NCD003162542_Badin Business Park_Corrective Action_20220127

Badin Business Park LLC

Highway 740
P.O. Box 576
Badin, NC 28009
Tel: [phone]

January 27, 2022

ATTN: Derek Denard
Division of Water Resources
WQ Permitting Section – NPDES
1617 Mail Service Center
Raleigh, NC 27699-1617

Re: Response to Information Request
Badin Business Park LLC
NPDES No. NC0004308
Stanly County

Mr. Denard:

Please find attached Badin Business Park LLC’s responses to the Division of Water Resources request for
information regarding the recent soil removal project, dated December 20, 2021. As you will see in the
detailed responses below, this effort was part of our ongoing efforts to investigate and address potential
sources of constituents on the site, particularly with regard to Outfall 005.
For ease of discussion and mutual understanding, each request raised by your office is presented below
in bold and italics and is followed by Badin Business Park’s (BBP) response. We hope you find the
following sufficient to address your concerns. Please contact me should you have additional questions or
concerns regarding this project.

1. Provide a map depicting the footprint of the excavated area and reasons and supporting data for
the removal of the soils.
Response: The excavation of soils from an area near the former Bath Mill (Building 204H) was conducted
during the week of October 11, 2021 as a positive step towards BBP’s commitment to investigate and
address potential sources of constituents quantified in aqueous samples collected at Outfall 005. A
depiction of the excavated area is provided on Figures 1 & 2 as Attachment 1. The basis for pursing the
project is as follows.
In March 2020, an electromagnetic (EM) geophysical evaluation was performed to assess for the
presence of previously unknown sources and/or pathways for constituents to enter the Outfall 005
storm sewer system. The geophysical survey was conducted on an approximate eleven-acre area west of
the former potrooms and an approximate seven-acre area north of the former potrooms. The EM
method was selected due to its ability to detect variations in shallow subsurface soil conductivity,
variations in shallow groundwater conductivity, and metallic materials.
Results from the EM evaluation were suggestive of potential buried structures, materials, and
conductive porewater and/or groundwater. One EM response corresponded to the location of the
Mr. Derek Denard
January 29, 2022
Page 2

former Bath Mill where recovered bath material, a fluoride-bearing mixture from the aluminum
reduction pots, was crushed and repurposed. This location is also near the Outfall 005 storm sewer
system.
In June 2020, four test pits (TP-205 through TP-208, See Attachment 2 for location) were installed at the
former Bath Mill and samples of soil and water were collected for analysis. The results of the soil and
water analysis are presented in Tables 1 and 2 respectively. Additionally, the laboratory reports are
included as Attachment 3. These sample results and the corresponding proximity to the Outfall 005
storm sewer network confirmed that the former Bath Mill area had a potential to contribute to
constituents quantified in aqueous samples collected at Outfall 005.
Table 1 - Soil Sample Analytical Results
Location
Method Unit
TP-205 TP-205 TP-206 TP-206 TP-207 TP-207 TP-208 TP-208
Depth Below
Land Surface 2.0' 6.0' 2.0' 4.0' 2.0' 9.5' 2.0' 9.5'
Sample
Identification
ABP-TP-
205 (2.0)
ABP-TP-
205 (6.0)
ABP-TP-
206 (2.0)
ABP-TP-
206 (4.0)
ABP-TP-
207 (2.0)
ABP-TP-
207 (9.5)
ABP-TP-
208 (2.0)
ABP-TP-
208 (9.5)
Sample Date 6/29/2020 6/29/2020 6/29/2020 6/29/2020 6/29/2020 6/29/2020 6/29/2020 6/29/2020
Sample Time 13:15 13:50 14:05 14:20 15:00 15:10 15:30 15:40
ASTM Leach (D3987-85)
Fluoride 300.0 R2.1 mg/L 4.8 2.2 10 25 1.1 3.2 1.7 0.17
Total Cyanide
9012B /
9012B mg/L < 0.010 < 0.010 < 0.010 < 0.010 < 0.010 < 0.010 < 0.010 < 0.010
Total (Dry Weight)
Fluorine
ATSM D3761
/ 9056 mg/kg 101 197 811 7250 264 118 113 285
Fluoride
4500 F-B /
9056A mg/kg 190 610 690 NA NA NA NA NA
Total Cyanide
9012A /
9012A mg/kg < 0.071 < 0.075 0.068 0.13 < 0.064 0.074 < 0.068 < 0.076
Notes:
• Method indicates both preparation and analysis as applicable.
• Samples ABP-TP-206 (4.0), ABP-TP-207 (2.0), ABP-TP-207 (9.5), ABP-TP-208 (2.0) and ABP-TP-208 (9.5) were not
analyzed for fluoride using distillation method 4500.
Acronyms:
• mg/L - Milligrams per liter.
• mg/kg- Milligrams per kilogram.
• NA - Not analyzed.

Mr. Derek Denard
January 29, 2022
Page 3

Table 2 - Water Sample Analytical Results
Location
Method Unit
TP-205
Sample Identification ABP-TP-205W
Sample Date 6/29/2020
Sample Time 14:35
Total
Fluoride 300.0-1993 R2.1 mg/L 21
Total Cyanide D7511-12 mg/L < 0.0060

2. This map, or information in support of the map, must indicate the area of onsite excavation,
include the dimensions of the excavated area, the total volume of soils excavated, and any pre-
activity topographic survey of the excavated area that may exist, as well as a topographic survey
of the post excavation area.
Response: The approximate boundaries of the excavation area are shown on Figures 1 and 2. The
dimensions of the excavated area were approximately 80 feet (north/south) by 50 feet (east/west). The
pre-excavation topography is shown on Figure 1; the excavation area and adjacent areas are generally
flat. Soils to a depth of eight feet below grade (~1,200 In-Situ Cubic Yards) were excavated and loaded to
trucks. A total of 102 truckloads containing approximately 1,893 tons of solid materials were sent offsite
for disposal. An additional three to four feet of soils below the base of the excavation were excavated to
be mixed with quick lime at an approximate 5-10% dosing ratio by mass. The remaining excavation was
backfilled to match surrounding grade with native soils supplied from a local property (61608 Hwy 740
in Badin NC).

3. Explain how much surface area was disturbed (including access roads), detail what stabilization
measures/erosion control measures were used and if there were any erosion/turbidity issues with
the area of disturbance.
Response: See previous response for description of excavation area. Truck traffic was limited to existing
paved access roads. No erosion/turbidity issues were identified as construction occurred during a brief
period of time with no precipitation. Further, the excavation was performed such that potential runoff
would be directed inward into the excavation.

4. Detail how the excavated area was stabilized, if the area was back filled or capped, and where this
back fill material came from. Also, explain how the work area was ultimately managed such that
soils, turbidity, solids or other waste did not erode or otherwise course from the area of
disturbance to surface waters.
Response: See previous responses.
Mr. Derek Denard
January 29, 2022
Page 4

5. Detail how this work and the ultimate stabilization of the area was monitored during this effort.
Response: Monitoring of the construction activity was conducted periodically by both Site personnel
and a consultant.

6. A DWR NPDES file review did not reveal notification of this soil removal activity for the project
starting on October 12th. Please provide any prior notifications (e.g. including plans for this
material removal, information on truck traffic, ultimate disposal, or of this work occurring on
October 12, 2021).
Response: Notification of the investigation activity leading to the decision to remove this material was
first reviewed with DWR personnel during a meeting (conducted remotely) on February 18, 2021 to
review the Outfall 005 compliance status. The plan to remove the material was later discussed with
DWR personnel during a follow up meeting (conducted remotely) on June 15, 2021. The slides shared
during the meetings along with the respective meeting invitations are attached for reference as
Attachment 2. During both meetings, there was a general recognition that the removal could be a self-
implemented activity given the facts of the matter. A courtesy call was made to the Division of Waste
Management (DWM) the week prior to keep the DWM apprised of on-site activity.

7. Include a photographic record of the excavation area prior to excavation (if one exists) and a
photographic record of the current site conditions.
Response: Three photos are provided. One prior to excavation, one during excavation, and one post
excavation.
Pre-Excavation Photo (Taken June 2020)

Mr. Derek Denard
January 29, 2022
Page 5

Representative Open Excavation Photo (Taken Oct 14, 2021)

Post Excavation Photo (Taken Jan 10, 2022)

8. Provide all sampling results and laboratory analytical documentation of the excavated soils.
Response: See previous response for a summary table of investigative results and reference to the
laboratory reports.

9. Provide a complete record of the NPDES monitoring that occurred during and after the excavation
activities and identify any changes that may have occurred because of the soil disturbance.
Mr. Derek Denard
January 29, 2022
Page 6

Response: No changes were observed correlated to this activity. NPDES monitoring prior, during, and
after the excavation activity has been documented in routine discharge monitoring reports (DMRs).

10. Provide documentation that the soil excavation did not impact an existing RCRA solid waste
management unit or area of concern.
Response: The excavation area is not associated with an existing RCRA solid Waste Management Unit or
Area of Concern. See the following figure which shows the location of the excavation area compared to
the location of the identified SWMUs (shown in blue).

Mr. Derek Denard
January 29, 2022
Page 7

11. Finally, please provide any data/information you provided and explain in your written response
the information you provided to the landfill, (Republic Services' Uwharrie Landfill in Montgomery
County, NC) as to the sample results and sources of this material for use as cover material.
Response:
A verbal inquiry for disposal of the soil and crushed concrete was first made to the landfill
representative by telephone in early March 2021 followed by the submittal of analytical results by email
accompanied with the following text, “Attached is the analytical for the 1900 tons of soil and crushed
concrete. Can you provide a profile and disposal cost per ton for this material. They will deliver this
material over the course of one week approximately 80 -85 loads.” The analytical results, included as
Attachment 4, are of a representative sample composited from several grab samples collected from the
soils returned to the test pit locations at the bath mill area as previously described. The landfill provided
a Waste Profile by email for review and signature (see Attachment 5).

Sincerely,

Robyn L. Gross
Director, Asset Management Americas

Attachments:
Figures 1 & 2
Referenced Slides
Analytical Report – Soil & Water Samples
Analytical Report – Waste Characterization
Waste Profile

cc via email: Robert C. McDaniel, Hazardous Waste Section

Attachment 1
Figures 1 & 2

Attachment 2
Referenced Slides & Meeting Invitations

Extract from February 18, 2021 Presentation

Extract from June 15, 2021 Presentation

1
Gross, Robyn L.
Subject:Badin Business Park, LLC
Start:Thu 2/18/2021 3:00 PM
End:Thu 2/18/2021 4:30 PM
Recurrence:(none)
Meeting Status:Accepted
Organizer:Denard, Derek

In attendance with Badin Business Park, LLC:

Robyn Gross - Director, Alcoa Asset Management
Jason Mibroda - Alcoa Remediation Manager
Chelsea Cramer - Alcoa In-House Council
Rajat Ghosh - Alcoa Environmental Technical Manager
Steve Parascandola - Outside Council for Alcoa
Nathan Siria - FTN Associates, ENV consultant for Alcoa
Philip Massirer - FTN Associates, ENV consultant for Alcoa

In attendance with the NC DEQ Division of Water Resources (DWR):

Jeff Poupart, Section Chief - Water Quality Permitting Section (WQPS) DWR
Andrew Hargrove, Asst. General Counsel, Office of General Counsel - NCDEQ
Anna Gurney, PIO, Division of Water Resources
John Hennessy, Supervisor - Compliance & Expedited Permitting Unit WQPS DWR
Derek Denard, Environmental Specialist - Compliance & Expedited Permitting Unit
Mike Templeton, Acting Supervisor - Industrial Permitting Unit WQPS DWR
David Hill, Environmental Specialist II - Industrial Permitting Unit WQPS DWR
Corey Basinger, Regional Supervisor - WQ Regional Office Section - Mooresville RO
Andrew Pitner, Asst. Regional Supervisor - WQ Regional Office Section - Mooresville RO
Roberto Scheller, Environmental Specialist II -WQ Regional Office Section - Mooresville RO

If MS Teams is not working for us because of internet disruptions form the inclement ice storm, I have reserved 704-342-
6203 as a backup. I should be able to keep my cell phone charged and call into MS Teams to see if everyone can join.
Hopefully, we will have no issues. Stay safe.

Derek

________________________________________________________________________________
Microsoft Teams meeting
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________________________________________________________________________________
1
Gross, Robyn L.
Subject:Badin Park
Start:Tue 6/15/2021 9:00 AM
End:Tue 6/15/2021 10:30 AM
Recurrence:(none)
Meeting Status:Accepted
Organizer:Dowden, Doug
CAUTION: This email originated from outside of the organization. Do not click links or open attachments unless you recognize the
sender and know the content is safe.

A meeting to discuss Badin Park.

From: Gross, Robyn L. <[e-mail]>
Sent: Friday, June 11, 2021 11:46 AM
To: Dowden, Doug <[e-mail]>
Subject: RE: [External] RE: Badin Lake

CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment
to Report Spam.

Doug,
Here are some options for next week:
Tuesday 6/15 - any time between 8:00 AM and 1:00 PM
Wednesday 6/16 - any time between 8:00 AM and 10:00 AM or 1:00-3:00 PM

Can you check and let me know if any will work. Also, I can send a teams invite if you’d like us to.

Thanks and have a great weekend.
Robyn

________________________________________________________________________________
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Join on your computer or mobile app
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________________________________________________________________________________
Name Attendance Response
Dowden, Doug Meeting Organizer None
Gurney, Anna Required Attendee None
Denard, Derek Required Attendee None
Hill, David A Required Attendee None
Gross, Robyn L. Required Attendee None

Attachment 3
Laboratory Report – Soil & Water Samples
ANALYTICAL REPORT
Eurofins TestAmerica, Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-185778-1
Client Project/Site: Badin Business Park
For:
Civil & Environmental Consultants Inc
2704 Cherokee Farm Way
Suite 101
Knoxville, Tennessee 37920
Attn: Michael Worden
Authorized for release by:
7/23/2020 11:46:27 AM
Sheila Hoffman, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Method Summary
Job ID: 680-185778-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Method Method Description LaboratoryProtocol
SW8469056AAnions, Ion Chromatography TAL CF
EPAEPA 300.0 R2.1 Anions, Ion Chromatography TAL PIT
SW8469012ACyanide, Total and/or Amenable TAL SAV
SW846EPA 9012B Cyanide, Total andor Amenable TAL PIT
EPAMoisturePercent Moisture TAL SAV
SM4500 F-B Fluoride Distillation TAL CF
SW8469012ACyanide, Total and/or Amenable, Distillation TAL SAV
SW8469012BCyanide, Total and/or Amenable, Distillation TAL PIT
ASTMD3987-85 ASTM Leaching Procedure TAL PIT
Protocol References:
ASTM = ASTM International
EPA = US Environmental Protection Agency
SM = "Standard Methods For The Examination Of Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL CF = Eurofins TestAmerica, Cedar Falls, 3019 Venture Way, Cedar Falls, IA 50613, TEL [phone]
TAL PIT = Eurofins TestAmerica, Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins TestAmerica, Savannah
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Sample Summary
Job ID: 680-185778-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Lab Sample ID Client Sample ID ReceivedCollectedMatrix Asset ID
680-185778-1 ABP-TP-201 (5.8)Solid 06/29/20 08:50 07/01/20 10:00
680-185778-2 ABP-TP-202 (5.0)Solid 06/29/20 09:45 07/01/20 10:00
680-185778-3 ABP-TP-203 (6.0)Solid 06/29/20 11:00 07/01/20 10:00
680-185778-4 ABP-TP-204 (4.5)Solid 06/29/20 11:40 07/01/20 10:00
680-185778-5 ABP-TP-205 (2.0)Solid 06/29/20 13:15 07/01/20 10:00
680-185778-6 ABP-TP-205 (6.0)Solid 06/29/20 13:50 07/01/20 10:00
680-185778-7 ABP-TP-206 (2.0)Solid 06/29/20 14:05 07/01/20 10:00
680-185778-8 ABP-TP-206 (4.0)Solid 06/29/20 14:20 07/01/20 10:00
680-185778-9 ABP-TP-207 (2.0)Solid 06/29/20 15:00 07/01/20 10:00
680-185778-10 ABP-TP-207 (9.5)Solid 06/29/20 15:10 07/01/20 10:00
680-185778-11 ABP-TP-208 (2.0)Solid 06/29/20 15:30 07/01/20 10:00
680-185778-12 ABP-TP-208 (9.5)Solid 06/29/20 15:40 07/01/20 10:00
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Definitions/Glossary
Job ID: 680-185778-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Qualifiers
HPLC/IC
Qualifier Description
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
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Case Narrative
Client: Civil & Environmental Consultants Inc Job ID: 680-185778-1
Project/Site: Badin Business Park
Job ID: 680-185778-1
Laboratory: Eurofins TestAmerica, Savannah
Narrative
CASE NARRATIVE
Client: Civil & Environmental Consultants Inc
Project: Badin Business Park
Report Number: 680-185778-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
EXCEPTIONDuring the Fluoride distillation for method 4500 of ABP-TP-207(2.0), a violent reaction took place that caused the distillation apparatus to explode. The laboratory determined they would be unable to distill the remaining samples, due to EHS concerns. As a result, he
following samples were not analyzed for Fluoride using Fluoride distillation method 4500: ABP-TP-206 (4.0) (680-185778-8),
ABP-TP-207 (2.0) (680-185778-9), ABP-TP-207 (9.5) (680-185778-10), ABP-TP-208 (2.0) (680-185778-11) and ABP-TP-208 (9.5)
(680-185778-12).
RECEIPT
The samples were received on 07/01/2020; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 2.5º C and 3.2º C.
FLUORIDE
Samples ABP-TP-201 (5.8) (680-185778-1), ABP-TP-202 (5.0) (680-185778-2), ABP-TP-203 (6.0) (680-185778-3), ABP-TP-204 (4.5)
(680-185778-4), ABP-TP-205 (2.0) (680-185778-5), ABP-TP-205 (6.0) (680-185778-6), ABP-TP-206 (2.0) (680-185778-7), ABP-TP-206
(4.0) (680-185778-8), ABP-TP-207 (2.0) (680-185778-9), ABP-TP-207 (9.5) (680-185778-10), ABP-TP-208 (2.0) (680-185778-11) and
ABP-TP-208 (9.5) (680-185778-12) were analyzed for fluoride in accordance with ASTM D3987-85/EPA SW-846 Method 9038. The
samples were leached on 07/08/2020 and analyzed on 07/17/2020 and 07/19/2020.
Samples ABP-TP-204 (4.5) (680-185778-4)[5X], ABP-TP-206 (2.0) (680-185778-7)[10X] and ABP-TP-206 (4.0) (680-185778-8)[10X]
required dilution prior to analysis. The reporting limits have been adjusted accordingly.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL AND AMENABLE CYANIDE
Samples ABP-TP-201 (5.8) (680-185778-1), ABP-TP-202 (5.0) (680-185778-2), ABP-TP-203 (6.0) (680-185778-3), ABP-TP-204 (4.5)
(680-185778-4), ABP-TP-205 (2.0) (680-185778-5), ABP-TP-205 (6.0) (680-185778-6), ABP-TP-206 (2.0) (680-185778-7), ABP-TP-206
(4.0) (680-185778-8), ABP-TP-207 (2.0) (680-185778-9), ABP-TP-207 (9.5) (680-185778-10), ABP-TP-208 (2.0) (680-185778-11) and
ABP-TP-208 (9.5) (680-185778-12) were analyzed for total and amenable cyanide in accordance with EPA SW-846 Method 9012A. The
samples were prepared and analyzed on 07/13/2020.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CYANIDE (SOLID)
Samples ABP-TP-201 (5.8) (680-185778-1), ABP-TP-202 (5.0) (680-185778-2), ABP-TP-203 (6.0) (680-185778-3), ABP-TP-204 (4.5)
(680-185778-4), ABP-TP-205 (2.0) (680-185778-5), ABP-TP-205 (6.0) (680-185778-6), ABP-TP-206 (2.0) (680-185778-7), ABP-TP-206
(4.0) (680-185778-8), ABP-TP-207 (2.0) (680-185778-9), ABP-TP-207 (9.5) (680-185778-10), ABP-TP-208 (2.0) (680-185778-11) and
ABP-TP-208 (9.5) (680-185778-12) were analyzed for Cyanide (Solid) in accordance with 9012B. The samples were leached on
Eurofins TestAmerica, SavannahPage 5 of 39 7/23/2020
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Case Narrative
Client: Civil & Environmental Consultants Inc Job ID: 680-185778-1
Project/Site: Badin Business Park
Job ID: 680-185778-1 (Continued)
Laboratory: Eurofins TestAmerica, Savannah (Continued)
07/08/2020, and prepared and analyzed on 07/17/2020.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
FLUORIDE
Samples ABP-TP-201 (5.8) (680-185778-1), ABP-TP-202 (5.0) (680-185778-2), ABP-TP-203 (6.0) (680-185778-3), ABP-TP-204 (4.5)
(680-185778-4), ABP-TP-205 (2.0) (680-185778-5), ABP-TP-205 (6.0) (680-185778-6) and ABP-TP-206 (2.0) (680-185778-7) were
analyzed for fluoride in accordance with 9056. The samples were prepared on 07/13/2020 and 07/14/2020 and analyzed on 07/14/2020.
Fluoride failed the recovery criteria low for the MS of sample ABP-TP-201 (5.8)MS (680-185778-1) in batch 310-285249.
Fluoride failed the recovery criteria low for the MSD of sample ABP-TP-201 (5.8)MSD (680-185778-1) in batch 310-285249.
The presence of the '4' qualifier indicates analytes where the concentration in the unspiked sample exceeded four times the spiking
amount.
Refer to the QC report for details.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
PERCENT SOLIDS/MOISTURE
Samples ABP-TP-201 (5.8) (680-185778-1), ABP-TP-202 (5.0) (680-185778-2), ABP-TP-203 (6.0) (680-185778-3), ABP-TP-204 (4.5)
(680-185778-4), ABP-TP-205 (2.0) (680-185778-5), ABP-TP-205 (6.0) (680-185778-6), ABP-TP-206 (2.0) (680-185778-7), ABP-TP-206
(4.0) (680-185778-8), ABP-TP-207 (2.0) (680-185778-9), ABP-TP-207 (9.5) (680-185778-10), ABP-TP-208 (2.0) (680-185778-11) and
ABP-TP-208 (9.5) (680-185778-12) were analyzed for Percent Solids/Moisture in accordance with TestAmerica SOP. The samples were
analyzed on 07/09/2020.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins TestAmerica, SavannahPage 6 of 39 7/23/2020
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Client Sample Results
Job ID: 680-185778-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Lab Sample ID: 680-185778-1Client Sample ID: ABP-TP-201 (5.8)
Matrix: SolidDate Collected: 06/29/20 08:50
Date Received: 07/01/20 10:00
Method: EPA 300.0 R2.1 - Anions, Ion Chromatography - ASTM Leach
RL MDL
Fluoride 1.2 0.10 mg/L 07/17/20 15:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry - ASTM Leach
RL MDL
Cyanide, Total <10 10 ug/L 07/17/20 12:35 07/17/20 16:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185778-1Client Sample ID: ABP-TP-201 (5.8)
Matrix: SolidDate Collected: 06/29/20 08:50
Percent Solids: 84.1Date Received: 07/01/20 10:00
Method: 9056A - Anions, Ion Chromatography
RL MDL
Fluoride 490 36 mg/Kg ☼07/13/20 08:51 07/14/20 19:33 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total 0.095 0.068 mg/Kg ☼07/13/20 12:50 07/13/20 15:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185778-2Client Sample ID: ABP-TP-202 (5.0)
Matrix: SolidDate Collected: 06/29/20 09:45
Date Received: 07/01/20 10:00
Method: EPA 300.0 R2.1 - Anions, Ion Chromatography - ASTM Leach
RL MDL
Fluoride 0.66 0.10 mg/L 07/17/20 16:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry - ASTM Leach
RL MDL
Cyanide, Total <10 10 ug/L 07/17/20 12:35 07/17/20 16:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185778-2Client Sample ID: ABP-TP-202 (5.0)
Matrix: SolidDate Collected: 06/29/20 09:45
Percent Solids: 87.9Date Received: 07/01/20 10:00
Method: 9056A - Anions, Ion Chromatography
RL MDL
Fluoride 320 35 mg/Kg ☼07/13/20 12:06 07/14/20 20:20 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total 0.35 0.059 mg/Kg ☼07/13/20 12:50 07/13/20 15:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185778-3Client Sample ID: ABP-TP-203 (6.0)
Matrix: SolidDate Collected: 06/29/20 11:00
Date Received: 07/01/20 10:00
Method: EPA 300.0 R2.1 - Anions, Ion Chromatography - ASTM Leach
RL MDL
Fluoride 0.73 0.10 mg/L 07/17/20 16:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry - ASTM Leach
RL MDL
Cyanide, Total <10 10 ug/L 07/17/20 12:35 07/17/20 17:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Eurofins TestAmerica, Savannah
Page 7 of 39 7/23/2020
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Client Sample Results
Job ID: 680-185778-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Lab Sample ID: 680-185778-3Client Sample ID: ABP-TP-203 (6.0)
Matrix: SolidDate Collected: 06/29/20 11:00
Percent Solids: 87.1Date Received: 07/01/20 10:00
Method: 9056A - Anions, Ion Chromatography
RL MDL
Fluoride 280 31 mg/Kg ☼07/13/20 12:06 07/14/20 20:36 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total 0.52 0.063 mg/Kg ☼07/13/20 12:50 07/13/20 15:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185778-4Client Sample ID: ABP-TP-204 (4.5)
Matrix: SolidDate Collected: 06/29/20 11:40
Date Received: 07/01/20 10:00
Method: EPA 300.0 R2.1 - Anions, Ion Chromatography - ASTM Leach
RL MDL
Fluoride 6.2 0.50 mg/L 07/19/20 02:41 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry - ASTM Leach
RL MDL
Cyanide, Total <10 10 ug/L 07/17/20 12:35 07/17/20 17:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185778-4Client Sample ID: ABP-TP-204 (4.5)
Matrix: SolidDate Collected: 06/29/20 11:40
Percent Solids: 77.5Date Received: 07/01/20 10:00
Method: 9056A - Anions, Ion Chromatography
RL MDL
Fluoride 550 39 mg/Kg ☼07/13/20 14:12 07/14/20 20:52 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total <0.067 0.067 mg/Kg ☼07/13/20 12:50 07/13/20 15:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185778-5Client Sample ID: ABP-TP-205 (2.0)
Matrix: SolidDate Collected: 06/29/20 13:15
Date Received: 07/01/20 10:00
Method: EPA 300.0 R2.1 - Anions, Ion Chromatography - ASTM Leach
RL MDL
Fluoride 4.8 0.10 mg/L 07/17/20 17:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry - ASTM Leach
RL MDL
Cyanide, Total <10 10 ug/L 07/17/20 12:35 07/17/20 17:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185778-5Client Sample ID: ABP-TP-205 (2.0)
Matrix: SolidDate Collected: 06/29/20 13:15
Percent Solids: 77.0Date Received: 07/01/20 10:00
Method: 9056A - Anions, Ion Chromatography
RL MDL
Fluoride 190 33 mg/Kg ☼07/13/20 14:12 07/14/20 21:09 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total <0.071 0.071 mg/Kg ☼07/13/20 12:50 07/13/20 16:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Eurofins TestAmerica, Savannah
Page 8 of 39 7/23/2020
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Client Sample Results
Job ID: 680-185778-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Lab Sample ID: 680-185778-6Client Sample ID: ABP-TP-205 (6.0)
Matrix: SolidDate Collected: 06/29/20 13:50
Date Received: 07/01/20 10:00
Method: EPA 300.0 R2.1 - Anions, Ion Chromatography - ASTM Leach
RL MDL
Fluoride 2.2 0.10 mg/L 07/17/20 18:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry - ASTM Leach
RL MDL
Cyanide, Total <10 10 ug/L 07/17/20 12:35 07/17/20 17:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185778-6Client Sample ID: ABP-TP-205 (6.0)
Matrix: SolidDate Collected: 06/29/20 13:50
Percent Solids: 77.2Date Received: 07/01/20 10:00
Method: 9056A - Anions, Ion Chromatography
RL MDL
Fluoride 610 35 mg/Kg ☼07/14/20 08:17 07/14/20 21:25 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total <0.075 0.075 mg/Kg ☼07/13/20 12:50 07/13/20 16:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185778-7Client Sample ID: ABP-TP-206 (2.0)
Matrix: SolidDate Collected: 06/29/20 14:05
Date Received: 07/01/20 10:00
Method: EPA 300.0 R2.1 - Anions, Ion Chromatography - ASTM Leach
RL MDL
Fluoride 10 1.0 mg/L 07/19/20 02:56 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry - ASTM Leach
RL MDL
Cyanide, Total <10 10 ug/L 07/17/20 12:35 07/17/20 17:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185778-7Client Sample ID: ABP-TP-206 (2.0)
Matrix: SolidDate Collected: 06/29/20 14:05
Percent Solids: 92.8Date Received: 07/01/20 10:00
Method: 9056A - Anions, Ion Chromatography
RL MDL
Fluoride 690 32 mg/Kg ☼07/14/20 08:17 07/14/20 21:42 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total 0.068 0.058 mg/Kg ☼07/13/20 12:50 07/13/20 16:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185778-8Client Sample ID: ABP-TP-206 (4.0)
Matrix: SolidDate Collected: 06/29/20 14:20
Date Received: 07/01/20 10:00
Method: EPA 300.0 R2.1 - Anions, Ion Chromatography - ASTM Leach
RL MDL
Fluoride 25 1.0 mg/L 07/19/20 03:12 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry - ASTM Leach
RL MDL
Cyanide, Total <10 10 ug/L 07/17/20 12:35 07/17/20 17:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Eurofins TestAmerica, Savannah
Page 9 of 39 7/23/2020
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Client Sample Results
Job ID: 680-185778-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Lab Sample ID: 680-185778-8Client Sample ID: ABP-TP-206 (4.0)
Matrix: SolidDate Collected: 06/29/20 14:20
Percent Solids: 89.2Date Received: 07/01/20 10:00
General Chemistry
RL MDL
Cyanide, Total 0.13 0.059 mg/Kg ☼07/13/20 12:50 07/13/20 16:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185778-9Client Sample ID: ABP-TP-207 (2.0)
Matrix: SolidDate Collected: 06/29/20 15:00
Date Received: 07/01/20 10:00
Method: EPA 300.0 R2.1 - Anions, Ion Chromatography - ASTM Leach
RL MDL
Fluoride 1.1 0.10 mg/L 07/17/20 18:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry - ASTM Leach
RL MDL
Cyanide, Total <10 10 ug/L 07/17/20 12:35 07/17/20 17:11 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185778-9Client Sample ID: ABP-TP-207 (2.0)
Matrix: SolidDate Collected: 06/29/20 15:00
Percent Solids: 80.5Date Received: 07/01/20 10:00
General Chemistry
RL MDL
Cyanide, Total <0.064 0.064 mg/Kg ☼07/13/20 12:50 07/13/20 16:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185778-10Client Sample ID: ABP-TP-207 (9.5)
Matrix: SolidDate Collected: 06/29/20 15:10
Date Received: 07/01/20 10:00
Method: EPA 300.0 R2.1 - Anions, Ion Chromatography - ASTM Leach
RL MDL
Fluoride 3.2 0.10 mg/L 07/17/20 18:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry - ASTM Leach
RL MDL
Cyanide, Total <10 10 ug/L 07/17/20 12:35 07/17/20 17:16 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185778-10Client Sample ID: ABP-TP-207 (9.5)
Matrix: SolidDate Collected: 06/29/20 15:10
Percent Solids: 79.3Date Received: 07/01/20 10:00
General Chemistry
RL MDL
Cyanide, Total 0.074 0.074 mg/Kg ☼07/13/20 12:50 07/13/20 16:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185778-11Client Sample ID: ABP-TP-208 (2.0)
Matrix: SolidDate Collected: 06/29/20 15:30
Date Received: 07/01/20 10:00
Method: EPA 300.0 R2.1 - Anions, Ion Chromatography - ASTM Leach
RL MDL
Fluoride 1.7 0.10 mg/L 07/17/20 19:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry - ASTM Leach
RL MDL
Cyanide, Total <10 10 ug/L 07/17/20 12:35 07/17/20 17:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Eurofins TestAmerica, Savannah
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Client Sample Results
Job ID: 680-185778-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Lab Sample ID: 680-185778-11Client Sample ID: ABP-TP-208 (2.0)
Matrix: SolidDate Collected: 06/29/20 15:30
Percent Solids: 76.9Date Received: 07/01/20 10:00
General Chemistry
RL MDL
Cyanide, Total <0.068 0.068 mg/Kg ☼07/13/20 12:50 07/13/20 16:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185778-12Client Sample ID: ABP-TP-208 (9.5)
Matrix: SolidDate Collected: 06/29/20 15:40
Date Received: 07/01/20 10:00
Method: EPA 300.0 R2.1 - Anions, Ion Chromatography - ASTM Leach
RL MDL
Fluoride 0.17 0.10 mg/L 07/17/20 19:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry - ASTM Leach
RL MDL
Cyanide, Total <10 10 ug/L 07/17/20 12:35 07/17/20 17:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185778-12Client Sample ID: ABP-TP-208 (9.5)
Matrix: SolidDate Collected: 06/29/20 15:40
Percent Solids: 74.6Date Received: 07/01/20 10:00
General Chemistry
RL MDL
Cyanide, Total <0.076 0.076 mg/Kg ☼07/13/20 12:50 07/13/20 16:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Eurofins TestAmerica, Savannah
Page 11 of 39 7/23/2020
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QC Sample Results
Job ID: 680-185778-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Method: 9056A - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 310-284770/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 285249 Prep Batch: 284770
RL MDL
Fluoride <28 28 mg/Kg 07/10/20 09:00 07/14/20 18:31 10
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 310-284770/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 285249 Prep Batch: 284770
Fluoride 450 413 mg/Kg 92 90 -110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: ABP-TP-201 (5.8)Lab Sample ID: 680-185778-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 285249 Prep Batch: 284770
Fluoride 490 58.6 402 4 mg/Kg -151 80 -120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: ABP-TP-201 (5.8)Lab Sample ID: 680-185778-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 285249 Prep Batch: 284770
Fluoride 490 57.0 461 4 mg/Kg -51 80 -120 14 15☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: EPA 300.0 R2.1 - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 180-322104/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 322104
RL MDL
Fluoride <0.10 0.10 mg/L 07/17/20 15:06 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-322104/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 322104
Fluoride 2.50 2.47 mg/L 99 90 -110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method BlankLab Sample ID: MB 180-322142/42
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 322142
RL MDL
Fluoride <0.10 0.10 mg/L 07/18/20 22:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Eurofins TestAmerica, Savannah
Page 12 of 39 7/23/2020
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QC Sample Results
Job ID: 680-185778-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Method: EPA 300.0 R2.1 - Anions, Ion Chromatography (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-322142/41
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 322142
Fluoride 2.50 2.61 mg/L 105 90 -110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method BlankLab Sample ID: LB 180-320750/1-A
Matrix: Solid Prep Type: ASTM Leach
Analysis Batch: 322104
RL MDL
Fluoride <0.10 0.10 mg/L 07/17/20 15:36 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: ABP-TP-201 (5.8)Lab Sample ID: 680-185778-1 MS
Matrix: Solid Prep Type: ASTM Leach
Analysis Batch: 322104
Fluoride 1.2 2.50 3.55 mg/L 95 90 -110
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: ABP-TP-201 (5.8)Lab Sample ID: 680-185778-1 MSD
Matrix: Solid Prep Type: ASTM Leach
Analysis Batch: 322104
Fluoride 1.2 2.50 3.59 mg/L 97 90 -110 1 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: 9012A - Cyanide, Total and/or Amenable
Client Sample ID: Method BlankLab Sample ID: MB 680-626052/12-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 626168 Prep Batch: 626052
RL MDL
Cyanide, Total <0.010 0.010 mg/Kg 07/13/20 12:50 07/13/20 15:45 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-626052/13-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 626168 Prep Batch: 626052
Cyanide, Total 0.0500 0.0512 mg/Kg 102 75 -125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: ABP-TP-204 (4.5)Lab Sample ID: 680-185778-4 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 626168 Prep Batch: 626052
Cyanide, Total <0.067 0.377 0.362 mg/Kg 83 75 -125☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Eurofins TestAmerica, Savannah
Page 13 of 39 7/23/2020
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QC Sample Results
Job ID: 680-185778-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Method: 9012A - Cyanide, Total and/or Amenable (Continued)
Client Sample ID: ABP-TP-204 (4.5)Lab Sample ID: 680-185778-4 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 626168 Prep Batch: 626052
Cyanide, Total <0.067 0.340 0.343 mg/Kg 87 75 -125 5 30☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: EPA 9012B - Cyanide, Total andor Amenable
Client Sample ID: Method BlankLab Sample ID: MB 180-322056/4-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 322148 Prep Batch: 322056
RL MDL
Cyanide, Total <10 10 ug/L 07/17/20 12:35 07/17/20 16:46 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: HLCS 180-322056/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 322148 Prep Batch: 322056
Cyanide, Total 250 272 ug/L 109 90 -110
Analyte
HLCS HLCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-322056/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 322148 Prep Batch: 322056
Cyanide, Total 200 219 ug/L 109 85 -115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LLCS 180-322056/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 322148 Prep Batch: 322056
Cyanide, Total 50.0 49.9 ug/L 100 90 -110
Analyte
LLCS LLCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method BlankLab Sample ID: LB 180-320750/1-C
Matrix: Solid Prep Type: ASTM Leach
Analysis Batch: 322148 Prep Batch: 322056
RL MDL
Cyanide, Total <10 10 ug/L 07/17/20 12:35 07/17/20 16:48 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: ABP-TP-201 (5.8)Lab Sample ID: 680-185778-1 MS
Matrix: Solid Prep Type: ASTM Leach
Analysis Batch: 322148 Prep Batch: 322056
Cyanide, Total <10 200 213 ug/L 106 75 -125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Eurofins TestAmerica, Savannah
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QC Sample Results
Job ID: 680-185778-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Method: EPA 9012B - Cyanide, Total andor Amenable (Continued)
Client Sample ID: ABP-TP-201 (5.8)Lab Sample ID: 680-185778-1 MSD
Matrix: Solid Prep Type: ASTM Leach
Analysis Batch: 322148 Prep Batch: 322056
Cyanide, Total <10 200 210 ug/L 105 75 -125 1 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Eurofins TestAmerica, Savannah
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QC Association Summary
Job ID: 680-185778-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
HPLC/IC
Prep Batch: 284770
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 4500 F-B680-185778-1 ABP-TP-201 (5.8)Total/NA
Solid 4500 F-B680-185778-2 ABP-TP-202 (5.0)Total/NA
Solid 4500 F-B680-185778-3 ABP-TP-203 (6.0)Total/NA
Solid 4500 F-B680-185778-4 ABP-TP-204 (4.5)Total/NA
Solid 4500 F-B680-185778-5 ABP-TP-205 (2.0)Total/NA
Solid 4500 F-B680-185778-6 ABP-TP-205 (6.0)Total/NA
Solid 4500 F-B680-185778-7 ABP-TP-206 (2.0)Total/NA
Solid 4500 F-BMB 310-284770/1-A Method Blank Total/NA
Solid 4500 F-BLCS 310-284770/2-A Lab Control Sample Total/NA
Solid 4500 F-B680-185778-1 MS ABP-TP-201 (5.8)Total/NA
Solid 4500 F-B680-185778-1 MSD ABP-TP-201 (5.8)Total/NA
Analysis Batch: 285249
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9056A 284770680-185778-1 ABP-TP-201 (5.8)Total/NA
Solid 9056A 284770680-185778-2 ABP-TP-202 (5.0)Total/NA
Solid 9056A 284770680-185778-3 ABP-TP-203 (6.0)Total/NA
Solid 9056A 284770680-185778-4 ABP-TP-204 (4.5)Total/NA
Solid 9056A 284770680-185778-5 ABP-TP-205 (2.0)Total/NA
Solid 9056A 284770680-185778-6 ABP-TP-205 (6.0)Total/NA
Solid 9056A 284770680-185778-7 ABP-TP-206 (2.0)Total/NA
Solid 9056A 284770MB 310-284770/1-A Method Blank Total/NA
Solid 9056A 284770LCS 310-284770/2-A Lab Control Sample Total/NA
Solid 9056A 284770680-185778-1 MS ABP-TP-201 (5.8)Total/NA
Solid 9056A 284770680-185778-1 MSD ABP-TP-201 (5.8)Total/NA
Leach Batch: 320750
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid D3987-85680-185778-1 ABP-TP-201 (5.8)ASTM Leach
Solid D3987-85680-185778-2 ABP-TP-202 (5.0)ASTM Leach
Solid D3987-85680-185778-3 ABP-TP-203 (6.0)ASTM Leach
Solid D3987-85680-185778-4 ABP-TP-204 (4.5)ASTM Leach
Solid D3987-85680-185778-5 ABP-TP-205 (2.0)ASTM Leach
Solid D3987-85680-185778-6 ABP-TP-205 (6.0)ASTM Leach
Solid D3987-85680-185778-7 ABP-TP-206 (2.0)ASTM Leach
Solid D3987-85680-185778-8 ABP-TP-206 (4.0)ASTM Leach
Solid D3987-85680-185778-9 ABP-TP-207 (2.0)ASTM Leach
Solid D3987-85680-185778-10 ABP-TP-207 (9.5)ASTM Leach
Solid D3987-85680-185778-11 ABP-TP-208 (2.0)ASTM Leach
Solid D3987-85680-185778-12 ABP-TP-208 (9.5)ASTM Leach
Solid D3987-85LB 180-320750/1-A Method Blank ASTM Leach
Solid D3987-85680-185778-1 MS ABP-TP-201 (5.8)ASTM Leach
Solid D3987-85680-185778-1 MSD ABP-TP-201 (5.8)ASTM Leach
Analysis Batch: 322104
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid EPA 300.0 R2.1 320750680-185778-1 ABP-TP-201 (5.8)ASTM Leach
Solid EPA 300.0 R2.1 320750680-185778-2 ABP-TP-202 (5.0)ASTM Leach
Solid EPA 300.0 R2.1 320750680-185778-3 ABP-TP-203 (6.0)ASTM Leach
Solid EPA 300.0 R2.1 320750680-185778-5 ABP-TP-205 (2.0)ASTM Leach
Solid EPA 300.0 R2.1 320750680-185778-6 ABP-TP-205 (6.0)ASTM Leach
Eurofins TestAmerica, Savannah
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QC Association Summary
Job ID: 680-185778-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
HPLC/IC (Continued)
Analysis Batch: 322104 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid EPA 300.0 R2.1 320750680-185778-9 ABP-TP-207 (2.0)ASTM Leach
Solid EPA 300.0 R2.1 320750680-185778-10 ABP-TP-207 (9.5)ASTM Leach
Solid EPA 300.0 R2.1 320750680-185778-11 ABP-TP-208 (2.0)ASTM Leach
Solid EPA 300.0 R2.1 320750680-185778-12 ABP-TP-208 (9.5)ASTM Leach
Solid EPA 300.0 R2.1 320750LB 180-320750/1-A Method Blank ASTM Leach
Solid EPA 300.0 R2.1MB 180-322104/6 Method Blank Total/NA
Solid EPA 300.0 R2.1LCS 180-322104/5 Lab Control Sample Total/NA
Solid EPA 300.0 R2.1 320750680-185778-1 MS ABP-TP-201 (5.8)ASTM Leach
Solid EPA 300.0 R2.1 320750680-185778-1 MSD ABP-TP-201 (5.8)ASTM Leach
Analysis Batch: 322142
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid EPA 300.0 R2.1 320750680-185778-4 ABP-TP-204 (4.5)ASTM Leach
Solid EPA 300.0 R2.1 320750680-185778-7 ABP-TP-206 (2.0)ASTM Leach
Solid EPA 300.0 R2.1 320750680-185778-8 ABP-TP-206 (4.0)ASTM Leach
Solid EPA 300.0 R2.1MB 180-322142/42 Method Blank Total/NA
Solid EPA 300.0 R2.1LCS 180-322142/41 Lab Control Sample Total/NA
General Chemistry
Leach Batch: 320750
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid D3987-85680-185778-1 ABP-TP-201 (5.8)ASTM Leach
Solid D3987-85680-185778-2 ABP-TP-202 (5.0)ASTM Leach
Solid D3987-85680-185778-3 ABP-TP-203 (6.0)ASTM Leach
Solid D3987-85680-185778-4 ABP-TP-204 (4.5)ASTM Leach
Solid D3987-85680-185778-5 ABP-TP-205 (2.0)ASTM Leach
Solid D3987-85680-185778-6 ABP-TP-205 (6.0)ASTM Leach
Solid D3987-85680-185778-7 ABP-TP-206 (2.0)ASTM Leach
Solid D3987-85680-185778-8 ABP-TP-206 (4.0)ASTM Leach
Solid D3987-85680-185778-9 ABP-TP-207 (2.0)ASTM Leach
Solid D3987-85680-185778-10 ABP-TP-207 (9.5)ASTM Leach
Solid D3987-85680-185778-11 ABP-TP-208 (2.0)ASTM Leach
Solid D3987-85680-185778-12 ABP-TP-208 (9.5)ASTM Leach
Solid D3987-85LB 180-320750/1-C Method Blank ASTM Leach
Solid D3987-85680-185778-1 MS ABP-TP-201 (5.8)ASTM Leach
Solid D3987-85680-185778-1 MSD ABP-TP-201 (5.8)ASTM Leach
Prep Batch: 322056
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9012B 320750680-185778-1 ABP-TP-201 (5.8)ASTM Leach
Solid 9012B 320750680-185778-2 ABP-TP-202 (5.0)ASTM Leach
Solid 9012B 320750680-185778-3 ABP-TP-203 (6.0)ASTM Leach
Solid 9012B 320750680-185778-4 ABP-TP-204 (4.5)ASTM Leach
Solid 9012B 320750680-185778-5 ABP-TP-205 (2.0)ASTM Leach
Solid 9012B 320750680-185778-6 ABP-TP-205 (6.0)ASTM Leach
Solid 9012B 320750680-185778-7 ABP-TP-206 (2.0)ASTM Leach
Solid 9012B 320750680-185778-8 ABP-TP-206 (4.0)ASTM Leach
Solid 9012B 320750680-185778-9 ABP-TP-207 (2.0)ASTM Leach
Solid 9012B 320750680-185778-10 ABP-TP-207 (9.5)ASTM Leach
Solid 9012B 320750680-185778-11 ABP-TP-208 (2.0)ASTM Leach
Eurofins TestAmerica, Savannah
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QC Association Summary
Job ID: 680-185778-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
General Chemistry (Continued)
Prep Batch: 322056 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9012B 320750680-185778-12 ABP-TP-208 (9.5)ASTM Leach
Solid 9012B 320750LB 180-320750/1-C Method Blank ASTM Leach
Solid 9012BMB 180-322056/4-A Method Blank Total/NA
Solid 9012BHLCS 180-322056/2-A Lab Control Sample Total/NA
Solid 9012BLCS 180-322056/3-A Lab Control Sample Total/NA
Solid 9012BLLCS 180-322056/1-A Lab Control Sample Total/NA
Solid 9012B 320750680-185778-1 MS ABP-TP-201 (5.8)ASTM Leach
Solid 9012B 320750680-185778-1 MSD ABP-TP-201 (5.8)ASTM Leach
Analysis Batch: 322148
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid EPA 9012B 322056680-185778-1 ABP-TP-201 (5.8)ASTM Leach
Solid EPA 9012B 322056680-185778-2 ABP-TP-202 (5.0)ASTM Leach
Solid EPA 9012B 322056680-185778-3 ABP-TP-203 (6.0)ASTM Leach
Solid EPA 9012B 322056680-185778-4 ABP-TP-204 (4.5)ASTM Leach
Solid EPA 9012B 322056680-185778-5 ABP-TP-205 (2.0)ASTM Leach
Solid EPA 9012B 322056680-185778-6 ABP-TP-205 (6.0)ASTM Leach
Solid EPA 9012B 322056680-185778-7 ABP-TP-206 (2.0)ASTM Leach
Solid EPA 9012B 322056680-185778-8 ABP-TP-206 (4.0)ASTM Leach
Solid EPA 9012B 322056680-185778-9 ABP-TP-207 (2.0)ASTM Leach
Solid EPA 9012B 322056680-185778-10 ABP-TP-207 (9.5)ASTM Leach
Solid EPA 9012B 322056680-185778-11 ABP-TP-208 (2.0)ASTM Leach
Solid EPA 9012B 322056680-185778-12 ABP-TP-208 (9.5)ASTM Leach
Solid EPA 9012B 322056LB 180-320750/1-C Method Blank ASTM Leach
Solid EPA 9012B 322056MB 180-322056/4-A Method Blank Total/NA
Solid EPA 9012B 322056HLCS 180-322056/2-A Lab Control Sample Total/NA
Solid EPA 9012B 322056LCS 180-322056/3-A Lab Control Sample Total/NA
Solid EPA 9012B 322056LLCS 180-322056/1-A Lab Control Sample Total/NA
Solid EPA 9012B 322056680-185778-1 MS ABP-TP-201 (5.8)ASTM Leach
Solid EPA 9012B 322056680-185778-1 MSD ABP-TP-201 (5.8)ASTM Leach
Analysis Batch: 625595
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture680-185778-1 ABP-TP-201 (5.8)Total/NA
Solid Moisture680-185778-2 ABP-TP-202 (5.0)Total/NA
Solid Moisture680-185778-3 ABP-TP-203 (6.0)Total/NA
Solid Moisture680-185778-4 ABP-TP-204 (4.5)Total/NA
Solid Moisture680-185778-5 ABP-TP-205 (2.0)Total/NA
Solid Moisture680-185778-6 ABP-TP-205 (6.0)Total/NA
Solid Moisture680-185778-7 ABP-TP-206 (2.0)Total/NA
Solid Moisture680-185778-8 ABP-TP-206 (4.0)Total/NA
Solid Moisture680-185778-9 ABP-TP-207 (2.0)Total/NA
Solid Moisture680-185778-10 ABP-TP-207 (9.5)Total/NA
Solid Moisture680-185778-11 ABP-TP-208 (2.0)Total/NA
Solid Moisture680-185778-12 ABP-TP-208 (9.5)Total/NA
Prep Batch: 626052
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9012A680-185778-1 ABP-TP-201 (5.8)Total/NA
Solid 9012A680-185778-2 ABP-TP-202 (5.0)Total/NA
Solid 9012A680-185778-3 ABP-TP-203 (6.0)Total/NA
Eurofins TestAmerica, Savannah
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QC Association Summary
Job ID: 680-185778-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
General Chemistry (Continued)
Prep Batch: 626052 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9012A680-185778-4 ABP-TP-204 (4.5)Total/NA
Solid 9012A680-185778-5 ABP-TP-205 (2.0)Total/NA
Solid 9012A680-185778-6 ABP-TP-205 (6.0)Total/NA
Solid 9012A680-185778-7 ABP-TP-206 (2.0)Total/NA
Solid 9012A680-185778-8 ABP-TP-206 (4.0)Total/NA
Solid 9012A680-185778-9 ABP-TP-207 (2.0)Total/NA
Solid 9012A680-185778-10 ABP-TP-207 (9.5)Total/NA
Solid 9012A680-185778-11 ABP-TP-208 (2.0)Total/NA
Solid 9012A680-185778-12 ABP-TP-208 (9.5)Total/NA
Solid 9012AMB 680-626052/12-A Method Blank Total/NA
Solid 9012ALCS 680-626052/13-A Lab Control Sample Total/NA
Solid 9012A680-185778-4 MS ABP-TP-204 (4.5)Total/NA
Solid 9012A680-185778-4 MSD ABP-TP-204 (4.5)Total/NA
Analysis Batch: 626168
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9012A 626052680-185778-1 ABP-TP-201 (5.8)Total/NA
Solid 9012A 626052680-185778-2 ABP-TP-202 (5.0)Total/NA
Solid 9012A 626052680-185778-3 ABP-TP-203 (6.0)Total/NA
Solid 9012A 626052680-185778-4 ABP-TP-204 (4.5)Total/NA
Solid 9012A 626052680-185778-5 ABP-TP-205 (2.0)Total/NA
Solid 9012A 626052680-185778-6 ABP-TP-205 (6.0)Total/NA
Solid 9012A 626052680-185778-7 ABP-TP-206 (2.0)Total/NA
Solid 9012A 626052680-185778-8 ABP-TP-206 (4.0)Total/NA
Solid 9012A 626052680-185778-9 ABP-TP-207 (2.0)Total/NA
Solid 9012A 626052680-185778-10 ABP-TP-207 (9.5)Total/NA
Solid 9012A 626052680-185778-11 ABP-TP-208 (2.0)Total/NA
Solid 9012A 626052680-185778-12 ABP-TP-208 (9.5)Total/NA
Solid 9012A 626052MB 680-626052/12-A Method Blank Total/NA
Solid 9012A 626052LCS 680-626052/13-A Lab Control Sample Total/NA
Solid 9012A 626052680-185778-4 MS ABP-TP-204 (4.5)Total/NA
Solid 9012A 626052680-185778-4 MSD ABP-TP-204 (4.5)Total/NA
Eurofins TestAmerica, Savannah
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Lab Chronicle
Client: Civil & Environmental Consultants Inc Job ID: 680-185778-1
Project/Site: Badin Business Park
Client Sample ID: ABP-TP-201 (5.8)Lab Sample ID: 680-185778-1
Matrix: SolidDate Collected: 06/29/20 08:50
Date Received: 07/01/20 10:00
Leach D3987-85 GRN07/08/20 16:30 TAL PIT320750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
ASTM Leach 100.35 g 2000 mL
Analysis EPA 300.0 R2.1 1 322104 07/17/20 15:51 EPS TAL PITASTM Leach
CHICS2000Instrument ID:
Leach D3987-85 320750 07/08/20 16:30 GRN TAL PITASTM Leach 100.35 g 2000 mL
Prep 9012B 322056 07/17/20 12:35 CMR TAL PITASTM Leach 6 mL 6 mL
Analysis EPA 9012B 1 322148 07/17/20 16:50 CMR TAL PITASTM Leach
SEAL2Instrument ID:
Analysis Moisture 1 625595 07/09/20 07:15 JEB TAL SAVTotal/NA
NOEQUIPInstrument ID:
Client Sample ID: ABP-TP-201 (5.8)Lab Sample ID: 680-185778-1
Matrix: SolidDate Collected: 06/29/20 08:50
Percent Solids: 84.1Date Received: 07/01/20 10:00
Prep 4500 F-B LBB07/13/20 08:51 TAL CF284770
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10.192 mL 310 mL
Analysis 9056A 10 285249 07/14/20 19:33 ACJ TAL CFTotal/NA 10 mL 10 mL
OpheliaInstrument ID:
Prep 9012A 626052 07/13/20 12:50 JER TAL SAVTotal/NA 1.0509 g 6 mL
Analysis 9012A 1 626168 07/13/20 15:53 JER TAL SAVTotal/NA
KONELAB4Instrument ID:
Client Sample ID: ABP-TP-202 (5.0)Lab Sample ID: 680-185778-2
Matrix: SolidDate Collected: 06/29/20 09:45
Date Received: 07/01/20 10:00
Leach D3987-85 GRN07/08/20 16:30 TAL PIT320750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
ASTM Leach 100.35 g 2000 mL
Analysis EPA 300.0 R2.1 1 322104 07/17/20 16:34 EPS TAL PITASTM Leach
CHICS2000Instrument ID:
Leach D3987-85 320750 07/08/20 16:30 GRN TAL PITASTM Leach 100.35 g 2000 mL
Prep 9012B 322056 07/17/20 12:35 CMR TAL PITASTM Leach 6 mL 6 mL
Analysis EPA 9012B 1 322148 07/17/20 16:59 CMR TAL PITASTM Leach
SEAL2Instrument ID:
Analysis Moisture 1 625595 07/09/20 07:15 JEB TAL SAVTotal/NA
NOEQUIPInstrument ID:
Client Sample ID: ABP-TP-202 (5.0)Lab Sample ID: 680-185778-2
Matrix: SolidDate Collected: 06/29/20 09:45
Percent Solids: 87.9Date Received: 07/01/20 10:00
Prep 4500 F-B LBB07/13/20 12:06 TAL CF284770
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10.028 mL 310 mL
Analysis 9056A 10 285249 07/14/20 20:20 ACJ TAL CFTotal/NA 10 mL 10 mL
OpheliaInstrument ID:
Eurofins TestAmerica, Savannah
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Lab Chronicle
Client: Civil & Environmental Consultants Inc Job ID: 680-185778-1
Project/Site: Badin Business Park
Client Sample ID: ABP-TP-202 (5.0)Lab Sample ID: 680-185778-2
Matrix: SolidDate Collected: 06/29/20 09:45
Percent Solids: 87.9Date Received: 07/01/20 10:00
Prep 9012A JER07/13/20 12:50 TAL SAV626052
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1.1501 g 6 mL
Analysis 9012A 1 626168 07/13/20 15:53 JER TAL SAVTotal/NA
KONELAB4Instrument ID:
Client Sample ID: ABP-TP-203 (6.0)Lab Sample ID: 680-185778-3
Matrix: SolidDate Collected: 06/29/20 11:00
Date Received: 07/01/20 10:00
Leach D3987-85 GRN07/08/20 16:30 TAL PIT320750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
ASTM Leach 100.58 g 2000 mL
Analysis EPA 300.0 R2.1 1 322104 07/17/20 16:48 EPS TAL PITASTM Leach
CHICS2000Instrument ID:
Leach D3987-85 320750 07/08/20 16:30 GRN TAL PITASTM Leach 100.58 g 2000 mL
Prep 9012B 322056 07/17/20 12:35 CMR TAL PITASTM Leach 6 mL 6 mL
Analysis EPA 9012B 1 322148 07/17/20 17:00 CMR TAL PITASTM Leach
SEAL2Instrument ID:
Analysis Moisture 1 625595 07/09/20 07:15 JEB TAL SAVTotal/NA
NOEQUIPInstrument ID:
Client Sample ID: ABP-TP-203 (6.0)Lab Sample ID: 680-185778-3
Matrix: SolidDate Collected: 06/29/20 11:00
Percent Solids: 87.1Date Received: 07/01/20 10:00
Prep 4500 F-B LBB07/13/20 12:06 TAL CF284770
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10.671 mL 290 mL
Analysis 9056A 10 285249 07/14/20 20:36 ACJ TAL CFTotal/NA 10 mL 10 mL
OpheliaInstrument ID:
Prep 9012A 626052 07/13/20 12:50 JER TAL SAVTotal/NA 1.0857 g 6 mL
Analysis 9012A 1 626168 07/13/20 15:53 JER TAL SAVTotal/NA
KONELAB4Instrument ID:
Client Sample ID: ABP-TP-204 (4.5)Lab Sample ID: 680-185778-4
Matrix: SolidDate Collected: 06/29/20 11:40
Date Received: 07/01/20 10:00
Leach D3987-85 GRN07/08/20 16:30 TAL PIT320750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
ASTM Leach 100.52 g 2000 mL
Analysis EPA 300.0 R2.1 5 322142 07/19/20 02:41 EPS TAL PITASTM Leach
CHIC2100AInstrument ID:
Leach D3987-85 320750 07/08/20 16:30 GRN TAL PITASTM Leach 100.52 g 2000 mL
Prep 9012B 322056 07/17/20 12:35 CMR TAL PITASTM Leach 6 mL 6 mL
Analysis EPA 9012B 1 322148 07/17/20 17:02 CMR TAL PITASTM Leach
SEAL2Instrument ID:
Analysis Moisture 1 625595 07/09/20 07:15 JEB TAL SAVTotal/NA
NOEQUIPInstrument ID:
Eurofins TestAmerica, Savannah
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Lab Chronicle
Client: Civil & Environmental Consultants Inc Job ID: 680-185778-1
Project/Site: Badin Business Park
Client Sample ID: ABP-TP-204 (4.5)Lab Sample ID: 680-185778-4
Matrix: SolidDate Collected: 06/29/20 11:40
Percent Solids: 77.5Date Received: 07/01/20 10:00
Prep 4500 F-B LBB07/13/20 14:12 TAL CF284770
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10.000 mL 305 mL
Analysis 9056A 10 285249 07/14/20 20:52 ACJ TAL CFTotal/NA 10 mL 10 mL
OpheliaInstrument ID:
Prep 9012A 626052 07/13/20 12:50 JER TAL SAVTotal/NA 1.1631 g 6 mL
Analysis 9012A 1 626168 07/13/20 15:53 JER TAL SAVTotal/NA
KONELAB4Instrument ID:
Client Sample ID: ABP-TP-205 (2.0)Lab Sample ID: 680-185778-5
Matrix: SolidDate Collected: 06/29/20 13:15
Date Received: 07/01/20 10:00
Leach D3987-85 GRN07/08/20 16:30 TAL PIT320750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
ASTM Leach 100.14 g 2000 mL
Analysis EPA 300.0 R2.1 1 322104 07/17/20 17:17 EPS TAL PITASTM Leach
CHICS2000Instrument ID:
Leach D3987-85 320750 07/08/20 16:30 GRN TAL PITASTM Leach 100.14 g 2000 mL
Prep 9012B 322056 07/17/20 12:35 CMR TAL PITASTM Leach 6 mL 6 mL
Analysis EPA 9012B 1 322148 07/17/20 17:04 CMR TAL PITASTM Leach
SEAL2Instrument ID:
Analysis Moisture 1 625595 07/09/20 07:15 JEB TAL SAVTotal/NA
NOEQUIPInstrument ID:
Client Sample ID: ABP-TP-205 (2.0)Lab Sample ID: 680-185778-5
Matrix: SolidDate Collected: 06/29/20 13:15
Percent Solids: 77.0Date Received: 07/01/20 10:00
Prep 4500 F-B LBB07/13/20 14:12 TAL CF284770
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10.682 mL 275 mL
Analysis 9056A 10 285249 07/14/20 21:09 ACJ TAL CFTotal/NA 10 mL 10 mL
OpheliaInstrument ID:
Prep 9012A 626052 07/13/20 12:50 JER TAL SAVTotal/NA 1.1028 g 6 mL
Analysis 9012A 1 626168 07/13/20 16:00 JER TAL SAVTotal/NA
KONELAB4Instrument ID:
Client Sample ID: ABP-TP-205 (6.0)Lab Sample ID: 680-185778-6
Matrix: SolidDate Collected: 06/29/20 13:50
Date Received: 07/01/20 10:00
Leach D3987-85 GRN07/08/20 16:30 TAL PIT320750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
ASTM Leach 100.08 g 2000 mL
Analysis EPA 300.0 R2.1 1 322104 07/17/20 18:00 EPS TAL PITASTM Leach
CHICS2000Instrument ID:
Leach D3987-85 320750 07/08/20 16:30 GRN TAL PITASTM Leach 100.08 g 2000 mL
Prep 9012B 322056 07/17/20 12:35 CMR TAL PITASTM Leach 6 mL 6 mL
Analysis EPA 9012B 1 322148 07/17/20 17:05 CMR TAL PITASTM Leach
SEAL2Instrument ID:
Eurofins TestAmerica, Savannah
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Lab Chronicle
Client: Civil & Environmental Consultants Inc Job ID: 680-185778-1
Project/Site: Badin Business Park
Client Sample ID: ABP-TP-205 (6.0)Lab Sample ID: 680-185778-6
Matrix: SolidDate Collected: 06/29/20 13:50
Date Received: 07/01/20 10:00
Analysis Moisture JEB07/09/20 07:151 TAL SAV625595
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: ABP-TP-205 (6.0)Lab Sample ID: 680-185778-6
Matrix: SolidDate Collected: 06/29/20 13:50
Percent Solids: 77.2Date Received: 07/01/20 10:00
Prep 4500 F-B LBB07/14/20 08:17 TAL CF284770
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10.773 mL 295 mL
Analysis 9056A 10 285249 07/14/20 21:25 ACJ TAL CFTotal/NA 10 mL 10 mL
OpheliaInstrument ID:
Prep 9012A 626052 07/13/20 12:50 JER TAL SAVTotal/NA 1.0325 g 6 mL
Analysis 9012A 1 626168 07/13/20 16:00 JER TAL SAVTotal/NA
KONELAB4Instrument ID:
Client Sample ID: ABP-TP-206 (2.0)Lab Sample ID: 680-185778-7
Matrix: SolidDate Collected: 06/29/20 14:05
Date Received: 07/01/20 10:00
Leach D3987-85 GRN07/08/20 16:30 TAL PIT320750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
ASTM Leach 100.27 g 2000 mL
Analysis EPA 300.0 R2.1 10 322142 07/19/20 02:56 EPS TAL PITASTM Leach
CHIC2100AInstrument ID:
Leach D3987-85 320750 07/08/20 16:30 GRN TAL PITASTM Leach 100.27 g 2000 mL
Prep 9012B 322056 07/17/20 12:35 CMR TAL PITASTM Leach 6 mL 6 mL
Analysis EPA 9012B 1 322148 07/17/20 17:07 CMR TAL PITASTM Leach
SEAL2Instrument ID:
Analysis Moisture 1 625595 07/09/20 07:15 JEB TAL SAVTotal/NA
NOEQUIPInstrument ID:
Client Sample ID: ABP-TP-206 (2.0)Lab Sample ID: 680-185778-7
Matrix: SolidDate Collected: 06/29/20 14:05
Percent Solids: 92.8Date Received: 07/01/20 10:00
Prep 4500 F-B LBB07/14/20 08:17 TAL CF284770
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 10.091 mL 300 mL
Analysis 9056A 10 285249 07/14/20 21:42 ACJ TAL CFTotal/NA 10 mL 10 mL
OpheliaInstrument ID:
Prep 9012A 626052 07/13/20 12:50 JER TAL SAVTotal/NA 1.1134 g 6 mL
Analysis 9012A 1 626168 07/13/20 16:00 JER TAL SAVTotal/NA
KONELAB4Instrument ID:
Eurofins TestAmerica, Savannah
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Lab Chronicle
Client: Civil & Environmental Consultants Inc Job ID: 680-185778-1
Project/Site: Badin Business Park
Client Sample ID: ABP-TP-206 (4.0)Lab Sample ID: 680-185778-8
Matrix: SolidDate Collected: 06/29/20 14:20
Date Received: 07/01/20 10:00
Leach D3987-85 GRN07/08/20 16:30 TAL PIT320750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
ASTM Leach 100.05 g 2000 mL
Analysis EPA 300.0 R2.1 10 322142 07/19/20 03:12 EPS TAL PITASTM Leach
CHIC2100AInstrument ID:
Leach D3987-85 320750 07/08/20 16:30 GRN TAL PITASTM Leach 100.05 g 2000 mL
Prep 9012B 322056 07/17/20 12:35 CMR TAL PITASTM Leach 6 mL 6 mL
Analysis EPA 9012B 1 322148 07/17/20 17:09 CMR TAL PITASTM Leach
SEAL2Instrument ID:
Analysis Moisture 1 625595 07/09/20 07:15 JEB TAL SAVTotal/NA
NOEQUIPInstrument ID:
Client Sample ID: ABP-TP-206 (4.0)Lab Sample ID: 680-185778-8
Matrix: SolidDate Collected: 06/29/20 14:20
Percent Solids: 89.2Date Received: 07/01/20 10:00
Prep 9012A JER07/13/20 12:50 TAL SAV626052
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1.1388 g 6 mL
Analysis 9012A 1 626168 07/13/20 16:00 JER TAL SAVTotal/NA
KONELAB4Instrument ID:
Client Sample ID: ABP-TP-207 (2.0)Lab Sample ID: 680-185778-9
Matrix: SolidDate Collected: 06/29/20 15:00
Date Received: 07/01/20 10:00
Leach D3987-85 GRN07/08/20 16:30 TAL PIT320750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
ASTM Leach 100.08 g 2000 mL
Analysis EPA 300.0 R2.1 1 322104 07/17/20 18:44 EPS TAL PITASTM Leach
CHICS2000Instrument ID:
Leach D3987-85 320750 07/08/20 16:30 GRN TAL PITASTM Leach 100.08 g 2000 mL
Prep 9012B 322056 07/17/20 12:35 CMR TAL PITASTM Leach 6 mL 6 mL
Analysis EPA 9012B 1 322148 07/17/20 17:11 CMR TAL PITASTM Leach
SEAL2Instrument ID:
Analysis Moisture 1 625595 07/09/20 07:15 JEB TAL SAVTotal/NA
NOEQUIPInstrument ID:
Client Sample ID: ABP-TP-207 (2.0)Lab Sample ID: 680-185778-9
Matrix: SolidDate Collected: 06/29/20 15:00
Percent Solids: 80.5Date Received: 07/01/20 10:00
Prep 9012A JER07/13/20 12:50 TAL SAV626052
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1.1619 g 6 mL
Analysis 9012A 1 626168 07/13/20 16:00 JER TAL SAVTotal/NA
KONELAB4Instrument ID:
Eurofins TestAmerica, Savannah
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Lab Chronicle
Client: Civil & Environmental Consultants Inc Job ID: 680-185778-1
Project/Site: Badin Business Park
Client Sample ID: ABP-TP-207 (9.5)Lab Sample ID: 680-185778-10
Matrix: SolidDate Collected: 06/29/20 15:10
Date Received: 07/01/20 10:00
Leach D3987-85 GRN07/08/20 16:30 TAL PIT320750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
ASTM Leach 100.64 g 2000 mL
Analysis EPA 300.0 R2.1 1 322104 07/17/20 18:58 EPS TAL PITASTM Leach
CHICS2000Instrument ID:
Leach D3987-85 320750 07/08/20 16:30 GRN TAL PITASTM Leach 100.64 g 2000 mL
Prep 9012B 322056 07/17/20 12:35 CMR TAL PITASTM Leach 6 mL 6 mL
Analysis EPA 9012B 1 322148 07/17/20 17:16 CMR TAL PITASTM Leach
SEAL2Instrument ID:
Analysis Moisture 1 625595 07/09/20 07:15 JEB TAL SAVTotal/NA
NOEQUIPInstrument ID:
Client Sample ID: ABP-TP-207 (9.5)Lab Sample ID: 680-185778-10
Matrix: SolidDate Collected: 06/29/20 15:10
Percent Solids: 79.3Date Received: 07/01/20 10:00
Prep 9012A JER07/13/20 12:50 TAL SAV626052
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1.0212 g 6 mL
Analysis 9012A 1 626168 07/13/20 16:00 JER TAL SAVTotal/NA
KONELAB4Instrument ID:
Client Sample ID: ABP-TP-208 (2.0)Lab Sample ID: 680-185778-11
Matrix: SolidDate Collected: 06/29/20 15:30
Date Received: 07/01/20 10:00
Leach D3987-85 GRN07/08/20 16:30 TAL PIT320750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
ASTM Leach 100.06 g 2000 mL
Analysis EPA 300.0 R2.1 1 322104 07/17/20 19:13 EPS TAL PITASTM Leach
CHICS2000Instrument ID:
Leach D3987-85 320750 07/08/20 16:30 GRN TAL PITASTM Leach 100.06 g 2000 mL
Prep 9012B 322056 07/17/20 12:35 CMR TAL PITASTM Leach 6 mL 6 mL
Analysis EPA 9012B 1 322148 07/17/20 17:17 CMR TAL PITASTM Leach
SEAL2Instrument ID:
Analysis Moisture 1 625595 07/09/20 07:15 JEB TAL SAVTotal/NA
NOEQUIPInstrument ID:
Client Sample ID: ABP-TP-208 (2.0)Lab Sample ID: 680-185778-11
Matrix: SolidDate Collected: 06/29/20 15:30
Percent Solids: 76.9Date Received: 07/01/20 10:00
Prep 9012A JER07/13/20 12:50 TAL SAV626052
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1.1403 g 6 mL
Analysis 9012A 1 626168 07/13/20 16:00 JER TAL SAVTotal/NA
KONELAB4Instrument ID:
Eurofins TestAmerica, Savannah
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Lab Chronicle
Client: Civil & Environmental Consultants Inc Job ID: 680-185778-1
Project/Site: Badin Business Park
Client Sample ID: ABP-TP-208 (9.5)Lab Sample ID: 680-185778-12
Matrix: SolidDate Collected: 06/29/20 15:40
Date Received: 07/01/20 10:00
Leach D3987-85 GRN07/08/20 16:30 TAL PIT320750
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
ASTM Leach 100.08 g 2000 mL
Analysis EPA 300.0 R2.1 1 322104 07/17/20 19:27 EPS TAL PITASTM Leach
CHICS2000Instrument ID:
Leach D3987-85 320750 07/08/20 16:30 GRN TAL PITASTM Leach 100.08 g 2000 mL
Prep 9012B 322056 07/17/20 12:35 CMR TAL PITASTM Leach 6 mL 6 mL
Analysis EPA 9012B 1 322148 07/17/20 17:19 CMR TAL PITASTM Leach
SEAL2Instrument ID:
Analysis Moisture 1 625595 07/09/20 07:15 JEB TAL SAVTotal/NA
NOEQUIPInstrument ID:
Client Sample ID: ABP-TP-208 (9.5)Lab Sample ID: 680-185778-12
Matrix: SolidDate Collected: 06/29/20 15:40
Percent Solids: 74.6Date Received: 07/01/20 10:00
Prep 9012A JER07/13/20 12:50 TAL SAV626052
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1.0651 g 6 mL
Analysis 9012A 1 626168 07/13/20 16:00 JER TAL SAVTotal/NA
KONELAB4Instrument ID:
Laboratory References:
TAL CF = Eurofins TestAmerica, Cedar Falls, 3019 Venture Way, Cedar Falls, IA 50613, TEL [phone]
TAL PIT = Eurofins TestAmerica, Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins TestAmerica, Savannah
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Login Sample Receipt Checklist
Client: Civil & Environmental Consultants Inc Job Number: 680-185778-1
Login Number: 185778
Question Answer Comment
Creator: Banda, Christy S
List Source: Eurofins TestAmerica, Savannah
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins TestAmerica, Savannah
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Login Sample Receipt Checklist
Client: Civil & Environmental Consultants Inc Job Number: 680-185778-1
Login Number: 185778
Question Answer Comment
Creator: Johnson, Josie A
List Source: Eurofins TestAmerica, Cedar Falls
List Creation: 07/07/20 11:43 AMList Number: 3
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
N/AThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins TestAmerica, Savannah
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Login Sample Receipt Checklist
Client: Civil & Environmental Consultants Inc Job Number: 680-185778-1
Login Number: 185778
Question Answer Comment
Creator: Say, Thomas C
List Source: Eurofins TestAmerica, Pittsburgh
List Creation: 07/07/20 11:19 AMList Number: 2
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins TestAmerica, Savannah
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Accreditation/Certification Summary
Client: Civil & Environmental Consultants Inc Job ID: 680-185778-1
Project/Site: Badin Business Park
Laboratory: Eurofins TestAmerica, Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)269State 12-31-20
Laboratory: Eurofins TestAmerica, Cedar Falls
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program Identification Number Expiration Date
AIHA-LAP, LLC 101044Industrial Hygiene Laboratory
Accreditation Program (IHLAP)
11-01-20
Colorado Petroleum Storage Tank Program IA100001 (OR)09-29-20
Georgia State IA100001 (OR)09-29-20
Illinois NELAP 200024 11-29-20
Iowa State 007 12-01-21
Kansas NELAP E-10341 01-31-21
Minnesota NELAP 019-999-319 12-31-20
Minnesota (Petrofund)State 3349 08-22-21
North Dakota State R-186 09-30-20
Oregon NELAP IA100001 09-29-20
USDA US Federal Programs P330-19-00003 01-02-22
Laboratory: Eurofins TestAmerica, Pittsburgh
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program Identification Number Expiration Date
Arkansas DEQ 19-033-0State 06-27-21
California State 2891 04-30-21
Connecticut State PH-0688 09-30-20
Florida NELAP E871008 06-30-21
Georgia State PA 02-00416 04-30-21
Illinois NELAP 004375 06-30-21
Kansas NELAP E-10350 01-31-21
Kentucky (UST)State 162013 04-30-21
Kentucky (WW)State KY98043 12-31-20
Louisiana NELAP 04041 06-30-21
Maine State PA00164 03-06-22
Minnesota NELAP 042-999-482 12-31-20
Nevada State PA00164 07-31-20
New Hampshire NELAP 2030 04-05-21
New Jersey NELAP PA005 06-30-21
New York NELAP 11182 04-01-21
North Carolina (WW/SW)State 434 01-01-21
North Dakota State R-227 04-30-21
Oregon NELAP PA-2151 02-06-21
Pennsylvania NELAP 02-00416 05-23-21
Rhode Island State LAO00362 12-31-20
South Carolina State 89014 04-30-21
Texas NELAP T104704528 03-31-21
US Fish & Wildlife US Federal Programs 058448 07-31-20
USDA Federal P-Soil-01 06-26-22
USDA US Federal Programs P330-16-00211 06-26-22
Utah NELAP PA001462019-8 05-31-21
Virginia NELAP 10043 09-15-20
Eurofins TestAmerica, Savannah
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Accreditation/Certification Summary
Client: Civil & Environmental Consultants Inc Job ID: 680-185778-1
Project/Site: Badin Business Park
Laboratory: Eurofins TestAmerica, Pittsburgh (Continued)
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program Identification Number Expiration Date
West Virginia DEP 142State 02-01-21
Wisconsin State 998027800 08-31-20
Eurofins TestAmerica, Savannah
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ANALYTICAL REPORT
Eurofins TestAmerica, Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-185778-2
Client Project/Site: Badin Business Park
For:
Civil & Environmental Consultants Inc
2704 Cherokee Farm Way
Suite 101
Knoxville, Tennessee 37920
Attn: Michael Worden
Authorized for release by:
8/20/2020 3:34:29 PM
Sheila Hoffman, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Method Summary
Job ID: 680-185778-2Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Method Method Description LaboratoryProtocol
NoneSubcontractASMTD3761/EPA 9056 Fl GeochemTes
Protocol References:
None = None
Laboratory References:
GeochemTes = Geochemical Testing Inc., 2005 North Center Avenue, Somerset, PA 15501
Eurofins TestAmerica, Savannah
Page 2 of 21 8/20/2020
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Sample Summary
Job ID: 680-185778-2Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Lab Sample ID Client Sample ID ReceivedCollectedMatrix Asset ID
680-185778-1 ABP-TP-201 (5.8)Solid 06/29/20 08:50 07/01/20 10:00
680-185778-2 ABP-TP-202 (5.0)Solid 06/29/20 09:45 07/01/20 10:00
680-185778-3 ABP-TP-203 (6.0)Solid 06/29/20 11:00 07/01/20 10:00
680-185778-4 ABP-TP-204 (4.5)Solid 06/29/20 11:40 07/01/20 10:00
680-185778-5 ABP-TP-205 (2.0)Solid 06/29/20 13:15 07/01/20 10:00
680-185778-6 ABP-TP-205 (6.0)Solid 06/29/20 13:50 07/01/20 10:00
680-185778-7 ABP-TP-206 (2.0)Solid 06/29/20 14:05 07/01/20 10:00
680-185778-8 ABP-TP-206 (4.0)Solid 06/29/20 14:20 07/01/20 10:00
680-185778-9 ABP-TP-207 (2.0)Solid 06/29/20 15:00 07/01/20 10:00
680-185778-10 ABP-TP-207 (9.5)Solid 06/29/20 15:10 07/01/20 10:00
680-185778-11 ABP-TP-208 (2.0)Solid 06/29/20 15:30 07/01/20 10:00
680-185778-12 ABP-TP-208 (9.5)Solid 06/29/20 15:40 07/01/20 10:00
Eurofins TestAmerica, Savannah
Page 3 of 21 8/20/2020
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Case Narrative
Client: Civil & Environmental Consultants Inc Job ID: 680-185778-2
Project/Site: Badin Business Park
Job ID: 680-185778-2
Laboratory: Eurofins TestAmerica, Savannah
Narrative
Job Narrative
680-185778-2
Comments
No additional comments.
Receipt
The samples were received on 7/1/2020 10:00 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperatures of the 2 coolers at receipt time were 2.5º C and 3.2º C.
Subcontract Work
Method ASMTD3761/EPA 9056 Fl: This method was subcontracted to Geochemical Testing Inc.. The subcontract laboratory certification
is different from that of the facility issuing the final report.
Eurofins TestAmerica, SavannahPage 4 of 21 8/20/2020
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Thursday, August 20, 2020
TEST AMERICA - PGH
Sheila Hoffman
Dear Sheila Hoffman:
Order No.: G2008378
301 ALPHA DRIVE
RIDC PARK
PITTSBURGH, PA 15238
2005 N. Center Ave.
Somerset, PA 15501
814/443-1671
814/445-6666
FAX: [phone]
Geochemical Testing received 13 sample(s) on 8/6/2020 for the analyses presented in the
following report.
There were no problems with sample receipt protocols and analyses met the TNI/NELAC, EPA,
and laboratory specifications except where noted in the Case Narrative or Laboratory Results.
If you have any questions regarding these tests results, please feel free to call.
Sincerely,
Timothy W. Bergstresser
Director of Technical Services
Report(s) To:
DAVE DUNLAP
Page 1 of 15 Page 5 of 21 8/20/2020
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20-Aug-20Date:Geochemical Testing
Project:
CLIENT:TEST AMERICA - PGH
Lab Order:G2008378 CASE NARRATIVEPWS: 0
No problems were encountered during analysis of this workorder, except if noted in this report.
Legend:
J - Indicates an estimated value.
B - Analyte detected in the associated Method Blank
S - Surrogate Recovery outside accepted recovery limits
ND - Not Detected
E - Value above quantitation range I.D. 56-00306 PA DEP
** - Value exceeds Action Limit
U - The analyte was not detected at or above the listed
concentration, which is below the laboratory quantitation limit.
H - Method Hold Time exceeded and is not compliant with
40CFR136 Table II.
Q - Qualifier DF - Dilution FactorQL -Quantitation Limit
MCL - Contaminant Limit
Q1 - See case narrative
T - Sample received above required temperature and is not
compliant with 40CFR136 Table II.
MDA - Minimum Detectable Activity.
TICs - Tentatively Identified Compounds.
T1 - Sample received above required temperature
Page 2 of 15 Page 6 of 21 8/20/2020
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Project:
Client Sample ID:680-185778-1
Collection Date:6/29/2020 8:50:00 AM
Matrix:SOLID
Analyses Result Q Units Date AnalyzedQL
CLIENT:TEST AMERICA - PGH
Lab Order:G2008378
Lab ID:G2008378-001
DF
Geochemical Testing Date:20-Aug-20
Received Date:8/6/2020 12:30:18 PM
Laboratory Results
Sampled By:Test America
ABP-TP-201 5.8
Date Prepared
FLUORINE EPA 9056AAnalyst:CKT ASTM D 3761
Fluorine 08/14/20 1:46 PM10mg/Kg-dry 1122 08/14/20 8:00 AM
I.D. 56-00306 PA DEP
Page 3 of 15 Page 7 of 21 8/20/2020
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Project:
Client Sample ID:680-185778-2
Collection Date:6/29/2020 9:45:00 AM
Matrix:SOLID
Analyses Result Q Units Date AnalyzedQL
CLIENT:TEST AMERICA - PGH
Lab Order:G2008378
Lab ID:G2008378-002
DF
Geochemical Testing Date:20-Aug-20
Received Date:8/6/2020 12:30:18 PM
Laboratory Results
Sampled By:Test America
ABP-TP-201 5.8
Date Prepared
FLUORINE EPA 9056AAnalyst:CKT ASTM D 3761
Fluorine 08/14/20 1:46 PM10mg/Kg-dry 1139 08/14/20 8:00 AM
I.D. 56-00306 PA DEP
Page 4 of 15 Page 8 of 21 8/20/2020
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Project:
Client Sample ID:680-185778-3
Collection Date:6/29/2020 11:00:00 AM
Matrix:SOLID
Analyses Result Q Units Date AnalyzedQL
CLIENT:TEST AMERICA - PGH
Lab Order:G2008378
Lab ID:G2008378-003
DF
Geochemical Testing Date:20-Aug-20
Received Date:8/6/2020 12:30:18 PM
Laboratory Results
Sampled By:Test America
ABP-TP-201 5.8
Date Prepared
FLUORINE EPA 9056AAnalyst:CKT ASTM D 3761
Fluorine 08/14/20 1:46 PM10mg/Kg-dry 174 08/14/20 8:00 AM
I.D. 56-00306 PA DEP
Page 5 of 15 Page 9 of 21 8/20/2020
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Project:
Client Sample ID:680-185778-4
Collection Date:6/29/2020 11:40:00 AM
Matrix:SOLID
Analyses Result Q Units Date AnalyzedQL
CLIENT:TEST AMERICA - PGH
Lab Order:G2008378
Lab ID:G2008378-004
DF
Geochemical Testing Date:20-Aug-20
Received Date:8/6/2020 12:30:18 PM
Laboratory Results
Sampled By:Test America
ABP-TP-201 5.8
Date Prepared
FLUORINE EPA 9056AAnalyst:CKT ASTM D 3761
Fluorine 08/14/20 1:46 PM10mg/Kg-dry 155 08/14/20 8:00 AM
I.D. 56-00306 PA DEP
Page 6 of 15 Page 10 of 21 8/20/2020
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Project:
Client Sample ID:680-185778-5
Collection Date:6/29/2020 1:15:00 PM
Matrix:SOLID
Analyses Result Q Units Date AnalyzedQL
CLIENT:TEST AMERICA - PGH
Lab Order:G2008378
Lab ID:G2008378-005
DF
Geochemical Testing Date:20-Aug-20
Received Date:8/6/2020 12:30:18 PM
Laboratory Results
Sampled By:Test America
ABP-TP-201 5.8
Date Prepared
FLUORINE EPA 9056AAnalyst:CKT ASTM D 3761
Fluorine 08/14/20 1:46 PM10mg/Kg-dry 1101 08/14/20 8:00 AM
I.D. 56-00306 PA DEP
Page 7 of 15 Page 11 of 21 8/20/2020
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Project:
Client Sample ID:680-185778-6
Collection Date:6/29/2020 1:50:00 PM
Matrix:SOLID
Analyses Result Q Units Date AnalyzedQL
CLIENT:TEST AMERICA - PGH
Lab Order:G2008378
Lab ID:G2008378-006
DF
Geochemical Testing Date:20-Aug-20
Received Date:8/6/2020 12:30:18 PM
Laboratory Results
Sampled By:Test America
ABP-TP-201 5.8
Date Prepared
FLUORINE EPA 9056AAnalyst:CKT ASTM D 3761
Fluorine 08/14/20 1:46 PM10mg/Kg-dry 1197 08/14/20 8:00 AM
I.D. 56-00306 PA DEP
Page 8 of 15 Page 12 of 21 8/20/2020
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Project:
Client Sample ID:680-185778-7
Collection Date:6/29/2020 2:05:00 PM
Matrix:SOLID
Analyses Result Q Units Date AnalyzedQL
CLIENT:TEST AMERICA - PGH
Lab Order:G2008378
Lab ID:G2008378-007
DF
Geochemical Testing Date:20-Aug-20
Received Date:8/6/2020 12:30:18 PM
Laboratory Results
Sampled By:Test America
ABP-TP-201 5.8
Date Prepared
FLUORINE EPA 9056AAnalyst:MBG ASTM D 3761
Fluorine 08/18/20 5:16 PM10mg/Kg-dry 1811 08/14/20 8:00 AM
I.D. 56-00306 PA DEP
Page 9 of 15 Page 13 of 21 8/20/2020
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Project:
Client Sample ID:680-185778-8
Collection Date:6/29/2020 2:20:00 PM
Matrix:SOLID
Analyses Result Q Units Date AnalyzedQL
CLIENT:TEST AMERICA - PGH
Lab Order:G2008378
Lab ID:G2008378-008
DF
Geochemical Testing Date:20-Aug-20
Received Date:8/6/2020 12:30:18 PM
Laboratory Results
Sampled By:Test America
ABP-TP-201 5.8
Date Prepared
FLUORINE EPA 9056AAnalyst:MBG ASTM D 3761
Fluorine 08/17/20 1:00 PM10mg/Kg-dry 17250 08/14/20 8:00 AM
I.D. 56-00306 PA DEP
Page 10 of 15 Page 14 of 21 8/20/2020
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Project:
Client Sample ID:680-185778-9
Collection Date:6/29/2020 3:00:00 PM
Matrix:SOLID
Analyses Result Q Units Date AnalyzedQL
CLIENT:TEST AMERICA - PGH
Lab Order:G2008378
Lab ID:G2008378-009
DF
Geochemical Testing Date:20-Aug-20
Received Date:8/6/2020 12:30:18 PM
Laboratory Results
Sampled By:Test America
ABP-TP-201 5.8
Date Prepared
FLUORINE EPA 9056AAnalyst:MBG ASTM D 3761
Fluorine 08/18/20 5:16 PM10mg/Kg-dry 1264 08/14/20 8:00 AM
I.D. 56-00306 PA DEP
Page 11 of 15 Page 15 of 21 8/20/2020
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Project:
Client Sample ID:680-185778-10
Collection Date:6/29/2020 3:10:00 PM
Matrix:SOLID
Analyses Result Q Units Date AnalyzedQL
CLIENT:TEST AMERICA - PGH
Lab Order:G2008378
Lab ID:G2008378-010
DF
Geochemical Testing Date:20-Aug-20
Received Date:8/6/2020 12:30:18 PM
Laboratory Results
Sampled By:Test America
ABP-TP-201 5.8
Date Prepared
FLUORINE EPA 9056AAnalyst:CKT ASTM D 3761
Fluorine 08/14/20 1:46 PM10mg/Kg-dry 1118 08/14/20 8:00 AM
I.D. 56-00306 PA DEP
Page 12 of 15 Page 16 of 21 8/20/2020
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Project:
Client Sample ID:680-185778-11
Collection Date:6/29/2020 3:30:00 PM
Matrix:SOLID
Analyses Result Q Units Date AnalyzedQL
CLIENT:TEST AMERICA - PGH
Lab Order:G2008378
Lab ID:G2008378-011
DF
Geochemical Testing Date:20-Aug-20
Received Date:8/6/2020 12:30:18 PM
Laboratory Results
Sampled By:Test America
ABP-TP-201 5.8
Date Prepared
FLUORINE EPA 9056AAnalyst:CKT ASTM D 3761
Fluorine 08/14/20 1:46 PM10mg/Kg-dry 1113 08/14/20 8:00 AM
I.D. 56-00306 PA DEP
Page 13 of 15 Page 17 of 21 8/20/2020
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Project:
Client Sample ID:680-185778-12
Collection Date:6/29/2020 3:40:00 PM
Matrix:SOLID
Analyses Result Q Units Date AnalyzedQL
CLIENT:TEST AMERICA - PGH
Lab Order:G2008378
Lab ID:G2008378-012
DF
Geochemical Testing Date:20-Aug-20
Received Date:8/6/2020 12:30:18 PM
Laboratory Results
Sampled By:Test America
ABP-TP-201 5.8
Date Prepared
FLUORINE EPA 9056AAnalyst:MBG ASTM D 3761
Fluorine 08/18/20 5:16 PM10mg/Kg-dry 1285 08/14/20 8:00 AM
I.D. 56-00306 PA DEP
Page 14 of 15 Page 18 of 21 8/20/2020
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Project:
Client Sample ID:180-108140-B-1
Collection Date:7/9/2020 8:30:00 AM
Matrix:SOLID
Analyses Result Q Units Date AnalyzedQL
CLIENT:TEST AMERICA - PGH
Lab Order:G2008378
Lab ID:G2008378-013
DF
Geochemical Testing Date:20-Aug-20
Received Date:8/6/2020 12:30:18 PM
Laboratory Results
Sampled By:Test America
ABP-TP-201 5.8
Date Prepared
FLUORINE EPA 9056AAnalyst:MBG ASTM D 3761
Fluorine 08/18/20 5:16 PM10mg/Kg-dry 11640 08/14/20 8:00 AM
I.D. 56-00306 PA DEP
Page 15 of 15 Page 19 of 21 8/20/2020
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Page 20 of 21 8/20/2020
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Page 21 of 21 8/20/2020
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ANALYTICAL REPORT
Eurofins TestAmerica, Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-185779-1
Client Project/Site: Badin Business Park
Revision: 1
For:
Civil & Environmental Consultants Inc
2704 Cherokee Farm Way
Suite 101
Knoxville, Tennessee 37920
Attn: Michael Worden
Authorized for release by:
7/20/2020 11:38:23 AM
Sheila Hoffman, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Definitions/Glossary
Job ID: 680-185779-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Qualifiers
General Chemistry
Qualifier Description
F1 MS and/or MSD recovery exceeds control limits.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins TestAmerica, Savannah
Page 2 of 15 7/20/2020 (Rev. 1)
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Sample Summary
Job ID: 680-185779-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Lab Sample ID Client Sample ID ReceivedCollectedMatrix Asset ID
680-185779-1 ABP-TP-202W Water 06/29/20 09:45 07/01/20 10:00
680-185779-2 ABP-TP-204W Water 06/29/20 11:40 07/01/20 10:00
680-185779-3 ABP-TP-205W Water 06/29/20 14:35 07/01/20 10:00
Eurofins TestAmerica, Savannah
Page 3 of 15 7/20/2020 (Rev. 1)
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Case Narrative
Client: Civil & Environmental Consultants Inc Job ID: 680-185779-1
Project/Site: Badin Business Park
Job ID: 680-185779-1
Laboratory: Eurofins TestAmerica, Savannah
Narrative
CASE NARRATIVE
Client: Civil & Environmental Consultants Inc
Project: Badin Business Park
Report Number: 680-185779-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
REVISION
Sample ID prefix was revised to ABP
RECEIPT
The samples were received on 07/01/2020; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 2.5 C.
ANIONS BY ION CHROMATOGRAPHY (28 DAY)
Samples ABP-TP-202W (680-185779-1), ABP-TP-204W (680-185779-2) and ABP-TP-205W (680-185779-3) were analyzed for Anions by
Ion Chromatography (28 Day) in accordance with EPA Method 300.0. The samples were analyzed on 07/04/2020 and 07/10/2020.
Sample ABP-TP-205W (680-185779-3)[5X] required dilution prior to analysis. The reporting limits have been adjusted accordingly.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CYANIDE
Samples ABP-TP-202W (680-185779-1), ABP-TP-204W (680-185779-2) and ABP-TP-205W (680-185779-3) were analyzed for cyanide in
accordance with D7511-12. The samples were analyzed on 07/13/2020.
The following samples were found to contain residual chlorine: ABP-TP-202W (680-185779-1), ABP-TP-205W (680-185779-3) and
ABP-TP-204W (680-185779-2). The chlorine was treated and removed prior to preparation/analysis.
Cyanide, Total and Cyanide, Total failed the recovery criteria low for the MS of sample ABP-TP-205WMS (680-185779-3) in batch
410-22809.
Refer to the QC report for details.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins TestAmerica, SavannahPage 4 of 15 7/20/2020 (Rev. 1)
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Client Sample Results
Job ID: 680-185779-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Lab Sample ID: 680-185779-1Client Sample ID: ABP-TP-202W
Matrix: WaterDate Collected: 06/29/20 09:45
Date Received: 07/01/20 10:00
Method: 300.0-1993 R2.1 - Anions, Ion Chromatography
RL MDL
Fluoride 3.3 0.10 mg/L 07/04/20 07:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total <0.0060 0.0060 mg/L 07/13/20 15:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185779-2Client Sample ID: ABP-TP-204W
Matrix: WaterDate Collected: 06/29/20 11:40
Date Received: 07/01/20 10:00
Method: 300.0-1993 R2.1 - Anions, Ion Chromatography
RL MDL
Fluoride 2.0 0.10 mg/L 07/04/20 07:22 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total <0.0060 0.0060 mg/L 07/13/20 15:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 680-185779-3Client Sample ID: ABP-TP-205W
Matrix: WaterDate Collected: 06/29/20 14:35
Date Received: 07/01/20 10:00
Method: 300.0-1993 R2.1 - Anions, Ion Chromatography
RL MDL
Fluoride 21 0.50 mg/L 07/10/20 18:33 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total <0.0060 F1 0.0060 mg/L 07/13/20 15:06 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Eurofins TestAmerica, Savannah
Page 5 of 15 7/20/2020 (Rev. 1)
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QC Sample Results
Job ID: 680-185779-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Method: 300.0-1993 R2.1 - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 680-625066/33
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625066
RL MDL
Fluoride <0.10 0.10 mg/L 07/04/20 01:27 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-625066/34
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625066
Fluoride 2.00 1.92 mg/L 96 90-110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-625066/35
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625066
Fluoride 2.00 1.90 mg/L 95 90-110 1 15
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Method BlankLab Sample ID: MB 680-625870/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625870
RL MDL
Fluoride <0.10 0.10 mg/L 07/10/20 14:49 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-625870/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625870
Fluoride 2.00 1.92 mg/L 96 90-110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-625870/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 625870
Fluoride 2.00 1.91 mg/L 96 90-110 0 15
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Method: D7511-12 - Total Cyanide
Client Sample ID: Method BlankLab Sample ID: MB 410-22809/19
Matrix: Water Prep Type: Total/NA
Analysis Batch: 22809
RL MDL
Cyanide, Total <0.0060 0.0060 mg/L 07/13/20 15:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Eurofins TestAmerica, Savannah
Page 6 of 15 7/20/2020 (Rev. 1)
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QC Sample Results
Job ID: 680-185779-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Method: D7511-12 - Total Cyanide (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-22809/18
Matrix: Water Prep Type: Total/NA
Analysis Batch: 22809
Cyanide, Total 0.0403 0.0401 mg/L 99 84-116
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: ABP-TP-205WLab Sample ID: 680-185779-3 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 22809
Cyanide, Total <0.0060 F1 0.0200 0.0158 F1 mg/L 79 84-116
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: ABP-TP-205WLab Sample ID: 680-185779-3 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 22809
Cyanide, Total <0.0060 F1 0.0200 0.0162 F1 mg/L 81 84-116
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: ABP-TP-205WLab Sample ID: 680-185779-3 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 22809
Cyanide, Total <0.0060 F1 <0.0060 mg/L NC 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Eurofins TestAmerica, Savannah
Page 7 of 15 7/20/2020 (Rev. 1)
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QC Association Summary
Job ID: 680-185779-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
HPLC/IC
Analysis Batch: 625066
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 300.0-1993 R2.1680-185779-1 ABP-TP-202W Total/NA
Water 300.0-1993 R2.1680-185779-2 ABP-TP-204W Total/NA
Water 300.0-1993 R2.1MB 680-625066/33 Method Blank Total/NA
Water 300.0-1993 R2.1LCS 680-625066/34 Lab Control Sample Total/NA
Water 300.0-1993 R2.1LCSD 680-625066/35 Lab Control Sample Dup Total/NA
Analysis Batch: 625870
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 300.0-1993 R2.1680-185779-3 ABP-TP-205W Total/NA
Water 300.0-1993 R2.1MB 680-625870/2 Method Blank Total/NA
Water 300.0-1993 R2.1LCS 680-625870/3 Lab Control Sample Total/NA
Water 300.0-1993 R2.1LCSD 680-625870/4 Lab Control Sample Dup Total/NA
General Chemistry
Analysis Batch: 22809
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water D7511-12680-185779-1 ABP-TP-202W Total/NA
Water D7511-12680-185779-2 ABP-TP-204W Total/NA
Water D7511-12680-185779-3 ABP-TP-205W Total/NA
Water D7511-12MB 410-22809/19 Method Blank Total/NA
Water D7511-12LCS 410-22809/18 Lab Control Sample Total/NA
Water D7511-12680-185779-3 MS ABP-TP-205W Total/NA
Water D7511-12680-185779-3 MS ABP-TP-205W Total/NA
Water D7511-12680-185779-3 DU ABP-TP-205W Total/NA
Eurofins TestAmerica, Savannah
Page 8 of 15 7/20/2020 (Rev. 1)
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Lab Chronicle
Client: Civil & Environmental Consultants Inc Job ID: 680-185779-1
Project/Site: Badin Business Park
Client Sample ID: ABP-TP-202W Lab Sample ID: 680-185779-1
Matrix: WaterDate Collected: 06/29/20 09:45
Date Received: 07/01/20 10:00
Analysis 300.0-1993 R2.1 UI07/04/20 07:091 TAL SAV625066
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CICK
Analysis D7511-12 1 22809 07/13/20 15:18 L8MI ELLETotal/NA
22683_AmpInstrument ID:
Client Sample ID: ABP-TP-204W Lab Sample ID: 680-185779-2
Matrix: WaterDate Collected: 06/29/20 11:40
Date Received: 07/01/20 10:00
Analysis 300.0-1993 R2.1 UI07/04/20 07:221 TAL SAV625066
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CICK
Analysis D7511-12 1 22809 07/13/20 15:15 L8MI ELLETotal/NA
22683_AmpInstrument ID:
Client Sample ID: ABP-TP-205W Lab Sample ID: 680-185779-3
Matrix: WaterDate Collected: 06/29/20 14:35
Date Received: 07/01/20 10:00
Analysis 300.0-1993 R2.1 CS07/10/20 18:335 TAL SAV625870
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CICK
Analysis D7511-12 1 22809 07/13/20 15:06 L8MI ELLETotal/NA
22683_AmpInstrument ID:
Laboratory References:
ELLE = Eurofins Lancaster Laboratories Env, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL [phone]
TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins TestAmerica, Savannah
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Accreditation/Certification Summary
Client: Civil & Environmental Consultants Inc Job ID: 680-185779-1
Project/Site: Badin Business Park
Laboratory: Eurofins TestAmerica, Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)269State 12-31-20
Laboratory: Eurofins Lancaster Laboratories Env, LLC
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)521State 12-31-20
Eurofins TestAmerica, Savannah
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Method Summary
Job ID: 680-185779-1Client: Civil & Environmental Consultants Inc
Project/Site: Badin Business Park
Method Method Description LaboratoryProtocol
MCAWW300.0-1993 R2.1 Anions, Ion Chromatography TAL SAV
ASTMD7511-12 Total Cyanide ELLE
Protocol References:
ASTM = ASTM International
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
Laboratory References:
ELLE = Eurofins Lancaster Laboratories Env, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL [phone]
TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins TestAmerica, Savannah
Page 11 of 15 7/20/2020 (Rev. 1)
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Page 12 of 15 7/20/2020 (Rev. 1)
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Login Sample Receipt Checklist
Client: Civil & Environmental Consultants Inc Job Number: 680-185779-1
Login Number: 185779
Question Answer Comment
Creator: Banda, Christy S
List Source: Eurofins TestAmerica, Savannah
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins TestAmerica, Savannah
Page 14 of 15 7/20/2020 (Rev. 1)
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Login Sample Receipt Checklist
Client: Civil & Environmental Consultants Inc Job Number: 680-185779-1
Login Number: 185779
Question Answer Comment
Creator: Rivera-Santa, Julissa
List Source: Eurofins Lancaster Laboratories Env
List Creation: 07/07/20 01:15 PMList Number: 2
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable (</=6C, not frozen).
TrueCooler Temperature is recorded.
N/AWV: Container Temperature is acceptable (</=6C, not frozen).
N/AWV: Container Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueThere is sufficient vol. for all requested analyses.
TrueMultiphasic samples are not present.
N/ASamples do not require splitting or compositing.
FalseIs the Field Sampler's name present on COC?Received project as a subcontract.
N/ASample Preservation Verified.
N/AResidual Chlorine Checked.
N/ASample custody seals are intact.
Eurofins TestAmerica, Savannah
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Attachment 4
Laboratory Report – Bath Mill Soils
Composite
ANALYTICAL REPORT
Eurofins TestAmerica, Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-195839-1
Client Project/Site: Alcoa - Badin, NC-Waste Characterization
For:
Civil & Environmental Consultants Inc
2704 Cherokee Farm Way
Suite 101
Knoxville, Tennessee 37920
Attn: Michael Worden
Authorized for release by:
3/15/2021 4:10:55 PM
Sheila Hoffman, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Method Summary
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
Method Method Description LaboratoryProtocol
40CFR136A624.1 Volatile Organic Compounds (GC/MS)TAL SAV
SW8468260DVolatile Organic Compounds by GC/MS TAL SAV
SW8468270ESemivolatile Organic Compounds (GC/MS)TAL SAV
MCAWW300.0 Anions, Ion Chromatography TAL SAV
SW8469056AAnions, Ion Chromatography TAL SAV
SW8466010DMetals (ICP)TAL SAV
SW8467470AMercury (CVAA)TAL SAV
SW8461030Ignitability, Solids TAL SAV
SM2540 D-2011 Total Suspended Solids (Dried at 103-105°C)TAL SAV
SW8469012BCyanide, Total andor Amenable TAL SAV
SW8469034Sulfide, Acid Soluble and Insoluble (Titrimetric)TAL SAV
SW8469045DpH TAL SAV
EPAMoisturePercent Moisture TAL SAV
SW8461311TCLP Extraction TAL SAV
SW8463010APreparation, Total Metals TAL SAV
SW8463510CLiquid-Liquid Extraction (Separatory Funnel)TAL SAV
SW8465030BPurge and Trap TAL SAV
SW8467470APreparation, Mercury TAL SAV
SW8469012BCyanide, Total and/or Amenable, Distillation TAL SAV
SW8469013Cyanide Extraction (Solids and Oils)TAL SAV
SW8469030BSulfide, Distillation (Acid Soluble and Insoluble)TAL SAV
ASTMDI Leach Deionized Water Leaching Procedure TAL SAV
Protocol References:
40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 40CFR, Part 136, Appendix A, October 26, 1984 and
subsequent revisions.
ASTM = ASTM International
EPA = US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins TestAmerica, Savannah
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Sample Summary
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
Lab Sample ID Client Sample ID ReceivedCollectedMatrix Asset ID
680-195839-1 204 Bath Mill Area Solid 03/04/21 09:30 03/05/21 10:00
680-195839-2 Outfall 012 Water 03/02/21 10:30 03/05/21 10:00
680-195839-3 Trip Blank Water 03/02/21 00:00 03/05/21 10:00
Eurofins TestAmerica, Savannah
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Definitions/Glossary
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
Qualifiers
GC/MS VOA
Qualifier Description
*+LCS and/or LCSD is outside acceptance limits, high biased.
Qualifier
GC/MS Semi VOA
Qualifier Description
*-LCS and/or LCSD is outside acceptance limits, low biased.
Qualifier
F1 MS and/or MSD recovery exceeds control limits.
F2 MS/MSD RPD exceeds control limits
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
General Chemistry
Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins TestAmerica, Savannah
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Case Narrative
Client: Civil & Environmental Consultants Inc Job ID: 680-195839-1
Project/Site: Alcoa - Badin, NC-Waste Characterization
Job ID: 680-195839-1
Laboratory: Eurofins TestAmerica, Savannah
Narrative
CASE NARRATIVE
Client: Civil & Environmental Consultants Inc
Project: Alcoa - Badin, NC-Waste Characterization
Report Number: 680-195839-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 03/05/2021; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 0.6 C.
VOLATILE ORGANIC COMPOUNDS (GC/MS)
Samples Outfall 012 (680-195839-2) and Trip Blank (680-195839-3) were analyzed for Volatile Organic Compounds (GC/MS) in
accordance with EPA Method 624. The samples were analyzed on 03/08/2021.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TCLP VOLATILES BY GC/MS
Sample 204 Bath Mill Area (680-195839-1) was analyzed for TCLP Volatiles by GC/MS in accordance with EPA SW-846 Method 1311. The
samples were leached on 03/08/2021 and analyzed on 03/10/2021.
Sample 204 Bath Mill Area (680-195839-1)[20X] required dilution prior to analysis. The reporting limits have been adjusted accordingly.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
SEMIVOLATILE ORGANIC COMPOUNDS (GC-MS) - TCLP
Sample 204 Bath Mill Area (680-195839-1) was analyzed for semivolatile organic compounds (GC-MS) - TCLP in accordance with 8270E.
The samples were leached on 03/09/2021, prepared on 03/11/2021 and analyzed on 03/12/2021.
The following analyte recovered outside control limits for the LCS associated with preparation batch 680-658991 and analytical batch
680-659117: 1,4-Dichlorobenzene. This is not indicative of a systematic control problem because these were random marginal
exceedances. Qualified results have been reported.
The laboratory control sample and/or the laboratory control sample duplicate (LCS/LCSD) for preparation batch 680-658991 and analytical
batch 680-659117 recovered outside control limits for the following analyte: Hexachloroethane. Hexachloroethane has been identified as
a poor performing analyte when analyzed using this method; therefore, re-extraction/re-analysis was not performed. These results have
been reported and qualified.
Refer to the QC report for details.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
9056 ANIONS
Sample 204 Bath Mill Area (680-195839-1) was analyzed for 9056 Anions in accordance with EPA SW-846 Method 9056 (DI Leach). The
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Case Narrative
Client: Civil & Environmental Consultants Inc Job ID: 680-195839-1
Project/Site: Alcoa - Badin, NC-Waste Characterization
Job ID: 680-195839-1 (Continued)
Laboratory: Eurofins TestAmerica, Savannah (Continued)
samples were leached on 03/09/2021 and analyzed on 03/10/2021.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
METALS BY ICP (TCLP)
Sample 204 Bath Mill Area (680-195839-1) was analyzed for Metals by ICP (TCLP) in accordance with EPA SW-846 Method 1311/6010D.
The samples were leached on 03/09/2021, and prepared and analyzed on 03/10/2021.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
METALS (ICP)
Sample Outfall 012 (680-195839-2) was analyzed for Metals (ICP) in accordance with SW-846 Method 6010D. The samples were
prepared on 03/08/2021 and analyzed on 03/09/2021.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
MERCURY - TCLP
Sample 204 Bath Mill Area (680-195839-1) was analyzed for mercury - TCLP in accordance with EPA SW-846 Methods 1311/7470A. The
samples were leached on 03/09/2021, and prepared and analyzed on 03/10/2021.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
IGNITABILITY FOR SOLIDS
Sample 204 Bath Mill Area (680-195839-1) was analyzed for ignitability for solids in accordance with EPA SW-846 Method 1030. The
samples were analyzed on 03/08/2021.
The following sample did not ignite: 204 Bath Mill Area (680-195839-1); therefore, an ignitability value could not be obtained. The result
has been reported as "No Burn" (NB).
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL SUSPENDED SOLIDS
Sample Outfall 012 (680-195839-2) was analyzed for total suspended solids in accordance with SM 2540D. The samples were analyzed
on 03/09/2021.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
ANIONS BY ION CHROMATOGRAPHY (28 DAY)
Sample Outfall 012 (680-195839-2) was analyzed for Anions by Ion Chromatography (28 Day) in accordance with EPA Method 300.0. The
samples were analyzed on 03/08/2021.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CYANIDE
Sample 204 Bath Mill Area (680-195839-1) was analyzed for Cyanide in accordance with EPA SW-846 Method 9012B. The samples were
leached on 03/11/2021, and prepared and analyzed on 03/14/2021.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL SULFIDE
Sample 204 Bath Mill Area (680-195839-1) was analyzed for total sulfide in accordance with EPA SW-846 Method 9034. The samples were
prepared and analyzed on 03/09/2021.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Case Narrative
Client: Civil & Environmental Consultants Inc Job ID: 680-195839-1
Project/Site: Alcoa - Badin, NC-Waste Characterization
Job ID: 680-195839-1 (Continued)
Laboratory: Eurofins TestAmerica, Savannah (Continued)
CORROSIVITY (PH)
Sample 204 Bath Mill Area (680-195839-1) was analyzed for corrosivity (pH) in accordance with EPA SW-846 Method 9045D. The samples
were analyzed on 03/10/2021.
This analysis is considered a field test and is to be performed within 15 minutes of collection. This sample(s) was performed in the
laboratory outside the 15 minute timeframe.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
PERCENT SOLIDS/MOISTURE
Sample 204 Bath Mill Area (680-195839-1) was analyzed for Percent Solids/Moisture in accordance with TestAmerica SOP. The samples
were analyzed on 03/08/2021.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Client Sample Results
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
Lab Sample ID: 680-195839-1Client Sample ID: 204 Bath Mill Area
Matrix: SolidDate Collected: 03/04/21 09:30
Date Received: 03/05/21 10:00
Method: 8260D - Volatile Organic Compounds by GC/MS - TCLP
RL MDL
1,1-Dichloroethene <0.0072 0.020 0.0072 mg/L 03/10/21 07:25 20
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.020 0.010 mg/L 03/10/21 07:25 201,2-Dichloroethane <0.010
0.020 0.0092 mg/L 03/10/21 07:25 201,4-Dichlorobenzene <0.0092
0.20 0.068 mg/L 03/10/21 07:25 202-Butanone (MEK)<0.068 *+
0.020 0.0086 mg/L 03/10/21 07:25 20Benzene<0.0086
0.020 0.0066 mg/L 03/10/21 07:25 20Carbon tetrachloride <0.0066
0.020 0.0052 mg/L 03/10/21 07:25 20Chlorobenzene<0.0052
0.020 0.010 mg/L 03/10/21 07:25 20Chloroform<0.010
0.10 0.050 mg/L 03/10/21 07:25 20Hexachlorobutadiene<0.050
0.020 0.015 mg/L 03/10/21 07:25 20Tetrachloroethene<0.015
0.020 0.0096 mg/L 03/10/21 07:25 20Trichloroethene<0.0096
0.020 0.010 mg/L 03/10/21 07:25 20Vinyl chloride <0.010
4-Bromofluorobenzene (Surr)104 70-130 03/10/21 07:25 20
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)105 03/10/21 07:25 2070-130
Toluene-d8 (Surr)110 03/10/21 07:25 2070-130
1,2-Dichloroethane-d4 (Surr)93 03/10/21 07:25 2060-124
Method: 8270E - Semivolatile Organic Compounds (GC/MS) - TCLP
RL MDL
1,4-Dichlorobenzene <0.016 F2 *-0.050 0.016 mg/L 03/11/21 08:13 03/12/21 16:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.25 0.037 mg/L 03/11/21 08:13 03/12/21 16:49 1Pyridine<0.037 F2 F1
0.050 0.0080 mg/L 03/11/21 08:13 03/12/21 16:49 1Hexachlorobenzene<0.0080
0.050 0.012 mg/L 03/11/21 08:13 03/12/21 16:49 12,4-Dinitrotoluene <0.012
0.050 0.018 mg/L 03/11/21 08:13 03/12/21 16:49 1Hexachloroethane<0.018 F2 *-
0.050 0.020 mg/L 03/11/21 08:13 03/12/21 16:49 1Hexachlorobutadiene<0.020 F2
0.25 0.050 mg/L 03/11/21 08:13 03/12/21 16:49 1Pentachlorophenol<0.050
0.050 0.011 mg/L 03/11/21 08:13 03/12/21 16:49 12,4,6-Trichlorophenol <0.011
0.050 0.016 mg/L 03/11/21 08:13 03/12/21 16:49 12,4,5-Trichlorophenol <0.016
0.050 0.018 mg/L 03/11/21 08:13 03/12/21 16:49 1Nitrobenzene<0.018
0.050 0.0090 mg/L 03/11/21 08:13 03/12/21 16:49 12-Methylphenol <0.0090
0.050 0.0070 mg/L 03/11/21 08:13 03/12/21 16:49 13 & 4 Methylphenol <0.0070
2,4,6-Tribromophenol (Surr)106 10-130 03/11/21 08:13 03/12/21 16:49 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorobiphenyl (Surr)52 03/11/21 08:13 03/12/21 16:49 110-130
2-Fluorophenol (Surr)29 03/11/21 08:13 03/12/21 16:49 110-130
Terphenyl-d14 (Surr)112 03/11/21 08:13 03/12/21 16:49 113-130
Phenol-d5 (Surr)21 03/11/21 08:13 03/12/21 16:49 110-130
Nitrobenzene-d5 (Surr)57 03/11/21 08:13 03/12/21 16:49 111-130
Method: 6010D - Metals (ICP) - TCLP
RL MDL
Arsenic <0.20 0.20 0.20 mg/L 03/10/21 11:10 03/10/21 20:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.0 1.0 mg/L 03/10/21 11:10 03/10/21 20:33 1Barium<1.0
0.10 0.10 mg/L 03/10/21 11:10 03/10/21 20:33 1Cadmium<0.10
0.20 0.20 mg/L 03/10/21 11:10 03/10/21 20:33 1Chromium<0.20
0.20 0.20 mg/L 03/10/21 11:10 03/10/21 20:33 1Lead<0.20
0.50 0.50 mg/L 03/10/21 11:10 03/10/21 20:33 1Selenium<0.50
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Client Sample Results
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
Lab Sample ID: 680-195839-1Client Sample ID: 204 Bath Mill Area
Matrix: SolidDate Collected: 03/04/21 09:30
Date Received: 03/05/21 10:00
Method: 6010D - Metals (ICP) - TCLP (Continued)
RL MDL
Silver <0.10 0.10 0.10 mg/L 03/10/21 11:10 03/10/21 20:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: 7470A - Mercury (CVAA) - TCLP
RL MDL
Mercury <0.020 0.020 0.020 mg/L 03/10/21 11:49 03/10/21 20:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
NONE NONE
Ignitability NB mm/sec 03/08/21 11:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
RL RL
Temperature 19.6 HF 0.1 0.1 Celsius 03/10/21 10:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.1 0.1 PH Units 03/10/21 10:59 1Soil pH in Water 8.6 HF
Lab Sample ID: 680-195839-1Client Sample ID: 204 Bath Mill Area
Matrix: SolidDate Collected: 03/04/21 09:30
Percent Solids: 79.8Date Received: 03/05/21 10:00
Method: 9056A - Anions, Ion Chromatography - Soluble
RL MDL
Fluoride 53 2.5 1.0 mg/Kg ☼03/10/21 15:49 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL MDL
Cyanide, Total <0.63 0.63 0.63 mg/Kg ☼03/14/21 15:29 03/14/21 16:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
74 74 mg/Kg 03/09/21 08:01 03/09/21 09:43 1☼Sulfide 140
Lab Sample ID: 680-195839-2Client Sample ID: Outfall 012
Matrix: WaterDate Collected: 03/02/21 10:30
Date Received: 03/05/21 10:00
Method: 624.1 - Volatile Organic Compounds (GC/MS)
RL MDL
Trichloroethene <0.48 1.0 0.48 ug/L 03/08/21 16:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichloroethane-d4 (Surr)85 60-140 03/08/21 16:51 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)93 03/08/21 16:51 160-140
Dibromofluoromethane (Surr)86 03/08/21 16:51 160-140
Toluene-d8 (Surr)95 03/08/21 16:51 160-140
Method: 300.0 - Anions, Ion Chromatography
RL MDL
Fluoride 1.1 0.10 0.040 mg/L 03/08/21 17:22 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Method: 6010D - Metals (ICP)
RL MDL
Aluminum 40 J 200 24 ug/L 03/08/21 11:55 03/09/21 22:22 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Total Suspended Solids <3.3 3.3 3.3 mg/L 03/09/21 15:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Eurofins TestAmerica, Savannah
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Client Sample Results
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
Lab Sample ID: 680-195839-3Client Sample ID: Trip Blank
Matrix: WaterDate Collected: 03/02/21 00:00
Date Received: 03/05/21 10:00
Method: 624.1 - Volatile Organic Compounds (GC/MS)
RL MDL
Trichloroethene <0.48 1.0 0.48 ug/L 03/08/21 14:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dichloroethane-d4 (Surr)91 60-140 03/08/21 14:53 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)107 03/08/21 14:53 160-140
Dibromofluoromethane (Surr)106 03/08/21 14:53 160-140
Toluene-d8 (Surr)107 03/08/21 14:53 160-140
Eurofins TestAmerica, Savannah
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QC Sample Results
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
Method: 624.1 - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-658413/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 658413
RL MDL
Trichloroethene <0.48 1.0 0.48 ug/L 03/08/21 12:59 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
1,2-Dichloroethane-d4 (Surr)87 60-140 03/08/21 12:59 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
91 03/08/21 12:59 14-Bromofluorobenzene (Surr)60-140
86 03/08/21 12:59 1Dibromofluoromethane (Surr)60-140
90 03/08/21 12:59 1Toluene-d8 (Surr)60-140
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-658413/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 658413
Trichloroethene 50.0 44.1 ug/L 88 65-135
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dichloroethane-d4 (Surr)60 -140
Surrogate
97
LCS LCS
Qualifier Limits%Recovery
884-Bromofluorobenzene (Surr)60 -140
94Dibromofluoromethane (Surr)60 -140
88Toluene-d8 (Surr)60 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-658413/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 658413
Trichloroethene 50.0 43.7 ug/L 87 65-135 1 48
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,2-Dichloroethane-d4 (Surr)60 -140
Surrogate
100
LCSD LCSD
Qualifier Limits%Recovery
874-Bromofluorobenzene (Surr)60 -140
96Dibromofluoromethane (Surr)60 -140
88Toluene-d8 (Surr)60 -140
Client Sample ID: Method BlankLab Sample ID: MB 680-658417/10
Matrix: Water Prep Type: Total/NA
Analysis Batch: 658417
RL MDL
Trichloroethene <0.48 1.0 0.48 ug/L 03/08/21 14:04 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
1,2-Dichloroethane-d4 (Surr)92 60-140 03/08/21 14:04 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
103 03/08/21 14:04 14-Bromofluorobenzene (Surr)60-140
108 03/08/21 14:04 1Dibromofluoromethane (Surr)60-140
103 03/08/21 14:04 1Toluene-d8 (Surr)60-140
Eurofins TestAmerica, Savannah
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QC Sample Results
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
Method: 624.1 - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-658417/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 658417
Trichloroethene 50.0 51.0 ug/L 102 65-135
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dichloroethane-d4 (Surr)60 -140
Surrogate
112
LCS LCS
Qualifier Limits%Recovery
964-Bromofluorobenzene (Surr)60 -140
113Dibromofluoromethane (Surr)60 -140
103Toluene-d8 (Surr)60 -140
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-658417/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 658417
Trichloroethene 50.0 51.1 ug/L 102 65-135 0 48
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,2-Dichloroethane-d4 (Surr)60 -140
Surrogate
102
LCSD LCSD
Qualifier Limits%Recovery
1034-Bromofluorobenzene (Surr)60 -140
105Dibromofluoromethane (Surr)60 -140
101Toluene-d8 (Surr)60 -140
Method: 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-658727/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 658727
1,1-Dichloroethene 0.0500 0.0513 mg/L 103 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dichloroethane 0.0500 0.0548 mg/L 110 70-130
1,4-Dichlorobenzene 0.0500 0.0521 mg/L 104 70-130
2-Butanone (MEK)0.250 0.302 *+mg/L 121 69-114
Benzene 0.0500 0.0496 mg/L 99 70-130
Carbon tetrachloride 0.0500 0.0484 mg/L 97 70-130
Chlorobenzene 0.0500 0.0485 mg/L 97 70-130
Chloroform 0.0500 0.0508 mg/L 102 70-130
Hexachlorobutadiene 0.0500 0.0499 mg/L 100 70-130
Tetrachloroethene 0.0500 0.0530 mg/L 106 70-130
Trichloroethene 0.0500 0.0532 mg/L 106 70-130
Vinyl chloride 0.0500 0.0532 mg/L 106 66-129
4-Bromofluorobenzene (Surr)70 -130
Surrogate
105
LCS LCS
Qualifier Limits%Recovery
111Dibromofluoromethane (Surr)70 -130
100Toluene-d8 (Surr)70 -130
1141,2-Dichloroethane-d4 (Surr)60 -124
Eurofins TestAmerica, Savannah
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QC Sample Results
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: LB 680-658454/1-A
Matrix: Solid Prep Type: TCLP
Analysis Batch: 658727
RL MDL
1,1-Dichloroethene <0.0072 0.020 0.0072 mg/L 03/10/21 04:58 20
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.010 0.0100.020 mg/L 03/10/21 04:58 201,2-Dichloroethane
<0.0092 0.00920.020 mg/L 03/10/21 04:58 201,4-Dichlorobenzene
<0.068 0.0680.20 mg/L 03/10/21 04:58 202-Butanone (MEK)
<0.0086 0.00860.020 mg/L 03/10/21 04:58 20Benzene
<0.0066 0.00660.020 mg/L 03/10/21 04:58 20Carbon tetrachloride
<0.0052 0.00520.020 mg/L 03/10/21 04:58 20Chlorobenzene
<0.010 0.0100.020 mg/L 03/10/21 04:58 20Chloroform
<0.050 0.0500.10 mg/L 03/10/21 04:58 20Hexachlorobutadiene
<0.015 0.0150.020 mg/L 03/10/21 04:58 20Tetrachloroethene
<0.0096 0.00960.020 mg/L 03/10/21 04:58 20Trichloroethene
<0.010 0.0100.020 mg/L 03/10/21 04:58 20Vinyl chloride
4-Bromofluorobenzene (Surr)106 70-130 03/10/21 04:58 20
LB LB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
105 03/10/21 04:58 20Dibromofluoromethane (Surr)70-130
105 03/10/21 04:58 20Toluene-d8 (Surr)70-130
92 03/10/21 04:58 201,2-Dichloroethane-d4 (Surr)60-124
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 680-658991/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 659117 Prep Batch: 658991
RL MDL
1,4-Dichlorobenzene <0.0032 0.010 0.0032 mg/L 03/11/21 08:13 03/11/21 23:00 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.0074 0.00740.050 mg/L 03/11/21 08:13 03/11/21 23:00 1Pyridine
<0.0016 0.00160.010 mg/L 03/11/21 08:13 03/11/21 23:00 1Hexachlorobenzene
<0.0024 0.00240.010 mg/L 03/11/21 08:13 03/11/21 23:00 12,4-Dinitrotoluene
<0.0036 0.00360.010 mg/L 03/11/21 08:13 03/11/21 23:00 1Hexachloroethane
<0.0040 0.00400.010 mg/L 03/11/21 08:13 03/11/21 23:00 1Hexachlorobutadiene
<0.010 0.0100.050 mg/L 03/11/21 08:13 03/11/21 23:00 1Pentachlorophenol
<0.0022 0.00220.010 mg/L 03/11/21 08:13 03/11/21 23:00 12,4,6-Trichlorophenol
<0.0032 0.00320.010 mg/L 03/11/21 08:13 03/11/21 23:00 12,4,5-Trichlorophenol
<0.0036 0.00360.010 mg/L 03/11/21 08:13 03/11/21 23:00 1Nitrobenzene
<0.0018 0.00180.010 mg/L 03/11/21 08:13 03/11/21 23:00 12-Methylphenol
<0.0014 0.00140.010 mg/L 03/11/21 08:13 03/11/21 23:00 13 & 4 Methylphenol
2,4,6-Tribromophenol (Surr)120 10-130 03/11/21 23:00 1
MB MB
Surrogate
03/11/21 08:13
Dil FacPreparedAnalyzedQualifierLimits%Recovery
70 03/11/21 08:13 03/11/21 23:00 12-Fluorobiphenyl (Surr)10-130
36 03/11/21 08:13 03/11/21 23:00 12-Fluorophenol (Surr)10-130
114 03/11/21 08:13 03/11/21 23:00 1Terphenyl-d14 (Surr)13-130
25 03/11/21 08:13 03/11/21 23:00 1Phenol-d5 (Surr)10-130
72 03/11/21 08:13 03/11/21 23:00 1Nitrobenzene-d5 (Surr)11-130
Eurofins TestAmerica, Savannah
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QC Sample Results
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-658991/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 659117 Prep Batch: 658991
1,4-Dichlorobenzene 0.200 0.0556 *-mg/L 28 30-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Pyridine 0.400 0.129 mg/L 32 30-130
Hexachlorobenzene 0.200 0.184 mg/L 92 30-130
2,4-Dinitrotoluene 0.200 0.198 mg/L 99 30-130
Hexachloroethane 0.200 0.0421 *-mg/L 21 30-130
Hexachlorobutadiene 0.200 0.0736 mg/L 37 30-130
Pentachlorophenol 0.400 0.311 mg/L 78 30-130
2,4,6-Trichlorophenol 0.200 0.161 mg/L 81 30-130
2,4,5-Trichlorophenol 0.200 0.163 mg/L 81 30-130
Nitrobenzene 0.200 0.140 mg/L 70 30-130
2-Methylphenol 0.200 0.0990 mg/L 49 30-130
3 & 4 Methylphenol 0.200 0.0959 mg/L 48 30-130
2,4,6-Tribromophenol (Surr)10 -130
Surrogate
119
LCS LCS
Qualifier Limits%Recovery
632-Fluorobiphenyl (Surr)10 -130
322-Fluorophenol (Surr)10 -130
118Terphenyl-d14 (Surr)13 -130
21Phenol-d5 (Surr)10 -130
58Nitrobenzene-d5 (Surr)11 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-658991/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 659117 Prep Batch: 658991
1,4-Dichlorobenzene 0.200 0.0627 mg/L 31 30-130 12 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Pyridine 0.400 0.167 mg/L 42 30-130 26 30
Hexachlorobenzene 0.200 0.184 mg/L 92 30-130 0 30
2,4-Dinitrotoluene 0.200 0.219 mg/L 109 30-130 10 30
Hexachloroethane 0.200 0.0461 *-mg/L 23 30-130 9 30
Hexachlorobutadiene 0.200 0.0722 mg/L 36 30-130 2 30
Pentachlorophenol 0.400 0.325 mg/L 81 30-130 4 30
2,4,6-Trichlorophenol 0.200 0.199 mg/L 99 30-130 21 30
2,4,5-Trichlorophenol 0.200 0.190 mg/L 95 30-130 16 30
Nitrobenzene 0.200 0.168 mg/L 84 30-130 18 30
2-Methylphenol 0.200 0.128 mg/L 64 30-130 25 30
3 & 4 Methylphenol 0.200 0.113 mg/L 57 30-130 17 30
2,4,6-Tribromophenol (Surr)10 -130
Surrogate
129
LCSD LCSD
Qualifier Limits%Recovery
722-Fluorobiphenyl (Surr)10 -130
402-Fluorophenol (Surr)10 -130
124Terphenyl-d14 (Surr)13 -130
26Phenol-d5 (Surr)10 -130
69Nitrobenzene-d5 (Surr)11 -130
Eurofins TestAmerica, Savannah
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QC Sample Results
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: LB2 680-658593/7-I
Matrix: Solid Prep Type: TCLP
Analysis Batch: 659117 Prep Batch: 658991
RL MDL
1,4-Dichlorobenzene <0.016 0.050 0.016 mg/L 03/11/21 08:13 03/12/21 00:07 1
LB2 LB2
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.037 0.0370.25 mg/L 03/11/21 08:13 03/12/21 00:07 1Pyridine
<0.0080 0.00800.050 mg/L 03/11/21 08:13 03/12/21 00:07 1Hexachlorobenzene
<0.012 0.0120.050 mg/L 03/11/21 08:13 03/12/21 00:07 12,4-Dinitrotoluene
<0.018 0.0180.050 mg/L 03/11/21 08:13 03/12/21 00:07 1Hexachloroethane
<0.020 0.0200.050 mg/L 03/11/21 08:13 03/12/21 00:07 1Hexachlorobutadiene
<0.050 0.0500.25 mg/L 03/11/21 08:13 03/12/21 00:07 1Pentachlorophenol
<0.011 0.0110.050 mg/L 03/11/21 08:13 03/12/21 00:07 12,4,6-Trichlorophenol
<0.016 0.0160.050 mg/L 03/11/21 08:13 03/12/21 00:07 12,4,5-Trichlorophenol
<0.018 0.0180.050 mg/L 03/11/21 08:13 03/12/21 00:07 1Nitrobenzene
<0.0090 0.00900.050 mg/L 03/11/21 08:13 03/12/21 00:07 12-Methylphenol
<0.0070 0.00700.050 mg/L 03/11/21 08:13 03/12/21 00:07 13 & 4 Methylphenol
2,4,6-Tribromophenol (Surr)121 10-130 03/12/21 00:07 1
LB2 LB2
Surrogate
03/11/21 08:13
Dil FacPreparedAnalyzedQualifierLimits%Recovery
66 03/11/21 08:13 03/12/21 00:07 12-Fluorobiphenyl (Surr)10-130
33 03/11/21 08:13 03/12/21 00:07 12-Fluorophenol (Surr)10-130
121 03/11/21 08:13 03/12/21 00:07 1Terphenyl-d14 (Surr)13-130
24 03/11/21 08:13 03/12/21 00:07 1Phenol-d5 (Surr)10-130
65 03/11/21 08:13 03/12/21 00:07 1Nitrobenzene-d5 (Surr)11-130
Client Sample ID: 204 Bath Mill AreaLab Sample ID: 680-195839-1 MS
Matrix: Solid Prep Type: TCLP
Analysis Batch: 659266 Prep Batch: 658991
1,4-Dichlorobenzene <0.016 F2 *-1.00 0.478 mg/L 48 30-130
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Pyridine <0.037 F2 F1 2.00 0.739 mg/L 37 30-130
Hexachlorobenzene <0.0080 1.00 0.868 mg/L 87 30-130
2,4-Dinitrotoluene <0.012 1.00 0.898 mg/L 90 30-130
Hexachloroethane <0.018 F2 *-1.00 0.381 mg/L 38 30-130
Hexachlorobutadiene <0.020 F2 1.00 0.577 mg/L 58 30-130
Pentachlorophenol <0.050 2.00 1.45 mg/L 73 30-130
2,4,6-Trichlorophenol <0.011 1.00 0.855 mg/L 86 30-130
2,4,5-Trichlorophenol <0.016 1.00 0.814 mg/L 81 30-130
Nitrobenzene <0.018 1.00 0.822 mg/L 82 30-130
2-Methylphenol <0.0090 1.00 0.580 mg/L 58 30-130
3 & 4 Methylphenol <0.0070 1.00 0.577 mg/L 58 30-130
2,4,6-Tribromophenol (Surr)10 -130
Surrogate
109
MS MS
Qualifier Limits%Recovery
752-Fluorobiphenyl (Surr)10 -130
402-Fluorophenol (Surr)10 -130
104Terphenyl-d14 (Surr)13 -130
25Phenol-d5 (Surr)10 -130
66Nitrobenzene-d5 (Surr)11 -130
Eurofins TestAmerica, Savannah
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QC Sample Results
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: 204 Bath Mill AreaLab Sample ID: 680-195839-1 MSD
Matrix: Solid Prep Type: TCLP
Analysis Batch: 659266 Prep Batch: 658991
1,4-Dichlorobenzene <0.016 F2 *-1.00 0.690 F2 mg/L 69 30-130 36 30
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Pyridine <0.037 F2 F1 2.00 0.539 F2 F1 mg/L 27 30-130 31 30
Hexachlorobenzene <0.0080 1.00 1.10 mg/L 110 30-130 24 30
2,4-Dinitrotoluene <0.012 1.00 1.10 mg/L 110 30-130 21 30
Hexachloroethane <0.018 F2 *-1.00 0.612 F2 mg/L 61 30-130 47 30
Hexachlorobutadiene <0.020 F2 1.00 0.959 F2 mg/L 96 30-130 50 30
Pentachlorophenol <0.050 2.00 1.78 mg/L 89 30-130 20 30
2,4,6-Trichlorophenol <0.011 1.00 0.950 mg/L 95 30-130 10 30
2,4,5-Trichlorophenol <0.016 1.00 0.945 mg/L 95 30-130 15 30
Nitrobenzene <0.018 1.00 0.988 mg/L 99 30-130 18 30
2-Methylphenol <0.0090 1.00 0.644 mg/L 64 30-130 10 30
3 & 4 Methylphenol <0.0070 1.00 0.638 mg/L 64 30-130 10 30
2,4,6-Tribromophenol (Surr)10 -130
Surrogate
129
MSD MSD
Qualifier Limits%Recovery
872-Fluorobiphenyl (Surr)10 -130
462-Fluorophenol (Surr)10 -130
129Terphenyl-d14 (Surr)13 -130
29Phenol-d5 (Surr)10 -130
81Nitrobenzene-d5 (Surr)11 -130
Method: 300.0 - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 680-658433/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 658433
RL MDL
Fluoride <0.040 0.10 0.040 mg/L 03/08/21 10:35 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-658433/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 658433
Fluoride 2.00 2.11 mg/L 105 90-110
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-658433/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 658433
Fluoride 2.00 2.11 mg/L 105 90-110 0 15
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Eurofins TestAmerica, Savannah
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QC Sample Results
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
Method: 9056A - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 680-658768/1-A
Matrix: Solid Prep Type: Soluble
Analysis Batch: 658839
RL MDL
Fluoride <0.80 2.0 0.80 mg/Kg 03/10/21 15:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-658768/2-A
Matrix: Solid Prep Type: Soluble
Analysis Batch: 658839
Fluoride 20.1 20.3 mg/Kg 101 75-125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-658768/3-A
Matrix: Solid Prep Type: Soluble
Analysis Batch: 658839
Fluoride 20.1 20.4 mg/Kg 101 75-125 0 15
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 680-658490/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 658799 Prep Batch: 658490
RL MDL
Aluminum <24 200 24 ug/L 03/08/21 11:55 03/09/21 22:01 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-658490/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 658799 Prep Batch: 658490
Aluminum 5000 4640 ug/L 93 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Outfall 012Lab Sample ID: 680-195839-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 658799 Prep Batch: 658490
Aluminum 40 J 5000 4900 ug/L 97 75-125
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Outfall 012Lab Sample ID: 680-195839-2 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 658799 Prep Batch: 658490
Aluminum 40 J 5000 5060 ug/L 100 75-125 3 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Eurofins TestAmerica, Savannah
Page 17 of 30 3/15/2021
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QC Sample Results
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 680-658870/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 659034 Prep Batch: 658870
RL MDL
Arsenic <0.020 0.020 0.020 mg/L 03/10/21 11:10 03/10/21 19:08 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<0.10 0.100.10 mg/L 03/10/21 11:10 03/10/21 19:08 1Barium
<0.010 0.0100.010 mg/L 03/10/21 11:10 03/10/21 19:08 1Cadmium
<0.020 0.0200.020 mg/L 03/10/21 11:10 03/10/21 19:08 1Chromium
<0.020 0.0200.020 mg/L 03/10/21 11:10 03/10/21 19:08 1Lead
<0.050 0.0500.050 mg/L 03/10/21 11:10 03/10/21 19:08 1Selenium
<0.010 0.0100.010 mg/L 03/10/21 11:10 03/10/21 19:08 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-658870/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 659034 Prep Batch: 658870
Arsenic 2.00 1.97 mg/L 98 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Barium 2.00 1.95 mg/L 97 80-120
Cadmium 1.00 0.970 mg/L 97 80-120
Chromium 2.00 1.95 mg/L 98 80-120
Lead 9.08 8.58 mg/L 94 80-120
Selenium 2.00 2.04 mg/L 102 80-120
Silver 1.00 0.956 mg/L 96 80-120
Client Sample ID: Method BlankLab Sample ID: LB 680-658593/1-C
Matrix: Solid Prep Type: TCLP
Analysis Batch: 659034 Prep Batch: 658870
RL MDL
Arsenic <0.20 0.20 0.20 mg/L 03/10/21 11:10 03/10/21 19:27 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.0 1.01.0 mg/L 03/10/21 11:10 03/10/21 19:27 1Barium
<0.10 0.100.10 mg/L 03/10/21 11:10 03/10/21 19:27 1Cadmium
<0.20 0.200.20 mg/L 03/10/21 11:10 03/10/21 19:27 1Chromium
<0.20 0.200.20 mg/L 03/10/21 11:10 03/10/21 19:27 1Lead
<0.50 0.500.50 mg/L 03/10/21 11:10 03/10/21 19:27 1Selenium
<0.10 0.100.10 mg/L 03/10/21 11:10 03/10/21 19:27 1Silver
Client Sample ID: Method BlankLab Sample ID: LB2 680-658593/7-C
Matrix: Solid Prep Type: TCLP
Analysis Batch: 659034 Prep Batch: 658870
RL MDL
Arsenic <0.20 0.20 0.20 mg/L 03/10/21 11:10 03/10/21 20:24 1
LB2 LB2
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.0 1.01.0 mg/L 03/10/21 11:10 03/10/21 20:24 1Barium
<0.10 0.100.10 mg/L 03/10/21 11:10 03/10/21 20:24 1Cadmium
<0.20 0.200.20 mg/L 03/10/21 11:10 03/10/21 20:24 1Chromium
<0.20 0.200.20 mg/L 03/10/21 11:10 03/10/21 20:24 1Lead
<0.50 0.500.50 mg/L 03/10/21 11:10 03/10/21 20:24 1Selenium
<0.10 0.100.10 mg/L 03/10/21 11:10 03/10/21 20:24 1Silver
Eurofins TestAmerica, Savannah
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QC Sample Results
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 680-658875/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 658999 Prep Batch: 658875
RL MDL
Mercury <0.00020 0.00020 0.00020 mg/L 03/10/21 11:49 03/10/21 19:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-658875/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 658999 Prep Batch: 658875
Mercury 0.250 0.244 mg/L 98 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method BlankLab Sample ID: LB 680-658593/1-D
Matrix: Solid Prep Type: TCLP
Analysis Batch: 658999 Prep Batch: 658875
RL MDL
Mercury <0.020 0.020 0.020 mg/L 03/10/21 11:49 03/10/21 19:12 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Method BlankLab Sample ID: LB2 680-658593/7-D
Matrix: Solid Prep Type: TCLP
Analysis Batch: 658999 Prep Batch: 658875
RL MDL
Mercury <0.020 0.020 0.020 mg/L 03/10/21 11:49 03/10/21 19:40 1
LB2 LB2
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Method: 1030 - Ignitability, Solids
Client Sample ID: Method BlankLab Sample ID: MB 680-658481/1
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 658481
NONE NONE
Ignitability NB mm/sec 03/08/21 11:35 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-658481/2
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 658481
Ignitability 2.59 2.588 mm/sec 100 75-125
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-658481/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 658481
Ignitability 2.66 2.656 mm/sec 100 75-125 3 10
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Eurofins TestAmerica, Savannah
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QC Sample Results
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
Method: 2540 D-2011 - Total Suspended Solids (Dried at 103-105°C)
Client Sample ID: Method BlankLab Sample ID: MB 680-658741/1
Matrix: Water Prep Type: Total/NA
Analysis Batch: 658741
RL RL
Total Suspended Solids <2.5 2.5 2.5 mg/L 03/09/21 15:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-658741/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 658741
Total Suspended Solids 951 918 mg/L 97 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-658741/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 658741
Total Suspended Solids 951 954 mg/L 100 80-120 4 25
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Method: 9012B - Cyanide, Total andor Amenable
Client Sample ID: Method BlankLab Sample ID: MB 680-659116/1-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 659505 Prep Batch: 659504
RL MDL
Cyanide, Total <0.50 0.50 0.50 mg/Kg 03/14/21 15:29 03/14/21 16:34 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-659116/2-B
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 659505 Prep Batch: 659504
Cyanide, Total 1.00 0.991 mg/Kg 99 85-115
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: 204 Bath Mill AreaLab Sample ID: 680-195839-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 659505 Prep Batch: 659504
Cyanide, Total <0.63 1.25 1.26 mg/Kg 100 85-115☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: 204 Bath Mill AreaLab Sample ID: 680-195839-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 659505 Prep Batch: 659504
Cyanide, Total <0.63 1.25 1.26 mg/Kg 101 85-115 0 30☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Eurofins TestAmerica, Savannah
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QC Sample Results
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
Method: 9034 - Sulfide, Acid Soluble and Insoluble (Titrimetric)
Client Sample ID: Method BlankLab Sample ID: MB 680-658578/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 658602 Prep Batch: 658578
RL MDL
Sulfide <60 60 60 mg/Kg 03/09/21 08:01 03/09/21 09:43 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-658578/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 658602 Prep Batch: 658578
Sulfide 1250 1170 mg/Kg 93 50-150
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-658578/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 658602 Prep Batch: 658578
Sulfide 1250 1180 mg/Kg 95 50-150 1 50
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Client Sample ID: 204 Bath Mill AreaLab Sample ID: 680-195839-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 658602 Prep Batch: 658578
Sulfide 140 1550 1070 mg/Kg 60 50-150☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: 204 Bath Mill AreaLab Sample ID: 680-195839-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 658602 Prep Batch: 658578
Sulfide 140 1630 1160 mg/Kg 63 50-150 8 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: 204 Bath Mill AreaLab Sample ID: 680-195839-1 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 658602 Prep Batch: 658578
Sulfide 140 215 mg/Kg 43 50☼
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: 9045D - pH
Client Sample ID: Lab Control SampleLab Sample ID: LCS 680-658864/1
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 658864
pH 7.01 7.1 PH Units 101 79-126
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Eurofins TestAmerica, Savannah
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QC Association Summary
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
GC/MS VOA
Analysis Batch: 658413
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 624.1680-195839-2 Outfall 012 Total/NA
Water 624.1MB 680-658413/9 Method Blank Total/NA
Water 624.1LCS 680-658413/4 Lab Control Sample Total/NA
Water 624.1LCSD 680-658413/5 Lab Control Sample Dup Total/NA
Analysis Batch: 658417
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 624.1680-195839-3 Trip Blank Total/NA
Water 624.1MB 680-658417/10 Method Blank Total/NA
Water 624.1LCS 680-658417/5 Lab Control Sample Total/NA
Water 624.1LCSD 680-658417/6 Lab Control Sample Dup Total/NA
Leach Batch: 658454
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 1311680-195839-1 204 Bath Mill Area TCLP
Solid 1311LB 680-658454/1-A Method Blank TCLP
Analysis Batch: 658727
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260D 658454680-195839-1 204 Bath Mill Area TCLP
Solid 8260D 658454LB 680-658454/1-A Method Blank TCLP
Solid 8260DLCS 680-658727/7 Lab Control Sample Total/NA
GC/MS Semi VOA
Leach Batch: 658593
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 1311680-195839-1 204 Bath Mill Area TCLP
Solid 1311LB2 680-658593/7-I Method Blank TCLP
Solid 1311680-195839-1 MS 204 Bath Mill Area TCLP
Solid 1311680-195839-1 MSD 204 Bath Mill Area TCLP
Prep Batch: 658991
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3510C 658593680-195839-1 204 Bath Mill Area TCLP
Solid 3510C 658593LB2 680-658593/7-I Method Blank TCLP
Solid 3510CMB 680-658991/1-A Method Blank Total/NA
Solid 3510CLCS 680-658991/2-A Lab Control Sample Total/NA
Solid 3510CLCSD 680-658991/3-A Lab Control Sample Dup Total/NA
Solid 3510C 658593680-195839-1 MS 204 Bath Mill Area TCLP
Solid 3510C 658593680-195839-1 MSD 204 Bath Mill Area TCLP
Analysis Batch: 659117
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270E 658991LB2 680-658593/7-I Method Blank TCLP
Solid 8270E 658991MB 680-658991/1-A Method Blank Total/NA
Solid 8270E 658991LCS 680-658991/2-A Lab Control Sample Total/NA
Solid 8270E 658991LCSD 680-658991/3-A Lab Control Sample Dup Total/NA
Eurofins TestAmerica, Savannah
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QC Association Summary
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
GC/MS Semi VOA
Analysis Batch: 659266
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270E 658991680-195839-1 204 Bath Mill Area TCLP
Solid 8270E 658991680-195839-1 MS 204 Bath Mill Area TCLP
Solid 8270E 658991680-195839-1 MSD 204 Bath Mill Area TCLP
HPLC/IC
Analysis Batch: 658433
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 300.0680-195839-2 Outfall 012 Total/NA
Water 300.0MB 680-658433/2 Method Blank Total/NA
Water 300.0LCS 680-658433/3 Lab Control Sample Total/NA
Water 300.0LCSD 680-658433/4 Lab Control Sample Dup Total/NA
Leach Batch: 658768
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid DI Leach680-195839-1 204 Bath Mill Area Soluble
Solid DI LeachMB 680-658768/1-A Method Blank Soluble
Solid DI LeachLCS 680-658768/2-A Lab Control Sample Soluble
Solid DI LeachLCSD 680-658768/3-A Lab Control Sample Dup Soluble
Analysis Batch: 658839
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9056A 658768680-195839-1 204 Bath Mill Area Soluble
Solid 9056A 658768MB 680-658768/1-A Method Blank Soluble
Solid 9056A 658768LCS 680-658768/2-A Lab Control Sample Soluble
Solid 9056A 658768LCSD 680-658768/3-A Lab Control Sample Dup Soluble
Metals
Prep Batch: 658490
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A680-195839-2 Outfall 012 Total/NA
Water 3010AMB 680-658490/1-A Method Blank Total/NA
Water 3010ALCS 680-658490/2-A Lab Control Sample Total/NA
Water 3010A680-195839-2 MS Outfall 012 Total/NA
Water 3010A680-195839-2 MSD Outfall 012 Total/NA
Leach Batch: 658593
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 1311680-195839-1 204 Bath Mill Area TCLP
Solid 1311LB 680-658593/1-C Method Blank TCLP
Solid 1311LB 680-658593/1-D Method Blank TCLP
Solid 1311LB2 680-658593/7-C Method Blank TCLP
Solid 1311LB2 680-658593/7-D Method Blank TCLP
Analysis Batch: 658799
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6010D 658490680-195839-2 Outfall 012 Total/NA
Water 6010D 658490MB 680-658490/1-A Method Blank Total/NA
Water 6010D 658490LCS 680-658490/2-A Lab Control Sample Total/NA
Water 6010D 658490680-195839-2 MS Outfall 012 Total/NA
Water 6010D 658490680-195839-2 MSD Outfall 012 Total/NA
Eurofins TestAmerica, Savannah
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QC Association Summary
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
Metals
Prep Batch: 658870
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3010A 658593680-195839-1 204 Bath Mill Area TCLP
Solid 3010A 658593LB 680-658593/1-C Method Blank TCLP
Solid 3010A 658593LB2 680-658593/7-C Method Blank TCLP
Solid 3010AMB 680-658870/1-A Method Blank Total/NA
Solid 3010ALCS 680-658870/2-A Lab Control Sample Total/NA
Prep Batch: 658875
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7470A 658593680-195839-1 204 Bath Mill Area TCLP
Solid 7470A 658593LB 680-658593/1-D Method Blank TCLP
Solid 7470A 658593LB2 680-658593/7-D Method Blank TCLP
Solid 7470AMB 680-658875/1-A Method Blank Total/NA
Solid 7470ALCS 680-658875/2-A Lab Control Sample Total/NA
Analysis Batch: 658999
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7470A 658875680-195839-1 204 Bath Mill Area TCLP
Solid 7470A 658875LB 680-658593/1-D Method Blank TCLP
Solid 7470A 658875LB2 680-658593/7-D Method Blank TCLP
Solid 7470A 658875MB 680-658875/1-A Method Blank Total/NA
Solid 7470A 658875LCS 680-658875/2-A Lab Control Sample Total/NA
Analysis Batch: 659034
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010D 658870680-195839-1 204 Bath Mill Area TCLP
Solid 6010D 658870LB 680-658593/1-C Method Blank TCLP
Solid 6010D 658870LB2 680-658593/7-C Method Blank TCLP
Solid 6010D 658870MB 680-658870/1-A Method Blank Total/NA
Solid 6010D 658870LCS 680-658870/2-A Lab Control Sample Total/NA
General Chemistry
Analysis Batch: 658394
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture680-195839-1 204 Bath Mill Area Total/NA
Analysis Batch: 658481
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 1030680-195839-1 204 Bath Mill Area Total/NA
Solid 1030MB 680-658481/1 Method Blank Total/NA
Solid 1030LCS 680-658481/2 Lab Control Sample Total/NA
Solid 1030LCSD 680-658481/7 Lab Control Sample Dup Total/NA
Prep Batch: 658578
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9030B680-195839-1 204 Bath Mill Area Total/NA
Solid 9030BMB 680-658578/1-A Method Blank Total/NA
Solid 9030BLCS 680-658578/2-A Lab Control Sample Total/NA
Solid 9030BLCSD 680-658578/3-A Lab Control Sample Dup Total/NA
Solid 9030B680-195839-1 MS 204 Bath Mill Area Total/NA
Solid 9030B680-195839-1 MSD 204 Bath Mill Area Total/NA
Eurofins TestAmerica, Savannah
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QC Association Summary
Job ID: 680-195839-1Client: Civil & Environmental Consultants Inc
Project/Site: Alcoa - Badin, NC-Waste Characterization
General Chemistry (Continued)
Prep Batch: 658578 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9030B680-195839-1 DU 204 Bath Mill Area Total/NA
Analysis Batch: 658602
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9034 658578680-195839-1 204 Bath Mill Area Total/NA
Solid 9034 658578MB 680-658578/1-A Method Blank Total/NA
Solid 9034 658578LCS 680-658578/2-A Lab Control Sample Total/NA
Solid 9034 658578LCSD 680-658578/3-A Lab Control Sample Dup Total/NA
Solid 9034 658578680-195839-1 MS 204 Bath Mill Area Total/NA
Solid 9034 658578680-195839-1 MSD 204 Bath Mill Area Total/NA
Solid 9034 658578680-195839-1 DU 204 Bath Mill Area Total/NA
Analysis Batch: 658741
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 2540 D-2011680-195839-2 Outfall 012 Total/NA
Water 2540 D-2011MB 680-658741/1 Method Blank Total/NA
Water 2540 D-2011LCS 680-658741/2 Lab Control Sample Total/NA
Water 2540 D-2011LCSD 680-658741/3 Lab Control Sample Dup Total/NA
Analysis Batch: 658864
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9045D680-195839-1 204 Bath Mill Area Total/NA
Solid 9045DLCS 680-658864/1 Lab Control Sample Total/NA
Leach Batch: 659116
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9013680-195839-1 204 Bath Mill Area Total/NA
Solid 9013MB 680-659116/1-B Method Blank Total/NA
Solid 9013LCS 680-659116/2-B Lab Control Sample Total/NA
Solid 9013680-195839-1 MS 204 Bath Mill Area Total/NA
Solid 9013680-195839-1 MSD 204 Bath Mill Area Total/NA
Prep Batch: 659504
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9012B 659116680-195839-1 204 Bath Mill Area Total/NA
Solid 9012B 659116MB 680-659116/1-B Method Blank Total/NA
Solid 9012B 659116LCS 680-659116/2-B Lab Control Sample Total/NA
Solid 9012B 659116680-195839-1 MS 204 Bath Mill Area Total/NA
Solid 9012B 659116680-195839-1 MSD 204 Bath Mill Area Total/NA
Analysis Batch: 659505
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9012B 659504680-195839-1 204 Bath Mill Area Total/NA
Solid 9012B 659504MB 680-659116/1-B Method Blank Total/NA
Solid 9012B 659504LCS 680-659116/2-B Lab Control Sample Total/NA
Solid 9012B 659504680-195839-1 MS 204 Bath Mill Area Total/NA
Solid 9012B 659504680-195839-1 MSD 204 Bath Mill Area Total/NA
Eurofins TestAmerica, Savannah
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Lab Chronicle
Client: Civil & Environmental Consultants Inc Job ID: 680-195839-1
Project/Site: Alcoa - Badin, NC-Waste Characterization
Client Sample ID: 204 Bath Mill Area Lab Sample ID: 680-195839-1
Matrix: SolidDate Collected: 03/04/21 09:30
Date Received: 03/05/21 10:00
Leach 1311 JEB03/08/21 12:29 TAL SAV658454
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
TCLP 25.00 g 500 mL
Analysis 8260D 20 658727 03/10/21 07:25 EMA TAL SAVTCLP5 mL 5 mL
CMSP2Instrument ID:
Leach 1311 658593 03/09/21 12:34 JEB TAL SAVTCLP100.02 g 2000 mL
Prep 3510C 658991 03/11/21 08:13 TRA TAL SAVTCLP100 mL 1 mL
Analysis 8270E 1 659266 03/12/21 16:49 DBM TAL SAVTCLP
CMSNInstrument ID:
Leach 1311 658593 03/09/21 12:34 JEB TAL SAVTCLP100.02 g 2000 mL
Prep 3010A 658870 03/10/21 11:10 BCB TAL SAVTCLP5 mL 50 mL
Analysis 6010D 1 659034 03/10/21 20:33 BCB TAL SAVTCLP
ICPEInstrument ID:
Leach 1311 658593 03/09/21 12:34 JEB TAL SAVTCLP100.02 g 2000 mL
Prep 7470A 658875 03/10/21 11:49 JKL TAL SAVTCLP0.50 mL 50 mL
Analysis 7470A 1 658999 03/10/21 20:08 JKL TAL SAVTCLP
LEEMAN2Instrument ID:
Analysis 1030 1 658481 03/08/21 11:35 SM TAL SAVTotal/NA
SPC8Instrument ID:
Analysis 9045D 1 658864 03/10/21 10:59 SM TAL SAVTotal/NA 20.01 g 20 mL
GEpHM4Instrument ID:
Analysis Moisture 1 658394 03/08/21 06:52 JEB TAL SAVTotal/NA
NOEQUIPInstrument ID:
Client Sample ID: 204 Bath Mill Area Lab Sample ID: 680-195839-1
Matrix: SolidDate Collected: 03/04/21 09:30
Percent Solids: 79.8Date Received: 03/05/21 10:00
Leach DI Leach KMB03/09/21 16:56 TAL SAV658768
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Soluble 9.93 g 100 mL
Analysis 9056A 1 658839 03/10/21 15:49 UI TAL SAVSoluble5 mL 5 mL
CICHInstrument ID:
Leach 9013 659116 03/11/21 14:01 CMR TAL SAVTotal/NA 10.0 g 200 mL
Prep 9012B 659504 03/14/21 15:29 CMR TAL SAVTotal/NA 6 mL 6 mL
Analysis 9012B 1 659505 03/14/21 16:35 CMR TAL SAVTotal/NA
KONELAB4Instrument ID:
Prep 9030B 658578 03/09/21 08:01 NVF TAL SAVTotal/NA 1.02 g 6 mL
Analysis 9034 1 658602 03/09/21 09:43 NVF TAL SAVTotal/NA 6 mL 6 mL
NOEQUIPInstrument ID:
Client Sample ID: Outfall 012 Lab Sample ID: 680-195839-2
Matrix: WaterDate Collected: 03/02/21 10:30
Date Received: 03/05/21 10:00
Analysis 624.1 Y1S03/08/21 16:511 TAL SAV658413
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CMSB
Eurofins TestAmerica, Savannah
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Lab Chronicle
Client: Civil & Environmental Consultants Inc Job ID: 680-195839-1
Project/Site: Alcoa - Badin, NC-Waste Characterization
Client Sample ID: Outfall 012 Lab Sample ID: 680-195839-2
Matrix: WaterDate Collected: 03/02/21 10:30
Date Received: 03/05/21 10:00
Analysis 300.0 T1C03/08/21 17:221 TAL SAV658433
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3010A 658490 03/08/21 11:55 BJB TAL SAVTotal/NA 50 mL 50 mL
Analysis 6010D 1 658799 03/09/21 22:22 BWR TAL SAVTotal/NA
ICPEInstrument ID:
Analysis 2540 D-2011 1 658741 03/09/21 15:40 MS TAL SAVTotal/NA 750 mL 1000 mL
NOEQUIPInstrument ID:
Client Sample ID: Trip Blank Lab Sample ID: 680-195839-3
Matrix: WaterDate Collected: 03/02/21 00:00
Date Received: 03/05/21 10:00
Analysis 624.1 Y1S03/08/21 14:531 TAL SAV658417
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Instrument ID:CMSP2
Laboratory References:
TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins TestAmerica, Savannah
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Login Sample Receipt Checklist
Client: Civil & Environmental Consultants Inc Job Number: 680-195839-1
Login Number: 195839
Question Answer Comment
Creator: Chamberlain, Kim A
List Source: Eurofins TestAmerica, Savannah
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins TestAmerica, Savannah
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Accreditation/Certification Summary
Client: Civil & Environmental Consultants Inc Job ID: 680-195839-1
Project/Site: Alcoa - Badin, NC-Waste Characterization
Laboratory: Eurofins TestAmerica, Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)269State 12-31-21
Eurofins TestAmerica, Savannah
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Attachment 5
Waste Profile