0.28 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 320 7,400 5.8 21.4 11,617 9 -51 0.19 Mar-20 <0.015 0.22 <0.005 <0.01 L 0.03 <0.0002 <0.02 <0.01 480 8,500 6.0 17.0 14,566 5 2 0.25 Nov-20 <0.015 0.26 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 400 8,500 5.6 23.8 8,023 2 -116 0.43 Mar-21 <0.015 0.23 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 430 6,200 6.1 16.1 10,125 8 -80 0.41 Duplicate (FD-01) Mar-21 <0.015 0.22 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 430 6,100 -- -- -- Nov-21 <0.015 <0.025 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 380 6,800 5.8 20.2 10,278 4.5 -27 0.31 Duplicate (FD-01) Nov-21 <0.015 0.27 <0.005 <0.01 0.031 <0.0002 <0.02 <0.01 410 7,000 -- - -- Jul-04 <0.01 0.54 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 13 MW-1D <0.01 <0.01 7.7 Page 1 of 9 DRAFT Swift Creek Tables 2021 11.xlsx/Table A1-Historic Groundwater APPENDIX Al GROUNDWATER ANALYTICAL RESULTS SUMMARY SWIFT CREEK STRUCTURAL FILL - CCB0057 BATTLEBORO, NORTH CAROLINA o Q v cc _ 0 O CD D oo 0- o cn ° m o CL Z c m'C-o Sample °' D o r S 3 cn c m m 6 m x0( < 0 Location / ID Date C' 3 C' D C' v 3 O Q C C' <' mCD N 0_ -O = C' v i3 n <' 3 �' Q v �' 3 -'. p' < (c c0 < r CD Q 0' C NC 2L Ground Water Standard (mg/1) 0.01 0.7 0.002 0.01 0.015 0.001 0.02 0.02 250 500 6.5 - 8.5 NE NE NE NE NE Oct-06 <0.01 0.341 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 20 May-07 <0.01 0.343 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 12 Oct-07 <0.01 0.365 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 11 Jun-08 <0.01 0.334 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 14 Jan-08 <0.01 0.356 NR NR <0.010 <0.0002 NR NR 14 Jun-09 <0.01 0.403 NR NR <0.010 <0.0002 NR NR 20 Jun-18 <0.01 0.66 <0.005 <0.01 <0.010 <0.0002 <0.02 <0.01 19 8,200 6.9 25.6 1,221 3 -93 0.18 Jan-19 <0.01 0.67 <0.005 <0.01 <0.010 <0.0002 <0.02 <0.01 17 750 6.9 8.9 1,165 7 -46 0.85 Jun-19 <0.01 0.66 <0.005 <0.01 <0.010 <0.0002 <0.02 <0.01 13 800 6.8 22.4 1,374 11 -56 0.23 Mar-20 <0.01 0.67 <0.005 <0.01 <0.010 <0.0002 <0.02 <0.01 13 730 7.0 18.2 1,344 9 11 1.97 Nov-20 <0.01 0.6 <0.005 <0.01 <0.010 <0.0002 <0.02 <0.01 16 810 6.9 24.4 1,304 2 -68 0.40 Mar-21 <0.01 0.59 <0.005 <0.01 <0.010 <0.0002 <0.02 <0.01 15 780 7.1 20.9 1,229 10 94 1.78 Nov-21 <0.015 0.027 <0.005 <0.01 <0.010 <0.0002 <0.02 <0.01 16 720 7.0 20.4 1,205 1 -41 0.97 Jun-04 <0.01 <0.10 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 32 MW-2S Dec-05 <0.01 0.18 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 10.1 Oct-06 <0.01 0.198 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 May-07 <0.01 0.232 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 4.4 Oct-07 <0.01 0.256 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 3.6 Jun-08 <0.01 0.103 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 4.4 Jan-09 <0.01 0.164 NR NR <0.010 <0.0002 NR NR <5 Jun-09 <0.01 0.173 NR NR <0.010 <0.0002 NR NR <5 Dec-09 <0.01 0.218 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 <5 Jun-10 <0.01 0.229 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 <5 Dec-10 <0.01 0.235 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 <5 Jun-11 <0.01 0.182 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 <5 Dec-11 <0.01 0.216 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 <5 Jun-12 <0.01 0.178 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 <5 Jun-13 <0.01 0.21 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 Dec-13 I <0.01 1 0.199 <0.001 I <0.01 I <0.01 1 <0.0002 <0.01 I <0.01 1 <5 Page 2of9 DRAFT Swift Creek Tables 2021 11.xlsx/Table A1-Historic Groundwater APPENDIX Al GROUNDWATER ANALYTICAL RESULTS SUMMARY SWIFT CREEK STRUCTURAL FILL - CCB0057 BATTLEBORO, NORTH CAROLINA o Q v cc _ 0 O CD D oo 0- o cn ° m o CL Z c m'C-o Sample °' 3 0 r S 3 cn c m m 6 m x0( < 0 Location / ID Date 0' C' 3 C' 5 C' v 3 O Q C C' <' mCD N 0_ C -O = C' v i3 n <' 3 �' Q v �' 3 -'. p' < (c c0 < r CD Q NC 2L Ground Water Standard (mg/1) 0.01 0.7 0.002 0.01 0.015 0.001 0.02 0.02 250 500 6.5 - 8.5 NE NE NE NE NE Jun-14 <0.01 0.165 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 Dec-14 <0.01 0.2 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 Jun-18 <0.015 0.13 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 <1 790 6.3 21.0 448 0 -36 0.18 Jan-19 <0.015 0.21 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 <1 400 6.9 10.0 611 5 -124 0.55 Jun-19 <0.015 0.24 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 <1 430 7.0 20.8 641 2 -152 0.18 Mar-20 <0.015 0.28 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 <1 400 6.9 16.8 759 4 -146 0.36 Nov-20 <0.015 0.24 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 <1 400 6.3 21.3 732 15 -120 0.34 Mar-21 <0.015 0.23 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 <1 340 6.6 16.7 615 2 -101 0.20 Nov-21 <0.015 0.20 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 <1.0 360 6.9 18.8 684 25 -106 0.30 M W -2 D Jun-04 <0.01 0.17 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 5.6 Dec-05 <0.01 0.3 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 3.1 Oct-06 <0.01 0.29 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 11 May-07 <0.01 0.254 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 2.9 Oct-07 <0.01 0.273 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 4.8 Jun-08 <0.01 0.265 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 22 Jan-09 <0.01 0.253 NR NR <0.010 <0.0002 NR NR 16 Jun-09 <0.01 0.289 NR NR <0.010 <0.0002 NR NR 6.3 Jun-18 <0.015 0.13 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 <1 790 7.1 25.0 444 10 18 1.30 Jan-19 <0.015 0.30 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 1.5 310 7.2 9.7 474 5 -94 880.38 Jun-19 <0.015 0.29 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 <1 330 7.3 20.0 501 10 -63 0.27 Mar-20 <0.015 0.29 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 <1 300 7.1 19.4 540 2 75 0.52 Nov-20 <0.015 0.27 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 1.3 300 7.1 22.0 529 3 -86 0.34 Mar-21 <0.015 0.27 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 <1 300 7.3 20.4 538 2 -84 0.61 Nov-21 <0.015 0.07 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 1.1 320 7.2 18.3 478 3 -91 0.34 Dec-05 <0.01 <0.0002 <0.01 <0.01 334 MW-3 Oct-06 <0.01 0.192 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 580 May-07 <0.01 0.342 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 570 Nov-07 <0.01 0.133 <0.001 <0.01 0.036 <0.0002 <0.01 <0.01 380 Page 3 of 9 DRAFT Swift Creek Tables 2021 11.xlsx/Table A1-Historic Groundwater APPENDIX Al GROUNDWATER ANALYTICAL RESULTS SUMMARY SWIFT CREEK STRUCTURAL FILL - CCB0057 BATTLEBORO, NORTH CAROLINA Sample Location / ID Date D 0' oo °' C' 3 0- D C' D o o C' v 3 r O Q S C 3 C' cn <' mCD cn c N o v ° m 0_ C -O = Q cc m m C' v i3 _ 0 o CL n <' 3 �' Z c 6 Q v �' O CD m'C-o m 3 -'. p' < x0( < 0 (c c0 < r CD Q NC 2L Ground Water Standard (mg/1) 0.01 0.7 0.002 1 0.01 0.015 0.001 0.02 1 0.02 250 500 6.5 - 8.5 NE NE NE NE NE Jun-08 <0.01 0.145 <0.001 <0.01 0.022 <0.0002 <0.01 <0.01 370 Jan-09 <0.01 0.144 <0.001 <0.01 0.013 <0.0002 <0.01 <0.01 550 Jun-09 <0.01 0.202 <0.001 <0.01 0.081 <0.0002 <0.01 <0.01 570 Dec-09 0.012 0.192 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 710 Jun-10 0.011 0.094 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 840 Dec-10 <0.01 0.125 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 690 Jun-11 <0.10 0.119 <0.01 <0.10 <0.10 <0.0002 <0.10 <0.10 790 Dec-11 <0.01 0.234 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 410 Jun-12 <0.01 0.125 <0.001 <0.01 <0.01 <0.0002 <0.05 <0.01 1,000 Dec-12 0.013 0.136 <0.001 <0.01 <0.01 <0.0002 0.011 <0.01 910 Jun-13 <0.10d 0.201 <0.01 d <0.1 d <0.1 d <0.0002 <0.1 d <0.1 d 950 Dec-13 <0.050d 0.162 <0.005d <0.05d <0.05d <0.0002 <0.05d <0.05d 890 Jun-14 <0.027d 0.116 <0.002d <0.07d <0.01d <0.0002 <0.025d <0.07d 970 Dec-14 <0.050d 0.151 <0.005d <0.05d <0.05d <0.0002 <0.05d <0.05d 760 Jun-18 <0.015 0.066 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 980 830 5.5 27.2 7,611 9 60 0.30 Jan-19 <0.015 0.088 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 930 130 -- 4.4 5,256 11 679 369.94 Jun-19 <0.015 0.072 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 1,000 4,400 5.2 22.9 6,520 10 -39 0.20 Mar-20 <0.015 0.044 <0.005 <0.01 0.014 <0.0002 <0.02 <0.01 580 1,600 5.6 16.0 2,456 10.8 -49 0.63 Nov-20 <0.015 0.049 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 710 25,000 5.2 18.9 2,921 6.3 66 0.20 Duplicate (FD-01) Nov-20 <0.015 0.26 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 370 6,400 -- -- -- - -- Mar-21 <0.015 0.038 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 240 830 6.0 17.5 1,357 19.8 57 0.38 Nov-21 <0.015 <0.025 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 810 2,700 5.4 19.5 3,831 6.0 48 0.39 MW-4 Dec-05 <0.01 0.46 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 5.7 Oct-06 <0.01 0.171 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 May-07 <0.01 <0.100 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 8.6 Oct-07 <0.01 0.147 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 5.9 Jun-08 <0.01 0.198 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 5.4 Jan-09 <0.01 0.083 NR NR <0.010 <0.0002 NR NR 6.4 Jun-09 I <0.01 1 0.3491 NRI NRI <0.010 <0.00021 NRI NRI 7.7 Page 4of9 DRAFT Swift Creek Tables 2021 11.xlsx/Table A1-Historic Groundwater APPENDIX Al GROUNDWATER ANALYTICAL RESULTS SUMMARY SWIFT CREEK STRUCTURAL FILL - CCB0057 BATTLEBORO, NORTH CAROLINA o Q v cc _ 0 O CD D oo 0- o cn ° m o CL Z c m'C-o Sample °' 3 0 r S 3 cn c m m 6 m x0( < 0 Location / ID Date 0' C' 3 C' 5 C' v 3 O Q C C' <' mCD N 0_ C -O = C' v i3 n <' 3 �' Q v �' 3 -'. p' < (c c0 < r CD Q NC 2L Ground Water Standard (mg/1) 0.01 0.7 0.002 1 0.01 0.015 0.001 0.02 1 0.02 250 500 6.5 - 8.5 NE NE NE NE NE Dec-09 <0.01 0.121 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 7.5 Jun-10 <0.01 0.181 <0.001 0.018 <0.010 0.0006 <0.01 <0.01 15 Dec-10 0.016 0.195 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 16 Jun-11 <0.01 0.227 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 28 Dec-11 <0.01 0.516 0.003 <0.01 0.021 <0.0002 <0.01 <0.01 51 Jun-12 <0.01 0.356 0.008 <0.01 0.032 <0.0002 <0.01 <0.01 100 Jun-13 <0.01 0.109 0.004 <0.01 0.021 0.00078 <0.01 <0.01 250 Dec-13 <0.01 0.167 0.006 <0.01 <0.010 <0.0002 <0.01 <0.01 130 Jul-14 <0.01 0.085 0.0017 <0.01 <0.010 0.00101 <0.01 <0.01 190 Dec-14 <0.01 0.071 0.0017 <0.01 <0.010 0.00111 <0.01 <0.01 260 Jun-18 <0.01 0.041 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 66 450 6.4 25.1 72 7 56 0.28 Jan-19 <0.01 0.044 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 46 320 6.7 9.3 499 13 52 0.83 Jun-19 <0.01 0.052 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 30 310 6.9 22.0 553 7 -91 0.47 Mar-20 <0.01 0.054 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 37 <25 6.5 16.0 455 5 -51 0.42 Nov-20 <0.01 0.061 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 29 250 6.3 43.0 442 10 43 0.52 Mar-21 <0.01 0.059 <0.005 0.14 <0.01 <0.0002 <0.02 <0.01 17 200 6.4 16.9 345 22 9 0.26 Nov-21 0.035 0.025 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 25 230 6.4 21.9 320 6 14 0.29 Dec-05 <0.01 0.45 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 6.1 MW-5S Oct-06 <0.01 0.121 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 7 May-07 <0.01 0.218 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 4.7 Oct-07 <0.01 0.278 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 4.9 Jun-08 <0.01 0.046 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 8.7 Jan-09 <0.01 0.051 NR NR <0.010 <0.0002 NR NR 10 Jun-09 <0.01 0.058 NR NR <0.010 <0.0002 NR NR 13 Dec-09 <0.01 0.056 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 17 Jun-10 <0.01 0.057 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 12 Dec-10 <0.01 0.102 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 14 Jun-11 <0.01 0.064 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 17 Dec-11 <0.01 0.087 <0.001 <0.01 <0.010 <0.0002 <0.01 I <0.01 1 21 Page 5of9 DRAFT Swift Creek Tables 2021 11.xlsx/Table A1-Historic Groundwater APPENDIX Al GROUNDWATER ANALYTICAL RESULTS SUMMARY SWIFT CREEK STRUCTURAL FILL - CCB0057 BATTLEBORO, NORTH CAROLINA Sample Location / ID Date D 0' oo °' C' 3 0- 3 C' 5 o 0 C' v 3 r O Q S C 3 C' cn <' mCD cn c N o v ° m 0_ C -O = Q cc m m C' v i3 _ 0 o CL n <' 3 �' Z c 6 Q v �' O CD m'C- 3 -'. < o m p' x0( < 0 (c c0 < r CD Q NC 2L Ground Water Standard (mg/1) 1 0.01 0.7 0.002 0.01 0.015 0.001 0.02 0.02 250 500 6.5 - 8.5 NE NE NE NE NE Jun-12 <0.01 0.095 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 22 Dec-12 <0.01 0.131 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 25 Jun-13 <0.01 0.025 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 22 Dec-13 <0.01 0.088 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 21 Jun-14 <0.01 0.052 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 14 Dec-14 <0.01 0.082 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 21 Monitor Well Abandoned on 4/17/15 by NCDOT and replaced on 6/11/18 by MW-5RS MW-5RS Jun-18 <0.015 0.098 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 12 420 6.9 23.9 454 7 45 3.37 Jan-19 <0.015 0.10 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 3.4 260 6.6 12.6 382 2 78 0.99 Jun-19 <0.015 0.11 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 <1.0 320 7.0 25.3 594 9 -106 0.17 Mar-20 <0.015 0.09 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 3.1 230 6.6 16.4 363 4 -13 1.10 Nov-20 <0.015 0.10 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 3.1 290 7.0 22.0 477 1 -17 0.32 Mar-21 <0.015 0.07 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 2.3 210 6.4 18.2 297 3 143 0.69 Nov-21 <0.015 <0.025 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 2.8 300 7.0 22.8 450 3 24 0.47 Dec-05 <0.01 0.17 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 8.1 MW-513 Oct-06 <0.01 0.236 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 6 May-07 <0.01 0.227 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 5.8 Oct-07 <0.01 0.258 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 6.6 Jun-08 <0.01 0.254 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 10 Jan-09 <0.01 0.255 NR NR <0.010 <0.0002 NR NR 10 Jun-09 <0.01 0.261 NR NR <0.010 <0.0002 NR NR 17 Monitor Well Abandoned on 4/17/15 by NCDOT and replaced on 6/11/18 by MW-5RD MW-5RD Jun-18 <0.01 0.15 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 26 230 7.3 23.0 327 20 29 0.12 Jan-19 <0.01 0.22 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 17 230 7.4 11.9 374 10 -125 730.47 Jun-19 <0.01 0.21 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 14 250 7.3 24.0 388 9 -94 0.21 Mar-20 <0.01 0.25 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 11 240 7.3 16.2 383 4 -1 2.09 Nov-20 I <0.01 1 0.22 <0.001 I <0.01 I <0.01 1 <0.0002 <0.01 I <0.01 1 7.91 2401 7.31 21.51 3841 10 -1201 0.67 Page 6of9 DRAFT Swift Creek Tables 2021 11.xlsx/Table A1-Historic Groundwater APPENDIX Al GROUNDWATER ANALYTICAL RESULTS SUMMARY SWIFT CREEK STRUCTURAL FILL - CCB0057 BATTLEBORO, NORTH CAROLINA o Q v cc _ 0 O CD D oo Q o cn m(D o� Z c m' CL O o Sample °' 3 0 r S 3 cn m F E 6 m E ,< O Location / ID Date c' �' c' °' m Q �' 5 <' m m n = �' v m <' 3 �' v �' < 0 cQ < r(D Q � NC 2L Ground Water Standard (mg/1) 0.01 0.7 0.002 0.01 0.015 1 0.001 0.02 1 0.02 250 500 6.5 - 8.5 NE NE NE NE NE Mar-21 <0.01 0.096 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 4.7 140 7.4 18.6 265 4 136 1.77 Nov-21 <0.01 <0.025 <0.005 <0.01 <0.01 <0.0002 <0.01 <0.01 6.0 190 7.4 21.6 321 1 -45 1.05 Dec-05 <0.01 1.3 <0.001 <0.01 0.01 <0.0002 <0.01 <0.01 174 MW-6 Oct-06 <0.01 0.816 <0.001 <0.01 0.013 <0.0002 <0.01 <0.01 510 May-07 <0.01 0.312 <0.001 <0.01 0.032 <0.0002 <0.01 <0.01 220 Nov-07 <0.01 0.12 <0.001 <0.01 0.074 0.00026 <0.01 <0.01 290 Jun-08 <0.01 0.08 <0.001 <0.01 0.054 0.00091 <0.01 <0.01 490 Jan-09 <0.01 0.066 NR NR 0.014 <0.0002 NR NR 560 Jun-09 0.018 0.155 NR NR 0.016 0.00026 NR NR 430 Dec-09 0.014 0.126 <0.001 <0.01 0.01 <0.0002 <0.01 <0.01 220 Jun-10 0.109 0.313 <0.001 <0.01 0.155 0.0003 <0.01 <0.01 300 Dec-10 0.018 0.138 <0.001 <0.01 <0.010 <0.0002 <0.01 <0.01 350 Jun-11 <0.10 0.717 <0.01 <0.10 <0.10 0.00095 <0.10 <0.10 460 Dec-11 <0.01 0.148 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 260 Jun-12 <0.05 0.156 <0.001 <0.01 <0.01 <0.0002 <0.05 <0.01 330 Dec-12 0.031 0.131 <0.001 <0.01 <0.01 <0.0002 0.012 <0.01 270 Jun-13 <0.01 0.152 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 270 Dec-13 <0.05d 0.247 <0.005d <0.05d <0.05d <0.0002 <0.05d <0.05d 300 Jun-14 0.0189 0.193 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 260 Dec-14 0.099 0.155 <0.005d <0.05d 0.122 <0.0002 <0.05d <0.05d 660 Jun-18 0.043 0.047 <0.005 <0.01 0.045 <0.0002 <0.02 <0.01 1,000 6,300 3.9 25.3 9,665 0 196 0.78 Jan-19 0.039 0.077 <0.005 <0.01 0.022 <0.0002 <0.02 <0.01 870 3,600 3.8 8.3 4,993 4 290 975.76 Jun-19 0.083 0.086 <0.005 <0.01 0.074 <0.0002 <0.02 <0.01 760 7,100 3.8 22.0 11,164 5 45 0.20 Mar-20 0.073 0.11 <0.005 <0.01 0.160 <0.0002 <0.02 <0.01 740 7,000 3.7 16.6 11,118 2 246 0.28 Nov-20 0.066 0.078 <0.005 <0.01 0.085 <0.0002 <0.02 <0.01 820 7,700 3.5 23.0 9,811 1 294 0.20 Mar-21 0.055 0.075 <0.005 <0.01 0.052 <0.0002 <0.02 <0.01 600 5,800 3.8 17.6 8,772 1 105 0.26 Nov-21 5 <0.005 <0.01 <0.0002 <0.02 <0.01 790 5,500 3.7 20.2 9,522 0 231 0.30 Page 7 of 9 DRAFT Swift Creek Tables 2021 11.xlsx/Table A1-Historic Groundwater APPENDIX Al GROUNDWATER ANALYTICAL RESULTS SUMMARY SWIFT CREEK STRUCTURAL FILL - CCB0057 BATTLEBORO, NORTH CAROLINA o Q CD v cc (D _ 0 3 O CD j. D oo N Q o (D m cn ° (') -O m m Q o c Zc CD XX m QQ O� Sample °' 3 0 r cn c CD m S 0 m o Location / ID Date M. c) C C 3 C" ° CD n C C 3 <. N �- -6 = C" C V n< 3 Q m 3 -� �' <� cQ < r 3 Q NC 2L Ground Water Standard (mg/1) 0.01 0.7 0.002 0.01 0.015 0.001 0.02 1 0.02 250 500 6.5 - 8.5 NE NE NE NE NE Dec-05 0.038 <0. <0.001 <0.01 0.093 <0.01 <0.01 379 MW-7 Oct-06 0.03 0.059 <0.001 <0.01 0.053 <0.01 <0.01 500 May-07 0.017 <0.1' <0.001 <0.01 0.047 0.0003 <0.01 <0.01 460 Nov-07 0.029 <0.001 <0.01 0.124 0.00072 <0.01 <0.01 250 Jun-08 0.019 0.042 <0.001 <0.01 0.072 <0.0002 <0.01 <0.01 420 Jan-09 0.022 0.052 <0.001 <0.01 0.088 <0.0002 <0.01 <0.01 500 Jun-09 0.072 0.08 <0.001 <0.01 0.171 <0.0002 <0.01 <0.01 500 Dec-09 0.128 0.123 <0.01 <0.01 0.273 0.0006 <0.10 <0.10 490 Jun-10 0.208 0.172 <0.01 <0.01 0.379 0.0002 <0.10 <0.10 530 Dec-10 0.23 0.255 <0.01 <0.01 0.649 0.00057 <0.10 <0.10 590 Jun-11 0.134 0.159 <0.01 <0.10 0.396 0.00033 <0.10 <0.10 540 Dec-11 0.107 0.172 <0.01 <0.10 0.468 <0.0002 <0.10 <0.10 640 Jun-12 0.059 0.12 <0.005 <0.05 0.27 <0.0002 <0.05 <0.05 580 Dec-12 <0. I U0d 0.158 <0.01 <0.10 0.397 <0.0002 <0.10 <0.10 700 Jun-13 <0.100d 0.114 <0.01d <0.10d 0.19 <0.0002 <0.10d <0.10d 600 Dec-13 0.07 0.119 <0.05d <0.050d 0.235 <0.0002 <0.050d <0.050d 470 Jun-14 0.078 0.093 <0.002d <0.007d 0.139 <0.0002 <0.025d <0.010d 670 Dec-14 0.167 0.205 <n nFri <0.050d 0.553 <0.0002 <0.050d <0.050d 710 Jun-18 0.041 0.1 0.0074 <0.02 0.089 <0.0002 <0.02 <0.01 770 9,400 3.8 23.0 13,584 2 243 1.37 Jan-19 0.089 0.097 <0.005 <0.01 0.190 <0.0002 <0.02 <0.01 920 8,100 3.8 8.1 10,375 2 250 0.97 Jun-19 0.077 0.16 0.012 <0.01 0.160 <0.0002 <0.02 <0.01 630 10,000 3.7 21.5 15,916 9 128 0.31 Mar-20 0.093 0.13 0.012 <0.01 0.260 <0.0002 <0.02 <0.01 770 10,000 4.0 12.0 16,317 5 193 0.41 Nov-20 0.089 0.14 005 <0.01 0.260 <0.0002 <0.02 <0.01 640 12,000 3.5 20.9 16,203 3 259 0.24 Mar-21 0.080 0.092 <0.005 <0.01 0.160 <0.0002 <0.02 <0.01 670 8,000 3.8 16.0 12,734 8 186 0.25 Nov-21 0.090 0.13 <0.005 <0.01 0.270 <0.0002 <0.02 <0.01 700 10,000 3.7 20.9 15,392 4 205 0.27 MW-8 May-07 0.025 <0.001 <0.01 0.024 <0.0002 <0.01 <0.01 400 Nov-07 0.03 <0.001 <0.01 0.038 <0.0002 <0.01 <0.01 430 Jun-08 0.031 0.048 <0.001 <0.01 0.027 <0.0002 <0.01 <0.01 300 Jan-09 0.028 0.039 NRI NR 0.032 <0.00021 NRI NR 350 Page 8of9 DRAFT Swift Creek Tables 2021 11.xlsx/Table A1-Historic Groundwater APPENDIX Al GROUNDWATER ANALYTICAL RESULTS SUMMARY SWIFT CREEK STRUCTURAL FILL - CCB0057 BATTLEBORO, NORTH CAROLINA Sample Location / ID Date D 0' oo °' C' 3 0- 3 C' 5 o 0 C' v 3 r O Q S C 3 C' cn <' mCD cn c N o v ° m 0_ C -O = Q cc m m C' v i3 _ 0 CL o n <' 3 �' Z c 6 Q Z, �' O CD in' C- o m 3 -'. p' < x0 < 0 (c c0 < r CD Q NC 2L Ground Water Standard (mg/1) 0.01 0.7 0.002 0.01 0.015 0.001 0.02 0.02 250 500 6.5 - 8.5 NE NE NE NE NE Jun-09 0.159 0.114 NR NR 0.173 0.0003 NR NR 460 Dec-09 0.569 0.286j <0.016 <0.050 0.376j 0.0002 <0.135 <0.095 460 Jun-10 0.366 0.232 <0.016 <0.050 0.283 0.0002 <0.135 <0.095 500 Dec-10 0.267 0.243 <0.01 <0.100 0.369 0.0013 <0.100 <0.100 470 Jun-11 0.207 0.223 <0.01 <0.100 0.103 <0.0002 <0.100 <0.100 410 Dec-11 0.321 <0.01 <0.100 <0.0002 <0.100 <0.100 270 Jun-12 0.146 0.169 <0.005 <0.05 0.199 <0.0002 <0.05 <0.05 580 Dec-12 0.11 0.168 <0.01 <0.100 0.234 <0.0002 <0.10 <0.10 580 Jun-13 0.14 0.172 <0.01d <0.100d 0.169 <0.0002 <0.10d <0.10d 620 Dec-13 0.126 0.177 <0.05d <0.050d 0.211 <0.0002 <0.050d <0.050d 510 Jun-14 0.154 0.13 <0.002d <0.007d 0.168 <0.0002 <0.025d <0.010d 700 Dec-14 0.124 0.143 <0.05d <0.050d 0.263 <0.0002 <0.050d <0.050d 620 Jun-18 0.055 0.056 <0.005 <0.02 0.10 <0.0002 <0.02 <0.01 1,000 8,400 3.9 19.0 11,539 0 125 0.69 Jan-19 0.1 0.093 <0.005 <0.01 0.100 <0.0002 <0.02 <0.01 870 7,800 3.8 9.2 11,013 5 216 0.64 Jun-19 0.092 0.092 <0.005 <0.01 0.190 <0.0002 <0.02 <0.01 780 9,900 3.9 20.5 14,721 2 92 0.33 Mar-20 0.09 0.1 <0.005 <0.01 0.150 <0.0002 <0.02 <0.01 710 8,100 3.9 13.3 13,074 38 251 0.76 Nov-20 0.078 0.092 <0.005 <0.01 0.230 <0.0002 <0.02 <0.01 660 16,000 3.4 20.4 13,803 5 204 0.59 Mar-21 Monitor well unable to be sampled due to biological hazel Nov-21 1 0.071 0.089 <0.005 <0.01 1 0.240 <0.0002 <0.02 <0.01 1 610 7,3001 3.9 19.51 12,230 91 2351 0.29 All concentrations in milligrams per liter (mg/L) unless otherwise noted NE - Not established -- - Not sampled Bold with gray background indicates exceedance of NC 2L Groundwater Standard Page 9of9 DRAFT Swift Creek Tables 2021 11.xlsx/Table A1-Historic Groundwater APPENDIX A2 SURFACE WATER ANALYTICAL RESULTS SUMMARY SWIFT CREEK STRUCTURAL FILL - CCB0057 BATTLEBORO, NORTH CAROLINA O xQ O Q (D 0). N O O (D (7 7 < D W a o CD cn n m o c c v' 0. O Sample m °' 3 o r CD - �_ C o m y � LT Location / ID Date ' 3 v C °n) m V ` m o m NC 2B Surface Water Standard - Class C (ug/1) 0.15 1 NE 1 0.002 h 0.05 h 0.025 1 0.0000121 0.005 1 0.00006 1 NE I NE 1 6.0 - 9.0 1 NE I NE 1 50 1 NE 1 >5.0 04/03/03 <0.01 <0.10 <0.001 <0.01 <0.005 <0.0002 <0.01 <0.01 12 SW-01 06/22/04 <0.01 <0.10 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <2.0 12/01 /05 <0.01 <0.10 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 6.3 10/06/06 <0.01 <0.10 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 Surface Water - Upstream 05/04/07 <0.01 <0.10 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 6.6 10/22/07 <0.01 <0.10 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 3.8 06/18/08 <0.01 <0.10 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 2.5 01/14/09 <0.01 <0.10 NR NR <0.01 <0.0002 NR NR 5.6 06/24/09 <0.01 0.03 NR NR <0.01 <0.0002 NR NR <5 12/16/09 <0.01 0.048 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 6.2 06/30/10 <0.01 0.032 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 12/14/10 <0.01 0.025 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 06/27/11 <0.01 0.041 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 12/19/11 <0.01 0.025 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 12/18/12 <0.01 0.028 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 06/25/13 <0.01 0.04 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 04/13/12 <0.01 0.025 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 5.3 06/27/14 <0.01 0.03 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 12/17/14 <0.01 0.027 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 06/28/18 <0.015 0.031 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 <1 73 6.95 28.46 101 NM -2.5 4.2 01 /21 /19 <0.015 0.090 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 6.1 79 7.84 6.50 107 11.0 37.1 19.2 06/17/19 <0.015 0.058 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 1.7 110 8.21 27.00 91 139.0 -130.0 2.1 03/09/20 <0.015 0.046 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 3.4 110 6.65 13.00 176 14.4 -45.6 8.4 11 /09/20 <0.015 0.032 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 1.8 91 6.79 15.20 94 9.7 26.2 4.2 03/26/21 <0.015 0.031 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 2.0 66 6.68 19.20 92 39.0 126.5 6.5 11 /01 /21 <0.015 0.027 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 2.3 75 7.32 14.40 77 13.9 35.4 8.2 04/03/03 <0.01 <0.10 <0.001 <0.01 <0.005 <0.0002 <0.01 <0.01 12 SW-02 06/22/04 <0.01 <0.10 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <2.0 12/01 /05 <0.01 <0.10 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 6.3 10/06/06 <0.01 0.09 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 Surface Water - Downstream 05/04/07 <0.01 <0.10 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 6.6 10/22/07 DRY <0.0002 <0.01 <0.01 3.8 08/07/08 <0.01 <0.10 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 2.5 01/14/09 <0.01 <0.10 NR NR <0.01 <0.0002 NR NR 5.6 06/24/09 <0.01 0.088 NR NR <0.01 <0.0002 NR NR <5 12/16/09 <0.01 0.025 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 6.2 06/30/10 DRY <0.0002 <0.01 <0.01 <5 12/14/10 <0.01 0.034 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 06/27/11 DRY <0.0002 <0.01 <0.01 <5 12/19/11 <0.01 0.027 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 12/18/12 <0.01 0.031 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 06/25/13 <0.01 0.037 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 04/13/12 <0.01 0.023 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 5.3 06/27/14 <0.01 0.038 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 12/17/14 <0.01 0.027 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 06/28/18 <0.015 0.089 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 <1 130 6.98 29.68 369 90.0 -0.4 0.7 01 /21 /19 <0.01 0.027 <0.0002 <0.02 <0.01 <0.0002 <0.02 <0.01 7 100 5.81 3.60 171 6.6 139.6 14.2 06/17/19 <0.01 0.052 <0.0002 <0.02 <0.01 <0.0002 <0.02 <0.01 <1 150 5.76 26.10 225 23.4 44.2 1.6 03/09/20 <0.015 <0.025 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 4.9 98 6.94 13.40 166 5.2 -39.0 9.8 11 /09/20 <0.015 0.039 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 1.1 91 6.41 19.30 133 11.0 -72.0 13.0 03/25/21 <0.015 0.026 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 2.8 66 7.16 20.40 65 16.2 65.1 9.9 11 /09/20 <0.015 <0.025 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 2.5 67 6.8 18.3 325.3 11.4 63.4 3.78 11 /01 /21 <0.015 0.048 <0.005 <0.01 I <0.01 <0.0002 <0.02 <0.01 5.3 1101 6.71 17.11 184.51 6.98 -8.71 2.48 Page 1 of 2 DRAFT Swift Creek Tables 2021 11.xisx/Table A2-Historic SurfaceWater APPENDIX A2 SURFACE WATER ANALYTICAL RESULTS SUMMARY SWIFT CREEK STRUCTURAL FILL - CCB0057 BATTLEBORO, NORTH CAROLINA Sample Location / ID Date D m co °' c' Q 3 c' s o o B c' v 3 r Q - c Z m c' u) <' m (n v m 4 o a o - N a = Q m (D CD N� n(D m °' c' c V m _� o c <' 3 g c z 6 C n v O x) i v 17 ° �C iv' a 0 - < 0 O N. p <- 0. O cQ r NC 2B Surface Water Standard - Class C (ug/I) 0.15 1 NE 1 0.002 " 0.05 " 0.025 1 0.0000121 0.005 1 0.00006 1 NE I NE 1 6.0 - 9.0 1 NE I NE 1 50 1 NE 1 15.0 05/04/07 <0.01 <0.10 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 2.4 SW-03 10/22/07 DRY 06/18/08 <0.01 0.089 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 3.3 01/14/09 <0.01 <0.10 NR NR <0.01 <0.0002 NR NR 20 Surface Water - Downstream 06/24/09 <0.01 0.087 NR NR <0.01 <0.0002 NR NR <5 12/16/09 <0.01 0.075 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 14 06/30/10 <0.01 0.328 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 47 12/14/10 <0.01 0.074 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 16 06/27/11 DRY 12/19/11 <0.01 0.065 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 8 12/18/12 <0.01 0.067 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 6.5 06/25/13 <0.01 0.087 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 7.4 04/13/12 <0.01 0.051 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 23 06/27/14 <0.01 0.038 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 <5 12/17/14 <0.01 0.08 <0.001 <0.01 <0.01 <0.0002 <0.01 <0.01 9.9 06/28/18 <0.015 0.032 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 <1 76 NM NM NM NM NM NM 01/21/19 <0.015 0.03 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 31 160 5.6 6.3 257 14.5 138 13.1 06/17/19 <0.015 0.025 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 < 99 5.7 26.4 235.5 19.7 48.4 5.06 03/09/20 <0.015 0.035 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 9.8 94 6.3 10.5 265.4 6.98 55.1 8.9 11/09/20 <0.015 <0.025 <0.005 <0.01 <0.01 <0.0002 <0.02 <0.01 2.5 67 6.8 18.3 325.3 11.4 63.4 3.78 03/25/21 Unable to collect sample due to biological hazard near sampling location 11 /01 /21 <0.015 0.026 <0.005 10.01 <0.01 <0.0002 <0.02 <0.01 9.3 82 6.5 20.7 172.8 7.28 34.6 3.14 All concentrations in micrograms per liter (ug/L) unless otherwise noted NE - Not established -- - Not sampled NM - Not measured Bold indicates exceedance of NC 2B Water Quality Standard h = hardness dependent dissolved metal standard Page 2 of 2 DRAFT Swift Creek Tables 2021 11.xlsx/Table A2-Historic SurfaceWater WATER QUALITY MONITORING REPORT— NOVEMBER 2021 APPENDIX B FIELD SHEETS November 2021 www.erm.com Version: 1.0 Project No.: 0397281 Client: ReUse Technology January 19, 2022 P:\Projects\0397281 ReUse CAP Implementation Swift Cr.DW\Post Closure Monitoring\2021-11 GWS\Swift Creek Water Quality Monitoring Report DRAFT TW_bpw.docx ERM Bottle Order/Label Sheet Site: Swift Creek ERM Project Number: 0397281 %BOTTLE LABEL water Level Metals (6010) Sulfate ( (300) TDS (2540C) *MW-OIS-WG-202003 4�.77 X X X MW-0ID-WG-202003 G UI X X X MW-02S-WG-202003 LI,;� ( X X X MW-02D-WG-202003 t-I.7Z X X X MW-03-WG-202003 - X X X MW-04-WG-202003 (7.` Ll X X X MW-05RS-WG-202003 7, ; ( X X X MW-05RD-WG-202003 'f X X X MW-06-WG-202003 i .q2 X X X MW-07-WG-202003 �, X X X MW-08-WG-202003 3 X X X SW-01-WG-202003 X X X SW-02-WG-202003 X X X SW-03-WG-202003 X X X FD-01-WG-202003 X X X AX �..wl,.......: x.. ..,, �.::., X7 SUM (Bottle Count): 16 16 16 Notes Please include: - 1 trip blank per cooler. At least 1 CoC per cooler. 1 custody seal per cooler. Prepaid shipping labels, if possible. *Collect FD-01 at MW-01S Key: =Normal sample = Duplicate sample = QAQC sample = Extra set for breakag, ERM Field Team Note: add the sample day in dd format to the end of the sample iD (i.e, MW-C WATER MATRIX SAMPLING FIELD DATA FORM >ttNt Site Name: Swift Creek ERM Project Number: 0397281 Sample Type: (Monitor Well, DPT, Surface Water, Potable WSW; other) Maht�on Sample ID: W. ^ W (J —Z 2 Date: 2 Time: 6613 Sampling Personnel (circle one : n Woodruff ohn Haffn r Weather Conditions (circle one): nn , Partl Cloudy, Cloudy, Rain, Other Well T pe: F sh Surlace Completion, ti up Com lelio Well Tag Present: es No Weli Locked: No Lock Present: No Well ID info on Tag: e , No o Well Bolted: es No Well Cap: Well Cap Condition: c , Replace, Other: Well Pad Corldifion, Cracked, Replace, Other: Well Location: r s Asphalt, Concrete, Woods, Other: Additional Comments: Total Depth of Well .D.): Screen Length: 57 uut 1s, 20 Depth to Water (D.T.W): (1) Well Diameter: 2 q, e, a Total Volume Purged: i' Casing Type: v ,steel Purge Rate: mUmin Sampling Device: a, Monsoon, Orundfos, Bailer, Other: Tubing Type:P h e Measuring Point: Top o a g other: Pump Intake (ft below M.P.): Color: a Odor: Yes, N Time: min Volume Pur ed DTW: feet Temp cc) pH Sid units SPC uS/cm DO m /L ORP mV Turb NTU Comments: Stabalization Criteria 2 (gallop»- (see note below)3 +1. 3% +/- 0.1 unit +/- 3% +/- 10% +/- 10 My +/- 10%4 60 1 CO 5. $ J 6. 5 Y o," - s -2. 1�oo036 S -I& t9x 9)T ,13 0.8 2 •0 0,2 u 327 O -22a 3s oA Or —a •2 6 e 0 3' Oe26 -23,( 1 S YB 5, 23 -2G• 500 5e Field Parameters measured with: YSI Pro/ ql + r- Official Sampling Dale & Time' I (l/I /L ` IS 5J "—" I ~W r"{ �Zoa4i`Id`o Samples Collected: Analysis Requested' Preservative: Hold Time (days): Lab. Metals solo HNO3 25 Pace Analytical Sulfate 300 TDS 254OG Notes: (1)-0 vedepth to bottom of well until after paging and spl'ng forefoot leswing pentlfines Natmay be resting on the well boMm. (z)-saer�<so�aOrders brand On mme most recent tons trunks meaamemenn. (J) -Total tl,axtloxn hwell to be less Nen 0.1 m (0.32 e). Paging rela to be lowered as necessaryto keep arawaovm below 0.1 m (0.32 S. (4)W IO%vMen Val)=sendi : NTUs. (b)-DO is not aO Volume seal)=g,on rule: (e)-ORPa not a$aminonnedorsfor One me MKinAvmersampling'' SE sadmtl OperagPmocedur (])-ORPq not a steMlizafion cmeam for tl,e'Olev,Wmter samplv,g'SESD standard Opnaune Procedure. WATER MATRIX SAMPLING FIELD DATA FORM Site Name: Swift Creek--y ERM Project Number: 0397281 Sample Type: (rNanitar-Weft DPT, Surface Water, Potable WSW; other) Sample ID: iVnW - -- 6.(6-:zc'9 6Eel Date: Time: L T� Sampling Personnel circle one): Jordan Woodruff John Haffner Weather Conditions circle one): au Partly Cloudy, Cloudy, Rain, Other Well T pe: Flush Surface Completion, Stick Up Com letio Well Tag Present: 1 ems, No Well Locked: s, No Lock Present: No Well ID info on Tag: No Well Bolted: Yes, M1Jryp Well Cap: Yes, Well Cap Condition: c o�e , Replace, Other: Well Pad Condition: o d, Cracked, Replace, Other: Well Location: , Asphalt, Concrete, Woods, Other: Additional Comments: Total Depth of Well T.D.: 7h 7 Screen Length: 5, R, 155 20 Depth to Water (D.T.W): Well Diameter: Q, 4, s, a Total Volume Purged: Casing Type: V Steel Purge Rate: .1670 mumin Sam lin Device: ns tic, Monsoon, Grundfos, Bailer, Other: TubingType: Polyethylene Measurin Point: Top of casing other: Pump Intake (ft below fil 3 a7 Color: Odor: Yes, '(d Time: min Volume Purged DTW: feet Temp pc pH std units SpC uS/cm DO m /L ORP my Turb NTU Comments: Stabalizalion Critenb2 (gallons) (see note below)' +/- 3% +I- 0.1 unit +/- 3% +/- 10 % +/- 10 my +/. 10%, 5 ,2o 04n'1T I IZt� -39 _3r1.3 - Z erw� O.'�i Q�t "2�2g' d sJ j0_ Qa7 ^.i, .` f3 2f 4'S D'. 7 _s-IT4 3 I jufoj 67 o I' 20-1 6LW 12n.t GJ. I i 1,31 ' 2r 1- 1 2&7 16 q9 120&. .,/0 _ilo,, 11, 22 20 q 6,19 fr�;- J-"i# Z 077 _3t Field Parameters measured with: Ysl Pro/ Official Sampling Date & Time: Samples Collected: Analysis Requested: Preservative: Hold Time (days): Lab: Metals 6010 HNW 29 Pace Analytical Sulfate 300 TDS 2540C Notes: -Do not manage earth to bottom ofwell until aper purging and sampling to reduce resuspending fines pact maybe resting on One well botlom. (2)-Stabilization nlerla based on Wee (3)4110 %datum InweG roer less B,mi 011rm(0.32fl)e PulB�Beare lobe lowered asnecessary fokeep drawdown below 0.1 m(0.32 fi). (5) H-f0%when Nrbidily Is over 10 NiUs. (5)well uma(Bakio.W1alb a np: (E) -OO not as stabilization izetlon criterionforte forte vafersamplinB' SEED Elandarard operating Procedure. p) -oaPla not aatabe2aaon ememn mrlhe ^crounawaterramvnnq sas0 slanaem opemunB Procedure, WATER MATRIX SAMPLINQ FIELD DATA FORM ERM Site Name: Swift Creek ERM',tProject Number: Sample Type: (Monitor Well, DPT, Surtace Water, Potable WSW; other) NoY7 a/'' Lli 0397281 Sample lD 2 ��b Date: 2 Time: Sampling Personnel (circle one): Jordan Woodruff John Haffner Weather Conditions circle one): u Partly Cloudy, 06�*�,Zaih,.Gfher Well Type: Flush Surface Completion, ick Up Completion Well Tag Present: eNo Well Locked es No Lock Present:a No Well ID info on `fag. yes No Well Bolted: No Well Cap: Yes, Well Cap Condition cod Replace, Other: Well Pad Condition. Goo , Cracked, Replace, Other: Well Location: Grass, Asp all, Concret ootl ,Other: Additional Comments: Total Depth of Well (F.D.): Screen Length: 51 0 15, 20 Depth to Water (D.T.W): t') Well Diameter: a, e, 8 Total Volume Purged: Casing Type: v , steel Purge Rate: mL/min Sampling Device: Monsoon, Grundfos, Bailer, Other: Tubing Type: Po to ene Measuring Point: pot Casin other: Pump Intake (ft below M.P.): Color: L ectr Odor: Yes, o Time: min Volume Purged DTW: feet Temp4stdunits (Gc SPC uS/cm DO m /L ORP mV Turb NTU Comments: Stabalization Criteria' (gallons) (see note belo,d)33% +/- +I- 3% +/- 10% +/- 10 my +/- 10%4 0- U- -O6. 21• —! .8 G 0s" Field Parameters measured with vs1 `Prro1/ 137` Official Sampling Date & Time: II1 112' OU Samples Collected Analysis Reguested: Preservative: Hold Time (days): Lab: Metals solo HNO3 28 Pace Analytical Sulfate 300 TDS 2540G arbitration criton Miss recent consurnifirmasurements Notes: (t) Do not measure tlepN to bottom o(well are after purging and aempfN9 to reduce resaape,m'ma fines t,al maybe resOn9 an Newell bplfom- �S�- Total tlavdavmeNwell slodbe less Nanoo.f mte.32 fi)eP Oengrefefpbe lovreretl as necessary to keep dmvgpvn, belowe.l m(0.32 P). (4)Well f0%Volume en all=4y0overle NTUs. (e)- oR Isnot e abbclizate critern Ima be uponavemodeler sampling' aSE 9 nds ema Gpna4ng procedure te (i)-ORPk not asiabilizeOan aMnon far Ne "G,aundvmfersampli,g' SD Slantla,d Gpxa6ng Procedu,e. WATER MATRIX SAMPLING FIELD DATA FORM ERM Site Name: Swift Creek Sample Type: ( omtor ell, DPT, Surface Water, Potable ERM Project Number: 0397281 WSW; other) Sample ID: 0i Date: E (A 2 i Time: I Sampling Personnel circle one): Jordan Woodruff John Haffner Weather Conditions circle one): lgiiily, Partly Cloudy, Cloudy, Rain, Other. Well Type: Flush Surface Completio Stick U Compielf Well Tag Present: 'ies No Well Locked: Wis, No Lock Present: Vs, No Well ID info on Tag: des, No Well Bolted: Yes, 70 Well Cap: Yes, Well Cap Condition: Replace, Other: Well Pad Condition: c00 , Cracked, Replace, Othel Well Location: 99, Asphalt, Concrete, Sods Other: Additional Comments: Total Depth of Well T.D.: }r - 4Screen Length: 5, 15, o) 20 Depth to Water (D.T.W): 1t) (. 7; Y Well Diameter: .h`! 4, e, a Total Volume Purged: Casing Type: Q, Steel Pur a Rate: `.' f ,00 mUmin Sampling Device: eri l itic, Monsoon, Grundfos, Bailer, Other: Tubing Type: Polyethylene Measuring Point: Top of Casing other: Pump Intake (ft below MR): 6 f=l Color: C le Odor: Yes, Time: min Volume Purged DTW: feet Temp eC pH std units SpC uS/cm DO m /L ORP mV Turb NTU Comments: Stabalization Criterial (gallons) (see note below)' +/- 3% +/- 0.1 unit +/- 3% +/- 10% +/- 10 my +/- 10%4 b u5 - s.; 0,7b _Yqer 2. ,. w _ 1 I - �ey-3 it - r#l.7 -'+N I7 '3 rJ 70 .ad %-i4 t'(7$,. ^-ay 70i ldi K. 4 a171 01 -404 n.hro 1i0 (�.-to .r�. .f h` r-177.G ?1y Field Parameters measured with: YSI Pro / ( ��(✓ � �" i "� � "� Official Sampling Date & Time: j i �l / 2 ( ��/ 71 Samples Collected: Analysis Requested: Preservative: Hold Time (days): Lab: Metals solo NN03 2s Pace Analytical Sulfate 300 TDS 2540C Notes: (1)-Do not measure depth to bottom of well untll after posting and sampling to reduce resuspendng Ines Ual maybe resting an Me weA boham. (z)-Stabilization rumors based on three maameaamless co„aecawe maaaaramema. (4)-T wan robe 10 NTUnO.im(o.ffitt). Posting stem be lowered as necessary to keep araveaown below 0.1 m(g.a2 if). (4)N Vowhenfall=M Is over to NTUs. (5) we0 Volume stabilization with: (7)-o nnmerionfor or e 'GMe 'Groundwater mamipgg' ESD SEED Standard Opeb'ng Procedure. (n-ORP is not a sfabllhatlon cmeaan for Na "Orounawater samping' SESD sUnaa,a Operating Proceaum. WATER MATRIX SAMPLING FIELD DATA FORM Site Name: Sample Type: Swift Creek ( for I, DPT, Surface Water, Potable ERM Project WSW; other) Number: 0397281 Sample ID: AAE„s - �' '> -- kN x2.1911 2- Date: Time: Sampling Personnel circle one): Jordan Woodruff John Haffner Weather Conditions circle one): Ea , Partly Cloudy, Cloudy, Rain, Other Well Type: Flush Surface Completion ick UPC Well Tag Present: ppyy Yes, 4Jd Well Locked: YQs, No Lock Present: `9e ,, No Well ID info on Tag: Yes, ado' Well Bolted: Yes, Well Cap: No Well Cap Condition: nq d, Replace, Other: Well Pad Condition: 0, Cracked, Replace, Other: Well Location: 61, Asphalt, Concrete, Woods, Other: Additional Comments: Total Depth of Well T.D.: 20 if Screen Length: s, 10 16, 20 Depth to Water (D.T.W): 01 fj?_ Well Diameter: CP 4, s, a Total Volume Purged: Casing Type: t&Steel Pur a Rate: !` ,?:7 mUmin Sampling Device: tic, Monsoon, 0rundfos, Bailer, Other: Tubing Type: Polyethylene Measurin Point: Top of Casing other: Pump Intake (ft below M.P.): `5 rfi Color: .clea Odor: Yes, Time: min Volume Purged DTW: feetstd pH units SPC uS/cm DO m /L ORP mV Turb NTU Comments: Stabalization Critena' (gallons) (see note below)'0.1 +/- unit +/- 3% +/- 10% +/- 10 mV +/- 10%" n O 35r jq7 5b }t,tgL) i, � q75 �/ y�5- 3 y asf of K s'-7 1 'v ; a� ! q. s. IT — 0 `7 c( 7,11 3 •a7 0��0 R 7.4 � 3t�0 `t6� 4V/ 0 (.71 ( 10 } S.`(1 7131 1t7.:;/0/ Ll'�-7 6.9'1 133� Field Parameters measured with: Ysl Pro / HA01 2 (7 W Official Sampling Date &Time: � (/2 121 &i I � 2 Samples Collected: Analysis Requested: Preservative: Hold Time (days): Lab: Metals solo HNO3 28 Pace.Analylical Sulfate Soo TDS 2540C Notes: -Do not measure aepmmbOtto mmwell „nw aver purging and sampling mreduce resuspending firms died may belosing on Me well bottom.. (2)-sfabd eanencnfeaa based on Ihree most recent consecutive meawremenk. (3)-Total drawtlown in well to be less Man 0.1 m (0.32 n). Pu,efnp rate to be lowered as necessary to keep amwdown befaw 0.f in (0.32 n). (4) N-10%when lu,blai0.Is over 10 NTUs. (b) Well Volume (gags O.on deft (S)- oolanot ot asta izaaon«ifedonn for for Me Groundwaletersoming'SE Iandmdopem4ng Procedure. (])-ORP Is not a stabilization cMedan far the'GrounAvalersampRng'SEso Standard opemang Procedure. WATER MATRIX SAMPLING FIELD DATA FORM Site Name: Swift Creek ERM;;��Project Number: Sample Type: (Monitor Well, DPT, Surface Water, Potable WSW; other) !w I rf 0397281 Sample ID: 0"� Date: I 21 Time: 2S Sampling Personnel circle one): Jordan Woodruff �hn Haling Weather Conditions (circle one): S n Partly Cloudy, Cloudy, Rain, Other Well T a: Flush Surface Compietio , tic u Co leuon Well Tag Present: No Well Locked. a , No Lock Present: No Well ID info on Tag: No Well Bolted: a Na- Well Cap: e , No Well Cap Condition. , Replace, Other: Well Pad CO ItlOn: Good, Cracked, Replace, Other: Well Locatio s, sphalt, Concrete, Woods, Other: Additional Comments: Total Depth of Well (f.D.): Screen Length: 51 015, 20 Depth to Water (D,T.1N): m Well Diameter: 2 a, e, 8 Total Volume Purged: Casing Type: Pv , Steel Purge Rate: murrain Sam tin Device: eristalt Monsoon, Grundfos, Bailer, Other: TubingType:olyethylene Measuring Pant: o or cas g other: Pump Intake (ft "P"): Color: Odor: Yesd6jo Time: min Volume Pure DTW: feet Temp ^c pH std units SPC uS/cm DO m /L ORP my Turb NTU Comments: Stabalization Criteria' .(yrylftlffT (see note below)' +I- 3% +/- 0.1 unit +/- 3% +/- 10% +/- 10mv +/- t0%' 2 V d 2ION6. KOO is. 6 6 t�. 2000 a D o `t YS Ul DD 1 z24.5 6. 23 0' 4A I.` <eDb 73.10 a4l cuy 3 t Mir 2b 3. ,. 6" p0 2 p D 5- Field Parameters measured with: vsl Pro/ livi'T Official Sampling Date &Time' I(1�14I D2� Samples Collected Analysis Requested Preservative: Hold Time (days): Lab: Metals 6010 HNO3 28 Pace Analytical Sulfate 300 TDS 2540C ON tes; (I) -Do not Measure depN to bottom ofrvell untaselllobe il after purging and sampling to reduce resozperding fines Nat maybe res4ng on Nevrell boflam. (2)-StabT a0on nHedn based an tree most resent <onseagvo measuremen6. (3) Total tlmxdoan in y a o u less Nan 0.1 m (0,32 p). Puging or [a lobe loweretl as necessary to keep Nawdovm below 0.l m (O.J2 a). (5) WeiIVooluenialo=y041d to NTUs. (b) Well Volume(gap=Oism smaller (el-G adea forMeMe'GrouAvalersampling' aSE standardtandard Stanford crooninProcedure. (]) � ORPk not a�tab sterilization cnledan for Ne'Gm,ndwatersamping' SEW standard Opae0n0 Proredxe. WATER MATRIX SAMPLING FIELD DATA FORM ERM Site Name; Swift Creek ERM Project Number: 0397281 Sample Type: (go=nftor WiA, DPT, Surface Water, Potable WSW; other) Sample ID: M LA/ Date: iir 2( Time: I ��Ira Sampling Personnel circle one): Jordan Woodruff John Haffner Weather Conditions circle one): un Partly Cloudy, Cloudy, Rain, Other Well Type: ash Surface Com le` U ' Stick Up Completion Well Tag Present: es, No Well Locked: Yes, Lock Present: z No Well ID info on Tag: No Well Bolted: e$�s. No eS Well Cap: No Well Cap Condition: a , Replace, Other: Well Pad Condition: Good, Cracked, Replace, Other Well Location: r , Asphalt, Concrete, Woods, Other: Additional Comments: Total Depth of Well (T.D.): L Screen Length: 5, 0 15, 20 Depth to Water (D.T.W): (1) 7• Well Diameter: a� 4, s, e Total Volume Purged: 20? vn Casing Ty e: Steel Purge Rate: '.� 1,00 mUmin Sampling Device: eristafff Monsoon, Grundfos, Bailer, Other: Tubing Type: Polyethylene Measuring Point: Top of Casing other: Pump Intake (ft below M.P.): p' g' ¢" Color: h+-✓ Odor: Yes, Time: min Volume Purged DTW: feet Temp ec pH std units SpC uS/cm DO m /L ORP mV Turb NTU Comments: Stabalization Criteria2 y L (gellerls) (see note below)' +/- 3% +/- 0.1 unit +/- 3% +/- 10% +/- 10 my +/- 10%4 ',KEY 22.( e,�j• "t�lJ-6 v,75 t-1.(eraof `L2. Z '��b f.l�`f. J -lira' 2-- . (y (703 %3r2n.�. a r<' fl9:'J .0IT 2Z.Z 7.00 ��1, 26, 110f 1 h nD q t," 24t G-lot ( f+5 =x rJ t7J •Kh 22 . G-. �.. Qsi O-wl 26 ° t D Field Parameters measured with: Official Sampling Date & Time: Samples Collected: Analysis Requested: Preservative: Hold Time (days): Lab: Metals solo HNO3 28 Pace Analytical Sulfate sop TDS 2540C Notes: (1) be -Do not measure depN to bottom Orwell until after purring and sampfng to seduce resuspentlNO fines that maybe rastirg on Newell bottom. StalAzalion arttedabased on (4)-Total whonto InweA toer lossthanNano011sm(0.02fl)ePurging rate to be lowered as necessary to keep drawdown below 0.1 m(0.32 S. (4)WF10°/urna(lal) 0,Isoverf0NTas. (b) Well snots stay=o.o41d36: (E)- DOIsseta afabNizatloncriterion for roundwater aargo'GEED Statlmdd Opera,0Procedure. (])-ORP Is not a slabAizatlan criterion for me 'Groundwater sampling' SESD Standard Operating Procedure. WATER MATRIX SAMPLING FIELD DATA FORM Site Name: Swift Creek Sample Type: (Monitor Well, DPT, Surface Water, Potable ERM Project WSW; other) Number: 0397281 Sample ID: 202j j of Data: 2 Time: Sampling Personnel circle one): Jordan Woodruff o ffner Weather Conditions circle one): unn , Partly Cloud oud , Rain, Other Well T e: Flush to Is Up Completion Well Tag Present: Yes, No Well Locked: Yes, o oc Present: Yes, No Well ID info on Tag: Yes, No Well Bolted: Yes, No Well Cap: Yes, No Well Cap Condition: Good, Replace, Other: Well Pad Condition: Good, Cracked, Replace, Other: Well Location: Grass, Asphalt, Concrete, Woods, Other: Additional Comments: Total Depth of Well T.D.: 7, Screen Length: 5 10, 15, 20 Depth to Water (D.T.W): 11) 7 ryi Well Diameter: z, 45 a, 8 Total Volume Purged: �, Casin Type: ;)steel Purge Rate: m min Sampling Device: P vista ' Monsoon, Grundfos, Bailer, Other: TubingType: olyeth lene, Measurin Point: of Casl other: Pump Intake (ft a .): Color: Odor: Yes, N , Time: min Volume Purged DTW: feet Temp eC pH std units SPC uS/cm DO m /L ORP mV Turb NTU Comments: Slabalizalion Criteria' M (Mg1151is) (see note below)' +/. 3% +/- 0.1unit +/- 3% +/- 10% +/- 10MV +/- 1o%d 1i > 0 `iu .5 �L 2 2 m1 "i u f�,o 22a1ziq i`t ro oaf P 6 5 2 A i,la ` Field Parameters measured with: Official Sampling Date &Time: Samples Collected: Analysis Requested: Preservative: Hold Time (days): Lab: Metals sour HNO3 2e Pace Analytical Sulfate Soo TDS 25400 Noes: In- -Do not na1 measure aepm to bottom of well u,ml anarpmelna and aampr„a to reduce reauspeasking ethan uea met maybe raen„a on me well honour. -Stablization Me,la based on mree most recent<onseculive measurements. (4)-Total wIwn wn Nweg to be less TUB.g.1 m (0.32 n). Pouring rate to be lowered as necessary to keep drawtlown below 0.1 m (0.32 IS, (5) won VRuben Wmlairy Isover cDc a NTUs. (6) wen volume (gag = dorl ilea (7)- OOIsnot a as ubaizagonc,lleaoncarme"Groundwaterasmpmg"SEED Standard Operating Procedure. (])-ORP h net a ambRiutian criterion forme "Groundwater sampling' SESO Standard Operatl,g Procedure. WATER MATRIX SAMPLING FIELD DATA FORM Site Name: Swift Creek Sample Type: ( o ERM Project 1, DPT, Surface Water, Potable WSW, other) Number: 0397281 Sample ID: J r Ei. V.1r- 20l (' Date: (I z , f Time: Sampling Personnel circle one): Jordan Woodruff John Haffner Weather Conditions (circle one); u , Partly Cloudy, Cloudy, Rain, Other Well Type: Flush Surface Completion, 'ck Up Completio Well Tag Present: Ke§, No Well Locked: , No Lock Present: 6Z No Well ID info on Tag: JrR, No Well Bolted: Yes, Well Cap: 1�sg , No Well Cap Condition: o Replace, Other: Well Pad Condition: o ,Cracked, Replace, Other: Well Location: a ,Asphalt, Concrete, Woods, Other: Additional Comments: Total Depth of Well (T.D.: ' Lt f Screen Length: �} 5, t'9( 15, 20 Depth to Water (D.T.W): (11 is - j f--'� Well Diameter: Cz! a, s, a Total Volume Purged: Casin T e: Steel Purge Rate: +� 1 C) C mL/min Sampling Device: Ejfistal' , Monsoon, Grundfos, Railer, Other: Tubing Type: Polyethylene Measuring Point: Top of casing other: Pump Intake (ft below M.P.): 7, Color: COY Odor: Yes, Time: min Volume Purged DTW: feet(CC) Temp pH std units SPC uS/cm DO m /L ORP mV Turb NTU Comments: Stabalization Cdteriat? (gallons) (see note below)' +/- 3% +/- 0.1 unit +/- 3% +/- 10% +/- 10 my +/- 10%4 y 2 2 7� E 7 3 0 7 j 6 7/J0 .-�7� `)+r- ^J(e n� zr 0.1jfq" 7-fSa- y J -O U✓ f .-rig ZD -7 74 " 1�z&E r9.r-r2 21q.5 .35i a.T' 7°( f-7o . Q-3q '2=S_3 LLh 3 QO 2.�JC*^ S.Ya 20. S 3-7`1 4h i2 L ";52 1 2261 in76 2,0 -3.7+f 5"72 O7 to H31.x 3.5i . c(Iq- `tjy nQ Field Parameters measured with: vsl Pro/ Official Sampling Date & Time: 1 [ �'L �Z 1 ( t-I i0 Samples Collected: Analysis Requested: Preservative: Hold Time (days): Lab: Metals ee10 HNO3 2a Pace Analytical Sulfate 300 TDs 2640C Notes: -Do no I are depth to bottom of well and after purging and seraphim to reduce resuspending fines Net maybe reachin- Tell be g an the well bottom. (2)-SIabR 4one,Heela based an Wee most recent consecutive meesuremenfa. p) V 10 drawdown N well to over less than 0.1 m (0.32 Hj. Purging rate to be lowered as necessary to keep drewtlown belawe.i m (0.3211). (4)H-1e%when Nrbitlilyisovio NTDs. (6)Weg-DO Is not a(gali hedcrigM1: (7)-OOfsnota aboasci liallanmtedonfor r Me 'Groundwater saamplin 'SESSESD Standard Spending Procedure. (1)-ORP Is not a stabfi'vation c,Hedon for Ne'GraunM�aler sampling' SESO Standard OperalNg Pracedae. WATER MATRIX SAMPLING FIELD DATA FORM fl ERM Site Name: Swift Creek Sample Type: (Monitor Well, DPT, Surface Water, Potable ERM Project Number: 0397281 WSW; other) Sample ID: °A p✓-;j - 240L1I ;5y Date: 2 Time: f( Sampling Personnel circle one): Jordan Woodruff John Haffner Weather Conditions circle one): unn Peril Cloud , Cloudy, Rain, Other. Well Type: Flush Surface Complelio Stick Well Tag Present: 12, No Well Locked: �, No Lock Present: ' eke, No Well ID info on Tag: es No Well Bolted: Yes, '® Well Cap: No Well Cap Condition: , Replace, Other: Well Pad Condition: CGogU, Cracked, Replace, Other: Well Location: era , Asphalt, Concrete, Woods, Other: Additional Comments: Total Depth of Well Screen Length: 5, 0�, 15, 20 Depth to Water (D.T.W): tl) X. 7 Well Diameter: (� a, s, s Total Volume Purged: Casin T e: Pv , Steel Pure Rate: "` mL/min Samplin Device: ris ic, Monsoon, Grundfos, Sailer, Other. Tubing Type: Polyethylene Measuring Point: Top of Casing other: Pump Intake (ft below M.P.): 7- Color: , t-e4A/ Odor: Yes, Time: min Volume Purged DTW: feet Temp aC pH std units SPC uS/cm DO m /L ORP mV Turb NTU Comments: Stabalization Crileriag (gallons) (see note below)' +/- 3% +/- 0.1 unit +/- 3% +/- 10% +/- 10 mV +/- 10 4 c79 7o .J 20 3.72. IT370 0.3`6 -20? 5. 7 `5 �l o 1� 2^ 7f7 15`34 ZS> _ 2 Field Parameters measured with: YSI Pro/! 2 j{{02 1.:Y Official Sampling Date & Time: [ l / / / 2 ( I'4 f i7 Samples Collected: Analysis Requested: Preservative: Hold Time (days): Lab: Metals solo HNO3 26 Pace Analytical Sulfate sop TDS 2540C Notes: (I) - Do not measure depth to bottom of took onel aflerpurgNH and sampling to reduce resuspending fines met maybe resdng an Nowetlbottom. (2)-Spoliation crfleda based on Nree most resent [onsecuE've meesuremenh. (4)+1-10 Wien wnNwell Lobe less Pon 0.1m(o.J2IT, Purging rate fa belowered as neceueryla keep dmwdom befaw 0.1 m(0.32 it). (4)al-f Volumen aft= 0.04over 10 NTn3. (5)- Well -DO not a (gap=OA41tl3M1: (e)-o ezatlonn critunfor rthe me'Greaurdyersamplingg' ESD SEED Standard Operating PProcedur IT)-oRP[la not e mobilization <iiledon for me "crounAvaler sampling'sE50 Standard apemling Procedure. WATER MATRIX SAMPLING FIELD DATA FORM ER[vt Site Name: Swift Creek ERM Project Number: 0397281 Sample Type: (Monitor Well, DIST, Surface Water, Potable WSW; other) Sample lD: Date: tC 2t Time: L [ Sampling Personnel (circle one): J rdan Woodruff oh Haffne Weather Conditions (circle one): ,Sun'hy, Partly Cl.udy, Clouq , Rain, Other Well Type: Flush Surface Completion, Stick Up Completion Well Tag Present' Ye o Well Locked: es` No Lock Present: es No Well ID info on Tag: Yes No Well Bolted: es No Well Cap: es, No W¢II Cap Condition o Replace, Other: Well Pad Condltl0 o , Cracked, Replace, Other: Well Location: Grass, Asphalt, Concrete, ood Other: Additional Comments: Total Depth of Well (r.D.): Screen Length: s, op 15, 20 Depth to Water (D.T.W): (1) Well Diameter: 4, s, s Total Volume Purged: Casing Type: Steel Purge Rate: munnin Sampling Device: erist tic, Monsoon, Grundfos, Bailer, Other: TubingT e: olyethylene Measuring Point: Top of Casing other: Pump Intake (ft below M.P.): Color: Odor: Yes, No Time: min Volume Pur ed DTW: feet Temp ac pH std units SPC uS/cm DO m /L ORP mV Turb NTU Comments: Stabalization Criteriaz (gauons) (see note below)3 +/- 3% +/- 0.1 unit +/- 3% +/- 10% +I- 10 my +/- 10%4 W ri' S' 3} S y P 2 C:2� It1 Field Parameters measured with: vsl tPro(r /�� ((� �.p _ Official Sampling Date & Time: {C (/ ° ( / ( f ? /�''"' Samples Collected: Analysis Requested: Preservative: Hold Time (days): Lab: Metals solo HNO3 28 Pace Analytical Sulfate 300 TDS 2sa0C Notes: nl-Do not measve depth to bottom :)well unN agsr plll9ng and samplers to reduce ressspersfin9 fines that maybe resOng on nevmll bogom. (2)-Slab3izaC'on ttilena basetl on three most recent consea,we measuremen6. (J) Total dmlWovm A well to be less non 0.1 an (0.32 to. nursing rat: to belowxed asnecessaryto keep tlmwdovm below0.i an 10.32 fiI. olgmen bag =0.is over 10 NTDs. (6) Well Volume(Val anon heel (g)-DOIsnotasdbilzab'oonilalonlo,the"Grauntlwaler sampling' SEW Standard Operating Procedure. (])-ORPh nolastabilize0on aite,lon for tl,e'Growtlrrzler samgog SD SWntlartl Operand Preretlure. WATER MATRIX SAMPLING FIELD DATA FORM ERM Site Name; Swift Creek Sample Type: (Monitor Well, DPT, ERM Proiect Number: 0397281 ace , Potable WSW; other) Sample ID: Date: Time: Sampling Personnel circle one): Jordan Woodruff John Haffner Weather Conditions circle one): Sunny, Partly Cloudy, Cloudy, Rain, Other Well Type: Flush Surface Completion, Stick Up Completion Well Tag Present: Yes, No Well Locked: Yes, No Lock Present: Yes, No Well ID info on Tag: Yes, No Well Bolted: Yes, No Well Cap: Yes, No Well Cap Condition: Good, Replace, Other: Well Pad Condition: Good, Cracked, Replace, Other: Well Location: Grass, Asphalt, Concrete, Woods, Other: Additional Comments: Total Depth of Well T.D.: Screen Length: 5, lo, 15, 20 Depth to Water (D.T.W): t11 Well Diameter: 21 41 s, 8 Total Volume Purged: Casing Type: PVC, Steel Purge Rate: mUmin Sampling Device: Peristaltic, Monsoon, Grundfos, Bailer, Other: Tubing Type: Polyethylene Measuring Point: Top of casing other: Pump Intake (ft below M.P.): Color: Odor: Yes, No Time: min Volume Purged DTW: feet Temp °C pH std units SPC uS/cm DO m /L ORP mV Turb NTU Comments: Stabalization Criteria (gallons) (see note below)" +/- 3% +/- 0.1 unit +/- 3% +/- 10% +/- 10 mV +/. 10%, 01,- 7- B.iE 7 f ti. 4Vv - F t - 1�/Ft5� -T.�TT- Lof 13 172,if �i. L L.( 7-2. Field Parameters measured with YslPro/qfttil 2{oo ( Official Sampling Date & Time: ,r '� 1'/9- 1 [ /'�2 z le r Samples Collected: Analysis Requested: Preservative: Hold Time (days): Lab: Metals 6010 HNO3 28 Pace Analytical Sulfate soo TDS 2540C Notes: (1)-Do not measure depN to page; in of well until after pwging and sempling to reduce resusDendng tines Naf maybe restmg on Newell bogam. Stabileramm rdeda based on tree most recent consecutive measurements. (3)-Total dmwtlown In well to be less Nan g.1 m (g.32 fl). Pmgtng rate to he towered as necessary to keep drawtlown beluwe.l in (0.32 fl). (6)Well Volume (get) tlM1y le over le MUs. (b)-DOVolume(gal)= min crufr (7)-0 Mission for on e'Groundwatundwater eamplinyg' ESD SESO StandarOperating procedure. (])-One Is not alslabPrzatlon mledon for Ne'Grountlwalersamgling' SEGO EUntlartl Operating Procedure. WATER QUALITY MONITORING REPORT— NOVEMBER 2021 APPENDIX C LABORATORY DATA November 2021 www.erm.com Version: 1.0 Project No.: 0397281 Client: ReUse Technology January 19, 2022 P:\Projects\0397281 ReUse CAP Implementation Swift Cr.DW\Post Closure Monitoring\2021-11 GWS\Swift Creek Water Quality Monitoring Report DRAFT TW_bpw.docx 0 aceAnalytical Report of Analysis ERM NC, Inc. 300 West Summit Avenue Suite 330 Charlotte, NC 28203 Attention: Chris Means Project Name: Swift Creek Project Number: SEE EDD INFO Lot Number:WK08047 Date Completed:12/02/2021 12/02/2021 4:55 PM Approved and released by: Project Manager I: Hannah K. Lucas PCCRFO 24r iANSI National Accreditation Board qe0 A C C R E D I T E D TESTING LABORATORY The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC. Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Page 1 of 58 PACE ANALYTICAL SERVICES, LLC SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative ERM NC, Inc. Lot Number: WK08047 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace") Laboratory Quality Manual, standard operating procedures (SOPS), and Pace policies. Any exceptions to the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or discussed below. Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI scope of accreditation: Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid Chemical Material: TOC Walkley-Black. If you have any questions regarding this report please contact the Pace Project Manager listed on the cover page. Inorganic non-metals Samples -001, -002, -003, -004, -007, -008, -010, -011, -013, -014 and -015 were analyzed one day outside of the 7-day holding time due to laboratory constraints. Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 2 of 58 PACE ANALYTICAL SERVICES, LLC Sample Summary ERM NC, Inc. Lot Number: WK08047 Sample Number Sample ID Matrix Date Sampled Date Received 001 MW-01 S-WG-2021 1101 Aqueous 11/01/20211550 11/04/2021 002 MW-01D-WG-20211101 Aqueous 11/01/20211535 11/04/2021 003 MW-02S-WG-20211101 Aqueous 11/01/20211710 11/04/2021 004 MW-02D-WG-20211101 Aqueous 11/01/20211715 11/04/2021 005 MW-03-WG-20211101 Aqueous 11/02/20211320 11/04/2021 006 MW-04-WG-20211101 Aqueous 11/02/20211325 11/04/2021 007 MW-05RS-WG-20211101 Aqueous 11/01/20211115 11/04/2021 008 MW-05RD-WG-20211101 Aqueous 11/01/20211140 11/04/2021 009 MW-06-WG-20211101 Aqueous 11/02/20211410 11/04/2021 010 MW-07-WG-20211101 Aqueous 11/01/20211415 11/04/2021 011 MW-08-WG-20211101 Aqueous 11/01/20211415 11/04/2021 012 SW-01-WS-20211101 Aqueous 11/02/20211420 11/04/2021 013 SW-02-WS-20211101 Aqueous 11/01/20211640 11/04/2021 014 SW-03-WS-20211101 Aqueous 11/01/20211430 11/04/2021 015 FD-01 -WG-2021 1101 Aqueous 11/01/2021 11/04/2021 (15 samples) Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 3 of 58 PACE ANALYTICAL SERVICES, LLC Detection Summary ERM NC, Inc. Lot Number: WK08047 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 MW-01 S-WG-2021 1101 Aqueous Sulfate 300.0 380 mg/L 7 001 MW-01S-WG-20211101 Aqueous TDS SM 2540C- 6800 H mg/L 7 002 MW-01 D-WG-2021 1101 Aqueous Sulfate 300.0 16 mg/L 9 002 MW-01 D-WG-2021 1101 Aqueous TDS SM 2540C- 720 H mg/L 9 002 MW-01 D-WG-2021 1101 Aqueous Barium 6010D 0.027 mg/L 10 003 MW-02S-WG-20211101 Aqueous TDS SM 2540C- 360 H mg/L 11 003 MW-02S-WG-20211101 Aqueous Barium 6010D 0.20 mg/L 12 004 MW-02D-WG-20211101 Aqueous Sulfate 300.0 1.1 mg/L 13 004 MW-02D-WG-20211101 Aqueous TDS SM 2540C- 320 H mg/L 13 004 MW-02D-WG-20211101 Aqueous Barium 6010D 0.066 mg/L 14 005 MW-03-WG-20211101 Aqueous Sulfate 300.0 810 mg/L 15 005 MW-03-WG-20211101 Aqueous TDS SM 2540C- 2700 mg/L 15 006 MW-04-WG-20211101 Aqueous Sulfate 300.0 25 mg/L 17 006 MW-04-WG-20211101 Aqueous TDS SM 2540C- 230 mg/L 17 006 MW-04-WG-20211101 Aqueous Arsenic 6010D 0.035 mg/L 18 006 MW-04-WG-20211101 Aqueous Barium 6010D 0.025 mg/L 18 007 MW-05RS-WG-20211101 Aqueous Sulfate 300.0 2.8 mg/L 19 007 MW-05RS-WG-20211101 Aqueous TDS SM 2540C- 300 H mg/L 19 008 MW-05RD-WG-20211101 Aqueous Sulfate 300.0 6.0 mg/L 21 008 MW-05RD-WG-20211101 Aqueous TDS SM 2540C- 190 H mg/L 21 009 MW-06-WG-20211101 Aqueous Sulfate 300.0 790 mg/L 23 009 MW-06-WG-20211101 Aqueous TDS SM 2540C- 5500 mg/L 23 010 MW-07-WG-20211101 Aqueous Sulfate 300.0 700 mg/L 25 010 MW-07-WG-20211101 Aqueous TDS SM 2540C- 10000 H mg/L 25 010 MW-07-WG-20211101 Aqueous Arsenic 6010D 0.090 mg/L 26 010 MW-07-WG-20211101 Aqueous Barium 6010D 0.13 mg/L 26 010 MW-07-WG-20211101 Aqueous Lead 6010D 0.27 mg/L 26 011 MW-08-WG-20211101 Aqueous Sulfate 300.0 610 mg/L 27 011 MW-08-WG-20211101 Aqueous TDS SM 2540C- 7300 H mg/L 27 011 MW-08-WG-20211101 Aqueous Arsenic 6010D 0.070 mg/L 28 011 MW-08-WG-20211101 Aqueous Barium 6010D 0.089 mg/L 28 011 MW-08-WG-20211101 Aqueous Lead 6010D 0.24 mg/L 28 012 SW-01-WS-20211101 Aqueous Sulfate 300.0 2.3 mg/L 29 012 SW-01-WS-20211101 Aqueous TDS SM 2540C- 75 mg/L 29 012 SW-01-WS-20211101 Aqueous Barium 6010D 0.027 mg/L 30 013 SW-02-WS-20211101 Aqueous Sulfate 300.0 5.3 mg/L 31 013 SW-02-WS-20211101 Aqueous TDS SM 2540C- 110 H mg/L 31 013 SW-02-WS-20211101 Aqueous Barium 6010D 0.048 mg/L 32 014 SW-03-WS-20211101 Aqueous Sulfate 300.0 9.3 mg/L 33 014 SW-03-WS-20211101 Aqueous TDS SM 2540C- 82 H mg/L 33 014 SW-03-WS-20211101 Aqueous Barium 6010D 0.026 mg/L 34 015 FD-01 -WG-2021 1101 Aqueous Sulfate 300.0 410 mg/L 35 015 FD-01 -WG-2021 1101 Aqueous TDS SM 2540C- 7000 H mg/L 35 015 FD-01 -WG-2021 1101 Aqueous Barium 6010D 0.27 mg/L 36 015 FD-01 -WG-2021 1101 Aqueous Lead 6010D 0.031 mg/L 36 Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 4 of 58 Detection Summary (Continued) Lot Number: WK08047 Sample Sample ID Matrix Parameter Method Result Q Units Page (45 detections) Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 5 of 58 Inorganic non-metals Client:ERM NC, Inc. Laboratory ID:WK08047-001 Description: MW-01 S-WG-2021 1101 Matrix: Aqueous Date Sampled: 11/01/2021 1550 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Sulfate) 300.0 5 11/10/2021 0043 AMR 21980 1 (TDS) SM 2540C-2011 1 11/10/2021 1920 SJL 22041 CAS Analytical Parameter Number Method Result Q LOQ Units Run Sulfate 300.0 380 5.0 mg/L 1 TDS SM 254OC-2011 6800 H 25 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 6 of 58 Metals Client:ERM NC, Inc. Laboratory ID:WK08047-001 Description: MW-01 S-WG-2021 1101 Matrix: Aqueous Date Sampled: 11/01/2021 1550 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 11/12/2021 1051 CMS2 11/11/2021 1442 22159 1 3005A 601OD 1 11/10/2021 1701 KSH2 11/09/2021 1158 21737 Parameter CAS Analytical Number Method Result Q LOQ Units Run Arsenic 7440-38-2 6010D ND 0.015 mg/L 1 Barium 7440-39-3 6010D ND 0.025 mg/L 1 Cadmium 7440-43-9 6010D ND 0.0050 mg/L 1 Chromium 7440-47-3 6010D ND 0.010 mg/L 1 Lead 7439-92-1 6010D ND 0.010 mg/L 1 Mercury 7439-97-6 7470A ND 0.00020 mg/L 1 Selenium 7782-49-2 6010D ND 0.020 mg/L 1 Silver 7440-22-4 6010D ND 0.010 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 7 of 58 Inorganic non-metals Client:ERM NC, Inc. Laboratory ID:WK08047-002 Description: MW-01D-WG-20211101 Matrix: Aqueous Date Sampled: 11/01/2021 1535 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Sulfate) 300.0 1 11/10/2021 0102 AMR 21980 1 (TDS) SM 2540C-2011 1 11/10/2021 1920 SJL 22041 CAS Analytical Parameter Number Method Result Q LOQ Units Run Sulfate 300.0 16 1.0 mg/L 1 TDS SM 254OC-2011 720 H 25 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 8 of 58 Metals Client:ERM NC, Inc. Laboratory ID:WK08047-002 Description: MW-01D-WG-20211101 Matrix: Aqueous Date Sampled: 11/01/2021 1535 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 11/12/2021 1053 CMS2 11/11/2021 1442 22159 1 3005A 601OD 1 11/10/2021 1712 KSH2 11/09/2021 1158 21737 Parameter CAS Analytical Number Method Result Q LOQ Units Run Arsenic 7440-38-2 6010D ND 0.015 mg/L 1 Barium 7440-39-3 6010D 0.027 0.025 mg/L 1 Cadmium 7440-43-9 6010D ND 0.0050 mg/L 1 Chromium 7440-47-3 6010D ND 0.010 mg/L 1 Lead 7439-92-1 6010D ND 0.010 mg/L 1 Mercury 7439-97-6 7470A ND 0.00020 mg/L 1 Selenium 7782-49-2 6010D ND 0.020 mg/L 1 Silver 7440-22-4 6010D ND 0.010 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 9 of 58 Inorganic non-metals Client:ERM NC, Inc. Laboratory ID:WK08047-003 Description: MW-02S-WG-20211101 Matrix: Aqueous Date Sampled: 11/01/2021 1710 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Sulfate) 300.0 1 11/10/2021 0159 AMR 21980 1 (TDS) SM 2540C-2011 1 11/10/2021 1920 SJL 22041 CAS Analytical Parameter Number Method Result Q LOQ Units Run Sulfate 300.0 ND 1.0 mg/L 1 TDS SM 2540C-2011 360 H 25 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 10 of 58 Metals Client:ERM NC, Inc. Laboratory ID:WK08047-003 Description: MW-02S-WG-20211101 Matrix: Aqueous Date Sampled: 11/01/2021 1710 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 11/12/2021 1056 CMS2 11/11/2021 1442 22159 1 3005A 601OD 1 11/10/2021 1716 KSH2 11/09/2021 1158 21737 Parameter CAS Analytical Number Method Result Q LOQ Units Run Arsenic 7440-38-2 6010D ND 0.015 mg/L 1 Barium 7440-39-3 6010D 0.20 0.025 mg/L 1 Cadmium 7440-43-9 6010D ND 0.0050 mg/L 1 Chromium 7440-47-3 6010D ND 0.010 mg/L 1 Lead 7439-92-1 6010D ND 0.010 mg/L 1 Mercury 7439-97-6 7470A ND 0.00020 mg/L 1 Selenium 7782-49-2 6010D ND 0.020 mg/L 1 Silver 7440-22-4 6010D ND 0.010 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 11 of 58 Inorganic non-metals Client:ERM NC, Inc. Laboratory ID:WK08047-004 Description: MW-02D-WG-20211101 Matrix: Aqueous Date Sampled: 11/01/2021 1715 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Sulfate) 300.0 1 11/10/2021 0218 AMR 21980 1 (TDS) SM 2540C-2011 1 11/10/2021 1920 SJL 22041 CAS Analytical Parameter Number Method Result Q LOQ Units Run Sulfate 300.0 1.1 1.0 mg/L 1 TDS SM 254OC-2011 320 H 25 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 12 of 58 Metals Client:ERM NC, Inc. Laboratory ID:WK08047-004 Description: MW-02D-WG-20211101 Matrix: Aqueous Date Sampled: 11/01/2021 1715 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 11/12/2021 1059 CMS2 11/11/2021 1442 22159 1 3005A 601OD 1 11/10/2021 1720 KSH2 11/09/2021 1158 21737 Parameter CAS Analytical Number Method Result Q LOQ Units Run Arsenic 7440-38-2 6010D ND 0.015 mg/L 1 Barium 7440-39-3 6010D 0.066 0.025 mg/L 1 Cadmium 7440-43-9 6010D ND 0.0050 mg/L 1 Chromium 7440-47-3 6010D ND 0.010 mg/L 1 Lead 7439-92-1 6010D ND 0.010 mg/L 1 Mercury 7439-97-6 7470A ND 0.00020 mg/L 1 Selenium 7782-49-2 6010D ND 0.020 mg/L 1 Silver 7440-22-4 6010D ND 0.010 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 13 of 58 Inorganic non-metals Client:ERM NC, Inc. Laboratory ID:WK08047-005 Description: MW-03-WG-20211101 Matrix: Aqueous Date Sampled:11/02/2021 1320 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Sulfate) 300.0 5 11/10/2021 0237 AMR 21980 1 (TDS) SM 2540C-2011 1 11/09/2021 2000 MSG 21861 CAS Analytical Parameter Number Method Result Q LOQ Units Run Sulfate 300.0 810 5.0 mg/L 1 TDS SM 254OC-2011 2700 25 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 14 of 58 Metals Client:ERM NC, Inc. Laboratory ID:WK08047-005 Description: MW-03-WG-20211101 Matrix: Aqueous Date Sampled:11/02/2021 1320 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 11/12/2021 1101 CMS2 11/11/2021 1442 22159 1 3005A 601OD 1 11/10/2021 1723 KSH2 11/09/2021 1158 21737 Parameter CAS Analytical Number Method Result Q LOQ Units Run Arsenic 7440-38-2 6010D ND 0.015 mg/L 1 Barium 7440-39-3 6010D ND 0.025 mg/L 1 Cadmium 7440-43-9 6010D ND 0.0050 mg/L 1 Chromium 7440-47-3 6010D ND 0.010 mg/L 1 Lead 7439-92-1 6010D ND 0.010 mg/L 1 Mercury 7439-97-6 7470A ND 0.00020 mg/L 1 Selenium 7782-49-2 6010D ND 0.020 mg/L 1 Silver 7440-22-4 6010D ND 0.010 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 15 of 58 Inorganic non-metals Client:ERM NC, Inc. Laboratory ID:WK08047-006 Description: MW-04-WG-20211101 Matrix: Aqueous Date Sampled:11/02/2021 1325 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Sulfate) 300.0 1 11/10/2021 0256 AMR 21980 1 (TDS) SM 2540C-2011 1 11/09/2021 2000 MSG 21861 CAS Analytical Parameter Number Method Result Q LOQ Units Run Sulfate 300.0 25 1.0 mg/L 1 TDS SM 254OC-2011 230 25 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 16 of 58 Metals Client:ERM NC, Inc. Laboratory ID:WK08047-006 Description: MW-04-WG-20211101 Matrix: Aqueous Date Sampled:11/02/2021 1325 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 11/12/2021 1104 CMS2 11/11/2021 1442 22159 1 3005A 601OD 1 11/10/2021 1727 KSH2 11/09/2021 1158 21737 Parameter CAS Analytical Number Method Result Q LOQ Units Run Arsenic 7440-38-2 6010D 0.035 0.015 mg/L 1 Barium 7440-39-3 6010D 0.025 0.025 mg/L 1 Cadmium 7440-43-9 6010D ND 0.0050 mg/L 1 Chromium 7440-47-3 6010D ND 0.010 mg/L 1 Lead 7439-92-1 6010D ND 0.010 mg/L 1 Mercury 7439-97-6 7470A ND 0.00020 mg/L 1 Selenium 7782-49-2 6010D ND 0.020 mg/L 1 Silver 7440-22-4 6010D ND 0.010 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 17 of 58 Inorganic non-metals Client:ERM NC, Inc. Laboratory ID:WK08047-007 Description: MW-05RS-WG-20211101 Matrix: Aqueous Date Sampled: 11/01/2021 1115 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Sulfate) 300.0 1 11/10/2021 1918 AMR 22170 1 (TDS) SM 2540C-2011 1 11/09/2021 2000 MSG 21861 CAS Analytical Parameter Number Method Result Q LOQ Units Run Sulfate 300.0 2.8 1.0 mg/L 1 TDS SM 254OC-2011 300 H 25 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 18 of 58 Metals Client:ERM NC, Inc. Laboratory ID:WK08047-007 Description: MW-05RS-WG-20211101 Matrix: Aqueous Date Sampled: 11/01/2021 1115 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 11/12/2021 1112 CMS2 11/11/2021 1442 22159 1 3005A 601OD 1 11/10/2021 1731 KSH2 11/09/2021 1158 21737 Parameter CAS Analytical Number Method Result Q LOQ Units Run Arsenic 7440-38-2 6010D ND 0.015 mg/L 1 Barium 7440-39-3 6010D ND 0.025 mg/L 1 Cadmium 7440-43-9 6010D ND 0.0050 mg/L 1 Chromium 7440-47-3 6010D ND 0.010 mg/L 1 Lead 7439-92-1 6010D ND 0.010 mg/L 1 Mercury 7439-97-6 7470A ND 0.00020 mg/L 1 Selenium 7782-49-2 6010D ND 0.020 mg/L 1 Silver 7440-22-4 6010D ND 0.010 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 19 of 58 Inorganic non-metals Client:ERM NC, Inc. Laboratory ID:WK08047-008 Description: MW-05RD-WG-20211101 Matrix: Aqueous Date Sampled: 11/01/2021 1140 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Sulfate) 300.0 1 11/10/2021 1937 AMR 22170 1 (TDS) SM 2540C-2011 1 11/09/2021 2000 MSG 21861 CAS Analytical Parameter Number Method Result Q LOQ Units Run Sulfate 300.0 6.0 1.0 mg/L 1 TDS SM 254OC-2011 190 H 25 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 20 of 58 Metals Client:ERM NC, Inc. Laboratory ID:WK08047-008 Description: MW-05RD-WG-20211101 Matrix: Aqueous Date Sampled: 11/01/2021 1140 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 11/12/2021 1115 CMS2 11/11/2021 1442 22159 1 3005A 601OD 1 11/10/2021 1735 KSH2 11/09/2021 1158 21737 Parameter CAS Analytical Number Method Result Q LOQ Units Run Arsenic 7440-38-2 6010D ND 0.015 mg/L 1 Barium 7440-39-3 6010D ND 0.025 mg/L 1 Cadmium 7440-43-9 6010D ND 0.0050 mg/L 1 Chromium 7440-47-3 6010D ND 0.010 mg/L 1 Lead 7439-92-1 6010D ND 0.010 mg/L 1 Mercury 7439-97-6 7470A ND 0.00020 mg/L 1 Selenium 7782-49-2 6010D ND 0.020 mg/L 1 Silver 7440-22-4 6010D ND 0.010 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 21 of 58 Inorganic non-metals Client:ERM NC, Inc. Laboratory ID:WK08047-009 Description: MW-06-WG-20211101 Matrix: Aqueous Date Sampled:11/02/2021 1410 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Sulfate) 300.0 5 11/10/2021 1956 AMR 22170 1 (TDS) SM 2540C-2011 1 11/09/2021 2000 MSG 21861 CAS Analytical Parameter Number Method Result Q LOQ Units Run Sulfate 300.0 790 5.0 mg/L 1 TDS SM 254OC-2011 5500 25 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 22 of 58 Metals Client:ERM NC, Inc. Laboratory ID:WK08047-009 Description: MW-06-WG-20211101 Matrix: Aqueous Date Sampled:11/02/2021 1410 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 11/12/2021 1118 CMS2 11/11/2021 1442 22159 1 3005A 601OD 1 11/10/2021 1739 KSH2 11/09/2021 1158 21737 Parameter CAS Analytical Number Method Result Q LOQ Units Run Arsenic 7440-38-2 6010D ND 0.015 mg/L 1 Barium 7440-39-3 6010D ND 0.025 mg/L 1 Cadmium 7440-43-9 6010D ND 0.0050 mg/L 1 Chromium 7440-47-3 6010D ND 0.010 mg/L 1 Lead 7439-92-1 6010D ND 0.010 mg/L 1 Mercury 7439-97-6 7470A ND 0.00020 mg/L 1 Selenium 7782-49-2 6010D ND 0.020 mg/L 1 Silver 7440-22-4 6010D ND 0.010 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 23 of 58 Inorganic non-metals Client:ERM NC, Inc. Laboratory ID:WK08047-010 Description: MW-07-WG-20211101 Matrix: Aqueous Date Sampled: 11/01/2021 1415 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Sulfate) 300.0 5 11/10/2021 2015 AMR 22170 1 (TDS) SM 2540C-2011 1 11/09/2021 2000 MSG 21861 CAS Analytical Parameter Number Method Result Q LOQ Units Run Sulfate 300.0 700 5.0 mg/L 1 TDS SM 254OC-2011 10000 H 25 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 24 of 58 Metals Client:ERM NC, Inc. Laboratory ID:WK08047-010 Description: MW-07-WG-20211101 Matrix: Aqueous Date Sampled: 11/01/2021 1415 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 11/12/2021 1120 CMS2 11/11/2021 1442 22159 1 3005A 601OD 1 11/10/2021 1239 KSH2 11/10/2021 0143 21875 Parameter CAS Analytical Number Method Result Q LOQ Units Run Arsenic 7440-38-2 6010D 0.090 0.015 mg/L 1 Barium 7440-39-3 6010D 0.13 0.025 mg/L 1 Cadmium 7440-43-9 6010D ND 0.0050 mg/L 1 Chromium 7440-47-3 6010D ND 0.010 mg/L 1 Lead 7439-92-1 6010D 0.27 0.010 mg/L 1 Mercury 7439-97-6 7470A ND 0.00020 mg/L 1 Selenium 7782-49-2 6010D ND 0.020 mg/L 1 Silver 7440-22-4 6010D ND 0.010 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 25 of 58 Inorganic non-metals Client:ERM NC, Inc. Laboratory ID:WK08047-011 Description: MW-08-WG-20211101 Matrix: Aqueous Date Sampled: 11/01/2021 1415 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Sulfate) 300.0 5 11/10/2021 2034 AMR 22170 1 (TDS) SM 2540C-2011 1 11/09/2021 2000 MSG 21861 CAS Analytical Parameter Number Method Result Q LOQ Units Run Sulfate 300.0 610 5.0 mg/L 1 TDS SM 254OC-2011 7300 H 25 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 26 of 58 Metals Client:ERM NC, Inc. Laboratory ID:WK08047-011 Description: MW-08-WG-20211101 Matrix: Aqueous Date Sampled: 11/01/2021 1415 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 11/12/2021 1123 CMS2 11/11/2021 1442 22159 1 3005A 601OD 1 11/10/2021 1307 KSH2 11/10/2021 0143 21875 Parameter CAS Analytical Number Method Result Q LOQ Units Run Arsenic 7440-38-2 6010D 0.070 0.015 mg/L 1 Barium 7440-39-3 6010D 0.089 0.025 mg/L 1 Cadmium 7440-43-9 6010D ND 0.0050 mg/L 1 Chromium 7440-47-3 6010D ND 0.010 mg/L 1 Lead 7439-92-1 6010D 0.24 0.010 mg/L 1 Mercury 7439-97-6 7470A ND 0.00020 mg/L 1 Selenium 7782-49-2 6010D ND 0.020 mg/L 1 Silver 7440-22-4 6010D ND 0.010 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 27 of 58 Inorganic non-metals Client:ERM NC, Inc. Laboratory ID:WK08047-012 Description: SW-01 -WS-2021 1101 Matrix: Aqueous Date Sampled:11/02/2021 1420 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Sulfate) 300.0 1 11/10/2021 2053 AMR 22170 1 (TDS) SM 2540C-2011 1 11/09/2021 2000 MSG 21861 CAS Analytical Parameter Number Method Result Q LOQ Units Run Sulfate 300.0 2.3 1.0 mg/L 1 TDS SM 254OC-2011 75 25 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 28 of 58 Metals Client:ERM NC, Inc. Laboratory ID:WK08047-012 Description: SW-01 -WS-2021 1101 Matrix: Aqueous Date Sampled:11/02/2021 1420 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 11/12/2021 1126 CMS2 11/11/2021 1442 22159 1 3005A 601OD 1 11/10/2021 1311 KSH2 11/10/2021 0143 21875 Parameter CAS Analytical Number Method Result Q LOQ Units Run Arsenic 7440-38-2 6010D ND 0.015 mg/L 1 Barium 7440-39-3 6010D 0.027 0.025 mg/L 1 Cadmium 7440-43-9 6010D ND 0.0050 mg/L 1 Chromium 7440-47-3 6010D ND 0.010 mg/L 1 Lead 7439-92-1 6010D ND 0.010 mg/L 1 Mercury 7439-97-6 7470A ND 0.00020 mg/L 1 Selenium 7782-49-2 6010D ND 0.020 mg/L 1 Silver 7440-22-4 6010D ND 0.010 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 29 of 58 Inorganic non-metals Client:ERM NC, Inc. Laboratory ID:WK08047-013 Description: SW-02-WS-20211101 Matrix: Aqueous Date Sampled: 11/01/2021 1640 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Sulfate) 300.0 1 11/10/2021 2112 AMR 22170 1 (TDS) SM 2540C-2011 1 11/10/2021 1920 SJL 22041 CAS Analytical Parameter Number Method Result Q LOQ Units Run Sulfate 300.0 5.3 1.0 mg/L 1 TDS SM 254OC-2011 110 H 25 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 30 of 58 Metals Client:ERM NC, Inc. Laboratory ID:WK08047-013 Description: SW-02-WS-20211101 Matrix: Aqueous Date Sampled: 11/01/2021 1640 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 11/12/2021 1128 CMS2 11/11/2021 1442 22159 1 3005A 601OD 1 11/10/2021 1315 KSH2 11/10/2021 0143 21875 Parameter CAS Analytical Number Method Result Q LOQ Units Run Arsenic 7440-38-2 6010D ND 0.015 mg/L 1 Barium 7440-39-3 6010D 0.048 0.025 mg/L 1 Cadmium 7440-43-9 6010D ND 0.0050 mg/L 1 Chromium 7440-47-3 6010D ND 0.010 mg/L 1 Lead 7439-92-1 6010D ND 0.010 mg/L 1 Mercury 7439-97-6 7470A ND 0.00020 mg/L 1 Selenium 7782-49-2 6010D ND 0.020 mg/L 1 Silver 7440-22-4 6010D ND 0.010 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 31 of 58 Inorganic non-metals Client:ERM NC, Inc. Laboratory ID:WK08047-014 Description: SW-03-WS-20211101 Matrix: Aqueous Date Sampled: 11/01/2021 1430 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Sulfate) 300.0 1 11/10/2021 2209 AMR 22170 1 (TDS) SM 2540C-2011 1 11/09/2021 2000 MSG 21861 CAS Analytical Parameter Number Method Result Q LOQ Units Run Sulfate 300.0 9.3 1.0 mg/L 1 TDS SM 254OC-2011 82 H 25 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 32 of 58 Metals Client:ERM NC, Inc. Laboratory ID:WK08047-014 Description: SW-03-WS-20211101 Matrix: Aqueous Date Sampled: 11/01/2021 1430 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 11/12/2021 1131 CMS2 11/11/2021 1442 22159 1 3005A 601OD 1 11/10/2021 1318 KSH2 11/10/2021 0143 21875 Parameter CAS Analytical Number Method Result Q LOQ Units Run Arsenic 7440-38-2 6010D ND 0.015 mg/L 1 Barium 7440-39-3 6010D 0.026 0.025 mg/L 1 Cadmium 7440-43-9 6010D ND 0.0050 mg/L 1 Chromium 7440-47-3 6010D ND 0.010 mg/L 1 Lead 7439-92-1 6010D ND 0.010 mg/L 1 Mercury 7439-97-6 7470A ND 0.00020 mg/L 1 Selenium 7782-49-2 6010D ND 0.020 mg/L 1 Silver 7440-22-4 6010D ND 0.010 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 33 of 58 Inorganic non-metals Client:ERM NC, Inc. Laboratory ID:WK08047-015 Description: FD-01-WG-20211101 Matrix: Aqueous Date Sampled:11/01/2021 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Sulfate) 300.0 5 11/10/2021 2228 AMR 22170 1 (TDS) SM 2540C-2011 1 11/09/2021 2000 MSG 21861 CAS Analytical Parameter Number Method Result Q LOQ Units Run Sulfate 300.0 410 5.0 mg/L 1 TDS SM 254OC-2011 7000 H 25 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 34 of 58 Metals Client:ERM NC, Inc. Laboratory ID:WK08047-015 Description: FD-01-WG-20211101 Matrix: Aqueous Date Sampled:11/01/2021 Date Received: 11 /04/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 11/12/2021 1134 CMS2 11/11/2021 1442 22159 1 3005A 601OD 1 11/10/2021 1322 KSH2 11/10/2021 0143 21875 Parameter CAS Analytical Number Method Result Q LOQ Units Run Arsenic 7440-38-2 6010D ND 0.015 mg/L 1 Barium 7440-39-3 6010D 0.27 0.025 mg/L 1 Cadmium 7440-43-9 6010D ND 0.0050 mg/L 1 Chromium 7440-47-3 6010D ND 0.010 mg/L 1 Lead 7439-92-1 6010D 0.031 0.010 mg/L 1 Mercury 7439-97-6 7470A ND 0.00020 mg/L 1 Selenium 7782-49-2 6010D ND 0.020 mg/L 1 Silver 7440-22-4 6010D ND 0.010 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 35 of 58 QC Summary Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 36 of 58 Inorganic non-metals - MB Sample ID: WQ21861-001 Matrix: Aqueous Batch: 21861 Analytical Method: SM 2540C-2011 Parameter Result Q Dil LOQ Units Analysis Date TDS ND 1 25 mg/L 11/09/2021 1903 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 37 of 58 Inorganic non-metals - LCS Sample ID: WQ21861-002 Matrix: Aqueous Batch: 21861 Analytical Method: SM 2540C-2011 Spike Amount Result %Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date TDS 1500 1500 1 101 90-110 11 /09/2021 1903 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 38 of 58 Inorganic non-metals - MB Sample ID: WQ21980-001 Matrix: Aqueous Batch: 21980 Analytical Method: 300.0 Parameter Result Q Dil LOQ Units Analysis Date Sulfate ND 1 1.0 mg/L 11 /09/2021 1806 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 39 of 58 Inorganic non-metals - LCS Sample ID: WQ21980-002 Matrix: Aqueous Batch: 21980 Analytical Method: 300.0 Spike Amount Result %Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Sulfate 20 20 1 102 90-110 11/09/2021 1844 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 40 of 58 Inorganic non-metals - MS Sample ID: WK08047-006MS Matrix: Aqueous Batch: 21980 Analytical Method: 300.0 Sample Spike Amount Amount Result %Rec Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Sulfate 25 10 34 1 98 90-110 11/10/2021 0315 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 41 of 58 Inorganic non-metals - MSD Sample ID: WK08047-OO6MD Matrix: Aqueous Batch: 21980 Analytical Method: 300.0 Sample Spike Amount Amount Result %Rec % RPD Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date Sulfate 25 10 35 1 100 0.55 90-110 20 11/10/2021 0334 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 42 of 58 Inorganic non-metals - MB Sample ID: WQ22041-001 Matrix: Aqueous Batch:22041 Analytical Method: SM 2540C-2011 Parameter Result Q Dil LOQ Units Analysis Date TDS ND 1 25 mg/L 11/10/2021 1920 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 43 of 58 Inorganic non-metals - LCS Sample ID: WQ22041-002 Matrix: Aqueous Batch:22041 Analytical Method: SM 2540C-2011 Spike Amount Result %Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date TDS 1500 1500 1 101 90-110 11/10/2021 1920 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 44 of 58 Inorganic non-metals - MB Sample ID: WQ22170-001 Matrix: Aqueous Batch: 22170 Analytical Method: 300.0 Parameter Result Q Dil LOQ Units Analysis Date Sulfate ND 1 1.0 mg/L 11/10/2021 1728 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 45 of 58 Inorganic non-metals - LCS Sample ID: WQ22170-002 Matrix: Aqueous Batch: 22170 Analytical Method: 300.0 Spike Amount Result %Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Sulfate 20 20 1 102 90-110 11/10/2021 1900 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 46 of 58 Metals - MB Sample ID: WQ21737-001 Matrix: Aqueous Batch:21737 Prep Method: 3005A Analytical Method: 6010D Prep Date: 11/09/2021 1158 Parameter Result Q Dil LOQ Units Analysis Date Arsenic ND 1 0.015 mg/L 11/10/2021 1547 Barium ND 1 0.025 mg/L 11/10/2021 1547 Cadmium ND 1 0.0050 mg/L 11/10/2021 1547 Chromium ND 1 0.010 mg/L 11/11/2021 1058 Lead ND 1 0.010 mg/L 11/10/2021 1547 Selenium ND 1 0.020 mg/L 11/10/2021 1547 Silver ND 1 0.010 mg/L 11/10/2021 1547 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 47 of 58 Metals - LCS Sample ID: WQ21737-002 Matrix: Aqueous Batch: 21737 Prep Method: 3OO5A Analytical Method: 6010D Prep Date: 11/09/2021 1158 Spike Amount Result %Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Arsenic 0.40 0.36 1 89 80-120 11/10/2021 1551 Barium 2.0 1.9 1 95 80-120 11/10/2021 1551 Cadmium 0.40 0.38 1 95 80-120 11/10/2021 1551 Chromium 2.0 1.9 1 96 80-120 11/11/2021 1101 Lead 0.40 0.38 1 96 80-120 11/10/2021 1551 Selenium 0.40 0.38 1 94 80-120 11/10/2021 1551 Silver 0.40 0.38 1 96 80-120 11/10/2021 1551 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 48 of 58 Metals - MB Sample ID: WQ21875-001 Matrix: Aqueous Batch: 21875 Prep Method: 3005A Analytical Method: 6010D Prep Date: 11/10/2021 0143 Parameter Result Q Dil LOQ Units Analysis Date Arsenic ND 1 0.015 mg/L 11/10/2021 1221 Barium ND 1 0.025 mg/L 11/10/2021 1221 Cadmium ND 1 0.0050 mg/L 11/10/2021 1221 Chromium ND 1 0.010 mg/L 11/10/2021 1221 Lead ND 1 0.010 mg/L 11/10/2021 1221 Selenium ND 1 0.020 mg/L 11/10/2021 1221 Silver ND 1 0.010 mg/L 11/10/2021 1221 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 49 of 58 Metals - LCS Sample ID: WQ21875-002 Matrix: Aqueous Batch: 21875 Prep Method: 3005A Analytical Method: 6010D Prep Date: 11/10/2021 0143 Spike Amount Result %Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Arsenic 0.40 0.41 1 103 80-120 11/10/2021 1225 Barium 2.0 1.9 1 96 80-120 11/10/2021 1225 Cadmium 0.40 0.37 1 93 80-120 11/10/2021 1225 Chromium 2.0 2.0 1 100 80-120 11/10/2021 1225 Lead 0.40 0.40 1 99 80-120 11/10/2021 1225 Selenium 0.40 0.38 1 94 80-120 11/10/2021 1225 Silver 0.40 0.40 1 99 80-120 11/10/2021 1225 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 50 of 58 Metals - MS Sample ID: WK08047-01OMS Matrix: Aqueous Batch: 21875 Prep Method: 3005A Analytical Method: 6010D Prep Date: 11/10/2021 0143 Sample Spike Amount Amount Result %Rec Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Arsenic 0.090 0.40 0.56 1 118 75-125 11/10/2021 1243 Barium 0.13 2.0 2.0 1 95 75-125 11/10/2021 1243 Cadmium ND 0.40 0.42 1 104 75-125 11/10/2021 1243 Chromium ND 2.0 1.8 1 92 75-125 11/10/2021 1243 Lead 0.27 0.40 0.64 1 93 75-125 11/10/2021 1243 Selenium ND 0.40 0.43 1 107 75-125 11/10/2021 1243 Silver ND 0.40 0.40 1 99 75-125 11/10/2021 1243 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 51 of 58 Metals - MSD Sample ID: WK08047-01OMD Matrix: Aqueous Batch: 21875 Prep Method: 3005A Analytical Method: 6010D Prep Date: 11/10/2021 0143 Sample Spike Amount Amount Result %Rec % RPD Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date Arsenic 0.090 0.40 0.56 1 117 0.45 75-125 20 11/10/2021 1248 Barium 0.13 2.0 2.0 1 92 3.0 75-125 20 11/10/2021 1248 Cadmium ND 0.40 0.40 1 101 3.1 75-125 20 11/10/2021 1248 Chromium ND 2.0 1.8 1 92 0.15 75-125 20 11/10/2021 1248 Lead 0.27 0.40 0.63 1 91 1.4 75-125 20 11/10/2021 1248 Selenium ND 0.40 0.43 1 107 0.40 75-125 20 11/10/2021 1248 Silver ND 0.40 0.39 1 99 0.58 75-125 20 11/10/2021 1248 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 52 of 58 Metals - MB Sample ID: WQ22159-001 Matrix: Aqueous Batch: 22159 Prep Method: Analytical Method: 7470A Prep Date: 11/11/2021 1442 Parameter Result Q Dil LOQ Units Analysis Date Mercury ND 1 0.00020 mg/L 11/12/2021 1043 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 53 of 58 Metals - LCS Sample ID: WQ22159-002 Matrix: Aqueous Batch: 22159 Prep Method: Analytical Method: 7470A Prep Date: 11/11/2021 1442 Spike Amount Result %Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Mercury 0.0020 0.0019 1 93 80-120 11/12/2021 1045 LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % = RSD is out of criteria + = RPD is out of criteria Note: Calculations are performed before rounding to avoid round -off errors in calculated results Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 54 of 58 Chain of Custody and Miscellaneous Documents Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 55 of 58 PACE ANALYTICAL SERVICES, LLC i f�RE I9 i � I I r x � h 7 11 �+ a ILLI @ 3 = O m2r n Lb L2 ems} {`•, a 4N! A i � tx X X k J X 1'k i 2 � J i Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 56 of 58 PACE ANALYTICAL SERVICES, LLC CIQ OWN X -Ayl IL Z= L w too! n -saw a IR 9 L Eli VS ELD �7-1 rj C�7 N Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 57 of 58 PACE ANALYTICAL SERVICES, LLC Samples lkerelpt Cheallst (SRCI (ME0018C-1$j Revised;9129/202D Ar tj+lreaf lss aingAuthority- PXe EW - WCOt, pagc I of 1 sample Receipt Checklist (SRC) C L=eut. ERq Cooler Tn"crtcd byjd9ta: Jzq I f 11,1O&'2C21 Lot #: Vly ll {U47 twieanSofrtx•,eipt: ©Pace I=e��l Tip;; ve F'edEx Other; :J Ym ; Na I, Were1`1SWd Sea] sp:C CTI:❑rttkCook{"' 'd Yes Na NAt 2, TFoi stud seaCa u�re I�senl, uerr th intact and unbrolugi? pH Strip ID- zt,ssx _ Cl1Enrim Strip J D: .__ TcSfed ,. ,cH Or[gina[temperature upon r>=pp,pt!Derived (Corrected) temperaWl'a UIFWI reeeipL V-S-olid Snay-Cup [D- NJ6 oC NA r• NA KA + NA aC NA r NA CC — Method- LlTa j?c.rarure Bank 6L auis( 13+xtlo IR Gun ID, its Gun OoriwAi-an Factor: " "C Method ul rwJarit: � Wet ]ce ❑ Ice flacks rw acks L1 Drou None — Yes No �i A [fr rnpeiotLLYr ❑Erin} c4oleC o�€Ceeded b.4'C, was ProjeCt [wfel, erA1o#ificd° P.M wah N116FICri by; phone t entfl +' Flo-facc (c rcle one). J No NA 4, Is the €oanrnomiul ccw Ices peeking s.in attadicd to tJiis fonu" I Yes No {. 14'crc mts�r cuaitrkdy j�J'ooedtet_Es (ra.i,7yr,i;l�4xl�rccaived} follovt ad? Yefi 7. No d, Were sniff pie [Ds 1 iy Led on the COM + Xes LD NC} No 1. Ww sample 1Ds listed an allsamplc OOi]taiiiars? Yes S. 1WEi collection date & limit list d on the O0C9 0 YES No 9. Wit; oReudpn date limo I:stcd an aC mmpie =tairiers? LO, Lhd ali COn�aiher label information (ID, dulr:, time) agree Witt rite Coe? ! Yes Mo ,e Yfe Rio 11. Ware tests err he PCTR:TmPtl listed oil the COC? No 12. Did all samples aRL,,re in the prgpor Qvntai sari fa, imch [csl anrVrW in good c611ditlon (unLrckeu, lids bu, Clc,)'? I Yes j No 13, W tad: u� samp]e vnli ime, available? es +2 N t} 114. WOLT all ar 49 hours, wh]Ghcver anm:s iflrst? Ycs No IS. We --any eamul4s ContaineJS riiSS[rsg+excess (circle nee) NrrmplPs Not Ji3red on COC;i ElYsr has �N• 16. For VOA a,id RSK-175 samples. were hlthl,ies present �1p siz6' ('r;"or Timm in diamprer; in any of the VGA r615? Yes No NA li- Wt3,L -Al 13RO,tr auls,'nutrient sarn ]gsroceivemda[ aPAof,� T2 18. Wercall cyanide sam les zepCivod tale a 2 and ia,[rda cram Les reLA�ivrd Ld u pH YLs No � NA © Yes ❑ N+r ❑J NA 19, ",all app 'C8 Le NFI�,fT FChrcyartFde pJrecta Il625,11608.3 -Sn gr I.) SAm p; ixs free of - re€idual efilurim? . Were c[kiit mmarkslreyuesls (i,e, requested dilutions, LN4SIK1811 designations, etc.-,} corract! Lrpnscribcd rim Tire 7 Y � ir,#o the carinsarlt see:irrn in I,)N]S, 21- Was 1hn {rote m°mLr�r [istntl +�t ihs container Jai?el? If . QU.0to ii AIaa ❑ Yes ❑ # ` I� IA 'J yCS1 LJ N., 1 �Sarnple Prr_:mratian (Mkis[ bacompicted for any sarrplo(sj Mocu'rectlp pnewrverlorwv h hcsdspace.) -- S�rrnplc(s) Y WCrr received incorrxtl3y preserved ale¢ vwwo u0jimW acti�ardtnrly ill %111Pic ]1:Cc[v[n_u ►eith ��� rnL of circle one: H2SO4. HAW, :10, Knoll using Sit f NA, Tirhr, u-/ prcaervZion If more than ono przs�irwatjvc is neaded, p1e:i5n note lit the cainrrienib 13Cl15w. `1'7[1'lul�1 NA were 70teiwdWith bubb.es irni Fndiami:lar, R arriples(s) rJA WeTe recei 4Vd w [lh TRC > 0.5 m o�L (If *19 fs na) and were 11ji1sud acc4?rdjngly :n sample receiving with sodjuF:t thiosj[ tte (Na2Sa�) with Shealy Jf}; NA R bueadc libels applied by; a�t1 jam- 111D8,�Tnx; Commen Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 58 of 58 ERM has over 160 offices across the following countries and territories worldwide Argentina The Netherlands ERM's Charlotte, NC Office Australia New Zealand ERM NC, Inc. 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