2019.08.26_CCO.p12and11.1_CapeFearPFASLoadingReductionPlan

The Chemours Company
Fayetteville Works
22828 NC Highway 87 W
Fayetteville, NC 28306

August 26, 2019
Sheila Holman
Assistant Secretary for the Environment
1601 Mail Service Center
Raleigh, NC 27699-1601
[e-mail]

Kemp Burdette
Cape Fear River Watch
617 Surry Street
Wilmington, NC 28401
[phone]
[e-mail]

Re: Submission Pursuant to Consent Order Paragraphs 12 and 11.1
Dear Ms. Holman and Mr. Burdette,
Chemours is pleased to submit the enclosed Cape Fear River PFAS Loading Reduction
Plan, pursuant to paragraphs 12 and 11.1 of the Consent Order entered by the Superior Court for
Bladen County on February 25, 2019. The Reduction Plan and its attachments were developed
by our consultant, Geosyntec Consultants of NC, P.C. DEQ has approved Geosyntec as a third
party for this work under the Consent Order.

As we have previously reported, Chemours has already implemented several actions that
have significantly reduced PFAS loadings originating from Fayetteville Works to the Cape Fear
River. These actions have included, among others, the cessation of process wastewater
discharges, installation of new air emissions controls, lining of the cooling water channel and
sediment ponds, and groundwater extraction from three perched zone monitoring wells.

The enclosed Reduction Plan proposes the implementation of seven additional actions to
further reduce PFAS loadings to the River. Geosyntec has developed these recommended
actions, and Chemours has agreed their implementation will support reducing loading to the
River in accordance with Consent Order paragraph 12. The seven proposed actions are:

1. Capture and Treat Old Outfall 002 Water
2. Capture and Treat Groundwater from Seeps
3. Targeted Sediment Removal from Conveyance Network
4. Develop a Stormwater Pollution Prevention Plan
5. Targeted Stormwater Source Control and/or Treatment
6. Decommission and Replace Remaining Portion of the Terracotta Pipe
7. Assess Potential for Groundwater Intrusion into Conveyance Network

2

The seven actions proposed in the enclosed Reduction Plan are supported by recent
environmental characterization work and data analyses presented in four separate reports
attached to the Reduction Plan. These attached reports are the 1) PFAS Mass Loading Model, 2)
Seeps and Creeks Investigation Report, 3) Outfall 002 Assessment, and 4) Terracotta Pipe
Grouting Report. The PFAS Mass Loading Model report includes the characterization of PFAS
in downstream raw water intakes, pursuant to paragraph 11.1 of the Consent Order.

We would also like to emphasize that our environmental data collection, characterization,
and assessment efforts remain ongoing. Pursuant to paragraph 16 of the Consent Order,
Chemours will be submitting before the end of this year a Corrective Action Plan, and in that
Plan Chemours anticipates that it will propose additional actions to further reduce PFAS mass
loading from Fayetteville Works to the Cape Fear River based on the outcome of our ongoing
efforts.

***

As specified in the Consent Order, Chemours is simultaneously transmitting this
submission to downstream public water utilities. We look forward to meeting with DEQ and
Cape Fear River Watch soon to discuss this submission and the path forward for implementation.

Sincerely,

Brian D. Long
Plant Manager
Chemours – Fayetteville Works

Enclosure
Cape Fear River PFAS Loading Reduction Plan and Attachments

3
Cc:
William F. Lane, DEQ
Francisco Benzoni, NC DOJ
Michael Abraczinskas, DAQ
Michael Scott, DWM
Linda Culpepper, DWR
David C. Shelton, Chemours
John F. Savarese, WLRK
Geoff Gisler, SELC
Downstream Public Water Utilities

CAPE FEAR RIVER PFAS LOADING
REDUCTION PLAN
Chemours Fayetteville Works, NC
Prepared for
The Chemours Company FC, LLC 22828 NC Highway 87
Fayetteville, NC 28306

Prepared by
Geosyntec Consultants of NC, P.C.
2501 Blue Ridge Road, Suite 430
Raleigh, NC 27607
Geosyntec Project Number TR0795

August 26, 2019

Reduction Plan ii August 26, 2019
TABLE OF CONTENTS
EXECUTIVE SUMMARY .............................................................................................. v
1 INTRODUCTION ................................................................................................ 1
2 SITE SETTING AND PFAS MASS LOADING MODEL ASSESSMENT ....... 3
2.1 Site Setting ................................................................................................... 3
2.2 PFAS at the Site ........................................................................................... 9
2.3 PFAS Mass Loading Model ...................................................................... 10
2.4 Modeled Estimates of Downstream HFPO-DA Concentrations ............... 14
3 COMPLETED REDUCTION ACTIONS .......................................................... 16
4 CONSENT ORDER PARAGRAPH 12 PROPOSED ACTIONS ..................... 18
4.1 Overview of Proposed Actions .................................................................. 18
4.2 Planned and In-Progress Additional Assessment Activities ...................... 19
4.3 Detailed Descriptions of Proposed Actions ............................................... 21
Action 1: Capture and Treat Old Outfall 002 Water ................................ 21
Action 2: Capture and Treat Seeps ........................................................... 21
Action 3: Targeted Sediment Removal from Conveyance Network ........ 22
Action 4: Develop and Implement a Stormwater Pollution Prevention Plan
(SWPPP) ................................................................................................... 23
Action 5: Implement Targeted Stormwater Source Control and/or
Treatment .................................................................................................. 24
Action 6: Decommission and Replace Remaining Portion of the
Terracotta Pipe .......................................................................................... 25
Action 7: Assess Potential for Groundwater Intrusion into Conveyance
Network .................................................................................................... 25
5 PARAGRAPH 12(D) OUTFALL 002 ............................................................... 28
6 SUMMARY ........................................................................................................ 32
7 REFERENCES ................................................................................................... 33

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LIST OF TABLES
Table 1: Mass Loading Model Total Table 3+ PFAS including HFPO-DA Contributions
per Pathway .................................................................................................................... 13
Table 5: Proposed Paragraph 12 PFAS Loading Reduction Actions ............................. 18
Table 6: Potential Outfall 002 Control Approaches ....................................................... 29
Table 7: Estimated Outfall 002 HFPO-DA Reductions by Conveyance Network Flow
Component ...................................................................................................................... 30

LIST OF FIGURES
Figure 1: Cape Fear River Watershed and Downstream Intakes ...................................... 4
Figure 2: Site Location ..................................................................................................... 5
Figure 3: Site Conveyance Network ................................................................................. 6
Figure 4: Site Geology Cross-Section adapted from Parsons, 2018. ................................ 8
Figure 5: PFAS Transport Pathways Conceptual Diagram (not to scale) ...................... 12
Figure 6: Modeled and Measured HFPO-DA Concentration Time Series at Kings Bluff
Intake Canal. ................................................................................................................... 15
Figure 7: Lower and Best Estimates of HFPO-DA Load Reductions in Outfall 002
Compared to 2018 Loads. ............................................................................................... 31

LIST OF ATTACHMENTS

ATTACHMENT 1: Cape Fear River PFAS Mass Loading Model Assessment and Paragraph 11.1 Characterization of PFAS at Intakes.
ATTACHMENT 2: Seeps and Creeks Investigation Report
ATTACHMENT 3: Assessment of HFPO-DA and PFMOAA in Outfall 002
Discharge and Evaluation of Potential Control Options
ATTACHMENT 4: Decommissioning Summary of Grouting of East-West Section of Terracotta Pipe from Chemours Monomers IXM Area
ATTACHMENT 5: HFPO-DA Loading Reductions Estimate

Reduction Plan iv August 26, 2019
ACRONYMS AND ABBREVIATIONS % Percent
CAP Corrective Action Plan
CFRW Cape Fear River Watch
cfs Cubic Feet Per Second
DFSA Difluoro-sulfo-acetic acid
EPA United States Environmental Protection Agency
EPA RTC NC EPA Research Triangle Park North Carolina
ft feet
ft bgs feet below ground surface
HDPE high density polypropylene
HFPO Hexafluoropropylene Oxide
HFPO-DA Hexafluoropropylene Oxide Dimer Acid
HP/EC hydraulic profiling and electrical conductivity
L/s liters per second
lbs/yr pounds per year
mg/s milligrams per second
MMF Difluoromalonic acid
MSL Mean Sea Level
MTP Perfluoro-2-methoxypropanoic acid
NCDEQ North Carolina Department of Environmental Quality
ng/L nanograms per liter
NCCW Non Contact Cooling Water
NVHOS Perfluoroethoxysulfonic acid
PFAS per- and polyfluoroalkyl substances
PFMOAA perfluoro-1-methoxyacetic acid
PMPA Perfluoromethoxypropyl carboxylic acid
PPA Area Polymer Processing Acid Area
PPF Acid Perfluoropropionic acid
SWPPP Stormwater Pollution Prevention Plan
TA TestAmerica Laboratories, Inc.
WWTP Wastewater treatment plant

Reduction Plan v August 26, 2019
EXECUTIVE SUMMARY
Geosyntec Consultants of NC, P.C.(Geosyntec) has prepared this Cape Fear River PFAS
Reduction Plan (Reduction Plan) for The Chemours Company FC, LLC (Chemours)
pursuant to Paragraph 12 of the Consent Order among Chemours, the North Carolina
Department of Environmental Quality (NCDEQ) and Cape Fear River Watch (CFRW).
Geosyntec has developed the proposed recommended actions detailed in this plan and
Chemours anticipates that following NCDEQ and CFRW review, the parties will come
to an agreement to amend the Consent Order to incorporate the proposed recommended
actions.
This Reduction Plan proposes Chemours implement seven actions, listed in the table
below within five years of Consent Order Amendment, to reduce mass loading of PFAS
originating from the Chemours Fayetteville Works Facility (the Site). Four of these
actions would be implemented within two years of Consent Order Amendment and three
of the actions would be implemented within five years of Consent Order Amendment
(assuming all necessary permits and authorizations are provided in a timely manner). The
actions proposed here also support the requirements of Consent Order Paragraph 16
pursuant to which Chemours will submit a Corrective Action Plan for Groundwater by
December 31, 2019. As part of the Corrective Action Plan submittal, Chemours
anticipates that it will propose additional actions to reduce PFAS mass loading to the
Cape Fear River based on the outcome of environmental characterization efforts and
quantitative analyses presently on-going in support of the Corrective Action Plan
preparation.

Proposed Actions to Reduce PFAS Loading to Cape Fear River Approximate Years to Implement
1) Capture and Treat Old Outfall 002 Water 2
2) Capture and Treat Groundwater from Seeps 5
3) Targeted Sediment Removal from Conveyance Network 1
4) Develop a Stormwater Pollution Prevention Plan (SWPPP) 1
5) Targeted Stormwater Source Control and/or Treatment 4
6) Decommission and Replace Remaining Portion of the Terracotta Pipe 2
7) Assess Potential for Groundwater Intrusion into Conveyance Network 5

Reduction Plan 1 August 26, 2019
1 INTRODUCTION
Geosyntec has prepared this per- and polyfluoroalkyl substances (PFAS) reduction plan
(Reduction Plan) pursuant to Paragraph 12 of the February 25, 2019 Consent Order
among Chemours, the North Carolina Department of Environmental Quality (NCDEQ)
and Cape Fear River Watch (CFRW). To date Chemours has already implemented a
number of actions which have reduced PFAS loading originating from the Chemours
Fayetteville Works Site (the Site). Specifically, Hexafluoropropylene Oxide Dimer Acid
(HFPO-DA) load has been reduced by over 95% downstream in the Cape Fear River as
described later in Section 3. This Reduction Plan proposes seven additional actions to
further reduce the remaining HFPO-DA and PFAS loadings to the Cape Fear River.
Geosyntec has developed these recommended actions and Chemours has agreed their
implementation will support reducing loading to the Cape Fear River in accordance with
Consent Order Paragraph 12. Four of the actions proposed in the Reduction Plan would
be completed within two years of Consent Order Amendment and three of the actions
would be completed within five years of Consent Order Amendment (assuming all
necessary permits and authorizations are timely provided). Taken together these actions
are estimated to reduce PFAS loading in the Cape Fear River of Table 3+ compounds,
the compounds identified at the Site, by greater than 50% from present loading (based on
mass loading results).
In addition to Old Outfall 002 and the Seeps, onsite groundwater discharge contributes
relatively more mass to the Cape Fear River than the remaining other pathways. At this
time, assessment of onsite groundwater discharge is ongoing. The results of this ongoing
assessment will be presented in the Consent Order paragraph 18 assessment report due
September 30, 2019. Onsite groundwater will also be addressed in the Consent Order
paragraph 16 Corrective Action Plan due December 31, 2019.
The actions proposed in this Reduction Plan are supported by recent environmental
characterization work and data analyses presented in four separate reports attached to this
Reduction Plan. These reports are:
• “PFAS Mass Loading Model” – Cape Fear River PFAS Mass Loading Model
Assessment and Paragraph 11.1 Characterization of PFAS at Intakes
(Attachment 1): This report identifies transport pathways that contribute
measurable PFAS load to the Cape Fear River by estimating total PFAS mass
loading originating from the facility to the Cape Fear River and comparing
these estimates to empirically measured PFAS loading in the Cape Fear River.
The results of the modeling analysis are used in this Reduction Plan to support

Reduction Plan 2 August 26, 2019
the selection actions proposed. The PFAS Mass Loading Model Report also
presents a Characterization of PFAS at downstream raw water intakes
pursuant to Paragraph 11.1 of the Consent Order.
• Seeps and Creeks Investigation Report (Attachment 2): This document
presents a summary of recent environmental characterization work and data
that are used in the PFAS Mass Loading Model.
• “Outfall 002 Assessment” – Assessment of HFPO-DA and PFMOAA in
Outfall 002 Discharge and Evaluation of Potential Control Options
(Attachment 3): This document presents data and a technical analysis related
to Outfall 002 to support actions proposed in this Reduction Plan, along with
an evaluation of potential reductions of HFPO-DA and perfluoro-1-
methoxyacetic acid (PFMOAA) from eight potential control approaches (nine
including in-progress air emissions reductions).
• “Terracotta Pipe Grouting Report” – Decommissioning Summary of Grouting
of East-West Section of Terracotta Pipe from Chemours Monomers IXM Area
(Attachment 4): This document summarizes the recent work completed at the
Site to decommission a portion of the terracotta pipe.
• HFPO-DA Loading Reductions Estimate (Attachment 5): This document
presents an assessment of HFPO-DA loading reductions since June 2017 at
Outfall 002, to the Cape Fear River and to the environment.
The remainder of this report is organized as follows:
• Section 2: Site Setting and PFAS Mass Loading Model Assessment – This
section presents an overview description of the facility, environmental setting,
PFAS mass loading pathways to the Cape Fear River and results of the PFAS
Mass Loading Model.
• Section 3: Completed Reduction Actions – This section lists actions
Chemours has already undertaken to reduce PFAS loading the environment
and the Cape Fear River.
• Section 4: Consent Order Paragraph 12 Proposed Actions – This section
lists the proposed actions, including interim benchmarks, to reduce PFAS
loading originating from the facility and reaching the Cape Fear River.
• Section 5: Paragraph 12(d) Outfall 002 – Pursuant to Consent Order
Paragraph 12(d) this section evaluates whether an 80% reduction in HFPO-
DA and (PFMOAA) in Outfall 002 is technologically and/or economically
feasible within 2 years of Consent Order Amendment.

Reduction Plan 3 August 26, 2019
• Section 6: Summary – This section summarizes the Reduction Plan actions
presented in this document.
• Section 7: References – This section lists documents referenced.
2 SITE SETTING AND PFAS MASS LOADING MODEL ASSESSMENT
This section presents an overview description of the Site Setting and reviews the
distribution of Site Associated PFAS and the Mass Loading Model results.
2.1 Site Setting
The Site is located on the Cape Fear River 7-miles upstream of the Bladen Bluffs water
intake and 55-miles upstream of the Kings Bluff Intake Canal as shown on Figure 1. The
Site is situated in the northwestern portion of Bladen County and southern portion of
Cumberland county about 20 miles from the Fayetteville, NC city center. There are
several operating areas at the site as shown in Figure 2. Chemours operates two
manufacturing areas on the Site, the Chemours Monomers IXM Area and the Polymer
Processing Aid Area (PPA Area). Chemours also operates the wastewater treatment plant
(WWTP) and Power Area; filtered water and demineralized water are produced in the
Power Area. Two tenants also operate on the Site; Kuraray America Inc. (Kuraray) and
E.I. du Pont de Nemours and Company (DuPont).
The land surface is relatively flat in the manufacturing areas of the Site and slopes down
a bluff with about a 100-foot change in elevation towards the Cape Fear River on the east
side of the Site. To the north of the Site, the property slopes towards Willis Creek, which
is a tributary that discharges to the Cape Fear River. To the south of the manufacturing
area is the Old Outfall Channel, which also discharges to the Cape Fear River. Farther
south, off the Site, is Georgia Branch Creek which is a tributary to the Cape Fear River.
River water used at the Site as non-contact cooling water (NCCW) is transmitted through
the Site Conveyance Network to Outfall 002 through a series of channels and piping
sections shown in Figure 3. The Site Conveyance Network also transmits stormwater and
treated process water from the Waste Water Treatment Plant. There are five sections of
the Site Conveyance Network identified in Figure 3:
• The Wood Lined Trench which transmits NCCW from Kuraray operations and
stormwater from the western portion of the Site;
• The Cooling Water Channel which transmits NCCW from the Chemours
Monomers IXM Area and stormwater from the northeast portion of the Site;

Reduction Plan 4 August 26, 2019
• The Wastewater Treatment Plant Discharge which transmits treated sanitary,
some NCCW, Kuraray and DuPont process waters, and some stormwater;
• The DuPont Area Ditches which transmit NCCW for DuPont operations and
stormwater from the southeast portion of the Site; and
• The Open Channel to Outfall 002 which transmits the combined flows from the
previous sections to Outfall 002 with some additional stormwater additions.

Figure 1: Cape Fear River Watershed and Downstream Intakes

Reduction Plan 5 August 26, 2019

Figure 2: Site Location

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Figure 3: Site Conveyance Network
Site Geology
As described by Parsons (2018), Bladen County is within the Coastal Plain Physiographic
Province, which consists of a seaward thickening wedge of sedimentary deposits ranging
in age from Cretaceous to Recent. Paleozoic metamorphic and igneous rocks underlie
these deposits. The Site is underlain by the Black Creek Formation, which is characterized
by lignitic clay with thin beds and laminae of fine-grained micaceous sand as well as thick
lenses of cross-bedded sand. The upper portion of the formation may also contain
glauconitic, fossiliferous clayey sand lenses. The Black Creek Formation and surficial
deposits are the principal potable water aquifers in the region.
Based on the lithology logged during onsite investigations, the Site is underlain by a fine-
to medium-grained sand unit with thin discontinuous interbedded silt/clay lenses. The

Reduction Plan 7 August 26, 2019
sand extends to a depth of approximately 65 feet below ground surface (ft bgs) (elevation
of +80 feet MSL). The saturated portion of this unit has been identified as the Surficial
Aquifer. Beneath this unit is a 7- to 15-foot-thick, laterally-continuous dense clay that has
been identified as the Black Creek Confining Unit.
The elevation of this unit (approximately +65 to +77 ft MSL) indicates that it, too, should
outcrop along the bluff face adjacent to the Cape Fear River, and potentially along the
embankment near Willis Creek. Beneath this confining unit is the Black Creek Aquifer,
which is approximately 8 to 20 ft thick and is encountered at depth between 80 and 100
ft bgs (elevation of approximately +45 to +65 ft MSL) at the top of the bluff. Beneath this
aquifer is a massive dense clay (with minor sand stringers) that has been identified as the
Upper Cape Fear Confining Unit. This unit was not fully penetrated at the Site; however,
it extended to at least 200 ft bgs (elevation of -55 ft MSL).
Beneath the manufacturing area, the uppermost sand unit is locally bisected by an aerially
extensive stiff clay lens. This clay lens is limited in lateral extent to the east, north and
south by local topography and pinches out (terminates) to the west of the manufacturing
area. The depth to the top of the clay lens is approximately 15 to 18 ft bgs. The clay lens
becomes thinner moving west across the manufacturing area and ranges from
approximately one foot to approximately 19 feet (ft) thick.
Site Hydrogeology
The hydrogeology of the Site includes a perched water zone and two aquifers; the Perched
Zone, the Surficial Aquifer and the Black Creek Aquifer as shown in Figure 4. The
Perched Zone is aerially limited and generally is located above the top of a discontinuous
clay layer present in the manufacturing area. Based on recent investigations and on-going
evaluations, the Perched Zone may have been influenced by seepage of water through the
previously unlined sedimentation basins and infiltration of non-contact cooling water
from previously unlined drainage ditches. In 2018, the sedimentation basins and Cooling
Water Channel were lined. Where perched water is present, it is encountered from
between 6 to 20 ft bgs. The lateral extent of the Perched Zone is controlled by topography
and the lateral extent of the clay lens.
The Surficial and Black Creek Aquifers are mostly separated by the Black Creek
confining unit, a clay layer. This clay layer is not fully confining as geological and
geochemical data indicate water and PFAS transfer has occurred from the Surficial
Aquifer to the Black Creek Aquifer. The Black Creek Aquifer is the uppermost identified
regional hydrogeologic unit. Flow in the Black Creek Aquifer is toward the Cape Fear
River. The Cape Fear River stage is also lower than the base of the Black Creek Aquifer,
indicating that the Cape Fear River is also a discharge boundary for the Black Creek
Aquifer.

Reduction Plan 8 August 26, 2019
Below the Black Creek Aquifer is the Upper Cape Fear Confining Unit. This clay is over
30-ft thick and is an aquitard to potential further downward flow based on limited onsite
geological borings and USGS groundwater wells at the Site that demonstrate minimal
hydraulic connection between the Black Creek Aquifer and the Upper Cape Fear Aquifer.

Figure 4: Site Geology Cross-Section adapted from Parsons, 2018.
The Surficial Aquifer is a shallow unconfined aquifer encountered at approximately 50 ft
bgs. Groundwater elevations range from approximately 100 to 107 ft above MSL in the
western areas of the Site to approximately 93 ft above MSL in the eastern areas of the
Site, indicating that groundwater flow is generally toward the Cape Fear River. The Cape
Fear River stage is typically near +30 ft MSL, which is lower than the base elevation of
the Surficial Aquifer, indicating that the Cape Fear River is a discharge boundary for the
Surficial Aquifer. Based on groundwater elevations near Willis Creek, portions of the
creek are “gaining” (groundwater discharges to the creek) and portions are “losing”
(surface water infiltrates to the underlying groundwater). Georgia Branch Creek also
appears to be a gaining stream near where State Road 1303 crosses Highway 87.
The Surficial and Black Creek Aquifers are mostly separated by the Black Creek
confining unit, a clay layer. This clay layer is not fully confining as geological and

Reduction Plan 9 August 26, 2019
geochemical data indicate water and PFAS transfer has occurred from the Surficial
Aquifer to the Black Creek Aquifer. The Black Creek Aquifer is the uppermost identified
regional hydrogeologic unit. Flow in the Black Creek Aquifer is toward the Cape Fear
River. The Cape Fear River stage is also lower than the base of the Black Creek Aquifer,
indicating that the Cape Fear River is also a discharge boundary for the Black Creek
Aquifer.
Below the Black Creek Aquifer is the Upper Cape Fear Confining Unit. This clay is over
34-ft thick and is an aquitard to potential further downward flow based on limited onsite
geological borings and USGS groundwater wells at the Site that demonstrate minimal
hydraulic connection between the Black Creek Aquifer and the Upper Cape Fear Aquifer.
Groundwater in the Perched Zone, and the Surficial and Black Creek Aquifers at Site
flow towards the bluff. As groundwater reaches the bluff above the Cape Fear River, it is
expressed at ground surface as seeps. The confluence of the “seeps” create four
channelized flows of expressed groundwater towards the river, designated as Seeps A, B,
C, and D.
The Cape Fear River
The Site is located adjacent to the west bank of the Cape Fear River and draws water for
use at the Site, with more than 95% of the water used as non-contact cooling water and
then returned to the river. The Cape Fear River is also a water source for downstream
communities served by raw water intakes located at Bladen Bluffs and Kings Bluff Intake
Canal, located approximately 5 miles and 55 miles downstream. Drinking water sourced
from the Cape Fear River contains certain chemicals from several sources including 1,4-
dioxane, trihalomethanes associated with bromide content in raw river water,
pharmaceuticals, personal care products, endocrine disrupting chemicals, and PFAS. A
brief description of these chemicals and their presence in the Cape Fear River was
reported previously (Geosyntec, 2018).

2.2 PFAS at the Site
PFAS is a term used for a group of man-made carbon-based chemicals composed of a
fully or partially fluorinated chain of carbon atoms (referred to as a “tail”) at one end of
the carbon chain and a nonfluorinated, polar functional group (referred to as a “head”) at
the other end. Recent estimates (Wang et. al., 2017) suggest over 3,000 PFAS are or have
been produced across various industries and for various applications. Chemours
manufactures per- and polyfluoroalkyl ether compounds and polymers at the Site. The
PFAS originating from the Chemours Fayetteville Works Site are characterized primarily
by the presence of ether bonds, i.e. two carbons connected by an oxygen atom. To date

Reduction Plan 10 August 26, 2019
twenty-four (24) PFAS compounds that are present in Site process water have been
identified and had reference standards produced (Geosyntec, 2019a). Of these twenty-
four (24) compounds, analytical methods exist for twenty (20), the Table 3+ SOP method,
with methods presently being developed for the remaining four (4) compounds [Difluoro-
sulfo-acetic acid (DFSA), Difluoromalonic acid (MMF), Perfluoro-2-methoxypropanoic
acid (MTP) and Perfluoropropionic acid (PPF Acid)]. PFAS from other sources are also
present in the Cape Fear River (Geosyntec, 2018).
The current grouping of Table 3+ PFAS, including HFPO-DA which can also be analyzed
by other methods, is used to represent PFAS loads originating from the facility. In site
groundwater and process water Table 3+ PFAS constitute over 99% of the quantitated
PFAS mass (Attachment 1 and 2).
PFAS associated with the Site have been released through a range of pathways, including:
(i) to air via air emissions, (ii) to surface water via Outfall 002, and (iii) to soil and
groundwater from piping that has either been replaced or will be replaced as described
later in this Reduction Plan. These PFAS releases have resulted in PFAS being detected
in environmental media both onsite and offsite. Geosyntec developed a mass loading
model (Attachment 1) pursuant to Consent Order Paragraph 12 that assesses relative
PFAS loading contributions from nine different transport pathways.

2.3 PFAS Mass Loading Model

The PFAS Mass Loading Model assesses the contribution of different transport pathways
to overall mass loading of PFAS originating from the facility to the Cape Fear River.
Pathways contributing to loading are shown in Figure 5 and listed below as follows:
Transport Pathway 1: Upstream Cape Fear River and Groundwater – pathway is
comprised of contributions from non-Chemours related
PFAS sources on the Cape Fear River and tributaries
upstream of the Site, and upstream offsite groundwater
with Table 3+ compounds present from aerial deposition
Transport Pathway 2: Willis Creek – Groundwater and stormwater discharge and
aerial deposition to Willis Creek and then to the Cape Fear
River
Transport Pathway 3: Direct aerial deposition of PFAS on the Cape Fear River;

Reduction Plan 11 August 26, 2019
Transport Pathway 4: Outfall 002 – Comprised of (i) water drawn from the Cape
Fear River and used as non-contact cooling water, (ii)
treated non-Chemours process water and (iii) Site
stormwater which are then discharged through Outfall 002;
Transport Pathway 5: Onsite Groundwater – Direct upwelling of site
groundwater to Cape Fear River from Black Creek
Aquifer;
Transport Pathway 6: Seeps – Groundwater Seeps (currently identified seeps are
A, B, C and D) above the Cape Fear River water level on
the bluff face from the facility that discharge into the Cape
Fear River;
Transport Pathway 7: Old Outfall 002 – Groundwater discharge to Old Outfall
002 and stormwater runoff flows into the Cape Fear River;
Transport Pathway 8: Adjacent and Downstream Groundwater – Offsite
groundwater adjacent and downstream of the Site
upwelling to the Cape Fear River; and,
Transport Pathway 9: Georgia Branch Creek – Groundwater, stormwater
discharge and aerial deposition to Georgia Branch Creek
and then to the Cape Fear River.
The PFAS Mass Loading Model Report (Attachment 1) estimated PFAS loading to the
Cape Fear River using a combination of measured and estimated data to develop mass
loading estimates by pathway. The recent investigations of the seeps and creeks at the
Site (Attachment 2) are the basis for much of the measured data used in the mass loading
model. The inputs used in the model (e.g. groundwater concentrations, seep flow rates,
river flow rates, etc.,) are described in the PFAS Mass Loading Model Report
(Attachment 1). The model was then calibrated and evaluated against observed
downstream river PFAS mass loadings. The best calibrated version of the model was used
to assign loadings coming for each of the nine transport pathways to the observed
concentrations in the Cape Fear River. The model was calibrated using the sum of Table
3+ PFAS loadings. The sum of Table 3+ compounds was selected as the calibration
parameter as the Table 3+ compounds represent greater than 99% of the PFAS mass
quantitated in Site groundwater, seeps and the Old Outfall 002.

Reduction Plan 12 August 26, 2019

Figure 5: PFAS Transport Pathways Conceptual Diagram (not to scale)

The mass loading model estimated that the Old Outfall 002 and Seeps (Transport
Pathways 7 and 6 respectively) have the highest contribution of Table 3+ PFAS mass
loading to the Cape Fear River. As described in the mass loading model report
(Attachment 1), these estimates are based on two mass loading characterization events
(May and June 2019). These two pathways (Transport Pathways 7 and 6) combined are
estimated to contribute greater than 50% of the loading to the Cape Fear River. Onsite
groundwater is the next highest mass loading pathway to the Cape Fear River with
estimated loadings between 17% to 22%.

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Table 1: Mass Loading Model Total Table 3+ PFAS including HFPO-DA Contributions per Pathway
Pathway
Total Table 3+ Estimated Loading Percentage per Pathway per Event May 2019 Event June 2019 Event [1] Upstream River Water and Groundwater 4% 15%
[2] Willis Creek 10% 4%
[3] Aerial Deposition on the River < 2% < 2%
[4] Outfall 002 4% 7%
[5] Onsite Groundwater 22% 17%
[6] Seeps 32% 24%
[7] Old Outfall 002 23% 29%
[8] Offsite Adjacent and Downstream Groundwater < 2% < 2%
[9] Georgia Branch Creek 4% 3%

For all Transport Pathways, the loading estimates will vary over time due to a range of
potential factors, including but not limited to:
• Detections of PFAS at or near analytical practical quantitation limits have more
variability;
• Elevated method reporting limits;
• Standard uncertainty (often ± 20%) in analytical laboratory results;
• Flow rate estimates in the river, seeps, groundwater and creeks are over- or under-
predicted compared to actual flow rates.
Transport Pathway 1 (upstream river water and groundwater) may have additional
variability due to the presence of three Table 3+ compounds, Byproduct 4, Byproduct 5
and (NVHOS), whose upstream load is not consistent with identified release pathways
from the Site (Attachment 2). Analytical results from Byproduct 4 and 5 also had a
consistent high bias based on data quality evaluations. These three compounds were
detected in both the May and June events at locations upstream where no other Table 3+
compounds were detected, including PMPA, which has the highest offsite concentrations
in the immediate area surrounding the Site. In upcoming quarterly sampling events,
Chemours will collect Cape Fear River samples at these same upstream locations and
additional locations to assess the spatial and temporal trends of these three compounds in
the upstream Cape Fear River.
Last, future events taken during, or immediately after, larger storm events may result in
pathways with stormwater components potentially having higher mass loadings, i.e.
variability, potentially from stormwater runoff.

Reduction Plan 14 August 26, 2019

2.4 Modeled Estimates of Downstream HFPO-DA Concentrations
The mass loading model simulates concentrations of PFAS originating from the Site at
downstream intakes over time as shown in Figure 66 for Kings Bluff Intake Canal. This
plot shows the measured concentrations of HFPO-DA from samples collected at Kings
Bluff Intake Canal compared to modeled concentrations estimated from the mass loading
model. To simulate the modeled time series, the model incorporated the twice weekly
Outfall 002 sample concentration results, measured Outfall 002 flow rates and Cape Fear
River flow volumes; all other loading parameters developed for the model as presented
in the PFAS Mass Loading Model Report were kept constant. As Figure 6 results show
modeled HFPO-DA results correspond to measured data. This suggests that the model is
also a useful predictive tool to understand the benefit of potential PFAS mass loading
reductions to river loads and concentrations.

Reduction Plan 15 August 26, 2019

Figure 6: Modeled and Measured HFPO-DA Concentration Time Series at Kings Bluff Intake Canal. Modeled HFPO-DA concentrations are calculated based on calculated and estimated mass loadings from off-Site and onsite groundwater, nearby tributaries, Outfall 002, and Old Outfall 002.

Reduction Plan 16 August 26, 2019
3 COMPLETED REDUCTION ACTIONS
Actions already implemented by Chemours have reduced yearly HFPO-DA mass
loadings from the facility to the environment by at minimum 5,150 pounds per year
(lbs/yr) compared to pre-June 2017 emissions and discharges (Attachment 5).
Specifically, air emission reductions to date, on an annualized basis for 2019, have
resulted in an estimated yearly reduction of 2,150 pounds of HFPO-DA, a greater than
93% reduction. Cessation of Chemours process water discharge to Outfall 002 resulted
in at minimum an estimated yearly reduction of 3,000 lbs/yr of HFPO-DA.
These actions have reduced HFPO-DA mass loadings, through Outfall 002, by over 99%
from June 2017 levels to 2018 levels (Attachment 5). This has resulted in a reduction of
HFPO-DA loading in the Cape Fear River. Present estimates of HFPO-DA mass loading
to the Cape Fear River from all pathways are between 64 and 129 pounds per year (lbs/yr).
This represents upwards of a 95% reduction in mass loading to the Cape Fear River
(Attachment 5).
These reductions will be further enhanced by implementation of the Thermal Oxidizer by
the end of 2019, which will control over 99.99% of PFAS emissions routed to it, and the
actions proposed in this plan will further reduce HFPO-DA and other PFAS loadings to
the environment.
Chemours has also implemented multiple actions to further reduce loading of PFAS to
the Cape Fear River including lining of the previously unlined portions of the Cooling
Water Channel and sediment ponds as well as groundwater extraction from three perched
zone monitoring wells. Specifically, in November 2018 Chemours lined the Cooling
Water Channel surrounding the Monomers IXM Area and the sediment ponds to the west
of the Monomers IXM Area to reduce infiltration of water to the Perched Zone. Over
time, as the water table of the Perched Zone declines from these measures, the mass
loading coming from the Perched Zone to other geological units and seeps will decline
leading to reduced mass loads to the Cape Fear River.
Between February 2018 and February 2019 over 45,000 gallons of groundwater from
MW-24, NAF-03 and NAF-12 were extracted, and extraction of groundwater from these
three wells will continue (Parsons, 2019a). The extracted groundwater has elevated
concentrations of Table3+ compounds and this water is disposed of offsite. This
groundwater extraction reduces the hydraulic head in the Perched Zone and consequently
reduces the PFAS loading from the Perched Zone to the Cape Fear River via aquifers and
groundwater seeps. This groundwater extraction also reduces the amount of PFAS mass
present in the aquifer.

Reduction Plan 17 August 26, 2019
Last, Outfall 002 loading rates in 2019, integrating both dry and wet weather periods, are
presently 8% lower than in calendar year 2018. This reduction is potentially a result of
various completed actions at the Site, including reduced air emissions. Loading at Outfall
002 is expected to continue a downward trajectory year over year.

Reduction Plan 18 August 26, 2019
4 CONSENT ORDER PARAGRAPH 12 PROPOSED ACTIONS
This section presents the seven proposed actions to reduce mass loading of PFAS
originating from the Site. First an overview of the actions is presented, followed by
additional assessment activities that are planned and in-progress that support developing
and refining these actions and last a detailed description of each proposed action, along
with proposed interim benchmarks are presented.

4.1 Overview of Proposed Actions
Beyond actions taken to date (Section 3), the following seven additional proposed actions
are estimated to reduce the remaining mass loading of Total Table 3+ PFAS to the Cape
Fear River by greater than 50%. These proposed reductions are summarized in Table 2
below and described in the sub-sections below.
Table 2: Proposed Paragraph 12 PFAS Loading Reduction Actions
Proposed Action Years to Implement Pathway(s) Reduced
Estimated Cape Fear River
Total Table3+ PFAS Loading
Reduction *,**
lbs/yr %
1) Capture and Treat Old Outfall 002 Water with
a 99% reduction in loading 2 [7] Old Outfall
002 320 to 400 23% to 29%
2) Capture and Treat Seeps with a 95%
reduction in loading 5 [5] Seeps 430 to 320 30% to 23%
3) Targeted Sediment Removal from
Conveyance Network 1 [4] Outfall 002 20 to 40
Using a 40% reduction at Outfall 002
from actions
3 to 7 (mid-range between lower and best
estimates)
1.6% to 2.8%
Using a 40%
loading
reduction at Outfall 002 from actions
3 to 7 (mid-
range between lower and best estimates)

4) Develop and Implement a Stormwater Pollution Prevention Plan (SWPPP) 1 [4] Outfall 002
5) Targeted Stormwater Source Control and/or
Treatment 4 [4] Outfall 002
6) Terracotta Pipe Decommissioning and Replacement 2 [4] Outfall 002
7) Assessing Potential for Groundwater
Intrusion into Conveyance Network 5 [4] Outfall 002
* reductions based on mass loading model estimates from two characterization events. Subsequent characterization
events may yield different estimates depending on environmental conditions at the time of sampling due to the
dynamic nature of the different transport pathways.
** Total estimated reductions were estimated by summing the may estimates (left hand side number together) and
the June estimates (right hand side numbers) together. Both events estimated a 55% reduction for proposed actions.
These proposed actions are believed to be feasible within a two to five-year time period
based on the present state of knowledge regarding the Site and its subsurface conditions.
The first two proposed actions target reducing the highest PFAS concentration pathways

Reduction Plan 19 August 26, 2019
(Seeps and Old Outfall) that presently reach the Cape Fear River directly. The other five
actions work systematically to reduce Outfall 002 PFAS loadings contributed by the Site.
Taken together, these seven actions are estimated to achieve a greater than 50% reduction
of Total Table 3+ PFAS mass loading to the Cape Fear River.

4.2 Planned and In-Progress Additional Assessment Activities
Based on current data and understandings, technologically and economically feasible
actions that could be implemented in two to five years were not identified for the Willis
Creek, Georgia Branch Creek and offsite groundwater pathways. Any potential actions
for these pathways would be extensively disruptive to local wildlife habitats and costs
would be disproportionately high compared to relative benefits.
In addition to Old Outfall 002 and the Seeps, onsite groundwater discharge contributes
relatively more mass to the Cape Fear River than the remaining other pathways.
Geosyntec has recommended that Chemours conduct additional assessment activities
regarding the total PFAS loading originating from the facility, including onsite
groundwater. Some of these activities will be presented in the Consent Order paragraph
18 On and Offsite Assessment report due September 30, 2019. Based on these activities,
Chemours anticipates that it may propose additional actions, including addressing onsite
groundwater in the Corrective Action Plan due December 31, 2019 pursuant to Consent
Order paragraph 16. These anticipated additional actions would be directed toward
reducing total PFAS loading and some of them may potentially be completed within two
to five years. Activities recommended and presently being conducted to assess anticipated
additional actions include the following:
• Completing six additional quarterly assessments of mass loading to the Cape
Fear River. Activities in these events will include sampling and flow gauging
at the mouths of Seeps A through D, Old Outfall 002, Outfall 002, Willis
Creek, Georgia Branch Creek. Also, samples will be collected upstream and
downstream of the Site in the Cape Fear River;
• Conducting an assessment of Cape Fear River bottom sediment temperatures
adjacent to the Site to identify potential zones of increased groundwater
upwelling. This will be reported in the On and Offsite Assessment Report due
on September 30, 2019;
• Conducting further site investigation and characterization activities, including
the installation of additional monitoring wells onsite to further delineate PFAS
concentrations and geology. Multiple wells have been installed as noted below

Reduction Plan 20 August 26, 2019
to further assess hydrogeology and groundwater PFAS concentrations. These
wells will be reported in the On and Offsite Assessment Report due on
September 30, 2019.
o Fifteen additional wells installed adjacent to the Cape Fear River (six pre-
existing wells);
o Two additional wells installed adjacent to Old Outfall 002 (ten wells were
installed adjacent to Old Outfall 002 as part of the PlumeStop™ pilot study
(Parsons, 2019);
o One well installed adjacent to Willis Creek (four pre-existing wells); and
o Three wells installed adjacent to Georgia Branch Creek (no pre-existing
wells).
• Characterizing further the geology and hydrogeology at 24 locations adjacent
to the Cape Fear River using hydraulic profiling and electrical conductivity
(HPT/EC) tools. This characterization will be reported in the On and Offsite
Assessment Report due on September 30, 2019;
• Preparing a numerical model to evaluate groundwater flow conditions in the
three water bearing units at Site and evaluate groundwater interactions with
the Cape Fear River, to assess the efficacy and support design of potential
future actions. This will be prepared to support the Corrective Action Plan due
December 31, 2019.
• Installing 20 offsite monitoring wells to support further understanding of the
horizontal and vertical distribution of PFAS originating from the facility
potentially present offsite. These wells will be reported in the On and Offsite
Assessment Report due on September 30, 2019;
• Conducting continued bimonthly sampling characterization sampling
pursuant to Paragraph 11(b) and (c) of the Consent Order; and
• Conducting two additional stormwater grab sampling events to assess spatial
and temporal trends and loadings from different areas to loads observed at
Outfall 002.

Reduction Plan 21 August 26, 2019
4.3 Detailed Descriptions of Proposed Actions
The following sub-sections list and describe the actions Chemours proposes
implementing. The sub-section for each action includes background, the specific
proposed action, and proposed benchmarks with associated dates. The first action
describes capturing water from Old Outfall 002 and the second action describes capture
and treating the seeps. Actions 3 through 7 describe proposed actions to reduce mass
loading to the Cape Fear River attributable to Outfall 002. Later in the Reductions Plan
Section 5 presents an assessment pursuant to Paragraph 12(d) of the Consent Order if
80% reductions to Outfall 002 loads are technologically and/or economically feasible in
a two-year time period after Consent Order Amendment.
Action 1: Capture and Treat Old Outfall 002 Water
Background: Based on estimates presented in the Mass Loading Model report
(Attachment 1) the Old Outfall 002 contributes between 23% to 29% of Total Table 3+
PFAS Loadings to the Cape Fear River. As part of the Consent Order, Chemours is
required to implement a remedy that either: (i) captures and treats the dry weather flow
of Old Outfall 002 at the location of a proposed dam just upstream of where Old Outfall
002 crosses under Glengerry Road and reduce concentrations of HFPO-DA and
PFMOAA in the treated water by 99% or (ii) achieves equivalent or greater reductions.
Implementing this 99% reduction remedy will reduce loading of PFAS originating from
the facility to the Cape Fear River by an estimated 23 to 29%.
Proposed Actions and Benchmarks: Chemours will continue to comply with the existing
Consent Order requirements by implementing an ex situ capture and treat remedy for Old
Outfall 002.
Action 2: Capture and Treat Seeps
Background: Water samples collected from Seeps A to D were found to have elevated
PFAS concentrations. Based on estimates presented in the Mass Loading Model report
the Seeps contribute between 24% to 32% of the Total Table 3+ PFAS loading to the
Cape Fear River.
Proposed Action: Within five years of Consent Order Amendment, Chemours will
implement a capture and treat remedy which will aim to reduce PFAS mass loading from
Seeps A, B, C and D by up to 95% provided NCDEQ and other permitting authorities
issue required permits. Chemours is presently conducting a detailed evaluation of
potential capture approaches, including ex situ capture and treatment of the seeps and in
situ groundwater capture and treatment. The capture and treat remedy may also be
supported by other measures which would limit mass loading to the seeps. For example,

Reduction Plan 22 August 26, 2019
these measures may include hydraulic containment, capping, or in situ sorptive remedies.
These supportive approaches will be evaluated as part of Consent Order Paragraph 16
(Corrective Action Plan).
Proposed Benchmarks: Chemours proposes proceeding with the following benchmarks
and schedule for seep capture provided permitting authorities grant required permits:
• Select Seep Capture Approach. December 31, 2019. The capture approach for
the seeps will be included as part of the Corrective Action Plan. The selection
of the capture approach will be supported by a numerical modeling analysis.
• Initial Seep Capture Design. 1 year and 6 months from Consent Order
amendment. Initial design will be based on the outcome of numerical model
evaluation and continued quarterly seeps and creeks monitoring.
• Final Seep Capture Design. 2 years and 6 months from Consent Order
amendment. The final design will be based on additional quarterly seeps and
creeks monitoring results.
• Permit Approval for Seep Capture. 3 years and 6 months from Consent Order
Amendment. NCDEQ and other potential permitting authorities have issued
required permits.
• Remedy Implementation. 5 years from Consent Order Amendment. Seep
Capture Remedy Constructed and Operational. Mass Loading reduction of
95% Total Table 3+ PFAS from seeps.

Action 3: Targeted Sediment Removal from Conveyance Network
Background: PFAS from historical aerial deposition may be present in onsite soils. If
impacted soils enter the Site Conveyance Network, they can contribute PFAS to the Cape
Fear River via Outfall 002. Investigations of the Site Conveyance Network indicate
potential increases in PFAS contributions from sediments present in the Conveyance
Network in the open section of the Cooling Water Channel surrounding Monomers IXM
and in the Open Channel from where the Waste Water Treatment Facility effluent joins
the Channel to the end of the Channel.
Presently the loading reductions at Outfall 002 from targeted sediment removal cannot
be accurately quantified. Removing sediments from the Cooling Water Channel and the
Open Channel to Outfall 002 is expected to support reducing loadings from these Site
Conveyance flow components.

Reduction Plan 23 August 26, 2019
Proposed Action: Chemours will develop a plan to remove sediment present in the
sections of the Site Conveyance Network. Chemours will perform the sediment removal
during the yearly turnaroud (when the Site pauses production activities), including
passing water through the Site Conveyance Network, to perform yearly preventative
maintenance.
Proposed Benchmarks: Chemours will remove sediments from the open section of the
Cooling Water Channel and the Open Channel to Outfall 002 from the Wastewater
Treatment Plant to and including the Outfall 002 sump within 1 year of Consent Order
Amendment with reporting due within 1 year and six months of Consent Order
Amendment.

Action 4: Develop and Implement a Stormwater Pollution Prevention Plan (SWPPP)
Background: PFAS from historical aerial deposition may be present onsite soils. If these
soils enter the Site Conveyance Network, they can contribute to PFAS at Outfall 002.
Stormwater Pollution Prevention Plans provide facility-specific guidance on best
management practices to reduce the potential for stormwater-related increases in
discharge concentrations. Implementation of the SWPPPs reduce the potential for
stormwater contamination from industrial activities and potential sources, such as
impacted soils or active construction or soil stockpiling, which will reduce the potential
for increased Outfall 002 PFAS concentrations during rainfall events.
Presently the expected loading reductions at Outfall 002 from developing and
implementing a SWPPP cannot be accurately quantified. This action will help to put in
place best practices that are expected to support and help maintain anticipated loading
reductions across the entire Site Conveyance Network and at Outfall 002.
Proposed Action: Chemours will fund a third party to prepare a SWPPP. Facility
personnel will be trained to support implementation and compliance with SWPPP best
management practices (BMPs) and inspection procedures.
Proposed Benchmarks: A SWPPP will be prepared within 120 days of Consent Order
Amendment. Identified facility staff will be trained on how to implement the SWPPP
within one year of Consent Order Amendment.

Reduction Plan 24 August 26, 2019
Action 5: Implement Targeted Stormwater Source Control and/or Treatment
Background: A stormwater grab sampling program was completed in June 2019. This
program consisted of collecting water samples from 24 locations across the Site and
results from this program indicated areas of elevated PFAS concentrations in stormwater.
This suggests that some combination of targeted source control and stormwater collection
and treatment could achieve measurable mass loading reductions. At present only one
stormwater grab sampling event has been possible due to rainfall patterns since April
2019. A preliminary analysis using the data from this one sampling event suggest that
between 16% and 30% of HFPO-DA loading at Outfall 002 can be reduced through
targeted stormwater source control and/or treatment approaches. Since only one data set
exists at present, additional data and assessment activities are necessary to develop a
better understanding of stormwater levels and spatial patterns throughout the Site in order
to select and design suitable approaches.
Proposed Action: Chemours will fund third party contractors to conduct two additional
stormwater grab sampling programs to evaluate stormwater concentrations. Chemours
will also fund a third-party contractor to develop a hydrologic stormwater model to assess
potential mass loading reductions and to develop a targeted stormwater action plan and
best management practices based on the data from the stormwater grab sampling events
and the outcome of the modeling analysis. This plan will outline initial actions to be
performed. The performance evaluation reporting of the actions will include any
potentially recommended supplementary actions.
Proposed Benchmarks: Chemours proposes proceeding with the following benchmarks
and schedule for Targeted Stormwater Source Control and/or Treatment provided
permitting authorities grant required permits:
• Complete Stormwater Grab Sample Program: 8 months after Consent Order
amendment.
• Complete Hydrologic Model Analysis: 1 year after Consent Order
Amendment.
• Complete Targeted Stormwater Action Plan: 1 year and 6 months after
Consent Order Amendment.
• Stormwater Actions Plan Actions Implemented: 2 years and 6 months after
Consent Order Amendment.
• Evaluation of Initial Actions and Supplemental Recommendations: 4 years
after Consent Order Amendment.

Reduction Plan 25 August 26, 2019
Action 6: Decommission and Replace Remaining Portion of the Terracotta Pipe
Background: The remaining portion of the terracotta pipe is a buried pipe at the Site and
is presently used to: (i) transmit process water from Kuraray operations to the Wastewater
Treatment Plant and (ii) transmit filter wash water from the filtered and demineralized
water production facility to the Wastewater Treatment Plant. Prior to June 21, 2017,
process wastewaters from the Chemours Monomers IXM Area were transmitted to the
Wastewater Treatment Plant via an east-west section of the terracotta pipe. Between June
21, 2017 and November 29, 2017 Chemours diverted process wastewater from the
Monomers IXM area away from the Wastewater Treatment Plant and to offsite disposal.
On November 29, 2017, Chemours severed the terracotta pipe connection from the
Chemours Monomers IXM Area to prevent the potential for process wastewater to be
conveyed by the terracotta pipe. In February 2019, Chemours grouted the east-west
section of the terracotta pipe (Attachment 4) to limit the potential for groundwater or
stormwater to infiltrate this section of the pipe and potentially be transmitted to the
Wastewater Treatment Plant and then to Outfall 002 and the Cape Fear River.
Recent sampling at locations along the terracotta pipe indicate that PFAS are still present,
potentially adhered to remnant sediments or potentially infused onto/into the clay pipe
itself (Attachment 3). Kuraray and Chemours are planning to decommission the terracotta
pipe and replace it with an above ground pipe. Replacing the terracotta pipe is estimated
to reduce HFPO-DA loadings to Outfall 002 between 1% and 2%.
Proposed Action: Within 2 years of Consent Order Amendment, Chemours will
decommission the terracotta pipe by removing the connection of the terracotta pipe to the
Wastewater Treatment Plant. Flows of water to the Wastewater Treatment Plant from the
terracotta pipe will be transmitted through newly constructed above ground piping.
Proposed Benchmarks: Chemours will decommission the terracotta pipe within two years
of the Consent Order Amendment.

Action 7: Assess Potential for Groundwater Intrusion into Conveyance Network
Background: Water samples collected from the Outfall 002 Open Channel during
sampling events conducted in April and June 2019 pursuant to Consent Order Paragraph
11(b) have shown increases in HFPO-DA concentrations along the Open Channel to
Outfall 002, near the DuPont Area (Attachment 3; Geosyntec 2019b) with no point
sources evident suggesting a diffuse source. The source of these increased HFPO-DA
concentrations has not been determined but may be potentially related to:

Reduction Plan 26 August 26, 2019
• Sediments in the channel. Sediment samples in the Outfall 002 open channel were
too fine and could not be reliably collected during sampling conducted in July
2019. These sediments can be removed as per Action 3 above, and samples of
the removed sediment would be sent for analysis of PFAS concentrations; and
• Potentially perched zone groundwater containing HFPO-DA enters the Open
Channel to Outfall 002 near the DuPont Area where perched zone groundwater
levels may potentially be higher than water levels in the Outfall Channel.
Groundwater in this area also contains HFPO-DA at concentrations higher than
in Outfall 002 (66,000 ng/L at PZ-24; Parsons, 2019c). The Outfall Channel is
lined with a grout filled revetment mat and underlain with Geotextile to limit
connectivity with the surrounding environment. If groundwater levels are higher
than the water levels in the Outfall Channel, then groundwater intrusion is
possible in principle but may be limited by the materials from which the channel
is constructed.
While at present the expected reductions from this action to PFAS loading at Outfall 002
cannot be accurately quantified, this action in combination with Actions 3 described in
this document have the potential to reduce facility-based loadings from the Open Channel
to Outfall 002. Loadings from the Open Channel to Outfall 002 were estimated to
represent between 38% and 69% of the dry weather loading attributable to the facility
(i.e. excluding intake contributions) from the April and June 2019 sampling events
respectively (Attachment 3).
Proposed Actions: During Site turnaround Chemours will (a) survey the elevations of the
bottom of the Open Channel and the Outfall 002 sump near the DuPont Area to compare
channel bottom elevations to measured nearby groundwater elevations in monitoring
wells, and (b) inspect the Open Channel from where the Cooling Water Channel joins the
Open Channel to the end of the Open Channel, including the sump, for groundwater
entering the Open Channel. If this assessment indicates there is a potential for
groundwater to enter into the Site Conveyance Network in this area, Chemours will
prepare an action plan to mitigate this contribution to Outfall 002 concentrations.
Proposed Benchmarks: Chemours proposes proceeding with the following benchmarks
and schedule for assessing the potential for groundwater intrusion into the Open Channel
to Outfall 002:
• Open Channel sediment removal within 1 year of Consent Order Amendment
with reporting due within 1 year and six months of Consent Order
Amendment.

Reduction Plan 27 August 26, 2019
• Survey elevation of bottom of Open Channel to Outfall 002 and measure water
levels in nearby groundwater wells during Site turnaround within 1 year of
consent order amendment with reporting due within 1 year and 6 months of
consent order amendment.
• Inspect Open Channel to Outfall 002 for evidence of any direct connection to
groundwater during Site turnaround within 1 year of consent order
amendment with reporting due within 1 year and 6 months of consent order
amendment.
• If necessary, assess potential alternatives for reducing groundwater intrusion:
1 year after Consent Order Amendment.
• Conduct actions resulting from alternatives analysis (if necessary): 3 to 5 years
after Consent Order Amendment depending on actions recommended and
permitting authorities granting any potentially required permits.

Reduction Plan 28 August 26, 2019
5 PARAGRAPH 12(D) OUTFALL 002
Of the seven (7) actions Chemours has proposed implementing five (5) proposed actions
will reduce Total Table 3+ PFAS loadings to Outfall 002. Similar to Cape Fear River
PFAS Loading reductions described earlier, Chemours has reduced HFPO-DA loadings
to Outfall 002 by over 99% through completed actions as described in Section 3. With
these reductions, Outfall 002 in contributes only between 4% to 7% of Total Table 3+
PFAS mass loading to the Cape Fear River and between 1% and 4% of HFPO-DA loading
to the Cape Fear River (Attachment 1). Consequently, any reductions to Outfall 002 under
normal operating conditions do little to reduce total mass loadings, especially compared
to the proposed reductions for the Old Outfall and the Seeps which together will result in
greater than 50% reductions of Total Table 3+ PFAS loading to the Cape Fear River.
Regarding further Outfall 002 reductions the Consent Order states:
The burden is on Chemours to demonstrate that the concentrations of GenX
and perfluoro-1-methoxyacetic acid (PFMOAA) detected in Outfall 002
cannot be reduced by at least 80% from baseline levels, including after
measurable storm events, as defined in 40 C.F.R. 122.21(g)(7)(ii), within 2
years.
The Outfall 002 Assessment Report (Attachment 3) reported the Outfall 002 load for
HFPO-DA and PFMOAA for the calendar year 2018. could further reduce HFPO-DA
and PFMOAA concentrations at Outfall 002 and assessed potential reductions from these
approaches. These approaches are listed in Table 3 below, including the time length to
implement, anticipated Outfall 002 reductions where they can be estimated, and if the
approach is technologically and economically feasible.
The five proposed actions related to Outfall 002 are estimated to achieve a combined
HFPO-DA reduction between 27% to 53% of Outfall 002 yearly HFPO-DA loading; this
is estimated to be 0.4% to 2.4% of the HFPO-DA loading to the Cape Fear River. The
anticipated loadings for PFMOAA could not be assessed; the available PFMOAA data
were too limited to make reduction estimates at present. The estimated HFPO-DA
loading reductions would be achieved by reducing the dry weather loads from the Cooling
Water Channel and the Open Channel, reducing loads from stormwater through targeted
source control and treatment and replacing the terracotta pipe. Including HFPO-DA
reductions in 2019 increases the estimated potential combined HFPO-DA loading
reduction total to 35% to 61% at Outfall 002, or 0.5% to 2.7% of HFPO-DA loadings to
the Cape Fear River. These estimated potential reductions are summarized below in
Figure 7, with both lower and “best” estimates shown (Attachment 3).

Reduction Plan 29 August 26, 2019
Two control approaches, G and H in Table 3 were at present assessed to be economically
infeasible. Approaches G, (Separating Stormwater and Non-Contact Cooling Water
Conveyances and Treating Stormwater End of Pipe), requires extensive construction of
piping network. Both approaches G and H (treating stormwater and non-contact cooling
water end of pipe) would require enormous treatment media usage and treatment system
infrastructure. The extremely high anticipated costs would be disproportionately large
compared to estimated benefits to Cape Fear River loading reductions, particularly as
Outfall 002 at present is only a relatively small contributor to River loadings.

Table 3: Potential Outfall 002 Control Approaches
Potential Outfall 002 Control Approaches Years to Implement
HFPO-DA Reduction to Outfall 002
HFPO-DA Reduction to Cape Fear River
Technologically and Economically Feasible
A: Targeted Sediment Removal – Proposed Action 3 1 NQ Note 1 NQ Note 1 
B: Develop and Implement a SWPPP – Proposed Action 4 1 NQ Note 1 NQ Note 1 
C: Targeted Stormwater Source Control and/or Treatment – Proposed Action 5 4 16 to 30% 1% 
E: Reducing Potential Groundwater Intrusion – Proposed Action 7 3 to 5 6 to 13% 0.5% 
D: Decommissioning and Replacing the Remaining Portion of the Terracotta Pipe – Proposed Action 6
2 1 to 2% 0.1% 
F: Additional Investigation to Assess
and Control Dry Weather Cooling
Water Channel Sources – Note 1
2 to 4 Note 1 4 to 8% 0.2 to 0.4%  Note 1
G: Separating Stormwater and Non-Contact Cooling Water Conveyances and Treating Stormwater End of Pipe 5 40% 2% 
H: Treating Stormwater and Non-Contact Cooling Water End of Pipe 3 80% 3% 
NQ – not quantifiable
1 – Targeted sediment treatment, SWPPP actions and targeted stormwater source control and treatment may accomplish
Cooling Water Channel loading reductions making no additional benefit to further investigations. The range of 2 to 4
years for these additional investigations recognizes that the targeted sediment removal and targeted stormwater
approaches would be attempted first in this sequence.

Reduction Plan 30 August 26, 2019
Table 4: Estimated Outfall 002 HFPO-DA Reductions by Conveyance Network Flow Component
Conveyance Network Flow Component Actions Estimated to Contribute to Loading Reductions
Estimated Range of HFPO-DA Reductions at Outfall 002
2018 to 2019 Reductions - Air abatement, - Site practices 8%
Stormwater (Targeted Areas) - Action 5 – Targeted Stormwater 16 to 30%
Open Channel to Outfall 002
- Action 3 – Sediment Removal - Action 4 – SWPPP - Action 7 – Assess Groundwater Intrusion 6 to 13%
Wastewater Treatment Plant / Terracotta Pipe - Action 6: Terracotta Pipe 1 to 2%
Cooling Water Channel* (i.e. CWC)
- Action 3 – Sediment Removal
- Action 4 – SWPPP - Action 5 – Targeted Stormwater - If needed, further assessment - As Needed Investigation and Control of
Dry Weather Loading Sources
4 to 8%
Total 35% to 61%
* The anticipated reduction percentages presented for the Cooling Water Channel assume that sediment removal,
stormwater actions and SWPPP together will accomplish the estimated reductions shown here and if not then the
Cooling Water Channel investigation and control of dry weather loading sources, which is a potential action under
consideration not a proposed action at this time, would be implemented later as necessary.

Reduction Plan 31 August 26, 2019

Figure 7: Lower and Best Estimates of HFPO-DA Load Reductions in Outfall 002 Compared to 2018 Loads. The anticipated reduction percentages presented for the Cooling Water Channel assume that
sediment removal, stormwater actions and SWPPP together will accomplish the estimated reductions shown here and if not then the Cooling Water Channel investigation and control of dry weather loading sources, which is a potential action under consideration not a proposed
action at this time, would be implemented later as necessary. CWC – Cooling Water Channel WWTP – Wastewater Treatment Plant

0%
10%
20%
30%
40%
50%
60%
70%
80%
90%
100%
Lower Estimate of Reductions
from Proposed Control Measures
Best Estimate of Reductions from
Proposed Control MeasuresReductions as Percent of Total LoadReductions Yielded in 2019
CWC Contributions
WWTP/Terracotta Pipe
Open Channel Contributions
Stormwater (Targeted Areas)

Reduction Plan 32 August 26, 2019
6 SUMMARY
To date Chemours has reduced the loading of HFPO-DA in the Cape Fear River by over
95%. Chemours is committed to further reducing PFAS loadings, including HFPO-DA,
to the Cape Fear River. Pursuant to Consent Order Paragraph 12 Geosyntec has developed
the proposed recommended actions detailed in this plan and Chemours anticipates that
following NCDEQ and CFRW review, the parties will come to an agreement to amend
the Consent Order to incorporate the proposed recommended actions.
This reduction plan proposes seven actions that would reduce the Total Table 3+ PFAS
loadings in the Cape Fear River by greater than 50% from observed May and June 2019
levels. These actions will be implemented over a two to five-year period upon Consent
Order Amendment.
The selection of these actions was supported by numerous field investigations,
development of a PFAS Mass Loading Model and an assessment of HFPO-DA and
PFMOAA at Outfall 002. The PFAS Mass Loading Model identified three PFAS
transport pathways (the Old Outfall 002 onsite groundwater and Seeps) as primary
contributors to Cape Fear River Table 3+ PFAS mass loading. Consequently, two of the
actions focus on reducing mass loading from these pathways. The Outfall 002 assessment
identified areas of HFPO-DA and PFMOAA loading in the Site Conveyance network that
guided the selection of five actions to reduce HFPO-DA and PFMOAA loading at Outfall
002.
Chemours is also advancing additional characterization efforts at the Site to support the
selection and placement of these and other actions to further reduce PFAS loading
originating from the facility to the Cape Fear River. These potential additional actions
will be evaluated in the Corrective Action Plan due December 31, 2019.

Reduction Plan 33 August 26, 2019
7 REFERENCES
Geosyntec 2018: Assessment of the Chemical and Spatial Distribution of PFAS in the
Cape Fear River, September 17, 2018
Geosyntec 2019a: Site Associated PFAS Fate and Transport Study, Chemours
Fayetteville Works. June 2019.
Geosyntec 2019b: Characterization of PFAS in Process and Non-Process Wastewater and
Stormwater Quarterly Report #1. Chemours Fayetteville Works July 31, 2019.
Parsons, 2018. Additional Site Investigation Report, Chemours Fayetteville Works Site.
RCRA Permit No. NCD047368642-R1. January 31, 2018.
Parsons, 2019a: Results of Temporary Perched Zone Groundwater Pumping, Chemours
Fayetteville Works Site. RCRA Permit No. NCD047368642-R2-M3. June 2019.
Parsons, 2019b: Old Outfall 002 Remedial Options Plan, Chemours Fayetteville Works
Site. RCRA Permit No. NCD047368642-R2-M3. May 2019.
Parsons, 2019c: Southeast Perched Zone Investigation Report. Chemours Fayetteville
Works. RCRA Permit No. NCD047368642-R2-M3. March 2019

ATTACHMENT 1:
Cape Fear River PFAS Mass Loading Model
Assessment and Paragraph 11.1
Characterization of PFAS at Intakes

CAPE FEAR RIVER PFAS MASS
LOADING MODEL ASSESSMENT AND
PARAGRAPH 11.1
CHARACTERIZATION OF PFAS AT
INTAKES
Chemours Fayetteville Works, NC
Prepared for
The Chemours Company FC, LLC Fayetteville Works
22828 NC Highway 87 W
Fayetteville, NC 28306 Prepared by
Geosyntec Consultants of NC, P.C. 2501 Blue Ridge Road, Suite 430 Raleigh, NC 27607
Geosyntec Project Number TR0795
August 2019

PFAS Mass Loading Model Assessment i August 26, 2019
TABLE OF CONTENTS
EXECUTIVE SUMMARY ......................................................................................................... VII
1. INTRODUCTION ....................................................................................................................1 1.1 Objectives .................................................................................................................................1
1.2 Document Organization ...........................................................................................................2
2. SITE BACKGROUND .............................................................................................................3
3. SITE SETTING ........................................................................................................................4 3.2 Cape Fear River and Downstream Public Water Utility Intakes ..............................................7
3.3 Potential PFAS Transport Pathways to Cape Fear River .........................................................7
4. PFAS MASS LOADING MODEL DESIGN ...........................................................................9
4.1 Upstream Cape Fear River (Transport Pathway 1) ................................................................11
4.2 Tributaries – Willis Creek, Georgia Branch Creek, and Old Outfall 002 (Transport Pathways 2, 7 and 9) ......................................................................................................................................12
4.3 Aerial Deposition to the Cape Fear River (Transport Pathway 3) .........................................12
4.4 Onsite Groundwater (Transport Pathways 5 and 6) ...............................................................12
4.4.1 Indirect Pathway – Groundwater Seeps to River (Transport Pathway 6) .........13
4.4.2 Direct Pathway – Groundwater Discharge to River (Transport Pathway 5) .....13
4.5 Outfall 002 and Facility Stormwater Runoff (Transport Pathway 4) .....................................13
4.6 Offsite Groundwater (Transport Pathway 8) ..........................................................................14
5. MODEL CALIBRATION AND SENSITIVITY ANALYSIS ..............................................15 5.1 Model Calibration ...................................................................................................................15
5.2 Model Results .........................................................................................................................17
5.3 Sensitivity Analysis ................................................................................................................19
6. LIMITATIONS AND ASSUMPTIONS ................................................................................21
7. SUPPLEMENTAL ACTIVITIES ..........................................................................................22
8. CONSENT ORDER PARAGRAPH 11.1 ANALYSIS .........................................................23
8.1 Assessment Methodology .......................................................................................................24
8.1.1 PFAS Compound Source Origination Assessment ...........................................24
9. SUMMARY ...........................................................................................................................26
10. REFERENCES .......................................................................................................................28

PFAS Mass Loading Model Assessment ii August 26, 2019

LIST OF TABLES
Table 1: PFAS Mass Loading Model Potential Pathways
Table 2: Analytical Methods and Analyte List
Table 3: Summary of Analytical Results – Total PFAS and Total Table 3+
Table 4: Summary of Flow Rate Input Values
Table 5: Model Estimated Total Table 3+ Mass Loading Calibration
Table 6: Model Estimated Total Table 3+ Mass Loading Contributions Per Pathway
Table 7-A: Observed Concentrations and Mass Loading at Bladen Bluffs - May 2019 and June 2019
Table 7-B: Observed Concentrations and Mass Loading at Kings Bluff - May 2019 and June 2019
Table 8-A: Estimated Pathway Contribution to Observed Concentration at Bladen Bluffs - May 2019
Table 8-B: Estimated Pathway Contribution to Observed Concentration at Bladen Bluffs -
June 2019
Table 8-C: Estimated Pathway Contribution to Observed Concentration at Kings Bluff - May 2019
Table 8-D: Estimated Pathway Contribution to Observed Concentration at Kings Bluff - June 2019
Table 9-A: Estimated Mass Loading with 1st Quartile Input Values – May 2019
Table 9-B: Estimated Mass Loading with 1st Quartile Input Values – June 2019
Table 10-A: Estimated Contribution Percentage of Pathway to Total Mass Loading – May 2019
Table 10-B: Estimated Contribution Percentage of Pathway to Total Mass Loading – June
2019
Table 11: Estimated Mass Loading Source Origination Percentages Per Compound Per Pathway

PFAS Mass Loading Model Assessment iii August 26, 2019
LIST OF FIGURES
Figure 1: Site Location Map
Figure 2: Potential PFAS Pathways to the Cape Fear River from Site
Figure 3: Cape Fear River Watershed and Downstream Public Utility Intakes
Figure 4: Comparison of Observed and Best-fit Modeled Total Table 3+ Mass Loading at Bladen Bluffs
Figure 5: Estimated Pathway Contributions to Observed Total Table 3+ Concentrations Adjacent to Bladen Bluffs Intake
Figure 6: Modeled and Empirical HFPO-DA Time Series at Kings Bluff
Figure 7: Estimated Source of Observed Total PFAS Concentration at Bladen Bluffs and Kings Bluff

PFAS Mass Loading Model Assessment iv August 26, 2019

LIST OF APPENDICES
Appendix A: Supplemental Analytical Data
Appendix B: Supplemental Flow Gauging Data
Appendix C: Supporting Calculations – Direct Aerial Deposition on Cape Fear River
Appendix D: Supporting Calculations – On Site Groundwater Flow Estimate
Appendix E: Supporting Calculations – Off Site Groundwater Flow Estimate
Appendix F: Summary of Sensitivity Analysis Results

PFAS Mass Loading Model Assessment v August 26, 2019
ACRONYMS AND ABBREVIATIONS
% Percent
bgs Below Ground Surface
CFPUA Cape Fear Public Utility Authority
CO Consent Order
CSM Conceptual Site Model
DuPont E.I. du Pont de Nemours and Company
EPA Environmental Protection Agency (United States)
ft Feet
HPT/EC Hydraulic Profiling Tool and Electrical Conductivity
HFPO-DA Hexafluoropropylene oxide dimer acid
LTW Long-Term Wells
MSL Mean Sea Level
m/s Meters per Second
NCDEQ North Carolina Department of Environmental Quality
NRMSE Normalized Root Mean Square Error
NVHOS Perfluoroethoxysulfonic acid
PFAS Per- and polyfluoroalkyl substances
PMPA Perfluoro-2-methoxypropanoic acid
PVF Polyvinyl Fluoride
SOP Standard Operating Protocol
USGS United States Geological Survey
WWTP Wastewater Treatment Plant

PFAS Mass Loading Model Assessment vii August 26, 2019
EXECUTIVE SUMMARY
Geosyntec Consultants of NC, P.C. (Geosyntec) has prepared this report for The Chemours
Company FC, LLC (Chemours) to describe the mass loading model developed to inform a plan to
reduce per- and polyfluoroalkyl substances (PFAS) to the Cape Fear River from the Chemours
Fayetteville Works Site (the Site) pursuant to Paragraph 12 of the executed Consent Order (CO)
dated 25 February 2019 among the North Carolina Department of Environmental Quality
(NCDEQ), Cape Fear River Watch, and Chemours. The model presented in this report is required
by Consent Order Paragraph 12 and is one of four documents supporting the Cape Fear River
PFAS Reduction Plan (“the Reduction Plan”). The objective of the model is to identify the PFAS
loading from transport pathways originating from the Site to the Cape Fear River. This objective
is accomplished by estimating total PFAS mass loading originating from the Site to the Cape Fear
River, including estimates of loading from nine transport pathways, and comparing these estimates
to empirically measured PFAS loading in the Cape Fear River. The results of the modeling analysis
have been used to support the selection of PFAS mass loading reduction actions being proposed
in the Reduction Plan.
PFAS mass loading is defined, in this model, as the combined mass per unit time (e.g. nanograms
per second) from potential sources. The model estimates PFAS contributions from nine pathways
(i.e. compartments) such as various creeks and groundwater to estimate Cape Fear River mass
loading using measured Cape Fear River flow volumes. These estimated mass loading are then
compared to measured in-river mass loading as an assessment of model calibration. The mass
loading model constructed, calibrated, and applied is a quantitative estimate of the current
understanding of the conceptual site model and transport pathways. It is based on availability of
data points, and thus in a complex and dynamic environment, there are uncertainties. The model
was constructed based on discrete field observations, which were then interpolated to approximate
conditions across the model domain and assumed to be representative in between the measured
points. This model is useful to identify trends in mass loading to the Cape Fear River for a range
of conditions and support identification of potential target pathways for actions to achieve
objectives for mass loading and corresponding concentration reductions of Site associated PFAS
in the Cape Fear River.
A total of 21 iterative calibration scenarios were performed to optimize the model-estimated total
Table 3+ mass loading in the Cape Fear River to approximately match empirical mass loading at
the Bladen Bluffs raw water intake based on the May and June 2019 field programs. For each
calibration iteration, the estimated total Table 3+ mass loading to the river was compared to
empirical loading at Bladen Bluffs, for the same sampling time period and five input parameter
scenarios (1st quartile, median, 3rd quartile, average and geometric mean values for concentration
and flow) to assess how the variability in the possible set of input parameters chosen would affect

PFAS Mass Loading Model Assessment viii August 26, 2019
results. Calibrated model-fit was tested through computation of a normalized root mean square
error (NRMSE) between modeled and empirical mass loading. Calibration results indicate that a
lower bound NRMSE of 0.16 was achieved assuming the 1st quartile model input parameter values
for nine calibration steps. To identify a best-fit model amongst these nine calibrations steps, the
lowest sum of NRMSE between modeled and empirical mass loading for all five input parameter
scenarios was evaluated. Calibration results indicate that a best-fit model was achieved for
calibration step 8 assuming the 1st quartile model input parameter values. The best-fit model
identified in calibration assumes the following 1st quartile model input parameter values: (a) onsite
discharge area of 58%; (b) upper Black Creek Aquifer hydraulic conductivity of 1x10-6 meters per
second (m/s); (c) lower Black Creek Aquifer hydraulic conductivity of 1.5x10-4 m/s; and (d) offsite
Surficial Aquifer hydraulic conductivity of 2.5x10-4 m/s.
From the nine transport pathways evaluated the mass loading model estimates that the Old Outfall
002 and Seeps (Transport Pathways 7 and 6 respectively) are the largest contributors of Table 3+
PFAS mass to the Cape Fear River based on inputs from the two mass loading characterization
events (May and June 2019). These two pathways combined contribute approximately 53% to 55%
of the loading of Table 3+ PFAS to the Cape Fear River. Onsite groundwater (Transport Pathway
5) is the next largest contributing mass loading pathway to the Cape Fear River with 17% and
22%.
Additional assessments and characterization of onsite groundwater are currently being undertaken,
including preparing a numerical groundwater model to evaluate groundwater interactions with the
Cape Fear River and to evaluate the efficacy and support design of potential future actions.
Additionally, six more quarterly field events evaluating mass loading to the river will be completed
to assess and refine these mass loading findings over time and in different weather and seasonal
conditions.
Pathway
Total Table 3+
Estimated Loading Percentage per Pathway per Event May 2019
Event
June 2019
Event
[1] Upstream River Water and Groundwater 4% 15%
[2] Willis Creek 10% 4%
[3] Aerial Deposition on Water Features < 2% < 2%
[4] Outfall 002 4% 7%
[5] Onsite Groundwater 22% 17%
[6] Seeps 32% 24%
[7] Old Outfall 002 23% 29%
[8] Offsite Adjacent and Downstream Groundwater < 2% < 2%
[9] Georgia Branch Creek 4% 3%

PFAS Mass Loading Model Assessment ix August 26, 2019
Using a combination of mass loading model assessment results and observed PFAS concentrations
at downriver raw water intakes, an assessment was performed pursuant to Paragraph 11.1 of the
Consent Order, to estimate the percentage of PFAS loading at downriver raw water intakes as
originating from the Site, other sources, or at present unknown sources (which could be either the
Site or the other sources). On a total PFAS basis this analysis indicated that at Bladen Bluffs and
Kings Bluff raw water intakes for the May and June 2019 sampling events, between 68% to 84%
of PFAS may have originated from the Site. Meanwhile, between 13% to 29% of PFAS may have
originated from other, non-Chemours sources and 2% to 3% may have originated from unknown
sources which may potentially be non-Chemours or Chemours sources; the unknown sources will
assessed in upcoming planned characterization activities. Actions proposed in the Reduction Plan
and the upcoming Corrective Action Plan due on December 31, 2019 will reduce the total PFAS
loading to the Cape Fear River and significantly reduce the loading originating from the Site.
The mass loading model developed provides a basis for continued evaluation of the PFAS mass
load contributions to the Cape Fear River. Additional sampling events are planned, and this data
will be used in the model to confirm the parameters used to date. In the first two sampling events,
the largest contributing pathways are the seeps (A to D) and Old Outfall 002. The mass loading
model will serve to inform proposed PFAS loading reductions and as remedial measures are put
in place to then support quantification of PFAS loading reductions.

PFAS Mass Loading Model Assessment 1 August 26, 2019
1. INTRODUCTION
Geosyntec Consultants of NC, P.C. (Geosyntec) has prepared this report which describes the mass
loading model assessment completed for The Chemours Company FC, LLC (Chemours) for the
Fayetteville Works (Site) in Bladen County, North Carolina. This report describes a mass loading
model that was developed to inform a plan to reduce per- and polyfluoroalkyl substances (PFAS)
to the Cape Fear River from the Site pursuant to Paragraph 12 of the executed Consent Order (CO)
dated 25 February 2019 among the North Carolina Department of Environmental Quality
(NCDEQ), Cape Fear River Watch, and Chemours. This report also presents a characterization of
PFAS at downstream raw water intakes based on the mass loading model assessment pursuant to
Paragraph 11.1 of the CO.
CO Paragraph 12 relates to the “Accelerated Reduction of PFAS Contamination in the Cape Fear
River and Downstream Water Intakes” and requires the development of a model that accounts for
sources of PFAS from the Facility contributing loading of PFAS into the Cape Fear River, Willis
Creek, Georgia Branch, and Old Outfall 002. Geosyntec has been approved by NCDEQ and
contracted by Chemours to perform the modeling effort for CO Paragraph 12(b). This model is
presented here in this report.
1.1 Objectives
The objective of this report is to describe the modeling analyses (the PFAS mass loading model)
undertaken to estimate PFAS mass loading originating from the facility to the Cape Fear River
directly and through Willis Creek, Georgia Branch Creek, Old Outfall 002, four groundwater seeps
on the bluff near the manufacturing area to the Cape Fear River, and discharging groundwater that
reach the Cape Fear River from the Site.
The objective of the model is to evaluate total PFAS mass loading originating from the facility to
the Cape Fear River and estimate the percentage of mass loading coming from each transport
pathway in empirically measured PFAS mass in the river. The results of the modeling analysis will
be used to support the selection of PFAS mass loading reductions actions by helping identify which
transport pathways contribute the most to total PFAS loading from the facility in the Cape Fear
River.
PFAS mass loading is defined, in this model, as the combined mass per unit time (e.g. nanograms
per second) from potential sources. The model estimates PFAS contributions from multiple
pathways (i.e. compartments) such as various creeks and groundwater to estimate Cape Fear River
concentrations using measured Cape Fear River flow volumes. These estimated concentrations are
then compared to measured in-river concentrations as an assessment of model calibration. Results
from the calibrated model are then used in combination with known background and upstream

PFAS Mass Loading Model Assessment 2 August 26, 2019
PFAS concentrations to characterize PFAS mass loading contributions from the Site to
downstream raw water intakes, as required in Paragraph 11.1 in the CO, and assess potential
reductions in PFAS mass loading to the Cape Fear River.
1.2 Document Organization
The remainder of this document contains the following sections:
• Section 2 – Site Background – this section describes Site background and use;
• Section 3 – Site Setting – this section describes the Site setting, including the current
understanding of the conceptual site model and potential transport pathways for PFAS
originating from the facility;
• Section 4 – PFAS Mass Loading Model Design – this section describes how the PFAS
mass loading model was constructed and developed;
• Section 5 – Model Calibration and Sensitivity Analysis – this section describes how
the model was calibrated, including calibration datasets; and procedures for addressing
uncertainties associated with the model;
• Section 6 – Limitations and Assumptions – this section presents a discussion of some
limitations and assumptions of the mass loading model assessment;
• Section 7 – Supplemental Activities – this section summarizes additional and ongoing
field activities;
• Section 8 – Paragraph 11.1 Characterization of PFAS Mass Loading in
Downstream Raw Water Intakes – this section describes PFAS mass loading
contributions from the Site to downstream raw water intakes;
• Section 9 – Summary – this section describes a summary of the mass loading model
assessment results as it pertains to the PFAS Reduction Plan; and
• Section 10 – References – this section lists work plan reference documentation.

PFAS Mass Loading Model Assessment 3 August 26, 2019
2. SITE BACKGROUND
The Site is located within a 2,177-acre property at 22828 NC Highway 87, approximately 20 miles
southeast of the city of Fayetteville along the Bladen-Cumberland county line in North Carolina.
Figure 1 presents an overview of the Site. The Site is bounded by NC Highway 87 to the west,
Cape Fear River to the east, and on the north and south by undeveloped areas and farmland. Willis
Creek and Georgia Branch Creek, tributaries to the Cape Fear River, are located toward the
northern and southern property boundaries, respectively, with Georgia Branch Creek being offsite
for its entire course.
The Site property was originally purchased by E.I. du Pont de Nemours and Company (DuPont)
in 1970 for production of nylon strapping and elastomeric tape. DuPont sold its Butacite® and
SentryGlas® manufacturing units to Kuraray America Inc. (Kuraray) in June 2014 and
subsequently separated its specialty chemicals business to Chemours in July 2015. Presently, the
Site consists of five manufacturing areas (Figure 1): Chemours Monomers IXM (Area 1);
Chemours Polymer Processing Aid (PPA; Area 2); Kuraray Butacite® (Area 3); Kuraray
SentryGlas® (Area 4); and DuPont Company polyvinyl fluoride (PVF) resin manufacturing unit
(Area 5). In addition to the manufacturing operations, Chemours operates two natural gas-fired
boilers and a wastewater treatment plant (WWTP) for the treatment of sanitary wastewaters as
well as process wastewaters from Kuraray and DuPont.

PFAS Mass Loading Model Assessment 4 August 26, 2019
3. SITE SETTING
A description of the Site setting, including the physical setting of the Site, Site geology and
hydrogeology and site associated PFAS were provided in the Cape Fear River PFAS Mass
Loading Model Scope of Work document (Geosyntec, 2019a). The recent investigation
summarized in the Seeps and Creeks Investigation Report (Geosyntec 2019b) also provided
additional details on the site geology and hydrogeology. A brief summary of the Conceptual Site
Model (CSM), as it relates to PFAS loading to the Cape Fear River, and potential transport
pathways of PFAS from the Site to the Cape Fear River are summarized here.
The land surface is relatively flat in the manufacturing areas of the Site and slopes down a bluff
with about a 100-foot change in elevation towards the Cape Fear River on the east side of the Site.
To the north of the Site, the property slopes towards Willis Creek, which is a tributary that
discharges to the Cape Fear River. To the south of the manufacturing area is the Old Outfall
Channel, which also discharges to the Cape Fear River. Further south, off the Site, is Georgia
Branch Creek which is a tributary to the Cape Fear River.
Site Geology
As described by Parsons (2018), Bladen County is within the Coastal Plain Physiographic
Province, which consists of a seaward thickening wedge of sedimentary deposits ranging in age
from Cretaceous to Recent. Paleozoic metamorphic and igneous rocks underlie these deposits. The
Site is underlain by the Black Creek Formation, which is characterized by lignitic clay with thin
beds and laminae of fine-grained micaceous sand as well as thick lenses of cross-bedded sand. The
upper portion of the formation may also contain glauconitic, fossiliferous clayey sand lenses. The
Black Creek Formation and surficial deposits are the principal potable water aquifers in the region.
Based on the lithology logged during previous onsite investigations, the Site is underlain by a fine-
to medium-grained sand unit with thin discontinuous interbedded silt/clay lenses. The sand extends
to a depth of approximately 65 feet below ground surface (ft bgs) (elevation of +80 feet MSL).
The saturated portion of this unit has been identified as the Surficial Aquifer. Beneath this unit is
a 7- to 15-foot-thick, laterally-continuous dense clay that has been identified as the Black Creek
Confining Unit.
The elevation of this unit (approximately +65 to +77 ft MSL) indicates that it, too, should outcrop
along the bluff face adjacent to the Cape Fear River, and potentially along the embankment near
Willis Creek. Beneath this confining unit is the Black Creek Aquifer, which is approximately 8 to
20 ft thick and is encountered at depth between 80 and 100 ft bgs (elevation of approximately +45
to +65 ft MSL) at the top of the bluff. Beneath this aquifer is a massive dense clay (with minor

PFAS Mass Loading Model Assessment 5 August 26, 2019
sand stringers) that has been identified as the Upper Cape Fear Confining Unit. This unit was not
fully penetrated at the Site; however, it extended to at least 200 ft bgs (elevation of -55 ft MSL).
Beneath the manufacturing area, the uppermost sand unit is locally bisected by an aerially
extensive stiff clay lens. This clay lens is limited in lateral extent to the east, north and south by
local topography and pinches out (terminates) to the west of the manufacturing area. The depth to
the top of the clay lens is approximately 15 to 18 ft bgs. The clay lens becomes thinner moving
west across the manufacturing area and ranges from approximately one foot to approximately 19
ft thick.
Site Hydrogeology
The hydrogeology of the Site includes a perched water zone and two aquifers; the Perched Zone,
the Surficial Aquifer and the Black Creek Aquifer.
The Perched Zone is aerially limited and generally is located above the top of a discontinuous clay
layer present in the manufacturing area. Based on recent investigations and on-going evaluations,
the Perched Zone may have been influenced by seepage of surface water through the previously
unlined sedimentation basins and infiltration of non-contact cooling water from previously unlined
drainage ditches. In 2018, the sedimentation basins and cooling water channel were lined. Perched
zone water flows radially from a potentiometric high near the sedimentation basins. Where perched
water is present, it is encountered from between 6 to 20 feet bgs. The lateral extent of the Perched
Zone is controlled by topography and the lateral extent of the clay lens. The Seeps and Creeks
Investigation Report (Geosyntec 2019b) indicate seepage faces along the bluff appear to be
consistent with Perched Zone water.
The Surficial Aquifer is a shallow unconfined aquifer encountered at approximately 50 ft bgs.
Groundwater elevations range from approximately 100 to 107 ft above MSL in the western areas
of the Site to approximately 93 ft above MSL in the eastern areas of the Site, indicating that
groundwater flow is generally toward the Cape Fear River. The Cape Fear River stage is typically
near +30 ft MSL, which is lower than the base elevation of the Surficial Aquifer, indicating that
the Cape Fear River is a discharge boundary through seeps and creeks, for the Surficial Aquifer.
Based on groundwater elevations near Willis Creek, portions of the creek are “gaining”
(groundwater discharges to the creek) and portions are “losing” (surface water infiltrates to the
underlying groundwater). Georgia Branch Creek also appears to be a gaining stream near where
State Road 1303 crosses Highway 87.
The Surficial and Black Creek Aquifers are mostly separated by the Black Creek confining unit, a
clay layer. This clay layer is not fully confining as geological and geochemical data indicate water
and PFAS transfer has occurred from the Surficial Aquifer to the Black Creek Aquifer. The Black

PFAS Mass Loading Model Assessment 6 August 26, 2019
Creek Aquifer is the uppermost identified regional hydrogeologic unit. Flow in the Black Creek
Aquifer is toward the Cape Fear River. The Cape Fear River stage is also lower than the base of
the Black Creek Aquifer, indicating that the Cape Fear River is also a discharge boundary for the
Black Creek Aquifer.
Below the Black Creek Aquifer is the Upper Cape Fear Confining Unit. This clay is over 30-feet
(ft) thick and is an aquitard to potential further downward flow based on limited onsite geological
borings and United States Geological Survey (USGS) groundwater wells at the Site that
demonstrate minimal hydraulic connection between the Black Creek Aquifer and the Upper Cape
Fear Aquifer. The Black Creek Aquifer typically comprises of fine to medium grained, well sorted
sands and appears to be in direct connection to the Cape Fear River along the river bank. However,
the upper 20-25 feet of the Black Creek Aquifer near the Cape Fear River is overlain by fine
grained materials including silt to sandy and silty clay as noted in the Long-Term Well (LTW)
logs. This upper portion of the aquifer is likely to have lower groundwater upwelling to the Cape
Fear River in comparison to fine to medium grained, well sorted sands in the lower part of the
aquifer.
Historic borings and recent field investigations have shown that the Upper Cape Fear Confining
Unit, a regionally extensive lithologic unit comprising of hard, fat clay, underlies the Black Creek
Aquifer, at elevations similar to the Cape Fear River bottom. This unit was not fully penetrated at
the Site; however, it extended to at least 200 feet bgs (elevation of -55 feet MSL). This clay is over
34-feet (ft) thick and is an aquitard to potential further downward flow based on limited onsite
geological borings and USGS groundwater wells at the Site that demonstrate minimal hydraulic
connection between the Black Creek Aquifer and the Upper Cape Fear Aquifer.
Recent field investigations have identified that groundwater seeps to surface where the three
primary aquifer units onsite intersect the side of the bluff slope below the facility (Geosyntec,
2019b). The groundwater seeps out and flows towards the Cape Fear River in a series of naturally
occurring erosional channels. These channels have been observed to contain a steady flow of water
where they intersect groundwater. These channels and the water that flows in them are herein
referred to as Seeps. The four seeps observed on the eastern bluff adjacent to the Cape Fear River
from north to south are named Seep A, Seep B, Seep C and Seep D (Figure 2).
In addition to the onsite seeps, there are three perennial surface water features that are tributaries
to the Cape Fear River at or adjacent to the Site. To the north of the Site is Willis Creek, in
proximity to the water intake for the Site. To the south of the Site is Georgia Branch Creek which
discharges to the Cape Fear River approximately 7,500 feet south of the W.O. Huske Dam. Old
Outfall 002 is fed by discharging groundwater and Old Outfall 002 discharges into the Cape Fear
River approximately 1,350 feet south of W.O. Huske Dam.

PFAS Mass Loading Model Assessment 7 August 26, 2019
3.2 Cape Fear River and Downstream Public Water Utility Intakes
The Cape Fear River and its entire watershed are located in the state of North Carolina (Figure 3).
The Cape Fear River drains 9,164 square miles and empties into the Atlantic Ocean near the City
of Wilmington, North Carolina. The Site is situated on the western bank of the Cape Fear River
and draws water from the Cape Fear River and returns over 95% of this water via Outfall 002 after
being used primarily as non-contact cooling water. Two lock and dam systems with USGS stream
gauges are located downstream of the Site: (1) W.O. Huske Lock and Dam, located 0.5 river miles
from the Site (USGS 02105500); and (2) Cape Fear Lock and Dam #1, located 55 river miles
downstream (USGS 02105769).
The Cape Fear River is also a water source for downstream communities of the Site. Raw water
intakes are located at Bladen Bluffs and Kings Bluff Intake Canal, located approximately 5 miles
and 55 miles downstream from the Site. These intakes serve as Cape Fear River water intakes for
the Lower Cape Fear Water and Sewer Authority which in turn provides water to Cape Fear Public
Utility Authority (CFPUA) and other water providers. Drinking water sourced from the Cape Fear
River does contain certain chemicals from several sources including 1,4-dioxane, trihalomethanes
associated with bromide content in raw river water, pharmaceuticals, personal care products,
endocrine disrupting chemicals, and PFAS. A brief description of these chemicals and their
presence in the Cape Fear River was reported previously (Geosyntec, 2018b).
3.3 Potential PFAS Transport Pathways to Cape Fear River
Potential pathways for PFAS originating from the Site that may reach the Cape Fear River were
identified by reviewing available Site data at the time of this assessment. Nine potential pathways
(Table 1) were identified as potentially contributing to observed in-river PFAS concentrations.
These pathways represent compartments to model as part of the PFAS loading model. The
potential pathways are listed below, and shown on the conceptual diagram provided in Figure 2:
Transport Pathway 1: Upstream Cape Fear River and Groundwater – This pathway is
comprised of contributions from non-Chemours related PFAS
sources on the Cape Fear River and tributaries upstream of the Site,
and upstream offsite groundwater with Table 3+ compounds present
from aerial deposition;
Transport Pathway 2: Willis Creek – Groundwater and stormwater discharge and aerial
deposition to Willis Creek and then to the Cape Fear River;
Transport Pathway 3: Direct aerial deposition of PFAS on the Cape Fear River;

PFAS Mass Loading Model Assessment 8 August 26, 2019
Transport Pathway 4: Outfall 002 – Comprised of (i) water drawn from the Cape Fear
River and used as non-contact cooling water, (ii) treated non-
Chemours process water and (iii) Site stormwater, which are then
discharged through Outfall 002;
Transport Pathway 5: Onsite Groundwater – Direct upwelling of site groundwater to the
Cape Fear River from the Black Creek Aquifer;
Transport Pathway 6: Seeps – Groundwater Seeps (currently identified seeps are A, B, C
and D) above the Cape Fear River water level on the bluff face from
the facility that discharge into the Cape Fear River;
Transport Pathway 7: Old Outfall 002 – Groundwater discharge to Old Outfall 002 and
stormwater runoff that flows into the Cape Fear River;
Transport Pathway 8: Adjacent and Downstream Groundwater – Offsite groundwater
adjacent and downstream of the Site upwelling to the Cape Fear
River; and,
Transport Pathway 9: Georgia Branch Creek – Groundwater, stormwater discharge and
aerial deposition to Georgia Branch Creek and then to the Cape Fear
River.

PFAS Mass Loading Model Assessment 9 August 26, 2019
4. PFAS MASS LOADING MODEL DESIGN
The objective of the model is to estimate total PFAS mass loading originating from the facility to
the Cape Fear River and estimate the percentage of mass loading coming from each transport
pathway in empirically measured PFAS mass loads in the river. The model is comprised of
multiple compartments that describe bulk PFAS mass transfer to the Cape Fear River. Each
compartment represents a pathway that has been parameterized primarily using measured data.
This approach is designed to identify broad trends in mass loading to the Cape Fear River for a
range of conditions and to support identification of potential target pathways for actions to achieve
objectives for mass load and corresponding concentration reductions of Site associated PFAS in
the Cape Fear River.
Site associated PFAS concentrations in the Cape Fear River are derived from the PFAS mass
loading to the Cape Fear River and the volume of water flowing through the Cape Fear River.
PFAS mass load entering the Cape Fear River is defined in this model as the combined mass per
unit time or mass load (e.g. nanograms per second) from potential pathways identified in Section
3.3 above. Total PFAS mass load entering the Cape Fear River is calculated as:
𝐶𝐶𝐶𝐶𝐶𝐶𝑇𝑇𝑀𝑀=
⎩⎪⎪⎪⎪⎪⎨⎪⎪⎪⎪⎪⎧��𝑀𝑀𝑛𝑛,𝑖𝑖𝑖𝑖=57
𝑖𝑖=1
𝑛𝑛=9
𝑛𝑛=1 =���𝐶𝐶𝑛𝑛,𝑖𝑖× 𝑄𝑄𝑛𝑛� ∶ 𝑄𝑄𝑛𝑛𝑖𝑖=57
𝑖𝑖=1 →𝑛𝑛=9
𝑛𝑛=1 𝑑𝑑𝑑𝑑𝑑𝑑 (𝐶𝐶𝐹𝐹𝐹𝐹𝑑𝑑𝐹𝐹𝐹𝐹𝑑𝑑𝑑𝑑 2019).
��𝑀𝑀𝑛𝑛,𝑖𝑖𝑖𝑖=57
𝑖𝑖=1
𝑛𝑛=9
𝑛𝑛=1 =���𝐶𝐶𝑛𝑛,𝑖𝑖× 𝑄𝑄𝑛𝑛� ∶ 𝑄𝑄𝑛𝑛𝑖𝑖=57
𝑖𝑖=1 →𝑛𝑛=9
𝑛𝑛=1 𝑑𝑑𝑑𝑑𝑑𝑑 (𝑀𝑀𝐹𝐹𝑑𝑑 2019).
��𝑀𝑀𝑛𝑛,𝑖𝑖𝑖𝑖=57
𝑖𝑖=1
𝑛𝑛=9
𝑛𝑛=1 =���𝐶𝐶𝑛𝑛,𝑖𝑖× 𝑄𝑄𝑛𝑛� ∶ 𝑄𝑄𝑛𝑛𝑖𝑖=57
𝑖𝑖=1 →𝑛𝑛=9
𝑛𝑛=1 𝑤𝑤𝐹𝐹𝑤𝑤 (𝐽𝐽𝐹𝐹𝐽𝐽𝐹𝐹 2019).

where,
CFRTM = total PFAS mass load entering the Cape Fear River measured in mass per unit time
[MT-1], typically nanograms per second.
n = represents each of the 9 potential PFAS transport pathways listed in Table 1. To facilitate
model construction, the Seeps (Transport Pathway 6) were further discretized as Seep A
(Transport Pathway 6A), Seep B (Transport Pathway 6B), Seep C (Transport Pathway 6C)
and Seep D (Transport Pathway 6D).

PFAS Mass Loading Model Assessment 10 August 26, 2019
i = represents each of the 57 PFAS constituents listed in Table 2.
Mn,i = mass load of each PFAS constituent i from each potential pathway n with measured
units in mass per unit time [MT-1], typically nanograms per second.
Cn,i = concentration of each PFAS constituent i from each potential pathway n with measured
units in mass per unit volume [ML-3], typically nanograms per liter.
Qn = volumetric flow rate from each potential pathway n with measured units in volume per
time [L3T-1], typically liters per second. Three flow conditions, two representing quiescent
(dry.) conditions in February 2019 and May 2019, and one storm (wet.) condition in June 2019
are used to compute total PFAS mass load entering the Cape Fear River.
The Site associated PFAS mass loading for each potential pathway is estimated using the
approaches described in the following sub-sections. These estimates are then used to calculate the
total PFAS mass loading of Site related PFAS using the above formula for each of the three discrete
flow conditions in February, May and June 2019. A similar analytical mass loading model was
previously developed for hexafluoropropylene oxide dimer acid (HFPO-DA) in February 2018
(Appendix A of Parsons, 2018a).
Model inputs for each potential pathway (i.e., PFAS concentrations and volumetric flow of water)
are a combination of measured data, calculations and professional judgement, as available at the
time of model development. Table 1 summarizes the transport pathways and the model input data
used for developing this model and is discussed further for each pathway below.
The mass loading pathways contributing to the Cape Fear River, as well as the Cape Fear River
itself, represent a complex and dynamic environment. To minimize temporal uncertainties in the
model, model input analytical samples and flow measurements were collected during three field
investigation programs conducted February 1-7, May 20-30 and June 4-7, 2019. Sample locations,
methods and results are described in detail in the Seeps and Creeks Investigation Report
(Geosyntec, 2019b). The Seeps and Creeks Investigation Report (Geosyntec, 2019b) characterizes
the February and May field programs as “dry weather” events representing baseflow conditions.
The June 2019 field program was characterized as a “wet weather” event since there was greater
than 0.25 inches of rain in the 72 hours prior to sample collection. These field program
characterizations are carried forward in this assessment.
Further, the model is computed assuming representative model input parameter scenarios that
encompass a meaningful range of observed values. The model input parameter scenarios discussed
here are used to apportion relative mass loading for each potential pathway and assess how the
variability in the possible set of input parameters chosen would affect results. The most
representative model input parameter scenario is selected based on a comparison of modeled and

PFAS Mass Loading Model Assessment 11 August 26, 2019
empirical mass loading observed at Bladen Bluffs in the Cape Fear River (Section 5). The five
model input scenarios for concentrations and flow are:
(1) Input parameters assuming 1st Quartile values for concentration and flow;
(2) Input parameters assuming median values for concentration and flow;
(3) Input parameters assuming 3rd Quartile values for concentration and flow;
(4) Input parameters assuming average values for concentration and flow; and,
(5) Input parameters assuming geometric mean values for concentration and flow.
For each of the three field investigation programs (February, May and June 2019) these model
input scenarios were used for this assessment. The following subsections describe how PFAS mass
loading from the different PFAS transport pathways listed in Table 1 are estimated in the model
and field work that was performed to support these estimations.
4.1 Upstream Cape Fear River (Transport Pathway 1)
The upstream PFAS mass loading contribution to Cape Fear River was estimated using measured
Cape Fear River PFAS concentration and flow rates as described below (and see Table 1).
Sampling locations, analytical methods and assessment techniques for PFAS concentrations in the
Cape Fear River are described in detail in the Seeps and Creeks Investigation Report (Geosyntec,
2019b). One water sample was collected immediately upstream of the Site and Willis Creek at
River Mile 76 to estimate upstream PFAS mass loading contribution to Cape Fear River. River
water samples were collected at the thalweg (i.e., deepest point of the river transect) at mid-depth
in the water column. As described in the Seeps and Creeks Investigation Report (Geosyntec,
2019b), additional upstream samples were collected at River Miles -56 and -68 but these were
determined to be too far upstream to be representative in this model. PFAS compound analytical
data for transport pathway 1 is included in Appendix A.
Volumetric flow rates for the Cape Fear River were measured at the USGS flow gauging station
located at the W.O. Huske Dam, ID (USGS# 02105500; USGS, 2019), approximately 0.5 river
miles downstream of the Site (Appendix B). Volumetric flow rate immediately upstream of the
Site (River Mile 76) was estimated using a volumetric budget accounting for flows between River
Mile 76 and the W.O. Huske Dam, as depicted in Figure 3. The volumetric flow rate at River Mile
76 was estimated by subtracting inflows from Willis Creek, upwelling groundwater, seeps to the
river, and Outfall 002 and by adding the river water intake from Chemours to the flow rate
measurement from the W.O. Huske Dam. Due to the short reach between upstream sample

PFAS Mass Loading Model Assessment 12 August 26, 2019
location and W.O. Huske Dam, the calculated upstream flow rate was similar (≤ ± 2%) to the
measured volumetric flow rate at W.O. Huske Dam during the period of sample collection.
4.2 Tributaries – Willis Creek, Georgia Branch Creek, and Old Outfall 002 (Transport
Pathways 2, 7 and 9)
Mass loading of PFAS from tributaries to the Cape Fear River used PFAS concentrations and creek
flow data (Table 1). Tributaries contributing to PFAS mass loading into the Cape Fear River
include Willis Creek, Georgia Branch Creek, and Old Outfall 002. PFAS samples were collected
at each tributary at a location near the discharge point to the Cape Fear River, but still far enough
upstream in the tributary where they are not potentially influenced by the Cape Fear River. Since
analytical sample locations were near the discharge point to the Cape Fear River, model input for
tributaries would account for loading from groundwater discharging to the tributary, onsite surface
water runoff into the tributary and direct aerial deposition on these tributaries. Analytical results
used in the model from each tributary are provided in Appendix A and summarized in Table 3.
Sample locations, methods and results are presented in the Seeps and Creeks Investigation Report
(Geosyntec, 2019b).
Volumetric discharge rates for the tributaries were obtained from three independent flow
measurement methods as outlined in the Seeps and Creeks Investigation Report (Geosyntec,
2019b). A summary of the measured and estimated flow values for all tributaries are provided in
Table 3 and Appendix B. Detailed methods and results of flow measurements are presented in the
Seeps and Creeks Investigation Report (Geosyntec, 2019b).
4.3 Aerial Deposition to the Cape Fear River (Transport Pathway 3)
The mass loading from direct aerial deposition of PFAS to the Cape Fear River was estimated
using air deposition modeling results for HFPO-DA from the Site (ERM, 2018). Average
deposition rates to the Cape Fear River were estimated based on the reported aerial extent and
deposition contours. Estimated deposition rates were combined with the average river surface area
and estimated residence time of flowing Cape Fear River water to estimate a mass loading from
aerial deposition. The mass loading of Table 3+ PFAS compounds was estimated by using the
relative concentration ratios of other Table 3+ PFAS to HFPO-DA based on measured
concentrations from offsite wells. Supporting documentation for this estimation is included in
Appendix C.
4.4 Onsite Groundwater (Transport Pathways 5 and 6)
Based on the current characterization of the Site CSM, there are two groundwater PFAS mass
loading pathways to the Cape Fear River. First, the indirect pathway of groundwater to seeps to

PFAS Mass Loading Model Assessment 13 August 26, 2019
river, and secondly, the direct pathway of Black Creek aquifer groundwater discharging directly
to the river.
4.4.1 Indirect Pathway – Groundwater Seeps to River (Transport Pathway 6)
Four seeps at the Site have been identified and these discharge directly to the Cape Fear River:
Seep A, Seep B, Seep C and Seep D (Figure 2). The PFAS mass loading from these seeps to the
Cape Fear River was estimated using measured PFAS concentrations) and flow values that are
reported in the Seeps and Creeks Investigation Report (Geosyntec, 2019b) and summarized in
Table 3 and Table 4, respectively. Flow rates and PFAS concentrations at Seep A, Seep B and
Seep C were measured in February, May and June 2019. Seep D was identified following the
February field event, so flow rates and PFAS concentrations were measured in May and June 2019.
4.4.2 Direct Pathway – Groundwater Discharge to River (Transport Pathway 5)
The PFAS mass loading of onsite groundwater discharge from the Black Creek Aquifer to the
Cape Fear River was developed using a forward assessment based on Darcy’s Law using
hydrogeological data as described in detail in Appendix D. The PFAS mass loading from onsite
groundwater discharge was estimated using groundwater concentration data from LTW wells at
the Cape Fear River bank (Appendix A) and estimated volumetric groundwater discharge
(Appendix D). Hydraulic parameters used in the calculation included: (1) hydraulic gradients from
measured LTW Well water level data and Cape Fear River water gauge heights reported from
USGS (USGS, 2019); (2) estimated representative discharge areas in contact with the Cape Fear
River; and (3) estimated hydraulic conductivities.
4.5 Outfall 002 and Facility Stormwater Runoff (Transport Pathway 4)
The mass loading of PFAS from Outfall 002 to the Cape Fear River was estimated using measured
PFAS concentrations and measured Outfall 002 volumetric flow rates. PFAS concentration data
used in the model were compiled from two datasets (Appendix A): (1) composite samples of
Outfall 002 water that Chemours collects each week for analysis for HFPO-DA and Table 3+
compounds, and (2) Outfall 002 water samples results reported in the Seeps and Creeks
Investigation Report (Geosyntec, 2019b). Comparison of Outfall 002 and river intake sample
PFAS concentrations show that all Environmental Protection Agency (EPA) Method 537 PFAS
compounds (Table 2) in the Outfall 002 were present in intake water from Cape Fear River and
did not originate from the Site (Appendix A) as water passed through the conveyance network.
These EPA 537 PFAS compounds were assigned zero concentrations for computing analytical
summary statistics (Table 3). Additionally, Table 3+ PFAS compounds for Outfall 002 were input
into the model after accounting for their contribution from the Cape Fear River. Daily volumetric
discharge from Outfall 002 to the Cape Fear River is recorded (Appendix B) and used in the PFAS

PFAS Mass Loading Model Assessment 14 August 26, 2019
Loading Model. These data capture water flowing through Outfall 002, including non-contact
cooling water, treated non-Chemours process wastewater (DuPont and Kuraray process water),
treated sanitary water and stormwater within the manufacturing area of the Site.
4.6 Offsite Groundwater (Transport Pathway 8)
The offsite groundwater PFAS mass loading contributions were estimated by separating offsite
discharging groundwater into different zones based on the distance of the selected area from the
Site. In each zone, the discharge mass loading was estimated using measured residential well
concentrations (Appendix A) and volumetric discharge rate estimated using Darcy’s Law
(Appendix E). A detailed description for estimating offsite groundwater mass loading is provided
in Appendix E.

PFAS Mass Loading Model Assessment 15 August 26, 2019
5. MODEL CALIBRATION AND SENSITIVITY ANALYSIS
The PFAS mass loading model was calibrated to help provide reasonable estimates of modeled
loading contributions to Cape Fear River. The sensitivity of the model to potential variability of
input parameters was assessed to understand the uncertainties in the model and identify parameters
that may influence PFAS mass loading to the Cape Fear River. Details of the calibration and
sensitivity procedures are described below.
5.1 Model Calibration
The mass loading model was calibrated by varying assumed input parameters to achieve a model-
estimated, total mass loading in the Cape Fear River generated from all pathways, that best fit with
empirical observed mass loading in the river. Empirical mass loading in the Cape Fear River was
computed at the Bladen Bluffs raw water intake, approximately 7 miles downstream of the Site
(River Mile 84) (Figure 3), to allow for both model calibration and characterization of PFAS at
downstream raw water intakes based on the mass loading model assessment. Mass loading at
Bladen Bluffs was computed using volumetric flow rates for the Cape Fear River measured at the
closest available USGS flow gauging station located at the W.O. Huske Dam and measured
analytical results from samples that were collected near the Bladen Bluffs raw water intake (Figure
3).
The mathematical summation of Table 3+ compounds (see Table 2 for a list of Table 3+
compounds) was used in the calibration process. The mass loading estimated from the May and
June 2019 field programs were included in the calibration since complete Table3+ analytical data
from February was not available at the time of this assessment as a final laboratory standard
operating protocol (SOP) had yet to be finalized.
The model was calibrated by adjusting estimated or measured parameters within ranges of reported
variabilities or reasonable uncertainties. Parameters that were calibrated were selected based on
the relative uncertainty in estimation of parameter, and the relative mass loading contribution of
the transport pathway on modeled loading to the river. Based on a review of model parameters,
the onsite and offsite groundwater flow parameters were identified for their relatively high
uncertainties in estimating mass loading. Other estimated parameters (e.g., aerial deposition
contribution) were evaluated as part of a sensitivity analysis described in Section 5.2.
Model calibration was performed by varying the onsite groundwater flow component and the
offsite groundwater flow component. The onsite groundwater flow component was varied through
(a) modification of the onsite groundwater discharge area; or (b) modification of assumed
hydraulic conductivity values for the upper and lower portions of the Black Creek Aquifer (see
Appendix D for a description of onsite groundwater flow calculations). The offsite groundwater

PFAS Mass Loading Model Assessment 16 August 26, 2019
flow component was varied through modification of assumed hydraulic conductivity values for
the Surficial Aquifer. Model parameters that were varied in the calibration process are indicated
in Table 5 and briefly described below.
While the original model assumed a conservative discharge area of 100% along the entire site-side
bank of the Cape Fear River (approximately 1 mile long), calibration iterations were performed by
assuming 40% to 75% of this area, limits estimated from available lithologic information. An
assessment of Cape Fear River bottom temperatures adjacent to the Site to identify potential zones
of groundwater upwelling has been recently completed to refine these estimates. Results from this
effort will be reported in the Comprehensive On- and Offsite Assessment Report pursuant to
Paragraph 18 of the Consent Order due September 30, 2019. Further, the assumed hydraulic
conductivity values for the upper and lower portions of the Black Creek Aquifer was varied
between 5x10-7 meters per second (m/s) to 1x10-6 m/s and 1x10-4 m/s to 2x10-4 m/s, respectively.
Offsite groundwater flow was varied by modifying the hydraulic conductivity values for the
Surficial Aquifer from 2.5 x 10-4 m/s, estimated for onsite surficial aquifer (Parsons, 2018b) to 1
x 10-6 m/s, a literature value assumed for silts and silty sands (Freeze and Cherry, 1979).
A total of 21 iterative calibration scenarios were performed to optimize the model-estimated total
Table 3+ mass loading in the Cape Fear River to obtain a best fit match to observed mass loading
at the Bladen Bluffs raw water intake for May and June 2019 field programs. For each calibration
iteration, the estimated total Table 3+ mass loading to the river was compared to empirical loading
at Bladen Bluffs, for the same sampling time period and assuming the five input parameter
scenarios discussed in Section 4 (1st quartile, median, 3rd quartile, average and geometric mean
values for concentration and flow) to assess how the variability in the possible set of input
parameters chosen would affect results. Calibrated model-fit was tested through computation of a
normalized root mean square error (NRMSE) between modeled and empirical mass loading (Table
5).
Calibration results indicate that a lower bound NRMSE of 0.16 was achieved assuming the 1st
quartile model input parameter values for nine calibration steps (steps 5, 6, 7, 8, 15, 16, 17, 19, 20;
Table 5). To identify a best-fit model amongst these nine calibrations steps, the lowest sum of
NRMSE between modeled and empirical mass loading for all five input parameter scenarios was
evaluated. Calibration results indicate that a best-fit model was achieved for calibration step 8
assuming the 1st quartile model input parameter values. Figure 4 presents the best-fit model
estimated mass loading assuming the 1st quartile model input parameter values with the observed,
empirical mass loading at Bladen Bluffs for the same (median, 3rd quartile, average and geometric
mean values for concentration and flow) overestimate the observed, empirical mass loading at
Bladen Bluffs for the same sampling time period (Table 5) and are not likely to be appropriate
model input metrics. The best-fit model identified in calibration step number 8 (Table 5) assumes

PFAS Mass Loading Model Assessment 17 August 26, 2019
the following 1st quartile model input parameter values: (a) onsite discharge area of 58%; (b) upper
Black Creek Aquifer hydraulic conductivity of 1x10-6 m/s; (c) lower Black Creek Aquifer
hydraulic conductivity of 1.5x10-4 m/s; and (d) offsite Surficial Aquifer hydraulic conductivity of
2.5x10-4 m/s. Mass loading model results from this best-fit and calibrated model are discussed in
the remainder of this report.
Ongoing field work, described in Section 7, is expected to refine some of the parameter estimates
discussed here, including refining discharge area estimates and hydraulic conductivity estimates.
This calibration iteration was limited to available analytical data collected from two discreet field
events in May and June of 2019. Calibration of this model will be an ongoing process that will
become more optimized with additional data.
5.2 Model Results
The estimated total Table 3+ PFAS loading, by transport pathway, as calculated from the calibrated
mass loading model is summarized in Table 6 and presented in Figure 5. The mass loading model
estimates that the Old Outfall 002 and Seeps (Transport Pathways 7 and 6 respectively) have the
highest contribution of Table 3+ PFAS mass loading to the Cape Fear River based on inputs from
both mass loading characterization events (May and June 2019). These two pathways (Transport
Pathways 7 and 6) combined contribute approximately 55% of the loading to the Cape Fear River.
Onsite groundwater (Transport Pathway 5) is the next highest mass loading pathway to the Cape
Fear River. Additional assessments and characterization of this component is currently being
undertaken as described in Section 7. A numerical groundwater model is also being prepared to
evaluate groundwater interactions with the Cape Fear River and to evaluate the efficacy and
support design of potential future actions.
The upstream river and groundwater (Transport Pathway 1) is the next highest mass load pathway
to the Cape Fear River (4% to 15%). A 10% difference in mass loading between the May and June
2019 characterization events is observed for the upstream river. For upstream river and all
Transport Pathways, the loading estimates will vary over time due to a range of possible reasons,
including:
• Detections of any PFAS at or near analytical practical quantitation limits have more
variability;
• Elevated method reporting limits; and
• Flow rate estimates are over- or under-predicted compared to actual flow rates.
Additionally, Transport Pathway 1 (Upstream river water and groundwater) may have additional variability due to the presence of three Table 3+ compounds, Byproduct 4, Byproduct 5 and perfluoroethoxysulfonic acid (NVHOS) which were observed in the upstream Cape Fear River

PFAS Mass Loading Model Assessment 18 August 26, 2019
sample collected in May and June 2019 at River Miles 56 and 68. The results for these compounds were J-qualified due to variable recoveries in the matrix spikes outside the acceptable range
defined in the SOP which may cause the results to be overestimated. The detection of these
compounds is not consistent with known transport pathways for PFAS originating from the facility. Specifically, in offsite groundwater, which is the transport pathway leading to upstream detections attributable to aerial emissions of PFAS from the facility, Perfluoro-2-methoxypropanoic acid (PMPA) is the compound detected at the highest concentrations based on
groundwater data reported in the Post Florence Report (Geosyntec, 2019d). Therefore, PMPA is
expected to be detected first amongst the PFAS potentially reaching the river from offsite groundwater in the upstream river samples. In samples from River Mile 56, only these three Table 3+ samples are detected. While closer to Site in the upstream river at River Mile 68 PMPA is detected consistent with expected trends from offsite groundwater. These observations of
Byproduct 4, Byproduct 5 and NVHOS will be further evaluated spatially and temporally through
additional sampling events in the Cape Fear River to further understand their concentration and distribution.
Outfall 002 (Transport Pathway 4) contributed 4% – 7% of the total Table 3+ mass load to the Cape Fear River in May and June 2019. Outfall 002 loading rates in 2019, integrating both dry and wet weather periods, are presently 8% lower than in calendar year 2018. This reduction is
potentially a result of various completed actions at the Site, including reduced air emissions. Loading at Outfall 002 is expected to continue a downward trajectory year over year. Outfall 002 is further discussed in the Assessment of HFPO-DA and PFMOAA in Outfall 002 Discharge and Evaluation of Potential Control Options (Geosyntec, 2019c).
Willis Creek and Georgia Branch Creek (Transport Pathways 2 and 9, respectively) are modeled
to contribute between 7% to 14% of the total Table 3+ mass load to the Cape Fear River in May
and June 2019. The variation seen in the mass loading contribution is likely due to the possible
reasons listed above. As noted in Section 7, additional wells are being installed adjacent to Willis
Creek and Georgia Branch Creek to monitor groundwater quality near these tributaries. Aerial
deposition and Offsite Groundwater (Transport Pathways 3 and 8, respectively) contributed less
than 0.5% of the total mass loading to the Cape Fear River in May and June 2019.
The mass loading model that has been developed can accurately simulate concentrations of PFAS
originating from the Site at downstream intakes over time as shown in Figure 6 for Kings Bluff
Intake Canal. This plot shows the measured concentrations of HFPO-DA from both raw and
finished water samples collected at Kings Bluff Intake Canal compared to modeled concentrations
estimated from the mass loading model. HFPO-DA was selected in this representation because of
its low detection limit and the availability of public data for the time period simulated. To simulate
the modeled time series, the model incorporated the twice weekly Outfall 002 sample
concentration results, measured Outfall 002 flow rates and Cape Fear River flow volumes; all other
loading parameters developed for the calibrated model were kept constant. This suggests that the

PFAS Mass Loading Model Assessment 19 August 26, 2019
model is also a useful predictive tool to understand the benefit of potential PFAS mass loading
reductions to river loads and concentrations.
5.3 Sensitivity Analysis
A sensitivity analysis was performed to assess potential uncertainties in modeled results,
specifically how the potential range of model input parameters values affects the estimated PFAS
mass loads in the Cape Fear River. Model input parameters for the following Transport Pathways
are included in the sensitivity analysis: (a) Aerial deposition rates on the Cape Fear River; (b) Flow
rates at Willis Creek, Georgia Branch, Old Outfall 002 and Seep A, Seep B, Seep C and Seep D;
(c) Onsite groundwater flow rates; and (d) Offsite groundwater discharge rates. For each test, one
of the above Transport Pathway inputs to the calibrated model is varied and the resulting model
estimated Total Table 3+ PFAS mass loading is compared with the original calibrated model Total
Table 3+ PFAS mass loading. Results of the sensitivity analyses are summarized in Appendix F
and described below for each of the Transport Pathways.
(a) Aerial deposition – Aerial deposition of PFAS directly on the Cape Fear River, identified as
Transport Pathway Number 3, is estimated using air deposition modeling results for HFPO-DA in
October 2018 as described in Appendix C (ERM, 2018). To test the sensitivity of the model to
variations in model inputs for this pathway, calculated HFPO-DA deposition on the Cape Fear River
was increased six-fold. However, this six-fold increase only resulted in less than 0.5% variation in
Total Table 3+ estimated mass loading, suggesting that the mass loading is not very sensitive to
variations in Transport Pathway model input.
(b) Flow rates at seeps and tributaries – Flow rates at Willis Creek were first decreased by 10% and 50
% and then increased by the same amount (Appendix F). This variation in flow rate input at Willis
Creek only resulted in less than 5% variation in estimated Total Table 3+ estimated mass loading,
suggesting that this pathway model input is not very sensitive. Flow rates at Seep A, Seep B, Seep C
and Seep D were varied by ±50%. A 50% reduction in seep flow yields less than 8 % decrease in
Total Table 3+ estimated mass loading, driven by sensitivity to flows at Seep A and Seep B. A
similar 50% increase in seep flow yields less than 14 % increase in Total Table 3+ estimated mass
loading, driven by sensitivity to flows at Seep A and Seep B. This suggests that Total Table 3+
estimated mass loading is likely moderately sensitive to seep flow input variations. Sensitivity of
Total Table 3+ estimated mass loading to flow rates at Old Outfall 002 were tested by varying measured
flow values by ±50% and +100%. A ±50% variation in flow at the Old Outfall 002 yields a 9% to
16% variation in Total Table 3+ estimated mass loading. A +100% variation in flow at the Old
Outfall 002 yields a 16% to 21% variation in Total Table 3+ estimated mass loading. These results
suggest that the estimated mass loading is moderately sensitive to Old Outfall 002 flow input
variations. Flow rates at Georgia Branch Creek were also varied ±50% to yield a ≤ 2% variation

PFAS Mass Loading Model Assessment 20 August 26, 2019
in Total Table 3+ estimated mass loading, suggesting that the mass loading is not very sensitive to
variations in Transport Pathway model input.
(c) Onsite groundwater flow – As discussed in Section 5, onsite groundwater model input parameters
were varied during the calibration process. Model sensitivity to onsite groundwater flow is evaluated
through adjusting the discharge area parameter (see also Appendix D and Appendix F). Results show
that a 35% increase in discharge area resulted in a 16% increase in Total Table 3+ estimated mass
loading. This suggests that the mass loading is moderately sensitive to variations in Transport
Pathway model input.
(d) Offsite groundwater flow - Model sensitivity to offsite groundwater flow is tested through variation
of the assumed hydraulic conductivity over two orders of magnitude (Appendix F). However, this large
variation in model input only resulted in less than 0.5% variation in Total Table 3+ estimated mass
loading, suggesting that the mass loading is not very sensitive to variations in Transport Pathway model
input.
In summary, the Total Table 3+ estimated mass loading appears to be most sensitive to flow rates at
the Seeps, Old Outfall 002 and onsite groundwater flux.
Additionally, the model sensitivity to variations in reported analytical concentrations that are close to
their practical quantitation limits was evaluated. A small increase in analytical concentrations close to
their practical quantitation limits, that may be attributable to natural variations or when considering
tolerance on QA recoveries, could lead to an analyte detection and additional mass loading. Mass
loading is likely to be appreciable in such a scenario for a pathway with a large flow component. The
upstream Cape Fear River sample location at River Mile 76, is chosen for this assessment because of
its large flow component and analytical results from this sample displayed a number of non-detects in
May (40 PFAS compounds non-detect) and June (37 PFAS compounds non-detect). Model sensitivity
is evaluated by calculating Total Table 3+ estimated mass loading for Transport Pathway 1, assuming
all analytical results lower than the detection limits (i.e., non-detect) values equal to their reporting
limit and comparing with the original model, which assumed non-detect values to be zero. Non-detect
values were not assumed equal to their reporting limit in the original model input because Total Table
3+ estimated mass loading from the model grossly overestimated the observed empirical Total Table
3+ mass loading at Bladen Bluffs raw water intake due to the large number of non-detects reported in
the model dataset. Comparison of Total Table 3+ estimated mass loading for Transport Pathway 1
suggests that assuming non-detect values to be equal to their reporting limit increases their pathway
contribution from 8% to 20%. While the upstream Cape Fear River sample at River Mile 76 maybe an
extreme sample due to the large number of analytes that were lower than the detection limits, it is
evident that the model can be highly sensitive to reported analytical concentrations that are close to
their method detection limits. Model sensitivity is likely to be larger as the analytical result gets closer
to the method detection limit. As analytical methods improve and detection limits get lower, the model
and inherent assumptions will likely need to be re-evaluated.

PFAS Mass Loading Model Assessment 21 August 26, 2019
6. LIMITATIONS AND ASSUMPTIONS
The mass loading model constructed, calibrated, and applied is a quantitative estimate of the
current understanding of the conceptual site model and transport pathways. It is based on
availability of data points, and thus in a complex and dynamic environment, there are unavoidable
uncertainties. The model was constructed based on discrete field-observations, which were then
interpolated to approximate conditions across the model domain and assumed to be representative
in between the measured points. This model is useful to identify distributions in mass loading to
the Cape Fear River for a range of conditions and support identification of potential target
pathways for actions to achieve objectives for mass loading and corresponding concentration
reductions of PFAS originating from the facility in the Cape Fear River.
This section summarizes the primary uncertainties associated with this model, the physical
characterization and potential impacts of the uncertainty.
• Model assessment was primarily developed with available analytical data from three
discrete events in 2019 (February, May and June). While seasonal or temporal trends may
be captured within these events, a larger input dataset to the model may improve model
calibration and its ability to predict mass loading in a dynamic and complex system such
as the Cape Fear River. Additional sampling of Seeps and Creeks is planned for, including
the installation of flumes to obtain more accurate flow measurements (Geosyntec, 2019b).
A numerical groundwater model is being developed and this may help constrain these
uncertainties.
• The groundwater mass loading pathway has much more uncertainty than other pathways
because it is based on measured concentrations and estimated flow values that have more
inherent variability. Groundwater flow is heterogenous, and hydraulic conductivity can
vary by orders of magnitude in the same aquifer. Consequently, this leads to a broader
uncertainty in groundwater discharge rates. A river bottom temperature field program has
been completed to assess if areas of onsite groundwater discharge can be identified.
• Offsite groundwater data is currently based on limited data from residential wells at the
time of this assessment. Estimates of additions of Table 3+ compounds from offsite
groundwater to the Cape Fear River could be refined with additional PFAS characterization
of the Cape Fear River as better analytical capabilities exist for Table 3+ than in June 2018
when the first regional river sampling program was implemented (Geosyntec, 2018b).

PFAS Mass Loading Model Assessment 22 August 26, 2019
7. SUPPLEMENTAL ACTIVITIES
Geosyntec recommends Chemours conduct additional assessment activities regarding the total
PFAS loading originating from the facility. These activities will generate additional data that will
support continued refinement of the mass loading model. These activities include:
• Completing six additional quarterly assessments of mass loading to the Cape Fear River.
Activities in these events will include sampling and flow gauging at the mouths of Seeps A
through D, Old Outfall 002, Outfall 002, Willis Creek, Georgia Branch Creek. Also, samples
will be collected upstream and downstream of the Site in the Cape Fear River;
• Conducting an assessment of Cape Fear River bottom sediment temperatures adjacent to the
Site to identify potential zones of increased groundwater upwelling. This will be reported in
the On and Offsite Assessment Report due on September 30, 2019;
• Conducting further site investigation and characterization activities, including the installation
of additional monitoring wells onsite to further delineate PFAS concentrations and geology.
Multiple wells have been installed as noted below to further assess hydrogeology and
groundwater PFAS concentrations. These wells will be reported in the On and Offsite
Assessment Report due on September 30, 2019.
o Fifteen additional wells installed adjacent to the Cape Fear River (six pre-existing wells);
o Two additional wells installed adjacent to Old Outfall 002 (ten wells were installed
adjacent to Old Outfall 002 as part of the PlumeStop™ pilot study (Parsons, 2019);
o One well installed adjacent to Willis Creek (four pre-existing wells); and
o Three wells installed adjacent to Georgia Branch Creek (no pre-existing wells).
• Characterizing further the geology and hydrogeology at 24 locations adjacent to the Cape Fear
River using hydraulic profiling and electrical conductivity (HPT/EC) tools. This
characterization will be reported in the On and Offsite Assessment Report due on September
30, 2019;
• Preparing a numerical model to evaluate groundwater flow conditions in the three water
bearing units at Site and evaluate groundwater interactions with the Cape Fear River, to assess
the efficacy and support design of potential future actions. This will be prepared to support the
Corrective Action Plan due December 31, 2019; and
• Installing 20 offsite monitoring wells to support further understanding of the horizontal and
vertical distribution of PFAS originating from the facility potentially present offsite. These
wells will be reported in the On and Offsite Assessment Report due on September 30, 2019.

PFAS Mass Loading Model Assessment 23 August 26, 2019

8. CONSENT ORDER PARAGRAPH 11.1 ANALYSIS
Pursuant to Paragraph 11.1 of the Consent Order, this analysis estimates the percentage of PFAS
loading detected at downriver raw water intakes as originating from Chemours, other, or unknown
sources. Specifically, the Consent Order requires:
Chemours shall submit an analysis to DEQ reporting contributions of PFAS
(including identification and mass loading of each PFAS) from the Facility to
the raw water intakes of downstream public water utilities.
To facilitate this analysis, Chemours collected samples from the Cape Fear River adjacent to the
Bladen Bluffs and Kings Bluff raw water intakes in May and June 2019 (Creeks and Seeps
Investigation; Geosyntec, 2019b) and analyzed these samples to quantitate PFAS by laboratory
methods Table 3+ and EPA 537. The total concentrations for these samples are presented in Tables
8A to 8D and in the intext table below along with the attribution of each compound to the three
identified categories of sources. These sources are as follows:
• PFAS Originating from the Site – This includes PFAS detected in the Cape Fear River that
were assessed to originally or directly have come from PFAS releases to the environment
at the Site and have reached the Cape Fear River via one of the nine transport pathways
described in Section 3.3;
• PFAS Originating from Other Sources – This includes PFAS detected in the Cape Fear
River that were assessed to come from sources other than the Site;
• PFAS Originating from Unknown Sources – This includes PFAS where the source may
potentially either be the facility or other sources, but with the presently available data, the
source type could not be determined.
On a total PFAS basis this analysis indicates that at the Bladen Bluffs and Kings Bluff raw water
intakes for the May and June 2019 sampling events, between 68% to 84% of PFAS quantitated
and detected originate from the Site (Figure 7). Meanwhile, for these quantitated and detected
compounds, between 13% and 29% originate from other sources and 2% to 3% originate from
unknown sources. Actions proposed by Chemours in the Reductions Plan (Geosyntec, 2019d) and
the upcoming Corrective Action Plan due on December 31, 2019 will reduce the total PFAS
loading to the Cape Fear River and significantly reduce the loading originating from the facility as
is described in the Reductions Plan.

PFAS Mass Loading Model Assessment 24 August 26, 2019

Location Samp-ling Event
Concentration (ng/L) Percentage (%)
Total Observed PFAS Concentra-tion (ng/L)
PFAS Originating from Facility
PFAS Originating from Other Sources
PFAS Originating from Unknown Sources
PFAS Originating from Facility
PFAS Originating from Other Sources
PFAS Originating from Unknown Sources
Bladen Bluffs
May-19 361 288 67 6 80% 19% 2%
Jun-19 188 478 89 16 82% 15% 3%
Kings Bluff
May-19 582 129 54 5 68% 29% 3%
Jun-19 600 507 77 17 84% 13% 3%
* Note, values may differ slightly from attached tables due to rounding of significant digits for table presentation.

8.1 Assessment Methodology
Observed PFAS mass loading at Bladen Bluffs and Kings Bluff raw water intakes were estimated
based on measured concentrations and flow rates during the May 2019 and June 2019
characterization events (Tables 7A and 7B). The contributions per PFAS compound and Transport
Pathway to the total mass loading for each of these events were estimated using (1) the percentage
of the total mass loading attributed to each Transport Pathway based on the outcome of the mass
loading model assessment and (2) the estimated source of PFAS origination per compound per
Transport Pathway (Tables 8A, 8B, 8C, and 8D).
The best-fit modeled mass loading for each Transport Pathway are presented for the May 2019
and June 2019 characterization events in Tables 9A and 9B, respectively. The subsequent
estimated percentage of each Transport Pathway to the mass loading are presented by compound
in Tables 10A and 10B for the May 2019 and June 2019 characterization events, respectively. The
observed PFAS mass loading at Bladen Bluffs and Kings Bluff were distributed to each Transport
Pathway based on these percentages.
Table 11 summarizes the estimated origination source of PFAS mass loading by compound and
Transport Pathway. Percentages of PFAS mass loading generated from the Site, Other sources, or
Unknown sources were estimated per compound and per Transport Pathway. The observed PFAS
mass loading from each Transport Pathway were distributed based on the source origination
percentages to estimate the portion of PFAS loading originating from the Site, Other, and
Unknown sources.

8.1.1 PFAS Compound Source Origination Assessment
The source origination assessment for each Transport Pathway was developed as described below.

PFAS Mass Loading Model Assessment 25 August 26, 2019
For Transport Pathway 1 (Upstream River): Table 3+ compounds were estimated to originate from
the Site with the exception of Byproduct 4, Byproduct 5 and NVHOS whose detection in upstream
river samples was not consistent with known loading pathways for PFAS originating from the Site.
The fraction of these compounds originating from the Site was calculated using June event Table
3+ data where the River Mile 76 concentrations of each of the three compounds were subtracted
from the River Mile 56 concentrations of each of the three compounds and then divided by the
River Mile 76 concentration. The remainder contribution was estimated to originate from
Unknown sources. All EPA 537 compounds were estimated to originate from Other sources.
For Transport Pathways 2, 5, 6, and 7 (Willis Creek, Onsite Groundwater, Seeps and Old Outfall
002: All Table 3+ compounds were estimated to originate from the Site. For the EPA 537
compounds, the percentage increase between the median Pathway concentration for all sampling
events and the median Upriver [Transport Pathway 1] concentration for all sampling events were
estimated to originate from the Site. If the Pathway median was not detected or less than the
Upriver concentration, then the contribution from the Site was estimated to be 0%. The remaining
EPA 537 compound percentages were estimated to originate from Other sources.
For Transport Pathway 3 (Aerial Deposition on River): All Table 3+ compounds were estimated
to originate from the Site. All EPA 537 compounds were estimated to originate from Other sources.
For Transport Pathway 4 (Outfall 002): All Table 3+ compounds and EPA 537 compounds were
estimated to originate from the Site. This Pathway only represents new loading introduced by the
Site to the river by Outfall 002 and does not account for any offsite loading.
For Transport Pathway 8 (Adjacent and Downstream Groundwater): All Table 3+ compounds
were estimated to originate from the Site. For the EPA 537 compounds, the percentage increase
between the estimated median offsite groundwater concentration and the median Upriver
[Transport Pathway 1] concentration for all sampling events was estimated to originate from
Unknown sources. If the estimated median offsite groundwater concentration was not detected or
less than the median Upriver concentration, then the Unknown portion was considered 0%. The
remaining EPA 537 compound percentages were estimated to originate from Other sources.
For Transport Pathway 9 (Georgia Branch Creek): All Table 3+ compounds were estimated to
originate from the Site. For the EPA 537 compounds, the percentage increase between the median
Pathway concentration for all sampling events and the median Upriver [Transport Pathway 1]
concentration for all sampling events was estimated to originate from Unknown sources. If the
median Pathway concentration was not detected or less than the median Upriver concentration,
then the Unknown portion was considered 0%. The remaining EPA 537 compound percentages
were estimated to originate from Other sources.

PFAS Mass Loading Model Assessment 26 August 2019
9. SUMMARY
A mass loading model was developed to inform a plan to reduce PFAS to the Cape Fear River
from the Chemours Fayetteville Works Site pursuant to Paragraph 12 of the executed CO dated 25
February 2019 among NCDEQ, Cape Fear River Watch, and Chemours. The objective of the
model is to identify which of the nine potential transport pathways, presently identified in the
CSM, contribute significant PFAS load, originating from the Site, to the Cape Fear River. This
objective is accomplished by estimating total PFAS mass loading originating from the facility to
the Cape Fear River, including estimates of loading from each of the potential transport pathways
identified, and comparing these estimates to empirically measured PFAS loading in the Cape Fear
River.
PFAS mass loading is defined, in this model, as the combined mass per unit time (e.g. nanograms
per second) from potential sources. The model estimates PFAS contributions from multiple
pathways (i.e. compartments), such as various creeks and groundwater, that have been
parameterized primarily using measured data (Geosyntec, 2019b), to estimate Cape Fear River
mass loading using measured Cape Fear River flow volumes. These estimated mass loading are
then compared to measured in-river mass loading as an assessment of model calibration. For each
calibration iteration, the estimated total Table 3+ mass loading to the river was compared to
empirical loading at Bladen Bluffs, for the same sampling time period (May and June 2019) and
five input parameter scenarios (1st quartile, median, 3rd quartile, average and geometric mean
values for concentration and flow). Five input parameter scenarios were chosen to assess how the
variability in the possible set of input parameters chosen would affect results and apportion relative
mass loading for each potential pathway. The most representative model input parameter scenario
is selected based on computation of a NRMSE between modeled and empirical mass loading
observed at Bladen Bluffs in the Cape Fear River. The best-fit model identified in calibration
assumes the following 1st quartile model input parameter values: (a) onsite discharge area of 58%;
(b) upper Black Creek Aquifer hydraulic conductivity of 1x10-6 m/s; (c) lower Black Creek
Aquifer hydraulic conductivity of 1.5x10-4 m/s; and (d) offsite Surficial Aquifer hydraulic
conductivity of 2.5x10-4 m/s.
The mass loading model estimates that the Old Outfall 002 and Seeps (Transport Pathways 7 and
6 respectively) have the highest contribution of approximately 53% to 55% of the Table 3+ PFAS
mass loading to the Cape Fear River based on inputs from both mass loading characterization
events (May and June 2019). Onsite groundwater (Transport Pathway 5) is the next highest mass
loading pathway to the Cape Fear River between 17% and 22%. Additional assessments and
characterization of onsite groundwater is currently being undertaken. A numerical groundwater
model is also being prepared to evaluate groundwater interactions with the Cape Fear River and to
evaluate the efficacy and support design of potential future actions. Additionally, six more

PFAS Mass Loading Model Assessment 27 August 2019
quarterly field events evaluating mass loading to the river will be used to assess and refine these
mass loading findings over time and in different weather and season conditions.
An assessment of PFAS loading at downriver raw water intakes was performed pursuant to
Paragraph 11.1 of the Consent Order, using a combination of mass loading model assessment
results and observed PFAS concentrations at Raw Water Intake. An estimate of the percentage of
PFAS loading at downriver raw water intakes as originating from the Site, other sources or at
present unknown sources which could be either the facility or the other sources was evaluated. On
a total PFAS basis, this analysis indicated that at Bladen Bluffs and Kings Bluff raw water intakes
for the May and June 2019 sampling events, between 68% to 84% of PFAS may have originated
from the Site. Meanwhile for these quantitated and detected compounds between 13% to 29%
originate from other sources and 2% to 3% originate from unknown sources. Actions proposed by
Chemours in the Reduction Plan (Geosyntec, 2019d) and the upcoming Corrective Action Plan
due on December 31, 2019 will reduce the total PFAS loading to the Cape Fear River and
significantly reduce the loading originating from the facility as is described in the Reduction Plan.
The mass loading model constructed, calibrated, and applied is a quantitative estimate of the
current understanding of the conceptual site model and transport pathways. It is based on
availability of data points, and thus in a complex and dynamic environment, there are unavoidable
uncertainties. The model was constructed based on discrete field-observations, which were then
interpolated to approximate conditions across the model domain and assumed to be representative
in between the measured points. This model is useful to identify trends in mass loading to the
Cape Fear River for a discreet range of conditions and support identification of potential target
pathways for actions to achieve objectives for mass loading and corresponding concentration
reductions of Site associated PFAS in the Cape Fear River.

PFAS Mass Loading Model Assessment 28 August 2019
10. REFERENCES
ERM, 2018. Modeling Report: HFPO-DA Atmospheric Deposition and Screening Groundwater
Effects. 27 April 2018.
Freeze, R. A. and J. A. Cherry. 1979. Groundwater, Prentice Hall, Englewood Cliffs, N.J.
Geosyntec, 2018a. Assessment of Impact of Current and Anticipated Reduced Air Emissions on
Groundwater Concentrations of HFPO Dimer Acid in the Vicinity of the Chemours
Fayetteville Works. 27 April 2018.
Geosyntec, 2018b. Assessment of the Chemical and Spatial Distribution of PFAS in the Cape Fear
River. Chemours Fayetteville Works. 17 September 2018.
Geosyntec, 2019a. Cape Fear River PFAS Mass Loading Model Scope of Work. Chemours
Fayetteville Works. 12 April 2019.
Geosyntec, 2019b. Seeps and Creeks Investigation Report. Chemours Fayetteville Works. 26
August 2019.
Geosyntec, 2019c. Assessment of HFPO-DA and PFMOAA in Outfall 002 Discharge and
Evaluation of Potential Control Options. Chemours Fayetteville Works. 26 August 2019.
Geosyntec, 2019d. Post Hurricane Florence PFAS Characterization. Chemours Fayetteville
Works. April 2019
Parsons, 2018. Additional Site Investigation Report. 30 March 2018.
Parsons, 2019. Old Outfall 002 Remedial Options Plan. Chemours Fayetteville Works. May 2019.
USGS, 2019. National Water Information System: Web Interface. Accessed March 2019.
https://waterdata.usgs.gov/nwis/uv?site_no=02105500

TABLES
TABLE 1
PFAS MASS LOADING MODEL POTENTIAL PATHWAYS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
Transport
Pathway
Number
Potential PFAS Transport Pathway Analytical Data Source for Mass Loading Model1 Flow Data Source for Mass Loading Model1
1 Upstream River and Groundwater Measured from Cape Fear River samples collected in February, May, and June
2019 as reported in Seeps and Creeks Investigation Report2.
Measured flow rates from USGS gauging station at W.O. Huske Dam
during February, May and June 2019 volumetrically adjusted for flow
pathways between River Mile 76 and W.O. Huske Dam3.
2 Willis Creek Measured from Willis Creek samples collected in February, May, and June 2019
as reported in Seeps and Creeks Investigation Report2.
Measured flow rates through salt dilution tests, weir gauging and point
velocity methods during February, May and June 2019 as reported in
Seeps and Creeks Investigation Report2.
3 Aerial Deposition on River Estimated from air deposition modeling4.Estimated from air deposition modeling4.
4 Outfall 002 Measured from Outfall 002 samples collected in February, May, and June 2019
as reported in Seeps and Creeks Investigation Report2.Measured daily Outfall 002 flow rates.
5 Onsite Groundwater Measured from LTW well samples in October and November 2018, reported in
Post Florence Report5.
Estimated from calculated hydraulic gradients based on June 2019 water
levels and hydraulic conductivities of LTW wells from slug tests
performed in 2019. Supporting calculations provided in Appendix C.
6 Seeps Measured from Seeps A, B, C, and D samples collected in February, May, and
June 2019 as reported in Seeps and Creeks Investigation Report2.
Measured flow rates through salt dilution tests, weir gauging and point
velocity methods during February, May and June 2019 as reported in
Seeps and Creeks Investigation Report2.
7 Old Outfall 002 Measured from Old Outfall 002 samples collected in February, May, and June
2019 as reported in Seeps and Creeks Investigation Report2.
Measured flow rates through salt dilution tests, weir gauging and point
velocity methods during February, May and June 2019 as reported in
Seeps and Creeks Investigation Report2.
8 Adjacent and Downstream Groundwater Estimated from residential well samples collected between September 2017 and
April 2019. Supporting calculations provided in Appendix D.
Estimated from calculated hydraulic gradients based on June 2019 water
levels and calculated hydraulic conductivities of LTW wells from slug
tests performed in 2019. Supporting calculations provided in Appendix D.
9 Georgia Branch Creek Measured from Georgia Branch Creek samples collected in May, and June 2019
as reported in Seeps and Creeks Investigation Report2.
Measured flow rates through salt dilution tests, weir gauging and point
velocity methods during February, May and June 2019 as reported in
Seeps and Creeks Investigation Report2.
Notes
1. Flow and concentration data are multiplied together to estimate the PFAS mass load in the Cape Fear River originating from each pathway.
2. Seeps and Creeks Investigation Report, Geosyntec, 2019.
3. Cape Fear River flow rates measured at USGS gauging station #02105500 located at William O Huske Lock & Dam accessed from https://waterdata.usgs.gov on 2019-07-12 23:42:42 EDT.
4. ERM, 2018. Modeling Report: HFPO-DA Atmospheric Deposition and Screening Groundwater Effects. 27 April 2018.
5. Post Hurricane Florence PFAS Characterization Report, Geosyntec 2019.
August 2019
TABLE 2
ANALYTICAL METHODS AND ANALYTE LIST
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
Analytical Method Common Name Chemical Name CASN Chemical Formula
HFPO-DA Hexafluoropropylene oxide dimer acid 13252-13-6 C6HF11O3
PEPA Perfluoroethoxypropyl
carboxylic acid 267239-61-2 C5HF9O3
PFECA-G Perfluoro-4-isopropoxybutanoic acid 801212-59-9 C12H9F9O3S
PFMOAA Perfluoro-2-methoxyacetic acid 674-13-5 C3HF5O3
PFO2HxA Perfluoro(3,5-dioxahexanoic) acid 39492-88-1 C4HF7O4
PFO3OA Perfluoro(3,5,7-trioxaoctanoic)
acid 39492-89-2 C5HF9O5
PFO4DA Perfluoro(3,5,7,9-tetraoxadecanoic)
acid 39492-90-5 C6HF11O6
PMPA 2,3,3,3-Tetrafluoro-2-(trifluoromethoxy)propanoic 13140-29-9 C4HF7O3
Hydro-EVE Acid Hydro-EVE Acid 773804-62-9 C8H2F14O4
EVE Acid Perfluoroethoxypropionic
acid 69087-46-3 C8HF13O4
PFECA B Perfluoro-3,6-dioxaheptanoic acid 151772-58-6 C5HF9O4
R-EVE R-EVE EVS1428 C8H2F12O5
PFO5DA Perfluoro-3,5,7,9,11-
pentaoxadodecanoic acid 39492-91-6 C7HF13O7
Byproduct 4 Byproduct 4 EVS1429 C7H2F12O6S
Byproduct 5 Byproduct 6 EVS1430 C6H2F12O4S
Byproduct 6 Byproduct 5 EVS1431 C7H3F11O7S
NVHOS NVHOS 1132933-86-8 C4H2F8O4S
PES PES 113507-82-7 C4HF9O4S
PFESA-BP1 PFESA-BP1 29311-67-9 C7HF13O5S
PFESA-BP2 PFESA-BP2 749836-20-2 C7H2F14O5S
PFBA Perfluorobutanoic acid 375-22-4 C4HF7O2
PFDA Perfluorodecanoic acid 335-76-2 C10HF19O2
PFDoA Perfluorododecanoic acid 307-55-1 C12HF23O2
PFHpA Perfluoroheptanoic acid 375-85-9 C7HF13O2
PFNA Perfluorononanoic acid 375-95-1 C9HF17O2
PFOA Perfluorooctanoic acid 335-67-1 C8HF15O
PFHxA Perfluorohexanoic acid 307-24-4 C6HF11O2
PFPeA Perfluoropentanoic acid 2706-90-3 C5HF9O2
PFTeA Perfluorotetradecanoic acid 376-06-7 C14HF27O2
PFTriA Perfluorotridecanoic acid 72629-94-8 C13HF25O2
PFUnA Perfluoroundecanoic acid 2058-94-8 C11HF21O2
PFBS Perfluorobutanesulfonate 375-73-5 C4HF9SO
PFDS Perfluorodecanesulfonate 335-77-3 C10HF21O3S
PFHpS Perfluoroheptanesulfonic acid 375-92-8 C7HF15O3S
PFHxS Perfluorohexanesulfonic acid 355-46-4 C6HF13SO3
PFNS Perfluorononanesulfonate 68259-12-1 C9HF19O3S
PFOS Perfluorosulfonic acid 1763-23-1 C8HF17SO3
PFPeS Perfluoropentane sulfonic acid 2706-91-4 C5HF11O3S
10:2 FTS Fluorotelomer sulfonate 10:2 120226-60-0 C12H5F21O3
4:2 FTS Fluorotelomer sulfonate 4:2 757124-72-4 C6H5F9O3S
6:2 FTS Fluorotelomer sulfonate 6:2 27619-97-2 C8H5F13SO3
8:2 FTS Fluorotelomer sulfonate 8:2 39108-34-4 C10H5F17O3S
NEtFOSAA N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 C12H8F17NO4S
NEtPFOSA N-ethylperfluoro-1-octanesulfonamide 4151-50-2 C10H6F17NO2S
NEtPFOSAE N-ethyl perfluorooctane sulphonamidoethanol 1691-99-2 C12H10F17NO3S
NMeFOSAA N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 C11H6F17NO4S
NMePFOSA N-methyl perfluoro-1-octanesulfonamide 31506-32-8 C9H4F17NO2S
NMePFOSAE N-methyl perfluorooctane sulfonamidoethanol 24448-09-7 C11H8F17NO3S
PFDOS Perfluorododecanesulfonic acid 79780-39-5 C12HF25O3S
PFHxDA Perfluorohexadecanoic acid 67905-19-5 C16HF31O2
PFODA Perfluorooctadecanoic acid 16517-11-6 C18HF35O2
PFOSA Perfluorooctane Sulfonamide 754-91-6 C8H2F17NO2S
F-53B Major F-53B Major 73606-19-6 C8HClF16O4S
F-53B Minor F-53B Minor 83329-89-9 C10HClF20O4S
ADONA 4,8-dioxa-3H-perfluorononanoate 958445-44-8 C7H2F12O4
NaDONA NaDONA EVS1361 --
DONA DONA 919005-14-4 --
Notes:
1. Abbreviations:
EPA - Environmental Protection Agency
ng/L - nanograms per liter
PFAS - Per- and Polyfluoroalkyl substances
SOP - Standard Operating Procedure
Table 3+ Lab SOP
EPA Method 537 Mod
August 2019
TABLE 3
SUMMARY OF ANALYTICAL RESULTS – TOTAL PFAS AND TOTAL TABLE 3+
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
Transport Pathway
Number
Potential PFAS Transport
Pathway Common Name Sampling Event 1st Quartile
Concentration
(ng/L)
Median Concentration
(ng/L)
3rd Quartile
Concentration
(ng/L)
Average
Concentration
(ng/L)
Geometric Mean
Concentration
(ng/L)
Total Table 3+Surface Water 02/19 2.9 2.9 2.9 2.9 2.9
Total PFAS Surface Water 02/19 31.7 31.7 31.7 31.7 31.7
Total Table 3+Surface Water 05/19 12.8 12.8 12.8 12.8 12.8
Total PFAS Surface Water 05/19 67.1 67.1 67.1 67.1 67.1
Total Table 3+Surface Water 06/19 69.6 69.6 69.6 69.6 69.6
Total PFAS Surface Water 06/19 162.7 162.7 162.7 162.7 162.7
Total Table 3+Surface Water 02/19 2,048.5 2,260.0 2,471.5 2,260.0 2,163.6
Total PFAS Surface Water 02/19 2,075.0 2,286.5 2,498.0 2,286.5 2,190.1
Total Table 3+Surface Water 05/19 5,751.5 6,579.0 7,406.5 6,579.0 6,217.7
Total PFAS Surface Water 05/19 5,799.5 6,627.0 7,454.5 6,627.0 6,265.7
Total Table 3+Surface Water 06/19 2,692.4 2,692.4 2,692.4 2,692.4 2,692.4
Total PFAS Surface Water 06/19 2,732.9 2,732.9 2,732.9 2,732.9 2,732.9
Total Table 3+Surface Water 02/19 26.4 26.4 26.9 26.7 26.7
Total PFAS Surface Water 02/19 26.4 26.4 26.9 26.7 26.7
Total Table 3+Surface Water 05/19 357.2 594.7 832.3 594.7 318.3
Total PFAS Surface Water 05/19 357.2 594.7 832.3 594.7 318.3
Total Table 3+Surface Water 06/19 798.7 973.4 1,696.0 1,338.6 1,046.2
Total PFAS Surface Water 06/19 798.7 973.4 1,696.0 1,338.6 1,046.2
Total Table 3+Surface Water 02/19 203,062.0 213,337.0 223,612.0 213,337.0 211,983.3
Total PFAS Surface Water 02/19 204,040.6 214,315.6 224,590.6 214,315.6 212,961.9
Total Table 3+Surface Water 05/19 297,520.5 300,574.0 302,574.0 299,871.7 299,679.2
Total PFAS Surface Water 05/19 298,792.3 301,875.8 303,877.9 301,154.9 300,961.8
Total Table 3+Surface Water 06/19 197,620.0 197,620.0 197,620.0 197,620.0 197,620.0
Total PFAS Surface Water 06/19 198,495.9 198,495.9 198,495.9 198,495.9 198,495.9
Total Table 3+Surface Water 02/19 345,036.5 347,829.0 350,621.5 347,829.0 347,662.8
Total PFAS Surface Water 02/19 347,462.5 350,255.0 353,047.5 350,255.0 350,088.8
Total Table 3+Surface Water 05/19 309,023.0 309,023.0 309,023.0 309,023.0 309,023.0
Total PFAS Surface Water 05/19 310,903.5 310,903.5 310,903.5 310,903.5 310,903.5
Total Table 3+Surface Water 06/19 338,288.0 338,288.0 338,288.0 338,288.0 338,288.0
Total PFAS Surface Water 06/19 340,652.0 340,652.0 340,652.0 340,652.0 340,652.0
Total Table 3+Surface Water 02/19 343,584.0 346,679.0 348,429.0 345,782.3 345,737.2
Total PFAS Surface Water 02/19 345,981.3 349,077.5 350,828.8 348,180.8 348,135.6
Total Table 3+Surface Water 05/19 347,669.0 347,669.0 347,669.0 347,669.0 347,669.0
Total PFAS Surface Water 05/19 350,121.4 350,121.4 350,121.4 350,121.4 350,121.4
Total Table 3+Surface Water 06/19 346,000.0 346,000.0 346,000.0 346,000.0 346,000.0
Total PFAS Surface Water 06/19 348,447.3 348,447.3 348,447.3 348,447.3 348,447.3
Total Table 3+Surface Water 02/19 NS NS NS NS NS
Total PFAS Surface Water 02/19 NS NS NS NS NS
Total Table 3+Surface Water 05/19 164,470.0 166,685.0 168,900.0 166,685.0 166,562.5
Total PFAS Surface Water 05/19 165,567.6 167,791.7 170,015.7 167,791.7 167,669.0
Total Table 3+Surface Water 06/19 155,467.0 155,467.0 155,467.0 155,467.0 155,467.0
Total PFAS Surface Water 06/19 156,629.9 156,629.9 156,629.9 156,629.9 156,629.9
Total Table 3+Surface Water 02/19 129,320.0 133,040.0 136,760.0 133,040.0 132,784.7
Total PFAS Surface Water 02/19 129,320.0 133,040.0 136,760.0 133,040.0 132,784.7
Total Table 3+Surface Water 05/19 112,930.0 112,930.0 112,930.0 112,930.0 112,930.0
Total PFAS Surface Water 05/19 113,249.5 113,249.5 113,249.5 113,249.5 113,249.5
Total Table 3+Surface Water 06/19 132,549.0 132,549.0 132,549.0 132,549.0 132,549.0
Total PFAS Surface Water 06/19 132,884.1 132,884.1 132,884.1 132,884.1 132,884.1
Total Table 3+Surface Water 02/19 NS NS NS NS NS
Total PFAS Surface Water 02/19 NS NS NS NS NS
Total Table 3+Surface Water 05/19 2,553.0 2,553.0 2,553.0 2,553.0 2,553.0
Total PFAS Surface Water 05/19 2,585.9 2,585.9 2,585.9 2,585.9 2,585.9
Total Table 3+Surface Water 06/19 2,517.7 2,517.7 2,517.7 2,517.7 2,517.7
Total PFAS Surface Water 06/19 2,547.7 2,547.7 2,547.7 2,547.7 2,547.7
Notes:
2. Supporting calculations for estimating PFAS concentrations for aerial deposition (transport pathway 3), onsite groundwater (transport pathway 5) and offsite groundwater (transport pathway 8) are provided in Appendices C, D and E.
3. Abbreviations:
ng/L - nanograms per liter
PFAS - Per- and Polyfluoroalkyl substances
NS - Samples not collected during corresponding sampling event.
1. Total Table 3+ and Total PFAS computed as sum of analytical results for PFAS compounds listed in Table 1, assuming non-detected samples as zero concentrations. Summary statistics for all PFAS compounds listed in Table 1 and additional supporting
data provided in Appendix A.
Upstream River and
Groundwater
Willis Creek
Outfall 002
1
2
4
Seep A6A
Seep B6B
Seep C6C
Seep D6D
Old Outfall 0027
Georgia Branch Creek9
August 2019
TABLE 4
SUMMARY OF FLOW RATE INPUT VALUES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
Transport
Pathway
Number7
Potential PFAS Transport Pathway Sampling Event1 1st Quartile Flow
(L/s)
Median Flow
(L/s)
3rd Quartile Flow
(L/s)
Average Flow
(L/s)
Geometric Mean
Flow
(L/s)
Surface Water 02/19 138,093 163,837 182,346 170,893 165,672
Surface Water 05/19 33,559 38,348 44,407 39,974 39,267
Surface Water 06/19 26,847 29,472 32,248 29,625 29,488
Surface Water 02/19 183 184 186 184 184
Surface Water 05/19 ok, thanks 184 184 184 184
Surface Water 06/19 184 184 184 184 184
Surface Water 02/19 813 836 871 868 863
Surface Water 05/19 1,052 1,082 1,106 1,082 1,081
Surface Water 06/19 1,151 1,173 1,197 1,175 1,174
Surface Water 02/19 19 21 28 23 23
Surface Water 05/19 20 22 28 25 24
Surface Water 06/19 19 21 28 23 23
Surface Water 02/19 4 4 4 4 4
Surface Water 05/19 3 4 4 3 3
Surface Water 06/19 7 7 7 7 7
Surface Water 02/19 5 6 6 6 6
Surface Water 05/19 5 6 6 6 6
Surface Water 06/19 3 3 3 3 3
Surface Water 02/19 1 1 1 1 1
Surface Water 05/19 1 1 1 1 1
Surface Water 06/19 1 1 1 1 1
Surface Water 02/19 3 3 3 3 3
Surface Water 05/19 3 3 3 3 3
Surface Water 06/19 3 3 3 3 3
Surface Water 02/19 24 27 36 33 31
Surface Water 05/19 21 24 42 30 28
Surface Water 06/19 28 31 32 29 29
Surface Water 02/19 568 724 962 788 761
Surface Water 05/19 568 724 962 788 761
Surface Water 06/19 568 724 962 788 761
Surface Water 02/19 153 154 154 154 154
Surface Water 05/19 153 154 154 154 154
Surface Water 06/19 161 162 165 162 161
Notes:
2. Flow summary statistics not computed where only minimum and maximum flow values reported in Seeps and Creeks Investigation Report (Geosyntec, 2019).
8. Abbreviations:
L/s - liter per second
NA - not applicable.
7. Supporting calculations for estimating PFAS concentrations for aerial deposition (transport pathway 3), onsite groundwater (transport pathway 5) and offsite groundwater (transport pathway 8) are
provided in Appendices C, D and E.
6. Flows at Seep D were not measured in February and May 2019; measurements from June 2019 were used.
Outfall 0024
Onsite Groundwater
Upstream River and Groundwater31
Willis Creek2
5
Seep A6A
Seep B
Seep C6C
6B
Seep D66D
Old Outfall 0027
5. Offsite groundwater estimated from calculated hydraulic gradients based on June 2019 water levels and calculated hydraulic conductivities of LTW wells from slug tests performed in 2019.
Supporting calculations provided in Appendix D.
Georgia Branch Creek9
Adjacent and Downstream
Groundwater8
1. Sampling Event "Surface Water 02/19", "Surface Water 05/19" and "Surface Water 06/19" reported in Seeps and Creeks Investigation Report (Geosyntec, 2019). "Surface Water 02/19" performed
February 1 - 7, 2019; "Surface Water 05/19" performed May 20 - 30, 2019; "Surface Water 06/19" performed June 4 - 7, 2019.
3. Upstream river flow computed from measured flow rates from USGS gauging station at W.O. Huske Dam during February, May and June 2019 volumetrically adjusted for inflow/outflow from flow
pathways 2 - 9 that occur between River Mile 76 (upstream sampling point) and W.O. Huske Dam.
4. Onsite groundwater estimated from calculated hydraulic gradients based on June 2019 water levels and hydraulic conductivities of Long-Term Wells (LTW) from slug tests performed in 2019.
Supporting calculations provided in Appendix C.
August 2019
TABLE 5
MODEL ESTIMATED TOTAL TABLE 3+ MASS LOADING CALIBRATION
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
Model Observed
May-19 Average 14.09 11.85 No changes made.
Jun-19 Average 15.86 14.83 Model input parameters:
May-19 Geomean 12.55 11.64 Upper Black Creek Aquifer Hydraulic Conductivity = 1 x 10-6 m/s;
Jun-19 Geomean 14.56 14.76 Lower Black Creek Aquifer Hydraulic Conductivity = 1.5 x 10-4 m/s;
May-19 Median 12.39 11.37 Groundwater discharge length = 52%;
Jun-19 Median 14.60 14.75 Offsite gradient adjustment factor = 0.475.
May-19 Q1 9.99 9.96
Jun-19 Q1 12.37 13.45
May-19 Q3 18.06 13.15
Jun-19 Q3 18.83 16.13
May-19 Average 12.71 11.85 Changed groundwater discharge length from 52% to 41%.
Jun-19 Average 14.48 14.83
May-19 Geomean 11.39 11.64 Model input parameters:
Jun-19 Geomean 13.39 14.76 Upper Black Creek Aquifer Hydraulic Conductivity = 1 x 10-6 m/s;
May-19 Median 11.22 11.37 Lower Black Creek Aquifer Hydraulic Conductivity = 1.5 x 10-4 m/s;
Jun-19 Median 13.43 14.75 Groundwater discharge length = 41%;
May-19 Q1 9.29 9.96 Offsite gradient adjustment factor = 0.475.
Jun-19 Q1 11.67 13.45
May-19 Q3 16.16 13.15
Jun-19 Q3 16.93 16.13
May-19 Average 17.10 11.85 Changed groundwater discharge length from 41% to 76%.
Jun-19 Average 18.87 14.83
May-19 Geomean 15.09 11.64 Model input parameters:
Jun-19 Geomean 17.09 14.76 Upper Black Creek Aquifer Hydraulic Conductivity = 1 x 10-6 m/s;
May-19 Median 14.94 11.37 Lower Black Creek Aquifer Hydraulic Conductivity = 1.5 x 10-4 m/s;
Jun-19 Median 17.15 14.75 Groundwater discharge length = 76%;
May-19 Q1 11.53 9.96 Offsite gradient adjustment factor = 0.475.
Jun-19 Q1 13.91 13.45
May-19 Q3 22.21 13.15
Jun-19 Q3 22.97 16.13
May-19 Average 15.47 11.85 Changed groundwater discharge from 76% to 63%.
Jun-19 Average 17.24 14.83
May-19 Geomean 13.71 11.64 Model input parameters:
Jun-19 Geomean 15.72 14.76 Upper Black Creek Aquifer Hydraulic Conductivity = 1 x 10-6 m/s;
May-19 Median 13.56 11.37 Lower Black Creek Aquifer Hydraulic Conductivity = 1.5 x 10-4 m/s;
Jun-19 Median 15.77 14.75 Groundwater discharge length = 63%;
May-19 Q1 10.70 9.96 Offsite gradient adjustment factor = 0.475.
Jun-19 Q1 13.07 13.45
May-19 Q3 19.96 13.15
Jun-19 Q3 20.73 16.13
--
Description of changes CommentsScenario
0.59
0.21
0.22
Total Table 3+ Mass Loading
(mg/s)NRMSE
0.22
1.33
0
1
Calibration
Step Event Date
1.95
0.22
0.31
0.28
0.39
0.74
1.57
0.94
0.902
3
0.33
2.70
1.03
0.52
0.51
0.17
Improved NRMSE for
average, maximum,
minimum and 3rd quantile -
worsened for all other
metrics. Overall NRMSE not
lowest, continue calibration.
Improved NRMSE only for
minimum and 1st quartile.
Continue calibration.
Improved NRMSE for all
metrics except minimum and
1st quartile. Continue
calibration.
Page 1 of 6 August 2019
TABLE 5
MODEL ESTIMATED TOTAL TABLE 3+ MASS LOADING CALIBRATION
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
Model Observed
Description of changes CommentsScenario
Total Table 3+ Mass Loading
(mg/s)NRMSECalibration
Step Event Date
May-19 Average 14.71 11.85 Changed groundwater discharge from 63% to 57%.
Jun-19 Average 16.49 14.83
May-19 Geomean 13.08 11.64 Model input parameters:
Jun-19 Geomean 15.08 14.76 Upper Black Creek Aquifer Hydraulic Conductivity = 1 x 10-6 m/s;
May-19 Median 12.92 11.37 Lower Black Creek Aquifer Hydraulic Conductivity = 1.5 x 10-4 m/s;
Jun-19 Median 15.13 14.75 Groundwater discharge length = 57%;
May-19 Q1 10.31 9.96 Offsite gradient adjustment factor = 0.475.
Jun-19 Q1 12.69 13.45
May-19 Q3 18.92 13.15
Jun-19 Q3 19.69 16.13
May-19 Average 15.09 11.85 Changed groundwater discharge from 57% to 60%.
Jun-19 Average 16.86 14.83
May-19 Geomean 13.39 11.64 Model input parameters:
Jun-19 Geomean 15.40 14.76 Upper Black Creek Aquifer Hydraulic Conductivity = 1 x 10-6 m/s;
May-19 Median 13.24 11.37 Lower Black Creek Aquifer Hydraulic Conductivity = 1.5 x 10-4 m/s;
Jun-19 Median 15.45 14.75 Groundwater discharge length = 60%;
May-19 Q1 10.51 9.96 Offsite gradient adjustment factor = 0.475.
Jun-19 Q1 12.88 13.45
May-19 Q3 19.44 13.15
Jun-19 Q3 20.21 16.13
May-19 Average 15.22 11.85 Changed groundwater discharge from 60% to 61%.
Jun-19 Average 16.99 14.83
May-19 Geomean 13.50 11.64 Model input parameters:
Jun-19 Geomean 15.51 14.76 Upper Black Creek Aquifer Hydraulic Conductivity = 1 x 10-6 m/s;
May-19 Median 13.35 11.37 Lower Black Creek Aquifer Hydraulic Conductivity = 1.5 x 10-4 m/s;
Jun-19 Median 15.56 14.75 Groundwater discharge length = 61%;
May-19 Q1 10.57 9.96 Offsite gradient adjustment factor = 0.475.
Jun-19 Q1 12.95 13.45
May-19 Q3 19.61 13.15
Jun-19 Q3 20.38 16.13
May-19 Average 14.96 11.85 Changed groundwater discharge from 61% to 59%.
Jun-19 Average 16.74 14.83
May-19 Geomean 13.29 11.64 Model input parameters:
Jun-19 Geomean 15.30 14.76 Upper Black Creek Aquifer Hydraulic Conductivity = 1 x 10-6 m/s;
May-19 Median 13.13 11.37 Lower Black Creek Aquifer Hydraulic Conductivity = 1.5 x 10-4 m/s;
Jun-19 Median 15.35 14.75 Groundwater discharge length = 59%;
May-19 Q1 10.44 9.96 Offsite gradient adjustment factor = 0.475.
Jun-19 Q1 12.82 13.45
May-19 Q3 19.27 13.15
Jun-19 Q3 20.04 16.13
4
5
6
7
0.79
0.33
0.33
0.45
0.17
1.61
0.45
0.16
1.84
0.87
0.39
0.91
0.42
0.42
0.16
1.78
0.95
0.39
0.16
1.73
Improved NRMSE for all
metrics except minimum and
1st quartile. Continue
calibration.
Worsened NRMSE for all
metrics except 1st quartile.
1st quartile model input
scenario is the lowest
NRMSE for all models thus
far. Continue calibration to
get overall NRMSE for all
metrics lower.
Worsened NRMSE for all
metrics except minimum and
1st quartile. Continue
calibration to get overall
NRMSE for all metrics
lower.
Improved NRMSE as
compared to run #5 and run
#6. Continue calibration.
Page 2 of 6 August 2019
TABLE 5
MODEL ESTIMATED TOTAL TABLE 3+ MASS LOADING CALIBRATION
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
Model Observed
Description of changes CommentsScenario
Total Table 3+ Mass Loading
(mg/s)NRMSECalibration
Step Event Date
May-19 Average 14.84 11.85 Changed groundwater discharge from 59% to 58%.
Jun-19 Average 16.61 14.83
May-19 Geomean 13.18 11.64 Model input parameters:
Jun-19 Geomean 15.19 14.76 Upper Black Creek Aquifer Hydraulic Conductivity = 1 x 10-6 m/s;
May-19 Median 13.03 11.37 Lower Black Creek Aquifer Hydraulic Conductivity = 1.5 x 10-4 m/s;
Jun-19 Median 15.24 14.75 Groundwater discharge length = 58%;
May-19 Q1 10.38 9.96 Offsite gradient adjustment factor = 0.475.
Jun-19 Q1 12.76 13.45
May-19 Q3 19.10 13.15
Jun-19 Q3 19.87 16.13
May-19 Average 14.59 11.85 Changed groundwater discharge from 58% to 56%.
Jun-19 Average 16.36 14.83
May-19 Geomean 12.97 11.64 Model input parameters:
Jun-19 Geomean 14.98 14.76 Upper Black Creek Aquifer Hydraulic Conductivity = 1 x 10-6 m/s;
May-19 Median 12.82 11.37 Lower Black Creek Aquifer Hydraulic Conductivity = 1.5 x 10-4 m/s;
Jun-19 Median 15.03 14.75 Groundwater discharge length = 56%;
May-19 Q1 10.25 9.96 Offsite gradient adjustment factor = 0.475.
Jun-19 Q1 12.63 13.45
May-19 Q3 18.75 13.15
Jun-19 Q3 19.52 16.13
May-19 Average 14.34 11.85 Changed groundwater discharge from 56% to 54%.
Jun-19 Average 16.11 14.83
May-19 Geomean 12.76 11.64 Model input parameters:
Jun-19 Geomean 14.77 14.76 Upper Black Creek Aquifer Hydraulic Conductivity = 1 x 10-6 m/s;
May-19 Median 12.60 11.37 Lower Black Creek Aquifer Hydraulic Conductivity = 1.5 x 10-4 m/s;
Jun-19 Median 14.82 14.75 Groundwater discharge length = 54%;
May-19 Q1 10.12 9.96 Offsite gradient adjustment factor = 0.475.
Jun-19 Q1 12.50 13.45
May-19 Q3 18.41 13.15
Jun-19 Q3 19.17 16.13
May-19 Average 12.44 11.85 Changed groundwater discharge from 54% to 58%.
Jun-19 Average 14.21 14.83
May-19 Geomean 11.16 11.64 Model input parameters:
Jun-19 Geomean 13.17 14.76 Upper Black Creek Aquifer Hydraulic Conductivity = 1 x 10-6 m/s;
May-19 Median 10.99 11.37 Lower Black Creek Aquifer Hydraulic Conductivity = 1.5 x 10-4 m/s;
Jun-19 Median 13.21 14.75 Groundwater discharge length = 58%;
May-19 Q1 9.15 9.96 Offsite gradient adjustment factor = 0.475.
Jun-19 Q1 11.53 13.45
May-19 Q3 15.79 13.15
Jun-19 Q3 16.56 16.13
8
9
10
11
0.16
1.67
0.75
0.31
0.31
0.18
0.83
0.36
0.36
0.20
0.38
0.33
0.42
0.63
1.56
0.67
0.25
0.26
0.19
1.44
Improved NRMSE as
compared to run #7. 1st
quartile model input scenario
is the lowest NRMSE for all
models thus far.
Worsened NRMSE for all
metrics. Continue
calibration.
Worsened NRMSE for all
metrics. Continue
calibration.
Worsened NRMSE for 1st
quartile and median but
improved for all other metric
compared to run #10.
However, model not lowest
NRMSE amongst all models
tested thus far. Continue
calibration.
Page 3 of 6 August 2019
TABLE 5
MODEL ESTIMATED TOTAL TABLE 3+ MASS LOADING CALIBRATION
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
Model Observed
Description of changes CommentsScenario
Total Table 3+ Mass Loading
(mg/s)NRMSECalibration
Step Event Date
May-19 Average 17.24 11.85 Changed Lower Black Creek Aquifer Hydraulic Conductivity from 1. 5 x 10-4 m/s to 2 x 10-4 m/s.
Jun-19 Average 19.02 14.83
May-19 Geomean 15.21 11.64 Model input parameters:
Jun-19 Geomean 17.21 14.76 Upper Black Creek Aquifer Hydraulic Conductivity = 1 x 10-6 m/s;
May-19 Median 15.06 11.37 Lower Black Creek Aquifer Hydraulic Conductivity = 2 x 10-4 m/s;
Jun-19 Median 17.27 14.75 Groundwater discharge length = 58%;
May-19 Q1 11.60 9.96 Offsite gradient adjustment factor = 0.475.
Jun-19 Q1 13.98 13.45
May-19 Q3 22.40 13.15
Jun-19 Q3 23.17 16.13
May-19 Average 13.40 11.85 Changed Lower Black Creek Aquifer Hydraulic Conductivity from 2 x 10-4 m/s to 1.2 x 10-4 m/s.
Jun-19 Average 15.17 14.83
May-19 Geomean 11.97 11.64 Model input parameters:
Jun-19 Geomean 13.98 14.76 Upper Black Creek Aquifer Hydraulic Conductivity = 1 x 10-6 m/s;
May-19 Median 11.81 11.37 Lower Black Creek Aquifer Hydraulic Conductivity = 1.2 x 10-4 m/s;
Jun-19 Median 14.02 14.75 Groundwater discharge length = 58%;
May-19 Q1 9.64 9.96 Offsite gradient adjustment factor = 0.475.
Jun-19 Q1 12.02 13.45
May-19 Q3 17.11 13.15
Jun-19 Q3 17.88 16.13
May-19 Average 15.80 11.85 Changed Lower Black Creek Aquifer Hydraulic Conductivity from 1.2 x 10-4 m/s to 1.7 x 10-4 m/s.
Jun-19 Average 17.57 14.83
May-19 Geomean 13.99 11.64 Model input parameters:
Jun-19 Geomean 16.00 14.76 Upper Black Creek Aquifer Hydraulic Conductivity = 1 x 10-6 m/s;
May-19 Median 13.84 11.37 Lower Black Creek Aquifer Hydraulic Conductivity = 1.7 x 10-4 m/s;
Jun-19 Median 16.05 14.75 Groundwater discharge length = 58%;
May-19 Q1 10.87 9.96 Offsite gradient adjustment factor = 0.475.
Jun-19 Q1 13.24 13.45
May-19 Q3 20.42 13.15
Jun-19 Q3 21.19 16.13
May-19 Average 15.32 11.85 Changed Lower Black Creek Aquifer Hydraulic Conductivity from 1.7 x 10-4 m/s to 1.6 x 10-4 m/s;
Jun-19 Average 17.09 14.83
May-19 Geomean 13.59 11.64 Model input parameters:
Jun-19 Geomean 15.59 14.76 Upper Black Creek Aquifer Hydraulic Conductivity = 1 x 10-6 m/s;
May-19 Median 13.44 11.37 Lower Black Creek Aquifer Hydraulic Conductivity = 1.6 x 10-4 m/s;
Jun-19 Median 15.65 14.75 Groundwater discharge length = 58%;
May-19 Q1 10.62 9.96 Offsite gradient adjustment factor = 0.475
Jun-19 Q1 13.00 13.45
May-19 Q3 19.76 13.15
Jun-19 Q3 20.53 16.13
14
15
12
13
1.62
0.18
0.30
1.03
1.14
0.60
0.58
0.98
0.94
0.35
2.76
0.38
0.19
1.89
0.19
2.10
0.98
0.48
0.47
0.16
Worsened NRSME for all
scenarios compared to run
#8. However, model not
lowest NRMSE amongst all
models tested thus far.
Continue calibration.
Improved best estimate
NRMSE as compared to
calibration run #8 for some
metrics. However, model not
lowest NRMSE amongst all
models tested thus far.
Continue calibration.
Worsened NRSME for all
scenarios compared to run
#8. However, model not
lowest NRMSE amongst all
models tested thus far.
Continue calibration.
Worsened NRSME for all
scenarios compared to run
#8. However, model not
lowest NRMSE amongst all
models tested thus far.
Continue calibration.
Page 4 of 6 August 2019
TABLE 5
MODEL ESTIMATED TOTAL TABLE 3+ MASS LOADING CALIBRATION
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
Model Observed
Description of changes CommentsScenario
Total Table 3+ Mass Loading
(mg/s)NRMSECalibration
Step Event Date
May-19 Average 14.91 11.85 Changed Lower Black Creek Aquifer Hydraulic Conductivity from 1.6 x 10-4 m/s to 1.5 x 10-4 m/s
Jun-19 Average 16.69 14.83 and Upper Black Creek Aquifer Hydraulic Conductivity from 1 x 10-6 m/s to 2 x 10-6 m/s.
May-19 Geomean 13.24 11.64
Jun-19 Geomean 15.25 14.76 Model input parameters:
May-19 Median 13.09 11.37 Upper Black Creek Aquifer Hydraulic Conductivity = 2 x 10-6 m/s;
Jun-19 Median 15.30 14.75 Lower Black Creek Aquifer Hydraulic Conductivity = 1.5 x 10-4 m/s;
May-19 Q1 10.41 9.96 Groundwater discharge length = 58%;
Jun-19 Q1 12.79 13.45 Offsite gradient adjustment factor = 0.475.
May-19 Q3 19.20 13.15
Jun-19 Q3 19.96 16.13
May-19 Average 14.88 11.85 Changed Upper Black Creek Aquifer Hydraulic Conductivity from 2 x 10-6 m/s to 1.5-6 m/s.
Jun-19 Average 16.65 14.83
May-19 Geomean 13.21 11.64 Model input parameters:
Jun-19 Geomean 15.22 14.76 Upper Black Creek Aquifer Hydraulic Conductivity = 1.5 x 10-6 m/s;
May-19 Median 13.06 11.37 Lower Black Creek Aquifer Hydraulic Conductivity = 1.5 x 10-4 m/s;
Jun-19 Median 15.27 14.75 Groundwater discharge length = 58%;
May-19 Q1 10.40 9.96 Offsite gradient adjustment factor = 0.475.
Jun-19 Q1 12.77 13.45
May-19 Q3 19.15 13.15
Jun-19 Q3 19.91 16.13
May-19 Average 14.80 11.85 Changed Upper Black Creek Aquifer Hydraulic Conductivity from 1.5-6 m/s to 0.5 x 10-6 m/s
Jun-19 Average 16.58 14.83
May-19 Geomean 13.15 11.64 Model input parameters:
Jun-19 Geomean 15.16 14.76 Upper Black Creek Aquifer Hydraulic Conductivity = 0.5 x 10-6 m/s;
May-19 Median 13.00 11.37 Lower Black Creek Aquifer Hydraulic Conductivity = 1.5 x 10-4 m/s;
Jun-19 Median 15.21 14.75 Groundwater discharge length = 58%;
May-19 Q1 10.36 9.96 Offsite gradient adjustment factor = 0.475
Jun-19 Q1 12.74 13.45
May-19 Q3 19.05 13.15
Jun-19 Q3 19.82 16.13
May-19 Average 14.82 11.85 Changed Upper Black Creek Aquifer Hydraulic Conductivity from 0.5 x 10-6 m/s to 0.8 x 10-6 m/s.
Jun-19 Average 16.60 14.83
May-19 Geomean 13.17 11.64 Model input parameters:
Jun-19 Geomean 15.18 14.76 Upper Black Creek Aquifer Hydraulic Conductivity = 0.8 x 10-6 m/s;
May-19 Median 13.02 11.37 Lower Black Creek Aquifer Hydraulic Conductivity = 1.5 x 10-4 m/s;
Jun-19 Median 15.23 14.75 Groundwater discharge length = 58%;
May-19 Q1 10.37 9.96 Offsite gradient adjustment factor = 0.475.
Jun-19 Q1 12.75 13.45
May-19 Q3 19.08 13.15
Jun-19 Q3 19.85 16.13
16
17
18
19
0.85
0.38
0.38
0.16
1.70
0.35
0.35
0.17
1.65
0.82
0.36
0.84
0.37
0.37
0.16
1.68
0.82
0.36
0.16
1.66
Slightly better NRMSE than
run #8 for most scenarios
except 1st quartile.
However, model not lowest
NRMSE amongst all models
tested thus far. Continue
calibration.
Worsened NRSME for all
scenarios compared to run
#8. However, model not
lowest NRMSE amongst all
models tested thus far.
Continue calibration.
Worsened NRSME for all
scenarios compared to run
#8 but not by much.
However, model not lowest
NRMSE amongst all models
tested thus far. Continue
calibration.
Slightly better NRMSE than
run #8 for most scenarios
except 1st quartile.
However, model not lowest
NRMSE amongst all models
tested thus far. Continue
calibration.
Page 5 of 6 August 2019
TABLE 5
MODEL ESTIMATED TOTAL TABLE 3+ MASS LOADING CALIBRATION
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
Model Observed
Description of changes CommentsScenario
Total Table 3+ Mass Loading
(mg/s)NRMSECalibration
Step Event Date
May-19 Average 14.74 11.85 Changed Upper Black Creek Aquifer Hydraulic Conductivity from 0.8 10-6 m/s to 1 x 10-6 m/s and
Jun-19 Average 16.51 14.83 offsite gradient adjustment factor from 0.475 to 0.376.
May-19 Geomean 13.14 11.64
Jun-19 Geomean 15.15 14.76 Model input parameters:
May-19 Median 12.99 11.37 Upper Black Creek Aquifer Hydraulic Conductivity = 1 x 10-6 m/s;
Jun-19 Median 15.20 14.75 Lower Black Creek Aquifer Hydraulic Conductivity = 1.5 x 10-4 m/s;
May-19 Q1 10.36 9.96 Groundwater discharge length = 58%;
Jun-19 Q1 12.74 13.45 Offsite gradient adjustment factor = 0.376.
May-19 Q3 18.97 13.15
Jun-19 Q3 19.74 16.13
May-19 Average 14.42 11.85 Changed Offsite Surficial Aquifer Hydraulic Conductivity from 2.5 x 10-4 m/s to 1 x 10-6 m/s .
Jun-19 Average 16.20 14.83
May-19 Geomean 13.04 11.64 Model input parameters:
Jun-19 Geomean 15.04 14.76 Upper Black Creek Aquifer Hydraulic Conductivity = 1 x 10-6 m/s;
May-19 Median 12.90 11.37 Lower Black Creek Aquifer Hydraulic Conductivity = 1.5 x 10-4 m/s;
Jun-19 Median 15.11 14.75 Groundwater discharge length = 58%;
May-19 Q1 10.34 9.96 Offsite gradient adjustment factor = 0.376.
Jun-19 Q1 12.72 13.45
May-19 Q3 18.57 13.15
Jun-19 Q3 19.34 16.13
Notes:
2. Total Table 3+ loading percentage computed includes sum of Table 3+ PFAS compounds listed in Table 2 and Hexafluoropropylene oxide dimer acid (HFPO-DA).
3. February-19 moading pecentage not shown here because dataset not complete at the time of this assessment.
4. Normalized Root Mean Square calculated as
where,
observed refers to observed empirical mass loading at Bladen's Bluff
model refers to model-estimated total Table 3+ mass loading in the Cape Fear River at Bladen's Bluff
n is the number of field sampling event datasets used in the calibration (May and June 2019)
5. Abbreviations:
NRMSE - Normalized Root Mean Square Error
RMSE - Root Mean Square Error
PFAS - Per- andper- and polyfluoroalkyl substances
Q1 - 1st Quartile
Q3 - 3rd Quartile
1. February-19, May-19 and June-19 correspond to field sampling events "Surface Water 02/19", "Surface Water 05/19" and "Surface Water 06/19" reported in Seeps and Creeks Investigation Report (Geosyntec, 2019). "Surface Water 02/19" performed
February 1 - 7, 2019; "Surface Water 05/19" performed May 20 - 30, 2019; "Surface Water 06/19" performed June 4 - 7, 2019.
20
21
1.50
0.16
1.63
0.69
0.32
0.33
0.17
0.79
0.35
0.35
Improved NRMSE for most
metrics as compared to run
#19 but model not lowest
NRMSE amongst all models
tested thus far. Continue
calibration.
NRMSE did not improve in
comparison to run #8. Run
#8 1st quartile scenario
determined to yield best-fit
model
𝑅𝑅𝑅𝑅𝑅𝑅𝑅𝑅=∑𝑖𝑖=1𝑛𝑛=2 𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜−𝑚𝑚𝑜𝑜𝑜𝑜𝑜𝑜𝑚𝑚2𝑛𝑛𝑁𝑁𝑅𝑅𝑅𝑅𝑅𝑅𝑅𝑅=𝑅𝑅𝑅𝑅𝑅𝑅𝑅𝑅𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑚𝑚𝑚𝑚𝑚𝑚−𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑚𝑚𝑖𝑖𝑛𝑛
Page 6 of 6 August 2019
TABLE 6
MODEL ESTIMATED TOTAL TABLE 3+
MASS LOADING CONTRIBUTIONS PER PATHWAY
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
May - 20191
(%)
June - 20191
(%)
1 Upstream River and Groundwater 4%15%
2 Willis Creek 10%4%
3 Aerial Deposition on River < 2%< 2%
4 Outfall 002 4%7%
5 Onsite Groundwater 22%17%
6A Seep A 9%10%
6B Seep B 16%8%
6C Seep C 2%2%
6D Seep D 5%4%
7 Old Outfall 002 23%29%
8 Adjacent and Downstream Groundwater < 2%< 2%
9 Georgia Branch Creek 4%3%
100%100%
32%24%
55%53%
Notes:
4. Abbreviations:
NA - Not Applicable.
Total
Total Seeps
Transport
Pathway Number Potential PFAS Transport Pathway
Total Table 3+ Estimated Loading Percentage2
1. May-2019 and June-2019 correspond to field sampling events "Surface Water 02/19", "Surface Water 05/19" and
"Surface Water 06/19" reported in Seeps and Creeks Investigation Report (Geosyntec, 2019). "Surface Water
3. February-19 moading pecentage not shown here because dataset not complete at the time of this assessment.
Total Seeps, Old Outfall 002
2. Total Table 3+ loading percentage computed includes Table 3+ listed in Table 2 and Hexafluoropropylene oxide
dimer acid (HFPO-DA).
Page 1 of 1 August 2019
TABLE 7-A
OBSERVED CONCENTRATIONS AND MASS LOADINGS AT BLADEN BLUFFS - MAY 2019 AND JUNE 2019
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C
Measured
Concentration
at Bladen Bluffs
Observed
Mass Loading
at Bladen
Bluffs
Measured
Concentration
Observed Mass
Loading at
Bladen Bluffs
ng/L ng/s ng/L ng/s
HFPO-DA Hexafluoropropylene oxide dimer acid 13252-13-6 28 1,443,027 57 1,856,169
PEPA Perfluoroethoxypropyl carboxylic acid 267239-61-2 ND ND ND ND
PFECA-G Perfluoro-4-isopropoxybutanoic acid 801212-59-9 ND ND ND ND
PFMOAA Perfluoro-2-methoxyaceticacid 674-13-5 130 6,699,766 180 5,861,587
PFO2HxA Perfluoro(3,5-dioxahexanoic) acid 39492-88-1 40 2,061,466 64 2,084,120
PFO3OA Perfluoro(3,5,7-trioxaoctanoic) acid 39492-89-2 9.9 510,213 16 521,030
PFO4DA Perfluoro(3,5,7,9-tetraoxadecanoic) acid 39492-90-5 3.5 180,378 6 208,412
PMPA Perfluoromethoxypropyl carboxylic acid 13140-29-9 31 1,597,636 55 1,791,041
Hydro-EVE Acid Perfluoroethoxsypropanoic acid 773804-62-9 ND ND ND ND
EVE Acid Perfluoroethoxypropionic acid 69087-46-3 ND ND ND ND
PFECA B Perfluoro-3,6-dioxaheptanoic acid 151772-58-6 ND ND ND ND
R-EVE R-EVE EVS1428 4 206,147 6 205,156
PFO5DA Perfluoro-3,5,7,9,11-pentaoxadodecanoic acid 39492-91-6 ND ND 3 110,719
Byproduct 4 Byproduct 4 EVS1429 9.6 494,752 19 618,723
Byproduct 5 Byproduct 5 EVS1430 31 1,597,636 69 2,246,942
Byproduct 6 Byproduct 6 EVS1431 ND ND ND ND
NVHOS Perfluoroethoxysulfonic acid 1132933-86-8 6.1 314,374 9 283,310
PES Perfluoroethoxyethanesulfonic acid 113507-82-7 ND ND ND ND
PFESA-BP1 Byproduct 1 29311-67-9 ND ND 2 78,154
PFESA-BP2 Byproduct 2 749836-20-2 ND ND 5 159,565
PFBA Perfluorobutanoic acid 375-22-4 6.8 350,449 9 276,797
PFDA Perfluorodecanoic acid 335-76-2 ND ND ND ND
PFDoA Perfluorododecanoic acid 307-55-1 ND ND ND ND
PFHpA Perfluoroheptanoic acid 375-85-9 8.2 422,601 10 325,644
PFNA Perfluorononanoic acid 375-95-1 ND ND ND ND
PFOA Perfluorooctanoic acid 335-67-1 6.8 350,449 9 283,310
PFHxA Perfluorohexanoic acid 307-24-4 12 618,440 17 553,594
PFPeA Perfluoropentanoic acid 2706-90-3 13 669,977 20 651,287
PFTeA Perfluorotetradecanoic acid 376-06-7 ND ND ND ND
PFTriA Perfluorotridecanoic acid 72629-94-8 ND ND ND ND
PFUnA Perfluoroundecanoic acid 2058-94-8 ND ND ND ND
PFBS Perfluorobutanesulfonic acid 375-73-5 3.3 170,071 4 140,027
PFDS Perfluorodecanesulfonic acid 335-77-3 ND ND ND ND
PFHpS Perfluoroheptanesulfonic acid 375-92-8 ND ND ND ND
PFHxS Perfluorohexanesulfonic acid 355-46-4 5 257,683 7 218,181
PFNS Perfluorononanesulfonic acid 68259-12-1 ND ND ND ND
PFOS Perfluorooctanesulfonic acid 1763-23-1 13 669,977 15 488,466
PFPeS Perfluoropentanesulfonic acid 2706-91-4 ND ND ND ND
10:2 FTS 10:2-fluorotelomersulfonic acid 120226-60-0 ND ND ND ND
4:2 FTS 4:2 fluorotelomersulfonic acid 757124-72-4 ND ND ND ND
6:2 FTS 6:2 fluorotelomersulfonic acid 27619-97-2 ND ND ND ND
8:2 FTS 8:2 fluorotelomersulfonic acid 39108-34-4 ND ND ND ND
NEtFOSAA NEtFOSAA 2991-50-6 ND ND ND ND
NEtPFOSA NEtPFOSA 4151-50-2 NS NS NS NS
NEtPFOSAE NEtPFOSAE 1691-99-2 NS NS NS NS
NMeFOSAA NMeFOSAA 2355-31-9 ND ND ND ND
NMePFOSA NMePFOSA 31506-32-8 NS NS NS NS
NMePFOSAE NMePFOSAE 24448-09-7 NS NS NS NS
PFDOS Perfluorododecanesulfonic acid 79780-39-5 ND ND ND ND
PFHxDA Perfluorohexadecanoic acid 67905-19-5 NS NS NS NS
PFODA Perfluorooctadecanoic acid 16517-11-6 ND ND ND ND
PFOSA Perfluorooctanesulfonamide 754-91-6 ND ND ND ND
F-53B Major F-53B Major 73606-19-6 NS NS NS NS
F-53B Minor F-53B Minor 83329-89-9 NS NS NS NS
ADONA 4,8-dioxa-3H-perfluorononanoate 958445-44-8 NS NS NS NS
NaDONA NaDONA EVS1361 NS NS NS NS
DONA DONA 919005-14-4 NS NS NS NS
Notes:
2. Abbreviations:
ng/L - nanograms per liter
ng/s - nanograms per second
ND - Compound was not detected at laboratory detection limit.
NS - Compound was analyzed for in collected sample(s) or sample was not collected.
1. To account for 1 day of travel time, the mass loading was calculated using the average flow rate at USGS Station No. 02105500 one day prior to the date of sampling at the Bladen Bluffs intake.
The Bladen Bluffs intake was sampled on May 22, 2019 and June 7, 2019 for the May and June sampling events, respectively. The average flow rate measured one day prior was 1,820 cubic feet
per second (May 21, 2019) and 1,150 cubic feet per second (June 6, 2019) for the May and June sampling events, respectively.
Table 3+ Lab SOP
EPA Method 537 Mod
May 2019 Sampling Event June 2019 Sampling Event
Analytical Method Common Name Chemical Name CASN
August 2019
TABLE 7-B
OBSERVED CONCENTRATIONS AND MASS LOADINGS AT KINGS BLUFF - MAY 2019 AND JUNE 2019
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C
Measured
Concentration
at Bladen Bluffs
Observed
Mass Loading
at Bladen
Bluffs
Measured
Concentration
Observed Mass
Loading at
Bladen Bluffs
ng/L ng/s ng/L ng/s
HFPO-DA Hexafluoropropylene oxide dimer acid 13252-13-6 17 897,078 37 1,424,904
PEPA Perfluoroethoxypropyl carboxylic acid 267239-61-2 ND ND ND ND
PFECA-G Perfluoro-4-isopropoxybutanoic acid 801212-59-9 ND ND ND ND
PFMOAA Perfluoro-2-methoxyaceticacid 674-13-5 8 440,384 230 8,857,510
PFO2HxA Perfluoro(3,5-dioxahexanoic) acid 39492-88-1 29 1,576,682 66 2,541,720
PFO3OA Perfluoro(3,5,7-trioxaoctanoic) acid 39492-89-2 8 410,481 20 770,218
PFO4DA Perfluoro(3,5,7,9-tetraoxadecanoic) acid 39492-90-5 2 130,484 8.2 315,789
PMPA Perfluoromethoxypropyl carboxylic acid 13140-29-9 25 1,359,209 35 1,347,882
Hydro-EVE Acid Perfluoroethoxsypropanoic acid 773804-62-9 ND ND ND ND
EVE Acid Perfluoroethoxypropionic acid 69087-46-3 ND ND ND ND
PFECA B Perfluoro-3,6-dioxaheptanoic acid 151772-58-6 ND ND ND ND
R-EVE R-EVE EVS1428 10 543,683 8.3 319,641
PFO5DA Perfluoro-3,5,7,9,11-pentaoxadodecanoic acid 39492-91-6 ND ND 3.2 123,235
Byproduct 4 Byproduct 4 EVS1429 20 1,087,367 19 731,707
Byproduct 5 Byproduct 5 EVS1430 8 432,228 82 3,157,895
Byproduct 6 Byproduct 6 EVS1431 ND ND ND ND
NVHOS Perfluoroethoxysulfonic acid 1132933-86-8 6.2 337,084 9 346,598
PES Perfluoroethoxyethanesulfonic acid 113507-82-7 ND ND ND ND
PFESA-BP1 Byproduct 1 29311-67-9 ND ND ND ND
PFESA-BP2 Byproduct 2 749836-20-2 ND ND 5 192,555
PFBA Perfluorobutanoic acid 375-22-4 4.9 266,405 7.3 281,130
PFDA Perfluorodecanoic acid 335-76-2 ND ND ND ND
PFDoA Perfluorododecanoic acid 307-55-1 ND ND ND ND
PFHpA Perfluoroheptanoic acid 375-85-9 6.0 326,210 9.6 369,705
PFNA Perfluorononanoic acid 375-95-1 ND ND ND ND
PFOA Perfluorooctanoic acid 335-67-1 6.7 364,268 7.1 273,427
PFHxA Perfluorohexanoic acid 307-24-4 8.95 486,597 15 577,664
PFPeA Perfluoropentanoic acid 2706-90-3 9.65 524,655 16 616,175
PFTeA Perfluorotetradecanoic acid 376-06-7 ND ND ND ND
PFTriA Perfluorotridecanoic acid 72629-94-8 ND ND ND ND
PFUnA Perfluoroundecanoic acid 2058-94-8 ND ND ND ND
PFBS Perfluorobutanesulfonic acid 375-73-5 2.8 152,231 3.3 127,086
PFDS Perfluorodecanesulfonic acid 335-77-3 ND ND ND ND
PFHpS Perfluoroheptanesulfonic acid 375-92-8 ND ND ND ND
PFHxS Perfluorohexanesulfonic acid 355-46-4 4.3 231,065 5.5 211,810
PFNS Perfluorononanesulfonic acid 68259-12-1 ND ND ND ND
PFOS Perfluorooctanesulfonic acid 1763-23-1 12 652,420 14 539,153
PFPeS Perfluoropentanesulfonic acid 2706-91-4 ND ND ND ND
10:2 FTS 10:2-fluorotelomersulfonic acid 120226-60-0 ND ND ND ND
4:2 FTS 4:2 fluorotelomersulfonic acid 757124-72-4 ND ND ND ND
6:2 FTS 6:2 fluorotelomersulfonic acid 27619-97-2 ND ND ND ND
8:2 FTS 8:2 fluorotelomersulfonic acid 39108-34-4 ND ND ND ND
NEtFOSAA NEtFOSAA 2991-50-6 ND ND ND ND
NEtPFOSA NEtPFOSA 4151-50-2 NS NS NS NS
NEtPFOSAE NEtPFOSAE 1691-99-2 NS NS NS NS
NMeFOSAA NMeFOSAA 2355-31-9 ND ND ND ND
NMePFOSA NMePFOSA 31506-32-8 NS NS NS NS
NMePFOSAE NMePFOSAE 24448-09-7 NS NS NS NS
PFDOS Perfluorododecanesulfonic acid 79780-39-5 ND ND ND ND
PFHxDA Perfluorohexadecanoic acid 67905-19-5 NS NS NS NS
PFODA Perfluorooctadecanoic acid 16517-11-6 ND ND ND ND
PFOSA Perfluorooctanesulfonamide 754-91-6 ND ND ND ND
F-53B Major F-53B Major 73606-19-6 NS NS NS NS
F-53B Minor F-53B Minor 83329-89-9 NS NS NS NS
ADONA 4,8-dioxa-3H-perfluorononanoate 958445-44-8 NS NS NS NS
NaDONA NaDONA EVS1361 NS NS NS NS
DONA DONA 919005-14-4 NS NS NS NS
Notes:
3. Abbreviations:
ng/L - nanograms per liter
ng/s - nanograms per second
ND - Compound was not detected at laboratory detection limit.
NS - Compound was analyzed for in collected sample(s) or sample was not collected.
Table 3+ Lab SOP
EPA Method 537 Mod
1.Mass loading was calculated using the average flow rate at USGS Station No. 02105769 on the date of sampling at the Kings Bluff intake. The Kings Bluff intake was sampled on May 22, 2019
and June 7, 2019 for the May and June sampling events, respectively. The average flow rates measured on those dates were 1,920 cubic feet per second (May 21, 2019) and 1,360 cubic feet per
second (June 6, 2019) for the May and June sampling events, respectively.
2. A duplicate sample was analyzed at Kings Bluff for the May Sampling event. When an analyte was detected in both the primary sample and the duplicate sample, the average of the two values
was used. Otherwise, the value from the primary sample was used.
Analytical Method Common Name Chemical Name CASN
May 2019 Sampling Event June 2019 Sampling Event
August 2019
TABLE 8-AESTIMATED PATHWAY CONTRIBUTION TO OBSERVED CONCENTRATION AT BLADEN BLUFFS - MAY 2019Chemours Fayetteville Works, North CarolinaGeosyntec Consultants NC, P.C123456A6B6C6D789Observed Concentration at Bladen BluffsUpstream River and GroundwaterWillis CreekAerial Deposition on RiverOutfall 002Onsite GroundwaterSeep A Seep B Seep C Seep D Old Outfall 002Adjacent and Downstream GroundwaterGeorgia Branch Creekng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/L%%%HFPO-DA Hexafluoropropylene oxide dimer acid 13252-13-6 28.00.05.00.00.45.82.84.10.81.54.80.22.628.028.000100%0%0%PEPAPerfluoroethoxypropyl carboxylic acid 267239-61-2 NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -PFECA-G Perfluoro-4-isopropoxybutanoic acid 801212-59-9 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFMOAAPerfluoro-2-methoxyaceticacid674-13-5 130.00.06.80.03.833.59.422.93.37.742.50.10.0130.0130.000100%0%0%PFO2HxAPerfluoro(3,5-dioxahexanoic) acid 39492-88-1 40.02.54.10.01.910.83.35.00.91.98.20.11.440.040.000100%0%0%PFO3OAPerfluoro(3,5,7-trioxaoctanoic) acid 39492-89-2 9.90.00.80.00.92.61.31.20.30.52.30.00.09.99.900100%0%0%PFO4DA Perfluoro(3,5,7,9-tetraoxadecanoic) acid 39492-90-5 3.50.00.90.00.60.00.80.20.10.20.80.00.03.53.500100%0%0%PMPA Perfluoromethoxypropyl carboxylic acid 13140-29-9 310.07.30.10.07.02.14.90.20.73.20.35.331.031.000100%0%0%Hydro-EVE Acid Perfluoroethoxsypropanoic acid 773804-62-9 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---EVE AcidPerfluoroethoxypropionic acid69087-46-3 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFECA BPerfluoro-3,6-dioxaheptanoic acid 151772-58-6 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---R-EVER-EVEEVS1428 4.00.00.00.00.10.00.81.80.10.50.60.00.04.04.000100%0%0%PFO5DA Perfluoro-3,5,7,9,11-pentaoxadodecanoic acid 39492-91-6 NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -Byproduct 4Byproduct 4EVS1429 9.60.00.00.00.80.02.23.60.20.72.00.00.09.69.600100%0%0%Byproduct 5Byproduct 5EVS1430 31.011.72.70.00.30.06.97.70.10.51.10.00.031.029.30295%0%5%Byproduct 6Byproduct 6EVS1431 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND-- -NVHOSPerfluoroethoxysulfonic acid 1132933-86-8 6.14.30.00.00.50.00.10.50.00.10.60.00.06.11.80429%0%71%PESPerfluoroethoxyethanesulfonic acid 113507-82-7 NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -PFESA-BP1Byproduct 129311-67-9 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND- - -PFESA-BP2Byproduct 2749836-20-2 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---293.118.527.60.29.259.729.951.76.014.366.20.79.2293.1287.10698%0%2%PFBAPerfluorobutanoic acid375-22-4 6.86.40.10.00.00.10.00.10.00.00.10.00.16.80.36.50.04%96%0%PFDAPerfluorodecanoic acid335-76-2 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND - - -PFDoAPerfluorododecanoic acid307-55-1 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFHpAPerfluoroheptanoic acid375-85-9 8.28.10.00.00.00.00.00.00.00.00.00.00.08.20.08.20.01%99%0%PFNAPerfluorononanoic acid375-95-1 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND - - -PFOAPerfluorooctanoic acid335-67-1 6.86.70.00.00.00.00.00.00.00.00.00.00.06.80.06.80.00%100%0%PFHxAPerfluorohexanoic acid307-24-4 12.011.90.00.00.00.00.00.00.00.00.00.00.012.00.012.00.00%100%0%PFPeAPerfluoropentanoic acid2706-90-3 13.012.10.10.00.00.30.10.20.00.10.10.00.013.00.712.30.06%94%0%PFTeAPerfluorotetradecanoic acid376-06-7 NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -PFTriAPerfluorotridecanoic acid72629-94-8 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFUnAPerfluoroundecanoic acid2058-94-8 NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -PFBSPerfluorobutanesulfonic acid375-73-5 3.33.30.00.00.00.00.00.00.00.00.00.00.03.30.03.30.00%100%0%PFDSPerfluorodecanesulfonic acid335-77-3 NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -PFHpSPerfluoroheptanesulfonic acid375-92-8 NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -PFHxSPerfluorohexanesulfonic acid355-46-4 5.05.00.00.00.00.00.00.00.00.00.00.00.05.00.05.00.00%100%0%PFNSPerfluorononanesulfonic acid68259-12-1 NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -PFOSPerfluorooctanesulfonic acid1763-23-1 13.013.00.00.00.00.00.00.00.00.00.00.00.013.00.013.00.00%100%0%PFPeSPerfluoropentanesulfonic acid2706-91-4 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---10:2 FTS10:2-fluorotelomersulfonic acid 120226-60-0 NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -4:2 FTS4:2 fluorotelomersulfonic acid 757124-72-4 NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -6:2 FTS6:2 fluorotelomersulfonic acid27619-97-2 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---8:2 FTS8:2 fluorotelomersulfonic acid39108-34-4 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---NEtFOSAANEtFOSAA2991-50-6 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---NEtPFOSANEtPFOSA4151-50-2 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---NEtPFOSAENEtPFOSAE1691-99-2 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---NMeFOSAANMeFOSAA2355-31-9 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---NMePFOSANMePFOSA31506-32-8 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---NMePFOSAENMePFOSAE24448-09-7 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---PFDOSPerfluorododecanesulfonic acid 79780-39-5 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFHxDAPerfluorohexadecanoic acid67905-19-5 NSNSNSNSNSNSNSNSNSNSNSNSNSNS NS NS NS - - -PFODAPerfluorooctadecanoic acid16517-11-6 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFOSAPerfluorooctanesulfonamide754-91-6 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---F-53B MajorF-53B Major73606-19-6 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS-- -F-53B MinorF-53B Minor83329-89-9 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS - - -ADONA4,8-dioxa-3H-perfluorononanoate 958445-44-8 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---NaDONANaDONAEVS1361 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---DONADONA919005-14-4 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---68.166.50.30.00.00.40.10.30.00.10.20.00.268.11.167.00.02%98%0%361.285.027.80.29.260.130.052.06.014.466.40.79.4361.2288.267.06.080%19%2%Notes:1. Estimated percentage contribution of pathway to total mass loading based on 1st Quartile Input Values for May 2019 event; see Table 10-A.2. Percentage of pathway contribution allocated to Site, Other, or Unknown sources per pathway per compound presented in Table 11.3. Abbreviations:ng/L - nanograms per literng/s - nanograms per secondND - Compound was not detected at laboratory detection limit.NS - Compound was analyzed for in collected sample(s) or sample was not collected.Total PFAS Mass LoadingEPA Method 537 ModTotal Table 3+Table 3+ Lab SOPTotal PFAS ConcentrationTotal EPA Method 537Analytical Method Common Name Chemical NameCASNTransport Pathway Number →Percentage of Concentration of PFAS Originating from FacilityPercentage of Total Concentration of PFAS from Other SourcesPercentage of Total Concentration of PFAS from Unknown SourcesTotal Concentration of PFAS Originating from FacilityTotal Concentration of PFAS from Other SourcesTotal Concentration of PFAS from Unknown SourcesAugust 2019
TABLE 8-BESTIMATED PATHWAY CONTRIBUTION TO OBSERVED CONCENTRATION AT BLADEN BLUFFS - JUNE 2019Chemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC, P.C.123456A6B6C6D789Observed Mass Loading at Bladen BluffsUpstream River and GroundwaterWillis CreekAerial Deposition on RiverOutfall 002Onsite GroundwaterSeep A Seep B Seep C Seep D Old Outfall 002Adjacent and Downstream GroundwaterGeorgia Branch Creekng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/L%%%HFPO-DA Hexafluoropropylene oxide dimer acid 13252-13-6 57.010.23.20.12.68.97.44.61.92.79.70.35.457.057.000100%0%0%PEPAPerfluoroethoxypropyl carboxylic acid 267239-61-2 NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -PFECA-G Perfluoro-4-isopropoxybutanoic acid 801212-59-9 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFMOAAPerfluoro-2-methoxyaceticacid674-13-5 180.00.04.90.06.836.915.915.85.38.984.60.10.7180.0180.000100%0%0%PFO2HxAPerfluoro(3,5-dioxahexanoic) acid39492-88-1 64.04.22.70.14.316.87.14.21.62.518.00.22.364.064.000100%0%0%PFO3OAPerfluoro(3,5,7-trioxaoctanoic) acid39492-89-2 16.00.00.40.02.13.72.60.90.50.84.60.00.316.016.000100%0%0%PFO4DA Perfluoro(3,5,7,9-tetraoxadecanoic) acid 39492-90-5 6.40.00.10.02.30.01.50.20.10.21.70.00.16.46.400100%0%0%PMPA Perfluoromethoxypropyl carboxylic acid 13140-29-9 55.018.93.90.10.39.74.54.20.40.86.00.45.755.055.000100%0%0%Hydro-EVE Acid Perfluoroethoxsypropanoic acid773804-62-9 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---EVE AcidPerfluoroethoxypropionic acid69087-46-3 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFECA BPerfluoro-3,6-dioxaheptanoic acid151772-58-6 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---R-EVER-EVEEVS14286.33.70.40.00.10.00.50.70.10.20.40.00.36.36.300100%0%0%PFO5DA Perfluoro-3,5,7,9,11-pentaoxadodecanoic acid 39492-91-6 3.40.00.00.01.80.01.00.00.00.00.50.00.03.43.400100%0%0%Byproduct 4Byproduct 4EVS1429 19.013.90.50.01.60.00.70.80.10.20.70.00.519.015.50482%0%18%Byproduct 5Byproduct 5EVS1430 69.042.73.40.04.60.08.37.20.20.52.20.00.069.063.00691%0%9%Byproduct 6Byproduct 6EVS1431NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---NVHOSPerfluoroethoxysulfonic acid1132933-86-8 8.76.00.10.01.20.00.20.30.10.10.80.00.08.72.70631%0%69%PESPerfluoroethoxyethanesulfonic acid113507-82-7 NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -PFESA-BP1Byproduct 129311-67-9 2.40.00.00.01.10.00.80.20.00.00.20.00.02.42.400100%0%0%PFESA-BP2Byproduct 2749836-20-2 4.90.00.10.04.10.00.20.10.00.00.20.00.14.94.900100%0%0%492.1 99.619.80.333.076.050.839.310.316.9129.61.115.5492.1476.601697%0%3%PFBAPerfluorobutanoic acid375-22-48.58.00.10.00.00.10.10.10.00.00.10.00.18.50.38.20.04%96%0%PFDAPerfluorodecanoic acid335-76-2NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND - - -PFDoAPerfluorododecanoic acid307-55-1NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFHpAPerfluoroheptanoic acid375-85-910.09.90.00.00.00.00.00.00.00.00.00.00.010.00.19.90.01%99%0%PFNAPerfluorononanoic acid375-95-1NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND - - -PFOAPerfluorooctanoic acid335-67-18.78.60.00.00.00.00.00.00.00.00.00.00.08.70.08.70.00%100%0%PFHxAPerfluorohexanoic acid307-24-417.016.90.00.00.00.00.00.00.00.00.00.00.017.00.017.00.00%100%0%PFPeAPerfluoropentanoic acid2706-90-3 20.019.00.10.00.00.30.10.20.00.10.20.00.120.00.819.10.04%96%0%PFTeAPerfluorotetradecanoic acid376-06-7NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -PFTriAPerfluorotridecanoic acid72629-94-8 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFUnAPerfluoroundecanoic acid2058-94-8 NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -PFBSPerfluorobutanesulfonic acid375-73-54.34.30.00.00.00.00.00.00.00.00.00.00.04.30.04.30.00%100%0%PFDSPerfluorodecanesulfonic acid335-77-3NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -PFHpSPerfluoroheptanesulfonic acid375-92-8NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -PFHxSPerfluorohexanesulfonic acid355-46-46.76.70.00.00.00.00.00.00.00.00.00.00.06.70.06.70.00%100%0%PFNSPerfluorononanesulfonic acid68259-12-1 NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -PFOSPerfluorooctanesulfonic acid1763-23-1 15.015.00.00.00.00.00.00.00.00.00.00.00.015.00.015.00.00%100%0%PFPeSPerfluoropentanesulfonic acid2706-91-4 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---10:2 FTS10:2-fluorotelomersulfonic acid120226-60-0 NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -4:2 FTS4:2 fluorotelomersulfonic acid757124-72-4 NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -6:2 FTS6:2 fluorotelomersulfonic acid27619-97-2 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---8:2 FTS8:2 fluorotelomersulfonic acid39108-34-4 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---NEtFOSAANEtFOSAA2991-50-6 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---NEtPFOSANEtPFOSA4151-50-2NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---NEtPFOSAENEtPFOSAE1691-99-2NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---NMeFOSAANMeFOSAA2355-31-9 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---NMePFOSANMePFOSA31506-32-8 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---NMePFOSAENMePFOSAE24448-09-7 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---PFDOSPerfluorododecanesulfonic acid79780-39-5 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFHxDAPerfluorohexadecanoic acid67905-19-5 NSNSNSNSNSNSNSNSNSNSNSNSNSNS NS NS NS - - -PFODAPerfluorooctadecanoic acid16517-11-6 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFOSAPerfluorooctanesulfonamide754-91-6NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---F-53B MajorF-53B Major73606-19-6 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---F-53B MinorF-53B Minor83329-89-9 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS - --ADONA4,8-dioxa-3H-perfluorononanoate958445-44-8 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---NaDONANaDONAEVS1361NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---DONADONA919005-14-4 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---90.288.30.30.00.00.40.20.30.10.10.30.00.290.21.288.90.01%99%0%582.3 187.920.00.333.076.451.039.510.417.0129.91.115.7582.3477.888.915.582%15%3%Notes:1. Estimated percentage contribution of pathway to total mass loading based on 1st Quartile Input Values for May 2019 event; see Table 10-B.2. Percentage of pathway contribution allocated to Site, Other, or Unknown sources per pathway per compound presented in Table 11.3. Abbreviations:ng/L - nanograms per literng/s - nanograms per secondND - Compound was not detected at laboratory detection limit.NS - Compound was analyzed for in collected sample(s) or sample was not collected.Total PFAS Mass LoadingPercentage of Concentration of PFAS Originating from FacilityTransport Pathway Number →Total PFAS ConcentrationTotal Concentration of PFAS Originating from FacilityTotal Concentration of PFAS from Other SourcesTotal Concentration of PFAS from Unknown SourcesAnalytical MethodCommon Name Chemical NameCASNPercentage of Total Concentration of PFAS from Other SourcesPercentage of Total Concentration of PFAS from Unknown SourcesTable 3+ Lab SOPTotal Table 3+EPA Method 537 ModTotal EPA Method 537August 2019
TABLE 8-CESTIMATED PATHWAY CONTRIBUTION TO OBSERVED CONCENTRATION AT KINGS BLUFF - MAY 2019Chemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC, P.C.123456A6B6C6D789Observed Concentration at Kings Bluff*Upstream River and GroundwaterWillis CreekAerial Deposition on RiverOutfall 002Onsite GroundwaterSeep A Seep B Seep C Seep D Old Outfall 002Adjacent and Downstream GroundwaterGeorgia Branch Creekng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/L%%%HFPO-DA Hexafluoropropylene oxide dimer acid 13252-13-6 16.50.03.00.00.23.41.72.40.40.92.90.11.516.516.500100%0%0%PEPAPerfluoroethoxypropyl carboxylic acid 267239-61-2 NDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND ND - - -PFECA-G Perfluoro-4-isopropoxybutanoic acid 801212-59-9 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFMOAAPerfluoro-2-methoxyaceticacid674-13-5 8.10.00.40.00.22.10.61.40.20.52.70.00.08.18.100100%0%0%PFO2HxAPerfluoro(3,5-dioxahexanoic) acid 39492-88-1 29.01.83.00.01.47.82.43.60.61.35.90.11.029.029.000100%0%0%PFO3OAPerfluoro(3,5,7-trioxaoctanoic) acid 39492-89-2 7.60.00.60.00.72.01.00.90.20.41.80.00.07.67.600100%0%0%PFO4DA Perfluoro(3,5,7,9-tetraoxadecanoic) acid 39492-90-5 2.40.00.60.00.40.00.60.10.00.10.60.00.02.42.400100%0%0%PMPA Perfluoromethoxypropyl carboxylic acid 13140-29-9 25.00.05.90.10.05.61.74.00.20.62.60.24.225.025.000100%0%0%Hydro-EVE Acid Perfluoroethoxsypropanoic acid 773804-62-9 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---EVE AcidPerfluoroethoxypropionic acid69087-46-3 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFECA BPerfluoro-3,6-dioxaheptanoic acid 151772-58-6 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---R-EVER-EVEEVS1428 10.00.00.00.00.30.02.14.40.31.31.50.00.010.010.000100%0%0%PFO5DA Perfluoro-3,5,7,9,11-pentaoxadodecanoic acid 39492-91-6 NDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND ND - - -Byproduct 4Byproduct 4EVS1429 20.00.00.00.01.70.04.77.60.41.44.20.00.020.020.000100%0%0%Byproduct 5Byproduct 5EVS1430 8.03.00.70.00.10.01.82.00.00.10.30.00.08.07.50095%0%5%Byproduct 6Byproduct 6EVS1431 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---NVHOSPerfluoroethoxysulfonic acid 1132933-86-8 6.24.40.00.00.50.00.10.50.00.10.60.00.06.21.80429%0%71%PESPerfluoroethoxyethanesulfonic acid 113507-82-7 NDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND ND - - -PFESA-BP1Byproduct 129311-67-9 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND- - -PFESA-BP2Byproduct 2749836-20-2 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---132.79.214.10.15.520.916.626.92.56.822.90.56.8132.7127.90.04.896%0%4%PFBAPerfluorobutanoic acid375-22-4 4.94.60.00.00.00.10.00.10.00.00.00.00.04.90.24.70.04%96%0%PFDAPerfluorodecanoic acid335-76-2 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND - - -PFDoAPerfluorododecanoic acid307-55-1 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFHpAPerfluoroheptanoic acid375-85-9 6.05.90.00.00.00.00.00.00.00.00.00.00.06.00.06.00.01%99%0%PFNAPerfluorononanoic acid375-95-1 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND - - -PFOAPerfluorooctanoic acid335-67-1 6.76.60.00.00.00.00.00.00.00.00.00.00.06.70.06.70.00%100%0%PFHxAPerfluorohexanoic acid307-24-4 9.08.90.00.00.00.00.00.00.00.00.00.00.09.00.08.90.00%100%0%PFPeAPerfluoropentanoic acid2706-90-3 9.79.00.00.00.00.20.10.10.00.00.10.00.09.60.59.10.06%94%0%PFTeAPerfluorotetradecanoic acid376-06-7 NDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND ND - - -PFTriAPerfluorotridecanoic acid72629-94-8 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFUnAPerfluoroundecanoic acid2058-94-8 NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -PFBSPerfluorobutanesulfonic acid375-73-5 2.82.80.00.00.00.00.00.00.00.00.00.00.02.80.02.80.00%100%0%PFDSPerfluorodecanesulfonic acid335-77-3 NDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND ND - - -PFHpSPerfluoroheptanesulfonic acid375-92-8 NDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND ND - - -PFHxSPerfluorohexanesulfonic acid355-46-4 4.34.20.00.00.00.00.00.00.00.00.00.00.04.20.04.20.00%100%0%PFNSPerfluorononanesulfonic acid68259-12-1 NDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND ND - - -PFOSPerfluorooctanesulfonic acid1763-23-1 12.012.00.00.00.00.00.00.00.00.00.00.00.012.00.012.00.00%100%0%PFPeSPerfluoropentanesulfonic acid2706-91-4 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---10:2 FTS10:2-fluorotelomersulfonic acid 120226-60-0 NDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND ND - - -4:2 FTS4:2 fluorotelomersulfonic acid 757124-72-4 NDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND ND - - -6:2 FTS6:2 fluorotelomersulfonic acid27619-97-2 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---8:2 FTS8:2 fluorotelomersulfonic acid39108-34-4 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---NEtFOSAANEtFOSAA2991-50-6 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---NEtPFOSANEtPFOSA4151-50-2 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---NEtPFOSAENEtPFOSAE1691-99-2 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---NMeFOSAANMeFOSAA2355-31-9 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---NMePFOSANMePFOSA31506-32-8 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---NMePFOSAENMePFOSAE24448-09-7 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---PFDOSPerfluorododecanesulfonic acid 79780-39-5 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFHxDAPerfluorohexadecanoic acid67905-19-5 NSNSNSNSNSNSNSNSNSNSNSNSNS NS NS NS NS - - -PFODAPerfluorooctadecanoic acid16517-11-6 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFOSAPerfluorooctanesulfonamide754-91-6 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---F-53B MajorF-53B Major73606-19-6 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS-- -F-53B MinorF-53B Minor83329-89-9 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS - - -ADONA4,8-dioxa-3H-perfluorononanoate 958445-44-8 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---NaDONANaDONAEVS1361 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---DONADONA919005-14-4 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---55.354.00.20.00.00.30.10.20.00.10.20.00.155.20.854.50.01%99%0%188.063.314.30.15.521.216.727.12.56.923.00.56.9187.9128.754.54.868%29%3%Notes:* Observed concentration at Kings Bluff is the sum of the average of each reported PFAS compound value from the parent and duplicate samples collected on May 23, 2019.1. Estimated percentage contribution of pathway to total mass loading based on 1st Quartile Input Values for May 2019 event; see Table 10-A.2. Percentage of pathway contribution allocated to Site, Other, or Unknown sources per pathway per compound presented in Table 11.3. Abbreviations:ng/L - nanograms per literng/s - nanograms per secondND - Compound was not detected at laboratory detection limit.NS - Compound was analyzed for in collected sample(s) or sample was not collected.Table 3+ Lab SOPTotal Table 3+EPA Method 537 ModTotal EPA Method 537Total PFAS Mass LoadingPercentage of Total Concentration of PFAS from Other SourcesPercentage of Total Concentration of PFAS from Unknown SourcesAnalytical Method Common Name Chemical NameCASNTransport Pathway Number →Total PFAS ConcentrationTotal Concentration of PFAS Originating from FacilityTotal Concentration of PFAS from Other SourcesTotal Concentration of PFAS from Unknown SourcesPercentage of Concentration of PFAS Originating from FacilityAugust 2019
TABLE 8-DESTIMATED PATHWAY CONTRIBUTION TO OBSERVED CONCENTRATION AT KINGS BLUFF - JUNE 2019Chemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC, P.C.123456A6B6C6D789Observed Mass Loading at Kings BluffUpstream River and GroundwaterWillis CreekAerial Deposition on RiverOutfall 002Onsite GroundwaterSeep A Seep B Seep C Seep D Old Outfall 002Adjacent and Downstream GroundwaterGeorgia Branch Creekng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/Lng/L%%%HFPO-DA Hexafluoropropylene oxide dimer acid 13252-13-6 37.06.62.10.01.75.84.83.01.21.76.30.23.537.037.00.00.0100%0%0%PEPAPerfluoroethoxypropyl carboxylic acid 267239-61-2 NDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND ND - - -PFECA-G Perfluoro-4-isopropoxybutanoic acid 801212-59-9 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFMOAAPerfluoro-2-methoxyaceticacid674-13-5 230.00.06.20.08.747.120.320.26.811.4108.10.10.9230.0230.00.00.0100%0%0%PFO2HxAPerfluoro(3,5-dioxahexanoic) acid39492-88-1 66.04.32.80.14.517.37.34.41.72.618.50.32.366.066.00.00.0100%0%0%PFO3OAPerfluoro(3,5,7-trioxaoctanoic) acid39492-89-2 20.00.00.50.02.64.63.21.20.61.05.80.00.420.020.00.00.0100%0%0%PFO4DA Perfluoro(3,5,7,9-tetraoxadecanoic) acid 39492-90-5 8.20.00.20.03.00.02.00.30.20.32.20.00.28.28.20.00.0100%0%0%PMPA Perfluoromethoxypropyl carboxylic acid 13140-29-9 35.012.12.50.10.26.22.82.70.30.53.80.33.635.035.00.00.0100%0%0%Hydro-EVE Acid Perfluoroethoxsypropanoic acid773804-62-9 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---EVE AcidPerfluoroethoxypropionic acid69087-46-3 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFECA BPerfluoro-3,6-dioxaheptanoic acid151772-58-6 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---R-EVER-EVEEVS14288.34.90.50.00.10.00.70.90.10.30.50.00.48.38.30.00.0100%0%0%PFO5DA Perfluoro-3,5,7,9,11-pentaoxadodecanoic acid 39492-91-6 3.20.00.00.01.70.00.90.00.00.00.50.00.03.23.20.00.0100%0%0%Byproduct 4Byproduct 4EVS1429 19.013.90.50.01.60.00.70.80.10.20.70.00.519.015.50.03.582%0%18%Byproduct 5Byproduct 5EVS1430 82.050.74.10.05.40.09.98.60.20.52.60.00.082.074.80.07.291%0%9%Byproduct 6Byproduct 6EVS1431NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---NVHOSPerfluoroethoxysulfonic acid1132933-86-8 9.06.20.10.01.20.00.20.30.10.10.80.00.09.02.80.06.231%0%69%PESPerfluoroethoxyethanesulfonic acid113507-82-7 NDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND ND - - -PFESA-BP1Byproduct 129311-67-9 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFESA-BP2Byproduct 2749836-20-2 5.00.00.10.04.20.00.20.10.00.00.30.00.15.05.00.00.0100%0%0%522.7 98.619.50.235.081.053.142.311.218.6150.10.912.0522.7505.80.016.997%0%3%PFBAPerfluorobutanoic acid375-22-47.36.90.00.00.00.10.00.10.00.00.10.00.17.30.37.00.04%96%0%PFDAPerfluorodecanoic acid335-76-2NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND ---PFDoAPerfluorododecanoic acid307-55-1NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFHpAPerfluoroheptanoic acid375-85-99.69.50.00.00.00.00.00.00.00.00.00.00.09.60.09.60.01%99%0%PFNAPerfluorononanoic acid375-95-1NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND ---PFOAPerfluorooctanoic acid335-67-17.17.00.00.00.00.00.00.00.00.00.00.00.07.10.07.10.00%100%0%PFHxAPerfluorohexanoic acid307-24-415.014.90.00.00.00.00.00.00.00.00.00.00.015.00.015.00.00%100%0%PFPeAPerfluoropentanoic acid2706-90-3 16.015.20.10.00.00.30.10.10.00.10.10.00.016.00.715.30.04%96%0%PFTeAPerfluorotetradecanoic acid376-06-7NDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND ND - - -PFTriAPerfluorotridecanoic acid72629-94-8 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFUnAPerfluoroundecanoic acid2058-94-8 NDNDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND - - -PFBSPerfluorobutanesulfonic acid375-73-53.33.30.00.00.00.00.00.00.00.00.00.00.03.30.03.30.00%100%0%PFDSPerfluorodecanesulfonic acid335-77-3NDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND ND - - -PFHpSPerfluoroheptanesulfonic acid375-92-8NDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND ND - - -PFHxSPerfluorohexanesulfonic acid355-46-45.55.50.00.00.00.00.00.00.00.00.00.00.05.50.05.50.00%100%0%PFNSPerfluorononanesulfonic acid68259-12-1 NDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND ND - - -PFOSPerfluorooctanesulfonic acid1763-23-1 14.014.00.00.00.00.00.00.00.00.00.00.00.014.00.014.00.00%100%0%PFPeSPerfluoropentanesulfonic acid2706-91-4 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---10:2 FTS10:2-fluorotelomersulfonic acid120226-60-0 NDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND ND - - -4:2 FTS4:2 fluorotelomersulfonic acid757124-72-4 NDNDNDNDNDNDNDNDNDNDNDNDND ND ND ND ND - - -6:2 FTS6:2 fluorotelomersulfonic acid27619-97-2 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---8:2 FTS8:2 fluorotelomersulfonic acid39108-34-4 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---NEtFOSAANEtFOSAA2991-50-6 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---NEtPFOSANEtPFOSA4151-50-2NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---NEtPFOSAENEtPFOSAE1691-99-2NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---NMeFOSAANMeFOSAA2355-31-9 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---NMePFOSANMePFOSA31506-32-8 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---NMePFOSAENMePFOSAE24448-09-7 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---PFDOSPerfluorododecanesulfonic acid79780-39-5 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFHxDAPerfluorohexadecanoic acid67905-19-5 NSNSNSNSNSNSNSNSNSNSNSNSNS NS NS NS NS - - -PFODAPerfluorooctadecanoic acid16517-11-6 NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---PFOSAPerfluorooctanesulfonamide754-91-6NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND---F-53B MajorF-53B Major73606-19-6 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---F-53B MinorF-53B Minor83329-89-9 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS ---ADONA4,8-dioxa-3H-perfluorononanoate958445-44-8 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---NaDONANaDONAEVS1361NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---DONADONA919005-14-4 NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNS---77.876.20.20.00.00.40.20.20.10.10.30.00.177.81.076.80.01%99%0%600.5 174.919.80.235.081.453.342.511.318.7150.30.912.2600.5506.976.816.984%13%3%Notes:1. Estimated percentage contribution of pathway to total mass loading based on 1st Quartile Input Values for May 2019 event; see Table 10-B.2. Percentage of pathway contribution allocated to Site, Other, or Unknown sources per pathway per compound presented in Table 11.3. Abbreviations:ng/L - nanograms per literng/s - nanograms per secondND - Compound was not detected at laboratory detection limit.NS - Compound was analyzed for in collected sample(s) or sample was not collected.Table 3+ Lab SOPTotal Table 3+EPA Method 537 ModTotal EPA Method 537Total PFAS Mass LoadingPercentage of Total Concentration of PFAS from Other SourcesPercentage of Total Concentration of PFAS from Unknown SourcesAnalytical MethodCommon Name Chemical NameCASNTransport Pathway Number →Total PFAS ConcentrationTotal Concentration of PFAS Originating from FacilityTotal Concentration of PFAS from Other SourcesTotal Concentration of PFAS from Unknown SourcesPercentage of Concentration of PFAS Originating from FacilityAugust 2019
TABLE 9-AESTIMATED MASS LOADING WITH 1st QUARTILE INPUT VALUES - MAY 2019Chemours Fayetteville Works, North CarolinaGeosyntec Consultants NC, P.C123456A6B6C6D789Transport Pathway →Upstream River and GroundwaterWillis CreekAerial Deposition on RiverOutfall 002Onsite GroundwaterSeep A Seep B Seep C Seep DOld Outfall 002Adjacent and Downstream GroundwaterGeorgia Branch CreekCASNng/sng/sng/sng/sng/sng/sng/sng/sng/sng/sng/sng/sng/sHFPO-DA Hexafluoropropylene oxide dimer acid 13252-13-6 NA 148,771 1,132 11,215 172,500 82,922 119,856 22,315 45,134 143,407 4,881 76,446 828,577PEPAPerfluoroethoxypropyl carboxylic acid 267239-61-2 NA 66,120 7550 54,794 35,770 70,824 3,099 8,801 40,668 3,254 45,868 329,953PFECA-G Perfluoro-4-isopropoxybutanoic acid 801212-59-9 NA NA ND0NA NANANANANANANA -PFMOAAPerfluoro-2-methoxyaceticacid674-13-5 NA 243,359 553 134,145 1,197,351 334,938 817,200 119,633 273,813 1,519,685 2,386 NA 4,643,065PFO2HxAPerfluoro(3,5-dioxahexanoic) acid 39492-88-1 117,455 192,392 1,635 90,283 507,352 154,462 234,264 40,911 87,259 385,272 7,050 64,215 1,882,549PFO3OAPerfluoro(3,5,7-trioxaoctanoic) acid 39492-89-2 NA 33,978 126 37,507 113,647 58,533 52,301 11,777 23,921 102,739 542 NA 435,072PFO4DA Perfluoro(3,5,7,9-tetraoxadecanoic) acid 39492-90-5 NA 36,733 126 23,471 NA 35,770 7,082 3,037 7,071 34,246 542 NA 148,079`PMPA Perfluoromethoxypropyl carboxylic acid 13140-29-9 NA 275,501 2,515 0 263,823 79,670 185,232 8,678 27,231 119,863 10,846 198,760 1,172,119Hydro-EVE Acid Perfluoroethoxsypropanoic acid 773804-62-9 NA NA NA 2,803 NA 8,130 9,262 1,550 3,912 4,281 NA NA 29,936EVE AcidPerfluoroethoxypropionic acid69087-46-3 NA NA NA 1,449 NA 5,366 15,799 NA NA NA NA NA 22,614PFECA BPerfluoro-3,6-dioxaheptanoic acid 151772-58-6 NA NA NA0NA NA N`A NA NA NA NA NA-R-EVER-EVEEVS1428 NA NA NA 760 NA 5,203 10,896 744 3,310 3,639 NA NA 24,551PFO5DA Perfluoro-3,5,7,9,11-pentaoxadodecanoic acid 39492-91-6 NA 8,265 252 9,872 NA 20,161 1,144 60451 13,270 1,085 NA 54,561Byproduct 4Byproduct 4EVS1429 NA NA NA 3,577 NA 9,755 15,799 806 2,941 8,776 NA NA 41,654Byproduct 5Byproduct 5EVS1430 174,505 40,407 NA 4,516 NA 102,433 114,408 1,178 7,598 16,909 NA NA 461,952Byproduct 6Byproduct 6EVS1431 NA NA NA 1,986 NA 229 2893245NA NA NA 2,581NVHOSPerfluoroethoxysulfonic acid 1132933-86-8 137,590 NA NA 15,113 NA 4,553 14,710 1,240 2,415 17,765 NA NA 193,385PESPerfluoroethoxyethanesulfonic acid 113507-82-7 NA NA NA0NA NA NA NA NA NA NA NA-PFESA-BP1Byproduct 129311-67-9 NA NA ND 11,744 NA 24,064 10,896 NA NA NA NA NA 46,703PFESA-BP2Byproduct 2749836-20-2 NA 10,836 ND 27,396 NA 5,528 3,596 446 978 6,635 NA 5,045 60,461429,550 1,056,363 7,093 375,836 2,309,468 967,485 1,683,557 215,507 494,879 2,417,156 30,587 390,334 10,377,814PFBAPerfluorobutanoic acid375-22-4 208,063 1,837 NA NA 2,638 1,171 2,561 242 632 1,841 130 1,682 220,796PFDAPerfluorodecanoic acid335-76-2 NA NA NA NA NA NA12NA NA NA NA NA 12PFDoAPerfluorododecanoic acid307-55-1 NA NA NA NA NA NA NA NA NA NA NA NA-PFHpAPerfluoroheptanoic acid375-85-9 281,892 478 NA NA 304 390 763 149 283 535 NA 367 285,161PFNAPerfluorononanoic acid375-95-1 NA NA NA NA438565NA8161 NA NA 361PFOAPerfluorooctanoic acid335-67-1 231,554 1,616 NA NA9412093113468557581 234,846PFHxAPerfluorohexanoic acid307-24-4 405,062 845 NA NA 244 NA 202 NA 121 36464505 407,405PFPeAPerfluoropentanoic acid2706-90-3 402,703 2,204 NA NA 9,538 2,341 6,538 1,116 2,219 3,211 NA 1,529 431,399PFTeAPerfluorotetradecanoic acid376-06-7 NA NA NA NA NA NA NA NA NA NA NA NA-PFTriAPerfluorotridecanoic acid72629-94-8 NA NA NA NA NA NA NA NA NA NA NA NA-PFUnAPerfluoroundecanoic acid2058-94-8 NA NA NA NA NA NA NA NA NA NA NA NA-PFBSPerfluorobutanesulfonic acid375-73-5 104,032 661 NA NA45NA NA NA NA NA NA NA 104,738PFDSPerfluorodecanesulfonic acid335-77-3 NA NA NA NA NA NA NA NA NA NA NA NA-PFHpSPerfluoroheptanesulfonic acid375-92-8 NA NA NA NA NA NA NA NA NA NA NANA -PFHxSPerfluorohexanesulfonic acid355-46-4 157,725 404 NA NA 11011NA16NA NA NA 158,257PFNSPerfluorononanesulfonic acid68259-12-1 NA NA NA NA NA NA NA NA NA NA NANA -PFOSPerfluorooctanesulfonic acid1763-23-1 436,262 771 NA NA 24418131NA43NA 367 437,718PFPeSPerfluoropentanesulfonic acid2706-91-4 NA NA NA NA NA NA NA NA NA NA NA NA-10:2 FTS10:2-fluorotelomersulfonic acid 120226-60-0 NA NA NA NA NA NA NANANANANANA -4:2 FTS4:2 fluorotelomersulfonic acid 757124-72-4 NA NA NA NA NA NA NA NANANANANA -6:2 FTS6:2 fluorotelomersulfonic acid27619-97-2 NA NA NA NA NA NA NA NA NA NA NA NA-8:2 FTS8:2 fluorotelomersulfonic acid39108-34-4 NA NA NA NA NA NA NA NA NA NA NA NA-NEtFOSAANEtFOSAA2991-50-6 NA NA NA NA NA NA NA NA NA NA NA NA-NEtPFOSANEtPFOSA4151-50-2 NA NA NA NA NA NA NA NA NA NA NA NA-NEtPFOSAENEtPFOSAE1691-99-2 NA NA NA NA NA NA NA NA NA NA NA NA-NMeFOSAANMeFOSAA2355-31-9 NA NA NA NA NA NA NA NA NA NA NA NA-NMePFOSANMePFOSA31506-32-8 NA NA NA NA NA NA NA NA NA NA NA NA-NMePFOSAENMePFOSAE24448-09-7 NA NA NA NA NA NA NA NA NA NA NA NA-PFDOSPerfluorododecanesulfonic acid 79780-39-5 NA NA NA NA NA NA NA NA NA NA NA NA-PFHxDAPerfluorohexadecanoic acid67905-19-5 NA NA NA NA NA NA NA NA NA NA NANA -PFODAPerfluorooctadecanoic acid16517-11-6 NA NA NA NA NA NA NA NA NA NA NA NA-PFOSAPerfluorooctanesulfonamide754-91-6 NA NA NA NA NA NA NA NA NA NA NA NA-F-53B MajorF-53B Major73606-19-6 NA NA NA NA NA NA NA NA NA NA NA NA-F-53B MinorF-53B Minor83329-89-9 NA NA NA NA NA NA NA NA NA NA NA NA-ADONA4,8-dioxa-3H-perfluorononanoate 958445-44-8 NA NA NA NA NA NA NA NA NA NA NA NA-NaDONANaDONAEVS1361 NA NA NA NA NA NA NA NA NA NA NA NA-DONADONA919005-14-4 NA NA NA NA NA NA NA NA NA NA NA NA-2,227,295 8,816-- 13,259 4,136 10,245 1,520 3,303 6,839 252 5,030 2,280,6942,656,845 1,065,179 7,093 375,836 2,322,727 971,621 1,693,802 217,027 498,181 2,423,995 30,838 395,364 12,658,507Notes:1. Calculated mass loading presented in this table from the mass loading model.2. Abbreviations:ng/s - nanograms per secondNA - Sample was not detected at laboratory detection limit or was not analyzed for in collected sample.Total PFAS Mass LoadingTotal Esimated Mass LoadingTotal Table 3+Table 3+ Lab SOPTotal EPA Method 537EPA Method 537 ModTransport Pathway Number →Analytical MethodCommon NameChemical NameAugust 2019
TABLE 9-BESTIMATED MASS LOADING WITH 1st QUARTILE INPUT VALUES - JUNE 2019Chemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC, P.C.123456A6B6C6D789Transport Pathway →Upstream River and GroundwaterWillis CreekAerial Deposition on RiverOutfall 002Onsite GroundwaterSeep A Seep B Seep C Seep DOld Outfall 002Adjacent and Downstream GroundwaterGeorgia Branch CreekCASNng/sng/sng/sng/sng/sng/sng/sng/sng/sng/sng/sng/sng/sHFPO-DA Hexafluoropropylene oxide dimer acid 13252-13-6 185,242 58,774 1,132 46,666 161,667 134,130 82,919 34,295 48,143 175,434 4,881 98,328 1,031,610PEPAPerfluoroethoxypropyl carboxylic acid 267239-61-2 NA 25,713 755 2,682 51,353 46,275 46,066 3,266 7,221 50,932 3,254 45,134 282,652PFECA-G Perfluoro-4-isopropoxybutanoic acid 801212-59-9 NA NA ND70NA NA NA NA NA NA NA NA 70PFMOAAPerfluoro-2-methoxyaceticacid674-13-5 NA 148,771 553 207,833 1,122,161 482,867 482,158 162,492 270,804 2,574,917 2,386 22,567 5,477,510PFO2HxAPerfluoro(3,5-dioxahexanoic) acid 39492-88-1 118,125 77,140 1,635 123,323 475,492 201,195 119,772 45,727 72,214 509,324 7,050 64,477 1,815,475PFO3OA Perfluoro(3,5,7-trioxaoctanoic) acid 39492-89-2 NA 12,306 126 59,078 106,510 73,771 27,025 13,881 22,266 132,990 542 9,672 458,168PFO4DA Perfluoro(3,5,7,9-tetraoxadecanoic) acid 39492-90-5 NA 2,939 126 54,683 NA 35,544 4,607 2,940 5,416 39,614 542 2,740 149,150PMPA Perfluoromethoxypropyl carboxylic acid 13140-29-9 483,240 99,180 2,515 8,480 247,256 114,010 107,488 10,615 21,664 152,797 10,846 145,074 1,403,166Hydro-EVE Acid Perfluoroethoxsypropanoic acid 773804-62-9 NA 992 NA 6,486 NA 9,389 6,756 1,715 3,611 5,659 NA 355 34,963EVE AcidPerfluoroethoxypropionic acid69087-46-3 NA NA NA 6,091 NA 6,505 13,206 NA NA 679 NA NA 26,481PFECA BPerfluoro-3,6-dioxaheptanoic acid 151772-58-6 NA NA NA24NA NA NA NA NA NA NA NA 24R-EVER-EVEEVS1428 53,693 5,143 NA 1,596 NA 7,377 9,827 1,551 3,009 5,659 NA 3,869 91,725PFO5DA Perfluoro-3,5,7,9,11-pentaoxadodecanoic acid 39492-91-6 NA 735 252 54,734 NA 30,850 829 NA 361 16,129 1,085 322 105,296Byproduct 4Byproduct 4EVS1429 212,089 7,530 NA 24,839 NA 11,401 11,977 1,225 2,528 11,035 NA 7,898 290,523Byproduct 5Byproduct 5EVS1430 617,474 49,590 NA 66,317 NA 120,717 104,416 2,531 6,620 31,125 NA NA 998,791Byproduct 6Byproduct 6EVS1431 NA NA NA 4,193 NA 335 2403351424 NA NA 5,276NVHOSPerfluoroethoxysulfonic acid 1132933-86-8 198,665 2,571 NA 38,944 NA 6,706 9,827 1,715 2,708 25,466 NA 725 287,329PESPerfluoroethoxyethanesulfonic acid 113507-82-7 NA NA NA 469 NA NA NA NA NA NA NA NA 469PFESA-BP1Byproduct 129311-67-9 NA NA ND 48,313 NA 35,544 8,906 NA NA 8,489 NA NA 101,252PFESA-BP2Byproduct 2749836-20-2 NA 3,122 ND 164,146 NA 8,718 2,887 539 1,173 9,904 NA 4,675 195,1641,868,529 494,506 7,093 918,968 2,164,439 1,325,336 1,038,907 282,525 467,789 3,750,579 30,587 405,836 12,755,093PFBAPerfluorobutanoic acid375-22-4 228,197 1,598 NA NA 2,473 1,610 1,843 327 632 2,547 130 1,773 241,128PFDAPerfluorodecanoic acid335-76-2 NA NA NA NA NA NA8NA NA NA NA NA8PFDoAPerfluorododecanoic acid307-55-1 NA NA NA NA NA NA NA NA NA NA NA NA-PFHpAPerfluoroheptanoic acid375-85-9 322,160 459 NA NA 285 530 522 188 301 736 NA 371 325,552PFNAPerfluorononanoic acid375-95-1 NA NA NA NA4010149NA8201 NA NA 399PFOAPerfluorooctanoic acid335-67-1 222,827 1,010 NA NA8824174134296257596 225,912PFHxAPerfluorohexanoic acid307-24-4 483,240 771 NA NA 228 NA 14481132 45364500 485,614PFPeAPerfluoropentanoic acid2706-90-3 536,934 1,782 NA NA 8,939 3,286 4,607 1,388 2,377 4,527 NA 1,596 565,436PFTeAPerfluorotetradecanoic acid376-06-7 NA NA NA NA NA NA NA NA NA NA NA NA-PFTriAPerfluorotridecanoic acid72629-94-8 NA NA NA NA NA NA NA NA NA NA NA NA-PFUnAPerfluoroundecanoic acid2058-94-8 NA NA NA NA NA NA NA NA NA NA NA NA-PFBSPerfluorobutanesulfonic acid375-73-5 120,810 680 NA NA4215NA NA NA NA NA NA 121,546PFDSPerfluorodecanesulfonic acid335-77-3 NA NA NA NA NA NA NA NA NA NA NA NA-PFHpSPerfluoroheptanesulfonic acid375-92-8 NA NA NA NA NA NA NA NA NA NA NANA -PFHxSPerfluorohexanesulfonic acid355-46-4 182,557 478 NA NA 10327726NA NA NA 183,179PFNSPerfluorononanesulfonic acid68259-12-1 NA NA NA NA NA NA NA NA NA NA NANA -PFOSPerfluorooctanesulfonic acid1763-23-1 402,700 661 NA NA 228657NA NA57NA NA 403,718PFPeSPerfluoropentanesulfonic acid2706-91-4 NA NA NA NA NA NA NA NA NA NA NA NA-10:2 FTS10:2-fluorotelomersulfonic acid 120226-60-0 NA NA NA NA NA NA NANANANANANA -4:2 FTS4:2 fluorotelomersulfonic acid 757124-72-4 NA NA NA NA NA NA NA NANANANANA -6:2 FTS6:2 fluorotelomersulfonic acid27619-97-2 NA NA NA NA NA NA NA NA NA NA NA NA-8:2 FTS8:2 fluorotelomersulfonic acid39108-34-4 NA NA NA NA NA NA NA NA NA NA NA NA-NEtFOSAANEtFOSAA2991-50-6 NA NA NA NA NA NA NA NA NA NA NA NA-NEtPFOSANEtPFOSA4151-50-2 NA NA NA NA NA NA NA NA NA NA NA NA-NEtPFOSAENEtPFOSAE1691-99-2 NA NA NA NA NA NA NA NA NA NA NA NA-NMeFOSAANMeFOSAA2355-31-9 NA NA NA NA NA NA NA NA NA NA NA NA-NMePFOSANMePFOSA31506-32-8 NA NA NA NA NA NA NA NA NA NA NA NA-NMePFOSAENMePFOSAE24448-09-7 NA NA NA NA NA NA NA NA NA NA NA NA-PFDOSPerfluorododecanesulfonic acid 79780-39-5 NA NA NA NA NA NA NA NA NA NA NA NA-PFHxDAPerfluorohexadecanoic acid67905-19-5 NA NA NA NA NA NA NA NA NA NA NANA -PFODAPerfluorooctadecanoic acid16517-11-6 NA NA NA NA NA NA NA NA NA NA NA NA-PFOSAPerfluorooctanesulfonamide754-91-6 NA NA NA NA NA NA NA NA NA NA NA NA-F-53B MajorF-53B Major73606-19-6 NA NA NA NA NA NA NA NA NA NA NA NA-F-53B MinorF-53B Minor83329-89-9 NA NA NA NA NA NA NA NA NA NA NA NA-ADONA4,8-dioxa-3H-perfluorononanoate 958445-44-8 NA NA NA NA NA NA NA NA NANA NANA-NaDONANaDONAEVS1361NA NA NA NA NA NA NA NA NA NA NA NA-DONADONA919005-14-4 NA NA NA NA NA NA NA NA NA NA NA NA-2,499,426 7,439-- 12,427 5,874 7,260 1,998 3,499 9,482 252 4,836 2,552,4924,367,955 501,944 7,093 918,968 2,176,865 1,331,210 1,046,167 284,523 471,288 3,760,061 30,838 410,672 15,307,585Notes:1. Calculated mass loading presented in this table from the mass loading model.2. Abbreviations:ng/s - nanograms per secondNA - Sample was not detected at laboratory detection limit or was not analyzed for in collected sample.Total PFAS Mass LoadingTransport Pathway Number →Analytical MethodCommon Name Chemical NameTotal Esimated Mass LoadingTable 3+ Lab SOPTotal Table 3+EPA Method 537 ModTotal EPA Method 537August 2019
TABLE 10-AESTIMATED CONTRIBUTION PERCENTAGE OF PATHWAY TO TOTAL MASS LOADING - MAY 2019Chemours Fayetteville Works, North CarolinaGeosyntec Consultants NC, P.C1 23456A6B6C6D7 8 9Transport Pathway →Upstream River and GroundwaterWillis CreekAerial Deposition on RiverOutfall 002Onsite GroundwaterSeep A Seep B Seep C Seep D Old Outfall 002Adjacent and Downstream GroundwaterGeorgia Branch CreekCASN% %%%%%%%%% % %HFPO-DA Hexafluoropropylene oxide dimer acid 13252-13-6 NA18.0%0.1%1.4%20.8%10.0%14.5%2.7%5.4%17.3%0.6%9.2%PEPA Perfluoroethoxypropyl carboxylic acid 267239-61-2 NA20.0%0.2%0.0%16.6%10.8%21.5%0.9%2.7%12.3%1.0%13.9%PFECA-G Perfluoro-4-isopropoxybutanoic acid 801212-59-9 NANANANANANANANANANANANAPFMOAAPerfluoro-2-methoxyaceticacid674-13-5NA5.2%0.0%2.9%25.8%7.2%17.6%2.6%5.9%32.7%0.1%NAPFO2HxA Perfluoro(3,5-dioxahexanoic) acid 39492-88-1 6.2%10.2%0.1%4.8%27.0%8.2%12.4%2.2%4.6%20.5%0.4%3.4%PFO3OA Perfluoro(3,5,7-trioxaoctanoic) acid 39492-89-2 NA7.8%0.0%8.6%26.1%13.5%12.0%2.7%5.5%23.6%0.1%NAPFO4DA Perfluoro(3,5,7,9-tetraoxadecanoic) acid 39492-90-5 NA24.8%0.1%15.9%NA24.2%4.8%2.1%4.8%23.1%0.4%NAPMPA Perfluoromethoxypropyl carboxylic acid 13140-29-9 NA23.5%0.2%0.0%22.5%6.8%15.8%0.7%2.3%10.2%0.9%17.0%Hydro-EVE AcidPerfluoroethoxsypropanoic acid 773804-62-9 NANANA9.4%NA27.2%30.9%5.2%13.1%14.3%NANAEVE AcidPerfluoroethoxypropionic acid69087-46-3 NANANA6.4%NA23.7%69.9%NANANANANAPFECA BPerfluoro-3,6-dioxaheptanoic acid 151772-58-6 NANANANANANANANANANANANAR-EVER-EVEEVS1428 NANANA3.1%NA21.2%44.4%3.0%13.5%14.8%NANAPFO5DA Perfluoro-3,5,7,9,11-pentaoxadodecanoic acid 39492-91-6 NA15.1%0.5%18.1%NA37.0%2.1%0.1%0.8%24.3%2.0%NAByproduct 4Byproduct 4EVS1429 NANANA8.6%NA23.4%37.9%1.9%7.1%21.1%NA NAByproduct 5Byproduct 5EVS1430 37.8%8.7%NA1.0%NA22.2%24.8%0.3%1.6%3.7%NANAByproduct 6Byproduct 6EVS1431 NANANA76.9%NA8.9%11.2%1.2%1.7%NANANANVHOSPerfluoroethoxysulfonic acid1132933-86-8 71.1%NANA7.8%NA2.4%7.6%0.6%1.2%9.2%NANAPESPerfluoroethoxyethanesulfonic acid 113507-82-7 NANANANANANANANANANA NA NAPFESA-BP1Byproduct 129311-67-9 NANANA25.1%NA51.5%23.3%NANANANANAPFESA-BP2Byproduct 2749836-20-2 NA17.9%NA45.3%NA9.1%5.9%0.7%1.6%11.0%NA8.3%PFBAPerfluorobutanoic acid375-22-4 94.2%0.8%0.0%NA1.2%0.5%1.2%0.1%0.3%0.8%0.1%0.8%PFDAPerfluorodecanoic acid335-76-2NANANANANANA100%NANANANANAPFDoAPerfluorododecanoic acid307-55-1NANANANANANANANANANANANAPFHpAPerfluoroheptanoic acid375-85-9 98.8%0.2%NANA0.1%0.1%0.3%0.1%0.1%0.2%NA0.1%PFNAPerfluorononanoic acid375-95-1NANANANA11.1%22.0%17.0%NA2.1%41.7%NANAPFOAPerfluorooctanoic acid335-67-1 98.6%0.7%0.0%NA0.0%0.1%0.0%0.0%0.0%0.3%0.0%0.2%PFHxAPerfluorohexanoic acid307-24-4 99.4%0.2%0.0%NA0.1%NA0.0%NA0.0%0.1%0.0%0.1%PFPeAPerfluoropentanoic acid2706-90-3 93.3%0.5%NANA2.2%0.5%1.5%0.3%0.5%0.7%NA0.4%PFTeAPerfluorotetradecanoic acid376-06-7NANANANANANANANANANANANAPFTriAPerfluorotridecanoic acid72629-94-8 NANANANANANANANANANANANAPFUnAPerfluoroundecanoic acid2058-94-8 NANANANANANANANANANANANAPFBSPerfluorobutanesulfonic acid375-73-5 99.3%0.6%NANA0.0%NANANANANANANAPFDSPerfluorodecanesulfonic acid335-77-3NANANANANANANANANANANANAPFHpSPerfluoroheptanesulfonic acid375-92-8NANANANANANANANANANANANAPFHxSPerfluorohexanesulfonic acid355-46-4 99.6%0.3%NANA0.1%0.0%NA0.0%0.0%NANANAPFNSPerfluorononanesulfonic acid68259-12-1 NANANANANANANANANANANANAPFOSPerfluorooctanesulfonic acid1763-23-1 99.6%0.2%NANA0.1%0.0%0.0%0.0%NA0.0%NA0.1%PFPeSPerfluoropentanesulfonic acid2706-91-4 NANANANANANANANANANANANA10:2 FTS10:2-fluorotelomersulfonic acid 120226-60-0 NANANANANANANANANANA NA NA4:2 FTS4:2 fluorotelomersulfonic acid757124-72-4 NANANANANANANANANANA NA NA6:2 FTS6:2 fluorotelomersulfonic acid27619-97-2 NANANANANANANANANANANANA8:2 FTS8:2 fluorotelomersulfonic acid39108-34-4 NANANANANANANANANANANANANEtFOSAANEtFOSAA2991-50-6 NANANANANANANANANANANANANEtPFOSANEtPFOSA4151-50-2 NANANANANANANANANANANANANEtPFOSAENEtPFOSAE1691-99-2 NANANANANANANANANANANANANMeFOSAANMeFOSAA2355-31-9 NANANANANANANANANANANANANMePFOSANMePFOSA31506-32-8 NANANANANANANANANANANANANMePFOSAENMePFOSAE24448-09-7 NANANANANANANANANANANANAPFDOSPerfluorododecanesulfonic acid79780-39-5 NANANANANANANANANANANANAPFHxDAPerfluorohexadecanoic acid67905-19-5 NANANANANANANANANANANANAPFODAPerfluorooctadecanoic acid16517-11-6 NANANANANANANANANANANANAPFOSAPerfluorooctanesulfonamide754-91-6NANANANANANANANANANANANAF-53B MajorF-53B Major73606-19-6 NANANANANANANANANANANANAF-53B MinorF-53B Minor83329-89-9 NANANANANANANANANANANANAADONA4,8-dioxa-3H-perfluorononanoate 958445-44-8 NANANANANANANANANANANANANaDONANaDONAEVS1361 NANANANANANANANANANANANADONADONA919005-14-4 NANANANANANANANANANANANANotes:1. Estimated contribution percentage of pathway to total mass loading presented in this table is for the May 2019 sampling event from the mass loading model. The estimated contribution percentage is based on 1st Quartile Input Values.2. Abbreviations:ng/s - nanograms per secondNA - Sample was not detected at laboratory detection limit or was not analyzed for in collected sample.Analytical MethodCommon NameChemical NameTransport Pathway Number →Table 3+ Lab SOPEPA Method 537 ModAugust 2019
TABLE 10-BESTIMATED CONTRIBUTION PERCENTAGE OF PATHWAY TO TOTAL MASS LOADING - JUNE 2019Chemours Fayetteville Works, North CarolinaGeosyntec Consultants NC, P.C123456A6B6C6D789Transport Pathway →Upstream River and GroundwaterWillis CreekAerial Deposition on RiverOutfall 002Onsite GroundwaterSeep A Seep B Seep C Seep D Old Outfall 002Adjacent and Downstream GroundwaterGeorgia Branch CreekCASN%%%%%%%%%%%%HFPO-DA Hexafluoropropylene oxide dimer acid 13252-13-6 18.0%5.7%0.1%4.5%15.7%13.0%8.0%3.3%4.7%17.0%0.5%9.5%PEPA Perfluoroethoxypropyl carboxylic acid 267239-61-2 NA9.1%0.3%0.9%18.2%16.4%16.3%1.2%2.6%18.0%1.2%16.0%PFECA-G Perfluoro-4-isopropoxybutanoic acid 801212-59-9 NANANA100.0%NANANANANANANANAPFMOAAPerfluoro-2-methoxyaceticacid674-13-5 NA2.7%0.0%3.8%20.5%8.8%8.8%3.0%4.9%47.0%0.0%0.4%PFO2HxA Perfluoro(3,5-dioxahexanoic) acid 39492-88-1 6.5%4.2%0.1%6.8%26.2%11.1%6.6%2.5%4.0%28.1%0.4%3.6%PFO3OA Perfluoro(3,5,7-trioxaoctanoic) acid 39492-89-2 NA2.7%0.0%12.9%23.2%16.1%5.9%3.0%4.9%29.0%0.1%2.1%PFO4DA Perfluoro(3,5,7,9-tetraoxadecanoic) acid 39492-90-5 NA2.0%0.1%36.7%NA23.8%3.1%2.0%3.6%26.6%0.4%1.8%PMPA Perfluoromethoxypropyl carboxylic acid 13140-29-9 34.4%7.1%0.2%0.6%17.6%8.1%7.7%0.8%1.5%10.9%0.8%10.3%Hydro-EVE AcidPerfluoroethoxsypropanoic acid 773804-62-9 NA2.8%NA18.6%NA26.9%19.3%4.9%10.3%16.2%NA1.0%EVE AcidPerfluoroethoxypropionic acid69087-46-3 NANANA23.0%NA24.6%49.9%NANA2.6%NANAPFECA B Perfluoro-3,6-dioxaheptanoic acid 151772-58-6 NANANA100.0%NANANANANANANANAR-EVER-EVEEVS1428 58.5%5.6%NA1.7%NA8.0%10.7%1.7%3.3%6.2%NA4.2%PFO5DA Perfluoro-3,5,7,9,11-pentaoxadodecanoic acid 39492-91-6 NA0.7%0.2%52.0%NA29.3%0.8%NA0.3%15.3%1.0%0.3%Byproduct 4Byproduct 4EVS1429 73.0%2.6%NA8.5%NA3.9%4.1%0.4%0.9%3.8%NA2.7%Byproduct 5Byproduct 5EVS1430 61.8%5.0%NA6.6%NA12.1%10.5%0.3%0.7%3.1%NANAByproduct 6Byproduct 6EVS1431 NANANA79.5%NA6.4%4.5%0.6%1.0%8.0%NANANVHOSPerfluoroethoxysulfonic acid1132933-86-8 69.1%0.9%NA13.6%NA2.3%3.4%0.6%0.9%8.9%NA0.3%PESPerfluoroethoxyethanesulfonic acid 113507-82-7 NANANA100.0%NANANANANANANANAPFESA-BP1Byproduct 129311-67-9 NANANA47.7%NA35.1%8.8%NANA8.4%NANAPFESA-BP2Byproduct 2749836-20-2 NA1.6%NA84.1%NA4.5%1.5%0.3%0.6%5.1%NA2.4%PFBAPerfluorobutanoic acid375-22-4 94.6%0.7%0.0%0.0%1.0%0.7%0.8%0.1%0.3%1.1%0.1%0.7%PFDAPerfluorodecanoic acid335-76-2 NANANANANANA24.9%NANANANANAPFDoAPerfluorododecanoic acid307-55-1 NANANANANANANANANANANANAPFHpAPerfluoroheptanoic acid375-85-9 98.9%0.1%NA0.0%0.1%0.2%0.2%0.1%0.1%0.2%NA0.1%PFNAPerfluorononanoic acid375-95-1 NANANANA9.4%23.8%11.6%NA2.0%47.5%NANAPFOAPerfluorooctanoic acid335-67-1 98.6%0.4%0.0%0.0%0.0%0.1%0.0%0.0%0.0%0.4%0.0%0.3%PFHxAPerfluorohexanoic acid307-24-4 99.5%0.2%0.0%0.0%0.0%NA0.0%0.0%0.0%0.1%0.0%0.1%PFPeAPerfluoropentanoic acid2706-90-3 94.9%0.3%NA0.0%1.6%0.6%0.8%0.2%0.4%0.8%NA0.3%PFTeAPerfluorotetradecanoic acid376-06-7 NANANANANANANANANANANANAPFTriAPerfluorotridecanoic acid72629-94-8 NANANANANANANANANANANANAPFUnAPerfluoroundecanoic acid2058-94-8 NANANANANANANANANANANANAPFBSPerfluorobutanesulfonic acid375-73-5 99.4%0.6%NA0.0%0.0%0.0%NANANANANANAPFDSPerfluorodecanesulfonic acid335-77-3 NANANANANANANANANANANANAPFHpSPerfluoroheptanesulfonic acid375-92-8 NANANANANANANANANANANANAPFHxSPerfluorohexanesulfonic acid355-46-4 99.6%0.3%NA0.0%0.1%0.0%0.0%0.0%0.0%NANANAPFNSPerfluorononanesulfonic acid68259-12-1 NANANANANANANANANANANANAPFOSPerfluorooctanesulfonic acid1763-23-1 99.7%0.2%NA0.0%0.1%0.0%0.0%NANA0.0%NANAPFPeSPerfluoropentanesulfonic acid2706-91-4 NANANANANANANANANANANANA10:2 FTS10:2-fluorotelomersulfonic acid 120226-60-0 NANANANANANANANANANANANA4:2 FTS4:2 fluorotelomersulfonic acid757124-72-4 NANANANANANANANANANANANA6:2 FTS6:2 fluorotelomersulfonic acid27619-97-2 NANANANANANANANANANANANA8:2 FTS8:2 fluorotelomersulfonic acid39108-34-4 NANANANANANANANANANANANANEtFOSAANEtFOSAA2991-50-6 NANANANANANANANANANANANANEtPFOSANEtPFOSA4151-50-2 NANANANANANANANANANANANANEtPFOSAENEtPFOSAE1691-99-2 NANANANANANANANANANANANANMeFOSAANMeFOSAA2355-31-9 NANANANANANANANANANANANANMePFOSANMePFOSA31506-32-8 NANANANANANANANANANANANANMePFOSAENMePFOSAE24448-09-7 NANANANANANANANANANANANAPFDOSPerfluorododecanesulfonic acid79780-39-5 NANANANANANANANANANANANAPFHxDAPerfluorohexadecanoic acid67905-19-5 NANANANANANANANANANANANAPFODAPerfluorooctadecanoic acid16517-11-6 NANANANANANANANANANANANAPFOSAPerfluorooctanesulfonamide754-91-6 NANANANANANANANANANANANAF-53B MajorF-53B Major73606-19-6 NANANANANANANANANANANANAF-53B MinorF-53B Minor83329-89-9 NANANANANANANANANANANANAADONA4,8-dioxa-3H-perfluorononanoate 958445-44-8 NANANANANANANANANANANANANaDONANaDONAEVS1361 NANANANANANANANANANANANADONADONA919005-14-4 NANANANANANANANANANANANANotes:1. Estimated contribution percentage of pathway to total mass loading presented in this table is for the June 2019 sampling event from the mass loading model. The estimated contribution percentage is based on 1st Quartile Input Values.2. Abbreviations:ng/s - nanograms per secondNA - Sample was not detected at laboratory detection limit or was not analyzed for in collected sample.Transport Pathway Number →Analytical Method Common NameChemical NameTable 3+ Lab SOPEPA Method 537 ModAugust 2019
TABLE 11ESTIMATED MASS LOADING SOURCE ORIGINATION PERCENTAGES PER COMPOUND PER PATHWAYChemours Fayetteville Works, North CarolinaGeosyntec Consultants NC P.C.Transport Pathway →SourceSite Other Unknown Site Other Unknown Site Other Unknown Site Other Unknown Site Other Unknown Site Other Unknown Site Other Unknown Site Other Unknown Site Other Unknown Site Other Unknown Site Other Unknown Site Other UnknownCASNHFPO-DA Hexafluoropropylene oxide dimer acid 13252-13-6 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - -PEPA Perfluoroethoxypropyl carboxylic acid 267239-61-2 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - -PFECA-G Perfluoro-4-isopropoxybutanoic acid 801212-59-9 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - -PFMOAA Perfluoro-2-methoxyaceticacid 674-13-5 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - -PFO2HxA Perfluoro(3,5-dioxahexanoic) acid39492-88-1 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - -PFO3OA Perfluoro(3,5,7-trioxaoctanoic) acid39492-89-2 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - -PFO4DA Perfluoro(3,5,7,9-tetraoxadecanoic) acid 39492-90-5 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100%--PMPA Perfluoromethoxypropyl carboxylic acid 13140-29-9 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - -Hydro-EVE Acid Perfluoroethoxsypropanoic acid773804-62-9 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - -EVE AcidPerfluoroethoxypropionic acid69087-46-3 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - -PFECA BPerfluoro-3,6-dioxaheptanoic acid151772-58-6 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - -R-EVER-EVEEVS1428 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - -PFO5DA Perfluoro-3,5,7,9,11-pentaoxadodecanoic acid 39492-91-6 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - -Byproduct 4Byproduct 4EVS1429 75% - 25% 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - -Byproduct 5Byproduct 5EVS1431 86% - 14% 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - -Byproduct 6Byproduct 6EVS1430 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - -NVHOSPerfluoroethoxysulfonic acid1132933-86-8 1% - 99% 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - -PESPerfluoroethoxyethanesulfonic acid113507-82-7 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - -PFESA-BP1Byproduct 129311-67-9 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - -PFESA-BP2Byproduct 2749836-20-2 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - -PFBAPerfluorobutanoic acid375-22-4- 100% - - 100% - - 100% - 100% - - 95% 5% - 97% 3% - 98% 2% - 97% 3% - 95% 5% - 89% 11% - - 100% - - 88% 12%PFDAPerfluorodecanoic acid335-76-2- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -PFDoAPerfluorododecanoic acid307-55-1- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -PFHpAPerfluoroheptanoic acid375-85-9- 100% - - 100% - - 100% - 100% - - 60% 40% - 83% 17% - 87% 13% - 91% 9% - 79% 21% - 22% 78% - - 100% - - 100% -PFNAPerfluorononanoic acid375-95-1- 100% - - 100% - - 100% - 100% - - - 100% - 84% 16% - 71% 29% - - 100% - - 100% - 44% 56% - - 100% - - 100% -PFOAPerfluorooctanoic acid335-67-1- 100% - - 100% - - 100% - 100% - - - 100% - 68% 32% - 41% 59% - 31% 69% - - 100% - 64% 36% - - 100% - - 100% -PFHxAPerfluorohexanoic acid307-24-4- 100% - - 100% - - 100% - 100% - - - 100% - 29% 71% - 41% 59% - 66% 34% - 33% 67% - - 100% - - 100% - - 100% -PFPeAPerfluoropentanoic acid2706-90-3- 100% - - 100% - - 100% - 100% - - 96% 4% - 97% 3% - 99% 1% - 99% 1% - 97% 3% - 86% 14% - - 100% - - 100% -PFTeAPerfluorotetradecanoic acid376-06-7- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -PFTriAPerfluorotridecanoic acid72629-94-8- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -PFUnAPerfluoroundecanoic acid2058-94-8- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -PFBSPerfluorobutanesulfonic acid375-73-5- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -PFDSPerfluorodecanesulfonic acid335-77-3- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -PFHpSPerfluoroheptanesulfonic acid375-92-8- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -PFHxSPerfluorohexanesulfonic acid355-46-4- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -PFNSPerfluorononanesulfonic acid68259-12-1- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -PFOSPerfluorooctanesulfonic acid1763-23-1- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -PFPeSPerfluoropentanesulfonic acid2706-91-4- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -10:2 FTS10:2-fluorotelomersulfonic acid120226-60-0 - 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -4:2 FTS4:2 fluorotelomersulfonic acid757124-72-4 - 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -6:2 FTS6:2 fluorotelomersulfonic acid27619-97-2- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -8:2 FTS8:2 fluorotelomersulfonic acid39108-34-4- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -NEtFOSAANEtFOSAA2991-50-6- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -NEtPFOSANEtPFOSA4151-50-2- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -NEtPFOSAENEtPFOSAE1691-99-2- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -NMeFOSAANMeFOSAA2355-31-9- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -NMePFOSANMePFOSA31506-32-8- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -NMePFOSAENMePFOSAE24448-09-7- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -PFDOSPerfluorododecanesulfonic acid79780-39-5- 100% - - 100% - - 100% -100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -PFHxDAPerfluorohexadecanoic acid67905-19-5- 100%-- 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -PFODAPerfluorooctadecanoic acid16517-11-6- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -PFOSAPerfluorooctanesulfonamide754-91-6- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -F-53B MajorF-53B Major73606-19-6- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -F-53B MinorF-53B Minor83329-89-9- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -ADONA4,8-dioxa-3H-perfluorononanoate958445-44-8 - 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -NaDONANaDONAEVS1361- 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -DONADONA919005-14-4 - 100% - - 100% - - 100% - 100% - - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% - - 100% -Notes:1. The source of the mass loading was estimated by compound and pathway as either Site (generated from the Site), Other (generated from Other sources), or Unknown (compound may be generated from either the Site or Other sources).4. For Pathway 3, all Table 3+ compounds were estimated to originate from the Site. All EPA 537 compounds were estimated to originate from Other sources.4. For Pathway 4, all Table 3+ compounds and EPA 537 compounds estimated to originate from the Site. This Pathway only represents new loading introduced by the Site to the river by Outfall 002 and does not account for PFAS present in water collected at the intake. 2. For Pathway 1, Table 3+ compounds were estimated to oringinate from the Site with the exception of Byproduct 4, Byproduct 5 and NVHOS whose detection in upstream river samples was not consistent with known loading pathways for PFAS originating from the Site. The fraction of these compounds originating from the Site was calculated using June event Table 3+ data where the River Mile 76 concentrations of each of the three compounds were subtracted from the River Mile 56 concentrations of each of the three compounds and then deivided by the River Mile 76 concentration. The remainder contriubtion were estimated to originate from unkown sources. All EPA 537 compounds were estimated to originate from Other sources.3. For Pathways 2, 5, 6, and 7, all Table 3+ compounds were estimated to orignate from the Site. For the EPA 537 compounds, the percentage increase between the median Pathway concentration for all sampling events and the median Upriver [Pathway 1] concentration for all sampling events were estimated to originate from the Site. If the Pathway median was not detected or less than the Upriver concentration, then the contribution from the Site was estimated to be 0%. The remaining EPA 537 compound percentages were estimated to originate from Other sources.5. For Pathway 8, all Table 3+ compounds were estimated to originate from the Site. For the EPA 537 compounds, the percentage increase between the estimated median offsite groundwater concentration and the median Upriver [Pathway 1] concentration for all sampling events was esimated to originate from Unknown sources. If the estimated median offsite groundwater concentration was not detected or less than the median Upriver concentration, then the Unknown portion was considered 0%. The remaining EPA 537 compound percentages were estimated to originate from Other sources.6. For Pathway 9, all Table 3+ compounds were estimated to originate from the Site. For the EPA 537 compounds, the percentage increase between the median Pathway concentration for all sampling events and the median Upriver [Pathway 1] concentration for all sampling events was estimated to originate from Unknown sources. If the median Pathway concentration was not detected or less than the median Upriver concentration, then the Unknown portion was considered 0%. The remaining EPA 537 compound percentages were estimated to originate from Other sources.EPA Method 537 Mod6C6DTransport Pathway Number →12345Aerial Deposition on River Outfall 002 Onsite Groundwater6A 6B9Table 3+ Lab SOP78Seep A Seep B Seep C Seep D Old Outfall 002Adjacent and Downstream GroundwaterGeorgia Branch CreekUpstream River and GroundwaterWillis CreekAnalytical MethodCommon Name Chemical NameAugust 2019

FIGURES
")
")
")
Willis Creek
Old Outfall 002Cape Fear RiverOutfall 002
W.O. Huske Dam
Site River Water Intake
NC Highway 87
Seep A
Seep B
Seep C
Seep D
GBCTributary1GeorgiaBranchCreek
Site Location Map
Figure
1Raleigh, NC
2,000 0 2,0001,000 Feet
³
August 2019
Legend
")Site Features
Cape Fear River
Nearby Tributaries
Observed Seep (Natural Drainage)
Site Drainage Network
Site Boundary
Notes:Basemap Sources: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AeroGRID,IGN, and the GIS User Community
Areas at Site
Chemours Monomers IXM
Chemours PPA
Dupont / Dow Leased
Former DuPont PMDF Area
Kuraray America Leased
Wastewater Treatment Plant
Chemours Fayetteville Works, North Carolina
RainRain
Cape F
e
ar
Ri
v
e
r
Cape F
e
ar
Ri
v
e
r
Perched Zo
n
e
Surficial Aq
u
i
f
e
r
Black Cre
e
k
Aquifer
Groun
d
w
a
t
e
r
ChemoursFayetteville WorksManufacturing Area
ChemoursFayetteville WorksManufacturing Area
Perched Zone Clay
Black CreekConfining Unit
Perched Zone Clay
Black CreekConfining Unit
Non-contact cooling water from river
Non-Chemours treated process water
Stormwater
(4) Outfall 002 (Pipe to River)
Groundwater
Seep B
Seep A
Seep C
Seep D
(1) Upstream
Cape Fear River
(3) Aerial Deposition
(9) G
e
orgi
a
Branch Creek
(2) Willis Creek
(
7
)
Old Outfall
0
02(6) Seeps
(
5
) OnSite Groundwater (8) Adjacentand Downstream
(3) Aerial Deposition
(9) G
e
orgi
a
Branch Creek
(2) Willis Creek
(
7
)
Old Outfall
0
02(6) Seeps
(
5
) OnSite Groundwater
(
8
)
A
dja
cent and
W.O. Huske DamW.O. Huske Dam Upper Cape Fear Confining Unit(4) Outfall 002 (Pipe to River)
(1) Upstream
Cape Fear River
Down
stre
a
m Groundwater
(
8
)
A
dja
cent and Down
stre
a
m Groundwater
Groundwater
(8) Adjacentand Downstream

Raleigh, NC August 2019
Figure
2
Potential PFAS Pathways to the Cape Fear River from Site
Chemours Fayetteville Works, North Carolina
Note: Image is conceptual and is not to scale.
Cape Fear Lockand Dam #1/ Kings Bluff Intake Canal
ChemoursFayettevilleWorks
Start ofCape FearRiver
Greensboro
Wilmington
Fayetteville
Raleigh
Bladen Bluffs Intake
WO HuskeLock and Dam
Virginia
NorthCarolina
SouthCarolina
Cape Fear River Watershed and DownstreamPublic Utility Intakes
Chemours Fayetteville Works, North Carolina
Figure
3Raleigh, NC
20 0 2010 Miles
August 2019
Legend
Chemours Fayetteville Works
Cape Fear River
State Boundaries
Upper Basin
Middle Basin
Lower Basin
³Dee
p R
i
v
er HawRiver
LittleRiver
CapeFearRiver
Notes:Basemap and state boundaries provided by Esri, Garmin, USGS, NPS
Comparison of Observed and Best-fit Modeled
Total Table 3+ Mass Loading at Bladen Bluffs
Chemours, Fayetteville Works, North Carolina
Figure
4
Raleigh, NC August 2019
Notes:
-Best-fit model estimated mass loading based on
1st Quartile input parameter value scenario
-Total Table 3+ includes HFPO-DA
(hexaflouropropylene oxide dimer acid)
Acronyms:
-mg/s: milligrams per second
0
2
4
6
8
10
12
14
16
May 2019 June 2019Total Table 3+ Mass Loading (mg/s)Model Estimated Total Table 3+ Mass Loading
Observed Total Table 3+ Mass Loading
Estimated Pathway Contributions to Observed Total Table 3+
Concentrations Adjacent to Bladen Bluffs Intake
Chemours, Fayetteville Works, North Carolina
Figure
5
Raleigh August 2019
0
100
200
300
400
500
600
May JuneObserved Total Table 3+ Concentration (ng/L)Legend:
Upstream River and Groundwater
Willis Creek
Aerial Deposition on River
Outfall 002
Onsite Groundwater
Seeps
Old Outfall 002
Adjacent and Downstream Groundwater
Georgia Branch Creek
Notes: 
‐ February 2019 sampling even not plotted since not all Table 3+ 
compounds were analyzed for in collectedsamples due to 
analytical method not yet being finalized.
‐ Pathway percentage based on Input Parameters 1st Quartile
Values Scenario
‐Total Table 3+ includes HFPO‐DA: (hexaflouropropyleneoxide dimer acid) 
Acronyms:
‐ ng/L: nanograms per liter
Modeled and Empirical HFPO-DA Time Series at Kings Bluff Chemours Fayetteville Works, North CarolinaFigure6Raleigh, NCAugust 2019020406080100120140HFPO‐DA Concentration (ng/L)Modeled ConcentrationKings Bluff Finished Water Detected DataKings Bluff Raw Water Intake Detected DataNotes: ‐ Modeled HFPO‐DA concentrations are calculated based on calculated and estimated mass fluxes from off‐Site and on‐Site groundwater, nearby tributaries, Outfall 002.‐ All water intake HFPO‐DA results are detected. ‐ Plotted Kings Bluff Data are a combined set of publicly accessed data from downriver intakes including Cape Fear Public Utility Authority, North Carolina Department of Environmental Quality, Brunswick County, Pender County and data provided directly from Cape Fear Public Utility Authority.Acronyms: ‐ HFPO‐DA: Hexafluoropropylene oxide dimer acid‐ ng / L: nanograms per liter
Estimated Source of Observed Total PFAS Concentration at Bladen 
Bluffs and Kings Bluff
Chemours Fayetteville Works, North Carolina
Figure
7
Raleigh, NC August 2019
Notes: 
‐ Source of Total PFAS based on the estimated 
contribution percentage of each pathway to the 
total mass loading and the estimated origination 
of that pathway from Site, Other or Unknown 
sources for compounds analyzed for and detected 
in samples of river water.
Acronyms:
‐ PFAS: per‐ and polyflouroalkyl substances
‐ ng/L: nanograms per liter
0
100
200
300
400
500
600
700
Bladen Bluffs Kings Bluff Bladen Bluffs Kings BluffTotal PFAS Concentration (ng/L)PFAS Originating from Facility
PFAS Originating from Other Sources
PFAS Originating from Unknown Sources
May 2019 June 2019

Appendix A – Supplemental Analytical Data 1 August 2019
APPENDIX A
SUPPLEMENTAL ANALYTICAL DATA
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluorooctadecanoic acid 16517-11-6 0.00170 U N 0.00170 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.00260 U N 0.00260 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Hfpo Dimer Acid 13252-13-6 0.00290 J Y 0.00170 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 0.05000 U N 0.05000 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00260 U N 0.00260 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 0.05000 U N 0.05000 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified PFOA 335-67-1 0.00610 Y 0.00087 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.00260 U N 0.00260 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluorododecanoic Acid 307-55-1 0.00170 U N 0.00170 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluorohexanoic Acid 307-24-4 0.00570 Y 0.00170 20279181FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.00790 U UJ N 0.00790 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluorodecanoic Acid 335-76-2 0.00170 U N 0.00170 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluorodecane Sulfonic Acid 335-77-3 0.00170 U N 0.00170 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluorohexane Sulfonic Acid 355-46-4 0.00350 Y 0.00170 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluorobutanoic Acid 375-22-4 0.00520 U N 0.00520 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluorobutane Sulfonic Acid 375-73-5 0.00200 J Y 0.00087 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluoroheptanoic Acid 375-85-9 0.00370 Y 0.00087 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00170 U N 0.00170 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluorononanoic Acid 375-95-1 0.00170 U N 0.00170 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluorotetradecanoic Acid 376-06-7 0.00087 U N 0.00087 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.00520 U N 0.00520 20279181FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.10000 U N 0.10000 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 0.05000 U N 0.05000 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 0.05000 U N 0.05000 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.00790 U UJ N 0.00790 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluorooctane Sulfonamide 754-91-6 0.00260 U N 0.00260 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluorotridecanoic Acid 72629-94-8 0.00087 U N 0.00087 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.05000 U N 0.05000 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified F-53B Major 73606-19-6 0.00087 U UJ N 0.00087 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluorononanesulfonic acid 68259-12-1 0.00170 U N 0.00170 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluorohexadecanoic acid (PFHxDA)67905-19-5 0.00087 U N 0.00087 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 0.05000 U N 0.05000 20279181FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.00260 U N 0.00260 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00170 U N 0.00170 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluoropentanoic Acid 2706-90-3 0.00520 U N 0.00520 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.00170 U N 0.00170 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.05000 U N 0.05000 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 0.05000 U N 0.05000 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.00260 U N 0.00260 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified PFOS 1763-23-1 0.00780 Y 0.00170 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluoroundecanoic Acid 2058-94-8 0.00170 U N 0.00170 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.00260 U N 0.00260 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified F-53B Minor 83329-89-9 0.00170 U UJ N 0.00170 20279181FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified ADONA 958445-44-8 0.00087 U UJ N 0.00087 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 EPA 537 Rev. 1.1 modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00087 U N 0.00087 2027918
1 FAY-SW-CFR-RM-76-020219 LANC CFR-MILE-76 2/4/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.05000 U N 0.05000 2027918
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.00200 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.00410 H Y 0.00200 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.00200 U,H N 0.00200 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 0.01000 U,H N 0.01000 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified Hfpo Dimer Acid 13252-13-6 0.00400 U N 0.00400 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.00200 U,H N 0.00200 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.00200 U,H N 0.00200 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.00200 280-124268-11FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.02000 280-124268-1
Page 1 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.00200 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.00200 U N 0.00200 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.00200 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.00840 Y 0.00200 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00310 Y 0.00200 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.00620 Y 0.00200 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00470 Y 0.00200 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.00200 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.00200 U,H N 0.00200 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.00200 280-124268-11FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.02000 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified PFOA 335-67-1 0.00690 Y 0.00200 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.00200 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 0.00350 H Y 0.00200 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.00200 U,H N 0.00200 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 0.00200 U,H N 0.00200 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 0.00200 U,H N 0.00200 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.00200 U,H N 0.00200 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.02000 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 0.00200 U,H N 0.00200 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 0.00500 U,H N 0.00500 280-124268-31FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.00200 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.00200 U,H N 0.00200 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.00200 U,H N 0.00200 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.00200 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.00200 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.02000 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.00200 U,H N 0.00200 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.00200 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified PFOS 1763-23-1 0.01300 Y 0.00200 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 0.02000 U,H N 0.02000 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.00200 U,H N 0.00200 280-124268-31FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.02000 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 0.01200 Y 0.00200 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.00200 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.00200 U,H N 0.00200 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.00200 280-124268-1
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 0.00520 H,F1 J Y 0.00200 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 0.00200 U,H,F1 N 0.00200 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 0.00200 U,H,F1 N 0.00200 280-124268-3
1 FAY-SW-CFR-RM-76-052219 TAL-SAC CFR-MILE-76 5/22/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.00200 U,H N 0.00200 280-124268-3
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.00200 U N 0.00200 280-124971-11FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified Hfpo Dimer Acid 13252-13-6 0.00690 Y 0.00400 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 0.01800 Y 0.01000 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.00740 Y 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 0.00440 Y 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.02000 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified PFOA 335-67-1 0.00830 Y 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.02000 280-124971-11FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.00200 280-124971-1
Page 2 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00680 Y 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.00850 Y 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00450 Y 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.01200 Y 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.00200 U N 0.00200 280-124971-11FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 0.00500 U N 0.00500 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.02000 280-124971-11FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 0.02000 Y 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.02000 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 0.02000 U N 0.02000 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified PFOS 1763-23-1 0.01500 I Y 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.02000 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 0.00790 F1 J Y 0.00200 280-124971-11FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 0.00200 F1,^J Y 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 0.02300 F1,^J Y 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.00200 280-124971-1
1 FAY-SW-CFR-RM-76-060719 TAL-SAC CFR-MILE-76 6/7/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.00200 U N 0.00200 280-124971-1
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U,H N 0.04600 320-51045-1
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00260 U N 0.00260 2028553
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.05400 U,H N 0.05400 320-51045-1
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U,H N 0.06000 320-51045-1
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Hfpo Dimer Acid 13252-13-6 0.29000 J Y 0.00170 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 0.44000 Y 0.05000 2028553
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 1.20000 H Y 0.57000 320-51045-12FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorooctadecanoic acid 16517-11-6 0.00170 U N 0.00170 2028553
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.01500 U,H N 0.01500 320-51045-1
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.00770 U UJ N 0.00770 2028553
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U,H N 0.03500 320-51045-1
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified PFOA 335-67-1 0.00470 Y 0.00085 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorododecanoic Acid 307-55-1 0.00170 U N 0.00170 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorohexanoic Acid 307-24-4 0.00250 Y 0.00170 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.00260 U N 0.00260 2028553
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.02700 U,H N 0.02700 320-51045-1
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorodecanoic Acid 335-76-2 0.00170 U N 0.00170 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorodecane Sulfonic Acid 335-77-3 0.00170 U N 0.00170 20285532FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorobutane Sulfonic Acid 375-73-5 0.00310 Y 0.00085 2028553
Page 3 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorobutanoic Acid 375-22-4 0.00540 Y 0.00510 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorohexane Sulfonic Acid 355-46-4 0.00170 U N 0.00170 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluoroheptanoic Acid 375-85-9 0.00180 Y 0.00085 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00170 U N 0.00170 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorotetradecanoic Acid 376-06-7 0.00085 U N 0.00085 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.00510 U N 0.00510 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorononanoic Acid 375-95-1 0.00170 U N 0.00170 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.00770 U UJ N 0.00770 2028553
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U,H N 0.03700 320-51045-1
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.10000 U N 0.10000 20285532FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.03400 H Y 0.03400 320-51045-1
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 0.05000 U N 0.05000 2028553
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 0.07900 U,H N 0.07900 320-51045-1
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 0.31000 Y 0.05000 2028553
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 0.33000 H Y 0.08100 320-51045-1
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 0.05200 Y 0.05000 2028553
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 0.05800 H Y 0.05800 320-51045-1
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.05000 U N 0.05000 2028553
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.03000 U,H N 0.03000 320-51045-1
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.02400 U,H N 0.02400 320-51045-1
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorotridecanoic Acid 72629-94-8 0.00085 U N 0.00085 20285532FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified F-53B Major 73606-19-6 0.00085 U UJ N 0.00085 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 0.49000 Y 0.05000 2028553
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 0.21000 U,H N 0.21000 320-51045-1
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorononanesulfonic acid 68259-12-1 0.00170 U N 0.00170 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorohexadecanoic acid (PFHxDA)67905-19-5 0.00085 U N 0.00085 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorooctane Sulfonamide 754-91-6 0.00260 U N 0.00260 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.00260 U N 0.00260 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.05000 U N 0.05000 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.00260 U N 0.00260 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.00260 U UJ N 0.00260 2028553
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U,H N 0.11000 320-51045-12FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified PFOS 1763-23-1 0.00230 Y 0.00170 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluoroundecanoic Acid 2058-94-8 0.00170 U N 0.00170 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.00260 U UJ N 0.00260 2028553
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U,H N 0.06000 320-51045-1
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 0.13000 Y 0.05000 2028553
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 0.19000 H Y 0.04700 320-51045-1
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.00170 U N 0.00170 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00170 U N 0.00170 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluoropentanoic Acid 2706-90-3 0.00670 Y 0.00510 2028553
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 0.16000 U,H N 0.16000 320-51045-1
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 0.07000 U,H N 0.07000 320-51045-12FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.05000 U N 0.05000 2028553
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U,H N 0.04100 320-51045-1
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified F-53B Minor 83329-89-9 0.00170 U UJ N 0.00170 2028553
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified ADONA 958445-44-8 0.00085 U UJ N 0.00085 2028553
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 0.02800 U,H N 0.02800 320-51045-1
2 FAY-SW-WC-1-020719 LANC WC-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00085 U N 0.00085 2028553
2 FAY-SW-WC-1-020719 TAL-SAC WC-1 2/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 0.09100 H Y 0.05800 320-51045-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U N 0.06000 280-124323-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 2.40000 Y 0.57000 280-124323-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.05400 U N 0.05400 280-124323-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U N 0.04600 280-124323-12FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.01500 U N 0.01500 280-124323-1
Page 4 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.02700 U N 0.02700 280-124323-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U N 0.03500 280-124323-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 0.38000 Y 0.05800 280-124323-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 2.00000 Y 0.08100 280-124323-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 0.20000 Y 0.07900 280-124323-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.03400 U N 0.03400 280-124323-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U N 0.03700 280-124323-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 1.30000 Y 0.21000 280-124323-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.02400 U N 0.02400 280-124323-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.05900 Y 0.03000 280-124323-12FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 0.72000 Y 0.04700 280-124323-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U N 0.06000 280-124323-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U N 0.11000 280-124323-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 0.05800 U,F1 UJ N 0.05800 280-124323-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 0.02800 U N 0.02800 280-124323-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U N 0.04100 280-124323-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 0.07000 U N 0.07000 280-124323-1
2 FAY-SW-WC-1-TR2-052219 TAL-SAC WC-1 5/22/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 0.16000 U N 0.16000 280-124323-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U,H N 0.04600 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.05400 U,H N 0.05400 280-124599-12FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 1.20000 H Y 0.57000 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified Hfpo Dimer Acid 13252-13-6 0.81000 E Y 0.00400 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U,H N 0.06000 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.01500 U,H N 0.01500 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U,H N 0.03500 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified PFOA 335-67-1 0.00880 Y 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.02700 U,H N 0.02700 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.02000 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.00200 U N 0.00200 280-124599-12FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.00260 Y 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00220 I Y 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00360 Y 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.01000 Y 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.02000 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U,H N 0.03700 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.04500 H Y 0.03400 280-124599-12FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 0.07900 U,H N 0.07900 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 0.73000 H Y 0.08100 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 0.12000 H Y 0.05800 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.03000 U,H N 0.03000 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.02400 U,H N 0.02400 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 1.40000 H Y 0.21000 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.02000 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U,H N 0.11000 280-124599-12FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.02000 280-124599-1
Page 5 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U,H N 0.06000 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified PFOS 1763-23-1 0.00420 I Y 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 0.24000 H Y 0.04700 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 0.01200 Y 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.02000 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 0.16000 U,H N 0.16000 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 0.07000 U,H N 0.07000 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U,H N 0.04100 280-124599-12FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 0.02800 U,H N 0.02800 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.00200 280-124599-1
2 FAY-SW-WC-1-053019 TAL-SAC WC-1 5/30/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 0.22000 H,F1 J Y 0.05800 280-124599-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.00200 U,H N 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified Hfpo Dimer Acid 13252-13-6 0.32000 Y 0.00400 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 0.54000 H,F1 J Y 0.01000 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.01400 H Y 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.00200 U,H N 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.00200 U,H N 0.00200 280-124971-12FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.02000 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.00870 Y 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00370 Y 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00260 Y 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.00250 Y 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.00200 U N 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.00200 280-124971-12FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.02000 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.00200 U,H N 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified PFOA 335-67-1 0.00550 Y 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.00200 U,H,*N 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 0.06700 H Y 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 0.42000 H,F1 J Y 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 0.01600 H Y 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.00400 H,*J Y 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.00200 U,H,*N 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.02000 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.00200 280-124971-12FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 0.81000 H Y 0.00500 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.00200 U,H N 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.01700 H Y 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.02000 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 0.00970 Y 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 0.14000 H Y 0.02000 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified PFOS 1763-23-1 0.00360 I Y 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.00200 280-124971-12FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.00200 U,H N 0.00200 280-124971-1
Page 6 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.02000 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.00200 U,H N 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 0.27000 H,F1 J Y 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 0.00540 H Y 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.00200 U,H N 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 0.02800 H,F1 J Y 0.00200 280-124971-1
2 FAY-SW-WC-1-060719 TAL-SAC WC-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 0.04100 H,F1 J Y 0.00200 280-124971-1
4 O90618 Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.02700 H Y 0.01000 280-125541-1
4 O90620 Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.03300 H Y 0.01000 280-125541-14O90625Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.04400 Y 0.01000 280-125815-1
4 O90627 Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.02800 Y 0.01000 280-125815-1
4 O90701 Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.03300 Y 0.01000 280-125979-1
4 O90703 Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.04200 Y 0.01000 280-125979-1
4 O90708 Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.32000 Y 0.01000 280-126229-1
4 O90712 Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.06800 Y 0.01000 280-126229-1
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.00492 Y 0.01136
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00091 Y 0.00120
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.01215 Y 0.00481
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.03812 Y 0.01168
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00035 Y 0.00346
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.00798 Y 0.02348
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.00771 Y 0.00936
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.02806 Y 0.00481
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.00773 Y 0.00925
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.01155 Y 0.00815
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.01135 Y 0.00703
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.01632 N 0.01632
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.02213 Y 0.01055
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.00215 Y 0.00521
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.01210 Y 0.00729
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00268 Y 0.00204
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00048 Y 0.00619
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.00183 Y 0.01075
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.00302 Y 0.00729
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.00554 Y 0.00665
4 O90503.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00171 Y 0.00115
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.02926 Y 0.01136
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00109 Y 0.00120
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.02522 Y 0.00481
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.14104 Y 0.01168
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00028 Y 0.00346
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.01249 Y 0.02348
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.42711 Y 0.00936
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.04330 Y 0.00481
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.01617 Y 0.00925
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.01226 Y 0.00815
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.01229 Y 0.00703
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.02079 Y 0.01632
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.02767 Y 0.01055
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.00780 Y 0.00521
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.03906 Y 0.00729
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00473 Y 0.00204
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00054 Y 0.006194O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.00138 Y 0.01075
Page 7 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.00949 Y 0.00729
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.00961 Y 0.00665
4 O90507.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00281 Y 0.00115
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.00701 Y 0.01136
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00088 Y 0.00120
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.01036 Y 0.00481
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.17133 Y 0.01168
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00028 Y 0.00346
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.00521 Y 0.02348
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.01767 Y 0.00936
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.02595 Y 0.00481
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.00570 Y 0.00925
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.00443 Y 0.00815
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.00301 Y 0.00703
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.05074 Y 0.01632
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.02653 Y 0.01055
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.00807 Y 0.00521
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.01955 Y 0.00729
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00369 Y 0.00204
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00060 Y 0.00619
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.00092 Y 0.01075
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.01607 Y 0.00729
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.00525 Y 0.00665
4 O90509.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00485 Y 0.00115
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.01027 Y 0.01136
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00094 Y 0.00120
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.01183 Y 0.00481
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.04667 Y 0.01168
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00023 Y 0.00346
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.00576 Y 0.02348
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.02445 Y 0.00936
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.03233 Y 0.00481
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.00581 Y 0.00925
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.00541 Y 0.00815
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.00382 Y 0.00703
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.01632 N 0.01632
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.02563 Y 0.01055
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.00398 Y 0.00521
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.01643 Y 0.00729
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00141 Y 0.00204
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00044 Y 0.00619
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.00064 Y 0.01075
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.03676 Y 0.00729
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.00433 Y 0.00665
4 O90514.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00221 Y 0.00115
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.00782 Y 0.01136
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00073 Y 0.00120
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.01538 Y 0.00481
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.04658 Y 0.01168
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00346 N 0.00346
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.00487 Y 0.02348
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.00588 Y 0.00936
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.03903 Y 0.00481
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.01745 Y 0.009254O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.01569 Y 0.00815
Page 8 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.01703 Y 0.00703
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.01632 N 0.01632
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.03194 Y 0.01055
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.00096 Y 0.00521
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.01319 Y 0.00729
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00154 Y 0.00204
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00619 N 0.00619
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.00137 Y 0.01075
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.00237 Y 0.00729
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.00204 Y 0.00665
4 O90517.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00166 Y 0.00115
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.01014 Y 0.01136
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00096 Y 0.00120
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.01287 Y 0.00481
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.04363 Y 0.01168
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00346 Y 0.00346
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.00315 Y 0.02348
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.01787 Y 0.00936
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.03188 Y 0.00481
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.00756 Y 0.00925
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.00784 Y 0.00815
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.00580 Y 0.00703
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.02336 Y 0.01632
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.01631 Y 0.01055
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.00126 Y 0.00521
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.01907 Y 0.00729
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00175 Y 0.00204
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00619 N 0.00619
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.00091 Y 0.01075
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.00364 Y 0.00729
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.00183 Y 0.00665
4 O90521.d Onsite-Lab Outfall 002 5/21/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00183 Y 0.00115
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.04117 Y 0.01136
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00099 Y 0.00120
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.01345 Y 0.00481
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.03283 Y 0.01168
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00346 Y 0.00346
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.02348 N 0.02348
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.00893 Y 0.00936
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.32383 Y 0.00481
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.13017 Y 0.00925
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.06571 Y 0.00815
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.02014 Y 0.00703
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.06665 Y 0.01632
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.46102 Y 0.01055
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.00174 Y 0.00521
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.04693 Y 0.00729
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00541 Y 0.00204
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00007 Y 0.00619
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.00081 Y 0.01075
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.00451 Y 0.00729
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.01186 Y 0.00665
4 O90524.d Onsite-Lab Outfall 002 5/24/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00206 Y 0.00115
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.13190 Y 0.011364O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00090 Y 0.00120
Page 9 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.02723 Y 0.00481
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.05115 Y 0.01168
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00006 Y 0.00346
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.00725 Y 0.02348
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.01847 Y 0.00936
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.90548 Y 0.00481
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.37753 Y 0.00925
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.21774 Y 0.00815
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.08791 Y 0.00703
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.19608 Y 0.01632
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 1.30581 Y 0.01055
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.00648 Y 0.00521
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.17692 Y 0.00729
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.01684 Y 0.00204
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00026 Y 0.00619
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.00054 Y 0.01075
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.01783 Y 0.00729
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.06386 Y 0.00665
4 O90528.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00468 Y 0.00115
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.07938 Y 0.01136
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00076 Y 0.00120
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.01617 Y 0.00481
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.03732 Y 0.01168
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00346 Y 0.00346
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.00420 Y 0.02348
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.01820 Y 0.00936
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.39842 Y 0.00481
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.19131 Y 0.00925
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.12740 Y 0.00815
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.06211 Y 0.00703
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.08853 Y 0.01632
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.52438 Y 0.01055
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.00635 Y 0.00521
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.13270 Y 0.00729
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00957 Y 0.00204
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00619 N 0.00619
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.00064 Y 0.01075
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.01767 Y 0.00729
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.07475 Y 0.00665
4 O90531.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00367 Y 0.00115
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.06789 Y 0.01136
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00081 Y 0.00120
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.02439 Y 0.00481
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.16473 Y 0.01168
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00008 Y 0.00346
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.00909 Y 0.02348
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.32104 Y 0.00936
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.21141 Y 0.00481
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.09458 Y 0.00925
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.07933 Y 0.00815
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.05027 Y 0.00703
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.06669 Y 0.01632
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.24148 Y 0.01055
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.01682 Y 0.005214O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.15901 Y 0.00729
Page 10 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00795 Y 0.00204
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00024 Y 0.00619
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.00159 Y 0.01075
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.02568 Y 0.00729
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.05853 Y 0.00665
4 O90604.d Onsite-Lab Outfall 002 6/4/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00458 Y 0.00115
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.03399 Y 0.01136
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00103 Y 0.00120
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.01474 Y 0.00481
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.06911 Y 0.01168
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00346 N 0.00346
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.00466 Y 0.02348
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.06998 Y 0.00936
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.12436 Y 0.00481
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.05139 Y 0.00925
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.04905 Y 0.00815
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.04487 Y 0.00703
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.00326 Y 0.01632
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.11977 Y 0.01055
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.00779 Y 0.00521
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.12631 Y 0.00729
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00677 Y 0.00204
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00619 N 0.00619
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.00119 Y 0.01075
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.01750 Y 0.00729
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.05674 Y 0.00665
4 O90607.d Onsite-Lab Outfall 002 6/7/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00329 Y 0.00115
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.01727 Y 0.01136
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00058 Y 0.00120
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.00597 Y 0.00481
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.06227 Y 0.01168
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00346 N 0.00346
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.00926 Y 0.02348
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.03956 Y 0.00936
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.04386 Y 0.00481
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.02026 Y 0.00925
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.02288 Y 0.00815
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.03547 Y 0.00703
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.37986 Y 0.01632
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.07790 Y 0.01055
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.01267 Y 0.00521
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.11140 Y 0.00729
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00326 Y 0.00204
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00094 Y 0.00619
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.00007 Y 0.01075
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.01409 Y 0.00729
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.09535 Y 0.00665
4 O90614.d Onsite-Lab Outfall 002 6/14/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00350 Y 0.00115
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.01077 Y 0.01136
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00060 Y 0.00120
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.00481 N 0.00481
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.01439 Y 0.01168
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00346 N 0.00346
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.02348 N 0.023484O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.00883 Y 0.00936
Page 11 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.02762 Y 0.00481
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.00994 Y 0.00925
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.01098 Y 0.00815
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.02102 Y 0.00703
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.01632 N 0.01632
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.01082 Y 0.01055
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.00191 Y 0.00521
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.07616 Y 0.00729
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00058 Y 0.00204
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00061 Y 0.00619
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.00031 Y 0.01075
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.00039 Y 0.00729
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.01185 Y 0.00665
4 O90618.d Onsite-Lab Outfall 002 6/18/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00298 Y 0.00115
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.00836 Y 0.01136
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00058 Y 0.00120
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.00481 N 0.00481
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.01883 Y 0.01168
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00346 N 0.00346
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.02348 N 0.02348
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.01240 Y 0.00936
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.02365 Y 0.00481
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.00827 Y 0.00925
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.00709 Y 0.00815
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.01661 Y 0.00703
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.07908 Y 0.01632
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.01000 Y 0.01055
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.00289 Y 0.00521
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.07029 Y 0.00729
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00039 Y 0.00204
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00071 Y 0.00619
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.01075 N 0.01075
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.00211 Y 0.00729
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.01152 Y 0.00665
4 O90620.d Onsite-Lab Outfall 002 6/20/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00291 Y 0.00115
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.01131 Y 0.01136
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00057 Y 0.00120
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.00481 N 0.00481
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.03321 Y 0.01168
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00346 N 0.00346
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.02348 N 0.02348
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.04251 Y 0.00936
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.02653 Y 0.00481
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.00954 Y 0.00925
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.01040 Y 0.00815
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.01570 Y 0.00703
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.01632 N 0.01632
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.00181 Y 0.01055
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.00491 Y 0.00521
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.08031 Y 0.00729
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00174 Y 0.00204
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00060 Y 0.00619
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.00023 Y 0.01075
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.00729 N 0.007294O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.01138 Y 0.00665
Page 12 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
4 O90625.d Onsite-Lab Outfall 002 6/25/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00254 Y 0.00115
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.00965 Y 0.01136
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00061 Y 0.00120
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.00481 N 0.00481
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.01337 Y 0.01168
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00346 N 0.00346
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.02348 N 0.02348
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.07597 Y 0.00936
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.01675 Y 0.00481
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.00545 Y 0.00925
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.00815 N 0.00815
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.01156 Y 0.00703
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.01632 N 0.01632
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.00580 Y 0.01055
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.00502 Y 0.00521
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.07592 Y 0.00729
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00047 Y 0.00204
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00063 Y 0.00619
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.01075 N 0.01075
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.00031 Y 0.00729
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.00968 Y 0.00665
4 O90628.d Onsite-Lab Outfall 002 6/28/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00236 Y 0.00115
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.00137 Y 0.01136
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00054 Y 0.00120
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.00481 N 0.00481
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.02300 Y 0.01168
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00346 N 0.00346
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.02348 N 0.02348
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.01027 Y 0.00936
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.02970 Y 0.00481
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.00889 Y 0.00925
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.00938 Y 0.00815
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.01686 Y 0.00703
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.03549 Y 0.01632
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.01161 Y 0.01055
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.00290 Y 0.00521
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.06679 Y 0.00729
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00087 Y 0.00204
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00075 Y 0.00619
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.00011 Y 0.01075
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.00729 N 0.00729
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.00835 Y 0.00665
4 O90701.d Onsite-Lab Outfall 002 7/1/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00261 Y 0.00115
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.01322 Y 0.01136
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00058 Y 0.00120
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.00481 N 0.00481
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.02203 Y 0.01168
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00346 N 0.00346
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.02348 N 0.02348
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.02986 Y 0.00936
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.02814 Y 0.00481
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.00646 Y 0.00925
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.00691 Y 0.00815
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.00752 Y 0.007034O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.02734 Y 0.01632
Page 13 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.00682 Y 0.01055
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.00766 Y 0.00521
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.06523 Y 0.00729
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00060 Y 0.00204
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00068 Y 0.00619
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.00007 Y 0.01075
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.00154 Y 0.00729
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.00917 Y 0.00665
4 O90703.d Onsite-Lab Outfall 002 7/3/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00204 Y 0.00115
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.03117 Y 0.01136
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00057 Y 0.00120
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.01288 Y 0.00481
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.25504 Y 0.01168
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00346 N 0.00346
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.00102 Y 0.02348
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.08267 Y 0.00936
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.08130 Y 0.00481
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.02275 Y 0.00925
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.01411 Y 0.00815
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.01599 Y 0.00703
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.02674 Y 0.01632
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.01486 Y 0.01055
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.00023 Y 0.00521
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.11438 Y 0.00729
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00058 Y 0.00204
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00066 Y 0.00619
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.00091 Y 0.01075
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.00563 Y 0.00729
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.01478 Y 0.00665
4 O90708.d Onsite-Lab Outfall 002 7/8/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00310 Y 0.00115
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.00975 Y 0.01136
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00059 Y 0.00120
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.00481 N 0.00481
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.04042 Y 0.01168
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00346 N 0.00346
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.02348 N 0.02348
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.02327 Y 0.00936
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.02695 Y 0.00481
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.00548 Y 0.00925
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.00708 Y 0.00815
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.00627 Y 0.00703
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.07399 Y 0.01632
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.00323 Y 0.01055
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.00372 Y 0.00521
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.06017 Y 0.00729
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00194 Y 0.00204
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00061 Y 0.00619
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.01075 N 0.01075
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.00729 N 0.00729
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.00681 Y 0.00665
4 O90712.d Onsite-Lab Outfall 002 7/12/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00227 Y 0.00115
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab NVHOS 1132933-86-8 0.00178 Y 0.01136
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab PES 113507-82-7 0.00051 Y 0.00120
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab PMPA 13140-29-9 0.00481 N 0.004814O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.04631 Y 0.01168
Page 14 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab PFECA_B 151772-58-6 0.00346 N 0.00346
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab PEPA 267239-61-2 0.02348 N 0.02348
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab Byproduct 1 29311-67-9 0.01412 Y 0.00936
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab PFO2HxA 39492-88-1 0.01526 Y 0.00481
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab PFO3OA 39492-89-2 0.00260 Y 0.00925
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab PFO4DA 39492-90-5 0.00327 Y 0.00815
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab PFO5DA 39492-91-6 0.00558 Y 0.00703
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab PPF Acid 422-64-0 0.00496 Y 0.01632
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.01055 N 0.01055
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab EVE-Acid 69087-46-3 0.00365 Y 0.00521
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab Byproduct 2 749836-20-2 0.04769 Y 0.00729
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab Hydro-EVE Acid 773804-62-9 0.00039 Y 0.00204
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab PFECA_G 801212-59-9 0.00071 Y 0.00619
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab R-EVE EVS1428 0.01075 N 0.01075
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab Byproduct 4 EVS1429 0.00064 Y 0.00729
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab Byproduct 5 EVS1430 0.00754 Y 0.00665
4 O90716.d Onsite-Lab Outfall 002 7/16/2019 Preliminary data from Onsite Lab Byproduct 6 EVS1431 0.00131 Y 0.00115
4 O90716.d Onsite-Lab Outfall 002 1/3/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.19000 Y
4 O90716.d Onsite-Lab Outfall 002 1/7/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.34000 Y
4 O90716.d Onsite-Lab Outfall 002 1/10/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.11000 Y
4 O90716.d Onsite-Lab Outfall 002 1/14/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.24000 Y
4 O90716.d Onsite-Lab Outfall 002 1/17/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.09200 Y
4 O90716.d Onsite-Lab Outfall 002 1/22/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.19000 Y
4 O90716.d Onsite-Lab Outfall 002 1/25/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.34000 Y
4 O90716.d Onsite-Lab Outfall 002 1/28/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.08500 Y
4 O90716.d Onsite-Lab Outfall 002 2/1/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.08800 Y
4 O90716.d Onsite-Lab Outfall 002 2/4/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.09100 Y
4 O90716.d Onsite-Lab Outfall 002 2/7/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.08800 Y
4 O90716.d Onsite-Lab Outfall 002 2/11/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.09000 Y
4 O90716.d Onsite-Lab Outfall 002 2/14/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.24000 Y
4 O90716.d Onsite-Lab Outfall 002 2/18/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.15000 Y
4 O90716.d Onsite-Lab Outfall 002 2/25/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.35000 Y
4 O90716.d Onsite-Lab Outfall 002 2/28/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.05400 Y
4 O90716.d Onsite-Lab Outfall 002 3/4/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.29000 Y
4 O90716.d Onsite-Lab Outfall 002 3/7/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.06200 Y
4 O90716.d Onsite-Lab Outfall 002 3/11/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.11000 Y
4 O90716.d Onsite-Lab Outfall 002 3/14/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.04900 Y
4 O90716.d Onsite-Lab Outfall 002 3/18/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.12000 Y
4 O90716.d Onsite-Lab Outfall 002 3/21/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.07200 Y
4 O90716.d Onsite-Lab Outfall 002 3/25/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.08700 Y
4 O90716.d Onsite-Lab Outfall 002 3/28/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.11000 Y
4 O90716.d Onsite-Lab Outfall 002 4/1/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.06800 Y
4 O90716.d Onsite-Lab Outfall 002 4/5/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.35000 Y
4 O90716.d Onsite-Lab Outfall 002 4/8/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.04800 Y
4 O90716.d Onsite-Lab Outfall 002 4/9/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.24000 Y
4 O90716.d Onsite-Lab Outfall 002 4/12/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.07300 Y
4 O90716.d Onsite-Lab Outfall 002 4/16/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.14000 Y
4 O90716.d Onsite-Lab Outfall 002 4/18/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.04800 Y
4 O90716.d Onsite-Lab Outfall 002 4/23/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.14000 Y
4 O90716.d Onsite-Lab Outfall 002 4/24/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.06200 Y
4 O90716.d Onsite-Lab Outfall 002 4/26/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.05900 Y
4 O90716.d Onsite-Lab Outfall 002 4/30/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.05800 Y
4 O90716.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.05600 Y
4 O90716.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.19000 Y4O90716.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.29000 Y
Page 15 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
4 O90716.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.08300 Y
4 O90716.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.04700 Y
4 O90716.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.07600 Y
4 O90716.d Onsite-Lab Outfall 002 5/30/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.09950 Y
4 O90716.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab HFPO-DA 13252-13-6 0.06800 Y
4 O90716.d Onsite-Lab Outfall 002 1/28/2019 Preliminary data from Onsite Lab PFOA 335-67-1 0.08500 Y
4 O90716.d Onsite-Lab Outfall 002 2/18/2019 Preliminary data from Onsite Lab PFOA 335-67-1 0.15000 Y
4 O90716.d Onsite-Lab Outfall 002 2/4/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 2/7/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 2/11/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 2/14/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 2/18/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 2/25/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 2/28/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 3/4/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 1.30000 Y
4 O90716.d Onsite-Lab Outfall 002 3/7/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.72000 Y
4 O90716.d Onsite-Lab Outfall 002 3/11/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 3/14/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 3/18/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 3/21/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 3/25/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 3/28/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 4/1/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 4/5/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 4/8/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 4/9/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 4/12/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 4/16/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 4/18/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 4/23/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.12000 Y
4 O90716.d Onsite-Lab Outfall 002 4/24/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 4/26/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.07000 Y
4 O90716.d Onsite-Lab Outfall 002 4/30/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 5/3/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 5/7/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 5/9/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 5/14/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 5/17/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 5/20/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 0.21000 N
4 O90716.d Onsite-Lab Outfall 002 5/28/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 5.50000 Y
4 O90716.d Onsite-Lab Outfall 002 5/30/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 2.55000 Y
4 O90716.d Onsite-Lab Outfall 002 5/31/2019 Preliminary data from Onsite Lab PFMOAA 674-13-5 2.10000 Y
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U N 0.060 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 0.57000 U N 0.57 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U N 0.046 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.05400 U N 0.054 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.01500 U N 0.015 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U,F1 UJ N 0.035 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.02700 U N 0.027 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 0.08100 U N 0.081 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 0.05800 U N 0.058 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 0.07900 U N 0.079 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.03400 U N 0.034 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U,F1 UJ N 0.037 280-124212-14DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 0.21000 U N 0.21 280-124212-1
Page 16 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.03000 U N 0.030 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.02400 U N 0.024 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 0.04700 U N 0.047 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U N 0.060 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U N 0.11 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U N 0.041 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 0.02800 U N 0.028 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 0.07000 U N 0.070 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 0.16000 U N 0.16 280-124212-1
4 DSTW-OUTFALL 002-052019 TAL-SAC Outfall 002 5/20/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 0.05800 U N 0.058 280-124212-14FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U,H N 0.046 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.10000 H Y 0.054 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 0.64000 H Y 0.57 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP Hfpo Dimer Acid 13252-13-6 0.11000 H Y 0.086 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U,H N 0.060 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U,H N 0.060 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U,H N 0.035 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 0.64000 H Y 0.081 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.14000 H Y 0.034 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 0.22000 H Y 0.079 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 0.32000 H Y 0.058 280-124597-14FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U,H N 0.037 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.19000 H Y 0.030 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.02400 U,H N 0.024 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 2.50000 H Y 0.21 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 0.02800 U,H N 0.028 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U,H N 0.11 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 0.04700 U,H N 0.047 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.03000 H Y 0.027 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.01500 U,H N 0.015 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 1.30000 H,F1 J Y 0.058 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 0.23000 H Y 0.16 280-124597-14FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 0.07000 U,H N 0.070 280-124597-1
4 FAY-DSTW-OUTFALL002-053019 TAL-SAC Outfall 002 5/30/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U,H N 0.041 280-124597-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00000 U N 0.0020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified Hfpo Dimer Acid 13252-13-6 0.01200 U,H N 0.0060 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00000 Y 0.0040 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.00000 U,H N 0.057 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00000 H Y 0.0054 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.00000 U N 0.0020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified PFOA 335-67-1 0.00000 U,H N 0.0046 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00000 H Y 0.0020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00000 U N 0.020 280-124971-14WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.00000 U N 0.0020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00000 U N 0.020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.00000 H Y 0.0027 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00000 U,H,*N 0.0035 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00000 Y 0.0020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00000 U N 0.0020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.00000 U N 0.0020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.00000 Y 0.0020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00000 Y 0.0020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00000 Y 0.0020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00000 Y 0.0020 280-124971-14WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.00000 U N 0.0020 280-124971-1
Page 17 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00000 U N 0.0020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 0.00000 U N 0.0020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.00000 H,*J Y 0.0034 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified PFOS 1763-23-1 0.00000 H Y 0.0081 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00000 H Y 0.0058 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00000 H Y 0.0079 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.00000 U N 0.020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.00000 U N 0.0020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 0.09700 U,H,*N 0.0037 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 0.55440 U N 0.0020 280-124971-14WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.00400 H Y 0.021 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.00280 H Y 0.0030 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 0.00450 H Y 0.0024 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.00000 U N 0.0020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.00000 U N 0.020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.03370 U N 0.0020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 0.00000 Y 0.0020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.00000 U,H N 0.020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.00000 U N 0.020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.00000 U,H N 0.011 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.01400 U,H N 0.0060 280-124971-14WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.21000 Y 0.0020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 0.48000 U N 0.0020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 0.09000 U N 0.0020 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 0.05130 H Y 0.0028 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 0.04600 U,H N 0.0041 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.06100 H Y 0.0070 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 0.00000 H Y 0.016 280-124971-1
4 WSTW-OUTFALL 002-060719 TAL-SAC Outfall 002 6/7/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 0.01300 H Y 0.0058 280-124971-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 22.00000 H,F1 J Y 17 320-44881-3
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Hfpo Dimer Acid 13252-13-6 24.00000 Y 0.13 320-44881-15PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 4.50000 U,H N 4.5 320-44881-3
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified PFOS 1763-23-1 0.01200 Y 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 3.30000 U,H N 3.3 320-44881-3
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 20.00000 U,H UJ N 20 320-44881-3
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluoropentanoic Acid 2706-90-3 0.47000 Y 0.043 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 23.00000 U,H UJ N 23 320-44881-35PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluorohexanoic Acid 307-24-4 0.02600 Y 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 10.00000 U,H,*,F1 UJ N 10 320-44881-3
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified PFOA 335-67-1 0.03400 Y 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00540 Y 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluorobutanoic Acid 375-22-4 0.19000 Y 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00220 Y 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluoroheptanoic Acid 375-85-9 0.05000 Y 0.0020 320-44881-15PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 320-44881-1
Page 18 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluorononanoic Acid 375-95-1 0.00210 Y 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 35.00000 H,F1 J Y 18 320-44881-3
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 18.00000 U,H UJ N 18 320-44881-3
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 19.00000 U,H UJ N 19 320-44881-3
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 21.00000 U,H UJ N 21 320-44881-3
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 16.00000 U,H,*UJ N 16 320-44881-3
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 59.00000 H Y 19 320-44881-3
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluorohexadecanoic acid (PFHxDA)67905-19-5 0.00200 U N 0.0020 320-44881-15PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified F-53B Major 73606-19-6 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 19.00000 U,H UJ N 19 320-44881-3
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U,F1 N 0.020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 19.00000 U,H UJ N 19 320-44881-3
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified F-53B Minor 83329-89-9 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified ADONA 958445-44-8 0.00210 U N 0.0021 320-44881-1
5 PF1018-LTW-01 TAL-SAC LTW-01 10/31/2018 537 Modified NaDONA EVS1361 0.00210 U N 0.0021 320-44881-15PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 8.40000 U,H,F1 N 8.4 320-41147-1
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Hfpo Dimer Acid 13252-13-6 8.30000 Y 0.12 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 2.30000 U,H N 2.3 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified PFOS 1763-23-1 0.00200 U N 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 1.70000 U,H N 1.7 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 10.00000 U,H N 10 320-41147-1
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluoropentanoic Acid 2706-90-3 0.25000 Y 0.0020 19657805PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 12.00000 U,H UJ N 12 320-41147-1
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluorohexanoic Acid 307-24-4 0.00860 Y 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 5.20000 U,H,F1,*UJ N 5.2 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified PFOA 335-67-1 0.00200 U N 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00200 U N 0.0020 19657805PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluorobutanoic Acid 375-22-4 0.06700 Y 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00200 U N 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluoroheptanoic Acid 375-85-9 0.01200 Y 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluorononanoic Acid 375-95-1 0.00200 U N 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 15.00000 H Y 9.2 320-41147-1
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 8.80000 U,H,F1 N 8.8 320-41147-1
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 9.70000 U,H N 9.7 320-41147-1
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 11.00000 U,H UJ N 11 320-41147-15PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 8.20000 U,H,F1,*UJ N 8.2 1965780
Page 19 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 44.00000 H Y 9.5 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluorohexadecanoic acid (PFHxDA)67905-19-5 0.00200 U N 0.0020 320-41147-1
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified F-53B Major 73606-19-6 0.00200 U N 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 9.50000 U,H,F1 UJ N 9.5 320-41147-1
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 9.60000 U,H N 9.6 320-41147-15PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified F-53B Minor 83329-89-9 0.00200 U N 0.0020 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified ADONA 958445-44-8 0.00210 U N 0.0021 1965780
5 PF1018-LTW-02 TAL-SAC LTW-02 10/31/2018 537 Modified NaDONA EVS1361 0.00210 U N 0.0021 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.10:2 Fluorotelomer sulfonate 120226-60-0 0.00830 U N 0.0083 320-45387-2
5 GW0718-LTW-03 TAL-SAC LTW-03 7/13/2018 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 10.00000 Y 2.0 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 SW8321B Hfpo Dimer Acid 13252-13-6 8.50000 Z J Y 0.092 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluorooctadecanoic acid 16517-11-6 0.00180 U N 0.0018 320-45387-2
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.00280 U N 0.0028 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.PFOS 1763-23-1 0.00180 U N 0.0018 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluoroundecanoic Acid 2058-94-8 0.00180 U N 0.0018 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.00280 U N 0.0028 320-45387-25GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.00280 U N 0.0028 320-45387-2
5 GW0718-LTW-03 TAL-SAC LTW-03 7/13/2018 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 2.70000 Y 2.0 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluoropentanoic Acid 2706-90-3 0.58000 Y 0.055 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00180 U N 0.0018 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.6:2 Fluorotelomer sulfonate 27619-97-2 0.00180 U N 0.0018 320-45387-2
5 GW0718-LTW-03 TAL-SAC LTW-03 7/13/2018 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 1.20000 U N 2.0 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.00280 U N 0.0028 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluorohexanoic Acid 307-24-4 0.01200 Y 0.0018 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluorododecanoic Acid 307-55-1 0.00180 U N 0.0018 320-45387-2
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.00830 U N 0.0083 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.PFOA 335-67-1 0.00092 U N 0.00092 320-45387-15GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluorodecanoic Acid 335-76-2 0.00180 U N 0.0018 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluorodecane Sulfonic Acid 335-77-3 0.00180 U N 0.0018 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluorohexane Sulfonic Acid 355-46-4 0.00180 U N 0.0018 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluorobutanoic Acid 375-22-4 0.13000 Y 0.0055 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluorobutane Sulfonic Acid 375-73-5 0.00092 U N 0.00092 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluoroheptanoic Acid 375-85-9 0.01500 Y 0.00092 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00180 U N 0.0018 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluorononanoic Acid 375-95-1 0.00180 U N 0.0018 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluorotetradecanoic Acid 376-06-7 0.00092 U N 0.00092 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.00550 U N 0.0055 320-45387-2
5 GW0718-LTW-03 TAL-SAC LTW-03 7/13/2018 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 37.00000 F1 J Y 2.0 320-45387-25GW0718-LTW-03 TAL-SAC LTW-03 7/13/2018 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 5.60000 Y 2.0 320-45387-2
5 GW0718-LTW-03 TAL-SAC LTW-03 7/13/2018 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 0.97000 U N 2.0 320-45387-2
5 GW0718-LTW-03 TAL-SAC LTW-03 7/13/2018 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 1.10000 U N 2.0 320-45387-2
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.00830 U UJ N 0.0083 320-45387-2
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluorononanesulfonate 474511-07-4 0.00180 U N 0.0018 320-45387-1
5 GW0718-LTW-03 TAL-SAC LTW-03 7/13/2018 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 151.00000 Y 2.0 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluorohexadecanoic acid (PFHxDA)67905-19-5 0.00092 U N 0.00092 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluorotridecanoic Acid 72629-94-8 0.00092 U N 0.00092 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 SW8321B F-53B Major 73606-19-6 0.00092 U UJ N 0.00092 320-45387-2
5 GW0718-LTW-03 TAL-SAC LTW-03 7/13/2018 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.95000 U N 2.0 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluorooctane Sulfonamide 754-91-6 0.00280 U N 0.0028 320-45387-15GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.00280 U N 0.0028 320-45387-1
Page 20 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 537 Rev. 1.1 MOD.Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00092 U N 0.00092 320-45387-2
5 GW0718-LTW-03 TAL-SAC LTW-03 7/13/2018 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.96000 U N 2.0 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 SW8321B F-53B Minor 83329-89-9 0.00092 UZ UJ N 0.00092 320-45387-1
5 GW0718-LTW-03 LANC LTW-03 7/13/2018 SW8321B NaDONA EVS1361 0.00092 U UJ N 0.00092 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 42.00000 U,H N 42 320-45387-2
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Hfpo Dimer Acid 13252-13-6 18.00000 Y 0.14 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 11.00000 U,H,*UJ N 11 320-45387-2
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified PFOS 1763-23-1 0.00200 U N 0.0020 320-45387-15PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 8.30000 U,H N 8.3 320-45387-2
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 50.00000 U,H N 50 320-45387-2
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluoropentanoic Acid 2706-90-3 1.60000 Y 0.047 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 58.00000 U,H N 58 320-45387-2
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluorohexanoic Acid 307-24-4 0.03700 Y 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 320-45387-15PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 26.00000 U,H,*UJ N 26 320-45387-2
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified PFOA 335-67-1 0.00600 Y 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00200 U N 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluorobutanoic Acid 375-22-4 0.37000 Y 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00200 U N 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluoroheptanoic Acid 375-85-9 0.06500 Y 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluorononanoic Acid 375-95-1 0.00200 U N 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 320-45387-15PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 46.00000 U,H N 46 320-45387-2
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 44.00000 U,H N 44 320-45387-2
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 49.00000 U,H N 49 320-45387-2
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 53.00000 U,H N 53 320-45387-2
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 41.00000 U,H,*UJ N 41 320-45387-2
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 99.00000 H Y 47 320-45387-2
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluorohexadecanoic acid (PFHxDA)67905-19-5 0.00200 U N 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified F-53B Major 73606-19-6 0.00200 U N 0.0020 320-45387-15PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 47.00000 U,H N 47 320-45387-2
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 48.00000 U,H N 48 320-45387-2
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified F-53B Minor 83329-89-9 0.00200 U N 0.0020 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified ADONA 958445-44-8 0.00210 U N 0.0021 320-45387-1
5 PF1018-LTW-04 TAL-SAC LTW-04 11/12/2018 537 Modified NaDONA EVS1361 0.00210 U N 0.0021 320-45387-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 84.00000 U,H N 84 320-44881-3
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Hfpo Dimer Acid 13252-13-6 33.00000 Y 0.13 320-44881-15PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 320-44881-1
Page 21 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 23.00000 U,H N 23 320-44881-3
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified PFOS 1763-23-1 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 17.00000 U,H N 17 320-44881-3
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 100.00000 U,H N 100 320-44881-3
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluoropentanoic Acid 2706-90-3 3.10000 Y 0.044 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 120.00000 U,H N 120 320-44881-35PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluorohexanoic Acid 307-24-4 0.12000 Y 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 52.00000 U,H N 52 320-44881-3
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified PFOA 335-67-1 0.00330 Y 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluorobutanoic Acid 375-22-4 0.40000 Y 0.031 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluoroheptanoic Acid 375-85-9 0.28000 Y 0.0020 320-44881-15PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluorononanoic Acid 375-95-1 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 92.00000 U,H N 92 320-44881-3
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 88.00000 U,H N 88 320-44881-3
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 97.00000 U,H N 97 320-44881-3
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 110.00000 U,H N 110 320-44881-3
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 82.00000 U,H,*UJ N 82 320-44881-3
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 262.00000 H Y 95 320-44881-3
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluorohexadecanoic acid (PFHxDA)67905-19-5 0.00200 U N 0.0020 320-44881-15PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified F-53B Major 73606-19-6 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 95.00000 U,H N 95 320-44881-3
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 96.00000 U,H N 96 320-44881-3
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified F-53B Minor 83329-89-9 0.00200 U N 0.0020 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified ADONA 958445-44-8 0.00210 U N 0.0021 320-44881-1
5 PF1018-LTW-05 TAL-SAC LTW-05 11/12/2018 537 Modified NaDONA EVS1361 0.00210 U N 0.0021 320-44881-16FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00250 U N 0.0025 2028553
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U,H N 0.046 320-51045-1
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.98000 H Y 0.054 320-51045-1
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Hfpo Dimer Acid 13252-13-6 10.00000 J Y 0.17 2028553
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U,H N 0.060 320-51045-1
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 19.00000 Y 0.050 2028553
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 25.00000 H Y 0.57 320-51045-1
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorooctadecanoic acid 16517-11-6 0.00170 U N 0.0017 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.00250 U N 0.0025 2028553
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U,H N 0.060 320-51045-1
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.04700 H Y 0.015 320-51045-16FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorononanoic Acid 375-95-1 0.02000 Y 0.0017 2028553
Page 22 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorotetradecanoic Acid 376-06-7 0.00085 U N 0.00085 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00170 U N 0.0017 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluoroheptanoic Acid 375-85-9 0.09400 Y 0.00085 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorohexane Sulfonic Acid 355-46-4 0.00290 Y 0.0017 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorobutanoic Acid 375-22-4 0.26000 Y 0.0051 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorobutane Sulfonic Acid 375-73-5 0.00140 Y 0.00085 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorodecane Sulfonic Acid 335-77-3 0.00170 U N 0.0017 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorodecanoic Acid 335-76-2 0.00170 U N 0.0017 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified PFOA 335-67-1 0.03500 Y 0.00085 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.00760 U UJ N 0.0076 20285536FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U,H N 0.035 320-51045-1
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.00250 U N 0.0025 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorododecanoic Acid 307-55-1 0.00170 U N 0.0017 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorohexanoic Acid 307-24-4 0.03900 Y 0.0017 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.00510 U N 0.0051 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 6.80000 Y 0.050 2028553
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 8.10000 H Y 0.079 320-51045-1
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 6.30000 Y 0.10 2028553
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 5.60000 H Y 0.034 320-51045-1
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 12.00000 Y 0.050 2028553
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 14.00000 H Y 0.058 320-51045-16FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 35.00000 Y 0.050 2028553
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 41.00000 H Y 0.081 320-51045-1
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.00760 U UJ N 0.0076 2028553
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U,H N 0.037 320-51045-1
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified F-53B Major 73606-19-6 0.00085 U UJ N 0.00085 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorotridecanoic Acid 72629-94-8 0.00085 U N 0.00085 2028553
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.96000 H Y 0.024 320-51045-1
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 1.20000 Y 0.050 2028553
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 1.20000 H Y 0.030 320-51045-1
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorohexadecanoic acid (PFHxDA)67905-19-5 0.00085 U N 0.00085 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorononanesulfonic acid 68259-12-1 0.00170 U N 0.0017 20285536FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 62.00000 Y 0.050 2028553
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 84.00000 H Y 0.21 320-51045-1
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.00250 U N 0.0025 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorooctane Sulfonamide 754-91-6 0.00250 U N 0.0025 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluoroundecanoic Acid 2058-94-8 0.00170 U N 0.0017 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified PFOS 1763-23-1 0.00630 Y 0.0017 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.00250 U N 0.0025 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.00250 U N 0.0025 2028553
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U,H N 0.11 320-51045-1
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluoropentanoic Acid 2706-90-3 0.52000 Y 0.051 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00170 U N 0.0017 20285536FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.00170 U N 0.0017 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 7.10000 Y 0.050 2028553
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 9.90000 H Y 0.047 320-51045-1
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 4.30000 Y 0.050 2028553
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 4.00000 H Y 0.027 320-51045-1
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 23.00000 H Y 0.058 320-51045-1
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 2.20000 H Y 0.16 320-51045-1
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 1.20000 H Y 0.070 320-51045-1
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified F-53B Minor 83329-89-9 0.00170 U UJ N 0.0017 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified ADONA 958445-44-8 0.00085 U UJ N 0.00085 2028553
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.05000 U N 0.050 20285536FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U,H N 0.041 320-51045-1
Page 23 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
6 FAY-SW-SEEP-A-1-020719 LANC SEEP-A-1 2/7/2019 EPA 537 Rev. 1.1 modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00085 U N 0.00085 2028553
6 FAY-SW-SEEP-A-1-020719 TAL-SAC SEEP-A-1 2/7/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 1.70000 H Y 0.028 320-51045-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U N 0.060 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U N 0.060 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 25.00000 F1 J Y 0.57 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 24.00000 J Y 0.57 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U N 0.060 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U N 0.060 280-124212-16FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 1.40000 Y 0.054 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 1.40000 Y 0.054 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U N 0.046 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U N 0.046 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 47.00000 Y 0.081 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 48.00000 Y 0.081 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 280-124212-16FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U UJ N 0.035 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U N 0.035 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified PFOA 335-67-1 0.03700 Y 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified PFOA 335-67-1 0.03900 Y 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00330 Y 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00330 Y 0.0020 280-124212-16FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.36000 Y 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.36000 Y 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.12000 Y 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.12000 Y 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.02600 Y 0.0020 280-124212-16FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.02800 Y 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U UJ N 0.037 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U,F1 UJ N 0.037 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 18.00000 Y 0.058 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 18.00000 Y 0.058 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 6.20000 Y 0.034 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 7.10000 Y 0.034 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 11.00000 Y 0.079 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 11.00000 Y 0.079 280-124212-16FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 280-124212-1
Page 24 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 2.50000 Y 0.028 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 2.50000 Y 0.028 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 103.00000 Y 0.21 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 103.00000 F1 J Y 0.21 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 1.70000 Y 0.024 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 1.60000 Y 0.024 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 1.70000 Y 0.030 280-124212-16FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 1.80000 Y 0.030 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 7.40000 Y 0.027 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 7.40000 Y 0.027 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 11.00000 Y 0.047 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 11.00000 Y 0.047 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 280-124212-16FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 0.69000 Y 0.0023 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 0.75000 Y 0.0024 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U N 0.11 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U N 0.11 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified PFOS 1763-23-1 0.00550 Y 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified PFOS 1763-23-1 0.00570 Y 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 280-124212-16FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U N 0.041 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U N 0.041 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 1.60000 Y 0.070 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 1.60000 Y 0.070 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 3.00000 Y 0.16 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 3.00000 Y 0.16 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 32.00000 Y 0.058 280-124212-1
6 FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 31.00000 Y 0.058 280-124212-16FAY-SW-SEEPA-1-052019 TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.06700 Y 0.015 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.07400 Y 0.015 280-124212-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U,H N 0.046 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 1.00000 H Y 0.054 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U,H N 0.060 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified Hfpo Dimer Acid 13252-13-6 20.00000 E Y 0.014 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 17.00000 H Y 0.57 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.05000 H Y 0.015 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.01500 Y 0.0020 280-124971-16FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 280-124971-1
Page 25 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.07900 Y 0.0020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.24000 Y 0.0020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00400 Y 0.0020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00220 Y 0.0020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.0020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified PFOA 335-67-1 0.03600 Y 0.0020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U,H,*N 0.035 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 280-124971-16FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 5.30000 H Y 0.079 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 4.60000 H,*J Y 0.034 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 11.00000 H Y 0.058 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 30.00000 H Y 0.081 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U,H,*N 0.037 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.97000 H Y 0.024 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 1.30000 H Y 0.030 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 280-124971-16FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 72.00000 H Y 0.21 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified PFOS 1763-23-1 0.00970 Y 0.0020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U,H N 0.060 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U,H N 0.11 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 0.49000 Y 0.0045 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 280-124971-16FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 6.90000 H Y 0.047 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 5.30000 H Y 0.027 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 18.00000 H Y 0.058 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 1.70000 H Y 0.16 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 1.10000 H Y 0.070 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 1.40000 H Y 0.028 280-124971-1
6 FAY-SW-SEEP A-1-060719 TAL-SAC SEEP-A-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U,H N 0.041 280-124971-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 1.40000 Y 0.054 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U N 0.046 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 280-124212-16FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 25.00000 F1 J Y 0.57 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U N 0.060 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U N 0.060 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified PFOS 1763-23-1 0.00550 Y 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U N 0.11 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 11.00000 Y 0.047 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 0.75000 Y 0.0024 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 280-124212-16FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 280-124212-1
Page 26 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 7.40000 Y 0.027 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U N 0.035 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified PFOA 335-67-1 0.03700 Y 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00330 Y 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.36000 Y 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00200 U N 0.0020 280-124212-16FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.12000 Y 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.02600 Y 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 48.00000 Y 0.081 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 18.00000 Y 0.058 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 11.00000 Y 0.079 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 6.20000 Y 0.034 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U,F1 UJ N 0.037 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 103.00000 Y 0.21 280-124212-16FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 1.70000 Y 0.024 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 1.70000 Y 0.030 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 2.50000 Y 0.028 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U N 0.041 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP Hfpo Dimer Acid (trial)EVS1200 38.00000 Y 0.086 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 1.60000 Y 0.070 280-124212-16FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 3.00000 Y 0.16 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 32.00000 Y 0.058 280-124212-1
6 FAY-SW-SEEPA-1-052019-D TAL-SAC SEEP-A-1 5/20/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.07400 Y 0.015 280-124212-1
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorooctadecanoic acid 16517-11-6 0.01800 U N 0.018 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 38.00000 Y 0.050 2028125
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 42.00000 H Y 0.57 320-51045-1
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U,H N 0.060 320-51045-1
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Hfpo Dimer Acid 13252-13-6 24.00000 J Y 1.8 2028125
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 3.30000 H Y 0.054 320-51045-1
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.02700 U N 0.027 2028125
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U,H N 0.046 320-51045-17FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.08400 H Y 0.015 320-51045-1
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.05400 U N 0.054 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorodecanoic Acid 335-76-2 0.01800 U N 0.018 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorodecane Sulfonic Acid 335-77-3 0.01800 U N 0.018 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorobutane Sulfonic Acid 375-73-5 0.00900 U N 0.009 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorobutanoic Acid 375-22-4 0.56000 Y 0.054 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorohexane Sulfonic Acid 355-46-4 0.01800 U N 0.018 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluoroheptanoic Acid 375-85-9 0.17000 Y 0.009 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.01800 U N 0.018 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorotetradecanoic Acid 376-06-7 0.00900 U N 0.009 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorononanoic Acid 375-95-1 0.01800 Y 0.018 20281257FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorohexanoic Acid 307-24-4 0.04700 Y 0.018 2028125
Page 27 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorododecanoic Acid 307-55-1 0.01800 U N 0.018 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02700 U N 0.027 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified PFOA 335-67-1 0.03100 Y 0.009 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.08100 U N 0.081 2028125
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U,H N 0.035 320-51045-1
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 43.00000 Y 0.050 2028125
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 43.00000 H Y 0.081 320-51045-1
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 11.00000 Y 0.050 2028125
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 9.20000 H Y 0.058 320-51045-1
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 2.00000 Y 0.050 20281257FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 1.80000 H Y 0.079 320-51045-1
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.46000 Y 0.10 2028125
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.53000 H Y 0.034 320-51045-1
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.08100 U N 0.081 2028125
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U,H N 0.037 320-51045-1
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02700 U N 0.027 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorooctane Sulfonamide 754-91-6 0.02700 U N 0.027 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorononanesulfonic acid 68259-12-1 0.01800 U N 0.018 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorohexadecanoic acid (PFHxDA)67905-19-5 0.00900 U N 0.009 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 150.00000 Y 0.50 2028125
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 148.00000 H Y 0.21 320-51045-17FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 1.10000 Y 0.050 2028125
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 1.10000 H Y 0.030 320-51045-1
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorotridecanoic Acid 72629-94-8 0.00900 U N 0.009 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified F-53B Major 73606-19-6 0.00900 U N 0.009 2028125
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 6.10000 H Y 0.024 320-51045-1
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluoropentanoic Acid 2706-90-3 1.60000 Y 0.054 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.01800 U N 0.018 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.01800 U N 0.018 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 15.00000 Y 0.050 2028125
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 17.00000 H Y 0.047 320-51045-1
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified PFOS 1763-23-1 0.01800 U N 0.018 20281257FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluoroundecanoic Acid 2058-94-8 0.01800 U N 0.018 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.02700 U N 0.027 2028125
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U,H N 0.060 320-51045-1
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02700 U N 0.027 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.02700 U N 0.027 2028125
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U,H N 0.11 320-51045-1
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 4.60000 Y 0.050 2028125
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 3.50000 H Y 0.027 320-51045-1
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00900 U N 0.009 2028125
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 2.80000 H Y 0.028 320-51045-1
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.05000 U N 0.050 20281257FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U,H N 0.041 320-51045-1
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified ADONA 958445-44-8 0.00900 U N 0.009 2028125
7 FAY-SW-SEEP-B-1-020519 LANC SEEP-B-1 2/5/2019 EPA 537 Rev. 1.1 modified F-53B Minor 83329-89-9 0.01800 U N 0.018 2028125
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 3.20000 H Y 0.070 320-51045-1
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 4.70000 H Y 0.16 320-51045-1
7 FAY-SW-SEEP-B-1-020519 TAL-SAC SEEP-B-1 2/5/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 38.00000 H,*Y 0.058 320-51045-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U N 0.046 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 2.70000 Y 0.054 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U N 0.060 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 34.00000 Y 0.57 280-124257-17FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 280-124257-1
Page 28 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.05300 Y 0.015 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U N 0.035 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified PFOA 335-67-1 0.01700 Y 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.01200 Y 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.14000 Y 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00200 U N 0.0020 280-124257-17FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.47000 Y 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00200 U N 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00220 Y 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U N 0.037 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.21000 Y 0.034 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 1.30000 Y 0.079 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 9.60000 Y 0.058 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 43.00000 Y 0.081 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 2.90000 Y 0.024 280-124257-17FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.66000 Y 0.030 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 150.00000 Y 0.21 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 2.00000 Y 0.027 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U N 0.11 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U N 0.060 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 280-124257-17FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified PFOS 1763-23-1 0.00230 Y 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 13.00000 Y 0.047 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 1.20000 Y 0.0023 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 21.00000 F1 J Y 0.058 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 2.90000 Y 0.16 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 2.00000 Y 0.070 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U N 0.041 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 1.70000 Y 0.028 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 280-124257-17FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 35.00000 H Y 0.57 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U,H N 0.060 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified Hfpo Dimer Acid 13252-13-6 27.00000 E Y 0.014 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 3.20000 H Y 0.054 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U,H N 0.046 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.07800 H Y 0.015 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00260 Y 0.0020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 280-124971-17FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00200 U N 0.0020 280-124971-1
Page 29 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.60000 Y 0.0033 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00220 Y 0.0020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.17000 Y 0.0020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.01600 Y 0.0020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified PFOA 335-67-1 0.02400 Y 0.0020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U,H N 0.035 280-124971-17FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 39.00000 H Y 0.081 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 8.80000 H Y 0.058 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 1.50000 H Y 0.079 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.27000 H Y 0.034 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U,H N 0.037 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 157.00000 H Y 0.21 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.94000 H Y 0.030 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 280-124971-17FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 4.30000 H Y 0.024 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 1.50000 Y 0.0046 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 15.00000 H Y 0.047 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified PFOS 1763-23-1 0.00220 I Y 0.0020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U,H N 0.060 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U,H N 0.11 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 2.90000 H Y 0.027 280-124971-17FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 2.20000 H Y 0.028 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U,H N 0.041 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 3.20000 H Y 0.070 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 3.90000 H Y 0.16 280-124971-1
7 FAY-SW-SEEP B-1-060719 TAL-SAC SEEP-B-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 34.00000 H Y 0.058 280-124971-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 2.00000 Y 0.027 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 280-124257-17FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U N 0.035 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified PFOA 335-67-1 0.01700 Y 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00220 Y 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00200 U N 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.47000 Y 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00200 U N 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.14000 Y 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.01200 Y 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 280-124257-17FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 280-124257-1
Page 30 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 43.00000 Y 0.081 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 9.60000 Y 0.058 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 1.30000 Y 0.079 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.21000 Y 0.034 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U N 0.037 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 150.00000 Y 0.21 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 2.90000 Y 0.024 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.66000 Y 0.030 280-124257-17FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 1.70000 Y 0.028 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U N 0.041 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP Hfpo Dimer Acid (trial)EVS1200 25.00000 Y 0.086 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 2.00000 Y 0.070 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 2.90000 Y 0.16 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 21.00000 F1 J Y 0.058 280-124257-1
7 FAY-SW-SEEP-B-1-052119 TAL-SAC SEEP-B-1 5/21/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.05300 Y 0.015 280-124257-1
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.09200 U,H N 0.092 320-51045-18FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.02700 U N 0.027 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.02600 U N 0.026 2028125
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 2.00000 H Y 0.11 320-51045-1
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.12000 U,H N 0.12 320-51045-1
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Hfpo Dimer Acid 13252-13-6 27.00000 J Y 1.8 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Hfpo Dimer Acid 13252-13-6 27.00000 J Y 1.7 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 16.00000 Y 0.050 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 15.00000 Y 0.050 2028125
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 16.00000 H Y 1.1 320-51045-1
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorooctadecanoic acid 16517-11-6 0.01800 U N 0.018 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorooctadecanoic acid 16517-11-6 0.01700 U N 0.017 20281258FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.02700 U N 0.027 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.02600 U N 0.026 2028125
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.12000 U,H N 0.12 320-51045-1
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.03100 U,H N 0.031 320-51045-1
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.08200 U N 0.082 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.07900 U N 0.079 2028125
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.06900 U,H N 0.069 320-51045-1
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified PFOA 335-67-1 0.02000 Y 0.0091 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified PFOA 335-67-1 0.01700 Y 0.0087 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02700 U N 0.027 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02600 U N 0.026 20281258FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorododecanoic Acid 307-55-1 0.01800 U N 0.018 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorododecanoic Acid 307-55-1 0.01700 U N 0.017 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorohexanoic Acid 307-24-4 0.08100 Y 0.018 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorohexanoic Acid 307-24-4 0.07900 Y 0.017 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorononanoic Acid 375-95-1 0.01800 U N 0.018 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorononanoic Acid 375-95-1 0.01700 U N 0.017 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorotetradecanoic Acid 376-06-7 0.00910 U N 0.0091 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorotetradecanoic Acid 376-06-7 0.00870 U N 0.0087 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.05400 U N 0.054 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.05200 U N 0.052 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.01800 U N 0.018 20281258FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.01700 U N 0.017 2028125
Page 31 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluoroheptanoic Acid 375-85-9 0.22000 Y 0.0091 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluoroheptanoic Acid 375-85-9 0.22000 Y 0.0087 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorobutanoic Acid 375-22-4 0.38000 Y 0.054 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorobutanoic Acid 375-22-4 0.38000 Y 0.052 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorobutane Sulfonic Acid 375-73-5 0.00910 U N 0.0091 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorobutane Sulfonic Acid 375-73-5 0.00870 U N 0.0087 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorohexane Sulfonic Acid 355-46-4 0.01800 U N 0.018 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorohexane Sulfonic Acid 355-46-4 0.01700 U N 0.017 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorodecanoic Acid 335-76-2 0.01800 U N 0.018 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorodecanoic Acid 335-76-2 0.01700 U N 0.017 20281258FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorodecane Sulfonic Acid 335-77-3 0.01800 U N 0.018 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorodecane Sulfonic Acid 335-77-3 0.01700 U N 0.017 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 62.00000 Y 0.050 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 62.00000 Y 0.050 2028125
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 64.00000 H Y 0.16 320-51045-1
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.08200 U N 0.082 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.07900 U N 0.079 2028125
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.07500 U,H N 0.075 320-51045-1
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.10000 U N 0.10 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.10000 U N 0.10 2028125
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.08900 H Y 0.067 320-51045-18FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 4.50000 Y 0.050 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 4.40000 Y 0.050 2028125
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 4.60000 H Y 0.16 320-51045-1
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 21.00000 Y 0.050 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 22.00000 Y 0.050 2028125
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 20.00000 H Y 0.12 320-51045-1
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorotridecanoic Acid 72629-94-8 0.00910 U N 0.0091 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorotridecanoic Acid 72629-94-8 0.00870 U N 0.0087 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified F-53B Major 73606-19-6 0.00910 U N 0.0091 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified F-53B Major 73606-19-6 0.00870 U N 0.0087 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.59000 J Y 0.050 20281258FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.50000 J Y 0.050 2028125
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.59000 H Y 0.061 320-51045-1
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorooctane Sulfonamide 754-91-6 0.02700 U N 0.027 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorooctane Sulfonamide 754-91-6 0.02600 U N 0.026 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 200.00000 Y 0.50 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 200.00000 Y 0.50 2028125
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 196.00000 H Y 0.42 320-51045-1
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorohexadecanoic acid (PFHxDA)67905-19-5 0.00910 U N 0.0091 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorohexadecanoic acid (PFHxDA)67905-19-5 0.00870 U N 0.0087 2028125
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.04900 U,H N 0.049 320-51045-1
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorononanesulfonic acid 68259-12-1 0.01800 U N 0.018 20281258FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorononanesulfonic acid 68259-12-1 0.01700 U N 0.017 2028125
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 2.30000 H Y 0.056 320-51045-1
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02700 U N 0.027 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02600 U N 0.026 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.05000 U N 0.050 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.05000 U N 0.050 2028125
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.05300 U,H N 0.053 320-51045-1
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.02700 U N 0.027 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.02600 U N 0.026 2028125
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.22000 U,H N 0.22 320-51045-1
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluoroundecanoic Acid 2058-94-8 0.01800 U N 0.018 20281258FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluoroundecanoic Acid 2058-94-8 0.01700 U N 0.017 2028125
Page 32 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02700 U N 0.027 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02600 U N 0.026 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified PFOS 1763-23-1 0.01800 U N 0.018 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified PFOS 1763-23-1 0.01700 U N 0.017 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 4.70000 Y 0.050 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 4.70000 Y 0.050 2028125
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 5.10000 H Y 0.093 320-51045-1
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluoropentanoic Acid 2706-90-3 1.70000 Y 0.054 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluoropentanoic Acid 2706-90-3 1.70000 Y 0.052 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.01800 U N 0.018 20281258FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.01700 U N 0.017 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.01800 U N 0.018 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.01700 U N 0.017 2028125
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 1.60000 H Y 0.32 320-51045-1
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 3.00000 H Y 0.12 320-51045-1
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 1.90000 H Y 0.14 320-51045-1
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.05000 U N 0.050 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.05000 U N 0.050 2028125
8 FAY-SW-SEEP-C-1-020519 TAL-SAC SEEP-C-1 2/5/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.08200 U,H N 0.082 320-51045-1
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified ADONA 958445-44-8 0.00910 U N 0.0091 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified ADONA 958445-44-8 0.00870 U N 0.0087 20281258FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified F-53B Minor 83329-89-9 0.01800 U N 0.018 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified F-53B Minor 83329-89-9 0.01700 U N 0.017 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00910 U N 0.0091 2028125
8 FAY-SW-SEEP-C-1-020519 LANC SEEP-C-1 2/5/2019 EPA 537 Rev. 1.1 modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00870 U N 0.0087 2028125
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.09000 U N 0.090 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 14.00000 Y 0.85 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified Hfpo Dimer Acid 13252-13-6 36.00000 E Y 0.015 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.09000 U N 0.090 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 2.00000 Y 0.080 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 280-124325-18FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.06900 U N 0.069 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 66.00000 Y 0.12 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.0020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00220 Y 0.0020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00200 U N 0.0020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.39000 Y 0.0020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.24000 Y 0.0020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.00200 U N 0.0020 280-124325-18FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified PFOA 335-67-1 0.01800 Y 0.0020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.05200 U N 0.052 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 19.00000 Y 0.087 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 4.90000 Y 0.12 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.09700 Y 0.050 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.05600 U N 0.056 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 2.50000 Y 0.042 280-124325-18FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 280-124325-1
Page 33 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.03600 U N 0.036 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 193.00000 Y 0.32 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.72000 Y 0.045 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 1.80000 Y 0.0048 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 5.00000 Y 0.070 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified PFOS 1763-23-1 0.00220 Y 0.0020 280-124325-18FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.16000 U N 0.16 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.04000 U N 0.040 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.06100 U N 0.061 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 1.20000 F1 Y 0.11 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 1.90000 F1 Y 0.087 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 1.30000 Y 0.24 280-124325-1
8 FAY-SW-SEEP-C-1-052319 TAL-SAC SEEP-C-1 5/23/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.05200 Y 0.023 280-124325-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.09200 U,H N 0.092 280-124971-18FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 2.10000 H Y 0.11 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.12000 U,H N 0.12 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified Hfpo Dimer Acid 13252-13-6 42.00000 E Y 0.016 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 13.00000 H Y 1.1 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.12000 U,H N 0.12 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.04000 H Y 0.031 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.06900 U,H,*N 0.069 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified PFOA 335-67-1 0.01600 Y 0.0020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 280-124971-18FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.00200 U N 0.0020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.23000 Y 0.0020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.40000 Y 0.0020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00230 Y 0.0020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00200 U N 0.0020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.0020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 280-124971-18FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.07500 U,H,*N 0.075 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.06700 U,H,F1,*N 0.067 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 3.60000 H Y 0.16 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 17.00000 H Y 0.12 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 56.00000 H Y 0.16 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.04900 U,H N 0.049 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.66000 H,F1 Y 0.061 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 199.00000 H Y 0.42 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 280-124971-18FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 280-124971-1
Page 34 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.05300 U,H N 0.053 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.22000 U,H N 0.22 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified PFOS 1763-23-1 0.00200 U N 0.0020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 4.00000 H Y 0.093 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 1.70000 Y 0.0051 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 1.50000 H Y 0.32 280-124971-18FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 3.10000 H Y 0.12 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 1.90000 H Y 0.14 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 2.10000 H Y 0.056 280-124971-1
8 FAY-SW-SEEP C-1-060719 TAL-SAC SEEP-C-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.08200 U,H N 0.082 280-124971-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.81000 H Y 0.054 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.80000 H Y 0.054 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U,H N 0.046 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U,H N 0.046 280-124599-19FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U,H N 0.060 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U,H N 0.060 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified Hfpo Dimer Acid 13252-13-6 19.00000 E Y 0.0071 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified Hfpo Dimer Acid 13252-13-6 15.00000 E Y 0.0070 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 9.00000 H Y 0.57 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 9.20000 H Y 0.57 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U,H N 0.060 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U,H N 0.060 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U,H N 0.035 280-124599-19FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U,H N 0.035 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified PFOA 335-67-1 0.01200 Y 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified PFOA 335-67-1 0.01100 Y 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 280-124599-19FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00200 I Y 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00200 I Y 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.21000 Y 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.21000 Y 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.09700 Y 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.09300 Y 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 280-124599-19FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 280-124599-1
Page 35 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.00270 Y 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.00260 Y 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 29.00000 H Y 0.081 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 29.00000 H Y 0.081 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U,H N 0.037 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U,H N 0.037 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.15000 H Y 0.034 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.15000 H Y 0.034 280-124599-19FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 2.50000 H Y 0.079 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 2.30000 H Y 0.079 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 7.90000 H Y 0.058 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 8.10000 H Y 0.058 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.32000 H Y 0.030 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.34000 H Y 0.030 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 91.00000 H Y 0.21 280-124599-19FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 91.00000 H Y 0.21 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.02400 U,H N 0.024 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.02400 U,H N 0.024 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 1.30000 H Y 0.028 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 1.30000 H Y 0.028 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.02700 U,H N 0.027 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.02700 U,H N 0.027 280-124599-19FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U,H N 0.11 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U,H N 0.11 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified PFOS 1763-23-1 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified PFOS 1763-23-1 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 2.90000 H Y 0.047 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 3.00000 H Y 0.047 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 280-124599-19FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 0.73000 Y 0.0023 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 0.76000 Y 0.0023 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.01500 U,H N 0.015 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.01500 H Y 0.015 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 2.60000 H Y 0.058 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 2.50000 H Y 0.058 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 1.10000 H Y 0.070 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 1.10000 H Y 0.070 280-124599-19FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 1.00000 H Y 0.16 280-124599-1
Page 36 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 0.97000 H Y 0.16 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U,H N 0.041 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U,H N 0.041 280-124599-1
9 FAY-SW-SEEP-D-1-053019 TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP-D-1-053019-D TAL-SAC SEEP-D-1 5/30/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 280-124599-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U,H N 0.060 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 7.20000 H Y 0.57 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified Hfpo Dimer Acid 13252-13-6 16.00000 E Y 0.014 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U,H N 0.060 280-124971-19FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.90000 H Y 0.054 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U,H N 0.046 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.01700 H Y 0.015 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.00280 Y 0.0020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.10000 Y 0.0020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.21000 Y 0.0020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00200 U N 0.0020 280-124971-19FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00210 Y 0.0020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.0020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified PFOA 335-67-1 0.01400 Y 0.0020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U,H,*N 0.035 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 7.40000 H Y 0.058 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 24.00000 H Y 0.081 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 1.80000 H Y 0.079 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.12000 H,*J Y 0.034 280-124971-19FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U,H,*N 0.037 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 90.00000 H Y 0.21 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.02400 U,H N 0.024 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.39000 H Y 0.030 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 0.79000 Y 0.0046 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 280-124971-19FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 2.40000 H Y 0.047 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified PFOS 1763-23-1 0.00200 U N 0.0020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U,H N 0.11 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.02700 U,H N 0.027 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 1.20000 H Y 0.028 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U,H N 0.041 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 1.00000 H Y 0.070 280-124971-1
9 FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 2.20000 H Y 0.058 280-124971-19FAY-SW-SEEP D-1-060719 TAL-SAC SEEP-D-1 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 0.84000 H Y 0.16 280-124971-1
Page 37 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
10 FAY-SW-OLDOF-2-020119 LANC OLDOF-2 2/1/2019 EPA 537 Rev. 1.1 modified Hfpo Dimer Acid 13252-13-6 5.90000 Y 0.18 2027689
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U,H N 0.060 320-51031-1
10 FAY-SW-OLDOF-2-020119 LANC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 5.80000 Y 0.050 2027689
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 6.00000 H Y 0.57 320-51031-1
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U,H N 0.046 320-51031-1
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.80000 H Y 0.054 320-51031-1
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U,H N 0.060 320-51031-1
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.01500 U,H N 0.015 320-51031-1
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U,H N 0.035 320-51031-1
10 FAY-SW-OLDOF-2-020119 LANC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.82000 Y 0.10 202768910FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.95000 H J Y 0.034 320-51031-1
10 FAY-SW-OLDOF-2-020119 LANC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 1.80000 Y 0.050 2027689
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 1.60000 H Y 0.079 320-51031-1
10 FAY-SW-OLDOF-2-020119 LANC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 22.00000 Y 0.050 2027689
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 18.00000 H Y 0.081 320-51031-1
10 FAY-SW-OLDOF-2-020119 LANC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 6.40000 Y 0.050 2027689
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 5.20000 H Y 0.058 320-51031-1
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U,H N 0.037 320-51031-1
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 0.20000 H Y 0.028 320-51031-1
10 FAY-SW-OLDOF-2-020119 LANC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.33000 Y 0.050 2027689
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.34000 H Y 0.030 320-51031-110FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.02400 U,H N 0.024 320-51031-1
10 FAY-SW-OLDOF-2-020119 LANC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 83.00000 Y 0.050 2027689
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 92.00000 H Y 0.21 320-51031-1
10 FAY-SW-OLDOF-2-020119 LANC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 1.90000 Y 0.050 2027689
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 2.00000 H Y 0.047 320-51031-1
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U,H N 0.11 320-51031-1
10 FAY-SW-OLDOF-2-020119 LANC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.18000 Y 0.050 2027689
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.14000 H Y 0.027 320-51031-1
10 FAY-SW-OLDOF-2-020119 LANC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.05000 U N 0.050 2027689
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U,H N 0.041 320-51031-1
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 0.19000 H Y 0.070 320-51031-110FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 0.42000 H Y 0.16 320-51031-1
10 FAY-SW-OLDOF-2-020119 TAL-SAC OLDOF-2 2/1/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 1.30000 H Y 0.058 320-51031-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U N 0.060 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.83000 Y 0.054 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U N 0.046 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 5.60000 Y 0.57 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U N 0.060 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.01500 U N 0.015 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U N 0.035 280-124472-110FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified PFOA 335-67-1 0.03200 Y 0.0020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.0020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00200 U N 0.0020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00200 U N 0.0020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.08600 Y 0.0020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.02500 Y 0.0020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 280-124472-110FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 280-124472-1
Page 38 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.00750 Y 0.0020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U N 0.037 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 4.80000 Y 0.058 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 18.00000 Y 0.081 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 1.60000 Y 0.079 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.62000 Y 0.034 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 71.00000 Y 0.21 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.02400 U N 0.024 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 280-124472-110FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.31000 Y 0.030 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 0.20000 Y 0.028 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.02700 U N 0.027 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U N 0.11 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified PFOS 1763-23-1 0.00200 Y 0.0020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 1.90000 Y 0.047 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 280-124472-110FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 0.15000 Y 0.0020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 0.79000 Y 0.058 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 0.41000 Y 0.16 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 0.17000 F1 J Y 0.070 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U N 0.041 280-124472-1
10 FAY-SW-OLDOF-2-052419 TAL-SAC OLDOF-2 5/24/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 280-124472-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U,H N 0.060 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified Hfpo Dimer Acid 13252-13-6 6.20000 E Y 0.0040 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 5.40000 H Y 0.57 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 280-124971-110FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U,H N 0.046 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.90000 H Y 0.054 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U,H N 0.060 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.01500 H Y 0.015 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.00710 Y 0.0020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.02600 Y 0.0020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.09000 Y 0.0020 280-124971-110FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00200 U N 0.0020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00200 U N 0.0020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.0020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified PFOA 335-67-1 0.03400 Y 0.0020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U,H,*N 0.035 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 18.00000 H Y 0.081 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.57000 H,*J Y 0.034 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 1.40000 H Y 0.079 280-124971-110FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 4.70000 H Y 0.058 280-124971-1
Page 39 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U,H,*N 0.037 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 0.20000 H Y 0.028 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.35000 H Y 0.030 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.02400 H Y 0.024 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 91.00000 H Y 0.21 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 280-124971-110FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 0.16000 Y 0.0020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 1.80000 H Y 0.047 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified PFOS 1763-23-1 0.00200 Y 0.0020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U,H N 0.11 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.30000 H,F1 Y 0.027 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U,H N 0.041 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 0.20000 H Y 0.070 280-124971-110FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 0.39000 H,F1 Y 0.16 280-124971-1
10 FAY-SW-OLDOF-2-060719 TAL-SAC OLDOF-2 6/7/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 1.10000 H Y 0.058 280-124971-1
11 Residential Well Residential Well 12/14/2017 Hfpo Dimer Acid 13252-13-6 0.02100 Y
11 Residential Well Residential Well 12/12/2017 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 12/13/2017 Hfpo Dimer Acid 13252-13-6 0.03800 Y
11 Residential Well Residential Well 1/24/2018 Hfpo Dimer Acid 13252-13-6 0.05000 Y
11 Residential Well Residential Well 1/24/2018 Hfpo Dimer Acid 13252-13-6 0.01500 Y
11 Residential Well Residential Well 1/24/2018 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 4/25/2018 Hfpo Dimer Acid 13252-13-6 0.00179 Y
11 Residential Well Residential Well 4/25/2018 Hfpo Dimer Acid 13252-13-6 0.00179 Y
11 Residential Well Residential Well 4/25/2018 Hfpo Dimer Acid 13252-13-6 0.00179 Y11Residential Well Residential Well 1/9/2018 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 4/11/2018 Hfpo Dimer Acid 13252-13-6 0.03690 Y
11 Residential Well Residential Well 12/11/2017 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 1/15/2018 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 11/30/2017 Hfpo Dimer Acid 13252-13-6 0.01300 Y
11 Residential Well Residential Well 11/30/2017 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 4/11/2018 Hfpo Dimer Acid 13252-13-6 0.00186 Y
11 Residential Well Residential Well 4/11/2018 Hfpo Dimer Acid 13252-13-6 0.00182 Y
11 Residential Well Residential Well 3/18/2019 Hfpo Dimer Acid 13252-13-6 0.94000 Y
11 Residential Well Residential Well 8/6/2018 Hfpo Dimer Acid 13252-13-6 0.78000 Y
11 Residential Well Residential Well 10/18/2017 Hfpo Dimer Acid 13252-13-6 0.04900 Y11Residential Well Residential Well 12/15/2017 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 1/31/2018 Hfpo Dimer Acid 13252-13-6 0.52700 Y
11 Residential Well Residential Well 11/30/2017 Hfpo Dimer Acid 13252-13-6 0.02000 Y
11 Residential Well Residential Well 11/29/2017 Hfpo Dimer Acid 13252-13-6 0.00400 N
11 Residential Well Residential Well 8/14/2018 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 12/12/2017 Hfpo Dimer Acid 13252-13-6 0.07600 Y
11 Residential Well Residential Well 12/14/2017 Hfpo Dimer Acid 13252-13-6 0.07800 Y
11 Residential Well Residential Well 1/5/2018 Hfpo Dimer Acid 13252-13-6 0.01200 Y
11 Residential Well Residential Well 1/5/2018 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 12/7/2017 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 12/6/2017 Hfpo Dimer Acid 13252-13-6 0.08500 Y11Residential Well Residential Well 4/30/2019 Hfpo Dimer Acid 13252-13-6 0.24000 Y
Page 40 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
11 Residential Well Residential Well 5/9/2018 Hfpo Dimer Acid 13252-13-6 0.03600 Y
11 Residential Well Residential Well 1/4/2018 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 9/22/2017 Hfpo Dimer Acid 13252-13-6 0.25000 Y
11 Residential Well Residential Well 12/5/2017 Hfpo Dimer Acid 13252-13-6 0.02400 Y
11 Residential Well Residential Well 12/6/2017 Hfpo Dimer Acid 13252-13-6 0.06300 Y
11 Residential Well Residential Well 12/5/2017 Hfpo Dimer Acid 13252-13-6 0.09400 Y
11 Residential Well Residential Well 12/5/2017 Hfpo Dimer Acid 13252-13-6 0.15000 Y
11 Residential Well Residential Well 2/1/2018 Hfpo Dimer Acid 13252-13-6 0.01800 Y
11 Residential Well Residential Well 2/8/2018 Hfpo Dimer Acid 13252-13-6 0.01400 Y
11 Residential Well Residential Well 12/14/2017 Hfpo Dimer Acid 13252-13-6 0.07800 Y11Residential Well Residential Well 3/1/2018 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 2/7/2018 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 12/15/2017 Hfpo Dimer Acid 13252-13-6 0.02300 Y
11 Residential Well Residential Well 2/8/2018 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 11/13/2017 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 12/6/2017 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 12/7/2017 Hfpo Dimer Acid 13252-13-6 0.42000 Y
11 Residential Well Residential Well 12/7/2017 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 12/7/2017 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 7/27/2018 Hfpo Dimer Acid 13252-13-6 0.12000 Y
11 Residential Well Residential Well 7/27/2018 Hfpo Dimer Acid 13252-13-6 0.02200 Y11Residential Well Residential Well 10/20/2017 Hfpo Dimer Acid 13252-13-6 0.36000 Y
11 Residential Well Residential Well 10/16/2017 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 4/9/2019 Hfpo Dimer Acid 13252-13-6 0.40000 Y
11 Residential Well Residential Well 10/20/2017 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 10/23/2017 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 10/23/2017 Hfpo Dimer Acid 13252-13-6 0.09500 Y
11 Residential Well Residential Well 10/23/2017 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 10/23/2017 Hfpo Dimer Acid 13252-13-6 0.01000 N
11 Residential Well Residential Well 11/6/2017 Hfpo Dimer Acid 13252-13-6 0.34000 Y
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.06000 U N 0.060 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 1.30000 Y 0.57 280-124472-112FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.04600 U N 0.046 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.05400 U N 0.054 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.06000 U N 0.060 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 0.42000 Y 0.081 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.00200 U N 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.00240 Y 0.0020 280-124472-112FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.01100 Y 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00200 U N 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00200 U N 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.03500 U N 0.035 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified PFOA 335-67-1 0.00380 Y 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.03400 U N 0.034 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 0.05800 U N 0.058 280-124472-112FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 0.07900 U N 0.079 280-124472-1
Page 41 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.03700 U N 0.037 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 0.02800 U N 0.028 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.03300 Y 0.030 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.02400 U N 0.024 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 0.21000 U N 0.21 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 0.30000 Y 0.047 280-124472-112FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.02700 U N 0.027 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 0.01000 Y 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.11000 U N 0.11 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified PFOS 1763-23-1 0.00240 Y 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.04100 U N 0.041 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 0.16000 U N 0.16 280-124472-112FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 0.07000 U N 0.070 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 0.05800 U N 0.058 280-124472-1
12 FAY-SW-GBC-1-052919 TAL-SAC GBC-1 05/29/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.01500 U N 0.015 280-124472-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.00450 Y 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 0.90000 Y 0.010 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified Hfpo Dimer Acid 13252-13-6 0.61000 E Y 0.0040 280-124971-112FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified PFOA 335-67-1 0.00370 Y 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.00200 U,*N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.01100 Y 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.00230 Y 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 280-124971-112FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 0.40000 Y 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.00200 U,*N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 0.01700 Y 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 0.06000 Y 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.00200 *J Y 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 0.14000 F1 J Y 0.0050 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 280-124971-112FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 280-124971-1
Page 42 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.02900 Y 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 0.00220 Y 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified PFOS 1763-23-1 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 0.00990 Y 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 280-124971-112FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 0.28000 Y 0.020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 0.00200 U,F1 N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 0.02400 F1 J Y 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 0.04900 F1 J Y 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.00200 U N 0.0020 280-124971-1
12 FAY-SW-GBC-1-060719 TAL-SAC GBC-1 06/07/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.00200 U,H N 0.0020 280-124268-313FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified Hfpo Dimer Acid 13252-13-6 0.02800 Y 0.0040 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.00200 U,H N 0.0020 280-124268-3
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 0.03100 H Y 0.010 280-124268-3
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.00200 U,H N 0.0020 280-124268-3
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.00610 H Y 0.0020 280-124268-3
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified PFOA 335-67-1 0.00680 Y 0.0020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.00200 U,H N 0.0020 280-124268-3
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.0020 280-124268-113FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00500 Y 0.0020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.00680 Y 0.0020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00330 Y 0.0020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.00820 Y 0.0020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.00200 U N 0.0020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 0.04000 H Y 0.0020 280-124268-3
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.00200 U,H N 0.0020 280-124268-313FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 0.00350 H Y 0.0020 280-124268-3
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.00200 U,H N 0.0020 280-124268-3
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 0.00990 H Y 0.0020 280-124268-3
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.00200 U,H N 0.0020 280-124268-3
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.00200 U,H N 0.0020 280-124268-3
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 0.13000 H Y 0.0050 280-124268-3
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 0.00200 U,H N 0.0020 280-124268-313FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 0.01300 Y 0.0020 280-124268-1
Page 43 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 0.02000 U,H N 0.020 280-124268-3
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified PFOS 1763-23-1 0.01300 Y 0.0020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.00200 U,H N 0.0020 280-124268-3
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 280-124268-1
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.00200 U,H N 0.0020 280-124268-3
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.00200 U,H N 0.0020 280-124268-3
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 0.03100 H,F1 J Y 0.0020 280-124268-313FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 0.00960 H,F1 J Y 0.0020 280-124268-3
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 0.00400 H,F1 J Y 0.0020 280-124268-3
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.00200 U,H N 0.0020 280-124268-3
13 FAY-SW-CFR-BLADEN-052219 TAL-SAC CFR-BLADEN 05/22/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 280-124268-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP NVHOS 1132933-86-8 0.00870 Y 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP PES 113507-82-7 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 0.05500 Y 0.010 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP PFECA B 151772-58-6 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified Hfpo Dimer Acid 13252-13-6 0.05700 Y 0.0040 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.00200 U N 0.0020 280-124971-113FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified Perfluorooctadecanoic acid 16517-11-6 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP Byproduct 6 EVS1431 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 0.06400 Y 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.02000 U N 0.020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified Perfluorotetradecanoic Acid 376-06-7 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified Perfluorononanoic Acid 375-95-1 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified Perfluoroheptanoic Acid 375-85-9 0.01000 Y 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified Perfluorobutane Sulfonic Acid 375-73-5 0.00430 Y 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified Perfluorobutanoic Acid 375-22-4 0.00850 Y 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified Perfluorohexane Sulfonic Acid 355-46-4 0.00670 Y 0.0020 280-124971-113FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified Perfluorodecane Sulfonic Acid 335-77-3 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified Perfluorodecanoic Acid 335-76-2 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified Perfluorododecanoic Acid 307-55-1 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.02000 U N 0.020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified PFOA 335-67-1 0.00870 Y 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 0.01600 Y 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.00340 Y 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 0.00640 Y 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified Perfluorooctane Sulfonamide 754-91-6 0.00200 U N 0.0020 280-124971-113FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.02000 U N 0.020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 0.18000 Y 0.0050 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified Perfluorononanesulfonic acid 68259-12-1 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP EVE Acid 69087-46-3 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified Perfluorotridecanoic Acid 72629-94-8 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.00490 Y 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.00240 Y 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.02000 U N 0.020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified PFOS 1763-23-1 0.01500 Y 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified Perfluoroundecanoic Acid 2058-94-8 0.00200 U N 0.0020 280-124971-113FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 0.02000 U N 0.020 280-124971-1
Page 44 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.02000 U N 0.020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified Perfluoropentanoic Acid 2706-90-3 0.02000 Y 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 537 Modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP Hydro-EVE Acid 773804-62-9 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.00200 U N 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP R-EVE EVS1428 0.00630 F1,^J Y 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP Byproduct 5 EVS1430 0.06900 F1,^J Y 0.0020 280-124971-1
13 FAY-SW-CFR-BLADEN-060719 TAL-SAC CFR-BLADEN 06/07/2019 Cl. Spec. Table 3 Compound SOP Byproduct 4 EVS1429 0.01900 F1 J Y 0.0020 280-124971-1
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified 10:2 Fluorotelomer sulfonate 120226-60-0 0.00270 U N 0.0027 202791813FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 Cl. Spec. Table 3 Compound SOP PMPA 13140-29-9 0.05000 U N 0.050 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Hfpo Dimer Acid 13252-13-6 0.01300 Y 0.0018 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol 1691-99-2 0.00270 U N 0.0027 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluorooctadecanoic acid 16517-11-6 0.00180 U N 0.0018 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluorotetradecanoic Acid 376-06-7 0.00089 U N 0.00089 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified 1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)39108-34-4 0.00530 U N 0.0053 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluoroheptane sulfonic acid (PFHpS)375-92-8 0.00180 U N 0.0018 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluorononanoic Acid 375-95-1 0.00180 U N 0.0018 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluoroheptanoic Acid 375-85-9 0.00350 Y 0.00089 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluorobutane Sulfonic Acid 375-73-5 0.00220 J Y 0.00089 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluorobutanoic Acid 375-22-4 0.00530 U N 0.0053 202791813FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluorohexane Sulfonic Acid 355-46-4 0.00330 Y 0.0018 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluorodecane Sulfonic Acid 335-77-3 0.00180 U N 0.0018 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified N-methyl perfluoro-1-octanesulfonamide 31506-32-8 0.00800 U UJ N 0.008 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluorododecanoic Acid 307-55-1 0.00180 U N 0.0018 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluorohexanoic Acid 307-24-4 0.00560 Y 0.0018 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified N-ethyl perfluorooctane sulfonamidoacetic acid 2991-50-6 0.00270 U N 0.0027 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified PFOA 335-67-1 0.00570 Y 0.00089 2027918
Page 45 of 46 August 2019
APPENDIX A
SUMMARY OF ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Pathway Field Sample ID Lab ID Location ID Sample Date Laboratory Analytical Method Parameter Name Parameter
Code
Report
Result
(µg/L)
Lab
Qualifier
Validation
Qualifier Detected
Report
Detection
Limit
(µg/L)
Sample
Delivery
Group (SDG)
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluorodecanoic Acid 335-76-2 0.00180 U N 0.0018 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 Cl. Spec. Table 3 Compound SOP PFO2HxA 39492-88-1 0.05000 U N 0.050 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified N-ethylperfluoro-1-octanesulfonamide 4151-50-2 0.00800 U UJ N 0.008 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 Cl. Spec. Table 3 Compound SOP PFO4DA 39492-90-5 0.05000 U N 0.050 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 Cl. Spec. Table 3 Compound SOP PFO3OA 39492-89-2 0.05000 U N 0.050 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 Cl. Spec. Table 3 Compound SOP PFO5DA 39492-91-6 0.10000 U N 0.10 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified 1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)757124-72-4 0.00270 U N 0.0027 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 Cl. Spec. Table 3 Compound SOP PFMOAA 674-13-5 0.05600 Y 0.050 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluorononanesulfonic acid 68259-12-1 0.00180 U N 0.0018 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluorohexadecanoic acid (PFHxDA)67905-19-5 0.00089 U N 0.00089 202791813FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP2 749836-20-2 0.05000 U N 0.050 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified F-53B Major 73606-19-6 0.00089 U N 0.00089 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluorotridecanoic Acid 72629-94-8 0.00089 U N 0.00089 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluorooctane Sulfonamide 754-91-6 0.00270 U N 0.0027 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified N-methyl perfluorooctane sulfonamidoacetic acid 2355-31-9 0.00270 U N 0.0027 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol 24448-09-7 0.00270 U N 0.0027 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluoroundecanoic Acid 2058-94-8 0.00180 U N 0.0018 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified PFOS 1763-23-1 0.00840 Y 0.0018 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 Cl. Spec. Table 3 Compound SOP PEPA 267239-61-2 0.05000 Y 0.050 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 Cl. Spec. Table 3 Compound SOP PFESA-BP1 29311-67-9 0.05000 U N 0.050 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified 6:2 Fluorotelomer sulfonate 27619-97-2 0.00180 U N 0.0018 202791813FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluoropentanoic Acid 2706-90-3 0.00580 Y 0.0053 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluoropentane sulfonic acid (PFPeS)2706-91-4 0.00180 U N 0.0018 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 Cl. Spec. Table 3 Compound SOP PFECA-G 801212-59-9 0.05000 U N 0.050 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified Perfluorododecane sulfonic acid (PFDoS)79780-39-5 0.00089 U N 0.00089 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified ADONA 958445-44-8 0.00089 U N 0.00089 2027918
13 FAY-SW-CFR-RM-84-020219 LANC CFR-MILE-84 02/04/2019 EPA 537 Rev. 1.1 modified F-53B Minor 83329-89-9 0.00180 U N 0.0018 2027918
Notes:
1. Pathway numbers correspond to Table 1 of the Chemours Fayetteville Works Cape Fear River PFAS Mass Loading Model Assessment and Paragraph 11.1 Characterization of PFAS at Intakes (Geosyntec, 2019).
2. Sampling locations, analytical methods, assessment techniques, and laboratory reports for PFAS concentrations are described in detail in the Seeps and Creeks Investigation Report (Geosyntec, 2019).
3. Onsite laboratory data available only for Outfall 002.
4. Abbreviations
LANC - Eurofins Lancaster
TAL-SAC - TestAmerica Sacramento
J - Analyte detected. Reported value may not be accurate or precise
QA/QC - Quality assurance/ quality controlSOP - standard operating procedure
U – Analyte not detected. Reporting limit may not be accurate or precise.
µg/L - micrograms per liter
-- - No data reported
N - Analyte not detected above associated reporting limit.
Y - Analyte detected above associated reporting limit.
FS - Field Sample
DUP - Duplicate sample
* - Laboratory control spike or laboratory control spike duplicate is outside acceptance limits.
^ - Instrument related quality control is outside acceptance limits.
E - Result exceeded calibration range.F1 - Matrix spike and/or matrix spike duplicate recovery is outside acceptance limits.
H - Sample was prepped or analyzed beyond the specified holding time.
I - Value is estimated maximum possible concentration.
Page 46 of 46 August 2019

Appendix B – Supplemental Flow Gauging Data 1 August 2019
APPENDIX B
SUPPLEMENTAL FLOW GAUGING DATA
APPENDIX B-1
SUMMARY OF FLOW CALCULATIONS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Pathway Sampling Event Start Date End Date Minimum
Flow (L/s)
1st Quartile
Flow (L/s)
Median Flow
(L/s)
3rd Quartile
Flow (L/s)
Maximum
Flow (L/s)
Average Flow
(L/s)
Geomean
Flow (L/s)Comments
1 Surface Water 02/19 2/1/2019 2/7/2019 123,986 138,290 164,036 182,549 267,449 171,093 165,871
2 Surface Water 02/19 2/1/2019 2/7/2019 184 NA NA NA 309 NA NA
3 Surface Water 02/19 2/1/2019 2/7/2019 NA NA NA NA NA NA NA
4 Surface Water 02/19 2/1/2019 2/7/2019 773 813 836 871 1,099 868 863
5 Surface Water 02/19 2/1/2019 2/7/2019 10 19 20 24 15 22 21
6 Surface Water 02/19 2/1/2019 2/7/2019 1.7 NA NA NA 4.3 NA NA
7 Surface Water 02/19 2/1/2019 2/7/2019 2.2 NA NA NA 5.5 NA NA
8 Surface Water 02/19 2/1/2019 2/7/2019 0.5 NA NA NA 1.3 NA NA
9 Surface Water 06/19 6/4/2019 6/7/2019 1.2 NA NA NA 3.1 NA NA Flows at Seep D were not measured in February 2019;
Measurements from June 2019 were used.
10 Surface Water 02/19 2/1/2019 2/7/2019 25 NA NA NA 55 NA NA
11 Surface Water 02/19 2/1/2019 2/7/2019 195 NA NA NA 313 NA NA
12 Surface Water 05/19 5/20/2019 5/30/2019 154 NA NA NA 258 NA NA Flows at GBC were not measured in February 2019;
Measurements from May 2019 were used.
1 Surface Water 05/19 5/20/2019 5/30/2019 30,821 33,756 38,547 44,609 55,558 40,173 39,466
2 Surface Water 05/19 5/20/2019 5/30/2019 183 NA NA NA 184 NA NA
3 Surface Water 05/19 5/20/2019 5/30/2019 NA NA NA NA NA NA NA
4 Surface Water 05/19 5/20/2019 5/30/2019 971 1,052 1,082 1,106 1,200 1,082 1,081
5 Surface Water 05/19 5/20/2019 5/30/2019 10 19 20 24 16 22 21
6A Surface Water 05/19 5/20/2019 5/30/2019 1.9 NA NA NA 3.8 NA NA
6B Surface Water 02/19 2/1/2019 2/7/2019 2.2 NA NA NA 5.5 NA NA Flows at Seep B were not measured in May 2019;
Measurements from Feb 2019 were used.
6C Surface Water 05/19 5/20/2019 5/30/2019 0.4 NA NA NA 1.2 NA NA
6D Surface Water 06/19 6/4/2019 6/7/2019 1.2 NA NA NA 3.1 NA NA Flows at Seep D were not measured in May 2019;
Measurements from June 2019 were used.
7 Surface Water 05/19 5/20/2019 5/30/2019 22 NA NA NA 44 NA NA
8 Surface Water 05/19 5/20/2019 5/30/2019 195 NA NA NA 313 NA NA
9 Surface Water 05/19 5/20/2019 5/30/2019 154 NA NA NA 258 NA NA
1 Surface Water 06/19 6/4/2019 6/7/2019 26,703 27,044 29,670 32,450 32,885 29,824 29,687
2 Surface Water 06/19 6/4/2019 6/7/2019 183 NA NA NA 184 NA NA
3 Surface Water 06/19 6/4/2019 6/7/2019 NA NA NA NA NA NA NA
4 Surface Water 06/19 6/4/2019 6/7/2019 1,139 1,151 1,173 1,197 1,214 1,175 1,174
5 Surface Water 06/19 6/4/2019 6/7/2019 6.3 19 20 24 11 22 21
6A Surface Water 06/19 6/4/2019 6/7/2019 6.9 NA NA NA 12 NA NA
6B Surface Water 06/19 6/4/2019 6/7/2019 1.3 NA NA NA 3.2 NA NA
6C Surface Water 06/19 6/4/2019 6/7/2019 0.3 NA NA NA 0.8 NA NA
6D Surface Water 06/19 6/4/2019 6/7/2019 1.2 NA NA NA 3.1 NA NA
7 Surface Water 06/19 6/4/2019 6/7/2019 28 NA NA NA 32 NA NA
8 Surface Water 06/19 6/4/2019 6/7/2019 195 NA NA NA 313 NA NA
9 Surface Water 06/19 6/4/2019 6/7/2019 161 NA NA NA 271 NA NA
Notes:
1) L/s: Liter per second.
Page 1 of 1 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
1/1/2017 2,500 2.4 0.02 70,792 251 19 2 8,911 0.3 0.2 287.5 12.0
1/2/2017 2,780 2.6 0.61 78,721 251 19 2 9,792 0.3 0.2 284.1 11.8
1/3/2017 5,380 3.7 0.52 152,345 251 20 2 16,796 0.3 0.2 251.8 10.5
1/4/2017 8,630 4.9 0 244,374 251 21 2 24,128 0.4 0.2 225.5 9.4
1/5/2017 8,800 4.9 0 249,188 251 21 2 24,446 0.4 0.2 224.1 9.3
1/6/2017 7,100 4.4 0.35 201,050 251 21 2 20,843 0.3 0.2 236.8 9.9
1/7/2017 7,990 4.7 0.57 226,252 251 21 2 22,734 0.4 0.2 229.5 9.6
1/8/2017 9,260 5.1 0.01 262,214 251 22 2 25,402 0.4 0.2 221.3 9.2
1/9/2017 8,760 4.9 0.04 248,056 251 21 2 24,383 0.4 0.2 224.5 9.4
1/10/2017 7,560 4.5 0.05 214,075 251 21 2 21,850 0.3 0.2 233.1 9.7
1/11/2017 6,720 4.2 0 190,289 251 21 2 19,965 0.3 0.2 239.7 10.0
1/12/2017 6,210 4.1 0 175,848 251 20 2 18,904 0.3 0.2 245.6 10.2
1/13/2017 6,020 4.0 0 170,467 251 20 2 18,468 0.3 0.2 247.5 10.3
1/14/2017 6,040 4.0 0 171,034 251 20 2 18,530 0.3 0.2 247.5 10.3
1/15/2017 5,230 3.7 0 148,097 251 20 2 16,611 0.3 0.2 256.2 10.7
1/16/2017 4,230 3.3 0 119,780 251 20 2 14,103 0.3 0.2 268.9 11.2
1/17/2017 3,810 3.1 0 107,887 251 20 2 12,953 0.3 0.2 274.2 11.4
1/18/2017 3,510 2.9 0 99,392 251 19 2 12,111 0.3 0.2 278.3 11.6
1/19/2017 2,950 2.7 0 83,535 251 19 2 10,383 0.3 0.2 283.9 11.8
1/20/2017 2,680 2.5 0 75,889 251 19 2 9,557 0.3 0.2 287.6 12.0
1/21/2017 2,630 2.5 0.03 74,473 251 19 2 9,322 0.3 0.2 285.9 11.9
1/22/2017 2,670 2.5 0.31 75,606 251 19 2 9,498 0.3 0.2 286.9 12.0
1/23/2017 3,140 2.8 0.04 88,915 251 19 2 10,976 0.3 0.2 282.0 11.7
1/24/2017 5,060 3.6 0 143,283 251 20 2 15,996 0.3 0.2 255.0 10.6
1/25/2017 9,720 5.2 0 275,240 251 22 2 26,360 0.4 0.3 218.8 9.1
1/26/2017 9,340 5.1 0.01 264,479 251 22 2 25,593 0.4 0.2 221.0 9.2
1/27/2017 8,280 4.8 0 234,463 251 21 2 23,367 0.4 0.2 227.6 9.5
1/28/2017 7,470 4.5 0 211,527 251 21 2 21,661 0.3 0.2 233.9 9.7
1/29/2017 7,090 4.4 0 200,766 251 21 2 20,843 0.3 0.2 237.1 9.9
1/30/2017 6,800 4.3 0 192,555 251 21 2 20,153 0.3 0.2 239.1 10.0
1/31/2017 5,970 4.0 0 169,052 251 20 2 18,344 0.3 0.2 247.9 10.3
2/1/2017 4,590 3.4 0 129,974 251 20 2 14,955 0.3 0.2 262.8 11.0
2/2/2017 2,960 2.7 0 83,818 251 19 2 10,442 0.3 0.2 284.6 11.9
2/3/2017 2,660 2.5 0.03 75,323 251 19 2 9,498 0.3 0.2 288.0 12.0
2/4/2017 2,530 2.4 0 71,642 251 19 2 9,028 0.3 0.2 287.9 12.0
2/5/2017 2,410 2.4 0 68,244 251 19 2 8,619 0.3 0.2 288.5 12.0
2/6/2017 2,390 2.3 0 67,677 251 19 2 8,561 0.3 0.2 288.9 12.0
2/7/2017 2,290 2.3 0 64,846 251 19 2 8,153 0.3 0.2 287.2 12.0
2/8/2017 2,030 2.1 0.14 57,483 251 19 2 7,170 0.3 0.2 284.9 11.9
2/9/2017 2,040 2.1 0.16 57,766 251 19 2 7,227 0.3 0.2 285.8 11.9
Page 1 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
2/10/2017 2,170 2.2 0 61,448 251 19 2 7,747 0.3 0.2 288.0 12.0
2/11/2017 2,300 2.3 0 65,129 251 19 2 8,211 0.3 0.2 288.0 12.0
2/12/2017 2,390 2.3 0 67,677 251 19 2 8,561 0.3 0.2 288.9 12.0
2/13/2017 2,260 2.3 0 63,996 251 19 2 8,095 0.3 0.2 288.9 12.0
2/14/2017 2,120 2.2 0 60,032 251 19 2 7,574 0.3 0.2 288.2 12.0
2/15/2017 2,270 2.3 0.7 64,279 251 19 2 8,095 0.3 0.2 287.7 12.0
2/16/2017 3,000 2.7 0 84,951 251 19 2 10,561 0.3 0.2 284.0 11.8
2/17/2017 3,300 2.8 0 93,446 251 19 2 11,513 0.3 0.2 281.4 11.7
2/18/2017 3,240 2.8 0 91,747 251 19 2 11,333 0.3 0.2 282.2 11.8
2/19/2017 2,980 2.7 0 84,384 251 19 2 10,501 0.3 0.2 284.3 11.8
2/20/2017 2,720 2.5 0 77,022 251 19 2 9,674 0.3 0.2 286.9 12.0
2/21/2017 2,540 2.4 0 71,925 251 19 2 9,028 0.3 0.2 286.7 11.9
2/22/2017 2,310 2.3 0 65,412 251 19 2 8,270 0.3 0.2 288.8 12.0
2/23/2017 1,910 2.0 0 54,085 251 18 2 6,710 0.3 0.2 283.4 11.8
2/24/2017 1,800 2.0 0 50,970 251 18 2 6,310 0.3 0.2 282.8 11.8
2/25/2017 1,730 1.9 0 48,988 251 18 2 6,025 0.3 0.2 280.9 11.7
2/26/2017 1,730 1.9 0 48,988 251 18 2 6,025 0.3 0.2 280.9 11.7
2/27/2017 1,690 1.9 0 47,855 251 18 2 5,854 0.3 0.2 279.4 11.6
2/28/2017 1,650 1.8 0 46,723 251 18 2 5,684 0.3 0.2 277.9 11.6
3/1/2017 1,630 1.8 0.46 46,156 251 18 2 5,627 0.3 0.2 278.5 11.6
3/2/2017 1,900 2.0 0.09 53,802 251 18 2 6,710 0.3 0.2 284.9 11.9
3/3/2017 2,240 2.2 0 63,430 251 19 2 7,979 0.3 0.2 287.3 12.0
3/4/2017 2,640 2.5 0 74,756 251 19 2 9,380 0.3 0.2 286.6 11.9
3/5/2017 2,610 2.5 0 73,907 251 19 2 9,322 0.3 0.2 288.1 12.0
3/6/2017 2,180 2.2 0 61,731 251 19 2 7,747 0.3 0.2 286.7 11.9
3/7/2017 1,920 2.0 0 54,368 251 18 2 6,767 0.3 0.2 284.3 11.8
3/8/2017 2,360 2.3 0.01 66,828 251 19 2 8,386 0.3 0.2 286.6 11.9
3/9/2017 2,420 2.4 0 68,527 251 19 2 8,678 0.3 0.2 289.3 12.1
3/10/2017 2,390 2.3 0.06 67,677 251 19 2 8,561 0.3 0.2 288.9 12.0
3/11/2017 2,330 2.3 0 65,978 251 19 2 8,328 0.3 0.2 288.3 12.0
3/12/2017 1,930 2.0 0.19 54,652 251 18 2 6,825 0.3 0.2 285.3 11.9
3/13/2017 1,810 2.0 0.88 51,253 251 18 2 6,367 0.3 0.2 283.7 11.8
3/14/2017 2,320 2.3 0.34 65,695 251 19 2 8,270 0.3 0.2 287.5 12.0
3/15/2017 2,790 2.6 0 79,004 251 19 2 9,910 0.3 0.2 286.5 11.9
3/16/2017 2,860 2.6 0 80,986 251 19 2 10,146 0.3 0.2 286.2 11.9
3/17/2017 2,760 2.6 0 78,154 251 19 2 9,792 0.3 0.2 286.2 11.9
3/18/2017 2,510 2.4 0.24 71,075 251 19 2 8,970 0.3 0.2 288.3 12.0
3/19/2017 2,400 2.3 0 67,960 251 19 2 8,561 0.3 0.2 287.7 12.0
3/20/2017 2,240 2.3 0 63,430 251 19 2 8,037 0.3 0.2 289.4 12.1
3/21/2017 2,280 2.3 0.01 64,562 251 19 2 8,153 0.3 0.2 288.5 12.0
Page 2 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
3/22/2017 2,610 0.37 73,907 251 16 2 -5,339 -0.5 -0.3 -165.0 -6.9
3/23/2017 2,730 2.5 0 77,305 251 19 2 9,674 0.3 0.2 285.9 11.9
3/24/2017 2,590 2.5 0 73,341 251 19 2 9,204 0.3 0.2 286.7 11.9
3/25/2017 2,060 2.1 0 58,333 251 19 2 7,343 0.3 0.2 287.5 12.0
3/26/2017 1,820 2.0 0 51,537 251 18 2 6,367 0.3 0.2 282.2 11.8
3/27/2017 1,640 1.8 0 46,440 251 18 2 5,627 0.3 0.2 276.8 11.5
3/28/2017 1,580 1.8 0.14 44,741 251 18 2 5,344 0.3 0.2 272.8 11.4
3/29/2017 1,580 1.8 0 44,741 251 18 2 5,400 0.3 0.2 275.7 11.5
3/30/2017 1,540 1.8 0 43,608 251 18 2 5,231 0.3 0.2 274.0 11.4
3/31/2017 1,790 1.9 1.24 50,687 251 18 2 6,253 0.3 0.2 281.8 11.7
4/1/2017 2,820 2.6 0 79,854 251 19 2 9,969 0.3 0.2 285.2 11.9
4/2/2017 3,000 2.7 0 84,951 251 19 2 10,561 0.3 0.2 284.0 11.8
4/3/2017 2,640 2.5 0.57 74,756 251 19 2 9,380 0.3 0.2 286.6 11.9
4/4/2017 3,040 2.7 0 86,083 251 19 2 10,679 0.3 0.2 283.4 11.8
4/5/2017 4,200 3.3 0.84 118,931 251 20 2 13,981 0.3 0.2 268.5 11.2
4/6/2017 5,620 3.8 0.01 159,141 251 20 2 17,538 0.3 0.2 251.7 10.5
4/7/2017 6,570 4.2 0 186,042 251 21 2 19,653 0.3 0.2 241.3 10.1
4/8/2017 7,730 4.6 0 218,889 251 21 2 22,228 0.3 0.2 232.0 9.7
4/9/2017 6,980 4.3 0 197,652 251 21 2 20,592 0.3 0.2 238.0 9.9
4/10/2017 4,940 3.6 0 139,885 251 20 2 15,812 0.3 0.2 258.2 10.8
4/11/2017 2,670 2.5 0 75,606 251 19 2 9,439 0.3 0.2 285.2 11.9
4/12/2017 2,070 2.1 0 58,616 251 19 2 7,343 0.3 0.2 286.1 11.9
4/13/2017 1,850 2.0 0 52,386 251 18 2 6,481 0.3 0.2 282.6 11.8
4/14/2017 1,740 1.9 0 49,271 251 18 2 6,082 0.3 0.2 281.9 11.7
4/15/2017 1,670 1.9 0 47,289 251 18 2 5,797 0.3 0.2 280.0 11.7
4/16/2017 1,580 1.8 0 44,741 251 18 2 5,400 0.3 0.2 275.7 11.5
4/17/2017 1,510 1.7 0.04 42,758 251 18 2 5,062 0.3 0.2 270.4 11.3
4/18/2017 1,480 1.7 0.02 41,909 251 18 2 4,949 0.3 0.2 269.8 11.2
4/19/2017 1,360 1.6 0 38,511 251 18 2 4,388 0.3 0.2 260.3 10.8
4/20/2017 1,290 1.6 0 36,529 251 18 2 4,053 0.3 0.2 253.5 10.6
4/21/2017 1,260 1.5 0 35,679 251 18 2 3,942 0.3 0.2 252.4 10.5
4/22/2017 1,260 1.5 0.18 35,679 251 18 2 3,942 0.3 0.2 252.4 10.5
4/23/2017 1,300 1.6 0.13 36,812 251 18 2 4,109 0.3 0.2 255.0 10.6
4/24/2017 2,160 2.1 3.07 61,164 251 19 2 7,343 0.3 0.2 274.2 11.4
4/25/2017 12,700 0.12 359,624 251 16 2 -5,339 -2.4 -1.6 -33.9 -1.4
4/26/2017 24,500 14.9 0 693,763 251 31 2 88,288 0.3 0.2 290.7 12.1
4/27/2017 23,200 15.7 0 656,951 251 32 2 92,911 0.2 0.2 323.1 13.5
4/28/2017 22,000 15.2 0 622,971 251 32 2 90,038 0.2 0.2 330.1 13.8
4/29/2017 19,800 13.7 0 560,674 251 30 2 80,690 0.2 0.2 328.7 13.7
4/30/2017 17,600 11.7 0 498,377 251 28 2 68,031 0.3 0.2 311.8 13.0
Page 3 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
5/1/2017 16,000 10.0 0.39 453,070 251 26 2 57,525 0.3 0.2 290.0 12.1
5/2/2017 15,000 9.1 0 424,753 251 25 2 51,207 0.3 0.2 275.4 11.5
5/3/2017 14,300 8.4 0 404,931 251 25 2 46,829 0.3 0.2 264.2 11.0
5/4/2017 13,800 7.9 0.02 390,772 251 24 2 43,493 0.3 0.2 254.2 10.6
5/5/2017 13,700 7.7 0.83 387,941 251 24 2 42,512 0.3 0.2 250.3 10.4
5/6/2017 14,700 8.3 0 416,258 251 25 2 46,044 0.3 0.2 252.7 10.5
5/7/2017 14,400 8.3 0 407,763 251 25 2 45,978 0.3 0.2 257.6 10.7
5/8/2017 11,400 6.6 0 322,812 251 23 2 35,270 0.3 0.2 249.6 10.4
5/9/2017 7,790 4.7 0 220,588 251 21 2 22,860 0.3 0.2 236.7 9.9
5/10/2017 5,710 3.9 0 161,689 251 20 2 18,220 0.3 0.2 257.4 10.7
5/11/2017 3,560 3.1 0 100,808 251 19 2 12,772 0.3 0.2 289.4 12.1
5/12/2017 3,130 2.8 0 88,632 251 19 2 11,513 0.3 0.2 296.7 12.4
5/13/2017 2,770 2.7 0.02 78,438 251 19 2 10,383 0.3 0.2 302.4 12.6
5/14/2017 2,530 2.5 0 71,642 251 19 2 9,557 0.3 0.2 304.7 12.7
5/15/2017 2,410 2.4 0 68,244 251 19 2 9,146 0.3 0.2 306.1 12.8
5/16/2017 2,150 2.3 0 60,881 251 19 2 8,153 0.3 0.2 305.9 12.7
5/17/2017 1,650 1.9 0 46,723 251 18 2 6,196 0.3 0.2 302.9 12.6
5/18/2017 1,460 1.8 0 41,343 251 18 2 5,400 0.3 0.2 298.4 12.4
5/19/2017 1,360 1.7 0 38,511 251 18 2 4,893 0.3 0.2 290.2 12.1
5/20/2017 1,270 1.6 0 35,962 251 18 2 4,444 0.3 0.2 282.3 11.8
5/21/2017 1,480 1.8 0 41,909 251 18 2 5,457 0.3 0.2 297.4 12.4
5/22/2017 1,490 1.8 1.25 42,192 251 18 2 5,514 0.3 0.2 298.5 12.4
5/23/2017 2,520 2.5 0.76 71,358 251 19 2 9,204 0.3 0.2 294.6 12.3
5/24/2017 5,640 3.9 0.35 159,707 251 20 2 18,033 0.3 0.2 257.9 10.7
5/25/2017 9,210 5.2 0 260,798 251 22 2 25,848 0.4 0.2 226.4 9.4
5/26/2017 11,900 6.0 0 336,970 251 22 2 30,990 0.4 0.3 210.1 8.8
5/27/2017 12,900 6.6 0 365,287 251 23 2 35,074 0.4 0.3 219.3 9.1
5/28/2017 10,700 5.6 0.06 302,990 251 22 2 28,926 0.4 0.3 218.1 9.1
5/29/2017 7,890 0.26 223,420 251 16 2 -5,339 -1.5 -1.0 -54.6 -2.3
5/30/2017 6,800 0.08 192,555 251 16 2 -5,339 -1.3 -0.9 -63.3 -2.6
5/31/2017 6,860 0 194,254 251 16 2 -5,339 -1.3 -0.9 -62.8 -2.6
6/1/2017 7,510 0 212,660 251 16 2 -5,339 -1.4 -1.0 -57.3 -2.4
6/2/2017 7,680 4.7 0 217,473 251 21 2 22,671 0.3 0.2 238.1 9.9
6/3/2017 6,570 4.3 0.13 186,042 251 21 2 20,216 0.3 0.2 248.2 10.3
6/4/2017 4,360 3.4 0 123,461 251 20 2 14,955 0.3 0.2 276.7 11.5
6/5/2017 2,810 2.7 1.66 79,570 251 19 2 10,501 0.3 0.2 301.5 12.6
6/6/2017 3,460 3.0 0 97,976 251 19 2 12,471 0.3 0.2 290.8 12.1
6/7/2017 4,190 3.4 0 118,648 251 20 2 14,589 0.3 0.2 280.9 11.7
6/8/2017 4,530 3.5 0.02 128,275 251 20 2 15,444 0.3 0.2 275.0 11.5
6/9/2017 4,540 3.5 0 128,558 251 20 2 15,444 0.3 0.2 274.4 11.4
Page 4 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
6/10/2017 3,500 3.0 0 99,109 251 19 2 12,591 0.3 0.2 290.2 12.1
6/11/2017 2,340 2.4 0 66,261 251 19 2 8,853 0.3 0.2 305.2 12.7
6/12/2017 1,960 2.2 0 55,501 251 19 2 7,458 0.3 0.2 307.0 12.8
6/13/2017 1,530 1.8 0 43,325 251 18 2 5,684 0.3 0.2 299.7 12.5
6/14/2017 1,130 1.5 0.96 31,998 251 18 2 3,775 0.3 0.2 269.5 11.2
6/15/2017 1,300 1.7 0.03 36,812 251 18 2 4,612 0.3 0.2 286.2 11.9
6/16/2017 1,530 1.8 0.04 43,325 251 18 2 5,684 0.3 0.2 299.7 12.5
6/17/2017 1,460 1.8 0.03 41,343 251 18 2 5,400 0.3 0.2 298.4 12.4
6/18/2017 1,900 2.1 0 53,802 251 19 2 7,170 0.3 0.2 304.4 12.7
6/19/2017 2,010 2.2 0 56,917 251 19 2 7,631 0.3 0.2 306.3 12.8
6/20/2017 3,220 2.8 0.74 91,180 251 19 2 11,453 0.3 0.2 286.9 12.0
6/21/2017 5,400 3.8 0.12 152,911 251 20 2 17,538 0.3 0.2 262.0 10.9
6/22/2017 9,480 5.2 0.4 268,444 251 22 2 26,360 0.4 0.2 224.3 9.3
6/23/2017 8,360 4.9 0 236,729 251 21 2 24,128 0.3 0.2 232.8 9.7
6/24/2017 8,710 5.0 1.93 246,640 251 21 2 24,764 0.4 0.2 229.4 9.6
6/25/2017 11,700 5.9 0.01 331,307 251 22 2 30,602 0.4 0.3 211.0 8.8
6/26/2017 11,600 5.9 0 328,475 251 22 2 30,538 0.4 0.3 212.4 8.8
6/27/2017 10,200 5.5 0 288,832 251 22 2 27,833 0.4 0.2 220.1 9.2
6/28/2017 9,160 5.1 0 259,382 251 22 2 25,721 0.4 0.2 226.5 9.4
6/29/2017 8,060 4.8 0 228,234 251 21 2 23,430 0.3 0.2 234.5 9.8
6/30/2017 6,560 4.3 1.84 185,759 251 21 2 20,216 0.3 0.2 248.6 10.4
7/1/2017 5,420 3.8 0.01 153,477 251 20 2 17,538 0.3 0.2 261.0 10.9
7/2/2017 3,110 2.8 0 88,065 251 19 2 11,453 0.3 0.2 297.1 12.4
7/3/2017 2,730 2.6 0.2 77,305 251 19 2 10,205 0.3 0.2 301.5 12.6
7/4/2017 3,170 2.9 0.03 89,764 251 19 2 11,632 0.3 0.2 296.0 12.3
7/5/2017 2,820 2.7 0 79,854 251 19 2 10,501 0.3 0.2 300.4 12.5
7/6/2017 2,300 2.4 0 65,129 251 19 2 8,736 0.3 0.2 306.4 12.8
7/7/2017 1,880 2.1 0 53,236 251 19 2 7,170 0.3 0.2 307.6 12.8
7/8/2017 1,710 2.0 0 48,422 251 18 2 6,481 0.3 0.2 305.7 12.7
7/9/2017 1,680 2.0 0 47,572 251 18 2 6,310 0.3 0.2 303.0 12.6
7/10/2017 1,630 1.9 0.82 46,156 251 18 2 6,082 0.3 0.2 301.0 12.5
7/11/2017 1,510 1.8 0 42,758 251 18 2 5,570 0.3 0.2 297.6 12.4
7/12/2017 1,530 1.8 0 43,325 251 18 2 5,684 0.3 0.2 299.7 12.5
7/13/2017 1,430 1.8 0 40,493 251 18 2 5,231 0.3 0.2 295.1 12.3
7/14/2017 1,220 1.6 0 34,547 251 18 2 4,221 0.3 0.2 279.1 11.6
7/15/2017 1,130 1.5 0.33 31,998 251 18 2 3,775 0.3 0.2 269.5 11.2
7/16/2017 1,310 1.7 0.12 37,095 251 18 2 4,668 0.3 0.2 287.5 12.0
7/17/2017 1,430 1.8 0.05 40,493 251 18 2 5,231 0.3 0.2 295.1 12.3
7/18/2017 1,420 1.8 0.31 40,210 251 18 2 5,175 0.3 0.2 294.0 12.2
7/19/2017 1,320 1.7 0 37,378 251 18 2 4,724 0.3 0.2 288.7 12.0
Page 5 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
7/20/2017 1,320 1.7 0 37,378 251 18 2 4,724 0.3 0.2 288.7 12.0
7/21/2017 1,410 1.7 0 39,927 251 18 2 5,118 0.3 0.2 292.8 12.2
7/22/2017 1,480 1.8 0 41,909 251 18 2 5,457 0.3 0.2 297.4 12.4
7/23/2017 1,360 1.7 0.13 38,511 251 18 2 4,893 0.3 0.2 290.2 12.1
7/24/2017 1,490 1.8 0 42,192 251 18 2 5,457 0.3 0.2 295.4 12.3
7/25/2017 1,420 1.8 0 40,210 251 18 2 5,175 0.3 0.2 294.0 12.2
7/26/2017 1,300 1.7 0 36,812 251 18 2 4,612 0.3 0.2 286.2 11.9
7/27/2017 1,140 1.5 0 32,281 251 18 2 3,831 0.3 0.2 271.1 11.3
7/28/2017 1,050 1.4 0 29,733 251 18 2 3,384 0.3 0.2 260.0 10.8
7/29/2017 1,060 1.4 0.44 30,016 251 18 2 3,384 0.3 0.2 257.5 10.7
7/30/2017 1,050 1.4 0 29,733 251 18 2 3,384 0.3 0.2 260.0 10.8
7/31/2017 1,050 1.4 0 29,733 251 18 2 3,328 0.3 0.2 255.7 10.7
8/1/2017 1,010 1.4 0 28,600 251 18 2 3,159 0.3 0.2 252.3 10.5
8/2/2017 964 1.3 0 27,297 251 18 2 2,877 0.3 0.2 240.7 10.0
8/3/2017 946 1.3 0 26,788 251 18 2 2,763 0.3 0.2 235.6 9.8
8/4/2017 929 1.3 0.02 26,306 251 18 2 2,650 0.4 0.2 230.1 9.6
8/5/2017 943 1.3 0 26,703 251 18 2 2,763 0.3 0.2 236.4 9.8
8/6/2017 941 1.3 0 26,646 251 18 2 2,763 0.3 0.2 236.9 9.9
8/7/2017 994 1.4 0.12 28,147 251 18 2 3,047 0.3 0.2 247.2 10.3
8/8/2017 1,210 1.6 1.4 34,263 251 18 2 4,165 0.3 0.2 277.7 11.6
8/9/2017 1,380 1.7 0.11 39,077 251 18 2 5,005 0.3 0.2 292.6 12.2
8/10/2017 1,460 1.8 0 41,343 251 18 2 5,344 0.3 0.2 295.3 12.3
8/11/2017 1,300 1.7 0.01 36,812 251 18 2 4,612 0.3 0.2 286.2 11.9
8/12/2017 1,270 1.6 0.47 35,962 251 18 2 4,444 0.3 0.2 282.3 11.8
8/13/2017 2,290 2.3 1.72 64,846 251 19 2 8,561 0.3 0.2 301.6 12.6
8/14/2017 2,880 2.7 0.01 81,553 251 19 2 10,679 0.3 0.2 299.1 12.5
8/15/2017 1,910 2.1 0.05 54,085 251 19 2 7,227 0.3 0.2 305.2 12.7
8/16/2017 1,460 1.8 0 41,343 251 18 2 5,400 0.3 0.2 298.4 12.4
8/17/2017 1,280 1.6 0.24 36,246 251 18 2 4,500 0.3 0.2 283.6 11.8
8/18/2017 1,360 1.7 0 38,511 251 18 2 4,893 0.3 0.2 290.2 12.1
8/19/2017 1,330 1.7 0 37,661 251 18 2 4,780 0.3 0.2 289.9 12.1
8/20/2017 1,160 1.5 0 32,848 251 18 2 3,942 0.3 0.2 274.1 11.4
8/21/2017 1,030 1.4 0 29,166 251 18 2 3,272 0.3 0.2 256.2 10.7
8/22/2017 1,020 1.4 0 28,883 251 18 2 3,216 0.3 0.2 254.3 10.6
8/23/2017 1,000 1.4 1.02 28,317 251 18 2 3,103 0.3 0.2 250.3 10.4
8/24/2017 1,060 1.4 0 30,016 251 18 2 3,384 0.3 0.2 257.5 10.7
8/25/2017 1,110 1.5 0 31,432 251 18 2 3,664 0.3 0.2 266.3 11.1
8/26/2017 984 1.4 0 27,864 251 18 2 2,990 0.3 0.2 245.1 10.2
8/27/2017 892 1.3 0 25,259 251 18 2 2,479 0.4 0.2 224.1 9.3
8/28/2017 999 1.4 0.22 28,289 251 18 2 3,047 0.3 0.2 246.0 10.2
Page 6 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
8/29/2017 1,000 1.4 0.01 28,317 251 18 2 3,103 0.3 0.2 250.3 10.4
8/30/2017 930 1.3 0 26,335 251 18 2 2,650 0.4 0.2 229.8 9.6
8/31/2017 885 1.3 0.29 25,060 251 18 2 2,421 0.4 0.2 220.7 9.2
9/1/2017 994 1.4 0.93 28,147 251 18 2 2,990 0.3 0.2 242.6 10.1
9/2/2017 2,240 2.3 0.05 63,430 251 19 2 8,503 0.3 0.2 306.2 12.8
9/3/2017 2,290 2.4 0 64,846 251 19 2 8,678 0.3 0.2 305.7 12.7
9/4/2017 1,630 1.9 0 46,156 251 18 2 6,082 0.3 0.2 301.0 12.5
9/5/2017 1,330 1.7 0.05 37,661 251 18 2 4,780 0.3 0.2 289.9 12.1
9/6/2017 1,480 1.8 0.57 41,909 251 18 2 5,457 0.3 0.2 297.4 12.4
9/7/2017 1,680 2.0 0 47,572 251 18 2 6,310 0.3 0.2 303.0 12.6
9/8/2017 1,750 2.0 0 49,554 251 18 2 6,596 0.3 0.2 304.0 12.7
9/9/2017 1,410 1.7 0 39,927 251 18 2 5,118 0.3 0.2 292.8 12.2
9/10/2017 1,250 1.6 0 35,396 251 18 2 4,388 0.3 0.2 283.2 11.8
9/11/2017 1,160 1.5 0.05 32,848 251 18 2 3,887 0.3 0.2 270.3 11.3
9/12/2017 1,310 1.7 0.96 37,095 251 18 2 4,612 0.3 0.2 284.0 11.8
9/13/2017 1,500 1.8 0 42,475 251 18 2 5,570 0.3 0.2 299.6 12.5
9/14/2017 1,380 1.7 0 39,077 251 18 2 5,005 0.3 0.2 292.6 12.2
9/15/2017 1,250 1.6 0 35,396 251 18 2 4,388 0.3 0.2 283.2 11.8
9/16/2017 1,170 1.5 0 33,131 251 18 2 3,942 0.3 0.2 271.8 11.3
9/17/2017 1,090 1.5 0 30,865 251 18 2 3,552 0.3 0.2 262.9 11.0
9/18/2017 1,010 1.4 0 28,600 251 18 2 3,159 0.3 0.2 252.3 10.5
9/19/2017 948 1.3 0 26,844 251 18 2 2,763 0.3 0.2 235.1 9.8
9/20/2017 923 1.3 0.28 26,136 251 18 2 2,650 0.3 0.2 231.6 9.6
9/21/2017 943 1.3 0 26,703 251 18 2 2,763 0.3 0.2 236.4 9.8
9/22/2017 892 1.3 0 25,259 251 18 2 2,479 0.4 0.2 224.1 9.3
9/23/2017 860 1.2 0 24,352 251 18 2 2,250 0.4 0.3 211.0 8.8
9/24/2017 839 1.2 0 23,758 251 18 2 2,135 0.4 0.3 205.2 8.6
9/25/2017 814 1.2 0 23,050 251 18 2 1,962 0.4 0.3 194.4 8.1
9/26/2017 820 1.2 0 23,220 251 18 2 2,020 0.4 0.3 198.7 8.3
9/27/2017 804 1.2 0 22,767 251 18 2 1,904 0.4 0.3 191.0 8.0
9/28/2017 786 1.2 0 22,257 251 18 2 1,788 0.4 0.3 183.5 7.6
9/29/2017 793 1.2 0 22,455 251 18 2 1,846 0.4 0.3 187.8 7.8
9/30/2017 777 1.1 0 22,002 251 18 2 1,730 0.4 0.3 179.7 7.5
10/1/2017 775 1.1 0 21,946 251 18 2 1,730 0.4 0.3 180.1 7.5
10/2/2017 758 1.1 0 21,464 251 18 2 1,614 0.5 0.3 171.8 7.2
10/3/2017 766 1.1 0 21,691 251 18 2 1,672 0.5 0.3 176.1 7.3
10/4/2017 792 1.2 0 22,427 251 18 2 1,846 0.4 0.3 188.0 7.8
10/5/2017 790 1.2 0 22,370 251 18 2 1,788 0.4 0.3 182.6 7.6
10/6/2017 791 1.2 0 22,399 251 18 2 1,846 0.4 0.3 188.3 7.8
10/7/2017 786 1.2 1.86 22,257 251 18 2 1,788 0.4 0.3 183.5 7.6
Page 7 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
10/8/2017 893 1.3 1.14 25,287 251 18 2 2,421 0.4 0.3 218.7 9.1
10/9/2017 1,040 1.4 0.08 29,450 251 18 2 3,272 0.3 0.2 253.8 10.6
10/10/2017 1,050 1.4 0 29,733 251 18 2 3,328 0.3 0.2 255.7 10.7
10/11/2017 1,030 1.4 0 29,166 251 18 2 3,216 0.3 0.2 251.8 10.5
10/12/2017 957 1.3 0 27,099 251 18 2 2,820 0.3 0.2 237.7 9.9
10/13/2017 974 1.4 0 27,581 251 18 2 2,933 0.3 0.2 242.9 10.1
10/14/2017 986 1.4 0 27,920 251 18 2 2,990 0.3 0.2 244.6 10.2
10/15/2017 907 1.3 0 25,683 251 18 2 2,536 0.4 0.2 225.5 9.4
10/16/2017 841 1.2 0.09 23,814 251 18 2 2,135 0.4 0.3 204.8 8.5
10/17/2017 839 1.2 0.01 23,758 251 18 2 2,135 0.4 0.3 205.2 8.6
10/18/2017 814 1.2 0 23,050 251 18 2 1,962 0.4 0.3 194.4 8.1
10/19/2017 780 1.1 0 22,087 251 18 2 1,730 0.5 0.3 179.0 7.5
10/20/2017 771 1.1 0 21,832 251 18 2 1,672 0.5 0.3 175.0 7.3
10/21/2017 770 1.1 0 21,804 251 18 2 1,672 0.5 0.3 175.2 7.3
10/22/2017 761 1.1 0 21,549 251 18 2 1,614 0.5 0.3 171.1 7.1
10/23/2017 741 1.1 0.15 20,983 251 18 2 1,498 0.5 0.3 163.1 6.8
10/24/2017 928 1.3 0.01 26,278 251 18 2 2,650 0.4 0.2 230.3 9.6
10/25/2017 1,370 1.7 0 38,794 251 18 2 4,949 0.3 0.2 291.4 12.1
10/26/2017 1,360 1.7 0 38,511 251 18 2 4,893 0.3 0.2 290.2 12.1
10/27/2017 1,190 1.6 0 33,697 251 18 2 4,109 0.3 0.2 278.5 11.6
10/28/2017 1,050 1.4 0.73 29,733 251 18 2 3,328 0.3 0.2 255.7 10.7
10/29/2017 1,250 1.6 0.03 35,396 251 18 2 4,388 0.3 0.2 283.2 11.8
10/30/2017 1,220 1.6 0 34,547 251 18 2 4,221 0.3 0.2 279.1 11.6
10/31/2017 1,040 1.4 0 29,450 251 18 2 3,272 0.3 0.2 253.8 10.6
11/1/2017 900 1.3 0 25,485 251 18 2 2,479 0.4 0.2 222.2 9.3
11/2/2017 803 1.2 0 22,738 251 18 2 1,904 0.4 0.3 191.3 8.0
11/3/2017 776 1.1 0 21,974 251 18 2 1,730 0.4 0.3 179.9 7.5
11/4/2017 792 1.2 0 22,427 251 18 2 1,846 0.4 0.3 188.0 7.8
11/5/2017 755 1.1 0 21,379 251 18 2 1,556 0.5 0.3 166.3 6.9
11/6/2017 756 1.1 0 21,408 251 18 2 1,556 0.5 0.3 166.1 6.9
11/7/2017 792 1.2 0 22,427 251 18 2 1,846 0.4 0.3 188.0 7.8
11/8/2017 804 1.2 0.03 22,767 251 18 2 1,904 0.4 0.3 191.0 8.0
11/9/2017 819 1.2 0.22 23,191 251 18 2 2,020 0.4 0.3 198.9 8.3
11/10/2017 881 1.3 0.01 24,947 251 18 2 2,364 0.4 0.3 216.5 9.0
11/11/2017 897 1.3 0 25,400 251 18 2 2,479 0.4 0.2 222.9 9.3
11/12/2017 874 1.3 0 24,749 251 18 2 2,364 0.4 0.3 218.2 9.1
11/13/2017 863 1.2 0.14 24,437 251 18 2 2,250 0.4 0.3 210.3 8.8
11/14/2017 899 1.3 0 25,457 251 18 2 2,479 0.4 0.2 222.4 9.3
11/15/2017 955 1.3 0 27,043 251 18 2 2,820 0.3 0.2 238.2 9.9
11/16/2017 973 1.4 0 27,552 251 18 2 2,933 0.3 0.2 243.2 10.1
Page 8 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
11/17/2017 917 1.3 0 25,967 251 18 2 2,593 0.4 0.2 228.1 9.5
11/18/2017 854 1.2 0 24,183 251 18 2 2,192 0.4 0.3 207.1 8.6
11/19/2017 856 1.2 0.06 24,239 251 18 2 2,250 0.4 0.3 212.0 8.8
11/20/2017 856 1.2 0 24,239 251 18 2 2,250 0.4 0.3 212.0 8.8
11/21/2017 832 1.2 0 23,560 251 18 2 2,077 0.4 0.3 201.4 8.4
11/22/2017 829 1.2 0.03 23,475 251 18 2 2,077 0.4 0.3 202.1 8.4
11/23/2017 867 1.2 0 24,551 251 18 2 2,307 0.4 0.3 214.6 8.9
11/24/2017 890 1.3 0 25,202 251 18 2 2,421 0.4 0.3 219.5 9.1
11/25/2017 863 1.2 0 24,437 251 18 2 2,250 0.4 0.3 210.3 8.8
11/26/2017 830 1.2 0 23,503 251 18 2 2,077 0.4 0.3 201.9 8.4
11/27/2017 799 1.2 0 22,625 251 18 2 1,846 0.4 0.3 186.4 7.8
11/28/2017 797 1.2 0 22,569 251 18 2 1,846 0.4 0.3 186.9 7.8
11/29/2017 793 1.2 0 22,455 251 18 2 1,846 0.4 0.3 187.8 7.8
11/30/2017 790 1.2 0 22,370 251 18 2 1,788 0.4 0.3 182.6 7.6
12/1/2017 814 1.2 0 23,050 251 18 2 1,962 0.4 0.3 194.4 8.1
12/2/2017 803 1.2 0.09 22,738 251 18 2 1,904 0.4 0.3 191.3 8.0
12/3/2017 792 1.2 0.01 22,427 251 18 2 1,846 0.4 0.3 188.0 7.8
12/4/2017 797 1.2 0 22,569 251 18 2 1,846 0.4 0.3 186.9 7.8
12/5/2017 802 1.2 0 22,710 251 18 2 1,904 0.4 0.3 191.5 8.0
12/6/2017 843 1.2 0.24 23,871 251 18 2 2,135 0.4 0.3 204.3 8.5
12/7/2017 870 1.2 0.07 24,636 251 18 2 2,307 0.4 0.3 213.9 8.9
12/8/2017 994 1.4 2.43 28,147 251 18 2 3,047 0.3 0.2 247.2 10.3
12/9/2017 1,950 2.1 0.3 55,218 251 19 2 7,400 0.3 0.2 306.1 12.8
12/10/2017 2,350 2.4 0 66,545 251 19 2 8,911 0.3 0.2 305.9 12.7
12/11/2017 2,190 2.3 0 62,014 251 19 2 8,328 0.3 0.2 306.7 12.8
12/12/2017 1,850 2.1 0 52,386 251 19 2 7,055 0.3 0.2 307.6 12.8
12/13/2017 1,560 1.9 0 44,174 251 18 2 5,797 0.3 0.2 299.8 12.5
12/14/2017 1,360 1.7 0 38,511 251 18 2 4,893 0.3 0.2 290.2 12.1
12/15/2017 1,160 1.5 0 32,848 251 18 2 3,942 0.3 0.2 274.1 11.4
12/16/2017 1,040 1.4 0 29,450 251 18 2 3,272 0.3 0.2 253.8 10.6
12/17/2017 966 1.3 0 27,354 251 18 2 2,877 0.3 0.2 240.2 10.0
12/18/2017 934 1.3 0 26,448 251 18 2 2,707 0.3 0.2 233.8 9.7
12/19/2017 898 1.3 0 25,429 251 18 2 2,479 0.4 0.2 222.6 9.3
12/20/2017 962 1.3 0.57 27,241 251 18 2 2,877 0.3 0.2 241.2 10.1
12/21/2017 1,270 1.6 0 35,962 251 18 2 4,444 0.3 0.2 282.3 11.8
12/22/2017 1,460 1.8 0 41,343 251 18 2 5,344 0.3 0.2 295.3 12.3
12/23/2017 1,410 1.8 0 39,927 251 18 2 5,175 0.3 0.2 296.0 12.3
12/24/2017 1,290 1.6 0.03 36,529 251 18 2 4,556 0.3 0.2 284.9 11.9
12/25/2017 1,150 1.5 0.01 32,564 251 18 2 3,887 0.3 0.2 272.6 11.4
12/26/2017 1,050 1.4 0 29,733 251 18 2 3,384 0.3 0.2 260.0 10.8
Page 9 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
12/27/2017 1,010 1.4 0.15 28,600 251 18 2 3,103 0.3 0.2 247.8 10.3
12/28/2017 991 1.4 0 28,062 251 18 2 3,047 0.3 0.2 248.0 10.3
12/29/2017 966 1.3 0 27,354 251 18 2 2,877 0.3 0.2 240.2 10.0
12/30/2017 911 1.3 0 25,797 251 18 2 2,593 0.4 0.2 229.6 9.6
12/31/2017 897 1.3 0 25,400 251 18 2 2,479 0.4 0.2 222.9 9.3
1/1/2018 867 1.2 0 24,551 251 18 2 2,307 0.4 0.3 214.6 8.9
1/2/2018 837 1.2 0 23,701 251 18 2 2,135 0.4 0.3 205.7 8.6
1/3/2018 828 1.2 0 23,446 251 18 2 2,077 0.4 0.3 202.4 8.4
1/4/2018 823 1.2 0.01 23,305 251 18 2 2,020 0.4 0.3 197.9 8.2
1/5/2018 827 1.2 0 23,418 251 18 2 2,077 0.4 0.3 202.6 8.4
1/6/2018 814 1.2 0 23,050 251 18 2 1,962 0.4 0.3 194.4 8.1
1/7/2018 806 1.2 0 22,823 251 18 2 1,904 0.4 0.3 190.6 7.9
1/8/2018 830 1.2 0 23,503 251 18 2 2,077 0.4 0.3 201.9 8.4
1/9/2018 853 1.2 0 24,154 251 18 2 2,192 0.4 0.3 207.3 8.6
1/10/2018 854 1.2 0 24,183 251 18 2 2,192 0.4 0.3 207.1 8.6
1/11/2018 893 1.3 0.09 25,287 251 18 2 2,479 0.4 0.2 223.9 9.3
1/12/2018 933 1.3 0.22 26,420 251 18 2 2,707 0.3 0.2 234.0 9.8
1/13/2018 1,090 1.5 0 30,865 251 18 2 3,552 0.3 0.2 262.9 11.0
1/14/2018 1,300 1.7 0 36,812 251 18 2 4,612 0.3 0.2 286.2 11.9
1/15/2018 1,290 1.6 0 36,529 251 18 2 4,556 0.3 0.2 284.9 11.9
1/16/2018 1,200 1.6 0 33,980 251 18 2 4,109 0.3 0.2 276.2 11.5
1/17/2018 1,230 1.6 0.2 34,830 251 18 2 4,276 0.3 0.2 280.5 11.7
1/18/2018 1,200 1.6 0.07 33,980 251 18 2 4,109 0.3 0.2 276.2 11.5
1/19/2018 1,140 1.5 0.01 32,281 251 18 2 3,831 0.3 0.2 271.1 11.3
1/20/2018 1,060 1.4 0 30,016 251 18 2 3,384 0.3 0.2 257.5 10.7
1/21/2018 1,040 1.4 0 29,450 251 18 2 3,272 0.3 0.2 253.8 10.6
1/22/2018 1,020 1.4 0 28,883 251 18 2 3,216 0.3 0.2 254.3 10.6
1/23/2018 1,060 1.4 0.08 30,016 251 18 2 3,384 0.3 0.2 257.5 10.7
1/24/2018 1,150 1.5 0 32,564 251 18 2 3,887 0.3 0.2 272.6 11.4
1/25/2018 1,330 1.7 0 37,661 251 18 2 4,724 0.3 0.2 286.5 11.9
1/26/2018 1,830 2.1 0 51,820 251 18 2 6,940 0.3 0.2 305.9 12.7
1/27/2018 1,530 1.8 0 43,325 251 18 2 5,684 0.3 0.2 299.7 12.5
1/28/2018 1,280 1.6 1.04 36,246 251 18 2 4,556 0.3 0.2 287.1 12.0
1/29/2018 3,320 2.8 1.04 94,012 251 19 2 11,513 0.3 0.2 279.7 11.7
1/30/2018 7,650 4.5 0.03 216,624 251 21 2 21,913 0.3 0.2 231.1 9.6
1/31/2018 9,060 5.0 0 256,551 251 21 2 24,764 0.4 0.2 220.5 9.2
2/1/2018 6,040 3.9 0 171,034 251 20 2 18,220 0.3 0.2 243.3 10.1
2/2/2018 3,940 3.1 0.18 111,568 251 20 2 13,073 0.3 0.2 267.7 11.2
2/3/2018 2,930 2.6 0 82,968 251 19 2 10,087 0.3 0.2 277.7 11.6
2/4/2018 2,540 2.4 1.12 71,925 251 19 2 8,853 0.3 0.2 281.2 11.7
Page 10 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
2/5/2018 3,960 3.1 0 112,135 251 20 2 13,073 0.3 0.2 266.3 11.1
2/6/2018 6,030 3.9 0 170,751 251 20 2 18,220 0.3 0.2 243.7 10.2
2/7/2018 6,480 4.1 0.08 183,493 251 21 2 19,215 0.3 0.2 239.2 10.0
2/8/2018 4,680 3.4 0.03 132,523 251 20 2 15,016 0.3 0.2 258.8 10.8
2/9/2018 3,650 3.0 0 103,356 251 19 2 12,231 0.3 0.2 270.3 11.3
2/10/2018 3,930 3.1 0.21 111,285 251 20 2 13,013 0.3 0.2 267.1 11.1
2/11/2018 3,930 3.1 0 111,285 251 20 2 13,073 0.3 0.2 268.3 11.2
2/12/2018 3,410 2.9 0.01 96,560 251 19 2 11,572 0.3 0.2 273.8 11.4
2/13/2018 3,870 3.1 0 109,586 251 19 2 12,832 0.3 0.2 267.5 11.1
2/14/2018 4,820 3.5 0 136,487 251 20 2 15,383 0.3 0.2 257.5 10.7
2/15/2018 4,280 3.3 0 121,196 251 20 2 14,042 0.3 0.2 264.7 11.0
2/16/2018 4,030 3.1 0 114,117 251 20 2 13,315 0.3 0.2 266.5 11.1
2/17/2018 3,840 3.1 0 108,737 251 19 2 12,832 0.3 0.2 269.6 11.2
2/18/2018 3,610 3.0 0 102,224 251 19 2 12,171 0.3 0.2 272.0 11.3
2/19/2018 3,330 2.8 0.04 94,295 251 19 2 11,333 0.3 0.2 274.5 11.4
2/20/2018 3,260 2.8 0.01 92,313 251 19 2 11,155 0.3 0.2 276.0 11.5
2/21/2018 3,200 2.8 0 90,614 251 19 2 10,976 0.3 0.2 276.7 11.5
2/22/2018 3,100 2.7 0 87,782 251 19 2 10,679 0.3 0.2 277.9 11.6
2/23/2018 2,840 2.6 0 80,420 251 19 2 9,792 0.3 0.2 278.1 11.6
2/24/2018 2,080 2.1 0 58,899 251 19 2 7,170 0.3 0.2 278.1 11.6
2/25/2018 1,930 2.0 0 54,652 251 18 2 6,596 0.3 0.2 275.7 11.5
2/26/2018 1,810 1.9 0.22 51,253 251 18 2 6,139 0.3 0.2 273.6 11.4
2/27/2018 1,780 1.9 0.01 50,404 251 18 2 5,968 0.3 0.2 270.4 11.3
2/28/2018 1,730 1.9 0.07 48,988 251 18 2 5,797 0.3 0.2 270.3 11.3
3/1/2018 1,830 1.9 0.9 51,820 251 18 2 6,196 0.3 0.2 273.1 11.4
3/2/2018 2,760 2.5 0 78,154 251 19 2 9,557 0.3 0.2 279.3 11.6
3/3/2018 3,570 2.9 0 101,091 251 19 2 12,051 0.3 0.2 272.3 11.3
3/4/2018 4,610 3.4 0 130,541 251 20 2 14,894 0.3 0.2 260.6 10.9
3/5/2018 4,180 3.2 0 118,364 251 20 2 13,739 0.3 0.2 265.1 11.0
3/6/2018 3,450 2.9 0.26 97,693 251 19 2 11,692 0.3 0.2 273.4 11.4
3/7/2018 2,810 2.5 0.02 79,570 251 19 2 9,733 0.3 0.2 279.4 11.6
3/8/2018 2,440 2.3 0 69,093 251 19 2 8,503 0.3 0.2 281.1 11.7
3/9/2018 2,680 2.5 0 75,889 251 19 2 9,263 0.3 0.2 278.8 11.6
3/10/2018 3,070 2.7 0 86,933 251 19 2 10,561 0.3 0.2 277.5 11.6
3/11/2018 2,710 2.5 0.02 76,739 251 19 2 9,380 0.3 0.2 279.2 11.6
3/12/2018 2,540 2.4 0.63 71,925 251 19 2 8,794 0.3 0.2 279.3 11.6
3/13/2018 4,120 3.2 0.01 116,665 251 20 2 13,375 0.3 0.2 261.9 10.9
3/14/2018 7,530 4.5 0 213,226 251 21 2 21,535 0.3 0.2 230.7 9.6
3/15/2018 7,930 4.6 0 224,553 251 21 2 22,418 0.4 0.2 228.0 9.5
3/16/2018 7,540 4.5 0 213,509 251 21 2 21,535 0.4 0.2 230.4 9.6
Page 11 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
3/17/2018 6,180 4.0 0 174,998 251 20 2 18,530 0.3 0.2 241.9 10.1
3/18/2018 5,000 3.6 0 141,584 251 20 2 15,812 0.3 0.2 255.1 10.6
3/19/2018 4,480 3.3 0.01 126,859 251 20 2 14,528 0.3 0.2 261.6 10.9
3/20/2018 4,650 3.4 0.57 131,673 251 20 2 14,955 0.3 0.2 259.4 10.8
3/21/2018 7,350 4.4 0.1 208,129 251 21 2 21,094 0.3 0.2 231.5 9.6
3/22/2018 10,900 5.6 0 308,654 251 22 2 28,540 0.4 0.3 211.2 8.8
3/23/2018 11,000 5.6 0 311,485 251 22 2 28,797 0.4 0.3 211.2 8.8
3/24/2018 8,390 4.8 0.43 237,578 251 21 2 23,304 0.4 0.2 224.1 9.3
3/25/2018 6,990 4.3 0.21 197,935 251 21 2 20,341 0.3 0.2 234.7 9.8
3/26/2018 7,550 4.5 0 213,792 251 21 2 21,598 0.3 0.2 230.8 9.6
3/27/2018 7,950 4.6 0.01 225,119 251 21 2 22,418 0.4 0.2 227.5 9.5
3/28/2018 7,540 4.5 0 213,509 251 21 2 21,535 0.4 0.2 230.4 9.6
3/29/2018 7,250 4.4 0 205,297 251 21 2 20,906 0.3 0.2 232.6 9.7
3/30/2018 6,730 4.2 0 190,572 251 21 2 19,778 0.3 0.2 237.1 9.9
3/31/2018 5,530 3.8 0 156,592 251 20 2 17,043 0.3 0.2 248.6 10.4
4/1/2018 3,900 3.1 0 110,436 251 20 2 12,953 0.3 0.2 267.9 11.2
4/2/2018 3,440 2.9 0 97,410 251 19 2 11,692 0.3 0.2 274.2 11.4
4/3/2018 2,880 2.6 0 81,553 251 19 2 9,969 0.3 0.2 279.2 11.6
4/4/2018 2,360 2.3 0 66,828 251 19 2 8,211 0.3 0.2 280.7 11.7
4/5/2018 2,200 2.2 0 62,297 251 19 2 7,574 0.3 0.2 277.7 11.6
4/6/2018 1,990 2.0 0 56,351 251 18 2 6,825 0.3 0.2 276.7 11.5
4/7/2018 1,940 2.0 0.68 54,935 251 18 2 6,653 0.3 0.2 276.6 11.5
4/8/2018 2,440 2.3 0.25 69,093 251 19 2 8,444 0.3 0.2 279.2 11.6
4/9/2018 3,280 2.8 0.04 92,879 251 19 2 11,214 0.3 0.2 275.8 11.5
4/10/2018 4,250 3.2 0 120,347 251 20 2 13,860 0.3 0.2 263.1 11.0
4/11/2018 5,210 3.6 0 147,531 251 20 2 16,365 0.3 0.2 253.4 10.6
4/12/2018 4,640 3.4 0 131,390 251 20 2 14,955 0.3 0.2 260.0 10.8
4/13/2018 3,450 2.9 0 97,693 251 19 2 11,632 0.3 0.2 272.0 11.3
4/14/2018 2,260 2.2 0 63,996 251 19 2 7,805 0.3 0.2 278.6 11.6
4/15/2018 2,000 2.0 1.06 56,634 251 18 2 6,825 0.3 0.2 275.3 11.5
4/16/2018 5,330 3.5 0 150,929 251 20 2 15,322 0.3 0.2 231.9 9.7
4/17/2018 15,300 7.7 0 433,248 251 24 2 42,120 0.4 0.2 222.1 9.3
4/18/2018 13,900 7.7 0 393,604 251 24 2 42,316 0.3 0.2 245.6 10.2
4/19/2018 13,100 7.4 0 370,951 251 24 2 40,355 0.3 0.2 248.5 10.4
4/20/2018 11,800 6.2 0 334,139 251 23 2 32,608 0.4 0.2 222.9 9.3
4/21/2018 9,910 5.3 0 280,620 251 22 2 26,488 0.4 0.3 215.6 9.0
4/22/2018 8,180 4.7 0 231,632 251 21 2 22,924 0.4 0.2 226.1 9.4
4/23/2018 7,570 4.5 0.23 214,359 251 21 2 21,598 0.4 0.2 230.1 9.6
4/24/2018 6,600 4.1 1.18 186,891 251 21 2 19,465 0.3 0.2 237.9 9.9
4/25/2018 7,670 4.5 0 217,190 251 21 2 21,724 0.4 0.2 228.5 9.5
Page 12 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
4/26/2018 14,600 7.3 0 413,426 251 24 2 39,441 0.4 0.3 217.9 9.1
4/27/2018 13,700 7.8 0.13 387,941 251 24 2 42,839 0.3 0.2 252.2 10.5
4/28/2018 12,000 6.3 0 339,802 251 23 2 33,191 0.4 0.2 223.1 9.3
4/29/2018 12,000 5.9 0 339,802 251 22 2 30,538 0.4 0.3 205.3 8.6
4/30/2018 9,520 5.1 0 269,576 251 22 2 25,721 0.4 0.3 217.9 9.1
5/1/2018 8,010 4.6 0 226,818 251 21 2 22,544 0.4 0.2 227.0 9.5
5/2/2018 7,290 4.4 0 206,430 251 21 2 21,031 0.3 0.2 232.7 9.7
5/3/2018 6,830 4.2 0 193,404 251 21 2 19,965 0.3 0.2 235.8 9.8
5/4/2018 6,690 4.2 0 189,440 251 21 2 19,653 0.3 0.2 237.0 9.9
5/5/2018 5,470 3.7 0 154,893 251 20 2 16,920 0.3 0.2 249.5 10.4
5/6/2018 4,220 3.2 0.04 119,497 251 20 2 13,860 0.3 0.2 264.9 11.0
5/7/2018 4,000 3.1 0 113,267 251 20 2 13,255 0.3 0.2 267.3 11.1
5/8/2018 3,560 2.9 0 100,808 251 19 2 11,991 0.3 0.2 271.7 11.3
5/9/2018 2,730 2.5 0 77,305 251 19 2 9,439 0.3 0.2 278.9 11.6
5/10/2018 2,130 2.1 0.08 60,315 251 19 2 7,343 0.3 0.2 278.1 11.6
5/11/2018 1,850 1.9 0 52,386 251 18 2 6,253 0.3 0.2 272.6 11.4
5/12/2018 1,420 1.6 0 40,210 251 18 2 4,444 0.3 0.2 252.5 10.5
5/13/2018 1,350 1.6 0 38,228 251 18 2 4,109 0.3 0.2 245.5 10.2
5/14/2018 1,290 1.5 0 36,529 251 18 2 3,831 0.3 0.2 239.6 10.0
5/15/2018 1,280 1.5 0 36,246 251 18 2 3,831 0.3 0.2 241.4 10.1
5/16/2018 1,280 1.5 0.25 36,246 251 18 2 3,831 0.3 0.2 241.4 10.1
5/17/2018 1,490 1.7 0.8 42,192 251 18 2 4,780 0.3 0.2 258.8 10.8
5/18/2018 2,030 2.1 0.01 57,483 251 18 2 6,940 0.3 0.2 275.8 11.5
5/19/2018 2,930 2.6 0.23 82,968 251 19 2 10,087 0.3 0.2 277.7 11.6
5/20/2018 4,260 3.2 0 120,630 251 20 2 13,799 0.3 0.2 261.3 10.9
5/21/2018 7,970 4.6 0 225,685 251 21 2 22,481 0.4 0.2 227.5 9.5
5/22/2018 7,440 4.4 0 210,677 251 21 2 21,346 0.3 0.2 231.4 9.6
5/23/2018 7,830 4.6 0.07 221,721 251 21 2 22,165 0.4 0.2 228.4 9.5
5/24/2018 8,620 4.8 1.86 244,091 251 21 2 23,874 0.4 0.2 223.4 9.3
5/25/2018 7,540 4.5 0 213,509 251 21 2 21,661 0.3 0.2 231.7 9.7
5/26/2018 5,430 3.7 0.02 153,760 251 20 2 16,981 0.3 0.2 252.3 10.5
5/27/2018 3,330 2.9 0 94,295 251 19 2 11,632 0.3 0.2 281.8 11.7
5/28/2018 2,520 2.4 0.58 71,358 251 19 2 9,146 0.3 0.2 292.8 12.2
5/29/2018 2,910 2.7 0.13 82,402 251 19 2 10,501 0.3 0.2 291.1 12.1
5/30/2018 4,410 3.4 0 124,877 251 20 2 14,955 0.3 0.2 273.6 11.4
5/31/2018 6,070 4.1 0 171,883 251 20 2 18,966 0.3 0.2 252.0 10.5
6/1/2018 7,590 4.6 0 214,925 251 21 2 22,481 0.3 0.2 238.9 10.0
6/2/2018 5,750 4.0 0 162,822 251 20 2 18,406 0.3 0.2 258.2 10.8
6/3/2018 4,240 3.4 0 120,063 251 20 2 14,650 0.3 0.2 278.7 11.6
6/4/2018 2,970 2.8 0 84,101 251 19 2 10,976 0.3 0.2 298.1 12.4
Page 13 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
6/5/2018 2,290 2.4 0 64,846 251 19 2 8,678 0.3 0.2 305.7 12.7
6/6/2018 1,800 2.0 0 50,970 251 18 2 6,825 0.3 0.2 305.9 12.7
6/7/2018 1,510 1.8 0 42,758 251 18 2 5,627 0.3 0.2 300.6 12.5
6/8/2018 1,270 1.6 0 35,962 251 18 2 4,444 0.3 0.2 282.3 11.8
6/9/2018 1,140 1.5 0.02 32,281 251 18 2 3,831 0.3 0.2 271.1 11.3
6/10/2018 1,040 1.4 0 29,450 251 18 2 3,272 0.3 0.2 253.8 10.6
6/11/2018 1,060 1.4 1.81 30,016 251 18 2 3,384 0.3 0.2 257.5 10.7
6/12/2018 1,770 2.0 0.73 50,121 251 18 2 6,653 0.3 0.2 303.2 12.6
6/13/2018 2,000 2.2 0 56,634 251 19 2 7,574 0.3 0.2 305.5 12.7
6/14/2018 1,510 1.8 0 42,758 251 18 2 5,570 0.3 0.2 297.6 12.4
6/15/2018 1,270 1.6 0 35,962 251 18 2 4,500 0.3 0.2 285.8 11.9
6/16/2018 1,130 1.5 0 31,998 251 18 2 3,775 0.3 0.2 269.5 11.2
6/17/2018 1,040 1.4 0 29,450 251 18 2 3,328 0.3 0.2 258.1 10.8
6/18/2018 971 1.4 0.35 27,496 251 18 2 2,933 0.3 0.2 243.7 10.2
6/19/2018 941 1.3 0 26,646 251 18 2 2,763 0.3 0.2 236.9 9.9
6/20/2018 907 1.3 0 25,683 251 18 2 2,536 0.4 0.2 225.5 9.4
6/21/2018 999 1.4 0 28,289 251 18 2 3,047 0.3 0.2 246.0 10.2
6/22/2018 1,060 1.4 0 30,016 251 18 2 3,440 0.3 0.2 261.8 10.9
6/23/2018 1,020 1.4 0 28,883 251 18 2 3,159 0.3 0.2 249.9 10.4
6/24/2018 940 1.3 0.07 26,618 251 18 2 2,763 0.3 0.2 237.1 9.9
6/25/2018 1,040 1.4 0.45 29,450 251 18 2 3,272 0.3 0.2 253.8 10.6
6/26/2018 1,340 1.7 0.76 37,945 251 18 2 4,780 0.3 0.2 287.8 12.0
6/27/2018 2,170 2.3 0.01 61,448 251 19 2 8,270 0.3 0.2 307.4 12.8
6/28/2018 1,990 2.2 0 56,351 251 19 2 7,574 0.3 0.2 307.0 12.8
6/29/2018 1,650 1.9 0 46,723 251 18 2 6,196 0.3 0.2 302.9 12.6
6/30/2018 1,390 1.7 0 39,360 251 18 2 5,062 0.3 0.2 293.8 12.2
7/1/2018 1,230 1.6 0 34,830 251 18 2 4,276 0.3 0.2 280.5 11.7
7/2/2018 1,090 1.5 0 30,865 251 18 2 3,552 0.3 0.2 262.9 11.0
7/3/2018 965 1.3 0 27,326 251 18 2 2,877 0.3 0.2 240.5 10.0
7/4/2018 881 1.3 0 24,947 251 18 2 2,364 0.4 0.3 216.5 9.0
7/5/2018 857 1.2 0.38 24,268 251 18 2 2,250 0.4 0.3 211.7 8.8
7/6/2018 931 1.3 0.01 26,363 251 18 2 2,707 0.3 0.2 234.5 9.8
7/7/2018 1,120 1.5 0.16 31,715 251 18 2 3,664 0.3 0.2 263.9 11.0
7/8/2018 1,670 2.0 0 47,289 251 18 2 6,310 0.3 0.2 304.8 12.7
7/9/2018 1,700 2.0 0 48,139 251 18 2 6,424 0.3 0.2 304.8 12.7
7/10/2018 1,570 1.9 0 44,457 251 18 2 5,854 0.3 0.2 300.8 12.5
7/11/2018 1,190 1.6 0 33,697 251 18 2 4,053 0.3 0.2 274.8 11.4
7/12/2018 998 1.4 0.12 28,260 251 18 2 3,047 0.3 0.2 246.2 10.3
7/13/2018 957 1.3 0 27,099 251 18 2 2,820 0.3 0.2 237.7 9.9
7/14/2018 851 1.2 0 24,098 251 18 2 2,192 0.4 0.3 207.8 8.7
Page 14 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
7/15/2018 799 1.2 0 22,625 251 18 2 1,846 0.4 0.3 186.4 7.8
7/16/2018 811 1.2 0 22,965 251 18 2 1,962 0.4 0.3 195.1 8.1
7/17/2018 802 1.2 0.07 22,710 251 18 2 1,904 0.4 0.3 191.5 8.0
7/18/2018 1,670 1.9 0 47,289 251 18 2 6,025 0.3 0.2 291.0 12.1
7/19/2018 1,700 2.0 0 48,139 251 18 2 6,367 0.3 0.2 302.1 12.6
7/20/2018 1,100 1.5 0.01 31,149 251 18 2 3,608 0.3 0.2 264.6 11.0
7/21/2018 893 1.3 0.01 25,287 251 18 2 2,479 0.4 0.2 223.9 9.3
7/22/2018 1,400 1.7 0.01 39,644 251 18 2 4,837 0.3 0.2 278.7 11.6
7/23/2018 3,880 3.2 0 109,869 251 20 2 13,436 0.3 0.2 279.3 11.6
7/24/2018 6,730 4.3 0.02 190,572 251 21 2 20,592 0.3 0.2 246.8 10.3
7/25/2018 4,670 3.5 0.09 132,240 251 20 2 15,751 0.3 0.2 272.1 11.3
7/26/2018 3,900 3.2 0 110,436 251 20 2 13,739 0.3 0.2 284.2 11.8
7/27/2018 3,040 2.8 0 86,083 251 19 2 11,214 0.3 0.2 297.6 12.4
7/28/2018 2,720 2.6 1.96 77,022 251 19 2 10,205 0.3 0.2 302.7 12.6
7/29/2018 3,270 2.9 0.06 92,596 251 19 2 11,931 0.3 0.2 294.3 12.3
7/30/2018 3,520 3.0 0.78 99,675 251 19 2 12,652 0.3 0.2 289.9 12.1
7/31/2018 4,160 3.3 0.19 117,798 251 20 2 14,468 0.3 0.2 280.5 11.7
8/1/2018 3,820 3.2 0.43 108,170 251 20 2 13,557 0.3 0.2 286.3 11.9
8/2/2018 3,720 3.1 0.66 105,339 251 20 2 13,255 0.3 0.2 287.4 12.0
8/3/2018 3,510 3.0 0.46 99,392 251 19 2 12,652 0.3 0.2 290.8 12.1
8/4/2018 8,470 4.9 0.59 239,844 251 21 2 24,192 0.4 0.2 230.4 9.6
8/5/2018 9,730 5.3 0.08 275,523 251 22 2 26,872 0.4 0.2 222.8 9.3
8/6/2018 8,560 4.9 0.01 242,392 251 21 2 24,510 0.3 0.2 231.0 9.6
8/7/2018 8,030 4.8 0 227,384 251 21 2 23,430 0.3 0.2 235.4 9.8
8/8/2018 7,660 4.6 0.11 216,907 251 21 2 22,607 0.3 0.2 238.1 9.9
8/9/2018 8,590 4.9 0 243,242 251 21 2 24,510 0.4 0.2 230.2 9.6
8/10/2018 9,930 5.4 0.12 281,186 251 22 2 27,192 0.4 0.2 220.9 9.2
8/11/2018 6,660 4.3 0.01 188,590 251 21 2 20,466 0.3 0.2 247.9 10.3
8/12/2018 7,350 4.5 0.73 208,129 251 21 2 21,913 0.3 0.2 240.5 10.0
8/13/2018 10,500 5.5 0.43 297,327 251 22 2 28,283 0.4 0.3 217.3 9.1
8/14/2018 12,400 6.1 0 351,129 251 23 2 32,025 0.4 0.3 208.3 8.7
8/15/2018 12,700 6.6 0 359,624 251 23 2 35,270 0.4 0.2 224.0 9.3
8/16/2018 11,600 6.0 0 328,475 251 22 2 31,119 0.4 0.3 216.4 9.0
8/17/2018 9,160 5.1 0.27 259,382 251 22 2 25,721 0.4 0.2 226.5 9.4
8/18/2018 6,580 4.3 0.16 186,325 251 21 2 20,216 0.3 0.2 247.8 10.3
8/19/2018 5,850 4.0 0.17 165,654 251 20 2 18,468 0.3 0.2 254.7 10.6
8/20/2018 11,600 5.9 0.55 328,475 251 22 2 30,473 0.4 0.3 211.9 8.8
8/21/2018 14,000 7.0 0.01 396,436 251 23 2 37,549 0.4 0.3 216.4 9.0
8/22/2018 14,300 8.1 0 404,931 251 24 2 44,670 0.3 0.2 252.0 10.5
8/23/2018 11,700 6.3 0 331,307 251 23 2 33,256 0.4 0.2 229.3 9.6
Page 15 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
8/24/2018 10,900 5.7 0 308,654 251 22 2 29,119 0.4 0.3 215.5 9.0
8/25/2018 7,430 4.6 0 210,394 251 21 2 22,039 0.3 0.2 239.3 10.0
8/26/2018 4,220 3.4 0 119,497 251 20 2 14,589 0.3 0.2 278.9 11.6
8/27/2018 3,160 2.9 0 89,481 251 19 2 11,572 0.3 0.2 295.4 12.3
8/28/2018 2,070 2.2 0 58,616 251 19 2 7,863 0.3 0.2 306.4 12.8
8/29/2018 1,600 1.9 0 45,307 251 18 2 5,968 0.3 0.2 300.9 12.5
8/30/2018 1,440 1.8 0 40,776 251 18 2 5,231 0.3 0.2 293.0 12.2
8/31/2018 1,360 1.7 0 38,511 251 18 2 4,893 0.3 0.2 290.2 12.1
9/1/2018 1,350 1.7 38,228 251 18 2 4,893 0.3 0.2 292.4 12.2
9/2/2018 1,580 1.9 44,741 251 18 2 5,911 0.3 0.2 301.8 12.6
9/3/2018 1,770 2.0 50,121 251 18 2 6,653 0.3 0.2 303.2 12.6
9/4/2018 1,830 2.1 51,820 251 18 2 6,940 0.3 0.2 305.9 12.7
9/5/2018 1,670 1.9 47,289 251 18 2 6,253 0.3 0.2 302.0 12.6
9/6/2018 1,430 1.8 40,493 251 18 2 5,231 0.3 0.2 295.1 12.3
9/7/2018 1,300 1.7 36,812 251 18 2 4,612 0.3 0.2 286.2 11.9
9/8/2018 1,230 1.6 34,830 251 18 2 4,276 0.3 0.2 280.5 11.7
9/9/2018 1,320 1.7 37,378 251 18 2 4,724 0.3 0.2 288.7 12.0
9/10/2018 1,390 1.7 39,360 251 18 2 5,062 0.3 0.2 293.8 12.2
9/11/2018 1,580 1.9 44,741 251 18 2 5,911 0.3 0.2 301.8 12.6
9/12/2018 2,390 2.4 67,677 251 19 2 9,028 0.3 0.2 304.7 12.7
9/13/2018 2,880 2.7 81,553 251 19 2 10,738 0.3 0.2 300.8 12.5
9/14/2018 3,450 3.0 97,693 251 19 2 12,411 0.3 0.2 290.2 12.1
9/15/2018 14,200 8.0 402,099 251 24 2 44,343 0.3 0.2 251.9 10.5
9/16/2018 35,400 21.2 1,002,416 251 38 2 123,534 0.3 0.2 281.5 11.7
9/17/2018 60,500 31.0 1,713,169 251 47 2 164,735 0.4 0.3 219.6 9.2
9/18/2018 77,500 36.0 2,194,556 251 52 2 178,236 0.4 0.3 185.5 7.7
9/19/2018 83,200 38.3 2,355,962 251 55 2 182,750 0.5 0.3 177.2 7.4
9/20/2018 79,100 38.4 2,239,863 251 55 2 182,938 0.4 0.3 186.6 7.8
9/21/2018 64,200 36.4 0 1,817,942 251 53 2 179,125 0.4 0.2 225.1 9.4
9/22/2018 38,500 31.2 0 1,090,199 251 48 2 165,282 0.2 0.2 346.3 14.4
9/23/2018 17,000 23.3 0 481,386 251 40 2 133,677 0.1 0.1 634.3 26.4
9/24/2018 8,520 15.2 0 241,260 251 32 2 89,797 0.1 0.1 850.2 35.4
9/25/2018 9,940 9.3 0 281,469 251 26 2 53,034 0.2 0.1 430.4 17.9
9/26/2018 8,740 6.4 0.35 247,489 251 23 2 33,645 0.3 0.2 310.5 12.9
9/27/2018 10,500 5.7 0.13 297,327 251 22 2 29,634 0.4 0.2 227.7 9.5
9/28/2018 12,300 7.0 0.28 348,297 251 23 2 37,679 0.3 0.2 247.1 10.3
9/29/2018 15,000 8.8 0 424,753 251 25 2 49,444 0.3 0.2 265.9 11.1
9/30/2018 15,300 9.2 0 433,248 251 26 2 52,186 0.3 0.2 275.1 11.5
10/1/2018 14,300 8.6 0 404,931 251 25 2 48,006 0.3 0.2 270.8 11.3
10/2/2018 13,100 7.8 0 370,951 251 24 2 43,166 0.3 0.2 265.8 11.1
Page 16 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
10/3/2018 12,100 7.2 0 342,634 251 24 2 38,919 0.3 0.2 259.5 10.8
10/4/2018 11,400 6.7 0 322,812 251 23 2 35,855 0.3 0.2 253.7 10.6
10/5/2018 11,500 6.4 0 325,644 251 23 2 33,840 0.3 0.2 237.4 9.9
10/6/2018 11,900 6.1 0 336,970 251 23 2 31,830 0.4 0.3 215.8 9.0
10/7/2018 11,500 5.8 0 325,644 251 22 2 30,215 0.4 0.3 211.9 8.8
10/8/2018 11,100 5.7 0 314,317 251 22 2 29,506 0.4 0.3 214.4 8.9
10/9/2018 10,800 5.6 0 305,822 251 22 2 28,862 0.4 0.3 215.6 9.0
10/10/2018 6,320 4.1 0.07 178,962 251 21 2 19,340 0.3 0.2 246.9 10.3
10/11/2018 2,820 2.7 0.67 79,854 251 19 2 10,501 0.3 0.2 300.4 12.5
10/12/2018 8,900 4.9 0 252,020 251 21 2 24,319 0.4 0.2 220.4 9.2
10/13/2018 16,200 9.1 0 458,733 251 26 2 51,729 0.3 0.2 257.6 10.7
10/14/2018 16,200 9.7 0 458,733 251 26 2 55,184 0.3 0.2 274.8 11.4
10/15/2018 12,500 7.8 0 353,961 251 24 2 42,970 0.3 0.2 277.3 11.6
10/16/2018 11,400 6.0 0.24 322,812 251 22 2 31,313 0.4 0.2 221.6 9.2
10/17/2018 12,300 6.8 0.03 348,297 251 23 2 36,246 0.3 0.2 237.7 9.9
10/18/2018 12,400 7.2 0 351,129 251 24 2 39,180 0.3 0.2 254.9 10.6
10/19/2018 11,900 7.0 0 336,970 251 23 2 37,810 0.3 0.2 256.3 10.7
10/20/2018 11,200 6.5 0 317,149 251 23 2 34,749 0.3 0.2 250.3 10.4
10/21/2018 11,700 6.0 0 331,307 251 22 2 31,378 0.4 0.3 216.3 9.0
10/22/2018 11,400 5.8 0 322,812 251 22 2 30,086 0.4 0.3 212.9 8.9
10/23/2018 10,300 5.5 0 291,664 251 22 2 28,026 0.4 0.3 219.5 9.1
10/24/2018 8,600 5.0 0 243,525 251 21 2 24,573 0.3 0.2 230.5 9.6
10/25/2018 7,530 4.6 0 213,226 251 21 2 22,355 0.3 0.2 239.5 10.0
10/26/2018 6,910 4.4 1.05 195,669 251 21 2 20,969 0.3 0.2 244.8 10.2
10/27/2018 9,040 5.1 0.02 255,984 251 22 2 25,402 0.4 0.2 226.7 9.4
10/28/2018 14,800 7.8 0 419,089 251 24 2 43,100 0.3 0.2 234.9 9.8
10/29/2018 14,600 8.6 0 413,426 251 25 2 48,136 0.3 0.2 266.0 11.1
10/30/2018 11,500 6.9 0 325,644 251 23 2 37,223 0.3 0.2 261.1 10.9
10/31/2018 10,300 5.6 0 291,664 251 22 2 28,476 0.4 0.2 223.0 9.3
11/1/2018 8,640 5.0 0.11 244,658 251 21 2 24,701 0.3 0.2 230.6 9.6
11/2/2018 6,460 4.2 0.04 182,927 251 21 2 19,965 0.3 0.2 249.3 10.4
11/3/2018 4,960 3.7 0 140,452 251 20 2 16,488 0.3 0.2 268.2 11.2
11/4/2018 6,150 4.1 0.08 174,149 251 21 2 19,340 0.3 0.2 253.7 10.6
11/5/2018 5,970 4.1 0.18 169,052 251 20 2 18,904 0.3 0.2 255.4 10.6
11/6/2018 7,320 4.5 0.04 207,279 251 21 2 21,787 0.3 0.2 240.1 10.0
11/7/2018 12,500 6.2 0.05 353,961 251 23 2 32,478 0.4 0.3 209.6 8.7
11/8/2018 10,400 5.5 0.3 294,495 251 22 2 28,219 0.4 0.3 218.9 9.1
11/9/2018 8,940 5.1 0.04 253,153 251 21 2 25,274 0.4 0.2 228.1 9.5
11/10/2018 9,150 5.1 0.01 259,099 251 22 2 25,721 0.4 0.2 226.8 9.4
11/11/2018 8,660 5.0 0 245,224 251 21 2 24,701 0.4 0.2 230.1 9.6
Page 17 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
11/12/2018 8,920 5.1 1.5 252,586 251 21 2 25,274 0.4 0.2 228.6 9.5
11/13/2018 19,600 10.4 1.57 555,010 251 27 2 59,859 0.3 0.2 246.4 10.3
11/14/2018 37,400 21.6 0.07 1,059,050 251 38 2 125,662 0.3 0.2 271.0 11.3
11/15/2018 36,400 23.7 0.64 1,030,733 251 40 2 135,558 0.3 0.2 300.4 12.5
11/16/2018 39,200 25.0 0 1,110,020 251 41 2 141,602 0.3 0.2 291.4 12.1
11/17/2018 35,300 24.7 0 999,585 251 41 2 140,223 0.3 0.2 320.4 13.4
11/18/2018 27,100 21.7 0 767,387 251 38 2 125,863 0.2 0.1 374.6 15.6
11/19/2018 18,200 16.9 0.11 515,367 251 33 2 100,017 0.2 0.1 443.3 18.5
11/20/2018 15,900 12.0 0 450,238 251 28 2 70,262 0.2 0.2 356.5 14.9
11/21/2018 16,700 10.6 0 472,891 251 27 2 61,541 0.3 0.2 297.3 12.4
11/22/2018 15,100 9.4 0 427,584 251 26 2 53,686 0.3 0.2 286.8 12.0
11/23/2018 11,500 7.1 0 325,644 251 24 2 38,592 0.3 0.2 270.7 11.3
11/24/2018 11,500 6.2 1.09 325,644 251 23 2 32,672 0.4 0.2 229.2 9.5
11/25/2018 13,200 7.3 0 373,782 251 24 2 40,029 0.3 0.2 244.6 10.2
11/26/2018 14,800 8.6 0 419,089 251 25 2 48,071 0.3 0.2 262.0 10.9
11/27/2018 15,400 9.1 0 436,079 251 26 2 51,403 0.3 0.2 269.3 11.2
11/28/2018 15,300 9.1 0 433,248 251 26 2 51,599 0.3 0.2 272.0 11.3
11/29/2018 15,100 9.0 0 427,584 251 25 2 50,554 0.3 0.2 270.1 11.3
11/30/2018 15,500 9.2 0 438,911 251 26 2 52,447 0.3 0.2 273.0 11.4
12/1/2018 15,700 9.4 1.11 444,574 251 26 2 53,425 0.3 0.2 274.5 11.4
12/2/2018 17,300 10.4 0.01 489,881 251 27 2 59,989 0.3 0.2 279.7 11.7
12/3/2018 18,700 11.7 0 529,525 251 28 2 68,158 0.3 0.2 294.0 12.3
12/4/2018 18,900 12.0 0 535,188 251 28 2 70,325 0.3 0.2 300.2 12.5
12/5/2018 18,100 11.5 0 512,535 251 28 2 67,199 0.3 0.2 299.5 12.5
12/6/2018 17,200 10.7 0 487,050 251 27 2 62,057 0.3 0.2 291.0 12.1
12/7/2018 13,600 8.6 0 385,109 251 25 2 48,267 0.3 0.2 286.3 11.9
12/8/2018 9,960 5.7 0.39 282,036 251 22 2 29,506 0.3 0.2 239.0 10.0
12/9/2018 10,400 5.4 1.56 294,495 251 22 2 27,641 0.4 0.3 214.4 8.9
12/10/2018 17,000 9.4 0.35 481,386 251 26 2 53,230 0.3 0.2 252.6 10.5
12/11/2018 23,300 15.0 0.02 659,783 251 31 2 88,892 0.3 0.2 307.8 12.8
12/12/2018 21,500 15.1 0 608,812 251 32 2 89,375 0.2 0.2 335.3 14.0
12/13/2018 17,900 12.6 0 506,872 251 29 2 73,746 0.2 0.2 332.3 13.8
12/14/2018 13,600 8.9 1.49 385,109 251 25 2 50,032 0.3 0.2 296.8 12.4
12/15/2018 15,900 9.6 0.43 450,238 251 26 2 54,533 0.3 0.2 276.7 11.5
12/16/2018 22,000 14.1 0.01 622,971 251 31 2 83,529 0.3 0.2 306.3 12.8
12/17/2018 21,400 14.7 0 605,981 251 31 2 87,014 0.2 0.2 328.0 13.7
12/18/2018 19,200 13.4 0 543,683 251 30 2 78,764 0.2 0.2 330.9 13.8
12/19/2018 16,500 10.9 0 467,228 251 27 2 63,347 0.3 0.2 309.7 12.9
12/20/2018 14,100 8.9 0.39 399,268 251 25 2 50,097 0.3 0.2 286.6 11.9
12/21/2018 12,600 7.6 0.15 356,792 251 24 2 41,662 0.3 0.2 266.7 11.1
Page 18 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
12/22/2018 18,400 10.9 0 521,030 251 27 2 63,476 0.3 0.2 278.3 11.6
12/23/2018 20,400 13.0 0 577,664 251 29 2 76,514 0.3 0.2 302.6 12.6
12/24/2018 19,400 12.8 0 549,347 251 29 2 75,321 0.3 0.2 313.2 13.0
12/25/2018 17,200 11.0 0 487,050 251 27 2 63,862 0.3 0.2 299.5 12.5
12/26/2018 15,600 9.7 0 441,743 251 26 2 55,314 0.3 0.2 286.0 11.9
12/27/2018 15,200 9.2 0.05 430,416 251 26 2 51,925 0.3 0.2 275.6 11.5
12/28/2018 13,900 8.5 0.6 393,604 251 25 2 47,286 0.3 0.2 274.4 11.4
12/29/2018 14,600 8.5 0.01 413,426 251 25 2 47,679 0.3 0.2 263.4 11.0
12/30/2018 20,200 12.4 0.2 572,000 251 29 2 72,482 0.3 0.2 289.5 12.1
12/31/2018 21,200 13.8 0 600,317 251 30 2 81,804 0.3 0.2 311.3 13.0
1/1/2019 20,600 13.8 0.01 583,327 251 30 2 81,433 0.3 0.2 318.9 13.3
1/2/2019 19,800 13.2 0 560,674 251 30 2 78,077 0.3 0.2 318.1 13.3
1/3/2019 19,600 12.9 0.22 555,010 251 29 2 76,137 0.3 0.2 313.4 13.1
1/4/2019 19,900 13.1 0.76 563,505 251 30 2 77,140 0.3 0.2 312.7 13.0
1/5/2019 20,800 13.8 0 588,990 251 30 2 81,309 0.3 0.2 315.3 13.1
1/6/2019 21,700 14.6 0 614,476 251 31 2 86,527 0.3 0.2 321.7 13.4
1/7/2019 20,100 13.9 0 569,169 251 30 2 81,989 0.2 0.2 329.0 13.7
1/8/2019 19,400 12.9 0 549,347 251 29 2 76,137 0.3 0.2 316.6 13.2
1/9/2019 19,300 12.7 0 546,515 251 29 2 74,881 0.3 0.2 313.0 13.0
1/10/2019 18,600 12.1 0 526,693 251 29 2 70,770 0.3 0.2 306.9 12.8
1/11/2019 17,900 11.4 0 506,872 251 28 2 66,431 0.3 0.2 299.4 12.5
1/12/2019 17,300 10.8 0 489,881 251 27 2 62,509 0.3 0.2 291.5 12.1
1/13/2019 17,100 10.5 0.7 484,218 251 27 2 60,765 0.3 0.2 286.6 11.9
1/14/2019 19,400 12.0 0 549,347 251 28 2 70,071 0.3 0.2 291.4 12.1
1/15/2019 20,900 13.5 0 591,822 251 30 2 79,946 0.3 0.2 308.6 12.9
1/16/2019 19,400 12.9 0 549,347 251 29 2 75,698 0.3 0.2 314.8 13.1
1/17/2019 17,300 11.2 0.17 489,881 251 28 2 65,148 0.3 0.2 303.8 12.7
1/18/2019 14,400 9.0 0 407,763 251 25 2 51,077 0.3 0.2 286.1 11.9
1/19/2019 9,790 6.0 0 277,222 251 22 2 31,507 0.3 0.2 259.6 10.8
1/20/2019 7,940 4.7 0.5 224,836 251 21 2 22,671 0.4 0.2 230.3 9.6
1/21/2019 10,200 5.4 0 288,832 251 22 2 27,256 0.4 0.3 215.6 9.0
1/22/2019 11,700 5.8 0 331,307 251 22 2 30,279 0.4 0.3 208.8 8.7
1/23/2019 11,200 5.7 0 317,149 251 22 2 29,248 0.4 0.3 210.7 8.8
1/24/2019 12,500 6.4 0.83 353,961 251 23 2 34,165 0.4 0.2 220.5 9.2
1/25/2019 12,900 7.4 0 365,287 251 24 2 40,355 0.3 0.2 252.4 10.5
1/26/2019 16,100 9.3 0 455,901 251 26 2 53,099 0.3 0.2 266.0 11.1
1/27/2019 16,600 10.1 0 470,060 251 27 2 58,109 0.3 0.2 282.4 11.8
1/28/2019 14,200 8.7 0 402,099 251 25 2 48,659 0.3 0.2 276.4 11.5
1/29/2019 11,900 7.2 0.09 336,970 251 24 2 39,245 0.3 0.2 266.0 11.1
1/30/2019 11,100 6.4 0 314,317 251 23 2 33,645 0.3 0.2 244.5 10.2
Page 19 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
1/31/2019 12,000 6.0 0 339,802 251 22 2 31,442 0.4 0.3 211.4 8.8
2/1/2019 9,470 5.1 0 268,161 251 22 2 25,785 0.4 0.3 219.6 9.2
2/2/2019 6,770 4.2 0 191,705 251 21 2 20,090 0.3 0.2 239.4 10.0
2/3/2019 6,140 4.0 0 173,865 251 20 2 18,717 0.3 0.2 245.9 10.2
2/4/2019 5,800 3.9 0 164,238 251 20 2 17,971 0.3 0.2 249.9 10.4
2/5/2019 5,180 3.7 0 146,681 251 20 2 16,488 0.3 0.2 256.8 10.7
2/6/2019 4,600 3.4 0 130,257 251 20 2 15,077 0.3 0.2 264.4 11.0
2/7/2019 4,390 3.3 0 124,311 251 20 2 14,528 0.3 0.2 267.0 11.1
2/8/2019 4,210 3.3 0 119,214 251 20 2 14,042 0.3 0.2 269.1 11.2
2/9/2019 3,810 3.1 0 107,887 251 20 2 12,953 0.3 0.2 274.2 11.4
2/10/2019 3,570 3.0 0 101,091 251 19 2 12,291 0.3 0.2 277.7 11.6
2/11/2019 3,460 2.9 0.25 97,976 251 19 2 11,931 0.3 0.2 278.2 11.6
2/12/2019 3,700 3.0 0.25 104,772 251 19 2 12,652 0.3 0.2 275.8 11.5
2/13/2019 4,500 3.4 0.02 127,426 251 20 2 14,833 0.3 0.2 265.9 11.1
2/14/2019 5,050 3.6 0 143,000 251 20 2 16,181 0.3 0.2 258.5 10.8
2/15/2019 6,340 4.1 0 179,529 251 21 2 19,153 0.3 0.2 243.7 10.2
2/16/2019 7,770 4.6 0.6 220,022 251 21 2 22,291 0.3 0.2 231.4 9.6
2/17/2019 11,500 5.8 0.04 325,644 251 22 2 29,828 0.4 0.3 209.2 8.7
2/18/2019 12,700 7.0 0.12 359,624 251 23 2 37,875 0.3 0.2 240.6 10.0
2/19/2019 13,200 7.6 0.11 373,782 251 24 2 41,597 0.3 0.2 254.2 10.6
2/20/2019 13,900 8.1 0.19 393,604 251 25 2 45,193 0.3 0.2 262.3 10.9
2/21/2019 15,300 8.9 0.16 433,248 251 25 2 50,228 0.3 0.2 264.8 11.0
2/22/2019 18,500 11.2 0.28 523,862 251 28 2 64,955 0.3 0.2 283.2 11.8
2/23/2019 21,600 13.6 0.46 611,644 251 30 2 80,566 0.3 0.2 300.9 12.5
2/24/2019 23,800 15.9 0.01 673,941 251 32 2 94,099 0.3 0.2 318.9 13.3
2/25/2019 23,600 16.7 0 668,278 251 33 2 98,914 0.2 0.2 338.1 14.1
2/26/2019 21,200 15.5 0 600,317 251 32 2 91,598 0.2 0.2 348.5 14.5
2/27/2019 17,200 12.1 0 487,050 251 29 2 71,151 0.2 0.2 333.7 13.9
2/28/2019 14,700 9.3 0 416,258 251 26 2 52,904 0.3 0.2 290.3 12.1
3/1/2019 14,000 8.5 0.68 396,436 251 25 2 47,482 0.3 0.2 273.6 11.4
3/2/2019 14,800 8.7 0.01 419,089 251 25 2 48,921 0.3 0.2 266.6 11.1
3/3/2019 16,100 9.7 1.04 455,901 251 26 2 55,445 0.3 0.2 277.8 11.6
3/4/2019 15,600 9.4 0.14 441,743 251 26 2 53,425 0.3 0.2 276.3 11.5
3/5/2019 18,400 11.3 0 521,030 251 28 2 65,790 0.3 0.2 288.4 12.0
3/6/2019 16,400 10.3 0 464,396 251 27 2 59,600 0.3 0.2 293.2 12.2
3/7/2019 12,600 7.8 0 356,792 251 24 2 42,970 0.3 0.2 275.1 11.5
3/8/2019 12,800 7.5 0.51 362,456 251 24 2 41,074 0.3 0.2 258.9 10.8
3/9/2019 15,000 8.7 0.07 424,753 251 25 2 49,182 0.3 0.2 264.5 11.0
3/10/2019 16,700 10.0 0 472,891 251 26 2 57,460 0.3 0.2 277.6 11.6
3/11/2019 17,300 10.6 0 489,881 251 27 2 60,959 0.3 0.2 284.2 11.8
Page 20 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
3/12/2019 17,300 10.6 0 489,881 251 27 2 61,411 0.3 0.2 286.3 11.9
3/13/2019 16,800 10.3 0 475,723 251 27 2 59,406 0.3 0.2 285.2 11.9
3/14/2019 16,100 9.8 0 455,901 251 26 2 56,355 0.3 0.2 282.4 11.8
3/15/2019 15,500 9.4 0.7 438,911 251 26 2 53,686 0.3 0.2 279.4 11.6
3/16/2019 15,300 9.2 0 433,248 251 26 2 52,317 0.3 0.2 275.8 11.5
3/17/2019 15,000 9.0 0 424,753 251 25 2 51,011 0.3 0.2 274.3 11.4
3/18/2019 14,800 8.8 0 419,089 251 25 2 49,836 0.3 0.2 271.6 11.3
3/19/2019 14,400 8.6 0 407,763 251 25 2 48,006 0.3 0.2 268.9 11.2
3/20/2019 12,400 7.5 0.19 351,129 251 24 2 41,074 0.3 0.2 267.2 11.1
3/21/2019 10,500 5.8 0.15 297,327 251 22 2 30,279 0.3 0.2 232.6 9.7
3/22/2019 13,000 6.8 0.01 368,119 251 23 2 36,376 0.4 0.2 225.7 9.4
3/23/2019 14,400 8.4 0 407,763 251 25 2 46,698 0.3 0.2 261.6 10.9
3/24/2019 11,300 6.7 0 319,980 251 23 2 36,050 0.3 0.2 257.4 10.7
3/25/2019 10,400 5.4 0.53 294,495 251 22 2 27,705 0.4 0.3 214.9 9.0
3/26/2019 10,700 5.5 0.07 302,990 251 22 2 28,347 0.4 0.3 213.7 8.9
3/27/2019 12,200 6.0 0 345,466 251 22 2 31,184 0.4 0.3 206.2 8.6
3/28/2019 12,400 6.1 0 351,129 251 22 2 31,701 0.4 0.3 206.2 8.6
3/29/2019 11,400 5.8 0 322,812 251 22 2 29,699 0.4 0.3 210.1 8.8
3/30/2019 7,730 4.6 0 218,889 251 21 2 22,039 0.4 0.2 230.0 9.6
3/31/2019 4,330 3.3 0 122,612 251 20 2 14,346 0.3 0.2 267.3 11.1
4/1/2019 3,950 3.2 0 111,852 251 20 2 13,375 0.3 0.2 273.2 11.4
4/2/2019 4,520 3.4 1.02 127,992 251 20 2 14,772 0.3 0.2 263.6 11.0
4/3/2019 6,470 4.1 0 183,210 251 21 2 19,465 0.3 0.2 242.7 10.1
4/4/2019 6,450 4.1 0 182,644 251 21 2 19,403 0.3 0.2 242.7 10.1
4/5/2019 6,020 4.0 1.03 170,467 251 20 2 18,468 0.3 0.2 247.5 10.3
4/6/2019 7,320 4.4 0 207,279 251 21 2 21,283 0.3 0.2 234.5 9.8
4/7/2019 11,200 5.7 0 317,149 251 22 2 29,312 0.4 0.3 211.1 8.8
4/8/2019 9,860 5.3 0 279,204 251 22 2 26,616 0.4 0.3 217.7 9.1
4/9/2019 11,300 5.8 0.03 319,980 251 22 2 30,086 0.4 0.3 214.8 8.9
4/10/2019 18,000 10.4 0 509,703 251 27 2 60,247 0.3 0.2 270.0 11.2
4/11/2019 16,400 10.2 0 464,396 251 27 2 58,693 0.3 0.2 288.7 12.0
4/12/2019 12,300 7.6 1.1 348,297 251 24 2 41,531 0.3 0.2 272.4 11.3
4/13/2019 17,500 10.1 1.18 495,545 251 26 2 57,849 0.3 0.2 266.7 11.1
4/14/2019 24,500 15.8 0.23 693,763 251 32 2 93,743 0.3 0.2 308.7 12.9
4/15/2019 22,900 16.1 0 648,456 251 33 2 95,459 0.2 0.2 336.3 14.0
4/16/2019 21,800 15.5 0 617,307 251 32 2 91,717 0.2 0.2 339.4 14.1
4/17/2019 16,100 11.6 0 455,901 251 28 2 67,903 0.2 0.2 340.2 14.2
4/18/2019 10,500 7.0 0 297,327 251 23 2 37,614 0.3 0.2 289.0 12.0
4/19/2019 8,840 5.1 0.48 250,321 251 21 2 25,274 0.3 0.2 230.6 9.6
4/20/2019 8,550 4.8 0 242,109 251 21 2 23,684 0.4 0.2 223.5 9.3
Page 21 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
4/21/2019 12,500 6.6 0 353,961 251 23 2 35,270 0.4 0.2 227.6 9.5
4/22/2019 11,000 5.7 0 311,485 251 22 2 29,634 0.4 0.3 217.3 9.1
4/23/2019 12,300 6.2 0 348,297 251 23 2 32,737 0.4 0.3 214.7 8.9
4/24/2019 12,700 7.3 0 359,624 251 24 2 39,833 0.3 0.2 253.0 10.5
4/25/2019 12,300 7.2 0 348,297 251 24 2 39,114 0.3 0.2 256.5 10.7
4/26/2019 11,600 6.8 0.05 328,475 251 23 2 36,506 0.3 0.2 253.9 10.6
4/27/2019 11,500 6.5 0 325,644 251 23 2 34,684 0.3 0.2 243.3 10.1
4/28/2019 11,800 6.3 0 334,139 251 23 2 33,450 0.4 0.2 228.7 9.5
4/29/2019 12,200 6.2 0 345,466 251 23 2 32,543 0.4 0.3 215.2 9.0
4/30/2019 12,400 6.1 0 351,129 251 22 2 31,766 0.4 0.3 206.6 8.6
5/1/2019 12,200 5.9 0 345,466 251 22 2 30,925 0.4 0.3 204.5 8.5
5/2/2019 11,900 5.8 0 336,970 251 22 2 30,279 0.4 0.3 205.3 8.6
5/3/2019 11,700 5.8 0 331,307 251 22 2 29,892 0.4 0.3 206.1 8.6
5/4/2019 10,800 5.5 0.16 305,822 251 22 2 27,898 0.4 0.3 208.4 8.7
5/5/2019 10,100 5.3 0.39 286,000 251 22 2 26,552 0.4 0.3 212.1 8.8
5/6/2019 10,700 5.5 0 302,990 251 22 2 27,769 0.4 0.3 209.4 8.7
5/7/2019 11,000 5.5 0 311,485 251 22 2 28,347 0.4 0.3 207.9 8.7
5/8/2019 8,570 4.7 0 242,675 251 21 2 23,240 0.4 0.3 218.8 9.1
5/9/2019 5,530 3.7 0 156,592 251 20 2 16,488 0.3 0.2 240.5 10.0
5/10/2019 3,500 2.8 0 99,109 251 19 2 11,333 0.3 0.2 261.2 10.9
5/11/2019 2,800 2.4 0 79,287 251 19 2 9,146 0.3 0.2 263.5 11.0
5/12/2019 2,700 2.4 0.13 76,455 251 19 2 8,794 0.3 0.2 262.7 10.9
5/13/2019 2,670 2.4 0 75,606 251 19 2 8,678 0.3 0.2 262.2 10.9
5/14/2019 2,860 2.5 0 80,986 251 19 2 9,263 0.3 0.2 261.3 10.9
5/15/2019 2,980 2.5 0 84,384 251 19 2 9,615 0.3 0.2 260.3 10.8
5/16/2019 3,110 2.6 0 88,065 251 19 2 10,028 0.3 0.2 260.1 10.8
5/17/2019 3,150 2.6 0 89,198 251 19 2 10,146 0.3 0.2 259.8 10.8
5/18/2019 2,750 2.4 0 77,871 251 19 2 8,853 0.3 0.2 259.7 10.8
5/19/2019 2,200 2.1 0 62,297 251 18 2 6,997 0.3 0.2 256.6 10.7
5/20/2019 1,980 1.9 0.24 56,067 251 18 2 6,139 0.3 0.2 250.1 10.4
5/21/2019 1,820 1.8 0 51,537 251 18 2 5,570 0.3 0.2 246.9 10.3
5/22/2019 1,640 1.7 0 46,440 251 18 2 4,780 0.3 0.2 235.1 9.8
5/23/2019 1,530 1.6 0 43,325 251 18 2 4,332 0.4 0.2 228.4 9.5
5/24/2019 1,440 1.5 0 40,776 251 18 2 3,942 0.4 0.2 220.8 9.2
5/25/2019 1,370 1.5 0 38,794 251 18 2 3,608 0.4 0.3 212.4 8.9
5/26/2019 1,280 1.4 0 36,246 251 18 2 3,159 0.4 0.3 199.1 8.3
5/27/2019 1,220 1.3 0 34,547 251 18 2 2,877 0.4 0.3 190.2 7.9
5/28/2019 1,180 1.3 0 33,414 251 18 2 2,707 0.4 0.3 185.0 7.7
5/29/2019 1,140 1.3 0 32,281 251 18 2 2,479 0.5 0.3 175.4 7.3
5/30/2019 1,100 1.2 0 31,149 251 18 2 2,250 0.5 0.3 165.0 6.9
Page 22 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
5/31/2019 1,130 1.3 0.1 31,998 251 18 2 2,421 0.5 0.3 172.9 7.2
6/1/2019 1,110 1.2 0 31,432 251 18 2 2,307 0.5 0.3 167.6 7.0
6/2/2019 1,060 1.2 0 30,016 251 18 2 2,020 0.5 0.4 153.7 6.4
6/3/2019 1,000 1.1 0 28,317 251 18 2 1,730 0.6 0.4 139.6 5.8
6/4/2019 959 1.1 0 27,156 251 18 2 1,498 0.6 0.4 126.0 5.3
6/5/2019 967 1.1 0.84 27,382 251 18 2 1,498 0.6 0.4 125.0 5.2
6/6/2019 1,150 1.3 0.01 32,564 251 18 2 2,536 0.5 0.3 177.9 7.4
6/7/2019 1,180 1.3 0 33,414 251 18 2 2,707 0.4 0.3 185.0 7.7
6/8/2019 1,400 1.5 0.01 39,644 251 18 2 3,720 0.4 0.3 214.3 8.9
6/9/2019 2,910 2.5 2.19 82,402 251 19 2 9,322 0.3 0.2 258.4 10.8
6/10/2019 7,470 4.3 0.79 211,527 251 21 2 20,466 0.4 0.2 221.0 9.2
6/11/2019 11,500 5.7 0.06 325,644 251 22 2 29,183 0.4 0.3 204.7 8.5
6/12/2019 11,200 5.6 0.39 317,149 251 22 2 28,476 0.4 0.3 205.1 8.5
6/13/2019 9,290 4.9 0.02 263,064 251 21 2 24,510 0.4 0.3 212.8 8.9
6/14/2019 8,460 4.7 0 239,561 251 21 2 22,797 0.4 0.3 217.4 9.1
6/15/2019 8,400 4.7 0 237,862 251 21 2 22,671 0.4 0.3 217.7 9.1
6/16/2019 8,170 4.6 0 231,349 251 21 2 22,228 0.4 0.3 219.5 9.1
6/17/2019 7,360 4.3 0 208,412 251 21 2 20,466 0.4 0.2 224.3 9.3
6/18/2019 6,800 4.1 0 192,555 251 21 2 19,215 0.4 0.2 227.9 9.5
6/19/2019 5,260 3.5 0 148,947 251 20 2 15,751 0.3 0.2 241.6 10.1
6/20/2019 3,760 2.9 0.08 106,471 251 19 2 11,871 0.3 0.2 254.7 10.6
6/21/2019 3,080 2.6 0 87,216 251 19 2 9,910 0.3 0.2 259.5 10.8
6/22/2019 2,920 2.5 0.23 82,685 251 19 2 9,439 0.3 0.2 260.8 10.9
6/23/2019 2,610 2.3 0 73,907 251 19 2 8,444 0.3 0.2 261.0 10.9
6/24/2019 2,860 2.5 0 80,986 251 19 2 9,204 0.3 0.2 259.6 10.8
6/25/2019 3,500 2.8 0 99,109 251 19 2 11,214 0.3 0.2 258.5 10.8
6/26/2019 3,110 2.6 0 88,065 251 19 2 9,969 0.3 0.2 258.6 10.8
6/27/2019 2,000 1.9 0 56,634 251 18 2 6,196 0.3 0.2 249.9 10.4
6/28/2019 1,460 1.5 0 41,343 251 18 2 3,998 0.4 0.2 220.9 9.2
6/29/2019 1,160 1.3 0 32,848 251 18 2 2,593 0.4 0.3 180.3 7.5
6/30/2019 1,120 1.3 0 31,715 251 18 2 2,364 0.5 0.3 170.3 7.1
7/1/2019 1,080 1.2 0 30,582 251 18 2 2,135 0.5 0.3 159.4 6.6
7/2/2019 1,020 1.2 0.03 28,883 251 18 2 1,846 0.6 0.4 146.0 6.1
7/3/2019 1,040 1.2 0 29,450 251 18 2 1,962 0.5 0.4 152.2 6.3
7/4/2019 1,250 1.3 1.72 35,396 251 18 2 2,877 0.4 0.3 185.6 7.7
7/5/2019 2,430 2.2 0 68,810 251 19 2 7,805 0.3 0.2 259.1 10.8
7/6/2019 2,360 2.2 0 66,828 251 19 2 7,516 0.3 0.2 256.9 10.7
7/7/2019 1,750 1.8 0 49,554 251 18 2 5,231 0.3 0.2 241.1 10.0
7/8/2019 1,830 1.8 0.43 51,820 251 18 2 5,514 0.3 0.2 243.0 10.1
7/9/2019 2,130 2.0 0 60,315 251 18 2 6,710 0.3 0.2 254.1 10.6
Page 23 of 24 August 2019
APPENDIX B-2
SUMMARY OF FLOW IN CAPE FEAR RIVER AT WILM O'HUSKE LOCK NR TARHEEL, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date
USGS Reported
Average
Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported
Average
Discharge (L/s)
Measured
River Width
(ft)
Estimated
River Depth
(ft)
Z Value3
Calculated Total
Cross Sectional
Area (ft2)
Calculated
River
Velocity (ft/s)
Calculated
River
Velocity
(mph)
Calculated
Travel Time to
Kelly (hrs)
Calculated
Travel Time to
Kelly (days)
7/10/2019 2,000 1.9 0.01 56,634 251 18 2 6,253 0.3 0.2 252.2 10.5
7/11/2019 1,780 1.8 0 50,404 251 18 2 5,400 0.3 0.2 244.7 10.2
7/12/2019 2,490 2.2 0.15 70,509 251 19 2 7,921 0.3 0.2 256.6 10.7
7/13/2019 3,090 2.6 0 87,499 251 19 2 9,969 0.3 0.2 260.2 10.8
7/14/2019 2,520 2.3 0 71,358 251 19 2 8,095 0.3 0.2 259.1 10.8
7/15/2019 2,270 2.1 0 64,279 251 19 2 7,227 0.3 0.2 256.8 10.7
7/16/2019 1,820 1.8 0 51,537 251 18 2 5,514 0.3 0.2 244.4 10.2
7/17/2019 1,470 1.6 0 41,626 251 18 2 4,053 0.4 0.2 222.4 9.3
Notes:
1) Measurements are recorded from the USGS flow gauging station at the W.O. Huske Dam, ID 02105500 (USGS, 2019).
2) The minimum value recorded by a USGS raingage is 0.01 inches. Anything detected below this threshold is recorded as 0 inches.
3) Z value is an estimated factor used to compute total cross sectional area from river depth.
cfs: cubic feet per second.
ft: feet.
ft2: feet squared.
hrs: hours.
L/s: Liter per second.
mph: miles per hour.
USGS - United States Geological Survey.
Page 24 of 24 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
1/1/2017 3,150 16 0.10 89,198
1/2/2017 3,270 17 1.63 92,596
1/3/2017 4,160 17 0.10 117,798
1/4/2017 6,550 18 0.00 185,475
1/5/2017 8,490 18 0.00 240,410
1/6/2017 8,400 18 0.05 237,862
1/7/2017 7,650 18 0.47 216,624
1/8/2017 8,450 18 0.00 239,277
1/9/2017 9,110 19 0.00 257,966
1/10/2017 8,650 18 0.00 244,941
1/11/2017 7,660 18 0.01 216,907
1/12/2017 6,860 18 0.00 194,254
1/13/2017 6,410 18 0.00 181,511
1/14/2017 6,260 18 0.00 177,263
1/15/2017 6,090 18 0.00 172,450
1/16/2017 5,280 17 0.00 149,513
1/17/2017 4,570 17 0.00 129,408
1/18/2017 4,210 17 0.00 119,214
1/19/2017 3,770 17 0.00 106,755
1/20/2017 3,190 16 0.00 90,331
1/21/2017 2,950 16 0.30 83,535
1/22/2017 2,910 16 0.38 82,402
1/23/2017 3,190 16 0.05 90,331
1/24/2017 3,830 17 0.00 108,454
1/25/2017 6,160 18 0.00 174,432
1/26/2017 8,620 18 0.02 244,091
1/27/2017 8,370 18 0.00 237,012
1/28/2017 7,540 18 0.00 213,509
1/29/2017 6,770 18 0.00 191,705
1/30/2017 6,370 18 0.00 180,378
1/31/2017 6,140 18 0.00 173,865
2/1/2017 5,740 18 0.00 162,539
2/2/2017 4,440 17 0.00 125,727
2/3/2017 3,360 17 0.09 95,145
2/4/2017 2,980 16 0.00 84,384
2/5/2017 2,790 16 0.00 79,004
2/6/2017 2,690 16 0.00 76,172
2/7/2017 2,630 16 0.00 74,473
2/8/2017 2,520 16 0.50 71,358
2/9/2017 2,420 16 0.20 68,527
2/10/2017 2,400 16 0.00 67,960
Page 1 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
2/11/2017 2,500 16 0.00 70,792
2/12/2017 2,620 16 0.00 74,190
2/13/2017 2,630 16 0.00 74,473
2/14/2017 2,470 16 0.00 69,943
2/15/2017 2,380 16 0.81 67,394
2/16/2017 2,820 16 0.00 79,854
2/17/2017 3,300 17 0.00 93,446
2/18/2017 3,480 17 0.00 98,543
2/19/2017 3,390 17 0.00 95,994
2/20/2017 3,120 16 0.00 88,349
2/21/2017 2,870 16 0.00 81,269
2/22/2017 2,690 16 0.00 76,172
2/23/2017 2,400 16 0.00 67,960
2/24/2017 2,120 16 0.00 60,032
2/25/2017 2,010 16 0.00 56,917
2/26/2017 1,940 16 0.00 54,935
2/27/2017 1,880 16 0.00 53,236
2/28/2017 1,840 16 0.08 52,103
3/1/2017 1,790 16 0.01 50,687
3/2/2017 1,860 16 0.10 52,669
3/3/2017 2,040 16 0.00 57,766
3/4/2017 2,380 16 0.00 67,394
3/5/2017 2,690 16 0.00 76,172
3/6/2017 2,570 16 0.00 72,774
3/7/2017 2,240 16 0.00 63,430
3/8/2017 2,260 16 0.00 63,996
3/9/2017 2,460 16 0.00 69,659
3/10/2017 2,460 16 0.02 69,659
3/11/2017 2,350 16 0.00 66,545
3/12/2017 2,210 16 0.35 62,580
3/13/2017 1,960 16 0.68 55,501
3/14/2017 2,160 16 0.13 61,164
3/15/2017 2,680 16 0.00 75,889
3/16/2017 2,960 16 0.00 83,818
3/17/2017 3,050 16 0.00 86,366
3/18/2017 2,900 16 0.12 82,119
3/19/2017 2,840 16 0.01 80,420
3/20/2017 2,650 16 0.00 75,040
Page 2 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
3/21/2017 2,440 16 0.00 69,093
3/22/2017 2,560 16 0.13 72,491
3/23/2017 2,760 16 0.00 78,154
3/24/2017 2,740 16 0.00 77,588
3/25/2017 2,500 16 0.00 70,792
3/26/2017 2,140 16 0.00 60,598
3/27/2017 1,920 16 0.00 54,368
3/28/2017 1,820 16 0.41 51,537
3/29/2017 1,730 16 0.00 48,988
3/30/2017 1,680 16 0.00 47,572
3/31/2017 1,800 16 0.41 50,970
4/1/2017 2,380 16 0.00 67,394
4/2/2017 3,070 16 0.00 86,933
4/3/2017 3,090 16 0.56 87,499
4/4/2017 3,110 16 0.01 88,065
4/5/2017 3,580 17 0.73 101,374
4/6/2017 5,000 17 0.30 141,584
4/7/2017 6,090 18 0.00 172,450
4/8/2017 6,710 18 0.00 190,006
4/9/2017 7,110 18 0.00 201,333
4/10/2017 6,220 18 0.00 176,131
4/11/2017 4,370 17 0.00 123,745
4/12/2017 2,890 16 0.00 81,836
4/13/2017 2,270 16 0.39 64,279
4/14/2017 2,030 16 0.00 57,483
4/15/2017 1,870 16 0.00 52,953
4/16/2017 1,740 16 0.00 49,271
4/17/2017 1,660 16 0.00 47,006
4/18/2017 1,590 16 0.02 45,024
4/19/2017 1,560 16 0.15 44,174
4/20/2017 1,510 16 0.00 42,758
4/21/2017 1,430 15 0.00 40,493
4/22/2017 1,390 15 0.00 39,360
4/23/2017 1,350 15 0.02 38,228
4/24/2017 1,710 16 2.43 48,422
4/25/2017 5,040 17 0.44 142,717
4/26/2017 12,600 19 0.00 356,792
4/27/2017 17,100 20 0.00 484,218
4/28/2017 19,000 21 0.00 538,020
4/29/2017 20,000 21 0.00 566,337
4/30/2017 20,200 21 0.00 572,000
Page 3 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
5/1/2017 19,200 21 0.01 543,683
5/2/2017 17,800 20 0.37 504,040
5/3/2017 16,300 20 0.00 461,565
5/4/2017 15,200 20 0.06 430,416
5/5/2017 14,400 20 0.50 407,763
5/6/2017 14,000 20 0.09 396,436
5/7/2017 14,100 20 0.06 399,268
5/8/2017 14,000 20 0.00 396,436
5/9/2017 12,200 19 0.00 345,466
5/10/2017 8,810 18 0.00 249,471
5/11/2017 5,820 18 0.00 164,804
5/12/2017 4,090 17 0.00 115,816
5/13/2017 3,480 17 0.00 98,543
5/14/2017 3,060 16 0.00 86,650
5/15/2017 2,810 16 0.00 79,570
5/16/2017 2,630 16 0.00 74,473
5/17/2017 2,260 16 0.00 63,996
5/18/2017 1,850 16 0.00 52,386
5/19/2017 1,650 16 0.00 46,723
5/20/2017 1,520 16 0.00 43,042
5/21/2017 1,470 15 0.00 41,626
5/22/2017 1,630 16 0.66 46,156
5/23/2017 1,890 16 1.18 53,519
5/24/2017 3,550 17 0.51 100,525
5/25/2017 6,340 18 0.28 179,529
5/26/2017 8,780 18 0.00 248,622
5/27/2017 10,800 19 0.00 305,822
5/28/2017 11,700 19 0.19 331,307
5/29/2017 10,400 19 0.25 294,495
5/30/2017 8,160 18 0.12 231,065
5/31/2017 6,980 18 0.00 197,652
6/1/2017 7,030 18 0.00 199,067
6/2/2017 7,680 18 0.03 217,473
6/3/2017 7,640 18 0.00 216,341
6/4/2017 6,370 18 0.00 180,378
6/5/2017 4,390 17 0.64 124,311
6/6/2017 3,460 17 0.09 97,976
6/7/2017 4,020 17 0.30 113,834
6/8/2017 4,470 17 0.34 126,576
6/9/2017 4,840 17 0.00 137,054
6/10/2017 4,550 17 0.00 128,842
Page 4 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
6/11/2017 3,510 17 0.00 99,392
6/12/2017 2,560 16 0.00 72,491
6/13/2017 2,090 16 0.00 59,182
6/14/2017 1,670 16 0.77 47,289
6/15/2017 1,580 16 0.08 44,741
6/16/2017 1,770 16 0.25 50,121
6/17/2017 1,890 16 0.03 53,519
6/18/2017 1,920 16 0.03 54,368
6/19/2017 2,300 16 0.07 65,129
6/20/2017 2,500 16 0.59 70,792
6/21/2017 4,250 17 0.04 120,347
6/22/2017 6,620 18 0.14 187,458
6/23/2017 8,950 19 0.00 253,436
6/24/2017 8,630 18 0.42 244,374
6/25/2017 9,630 19 0.01 272,691
6/26/2017 11,100 19 0.02 314,317
6/27/2017 11,200 19 0.00 317,149
6/28/2017 10,500 19 0.00 297,327
6/29/2017 9,510 19 0.00 269,293
6/30/2017 8,210 18 1.68 232,481
7/1/2017 7,200 18 0.02 203,881
7/2/2017 5,400 17 0.00 152,911
7/3/2017 3,640 17 0.00 103,073
7/4/2017 3,390 17 0.00 95,994
7/5/2017 3,330 17 0.00 94,295
7/6/2017 2,950 16 0.00 83,535
7/7/2017 2,510 16 0.28 71,075
7/8/2017 2,240 16 0.38 63,430
7/9/2017 2,040 16 0.60 57,766
7/10/2017 1,950 16 0.46 55,218
7/11/2017 1,970 16 0.05 55,784
7/12/2017 1,840 16 0.01 52,103
7/13/2017 1,800 16 0.00 50,970
7/14/2017 1,580 16 0.00 44,741
7/15/2017 1,400 15 0.67 39,644
7/16/2017 1,400 15 0.02 39,644
7/17/2017 1,490 15 0.04 42,192
7/18/2017 1,870 16 0.16 52,953
7/19/2017 1,930 16 0.10 54,652
7/20/2017 1,630 16 0.01 46,156
7/21/2017 1,550 16 0.00 43,891
Page 5 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
7/22/2017 1,590 16 0.00 45,024
7/23/2017 1,550 16 0.00 43,891
7/24/2017 1,550 16 0.00 43,891
7/25/2017 1,590 16 0.00 45,024
7/26/2017 1,510 16 0.00 42,758
7/27/2017 1,370 15 0.00 38,794
7/28/2017 1,220 15 0.00 34,547
7/29/2017 1,150 15 0.62 32,564
7/30/2017 1,120 15 0.00 31,715
7/31/2017 1,090 15 0.00 30,865
8/1/2017 1,060 15 0.00 30,016
8/2/2017 1,030 15 0.00 29,166
8/3/2017 976 15 0.00 27,637
8/4/2017 956 15 0.01 27,071
8/5/2017 957 15 0.01 27,099
8/6/2017 982 15 0.00 27,807
8/7/2017 974 15 0.24 27,581
8/8/2017 1,130 15 1.40 31,998
8/9/2017 1,460 15 0.00 41,343
8/10/2017 1,590 16 0.05 45,024
8/11/2017 1,550 16 0.21 43,891
8/12/2017 1,400 15 0.26 39,644
8/13/2017 1,590 16 0.77 45,024
8/14/2017 2,950 16 0.01 83,535
8/15/2017 2,980 16 0.42 84,384
8/16/2017 2,180 16 0.00 61,731
8/17/2017 1,680 16 0.00 47,572
8/18/2017 1,580 16 0.00 44,741
8/19/2017 1,640 16 1.27 46,440
8/20/2017 1,580 16 0.00 44,741
8/21/2017 1,370 15 0.00 38,794
8/22/2017 1,210 15 0.01 34,263
8/23/2017 1,150 15 0.57 32,564
8/24/2017 1,260 15 0.57 35,679
8/25/2017 1,590 16 0.65 45,024
8/26/2017 1,520 16 0.00 43,042
8/27/2017 1,280 15 0.00 36,246
8/28/2017 1,110 15 0.02 31,432
8/29/2017 1,160 15 0.07 32,848
8/30/2017 1,130 15 0.00 31,998
8/31/2017 1,060 15 0.29 30,016
Page 6 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
9/1/2017 1,110 15 0.01 31,432
9/2/2017 1,550 16 0.52 43,891
9/3/2017 2,540 16 0.00 71,925
9/4/2017 2,480 16 0.00 70,226
9/5/2017 1,850 16 0.19 52,386
9/6/2017 1,750 16 1.17 49,554
9/7/2017 2,000 16 0.00 56,634
9/8/2017 2,180 16 0.00 61,731
9/9/2017 2,090 16 0.00 59,182
9/10/2017 1,740 16 0.00 49,271
9/11/2017 1,530 16 0.08 43,325
9/12/2017 1,980 16 3.08 56,067
9/13/2017 2,530 16 0.00 71,642
9/14/2017 2,350 16 0.00 66,545
9/15/2017 2,130 16 0.00 60,315
9/16/2017 1,840 16 0.00 52,103
9/17/2017 1,600 16 0.00 45,307
9/18/2017 1,430 15 0.00 40,493
9/19/2017 1,310 15 0.00 37,095
9/20/2017 1,220 15 0.16 34,547
9/21/2017 1,210 15 0.24 34,263
9/22/2017 1,180 15 0.00 33,414
9/23/2017 1,120 15 0.00 31,715
9/24/2017 1,070 15 0.00 30,299
9/25/2017 1,010 15 0.00 28,600
9/26/2017 991 15 0.00 28,062
9/27/2017 965 15 0.00 27,326
9/28/2017 929 15 0.00 26,306
9/29/2017 909 15 0.00 25,740
9/30/2017 875 15 0.00 24,777
10/1/2017 822 15 0.00 23,276
10/2/2017 812 15 0.00 22,993
10/3/2017 825 15 0.00 23,361
10/4/2017 837 15 0.00 23,701
10/5/2017 849 15 0.00 24,041
10/6/2017 855 15 0.00 24,211
10/7/2017 862 15 0.15 24,409
10/8/2017 919 15 0.06 26,023
10/9/2017 1,080 15 0.50 30,582
10/10/2017 1,250 15 0.01 35,396
10/11/2017 1,280 15 0.03 36,246
Page 7 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
10/12/2017 1,240 15 0.01 35,113
10/13/2017 1,150 15 0.00 32,564
10/14/2017 1,120 15 0.00 31,715
10/15/2017 1,100 15 0.00 31,149
10/16/2017 1,040 15 0.24 29,450
10/17/2017 958 15 0.00 27,128
10/18/2017 933 15 0.00 26,420
10/19/2017 901 15 0.00 25,513
10/20/2017 863 15 0.00 24,437
10/21/2017 847 15 0.00 23,984
10/22/2017 837 15 0.00 23,701
10/23/2017 803 15 0.96 22,738
10/24/2017 893 15 0.01 25,287
10/25/2017 1,080 15 0.00 30,582
10/26/2017 1,410 15 0.00 39,927
10/27/2017 1,430 15 0.00 40,493
10/28/2017 1,300 15 0.26 36,812
10/29/2017 1,340 15 0.57 37,945
10/30/2017 1,430 15 0.00 40,493
10/31/2017 1,370 15 0.00 38,794
11/1/2017 1,200 15 0.00 33,980
11/2/2017 1,050 15 0.00 29,733
11/3/2017 929 15 0.00 26,306
11/4/2017 886 15 0.00 25,089
11/5/2017 880 15 0.00 24,919
11/6/2017 852 15 0.00 24,126
11/7/2017 848 15 0.00 24,013
11/8/2017 874 15 0.01 24,749
11/9/2017 914 15 0.42 25,882
11/10/2017 970 15 0.00 27,467
11/11/2017 1,030 15 0.00 29,166
11/12/2017 1,060 15 0.00 30,016
11/13/2017 1,060 15 0.18 30,016
11/14/2017 1,050 15 0.00 29,733
11/15/2017 1,080 15 0.00 30,582
11/16/2017 1,130 15 0.00 31,998
11/17/2017 1,150 15 0.00 32,564
11/18/2017 1,090 15 0.00 30,865
11/19/2017 1,050 15 0.02 29,733
11/20/2017 1,010 15 0.00 28,600
11/21/2017 1,010 15 0.01 28,600
Page 8 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
11/22/2017 1,010 15 0.03 28,600
11/23/2017 996 15 0.00 28,204
11/24/2017 1,050 15 0.00 29,733
11/25/2017 1,070 15 0.00 30,299
11/26/2017 1,050 15 0.00 29,733
11/27/2017 1,000 15 0.00 28,317
11/28/2017 964 15 0.00 27,297
11/29/2017 963 15 0.00 27,269
11/30/2017 957 15 0.00 27,099
12/1/2017 966 15 0.00 27,354
12/2/2017 996 15 0.00 28,204
12/3/2017 1,010 15 0.00 28,600
12/4/2017 996 15 0.00 28,204
12/5/2017 1,000 15 0.01 28,317
12/6/2017 1,040 15 0.25 29,450
12/7/2017 1,100 15 0.21 31,149
12/8/2017 1,270 15 1.37 35,962
12/9/2017 2,160 16 0.42 61,164
12/10/2017 3,080 16 0.00 87,216
12/11/2017 3,200 17 0.00 90,614
12/12/2017 2,770 16 0.00 78,438
12/13/2017 2,220 16 62,863
12/14/2017 1,850 16 0.00 52,386
12/15/2017 1,560 16 0.01 44,174
12/16/2017 1,290 15 0.00 36,529
12/17/2017 1,100 15 0.00 31,149
12/18/2017 988 15 0.02 27,977
12/19/2017 921 15 0.00 26,080
12/20/2017 935 15 0.72 26,476
12/21/2017 1,210 15 0.01 34,263
12/22/2017 1,490 16 0.01 42,192
12/23/2017 1,650 16 0.00 46,723
12/24/2017 1,660 16 0.50 47,006
12/25/2017 1,520 16 0.01 43,042
12/26/2017 1,330 16 0.00 37,661
12/27/2017 1,250 16 0.34 35,396
12/28/2017 1,210 15 0.00 34,263
12/29/2017 1,180 15 0.00 33,414
12/30/2017 1,220 15 0.00 34,547
12/31/2017 1,110 15 0.00 31,432
1/1/2018 1,030 15 0.00 29,166
Page 9 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
1/2/2018 971 15 0.00 27,496
1/3/2018 974 15 27,581
1/4/2018 967 15 27,382
1/5/2018 906 15 0.00 25,655
1/6/2018 883 15 0.00 25,004
1/7/2018 854 15 0.00 24,183
1/8/2018 840 15 0.00 23,786
1/9/2018 866 15 0.00 24,522
1/10/2018 883 15 0.01 25,004
1/11/2018 863 15 0.14 24,437
1/12/2018 919 15 1.32 26,023
1/13/2018 1,180 15 0.01 33,414
1/14/2018 1,380 16 0.00 39,077
1/15/2018 1,540 16 0.00 43,608
1/16/2018 1,520 16 0.00 43,042
1/17/2018 1,480 16 0.08 41,909
1/18/2018 1,530 16 0.00 43,325
1/19/2018 1,500 16 0.00 42,475
1/20/2018 1,420 16 0.00 40,210
1/21/2018 1,340 16 0.00 37,945
1/22/2018 1,300 16 0.06 36,812
1/23/2018 1,290 16 0.07 36,529
1/24/2018 1,340 16 0.00 37,945
1/25/2018 1,400 16 0.00 39,644
1/26/2018 1,700 16 0.00 48,139
1/27/2018 2,000 16 0.00 56,634
1/28/2018 1,780 16 1.16 50,404
1/29/2018 2,500 16 0.54 70,792
1/30/2018 5,250 17 0.00 148,663
1/31/2018 8,090 18 0.00 229,083
2/1/2018 8,200 18 0.00 232,198
2/2/2018 5,930 18 0.09 167,919
2/3/2018 4,200 17 0.00 118,931
2/4/2018 3,250 17 0.54 92,030
2/5/2018 3,340 17 0.00 94,578
2/6/2018 4,680 17 0.00 132,523
2/7/2018 6,290 18 178,113
2/8/2018 6,050 18 171,317
2/9/2018 4,730 17 133,939
2/10/2018 4,030 17 114,117
2/11/2018 4,260 17 120,630
Page 10 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
2/12/2018 4,070 17 115,250
2/13/2018 3,650 17 0.00 103,356
2/14/2018 4,390 17 0.00 124,311
2/15/2018 4,680 17 0.00 132,523
2/16/2018 4,350 17 0.00 123,178
2/17/2018 4,120 17 0.00 116,665
2/18/2018 3,890 17 0.00 110,153
2/19/2018 3,660 17 0.11 103,640
2/20/2018 3,420 17 0.01 96,844
2/21/2018 3,340 17 0.00 94,578
2/22/2018 3,270 17 0.00 92,596
2/23/2018 3,220 16 0.00 91,180
2/24/2018 2,690 16 0.00 76,172
2/25/2018 2,170 16 0.00 61,448
2/26/2018 1,970 16 0.08 55,784
2/27/2018 1,870 16 0.00 52,953
2/28/2018 1,790 16 0.12 50,687
3/1/2018 1,820 16 0.82 51,537
3/2/2018 2,300 16 0.01 65,129
3/3/2018 3,080 16 0.00 87,216
3/4/2018 3,960 17 0.00 112,135
3/5/2018 4,510 17 0.00 127,709
3/6/2018 4,110 17 0.09 116,382
3/7/2018 3,520 17 0.22 99,675
3/8/2018 2,860 16 0.00 80,986
3/9/2018 2,570 16 0.00 72,774
3/10/2018 2,850 16 0.00 80,703
3/11/2018 2,980 16 0.05 84,384
3/12/2018 2,730 16 0.47 77,305
3/13/2018 2,850 16 0.01 80,703
3/14/2018 4,930 17 0.00 139,602
3/15/2018 7,050 18 0.00 199,634
3/16/2018 7,530 18 0.00 213,226
3/17/2018 7,070 18 0.00 200,200
3/18/2018 5,820 18 0.00 164,804
3/19/2018 4,920 17 0.00 139,319
3/20/2018 4,590 17 1.89 129,974
3/21/2018 5,310 17 0.01 150,362
3/22/2018 7,830 18 0.00 221,721
3/23/2018 10,300 19 0.00 291,664
3/24/2018 10,300 19 0.14 291,664
Page 11 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
3/25/2018 8,270 18 0.18 234,180
3/26/2018 7,260 18 0.00 205,580
3/27/2018 7,540 18 0.00 213,509
3/28/2018 7,560 18 0.00 214,075
3/29/2018 7,390 18 0.00 209,261
3/30/2018 6,950 18 0.00 196,802
3/31/2018 6,420 18 0.00 181,794
4/1/2018 5,040 17 0.00 142,717
4/2/2018 3,980 17 0.00 112,701
4/3/2018 3,500 17 0.00 99,109
4/4/2018 2,860 16 0.04 80,986
4/5/2018 2,360 16 0.00 66,828
4/6/2018 2,260 16 0.00 63,996
4/7/2018 2,160 16 0.85 61,164
4/8/2018 2,390 16 0.20 67,677
4/9/2018 3,020 16 0.29 85,517
4/10/2018 3,690 17 0.01 104,489
4/11/2018 4,810 17 0.00 136,204
4/12/2018 5,120 17 0.00 144,982
4/13/2018 4,620 17 0.00 130,824
4/14/2018 3,340 17 0.00 94,578
4/15/2018 2,450 16 0.75 69,376
4/16/2018 2,640 16 0.01 74,756
4/17/2018 8,050 18 0.00 227,951
4/18/2018 13,100 20 0.00 370,951
4/19/2018 14,100 20 0.00 399,268
4/20/2018 13,900 20 0.00 393,604
4/21/2018 12,700 19 0.00 359,624
4/22/2018 10,300 19 0.00 291,664
4/23/2018 8,410 18 0.25 238,145
4/24/2018 7,960 18 1.36 225,402
4/25/2018 7,310 18 0.00 206,996
4/26/2018 9,520 19 0.00 269,576
4/27/2018 13,500 20 0.09 382,277
4/28/2018 14,400 20 0.00 407,763
4/29/2018 13,700 20 0.00 387,941
4/30/2018 12,400 19 0.00 351,129
5/1/2018 10,300 19 0.00 291,664
5/2/2018 8,500 18 0.00 240,693
5/3/2018 7,490 18 0.00 212,093
5/4/2018 6,940 18 0.00 196,519
Page 12 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
5/5/2018 6,570 18 0.00 186,042
5/6/2018 5,310 17 0.50 150,362
5/7/2018 4,430 17 0.00 125,444
5/8/2018 4,030 17 0.00 114,117
5/9/2018 3,450 17 0.00 97,693
5/10/2018 2,780 16 0.00 78,721
5/11/2018 2,370 16 0.00 67,111
5/12/2018 1,840 16 0.00 52,103
5/13/2018 1,480 15 0.00 41,909
5/14/2018 1,350 15 0.00 38,228
5/15/2018 1,300 15 0.07 36,812
5/16/2018 1,330 15 0.00 37,661
5/17/2018 1,410 15 0.06 39,927
5/18/2018 1,770 16 0.55 50,121
5/19/2018 2,480 16 1.46 70,226
5/20/2018 3,550 17 0.02 100,525
5/21/2018 5,610 17 0.00 158,858
5/22/2018 7,540 18 0.01 213,509
5/23/2018 7,360 18 0.02 208,412
5/24/2018 8,300 18 0.00 235,030
5/25/2018 8,730 18 0.08 247,206
5/26/2018 7,540 18 0.08 213,509
5/27/2018 5,200 17 0.14 147,248
5/28/2018 3,710 17 2.15 105,056
5/29/2018 3,800 17 0.77 107,604
5/30/2018 4,280 17 0.01 121,196
5/31/2018 5,230 17 0.06 148,097
6/1/2018 6,800 18 0.01 192,555
6/2/2018 7,360 18 0.04 208,412
6/3/2018 6,050 18 0.00 171,317
6/4/2018 4,450 17 0.00 126,010
6/5/2018 3,170 17 0.00 89,764
6/6/2018 2,340 16 0.00 66,261
6/7/2018 1,830 16 0.03 51,820
6/8/2018 1,480 16 0.00 41,909
6/9/2018 1,290 15 1.00 36,529
6/10/2018 1,200 15 0.01 33,980
6/11/2018 1,070 15 0.60 30,299
6/12/2018 1,440 16 0.02 40,776
6/13/2018 2,120 16 0.00 60,032
Page 13 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
6/14/2018 2,030 16 0.36 57,483
6/15/2018 1,660 16 0.00 47,006
6/16/2018 1,420 16 0.00 40,210
6/17/2018 1,230 15 0.00 34,830
6/18/2018 1,100 15 0.00 31,149
6/19/2018 1,050 15 0.00 29,733
6/20/2018 988 15 0.00 27,977
6/21/2018 948 15 0.00 26,844
6/22/2018 1,000 15 0.02 28,317
6/23/2018 1,000 15 0.12 28,317
6/24/2018 973 15 1.37 27,552
6/25/2018 1,040 15 0.95 29,450
6/26/2018 1,260 15 1.06 35,679
6/27/2018 1,920 16 0.00 54,368
6/28/2018 2,370 16 0.00 67,111
6/29/2018 2,530 16 0.00 71,642
6/30/2018 2,150 16 0.07 60,881
7/1/2018 1,660 16 0.05 47,006
7/2/2018 1,340 15 0.00 37,945
7/3/2018 1,110 15 0.00 31,432
7/4/2018 954 15 0.00 27,014
7/5/2018 859 15 0.37 24,324
7/6/2018 852 15 0.01 24,126
7/7/2018 965 15 0.00 27,326
7/8/2018 1,290 15 0.00 36,529
7/9/2018 1,670 16 0.00 47,289
7/10/2018 1,670 16 0.00 47,289
7/11/2018 1,520 16 0.00 43,042
7/12/2018 1,190 15 0.54 33,697
7/13/2018 1,050 15 0.01 29,733
7/14/2018 970 15 0.00 27,467
7/15/2018 851 15 0.00 24,098
7/16/2018 792 15 0.00 22,427
7/17/2018 784 15 0.02 22,200
7/18/2018 906 15 0.27 25,655
7/19/2018 1,800 16 0.00 50,970
7/20/2018 1,600 16 0.42 45,307
7/21/2018 1,140 15 0.05 32,281
7/22/2018 926 15 0.00 26,221
7/23/2018 1,960 16 0.11 55,501
7/24/2018 5,140 17 0.63 145,549
Page 14 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
7/25/2018 6,340 18 0.38 179,529
7/26/2018 5,050 17 0.01 143,000
7/27/2018 4,210 17 0.00 119,214
7/28/2018 3,370 17 0.01 95,428
7/29/2018 3,470 17 0.03 98,259
7/30/2018 3,920 17 0.67 111,002
7/31/2018 4,350 17 0.09 123,178
8/1/2018 4,550 17 0.31 128,842
8/2/2018 4,420 17 0.88 125,160
8/3/2018 4,290 17 0.10 121,479
8/4/2018 5,250 17 0.09 148,663
8/5/2018 8,980 19 0.12 254,285
8/6/2018 9,550 19 0.01 270,426
8/7/2018 9,010 19 0.00 255,135
8/8/2018 8,620 18 0.14 244,091
8/9/2018 8,390 18 0.00 237,578
8/10/2018 9,610 19 0.00 272,125
8/11/2018 9,570 19 0.22 270,992
8/12/2018 7,910 18 0.00 223,986
8/13/2018 9,060 19 0.19 256,551
8/14/2018 11,300 19 0.02 319,980
8/15/2018 12,500 19 0.00 353,961
8/16/2018 13,300 20 0.00 376,614
8/17/2018 12,500 19 0.11 353,961
8/18/2018 10,200 19 0.02 288,832
8/19/2018 6,960 18 0.00 197,085
8/20/2018 7,680 18 0.00 217,473
8/21/2018 11,300 19 0.00 319,980
8/22/2018 13,800 20 0.00 390,772
8/23/2018 14,600 20 0.02 413,426
8/24/2018 13,700 20 0.00 387,941
8/25/2018 12,100 19 0.00 342,634
8/26/2018 8,090 18 0.00 229,083
8/27/2018 4,930 17 0.00 139,602
8/28/2018 3,310 17 0.00 93,729
8/29/2018 2,200 16 0.00 62,297
8/30/2018 1,680 16 0.00 47,572
8/31/2018 1,470 16 0.00 41,626
9/1/2018 1,370 15 0.00 38,794
9/2/2018 1,420 16 0.00 40,210
9/3/2018 1,610 16 0.16 45,590
Page 15 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
9/4/2018 1,810 16 0.00 51,253
9/5/2018 1,810 16 0.00 51,253
9/6/2018 1,610 16 0.00 45,590
9/7/2018 1,370 15 0.08 38,794
9/8/2018 1,240 15 0.01 35,113
9/9/2018 1,200 15 0.02 33,980
9/10/2018 1,280 15 0.67 36,246
9/11/2018 1,390 16 0.08 39,360
9/12/2018 1,790 16 0.00 50,687
9/13/2018 2,710 16 0.64 76,739
9/14/2018 3,500 17 6.37 99,109
9/15/2018 11,300 19 9.03 319,980
9/16/2018 27,600 22 6.07 781,545
9/17/2018 43,200 24 2.37 1,223,288
9/18/2018 56,800 0.00 1,608,397
9/19/2018 65,700 0.00 1,860,417
9/20/2018 73,700 30 0.00 2,086,952
9/21/2018 76,300 31 0.00 2,160,575
9/22/2018 75,400 30 0.00 2,135,090
9/23/2018 72,200 30 0.00 2,044,476
9/24/2018 65,800 28 0.00 1,863,249
9/25/2018 56,300 27 0.00 1,594,238
9/26/2018 42,300 24 0.00 1,197,803
9/27/2018 26,200 22 0.00 741,901
9/28/2018 18,000 20 0.00 509,703
9/29/2018 16,000 20 0.00 453,070
9/30/2018 16,200 20 0.00 458,733
10/1/2018 16,400 20 0.00 464,396
10/2/2018 16,000 20 0.00 453,070
10/3/2018 15,100 20 0.00 427,584
10/4/2018 14,300 20 0.00 404,931
10/5/2018 13,600 20 0.00 385,109
10/6/2018 13,000 19 0.04 368,119
10/7/2018 12,300 19 0.00 348,297
10/8/2018 11,600 19 0.07 328,475
10/9/2018 11,100 19 0.00 314,317
10/10/2018 10,400 19 0.16 294,495
10/11/2018 6,420 18 0.13 181,794
10/12/2018 4,530 17 0.00 128,275
10/13/2018 9,740 19 0.00 275,806
10/14/2018 13,500 20 0.00 382,277
Page 16 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
10/15/2018 14,500 20 0.00 410,594
10/16/2018 13,600 20 0.64 385,109
10/17/2018 12,500 19 0.09 353,961
10/18/2018 12,700 19 0.00 359,624
10/19/2018 12,900 19 0.00 365,287
10/20/2018 12,800 19 0.00 362,456
10/21/2018 12,300 19 0.00 348,297
10/22/2018 11,500 19 0.00 325,644
10/23/2018 10,900 19 0.00 308,654
10/24/2018 9,980 19 0.00 282,602
10/25/2018 8,600 18 0.00 243,525
10/26/2018 7,500 18 0.62 212,376
10/27/2018 7,200 18 0.00 203,881
10/28/2018 9,440 19 0.00 267,311
10/29/2018 12,500 19 0.00 353,961
10/30/2018 13,400 20 0.00 379,446
10/31/2018 12,600 19 0.00 356,792
11/1/2018 10,800 19 0.11 305,822
11/2/2018 8,860 18 0.02 250,887
11/3/2018 6,420 18 0.00 181,794
11/4/2018 5,680 18 0.07 160,840
11/5/2018 6,040 18 0.09 171,034
11/6/2018 6,020 18 0.16 170,467
11/7/2018 7,880 18 0.12 223,137
11/8/2018 10,700 19 0.96 302,990
11/9/2018 10,100 19 0.00 286,000
11/10/2018 9,320 19 0.01 263,913
11/11/2018 8,980 19 0.00 254,285
11/12/2018 8,560 18 0.20 242,392
11/13/2018 9,740 19 0.30 275,806
11/14/2018 15,700 20 0.02 444,574
11/15/2018 20,600 21 0.23 583,327
11/16/2018 27,400 22 0.00 775,882
11/17/2018 34,700 23 0.00 982,595
11/18/2018 39,500 24 0.00 1,118,515
11/19/2018 39,200 24 0.44 1,110,020
11/20/2018 33,800 23 0.00 957,109
11/21/2018 26,500 22 0.00 750,396
11/22/2018 21,600 21 0.01 611,644
11/23/2018 19,200 21 0.00 543,683
11/24/2018 16,700 20 0.49 472,891
Page 17 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
11/25/2018 15,200 20 0.00 430,416
11/26/2018 15,600 20 0.03 441,743
11/27/2018 16,300 20 0.00 461,565
11/28/2018 16,900 20 0.00 478,555
11/29/2018 17,000 20 0.00 481,386
11/30/2018 17,100 20 0.00 484,218
12/1/2018 17,300 20 0.61 489,881
12/2/2018 17,600 20 0.05 498,377
12/3/2018 18,300 20 0.01 518,198
12/4/2018 19,000 21 0.00 538,020
12/5/2018 19,500 21 0.00 552,179
12/6/2018 19,600 21 0.00 555,010
12/7/2018 19,100 21 0.00 540,852
12/8/2018 17,400 20 0.74 492,713
12/9/2018 14,800 20 1.16 419,089
12/10/2018 14,600 20 0.21 413,426
12/11/2018 17,400 20 0.01 492,713
12/12/2018 19,900 21 0.00 563,505
12/13/2018 21,400 21 0.00 605,981
12/14/2018 21,500 21 1.87 608,812
12/15/2018 20,200 21 0.42 572,000
12/16/2018 19,600 21 0.01 555,010
12/17/2018 20,600 21 0.00 583,327
12/18/2018 21,600 21 0.00 611,644
12/19/2018 21,800 21 0.00 617,307
12/20/2018 20,800 21 0.37 588,990
12/21/2018 18,900 21 0.26 535,188
12/22/2018 17,600 20 0.00 498,377
12/23/2018 18,600 20 0.01 526,693
12/24/2018 19,800 21 0.00 560,674
12/25/2018 20,300 21 0.00 574,832
12/26/2018 19,900 21 0.00 563,505
12/27/2018 18,800 21 0.04 532,357
12/28/2018 18,100 20 0.79 512,535
12/29/2018 17,300 20 0.00 489,881
12/30/2018 17,500 20 0.21 495,545
12/31/2018 19,100 21 0.00 540,852
1/1/2019 20,300 21 0.00 574,832
1/2/2019 21,000 21 0.02 594,654
1/3/2019 21,200 21 0.03 600,317
1/4/2019 21,000 21 0.31 594,654
Page 18 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
1/5/2019 21,000 21 0.00 594,654
1/6/2019 21,300 21 0.00 603,149
1/7/2019 21,600 21 0.00 611,644
1/8/2019 21,800 21 0.00 617,307
1/9/2019 21,300 21 0.00 603,149
1/10/2019 20,900 21 0.00 591,822
1/11/2019 20,500 21 0.00 580,495
1/12/2019 20,000 21 0.00 566,337
1/13/2019 19,400 21 0.25 549,347
1/14/2019 19,000 21 0.00 538,020
1/15/2019 19,500 21 0.00 552,179
1/16/2019 20,200 21 0.00 572,000
1/17/2019 20,500 21 0.12 580,495
1/18/2019 20,000 21 0.01 566,337
1/19/2019 18,200 20 0.00 515,367
1/20/2019 14,500 20 0.15 410,594
1/21/2019 11,600 19 0.00 328,475
1/22/2019 11,900 19 0.00 336,970
1/23/2019 12,300 19 0.00 348,297
1/24/2019 12,800 0.68 362,456
1/25/2019 14,500 0.00 410,594
1/26/2019 16,700 0.00 472,891
1/27/2019 18,400 0.00 521,030
1/28/2019 17,900 0.00 506,872
1/29/2019 16,200 0.00 458,733
1/30/2019 14,800 20 0.00 419,089
1/31/2019 13,600 19 0.00 385,109
2/1/2019 12,500 19 0.00 353,961
2/2/2019 10,200 19 0.00 288,832
2/3/2019 7,860 18 0.11 222,570
2/4/2019 6,900 18 0.01 195,386
2/5/2019 6,360 17 0.00 180,095
2/6/2019 5,740 17 0.00 162,539
2/7/2019 5,310 17 0.00 150,362
2/8/2019 5,110 17 0.00 144,699
2/9/2019 4,820 17 0.00 136,487
2/10/2019 4,430 17 0.00 125,444
2/11/2019 4,230 17 0.47 119,780
2/12/2019 4,300 17 0.01 121,762
2/13/2019 4,750 17 0.03 134,505
2/14/2019 5,350 17 0.00 151,495
Page 19 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
2/15/2019 5,960 17 0.00 168,768
2/16/2019 7,210 18 0.25 204,164
2/17/2019 8,680 18 0.00 245,790
2/18/2019 11,300 19 0.02 319,980
2/19/2019 13,000 19 0.10 368,119
2/20/2019 14,100 20 0.20 399,268
2/21/2019 14,700 20 0.00 416,258
2/22/2019 15,700 20 0.14 444,574
2/23/2019 17,100 20 0.10 484,218
2/24/2019 18,600 21 0.01 526,693
2/25/2019 19,900 21 0.00 563,505
2/26/2019 21,100 21 0.00 597,485
2/27/2019 21,800 21 0.00 617,307
2/28/2019 20,600 21 0.00 583,327
3/1/2019 18,500 20 0.53 523,862
3/2/2019 16,900 20 0.15 478,555
3/3/2019 16,500 20 0.51 467,228
3/4/2019 16,800 20 0.09 475,723
3/5/2019 17,000 20 0.28 481,386
3/6/2019 17,700 20 0.00 501,208
3/7/2019 17,500 20 0.00 495,545
3/8/2019 16,000 20 0.24 453,070
3/9/2019 15,400 20 0.02 436,079
3/10/2019 15,900 20 0.00 450,238
3/11/2019 16,700 20 0.00 472,891
3/12/2019 17,200 20 0.00 487,050
3/13/2019 17,400 20 0.00 492,713
3/14/2019 17,400 20 0.00 492,713
3/15/2019 17,100 20 0.00 484,218
3/16/2019 16,700 20 0.00 472,891
3/17/2019 16,400 20 0.00 464,396
3/18/2019 16,100 20 0.00 455,901
3/19/2019 15,900 20 0.00 450,238
3/20/2019 15,500 20 0.23 438,911
3/21/2019 14,500 20 0.22 410,594
3/22/2019 12,900 19 0.01 365,287
3/23/2019 13,600 19 0.00 385,109
3/24/2019 14,400 20 0.00 407,763
3/25/2019 13,300 19 0.01 376,614
3/26/2019 11,700 19 0.05 331,307
3/27/2019 11,400 19 0.00 322,812
Page 20 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
3/28/2019 11,900 19 0.00 336,970
3/29/2019 12,000 19 0.00 339,802
3/30/2019 11,400 19 0.00 322,812
3/31/2019 8,160 18 0.00 231,065
4/1/2019 5,650 17 0.00 159,990
4/2/2019 5,160 17 1.21 146,115
4/3/2019 6,220 17 0.00 176,131
4/4/2019 7,180 18 0.00 203,315
4/5/2019 7,280 18 1.24 206,147
4/6/2019 8,090 18 0.07 229,083
4/7/2019 9,490 18 0.00 268,727
4/8/2019 11,200 19 0.00 317,149
4/9/2019 10,700 19 0.02 302,990
4/10/2019 12,600 19 0.00 356,792
4/11/2019 15,800 20 0.00 447,406
4/12/2019 16,500 20 0.65 467,228
4/13/2019 15,800 20 0.04 447,406
4/14/2019 17,100 20 0.01 484,218
4/15/2019 19,500 21 0.00 552,179
4/16/2019 21,100 21 0.00 597,485
4/17/2019 21,900 21 0.00 620,139
4/18/2019 20,800 21 0.00 588,990
4/19/2019 17,300 20 1.35 489,881
4/20/2019 13,300 19 0.00 376,614
4/21/2019 12,000 19 0.00 339,802
4/22/2019 13,000 19 0.00 368,119
4/23/2019 12,400 19 0.00 351,129
4/24/2019 13,000 19 0.00 368,119
4/25/2019 13,800 20 0.00 390,772
4/26/2019 14,000 20 0.07 396,436
4/27/2019 13,700 20 0.00 387,941
4/28/2019 13,300 19 0.00 376,614
4/29/2019 12,900 19 0.00 365,287
4/30/2019 12,500 19 0.00 353,961
5/1/2019 12,200 19 0.00 345,466
5/2/2019 11,800 19 0.00 334,139
5/3/2019 11,600 19 0.00 328,475
5/4/2019 11,300 19 0.00 319,980
5/5/2019 10,600 19 0.13 300,159
5/6/2019 10,200 19 0.00 288,832
5/7/2019 10,500 19 0.00 297,327
Page 21 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
5/8/2019 10,100 19 0.00 286,000
5/9/2019 8,000 18 0.00 226,535
5/10/2019 5,390 17 0.00 152,628
5/11/2019 3,740 17 0.00 105,905
5/12/2019 3,070 16 0.16 86,933
5/13/2019 2,910 16 0.00 82,402
5/14/2019 2,870 16 0.00 81,269
5/15/2019 2,990 16 0.00 84,667
5/16/2019 3,120 16 0.00 88,349
5/17/2019 3,260 16 0.00 92,313
5/18/2019 3,190 16 0.00 90,331
5/19/2019 2,730 16 0.00 77,305
5/20/2019 2,320 16 0.00 65,695
5/21/2019 2,110 16 0.00 59,749
5/22/2019 1,920 16 0.00 54,368
5/23/2019 1,790 16 0.00 50,687
5/24/2019 1,700 15 0.00 48,139
5/25/2019 1,590 15 0.00 45,024
5/26/2019 1,550 15 0.00 43,891
5/27/2019 1,440 15 0.00 40,776
5/28/2019 1,380 15 0.00 39,077
5/29/2019 1,340 15 0.00 37,945
5/30/2019 1,280 15 0.00 36,246
5/31/2019 1,280 15 0.01 36,246
6/1/2019 1,320 15 0.00 37,378
6/2/2019 1,290 15 0.00 36,529
6/3/2019 1,240 15 0.00 35,113
6/4/2019 1,120 15 0.00 31,715
6/5/2019 1,020 15 0.05 28,883
6/6/2019 1,220 15 0.01 34,547
6/7/2019 1,360 15 0.54 38,511
6/8/2019 1,490 15 1.40 42,192
6/9/2019 2,090 16 0.59 59,182
6/10/2019 4,140 17 0.03 117,232
6/11/2019 8,110 18 0.01 229,650
6/12/2019 10,300 19 0.16 291,664
6/13/2019 10,400 19 0.19 294,495
6/14/2019 9,290 18 0.00 263,064
6/15/2019 8,460 18 0.00 239,561
6/16/2019 8,180 18 0.00 231,632
6/17/2019 7,750 18 0.00 219,456
Page 22 of 23 August 2019
APPENDIX B-3
SUMMARY OF FLOW IN CAPE FEAR RIVER AT LOCK #1 NR KELLY, NC
Chemours Fayetteville Works, North Carolina
Geosyntec Consultatns of NC, P.C.
Date
USGS Reported
Average Discharge1
(cfs)
USGS Reported
Average Gage
Height1 (ft)
USGS Reported Total
Precipitation1,2 (inches)
USGS Reported Average
Discharge (L/s)
6/18/2019 7,040 18 0.06 199,351
6/19/2019 6,400 18 0.00 181,228
6/20/2019 4,990 17 0.03 141,301
6/21/2019 3,820 17 0.00 108,170
6/22/2019 3,310 16 0.06 93,729
6/23/2019 3,020 16 0.00 85,517
6/24/2019 2,800 16 0.00 79,287
6/25/2019 3,190 16 0.00 90,331
6/26/2019 3,490 16 0.00 98,826
6/27/2019 2,910 16 0.00 82,402
6/28/2019 2,080 16 0.00 58,899
6/29/2019 1,600 15 0.00 45,307
6/30/2019 1,380 15 0.00 39,077
7/1/2019 1,320 15 0.00 37,378
7/2/2019 1,260 15 0.00 35,679
7/3/2019 1,230 15 1.07 34,830
7/4/2019 1,270 15 0.06 35,962
7/5/2019 2,030 16 0.36 57,483
7/6/2019 2,600 16 0.03 73,624
7/7/2019 2,330 16 0.01 65,978
7/8/2019 1,920 16 1.58 54,368
7/9/2019 2,020 16 2.36 57,200
7/10/2019 2,310 16 0.00 65,412
7/11/2019 2,250 16 0.25 63,713
7/12/2019 2,130 16 0.00 60,315
7/13/2019 3,050 16 2.67 86,366
7/14/2019 3,410 16 0.00 96,560
7/15/2019 2,810 16 0.00 79,570
7/16/2019 2,370 16 0.00 67,111
7/17/2019 1,920 16 0.00 54,368
7/18/2019 1,580 15 0.08 44,741
7/19/2019 1,380 15 0.00 39,077
7/20/2019 1,430 15 0.00 40,493
7/21/2019 1,380 15 0.00 39,077
7/22/2019 1,350 15 0.00 38,228
7/23/2019 1,460 15 0.68 41,343
7/24/2019 1,840 16 0.00 52,103
Notes:
cfs: cubic feet per L/s: Liter per second.
ft: feet.USGS - United States Geological Survey.
1) Measurements are recorded from the USGS flow gauging station at the Lock #1 near Kelly, ID 02105769 (USGS, 2019).
2) The minimum value recorded by a USGS raingage is 0.01 inches. Anything detected below this threshold is recorded as 0 inches.
Page 23 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
1/1/2017 11.6 509
1/2/2017 14.3 626
1/3/2017 14.0 613
1/4/2017 10.8 474
1/5/2017 11.4 500
1/6/2017 16.2 710
1/7/2017 17.5 766
1/8/2017 16.0 702
1/9/2017 15.6 681
1/10/2017 15.7 687
1/11/2017 16.2 710
1/12/2017 15.7 688
1/13/2017 15.6 684
1/14/2017 15.9 696
1/15/2017 15.7 687
1/16/2017 15.8 693
1/17/2017 15.9 696
1/18/2017 15.5 680
1/19/2017 16.6 729
1/20/2017 16.0 699
1/21/2017 15.8 693
1/22/2017 15.0 659
1/23/2017 15.6 685
1/24/2017 16.1 706
1/25/2017 15.6 685
1/26/2017 17.3 758
1/27/2017 14.3 625
1/28/2017 16.1 703
1/29/2017 15.8 694
1/30/2017 16.2 708
1/31/2017 15.5 679
2/1/2017 15.4 674
2/2/2017 16.0 699
2/3/2017 15.5 680
2/4/2017 16.2 712
2/5/2017 15.5 677
2/6/2017 16.0 701
2/7/2017 15.8 693
2/8/2017 14.7 642
Page 1 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
2/9/2017 11.3 495
2/10/2017 11.2 490
2/11/2017 9.6 419
2/12/2017 9.7 425
2/13/2017 10.7 470
2/14/2017 10.4 456
2/15/2017 12.3 539
2/16/2017 11.6 509
2/17/2017 11.0 482
2/18/2017 10.9 477
2/19/2017 10.1 441
2/20/2017 10.0 436
2/21/2017 11.6 510
2/22/2017 9.7 424
2/23/2017 9.9 433
2/24/2017 15.7 686
2/25/2017 17.0 744
2/26/2017 15.9 696
2/27/2017 17.1 749
2/28/2017 17.7 775
3/1/2017 18.2 797
3/2/2017 17.8 780
3/3/2017 16.6 727
3/4/2017 15.9 697
3/5/2017 12.9 564
3/6/2017 12.2 532
3/7/2017 12.4 544
3/8/2017 15.1 661
3/9/2017 12.3 539
3/10/2017 11.2 491
3/11/2017 9.5 417
3/12/2017 10.5 461
3/13/2017 14.6 638
3/14/2017 10.9 477
3/15/2017 12.3 538
3/16/2017 13.6 596
3/17/2017 14.3 626
3/18/2017 13.5 594
3/19/2017 14.1 617
3/20/2017 13.5 591
Page 2 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
3/21/2017 10.6 465
3/22/2017 10.3 450
3/23/2017 10.8 473
3/24/2017 12.0 526
3/25/2017 10.6 464
3/26/2017 12.6 554
3/27/2017 13.5 590
3/28/2017 12.4 542
3/29/2017 10.9 477
3/30/2017 14.8 646
3/31/2017 14.8 650
4/1/2017 11.5 503
4/2/2017 13.1 574
4/3/2017 11.9 523
4/4/2017 10.8 474
4/5/2017 12.8 560
4/6/2017 12.4 542
4/7/2017 12.2 535
4/8/2017 13.4 589
4/9/2017 19.9 873
4/10/2017 20.6 901
4/11/2017 20.5 898
4/12/2017 21.8 954
4/13/2017 20.9 915
4/14/2017 22.2 972
4/15/2017 20.6 904
4/16/2017 20.7 909
4/17/2017 20.5 898
4/18/2017 19.5 854
4/19/2017 18.5 810
4/20/2017 19.9 872
4/21/2017 19.2 840
4/22/2017 19.7 863
4/23/2017 18.0 791
4/24/2017 25.5 1,117
4/25/2017 13.9 609
4/26/2017 10.6 463
4/27/2017 9.9 434
4/28/2017 11.8 519
4/29/2017 11.8 516
Page 3 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
4/30/2017 16.2 709
5/1/2017 17.5 766
5/2/2017 16.4 720
5/3/2017 16.5 723
5/4/2017 18.9 826
5/5/2017 19.1 837
5/6/2017 14.9 655
5/7/2017 15.0 656
5/8/2017 17.0 746
5/9/2017 15.6 684
5/10/2017 17.5 768
5/11/2017 15.9 697
5/12/2017 18.5 810
5/13/2017 14.6 639
5/14/2017 15.7 688
5/15/2017 23.5 1,031
5/16/2017 29.6 1,297
5/17/2017 20.7 909
5/18/2017 22.9 1,005
5/19/2017 22.0 962
5/20/2017 22.6 989
5/21/2017 23.4 1,024
5/22/2017 25.3 1,107
5/23/2017 23.4 1,026
5/24/2017 24.0 1,050
5/25/2017 22.2 972
5/26/2017 21.6 948
5/27/2017 21.9 961
5/28/2017 23.3 1,020
5/29/2017 21.5 942
5/30/2017 22.5 984
5/31/2017 21.7 949
6/1/2017 21.1 924
6/2/2017 22.5 987
6/3/2017 21.8 953
6/4/2017 22.0 965
6/5/2017 26.5 1,160
6/6/2017 22.4 983
6/7/2017 22.1 967
6/8/2017 21.4 938
Page 4 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
6/9/2017 21.6 948
6/10/2017 21.5 941
6/11/2017 22.0 962
6/12/2017 22.7 994
6/13/2017 22.4 983
6/14/2017 22.1 969
6/15/2017 24.3 1,063
6/16/2017 23.8 1,045
6/17/2017 23.8 1,044
6/18/2017 22.9 1,005
6/19/2017 22.9 1,005
6/20/2017 23.9 1,049
6/21/2017 19.0 832
6/22/2017 22.8 1,000
6/23/2017 22.2 973
6/24/2017 26.8 1,172
6/25/2017 21.6 946
6/26/2017 20.6 902
6/27/2017 21.3 934
6/28/2017 19.4 852
6/29/2017 21.0 919
6/30/2017 24.8 1,085
7/1/2017 21.7 949
7/2/2017 22.1 969
7/3/2017 23.3 1,023
7/4/2017 21.8 956
7/5/2017 23.7 1,039
7/6/2017 23.7 1,039
7/7/2017 24.3 1,063
7/8/2017 24.7 1,082
7/9/2017 23.6 1,032
7/10/2017 25.0 1,095
7/11/2017 23.6 1,032
7/12/2017 24.1 1,057
7/13/2017 24.0 1,052
7/14/2017 23.7 1,037
7/15/2017 24.1 1,057
7/16/2017 24.0 1,052
7/17/2017 24.2 1,062
7/18/2017 24.4 1,068
Page 5 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
7/19/2017 24.2 1,060
7/20/2017 24.5 1,073
7/21/2017 24.5 1,071
7/22/2017 25.0 1,096
7/23/2017 23.9 1,046
7/24/2017 26.8 1,175
7/25/2017 22.4 981
7/26/2017 24.5 1,075
7/27/2017 24.8 1,087
7/28/2017 24.5 1,074
7/29/2017 24.0 1,051
7/30/2017 25.2 1,102
7/31/2017 23.8 1,043
8/1/2017 23.5 1,028
8/2/2017 22.1 966
8/3/2017 23.1 1,011
8/4/2017 23.2 1,016
8/5/2017 23.6 1,035
8/6/2017 23.9 1,045
8/7/2017 24.4 1,068
8/8/2017 24.5 1,072
8/9/2017 22.6 991
8/10/2017 23.8 1,044
8/11/2017 24.1 1,056
8/12/2017 23.7 1,039
8/13/2017 27.0 1,181
8/14/2017 23.6 1,034
8/15/2017 23.1 1,012
8/16/2017 25.0 1,097
8/17/2017 25.6 1,121
8/18/2017 25.0 1,097
8/19/2017 24.7 1,081
8/20/2017 26.8 1,174
8/21/2017 24.9 1,089
8/22/2017 26.3 1,154
8/23/2017 26.7 1,169
8/24/2017 26.1 1,144
8/25/2017 25.6 1,123
8/26/2017 25.0 1,096
8/27/2017 25.3 1,109
Page 6 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
8/28/2017 25.0 1,094
8/29/2017 24.6 1,079
8/30/2017 25.0 1,096
8/31/2017 25.1 1,099
9/1/2017 26.5 1,160
9/2/2017 24.4 1,069
9/3/2017 24.8 1,085
9/4/2017 22.7 993
9/5/2017 24.8 1,085
9/6/2017 25.0 1,095
9/7/2017 23.9 1,046
9/8/2017 23.5 1,031
9/9/2017 21.1 926
9/10/2017 21.1 924
9/11/2017 21.8 954
9/12/2017 22.2 974
9/13/2017 21.5 944
9/14/2017 22.4 980
9/15/2017 21.1 925
9/16/2017 21.7 951
9/17/2017 21.2 929
9/18/2017 22.3 976
9/19/2017 21.8 956
9/20/2017 22.4 981
9/21/2017 22.1 970
9/22/2017 20.4 894
9/23/2017 17.7 777
9/24/2017 17.6 772
9/25/2017 16.8 737
9/26/2017 19.7 862
9/27/2017 21.9 958
9/28/2017 22.4 983
9/29/2017 21.6 945
9/30/2017 20.8 909
10/1/2017 21.9 961
10/2/2017 19.1 838
10/3/2017 19.0 834
10/4/2017 21.1 927
10/5/2017 21.3 935
10/6/2017 20.5 897
Page 7 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
10/7/2017 25.1 1,100
10/8/2017 22.0 963
10/9/2017 20.5 897
10/10/2017 20.8 910
10/11/2017 20.6 902
10/12/2017 20.3 889
10/13/2017 15.7 690
10/14/2017 14.7 644
10/15/2017 14.6 639
10/16/2017 16.3 713
10/17/2017 4.6 203
10/18/2017 0.0 0
10/19/2017 0.0 0
10/20/2017 0.0 0
10/21/2017 0.0 0
10/22/2017 0.0 0
10/23/2017 0.7 30
10/24/2017 0.0 0
10/25/2017 0.0 0
10/26/2017 0.0 0
10/27/2017 2.2 98
10/28/2017 3.8 167
10/29/2017 8.9 391
10/30/2017 8.9 388
10/31/2017 9.0 392
11/1/2017 10.3 450
11/2/2017 22.0 963
11/3/2017 27.5 1,205
11/4/2017 28.9 1,264
11/5/2017 28.3 1,242
11/6/2017 29.3 1,285
11/7/2017 27.3 1,197
11/8/2017 20.1 883
11/9/2017 24.7 1,080
11/10/2017 24.7 1,083
11/11/2017 23.4 1,026
11/12/2017 24.5 1,074
11/13/2017 24.5 1,075
11/14/2017 24.4 1,069
11/15/2017 24.1 1,056
Page 8 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
11/16/2017 24.0 1,053
11/17/2017 25.4 1,111
11/18/2017 23.8 1,042
11/19/2017 24.8 1,086
11/20/2017 23.3 1,022
11/21/2017 24.1 1,057
11/22/2017 24.3 1,063
11/23/2017 24.0 1,052
11/24/2017 24.4 1,067
11/25/2017 24.3 1,066
11/26/2017 25.6 1,123
11/27/2017 23.9 1,048
11/28/2017 24.7 1,084
11/29/2017 23.5 1,028
11/30/2017 24.3 1,063
12/1/2017 23.1 1,012
12/2/2017 24.1 1,057
12/3/2017 24.0 1,053
12/4/2017 23.2 1,018
12/5/2017 23.1 1,010
12/6/2017 23.9 1,047
12/7/2017 23.4 1,024
12/8/2017 28.8 1,263
12/9/2017 24.0 1,050
12/10/2017 25.3 1,109
12/11/2017 22.2 974
12/12/2017 23.7 1,037
12/13/2017 23.7 1,040
12/14/2017 23.7 1,039
12/15/2017 23.4 1,023
12/16/2017 24.5 1,072
12/17/2017 24.0 1,052
12/18/2017 24.6 1,076
12/19/2017 24.3 1,066
12/20/2017 25.4 1,111
12/21/2017 12.5 547
12/22/2017 14.2 620
12/23/2017 12.5 547
12/24/2017 13.6 597
12/25/2017 12.3 539
Page 9 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
12/26/2017 12.4 542
12/27/2017 10.7 468
12/28/2017 15.5 677
12/29/2017 13.1 575
12/30/2017 14.0 613
12/31/2017 13.5 590
1/1/2018 15.9 695
1/2/2018 17.4 762
1/3/2018 19.4 851
1/4/2018 19.5 856
1/5/2018 18.1 793
1/6/2018 20.0 876
1/7/2018 18.1 793
1/8/2018 14.2 621
1/9/2018 13.9 607
1/10/2018 16.2 712
1/11/2018 18.6 815
1/12/2018 19.0 834
1/13/2018 19.9 873
1/14/2018 21.2 930
1/15/2018 16.7 730
1/16/2018 17.2 755
1/17/2018 19.0 831
1/18/2018 15.4 674
1/19/2018 17.3 759
1/20/2018 16.8 736
1/21/2018 16.9 739
1/22/2018 17.4 761
1/23/2018 15.3 669
1/24/2018 18.1 793
1/25/2018 20.9 914
1/26/2018 17.4 760
1/27/2018 18.8 825
1/28/2018 20.7 906
1/29/2018 20.4 896
1/30/2018 18.1 793
1/31/2018 17.8 781
2/1/2018 18.6 814
2/2/2018 19.4 849
2/3/2018 18.4 805
Page 10 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
2/4/2018 21.2 928
2/5/2018 18.6 814
2/6/2018 19.1 838
2/7/2018 18.5 811
2/8/2018 16.3 715
2/9/2018 18.7 817
2/10/2018 19.6 858
2/11/2018 19.6 858
2/12/2018 18.8 824
2/13/2018 19.1 836
2/14/2018 19.4 848
2/15/2018 19.3 846
2/16/2018 19.4 849
2/17/2018 19.8 868
2/18/2018 19.5 853
2/19/2018 19.5 854
2/20/2018 18.9 830
2/21/2018 19.3 845
2/22/2018 18.4 808
2/23/2018 11.6 508
2/24/2018 10.8 472
2/25/2018 10.9 479
2/26/2018 10.7 470
2/27/2018 11.0 481
2/28/2018 11.1 486
3/1/2018 12.0 528
3/2/2018 11.2 493
3/3/2018 10.1 441
3/4/2018 11.8 515
3/5/2018 7.9 345
3/6/2018 9.8 427
3/7/2018 9.4 410
3/8/2018 9.3 407
3/9/2018 9.0 396
3/10/2018 9.2 405
3/11/2018 9.7 424
3/12/2018 10.6 462
3/13/2018 9.1 400
3/14/2018 9.0 395
3/15/2018 9.6 421
Page 11 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
3/16/2018 10.2 447
3/17/2018 12.2 536
3/18/2018 13.9 610
3/19/2018 13.1 572
3/20/2018 12.0 527
3/21/2018 12.6 552
3/22/2018 14.1 618
3/23/2018 13.5 593
3/24/2018 12.1 530
3/25/2018 13.3 581
3/26/2018 13.7 601
3/27/2018 12.8 563
3/28/2018 12.6 553
3/29/2018 12.7 554
3/30/2018 14.3 626
3/31/2018 16.2 711
4/1/2018 16.3 715
4/2/2018 17.4 764
4/3/2018 18.6 814
4/4/2018 18.0 788
4/5/2018 18.1 793
4/6/2018 18.8 826
4/7/2018 19.3 846
4/8/2018 15.7 690
4/9/2018 17.9 784
4/10/2018 16.8 735
4/11/2018 16.5 723
4/12/2018 14.8 649
4/13/2018 15.3 672
4/14/2018 18.6 815
4/15/2018 18.6 815
4/16/2018 19.4 848
4/17/2018 18.8 825
4/18/2018 16.4 719
4/19/2018 23.6 1,035
4/20/2018 17.3 756
4/21/2018 21.2 930
4/22/2018 20.4 896
4/23/2018 19.8 867
4/24/2018 16.0 703
Page 12 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
4/25/2018 14.2 620
4/26/2018 12.5 548
4/27/2018 18.4 808
4/28/2018 17.4 760
4/29/2018 17.8 782
4/30/2018 18.1 793
5/1/2018 17.5 767
5/2/2018 19.8 866
5/3/2018 20.5 899
5/4/2018 20.9 917
5/5/2018 21.4 939
5/6/2018 22.3 975
5/7/2018 21.0 919
5/8/2018 20.2 883
5/9/2018 22.9 1,004
5/10/2018 20.8 910
5/11/2018 21.6 948
5/12/2018 21.9 959
5/13/2018 20.0 878
5/14/2018 21.6 948
5/15/2018 20.4 892
5/16/2018 20.1 878
5/17/2018 23.1 1,013
5/18/2018 21.0 919
5/19/2018 20.9 915
5/20/2018 19.4 851
5/21/2018 20.7 905
5/22/2018 20.2 885
5/23/2018 19.4 852
5/24/2018 30.0 1,313
5/25/2018 22.2 973
5/26/2018 23.9 1,046
5/27/2018 22.8 998
5/28/2018 24.2 1,061
5/29/2018 24.1 1,057
5/30/2018 22.7 995
5/31/2018 22.7 994
6/1/2018 23.1 1,014
6/2/2018 22.2 975
6/3/2018 23.0 1,008
Page 13 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
6/4/2018 22.7 993
6/5/2018 22.5 986
6/6/2018 22.0 963
6/7/2018 22.2 972
6/8/2018 23.7 1,037
6/9/2018 22.4 982
6/10/2018 22.7 997
6/11/2018 25.0 1,095
6/12/2018 24.9 1,090
6/13/2018 22.6 988
6/14/2018 23.5 1,029
6/15/2018 22.9 1,005
6/16/2018 22.3 979
6/17/2018 23.6 1,032
6/18/2018 23.5 1,030
6/19/2018 21.7 951
6/20/2018 30.3 1,327
6/21/2018 20.2 884
6/22/2018 26.1 1,142
6/23/2018 25.4 1,113
6/24/2018 25.8 1,130
6/25/2018 26.1 1,145
6/26/2018 29.3 1,285
6/27/2018 26.2 1,147
6/28/2018 26.5 1,161
6/29/2018 28.1 1,231
6/30/2018 28.1 1,232
7/1/2018 28.3 1,239
7/2/2018 26.6 1,165
7/3/2018 25.2 1,105
7/4/2018 26.2 1,150
7/5/2018 27.1 1,186
7/6/2018 26.3 1,151
7/7/2018 26.1 1,142
7/8/2018 25.4 1,114
7/9/2018 27.0 1,182
7/10/2018 26.2 1,146
7/11/2018 26.1 1,141
7/12/2018 26.4 1,158
7/13/2018 25.5 1,118
Page 14 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
7/14/2018 26.8 1,174
7/15/2018 27.7 1,212
7/16/2018 26.0 1,140
7/17/2018 27.3 1,195
7/18/2018 27.0 1,183
7/19/2018 27.3 1,195
7/20/2018 28.7 1,256
7/21/2018 27.8 1,220
7/22/2018 27.2 1,193
7/23/2018 32.4 1,420
7/24/2018 23.3 1,019
7/25/2018 28.3 1,241
7/26/2018 25.4 1,111
7/27/2018 29.4 1,290
7/28/2018 28.6 1,254
7/29/2018 29.0 1,271
7/30/2018 29.0 1,270
7/31/2018 27.7 1,214
8/1/2018 27.7 1,212
8/2/2018 27.5 1,205
8/3/2018 28.3 1,238
8/4/2018 24.4 1,071
8/5/2018 23.2 1,017
8/6/2018 23.7 1,037
8/7/2018 25.9 1,134
8/8/2018 26.5 1,161
8/9/2018 23.0 1,006
8/10/2018 26.4 1,155
8/11/2018 25.7 1,125
8/12/2018 26.7 1,169
8/13/2018 24.6 1,080
8/14/2018 25.9 1,135
8/15/2018 26.2 1,147
8/16/2018 25.1 1,100
8/17/2018 25.3 1,107
8/18/2018 25.0 1,095
8/19/2018 25.2 1,105
8/20/2018 27.0 1,183
8/21/2018 24.6 1,076
8/22/2018 25.8 1,131
Page 15 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
8/23/2018 23.4 1,027
8/24/2018 25.5 1,119
8/25/2018 22.9 1,004
8/26/2018 26.0 1,138
8/27/2018 25.4 1,114
8/28/2018 27.0 1,183
8/29/2018 26.7 1,171
8/30/2018 26.5 1,159
8/31/2018 28.4 1,243
9/1/2018 26.3 1,150
9/2/2018 26.9 1,178
9/3/2018 28.8 1,262
9/4/2018 27.8 1,218
9/5/2018 28.3 1,239
9/6/2018 30.1 1,317
9/7/2018 25.2 1,104
9/8/2018 28.0 1,227
9/9/2018 25.4 1,112
9/10/2018 30.1 1,320
9/11/2018 28.0 1,225
9/12/2018 15.5 681
9/13/2018 14.1 618
9/14/2018 24.1 1,057
9/15/2018 32.0 1,403
9/16/2018 48.3 2,117
9/17/2018 11.4 500
9/18/2018 12.7 557
9/19/2018 18.4 804
9/20/2018 18.6 815
9/21/2018 18.1 792
9/22/2018 17.9 786
9/23/2018 23.4 1,026
9/24/2018 22.9 1,005
9/25/2018 22.7 993
9/26/2018 22.9 1,002
9/27/2018 25.9 1,133
9/28/2018 23.3 1,020
9/29/2018 24.8 1,086
9/30/2018 23.8 1,043
10/1/2018 23.3 1,021
Page 16 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
10/2/2018 24.6 1,078
10/3/2018 22.9 1,003
10/4/2018 22.9 1,003
10/5/2018 23.3 1,022
10/6/2018 24.7 1,080
10/7/2018 24.4 1,070
10/8/2018 22.5 984
10/9/2018 18.2 795
10/10/2018 16.6 728
10/11/2018 18.5 810
10/12/2018 3.0 133
10/13/2018 0.0 0
10/14/2018 0.0 0
10/15/2018 0.0 0
10/16/2018 0.0 0
10/17/2018 0.0 0
10/18/2018 0.0 0
10/19/2018 0.0 0
10/20/2018 0.0 0
10/21/2018 0.0 0
10/22/2018 21.6 946
10/23/2018 21.6 946
10/24/2018 21.6 946
10/25/2018 21.6 946
10/26/2018 21.6 946
10/27/2018 21.6 946
10/28/2018 21.6 946
10/29/2018 21.6 946
10/30/2018 21.6 946
10/31/2018 19.0 832
11/1/2018 18.3 803
11/2/2018 19.8 869
11/3/2018 19.3 845
11/4/2018 19.5 854
11/5/2018 19.7 863
11/6/2018 20.8 912
11/7/2018 19.1 835
11/8/2018 22.0 963
11/9/2018 21.8 953
11/10/2018 21.0 921
Page 17 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
11/11/2018 22.2 972
11/12/2018 30.6 1,342
11/13/2018 22.5 986
11/14/2018 22.7 995
11/15/2018 21.5 944
11/16/2018 22.1 968
11/17/2018 21.7 949
11/18/2018 21.0 919
11/19/2018 21.2 931
11/20/2018 21.6 948
11/21/2018 21.2 928
11/22/2018 21.7 951
11/23/2018 22.1 968
11/24/2018 23.9 1,047
11/25/2018 19.3 844
11/26/2018 19.3 845
11/27/2018 19.4 851
11/28/2018 19.7 865
11/29/2018 19.9 872
11/30/2018 20.1 882
12/1/2018 22.4 981
12/2/2018 19.9 870
12/3/2018 18.4 807
12/4/2018 19.0 831
12/5/2018 19.2 840
12/6/2018 19.2 842
12/7/2018 19.7 862
12/8/2018 21.0 918
12/9/2018 23.4 1,026
12/10/2018 20.4 893
12/11/2018 20.1 881
12/12/2018 19.0 834
12/13/2018 19.7 862
12/14/2018 26.1 1,144
12/15/2018 20.7 906
12/16/2018 20.2 883
12/17/2018 21.0 921
12/18/2018 14.9 653
12/19/2018 17.5 766
12/20/2018 19.3 847
Page 18 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
12/21/2018 17.8 779
12/22/2018 18.4 807
12/23/2018 18.9 829
12/24/2018 17.3 759
12/25/2018 18.4 805
12/26/2018 18.4 804
12/27/2018 17.7 778
12/28/2018 18.7 821
12/29/2018 18.9 826
12/30/2018 16.8 738
12/31/2018 17.8 779
1/1/2019 18.3 802
1/2/2019 18.1 793
1/3/2019 18.5 811
1/4/2019 20.8 912
1/5/2019 18.5 811
1/6/2019 18.4 808
1/7/2019 18.7 819
1/8/2019 18.9 829
1/9/2019 18.8 823
1/10/2019 18.6 815
1/11/2019 18.2 795
1/12/2019 19.6 860
1/13/2019 19.1 838
1/14/2019 19.5 855
1/15/2019 18.6 815
1/16/2019 19.0 831
1/17/2019 19.7 863
1/18/2019 19.6 857
1/19/2019 20.2 885
1/20/2019 20.1 880
1/21/2019 20.1 880
1/22/2019 18.7 819
1/23/2019 21.8 953
1/24/2019 17.4 761
1/25/2019 18.9 826
1/26/2019 19.5 854
1/27/2019 18.5 811
1/28/2019 19.0 832
1/29/2019 18.8 825
Page 19 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
1/30/2019 18.8 823
1/31/2019 12.8 560
2/1/2019 25.1 1,099
2/2/2019 19.2 842
2/3/2019 19.1 836
2/4/2019 18.7 821
2/5/2019 18.4 805
2/6/2019 20.5 899
2/7/2019 17.6 773
2/8/2019 19.2 843
2/9/2019 19.3 846
2/10/2019 19.6 858
2/11/2019 19.2 839
2/12/2019 21.6 947
2/13/2019 21.3 933
2/14/2019 22.3 976
2/15/2019 23.5 1,031
2/16/2019 22.2 973
2/17/2019 23.2 1,015
2/18/2019 22.0 962
2/19/2019 22.5 987
2/20/2019 22.8 1,001
2/21/2019 23.8 1,043
2/22/2019 23.7 1,037
2/23/2019 25.0 1,094
2/24/2019 20.1 883
2/25/2019 23.6 1,034
2/26/2019 22.9 1,005
2/27/2019 23.0 1,010
2/28/2019 22.8 999
3/1/2019 24.1 1,057
3/2/2019 23.1 1,011
3/3/2019 25.7 1,125
3/4/2019 23.8 1,042
3/5/2019 22.8 999
3/6/2019 23.9 1,047
3/7/2019 22.8 1,000
3/8/2019 24.0 1,049
3/9/2019 22.2 974
3/10/2019 23.5 1,031
Page 20 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
3/11/2019 23.3 1,021
3/12/2019 22.9 1,004
3/13/2019 22.7 993
3/14/2019 23.0 1,006
3/15/2019 23.9 1,045
3/16/2019 23.0 1,006
3/17/2019 22.7 994
3/18/2019 22.6 990
3/19/2019 22.7 995
3/20/2019 22.0 964
3/21/2019 22.1 969
3/22/2019 21.0 921
3/23/2019 22.9 1,004
3/24/2019 20.9 917
3/25/2019 21.7 953
3/26/2019 21.3 935
3/27/2019 21.3 933
3/28/2019 21.9 961
3/29/2019 22.0 964
3/30/2019 21.8 954
3/31/2019 23.1 1,014
4/1/2019 19.4 848
4/2/2019 22.9 1,005
4/3/2019 21.2 927
4/4/2019 22.7 994
4/5/2019 23.9 1,046
4/6/2019 22.2 972
4/7/2019 20.6 904
4/8/2019 21.2 929
4/9/2019 21.1 925
4/10/2019 22.2 971
4/11/2019 22.5 985
4/12/2019 23.2 1,016
4/13/2019 23.0 1,009
4/14/2019 22.7 996
4/15/2019 21.9 962
4/16/2019 22.0 964
4/17/2019 22.3 978
4/18/2019 21.6 945
4/19/2019 22.7 994
Page 21 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
4/20/2019 22.7 994
4/21/2019 21.8 955
4/22/2019 21.2 930
4/23/2019 21.6 947
4/24/2019 21.1 922
4/25/2019 21.1 926
4/26/2019 22.5 984
4/27/2019 20.5 899
4/28/2019 21.0 921
4/29/2019 20.7 907
4/30/2019 22.4 983
5/1/2019 22.6 989
5/2/2019 21.4 936
5/3/2019 21.9 958
5/4/2019 24.4 1,070
5/5/2019 21.4 939
5/6/2019 21.9 961
5/7/2019 22.0 964
5/8/2019 23.4 1,026
5/9/2019 22.4 979
5/10/2019 23.8 1,044
5/11/2019 22.3 978
5/12/2019 23.1 1,014
5/13/2019 16.8 735
5/14/2019 23.6 1,034
5/15/2019 20.7 905
5/16/2019 20.8 913
5/17/2019 22.2 971
5/18/2019 21.3 934
5/19/2019 23.0 1,006
5/20/2019 22.2 971
5/21/2019 23.6 1,034
5/22/2019 23.4 1,027
5/23/2019 24.4 1,071
5/24/2019 24.5 1,076
5/25/2019 25.1 1,098
5/26/2019 25.2 1,105
5/27/2019 25.3 1,107
5/28/2019 24.7 1,082
5/29/2019 25.9 1,134
Page 22 of 23 August 2019
APPENDIX B-4
SUMMARY OF OUTFALL 002 DAILY DISCHARGE RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
Date Outfall 002 Flow
(MGD)*
Outfall 002 Flow
(L/s)
5/30/2019 27.4 1,200
5/31/2019 27.0 1,182
6/1/2019 25.3 1,108
6/2/2019 27.0 1,181
6/3/2019 26.9 1,177
6/4/2019 26.0 1,139
6/5/2019 27.7 1,214
6/6/2019 27.2 1,192
6/7/2019 26.4 1,155
6/8/2019 26.2 1,150
6/9/2019 33.5 1,466
6/10/2019 28.9 1,267
6/11/2019 28.9 1,267
6/12/2019 26.4 1,155
6/13/2019 25.1 1,099
6/14/2019 23.8 1,044
6/15/2019 24.2 1,059
6/16/2019 24.3 1,064
6/17/2019 24.0 1,053
6/18/2019 24.3 1,065
6/19/2019 24.3 1,063
6/20/2019 23.1 1,010
6/21/2019 24.3 1,064
6/22/2019 24.2 1,060
6/23/2019 23.6 1,035
6/24/2019 24.1 1,057
6/25/2019 23.2 1,017
6/26/2019 23.8 1,044
6/27/2019 24.2 1,061
6/28/2019 24.2 1,061
6/29/2019 23.8 1,043
6/30/2019 23.3 1,022
Notes:
1) *Data provided by Chemours Fayetteville Works.
3) L/s: Liter per second
2) MGD: Millions of gallons per day.
Page 23 of 23 August 2019

Appendix C – Direct Aerial Deposition 1 August 2019
APPENDIX C
SUPPORTING CALCULATIONS – DIRECT AERIAL DEPOSITION ON CAPE FEAR RIVER

Appendix C – Direct Aerial Deposition 2 August 2019
INTRODUCTION AND OBJECTIVE
Nine potential pathways (Table 1) were identified as potentially contributing to observed Cape
Fear River per- and polyfluoroalkyl substances (PFAS) concentrations. These pathways include
direct PFAS aerial deposition to the Cape Fear River. This pathway was identified as Transport
Pathway Number 3 in the PFAS mass loading design (Section 4) of the Chemours Fayetteville
Works Cape Fear River PFAS Mass Loading Model Assessment and Paragraph 11.1
Characterization of PFAS at Intakes (Geosyntec, 2019). The mass loading from direct aerial
deposition of PFAS to the Cape Fear River was estimated using air deposition modeling results
for HFPO-DA (ERM, 2018).
The objective of the supporting calculations presented in this appendix is to estimate aerial
deposited PFAS directly on the Cape Fear River.
APPROACH
HFPO-DA mass loading directly to the Cape Fear River was first estimated using the reported aerial
extent and deposition contours modeled for October 2018 (ERM, 2018). As depicted in (Table C-1), the
HFPO-DA air loading data (ug/m2) provided from ERM (2018) was used to calculate the net hourly
deposition rate (ng/m2/hr) using the following equation: 𝑁𝑁𝑁𝑁𝑁𝑁 ℎ𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜𝑜 𝑑𝑑𝑁𝑁𝑑𝑑𝑜𝑜𝑑𝑑𝑑𝑑𝑁𝑁𝑑𝑑𝑜𝑜𝑑𝑑 𝑜𝑜𝑟𝑟𝑁𝑁𝑁𝑁= 𝐴𝐴𝑑𝑑𝑜𝑜 𝑜𝑜𝑜𝑜𝑟𝑟𝑑𝑑𝑑𝑑𝑑𝑑𝑙𝑙𝑇𝑇𝑑𝑑𝑇𝑇𝑁𝑁
Depositional area along the river was calculated using available data for river width and computed
river lengths where deposition contours were modeled. Eighteen (18) sections (Figure C-1)
provided from FEMA (2007) were selected along the Cape Fear River to measure the average river
width (m). Cross section width calculations are shown in Table C-2. As depicted in Figures C-2,
C-3, C-4, C-5, and C-6, sections along the Cape Fear River with HFPO-DA concentrations
contours ranging from 40 to 640 ug/m2 were selected, and the length of the Cape Fear River along
each of the sections was measured. Section lengths and river widths were used to calculate section
areas (m2) (Table C-3). Start and end deposition rates (ng/m2/hr) for each section along the Cape
Fear River were estimated based on the deposition contours and corresponding net hourly
deposition rate (Table C-1); a combined deposition rate for each section was calculated as the
average of the start and end deposition rates. River velocity (m/hr) was estimated from measured
flow rates and the calculated river cross sectional area. Section lengths were used to calculate
HFPO-DA travel time based on the river velocity (Table C-3). Finally, as depicted in Table C-3,
combined deposition rate (ng/m2/hr), section area (m2), and travel time (hr) were used to calculate
mass HFPO-DA deposited (ng) as follows: 𝑀𝑀𝑟𝑟𝑑𝑑𝑑𝑑 𝐻𝐻𝐻𝐻𝐻𝐻𝐻𝐻−𝐷𝐷𝐴𝐴 𝑑𝑑𝑁𝑁𝑑𝑑𝑜𝑜𝑑𝑑𝑑𝑑𝑁𝑁𝑁𝑁𝑑𝑑= 𝐶𝐶𝑜𝑜𝑇𝑇𝐶𝐶𝑑𝑑𝑑𝑑𝑁𝑁𝑑𝑑 𝑑𝑑𝑁𝑁𝑑𝑑𝑜𝑜𝑑𝑑𝑑𝑑𝑁𝑁𝑑𝑑𝑜𝑜𝑑𝑑 𝑜𝑜𝑟𝑟𝑁𝑁𝑁𝑁 𝑥𝑥 𝑆𝑆𝑁𝑁𝑆𝑆𝑁𝑁𝑑𝑑𝑜𝑜𝑑𝑑 𝑟𝑟𝑜𝑜𝑁𝑁𝑟𝑟 𝑥𝑥 𝑇𝑇𝑜𝑜𝑟𝑟𝑇𝑇𝑁𝑁𝑜𝑜 𝑁𝑁𝑑𝑑𝑇𝑇𝑁𝑁
Residential well data from six locations in the Granular Activated Carbon Pilot Well testing program (Chemours, 2019) were used to build a relationship between HFPO-DA and other PFAS compounds since modeled aerial deposition results are only available for HFPO-DA. The
average ratios of measured HFPO-DA to other compounds across the six locations were used to

Appendix C – Direct Aerial Deposition 3 August 2019
estimate mass loading of other PFAS compounds. This relationship is provided in Table E-3 of Appendix E.

Appendix C – Direct Aerial Deposition 4 August 2019
REFERENCES
Chemours, 2019. Residential Well Carbon Pilot Testing Data. Available at:
https://www.chemours.com/Fayetteville-Works/en-us/c3-dimer-acid/compliance-testing/
ERM, 2018. Modeling Report: HFPO-DA Atmospheric Deposition and Screening Groundwater
Effects. 27 April 2018.
Federal Emergency Management Agency (FEMA), 2007. "A Report of Flood Hazards in Bladen
County, North Carolina and Incorporated Areas." (2007) Flood Insurance Study, Federal
Emergency Management Agency. North Carolina Flood Risk Information System Engineering
Model. Cape Fear River ADJ. HEC-RAS 5.0.7.

Appendix C – Direct Aerial Deposition 1 August 2019
APPENDIX C
TABLES
TABLE C-1
NET HOURLY HFPO-DA DEPOSITION RATE
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
HFPO-DA Air Loading1
(µg/m2)
HFPO-DA Air Loading
(ng/m2)
Time
(year)
Time
(hour)
HFPO-DA Net Hourly Deposition Rate
(ng/m2/hr)
40 40,000 1 8,760 4.6
80 80,000 1 8,760 9.1
160 160,000 1 8,760 18.3
320 320,000 1 8,760 36.5
640 640,000 1 8,760 73.1
Notes:
2. Abbreviations
HFPO-DA: Hexafluoropropylene oxide dimer acid; or dimer acid.
ug/m2: micrograms per meter square.
ng /L: nanograms per liter.
ng/m2/hr: nanograms per meter square per hour.
1. HFPO-DA model values are from ERM (2018). Modeling Report: HFPO-DA Atmospheric Deposition and Screening Groundwater Effects.
27 April 2018.
Page 1 of 1 August 2019
TABLE C-2
ESTIMATION OF AVERAGE RIVER WIDTH
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
Cross section ID*Model point ID**Easting
(ft NAD83)
Northing
(ft NAD83)
River Depth
(ft NAVD88)
Distance
(ft)
Cross Section Width
(m)
0 2,052,368 399,949 38.75 0
1 2,052,366 399,949 38.22 2
2 2,052,334 399,946 28.90 34
3 2,052,254 399,938 7.90 114
4 2,052,155 399,928 7.90 213
5 2,052,095 399,922 28.90 273
6 2,052,093 399,922 31.58 275
18 2,053,460 394,655 29.54 0
19 2,053,436 394,649 27.24 24
20 2,053,281 394,613 23.00 179
21 2,053,277 394,612 22.15 183
22 2,053,180 394,590 1.00 280
23 2,053,079 394,566 1.00 381
24 2,052,977 394,543 23.00 483
25 2,052,949 394,536 28.11 512
26 2,052,924 394,531 30.19 536
7 2,053,113 396,901 39.02 0
8 2,053,070 396,895 28.07 43
9 2,052,990 396,886 7.07 122
10 2,052,891 396,874 7.07 222
11 2,052,831 396,867 28.07 281
12 2,052,815 396,865 36.27 298
21 2,053,373 393,937 29.14 0
22 2,053,349 393,931 21.75 24
23 2,053,271 393,913 0.75 102
24 2,053,174 393,891 0.75 200
25 2,053,115 393,877 21.75 258
26 2,053,081 393,869 33.29 292
13 2,053,209 394,897 26.00 0
14 2,053,130 394,878 4.59 80
15 2,053,032 394,854 4.59 177
16 2,052,974 394,840 26.00 235
17 2,052,961 394,837 36.39 248
31 2,053,769 390,652 22.07 0
32 2,053,729 390,645 1.07 40
33 2,053,643 390,630 1.07 126
34 2,053,602 390,623 22.07 167
35 2,053,572 390,618 25.37 197
27 2,053,560 392,482 0.75 0
28 2,053,430 392,455 0.75 129
29 2,053,370 392,443 21.75 190
30 2,053,322 392,433 45.09 238
1271 2,054,059 387,249 50.87 0
1272 2,054,022 387,215 39.63 37
1273 2,053,995 387,190 22.50 65
1274 2,053,946 387,145 -0.50 113
1275 2,053,861 387,067 -0.50 199
1276 2,053,812 387,023 22.50 247
1277 2,053,801 387,012 38.10 258
1278 2,053,727 386,945 72.26 332
1193 2,053,950 388,876 37.23 0
1194 2,053,902 388,874 21.86 49
1195 2,053,843 388,871 0.86 107
1196 2,053,717 388,866 0.86 233
1197 2,053,659 388,864 21.86 291
1198 2,053,650 388,863 30.55 300
1199 2,053,600 388,861 46.74 350
1271 2,054,059 387,249 50.87 0
1272 2,054,022 387,215 39.63 37
1273 2,053,995 387,190 22.50 65
1274 2,053,946 387,145 -0.50 113
1275 2,053,861 387,067 -0.50 199
1276 2,053,812 387,023 22.50 247
1277 2,053,801 387,012 38.10 258
1278 2,053,727 386,945 72.26 332
1498 2,057,643 382,269 37.28 0
1499 2,057,610 382,246 21.69 34
1500 2,057,556 382,208 -1.31 87
1501 2,057,461 382,141 -1.31 182
1502 2,057,408 382,103 21.69 236
1503 2,057,398 382,096 23.87 245
1504 2,057,358 382,067 34.27 286
612082
606667
608468
616535
613542
610240
84
163
91
89
76***
60***
606667
600052
619506
614224
614517
72
101
107
101
87
Page 1 of 2 August 2019
TABLE C-2
ESTIMATION OF AVERAGE RIVER WIDTH
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
Cross section ID*Model point ID**Easting
(ft NAD83)
Northing
(ft NAD83)
River Depth
(ft NAVD88)
Distance
(ft)
Cross Section Width
(m)
1331 2,055,879 386,154 41.88 0
1332 2,055,812 386,120 21.60 66
1333 2,055,753 386,090 -1.40 126
1334 2,055,647 386,037 -1.40 232
1335 2,055,588 386,007 21.60 291
1336 2,055,566 385,996 32.19 312
1565 2,058,901 380,593 36.02 0
1566 2,058,830 380,549 22.16 71
1567 2,058,774 380,515 -0.84 127
1568 2,058,675 380,453 -0.84 225
1569 2,058,619 380,418 22.16 281
1570 2,058,518 380,356 44.33 382
1406 2,056,453 383,857 38.32 0
1407 2,056,356 383,798 22.26 97
1408 2,056,301 383,763 -0.74 152
1409 2,056,202 383,702 -0.74 251
1410 2,056,146 383,667 22.26 307
1411 2,056,113 383,647 32.30 340
1717 2,060,560 377,186 40.59 0
1718 2,060,482 377,157 21.78 78
1719 2,060,421 377,134 -1.22 140
1720 2,060,312 377,094 -1.22 249
1721 2,060,250 377,071 21.78 310
1722 2,060,232 377,065 37.79 328
1644 2,059,549 379,003 30.99 0
1645 2,059,534 378,996 21.71 15
1646 2,059,474 378,970 -1.29 75
1647 2,059,368 378,923 -1.29 181
1648 2,059,308 378,896 21.71 241
1649 2,059,275 378,881 36.48 274
2042 2,061,270 371,304 30.59 0
2043 2,061,246 371,290 20.10 24
2044 2,061,179 371,252 -2.90 91
2045 2,061,092 371,203 -2.90 178
2046 2,061,042 371,174 20.10 228
2047 2,060,966 371,131 42.37 305
1825 2,060,295 374,663 23.04 0
1826 2,060,270 374,661 20.21 24
1827 2,060,201 374,658 -2.79 93
1828 2,060,079 374,653 -2.79 215
1829 2,060,010 374,650 20.21 284
1830 2,059,995 374,649 35.89 300
1931 2,060,424 373,459 40.67 0
1932 2,060,378 373,442 23.21 47
1933 2,060,372 373,439 20.40 52
1934 2,060,311 373,416 -2.60 114
1935 2,060,202 373,376 -2.60 223
1936 2,060,140 373,353 20.40 284
1937 2,060,097 373,336 31.19 328
99
94
97
Notes:
*Cross sections locations are shown in Figure C-1.
**Model point ID: are locations with northing, easting, and river depths provided in the HEC-RAS model.
***Excluded from average, median and geomean river cross section width calculation due to model points not clearly visible.
1. Data provided from: "A Report of Flood Hazards in Bladen County, North Carolina and Incorporated Areas." RiverADJ. HEC-RAS 5.0.7.
(2007) Flood Insurance Study, Federal Emergency Management Agency. North Carolina Flood Risk Information System Engineering Model.
Cape Fear RiverADJ. HEC-RAS 5.0.7.
2. The horizontal datum is North American Datum 1983 projected into North Carolina East State Plane (3200).
3. The vertical datum is North American Datum 1988 projected into North Carolina East State Plane (3200).
4. Abbreviations
ft: feet
m: meter
***Geomean River Cross Section Width (m)=
***Average River Cross Section Width (m)=
***Median River Cross Section Width (m)=
591595
590322
602061
594185
596259
587968
604474
597968
100
116
104
100
84
93
91
95
Page 2 of 2 August 2019
TABLE C-3
CALCULATION OF HFPO-DA DEPOSITED MASS AND MASS FLUX
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
Section
Depositon Rate
at Section Start
(µg/m2/yr)
Depositon Rate at
Section End
(µg/m2/yr)
Start Deposition Rate**
(ng/m2/hr)
End Deposition Rate**
(ng/m2/hr)
Combined Deposition Rate
(ng/m2/hr)
Average River Width
(m)
Section Area
(m2)
Estimated River
Velocity***
(ft/s)
Estimated
River Velocity
(m/hr)
Estimated
Travel Time
(hr)
Calculated Mass
Deposited
(ng)
Calculated
Mass Loading
(ng/s)
Center 160 160 18 18 18 99 89,028 0.2 219 4.1 6,694,345 452
Up River 160 80 18 9 14 99 48,300 0.2 219 2.2 1,477,776 184
Up River 80 40 9 5 7 99 89,570 0.2 219 4.1 2,541,053 170
Down River 160 80 18 9 14 99 57,813 0.2 219 2.7 2,117,225 220
Down River 80 40 9 5 7 99 55,672 0.2 219 2.6 981,677 106
Total 1,132
Notes:
*River cross sections are shown in Figures C-2 through C-6
**Based on model deposition rate, Table C-1, Appendix C
***River velocity is calculated from data from May 2019, Table B-2, Appendix B
1. Abbreviations
HFPO-DA: Hexafluoropropylene oxide dimer acid; or dimer acid
µg/m2/yr: micrograms per meter square per year
ng/m2/hr: nanograms per meter square per hour
m: meter
m2: meter square
ft/s: feet per second
hr: hours
ng/s: nanograms per second
Page 1 of 1 August 2019

Appendix C – Direct Aerial Deposition 1 August 2019
APPENDIX C
FIGURES
591595
616535
619506
602061604474
608468
587968614517
590322600052596259
594185597968610240606667612082
613542
614224
Cape Fear River Cross Sections Locations
Chemours Fayetteville Works, North Carolina
Figure
C-1
Notes:1. Cape Fear River cross section locations obtained from "A Report of Flood Hazards in Bladen County, North Carolina and Incorporated Areas." (2007) Flood Insurance Study, Federal Emergency Management Agency. North Carolina Flood Risk Information System Engineering Model. Cape Fear RiverADJ. HEC-RAS 5.0.7.2. Cross sections used for calculation of average river widths for calculation of aerial mass loading.Raleigh, NC
1 0 10.5 Miles
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Legend
Cross Section
Length (m): 903.00
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS,AeroGRID, IGN, and the GIS User Community
Measurement of Cape Fear River Length at Center Section
Chemours Fayetteville Works, North Carolina
Figure
C-2
Notes:HFPO-DA - Hexafluoropropylene oxide dimer acid; or dimer acid; or GenX
µg / m2/yr - micrograms per square meter per year
HFPO-DA deposition model contours for October 2018 from ERM, 2018, Modeling Report: HFPO-DA Atmospheric Deposition and Screening Groundwater Effects. 27 April 2018.
Raleigh, NC
1 0 10.5 Miles
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Legend
Site Boundary
Modeled Deposition Contours,October 2018 Scenario
40 µg/m2/yr
80 µg/m2/yr
160 µg/m2/yr
320 µg/m2/yr
640 µg/m2/yr
Length (m): 489.90
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS,AeroGRID, IGN, and the GIS User Community
Measurement of Cape Fear River Length at Up-River Section 1
Chemours Fayetteville Works, North Carolina
Figure
C-3
Notes:HFPO-DA - Hexafluoropropylene oxide dimer acid; or dimer acid; or GenX
µg /m2/yr - micrograms per square meter per year
HFPO-DA deposition model contours for October 2018 from ERM, 2018, Modeling Report: HFPO-DA Atmospheric Deposition and Screening Groundwater Effects. 27 April 2018.
Raleigh, NC
1 0 10.5 Miles
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Legend
Site Boundary
Modeled Deposition Contours, October 2018 Scenario
40 µg/m2/yr
80 µg/m2/yr
160 µg/m2/yr
320 µg/m2/yr
640 µg/m2/yr
Length (m): 908.05
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS,AeroGRID, IGN, and the GIS User Community
Measurement of Cape Fear River Length at Up-River Section 2
Chemours Fayetteville Works, North Carolina
Figure
C-4
Notes:HFPO-DA - Hexafluoropropylene oxide dimer acid; or dimer acid; or GenX
µg / m2/yr - micrograms per square meter per year
HFPO-DA deposition model contours for October 2018 from ERM, 2018, Modeling Report: HFPO-DA Atmospheric Deposition and Screening Groundwater Effects. 27 April 2018.
Raleigh, NC
1 0 10.5 Miles
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Legend
Site Boundary
Modeled Deposition Contours, October 2018 Scenario
40 µg/m2/yr
80 µg/m2/yr
160 µg/m2/yr
320 µg/m2/yr
640 µg/m2/yr
Length (m): 586.39
Measurement of Cape Fear River Length at Down-River Section 1
Chemours Fayetteville Works, North Carolina
Figure
C-5
Notes:HFPO-DA - Hexafluoropropylene oxide dimer acid; or dimer acid; or GenX
µg /m2/yr - micrograms per square meter per year
HFPO-DA deposition model contours for October 2018 from ERM, 2018, Modeling Report: HFPO-DA Atmospheric Deposition and Screening Groundwater Effects. 27 April 2018.
Raleigh, NC
1 0 10.5 Miles
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Legend
Site Boundary
Modeled Deposition Contours, October 2018 Scenario
40 µg/m2/yr
80 µg/m2/yr
160 µg/m2/yr
320 µg/m2/yr
640 µg/m2/yr
Length (m): 564.68
Measurement of Cape Fear River Length at Down-River Section 2
Chemours Fayetteville Works, North Carolina
Figure
C-6
Notes:HFPO-DA - Hexafluoropropylene oxide dimer acid; or dimer acid; or GenX
µg /m2/yr - micrograms per square meter per year
HFPO-DA deposition model contours for October 2018 from ERM, 2018, Modeling Report: HFPO-DA Atmospheric Deposition and Screening Groundwater Effects. 27 April 2018.
Raleigh, NC
1 0 10.5 Miles
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Legend
Site Boundary
Modeled Deposition Contours, October 2018 Scenario
40 µg/m2/yr
80 µg/m2/yr
160 µg/m2/yr
320 µg/m2/yr
640 µg/m2/yr

Appendix D – Onsite Groundwater Flow 1 August 2019
APPENDIX D
SUPPORTING CALCULATIONS - ONSITE GROUNDWATER FLOW ESTIMATE

Appendix D – Onsite Groundwater Flow 2 August 2019
INTRODUCTION AND OBJECTIVE
Based on the current understanding of the conceptual site model, the Black Creek Aquifer is the
primary hydrogeologic unit that is potentially in hydraulic connection with the Cape Fear River.
The Cape Fear River stage appears to typically be lower than the top of the Black Creek Aquifer,
except during peak rainfall or flooding, indicating that the Cape Fear River is a discharge boundary
for the aquifer. Onsite groundwater from the Black Creek Aquifer discharging to the Cape Fear
River is therefore a potential pathway for per- and polyfluoroalkyl substances (PFAS) mass
loading to the Cape Fear River. This pathway was identified as Transport Pathway Number 6 in
the PFAS mass loading design (Section 4) of the Chemours Fayetteville Works Cape Fear River
PFAS Mass Loading Model Assessment and Paragraph 11.1 Characterization of PFAS at Intakes
(Geosyntec, 2019). The objective of the supporting calculations presented in this appendix is to
estimate PFAS mass loading from onsite groundwater discharge through a forward assessment
based on Darcy’s Law using available hydrogeological data as described below.
APPROACH
The PFAS mass loading from onsite groundwater discharge was estimated using groundwater
concentration data from the five LTW wells located along the Cape Fear River bank and estimated
volumetric groundwater discharge. Groundwater samples from the five LTW wells were collected
in July-November 2018, as part of the Post Hurricane Florence PFAS Characterization Report
(Geosyntec, 2019) and for other sampling programs implemented since June 2017. PFAS
analytical results for these groundwater samples are presented in Appendix A.
Volumetric groundwater discharge was estimated using Darcy’s Law: 𝑄𝑄=𝐾𝐾𝐾𝐾𝐾𝐾
where Q, the volumetric discharge [L3T-1], is the groundwater discharge being estimated;
K, the hydraulic conductivity of the aquifer [LT-1];
i, the hydraulic gradient [LL-1]; and,
A, the cross-sectional area of discharge from the Black Creek Aquifer into the Cape Fear
River [L2].
The hydraulic gradient is calculated as: 𝐾𝐾= (𝐿𝐿𝐿𝐿𝐿𝐿 𝐿𝐿𝑊𝑊𝑊𝑊𝑊𝑊𝑊𝑊 𝐿𝐿𝑊𝑊𝐿𝐿𝑊𝑊𝐿𝐿 𝐸𝐸𝐿𝐿𝑊𝑊𝐿𝐿𝑊𝑊𝑊𝑊𝐾𝐾𝐸𝐸𝐸𝐸−𝐶𝐶𝑊𝑊𝐶𝐶𝑊𝑊 𝐹𝐹𝑊𝑊𝑊𝑊𝑊𝑊 𝑅𝑅𝐾𝐾𝐿𝐿𝑊𝑊𝑊𝑊 𝑆𝑆𝑊𝑊𝑊𝑊𝑆𝑆𝑊𝑊 𝐸𝐸𝐿𝐿𝑊𝑊𝐿𝐿𝑊𝑊𝑊𝑊𝐾𝐾𝐸𝐸𝐸𝐸)𝐸𝐸𝐸𝐸𝑊𝑊𝐾𝐾𝐸𝐸𝑊𝑊𝑊𝑊𝑊𝑊𝐸𝐸 𝐸𝐸𝐾𝐾𝐸𝐸𝑊𝑊𝑊𝑊𝐸𝐸𝑑𝑑𝑊𝑊 𝑓𝑓𝑊𝑊𝐸𝐸𝐸𝐸 𝐿𝐿𝐿𝐿𝐿𝐿 𝑤𝑤𝑊𝑊𝐿𝐿𝐿𝐿 𝑊𝑊𝐸𝐸 𝑊𝑊𝐾𝐾𝐿𝐿𝑊𝑊𝑊𝑊
Available LTW water level elevations measured in April 2014, September 2015 and June 2019
along with corresponding Cape Fear River stage elevations measured at the USGS flow gauging
station located at the W.O. Huske Dam, ID (USGS# 02105500; USGS, 2019), approximately 0.5
river miles downstream of the Site (Appendix B) were used to compute hydraulic gradients (Table
D-1). Summary statistics for calculated gradients from all five LTW wells indicate gradients vary
between 0.045 to 0.083 feet/feet (Table D-1). This range in computed gradients from all LTW

Appendix D – Onsite Groundwater Flow 3 August 2019
wells were compared with computed gradients at LTW-05 for the entire year of 2018 to account
for any seasonal variations (Figure D-1). This comparison shows that calculated gradients from
all five LTW wells used in this calculation is a conservative measure. Summary statistics for
calculated gradients from all five LTW wells were used in computing minimum, 1st quartile,
median, 3rd quartile and maximum volumetric groundwater discharge.
The hydraulic conductivity of the Black Creek aquifer is selected from literature values based on
the observed soil lithologies described for the LTW wells (Table D-2; Freeze and Cherry, 1979).
Cross-sectional discharge area along the Cape Fear River is discretized into four layers based on
representative lithologic materials encountered: (1) Upper Black Creek Aquifer consists of fine
grained material including silts, clays and silty sands; (2) Black Creek Confining Unit consists of
lignitic, fat clay; (3) Lower Black Creek Aquifer consists of medium to coarse-grained sands; and
(4) Upper Cape Fear Confining Unit consists of hard, fat clay. Unit thicknesses for the four layers
are estimated from LTW well lithology and shown in Table D-2. Estimated representative
discharge areas in contact with the Cape Fear River is estimated based on an assumed discharge
length of 5,000 feet between Willis Creek and W.O. Huske Dam along the river and the
approximate thickness of the Black Creek Aquifer in that area (Table D-2). The calculated
discharge area was varied as part of model calibration. As a refinement to the model, an assessment
of Cape Fear River bottom sediment temperatures adjacent to the Site is ongoing to identify
potential zones of increased groundwater upwelling.
Minimum, 1st quartile, median, 3rd quartile and maximum volumetric groundwater discharge
calculated using Darcy’s Law are presented in Table D-3.

Appendix D – Onsite Groundwater Flow 4 August 2019
REFERENCES
Freeze, R. A. and J. A. Cherry. 1979. Groundwater, Prentice Hall, Englewood Cliffs, N.J.
Geosyntec, 2019. Post Hurricane Florence PFAS Characterization. April 2019.
USGS, 2019. National Water Information System: Web Interface. Accessed March 2019.
https://waterdata.usgs.gov/nwis/uv?site_no=02105500

Appendix D – Onsite Groundwater Flow 1 August 2019
APPENDIX D
TABLES
TABLE D-1
ONSITE GROUNDWATER HYDRAULIC GRADIENTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
Location Date and Time
W.O. Huske
Gage Height1
(ft NGVD 29)
W.O. Huske
Gage Height2
(ft)
W.O. Huske
Water Level
(ft NGVD 29)
W.O. Huske
Water Level
(ft NAVD 88)
Measured Top of
Casing Elevation
(ft NAVD 88)
Measured
Depth to Water
(ft btoc)
Calculated
Water Level
(ft NAVD 88)
Estimated
Distance to River
(ft)
Calculated
Delta Head
(ft)
Calculated
Hydraulic Gradient3
(ft/ft)
Calculated
Hydraulic Gradient3
(m/m)
LTW-01 4/3/2014 18:30 28.97 3.71 32.68 33.59 53.83 15.39 38.44 85 4.854 0.0571 0.0571
LTW-02 4/3/2014 17:20 28.97 3.75 32.72 33.63 52.48 9.53 42.95 130 9.324 0.0717 0.0717
LTW-03 4/3/2014 15:40 28.97 3.74 32.71 33.62 52.91 10.69 42.22 110 8.604 0.0782 0.0782
LTW-04 4/3/2014 9:47 28.97 3.85 32.82 33.73 51.86 7.89 43.97 170 10.244 0.0603 0.0603
LTW-05 4/3/2014 11:07 28.97 3.83 32.80 33.71 52.01 10.76 41.25 145 7.544 0.0520 0.0520
LTW-01 9/16/2015 9:13 28.97 1.23 30.20 31.11 53.83 18.02 35.81 85 4.704 0.0553 0.0553
LTW-02 9/16/2015 13:47 28.97 1.23 30.20 31.11 52.48 10.58 41.9 130 10.794 0.0830 0.0830
LTW-03 9/15/2015 15:12 28.97 1.20 30.17 31.08 52.91 14.23 38.68 110 7.604 0.0691 0.0691
LTW-04 9/15/2015 17:45 28.97 1.20 30.17 31.08 51.86 11.85 40.01 170 8.934 0.0526 0.0526
LTW-05 9/16/2015 10:52 28.97 1.22 30.19 31.10 52.01 11.02 40.99 145 9.894 0.0682 0.0682
LTW-01 6/13/2019 15:40 28.97 4.87 33.84 34.75 53.83 15.23 38.6 85 3.854 0.0453 0.0453
LTW-02 6/13/2019 15:41 28.97 4.87 33.84 34.75 52.48 9.78 42.7 130 7.954 0.0612 0.0612
LTW-03 6/13/2019 15:50 28.97 4.87 33.84 34.75 52.91 12.23 40.68 110 5.934 0.0539 0.0539
LTW-04 6/13/2019 14:02 28.97 4.90 33.87 34.78 51.86 8.14 43.72 170 8.944 0.0526 0.0526
LTW-05 6/13/2019 13:57 28.97 4.91 33.88 34.79 52.01 9.18 42.83 145 8.044 0.0555 0.0555
Notes:
1. The datum of the USGS Gaging Station 02105500 at W.O. Huske is 28.97 feet above NGVD29 (USGS, 2019).
2. Daily mean gage heights are obtained from the USGS Gaging Station 02105500 at the W.O. Huske Dam (USGS, 2019).
3. W.O. Huske water level datum converted from feet above NGVD29 to feet above NAVD88 by a datum shift factor of +0.276 obtained from the VERTCON tool at the National Geodetic Survey (https://www.ngs.noaa.gov/TOOLS/Vertcon/vertcon.html).
4. Calculated hydraulic gradient, i (feet/ feet) = (Water level elevation in LTW well - Cape Fear River Stage elevation) / (Estimated distance from LTW well to river)
5. Abbreviations
ft - feet
ft btoc - feet below top of casing
ft NGVD 29 - feet above the National Geodetic Vertical Datum of 1929
ft NAVD 88 - feet above the North American Vertical Datum of 1988
ft/ft - feet per feet
m/m - meter per meter
Page 1 of 1 August 2019
TABLE D-2
ONSITE GROUNDWATER ESTIMATED DISCHARGE AREA AND HYDRAULIC CONDUCTIVITY
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
Geologic Unit
Estimated unit
thickness
(feet)
Discharge Area
length
(feet)
Estimated Discharge Area
(feet2)
Hydraulic
Conductivity
(m/s)
Representative Lithologic
Material
Upper Black Creek Aquifer 21 - 24 2900 65,250 1.0 x 10-6 Silts, Silty Sand
Blac Creek Confining Unit 1 - 3 2900 5,800 1.0 x 10-8 Clay
Lower Black Creek Aquifer 10 - 20 2900 43,500 1.5 x 10-4 Medium to coarse-grained Sands
Upper Cape Fear Confining Unit > 35 2900 26,100 1.0 x 10-9 Clay
Notes:
5. Abbreviations:
m/s - meters per second
1. Discharge area length presented is from the calibrated mass loading model, assumed to be 58% of total length.
2. Upper Cape Fear Confining Unit is not fully penetrated at the Site and is assumed to be 10 feet in thickness for discharge area calculations. However, this unit does
not discharge significant groundwater due to low hydraulic conductivity values.
3. Unit thickness estimated from available onsite lithology for LTW wells.
4. Hydraulic conductivity values presented in this table are within the range of literature values provided for representative lithologic material. Final hydraulic
conductivity values from the calibrated mass loading model are indicated here. Representative literature hydraulic conductivity values based on range presented in
Freeze, R. A. and J. A. Cherry. 1979. Groundwater, Prentice Hall, Englewood Cliffs, N.J.
Page 1 of 1 August 2019
TABLE D-3
ONSITE GROUNDWATER UPWELLING FLOW RATES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
Geologic Completion Zone
Estimated Discharge
Area1
(feet2)
Estimated Discharge
Area1
(m2)
Estimated Hydraulic
Conductivty2
(m/s)
Hydraulic Gradient (m/m)
Upwelling Rate
(m3/s)
Upwelling Rate (L/s)
Upper Black Creek Aquifer 65,250 6,062 1.00E-06
Black Creek Confining Unit 5,800 539 1.00E-08
Lower Black Creek Aquifer 43,500 4,041 1.50E-04
Upper Cape Fear Confining Unit 26,100 2,425 1.00E-09
Upper Black Creek Aquifer 65,250 6,062 1.00E-06
Black Creek Confining Unit 5,800 539 1.00E-08
Lower Black Creek Aquifer 43,500 4,041 1.50E-04
Upper Cape Fear Confining Unit 26,100 2,425 1.00E-09
Upper Black Creek Aquifer 65,250 6,062 1.00E-06
Black Creek Confining Unit 5,800 539 1.00E-08
Lower Black Creek Aquifer 43,500 4,041 1.50E-04
Upper Cape Fear Confining Unit 26,100 2,425 1.00E-09
Upper Black Creek Aquifer 65,250 6,062 1.00E-06
Black Creek Confining Unit 5,800 539 1.00E-08
Lower Black Creek Aquifer 43,500 4,041 1.50E-04
Upper Cape Fear Confining Unit 26,100 2,425 1.00E-09
Upper Black Creek Aquifer 65,250 6,062 1.00E-06
Black Creek Confining Unit 5,800 539 1.00E-08
Lower Black Creek Aquifer 43,500 4,041 1.50E-04
Upper Cape Fear Confining Unit 26,100 2,425 1.00E-09
Upper Black Creek Aquifer 65,250 6,062 1.00E-06
Black Creek Confining Unit 5,800 539 1.00E-08
Lower Black Creek Aquifer 43,500 4,041 1.50E-04
Upper Cape Fear Confining Unit 26,100 2,425 1.00E-09
Upper Black Creek Aquifer 65,250 6,062 1.00E-06
Black Creek Confining Unit 5,800 539 1.00E-08
Lower Black Creek Aquifer 43,500 4,041 1.50E-04
Upper Cape Fear Confining Unit 26,100 2,425 1.00E-09
Notes:
L/s - liter per second
m2 - squared meters
m/s - meters per second
m/m - meter per meter
0.028
Average
0.083 0.051 51
33
0.045 28
0.061 0.037 37
Minimum
1st Quartile
Median
3rd Quartile
Maximum
0.035 35
0.069 0.042 42
0.057
0.053 0.033
1. The estimated discharge area is calculated based on geologic unit thickess provided in Table D-2 and a model-calibrated discharge length of 2600 feet along the Cape Fear River.
2. Hydraulic conductivity values presented in this table are within the range of literature values provided for representative lithologic material. Final hydraulic conductivity values from
the calibrated mass loading model are indicated here. Representative literature hydraulic conductivity values based on range presented in Freeze, R. A. and J. A. Cherry. 1979.
Groundwater, Prentice Hall, Englewood Cliffs, N.J.
Geometric Mean
0.060 0.037 37
Page 1 of 1 August 2019

Appendix D – Onsite Groundwater Flow 1 August 2019
APPENDIX D
FIGURES
Notes: C:\Users\rwarrier\Desktop\Appendices - Relabel\Appendix C - new D\[Appendix C.xlsx]Figure C-2Computed Hydraulic Gradient between
LTW-05 and Cape Fear River
Chemours Fayetteville Works, North Carolina
Figure
D-1
Raleigh, NC August 2019
1. Hydraulic gradients between LTW-05 and Cape Fear River calculated as:
i = ((LTW Water Level Elevation) - (Cape Fear River Stage Elevation)) / (Estimated distance from
LTW well to river).
2. Cape Fear River stage elevations measured at the USGS flow gauging station located at the W.O.
Huske Dam, ID (USGS# 02105500; USGS, 2019), approximately 0.5 river miles downstream of the
Site.
3. Estimated distance from LTW-05 to Cape Fear River is 145 feet.
-0.02
0.00
0.02
0.04
0.06
0.08
0.10
Jan-18 Jan-18 Mar-18 Apr-18 May-18 May-18 Jun-18 Jul-18 Aug-18 Sep-18 Oct-18 Nov-18 Dec-18 Jan-19Computed Hydraulic Gradient (feet/feet)Hurricane Florence

Appendix E – Offsite Groundwater Flow 1 August 2019
APPENDIX E
SUPPORTING CALCULATIONS - OFFSITE GROUNDWATER MASS LOADING ESTIMATE

Appendix E – Offsite Groundwater Flow 2 August 2019
INTRODUCTION AND OBJECTIVE
Sampling of residential offsite groundwater wells indicate that aerial deposition has potentially
contributed to the detection of PFAS compounds in the groundwater outside the Site property
boundary. Offsite groundwater upwelling to the Cape Fear River is therefore a potential pathway
for per- and polyfluoroalkyl substances (PFAS) mass loading to the Cape Fear River. This pathway
was identified as Transport Pathway Number 8 in the PFAS mass loading design (Section 4) of
the Chemours Fayetteville Works Cape Fear River PFAS Mass Loading Model Assessment and
Paragraph 11.1 Characterization of PFAS at Intakes (Geosyntec, 2019). The objective of the
supporting calculations presented in this appendix is to estimate PFAS mass loading from offsite
groundwater discharge through a forward assessment based on Darcy’s Law using available
hydrogeological data as described below.
APPROACH
The discharge and PFAS concentrations in offsite groundwater used to estimate the PFAS mass
loading from offsite groundwater (Transport Pathway 8) were limited by data availability and
therefore required the assumptions described below.
Volumetric groundwater discharge upwelling to the Cape Fear River is estimated using Darcy’s
Law similar to the estimation of onsite groundwater flow (Appendix D): 𝑄𝑄=𝐾𝐾𝐾𝐾𝐾𝐾
where Q, the volumetric discharge [L3T-1], is the groundwater discharge being estimated;
K, the hydraulic conductivity of the aquifer [LT-1], assumed to be 2.5 x 10-4 m/s, derived
from onsite pump tests in the Surficial Aquifer (Parsons, 2018b);
i, the hydraulic gradient [LL-1]; an estimated value that is calculated based on the onsite
groundwater hydraulic gradient (refer to Appendix D) and an adjustment factor that is
based on topographic variations which is assumed to be reflective of gradient variations in
an unconfined aquifer system. This gradient adjustment factor is computed from slope
differences using LiDAR digital elevation models in ArcGIS (refer to Figure E-1); and,
A, the cross-sectional area of groundwater discharge into the Cape Fear River [L2],
estimated based on measurements presented in Appendix C and the approximate
thickness of the aquifer estimated from onsite information.
Minimum, 1st quartile, median, 3rd quartile and maximum volumetric groundwater discharge was
calculated using Darcy’s Law as presented in Table E-1.
PFAS concentrations were estimated from spatial monitoring well clusters; offsite groundwater
wells were grouped together by observed HFPO-DA concentrations from the Offsite Residential
Well program (Table E-2, Figure E-2). The offsite groundwater wells were grouped in to the
following clusters:
A. 3 to 5 miles from the Site on the east side of the Cape Fear River;

Appendix E – Offsite Groundwater Flow 3 August 2019
B. 5 to 6 miles away from the Site on the east side of the Cape Fear River;
C. 1 to 3 miles from the Site on the east side of the Cape Fear River;
D. 3 to 4 miles from the Site on the west side of the Cape Fear River; and
E. 1 to 3 miles from the Site on the west side of the Cape Fear River.
Statistics were performed on the concentration clusters to analyze the correlation of HFPO-DA
concentration with both (1) distance from the Site and (2) the side of the river where the
sampling location is situated. These concentrations were used to develop minimum, 1st quartile,
median, 3rd quartile and maximum HFPO-DA concentrations for input into the Mass Loading
Model (Table E-1).
Data from six locations in the Granular Activated Carbon Pilot Well testing program (Chemours,
2019) were used to build a relationship between HFPO-DA and other PFAS compounds. The
average ratios of the measured HFPO-DA to other compounds across the six locations were used
to estimate concentrations of other PFAS compounds (Table E-3).

Appendix E – Offsite Groundwater Flow 4 August 2019
REFERENCES
Chemours, 2019. Residential Well Carbon Pilot Testing Data. Available at:
https://www.chemours.com/Fayetteville-Works/en-us/c3-dimer-acid/compliance-testing/
Geosyntec, 2019. Chemours Fayetteville Works Cape Fear River PFAS Mass Loading Model
Assessment and Paragraph 11.1 Characterization of PFAS at Intakes. August 2019.

Appendix E – Offsite Groundwater Flow 1 August 2019
APPENDIX E
TABLES
TABLE E-1
OFFSITE GROUNDWATER FLOW ESTIMATE
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
Statistics Area Section River Length1 (m)River Depth2
(m)
Proportion of
Upwelling in the
River Bottom3
Upwelling Area
(m2)
On-Site Hydraulic
Gradient4
(m/m)
Gradient
Adjustment
Factor5
Adjusted Upwelling
Hydraulic Gradient
(m/m)
Hydraulic
Conductivity (m/s)
Upwelling Rate
(m3/s)
HFPO-DA
Concentrations6
(ng/L)
Mass Loading
(ng/s)
Mass Loading
(ng/s)
A East, Adjacent Site 3,303 14 19,068 0.045 0.48 0.022 0.105 1.8 188
B East, Downstream 2,048 14 11,825 0.045 0.48 0.022 0.065 1.8 118
C East, Downstream 5,206 14 30,056 0.045 0.48 0.022 0.165 4.0 661
D West, Downstream 1,757 14 10,146 0.045 0.48 0.022 0.056 10 558
E West, Downstream 2,591 14 14,957 0.045 0.48 0.022 0.082 10 822
A East, Adjacent Site 3,303 14 22,888 0.045 0.48 0.022 0.126 8.0 1,002
B East, Downstream 2,048 14 14,194 0.045 0.48 0.022 0.078 1.8 142
C East, Downstream 5,206 14 36,076 0.045 0.48 0.022 0.198 11 2,081
D West, Downstream 1,757 14 12,179 0.045 0.48 0.022 0.067 10 669
E West, Downstream 2,591 14 17,954 0.045 0.48 0.022 0.099 10 987
A East, Adjacent Site 3,303 14 29,194 0.045 0.48 0.022 0.160 10 1,604
B East, Downstream 2,048 14 18,105 0.045 0.48 0.022 0.099 1.8 181
C East, Downstream 5,206 14 46,017 0.045 0.48 0.022 0.253 56 14,160
D West, Downstream 1,757 14 15,535 0.045 0.48 0.022 0.085 14 1,195
E West, Downstream 2,591 14 22,901 0.045 0.48 0.022 0.126 10 1,258
A East, Adjacent Site 3,303 16 38,780 0.045 0.48 0.022 0.213 17 3,516
B East, Downstream 2,048 16 24,049 0.045 0.48 0.022 0.132 1.8 241
C East, Downstream 5,206 16 61,126 0.045 0.48 0.022 0.336 136 45,679
D West, Downstream 1,757 16 20,635 0.045 0.48 0.022 0.113 21 2,324
E West, Downstream 2,591 16 30,420 0.045 0.48 0.022 0.167 175 29,252AEast, Adjacent Site 3,303 16 41,275 0.045 0.48 0.022 0.227 50 11,340
B East, Downstream 2,048 16 25,597 0.045 0.48 0.022 0.141 1.8 256
C East, Downstream 5,206 16 65,058 0.045 0.48 0.022 0.357 940 336,037
D West, Downstream 1,757 16 21,963 0.045 0.48 0.022 0.121 78 9,413
E West, Downstream 2,591 16 32,377 0.045 0.48 0.022 0.178 420 74,720
A East, Adjacent Site 3,303 16 31,788 0.045 0.48 0.022 0.175 15 2,632BEast, Downstream 2,048 16 19,713 0.045 0.48 0.022 0.108 1.8 197CEast, Downstream 5,206 16 50,104 0.045 0.48 0.022 0.275 158 43,525
D West, Downstream 1,757 16 16,915 0.045 0.48 0.022 0.093 23 2,164
E West, Downstream 2,591 16 24,935 0.045 0.48 0.022 0.137 115 15,817
A East, Adjacent Site 3,303 16 30,689 0.045 0.48 0.022 0.169 9.3 1,566BEast, Downstream 2,048 16 19,032 0.045 0.48 0.022 0.105 1.8 190CEast, Downstream 5,206 16 48,372 0.045 0.48 0.022 0.266 51 13,639DWest, Downstream 1,757 16 16,330 0.045 0.48 0.022 0.090 17 1,547
E West, Downstream 2,591 16 24,073 0.045 0.48 0.022 0.132 35 4,635
Notes:
1. River lengths are estimated based on the aerial deposition calculations in Appendix C.
2. River depths are measured in the onsite groundwater flow calculations in Appendix D.
3. The proportion of groundwater upwelling in the river bottom are estimated by taking the ratio of the Black Creek Aquifer discharge area to the total onsite groundwater discharge area, which can be found in Appendix D.
4. Onsite groundwater hydraulic gradients are calculated in Appendix D.
5. Gradient adjustments were calculated using a 20 ft LiDAR DEM to generate a slope map which was divided into different zones (Figures E-1 and E-2).
6. HFPO-DA concentrations statistics are listed in Table E-2.
HFPO-DA: Hexafluoropropylene oxide dimer acid; or dimer acid
L/s - liter per second
m - meter
m2 - squared meter
m/m - meter per meter
m/s - meter per second
m3/s - cubic meter per second
ng/L - nanogram per liter
ng/s - nanogram per second
64335.5
21576.8
2345.8
4880.8
18398.6
81012.0
431766.8
2.55E-04
2.55E-04
2.55E-04
2.55E-04
2.55E-04
63%
76%
80%
62%
60%
Median
3rd Quartile
Maximum
Average
Geometric Mean
Minimum
1st Quartile
41%
49%
2.55E-04
2.55E-04
Page 1 of 1 August 2019
TABLE E-2
OFFSITE RESIDENTIAL WELL HFPO-DA CONCENTRATIONS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC P.C.
Area Location Sample Date HFPO-DA
Concentration (ng/L)
Number of Locations
With Detects
Minimum
Concentration (ng/L)
1st Quartile
Concentration (ng/L)
Median Concentration
(ng/L)
3rd Quartile
Concentration (ng/L)
Maximum
Concentration (ng/L)
Average Concentration
(ng/L)
Geometric Mean
Concentration (ng/L)
Private Well 14-Dec-17 21
Private Well 12-Dec-17 <10
Private Well 13-Dec-17 38
Private Well 24-Jan-18 50
Private Well 24-Jan-18 15
Private Well 24-Jan-18 <10
Private Well 25-Apr-18 1.79
Private Well 25-Apr-18 1.79
Private Well 25-Apr-18 1.79
Private Well 9-Jan-18 <10
Private Well 11-Apr-18 36.9
Private Well 11-Dec-17 <10
Private Well 15-Jan-18 <10
Private Well 30-Nov-17 13
Private Well 30-Nov-17 <10
Private Well 11-Apr-18 1.86
B Private Well 11-Apr-18 1.82 1 1.8 1.8 1.8 1.8 1.8 1.8 1.8
Private Well 18-Oct-17 49
Private Well 15-Dec-17 <10
Private Well 31-Jan-18 527
Private Well 30-Nov-17 20
Private Well 29-Nov-17 <4
Private Well 30-Apr-19 240
Private Well 14-Aug-18 <10
Private Well 9-May-18 36
Private Well 4-Jan-18 <10
Private Well 12-Dec-17 76
Private Well 18-Mar-19 940
Private Well 6-Aug-18 780
Private Well 22-Sep-17 250
Private Well 14-Dec-17 78
Private Well 5-Jan-18 12
Private Well 5-Jan-18 <10
Private Well 5-Dec-17 24
Private Well 6-Dec-17 63
Private Well 5-Dec-17 94
Private Well 5-Dec-17 150
Private Well 7-Dec-17 <10
Private Well 6-Dec-17 85
Private Well 1-Feb-18 18
Private Well 1-Mar-18 <10
Private Well 7-Feb-18 <10
Private Well 15-Dec-17 23
Private Well 8-Feb-18 <10
Private Well 8-Feb-18 14
Private Well 14-Dec-17 78
Private Well 13-Nov-17 <10
Private Well 6-Dec-17 <10
Private Well 7-Dec-17 420
Private Well 7-Dec-17 <10
Private Well 7-Dec-17 <10
Private Well 27-Jul-18 120
Private Well 27-Jul-18 22
Private Well 20-Oct-17 360
Private Well 16-Oct-17 <10
Private Well 9-Apr-19 400
Private Well 20-Oct-17 <10
Private Well 23-Oct-17 <10
Private Well 23-Oct-17 95
Private Well 23-Oct-17 <10
Private Well 23-Oct-17 <10
Private Well 6-Nov-17 340
Notes:
HFPO-DA: Hexafluoropropylene oxide dimer acid; or dimer acid
ng/L - nanograms per liter
< - not detected
10 175 115 35
78 23 17
420
136 940 158 51
4 1.8 10 14 21
16 1.8 11 56
10 17 50 15 9.3101.8 8.0
E
D
A
C
7 1.8 10
Page 1 of 1 August 2019
TABLE E-3
RATIO OF OTHER PFAS COMPOUNDS TO HFPO-DA
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
HFPO-DA Hexafluoropropylene oxide dimer acid 13252-13-6 1.00
PEPA Perfluoroethoxypropyl carboxylic acid 267239-61-2 0.67
PFECA-G Perfluoro-4-isopropoxybutanoic acid 801212-59-9 NA
PFMOAA Perfluoro-2-methoxyaceticacid 674-13-5 0.49
PFO2HxA Perfluoro(3,5-dioxahexanoic) acid 39492-88-1 1.44
PFO3OA Perfluoro(3,5,7-trioxaoctanoic) acid 39492-89-2 0.11
PFO4DA Perfluoro(3,5,7,9-tetraoxadecanoic) acid 39492-90-5 0.11
PMPA Perfluoromethoxypropyl carboxylic acid 13140-29-9 2.22
Hydro-EVE Acid Perfluoroethoxsypropanoic acid 773804-62-9 NA
EVE Acid Perfluoroethoxypropionic acid 69087-46-3 NA
PFECA B Perfluoro-3,6-dioxaheptanoic acid 151772-58-6 NA
R-EVE R-EVE EVS1428 NA
PFO5DA Perfluoro-3,5,7,9,11-pentaoxadodecanoic acid 39492-91-6 0.22
Byproduct 4 Byproduct 4 EVS1429 NA
Byproduct 5 Byproduct 5 EVS1430 NA
Byproduct 6 Byproduct 6 EVS1431 NA
NVHOS Perfluoroethoxysulfonic acid 1132933-86-8 NA
PES Perfluoroethoxyethanesulfonic acid 113507-82-7 NA
PFESA-BP1 Byproduct 1 29311-67-9 NA
PFESA-BP2 Byproduct 2 749836-20-2 NA
PFBA Perfluorobutanoic acid 375-22-4 0.03
PFDA Perfluorodecanoic acid 335-76-2 NA
PFDoA Perfluorododecanoic acid 307-55-1 NA
PFHpA Perfluoroheptanoic acid 375-85-9 NA
PFNA Perfluorononanoic acid 375-95-1 NA
PFOA Perfluorooctanoic acid 335-67-1 0.01
PFHxA Perfluorohexanoic acid 307-24-4 0.01
PFPeA Perfluoropentanoic acid 2706-90-3 NA
PFTeA Perfluorotetradecanoic acid 376-06-7 NA
PFTriA Perfluorotridecanoic acid 72629-94-8 NA
PFUnA Perfluoroundecanoic acid 2058-94-8 NA
PFBS Perfluorobutanesulfonic acid 375-73-5 NA
PFDS Perfluorodecanesulfonic acid 335-77-3 NA
PFHpS Perfluoroheptanesulfonic acid 375-92-8 NA
PFHxS Perfluorohexanesulfonic acid 355-46-4 NA
PFNS Perfluorononanesulfonic acid 68259-12-1 NA
PFOS Perfluorooctanesulfonic acid 1763-23-1 NA
PFPeS Perfluoropentanesulfonic acid 2706-91-4 NA
10:2 FTS 10:2-fluorotelomersulfonic acid 120226-60-0 NA
4:2 FTS 4:2 fluorotelomersulfonic acid 757124-72-4 NA
6:2 FTS 6:2 fluorotelomersulfonic acid 27619-97-2 NA
8:2 FTS 8:2 fluorotelomersulfonic acid 39108-34-4 NA
NEtFOSAA NEtFOSAA 2991-50-6 NA
NEtPFOSA NEtPFOSA 4151-50-2 NA
NEtPFOSAE NEtPFOSAE 1691-99-2 NA
NMeFOSAA NMeFOSAA 2355-31-9 NA
NMePFOSA NMePFOSA 31506-32-8 NA
NMePFOSAE NMePFOSAE 24448-09-7 NA
PFDOS Perfluorododecanesulfonic acid 79780-39-5 NA
PFHxDA Perfluorohexadecanoic acid 67905-19-5 NA
PFODA Perfluorooctadecanoic acid 16517-11-6 NA
PFOSA Perfluorooctanesulfonamide 754-91-6 NA
F-53B Major F-53B Major 73606-19-6 NA
F-53B Minor F-53B Minor 83329-89-9 NA
ADONA 4,8-dioxa-3H-perfluorononanoate 958445-44-8 NA
NaDONA NaDONA EVS1361 NA
DONA DONA 919005-14-4 NA
Notes:
EPA Method 537 Mod
Approximate Concentration
Ratio to HFPO-DA
1. Approximate concentration ratios based on measured PFAS concentrations from Locations 30, 48, 71, 75, 77, and 79 of the Carbon Pilot Well
Testing Program. The average of the concentration ratios among the six locations were used. For EPA 537 compounds, compounds detected less than
50% of the time in collected samples were classified as being NA.
Analytical Method Common Name Chemical Name CASN
Table 3+ Lab SOP
Page 1 of 1 August 2019

Appendix E – Offsite Groundwater Flow 1 August 2019
APPENDIX E
FIGURES
So urce s: E sri, H E R E, G armi n , I nt erm ap , i ncre me nt P C orp . , G E B C O , U S G S , F AO , N P S , N R C A N , G e oB as e, IG N , K ad ast e r N L , O rd na nce Su rve y, E sri Jap an , M ET I , E sri C hi na (H o ng K o ng ), (c) O pe nS t ree tM ap c on tri bu t ors, an d t he G IS U se r C o mmu ni ty
HFPO-DA Sampling at Offsite Residential Wells
Chemours Fayetteville Works, North Carolina
Figure
E-2Raleigh, NC
2 0 21 Miles
³Path: H:\MXDs\TR0726_ProposedOffSiteLocations_All_Aquifers.mxd Last Revised: 8/19/2019 Author: SLauAugust 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
N
S
W E
6 mi
4 mi
2 mi
Notes:1. Black lines represent cardinal directions(N, E, S, W)
2. ng/L = nanograms per liter
Legend
Offsite Private Well HFPO-DA Concentrations (ng/L)
Non-detect or 0-10
10-70
70-140
140-1,400
>1,400
Site Boundary
D B
A
C
E

Appendix F – Summary of Sensitivity Analysis Results 1 August 2019
APPENDIX F
SUMMARY OF SENSITIVITY ANALYSIS RESULTS
TABLE F-1
SUMMARY OF SENSTIVITY ANALYSIS RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
May-19 Jun-19 May-19 Jun-19 May-19 Jun-19 May-19 Jun-19 May-19 Jun-19
1 Up-Stream River 429,550 1,868,529 429,550 1,868,529 4 15 4 15 ----
2 Willis Creek 1,056,363 494,506 1,056,363 494,506 10 4 10 4 ----
3 Aerial Deposition on River 7,093 7,093 41,598 41,598 0.1 0.1 0.4 0.3 -0.3 -0.3
4 Outfall 002 375,836 918,968 375,836 918,968 4 7 4 7 ----
5 Onsite Groundwater 2,309,468 2,164,439 2,309,468 2,164,439 22 17 22 17 ----
6A Seep A 967,485 1,325,336 967,485 1,325,336 9 10 9 10 ----
6B Seep B 1,683,557 1,038,907 1,683,557 1,038,907 16 8 16 8 ----
6C Seep C 215,507 282,525 215,507 282,525 2 2 2 2 ----
6D Seep D 494,879 467,789 494,879 467,789 5 4 5 4 ----
7 Old Outfall 002 2,417,156 3,750,579 2,417,156 3,750,579 23 29 23 29 ----
8 Offsite Groundwater 30,587 30,587 30,587 30,587 0 0 0 0 ----
9 Georgia Branch Creek 390,334 405,836 390,334 405,836 4 3 4 3 ----
10,377,814 12,755,093 10,412,319 12,789,599 100 100 100 100 ----
9,959,601 13,447,005 9,959,601 13,447,005 ------------
1 Up-Stream River 429,550 1,868,529 429,550 1,868,529 4 15 4 15 0 0
2 Willis Creek 1,056,363 494,506 948,998 444,246 10 4 9 3 0.9 0.4
3 Aerial Deposition on River 7,093 7,093 7,093 7,093 < 2%< 2%< 2%< 2%----
4 Outfall 002 375,836 918,968 375,836 918,968 4 7 4 7 ----
5 Onsite Groundwater 2,309,468 2,164,439 2,309,468 2,164,439 22 17 22 17 ----
6A Seep A 967,485 1,325,336 967,485 1,325,336 9 10 9 10 ----
6B Seep B 1,683,557 1,038,907 1,683,557 1,038,907 16 8 16 8 ----
6C Seep C 215,507 282,525 215,507 282,525 2 2 2 2 ----
6D Seep D 494,879 467,789 494,879 467,789 5 4 5 4 ----
7 Old Outfall 002 2,417,156 3,750,579 2,417,156 3,750,579 23 29 24 30 ----
8 Offsite Groundwater 30,587 30,587 30,587 30,587 < 2%< 2%< 2%< 2%----
9 Georgia Branch Creek 390,334 405,836 390,334 405,836 4 3 4 3 ----
10,377,814 12,755,093 10,270,448 12,704,833 100 100 100 100 ----
9,959,601 13,447,005 9,959,601 13,447,005 ------------
1 Up-Stream River 429,550 1,868,529 429,550 1,868,529 4 15 4 15 ----
2 Willis Creek 1,056,363 494,506 529,138 247,701 10 4 5 2 5 2
3 Aerial Deposition on River 7,093 7,093 7,093 7,093 < 2%< 2%< 2%< 2%----
4 Outfall 002 375,836 918,968 375,836 918,968 4 7 4 7 ----
5 Onsite Groundwater 2,309,468 2,164,439 2,309,468 2,164,439 22 17 23 17 ----
6A Seep A 967,485 1,325,336 967,485 1,325,336 9 10 10 11 ----
6B Seep B 1,683,557 1,038,907 1,683,557 1,038,907 16 8 17 8 ----
6C Seep C 215,507 282,525 215,507 282,525 2 2 2 2 ----
6D Seep D 494,879 467,789 494,879 467,789 5 4 5 4 ----
7 Old Outfall 002 2,417,156 3,750,579 2,417,156 3,750,579 23 29 25 30 ----
8 Offsite Groundwater 30,587 30,587 30,587 30,587 < 2%< 2%< 2%< 2%----
9 Georgia Branch Creek 390,334 405,836 390,334 405,836 4 3 4 3 ----
10,377,814 12,755,093 9,850,589 12,508,288 100 100 100 100 ----
9,959,601 13,447,005 9,959,601 13,447,005 ------------
Flow Rates for
Willis Creek
Reduced Willis Creek
Flow by 10%
Less than 1% variation
between original and
sensitivity model
Total Estimated Mass Flux and Corresponding River Concentration
Measured Concentration and Calculated Mass Loading at Bladen Bluffs
Flow Rates for
Willis Creek
Reduced Willis Creek
Flow by 50%
2 - 5 % variation between
original and sensitivity
model
Total Estimated Mass Flux and Corresponding River Concentration
Measured Concentration and Calculated Mass Loading at Bladen Bluffs
Empirical Total
Table 3+
Estimated
Loading
(%)
Modeled Total
Table 3+
Estimated
Loading
(%)
[Original -
Sensitivty]
(%)Observations
Aerial deposition
on River
Aerial deposition load
varied from 1,132
ng/s to 6,638 ng/s
Less than 0.5 % variation
between original and
sensitivity model
Total Estimated Mass Flux and Corresponding River Concentration
Measured Concentration and Calculated Mass Loading at Bladen Bluffs
Sensitivity
Scenario Descirption
Transport
Pathway
Number
Potential PFAS Transport Pathway
Calibrated, Original Total
Table3+ Mass Loading
Estimate
(ng/s)
Modeled Sensitivty Total
Table 3+ Mass Loading
Estimate
(ng/s)
Page 1 of 5 August 2019
TABLE F-1
SUMMARY OF SENSTIVITY ANALYSIS RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
May-19 Jun-19 May-19 Jun-19 May-19 Jun-19 May-19 Jun-19 May-19 Jun-19
Empirical Total
Table 3+
Estimated
Loading
(%)
Modeled Total
Table 3+
Estimated
Loading
(%)
[Original -
Sensitivty]
(%)ObservationsSensitivity
Scenario Descirption
Transport
Pathway
Number
Potential PFAS Transport Pathway
Calibrated, Original Total
Table3+ Mass Loading
Estimate
(ng/s)
Modeled Sensitivty Total
Table 3+ Mass Loading
Estimate
(ng/s)
1 Up-Stream River 429,550 1,868,529 429,550 1,868,529 4 15 4 15 ----
2 Willis Creek 1,056,363 494,506 1,161,803 543,865 10 4 11 4 -0.9 -0.4
3 Aerial Deposition on River 7,093 7,093 7,093 7,093 < 2%< 2%< 2%< 2%----
4 Outfall 002 375,836 918,968 375,836 918,968 4 7 4 7 ----
5 Onsite Groundwater 2,309,468 2,164,439 2,309,468 2,164,439 22 17 22 17 ----
6A Seep A 967,485 1,325,336 967,485 1,325,336 9 10 9 10 ----
6B Seep B 1,683,557 1,038,907 1,683,557 1,038,907 16 8 16 8 ----
6C Seep C 215,507 282,525 215,507 282,525 2 2 2 2 ----
6D Seep D 494,879 467,789 494,879 467,789 5 4 5 4 ----
7 Old Outfall 002 2,417,156 3,750,579 2,417,156 3,750,579 23 29 23 29 ----
8 Offsite Groundwater 30,587 30,587 30,587 30,587 < 2%< 2%< 2%< 2%----
9 Georgia Branch Creek 390,334 405,836 390,334 405,836 4 3 4 3 ----
10,377,814 12,755,093 10,483,254 12,804,452 100 100 100 100 ----
9,959,601 13,447,005 9,959,601 13,447,005 ------------
1 Up-Stream River 429,550 1,868,529 429,550 1,868,529 4 15 4 14 ----
2 Willis Creek 1,056,363 494,506 1,587,414 743,102 10 4 15 6 -4 -2
3 Aerial Deposition on River 7,093 7,093 7,093 7,093 < 2%< 2%< 2%< 2%----
4 Outfall 002 375,836 918,968 375,836 918,968 4 7 3 7 ----
5 Onsite Groundwater 2,309,468 2,164,439 2,309,468 2,164,439 22 17 21 17 ----
6A Seep A 967,485 1,325,336 967,485 1,325,336 9 10 9 10 ----
6B Seep B 1,683,557 1,038,907 1,683,557 1,038,907 16 8 15 8 ----
6C Seep C 215,507 282,525 215,507 282,525 2 2 2 2 ----
6D Seep D 494,879 467,789 494,879 467,789 5 4 5 4 ----
7 Old Outfall 002 2,417,156 3,750,579 2,417,156 3,750,579 23 29 22 29 ----
8 Offsite Groundwater 30,587 30,587 30,587 30,587 < 2%< 2%< 2%< 2%----
9 Georgia Branch Creek 390,334 405,836 390,334 405,836 4 3 4 3 ----
10,377,814 12,755,093 10,908,865 13,003,690 100 100 100 100 ----
9,959,601 13,447,005 9,959,601 13,447,005
1 Up-Stream River 429,550 1,868,529 429,550 1,868,529 4 15 5 17 ----
2 Willis Creek 1,056,363 494,506 1,056,363 494,506 10 4 12 4 ----
3 Aerial Deposition on River 7,093 7,093 7,093 7,093 < 2%< 2%< 2%< 2%----
4 Outfall 002 375,836 918,968 375,836 918,968 4 7 4 8 ----
5 Onsite Groundwater 2,309,468 2,164,439 2,309,468 2,164,439 22 17 27 19 ----
6A Seep A 967,485 1,325,336 446,281 296,430 9 10 5 3 4 8
6B Seep B 1,683,557 1,038,907 772,558 845,720 16 8 9 8 7 1
6C Seep C 215,507 282,525 173,835 173,000 2 2 2 2 0 1
6D Seep D 494,879 467,789 246,705 233,201 5 4 3 2 2 2
7 Old Outfall 002 2,417,156 3,750,579 2,417,156 3,750,579 23 29 28 34 ----
8 Offsite Groundwater 30,587 30,587 30,587 30,587 < 2%< 2%< 2%< 2%----
9 Georgia Branch Creek 390,334 405,836 390,334 405,836 4 3 5 4 ----
10,377,814 12,755,093 8,655,764 11,188,887 100 100 100 100 ----
9,959,601 13,447,005 9,959,601 13,447,005 ------------
Flow Rates for
Seeps
Reduced Seeps Flow
by 50%
Less than 8% decrease in
overall mass loading
between original and
sensitivity model. Decrease
in mass loading for Seep A
between 4% and 8 %, Seep
B between 1% and 7 %,
Seep C less than 1 %, and
Seep D less than 2%
Total Estimated Mass Flux and Corresponding River Concentration
Measured Concentration and Calculated Mass Loading at Bladen Bluffs
Flow Rates for
Willis Creek
Increase Willis Creek
Flow by 10%
Less than 2% variation
between original and
sensitivity model
Total Estimated Mass Flux and Corresponding River Concentration
Measured Concentration and Calculated Mass Loading at Bladen Bluffs
Flow Rates for
Willis Creek
Increase Willis Creek
Flow by 50%
2 - 5 % variation between
original and sensitivity
model
Total Estimated Mass Flux and Corresponding River Concentration
Measured Concentration and Calculated Mass Loading at Bladen Bluffs
Page 2 of 5 August 2019
TABLE F-1
SUMMARY OF SENSTIVITY ANALYSIS RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
May-19 Jun-19 May-19 Jun-19 May-19 Jun-19 May-19 Jun-19 May-19 Jun-19
Empirical Total
Table 3+
Estimated
Loading
(%)
Modeled Total
Table 3+
Estimated
Loading
(%)
[Original -
Sensitivty]
(%)ObservationsSensitivity
Scenario Descirption
Transport
Pathway
Number
Potential PFAS Transport Pathway
Calibrated, Original Total
Table3+ Mass Loading
Estimate
(ng/s)
Modeled Sensitivty Total
Table 3+ Mass Loading
Estimate
(ng/s)
1 Up-Stream River 429,550 1,868,529 429,550 1,868,529 4 15 4 13 ----
2 Willis Creek 1,056,363 494,506 1,056,363 494,506 10 4 9 4 ----
3 Aerial Deposition on River 7,093 7,093 7,093 7,093 < 2%< 2%< 2%< 2%----
4 Outfall 002 375,836 918,968 375,836 918,968 4 7 3 7 ----
5 Onsite Groundwater 2,309,468 2,164,439 2,309,468 2,164,439 22 17 20 15 ----
6A Seep A 967,485 1,325,336 1,338,842 889,290 9 10 11 6 -2 4
6B Seep B 1,683,557 1,038,907 2,317,673 2,537,160 16 8 20 18 -4 -10
6C Seep C 215,507 282,525 521,504 519,000 2 2 4 4 -2 -1
6D Seep D 494,879 467,789 493,410 466,401 5 4 4 3 1 0
7 Old Outfall 002 2,417,156 3,750,579 2,417,156 3,750,579 23 29 21 27 ----
8 Offsite Groundwater 30,587 30,587 30,587 30,587 < 2%< 2%< 2%< 2%----
9 Georgia Branch Creek 390,334 405,836 390,334 405,836 4 3 3 3 ----
10,377,814 12,755,093 11,687,814 14,052,387 100 100 100 100 ----
9,959,601 13,447,005 9,959,601 13,447,005 ------------
1 Up-Stream River 429,550 1,868,529 429,550 1,868,529 4 15 5 18 ----
2 Willis Creek 1,056,363 494,506 1,056,363 494,506 10 4 12 5 ----
3 Aerial Deposition on River 7,093 7,093 7,093 7,093 < 2%< 2%< 2%< 2%----
4 Outfall 002 375,836 918,968 375,836 918,968 4 7 4 9 ----
5 Onsite Groundwater 2,309,468 2,164,439 2,309,468 2,164,439 22 17 25 21 ----
6A Seep A 967,485 1,325,336 967,485 1,325,336 9 10 11 13 ----
6B Seep B 1,683,557 1,038,907 1,683,557 1,038,907 16 8 18 10 ----
6C Seep C 215,507 282,525 215,507 282,525 2 2 2 3 ----
6D Seep D 494,879 467,789 494,879 467,789 5 4 5 4 ----
7 Old Outfall 002 2,417,156 3,750,579 1,185,765 1,391,765 23 29 13 13 10 16
8 Offsite Groundwater 30,587 30,587 30,587 30,587 < 2%< 2%< 2%< 2%----
9 Georgia Branch Creek 390,334 405,836 390,334 405,836 4 3 4 4 ----
10,377,814 12,755,093 9,146,422 10,396,278 100 100 100 100 ----
9,959,601 13,447,005 9,959,601 13,447,005 ------------
1 Up-Stream River 429,550 1,868,529 429,550 1,868,529 4 15 3 13 ----
2 Willis Creek 1,056,363 494,506 1,056,363 494,506 10 4 8 3 ----
3 Aerial Deposition on River 7,093 7,093 7,093 7,093 < 2%< 2%< 2%< 2%----
4 Outfall 002 375,836 918,968 375,836 918,968 4 7 3 6 ----
5 Onsite Groundwater 2,309,468 2,164,439 2,309,468 2,164,439 22 17 18 15 ----
6A Seep A 967,485 1,325,336 967,485 1,325,336 9 10 8 9 ----
6B Seep B 1,683,557 1,038,907 1,683,557 1,038,907 16 8 13 7 ----
6C Seep C 215,507 282,525 215,507 282,525 2 2 2 2 ----
6D Seep D 494,879 467,789 494,879 467,789 5 4 4 3 ----
7 Old Outfall 002 2,417,156 3,750,579 4,743,060 5,567,058 23 29 37 38 -14 -9
8 Offsite Groundwater 30,587 30,587 30,587 30,587 < 2%< 2%< 2%< 2%----
9 Georgia Branch Creek 390,334 405,836 390,334 405,836 4 3 3 3 ----
10,377,814 12,755,093 12,703,717 14,571,572 100 100 100 100 ----
9,959,601 13,447,005 9,959,601 13,447,005 ------------
Flow Rates for
Old Outfall 002
Reduced Old Outfall
002 Flow by 50%
Estimated loading lower by
10% to 16% between
original and sensitivity
model
Total Estimated Mass Flux and Corresponding River Concentration
Measured Concentration and Calculated Mass Loading at Bladen Bluffs
Flow Rates for
Old Outfall 002
Increased Old Outfall
002 Flow by 50%
Estimated loading
increased by 9% to 14%
between original and
sensitivity model
Total Estimated Mass Flux and Corresponding River Concentration
Measured Concentration and Calculated Mass Loading at Bladen Bluffs
Flow Rates for
Seeps
Increase Seeps Flow
by 50%
Less than 14% increase in
overall mass loading
between original and
sensitivity model. Decrease
in mass loading for Seep A
between 2% and 4 %, Seep
B between 4 and 10 %,
Seep C between 1 and 23
%, and Seep D less than
1%
Total Estimated Mass Flux and Corresponding River Concentration
Measured Concentration and Calculated Mass Loading at Bladen Bluffs
Page 3 of 5 August 2019
TABLE F-1
SUMMARY OF SENSTIVITY ANALYSIS RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
May-19 Jun-19 May-19 Jun-19 May-19 Jun-19 May-19 Jun-19 May-19 Jun-19
Empirical Total
Table 3+
Estimated
Loading
(%)
Modeled Total
Table 3+
Estimated
Loading
(%)
[Original -
Sensitivty]
(%)ObservationsSensitivity
Scenario Descirption
Transport
Pathway
Number
Potential PFAS Transport Pathway
Calibrated, Original Total
Table3+ Mass Loading
Estimate
(ng/s)
Modeled Sensitivty Total
Table 3+ Mass Loading
Estimate
(ng/s)
1 Up-Stream River 429,550 1,868,529 429,550 1,868,529 4 15 3 11 ----
2 Willis Creek 1,056,363 494,506 1,056,363 494,506 10 4 7 3 ----
3 Aerial Deposition on River 7,093 7,093 7,093 7,093 < 2%< 2%< 2%< 2%----
4 Outfall 002 375,836 918,968 375,836 918,968 4 7 3 6 ----
5 Onsite Groundwater 2,309,468 2,164,439 2,309,468 2,164,439 22 17 16 13 ----
6A Seep A 967,485 1,325,336 967,485 1,325,336 9 10 7 8 ----
6B Seep B 1,683,557 1,038,907 1,683,557 1,038,907 16 8 12 6 ----
6C Seep C 215,507 282,525 215,507 282,525 2 2 2 2 ----
6D Seep D 494,879 467,789 494,879 467,789 5 4 3 3 ----
7 Old Outfall 002 2,417,156 3,750,579 6,324,080 7,422,744 23 29 44 45 -21 -16
8 Offsite Groundwater 30,587 30,587 30,587 30,587 < 2%< 2%< 2%< 2%----
9 Georgia Branch Creek 390,334 405,836 390,334 405,836 4 3 3 2 ----
10,377,814 12,755,093 14,284,737 16,427,258 100 100 100 100 ----
9,959,601 13,447,005 9,959,601 13,447,005 ------------
1 Up-Stream River 429,550 1,868,529 429,550 1,868,529 4 15 4 15 ----
2 Willis Creek 1,056,363 494,506 1,056,363 494,506 10 4 10 4 ----
3 Aerial Deposition on River 7,093 7,093 7,093 7,093 < 2%< 2%< 2%< 2%----
4 Outfall 002 375,836 918,968 375,836 918,968 4 7 4 7 ----
5 Onsite Groundwater 2,309,468 2,164,439 2,309,468 2,164,439 22 17 23 17 ----
6A Seep A 967,485 1,325,336 967,485 1,325,336 9 10 9 11 ----
6B Seep B 1,683,557 1,038,907 1,683,557 1,038,907 16 8 17 8 ----
6C Seep C 215,507 282,525 215,507 282,525 2 2 2 2 ----
6D Seep D 494,879 467,789 494,879 467,789 5 4 5 4 ----
7 Old Outfall 002 2,417,156 3,750,579 2,417,156 3,750,579 23 29 24 30 ----
8 Offsite Groundwater 30,587 30,587 30,587 30,587 < 2%< 2%< 2%< 2%----
9 Georgia Branch Creek 390,334 405,836 196,581 193,863 4 3 2 2 2 2
10,377,814 12,755,093 10,184,061 12,543,120 100 100 100 100 ----
9,959,601 13,447,005 9,959,601 13,447,005 ------------
1 Up-Stream River 429,550 1,868,529 429,550 1,868,529 4 15 4 14 ----
2 Willis Creek 1,056,363 494,506 1,056,363 494,506 10 4 10 4 ----
3 Aerial Deposition on River 7,093 7,093 7,093 7,093 < 2%< 2%< 2%< 2%----
4 Outfall 002 375,836 918,968 375,836 918,968 4 7 4 7 ----
5 Onsite Groundwater 2,309,468 2,164,439 2,309,468 2,164,439 22 17 22 17 ----
6A Seep A 967,485 1,325,336 967,485 1,325,336 9 10 9 10 ----
6B Seep B 1,683,557 1,038,907 1,683,557 1,038,907 16 8 16 8 ----
6C Seep C 215,507 282,525 215,507 282,525 2 2 2 2 ----
6D Seep D 494,879 467,789 494,879 467,789 5 4 5 4 ----
7 Old Outfall 002 2,417,156 3,750,579 2,417,156 3,750,579 23 29 23 29 ----
8 Offsite Groundwater 30,587 30,587 30,587 30,587 < 2%< 2%< 2%< 2%----
9 Georgia Branch Creek 390,334 405,836 617,826 609,283 4 3 6 5 -2 -2
10,377,814 12,755,093 10,605,306 12,958,541 100 100 100 100 ----
9,959,601 13,447,005 9,959,601 13,447,005 ------------
Flow Rates for
Georgia Branch
Creek
Increased Georgia
Branch Creek Flow
by 50%
50% incease in Georgia
Branch Creek flow rate
increases estimated loading
by 2%
Total Estimated Mass Flux and Corresponding River Concentration
Measured Concentration and Calculated Mass Loading at Bladen Bluffs
Flow Rates for
Old Outfall 002
Increased Old Outfall
002 Flow by 100%
Estimated loading between
original and sensitivity
model increased by 16% to
21%
Total Estimated Mass Flux and Corresponding River Concentration
Measured Concentration and Calculated Mass Loading at Bladen Bluffs
Flow Rates for
Georgia Branch
Creek
Decreased Flow by
50%
Estimated loading between
original and sensitivity
model decreased by 2%
Total Estimated Mass Flux and Corresponding River Concentration
Measured Concentration and Calculated Mass Loading at Bladen Bluffs
Page 4 of 5 August 2019
TABLE F-1
SUMMARY OF SENSTIVITY ANALYSIS RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC, P.C.
May-19 Jun-19 May-19 Jun-19 May-19 Jun-19 May-19 Jun-19 May-19 Jun-19
Empirical Total
Table 3+
Estimated
Loading
(%)
Modeled Total
Table 3+
Estimated
Loading
(%)
[Original -
Sensitivty]
(%)ObservationsSensitivity
Scenario Descirption
Transport
Pathway
Number
Potential PFAS Transport Pathway
Calibrated, Original Total
Table3+ Mass Loading
Estimate
(ng/s)
Modeled Sensitivty Total
Table 3+ Mass Loading
Estimate
(ng/s)
9,289,800 11,667,623 -------------7 -13
9,959,601 13,447,005 ----------------
11,529,828 13,906,533 ------------16 3
9,959,601 13,447,005 ----------------
10,339,952 12,717,236 -------------0.2 -0.2
10,364,058 12,741,341 ----------------
1 Up-Stream River 429,550 1,868,529 2,610,860 3,130,323 4%15%25%22%-20%-8%
2 Willis Creek 1,056,363 494,506 1,056,363 494,506 10%4%10%4%----
3 Aerial Deposition on River 7,093 7,093 7,093 7,093 < 2%< 2%< 2%< 2%----
4 Outfall 002 375,836 918,968 375,836 918,968 4%7%4%7%----
5 Onsite Groundwater 2,309,468 2,164,439 2,309,468 2,164,439 22%17%22%17%----
6A Seep A 967,485 1,325,336 967,485 1,325,336 9%10%9%10%----
6B Seep B 1,683,557 1,038,907 1,683,557 1,038,907 16%8%16%8%----
6C Seep C 215,507 282,525 215,507 282,525 2%2%2%2%----
6D Seep D 494,879 467,789 494,879 467,789 5%4%5%4%----
7 Old Outfall 002 2,417,156 3,750,579 2,417,156 3,750,579 23%29%23%29%----
8 Offsite Groundwater 30,587 30,587 30,587 30,587 < 2%< 2%< 2%< 2%----
9 Georgia Branch Creek 390,334 405,836 390,334 405,836 4%3%4%3%----
10,377,814 12,755,093 10,605,306 14,016,887 ------------
9,959,601 13,447,005 9,959,601 13,447,005 ------------
Notes:
- ng/s: nanograms per second
- %: percent
1. For each sensitivity test, one of the above Transport Pathway inputs to the calibrated model is varied and the resulting model estimated Total Table 3+ PFAS mass loading is compared with the original calibrated model Total Table 3+ PFAS mass loading.
Upstream
Concentrations
Changed CFR-RM-76
sample non-detect
concentrations from
zero to method
detection limit
Total Estimated Mass Flux and Corresponding River Concentration
Measured Concentration and Calculated Mass Loading at Bladen Bluffs
Up-stream River Tranpost
Pathway increased 8 - 20%
when changing non-detect
samples from zero to
method detection limit.
Changed offsite
hydraulic conductivity
value from 2.5 x 10-4
m/s to 1 x 10-6 m/s
Total Estimated Mass Flux and Corresponding River Concentration 2 order of mag increase in
offsite K value - less than
0.2% change in mass
loadingMeasured Concentration and Calculated Mass Loading at Bladen Bluffs
On site
groundwater
Off site
groundwater
Discharge length
varied from 52% -
41%
Total Estimated Mass Flux and Corresponding River Concentration 9% decrease in discharge
length < 4% decrease in
total mass loadingMeasured Concentration and Calculated Mass Loading at Bladen Bluffs
Discharge length
varied from 41% -
76%
Total Estimated Mass Flux and Corresponding River Concentration 35% increase in discharge
length < 16% increase in
total mass loadingMeasured Concentration and Calculated Mass Loading at Bladen Bluffs
Page 5 of 5 August 2019
ATTACHMENT 2:
Seeps and Creeks Investigation Report

SEEPS AND CREEKS INVESTIGATION
REPORT
Prepared for
The Chemours Company FC, LLC 22828 NC Highway 87
Fayetteville, NC 28306

Prepared by
Geosyntec Consultants of NC, P.C.
2501 Blue Ridge Road, Suite 430
Raleigh, NC 27607
Geosyntec Project Number TR0795

August 26, 2019

Seeps and Creeks Investigation Report ii August 26, 2019

TABLE OF CONTENTS
1. INTRODUCTION ................................................................................................ 1
1.1 Site Setting ................................................................................................... 1
1.2 Objectives .................................................................................................... 4
1.3 Scope of Work ............................................................................................. 5
1.4 Report Organization .................................................................................... 5
2. SCOPE AND METHODS .................................................................................... 7
2.1 Scope of Field Events .................................................................................. 7
2.1.1 February 2019 Event ....................................................................... 7
2.1.2 May 2019 Event .............................................................................. 7
2.1.3 June 2019 Event .............................................................................. 8
2.2 Field Methods .............................................................................................. 9
2.2.1 General Field Procedures ................................................................ 9
2.2.2 Decontamination Methods .............................................................. 9
2.2.3 Sample Shipping, Chain of Custody, and Holding Times .............. 9
2.2.4 Field QA/QC ................................................................................. 10
2.2.5 Creek and Seep Sample Collection Methods ................................ 10
2.2.6 Cape Fear River Water Sample Collection Methods .................... 10
2.2.7 Seep Identification Methods ......................................................... 10
2.2.8 Flow Measurement Methods ......................................................... 11
2.2.9 Documentation .............................................................................. 12
2.3 Laboratory Methods .................................................................................. 12
2.3.1 Analytical Methods ....................................................................... 12
2.3.2 Laboratory QA/QC........................................................................ 13
3. RESULTS AND OBSERVATIONS .................................................................. 14
3.1 Laboratory Analytical Data Quality .......................................................... 14
3.1.1 Data Management and Reporting.................................................. 15
3.1.2 QA/QC Samples ............................................................................ 15
3.2 Results ....................................................................................................... 16
3.2.1 Analytical Laboratory Compound Reporting Limits .................... 17
3.2.2 Flow Gauging Limitations and Assumptions ................................ 18
3.3 Observations .............................................................................................. 18

Seeps and Creeks Investigation Report iii August 26, 2019

3.3.1 February 2019 Event ..................................................................... 19
3.3.2 May 2019 Event ............................................................................ 19
3.3.3 June 2019 Event ............................................................................ 19
3.3.4 Cape Fear River Concentrations ................................................... 20
3.3.5 Flow Observations ........................................................................ 21
4. SUMMARY AND PLANNED FUTURE ACTIONS ....................................... 22
5. REFERENCES ................................................................................................... 24

Seeps and Creeks Investigation Report iv August 26, 2019

LIST OF TABLES
Table 1: Location Summary
Table 2: PFAS and Associated Analytical Methods
Table 3: Total Daily Precipitation – February, May, and June 2019
Table 4: Analytical Results
Table 5: Stream Bed Temperature Survey Results
Table 6A: Total Table 3+ Concentrations
Table 6B: HFPO-DA Concentrations
Table 7: Flow Measurement Summary
Table 8A: Estimated Flow Rates – Seeps A to D, Georgia Branch Creek, and Willis Creek
Table 8B: Estimated Flow Rates – Old Outfall 002

Seeps and Creeks Investigation Report v August 26, 2019

LIST OF FIGURES
Figure 1: Site Location and Site Features
Figure 2A: Sample and Flow Measurement Locations – February 2019 Event
Figure 2B: Sample and Flow Measurement Locations – May 2019 Event
Figure 2C: Sample and Flow Measurement Locations – June 2019 Event
Figure 3A: Identified Seeps – Seeps A and B
Figure 3B: Identified Seeps – Old Outfall 002 and Seeps C and D
Figure 4A: Total Table 3+ Concentrations – February 2019 Event
Figure 4B: Total Table 3+ Concentrations – May 2019 Event
Figure 4C: Total Table 3+ Concentrations – June 2019 Event
Figure 5A: HFPO-DA Concentrations – February 2019 Event
Figure 5B: HFPO-DA Concentrations – May 2019 Event
Figure 5C: HFPO-DA Concentrations – June 2019 Event
Figure 6A: Cape Fear River Total Table 3+ Concentrations – February, May, and June
2019 Events
Figure 6B: Cape Fear River HFPO-DA Concentrations – February, May, and June 2019
Events

Seeps and Creeks Investigation Report vi August 26, 2019

LIST OF APPENDICES
Appendix A: Field Photograph Record
Appendix B: Field Parameters
Appendix C: Infrared Photograph Record
Appendix D: Flow Velocity Measurement Summary
Appendix E: Salt Dilution Gauging Summary
Appendix F: Temporary Weir Installation Summary
Appendix G: Laboratory Reports & DVM Report

Seeps and Creeks Investigation Report vii August 26, 2019

ACRONYMS AND ABBREVIATIONS
COC – Chain of Custody
DFSA – Difluoro-sulfo-acetic acid
DQO – data quality objectives
DVM – Data Verification Module
EIM – Environmental Information Management
ft bgs – feet below ground surface
GPM – gallons per minute
HDPE – High Density Polyethylene
HFPO-DA – Hexafluoropropylene oxide dimer acid
mL – Milliliter
MMF – Difluoromalonic acid
MS – Matrix spike
MSD – Matrix spike duplicate
MSL – mean sea level
MTP – Perfluoro-2-methoxypropanoic acid
NCDEQ – The North Carolina Department of Environmental Quality
ng/L – Nanograms per liter
NVHOS - Perfluoroethoxysulfonic acid
PFAS – Per- and polyfluoroalkyl substances
PFO5DA – Perfluoro(3,5,7,9,11-pentaoxadodecanoic) acid
PPF Acid – Perfluoropropionic acid
QA/QC – Quality assurance/ quality control
RPD – Relative percent difference
SOP –Standard Operating Procedure
µS/cm – microsiemens per centimeter
WWTP – wastewater treatment plant

Seeps and Creeks Investigation Report August 26, 2019

Seeps and Creeks Investigation Report 1 August 26, 2019

1. INTRODUCTION
This report was prepared by Geosyntec Consultants of NC, P.C. (Geosyntec) for The
Chemours Company FC, LLC (Chemours) to provide a summary of assessment activities
conducted to evaluate flow rates and concentrations of per- and polyfluoroalkyl
substances (“PFAS”) in seeps and creeks in the vicinity of the Chemours Fayetteville
Works, North Carolina site (the Site, Figure 1). This report was prepared to support the
PFAS mass loading evaluation prepared pursuant to Paragraph 12(a) in the executed
Consent Order entered February 25, 2019 between Chemours and the North Carolina
Department of Environmental Quality (NCDEQ) with the Cape Fear River Watch as
intervenor.
1.1 Site Setting
The Site is located in the northwestern portion of Bladen County and southern portion of
Cumberland County about 20 miles from Fayetteville, NC. Chemours operates two
manufacturing areas on the Site, the Chemours Monomers IXM Area and the Polymer
Processing Aid Area (PPA Area). Chemours also operates the wastewater treatment plant
(WWTP) and Power Area at the Site; filtered water and demineralized water are produced
in the Power Area. Two tenants also operate on the Site; Kuraray America Inc. (Kuraray)
and E.I. du Pont de Nemours and Company (DuPont).
The land surface is relatively flat in the manufacturing areas of the Site and slopes down
a bluff with about a 100-foot change in elevation towards the Cape Fear River on the east
side of the Site. To the north of the Site, the property slopes towards Willis Creek, which
is a tributary that discharges to the Cape Fear River. To the south of the manufacturing
area is the Old Outfall Channel, which also discharges to the Cape Fear River. Further
south, off the Site, is Georgia Branch Creek which is a tributary to the Cape Fear River.
Site Geology
As described by Parsons (2018), Bladen County is within the Coastal Plain Physiographic
Province, which consists of a seaward thickening wedge of sedimentary deposits ranging
in age from Cretaceous to Recent. Paleozoic metamorphic and igneous rocks underlie
these deposits. The Site is underlain by the Black Creek Formation, which is characterized
by lignitic clay with thin beds and laminae of fine-grained micaceous sand as well as thick
lenses of cross-bedded sand. The upper portion of the formation may also contain
glauconitic, fossiliferous clayey sand lenses. The Black Creek Formation and surficial
deposits are the principal potable water aquifers in the region.

Seeps and Creeks Investigation Report 2 August 26, 2019

Based on the lithology logged during previous on-site investigations, the Site is underlain
by a fine- to medium-grained sand unit with thin discontinuous interbedded silt/clay
lenses. The sand extends to a depth of approximately 65 feet below ground surface (ft
bgs) (elevation of +80 feet mean sea level, MSL). The saturated portion of this unit has
been identified as the Surficial Aquifer. Beneath this unit is a 7- to 15-foot-thick, laterally-
continuous dense clay that has been identified as the Black Creek Confining Unit.
The elevation of this unit (approximately +65 to +77 ft MSL) indicates that it, too, should
outcrop along the bluff face adjacent to the Cape Fear River, and potentially along the
embankment near Willis Creek. Beneath this confining unit is the Black Creek Aquifer,
which is approximately 8 to 20 ft thick and is encountered at depth between 80 and 100
ft bgs (elevation of approximately +45 to +65 ft MSL) at the top of the bluff. Beneath this
aquifer is a massive dense clay (with minor sand stringers) that has been identified as the
Upper Cape Fear Confining Unit. This unit was not fully penetrated at the Site; however,
it extended to at least 200 ft bgs (elevation of -55 ft MSL).
Beneath the manufacturing area, the uppermost sand unit is locally bisected by an aerially
extensive stiff clay lens. This clay lens is limited in lateral extent to the east, north and
south by local topography and pinches out (terminates) to the west of the manufacturing
area. The depth to the top of the clay lens is approximately 15 to 18 ft bgs. The clay lens
becomes thinner moving west across the manufacturing area and ranges from
approximately one foot to approximately 19 feet (ft) thick.
Site Hydrogeology
The hydrogeology of the Site includes a perched water zone and two aquifers; the Perched
Zone, the Surficial Aquifer and the Black Creek Aquifer.
The Perched Zone is aerially limited and generally is located above the top of a
discontinuous clay layer present in the manufacturing area. Based on recent investigations
and on-going evaluations, the Perched Zone may have been influenced by seepage of
water through the previously unlined sedimentation basins and infiltration of non-contact
cooling water from previously unlined drainage ditches. In 2018, the sedimentation basins
and cooling water channel were lined. Where perched water is present, it is encountered
from between 6 to 20 ft bgs. The lateral extent of the Perched Zone is controlled by
topography and the lateral extent of the clay lens.
The Surficial and Black Creek Aquifers are mostly separated by the Black Creek
confining unit, a clay layer. This clay layer is not fully confining as geological and
geochemical data indicate water and PFAS transfer has occurred from the Surficial

Seeps and Creeks Investigation Report 3 August 26, 2019

Aquifer to the Black Creek Aquifer. The Black Creek Aquifer is the uppermost identified
regional hydrogeologic unit. Flow in the Black Creek Aquifer is toward the Cape Fear
River. The Cape Fear River stage is also lower than the base of the Black Creek Aquifer,
indicating that the Cape Fear River is also a discharge boundary for the Black Creek
Aquifer.
Below the Black Creek Aquifer is the Upper Cape Fear Confining Unit. This clay is over
30-ft thick and is an aquitard to potential further downward flow based on limited on Site
geological borings and USGS groundwater wells at the Site that demonstrate minimal
hydraulic connection between the Black Creek Aquifer and the Upper Cape Fear Aquifer.
The Surficial Aquifer is a shallow unconfined aquifer encountered at approximately 50 ft
bgs. Groundwater elevations range from approximately 100 to 107 ft above MSL in the
western areas of the Site to approximately 93 ft above MSL in the eastern areas of the
Site, indicating that groundwater flow is generally toward the Cape Fear River. The Cape
Fear River stage is typically near +30 ft MSL, which is lower than the base elevation of
the Surficial Aquifer, indicating that the Cape Fear River is a discharge boundary for the
Surficial Aquifer. Based on groundwater elevations near Willis Creek, portions of the
creek are “gaining” (groundwater discharges to the creek) and portions are “losing”
(surface water infiltrates to the underlying groundwater). Georgia Branch Creek also
appears to be a gaining stream near where State Road 1303 crosses Highway 87.
The focus of this report is to further assess the bluff and evaluate if groundwater is
contributing to the seeps.
PFAS Originating from the Site
PFAS is a term used for a group of man-made carbon-based chemicals composed of a
fully or partially fluorinated chain of carbon atoms (referred to as a “tail”) at one end of
the carbon chain and a nonfluorinated, polar functional group (referred to as a “head”) at
the other end. Recent estimates (Wang et. al., 2017) suggest over 3,000 PFAS are or have
been produced across various industries and for various applications. Chemours
manufactures per- and polyfluoroalkyl ether compounds and polymers at the Site. The
PFAS originating from the Chemours Fayetteville Works Site are characterized primarily
by the presence of ether bonds, i.e. two carbons connected by an oxygen atom. To date
twenty-four (24) PFAS compounds that are present in Site process water have been
identified and had reference standards produced (Geosyntec, 2019a). Of these twenty-
four (24) compounds, analytical methods exist for twenty (20), the Table 3+ SOP method,
with methods presently being developed for the remaining four (4) compounds [Difluoro-
sulfo-acetic acid (DFSA), Difluoromalonic acid (MMF), Perfluoro-2-methoxypropanoic

Seeps and Creeks Investigation Report 4 August 26, 2019

acid (MTP) and Perfluoropropionic acid (PPF Acid)]. PFAS from other sources are also
present in the Cape Fear River (Geosyntec, 2018). The current grouping of Table 3+
PFAS, including Hexafluoropropylene oxide dimer acid (HFPO-DA) which can also be
analyzed by other methods, is used to represent PFAS loads originating from the facility
Before modifying operations, PFAS associated with the Site were released through a
range of pathways, including: (i) to air via air emissions, (ii) to surface water via Outfall
002, and (iii) to soil and groundwater from piping that has either been replaced or will be
replaced as described later in this Reduction Plan. These PFAS releases have resulted in
PFAS being detected in environmental media both onsite and offsite. Geosyntec
developed a mass loading model (Geosyntec, 2019b) pursuant to Consent Order
Paragraph 12 that assesses relative PFAS loading contributions from nine different
transport pathways.
1.2 Objectives
Paragraph 12(a) of the Consent Order requires that Chemours develop a plan to achieve
the maximum reductions in PFAS loading from the Site to the Cape Fear River that are
economically and technically feasible within a two-year period. Development of this plan
required evaluation of PFAS loadings from the Site that reach the Cape Fear River. While
other investigations are evaluating PFAS loadings from Outfall 002 at the Site, it was also
necessary to understand potential PFAS loadings from other pathways in the vicinity of
the Site. These pathways included Old Outfall 002, creeks upstream and downstream of
the site (Willis Creek and Georgia Branch Creek, respectively) and groundwater seeps
north, east, and south of the manufacturing area. Several groundwater seeps were
observed at and downgradient of the bluff on the eastern side of the Site, and others were
observed along the reaches of Old Outfall 002, Willis Creek, and Georgia Branch Creek.
Flow from these seeps and creeks may contribute PFAS loading to the Cape Fear River
separate from the contribution due to Outfall 002. The Seeps and Creeks Investigation
was implemented to evaluate PFAS loading from the Site to the Cape Fear River
associated with the seeps and creeks.
In order to evaluate mass loading from seeps and creeks, Chemours and its contractors
conducted three rounds of sample collection and flow measurements in February, May,
and June 2019. The field effort was conducted according to the following workplans:
• Creeks, Old Outfall 002 and Seeps Assessment Workplan (Geosyntec, 2019c);
• Additional Creeks, Old Outfall 002 and Seeps Investigation Plan (Geosyntec,
2019d); and

Seeps and Creeks Investigation Report 5 August 26, 2019

• Willis Creek and Seep D Assessment Plan (Geosyntec, 2019e)
The objectives of the Seeps and Creeks Investigation were as follows:
• Identify seeps and creeks in the vicinity of the Site that enter the Cape Fear River;
• Assess the base volumetric flow rate of seeps and creeks entering the Cape Fear
River at and near the Site;
• Assess gain in stream flow of the creeks and seeping water flow towards the Cape
Fear River;
• Assess PFAS concentrations in waters to obtain more information on PFAS mass
loading as it pertains to the Cape Fear River during wet and dry conditions;
• Assess regions of groundwater upwelling near the stream bed in Willis Creek,
Georgia Branch Creek, Old Outfall 002, and the channels with flowing water from
seeps.
1.3 Scope of Work
The Seeps and Creeks Investigation was conducted during field events in February, May,
and June 2019. Activities conducted to support the Seeps and Creeks Investigation were
as follows:
• Collecting water samples from seeps, creeks, and the Cape Fear River for PFAS
during wet and dry conditions;
• Gauging seep and creek volumetric flow during wet and dry conditions;
• Assessing temperature contrasts near the stream bed to aid in identification of
areas of groundwater upwelling; and
• Observing stream channels to visually identify areas of groundwater seepage.

Further details on scope conducted for each field event are described in Section 2.1
below.
1.4 Report Organization
The remainder of this document is organized as follows:
Section 2 – Scope and Methods: This section describes the scope of work conducted
during each field event and the methods implemented in the field and laboratory;
Section 3 – Results and Observations: This section presents the results of the Seeps and
Creeks Investigation and discusses the results in the context of the investigation
objectives;

Seeps and Creeks Investigation Report 6 August 26, 2019

Section 4 – Summary and Planned Future Actions: This section summarizes the
findings of the Seeps and Creeks Investigation and describes additional planned efforts
related to the seeps and creeks; and
Section 5 – References: This section lists the references used in this report.

Seeps and Creeks Investigation Report 7 August 26, 2019

2. SCOPE AND METHODS
This section describes the methods implemented during the Seeps and Creeks
Investigation as well as the scope of work conducted during each field event. A photo log
is provided in Appendix A, showing select seep areas and activities.
2.1 Scope of Field Events
2.1.1 February 2019 Event
The February 2019 Event was completed by Geosyntec and Parsons of North Carolina
Inc. (Parsons) according to the Creeks, Old Outfall 002 and Seeps Assessment Workplan
(Geosyntec, 2019c) between February 1 and 7, 2019. Sampling and flow gauging
locations are shown on Figure 2A and listed in Table 1. Compounds evaluated as part of
this field event are listed in Table 2. Samples for PFAS analysis were collected at thirty-
eight locations, and flow rates were measured at fifteen locations. In the three days (72
hours) preceding the start of this field event 0.09 inches of rain was measured in the
vicinity of the Site; otherwise there was no measurable precipitation during this event
(Table 3). The February 2019 Event was considered a dry weather event for the purposes
of the Seeps and Creeks Investigation, since there was a continuous period of 72 hours
without rainfall greater than 0.25 inches prior to sample collection.
Samples were collected for PFAS analysis from locations in Seep A, Seep B, Seep C, Old
Outfall 002, Willis Creek, and the Cape Fear River (Figure 2A). Flow gauging
measurements were conducted at locations in Seep A, Seep B, Seep C, Old Outfall 002,
and Willis Creek. Flow was measured at these locations using salt dilution gauging and
flow velocity gauging. Temperature contrasts between groundwater and surface water
were assessed in Old Outfall 002 using a submersible temperature probe and an infrared
camera.
2.1.2 May 2019 Event
The May 2019 Event was completed by Geosyntec and Parsons according to the Creeks,
Old Outfall 002 and Seeps Assessment Workplan (Geosyntec, 2019c) and the Additional
Creeks, Old Outfall 002 and Seeps Investigation Plan (Geosyntec, 2019d) between May
20 and 30, 2019. Sampling and flow gauging locations are shown on Figure 2B and listed
in Table 1. Compounds evaluated as part of this field event are listed in Table 2. Samples
for PFAS analysis were collected at thirty-eight locations, and flow rates were measured
at eleven locations. On the first day of this sampling event, approximately 0.24 inches of
rain was measured in the vicinity of the Site; otherwise there was no measurable

Seeps and Creeks Investigation Report 8 August 26, 2019

precipitation during this event (Table 3). The May 2019 Event was considered a dry
weather event for the purposes of the Seeps and Creeks Investigation, since there was a
continuous period of 72 hours without rainfall greater than 0.25 inches prior to sample
collection.
Samples were collected for PFAS analysis from locations in Seep A, Seep B, Seep C,
Seep D, Old Outfall 002, Willis Creek, Georgia Branch Creek, the Cape Fear River, the
excess river water location, and Outfall 002. Flow gauging measurements were conducted
at locations in Seep A, Seep B, Seep C, Seep D, Old Outfall 002, Willis Creek, and
Georgia Branch Creek. Flow was measured at these locations using salt dilution gauging,
flow velocity gauging, and temporary weir installation. Additional areas were inspected
for other channelized seeps that may reach the Cape Fear River so that they could be
incorporated into the investigation.
2.1.3 June 2019 Event
The June 2019 Event was completed by Geosyntec and Parsons according to the Creeks,
Old Outfall 002 and Seeps Assessment Workplan (Geosyntec, 2019c), the Additional
Creeks, Old Outfall 002 and Seeps Investigation Plan (Geosyntec, 2019d), and the Willis
Creek and Seep D Assessment Plan (Geosyntec, 2019e) on June 7, 2019. Sampling and
flow gauging locations are shown on Figure 2C and listed in Table 1. Compounds
evaluated as part of this field event are listed in Table 2. Samples for PFAS analysis were
collected at seventeen locations, and flow rates were measured at sixteen locations. In the
two days (48 hours) preceding the start of the sampling event approximately 0.8 inches
of rain was measured in the vicinity of the Site; otherwise there was no measurable
precipitation during this event (Table 3). The June 2019 Event was considered a wet
weather event for the purposes of the Seeps and Creeks Investigation, since there was
greater than 0.25 inches of rain in the 72 hours prior to sample collection.
Samples were collected for PFAS analysis from locations in Seep A, Seep B, Seep C,
Seep D, Old Outfall 002, Willis Creek, Georgia Branch Creek, the Cape Fear River, the
excess river water location, and Outfall 002. Flow gauging measurements were conducted
at locations in Seep A, Seep B, Seep C, Seep D, Old Outfall 002, Willis Creek, and
Georgia Branch Creek. Flow was measured at these locations using salt dilution gauging,
flow velocity gauging, and temporary weir installation.

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2.2 Field Methods
2.2.1 General Field Procedures
All equipment was inspected by the field program supervisor and calibrated daily prior
to use in the field according to the manufacturer’s recommendations. Samples were
collected for PFAS analysis before flow rate assessment. Samples were collected in 250
milliliter (mL) high density polyethylene (HDPE) bottles with a wide-mouth screw-cap.
Sample bottles were filled and caps were securely fastened after sample collection. Each
sample was labeled with a unique sample identification number, date, time and location
of sampling, and the initials of the individual collecting the sample. A field notebook was
used to record information regarding additional items such as quality assurance/ quality
control (QA/QC), sample identifications, color, odor, turbidity, and other field
parameters. Field parameters recorded from the sampling events are provided in
Appendix B.
2.2.2 Decontamination Methods
Sample containers were new and used only once for each sample. Disposable equipment
(e.g., gloves, tubing, etc.) was not reused, therefore; these items did not require
decontamination.
All non-dedicated or non-disposable sampling equipment was decontaminated
immediately before sample collection in the following manner:
• De-ionized water rinse;
• Scrub with de-ionized water containing non-phosphate detergent (i.e.,
Alconox®); and
• De-ionized water rinse.
2.2.3 Sample Shipping, Chain of Custody, and Holding Times
Upon sample collection, each labeled, containerized sample was placed into a heavy
plastic bag inside an insulated sample cooler with ice. Prior to shipment of the samples
to the laboratory, a chain of custody (COC) form was completed by the field sample
custodian. Sample locations, sample identification numbers, description of samples,
number of samples collected, and specific laboratory analyses to be performed on the
samples were recorded on the COC form. The COC was signed by the field personnel
relinquishing the samples to the courier and was signed by the laboratory upon receipt of
the cooler.

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2.2.4 Field QA/QC
The following field QA/QC samples were collected and analyzed along with the
investigative samples:
• February 2019 Event
o One equipment blank
o Six field blanks
• May 2019 Event
o Three equipment blanks
o Seven field blanks
o Five field duplicates
• June 2019 Event
o One equipment blank
o One field blank
o One field duplicate
2.2.5 Creek and Seep Sample Collection Methods
Creek and seep water samples were collected as grab samples. Sample bottles were
lowered into the flowing water of the creek to collect the sample. The bottles were
lowered into the stream either using a properly decontaminated dip rod with bottle
attached with a nylon zip tie, or in shallow streams, by hand. The bottle was lowered into
the stream with the cap removed, open and facing oncoming flow. Where possible, the
sample was collected from the middle of the stream. Care was taken to avoid collecting
suspended solids or other materials in the sample.
2.2.6 Cape Fear River Water Sample Collection Methods
Cape Fear River water samples were collected using a peristaltic pump and new dedicated
HDPE tubing and dedicated silicone tubing for the pump head at each location. The
tubing was lowered to the specified sampling depth below the water surface using an
anchor weight and the tubing fastened to the anchor pointing upwards. Surface water was
pumped directly from the submerged tubing through the pump head to a sample bottle.
2.2.7 Seep Identification Methods
Seeps were identified for incorporation into the investigation by visual inspection and via
temperature assessment.

Seeps and Creeks Investigation Report 11 August 26, 2019

Visual Inspection
Areas downgradient of the Site were inspected visually for channelized seeps. Such seeps
were photographed and geolocated, and a sample was collected from the mouth of the
seep before it reaches the river. Flow gauging was conducted at such locations using a
weir, depending on site conditions.
Temperature Assessment
Areas of groundwater upwelling into surface water bodies were assessed using
temperature differentials of groundwater versus surface water. Areas of upwelling were
identified by placing a submersible temperature probe at the bottom of the stream and
recording the temperature. If the temperature is similar to surface water temperatures,
then the stream may not be in a zone of upwelling. However, if the stream bottom
temperatures are different than surface water, groundwater is likely upwelling in this
zone. Areas of upwelling were also identified by taking photographs of streams using an
infrared camera where the water column was shallow enough to observe temperature
differentials. The temperature assessment was only completed on Old Outfall 002 and
only in the February event. In May and June, the temperature differences between
groundwater and surface water were too similar, and the presence of seeping groundwater
had been previously been identified in the February event in all seeps features. Infrared
photographs are provided in Appendix C. Temperature assessments were conducted at
Old Outfall 002 during part of the February Event (Table 1), on days when the ambient
temperature was cool enough for the surface water/ groundwater temperature gradient to
be observable. Otherwise, seeps were identified visually.
2.2.8 Flow Measurement Methods
Flow rate was measured after sample collection by one or more of several methods,
depending on stream bed geometry, stream morphology, site accessibility, and health and
safety considerations.
Flow Velocity Gauging
The flow rate of the streams can be measured using a submersible flow meter in deeper
(greater than one foot deep), less turbulent and more laminar flow sections of streams.
The height of the water and stream bottom is first recorded from a uniform reference
plane along the cross section of the stream at a minimum of 4 points along each transect.
The flow meter is placed beneath the flowing stream along the cross section of the stream
at regular intervals (e.g. 4-5 points along each transect) and the water velocity is recorded

Seeps and Creeks Investigation Report 12 August 26, 2019

at a minimum of 3 water depths at each point along the transect (e.g. top-third, middle-
third and bottom-third of the water column). These measurements are then used to
calculate the volumetric flow of water passing through the feature based on the geometry
and measured flow rates. A description of flow velocity measurement data is provided in
Appendix D.
Salt Dilution Streamflow Gauging
The flow of streams can be measured by dosing at a constant flow rate into the stream a
sodium chloride solution at a known concentration (Moore, 2004). Using a Mariotte
bottle or constant flow pump, the salt solution was dosed into the flowing stream at a
known flow rate. The relative concentration of salt in the stock solution and in the stream
was measured using a conductivity probe reporting the result in units of microsiemens
per centimeter (µS/cm). Using the known flow rate of the stock solution and the known
concentrations of the stream and stock solution, the flow rate of the stream was calculated.
Details on the salt dilution gauging data are provided in Appendix E.
Weir Installation
Temporary weirs were installed during the May and June events at some locations to
refine previous flow rate estimates determined by flow velocity gauging and salt dilution
streamflow gauging. Weirs were installed at accessible locations at the mouths of surface
water features where the channel was at least 1.5 feet wide. Weirs were driven into the
channel bottoms and sides and then stabilized. Water level, weir plate notch height from
the creek bed, horizontal distance of the measurement point from the weir plate along the
creek channel, thickness of downstream water column, and creek width at the weir
installation location were recorded and used to calculate flow rate. Supporting details
on weir installation are provided in Appendix F.
2.2.9 Documentation
The project field team kept a daily record of field activities during the execution of field
work including sampling notes and observations, instrument calibration records, sample
COC, and shipping records.
2.3 Laboratory Methods
2.3.1 Analytical Methods
Samples were analyzed for PFAS by the following methods:

Seeps and Creeks Investigation Report 13 August 26, 2019

• Table 3+ Laboratory Standard Operating Procedure (SOP); and
• EPA Method 537 Mod (Laboratory SOP).
PFAS reported under each of these methods are listed in Table 2.
2.3.2 Laboratory QA/QC
Field sampling and laboratory analyses were performed in accordance with the Creeks,
Old Outfall 002 and Seeps Assessment Workplan (Geosyntec, 2019c). Samples were
collected by the field team and shipped to TestAmerica Sacramento (TestAmerica) or
Eurofins Lancaster Laboratories (Lancaster) under COC. Laboratory analyses were
performed within the guidelines specified by the laboratory SOPs. The collection
frequency of field duplicates, matrix spike / matrix spike duplicates (MS/MSD), field
blanks, and equipment blanks was largely in accordance with the Creeks, Old Outfall 002
and Seeps Assessment Workplan (Geosyntec, 2019c). In some instances, field QA/QC
sample collection deviated from the Workplan due to the significant amount of equipment
and bottleware that the field team needed to carry with them. Flow measurement and
collection of investigative samples were deemed the top priorities. Sufficient field
QA/QC samples were collected to evaluate the data quality.

Seeps and Creeks Investigation Report 14 August 26, 2019

3. RESULTS AND OBSERVATIONS
Over three field events (February, May and June 2019) field teams identified four seeps,
of varying size and reach discharging directly from the Site to the Cape Fear River. These
seeps (A to D), Old Outfall 002 and Willis and Georgia Branch Creeks were gauged for
flow, and samples collected to assess PFAS concentrations. Sampling was conducted
under wet and dry conditions. In total 94 discrete water samples were collected from the
seeps and creeks for PFAS analysis. A temperature survey of Old Outfall 002 was
conducted to evaluate temperature variations as an indicator for groundwater upwelling.
3.1 Laboratory Analytical Data Quality
All data were reviewed using the Data Verification Module (DVM) within the LocusTM
Environmental Information Management (EIM) system, which is a commercial software
program used to manage data. Following the DVM process, a manual review of the data
was conducted. The DVM and the manual review results were combined in a data review
narrative report for each set of sample results, which were consistent with Stage 2b of the
EPA Guidance for Labeling Externally Validated Laboratory Analytical Data for
Superfund Use (EPA-540-R-08-005 2009). The narrative report summarizes which
samples were qualified (if any), the specific reasons for the qualification, and any
potential bias in reported results. The data usability, in view of the project’s data quality
objectives (DQOs), was assessed and the data were entered into the EIM system.
The data were evaluated by the DVM against the following data usability checks:
• Hold time criteria;
• Field and laboratory blank contamination;
• Completeness of QA/QC samples;
• MS/MSD recoveries and the relative percent differences (RPDs) between these
spikes;
• Laboratory control sample/control sample duplicate recoveries and the RPD
between these spikes;
• Surrogate spike recoveries for organic analyses; and
• RPD between field duplicate sample pairs.
The manual review includes instrument-related QC results for calibration standards,
blanks, and recoveries. The data review process (DVM plus manual review) applied the
following data evaluation qualifiers to analysis results, as warranted:

Seeps and Creeks Investigation Report 15 August 26, 2019

• J – Analyte present. Reported value may not be accurate or precise;
• UJ – Analyte not detected. Reporting limit may not be accurate or precise; and
• B – Analyte detected in a blank sample. Reported value may have high bias.
The data review process described above was performed for all laboratory chemical
analysis data generated for the sampling events. The DQOs were met for the analytical
results for accuracy and precision. The data collected are believed to be complete,
representative, and comparable.
3.1.1 Data Management and Reporting
Chemours’s Analytical Data Quality Management team currently uses the EIM system
for management of analytical data, xyz Site coordinate data, and field parameter data.
Validation and qualification of data are performed by AECOM, who maintains the EIM
system for the Chemours Fayetteville Site. A whitebook consisting of the data review
narrative and the laboratory analytical report produced by AECOM summarizes the
findings of the DVM and manual review process (Appendix G).
3.1.2 QA/QC Samples
PFAS concentrations for all field QA/QC samples are reported in Table 4. The following
observations were noted for the QA/QC samples:
• No PFAS were detected above the associated reporting limits in the equipment
blanks submitted for analysis.
• No PFAS were detected above the associated reporting limits in the field blanks
submitted for analysis, with the following exceptions:
o Perfluoro-3,5,7,9,11-pentaoxadodecanoic acid (PFO5DA) was detected at
or above the associated reporting limit (34 nanograms per liter [ng/L]) in
one field blank collected in the February 2019 Event (370 ng/L) and in
two field blanks collected in the May 2019 Event (34 ng/L and 37 ng/L).
The February 2019 field blank result was J-qualified along with associated
investigative samples collected the same day. PFO5DA in the May 2019
field blanks were both detected at or within 5-times the reporting limit. No
further qualification was required.
o Byproduct 5 was detected at the reporting limit (58 ng/L) in one field blank
collected in the February 2019 Event. No further qualification was
required.

Seeps and Creeks Investigation Report 16 August 26, 2019

o HFPO-DA was detected within 5-times the reporting limit (1.8 ng/L) in
one field blank collected in the February 2019 Event (2.2 ng/L J). No
further qualification was required.
o Byproduct 1 was detected at the reporting limit (27 ng/L) in one field blank
collected in the May 2019 Event. No further qualification was required.
• The RPD for all field duplicate pairs was less than 30% for all PFAS, or less than
50% for PFAS detected within a factor of five of the associated reporting limits,
with the following exceptions:
o Byproduct 4 was detected at 20 ng/L in the parent sample FAY-SW-CFR-
KINGS-052319 and was non-detect at the reporting limit (2 ng/L) in the
associated field duplicate FAY-SW-CFR-KINGS-052319-D. The parent
sample FAY-SW-CFR-KINGS-052319 was J-qualified during the DVM
review as estimated.
o Byproduct 5 was detected at 2 ng/L in the parent sample FAY-SW-CFR-
RM-56-060719 and was detected at 4.5 ng/L in the associated field
duplicate FAY-SW-CFR-RM-56-060719-D. Both results were J-qualified
during the DVM review as estimated.
• In addition to data validation based on the field QA/QC results, field results were
qualified based on laboratory QA/QC results, as described in the laboratory
reports and DVM reports in Appendix G. Several results were J-qualified due to
laboratory hold time exceedances, discussed further below in Section 3.2. In
addition, some results, including those for some samples collected in the Cape
Fear River upstream of the Site, were J-qualified and biased high due to variable
matrix spike recoveries. These sample results are discussed further below in
Section 3.3.4.
3.2 Results
Seeps identified during the Seeps and Creeks Investigation are shown on Figures 3A and
3B. The summary of locations identified via temperature assessment are reported in Table
5. Temperature assessments were conducted at Old Outfall 002 during part of the
February Event (Table 1), on days when the ambient temperature was cool enough for
the surface water/ groundwater temperature gradient to be observable. Otherwise, seeps
were identified visually. Infrared photographs are provided in Appendix C. During some
days in the February event, the May, and June events, the potential temperature
differential was not significant enough to utilize this method to identify groundwater
upwelling, and the presence of seeping groundwater had previously been identified in the
February event in all seep features.

Seeps and Creeks Investigation Report 17 August 26, 2019

PFAS concentrations for samples collected during the Seeps and Creeks Investigation are
reported in Table 4. Total Table 3+ Laboratory SOP concentrations are also reported in
Table 4. Figures 4A, 4B, and 4C present the total Table 3+ Laboratory SOP
concentrations reported for samples collected in February, May, and June, respectively.
Figures 5A, 5B, and 5C present the HFPO-DA concentrations reported for samples
collected in February, May, and June, respectively. Figure 6A presents the total Table 3+
Laboratory SOP concentrations reported for samples collected from the Cape Fear River
in February, May, and June. Figure 6B presents the HFPO-DA concentrations reported
for samples collected from the Cape Fear River in February, May, and June. Table 6A
summarizes the total Table 3+ Laboratory SOP concentrations at select locations, and
Table 6B summarizes the HFPO-DA concentrations at select locations. Appendix G
provides the analytical reports and data review narrative whitebook for the Seeps and
Creeks Investigation.
Several Table 3+ analytical compound results were J-qualified, as estimated, due to
laboratory hold time exceedances. The hold time exceedances are largely due to
additional time required by the laboratories to complete method development of Table
3+. Since these hold time exceedances did not result in rejection of the results, the J-
qualified data still meet data quality standards and are usable as reported.
Calculated flow rates for all locations measured during the Seeps and Creeks
Investigation are reported in Table 7. Table 8A presents the estimated flow rates measured
for Seeps A through D and Georgia Branch Creek and Willis Creek, respectively, using
the specified flow gauging method during each field event. Table 8B presents the
estimated flow rates measured for Old Outfall 002 using available flow gauging
techniques during each field event. The estimated flow rates are determined based on the
geometric mean of field measurements.
3.2.1 Analytical Laboratory Compound Reporting Limits
Several PFAS reported in Table 4 were not detected at elevated reporting limits. The
laboratories originally ran the samples using the high-level analysis as a precaution
against instrumentation fouling. Now that more information on relative concentrations
have been identified, future collected water samples for Table 3+ compounds will be
analyzed at low-level analysis where appropriate which should provide lower reporting
limits.

Seeps and Creeks Investigation Report 18 August 26, 2019

3.2.2 Flow Gauging Limitations and Assumptions
The flow gauging methods used in this investigation depended upon stream bed
geometry, stream morphology, site accessibility, and health and safety considerations.
The following limitations and assumptions were noted during flow gauging activities that
may affect the accuracy of results. Table 7 identifies calculated flow rates that may be
inaccurate due to these limitations.
Flow velocity gauging is most accurate in deep, less turbulent and more laminar flow
sections of streams. This method depends on uniform water column thickness, so it
becomes inaccurate if water column thickness is variable. This is often difficult to observe
in deep or turbid water.
Salt dilution gauging becomes less accurate in streams with complex morphology and in
very shallow streams, since this method requires relatively uniform flow across the width
of a channel. Comparison of flow rates determined by salt dilution gauging to those
determined by other methods indicates that salt dilution gauging tended to estimate higher
flows when flows were less than 100 gallons per minute (GPM) and estimate lower flows
when flows were greater than 100 GPM relative to the other methods.
Weir gauging requires all flow in a stream be diverted towards the weir. Any flow under
or around the weir may lead to underestimates of flow rates. This is particularly
challenging in sandy streams where water can flow through the sandy substrate of the
stream bypassing the weir, and if there are tree roots or other debris present that can
provide a preferential flow pathway also bypassing the weir.
3.3 Observations
Several seeps were identified during the Seeps and Creeks Investigation (Figure 3A and
3B). Both Seep A and Seep B can be traced from near the top of the bluff at the Site
facilities down to the Cape Fear River. Seep C and Seep D both appear to begin farther
from the facility and closer to the Cape Fear River. During field investigations, an
additional branch of Seep A was identified, this surface water at this area is most likely
discharging water from the pump house (located just north of SEEP-A-5-B-1 to the main
section of Seep A as shown in Figure 3A). At Seep A, near location SEEP-A-3-B12,
runoff from the parking lot at Chemours Monomers IXM appeared to contribute water
flow to the seep (Figure 3A). Several seeps were also identified in Old Outfall 002, Willis
Creek, and Georgia Branch Creek (as identified in Figures 2A, 2B, and 2C).

Seeps and Creeks Investigation Report 19 August 26, 2019

3.3.1 February 2019 Event
The February 2019 event was a dry weather event. Elevated PFAS concentrations were
reported in samples collected from Seep A, Seep B, Seep C, and Old Outfall 002. In each
of the seeps, at least two samples collected were reported to have total Table 3+
compounds greater than 100,000 ng/L. Samples collected from Seep A, Seep B, and Seep
C were reported to have HFPO-DA concentrations typically between 10,000 ng/L and
100,000 ng/L, while samples collected from all locations along Old Outfall 002 were
reported to have concentrations less than 10,000 ng/L. Lower concentrations were
observed in Willis Creek, with total Table 3+ concentrations less than 2,200 ng/L. No
consistent trend was observed moving upgradient to downgradient in Seeps A, B, and C
and Old Outfall 002, while the samples collected from Willis Creek reported higher PFAS
concentration closer to the Cape Fear River. Samples were not collected from Seep D or
the portion of Seep A in the vicinity of the pump house during the February Event since
they had not been identified at that time. Samples were not collected from Georgia Branch
Creek due to delayed access approvals.
3.3.2 May 2019 Event
The May 2019 event was a dry weather event. Samples collected from Seep A, Seep B,
Seep C, and Old Outfall 002 had PFAS concentrations, similar to those observed in
February. Seep D was identified in May and samples collected and analyzed were
reported to have total Table 3+ compounds of approximately 170,000 ng/L. Samples were
also collected from the portion of Seep A in the vicinity of the pump house. The samples
analyzed from the water collected at these locations have total Table 3+ compound
concentrations similar to samples collected from other portions of Seep A. HFPO-DA
concentrations in samples collected from the seeps and Old Outfall 002 in May were
similar in magnitude to those collected in February. PFAS concentrations in the samples
collected from Willis Creek were higher in May than in February, with total Table 3+
compounds between 3,000 ng/L and 22,000 ng/L. PFAS concentrations in samples
collected along Georgia Branch Creek were observed to have total Table 3+ compounds
between 1,100 and 3,500 ng/L. Both the sample collected at the excess river water
location and the sample collected at Outfall 002 were non-detect for HFPO-DA in May,
with a reporting limit of 86 ng/L. All Table 3+ compounds were similarly non-detect.
Subsequent samples collected in June at these locations had improved reporting limits.
3.3.3 June 2019 Event
The June 2019 Event was a wet weather event. Samples were primarily collected from
the mouths of the seeps and creeks. PFAS concentrations in samples collected at these

Seeps and Creeks Investigation Report 20 August 26, 2019

locations were similar to those observed in February and May. The precipitation leading
up to the wet June event did not appear to affect PFAS concentrations in the seeps and
creeks. The sample collected at the excess river water location in June had total Table 3+
concentration of less than 130 ng/L with HFPO-DA reported at 28 ng/L. The sample
collected at Outfall 002 had total Table 3+ concentration of approximately 1,800 ng/L
with HFPO-DA reported at 40 ng/L. These results are similar to previous observations at
the excess river water location and Outfall 002.
3.3.4 Cape Fear River Concentrations
PFAS concentrations in the Cape Fear River are presented in Figure 6A and 6B. PFAS
concentrations reported from samples collected during the February Event are higher
downstream (River Mile 84) than upstream (River Mile 76) of the Site (e.g., HFPO-DA
concentration of 13 ng/L downstream and 2.9 J ng/L upstream). In May, upstream
samples collected at River Mile 56, 68, and 76 were non-detect at the reporting limit for
HFPO-DA. Downstream concentrations were higher, with HFPO-DA concentrations of
28 ng/L at Bladen Bluffs and 17 ng/L at Kings Bluff. In June, HFPO-DA concentrations
followed similar patterns to the May samples, with low to non-detect results upstream
and results between 30 and 60 ng/L downstream.
Other PFAS, particularly Byproduct 4, Byproduct 5, and perfluoroethoxysulfonic acid
(NVHOS) were observed in the upstream Cape Fear River samples in May and June 2019
at River Miles 56 and 68. The results for these compounds were J-qualified due to variable
recoveries in the matrix spikes outside the acceptable range defined in the SOP which
may cause the results to be overestimated. The detection of these compounds is not
consistent with known transport pathways for PFAS originating from the facility.
Specifically, in offsite groundwater, which is the transport pathway leading to upstream
detections attributable to aerial emissions of PFAS from the facility, PMPA is the
compound detected at the highest concentrations based on groundwater data reported in
the Post Florence Report (Geosyntec, 2019f). Therefore, PMPA is expected to be detected
first amongst the PFAS potentially reaching the river from offsite groundwater in the
upstream river samples. In samples from River Mile 56, only these three Table 3+
samples are detected. While closer to Site in the upstream river at River Mile 68 PMPA
is detected consistent with expected trends from offsite groundwater. These observations
of Byproduct 4, Byproduct 5 and NVHOS will be further evaluated spatially and
temporally through additional sampling events in the Cape Fear River to further
understand their concentration and distribution.

Seeps and Creeks Investigation Report 21 August 26, 2019

3.3.5 Flow Observations
Seeps A and B have larger reaches compared to Seeps C and D and they were observed
to have higher flow rates compared to Seeps C and Seep D. Flow rates at the mouths of
Seeps A and B were 60 to 110 GPM and 50 to 90 GPM, respectively, determined by salt
dilution gauging, while flow rates at the mouths of Seeps C and D were 10 to 15 GPM
and 20 to 50 GPM, respectively, determined by salt dilution gauging and weir gauging.
Flow rates in the seeps were variable between February, May, and June. Flow rates in
Willis Creek were highest in June compared to February and May, which may be related
to the precipitation observed prior to the June Event compared to the dry weather events
in February and May. As discussed in Section 3.2.2, there are limitations to each of the
flow gauging methods applied during the Seeps and Creeks Investigation. Table 7 and
Table 8B demonstrate the variability in flow gauge results across these methods due to
their limitations. The variability observed in the flow gauging results may be related to
these limitations, which provide a foundation for continued flow assessment to increase
understanding of seasonal variability and variability due to precipitation.

Seeps and Creeks Investigation Report 22 August 26, 2019

4. SUMMARY AND PLANNED FUTURE ACTIONS
This report provides a summary of the investigative activities and results of the Seeps and
Creeks Investigations, conducted in February, May, and June 2019. The objectives of
these field investigations were met. Seeps were identified, seep and creek flow rates
measured, upwelling in stream beds was assessed and water samples collected from the
seeps and creeks were analyzed for PFAS. These data further inform the site conceptual
model and provide empirical data for the mass loading model that is being developed.
Four seeps (A to D) on the western edge of the Cape Fear River were identified and
groundwater contributions to the seeps were investigated. Visual observations, flow
gauging and temperature surveys were used in various locations to assess seepage. Seeps
A and B have larger reaches compared to Seeps C and D and they were observed to have
higher flow rates compared to Seeps C and D. Flow rates at the mouths of Seeps A and
B were 60 to 110 GPM and 50 to 90 GPM, respectively, determined by salt dilution
gauging, while flow rates at the mouths of Seeps C and D were 10 to 15 GPM and 20 to
50 GPM, respectively.
Flow rates in the seeps were variable between February, May, and June. Flow rates in
Willis Creek were highest in June compared to February and May, which may be related
to the precipitation observed prior to the June Event compared to the dry events in
February and May.
In this program more than 90 samples from Seeps, Willis and Georgia Branch Creeks and
Old Outfall 002 were collected and analyzed for PFAS and Table 3+ compounds. The
results of these characterization activities indicate that the seeps and creeks contribute
PFAS load to the Cape Fear River. The results included in this report provide a
preliminary understanding of flow conditions in the seeps and PFAS concentrations from
these seeps and creeks that are reaching the Cape Fear River.
The contents of this report support the PFAS mass loading evaluation prepared pursuant
to Paragraph 12(a) in the executed Consent Order. The results of the Seeps and Creeks
Investigation provide data to inform the Mass Loading Model on the contributions of
PFAS from the seeps and Creeks to the Cape Fear River.
The seeps along the bluff were investigated. There are numerous locations within the
seeps where the temperature profiles indicate upwelling of groundwater. Multiple flow
gauging events were completed to understand the flow from the creeks and seeps.

Seeps and Creeks Investigation Report 23 August 26, 2019

In order to evaluate potential variability in flow and PFAS concentrations over time and
due to seasonality effects, Geosyntec recommends that a monitoring program continue
with six additional quarterly rounds of sampling and flow gauging activities for the Seeps,
Old Outfall 002, Outfall 002, Willis Creek, Georgia Branch Creek, and the Cape Fear
River upstream and downstream of the Site.
The contents of this report support the PFAS mass loading evaluation prepared pursuant
to Paragraph 12(a) in the executed Consent Order. The results of the Seeps and Creeks
Investigation provided data to inform the Mass Loading Model which in turn informs the
Reductions Plan.

Seeps and Creeks Investigation Report 24 August 26, 2019

5. REFERENCES
Geosyntec, 2018. Assessment of the Chemical and Spatial Distribution of PFAS in the
Cape Fear River. Chemours Fayetteville Works. 17 September 2018.
Geosyntec, 2019a. Site Associated PFAS Fate and Transport Study, Chemours
Fayetteville Works. June, 2019.
Geosyntec, 2019b. Cape Fear River Mass Loading Model Assessment and Paragraph 11.1
Characterization of PFAS at Intakes. August, 2019.
Geosyntec, 2019c. Creeks, Old Outfall 002 and Seeps Assessment Workplan. February
12, 2019.
Geosyntec, 2019d. Additional Creeks, Old Outfall 002 and Seeps Investigation Plan. May
13, 2019.
Geosyntec, 2019e. Willis Creek and Seep D Assessment Plan. June 17, 2019
Geosyntec, 2019f. Post Hurricane Florence PFAS Characterization. Chemours
Fayetteville Works. April 2019.
Moore, R.D., 2004. Introduction to salt dilution gauging for streamflow measurement:
Part 1. Streamline Watershed Management Bulletin, 7(4), pp.20-23.
Parsons 2018. Long Term Monitoring Plan. Chemours Fayetteville Works. RCRA
PERMIT NO. NCD047368642-R2-M3.
Wang, Z. et al., 2017. A never-ending story of per- and polyfluoroalkyl substances
(PFASs)? Environmental Science and Technology, 51(5), pp 2508-2518.

TABLES

TABLE 1LOCATION SUMMARYChemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC P.C.February May June February May June February May JuneOLDOF-1 Old Outfall 002 Location 1 Y -- -- Y -- -- -- -- --OLDOF-2 Old Outfall 002 Location 2YYYYYY------OLDOF-2J Old Outfall 002 Location 2J Y -- -- -- -- -- Y -- --OLDOF-2L Old Outfall 002 Location 2L Y -- -- -- -- -- Y -- --OLDOF-3 Old Outfall 002 Location 3 Y -- -- Y -- -- -- -- --OLDOF-4 Old Outfall 002 Location 4 Y -- -- -- -- -- -- -- --OLDOF-5 Old Outfall 002 Location 5 Y -- -- Y -- -- -- -- --OLDOF-5K Old Outfall 002 Location 5K Y -- -- -- -- -- Y -- --OLDOF-TR1-1 (1)Old Outfall 002 Tributary 1 Location 1 Y----Y----------OLDOF-TR1-1-1 (1)Old Outfall 002 Tributary 1 Location 1 Y----------------SEEP-A-1Seep A Location 1YYYYYY------SEEP-A-10 Seep A Location 10YY--------------SEEP-A-11 Seep A Location 11Y----------------SEEP-A-12 Seep A Location 12Y----------------SEEP-A-2Seep A Location 2Y----------------SEEP-A-3Seep A Location 3YYYYYY------SEEP-A-4Seep A Location 4YYYYYY------SEEP-A-5Seep A Location 5YY----Y--------SEEP-A-5-B-1 Seep A5 Location B1--Y--------------SEEP-A-5-D1-2 Seep A5 Location D1-2--Y--------------SEEP-A-6Seep A Location 6Y----------------SEEP-A-7Seep A Location 7Y----------------SEEP-A-8Seep A Location 8Y----------------SEEP-A-9Seep A Location 9Y----------------SEEP-A-TR1 (2)Seep A Tributary 1--Y--------------SEEP-A-TR1-1 (2)Seep A Tributary 1----Y--Y--------SEEP-A-TR2-1 Seep A Tributary 2-1--Y--------------SEEP-A-TR3-1 Seep A Tributary 3-1--Y--------------SEEP-A-TR4-1 Seep A Tributary 4-1--Y--------------SEEP-B-1Seep B Location 1YYYY--Y------SEEP-B-2Seep B Location 2YYYYYY------SEEP-B-3Seep B Location 3Y----Y----------SEEP-B-3-A (3)Seep B Location 3A--Y--Y----------SEEP-B-3-A1 (3)Seep B Location 3AY----------------SEEP-B-3-E4 Seep B Location 3E4Y----------------SEEP-B-4Seep B Location 4Y----------------SEEP-B-4-A3 Seep B Location 4A3Y----------------SEEP-B-TR1 Seep B Tributary 1--YY------------SEEP-B-TR2 Seep B Tributary 2--YY----Y------Temperature AssessmentLocation DescriptionFlow MeasurementSample CollectionLocation IDPage 1 of 2August 2019
TABLE 1LOCATION SUMMARYChemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC P.C.February May June February May June February May JuneTemperature AssessmentLocation DescriptionFlow MeasurementSample CollectionLocation IDSEEP-C-1Seep C Location 1YYYYYY------SEEP-C-1-E2 Seep C Location 1E2Y----------------SEEP-D-1Seep D Location 1--YY--YY------WC-1Willis Creek Location 1YYYYYY------WC-1-TR1 Willis Creek Location 1 Tributary 1--Y--------------WC-1-TR2 Willis Creek Location 1 Tributary 2--Y------Y------WC-2Willis Creek Location 2Y----------------WC-3Willis Creek Location 3Y----------------WC-3-TR2 Willis Creek Location 3 Tributary 2--Y------Y------WC-3-TR3 Willis Creek Location 3 Tributary 3--Y------Y------WC-3-TR5 Willis Creek Location 3 Tributary 5----------Y------WC-4Willis Creek Location 4Y----------------WC-4-TR1 Willis Creek Location 4 Tributary 1--Y------Y------WC-5Willis Creek Location 5Y----Y----------GBC-1Georgia Branch Creek Location 1--YY--YY------GBC-2Georgia Branch Creek Location 2--Y--------------GBC-3Georgia Branch Creek Location 3--Y--------------GBC-5Georgia Branch Creek Location 5--Y--------------GBC-6Georgia Branch Creek Location 6--Y--------------GBC-7Georgia Branch Creek Location 7--Y--------------GBC-TR1-1 Georgia Branch Creek Tributary 1--Y--------------GBC-TR2-1 Georgia Branch Creek Tributary 2--Y--------------CFR-MILE-56 Cape Fear River Mile 56--YY------------CFR-MILE-68 Cape Fear River Mile 68--YY------------CFR-MILE-76 Cape Fear River Mile 76YYY------------CFR-MILE-84 Cape Fear River Mile 84Y----------------CFR-BLADEN Cape Fear River at Bladen Bluffs--YY------------CFR-KINGS Cape Fear River at Kings Bluff--YY------------Notes:Y - Sampling, flow measurement, or temperature assessment was conducted(1) - Location IDs OLDOF-TR1-1 and OLDOF-TR1-1-1 represent the same location. Two location IDs are listed due to naming inconsistencies between the field and the laboratory. (2) - Location IDs SEEP-A-TR1 and SEEP-A-TR1-1 represent the same location. Two location IDs are listed due to naming inconsistencies between the field and the laboratory. (3) - Location IDs SEEP-B-3-A and SEEP-B-3-A1 represent the same location. Two location IDs are listed due to naming inconsistencies between the field and the laboratory. Page 2 of 2August 2019
TABLE 2
PFAS AND ASSOCIATED ANALYTICAL METHODS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
HFPO-DA* Hexafluoropropylene oxide dimer acid 13252-13-6 C6HF11O3
PEPA Perfluoroethoxypropyl carboxylic acid 267239-61-2 C5HF9O3
PFECA-G Perfluoro-4-isopropoxybutanoic acid 801212-59-9 C12H9F9O3S
PFMOAA Perfluoro-2-methoxyaceticacid 674-13-5 C3HF5O3
PFO2HxA Perfluoro(3,5-dioxahexanoic) acid 39492-88-1 C4HF7O4
PFO3OA Perfluoro(3,5,7-trioxaoctanoic) acid 39492-89-2 C5HF9O5
PFO4DA Perfluoro(3,5,7,9-tetraoxadecanoic) acid 39492-90-5 C6HF11O6
PMPA Perfluoromethoxypropyl carboxylic acid 13140-29-9 C4HF7O3
Hydro-EVE Acid Perfluoroethoxsypropanoic acid 773804-62-9 C8H2F14O4
EVE Acid Perfluoroethoxypropionic acid 69087-46-3 C8HF13O4
PFECA B Perfluoro-3,6-dioxaheptanoic acid 151772-58-6 C5HF9O4
R-EVE R-EVE N/A C8H2F12O5
PFO5DA Perfluoro-3,5,7,9,11-pentaoxadodecanoic acid 39492-91-6 C7HF13O7
Byproduct 4 Byproduct 4 N/A C7H2F12O6S
Byproduct 5 Byproduct 5 N/A C7H3F11O7S
Byproduct 6 Byproduct 6 N/A C6H2F12O4S
NVHOS Perfluoroethoxysulfonic acid 1132933-86-8 C4H2F8O4S
PES Perfluoroethoxyethanesulfonic acid 113507-82-7 C4HF9O4S
PFESA-BP1 Byproduct 1 29311-67-9 C7HF13O5S
PFESA-BP2 Byproduct 2 749836-20-2 C7H2F14O5S
PFBA Perfluorobutanoic acid 375-22-4 C4HF7O2
PFDA Perfluorodecanoic acid 335-76-2 C10HF19O2
PFDoA Perfluorododecanoic acid 307-55-1 C12HF23O2
PFHpA Perfluoroheptanoic acid 375-85-9 C7HF13O2
PFNA Perfluorononanoic acid 375-95-1 C9HF17O2
PFOA Perfluorooctanoic acid 335-67-1 C8HF15O
PFHxA Perfluorohexanoic acid 307-24-4 C6HF11O2
PFPeA Perfluoropentanoic acid 2706-90-3 C5HF9O2
PFTeA Perfluorotetradecanoic acid 376-06-7 C14HF27O2
PFTriA Perfluorotridecanoic acid 72629-94-8 C13HF25O2
PFUnA Perfluoroundecanoic acid 2058-94-8 C11HF21O2
PFBS Perfluorobutanesulfonic acid 375-73-5 C4HF9SO
PFDS Perfluorodecanesulfonic acid 335-77-3 C10HF21O3S
PFHpS Perfluoroheptanesulfonic acid 375-92-8 C7HF15O3S
PFHxS Perfluorohexanesulfonic acid 355-46-4 C6HF13SO3
PFNS Perfluorononanesulfonic acid 68259-12-1 C9HF19O3S
PFOS Perfluorooctanesulfonic acid 1763-23-1 C8HF17SO3
PFPeS Perfluoropentanesulfonic acid 2706-91-4 C5HF11O3S
10:2 FTS 10:2-fluorotelomersulfonic acid 120226-60-0 C12H5F21O3
4:2 FTS 4:2 fluorotelomersulfonic acid 757124-72-4 C6H5F9O3S
6:2 FTS 6:2 fluorotelomersulfonic acid 27619-97-2 C8H5F13SO3
8:2 FTS 8:2 fluorotelomersulfonic acid 39108-34-4 C10H5F17O3S
NEtFOSAA NEtFOSAA 2991-50-6 C12H8F17NO4S
NEtPFOSA NEtPFOSA 4151-50-2 C10H6F17NO2S
NEtPFOSAE NEtPFOSAE 1691-99-2 C12H10F17NO3S
NMeFOSAA NMeFOSAA 2355-31-9 C11H6F17NO4S
NMePFOSA NMePFOSA 31506-32-8 C9H4F17NO2S
NMePFOSAE NMePFOSAE 24448-09-7 C11H8F17NO3S
PFDOS Perfluorododecanesulfonic acid 79780-39-5 C12HF25O3S
PFHxDA Perfluorohexadecanoic acid 67905-19-5 C16HF31O2
PFODA Perfluorooctadecanoic acid 16517-11-6 C18HF35O2
PFOSA Perfluorooctanesulfonamide 754-91-6 C8H2F17NO2S
Notes:
*Depending on the laboratory, HFPO-DA may also appear on the EPA Method 537 Mod analyte list
EPA - Environmental Protection Agency
PFAS - per- and polyfluoroalkyl substances
SOP - Standard Operating Procedure
CASN Chemical Formula
Table 3+ Lab SOP
EPA Method 537
Mod
Analytical Method Common Name Chemical Name
August 2019
TABLE 3
TOTAL DAILY PRECIPITATION -
FEBRUARY, MAY, AND JUNE 2019
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Total Precipitation
(inches)
1/29/2019 0.09
1/30/2019 --
1/31/2019 --
2/1/2019 --
2/2/2019 --
2/3/2019 --
2/4/2019 --
2/5/2019 --
2/6/2019 --
2/7/2019 --
2/8/2019 --
2/9/2019 --
2/10/2019 --
2/11/2019 0.25
2/12/2019 0.25
2/13/2019 0.02
2/14/2019 --
2/15/2019 --
2/16/2019 0.6
2/17/2019 0.04
2/18/2019 0.12
2/19/2019 0.11
2/20/2019 0.19
2/21/2019 0.16
2/22/2019 0.28
2/23/2019 0.46
2/24/2019 0.01
2/25/2019 --
2/26/2019 --
2/27/2019 --
2/28/2019 --
5/1/2019 --
5/2/2019 --
5/3/2019 --
5/4/2019 0.16
5/5/2019 0.39
5/6/2019 --
5/7/2019 --
5/8/2019 --
5/9/2019 --
5/10/2019 --
5/11/2019 --
5/12/2019 0.13
5/13/2019 --
5/14/2019 --
5/15/2019 --
5/16/2019 --
5/17/2019 --
Page 1 of 2 August 2019
TABLE 3
TOTAL DAILY PRECIPITATION -
FEBRUARY, MAY, AND JUNE 2019
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Total Precipitation
(inches)
5/18/2019 --
5/19/2019 --
5/20/2019 0.24
5/21/2019 --
5/22/2019 --
5/23/2019 --
5/24/2019 --
5/25/2019 --
5/26/2019 --
5/27/2019 --
5/28/2019 --
5/29/2019 --
5/30/2019 --
5/31/2019 0.1
6/1/2019 --
6/2/2019 --
6/3/2019 --
6/4/2019 --
6/5/2019 0.8
6/6/2019 --
6/7/2019 --
6/8/2019 --
6/9/2019 2.2
6/10/2019 0.8
6/11/2019 0.1
6/12/2019 0.4
6/13/2019 --
6/14/2019 --
6/15/2019 --
6/16/2019 --
6/17/2019 --
6/18/2019 --
6/19/2019 --
6/20/2019 0.1
6/21/2019 --
6/22/2019 0.2
6/23/2019 --
6/24/2019 --
6/25/2019 --
6/26/2019 --
6/27/2019 --
6/28/2019 --
6/29/2019 --
6/30/2019 --
Notes:
-- - below USGS measurement threshold
Precipitation data obtained from USGS rain gauge at
W.O. Huske Dam.
Seeps and Creeks field event
USGS - United States Geological Survey
Page 2 of 2 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID OLDOF-1 OLDOF-1 OLDOF-2 OLDOF-2
Field Sample ID FAY-SW-OLDOF-1-020119 FAY-SW-OLDOF-1-020119 FAY-SW-OLDOF-2-020119 FAY-SW-OLDOF-2-020119
Laboratory Sample ID 9978959 / 9978962 320-51031-7 9978966 / 9978963 320-51031-8
Date Sampled 2/1/2019 2/1/2019 2/1/2019 2/1/2019
QA/QC --------
Laboratory Eurofins Lancaster TestAmerica Sacramento Eurofins Lancaster TestAmerica Sacramento
Table 3+ Lab SOP (ng/L)
HFPO-DA --------
PEPA 1,900 J 1,900 J 1,900 J 2,000 J
PFECA-G <50 UJ <41 UJ <50 UJ <41 UJ
PFMOAA 83,000 J 93,000 J 83,000 J 92,000 J
PFO2HxA 21,000 J 17,000 J 22,000 J 18,000 J
PFO3OA 6,400 J 5,200 J 6,400 J 5,200 J
PFO4DA 1,700 J 1,700 J 1,800 J 1,600 J
PMPA 5,600 J 5,800 J 5,800 J 6,000 J
Hydro-EVE Acid --200 J --200 J
EVE Acid --<24 UJ --<24 UJ
PFECA B --<60 UJ --<60 UJ
R-EVE --190 J --190 J
PFO5DA 670 B 970 B 820 B 950 B
Byproduct 4 --450 J --420 J
Byproduct 5 --1,200 J --1,300 J
Byproduct 6 --<15 UJ --<15 UJ
NVHOS --750 J --800 J
PES --<46 UJ --<46 UJ
PFESA-BP1 260 J 190 J 180 J 140 J
PFESA-BP2 300 J 310 J 330 J 340 J
N-ethylperfluoro-1-octanesulfonamide --<37 UJ --<37 UJ
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol --<60 UJ --<60 UJ
N-methyl perfluoro-1-octanesulfonamide --<35 UJ --<35 UJ
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol --<110 UJ --<110 UJ
Total Table 3+ Compounds*130,000 140,000
EPA Method 537 Mod (ng/L)
HFPO-DA 4,800 J --5,900 --
Perfluorobutanoic Acid 77 ------
Perfluorodecanoic Acid <1.7 ------
Perfluorododecanoic Acid <1.7 ------
Perfluoroheptanoic Acid 25 ------
Perfluorononanoic Acid 7.4 ------
Perfluorooctanoic acid 28 ------
Perfluorohexanoic Acid 14 ------
Perfluoropentanoic Acid 170 ------
Perfluorotetradecanoic Acid <0.86 ------
Perfluorotridecanoic Acid <0.86 ------
Perfluoroundecanoic Acid <1.7 ------
Perfluorobutane Sulfonic Acid 1.4 J ------
Perfluorodecane Sulfonic Acid <1.7 ------
Perfluoroheptane sulfonic acid (PFHpS)<1.7 ------
Perfluorohexane Sulfonic Acid <1.7 ------
Perfluorononanesulfonic acid <1.7 ------
Perfluorooctanesulfonic acid 1.9 ------
Perfluoropentane sulfonic acid (PFPeS)<1.7 ------
10:2 Fluorotelomer sulfonate <2.6 ------
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)<2.6 ------
6:2 Fluorotelomer sulfonate <1.7 ------
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)<5.2 ------
N-ethyl perfluorooctane sulfonamidoacetic acid <2.6 ------
N-ethylperfluoro-1-octanesulfonamide <7.8 UJ ------
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol <2.6 ------
N-methyl perfluorooctane sulfonamidoacetic acid <2.6 ------
N-methyl perfluoro-1-octanesulfonamide <7.8 UJ ------
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol <2.6 ------
Perfluorododecane sulfonic acid (PFDoS)<0.86 ------
Perfluorohexadecanoic acid (PFHxDA)<0.86 ------
Perfluorooctadecanoic acid <1.7 ------
Perfluorooctane Sulfonamide <2.6 ------
ADONA <0.86 UJ ------
F-53B Major <0.86 UJ ------
F-53B Minor <1.7 UJ ------
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
February 2019
Page 1 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
OLDOF-2J OLDOF-2J OLDOF-2L OLDOF-2L
FAY-SW-OLDOF-2J-020219 FAY-SW-OLDOF-2J-020219 FAY-SW-OLDOF-2L-020219 FAY-SW-OLDOF-2L-020219
9979923 / 9979920 320-51031-3 9979927 / 9979924 320-51031-2
2/2/2019 2/2/2019 2/2/2019 2/2/2019
--------
Eurofins Lancaster TestAmerica Sacramento Eurofins Lancaster TestAmerica Sacramento
--------
1,400 J 1,300 J 2,100 J 2,100 J
<50 UJ <41 UJ <50 UJ <41 UJ
630 J 490 J 99,000 J 104,000 J
1,700 J 1,300 J 23,000 J 21,000 J
400 J 290 J 6,900 J 5,400 J
<50 UJ <79 UJ 2,100 J 1,800 J
3,700 J 3,700 J 6,200 J 6,200 J
--<28 UJ --220 J
--<24 UJ --<24 UJ
--<60 UJ --<60 UJ
--120 J --190 J
<100 UJ 34 J 810 J 870 J
--180 J --490 J
--<58 UJ --1,500 J
--<15 UJ --<15 UJ
--<54 UJ --890 J
--<46 UJ --<46 UJ
<50 UJ <27 UJ 240 J 250 J
<50 UJ 71 J 350 J 350 J
--<37 UJ --<37 UJ
--<60 UJ --<60 UJ
--<35 UJ --<35 UJ
--<110 UJ --<110 UJ
8,700 150,000
1,200 --6,400 --
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
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--------
--------
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--------
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February 2019
Page 2 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
OLDOF-3 OLDOF-3 OLDOF-4 OLDOF-4
FAY-SW-OLDOF-3-020219 FAY-SW-OLDOF-3-020219 FAY-SW-OLDOF-4-020219 FAY-SW-OLDOF-4-020219
9979931 / 9979928 320-51031-4 9979935 / 9979932 320-51031-5
2/2/2019 2/2/2019 2/2/2019 2/2/2019
--------
Eurofins Lancaster TestAmerica Sacramento Eurofins Lancaster TestAmerica Sacramento
--------
2,200 J 2,000 J 2,400 J 2,300 J
<50 UJ <41 UJ <50 UJ <41 UJ
110,000 J 109,000 J 140,000 J 140,000 J
25,000 J 23,000 J 31,000 J 25,000 J
7,400 J 5,500 J 9,000 J 7,100 J
2,200 J 1,800 J 2,800 J 2,100 J
6,600 J 6,600 J 7,300 J 7,000 J
--240 J --310 J
--<24 UJ --<24 UJ
--<60 UJ --<60 UJ
--220 J --240 J
850 J 790 J 1,100 J 1,100 J
--560 J --620 J
--1,800 J --1,900 J
--18 J --19 J
--1,100 J --1,200 J
--<46 UJ --<46 UJ
100 J 170 J 230 J 240 J
400 J 420 J 480 J 470 J
--<37 UJ --<37 UJ
--<60 UJ --<60 UJ
--<35 UJ --<35 UJ
--<110 UJ --<110 UJ
160,000 200,000
5,600 --6,900 --
--------
--------
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--------
--------
--------
--------
--------
--------
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February 2019
Page 3 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
OLDOF-5 OLDOF-5 OLDOF-5K OLDOF-5K
FAY-SW-OLDOF-5-020219 FAY-SW-OLDOF-5-020219 FAY-SW-OLDOF-5K-020219 FAY-SW-OLDOF-5K-020219
9979943 / 9979940 320-51024-1 9979947 / 9979944 320-51024-2
2/2/2019 2/2/2019 2/2/2019 2/2/2019
--------
Eurofins Lancaster TestAmerica Sacramento Eurofins Lancaster TestAmerica Sacramento
--------
2,700 J 2,700 J 1,900 J 1,700 J
<50 UJ <41 UJ <50 UJ <41 UJ
190,000 J 200,000 J 18,000 J 16,000 J
43,000 J 37,000 J 6,600 J 5,400 J
14,000 J 11,000 J 1,700 J 1,300 J
5,200 J 4,400 J 1,700 J 1,300 J
8,600 J 8,200 J 5,400 J 4,500 J
--550 J --200 J
--370 J --31 J
--<60 UJ --<60 UJ
--310 J --210 J
4,200 J 4,200 J 590 J 580 J
--800 J --350 J
--3,200 J --<58 UJ
--32 J --15 J
--1,700 J --210 J
--<46 UJ --<46 UJ
4,600 J 3,700 J <50 UJ <27 UJ
990 J 990 J 540 J 500 J
--<37 UJ --<37 UJ
--<60 UJ --<60 UJ
--<35 UJ --<35 UJ
--<110 UJ --<110 UJ
290,000 39,000
7,600 --6,400 --
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February 2019
Page 4 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
OLDOF-TR1-1 OLDOF-TR1-1-1 SEEP-A-1 SEEP-A-1
FAY-SW-OLDOF-TR1-1-020219 FAY-SW-OLDOF-TR1-1-1-020219 FAY-SW-SEEP-A-1-020719 FAY-SW-SEEP-A-1-020719
320-51031-1 9979919 / 9979916 9982593 / 9982596 320-51045-13
2/2/2019 2/2/2019 2/7/2019 2/7/2019
--------
TestAmerica Sacramento Eurofins Lancaster Eurofins Lancaster TestAmerica Sacramento
--------
1,300 J 1,200 7,100 J 9,900 J
<41 UJ <50 <50 UJ <41 UJ
340 J 550 62,000 J 84,000 J
1,600 J 1,800 35,000 J 41,000 J
270 J 280 12,000 J 14,000 J
160 J 170 6,800 J 8,100 J
3,800 J 3,300 19,000 J 25,000 J
<28 UJ ----1,700 J
<24 UJ ----960 J
<60 UJ ----<60 UJ
<70 UJ ----1,200 J
250 J <100 6,300 J 5,600 J
<160 UJ ----2,200 J
<58 UJ ----23,000 J
<15 UJ ----47 J
<54 UJ ----980 J
<46 UJ ----<46 UJ
<27 UJ <50 4,300 J 4,000 J
110 J 88 1,200 J 1,200 J
<37 UJ ----<37 UJ
<60 UJ ----<60 UJ
<35 UJ ----<35 UJ
<110 UJ ----<110 UJ
9,600 230,000
--1,800 10,000 J --
----260 --
----<1.7 --
----<1.7 --
----94 --
----20 --
----35 --
----39 --
----520 --
----<0.85 --
----<0.85 --
----<1.7 --
----1.4 --
----<1.7 --
----<1.7 --
----2.9 --
----<1.7 --
----6.3 --
----<1.7 --
----<2.5 --
----<2.5 --
----<1.7 --
----<5.1 --
----<2.5 --
----<7.6 UJ --
----<2.5 --
----<2.5 --
----<7.6 UJ --
----<2.5 --
----<0.85 --
----<0.85 --
----<1.7 --
----<2.5 --
----<0.85 UJ --
----<0.85 UJ --
----<1.7 UJ --
February 2019
Page 5 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
SEEP-A-10 SEEP-A-10 SEEP-A-11 SEEP-A-11
FAY-SW-SEEP-A-10-020719 FAY-SW-SEEP-A-10-020719 FAY-SW-SEEP-A-11-020719 FAY-SW-SEEP-A-11-020719
9982632 / 9982629 320-51045-22 9982636 / 9982633 320-51045-23
2/7/2019 2/7/2019 2/7/2019 2/7/2019
--------
Eurofins Lancaster TestAmerica Sacramento Eurofins Lancaster TestAmerica Sacramento
--------
19,000 J 22,000 J 18,000 J 22,000 J
<50 UJ <200 UJ <50 UJ <200 UJ
75,000 J 84,000 J 76,000 J 90,000 J
59,000 J 65,000 J 62,000 J 67,000 J
25,000 J 25,000 J 26,000 J 26,000 J
19,000 J 21,000 J 20,000 J 22,000 J
48,000 J 52,000 J 46,000 J 51,000 J
--9,800 J --10,000 J
--24,000 J --24,000 J
--<300 UJ --<300 UJ
--4,700 J --4,600 J
17,000 J 25,000 J 16,000 J 24,000 J
--6,700 J --6,900 J
--70,000 J --74,000 J
--240 J --240 J
--3,300 J --3,700 J
--<230 UJ --<230 UJ
49,000 J 50,000 J 51,000 J 54,000 J
6,100 J 6,900 J 6,100 J 7,100 J
--<190 UJ --<190 UJ
--<300 UJ --<300 UJ
--<170 UJ --<170 UJ
--<550 UJ --<550 UJ
530,000 540,000
61,000 J --55,000 J --
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February 2019
Page 6 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
SEEP-A-12 SEEP-A-12 SEEP-A-2 SEEP-A-2
FAY-SW-SEEP-A-12-020719 FAY-SW-SEEP-A-12-020719 FAY-SW-SEEP-A-2-020719 FAY-SW-SEEP-A-2-020719
9982640 / 9982637 320-51045-24 9982600 / 9982597 320-51045-14
2/7/2019 2/7/2019 2/7/2019 2/7/2019
--------
Eurofins Lancaster TestAmerica Sacramento Eurofins Lancaster TestAmerica Sacramento
--------
7,400 J 8,700 J 6,900 J 8,900 J
<50 UJ <41 UJ <50 UJ <41 UJ
15,000 J 16,000 J 68,000 J 82,000 J
30,000 J 30,000 J 36,000 J 40,000 J
4,800 J 5,200 J 14,000 J 14,000 J
4,200 J 4,600 J 7,200 J 7,600 J
20,000 J 22,000 J 19,000 J 23,000 J
--310 J --1,800 J
--39 J --830 J
--<60 UJ --<60 UJ
--890 J --1,200 J
2,500 J 4,100 J 4,600 J 5,900 J
--2,100 J --2,200 J
--490 J --23,000 J
--26 J --47 J
--570 J --1,000 J
--<46 UJ --<46 UJ
98 J 120 J 4,100 J 3,800 J
1,300 J 1,400 J 990 J 1,200 J
--<37 UJ --<37 UJ
--<60 UJ --<60 UJ
--<35 UJ --<35 UJ
--<110 UJ --<110 UJ
120,000 240,000
20,000 J --27,000 J --
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
February 2019
Page 7 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
SEEP-A-3 SEEP-A-3 SEEP-A-4 SEEP-A-4
FAY-SW-SEEP-A-3-020719 FAY-SW-SEEP-A-3-020719 FAY-SW-SEEP-A-4-020719 FAY-SW-SEEP-A-4-020719
9982601 / 9982604 320-51045-15 9982608 / 9982605 320-51045-16
2/7/2019 2/7/2019 2/7/2019 2/7/2019
--------
Eurofins Lancaster TestAmerica Sacramento Eurofins Lancaster TestAmerica Sacramento
--------
6,700 J 8,400 J 9,300 J 12,000 J
<50 UJ <41 UJ <50 UJ <41 UJ
69,000 J 79,000 J 42,000 J 49,000 J
36,000 J 38,000 J 27,000 J 28,000 J
14,000 J 13,000 J 8,100 J 8,100 J
7,300 J 7,700 J 4,100 J 4,300 J
18,000 J 22,000 J 23,000 J 28,000 J
--1,600 J --860 J
--930 J --240 J
--<60 UJ --<60 UJ
--1,200 J --770 J
4,800 J 5,500 J 3,600 J 4,300 J
--2,200 J --1,300 J
--23,000 J --6,500 J
--45 J --26 J
--910 J --640 J
--<46 UJ --<46 UJ
4,500 J 3,700 J 700 J 560 J
1,000 J 1,100 J 770 J 830 J
--<37 UJ --<37 UJ
--<60 UJ --<60 UJ
--<35 UJ --<35 UJ
--<110 UJ --<110 UJ
220,000 160,000
13,000 J --17,000 J --
250 ------
<1.8 ------
<1.8 ------
92 ------
19 ------
35 ------
39 ------
550 ------
<0.9 ------
<0.9 ------
<1.8 ------
1.6 J ------
<1.8 ------
<1.8 ------
3 ------
<1.8 ------
5.6 ------
<1.8 ------
<2.7 ------
<2.7 ------
<1.8 ------
<5.4 ------
<2.7 ------
<8.1 UJ ------
<2.7 UJ ------
<2.7 ------
<8.1 UJ ------
<2.7 UJ ------
<0.9 ------
<0.9 ------
<1.8 ------
3 ------
<0.9 UJ ------
<0.9 UJ ------
<1.8 UJ ------
February 2019
Page 8 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
SEEP-A-5 SEEP-A-5 SEEP-A-6 SEEP-A-6
FAY-SW-SEEP-A-5-020719 FAY-SW-SEEP-A-5-020719 FAY-SW-SEEP-A-6-020719 FAY-SW-SEEP-A-6-020719
9982612 / 9982609 320-51045-17 9982616 / 9982613 320-51045-18
2/7/2019 2/7/2019 2/7/2019 2/7/2019
--------
Eurofins Lancaster TestAmerica Sacramento Eurofins Lancaster TestAmerica Sacramento
--------
15,000 J 20,000 J 14,000 J 18,000 J
<50 UJ <41 UJ <50 UJ <41 UJ
25,000 J 30,000 J 15,000 J 17,000 J
23,000 J 28,000 J 18,000 J 20,000 J
8,000 J 8,500 J 6,000 J 6,000 J
5,600 J 6,300 J 5,000 J 5,700 J
31,000 J 42,000 J 29,000 J 38,000 J
--1,300 J --1,000 J
--520 J --670 J
--<60 UJ --<60 UJ
--1,200 J --870 J
3,800 J 4,500 J 3,800 J 4,700 J
--2,000 J --1,400 J
--9,900 J --6,900 J
--40 J --31 J
--610 J --380 J
--<46 UJ --<46 UJ
1,300 J 1,100 J 1,500 J 1,500 J
1,100 J 1,200 J 1,200 J 1,300 J
--<37 UJ --<37 UJ
--<60 UJ --<60 UJ
--<35 UJ --<35 UJ
--<110 UJ --<110 UJ
180,000 140,000
18,000 J --18,000 J --
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
February 2019
Page 9 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
SEEP-A-7 SEEP-A-7 SEEP-A-8 SEEP-A-8
FAY-SW-SEEP-A-7-020719 FAY-SW-SEEP-A-7-020719 FAY-SW-SEEP-A-8-020719 FAY-SW-SEEP-A-8-020719
9982620 / 9982617 320-51045-19 9982624 / 9982621 320-51045-20
2/7/2019 2/7/2019 2/7/2019 2/7/2019
--------
Eurofins Lancaster TestAmerica Sacramento Eurofins Lancaster TestAmerica Sacramento
--------
17,000 J 22,000 J 15,000 J 19,000 J
<50 UJ <41 UJ <50 UJ <41 UJ
41,000 J 43,000 J 17,000 J 17,000 J
31,000 J 35,000 J 18,000 J 20,000 J
9,800 J 11,000 J 5,800 J 6,300 J
6,200 J 8,000 J 5,300 J 6,700 J
39,000 J 46,000 J 34,000 J 38,000 J
--1,800 J --1,300 J
--560 J --540 J
--<60 UJ --<60 UJ
--1,500 J --800 J
4,200 J 5,700 J 4,200 J 6,200 J
--2,500 J --1,500 J
--13,000 J --6,000 J
--51 J --37 J
--880 J --380 J
--<46 UJ --<46 UJ
990 J 1,300 J 2,800 J 1,600 J
1,300 J 1,400 J 1,400 J 1,500 J
--<37 UJ --<37 UJ
--<60 UJ --<60 UJ
--<35 UJ --<35 UJ
--<110 UJ --<110 UJ
220,000 140,000
28,000 J --13,000 J --
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
February 2019
Page 10 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
SEEP-A-9 SEEP-A-9 SEEP-B-1 SEEP-B-1
FAY-SW-SEEP-A-9-020719 FAY-SW-SEEP-A-9-020719 FAY-SW-SEEP-B-1-020519 FAY-SW-SEEP-B-1-020519
9982628 / 9982625 320-51045-21 9980817 320-51045-1
2/7/2019 2/7/2019 2/5/2019 2/5/2019
--------
Eurofins Lancaster TestAmerica Sacramento Eurofins Lancaster TestAmerica Sacramento
--------
18,000 J 22,000 J 15,000 J 17,000 J
<50 UJ <41 UJ <50 UJ <41 UJ
73,000 J 75,000 J 150,000 J 148,000 J
58,000 J 63,000 J 43,000 J 43,000 J
24,000 J 24,000 J 11,000 J 9,200 J
19,000 J 21,000 J 2,000 J 1,800 J
47,000 J 50,000 J 38,000 J 42,000 J
--8,300 J --2,800 J
--22,000 J --6,100 J
--<60 UJ --<60 UJ
--5,100 J --3,200 J
15,000 J 17,000 J 460 J 530 J
--8,200 J --4,700 J
--84,000 J --38,000 J
--200 J --84 J
--3,000 J --3,300 J
--<46 UJ --<46 UJ
46,000 J 43,000 J 4,600 J 3,500 J
5,600 J 6,000 J 1,100 J 1,100 J
--<37 UJ --<37 UJ
--<60 UJ --<60 UJ
--<35 UJ --<35 UJ
--<110 UJ --<110 UJ
510,000 350,000
57,000 J --24,000 J --
----560 --
----<18 --
----<18 --
----170 --
----18 --
----31 --
----47 --
----1,600 --
----<9 --
----<9 --
----<18 --
----<9 --
----<18 --
----<18 --
----<18 --
----<18 --
----<18 --
----<18 --
----<27 --
----<27 --
----<18 --
----<54 --
----<27 --
----<81 --
----<27 --
----<27 --
----<81 --
----<27 --
----<9 --
----<9 --
----<18 --
----<27 --
----<9 --
----<9 --
----<18 --
February 2019
Page 11 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
SEEP-B-2 SEEP-B-2 SEEP-B-3 SEEP-B-3
FAY-SW-SEEP-B-2-020519 FAY-SW-SEEP-B-2-020519 FAY-SW-SEEP-B-3-020619 FAY-SW-SEEP-B-3-020619
9980824 / 9980821 320-51045-2 9981743 / 9981740 320-51045-3
2/5/2019 2/5/2019 2/6/2019 2/6/2019
--------
Eurofins Lancaster TestAmerica Sacramento Eurofins Lancaster TestAmerica Sacramento
--------
34,000 J 32,000 J 35,000 J 38,000 J
<50 UJ <41 UJ <50 UJ <41 UJ
9,200 J 8,000 J 5,000 J 5,100 J
19,000 J 16,000 J 17,000 J 16,000 J
4,500 J 3,400 J 3,800 J 3,300 J
2,800 J 2,400 J 2,700 J 2,500 J
66,000 J 61,000 J 66,000 J 72,000 J
--7,100 J --9,100 J
--24,000 J --34,000 J
-- <60 UJ -- <60 UJ
--9,600 J --13,000 J
1,300 J 1,300 J 1,700 J 1,500 J
--11,000 J --14,000 J
--77,000 J --99,000 J
--230 J --280 J
--6,300 J --7,800 J
-- <46 UJ -- <46 UJ
19,000 J 14,000 J 23,000 J 22,000 J
3,200 J 3,000 J 3,500 J 3,900 J
-- <37 UJ -- <37 UJ
-- <60 UJ -- <60 UJ
-- <35 UJ -- <35 UJ
-- <110 UJ -- <110 UJ
310,000 380,000
38,000 J --40,000 J --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
-- -- -- --
February 2019
Page 12 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
SEEP-B-3-A1 SEEP-B-3-A1 SEEP-B-3-E4 SEEP-B-3-E4
FAY-SW-SEEP-B-3-A1-020619 FAY-SW-SEEP-B-3-A1-020619 FAY-SW-SEEP-B-3-E4-020619 FAY-SW-SEEP-B-3-E4-020619
9981747 / 9981744 320-51045-7 9981751 / 9981748 320-51045-8
2/6/2019 2/6/2019 2/6/2019 2/6/2019
--------
Eurofins Lancaster TestAmerica Sacramento Eurofins Lancaster TestAmerica Sacramento
--------
36,000 J 42,000 J 4,800 J 6,500 J
<50 UJ <41 UJ <50 UJ <41 UJ
4,800 J 5,600 J 1,600 J 1,800 J
18,000 J 17,000 J 5,400 J 5,900 J
3,700 J 3,200 J 980 J 1,000 J
2,900 J 2,800 J 990 J 1,200 J
70,000 J 79,000 J 13,000 J 16,000 J
--11,000 J --120 J
--46,000 J --<24 UJ
--<60 UJ --<60 UJ
--13,000 J --640 J
1,900 J 1,900 J 390 J 610 J
--16,000 J --730 J
--119,000 J --150 J
--340 J --<15 UJ
--8,500 J --75 J
--<46 UJ --<46 UJ
31,000 J 30,000 J <50 UJ <27 UJ
4,100 J 4,700 J 250 J 300 J
--37 J --<37 UJ
--<60 UJ --<60 UJ
--<35 UJ --<35 UJ
--<110 UJ --<110 UJ
460,000 45,000
58,000 J --10,000 J --
--------
--------
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--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
February 2019
Page 13 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
SEEP-B-4 SEEP-B-4 SEEP-B-4-A3 SEEP-B-4-A3
FAY-SW-SEEP-B-4-020619 FAY-SW-SEEP-B-4-020619 FAY-SW-SEEP-B-4-A3-020619 FAY-SW-SEEP-B-4-A3-020619
9981755 / 9981752 320-51045-9 9981759 / 9981756 320-51045-10
2/6/2019 2/6/2019 2/6/2019 2/6/2019
--------
Eurofins Lancaster TestAmerica Sacramento Eurofins Lancaster TestAmerica Sacramento
--------
60,000 J 61,000 J 33,000 J 36,000 J
<50 UJ <41 UJ <50 UJ <41 UJ
6,700 J 6,800 J 4,900 J 5,200 J
24,000 J 22,000 J 18,000 J 17,000 J
5,000 J 4,100 J 4,900 J 4,000 J
3,800 J 3,400 J 3,700 J 3,200 J
120,000 J 111,000 J 66,000 J 71,000 J
--16,000 J --9,100 J
--75,000 J --64,000 J
--<60 UJ --<60 UJ
--21,000 J --16,000 J
2,600 J 2,500 J 2,800 J 2,600 J
--24,000 J --18,000 J
--171,000 J --96,000 J
--500 J --290 J
--13,000 J --6,300 J
--<46 UJ --<46 UJ
69,000 J 51,000 J 42,000 J 40,000 J
6,200 J 6,800 J 4,000 J 4,400 J
--<37 UJ --<37 UJ
--<60 UJ --<60 UJ
--<35 UJ --<35 UJ
--<110 UJ --<110 UJ
670,000 430,000
82,000 J --32,000 J --
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
--------
February 2019
Page 14 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
SEEP-C-1 SEEP-C-1 SEEP-C-1-E2 SEEP-C-1-E2
FAY-SW-SEEP-C-1-020519 FAY-SW-SEEP-C-1-020519 FAY-SW-SEEP-C-1-E2-020519 FAY-SW-SEEP-C-1-E2-020519
9980825 / 9980829 320-51045-4 9980836 / 9980833 320-51045-5
2/5/2019 2/5/2019 2/5/2019 2/5/2019
--------
Eurofins Lancaster TestAmerica Sacramento Eurofins Lancaster TestAmerica Sacramento
--------
4,700 J 5,100 J 4,600 J 4,400 J
<50 UJ <82 UJ <50 UJ <41 UJ
200,000 J 196,000 J 180,000 J 164,000 J
62,000 J 64,000 J 46,000 J 40,000 J
21,000 J 20,000 J 13,000 J 9,600 J
4,500 J 4,600 J 2,600 J 2,200 J
16,000 J 16,000 J 14,000 J 12,000 J
--2,300 J --580 J
--<49 UJ --<24 UJ
-- <120 UJ -- <60 UJ
--1,900 J --990 J
<100 UJ 89 J <100 UJ 92 J
--1,600 J --1,200 J
--3,000 J --1,500 J
-- <31 UJ --17 J
--2,000 J --1,600 J
-- <92 UJ -- <46 UJ
<50 UJ <53 UJ <50 UJ <27 UJ
590 J 590 J 260 J 250 J
--<75 UJ --<37 UJ
--<120 UJ --<60 UJ
--<69 UJ --<35 UJ
--<220 UJ --<110 UJ
340,000 260,000
27,000 J --17,000 J --
380 ------
<18 ------
<18 ------
220 ------
<17 ------
20 ------
81 ------
1,700 ------
<9.1 ------
<9.1 ------
<18 ------
<9.1 ------
<18 ------
<18 ------
<18 ------
<18 ------
<18 ------
<18 ------
<27 ------
<27 ------
<18 ------
<54 ------
<27 ------
<82 ------
<27 ------
<27 ------
<82 ------
<27 ------
<9.1 ------
<8.7 ------
<18 ------
<27 ------
<9.1 ------
<9.1 ------
<18 ------
February 2019
Page 15 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
WC-1 WC-1 WC-2 WC-3
FAY-SW-WC-1-020719 FAY-SW-WC-1-020719 FAY-SW-WC-2-020719 FAY-SW-WC-3-020719
9982641 320-51045-25 9982648 / 9982645 9982649 / 9982652
2/7/2019 2/7/2019 2/7/2019 2/7/2019
--------
Eurofins Lancaster TestAmerica Sacramento Eurofins Lancaster Eurofins Lancaster
--------
130 J 190 J 64 <50
<50 UJ <41 UJ <50 <50
490 J <210 UJ 56 59
310 J 330 J 140 110
52 J 58 J <50 <50
<50 UJ <79 UJ <50 <50
440 J 1,200 J 290 270
--<28 UJ ----
--<24 UJ ----
--<60 UJ ----
--<70 UJ ----
<100 UJ 34 J <100 <100
--<160 UJ ----
--91 J ----
--<15 UJ ----
--<54 UJ ----
--<46 UJ ----
<50 UJ <27 UJ <50 <50
<50 UJ <30 UJ <50 <50
--<37 UJ ----
--<60 UJ ----
--<35 UJ ----
--<110 UJ ----
2,200 680 560
290 J --130 J 120 J
5.4 ----<5.1
<1.7 ----<1.7
<1.7 ----<1.7
1.8 ----1.5
<1.7 ----<1.7
4.7 ----2.5
2.5 ----2.2
6.7 ----<5.1
<0.85 ----<0.86
<0.85 ----<0.86
<1.7 ----<1.7
3.1 ----3.1
<1.7 ----<1.7
<1.7 ----<1.7
<1.7 ----<1.7
<1.7 ----<1.7
2.3 ----2.1
<1.7 ----<1.7
<2.6 ----<2.6
<2.6 ----<2.6
<1.7 ----<1.7
<5.1 ----<5.1
<2.6 ----<2.6
<7.7 UJ ----<7.7 UJ
<2.6 UJ ----<2.6 UJ
<2.6 ----<2.6
<7.7 UJ ----<7.7 UJ
<2.6 UJ ----<2.6 UJ
<0.85 ----<0.86
<0.85 ----<0.86
<1.7 ----<1.7
<2.6 ----<2.6
<0.85 UJ ----<0.86 UJ
<0.85 UJ ----<0.86 UJ
<1.7 UJ ----<1.7 UJ
February 2019
Page 16 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
WC-4 WC-5 CFR-MILE-76 CFR-MILE-76
FAY-SW-WC-4-020719 FAY-SW-WC-5-020719 FAY-SW-CFR-RM-76-020219 FAY-SW-CFR-RM-76-020419
9982656 / 9982653 9982660 / 9982657 9979948 / 9979951 320-51024-3
2/7/2019 2/7/2019 2/4/2019 2/4/2019
--------
Eurofins Lancaster Eurofins Lancaster Eurofins Lancaster TestAmerica Sacramento
--------
<50 74 <50 <20 UJ
<50 <50 <50 <2 UJ
<50 <50 <50 <5 UJ
82 74 <50 2 J
<50 <50 <50 <2 UJ
<50 <50 <50 <2 UJ
210 190 <50 11 J
------<2 UJ
------<2 UJ
------<2 UJ
------<2 UJ
<100 <100 <100 <2 UJ
------<2 UJ
------<2 UJ
------<2 UJ
------2.2 J
------<2 UJ
<50 <50 <50 <2 UJ
<50 <50 <50 <2 UJ
------<2 UJ
------<2 UJ
------<2 UJ
------<2 UJ
340 370 18
51 J 33 J 2.9 J --
----<5.2 --
----<1.7 --
----<1.7 --
----3.7 --
----<1.7 --
----6.1 --
----5.7 --
----<5.2 --
----<0.87 --
----<0.87 --
----<1.7 --
----2 J --
----<1.7 --
----<1.7 --
----3.5 --
----<1.7 --
----7.8 --
----<1.7 --
----<2.6 --
----<2.6 --
----<1.7 --
----<5.2 --
----<2.6 --
----<7.9 UJ --
----<2.6 --
----<2.6 --
----<7.9 UJ --
----<2.6 --
----<0.87 --
----<0.87 --
----<1.7 --
----<2.6 --
----<0.87 UJ --
----<0.87 UJ --
----<1.7 UJ --
February 2019
Page 17 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
CFR-MILE-84 CFR-MILE-84 EQBLK EQBLK FBLK
FAY-SW-CFR-RM-84-020219 FAY-SW-CFR-RM-84-020419 EB-020419 EB-020419 FB-020119
9979952 320-51024-4 9979956 320-51024-5 9978967
2/4/2019 2/4/2019 2/4/2019 2/4/2019 2/1/2019
----Field Blank Field Blank Field Blank
Eurofins Lancaster TestAmerica Sacramento Eurofins Lancaster TestAmerica Sacramento Eurofins Lancaster
----------
50 <20 UJ <50 UJ <20 UJ <50 UJ
<50 <2 UJ <50 UJ <2 UJ <50 UJ
56 55 J <50 UJ <5 UJ <50 UJ
<50 17 J <50 UJ <2 UJ <50 UJ
<50 3.6 J <50 UJ <2 UJ <50 UJ
<50 <2 UJ <50 UJ <2 UJ <50 UJ
<50 31 J <50 UJ <10 UJ <50 UJ
--<2 UJ --<2 UJ --
--<2 UJ --<2 UJ --
--<2 UJ --<2 UJ --
--<2 UJ --<2 UJ --
<100 <2 UJ <100 UJ <2 UJ <100 UJ
--8.3 J --<2 UJ --
--14 J --<2 UJ --
--<2 UJ --<2 UJ --
--2.9 J --<2 UJ --
--<2 UJ --<2 UJ --
<50 <2 UJ <50 UJ <2 UJ <50 UJ
<50 <2 UJ <50 UJ <2 UJ <50 UJ
--<2 UJ --<2 UJ --
--<2 UJ --<2 UJ --
--<2 UJ --<2 UJ --
--<2 UJ --<2 UJ --
140 ND
13 --<1.8 --<1.8
<5.3 --<5.4 --<5.4
<1.8 --<1.8 --<1.8
<1.8 --<1.8 --<1.8
3.5 --<0.91 --<0.9
<1.8 --<1.8 --<1.8
5.7 --<0.91 --<0.9
5.6 --<1.8 --<1.8
5.8 --<5.4 --<5.4
<0.89 --<0.91 --<0.9
<0.89 --<0.91 --<0.9
<1.8 --<1.8 --<1.8
2.2 J --<0.91 --<0.9
<1.8 --<1.8 --<1.8
<1.8 --<1.8 --<1.8
3.3 --<1.8 --<1.8
<1.8 --<1.8 --<1.8
8.4 --<1.8 --<1.8
<1.8 --<1.8 --<1.8
<2.7 --<2.7 --<2.7
<2.7 --<2.7 --<2.7
<1.8 --<1.8 --<1.8
<5.3 --<5.4 --<5.4
<2.7 --<2.7 --<2.7
<8 UJ --<8.2 --<8.1
<2.7 --<2.7 --<2.7
<2.7 --<2.7 --<2.7
<8 UJ --<8.2 --<8.1
<2.7 --<2.7 --<2.7
<0.89 --<0.91 --<0.9
<0.89 --<0.91 --<0.9
<1.8 --<1.8 --<1.8
<2.7 --<2.7 --<2.7
<0.89 --<0.91 --<0.9
<0.89 --<0.91 --<0.9
<1.8 --<1.8 --<1.8
February 2019
Page 18 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
FBLK FBLK FBLK FBLK FBLK
FB-020119 FB-020219 FB-020219 FB-S-020519 FB-020519
320-51031-9 9979939 / 9979936 320-51031-6 9980837 320-51045-11
2/1/2019 2/2/2019 2/2/2019 2/5/2019 2/5/2019
Field Blank Field Blank Field Blank Field Blank Field Blank
TestAmerica Sacramento Eurofins Lancaster TestAmerica Sacramento Eurofins Lancaster TestAmerica Sacramento
----------
<47 UJ <50 UJ <47 UJ <50 <47 UJ
<41 UJ <50 UJ <41 UJ <50 <41 UJ
<210 UJ <50 UJ <210 UJ <50 <210 UJ
<81 UJ <50 UJ <81 UJ <50 <81 UJ
<58 UJ <50 UJ <58 UJ <50 <58 UJ
<79 UJ <50 UJ <79 UJ <50 <79 UJ
<570 UJ <50 UJ <570 UJ <50 <570 UJ
<28 UJ --<28 UJ --<28 UJ
<24 UJ --<24 UJ --<24 UJ
<60 UJ --<60 UJ --<60 UJ
<70 UJ --<70 UJ --<70 UJ
370 J <100 UJ <34 UJ <100 <34 UJ
<160 UJ --<160 UJ --<160 UJ
<58 UJ --<58 UJ --58 J
<15 UJ --<15 UJ --<15 UJ
<54 UJ --<54 UJ --<54 UJ
<46 UJ --<46 UJ --<46 UJ
<27 UJ <50 UJ <27 UJ <50 <27 UJ
<30 UJ <50 UJ <30 UJ <50 <30 UJ
<37 UJ --<37 UJ --<37 UJ
<60 UJ --<60 UJ --<60 UJ
<35 UJ --<35 UJ --<35 UJ
<110 UJ --<110 UJ --<110 UJ
370 ND 58
--<1.8 --<1.8 UJ --
------<5.3 --
------<1.8 --
------<1.8 --
------<0.88 --
------<1.8 --
------<0.88 --
------<1.8 --
------<5.3 --
------<0.88 --
------<0.88 --
------<1.8 --
------<0.88 --
------<1.8 --
------<1.8 --
------<1.8 --
------<1.8 --
------<1.8 --
------<1.8 --
------<2.6 --
------<2.6 --
------<1.8 --
------<5.3 --
------<2.6 --
------<7.9 --
------<2.6 --
------<2.6 --
------<7.9 --
------<2.6 --
------<0.88 --
------<0.88 --
------<1.8 --
------<2.6 --
------<0.88 --
------<0.88 --
------<1.8 --
February 2019
Page 19 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
FBLK FBLK FBLK OLDOF-2 SEEP-A-1
FB-020619 FB-020619 FB-020719 FAY-SW-OLDOF-2-052419 FAY-SW-SEEPA-1-052019
9981763 / 9981760 320-51045-12 9982661 / 9982664 280-124472-2 280-124212-1
2/6/2019 2/6/2019 2/7/2019 5/24/2019 5/20/2019
Field Blank Field Blank Field Blank ----
Eurofins Lancaster TestAmerica Sacramento Eurofins Lancaster TestAmerica Sacramento TestAmerica Sacramento
----------
<50 UJ <47 UJ <50 1,900 11,000
<50 UJ <41 UJ <50 <41 <41
<50 UJ <210 UJ <50 71,000 103,000 J
<50 UJ <81 UJ <50 18,000 47,000
<50 UJ <58 UJ <50 4,800 18,000
<50 UJ <79 UJ <50 1,600 11,000
<50 UJ <570 UJ <50 5,600 24,000 J
--<28 UJ --200 2,500
--<24 UJ --<24 1,600
--<60 UJ --<60 <60
--<70 UJ --170 J 1,600
<100 UJ <34 UJ <100 620 7,100
--<160 UJ --410 3,000
--<58 UJ --790 31,000
--<15 UJ --<15 67
--<54 UJ --830 1,400
--<46 UJ --<46 <46
<50 UJ <27 UJ <50 <27 7,400
<50 UJ <30 UJ <50 310 1,800
--<37 UJ --<37 <37 UJ
--<60 UJ --<60 <60
--<35 UJ --<35 <35 UJ
--<110 UJ --<110 <110
ND 2 110,000 300,000
<1.8 UJ --2.2 J 6,700 J 24,000 J
----<5.4 86 360
----<1.8 <2 <2
----<1.8 <2 <2
----<0.9 25 120
----<1.8 7.5 28
----<0.9 32 39
----<1.8 17 50
----<5.4 150 690
----<0.9 <2 <2
----<0.9 <2 <2
----<1.8 <2 <2
----<0.9 <2 <2
----<1.8 <2 <2
----<1.8 <2 <2
----<1.8 <2 3.3
----<1.8 <2 <2
----<1.8 2 5.7
----<1.8 <2 <2
----<2.7 <2 <2
----<2.7 UJ <20 <20
----<1.8 <20 <20
----<5.4 <20 <20
----<2.7 <20 <20
----<8.1 ----
----<2.7 ----
----<2.7 <20 <20
----<8.1 ----
----<2.7 ----
----<0.9 <2 <2
----<0.9 <2 <2
----<1.8 <2 <2
----<2.7 <2 <2
----<0.9 ----
----<0.9 ----
----<1.8 ----
February 2019 May 2019
Page 20 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
SEEP-A-1 SEEP-A-10 SEEP-A-3 SEEP-A-4
FAY-SW-SEEPA-1-052019-D FAY-SW-SEEPA-10-052019 FAY-SW-SEEPA-3-052119 FAY-SW-SEEPA-4-052119
280-124212-2 280-124212-3 280-124212-14 280-124212-8
5/20/2019 5/20/2019 5/21/2019 5/21/2019
Field Duplicate ------
TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento
----41,000 --
11,000 29,000 12,000 11,000
<41 <41 <41 <41
103,000 26,000 118,000 J 45,000
48,000 36,000 57,000 26,000
18,000 14,000 J 22,000 7,400
11,000 13,000 11,000 3,300
25,000 J 61,000 J 31,000 25,000
2,500 6,800 2,800 710
1,700 12,000 2,100 76
<60 <60 <60 <60
1,600 5,100 J 1,800 J 770
6,200 12,000 7,900 1,800
3,000 7,900 J 3,900 J 1,300
32,000 71,000 J 37,000 J 5,500
74 150 79 25
1,400 2,000 1,800 680
<46 <46 <46 <46
7,400 27,000 9,000 260
1,700 3,600 1,900 650
<37 UJ <37 UJ <37 UJ <37 UJ
<60 <60 <60 <60
<35 <35 UJ <35 UJ <35 UJ
<110 <110 <110 <110
300,000 370,000 320,000 150,000
30,000 J 48,000 J --20,000 J
360 690 --330
<2 11 --<2
<2 <2 --<2
120 180 --71
26 75 --11
37 79 --31
52 55 --25
750 930 --450
<2 <2 --<2
<2 <2 --<2
<2 9.8 --<2
<2 <2 --<2
<2 <2 --<2
<2 <2 --<2
3.3 <2 --<2
<2 <2 --<2
5.5 9.5 --4.5
<2 <2 --<2
<2 <2 --<2
<20 <20 --<20
<20 <20 --<20
<20 <20 --<20
<20 <20 --<20
--------
--------
<20 <20 --<20
--------
--------
<2 <2 --<2
<2 <2 --<2
<2 <2 --<2
<2 <2 --<2
--------
--------
--------
May 2019
Page 21 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
SEEP-A-5 SEEP-A-5-B-1 SEEP-A-5-B-1 SEEP-A-5-D1-2
FAY-SW-SEEPA-5-052119 FAY-SW-SEEPA-5-B-1-052119 FAY-SW-SEEPA-5-B-1-052119-D FAY-SW-SEEPA-5-D1-2-052119
280-124212-9 280-124212-5 280-124212-6 280-124212-4
5/21/2019 5/21/2019 5/21/2019 5/21/2019
----Field Duplicate --
TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento
--------
20,000 <47 <47 6,800
<41 <41 <41 <41
25,000 <210 <210 6,800
24,000 <81 <81 16,000
7,000 J <58 <58 2,800
5,300 <79 <79 1,800
38,000 J <570 <570 17,000
1,200 <28 <28 100
740 <24 <24 <24
<60 <60 <60 <60
1,000 J <70 <70 260
4,200 <34 <34 360 B
1,600 J <160 <160 480
6,300 J <58 <58 <58
37 <15 <15 <15
550 <54 <54 120
<46 <46 <46 <46
1,800 <27 <27 <27
1,400 <30 <30 330
<37 UJ <37 UJ <37 UJ <37 UJ
<60 <60 <60 <60
<35 UJ <35 UJ <35 UJ <35 UJ
<110 <110 <110 <110
170,000 42 38 65,000
29,000 J 42 J 38 J 12,000 J
620 6.2 6.4 120
<2 <2 <2 <2
<2 <2 <2 <2
82 8.6 8.6 37
25 <2 <2 3
53 9 8.7 60
32 13 13 14
530 12 13 190
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
<2 3.2 3.3 <2
<2 <2 <2 <2
<2 <2 <2 <2
<2 4.9 5 <2
<2 <2 <2 <2
4.6 11 11 2.3
<2 <2 <2 <2
<2 <2 <2 <2
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
--------
--------
<20 <20 <20 <20
--------
--------
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 UJ <2 <2
<2 <2 <2 <2
--------
--------
--------
May 2019
Page 22 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
SEEP-A-TR1 SEEP-A-TR2-1 SEEP-A-TR3-1 SEEP-A-TR4-1
FAY-SW-SEEPA-TR1-052119 FAY-SW-SEEP-A-TR2-1-052119 FAY-SW-SEEP-A-TR3-1-052119 FAY-SW-SEEP-A-TR4-1-052119
280-124212-7 280-124222-3 280-124222-1 280-124222-4
5/21/2019 5/21/2019 5/21/2019 5/21/2019
--------
TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento
--------
6,600 6,800 8,800 5,700
<41 <41 <41 <41
24,000 24,000 30,000 5,000
20,000 21,000 27,000 14,000
5,100 5,500 5,500 2,200
1,900 1,900 1,500 1,300
16,000 19,000 25,000 16,000
220 240 130 91
<24 <24 <24 <24
<60 <60 <60 <60
510 570 J 600 J 260 J
230 B 220 170 320
860 960 J 1,100 J 540 J
980 1,200 J 980 J <58
<15 15 <15 <15
280 J 360 370 120
<46 <46 <46 <46
<27 <27 <27 <27
250 290 260 310
<37 UJ <37 UJ <37 UJ <37 UJ
<60 <60 <60 <60
<35 UJ <35 UJ <35 UJ <35 UJ
<110 <110 <110 <110
89,000 82,000 100,000 46,000
12,000 J ------
150 140 160 97
<2 <2 <2 <2
<2 <2 <2 <2
45 41 39 32
2.9 2 <2 2.5
26 25 24 56
17 ------
250 270 310 170
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
2.2 2 <2 <2
<2 <2 <2 <2
8.8 6.1 <2 3.1 I
<2 <2 <2 <2
<2 <2 <2 <2
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
--------
--------
<20 <20 <20 <20
--------
--------
<2 <2 <2 <2
<2 ------
<2 <2 <2 <2
<2 <2 <2 <2
--------
--------
--------
May 2019
Page 23 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
SEEP-B-1 SEEP-B-2 SEEP-B-3-A SEEP-B-TR1
FAY-SW-SEEP-B-1-052119 FAY-SW-SEEP-B-2 -052119 FAY-SW-SEEP-B-3A-052119 FAY-SW-SEEPB-TR1- 052119
280-124257-1 280-124257-2 280-124257-5 280-124257-3
5/21/2019 5/21/2019 5/21/2019 5/21/2019
--------
TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento
--75,000 150,000 17,000
13,000 46,000 99,000 13,000
<41 <41 <200 <41
150,000 11,000 J 6,600 38,000 J
43,000 17,000 22,000 19,000
9,600 4,100 4,900 4,700
1,300 2,500 3,800 1,500
34,000 81,000 166,000 30,000
1,700 8,300 19,000 110
2,900 22,000 89,000 <24
<60 <60 <300 <60
2,000 J 9,000 19,000 J 500 J
210 1,300 2,800 130
2,900 J 11,000 22,000 J 880 J
21,000 J 56,000 J 113,000 1,200 J
53 250 J 610 <15
2,700 6,600 15,000 430
<46 <46 <230 <46
2,000 15,000 58,000 J <27
660 3,300 7,700 170
<37 <37 <190 <37
<60 <60 <300 <60
<35 <35 <170 <35
<110 <110 <550 <110
310,000 290,000 650,000 110,000
22,000 J ------
470 ------
2.2 ------
<2 ------
140 ------
12 ------
17 ------
37 ------
1,200 ------
<2 ------
<2 ------
<2 ------
<2 ------
<2 ------
<2 ------
<2 ------
<2 ------
2.3 ------
<2 ------
<2 ------
<20 ------
<20 ------
<20 ------
<20 ------
--------
--------
<20 ------
--------
--------
<2 ------
<2 ------
<2 ------
<2 ------
--------
--------
--------
May 2019
Page 24 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
SEEP-B-TR2 SEEP-C-1 SEEP-D-1 SEEP-D-1
FAY-SW-SEEPB-TR2- 052119 FAY-SW-SEEP-C-1-052319 FAY-SW-SEEP-D-1-053019 FAY-SW-SEEP-D-1-053019-D
280-124257-4 280-124325-4 280-124599-1 280-124599-2
5/21/2019 5/23/2019 5/30/2019 5/30/2019
------Field Duplicate
TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento
42,000 ------
22,000 5,000 2,900 J 3,000 J
<41 <61 <41 UJ <41 UJ
82,000 193,000 91,000 J 91,000 J
28,000 66,000 29,000 J 29,000 J
5,400 19,000 7,900 J 8,100 J
1,400 4,900 2,300 J 2,500 J
44,000 14,000 9,200 J 9,000 J
4,600 2,500 1,300 J 1,300 J
2,500 <36 <24 UJ <24 UJ
<60 <90 <60 UJ <60 UJ
5,700 1,200 1,100 J 1,100 J
440 97 J 150 B 150 B
6,400 J 1,300 970 J 1,000 J
34,000 J 1,900 2,600 J 2,500 J
130 52 J 15 J <15 UJ
4,900 2,000 810 J 800 J
<46 <69 <46 UJ <46 UJ
2,700 <40 <27 UJ <27 UJ
1,700 720 320 J 340 J
<37 <56 <37 UJ <37 UJ
<60 <90 <60 UJ <60 UJ
<35 <52 <35 UJ <35 UJ
<110 <160 <110 UJ <110 UJ
250,000 350,000 170,000 160,000
--36,000 J 19,000 J 15,000 J
--390 210 210
--<2 <2 <2
--<2 <2 <2
--240 97 93
--<2 2.7 2.6
--18 12 11
--92 40 41
--1,800 760 730
--<2 <2 <2
--<2 <2 <2
--<2 <2 <2
--<2 <2 <2
--<2 <2 <2
--<2 <2 <2
--2.2 2 2
--<2 <2 <2
--2.2 <2 <2
--<2 <2 <2
--<2 <2 <2
--<20 <20 <20
--<20 <20 <20
--<20 <20 <20
--<20 <20 <20
--------
--------
--<20 <20 <20
--------
--------
--<2 <2 <2
--<2 <2 <2
--<2 <2 <2
--<2 <2 <2
--------
--------
--------
May 2019
Page 25 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
WC-1 WC-1-TR1 WC-1-TR2 WC-3-TR2
FAY-SW-WC-1-053019 FAY-SW-WC-1-TR1-052119 FAY-SW-WC-1-TR2-052219 FAY-SW-WC-3-TR2-052319
280-124599-3 280-124212-10 280-124323-2 280-124323-3
5/30/2019 5/21/2019 5/22/2019 5/23/2019
--------
TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento
----3,900 11,000
240 J <47 720 2,800
<41 UJ <41 <41 <41
1,400 J <210 1,300 2,100
730 J <81 2,000 6,500
120 J <58 380 1,000
<79 UJ <79 200 520
1,200 J <570 2,400 8,300
<28 UJ <28 <28 30
<24 UJ <24 <24 <24
<60 UJ <60 <60 <60
<70 UJ <70 <70 <70
45 B <34 <34 <34
<160 UJ <160 <160 <160
220 J <58 <58 UJ <58 UJ
<15 UJ <15 <15 <15
<54 UJ <54 <54 <54
<46 UJ <46 <46 <46
<27 UJ <27 <27 <27
<30 UJ <30 59 93
<37 UJ <37 UJ <37 <37
<60 UJ <60 <60 <60
<35 UJ <35 UJ <35 <35
<110 UJ <110 <110 <110
4,800 62 7,100 21,000
810 J 62 J ----
10 6 ----
<2 <2 ----
<2 <2 ----
2.6 8.1 ----
<2 <2 ----
8.8 7.4 ----
4.6 12 ----
12 12 ----
<2 <2 ----
<2 <2 ----
<2 <2 ----
3.6 3.3 ----
<2 <2 ----
<2 <2 ----
2.2 4.5 ----
<2 <2 ----
4.2 11 ----
<2 <2 ----
<2 <2 ----
<20 <20 ----
<20 <20 ----
<20 <20 ----
<20 <20 ----
--------
--------
<20 <20 ----
--------
--------
<2 <2 ----
<2 <2 ----
<2 <2 ----
<2 <2 ----
--------
--------
--------
May 2019
Page 26 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
WC-3-TR3 WC-4-TR1 GBC-1 GBC-2
FAY-SW-WC-3-TR3-052319 FAY-SW-WC-4-TR1-052219 FAY-SW-GBC-1-052919 FAY-SW-GBC-2-052919
280-124323-4 280-124323-5 280-124472-4 280-124472-5
5/23/2019 5/22/2019 5/29/2019 5/29/2019
--------
TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento
2,400 1,700 --640
510 370 300 J 280
<41 <41 <41 <41
350 520 <210 <210
1,300 1,100 420 J 370
260 210 <58 65
85 <79 <79 <79
1,700 1,300 1,300 J 1,200
<28 <28 <28 <28
<24 <24 <24 <24
<60 <60 <60 <60
<70 <70 <70 <70 UJ
<34 <34 <34 <34
<160 <160 <160 <160
<58 UJ <58 UJ <58 <58
<15 <15 <15 <15
<54 <54 <54 <54
<46 <46 <46 <46
<27 <27 <27 <27
40 <30 33 30
<37 <37 <37 <37
<60 <60 <60 <60
<35 <35 <35 <35
<110 <110 <110 <110
4,200 3,500 2,600 1,900
----500 J --
----11 --
----<2 --
----<2 --
----2.4 --
----<2 --
----3.8 --
----3.3 --
----10 --
----<2 --
----<2 --
----<2 --
----<2 --
----<2 --
----<2 --
----<2 --
----<2 --
----2.4 --
----<2 --
----<2 --
----<20 --
----<20 --
----<20 --
----<20 --
--------
--------
----<20 --
--------
--------
----<2 --
----<2 --
----<2 --
----<2 --
--------
--------
--------
May 2019
Page 27 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
GBC-3 GBC-5 GBC-5 GBC-6 GBC-7
FAY-SW-GBC-3-052919 FAY-SW-GBC-5-052919 FAY-SW-GBC-5-052919-D FAY-SW-GBC-6-052919 FAY-SW-GBC-7-052919
280-124472-6 280-124472-9 280-124472-10 280-124472-11 280-124472-12
5/29/2019 5/29/2019 5/29/2019 5/29/2019 5/29/2019
----Field Duplicate ----
TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento
680 1,300 1,200 1,400 1,200
310 520 490 J 550 410
<41 <41 <41 <41 <41
<210 210 <210 <210 <210
460 780 690 J 820 780
70 130 130 J 140 130
<79 <79 <79 <79 <79
1,400 1,600 J 1,800 J 1,900 1,600
<28 <28 <28 <28 <28
<24 <24 <24 <24 <24
<60 <60 <60 <60 <60
<70 <70 <70 <70 <70
<34 <34 34 <34 34
<160 <160 <160 <160 <160
<58 <58 <58 <58 <58
<15 <15 <15 <15 <15
<54 <54 <54 <54 <54
<46 <46 <46 <46 <46
<27 <27 <27 <27 <27
31 39 35 47 56
<37 <37 <37 <37 <37
<60 <60 <60 <60 <60
<35 <35 <35 <35 <35
<110 <110 <110 <110 <110
2,300 3,300 3,200 3,500 3,000
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
----------
May 2019
Page 28 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
GBC-TR1 GBC-TR2 CFR-MILE-56 CFR-MILE-68
FAY-SW-GBC-TR1-1-052919 FAY-SW-GBC-TR2-1-052919 FAY-SW-CFR-RM-56-052219 FAY-SW-CFR-RM-08-052219
280-124472-7 280-124472-8 280-124268-1 280-124268-2
5/29/2019 5/29/2019 5/22/2019 5/22/2019
--------
TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento
160 490 ----
110 230 <20 UJ <20 UJ
<41 <41 <2 UJ <2 UJ
<210 <210 <5 UJ <5 UJ
130 310 <2 UJ 2 J
<58 <58 <2 UJ <2 UJ
<79 <79 <2 UJ <2 UJ
900 1,100 <10 UJ 10 J
<28 <28 <2 UJ <2 UJ
<24 <24 <2 UJ <2 UJ
<60 <60 <2 UJ <2 UJ
<70 <70 UJ <2 UJ <2 UJ
<34 <34 <2 UJ <2 UJ
<160 <160 2 J 4.9 J
<58 <58 UJ 12 J 7.9 J
<15 <15 <2 UJ <2 UJ
<54 <54 2.8 J 7.6 J
<46 <46 <2 UJ <2 UJ
<27 <27 <2 UJ <2 UJ
<30 <30 <2 UJ <2 UJ
<37 <37 <2 UJ <2 UJ
<60 <60 <2 UJ <2 UJ
<35 <35 <2 UJ <2 UJ
<110 <110 <2 UJ <2 UJ
1,100 1,600 17 32
----<4 <4
----7.9 6.9
----<2 <2
----<2 <2
----13 9.5
----<2 <2
----8.3 7.2
----18 15
----17 13
----<2 <2
----<2 <2
----<2 <2
----3 3.3
----<2 <2
----<2 <2
----5 5.4
----<2 <2
----15 13
----<2 <2
----<2 <2
----<20 <20
----<20 <20
----<20 <20
----<20 <20
--------
--------
----<20 <20
--------
--------
----<2 <2
----<2 <2
----<2 <2
----<2 <2
--------
--------
--------
May 2019
Page 29 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
CFR-MILE-76 CFR-BLADEN CFR-KINGS CFR-KINGS
FAY-SW-CFR-RM-76-052219 FAY-SW-CFR-BLADEN-052219 FAY-SW-CFR-KINGS-052319 FAY-SW-CFR-KINGS-052319-D
280-124268-3 280-124268-4 280-124325-2 280-124325-3
5/22/2019 5/22/2019 5/23/2019 5/23/2019
------Field Duplicate
TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento
--------
<20 UJ <20 UJ <20 <20
<2 UJ <2 UJ <2 <2
<5 UJ 130 J 7.8 J 8.4 J
3.5 J 40 J 29 29
<2 UJ 9.9 J 7.5 7.6
<2 UJ 3.5 J 2.4 2.4
<10 UJ 31 J 29 21
<2 UJ <2 UJ <2 <2
<2 UJ <2 UJ <2 <2
<2 UJ <2 UJ <2 <2
<2 UJ 4 J 10 J <2
<2 UJ <2 UJ <2 <2
<2 UJ 9.6 J 20 J <2
5.2 J 31 J 7.6 J 8.3 J
<2 UJ <2 UJ <2 <2
4.1 J 6.1 J 6.2 J <2
<2 UJ <2 UJ <2 <2
<2 UJ <2 UJ <2 <2
<2 UJ <2 UJ <2 <2
<2 UJ <2 UJ <2 <2
<2 UJ <2 UJ <2 <2
<2 UJ <2 UJ <2 <2
<2 UJ <2 UJ <2 <2
13 270 140 93
<4 28 17 16
6.2 6.8 4.9 4.9
<2 <2 <2 <2
<2 <2 <2 <2
8.4 8.2 6.3 5.7
<2 <2 <2 <2
6.9 6.8 6.7 6.7
12 12 8.9 9
12 13 9.9 9.4
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
3.1 3.3 2.7 2.9
<2 <2 <2 <2
<2 <2 <2 <2
4.7 5 4.2 4.3
<2 <2 <2 <2
13 13 12 12
<2 <2 <2 <2
<2 <2 <2 <2
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
--------
--------
<20 <20 <20 <20
--------
--------
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 <2 UJ <2
<2 <2 <2 <2
--------
--------
--------
May 2019
Page 30 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
Outfall 002 Excess River Water EQBLK EQBLK
DSTW-OUTFALL 002-052019 DSTW-EXCESS RIVER WATER-052019 EB-052219 EB2-052319
280-124212-12 280-124212-11 280-124268-5 280-124325-1
5/20/2019 5/20/2019 5/22/2019 5/23/2019
----Equipment Blank Equipment Blank
TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento
<86 <86 ----
<47 <47 <47 <20
<41 <41 <41 <2
<210 <210 <210 <5
<81 <81 <81 <2
<58 <58 <58 <2
<79 <79 <79 <2
<570 <570 <570 <10
<28 <28 <28 <2
<24 <24 <24 <2
<60 <60 <60 <2
<70 <70 <70 <2
<34 <34 <34 <2
<160 <160 <160 <2
<58 <58 <58 <2
<15 <15 <15 <2
<54 <54 <54 <2
<46 <46 <46 <2
<27 <27 <27 <2
<30 <30 <30 <2
<37 UJ <37 UJ <37 <2
<60 <60 <60 <2
<35 UJ <35 UJ <35 <2
<110 <110 <110 <2
ND ND ND ND
----<4 <4
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----<20 <20
----<20 <20
----<20 <20
----<20 <20
--------
--------
----<20 <20
--------
--------
----<2 <2
----<2 <2
----<2 <2
----<2 <2
--------
--------
--------
May 2019
Page 31 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
FBLK FBLK FBLK FBLK FBLK
FB1-052019 FB2-052119 FB3-052219 FB4-052319 FB5-052419
280-124212-13 280-124222-2 280-124257-6 280-124323-1 280-124472-1
5/20/2019 5/21/2019 5/22/2019 5/23/2019 5/24/2019
Field Blank Field Blank Field Blank Field Blank Field Blank
TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento
<86 --------
<47 <47 <47 <47 <47
<41 <41 <41 <41 <41
<210 <210 <210 <210 <210
<81 <81 <81 <81 <81
<58 <58 <58 <58 <58
<79 <79 <79 <79 <79
<570 <570 <570 <570 <570
<28 <28 <28 <28 <28
<24 <24 <24 <24 <24
<60 <60 <60 <60 <60
<70 <70 <70 <70 <70 UJ
34 <34 <34 <34 <34
<160 <160 <160 <160 <160
<58 <58 <58 <58 UJ <58
<15 <15 <15 <15 <15
<54 <54 <54 <54 <54
<46 <46 <46 <46 <46
<27 27 <27 <27 <27
<30 <30 <30 <30 <30
<37 UJ <37 UJ <37 <37 <37
<60 <60 <60 <60 <60
<35 UJ <35 UJ <35 <35 <35
<110 <110 <110 <110 <110
34 27 ND ND ND
----<4 <4 <4
--<2 <2 <2 <2
--<2 <2 <2 <2
--<2 <2 <2 <2
--<2 <2 <2 <2
--<2 <2 <2 <2
--<2 <2 <2 <2
----<2 <2 <2
--<2 <2 <2 <2
--<2 <2 <2 <2
--<2 <2 <2 <2
--<2 <2 <2 <2
--<2 <2 <2 <2
--<2 <2 <2 <2
--<2 <2 <2 <2
--<2 <2 <2 <2
--<2 <2 <2 <2
--<2 <2 <2 <2
--<2 <2 <2 <2
--<2 <2 <2 <2
--<20 <20 <20 <20
--<20 <20 <20 <20
--<20 <20 <20 <20
--<20 <20 <20 <20
----------
----------
--<20 <20 <20 <20
----------
----------
--<2 <2 <2 <2
----<2 <2 <2
--<2 <2 <2 <2
--<2 <2 <2 <2
----------
----------
----------
May 2019
Page 32 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
FBLK FBLK OLDOF-2 SEEP-A-1 SEEP-A-3
FB6-052919 FB7-053019 FAY-SW-OLDOF-2-060719 FAY-SW-SEEP A-1-060719 FAY-SW-SEEP A-3-060719
280-124472-3 280-124599-4 280-124971-2 280-124971-6 280-124971-7
5/29/2019 5/30/2019 6/7/2019 6/7/2019 6/7/2019
Field Blank Field Blank ------
TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento
--------34,000 J
<47 <47 UJ 1,800 J 6,900 J 9,800 J
<41 <41 UJ <41 UJ <41 UJ <41 UJ
<210 <210 UJ 91,000 J 72,000 J 122,000 J
<81 <81 UJ 18,000 J 30,000 J 48,000 J
<58 <58 UJ 4,700 J 11,000 J 17,000 J
<79 <79 UJ 1,400 J 5,300 J 8,900 J
<570 <570 UJ 5,400 J 17,000 J 25,000 J
<28 <28 UJ 200 J 1,400 J 2,600 J
<24 <24 UJ 24 J 970 J 1,800 J
<60 <60 UJ <60 UJ <60 UJ <60 UJ
<70 UJ <70 UJ 200 J 1,100 J 1,700 J
<34 37 J 570 J 4,600 J 8,000 J
<160 <160 UJ 390 J 1,700 J 3,000 J
<58 UJ <58 UJ 1,100 J 18,000 J 33,000 J
<15 <15 UJ 15 J 50 J 88 J
<54 <54 UJ 900 J 1,000 J 1,700 J
<46 <46 UJ <46 UJ <46 UJ <46 UJ
<27 <27 UJ 300 J 5,300 J 11,000 J
<30 <30 UJ 350 J 1,300 J 2,200 J
<37 <37 UJ <37 UJ <37 UJ <37 UJ
<60 <60 UJ <60 UJ <60 UJ <60 UJ
<35 <35 UJ <35 UJ <35 UJ <35 UJ
<110 <110 UJ <110 UJ <110 UJ <110 UJ
ND 37 130,000 200,000 330,000
<4 <4 6,200 J 20,000 J --
<2 <2 90 240 --
<2 <2 <2 <2 --
<2 <2 <2 <2 --
<2 <2 26 79 --
<2 <2 7.1 15 --
<2 <2 34 36 --
<2 <2 16 37 --
<2 <2 160 490 --
<2 <2 <2 <2 --
<2 <2 <2 <2 --
<2 <2 <2 <2 --
<2 <2 <2 2.2 --
<2 <2 <2 <2 --
<2 <2 <2 <2 --
<2 <2 <2 4 --
<2 <2 <2 <2 --
<2 <2 2 9.7 --
<2 <2 <2 <2 --
<2 <2 <2 <2 --
<20 <20 <20 <20 --
<20 <20 <20 <20 --
<20 <20 <20 <20 --
<20 <20 <20 <20 --
----------
----------
<20 <20 <20 <20 --
----------
----------
<2 <2 <2 <2 --
<2 <2 <2 <2 --
<2 <2 <2 <2 --
<2 <2 <2 <2 --
----------
----------
----------
June 2019May 2019
Page 33 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
SEEP-A-4 SEEP-A-TR1-1 SEEP-B-1 SEEP-B-2
FAY-SW-SEEP A-4-060719 FAY-SW-SEEP A-TR1-1-060719 FAY-SW-SEEP B-1-060719 FAY-SW-SEEP B-2-060719
280-124971-9 280-124971-8 280-124971-16 280-124971-19
6/7/2019 6/7/2019 6/7/2019 6/7/2019
--------
TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento
19,000 J 5,000 J --85,000 J
11,000 J 1,900 J 15,000 J 50,000 J
<20 UJ <4.1 UJ <41 UJ 41 J
59,000 J 7,900 J 157,000 J 13,000 J
25,000 J 5,800 J 39,000 J 18,000 J
6,900 J 1,300 J 8,800 J 4,200 J
2,600 J 470 J 1,500 J 2,500 J
25,000 J 5,200 J 35,000 J 87,000 J
700 J 62 J 2,200 J 8,900 J
87 J <2.4 UJ 4,300 J 24,000 J
<30 UJ <6 UJ <60 UJ 60 J
950 J 170 J 3,200 J 11,000 J
2,000 J 110 J 270 J 1,200 J
1,400 J 290 J 3,900 J 12,000 J
6,200 J 300 J 34,000 J 74,000 J
29 J 5.2 J 78 J 380 J
760 J 110 J 3,200 J 7,700 J
<23 UJ <4.6 UJ <46 UJ 46 J
380 J 5.5 J 2,900 J 17,000 J
770 J 140 J 940 J 3,800 J
<19 UJ 3.7 J <37 UJ 37 J
<30 UJ <6 UJ <60 UJ 60 J
<17 UJ <3.5 UJ <35 UJ 35 J
<55 UJ <11 UJ <110 UJ 110 J
160,000 29,000 340,000 420,000
----27,000 J --
----600 --
----2.6 --
----<2 --
----170 --
----16 --
----24 --
----47 --
----1,500 --
----<2 --
----<2 --
----<2 --
----<2 --
----<2 --
----<2 --
----2.2 --
----<2 --
----2.2 --
----<2 --
----<2 --
----<20 --
----<20 --
----<20 --
----<20 --
--------
--------
----<20 --
--------
--------
----<2 --
----<2 --
----<2 --
----<2 --
--------
--------
--------
June 2019
Page 34 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
SEEP-B-TR1 SEEP-B-TR2 SEEP-C-1 SEEP-D-1
FAY-SW-SEEPB-TR1-060719 FAY-SW-SEEP B-TR2-060719 FAY-SW-SEEP C-1-060719 FAY-SW-SEEP D-1-060719
280-124971-17 280-124971-18 280-124971-1 280-124971-5
6/7/2019 6/7/2019 6/7/2019 6/7/2019
--------
TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento
19,000 J 40,000 J ----
16,000 J 19,000 J 4,000 J 2,400 J
<8.2 UJ <31 UJ <82 UJ <41 UJ
17,000 J 82,000 J 199,000 J 90,000 J
15,000 J 27,000 J 56,000 J 24,000 J
3,500 J 4,900 J 17,000 J 7,400 J
1,500 J 1,300 J 3,600 J 1,800 J
34,000 J 37,000 J 13,000 J 7,200 J
83 J 3,900 J 2,100 J 1,200 J
<4.9 UJ 2,100 J <49 UJ <24 UJ
<12 UJ <45 UJ <120 UJ <60 UJ
820 J 5,700 J 1,900 J 1,000 J
160 J 380 J <67 UJ 120 J
1,200 J 6,000 J 1,500 J 840 J
110 J 37,000 J 3,100 J 2,200 J
8.6 J 130 J 40 J 17 J
210 J 4,300 J 2,100 J 900 J
<9.2 UJ <34 UJ <92 UJ <46 UJ
<5.3 UJ 2,300 J <53 UJ <27 UJ
180 J 1,400 J 660 J 390 J
<7.5 UJ <28 UJ <75 UJ <37 UJ
<12 UJ <45 UJ <120 UJ <60 UJ
<6.9 UJ <26 UJ <69 UJ <35 UJ
<22 UJ <82 UJ <220 UJ <110 UJ
110,000 270,000 350,000 160,000
----42,000 J 16,000 J
----400 210
----<2 <2
----<2 <2
----230 100
----<2 2.8
----16 14
----99 44
----1,700 790
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----2.3 2.1
----<2 <2
----<2 <2
----<2 <2
----<2 <2
----<20 <20
----<20 <20
----<20 <20
----<20 <20
--------
--------
----<20 <20
--------
--------
----<2 <2
----<2 <2
----<2 <2
----<2 <2
--------
--------
--------
June 2019
Page 35 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
WC-1 GBC-1 CFR-MILE-56 CFR-MILE-56
FAY-SW-WC-1-060719 FAY-SW-GBC-1-060719 FAY-SW-CFR-RM-56-060719 FAY-SW-CFR-RM-56-060719-D
280-124971-3 280-124971-4 280-124971-10 280-124971-11
6/7/2019 6/7/2019 6/7/2019 6/7/2019
------Field Duplicate
TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento
--------
140 J 280 <20 <20
<2 UJ <2 <2 <2
810 J 140 J <5 UJ <5 UJ
420 J 400 <2 <2
67 J 60 <2 <2
16 J 17 <2 <2
540 J 900 <10 <10
5.4 J 2.2 <2 <2
<2 UJ <2 <2 <2
<2 UJ <2 <2 <2
28 J 24 J <2 <2
4 J 2 J <2 <2
41 J 49 J 2 J 2 J
270 J <2 2 J 4.5 J
<2 UJ <2 <2 <2
14 J 4.5 7.5 7.2
<2 UJ <2 <2 <2
<2 UJ <2 <2 <2
17 J 29 <2 <2
<2 UJ <2 <2 <2
<2 UJ <2 <2 <2
<2 UJ <2 <2 <2
<2 UJ <2 <2 <2
2,700 2,500 12 14
320 610 J <4 <4
8.7 11 10 11
<2 <2 <2 <2
<2 <2 <2 <2
2.5 2.3 16 16
<2 <2 <2 <2
5.5 3.7 10 9.9
4.2 3.1 26 26
9.7 9.9 25 25
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
3.7 <2 4.3 4.2
<2 <2 <2 <2
<2 <2 <2 <2
2.6 <2 6.7 7.2
<2 <2 <2 <2
3.6 <2 18 17
<2 <2 <2 <2
<2 <2 <2 <2
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
--------
--------
<20 <20 <20 <20
--------
--------
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
--------
--------
--------
June 2019
Page 36 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
CFR-MILE-68 CFR-MILE-76 CFR-BLADEN CFR-KINGS
FAY-SW-CFR-RM-68-060719 FAY-SW-CFR-RM-76-060719 FAY-SW-CFR-BLADEN-060719 FAY-SW-CFR-KINGS-060719
280-124971-20 280-124971-21 280-124971-22 280-124971-23
6/7/2019 6/7/2019 6/7/2019 6/7/2019
--------
TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento
--------
<20 <20 <20 <20
<2 <2 <2 <2
<5 <5 180 230 J
<2 4.4 64 66
<2 <2 16 20
<2 <2 6.4 8.2
12 18 55 35
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
23 J 2 J 6.3 J 8.3 J
<2 <2 3.4 3.2
20 J 7.9 J 19 J 19 J
320 J 23 J 69 J 82 J
<2 <2 <2 <2
8.2 7.4 8.7 9
<2 <2 <2 <2
<2 <2 2.4 <2
<2 <2 4.9 5
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
390 70 490 520
5 6.9 57 37
8.5 8.5 8.5 7.3
<2 <2 <2 <2
<2 <2 <2 <2
13 12 10 9.6
<2 <2 <2 <2
9.6 8.3 8.7 7.1
21 18 17 15
22 20 20 16
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
4.7 4.5 4.3 3.3
<2 <2 <2 <2
<2 <2 <2 <2
6.6 6.8 6.7 5.5
<2 <2 <2 <2
17 15 15 14
<2 <2 <2 <2
<2 <2 <2 <2
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
--------
--------
<20 <20 <20 <20
--------
--------
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
--------
--------
--------
June 2019
Page 37 of 38 August 2019
TABLE 4
ANALYTICAL RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Event
Location ID
Field Sample ID
Laboratory Sample ID
Date Sampled
QA/QC
Laboratory
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Total Table 3+ Compounds*
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
F-53B Major
F-53B Minor
Notes:
* - Total Table 3+ was calculated using TestAmerica Sacramento
data where it was available since this lab provides a more complete
dataset compared to Eurofins Lancaster. If HFPO-DA was not
analyzed under Table 3+, the corresponding HFPO-DA result from
EPA Method 537 Mod was included in the sum, including data
from Eurofins Lancaster. The total includes J qualified data but not
non-detect data. The total Table 3+ sum is rounded to two
significant figures.
Bold - Analyte detected above associated reporting limit
B - analyte detected in an associated blank
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ND - No Table 3+ compounds were detected above their associated
reporting limits.
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
Outfall 002 Excess River Water EQBLK FBLK
WSTW-OUTFALL 002-060719 WSTW-EXCESS RIVER WATER-060719 EB1-060719 FB1-060719
280-124971-13 280-124971-12 280-124971-15 280-124971-14
6/7/2019 6/7/2019 6/7/2019 6/7/2019
----Equipment Blank Field Blank
TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento TestAmerica Sacramento
--------
<20 UJ <20 <20 <20
<4.1 UJ <2 <2 <2
480 J <5 <5 <5
110 J 20 <2 <2
55 J 3.7 <2 <2
46 J <2 <2 <2
<57 UJ 37 <10 <10
4.5 J <2 <2 <2
2.8 J <2 <2 <2
<6 UJ <2 <2 <2
15 J 2 J <2 <2
61 J <2 <2 <2
110 J 13 J <2 <2
560 J 5.6 J <2 <2
4 J <2 <2 <2
42 J 8.3 <2 <2
<4.6 UJ <2 <2 <2
14 J <2 <2 <2
210 J <2 <2 <2
<3.7 UJ <2 <2 <2
<6 UJ <2 <2 <2
<3.5 UJ <2 <2 <2
<11 UJ <2 <2 <2
1,800 120 ND ND
40 28 <4 <4
8.4 8 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
12 13 <2 <2
<2 <2 <2 <2
12 12 <2 <2
20 22 <2 <2
21 22 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
4.3 4.1 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
7.4 7 <2 <2
<2 <2 <2 <2
15 16 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
--------
--------
<20 <20 <20 <20
--------
--------
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
<2 <2 <2 <2
--------
--------
--------
June 2019
Page 38 of 38 August 2019
TABLE 5
STREAM BED TEMPERATURE SURVEY RESULTS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location Stream Surface
Temp (°C)
Stream bottom
Temp (°C) -
Sediment surface
Stream bottom
Temp (°C) -
2-3 inches below
sediment
Observation
OLDOF-1A 12.9 13.5 --Upwelling
OLDOF-1B 11.7 12.8 --Upwelling
OLDOF-1C 15.9 15.3 --Upwelling
OLDOF-1D 11.6 11.7 --Upwelling
OLDOF-2A 14.0 ----Upwelling
OLDOF-2B 14.0 ----Upwelling
OLDOF-2C 13.9 9.6 --Upwelling
OLDOF-2D 14.0 12.8 --Upwelling
OLDOF-2E 12.0 13.6 17.4 Upwelling
OLDOF-2F 7.5 --10.2 Seep
OLDOF-2G 13.8 13.8 14.9 Upwelling
OLDOF-2H 13.3 13.8 16.3 Upwelling
OLDOF-2I 13.4 15.4 16.9 Seep
OLDOF-2J 16.6 14.6 14.4 Seep
OLDOF-2K 15.0 14.1 13.6 Seep
OLDOF-2L 14.4 14.4 15.7 Upwelling
OLDOF-2M 10.4 13.9 14.3 Seep
OLDOF-4A 16.8 16.6 15.4 Seep
OLDOF-4B 15.5 15.3 15.5 Seep
OLDOF-4C 15.4 15.8 17.3 Upwelling
OLDOF-4D 16.9 15.3 15.8 Seep
OLDOF-4E 17.2 15.4 17.1 Seep
OLDOF-4F 15.9 15.8 15.9 Seep
OLDOF-4G 14.3 15.9 16.4 Seep
OLDOF-4H 15.9 15.7 17.0 Seep
OLDOF-4I 16.7 16.0 17.2 Seep
OLDOF-4J 14.6 16.1 16.9 Seep
OLDOF-4K 17.5 16.1 17.3 Seep
OLDOF-4L 14.9 16.1 17.2 Seep
OLDOF-4M 16.8 16.2 18.1 Seep
OLDOF-4N 16.1 17.6 17.4 Seep
OLDOF-4P 13.6 17.5 18.2 Seep
OLDOF-5A 15.1 17.2 17.3 Seep
OLDOF-5B 16.5 16.9 17.9 Seep
OLDOF-5C 15.9 16.9 18.1 Seep
OLDOF-5D 16.1 17.6 18.4 Seep
OLDOF-5E 16.8 17.3 17.9 Seep
OLDOF-5F 17.9 17.4 18.7 Seep
OLDOF-5G 17.4 17.6 18.1 Seep
OLDOF-5H 17.9 17.8 19.2 Seep
OLDOF-5I 18.9 17.4 19.1 Seep
OLDOF-5J 14.4 16.9 17.3 Seep
OLDOF-5K 14.4 14.4 13.0 Seep
Notes
°C - degrees Celsius
Temp - temperature
-- - Temperature not recorded August 2019
TABLE 6A
TOTAL TABLE 3+ CONCENTRATIONS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
WC-1 2,200 2193 4,800 4765 2,700 2692.4
SEEP-A1 230,000 232,887 300,000 295467 200,000 197620
SEEP-B1 350,000 348314 310,000 309023 340,000 338288
SEEP-B2 310,000 314330 290,000 294350 420,000 420069
SEEP-C1 340,000 344179 350,000 347669 350,000 346000
SEEP-D1 ----170,000 168565 160,000 155467
OLDOF-2 140,000 135040 110,000 112930 130,000 132549
GBC-1 ----2,600 2553 2,500 2517.7
Notes:
ng/L: nanograms per liter
Green bars demonstrate the magnitude of the total Table 3+ concentration relative to other
locations during the same field event.
-- No sample collected
Location
Total Table 3+ Concentrations (ng/L)
February May June
Total Table 3+ concentrations includes the sum of all Table 3+ constituents. The total includes J
qualified data but not non-detect data. The total Table 3+ sum is rounded to two significant
figures.
HFPO-DA is included in the total Table 3+ result, including HFPO-DA results evaluated by EPA
Method 537 Mod.
August 2019
TABLE 6B
HFPO-DA CONCENTRATIONS
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
WC-1 290 J
290 810 J 810 320 320
SEEP-A1 10,000 J
10000 24,000 J 24000 20,000 J 20000
SEEP-B1 24,000 J
24000 22,000 J 22000 27,000 J 27000
SEEP-B2 38,000 J
38000 75,000 75000 85,000 J 85000
SEEP-C1 27,000 J
27000 36,000 J 36000 42,000 J 42000
SEEP-D1 --19,000 J 19000 16,000 J 16000
OLDOF-2 5,900 5900 6,700 J 6700 6,200 J 6200
GBC-2 --500 J 500 610 J 610
Notes:
HFPO-DA: hexafluoropropylene oxide dimer acid
ng/L: nanograms per liter
J - Reported value may not be accurate or precise
Green bars demonstrate the magnitude of the HFPO-DA concentration relative to other locations during the
same field event.
-- No sample collected
HFPO-DA Concentrations (ng/L)
Location February May June
HFPO-DA concentrations measured with EPA Method 537 Mod and Table 3+ analytical methods.
--
--
August 2019
TABLE 7FLOW MEASUREMENT SUMMARYChemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC P.C.WEIR GAUGING TESTSGRADUATED CYLINDERMinimum Median Maximum Mean Geo MeanA-A' B-B' C-C' Minimum Median Maximum Mean Geo MeanTEST-1 967 TEST-21,518TEST-31,220TEST-4365TEST-5485TEST-1582TEST-2380TEST-3468TEST-4370TEST-5463TEST-1395TEST-2326TEST-3315TEST-4362TEST-5344TEST-1534TEST-2481TEST-3804TEST-4350TEST-5275TEST-1338TEST-2342TEST-3371TEST-176.7TEST-280.6TEST-1141TEST-2143TEST-167.1TEST-269.0TEST-162.9TEST-259.0TEST-358.8TEST-1109TEST-2117TEST-3104TEST-150.7TEST-284.7Notes:1. Locations and flow rate measurements/calculations are grouped by date:February 2019 EventMay 2019 EventJune 2019 Event2. Gray shading indicates values calculated from salt dilution test that were determined to be inappropriate due to stream conditions or other factors. These values were excluded from summary statisticsor listed as NA (not appropriate). See comments section above.3. OLDOF-1 location is close to the river mouth but this location is wide, occasionally influenced by river water (e.g., in Feb 2019) and not ideal for tracer testing due to poor lateral mixing.4. Values indicated at Seep B-3A and Seep C-1 locations were determined from a single constant rate salt injection test.5. Flow gauging with weirs performed at select locations based on salt dilution results from the February 2019 field event. EC - electrical conductivity- - no measurements were taken.CALCULATED FLOW RATE (GPM)CALCULATED FLOW RATE (GPM) - Summary StatisticsFLOW RATE (GPM)OLDOF-1 2/1/2019NA NA NA NA NALOCATION DATESALT DILUTION TESTSFLOW VELOCITY METER MEASUREMENTSTEST #CALCULATED FLOW RATE (GPM) - Summary StatisticsComments - Salt Dilution GaugingCALCULATED FLOW RATE (GPM)CALCULATED FLOW RATE (GPM)---- -OLDOF-2 2/1/2019370 422 468 Salt dilution gauging was attempted at OLDOF-1 location during the February 2019 field event. However, this location is not ideal for tracer testing due to stream morphology. A temporary weir could not be installed at this location because of channel width and shallow water depth (less than few inches) precluded accurate point velocity measurements.- ------ 876 876 876 876 876420 402 Test-1 and -3 show broad peak EC response curve with disturbance; non-conclusive; suspect slow release from pool.-876OLDOF-2 5/24/2019315 344 395 348 347 -671 - 702-671 671-OLDOF-2 6/7/2019275 481 804 489 448 671 - - 671 671 671504 504 504 504-- 504OLDOF-3 2/2/2019338 342 371 EC response curve disturbed on rising peak for test-3 and test-5; test not conclusive; test value from -3 and -5 not included in summary statistics.-504 --OLDOF-TR-1 2/2/201976.7 78.6 80.6 78.6 78.6 --------350 350 EC response curve not "ideal"; some disturbance noted on all three tests following peak response.----- -OLDOF-5 2/2/2019141 142 143 142 142 ---------- ---SEEP-A1 2/7/201967.1 68.1 69.0 -----SEEP-A1 5/22/201958.8 59.0 62.9 60.2 60.2 -30------68.1 68.1 --- --- -SEEP-A1 6/7/2019104 109 117 110 110 ---------- ---SEEP-A3 2/7/2019NA NA NA-----------NA NAConcluded salt dilution gauging not appropriate at Seep-A3 and Seep-A4 due to insufficient stream reach.---Page 1 of 3August 2019
TABLE 7FLOW MEASUREMENT SUMMARYChemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC P.C.WEIR GAUGING TESTSGRADUATED CYLINDERMinimum Median Maximum Mean Geo MeanA-A' B-B' C-C' Minimum Median Maximum Mean Geo MeanCALCULATED FLOW RATE (GPM)CALCULATED FLOW RATE (GPM) - Summary StatisticsFLOW RATE (GPM)LOCATION DATESALT DILUTION TESTSFLOW VELOCITY METER MEASUREMENTSTEST #CALCULATED FLOW RATE (GPM) - Summary StatisticsComments - Salt Dilution GaugingCALCULATED FLOW RATE (GPM)CALCULATED FLOW RATE (GPM)TEST-144.8 TEST-246.0 TEST-344.9 TEST-444.6 TEST-148.1 TEST-248.3 TEST-350.6 TEST-1162 TEST-2171 SEEP-A4 5/21/2019 --------0.1 - 3.1 -------- -TEST-111.0 TEST-24.9 TEST-37.0 SEEP-A5 5/21/2019 --------< 1.0 -------- -SEEP A-TR1-1 5/21/2019 --------9.5 - 12 -------- -TEST-188.2 TEST-284.5 TEST-389.9 TEST-153.4 TEST-247.1 TEST-121.9 TEST-222.3 TEST-324.2 TEST-112.3 TEST-211.1 TEST-39.1 TEST-410.5 TEST-112.5 TEST-212.7 TEST-117.7 TEST-218.6 SEEP-B-TR-2 6/7/2019 TEST-13.7 3.7 3.7 3.7 3.7 3.7 -0.3 - 4.0-------- -SEEP-B3A 2/6/2019CONST. INJECTION- ------- -------- -Notes:1. Locations and flow rate measurements/calculations are grouped by date:February 2019 EventMay 2019 EventJune 2019 Event2. Gray shading indicates values calculated from salt dilution test that were determined to be inappropriate due to stream conditions or other factors. These values were excluded from summary statisticsor listed as NA (not appropriate). See comments section above.3. OLDOF-1 location is close to the river mouth but this location is wide, occasionally influenced by river water (e.g., in Feb 2019) and not ideal for tracer testing due to poor lateral mixing.4. Values indicated at Seep B-3A and Seep C-1 locations were determined from a single constant rate salt injection test.5. Flow gauging with weirs performed at select locations based on salt dilution results from the February 2019 field event. EC - electrical conductivity- - no measurements were taken.SEEP-A3 5/22/201944.6 44.9 46.0 45.1 45.1 -15 - 25-- -SEEP-A3 6/7/201948.1 48.3 50.6 49.0 49.0 ---------- ---SEEP-A4 2/7/2019NA NA NA-----SEEP-A4 6/7/20194.9 7.0 11.0 7.6 7.2 --------NA NAConcluded salt dilution gauging not appropriate at Seep-A3 and Seep-A4 due to insufficient stream reach.----- -SEEP-B1 2/5/201984.5 88.2 89.9 87.5 87.5 ---------- ---SEEP-B1 6/7/201947.1 50.3 53.4 -----SEEP-B2 2/5/201921.9 22.3 24.2 22.8 22.8 --------50.3 50.2 --- --- -SEEP-B2 5/22/201910.5 11.1 12.3 11.3 11.3 ---------- ---SEEP-B2 6/7/201912.5 12.6 12.7 EC response curve for test-3 demonstrated EC variations post-peak concentrations; not conclusive test.0.0 - 2.6- --SEEP-B3 2/6/201917.7 18.2 18.6 18.2 18.1 --------12.6 12.6 --- --- -------Page 2 of 3August 2019
TABLE 7FLOW MEASUREMENT SUMMARYChemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC P.C.WEIR GAUGING TESTSGRADUATED CYLINDERMinimum Median Maximum Mean Geo MeanA-A' B-B' C-C' Minimum Median Maximum Mean Geo MeanCALCULATED FLOW RATE (GPM)CALCULATED FLOW RATE (GPM) - Summary StatisticsFLOW RATE (GPM)LOCATION DATESALT DILUTION TESTSFLOW VELOCITY METER MEASUREMENTSTEST #CALCULATED FLOW RATE (GPM) - Summary StatisticsComments - Salt Dilution GaugingCALCULATED FLOW RATE (GPM)CALCULATED FLOW RATE (GPM)SEEP-C1 2/6/2019CONST. INJECTION- ----- - - -------- -SEEP-C1 5/23/2019 - ------ -6.5 - 20-------- -TEST-1 13.8 TEST-213.3 TEST-313.4 TEST-411.9 SEEP -D1 5/23/2019 --------14 - 32-------- -TEST-148.5 TEST-251.3 TEST-345.2 TEST-449.7 TEST-1472 TEST-2860 TEST-3735 TEST-4769 TEST-5514 TEST-6385 GBC-1 6/7/2019 ---------2301 2775 2612 2301 2612 2775 2563 2555-TEST-14,338 TEST-22,942 TEST-32,888 TEST-42,072 WC-1 5/30/2019 ---------2920 2902 - 2902 2911 2920 2911 2911-WC-1 6/7/2019 ---------6471 - - 6471 6471 6471 6471 6471-TEST-13,001 TEST-22,438 TEST-32,168 WC-OUTFALL 6/18/2019 --------- -------- 540WC-1-TR2 6/18/2019 --------- -------- 4.4WC-3-TR2 6/18/2019 --------- -------- 4.8WC-3-TR3 6/18/2019 --------- -------- 3.2WC-3-TR5 6/18/2019 --------- -------- 1.2WC-4-TR1 6/18/2019 --------- -------- 34.2Notes:1. Locations and flow rate measurements/calculations are grouped by date:February 2019 EventMay 2019 EventJune 2019 Event2. Gray shading indicates values calculated from salt dilution test that were determined to be inappropriate due to stream conditions or other factors. These values were excluded from summary statisticsor listed as NA (not appropriate). See comments section above.3. OLDOF-1 location is close to the river mouth but this location is wide, occasionally influenced by river water (e.g., in Feb 2019) and not ideal for tracer testing due to poor lateral mixing.4. Values indicated at Seep B-3A and Seep C-1 locations were determined from a single constant rate salt injection test.5. Flow gauging with weirs performed at select locations based on salt dilution results from the February 2019 field event. EC - electrical conductivity- - no measurements were taken.SEEP-C1 6/7/201911.9 13.3 13.8 13.1 13.1 ---- ---SEEP-D1 6/7/201945.2 49.1 51.3 -----GBC-1 5/29/2019NA NA NA NA NASalt dilution gauging was attempted at GBC-1 location during the May 2019 field event. However, this location is not ideal for tracer testing due to stream morphology as shown by EC response curves. A temporary weir could not be installed at this location because of channel width.-------48.7 48.6 --- -2442 2436-WC-1 2/7/20192,888 2,915 2,942 2,915 2,915 2423 2662 2242 2242 2423 2662---- ---WC-5 2/7/20192,168 2,168 2,168 Salt dilution gauging was attempted at WC-1 location - EC response curves for Test-1 and -4 not appropriate.----------2,168 2,168 Test -1 and -2 not appropriate based on EC response curve; suspect transducer or salt in deep pool.---Page 3 of 3August 2019
TABLE 8A
ESTIMATED FLOW RATES - SEEPS A TO D,
GEORGIA BRANCH CREEK, AND WILLIS CREEK
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Willis Creek 2,915 2,915 2,911 2,911 6,471 6471.48
SEEP-A1 68 68.1 60 60.2 110 109.81
SEEP-A3 ----45 45.1 49 49.00
SEEP-A4 ----1.6 1.6 7.2 7.20
SEEP-B1 87 87.5 ----50 50.16
SEEP-B2 23 22.8 11 11.3 13 12.55
SEEP-C1 ----13 13.2 13 13.09
SEEP-D1 ----23 23.1 49 48.63
Georgia Branch Creek --#REF!2,436 2,436 2,555 2554.96
Notes:
gpm: gallons per minute
Estimated flow rates calculated from salt dilution tests (if appropriate), weir gauging, or
flow velocity measurements (see Table 7). All values shown for the onsite seeps A through
D were determined from the geometric mean flow rate from salt dilution tests with the
exception of Seeps A4, C1, and D1 gauged during the May 2019 event. Flow rates for
Seeps A4, C1, and D1 gauged during the May 2019 event are the median flow rate
calculated from weir gauging measurements. Georgia Branch Creek flow rates were
determined from the geometric mean of flow velocity measurements. Willis Creek flow rates
were determined from the geometric mean of salt dilution tests (February and June 2019)
and the geometric mean of flow velocity measurements (May 2019).
-- No measurement conducted or results were deteremined to be inappropriate due to stream
conditions or other factors.
Location
Estimated Flow Rate (gpm)
February May June
Blue bars demonstrate the magnitude of the flow relative to other locations during the same
field event.
August 2019
TABLE 8B
ESTIMATED FLOW RATES - OLD OUTFALL 002
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants NC, P.C.
Salt Dilution Test 402 402.1 347 347.1 448 447.9
Weir Gauging Measurements ----686 686.5 ----
Flow Velocity Meter Measurements 876 876.0 671 670.7 504 503.84
Notes:
Old Outfall 002 flow rates measured at Location OLDOF-2
gpm: gallons per minute
Blue bars demonstrate the magnitude of the flow determined by one method relative to other methods
employed during the same field event.
-- No measurement conducted.
Methods
Estimated Flow Rate (gpm)
February May June
Estimated flow rates calculated from salt dilution tests (if appropriate), weir gauging, or flow velocity
measurements (see Table 7). Flow rates for Old Outfall 002 were estimated using all three methods for
comparison.
August 2019

FIGURES

")
")
")
Willis Creek
Old Outfall 002Cape Fear RiverOutfall 002
W.O. Huske Dam
Site River Water Intake
NC Highway 87
Seep A
Seep B
Seep C
Seep D
GBCTributary1GeorgiaBranchCreek
Site Location and Site Features
Figure
1Raleigh, NC
2,000 0 2,0001,000 Feet
³
August 2019
Legend
")Site Features
Cape Fear River
Nearby Tributaries
Observed Seep (Natural Drainage)
Site Drainage Network
Site Boundary
Notes:Basemap Sources: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AeroGRID,IGN, and the GIS User Community
Areas at Site
Chemours Monomers IXM
Chemours PPA
Dupont / Dow Leased
Former DuPont PMDF Area
Kuraray America Leased
Wastewater Treatment Plant
Chemours Fayetteville Works, North Carolina
!(
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#*
#*
#*#*
#*
#*
#*
#*
#*#*#*
#*#*
CFR-MILE-76
OLDOF-1
OLDOF-2OLDOF-2J
OLDOF-2L
OLDOF-3OLDOF-4
OLDOF-5
OLDOF-5K
OLDOF-TR1-1-1
SEEP-A-1
SEEP-A-10
SEEP-A-11
SEEP-A-12 SEEP-A-2
SEEP-A-3
SEEP-A-4
SEEP-A-5
SEEP-A-6
SEEP-A-7
SEEP-A-8
SEEP-A-9
SEEP-B-1SEEP-B-2
SEEP-B-3
SEEP-B-3-A1
SEEP-B-3-E4
SEEP-B-4-A3
SEEP-B-4
SEEP-C-1
SEEP-C-1
SEEP-C-1-E2
WC-1
WC-2
WC-3
WC-4
WC-5
Chemours Fayetteville Works, North Carolina
Figure
2ARaleigh, NC
1,000 0 1,000500 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US; Basemap provided by Esri (2017)
Legend
#*Flow Measurement Location
!(Sample Location
Observed Seep
Cape Fear River
Nearby Tributary
Site Boundary
Seep Areas
³
Sample and Flow Measurement Locations -February 2019 Event
1
1
1 0 10.5 Miles
!(
!(
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!(
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WC-1-TR1
SEEP A-3
WC-1
OLDOF-2
SEEP B-1SEEP B-2
SEEP B-TR2
SEEP B-3A
SEEP A-10
SEEP A-5
SEEP A-1
SEEP A-4
SEEP A-TR1-1
SEEP A-TR2-1SEEP A-TR3-1
SEEP A-TR4-1
SEEP C-1
SEEP D-1
WC-4-TR1
WC-3-TR3
WC-3-TR2
WC-1-TR2
CFR-RM-76
SEEP B-TR1 SEEP B-TR1
SEEP A-5-D1-2 SEEP A-5-B-1
EXCESS RIVER WATER
OUTFALL 002
Seep A - Event 1 Locations (Dry)
Chemours Fayetteville Works, North Carolina
Figure
1Raleigh
1,250 0 1,250625 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Sample and Flow Measurement Locations - May 2019 Event
Chemours Fayetteville Works, North Carolina
Figure
2B
1,000 0 1,000500 Feet
³
August 2019
Legend
#*Flow Measurement Locations
!(Sample Location
Observed Seep
Cape Fear River
Nearby Tributary
Site Boundary
Seep Areas
!(
!(
!(
!(
!(!(
!(
!(#*
GBC-6
GBC-5
GBC-3
GBC-2
GBC-TR1-1
GBC-1
GBC-7
GBC-TR2-1
1
2
1
2
³
³
1 0 10.5 Miles
2,000 0 2,0001,000 Feet
Raleigh, NC
!(
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SEEP A-TR1-1
SEEP A-4
SEEP A-1
SEEP B-TR2
SEEP B-2
SEEP B-1
OLDOF-2
WC-1
SEEP A-3
WC-3-TR2
WC-4-TR1
WC-3-TR5
EXCESS RIVER WATER
OUTFALL 002
Seep A - Event 1 Locations (Dry)
Chemours Fayetteville Works, North Carolina
Figure
1Raleigh
1,250 0 1,250625 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Figure
2C
1,000 0 1,000500 Feet
³
August 2019
Legend
#*Flow Measurement Locations
!(Sample Location
Observed Seep
Cape Fear River
Nearby Tributary
Site Boundary
Seep Areas
1
1
2
³
1 0 10.5 Miles
!(#*GBC-1
2 ³
1,000 0 1,000500 Feet
Sample and Flow Measurement Locations - June 2019 Event
Chemours Fayetteville Works, North Carolina
Raleigh, NC
")")
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SEEP -B-3 -E 4
SEE P -B-3-E5
SE EP-B -1-C7 SE EP-B-1-C6
S E EP -B -1 -C5
SEE P-B-1-C 4
SEE P -B-1-C 3
SEEP-B-1-C2
S EEP -B -1 -C1
S EE P -B -1-A1
S EEP -B -1-B 1
S EEP-B -1-B2
S EE P-B-1-D 1
SEE P -B-1-D 2
SEEP -B-1 -D3
SE EP-B -1-D4
SEEP-B-1-E1
SE EP-B-2-A 1
SEEP -B-4 -A 1
SEE P -B-4-A2
S EEP -B -4 -A3
SE EP-B-4-A 4
S EEP -B -3 -E 1
S EEP -B -3 -E2SEEP-B-3-E3
SEEP-A-1-A1
SEEP-A-3-B10
SEEP-A-3-B11
SEEP-A-3-B12
SEEP-A-4-B1
SEEP-A-5-A1SEEP-A-5-A2
SEEP-A-5-A3
SEEP-A-5-A4
SEEP-A-5-A6
SEEP-A-5-A6-2
SEEP-A-5-B1
SEEP-A-5-C1SEEP-A-5-D1
SEEP-A-5-D1-2
SEEP-A-6-A1
SEEP-A-7-A1
SEEP-A-7-B1
SEEP-A-10-A1
SEEP-A-10-B1
SEEP-A-10-C1
SEEP-A-10-C2
SEEP-A-12
SEEP-A-11
SEEP-A-10
SEEP-A-9
SEEP-A-8
SEEP-A-1SEEP-A-2
SEEP-B-2
SEEP-B-3
SEEP-B-3A
SEEP-B-4
SEEP-A-TR4-1
SEEP-A-TR3-1
SEEP-A-TR2-1
SEEP-A-TR1-1
SEEP-A-5 SEEP-A-4
SEEP-A-3
SEEP-B-1
SEEP-B-TR1
SEEP-B-TR2
SEEP-A-6
SEEP-A-7
520 0 520260 Feet
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Identified Seeps (Seeps A and B)
Chemours Fayetteville Works, North Carolina
Figure
3A
Raleigh, NC
500 0 500250 Feet
³
August 2019
Legend
")Seep Location
Observed Seep
Cape Fear River
Nearby Tributary
Site Boundary
Parking Lot
Pump House
1 0 10.5 Miles
³
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SEEP-D-1
SEEP-D-A1
SEEP-D-A1
SEEP-D
SEEP-D-A2
SEEP-D-B1SEEP-D3
SEEP-D2-B1
SEEP-D2-A1
SEEP-D-D2
SEEP-D-C1
SEEP-D-D1
SEEP-D2
OLDOF-4
OLDOF-TR1-1
OLDOF-3
OLD O F-2A
O L D O F -2B
O LDOF-2C
OLDOF 2D
OLDOF 2G
OLDOF 2HOLDOF 2I
OLDOF 2J
OLDOF 2K
OLDOF 2L
OLDOF 2M
OLDOF 4A
OLDOF 4B
OLDOF 4C
OLDOF 4D
OLDOF 4F
OLDOF 4G
OLDOF 4H
OLDOF 4I
OLDOF 4J
OLDOF 4K
OLDOF 4L
OLDOF 4M
OLDOF 4N
OLDOF 4O
OLDOF 5B
OLDOF 5C OLDOF 5D
OLDOF 5F
OLDOF 5G
OLDOF 5H
OLDOF 5IOLDOF 5J
OLDOF 5K S EEP -C-1A
SE E P-C -1 -A 2
SEE P-C -1-B 1
S E EP-C-1-B2
SEE P-C -2C
S EEP -C-1-C 1
SE E P-C -1 -C2
S EE P-C-1-D1SEEP-C -1 -E 1
S E EP-C-1-E2
SE EP -C-1-E3SEEP-C-1-F 1
SE EP-C -1-G1SEEP-C -1 -H1
OLDOF 2F
OLDOF 2E
OLDOF-1C
OLDOF-1B
OLDOF-1A
OLDOF 4E
OLDOF 5
OLDOF-2
OLDOF-1
SEEP-C-1
OLDOF 5A
*
520 0 520260 Feet
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Identified Seeps – Old Outfall 002 and Seeps C and D
Chemours Fayetteville Works, North Carolina
Figure
3B
Raleigh, NC
500 0 500250 Feet
³
August 2019
Legend
")Seep Location
Observed Seep
Cape Fear River
Nearby Tributary
Site Boundary
1 0 10.5 Miles
Notes:* - Tributary not examined for seeps
³
!(
!(!(!(!(
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!(
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CFR-MILE-7618
OLDOF-1130,000
OLDOF-2140,000
OLDOF-2J*8,700
OLDOF-2L150,000
OLDOF-3160,000
OLDOF-4200,000
OLDOF-5290,000
OLDOF-5K
39,000
OLDOF-TR1-1-19,600
SEEP-A-1230,000
SEEP-A-10530,000
SEEP-A-11540,000
SEEP-A-12120,000
SEEP-A-2240,000
SEEP-A-3220,000
SEEP-A-4160,000
SEEP-A-5180,000SEEP-A-6
140,000
SEEP-A-7220,000
SEEP-A-8140,000
SEEP-A-9510,000
SEEP-B-1350,000
SEEP-B-2310,000
SEEP-B-3380,000SEEP-B-3-A1460,000
SEEP-B-3-E445,000
SEEP-B-4670,000
SEEP-B-4-A3430,000
SEEP-C-1340,000
SEEP-C-1-E2
260,000
WC-12,200
WC-2680
WC-3560WC-4340
WC-5370
Chemours Fayetteville Works, North Carolina
Figure
4A
1,000 0 1,000500 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US; Basemap provided by Esri (2017)
Legend
!(Sample Location
Observed Seep
Cape Fear River
Nearby Tributary
Site Boundary
Seep Areas
³
Total Table 3+ Concentrations - February 2019 Event
Notes:* Sample was collected from seep water, not Old Outfall water.
HFPO-DA = hexafluoropropylene oxide dimer acid1. All results are in ng/L (nanograms per liter).2. If samples were analyzed by both TestAmerica Sacramento and Eurofins Lancaster, results from TestAmerica Sacramento are plotted here since this lab provided more complete Table 3+ results. All reported results are provided in Table 4.3. HFPO-DA is included in the total Table 3+ result, including HFPO-DA results evaluated by EPA Method 537 Mod.4. Non-detect values were not included in sum of total Table 3+ results.5. Total Table 3+ results include J-qualified data.
1
1
1 0 10.5 Miles
Raleigh, NC
!(
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!(
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!(
!(
SEEP A-5-B-1*42
SEEP A-5-D1-265,000
SEEP A-TR4-146,000
SEEP A-TR3-1100,000
SEEP A-TR2-182,000
SEEP A-TR1-189,000
SEEP A-4150,000
SEEP A-1300,000
SEEP A-5170,000
SEEP A-10370,000
SEEP B-3A
650,000 SEEP B-TR2250,000
SEEP B-2290,000
SEEP B-1310,000
SEEP B-TR1110,000
SEEP C-1350,000
OLDOF-2110,000
WC-14,800
CFR-RM-7613
SEEP A-3320,000
SEEP-D-1170,000
WC-1-TR1*62
WC-1-TR27,100
WC-3-TR221,000
WC-3-TR34,200
WC-4-TR13,500
EXCESS RIVER WATERND
OUTFALL 002ND
Seep A - Event 1 Locations (Dry)
Chemours Fayetteville Works, North Carolina
Figure
1Raleigh
1,250 0 1,250625 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Total Table 3+ Concentrations – May 2019 Event
Chemours Fayetteville Works, North Carolina
Figure
4B
1,000 0 1,000500 Feet
³
August 2019
Legend
!(Sample Locations
Observed Seep
Cape Fear River
Nearby Tributary
Site Boundary
Seep Areas
Notes:* - Sample collected in channel from river water pump station. Sample is
not a groundwater seep.ND = non detectHFPO-DA = hexafluoropropylene oxide dimer acid1. All results are in ng/L (nanograms per liter).2. HFPO-DA is included in the total Table 3+ result, including HFPO-DA results evaluated by EPA Method 537 Mod.3. Non-detect values were not included in sum of total Table 3+ results.4. Total Table 3+ results include J-qualified data.
!(
!(
!(
!(
!(!(
!(
!(
GBC-73,000
GBC-63,500
GBC-53,300
GBC-TR2-1
1,600 GBC-32,300 GBC-21,900
GBC-TR1-11,100
GBC-12,600
³
1 0 10.5 Miles
1
2
2,000 0 2,0001,000 Feet
³2
1
Raleigh, NC
!(
!(!(
!(!(!(!(
!(
!(
!(
!(
!(
!(
!(
!(
SEEP A-TR1-129,000
SEEP A-4
160,000
SEEP A-1200,000
SEEP B-TR2270,000
SEEP B-2420,000 SEEP B-1340,000
SEEP B-TR1110,000
SEEP C-1350,000
OLDOF-2
130,000
WC-12,700
CFR-RM-7670
SEEP A-3330,000
SEEP-D-1160,000
EXCESS RIVER WATER120
OUTFALL 0021,800
Seep A - Event 1 Locations (Dry)
Chemours Fayetteville Works, North Carolina
Figure
1Raleigh
1,250 0 1,250625 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Total Table 3+ Concentrations -
June 2019 Event
Chemours Fayetteville Works, North Carolina
Figure
4C
1,000 0 1,000500 Feet
³
August 2019
Legend
!(Sample Location
Observed Seep
Cape Fear River
Nearby Tributary
Site Boundary
Seep Areas
Notes:HFPO-DA = hexafluoropropylene oxide dimer acid1. All results are in ng/L (nanograms per liter).2. HFPO-DA is included in the total Table 3+ result, including HFPO-DA results evaluated by EPA Method 537 Mod.3. Non-detect values were not included in sum of total Table 3+results.4. Total Table 3+ results include J-qualified data.
!(
GBC-12,500
³1
2
1 0 10.5 Miles
2
1
600 0 600300 Feet
³
Raleigh, NC
!(
!(!(!(!(
!(!(
!(
!(
!(
!(!(!(
!(
!(!(!(
!(!(!(!(
!(
!(!(!(!(
!(
!(
!(
!(!(
!(
!(
!(
!(
!(
!(
CFR-MILE-76
2.9 J
OLDOF-14,800 J
OLDOF-25,900
OLDOF-2J*1,200
OLDOF-2L6,400
OLDOF-3
5,600
OLDOF-46,900
OLDOF-57,600
OLDOF-5K6,400
OLDOF-TR1-1-11,800
SEEP-A-110,000 J
SEEP-A-1061,000 J
SEEP-A-1155,000 J
SEEP-A-1220,000 J
SEEP-A-227,000 J
SEEP-A-313,000 J
SEEP-A-417,000 J
SEEP-A-5
18,000 JSEEP-A-618,000 J
SEEP-A-728,000 J
SEEP-A-813,000 J
SEEP-A-957,000 J
SEEP-B-124,000 J
SEEP-B-238,000 JSEEP-B-340,000 J
SEEP-B-3-A158,000 J
SEEP-B-3-E410,000 J
SEEP-B-4-A332,000 J
SEEP-B-482,000 J
SEEP-C-127,000 J
SEEP-C-1-E217,000 J
WC-1290 J
WC-2130 J
WC-3120 JWC-451 J
WC-533 J
Figure
5A
1,000 0 1,000500 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US; Basemap provided by Esri (2017)
Legend
!(Sample Location
Observed Seep
Cape Fear River
Nearby Tributary
Site Boundary
Seep Areas
³
HFPO-DA Concentrations - February 2019 Event
Chemours Fayetteville Works, North Carolina
1
1
1 0 10.5 Miles
Notes:* Sample was collected from seep water, not Old Outfall water.All results are in ng/L (nanograms per liter).J = Estimated value.
HFPO-DA = hexafluoropropylene oxide dimer acid.
Raleigh, NC
!(
!(!(
!(
!(
!(
!(!(
!(
!(
!(
!(!(!(!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
!(
SEEP A-5-B-142 J
SEEP A-5-D1-2
12,000 J SEEP A-TR4-1N/ASEEP A-TR3-1N/A
SEEP A-TR2-1N/A
SEEP A-TR1-1
12,000 J
SEEP A-4
20,000 J
SEEP A-124,000 J
SEEP A-529,000 J
SEEP A-1048,000 J
SEEP B-3A150,000
SEEP B-TR242,000
SEEP B-275,000 SEEP B-122,000 J
SEEP B-TR117,000
SEEP C-136,000 J
OLDOF-26,700 J
WC-1810 J
CFR-RM-76
ND
SEEP A-341,000
SEEP-D-119,000 J
WC-1-TR162 J
WC-1-TR23,900
WC-3-TR211,000
WC-3-TR32,400
WC-4-TR11,700
EXCESS RIVER WATERND
OUTFALL 002ND
Seep A - Event 1 Locations (Dry)
Chemours Fayetteville Works, North Carolina
Figure
1Raleigh
1,250 0 1,250625 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
HFPO-DA Concentrations - May 2019 Event
Chemours Fayetteville Works, North Carolina
Figure
5B
1,000 0 1,000500 Feet
³
August 2019
Legend
!(Sample Locations
Observed Seep
Cape Fear River
Nearby Tributary
Site Boundary
SeepAreas
Notes:All results are in ng/L (nanograms per liter).N/A = no data available.ND = non detect.HFPO-DA = hexafluoropropylene oxide dimer acid.
!(
!(
!(
!(
!(!(
!(
!(
GBC-71,200
GBC-61,400
GBC-51,300GBC-TR2-1490
GBC-3
680
GBC-2640
GBC-TR1-1160
GBC-1500 J
³
1 0 10.5 Miles
1,900 0 1,900950 Feet
³
1
2
1
2
Raleigh, NC
!(!(!(
!(!(!(!(
!(
!(
!(
!(
!(
!(
!(
!(
SEEP A-TR1-15,000 J
SEEP A-419,000 J
SEEP A-120,000 J
SEEP B-TR240,000 J
SEEP B-285,000 J
SEEP B-127,000 J
SEEP B-TR119,000 J
SEEP C-142,000 J
OLDOF-26,200 J
WC-1320
CFR-RM-766.9
SEEP A-334,000 J
SEEP-D-116,000 J
EXCESS RIVER WATER28
OUTFALL 00240
Seep A - Event 1 Locations (Dry)
Chemours Fayetteville Works, North Carolina
Figure
1Raleigh
1,250 0 1,250625 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Basemap Sources: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the GIS User Community
HFPO-DA Concentrations - June 2019 Event
Chemours Fayetteville Works, North Carolina
Figure
5C
1,000 0 1,000500 Feet
³
August 2019
Legend
!(Sample Location
Observed Seep
Cape Fear River
Nearby Tributary
Site Boundary
SeepAreas
Notes:All results are in ng/L (nanograms per liter).J = estimated value.HFPO-DA = hexafluoropropylene oxide dimer acid.
!(
GBC-1
610 J
³
1 0 10.5 Miles
1
2
2 ³
600 0 600300 Feet
1
Raleigh, NC
!(
!(
!(
!(
CFR-RM-76
1813
70
CFR-BLADEN
NS
270490
CFR-RM-68
NS32390
CFR-RM-56
NS17
12
CFR-RM-84140NS
NS Seep A - Event 1 Locations (Dry)
Chemours Fayetteville Works, North Carolina
Figure
1Raleigh
14,000 0 14,0007,000 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Cape Fear River Total Table 3+ Concentrations - February, May, and June 2019 Events
Chemours Fayetteville Works, North Carolina
Figure
6A
³
August 2019
Notes:Results are sum of Table 3+ Laboratory Standard Operating Procedure compounds listed in Table 2.HFPO-DA is included in the total Table 3+ result, including HFPO-DA results evaluated by EPA Method 537 Mod.If samples were analyzed by both TestAmerica Sacramento andEurofins Lancaster, results from TestAmerica Sacramento are plottedhere since this lab provided more complete Table 3+ results. All reportedresults are provided in Table 4.Total Table 3+ results include J-qualified data.All results are in ng/L (nanograms per liter).
NS = not sampled.
³
25 0 2512.5 Miles
1
!(
1
CFR-KINGS
NS140
520
Legend
!(Sample Locations
Site Boundary
Cape Fear River
³
2 0 21 Miles
2 0 21 Miles
Value
Value
Value
Concentration - February Event
Concentration - May Event
Concentration - June Event
2 - Downstream
2
Raleigh, NC
!(
!(
!(
!(
CFR-RM-762.9 J
ND
6.9
CFR-BLADEN
NS
2857
CFR-RM-68
NSND5.0
CFR-RM-56
NSND
ND
CFR-RM-84
13NS
NS Seep A - Event 1 Locations (Dry)
Chemours Fayetteville Works, North Carolina
Figure
1Raleigh
14,000 0 14,0007,000 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Cape Fear River HFPO-DA Concentrations - February, May, and June 2019 Events
Chemours Fayetteville Works, North Carolina
Figure
6B
³
August 2019
Notes:All results are in ng/L (nanograms per liter).
J = estimated value.ND = non detect.NS = not sampled.HFPO-DA = hexafluoropropylene oxide dimer acid.
³
30 0 3015 Miles
1
!(
1
CFR-KINGS
NS17
37
³
2 0 21 Miles
2 0 21 Miles
2
Legend
!(Sample Locations
Site Boundary
Cape Fear River
Value
Value
Value
Concentration - February Event
Concentration - May Event
Concentration - June Event
2 - Downstream
Raleigh, NC
APPENDIX A
Field Photograph Record

1 August 2019

APPENDIX A: FIELD PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
Photograph 1

Date: February 2019
Comments: Seep A
Photograph 2

Date: February 2019

Comments: Seep B

2 August 2019

APPENDIX A: FIELD PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
Photograph 3

Date: February 2019

Comments: Seep C
Photograph 4

Date: February 2019

Comments: Old Outfall
3 August 2019
APPENDIX A: FIELD PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
Photograph 5
Date: May 20, 2019
Comments: Operation of
a weir.
Photograph 6
Date: May 21, 2019
Comments: Example of
flow measurement using
a weir.
4 August 2019
APPENDIX A: FIELD PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
Photograph 7
Date: February 5, 2019
Comments: Operation of
a Mariotte Bottle for tracer injection into Seep
C.
APPENDIX B
Field Parameters

Table B1FIELD PARAMETERS Chemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC P.C.LocationDatepH Temperature (°C)Specific Conductivity (mS/cm)Dissolved Oxygen (mg/L)ORP (mV)Turbidity (NTU)CFR River Mile 565/22/20195.925.10.1086.02400.0CFR River Mile 685/22/20196.325.30.0906.21920.0CFR River Mile 765/22/20196.925.40.0866.21890.0CFR Bladen Bluffs5/22/20196.925.30.0987.01880.0CFR Kings Bluff5/23/20196.523.90.0935.01850.0Notes:°C - degrees CelsiusCFR - Cape Fear Rivermg/L - milligrams per litermS/cm - milliSiemens per centimetermV - millivoltNTU - nephelometric turbidity unitsORP - oxidation reduction potentialField parameters were collected from the Cape Fear River but not the seeps and creeks locations. Due to the need to carry all equipment and bottleware to each seep location, the field team elected to prioritize flow measurement and investigative sample collection over field parameter measurement. Seep and creek samples were collected facing oncoming flow from the center of the stream.August 2019
APPENDIX C
Infrared Photograph Record

1 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-1A

Date: February 1, 2019

Comments: Upwelling
OLDOF-1A

Date: February 1, 2019

Comments: Upwelling

2 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-1B

Date: February 2, 2019

Comments: Upwelling
OLDOF-1B

Date: February 2, 2019

Comments: Upwelling

3 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-1C

Date: February 2, 2019

Comments: Upwelling
OLDOF-1C

Date: February 2, 2019

Comments: Upwelling

4 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-1D

Date: February 2, 2019

Comments: Upwelling
OLDOF-1D

Date: February 2, 2019

Comments: Upwelling

5 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number:
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-2A

Date: February 2, 2019

Comments: Upwelling
OLDOF-2A

Date: February 2, 2019

Comments: Upwelling

6 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-2B

Date: February 2, 2019

Comments: Upwelling
OLDOF-2B

Date: February 2, 2019

Comments: Upwelling

7 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-2C

Date: February 2, 2019

Comments: Upwelling
OLDOF-2C

Date: February 2, 2019

Comments: Upwelling

8 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-2D

Date: February 2, 2019

Comments: Upwelling
OLDOF-2D

Date: February 2, 2019

Comments: Upwelling

9 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-2E

Date: February 2, 2019

Comments: Upwelling
OLDOF-2E

Date: February 2, 2019

Comments: Upwelling

10 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-2F

Date: February 2, 2019

Comments: Seep
OLDOF-2F

Date: February 2, 2019

Comments: Seep

11 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-2F

Date: February 2, 2019

Comments: Seep
OLDOF-2F

Date: February 2, 2019

Comments: Seep

12 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-2G

Date: February 2, 2019

Comments: Upwelling
OLDOF-2G

Date: February 2, 2019

Comments: Upwelling

13 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-2H

Date: February 2, 2019

Comments: Upwelling
OLDOF-2H

Date: February 2, 2019

Comments: Upwelling

14 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-2I

Date: February 2, 2019

Comments: Seep
OLDOF-2I

Date: February 2, 2019

Comments: Seep

15 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-2J

Date: February 3, 2019

Comments: Seep
OLDOF-2J

Date: February 3, 2019

Comments: Seep

16 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-2J

Date: February 3, 2019

Comments: Seep
OLDOF-2J

Date: February 3, 2019

Comments: Seep

17 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-2K

Date: February 3, 2019

Comments: Upwelling
OLDOF-2K

Date: February 3, 2019

Comments: Upwelling

18 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-2K

Date: February 3, 2019

Comments: Seep
OLDOF-2K

Date: February 3, 2019

Comments: Seep

19 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-2L

Date: February 3, 2019

Comments: Seep
OLDOF-2L

Date: February 3, 2019

Comments: Seep

20 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-2M

Date: February 3, 2019

Comments: Seep
OLDOF-2M

Date: February 3, 2019

Comments: Seep

21 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-4A

Date: February 3, 2019

Comments: Upwelling
OLDOF-4A

Date: February 3, 2019

Comments: Upwelling

22 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-4B

Date: February 3, 2019

Comments: Seep
OLDOF-4B

Date: February 3, 2019

Comments: Seep

23 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-4C

Date: February 3, 2019

Comments: Seep
OLDOF-4C

Date: February 3, 2019

Comments: Seep

24 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-4D

Date: February 3, 2019

Comments: Seep
OLDOF-4D

Date: February 3, 2019

Comments: Seep

25 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-4E

Date: February 3, 2019

Comments: Seep
OLDOF-4E

Date: February 3, 2019

Comments: Seep

26 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-4F

Date: February 3, 2019

Comments: Seep
OLDOF-4F

Date: February 3, 2019

Comments: Seep

27 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-4G

Date: February 3, 2019

Comments: Seep
OLDOF-4G

Date: February 3, 2019

Comments: Seep

28 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-4H

Date: February 3, 2019

Comments: Seep
OLDOF-4H

Date: February 3, 2019

Comments: Seep

29 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-4I

Date: February 4, 2019

Comments: Seep
OLDOF-4I

Date: February 4, 2019

Comments: Seep

30 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-4J

Date: February 4, 2019

Comments: Seep
OLDOF-4J

Date: February 4, 2019

Comments: Seep

31 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-4K

Date: February 4, 2019

Comments: Seep
OLDOF-4K

Date: February 4, 2019

Comments: Seep

32 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-4L

Date: February 4, 2019

Comments: Seep
OLDOF-4L

Date: February 4, 2019

Comments: Seep

33 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-4M

Date: February 4, 2019

Comments: Seep
OLDOF-4M

Date: February 4, 2019

Comments: Seep

34 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-4N

Date: February 4, 2019

Comments: Seep
OLDOF-4N

Date: February 4, 2019

Comments: Seep

35 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-4P

Date: February 4, 2019

Comments: Seep
OLDOF-4P

Date: February 4, 2019

Comments: Seep

36 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-5A

Date: February 4, 2019

Comments: Seep
OLDOF-5A

Date: February 4, 2019

Comments: Seep

37 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-5B

Date: February 4, 2019

Comments: Seep
OLDOF-5B

Date: February 4, 2019

Comments: Seep

38 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-5C

Date: February 4, 2019

Comments: Seep
OLDOF-5C

Date: February 4, 2019

Comments: Seep

39 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-5D

Date: February 4, 2019

Comments: Seep
OLDOF-5D

Date: February 4, 2019

Comments: Seep

40 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-5E

Date: February 4, 2019

Comments: Seep
OLDOF-5E

Date: February 4, 2019

Comments: Seep

41 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-5F

Date: February 4, 2019

Comments: Seep
OLDOF-5F

Date: February 4, 2019

Comments: Seep

42 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-5G

Date: February 4, 2019

Comments: Seep
OLDOF-5G

Date: February 4, 2019

Comments: Seep

43 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-5H

Date: February 4, 2019

Comments: Seep
OLDOF-5H

Date: February 4, 2019

Comments: Seep

44 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-5I

Date: February 4, 2019

Comments: Seep
OLDOF-5I

Date: February 4, 2019

Comments: Seep

45 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-5J

Date: February 4, 2019

Comments: Seep
OLDOF-5J

Date: February 4, 2019

Comments: Seep

46 August 2019

APPENDIX C: INFRARED CAMERA PHOTOGRAPH RECORD
Seeps and Creeks Investigation
Client: Chemours Project Number: TR0795
Site Name: Chemours Fayetteville Works Site Location: Fayetteville, North Carolina
OLDOF-5K

Date: February 4, 2019

Comments: Seep
OLDOF-5K

Date: February 4, 2019

Comments: Seep
APPENDIX D
Flow Velocity Measurement Summary

TABLE D1FLOW VELOCITY MEASUREMENT SUMMARY - SEEPS AND CREEKS INVESTIGATIONChemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC P.C.Distance Along Measured Cross SectionMeasured Depth to Water3Measured Depth to Creek BottomCalculated Water Column DepthCalculated Creek Cell Area4Measured Creek VelocityCalculated Discharge Through Creek Cell Area5,6(ft)(ft)(ft)(ft)(ft2)(ft/s)(ft3/s)Old Outfall Channel (OLDOF-02) February 1, 2019 A0.5--12--0.50----Old Outfall Channel (OLDOF-02) February 1, 2019 B1.012120.150.500.0750.080Old Outfall Channel (OLDOF-02) February 1, 2019 C1.512120.210.500.110.11Old Outfall Channel (OLDOF-02) February 1, 2019 D2.012120.190.500.0950.13Old Outfall Channel (OLDOF-02) February 1, 2019 E2.512130.430.500.220.33Old Outfall Channel (OLDOF-02) February 1, 2019 F3.012130.420.500.210.43Old Outfall Channel (OLDOF-02) February 1, 2019 G3.512130.500.500.250.46Old Outfall Channel (OLDOF-02) February 1, 2019 H4.012130.330.500.170.18Old Outfall Channel (OLDOF-02) February 1, 2019 I4.512120.300.500.150.16Old Outfall Channel (OLDOF-02) February 1, 2019 J5.012130.370.500.190.078Georgia Branch 04 (SW-GB-04) May 9, 2019A1.0dry11dry------Georgia Branch 04 (SW-GB-04) May 9, 2019B2.0dry11dry------Georgia Branch 04 (SW-GB-04) May 9, 2019C3.0dry11dry------Georgia Branch 04 (SW-GB-04) May 9, 2019D4.0dry11dry------Georgia Branch 04 (SW-GB-04) May 9, 2019E5.0dry11dry------Georgia Branch 04 (SW-GB-04) May 9, 2019F6.0dry12dry------Georgia Branch 04 (SW-GB-04) May 9, 2019G7.0dry12dry------Georgia Branch 04 (SW-GB-04) May 9, 2019H8.012130.90.87-0.020--Georgia Branch 04 (SW-GB-04) May 9, 2019I9.012131.21.0-0.010--Georgia Branch 04 (SW-GB-04) May 9, 2019J1012141.71.5-0.010--Georgia Branch 04 (SW-GB-04) May 9, 2019K1112141.81.80.030--Georgia Branch 04 (SW-GB-04) May 9, 2019L1212141.91.80.0300.053Georgia Branch 04 (SW-GB-04) May 9, 2019M1312141.71.80.0400.055Georgia Branch 04 (SW-GB-04) May 9, 2019N1412141.61.70.0500.062Georgia Branch 04 (SW-GB-04) May 9, 2019O1512141.71.70.0400.075Georgia Branch 04 (SW-GB-04) May 9, 2019P1612141.61.60.00.075Georgia Branch 04 (SW-GB-04) May 9, 2019Q1712131.01.3-0.010-Georgia Branch 04 (SW-GB-04) May 9, 2019R1812131.01.00.0-Georgia Branch 04 (SW-GB-04) May 9, 2019S19dry13dry------Georgia Branch 04 (SW-GB-04) May 9, 2019T20dry12dry------Georgia Branch 04 (SW-GB-04) May 9, 2019U 21dry12dry------Georgia Branch 04 (SW-GB-04) May 9, 2019V22dry12dry------Georgia Branch 04 (SW-GB-04) May 9, 2019W23dry11dry------Willis Creek 04 (SW-WC-04)May 9, 2019 Culvert Edge0.09.2101.0------Willis Creek 04 (SW-WC-04)May 9, 2019A0.59.2101.00.520.660.34Willis Creek 04 (SW-WC-04)May 9, 2019B1.09.2101.10.520.600.33Willis Creek 04 (SW-WC-04)May 9, 2019C1.59.1101.10.550.550.31Willis Creek 04 (SW-WC-04)May 9, 2019D2.09.1101.00.520.530.28Willis Creek 04 (SW-WC-04)May 9, 2019E2.59.1100.910.470.590.26Willis Creek 04 (SW-WC-04)May 9, 2019F3.09.2100.820.430.590.26Willis Creek 04 (SW-WC-04)May 9, 2019G3.59.1100.830.410.530.23Willis Creek 04 (SW-WC-04)May 9, 2019H4.09.1101.00.450.590.25Willis Creek 04 (SW-WC-04)May 9, 2019I4.59.1100.950.480.480.26Willis Creek 04 (SW-WC-04)May 9, 2019J5.09.1100.910.470.530.23Willis Creek 04 (SW-WC-04)May 9, 2019K5.59.1100.920.460.530.24Willis Creek 04 (SW-WC-04)May 9, 2019L6.09.2100.850.440.500.23Willis Creek 04 (SW-WC-04)May 9, 2019M7.09.2100.800.820.430.38Location1DateMeasurement Point2Page 1 of 3August 2019
TABLE D1FLOW VELOCITY MEASUREMENT SUMMARY - SEEPS AND CREEKS INVESTIGATIONChemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC P.C.Distance Along Measured Cross SectionMeasured Depth to Water3Measured Depth to Creek BottomCalculated Water Column DepthCalculated Creek Cell Area4Measured Creek VelocityCalculated Discharge Through Creek Cell Area5,6(ft)(ft)(ft)(ft)(ft2)(ft/s)(ft3/s)Location1DateMeasurement Point2Willis Creek 04 (SW-WC-04)May 9, 2019N7.59.1100.820.410.410.17Willis Creek 04 (SW-WC-04)May 9, 2019O8.09.19.90.790.400.320.15Willis Creek 04 (SW-WC-04)May 9, 2019 Culvert Edge8.59.19.90.790.40--0.13Old Outfall Channel (OLDOF-02) May 24, 2019N0.0dry12dry----0.0Old Outfall Channel (OLDOF-02) May 24, 2019A1.412120.210.150.830.12Old Outfall Channel (OLDOF-02) May 24, 2019B3.112130.380.491.20.60Old Outfall Channel (OLDOF-02) May 24, 2019C4.312130.290.421.30.55Old Outfall Channel (OLDOF-02) May 24, 2019S5.6dry12dry0.181.20.22Georgia Branch A-A'May 29, 2019 W0.0dry--dry----0.0Georgia Branch A-A'May 29, 2019A1.0----0.460.230.950.22Georgia Branch A-A'May 29, 2019B5.9----0.382.01.12.3Georgia Branch A-A'May 29, 2019C9.1----0.401.31.41.7Georgia Branch A-A'May 29, 2019D12----0.190.701.30.95Georgia Branch A-A'May 29, 2019E14dry--dry0.231.00.24Georgia Branch B-B'May 29, 2019 W0.0dry--dry----0.0Georgia Branch B-B'May 29, 2019A2.3----0.330.371.40.51Georgia Branch B-B'May 29, 2019B4.9----0.290.821.31.1Georgia Branch B-B'May 29, 2019C8.8----0.271.11.31.5Georgia Branch B-B'May 29, 2019D12----0.401.21.51.8Georgia Branch B-B'May 29, 2019E16dry--dry0.711.51.1Georgia Branch C-C'May 29, 2019 W0.0dry--dry----0.0Georgia Branch C-C'May 29, 2019A2.0----0.330.341.70.58Georgia Branch C-C'May 29, 2019B5.1----0.290.951.31.3Georgia Branch C-C'May 29, 2019C9.5----0.271.20.981.2Georgia Branch C-C'May 29, 2019D13----0.401.11.21.3Georgia Branch C-C'May 29, 2019E15dry--dry0.451.40.64Willis Creek A-A'May 30, 2019 W0.0dry--dry----0.0Willis Creek A-A'May 30, 2019A2.6----0.781.00.280.29Willis Creek A-A'May 30, 2019B5.2----0.752.00.631.2Willis Creek A-A'May 30, 2019C8.0----0.792.10.972.1Willis Creek A-A'May 30, 2019D11----0.772.20.881.9Willis Creek A-A'May 30, 2019E14dry--dry1.20.800.98Willis Creek B-B'May 30, 2019 W0.0dry--dry----0.0Willis Creek B-B'May 30, 2019A3.0----0.510.770.100.077Willis Creek B-B'May 30, 2019B9.7----1.316.10.493.0Willis Creek B-B'May 30, 2019C17----0.526.30.603.8Willis Creek B-B'May 30, 2019D23----0.663.5-0.012-0.042Willis Creek B-B'May 30, 2019E26dry--dry1.1-0.31-0.34Old Outfall Channel (OLDOF-02) June 7, 2019N0.0dry12dry----0.0Old Outfall Channel (OLDOF-02) June 7, 2019A1.212120.190.110.900.10Old Outfall Channel (OLDOF-02) June 7, 2019B2.312130.170.201.30.27Old Outfall Channel (OLDOF-02) June 7, 2019C3.512130.380.301.70.52Old Outfall Channel (OLDOF-02) June 7, 2019S4.2dry12dry0.141.70.24Georgia Branch A-A'June 7, 2019W0.0dry12dry----0.0Georgia Branch A-A'June 7, 2019A1.7----0.500.431.30.55Georgia Branch A-A'June 7, 2019B4.6----0.311.21.31.5Georgia Branch A-A'June 7, 2019C8.6----0.361.31.41.9Georgia Branch A-A'June 7, 2019D12----0.150.831.31.1Georgia Branch A-A'June 7, 2019E14dry12dry0.150.760.11Page 2 of 3August 2019
TABLE D1FLOW VELOCITY MEASUREMENT SUMMARY - SEEPS AND CREEKS INVESTIGATIONChemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC P.C.Distance Along Measured Cross SectionMeasured Depth to Water3Measured Depth to Creek BottomCalculated Water Column DepthCalculated Creek Cell Area4Measured Creek VelocityCalculated Discharge Through Creek Cell Area5,6(ft)(ft)(ft)(ft)(ft2)(ft/s)(ft3/s)Location1DateMeasurement Point2Georgia Branch B-B'June 7, 2019W0.0dry--dry----0.0Georgia Branch B-B'June 7, 2019A1.2----0.460.281.10.32Georgia Branch B-B'June 7, 2019B5.0----0.361.61.21.9Georgia Branch B-B'June 7, 2019C9.0----0.341.41.52.1Georgia Branch B-B'June 7, 2019D13----0.291.31.31.6Georgia Branch B-B'June 7, 2019E15dry--dry0.290.900.26Georgia Branch C-C'June 7, 2019W0.0dry--dry----0.0Georgia Branch C-C'June 7, 2019A2.5----0.350.451.40.62Georgia Branch C-C'June 7, 2019B5.8----0.441.31.51.9Georgia Branch C-C'June 7, 2019C9.8----0.171.21.51.8Georgia Branch C-C'June 7, 2019D14----0.270.881.31.1Georgia Branch C-C'June 7, 2019E16dry--dry0.271.20.33Willis Creek A-A'June 7, 2019W0.0dry--dry----0.0Willis Creek A-A'June 7, 2019A1.7----0.730.61-0.14-0.082Willis Creek A-A'June 7, 2019B4.3----1.22.60.421.1Willis Creek A-A'June 7, 2019C8.0----1.85.51.36.9Willis Creek A-A'June 7, 2019D11----1.54.01.25.0Willis Creek A-A'June 7, 2019E13dry--dry1.80.841.5Acronyms:-- - data not measured or calculatedft - feetft2 - square feetft3/s - cubic feet per secondNotes:5 - Discharge is calculated as creek velocity (ft/s) multiplied by the cross sectional area of each measurement cell (ft2).6 - Data for the channel's edge points are extrapolated from adjacent locations. 4 - Measurement cell areas are calculated assuming a rectangular geometry based on distances between measurement points and the calculated water column depths. A measurement cell is an areal section from the width of the river channel. 3 - The depth for the velocity meter was determined based on one depth measurement.2 - Measurement points E and W represent the eastern and western edge of a transect, respectively. Measurement points A through D are taken along the transect between points E and W at the listed distances along the cross section.1 - Locations A-A', B-B', or C-C' represent triplicate measurements from the same stream, taken along a transect with A furthest upstream and C furthest downstream, each transect a few feet apart. Measurement locations along these transects marked 'E' or 'W' stand for an east or west starting location. Page 3 of 3August 2019
APPENDIX E
Salt Dilution Gauging Summary

APPENDIX E1: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/1/2019 3:26:17 PM 347.8 -
2/1/2019 3:26:18 PM 347.9 -
2/1/2019 3:26:19 PM 347.9 -
2/1/2019 3:26:20 PM 347.9 -
2/1/2019 3:26:21 PM 347.8 -
2/1/2019 3:26:22 PM 347.9 -
2/1/2019 3:26:23 PM 348 -
2/1/2019 3:26:24 PM 348 -
2/1/2019 3:26:25 PM 348 -
2/1/2019 3:26:26 PM 348 -
2/1/2019 3:26:27 PM 348.1 -
2/1/2019 3:26:28 PM 348 -
2/1/2019 3:26:29 PM 347.9 -
2/1/2019 3:26:30 PM 347.8 -
2/1/2019 3:26:31 PM 347.8 -
2/1/2019 3:26:32 PM 347.7 -
2/1/2019 3:26:33 PM 347.7 -
2/1/2019 3:26:34 PM 347.6 -
2/1/2019 3:26:35 PM 347.5 -
2/1/2019 3:26:36 PM 347.3 -
2/1/2019 3:26:37 PM 347.2 -
2/1/2019 3:26:38 PM 347.1 -
2/1/2019 3:26:39 PM 346.9 -
2/1/2019 3:26:40 PM 346.7 -
2/1/2019 3:26:41 PM 346.6 -
2/1/2019 3:26:42 PM 346.5 -
2/1/2019 3:26:43 PM 346.5 -
2/1/2019 3:26:44 PM 346.6 -
2/1/2019 3:26:45 PM 347.5 -
2/1/2019 3:26:46 PM 414.9 67.4
2/1/2019 3:26:47 PM 474.3 126.8
2/1/2019 3:26:48 PM 629.4 281.9
2/1/2019 3:26:49 PM 795.2 447.7
2/1/2019 3:26:50 PM 1246.1 898.6
2/1/2019 3:26:51 PM 1337.1 989.6
2/1/2019 3:26:52 PM 1497.7 1150.2
2/1/2019 3:26:53 PM 1557.2 1209.7
2/1/2019 3:26:54 PM 1613.9 1266.4
2/1/2019 3:26:55 PM 1624.2 1276.7
2/1/2019 3:26:56 PM 1507 1159.5
2/1/2019 3:26:57 PM 1410.5 1063.0
2/1/2019 3:26:58 PM 1217.4 869.9
2/1/2019 3:26:59 PM 1062.3 714.8
2/1/2019 3:27:00 PM 947.5 600.0
2/1/2019 3:27:01 PM 851.8 504.3
2/1/2019 3:27:02 PM 779.5 432.0
2/1/2019 3:27:03 PM 673.1 325.6
2/1/2019 3:27:04 PM 560.2 212.7
2/1/2019 3:27:05 PM 553.1 205.6
2/1/2019 3:27:06 PM 513.1 165.6
2/1/2019 3:27:07 PM 494.2 146.7
2/1/2019 3:27:08 PM 476.7 129.2
2/1/2019 3:27:09 PM 468.5 121.0
2/1/2019 3:27:10 PM 459.7 112.2
2/1/2019 3:27:11 PM 451.3 103.8
2/1/2019 3:27:12 PM 442.7 95.2
2/1/2019 3:27:13 PM 437.5 90.0
2/1/2019 3:27:14 PM 431.9 84.4
2/1/2019 3:27:15 PM 426.8 79.3
2/1/2019 3:27:16 PM 421.5 74.0
2/1/2019 3:27:17 PM 417.4 69.9
2/1/2019 3:27:18 PM 413.2 65.7
2/1/2019 3:27:19 PM 409.9 62.4
2/1/2019 3:27:20 PM 404.8 57.3
2/1/2019 3:27:21 PM 397.2 49.7
2/1/2019 3:27:22 PM 389.5 42.0
2/1/2019 3:27:23 PM 382.4 34.9
2/1/2019 3:27:24 PM 378.8 31.3
2/1/2019 3:27:25 PM 374 26.5
2/1/2019 3:27:26 PM 369.8 22.3
Table E1 OLDOF-2 TEST-2 Data Log
Page 1 of 452 August 2019
APPENDIX E1: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-2 TEST-2 Data Log
2/1/2019 3:27:27 PM 367 19.5
2/1/2019 3:27:28 PM 364.4 16.9
2/1/2019 3:27:29 PM 362.6 15.1
2/1/2019 3:27:30 PM 360.6 13.1
2/1/2019 3:27:31 PM 359.2 11.7
2/1/2019 3:27:32 PM 357.8 -
2/1/2019 3:27:33 PM 356.6 -
2/1/2019 3:27:34 PM 355.5 -
2/1/2019 3:27:35 PM 354.6 -
2/1/2019 3:27:36 PM 353.7 -
2/1/2019 3:27:37 PM 353.2 -
2/1/2019 3:27:38 PM 352.7 -
2/1/2019 3:27:39 PM 352.4 -
2/1/2019 3:27:40 PM 352 -
2/1/2019 3:27:41 PM 351.7 -
2/1/2019 3:27:42 PM 351.4 -
2/1/2019 3:27:43 PM 351.1 -
2/1/2019 3:27:44 PM 350.8 -
2/1/2019 3:27:45 PM 350.5 -
2/1/2019 3:27:46 PM 350.3 -
2/1/2019 3:27:47 PM 350.1 -
2/1/2019 3:27:48 PM 349.9 -
2/1/2019 3:27:49 PM 349.7 -
2/1/2019 3:27:50 PM 349.4 -
2/1/2019 3:27:51 PM 349 -
2/1/2019 3:27:52 PM 348.6 -
2/1/2019 3:27:53 PM 348.3 -
2/1/2019 3:27:54 PM 348.1 -
2/1/2019 3:27:55 PM 347.9 -
2/1/2019 3:27:56 PM 347.6 -
2/1/2019 3:27:57 PM 347.4 -
2/1/2019 3:27:58 PM 347.3 -
2/1/2019 3:27:59 PM 347 -
Page 2 of 452 August 2019
APPENDIX E1: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
OLDOF-2 TEST-2 1441
OLDOF-2 TEST-2 1443
OLDOF-2 TEST-2 1444
OLDOF-2 TEST-2 1445
Location EC Reading
(µS/cms)
OLDOF-2 TEST-2 204
OLDOF-2 TEST-2 1,804
OLDOF-2 TEST-2 15,938
OLDOF-2 TEST-2 123,591
q 300,000
K 1.2395
23.9
379.8
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Table E2 OLDOF-2 TEST-2 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
(µS/cms)(°C)
342.3 13.9
343.7 13.9
340.7 13.9
340.8 13.9
Average 341.9 (µS/cms)
Geometric Mean 341.9 (µS/cms)
Average (pre-test)347.5 (µS/cms)
19.3
1,000 20.4
Average (post-test)350.9 (µS/cms)
Table E3 OLDOF-2 TEST-2 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement Part
2: Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8, no. 1,
2004, pp. 11–15.
Slope of Calibration Curve (µS/cms) / (mg/L)
Integral of Conductivity Data Curve SUM:Δt(ECt-
ECbkg)15,541.0 (s) . (µS/cms)
Calculated Flow Rate Q L/s
GPM
10,000 20.1
100,000 19.7
Table E4 OLDOF-2 TEST-2 Flow Calculation Summary
Mass of Salt injected mg
(mg/L)(°C)
100
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 3 of 452 August 2019
APPENDIX E2: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-4 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/1/2019 3:55:16 PM 337.1 -
2/1/2019 3:55:17 PM 336.9 -
2/1/2019 3:55:18 PM 336.8 -
2/1/2019 3:55:19 PM 337 -
2/1/2019 3:55:20 PM 337 -
2/1/2019 3:55:21 PM 336.6 -
2/1/2019 3:55:22 PM 336.2 -
2/1/2019 3:55:23 PM 335.9 -
2/1/2019 3:55:24 PM 335.8 -
2/1/2019 3:55:25 PM 335.7 -
2/1/2019 3:55:26 PM 335.6 -
2/1/2019 3:55:27 PM 335.6 -
2/1/2019 3:55:28 PM 335.5 -
2/1/2019 3:55:29 PM 335.5 -
2/1/2019 3:55:30 PM 335.4 -
2/1/2019 3:55:31 PM 335.2 -
2/1/2019 3:55:32 PM 335.1 -
2/1/2019 3:55:33 PM 335.1 -
2/1/2019 3:55:34 PM 335.1 -
2/1/2019 3:55:35 PM 335.1 -
2/1/2019 3:55:36 PM 335.1 -
2/1/2019 3:55:37 PM 335.1 -
2/1/2019 3:55:38 PM 334.9 -
2/1/2019 3:55:39 PM 334.6 -
2/1/2019 3:55:40 PM 334.5 -
2/1/2019 3:55:41 PM 334.7 -
2/1/2019 3:55:42 PM 335.6 -
2/1/2019 3:55:43 PM 337.5 -
2/1/2019 3:55:44 PM 416.6 80.9
2/1/2019 3:55:45 PM 540.5 204.8
2/1/2019 3:55:46 PM 656.9 321.2
2/1/2019 3:55:47 PM 739.7 404.0
2/1/2019 3:55:48 PM 1052.7 717.0
2/1/2019 3:55:49 PM 1171.5 835.8
2/1/2019 3:55:50 PM 1324.7 989.0
2/1/2019 3:55:51 PM 1382.1 1046.4
2/1/2019 3:55:52 PM 1423 1087.3
2/1/2019 3:55:53 PM 1452.7 1117.0
2/1/2019 3:55:54 PM 1565.2 1229.5
2/1/2019 3:55:55 PM 1541.5 1205.8
2/1/2019 3:55:56 PM 1398 1062.3
2/1/2019 3:55:57 PM 1338.6 1002.9
2/1/2019 3:55:58 PM 1094 758.3
2/1/2019 3:55:59 PM 982.6 646.9
2/1/2019 3:56:00 PM 877.9 542.2
2/1/2019 3:56:01 PM 754.8 419.1
2/1/2019 3:56:02 PM 663.6 327.9
2/1/2019 3:56:03 PM 509.4 173.7
2/1/2019 3:56:04 PM 543.1 207.4
2/1/2019 3:56:05 PM 531.6 195.9
2/1/2019 3:56:06 PM 521.9 186.2
2/1/2019 3:56:07 PM 511.4 175.7
2/1/2019 3:56:08 PM 448.6 112.9
2/1/2019 3:56:09 PM 430.5 94.8
2/1/2019 3:56:10 PM 414.6 78.9
2/1/2019 3:56:11 PM 409.1 73.4
2/1/2019 3:56:12 PM 400.4 64.7
2/1/2019 3:56:13 PM 394.4 58.7
2/1/2019 3:56:14 PM 390.9 55.2
2/1/2019 3:56:15 PM 387 51.3
2/1/2019 3:56:16 PM 384.6 48.9
2/1/2019 3:56:17 PM 382.2 46.5
2/1/2019 3:56:18 PM 380.3 44.6
2/1/2019 3:56:19 PM 378.7 43.0
2/1/2019 3:56:20 PM 376.2 40.5
2/1/2019 3:56:21 PM 374.8 39.1
2/1/2019 3:56:22 PM 373.2 37.5
2/1/2019 3:56:23 PM 371.4 35.7
2/1/2019 3:56:24 PM 369.9 34.2
2/1/2019 3:56:25 PM 365.8 30.1
Table E1 OLDOF-2 TEST-4 Data Log
Page 4 of 452 August 2019
APPENDIX E2: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-4 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-2 TEST-4 Data Log
2/1/2019 3:56:26 PM 362.7 27.0
2/1/2019 3:56:27 PM 360.3 24.6
2/1/2019 3:56:28 PM 358.1 -
2/1/2019 3:56:29 PM 356.4 -
2/1/2019 3:56:30 PM 354.5 -
2/1/2019 3:56:31 PM 353.2 -
2/1/2019 3:56:32 PM 352 -
2/1/2019 3:56:33 PM 351.2 -
2/1/2019 3:56:34 PM 350.7 -
2/1/2019 3:56:35 PM 350.2 -
2/1/2019 3:56:36 PM 350 -
2/1/2019 3:56:37 PM 350 -
2/1/2019 3:56:38 PM 350 -
Page 5 of 452 August 2019
APPENDIX E2: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-4 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
OLDOF-2 TEST-4 1441
OLDOF-2 TEST-4 1443
OLDOF-2 TEST-4 1444
OLDOF-2 TEST-4 1445
Location EC Reading
(µS/cms)
OLDOF-2 TEST-4 204
OLDOF-2 TEST-4 1,804
OLDOF-2 TEST-4 15,938
OLDOF-2 TEST-4 123,591
q 300,100
K 1.2395
23.3
369.5
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Table E2 OLDOF-2 TEST-4 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
(µS/cms) (°C)
342.3 13.9
343.7 13.9
340.7 13.9
340.8 13.9
Average 341.9 (µS/cms)
Geometric Mean 341.9 (µS/cms)
Average (pre-test) 338.5 (µS/cms)
1,000 20.4
Average (post-test) 351.0 (µS/cms)
Table E3 OLDOF-2 TEST-4 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement Part
2: Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8, no. 1,
2004, pp. 11–15.
Slope of Calibration Curve (µS/cms) / (mg/L)
Integral of Conductivity Data Curve SUM:Δt(ECt-
ECbkg)15,977.9 (s) . (µS/cms)
Calculated Flow Rate Q
L/s
GPM
10,000 20.1
100,000 19.7
Table E4 OLDOF-2 TEST-4 Flow Calculation Summary
Mass of Salt injected mg
(mg/L) (°C)
100 19.3
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 6 of 452 August 2019
APPENDIX E3: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-5 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/1/2019 3:59:04 PM 318.7 -
2/1/2019 3:59:05 PM 318.5 -
2/1/2019 3:59:06 PM 318.3 -
2/1/2019 3:59:07 PM 318.2 -
2/1/2019 3:59:08 PM 318.2 -
2/1/2019 3:59:09 PM 318.1 -
2/1/2019 3:59:10 PM 318.0 -
2/1/2019 3:59:11 PM 317.9 -
2/1/2019 3:59:12 PM 317.8 -
2/1/2019 3:59:13 PM 317.6 -
2/1/2019 3:59:14 PM 317.4 -
2/1/2019 3:59:15 PM 317.3 -
2/1/2019 3:59:16 PM 317.2 -
2/1/2019 3:59:17 PM 317.1 -
2/1/2019 3:59:18 PM 317.0 -
2/1/2019 3:59:19 PM 317.0 -
2/1/2019 3:59:20 PM 316.9 -
2/1/2019 3:59:21 PM 316.8 -
2/1/2019 3:59:22 PM 316.7 -
2/1/2019 3:59:23 PM 316.6 -
2/1/2019 3:59:24 PM 316.6 -
2/1/2019 3:59:25 PM 316.5 -
2/1/2019 3:59:26 PM 316.4 -
2/1/2019 3:59:27 PM 316.4 -
2/1/2019 3:59:28 PM 316.3 -
2/1/2019 3:59:29 PM 316.3 -
2/1/2019 3:59:30 PM 317.0 -
2/1/2019 3:59:31 PM 499.5 182.2
2/1/2019 3:59:32 PM 576.6 259.3
2/1/2019 3:59:33 PM 785.0 467.7
2/1/2019 3:59:34 PM 1184.0 866.7
2/1/2019 3:59:35 PM 1099.3 782.0
2/1/2019 3:59:36 PM 1428.3 1111.0
2/1/2019 3:59:37 PM 1486.1 1168.8
2/1/2019 3:59:38 PM 1586.7 1269.4
2/1/2019 3:59:39 PM 1571.5 1254.2
2/1/2019 3:59:40 PM 1342.9 1025.6
2/1/2019 3:59:41 PM 1169.6 852.3
2/1/2019 3:59:42 PM 1058.4 741.1
2/1/2019 3:59:43 PM 890.9 573.6
2/1/2019 3:59:44 PM 766.6 449.3
2/1/2019 3:59:45 PM 674.1 356.8
2/1/2019 3:59:46 PM 513.2 195.9
2/1/2019 3:59:47 PM 522.0 204.7
2/1/2019 3:59:48 PM 496.0 178.7
2/1/2019 3:59:49 PM 418.2 100.9
2/1/2019 3:59:50 PM 392.8 75.5
2/1/2019 3:59:51 PM 374.4 57.1
2/1/2019 3:59:52 PM 369.9 52.6
2/1/2019 3:59:53 PM 365.9 48.6
2/1/2019 3:59:54 PM 361.2 43.9
2/1/2019 3:59:55 PM 356.9 39.6
2/1/2019 3:59:56 PM 354.4 37.1
2/1/2019 3:59:57 PM 351.6 34.3
2/1/2019 3:59:58 PM 349.4 32.1
2/1/2019 3:59:59 PM 347.3 30.0
2/1/2019 4:00:00 PM 345.8 28.5
2/1/2019 4:00:01 PM 344.3 27.0
2/1/2019 4:00:02 PM 343.1 25.8
2/1/2019 4:00:03 PM 341.8 24.5
2/1/2019 4:00:04 PM 340.8 23.5
2/1/2019 4:00:05 PM 339.2 21.9
2/1/2019 4:00:06 PM 336.6 19.3
2/1/2019 4:00:07 PM 334.3 17.0
2/1/2019 4:00:08 PM 332.7 15.4
2/1/2019 4:00:09 PM 330.4 13.1
2/1/2019 4:00:10 PM 329.0 11.7
2/1/2019 4:00:11 PM 327.8 10.5
2/1/2019 4:00:12 PM 325.9 8.6
2/1/2019 4:00:13 PM 324.3 -
Table E1 OLDOF-2 TEST-5 Data Log
Page 7 of 452 August 2019
APPENDIX E3: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-5 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-2 TEST-5 Data Log
2/1/2019 4:00:14 PM 322.9 -
2/1/2019 4:00:15 PM 321.4 -
2/1/2019 4:00:16 PM 320.1 -
2/1/2019 4:00:17 PM 318.8 -
2/1/2019 4:00:18 PM 317.6 -
2/1/2019 4:00:19 PM 316.4 -
2/1/2019 4:00:20 PM 315.3 -
2/1/2019 4:00:21 PM 314.3 -
2/1/2019 4:00:22 PM 313.5 -
2/1/2019 4:00:23 PM 312.8 -
2/1/2019 4:00:24 PM 312.4 -
2/1/2019 4:00:25 PM 312.1 -
2/1/2019 4:00:26 PM 311.8 -
2/1/2019 4:00:27 PM 311.6 -
2/1/2019 4:00:28 PM 311.4 -
2/1/2019 4:00:29 PM 311.2 -
2/1/2019 4:00:30 PM 311.0 -
2/1/2019 4:00:31 PM 310.8 -
2/1/2019 4:00:32 PM 310.6 -
2/1/2019 4:00:33 PM 310.4 -
2/1/2019 4:00:34 PM 310.2 -
2/1/2019 4:00:35 PM 310.0 -
Page 8 of 452 August 2019
APPENDIX E3: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-5 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
OLDOF-2 TEST-5 1441
OLDOF-2 TEST-5 1443
OLDOF-2 TEST-5 1444
OLDOF-2 TEST-5 1445
Location EC Reading
(µS/cms)
OLDOF-2 TEST-5 204
OLDOF-2 TEST-5 1,804
OLDOF-2 TEST-5 15,938
OLDOF-2 TEST-5 123,591
q 300,000
K 1.2395
29.2
463.4
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Table E2 OLDOF-2 TEST-5 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
(µS/cms) (°C)
342.3 13.9
343.7 13.9
340.7 13.9
340.8 13.9
Average 341.9 (µS/cms)
Geometric Mean 341.9 (µS/cms)
Average (pre-test) 332.5 (µS/cms)
1,000 20.4
Average (post-test) 313.9 (µS/cms)
Table E3 OLDOF-2 TEST-5 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement
Part 2: Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8,
no. 1, 2004, pp. 11–15.
Slope of Calibration Curve (µS/cms) / (mg/L)
Integral of Conductivity Data Curve SUM:Δt(ECt‐
ECbkg)12,738.3 (s) . (µS/cms)
Calculated Flow Rate Q
L/s
GPM
10,000 20.1
100,000 19.7
Table E4 OLDOF-2 TEST-5 Flow Calculation Summary
Mass of Salt injected mg
(mg/L) (°C)
100 19.3
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 9 of 452 August 2019
APPENDIX E4: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-1 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
5/24/2019 10:22:59 AM 344.2 -
5/24/2019 10:23:00 AM 344.3 -
5/24/2019 10:23:01 AM 344.3 -
5/24/2019 10:23:02 AM 344.3 -
5/24/2019 10:23:03 AM 344.3 -
5/24/2019 10:23:04 AM 344.3 -
5/24/2019 10:23:05 AM 344.3 -
5/24/2019 10:23:06 AM 344.3 -
5/24/2019 10:23:07 AM 344.2 -
5/24/2019 10:23:08 AM 344.2 -
5/24/2019 10:23:09 AM 344.2 -
5/24/2019 10:23:10 AM 344.2 -
5/24/2019 10:23:11 AM 344.2 -
5/24/2019 10:23:12 AM 344.2 -
5/24/2019 10:23:13 AM 344.2 -
5/24/2019 10:23:14 AM 344.2 -
5/24/2019 10:23:15 AM 344.2 -
5/24/2019 10:23:16 AM 344.2 -
5/24/2019 10:23:17 AM 344.2 -
5/24/2019 10:23:18 AM 344.2 -
5/24/2019 10:23:19 AM 344.2 -
5/24/2019 10:23:20 AM 344.2 -
5/24/2019 10:23:21 AM 344.2 -
5/24/2019 10:23:22 AM 344.2 -
5/24/2019 10:23:23 AM 344.9 0.7
5/24/2019 10:23:24 AM 556.7 212.5
5/24/2019 10:23:25 AM 738.4 394.2
5/24/2019 10:23:26 AM 1397.3 1053.1
5/24/2019 10:23:27 AM 1679.4 1335.2
5/24/2019 10:23:28 AM 2151.7 1807.5
5/24/2019 10:23:29 AM 2238.9 1894.7
5/24/2019 10:23:30 AM 2176.3 1832.1
5/24/2019 10:23:31 AM 1947.2 1603.0
5/24/2019 10:23:32 AM 1551.4 1207.2
5/24/2019 10:23:33 AM 1340.2 996.0
5/24/2019 10:23:34 AM 1212.8 868.6
5/24/2019 10:23:35 AM 837.7 493.5
5/24/2019 10:23:36 AM 718.7 374.5
5/24/2019 10:23:37 AM 631 286.8
5/24/2019 10:23:38 AM 475.5 131.3
5/24/2019 10:23:39 AM 454.4 110.2
5/24/2019 10:23:40 AM 417.9 73.7
5/24/2019 10:23:41 AM 397 52.8
5/24/2019 10:23:42 AM 393.4 49.2
5/24/2019 10:23:43 AM 386.3 42.1
5/24/2019 10:23:44 AM 380.8 36.6
5/24/2019 10:23:45 AM 375.9 31.7
5/24/2019 10:23:46 AM 372.3 28.1
5/24/2019 10:23:47 AM 369.9 25.7
5/24/2019 10:23:48 AM 367.5 23.3
5/24/2019 10:23:49 AM 365.9 21.7
5/24/2019 10:23:50 AM 364.2 20.0
5/24/2019 10:23:51 AM 363 18.8
5/24/2019 10:23:52 AM 361.8 17.6
5/24/2019 10:23:53 AM 360.9 16.7
5/24/2019 10:23:54 AM 358.5 14.3
5/24/2019 10:23:55 AM 355.6 11.4
5/24/2019 10:23:56 AM 353.3 9.1
5/24/2019 10:23:57 AM 352.1 7.9
5/24/2019 10:23:58 AM 351.1 6.9
5/24/2019 10:23:59 AM 350.4 6.2
5/24/2019 10:24:00 AM 349.7 5.5
5/24/2019 10:24:01 AM 349.2 5.0
5/24/2019 10:24:02 AM 348.8 4.6
5/24/2019 10:24:03 AM 348.5 4.3
5/24/2019 10:24:04 AM 348.1 3.9
5/24/2019 10:24:05 AM 347.8 3.6
5/24/2019 10:24:06 AM 347.6 3.4
5/24/2019 10:24:07 AM 347.4 3.2
5/24/2019 10:24:08 AM 347.2 3.0
Table E1 OLDOF-2 TEST-1 Data Log
Page 10 of 452 August 2019
APPENDIX E4: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-1 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-2 TEST-1 Data Log
5/24/2019 10:24:09 AM 347 2.8
5/24/2019 10:24:10 AM 346.9 2.7
5/24/2019 10:24:11 AM 346.7 2.5
5/24/2019 10:24:12 AM 346.6 2.4
5/24/2019 10:24:13 AM 346.5 2.3
5/24/2019 10:24:14 AM 346.4 2.2
5/24/2019 10:24:15 AM 346.3 2.1
5/24/2019 10:24:16 AM 346.2 2.0
5/24/2019 10:24:17 AM 346.1 1.9
5/24/2019 10:24:18 AM 346 1.8
5/24/2019 10:24:19 AM 345.9 1.7
5/24/2019 10:24:20 AM 345.9 1.7
5/24/2019 10:24:21 AM 345.8 1.6
5/24/2019 10:24:22 AM 345.8 1.6
5/24/2019 10:24:23 AM 345.7 1.5
5/24/2019 10:24:24 AM 345.6 1.4
5/24/2019 10:24:25 AM 345.6 1.4
5/24/2019 10:24:26 AM 345.5 1.3
5/24/2019 10:24:27 AM 345.5 1.3
5/24/2019 10:24:28 AM 345.5 1.3
5/24/2019 10:24:29 AM 345.4 -
5/24/2019 10:24:30 AM 345.4 -
5/24/2019 10:24:31 AM 345.4 -
5/24/2019 10:24:32 AM 345.3 -
5/24/2019 10:24:33 AM 345.3 -
Page 11 of 452 August 2019
APPENDIX E4: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-1 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
OLDOF-2 TEST-1 1013
OLDOF-2 TEST-1 1014
OLDOF-2 TEST-1 1015
OLDOF-2 TEST-1 1016
OLDOF-2 TEST-1 1016
Location EC Reading
(µS/cms)
OLDOF-2 TEST-1 110
OLDOF-2 TEST-1 185
OLDOF-2 TEST-1 443
OLDOF-2 TEST-1 3,402
OLDOF-2 TEST-1 15,357
OLDOF-2 TEST-1 125,545
q 300,000
K 1.2584
24.9
394.6
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Table E2 OLDOF-2 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
(µS/cms)(°C)
343.8 20.6
344.1 20.6
343.0 20.6
344.2 20.6
344.2 20.6
Average 343.9 (µS/cms)
Geo Mean 343.9 (µS/cms)
Average (pre-test)344.2 (µS/cms)
Average (post-test)345.4 (µS/cms)
1,000 25.7
Table E3 OLDOF-2 TEST-1 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
(mg/L)(°C)
1 25.8
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement Part 2: Constant-Rate
Injection.” Streamline, Watershed Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Slope of Calibration Curve (µS/cms) / (mg/L)
Integral of Conductivity Data Curve SUM:Δt(ECt-
ECbkg)15,187.0 (s) . (µS/cms)
Calculated Flow Rate Q L/s
GPM
10,000 25.8
100,000 26.0
Table E4 OLDOF-2 TEST-1 Flow Calculation Summary
Mass of Salt injected mg
10 25.8
100 25.8
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 12 of 452 August 2019
APPENDIX E5: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-2 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
5/24/2019 10:30:22 AM 344.7 -
5/24/2019 10:30:23 AM 344.7 -
5/24/2019 10:30:24 AM 344.7 -
5/24/2019 10:30:25 AM 344.7 -
5/24/2019 10:30:26 AM 344.7 -
5/24/2019 10:30:27 AM 344.7 -
5/24/2019 10:30:28 AM 344.7 -
5/24/2019 10:30:29 AM 344.7 -
5/24/2019 10:30:30 AM 344.7 -
5/24/2019 10:30:31 AM 344.7 -
5/24/2019 10:30:32 AM 344.7 -
5/24/2019 10:30:33 AM 344.7 -
5/24/2019 10:30:34 AM 344.7 -
5/24/2019 10:30:35 AM 344.7 -
5/24/2019 10:30:36 AM 344.7 -
5/24/2019 10:30:37 AM 344.7 -
5/24/2019 10:30:38 AM 344.7 -
5/24/2019 10:30:39 AM 344.8 -
5/24/2019 10:30:40 AM 344.8 -
5/24/2019 10:30:41 AM 344.8 -
5/24/2019 10:30:42 AM 344.8 -
5/24/2019 10:30:43 AM 345.0 -
5/24/2019 10:30:44 AM 490.5 145.8
5/24/2019 10:30:45 AM 720.9 376.2
5/24/2019 10:30:46 AM 1557.4 1212.7
5/24/2019 10:30:47 AM 2090.1 1745.4
5/24/2019 10:30:48 AM 2642.1 2297.4
5/24/2019 10:30:49 AM 2860.0 2515.3
5/24/2019 10:30:50 AM 2728.0 2383.3
5/24/2019 10:30:51 AM 2400.6 2055.9
5/24/2019 10:30:52 AM 1814.0 1469.3
5/24/2019 10:30:53 AM 1582.0 1237.3
5/24/2019 10:30:54 AM 1316.6 971.9
5/24/2019 10:30:55 AM 894.2 549.5
5/24/2019 10:30:56 AM 706.5 361.8
5/24/2019 10:30:57 AM 638.1 293.4
5/24/2019 10:30:58 AM 499.5 154.8
5/24/2019 10:30:59 AM 487.7 143.0
5/24/2019 10:31:00 AM 417.5 72.8
5/24/2019 10:31:01 AM 391.5 46.8
5/24/2019 10:31:02 AM 375.6 30.9
5/24/2019 10:31:03 AM 371.7 27.0
5/24/2019 10:31:04 AM 367.8 23.1
5/24/2019 10:31:05 AM 365.4 20.7
5/24/2019 10:31:06 AM 363.1 18.4
5/24/2019 10:31:07 AM 361.2 16.5
5/24/2019 10:31:08 AM 360.0 15.3
5/24/2019 10:31:09 AM 358.9 14.2
5/24/2019 10:31:10 AM 358.1 13.4
5/24/2019 10:31:11 AM 357.3 12.6
5/24/2019 10:31:12 AM 356.7 12.0
5/24/2019 10:31:13 AM 356.1 11.4
5/24/2019 10:31:14 AM 355.6 10.9
5/24/2019 10:31:15 AM 355.1 10.4
5/24/2019 10:31:16 AM 354.3 9.6
5/24/2019 10:31:17 AM 352.9 8.2
5/24/2019 10:31:18 AM 352.0 7.3
5/24/2019 10:31:19 AM 351.3 6.6
5/24/2019 10:31:20 AM 350.8 6.1
5/24/2019 10:31:21 AM 350.3 5.6
5/24/2019 10:31:22 AM 349.9 5.2
5/24/2019 10:31:23 AM 349.5 4.8
5/24/2019 10:31:24 AM 349.2 4.5
5/24/2019 10:31:25 AM 348.8 4.1
5/24/2019 10:31:26 AM 348.5 3.8
5/24/2019 10:31:27 AM 348.3 3.6
5/24/2019 10:31:28 AM 348.0 3.3
5/24/2019 10:31:29 AM 347.8 3.1
5/24/2019 10:31:30 AM 347.6 2.9
5/24/2019 10:31:31 AM 347.5 2.8
Table E1 OLDOF-2 TEST-2 Data Log
Page 13 of 452 August 2019
APPENDIX E5: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-2 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-2 TEST-2 Data Log
5/24/2019 10:31:32 AM 347.3 2.6
5/24/2019 10:31:33 AM 347.2 2.5
5/24/2019 10:31:34 AM 347.0 2.3
5/24/2019 10:31:35 AM 346.9 2.2
5/24/2019 10:31:36 AM 346.8 2.1
5/24/2019 10:31:37 AM 346.7 2.0
5/24/2019 10:31:38 AM 346.6 1.9
5/24/2019 10:31:39 AM 346.6 1.9
5/24/2019 10:31:40 AM 346.6 1.9
5/24/2019 10:31:41 AM 346.6 1.9
5/24/2019 10:31:42 AM 346.6 1.9
5/24/2019 10:31:43 AM 346.6 1.9
5/24/2019 10:31:44 AM 346.6 1.9
5/24/2019 10:31:45 AM 346.6 1.9
5/24/2019 10:31:46 AM 346.6 1.9
5/24/2019 10:31:47 AM 346.6 1.9
5/24/2019 10:31:48 AM 346.5 1.8
5/24/2019 10:31:49 AM 346.5 1.8
Page 14 of 452 August 2019
APPENDIX E5: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-2 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
OLDOF-2 TEST-2 1013
OLDOF-2 TEST-2 1014
OLDOF-2 TEST-2 1015
OLDOF-2 TEST-2 1016
OLDOF-2 TEST-2 1016
Location EC Reading
(µS/cms)
OLDOF-2 TEST-2 110
OLDOF-2 TEST-2 185
OLDOF-2 TEST-2 443
OLDOF-2 TEST-2 3,402
OLDOF-2 TEST-2 15,357
OLDOF-2 TEST-2 125,545
q 300,300
K 1.2584
20.6
326.3
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Table E2 OLDOF-2 TEST-2 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
(µS/cms) (°C)
343.8 20.6
344.1 20.6
343.0 20.6
344.2 20.6
344.2 20.6
Average 343.9 (µS/cms)
Geo Mean 343.9 (µS/cms)
Average (pre-test)345.3 (µS/cms)
Average (post-test)346.6 (µS/cms)
1,000 25.7
Table E3 OLDOF-2 TEST-2 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
(mg/L)(°C)
1 25.8
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement Part 2: Constant-Rate
Injection.” Streamline, Watershed Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Slope of Calibration Curve (µS/cms) / (mg/L)
Integral of Conductivity Data Curve SUM:Δt(ECt-
ECbkg)18,385.1 (s) . (µS/cms)
Calculated Flow Rate Q L/s
GPM
10,000 25.8
100,000 26.0
Table E4 OLDOF-2 TEST-2 Flow Calculation Summary
Mass of Salt injected mg
10 25.8
100 25.8
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 15 of 452 August 2019
APPENDIX E6: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-3 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
5/24/2019 10:36:53 AM 345.3 -
5/24/2019 10:36:54 AM 345.3 -
5/24/2019 10:36:55 AM 345.3 -
5/24/2019 10:36:56 AM 345.3 -
5/24/2019 10:36:57 AM 345.3 -
5/24/2019 10:36:58 AM 345.3 -
5/24/2019 10:36:59 AM 345.3 -
5/24/2019 10:37:00 AM 345.3 -
5/24/2019 10:37:01 AM 345.3 -
5/24/2019 10:37:02 AM 345.3 -
5/24/2019 10:37:03 AM 345.3 -
5/24/2019 10:37:04 AM 345.3 -
5/24/2019 10:37:05 AM 345.3 -
5/24/2019 10:37:06 AM 345.3 -
5/24/2019 10:37:07 AM 345.3 -
5/24/2019 10:37:08 AM 345.3 -
5/24/2019 10:37:09 AM 345.3 -
5/24/2019 10:37:10 AM 345.3 -
5/24/2019 10:37:11 AM 345.3 -
5/24/2019 10:37:12 AM 345.3 -
5/24/2019 10:37:13 AM 345.3 -
5/24/2019 10:37:14 AM 345.3 -
5/24/2019 10:37:15 AM 345.3 -
5/24/2019 10:37:16 AM 345.3 -
5/24/2019 10:37:17 AM 346.3 1.0
5/24/2019 10:37:18 AM 502.6 157.3
5/24/2019 10:37:19 AM 724.2 378.9
5/24/2019 10:37:20 AM 1586.5 1241.2
5/24/2019 10:37:21 AM 1941.2 1595.9
5/24/2019 10:37:22 AM 2747.3 2402.0
5/24/2019 10:37:23 AM 2873.0 2527.7
5/24/2019 10:37:24 AM 2774.2 2428.9
5/24/2019 10:37:25 AM 2505.0 2159.7
5/24/2019 10:37:26 AM 2128.0 1782.7
5/24/2019 10:37:27 AM 1689.4 1344.1
5/24/2019 10:37:28 AM 1373.3 1028.0
5/24/2019 10:37:29 AM 985.9 640.6
5/24/2019 10:37:30 AM 754.5 409.2
5/24/2019 10:37:31 AM 646.6 301.3
5/24/2019 10:37:32 AM 481.5 136.2
5/24/2019 10:37:33 AM 445.7 100.4
5/24/2019 10:37:34 AM 412.9 67.6
5/24/2019 10:37:35 AM 389.9 44.6
5/24/2019 10:37:36 AM 383.0 37.7
5/24/2019 10:37:37 AM 376.8 31.5
5/24/2019 10:37:38 AM 371.7 26.4
5/24/2019 10:37:39 AM 368.0 22.7
5/24/2019 10:37:40 AM 365.5 20.2
5/24/2019 10:37:41 AM 363.4 18.1
5/24/2019 10:37:42 AM 361.9 16.6
5/24/2019 10:37:43 AM 360.5 15.2
5/24/2019 10:37:44 AM 359.5 14.2
5/24/2019 10:37:45 AM 358.5 13.2
5/24/2019 10:37:46 AM 357.7 12.4
5/24/2019 10:37:47 AM 357.0 11.7
5/24/2019 10:37:48 AM 355.7 10.4
5/24/2019 10:37:49 AM 353.2 7.9
5/24/2019 10:37:50 AM 351.8 6.5
5/24/2019 10:37:51 AM 350.8 5.5
5/24/2019 10:37:52 AM 350.1 4.8
5/24/2019 10:37:53 AM 349.6 4.3
5/24/2019 10:37:54 AM 349.2 3.9
5/24/2019 10:37:55 AM 348.8 3.5
5/24/2019 10:37:56 AM 348.5 3.2
5/24/2019 10:37:57 AM 348.3 3.0
5/24/2019 10:37:58 AM 348.1 2.8
5/24/2019 10:37:59 AM 347.8 2.5
5/24/2019 10:38:00 AM 347.6 2.3
5/24/2019 10:38:01 AM 347.5 2.2
5/24/2019 10:38:02 AM 347.3 2.0
Table E1 OLDOF-2 TEST-3 Data Log
Page 16 of 452 August 2019
APPENDIX E6: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-3 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-2 TEST-3 Data Log
5/24/2019 10:38:03 AM 347.2 1.9
5/24/2019 10:38:04 AM 347.1 1.8
5/24/2019 10:38:05 AM 347.0 1.7
5/24/2019 10:38:06 AM 346.9 1.6
5/24/2019 10:38:07 AM 346.9 1.6
5/24/2019 10:38:08 AM 346.8 1.5
5/24/2019 10:38:09 AM 346.7 1.4
5/24/2019 10:38:10 AM 346.7 1.4
5/24/2019 10:38:11 AM 346.6 1.3
5/24/2019 10:38:12 AM 346.5 1.2
5/24/2019 10:38:13 AM 346.5 1.2
Page 17 of 452 August 2019
APPENDIX E6: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-3 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
OLDOF-2 TEST-3 1013
OLDOF-2 TEST-3 1014
OLDOF-2 TEST-3 1015
OLDOF-2 TEST-3 1016
OLDOF-2 TEST-3 1016
Location EC Reading
(µS/cms)
OLDOF-2 TEST-3 110
OLDOF-2 TEST-3 185
OLDOF-2 TEST-3 443
OLDOF-2 TEST-3 3,402
OLDOF-2 TEST-3 15,357
OLDOF-2 TEST-3 125,545
q 300,600
K 1.2584
19.8
314.9
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Table E2 OLDOF-2 TEST-3 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
(µS/cms) (°C)
343.8 20.6
344.1 20.6
343.0 20.6
344.2 20.6
344.2 20.6
Average 343.9 (µS/cms)
Geo Mean 343.9 (µS/cms)
25.8
Average (pre-test) 344.2 (µS/cms)
Average (post-test) 345.4 (µS/cms)
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement Part 2: Constant-Rate
Injection.” Streamline, Watershed Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Slope of Calibration Curve (µS/cms) / (mg/L)
Integral of Conductivity Data Curve SUM:Δt(ECt-
ECbkg)19,068.6 (s) . (µS/cms)
10,000 25.8
100,000 26.0
Table E4 OLDOF-2 TEST-3 Flow Calculation Summary
Mass of Salt injected mg
10
Calculated Flow Rate Q L/s
GPM
25.8
100 25.8
1,000 25.7
Table E3 OLDOF-2 TEST-3 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
(mg/L)(°C)
1
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 18 of 452 August 2019
APPENDIX E7: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
5/24/2019 10:43:39 AM 345.8 -
5/24/2019 10:43:40 AM 345.8 -
5/24/2019 10:43:41 AM 345.8 -
5/24/2019 10:43:42 AM 345.8 -
5/24/2019 10:43:43 AM 345.8 -
5/24/2019 10:43:44 AM 345.8 -
5/24/2019 10:43:45 AM 345.8 -
5/24/2019 10:43:46 AM 345.7 -
5/24/2019 10:43:47 AM 345.7 -
5/24/2019 10:43:48 AM 345.7 -
5/24/2019 10:43:49 AM 345.7 -
5/24/2019 10:43:50 AM 345.7 -
5/24/2019 10:43:51 AM 345.7 -
5/24/2019 10:43:52 AM 345.7 -
5/24/2019 10:43:53 AM 345.7 -
5/24/2019 10:43:54 AM 345.6 -
5/24/2019 10:43:55 AM 345.6 -
5/24/2019 10:43:56 AM 345.6 -
5/24/2019 10:43:57 AM 345.6 -
5/24/2019 10:43:58 AM 345.6 -
5/24/2019 10:43:59 AM 345.6 -
5/24/2019 10:44:00 AM 345.6 -
5/24/2019 10:44:01 AM 346.0 0.3
5/24/2019 10:44:02 AM 503.7 158.0
5/24/2019 10:44:03 AM 725.2 379.5
5/24/2019 10:44:04 AM 1537.4 1191.7
5/24/2019 10:44:05 AM 1707.3 1361.6
5/24/2019 10:44:06 AM 2279.0 1933.3
5/24/2019 10:44:07 AM 2461.3 2115.6
5/24/2019 10:44:08 AM 2361.2 2015.5
5/24/2019 10:44:09 AM 2161.2 1815.5
5/24/2019 10:44:10 AM 1860.8 1515.1
5/24/2019 10:44:11 AM 1498.4 1152.7
5/24/2019 10:44:12 AM 1268.8 923.1
5/24/2019 10:44:13 AM 889.7 544.0
5/24/2019 10:44:14 AM 771.3 425.6
5/24/2019 10:44:15 AM 639.5 293.8
5/24/2019 10:44:16 AM 412.4 66.7
5/24/2019 10:44:17 AM 482.8 137.1
5/24/2019 10:44:18 AM 467.5 121.8
5/24/2019 10:44:19 AM 404.4 58.7
5/24/2019 10:44:20 AM 384.8 39.1
5/24/2019 10:44:21 AM 375.1 29.4
5/24/2019 10:44:22 AM 370.8 25.1
5/24/2019 10:44:23 AM 367.5 21.8
5/24/2019 10:44:24 AM 364.6 18.9
5/24/2019 10:44:25 AM 362.7 17.0
5/24/2019 10:44:26 AM 361.3 15.6
5/24/2019 10:44:27 AM 359.9 14.2
5/24/2019 10:44:28 AM 358.8 13.1
5/24/2019 10:44:29 AM 357.9 12.2
5/24/2019 10:44:30 AM 357.1 11.4
5/24/2019 10:44:31 AM 356.5 10.8
5/24/2019 10:44:32 AM 355.9 10.2
5/24/2019 10:44:33 AM 355.4 9.7
5/24/2019 10:44:34 AM 354.9 9.2
5/24/2019 10:44:35 AM 354.6 8.9
5/24/2019 10:44:36 AM 353.3 7.6
5/24/2019 10:44:37 AM 352.4 6.7
5/24/2019 10:44:38 AM 351.6 5.9
5/24/2019 10:44:39 AM 351.0 5.3
5/24/2019 10:44:40 AM 350.5 4.8
5/24/2019 10:44:41 AM 350.1 4.4
5/24/2019 10:44:42 AM 349.7 4.0
5/24/2019 10:44:43 AM 349.5 3.8
5/24/2019 10:44:44 AM 349.2 3.5
5/24/2019 10:44:45 AM 349.0 3.3
5/24/2019 10:44:46 AM 348.7 3.0
5/24/2019 10:44:47 AM 348.5 2.8
5/24/2019 10:44:48 AM 348.4 2.7
Table E1 OLDOF-2 TEST-4 Data Log
Page 19 of 452 August 2019
APPENDIX E7: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-2 TEST-4 Data Log
5/24/2019 10:44:49 AM 348.2 2.5
5/24/2019 10:44:50 AM 348.0 2.3
5/24/2019 10:44:51 AM 347.9 2.2
5/24/2019 10:44:52 AM 347.8 2.1
5/24/2019 10:44:53 AM 347.7 2.0
5/24/2019 10:44:54 AM 347.6 1.9
5/24/2019 10:44:55 AM 347.5 1.8
5/24/2019 10:44:56 AM 347.4 1.7
5/24/2019 10:44:57 AM 347.3 1.6
5/24/2019 10:44:58 AM 347.2 1.5
5/24/2019 10:44:59 AM 347.2 1.5
5/24/2019 10:45:00 AM 347.1 1.4
5/24/2019 10:45:01 AM 347.0 1.3
5/24/2019 10:45:02 AM 347.0 1.3
5/24/2019 10:45:03 AM 347.0 1.3
5/24/2019 10:45:04 AM 346.9 1.2
5/24/2019 10:45:05 AM 346.9 1.2
5/24/2019 10:45:06 AM 346.8 1.1
5/24/2019 10:45:07 AM 346.8 1.1
5/24/2019 10:45:08 AM 346.8 1.1
5/24/2019 10:45:09 AM 346.7 1.0
5/24/2019 10:45:10 AM 346.7 1.0
5/24/2019 10:45:11 AM 346.7 1.0
5/24/2019 10:45:12 AM 346.6 0.9
5/24/2019 10:45:13 AM 346.6 0.9
5/24/2019 10:45:14 AM 346.6 0.9
5/24/2019 10:45:15 AM 346.6 0.9
5/24/2019 10:45:16 AM 346.5 0.8
5/24/2019 10:45:17 AM 346.5 0.8
5/24/2019 10:45:18 AM 346.5 0.8
5/24/2019 10:45:19 AM 346.4 0.7
5/24/2019 10:45:20 AM 346.4 0.7
5/24/2019 10:45:21 AM 346.4 0.7
5/24/2019 10:45:22 AM 346.3 0.6
5/24/2019 10:45:23 AM 346.3 0.6
5/24/2019 10:45:24 AM 346.3 0.6
5/24/2019 10:45:25 AM 346.3 0.6
5/24/2019 10:45:26 AM 346.3 0.6
5/24/2019 10:45:27 AM 346.3 0.6
5/24/2019 10:45:28 AM 346.2 0.5
5/24/2019 10:45:29 AM 346.2 0.5
5/24/2019 10:45:30 AM 346.2 0.5
5/24/2019 10:45:31 AM 346.2 0.5
5/24/2019 10:45:32 AM 346.2 0.5
5/24/2019 10:45:33 AM 346.2 0.5
5/24/2019 10:45:34 AM 346.2 0.5
Page 20 of 452 August 2019
APPENDIX E7: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
OLDOF-2 TEST-4 1013
OLDOF-2 TEST-4 1014
OLDOF-2 TEST-4 1015
OLDOF-2 TEST-4 1016
OLDOF-2 TEST-4 1016
Location EC Reading
(µS/cms)
OLDOF-2 TEST-4 110
OLDOF-2 TEST-4 185
OLDOF-2 TEST-4 443
OLDOF-2 TEST-4 3,402
OLDOF-2 TEST-4 15,357
OLDOF-2 TEST-4 125,545
q 300,200
K 1.2584
22.8
361.6
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Table E2 OLDOF-2 TEST-4 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
(µS/cms) (°C)
343.8 20.6
344.1 20.6
343.0 20.6
344.2 20.6
344.2 20.6
Average 343.9 (µS/cms)
Geo Mean 343.9 (µS/cms)
Average (pre-test)345.7 (µS/cms)
Average (post-test)346.2 (µS/cms)
1,000 25.7
Table E3 OLDOF-2 TEST-4 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
(mg/L)(°C)
1 25.8
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement Part 2:
Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8, no. 1, 2004, pp.
11–15.
Slope of Calibration Curve (µS/cms) / (mg/L)
Integral of Conductivity Data
Curve
SUM:Δt(ECt‐
ECbkg)16,584.3 (s) . (µS/cms)
Calculated Flow Rate Q
L/s
GPM
10,000 25.8
100,000 26.0
Table E4 OLDOF-2 TEST-4 Flow Calculation Summary
Mass of Salt injected mg
10 25.8
100 25.8
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 21 of 452 August 2019
APPENDIX E8: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-5 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
5/24/2019 10:48:44 AM 346.0 -
5/24/2019 10:48:45 AM 345.9 -
5/24/2019 10:48:46 AM 345.9 -
5/24/2019 10:48:47 AM 345.9 -
5/24/2019 10:48:48 AM 345.9 -
5/24/2019 10:48:49 AM 345.9 -
5/24/2019 10:48:50 AM 345.9 -
5/24/2019 10:48:51 AM 345.8 -
5/24/2019 10:48:52 AM 345.8 -
5/24/2019 10:48:53 AM 345.8 -
5/24/2019 10:48:54 AM 345.8 -
5/24/2019 10:48:55 AM 345.8 -
5/24/2019 10:48:56 AM 345.8 -
5/24/2019 10:48:57 AM 345.8 -
5/24/2019 10:48:58 AM 345.8 -
5/24/2019 10:48:59 AM 345.7 -
5/24/2019 10:49:00 AM 345.7 -
5/24/2019 10:49:01 AM 345.7 -
5/24/2019 10:49:02 AM 345.7 -
5/24/2019 10:49:03 AM 345.7 -
5/24/2019 10:49:04 AM 345.7 -
5/24/2019 10:49:05 AM 346.3 -
5/24/2019 10:49:06 AM 470.0 124.2
5/24/2019 10:49:07 AM 723.1 377.3
5/24/2019 10:49:08 AM 1276.6 930.8
5/24/2019 10:49:09 AM 1587.8 1242.0
5/24/2019 10:49:10 AM 2389.2 2043.4
5/24/2019 10:49:11 AM 2407.9 2062.1
5/24/2019 10:49:12 AM 2398.0 2052.2
5/24/2019 10:49:13 AM 2377.3 2031.5
5/24/2019 10:49:14 AM 1970.3 1624.5
5/24/2019 10:49:15 AM 1680.1 1334.3
5/24/2019 10:49:16 AM 1333.4 987.6
5/24/2019 10:49:17 AM 1051.4 705.6
5/24/2019 10:49:18 AM 896.8 551.0
5/24/2019 10:49:19 AM 678.6 332.8
5/24/2019 10:49:20 AM 618.1 272.3
5/24/2019 10:49:21 AM 460.2 114.4
5/24/2019 10:49:22 AM 466.7 120.9
5/24/2019 10:49:23 AM 450.0 104.2
5/24/2019 10:49:24 AM 436.1 90.3
5/24/2019 10:49:25 AM 382.9 37.1
5/24/2019 10:49:26 AM 372.9 27.1
5/24/2019 10:49:27 AM 367.2 21.4
5/24/2019 10:49:28 AM 365.5 19.7
5/24/2019 10:49:29 AM 363.5 17.7
5/24/2019 10:49:30 AM 361.9 16.1
5/24/2019 10:49:31 AM 360.4 14.6
5/24/2019 10:49:32 AM 359.3 13.5
5/24/2019 10:49:33 AM 358.6 12.8
5/24/2019 10:49:34 AM 357.8 12.0
5/24/2019 10:49:35 AM 357.2 11.4
5/24/2019 10:49:36 AM 356.6 10.8
5/24/2019 10:49:37 AM 356.0 10.2
5/24/2019 10:49:38 AM 355.6 9.8
5/24/2019 10:49:39 AM 355.2 9.4
5/24/2019 10:49:40 AM 354.7 8.9
5/24/2019 10:49:41 AM 354.1 8.3
5/24/2019 10:49:42 AM 353.1 7.3
5/24/2019 10:49:43 AM 352.4 6.6
5/24/2019 10:49:44 AM 351.8 6.0
5/24/2019 10:49:45 AM 351.3 5.5
5/24/2019 10:49:46 AM 350.8 5.0
5/24/2019 10:49:47 AM 350.5 4.7
5/24/2019 10:49:48 AM 350.1 4.3
5/24/2019 10:49:49 AM 349.8 4.0
5/24/2019 10:49:50 AM 349.5 3.7
5/24/2019 10:49:51 AM 349.3 3.5
5/24/2019 10:49:52 AM 349.1 3.3
5/24/2019 10:49:53 AM 348.9 3.1
Table E1 OLDOF-2 TEST-5 Data Log
Page 22 of 452 August 2019
APPENDIX E8: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-5 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-2 TEST-5 Data Log
5/24/2019 10:49:54 AM 348.8 3.0
5/24/2019 10:49:55 AM 348.6 2.8
5/24/2019 10:49:56 AM 348.5 2.7
5/24/2019 10:49:57 AM 348.3 2.5
5/24/2019 10:49:58 AM 348.2 2.4
5/24/2019 10:49:59 AM 348.0 2.2
5/24/2019 10:50:00 AM 348.0 2.2
5/24/2019 10:50:01 AM 347.8 2.0
5/24/2019 10:50:02 AM 347.7 1.9
5/24/2019 10:50:03 AM 347.6 1.8
5/24/2019 10:50:04 AM 347.5 1.7
5/24/2019 10:50:05 AM 347.4 1.6
5/24/2019 10:50:06 AM 347.3 1.5
5/24/2019 10:50:07 AM 347.3 1.5
5/24/2019 10:50:08 AM 347.2 1.4
5/24/2019 10:50:09 AM 347.1 1.3
5/24/2019 10:50:10 AM 347.1 1.3
5/24/2019 10:50:11 AM 347.0 1.2
5/24/2019 10:50:12 AM 347.0 1.2
5/24/2019 10:50:13 AM 347.0 1.2
5/24/2019 10:50:14 AM 346.9 1.1
5/24/2019 10:50:15 AM 346.9 1.1
5/24/2019 10:50:16 AM 346.8 1.0
5/24/2019 10:50:17 AM 346.8 1.0
Page 23 of 452 August 2019
APPENDIX E8: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-5 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
OLDOF-2 TEST-5 1013
OLDOF-2 TEST-5 1014
OLDOF-2 TEST-5 1015
OLDOF-2 TEST-5 1016
OLDOF-2 TEST-5 1016
Location EC Reading
(µS/cms)
OLDOF-2 TEST-5 110
OLDOF-2 TEST-5 185
OLDOF-2 TEST-5 443
OLDOF-2 TEST-5 3,402
OLDOF-2 TEST-5 15,357
OLDOF-2 TEST-5 125,545
q 300,300
K 1.2584
21.7
343.6
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Table E2 OLDOF-2 TEST-5 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
(µS/cms) (°C)
343.8 20.6
344.1 20.6
343.0 20.6
344.2 20.6
344.2 20.6
Average 343.9 (µS/cms)
Geo Mean 343.9 (µS/cms)
Average (pre-test) 345.8 (µS/cms)
Average (post-test) 346.9 (µS/cms)
1,000 25.7
Table E3 OLDOF-2 TEST-5 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
(mg/L) (°C)
1 25.8
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement Part 2: Constant-Rate
Injection.” Streamline, Watershed Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Slope of Calibration Curve (µS/cms) / (mg/L)
Integral of Conductivity Data Curve SUM:Δt(ECt-
ECbkg)17,458.5 (s) . (µS/cms)
Calculated Flow Rate Q L/s
GPM
10,000 25.8
100,000 26.0
Table E4 OLDOF-2 TEST-5 Flow Calculation Summary
Mass of Salt injected mg
10 25.8
100 25.8
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 24 of 452 August 2019
APPENDIX E9: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-1 June
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 10:52:08 AM 339.2 -
6/7/2019 10:52:09 AM 339.2 -
6/7/2019 10:52:10 AM 339.1 -
6/7/2019 10:52:11 AM 339.1 -
6/7/2019 10:52:12 AM 501.3 162.1
6/7/2019 10:52:13 AM 1537.1 1198.0
6/7/2019 10:52:14 AM 1883.7 1544.5
6/7/2019 10:52:15 AM 1892.0 1552.9
6/7/2019 10:52:16 AM 1879.9 1540.7
6/7/2019 10:52:17 AM 1521.7 1182.6
6/7/2019 10:52:18 AM 1352.5 1013.3
6/7/2019 10:52:19 AM 1228.6 889.5
6/7/2019 10:52:20 AM 984.7 645.5
6/7/2019 10:52:21 AM 803.8 464.7
6/7/2019 10:52:22 AM 681.4 342.2
6/7/2019 10:52:23 AM 634.8 295.7
6/7/2019 10:52:24 AM 629.9 290.7
6/7/2019 10:52:25 AM 629.9 290.8
6/7/2019 10:52:26 AM 477.8 138.6
6/7/2019 10:52:27 AM 477.8 138.7
6/7/2019 10:52:28 AM 420.5 81.3
6/7/2019 10:52:29 AM 386.5 47.4
6/7/2019 10:52:30 AM 376.4 37.2
6/7/2019 10:52:31 AM 370.1 30.9
6/7/2019 10:52:32 AM 366.0 26.9
6/7/2019 10:52:33 AM 362.8 23.6
6/7/2019 10:52:34 AM 360.8 21.7
6/7/2019 10:52:35 AM 358.8 19.6
6/7/2019 10:52:36 AM 357.3 18.2
6/7/2019 10:52:37 AM 355.9 16.7
6/7/2019 10:52:38 AM 354.9 15.8
6/7/2019 10:52:39 AM 354.1 14.9
6/7/2019 10:52:40 AM 354.1 15.0
6/7/2019 10:52:41 AM 382.8 43.6
6/7/2019 10:52:42 AM 382.8 43.7
6/7/2019 10:52:43 AM 368.1 28.9
6/7/2019 10:52:44 AM 342.9 3.8
6/7/2019 10:52:45 AM 342.9 3.7
6/7/2019 10:52:46 AM 342.7 3.6
6/7/2019 10:52:47 AM 342.6 3.4
Table E1 OLDOF-2 TEST-1 Data Log
Page 25 of 452 August 2019
APPENDIX E9: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-1 June
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
OLDOF-2 TEST-1 1038
OLDOF-2 TEST-1 1039
OLDOF-2 TEST-1 1039
OLDOF-2 TEST-1 1040
Location EC Reading
(µS/cms)
OLDOF-2 TEST-1 246
OLDOF-2 TEST-1 2,167
OLDOF-2 TEST-1 17,538
OLDOF-2 TEST-1 136,514
q 299,500
K 1.3691
33.6
533.9
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Table E2 OLDOF-2 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
(µS/cms) (°C)
342.5 20.5
342.0 20.5
341.9 20.5
341.1 20.5
Average 341.9 (µS/cms)
Geo Mean 341.9 (µS/cms)
Average (pre-test) 339.2 (µS/cms)
Average (post-test) 356.9 (µS/cms)
Table E3 OLDOF-2 TEST-1 YSI Salt Dilution Calibration Data
Calibration
Concentration Temperature
25.2
Table E4 OLDOF-2 TEST-1 Flow Calculation Summary
Mass of Salt injected mg
(mg/L) (°C)
100 25.2
1,000 25.2
Calculated Flow Rate Q
L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement Part 2:
Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8, no. 1, 2004, pp.
11–15.
Slope of Calibration Curve (µS/cms) / (mg/L)
Integral of Conductivity
Data Curve
SUM:Δt(ECt-
ECbkg)12,190.5 (s) . (µS/cms)
10,000 25.2
100,000
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 26 of 452 August 2019
APPENDIX E10: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-2 June
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 11:26:38 AM 375.5 -
6/7/2019 11:26:39 AM 371.1 -
6/7/2019 11:26:40 AM 367.5 -
6/7/2019 11:26:41 AM 365.1 -
6/7/2019 11:26:42 AM 363.1 -
6/7/2019 11:26:43 AM 361.6 -
6/7/2019 11:26:44 AM 360.0 -
6/7/2019 11:26:45 AM 358.9 -
6/7/2019 11:26:46 AM 357.8 -
6/7/2019 11:26:47 AM 353.3 -
6/7/2019 11:26:48 AM 350.4 -
6/7/2019 11:26:49 AM 348.3 -
6/7/2019 11:26:50 AM 346.9 -
6/7/2019 11:26:51 AM 346.4 -
6/7/2019 11:26:52 AM 346.2 -
6/7/2019 11:26:53 AM 345.9 -
6/7/2019 11:26:54 AM 345.6 -
6/7/2019 11:26:55 AM 345.5 -
6/7/2019 11:26:56 AM 345.3 -
6/7/2019 11:26:57 AM 345.2 -
6/7/2019 11:26:58 AM 345.1 -
6/7/2019 11:26:59 AM 345.0 -
6/7/2019 11:27:00 AM 344.9 -
6/7/2019 11:27:01 AM 344.8 -
6/7/2019 11:27:02 AM 344.7 -
6/7/2019 11:27:03 AM 344.7 -
6/7/2019 11:27:04 AM 344.6 -
6/7/2019 11:27:05 AM 344.5 -
6/7/2019 11:27:06 AM 344.7 -
6/7/2019 11:27:07 AM 398.4 51.2
6/7/2019 11:27:08 AM 537.2 190.0
6/7/2019 11:27:09 AM 741.4 394.2
6/7/2019 11:27:10 AM 1234.7 887.5
6/7/2019 11:27:11 AM 1452.5 1105.3
6/7/2019 11:27:12 AM 1874.9 1527.7
6/7/2019 11:27:13 AM 1941.3 1594.1
6/7/2019 11:27:14 AM 1923.7 1576.5
6/7/2019 11:27:15 AM 1695.4 1348.2
6/7/2019 11:27:16 AM 1593.1 1245.9
6/7/2019 11:27:17 AM 1308.1 960.9
6/7/2019 11:27:18 AM 1105.0 757.8
6/7/2019 11:27:19 AM 857.4 510.2
6/7/2019 11:27:20 AM 757.6 410.4
6/7/2019 11:27:21 AM 604.9 257.7
6/7/2019 11:27:22 AM 508.1 160.9
6/7/2019 11:27:23 AM 525.5 178.3
6/7/2019 11:27:24 AM 467.9 120.7
6/7/2019 11:27:25 AM 418.1 70.9
6/7/2019 11:27:26 AM 399.9 52.7
6/7/2019 11:27:27 AM 382.4 35.2
6/7/2019 11:27:28 AM 379.9 32.7
6/7/2019 11:27:29 AM 373.2 26.0
6/7/2019 11:27:30 AM 369.0 21.8
6/7/2019 11:27:31 AM 365.8 18.6
6/7/2019 11:27:32 AM 363.7 16.5
6/7/2019 11:27:33 AM 361.7 14.5
6/7/2019 11:27:34 AM 360.2 13.0
6/7/2019 11:27:35 AM 358.9 11.7
6/7/2019 11:27:36 AM 358.2 11.0
6/7/2019 11:27:37 AM 357.1 9.9
6/7/2019 11:27:38 AM 356.4 9.2
6/7/2019 11:27:39 AM 355.6 8.4
6/7/2019 11:27:40 AM 354.8 7.6
6/7/2019 11:27:41 AM 352.8 5.6
6/7/2019 11:27:42 AM 351.3 4.1
6/7/2019 11:27:43 AM 350.4 3.2
6/7/2019 11:27:44 AM 349.4 2.2
6/7/2019 11:27:45 AM 348.7 1.5
6/7/2019 11:27:46 AM 348.1 0.9
6/7/2019 11:27:47 AM 347.6 0.4
Table E1 OLDOF-2 TEST-2 Data Log
Page 27 of 452 August 2019
APPENDIX E10: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-2 June
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-2 TEST-2 Data Log
6/7/2019 11:27:48 AM 347.3 0.1
6/7/2019 11:27:49 AM 346.9 -0.31
6/7/2019 11:27:50 AM 346.7 -0.51
6/7/2019 11:27:51 AM 346.5 -0.71
6/7/2019 11:27:52 AM 346.3 -0.91
6/7/2019 11:27:53 AM 346.1 -1.11
6/7/2019 11:27:54 AM 345.9 -1.31
6/7/2019 11:27:55 AM 345.8 -1.41
6/7/2019 11:27:56 AM 345.6 -1.61
6/7/2019 11:27:57 AM 345.5 -1.71
6/7/2019 11:27:58 AM 345.4 -1.81
6/7/2019 11:27:59 AM 345.3 -1.91
6/7/2019 11:28:00 AM 345.1 -2.11
6/7/2019 11:28:01 AM 345.1 -2.11
6/7/2019 11:28:02 AM 345.0 -2.21
6/7/2019 11:28:03 AM 344.9 -2.31
6/7/2019 11:28:04 AM 344.8 -2.41
6/7/2019 11:28:05 AM 344.7 -2.51
6/7/2019 11:28:06 AM 344.7 -2.51
6/7/2019 11:28:07 AM 344.6 -2.61
6/7/2019 11:28:08 AM 344.5 -2.71
6/7/2019 11:28:09 AM 344.4 -2.81
6/7/2019 11:28:10 AM 344.4 -2.81
6/7/2019 11:28:11 AM 344.3 -2.91
6/7/2019 11:28:12 AM 344.2 -3.01
6/7/2019 11:28:13 AM 344.2 -3.01
6/7/2019 11:28:14 AM 344.1 -3.11
6/7/2019 11:28:15 AM 344.1 -3.11
6/7/2019 11:28:16 AM 344.0 -3.21
6/7/2019 11:28:17 AM 344.0 -3.21
6/7/2019 11:28:18 AM 343.9 -3.3
6/7/2019 11:28:19 AM 343.9 -3.3
6/7/2019 11:28:20 AM 343.8 -3.4
6/7/2019 11:28:21 AM 343.8 -3.4
6/7/2019 11:28:22 AM 343.7 -3.5
6/7/2019 11:28:23 AM 343.7 -3.5
6/7/2019 11:28:24 AM 343.7 -3.5
6/7/2019 11:28:25 AM 343.6 -3.6
6/7/2019 11:28:26 AM 343.6 -3.6
6/7/2019 11:28:27 AM 343.5 -3.7
6/7/2019 11:28:28 AM 343.5 -3.7
6/7/2019 11:28:29 AM 343.4 -3.8
6/7/2019 11:28:30 AM 343.4 -3.8
6/7/2019 11:28:31 AM 343.3 -3.9
6/7/2019 11:28:32 AM 343.3 -3.9
6/7/2019 11:28:33 AM 343.2 -4.0
6/7/2019 11:28:34 AM 343.2 -4.0
6/7/2019 11:28:35 AM 343.1 -4.1
6/7/2019 11:28:36 AM 343.1 -4.1
Page 28 of 452 August 2019
APPENDIX E10: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-2 June
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
OLDOF-2 TEST-2 1038
OLDOF-2 TEST-2 1039
OLDOF-2 TEST-2 1039
OLDOF-2 TEST-2 1040
Location EC Reading
(µS/cms)
OLDOF-2 TEST-2 246
OLDOF-2 TEST-2 2,167
OLDOF-2 TEST-2 17,538
OLDOF-2 TEST-2 136,514
q 299,600
K 1.3691
30.3
481.5
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Location Time Background Stream EC
Background Stream
Temperature
(µS/cms)(°C)
342.5 20.5
342.0 20.5
341.9 20.5
341.1 20.5
Average 341.9 (µS/cms)
Geo Mean 341.9 (µS/cms)
Average (pre-test)347.2 (µS/cms)
100 25.2
1,000 25.2
Average (post-test)346.3 (µS/cms)
Calibration Concentration Temperature
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement Part 2: Constant-Rate
Injection.” Streamline, Watershed Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Slope of Calibration Curve (µS/cms) / (mg/L)
Integral of Conductivity Data Curve SUM:Δt(ECt-
ECbkg)13,522.2 (s) . (µS/cms)
Table E2 OLDOF-2 TEST-2 Stream Background Conductivity Data
Table E3 OLDOF-2 TEST-2 YSI Salt Dilution Calibration Data
Table E4 OLDOF-2 TEST-2 Flow Calculation Summary
Calculated Flow Rate Q L/s
GPM
10,000 25.2
100,000 25.2
Mass of Salt injected mg
(mg/L)(°C)
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 29 of 452 August 2019
APPENDIX E11: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-4 June
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 11:37:18 AM 375.0 -
6/7/2019 11:37:19 AM 372.1 -
6/7/2019 11:37:20 AM 370.0 -
6/7/2019 11:37:21 AM 368.1 -
6/7/2019 11:37:22 AM 366.7 -
6/7/2019 11:37:23 AM 365.2 -
6/7/2019 11:37:24 AM 363.8 -
6/7/2019 11:37:25 AM 362.3 -
6/7/2019 11:37:26 AM 357.4 -
6/7/2019 11:37:27 AM 354.8 -
6/7/2019 11:37:28 AM 353.7 -
6/7/2019 11:37:29 AM 351.7 -
6/7/2019 11:37:30 AM 350.7 -
6/7/2019 11:37:31 AM 349.8 -
6/7/2019 11:37:32 AM 349.1 -
6/7/2019 11:37:33 AM 348.3 -
6/7/2019 11:37:34 AM 347.7 -
6/7/2019 11:37:35 AM 347.1 -
6/7/2019 11:37:36 AM 346.6 -
6/7/2019 11:37:37 AM 346.2 -
6/7/2019 11:37:38 AM 345.8 -
6/7/2019 11:37:39 AM 345.6 -
6/7/2019 11:37:40 AM 346.2 -
6/7/2019 11:37:41 AM 514.9 165.5
6/7/2019 11:37:42 AM 709.1 359.7
6/7/2019 11:37:43 AM 1388.4 1039.0
6/7/2019 11:37:44 AM 1861.3 1511.9
6/7/2019 11:37:45 AM 2220.0 1870.6
6/7/2019 11:37:46 AM 2512.3 2162.9
6/7/2019 11:37:47 AM 2560.0 2210.6
6/7/2019 11:37:48 AM 2512.2 2162.8
6/7/2019 11:37:49 AM 2194.6 1845.2
6/7/2019 11:37:50 AM 1763.4 1414.0
6/7/2019 11:37:51 AM 1546.6 1197.2
6/7/2019 11:37:52 AM 1094.5 745.1
6/7/2019 11:37:53 AM 891.8 542.4
6/7/2019 11:37:54 AM 756.0 406.6
6/7/2019 11:37:55 AM 674.6 325.2
6/7/2019 11:37:56 AM 471.8 122.4
6/7/2019 11:37:57 AM 479.9 130.5
6/7/2019 11:37:58 AM 436.6 87.2
6/7/2019 11:37:59 AM 419.2 69.8
6/7/2019 11:38:00 AM 407.8 58.4
6/7/2019 11:38:01 AM 399.1 49.7
6/7/2019 11:38:02 AM 390.5 41.1
6/7/2019 11:38:03 AM 384.9 35.5
6/7/2019 11:38:04 AM 380.0 30.6
6/7/2019 11:38:05 AM 376.6 27.2
6/7/2019 11:38:06 AM 373.5 24.1
6/7/2019 11:38:07 AM 371.2 21.8
6/7/2019 11:38:08 AM 369.1 19.7
6/7/2019 11:38:09 AM 367.5 18.1
6/7/2019 11:38:10 AM 365.8 16.4
6/7/2019 11:38:11 AM 364.6 15.2
6/7/2019 11:38:12 AM 360.6 11.2
6/7/2019 11:38:13 AM 356.8 7.4
6/7/2019 11:38:14 AM 354.0 4.6
6/7/2019 11:38:15 AM 352.4 3.0
6/7/2019 11:38:16 AM 351.0 1.6
6/7/2019 11:38:17 AM 350.1 0.7
6/7/2019 11:38:18 AM 349.3 -0.1
6/7/2019 11:38:19 AM 348.7 -0.7
6/7/2019 11:38:20 AM 348.1 -1.3
6/7/2019 11:38:21 AM 347.6 -1.8
6/7/2019 11:38:22 AM 347.2 -2.2
6/7/2019 11:38:23 AM 346.8 -2.6
6/7/2019 11:38:24 AM 346.5 -2.9
6/7/2019 11:38:25 AM 346.1 -3.3
6/7/2019 11:38:26 AM 345.9 -3.5
6/7/2019 11:38:27 AM 345.6 -3.8
Table E1 OLDOF-2 TEST-4 Data Log
Page 30 of 452 August 2019
APPENDIX E11: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-4 June
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-2 TEST-4 Data Log
6/7/2019 11:38:28 AM 345.4 -4.0
6/7/2019 11:38:29 AM 345.2 -4.2
6/7/2019 11:38:30 AM 345.0 -4.4
6/7/2019 11:38:31 AM 344.8 -4.6
6/7/2019 11:38:32 AM 344.7 -4.7
6/7/2019 11:38:33 AM 344.5 -4.9
6/7/2019 11:38:34 AM 344.3 -5.1
6/7/2019 11:38:35 AM 344.2 -5.2
6/7/2019 11:38:36 AM 344.1 -5.3
6/7/2019 11:38:37 AM 343.9 -5.5
6/7/2019 11:38:38 AM 343.8 -5.6
6/7/2019 11:38:39 AM 343.7 -5.7
6/7/2019 11:38:40 AM 343.6 -5.8
6/7/2019 11:38:41 AM 343.5 -5.9
6/7/2019 11:38:42 AM 343.4 -6.0
Page 31 of 452 August 2019
APPENDIX E11: SALT DILUTION GAUGING SUMMARY
Old Outfall-2-Test-4 June
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
OLDOF-2 TEST-4 1038
OLDOF-2 TEST-4 1039
OLDOF-2 TEST-4 1039
OLDOF-2 TEST-4 1040
Location EC Reading
(µS/cms)
OLDOF-2 TEST-4 246
OLDOF-2 TEST-4 2,167
OLDOF-2 TEST-4 17,538
OLDOF-2 TEST-4 136,514
q 300,100
K 1.3691
22.0
349.6
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Table E2 OLDOF-2 TEST-4 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
(µS/cms) (°C)
342.5 20.5
342.0 20.5
341.9 20.5
341.1 20.5
Average 341.9 (µS/cms)
Geo Mean 341.9 (µS/cms)
Average (pre-test) 349.4 (µS/cms)
Average (post-test) 346.7 (µS/cms)
Table E3 OLDOF-2 TEST-4 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
Mass of Salt injected mg
(mg/L) (°C)
100 25.2
1,000 25.2
10,000 25.2
100,000 25.2
Table E4 OLDOF-2 TEST-4 Flow Calculation Summary
Slope of Calibration Curve (µS/cms) / (mg/L)
Integral of Conductivity Data Curve SUM:Δt(ECt-
ECbkg)18,657.0 (s) . (µS/cms)
Calculated Flow Rate Q
L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement Part 2: Constant-Rate
Injection.” Streamline, Watershed Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 32 of 452 August 2019
APPENDIX E12: SALT DILUTION GAUGING SUMMARY
Old Outfall-3-Test-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/2/2019 3:23:39 PM 258.2 `
2/2/2019 3:23:40 PM 258.3 -
2/2/2019 3:23:41 PM 258.2 -
2/2/2019 3:23:42 PM 258.0 -
2/2/2019 3:23:43 PM 257.9 -
2/2/2019 3:23:44 PM 257.9 -
2/2/2019 3:23:45 PM 257.9 -
2/2/2019 3:23:46 PM 258.0 -
2/2/2019 3:23:47 PM 258.0 -
2/2/2019 3:23:48 PM 258.1 -
2/2/2019 3:23:49 PM 258.2 -
2/2/2019 3:23:50 PM 258.3 -
2/2/2019 3:23:51 PM 258.3 -
2/2/2019 3:23:52 PM 258.2 -
2/2/2019 3:23:53 PM 258.1 -
2/2/2019 3:23:54 PM 258.1 -
2/2/2019 3:23:55 PM 258.1 -
2/2/2019 3:23:56 PM 258.2 -
2/2/2019 3:23:57 PM 258.2 -
2/2/2019 3:23:58 PM 258.2 -
2/2/2019 3:23:59 PM 258.1 -
2/2/2019 3:24:00 PM 257.9 -
2/2/2019 3:24:01 PM 257.8 -
2/2/2019 3:24:02 PM 257.6 -
2/2/2019 3:24:03 PM 257.4 -
2/2/2019 3:24:04 PM 257.2 -
2/2/2019 3:24:05 PM 257.1 -
2/2/2019 3:24:06 PM 257.0 -
2/2/2019 3:24:07 PM 257.0 -
2/2/2019 3:24:08 PM 256.9 -
2/2/2019 3:24:09 PM 256.8 -
2/2/2019 3:24:10 PM 256.7 -
2/2/2019 3:24:11 PM 256.7 -
2/2/2019 3:24:12 PM 256.7 -
2/2/2019 3:24:13 PM 256.7 -
2/2/2019 3:24:14 PM 256.8 -
2/2/2019 3:24:15 PM 257.0 -
2/2/2019 3:24:16 PM 257.5 -
2/2/2019 3:24:17 PM 258.5 -
2/2/2019 3:24:18 PM 260.8 -
2/2/2019 3:24:19 PM 320.4 62.6
2/2/2019 3:24:20 PM 347.8 90.0
2/2/2019 3:24:21 PM 392.8 135.0
2/2/2019 3:24:22 PM 422.2 164.4
2/2/2019 3:24:23 PM 442.9 185.1
2/2/2019 3:24:24 PM 538.0 280.2
2/2/2019 3:24:25 PM 558.3 300.5
2/2/2019 3:24:26 PM 608.4 350.6
2/2/2019 3:24:27 PM 618.3 360.5
2/2/2019 3:24:28 PM 635.8 378.0
2/2/2019 3:24:29 PM 644.9 387.1
2/2/2019 3:24:30 PM 654.9 397.1
2/2/2019 3:24:31 PM 663.4 405.6
2/2/2019 3:24:32 PM 672.0 414.2
2/2/2019 3:24:33 PM 678.2 420.4
2/2/2019 3:24:34 PM 683.2 425.4
2/2/2019 3:24:35 PM 685.7 427.9
2/2/2019 3:24:36 PM 686.7 428.9
2/2/2019 3:24:37 PM 686.4 428.6
2/2/2019 3:24:38 PM 685.0 427.2
2/2/2019 3:24:39 PM 682.6 424.8
2/2/2019 3:24:40 PM 634.2 376.4
2/2/2019 3:24:41 PM 618.1 360.3
2/2/2019 3:24:42 PM 603.2 345.4
2/2/2019 3:24:43 PM 590.0 332.2
2/2/2019 3:24:44 PM 583.3 325.5
2/2/2019 3:24:45 PM 574.4 316.6
2/2/2019 3:24:46 PM 565.9 308.1
2/2/2019 3:24:47 PM 557.0 299.2
2/2/2019 3:24:48 PM 550.5 292.7
Table E1 OLDOF-3-T1 Data Log
Page 33 of 452 August 2019
APPENDIX E12: SALT DILUTION GAUGING SUMMARY
Old Outfall-3-Test-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-3-T1 Data Log
2/2/2019 3:24:49 PM 544.4 286.6
2/2/2019 3:24:50 PM 538.9 281.1
2/2/2019 3:24:51 PM 486.8 229.0
2/2/2019 3:24:52 PM 478.8 221.0
2/2/2019 3:24:53 PM 463.4 205.6
2/2/2019 3:24:54 PM 460.1 202.3
2/2/2019 3:24:55 PM 451.8 194.0
2/2/2019 3:24:56 PM 445.8 188.0
2/2/2019 3:24:57 PM 439.9 182.1
2/2/2019 3:24:58 PM 435.7 177.9
2/2/2019 3:24:59 PM 432.0 174.2
2/2/2019 3:25:00 PM 429.1 171.3
2/2/2019 3:25:01 PM 426.3 168.5
2/2/2019 3:25:02 PM 423.8 166.0
2/2/2019 3:25:03 PM 420.7 162.9
2/2/2019 3:25:04 PM 417.6 159.8
2/2/2019 3:25:05 PM 414.1 156.3
2/2/2019 3:25:06 PM 411.0 153.2
2/2/2019 3:25:07 PM 405.0 147.2
2/2/2019 3:25:08 PM 399.1 141.3
2/2/2019 3:25:09 PM 392.9 135.1
2/2/2019 3:25:10 PM 387.8 130.0
2/2/2019 3:25:11 PM 382.1 124.3
2/2/2019 3:25:12 PM 377.2 119.4
2/2/2019 3:25:13 PM 371.7 113.9
2/2/2019 3:25:14 PM 366.8 109.0
2/2/2019 3:25:15 PM 361.3 103.5
2/2/2019 3:25:16 PM 357.0 99.2
2/2/2019 3:25:17 PM 352.6 94.8
2/2/2019 3:25:18 PM 348.9 91.1
2/2/2019 3:25:19 PM 344.9 87.1
2/2/2019 3:25:20 PM 341.5 83.7
2/2/2019 3:25:21 PM 337.7 79.9
2/2/2019 3:25:22 PM 334.6 76.8
2/2/2019 3:25:23 PM 331.1 73.3
2/2/2019 3:25:24 PM 328.0 70.2
2/2/2019 3:25:25 PM 324.4 66.6
2/2/2019 3:25:26 PM 321.3 63.5
2/2/2019 3:25:27 PM 318.1 60.3
2/2/2019 3:25:28 PM 315.5 57.7
2/2/2019 3:25:29 PM 312.6 54.8
2/2/2019 3:25:30 PM 310.2 52.4
2/2/2019 3:25:31 PM 307.6 49.8
2/2/2019 3:25:32 PM 305.5 47.7
2/2/2019 3:25:33 PM 303.2 45.4
2/2/2019 3:25:34 PM 301.0 43.2
2/2/2019 3:25:35 PM 299.1 41.3
2/2/2019 3:25:36 PM 297.1 39.3
2/2/2019 3:25:37 PM 295.5 37.7
2/2/2019 3:25:38 PM 293.8 36.0
2/2/2019 3:25:39 PM 292.4 34.6
2/2/2019 3:25:40 PM 290.8 33.0
2/2/2019 3:25:41 PM 289.4 31.6
2/2/2019 3:25:42 PM 287.7 29.9
2/2/2019 3:25:43 PM 286.3 28.5
2/2/2019 3:25:44 PM 284.9 27.1
2/2/2019 3:25:45 PM 283.8 26.0
2/2/2019 3:25:46 PM 282.6 24.8
2/2/2019 3:25:47 PM 281.6 23.8
2/2/2019 3:25:48 PM 280.4 22.6
2/2/2019 3:25:49 PM 279.4 21.6
2/2/2019 3:25:50 PM 278.4 20.6
2/2/2019 3:25:51 PM 277.5 19.7
2/2/2019 3:25:52 PM 276.6 18.8
2/2/2019 3:25:53 PM 275.8 18.0
2/2/2019 3:25:54 PM 275.1 17.3
2/2/2019 3:25:55 PM 274.5 16.7
2/2/2019 3:25:56 PM 273.7 15.9
2/2/2019 3:25:57 PM 273.0 15.2
2/2/2019 3:25:58 PM 272.1 14.3
2/2/2019 3:25:59 PM 271.4 13.6
2/2/2019 3:26:00 PM 270.8 13.0
2/2/2019 3:26:01 PM 270.4 12.6
2/2/2019 3:26:02 PM 269.8 12.0
2/2/2019 3:26:03 PM 269.3 11.5
2/2/2019 3:26:04 PM 268.6 10.8
2/2/2019 3:26:05 PM 268.1 10.3
Page 34 of 452 August 2019
APPENDIX E12: SALT DILUTION GAUGING SUMMARY
Old Outfall-3-Test-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-3-T1 Data Log
2/2/2019 3:26:06 PM 267.3 9.5
2/2/2019 3:26:07 PM 266.7 8.9
2/2/2019 3:26:08 PM 266.1 -
2/2/2019 3:26:09 PM 265.6 -
2/2/2019 3:26:10 PM 265.1 -
2/2/2019 3:26:11 PM 264.6 -
2/2/2019 3:26:12 PM 264.0 -
2/2/2019 3:26:13 PM 263.4 -
2/2/2019 3:26:14 PM 262.8 -
2/2/2019 3:26:15 PM 262.5 -
2/2/2019 3:26:16 PM 262.0 -
2/2/2019 3:26:17 PM 261.7 -
2/2/2019 3:26:18 PM 261.4 -
2/2/2019 3:26:19 PM 261.1 -
2/2/2019 3:26:20 PM 260.9 -
2/2/2019 3:26:21 PM 260.7 -
2/2/2019 3:26:22 PM 260.4 -
2/2/2019 3:26:23 PM 260.2 -
2/2/2019 3:26:24 PM 259.9 -
Page 35 of 452 August 2019
APPENDIX E12: SALT DILUTION GAUGING SUMMARY
Old Outfall-3-Test-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
OLDOF-3 TEST-1 1445
OLDOF-3 TEST-1 1446
OLDOF-3 TEST-1 1447
OLDOF-3 TEST-1 1449
OLDOF-3 TEST-1 1451
Location EC Reading
(µS/cms)
OLDOF-3 TEST-1 202.2
OLDOF-3 TEST-1 1,718.0
OLDOF-3 TEST-1 14,826.0
OLDOF-3 TEST-1 116,811.0
q 299,900
K 1.1713
21.33
338.50
Notes:
°C degrees celsius
mg/L miligrams per liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Table E2 OLDOF-3 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
(µS/cms) (°C)
264.8 14.3
269.1 14
220.7 14.3
256.8 14
257.3 14.3
Geometric Mean 253.1 (µS/cms)
Average (pre-test) 257.8 (µS/cms)
Average (post-test) 262.5 (µS/cms)
Table E3 OLDOF-3 TEST-1 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement
Part 2: Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8,
no. 1, 2004, pp. 11–15.
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Integral of Conductivity Data Curve SUM:Δt(ECt-
ECbkg)16,471.81 (s) . (µS/cms)
Calculated Flow Rate Q
L/s
GPM
10,000 17.3
100,000 17.7
Table E4 OLDOF-3-TEST-1 Flow Calculation Summary
(mg/L) (°C)
100 17.4
1,000 17.8
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 36 of 452 August 2019
APPENDIX E13: SALT DILUTION GAUGING SUMMARY
Old Outfall-3-Test-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/2/2019 3:23:39 PM 258.2 `
2/2/2019 3:23:40 PM 258.3 -
2/2/2019 3:23:41 PM 258.2 -
2/2/2019 3:23:42 PM 258.0 -
2/2/2019 3:23:43 PM 257.9 -
2/2/2019 3:23:44 PM 257.9 -
2/2/2019 3:23:45 PM 257.9 -
2/2/2019 3:23:46 PM 258.0 -
2/2/2019 3:23:47 PM 258.0 -
2/2/2019 3:23:48 PM 258.1 -
2/2/2019 3:23:49 PM 258.2 -
2/2/2019 3:23:50 PM 258.3 -
2/2/2019 3:23:51 PM 258.3 -
2/2/2019 3:23:52 PM 258.2 -
2/2/2019 3:23:53 PM 258.1 -
2/2/2019 3:23:54 PM 258.1 -
2/2/2019 3:23:55 PM 258.1 -
2/2/2019 3:23:56 PM 258.2 -
2/2/2019 3:23:57 PM 258.2 -
2/2/2019 3:23:58 PM 258.2 -
2/2/2019 3:23:59 PM 258.1 -
2/2/2019 3:24:00 PM 257.9 -
2/2/2019 3:24:01 PM 257.8 -
2/2/2019 3:24:02 PM 257.6 -
2/2/2019 3:24:03 PM 257.4 -
2/2/2019 3:24:04 PM 257.2 -
2/2/2019 3:24:05 PM 257.1 -
2/2/2019 3:24:06 PM 257.0 -
2/2/2019 3:24:07 PM 257.0 -
2/2/2019 3:24:08 PM 256.9 -
2/2/2019 3:24:09 PM 256.8 -
2/2/2019 3:24:10 PM 256.7 -
2/2/2019 3:24:11 PM 256.7 -
2/2/2019 3:24:12 PM 256.7 -
2/2/2019 3:24:13 PM 256.7 -
2/2/2019 3:24:14 PM 256.8 -
2/2/2019 3:24:15 PM 257.0 -
2/2/2019 3:24:16 PM 257.5 -
2/2/2019 3:24:17 PM 258.5 -
2/2/2019 3:24:18 PM 260.8 -
2/2/2019 3:24:19 PM 320.4 62.6
2/2/2019 3:24:20 PM 347.8 90.0
2/2/2019 3:24:21 PM 392.8 135.0
2/2/2019 3:24:22 PM 422.2 164.4
2/2/2019 3:24:23 PM 442.9 185.1
2/2/2019 3:24:24 PM 538.0 280.2
2/2/2019 3:24:25 PM 558.3 300.5
2/2/2019 3:24:26 PM 608.4 350.6
2/2/2019 3:24:27 PM 618.3 360.5
2/2/2019 3:24:28 PM 635.8 378.0
2/2/2019 3:24:29 PM 644.9 387.1
2/2/2019 3:24:30 PM 654.9 397.1
2/2/2019 3:24:31 PM 663.4 405.6
2/2/2019 3:24:32 PM 672.0 414.2
2/2/2019 3:24:33 PM 678.2 420.4
2/2/2019 3:24:34 PM 683.2 425.4
2/2/2019 3:24:35 PM 685.7 427.9
2/2/2019 3:24:36 PM 686.7 428.9
2/2/2019 3:24:37 PM 686.4 428.6
2/2/2019 3:24:38 PM 685.0 427.2
2/2/2019 3:24:39 PM 682.6 424.8
2/2/2019 3:24:40 PM 634.2 376.4
2/2/2019 3:24:41 PM 618.1 360.3
2/2/2019 3:24:42 PM 603.2 345.4
2/2/2019 3:24:43 PM 590.0 332.2
2/2/2019 3:24:44 PM 583.3 325.5
2/2/2019 3:24:45 PM 574.4 316.6
2/2/2019 3:24:46 PM 565.9 308.1
2/2/2019 3:24:47 PM 557.0 299.2
2/2/2019 3:24:48 PM 550.5 292.7
Table E1 OLDOF-3-T2 Data Log
Page 37 of 452 August 2019
APPENDIX E13: SALT DILUTION GAUGING SUMMARY
Old Outfall-3-Test-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-3-T2 Data Log
2/2/2019 3:24:49 PM 544.4 286.6
2/2/2019 3:24:50 PM 538.9 281.1
2/2/2019 3:24:51 PM 486.8 229.0
2/2/2019 3:24:52 PM 478.8 221.0
2/2/2019 3:24:53 PM 463.4 205.6
2/2/2019 3:24:54 PM 460.1 202.3
2/2/2019 3:24:55 PM 451.8 194.0
2/2/2019 3:24:56 PM 445.8 188.0
2/2/2019 3:24:57 PM 439.9 182.1
2/2/2019 3:24:58 PM 435.7 177.9
2/2/2019 3:24:59 PM 432.0 174.2
2/2/2019 3:25:00 PM 429.1 171.3
2/2/2019 3:25:01 PM 426.3 168.5
2/2/2019 3:25:02 PM 423.8 166.0
2/2/2019 3:25:03 PM 420.7 162.9
2/2/2019 3:25:04 PM 417.6 159.8
2/2/2019 3:25:05 PM 414.1 156.3
2/2/2019 3:25:06 PM 411.0 153.2
2/2/2019 3:25:07 PM 405.0 147.2
2/2/2019 3:25:08 PM 399.1 141.3
2/2/2019 3:25:09 PM 392.9 135.1
2/2/2019 3:25:10 PM 387.8 130.0
2/2/2019 3:25:11 PM 382.1 124.3
2/2/2019 3:25:12 PM 377.2 119.4
2/2/2019 3:25:13 PM 371.7 113.9
2/2/2019 3:25:14 PM 366.8 109.0
2/2/2019 3:25:15 PM 361.3 103.5
2/2/2019 3:25:16 PM 357.0 99.2
2/2/2019 3:25:17 PM 352.6 94.8
2/2/2019 3:25:18 PM 348.9 91.1
2/2/2019 3:25:19 PM 344.9 87.1
2/2/2019 3:25:20 PM 341.5 83.7
2/2/2019 3:25:21 PM 337.7 79.9
2/2/2019 3:25:22 PM 334.6 76.8
2/2/2019 3:25:23 PM 331.1 73.3
2/2/2019 3:25:24 PM 328.0 70.2
2/2/2019 3:25:25 PM 324.4 66.6
2/2/2019 3:25:26 PM 321.3 63.5
2/2/2019 3:25:27 PM 318.1 60.3
2/2/2019 3:25:28 PM 315.5 57.7
2/2/2019 3:25:29 PM 312.6 54.8
2/2/2019 3:25:30 PM 310.2 52.4
2/2/2019 3:25:31 PM 307.6 49.8
2/2/2019 3:25:32 PM 305.5 47.7
2/2/2019 3:25:33 PM 303.2 45.4
2/2/2019 3:25:34 PM 301.0 43.2
2/2/2019 3:25:35 PM 299.1 41.3
2/2/2019 3:25:36 PM 297.1 39.3
2/2/2019 3:25:37 PM 295.5 37.7
2/2/2019 3:25:38 PM 293.8 36.0
2/2/2019 3:25:39 PM 292.4 34.6
2/2/2019 3:25:40 PM 290.8 33.0
2/2/2019 3:25:41 PM 289.4 31.6
2/2/2019 3:25:42 PM 287.7 29.9
2/2/2019 3:25:43 PM 286.3 28.5
2/2/2019 3:25:44 PM 284.9 27.1
2/2/2019 3:25:45 PM 283.8 26.0
2/2/2019 3:25:46 PM 282.6 24.8
2/2/2019 3:25:47 PM 281.6 23.8
2/2/2019 3:25:48 PM 280.4 22.6
2/2/2019 3:25:49 PM 279.4 21.6
2/2/2019 3:25:50 PM 278.4 20.6
2/2/2019 3:25:51 PM 277.5 19.7
2/2/2019 3:25:52 PM 276.6 18.8
2/2/2019 3:25:53 PM 275.8 18.0
2/2/2019 3:25:54 PM 275.1 17.3
2/2/2019 3:25:55 PM 274.5 16.7
2/2/2019 3:25:56 PM 273.7 15.9
2/2/2019 3:25:57 PM 273.0 15.2
2/2/2019 3:25:58 PM 272.1 14.3
2/2/2019 3:25:59 PM 271.4 13.6
2/2/2019 3:26:00 PM 270.8 13.0
2/2/2019 3:26:01 PM 270.4 12.6
2/2/2019 3:26:02 PM 269.8 12.0
2/2/2019 3:26:03 PM 269.3 11.5
2/2/2019 3:26:04 PM 268.6 10.8
2/2/2019 3:26:05 PM 268.1 10.3
2/2/2019 3:26:06 PM 267.3 9.5
Page 38 of 452 August 2019
APPENDIX E13: SALT DILUTION GAUGING SUMMARY
Old Outfall-3-Test-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-3-T2 Data Log
2/2/2019 3:26:07 PM 266.7 8.9
2/2/2019 3:26:08 PM 266.1 -
2/2/2019 3:26:09 PM 265.6 -
2/2/2019 3:26:10 PM 265.1 -
2/2/2019 3:26:11 PM 264.6 -
2/2/2019 3:26:12 PM 264.0 -
2/2/2019 3:26:13 PM 263.4 -
2/2/2019 3:26:14 PM 262.8 -
2/2/2019 3:26:15 PM 262.5 -
2/2/2019 3:26:16 PM 262.0 -
2/2/2019 3:26:17 PM 261.7 -
2/2/2019 3:26:18 PM 261.4 -
2/2/2019 3:26:19 PM 261.1 -
2/2/2019 3:26:20 PM 260.9 -
2/2/2019 3:26:21 PM 260.7 -
2/2/2019 3:26:22 PM 260.4 -
2/2/2019 3:26:23 PM 260.2 -
2/2/2019 3:26:24 PM 259.9 -
Page 39 of 452 August 2019
APPENDIX E13: SALT DILUTION GAUGING SUMMARY
Old Outfall-3-Test-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
OLDOF-3 TEST-2 1445
OLDOF-3 TEST-2 1446
OLDOF-3 TEST-2 1447
OLDOF-3 TEST-2 1449
OLDOF-3 TEST-2 1451
Location EC Reading
(µS/cms)
OLDOF-3 TEST-2 202.2
OLDOF-3 TEST-2 1,718.0
OLDOF-3 TEST-2 14,826.0
OLDOF-3 TEST-2 116,811.0
q 299,900
K 1.1713
21.33
338.50
Notes:
°C degrees celsius
mg/L miligrams per liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Location Time Background Stream EC
Background Stream
Temperature
(µS/cms) (°C)
264.8 14.3
269.1 14
220.7 14.3
256.8 14
257.3 14.3
Geometric Mean 253.1 (µS/cms)
Average (pre-test) 257.8 (µS/cms)
17.8
Average (post-test) 262.5 (µS/cms)
Table E3 OLDOF3 TEST-2 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement
Part 2: Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8,
no. 1, 2004, pp. 11–15.
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Integral of Conductivity Data Curve SUM:Δt(ECt-
ECbkg)16,471.81 (s) . (µS/cms)
Table E2 OLDOF3 TEST-2 Stream Background Conductivity Data
Calculated Flow Rate Q
L/s
GPM
10,000 17.3
100,000 17.7
Table E4 OLDOF3 TEST-2 Flow Calculation Summary
(mg/L) (°C)
100 17.4
1,000
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 40 of 452 August 2019
APPENDIX E14: SALT DILUTION GAUGING SUMMARY
Old Outfall-3-Test-3 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/2/2019 3:50:39 PM 262.1 -
2/2/2019 3:50:40 PM 261.9 -
2/2/2019 3:50:41 PM 261.7 -
2/2/2019 3:50:42 PM 261.6 -
2/2/2019 3:50:43 PM 261.4 -
2/2/2019 3:50:44 PM 261.2 -
2/2/2019 3:50:45 PM 261.0 -
2/2/2019 3:50:46 PM 260.8 -
2/2/2019 3:50:47 PM 260.7 -
2/2/2019 3:50:48 PM 260.5 -
2/2/2019 3:50:49 PM 260.3 -
2/2/2019 3:50:50 PM 260.2 -
2/2/2019 3:50:51 PM 260.0 -
2/2/2019 3:50:52 PM 259.8 -
2/2/2019 3:50:53 PM 259.6 -
2/2/2019 3:50:54 PM 259.5 -
2/2/2019 3:50:55 PM 259.4 -
2/2/2019 3:50:56 PM 259.2 -
2/2/2019 3:50:57 PM 259.1 -
2/2/2019 3:50:58 PM 259.0 -
2/2/2019 3:50:59 PM 258.9 -
2/2/2019 3:51:00 PM 258.8 -
2/2/2019 3:51:01 PM 258.7 -
2/2/2019 3:51:02 PM 258.6 -
2/2/2019 3:51:03 PM 258.5 -
2/2/2019 3:51:04 PM 258.5 -
2/2/2019 3:51:05 PM 258.5 -
2/2/2019 3:51:06 PM 258.5 -
2/2/2019 3:51:07 PM 258.8 -
2/2/2019 3:51:08 PM 260.1 -
2/2/2019 3:51:09 PM 262.5 -
2/2/2019 3:51:10 PM 349.1 89.1
2/2/2019 3:51:11 PM 370.1 110.1
2/2/2019 3:51:12 PM 423.7 163.7
2/2/2019 3:51:13 PM 458.0 198.0
2/2/2019 3:51:14 PM 566.0 306.0
2/2/2019 3:51:15 PM 635.8 375.8
2/2/2019 3:51:16 PM 726.4 466.4
2/2/2019 3:51:17 PM 739.2 479.2
2/2/2019 3:51:18 PM 758.8 498.8
2/2/2019 3:51:19 PM 838.4 578.4
2/2/2019 3:51:20 PM 840.0 580.0
2/2/2019 3:51:21 PM 836.6 576.6
2/2/2019 3:51:22 PM 826.3 566.3
2/2/2019 3:51:23 PM 811.7 551.7
2/2/2019 3:51:24 PM 799.6 539.6
2/2/2019 3:51:25 PM 736.9 476.9
2/2/2019 3:51:26 PM 715.2 455.2
2/2/2019 3:51:27 PM 692.9 432.9
2/2/2019 3:51:28 PM 683.1 423.1
2/2/2019 3:51:29 PM 667.2 407.2
2/2/2019 3:51:30 PM 550.8 290.8
2/2/2019 3:51:31 PM 607.3 347.3
2/2/2019 3:51:32 PM 598.5 338.5
2/2/2019 3:51:33 PM 579.0 319.0
2/2/2019 3:51:34 PM 565.7 305.7
2/2/2019 3:51:35 PM 549.3 289.3
2/2/2019 3:51:36 PM 536.9 276.9
2/2/2019 3:51:37 PM 530.6 270.6
2/2/2019 3:51:38 PM 525.1 265.1
2/2/2019 3:51:39 PM 519.3 259.3
2/2/2019 3:51:40 PM 461.8 201.8
2/2/2019 3:51:41 PM 452.0 192.0
2/2/2019 3:51:42 PM 442.8 182.8
2/2/2019 3:51:43 PM 438.0 178.0
2/2/2019 3:51:44 PM 435.7 175.7
2/2/2019 3:51:45 PM 431.8 171.8
2/2/2019 3:51:46 PM 423.9 163.9
2/2/2019 3:51:47 PM 418.1 158.1
2/2/2019 3:51:48 PM 412.7 152.7
Table E1 OLDOF-3-T3 Data Log
Page 41 of 452 August 2019
APPENDIX E14: SALT DILUTION GAUGING SUMMARY
Old Outfall-3-Test-3 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-3-T3 Data Log
2/2/2019 3:51:49 PM 409.1 149.1
2/2/2019 3:51:50 PM 404.0 144.0
2/2/2019 3:51:51 PM 399.5 139.5
2/2/2019 3:51:52 PM 394.6 134.6
2/2/2019 3:51:53 PM 344.4 84.4
2/2/2019 3:51:54 PM 336.6 76.6
2/2/2019 3:51:55 PM 332.7 72.7
2/2/2019 3:51:56 PM 329.3 69.3
2/2/2019 3:51:57 PM 327.6 67.6
2/2/2019 3:51:58 PM 325.6 65.6
2/2/2019 3:51:59 PM 324.0 64.0
2/2/2019 3:52:00 PM 321.9 61.9
2/2/2019 3:52:01 PM 319.8 59.8
2/2/2019 3:52:02 PM 318.4 58.4
2/2/2019 3:52:03 PM 317.1 57.1
2/2/2019 3:52:04 PM 316.2 56.2
2/2/2019 3:52:05 PM 314.8 54.8
2/2/2019 3:52:06 PM 313.4 53.4
2/2/2019 3:52:07 PM 311.8 51.8
2/2/2019 3:52:08 PM 310.5 50.5
2/2/2019 3:52:09 PM 309.1 49.1
2/2/2019 3:52:10 PM 306.6 46.6
2/2/2019 3:52:11 PM 303.8 43.8
2/2/2019 3:52:12 PM 301.3 41.3
2/2/2019 3:52:13 PM 298.7 38.7
2/2/2019 3:52:14 PM 296.6 36.6
2/2/2019 3:52:15 PM 294.1 34.1
2/2/2019 3:52:16 PM 291.9 31.9
2/2/2019 3:52:17 PM 289.5 29.5
2/2/2019 3:52:18 PM 287.7 27.7
2/2/2019 3:52:19 PM 285.8 25.8
2/2/2019 3:52:20 PM 284.2 24.2
2/2/2019 3:52:21 PM 282.5 22.5
2/2/2019 3:52:22 PM 281.1 21.1
2/2/2019 3:52:23 PM 279.4 19.4
2/2/2019 3:52:24 PM 278.2 18.2
2/2/2019 3:52:25 PM 276.9 16.9
2/2/2019 3:52:26 PM 275.9 15.9
2/2/2019 3:52:27 PM 274.7 14.7
2/2/2019 3:52:28 PM 273.6 13.6
2/2/2019 3:52:29 PM 272.5 12.5
2/2/2019 3:52:30 PM 271.6 11.6
2/2/2019 3:52:31 PM 270.6 10.6
2/2/2019 3:52:32 PM 269.8 9.8
2/2/2019 3:52:33 PM 268.9 8.9
2/2/2019 3:52:34 PM 268.2 8.2
2/2/2019 3:52:35 PM 267.3 7.3
2/2/2019 3:52:36 PM 266.6 6.6
2/2/2019 3:52:37 PM 265.8 -
2/2/2019 3:52:38 PM 265.1 -
2/2/2019 3:52:39 PM 264.4 -
2/2/2019 3:52:40 PM 263.9 -
2/2/2019 3:52:41 PM 263.2 -
2/2/2019 3:52:42 PM 262.7 -
2/2/2019 3:52:43 PM 262.2 -
2/2/2019 3:52:44 PM 261.7 -
2/2/2019 3:52:45 PM 261.2 -
2/2/2019 3:52:46 PM 260.7 -
Page 42 of 452 August 2019
APPENDIX E14: SALT DILUTION GAUGING SUMMARY
Old Outfall-3-Test-3 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
OLDOF-3 TEST-3 1445
OLDOF-3 TEST-3 1446
OLDOF-3 TEST-3 1447
OLDOF-3 TEST-3 1449
OLDOF-3 TEST-3 1451
Location EC Reading
(µS/cms)
OLDOF-3 TEST-3 202.2
OLDOF-3 TEST-3 1,718.0
OLDOF-3 TEST-3 14,826.0
OLDOF-3 TEST-3 116,811.0
q 300,000
K 1.1713
23.4
371.0
Notes:
°C
mg/L degrees celsius
µS/cms miligrams per liter
GPM microSiemens per centimeter second
s gallons per minute
Ect second
Ecbkg raw electronic conductivty during test
Δt background electronic conductivity value
Equation for flotime interval between conductivity readings (1 second)
Table E2 OLDOF3 TEST-3 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
(µS/cms) (°C)
264.8 14.3
269.1 14
220.7 14.3
256.8 14
257.3 14.3
Average 253.7 (µS/cms)
Geometric Mean 253.1 (µS/cms)
100 17.4
Average (pre-test)260.0 (µS/cms)
Average (post-test)263.1 (µS/cms)
Table E3 OLDOF3 TEST-3 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
(mg/L)(°C)
Integral of Conductivity Data Curve SUM:Δt(ECt-
ECbkg)15034.4 (s) . (µS/cms)
1,000 17.8
10,000 17.3
100,000 17.7
Table E4 OLDOF3 TEST-3 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Calculated Flow Rate Q L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement
Part 2: Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8,
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 43 of 452 August 2019
APPENDIX E15: SALT DILUTION GAUGING SUMMARY
Old Outfall-5 Test-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/2/2019 10:16:17 AM 132.3 -
2/2/2019 10:16:18 AM 132.3 -
2/2/2019 10:16:19 AM 132.3 -
2/2/2019 10:16:20 AM 132.2 -
2/2/2019 10:16:21 AM 132.2 -
2/2/2019 10:16:22 AM 132.2 -
2/2/2019 10:16:23 AM 132.1 -
2/2/2019 10:16:24 AM 132.1 -
2/2/2019 10:16:25 AM 132.1 -
2/2/2019 10:16:26 AM 132.1 -
2/2/2019 10:16:27 AM 132.1 -
2/2/2019 10:16:28 AM 132.1 -
2/2/2019 10:16:29 AM 132.1 -
2/2/2019 10:16:30 AM 132.0 -
2/2/2019 10:16:31 AM 132.0 -
2/2/2019 10:16:32 AM 132.0 -
2/2/2019 10:16:33 AM 131.9 -
2/2/2019 10:16:34 AM 132.0 -
2/2/2019 10:16:35 AM 132.0 -
2/2/2019 10:16:36 AM 131.9 -
2/2/2019 10:16:37 AM 131.9 -
2/2/2019 10:16:38 AM 131.9 -
2/2/2019 10:16:39 AM 131.9 -
2/2/2019 10:16:40 AM 131.9 -
2/2/2019 10:16:41 AM 132.0 -
2/2/2019 10:16:42 AM 132.0 -
2/2/2019 10:16:43 AM 132.0 -
2/2/2019 10:16:44 AM 132.0 -
2/2/2019 10:16:45 AM 132.0 -
2/2/2019 10:16:46 AM 132.0 -
2/2/2019 10:16:47 AM 132.0 -
2/2/2019 10:16:48 AM 132.0 -
2/2/2019 10:16:49 AM 132.0 -
2/2/2019 10:16:50 AM 131.9 -
2/2/2019 10:16:51 AM 131.9 -
2/2/2019 10:16:52 AM 131.9 -
2/2/2019 10:16:53 AM 131.9 -
2/2/2019 10:16:54 AM 131.8 -
2/2/2019 10:16:55 AM 131.8 -
2/2/2019 10:16:56 AM 131.8 -
2/2/2019 10:16:57 AM 131.8 -
2/2/2019 10:16:58 AM 131.8 -
2/2/2019 10:16:59 AM 131.8 -
2/2/2019 10:17:00 AM 131.8 -
2/2/2019 10:17:01 AM 131.7 -
2/2/2019 10:17:02 AM 131.7 -
2/2/2019 10:17:03 AM 131.7 -
2/2/2019 10:17:04 AM 131.8 -
2/2/2019 10:17:05 AM 131.8 -
2/2/2019 10:17:06 AM 131.8 -
2/2/2019 10:17:07 AM 131.8 -
2/2/2019 10:17:08 AM 131.7 -
2/2/2019 10:17:09 AM 131.7 -
2/2/2019 10:17:10 AM 131.6 -
2/2/2019 10:17:11 AM 131.6 -
2/2/2019 10:17:12 AM 131.6 -
2/2/2019 10:17:13 AM 131.6 -
2/2/2019 10:17:14 AM 131.6 -
2/2/2019 10:17:15 AM 131.6 -
2/2/2019 10:17:16 AM 131.5 -
2/2/2019 10:17:17 AM 131.5 -
2/2/2019 10:17:18 AM 131.5 -
2/2/2019 10:17:19 AM 131.5 -
2/2/2019 10:17:20 AM 131.5 -
2/2/2019 10:17:21 AM 131.5 -
2/2/2019 10:17:22 AM 131.4 -
2/2/2019 10:17:23 AM 131.4 -
2/2/2019 10:17:24 AM 131.4 -
2/2/2019 10:17:25 AM 131.4 -
2/2/2019 10:17:26 AM 131.4 -
Table E1 OLDOF-5 TEST-1 Data Log
Page 44 of 452 August 2019
APPENDIX E15: SALT DILUTION GAUGING SUMMARY
Old Outfall-5 Test-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-5 TEST-1 Data Log
2/2/2019 10:17:27 AM 131.4 -
2/2/2019 10:17:28 AM 131.4 -
2/2/2019 10:17:29 AM 131.4 -
2/2/2019 10:17:30 AM 131.4 -
2/2/2019 10:17:31 AM 131.4 -
2/2/2019 10:17:32 AM 131.4 -
2/2/2019 10:17:33 AM 131.4 -
2/2/2019 10:17:34 AM 131.5 -
2/2/2019 10:17:35 AM 131.5 -
2/2/2019 10:17:36 AM 131.6 -
2/2/2019 10:17:37 AM 131.7 -
2/2/2019 10:17:38 AM 131.9 -
2/2/2019 10:17:39 AM 132.1 -
2/2/2019 10:17:40 AM 132.4 -
2/2/2019 10:17:41 AM 133.0 -
2/2/2019 10:17:42 AM 133.7 -
2/2/2019 10:17:43 AM 135.0 -
2/2/2019 10:17:44 AM 136.3 -
2/2/2019 10:17:45 AM 138.1 6.2
2/2/2019 10:17:46 AM 139.8 7.9
2/2/2019 10:17:47 AM 142.3 10.4
2/2/2019 10:17:48 AM 145.7 13.8
2/2/2019 10:17:49 AM 212.8 80.9
2/2/2019 10:17:50 AM 223.3 91.4
2/2/2019 10:17:51 AM 234.7 102.8
2/2/2019 10:17:52 AM 239.4 107.5
2/2/2019 10:17:53 AM 247.0 115.1
2/2/2019 10:17:54 AM 256.6 124.7
2/2/2019 10:17:55 AM 267.5 135.6
2/2/2019 10:17:56 AM 273.7 141.8
2/2/2019 10:17:57 AM 278.9 147.0
2/2/2019 10:17:58 AM 345.0 213.1
2/2/2019 10:17:59 AM 378.1 246.2
2/2/2019 10:18:00 AM 397.7 265.8
2/2/2019 10:18:01 AM 429.6 297.7
2/2/2019 10:18:02 AM 438.4 306.5
2/2/2019 10:18:03 AM 456.4 324.5
2/2/2019 10:18:04 AM 467.0 335.1
2/2/2019 10:18:05 AM 476.4 344.5
2/2/2019 10:18:06 AM 546.5 414.6
2/2/2019 10:18:07 AM 575.1 443.2
2/2/2019 10:18:08 AM 597.2 465.3
2/2/2019 10:18:09 AM 599.4 467.5
2/2/2019 10:18:10 AM 604.9 473.0
2/2/2019 10:18:11 AM 616.1 484.2
2/2/2019 10:18:12 AM 623.2 491.3
2/2/2019 10:18:13 AM 628.8 496.9
2/2/2019 10:18:14 AM 633.2 501.3
2/2/2019 10:18:15 AM 639.1 507.2
2/2/2019 10:18:16 AM 644.1 512.2
2/2/2019 10:18:17 AM 691.1 559.2
2/2/2019 10:18:18 AM 696.0 564.1
2/2/2019 10:18:19 AM 706.1 574.2
2/2/2019 10:18:20 AM 706.8 574.9
2/2/2019 10:18:21 AM 708.1 576.2
2/2/2019 10:18:22 AM 709.3 577.4
2/2/2019 10:18:23 AM 710.3 578.4
2/2/2019 10:18:24 AM 710.9 579.0
2/2/2019 10:18:25 AM 711.4 579.5
2/2/2019 10:18:26 AM 711.7 579.8
2/2/2019 10:18:27 AM 712.0 580.1
2/2/2019 10:18:28 AM 712.1 580.2
2/2/2019 10:18:29 AM 711.8 579.9
2/2/2019 10:18:30 AM 711.2 579.3
2/2/2019 10:18:31 AM 710.2 578.3
2/2/2019 10:18:32 AM 709.1 577.2
2/2/2019 10:18:33 AM 708.2 576.3
2/2/2019 10:18:34 AM 706.7 574.8
2/2/2019 10:18:35 AM 705.1 573.2
2/2/2019 10:18:36 AM 702.8 570.9
2/2/2019 10:18:37 AM 700.5 568.6
2/2/2019 10:18:38 AM 697.3 565.4
2/2/2019 10:18:39 AM 693.9 562.0
2/2/2019 10:18:40 AM 689.5 557.6
2/2/2019 10:18:41 AM 685.5 553.6
Page 45 of 452 August 2019
APPENDIX E15: SALT DILUTION GAUGING SUMMARY
Old Outfall-5 Test-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-5 TEST-1 Data Log
2/2/2019 10:18:42 AM 681.0 549.1
2/2/2019 10:18:43 AM 677.3 545.4
2/2/2019 10:18:44 AM 673.0 541.1
2/2/2019 10:18:45 AM 669.2 537.3
2/2/2019 10:18:46 AM 664.7 532.8
2/2/2019 10:18:47 AM 660.7 528.8
2/2/2019 10:18:48 AM 655.8 523.9
2/2/2019 10:18:49 AM 606.4 474.5
2/2/2019 10:18:50 AM 598.1 466.2
2/2/2019 10:18:51 AM 592.4 460.5
2/2/2019 10:18:52 AM 589.6 457.7
2/2/2019 10:18:53 AM 587.0 455.1
2/2/2019 10:18:54 AM 583.0 451.1
2/2/2019 10:18:55 AM 578.8 446.9
2/2/2019 10:18:56 AM 575.2 443.3
2/2/2019 10:18:57 AM 572.6 440.7
2/2/2019 10:18:58 AM 569.3 437.4
2/2/2019 10:18:59 AM 566.7 434.8
2/2/2019 10:19:00 AM 564.0 432.1
2/2/2019 10:19:01 AM 561.7 429.8
2/2/2019 10:19:02 AM 559.1 427.2
2/2/2019 10:19:03 AM 556.6 424.7
2/2/2019 10:19:04 AM 508.0 376.1
2/2/2019 10:19:05 AM 499.3 367.4
2/2/2019 10:19:06 AM 491.5 359.6
2/2/2019 10:19:07 AM 487.3 355.4
2/2/2019 10:19:08 AM 486.4 354.5
2/2/2019 10:19:09 AM 484.6 352.7
2/2/2019 10:19:10 AM 482.8 350.9
2/2/2019 10:19:11 AM 481.0 349.1
2/2/2019 10:19:12 AM 478.8 346.9
2/2/2019 10:19:13 AM 476.9 345.0
2/2/2019 10:19:14 AM 474.6 342.7
2/2/2019 10:19:15 AM 472.7 340.8
2/2/2019 10:19:16 AM 471.0 339.1
2/2/2019 10:19:17 AM 468.6 336.7
2/2/2019 10:19:18 AM 465.9 334.0
2/2/2019 10:19:19 AM 463.1 331.2
2/2/2019 10:19:20 AM 460.9 329.0
2/2/2019 10:19:21 AM 456.7 324.8
2/2/2019 10:19:22 AM 452.6 320.7
2/2/2019 10:19:23 AM 447.7 315.8
2/2/2019 10:19:24 AM 443.5 311.6
2/2/2019 10:19:25 AM 438.8 306.9
2/2/2019 10:19:26 AM 434.9 303.0
2/2/2019 10:19:27 AM 430.4 298.5
2/2/2019 10:19:28 AM 426.4 294.5
2/2/2019 10:19:29 AM 422.0 290.1
2/2/2019 10:19:30 AM 418.6 286.7
2/2/2019 10:19:31 AM 414.4 282.5
2/2/2019 10:19:32 AM 410.6 278.7
2/2/2019 10:19:33 AM 406.1 274.2
2/2/2019 10:19:34 AM 402.4 270.5
2/2/2019 10:19:35 AM 398.3 266.4
2/2/2019 10:19:36 AM 394.8 262.9
2/2/2019 10:19:37 AM 390.9 259.0
2/2/2019 10:19:38 AM 387.2 255.3
2/2/2019 10:19:39 AM 382.9 251.0
2/2/2019 10:19:40 AM 379.2 247.3
2/2/2019 10:19:41 AM 374.8 242.9
2/2/2019 10:19:42 AM 370.9 239.0
2/2/2019 10:19:43 AM 366.9 235.0
2/2/2019 10:19:44 AM 363.7 231.8
2/2/2019 10:19:45 AM 360.2 228.3
2/2/2019 10:19:46 AM 357.2 225.3
2/2/2019 10:19:47 AM 353.8 221.9
2/2/2019 10:19:48 AM 350.6 218.7
2/2/2019 10:19:49 AM 347.0 215.1
2/2/2019 10:19:50 AM 344.0 212.1
2/2/2019 10:19:51 AM 341.0 209.1
2/2/2019 10:19:52 AM 338.3 206.4
2/2/2019 10:19:53 AM 335.3 203.4
2/2/2019 10:19:54 AM 332.4 200.5
2/2/2019 10:19:55 AM 329.3 197.4
2/2/2019 10:19:56 AM 326.6 194.7
2/2/2019 10:19:57 AM 323.8 191.9
Page 46 of 452 August 2019
APPENDIX E15: SALT DILUTION GAUGING SUMMARY
Old Outfall-5 Test-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-5 TEST-1 Data Log
2/2/2019 10:19:58 AM 321.3 189.4
2/2/2019 10:19:59 AM 318.6 186.7
2/2/2019 10:20:00 AM 315.9 184.0
2/2/2019 10:20:01 AM 313.6 181.7
2/2/2019 10:20:02 AM 310.9 179.0
2/2/2019 10:20:03 AM 308.4 176.5
2/2/2019 10:20:04 AM 305.6 173.7
2/2/2019 10:20:05 AM 303.1 171.2
2/2/2019 10:20:06 AM 300.5 168.6
2/2/2019 10:20:07 AM 298.3 166.4
2/2/2019 10:20:08 AM 296.1 164.2
2/2/2019 10:20:09 AM 294.2 162.3
2/2/2019 10:20:10 AM 292.1 160.2
2/2/2019 10:20:11 AM 290.1 158.2
2/2/2019 10:20:12 AM 288.0 156.1
2/2/2019 10:20:13 AM 286.2 154.3
2/2/2019 10:20:14 AM 284.4 152.5
2/2/2019 10:20:15 AM 282.9 151.0
2/2/2019 10:20:16 AM 281.3 149.4
2/2/2019 10:20:17 AM 280.0 148.1
2/2/2019 10:20:18 AM 278.3 146.4
2/2/2019 10:20:19 AM 276.7 144.8
2/2/2019 10:20:20 AM 274.9 143.0
2/2/2019 10:20:21 AM 273.2 141.3
2/2/2019 10:20:22 AM 271.2 139.3
2/2/2019 10:20:23 AM 269.4 137.5
2/2/2019 10:20:24 AM 267.5 135.6
2/2/2019 10:20:25 AM 265.9 134.0
2/2/2019 10:20:26 AM 264.1 132.2
2/2/2019 10:20:27 AM 262.5 130.6
2/2/2019 10:20:28 AM 260.7 128.8
2/2/2019 10:20:29 AM 259.2 127.3
2/2/2019 10:20:30 AM 257.5 125.6
2/2/2019 10:20:31 AM 256.2 124.3
2/2/2019 10:20:32 AM 254.7 122.8
2/2/2019 10:20:33 AM 253.6 121.7
2/2/2019 10:20:34 AM 252.1 120.2
2/2/2019 10:20:35 AM 250.9 119.0
2/2/2019 10:20:36 AM 249.6 117.7
2/2/2019 10:20:37 AM 248.4 116.5
2/2/2019 10:20:38 AM 247.1 115.2
2/2/2019 10:20:39 AM 245.9 114.0
2/2/2019 10:20:40 AM 244.4 112.5
2/2/2019 10:20:41 AM 243.1 111.2
2/2/2019 10:20:42 AM 241.6 109.7
2/2/2019 10:20:43 AM 240.4 108.5
2/2/2019 10:20:44 AM 239.0 107.1
2/2/2019 10:20:45 AM 237.8 105.9
2/2/2019 10:20:46 AM 236.4 104.5
2/2/2019 10:20:47 AM 235.2 103.3
2/2/2019 10:20:48 AM 233.8 101.9
2/2/2019 10:20:49 AM 232.5 100.6
2/2/2019 10:20:50 AM 231.2 99.3
2/2/2019 10:20:51 AM 229.9 98.0
2/2/2019 10:20:52 AM 228.7 96.8
2/2/2019 10:20:53 AM 227.4 95.5
2/2/2019 10:20:54 AM 226.4 94.5
2/2/2019 10:20:55 AM 225.2 93.3
2/2/2019 10:20:56 AM 224.3 92.4
2/2/2019 10:20:57 AM 223.2 91.3
2/2/2019 10:20:58 AM 222.3 90.4
2/2/2019 10:20:59 AM 221.4 89.5
2/2/2019 10:21:00 AM 220.6 88.7
2/2/2019 10:21:01 AM 219.8 87.9
2/2/2019 10:21:02 AM 219.0 87.1
2/2/2019 10:21:03 AM 218.1 86.2
2/2/2019 10:21:04 AM 217.3 85.4
2/2/2019 10:21:05 AM 216.3 84.4
2/2/2019 10:21:06 AM 215.6 83.7
2/2/2019 10:21:07 AM 214.4 82.5
2/2/2019 10:21:08 AM 213.8 81.9
2/2/2019 10:21:09 AM 212.6 80.7
2/2/2019 10:21:10 AM 211.8 79.9
2/2/2019 10:21:11 AM 210.9 79.0
2/2/2019 10:21:12 AM 210.1 78.2
2/2/2019 10:21:13 AM 209.2 77.3
Page 47 of 452 August 2019
APPENDIX E15: SALT DILUTION GAUGING SUMMARY
Old Outfall-5 Test-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-5 TEST-1 Data Log
2/2/2019 10:21:14 AM 208.5 76.6
2/2/2019 10:21:15 AM 207.8 75.9
2/2/2019 10:21:16 AM 207.2 75.3
2/2/2019 10:21:17 AM 206.5 74.6
2/2/2019 10:21:18 AM 205.9 74.0
2/2/2019 10:21:19 AM 205.2 73.3
2/2/2019 10:21:20 AM 204.5 72.6
2/2/2019 10:21:21 AM 203.7 71.8
2/2/2019 10:21:22 AM 202.9 71.0
2/2/2019 10:21:23 AM 202.1 70.2
2/2/2019 10:21:24 AM 201.3 69.4
2/2/2019 10:21:25 AM 200.5 68.6
2/2/2019 10:21:26 AM 199.7 67.8
2/2/2019 10:21:27 AM 198.9 67.0
2/2/2019 10:21:28 AM 198.1 66.2
2/2/2019 10:21:29 AM 197.3 65.4
2/2/2019 10:21:30 AM 196.5 64.6
2/2/2019 10:21:31 AM 195.7 63.8
2/2/2019 10:21:32 AM 195.1 63.2
2/2/2019 10:21:33 AM 194.5 62.6
2/2/2019 10:21:34 AM 194.1 62.2
2/2/2019 10:21:35 AM 193.5 61.6
2/2/2019 10:21:36 AM 192.9 61.0
2/2/2019 10:21:37 AM 192.3 60.4
2/2/2019 10:21:38 AM 191.8 59.9
2/2/2019 10:21:39 AM 191.2 59.3
2/2/2019 10:21:40 AM 190.6 58.7
2/2/2019 10:21:41 AM 190.0 58.1
2/2/2019 10:21:42 AM 189.5 57.6
2/2/2019 10:21:43 AM 188.9 57.0
2/2/2019 10:21:44 AM 188.4 56.5
2/2/2019 10:21:45 AM 187.7 55.8
2/2/2019 10:21:46 AM 187.0 55.1
2/2/2019 10:21:47 AM 186.2 54.3
2/2/2019 10:21:48 AM 185.7 53.8
2/2/2019 10:21:49 AM 185.0 53.1
2/2/2019 10:21:50 AM 184.4 52.5
2/2/2019 10:21:51 AM 183.9 52.0
2/2/2019 10:21:52 AM 183.4 51.5
2/2/2019 10:21:53 AM 182.9 51.0
2/2/2019 10:21:54 AM 182.3 50.4
2/2/2019 10:21:55 AM 181.7 49.8
2/2/2019 10:21:56 AM 181.0 49.1
2/2/2019 10:21:57 AM 180.4 48.5
2/2/2019 10:21:58 AM 179.8 47.9
2/2/2019 10:21:59 AM 179.3 47.4
2/2/2019 10:22:00 AM 178.7 46.8
2/2/2019 10:22:01 AM 178.1 46.2
2/2/2019 10:22:02 AM 177.5 45.6
2/2/2019 10:22:03 AM 176.9 45.0
2/2/2019 10:22:04 AM 176.3 44.4
2/2/2019 10:22:05 AM 175.8 43.9
2/2/2019 10:22:06 AM 175.1 43.2
2/2/2019 10:22:07 AM 174.6 42.7
2/2/2019 10:22:08 AM 174.1 42.2
2/2/2019 10:22:09 AM 173.7 41.8
2/2/2019 10:22:10 AM 173.2 41.3
2/2/2019 10:22:11 AM 172.8 40.9
2/2/2019 10:22:12 AM 172.3 40.4
2/2/2019 10:22:13 AM 171.9 40.0
2/2/2019 10:22:14 AM 171.5 39.6
2/2/2019 10:22:15 AM 171.1 39.2
2/2/2019 10:22:16 AM 170.6 38.7
2/2/2019 10:22:17 AM 170.2 38.3
2/2/2019 10:22:18 AM 169.7 37.8
2/2/2019 10:22:19 AM 169.4 37.5
2/2/2019 10:22:20 AM 169.0 37.1
2/2/2019 10:22:21 AM 168.6 36.7
2/2/2019 10:22:22 AM 168.2 36.3
2/2/2019 10:22:23 AM 167.8 35.9
2/2/2019 10:22:24 AM 167.4 35.5
2/2/2019 10:22:25 AM 167.1 35.2
2/2/2019 10:22:26 AM 166.8 34.9
2/2/2019 10:22:27 AM 166.4 34.5
2/2/2019 10:22:28 AM 166.1 34.2
2/2/2019 10:22:29 AM 165.8 33.9
Page 48 of 452 August 2019
APPENDIX E15: SALT DILUTION GAUGING SUMMARY
Old Outfall-5 Test-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-5 TEST-1 Data Log
2/2/2019 10:22:30 AM 165.4 33.5
2/2/2019 10:22:31 AM 165.2 33.3
2/2/2019 10:22:32 AM 164.8 32.9
2/2/2019 10:22:33 AM 164.5 32.6
2/2/2019 10:22:34 AM 164.2 32.3
2/2/2019 10:22:35 AM 164.0 32.1
2/2/2019 10:22:36 AM 163.7 31.8
2/2/2019 10:22:37 AM 163.4 31.5
2/2/2019 10:22:38 AM 163.1 31.2
2/2/2019 10:22:39 AM 162.9 31.0
2/2/2019 10:22:40 AM 162.6 30.7
2/2/2019 10:22:41 AM 162.4 30.5
2/2/2019 10:22:42 AM 162.2 30.3
2/2/2019 10:22:43 AM 161.9 30.0
2/2/2019 10:22:44 AM 161.7 29.8
2/2/2019 10:22:45 AM 161.5 29.6
2/2/2019 10:22:46 AM 161.3 29.4
2/2/2019 10:22:47 AM 161.1 29.2
2/2/2019 10:22:48 AM 160.9 29.0
2/2/2019 10:22:49 AM 160.6 28.7
2/2/2019 10:22:50 AM 160.4 28.5
2/2/2019 10:22:51 AM 160.2 28.3
2/2/2019 10:22:52 AM 160.0 28.1
2/2/2019 10:22:53 AM 159.8 27.9
2/2/2019 10:22:54 AM 159.5 27.6
2/2/2019 10:22:55 AM 159.3 27.4
2/2/2019 10:22:56 AM 159.1 27.2
2/2/2019 10:22:57 AM 158.9 27.0
2/2/2019 10:22:58 AM 158.7 26.8
2/2/2019 10:22:59 AM 158.4 26.5
2/2/2019 10:23:00 AM 158.2 26.3
2/2/2019 10:23:01 AM 158.0 26.1
2/2/2019 10:23:02 AM 157.8 25.9
2/2/2019 10:23:03 AM 157.6 25.7
2/2/2019 10:23:04 AM 157.4 25.5
2/2/2019 10:23:05 AM 157.2 25.3
2/2/2019 10:23:06 AM 157.0 25.1
2/2/2019 10:23:07 AM 156.7 24.8
2/2/2019 10:23:08 AM 156.5 24.6
2/2/2019 10:23:09 AM 156.3 24.4
2/2/2019 10:23:10 AM 156.1 24.2
2/2/2019 10:23:11 AM 155.8 23.9
2/2/2019 10:23:12 AM 155.6 23.7
2/2/2019 10:23:13 AM 155.4 23.5
2/2/2019 10:23:14 AM 155.2 23.3
2/2/2019 10:23:15 AM 155.0 23.1
2/2/2019 10:23:16 AM 154.9 23.0
2/2/2019 10:23:17 AM 154.7 22.8
2/2/2019 10:23:18 AM 154.5 22.6
2/2/2019 10:23:19 AM 154.3 22.4
2/2/2019 10:23:20 AM 154.2 22.3
2/2/2019 10:23:21 AM 154.0 22.1
2/2/2019 10:23:22 AM 153.8 21.9
2/2/2019 10:23:23 AM 153.7 21.8
2/2/2019 10:23:24 AM 153.5 21.6
2/2/2019 10:23:25 AM 153.3 21.4
2/2/2019 10:23:26 AM 153.2 21.3
2/2/2019 10:23:27 AM 153.0 21.1
2/2/2019 10:23:28 AM 152.8 20.9
2/2/2019 10:23:29 AM 152.7 20.8
2/2/2019 10:23:30 AM 152.5 20.6
2/2/2019 10:23:31 AM 152.4 20.5
2/2/2019 10:23:32 AM 152.2 20.3
2/2/2019 10:23:33 AM 152.1 20.2
2/2/2019 10:23:34 AM 151.9 20.0
2/2/2019 10:23:35 AM 151.8 19.9
2/2/2019 10:23:36 AM 151.6 19.7
2/2/2019 10:23:37 AM 151.4 19.5
2/2/2019 10:23:38 AM 151.3 19.4
2/2/2019 10:23:39 AM 151.2 19.3
2/2/2019 10:23:40 AM 151.0 19.1
2/2/2019 10:23:41 AM 150.8 18.9
2/2/2019 10:23:42 AM 150.7 18.8
2/2/2019 10:23:43 AM 150.5 18.6
2/2/2019 10:23:44 AM 150.3 18.4
2/2/2019 10:23:45 AM 150.2 18.3
Page 49 of 452 August 2019
APPENDIX E15: SALT DILUTION GAUGING SUMMARY
Old Outfall-5 Test-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-5 TEST-1 Data Log
2/2/2019 10:23:46 AM 150.0 18.1
2/2/2019 10:23:47 AM 149.9 18.0
2/2/2019 10:23:48 AM 149.7 17.8
2/2/2019 10:23:49 AM 149.6 17.7
2/2/2019 10:23:50 AM 149.4 17.5
2/2/2019 10:23:51 AM 149.3 17.4
2/2/2019 10:23:52 AM 149.1 17.2
2/2/2019 10:23:53 AM 149.0 17.1
2/2/2019 10:23:54 AM 148.9 17.0
2/2/2019 10:23:55 AM 148.8 16.9
2/2/2019 10:23:56 AM 148.7 16.8
2/2/2019 10:23:57 AM 148.6 16.7
2/2/2019 10:23:58 AM 148.4 16.5
2/2/2019 10:23:59 AM 148.3 16.4
2/2/2019 10:24:00 AM 148.2 16.3
2/2/2019 10:24:01 AM 148.1 16.2
2/2/2019 10:24:02 AM 148.0 16.1
2/2/2019 10:24:03 AM 147.9 16.0
2/2/2019 10:24:04 AM 147.8 15.9
2/2/2019 10:24:05 AM 147.7 15.8
2/2/2019 10:24:06 AM 147.6 15.7
2/2/2019 10:24:07 AM 147.5 15.6
2/2/2019 10:24:08 AM 147.4 15.5
2/2/2019 10:24:09 AM 147.3 15.4
2/2/2019 10:24:10 AM 147.1 15.2
2/2/2019 10:24:11 AM 147.0 15.1
2/2/2019 10:24:12 AM 146.9 15.0
2/2/2019 10:24:13 AM 146.8 14.9
2/2/2019 10:24:14 AM 146.7 14.8
2/2/2019 10:24:15 AM 146.6 14.7
2/2/2019 10:24:16 AM 146.5 14.6
2/2/2019 10:24:17 AM 146.4 14.5
2/2/2019 10:24:18 AM 146.2 14.3
2/2/2019 10:24:19 AM 146.2 14.3
2/2/2019 10:24:20 AM 146.1 14.2
Page 50 of 452 August 2019
APPENDIX E15: SALT DILUTION GAUGING SUMMARY
Old Outfall-5 Test-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
OLDOF-5 TEST-1 944
OLDOF-5 TEST-1 946
OLDOF-5 TEST-1 947
OLDOF-5 TEST-1 948
Location EC Reading
(µS/cms)
OLDOF-5 TEST-1 205.3
OLDOF-5 TEST-1 1,752.0
OLDOF-5 TEST-1 15,375.0
OLDOF-5 TEST-1 191,178.0
q 300,100
K 1.9081
8.87
140.86
Notes:
°C degrees celsius
mg/L miligrams per liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Calculated Flow Rate Q L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement Part
2: Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8, no. 1,
2004, pp. 11–15.
Integral of Conductivity Data Curve SUM:Δt(ECt-
ECbkg)64,527.20 (s) . (µS/cms)
1,000 18.1
10,000 18.3
100,000 17.6
Table E4 OLDOF-5 TEST-1 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
100 17.3
Average (pre-test)131.9 (µS/cms)
Average (post-test)-(µS/cms)
Table E3 OLDOF-5 TEST-1 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
(mg/L)(°C)
129.6 -
130.8 -
Geometric Mean 130.2 (µS/cms)
(µS/cms)(°C)
129.5 -
131 -
Table E2 OLDOF-5 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 51 of 452 August 2019
APPENDIX E16: SALT DILUTION GAUGING SUMMARY
Old Outfall-5 Test-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/2/2019 10:29:21 AM 134.5 -
2/2/2019 10:29:22 AM 134.5 -
2/2/2019 10:29:23 AM 134.4 -
2/2/2019 10:29:24 AM 134.4 -
2/2/2019 10:29:25 AM 134.4 -
2/2/2019 10:29:26 AM 134.4 -
2/2/2019 10:29:27 AM 134.4 -
2/2/2019 10:29:28 AM 134.4 -
2/2/2019 10:29:29 AM 134.4 -
2/2/2019 10:29:30 AM 134.3 -
2/2/2019 10:29:31 AM 134.3 -
2/2/2019 10:29:32 AM 134.3 -
2/2/2019 10:29:33 AM 134.3 -
2/2/2019 10:29:34 AM 134.3 -
2/2/2019 10:29:35 AM 134.3 -
2/2/2019 10:29:36 AM 134.3 -
2/2/2019 10:29:37 AM 134.2 -
2/2/2019 10:29:38 AM 134.2 -
2/2/2019 10:29:39 AM 134.2 -
2/2/2019 10:29:40 AM 134.2 -
2/2/2019 10:29:41 AM 134.2 -
2/2/2019 10:29:42 AM 134.1 -
2/2/2019 10:29:43 AM 134.1 -
2/2/2019 10:29:44 AM 134.1 -
2/2/2019 10:29:45 AM 134.1 -
2/2/2019 10:29:46 AM 134.1 -
2/2/2019 10:29:47 AM 134.0 -
2/2/2019 10:29:48 AM 134.0 -
2/2/2019 10:29:49 AM 134.0 -
2/2/2019 10:29:50 AM 134.0 -
2/2/2019 10:29:51 AM 134.0 -
2/2/2019 10:29:52 AM 134.0 -
2/2/2019 10:29:53 AM 134.0 -
2/2/2019 10:29:54 AM 133.9 -
2/2/2019 10:29:55 AM 133.9 -
2/2/2019 10:29:56 AM 133.9 -
2/2/2019 10:29:57 AM 133.9 -
2/2/2019 10:29:58 AM 133.9 -
2/2/2019 10:29:59 AM 133.9 -
2/2/2019 10:30:00 AM 133.9 -
2/2/2019 10:30:01 AM 133.9 -
2/2/2019 10:30:02 AM 133.9 -
2/2/2019 10:30:03 AM 133.8 -
2/2/2019 10:30:04 AM 133.8 -
2/2/2019 10:30:05 AM 133.8 -
2/2/2019 10:30:06 AM 133.8 -
2/2/2019 10:30:07 AM 133.8 -
2/2/2019 10:30:08 AM 133.8 -
2/2/2019 10:30:09 AM 133.7 -
2/2/2019 10:30:10 AM 133.7 -
2/2/2019 10:30:11 AM 133.7 -
2/2/2019 10:30:12 AM 133.7 -
2/2/2019 10:30:13 AM 133.7 -
2/2/2019 10:30:14 AM 133.7 -
2/2/2019 10:30:15 AM 133.7 -
2/2/2019 10:30:16 AM 133.7 -
2/2/2019 10:30:17 AM 133.7 -
2/2/2019 10:30:18 AM 133.7 -
2/2/2019 10:30:19 AM 133.7 -
2/2/2019 10:30:20 AM 133.7 -
2/2/2019 10:30:21 AM 133.6 -
2/2/2019 10:30:22 AM 133.6 -
2/2/2019 10:30:23 AM 133.6 -
2/2/2019 10:30:24 AM 133.6 -
2/2/2019 10:30:25 AM 133.6 -
2/2/2019 10:30:26 AM 133.6 -
2/2/2019 10:30:27 AM 133.6 -
2/2/2019 10:30:28 AM 133.6 -
2/2/2019 10:30:29 AM 133.6 -
2/2/2019 10:30:30 AM 133.6 -
Table E1 OLDOF-5 TEST-2 Data Log
Page 52 of 452 August 2019
APPENDIX E16: SALT DILUTION GAUGING SUMMARY
Old Outfall-5 Test-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-5 TEST-2 Data Log
2/2/2019 10:30:31 AM 133.5 -
2/2/2019 10:30:32 AM 133.5 -
2/2/2019 10:30:33 AM 133.5 -
2/2/2019 10:30:34 AM 133.5 -
2/2/2019 10:30:35 AM 133.5 -
2/2/2019 10:30:36 AM 133.5 -
2/2/2019 10:30:37 AM 133.5 -
2/2/2019 10:30:38 AM 133.5 -
2/2/2019 10:30:39 AM 133.6 -
2/2/2019 10:30:40 AM 133.6 -
2/2/2019 10:30:41 AM 133.8 -
2/2/2019 10:30:42 AM 133.9 -
2/2/2019 10:30:43 AM 134.3 -
2/2/2019 10:30:44 AM 134.7 -
2/2/2019 10:30:45 AM 135.3 -
2/2/2019 10:30:46 AM 136.2 -
2/2/2019 10:30:47 AM 137.6 3.6
2/2/2019 10:30:48 AM 139.1 5.1
2/2/2019 10:30:49 AM 141.4 7.4
2/2/2019 10:30:50 AM 144.2 10.2
2/2/2019 10:30:51 AM 196.2 62.2
2/2/2019 10:30:52 AM 206.8 72.8
2/2/2019 10:30:53 AM 223.5 89.5
2/2/2019 10:30:54 AM 232.9 98.9
2/2/2019 10:30:55 AM 242.0 108.0
2/2/2019 10:30:56 AM 251.1 117.1
2/2/2019 10:30:57 AM 264.1 130.1
2/2/2019 10:30:58 AM 321.5 187.5
2/2/2019 10:30:59 AM 344.0 210.0
2/2/2019 10:31:00 AM 369.6 235.6
2/2/2019 10:31:01 AM 389.9 255.9
2/2/2019 10:31:02 AM 399.7 265.7
2/2/2019 10:31:03 AM 413.6 279.6
2/2/2019 10:31:04 AM 428.9 294.9
2/2/2019 10:31:05 AM 492.9 358.9
2/2/2019 10:31:06 AM 528.0 394.0
2/2/2019 10:31:07 AM 566.0 432.0
2/2/2019 10:31:08 AM 577.2 443.2
2/2/2019 10:31:09 AM 585.6 451.6
2/2/2019 10:31:10 AM 594.9 460.9
2/2/2019 10:31:11 AM 603.3 469.3
2/2/2019 10:31:12 AM 664.0 530.0
2/2/2019 10:31:13 AM 676.1 542.1
2/2/2019 10:31:14 AM 688.1 554.1
2/2/2019 10:31:15 AM 696.4 562.4
2/2/2019 10:31:16 AM 702.8 568.8
2/2/2019 10:31:17 AM 708.7 574.7
2/2/2019 10:31:18 AM 712.4 578.4
2/2/2019 10:31:19 AM 716.8 582.8
2/2/2019 10:31:20 AM 719.7 585.7
2/2/2019 10:31:21 AM 722.3 588.3
2/2/2019 10:31:22 AM 726.0 592.0
2/2/2019 10:31:23 AM 727.7 593.7
2/2/2019 10:31:24 AM 729.0 595.0
2/2/2019 10:31:25 AM 730.1 596.1
2/2/2019 10:31:26 AM 731.3 597.3
2/2/2019 10:31:27 AM 731.9 597.9
2/2/2019 10:31:28 AM 732.9 598.9
2/2/2019 10:31:29 AM 734.8 600.8
2/2/2019 10:31:30 AM 735.8 601.8
2/2/2019 10:31:31 AM 736.0 602.0
2/2/2019 10:31:32 AM 735.2 601.2
2/2/2019 10:31:33 AM 733.6 599.6
2/2/2019 10:31:34 AM 731.3 597.3
2/2/2019 10:31:35 AM 728.3 594.3
2/2/2019 10:31:36 AM 724.2 590.2
2/2/2019 10:31:37 AM 720.4 586.4
2/2/2019 10:31:38 AM 715.6 581.6
2/2/2019 10:31:39 AM 666.2 532.2
2/2/2019 10:31:40 AM 656.5 522.5
2/2/2019 10:31:41 AM 652.6 518.6
2/2/2019 10:31:42 AM 651.5 517.5
2/2/2019 10:31:43 AM 649.0 515.0
2/2/2019 10:31:44 AM 643.7 509.7
2/2/2019 10:31:45 AM 639.0 505.0
Page 53 of 452 August 2019
APPENDIX E16: SALT DILUTION GAUGING SUMMARY
Old Outfall-5 Test-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-5 TEST-2 Data Log
2/2/2019 10:31:46 AM 633.9 499.9
2/2/2019 10:31:47 AM 629.9 495.9
2/2/2019 10:31:48 AM 626.1 492.1
2/2/2019 10:31:49 AM 622.7 488.7
2/2/2019 10:31:50 AM 618.7 484.7
2/2/2019 10:31:51 AM 614.9 480.9
2/2/2019 10:31:52 AM 610.7 476.7
2/2/2019 10:31:53 AM 562.7 428.7
2/2/2019 10:31:54 AM 556.5 422.5
2/2/2019 10:31:55 AM 553.7 419.7
2/2/2019 10:31:56 AM 552.5 418.5
2/2/2019 10:31:57 AM 549.0 415.0
2/2/2019 10:31:58 AM 545.2 411.2
2/2/2019 10:31:59 AM 540.6 406.6
2/2/2019 10:32:00 AM 537.3 403.3
2/2/2019 10:32:01 AM 533.9 399.9
2/2/2019 10:32:02 AM 531.0 397.0
2/2/2019 10:32:03 AM 528.2 394.2
2/2/2019 10:32:04 AM 525.8 391.8
2/2/2019 10:32:05 AM 522.7 388.7
2/2/2019 10:32:06 AM 519.7 385.7
2/2/2019 10:32:07 AM 516.5 382.5
2/2/2019 10:32:08 AM 513.8 379.8
2/2/2019 10:32:09 AM 508.6 374.6
2/2/2019 10:32:10 AM 503.0 369.0
2/2/2019 10:32:11 AM 497.2 363.2
2/2/2019 10:32:12 AM 492.2 358.2
2/2/2019 10:32:13 AM 486.3 352.3
2/2/2019 10:32:14 AM 481.3 347.3
2/2/2019 10:32:15 AM 475.7 341.7
2/2/2019 10:32:16 AM 470.8 336.8
2/2/2019 10:32:17 AM 464.9 330.9
2/2/2019 10:32:18 AM 460.2 326.2
2/2/2019 10:32:19 AM 455.1 321.1
2/2/2019 10:32:20 AM 450.5 316.5
2/2/2019 10:32:21 AM 445.2 311.2
2/2/2019 10:32:22 AM 440.9 306.9
2/2/2019 10:32:23 AM 436.1 302.1
2/2/2019 10:32:24 AM 431.8 297.8
2/2/2019 10:32:25 AM 427.1 293.1
2/2/2019 10:32:26 AM 423.3 289.3
2/2/2019 10:32:27 AM 418.8 284.8
2/2/2019 10:32:28 AM 414.8 280.8
2/2/2019 10:32:29 AM 410.4 276.4
2/2/2019 10:32:30 AM 406.8 272.8
2/2/2019 10:32:31 AM 402.8 268.8
2/2/2019 10:32:32 AM 399.3 265.3
2/2/2019 10:32:33 AM 395.5 261.5
2/2/2019 10:32:34 AM 392.2 258.2
2/2/2019 10:32:35 AM 388.3 254.3
2/2/2019 10:32:36 AM 384.3 250.3
2/2/2019 10:32:37 AM 380.9 246.9
2/2/2019 10:32:38 AM 376.9 242.9
2/2/2019 10:32:39 AM 373.4 239.4
2/2/2019 10:32:40 AM 369.6 235.6
2/2/2019 10:32:41 AM 366.5 232.5
2/2/2019 10:32:42 AM 362.9 228.9
2/2/2019 10:32:43 AM 359.9 225.9
2/2/2019 10:32:44 AM 356.4 222.4
2/2/2019 10:32:45 AM 353.5 219.5
2/2/2019 10:32:46 AM 350.3 216.3
2/2/2019 10:32:47 AM 347.5 213.5
2/2/2019 10:32:48 AM 344.3 210.3
2/2/2019 10:32:49 AM 341.6 207.6
2/2/2019 10:32:50 AM 338.7 204.7
2/2/2019 10:32:51 AM 336.3 202.3
2/2/2019 10:32:52 AM 333.7 199.7
2/2/2019 10:32:53 AM 331.3 197.3
2/2/2019 10:32:54 AM 328.6 194.6
2/2/2019 10:32:55 AM 326.2 192.2
2/2/2019 10:32:56 AM 323.4 189.4
2/2/2019 10:32:57 AM 321.1 187.1
2/2/2019 10:32:58 AM 318.3 184.3
2/2/2019 10:32:59 AM 316.1 182.1
2/2/2019 10:33:00 AM 313.6 179.6
2/2/2019 10:33:01 AM 311.5 177.5
Page 54 of 452 August 2019
APPENDIX E16: SALT DILUTION GAUGING SUMMARY
Old Outfall-5 Test-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-5 TEST-2 Data Log
2/2/2019 10:33:02 AM 309.2 175.2
2/2/2019 10:33:03 AM 307.0 173.0
2/2/2019 10:33:04 AM 304.7 170.7
2/2/2019 10:33:05 AM 302.6 168.6
2/2/2019 10:33:06 AM 300.2 166.2
2/2/2019 10:33:07 AM 298.2 164.2
2/2/2019 10:33:08 AM 295.8 161.8
2/2/2019 10:33:09 AM 293.9 159.9
2/2/2019 10:33:10 AM 291.8 157.8
2/2/2019 10:33:11 AM 289.9 155.9
2/2/2019 10:33:12 AM 287.6 153.6
2/2/2019 10:33:13 AM 285.7 151.7
2/2/2019 10:33:14 AM 283.6 149.6
2/2/2019 10:33:15 AM 281.8 147.8
2/2/2019 10:33:16 AM 279.9 145.9
2/2/2019 10:33:17 AM 278.1 144.1
2/2/2019 10:33:18 AM 276.2 142.2
2/2/2019 10:33:19 AM 274.2 140.2
2/2/2019 10:33:20 AM 272.7 138.7
2/2/2019 10:33:21 AM 270.9 136.9
2/2/2019 10:33:22 AM 269.4 135.4
2/2/2019 10:33:23 AM 267.6 133.6
2/2/2019 10:33:24 AM 266.1 132.1
2/2/2019 10:33:25 AM 264.5 130.5
2/2/2019 10:33:26 AM 263.2 129.2
2/2/2019 10:33:27 AM 261.6 127.6
2/2/2019 10:33:28 AM 260.1 126.1
2/2/2019 10:33:29 AM 258.4 124.4
2/2/2019 10:33:30 AM 256.9 122.9
2/2/2019 10:33:31 AM 255.4 121.4
2/2/2019 10:33:32 AM 254.2 120.2
2/2/2019 10:33:33 AM 252.7 118.7
2/2/2019 10:33:34 AM 251.4 117.4
2/2/2019 10:33:35 AM 250.1 116.1
2/2/2019 10:33:36 AM 248.8 114.8
2/2/2019 10:33:37 AM 247.4 113.4
2/2/2019 10:33:38 AM 246.1 112.1
2/2/2019 10:33:39 AM 244.6 110.6
2/2/2019 10:33:40 AM 243.4 109.4
2/2/2019 10:33:41 AM 242.1 108.1
2/2/2019 10:33:42 AM 241.0 107.0
2/2/2019 10:33:43 AM 239.8 105.8
2/2/2019 10:33:44 AM 238.7 104.7
2/2/2019 10:33:45 AM 237.4 103.4
2/2/2019 10:33:46 AM 236.2 102.2
2/2/2019 10:33:47 AM 234.9 100.9
2/2/2019 10:33:48 AM 233.8 99.8
2/2/2019 10:33:49 AM 232.6 98.6
2/2/2019 10:33:50 AM 231.5 97.5
2/2/2019 10:33:51 AM 230.3 96.3
2/2/2019 10:33:52 AM 229.4 95.4
2/2/2019 10:33:53 AM 228.2 94.2
2/2/2019 10:33:54 AM 227.1 93.1
2/2/2019 10:33:55 AM 226.0 92.0
2/2/2019 10:33:56 AM 225.0 91.0
2/2/2019 10:33:57 AM 223.6 89.6
2/2/2019 10:33:58 AM 222.9 88.9
2/2/2019 10:33:59 AM 221.8 87.8
2/2/2019 10:34:00 AM 220.6 86.6
2/2/2019 10:34:01 AM 219.5 85.5
2/2/2019 10:34:02 AM 218.5 84.5
2/2/2019 10:34:03 AM 217.4 83.4
2/2/2019 10:34:04 AM 216.5 82.5
2/2/2019 10:34:05 AM 215.5 81.5
2/2/2019 10:34:06 AM 214.7 80.7
2/2/2019 10:34:07 AM 213.8 79.8
2/2/2019 10:34:08 AM 212.9 78.9
2/2/2019 10:34:09 AM 212.0 78.0
2/2/2019 10:34:10 AM 211.3 77.3
2/2/2019 10:34:11 AM 210.6 76.6
2/2/2019 10:34:12 AM 209.8 75.8
2/2/2019 10:34:13 AM 208.8 74.8
2/2/2019 10:34:14 AM 208.2 74.2
2/2/2019 10:34:15 AM 207.2 73.2
2/2/2019 10:34:16 AM 206.4 72.4
2/2/2019 10:34:17 AM 205.6 71.6
Page 55 of 452 August 2019
APPENDIX E16: SALT DILUTION GAUGING SUMMARY
Old Outfall-5 Test-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-5 TEST-2 Data Log
2/2/2019 10:34:18 AM 204.7 70.7
2/2/2019 10:34:19 AM 203.9 69.9
2/2/2019 10:34:20 AM 203.1 69.1
2/2/2019 10:34:21 AM 202.3 68.3
2/2/2019 10:34:22 AM 201.4 67.4
2/2/2019 10:34:23 AM 200.6 66.6
2/2/2019 10:34:24 AM 199.8 65.8
2/2/2019 10:34:25 AM 199.1 65.1
2/2/2019 10:34:26 AM 198.3 64.3
2/2/2019 10:34:27 AM 197.6 63.6
2/2/2019 10:34:28 AM 196.9 62.9
2/2/2019 10:34:29 AM 196.3 62.3
2/2/2019 10:34:30 AM 195.5 61.5
2/2/2019 10:34:31 AM 194.9 60.9
2/2/2019 10:34:32 AM 194.2 60.2
2/2/2019 10:34:33 AM 193.6 59.6
2/2/2019 10:34:34 AM 193.0 59.0
2/2/2019 10:34:35 AM 192.5 58.5
2/2/2019 10:34:36 AM 191.8 57.8
2/2/2019 10:34:37 AM 191.2 57.2
2/2/2019 10:34:38 AM 190.5 56.5
2/2/2019 10:34:39 AM 190.0 56.0
2/2/2019 10:34:40 AM 189.3 55.3
2/2/2019 10:34:41 AM 188.8 54.8
2/2/2019 10:34:42 AM 188.2 54.2
2/2/2019 10:34:43 AM 187.7 53.7
2/2/2019 10:34:44 AM 187.2 53.2
2/2/2019 10:34:45 AM 186.7 52.7
2/2/2019 10:34:46 AM 186.2 52.2
2/2/2019 10:34:47 AM 185.6 51.6
2/2/2019 10:34:48 AM 184.9 50.9
2/2/2019 10:34:49 AM 184.4 50.4
2/2/2019 10:34:50 AM 183.8 49.8
2/2/2019 10:34:51 AM 183.4 49.4
2/2/2019 10:34:52 AM 182.8 48.8
2/2/2019 10:34:53 AM 182.3 48.3
2/2/2019 10:34:54 AM 181.9 47.9
2/2/2019 10:34:55 AM 181.4 47.4
2/2/2019 10:34:56 AM 180.9 46.9
2/2/2019 10:34:57 AM 180.4 46.4
2/2/2019 10:34:58 AM 179.9 45.9
2/2/2019 10:34:59 AM 179.4 45.4
2/2/2019 10:35:00 AM 179.0 45.0
2/2/2019 10:35:01 AM 178.6 44.6
2/2/2019 10:35:02 AM 178.2 44.2
2/2/2019 10:35:03 AM 177.7 43.7
2/2/2019 10:35:04 AM 177.3 43.3
2/2/2019 10:35:05 AM 176.8 42.8
2/2/2019 10:35:06 AM 176.4 42.4
2/2/2019 10:35:07 AM 175.9 41.9
2/2/2019 10:35:08 AM 175.4 41.4
2/2/2019 10:35:09 AM 175.0 41.0
2/2/2019 10:35:10 AM 174.6 40.6
2/2/2019 10:35:11 AM 174.2 40.2
2/2/2019 10:35:12 AM 173.8 39.8
2/2/2019 10:35:13 AM 173.4 39.4
2/2/2019 10:35:14 AM 173.0 39.0
2/2/2019 10:35:15 AM 172.6 38.6
2/2/2019 10:35:16 AM 172.3 38.3
2/2/2019 10:35:17 AM 171.9 37.9
2/2/2019 10:35:18 AM 171.5 37.5
2/2/2019 10:35:19 AM 171.1 37.1
2/2/2019 10:35:20 AM 170.7 36.7
2/2/2019 10:35:21 AM 170.3 36.3
2/2/2019 10:35:22 AM 170.0 36.0
2/2/2019 10:35:23 AM 169.6 35.6
2/2/2019 10:35:24 AM 169.3 35.3
2/2/2019 10:35:25 AM 168.9 34.9
2/2/2019 10:35:26 AM 168.6 34.6
2/2/2019 10:35:27 AM 168.3 34.3
2/2/2019 10:35:28 AM 168.0 34.0
2/2/2019 10:35:29 AM 167.7 33.7
2/2/2019 10:35:30 AM 167.5 33.5
2/2/2019 10:35:31 AM 167.3 33.3
2/2/2019 10:35:32 AM 167.1 33.1
2/2/2019 10:35:33 AM 166.8 32.8
Page 56 of 452 August 2019
APPENDIX E16: SALT DILUTION GAUGING SUMMARY
Old Outfall-5 Test-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-5 TEST-2 Data Log
2/2/2019 10:35:34 AM 166.6 32.6
2/2/2019 10:35:35 AM 166.3 32.3
2/2/2019 10:35:36 AM 166.1 32.1
2/2/2019 10:35:37 AM 165.8 31.8
2/2/2019 10:35:38 AM 165.5 31.5
2/2/2019 10:35:39 AM 165.3 31.3
2/2/2019 10:35:40 AM 165.0 31.0
2/2/2019 10:35:41 AM 164.7 30.7
2/2/2019 10:35:42 AM 164.4 30.4
2/2/2019 10:35:43 AM 164.1 30.1
2/2/2019 10:35:44 AM 163.7 29.7
2/2/2019 10:35:45 AM 163.5 29.5
2/2/2019 10:35:46 AM 163.2 29.2
2/2/2019 10:35:47 AM 162.9 28.9
2/2/2019 10:35:48 AM 162.6 28.6
2/2/2019 10:35:49 AM 162.4 28.4
2/2/2019 10:35:50 AM 162.1 28.1
2/2/2019 10:35:51 AM 161.9 27.9
2/2/2019 10:35:52 AM 161.6 27.6
2/2/2019 10:35:53 AM 161.4 27.4
2/2/2019 10:35:54 AM 161.1 27.1
2/2/2019 10:35:55 AM 160.9 26.9
2/2/2019 10:35:56 AM 160.7 26.7
2/2/2019 10:35:57 AM 160.5 26.5
2/2/2019 10:35:58 AM 160.2 26.2
2/2/2019 10:35:59 AM 160.0 26.0
2/2/2019 10:36:00 AM 159.8 25.8
2/2/2019 10:36:01 AM 159.5 25.5
2/2/2019 10:36:02 AM 159.3 25.3
2/2/2019 10:36:03 AM 159.1 25.1
2/2/2019 10:36:04 AM 158.9 24.9
2/2/2019 10:36:05 AM 158.7 24.7
2/2/2019 10:36:06 AM 158.4 24.4
2/2/2019 10:36:07 AM 158.2 24.2
2/2/2019 10:36:08 AM 158.0 24.0
2/2/2019 10:36:09 AM 157.8 23.8
2/2/2019 10:36:10 AM 157.6 23.6
2/2/2019 10:36:11 AM 157.4 23.4
2/2/2019 10:36:12 AM 157.2 23.2
2/2/2019 10:36:13 AM 157.0 23.0
2/2/2019 10:36:14 AM 156.8 22.8
2/2/2019 10:36:15 AM 156.6 22.6
2/2/2019 10:36:16 AM 156.4 22.4
2/2/2019 10:36:17 AM 156.2 22.2
2/2/2019 10:36:18 AM 156.1 22.1
2/2/2019 10:36:19 AM 155.9 21.9
2/2/2019 10:36:20 AM 155.7 21.7
2/2/2019 10:36:21 AM 155.5 21.5
2/2/2019 10:36:22 AM 155.3 21.3
2/2/2019 10:36:23 AM 155.1 21.1
2/2/2019 10:36:24 AM 154.9 20.9
2/2/2019 10:36:25 AM 154.8 20.8
2/2/2019 10:36:26 AM 154.6 20.6
2/2/2019 10:36:27 AM 154.4 20.4
2/2/2019 10:36:28 AM 154.3 20.3
2/2/2019 10:36:29 AM 154.1 20.1
2/2/2019 10:36:30 AM 153.9 19.9
2/2/2019 10:36:31 AM 153.7 19.7
2/2/2019 10:36:32 AM 153.6 19.6
2/2/2019 10:36:33 AM 153.5 19.5
2/2/2019 10:36:34 AM 153.3 19.3
2/2/2019 10:36:35 AM 153.2 19.2
2/2/2019 10:36:36 AM 153.1 19.1
2/2/2019 10:36:37 AM 152.9 18.9
2/2/2019 10:36:38 AM 152.8 18.8
2/2/2019 10:36:39 AM 152.7 18.7
2/2/2019 10:36:40 AM 152.6 18.6
2/2/2019 10:36:41 AM 152.4 18.4
2/2/2019 10:36:42 AM 152.3 18.3
2/2/2019 10:36:43 AM 152.2 18.2
2/2/2019 10:36:44 AM 152.1 18.1
2/2/2019 10:36:45 AM 151.9 17.9
2/2/2019 10:36:46 AM 151.8 17.8
2/2/2019 10:36:47 AM 151.6 17.6
2/2/2019 10:36:48 AM 151.5 17.5
2/2/2019 10:36:49 AM 151.3 17.3
Page 57 of 452 August 2019
APPENDIX E16: SALT DILUTION GAUGING SUMMARY
Old Outfall-5 Test-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-5 TEST-2 Data Log
2/2/2019 10:36:50 AM 151.1 17.1
2/2/2019 10:36:51 AM 151.0 17.0
2/2/2019 10:36:52 AM 150.8 16.8
2/2/2019 10:36:53 AM 150.6 16.6
2/2/2019 10:36:54 AM 150.4 16.4
2/2/2019 10:36:55 AM 150.2 16.2
2/2/2019 10:36:56 AM 150.1 16.1
2/2/2019 10:36:57 AM 150.0 16.0
2/2/2019 10:36:58 AM 149.8 15.8
2/2/2019 10:36:59 AM 149.7 15.7
2/2/2019 10:37:00 AM 149.5 15.5
2/2/2019 10:37:01 AM 149.4 15.4
2/2/2019 10:37:02 AM 149.2 15.2
2/2/2019 10:37:03 AM 149.1 15.1
2/2/2019 10:37:04 AM 149.0 15.0
2/2/2019 10:37:05 AM 148.9 14.9
2/2/2019 10:37:06 AM 148.9 14.9
2/2/2019 10:37:07 AM 148.8 14.8
2/2/2019 10:37:08 AM 148.7 14.7
2/2/2019 10:37:09 AM 148.6 14.6
2/2/2019 10:37:10 AM 148.5 14.5
2/2/2019 10:37:11 AM 148.4 14.4
2/2/2019 10:37:12 AM 148.3 14.3
2/2/2019 10:37:13 AM 148.2 14.2
2/2/2019 10:37:14 AM 148.1 14.1
2/2/2019 10:37:15 AM 148.0 14.0
2/2/2019 10:37:16 AM 147.9 13.9
2/2/2019 10:37:17 AM 147.8 13.8
2/2/2019 10:37:18 AM 147.7 13.7
2/2/2019 10:37:19 AM 147.6 13.6
2/2/2019 10:37:20 AM 147.5 13.5
2/2/2019 10:37:21 AM 147.4 13.4
2/2/2019 10:37:22 AM 147.3 13.3
2/2/2019 10:37:23 AM 147.2 13.2
2/2/2019 10:37:24 AM 147.1 13.1
2/2/2019 10:37:25 AM 147.0 13.0
2/2/2019 10:37:26 AM 146.9 12.9
2/2/2019 10:37:27 AM 146.8 12.8
2/2/2019 10:37:28 AM 146.7 12.7
2/2/2019 10:37:29 AM 146.6 12.6
2/2/2019 10:37:30 AM 146.5 12.5
2/2/2019 10:37:31 AM 146.4 12.4
2/2/2019 10:37:32 AM 146.3 12.3
2/2/2019 10:37:33 AM 146.3 12.3
2/2/2019 10:37:34 AM 146.2 12.2
2/2/2019 10:37:35 AM 146.1 12.1
2/2/2019 10:37:36 AM 146.0 12.0
2/2/2019 10:37:37 AM 145.9 11.9
2/2/2019 10:37:38 AM 145.8 11.8
2/2/2019 10:37:39 AM 145.7 11.7
2/2/2019 10:37:40 AM 145.6 11.6
2/2/2019 10:37:41 AM 145.5 11.5
2/2/2019 10:37:42 AM 145.4 11.4
2/2/2019 10:37:43 AM 145.4 11.4
2/2/2019 10:37:44 AM 145.3 11.3
2/2/2019 10:37:45 AM 145.2 11.2
2/2/2019 10:37:46 AM 145.1 11.1
2/2/2019 10:37:47 AM 145.0 11.0
2/2/2019 10:37:48 AM 144.9 10.9
2/2/2019 10:37:49 AM 144.8 10.8
2/2/2019 10:37:50 AM 144.8 10.8
2/2/2019 10:37:51 AM 144.7 10.7
2/2/2019 10:37:52 AM 144.6 10.6
2/2/2019 10:37:53 AM 144.5 10.5
2/2/2019 10:37:54 AM 144.4 10.4
2/2/2019 10:37:55 AM 144.3 10.3
2/2/2019 10:37:56 AM 144.3 10.3
2/2/2019 10:37:57 AM 144.2 10.2
2/2/2019 10:37:58 AM 144.1 10.1
2/2/2019 10:37:59 AM 144.0 10.0
2/2/2019 10:38:00 AM 144.0 10.0
2/2/2019 10:38:01 AM 143.9 9.9
2/2/2019 10:38:02 AM 143.8 9.8
2/2/2019 10:38:03 AM 143.7 9.7
2/2/2019 10:38:04 AM 143.6 9.6
2/2/2019 10:38:05 AM 143.6 9.6
Page 58 of 452 August 2019
APPENDIX E16: SALT DILUTION GAUGING SUMMARY
Old Outfall-5 Test-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-5 TEST-2 Data Log
2/2/2019 10:38:06 AM 143.5 9.5
2/2/2019 10:38:07 AM 143.4 9.4
2/2/2019 10:38:08 AM 143.3 9.3
2/2/2019 10:38:09 AM 143.2 9.2
2/2/2019 10:38:10 AM 143.1 9.1
2/2/2019 10:38:11 AM 143.1 9.1
2/2/2019 10:38:12 AM 143.0 9.0
Page 59 of 452 August 2019
APPENDIX E16: SALT DILUTION GAUGING SUMMARY
Old Outfall-5 Test-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
OLDOF-5 TEST-2 944
OLDOF-5 TEST-2 946
OLDOF-5 TEST-2 947
OLDOF-5 TEST-2 948
Location EC Reading
(µS/cms)
OLDOF-5 TEST-2 205.3
OLDOF-5 TEST-2 1,752.0
OLDOF-5 TEST-2 15,375.0
OLDOF-5 TEST-2 191,178.0
q 300,700
K 1.9081
8.99
142.69
Notes:
°C degrees celsius
mg/L miligrams per liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Calculated Flow Rate Q L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement Part
2: Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8, no. 1,
2004, pp. 11–15.
(mg/L)(°C)
100 17.3
1,000 18.1
Integral of Conductivity Data Curve SUM:Δt(ECt-
ECbkg)63,825.34 (s) . (µS/cms)
10,000 18.3
100,000 17.6
Table E4 OLDOF-5 TEST-2 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Temperature
Average (pre-test)134.0 (µS/cms)
129.6 -
130.8 -
Geometric Mean 130.2 (µS/cms)
Average (post-test)-(µS/cms)
Table E3 OLDOF-5 TEST-2 YSI Salt Dilution Calibration Data
Calibration Concentration
(µS/cms)(°C)
129.5 -
131 -
Table E2 OLDOF-5 TEST-2 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 60 of 452 August 2019
APPENDIX E17: SALT DILUTION GAUGING SUMMARY
Old Outfall-TR-1 Test-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/2/2019 4:00:54 PM 171.9 -
2/2/2019 4:00:55 PM 171.8 -
2/2/2019 4:00:56 PM 171.7 -
2/2/2019 4:00:57 PM 171.7 -
2/2/2019 4:00:58 PM 171.6 -
2/2/2019 4:00:59 PM 171.5 -
2/2/2019 4:01:00 PM 171.4 -
2/2/2019 4:01:01 PM 171.3 -
2/2/2019 4:01:02 PM 171.2 -
2/2/2019 4:01:03 PM 171.1 -
2/2/2019 4:01:04 PM 171.0 -
2/2/2019 4:01:05 PM 170.9 -
2/2/2019 4:01:06 PM 170.9 -
2/2/2019 4:01:07 PM 170.8 -
2/2/2019 4:01:08 PM 170.8 -
2/2/2019 4:01:09 PM 170.7 -
2/2/2019 4:01:10 PM 170.7 -
2/2/2019 4:01:11 PM 170.7 -
2/2/2019 4:01:12 PM 170.7 -
2/2/2019 4:01:13 PM 170.8 -
2/2/2019 4:01:14 PM 170.8 -
2/2/2019 4:01:15 PM 170.8 -
2/2/2019 4:01:16 PM 170.8 -
2/2/2019 4:01:17 PM 170.9 -
2/2/2019 4:01:18 PM 170.9 -
2/2/2019 4:01:19 PM 170.9 -
2/2/2019 4:01:20 PM 170.9 -
2/2/2019 4:01:21 PM 170.9 -
2/2/2019 4:01:22 PM 170.9 -
2/2/2019 4:01:23 PM 170.8 -
2/2/2019 4:01:24 PM 170.8 -
2/2/2019 4:01:25 PM 170.9 -
2/2/2019 4:01:26 PM 171.0 -
2/2/2019 4:01:27 PM 171.7 -
2/2/2019 4:01:28 PM 173.2 -
2/2/2019 4:01:29 PM 278.4 107.3
2/2/2019 4:01:30 PM 392.2 221.1
2/2/2019 4:01:31 PM 461.6 290.5
2/2/2019 4:01:32 PM 618.6 447.5
2/2/2019 4:01:33 PM 767.5 596.4
2/2/2019 4:01:34 PM 870.7 699.6
2/2/2019 4:01:35 PM 1086.0 914.9
2/2/2019 4:01:36 PM 1223.8 1052.7
2/2/2019 4:01:37 PM 1302.6 1131.5
2/2/2019 4:01:38 PM 1352.3 1181.2
2/2/2019 4:01:39 PM 1377.6 1206.5
2/2/2019 4:01:40 PM 1391.7 1220.6
2/2/2019 4:01:41 PM 1401.0 1229.9
2/2/2019 4:01:42 PM 1402.4 1231.3
2/2/2019 4:01:43 PM 1396.2 1225.1
2/2/2019 4:01:44 PM 1390.0 1218.9
2/2/2019 4:01:45 PM 1298.2 1127.1
2/2/2019 4:01:46 PM 1270.5 1099.4
2/2/2019 4:01:47 PM 1230.0 1058.9
2/2/2019 4:01:48 PM 1185.0 1013.9
2/2/2019 4:01:49 PM 1172.6 1001.5
2/2/2019 4:01:50 PM 1149.4 978.3
2/2/2019 4:01:51 PM 1035.7 864.6
2/2/2019 4:01:52 PM 1000.6 829.5
2/2/2019 4:01:53 PM 946.0 774.9
2/2/2019 4:01:54 PM 925.5 754.4
2/2/2019 4:01:55 PM 906.9 735.8
2/2/2019 4:01:56 PM 803.3 632.2
2/2/2019 4:01:57 PM 769.5 598.4
2/2/2019 4:01:58 PM 739.0 567.9
2/2/2019 4:01:59 PM 731.3 560.2
2/2/2019 4:02:00 PM 634.7 463.6
2/2/2019 4:02:01 PM 640.4 469.3
2/2/2019 4:02:02 PM 630.6 459.5
Table E1 OLDOF-TR-1 TEST-1 Data Log
Page 61 of 452 August 2019
APPENDIX E17: SALT DILUTION GAUGING SUMMARY
Old Outfall-TR-1 Test-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-TR-1 TEST-1 Data Log
2/2/2019 4:02:03 PM 614.5 443.4
2/2/2019 4:02:04 PM 593.9 422.8
2/2/2019 4:02:05 PM 577.9 406.8
2/2/2019 4:02:06 PM 503.1 332.0
2/2/2019 4:02:07 PM 485.2 314.1
2/2/2019 4:02:08 PM 465.3 294.2
2/2/2019 4:02:09 PM 458.6 287.5
2/2/2019 4:02:10 PM 447.2 276.1
2/2/2019 4:02:11 PM 438.7 267.6
2/2/2019 4:02:12 PM 429.8 258.7
2/2/2019 4:02:13 PM 421.9 250.8
2/2/2019 4:02:14 PM 412.8 241.7
2/2/2019 4:02:15 PM 405.9 234.8
2/2/2019 4:02:16 PM 345.8 174.7
2/2/2019 4:02:17 PM 337.6 166.5
2/2/2019 4:02:18 PM 323.2 152.1
2/2/2019 4:02:19 PM 318.1 147.0
2/2/2019 4:02:20 PM 313.7 142.6
2/2/2019 4:02:21 PM 309.6 138.5
2/2/2019 4:02:22 PM 305.3 134.2
2/2/2019 4:02:23 PM 302.0 130.9
2/2/2019 4:02:24 PM 298.0 126.9
2/2/2019 4:02:25 PM 294.6 123.5
2/2/2019 4:02:26 PM 290.8 119.7
2/2/2019 4:02:27 PM 287.8 116.7
2/2/2019 4:02:28 PM 284.4 113.3
2/2/2019 4:02:29 PM 281.5 110.4
2/2/2019 4:02:30 PM 278.4 107.3
2/2/2019 4:02:31 PM 275.8 104.7
2/2/2019 4:02:32 PM 272.4 101.3
2/2/2019 4:02:33 PM 267.0 95.9
2/2/2019 4:02:34 PM 261.2 90.1
2/2/2019 4:02:35 PM 256.4 85.3
2/2/2019 4:02:36 PM 251.3 80.2
2/2/2019 4:02:37 PM 247.1 76.0
2/2/2019 4:02:38 PM 242.8 71.7
2/2/2019 4:02:39 PM 239.3 68.2
2/2/2019 4:02:40 PM 235.4 64.3
2/2/2019 4:02:41 PM 232.2 61.1
2/2/2019 4:02:42 PM 229.0 57.9
2/2/2019 4:02:43 PM 226.3 55.2
2/2/2019 4:02:44 PM 223.3 52.2
2/2/2019 4:02:45 PM 220.9 49.8
2/2/2019 4:02:46 PM 218.3 47.2
2/2/2019 4:02:47 PM 216.2 45.1
2/2/2019 4:02:48 PM 213.8 42.7
2/2/2019 4:02:49 PM 211.9 40.8
2/2/2019 4:02:50 PM 209.9 38.8
2/2/2019 4:02:51 PM 207.9 36.8
2/2/2019 4:02:52 PM 206.2 35.1
2/2/2019 4:02:53 PM 204.5 33.4
2/2/2019 4:02:54 PM 203.0 31.9
2/2/2019 4:02:55 PM 201.5 30.4
2/2/2019 4:02:56 PM 200.3 29.2
2/2/2019 4:02:57 PM 199.1 28.0
2/2/2019 4:02:58 PM 198.1 27.0
2/2/2019 4:02:59 PM 197.0 25.9
2/2/2019 4:03:00 PM 196.2 25.1
2/2/2019 4:03:01 PM 195.2 24.1
2/2/2019 4:03:02 PM 194.5 23.4
2/2/2019 4:03:03 PM 193.7 22.6
2/2/2019 4:03:04 PM 193.0 21.9
2/2/2019 4:03:05 PM 192.3 21.2
2/2/2019 4:03:06 PM 191.8 20.7
2/2/2019 4:03:07 PM 191.1 20.0
2/2/2019 4:03:08 PM 190.6 19.5
2/2/2019 4:03:09 PM 189.9 18.8
2/2/2019 4:03:10 PM 189.4 18.3
2/2/2019 4:03:11 PM 188.7 17.6
2/2/2019 4:03:12 PM 188.2 17.1
2/2/2019 4:03:13 PM 187.5 16.4
2/2/2019 4:03:14 PM 187.0 15.9
2/2/2019 4:03:15 PM 186.4 15.3
2/2/2019 4:03:16 PM 186.0 14.9
Page 62 of 452 August 2019
APPENDIX E17: SALT DILUTION GAUGING SUMMARY
Old Outfall-TR-1 Test-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-TR-1 TEST-1 Data Log
2/2/2019 4:03:17 PM 185.5 14.4
2/2/2019 4:03:18 PM 185.1 14.0
2/2/2019 4:03:19 PM 184.6 13.5
2/2/2019 4:03:20 PM 184.2 13.1
2/2/2019 4:03:21 PM 183.8 12.7
2/2/2019 4:03:22 PM 183.5 12.4
2/2/2019 4:03:23 PM 183.1 12.0
2/2/2019 4:03:24 PM 182.9 11.8
2/2/2019 4:03:25 PM 182.6 11.5
2/2/2019 4:03:26 PM 182.3 11.2
2/2/2019 4:03:27 PM 182.0 10.9
2/2/2019 4:03:28 PM 181.8 10.7
2/2/2019 4:03:29 PM 181.5 10.4
2/2/2019 4:03:30 PM 181.2 10.1
2/2/2019 4:03:31 PM 180.9 9.8
2/2/2019 4:03:32 PM 180.6 9.5
2/2/2019 4:03:33 PM 180.3 9.2
2/2/2019 4:03:34 PM 180.1 9.0
2/2/2019 4:03:35 PM 179.9 8.8
2/2/2019 4:03:36 PM 179.7 8.6
2/2/2019 4:03:37 PM 179.5 8.4
2/2/2019 4:03:38 PM 179.3 8.2
2/2/2019 4:03:39 PM 179.2 8.1
2/2/2019 4:03:40 PM 179.0 7.9
2/2/2019 4:03:41 PM 178.9 7.8
2/2/2019 4:03:42 PM 178.8 7.7
2/2/2019 4:03:43 PM 178.6 7.5
2/2/2019 4:03:44 PM 178.5 7.4
2/2/2019 4:03:45 PM 178.4 7.3
2/2/2019 4:03:46 PM 178.3 7.2
2/2/2019 4:03:47 PM 178.1 7.0
2/2/2019 4:03:48 PM 178.0 6.9
2/2/2019 4:03:49 PM 177.8 6.7
2/2/2019 4:03:50 PM 177.6 6.5
2/2/2019 4:03:51 PM 177.4 6.3
2/2/2019 4:03:52 PM 177.2 6.1
2/2/2019 4:03:53 PM 177.0 5.9
2/2/2019 4:03:54 PM 176.9 5.8
2/2/2019 4:03:55 PM 176.7 5.6
2/2/2019 4:03:56 PM 176.5 5.4
2/2/2019 4:03:57 PM 176.3 5.2
2/2/2019 4:03:58 PM 176.2 5.1
2/2/2019 4:03:59 PM 176.0 4.9
2/2/2019 4:04:00 PM 175.9 4.8
2/2/2019 4:04:01 PM 175.7 4.6
2/2/2019 4:04:02 PM 175.6 4.5
2/2/2019 4:04:03 PM 175.4 4.3
2/2/2019 4:04:04 PM 175.3 4.2
2/2/2019 4:04:05 PM 175.1 4.0
2/2/2019 4:04:06 PM 175.0 3.9
2/2/2019 4:04:07 PM 174.9 3.8
2/2/2019 4:04:08 PM 174.8 -
2/2/2019 4:04:09 PM 174.6 -
2/2/2019 4:04:10 PM 174.5 -
2/2/2019 4:04:11 PM 174.4 -
2/2/2019 4:04:12 PM 174.3 -
Page 63 of 452 August 2019
APPENDIX E17: SALT DILUTION GAUGING SUMMARY
Old Outfall-TR-1 Test-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
OLDOF-TR-1 TEST-1 1534
OLDOF-TR-1 TEST-1 1536
OLDOF-TR-1 TEST-1 1538
Location EC Reading
(µS/cms)
OLDOF-TR-1 TEST-1 202.2
OLDOF-TR-1 TEST-1 1,718.0
OLDOF-TR-1 TEST-1 14,826.0
OLDOF-TR-1 TEST-1 116,811.0
q 150,000
K 1.1713
4.83
76.73
Notes:
°C degrees celsius
mg/L miligrams per liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Calculated Flow Rate Q
L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement Part 2:
Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8, no. 1, 2004,
pp. 11–15.
Slope of Calibration Curve (µS/cms) / (mg/L)
Integral of Conductivity Data Curve SUM:Δt(ECt-
ECbkg)36,346.71 (s) . (µS/cms)
Mass of Salt injected mg
(mg/L)(°C)
100 17.4
1,000 17.8
10,000 17.3
100,000 17.7
Table E4 OLDOF-TR-1 TEST-1 Flow Calculation Summary
Average (post-test)174.6 (µS/cms)
Table E3 OLDOF-TR-1 TEST-1 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
Average (pre-test)171.1 (µS/cms)
(µS/cms)(°C)
166.9 10.3
157.9 10
150.0 9.9
Geometric Mean 158.1 (µS/cms)
Table E2 OLDOF-TR-1 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 64 of 452 August 2019
APPENDIX E18: SALT DILUTION GAUGING SUMMARY
Old Outfall-TR-1 Test-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/2/2019 4:10:10 PM 170.1 -
2/2/2019 4:10:11 PM 170.1 -
2/2/2019 4:10:12 PM 170.0 -
2/2/2019 4:10:13 PM 169.9 -
2/2/2019 4:10:14 PM 169.9 -
2/2/2019 4:10:15 PM 169.8 -
2/2/2019 4:10:16 PM 169.7 -
2/2/2019 4:10:17 PM 169.6 -
2/2/2019 4:10:18 PM 169.4 -
2/2/2019 4:10:19 PM 169.3 -
2/2/2019 4:10:20 PM 169.2 -
2/2/2019 4:10:21 PM 169.1 -
2/2/2019 4:10:22 PM 169.0 -
2/2/2019 4:10:23 PM 168.9 -
2/2/2019 4:10:24 PM 168.8 -
2/2/2019 4:10:25 PM 168.7 -
2/2/2019 4:10:26 PM 168.6 -
2/2/2019 4:10:27 PM 168.5 -
2/2/2019 4:10:28 PM 168.4 -
2/2/2019 4:10:29 PM 168.3 -
2/2/2019 4:10:30 PM 168.2 -
2/2/2019 4:10:31 PM 168.1 -
2/2/2019 4:10:32 PM 168.0 -
2/2/2019 4:10:33 PM 168.1 -
2/2/2019 4:10:34 PM 169.3 -
2/2/2019 4:10:35 PM 239.7 70.6
2/2/2019 4:10:36 PM 355.2 186.1
2/2/2019 4:10:37 PM 496.6 327.5
2/2/2019 4:10:38 PM 623.5 454.4
2/2/2019 4:10:39 PM 740.1 571.0
2/2/2019 4:10:40 PM 1318.7 1149.6
2/2/2019 4:10:41 PM 1353.2 1184.1
2/2/2019 4:10:42 PM 1503.3 1334.2
2/2/2019 4:10:43 PM 1526.3 1357.2
2/2/2019 4:10:44 PM 1571.2 1402.1
2/2/2019 4:10:45 PM 1598.7 1429.6
2/2/2019 4:10:46 PM 1615.6 1446.5
2/2/2019 4:10:47 PM 1615.8 1446.7
2/2/2019 4:10:48 PM 1606.0 1436.9
2/2/2019 4:10:49 PM 1466.1 1297.0
2/2/2019 4:10:50 PM 1402.1 1233.0
2/2/2019 4:10:51 PM 1330.9 1161.8
2/2/2019 4:10:52 PM 1292.9 1123.8
2/2/2019 4:10:53 PM 1148.3 979.2
2/2/2019 4:10:54 PM 1069.1 900.0
2/2/2019 4:10:55 PM 1006.6 837.5
2/2/2019 4:10:56 PM 972.7 803.6
2/2/2019 4:10:57 PM 945.7 776.6
2/2/2019 4:10:58 PM 914.6 745.5
2/2/2019 4:10:59 PM 803.5 634.4
2/2/2019 4:11:00 PM 764.8 595.7
2/2/2019 4:11:01 PM 743.2 574.1
2/2/2019 4:11:02 PM 741.9 572.8
2/2/2019 4:11:03 PM 619.3 450.2
2/2/2019 4:11:04 PM 606.0 436.9
2/2/2019 4:11:05 PM 588.8 419.7
2/2/2019 4:11:06 PM 578.9 409.8
2/2/2019 4:11:07 PM 567.0 397.9
2/2/2019 4:11:08 PM 555.2 386.1
2/2/2019 4:11:09 PM 484.4 315.3
2/2/2019 4:11:10 PM 465.7 296.6
2/2/2019 4:11:11 PM 443.9 274.8
2/2/2019 4:11:12 PM 434.4 265.3
2/2/2019 4:11:13 PM 424.5 255.4
2/2/2019 4:11:14 PM 415.7 246.6
2/2/2019 4:11:15 PM 405.9 236.8
2/2/2019 4:11:16 PM 398.3 229.2
2/2/2019 4:11:17 PM 388.7 219.6
2/2/2019 4:11:18 PM 382.3 213.2
Table E1 OLDOF-TR-1 TEST-2 Data Log
Page 65 of 452 August 2019
APPENDIX E18: SALT DILUTION GAUGING SUMMARY
Old Outfall-TR-1 Test-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 OLDOF-TR-1 TEST-2 Data Log
2/2/2019 4:11:19 PM 375.7 206.6
2/2/2019 4:11:20 PM 317.3 148.2
2/2/2019 4:11:21 PM 307.8 138.7
2/2/2019 4:11:22 PM 300.4 131.3
2/2/2019 4:11:23 PM 296.7 127.6
2/2/2019 4:11:24 PM 293.2 124.1
2/2/2019 4:11:25 PM 288.6 119.5
2/2/2019 4:11:26 PM 286.1 117.0
2/2/2019 4:11:27 PM 282.2 113.1
2/2/2019 4:11:28 PM 279.0 109.9
2/2/2019 4:11:29 PM 274.6 105.5
2/2/2019 4:11:30 PM 271.8 102.7
2/2/2019 4:11:31 PM 268.8 99.7
2/2/2019 4:11:32 PM 267.0 97.9
2/2/2019 4:11:33 PM 263.4 94.3
2/2/2019 4:11:34 PM 261.1 92.0
2/2/2019 4:11:35 PM 258.5 89.4
2/2/2019 4:11:36 PM 256.0 86.9
2/2/2019 4:11:37 PM 250.6 81.5
2/2/2019 4:11:38 PM 246.2 77.1
2/2/2019 4:11:39 PM 241.6 72.5
2/2/2019 4:11:40 PM 238.9 69.8
2/2/2019 4:11:41 PM 233.8 64.7
2/2/2019 4:11:42 PM 230.6 61.5
2/2/2019 4:11:43 PM 227.9 58.8
2/2/2019 4:11:44 PM 224.2 55.1
2/2/2019 4:11:45 PM 221.1 52.0
2/2/2019 4:11:46 PM 218.7 49.6
2/2/2019 4:11:47 PM 216.7 47.6
2/2/2019 4:11:48 PM 213.8 44.7
2/2/2019 4:11:49 PM 210.8 41.7
2/2/2019 4:11:50 PM 209.3 40.2
2/2/2019 4:11:51 PM 207.1 38.0
2/2/2019 4:11:52 PM 204.7 35.6
2/2/2019 4:11:53 PM 202.9 33.8
2/2/2019 4:11:54 PM 201.7 32.6
2/2/2019 4:11:55 PM 199.7 30.6
2/2/2019 4:11:56 PM 198.2 29.1
2/2/2019 4:11:57 PM 196.6 27.5
2/2/2019 4:11:58 PM 195.7 26.6
2/2/2019 4:11:59 PM 194.3 25.2
2/2/2019 4:12:00 PM 192.8 23.7
2/2/2019 4:12:01 PM 191.6 22.5
2/2/2019 4:12:02 PM 190.8 21.7
2/2/2019 4:12:03 PM 190.1 21.0
2/2/2019 4:12:04 PM 188.8 19.7
2/2/2019 4:12:05 PM 188.0 18.9
2/2/2019 4:12:06 PM 187.0 17.9
2/2/2019 4:12:07 PM 186.0 16.9
2/2/2019 4:12:08 PM 185.3 16.2
2/2/2019 4:12:09 PM 184.5 15.4
2/2/2019 4:12:10 PM 183.9 14.8
2/2/2019 4:12:11 PM 183.3 14.2
2/2/2019 4:12:12 PM 182.8 13.7
2/2/2019 4:12:13 PM 182.3 13.2
2/2/2019 4:12:14 PM 181.6 12.5
2/2/2019 4:12:15 PM 181.1 12.0
2/2/2019 4:12:16 PM 180.7 11.6
2/2/2019 4:12:17 PM 180.4 11.3
2/2/2019 4:12:18 PM 180.0 10.9
2/2/2019 4:12:19 PM 179.6 10.5
2/2/2019 4:12:20 PM 179.2 10.1
Page 66 of 452 August 2019
APPENDIX E18: SALT DILUTION GAUGING SUMMARY
Old Outfall-TR-1 Test-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
OLDOF-TR-1 TEST-2 1534
OLDOF-TR-1 TEST-2 1536
OLDOF-TR-1 TEST-2 1538
Location EC Reading
(µS/cms)
OLDOF-TR-1 TEST-2 202.2
OLDOF-TR-1 TEST-2 1,718.0
OLDOF-TR-1 TEST-2 14,826.0
OLDOF-TR-1 TEST-2 116,811.0
q 150,000
K 1.1713
5.08
80.56
Notes:
°C degrees celsius
mg/L miligrams per liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Calculated Flow Rate Q
L/s
GPM
17.8
10,000 17.3
100,000 17.7
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement Part 2:
Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8, no. 1, 2004,
pp. 11–15.
158.1
169.1
(µS/cms)
(µS/cms)
Geometric Mean
Table E4 OLDOF-TR-1 TEST-2 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Integral of Conductivity Data Curve SUM:Δt(ECt-
ECbkg)34,615.92 (s) . (µS/cms)
1,000
17.4
Average (post-test)-(µS/cms)
150.0 9.9
Average (pre-test)
Table E3 OLDOF-TR-1 TEST-2 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
(mg/L)(°C)
100
(µS/cms)(°C)
166.9 10.3
157.9 10
Table E2 OLDOF-TR-1 TEST-2 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 67 of 452 August 2019
APPENDIX E19: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/7/2019 12:18:35 PM 125.0 -
2/7/2019 12:18:36 PM 125.0 -
2/7/2019 12:18:37 PM 125.0 -
2/7/2019 12:18:38 PM 124.9 -
2/7/2019 12:18:39 PM 124.9 -
2/7/2019 12:18:40 PM 124.8 -
2/7/2019 12:18:41 PM 124.8 -
2/7/2019 12:18:42 PM 124.7 -
2/7/2019 12:18:43 PM 124.7 -
2/7/2019 12:18:44 PM 124.6 -
2/7/2019 12:18:45 PM 124.6 -
2/7/2019 12:18:46 PM 124.5 -
2/7/2019 12:18:47 PM 124.5 -
2/7/2019 12:18:48 PM 124.4 -
2/7/2019 12:18:49 PM 124.3 -
2/7/2019 12:18:50 PM 124.2 -
2/7/2019 12:18:51 PM 124.2 -
2/7/2019 12:18:52 PM 124.1 -
2/7/2019 12:18:53 PM 124.0 -
2/7/2019 12:18:54 PM 123.9 -
2/7/2019 12:18:55 PM 123.9 -
2/7/2019 12:18:56 PM 123.8 -
2/7/2019 12:18:57 PM 123.7 -
2/7/2019 12:18:58 PM 123.7 -
2/7/2019 12:18:59 PM 123.6 -
2/7/2019 12:19:00 PM 123.5 -
2/7/2019 12:19:01 PM 123.5 -
2/7/2019 12:19:02 PM 123.4 -
2/7/2019 12:19:03 PM 123.4 -
2/7/2019 12:19:04 PM 123.4 -
2/7/2019 12:19:05 PM 123.3 -
2/7/2019 12:19:06 PM 123.3 -
2/7/2019 12:19:07 PM 123.3 -
2/7/2019 12:19:08 PM 123.2 -
2/7/2019 12:19:09 PM 123.2 -
2/7/2019 12:19:10 PM 123.1 -
2/7/2019 12:19:11 PM 123.0 -
2/7/2019 12:19:12 PM 122.9 -
2/7/2019 12:19:13 PM 122.9 -
2/7/2019 12:19:14 PM 123.6 -
2/7/2019 12:19:15 PM 204.2 80.2
2/7/2019 12:19:16 PM 411.1 287.1
2/7/2019 12:19:17 PM 669.2 545.2
2/7/2019 12:19:18 PM 1719.2 1595.2
2/7/2019 12:19:19 PM 2286.7 2162.7
2/7/2019 12:19:20 PM 3328.8 3204.8
2/7/2019 12:19:21 PM 4140.1 4016.1
2/7/2019 12:19:22 PM 4929.7 4805.7
2/7/2019 12:19:23 PM 5077.9 4953.9
2/7/2019 12:19:24 PM 4830.3 4706.3
2/7/2019 12:19:25 PM 4533.6 4409.6
2/7/2019 12:19:26 PM 3796.7 3672.7
2/7/2019 12:19:27 PM 3314.1 3190.1
2/7/2019 12:19:28 PM 2809.5 2685.5
2/7/2019 12:19:29 PM 2541.9 2417.9
2/7/2019 12:19:30 PM 2243.9 2119.9
2/7/2019 12:19:31 PM 1943.8 1819.8
2/7/2019 12:19:32 PM 1821.7 1697.7
2/7/2019 12:19:33 PM 1601.3 1477.3
2/7/2019 12:19:34 PM 1429.3 1305.3
2/7/2019 12:19:35 PM 1279.3 1155.3
2/7/2019 12:19:36 PM 1212.6 1088.6
2/7/2019 12:19:37 PM 1031.1 907.1
2/7/2019 12:19:38 PM 949.1 825.1
2/7/2019 12:19:39 PM 877.0 753.0
2/7/2019 12:19:40 PM 858.3 734.3
2/7/2019 12:19:41 PM 835.7 711.7
2/7/2019 12:19:42 PM 739.6 615.6
2/7/2019 12:19:43 PM 683.8 559.8
2/7/2019 12:19:44 PM 644.8 520.8
Table E1 SEEP-A1 TEST-1 Data Log
Page 68 of 452 August 2019
APPENDIX E19: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-1 Data Log
2/7/2019 12:19:45 PM 628.6 504.6
2/7/2019 12:19:46 PM 611.9 487.9
2/7/2019 12:19:47 PM 513.9 389.9
2/7/2019 12:19:48 PM 531.6 407.6
2/7/2019 12:19:49 PM 509.9 385.9
2/7/2019 12:19:50 PM 494.1 370.1
2/7/2019 12:19:51 PM 481.0 357.0
2/7/2019 12:19:52 PM 472.0 348.0
2/7/2019 12:19:53 PM 464.4 340.4
2/7/2019 12:19:54 PM 458.0 334.0
2/7/2019 12:19:55 PM 407.5 283.5
2/7/2019 12:19:56 PM 390.1 266.1
2/7/2019 12:19:57 PM 382.9 258.9
2/7/2019 12:19:58 PM 370.1 246.1
2/7/2019 12:19:59 PM 360.6 236.6
2/7/2019 12:20:00 PM 353.1 229.1
2/7/2019 12:20:01 PM 347.2 223.2
2/7/2019 12:20:02 PM 341.9 217.9
2/7/2019 12:20:03 PM 335.7 211.7
2/7/2019 12:20:04 PM 330.4 206.4
2/7/2019 12:20:05 PM 325.3 201.3
2/7/2019 12:20:06 PM 321.6 197.6
2/7/2019 12:20:07 PM 276.4 152.4
2/7/2019 12:20:08 PM 265.4 141.4
2/7/2019 12:20:09 PM 254.6 130.6
2/7/2019 12:20:10 PM 246.5 122.5
2/7/2019 12:20:11 PM 243.4 119.4
2/7/2019 12:20:12 PM 239.1 115.1
2/7/2019 12:20:13 PM 236.2 112.2
2/7/2019 12:20:14 PM 233.4 109.4
2/7/2019 12:20:15 PM 231.3 107.3
2/7/2019 12:20:16 PM 228.9 104.9
2/7/2019 12:20:17 PM 227.5 103.5
2/7/2019 12:20:18 PM 226.8 102.8
2/7/2019 12:20:19 PM 226.2 102.2
2/7/2019 12:20:20 PM 225.2 101.2
2/7/2019 12:20:21 PM 224.4 100.4
2/7/2019 12:20:22 PM 223.3 99.3
2/7/2019 12:20:23 PM 222.0 98.0
2/7/2019 12:20:24 PM 218.7 94.7
2/7/2019 12:20:25 PM 215.4 91.4
2/7/2019 12:20:26 PM 211.4 87.4
2/7/2019 12:20:27 PM 208.0 84.0
2/7/2019 12:20:28 PM 204.1 80.1
2/7/2019 12:20:29 PM 200.8 76.8
2/7/2019 12:20:30 PM 197.0 73.0
2/7/2019 12:20:31 PM 193.3 69.3
2/7/2019 12:20:32 PM 188.7 64.7
2/7/2019 12:20:33 PM 184.9 60.9
2/7/2019 12:20:34 PM 180.2 56.2
2/7/2019 12:20:35 PM 176.3 52.3
2/7/2019 12:20:36 PM 172.3 48.3
2/7/2019 12:20:37 PM 169.3 45.3
2/7/2019 12:20:38 PM 166.6 42.6
2/7/2019 12:20:39 PM 164.4 40.4
2/7/2019 12:20:40 PM 162.2 38.2
2/7/2019 12:20:41 PM 160.5 36.5
2/7/2019 12:20:42 PM 158.6 34.6
2/7/2019 12:20:43 PM 157.0 33.0
2/7/2019 12:20:44 PM 155.1 31.1
2/7/2019 12:20:45 PM 153.7 29.7
2/7/2019 12:20:46 PM 152.2 28.2
2/7/2019 12:20:47 PM 151.2 27.2
2/7/2019 12:20:48 PM 150.1 26.1
2/7/2019 12:20:49 PM 149.2 25.2
2/7/2019 12:20:50 PM 148.0 24.0
2/7/2019 12:20:51 PM 146.8 22.8
2/7/2019 12:20:52 PM 145.7 21.7
2/7/2019 12:20:53 PM 144.5 20.5
2/7/2019 12:20:54 PM 143.3 19.3
2/7/2019 12:20:55 PM 142.0 18.0
2/7/2019 12:20:56 PM 140.8 16.8
2/7/2019 12:20:57 PM 139.3 15.3
2/7/2019 12:20:58 PM 137.5 13.5
2/7/2019 12:20:59 PM 136.3 12.3
Page 69 of 452 August 2019
APPENDIX E19: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-1 Data Log
2/7/2019 12:21:00 PM 134.8 10.8
2/7/2019 12:21:01 PM 133.0 9.0
2/7/2019 12:21:02 PM 131.4 7.4
2/7/2019 12:21:03 PM 129.7 5.7
2/7/2019 12:21:04 PM 128.1 4.1
2/7/2019 12:21:05 PM 126.4 2.4
2/7/2019 12:21:06 PM 124.9 0.9
2/7/2019 12:21:07 PM 123.2 -
2/7/2019 12:21:08 PM 121.3 -
2/7/2019 12:21:09 PM 120.1 -
2/7/2019 12:21:10 PM 119.0 -
2/7/2019 12:21:11 PM 117.8 -
2/7/2019 12:21:12 PM 116.8 -
2/7/2019 12:21:13 PM 115.5 -
2/7/2019 12:21:14 PM 114.9 -
2/7/2019 12:21:15 PM 114.0 -
2/7/2019 12:21:16 PM 113.4 -
2/7/2019 12:21:17 PM 112.5 -
2/7/2019 12:21:18 PM 112.0 -
2/7/2019 12:21:19 PM 111.4 -
2/7/2019 12:21:20 PM 110.9 -
2/7/2019 12:21:21 PM 110.2 -
2/7/2019 12:21:22 PM 109.7 -
2/7/2019 12:21:23 PM 109.1 -
2/7/2019 12:21:24 PM 108.6 -
2/7/2019 12:21:25 PM 108.1 -
2/7/2019 12:21:26 PM 107.6 -
2/7/2019 12:21:27 PM 107.1 -
2/7/2019 12:21:28 PM 106.7 -
2/7/2019 12:21:29 PM 106.2 -
2/7/2019 12:21:30 PM 105.9 -
2/7/2019 12:21:31 PM 105.5 -
2/7/2019 12:21:32 PM 105.2 -
2/7/2019 12:21:33 PM 104.8 -
2/7/2019 12:21:34 PM 104.6 -
2/7/2019 12:21:35 PM 104.3 -
2/7/2019 12:21:36 PM 104.0 -
2/7/2019 12:21:37 PM 103.8 -
2/7/2019 12:21:38 PM 103.5 -
2/7/2019 12:21:39 PM 103.1 -
2/7/2019 12:21:40 PM 102.6 -
2/7/2019 12:21:41 PM 102.2 -
2/7/2019 12:21:42 PM 101.7 -
2/7/2019 12:21:43 PM 101.2 -
2/7/2019 12:21:44 PM 100.8 -
2/7/2019 12:21:45 PM 100.4 -
2/7/2019 12:21:46 PM 99.9 -
2/7/2019 12:21:47 PM 99.5 -
2/7/2019 12:21:48 PM 99.0 -
2/7/2019 12:21:49 PM 98.6 -
2/7/2019 12:21:50 PM 98.1 -
2/7/2019 12:21:51 PM 97.7 -
2/7/2019 12:21:52 PM 97.4 -
2/7/2019 12:21:53 PM 97.2 -
2/7/2019 12:21:54 PM 96.9 -
2/7/2019 12:21:55 PM 96.7 -
2/7/2019 12:21:56 PM 96.5 -
2/7/2019 12:21:57 PM 96.2 -
2/7/2019 12:21:58 PM 96.0 -
2/7/2019 12:21:59 PM 95.7 -
2/7/2019 12:22:00 PM 95.5 -
2/7/2019 12:22:01 PM 95.3 -
2/7/2019 12:22:02 PM 95.1 -
2/7/2019 12:22:03 PM 94.9 -
2/7/2019 12:22:04 PM 94.6 -
2/7/2019 12:22:05 PM 94.5 -
2/7/2019 12:22:06 PM 94.3 -
2/7/2019 12:22:07 PM 94.1 -
2/7/2019 12:22:08 PM 93.9 -
2/7/2019 12:22:09 PM 93.7 -
2/7/2019 12:22:10 PM 93.5 -
2/7/2019 12:22:11 PM 93.4 -
2/7/2019 12:22:12 PM 93.2 -
2/7/2019 12:22:13 PM 93.0 -
2/7/2019 12:22:14 PM 92.8 -
2/7/2019 12:22:15 PM 92.7 -
Page 70 of 452 August 2019
APPENDIX E19: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-1 Data Log
2/7/2019 12:22:16 PM 92.5 -
2/7/2019 12:22:17 PM 92.4 -
2/7/2019 12:22:18 PM 92.2 -
2/7/2019 12:22:19 PM 92.0 -
2/7/2019 12:22:20 PM 91.9 -
2/7/2019 12:22:21 PM 91.7 -
2/7/2019 12:22:22 PM 91.5 -
2/7/2019 12:22:23 PM 91.3 -
2/7/2019 12:22:24 PM 91.2 -
2/7/2019 12:22:25 PM 91.1 -
2/7/2019 12:22:26 PM 91.0 -
2/7/2019 12:22:27 PM 90.9 -
2/7/2019 12:22:28 PM 90.8 -
2/7/2019 12:22:29 PM 90.7 -
2/7/2019 12:22:30 PM 90.6 -
2/7/2019 12:22:31 PM 90.5 -
2/7/2019 12:22:32 PM 90.4 -
2/7/2019 12:22:33 PM 90.4 -
2/7/2019 12:22:34 PM 90.3 -
2/7/2019 12:22:35 PM 90.2 -
2/7/2019 12:22:36 PM 90.1 -
2/7/2019 12:22:37 PM 90.0 -
2/7/2019 12:22:38 PM 89.9 -
2/7/2019 12:22:39 PM 89.7 -
2/7/2019 12:22:40 PM 89.6 -
2/7/2019 12:22:41 PM 89.5 -
2/7/2019 12:22:42 PM 89.3 -
2/7/2019 12:22:43 PM 89.2 -
2/7/2019 12:22:44 PM 89.1 -
2/7/2019 12:22:45 PM 88.9 -
2/7/2019 12:22:46 PM 88.8 -
2/7/2019 12:22:47 PM 88.6 -
2/7/2019 12:22:48 PM 88.5 -
2/7/2019 12:22:49 PM 88.4 -
2/7/2019 12:22:50 PM 88.3 -
2/7/2019 12:22:51 PM 88.2 -
2/7/2019 12:22:52 PM 88.1 -
2/7/2019 12:22:53 PM 87.9 -
2/7/2019 12:22:54 PM 87.8 -
2/7/2019 12:22:55 PM 87.7 -
2/7/2019 12:22:56 PM 87.6 -
2/7/2019 12:22:57 PM 87.5 -
2/7/2019 12:22:58 PM 87.4 -
2/7/2019 12:22:59 PM 87.3 -
2/7/2019 12:23:00 PM 87.2 -
2/7/2019 12:23:01 PM 87.1 -
2/7/2019 12:23:02 PM 87.0 -
2/7/2019 12:23:03 PM 87.0 -
2/7/2019 12:23:04 PM 86.9 -
2/7/2019 12:23:05 PM 86.9 -
2/7/2019 12:23:06 PM 86.8 -
2/7/2019 12:23:07 PM 86.8 -
2/7/2019 12:23:08 PM 86.8 -
2/7/2019 12:23:09 PM 86.8 -
2/7/2019 12:23:10 PM 86.8 -
2/7/2019 12:23:11 PM 86.7 -
2/7/2019 12:23:12 PM 86.7 -
2/7/2019 12:23:13 PM 86.7 -
2/7/2019 12:23:14 PM 86.7 -
2/7/2019 12:23:15 PM 86.7 -
2/7/2019 12:23:16 PM 86.7 -
2/7/2019 12:23:17 PM 86.7 -
2/7/2019 12:23:18 PM 86.7 -
Page 71 of 452 August 2019
APPENDIX E19: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-1 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-A1 TEST-1 1139
SEEP-A1 TEST-1 1140
SEEP-A1 TEST-1 1142
SEEP-A1 TEST-1 1143
SEEP-A1 TEST-1 1145
Location EC Reading
(µS/cms)
SEEP-A1 TEST-1 137.4
SEEP-A1 TEST-1 197.1
SEEP-A1 TEST-1 1,436.0
SEEP-A1 TEST-1 11,790.0
SEEP-A1 TEST-1 97,320.0
q 300,400
K 0.9753
4.23
67.15
Notes:
°C degrees celsius
mg/L miligrams per liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Calculated Flow Rate Q
L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement
Part 2: Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8,
no. 1, 2004, pp. 11–15.
Integral of Conductivity Data Curve SUM:Δt(ECt-
ECbkg)69,255.76 (s) . (µS/cms)
1,000 22.3
10,000 22.3
Table E4 SEEP-A1 TEST-1 Flow Calculation Summary
Mass of Salt injected mg
100,000 22.2
Slope of Calibration Curve (µS/cms) / (mg/L)
(mg/L) (°C)
100 22.2
Average (post-test) 96.4 (µS/cms)
Table E3 SEEP-A1 TEST-1 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
10 22.0
Geometric Mean 112.7 (µS/cms)
Average (pre-test) 124.0 (µS/cms)
115.9 17.9
109.8 18
101 18
(µS/cms) (°C)
110.1 18
128.7 17.9
Table E2 SEEP-A1 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 72 of 452 August 2019
APPENDIX E20: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/7/2019 12:29:45 PM 120.3 -
2/7/2019 12:29:46 PM 120.3 -
2/7/2019 12:29:47 PM 120.3 -
2/7/2019 12:29:48 PM 120.2 -
2/7/2019 12:29:49 PM 120.2 -
2/7/2019 12:29:50 PM 120.2 -
2/7/2019 12:29:51 PM 120.1 -
2/7/2019 12:29:52 PM 120.1 -
2/7/2019 12:29:53 PM 120.1 -
2/7/2019 12:29:54 PM 120.1 -
2/7/2019 12:29:55 PM 120.1 -
2/7/2019 12:29:56 PM 120.1 -
2/7/2019 12:29:57 PM 120.1 -
2/7/2019 12:29:58 PM 120.1 -
2/7/2019 12:29:59 PM 120.1 -
2/7/2019 12:30:00 PM 120.0 -
2/7/2019 12:30:01 PM 119.9 -
2/7/2019 12:30:02 PM 119.8 -
2/7/2019 12:30:03 PM 119.7 -
2/7/2019 12:30:04 PM 119.5 -
2/7/2019 12:30:05 PM 119.4 -
2/7/2019 12:30:06 PM 119.3 -
2/7/2019 12:30:07 PM 119.1 -
2/7/2019 12:30:08 PM 118.9 -
2/7/2019 12:30:09 PM 118.8 -
2/7/2019 12:30:10 PM 118.5 -
2/7/2019 12:30:11 PM 118.3 -
2/7/2019 12:30:12 PM 118.1 -
2/7/2019 12:30:13 PM 117.9 -
2/7/2019 12:30:14 PM 117.8 -
2/7/2019 12:30:15 PM 117.7 -
2/7/2019 12:30:16 PM 117.6 -
2/7/2019 12:30:17 PM 117.4 -
2/7/2019 12:30:18 PM 117.1 -
2/7/2019 12:30:19 PM 116.9 -
2/7/2019 12:30:20 PM 116.7 -
2/7/2019 12:30:21 PM 116.6 -
2/7/2019 12:30:22 PM 116.5 -
2/7/2019 12:30:23 PM 117.0 -
2/7/2019 12:30:24 PM 242.6 123.6
2/7/2019 12:30:25 PM 474.7 355.7
2/7/2019 12:30:26 PM 680.7 561.7
2/7/2019 12:30:27 PM 1774.0 1655.0
2/7/2019 12:30:28 PM 2377.7 2258.7
2/7/2019 12:30:29 PM 2927.5 2808.5
2/7/2019 12:30:30 PM 3175.5 3056.5
2/7/2019 12:30:31 PM 3183.0 3064.0
2/7/2019 12:30:32 PM 2919.9 2800.9
2/7/2019 12:30:33 PM 2466.4 2347.4
2/7/2019 12:30:34 PM 2057.4 1938.4
2/7/2019 12:30:35 PM 1692.7 1573.7
2/7/2019 12:30:36 PM 1318.0 1199.0
2/7/2019 12:30:37 PM 1090.5 971.5
2/7/2019 12:30:38 PM 922.9 803.9
2/7/2019 12:30:39 PM 774.9 655.9
2/7/2019 12:30:40 PM 675.1 556.1
2/7/2019 12:30:41 PM 587.8 468.8
2/7/2019 12:30:42 PM 423.6 304.6
2/7/2019 12:30:43 PM 477.1 358.1
2/7/2019 12:30:44 PM 472.4 353.4
2/7/2019 12:30:45 PM 460.8 341.8
2/7/2019 12:30:46 PM 396.5 277.5
2/7/2019 12:30:47 PM 369.5 250.5
2/7/2019 12:30:48 PM 352.7 233.7
2/7/2019 12:30:49 PM 345.6 226.6
2/7/2019 12:30:50 PM 337.5 218.5
2/7/2019 12:30:51 PM 326.7 207.7
2/7/2019 12:30:52 PM 321.4 202.4
2/7/2019 12:30:53 PM 311.3 192.3
2/7/2019 12:30:54 PM 262.4 143.4
Table E1 SEEP-A1 TEST-2 Data Log
Page 73 of 452 August 2019
APPENDIX E20: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-2 Data Log
2/7/2019 12:30:55 PM 250.9 131.9
2/7/2019 12:30:56 PM 241.4 122.4
2/7/2019 12:30:57 PM 235.8 116.8
2/7/2019 12:30:58 PM 231.7 112.7
2/7/2019 12:30:59 PM 226.9 107.9
2/7/2019 12:31:00 PM 223.4 104.4
2/7/2019 12:31:01 PM 219.6 100.6
2/7/2019 12:31:02 PM 216.7 97.7
2/7/2019 12:31:03 PM 213.5 94.5
2/7/2019 12:31:04 PM 211.1 92.1
2/7/2019 12:31:05 PM 208.6 89.6
2/7/2019 12:31:06 PM 206.6 87.6
2/7/2019 12:31:07 PM 204.3 85.3
2/7/2019 12:31:08 PM 202.5 83.5
2/7/2019 12:31:09 PM 200.5 81.5
2/7/2019 12:31:10 PM 198.7 79.7
2/7/2019 12:31:11 PM 194.3 75.3
2/7/2019 12:31:12 PM 190.7 71.7
2/7/2019 12:31:13 PM 187.1 68.1
2/7/2019 12:31:14 PM 184.2 65.2
2/7/2019 12:31:15 PM 181.3 62.3
2/7/2019 12:31:16 PM 178.9 59.9
2/7/2019 12:31:17 PM 176.3 57.3
2/7/2019 12:31:18 PM 174.2 55.2
2/7/2019 12:31:19 PM 171.9 52.9
2/7/2019 12:31:20 PM 170.2 51.2
2/7/2019 12:31:21 PM 168.3 49.3
2/7/2019 12:31:22 PM 166.7 47.7
2/7/2019 12:31:23 PM 165.0 46.0
2/7/2019 12:31:24 PM 163.5 44.5
2/7/2019 12:31:25 PM 161.8 42.8
2/7/2019 12:31:26 PM 160.4 41.4
2/7/2019 12:31:27 PM 158.7 39.7
2/7/2019 12:31:28 PM 157.3 38.3
2/7/2019 12:31:29 PM 155.8 36.8
2/7/2019 12:31:30 PM 154.5 35.5
2/7/2019 12:31:31 PM 153.0 34.0
2/7/2019 12:31:32 PM 151.6 32.6
2/7/2019 12:31:33 PM 150.0 31.0
2/7/2019 12:31:34 PM 148.3 29.3
2/7/2019 12:31:35 PM 146.9 27.9
2/7/2019 12:31:36 PM 145.3 26.3
2/7/2019 12:31:37 PM 144.0 25.0
2/7/2019 12:31:38 PM 142.6 23.6
2/7/2019 12:31:39 PM 141.4 22.4
2/7/2019 12:31:40 PM 140.0 21.0
2/7/2019 12:31:41 PM 138.8 19.8
2/7/2019 12:31:42 PM 137.5 18.5
2/7/2019 12:31:43 PM 136.3 17.3
2/7/2019 12:31:44 PM 135.1 16.1
2/7/2019 12:31:45 PM 134.1 15.1
2/7/2019 12:31:46 PM 132.9 13.9
2/7/2019 12:31:47 PM 132.0 13.0
2/7/2019 12:31:48 PM 131.0 12.0
2/7/2019 12:31:49 PM 130.1 11.1
2/7/2019 12:31:50 PM 129.2 10.2
2/7/2019 12:31:51 PM 128.4 9.4
2/7/2019 12:31:52 PM 127.6 8.6
2/7/2019 12:31:53 PM 126.9 7.9
2/7/2019 12:31:54 PM 126.2 7.2
2/7/2019 12:31:55 PM 125.6 6.6
2/7/2019 12:31:56 PM 125.0 6.0
2/7/2019 12:31:57 PM 124.5 5.5
2/7/2019 12:31:58 PM 124.0 5.0
2/7/2019 12:31:59 PM 123.6 4.6
2/7/2019 12:32:00 PM 123.2 4.2
2/7/2019 12:32:01 PM 122.9 3.9
2/7/2019 12:32:02 PM 122.6 3.6
2/7/2019 12:32:03 PM 122.3 3.3
2/7/2019 12:32:04 PM 122.0 3.0
2/7/2019 12:32:05 PM 121.7 2.7
2/7/2019 12:32:06 PM 121.4 2.4
2/7/2019 12:32:07 PM 121.1 2.1
2/7/2019 12:32:08 PM 120.7 -
2/7/2019 12:32:09 PM 120.4 -
Page 74 of 452 August 2019
APPENDIX E20: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-2 Data Log
2/7/2019 12:32:10 PM 120.1 -
2/7/2019 12:32:11 PM 119.9 -
2/7/2019 12:32:12 PM 119.5 -
2/7/2019 12:32:13 PM 119.2 -
2/7/2019 12:32:14 PM 118.8 -
2/7/2019 12:32:15 PM 118.5 -
2/7/2019 12:32:16 PM 118.1 -
2/7/2019 12:32:17 PM 117.8 -
2/7/2019 12:32:18 PM 117.5 -
2/7/2019 12:32:19 PM 117.2 -
2/7/2019 12:32:20 PM 116.8 -
2/7/2019 12:32:21 PM 116.6 -
2/7/2019 12:32:22 PM 116.3 -
2/7/2019 12:32:23 PM 116.0 -
2/7/2019 12:32:24 PM 115.7 -
2/7/2019 12:32:25 PM 115.5 -
2/7/2019 12:32:26 PM 115.2 -
2/7/2019 12:32:27 PM 114.9 -
2/7/2019 12:32:28 PM 114.6 -
2/7/2019 12:32:29 PM 114.2 -
2/7/2019 12:32:30 PM 113.9 -
2/7/2019 12:32:31 PM 113.6 -
2/7/2019 12:32:32 PM 113.2 -
2/7/2019 12:32:33 PM 112.8 -
2/7/2019 12:32:34 PM 112.4 -
2/7/2019 12:32:35 PM 112.0 -
2/7/2019 12:32:36 PM 111.6 -
2/7/2019 12:32:37 PM 111.1 -
2/7/2019 12:32:38 PM 110.7 -
2/7/2019 12:32:39 PM 110.3 -
2/7/2019 12:32:40 PM 109.9 -
2/7/2019 12:32:41 PM 109.6 -
2/7/2019 12:32:42 PM 109.2 -
2/7/2019 12:32:43 PM 108.8 -
2/7/2019 12:32:44 PM 108.5 -
2/7/2019 12:32:45 PM 108.2 -
2/7/2019 12:32:46 PM 108.0 -
2/7/2019 12:32:47 PM 107.8 -
2/7/2019 12:32:48 PM 107.6 -
2/7/2019 12:32:49 PM 107.5 -
2/7/2019 12:32:50 PM 107.4 -
2/7/2019 12:32:51 PM 107.3 -
2/7/2019 12:32:52 PM 107.2 -
2/7/2019 12:32:53 PM 107.0 -
2/7/2019 12:32:54 PM 106.9 -
2/7/2019 12:32:55 PM 106.9 -
2/7/2019 12:32:56 PM 106.8 -
2/7/2019 12:32:57 PM 106.8 -
2/7/2019 12:32:58 PM 106.8 -
2/7/2019 12:32:59 PM 106.7 -
2/7/2019 12:33:00 PM 106.6 -
2/7/2019 12:33:01 PM 106.5 -
2/7/2019 12:33:02 PM 106.3 -
2/7/2019 12:33:03 PM 106.0 -
2/7/2019 12:33:04 PM 105.8 -
2/7/2019 12:33:05 PM 105.6 -
2/7/2019 12:33:06 PM 105.4 -
2/7/2019 12:33:07 PM 105.2 -
2/7/2019 12:33:08 PM 104.9 -
2/7/2019 12:33:09 PM 104.7 -
2/7/2019 12:33:10 PM 104.4 -
2/7/2019 12:33:11 PM 104.1 -
2/7/2019 12:33:12 PM 103.9 -
2/7/2019 12:33:13 PM 103.6 -
2/7/2019 12:33:14 PM 103.4 -
2/7/2019 12:33:15 PM 103.2 -
2/7/2019 12:33:16 PM 103.0 -
2/7/2019 12:33:17 PM 102.7 -
2/7/2019 12:33:18 PM 102.5 -
2/7/2019 12:33:19 PM 102.3 -
2/7/2019 12:33:20 PM 102.1 -
2/7/2019 12:33:21 PM 101.9 -
2/7/2019 12:33:22 PM 101.7 -
2/7/2019 12:33:23 PM 101.5 -
2/7/2019 12:33:24 PM 101.3 -
2/7/2019 12:33:25 PM 101.2 -
Page 75 of 452 August 2019
APPENDIX E20: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-2 Data Log
2/7/2019 12:33:26 PM 101.0 -
2/7/2019 12:33:27 PM 100.8 -
2/7/2019 12:33:28 PM 100.6 -
2/7/2019 12:33:29 PM 100.5 -
2/7/2019 12:33:30 PM 100.4 -
2/7/2019 12:33:31 PM 100.2 -
2/7/2019 12:33:32 PM 100.1 -
2/7/2019 12:33:33 PM 100.0 -
2/7/2019 12:33:34 PM 99.8 -
2/7/2019 12:33:35 PM 99.7 -
2/7/2019 12:33:36 PM 99.6 -
2/7/2019 12:33:37 PM 99.5 -
2/7/2019 12:33:38 PM 99.4 -
2/7/2019 12:33:39 PM 99.3 -
2/7/2019 12:33:40 PM 99.3 -
2/7/2019 12:33:41 PM 99.2 -
2/7/2019 12:33:42 PM 99.2 -
2/7/2019 12:33:43 PM 99.1 -
2/7/2019 12:33:44 PM 99.0 -
2/7/2019 12:33:45 PM 99.0 -
2/7/2019 12:33:46 PM 98.8 -
2/7/2019 12:33:47 PM 98.8 -
2/7/2019 12:33:48 PM 98.7 -
2/7/2019 12:33:49 PM 98.6 -
2/7/2019 12:33:50 PM 98.5 -
2/7/2019 12:33:51 PM 98.4 -
2/7/2019 12:33:52 PM 98.2 -
2/7/2019 12:33:53 PM 98.1 -
2/7/2019 12:33:54 PM 98.0 -
2/7/2019 12:33:55 PM 97.9 -
2/7/2019 12:33:56 PM 97.7 -
2/7/2019 12:33:57 PM 97.6 -
2/7/2019 12:33:58 PM 97.6 -
2/7/2019 12:33:59 PM 97.5 -
2/7/2019 12:34:00 PM 97.4 -
2/7/2019 12:34:01 PM 97.3 -
2/7/2019 12:34:02 PM 97.2 -
2/7/2019 12:34:03 PM 97.1 -
2/7/2019 12:34:04 PM 97.1 -
2/7/2019 12:34:05 PM 97.1 -
2/7/2019 12:34:06 PM 97.0 -
2/7/2019 12:34:07 PM 97.0 -
2/7/2019 12:34:08 PM 96.9 -
2/7/2019 12:34:09 PM 96.8 -
2/7/2019 12:34:10 PM 96.8 -
2/7/2019 12:34:11 PM 96.8 -
2/7/2019 12:34:12 PM 96.7 -
2/7/2019 12:34:13 PM 96.7 -
2/7/2019 12:34:14 PM 96.7 -
2/7/2019 12:34:15 PM 96.7 -
2/7/2019 12:34:16 PM 96.6 -
2/7/2019 12:34:17 PM 96.5 -
2/7/2019 12:34:18 PM 96.5 -
2/7/2019 12:34:19 PM 96.4 -
2/7/2019 12:34:20 PM 96.3 -
2/7/2019 12:34:21 PM 96.2 -
2/7/2019 12:34:22 PM 96.2 -
Page 76 of 452 August 2019
APPENDIX E20: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-2 February
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-A1 TEST-1 1139
SEEP-A1 TEST-1 1140
SEEP-A1 TEST-1 1142
SEEP-A1 TEST-1 1143
SEEP-A1 TEST-1 1145
Location EC Reading
(µS/cms)
SEEP-A1 TEST-1 137.4
SEEP-A1 TEST-1 197.1
SEEP-A1 TEST-1 1,436.0
SEEP-A1 TEST-1 11,790.0
SEEP-A1 TEST-1 97,320.0
q 150,000
K 0.9753
4.40
69.00
Notes:
°C degrees celsius
mg/L miligrams per liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Calculated Flow Rate Q
L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement
Part 2: Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8,
no. 1, 2004, pp. 11–15.
Integral of Conductivity Data Curve SUM:Δt(ECt-
ECbkg)33,645.50 (s) . (µS/cms)
1,000 22.3
10,000 22.3
100,000 22.2
Table E4 SEEP-A1 TEST-2 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
(mg/L) (°C)
10 22.0
100 22.2
Average (post-test) 96.4 (µS/cms)
Table E3 SEEP-A1 TEST-2 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
Geometric Mean 112.7 (µS/cms)
Average (pre-test) 124.0 (µS/cms)
115.9 17.9
109.8 18
101 18
(µS/cms) (°C)
110.1 18
128.7 17.9
Table E2 SEEP-A1 TEST-2 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 77 of 452 August 2019
APPENDIX E21: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-1 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
5/23/2019 2:28:57 PM 168.9 -
5/23/2019 2:28:58 PM 168.8 -
5/23/2019 2:28:59 PM 168.7 -
5/23/2019 2:29:00 PM 168.5 -
5/23/2019 2:29:01 PM 168.4 -
5/23/2019 2:29:02 PM 168.2 -
5/23/2019 2:29:03 PM 168.1 -
5/23/2019 2:29:04 PM 167.9 -
5/23/2019 2:29:05 PM 167.8 -
5/23/2019 2:29:06 PM 167.6 -
5/23/2019 2:29:07 PM 167.5 -
5/23/2019 2:29:08 PM 167.4 -
5/23/2019 2:29:09 PM 167.3 -
5/23/2019 2:29:10 PM 167.2 -
5/23/2019 2:29:11 PM 167.1 -
5/23/2019 2:29:12 PM 167.0 -
5/23/2019 2:29:13 PM 166.9 -
5/23/2019 2:29:14 PM 166.9 -
5/23/2019 2:29:15 PM 166.8 -
5/23/2019 2:29:16 PM 166.7 -
5/23/2019 2:29:17 PM 166.6 -
5/23/2019 2:29:18 PM 166.5 -
5/23/2019 2:29:19 PM 166.5 -
5/23/2019 2:29:20 PM 167.2 -
5/23/2019 2:29:21 PM 473.2 305.7
5/23/2019 2:29:22 PM 783.0 615.5
5/23/2019 2:29:23 PM 3359.2 3191.7
5/23/2019 2:29:24 PM 4465.0 4297.5
5/23/2019 2:29:25 PM 6103.6 5936.1
5/23/2019 2:29:26 PM 6478.7 6311.2
5/23/2019 2:29:27 PM 6627.1 6459.6
5/23/2019 2:29:28 PM 6530.9 6363.4
5/23/2019 2:29:29 PM 5893.6 5726.1
5/23/2019 2:29:30 PM 5528.1 5360.6
5/23/2019 2:29:31 PM 5135.1 4967.6
5/23/2019 2:29:32 PM 4878.5 4711.0
5/23/2019 2:29:33 PM 4272.5 4105.0
5/23/2019 2:29:34 PM 3947.3 3779.8
5/23/2019 2:29:35 PM 3623.5 3456.0
5/23/2019 2:29:36 PM 3276.9 3109.4
5/23/2019 2:29:37 PM 2984.7 2817.2
5/23/2019 2:29:38 PM 2735.2 2567.7
5/23/2019 2:29:39 PM 2537.5 2370.0
5/23/2019 2:29:40 PM 2148.5 1981.0
5/23/2019 2:29:41 PM 1946.7 1779.2
5/23/2019 2:29:42 PM 1719.2 1551.7
5/23/2019 2:29:43 PM 1601.4 1433.9
5/23/2019 2:29:44 PM 1372.3 1204.8
5/23/2019 2:29:45 PM 1188.2 1020.7
5/23/2019 2:29:46 PM 1072.1 904.6
5/23/2019 2:29:47 PM 959.6 792.1
5/23/2019 2:29:48 PM 865.1 697.6
5/23/2019 2:29:49 PM 784.1 616.6
5/23/2019 2:29:50 PM 707.3 539.8
5/23/2019 2:29:51 PM 684.9 517.4
5/23/2019 2:29:52 PM 674.0 506.5
5/23/2019 2:29:53 PM 566.2 398.7
5/23/2019 2:29:54 PM 514.2 346.7
5/23/2019 2:29:55 PM 486.0 318.5
5/23/2019 2:29:56 PM 474.5 307.0
5/23/2019 2:29:57 PM 459.0 291.5
5/23/2019 2:29:58 PM 450.5 283.0
5/23/2019 2:29:59 PM 384.6 217.1
5/23/2019 2:30:00 PM 372.6 205.1
5/23/2019 2:30:01 PM 354.6 187.1
5/23/2019 2:30:02 PM 343.1 175.6
5/23/2019 2:30:03 PM 338.2 170.7
5/23/2019 2:30:04 PM 332.8 165.3
5/23/2019 2:30:05 PM 325.2 157.7
5/23/2019 2:30:06 PM 319.4 151.9
Table E1 SEEP-A1 TEST-1 Data Log
Page 78 of 452 August 2019
APPENDIX E21: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-1 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-1 Data Log
5/23/2019 2:30:07 PM 314.6 147.1
5/23/2019 2:30:08 PM 309.9 142.4
5/23/2019 2:30:09 PM 306.3 138.8
5/23/2019 2:30:10 PM 302.1 134.6
5/23/2019 2:30:11 PM 298.6 131.1
5/23/2019 2:30:12 PM 294.9 127.4
5/23/2019 2:30:13 PM 291.7 124.2
5/23/2019 2:30:14 PM 288.3 120.8
5/23/2019 2:30:15 PM 284.9 117.4
5/23/2019 2:30:16 PM 277.5 110.0
5/23/2019 2:30:17 PM 271.9 104.4
5/23/2019 2:30:18 PM 266.1 98.6
5/23/2019 2:30:19 PM 261.4 93.9
5/23/2019 2:30:20 PM 256.6 89.1
5/23/2019 2:30:21 PM 252.5 85.0
5/23/2019 2:30:22 PM 248.2 80.7
5/23/2019 2:30:23 PM 244.9 77.4
5/23/2019 2:30:24 PM 241.5 74.0
5/23/2019 2:30:25 PM 238.4 70.9
5/23/2019 2:30:26 PM 235.9 68.4
5/23/2019 2:30:27 PM 233.4 65.9
5/23/2019 2:30:28 PM 231.3 63.8
5/23/2019 2:30:29 PM 229.0 61.5
5/23/2019 2:30:30 PM 227.1 59.6
5/23/2019 2:30:31 PM 225.1 57.6
5/23/2019 2:30:32 PM 223.5 56.0
5/23/2019 2:30:33 PM 221.7 54.2
5/23/2019 2:30:34 PM 220.3 52.8
5/23/2019 2:30:35 PM 218.8 51.3
5/23/2019 2:30:36 PM 217.5 50.0
5/23/2019 2:30:37 PM 216.1 48.6
5/23/2019 2:30:38 PM 214.9 47.4
5/23/2019 2:30:39 PM 213.5 46.0
5/23/2019 2:30:40 PM 212.4 44.9
5/23/2019 2:30:41 PM 211.2 43.7
5/23/2019 2:30:42 PM 210.2 42.7
5/23/2019 2:30:43 PM 209.1 41.6
5/23/2019 2:30:44 PM 208.1 40.6
5/23/2019 2:30:45 PM 207.2 39.7
5/23/2019 2:30:46 PM 206.3 38.8
5/23/2019 2:30:47 PM 205.5 38.0
5/23/2019 2:30:48 PM 204.7 37.2
5/23/2019 2:30:49 PM 204.0 36.5
5/23/2019 2:30:50 PM 203.3 35.8
5/23/2019 2:30:51 PM 202.7 35.2
5/23/2019 2:30:52 PM 202.1 34.6
5/23/2019 2:30:53 PM 201.6 34.1
5/23/2019 2:30:54 PM 201.1 33.6
5/23/2019 2:30:55 PM 200.6 33.1
5/23/2019 2:30:56 PM 200.1 32.6
5/23/2019 2:30:57 PM 199.7 32.2
5/23/2019 2:30:58 PM 199.2 31.7
5/23/2019 2:30:59 PM 198.8 31.3
5/23/2019 2:31:00 PM 198.3 30.8
5/23/2019 2:31:01 PM 197.9 30.4
5/23/2019 2:31:02 PM 197.4 29.9
5/23/2019 2:31:03 PM 196.9 29.4
5/23/2019 2:31:04 PM 196.5 29.0
5/23/2019 2:31:05 PM 196.0 28.5
5/23/2019 2:31:06 PM 195.5 28.0
5/23/2019 2:31:07 PM 195.0 27.5
5/23/2019 2:31:08 PM 194.5 27.0
5/23/2019 2:31:09 PM 194.0 26.5
5/23/2019 2:31:10 PM 193.5 26.0
5/23/2019 2:31:11 PM 193.0 25.5
5/23/2019 2:31:12 PM 192.5 25.0
5/23/2019 2:31:13 PM 192.0 24.5
5/23/2019 2:31:14 PM 191.6 24.1
5/23/2019 2:31:15 PM 191.1 23.6
5/23/2019 2:31:16 PM 190.7 23.2
5/23/2019 2:31:17 PM 190.2 22.7
5/23/2019 2:31:18 PM 189.8 22.3
5/23/2019 2:31:19 PM 189.4 21.9
5/23/2019 2:31:20 PM 189.0 21.5
5/23/2019 2:31:21 PM 188.6 21.1
Page 79 of 452 August 2019
APPENDIX E21: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-1 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-1 Data Log
5/23/2019 2:31:22 PM 188.2 20.7
5/23/2019 2:31:23 PM 187.9 20.4
5/23/2019 2:31:24 PM 187.5 20.0
5/23/2019 2:31:25 PM 187.2 19.7
5/23/2019 2:31:26 PM 186.9 19.4
5/23/2019 2:31:27 PM 186.6 19.1
5/23/2019 2:31:28 PM 186.3 18.8
5/23/2019 2:31:29 PM 186.0 18.5
5/23/2019 2:31:30 PM 185.7 18.2
5/23/2019 2:31:31 PM 185.5 18.0
5/23/2019 2:31:32 PM 185.2 17.7
5/23/2019 2:31:33 PM 185.0 17.5
5/23/2019 2:31:34 PM 184.7 17.2
5/23/2019 2:31:35 PM 184.5 17.0
5/23/2019 2:31:36 PM 184.2 16.7
5/23/2019 2:31:37 PM 184.0 16.5
5/23/2019 2:31:38 PM 183.7 16.2
5/23/2019 2:31:39 PM 183.5 16.0
5/23/2019 2:31:40 PM 183.2 15.7
5/23/2019 2:31:41 PM 183.0 15.5
5/23/2019 2:31:42 PM 182.8 15.3
5/23/2019 2:31:43 PM 182.5 15.0
5/23/2019 2:31:44 PM 182.3 14.8
5/23/2019 2:31:45 PM 182.0 14.5
5/23/2019 2:31:46 PM 181.8 14.3
5/23/2019 2:31:47 PM 181.6 14.1
5/23/2019 2:31:48 PM 181.4 13.9
5/23/2019 2:31:49 PM 181.2 13.7
5/23/2019 2:31:50 PM 181.0 13.5
5/23/2019 2:31:51 PM 180.8 13.3
5/23/2019 2:31:52 PM 180.6 13.1
5/23/2019 2:31:53 PM 180.3 12.8
5/23/2019 2:31:54 PM 180.2 12.7
5/23/2019 2:31:55 PM 179.9 12.4
5/23/2019 2:31:56 PM 179.8 12.3
5/23/2019 2:31:57 PM 179.5 12.0
5/23/2019 2:31:58 PM 179.4 11.9
5/23/2019 2:31:59 PM 179.2 11.7
5/23/2019 2:32:00 PM 179.0 11.5
5/23/2019 2:32:01 PM 178.8 11.3
5/23/2019 2:32:02 PM 178.7 11.2
5/23/2019 2:32:03 PM 178.5 11.0
5/23/2019 2:32:04 PM 178.3 10.8
5/23/2019 2:32:05 PM 178.2 10.7
5/23/2019 2:32:06 PM 178.0 10.5
5/23/2019 2:32:07 PM 177.9 10.4
5/23/2019 2:32:08 PM 177.7 10.2
5/23/2019 2:32:09 PM 177.5 10.0
5/23/2019 2:32:10 PM 177.3 9.8
5/23/2019 2:32:11 PM 177.2 9.7
5/23/2019 2:32:12 PM 177.0 9.5
5/23/2019 2:32:13 PM 176.8 9.3
5/23/2019 2:32:14 PM 176.6 9.1
5/23/2019 2:32:15 PM 176.5 9.0
5/23/2019 2:32:16 PM 176.3 8.8
5/23/2019 2:32:17 PM 176.1 8.6
5/23/2019 2:32:18 PM 175.9 8.4
5/23/2019 2:32:19 PM 175.8 8.3
5/23/2019 2:32:20 PM 175.6 8.1
5/23/2019 2:32:21 PM 175.4 7.9
5/23/2019 2:32:22 PM 175.3 7.8
5/23/2019 2:32:23 PM 175.1 7.6
5/23/2019 2:32:24 PM 175.0 7.5
5/23/2019 2:32:25 PM 174.8 7.3
5/23/2019 2:32:26 PM 174.7 7.2
5/23/2019 2:32:27 PM 174.5 7.0
5/23/2019 2:32:28 PM 174.3 6.8
5/23/2019 2:32:29 PM 174.1 6.6
5/23/2019 2:32:30 PM 174.0 6.5
5/23/2019 2:32:31 PM 173.8 6.3
5/23/2019 2:32:32 PM 173.7 6.2
5/23/2019 2:32:33 PM 173.5 6.0
5/23/2019 2:32:34 PM 173.4 5.9
5/23/2019 2:32:35 PM 173.2 5.7
5/23/2019 2:32:36 PM 173.1 5.6
Page 80 of 452 August 2019
APPENDIX E21: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-1 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-1 Data Log
5/23/2019 2:32:37 PM 172.9 5.4
5/23/2019 2:32:38 PM 172.8 5.3
5/23/2019 2:32:39 PM 172.7 5.2
5/23/2019 2:32:40 PM 172.5 5.0
5/23/2019 2:32:41 PM 172.4 4.9
5/23/2019 2:32:42 PM 172.2 4.7
5/23/2019 2:32:43 PM 172.1 4.6
5/23/2019 2:32:44 PM 172.0 4.5
5/23/2019 2:32:45 PM 171.8 4.3
5/23/2019 2:32:46 PM 171.7 4.2
5/23/2019 2:32:47 PM 171.5 4.0
5/23/2019 2:32:48 PM 171.4 3.9
5/23/2019 2:32:49 PM 171.2 3.7
5/23/2019 2:32:50 PM 171.1 3.6
5/23/2019 2:32:51 PM 170.9 3.4
5/23/2019 2:32:52 PM 170.8 3.3
5/23/2019 2:32:53 PM 170.6 3.1
Page 81 of 452 August 2019
APPENDIX E21: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-1 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-A1 TEST-1 1418
SEEP-A1 TEST-1 1419
SEEP-A1 TEST-1 1420
SEEP-A1 TEST-1 1421
SEEP-A1 TEST-1 1422
EC Reading
(µS/cms)
SEEP-A1 TEST-1 39.4
SEEP-A1 TEST-1 180.0
SEEP-A1 TEST-1 453.0
SEEP-A1 TEST-1 3,480.0
SEEP-A1 TEST-1 15,600.0
SEEP-A1 TEST-1 129,760.0
q 300,000
K 1.3004
4.00
62.90
Notes:
°C degrees celsius
mg/L miligrams per liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
mgMass of Salt injected
Table E3 SEEP-A1 TEST-1 YSI Salt Dilution Calibration Data
Location Calibration Concentration
(mg/L)
Temperature
(°C)
100000 25.9
Table E4 SEEP-A1 TEST-1 Flow Calculation Summary
1000 25.2
10000 26.3
1
(s) . (µS/cms)98,513.0 SUM:Δt(ECt-
ECbkg)Integral of Conductivity Data Curve
(µS/cms) / (mg/L)Slope of Calibration Curve
Calculated Flow Rate Q L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement
Part 2: Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8,
no. 1, 2004, pp. 11–15.
25.8
10 25.3
100 24.6
Average (post-test)163.1 (µS/cms)
Geometric Mean 176.4 (µS/cms)
Average (pre-test)179.9 (µS/cms)
179 19.6
174.7 19.7
175.9 19.7
(µS/cms)(°C)
173 19.5
179.6 19.6
Table E2 SEEP-A1 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 82 of 452 August 2019
APPENDIX E22: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-2 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
5/23/2019 2:38:46 PM 179.8 -
5/23/2019 2:38:47 PM 179.8 -
5/23/2019 2:38:48 PM 179.8 -
5/23/2019 2:38:49 PM 179.8 -
5/23/2019 2:38:50 PM 179.8 -
5/23/2019 2:38:51 PM 179.8 -
5/23/2019 2:38:52 PM 179.8 -
5/23/2019 2:38:53 PM 179.8 -
5/23/2019 2:38:54 PM 179.8 -
5/23/2019 2:38:55 PM 179.8 -
5/23/2019 2:38:56 PM 179.8 -
5/23/2019 2:38:57 PM 179.8 -
5/23/2019 2:38:58 PM 179.8 -
5/23/2019 2:38:59 PM 179.8 -
5/23/2019 2:39:00 PM 179.8 -
5/23/2019 2:39:01 PM 179.8 -
5/23/2019 2:39:02 PM 179.8 -
5/23/2019 2:39:03 PM 179.7 -
5/23/2019 2:39:04 PM 179.8 -
5/23/2019 2:39:05 PM 347.1 167.3
5/23/2019 2:39:06 PM 722.2 542.4
5/23/2019 2:39:07 PM 2390.7 2210.9
5/23/2019 2:39:08 PM 5110.1 4930.3
5/23/2019 2:39:09 PM 6769.1 6589.3
5/23/2019 2:39:10 PM 7846.7 7666.9
5/23/2019 2:39:11 PM 8244.0 8064.2
5/23/2019 2:39:12 PM 7704.3 7524.5
5/23/2019 2:39:13 PM 7058.7 6878.9
5/23/2019 2:39:14 PM 6772.1 6592.3
5/23/2019 2:39:15 PM 5958.5 5778.7
5/23/2019 2:39:16 PM 5242.3 5062.5
5/23/2019 2:39:17 PM 4717.2 4537.4
5/23/2019 2:39:18 PM 4326.0 4146.2
5/23/2019 2:39:19 PM 3953.3 3773.5
5/23/2019 2:39:20 PM 3754.9 3575.1
5/23/2019 2:39:21 PM 3302.6 3122.8
5/23/2019 2:39:22 PM 2954.9 2775.1
5/23/2019 2:39:23 PM 2703.0 2523.2
5/23/2019 2:39:24 PM 2385.1 2205.3
5/23/2019 2:39:25 PM 2007.9 1828.1
5/23/2019 2:39:26 PM 1934.1 1754.3
5/23/2019 2:39:27 PM 1581.2 1401.4
5/23/2019 2:39:28 PM 1476.4 1296.6
5/23/2019 2:39:29 PM 1339.8 1160.0
5/23/2019 2:39:30 PM 1119.4 939.6
5/23/2019 2:39:31 PM 951.8 772.0
5/23/2019 2:39:32 PM 896.8 717.0
5/23/2019 2:39:33 PM 866.9 687.1
5/23/2019 2:39:34 PM 689.4 509.6
5/23/2019 2:39:35 PM 641.0 461.2
5/23/2019 2:39:36 PM 561.7 381.9
5/23/2019 2:39:37 PM 565.3 385.5
5/23/2019 2:39:38 PM 529.4 349.6
5/23/2019 2:39:39 PM 464.5 284.7
5/23/2019 2:39:40 PM 417.9 238.1
5/23/2019 2:39:41 PM 391.8 212.0
5/23/2019 2:39:42 PM 378.1 198.3
5/23/2019 2:39:43 PM 368.0 188.2
5/23/2019 2:39:44 PM 360.1 180.3
5/23/2019 2:39:45 PM 351.1 171.3
5/23/2019 2:39:46 PM 343.0 163.2
5/23/2019 2:39:47 PM 292.3 112.5
5/23/2019 2:39:48 PM 281.7 101.9
5/23/2019 2:39:49 PM 276.5 96.7
5/23/2019 2:39:50 PM 267.9 88.1
5/23/2019 2:39:51 PM 263.1 83.3
5/23/2019 2:39:52 PM 258.2 78.4
5/23/2019 2:39:53 PM 254.4 74.6
5/23/2019 2:39:54 PM 251.6 71.8
5/23/2019 2:39:55 PM 249.0 69.2
Table E1 SEEP-A1 TEST-2 Data Log
Page 83 of 452 August 2019
APPENDIX E22: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-2 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-2 Data Log
5/23/2019 2:39:56 PM 246.7 66.9
5/23/2019 2:39:57 PM 244.2 64.4
5/23/2019 2:39:58 PM 242.2 62.4
5/23/2019 2:39:59 PM 240.0 60.2
5/23/2019 2:40:00 PM 238.3 58.5
5/23/2019 2:40:01 PM 236.4 56.6
5/23/2019 2:40:02 PM 234.8 55.0
5/23/2019 2:40:03 PM 232.8 53.0
5/23/2019 2:40:04 PM 229.3 49.5
5/23/2019 2:40:05 PM 225.8 46.0
5/23/2019 2:40:06 PM 223.1 43.3
5/23/2019 2:40:07 PM 220.2 40.4
5/23/2019 2:40:08 PM 217.8 38.0
5/23/2019 2:40:09 PM 215.5 35.7
5/23/2019 2:40:10 PM 213.6 33.8
5/23/2019 2:40:11 PM 212.1 32.3
5/23/2019 2:40:12 PM 210.3 30.5
5/23/2019 2:40:13 PM 208.8 29.0
5/23/2019 2:40:14 PM 207.3 27.5
5/23/2019 2:40:15 PM 205.8 26.0
5/23/2019 2:40:16 PM 204.6 24.8
5/23/2019 2:40:17 PM 203.6 23.8
5/23/2019 2:40:18 PM 202.6 22.8
5/23/2019 2:40:19 PM 201.8 22.0
5/23/2019 2:40:20 PM 200.9 21.1
5/23/2019 2:40:21 PM 200.3 20.5
5/23/2019 2:40:22 PM 199.6 19.8
5/23/2019 2:40:23 PM 199.0 19.2
5/23/2019 2:40:24 PM 198.4 18.6
5/23/2019 2:40:25 PM 197.9 18.1
5/23/2019 2:40:26 PM 197.4 17.6
5/23/2019 2:40:27 PM 197.0 17.2
5/23/2019 2:40:28 PM 196.5 16.7
5/23/2019 2:40:29 PM 196.1 16.3
5/23/2019 2:40:30 PM 195.6 15.8
5/23/2019 2:40:31 PM 195.3 15.5
5/23/2019 2:40:32 PM 194.9 15.1
5/23/2019 2:40:33 PM 194.4 14.6
5/23/2019 2:40:34 PM 194.0 14.2
5/23/2019 2:40:35 PM 193.5 13.7
5/23/2019 2:40:36 PM 192.9 13.1
5/23/2019 2:40:37 PM 192.6 12.8
5/23/2019 2:40:38 PM 192.1 12.3
5/23/2019 2:40:39 PM 191.7 11.9
5/23/2019 2:40:40 PM 191.3 11.5
5/23/2019 2:40:41 PM 190.8 11.0
5/23/2019 2:40:42 PM 190.6 10.8
5/23/2019 2:40:43 PM 190.1 10.3
5/23/2019 2:40:44 PM 189.8 10.0
5/23/2019 2:40:45 PM 189.4 9.6
5/23/2019 2:40:46 PM 189.1 9.3
5/23/2019 2:40:47 PM 188.8 9.0
5/23/2019 2:40:48 PM 188.5 8.7
5/23/2019 2:40:49 PM 188.2 8.4
5/23/2019 2:40:50 PM 187.9 8.1
5/23/2019 2:40:51 PM 187.7 7.9
5/23/2019 2:40:52 PM 187.4 7.6
5/23/2019 2:40:53 PM 187.1 7.3
5/23/2019 2:40:54 PM 186.8 7.0
5/23/2019 2:40:55 PM 186.6 6.8
5/23/2019 2:40:56 PM 186.3 6.5
5/23/2019 2:40:57 PM 186.1 6.3
5/23/2019 2:40:58 PM 185.9 6.1
5/23/2019 2:40:59 PM 185.7 5.9
5/23/2019 2:41:00 PM 185.5 5.7
5/23/2019 2:41:01 PM 185.3 5.5
5/23/2019 2:41:02 PM 185.2 5.4
5/23/2019 2:41:03 PM 185.0 5.2
5/23/2019 2:41:04 PM 184.9 5.1
5/23/2019 2:41:05 PM 184.7 4.9
5/23/2019 2:41:06 PM 184.4 4.6
5/23/2019 2:41:07 PM 184.2 4.4
5/23/2019 2:41:08 PM 183.9 4.1
5/23/2019 2:41:09 PM 183.6 3.8
5/23/2019 2:41:10 PM 183.4 3.6
Page 84 of 452 August 2019
APPENDIX E22: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-2 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-2 Data Log
5/23/2019 2:41:11 PM 183.1 3.3
5/23/2019 2:41:12 PM 182.9 3.1
5/23/2019 2:41:13 PM 182.7 2.9
5/23/2019 2:41:14 PM 182.5 2.7
5/23/2019 2:41:15 PM 182.4 2.6
5/23/2019 2:41:16 PM 182.3 2.5
5/23/2019 2:41:17 PM 182.2 2.4
5/23/2019 2:41:18 PM 182.1 2.3
5/23/2019 2:41:19 PM 182.2 2.4
5/23/2019 2:41:20 PM 182.2 2.4
5/23/2019 2:41:21 PM 182.3 2.5
5/23/2019 2:41:22 PM 182.3 2.5
5/23/2019 2:41:23 PM 182.4 2.6
5/23/2019 2:41:24 PM 182.4 2.6
5/23/2019 2:41:25 PM 182.4 2.6
5/23/2019 2:41:26 PM 182.4 2.6
5/23/2019 2:41:27 PM 182.3 2.5
5/23/2019 2:41:28 PM 182.2 2.4
5/23/2019 2:41:29 PM 182.1 2.3
5/23/2019 2:41:30 PM 181.9 2.1
5/23/2019 2:41:31 PM 181.7 1.9
5/23/2019 2:41:32 PM 181.4 1.6
5/23/2019 2:41:33 PM 181.2 1.4
5/23/2019 2:41:34 PM 180.9 1.1
5/23/2019 2:41:35 PM 180.6 0.8
5/23/2019 2:41:36 PM 180.3 0.5
5/23/2019 2:41:37 PM 180.0 0.2
5/23/2019 2:41:38 PM 179.8 0.0
5/23/2019 2:41:39 PM 179.6 -0.2
5/23/2019 2:41:40 PM 179.4 -0.4
5/23/2019 2:41:41 PM 179.3 -0.5
5/23/2019 2:41:42 PM 179.1 -0.7
5/23/2019 2:41:43 PM 179.0 -0.8
5/23/2019 2:41:44 PM 178.9 -0.9
5/23/2019 2:41:45 PM 178.9 -0.9
5/23/2019 2:41:46 PM 178.9 -0.9
Page 85 of 452 August 2019
APPENDIX E22: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-2 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-A1 TEST-2 1418
SEEP-A1 TEST-2 1419
SEEP-A1 TEST-2 1420
SEEP-A1 TEST-2 1421
SEEP-A1 TEST-2 1422
EC Reading
(µS/cms)
SEEP-A1 TEST-2 39.4
SEEP-A1 TEST-2 180.0
SEEP-A1 TEST-2 453.0
SEEP-A1 TEST-2 3,480.0
SEEP-A1 TEST-2 15,600.0
SEEP-A1 TEST-2 129,760.0
q 300,800
K 1.3004
3.70
59.00
Notes:
°C degrees celsius
mg/L miligrams per liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Calculated Flow Rate Q L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement
Part 2: Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8,
no. 1, 2004, pp. 11–15.
Integral of Conductivity Data Curve SUM:Δt(ECt-
ECbkg)105,324.6 (s) . (µS/cms)
1000 25.2
10000 26.3
100000 25.9
Table E4 SEEP-A1 TEST-2 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
1 25.8
10 25.3
100 24.6
Average (post-test)163.1 (µS/cms)
Table E3 SEEP-A1 TEST-2 YSI Salt Dilution Calibration Data
Location Calibration Concentration Temperature
(mg/L)(°C)
Geometric Mean 176.4 (µS/cms)
Average (pre-test)179.9 (µS/cms)
179 19.6
174.7 19.7
175.9 19.7
(µS/cms)(°C)
173 19.5
179.6 19.6
Table E2 SEEP-A1 TEST-2 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 86 of 452 August 2019
APPENDIX E23: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-3 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
5/23/2019 2:49:19 PM 179.8 -
5/23/2019 2:49:20 PM 179.9 -
5/23/2019 2:49:21 PM 179.9 -
5/23/2019 2:49:22 PM 180.0 -
5/23/2019 2:49:23 PM 180.0 -
5/23/2019 2:49:24 PM 180.1 -
5/23/2019 2:49:25 PM 180.2 -
5/23/2019 2:49:26 PM 180.3 -
5/23/2019 2:49:27 PM 180.3 -
5/23/2019 2:49:28 PM 180.3 -
5/23/2019 2:49:29 PM 180.3 -
5/23/2019 2:49:30 PM 180.2 -
5/23/2019 2:49:31 PM 180.2 -
5/23/2019 2:49:32 PM 180.1 -
5/23/2019 2:49:33 PM 180.0 -
5/23/2019 2:49:34 PM 179.8 -
5/23/2019 2:49:35 PM 179.7 -
5/23/2019 2:49:36 PM 179.6 -
5/23/2019 2:49:37 PM 179.4 -
5/23/2019 2:49:38 PM 179.3 -
5/23/2019 2:49:39 PM 179.2 -
5/23/2019 2:49:40 PM 179.2 -
5/23/2019 2:49:41 PM 179.2 -
5/23/2019 2:49:42 PM 179.8 -
5/23/2019 2:49:43 PM 609.0 429.1
5/23/2019 2:49:44 PM 3498.1 3318.2
5/23/2019 2:49:45 PM 7553.0 7373.1
5/23/2019 2:49:46 PM 9610.6 9430.7
5/23/2019 2:49:47 PM 10174.5 9994.6
5/23/2019 2:49:48 PM 10145.7 9965.8
5/23/2019 2:49:49 PM 8907.0 8727.1
5/23/2019 2:49:50 PM 7230.4 7050.5
5/23/2019 2:49:51 PM 6486.8 6306.9
5/23/2019 2:49:52 PM 5468.8 5288.9
5/23/2019 2:49:53 PM 4435.1 4255.2
5/23/2019 2:49:54 PM 4105.0 3925.1
5/23/2019 2:49:55 PM 3941.1 3761.2
5/23/2019 2:49:56 PM 3475.6 3295.7
5/23/2019 2:49:57 PM 3172.3 2992.4
5/23/2019 2:49:58 PM 2813.3 2633.4
5/23/2019 2:49:59 PM 2658.8 2478.9
5/23/2019 2:50:00 PM 2348.2 2168.3
5/23/2019 2:50:01 PM 2095.3 1915.4
5/23/2019 2:50:02 PM 1804.3 1624.4
5/23/2019 2:50:03 PM 1664.7 1484.8
5/23/2019 2:50:04 PM 1253.5 1073.6
5/23/2019 2:50:05 PM 1086.8 906.9
5/23/2019 2:50:06 PM 955.7 775.8
5/23/2019 2:50:07 PM 869.5 689.6
5/23/2019 2:50:08 PM 798.2 618.3
5/23/2019 2:50:09 PM 715.5 535.6
5/23/2019 2:50:10 PM 688.3 508.4
5/23/2019 2:50:11 PM 682.6 502.7
5/23/2019 2:50:12 PM 528.2 348.3
5/23/2019 2:50:13 PM 506.4 326.5
5/23/2019 2:50:14 PM 478.9 299.0
5/23/2019 2:50:15 PM 473.6 293.7
5/23/2019 2:50:16 PM 457.5 277.6
5/23/2019 2:50:17 PM 381.5 201.6
5/23/2019 2:50:18 PM 366.4 186.5
5/23/2019 2:50:19 PM 346.1 166.2
5/23/2019 2:50:20 PM 343.6 163.7
5/23/2019 2:50:21 PM 337.4 157.5
5/23/2019 2:50:22 PM 329.3 149.4
5/23/2019 2:50:23 PM 318.7 138.8
5/23/2019 2:50:24 PM 310.8 130.9
5/23/2019 2:50:25 PM 303.2 123.3
5/23/2019 2:50:26 PM 297.2 117.3
5/23/2019 2:50:27 PM 291.1 111.2
5/23/2019 2:50:28 PM 285.9 106.0
5/23/2019 2:50:29 PM 282.0 102.1
Table E1 SEEP-A1 TEST-3 Data Log
Page 87 of 452 August 2019
APPENDIX E23: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-3 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-3 Data Log
5/23/2019 2:50:30 PM 277.8 97.9
5/23/2019 2:50:31 PM 232.9 53.0
5/23/2019 2:50:32 PM 228.6 48.7
5/23/2019 2:50:33 PM 226.4 46.5
5/23/2019 2:50:34 PM 224.8 44.9
5/23/2019 2:50:35 PM 223.2 43.3
5/23/2019 2:50:36 PM 221.1 41.2
5/23/2019 2:50:37 PM 220.0 40.1
5/23/2019 2:50:38 PM 218.8 38.9
5/23/2019 2:50:39 PM 217.6 37.7
5/23/2019 2:50:40 PM 216.4 36.5
5/23/2019 2:50:41 PM 215.5 35.6
5/23/2019 2:50:42 PM 214.5 34.6
5/23/2019 2:50:43 PM 213.6 33.7
5/23/2019 2:50:44 PM 212.6 32.7
5/23/2019 2:50:45 PM 211.7 31.8
5/23/2019 2:50:46 PM 210.8 30.9
5/23/2019 2:50:47 PM 209.5 29.6
5/23/2019 2:50:48 PM 207.8 27.9
5/23/2019 2:50:49 PM 206.0 26.1
5/23/2019 2:50:50 PM 204.6 24.7
5/23/2019 2:50:51 PM 203.1 23.2
5/23/2019 2:50:52 PM 202.0 22.1
5/23/2019 2:50:53 PM 200.8 20.9
5/23/2019 2:50:54 PM 199.9 20.0
5/23/2019 2:50:55 PM 198.9 19.0
5/23/2019 2:50:56 PM 198.2 18.3
5/23/2019 2:50:57 PM 197.5 17.6
5/23/2019 2:50:58 PM 197.0 17.1
5/23/2019 2:50:59 PM 196.5 16.6
5/23/2019 2:51:00 PM 196.2 16.3
5/23/2019 2:51:01 PM 195.9 16.0
5/23/2019 2:51:02 PM 195.5 15.6
5/23/2019 2:51:03 PM 195.1 15.2
5/23/2019 2:51:04 PM 194.8 14.9
5/23/2019 2:51:05 PM 194.3 14.4
5/23/2019 2:51:06 PM 193.8 13.9
5/23/2019 2:51:07 PM 193.4 13.5
5/23/2019 2:51:08 PM 192.9 13.0
5/23/2019 2:51:09 PM 192.4 12.5
5/23/2019 2:51:10 PM 191.9 12.0
5/23/2019 2:51:11 PM 191.4 11.5
5/23/2019 2:51:12 PM 190.8 10.9
5/23/2019 2:51:13 PM 190.3 10.4
5/23/2019 2:51:14 PM 189.7 9.8
5/23/2019 2:51:15 PM 189.3 9.4
5/23/2019 2:51:16 PM 188.8 8.9
5/23/2019 2:51:17 PM 188.4 8.5
5/23/2019 2:51:18 PM 188.0 8.1
5/23/2019 2:51:19 PM 187.6 7.7
5/23/2019 2:51:20 PM 187.2 7.3
5/23/2019 2:51:21 PM 186.9 7.0
5/23/2019 2:51:22 PM 186.6 6.7
5/23/2019 2:51:23 PM 186.4 6.5
5/23/2019 2:51:24 PM 186.1 6.2
5/23/2019 2:51:25 PM 185.9 6.0
5/23/2019 2:51:26 PM 185.6 5.7
5/23/2019 2:51:27 PM 185.4 5.5
5/23/2019 2:51:28 PM 185.1 5.2
5/23/2019 2:51:29 PM 184.8 4.9
5/23/2019 2:51:30 PM 184.6 4.7
5/23/2019 2:51:31 PM 184.3 4.4
5/23/2019 2:51:32 PM 184.1 4.2
5/23/2019 2:51:33 PM 183.9 4.0
5/23/2019 2:51:34 PM 183.7 3.8
5/23/2019 2:51:35 PM 183.4 3.5
5/23/2019 2:51:36 PM 183.1 3.2
5/23/2019 2:51:37 PM 182.8 2.9
5/23/2019 2:51:38 PM 182.5 2.6
5/23/2019 2:51:39 PM 182.2 2.3
5/23/2019 2:51:40 PM 182.0 2.1
5/23/2019 2:51:41 PM 181.7 1.8
5/23/2019 2:51:42 PM 181.3 1.4
5/23/2019 2:51:43 PM 181.0 1.1
5/23/2019 2:51:44 PM 180.6 0.7
5/23/2019 2:51:45 PM 180.2 0.3
5/23/2019 2:51:46 PM 179.8 -0.1
5/23/2019 2:51:47 PM 179.4 -0.5
5/23/2019 2:51:48 PM 179.0 -0.9
Page 88 of 452 August 2019
APPENDIX E23: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-3 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-3 Data Log
5/23/2019 2:51:49 PM 178.7 -1.2
5/23/2019 2:51:50 PM 178.2 -1.7
5/23/2019 2:51:51 PM 177.8 -2.1
5/23/2019 2:51:52 PM 177.4 -2.5
5/23/2019 2:51:53 PM 177.0 -2.9
5/23/2019 2:51:54 PM 176.5 -3.4
5/23/2019 2:51:55 PM 176.0 -3.9
5/23/2019 2:51:56 PM 175.5 -4.4
5/23/2019 2:51:57 PM 175.0 -4.9
5/23/2019 2:51:58 PM 174.5 -5.4
5/23/2019 2:51:59 PM 174.1 -5.8
5/23/2019 2:52:00 PM 173.8 -6.1
5/23/2019 2:52:01 PM 173.5 -6.4
5/23/2019 2:52:02 PM 173.4 -6.5
5/23/2019 2:52:03 PM 173.4 -6.5
5/23/2019 2:52:04 PM 173.3 -6.6
5/23/2019 2:52:05 PM 173.4 -6.5
5/23/2019 2:52:06 PM 173.5 -6.4
5/23/2019 2:52:07 PM 173.8 -6.1
5/23/2019 2:52:08 PM 174.1 -5.8
5/23/2019 2:52:09 PM 174.4 -5.5
5/23/2019 2:52:10 PM 174.7 -5.2
5/23/2019 2:52:11 PM 175.0 -4.9
5/23/2019 2:52:12 PM 175.3 -4.6
5/23/2019 2:52:13 PM 175.5 -4.4
5/23/2019 2:52:14 PM 175.7 -4.2
5/23/2019 2:52:15 PM 175.8 -4.1
5/23/2019 2:52:16 PM 175.8 -4.1
5/23/2019 2:52:17 PM 175.8 -4.1
5/23/2019 2:52:18 PM 175.8 -4.1
5/23/2019 2:52:19 PM 175.7 -4.2
5/23/2019 2:52:20 PM 175.6 -4.3
5/23/2019 2:52:21 PM 175.4 -4.5
5/23/2019 2:52:22 PM 175.2 -4.7
5/23/2019 2:52:23 PM 175.1 -4.8
5/23/2019 2:52:24 PM 174.8 -5.1
5/23/2019 2:52:25 PM 174.5 -5.4
5/23/2019 2:52:26 PM 174.1 -5.8
5/23/2019 2:52:27 PM 173.7 -6.2
5/23/2019 2:52:28 PM 173.2 -6.7
5/23/2019 2:52:29 PM 172.9 -7.0
5/23/2019 2:52:30 PM 172.4 -7.5
5/23/2019 2:52:31 PM 172.1 -7.8
5/23/2019 2:52:32 PM 171.6 -8.3
5/23/2019 2:52:33 PM 171.2 -8.7
5/23/2019 2:52:34 PM 170.8 -9.1
5/23/2019 2:52:35 PM 170.5 -9.4
5/23/2019 2:52:36 PM 170.2 -9.7
5/23/2019 2:52:37 PM 169.9 -10.0
5/23/2019 2:52:38 PM 169.7 -10.2
5/23/2019 2:52:39 PM 169.6 -10.3
5/23/2019 2:52:40 PM 169.5 -10.4
5/23/2019 2:52:41 PM 169.4 -10.5
5/23/2019 2:52:42 PM 169.3 -10.6
5/23/2019 2:52:43 PM 169.2 -10.7
5/23/2019 2:52:44 PM 169.1 -10.8
5/23/2019 2:52:45 PM 169.0 -10.9
5/23/2019 2:52:46 PM 168.9 -11.0
5/23/2019 2:52:47 PM 168.7 -11.2
5/23/2019 2:52:48 PM 168.6 -11.3
5/23/2019 2:52:49 PM 168.4 -11.5
5/23/2019 2:52:50 PM 168.2 -11.7
5/23/2019 2:52:51 PM 168.0 -11.9
5/23/2019 2:52:52 PM 167.8 -12.1
5/23/2019 2:52:53 PM 167.5 -12.4
5/23/2019 2:52:54 PM 167.3 -12.6
5/23/2019 2:52:55 PM 167.0 -12.9
5/23/2019 2:52:56 PM 166.8 -13.1
5/23/2019 2:52:57 PM 166.6 -13.3
5/23/2019 2:52:58 PM 166.4 -13.5
5/23/2019 2:52:59 PM 166.2 -13.7
5/23/2019 2:53:00 PM 166.1 -13.8
5/23/2019 2:53:01 PM 166.0 -13.9
5/23/2019 2:53:02 PM 165.9 -14.0
5/23/2019 2:53:03 PM 165.9 -14.0
5/23/2019 2:53:04 PM 165.8 -14.1
5/23/2019 2:53:05 PM 165.9 -14.0
5/23/2019 2:53:06 PM 165.9 -14.0
5/23/2019 2:53:07 PM 166.0 -13.9
5/23/2019 2:53:08 PM 166.1 -13.8
Page 89 of 452 August 2019
APPENDIX E23: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-3 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-3 Data Log
5/23/2019 2:53:09 PM 166.2 -13.7
5/23/2019 2:53:10 PM 166.4 -13.5
5/23/2019 2:53:11 PM 166.6 -13.3
5/23/2019 2:53:12 PM 166.6 -13.3
5/23/2019 2:53:13 PM 166.7 -13.2
5/23/2019 2:53:14 PM 166.8 -13.1
5/23/2019 2:53:15 PM 166.9 -13.0
5/23/2019 2:53:16 PM 166.9 -13.0
5/23/2019 2:53:17 PM 167.0 -12.9
5/23/2019 2:53:18 PM 167.0 -12.9
5/23/2019 2:53:19 PM 167.0 -12.9
5/23/2019 2:53:20 PM 166.9 -13.0
5/23/2019 2:53:21 PM 166.9 -13.0
5/23/2019 2:53:22 PM 166.8 -13.1
5/23/2019 2:53:23 PM 166.7 -13.2
5/23/2019 2:53:24 PM 166.5 -13.4
5/23/2019 2:53:25 PM 166.4 -13.5
5/23/2019 2:53:26 PM 166.2 -13.7
5/23/2019 2:53:27 PM 166.0 -13.9
5/23/2019 2:53:28 PM 165.8 -14.1
5/23/2019 2:53:29 PM 165.6 -14.3
5/23/2019 2:53:30 PM 165.4 -14.5
5/23/2019 2:53:31 PM 165.1 -14.8
5/23/2019 2:53:32 PM 164.9 -15.0
5/23/2019 2:53:33 PM 164.6 -15.3
5/23/2019 2:53:34 PM 164.4 -15.5
5/23/2019 2:53:35 PM 164.2 -15.7
5/23/2019 2:53:36 PM 164.0 -15.9
5/23/2019 2:53:37 PM 163.9 -16.0
5/23/2019 2:53:38 PM 163.8 -16.1
5/23/2019 2:53:39 PM 163.8 -16.1
5/23/2019 2:53:40 PM 163.7 -16.2
5/23/2019 2:53:41 PM 163.7 -16.2
5/23/2019 2:53:42 PM 163.6 -16.3
5/23/2019 2:53:43 PM 163.6 -16.3
5/23/2019 2:53:44 PM 163.6 -16.3
5/23/2019 2:53:45 PM 163.6 -16.3
5/23/2019 2:53:46 PM 163.6 -16.3
5/23/2019 2:53:47 PM 163.6 -16.3
5/23/2019 2:53:48 PM 163.5 -16.4
5/23/2019 2:53:49 PM 163.4 -16.5
5/23/2019 2:53:50 PM 163.3 -16.6
5/23/2019 2:53:51 PM 163.2 -16.7
5/23/2019 2:53:52 PM 163.0 -16.9
5/23/2019 2:53:53 PM 162.8 -17.1
5/23/2019 2:53:54 PM 162.6 -17.3
5/23/2019 2:53:55 PM 162.4 -17.5
5/23/2019 2:53:56 PM 162.1 -17.8
5/23/2019 2:53:57 PM 161.9 -18.0
5/23/2019 2:53:58 PM 161.6 -18.3
5/23/2019 2:53:59 PM 161.3 -18.6
5/23/2019 2:54:00 PM 161.0 -18.9
5/23/2019 2:54:01 PM 160.7 -19.2
5/23/2019 2:54:02 PM 160.4 -19.5
5/23/2019 2:54:03 PM 160.0 -19.9
5/23/2019 2:54:04 PM 159.7 -20.2
5/23/2019 2:54:05 PM 159.2 -20.7
5/23/2019 2:54:06 PM 158.8 -21.1
5/23/2019 2:54:07 PM 158.4 -21.5
5/23/2019 2:54:08 PM 158.0 -21.9
5/23/2019 2:54:09 PM 157.5 -22.4
5/23/2019 2:54:10 PM 157.1 -22.8
5/23/2019 2:54:11 PM 156.5 -23.4
5/23/2019 2:54:12 PM 156.1 -23.8
5/23/2019 2:54:13 PM 155.7 -24.2
5/23/2019 2:54:14 PM 155.2 -24.7
5/23/2019 2:54:15 PM 154.9 -25.0
5/23/2019 2:54:16 PM 154.6 -25.3
5/23/2019 2:54:17 PM 154.4 -25.5
5/23/2019 2:54:18 PM 154.3 -25.6
5/23/2019 2:54:19 PM 154.2 -25.7
5/23/2019 2:54:20 PM 154.1 -25.8
5/23/2019 2:54:21 PM 154.0 -25.9
5/23/2019 2:54:22 PM 154.1 -25.8
5/23/2019 2:54:23 PM 154.1 -25.8
5/23/2019 2:54:24 PM 154.3 -25.6
5/23/2019 2:54:25 PM 154.4 -25.5
5/23/2019 2:54:26 PM 154.5 -25.4
5/23/2019 2:54:27 PM 154.6 -25.3
5/23/2019 2:54:28 PM 154.7 -25.2
Page 90 of 452 August 2019
APPENDIX E23: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-3 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-3 Data Log
5/23/2019 2:54:29 PM 154.7 -25.2
5/23/2019 2:54:30 PM 154.7 -25.2
5/23/2019 2:54:31 PM 154.7 -25.2
5/23/2019 2:54:32 PM 154.7 -25.2
5/23/2019 2:54:33 PM 154.6 -25.3
5/23/2019 2:54:34 PM 154.6 -25.3
5/23/2019 2:54:35 PM 154.6 -25.3
5/23/2019 2:54:36 PM 154.5 -25.4
5/23/2019 2:54:37 PM 154.5 -25.4
5/23/2019 2:54:38 PM 154.5 -25.4
5/23/2019 2:54:39 PM 154.5 -25.4
5/23/2019 2:54:40 PM 154.5 -25.4
5/23/2019 2:54:41 PM 154.5 -25.4
5/23/2019 2:54:42 PM 154.5 -25.4
5/23/2019 2:54:43 PM 154.5 -25.4
5/23/2019 2:54:44 PM 154.6 -25.3
5/23/2019 2:54:45 PM 154.6 -25.3
5/23/2019 2:54:46 PM 154.6 -25.3
5/23/2019 2:54:47 PM 154.5 -25.4
5/23/2019 2:54:48 PM 154.5 -25.4
5/23/2019 2:54:49 PM 154.4 -25.5
5/23/2019 2:54:50 PM 154.3 -25.6
5/23/2019 2:54:51 PM 154.3 -25.6
5/23/2019 2:54:52 PM 154.1 -25.8
5/23/2019 2:54:53 PM 154.0 -25.9
5/23/2019 2:54:54 PM 153.8 -26.1
5/23/2019 2:54:55 PM 153.6 -26.3
5/23/2019 2:54:56 PM 153.3 -26.6
5/23/2019 2:54:57 PM 153.0 -26.9
5/23/2019 2:54:58 PM 152.8 -27.1
5/23/2019 2:54:59 PM 152.5 -27.4
5/23/2019 2:55:00 PM 152.2 -27.7
5/23/2019 2:55:01 PM 151.9 -28.0
5/23/2019 2:55:02 PM 151.4 -28.5
5/23/2019 2:55:03 PM 151.2 -28.7
5/23/2019 2:55:04 PM 150.7 -29.2
5/23/2019 2:55:05 PM 150.5 -29.4
5/23/2019 2:55:06 PM 150.2 -29.7
5/23/2019 2:55:07 PM 149.8 -30.1
5/23/2019 2:55:08 PM 149.6 -30.3
5/23/2019 2:55:09 PM 149.4 -30.5
5/23/2019 2:55:10 PM 149.1 -30.8
5/23/2019 2:55:11 PM 148.9 -31.0
5/23/2019 2:55:12 PM 148.7 -31.2
5/23/2019 2:55:13 PM 148.6 -31.3
5/23/2019 2:55:14 PM 148.5 -31.4
5/23/2019 2:55:15 PM 148.4 -31.5
5/23/2019 2:55:16 PM 148.2 -31.7
5/23/2019 2:55:17 PM 148.1 -31.8
5/23/2019 2:55:18 PM 148.0 -31.9
5/23/2019 2:55:19 PM 147.8 -32.1
5/23/2019 2:55:20 PM 147.7 -32.2
Page 91 of 452 August 2019
APPENDIX E23: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-3 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-A1 TEST-3 1418
SEEP-A1 TEST-3 1419
SEEP-A1 TEST-3 1420
SEEP-A1 TEST-3 1421
SEEP-A1 TEST-3 1422
Geo Mean
Average (pre-test)
Average (post-test)
Location EC Reading
(µS/cms)
SEEP-A1 TEST-3 39.4
SEEP-A1 TEST-3 180
SEEP-A1 TEST-3 453
SEEP-A1 TEST-3 3,480
SEEP-A1 TEST-3 15,600
SEEP-A1 TEST-3 129,760
q 299,800 mg
K 1.3004 (µS/cms) / (mg/L)
Q 3.7 L/s
58.8 GPM
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Location Time Background Stream EC Background Stream Temperature
1 25.8
174.7 19.7
175.9 19.7
Average 176.4 (µS/cms)
Table E3 SEEP-A1 TEST-3 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
(mg/L)(°C)
10 25.3
100 24.6
1,000 25.2
Slope of Calibration Curve
Integral of Conductivity Data Curve
Calculated Flow Rate
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement Part 2:
Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8, no. 1, 2004, pp.
11–15.
10000 26.3
100,000 25.9
Table E4 SEEP-A1 TEST-3 Flow Calculation Summary
Mass of Salt injected
(s) . (µS/cms)105257SUM:Δt(ECt-ECbkg)
(µS/cms)
(µS/cms)
(µS/cms)
163.1
179.9
176.4
173.0 19.5
179.6 19.6
179.0 19.6
(µS/cms)(°C)
Table E2 SEEP-A1 TEST-3 Stream Background Conductivity Data
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 92 of 452 August 2019
APPENDIX E24: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 11:21:29 AM 132.5 -
6/7/2019 11:21:30 AM 132.5 -
6/7/2019 11:21:31 AM 132.5 -
6/7/2019 11:21:32 AM 132.5 -
6/7/2019 11:21:33 AM 132.5 -
6/7/2019 11:21:34 AM 132.6 -
6/7/2019 11:21:35 AM 132.6 -
6/7/2019 11:21:36 AM 132.6 -
6/7/2019 11:21:37 AM 132.5 -
6/7/2019 11:21:38 AM 132.5 -
6/7/2019 11:21:39 AM 132.5 -
6/7/2019 11:21:40 AM 132.5 -
6/7/2019 11:21:41 AM 132.5 -
6/7/2019 11:21:42 AM 132.5 -
6/7/2019 11:21:43 AM 132.5 -
6/7/2019 11:21:44 AM 132.6 -
6/7/2019 11:21:45 AM 132.6 -
6/7/2019 11:21:46 AM 132.6 -
6/7/2019 11:21:47 AM 132.7 -
6/7/2019 11:21:48 AM 132.7 -
6/7/2019 11:21:49 AM 132.7 -
6/7/2019 11:21:50 AM 132.8 -
6/7/2019 11:21:51 AM 132.8 -
6/7/2019 11:21:52 AM 132.8 -
6/7/2019 11:21:53 AM 133.1 -
6/7/2019 11:21:54 AM 363.0 230.4
6/7/2019 11:21:55 AM 659.3 526.7
6/7/2019 11:21:56 AM 2317.4 2184.8
6/7/2019 11:21:57 AM 3486.7 3354.1
6/7/2019 11:21:58 AM 4258.2 4125.6
6/7/2019 11:21:59 AM 5047.8 4915.2
6/7/2019 11:22:00 AM 5166.2 5033.6
6/7/2019 11:22:01 AM 5147.5 5014.9
6/7/2019 11:22:02 AM 4479.8 4347.2
6/7/2019 11:22:03 AM 3847.1 3714.5
6/7/2019 11:22:04 AM 3423.0 3290.4
6/7/2019 11:22:05 AM 2947.7 2815.1
6/7/2019 11:22:06 AM 2604.1 2471.5
6/7/2019 11:22:07 AM 2137.7 2005.1
6/7/2019 11:22:08 AM 1971.2 1838.6
6/7/2019 11:22:09 AM 1598.9 1466.3
6/7/2019 11:22:10 AM 1462.3 1329.7
6/7/2019 11:22:11 AM 1255.6 1123.0
6/7/2019 11:22:12 AM 1110.6 978.0
6/7/2019 11:22:13 AM 975.7 843.1
6/7/2019 11:22:14 AM 853.7 721.1
6/7/2019 11:22:15 AM 789.8 657.2
6/7/2019 11:22:16 AM 699.8 567.2
6/7/2019 11:22:17 AM 641.9 509.3
6/7/2019 11:22:18 AM 586.8 454.2
6/7/2019 11:22:19 AM 495.6 363.0
6/7/2019 11:22:20 AM 502.6 370.0
6/7/2019 11:22:21 AM 481.8 349.2
6/7/2019 11:22:22 AM 409.2 276.6
6/7/2019 11:22:23 AM 383.0 250.4
6/7/2019 11:22:24 AM 351.1 218.5
6/7/2019 11:22:25 AM 332.6 200.0
6/7/2019 11:22:26 AM 323.2 190.6
6/7/2019 11:22:27 AM 312.0 179.4
6/7/2019 11:22:28 AM 301.0 168.4
6/7/2019 11:22:29 AM 293.8 161.2
6/7/2019 11:22:30 AM 286.6 154.0
6/7/2019 11:22:31 AM 236.0 103.4
6/7/2019 11:22:32 AM 224.2 91.6
6/7/2019 11:22:33 AM 214.9 82.3
6/7/2019 11:22:34 AM 212.1 79.5
6/7/2019 11:22:35 AM 209.4 76.8
6/7/2019 11:22:36 AM 204.6 72.0
6/7/2019 11:22:37 AM 200.3 67.7
Table E1 SEEP-A1 TEST-1 Data Log
Page 93 of 452 August 2019
APPENDIX E24: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-1 Data Log
6/7/2019 11:22:38 AM 197.2 64.6
6/7/2019 11:22:39 AM 194.1 61.5
6/7/2019 11:22:40 AM 191.6 59.0
6/7/2019 11:22:41 AM 189.0 56.4
6/7/2019 11:22:42 AM 186.9 54.3
6/7/2019 11:22:43 AM 184.7 52.1
6/7/2019 11:22:44 AM 183.0 50.4
6/7/2019 11:22:45 AM 181.1 48.5
6/7/2019 11:22:46 AM 179.5 46.9
6/7/2019 11:22:47 AM 177.1 44.5
6/7/2019 11:22:48 AM 173.6 41.0
6/7/2019 11:22:49 AM 170.1 37.5
6/7/2019 11:22:50 AM 167.5 34.9
6/7/2019 11:22:51 AM 164.8 32.2
6/7/2019 11:22:52 AM 162.7 30.1
6/7/2019 11:22:53 AM 160.6 28.0
6/7/2019 11:22:54 AM 159.0 26.4
6/7/2019 11:22:55 AM 157.3 24.7
6/7/2019 11:22:56 AM 155.9 23.3
6/7/2019 11:22:57 AM 154.5 21.9
6/7/2019 11:22:58 AM 153.2 20.6
6/7/2019 11:22:59 AM 152.2 19.6
6/7/2019 11:23:00 AM 151.1 18.5
6/7/2019 11:23:01 AM 150.3 17.7
6/7/2019 11:23:02 AM 149.3 16.7
6/7/2019 11:23:03 AM 148.5 15.9
6/7/2019 11:23:04 AM 147.7 15.1
6/7/2019 11:23:05 AM 147.0 14.4
6/7/2019 11:23:06 AM 146.2 13.6
6/7/2019 11:23:07 AM 145.6 13.0
6/7/2019 11:23:08 AM 144.9 12.3
6/7/2019 11:23:09 AM 144.4 11.8
6/7/2019 11:23:10 AM 143.9 11.3
6/7/2019 11:23:11 AM 143.5 10.9
6/7/2019 11:23:12 AM 143.0 10.4
6/7/2019 11:23:13 AM 142.7 10.1
6/7/2019 11:23:14 AM 142.2 9.6
6/7/2019 11:23:15 AM 141.9 9.3
6/7/2019 11:23:16 AM 141.5 8.9
6/7/2019 11:23:17 AM 141.3 8.7
6/7/2019 11:23:18 AM 141.0 8.4
6/7/2019 11:23:19 AM 140.7 8.1
6/7/2019 11:23:20 AM 140.5 7.9
6/7/2019 11:23:21 AM 140.2 7.6
6/7/2019 11:23:22 AM 139.9 7.3
6/7/2019 11:23:23 AM 139.6 7.0
6/7/2019 11:23:24 AM 139.4 6.8
6/7/2019 11:23:25 AM 139.1 6.5
6/7/2019 11:23:26 AM 138.9 6.3
6/7/2019 11:23:27 AM 138.7 6.1
6/7/2019 11:23:28 AM 138.5 5.9
6/7/2019 11:23:29 AM 138.3 5.7
6/7/2019 11:23:30 AM 138.1 5.5
6/7/2019 11:23:31 AM 137.9 5.3
6/7/2019 11:23:32 AM 137.7 5.1
6/7/2019 11:23:33 AM 137.6 5.0
6/7/2019 11:23:34 AM 137.4 4.8
6/7/2019 11:23:35 AM 137.3 4.7
6/7/2019 11:23:36 AM 137.2 4.6
6/7/2019 11:23:37 AM 137.0 4.4
6/7/2019 11:23:38 AM 136.9 4.3
6/7/2019 11:23:39 AM 136.8 4.2
6/7/2019 11:23:40 AM 136.6 4.0
6/7/2019 11:23:41 AM 136.5 3.9
6/7/2019 11:23:42 AM 136.4 3.8
6/7/2019 11:23:43 AM 136.3 3.7
6/7/2019 11:23:44 AM 136.1 3.5
6/7/2019 11:23:45 AM 136.0 3.4
6/7/2019 11:23:46 AM 135.9 3.3
6/7/2019 11:23:47 AM 135.8 3.2
6/7/2019 11:23:48 AM 135.7 3.1
6/7/2019 11:23:49 AM 135.6 3.0
6/7/2019 11:23:50 AM 135.6 3.0
6/7/2019 11:23:51 AM 135.7 3.1
6/7/2019 11:23:52 AM 135.9 3.3
6/7/2019 11:23:53 AM 136.1 3.5
6/7/2019 11:23:54 AM 136.5 3.9
Page 94 of 452 August 2019
APPENDIX E24: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-1 Data Log
6/7/2019 11:23:55 AM 136.9 4.3
6/7/2019 11:23:56 AM 137.3 4.7
6/7/2019 11:23:57 AM 137.7 5.1
6/7/2019 11:23:58 AM 138.2 5.6
6/7/2019 11:23:59 AM 138.6 6.0
6/7/2019 11:24:00 AM 139.0 6.4
6/7/2019 11:24:01 AM 139.4 6.8
6/7/2019 11:24:02 AM 139.7 7.1
6/7/2019 11:24:03 AM 140.0 7.4
6/7/2019 11:24:04 AM 140.2 7.6
6/7/2019 11:24:05 AM 140.3 7.7
6/7/2019 11:24:06 AM 140.3 7.7
6/7/2019 11:24:07 AM 140.3 7.7
6/7/2019 11:24:08 AM 140.2 7.6
6/7/2019 11:24:09 AM 140.1 7.5
6/7/2019 11:24:10 AM 139.9 7.3
6/7/2019 11:24:11 AM 139.8 7.2
6/7/2019 11:24:12 AM 139.6 7.0
6/7/2019 11:24:13 AM 139.5 6.9
6/7/2019 11:24:14 AM 139.4 6.8
6/7/2019 11:24:15 AM 139.2 6.6
6/7/2019 11:24:16 AM 139.1 6.5
6/7/2019 11:24:17 AM 138.9 6.3
6/7/2019 11:24:18 AM 138.7 6.1
6/7/2019 11:24:19 AM 138.4 5.8
6/7/2019 11:24:20 AM 138.1 5.5
6/7/2019 11:24:21 AM 137.8 5.2
6/7/2019 11:24:22 AM 137.5 4.9
6/7/2019 11:24:23 AM 137.2 4.6
6/7/2019 11:24:24 AM 136.8 4.2
6/7/2019 11:24:25 AM 136.5 3.9
6/7/2019 11:24:26 AM 136.2 3.6
6/7/2019 11:24:27 AM 135.9 3.3
6/7/2019 11:24:28 AM 135.6 3.0
6/7/2019 11:24:29 AM 135.3 2.7
6/7/2019 11:24:30 AM 135.1 2.5
6/7/2019 11:24:31 AM 134.9 2.3
6/7/2019 11:24:32 AM 134.8 2.2
6/7/2019 11:24:33 AM 134.6 2.0
6/7/2019 11:24:34 AM 134.5 1.9
6/7/2019 11:24:35 AM 134.5 1.9
6/7/2019 11:24:36 AM 134.4 1.8
6/7/2019 11:24:37 AM 134.4 1.8
6/7/2019 11:24:38 AM 134.3 1.7
6/7/2019 11:24:39 AM 134.3 1.7
6/7/2019 11:24:40 AM 134.2 1.6
6/7/2019 11:24:41 AM 134.1 1.5
6/7/2019 11:24:42 AM 134.0 1.4
6/7/2019 11:24:43 AM 133.9 1.3
6/7/2019 11:24:44 AM 133.8 1.2
6/7/2019 11:24:45 AM 133.7 1.1
6/7/2019 11:24:46 AM 133.6 1.0
6/7/2019 11:24:47 AM 133.5 0.9
6/7/2019 11:24:48 AM 133.4 0.8
6/7/2019 11:24:49 AM 133.2 0.6
6/7/2019 11:24:50 AM 133.1 0.5
6/7/2019 11:24:51 AM 133.0 0.4
6/7/2019 11:24:52 AM 132.9 0.3
6/7/2019 11:24:53 AM 132.7 0.1
6/7/2019 11:24:54 AM 132.6 0.0
6/7/2019 11:24:55 AM 132.5 -0.1
6/7/2019 11:24:56 AM 132.5 -0.1
6/7/2019 11:24:57 AM 132.4 -0.2
6/7/2019 11:24:58 AM 132.3 -0.3
6/7/2019 11:24:59 AM 132.2 -0.4
6/7/2019 11:25:00 AM 132.2 -0.4
6/7/2019 11:25:01 AM 132.1 -0.5
6/7/2019 11:25:02 AM 132.0 -0.6
6/7/2019 11:25:03 AM 132.0 -0.6
6/7/2019 11:25:04 AM 132.0 -0.6
6/7/2019 11:25:05 AM 131.9 -0.7
6/7/2019 11:25:06 AM 131.9 -0.7
6/7/2019 11:25:07 AM 131.9 -0.7
6/7/2019 11:25:08 AM 131.9 -0.7
6/7/2019 11:25:09 AM 131.8 -0.8
6/7/2019 11:25:10 AM 131.8 -0.8
6/7/2019 11:25:11 AM 131.8 -0.8
6/7/2019 11:25:12 AM 131.8 -0.8
6/7/2019 11:25:13 AM 131.8 -0.8
Page 95 of 452 August 2019
APPENDIX E24: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-1 Data Log
6/7/2019 11:25:14 AM 131.8 -0.8
6/7/2019 11:25:15 AM 131.7 -0.9
6/7/2019 11:25:16 AM 131.7 -0.9
6/7/2019 11:25:17 AM 131.7 -0.9
6/7/2019 11:25:18 AM 131.7 -0.9
6/7/2019 11:25:19 AM 131.7 -0.9
6/7/2019 11:25:20 AM 131.6 -1.0
6/7/2019 11:25:21 AM 131.6 -1.0
6/7/2019 11:25:22 AM 131.5 -1.1
6/7/2019 11:25:23 AM 131.5 -1.1
6/7/2019 11:25:24 AM 131.4 -1.2
6/7/2019 11:25:25 AM 131.3 -1.3
6/7/2019 11:25:26 AM 131.3 -1.3
6/7/2019 11:25:27 AM 131.2 -1.4
6/7/2019 11:25:28 AM 131.1 -1.5
6/7/2019 11:25:29 AM 131.0 -1.6
6/7/2019 11:25:30 AM 130.9 -1.7
6/7/2019 11:25:31 AM 130.9 -1.7
6/7/2019 11:25:32 AM 130.8 -1.8
6/7/2019 11:25:33 AM 130.7 -1.9
6/7/2019 11:25:34 AM 130.6 -2.0
6/7/2019 11:25:35 AM 130.6 -2.0
6/7/2019 11:25:36 AM 130.5 -2.1
6/7/2019 11:25:37 AM 130.4 -2.2
6/7/2019 11:25:38 AM 130.4 -2.2
6/7/2019 11:25:39 AM 130.3 -2.3
6/7/2019 11:25:40 AM 130.3 -2.3
6/7/2019 11:25:41 AM 130.2 -2.4
6/7/2019 11:25:42 AM 130.2 -2.4
6/7/2019 11:25:43 AM 130.1 -2.5
6/7/2019 11:25:44 AM 130.1 -2.5
6/7/2019 11:25:45 AM 130.0 -2.6
6/7/2019 11:25:46 AM 130.0 -2.6
6/7/2019 11:25:47 AM 129.9 -2.7
6/7/2019 11:25:48 AM 129.9 -2.7
6/7/2019 11:25:49 AM 129.8 -2.8
6/7/2019 11:25:50 AM 129.8 -2.8
6/7/2019 11:25:51 AM 129.7 -2.9
6/7/2019 11:25:52 AM 129.7 -2.9
6/7/2019 11:25:53 AM 129.6 -3.0
6/7/2019 11:25:54 AM 129.6 -3.0
6/7/2019 11:25:55 AM 129.5 -3.1
6/7/2019 11:25:56 AM 129.5 -3.1
6/7/2019 11:25:57 AM 129.4 -3.2
6/7/2019 11:25:58 AM 129.4 -3.2
6/7/2019 11:25:59 AM 129.3 -3.3
6/7/2019 11:26:00 AM 129.3 -3.3
6/7/2019 11:26:01 AM 129.3 -3.3
6/7/2019 11:26:02 AM 129.3 -3.3
6/7/2019 11:26:03 AM 129.2 -3.4
6/7/2019 11:26:04 AM 129.2 -3.4
6/7/2019 11:26:05 AM 129.2 -3.4
6/7/2019 11:26:06 AM 129.2 -3.4
6/7/2019 11:26:07 AM 129.1 -3.5
6/7/2019 11:26:08 AM 129.1 -3.5
6/7/2019 11:26:09 AM 129.1 -3.5
6/7/2019 11:26:10 AM 129.1 -3.5
6/7/2019 11:26:11 AM 129.1 -3.5
6/7/2019 11:26:12 AM 129.0 -3.6
6/7/2019 11:26:13 AM 129.0 -3.6
6/7/2019 11:26:14 AM 129.0 -3.6
6/7/2019 11:26:15 AM 129.0 -3.6
6/7/2019 11:26:16 AM 129.0 -3.6
6/7/2019 11:26:17 AM 129.0 -3.6
6/7/2019 11:26:18 AM 129.0 -3.6
6/7/2019 11:26:19 AM 129.0 -3.6
6/7/2019 11:26:20 AM 129.0 -3.6
6/7/2019 11:26:21 AM 129.0 -3.6
6/7/2019 11:26:22 AM 129.0 -3.6
6/7/2019 11:26:23 AM 129.0 -3.6
6/7/2019 11:26:24 AM 129.0 -3.6
6/7/2019 11:26:25 AM 129.1 -3.5
6/7/2019 11:26:26 AM 129.1 -3.5
6/7/2019 11:26:27 AM 129.1 -3.5
6/7/2019 11:26:28 AM 129.1 -3.5
6/7/2019 11:26:29 AM 129.1 -3.5
6/7/2019 11:26:30 AM 129.1 -3.5
6/7/2019 11:26:31 AM 129.1 -3.5
6/7/2019 11:26:32 AM 129.1 -3.5
6/7/2019 11:26:33 AM 129.1 -3.5
6/7/2019 11:26:34 AM 129.0 -3.6
6/7/2019 11:26:35 AM 129.0 -3.6
6/7/2019 11:26:36 AM 129.0 -3.6
6/7/2019 11:26:37 AM 129.0 -3.6
Page 96 of 452 August 2019
APPENDIX E24: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-A1 TEST-1 1054
SEEP-A1 TEST-1 1055
SEEP-A1 TEST-1 1100
SEEP-A1 TEST-1 1102
SEEP-A1 TEST-1 NR
Average
Geo Mean
Average (pre-test)
Average (post-test)
Location EC Reading
(µS/cms)
SEEP-A1 TEST-1 245
SEEP-A1 TEST-1 2,160
SEEP-A1 TEST-1 18,420
SEEP-A1 TEST-1 135,005
q 300,000 mg
K 1.3550 (µS/cms) / (mg/L)
(s) . (µS/cms)
Q 6.9 L/s
108.9 GPM
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
NR Not recorded
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)(°C)
Table E2 SEEP-A1 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC Background Stream Temperature
129.6 21.12
130.6 21.2
Table E3 SEEP-A1 TEST-1 YSI Salt Dilution Calibration Data
21.1
131.00 21.1
128.9 21.1
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement Part 2:
Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8, no. 1, 2004,
pp. 11–15.
(mg/L)(°C)
10000 NR
100,000 NR
Table E4 SEEP-A1 TEST-1 Flow Calculation Summary
Mass of Salt injected
Slope of Calibration Curve
Integral of Conductivity Data
Curve
Calculated Flow Rate
55260SUM:Δt(ECt-
ECbkg)
NR
NR
1,000
100
131.2
132.6
130.3
130.3 (µS/cms)
(µS/cms)
(µS/cms)
(µS/cms)
Calibration Concentration Temperature
131.6
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 97 of 452 August 2019
APPENDIX E25: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 11:31:57 AM 128.5 -
6/7/2019 11:31:58 AM 128.4 -
6/7/2019 11:31:59 AM 128.4 -
6/7/2019 11:32:00 AM 128.3 -
6/7/2019 11:32:01 AM 128.4 -
6/7/2019 11:32:02 AM 128.3 -
6/7/2019 11:32:03 AM 128.1 -
6/7/2019 11:32:04 AM 128.0 -
6/7/2019 11:32:05 AM 128.0 -
6/7/2019 11:32:06 AM 128.1 -
6/7/2019 11:32:07 AM 128.1 -
6/7/2019 11:32:08 AM 128.0 -
6/7/2019 11:32:09 AM 127.9 -
6/7/2019 11:32:10 AM 127.8 -
6/7/2019 11:32:11 AM 127.8 -
6/7/2019 11:32:12 AM 127.8 -
6/7/2019 11:32:13 AM 127.8 -
6/7/2019 11:32:14 AM 127.8 -
6/7/2019 11:32:15 AM 127.8 -
6/7/2019 11:32:16 AM 127.8 -
6/7/2019 11:32:17 AM 127.9 -
6/7/2019 11:32:18 AM 128.0 -
6/7/2019 11:32:19 AM 128.0 -
6/7/2019 11:32:20 AM 128.0 -
6/7/2019 11:32:21 AM 128.1 -
6/7/2019 11:32:22 AM 128.3 -
6/7/2019 11:32:23 AM 128.4 -
6/7/2019 11:32:24 AM 128.6 -
6/7/2019 11:32:25 AM 129.6 -
6/7/2019 11:32:26 AM 395.4 267.3
6/7/2019 11:32:27 AM 648.0 519.9
6/7/2019 11:32:28 AM 2436.8 2308.7
6/7/2019 11:32:29 AM 3134.3 3006.2
6/7/2019 11:32:30 AM 4180.7 4052.6
6/7/2019 11:32:31 AM 4529.2 4401.1
6/7/2019 11:32:32 AM 4472.9 4344.8
6/7/2019 11:32:33 AM 4371.8 4243.7
6/7/2019 11:32:34 AM 3653.2 3525.1
6/7/2019 11:32:35 AM 3169.5 3041.4
6/7/2019 11:32:36 AM 2705.3 2577.2
6/7/2019 11:32:37 AM 2285.6 2157.5
6/7/2019 11:32:38 AM 1896.7 1768.6
6/7/2019 11:32:39 AM 1684.7 1556.6
6/7/2019 11:32:40 AM 1450.2 1322.1
6/7/2019 11:32:41 AM 1226.3 1098.2
6/7/2019 11:32:42 AM 1052.8 924.7
6/7/2019 11:32:43 AM 937.6 809.5
6/7/2019 11:32:44 AM 807.6 679.5
6/7/2019 11:32:45 AM 708.6 580.5
6/7/2019 11:32:46 AM 646.6 518.5
6/7/2019 11:32:47 AM 614.5 486.4
6/7/2019 11:32:48 AM 480.4 352.3
6/7/2019 11:32:49 AM 484.3 356.2
6/7/2019 11:32:50 AM 455.2 327.1
6/7/2019 11:32:51 AM 430.6 302.5
6/7/2019 11:32:52 AM 411.5 283.4
6/7/2019 11:32:53 AM 393.4 265.3
6/7/2019 11:32:54 AM 381.8 253.7
6/7/2019 11:32:55 AM 317.4 189.3
6/7/2019 11:32:56 AM 302.1 174.0
6/7/2019 11:32:57 AM 284.6 156.5
6/7/2019 11:32:58 AM 279.5 151.4
6/7/2019 11:32:59 AM 271.7 143.6
6/7/2019 11:33:00 AM 266.6 138.5
6/7/2019 11:33:01 AM 261.1 133.0
6/7/2019 11:33:02 AM 256.9 128.8
6/7/2019 11:33:03 AM 252.1 124.0
6/7/2019 11:33:04 AM 248.2 120.1
6/7/2019 11:33:05 AM 244.0 115.9
6/7/2019 11:33:06 AM 240.0 111.9
Table E1 SEEP-A1 TEST-2 Data Log
Page 98 of 452 August 2019
APPENDIX E25: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-2 Data Log
6/7/2019 11:33:07 AM 236.9 108.8
6/7/2019 11:33:08 AM 233.6 105.5
6/7/2019 11:33:09 AM 230.9 102.8
6/7/2019 11:33:10 AM 228.1 100.0
6/7/2019 11:33:11 AM 223.2 95.1
6/7/2019 11:33:12 AM 217.1 89.0
6/7/2019 11:33:13 AM 212.2 84.1
6/7/2019 11:33:14 AM 207.2 79.1
6/7/2019 11:33:15 AM 203.2 75.1
6/7/2019 11:33:16 AM 199.2 71.1
6/7/2019 11:33:17 AM 196.1 68.0
6/7/2019 11:33:18 AM 192.9 64.8
6/7/2019 11:33:19 AM 190.4 62.3
6/7/2019 11:33:20 AM 187.8 59.7
6/7/2019 11:33:21 AM 185.7 57.6
6/7/2019 11:33:22 AM 183.5 55.4
6/7/2019 11:33:23 AM 181.6 53.5
6/7/2019 11:33:24 AM 179.7 51.6
6/7/2019 11:33:25 AM 177.9 49.8
6/7/2019 11:33:26 AM 176.6 48.5
6/7/2019 11:33:27 AM 175.1 47.0
6/7/2019 11:33:28 AM 173.9 45.8
6/7/2019 11:33:29 AM 172.6 44.5
6/7/2019 11:33:30 AM 171.6 43.5
6/7/2019 11:33:31 AM 170.5 42.4
6/7/2019 11:33:32 AM 169.7 41.6
6/7/2019 11:33:33 AM 168.8 40.7
6/7/2019 11:33:34 AM 168.0 39.9
6/7/2019 11:33:35 AM 167.2 39.1
6/7/2019 11:33:36 AM 166.5 38.4
6/7/2019 11:33:37 AM 165.8 37.7
6/7/2019 11:33:38 AM 165.2 37.1
6/7/2019 11:33:39 AM 164.6 36.5
6/7/2019 11:33:40 AM 164.0 35.9
6/7/2019 11:33:41 AM 163.5 35.4
6/7/2019 11:33:42 AM 163.0 34.9
6/7/2019 11:33:43 AM 162.5 34.4
6/7/2019 11:33:44 AM 162.1 34.0
6/7/2019 11:33:45 AM 161.7 33.6
6/7/2019 11:33:46 AM 161.3 33.2
6/7/2019 11:33:47 AM 160.9 32.8
6/7/2019 11:33:48 AM 160.5 32.4
6/7/2019 11:33:49 AM 160.2 32.1
6/7/2019 11:33:50 AM 159.9 31.8
6/7/2019 11:33:51 AM 159.6 31.5
6/7/2019 11:33:52 AM 159.2 31.1
6/7/2019 11:33:53 AM 159.0 30.9
6/7/2019 11:33:54 AM 158.6 30.5
6/7/2019 11:33:55 AM 158.4 30.3
6/7/2019 11:33:56 AM 158.1 30.0
6/7/2019 11:33:57 AM 157.8 29.7
6/7/2019 11:33:58 AM 157.5 29.4
6/7/2019 11:33:59 AM 157.2 29.1
6/7/2019 11:34:00 AM 156.9 28.8
6/7/2019 11:34:01 AM 156.7 28.6
6/7/2019 11:34:02 AM 156.4 28.3
6/7/2019 11:34:03 AM 156.1 28.0
6/7/2019 11:34:04 AM 155.9 27.8
6/7/2019 11:34:05 AM 155.6 27.5
6/7/2019 11:34:06 AM 155.4 27.3
6/7/2019 11:34:07 AM 155.1 27.0
6/7/2019 11:34:08 AM 154.9 26.8
6/7/2019 11:34:09 AM 154.7 26.6
6/7/2019 11:34:10 AM 154.5 26.4
6/7/2019 11:34:11 AM 154.2 26.1
6/7/2019 11:34:12 AM 154.0 25.9
6/7/2019 11:34:13 AM 153.8 25.7
6/7/2019 11:34:14 AM 153.6 25.5
6/7/2019 11:34:15 AM 153.4 25.3
6/7/2019 11:34:16 AM 153.3 25.2
6/7/2019 11:34:17 AM 153.1 25.0
6/7/2019 11:34:18 AM 152.9 24.8
6/7/2019 11:34:19 AM 152.8 24.7
6/7/2019 11:34:20 AM 152.6 24.5
6/7/2019 11:34:21 AM 152.4 24.3
6/7/2019 11:34:22 AM 152.2 24.1
6/7/2019 11:34:23 AM 152.1 24.0
Page 99 of 452 August 2019
APPENDIX E25: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-2 Data Log
6/7/2019 11:34:24 AM 152.0 23.9
6/7/2019 11:34:25 AM 151.8 23.7
6/7/2019 11:34:26 AM 151.7 23.6
6/7/2019 11:34:27 AM 151.6 23.5
6/7/2019 11:34:28 AM 151.5 23.4
6/7/2019 11:34:29 AM 151.3 23.2
6/7/2019 11:34:30 AM 151.2 23.1
6/7/2019 11:34:31 AM 151.1 23.0
6/7/2019 11:34:32 AM 151.0 22.9
6/7/2019 11:34:33 AM 150.9 22.8
6/7/2019 11:34:34 AM 150.8 22.7
6/7/2019 11:34:35 AM 150.7 22.6
6/7/2019 11:34:36 AM 150.6 22.5
6/7/2019 11:34:37 AM 150.5 22.4
6/7/2019 11:34:38 AM 150.4 22.3
6/7/2019 11:34:39 AM 150.4 22.3
6/7/2019 11:34:40 AM 150.3 22.2
6/7/2019 11:34:41 AM 150.2 22.1
6/7/2019 11:34:42 AM 150.1 22.0
6/7/2019 11:34:43 AM 150.0 21.9
6/7/2019 11:34:44 AM 149.9 21.8
6/7/2019 11:34:45 AM 149.9 21.8
6/7/2019 11:34:46 AM 149.8 21.7
6/7/2019 11:34:47 AM 149.7 21.6
6/7/2019 11:34:48 AM 149.6 21.5
6/7/2019 11:34:49 AM 149.5 21.4
6/7/2019 11:34:50 AM 149.4 21.3
6/7/2019 11:34:51 AM 149.4 21.3
6/7/2019 11:34:52 AM 149.3 21.2
6/7/2019 11:34:53 AM 149.2 21.1
6/7/2019 11:34:54 AM 149.2 21.1
6/7/2019 11:34:55 AM 149.1 21.0
6/7/2019 11:34:56 AM 149.0 20.9
6/7/2019 11:34:57 AM 149.0 20.9
6/7/2019 11:34:58 AM 148.9 20.8
6/7/2019 11:34:59 AM 148.8 20.7
6/7/2019 11:35:00 AM 148.8 20.7
6/7/2019 11:35:01 AM 148.7 20.6
6/7/2019 11:35:02 AM 148.6 20.5
6/7/2019 11:35:03 AM 148.5 20.4
6/7/2019 11:35:04 AM 148.5 20.4
6/7/2019 11:35:05 AM 148.4 20.3
6/7/2019 11:35:06 AM 148.4 20.3
6/7/2019 11:35:07 AM 148.3 20.2
6/7/2019 11:35:08 AM 148.2 20.1
6/7/2019 11:35:09 AM 148.2 20.1
6/7/2019 11:35:10 AM 148.1 20.0
6/7/2019 11:35:11 AM 148.0 19.9
6/7/2019 11:35:12 AM 147.9 19.8
6/7/2019 11:35:13 AM 147.9 19.8
6/7/2019 11:35:14 AM 147.8 19.7
6/7/2019 11:35:15 AM 147.7 19.6
6/7/2019 11:35:16 AM 147.6 19.5
6/7/2019 11:35:17 AM 147.6 19.5
6/7/2019 11:35:18 AM 147.5 19.4
6/7/2019 11:35:19 AM 147.4 19.3
6/7/2019 11:35:20 AM 147.3 19.2
6/7/2019 11:35:21 AM 147.3 19.2
6/7/2019 11:35:22 AM 147.2 19.1
6/7/2019 11:35:23 AM 147.2 19.1
6/7/2019 11:35:24 AM 147.1 19.0
6/7/2019 11:35:25 AM 147.1 19.0
6/7/2019 11:35:26 AM 147.0 18.9
6/7/2019 11:35:27 AM 147.0 18.9
6/7/2019 11:35:28 AM 146.9 18.8
6/7/2019 11:35:29 AM 146.8 18.7
6/7/2019 11:35:30 AM 146.8 18.7
6/7/2019 11:35:31 AM 146.7 18.6
6/7/2019 11:35:32 AM 146.6 18.5
6/7/2019 11:35:33 AM 146.6 18.5
6/7/2019 11:35:34 AM 146.5 18.4
6/7/2019 11:35:35 AM 146.4 18.3
6/7/2019 11:35:36 AM 146.4 18.3
6/7/2019 11:35:37 AM 146.3 18.2
6/7/2019 11:35:38 AM 146.2 18.1
6/7/2019 11:35:39 AM 146.2 18.1
6/7/2019 11:35:40 AM 146.2 18.1
6/7/2019 11:35:41 AM 146.1 18.0
6/7/2019 11:35:42 AM 146.1 18.0
Page 100 of 452 August 2019
APPENDIX E25: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-2 Data Log
6/7/2019 11:35:43 AM 146.0 17.9
6/7/2019 11:35:44 AM 145.9 17.8
6/7/2019 11:35:45 AM 145.9 17.8
6/7/2019 11:35:46 AM 145.8 17.7
6/7/2019 11:35:47 AM 145.7 17.6
6/7/2019 11:35:48 AM 145.7 17.6
6/7/2019 11:35:49 AM 145.7 17.6
6/7/2019 11:35:50 AM 145.6 17.5
6/7/2019 11:35:51 AM 145.5 17.4
6/7/2019 11:35:52 AM 145.4 17.3
6/7/2019 11:35:53 AM 145.4 17.3
6/7/2019 11:35:54 AM 145.3 17.2
6/7/2019 11:35:55 AM 145.3 17.2
6/7/2019 11:35:56 AM 145.2 17.1
6/7/2019 11:35:57 AM 145.1 17.0
6/7/2019 11:35:58 AM 145.1 17.0
6/7/2019 11:35:59 AM 145.0 16.9
6/7/2019 11:36:00 AM 145.0 16.9
6/7/2019 11:36:01 AM 145.0 16.9
6/7/2019 11:36:02 AM 144.9 16.8
6/7/2019 11:36:03 AM 144.8 16.7
6/7/2019 11:36:04 AM 144.8 16.7
6/7/2019 11:36:05 AM 144.7 16.6
6/7/2019 11:36:06 AM 144.6 16.5
6/7/2019 11:36:07 AM 144.6 16.5
6/7/2019 11:36:08 AM 144.5 16.4
6/7/2019 11:36:09 AM 144.5 16.4
6/7/2019 11:36:10 AM 144.4 16.3
6/7/2019 11:36:11 AM 144.3 16.2
6/7/2019 11:36:12 AM 144.3 16.2
6/7/2019 11:36:13 AM 144.2 16.1
6/7/2019 11:36:14 AM 144.1 16.0
6/7/2019 11:36:15 AM 144.0 15.9
6/7/2019 11:36:16 AM 144.0 15.9
6/7/2019 11:36:17 AM 143.9 15.8
6/7/2019 11:36:18 AM 143.8 15.7
6/7/2019 11:36:19 AM 143.8 15.7
6/7/2019 11:36:20 AM 143.7 15.6
6/7/2019 11:36:21 AM 143.6 15.5
6/7/2019 11:36:22 AM 143.6 15.5
6/7/2019 11:36:23 AM 143.5 15.4
6/7/2019 11:36:24 AM 143.5 15.4
6/7/2019 11:36:25 AM 143.4 15.3
6/7/2019 11:36:26 AM 143.4 15.3
6/7/2019 11:36:27 AM 143.3 15.2
6/7/2019 11:36:28 AM 143.3 15.2
6/7/2019 11:36:29 AM 143.3 15.2
6/7/2019 11:36:30 AM 143.2 15.1
6/7/2019 11:36:31 AM 143.2 15.1
6/7/2019 11:36:32 AM 143.2 15.1
6/7/2019 11:36:33 AM 143.1 15.0
6/7/2019 11:36:34 AM 143.1 15.0
6/7/2019 11:36:35 AM 143.1 15.0
6/7/2019 11:36:36 AM 143.0 14.9
6/7/2019 11:36:37 AM 143.0 14.9
6/7/2019 11:36:38 AM 142.9 14.8
6/7/2019 11:36:39 AM 142.9 14.8
6/7/2019 11:36:40 AM 142.8 14.7
6/7/2019 11:36:41 AM 142.8 14.7
6/7/2019 11:36:42 AM 142.7 14.6
6/7/2019 11:36:43 AM 142.7 14.6
6/7/2019 11:36:44 AM 142.6 14.5
6/7/2019 11:36:45 AM 142.5 14.4
6/7/2019 11:36:46 AM 142.4 14.3
6/7/2019 11:36:47 AM 142.2 14.1
6/7/2019 11:36:48 AM 142.1 14.0
6/7/2019 11:36:49 AM 142.0 13.9
6/7/2019 11:36:50 AM 141.9 13.8
6/7/2019 11:36:51 AM 141.7 13.6
6/7/2019 11:36:52 AM 141.6 13.5
6/7/2019 11:36:53 AM 141.4 13.3
6/7/2019 11:36:54 AM 141.3 13.2
6/7/2019 11:36:55 AM 141.1 13.0
6/7/2019 11:36:56 AM 141.0 12.9
6/7/2019 11:36:57 AM 140.9 12.8
6/7/2019 11:36:58 AM 140.8 12.7
6/7/2019 11:36:59 AM 140.7 12.6
6/7/2019 11:37:00 AM 140.6 12.5
6/7/2019 11:37:01 AM 140.5 12.4
Page 101 of 452 August 2019
APPENDIX E25: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-2 Data Log
6/7/2019 11:37:02 AM 140.4 12.3
6/7/2019 11:37:03 AM 140.3 12.2
6/7/2019 11:37:04 AM 140.2 12.1
6/7/2019 11:37:05 AM 140.2 12.1
6/7/2019 11:37:06 AM 140.1 12.0
6/7/2019 11:37:07 AM 140.0 11.9
6/7/2019 11:37:08 AM 139.9 11.8
6/7/2019 11:37:09 AM 139.9 11.8
6/7/2019 11:37:10 AM 139.8 11.7
6/7/2019 11:37:11 AM 139.8 11.7
6/7/2019 11:37:12 AM 139.7 11.6
6/7/2019 11:37:13 AM 139.6 11.5
6/7/2019 11:37:14 AM 139.6 11.5
6/7/2019 11:37:15 AM 139.5 11.4
6/7/2019 11:37:16 AM 139.4 11.3
6/7/2019 11:37:17 AM 139.4 11.3
6/7/2019 11:37:18 AM 139.3 11.2
6/7/2019 11:37:19 AM 139.2 11.1
6/7/2019 11:37:20 AM 139.1 11.0
6/7/2019 11:37:21 AM 139.1 11.0
6/7/2019 11:37:22 AM 139.0 10.9
6/7/2019 11:37:23 AM 138.9 10.8
6/7/2019 11:37:24 AM 138.8 10.7
6/7/2019 11:37:25 AM 138.7 10.6
6/7/2019 11:37:26 AM 138.6 10.5
6/7/2019 11:37:27 AM 138.6 10.5
6/7/2019 11:37:28 AM 138.5 10.4
6/7/2019 11:37:29 AM 138.4 10.3
6/7/2019 11:37:30 AM 138.3 10.2
6/7/2019 11:37:31 AM 138.2 10.1
6/7/2019 11:37:32 AM 138.1 10.0
6/7/2019 11:37:33 AM 138.0 9.9
6/7/2019 11:37:34 AM 137.9 9.8
6/7/2019 11:37:35 AM 137.8 9.7
6/7/2019 11:37:36 AM 137.7 9.6
6/7/2019 11:37:37 AM 137.6 9.5
6/7/2019 11:37:38 AM 137.5 9.4
6/7/2019 11:37:39 AM 137.4 9.3
6/7/2019 11:37:40 AM 137.3 9.2
6/7/2019 11:37:41 AM 137.2 9.1
6/7/2019 11:37:42 AM 137.2 9.1
6/7/2019 11:37:43 AM 137.0 8.9
6/7/2019 11:37:44 AM 136.9 8.8
6/7/2019 11:37:45 AM 136.8 8.7
6/7/2019 11:37:46 AM 136.7 8.6
6/7/2019 11:37:47 AM 136.5 8.4
6/7/2019 11:37:48 AM 136.3 8.2
6/7/2019 11:37:49 AM 136.2 8.1
6/7/2019 11:37:50 AM 136.0 7.9
6/7/2019 11:37:51 AM 135.9 7.8
6/7/2019 11:37:52 AM 135.7 7.6
6/7/2019 11:37:53 AM 135.6 7.5
6/7/2019 11:37:54 AM 135.4 7.3
6/7/2019 11:37:55 AM 135.3 7.2
6/7/2019 11:37:56 AM 135.1 7.0
6/7/2019 11:37:57 AM 135.0 6.9
6/7/2019 11:37:58 AM 134.9 6.8
6/7/2019 11:37:59 AM 134.8 6.7
6/7/2019 11:38:00 AM 134.7 6.6
6/7/2019 11:38:01 AM 134.7 6.6
6/7/2019 11:38:02 AM 134.6 6.5
6/7/2019 11:38:03 AM 134.5 6.4
6/7/2019 11:38:04 AM 134.5 6.4
6/7/2019 11:38:05 AM 134.4 6.3
6/7/2019 11:38:06 AM 134.4 6.3
6/7/2019 11:38:07 AM 134.3 6.2
6/7/2019 11:38:08 AM 134.3 6.2
6/7/2019 11:38:09 AM 134.2 6.1
6/7/2019 11:38:10 AM 134.2 6.1
6/7/2019 11:38:11 AM 134.1 6.0
6/7/2019 11:38:12 AM 134.1 6.0
6/7/2019 11:38:13 AM 134.0 5.9
6/7/2019 11:38:14 AM 134.0 5.9
6/7/2019 11:38:15 AM 133.9 5.8
6/7/2019 11:38:16 AM 133.9 5.8
6/7/2019 11:38:17 AM 133.9 5.8
6/7/2019 11:38:18 AM 133.8 5.7
6/7/2019 11:38:19 AM 133.8 5.7
6/7/2019 11:38:20 AM 133.8 5.7
Page 102 of 452 August 2019
APPENDIX E25: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-2 Data Log
6/7/2019 11:38:21 AM 133.8 5.7
6/7/2019 11:38:22 AM 133.8 5.7
6/7/2019 11:38:23 AM 133.8 5.7
6/7/2019 11:38:24 AM 133.8 5.7
6/7/2019 11:38:25 AM 133.8 5.7
6/7/2019 11:38:26 AM 133.8 5.7
6/7/2019 11:38:27 AM 133.8 5.7
6/7/2019 11:38:28 AM 133.7 5.6
6/7/2019 11:38:29 AM 133.7 5.6
6/7/2019 11:38:30 AM 133.7 5.6
6/7/2019 11:38:31 AM 133.7 5.6
6/7/2019 11:38:32 AM 133.7 5.6
6/7/2019 11:38:33 AM 133.7 5.6
6/7/2019 11:38:34 AM 133.7 5.6
6/7/2019 11:38:35 AM 133.7 5.6
6/7/2019 11:38:36 AM 133.7 5.6
6/7/2019 11:38:37 AM 133.7 5.6
6/7/2019 11:38:38 AM 133.7 5.6
6/7/2019 11:38:39 AM 133.7 5.6
6/7/2019 11:38:40 AM 133.7 5.6
6/7/2019 11:38:41 AM 133.7 5.6
6/7/2019 11:38:42 AM 133.7 5.6
6/7/2019 11:38:43 AM 133.7 5.6
6/7/2019 11:38:44 AM 133.7 5.6
6/7/2019 11:38:45 AM 133.8 5.7
6/7/2019 11:38:46 AM 133.8 5.7
6/7/2019 11:38:47 AM 133.8 5.7
6/7/2019 11:38:48 AM 133.9 5.8
6/7/2019 11:38:49 AM 133.9 5.8
6/7/2019 11:38:50 AM 134.0 5.9
6/7/2019 11:38:51 AM 134.0 5.9
6/7/2019 11:38:52 AM 134.1 6.0
6/7/2019 11:38:53 AM 134.1 6.0
6/7/2019 11:38:54 AM 134.2 6.1
6/7/2019 11:38:55 AM 134.2 6.1
6/7/2019 11:38:56 AM 134.3 6.2
6/7/2019 11:38:57 AM 134.3 6.2
6/7/2019 11:38:58 AM 134.3 6.2
6/7/2019 11:38:59 AM 134.3 6.2
6/7/2019 11:39:00 AM 134.4 6.3
6/7/2019 11:39:01 AM 134.4 6.3
6/7/2019 11:39:02 AM 134.4 6.3
6/7/2019 11:39:03 AM 134.4 6.3
6/7/2019 11:39:04 AM 134.5 6.4
Page 103 of 452 August 2019
APPENDIX E25: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-A1 TEST-3 1054
SEEP-A1 TEST-3 1055
SEEP-A1 TEST-3 1100
SEEP-A1 TEST-3 1102
SEEP-A1 TEST-3 NR
Average
Geo Mean
Average (pre-test)
Average (post-test)
Location EC Reading
(µS/cms)
SEEP-A1 TEST-3 245
SEEP-A1 TEST-3 2,160
SEEP-A1 TEST-3 18,420
SEEP-A1 TEST-3 135,005
q 300,400 mg
K 1.3550 (µS/cms) / (mg/L)
SUM:Δt(EC
t-ECbkg)55,097.9 (s) . (µS/cms)
Q 7.4 L/s
117.3 GPM
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
NR Not recorded
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms) (°C)
Table E2 SEEP-A1 TEST-2 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
129.6 21.12
130.6 21.2
Table E3 SEEP-A1 TEST-2 YSI Salt Dilution Calibration Data
21.1
131.0 21.1
128.9 21.1
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement
Part 2: Constant-Rate Injection.” Streamline, Watershed Management Bulletin,
vol. 8, no. 1, 2004, pp. 11–15.
(mg/L) (°C)
10000 NR
100,000 NR
Table E4 SEEP-A1 TEST-2 Flow Calculation Summary
Mass of Salt injected
Slope of Calibration Curve
Integral of Conductivity Data Curve
Calculated Flow Rate
1,000
100 NR
NR
134.3
128.1
130.3
130.3 (µS/cms)
(µS/cms)
(µS/cms)
(µS/cms)
Calibration
Concentration Temperature
131.6
Qൌ ௤
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Page 104 of 452 August 2019
APPENDIX E26: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 11:47:41 AM 132.7 -
6/7/2019 11:47:42 AM 132.7 -
6/7/2019 11:47:43 AM 132.6 -
6/7/2019 11:47:44 AM 132.6 -
6/7/2019 11:47:45 AM 132.6 -
6/7/2019 11:47:46 AM 132.6 -
6/7/2019 11:47:47 AM 132.6 -
6/7/2019 11:47:48 AM 132.6 -
6/7/2019 11:47:49 AM 132.6 -
6/7/2019 11:47:50 AM 132.6 -
6/7/2019 11:47:51 AM 132.6 -
6/7/2019 11:47:52 AM 132.6 -
6/7/2019 11:47:53 AM 132.6 -
6/7/2019 11:47:54 AM 132.6 -
6/7/2019 11:47:55 AM 132.6 -
6/7/2019 11:47:56 AM 132.6 -
6/7/2019 11:47:57 AM 132.6 -
6/7/2019 11:47:58 AM 132.6 -
6/7/2019 11:47:59 AM 132.6 -
6/7/2019 11:48:00 AM 132.6 -
6/7/2019 11:48:01 AM 132.6 -
6/7/2019 11:48:02 AM 132.6 -
6/7/2019 11:48:03 AM 132.6 -
6/7/2019 11:48:04 AM 132.6 -
6/7/2019 11:48:05 AM 132.5 -
6/7/2019 11:48:06 AM 132.5 -
6/7/2019 11:48:07 AM 132.5 -
6/7/2019 11:48:08 AM 132.5 -
6/7/2019 11:48:09 AM 132.9 -
6/7/2019 11:48:10 AM 218.9 86.3
6/7/2019 11:48:11 AM 547.0 414.4
6/7/2019 11:48:12 AM 1278.6 1146.0
6/7/2019 11:48:13 AM 2568.8 2436.2
6/7/2019 11:48:14 AM 3508.5 3375.9
6/7/2019 11:48:15 AM 4540.3 4407.7
6/7/2019 11:48:16 AM 5006.9 4874.3
6/7/2019 11:48:17 AM 4968.0 4835.4
6/7/2019 11:48:18 AM 5012.3 4879.7
6/7/2019 11:48:19 AM 4843.0 4710.4
6/7/2019 11:48:20 AM 4135.0 4002.4
6/7/2019 11:48:21 AM 3140.0 3007.4
6/7/2019 11:48:22 AM 2716.9 2584.3
6/7/2019 11:48:23 AM 2372.2 2239.6
6/7/2019 11:48:24 AM 2034.6 1902.0
6/7/2019 11:48:25 AM 1806.0 1673.4
6/7/2019 11:48:26 AM 1644.4 1511.8
6/7/2019 11:48:27 AM 1464.8 1332.2
6/7/2019 11:48:28 AM 1232.4 1099.8
6/7/2019 11:48:29 AM 997.7 865.1
6/7/2019 11:48:30 AM 904.8 772.2
6/7/2019 11:48:31 AM 843.6 711.0
6/7/2019 11:48:32 AM 765.3 632.7
6/7/2019 11:48:33 AM 667.2 534.6
6/7/2019 11:48:34 AM 628.0 495.4
6/7/2019 11:48:35 AM 621.2 488.6
6/7/2019 11:48:36 AM 510.7 378.1
6/7/2019 11:48:37 AM 496.9 364.3
6/7/2019 11:48:38 AM 441.0 308.4
6/7/2019 11:48:39 AM 420.6 288.0
6/7/2019 11:48:40 AM 403.1 270.5
6/7/2019 11:48:41 AM 387.1 254.5
6/7/2019 11:48:42 AM 374.5 241.9
6/7/2019 11:48:43 AM 321.2 188.6
6/7/2019 11:48:44 AM 303.7 171.1
6/7/2019 11:48:45 AM 293.2 160.6
6/7/2019 11:48:46 AM 290.2 157.6
6/7/2019 11:48:47 AM 282.4 149.8
6/7/2019 11:48:48 AM 272.4 139.8
6/7/2019 11:48:49 AM 264.2 131.6
6/7/2019 11:48:50 AM 258.2 125.6
Table E1 SEEP-A1 TEST-3 Data Log
Page 105 of 452 August 2019
APPENDIX E26: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-3 Data Log
6/7/2019 11:48:51 AM 252.2 119.6
6/7/2019 11:48:52 AM 247.5 114.9
6/7/2019 11:48:53 AM 242.4 109.8
6/7/2019 11:48:54 AM 238.5 105.9
6/7/2019 11:48:55 AM 234.2 101.6
6/7/2019 11:48:56 AM 230.7 98.1
6/7/2019 11:48:57 AM 227.0 94.4
6/7/2019 11:48:58 AM 224.2 91.6
6/7/2019 11:48:59 AM 221.1 88.5
6/7/2019 11:49:00 AM 214.4 81.8
6/7/2019 11:49:01 AM 207.9 75.3
6/7/2019 11:49:02 AM 202.9 70.3
6/7/2019 11:49:03 AM 197.9 65.3
6/7/2019 11:49:04 AM 193.4 60.8
6/7/2019 11:49:05 AM 189.9 57.3
6/7/2019 11:49:06 AM 186.5 53.9
6/7/2019 11:49:07 AM 183.7 51.1
6/7/2019 11:49:08 AM 181.0 48.4
6/7/2019 11:49:09 AM 178.9 46.3
6/7/2019 11:49:10 AM 176.6 44.0
6/7/2019 11:49:11 AM 174.9 42.3
6/7/2019 11:49:12 AM 173.0 40.4
6/7/2019 11:49:13 AM 171.5 38.9
6/7/2019 11:49:14 AM 169.9 37.3
6/7/2019 11:49:15 AM 168.5 35.9
6/7/2019 11:49:16 AM 167.1 34.5
6/7/2019 11:49:17 AM 166.0 33.4
6/7/2019 11:49:18 AM 164.8 32.2
6/7/2019 11:49:19 AM 163.8 31.2
6/7/2019 11:49:20 AM 162.8 30.2
6/7/2019 11:49:21 AM 161.9 29.3
6/7/2019 11:49:22 AM 161.1 28.5
6/7/2019 11:49:23 AM 160.4 27.8
6/7/2019 11:49:24 AM 159.6 27.0
6/7/2019 11:49:25 AM 158.9 26.3
6/7/2019 11:49:26 AM 158.3 25.7
6/7/2019 11:49:27 AM 157.6 25.0
6/7/2019 11:49:28 AM 157.2 24.6
6/7/2019 11:49:29 AM 156.6 24.0
6/7/2019 11:49:30 AM 156.2 23.6
6/7/2019 11:49:31 AM 155.8 23.2
6/7/2019 11:49:32 AM 155.5 22.9
6/7/2019 11:49:33 AM 155.2 22.6
6/7/2019 11:49:34 AM 154.9 22.3
6/7/2019 11:49:35 AM 154.5 21.9
6/7/2019 11:49:36 AM 154.2 21.6
6/7/2019 11:49:37 AM 153.9 21.3
6/7/2019 11:49:38 AM 153.6 21.0
6/7/2019 11:49:39 AM 153.3 20.7
6/7/2019 11:49:40 AM 153.1 20.5
6/7/2019 11:49:41 AM 152.8 20.2
6/7/2019 11:49:42 AM 152.5 19.9
6/7/2019 11:49:43 AM 152.2 19.6
6/7/2019 11:49:44 AM 151.9 19.3
6/7/2019 11:49:45 AM 151.6 19.0
6/7/2019 11:49:46 AM 151.3 18.7
6/7/2019 11:49:47 AM 151.0 18.4
6/7/2019 11:49:48 AM 150.7 18.1
6/7/2019 11:49:49 AM 150.5 17.9
6/7/2019 11:49:50 AM 150.1 17.5
6/7/2019 11:49:51 AM 149.8 17.2
6/7/2019 11:49:52 AM 149.5 16.9
6/7/2019 11:49:53 AM 149.1 16.5
6/7/2019 11:49:54 AM 148.8 16.2
6/7/2019 11:49:55 AM 148.5 15.9
6/7/2019 11:49:56 AM 148.1 15.5
6/7/2019 11:49:57 AM 147.8 15.2
6/7/2019 11:49:58 AM 147.5 14.9
6/7/2019 11:49:59 AM 147.2 14.6
6/7/2019 11:50:00 AM 146.9 14.3
6/7/2019 11:50:01 AM 146.6 14.0
6/7/2019 11:50:02 AM 146.3 13.7
6/7/2019 11:50:03 AM 146.1 13.5
6/7/2019 11:50:04 AM 145.9 13.3
6/7/2019 11:50:05 AM 145.7 13.1
6/7/2019 11:50:06 AM 145.5 12.9
6/7/2019 11:50:07 AM 145.3 12.7
Page 106 of 452 August 2019
APPENDIX E26: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-3 Data Log
6/7/2019 11:50:08 AM 145.2 12.6
6/7/2019 11:50:09 AM 145.0 12.4
6/7/2019 11:50:10 AM 144.9 12.3
6/7/2019 11:50:11 AM 144.7 12.1
6/7/2019 11:50:12 AM 144.5 11.9
6/7/2019 11:50:13 AM 144.4 11.8
6/7/2019 11:50:14 AM 144.2 11.6
6/7/2019 11:50:15 AM 144.1 11.5
6/7/2019 11:50:16 AM 144.0 11.4
6/7/2019 11:50:17 AM 143.8 11.2
6/7/2019 11:50:18 AM 143.7 11.1
6/7/2019 11:50:19 AM 143.5 10.9
6/7/2019 11:50:20 AM 143.4 10.8
6/7/2019 11:50:21 AM 143.3 10.7
6/7/2019 11:50:22 AM 143.2 10.6
6/7/2019 11:50:23 AM 143.1 10.5
6/7/2019 11:50:24 AM 143.0 10.4
6/7/2019 11:50:25 AM 142.9 10.3
6/7/2019 11:50:26 AM 142.8 10.2
6/7/2019 11:50:27 AM 142.7 10.1
6/7/2019 11:50:28 AM 142.6 10.0
6/7/2019 11:50:29 AM 142.5 9.9
6/7/2019 11:50:30 AM 142.4 9.8
6/7/2019 11:50:31 AM 142.3 9.7
6/7/2019 11:50:32 AM 142.3 9.7
6/7/2019 11:50:33 AM 142.2 9.6
6/7/2019 11:50:34 AM 142.1 9.5
6/7/2019 11:50:35 AM 142.1 9.5
6/7/2019 11:50:36 AM 142.0 9.4
6/7/2019 11:50:37 AM 141.9 9.3
6/7/2019 11:50:38 AM 141.8 9.2
6/7/2019 11:50:39 AM 141.8 9.2
6/7/2019 11:50:40 AM 141.7 9.1
6/7/2019 11:50:41 AM 141.6 9.0
6/7/2019 11:50:42 AM 141.6 9.0
6/7/2019 11:50:43 AM 141.5 8.9
6/7/2019 11:50:44 AM 141.4 8.8
6/7/2019 11:50:45 AM 141.4 8.8
6/7/2019 11:50:46 AM 141.3 8.7
6/7/2019 11:50:47 AM 141.3 8.7
6/7/2019 11:50:48 AM 141.2 8.6
6/7/2019 11:50:49 AM 141.1 8.5
6/7/2019 11:50:50 AM 141.1 8.5
6/7/2019 11:50:51 AM 141.0 8.4
6/7/2019 11:50:52 AM 141.0 8.4
6/7/2019 11:50:53 AM 140.9 8.3
6/7/2019 11:50:54 AM 140.8 8.2
6/7/2019 11:50:55 AM 140.7 8.1
6/7/2019 11:50:56 AM 140.7 8.1
6/7/2019 11:50:57 AM 140.6 8.0
6/7/2019 11:50:58 AM 140.5 7.9
6/7/2019 11:50:59 AM 140.4 7.8
6/7/2019 11:51:00 AM 140.4 7.8
6/7/2019 11:51:01 AM 140.3 7.7
6/7/2019 11:51:02 AM 140.2 7.6
6/7/2019 11:51:03 AM 140.1 7.5
6/7/2019 11:51:04 AM 140.1 7.5
6/7/2019 11:51:05 AM 140.0 7.4
6/7/2019 11:51:06 AM 139.9 7.3
6/7/2019 11:51:07 AM 139.8 7.2
6/7/2019 11:51:08 AM 139.8 7.2
6/7/2019 11:51:09 AM 139.7 7.1
6/7/2019 11:51:10 AM 139.7 7.1
6/7/2019 11:51:11 AM 139.6 7.0
6/7/2019 11:51:12 AM 139.5 6.9
6/7/2019 11:51:13 AM 139.5 6.9
6/7/2019 11:51:14 AM 139.5 6.9
6/7/2019 11:51:15 AM 139.4 6.8
6/7/2019 11:51:16 AM 139.4 6.8
6/7/2019 11:51:17 AM 139.3 6.7
6/7/2019 11:51:18 AM 139.3 6.7
6/7/2019 11:51:19 AM 139.3 6.7
6/7/2019 11:51:20 AM 139.3 6.7
6/7/2019 11:51:21 AM 139.2 6.6
6/7/2019 11:51:22 AM 139.2 6.6
6/7/2019 11:51:23 AM 139.2 6.6
6/7/2019 11:51:24 AM 139.2 6.6
6/7/2019 11:51:25 AM 139.2 6.6
6/7/2019 11:51:26 AM 139.2 6.6
Page 107 of 452 August 2019
APPENDIX E26: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A1 TEST-3 Data Log
6/7/2019 11:51:27 AM 139.1 6.5
6/7/2019 11:51:28 AM 139.1 6.5
6/7/2019 11:51:29 AM 139.1 6.5
6/7/2019 11:51:30 AM 139.1 6.5
6/7/2019 11:51:31 AM 139.1 6.5
6/7/2019 11:51:32 AM 139.1 6.5
6/7/2019 11:51:33 AM 139.1 6.5
6/7/2019 11:51:34 AM 139.1 6.5
6/7/2019 11:51:35 AM 139.0 6.4
6/7/2019 11:51:36 AM 139.0 6.4
6/7/2019 11:51:37 AM 139.0 6.4
6/7/2019 11:51:38 AM 139.0 6.4
6/7/2019 11:51:39 AM 139.0 6.4
6/7/2019 11:51:40 AM 139.0 6.4
6/7/2019 11:51:41 AM 139.0 6.4
6/7/2019 11:51:42 AM 139.0 6.4
6/7/2019 11:51:43 AM 139.0 6.4
6/7/2019 11:51:44 AM 138.9 6.3
6/7/2019 11:51:45 AM 138.9 6.3
6/7/2019 11:51:46 AM 138.9 6.3
6/7/2019 11:51:47 AM 138.9 6.3
6/7/2019 11:51:48 AM 138.9 6.3
6/7/2019 11:51:49 AM 138.9 6.3
6/7/2019 11:51:50 AM 138.8 6.2
6/7/2019 11:51:51 AM 138.8 6.2
6/7/2019 11:51:52 AM 138.8 6.2
6/7/2019 11:51:53 AM 138.8 6.2
6/7/2019 11:51:54 AM 138.8 6.2
6/7/2019 11:51:55 AM 138.8 6.2
6/7/2019 11:51:56 AM 138.8 6.2
6/7/2019 11:51:57 AM 138.8 6.2
6/7/2019 11:51:58 AM 138.8 6.2
6/7/2019 11:51:59 AM 138.8 6.2
6/7/2019 11:52:00 AM 138.8 6.2
6/7/2019 11:52:01 AM 138.8 6.2
6/7/2019 11:52:02 AM 138.8 6.2
6/7/2019 11:52:03 AM 138.8 6.2
6/7/2019 11:52:04 AM 138.8 6.2
6/7/2019 11:52:05 AM 138.8 6.2
6/7/2019 11:52:06 AM 138.8 6.2
6/7/2019 11:52:07 AM 138.8 6.2
6/7/2019 11:52:08 AM 138.8 6.2
6/7/2019 11:52:09 AM 138.8 6.2
6/7/2019 11:52:10 AM 138.8 6.2
6/7/2019 11:52:11 AM 138.8 6.2
6/7/2019 11:52:12 AM 138.8 6.2
6/7/2019 11:52:13 AM 138.8 6.2
6/7/2019 11:52:14 AM 138.9 6.3
6/7/2019 11:52:15 AM 138.9 6.3
6/7/2019 11:52:16 AM 138.9 6.3
6/7/2019 11:52:17 AM 138.9 6.3
6/7/2019 11:52:18 AM 138.9 6.3
6/7/2019 11:52:19 AM 138.9 6.3
6/7/2019 11:52:20 AM 138.9 6.3
6/7/2019 11:52:21 AM 138.9 6.3
6/7/2019 11:52:22 AM 138.9 6.3
6/7/2019 11:52:23 AM 138.9 6.3
6/7/2019 11:52:24 AM 138.9 6.3
6/7/2019 11:52:25 AM 138.9 6.3
6/7/2019 11:52:26 AM 138.9 6.3
6/7/2019 11:52:27 AM 139.0 6.4
6/7/2019 11:52:28 AM 139.0 6.4
6/7/2019 11:52:29 AM 139.0 6.4
6/7/2019 11:52:30 AM 139.0 6.4
6/7/2019 11:52:31 AM 139.0 6.4
6/7/2019 11:52:32 AM 139.0 6.4
6/7/2019 11:52:33 AM 139.0 6.4
6/7/2019 11:52:34 AM 139.0 6.4
6/7/2019 11:52:35 AM 139.0 6.4
6/7/2019 11:52:36 AM 139.0 6.4
6/7/2019 11:52:37 AM 139.0 6.4
6/7/2019 11:52:38 AM 139.0 6.4
Page 108 of 452 August 2019
APPENDIX E26: SALT DILUTION GAUGING SUMMARY
SEEP-A1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-A1 TEST-3 1054
SEEP-A1 TEST-3 1055
SEEP-A1 TEST-3 1100
SEEP-A1 TEST-3 1102
SEEP-A1 TEST-3 NR
Average
Geo Mean
Average (pre-test)
Average (post-test)
Location EC Reading
(µS/cms)
SEEP-A1 TEST-3 245
SEEP-A1 TEST-3 2,160
SEEP-A1 TEST-3 18,420
SEEP-A1 TEST-3 135,005
q 300,700 mg
K 1.3550 (µS/cms) / (mg/L)
(s) . (µS/cms)
Q 6.5 L/s
103.7 GPM
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
NR Not recorded
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
10000 NR
100,000 NR
Table E4 SEEP-A1 TEST-3 Flow Calculation Summary
Mass of Salt injected
Slope of Calibration Curve
Integral of Conductivity Data Curve
Calculated Flow Rate
62,355.3 SUM:Δt(EC
t-ECbkg)
139.0
132.6
130.3
130.3
130.6
129.6
131.6
131
128.9
(µS/cms)
Table E2 SEEP-A1 TEST-3 Stream Background Conductivity Data
Location Time Background Stream EC
(µS/cms)
21.2
(µS/cms)
21.12
21.1
21.1
21.1
(°C)
Background Stream Temperature
(µS/cms)
(µS/cms)
NR
NR
Table E3 SEEP-A1 TEST-3 YSI Salt Dilution Calibration Data
Calibration
Concentration Temperature
(mg/L)(°C)
1,000
100
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 109 of 452 August 2019
APPENDIX E27: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-1 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
5/23/2019 3:35:50 PM 202.9 -
5/23/2019 3:35:51 PM 202.9 -
5/23/2019 3:35:52 PM 202.9 -
5/23/2019 3:35:53 PM 202.9 -
5/23/2019 3:35:54 PM 202.9 -
5/23/2019 3:35:55 PM 202.9 -
5/23/2019 3:35:56 PM 203.0 -
5/23/2019 3:35:57 PM 203.0 -
5/23/2019 3:35:58 PM 203.0 -
5/23/2019 3:35:59 PM 203.1 -
5/23/2019 3:36:00 PM 203.1 -
5/23/2019 3:36:01 PM 203.2 -
5/23/2019 3:36:02 PM 203.3 -
5/23/2019 3:36:03 PM 203.3 -
5/23/2019 3:36:04 PM 203.3 -
5/23/2019 3:36:05 PM 203.3 -
5/23/2019 3:36:06 PM 203.3 -
5/23/2019 3:36:07 PM 203.3 -
5/23/2019 3:36:08 PM 203.4 -
5/23/2019 3:36:09 PM 203.4 -
5/23/2019 3:36:10 PM 203.5 -
5/23/2019 3:36:11 PM 203.6 -
5/23/2019 3:36:12 PM 203.6 -
5/23/2019 3:36:13 PM 203.7 -
5/23/2019 3:36:14 PM 203.8 -
5/23/2019 3:36:15 PM 203.8 -
5/23/2019 3:36:16 PM 203.8 -
5/23/2019 3:36:17 PM 204.0 -
5/23/2019 3:36:18 PM 204.0 -
5/23/2019 3:36:19 PM 204.1 -
5/23/2019 3:36:20 PM 204.2 -
5/23/2019 3:36:21 PM 204.3 -
5/23/2019 3:36:22 PM 204.3 -
5/23/2019 3:36:23 PM 204.4 -
5/23/2019 3:36:24 PM 204.6 -
5/23/2019 3:36:25 PM 204.7 -
5/23/2019 3:36:26 PM 205.0 -
5/23/2019 3:36:27 PM 205.6 -
5/23/2019 3:36:28 PM 206.6 -
5/23/2019 3:36:29 PM 257.1 53.4
5/23/2019 3:36:30 PM 299.7 96.0
5/23/2019 3:36:31 PM 354.5 150.8
5/23/2019 3:36:32 PM 405.1 201.4
5/23/2019 3:36:33 PM 420.3 216.6
5/23/2019 3:36:34 PM 710.7 507.0
5/23/2019 3:36:35 PM 687.9 484.2
5/23/2019 3:36:36 PM 749.5 545.8
5/23/2019 3:36:37 PM 1272.7 1069.0
5/23/2019 3:36:38 PM 1262.2 1058.5
5/23/2019 3:36:39 PM 1553.0 1349.3
5/23/2019 3:36:40 PM 1678.8 1475.1
5/23/2019 3:36:41 PM 1935.2 1731.5
5/23/2019 3:36:42 PM 2082.8 1879.1
5/23/2019 3:36:43 PM 2493.8 2290.1
5/23/2019 3:36:44 PM 2553.1 2349.4
5/23/2019 3:36:45 PM 2638.7 2435.0
5/23/2019 3:36:46 PM 2685.5 2481.8
5/23/2019 3:36:47 PM 2753.3 2549.6
5/23/2019 3:36:48 PM 2813.2 2609.5
5/23/2019 3:36:49 PM 2848.8 2645.1
5/23/2019 3:36:50 PM 2874.4 2670.7
5/23/2019 3:36:51 PM 2895.7 2692.0
5/23/2019 3:36:52 PM 2909.8 2706.1
5/23/2019 3:36:53 PM 2922.1 2718.4
5/23/2019 3:36:54 PM 2927.0 2723.3
5/23/2019 3:36:55 PM 2925.5 2721.8
5/23/2019 3:36:56 PM 2920.4 2716.7
5/23/2019 3:36:57 PM 2908.9 2705.2
5/23/2019 3:36:58 PM 2707.0 2503.3
5/23/2019 3:36:59 PM 2638.6 2434.9
Table E1 SEEP-A3 TEST-1 Data Log
Page 110 of 452 August 2019
APPENDIX E27: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-1 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-1 Data Log
5/23/2019 3:37:00 PM 2589.8 2386.1
5/23/2019 3:37:01 PM 2548.6 2344.9
5/23/2019 3:37:02 PM 2530.0 2326.3
5/23/2019 3:37:03 PM 2481.0 2277.3
5/23/2019 3:37:04 PM 2306.8 2103.1
5/23/2019 3:37:05 PM 2248.7 2045.0
5/23/2019 3:37:06 PM 2154.8 1951.1
5/23/2019 3:37:07 PM 2140.6 1936.9
5/23/2019 3:37:08 PM 2100.7 1897.0
5/23/2019 3:37:09 PM 2065.7 1862.0
5/23/2019 3:37:10 PM 1917.2 1713.5
5/23/2019 3:37:11 PM 1856.2 1652.5
5/23/2019 3:37:12 PM 1763.9 1560.2
5/23/2019 3:37:13 PM 1693.6 1489.9
5/23/2019 3:37:14 PM 1654.3 1450.6
5/23/2019 3:37:15 PM 1605.0 1401.3
5/23/2019 3:37:16 PM 1489.3 1285.6
5/23/2019 3:37:17 PM 1466.7 1263.0
5/23/2019 3:37:18 PM 1403.5 1199.8
5/23/2019 3:37:19 PM 1376.2 1172.5
5/23/2019 3:37:20 PM 1333.3 1129.6
5/23/2019 3:37:21 PM 1309.9 1106.2
5/23/2019 3:37:22 PM 1294.2 1090.5
5/23/2019 3:37:23 PM 1207.6 1003.9
5/23/2019 3:37:24 PM 1201.3 997.6
5/23/2019 3:37:25 PM 1141.8 938.1
5/23/2019 3:37:26 PM 1089.0 885.3
5/23/2019 3:37:27 PM 1067.6 863.9
5/23/2019 3:37:28 PM 996.1 792.4
5/23/2019 3:37:29 PM 973.7 770.0
5/23/2019 3:37:30 PM 957.2 753.5
5/23/2019 3:37:31 PM 949.2 745.5
5/23/2019 3:37:32 PM 931.9 728.2
5/23/2019 3:37:33 PM 924.0 720.3
5/23/2019 3:37:34 PM 921.9 718.2
5/23/2019 3:37:35 PM 916.8 713.1
5/23/2019 3:37:36 PM 899.7 696.0
5/23/2019 3:37:37 PM 860.7 657.0
5/23/2019 3:37:38 PM 845.5 641.8
5/23/2019 3:37:39 PM 836.4 632.7
5/23/2019 3:37:40 PM 823.5 619.8
5/23/2019 3:37:41 PM 810.8 607.1
5/23/2019 3:37:42 PM 748.9 545.2
5/23/2019 3:37:43 PM 731.5 527.8
5/23/2019 3:37:44 PM 722.4 518.7
5/23/2019 3:37:45 PM 695.0 491.3
5/23/2019 3:37:46 PM 681.3 477.6
5/23/2019 3:37:47 PM 678.4 474.7
5/23/2019 3:37:48 PM 599.1 395.4
5/23/2019 3:37:49 PM 609.3 405.6
5/23/2019 3:37:50 PM 590.9 387.2
5/23/2019 3:37:51 PM 588.7 385.0
5/23/2019 3:37:52 PM 581.8 378.1
5/23/2019 3:37:53 PM 577.1 373.4
5/23/2019 3:37:54 PM 573.2 369.5
5/23/2019 3:37:55 PM 569.2 365.5
5/23/2019 3:37:56 PM 564.9 361.2
5/23/2019 3:37:57 PM 560.7 357.0
5/23/2019 3:37:58 PM 556.5 352.8
5/23/2019 3:37:59 PM 552.8 349.1
5/23/2019 3:38:00 PM 548.6 344.9
5/23/2019 3:38:01 PM 545.2 341.5
5/23/2019 3:38:02 PM 541.4 337.7
5/23/2019 3:38:03 PM 490.2 286.5
5/23/2019 3:38:04 PM 489.0 285.3
5/23/2019 3:38:05 PM 476.2 272.5
5/23/2019 3:38:06 PM 473.7 270.0
5/23/2019 3:38:07 PM 467.1 263.4
5/23/2019 3:38:08 PM 461.4 257.7
5/23/2019 3:38:09 PM 457.0 253.3
5/23/2019 3:38:10 PM 453.0 249.3
5/23/2019 3:38:11 PM 449.4 245.7
5/23/2019 3:38:12 PM 446.7 243.0
5/23/2019 3:38:13 PM 444.3 240.6
5/23/2019 3:38:14 PM 442.0 238.3
5/23/2019 3:38:15 PM 439.4 235.7
5/23/2019 3:38:16 PM 437.3 233.6
Page 111 of 452 August 2019
APPENDIX E27: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-1 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-1 Data Log
5/23/2019 3:38:17 PM 434.9 231.2
5/23/2019 3:38:18 PM 433.1 229.4
5/23/2019 3:38:19 PM 429.1 225.4
5/23/2019 3:38:20 PM 424.9 221.2
5/23/2019 3:38:21 PM 420.8 217.1
5/23/2019 3:38:22 PM 417.2 213.5
5/23/2019 3:38:23 PM 413.6 209.9
5/23/2019 3:38:24 PM 410.5 206.8
5/23/2019 3:38:25 PM 408.1 204.4
5/23/2019 3:38:26 PM 403.7 200.0
5/23/2019 3:38:27 PM 401.7 198.0
5/23/2019 3:38:28 PM 398.8 195.1
5/23/2019 3:38:29 PM 395.3 191.6
5/23/2019 3:38:30 PM 393.1 189.4
5/23/2019 3:38:31 PM 389.6 185.9
5/23/2019 3:38:32 PM 386.4 182.7
5/23/2019 3:38:33 PM 383.6 179.9
5/23/2019 3:38:34 PM 380.3 176.6
5/23/2019 3:38:35 PM 377.7 174.0
5/23/2019 3:38:36 PM 374.5 170.8
5/23/2019 3:38:37 PM 371.4 167.7
5/23/2019 3:38:38 PM 367.7 164.0
5/23/2019 3:38:39 PM 364.7 161.0
5/23/2019 3:38:40 PM 360.8 157.1
5/23/2019 3:38:41 PM 357.7 154.0
5/23/2019 3:38:42 PM 354.1 150.4
5/23/2019 3:38:43 PM 351.2 147.5
5/23/2019 3:38:44 PM 347.8 144.1
5/23/2019 3:38:45 PM 345.0 141.3
5/23/2019 3:38:46 PM 342.1 138.4
5/23/2019 3:38:47 PM 339.9 136.2
5/23/2019 3:38:48 PM 337.4 133.7
5/23/2019 3:38:49 PM 334.8 131.1
5/23/2019 3:38:50 PM 332.8 129.1
5/23/2019 3:38:51 PM 330.1 126.4
5/23/2019 3:38:52 PM 328.5 124.8
5/23/2019 3:38:53 PM 327.3 123.6
5/23/2019 3:38:54 PM 325.3 121.6
5/23/2019 3:38:55 PM 324.0 120.3
5/23/2019 3:38:56 PM 321.9 118.2
5/23/2019 3:38:57 PM 320.1 116.4
5/23/2019 3:38:58 PM 318.8 115.1
5/23/2019 3:38:59 PM 316.4 112.7
5/23/2019 3:39:00 PM 315.3 111.6
5/23/2019 3:39:01 PM 313.1 109.4
5/23/2019 3:39:02 PM 311.8 108.1
5/23/2019 3:39:03 PM 310.3 106.6
5/23/2019 3:39:04 PM 308.6 104.9
5/23/2019 3:39:05 PM 307.0 103.3
5/23/2019 3:39:06 PM 305.2 101.5
5/23/2019 3:39:07 PM 303.6 99.9
5/23/2019 3:39:08 PM 301.9 98.2
5/23/2019 3:39:09 PM 300.6 96.9
5/23/2019 3:39:10 PM 299.3 95.6
5/23/2019 3:39:11 PM 298.1 94.4
5/23/2019 3:39:12 PM 297.3 93.6
5/23/2019 3:39:13 PM 296.5 92.8
5/23/2019 3:39:14 PM 295.6 91.9
5/23/2019 3:39:15 PM 294.7 91.0
5/23/2019 3:39:16 PM 293.4 89.7
5/23/2019 3:39:17 PM 292.7 89.0
5/23/2019 3:39:18 PM 291.7 88.0
5/23/2019 3:39:19 PM 290.8 87.1
5/23/2019 3:39:20 PM 289.9 86.2
5/23/2019 3:39:21 PM 288.9 85.2
5/23/2019 3:39:22 PM 288.2 84.5
5/23/2019 3:39:23 PM 287.3 83.6
5/23/2019 3:39:24 PM 286.4 82.7
5/23/2019 3:39:25 PM 285.3 81.6
5/23/2019 3:39:26 PM 284.0 80.3
5/23/2019 3:39:27 PM 283.0 79.3
5/23/2019 3:39:28 PM 282.0 78.3
5/23/2019 3:39:29 PM 280.9 77.2
5/23/2019 3:39:30 PM 280.0 76.3
5/23/2019 3:39:31 PM 279.0 75.3
5/23/2019 3:39:32 PM 278.0 74.3
5/23/2019 3:39:33 PM 276.9 73.2
5/23/2019 3:39:34 PM 276.0 72.3
5/23/2019 3:39:35 PM 274.9 71.2
Page 112 of 452 August 2019
APPENDIX E27: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-1 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-1 Data Log
5/23/2019 3:39:36 PM 273.6 69.9
5/23/2019 3:39:37 PM 272.8 69.1
5/23/2019 3:39:38 PM 271.8 68.1
5/23/2019 3:39:39 PM 270.8 67.1
5/23/2019 3:39:40 PM 269.9 66.2
5/23/2019 3:39:41 PM 268.8 65.1
5/23/2019 3:39:42 PM 267.7 64.0
5/23/2019 3:39:43 PM 266.8 63.1
5/23/2019 3:39:44 PM 265.8 62.1
5/23/2019 3:39:45 PM 265.0 61.3
5/23/2019 3:39:46 PM 264.0 60.3
5/23/2019 3:39:47 PM 263.0 59.3
5/23/2019 3:39:48 PM 262.1 58.4
5/23/2019 3:39:49 PM 261.1 57.4
5/23/2019 3:39:50 PM 260.1 56.4
5/23/2019 3:39:51 PM 259.2 55.5
5/23/2019 3:39:52 PM 258.2 54.5
5/23/2019 3:39:53 PM 257.3 53.6
5/23/2019 3:39:54 PM 256.3 52.6
5/23/2019 3:39:55 PM 255.6 51.9
5/23/2019 3:39:56 PM 254.7 51.0
5/23/2019 3:39:57 PM 254.0 50.3
5/23/2019 3:39:58 PM 253.2 49.5
5/23/2019 3:39:59 PM 252.5 48.8
5/23/2019 3:40:00 PM 251.9 48.2
5/23/2019 3:40:01 PM 251.3 47.6
5/23/2019 3:40:02 PM 250.6 46.9
5/23/2019 3:40:03 PM 250.0 46.3
5/23/2019 3:40:04 PM 249.5 45.8
5/23/2019 3:40:05 PM 249.1 45.4
5/23/2019 3:40:06 PM 248.7 45.0
5/23/2019 3:40:07 PM 248.2 44.5
5/23/2019 3:40:08 PM 247.9 44.2
5/23/2019 3:40:09 PM 247.5 43.8
5/23/2019 3:40:10 PM 247.1 43.4
5/23/2019 3:40:11 PM 246.7 43.0
5/23/2019 3:40:12 PM 246.4 42.7
5/23/2019 3:40:13 PM 246.0 42.3
5/23/2019 3:40:14 PM 245.6 41.9
5/23/2019 3:40:15 PM 245.1 41.4
5/23/2019 3:40:16 PM 244.7 41.0
5/23/2019 3:40:17 PM 244.3 40.6
5/23/2019 3:40:18 PM 243.9 40.2
5/23/2019 3:40:19 PM 243.4 39.7
5/23/2019 3:40:20 PM 243.0 39.3
5/23/2019 3:40:21 PM 242.5 38.8
5/23/2019 3:40:22 PM 242.0 38.3
5/23/2019 3:40:23 PM 241.6 37.9
5/23/2019 3:40:24 PM 241.1 37.4
5/23/2019 3:40:25 PM 240.8 37.1
5/23/2019 3:40:26 PM 240.3 36.6
5/23/2019 3:40:27 PM 240.0 36.3
5/23/2019 3:40:28 PM 239.6 35.9
5/23/2019 3:40:29 PM 239.2 35.5
5/23/2019 3:40:30 PM 238.7 35.0
5/23/2019 3:40:31 PM 238.3 34.6
5/23/2019 3:40:32 PM 238.0 34.3
5/23/2019 3:40:33 PM 237.6 33.9
5/23/2019 3:40:34 PM 237.3 33.6
5/23/2019 3:40:35 PM 237.0 33.3
5/23/2019 3:40:36 PM 236.6 32.9
5/23/2019 3:40:37 PM 236.4 32.7
5/23/2019 3:40:38 PM 236.0 32.3
5/23/2019 3:40:39 PM 235.7 32.0
5/23/2019 3:40:40 PM 235.4 31.7
5/23/2019 3:40:41 PM 235.1 31.4
5/23/2019 3:40:42 PM 234.7 31.0
5/23/2019 3:40:43 PM 234.5 30.8
5/23/2019 3:40:44 PM 234.1 30.4
5/23/2019 3:40:45 PM 233.8 30.1
5/23/2019 3:40:46 PM 233.5 29.8
5/23/2019 3:40:47 PM 233.1 29.4
5/23/2019 3:40:48 PM 232.8 29.1
5/23/2019 3:40:49 PM 232.4 28.7
5/23/2019 3:40:50 PM 232.0 28.3
5/23/2019 3:40:51 PM 231.7 28.0
5/23/2019 3:40:52 PM 231.4 27.7
5/23/2019 3:40:53 PM 231.1 27.4
5/23/2019 3:40:54 PM 230.8 27.1
Page 113 of 452 August 2019
APPENDIX E27: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-1 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-1 Data Log
5/23/2019 3:40:55 PM 230.6 26.9
5/23/2019 3:40:56 PM 230.3 26.6
5/23/2019 3:40:57 PM 230.1 26.4
5/23/2019 3:40:58 PM 229.9 26.2
5/23/2019 3:40:59 PM 229.7 26.0
5/23/2019 3:41:00 PM 229.5 25.8
5/23/2019 3:41:01 PM 229.3 25.6
5/23/2019 3:41:02 PM 229.1 25.4
5/23/2019 3:41:03 PM 228.8 25.1
5/23/2019 3:41:04 PM 228.6 24.9
5/23/2019 3:41:05 PM 228.4 24.7
5/23/2019 3:41:06 PM 228.2 24.5
5/23/2019 3:41:07 PM 228.0 24.3
5/23/2019 3:41:08 PM 227.8 24.1
5/23/2019 3:41:09 PM 227.6 23.9
5/23/2019 3:41:10 PM 227.5 23.8
5/23/2019 3:41:11 PM 227.3 23.6
5/23/2019 3:41:12 PM 227.2 23.5
5/23/2019 3:41:13 PM 227.1 23.4
5/23/2019 3:41:14 PM 226.9 23.2
5/23/2019 3:41:15 PM 226.8 23.1
5/23/2019 3:41:16 PM 226.7 23.0
5/23/2019 3:41:17 PM 226.6 22.9
5/23/2019 3:41:18 PM 226.5 22.8
5/23/2019 3:41:19 PM 226.4 22.7
5/23/2019 3:41:20 PM 226.2 22.5
5/23/2019 3:41:21 PM 226.0 22.3
5/23/2019 3:41:22 PM 225.8 22.1
5/23/2019 3:41:23 PM 225.7 22.0
5/23/2019 3:41:24 PM 225.5 21.8
5/23/2019 3:41:25 PM 225.3 21.6
5/23/2019 3:41:26 PM 225.1 21.4
5/23/2019 3:41:27 PM 224.9 21.2
5/23/2019 3:41:28 PM 224.7 21.0
5/23/2019 3:41:29 PM 224.6 20.9
5/23/2019 3:41:30 PM 224.4 20.7
5/23/2019 3:41:31 PM 224.2 20.5
5/23/2019 3:41:32 PM 224.0 20.3
5/23/2019 3:41:33 PM 223.8 20.1
5/23/2019 3:41:34 PM 223.7 20.0
5/23/2019 3:41:35 PM 223.5 19.8
5/23/2019 3:41:36 PM 223.3 19.6
5/23/2019 3:41:37 PM 223.1 19.4
5/23/2019 3:41:38 PM 223.0 19.3
5/23/2019 3:41:39 PM 222.8 19.1
5/23/2019 3:41:40 PM 222.6 18.9
5/23/2019 3:41:41 PM 222.4 18.7
5/23/2019 3:41:42 PM 222.2 18.5
5/23/2019 3:41:43 PM 222.1 18.4
5/23/2019 3:41:44 PM 221.9 18.2
5/23/2019 3:41:45 PM 221.7 18.0
5/23/2019 3:41:46 PM 221.6 17.9
5/23/2019 3:41:47 PM 221.4 17.7
5/23/2019 3:41:48 PM 221.3 17.6
5/23/2019 3:41:49 PM 221.2 17.5
5/23/2019 3:41:50 PM 221.0 17.3
5/23/2019 3:41:51 PM 220.9 17.2
5/23/2019 3:41:52 PM 220.8 17.1
5/23/2019 3:41:53 PM 220.7 17.0
5/23/2019 3:41:54 PM 220.7 17.0
5/23/2019 3:41:55 PM 220.6 16.9
5/23/2019 3:41:56 PM 220.5 16.8
5/23/2019 3:41:57 PM 220.5 16.8
5/23/2019 3:41:58 PM 220.4 16.7
5/23/2019 3:41:59 PM 220.3 16.6
5/23/2019 3:42:00 PM 220.2 16.5
5/23/2019 3:42:01 PM 220.1 16.4
5/23/2019 3:42:02 PM 219.9 16.2
5/23/2019 3:42:03 PM 219.9 16.2
5/23/2019 3:42:04 PM 219.8 16.1
5/23/2019 3:42:05 PM 219.7 16.0
5/23/2019 3:42:06 PM 219.6 15.9
5/23/2019 3:42:07 PM 219.5 15.8
5/23/2019 3:42:08 PM 219.4 15.7
5/23/2019 3:42:09 PM 219.3 15.6
5/23/2019 3:42:10 PM 219.3 15.6
5/23/2019 3:42:11 PM 219.2 15.5
5/23/2019 3:42:12 PM 219.1 15.4
5/23/2019 3:42:13 PM 219.1 15.4
Page 114 of 452 August 2019
APPENDIX E27: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-1 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-1 Data Log
5/23/2019 3:42:14 PM 219.0 15.3
5/23/2019 3:42:15 PM 218.9 15.2
5/23/2019 3:42:16 PM 218.8 15.1
5/23/2019 3:42:17 PM 218.8 15.1
5/23/2019 3:42:18 PM 218.7 15.0
5/23/2019 3:42:19 PM 218.6 14.9
5/23/2019 3:42:20 PM 218.5 14.8
5/23/2019 3:42:21 PM 218.4 14.7
5/23/2019 3:42:22 PM 218.4 14.7
5/23/2019 3:42:23 PM 218.3 14.6
5/23/2019 3:42:24 PM 218.3 14.6
5/23/2019 3:42:25 PM 218.2 14.5
5/23/2019 3:42:26 PM 218.2 14.5
5/23/2019 3:42:27 PM 218.2 14.5
5/23/2019 3:42:28 PM 218.1 14.4
5/23/2019 3:42:29 PM 218.0 14.3
5/23/2019 3:42:30 PM 218.0 14.3
5/23/2019 3:42:31 PM 217.9 14.2
5/23/2019 3:42:32 PM 217.8 14.1
5/23/2019 3:42:33 PM 217.7 14.0
5/23/2019 3:42:34 PM 217.6 13.9
5/23/2019 3:42:35 PM 217.5 13.8
5/23/2019 3:42:36 PM 217.4 13.7
5/23/2019 3:42:37 PM 217.3 13.6
5/23/2019 3:42:38 PM 217.2 13.5
5/23/2019 3:42:39 PM 217.1 13.4
5/23/2019 3:42:40 PM 217.0 13.3
5/23/2019 3:42:41 PM 216.9 13.2
5/23/2019 3:42:42 PM 216.8 13.1
5/23/2019 3:42:43 PM 216.7 13.0
5/23/2019 3:42:44 PM 216.6 12.9
5/23/2019 3:42:45 PM 216.5 12.8
5/23/2019 3:42:46 PM 216.3 12.6
5/23/2019 3:42:47 PM 216.2 12.5
5/23/2019 3:42:48 PM 216.1 12.4
5/23/2019 3:42:49 PM 216.0 12.3
5/23/2019 3:42:50 PM 215.9 12.2
5/23/2019 3:42:51 PM 215.8 12.1
5/23/2019 3:42:52 PM 215.7 12.0
5/23/2019 3:42:53 PM 215.6 11.9
5/23/2019 3:42:54 PM 215.5 11.8
5/23/2019 3:42:55 PM 215.3 11.6
5/23/2019 3:42:56 PM 215.3 11.6
Page 115 of 452 August 2019
APPENDIX E27: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-1 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-A3 TEST-1 1504
SEEP-A3 TEST-1 1504
SEEP-A3 TEST-1 1505
SEEP-A3 TEST-1 1506
Location EC Reading
(µS/cms)
SEEP-A3 TEST-1 48.7
SEEP-A3 TEST-1 181
SEEP-A3 TEST-1 450
SEEP-A3 TEST-1 3,464
SEEP-A3 TEST-1 15,648
SEEP-A3 TEST-1 127,541
q 300,500 mg
K 1.2785 (µS/cms) / (mg/L)
(s) . (µS/cms)
Q 2.8 L/s
44.8 GPM
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(°C)
Table E2 SEEP-A3 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC Background Stream Temperature
(µS/cms)
208.8 19.1
211.0 18.9
210.0 19
208.3 19
209.5 (µS/cms)
26.6
Average (pre-test)203.7 (µS/cms)
Average (post-test)217.8 (µS/cms)
Table E3 SEEP-A3 TEST-1 YSI Salt Dilution Calibration Data
Calibration
Concentration Temperature
(mg/L)(°C)
26.9
100 27.1
1,000 27.5
Calculated Flow Rate
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement Part
2: Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8, no. 1,
2004, pp. 11–15.
10000 27.4
100,000 27.5
Table E4 SEEP-A3 TEST-1 Flow Calculation Summary
Mass of Salt injected
135,994.7 SUM:Δt(EC
t-ECbkg)
Slope of Calibration Curve
Integral of Conductivity Data Curve
10
1
Geo Mean 209.5
Average
(µS/cms)
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 116 of 452 August 2019
APPENDIX E28: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-2 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
5/23/2019 3:46:15 PM 210.9 -
5/23/2019 3:46:16 PM 210.8 -
5/23/2019 3:46:17 PM 210.7 -
5/23/2019 3:46:18 PM 210.6 -
5/23/2019 3:46:19 PM 210.5 -
5/23/2019 3:46:20 PM 210.4 -
5/23/2019 3:46:21 PM 210.3 -
5/23/2019 3:46:22 PM 210.2 -
5/23/2019 3:46:23 PM 210.1 -
5/23/2019 3:46:24 PM 210.1 -
5/23/2019 3:46:25 PM 210.0 -
5/23/2019 3:46:26 PM 209.9 -
5/23/2019 3:46:27 PM 209.8 -
5/23/2019 3:46:28 PM 209.7 -
5/23/2019 3:46:29 PM 209.7 -
5/23/2019 3:46:30 PM 209.6 -
5/23/2019 3:46:31 PM 209.5 -
5/23/2019 3:46:32 PM 209.5 -
5/23/2019 3:46:33 PM 209.4 -
5/23/2019 3:46:34 PM 209.4 -
5/23/2019 3:46:35 PM 209.3 -
5/23/2019 3:46:36 PM 209.2 -
5/23/2019 3:46:37 PM 209.2 -
5/23/2019 3:46:38 PM 209.2 -
5/23/2019 3:46:39 PM 209.1 -
5/23/2019 3:46:40 PM 209.1 -
5/23/2019 3:46:41 PM 209.1 -
5/23/2019 3:46:42 PM 209.0 -
5/23/2019 3:46:43 PM 209.0 -
5/23/2019 3:46:44 PM 208.9 -
5/23/2019 3:46:45 PM 208.9 -
5/23/2019 3:46:46 PM 208.9 -
5/23/2019 3:46:47 PM 208.8 -
5/23/2019 3:46:48 PM 208.8 -
5/23/2019 3:46:49 PM 209.0 -
5/23/2019 3:46:50 PM 209.4 -
5/23/2019 3:46:51 PM 306.9 97.3
5/23/2019 3:46:52 PM 385.3 175.7
5/23/2019 3:46:53 PM 709.4 499.8
5/23/2019 3:46:54 PM 773.4 563.8
5/23/2019 3:46:55 PM 1564.6 1355.0
5/23/2019 3:46:56 PM 1776.4 1566.8
5/23/2019 3:46:57 PM 2291.4 2081.8
5/23/2019 3:46:58 PM 2722.9 2513.3
5/23/2019 3:46:59 PM 3068.7 2859.1
5/23/2019 3:47:00 PM 3563.0 3353.4
5/23/2019 3:47:01 PM 3730.4 3520.8
5/23/2019 3:47:02 PM 3799.9 3590.3
5/23/2019 3:47:03 PM 4128.5 3918.9
5/23/2019 3:47:04 PM 4186.5 3976.9
5/23/2019 3:47:05 PM 4241.6 4032.0
5/23/2019 3:47:06 PM 4299.4 4089.8
5/23/2019 3:47:07 PM 4289.5 4079.9
5/23/2019 3:47:08 PM 4257.6 4048.0
5/23/2019 3:47:09 PM 4236.4 4026.8
5/23/2019 3:47:10 PM 3953.0 3743.4
5/23/2019 3:47:11 PM 3847.8 3638.2
5/23/2019 3:47:12 PM 3640.9 3431.3
5/23/2019 3:47:13 PM 3629.6 3420.0
5/23/2019 3:47:14 PM 3305.3 3095.7
5/23/2019 3:47:15 PM 3260.0 3050.4
5/23/2019 3:47:16 PM 3131.2 2921.6
5/23/2019 3:47:17 PM 2912.9 2703.3
5/23/2019 3:47:18 PM 2878.7 2669.1
5/23/2019 3:47:19 PM 2670.1 2460.5
5/23/2019 3:47:20 PM 2564.5 2354.9
5/23/2019 3:47:21 PM 2457.7 2248.1
5/23/2019 3:47:22 PM 2318.1 2108.5
5/23/2019 3:47:23 PM 2272.3 2062.7
5/23/2019 3:47:24 PM 2016.6 1807.0
Table E1 SEEP-A3 TEST-2 Data Log
Page 118 of 452 August 2019
APPENDIX E28: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-2 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-2 Data Log
5/23/2019 3:47:25 PM 1934.4 1724.8
5/23/2019 3:47:26 PM 1852.2 1642.6
5/23/2019 3:47:27 PM 1745.6 1536.0
5/23/2019 3:47:28 PM 1563.5 1353.9
5/23/2019 3:47:29 PM 1485.9 1276.3
5/23/2019 3:47:30 PM 1385.6 1176.0
5/23/2019 3:47:31 PM 1368.7 1159.1
5/23/2019 3:47:32 PM 1340.9 1131.3
5/23/2019 3:47:33 PM 1224.4 1014.8
5/23/2019 3:47:34 PM 1127.4 917.8
5/23/2019 3:47:35 PM 1075.1 865.5
5/23/2019 3:47:36 PM 1062.3 852.7
5/23/2019 3:47:37 PM 930.4 720.8
5/23/2019 3:47:38 PM 909.1 699.5
5/23/2019 3:47:39 PM 870.2 660.6
5/23/2019 3:47:40 PM 845.0 635.4
5/23/2019 3:47:41 PM 753.9 544.3
5/23/2019 3:47:42 PM 758.4 548.8
5/23/2019 3:47:43 PM 711.7 502.1
5/23/2019 3:47:44 PM 704.4 494.8
5/23/2019 3:47:45 PM 705.0 495.4
5/23/2019 3:47:46 PM 698.3 488.7
5/23/2019 3:47:47 PM 549.2 339.6
5/23/2019 3:47:48 PM 620.7 411.1
5/23/2019 3:47:49 PM 621.4 411.8
5/23/2019 3:47:50 PM 615.3 405.7
5/23/2019 3:47:51 PM 609.8 400.2
5/23/2019 3:47:52 PM 598.2 388.6
5/23/2019 3:47:53 PM 588.9 379.3
5/23/2019 3:47:54 PM 582.9 373.3
5/23/2019 3:47:55 PM 575.3 365.7
5/23/2019 3:47:56 PM 517.5 307.9
5/23/2019 3:47:57 PM 511.1 301.5
5/23/2019 3:47:58 PM 506.1 296.5
5/23/2019 3:47:59 PM 496.1 286.5
5/23/2019 3:48:00 PM 493.0 283.4
5/23/2019 3:48:01 PM 489.8 280.2
5/23/2019 3:48:02 PM 487.2 277.6
5/23/2019 3:48:03 PM 483.7 274.1
5/23/2019 3:48:04 PM 479.8 270.2
5/23/2019 3:48:05 PM 476.3 266.7
5/23/2019 3:48:06 PM 472.6 263.0
5/23/2019 3:48:07 PM 469.2 259.6
5/23/2019 3:48:08 PM 465.5 255.9
5/23/2019 3:48:09 PM 461.9 252.3
5/23/2019 3:48:10 PM 458.9 249.3
5/23/2019 3:48:11 PM 455.8 246.2
5/23/2019 3:48:12 PM 453.0 243.4
5/23/2019 3:48:13 PM 447.7 238.1
5/23/2019 3:48:14 PM 441.8 232.2
5/23/2019 3:48:15 PM 435.2 225.6
5/23/2019 3:48:16 PM 430.0 220.4
5/23/2019 3:48:17 PM 424.1 214.5
5/23/2019 3:48:18 PM 419.3 209.7
5/23/2019 3:48:19 PM 413.9 204.3
5/23/2019 3:48:20 PM 409.5 199.9
5/23/2019 3:48:21 PM 404.6 195.0
5/23/2019 3:48:22 PM 400.6 191.0
5/23/2019 3:48:23 PM 396.2 186.6
5/23/2019 3:48:24 PM 392.4 182.8
5/23/2019 3:48:25 PM 388.3 178.7
5/23/2019 3:48:26 PM 385.0 175.4
5/23/2019 3:48:27 PM 381.4 171.8
5/23/2019 3:48:28 PM 378.3 168.7
5/23/2019 3:48:29 PM 374.6 165.0
5/23/2019 3:48:30 PM 371.1 161.5
5/23/2019 3:48:31 PM 368.2 158.6
5/23/2019 3:48:32 PM 364.9 155.3
5/23/2019 3:48:33 PM 362.2 152.6
5/23/2019 3:48:34 PM 359.0 149.4
5/23/2019 3:48:35 PM 356.2 146.6
5/23/2019 3:48:36 PM 353.0 143.4
5/23/2019 3:48:37 PM 350.2 140.6
5/23/2019 3:48:38 PM 347.1 137.5
5/23/2019 3:48:39 PM 344.3 134.7
5/23/2019 3:48:40 PM 341.3 131.7
5/23/2019 3:48:41 PM 338.8 129.2
Page 119 of 452 August 2019
APPENDIX E28: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-2 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-2 Data Log
5/23/2019 3:48:42 PM 336.1 126.5
5/23/2019 3:48:43 PM 333.7 124.1
5/23/2019 3:48:44 PM 331.1 121.5
5/23/2019 3:48:45 PM 328.8 119.2
5/23/2019 3:48:46 PM 326.3 116.7
5/23/2019 3:48:47 PM 324.0 114.4
5/23/2019 3:48:48 PM 321.6 112.0
5/23/2019 3:48:49 PM 319.3 109.7
5/23/2019 3:48:50 PM 317.4 107.8
5/23/2019 3:48:51 PM 315.2 105.6
5/23/2019 3:48:52 PM 313.3 103.7
5/23/2019 3:48:53 PM 311.0 101.4
5/23/2019 3:48:54 PM 309.1 99.5
5/23/2019 3:48:55 PM 307.0 97.4
5/23/2019 3:48:56 PM 305.2 95.6
5/23/2019 3:48:57 PM 303.2 93.6
5/23/2019 3:48:58 PM 301.5 91.9
5/23/2019 3:48:59 PM 299.5 89.9
5/23/2019 3:49:00 PM 297.9 88.3
5/23/2019 3:49:01 PM 296.1 86.5
5/23/2019 3:49:02 PM 294.5 84.9
5/23/2019 3:49:03 PM 292.8 83.2
5/23/2019 3:49:04 PM 291.3 81.7
5/23/2019 3:49:05 PM 289.7 80.1
5/23/2019 3:49:06 PM 288.4 78.8
5/23/2019 3:49:07 PM 286.8 77.2
5/23/2019 3:49:08 PM 285.5 75.9
5/23/2019 3:49:09 PM 284.0 74.4
5/23/2019 3:49:10 PM 282.5 72.9
5/23/2019 3:49:11 PM 281.2 71.6
5/23/2019 3:49:12 PM 279.7 70.1
5/23/2019 3:49:13 PM 278.5 68.9
5/23/2019 3:49:14 PM 277.1 67.5
5/23/2019 3:49:15 PM 275.9 66.3
5/23/2019 3:49:16 PM 274.5 64.9
5/23/2019 3:49:17 PM 273.5 63.9
5/23/2019 3:49:18 PM 272.3 62.7
5/23/2019 3:49:19 PM 271.2 61.6
5/23/2019 3:49:20 PM 270.0 60.4
5/23/2019 3:49:21 PM 269.0 59.4
5/23/2019 3:49:22 PM 267.9 58.3
5/23/2019 3:49:23 PM 266.9 57.3
5/23/2019 3:49:24 PM 265.8 56.2
5/23/2019 3:49:25 PM 264.9 55.3
5/23/2019 3:49:26 PM 263.9 54.3
5/23/2019 3:49:27 PM 263.0 53.4
5/23/2019 3:49:28 PM 262.1 52.5
5/23/2019 3:49:29 PM 261.1 51.5
5/23/2019 3:49:30 PM 260.3 50.7
5/23/2019 3:49:31 PM 259.3 49.7
5/23/2019 3:49:32 PM 258.4 48.8
5/23/2019 3:49:33 PM 257.5 47.9
5/23/2019 3:49:34 PM 256.7 47.1
5/23/2019 3:49:35 PM 255.8 46.2
5/23/2019 3:49:36 PM 255.0 45.4
5/23/2019 3:49:37 PM 254.2 44.6
5/23/2019 3:49:38 PM 253.5 43.9
5/23/2019 3:49:39 PM 252.7 43.1
5/23/2019 3:49:40 PM 252.0 42.4
5/23/2019 3:49:41 PM 251.2 41.6
5/23/2019 3:49:42 PM 250.5 40.9
5/23/2019 3:49:43 PM 249.7 40.1
5/23/2019 3:49:44 PM 249.1 39.5
5/23/2019 3:49:45 PM 248.3 38.7
5/23/2019 3:49:46 PM 247.7 38.1
5/23/2019 3:49:47 PM 247.0 37.4
5/23/2019 3:49:48 PM 246.4 36.8
5/23/2019 3:49:49 PM 245.8 36.2
5/23/2019 3:49:50 PM 245.1 35.5
5/23/2019 3:49:51 PM 244.6 35.0
5/23/2019 3:49:52 PM 243.9 34.3
5/23/2019 3:49:53 PM 243.4 33.8
5/23/2019 3:49:54 PM 242.7 33.1
5/23/2019 3:49:55 PM 242.3 32.7
5/23/2019 3:49:56 PM 241.8 32.2
5/23/2019 3:49:57 PM 241.2 31.6
5/23/2019 3:49:58 PM 240.8 31.2
5/23/2019 3:49:59 PM 240.3 30.7
5/23/2019 3:50:00 PM 239.7 30.1
Page 120 of 452 August 2019
APPENDIX E28: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-2 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-2 Data Log
5/23/2019 3:50:01 PM 239.3 29.7
5/23/2019 3:50:02 PM 238.8 29.2
5/23/2019 3:50:03 PM 238.2 28.6
5/23/2019 3:50:04 PM 237.7 28.1
5/23/2019 3:50:05 PM 237.4 27.8
5/23/2019 3:50:06 PM 236.8 27.2
5/23/2019 3:50:07 PM 236.5 26.9
5/23/2019 3:50:08 PM 236.0 26.4
5/23/2019 3:50:09 PM 235.5 25.9
5/23/2019 3:50:10 PM 235.1 25.5
5/23/2019 3:50:11 PM 234.8 25.2
5/23/2019 3:50:12 PM 234.3 24.7
5/23/2019 3:50:13 PM 233.9 24.3
5/23/2019 3:50:14 PM 233.6 24.0
5/23/2019 3:50:15 PM 233.2 23.6
5/23/2019 3:50:16 PM 232.8 23.2
5/23/2019 3:50:17 PM 232.6 23.0
5/23/2019 3:50:18 PM 232.2 22.6
5/23/2019 3:50:19 PM 231.8 22.2
5/23/2019 3:50:20 PM 231.6 22.0
5/23/2019 3:50:21 PM 231.2 21.6
5/23/2019 3:50:22 PM 230.9 21.3
5/23/2019 3:50:23 PM 230.7 21.1
5/23/2019 3:50:24 PM 230.3 20.7
5/23/2019 3:50:25 PM 230.0 20.4
5/23/2019 3:50:26 PM 229.8 20.2
5/23/2019 3:50:27 PM 229.3 19.7
5/23/2019 3:50:28 PM 229.1 19.5
5/23/2019 3:50:29 PM 228.9 19.3
5/23/2019 3:50:30 PM 228.5 18.9
5/23/2019 3:50:31 PM 228.3 18.7
5/23/2019 3:50:32 PM 228.0 18.4
5/23/2019 3:50:33 PM 227.6 18.0
5/23/2019 3:50:34 PM 227.4 17.8
5/23/2019 3:50:35 PM 227.2 17.6
5/23/2019 3:50:36 PM 226.8 17.2
5/23/2019 3:50:37 PM 226.5 16.9
5/23/2019 3:50:38 PM 226.3 16.7
5/23/2019 3:50:39 PM 226.0 16.4
5/23/2019 3:50:40 PM 225.8 16.2
5/23/2019 3:50:41 PM 225.5 15.9
5/23/2019 3:50:42 PM 225.3 15.7
5/23/2019 3:50:43 PM 225.0 15.4
5/23/2019 3:50:44 PM 224.7 15.1
5/23/2019 3:50:45 PM 224.5 14.9
5/23/2019 3:50:46 PM 224.2 14.6
5/23/2019 3:50:47 PM 224.0 14.4
5/23/2019 3:50:48 PM 223.8 14.2
5/23/2019 3:50:49 PM 223.5 13.9
5/23/2019 3:50:50 PM 223.4 13.8
5/23/2019 3:50:51 PM 223.1 13.5
5/23/2019 3:50:52 PM 222.9 13.3
5/23/2019 3:50:53 PM 222.7 13.1
5/23/2019 3:50:54 PM 222.5 12.9
5/23/2019 3:50:55 PM 222.3 12.7
5/23/2019 3:50:56 PM 222.1 12.5
5/23/2019 3:50:57 PM 221.9 12.3
5/23/2019 3:50:58 PM 221.7 12.1
5/23/2019 3:50:59 PM 221.5 11.9
5/23/2019 3:51:00 PM 221.4 11.8
5/23/2019 3:51:01 PM 221.1 11.5
5/23/2019 3:51:02 PM 221.0 11.4
5/23/2019 3:51:03 PM 220.8 11.2
5/23/2019 3:51:04 PM 220.6 11.0
5/23/2019 3:51:05 PM 220.5 10.9
5/23/2019 3:51:06 PM 220.3 10.7
5/23/2019 3:51:07 PM 220.1 10.5
5/23/2019 3:51:08 PM 220.0 10.4
5/23/2019 3:51:09 PM 219.7 10.1
5/23/2019 3:51:10 PM 219.6 10.0
5/23/2019 3:51:11 PM 219.4 9.8
5/23/2019 3:51:12 PM 219.2 9.6
5/23/2019 3:51:13 PM 219.1 9.5
5/23/2019 3:51:14 PM 218.9 9.3
5/23/2019 3:51:15 PM 218.7 9.1
5/23/2019 3:51:16 PM 218.6 9.0
5/23/2019 3:51:17 PM 218.4 8.8
5/23/2019 3:51:18 PM 218.2 8.6
5/23/2019 3:51:19 PM 218.0 8.4
Page 121 of 452 August 2019
APPENDIX E28: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-2 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-2 Data Log
5/23/2019 3:51:20 PM 217.9 8.3
5/23/2019 3:51:21 PM 217.7 8.1
5/23/2019 3:51:22 PM 217.6 8.0
5/23/2019 3:51:23 PM 217.4 7.8
5/23/2019 3:51:24 PM 217.3 7.7
5/23/2019 3:51:25 PM 217.2 7.6
5/23/2019 3:51:26 PM 217.0 7.4
5/23/2019 3:51:27 PM 216.9 7.3
5/23/2019 3:51:28 PM 216.7 7.1
5/23/2019 3:51:29 PM 216.6 7.0
5/23/2019 3:51:30 PM 216.5 6.9
5/23/2019 3:51:31 PM 216.4 6.8
5/23/2019 3:51:32 PM 216.3 6.7
5/23/2019 3:51:33 PM 216.2 6.6
5/23/2019 3:51:34 PM 216.0 6.4
5/23/2019 3:51:35 PM 216.0 6.4
5/23/2019 3:51:36 PM 215.8 6.2
5/23/2019 3:51:37 PM 215.7 6.1
5/23/2019 3:51:38 PM 215.7 6.1
5/23/2019 3:51:39 PM 215.5 5.9
5/23/2019 3:51:40 PM 215.5 5.9
5/23/2019 3:51:41 PM 215.4 5.8
5/23/2019 3:51:42 PM 215.3 5.7
5/23/2019 3:51:43 PM 215.2 5.6
5/23/2019 3:51:44 PM 215.1 5.5
5/23/2019 3:51:45 PM 215.0 5.4
5/23/2019 3:51:46 PM 215.0 5.4
5/23/2019 3:51:47 PM 214.9 5.3
5/23/2019 3:51:48 PM 214.8 5.2
5/23/2019 3:51:49 PM 214.7 5.1
5/23/2019 3:51:50 PM 214.7 5.1
5/23/2019 3:51:51 PM 214.6 5.0
5/23/2019 3:51:52 PM 214.5 4.9
5/23/2019 3:51:53 PM 214.4 4.8
5/23/2019 3:51:54 PM 214.3 4.7
5/23/2019 3:51:55 PM 214.2 4.6
5/23/2019 3:51:56 PM 214.1 4.5
5/23/2019 3:51:57 PM 214.1 4.5
5/23/2019 3:51:58 PM 214.0 4.4
5/23/2019 3:51:59 PM 213.8 4.2
5/23/2019 3:52:00 PM 213.8 4.2
5/23/2019 3:52:01 PM 213.7 4.1
5/23/2019 3:52:02 PM 213.6 4.0
5/23/2019 3:52:03 PM 213.5 3.9
5/23/2019 3:52:04 PM 213.4 3.8
5/23/2019 3:52:05 PM 213.4 3.8
5/23/2019 3:52:06 PM 213.3 3.7
5/23/2019 3:52:07 PM 213.2 3.6
5/23/2019 3:52:08 PM 213.1 3.5
5/23/2019 3:52:09 PM 213.1 3.5
5/23/2019 3:52:10 PM 213.0 3.4
5/23/2019 3:52:11 PM 212.9 3.3
5/23/2019 3:52:12 PM 212.8 3.2
5/23/2019 3:52:13 PM 212.8 3.2
5/23/2019 3:52:14 PM 212.7 3.1
5/23/2019 3:52:15 PM 212.6 3.0
5/23/2019 3:52:16 PM 212.6 3.0
5/23/2019 3:52:17 PM 212.5 2.9
5/23/2019 3:52:18 PM 212.4 2.8
5/23/2019 3:52:19 PM 212.3 2.7
5/23/2019 3:52:20 PM 212.3 2.7
5/23/2019 3:52:21 PM 212.2 2.6
5/23/2019 3:52:22 PM 212.1 2.5
5/23/2019 3:52:23 PM 212.1 2.5
5/23/2019 3:52:24 PM 212.0 2.4
5/23/2019 3:52:25 PM 211.9 2.3
5/23/2019 3:52:26 PM 211.9 2.3
5/23/2019 3:52:27 PM 211.8 2.2
5/23/2019 3:52:28 PM 211.7 2.1
5/23/2019 3:52:29 PM 211.7 2.1
5/23/2019 3:52:30 PM 211.6 2.0
5/23/2019 3:52:31 PM 211.6 2.0
5/23/2019 3:52:32 PM 211.5 1.9
5/23/2019 3:52:33 PM 211.4 1.8
5/23/2019 3:52:34 PM 211.4 1.8
5/23/2019 3:52:35 PM 211.3 1.7
5/23/2019 3:52:36 PM 211.3 1.7
5/23/2019 3:52:37 PM 211.3 1.7
5/23/2019 3:52:38 PM 211.2 1.6
Page 122 of 452 August 2019
APPENDIX E28: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-2 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-2 Data Log
5/23/2019 3:52:39 PM 211.2 1.6
5/23/2019 3:52:40 PM 211.1 1.5
5/23/2019 3:52:41 PM 211.1 1.5
5/23/2019 3:52:42 PM 211.1 1.5
5/23/2019 3:52:43 PM 211.0 1.4
5/23/2019 3:52:44 PM 210.9 1.3
5/23/2019 3:52:45 PM 210.9 1.3
5/23/2019 3:52:46 PM 210.8 1.2
5/23/2019 3:52:47 PM 210.8 1.2
5/23/2019 3:52:48 PM 210.7 1.1
5/23/2019 3:52:49 PM 210.7 1.1
5/23/2019 3:52:50 PM 210.6 1.0
Page 123 of 452 August 2019
APPENDIX E28: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-2 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-A3 TEST-2 1504
SEEP-A3 TEST-2 1504
SEEP-A3 TEST-2 1505
SEEP-A3 TEST-2 1506
Location EC Reading
(µS/cms)
SEEP-A3 TEST-2 48.7
SEEP-A3 TEST-2 181
SEEP-A3 TEST-2 450
SEEP-A3 TEST-2 3,464
SEEP-A3 TEST-2 15,648
SEEP-A3 TEST-2 127,541
q 300,300 mg
K 1.2785 (µS/cms) / (mg/L)
(s) . (µS/cms)
Q 2.9 L/s
46.0 GPM
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(°C)
Table E2 SEEP-A3 TEST-2 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
(µS/cms)
208.8 19.1
211.0 18.9
210.0 19
208.3 19
209.5 (µS/cms)
26.6
Average (pre-test) 209.6 (µS/cms)
Average (post-test) 214.2 (µS/cms)
Table E3 SEEP-A3TEST-2 YSI Salt Dilution Calibration Data
Calibration
Concentration Temperature
(mg/L) (°C)
26.9
100 27.1
1,000 27.5
Calculated Flow Rate
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
10000 27.4
100,000 27.5
Table E4 SEEP-A3 TEST-2 Flow Calculation Summary
Mass of Salt injected
132,598.3 SUM:Δt(EC
t-ECbkg)
Slope of Calibration Curve
Integral of Conductivity Data
Curve
10
1
Geo Mean 209.5
Average
(µS/cms)
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 124 of 452 August 2019
APPENDIX E29: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-3 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
5/23/2019 4:01:18 PM 211.6 -
5/23/2019 4:01:19 PM 211.5 -
5/23/2019 4:01:20 PM 211.3 -
5/23/2019 4:01:21 PM 211.2 -
5/23/2019 4:01:22 PM 211.1 -
5/23/2019 4:01:23 PM 211.0 -
5/23/2019 4:01:24 PM 211.0 -
5/23/2019 4:01:25 PM 210.9 -
5/23/2019 4:01:26 PM 210.8 -
5/23/2019 4:01:27 PM 210.8 -
5/23/2019 4:01:28 PM 210.6 -
5/23/2019 4:01:29 PM 210.5 -
5/23/2019 4:01:30 PM 210.3 -
5/23/2019 4:01:31 PM 210.1 -
5/23/2019 4:01:32 PM 210.1 -
5/23/2019 4:01:33 PM 210.1 -
5/23/2019 4:01:34 PM 210.1 -
5/23/2019 4:01:35 PM 210.1 -
5/23/2019 4:01:36 PM 210.1 -
5/23/2019 4:01:37 PM 210.2 -
5/23/2019 4:01:38 PM 210.2 -
5/23/2019 4:01:39 PM 210.2 -
5/23/2019 4:01:40 PM 210.2 -
5/23/2019 4:01:41 PM 210.3 -
5/23/2019 4:01:42 PM 210.3 -
5/23/2019 4:01:43 PM 210.4 -
5/23/2019 4:01:44 PM 210.4 -
5/23/2019 4:01:45 PM 210.5 -
5/23/2019 4:01:46 PM 210.7 -
5/23/2019 4:01:47 PM 211.0 -
5/23/2019 4:01:48 PM 262.8 52.2
5/23/2019 4:01:49 PM 313.4 102.8
5/23/2019 4:01:50 PM 402.8 192.2
5/23/2019 4:01:51 PM 478.0 267.4
5/23/2019 4:01:52 PM 744.1 533.5
5/23/2019 4:01:53 PM 1238.5 1027.9
5/23/2019 4:01:54 PM 1465.2 1254.6
5/23/2019 4:01:55 PM 1802.7 1592.1
5/23/2019 4:01:56 PM 2263.8 2053.2
5/23/2019 4:01:57 PM 2460.5 2249.9
5/23/2019 4:01:58 PM 3201.8 2991.2
5/23/2019 4:01:59 PM 3522.9 3312.3
5/23/2019 4:02:00 PM 4012.3 3801.7
5/23/2019 4:02:01 PM 4136.4 3925.8
5/23/2019 4:02:02 PM 4284.7 4074.1
5/23/2019 4:02:03 PM 4253.1 4042.5
5/23/2019 4:02:04 PM 4251.8 4041.2
5/23/2019 4:02:05 PM 4245.4 4034.8
5/23/2019 4:02:06 PM 4237.7 4027.1
5/23/2019 4:02:07 PM 4219.8 4009.2
5/23/2019 4:02:08 PM 4195.2 3984.6
5/23/2019 4:02:09 PM 3854.4 3643.8
5/23/2019 4:02:10 PM 3784.5 3573.9
5/23/2019 4:02:11 PM 3636.8 3426.2
5/23/2019 4:02:12 PM 3623.0 3412.4
5/23/2019 4:02:13 PM 3334.8 3124.2
5/23/2019 4:02:14 PM 3248.7 3038.1
5/23/2019 4:02:15 PM 3139.4 2928.8
5/23/2019 4:02:16 PM 3019.9 2809.3
5/23/2019 4:02:17 PM 2974.2 2763.6
5/23/2019 4:02:18 PM 2905.6 2695.0
5/23/2019 4:02:19 PM 2603.6 2393.0
5/23/2019 4:02:20 PM 2515.4 2304.8
5/23/2019 4:02:21 PM 2350.4 2139.8
5/23/2019 4:02:22 PM 2289.0 2078.4
5/23/2019 4:02:23 PM 2053.0 1842.4
5/23/2019 4:02:24 PM 1887.5 1676.9
5/23/2019 4:02:25 PM 1814.3 1603.7
5/23/2019 4:02:26 PM 1693.5 1482.9
5/23/2019 4:02:27 PM 1644.4 1433.8
5/23/2019 4:02:28 PM 1484.0 1273.4
5/23/2019 4:02:29 PM 1394.9 1184.3
5/23/2019 4:02:30 PM 1278.2 1067.6
5/23/2019 4:02:31 PM 1238.0 1027.4
5/23/2019 4:02:32 PM 1196.3 985.7
Table E1 SEEP-A3 TEST-3 Data Log
Page 125 of 452 August 2019
APPENDIX E29: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-3 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-3 Data Log
5/23/2019 4:02:33 PM 1169.2 958.6
5/23/2019 4:02:34 PM 1065.6 855.0
5/23/2019 4:02:35 PM 1010.1 799.5
5/23/2019 4:02:36 PM 960.5 749.9
5/23/2019 4:02:37 PM 948.0 737.4
5/23/2019 4:02:38 PM 932.7 722.1
5/23/2019 4:02:39 PM 913.3 702.7
5/23/2019 4:02:40 PM 830.2 619.6
5/23/2019 4:02:41 PM 792.1 581.5
5/23/2019 4:02:42 PM 779.7 569.1
5/23/2019 4:02:43 PM 755.1 544.5
5/23/2019 4:02:44 PM 732.0 521.4
5/23/2019 4:02:45 PM 713.7 503.1
5/23/2019 4:02:46 PM 655.9 445.3
5/23/2019 4:02:47 PM 655.7 445.1
5/23/2019 4:02:48 PM 600.9 390.3
5/23/2019 4:02:49 PM 602.1 391.5
5/23/2019 4:02:50 PM 597.1 386.5
5/23/2019 4:02:51 PM 589.1 378.5
5/23/2019 4:02:52 PM 583.8 373.2
5/23/2019 4:02:53 PM 577.5 366.9
5/23/2019 4:02:54 PM 572.4 361.8
5/23/2019 4:02:55 PM 566.5 355.9
5/23/2019 4:02:56 PM 561.6 351.0
5/23/2019 4:02:57 PM 556.7 346.1
5/23/2019 4:02:58 PM 552.3 341.7
5/23/2019 4:02:59 PM 503.3 292.7
5/23/2019 4:03:00 PM 493.3 282.7
5/23/2019 4:03:01 PM 486.5 275.9
5/23/2019 4:03:02 PM 482.4 271.8
5/23/2019 4:03:03 PM 477.7 267.1
5/23/2019 4:03:04 PM 472.4 261.8
5/23/2019 4:03:05 PM 468.3 257.7
5/23/2019 4:03:06 PM 464.7 254.1
5/23/2019 4:03:07 PM 461.3 250.7
5/23/2019 4:03:08 PM 458.1 247.5
5/23/2019 4:03:09 PM 455.3 244.7
5/23/2019 4:03:10 PM 452.4 241.8
5/23/2019 4:03:11 PM 449.7 239.1
5/23/2019 4:03:12 PM 446.6 236.0
5/23/2019 4:03:13 PM 444.1 233.5
5/23/2019 4:03:14 PM 441.2 230.6
5/23/2019 4:03:15 PM 438.4 227.8
5/23/2019 4:03:16 PM 432.4 221.8
5/23/2019 4:03:17 PM 427.5 216.9
5/23/2019 4:03:18 PM 422.0 211.4
5/23/2019 4:03:19 PM 417.2 206.6
5/23/2019 4:03:20 PM 411.7 201.1
5/23/2019 4:03:21 PM 406.7 196.1
5/23/2019 4:03:22 PM 401.3 190.7
5/23/2019 4:03:23 PM 396.1 185.5
5/23/2019 4:03:24 PM 391.8 181.2
5/23/2019 4:03:25 PM 387.1 176.5
5/23/2019 4:03:26 PM 383.1 172.5
5/23/2019 4:03:27 PM 378.6 168.0
5/23/2019 4:03:28 PM 374.7 164.1
5/23/2019 4:03:29 PM 370.4 159.8
5/23/2019 4:03:30 PM 366.8 156.2
5/23/2019 4:03:31 PM 362.8 152.2
5/23/2019 4:03:32 PM 359.6 149.0
5/23/2019 4:03:33 PM 356.4 145.8
5/23/2019 4:03:34 PM 353.7 143.1
5/23/2019 4:03:35 PM 350.8 140.2
5/23/2019 4:03:36 PM 348.2 137.6
5/23/2019 4:03:37 PM 345.4 134.8
5/23/2019 4:03:38 PM 343.0 132.4
5/23/2019 4:03:39 PM 340.4 129.8
5/23/2019 4:03:40 PM 338.1 127.5
5/23/2019 4:03:41 PM 335.8 125.2
5/23/2019 4:03:42 PM 333.7 123.1
5/23/2019 4:03:43 PM 331.9 121.3
5/23/2019 4:03:44 PM 330.1 119.5
5/23/2019 4:03:45 PM 328.4 117.8
5/23/2019 4:03:46 PM 326.6 116.0
5/23/2019 4:03:47 PM 325.0 114.4
5/23/2019 4:03:48 PM 323.2 112.6
5/23/2019 4:03:49 PM 321.5 110.9
5/23/2019 4:03:50 PM 319.7 109.1
5/23/2019 4:03:51 PM 318.2 107.6
5/23/2019 4:03:52 PM 316.4 105.8
5/23/2019 4:03:53 PM 314.9 104.3
5/23/2019 4:03:54 PM 313.1 102.5
5/23/2019 4:03:55 PM 311.4 100.8
5/23/2019 4:03:56 PM 309.4 98.8
5/23/2019 4:03:57 PM 307.7 97.1
Page 126 of 452 August 2019
APPENDIX E29: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-3 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-3 Data Log
5/23/2019 4:03:58 PM 305.8 95.2
5/23/2019 4:03:59 PM 304.2 93.6
5/23/2019 4:04:00 PM 302.4 91.8
5/23/2019 4:04:01 PM 300.8 90.2
5/23/2019 4:04:02 PM 299.2 88.6
5/23/2019 4:04:03 PM 297.6 87.0
5/23/2019 4:04:04 PM 296.2 85.6
5/23/2019 4:04:05 PM 294.7 84.1
5/23/2019 4:04:06 PM 293.3 82.7
5/23/2019 4:04:07 PM 291.8 81.2
5/23/2019 4:04:08 PM 290.6 80.0
5/23/2019 4:04:09 PM 289.3 78.7
5/23/2019 4:04:10 PM 288.3 77.7
5/23/2019 4:04:11 PM 287.0 76.4
5/23/2019 4:04:12 PM 285.8 75.2
5/23/2019 4:04:13 PM 284.5 73.9
5/23/2019 4:04:14 PM 283.4 72.8
5/23/2019 4:04:15 PM 282.1 71.5
5/23/2019 4:04:16 PM 281.0 70.4
5/23/2019 4:04:17 PM 279.7 69.1
5/23/2019 4:04:18 PM 278.7 68.1
5/23/2019 4:04:19 PM 277.5 66.9
5/23/2019 4:04:20 PM 276.4 65.8
5/23/2019 4:04:21 PM 275.2 64.6
5/23/2019 4:04:22 PM 274.1 63.5
5/23/2019 4:04:23 PM 272.9 62.3
5/23/2019 4:04:24 PM 271.8 61.2
5/23/2019 4:04:25 PM 270.8 60.2
5/23/2019 4:04:26 PM 269.8 59.2
5/23/2019 4:04:27 PM 268.9 58.3
5/23/2019 4:04:28 PM 267.9 57.3
5/23/2019 4:04:29 PM 267.0 56.4
5/23/2019 4:04:30 PM 266.0 55.4
5/23/2019 4:04:31 PM 265.1 54.5
5/23/2019 4:04:32 PM 264.1 53.5
5/23/2019 4:04:33 PM 263.3 52.7
5/23/2019 4:04:34 PM 262.4 51.8
5/23/2019 4:04:35 PM 261.5 50.9
5/23/2019 4:04:36 PM 260.7 50.1
5/23/2019 4:04:37 PM 259.9 49.3
5/23/2019 4:04:38 PM 259.1 48.5
5/23/2019 4:04:39 PM 258.3 47.7
5/23/2019 4:04:40 PM 257.5 46.9
5/23/2019 4:04:41 PM 256.7 46.1
5/23/2019 4:04:42 PM 255.9 45.3
5/23/2019 4:04:43 PM 255.1 44.5
5/23/2019 4:04:44 PM 254.4 43.8
5/23/2019 4:04:45 PM 253.6 43.0
5/23/2019 4:04:46 PM 253.0 42.4
5/23/2019 4:04:47 PM 252.3 41.7
5/23/2019 4:04:48 PM 251.7 41.1
5/23/2019 4:04:49 PM 251.1 40.5
5/23/2019 4:04:50 PM 250.5 39.9
5/23/2019 4:04:51 PM 249.9 39.3
5/23/2019 4:04:52 PM 249.3 38.7
5/23/2019 4:04:53 PM 248.8 38.2
5/23/2019 4:04:54 PM 248.3 37.7
5/23/2019 4:04:55 PM 247.7 37.1
5/23/2019 4:04:56 PM 247.2 36.6
5/23/2019 4:04:57 PM 246.7 36.1
5/23/2019 4:04:58 PM 246.2 35.6
5/23/2019 4:04:59 PM 245.6 35.0
5/23/2019 4:05:00 PM 245.2 34.6
5/23/2019 4:05:01 PM 244.6 34.0
5/23/2019 4:05:02 PM 244.2 33.6
5/23/2019 4:05:03 PM 243.8 33.2
5/23/2019 4:05:04 PM 243.2 32.6
5/23/2019 4:05:05 PM 242.8 32.2
5/23/2019 4:05:06 PM 242.2 31.6
5/23/2019 4:05:07 PM 241.7 31.1
5/23/2019 4:05:08 PM 241.2 30.6
5/23/2019 4:05:09 PM 240.8 30.2
5/23/2019 4:05:10 PM 240.3 29.7
5/23/2019 4:05:11 PM 239.8 29.2
5/23/2019 4:05:12 PM 239.3 28.7
5/23/2019 4:05:13 PM 238.8 28.2
5/23/2019 4:05:14 PM 238.3 27.7
Page 127 of 452 August 2019
APPENDIX E29: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-3 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-3 Data Log
5/23/2019 4:05:15 PM 237.9 27.3
5/23/2019 4:05:16 PM 237.4 26.8
5/23/2019 4:05:17 PM 237.0 26.4
5/23/2019 4:05:18 PM 236.5 25.9
5/23/2019 4:05:19 PM 236.1 25.5
5/23/2019 4:05:20 PM 235.7 25.1
5/23/2019 4:05:21 PM 235.4 24.8
5/23/2019 4:05:22 PM 235.0 24.4
5/23/2019 4:05:23 PM 234.7 24.1
5/23/2019 4:05:24 PM 234.4 23.8
5/23/2019 4:05:25 PM 234.1 23.5
5/23/2019 4:05:26 PM 233.8 23.2
5/23/2019 4:05:27 PM 233.5 22.9
5/23/2019 4:05:28 PM 233.2 22.6
5/23/2019 4:05:29 PM 233.0 22.4
5/23/2019 4:05:30 PM 232.6 22.0
5/23/2019 4:05:31 PM 232.4 21.8
5/23/2019 4:05:32 PM 232.0 21.4
5/23/2019 4:05:33 PM 231.8 21.2
5/23/2019 4:05:34 PM 231.5 20.9
5/23/2019 4:05:35 PM 231.1 20.5
5/23/2019 4:05:36 PM 230.9 20.3
5/23/2019 4:05:37 PM 230.7 20.1
5/23/2019 4:05:38 PM 230.4 19.8
5/23/2019 4:05:39 PM 230.1 19.5
5/23/2019 4:05:40 PM 229.8 19.2
5/23/2019 4:05:41 PM 229.6 19.0
5/23/2019 4:05:42 PM 229.3 18.7
5/23/2019 4:05:43 PM 229.0 18.4
5/23/2019 4:05:44 PM 228.7 18.1
5/23/2019 4:05:45 PM 228.5 17.9
5/23/2019 4:05:46 PM 228.3 17.7
5/23/2019 4:05:47 PM 228.0 17.4
5/23/2019 4:05:48 PM 227.8 17.2
5/23/2019 4:05:49 PM 227.6 17.0
5/23/2019 4:05:50 PM 227.3 16.7
5/23/2019 4:05:51 PM 227.1 16.5
5/23/2019 4:05:52 PM 226.9 16.3
5/23/2019 4:05:53 PM 226.7 16.1
5/23/2019 4:05:54 PM 226.5 15.9
5/23/2019 4:05:55 PM 226.3 15.7
5/23/2019 4:05:56 PM 226.1 15.5
5/23/2019 4:05:57 PM 225.9 15.3
5/23/2019 4:05:58 PM 225.7 15.1
5/23/2019 4:05:59 PM 225.5 14.9
5/23/2019 4:06:00 PM 225.3 14.7
5/23/2019 4:06:01 PM 225.1 14.5
5/23/2019 4:06:02 PM 224.9 14.3
5/23/2019 4:06:03 PM 224.7 14.1
5/23/2019 4:06:04 PM 224.5 13.9
5/23/2019 4:06:05 PM 224.3 13.7
5/23/2019 4:06:06 PM 224.2 13.6
5/23/2019 4:06:07 PM 224.0 13.4
5/23/2019 4:06:08 PM 223.8 13.2
5/23/2019 4:06:09 PM 223.7 13.1
5/23/2019 4:06:10 PM 223.5 12.9
5/23/2019 4:06:11 PM 223.3 12.7
5/23/2019 4:06:12 PM 223.1 12.5
5/23/2019 4:06:13 PM 222.9 12.3
5/23/2019 4:06:14 PM 222.7 12.1
5/23/2019 4:06:15 PM 222.6 12.0
5/23/2019 4:06:16 PM 222.4 11.8
5/23/2019 4:06:17 PM 222.2 11.6
5/23/2019 4:06:18 PM 222.0 11.4
5/23/2019 4:06:19 PM 221.9 11.3
5/23/2019 4:06:20 PM 221.7 11.1
5/23/2019 4:06:21 PM 221.5 10.9
5/23/2019 4:06:22 PM 221.3 10.7
5/23/2019 4:06:23 PM 221.1 10.5
5/23/2019 4:06:24 PM 220.9 10.3
5/23/2019 4:06:25 PM 220.8 10.2
5/23/2019 4:06:26 PM 220.6 10.0
5/23/2019 4:06:27 PM 220.4 9.8
5/23/2019 4:06:28 PM 220.3 9.7
5/23/2019 4:06:29 PM 220.1 9.5
5/23/2019 4:06:30 PM 220.0 9.4
5/23/2019 4:06:31 PM 219.8 9.2
5/23/2019 4:06:32 PM 219.7 9.1
5/23/2019 4:06:33 PM 219.6 9.0
5/23/2019 4:06:34 PM 219.5 8.9
5/23/2019 4:06:35 PM 219.4 8.8
5/23/2019 4:06:36 PM 219.4 8.8
5/23/2019 4:06:37 PM 219.3 8.7
5/23/2019 4:06:38 PM 219.2 8.6
5/23/2019 4:06:39 PM 219.1 8.5
5/23/2019 4:06:40 PM 219.0 8.4
Page 128 of 452 August 2019
APPENDIX E29: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-3 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-3 Data Log
5/23/2019 4:06:41 PM 219.0 8.4
5/23/2019 4:06:42 PM 218.9 8.3
5/23/2019 4:06:43 PM 218.7 8.1
5/23/2019 4:06:44 PM 218.6 8.0
5/23/2019 4:06:45 PM 218.5 7.9
5/23/2019 4:06:46 PM 218.4 7.8
5/23/2019 4:06:47 PM 218.3 7.7
5/23/2019 4:06:48 PM 218.2 7.6
5/23/2019 4:06:49 PM 218.1 7.5
5/23/2019 4:06:50 PM 218.0 7.4
5/23/2019 4:06:51 PM 217.9 7.3
5/23/2019 4:06:52 PM 217.8 7.2
5/23/2019 4:06:53 PM 217.7 7.1
5/23/2019 4:06:54 PM 217.6 7.0
5/23/2019 4:06:55 PM 217.5 6.9
5/23/2019 4:06:56 PM 217.5 6.9
5/23/2019 4:06:57 PM 217.4 6.8
5/23/2019 4:06:58 PM 217.3 6.7
5/23/2019 4:06:59 PM 217.2 6.6
5/23/2019 4:07:00 PM 217.1 6.5
5/23/2019 4:07:01 PM 217.0 6.4
5/23/2019 4:07:02 PM 217.0 6.4
5/23/2019 4:07:03 PM 216.9 6.3
5/23/2019 4:07:04 PM 216.8 6.2
5/23/2019 4:07:05 PM 216.7 6.1
5/23/2019 4:07:06 PM 216.7 6.1
5/23/2019 4:07:07 PM 216.6 6.0
5/23/2019 4:07:08 PM 216.5 5.9
5/23/2019 4:07:09 PM 216.5 5.9
5/23/2019 4:07:10 PM 216.4 5.8
5/23/2019 4:07:11 PM 216.3 5.7
5/23/2019 4:07:12 PM 216.2 5.6
5/23/2019 4:07:13 PM 216.1 5.5
5/23/2019 4:07:14 PM 216.0 5.4
5/23/2019 4:07:15 PM 216.0 5.4
5/23/2019 4:07:16 PM 215.9 5.3
5/23/2019 4:07:17 PM 215.8 5.2
5/23/2019 4:07:18 PM 215.7 5.1
5/23/2019 4:07:19 PM 215.7 5.1
5/23/2019 4:07:20 PM 215.6 5.0
5/23/2019 4:07:21 PM 215.5 4.9
5/23/2019 4:07:22 PM 215.4 4.8
5/23/2019 4:07:23 PM 215.4 4.8
5/23/2019 4:07:24 PM 215.3 4.7
5/23/2019 4:07:25 PM 215.3 4.7
5/23/2019 4:07:26 PM 215.2 4.6
5/23/2019 4:07:27 PM 215.2 4.6
5/23/2019 4:07:28 PM 215.1 4.5
5/23/2019 4:07:29 PM 215.0 4.4
5/23/2019 4:07:30 PM 215.0 4.4
5/23/2019 4:07:31 PM 214.9 4.3
5/23/2019 4:07:32 PM 214.8 4.2
5/23/2019 4:07:33 PM 214.8 4.2
5/23/2019 4:07:34 PM 214.7 4.1
5/23/2019 4:07:35 PM 214.6 4.0
5/23/2019 4:07:36 PM 214.5 3.9
5/23/2019 4:07:37 PM 214.5 3.9
5/23/2019 4:07:38 PM 214.4 3.8
5/23/2019 4:07:39 PM 214.3 3.7
5/23/2019 4:07:40 PM 214.3 3.7
5/23/2019 4:07:41 PM 214.2 3.6
5/23/2019 4:07:42 PM 214.2 3.6
5/23/2019 4:07:43 PM 214.1 3.5
5/23/2019 4:07:44 PM 214.1 3.5
5/23/2019 4:07:45 PM 214.0 3.4
5/23/2019 4:07:46 PM 214.0 3.4
5/23/2019 4:07:47 PM 213.9 3.3
5/23/2019 4:07:48 PM 213.9 3.3
5/23/2019 4:07:49 PM 213.8 3.2
5/23/2019 4:07:50 PM 213.8 3.2
5/23/2019 4:07:51 PM 213.8 3.2
5/23/2019 4:07:52 PM 213.7 3.1
5/23/2019 4:07:53 PM 213.7 3.1
5/23/2019 4:07:54 PM 213.6 3.0
5/23/2019 4:07:55 PM 213.6 3.0
5/23/2019 4:07:56 PM 213.5 2.9
5/23/2019 4:07:57 PM 213.5 2.9
5/23/2019 4:07:58 PM 213.4 2.8
5/23/2019 4:07:59 PM 213.4 2.8
5/23/2019 4:08:00 PM 213.3 2.7
5/23/2019 4:08:01 PM 213.3 2.7
5/23/2019 4:08:02 PM 213.3 2.7
Page 129 of 452 August 2019
APPENDIX E29: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-3 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-A3 TEST-3 1504
SEEP-A3 TEST-3 1504
SEEP-A3 TEST-3 1505
SEEP-A3 TEST-3 1506
Location EC Reading
(µS/cms)
SEEP-A3 TEST-3 48.7
SEEP-A3 TEST-3 181
SEEP-A3 TEST-3 450
SEEP-A3 TEST-3 3,464
SEEP-A3 TEST-3 15,648
SEEP-A3 TEST-3 127,541
q 300,100 mg
K 1.2785 (µS/cms) / (mg/L)
(s) . (µS/cms)
Q 2.8 L/s
44.9 GPM
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(°C)
Table E2 SEEP-A3 TEST-3 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
(µS/cms)
208.8 19.1
211.0 18.9
210.0 19
208.3 19
209.5 (µS/cms)
26.6
Average (pre-test)210.6 (µS/cms)
Average (post-test)216.1 (µS/cms)
Table E3 SEEP-A3 TEST-3 YSI Salt Dilution Calibration Data
Calibration
Concentration Temperature
(mg/L)(°C)
26.9
100 27.1
1,000 27.5
Calculated Flow Rate
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
10000 27.4
100,000 27.5
Table E4 SEEP-A3 TEST-3 Flow Calculation Summary
Mass of Salt injected
135,637.8 SUM:Δt(ECt-ECbkg)
Slope of Calibration Curve
Integral of Conductivity Data Curve
10
1
Geo Mean 209.5
Average
(µS/cms)
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 130 of 452 August 2019
APPENDIX E30: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-4 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
5/23/2019 4:01:18 PM 211.6 -
5/23/2019 4:01:19 PM 211.5 -
5/23/2019 4:01:20 PM 211.3 -
5/23/2019 4:01:21 PM 211.2 -
5/23/2019 4:01:22 PM 211.1 -
5/23/2019 4:01:23 PM 211.0 -
5/23/2019 4:01:24 PM 211.0 -
5/23/2019 4:01:25 PM 210.9 -
5/23/2019 4:01:26 PM 210.8 -
5/23/2019 4:01:27 PM 210.8 -
5/23/2019 4:01:28 PM 210.6 -
5/23/2019 4:01:29 PM 210.5 -
5/23/2019 4:01:30 PM 210.3 -
5/23/2019 4:01:31 PM 210.1 -
5/23/2019 4:01:32 PM 210.1 -
5/23/2019 4:01:33 PM 210.1 -
5/23/2019 4:01:34 PM 210.1 -
5/23/2019 4:01:35 PM 210.1 -
5/23/2019 4:01:36 PM 210.1 -
5/23/2019 4:01:37 PM 210.2 -
5/23/2019 4:01:38 PM 210.2 -
5/23/2019 4:01:39 PM 210.2 -
5/23/2019 4:01:40 PM 210.2 -
5/23/2019 4:01:41 PM 210.3 -
5/23/2019 4:01:42 PM 210.3 -
5/23/2019 4:01:43 PM 210.4 -
5/23/2019 4:01:44 PM 210.4 -
5/23/2019 4:01:45 PM 210.5 -
5/23/2019 4:01:46 PM 210.7 -
5/23/2019 4:01:47 PM 211.0 -
5/23/2019 4:01:48 PM 262.8 52.2
5/23/2019 4:01:49 PM 313.4 102.8
5/23/2019 4:01:50 PM 402.8 192.2
5/23/2019 4:01:51 PM 478.0 267.4
5/23/2019 4:01:52 PM 744.1 533.5
5/23/2019 4:01:53 PM 1238.5 1027.9
5/23/2019 4:01:54 PM 1465.2 1254.6
5/23/2019 4:01:55 PM 1802.7 1592.1
5/23/2019 4:01:56 PM 2263.8 2053.2
5/23/2019 4:01:57 PM 2460.5 2249.9
5/23/2019 4:01:58 PM 3201.8 2991.2
5/23/2019 4:01:59 PM 3522.9 3312.3
5/23/2019 4:02:00 PM 4012.3 3801.7
5/23/2019 4:02:01 PM 4136.4 3925.8
5/23/2019 4:02:02 PM 4284.7 4074.1
5/23/2019 4:02:03 PM 4253.1 4042.5
5/23/2019 4:02:04 PM 4251.8 4041.2
5/23/2019 4:02:05 PM 4245.4 4034.8
5/23/2019 4:02:06 PM 4237.7 4027.1
5/23/2019 4:02:07 PM 4219.8 4009.2
5/23/2019 4:02:08 PM 4195.2 3984.6
5/23/2019 4:02:09 PM 3854.4 3643.8
5/23/2019 4:02:10 PM 3784.5 3573.9
5/23/2019 4:02:11 PM 3636.8 3426.2
5/23/2019 4:02:12 PM 3623.0 3412.4
5/23/2019 4:02:13 PM 3334.8 3124.2
5/23/2019 4:02:14 PM 3248.7 3038.1
5/23/2019 4:02:15 PM 3139.4 2928.8
5/23/2019 4:02:16 PM 3019.9 2809.3
5/23/2019 4:02:17 PM 2974.2 2763.6
5/23/2019 4:02:18 PM 2905.6 2695.0
5/23/2019 4:02:19 PM 2603.6 2393.0
5/23/2019 4:02:20 PM 2515.4 2304.8
5/23/2019 4:02:21 PM 2350.4 2139.8
5/23/2019 4:02:22 PM 2289.0 2078.4
5/23/2019 4:02:23 PM 2053.0 1842.4
5/23/2019 4:02:24 PM 1887.5 1676.9
5/23/2019 4:02:25 PM 1814.3 1603.7
5/23/2019 4:02:26 PM 1693.5 1482.9
5/23/2019 4:02:27 PM 1644.4 1433.8
Table E1 SEEP-A3 TEST-4 Data Log
Page 131 of 452 August 2019
APPENDIX E30: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-4 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-4 Data Log
5/23/2019 4:02:28 PM 1484.0 1273.4
5/23/2019 4:02:29 PM 1394.9 1184.3
5/23/2019 4:02:30 PM 1278.2 1067.6
5/23/2019 4:02:31 PM 1238.0 1027.4
5/23/2019 4:02:32 PM 1196.3 985.7
5/23/2019 4:02:33 PM 1169.2 958.6
5/23/2019 4:02:34 PM 1065.6 855.0
5/23/2019 4:02:35 PM 1010.1 799.5
5/23/2019 4:02:36 PM 960.5 749.9
5/23/2019 4:02:37 PM 948.0 737.4
5/23/2019 4:02:38 PM 932.7 722.1
5/23/2019 4:02:39 PM 913.3 702.7
5/23/2019 4:02:40 PM 830.2 619.6
5/23/2019 4:02:41 PM 792.1 581.5
5/23/2019 4:02:42 PM 779.7 569.1
5/23/2019 4:02:43 PM 755.1 544.5
5/23/2019 4:02:44 PM 732.0 521.4
5/23/2019 4:02:45 PM 713.7 503.1
5/23/2019 4:02:46 PM 655.9 445.3
5/23/2019 4:02:47 PM 655.7 445.1
5/23/2019 4:02:48 PM 600.9 390.3
5/23/2019 4:02:49 PM 602.1 391.5
5/23/2019 4:02:50 PM 597.1 386.5
5/23/2019 4:02:51 PM 589.1 378.5
5/23/2019 4:02:52 PM 583.8 373.2
5/23/2019 4:02:53 PM 577.5 366.9
5/23/2019 4:02:54 PM 572.4 361.8
5/23/2019 4:02:55 PM 566.5 355.9
5/23/2019 4:02:56 PM 561.6 351.0
5/23/2019 4:02:57 PM 556.7 346.1
5/23/2019 4:02:58 PM 552.3 341.7
5/23/2019 4:02:59 PM 503.3 292.7
5/23/2019 4:03:00 PM 493.3 282.7
5/23/2019 4:03:01 PM 486.5 275.9
5/23/2019 4:03:02 PM 482.4 271.8
5/23/2019 4:03:03 PM 477.7 267.1
5/23/2019 4:03:04 PM 472.4 261.8
5/23/2019 4:03:05 PM 468.3 257.7
5/23/2019 4:03:06 PM 464.7 254.1
5/23/2019 4:03:07 PM 461.3 250.7
5/23/2019 4:03:08 PM 458.1 247.5
5/23/2019 4:03:09 PM 455.3 244.7
5/23/2019 4:03:10 PM 452.4 241.8
5/23/2019 4:03:11 PM 449.7 239.1
5/23/2019 4:03:12 PM 446.6 236.0
5/23/2019 4:03:13 PM 444.1 233.5
5/23/2019 4:03:14 PM 441.2 230.6
5/23/2019 4:03:15 PM 438.4 227.8
5/23/2019 4:03:16 PM 432.4 221.8
5/23/2019 4:03:17 PM 427.5 216.9
5/23/2019 4:03:18 PM 422.0 211.4
5/23/2019 4:03:19 PM 417.2 206.6
5/23/2019 4:03:20 PM 411.7 201.1
5/23/2019 4:03:21 PM 406.7 196.1
5/23/2019 4:03:22 PM 401.3 190.7
5/23/2019 4:03:23 PM 396.1 185.5
5/23/2019 4:03:24 PM 391.8 181.2
5/23/2019 4:03:25 PM 387.1 176.5
5/23/2019 4:03:26 PM 383.1 172.5
5/23/2019 4:03:27 PM 378.6 168.0
5/23/2019 4:03:28 PM 374.7 164.1
5/23/2019 4:03:29 PM 370.4 159.8
5/23/2019 4:03:30 PM 366.8 156.2
5/23/2019 4:03:31 PM 362.8 152.2
5/23/2019 4:03:32 PM 359.6 149.0
5/23/2019 4:03:33 PM 356.4 145.8
5/23/2019 4:03:34 PM 353.7 143.1
5/23/2019 4:03:35 PM 350.8 140.2
5/23/2019 4:03:36 PM 348.2 137.6
5/23/2019 4:03:37 PM 345.4 134.8
5/23/2019 4:03:38 PM 343.0 132.4
5/23/2019 4:03:39 PM 340.4 129.8
5/23/2019 4:03:40 PM 338.1 127.5
5/23/2019 4:03:41 PM 335.8 125.2
5/23/2019 4:03:42 PM 333.7 123.1
5/23/2019 4:03:43 PM 331.9 121.3
5/23/2019 4:03:44 PM 330.1 119.5
Page 132 of 452 August 2019
APPENDIX E30: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-4 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-4 Data Log
5/23/2019 4:03:45 PM 328.4 117.8
5/23/2019 4:03:46 PM 326.6 116.0
5/23/2019 4:03:47 PM 325.0 114.4
5/23/2019 4:03:48 PM 323.2 112.6
5/23/2019 4:03:49 PM 321.5 110.9
5/23/2019 4:03:50 PM 319.7 109.1
5/23/2019 4:03:51 PM 318.2 107.6
5/23/2019 4:03:52 PM 316.4 105.8
5/23/2019 4:03:53 PM 314.9 104.3
5/23/2019 4:03:54 PM 313.1 102.5
5/23/2019 4:03:55 PM 311.4 100.8
5/23/2019 4:03:56 PM 309.4 98.8
5/23/2019 4:03:57 PM 307.7 97.1
5/23/2019 4:03:58 PM 305.8 95.2
5/23/2019 4:03:59 PM 304.2 93.6
5/23/2019 4:04:00 PM 302.4 91.8
5/23/2019 4:04:01 PM 300.8 90.2
5/23/2019 4:04:02 PM 299.2 88.6
5/23/2019 4:04:03 PM 297.6 87.0
5/23/2019 4:04:04 PM 296.2 85.6
5/23/2019 4:04:05 PM 294.7 84.1
5/23/2019 4:04:06 PM 293.3 82.7
5/23/2019 4:04:07 PM 291.8 81.2
5/23/2019 4:04:08 PM 290.6 80.0
5/23/2019 4:04:09 PM 289.3 78.7
5/23/2019 4:04:10 PM 288.3 77.7
5/23/2019 4:04:11 PM 287.0 76.4
5/23/2019 4:04:12 PM 285.8 75.2
5/23/2019 4:04:13 PM 284.5 73.9
5/23/2019 4:04:14 PM 283.4 72.8
5/23/2019 4:04:15 PM 282.1 71.5
5/23/2019 4:04:16 PM 281.0 70.4
5/23/2019 4:04:17 PM 279.7 69.1
5/23/2019 4:04:18 PM 278.7 68.1
5/23/2019 4:04:19 PM 277.5 66.9
5/23/2019 4:04:20 PM 276.4 65.8
5/23/2019 4:04:21 PM 275.2 64.6
5/23/2019 4:04:22 PM 274.1 63.5
5/23/2019 4:04:23 PM 272.9 62.3
5/23/2019 4:04:24 PM 271.8 61.2
5/23/2019 4:04:25 PM 270.8 60.2
5/23/2019 4:04:26 PM 269.8 59.2
5/23/2019 4:04:27 PM 268.9 58.3
5/23/2019 4:04:28 PM 267.9 57.3
5/23/2019 4:04:29 PM 267.0 56.4
5/23/2019 4:04:30 PM 266.0 55.4
5/23/2019 4:04:31 PM 265.1 54.5
5/23/2019 4:04:32 PM 264.1 53.5
5/23/2019 4:04:33 PM 263.3 52.7
5/23/2019 4:04:34 PM 262.4 51.8
5/23/2019 4:04:35 PM 261.5 50.9
5/23/2019 4:04:36 PM 260.7 50.1
5/23/2019 4:04:37 PM 259.9 49.3
5/23/2019 4:04:38 PM 259.1 48.5
5/23/2019 4:04:39 PM 258.3 47.7
5/23/2019 4:04:40 PM 257.5 46.9
5/23/2019 4:04:41 PM 256.7 46.1
5/23/2019 4:04:42 PM 255.9 45.3
5/23/2019 4:04:43 PM 255.1 44.5
5/23/2019 4:04:44 PM 254.4 43.8
5/23/2019 4:04:45 PM 253.6 43.0
5/23/2019 4:04:46 PM 253.0 42.4
5/23/2019 4:04:47 PM 252.3 41.7
5/23/2019 4:04:48 PM 251.7 41.1
5/23/2019 4:04:49 PM 251.1 40.5
5/23/2019 4:04:50 PM 250.5 39.9
5/23/2019 4:04:51 PM 249.9 39.3
5/23/2019 4:04:52 PM 249.3 38.7
5/23/2019 4:04:53 PM 248.8 38.2
5/23/2019 4:04:54 PM 248.3 37.7
5/23/2019 4:04:55 PM 247.7 37.1
5/23/2019 4:04:56 PM 247.2 36.6
5/23/2019 4:04:57 PM 246.7 36.1
5/23/2019 4:04:58 PM 246.2 35.6
5/23/2019 4:04:59 PM 245.6 35.0
5/23/2019 4:05:00 PM 245.2 34.6
5/23/2019 4:05:01 PM 244.6 34.0
5/23/2019 4:05:02 PM 244.2 33.6
5/23/2019 4:05:03 PM 243.8 33.2
Page 133 of 452 August 2019
APPENDIX E30: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-4 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-4 Data Log
5/23/2019 4:05:04 PM 243.2 32.6
5/23/2019 4:05:05 PM 242.8 32.2
5/23/2019 4:05:06 PM 242.2 31.6
5/23/2019 4:05:07 PM 241.7 31.1
5/23/2019 4:05:08 PM 241.2 30.6
5/23/2019 4:05:09 PM 240.8 30.2
5/23/2019 4:05:10 PM 240.3 29.7
5/23/2019 4:05:11 PM 239.8 29.2
5/23/2019 4:05:12 PM 239.3 28.7
5/23/2019 4:05:13 PM 238.8 28.2
5/23/2019 4:05:14 PM 238.3 27.7
5/23/2019 4:05:15 PM 237.9 27.3
5/23/2019 4:05:16 PM 237.4 26.8
5/23/2019 4:05:17 PM 237.0 26.4
5/23/2019 4:05:18 PM 236.5 25.9
5/23/2019 4:05:19 PM 236.1 25.5
5/23/2019 4:05:20 PM 235.7 25.1
5/23/2019 4:05:21 PM 235.4 24.8
5/23/2019 4:05:22 PM 235.0 24.4
5/23/2019 4:05:23 PM 234.7 24.1
5/23/2019 4:05:24 PM 234.4 23.8
5/23/2019 4:05:25 PM 234.1 23.5
5/23/2019 4:05:26 PM 233.8 23.2
5/23/2019 4:05:27 PM 233.5 22.9
5/23/2019 4:05:28 PM 233.2 22.6
5/23/2019 4:05:29 PM 233.0 22.4
5/23/2019 4:05:30 PM 232.6 22.0
5/23/2019 4:05:31 PM 232.4 21.8
5/23/2019 4:05:32 PM 232.0 21.4
5/23/2019 4:05:33 PM 231.8 21.2
5/23/2019 4:05:34 PM 231.5 20.9
5/23/2019 4:05:35 PM 231.1 20.5
5/23/2019 4:05:36 PM 230.9 20.3
5/23/2019 4:05:37 PM 230.7 20.1
5/23/2019 4:05:38 PM 230.4 19.8
5/23/2019 4:05:39 PM 230.1 19.5
5/23/2019 4:05:40 PM 229.8 19.2
5/23/2019 4:05:41 PM 229.6 19.0
5/23/2019 4:05:42 PM 229.3 18.7
5/23/2019 4:05:43 PM 229.0 18.4
5/23/2019 4:05:44 PM 228.7 18.1
5/23/2019 4:05:45 PM 228.5 17.9
5/23/2019 4:05:46 PM 228.3 17.7
5/23/2019 4:05:47 PM 228.0 17.4
5/23/2019 4:05:48 PM 227.8 17.2
5/23/2019 4:05:49 PM 227.6 17.0
5/23/2019 4:05:50 PM 227.3 16.7
5/23/2019 4:05:51 PM 227.1 16.5
5/23/2019 4:05:52 PM 226.9 16.3
5/23/2019 4:05:53 PM 226.7 16.1
5/23/2019 4:05:54 PM 226.5 15.9
5/23/2019 4:05:55 PM 226.3 15.7
5/23/2019 4:05:56 PM 226.1 15.5
5/23/2019 4:05:57 PM 225.9 15.3
5/23/2019 4:05:58 PM 225.7 15.1
5/23/2019 4:05:59 PM 225.5 14.9
5/23/2019 4:06:00 PM 225.3 14.7
5/23/2019 4:06:01 PM 225.1 14.5
5/23/2019 4:06:02 PM 224.9 14.3
5/23/2019 4:06:03 PM 224.7 14.1
5/23/2019 4:06:04 PM 224.5 13.9
5/23/2019 4:06:05 PM 224.3 13.7
5/23/2019 4:06:06 PM 224.2 13.6
5/23/2019 4:06:07 PM 224.0 13.4
5/23/2019 4:06:08 PM 223.8 13.2
5/23/2019 4:06:09 PM 223.7 13.1
5/23/2019 4:06:10 PM 223.5 12.9
5/23/2019 4:06:11 PM 223.3 12.7
5/23/2019 4:06:12 PM 223.1 12.5
5/23/2019 4:06:13 PM 222.9 12.3
5/23/2019 4:06:14 PM 222.7 12.1
5/23/2019 4:06:15 PM 222.6 12.0
5/23/2019 4:06:16 PM 222.4 11.8
5/23/2019 4:06:17 PM 222.2 11.6
5/23/2019 4:06:18 PM 222.0 11.4
5/23/2019 4:06:19 PM 221.9 11.3
5/23/2019 4:06:20 PM 221.7 11.1
5/23/2019 4:06:21 PM 221.5 10.9
5/23/2019 4:06:22 PM 221.3 10.7
Page 134 of 452 August 2019
APPENDIX E30: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-4 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-4 Data Log
5/23/2019 4:06:23 PM 221.1 10.5
5/23/2019 4:06:24 PM 220.9 10.3
5/23/2019 4:06:25 PM 220.8 10.2
5/23/2019 4:06:26 PM 220.6 10.0
5/23/2019 4:06:27 PM 220.4 9.8
5/23/2019 4:06:28 PM 220.3 9.7
5/23/2019 4:06:29 PM 220.1 9.5
5/23/2019 4:06:30 PM 220.0 9.4
5/23/2019 4:06:31 PM 219.8 9.2
5/23/2019 4:06:32 PM 219.7 9.1
5/23/2019 4:06:33 PM 219.6 9.0
5/23/2019 4:06:34 PM 219.5 8.9
5/23/2019 4:06:35 PM 219.4 8.8
5/23/2019 4:06:36 PM 219.4 8.8
5/23/2019 4:06:37 PM 219.3 8.7
5/23/2019 4:06:38 PM 219.2 8.6
5/23/2019 4:06:39 PM 219.1 8.5
5/23/2019 4:06:40 PM 219.0 8.4
5/23/2019 4:06:41 PM 219.0 8.4
5/23/2019 4:06:42 PM 218.9 8.3
5/23/2019 4:06:43 PM 218.7 8.1
5/23/2019 4:06:44 PM 218.6 8.0
5/23/2019 4:06:45 PM 218.5 7.9
5/23/2019 4:06:46 PM 218.4 7.8
5/23/2019 4:06:47 PM 218.3 7.7
5/23/2019 4:06:48 PM 218.2 7.6
5/23/2019 4:06:49 PM 218.1 7.5
5/23/2019 4:06:50 PM 218.0 7.4
5/23/2019 4:06:51 PM 217.9 7.3
5/23/2019 4:06:52 PM 217.8 7.2
5/23/2019 4:06:53 PM 217.7 7.1
5/23/2019 4:06:54 PM 217.6 7.0
5/23/2019 4:06:55 PM 217.5 6.9
5/23/2019 4:06:56 PM 217.5 6.9
5/23/2019 4:06:57 PM 217.4 6.8
5/23/2019 4:06:58 PM 217.3 6.7
5/23/2019 4:06:59 PM 217.2 6.6
5/23/2019 4:07:00 PM 217.1 6.5
5/23/2019 4:07:01 PM 217.0 6.4
5/23/2019 4:07:02 PM 217.0 6.4
5/23/2019 4:07:03 PM 216.9 6.3
5/23/2019 4:07:04 PM 216.8 6.2
5/23/2019 4:07:05 PM 216.7 6.1
5/23/2019 4:07:06 PM 216.7 6.1
5/23/2019 4:07:07 PM 216.6 6.0
5/23/2019 4:07:08 PM 216.5 5.9
5/23/2019 4:07:09 PM 216.5 5.9
5/23/2019 4:07:10 PM 216.4 5.8
5/23/2019 4:07:11 PM 216.3 5.7
5/23/2019 4:07:12 PM 216.2 5.6
5/23/2019 4:07:13 PM 216.1 5.5
5/23/2019 4:07:14 PM 216.0 5.4
5/23/2019 4:07:15 PM 216.0 5.4
5/23/2019 4:07:16 PM 215.9 5.3
5/23/2019 4:07:17 PM 215.8 5.2
5/23/2019 4:07:18 PM 215.7 5.1
5/23/2019 4:07:19 PM 215.7 5.1
5/23/2019 4:07:20 PM 215.6 5.0
5/23/2019 4:07:21 PM 215.5 4.9
5/23/2019 4:07:22 PM 215.4 4.8
5/23/2019 4:07:23 PM 215.4 4.8
5/23/2019 4:07:24 PM 215.3 4.7
5/23/2019 4:07:25 PM 215.3 4.7
5/23/2019 4:07:26 PM 215.2 4.6
5/23/2019 4:07:27 PM 215.2 4.6
5/23/2019 4:07:28 PM 215.1 4.5
5/23/2019 4:07:29 PM 215.0 4.4
5/23/2019 4:07:30 PM 215.0 4.4
5/23/2019 4:07:31 PM 214.9 4.3
5/23/2019 4:07:32 PM 214.8 4.2
5/23/2019 4:07:33 PM 214.8 4.2
5/23/2019 4:07:34 PM 214.7 4.1
5/23/2019 4:07:35 PM 214.6 4.0
5/23/2019 4:07:36 PM 214.5 3.9
5/23/2019 4:07:37 PM 214.5 3.9
5/23/2019 4:07:38 PM 214.4 3.8
5/23/2019 4:07:39 PM 214.3 3.7
5/23/2019 4:07:40 PM 214.3 3.7
5/23/2019 4:07:41 PM 214.2 3.6
Page 135 of 452 August 2019
APPENDIX E30: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-4 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-4 Data Log
5/23/2019 4:07:42 PM 214.2 3.6
5/23/2019 4:07:43 PM 214.1 3.5
5/23/2019 4:07:44 PM 214.1 3.5
5/23/2019 4:07:45 PM 214.0 3.4
5/23/2019 4:07:46 PM 214.0 3.4
5/23/2019 4:07:47 PM 213.9 3.3
5/23/2019 4:07:48 PM 213.9 3.3
5/23/2019 4:07:49 PM 213.8 3.2
5/23/2019 4:07:50 PM 213.8 3.2
5/23/2019 4:07:51 PM 213.8 3.2
5/23/2019 4:07:52 PM 213.7 3.1
5/23/2019 4:07:53 PM 213.7 3.1
5/23/2019 4:07:54 PM 213.6 3.0
5/23/2019 4:07:55 PM 213.6 3.0
5/23/2019 4:07:56 PM 213.5 2.9
5/23/2019 4:07:57 PM 213.5 2.9
5/23/2019 4:07:58 PM 213.4 2.8
5/23/2019 4:07:59 PM 213.4 2.8
5/23/2019 4:08:00 PM 213.3 2.7
5/23/2019 4:08:01 PM 213.3 2.7
5/23/2019 4:08:02 PM 213.3 2.7
Page 136 of 452 August 2019
APPENDIX E30: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-4 MAY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-A3 TEST-4 1504
SEEP-A3 TEST-4 1504
SEEP-A3 TEST-4 1505
SEEP-A3 TEST-4 1506
Location EC Reading
(µS/cms)
SEEP-A3 TEST-4 48.7
SEEP-A3 TEST-4 181
SEEP-A3 TEST-4 450
SEEP-A3 TEST-4 3,464
SEEP-A3 TEST-4 15,648
SEEP-A3 TEST-4 127,541
q 300,000 mg
K 1.2785 (µS/cms) / (mg/L)
(s) . (µS/cms)
Q 2.8 L/s
44.6 GPM
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)(°C)
Table E2 SEEP-A3 TEST-4 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Geo Mean 209.5 (µS/cms)
208.8 19.1
211.0 18.9
210.0 19
208.3 19
Average 209.5 (µS/cms)
Table E3 SEEP-A3 TEST-4 YSI Salt Dilution Calibration Data
Calibration Temperature
(mg/L)(°C)
Average (pre-test)210.6 (µS/cms)
Average (post-test)216.1 (µS/cms)
27.1
1,000 27.5
1 26.6
136,609.0 SUM:Δt(EC
t-ECbkg)
Calculated Flow Rate
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
10000 27.4
100,000 27.5
Table E4 SEEP-A3 TEST-4 Flow Calculation Summary
Mass of Salt injected
Slope of Calibration Curve
Integral of Conductivity Data
Curve
10 26.9
100
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 137 of 452 August 2019
APPENDIX E31: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 12:55:18 PM 214.4 -
6/7/2019 12:55:19 PM 210.8 -
6/7/2019 12:55:20 PM 209.6 -
6/7/2019 12:55:21 PM 208.5 -
6/7/2019 12:55:22 PM 207.9 -
6/7/2019 12:55:23 PM 207.4 -
6/7/2019 12:55:24 PM 207.1 -
6/7/2019 12:55:25 PM 206.7 -
6/7/2019 12:55:26 PM 206.3 -
6/7/2019 12:55:27 PM 206.2 -
6/7/2019 12:55:28 PM 205.9 -
6/7/2019 12:55:29 PM 205.8 -
6/7/2019 12:55:30 PM 205.6 -
6/7/2019 12:55:31 PM 204.8 -
6/7/2019 12:55:32 PM 204.4 -
6/7/2019 12:55:33 PM 204.2 -
6/7/2019 12:55:34 PM 204.0 -
6/7/2019 12:55:35 PM 204.0 -
6/7/2019 12:55:36 PM 203.9 -
6/7/2019 12:55:37 PM 203.8 -
6/7/2019 12:55:38 PM 203.8 -
6/7/2019 12:55:39 PM 203.7 -
6/7/2019 12:55:40 PM 203.7 -
6/7/2019 12:55:41 PM 203.6 -
6/7/2019 12:55:42 PM 203.6 -
6/7/2019 12:55:43 PM 203.6 -
6/7/2019 12:55:44 PM 261.4 57.3
6/7/2019 12:55:45 PM 475.9 271.9
6/7/2019 12:55:46 PM 2633.0 2428.9
6/7/2019 12:55:47 PM 4051.4 3847.3
6/7/2019 12:55:48 PM 6542.3 6338.2
6/7/2019 12:55:49 PM 9940.7 9736.7
6/7/2019 12:55:50 PM 10413.6 10209.5
6/7/2019 12:55:51 PM 10383.0 10179.0
6/7/2019 12:55:52 PM 9620.2 9416.1
6/7/2019 12:55:53 PM 9076.6 8872.5
6/7/2019 12:55:54 PM 7480.7 7276.6
6/7/2019 12:55:55 PM 6783.4 6579.3
6/7/2019 12:55:56 PM 5713.1 5509.1
6/7/2019 12:55:57 PM 4956.8 4752.7
6/7/2019 12:55:58 PM 4180.2 3976.2
6/7/2019 12:55:59 PM 3678.0 3473.9
6/7/2019 12:56:00 PM 3265.8 3061.7
6/7/2019 12:56:01 PM 2814.1 2610.0
6/7/2019 12:56:02 PM 2599.3 2395.3
6/7/2019 12:56:03 PM 2288.5 2084.4
6/7/2019 12:56:04 PM 2099.8 1895.8
6/7/2019 12:56:05 PM 2084.6 1880.5
6/7/2019 12:56:06 PM 1877.0 1672.9
6/7/2019 12:56:07 PM 1676.3 1472.2
6/7/2019 12:56:08 PM 1465.8 1261.8
6/7/2019 12:56:09 PM 1443.7 1239.6
6/7/2019 12:56:10 PM 1396.1 1192.1
6/7/2019 12:56:11 PM 1208.4 1004.3
6/7/2019 12:56:12 PM 998.4 794.3
6/7/2019 12:56:13 PM 933.9 729.8
6/7/2019 12:56:14 PM 934.2 730.2
6/7/2019 12:56:15 PM 927.1 723.0
6/7/2019 12:56:16 PM 754.9 550.8
6/7/2019 12:56:17 PM 751.2 547.2
6/7/2019 12:56:18 PM 671.2 467.1
6/7/2019 12:56:19 PM 675.3 471.2
6/7/2019 12:56:20 PM 668.3 464.2
6/7/2019 12:56:21 PM 666.1 462.1
6/7/2019 12:56:22 PM 527.1 323.0
6/7/2019 12:56:23 PM 538.2 334.2
6/7/2019 12:56:24 PM 523.3 319.2
6/7/2019 12:56:25 PM 524.3 320.2
6/7/2019 12:56:26 PM 525.3 321.2
6/7/2019 12:56:27 PM 456.9 252.9
Table E1 SEEP-A3 TEST-1 Data Log
Page 138 of 452 August 2019
APPENDIX E31: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-1 Data Log
6/7/2019 12:56:28 PM 430.6 226.5
6/7/2019 12:56:29 PM 430.4 226.4
6/7/2019 12:56:30 PM 413.9 209.8
6/7/2019 12:56:31 PM 400.6 196.5
6/7/2019 12:56:32 PM 398.0 193.9
6/7/2019 12:56:33 PM 389.9 185.9
6/7/2019 12:56:34 PM 382.3 178.2
6/7/2019 12:56:35 PM 376.8 172.8
6/7/2019 12:56:36 PM 371.5 167.4
6/7/2019 12:56:37 PM 367.5 163.4
6/7/2019 12:56:38 PM 310.8 106.7
6/7/2019 12:56:39 PM 336.1 132.0
6/7/2019 12:56:40 PM 310.8 106.8
6/7/2019 12:56:41 PM 303.2 99.1
6/7/2019 12:56:42 PM 298.3 94.3
6/7/2019 12:56:43 PM 291.9 87.8
6/7/2019 12:56:44 PM 292.0 87.9
6/7/2019 12:56:45 PM 292.4 88.3
6/7/2019 12:56:46 PM 292.1 88.1
6/7/2019 12:56:47 PM 291.4 87.3
6/7/2019 12:56:48 PM 288.6 84.6
6/7/2019 12:56:49 PM 286.2 82.1
6/7/2019 12:56:50 PM 283.9 79.8
6/7/2019 12:56:51 PM 281.6 77.5
6/7/2019 12:56:52 PM 279.4 75.4
6/7/2019 12:56:53 PM 277.9 73.8
6/7/2019 12:56:54 PM 275.4 71.4
6/7/2019 12:56:55 PM 272.8 68.7
6/7/2019 12:56:56 PM 270.0 65.9
6/7/2019 12:56:57 PM 266.1 62.0
6/7/2019 12:56:58 PM 263.2 59.1
6/7/2019 12:56:59 PM 259.8 55.8
6/7/2019 12:57:00 PM 256.0 51.9
6/7/2019 12:57:01 PM 254.1 50.1
6/7/2019 12:57:02 PM 253.0 48.9
6/7/2019 12:57:03 PM 251.3 47.2
6/7/2019 12:57:04 PM 248.8 44.7
6/7/2019 12:57:05 PM 247.9 43.9
6/7/2019 12:57:06 PM 245.7 41.6
6/7/2019 12:57:07 PM 245.1 41.1
6/7/2019 12:57:08 PM 242.5 38.4
6/7/2019 12:57:09 PM 241.1 37.0
6/7/2019 12:57:10 PM 240.1 36.0
6/7/2019 12:57:11 PM 238.8 34.8
6/7/2019 12:57:12 PM 238.4 34.3
6/7/2019 12:57:13 PM 238.3 34.3
6/7/2019 12:57:14 PM 237.6 33.5
6/7/2019 12:57:15 PM 236.5 32.4
6/7/2019 12:57:16 PM 235.9 31.8
6/7/2019 12:57:17 PM 235.1 31.0
6/7/2019 12:57:18 PM 234.3 30.3
6/7/2019 12:57:19 PM 233.6 29.5
6/7/2019 12:57:20 PM 232.4 28.4
6/7/2019 12:57:21 PM 231.2 27.1
6/7/2019 12:57:22 PM 230.4 26.3
6/7/2019 12:57:23 PM 229.9 25.8
6/7/2019 12:57:24 PM 229.4 25.4
6/7/2019 12:57:25 PM 228.4 24.3
6/7/2019 12:57:26 PM 226.8 22.8
6/7/2019 12:57:27 PM 225.4 21.3
6/7/2019 12:57:28 PM 224.5 20.4
6/7/2019 12:57:29 PM 223.2 19.1
6/7/2019 12:57:30 PM 222.6 18.6
6/7/2019 12:57:31 PM 221.8 17.7
6/7/2019 12:57:32 PM 221.2 17.2
6/7/2019 12:57:33 PM 220.9 16.8
6/7/2019 12:57:34 PM 220.5 16.4
6/7/2019 12:57:35 PM 220.1 16.0
6/7/2019 12:57:36 PM 219.6 15.6
6/7/2019 12:57:37 PM 218.9 14.8
6/7/2019 12:57:38 PM 218.7 14.6
6/7/2019 12:57:39 PM 218.2 14.2
6/7/2019 12:57:40 PM 217.8 13.7
6/7/2019 12:57:41 PM 217.4 13.3
6/7/2019 12:57:42 PM 217.4 13.3
6/7/2019 12:57:43 PM 217.0 13.0
6/7/2019 12:57:44 PM 216.7 12.6
Page 139 of 452 August 2019
APPENDIX E31: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-1 Data Log
6/7/2019 12:57:45 PM 216.4 12.4
6/7/2019 12:57:46 PM 216.1 12.0
6/7/2019 12:57:47 PM 215.7 11.6
6/7/2019 12:57:48 PM 215.6 11.5
6/7/2019 12:57:49 PM 215.4 11.4
6/7/2019 12:57:50 PM 215.2 11.1
6/7/2019 12:57:51 PM 214.9 10.9
6/7/2019 12:57:52 PM 214.6 10.5
6/7/2019 12:57:53 PM 214.6 10.5
6/7/2019 12:57:54 PM 214.4 10.3
6/7/2019 12:57:55 PM 214.2 10.2
6/7/2019 12:57:56 PM 213.8 9.7
6/7/2019 12:57:57 PM 213.6 9.6
6/7/2019 12:57:58 PM 213.5 9.4
6/7/2019 12:57:59 PM 213.2 9.1
6/7/2019 12:58:00 PM 213.2 9.1
6/7/2019 12:58:01 PM 213.0 8.9
6/7/2019 12:58:02 PM 212.9 8.9
6/7/2019 12:58:03 PM 212.7 8.6
6/7/2019 12:58:04 PM 212.7 8.7
6/7/2019 12:58:05 PM 212.7 8.6
6/7/2019 12:58:06 PM 212.6 8.5
6/7/2019 12:58:07 PM 212.5 8.4
6/7/2019 12:58:08 PM 212.4 8.4
6/7/2019 12:58:09 PM 212.4 8.3
6/7/2019 12:58:10 PM 212.3 8.3
6/7/2019 12:58:11 PM 212.1 8.0
6/7/2019 12:58:12 PM 212.0 7.9
6/7/2019 12:58:13 PM 211.8 7.7
6/7/2019 12:58:14 PM 211.7 7.7
6/7/2019 12:58:15 PM 211.6 7.5
6/7/2019 12:58:16 PM 211.3 7.3
6/7/2019 12:58:17 PM 211.2 7.1
6/7/2019 12:58:18 PM 211.0 6.9
6/7/2019 12:58:19 PM 210.9 6.8
6/7/2019 12:58:20 PM 210.7 6.6
6/7/2019 12:58:21 PM 210.6 6.6
6/7/2019 12:58:22 PM 210.3 6.2
6/7/2019 12:58:23 PM 210.2 6.2
6/7/2019 12:58:24 PM 210.2 6.1
6/7/2019 12:58:25 PM 210.2 6.1
6/7/2019 12:58:26 PM 210.1 6.0
6/7/2019 12:58:27 PM 210.1 6.1
6/7/2019 12:58:28 PM 210.0 5.9
6/7/2019 12:58:29 PM 210.0 6.0
6/7/2019 12:58:30 PM 209.9 5.8
6/7/2019 12:58:31 PM 209.8 5.7
6/7/2019 12:58:32 PM 209.7 5.6
6/7/2019 12:58:33 PM 209.6 5.6
6/7/2019 12:58:34 PM 209.6 5.5
6/7/2019 12:58:35 PM 209.6 5.6
6/7/2019 12:58:36 PM 209.5 5.4
6/7/2019 12:58:37 PM 209.5 5.4
6/7/2019 12:58:38 PM 209.4 5.3
6/7/2019 12:58:39 PM 209.3 5.2
6/7/2019 12:58:40 PM 209.2 5.2
6/7/2019 12:58:41 PM 209.1 5.0
6/7/2019 12:58:42 PM 209.1 5.1
6/7/2019 12:58:43 PM 209.0 4.9
6/7/2019 12:58:44 PM 209.0 4.9
6/7/2019 12:58:45 PM 209.0 4.9
6/7/2019 12:58:46 PM 209.1 5.1
6/7/2019 12:58:47 PM 209.0 4.9
6/7/2019 12:58:48 PM 209.0 5.0
6/7/2019 12:58:49 PM 209.0 4.9
6/7/2019 12:58:50 PM 208.9 4.8
6/7/2019 12:58:51 PM 208.8 4.7
6/7/2019 12:58:52 PM 208.8 4.8
6/7/2019 12:58:53 PM 208.8 4.7
6/7/2019 12:58:54 PM 208.8 4.8
6/7/2019 12:58:55 PM 208.7 4.6
6/7/2019 12:58:56 PM 208.6 4.5
6/7/2019 12:58:57 PM 208.6 4.5
6/7/2019 12:58:58 PM 208.5 4.5
6/7/2019 12:58:59 PM 208.5 4.4
6/7/2019 12:59:00 PM 208.4 4.3
6/7/2019 12:59:01 PM 208.3 4.3
6/7/2019 12:59:02 PM 208.3 4.2
6/7/2019 12:59:03 PM 208.1 4.0
Page 140 of 452 August 2019
APPENDIX E31: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-1 Data Log
6/7/2019 12:59:04 PM 207.9 3.8
6/7/2019 12:59:05 PM 207.9 3.9
6/7/2019 12:59:06 PM 207.8 3.7
6/7/2019 12:59:07 PM 207.7 3.7
6/7/2019 12:59:08 PM 207.6 3.5
6/7/2019 12:59:09 PM 207.5 3.4
6/7/2019 12:59:10 PM 207.4 3.3
6/7/2019 12:59:11 PM 207.3 3.3
6/7/2019 12:59:12 PM 207.1 3.0
6/7/2019 12:59:13 PM 207.1 3.1
6/7/2019 12:59:14 PM 207.0 2.9
6/7/2019 12:59:15 PM 206.9 2.8
6/7/2019 12:59:16 PM 206.9 2.8
6/7/2019 12:59:17 PM 206.9 2.9
6/7/2019 12:59:18 PM 206.9 2.8
6/7/2019 12:59:19 PM 206.9 2.9
6/7/2019 12:59:20 PM 206.9 2.8
6/7/2019 12:59:21 PM 206.8 2.7
6/7/2019 12:59:22 PM 206.8 2.7
6/7/2019 12:59:23 PM 206.8 2.7
6/7/2019 12:59:24 PM 206.8 2.8
6/7/2019 12:59:25 PM 206.8 2.7
6/7/2019 12:59:26 PM 206.8 2.8
6/7/2019 12:59:27 PM 206.8 2.7
6/7/2019 12:59:28 PM 206.8 2.7
6/7/2019 12:59:29 PM 206.7 2.6
6/7/2019 12:59:30 PM 206.8 2.8
6/7/2019 12:59:31 PM 206.8 2.7
6/7/2019 12:59:32 PM 206.7 2.7
6/7/2019 12:59:33 PM 206.7 2.6
6/7/2019 12:59:34 PM 206.7 2.6
6/7/2019 12:59:35 PM 206.7 2.6
6/7/2019 12:59:36 PM 206.7 2.7
6/7/2019 12:59:37 PM 206.6 2.5
6/7/2019 12:59:38 PM 206.6 2.6
6/7/2019 12:59:39 PM 206.6 2.5
6/7/2019 12:59:40 PM 206.5 2.4
6/7/2019 12:59:41 PM 206.4 2.3
6/7/2019 12:59:42 PM 206.4 2.3
6/7/2019 12:59:43 PM 206.4 2.4
6/7/2019 12:59:44 PM 206.4 2.3
6/7/2019 12:59:45 PM 206.3 2.3
6/7/2019 12:59:46 PM 206.4 2.3
6/7/2019 12:59:47 PM 206.4 2.3
6/7/2019 12:59:48 PM 206.4 2.3
6/7/2019 12:59:49 PM 206.4 2.4
6/7/2019 12:59:50 PM 206.4 2.3
6/7/2019 12:59:51 PM 206.4 2.4
6/7/2019 12:59:52 PM 206.4 2.3
6/7/2019 12:59:53 PM 206.5 2.4
6/7/2019 12:59:54 PM 206.5 2.4
6/7/2019 12:59:55 PM 206.5 2.5
6/7/2019 12:59:56 PM 206.5 2.4
6/7/2019 12:59:57 PM 206.4 2.4
6/7/2019 12:59:58 PM 206.4 2.3
6/7/2019 12:59:59 PM 206.4 2.3
6/7/2019 1:00:00 PM 206.3 2.2
6/7/2019 1:00:01 PM 206.2 2.1
6/7/2019 1:00:02 PM 206.2 2.2
6/7/2019 1:00:03 PM 206.2 2.1
6/7/2019 1:00:04 PM 206.2 2.2
6/7/2019 1:00:05 PM 206.2 2.1
6/7/2019 1:00:06 PM 206.1 2.0
6/7/2019 1:00:07 PM 206.1 2.0
6/7/2019 1:00:08 PM 206.1 2.1
6/7/2019 1:00:09 PM 206.1 2.0
6/7/2019 1:00:10 PM 206.1 2.1
6/7/2019 1:00:11 PM 206.1 2.0
6/7/2019 1:00:12 PM 206.1 2.0
6/7/2019 1:00:13 PM 206.2 2.1
6/7/2019 1:00:14 PM 206.2 2.2
Page 141 of 452 August 2019
APPENDIX E31: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-A3 TEST-1 1240
SEEP-A3 TEST-1 1241
SEEP-A3 TEST-1 1243
SEEP-A3 TEST-1 1245
Location EC Reading
(µS/cms)
SEEP-A3 TEST-1 245
SEEP-A3 TEST-1 2,128
SEEP-A3 TEST-1 17,684
SEEP-A3 TEST-1 128,985
q 299,900
K 1.2947
3.0
48.1
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)(°C)
Table E2 SEEP-A3 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Geo Mean 200.1 (µS/cms)
198.1 18.6
198.4 18.6
202.4 18.6
201.4 18.6
Average 200.1 (µS/cms)
100 24.4
Average (pre-test)204.1 (µS/cms)
Average (post-test)207.5 (µS/cms)
Table E3 SEEP-A3 TEST-1 YSI Salt Dilution Calibration Data
Calibration
Concentration Temperature
(mg/L)(°C)
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement
Part 2: Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol.
8, no. 1, 2004, pp. 11–15.
Integral of Conductivity Data Curve SUM:Δt(EC
t-ECbkg)128,243.4 (s) . (µS/cms)
Calculated Flow Rate Q L/s
GPM
1,000 24.3
10000 24.2
100,000 24.2
Table E4 SEEP-A3 TEST-1 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 142 of 452 August 2019
APPENDIX E32: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 1:07:29 PM 211.5 -
6/7/2019 1:07:30 PM 211.5 -
6/7/2019 1:07:31 PM 211.5 -
6/7/2019 1:07:32 PM 211.5 -
6/7/2019 1:07:33 PM 211.5 -
6/7/2019 1:07:34 PM 211.3 -
6/7/2019 1:07:35 PM 211.2 -
6/7/2019 1:07:36 PM 210.9 -
6/7/2019 1:07:37 PM 210.7 -
6/7/2019 1:07:38 PM 210.5 -
6/7/2019 1:07:39 PM 210.3 -
6/7/2019 1:07:40 PM 210.1 -
6/7/2019 1:07:41 PM 209.9 -
6/7/2019 1:07:42 PM 209.7 -
6/7/2019 1:07:43 PM 209.6 -
6/7/2019 1:07:44 PM 209.3 -
6/7/2019 1:07:45 PM 209.2 -
6/7/2019 1:07:46 PM 209.0 -
6/7/2019 1:07:47 PM 208.8 -
6/7/2019 1:07:48 PM 208.6 -
6/7/2019 1:07:49 PM 208.5 -
6/7/2019 1:07:50 PM 208.3 -
6/7/2019 1:07:51 PM 208.1 -
6/7/2019 1:07:52 PM 208.8 -
6/7/2019 1:07:53 PM 732.4 523.4
6/7/2019 1:07:54 PM 3735.8 3526.8
6/7/2019 1:07:55 PM 6061.3 5852.3
6/7/2019 1:07:56 PM 7535.7 7326.7
6/7/2019 1:07:57 PM 8721.8 8512.8
6/7/2019 1:07:58 PM 9028.9 8819.9
6/7/2019 1:07:59 PM 8997.2 8788.2
6/7/2019 1:08:00 PM 8849.9 8640.9
6/7/2019 1:08:01 PM 7387.3 7178.3
6/7/2019 1:08:02 PM 7034.6 6825.6
6/7/2019 1:08:03 PM 5752.9 5543.9
6/7/2019 1:08:04 PM 5409.6 5200.6
6/7/2019 1:08:05 PM 4702.6 4493.6
6/7/2019 1:08:06 PM 4264.2 4055.2
6/7/2019 1:08:07 PM 3739.2 3530.2
6/7/2019 1:08:08 PM 3403.0 3194.0
6/7/2019 1:08:09 PM 3004.4 2795.4
6/7/2019 1:08:10 PM 2816.0 2607.0
6/7/2019 1:08:11 PM 2608.5 2399.5
6/7/2019 1:08:12 PM 2269.7 2060.7
6/7/2019 1:08:13 PM 1989.9 1780.9
6/7/2019 1:08:14 PM 1846.5 1637.5
6/7/2019 1:08:15 PM 1770.7 1561.7
6/7/2019 1:08:16 PM 1551.6 1342.6
6/7/2019 1:08:17 PM 1418.1 1209.1
6/7/2019 1:08:18 PM 1290.8 1081.8
6/7/2019 1:08:19 PM 1154.1 945.1
6/7/2019 1:08:20 PM 1109.0 900.0
6/7/2019 1:08:21 PM 1027.8 818.8
6/7/2019 1:08:22 PM 965.1 756.1
6/7/2019 1:08:23 PM 959.3 750.3
6/7/2019 1:08:24 PM 839.3 630.3
6/7/2019 1:08:25 PM 801.5 592.5
6/7/2019 1:08:26 PM 730.6 521.6
6/7/2019 1:08:27 PM 716.9 507.9
6/7/2019 1:08:28 PM 697.9 488.9
6/7/2019 1:08:29 PM 649.2 440.2
6/7/2019 1:08:30 PM 640.6 431.6
6/7/2019 1:08:31 PM 562.5 353.5
6/7/2019 1:08:32 PM 564.5 355.5
6/7/2019 1:08:33 PM 561.2 352.2
6/7/2019 1:08:34 PM 543.8 334.8
6/7/2019 1:08:35 PM 527.5 318.5
6/7/2019 1:08:36 PM 517.8 308.8
6/7/2019 1:08:37 PM 509.2 300.2
6/7/2019 1:08:38 PM 457.1 248.1
Table E1 SEEP-A3 TEST-2 Data Log
Page 143 of 452 August 2019
APPENDIX E32: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-2 Data Log
6/7/2019 1:08:39 PM 433.1 224.1
6/7/2019 1:08:40 PM 424.7 215.7
6/7/2019 1:08:41 PM 419.5 210.5
6/7/2019 1:08:42 PM 411.5 202.5
6/7/2019 1:08:43 PM 401.9 192.9
6/7/2019 1:08:44 PM 397.8 188.8
6/7/2019 1:08:45 PM 393.1 184.1
6/7/2019 1:08:46 PM 389.3 180.3
6/7/2019 1:08:47 PM 385.6 176.6
6/7/2019 1:08:48 PM 383.8 174.8
6/7/2019 1:08:49 PM 381.8 172.8
6/7/2019 1:08:50 PM 379.9 170.9
6/7/2019 1:08:51 PM 376.8 167.8
6/7/2019 1:08:52 PM 374.0 165.0
6/7/2019 1:08:53 PM 370.7 161.7
6/7/2019 1:08:54 PM 324.6 115.6
6/7/2019 1:08:55 PM 320.8 111.8
6/7/2019 1:08:56 PM 315.3 106.3
6/7/2019 1:08:57 PM 312.4 103.4
6/7/2019 1:08:58 PM 311.6 102.6
6/7/2019 1:08:59 PM 310.2 101.2
6/7/2019 1:09:00 PM 308.9 99.9
6/7/2019 1:09:01 PM 307.6 98.6
6/7/2019 1:09:02 PM 305.8 96.8
6/7/2019 1:09:03 PM 304.2 95.2
6/7/2019 1:09:04 PM 302.6 93.6
6/7/2019 1:09:05 PM 301.4 92.4
6/7/2019 1:09:06 PM 300.2 91.2
6/7/2019 1:09:07 PM 298.8 89.8
6/7/2019 1:09:08 PM 296.5 87.5
6/7/2019 1:09:09 PM 295.4 86.4
6/7/2019 1:09:10 PM 293.7 84.7
6/7/2019 1:09:11 PM 291.0 82.0
6/7/2019 1:09:12 PM 287.9 78.9
6/7/2019 1:09:13 PM 284.8 75.8
6/7/2019 1:09:14 PM 282.3 73.3
6/7/2019 1:09:15 PM 279.6 70.6
6/7/2019 1:09:16 PM 277.5 68.5
6/7/2019 1:09:17 PM 275.0 66.0
6/7/2019 1:09:18 PM 272.6 63.6
6/7/2019 1:09:19 PM 270.0 61.0
6/7/2019 1:09:20 PM 268.1 59.1
6/7/2019 1:09:21 PM 266.2 57.2
6/7/2019 1:09:22 PM 264.6 55.6
6/7/2019 1:09:23 PM 262.8 53.8
6/7/2019 1:09:24 PM 261.3 52.3
6/7/2019 1:09:25 PM 260.0 51.0
6/7/2019 1:09:26 PM 259.0 50.0
6/7/2019 1:09:27 PM 257.8 48.8
6/7/2019 1:09:28 PM 256.6 47.6
6/7/2019 1:09:29 PM 255.2 46.2
6/7/2019 1:09:30 PM 254.3 45.3
6/7/2019 1:09:31 PM 253.0 44.0
6/7/2019 1:09:32 PM 251.6 42.6
6/7/2019 1:09:33 PM 250.2 41.2
6/7/2019 1:09:34 PM 248.7 39.7
6/7/2019 1:09:35 PM 247.3 38.3
6/7/2019 1:09:36 PM 245.6 36.6
6/7/2019 1:09:37 PM 244.2 35.2
6/7/2019 1:09:38 PM 242.6 33.6
6/7/2019 1:09:39 PM 241.2 32.2
6/7/2019 1:09:40 PM 239.6 30.6
6/7/2019 1:09:41 PM 238.4 29.4
6/7/2019 1:09:42 PM 237.1 28.1
6/7/2019 1:09:43 PM 235.7 26.7
6/7/2019 1:09:44 PM 234.5 25.5
6/7/2019 1:09:45 PM 233.7 24.7
6/7/2019 1:09:46 PM 232.9 23.9
6/7/2019 1:09:47 PM 232.3 23.3
6/7/2019 1:09:48 PM 231.7 22.7
6/7/2019 1:09:49 PM 231.3 22.3
6/7/2019 1:09:50 PM 230.7 21.7
6/7/2019 1:09:51 PM 230.0 21.0
6/7/2019 1:09:52 PM 229.4 20.4
6/7/2019 1:09:53 PM 228.7 19.7
6/7/2019 1:09:54 PM 228.1 19.1
6/7/2019 1:09:55 PM 227.5 18.5
Page 144 of 452 August 2019
APPENDIX E32: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-2 Data Log
6/7/2019 1:09:56 PM 227.1 18.1
6/7/2019 1:09:57 PM 226.7 17.7
6/7/2019 1:09:58 PM 226.3 17.3
6/7/2019 1:09:59 PM 225.8 16.8
6/7/2019 1:10:00 PM 225.4 16.4
6/7/2019 1:10:01 PM 225.0 16.0
6/7/2019 1:10:02 PM 224.7 15.7
6/7/2019 1:10:03 PM 224.2 15.2
6/7/2019 1:10:04 PM 223.9 14.9
6/7/2019 1:10:05 PM 223.6 14.6
6/7/2019 1:10:06 PM 223.2 14.2
6/7/2019 1:10:07 PM 222.7 13.7
6/7/2019 1:10:08 PM 222.3 13.3
6/7/2019 1:10:09 PM 222.0 13.0
6/7/2019 1:10:10 PM 221.7 12.7
6/7/2019 1:10:11 PM 221.3 12.3
6/7/2019 1:10:12 PM 221.1 12.1
6/7/2019 1:10:13 PM 220.7 11.7
6/7/2019 1:10:14 PM 220.3 11.3
6/7/2019 1:10:15 PM 219.9 10.9
6/7/2019 1:10:16 PM 219.5 10.5
6/7/2019 1:10:17 PM 219.1 10.1
6/7/2019 1:10:18 PM 218.7 9.7
6/7/2019 1:10:19 PM 218.4 9.4
6/7/2019 1:10:20 PM 218.2 9.2
6/7/2019 1:10:21 PM 217.9 8.9
6/7/2019 1:10:22 PM 217.6 8.6
6/7/2019 1:10:23 PM 217.5 8.5
6/7/2019 1:10:24 PM 217.2 8.2
6/7/2019 1:10:25 PM 216.9 7.9
6/7/2019 1:10:26 PM 216.6 7.6
6/7/2019 1:10:27 PM 216.4 7.4
6/7/2019 1:10:28 PM 216.1 7.1
6/7/2019 1:10:29 PM 216.0 7.0
6/7/2019 1:10:30 PM 215.9 6.9
6/7/2019 1:10:31 PM 215.6 6.6
6/7/2019 1:10:32 PM 215.5 6.5
6/7/2019 1:10:33 PM 215.2 6.2
6/7/2019 1:10:34 PM 215.1 6.1
6/7/2019 1:10:35 PM 214.9 5.9
6/7/2019 1:10:36 PM 214.6 5.6
6/7/2019 1:10:37 PM 214.4 5.4
6/7/2019 1:10:38 PM 214.3 5.3
6/7/2019 1:10:39 PM 214.1 5.1
6/7/2019 1:10:40 PM 214.0 5.0
6/7/2019 1:10:41 PM 213.7 4.7
6/7/2019 1:10:42 PM 213.6 4.6
6/7/2019 1:10:43 PM 213.3 4.3
6/7/2019 1:10:44 PM 213.0 4.0
6/7/2019 1:10:45 PM 212.7 3.7
6/7/2019 1:10:46 PM 212.4 3.4
6/7/2019 1:10:47 PM 212.1 3.1
6/7/2019 1:10:48 PM 211.9 2.9
6/7/2019 1:10:49 PM 211.6 2.6
6/7/2019 1:10:50 PM 211.3 2.3
6/7/2019 1:10:51 PM 211.0 2.0
6/7/2019 1:10:52 PM 210.8 1.8
6/7/2019 1:10:53 PM 210.7 1.7
6/7/2019 1:10:54 PM 210.6 1.6
6/7/2019 1:10:55 PM 210.5 1.5
6/7/2019 1:10:56 PM 210.4 1.4
6/7/2019 1:10:57 PM 210.4 1.4
6/7/2019 1:10:58 PM 210.5 1.5
6/7/2019 1:10:59 PM 210.5 1.5
6/7/2019 1:11:00 PM 210.5 1.5
6/7/2019 1:11:01 PM 210.5 1.5
6/7/2019 1:11:02 PM 210.6 1.6
6/7/2019 1:11:03 PM 210.6 1.6
6/7/2019 1:11:04 PM 210.4 1.4
6/7/2019 1:11:05 PM 210.0 1.0
6/7/2019 1:11:06 PM 209.5 0.5
6/7/2019 1:11:07 PM 209.1 0.1
6/7/2019 1:11:08 PM 208.9 -0.1
6/7/2019 1:11:09 PM 208.4 -0.6
6/7/2019 1:11:10 PM 208.1 -0.9
6/7/2019 1:11:11 PM 207.4 -1.6
6/7/2019 1:11:12 PM 207.0 -2.0
6/7/2019 1:11:13 PM 206.2 -2.8
6/7/2019 1:11:14 PM 205.9 -3.1
Page 145 of 452 August 2019
APPENDIX E32: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-2 Data Log
6/7/2019 1:11:15 PM 205.3 -3.7
6/7/2019 1:11:16 PM 204.7 -4.3
6/7/2019 1:11:17 PM 204.3 -4.7
6/7/2019 1:11:18 PM 204.1 -4.9
6/7/2019 1:11:19 PM 203.8 -5.2
6/7/2019 1:11:20 PM 203.6 -5.4
6/7/2019 1:11:21 PM 203.3 -5.7
6/7/2019 1:11:22 PM 203.1 -5.9
6/7/2019 1:11:23 PM 203.0 -6.0
6/7/2019 1:11:24 PM 202.9 -6.1
6/7/2019 1:11:25 PM 202.8 -6.2
6/7/2019 1:11:26 PM 202.7 -6.3
6/7/2019 1:11:27 PM 202.6 -6.4
6/7/2019 1:11:28 PM 202.5 -6.5
6/7/2019 1:11:29 PM 202.4 -6.6
Page 146 of 452 August 2019
APPENDIX E32: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-A3 TEST-2 1240
SEEP-A3 TEST-2 1241
SEEP-A3 TEST-2 1243
SEEP-A3 TEST-2 1245
Location EC Reading
(µS/cms)
SEEP-A3 TEST-2 245
SEEP-A3 TEST-2 2,128
SEEP-A3 TEST-2 17,684
SEEP-A3 TEST-2 128,985
q 300,000
K 1.2947
3.0
48.3
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms) (°C)
Table E2 SEEP-A3 TEST-2 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Geo Mean 200.1 (µS/cms)
198.1 18.6
198.4 18.6
202.4 18.6
201.4 18.6
Average 200.1 (µS/cms)
100 24.4
Average (pre-test)209.0 (µS/cms)
Average (post-test)205.3 (µS/cms)
Table E3 SEEP-A3 TEST-2 YSI Salt Dilution Calibration Data
Calibration Temperature
(mg/L)(°C)
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)127,657.0 (s) . (µS/cms)
1,000 24.3
10000 24.2
100,000 24.2
Table E4 SEEP-A3 TEST-2 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Calculated Flow Rate Q
L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 147 of 452 August 2019
APPENDIX E33: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 1:15:19 PM 204.7 -
6/7/2019 1:15:20 PM 204.6 -
6/7/2019 1:15:21 PM 204.6 -
6/7/2019 1:15:22 PM 204.5 -
6/7/2019 1:15:23 PM 204.5 -
6/7/2019 1:15:24 PM 204.4 -
6/7/2019 1:15:25 PM 204.4 -
6/7/2019 1:15:26 PM 204.3 -
6/7/2019 1:15:27 PM 204.2 -
6/7/2019 1:15:28 PM 204.1 -
6/7/2019 1:15:29 PM 204.0 -
6/7/2019 1:15:30 PM 203.9 -
6/7/2019 1:15:31 PM 203.7 -
6/7/2019 1:15:32 PM 203.6 -
6/7/2019 1:15:33 PM 203.6 -
6/7/2019 1:15:34 PM 203.5 -
6/7/2019 1:15:35 PM 203.4 -
6/7/2019 1:15:36 PM 203.3 -
6/7/2019 1:15:37 PM 203.2 -
6/7/2019 1:15:38 PM 203.2 -
6/7/2019 1:15:39 PM 322.6 118.6
6/7/2019 1:15:40 PM 779.1 575.1
6/7/2019 1:15:41 PM 3104.0 2900.0
6/7/2019 1:15:42 PM 5397.8 5193.8
6/7/2019 1:15:43 PM 7238.7 7034.7
6/7/2019 1:15:44 PM 9225.7 9021.7
6/7/2019 1:15:45 PM 9880.8 9676.8
6/7/2019 1:15:46 PM 9904.9 9700.9
6/7/2019 1:15:47 PM 8647.4 8443.4
6/7/2019 1:15:48 PM 7547.1 7343.1
6/7/2019 1:15:49 PM 6550.3 6346.3
6/7/2019 1:15:50 PM 5891.1 5687.1
6/7/2019 1:15:51 PM 5198.0 4994.0
6/7/2019 1:15:52 PM 4523.8 4319.8
6/7/2019 1:15:53 PM 4033.9 3829.9
6/7/2019 1:15:54 PM 3692.1 3488.1
6/7/2019 1:15:55 PM 3104.0 2900.0
6/7/2019 1:15:56 PM 2777.9 2573.9
6/7/2019 1:15:57 PM 2570.5 2366.5
6/7/2019 1:15:58 PM 2454.1 2250.1
6/7/2019 1:15:59 PM 2207.0 2003.0
6/7/2019 1:16:00 PM 1945.3 1741.3
6/7/2019 1:16:01 PM 1785.7 1581.7
6/7/2019 1:16:02 PM 1520.1 1316.1
6/7/2019 1:16:03 PM 1423.0 1219.0
6/7/2019 1:16:04 PM 1274.5 1070.5
6/7/2019 1:16:05 PM 1243.6 1039.6
6/7/2019 1:16:06 PM 1070.2 866.2
6/7/2019 1:16:07 PM 1005.3 801.3
6/7/2019 1:16:08 PM 928.4 724.4
6/7/2019 1:16:09 PM 919.1 715.1
6/7/2019 1:16:10 PM 916.8 712.8
6/7/2019 1:16:11 PM 780.1 576.1
6/7/2019 1:16:12 PM 742.0 538.0
6/7/2019 1:16:13 PM 681.3 477.3
6/7/2019 1:16:14 PM 664.7 460.7
6/7/2019 1:16:15 PM 656.1 452.1
6/7/2019 1:16:16 PM 537.5 333.5
6/7/2019 1:16:17 PM 556.2 352.2
6/7/2019 1:16:18 PM 507.0 303.0
6/7/2019 1:16:19 PM 497.5 293.5
6/7/2019 1:16:20 PM 484.9 280.9
6/7/2019 1:16:21 PM 476.7 272.7
6/7/2019 1:16:22 PM 472.6 268.6
6/7/2019 1:16:23 PM 466.7 262.7
6/7/2019 1:16:24 PM 462.8 258.8
6/7/2019 1:16:25 PM 404.5 200.5
6/7/2019 1:16:26 PM 379.4 175.4
6/7/2019 1:16:27 PM 390.4 186.4
6/7/2019 1:16:28 PM 398.9 194.9
Table E1 SEEP-A3 TEST-3 Data Log
Page 148 of 452 August 2019
APPENDIX E33: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-3 Data Log
6/7/2019 1:16:29 PM 391.2 187.2
6/7/2019 1:16:30 PM 373.7 169.7
6/7/2019 1:16:31 PM 362.4 158.4
6/7/2019 1:16:32 PM 357.5 153.5
6/7/2019 1:16:33 PM 350.6 146.6
6/7/2019 1:16:34 PM 345.0 141.0
6/7/2019 1:16:35 PM 341.1 137.1
6/7/2019 1:16:36 PM 335.8 131.8
6/7/2019 1:16:37 PM 335.1 131.1
6/7/2019 1:16:38 PM 332.9 128.9
6/7/2019 1:16:39 PM 286.4 82.4
6/7/2019 1:16:40 PM 278.9 74.9
6/7/2019 1:16:41 PM 277.8 73.8
6/7/2019 1:16:42 PM 275.0 71.0
6/7/2019 1:16:43 PM 274.3 70.3
6/7/2019 1:16:44 PM 276.1 72.1
6/7/2019 1:16:45 PM 274.9 70.9
6/7/2019 1:16:46 PM 274.2 70.2
6/7/2019 1:16:47 PM 273.3 69.3
6/7/2019 1:16:48 PM 272.2 68.2
6/7/2019 1:16:49 PM 271.1 67.1
6/7/2019 1:16:50 PM 268.3 64.3
6/7/2019 1:16:51 PM 266.9 62.9
6/7/2019 1:16:52 PM 265.8 61.8
6/7/2019 1:16:53 PM 264.1 60.1
6/7/2019 1:16:54 PM 262.8 58.8
6/7/2019 1:16:55 PM 261.1 57.1
6/7/2019 1:16:56 PM 259.1 55.1
6/7/2019 1:16:57 PM 255.5 51.5
6/7/2019 1:16:58 PM 253.8 49.8
6/7/2019 1:16:59 PM 250.4 46.4
6/7/2019 1:17:00 PM 248.5 44.5
6/7/2019 1:17:01 PM 246.7 42.7
6/7/2019 1:17:02 PM 245.0 41.0
6/7/2019 1:17:03 PM 243.7 39.7
6/7/2019 1:17:04 PM 242.8 38.8
6/7/2019 1:17:05 PM 240.7 36.7
6/7/2019 1:17:06 PM 239.3 35.3
6/7/2019 1:17:07 PM 238.0 34.0
6/7/2019 1:17:08 PM 236.6 32.6
6/7/2019 1:17:09 PM 234.9 30.9
6/7/2019 1:17:10 PM 234.0 30.0
6/7/2019 1:17:11 PM 233.0 29.0
6/7/2019 1:17:12 PM 232.0 28.0
6/7/2019 1:17:13 PM 231.1 27.1
6/7/2019 1:17:14 PM 230.0 26.0
6/7/2019 1:17:15 PM 229.0 25.0
6/7/2019 1:17:16 PM 228.0 24.0
6/7/2019 1:17:17 PM 227.1 23.1
6/7/2019 1:17:18 PM 226.2 22.2
6/7/2019 1:17:19 PM 225.7 21.7
6/7/2019 1:17:20 PM 225.0 21.0
6/7/2019 1:17:21 PM 224.4 20.4
6/7/2019 1:17:22 PM 223.8 19.8
6/7/2019 1:17:23 PM 223.1 19.1
6/7/2019 1:17:24 PM 222.0 18.0
6/7/2019 1:17:25 PM 221.4 17.4
6/7/2019 1:17:26 PM 220.9 16.9
6/7/2019 1:17:27 PM 219.9 15.9
6/7/2019 1:17:28 PM 219.1 15.1
6/7/2019 1:17:29 PM 218.5 14.5
6/7/2019 1:17:30 PM 217.5 13.5
6/7/2019 1:17:31 PM 217.1 13.1
6/7/2019 1:17:32 PM 216.7 12.7
6/7/2019 1:17:33 PM 216.1 12.1
6/7/2019 1:17:34 PM 215.3 11.3
6/7/2019 1:17:35 PM 215.0 11.0
6/7/2019 1:17:36 PM 214.3 10.3
6/7/2019 1:17:37 PM 213.6 9.6
6/7/2019 1:17:38 PM 213.0 9.0
6/7/2019 1:17:39 PM 211.9 7.9
6/7/2019 1:17:40 PM 211.4 7.4
6/7/2019 1:17:41 PM 210.9 6.9
6/7/2019 1:17:42 PM 210.2 6.2
6/7/2019 1:17:43 PM 209.7 5.7
6/7/2019 1:17:44 PM 209.1 5.1
6/7/2019 1:17:45 PM 208.3 4.3
Page 149 of 452 August 2019
APPENDIX E33: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A3 TEST-3 Data Log
6/7/2019 1:17:46 PM 208.0 4.0
6/7/2019 1:17:47 PM 207.4 3.4
6/7/2019 1:17:48 PM 206.7 2.7
6/7/2019 1:17:49 PM 206.1 2.1
6/7/2019 1:17:50 PM 205.8 1.8
6/7/2019 1:17:51 PM 205.2 1.2
6/7/2019 1:17:52 PM 204.8 0.8
6/7/2019 1:17:53 PM 204.4 0.4
6/7/2019 1:17:54 PM 203.9 -0.1
6/7/2019 1:17:55 PM 203.5 -0.5
6/7/2019 1:17:56 PM 202.9 -1.1
6/7/2019 1:17:57 PM 202.3 -1.7
6/7/2019 1:17:58 PM 201.9 -2.1
6/7/2019 1:17:59 PM 201.5 -2.5
6/7/2019 1:18:00 PM 201.0 -3.0
6/7/2019 1:18:01 PM 200.7 -3.3
6/7/2019 1:18:02 PM 200.3 -3.7
6/7/2019 1:18:03 PM 200.0 -4.0
6/7/2019 1:18:04 PM 199.6 -4.4
6/7/2019 1:18:05 PM 199.2 -4.8
6/7/2019 1:18:06 PM 198.9 -5.1
6/7/2019 1:18:07 PM 198.7 -5.3
6/7/2019 1:18:08 PM 198.2 -5.8
6/7/2019 1:18:09 PM 197.8 -6.2
6/7/2019 1:18:10 PM 197.5 -6.5
6/7/2019 1:18:11 PM 197.3 -6.7
6/7/2019 1:18:12 PM 196.9 -7.1
6/7/2019 1:18:13 PM 196.7 -7.3
6/7/2019 1:18:14 PM 196.5 -7.5
Page 150 of 452 August 2019
APPENDIX E33: SALT DILUTION GAUGING SUMMARY
SEEP-A3 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-A3 TEST-3 1240
SEEP-A3 TEST-3 1241
SEEP-A3 TEST-3 1243
SEEP-A3 TEST-3 1245
Location EC Reading
(µS/cms)
SEEP-A3 TEST-3 245
SEEP-A3 TEST-3 2,128
SEEP-A3 TEST-3 17,684
SEEP-A3 TEST-3 128,985
q 300,500
K 1.2947
3.2
50.6
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)(°C)
Table E2 SEEP-A3 TEST-3 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Geo Mean 200.1 (µS/cms)
198.1 18.6
198.4 18.6
202.4 18.6
201.4 18.6
Average 200.1 (µS/cms)
100 24.4
Average (pre-test)204.0 (µS/cms)
Average (post-test)202.2 (µS/cms)
Table E3 SEEP-A3 TEST-3 YSI Salt Dilution Calibration Data
Calibration Temperature
(mg/L)(°C)
Integral of Conductivity
Data Curve
SUM:Δt(E
Ct-ECbkg)122,171.9 (s) . (µS/cms)
1,000 24.3
10000 24.2
100,000 24.2
Table E4 SEEP-A3 TEST-3 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Calculated Flow Rate Q
L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline,
Watershed Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 151 of 452 August 2019
APPENDIX E34: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 12:31:40 PM 108.6 -
6/7/2019 12:31:41 PM 108.6 -
6/7/2019 12:31:42 PM 108.5 -
6/7/2019 12:31:43 PM 108.5 -
6/7/2019 12:31:44 PM 108.5 -
6/7/2019 12:31:45 PM 108.5 -
6/7/2019 12:31:46 PM 108.5 -
6/7/2019 12:31:47 PM 108.4 -
6/7/2019 12:31:48 PM 108.4 -
6/7/2019 12:31:49 PM 108.4 -
6/7/2019 12:31:50 PM 108.4 -
6/7/2019 12:31:51 PM 108.4 -
6/7/2019 12:31:52 PM 108.3 -
6/7/2019 12:31:53 PM 108.3 -
6/7/2019 12:31:54 PM 108.3 -
6/7/2019 12:31:55 PM 108.3 -
6/7/2019 12:31:56 PM 108.3 -
6/7/2019 12:31:57 PM 108.3 -
6/7/2019 12:31:58 PM 108.3 -
6/7/2019 12:31:59 PM 108.3 -
6/7/2019 12:32:00 PM 108.3 -
6/7/2019 12:32:01 PM 108.7 -
6/7/2019 12:32:02 PM 571.9 463.5
6/7/2019 12:32:03 PM 4556.0 4447.6
6/7/2019 12:32:04 PM 6937.3 6828.9
6/7/2019 12:32:05 PM 24717.5 24609.1
6/7/2019 12:32:06 PM 31029.4 30921.0
6/7/2019 12:32:07 PM 39130.1 39021.7
6/7/2019 12:32:08 PM 41884.2 41775.8
6/7/2019 12:32:09 PM 42284.2 42175.8
6/7/2019 12:32:10 PM 41212.3 41103.9
6/7/2019 12:32:11 PM 37339.0 37230.6
6/7/2019 12:32:12 PM 33359.6 33251.2
6/7/2019 12:32:13 PM 29295.8 29187.4
6/7/2019 12:32:14 PM 27182.0 27073.6
6/7/2019 12:32:15 PM 21893.6 21785.2
6/7/2019 12:32:16 PM 18295.1 18186.7
6/7/2019 12:32:17 PM 15730.1 15621.7
6/7/2019 12:32:18 PM 13120.0 13011.6
6/7/2019 12:32:19 PM 11474.1 11365.7
6/7/2019 12:32:20 PM 9570.5 9462.1
6/7/2019 12:32:21 PM 8962.9 8854.5
6/7/2019 12:32:22 PM 7267.1 7158.7
6/7/2019 12:32:23 PM 6394.6 6286.2
6/7/2019 12:32:24 PM 5790.3 5681.9
6/7/2019 12:32:25 PM 5254.8 5146.4
6/7/2019 12:32:26 PM 4514.2 4405.8
6/7/2019 12:32:27 PM 4064.0 3955.6
6/7/2019 12:32:28 PM 3591.6 3483.2
6/7/2019 12:32:29 PM 3429.2 3320.8
6/7/2019 12:32:30 PM 3017.4 2909.0
6/7/2019 12:32:31 PM 2736.0 2627.6
6/7/2019 12:32:32 PM 2506.0 2397.6
6/7/2019 12:32:33 PM 2435.5 2327.1
6/7/2019 12:32:34 PM 2162.3 2053.9
6/7/2019 12:32:35 PM 2032.7 1924.3
6/7/2019 12:32:36 PM 1856.8 1748.4
6/7/2019 12:32:37 PM 1816.6 1708.2
6/7/2019 12:32:38 PM 1755.6 1647.2
6/7/2019 12:32:39 PM 1566.6 1458.2
6/7/2019 12:32:40 PM 1499.8 1391.4
6/7/2019 12:32:41 PM 1419.7 1311.3
6/7/2019 12:32:42 PM 1399.5 1291.1
6/7/2019 12:32:43 PM 1356.7 1248.3
6/7/2019 12:32:44 PM 1255.5 1147.1
6/7/2019 12:32:45 PM 1243.5 1135.1
6/7/2019 12:32:46 PM 1246.2 1137.8
6/7/2019 12:32:47 PM 1242.9 1134.5
6/7/2019 12:32:48 PM 1243.3 1134.9
6/7/2019 12:32:49 PM 1222.5 1114.1
Table E1 SEEP-A4 TEST-1 Data Log
Page 152 of 452 August 2019
APPENDIX E34: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A4 TEST-1 Data Log
6/7/2019 12:32:50 PM 1206.1 1097.7
6/7/2019 12:32:51 PM 1099.1 990.7
6/7/2019 12:32:52 PM 1087.0 978.6
6/7/2019 12:32:53 PM 1014.2 905.8
6/7/2019 12:32:54 PM 1008.2 899.8
6/7/2019 12:32:55 PM 985.9 877.5
6/7/2019 12:32:56 PM 967.9 859.5
6/7/2019 12:32:57 PM 897.3 788.9
6/7/2019 12:32:58 PM 861.6 753.2
6/7/2019 12:32:59 PM 842.5 734.1
6/7/2019 12:33:00 PM 839.9 731.5
6/7/2019 12:33:01 PM 826.2 717.8
6/7/2019 12:33:02 PM 762.1 653.7
6/7/2019 12:33:03 PM 731.0 622.6
6/7/2019 12:33:04 PM 700.0 591.6
6/7/2019 12:33:05 PM 681.1 572.7
6/7/2019 12:33:06 PM 667.2 558.8
6/7/2019 12:33:07 PM 652.5 544.1
6/7/2019 12:33:08 PM 592.7 484.3
6/7/2019 12:33:09 PM 574.5 466.1
6/7/2019 12:33:10 PM 514.0 405.6
6/7/2019 12:33:11 PM 533.8 425.4
6/7/2019 12:33:12 PM 528.9 420.5
6/7/2019 12:33:13 PM 525.3 416.9
6/7/2019 12:33:14 PM 521.0 412.6
6/7/2019 12:33:15 PM 517.0 408.6
6/7/2019 12:33:16 PM 512.5 404.1
6/7/2019 12:33:17 PM 508.6 400.2
6/7/2019 12:33:18 PM 504.5 396.1
6/7/2019 12:33:19 PM 500.3 391.9
6/7/2019 12:33:20 PM 496.7 388.3
6/7/2019 12:33:21 PM 492.7 384.3
6/7/2019 12:33:22 PM 447.2 338.8
6/7/2019 12:33:23 PM 434.3 325.9
6/7/2019 12:33:24 PM 426.5 318.1
6/7/2019 12:33:25 PM 420.4 312.0
6/7/2019 12:33:26 PM 416.1 307.7
6/7/2019 12:33:27 PM 411.5 303.1
6/7/2019 12:33:28 PM 407.6 299.2
6/7/2019 12:33:29 PM 403.5 295.1
6/7/2019 12:33:30 PM 400.2 291.8
6/7/2019 12:33:31 PM 396.4 288.0
6/7/2019 12:33:32 PM 393.3 284.9
6/7/2019 12:33:33 PM 390.6 282.2
6/7/2019 12:33:34 PM 389.3 280.9
6/7/2019 12:33:35 PM 388.8 280.4
6/7/2019 12:33:36 PM 388.8 280.4
6/7/2019 12:33:37 PM 388.9 280.5
6/7/2019 12:33:38 PM 388.6 280.2
6/7/2019 12:33:39 PM 385.6 277.2
6/7/2019 12:33:40 PM 382.7 274.3
6/7/2019 12:33:41 PM 380.4 272.0
6/7/2019 12:33:42 PM 377.8 269.4
6/7/2019 12:33:43 PM 375.5 267.1
6/7/2019 12:33:44 PM 373.2 264.8
6/7/2019 12:33:45 PM 371.4 263.0
6/7/2019 12:33:46 PM 369.1 260.7
6/7/2019 12:33:47 PM 366.6 258.2
6/7/2019 12:33:48 PM 363.0 254.6
6/7/2019 12:33:49 PM 359.2 250.8
6/7/2019 12:33:50 PM 354.6 246.2
6/7/2019 12:33:51 PM 350.7 242.3
6/7/2019 12:33:52 PM 346.5 238.1
6/7/2019 12:33:53 PM 343.0 234.6
6/7/2019 12:33:54 PM 339.2 230.8
6/7/2019 12:33:55 PM 335.9 227.5
6/7/2019 12:33:56 PM 332.1 223.7
6/7/2019 12:33:57 PM 328.7 220.3
6/7/2019 12:33:58 PM 324.9 216.5
6/7/2019 12:33:59 PM 320.8 212.4
6/7/2019 12:34:00 PM 317.2 208.8
6/7/2019 12:34:01 PM 313.0 204.6
6/7/2019 12:34:02 PM 309.3 200.9
6/7/2019 12:34:03 PM 305.0 196.6
6/7/2019 12:34:04 PM 301.2 192.8
6/7/2019 12:34:05 PM 297.0 188.6
6/7/2019 12:34:06 PM 293.4 185.0
Page 153 of 452 August 2019
APPENDIX E34: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A4 TEST-1 Data Log
6/7/2019 12:34:07 PM 289.5 181.1
6/7/2019 12:34:08 PM 286.2 177.8
6/7/2019 12:34:09 PM 282.5 174.1
6/7/2019 12:34:10 PM 279.5 171.1
6/7/2019 12:34:11 PM 276.1 167.7
6/7/2019 12:34:12 PM 273.4 165.0
6/7/2019 12:34:13 PM 270.3 161.9
6/7/2019 12:34:14 PM 267.7 159.3
6/7/2019 12:34:15 PM 265.0 156.6
6/7/2019 12:34:16 PM 262.6 154.2
6/7/2019 12:34:17 PM 259.9 151.5
6/7/2019 12:34:18 PM 257.6 149.2
6/7/2019 12:34:19 PM 254.9 146.5
6/7/2019 12:34:20 PM 252.2 143.8
6/7/2019 12:34:21 PM 249.8 141.4
6/7/2019 12:34:22 PM 247.1 138.7
6/7/2019 12:34:23 PM 244.8 136.4
6/7/2019 12:34:24 PM 242.2 133.8
6/7/2019 12:34:25 PM 240.0 131.6
6/7/2019 12:34:26 PM 237.7 129.3
6/7/2019 12:34:27 PM 235.6 127.2
6/7/2019 12:34:28 PM 233.3 124.9
6/7/2019 12:34:29 PM 231.4 123.0
6/7/2019 12:34:30 PM 229.3 120.9
6/7/2019 12:34:31 PM 227.4 119.0
6/7/2019 12:34:32 PM 225.3 116.9
6/7/2019 12:34:33 PM 223.5 115.1
6/7/2019 12:34:34 PM 221.6 113.2
6/7/2019 12:34:35 PM 219.9 111.5
6/7/2019 12:34:36 PM 218.0 109.6
6/7/2019 12:34:37 PM 216.4 108.0
6/7/2019 12:34:38 PM 214.5 106.1
6/7/2019 12:34:39 PM 212.9 104.5
6/7/2019 12:34:40 PM 211.2 102.8
6/7/2019 12:34:41 PM 209.7 101.3
6/7/2019 12:34:42 PM 208.4 100.0
6/7/2019 12:34:43 PM 207.0 98.6
6/7/2019 12:34:44 PM 206.0 97.6
6/7/2019 12:34:45 PM 205.0 96.6
6/7/2019 12:34:46 PM 204.1 95.7
6/7/2019 12:34:47 PM 203.2 94.8
6/7/2019 12:34:48 PM 202.5 94.1
6/7/2019 12:34:49 PM 201.7 93.3
6/7/2019 12:34:50 PM 201.0 92.6
6/7/2019 12:34:51 PM 200.3 91.9
6/7/2019 12:34:52 PM 199.7 91.3
6/7/2019 12:34:53 PM 199.0 90.6
6/7/2019 12:34:54 PM 198.4 90.0
6/7/2019 12:34:55 PM 197.8 89.4
6/7/2019 12:34:56 PM 197.4 89.0
6/7/2019 12:34:57 PM 196.9 88.5
6/7/2019 12:34:58 PM 196.5 88.1
6/7/2019 12:34:59 PM 196.0 87.6
6/7/2019 12:35:00 PM 195.7 87.3
6/7/2019 12:35:01 PM 195.5 87.1
6/7/2019 12:35:02 PM 195.3 86.9
6/7/2019 12:35:03 PM 195.2 86.8
6/7/2019 12:35:04 PM 195.1 86.7
6/7/2019 12:35:05 PM 195.0 86.6
6/7/2019 12:35:06 PM 194.9 86.5
6/7/2019 12:35:07 PM 194.8 86.4
6/7/2019 12:35:08 PM 194.6 86.2
6/7/2019 12:35:09 PM 194.3 85.9
6/7/2019 12:35:10 PM 193.9 85.5
6/7/2019 12:35:11 PM 193.6 85.2
6/7/2019 12:35:12 PM 193.2 84.8
6/7/2019 12:35:13 PM 192.9 84.5
6/7/2019 12:35:14 PM 192.4 84.0
6/7/2019 12:35:15 PM 192.0 83.6
6/7/2019 12:35:16 PM 191.4 83.0
6/7/2019 12:35:17 PM 190.9 82.5
6/7/2019 12:35:18 PM 190.1 81.7
6/7/2019 12:35:19 PM 189.5 81.1
6/7/2019 12:35:20 PM 188.7 80.3
6/7/2019 12:35:21 PM 188.0 79.6
6/7/2019 12:35:22 PM 187.2 78.8
6/7/2019 12:35:23 PM 186.4 78.0
6/7/2019 12:35:24 PM 185.7 77.3
6/7/2019 12:35:25 PM 184.9 76.5
Page 154 of 452 August 2019
APPENDIX E34: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A4 TEST-1 Data Log
6/7/2019 12:35:26 PM 184.1 75.7
6/7/2019 12:35:27 PM 183.2 74.8
6/7/2019 12:35:28 PM 182.2 73.8
6/7/2019 12:35:29 PM 180.7 72.3
6/7/2019 12:35:30 PM 179.1 70.7
6/7/2019 12:35:31 PM 177.0 68.6
6/7/2019 12:35:32 PM 175.0 66.6
6/7/2019 12:35:33 PM 172.7 64.3
6/7/2019 12:35:34 PM 170.7 62.3
6/7/2019 12:35:35 PM 168.4 60.0
6/7/2019 12:35:36 PM 166.5 58.1
6/7/2019 12:35:37 PM 164.4 56.0
6/7/2019 12:35:38 PM 162.5 54.1
6/7/2019 12:35:39 PM 160.5 52.1
6/7/2019 12:35:40 PM 158.8 50.4
6/7/2019 12:35:41 PM 157.3 48.9
6/7/2019 12:35:42 PM 156.4 48.0
6/7/2019 12:35:43 PM 155.7 47.3
6/7/2019 12:35:44 PM 155.5 47.1
6/7/2019 12:35:45 PM 155.4 47.0
6/7/2019 12:35:46 PM 155.4 47.0
6/7/2019 12:35:47 PM 155.4 47.0
6/7/2019 12:35:48 PM 155.5 47.1
6/7/2019 12:35:49 PM 155.5 47.1
6/7/2019 12:35:50 PM 155.6 47.2
6/7/2019 12:35:51 PM 155.6 47.2
6/7/2019 12:35:52 PM 155.7 47.3
6/7/2019 12:35:53 PM 155.7 47.3
6/7/2019 12:35:54 PM 155.7 47.3
6/7/2019 12:35:55 PM 155.7 47.3
6/7/2019 12:35:56 PM 155.8 47.4
6/7/2019 12:35:57 PM 155.8 47.4
6/7/2019 12:35:58 PM 155.8 47.4
6/7/2019 12:35:59 PM 155.8 47.4
6/7/2019 12:36:00 PM 155.9 47.5
6/7/2019 12:36:01 PM 155.9 47.5
6/7/2019 12:36:02 PM 156.0 47.6
6/7/2019 12:36:03 PM 156.0 47.6
6/7/2019 12:36:04 PM 156.0 47.6
6/7/2019 12:36:05 PM 156.1 47.7
6/7/2019 12:36:06 PM 156.2 47.8
6/7/2019 12:36:07 PM 156.3 47.9
6/7/2019 12:36:08 PM 156.3 47.9
6/7/2019 12:36:09 PM 156.3 47.9
6/7/2019 12:36:10 PM 156.3 47.9
6/7/2019 12:36:11 PM 156.3 47.9
6/7/2019 12:36:12 PM 156.2 47.8
6/7/2019 12:36:13 PM 156.2 47.8
6/7/2019 12:36:14 PM 156.1 47.7
6/7/2019 12:36:15 PM 156.0 47.6
6/7/2019 12:36:16 PM 155.9 47.5
6/7/2019 12:36:17 PM 155.9 47.5
6/7/2019 12:36:18 PM 155.8 47.4
6/7/2019 12:36:19 PM 155.7 47.3
6/7/2019 12:36:20 PM 155.5 47.1
6/7/2019 12:36:21 PM 155.3 46.9
6/7/2019 12:36:22 PM 155.2 46.8
6/7/2019 12:36:23 PM 155.0 46.6
6/7/2019 12:36:24 PM 154.8 46.4
6/7/2019 12:36:25 PM 154.6 46.2
6/7/2019 12:36:26 PM 154.4 46.0
6/7/2019 12:36:27 PM 154.3 45.9
6/7/2019 12:36:28 PM 154.1 45.7
6/7/2019 12:36:29 PM 153.9 45.5
6/7/2019 12:36:30 PM 153.7 45.3
6/7/2019 12:36:31 PM 153.5 45.1
6/7/2019 12:36:32 PM 153.4 45.0
6/7/2019 12:36:33 PM 153.4 45.0
6/7/2019 12:36:34 PM 153.4 45.0
6/7/2019 12:36:35 PM 153.4 45.0
6/7/2019 12:36:36 PM 153.6 45.2
6/7/2019 12:36:37 PM 153.7 45.3
6/7/2019 12:36:38 PM 153.8 45.4
6/7/2019 12:36:39 PM 153.9 45.5
6/7/2019 12:36:40 PM 154.0 45.6
6/7/2019 12:36:41 PM 154.1 45.7
6/7/2019 12:36:42 PM 154.2 45.8
6/7/2019 12:36:43 PM 154.3 45.9
6/7/2019 12:36:44 PM 154.4 46.0
Page 155 of 452 August 2019
APPENDIX E34: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A4 TEST-1 Data Log
6/7/2019 12:36:45 PM 154.3 45.9
6/7/2019 12:36:46 PM 154.2 45.8
6/7/2019 12:36:47 PM 154.0 45.6
6/7/2019 12:36:48 PM 153.9 45.5
6/7/2019 12:36:49 PM 153.6 45.2
6/7/2019 12:36:50 PM 153.3 44.9
6/7/2019 12:36:51 PM 153.0 44.6
6/7/2019 12:36:52 PM 152.8 44.4
6/7/2019 12:36:53 PM 152.5 44.1
6/7/2019 12:36:54 PM 152.3 43.9
6/7/2019 12:36:55 PM 152.0 43.6
6/7/2019 12:36:56 PM 151.7 43.3
6/7/2019 12:36:57 PM 151.5 43.1
6/7/2019 12:36:58 PM 151.3 42.9
6/7/2019 12:36:59 PM 151.1 42.7
6/7/2019 12:37:00 PM 150.9 42.5
6/7/2019 12:37:01 PM 150.7 42.3
6/7/2019 12:37:02 PM 150.6 42.2
6/7/2019 12:37:03 PM 150.4 42.0
6/7/2019 12:37:04 PM 150.3 41.9
6/7/2019 12:37:05 PM 150.1 41.7
6/7/2019 12:37:06 PM 150.0 41.6
6/7/2019 12:37:07 PM 149.9 41.5
6/7/2019 12:37:08 PM 149.7 41.3
6/7/2019 12:37:09 PM 149.6 41.2
6/7/2019 12:37:10 PM 149.5 41.1
6/7/2019 12:37:11 PM 149.4 41.0
6/7/2019 12:37:12 PM 149.3 40.9
6/7/2019 12:37:13 PM 149.2 40.8
6/7/2019 12:37:14 PM 149.1 40.7
6/7/2019 12:37:15 PM 149.1 40.7
6/7/2019 12:37:16 PM 149.0 40.6
6/7/2019 12:37:17 PM 148.9 40.5
6/7/2019 12:37:18 PM 148.8 40.4
6/7/2019 12:37:19 PM 148.7 40.3
6/7/2019 12:37:20 PM 148.6 40.2
6/7/2019 12:37:21 PM 148.6 40.2
6/7/2019 12:37:22 PM 148.5 40.1
6/7/2019 12:37:23 PM 148.4 40.0
6/7/2019 12:37:24 PM 148.3 39.9
6/7/2019 12:37:25 PM 148.2 39.8
6/7/2019 12:37:26 PM 148.2 39.8
6/7/2019 12:37:27 PM 148.1 39.7
6/7/2019 12:37:28 PM 148.0 39.6
6/7/2019 12:37:29 PM 147.9 39.5
6/7/2019 12:37:30 PM 147.8 39.4
6/7/2019 12:37:31 PM 147.7 39.3
6/7/2019 12:37:32 PM 147.6 39.2
6/7/2019 12:37:33 PM 147.6 39.2
6/7/2019 12:37:34 PM 147.5 39.1
6/7/2019 12:37:35 PM 147.4 39.0
6/7/2019 12:37:36 PM 147.3 38.9
6/7/2019 12:37:37 PM 147.3 38.9
6/7/2019 12:37:38 PM 147.2 38.8
6/7/2019 12:37:39 PM 147.2 38.8
6/7/2019 12:37:40 PM 147.1 38.7
6/7/2019 12:37:41 PM 147.1 38.7
6/7/2019 12:37:42 PM 147.0 38.6
6/7/2019 12:37:43 PM 147.0 38.6
6/7/2019 12:37:44 PM 147.0 38.6
6/7/2019 12:37:45 PM 147.0 38.6
6/7/2019 12:37:46 PM 147.0 38.6
6/7/2019 12:37:47 PM 146.9 38.5
6/7/2019 12:37:48 PM 146.9 38.5
6/7/2019 12:37:49 PM 146.9 38.5
6/7/2019 12:37:50 PM 146.9 38.5
6/7/2019 12:37:51 PM 146.9 38.5
6/7/2019 12:37:52 PM 146.9 38.5
6/7/2019 12:37:53 PM 146.9 38.5
6/7/2019 12:37:54 PM 147.0 38.6
6/7/2019 12:37:55 PM 147.0 38.6
6/7/2019 12:37:56 PM 147.0 38.6
6/7/2019 12:37:57 PM 147.0 38.6
6/7/2019 12:37:58 PM 147.0 38.6
6/7/2019 12:37:59 PM 147.0 38.6
6/7/2019 12:38:00 PM 147.0 38.6
6/7/2019 12:38:01 PM 147.0 38.6
6/7/2019 12:38:02 PM 147.1 38.7
6/7/2019 12:38:03 PM 147.1 38.7
Page 156 of 452 August 2019
APPENDIX E34: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A4 TEST-1 Data Log
6/7/2019 12:38:04 PM 147.1 38.7
6/7/2019 12:38:05 PM 147.1 38.7
6/7/2019 12:38:06 PM 147.1 38.7
6/7/2019 12:38:07 PM 147.2 38.8
6/7/2019 12:38:08 PM 147.2 38.8
6/7/2019 12:38:09 PM 147.2 38.8
6/7/2019 12:38:10 PM 147.3 38.9
6/7/2019 12:38:11 PM 147.3 38.9
6/7/2019 12:38:12 PM 147.3 38.9
6/7/2019 12:38:13 PM 147.4 39.0
6/7/2019 12:38:14 PM 147.4 39.0
6/7/2019 12:38:15 PM 147.4 39.0
6/7/2019 12:38:16 PM 147.5 39.1
6/7/2019 12:38:17 PM 147.5 39.1
6/7/2019 12:38:18 PM 147.6 39.2
6/7/2019 12:38:19 PM 147.6 39.2
6/7/2019 12:38:20 PM 147.6 39.2
6/7/2019 12:38:21 PM 147.7 39.3
6/7/2019 12:38:22 PM 147.7 39.3
6/7/2019 12:38:23 PM 147.7 39.3
6/7/2019 12:38:24 PM 147.7 39.3
6/7/2019 12:38:25 PM 147.8 39.4
6/7/2019 12:38:26 PM 147.8 39.4
6/7/2019 12:38:27 PM 147.8 39.4
6/7/2019 12:38:28 PM 147.8 39.4
6/7/2019 12:38:29 PM 147.8 39.4
6/7/2019 12:38:30 PM 147.8 39.4
6/7/2019 12:38:31 PM 147.7 39.3
6/7/2019 12:38:32 PM 147.7 39.3
6/7/2019 12:38:33 PM 147.7 39.3
6/7/2019 12:38:34 PM 147.7 39.3
6/7/2019 12:38:35 PM 147.6 39.2
6/7/2019 12:38:36 PM 147.6 39.2
6/7/2019 12:38:37 PM 147.5 39.1
6/7/2019 12:38:38 PM 147.5 39.1
6/7/2019 12:38:39 PM 147.4 39.0
6/7/2019 12:38:40 PM 147.4 39.0
6/7/2019 12:38:41 PM 147.4 39.0
6/7/2019 12:38:42 PM 147.3 38.9
6/7/2019 12:38:43 PM 147.3 38.9
6/7/2019 12:38:44 PM 147.3 38.9
6/7/2019 12:38:45 PM 147.2 38.8
6/7/2019 12:38:46 PM 147.2 38.8
6/7/2019 12:38:47 PM 147.2 38.8
6/7/2019 12:38:48 PM 147.2 38.8
6/7/2019 12:38:49 PM 147.2 38.8
6/7/2019 12:38:50 PM 147.3 38.9
6/7/2019 12:38:51 PM 147.3 38.9
6/7/2019 12:38:52 PM 147.3 38.9
6/7/2019 12:38:53 PM 147.4 39.0
6/7/2019 12:38:54 PM 147.4 39.0
6/7/2019 12:38:55 PM 147.4 39.0
6/7/2019 12:38:56 PM 147.5 39.1
6/7/2019 12:38:57 PM 147.5 39.1
6/7/2019 12:38:58 PM 147.5 39.1
6/7/2019 12:38:59 PM 147.5 39.1
6/7/2019 12:39:00 PM 147.5 39.1
6/7/2019 12:39:01 PM 147.4 39.0
6/7/2019 12:39:02 PM 147.4 39.0
6/7/2019 12:39:03 PM 147.3 38.9
6/7/2019 12:39:04 PM 147.2 38.8
6/7/2019 12:39:05 PM 147.1 38.7
6/7/2019 12:39:06 PM 147.0 38.6
6/7/2019 12:39:07 PM 146.9 38.5
6/7/2019 12:39:08 PM 146.8 38.4
6/7/2019 12:39:09 PM 146.7 38.3
6/7/2019 12:39:10 PM 146.5 38.1
6/7/2019 12:39:11 PM 146.4 38.0
6/7/2019 12:39:12 PM 146.2 37.8
6/7/2019 12:39:13 PM 146.1 37.7
6/7/2019 12:39:14 PM 145.9 37.5
6/7/2019 12:39:15 PM 145.8 37.4
6/7/2019 12:39:16 PM 145.6 37.2
6/7/2019 12:39:17 PM 145.5 37.1
6/7/2019 12:39:18 PM 145.3 36.9
6/7/2019 12:39:19 PM 145.2 36.8
6/7/2019 12:39:20 PM 145.0 36.6
6/7/2019 12:39:21 PM 144.8 36.4
6/7/2019 12:39:22 PM 144.7 36.3
Page 157 of 452 August 2019
APPENDIX E34: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A4 TEST-1 Data Log
6/7/2019 12:39:23 PM 144.5 36.1
6/7/2019 12:39:24 PM 144.4 36.0
6/7/2019 12:39:25 PM 144.2 35.8
6/7/2019 12:39:26 PM 144.1 35.7
6/7/2019 12:39:27 PM 143.9 35.5
6/7/2019 12:39:28 PM 143.8 35.4
6/7/2019 12:39:29 PM 143.7 35.3
6/7/2019 12:39:30 PM 143.5 35.1
6/7/2019 12:39:31 PM 143.4 35.0
6/7/2019 12:39:32 PM 143.2 34.8
6/7/2019 12:39:33 PM 143.1 34.7
6/7/2019 12:39:34 PM 143.0 34.6
6/7/2019 12:39:35 PM 142.8 34.4
6/7/2019 12:39:36 PM 142.7 34.3
6/7/2019 12:39:37 PM 142.6 34.2
6/7/2019 12:39:38 PM 142.4 34.0
6/7/2019 12:39:39 PM 142.3 33.9
6/7/2019 12:39:40 PM 142.2 33.8
6/7/2019 12:39:41 PM 142.0 33.6
6/7/2019 12:39:42 PM 141.9 33.5
6/7/2019 12:39:43 PM 141.8 33.4
6/7/2019 12:39:44 PM 141.6 33.2
6/7/2019 12:39:45 PM 141.5 33.1
6/7/2019 12:39:46 PM 141.4 33.0
6/7/2019 12:39:47 PM 141.2 32.8
6/7/2019 12:39:48 PM 141.1 32.7
6/7/2019 12:39:49 PM 141.0 32.6
6/7/2019 12:39:50 PM 140.8 32.4
6/7/2019 12:39:51 PM 140.7 32.3
6/7/2019 12:39:52 PM 140.6 32.2
6/7/2019 12:39:53 PM 140.5 32.1
6/7/2019 12:39:54 PM 140.3 31.9
6/7/2019 12:39:55 PM 140.2 31.8
6/7/2019 12:39:56 PM 140.1 31.7
6/7/2019 12:39:57 PM 140.0 31.6
6/7/2019 12:39:58 PM 139.9 31.5
6/7/2019 12:39:59 PM 139.8 31.4
6/7/2019 12:40:00 PM 139.7 31.3
6/7/2019 12:40:01 PM 139.6 31.2
6/7/2019 12:40:02 PM 139.5 31.1
6/7/2019 12:40:03 PM 139.4 31.0
6/7/2019 12:40:04 PM 139.3 30.9
6/7/2019 12:40:05 PM 139.3 30.9
6/7/2019 12:40:06 PM 139.2 30.8
6/7/2019 12:40:07 PM 139.1 30.7
6/7/2019 12:40:08 PM 139.0 30.6
6/7/2019 12:40:09 PM 138.9 30.5
6/7/2019 12:40:10 PM 138.8 30.4
6/7/2019 12:40:11 PM 138.7 30.3
6/7/2019 12:40:12 PM 138.6 30.2
6/7/2019 12:40:13 PM 138.6 30.2
6/7/2019 12:40:14 PM 138.5 30.1
6/7/2019 12:40:15 PM 138.4 30.0
6/7/2019 12:40:16 PM 138.4 30.0
6/7/2019 12:40:17 PM 138.3 29.9
6/7/2019 12:40:18 PM 138.2 29.8
6/7/2019 12:40:19 PM 138.1 29.7
6/7/2019 12:40:20 PM 138.1 29.7
6/7/2019 12:40:21 PM 138.0 29.6
6/7/2019 12:40:22 PM 138.0 29.6
6/7/2019 12:40:23 PM 137.9 29.5
6/7/2019 12:40:24 PM 137.9 29.5
6/7/2019 12:40:25 PM 137.9 29.5
6/7/2019 12:40:26 PM 137.8 29.4
6/7/2019 12:40:27 PM 137.8 29.4
6/7/2019 12:40:28 PM 137.8 29.4
6/7/2019 12:40:29 PM 137.7 29.3
6/7/2019 12:40:30 PM 137.7 29.3
6/7/2019 12:40:31 PM 137.7 29.3
6/7/2019 12:40:32 PM 137.7 29.3
6/7/2019 12:40:33 PM 137.7 29.3
6/7/2019 12:40:34 PM 137.7 29.3
6/7/2019 12:40:35 PM 137.7 29.3
6/7/2019 12:40:36 PM 137.7 29.3
6/7/2019 12:40:37 PM 137.7 29.3
6/7/2019 12:40:38 PM 137.7 29.3
6/7/2019 12:40:39 PM 137.7 29.3
6/7/2019 12:40:40 PM 137.7 29.3
6/7/2019 12:40:41 PM 137.7 29.3
Page 158 of 452 August 2019
APPENDIX E34: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A4 TEST-1 Data Log
6/7/2019 12:40:42 PM 137.7 29.3
6/7/2019 12:40:43 PM 137.7 29.3
6/7/2019 12:40:44 PM 137.7 29.3
6/7/2019 12:40:45 PM 137.7 29.3
6/7/2019 12:40:46 PM 137.7 29.3
6/7/2019 12:40:47 PM 137.8 29.4
6/7/2019 12:40:48 PM 137.8 29.4
6/7/2019 12:40:49 PM 137.8 29.4
Page 159 of 452 August 2019
APPENDIX E34: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-A4 TEST-1 1221
SEEP-A4 TEST-1 1222
SEEP-A4 TEST-1 1223
SEEP-A4 TEST-1 1224
Location EC Reading
(µS/cms)
SEEP-A4 TEST-1 243.7
SEEP-A4 TEST-1 2,163
SEEP-A4 TEST-1 18,130
SEEP-A4 TEST-1 133,511
q 300,700
K 1.3399
0.7
11.0
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Calculated Flow Rate Q
L/s
GPM
1,000 24.2
10000 24.1
100,000 24.1
Table E4 SEEP-A4 TEST-1 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)581,545.6 (s) . (µS/cms)
100 24.2
Average (pre-test)110.6 (µS/cms)
Average (post-test)142.6 (µS/cms)
Table E3 SEEP-A4 TEST-1 YSI Salt Dilution Calibration Data
Calibration Temperature
(mg/L)(°C)
Geo Mean 108.6 (µS/cms)
108.8 21.8
109.2 21.6
107.8 21.8
108.6 21.8
Average 108.6 (µS/cms)
(µS/cms)(°C)
Table E2 SEEP-A4 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 160 of 452 August 2019
APPENDIX E35: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 12:59:34 PM 113.4 -
6/7/2019 12:59:35 PM 113.4 -
6/7/2019 12:59:36 PM 113.3 -
6/7/2019 12:59:37 PM 113.2 -
6/7/2019 12:59:38 PM 113.1 -
6/7/2019 12:59:39 PM 113.0 -
6/7/2019 12:59:40 PM 112.9 -
6/7/2019 12:59:41 PM 112.8 -
6/7/2019 12:59:42 PM 112.7 -
6/7/2019 12:59:43 PM 112.6 -
6/7/2019 12:59:44 PM 112.5 -
6/7/2019 12:59:45 PM 112.4 -
6/7/2019 12:59:46 PM 112.3 -
6/7/2019 12:59:47 PM 112.3 -
6/7/2019 12:59:48 PM 112.2 -
6/7/2019 12:59:49 PM 112.2 -
6/7/2019 12:59:50 PM 112.2 -
6/7/2019 12:59:51 PM 112.2 -
6/7/2019 12:59:52 PM 112.2 -
6/7/2019 12:59:53 PM 112.2 -
6/7/2019 12:59:54 PM 112.5 -
6/7/2019 12:59:55 PM 332.9 220.3
6/7/2019 12:59:56 PM 625.3 512.7
6/7/2019 12:59:57 PM 3823.0 3710.4
6/7/2019 12:59:58 PM 6922.9 6810.3
6/7/2019 12:59:59 PM 10262.5 10149.9
6/7/2019 1:00:00 PM 14006.5 13893.9
6/7/2019 1:00:01 PM 17372.3 17259.7
6/7/2019 1:00:02 PM 18846.2 18733.6
6/7/2019 1:00:03 PM 20072.4 19959.8
6/7/2019 1:00:04 PM 20731.1 20618.5
6/7/2019 1:00:05 PM 20833.0 20720.4
6/7/2019 1:00:06 PM 20918.3 20805.7
6/7/2019 1:00:07 PM 20886.2 20773.6
6/7/2019 1:00:08 PM 20742.8 20630.2
6/7/2019 1:00:09 PM 19101.9 18989.3
6/7/2019 1:00:10 PM 18157.1 18044.5
6/7/2019 1:00:11 PM 17058.5 16945.9
6/7/2019 1:00:12 PM 16417.0 16304.4
6/7/2019 1:00:13 PM 15766.2 15653.6
6/7/2019 1:00:14 PM 14012.5 13899.9
6/7/2019 1:00:15 PM 13125.0 13012.4
6/7/2019 1:00:16 PM 12218.5 12105.9
6/7/2019 1:00:17 PM 11773.0 11660.4
6/7/2019 1:00:18 PM 11355.2 11242.6
6/7/2019 1:00:19 PM 10324.7 10212.1
6/7/2019 1:00:20 PM 9610.0 9497.4
6/7/2019 1:00:21 PM 9100.5 8987.9
6/7/2019 1:00:22 PM 8835.0 8722.4
6/7/2019 1:00:23 PM 8574.7 8462.1
6/7/2019 1:00:24 PM 7669.6 7557.0
6/7/2019 1:00:25 PM 7139.5 7026.9
6/7/2019 1:00:26 PM 6607.1 6494.5
6/7/2019 1:00:27 PM 6424.1 6311.5
6/7/2019 1:00:28 PM 5771.8 5659.2
6/7/2019 1:00:29 PM 5310.3 5197.7
6/7/2019 1:00:30 PM 5006.9 4894.3
6/7/2019 1:00:31 PM 4746.9 4634.3
6/7/2019 1:00:32 PM 4661.0 4548.4
6/7/2019 1:00:33 PM 4244.7 4132.1
6/7/2019 1:00:34 PM 4049.4 3936.8
6/7/2019 1:00:35 PM 3829.5 3716.9
6/7/2019 1:00:36 PM 3724.7 3612.1
6/7/2019 1:00:37 PM 3601.3 3488.7
6/7/2019 1:00:38 PM 3504.5 3391.9
6/7/2019 1:00:39 PM 3190.0 3077.4
6/7/2019 1:00:40 PM 3070.1 2957.5
6/7/2019 1:00:41 PM 2943.7 2831.1
6/7/2019 1:00:42 PM 2899.1 2786.5
6/7/2019 1:00:43 PM 2839.7 2727.1
Table E1 SEEP-A4 TEST-2 Data Log
Page 161 of 452 August 2019
APPENDIX E35: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A4 TEST-2 Data Log
6/7/2019 1:00:44 PM 2792.9 2680.3
6/7/2019 1:00:45 PM 2595.3 2482.7
6/7/2019 1:00:46 PM 2509.4 2396.8
6/7/2019 1:00:47 PM 2463.4 2350.8
6/7/2019 1:00:48 PM 2406.1 2293.5
6/7/2019 1:00:49 PM 2398.0 2285.4
6/7/2019 1:00:50 PM 2373.6 2261.0
6/7/2019 1:00:51 PM 2347.9 2235.3
6/7/2019 1:00:52 PM 2319.4 2206.8
6/7/2019 1:00:53 PM 2126.3 2013.7
6/7/2019 1:00:54 PM 2095.2 1982.6
6/7/2019 1:00:55 PM 2057.8 1945.2
6/7/2019 1:00:56 PM 2034.2 1921.6
6/7/2019 1:00:57 PM 1998.0 1885.4
6/7/2019 1:00:58 PM 1975.3 1862.7
6/7/2019 1:00:59 PM 1953.2 1840.6
6/7/2019 1:01:00 PM 1802.7 1690.1
6/7/2019 1:01:01 PM 1758.1 1645.5
6/7/2019 1:01:02 PM 1728.5 1615.9
6/7/2019 1:01:03 PM 1711.4 1598.8
6/7/2019 1:01:04 PM 1689.8 1577.2
6/7/2019 1:01:05 PM 1671.4 1558.8
6/7/2019 1:01:06 PM 1647.8 1535.2
6/7/2019 1:01:07 PM 1544.4 1431.8
6/7/2019 1:01:08 PM 1489.6 1377.0
6/7/2019 1:01:09 PM 1484.6 1372.0
6/7/2019 1:01:10 PM 1470.2 1357.6
6/7/2019 1:01:11 PM 1442.6 1330.0
6/7/2019 1:01:12 PM 1433.4 1320.8
6/7/2019 1:01:13 PM 1417.7 1305.1
6/7/2019 1:01:14 PM 1411.5 1298.9
6/7/2019 1:01:15 PM 1404.8 1292.2
6/7/2019 1:01:16 PM 1312.4 1199.8
6/7/2019 1:01:17 PM 1256.1 1143.5
6/7/2019 1:01:18 PM 1207.2 1094.6
6/7/2019 1:01:19 PM 1189.6 1077.0
6/7/2019 1:01:20 PM 1178.4 1065.8
6/7/2019 1:01:21 PM 1176.1 1063.5
6/7/2019 1:01:22 PM 1173.2 1060.6
6/7/2019 1:01:23 PM 1169.0 1056.4
6/7/2019 1:01:24 PM 1165.9 1053.3
6/7/2019 1:01:25 PM 1161.8 1049.2
6/7/2019 1:01:26 PM 1156.6 1044.0
6/7/2019 1:01:27 PM 1149.6 1037.0
6/7/2019 1:01:28 PM 1089.5 976.9
6/7/2019 1:01:29 PM 1101.7 989.1
6/7/2019 1:01:30 PM 1077.9 965.3
6/7/2019 1:01:31 PM 1069.9 957.3
6/7/2019 1:01:32 PM 1058.1 945.5
6/7/2019 1:01:33 PM 1038.7 926.1
6/7/2019 1:01:34 PM 999.7 887.1
6/7/2019 1:01:35 PM 964.6 852.0
6/7/2019 1:01:36 PM 956.7 844.1
6/7/2019 1:01:37 PM 951.7 839.1
6/7/2019 1:01:38 PM 933.3 820.7
6/7/2019 1:01:39 PM 926.0 813.4
6/7/2019 1:01:40 PM 916.9 804.3
6/7/2019 1:01:41 PM 854.8 742.2
6/7/2019 1:01:42 PM 826.8 714.2
6/7/2019 1:01:43 PM 830.4 717.8
6/7/2019 1:01:44 PM 819.0 706.4
6/7/2019 1:01:45 PM 804.4 691.8
6/7/2019 1:01:46 PM 800.3 687.7
6/7/2019 1:01:47 PM 796.0 683.4
6/7/2019 1:01:48 PM 789.3 676.7
6/7/2019 1:01:49 PM 712.8 600.2
6/7/2019 1:01:50 PM 696.9 584.3
6/7/2019 1:01:51 PM 668.9 556.3
6/7/2019 1:01:52 PM 654.2 541.6
6/7/2019 1:01:53 PM 641.0 528.4
6/7/2019 1:01:54 PM 628.3 515.7
6/7/2019 1:01:55 PM 574.4 461.8
6/7/2019 1:01:56 PM 555.2 442.6
6/7/2019 1:01:57 PM 608.1 495.5
6/7/2019 1:01:58 PM 633.9 521.3
6/7/2019 1:01:59 PM 635.2 522.6
6/7/2019 1:02:00 PM 634.4 521.8
Page 162 of 452 August 2019
APPENDIX E35: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A4 TEST-2 Data Log
6/7/2019 1:02:01 PM 638.0 525.4
6/7/2019 1:02:02 PM 642.2 529.6
6/7/2019 1:02:03 PM 647.7 535.1
6/7/2019 1:02:04 PM 650.4 537.8
6/7/2019 1:02:05 PM 653.7 541.1
6/7/2019 1:02:06 PM 701.8 589.2
6/7/2019 1:02:07 PM 728.0 615.4
6/7/2019 1:02:08 PM 773.8 661.2
6/7/2019 1:02:09 PM 841.9 729.3
6/7/2019 1:02:10 PM 844.3 731.7
6/7/2019 1:02:11 PM 889.1 776.5
6/7/2019 1:02:12 PM 858.7 746.1
6/7/2019 1:02:13 PM 849.1 736.5
6/7/2019 1:02:14 PM 827.9 715.3
6/7/2019 1:02:15 PM 831.2 718.6
6/7/2019 1:02:16 PM 815.2 702.6
6/7/2019 1:02:17 PM 808.7 696.1
6/7/2019 1:02:18 PM 805.9 693.3
6/7/2019 1:02:19 PM 806.7 694.1
6/7/2019 1:02:20 PM 862.1 749.5
6/7/2019 1:02:21 PM 891.9 779.3
6/7/2019 1:02:22 PM 779.3 666.7
6/7/2019 1:02:23 PM 761.9 649.3
6/7/2019 1:02:24 PM 762.8 650.2
6/7/2019 1:02:25 PM 750.1 637.5
6/7/2019 1:02:26 PM 749.4 636.8
6/7/2019 1:02:27 PM 750.9 638.3
6/7/2019 1:02:28 PM 750.3 637.7
6/7/2019 1:02:29 PM 750.8 638.2
6/7/2019 1:02:30 PM 750.3 637.7
6/7/2019 1:02:31 PM 748.3 635.7
6/7/2019 1:02:32 PM 747.4 634.8
6/7/2019 1:02:33 PM 746.3 633.7
6/7/2019 1:02:34 PM 745.9 633.3
6/7/2019 1:02:35 PM 743.3 630.7
6/7/2019 1:02:36 PM 657.6 545.0
6/7/2019 1:02:37 PM 643.7 531.1
6/7/2019 1:02:38 PM 603.5 490.9
6/7/2019 1:02:39 PM 597.4 484.8
6/7/2019 1:02:40 PM 594.6 482.0
6/7/2019 1:02:41 PM 592.2 479.6
6/7/2019 1:02:42 PM 548.7 436.1
6/7/2019 1:02:43 PM 557.3 444.7
6/7/2019 1:02:44 PM 550.0 437.4
6/7/2019 1:02:45 PM 542.5 429.9
6/7/2019 1:02:46 PM 534.9 422.3
6/7/2019 1:02:47 PM 525.1 412.5
6/7/2019 1:02:48 PM 517.4 404.8
6/7/2019 1:02:49 PM 509.4 396.8
6/7/2019 1:02:50 PM 501.9 389.3
6/7/2019 1:02:51 PM 440.9 328.3
6/7/2019 1:02:52 PM 423.5 310.9
6/7/2019 1:02:53 PM 417.7 305.1
6/7/2019 1:02:54 PM 413.2 300.6
6/7/2019 1:02:55 PM 410.4 297.8
6/7/2019 1:02:56 PM 409.1 296.5
6/7/2019 1:02:57 PM 406.0 293.4
6/7/2019 1:02:58 PM 402.4 289.8
6/7/2019 1:02:59 PM 398.9 286.3
6/7/2019 1:03:00 PM 394.3 281.7
6/7/2019 1:03:01 PM 390.2 277.6
6/7/2019 1:03:02 PM 386.1 273.5
6/7/2019 1:03:03 PM 383.0 270.4
6/7/2019 1:03:04 PM 380.3 267.7
6/7/2019 1:03:05 PM 378.1 265.5
6/7/2019 1:03:06 PM 375.6 263.0
6/7/2019 1:03:07 PM 371.4 258.8
6/7/2019 1:03:08 PM 365.2 252.6
6/7/2019 1:03:09 PM 359.8 247.2
6/7/2019 1:03:10 PM 354.2 241.6
6/7/2019 1:03:11 PM 348.5 235.9
6/7/2019 1:03:12 PM 343.9 231.3
6/7/2019 1:03:13 PM 339.0 226.4
6/7/2019 1:03:14 PM 335.1 222.5
6/7/2019 1:03:15 PM 330.8 218.2
6/7/2019 1:03:16 PM 327.7 215.1
6/7/2019 1:03:17 PM 324.3 211.7
6/7/2019 1:03:18 PM 321.1 208.5
6/7/2019 1:03:19 PM 317.6 205.0
Page 163 of 452 August 2019
APPENDIX E35: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A4 TEST-2 Data Log
6/7/2019 1:03:20 PM 315.5 202.9
6/7/2019 1:03:21 PM 313.3 200.7
6/7/2019 1:03:22 PM 311.4 198.8
6/7/2019 1:03:23 PM 309.4 196.8
6/7/2019 1:03:24 PM 307.9 195.3
6/7/2019 1:03:25 PM 306.7 194.1
6/7/2019 1:03:26 PM 305.6 193.0
6/7/2019 1:03:27 PM 304.6 192.0
6/7/2019 1:03:28 PM 304.0 191.4
6/7/2019 1:03:29 PM 302.8 190.2
6/7/2019 1:03:30 PM 300.9 188.3
6/7/2019 1:03:31 PM 299.4 186.8
6/7/2019 1:03:32 PM 297.5 184.9
6/7/2019 1:03:33 PM 295.4 182.8
6/7/2019 1:03:34 PM 292.6 180.0
6/7/2019 1:03:35 PM 290.2 177.6
6/7/2019 1:03:36 PM 287.6 175.0
6/7/2019 1:03:37 PM 285.4 172.8
6/7/2019 1:03:38 PM 282.7 170.1
6/7/2019 1:03:39 PM 280.5 167.9
6/7/2019 1:03:40 PM 278.1 165.5
6/7/2019 1:03:41 PM 275.8 163.2
6/7/2019 1:03:42 PM 273.1 160.5
6/7/2019 1:03:43 PM 270.8 158.2
6/7/2019 1:03:44 PM 268.5 155.9
6/7/2019 1:03:45 PM 266.5 153.9
6/7/2019 1:03:46 PM 264.4 151.8
6/7/2019 1:03:47 PM 262.7 150.1
6/7/2019 1:03:48 PM 260.8 148.2
6/7/2019 1:03:49 PM 259.2 146.6
6/7/2019 1:03:50 PM 257.3 144.7
6/7/2019 1:03:51 PM 255.4 142.8
6/7/2019 1:03:52 PM 253.8 141.2
6/7/2019 1:03:53 PM 252.3 139.7
6/7/2019 1:03:54 PM 251.3 138.7
6/7/2019 1:03:55 PM 250.6 138.0
6/7/2019 1:03:56 PM 250.4 137.8
6/7/2019 1:03:57 PM 250.3 137.7
6/7/2019 1:03:58 PM 250.6 138.0
6/7/2019 1:03:59 PM 251.2 138.6
6/7/2019 1:04:00 PM 252.0 139.4
6/7/2019 1:04:01 PM 252.9 140.3
6/7/2019 1:04:02 PM 253.9 141.3
6/7/2019 1:04:03 PM 255.9 143.3
6/7/2019 1:04:04 PM 258.5 145.9
6/7/2019 1:04:05 PM 261.4 148.8
6/7/2019 1:04:06 PM 263.6 151.0
6/7/2019 1:04:07 PM 266.1 153.5
6/7/2019 1:04:08 PM 268.0 155.4
6/7/2019 1:04:09 PM 270.1 157.5
6/7/2019 1:04:10 PM 271.7 159.1
6/7/2019 1:04:11 PM 273.8 161.2
6/7/2019 1:04:12 PM 275.6 163.0
6/7/2019 1:04:13 PM 276.7 164.1
6/7/2019 1:04:14 PM 277.7 165.1
6/7/2019 1:04:15 PM 278.4 165.8
6/7/2019 1:04:16 PM 279.2 166.6
6/7/2019 1:04:17 PM 279.7 167.1
6/7/2019 1:04:18 PM 280.4 167.8
6/7/2019 1:04:19 PM 281.7 169.1
6/7/2019 1:04:20 PM 283.3 170.7
6/7/2019 1:04:21 PM 284.8 172.2
6/7/2019 1:04:22 PM 327.8 215.2
6/7/2019 1:04:23 PM 327.2 214.6
6/7/2019 1:04:24 PM 334.2 221.6
6/7/2019 1:04:25 PM 339.9 227.3
6/7/2019 1:04:26 PM 341.2 228.6
6/7/2019 1:04:27 PM 342.1 229.5
6/7/2019 1:04:28 PM 342.4 229.8
6/7/2019 1:04:29 PM 341.8 229.2
6/7/2019 1:04:30 PM 340.2 227.6
6/7/2019 1:04:31 PM 339.0 226.4
6/7/2019 1:04:32 PM 339.2 226.6
6/7/2019 1:04:33 PM 340.1 227.5
6/7/2019 1:04:34 PM 341.0 228.4
6/7/2019 1:04:35 PM 341.5 228.9
6/7/2019 1:04:36 PM 342.1 229.5
6/7/2019 1:04:37 PM 342.8 230.2
6/7/2019 1:04:38 PM 343.4 230.8
Page 164 of 452 August 2019
APPENDIX E35: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A4 TEST-2 Data Log
6/7/2019 1:04:39 PM 344.1 231.5
6/7/2019 1:04:40 PM 344.7 232.1
6/7/2019 1:04:41 PM 345.4 232.8
6/7/2019 1:04:42 PM 345.8 233.2
6/7/2019 1:04:43 PM 346.5 233.9
6/7/2019 1:04:44 PM 347.0 234.4
6/7/2019 1:04:45 PM 346.7 234.1
6/7/2019 1:04:46 PM 345.8 233.2
6/7/2019 1:04:47 PM 344.2 231.6
6/7/2019 1:04:48 PM 342.6 230.0
6/7/2019 1:04:49 PM 340.8 228.2
6/7/2019 1:04:50 PM 339.1 226.5
6/7/2019 1:04:51 PM 337.3 224.7
6/7/2019 1:04:52 PM 335.6 223.0
6/7/2019 1:04:53 PM 333.6 221.0
6/7/2019 1:04:54 PM 331.6 219.0
6/7/2019 1:04:55 PM 330.1 217.5
6/7/2019 1:04:56 PM 328.3 215.7
6/7/2019 1:04:57 PM 326.5 213.9
6/7/2019 1:04:58 PM 324.9 212.3
6/7/2019 1:04:59 PM 324.2 211.6
6/7/2019 1:05:00 PM 324.1 211.5
6/7/2019 1:05:01 PM 324.2 211.6
6/7/2019 1:05:02 PM 324.6 212.0
6/7/2019 1:05:03 PM 324.9 212.3
6/7/2019 1:05:04 PM 325.3 212.7
6/7/2019 1:05:05 PM 325.9 213.3
6/7/2019 1:05:06 PM 326.6 214.0
6/7/2019 1:05:07 PM 327.1 214.5
6/7/2019 1:05:08 PM 327.8 215.2
6/7/2019 1:05:09 PM 328.7 216.1
6/7/2019 1:05:10 PM 330.4 217.8
6/7/2019 1:05:11 PM 331.8 219.2
6/7/2019 1:05:12 PM 332.6 220.0
6/7/2019 1:05:13 PM 332.7 220.1
6/7/2019 1:05:14 PM 332.7 220.1
6/7/2019 1:05:15 PM 332.5 219.9
6/7/2019 1:05:16 PM 332.2 219.6
6/7/2019 1:05:17 PM 331.7 219.1
6/7/2019 1:05:18 PM 330.9 218.3
6/7/2019 1:05:19 PM 329.9 217.3
6/7/2019 1:05:20 PM 329.0 216.4
6/7/2019 1:05:21 PM 328.1 215.5
6/7/2019 1:05:22 PM 326.9 214.3
6/7/2019 1:05:23 PM 325.3 212.7
6/7/2019 1:05:24 PM 324.0 211.4
6/7/2019 1:05:25 PM 322.7 210.1
6/7/2019 1:05:26 PM 321.8 209.2
6/7/2019 1:05:27 PM 321.1 208.5
6/7/2019 1:05:28 PM 320.4 207.8
6/7/2019 1:05:29 PM 319.9 207.3
6/7/2019 1:05:30 PM 319.7 207.1
6/7/2019 1:05:31 PM 319.7 207.1
6/7/2019 1:05:32 PM 319.6 207.0
6/7/2019 1:05:33 PM 319.6 207.0
6/7/2019 1:05:34 PM 319.9 207.3
6/7/2019 1:05:35 PM 320.2 207.6
6/7/2019 1:05:36 PM 320.5 207.9
6/7/2019 1:05:37 PM 320.7 208.1
6/7/2019 1:05:38 PM 321.3 208.7
6/7/2019 1:05:39 PM 321.4 208.8
6/7/2019 1:05:40 PM 321.2 208.6
6/7/2019 1:05:41 PM 321.1 208.5
6/7/2019 1:05:42 PM 320.3 207.7
6/7/2019 1:05:43 PM 319.4 206.8
6/7/2019 1:05:44 PM 318.1 205.5
6/7/2019 1:05:45 PM 316.7 204.1
6/7/2019 1:05:46 PM 315.1 202.5
6/7/2019 1:05:47 PM 313.5 200.9
6/7/2019 1:05:48 PM 311.4 198.8
6/7/2019 1:05:49 PM 309.8 197.2
6/7/2019 1:05:50 PM 308.3 195.7
6/7/2019 1:05:51 PM 306.8 194.2
6/7/2019 1:05:52 PM 305.4 192.8
6/7/2019 1:05:53 PM 304.4 191.8
6/7/2019 1:05:54 PM 303.5 190.9
6/7/2019 1:05:55 PM 303.0 190.4
6/7/2019 1:05:56 PM 302.7 190.1
6/7/2019 1:05:57 PM 302.6 190.0
Page 165 of 452 August 2019
APPENDIX E35: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A4 TEST-2 Data Log
6/7/2019 1:05:58 PM 302.7 190.1
6/7/2019 1:05:59 PM 303.1 190.5
6/7/2019 1:06:00 PM 303.6 191.0
6/7/2019 1:06:01 PM 304.5 191.9
6/7/2019 1:06:02 PM 305.3 192.7
6/7/2019 1:06:03 PM 306.3 193.7
6/7/2019 1:06:04 PM 307.1 194.5
6/7/2019 1:06:05 PM 307.7 195.1
6/7/2019 1:06:06 PM 308.1 195.5
6/7/2019 1:06:07 PM 308.1 195.5
6/7/2019 1:06:08 PM 308.1 195.5
6/7/2019 1:06:09 PM 308.0 195.4
6/7/2019 1:06:10 PM 307.9 195.3
6/7/2019 1:06:11 PM 307.7 195.1
6/7/2019 1:06:12 PM 307.8 195.2
6/7/2019 1:06:13 PM 307.9 195.3
6/7/2019 1:06:14 PM 308.3 195.7
6/7/2019 1:06:15 PM 308.8 196.2
6/7/2019 1:06:16 PM 309.0 196.4
6/7/2019 1:06:17 PM 309.1 196.5
6/7/2019 1:06:18 PM 309.4 196.8
6/7/2019 1:06:19 PM 309.8 197.2
6/7/2019 1:06:20 PM 310.8 198.2
6/7/2019 1:06:21 PM 311.8 199.2
6/7/2019 1:06:22 PM 313.0 200.4
6/7/2019 1:06:23 PM 314.0 201.4
6/7/2019 1:06:24 PM 315.4 202.8
6/7/2019 1:06:25 PM 316.5 203.9
6/7/2019 1:06:26 PM 317.5 204.9
6/7/2019 1:06:27 PM 318.2 205.6
6/7/2019 1:06:28 PM 319.3 206.7
6/7/2019 1:06:29 PM 320.8 208.2
6/7/2019 1:06:30 PM 323.3 210.7
Page 166 of 452 August 2019
APPENDIX E35: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-A4 TEST-2 1221
SEEP-A4 TEST-2 1222
SEEP-A4 TEST-2 1223
SEEP-A4 TEST-2 1224
Location EC Reading
(µS/cms)
SEEP-A4 TEST-2 243.7
SEEP-A4 TEST-2 2,163
SEEP-A4 TEST-2 18,130
SEEP-A4 TEST-2 133,511
q 150,300
K 1.3399
0.3
4.9
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Calculated Flow Rate Q
L/s
GPM
1,000 24.2
10000 24.1
100,000 24.1
Table E4 SEEP-A4 TEST-2 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Integral of Conductivity
Data Curve
SUM:Δt(E
Ct-ECbkg)646,633.0 (s) . (µS/cms)
100 24.2
Average (pre-test)110.6 (µS/cms)
Average (post-test)142.6 (µS/cms)
Table E3 SEEP-A4 TEST-2 YSI Salt Dilution Calibration Data
Calibration Temperature
(mg/L)(°C)
Geo Mean 108.6 (µS/cms)
108.8 21.8
109.2 21.6
107.8 21.8
108.6 21.8
Average 108.6 (µS/cms)
(µS/cms)(°C)
Table E2 SEEP-A4 TEST-2 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 167 of 452 August 2019
APPENDIX E36: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 1:19:50 PM 110.6 -
6/7/2019 1:19:51 PM 110.6 -
6/7/2019 1:19:52 PM 110.6 -
6/7/2019 1:19:53 PM 110.6 -
6/7/2019 1:19:54 PM 110.6 -
6/7/2019 1:19:55 PM 110.6 -
6/7/2019 1:19:56 PM 110.6 -
6/7/2019 1:19:57 PM 110.6 -
6/7/2019 1:19:58 PM 110.6 -
6/7/2019 1:19:59 PM 110.6 -
6/7/2019 1:20:00 PM 110.6 -
6/7/2019 1:20:01 PM 110.5 -
6/7/2019 1:20:02 PM 110.5 -
6/7/2019 1:20:03 PM 110.5 -
6/7/2019 1:20:04 PM 110.5 -
6/7/2019 1:20:05 PM 110.5 -
6/7/2019 1:20:06 PM 110.5 -
6/7/2019 1:20:07 PM 110.5 -
6/7/2019 1:20:08 PM 110.6 -
6/7/2019 1:20:09 PM 110.6 -
6/7/2019 1:20:10 PM 111.2 -
6/7/2019 1:20:11 PM 449.1 338.5
6/7/2019 1:20:12 PM 2476.8 2366.2
6/7/2019 1:20:13 PM 5174.5 5063.9
6/7/2019 1:20:14 PM 7074.2 6963.6
6/7/2019 1:20:15 PM 12451.5 12340.9
6/7/2019 1:20:16 PM 16177.0 16066.4
6/7/2019 1:20:17 PM 21004.6 20894.0
6/7/2019 1:20:18 PM 23476.0 23365.4
6/7/2019 1:20:19 PM 24631.7 24521.1
6/7/2019 1:20:20 PM 25108.0 24997.4
6/7/2019 1:20:21 PM 25045.2 24934.6
6/7/2019 1:20:22 PM 24800.8 24690.2
6/7/2019 1:20:23 PM 22855.0 22744.4
6/7/2019 1:20:24 PM 21212.8 21102.2
6/7/2019 1:20:25 PM 19756.2 19645.6
6/7/2019 1:20:26 PM 18542.5 18431.9
6/7/2019 1:20:27 PM 16384.3 16273.7
6/7/2019 1:20:28 PM 14803.7 14693.1
6/7/2019 1:20:29 PM 13267.4 13156.8
6/7/2019 1:20:30 PM 12464.9 12354.3
6/7/2019 1:20:31 PM 10659.9 10549.3
6/7/2019 1:20:32 PM 9405.6 9295.0
6/7/2019 1:20:33 PM 8222.7 8112.1
6/7/2019 1:20:34 PM 7317.8 7207.2
6/7/2019 1:20:35 PM 6449.9 6339.3
6/7/2019 1:20:36 PM 5863.2 5752.6
6/7/2019 1:20:37 PM 4871.8 4761.2
6/7/2019 1:20:38 PM 4613.4 4502.8
6/7/2019 1:20:39 PM 3753.0 3642.4
6/7/2019 1:20:40 PM 3358.9 3248.3
6/7/2019 1:20:41 PM 2978.3 2867.7
6/7/2019 1:20:42 PM 2679.7 2569.1
6/7/2019 1:20:43 PM 2393.6 2283.0
6/7/2019 1:20:44 PM 2169.4 2058.8
6/7/2019 1:20:45 PM 2053.8 1943.2
6/7/2019 1:20:46 PM 1848.4 1737.8
6/7/2019 1:20:47 PM 1680.3 1569.7
6/7/2019 1:20:48 PM 1563.7 1453.1
6/7/2019 1:20:49 PM 1490.5 1379.9
6/7/2019 1:20:50 PM 1441.3 1330.7
6/7/2019 1:20:51 PM 1256.8 1146.2
6/7/2019 1:20:52 PM 1178.7 1068.1
6/7/2019 1:20:53 PM 1116.6 1006.0
6/7/2019 1:20:54 PM 1090.6 980.0
6/7/2019 1:20:55 PM 992.2 881.6
6/7/2019 1:20:56 PM 942.0 831.4
6/7/2019 1:20:57 PM 905.8 795.2
6/7/2019 1:20:58 PM 872.5 761.9
6/7/2019 1:20:59 PM 858.4 747.8
Table E1 SEEP-A4 TEST-3 Data Log
Page 168 of 452 August 2019
APPENDIX E36: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A4 TEST-3 Data Log
6/7/2019 1:21:00 PM 834.7 724.1
6/7/2019 1:21:01 PM 770.5 659.9
6/7/2019 1:21:02 PM 744.8 634.2
6/7/2019 1:21:03 PM 721.2 610.6
6/7/2019 1:21:04 PM 707.5 596.9
6/7/2019 1:21:05 PM 695.2 584.6
6/7/2019 1:21:06 PM 682.6 572.0
6/7/2019 1:21:07 PM 673.1 562.5
6/7/2019 1:21:08 PM 608.4 497.8
6/7/2019 1:21:09 PM 585.7 475.1
6/7/2019 1:21:10 PM 575.2 464.6
6/7/2019 1:21:11 PM 478.4 367.8
6/7/2019 1:21:12 PM 536.5 425.9
6/7/2019 1:21:13 PM 523.3 412.7
6/7/2019 1:21:14 PM 508.6 398.0
6/7/2019 1:21:15 PM 502.4 391.8
6/7/2019 1:21:16 PM 496.1 385.5
6/7/2019 1:21:17 PM 489.9 379.3
6/7/2019 1:21:18 PM 484.8 374.2
6/7/2019 1:21:19 PM 478.9 368.3
6/7/2019 1:21:20 PM 473.8 363.2
6/7/2019 1:21:21 PM 468.1 357.5
6/7/2019 1:21:22 PM 463.6 353.0
6/7/2019 1:21:23 PM 414.3 303.7
6/7/2019 1:21:24 PM 407.6 297.0
6/7/2019 1:21:25 PM 401.1 290.5
6/7/2019 1:21:26 PM 398.4 287.8
6/7/2019 1:21:27 PM 394.1 283.5
6/7/2019 1:21:28 PM 390.8 280.2
6/7/2019 1:21:29 PM 387.5 276.9
6/7/2019 1:21:30 PM 384.7 274.1
6/7/2019 1:21:31 PM 381.9 271.3
6/7/2019 1:21:32 PM 379.4 268.8
6/7/2019 1:21:33 PM 376.6 266.0
6/7/2019 1:21:34 PM 374.2 263.6
6/7/2019 1:21:35 PM 372.0 261.4
6/7/2019 1:21:36 PM 369.1 258.5
6/7/2019 1:21:37 PM 366.4 255.8
6/7/2019 1:21:38 PM 363.4 252.8
6/7/2019 1:21:39 PM 359.5 248.9
6/7/2019 1:21:40 PM 354.0 243.4
6/7/2019 1:21:41 PM 349.3 238.7
6/7/2019 1:21:42 PM 344.2 233.6
6/7/2019 1:21:43 PM 339.8 229.2
6/7/2019 1:21:44 PM 335.0 224.4
6/7/2019 1:21:45 PM 330.8 220.2
6/7/2019 1:21:46 PM 326.1 215.5
6/7/2019 1:21:47 PM 321.9 211.3
6/7/2019 1:21:48 PM 317.2 206.6
6/7/2019 1:21:49 PM 313.6 203.0
6/7/2019 1:21:50 PM 309.7 199.1
6/7/2019 1:21:51 PM 306.4 195.8
6/7/2019 1:21:52 PM 302.7 192.1
6/7/2019 1:21:53 PM 299.5 188.9
6/7/2019 1:21:54 PM 296.1 185.5
6/7/2019 1:21:55 PM 292.6 182.0
6/7/2019 1:21:56 PM 289.7 179.1
6/7/2019 1:21:57 PM 286.4 175.8
6/7/2019 1:21:58 PM 283.6 173.0
6/7/2019 1:21:59 PM 280.5 169.9
6/7/2019 1:22:00 PM 277.9 167.3
6/7/2019 1:22:01 PM 274.9 164.3
6/7/2019 1:22:02 PM 272.3 161.7
6/7/2019 1:22:03 PM 269.5 158.9
6/7/2019 1:22:04 PM 267.1 156.5
6/7/2019 1:22:05 PM 264.5 153.9
6/7/2019 1:22:06 PM 262.2 151.6
6/7/2019 1:22:07 PM 259.6 149.0
6/7/2019 1:22:08 PM 257.4 146.8
6/7/2019 1:22:09 PM 254.8 144.2
6/7/2019 1:22:10 PM 252.6 142.0
6/7/2019 1:22:11 PM 250.3 139.7
6/7/2019 1:22:12 PM 248.4 137.8
6/7/2019 1:22:13 PM 246.4 135.8
6/7/2019 1:22:14 PM 244.5 133.9
6/7/2019 1:22:15 PM 242.9 132.3
6/7/2019 1:22:16 PM 241.0 130.4
Page 169 of 452 August 2019
APPENDIX E36: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A4 TEST-3 Data Log
6/7/2019 1:22:17 PM 239.3 128.7
6/7/2019 1:22:18 PM 237.4 126.8
6/7/2019 1:22:19 PM 235.7 125.1
6/7/2019 1:22:20 PM 233.9 123.3
6/7/2019 1:22:21 PM 232.3 121.7
6/7/2019 1:22:22 PM 230.5 119.9
6/7/2019 1:22:23 PM 228.9 118.3
6/7/2019 1:22:24 PM 227.0 116.4
6/7/2019 1:22:25 PM 225.3 114.7
6/7/2019 1:22:26 PM 223.4 112.8
6/7/2019 1:22:27 PM 221.9 111.3
6/7/2019 1:22:28 PM 220.2 109.6
6/7/2019 1:22:29 PM 218.9 108.3
6/7/2019 1:22:30 PM 217.3 106.7
6/7/2019 1:22:31 PM 216.0 105.4
6/7/2019 1:22:32 PM 214.6 104.0
6/7/2019 1:22:33 PM 213.5 102.9
6/7/2019 1:22:34 PM 212.2 101.6
6/7/2019 1:22:35 PM 211.0 100.4
6/7/2019 1:22:36 PM 210.0 99.4
6/7/2019 1:22:37 PM 208.9 98.3
6/7/2019 1:22:38 PM 208.0 97.4
6/7/2019 1:22:39 PM 207.0 96.4
6/7/2019 1:22:40 PM 206.1 95.5
6/7/2019 1:22:41 PM 205.1 94.5
6/7/2019 1:22:42 PM 204.1 93.5
6/7/2019 1:22:43 PM 203.0 92.4
6/7/2019 1:22:44 PM 202.1 91.5
6/7/2019 1:22:45 PM 201.1 90.5
6/7/2019 1:22:46 PM 200.3 89.7
6/7/2019 1:22:47 PM 199.4 88.8
6/7/2019 1:22:48 PM 198.6 88.0
6/7/2019 1:22:49 PM 197.6 87.0
6/7/2019 1:22:50 PM 196.7 86.1
6/7/2019 1:22:51 PM 195.7 85.1
6/7/2019 1:22:52 PM 194.8 84.2
6/7/2019 1:22:53 PM 193.7 83.1
6/7/2019 1:22:54 PM 192.8 82.2
6/7/2019 1:22:55 PM 191.8 81.2
6/7/2019 1:22:56 PM 191.0 80.4
6/7/2019 1:22:57 PM 190.2 79.6
6/7/2019 1:22:58 PM 189.3 78.7
6/7/2019 1:22:59 PM 188.5 77.9
6/7/2019 1:23:00 PM 187.7 77.1
6/7/2019 1:23:01 PM 187.0 76.4
6/7/2019 1:23:02 PM 186.3 75.7
6/7/2019 1:23:03 PM 185.7 75.1
6/7/2019 1:23:04 PM 185.1 74.5
6/7/2019 1:23:05 PM 184.5 73.9
6/7/2019 1:23:06 PM 184.0 73.4
6/7/2019 1:23:07 PM 183.5 72.9
6/7/2019 1:23:08 PM 182.9 72.3
6/7/2019 1:23:09 PM 182.4 71.8
6/7/2019 1:23:10 PM 181.9 71.3
6/7/2019 1:23:11 PM 181.4 70.8
6/7/2019 1:23:12 PM 180.8 70.2
6/7/2019 1:23:13 PM 180.4 69.8
6/7/2019 1:23:14 PM 179.9 69.3
6/7/2019 1:23:15 PM 179.5 68.9
6/7/2019 1:23:16 PM 179.0 68.4
6/7/2019 1:23:17 PM 178.5 67.9
6/7/2019 1:23:18 PM 178.0 67.4
6/7/2019 1:23:19 PM 177.4 66.8
6/7/2019 1:23:20 PM 176.7 66.1
6/7/2019 1:23:21 PM 176.0 65.4
6/7/2019 1:23:22 PM 175.2 64.6
6/7/2019 1:23:23 PM 174.4 63.8
6/7/2019 1:23:24 PM 173.6 63.0
6/7/2019 1:23:25 PM 172.8 62.2
6/7/2019 1:23:26 PM 172.0 61.4
6/7/2019 1:23:27 PM 171.2 60.6
6/7/2019 1:23:28 PM 170.4 59.8
6/7/2019 1:23:29 PM 169.5 58.9
6/7/2019 1:23:30 PM 168.8 58.2
6/7/2019 1:23:31 PM 168.1 57.5
6/7/2019 1:23:32 PM 167.5 56.9
6/7/2019 1:23:33 PM 166.9 56.3
6/7/2019 1:23:34 PM 166.5 55.9
6/7/2019 1:23:35 PM 166.1 55.5
Page 170 of 452 August 2019
APPENDIX E36: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A4 TEST-3 Data Log
6/7/2019 1:23:36 PM 165.8 55.2
6/7/2019 1:23:37 PM 165.5 54.9
6/7/2019 1:23:38 PM 165.3 54.7
6/7/2019 1:23:39 PM 165.2 54.6
6/7/2019 1:23:40 PM 165.0 54.4
6/7/2019 1:23:41 PM 165.0 54.4
6/7/2019 1:23:42 PM 165.0 54.4
6/7/2019 1:23:43 PM 165.0 54.4
6/7/2019 1:23:44 PM 165.0 54.4
6/7/2019 1:23:45 PM 165.1 54.5
6/7/2019 1:23:46 PM 165.2 54.6
6/7/2019 1:23:47 PM 165.2 54.6
6/7/2019 1:23:48 PM 165.3 54.7
6/7/2019 1:23:49 PM 165.3 54.7
6/7/2019 1:23:50 PM 165.2 54.6
6/7/2019 1:23:51 PM 165.2 54.6
6/7/2019 1:23:52 PM 165.1 54.5
6/7/2019 1:23:53 PM 165.0 54.4
6/7/2019 1:23:54 PM 164.8 54.2
6/7/2019 1:23:55 PM 164.5 53.9
6/7/2019 1:23:56 PM 164.2 53.6
6/7/2019 1:23:57 PM 163.9 53.3
6/7/2019 1:23:58 PM 163.6 53.0
6/7/2019 1:23:59 PM 163.2 52.6
6/7/2019 1:24:00 PM 162.8 52.2
6/7/2019 1:24:01 PM 162.5 51.9
6/7/2019 1:24:02 PM 162.1 51.5
6/7/2019 1:24:03 PM 161.6 51.0
6/7/2019 1:24:04 PM 161.2 50.6
6/7/2019 1:24:05 PM 160.6 50.0
6/7/2019 1:24:06 PM 160.1 49.5
6/7/2019 1:24:07 PM 159.6 49.0
6/7/2019 1:24:08 PM 159.1 48.5
6/7/2019 1:24:09 PM 158.6 48.0
6/7/2019 1:24:10 PM 158.2 47.6
6/7/2019 1:24:11 PM 157.6 47.0
6/7/2019 1:24:12 PM 157.2 46.6
6/7/2019 1:24:13 PM 156.7 46.1
6/7/2019 1:24:14 PM 156.3 45.7
6/7/2019 1:24:15 PM 155.9 45.3
6/7/2019 1:24:16 PM 155.6 45.0
6/7/2019 1:24:17 PM 155.3 44.7
6/7/2019 1:24:18 PM 155.0 44.4
6/7/2019 1:24:19 PM 154.9 44.3
6/7/2019 1:24:20 PM 154.7 44.1
6/7/2019 1:24:21 PM 154.7 44.1
6/7/2019 1:24:22 PM 154.7 44.1
6/7/2019 1:24:23 PM 154.7 44.1
6/7/2019 1:24:24 PM 154.8 44.2
6/7/2019 1:24:25 PM 155.1 44.5
6/7/2019 1:24:26 PM 155.4 44.8
6/7/2019 1:24:27 PM 155.8 45.2
6/7/2019 1:24:28 PM 156.3 45.7
6/7/2019 1:24:29 PM 156.7 46.1
6/7/2019 1:24:30 PM 157.1 46.5
6/7/2019 1:24:31 PM 157.4 46.8
6/7/2019 1:24:32 PM 157.6 47.0
6/7/2019 1:24:33 PM 157.7 47.1
6/7/2019 1:24:34 PM 157.7 47.1
6/7/2019 1:24:35 PM 157.7 47.1
6/7/2019 1:24:36 PM 157.5 46.9
6/7/2019 1:24:37 PM 157.4 46.8
6/7/2019 1:24:38 PM 157.1 46.5
6/7/2019 1:24:39 PM 156.8 46.2
6/7/2019 1:24:40 PM 156.6 46.0
6/7/2019 1:24:41 PM 156.3 45.7
6/7/2019 1:24:42 PM 156.2 45.6
6/7/2019 1:24:43 PM 156.0 45.4
6/7/2019 1:24:44 PM 155.9 45.3
6/7/2019 1:24:45 PM 155.8 45.2
6/7/2019 1:24:46 PM 155.7 45.1
6/7/2019 1:24:47 PM 155.6 45.0
6/7/2019 1:24:48 PM 155.5 44.9
6/7/2019 1:24:49 PM 155.4 44.8
6/7/2019 1:24:50 PM 155.3 44.7
6/7/2019 1:24:51 PM 155.0 44.4
6/7/2019 1:24:52 PM 154.8 44.2
6/7/2019 1:24:53 PM 154.3 43.7
6/7/2019 1:24:54 PM 153.9 43.3
Page 171 of 452 August 2019
APPENDIX E36: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A4 TEST-3 Data Log
6/7/2019 1:24:55 PM 153.2 42.6
6/7/2019 1:24:56 PM 152.6 42.0
6/7/2019 1:24:57 PM 151.9 41.3
6/7/2019 1:24:58 PM 151.3 40.7
6/7/2019 1:24:59 PM 150.6 40.0
6/7/2019 1:25:00 PM 149.9 39.3
6/7/2019 1:25:01 PM 149.4 38.8
6/7/2019 1:25:02 PM 148.8 38.2
6/7/2019 1:25:03 PM 148.3 37.7
6/7/2019 1:25:04 PM 147.8 37.2
6/7/2019 1:25:05 PM 147.3 36.7
6/7/2019 1:25:06 PM 146.8 36.2
6/7/2019 1:25:07 PM 146.4 35.8
6/7/2019 1:25:08 PM 145.9 35.3
6/7/2019 1:25:09 PM 145.6 35.0
6/7/2019 1:25:10 PM 145.3 34.7
6/7/2019 1:25:11 PM 145.1 34.5
6/7/2019 1:25:12 PM 144.9 34.3
6/7/2019 1:25:13 PM 144.8 34.2
6/7/2019 1:25:14 PM 144.8 34.2
6/7/2019 1:25:15 PM 144.7 34.1
6/7/2019 1:25:16 PM 144.6 34.0
6/7/2019 1:25:17 PM 144.5 33.9
6/7/2019 1:25:18 PM 144.4 33.8
6/7/2019 1:25:19 PM 144.4 33.8
6/7/2019 1:25:20 PM 144.3 33.7
6/7/2019 1:25:21 PM 144.3 33.7
6/7/2019 1:25:22 PM 144.3 33.7
6/7/2019 1:25:23 PM 144.2 33.6
6/7/2019 1:25:24 PM 144.2 33.6
6/7/2019 1:25:25 PM 144.2 33.6
6/7/2019 1:25:26 PM 144.2 33.6
6/7/2019 1:25:27 PM 144.2 33.6
6/7/2019 1:25:28 PM 144.2 33.6
6/7/2019 1:25:29 PM 144.3 33.7
6/7/2019 1:25:30 PM 144.4 33.8
6/7/2019 1:25:31 PM 144.5 33.9
6/7/2019 1:25:32 PM 144.7 34.1
6/7/2019 1:25:33 PM 144.9 34.3
6/7/2019 1:25:34 PM 145.1 34.5
6/7/2019 1:25:35 PM 145.2 34.6
6/7/2019 1:25:36 PM 145.3 34.7
6/7/2019 1:25:37 PM 145.3 34.7
6/7/2019 1:25:38 PM 145.3 34.7
6/7/2019 1:25:39 PM 145.3 34.7
6/7/2019 1:25:40 PM 145.2 34.6
6/7/2019 1:25:41 PM 145.1 34.5
6/7/2019 1:25:42 PM 145.0 34.4
6/7/2019 1:25:43 PM 144.9 34.3
6/7/2019 1:25:44 PM 144.7 34.1
6/7/2019 1:25:45 PM 144.4 33.8
6/7/2019 1:25:46 PM 144.2 33.6
6/7/2019 1:25:47 PM 143.9 33.3
6/7/2019 1:25:48 PM 143.6 33.0
6/7/2019 1:25:49 PM 143.4 32.8
6/7/2019 1:25:50 PM 143.1 32.5
6/7/2019 1:25:51 PM 143.0 32.4
6/7/2019 1:25:52 PM 142.8 32.2
6/7/2019 1:25:53 PM 142.7 32.1
6/7/2019 1:25:54 PM 142.6 32.0
6/7/2019 1:25:55 PM 142.5 31.9
6/7/2019 1:25:56 PM 142.4 31.8
6/7/2019 1:25:57 PM 142.2 31.6
6/7/2019 1:25:58 PM 142.1 31.5
6/7/2019 1:25:59 PM 142.0 31.4
6/7/2019 1:26:00 PM 141.9 31.3
6/7/2019 1:26:01 PM 141.7 31.1
6/7/2019 1:26:02 PM 141.6 31.0
6/7/2019 1:26:03 PM 141.5 30.9
6/7/2019 1:26:04 PM 141.4 30.8
6/7/2019 1:26:05 PM 141.2 30.6
6/7/2019 1:26:06 PM 141.1 30.5
6/7/2019 1:26:07 PM 140.9 30.3
6/7/2019 1:26:08 PM 140.8 30.2
6/7/2019 1:26:09 PM 140.7 30.1
6/7/2019 1:26:10 PM 140.6 30.0
6/7/2019 1:26:11 PM 140.6 30.0
6/7/2019 1:26:12 PM 140.6 30.0
6/7/2019 1:26:13 PM 140.6 30.0
Page 172 of 452 August 2019
APPENDIX E36: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A4 TEST-3 Data Log
6/7/2019 1:26:14 PM 140.6 30.0
6/7/2019 1:26:15 PM 140.7 30.1
6/7/2019 1:26:16 PM 140.8 30.2
6/7/2019 1:26:17 PM 140.9 30.3
6/7/2019 1:26:18 PM 141.0 30.4
6/7/2019 1:26:19 PM 141.1 30.5
6/7/2019 1:26:20 PM 141.2 30.6
6/7/2019 1:26:21 PM 141.2 30.6
6/7/2019 1:26:22 PM 141.2 30.6
6/7/2019 1:26:23 PM 141.2 30.6
6/7/2019 1:26:24 PM 141.1 30.5
6/7/2019 1:26:25 PM 141.2 30.6
6/7/2019 1:26:26 PM 141.2 30.6
6/7/2019 1:26:27 PM 141.3 30.7
6/7/2019 1:26:28 PM 141.4 30.8
6/7/2019 1:26:29 PM 141.4 30.8
6/7/2019 1:26:30 PM 141.4 30.8
6/7/2019 1:26:31 PM 141.4 30.8
6/7/2019 1:26:32 PM 141.3 30.7
6/7/2019 1:26:33 PM 141.3 30.7
6/7/2019 1:26:34 PM 141.2 30.6
6/7/2019 1:26:35 PM 141.2 30.6
6/7/2019 1:26:36 PM 141.3 30.7
6/7/2019 1:26:37 PM 141.3 30.7
6/7/2019 1:26:38 PM 141.3 30.7
6/7/2019 1:26:39 PM 141.2 30.6
6/7/2019 1:26:40 PM 141.1 30.5
6/7/2019 1:26:41 PM 140.9 30.3
6/7/2019 1:26:42 PM 140.8 30.2
6/7/2019 1:26:43 PM 140.6 30.0
6/7/2019 1:26:44 PM 140.6 30.0
6/7/2019 1:26:45 PM 140.5 29.9
6/7/2019 1:26:46 PM 140.5 29.9
6/7/2019 1:26:47 PM 140.5 29.9
6/7/2019 1:26:48 PM 140.5 29.9
6/7/2019 1:26:49 PM 140.5 29.9
6/7/2019 1:26:50 PM 140.5 29.9
6/7/2019 1:26:51 PM 140.5 29.9
6/7/2019 1:26:52 PM 140.6 30.0
6/7/2019 1:26:53 PM 140.7 30.1
6/7/2019 1:26:54 PM 140.7 30.1
6/7/2019 1:26:55 PM 140.8 30.2
6/7/2019 1:26:56 PM 140.9 30.3
6/7/2019 1:26:57 PM 141.0 30.4
6/7/2019 1:26:58 PM 141.1 30.5
6/7/2019 1:26:59 PM 141.2 30.6
6/7/2019 1:27:00 PM 141.3 30.7
6/7/2019 1:27:01 PM 141.5 30.9
6/7/2019 1:27:02 PM 141.6 31.0
6/7/2019 1:27:03 PM 141.8 31.2
6/7/2019 1:27:04 PM 142.0 31.4
6/7/2019 1:27:05 PM 142.2 31.6
6/7/2019 1:27:06 PM 142.5 31.9
6/7/2019 1:27:07 PM 142.6 32.0
6/7/2019 1:27:08 PM 142.8 32.2
6/7/2019 1:27:09 PM 143.0 32.4
6/7/2019 1:27:10 PM 143.1 32.5
6/7/2019 1:27:11 PM 143.2 32.6
6/7/2019 1:27:12 PM 143.2 32.6
6/7/2019 1:27:13 PM 143.3 32.7
6/7/2019 1:27:14 PM 143.3 32.7
6/7/2019 1:27:15 PM 143.3 32.7
6/7/2019 1:27:16 PM 143.3 32.7
6/7/2019 1:27:17 PM 143.2 32.6
6/7/2019 1:27:18 PM 143.1 32.5
6/7/2019 1:27:19 PM 143.1 32.5
6/7/2019 1:27:20 PM 142.9 32.3
6/7/2019 1:27:21 PM 142.9 32.3
6/7/2019 1:27:22 PM 142.8 32.2
6/7/2019 1:27:23 PM 142.7 32.1
6/7/2019 1:27:24 PM 142.6 32.0
6/7/2019 1:27:25 PM 142.5 31.9
6/7/2019 1:27:26 PM 142.5 31.9
6/7/2019 1:27:27 PM 142.4 31.8
6/7/2019 1:27:28 PM 142.4 31.8
6/7/2019 1:27:29 PM 142.4 31.8
6/7/2019 1:27:30 PM 142.4 31.8
6/7/2019 1:27:31 PM 142.4 31.8
6/7/2019 1:27:32 PM 142.4 31.8
Page 173 of 452 August 2019
APPENDIX E36: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-A4 TEST-3 Data Log
6/7/2019 1:27:33 PM 142.5 31.9
6/7/2019 1:27:34 PM 142.5 31.9
6/7/2019 1:27:35 PM 142.5 31.9
6/7/2019 1:27:36 PM 142.5 31.9
6/7/2019 1:27:37 PM 142.4 31.8
6/7/2019 1:27:38 PM 142.3 31.7
6/7/2019 1:27:39 PM 142.2 31.6
6/7/2019 1:27:40 PM 142.0 31.4
6/7/2019 1:27:41 PM 141.8 31.2
6/7/2019 1:27:42 PM 141.5 30.9
6/7/2019 1:27:43 PM 141.2 30.6
6/7/2019 1:27:44 PM 141.0 30.4
6/7/2019 1:27:45 PM 140.8 30.2
6/7/2019 1:27:46 PM 140.6 30.0
6/7/2019 1:27:47 PM 140.5 29.9
6/7/2019 1:27:48 PM 140.5 29.9
6/7/2019 1:27:49 PM 140.5 29.9
6/7/2019 1:27:50 PM 140.6 30.0
6/7/2019 1:27:51 PM 140.7 30.1
6/7/2019 1:27:52 PM 140.7 30.1
6/7/2019 1:27:53 PM 140.9 30.3
6/7/2019 1:27:54 PM 141.0 30.4
6/7/2019 1:27:55 PM 141.2 30.6
6/7/2019 1:27:56 PM 141.4 30.8
6/7/2019 1:27:57 PM 141.6 31.0
6/7/2019 1:27:58 PM 141.8 31.2
6/7/2019 1:27:59 PM 142.0 31.4
6/7/2019 1:28:00 PM 142.1 31.5
6/7/2019 1:28:01 PM 142.2 31.6
6/7/2019 1:28:02 PM 142.3 31.7
6/7/2019 1:28:03 PM 142.5 31.9
6/7/2019 1:28:04 PM 142.7 32.1
6/7/2019 1:28:05 PM 143.1 32.5
6/7/2019 1:28:06 PM 143.4 32.8
6/7/2019 1:28:07 PM 143.8 33.2
6/7/2019 1:28:08 PM 144.1 33.5
6/7/2019 1:28:09 PM 144.4 33.8
6/7/2019 1:28:10 PM 144.7 34.1
6/7/2019 1:28:11 PM 145.0 34.4
6/7/2019 1:28:12 PM 145.3 34.7
6/7/2019 1:28:13 PM 145.6 35.0
6/7/2019 1:28:14 PM 145.9 35.3
6/7/2019 1:28:15 PM 146.3 35.7
6/7/2019 1:28:16 PM 146.6 36.0
Page 174 of 452 August 2019
APPENDIX E36: SALT DILUTION GAUGING SUMMARY
SEEP-A4 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-A4 TEST-3 1221
SEEP-A4 TEST-3 1222
SEEP-A4 TEST-3 1223
SEEP-A4 TEST-3 1224
Location EC Reading
(µS/cms)
SEEP-A4 TEST-3 243.7
SEEP-A4 TEST-3 2,163
SEEP-A4 TEST-3 18,130
SEEP-A4 TEST-3 133,511
q 149,800
K 1.3399
0.4
7.0
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Calculated Flow Rate Q
L/s
GPM
455,011.3 (s) . (µS/cms)
1,000 24.2
10000 24.1
100,000 24.1
Table E4 SEEP-A4 TEST-3 Flow Calculation Summary
Mass of Salt injected mg
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
100 24.2
Average (pre-test)110.6 (µS/cms)
Table E3 SEEP-A4 TEST-3 YSI Salt Dilution Calibration Data
Calibration Temperature
(mg/L)(°C)
Average (post-test)142.6 (µS/cms)
Integral of Conductivity
Data Curve
SUM:Δt(E
Ct-ECbkg)
Slope of Calibration Curve (µS/cms) / (mg/L)
108.6 21.8
Average 108.6
Geo Mean 108.6 (µS/cms)
(µS/cms)
108.8 21.8
109.2 21.6
107.8 21.8
(µS/cms)(°C)
Table E2 SEEP-A4 TEST-3 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 175 of 452 August 2019
APPENDIX E37: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/5/2019 1:35:24 PM 112.4 -
2/5/2019 1:35:25 PM 112.3 -
2/5/2019 1:35:26 PM 112.3 -
2/5/2019 1:35:27 PM 112.2 -
2/5/2019 1:35:28 PM 112.2 -
2/5/2019 1:35:29 PM 112.1 -
2/5/2019 1:35:30 PM 112.1 -
2/5/2019 1:35:31 PM 112.0 -
2/5/2019 1:35:32 PM 111.9 -
2/5/2019 1:35:33 PM 111.8 -
2/5/2019 1:35:34 PM 111.8 -
2/5/2019 1:35:35 PM 111.7 -
2/5/2019 1:35:36 PM 111.6 -
2/5/2019 1:35:37 PM 111.6 -
2/5/2019 1:35:38 PM 111.6 -
2/5/2019 1:35:39 PM 111.5 -
2/5/2019 1:35:40 PM 111.5 -
2/5/2019 1:35:41 PM 111.4 -
2/5/2019 1:35:42 PM 111.4 -
2/5/2019 1:35:43 PM 111.3 -
2/5/2019 1:35:44 PM 111.3 -
2/5/2019 1:35:45 PM 111.2 -
2/5/2019 1:35:46 PM 111.2 -
2/5/2019 1:35:47 PM 111.1 -
2/5/2019 1:35:48 PM 111.1 -
2/5/2019 1:35:49 PM 111.0 -
2/5/2019 1:35:50 PM 111.0 -
2/5/2019 1:35:51 PM 110.9 -
2/5/2019 1:35:52 PM 110.8 -
2/5/2019 1:35:53 PM 110.8 -
2/5/2019 1:35:54 PM 110.7 -
2/5/2019 1:35:55 PM 110.7 -
2/5/2019 1:35:56 PM 110.6 -
2/5/2019 1:35:57 PM 110.6 -
2/5/2019 1:35:58 PM 110.6 -
2/5/2019 1:35:59 PM 110.5 -
2/5/2019 1:36:00 PM 110.5 -
2/5/2019 1:36:01 PM 110.4 -
2/5/2019 1:36:02 PM 110.4 -
2/5/2019 1:36:03 PM 110.4 -
2/5/2019 1:36:04 PM 110.4 -
2/5/2019 1:36:05 PM 110.6 -
2/5/2019 1:36:06 PM 111.3 -
2/5/2019 1:36:07 PM 113.0 1.7
2/5/2019 1:36:08 PM 182.5 71.2
2/5/2019 1:36:09 PM 243.0 131.7
2/5/2019 1:36:10 PM 389.8 278.5
2/5/2019 1:36:11 PM 499.9 388.6
2/5/2019 1:36:12 PM 622.6 511.3
2/5/2019 1:36:13 PM 702.1 590.8
2/5/2019 1:36:14 PM 1040.7 929.4
2/5/2019 1:36:15 PM 1027.8 916.5
2/5/2019 1:36:16 PM 1420.7 1309.4
2/5/2019 1:36:17 PM 1531.8 1420.5
2/5/2019 1:36:18 PM 1689.5 1578.2
2/5/2019 1:36:19 PM 1725.0 1613.7
2/5/2019 1:36:20 PM 1792.2 1680.9
2/5/2019 1:36:21 PM 1979.8 1868.5
2/5/2019 1:36:22 PM 2022.2 1910.9
2/5/2019 1:36:23 PM 2018.6 1907.3
2/5/2019 1:36:24 PM 2016.1 1904.8
2/5/2019 1:36:25 PM 2004.2 1892.9
2/5/2019 1:36:26 PM 1989.4 1878.1
2/5/2019 1:36:27 PM 1969.2 1857.9
2/5/2019 1:36:28 PM 1825.2 1713.9
2/5/2019 1:36:29 PM 1781.2 1669.9
2/5/2019 1:36:30 PM 1721.0 1609.7
2/5/2019 1:36:31 PM 1685.7 1574.4
2/5/2019 1:36:32 PM 1636.6 1525.3
2/5/2019 1:36:33 PM 1601.5 1490.2
Table E1 SEEP-B1 TEST-1 Data Log
Page 176 of 452 August 2019
APPENDIX E37: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B1 TEST-1 Data Log
2/5/2019 1:36:34 PM 1459.6 1348.3
2/5/2019 1:36:35 PM 1373.1 1261.8
2/5/2019 1:36:36 PM 1316.7 1205.4
2/5/2019 1:36:37 PM 1291.2 1179.9
2/5/2019 1:36:38 PM 1184.0 1072.7
2/5/2019 1:36:39 PM 1142.8 1031.5
2/5/2019 1:36:40 PM 1082.5 971.2
2/5/2019 1:36:41 PM 1040.7 929.4
2/5/2019 1:36:42 PM 1024.7 913.4
2/5/2019 1:36:43 PM 937.1 825.8
2/5/2019 1:36:44 PM 893.4 782.1
2/5/2019 1:36:45 PM 853.0 741.7
2/5/2019 1:36:46 PM 826.4 715.1
2/5/2019 1:36:47 PM 787.7 676.4
2/5/2019 1:36:48 PM 717.3 606.0
2/5/2019 1:36:49 PM 669.4 558.1
2/5/2019 1:36:50 PM 644.9 533.6
2/5/2019 1:36:51 PM 614.7 503.4
2/5/2019 1:36:52 PM 561.1 449.8
2/5/2019 1:36:53 PM 547.7 436.4
2/5/2019 1:36:54 PM 527.5 416.2
2/5/2019 1:36:55 PM 503.8 392.5
2/5/2019 1:36:56 PM 496.5 385.2
2/5/2019 1:36:57 PM 486.7 375.4
2/5/2019 1:36:58 PM 476.3 365.0
2/5/2019 1:36:59 PM 419.1 307.8
2/5/2019 1:37:00 PM 399.7 288.4
2/5/2019 1:37:01 PM 379.2 267.9
2/5/2019 1:37:02 PM 367.5 256.2
2/5/2019 1:37:03 PM 360.3 249.0
2/5/2019 1:37:04 PM 351.0 239.7
2/5/2019 1:37:05 PM 342.1 230.8
2/5/2019 1:37:06 PM 334.6 223.3
2/5/2019 1:37:07 PM 328.3 217.0
2/5/2019 1:37:08 PM 321.2 209.9
2/5/2019 1:37:09 PM 315.5 204.2
2/5/2019 1:37:10 PM 262.6 151.3
2/5/2019 1:37:11 PM 256.1 144.8
2/5/2019 1:37:12 PM 245.6 134.3
2/5/2019 1:37:13 PM 242.8 131.5
2/5/2019 1:37:14 PM 237.7 126.4
2/5/2019 1:37:15 PM 232.7 121.4
2/5/2019 1:37:16 PM 228.2 116.9
2/5/2019 1:37:17 PM 225.1 113.8
2/5/2019 1:37:18 PM 221.6 110.3
2/5/2019 1:37:19 PM 218.7 107.4
2/5/2019 1:37:20 PM 215.7 104.4
2/5/2019 1:37:21 PM 213.1 101.8
2/5/2019 1:37:22 PM 210.3 99.0
2/5/2019 1:37:23 PM 208.0 96.7
2/5/2019 1:37:24 PM 205.5 94.2
2/5/2019 1:37:25 PM 203.4 92.1
2/5/2019 1:37:26 PM 199.0 87.7
2/5/2019 1:37:27 PM 194.4 83.1
2/5/2019 1:37:28 PM 189.8 78.5
2/5/2019 1:37:29 PM 186.0 74.7
2/5/2019 1:37:30 PM 181.7 70.4
2/5/2019 1:37:31 PM 178.1 66.8
2/5/2019 1:37:32 PM 174.4 63.1
2/5/2019 1:37:33 PM 171.3 60.0
2/5/2019 1:37:34 PM 168.0 56.7
2/5/2019 1:37:35 PM 165.3 54.0
2/5/2019 1:37:36 PM 162.4 51.1
2/5/2019 1:37:37 PM 159.9 48.6
2/5/2019 1:37:38 PM 157.2 45.9
2/5/2019 1:37:39 PM 154.9 43.6
2/5/2019 1:37:40 PM 152.6 41.3
2/5/2019 1:37:41 PM 150.6 39.3
2/5/2019 1:37:42 PM 148.6 37.3
2/5/2019 1:37:43 PM 147.0 35.7
2/5/2019 1:37:44 PM 145.2 33.9
2/5/2019 1:37:45 PM 143.8 32.5
2/5/2019 1:37:46 PM 142.2 30.9
2/5/2019 1:37:47 PM 140.9 29.6
2/5/2019 1:37:48 PM 139.5 28.2
2/5/2019 1:37:49 PM 138.3 27.0
2/5/2019 1:37:50 PM 137.1 25.8
Page 177 of 452 August 2019
APPENDIX E37: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B1 TEST-1 Data Log
2/5/2019 1:37:51 PM 135.9 24.6
2/5/2019 1:37:52 PM 134.9 23.6
2/5/2019 1:37:53 PM 133.9 22.6
2/5/2019 1:37:54 PM 133.0 21.7
2/5/2019 1:37:55 PM 132.0 20.7
2/5/2019 1:37:56 PM 131.2 19.9
2/5/2019 1:37:57 PM 130.3 19.0
2/5/2019 1:37:58 PM 129.6 18.3
2/5/2019 1:37:59 PM 128.8 17.5
2/5/2019 1:38:00 PM 128.1 16.8
2/5/2019 1:38:01 PM 127.4 16.1
2/5/2019 1:38:02 PM 126.8 15.5
2/5/2019 1:38:03 PM 126.1 14.8
2/5/2019 1:38:04 PM 125.6 14.3
2/5/2019 1:38:05 PM 124.9 13.6
2/5/2019 1:38:06 PM 124.4 13.1
2/5/2019 1:38:07 PM 123.8 12.5
2/5/2019 1:38:08 PM 123.3 12.0
2/5/2019 1:38:09 PM 122.8 11.5
2/5/2019 1:38:10 PM 122.4 11.1
2/5/2019 1:38:11 PM 121.9 10.6
2/5/2019 1:38:12 PM 121.5 10.2
2/5/2019 1:38:13 PM 121.1 9.8
2/5/2019 1:38:14 PM 120.8 9.5
2/5/2019 1:38:15 PM 120.4 9.1
2/5/2019 1:38:16 PM 120.1 8.8
2/5/2019 1:38:17 PM 119.7 8.4
2/5/2019 1:38:18 PM 119.4 8.1
2/5/2019 1:38:19 PM 119.1 7.8
2/5/2019 1:38:20 PM 118.8 7.5
2/5/2019 1:38:21 PM 118.5 7.2
2/5/2019 1:38:22 PM 118.2 6.9
2/5/2019 1:38:23 PM 117.9 6.6
2/5/2019 1:38:24 PM 117.7 6.4
2/5/2019 1:38:25 PM 117.4 6.1
2/5/2019 1:38:26 PM 117.2 5.9
2/5/2019 1:38:27 PM 117.0 5.7
2/5/2019 1:38:28 PM 116.8 5.5
2/5/2019 1:38:29 PM 116.5 5.2
2/5/2019 1:38:30 PM 116.3 5.0
2/5/2019 1:38:31 PM 116.1 4.8
2/5/2019 1:38:32 PM 115.8 4.5
2/5/2019 1:38:33 PM 115.7 4.4
2/5/2019 1:38:34 PM 115.5 4.2
2/5/2019 1:38:35 PM 115.3 4.0
2/5/2019 1:38:36 PM 115.1 3.8
2/5/2019 1:38:37 PM 115.0 3.7
2/5/2019 1:38:38 PM 114.7 3.4
2/5/2019 1:38:39 PM 114.5 3.2
2/5/2019 1:38:40 PM 114.4 3.1
2/5/2019 1:38:41 PM 114.2 2.9
2/5/2019 1:38:42 PM 114.1 2.8
2/5/2019 1:38:43 PM 114.0 2.7
2/5/2019 1:38:44 PM 113.8 2.5
2/5/2019 1:38:45 PM 113.7 2.4
2/5/2019 1:38:46 PM 113.5 2.2
2/5/2019 1:38:47 PM 113.4 2.1
2/5/2019 1:38:48 PM 113.3 2.0
2/5/2019 1:38:49 PM 113.2 1.9
2/5/2019 1:38:50 PM 113.1 1.8
2/5/2019 1:38:51 PM 113.0 1.7
2/5/2019 1:38:52 PM 112.9 1.6
2/5/2019 1:38:53 PM 112.7 1.4
2/5/2019 1:38:54 PM 112.6 1.3
2/5/2019 1:38:55 PM 112.5 1.2
2/5/2019 1:38:56 PM 112.4 1.1
2/5/2019 1:38:57 PM 112.3 1.0
2/5/2019 1:38:58 PM 112.2 0.9
2/5/2019 1:38:59 PM 112.2 0.9
2/5/2019 1:39:00 PM 112.1 0.8
2/5/2019 1:39:01 PM 112.0 -
2/5/2019 1:39:02 PM 111.9 -
2/5/2019 1:39:03 PM 111.8 -
2/5/2019 1:39:04 PM 111.7 -
2/5/2019 1:39:05 PM 111.6 -
2/5/2019 1:39:06 PM 111.5 -
2/5/2019 1:39:07 PM 111.5 -
2/5/2019 1:39:08 PM 111.4 -
2/5/2019 1:39:09 PM 111.3 -
Page 178 of 452 August 2019
APPENDIX E37: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B1 TEST-1 Data Log
2/5/2019 1:39:10 PM 111.2 -
2/5/2019 1:39:11 PM 111.2 -
2/5/2019 1:39:12 PM 111.1 -
2/5/2019 1:39:13 PM 111.0 -
2/5/2019 1:39:14 PM 111.0 -
2/5/2019 1:39:15 PM 110.9 -
2/5/2019 1:39:16 PM 110.9 -
2/5/2019 1:39:17 PM 110.8 -
2/5/2019 1:39:18 PM 110.7 -
2/5/2019 1:39:19 PM 110.7 -
2/5/2019 1:39:20 PM 110.6 -
2/5/2019 1:39:21 PM 110.6 -
2/5/2019 1:39:22 PM 110.5 -
2/5/2019 1:39:23 PM 110.4 -
2/5/2019 1:39:24 PM 110.4 -
2/5/2019 1:39:25 PM 110.3 -
Page 179 of 452 August 2019
APPENDIX E37: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-B2 TEST-1 1259
SEEP-B2 TEST-1 1301
SEEP-B2 TEST-1 1306
SEEP-B2 TEST-1 1307
Location EC Reading
(µS/cms)
SEEP-B2 TEST-1 49.5
SEEP-B2 TEST-1 194
SEEP-B2 TEST-1 14,050
SEEP-B2 TEST-1 109,408
q 300,100
K 1.0972
5.6
88.2
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms) (°C)
Table E2 SEEP-B1 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
106.3 16
105.9 16
107.8 16
106.1 15.7
Average 106.5
Geo Mean 106.5 (µS/cms)
10 21.8
Average (pre-test)111.3 (µS/cms)
Average (post-test)111.1 (µS/cms)
Table E3 SEEP-B1 TEST-1 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
(mg/L)(°C)
Integral of Conductivity Data Curve SUM:Δt(ECt-
ECbkg)59,257.0 (s) . (µS/cms)
100 22.2
1,000 21.8
10,000 21.7
Table E4 SEEP-B1 TEST-1 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Calculated Flow Rate Q L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement Part
2: Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol. 8, no. 1,
2004, pp. 11–15.
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 180 of 452 August 2019
APPENDIX E38: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/5/2019 1:52:29 PM 106.8 -
2/5/2019 1:52:30 PM 106.8 -
2/5/2019 1:52:31 PM 106.8 -
2/5/2019 1:52:32 PM 106.7 -
2/5/2019 1:52:33 PM 106.7 -
2/5/2019 1:52:34 PM 106.7 -
2/5/2019 1:52:35 PM 106.7 -
2/5/2019 1:52:36 PM 106.7 -
2/5/2019 1:52:37 PM 106.7 -
2/5/2019 1:52:38 PM 106.7 -
2/5/2019 1:52:39 PM 106.7 -
2/5/2019 1:52:40 PM 106.7 -
2/5/2019 1:52:41 PM 106.7 -
2/5/2019 1:52:42 PM 106.8 -
2/5/2019 1:52:43 PM 106.8 -
2/5/2019 1:52:44 PM 106.9 -
2/5/2019 1:52:45 PM 107.0 -
2/5/2019 1:52:46 PM 107.0 -
2/5/2019 1:52:47 PM 107.1 -
2/5/2019 1:52:48 PM 107.1 -
2/5/2019 1:52:49 PM 107.2 -
2/5/2019 1:52:50 PM 107.3 -
2/5/2019 1:52:51 PM 107.3 -
2/5/2019 1:52:52 PM 107.4 -
2/5/2019 1:52:53 PM 107.4 -
2/5/2019 1:52:54 PM 107.5 -
2/5/2019 1:52:55 PM 107.5 -
2/5/2019 1:52:56 PM 107.5 -
2/5/2019 1:52:57 PM 107.4 -
2/5/2019 1:52:58 PM 107.4 -
2/5/2019 1:52:59 PM 107.4 -
2/5/2019 1:53:00 PM 107.4 -
2/5/2019 1:53:01 PM 107.4 -
2/5/2019 1:53:02 PM 107.4 -
2/5/2019 1:53:03 PM 107.4 -
2/5/2019 1:53:04 PM 107.4 -
2/5/2019 1:53:05 PM 107.4 -
2/5/2019 1:53:06 PM 107.4 -
2/5/2019 1:53:07 PM 107.4 -
2/5/2019 1:53:08 PM 107.4 -
2/5/2019 1:53:09 PM 107.5 -
2/5/2019 1:53:10 PM 107.8 -
2/5/2019 1:53:11 PM 109.1 2.0
2/5/2019 1:53:12 PM 158.8 51.7
2/5/2019 1:53:13 PM 225.1 118.0
2/5/2019 1:53:14 PM 315.4 208.3
2/5/2019 1:53:15 PM 443.3 336.2
2/5/2019 1:53:16 PM 559.6 452.5
2/5/2019 1:53:17 PM 733.7 626.6
2/5/2019 1:53:18 PM 1055.7 948.6
2/5/2019 1:53:19 PM 1324.5 1217.4
2/5/2019 1:53:20 PM 1506.0 1398.9
2/5/2019 1:53:21 PM 1724.2 1617.1
2/5/2019 1:53:22 PM 1871.7 1764.6
2/5/2019 1:53:23 PM 1958.2 1851.1
2/5/2019 1:53:24 PM 2011.8 1904.7
2/5/2019 1:53:25 PM 2066.0 1958.9
2/5/2019 1:53:26 PM 2098.8 1991.7
2/5/2019 1:53:27 PM 2120.8 2013.7
2/5/2019 1:53:28 PM 2129.7 2022.6
2/5/2019 1:53:29 PM 2130.6 2023.5
2/5/2019 1:53:30 PM 2124.5 2017.4
2/5/2019 1:53:31 PM 1991.8 1884.7
2/5/2019 1:53:32 PM 1930.0 1822.9
2/5/2019 1:53:33 PM 1867.1 1760.0
2/5/2019 1:53:34 PM 1808.3 1701.2
2/5/2019 1:53:35 PM 1777.5 1670.4
2/5/2019 1:53:36 PM 1636.1 1529.0
2/5/2019 1:53:37 PM 1580.3 1473.2
2/5/2019 1:53:38 PM 1497.1 1390.0
Table E1 SEEP-B1 TEST-2 Data Log
Page 181 of 452 August 2019
APPENDIX E38: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B1 TEST-2 Data Log
2/5/2019 1:53:39 PM 1445.1 1338.0
2/5/2019 1:53:40 PM 1406.6 1299.5
2/5/2019 1:53:41 PM 1289.4 1182.3
2/5/2019 1:53:42 PM 1215.6 1108.5
2/5/2019 1:53:43 PM 1161.8 1054.7
2/5/2019 1:53:44 PM 1114.2 1007.1
2/5/2019 1:53:45 PM 1089.0 981.9
2/5/2019 1:53:46 PM 1051.0 943.9
2/5/2019 1:53:47 PM 937.3 830.2
2/5/2019 1:53:48 PM 883.8 776.7
2/5/2019 1:53:49 PM 841.0 733.9
2/5/2019 1:53:50 PM 824.5 717.4
2/5/2019 1:53:51 PM 753.6 646.5
2/5/2019 1:53:52 PM 715.4 608.3
2/5/2019 1:53:53 PM 684.5 577.4
2/5/2019 1:53:54 PM 652.1 545.0
2/5/2019 1:53:55 PM 637.8 530.7
2/5/2019 1:53:56 PM 548.2 441.1
2/5/2019 1:53:57 PM 549.8 442.7
2/5/2019 1:53:58 PM 524.8 417.7
2/5/2019 1:53:59 PM 509.8 402.7
2/5/2019 1:54:00 PM 491.6 384.5
2/5/2019 1:54:01 PM 478.2 371.1
2/5/2019 1:54:02 PM 420.8 313.7
2/5/2019 1:54:03 PM 401.6 294.5
2/5/2019 1:54:04 PM 383.2 276.1
2/5/2019 1:54:05 PM 371.7 264.6
2/5/2019 1:54:06 PM 365.5 258.4
2/5/2019 1:54:07 PM 355.5 248.4
2/5/2019 1:54:08 PM 345.2 238.1
2/5/2019 1:54:09 PM 338.2 231.1
2/5/2019 1:54:10 PM 330.9 223.8
2/5/2019 1:54:11 PM 324.4 217.3
2/5/2019 1:54:12 PM 271.5 164.4
2/5/2019 1:54:13 PM 263.6 156.5
2/5/2019 1:54:14 PM 252.2 145.1
2/5/2019 1:54:15 PM 248.9 141.8
2/5/2019 1:54:16 PM 243.4 136.3
2/5/2019 1:54:17 PM 238.9 131.8
2/5/2019 1:54:18 PM 235.1 128.0
2/5/2019 1:54:19 PM 231.5 124.4
2/5/2019 1:54:20 PM 228.5 121.4
2/5/2019 1:54:21 PM 224.9 117.8
2/5/2019 1:54:22 PM 221.7 114.6
2/5/2019 1:54:23 PM 218.3 111.2
2/5/2019 1:54:24 PM 215.4 108.3
2/5/2019 1:54:25 PM 212.4 105.3
2/5/2019 1:54:26 PM 209.9 102.8
2/5/2019 1:54:27 PM 207.1 100.0
2/5/2019 1:54:28 PM 202.6 95.5
2/5/2019 1:54:29 PM 196.8 89.7
2/5/2019 1:54:30 PM 192.0 84.9
2/5/2019 1:54:31 PM 186.9 79.8
2/5/2019 1:54:32 PM 182.6 75.5
2/5/2019 1:54:33 PM 178.0 70.9
2/5/2019 1:54:34 PM 174.3 67.2
2/5/2019 1:54:35 PM 170.5 63.4
2/5/2019 1:54:36 PM 167.3 60.2
2/5/2019 1:54:37 PM 164.0 56.9
2/5/2019 1:54:38 PM 161.3 54.2
2/5/2019 1:54:39 PM 158.2 51.1
2/5/2019 1:54:40 PM 155.8 48.7
2/5/2019 1:54:41 PM 153.2 46.1
2/5/2019 1:54:42 PM 151.1 44.0
2/5/2019 1:54:43 PM 148.8 41.7
2/5/2019 1:54:44 PM 147.0 39.9
2/5/2019 1:54:45 PM 145.1 38.0
2/5/2019 1:54:46 PM 143.5 36.4
2/5/2019 1:54:47 PM 141.8 34.7
2/5/2019 1:54:48 PM 140.4 33.3
2/5/2019 1:54:49 PM 138.9 31.8
2/5/2019 1:54:50 PM 137.7 30.6
2/5/2019 1:54:51 PM 136.3 29.2
2/5/2019 1:54:52 PM 135.2 28.1
2/5/2019 1:54:53 PM 134.1 27.0
2/5/2019 1:54:54 PM 133.1 26.0
2/5/2019 1:54:55 PM 132.1 25.0
Page 182 of 452 August 2019
APPENDIX E38: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B1 TEST-2 Data Log
2/5/2019 1:54:56 PM 131.3 24.2
2/5/2019 1:54:57 PM 130.4 23.3
2/5/2019 1:54:58 PM 129.6 22.5
2/5/2019 1:54:59 PM 128.9 21.8
2/5/2019 1:55:00 PM 128.1 21.0
2/5/2019 1:55:01 PM 127.5 20.4
2/5/2019 1:55:02 PM 126.8 19.7
2/5/2019 1:55:03 PM 126.2 19.1
2/5/2019 1:55:04 PM 125.6 18.5
2/5/2019 1:55:05 PM 125.0 17.9
2/5/2019 1:55:06 PM 124.5 17.4
2/5/2019 1:55:07 PM 124.0 16.9
2/5/2019 1:55:08 PM 123.5 16.4
2/5/2019 1:55:09 PM 123.0 15.9
2/5/2019 1:55:10 PM 122.5 15.4
2/5/2019 1:55:11 PM 122.1 15.0
2/5/2019 1:55:12 PM 121.7 14.6
2/5/2019 1:55:13 PM 121.3 14.2
2/5/2019 1:55:14 PM 120.9 13.8
2/5/2019 1:55:15 PM 120.5 13.4
2/5/2019 1:55:16 PM 120.1 13.0
2/5/2019 1:55:17 PM 119.8 12.7
2/5/2019 1:55:18 PM 119.4 12.3
2/5/2019 1:55:19 PM 119.0 11.9
2/5/2019 1:55:20 PM 118.8 11.7
2/5/2019 1:55:21 PM 118.5 11.4
2/5/2019 1:55:22 PM 118.2 11.1
2/5/2019 1:55:23 PM 117.9 10.8
2/5/2019 1:55:24 PM 117.5 10.4
2/5/2019 1:55:25 PM 117.4 10.3
2/5/2019 1:55:26 PM 117.1 10.0
2/5/2019 1:55:27 PM 116.8 9.7
2/5/2019 1:55:28 PM 116.6 9.5
2/5/2019 1:55:29 PM 116.4 9.3
2/5/2019 1:55:30 PM 116.1 9.0
2/5/2019 1:55:31 PM 116.0 8.9
2/5/2019 1:55:32 PM 115.7 8.6
2/5/2019 1:55:33 PM 115.6 8.5
2/5/2019 1:55:34 PM 115.4 8.3
2/5/2019 1:55:35 PM 115.2 8.1
2/5/2019 1:55:36 PM 115.0 7.9
2/5/2019 1:55:37 PM 114.9 7.8
2/5/2019 1:55:38 PM 114.7 7.6
2/5/2019 1:55:39 PM 114.6 7.5
2/5/2019 1:55:40 PM 114.5 7.4
2/5/2019 1:55:41 PM 114.3 7.2
2/5/2019 1:55:42 PM 114.2 7.1
2/5/2019 1:55:43 PM 114.1 7.0
2/5/2019 1:55:44 PM 114.0 6.9
2/5/2019 1:55:45 PM 113.9 6.8
2/5/2019 1:55:46 PM 113.7 6.6
2/5/2019 1:55:47 PM 113.6 6.5
2/5/2019 1:55:48 PM 113.5 6.4
2/5/2019 1:55:49 PM 113.4 6.3
2/5/2019 1:55:50 PM 113.3 6.2
2/5/2019 1:55:51 PM 113.2 6.1
2/5/2019 1:55:52 PM 113.1 6.0
2/5/2019 1:55:53 PM 113.0 5.9
2/5/2019 1:55:54 PM 112.9 5.8
2/5/2019 1:55:55 PM 112.9 5.8
2/5/2019 1:55:56 PM 112.8 5.7
2/5/2019 1:55:57 PM 112.7 5.6
2/5/2019 1:55:58 PM 112.6 5.5
2/5/2019 1:55:59 PM 112.5 5.4
2/5/2019 1:56:00 PM 112.5 5.4
2/5/2019 1:56:01 PM 112.4 5.3
2/5/2019 1:56:02 PM 112.3 5.2
2/5/2019 1:56:03 PM 112.2 5.1
2/5/2019 1:56:04 PM 112.1 5.0
2/5/2019 1:56:05 PM 112.1 5.0
2/5/2019 1:56:06 PM 112.0 4.9
2/5/2019 1:56:07 PM 111.9 4.8
2/5/2019 1:56:08 PM 111.9 -
2/5/2019 1:56:09 PM 111.8 -
2/5/2019 1:56:10 PM 111.7 -
2/5/2019 1:56:11 PM 111.7 -
2/5/2019 1:56:12 PM 111.6 -
2/5/2019 1:56:13 PM 111.5 -
2/5/2019 1:56:14 PM 111.5 -
Page 183 of 452 August 2019
APPENDIX E38: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B1 TEST-2 Data Log
2/5/2019 1:56:15 PM 111.4 -
2/5/2019 1:56:16 PM 111.4 -
2/5/2019 1:56:17 PM 111.3 -
2/5/2019 1:56:18 PM 111.3 -
2/5/2019 1:56:19 PM 111.3 -
2/5/2019 1:56:20 PM 111.2 -
2/5/2019 1:56:21 PM 111.2 -
2/5/2019 1:56:22 PM 111.1 -
2/5/2019 1:56:23 PM 111.1 -
2/5/2019 1:56:24 PM 111.1 -
2/5/2019 1:56:25 PM 111.0 -
2/5/2019 1:56:26 PM 111.0 -
2/5/2019 1:56:27 PM 111.0 -
2/5/2019 1:56:28 PM 110.9 -
2/5/2019 1:56:29 PM 110.9 -
2/5/2019 1:56:30 PM 110.9 -
2/5/2019 1:56:31 PM 110.8 -
2/5/2019 1:56:32 PM 110.8 -
2/5/2019 1:56:33 PM 110.8 -
2/5/2019 1:56:34 PM 110.7 -
2/5/2019 1:56:35 PM 110.7 -
2/5/2019 1:56:36 PM 110.7 -
2/5/2019 1:56:37 PM 110.6 -
2/5/2019 1:56:38 PM 110.6 -
2/5/2019 1:56:39 PM 110.6 -
2/5/2019 1:56:40 PM 110.5 -
2/5/2019 1:56:41 PM 110.5 -
2/5/2019 1:56:42 PM 110.5 -
2/5/2019 1:56:43 PM 110.4 -
2/5/2019 1:56:44 PM 110.4 -
2/5/2019 1:56:45 PM 110.4 -
2/5/2019 1:56:46 PM 110.3 -
2/5/2019 1:56:47 PM 110.3 -
2/5/2019 1:56:48 PM 110.3 -
2/5/2019 1:56:49 PM 110.2 -
2/5/2019 1:56:50 PM 110.2 -
2/5/2019 1:56:51 PM 110.1 -
2/5/2019 1:56:52 PM 110.1 -
2/5/2019 1:56:53 PM 110.1 -
2/5/2019 1:56:54 PM 110.0 -
2/5/2019 1:56:55 PM 110.0 -
2/5/2019 1:56:56 PM 110.0 -
2/5/2019 1:56:57 PM 109.9 -
2/5/2019 1:56:58 PM 109.9 -
2/5/2019 1:56:59 PM 109.9 -
2/5/2019 1:57:00 PM 109.8 -
2/5/2019 1:57:01 PM 109.8 -
2/5/2019 1:57:02 PM 109.8 -
2/5/2019 1:57:03 PM 109.7 -
2/5/2019 1:57:04 PM 109.7 -
2/5/2019 1:57:05 PM 109.7 -
2/5/2019 1:57:06 PM 109.7 -
2/5/2019 1:57:07 PM 109.6 -
2/5/2019 1:57:08 PM 109.6 -
2/5/2019 1:57:09 PM 109.6 -
2/5/2019 1:57:10 PM 109.6 -
2/5/2019 1:57:11 PM 109.6 -
2/5/2019 1:57:12 PM 109.5 -
2/5/2019 1:57:13 PM 109.5 -
2/5/2019 1:57:14 PM 109.5 -
2/5/2019 1:57:15 PM 109.5 -
2/5/2019 1:57:16 PM 109.4 -
2/5/2019 1:57:17 PM 109.4 -
2/5/2019 1:57:18 PM 109.4 -
2/5/2019 1:57:19 PM 109.4 -
Page 184 of 452 August 2019
APPENDIX E38: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-B2 TEST-1 1259
SEEP-B2 TEST-1 1301
SEEP-B2 TEST-1 1306
SEEP-B2 TEST-1 1307
Location EC Reading
(µS/cms)
SEEP-B2 TEST-1 49.5
SEEP-B2 TEST-1 194
SEEP-B2 TEST-1 14,050
SEEP-B2 TEST-1 109,408
q 300,100
K 1.0972
5.3
84.5
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms) (°C)
Table E2 SEEP-B1 TEST-2 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
106.3 16
105.9 16
107.8 16
106.1 15.7
Average 106.5
Geo Mean 106.5 (µS/cms)
10 21.8
Average (pre-test)107.1 (µS/cms)
Average (post-test)110.4 (µS/cms)
Table E3 SEEP-B1 TEST-2 YSI Salt Dilution Calibration Data
Calibration
Concentration Temperature
(mg/L)(°C)
Integral of Conductivity
Data Curve
SUM:Δt(E
Ct-ECbkg)61,844.2 (s) . (µS/cms)
100 22.2
1,000 21.8
10,000 21.7
Table E4 SEEP-B1 TEST-2 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Calculated Flow Rate Q
L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for
Streamflow Measurement Part 2: Constant-Rate Injection.”
Streamline, Watershed Management Bulletin, vol. 8, no. 1, 2004,
pp. 11–15.
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 185 of 452 August 2019
APPENDIX E39: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-3 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/5/2019 2:06:33 PM 108.7 -
2/5/2019 2:06:34 PM 108.6 -
2/5/2019 2:06:35 PM 108.6 -
2/5/2019 2:06:36 PM 108.5 -
2/5/2019 2:06:37 PM 108.4 -
2/5/2019 2:06:38 PM 108.4 -
2/5/2019 2:06:39 PM 108.3 -
2/5/2019 2:06:40 PM 108.2 -
2/5/2019 2:06:41 PM 108.2 -
2/5/2019 2:06:42 PM 108.1 -
2/5/2019 2:06:43 PM 108.1 -
2/5/2019 2:06:44 PM 108.0 -
2/5/2019 2:06:45 PM 107.9 -
2/5/2019 2:06:46 PM 107.9 -
2/5/2019 2:06:47 PM 107.8 -
2/5/2019 2:06:48 PM 107.7 -
2/5/2019 2:06:49 PM 107.7 -
2/5/2019 2:06:50 PM 107.6 -
2/5/2019 2:06:51 PM 107.6 -
2/5/2019 2:06:52 PM 107.5 -
2/5/2019 2:06:53 PM 107.5 -
2/5/2019 2:06:54 PM 107.4 -
2/5/2019 2:06:55 PM 107.4 -
2/5/2019 2:06:56 PM 107.3 -
2/5/2019 2:06:57 PM 107.3 -
2/5/2019 2:06:58 PM 107.2 -
2/5/2019 2:06:59 PM 107.2 -
2/5/2019 2:07:00 PM 107.1 -
2/5/2019 2:07:01 PM 107.1 -
2/5/2019 2:07:02 PM 107.0 -
2/5/2019 2:07:03 PM 106.9 -
2/5/2019 2:07:04 PM 106.9 -
2/5/2019 2:07:05 PM 106.8 -
2/5/2019 2:07:06 PM 106.8 -
2/5/2019 2:07:07 PM 106.7 -
2/5/2019 2:07:08 PM 106.7 -
2/5/2019 2:07:09 PM 106.6 -
2/5/2019 2:07:10 PM 106.6 -
2/5/2019 2:07:11 PM 106.5 -
2/5/2019 2:07:12 PM 106.5 -
2/5/2019 2:07:13 PM 106.5 -
2/5/2019 2:07:14 PM 106.4 -
2/5/2019 2:07:15 PM 106.4 -
2/5/2019 2:07:16 PM 106.4 -
2/5/2019 2:07:17 PM 106.6 -
2/5/2019 2:07:18 PM 107.1 -
2/5/2019 2:07:19 PM 108.5 1.1
2/5/2019 2:07:20 PM 170.5 63.1
2/5/2019 2:07:21 PM 240.0 132.6
2/5/2019 2:07:22 PM 311.5 204.1
2/5/2019 2:07:23 PM 401.0 293.6
2/5/2019 2:07:24 PM 594.5 487.1
2/5/2019 2:07:25 PM 748.2 640.8
2/5/2019 2:07:26 PM 1056.0 948.6
2/5/2019 2:07:27 PM 1160.0 1052.6
2/5/2019 2:07:28 PM 1330.3 1222.9
2/5/2019 2:07:29 PM 1602.2 1494.8
2/5/2019 2:07:30 PM 1722.2 1614.8
2/5/2019 2:07:31 PM 1781.0 1673.6
2/5/2019 2:07:32 PM 1848.7 1741.3
2/5/2019 2:07:33 PM 1901.5 1794.1
2/5/2019 2:07:34 PM 1927.2 1819.8
2/5/2019 2:07:35 PM 1946.7 1839.3
2/5/2019 2:07:36 PM 1955.4 1848.0
2/5/2019 2:07:37 PM 1957.5 1850.1
2/5/2019 2:07:38 PM 1955.5 1848.1
2/5/2019 2:07:39 PM 1947.6 1840.2
2/5/2019 2:07:40 PM 1788.0 1680.6
2/5/2019 2:07:41 PM 1753.1 1645.7
2/5/2019 2:07:42 PM 1685.1 1577.7
Table E1 SEEP-B1 TEST-3 Data Log
Page 186 of 452 August 2019
APPENDIX E39: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-3 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B1 TEST-3 Data Log
2/5/2019 2:07:43 PM 1650.4 1543.0
2/5/2019 2:07:44 PM 1605.9 1498.5
2/5/2019 2:07:45 PM 1453.0 1345.6
2/5/2019 2:07:46 PM 1387.6 1280.2
2/5/2019 2:07:47 PM 1331.7 1224.3
2/5/2019 2:07:48 PM 1307.2 1199.8
2/5/2019 2:07:49 PM 1282.3 1174.9
2/5/2019 2:07:50 PM 1167.0 1059.6
2/5/2019 2:07:51 PM 1108.8 1001.4
2/5/2019 2:07:52 PM 1048.1 940.7
2/5/2019 2:07:53 PM 1006.1 898.7
2/5/2019 2:07:54 PM 918.8 811.4
2/5/2019 2:07:55 PM 891.1 783.7
2/5/2019 2:07:56 PM 849.5 742.1
2/5/2019 2:07:57 PM 805.2 697.8
2/5/2019 2:07:58 PM 792.1 684.7
2/5/2019 2:07:59 PM 722.3 614.9
2/5/2019 2:08:00 PM 676.3 568.9
2/5/2019 2:08:01 PM 640.5 533.1
2/5/2019 2:08:02 PM 619.6 512.2
2/5/2019 2:08:03 PM 467.3 359.9
2/5/2019 2:08:04 PM 549.4 442.0
2/5/2019 2:08:05 PM 527.7 420.3
2/5/2019 2:08:06 PM 502.5 395.1
2/5/2019 2:08:07 PM 493.4 386.0
2/5/2019 2:08:08 PM 481.0 373.6
2/5/2019 2:08:09 PM 471.6 364.2
2/5/2019 2:08:10 PM 413.8 306.4
2/5/2019 2:08:11 PM 400.8 293.4
2/5/2019 2:08:12 PM 381.0 273.6
2/5/2019 2:08:13 PM 369.1 261.7
2/5/2019 2:08:14 PM 357.5 250.1
2/5/2019 2:08:15 PM 349.9 242.5
2/5/2019 2:08:16 PM 343.0 235.6
2/5/2019 2:08:17 PM 336.5 229.1
2/5/2019 2:08:18 PM 329.5 222.1
2/5/2019 2:08:19 PM 323.8 216.4
2/5/2019 2:08:20 PM 317.8 210.4
2/5/2019 2:08:21 PM 265.6 158.2
2/5/2019 2:08:22 PM 254.9 147.5
2/5/2019 2:08:23 PM 246.4 139.0
2/5/2019 2:08:24 PM 242.7 135.3
2/5/2019 2:08:25 PM 237.7 130.3
2/5/2019 2:08:26 PM 232.2 124.8
2/5/2019 2:08:27 PM 228.7 121.3
2/5/2019 2:08:28 PM 225.5 118.1
2/5/2019 2:08:29 PM 222.8 115.4
2/5/2019 2:08:30 PM 220.5 113.1
2/5/2019 2:08:31 PM 217.6 110.2
2/5/2019 2:08:32 PM 215.1 107.7
2/5/2019 2:08:33 PM 212.3 104.9
2/5/2019 2:08:34 PM 209.9 102.5
2/5/2019 2:08:35 PM 207.2 99.8
2/5/2019 2:08:36 PM 205.1 97.7
2/5/2019 2:08:37 PM 201.2 93.8
2/5/2019 2:08:38 PM 196.8 89.4
2/5/2019 2:08:39 PM 192.2 84.8
2/5/2019 2:08:40 PM 188.4 81.0
2/5/2019 2:08:41 PM 184.1 76.7
2/5/2019 2:08:42 PM 180.4 73.0
2/5/2019 2:08:43 PM 176.4 69.0
2/5/2019 2:08:44 PM 173.3 65.9
2/5/2019 2:08:45 PM 170.0 62.6
2/5/2019 2:08:46 PM 167.3 59.9
2/5/2019 2:08:47 PM 164.5 57.1
2/5/2019 2:08:48 PM 161.6 54.2
2/5/2019 2:08:49 PM 159.0 51.6
2/5/2019 2:08:50 PM 156.8 49.4
2/5/2019 2:08:51 PM 154.5 47.1
2/5/2019 2:08:52 PM 152.6 45.2
2/5/2019 2:08:53 PM 150.7 43.3
2/5/2019 2:08:54 PM 149.0 41.6
2/5/2019 2:08:55 PM 147.3 39.9
2/5/2019 2:08:56 PM 145.8 38.4
2/5/2019 2:08:57 PM 144.2 36.8
2/5/2019 2:08:58 PM 142.9 35.5
2/5/2019 2:08:59 PM 141.4 34.0
Page 187 of 452 August 2019
APPENDIX E39: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-3 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B1 TEST-3 Data Log
2/5/2019 2:09:00 PM 140.2 32.8
2/5/2019 2:09:01 PM 138.9 31.5
2/5/2019 2:09:02 PM 137.9 30.5
2/5/2019 2:09:03 PM 136.7 29.3
2/5/2019 2:09:04 PM 135.8 28.4
2/5/2019 2:09:05 PM 134.9 27.5
2/5/2019 2:09:06 PM 134.0 26.6
2/5/2019 2:09:07 PM 133.1 25.7
2/5/2019 2:09:08 PM 132.3 24.9
2/5/2019 2:09:09 PM 131.5 24.1
2/5/2019 2:09:10 PM 130.7 23.3
2/5/2019 2:09:11 PM 129.9 22.5
2/5/2019 2:09:12 PM 129.3 21.9
2/5/2019 2:09:13 PM 128.5 21.1
2/5/2019 2:09:14 PM 127.9 20.5
2/5/2019 2:09:15 PM 127.2 19.8
2/5/2019 2:09:16 PM 126.6 19.2
2/5/2019 2:09:17 PM 126.0 18.6
2/5/2019 2:09:18 PM 125.4 18.0
2/5/2019 2:09:19 PM 124.8 17.4
2/5/2019 2:09:20 PM 124.4 17.0
2/5/2019 2:09:21 PM 123.8 16.4
2/5/2019 2:09:22 PM 123.3 15.9
2/5/2019 2:09:23 PM 122.9 15.5
2/5/2019 2:09:24 PM 122.5 15.1
2/5/2019 2:09:25 PM 122.2 14.8
2/5/2019 2:09:26 PM 121.8 14.4
2/5/2019 2:09:27 PM 121.4 14.0
2/5/2019 2:09:28 PM 121.1 13.7
2/5/2019 2:09:29 PM 120.8 13.4
2/5/2019 2:09:30 PM 120.4 13.0
2/5/2019 2:09:31 PM 120.2 12.8
2/5/2019 2:09:32 PM 119.9 12.5
2/5/2019 2:09:33 PM 119.6 12.2
2/5/2019 2:09:34 PM 119.3 11.9
2/5/2019 2:09:35 PM 119.1 11.7
2/5/2019 2:09:36 PM 118.8 11.4
2/5/2019 2:09:37 PM 118.6 11.2
2/5/2019 2:09:38 PM 118.3 10.9
2/5/2019 2:09:39 PM 118.1 10.7
2/5/2019 2:09:40 PM 117.8 10.4
2/5/2019 2:09:41 PM 117.6 10.2
2/5/2019 2:09:42 PM 117.4 10.0
2/5/2019 2:09:43 PM 117.2 9.8
2/5/2019 2:09:44 PM 117.0 9.6
2/5/2019 2:09:45 PM 116.8 9.4
2/5/2019 2:09:46 PM 116.5 9.1
2/5/2019 2:09:47 PM 116.4 9.0
2/5/2019 2:09:48 PM 116.1 8.7
2/5/2019 2:09:49 PM 115.9 8.5
2/5/2019 2:09:50 PM 115.7 8.3
2/5/2019 2:09:51 PM 115.6 8.2
2/5/2019 2:09:52 PM 115.4 8.0
2/5/2019 2:09:53 PM 115.2 7.8
2/5/2019 2:09:54 PM 115.0 7.6
2/5/2019 2:09:55 PM 114.9 7.5
2/5/2019 2:09:56 PM 114.7 7.3
2/5/2019 2:09:57 PM 114.5 7.1
2/5/2019 2:09:58 PM 114.4 7.0
2/5/2019 2:09:59 PM 114.2 6.8
2/5/2019 2:10:00 PM 114.0 6.6
2/5/2019 2:10:01 PM 113.9 6.5
2/5/2019 2:10:02 PM 113.8 6.4
2/5/2019 2:10:03 PM 113.6 6.2
2/5/2019 2:10:04 PM 113.5 6.1
2/5/2019 2:10:05 PM 113.4 6.0
2/5/2019 2:10:06 PM 113.2 5.8
2/5/2019 2:10:07 PM 113.1 5.7
2/5/2019 2:10:08 PM 113.0 5.6
2/5/2019 2:10:09 PM 112.8 5.4
2/5/2019 2:10:10 PM 112.7 5.3
2/5/2019 2:10:11 PM 112.5 5.1
2/5/2019 2:10:12 PM 112.4 5.0
2/5/2019 2:10:13 PM 112.3 4.9
2/5/2019 2:10:14 PM 112.2 4.8
2/5/2019 2:10:15 PM 112.0 4.6
2/5/2019 2:10:16 PM 111.9 -
2/5/2019 2:10:17 PM 111.8 -
2/5/2019 2:10:18 PM 111.7 -
Page 188 of 452 August 2019
APPENDIX E39: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-3 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B1 TEST-3 Data Log
2/5/2019 2:10:19 PM 111.5 -
2/5/2019 2:10:20 PM 111.4 -
2/5/2019 2:10:21 PM 111.3 -
2/5/2019 2:10:22 PM 111.2 -
2/5/2019 2:10:23 PM 111.1 -
2/5/2019 2:10:24 PM 111.0 -
2/5/2019 2:10:25 PM 110.9 -
2/5/2019 2:10:26 PM 110.9 -
2/5/2019 2:10:27 PM 110.8 -
2/5/2019 2:10:28 PM 110.7 -
2/5/2019 2:10:29 PM 110.6 -
2/5/2019 2:10:30 PM 110.5 -
2/5/2019 2:10:31 PM 110.4 -
2/5/2019 2:10:32 PM 110.3 -
2/5/2019 2:10:33 PM 110.2 -
2/5/2019 2:10:34 PM 110.2 -
2/5/2019 2:10:35 PM 110.1 -
2/5/2019 2:10:36 PM 110.0 -
2/5/2019 2:10:37 PM 109.9 -
2/5/2019 2:10:38 PM 109.8 -
2/5/2019 2:10:39 PM 109.7 -
2/5/2019 2:10:40 PM 109.7 -
2/5/2019 2:10:41 PM 109.6 -
2/5/2019 2:10:42 PM 109.5 -
2/5/2019 2:10:43 PM 109.4 -
2/5/2019 2:10:44 PM 109.4 -
2/5/2019 2:10:45 PM 109.3 -
2/5/2019 2:10:46 PM 109.2 -
2/5/2019 2:10:47 PM 109.1 -
2/5/2019 2:10:48 PM 109.1 -
2/5/2019 2:10:49 PM 109.0 -
2/5/2019 2:10:50 PM 108.9 -
2/5/2019 2:10:51 PM 108.9 -
2/5/2019 2:10:52 PM 108.8 -
2/5/2019 2:10:53 PM 108.7 -
2/5/2019 2:10:54 PM 108.7 -
2/5/2019 2:10:55 PM 108.6 -
2/5/2019 2:10:56 PM 108.6 -
2/5/2019 2:10:57 PM 108.5 -
2/5/2019 2:10:58 PM 108.4 -
2/5/2019 2:10:59 PM 108.4 -
2/5/2019 2:11:00 PM 108.3 -
2/5/2019 2:11:01 PM 108.3 -
2/5/2019 2:11:02 PM 108.2 -
2/5/2019 2:11:03 PM 108.2 -
2/5/2019 2:11:04 PM 108.1 -
2/5/2019 2:11:05 PM 108.1 -
2/5/2019 2:11:06 PM 108.0 -
2/5/2019 2:11:07 PM 108.0 -
2/5/2019 2:11:08 PM 108.0 -
2/5/2019 2:11:09 PM 107.9 -
2/5/2019 2:11:10 PM 107.9 -
2/5/2019 2:11:11 PM 107.8 -
2/5/2019 2:11:12 PM 107.8 -
2/5/2019 2:11:13 PM 107.8 -
2/5/2019 2:11:14 PM 107.7 -
2/5/2019 2:11:15 PM 107.7 -
2/5/2019 2:11:16 PM 107.7 -
2/5/2019 2:11:17 PM 107.7 -
2/5/2019 2:11:18 PM 107.6 -
2/5/2019 2:11:19 PM 107.6 -
2/5/2019 2:11:20 PM 107.6 -
2/5/2019 2:11:21 PM 107.6 -
2/5/2019 2:11:22 PM 107.5 -
2/5/2019 2:11:23 PM 107.5 -
2/5/2019 2:11:24 PM 107.5 -
2/5/2019 2:11:25 PM 107.5 -
2/5/2019 2:11:26 PM 107.4 -
2/5/2019 2:11:27 PM 107.4 -
2/5/2019 2:11:28 PM 107.4 -
2/5/2019 2:11:29 PM 107.3 -
2/5/2019 2:11:30 PM 107.3 -
2/5/2019 2:11:31 PM 107.3 -
2/5/2019 2:11:32 PM 107.2 -
2/5/2019 2:11:33 PM 107.2 -
2/5/2019 2:11:34 PM 107.1 -
2/5/2019 2:11:35 PM 107.1 -
2/5/2019 2:11:36 PM 107.1 -
2/5/2019 2:11:37 PM 107.0 -
Page 189 of 452 August 2019
APPENDIX E39: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-3 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B1 TEST-3 Data Log
2/5/2019 2:11:38 PM 107.0 -
2/5/2019 2:11:39 PM 107.0 -
2/5/2019 2:11:40 PM 106.9 -
2/5/2019 2:11:41 PM 106.9 -
2/5/2019 2:11:42 PM 106.8 -
2/5/2019 2:11:43 PM 106.8 -
2/5/2019 2:11:44 PM 106.8 -
2/5/2019 2:11:45 PM 106.7 -
2/5/2019 2:11:46 PM 106.7 -
2/5/2019 2:11:47 PM 106.7 -
2/5/2019 2:11:48 PM 106.6 -
2/5/2019 2:11:49 PM 106.6 -
2/5/2019 2:11:50 PM 106.6 -
2/5/2019 2:11:51 PM 106.5 -
Page 190 of 452 August 2019
APPENDIX E39: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-3 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-B2 TEST-1 1259
SEEP-B2 TEST-1 1301
SEEP-B2 TEST-1 1306
SEEP-B2 TEST-1 1307
Location EC Reading
(µS/cms)
SEEP-B2 TEST-1 49.5
SEEP-B2 TEST-1 194
SEEP-B2 TEST-1 14,050
SEEP-B2 TEST-1 109,408
q 300,200
K 1.0972
5.7
89.9
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)(°C)
Table E2 SEEP-B1 TEST-3 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
106.3 16
105.9 16
107.8 16
106.1 15.7
Average 106.5
Geo Mean 106.5 (µS/cms)
10 21.8
Average (pre-test)107.4 (µS/cms)
Average (post-test)108.6 (µS/cms)
Table E3 SEEP-B1 TEST-3 YSI Salt Dilution Calibration Data
Calibration
Concentration Temperature
(mg/L)(°C)
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)58,179.8 (s) . (µS/cms)
100 22.2
1,000 21.8
10,000 21.7
Table E4 SEEP-B1 TEST-3 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Calculated Flow Rate Q
L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline,
Watershed Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 191 of 452 August 2019
APPENDIX E40: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 3:48:59 PM 146.6 -
6/7/2019 3:49:00 PM 146.7 -
6/7/2019 3:49:01 PM 146.8 -
6/7/2019 3:49:02 PM 146.9 -
6/7/2019 3:49:03 PM 147.0 -
6/7/2019 3:49:04 PM 147.1 -
6/7/2019 3:49:05 PM 147.2 -
6/7/2019 3:49:06 PM 147.2 -
6/7/2019 3:49:07 PM 147.3 -
6/7/2019 3:49:08 PM 147.4 -
6/7/2019 3:49:09 PM 147.4 -
6/7/2019 3:49:10 PM 147.5 -
6/7/2019 3:49:11 PM 147.5 -
6/7/2019 3:49:12 PM 147.6 -
6/7/2019 3:49:13 PM 147.6 -
6/7/2019 3:49:14 PM 147.6 -
6/7/2019 3:49:15 PM 147.6 -
6/7/2019 3:49:16 PM 147.6 -
6/7/2019 3:49:17 PM 148.0 -
6/7/2019 3:49:18 PM 4828.9 4681.6
6/7/2019 3:49:19 PM 7460.4 7313.1
6/7/2019 3:49:20 PM 14204.1 14056.8
6/7/2019 3:49:21 PM 14726.8 14579.5
6/7/2019 3:49:22 PM 14533.2 14385.9
6/7/2019 3:49:23 PM 10887.2 10739.9
6/7/2019 3:49:24 PM 8926.6 8779.3
6/7/2019 3:49:25 PM 6691.8 6544.5
6/7/2019 3:49:26 PM 6482.3 6335.0
6/7/2019 3:49:27 PM 3697.4 3550.1
6/7/2019 3:49:28 PM 2897.1 2749.8
6/7/2019 3:49:29 PM 2108.2 1960.9
6/7/2019 3:49:30 PM 1765.2 1617.9
6/7/2019 3:49:31 PM 1581.2 1433.9
6/7/2019 3:49:32 PM 1441.8 1294.5
6/7/2019 3:49:33 PM 1047.5 900.2
6/7/2019 3:49:34 PM 957.8 810.5
6/7/2019 3:49:35 PM 916.1 768.8
6/7/2019 3:49:36 PM 743.9 596.6
6/7/2019 3:49:37 PM 647.5 500.2
6/7/2019 3:49:38 PM 411.4 264.1
6/7/2019 3:49:39 PM 524.1 376.8
6/7/2019 3:49:40 PM 537.1 389.8
6/7/2019 3:49:41 PM 470.3 323.0
6/7/2019 3:49:42 PM 459.2 311.9
6/7/2019 3:49:43 PM 452.1 304.8
6/7/2019 3:49:44 PM 418.4 271.1
6/7/2019 3:49:45 PM 404.5 257.2
6/7/2019 3:49:46 PM 342.0 194.7
6/7/2019 3:49:47 PM 333.6 186.3
6/7/2019 3:49:48 PM 322.8 175.5
6/7/2019 3:49:49 PM 314.6 167.3
6/7/2019 3:49:50 PM 303.4 156.1
6/7/2019 3:49:51 PM 285.2 137.9
6/7/2019 3:49:52 PM 269.4 122.1
6/7/2019 3:49:53 PM 262.9 115.6
6/7/2019 3:49:54 PM 259.8 112.5
6/7/2019 3:49:55 PM 256.8 109.5
6/7/2019 3:49:56 PM 252.3 105.0
6/7/2019 3:49:57 PM 248.6 101.3
6/7/2019 3:49:58 PM 244.8 97.5
6/7/2019 3:49:59 PM 241.6 94.3
6/7/2019 3:50:00 PM 238.4 91.1
6/7/2019 3:50:01 PM 235.6 88.3
6/7/2019 3:50:02 PM 232.0 84.7
6/7/2019 3:50:03 PM 225.8 78.5
6/7/2019 3:50:04 PM 221.0 73.7
6/7/2019 3:50:05 PM 217.4 70.1
6/7/2019 3:50:06 PM 213.8 66.5
6/7/2019 3:50:07 PM 209.8 62.5
6/7/2019 3:50:08 PM 206.6 59.3
Table E1 SEEP-B1 TEST-1 Data Log
Page 192 of 452 August 2019
APPENDIX E40: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B1 TEST-1 Data Log
6/7/2019 3:50:09 PM 203.7 56.4
6/7/2019 3:50:10 PM 201.6 54.3
6/7/2019 3:50:11 PM 200.0 52.7
6/7/2019 3:50:12 PM 198.8 51.5
6/7/2019 3:50:13 PM 197.4 50.1
6/7/2019 3:50:14 PM 196.4 49.1
6/7/2019 3:50:15 PM 195.6 48.3
6/7/2019 3:50:16 PM 194.8 47.5
6/7/2019 3:50:17 PM 193.6 46.3
6/7/2019 3:50:18 PM 192.6 45.3
6/7/2019 3:50:19 PM 190.6 43.3
6/7/2019 3:50:20 PM 189.4 42.1
6/7/2019 3:50:21 PM 188.4 41.1
6/7/2019 3:50:22 PM 187.8 40.5
6/7/2019 3:50:23 PM 187.6 40.3
6/7/2019 3:50:24 PM 186.5 39.2
6/7/2019 3:50:25 PM 185.3 38.0
6/7/2019 3:50:26 PM 184.2 36.9
6/7/2019 3:50:27 PM 183.3 36.0
6/7/2019 3:50:28 PM 182.1 34.8
6/7/2019 3:50:29 PM 181.1 33.8
6/7/2019 3:50:30 PM 180.2 32.9
6/7/2019 3:50:31 PM 179.3 32.0
6/7/2019 3:50:32 PM 178.3 31.0
6/7/2019 3:50:33 PM 177.5 30.2
6/7/2019 3:50:34 PM 176.6 29.3
6/7/2019 3:50:35 PM 175.8 28.5
6/7/2019 3:50:36 PM 174.5 27.2
6/7/2019 3:50:37 PM 173.6 26.3
6/7/2019 3:50:38 PM 172.9 25.6
6/7/2019 3:50:39 PM 172.5 25.2
6/7/2019 3:50:40 PM 172.0 24.7
6/7/2019 3:50:41 PM 171.4 24.1
6/7/2019 3:50:42 PM 170.9 23.6
6/7/2019 3:50:43 PM 170.4 23.1
6/7/2019 3:50:44 PM 170.0 22.7
6/7/2019 3:50:45 PM 169.8 22.5
6/7/2019 3:50:46 PM 169.5 22.2
6/7/2019 3:50:47 PM 169.2 21.9
6/7/2019 3:50:48 PM 169.1 21.8
6/7/2019 3:50:49 PM 169.3 22.0
6/7/2019 3:50:50 PM 169.3 22.0
6/7/2019 3:50:51 PM 169.1 21.8
6/7/2019 3:50:52 PM 168.8 21.5
6/7/2019 3:50:53 PM 168.2 20.9
6/7/2019 3:50:54 PM 167.9 20.6
6/7/2019 3:50:55 PM 167.5 20.2
6/7/2019 3:50:56 PM 167.3 20.0
6/7/2019 3:50:57 PM 167.1 19.8
6/7/2019 3:50:58 PM 166.8 19.5
6/7/2019 3:50:59 PM 166.5 19.2
6/7/2019 3:51:00 PM 166.2 18.9
6/7/2019 3:51:01 PM 165.8 18.5
6/7/2019 3:51:02 PM 165.1 17.8
6/7/2019 3:51:03 PM 164.7 17.4
6/7/2019 3:51:04 PM 164.3 17.0
6/7/2019 3:51:05 PM 164.1 16.8
6/7/2019 3:51:06 PM 164.0 16.7
6/7/2019 3:51:07 PM 163.9 16.6
6/7/2019 3:51:08 PM 163.8 16.5
6/7/2019 3:51:09 PM 163.7 16.4
6/7/2019 3:51:10 PM 163.6 16.3
6/7/2019 3:51:11 PM 163.5 16.2
6/7/2019 3:51:12 PM 163.4 16.1
6/7/2019 3:51:13 PM 163.3 16.0
6/7/2019 3:51:14 PM 163.2 15.9
6/7/2019 3:51:15 PM 163.1 15.8
6/7/2019 3:51:16 PM 163.0 15.7
6/7/2019 3:51:17 PM 162.9 15.6
6/7/2019 3:51:18 PM 162.7 15.4
6/7/2019 3:51:19 PM 162.4 15.1
6/7/2019 3:51:20 PM 162.2 14.9
6/7/2019 3:51:21 PM 161.9 14.6
6/7/2019 3:51:22 PM 161.5 14.2
6/7/2019 3:51:23 PM 161.3 14.0
6/7/2019 3:51:24 PM 161.1 13.8
6/7/2019 3:51:25 PM 160.9 13.6
Page 193 of 452 August 2019
APPENDIX E40: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B1 TEST-1 Data Log
6/7/2019 3:51:26 PM 160.6 13.3
6/7/2019 3:51:27 PM 160.4 13.1
6/7/2019 3:51:28 PM 160.2 12.9
6/7/2019 3:51:29 PM 160.1 12.8
6/7/2019 3:51:30 PM 160.0 12.7
6/7/2019 3:51:31 PM 159.8 12.5
6/7/2019 3:51:32 PM 159.7 12.4
6/7/2019 3:51:33 PM 159.6 12.3
6/7/2019 3:51:34 PM 159.5 12.2
6/7/2019 3:51:35 PM 159.4 12.1
6/7/2019 3:51:36 PM 159.3 12.0
6/7/2019 3:51:37 PM 159.2 11.9
6/7/2019 3:51:38 PM 159.2 11.9
6/7/2019 3:51:39 PM 159.1 11.8
6/7/2019 3:51:40 PM 159.0 11.7
6/7/2019 3:51:41 PM 158.9 11.6
6/7/2019 3:51:42 PM 158.8 11.5
6/7/2019 3:51:43 PM 158.7 11.4
6/7/2019 3:51:44 PM 158.6 11.3
6/7/2019 3:51:45 PM 158.5 11.2
6/7/2019 3:51:46 PM 158.4 11.1
6/7/2019 3:51:47 PM 158.2 10.9
6/7/2019 3:51:48 PM 158.0 10.7
6/7/2019 3:51:49 PM 157.9 10.6
6/7/2019 3:51:50 PM 157.7 10.4
6/7/2019 3:51:51 PM 157.5 10.2
6/7/2019 3:51:52 PM 157.4 10.1
6/7/2019 3:51:53 PM 157.3 10.0
6/7/2019 3:51:54 PM 157.1 9.8
6/7/2019 3:51:55 PM 156.9 9.6
6/7/2019 3:51:56 PM 156.7 9.4
6/7/2019 3:51:57 PM 156.5 9.2
6/7/2019 3:51:58 PM 156.4 9.1
6/7/2019 3:51:59 PM 156.4 9.1
6/7/2019 3:52:00 PM 156.3 9.0
6/7/2019 3:52:01 PM 156.3 9.0
6/7/2019 3:52:02 PM 156.3 9.0
6/7/2019 3:52:03 PM 156.2 8.9
6/7/2019 3:52:04 PM 156.1 8.8
6/7/2019 3:52:05 PM 156.0 8.7
6/7/2019 3:52:06 PM 156.0 8.7
6/7/2019 3:52:07 PM 155.8 8.5
6/7/2019 3:52:08 PM 155.7 8.4
6/7/2019 3:52:09 PM 155.6 8.3
6/7/2019 3:52:10 PM 155.4 8.1
6/7/2019 3:52:11 PM 155.3 8.0
6/7/2019 3:52:12 PM 155.1 7.8
6/7/2019 3:52:13 PM 154.9 7.6
6/7/2019 3:52:14 PM 154.8 7.5
6/7/2019 3:52:15 PM 154.7 7.4
6/7/2019 3:52:16 PM 154.6 7.3
6/7/2019 3:52:17 PM 154.5 7.2
6/7/2019 3:52:18 PM 154.3 7.0
6/7/2019 3:52:19 PM 154.2 6.9
6/7/2019 3:52:20 PM 154.1 6.8
6/7/2019 3:52:21 PM 154.1 6.8
6/7/2019 3:52:22 PM 154.1 6.8
6/7/2019 3:52:23 PM 154.1 6.8
6/7/2019 3:52:24 PM 154.0 6.7
6/7/2019 3:52:25 PM 153.9 6.6
6/7/2019 3:52:26 PM 153.9 6.6
6/7/2019 3:52:27 PM 153.8 6.5
6/7/2019 3:52:28 PM 153.8 6.5
6/7/2019 3:52:29 PM 153.7 6.4
6/7/2019 3:52:30 PM 153.7 6.4
6/7/2019 3:52:31 PM 153.7 6.4
6/7/2019 3:52:32 PM 153.6 6.3
6/7/2019 3:52:33 PM 153.5 6.2
6/7/2019 3:52:34 PM 153.4 6.1
6/7/2019 3:52:35 PM 153.3 6.0
6/7/2019 3:52:36 PM 153.2 5.9
6/7/2019 3:52:37 PM 153.1 5.8
6/7/2019 3:52:38 PM 153.1 5.8
6/7/2019 3:52:39 PM 153.0 5.7
6/7/2019 3:52:40 PM 153.0 5.7
6/7/2019 3:52:41 PM 152.9 5.6
6/7/2019 3:52:42 PM 152.8 5.5
6/7/2019 3:52:43 PM 152.7 5.4
6/7/2019 3:52:44 PM 152.7 5.4
Page 194 of 452 August 2019
APPENDIX E40: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B1 TEST-1 Data Log
6/7/2019 3:52:45 PM 152.6 5.3
6/7/2019 3:52:46 PM 152.6 5.3
6/7/2019 3:52:47 PM 152.5 5.2
6/7/2019 3:52:48 PM 152.5 5.2
6/7/2019 3:52:49 PM 152.5 5.2
6/7/2019 3:52:50 PM 152.5 5.2
6/7/2019 3:52:51 PM 152.4 5.1
6/7/2019 3:52:52 PM 152.4 5.1
6/7/2019 3:52:53 PM 152.4 5.1
6/7/2019 3:52:54 PM 152.4 5.1
6/7/2019 3:52:55 PM 152.3 5.0
6/7/2019 3:52:56 PM 152.3 5.0
6/7/2019 3:52:57 PM 152.2 4.9
6/7/2019 3:52:58 PM 152.2 4.9
6/7/2019 3:52:59 PM 152.2 4.9
6/7/2019 3:53:00 PM 152.1 4.8
6/7/2019 3:53:01 PM 152.1 4.8
6/7/2019 3:53:02 PM 152.0 4.7
6/7/2019 3:53:03 PM 151.9 4.6
6/7/2019 3:53:04 PM 151.9 4.6
6/7/2019 3:53:05 PM 151.8 4.5
6/7/2019 3:53:06 PM 151.7 4.4
6/7/2019 3:53:07 PM 151.7 4.4
6/7/2019 3:53:08 PM 151.6 4.3
6/7/2019 3:53:09 PM 151.5 4.2
6/7/2019 3:53:10 PM 151.4 4.1
6/7/2019 3:53:11 PM 151.4 4.1
6/7/2019 3:53:12 PM 151.3 4.0
6/7/2019 3:53:13 PM 151.3 4.0
Page 195 of 452 August 2019
APPENDIX E40: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-B2 TEST-1 1542
SEEP-B2 TEST-1 1544
SEEP-B2 TEST-1 1544
Location EC Reading
(µS/cms)
SEEP-B2 TEST-1 638
SEEP-B2 TEST-1 2,108
SEEP-B2 TEST-1 16,969
SEEP-B2 TEST-1 124,451
q 300,500
K 1.2491
3.4
53.4
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)(°C)
Table E2 SEEP-B1 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
154.3 19.4
152.3 19.4
144.6 19.4
Average 150.4
Geo Mean 150.3 (µS/cms)
100 24.2
Average (pre-test)147.3 (µS/cms)
Average (post-test)153.9 (µS/cms)
Table E3 SEEP-B1 TEST-1 YSI Salt Dilution Calibration Data
Calibration Temperature
(mg/L)(°C)
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)111,552.4 (s) . (µS/cms)
1,000 24.2
10,000 24.1
100,000 24.1
Table E4 SEEP-B1 TEST-1 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Calculated Flow Rate Q
L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 196 of 452 August 2019
APPENDIX E41: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 4:01:18 PM 149.1 -
6/7/2019 4:01:19 PM 149.1 -
6/7/2019 4:01:20 PM 149.1 -
6/7/2019 4:01:21 PM 149.1 -
6/7/2019 4:01:22 PM 149.0 -
6/7/2019 4:01:23 PM 149.0 -
6/7/2019 4:01:24 PM 149.0 -
6/7/2019 4:01:25 PM 149.0 -
6/7/2019 4:01:26 PM 149.0 -
6/7/2019 4:01:27 PM 149.0 -
6/7/2019 4:01:28 PM 149.0 -
6/7/2019 4:01:29 PM 149.0 -
6/7/2019 4:01:30 PM 149.0 -
6/7/2019 4:01:31 PM 149.0 -
6/7/2019 4:01:32 PM 149.0 -
6/7/2019 4:01:33 PM 149.0 -
6/7/2019 4:01:34 PM 149.0 -
6/7/2019 4:01:35 PM 149.0 -
6/7/2019 4:01:36 PM 333.2 184.2
6/7/2019 4:01:37 PM 6377.6 6228.6
6/7/2019 4:01:38 PM 13556.8 13407.8
6/7/2019 4:01:39 PM 15508.0 15359.0
6/7/2019 4:01:40 PM 16638.9 16489.9
6/7/2019 4:01:41 PM 14536.2 14387.2
6/7/2019 4:01:42 PM 12145.7 11996.7
6/7/2019 4:01:43 PM 10224.5 10075.5
6/7/2019 4:01:44 PM 7899.1 7750.1
6/7/2019 4:01:45 PM 6461.5 6312.5
6/7/2019 4:01:46 PM 4205.5 4056.5
6/7/2019 4:01:47 PM 2817.5 2668.5
6/7/2019 4:01:48 PM 2159.6 2010.6
6/7/2019 4:01:49 PM 1900.7 1751.7
6/7/2019 4:01:50 PM 1546.8 1397.8
6/7/2019 4:01:51 PM 1492.7 1343.7
6/7/2019 4:01:52 PM 1153.7 1004.7
6/7/2019 4:01:53 PM 996.5 847.5
6/7/2019 4:01:54 PM 912.3 763.3
6/7/2019 4:01:55 PM 758.2 609.2
6/7/2019 4:01:56 PM 692.3 543.3
6/7/2019 4:01:57 PM 629.6 480.6
6/7/2019 4:01:58 PM 497.4 348.4
6/7/2019 4:01:59 PM 519.2 370.2
6/7/2019 4:02:00 PM 449.6 300.6
6/7/2019 4:02:01 PM 393.3 244.3
6/7/2019 4:02:02 PM 362.4 213.4
6/7/2019 4:02:03 PM 334.7 185.7
6/7/2019 4:02:04 PM 323.9 174.9
6/7/2019 4:02:05 PM 312.8 163.8
6/7/2019 4:02:06 PM 304.6 155.6
6/7/2019 4:02:07 PM 295.5 146.5
6/7/2019 4:02:08 PM 287.9 138.9
6/7/2019 4:02:09 PM 281.4 132.4
6/7/2019 4:02:10 PM 276.7 127.7
6/7/2019 4:02:11 PM 271.7 122.7
6/7/2019 4:02:12 PM 267.6 118.6
6/7/2019 4:02:13 PM 263.3 114.3
6/7/2019 4:02:14 PM 260.8 111.8
6/7/2019 4:02:15 PM 258.9 109.9
6/7/2019 4:02:16 PM 257.0 108.0
6/7/2019 4:02:17 PM 250.5 101.5
6/7/2019 4:02:18 PM 245.8 96.8
6/7/2019 4:02:19 PM 245.0 96.0
6/7/2019 4:02:20 PM 286.5 137.5
6/7/2019 4:02:21 PM 281.4 132.4
6/7/2019 4:02:22 PM 260.6 111.6
6/7/2019 4:02:23 PM 249.6 100.6
6/7/2019 4:02:24 PM 231.8 82.8
6/7/2019 4:02:25 PM 223.1 74.1
6/7/2019 4:02:26 PM 217.3 68.3
6/7/2019 4:02:27 PM 213.6 64.6
Table E1 SEEP-B1 TEST-2 Data Log
Page 197 of 452 August 2019
APPENDIX E41: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B1 TEST-2 Data Log
6/7/2019 4:02:28 PM 209.9 60.9
6/7/2019 4:02:29 PM 207.0 58.0
6/7/2019 4:02:30 PM 204.2 55.2
6/7/2019 4:02:31 PM 202.0 53.0
6/7/2019 4:02:32 PM 199.8 50.8
6/7/2019 4:02:33 PM 198.1 49.1
6/7/2019 4:02:34 PM 196.9 47.9
6/7/2019 4:02:35 PM 196.6 47.6
6/7/2019 4:02:36 PM 194.6 45.6
6/7/2019 4:02:37 PM 191.9 42.9
6/7/2019 4:02:38 PM 189.8 40.8
6/7/2019 4:02:39 PM 187.4 38.4
6/7/2019 4:02:40 PM 185.6 36.6
6/7/2019 4:02:41 PM 184.0 35.0
6/7/2019 4:02:42 PM 183.7 34.7
6/7/2019 4:02:43 PM 183.8 34.8
6/7/2019 4:02:44 PM 184.1 35.1
6/7/2019 4:02:45 PM 183.9 34.9
6/7/2019 4:02:46 PM 183.7 34.7
6/7/2019 4:02:47 PM 183.0 34.0
6/7/2019 4:02:48 PM 181.5 32.5
6/7/2019 4:02:49 PM 179.6 30.6
6/7/2019 4:02:50 PM 178.7 29.7
6/7/2019 4:02:51 PM 178.5 29.5
6/7/2019 4:02:52 PM 178.5 29.5
6/7/2019 4:02:53 PM 178.8 29.8
6/7/2019 4:02:54 PM 179.0 30.0
6/7/2019 4:02:55 PM 178.4 29.4
6/7/2019 4:02:56 PM 177.3 28.3
6/7/2019 4:02:57 PM 176.1 27.1
6/7/2019 4:02:58 PM 174.9 25.9
6/7/2019 4:02:59 PM 174.1 25.1
6/7/2019 4:03:00 PM 173.5 24.5
6/7/2019 4:03:01 PM 173.2 24.2
6/7/2019 4:03:02 PM 173.0 24.0
6/7/2019 4:03:03 PM 172.5 23.5
6/7/2019 4:03:04 PM 171.4 22.4
6/7/2019 4:03:05 PM 170.4 21.4
6/7/2019 4:03:06 PM 169.7 20.7
6/7/2019 4:03:07 PM 169.2 20.2
6/7/2019 4:03:08 PM 168.6 19.6
6/7/2019 4:03:09 PM 168.0 19.0
6/7/2019 4:03:10 PM 167.4 18.4
6/7/2019 4:03:11 PM 167.1 18.1
6/7/2019 4:03:12 PM 167.4 18.4
6/7/2019 4:03:13 PM 168.2 19.2
6/7/2019 4:03:14 PM 168.6 19.6
6/7/2019 4:03:15 PM 168.7 19.7
6/7/2019 4:03:16 PM 168.4 19.4
6/7/2019 4:03:17 PM 168.1 19.1
6/7/2019 4:03:18 PM 168.0 19.0
6/7/2019 4:03:19 PM 167.6 18.6
6/7/2019 4:03:20 PM 167.5 18.5
6/7/2019 4:03:21 PM 167.4 18.4
6/7/2019 4:03:22 PM 167.2 18.2
6/7/2019 4:03:23 PM 167.2 18.2
6/7/2019 4:03:24 PM 167.2 18.2
6/7/2019 4:03:25 PM 166.4 17.4
6/7/2019 4:03:26 PM 165.1 16.1
6/7/2019 4:03:27 PM 164.2 15.2
6/7/2019 4:03:28 PM 163.7 14.7
6/7/2019 4:03:29 PM 163.2 14.2
6/7/2019 4:03:30 PM 162.9 13.9
6/7/2019 4:03:31 PM 162.6 13.6
6/7/2019 4:03:32 PM 162.3 13.3
6/7/2019 4:03:33 PM 161.6 12.6
6/7/2019 4:03:34 PM 160.9 11.9
6/7/2019 4:03:35 PM 160.5 11.5
6/7/2019 4:03:36 PM 159.9 10.9
6/7/2019 4:03:37 PM 159.5 10.5
6/7/2019 4:03:38 PM 159.1 10.1
6/7/2019 4:03:39 PM 158.9 9.9
6/7/2019 4:03:40 PM 158.6 9.6
6/7/2019 4:03:41 PM 158.3 9.3
6/7/2019 4:03:42 PM 158.2 9.2
6/7/2019 4:03:43 PM 158.1 9.1
6/7/2019 4:03:44 PM 158.0 9.0
Page 198 of 452 August 2019
APPENDIX E41: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B1 TEST-2 Data Log
6/7/2019 4:03:45 PM 157.9 8.9
6/7/2019 4:03:46 PM 157.9 8.9
6/7/2019 4:03:47 PM 157.8 8.8
6/7/2019 4:03:48 PM 157.5 8.5
6/7/2019 4:03:49 PM 157.3 8.3
6/7/2019 4:03:50 PM 157.2 8.2
6/7/2019 4:03:51 PM 157.2 8.2
6/7/2019 4:03:52 PM 157.3 8.3
6/7/2019 4:03:53 PM 157.5 8.5
6/7/2019 4:03:54 PM 157.5 8.5
6/7/2019 4:03:55 PM 157.4 8.4
6/7/2019 4:03:56 PM 157.2 8.2
6/7/2019 4:03:57 PM 157.1 8.1
6/7/2019 4:03:58 PM 156.9 7.9
6/7/2019 4:03:59 PM 156.8 7.8
6/7/2019 4:04:00 PM 156.7 7.7
6/7/2019 4:04:01 PM 156.5 7.5
6/7/2019 4:04:02 PM 156.3 7.3
6/7/2019 4:04:03 PM 156.2 7.2
6/7/2019 4:04:04 PM 156.1 7.1
6/7/2019 4:04:05 PM 156.0 7.0
6/7/2019 4:04:06 PM 155.7 6.7
6/7/2019 4:04:07 PM 155.5 6.5
6/7/2019 4:04:08 PM 155.4 6.4
6/7/2019 4:04:09 PM 155.2 6.2
6/7/2019 4:04:10 PM 155.2 6.2
6/7/2019 4:04:11 PM 155.2 6.2
6/7/2019 4:04:12 PM 155.2 6.2
6/7/2019 4:04:13 PM 155.2 6.2
6/7/2019 4:04:14 PM 155.3 6.3
6/7/2019 4:04:15 PM 155.2 6.2
6/7/2019 4:04:16 PM 155.2 6.2
6/7/2019 4:04:17 PM 155.1 6.1
6/7/2019 4:04:18 PM 155.0 6.0
6/7/2019 4:04:19 PM 154.9 5.9
6/7/2019 4:04:20 PM 154.8 5.8
6/7/2019 4:04:21 PM 154.7 5.7
6/7/2019 4:04:22 PM 154.6 5.6
6/7/2019 4:04:23 PM 154.6 5.6
6/7/2019 4:04:24 PM 154.5 5.5
6/7/2019 4:04:25 PM 154.4 5.4
6/7/2019 4:04:26 PM 154.2 5.2
6/7/2019 4:04:27 PM 154.1 5.1
6/7/2019 4:04:28 PM 154.0 5.0
6/7/2019 4:04:29 PM 153.8 4.8
6/7/2019 4:04:30 PM 153.8 4.8
6/7/2019 4:04:31 PM 153.9 4.9
6/7/2019 4:04:32 PM 154.0 5.0
6/7/2019 4:04:33 PM 154.1 5.1
6/7/2019 4:04:34 PM 154.0 5.0
6/7/2019 4:04:34 PM 153.9 0.0
6/7/2019 4:04:35 PM 153.8 4.8
6/7/2019 4:04:36 PM 153.7 4.7
6/7/2019 4:04:37 PM 153.6 4.6
6/7/2019 4:04:38 PM 153.6 4.6
6/7/2019 4:04:39 PM 153.5 4.5
6/7/2019 4:04:40 PM 153.5 4.5
6/7/2019 4:04:41 PM 153.4 4.4
6/7/2019 4:04:42 PM 153.2 4.2
6/7/2019 4:04:43 PM 152.9 3.9
6/7/2019 4:04:44 PM 152.6 3.6
6/7/2019 4:04:45 PM 152.4 3.4
6/7/2019 4:04:46 PM 152.3 3.3
Page 199 of 452 August 2019
APPENDIX E41: SALT DILUTION GAUGING SUMMARY
SEEP-B1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-B1 TEST-2 1542
SEEP-B1 TEST-2 1544
SEEP-B1 TEST-2 1544
Location EC Reading
(µS/cms)
SEEP-B1 TEST-2 638
SEEP-B1 TEST-2 2,108
SEEP-B1 TEST-2 16,969
SEEP-B1 TEST-2 124,451
q 300,400
K 1.2491
3.0
47.1
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)(°C)
Table E2 SEEP-B1 TEST-2 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
154.3 19.4
152.3 19.4
144.6 19.4
Average 150.4
Geo Mean 150.3 (µS/cms)
100 24.2
Average (pre-test)149.0 (µS/cms)
Average (post-test)155.2 (µS/cms)
Table E3 SEEP-B1 TEST-2 YSI Salt Dilution Calibration Data
Calibration
Concentration Temperature
(mg/L)(°C)
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)126,464.1 (s) . (µS/cms)
1,000 24.2
10,000 24.1
100,000 24.1
Table E4 SEEP-B1 TEST-2 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Calculated Flow Rate Q
L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline,
Watershed Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 200 of 452 August 2019
APPENDIX E42: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/5/2019 3:28:51 PM 97.5 -
2/5/2019 3:28:52 PM 97.6 -
2/5/2019 3:28:53 PM 97.6 -
2/5/2019 3:28:54 PM 97.6 -
2/5/2019 3:28:55 PM 97.5 -
2/5/2019 3:28:56 PM 97.5 -
2/5/2019 3:28:57 PM 97.4 -
2/5/2019 3:28:58 PM 97.4 -
2/5/2019 3:28:59 PM 97.3 -
2/5/2019 3:29:00 PM 97.2 -
2/5/2019 3:29:01 PM 97.1 -
2/5/2019 3:29:02 PM 97.0 -
2/5/2019 3:29:03 PM 97.0 -
2/5/2019 3:29:04 PM 97.0 -
2/5/2019 3:29:05 PM 96.9 -
2/5/2019 3:29:06 PM 96.9 -
2/5/2019 3:29:07 PM 96.8 -
2/5/2019 3:29:08 PM 96.8 -
2/5/2019 3:29:09 PM 96.8 -
2/5/2019 3:29:10 PM 96.8 -
2/5/2019 3:29:11 PM 96.8 -
2/5/2019 3:29:12 PM 96.9 -
2/5/2019 3:29:13 PM 96.9 -
2/5/2019 3:29:14 PM 97.0 -
2/5/2019 3:29:15 PM 97.0 -
2/5/2019 3:29:16 PM 97.0 -
2/5/2019 3:29:17 PM 97.0 -
2/5/2019 3:29:18 PM 97.0 -
2/5/2019 3:29:19 PM 97.0 -
2/5/2019 3:29:20 PM 97.0 -
2/5/2019 3:29:21 PM 97.0 -
2/5/2019 3:29:22 PM 97.1 -
2/5/2019 3:29:23 PM 97.1 -
2/5/2019 3:29:24 PM 97.0 -
2/5/2019 3:29:25 PM 97.0 -
2/5/2019 3:29:26 PM 97.0 -
2/5/2019 3:29:27 PM 97.0 -
2/5/2019 3:29:28 PM 97.0 -
2/5/2019 3:29:29 PM 97.1 -
2/5/2019 3:29:30 PM 97.1 -
2/5/2019 3:29:31 PM 97.2 0.1
2/5/2019 3:29:32 PM 97.2 0.1
2/5/2019 3:29:33 PM 97.3 0.2
2/5/2019 3:29:34 PM 97.6 0.5
2/5/2019 3:29:35 PM 97.9 0.8
2/5/2019 3:29:36 PM 98.4 1.3
2/5/2019 3:29:37 PM 99.1 2.0
2/5/2019 3:29:38 PM 100.2 3.1
2/5/2019 3:29:39 PM 101.6 4.5
2/5/2019 3:29:40 PM 104.2 7.1
2/5/2019 3:29:41 PM 107.5 10.4
2/5/2019 3:29:42 PM 191.3 94.2
2/5/2019 3:29:43 PM 221.4 124.3
2/5/2019 3:29:44 PM 282.6 185.5
2/5/2019 3:29:45 PM 300.6 203.5
2/5/2019 3:29:46 PM 385.5 288.4
2/5/2019 3:29:47 PM 467.1 370.0
2/5/2019 3:29:48 PM 581.6 484.5
2/5/2019 3:29:49 PM 683.6 586.5
2/5/2019 3:29:50 PM 822.3 725.2
2/5/2019 3:29:51 PM 966.3 869.2
2/5/2019 3:29:52 PM 1094.0 996.9
2/5/2019 3:29:53 PM 1294.8 1197.7
2/5/2019 3:29:54 PM 1506.8 1409.7
2/5/2019 3:29:55 PM 1621.0 1523.9
2/5/2019 3:29:56 PM 1736.5 1639.4
2/5/2019 3:29:57 PM 1781.6 1684.5
2/5/2019 3:29:58 PM 1970.7 1873.6
2/5/2019 3:29:59 PM 2133.2 2036.1
2/5/2019 3:30:00 PM 2228.6 2131.5
Table E1 SEEP-B2 TEST-1 Data Log
Page 201 of 452 August 2019
APPENDIX E42: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
2/5/2019 3:30:01 PM 2300.1 2203.0
2/5/2019 3:30:02 PM 2355.7 2258.6
2/5/2019 3:30:03 PM 2563.5 2466.4
2/5/2019 3:30:04 PM 2625.8 2528.7
2/5/2019 3:30:05 PM 2676.0 2578.9
2/5/2019 3:30:06 PM 2720.7 2623.6
2/5/2019 3:30:07 PM 2744.5 2647.4
2/5/2019 3:30:08 PM 2761.5 2664.4
2/5/2019 3:30:09 PM 2775.3 2678.2
2/5/2019 3:30:10 PM 2787.6 2690.5
2/5/2019 3:30:11 PM 2805.5 2708.4
2/5/2019 3:30:12 PM 2822.1 2725.0
2/5/2019 3:30:13 PM 2837.9 2740.8
2/5/2019 3:30:14 PM 2849.9 2752.8
2/5/2019 3:30:15 PM 2860.5 2763.4
2/5/2019 3:30:16 PM 2867.7 2770.6
2/5/2019 3:30:17 PM 2874.5 2777.4
2/5/2019 3:30:18 PM 2879.0 2781.9
2/5/2019 3:30:19 PM 2881.7 2784.6
2/5/2019 3:30:20 PM 2894.4 2797.3
2/5/2019 3:30:21 PM 2899.5 2802.4
2/5/2019 3:30:22 PM 2903.3 2806.2
2/5/2019 3:30:23 PM 2902.4 2805.3
2/5/2019 3:30:24 PM 2896.0 2798.9
2/5/2019 3:30:25 PM 2710.5 2613.4
2/5/2019 3:30:26 PM 2684.2 2587.1
2/5/2019 3:30:27 PM 2645.4 2548.3
2/5/2019 3:30:28 PM 2637.4 2540.3
2/5/2019 3:30:29 PM 2615.8 2518.7
2/5/2019 3:30:30 PM 2601.9 2504.8
2/5/2019 3:30:31 PM 2586.4 2489.3
2/5/2019 3:30:32 PM 2570.2 2473.1
2/5/2019 3:30:33 PM 2547.1 2450.0
2/5/2019 3:30:34 PM 2369.6 2272.5
2/5/2019 3:30:35 PM 2321.5 2224.4
2/5/2019 3:30:36 PM 2265.2 2168.1
2/5/2019 3:30:37 PM 2228.1 2131.0
2/5/2019 3:30:38 PM 2167.6 2070.5
2/5/2019 3:30:39 PM 2125.4 2028.3
2/5/2019 3:30:40 PM 2099.0 2001.9
2/5/2019 3:30:41 PM 1940.9 1843.8
2/5/2019 3:30:42 PM 1895.3 1798.2
2/5/2019 3:30:43 PM 1849.4 1752.3
2/5/2019 3:30:44 PM 1838.3 1741.2
2/5/2019 3:30:45 PM 1803.3 1706.2
2/5/2019 3:30:46 PM 1780.2 1683.1
2/5/2019 3:30:47 PM 1759.6 1662.5
2/5/2019 3:30:48 PM 1742.0 1644.9
2/5/2019 3:30:49 PM 1631.0 1533.9
2/5/2019 3:30:50 PM 1612.0 1514.9
2/5/2019 3:30:51 PM 1595.5 1498.4
2/5/2019 3:30:52 PM 1578.4 1481.3
2/5/2019 3:30:53 PM 1563.2 1466.1
2/5/2019 3:30:54 PM 1543.3 1446.2
2/5/2019 3:30:55 PM 1529.3 1432.2
2/5/2019 3:30:56 PM 1507.8 1410.7
2/5/2019 3:30:57 PM 1405.6 1308.5
2/5/2019 3:30:58 PM 1378.4 1281.3
2/5/2019 3:30:59 PM 1357.8 1260.7
2/5/2019 3:31:00 PM 1351.0 1253.9
2/5/2019 3:31:01 PM 1338.4 1241.3
2/5/2019 3:31:02 PM 1325.8 1228.7
2/5/2019 3:31:03 PM 1316.2 1219.1
2/5/2019 3:31:04 PM 1305.6 1208.5
2/5/2019 3:31:05 PM 1296.3 1199.2
2/5/2019 3:31:06 PM 1287.4 1190.3
2/5/2019 3:31:07 PM 1280.4 1183.3
2/5/2019 3:31:08 PM 1197.8 1100.7
2/5/2019 3:31:09 PM 1178.2 1081.1
2/5/2019 3:31:10 PM 1160.9 1063.8
2/5/2019 3:31:11 PM 1152.5 1055.4
2/5/2019 3:31:12 PM 1142.7 1045.6
2/5/2019 3:31:13 PM 1136.3 1039.2
2/5/2019 3:31:14 PM 1130.3 1033.2
2/5/2019 3:31:15 PM 1125.5 1028.4
2/5/2019 3:31:16 PM 1120.2 1023.1
2/5/2019 3:31:17 PM 1114.5 1017.4
Page 202 of 452 August 2019
APPENDIX E42: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
2/5/2019 3:31:18 PM 1109.1 1012.0
2/5/2019 3:31:19 PM 1104.7 1007.6
2/5/2019 3:31:20 PM 1099.2 1002.1
2/5/2019 3:31:21 PM 1095.1 998.0
2/5/2019 3:31:22 PM 1012.0 914.9
2/5/2019 3:31:23 PM 1001.4 904.3
2/5/2019 3:31:24 PM 978.9 881.8
2/5/2019 3:31:25 PM 969.9 872.8
2/5/2019 3:31:26 PM 952.6 855.5
2/5/2019 3:31:27 PM 940.0 842.9
2/5/2019 3:31:28 PM 889.6 792.5
2/5/2019 3:31:29 PM 873.2 776.1
2/5/2019 3:31:30 PM 862.3 765.2
2/5/2019 3:31:31 PM 854.3 757.2
2/5/2019 3:31:32 PM 844.6 747.5
2/5/2019 3:31:33 PM 838.4 741.3
2/5/2019 3:31:34 PM 833.0 735.9
2/5/2019 3:31:35 PM 827.6 730.5
2/5/2019 3:31:36 PM 822.4 725.3
2/5/2019 3:31:37 PM 817.3 720.2
2/5/2019 3:31:38 PM 812.4 715.3
2/5/2019 3:31:39 PM 763.4 666.3
2/5/2019 3:31:40 PM 751.1 654.0
2/5/2019 3:31:41 PM 737.2 640.1
2/5/2019 3:31:42 PM 724.9 627.8
2/5/2019 3:31:43 PM 723.0 625.9
2/5/2019 3:31:44 PM 720.3 623.2
2/5/2019 3:31:45 PM 714.8 617.7
2/5/2019 3:31:46 PM 709.7 612.6
2/5/2019 3:31:47 PM 705.1 608.0
2/5/2019 3:31:48 PM 702.8 605.7
2/5/2019 3:31:49 PM 618.8 521.7
2/5/2019 3:31:50 PM 628.5 531.4
2/5/2019 3:31:51 PM 618.9 521.8
2/5/2019 3:31:52 PM 613.9 516.8
2/5/2019 3:31:53 PM 605.4 508.3
2/5/2019 3:31:54 PM 598.7 501.6
2/5/2019 3:31:55 PM 591.3 494.2
2/5/2019 3:31:56 PM 584.9 487.8
2/5/2019 3:31:57 PM 578.3 481.2
2/5/2019 3:31:58 PM 572.9 475.8
2/5/2019 3:31:59 PM 567.3 470.2
2/5/2019 3:32:00 PM 562.5 465.4
2/5/2019 3:32:01 PM 557.4 460.3
2/5/2019 3:32:02 PM 505.5 408.4
2/5/2019 3:32:03 PM 496.8 399.7
2/5/2019 3:32:04 PM 490.5 393.4
2/5/2019 3:32:05 PM 485.4 388.3
2/5/2019 3:32:06 PM 479.9 382.8
2/5/2019 3:32:07 PM 474.7 377.6
2/5/2019 3:32:08 PM 471.2 374.1
2/5/2019 3:32:09 PM 467.5 370.4
2/5/2019 3:32:10 PM 464.1 367.0
2/5/2019 3:32:11 PM 460.3 363.2
2/5/2019 3:32:12 PM 457.1 360.0
2/5/2019 3:32:13 PM 453.6 356.5
2/5/2019 3:32:14 PM 450.6 353.5
2/5/2019 3:32:15 PM 447.2 350.1
2/5/2019 3:32:16 PM 444.2 347.1
2/5/2019 3:32:17 PM 440.9 343.8
2/5/2019 3:32:18 PM 437.5 340.4
2/5/2019 3:32:19 PM 430.8 333.7
2/5/2019 3:32:20 PM 425.0 327.9
2/5/2019 3:32:21 PM 418.4 321.3
2/5/2019 3:32:22 PM 412.9 315.8
2/5/2019 3:32:23 PM 406.9 309.8
2/5/2019 3:32:24 PM 401.0 303.9
2/5/2019 3:32:25 PM 396.0 298.9
2/5/2019 3:32:26 PM 390.5 293.4
2/5/2019 3:32:27 PM 385.7 288.6
2/5/2019 3:32:28 PM 380.4 283.3
2/5/2019 3:32:29 PM 376.1 279.0
2/5/2019 3:32:30 PM 371.3 274.2
2/5/2019 3:32:31 PM 367.2 270.1
2/5/2019 3:32:32 PM 362.7 265.6
2/5/2019 3:32:33 PM 359.0 261.9
2/5/2019 3:32:34 PM 354.9 257.8
2/5/2019 3:32:35 PM 351.4 254.3
2/5/2019 3:32:36 PM 347.6 250.5
Page 203 of 452 August 2019
APPENDIX E42: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
2/5/2019 3:32:37 PM 344.4 247.3
2/5/2019 3:32:38 PM 340.9 243.8
2/5/2019 3:32:39 PM 338.0 240.9
2/5/2019 3:32:40 PM 334.6 237.5
2/5/2019 3:32:41 PM 331.8 234.7
2/5/2019 3:32:42 PM 328.6 231.5
2/5/2019 3:32:43 PM 325.8 228.7
2/5/2019 3:32:44 PM 322.8 225.7
2/5/2019 3:32:45 PM 320.1 223.0
2/5/2019 3:32:46 PM 317.1 220.0
2/5/2019 3:32:47 PM 314.5 217.4
2/5/2019 3:32:48 PM 311.5 214.4
2/5/2019 3:32:49 PM 308.8 211.7
2/5/2019 3:32:50 PM 305.7 208.6
2/5/2019 3:32:51 PM 303.0 205.9
2/5/2019 3:32:52 PM 300.0 202.9
2/5/2019 3:32:53 PM 297.4 200.3
2/5/2019 3:32:54 PM 294.6 197.5
2/5/2019 3:32:55 PM 292.1 195.0
2/5/2019 3:32:56 PM 289.4 192.3
2/5/2019 3:32:57 PM 287.0 189.9
2/5/2019 3:32:58 PM 284.4 187.3
2/5/2019 3:32:59 PM 282.2 185.1
2/5/2019 3:33:00 PM 279.7 182.6
2/5/2019 3:33:01 PM 277.5 180.4
2/5/2019 3:33:02 PM 275.2 178.1
2/5/2019 3:33:03 PM 273.2 176.1
2/5/2019 3:33:04 PM 271.0 173.9
2/5/2019 3:33:05 PM 269.1 172.0
2/5/2019 3:33:06 PM 267.0 169.9
2/5/2019 3:33:07 PM 265.1 168.0
2/5/2019 3:33:08 PM 263.1 166.0
2/5/2019 3:33:09 PM 261.3 164.2
2/5/2019 3:33:10 PM 259.3 162.2
2/5/2019 3:33:11 PM 257.6 160.5
2/5/2019 3:33:12 PM 255.6 158.5
2/5/2019 3:33:13 PM 253.9 156.8
2/5/2019 3:33:14 PM 252.0 154.9
2/5/2019 3:33:15 PM 250.4 153.3
2/5/2019 3:33:16 PM 248.6 151.5
2/5/2019 3:33:17 PM 247.0 149.9
2/5/2019 3:33:18 PM 245.2 148.1
2/5/2019 3:33:19 PM 243.7 146.6
2/5/2019 3:33:20 PM 242.0 144.9
2/5/2019 3:33:21 PM 240.5 143.4
2/5/2019 3:33:22 PM 238.8 141.7
2/5/2019 3:33:23 PM 237.1 140.0
2/5/2019 3:33:24 PM 235.7 138.6
2/5/2019 3:33:25 PM 234.1 137.0
2/5/2019 3:33:26 PM 232.8 135.7
2/5/2019 3:33:27 PM 231.3 134.2
2/5/2019 3:33:28 PM 230.1 133.0
2/5/2019 3:33:29 PM 228.6 131.5
2/5/2019 3:33:30 PM 227.4 130.3
2/5/2019 3:33:31 PM 226.1 129.0
2/5/2019 3:33:32 PM 224.9 127.8
2/5/2019 3:33:33 PM 223.5 126.4
2/5/2019 3:33:34 PM 222.4 125.3
2/5/2019 3:33:35 PM 221.1 124.0
2/5/2019 3:33:36 PM 220.0 122.9
2/5/2019 3:33:37 PM 218.9 121.8
2/5/2019 3:33:38 PM 217.9 120.8
2/5/2019 3:33:39 PM 216.8 119.7
2/5/2019 3:33:40 PM 215.9 118.8
2/5/2019 3:33:41 PM 214.8 117.7
2/5/2019 3:33:42 PM 213.9 116.8
2/5/2019 3:33:43 PM 212.9 115.8
2/5/2019 3:33:44 PM 212.0 114.9
2/5/2019 3:33:45 PM 211.0 113.9
2/5/2019 3:33:46 PM 210.1 113.0
2/5/2019 3:33:47 PM 209.1 112.0
2/5/2019 3:33:48 PM 208.3 111.2
2/5/2019 3:33:49 PM 207.3 110.2
2/5/2019 3:33:50 PM 206.5 109.4
2/5/2019 3:33:51 PM 205.5 108.4
2/5/2019 3:33:52 PM 204.5 107.4
2/5/2019 3:33:53 PM 203.7 106.6
2/5/2019 3:33:54 PM 202.7 105.6
2/5/2019 3:33:55 PM 201.7 104.6
Page 204 of 452 August 2019
APPENDIX E42: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
2/5/2019 3:33:56 PM 200.8 103.7
2/5/2019 3:33:57 PM 199.9 102.8
2/5/2019 3:33:58 PM 199.0 101.9
2/5/2019 3:33:59 PM 198.0 100.9
2/5/2019 3:34:00 PM 197.1 100.0
2/5/2019 3:34:01 PM 196.1 99.0
2/5/2019 3:34:02 PM 195.2 98.1
2/5/2019 3:34:03 PM 194.2 97.1
2/5/2019 3:34:04 PM 193.3 96.2
2/5/2019 3:34:05 PM 192.3 95.2
2/5/2019 3:34:06 PM 191.5 94.4
2/5/2019 3:34:07 PM 190.5 93.4
2/5/2019 3:34:08 PM 189.7 92.6
2/5/2019 3:34:09 PM 188.8 91.7
2/5/2019 3:34:10 PM 188.0 90.9
2/5/2019 3:34:11 PM 187.2 90.1
2/5/2019 3:34:12 PM 186.5 89.4
2/5/2019 3:34:13 PM 185.6 88.5
2/5/2019 3:34:14 PM 184.9 87.8
2/5/2019 3:34:15 PM 184.0 86.9
2/5/2019 3:34:16 PM 183.3 86.2
2/5/2019 3:34:17 PM 182.5 85.4
2/5/2019 3:34:18 PM 181.7 84.6
2/5/2019 3:34:19 PM 180.9 83.8
2/5/2019 3:34:20 PM 180.2 83.1
2/5/2019 3:34:21 PM 179.4 82.3
2/5/2019 3:34:22 PM 178.7 81.6
2/5/2019 3:34:23 PM 177.9 80.8
2/5/2019 3:34:24 PM 177.3 80.2
2/5/2019 3:34:25 PM 176.5 79.4
2/5/2019 3:34:26 PM 175.9 78.8
2/5/2019 3:34:27 PM 175.2 78.1
2/5/2019 3:34:28 PM 174.6 77.5
2/5/2019 3:34:29 PM 173.9 76.8
2/5/2019 3:34:30 PM 173.3 76.2
2/5/2019 3:34:31 PM 172.6 75.5
2/5/2019 3:34:32 PM 172.0 74.9
2/5/2019 3:34:33 PM 171.4 74.3
2/5/2019 3:34:34 PM 170.7 73.6
2/5/2019 3:34:35 PM 170.1 73.0
2/5/2019 3:34:36 PM 169.5 72.4
2/5/2019 3:34:37 PM 168.9 71.8
2/5/2019 3:34:38 PM 168.3 71.2
2/5/2019 3:34:39 PM 167.7 70.6
2/5/2019 3:34:40 PM 167.1 70.0
2/5/2019 3:34:41 PM 166.5 69.4
2/5/2019 3:34:42 PM 165.8 68.7
2/5/2019 3:34:43 PM 165.3 68.2
2/5/2019 3:34:44 PM 164.6 67.5
2/5/2019 3:34:45 PM 164.1 67.0
2/5/2019 3:34:46 PM 163.4 66.3
2/5/2019 3:34:47 PM 162.9 65.8
2/5/2019 3:34:48 PM 162.2 65.1
2/5/2019 3:34:49 PM 161.7 64.6
2/5/2019 3:34:50 PM 161.1 64.0
2/5/2019 3:34:51 PM 160.5 63.4
2/5/2019 3:34:52 PM 159.9 62.8
2/5/2019 3:34:53 PM 159.3 62.2
2/5/2019 3:34:54 PM 158.7 61.6
2/5/2019 3:34:55 PM 158.2 61.1
2/5/2019 3:34:56 PM 157.6 60.5
2/5/2019 3:34:57 PM 157.1 60.0
2/5/2019 3:34:58 PM 156.5 59.4
2/5/2019 3:34:59 PM 156.1 59.0
2/5/2019 3:35:00 PM 155.5 58.4
2/5/2019 3:35:01 PM 155.1 58.0
2/5/2019 3:35:02 PM 154.5 57.4
2/5/2019 3:35:03 PM 154.1 57.0
2/5/2019 3:35:04 PM 153.6 56.5
2/5/2019 3:35:05 PM 153.2 56.1
2/5/2019 3:35:06 PM 152.7 55.6
2/5/2019 3:35:07 PM 152.3 55.2
2/5/2019 3:35:08 PM 151.9 54.8
2/5/2019 3:35:09 PM 151.5 54.4
2/5/2019 3:35:10 PM 151.1 54.0
2/5/2019 3:35:11 PM 150.8 53.7
2/5/2019 3:35:12 PM 150.3 53.2
2/5/2019 3:35:13 PM 150.0 52.9
2/5/2019 3:35:14 PM 149.6 52.5
Page 205 of 452 August 2019
APPENDIX E42: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
2/5/2019 3:35:15 PM 149.2 52.1
2/5/2019 3:35:16 PM 148.8 51.7
2/5/2019 3:35:17 PM 148.4 51.3
2/5/2019 3:35:18 PM 148.0 50.9
2/5/2019 3:35:19 PM 147.6 50.5
2/5/2019 3:35:20 PM 147.1 50.0
2/5/2019 3:35:21 PM 146.7 49.6
2/5/2019 3:35:22 PM 146.3 49.2
2/5/2019 3:35:23 PM 145.9 48.8
2/5/2019 3:35:24 PM 145.4 48.3
2/5/2019 3:35:25 PM 145.0 47.9
2/5/2019 3:35:26 PM 144.6 47.5
2/5/2019 3:35:27 PM 144.2 47.1
2/5/2019 3:35:28 PM 143.9 46.8
2/5/2019 3:35:29 PM 143.5 46.4
2/5/2019 3:35:30 PM 143.1 46.0
2/5/2019 3:35:31 PM 142.8 45.7
2/5/2019 3:35:32 PM 142.5 45.4
2/5/2019 3:35:33 PM 142.2 45.1
2/5/2019 3:35:34 PM 141.9 44.8
2/5/2019 3:35:35 PM 141.6 44.5
2/5/2019 3:35:36 PM 141.3 44.2
2/5/2019 3:35:37 PM 141.0 43.9
2/5/2019 3:35:38 PM 140.7 43.6
2/5/2019 3:35:39 PM 140.4 43.3
2/5/2019 3:35:40 PM 140.1 43.0
2/5/2019 3:35:41 PM 139.8 42.7
2/5/2019 3:35:42 PM 139.5 42.4
2/5/2019 3:35:43 PM 139.2 42.1
2/5/2019 3:35:44 PM 139.0 41.9
2/5/2019 3:35:45 PM 138.7 41.6
2/5/2019 3:35:46 PM 138.4 41.3
2/5/2019 3:35:47 PM 138.1 41.0
2/5/2019 3:35:48 PM 137.8 40.7
2/5/2019 3:35:49 PM 137.5 40.4
2/5/2019 3:35:50 PM 137.2 40.1
2/5/2019 3:35:51 PM 136.9 39.8
2/5/2019 3:35:52 PM 136.6 39.5
2/5/2019 3:35:53 PM 136.3 39.2
2/5/2019 3:35:54 PM 136.0 38.9
2/5/2019 3:35:55 PM 135.6 38.5
2/5/2019 3:35:56 PM 135.3 38.2
2/5/2019 3:35:57 PM 135.0 37.9
2/5/2019 3:35:58 PM 134.7 37.6
2/5/2019 3:35:59 PM 134.3 37.2
2/5/2019 3:36:00 PM 134.0 36.9
2/5/2019 3:36:01 PM 133.7 36.6
2/5/2019 3:36:02 PM 133.4 36.3
2/5/2019 3:36:03 PM 133.0 35.9
2/5/2019 3:36:04 PM 132.7 35.6
2/5/2019 3:36:05 PM 132.4 35.3
2/5/2019 3:36:06 PM 132.1 35.0
2/5/2019 3:36:07 PM 131.8 34.7
2/5/2019 3:36:08 PM 131.5 34.4
2/5/2019 3:36:09 PM 131.2 34.1
2/5/2019 3:36:10 PM 130.9 33.8
2/5/2019 3:36:11 PM 130.6 33.5
2/5/2019 3:36:12 PM 130.3 33.2
2/5/2019 3:36:13 PM 130.0 32.9
2/5/2019 3:36:14 PM 129.7 32.6
2/5/2019 3:36:15 PM 129.4 32.3
2/5/2019 3:36:16 PM 129.1 32.0
2/5/2019 3:36:17 PM 128.9 31.8
2/5/2019 3:36:18 PM 128.6 31.5
2/5/2019 3:36:19 PM 128.4 31.3
2/5/2019 3:36:20 PM 128.1 31.0
2/5/2019 3:36:21 PM 127.9 30.8
2/5/2019 3:36:22 PM 127.6 30.5
2/5/2019 3:36:23 PM 127.4 30.3
2/5/2019 3:36:24 PM 127.1 30.0
2/5/2019 3:36:25 PM 126.9 29.8
2/5/2019 3:36:26 PM 126.6 29.5
2/5/2019 3:36:27 PM 126.4 29.3
2/5/2019 3:36:28 PM 126.1 29.0
2/5/2019 3:36:29 PM 125.8 28.7
2/5/2019 3:36:30 PM 125.6 28.5
2/5/2019 3:36:31 PM 125.3 28.2
2/5/2019 3:36:32 PM 125.1 28.0
2/5/2019 3:36:33 PM 124.8 27.7
Page 206 of 452 August 2019
APPENDIX E42: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
2/5/2019 3:36:34 PM 124.6 27.5
2/5/2019 3:36:35 PM 124.3 27.2
2/5/2019 3:36:36 PM 124.1 27.0
2/5/2019 3:36:37 PM 123.8 26.7
2/5/2019 3:36:38 PM 123.5 26.4
2/5/2019 3:36:39 PM 123.3 26.2
2/5/2019 3:36:40 PM 123.1 26.0
2/5/2019 3:36:41 PM 122.8 25.7
2/5/2019 3:36:42 PM 122.6 25.5
2/5/2019 3:36:43 PM 122.3 25.2
2/5/2019 3:36:44 PM 122.1 25.0
2/5/2019 3:36:45 PM 121.9 24.8
2/5/2019 3:36:46 PM 121.6 24.5
2/5/2019 3:36:47 PM 121.4 24.3
2/5/2019 3:36:48 PM 121.2 24.1
2/5/2019 3:36:49 PM 121.0 23.9
2/5/2019 3:36:50 PM 120.7 23.6
2/5/2019 3:36:51 PM 120.6 23.5
2/5/2019 3:36:52 PM 120.3 23.2
2/5/2019 3:36:53 PM 120.2 23.1
2/5/2019 3:36:54 PM 119.9 22.8
2/5/2019 3:36:55 PM 119.8 22.7
2/5/2019 3:36:56 PM 119.5 22.4
2/5/2019 3:36:57 PM 119.4 22.3
2/5/2019 3:36:58 PM 119.2 22.1
2/5/2019 3:36:59 PM 119.0 21.9
2/5/2019 3:37:00 PM 118.9 21.8
2/5/2019 3:37:01 PM 118.7 21.6
2/5/2019 3:37:02 PM 118.5 21.4
2/5/2019 3:37:03 PM 118.3 21.2
2/5/2019 3:37:04 PM 118.2 21.1
2/5/2019 3:37:05 PM 118.0 20.9
2/5/2019 3:37:06 PM 117.8 20.7
2/5/2019 3:37:07 PM 117.7 20.6
2/5/2019 3:37:08 PM 117.5 20.4
2/5/2019 3:37:09 PM 117.3 20.2
2/5/2019 3:37:10 PM 117.2 20.1
2/5/2019 3:37:11 PM 117.0 19.9
2/5/2019 3:37:12 PM 116.8 19.7
2/5/2019 3:37:13 PM 116.7 19.6
2/5/2019 3:37:14 PM 116.5 19.4
2/5/2019 3:37:15 PM 116.4 19.3
2/5/2019 3:37:16 PM 116.2 19.1
2/5/2019 3:37:17 PM 116.1 19.0
2/5/2019 3:37:18 PM 115.9 18.8
2/5/2019 3:37:19 PM 115.8 18.7
2/5/2019 3:37:20 PM 115.7 18.6
2/5/2019 3:37:21 PM 115.6 18.5
2/5/2019 3:37:22 PM 115.5 18.4
2/5/2019 3:37:23 PM 115.3 18.2
2/5/2019 3:37:24 PM 115.2 18.1
2/5/2019 3:37:25 PM 115.1 18.0
2/5/2019 3:37:26 PM 115.0 17.9
2/5/2019 3:37:27 PM 114.9 17.8
2/5/2019 3:37:28 PM 114.9 17.8
2/5/2019 3:37:29 PM 114.8 17.7
2/5/2019 3:37:30 PM 114.7 17.6
2/5/2019 3:37:31 PM 114.6 17.5
2/5/2019 3:37:32 PM 114.5 17.4
2/5/2019 3:37:33 PM 114.3 17.2
2/5/2019 3:37:34 PM 114.3 17.2
2/5/2019 3:37:35 PM 114.1 17.0
2/5/2019 3:37:36 PM 114.0 16.9
2/5/2019 3:37:37 PM 113.9 16.8
2/5/2019 3:37:38 PM 113.8 16.7
2/5/2019 3:37:39 PM 113.7 16.6
2/5/2019 3:37:40 PM 113.6 16.5
2/5/2019 3:37:41 PM 113.5 16.4
2/5/2019 3:37:42 PM 113.4 16.3
2/5/2019 3:37:43 PM 113.2 16.1
2/5/2019 3:37:44 PM 113.1 16.0
2/5/2019 3:37:45 PM 113.0 15.9
2/5/2019 3:37:46 PM 112.9 15.8
2/5/2019 3:37:47 PM 112.8 15.7
2/5/2019 3:37:48 PM 112.6 15.5
2/5/2019 3:37:49 PM 112.5 15.4
2/5/2019 3:37:50 PM 112.4 15.3
2/5/2019 3:37:51 PM 112.3 15.2
2/5/2019 3:37:52 PM 112.2 15.1
Page 207 of 452 August 2019
APPENDIX E42: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
2/5/2019 3:37:53 PM 112.1 15.0
2/5/2019 3:37:54 PM 112.0 14.9
2/5/2019 3:37:55 PM 111.9 14.8
2/5/2019 3:37:56 PM 111.8 14.7
2/5/2019 3:37:57 PM 111.6 14.5
2/5/2019 3:37:58 PM 111.6 14.5
2/5/2019 3:37:59 PM 111.5 14.4
2/5/2019 3:38:00 PM 111.4 14.3
2/5/2019 3:38:01 PM 111.3 14.2
2/5/2019 3:38:02 PM 111.2 14.1
2/5/2019 3:38:03 PM 111.1 14.0
2/5/2019 3:38:04 PM 111.0 13.9
2/5/2019 3:38:05 PM 110.9 13.8
2/5/2019 3:38:06 PM 110.8 13.7
2/5/2019 3:38:07 PM 110.7 13.6
2/5/2019 3:38:08 PM 110.6 13.5
2/5/2019 3:38:09 PM 110.6 13.5
2/5/2019 3:38:10 PM 110.5 13.4
2/5/2019 3:38:11 PM 110.4 13.3
2/5/2019 3:38:12 PM 110.3 13.2
2/5/2019 3:38:13 PM 110.2 13.1
2/5/2019 3:38:14 PM 110.1 13.0
2/5/2019 3:38:15 PM 110.1 13.0
2/5/2019 3:38:16 PM 110.0 12.9
2/5/2019 3:38:17 PM 109.9 12.8
2/5/2019 3:38:18 PM 109.8 12.7
2/5/2019 3:38:19 PM 109.7 12.6
2/5/2019 3:38:20 PM 109.6 12.5
2/5/2019 3:38:21 PM 109.5 12.4
2/5/2019 3:38:22 PM 109.5 12.4
2/5/2019 3:38:23 PM 109.4 12.3
2/5/2019 3:38:24 PM 109.3 12.2
2/5/2019 3:38:25 PM 109.2 12.1
2/5/2019 3:38:26 PM 109.1 12.0
2/5/2019 3:38:27 PM 109.0 11.9
2/5/2019 3:38:28 PM 108.9 11.8
2/5/2019 3:38:29 PM 108.8 11.7
2/5/2019 3:38:30 PM 108.8 11.7
2/5/2019 3:38:31 PM 108.7 11.6
2/5/2019 3:38:32 PM 108.6 11.5
2/5/2019 3:38:33 PM 108.5 11.4
2/5/2019 3:38:34 PM 108.4 11.3
2/5/2019 3:38:35 PM 108.4 11.3
2/5/2019 3:38:36 PM 108.3 11.2
2/5/2019 3:38:37 PM 108.2 11.1
2/5/2019 3:38:38 PM 108.1 11.0
2/5/2019 3:38:39 PM 108.1 11.0
2/5/2019 3:38:40 PM 108.0 10.9
2/5/2019 3:38:41 PM 107.9 10.8
2/5/2019 3:38:42 PM 107.8 10.7
2/5/2019 3:38:43 PM 107.8 10.7
2/5/2019 3:38:44 PM 107.7 10.6
2/5/2019 3:38:45 PM 107.6 10.5
2/5/2019 3:38:46 PM 107.5 10.4
2/5/2019 3:38:47 PM 107.5 10.4
2/5/2019 3:38:48 PM 107.4 10.3
2/5/2019 3:38:49 PM 107.3 10.2
2/5/2019 3:38:50 PM 107.3 10.2
2/5/2019 3:38:51 PM 107.2 10.1
2/5/2019 3:38:52 PM 107.1 10.0
2/5/2019 3:38:53 PM 107.0 9.9
2/5/2019 3:38:54 PM 107.0 9.9
2/5/2019 3:38:55 PM 106.9 9.8
2/5/2019 3:38:56 PM 106.8 9.7
2/5/2019 3:38:57 PM 106.8 9.7
2/5/2019 3:38:58 PM 106.7 9.6
2/5/2019 3:38:59 PM 106.6 9.5
2/5/2019 3:39:00 PM 106.5 9.4
2/5/2019 3:39:01 PM 106.5 9.4
2/5/2019 3:39:02 PM 106.4 9.3
2/5/2019 3:39:03 PM 106.3 9.2
2/5/2019 3:39:04 PM 106.2 9.1
2/5/2019 3:39:05 PM 106.1 9.0
2/5/2019 3:39:06 PM 106.1 9.0
2/5/2019 3:39:07 PM 106.0 8.9
2/5/2019 3:39:08 PM 105.9 8.8
2/5/2019 3:39:09 PM 105.8 8.7
2/5/2019 3:39:10 PM 105.8 8.7
2/5/2019 3:39:11 PM 105.7 8.6
Page 208 of 452 August 2019
APPENDIX E42: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
2/5/2019 3:39:12 PM 105.6 8.5
2/5/2019 3:39:13 PM 105.5 8.4
2/5/2019 3:39:14 PM 105.5 8.4
2/5/2019 3:39:15 PM 105.4 8.3
2/5/2019 3:39:16 PM 105.3 8.2
2/5/2019 3:39:17 PM 105.2 8.1
2/5/2019 3:39:18 PM 105.2 8.1
2/5/2019 3:39:19 PM 105.1 8.0
2/5/2019 3:39:20 PM 105.0 7.9
2/5/2019 3:39:21 PM 105.0 7.9
2/5/2019 3:39:22 PM 104.9 7.8
2/5/2019 3:39:23 PM 104.8 7.7
2/5/2019 3:39:24 PM 104.7 7.6
2/5/2019 3:39:25 PM 104.7 7.6
2/6/2019 1:00:52 PM 85.9 56.5
2/6/2019 1:00:53 PM 85.8 56.5
2/6/2019 1:00:54 PM 85.6 56.5
2/6/2019 1:00:55 PM 85.5 56.5
2/6/2019 1:00:56 PM 85.4 56.5
2/6/2019 1:00:57 PM 85.2 56.5
2/6/2019 1:00:58 PM 85.1 56.5
2/6/2019 1:00:59 PM 84.9 56.5
2/6/2019 1:01:00 PM 84.8 56.5
2/6/2019 1:01:01 PM 84.6 56.5
2/6/2019 1:01:02 PM 84.5 56.5
2/6/2019 1:01:03 PM 84.4 56.5
2/6/2019 1:01:04 PM 84.3 56.5
2/6/2019 1:01:05 PM 84.2 56.5
2/6/2019 1:01:06 PM 84.1 56.5
2/6/2019 1:01:07 PM 84.0 56.5
2/6/2019 1:01:08 PM 83.9 56.5
2/6/2019 1:01:09 PM 83.8 56.5
2/6/2019 1:01:10 PM 83.7 56.5
2/6/2019 1:01:11 PM 83.6 56.5
2/6/2019 1:01:12 PM 83.5 56.5
2/6/2019 1:01:13 PM 83.4 56.5
2/6/2019 1:01:14 PM 83.3 56.5
2/6/2019 1:01:14 PM 83.2 56.5
2/6/2019 1:01:15 PM 83.1 56.5
2/6/2019 1:01:16 PM 83.0 56.5
2/6/2019 1:01:17 PM 82.9 56.5
2/6/2019 1:01:18 PM 82.7 56.5
2/6/2019 1:01:19 PM 82.6 56.5
2/6/2019 1:01:20 PM 82.5 56.5
2/6/2019 1:01:21 PM 82.4 56.5
2/6/2019 1:01:22 PM 82.3 56.5
2/6/2019 1:01:23 PM 82.2 56.5
2/6/2019 1:01:24 PM 82.1 56.5
2/6/2019 1:01:25 PM 82.0 56.5
2/6/2019 1:01:26 PM 81.9 56.5
2/6/2019 1:01:27 PM 81.8 56.5
2/6/2019 1:01:28 PM 81.7 56.5
2/6/2019 1:01:29 PM 81.6 56.5
2/6/2019 1:01:30 PM 81.5 56.5
2/6/2019 1:01:31 PM 81.4 56.5
2/6/2019 1:01:32 PM 81.4 56.5
2/6/2019 1:01:33 PM 81.3 56.5
2/6/2019 1:01:34 PM 81.2 56.5
2/6/2019 1:01:35 PM 81.1 56.5
2/6/2019 1:01:36 PM 81.0 56.5
2/6/2019 1:01:37 PM 81.0 56.5
2/6/2019 1:01:38 PM 80.9 56.5
2/6/2019 1:01:39 PM 80.8 56.5
2/6/2019 1:01:40 PM 80.7 56.5
2/6/2019 1:01:41 PM 80.6 56.5
2/6/2019 1:01:42 PM 80.5 56.5
2/6/2019 1:01:43 PM 80.4 56.5
2/6/2019 1:01:44 PM 80.3 56.5
2/6/2019 1:01:45 PM 80.2 56.5
2/6/2019 1:01:46 PM 80.1 56.5
2/6/2019 1:01:47 PM 80.0 56.5
2/6/2019 1:01:48 PM 79.9 56.5
2/6/2019 1:01:49 PM 79.8 56.5
2/6/2019 1:01:50 PM 79.8 56.5
2/6/2019 1:01:51 PM 79.7 56.5
2/6/2019 1:01:52 PM 79.6 56.5
2/6/2019 1:01:53 PM 79.6 56.5
2/6/2019 1:01:54 PM 79.5 56.5
2/6/2019 1:01:55 PM 79.4 56.5
Page 209 of 452 August 2019
APPENDIX E42: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
2/6/2019 1:01:56 PM 79.4 56.5
2/6/2019 1:01:57 PM 79.4 56.5
2/6/2019 1:01:58 PM 79.3 56.5
2/6/2019 1:01:59 PM 79.3 56.5
2/6/2019 1:02:00 PM 79.3 56.5
2/6/2019 1:02:01 PM 79.2 56.5
2/6/2019 1:02:02 PM 79.2 56.5
2/6/2019 1:02:03 PM 79.2 56.5
2/6/2019 1:02:04 PM 79.1 56.5
2/6/2019 1:02:05 PM 79.1 56.5
2/6/2019 1:02:06 PM 79.1 56.5
2/6/2019 1:02:07 PM 79.0 56.5
2/6/2019 1:02:08 PM 78.9 56.5
2/6/2019 1:02:09 PM 78.9 56.5
2/6/2019 1:02:10 PM 78.8 56.5
2/6/2019 1:02:11 PM 78.7 56.5
2/6/2019 1:02:12 PM 78.6 56.5
2/6/2019 1:02:13 PM 78.5 56.5
2/6/2019 1:02:14 PM 78.5 56.5
2/6/2019 1:02:15 PM 78.4 56.5
2/6/2019 1:02:16 PM 78.3 56.5
2/6/2019 1:02:17 PM 78.2 56.5
2/6/2019 1:02:18 PM 78.1 56.5
2/6/2019 1:02:19 PM 78.0 56.5
2/6/2019 1:02:20 PM 78.0 56.5
2/6/2019 1:02:21 PM 77.9 56.5
2/6/2019 1:02:22 PM 77.8 56.5
2/6/2019 1:02:23 PM 77.7 56.5
2/6/2019 1:02:24 PM 77.6 56.5
2/6/2019 1:02:25 PM 77.5 56.5
2/6/2019 1:02:26 PM 77.4 56.5
2/6/2019 1:02:27 PM 77.3 56.5
2/6/2019 1:02:28 PM 77.2 56.5
2/6/2019 1:02:29 PM 77.1 56.5
2/6/2019 1:02:30 PM 77.1 56.5
2/6/2019 1:02:31 PM 77.0 56.5
2/6/2019 1:02:32 PM 76.9 56.5
2/6/2019 1:02:33 PM 76.9 56.5
2/6/2019 1:02:34 PM 76.8 56.5
2/6/2019 1:02:35 PM 76.8 56.5
2/6/2019 1:02:36 PM 76.7 56.5
2/6/2019 1:02:37 PM 76.7 56.5
2/6/2019 1:02:38 PM 76.7 56.5
2/6/2019 1:02:39 PM 76.6 56.5
2/6/2019 1:02:40 PM 76.6 56.5
2/6/2019 1:02:41 PM 76.5 56.5
2/6/2019 1:02:42 PM 76.5 56.5
2/6/2019 1:02:43 PM 76.4 56.5
2/6/2019 1:02:44 PM 76.4 56.5
2/6/2019 1:02:45 PM 76.3 56.5
2/6/2019 1:02:46 PM 76.3 56.5
2/6/2019 1:02:47 PM 76.2 56.5
2/6/2019 1:02:48 PM 76.1 56.5
2/6/2019 1:02:49 PM 76.1 56.5
2/6/2019 1:02:50 PM 76.0 56.5
2/6/2019 1:02:51 PM 75.9 56.5
2/6/2019 1:02:52 PM 75.9 56.5
2/6/2019 1:02:53 PM 75.8 56.5
2/6/2019 1:02:54 PM 75.7 56.5
2/6/2019 1:02:55 PM 75.7 56.5
2/6/2019 1:02:56 PM 75.6 56.5
2/6/2019 1:02:57 PM 75.6 56.5
2/6/2019 1:02:58 PM 75.5 56.5
2/6/2019 1:02:59 PM 75.5 56.5
2/6/2019 1:03:00 PM 75.5 56.5
2/6/2019 1:03:01 PM 75.4 56.5
2/6/2019 1:03:02 PM 75.4 56.5
2/6/2019 1:03:03 PM 75.4 56.5
2/6/2019 1:03:04 PM 75.3 56.5
2/6/2019 1:03:05 PM 75.3 56.5
2/6/2019 1:03:06 PM 75.2 56.5
2/6/2019 1:03:07 PM 75.1 56.5
2/6/2019 1:03:08 PM 75.1 56.5
2/6/2019 1:03:09 PM 75.0 56.5
2/6/2019 1:03:10 PM 75.0 56.5
2/6/2019 1:03:11 PM 74.9 56.5
2/6/2019 1:03:12 PM 74.8 56.5
2/6/2019 1:03:13 PM 74.8 56.5
2/6/2019 1:03:14 PM 74.7 56.5
Page 210 of 452 August 2019
APPENDIX E42: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
2/6/2019 1:03:15 PM 74.6 56.5
2/6/2019 1:03:16 PM 74.5 56.5
2/6/2019 1:03:17 PM 74.5 56.5
2/6/2019 1:03:18 PM 74.4 56.5
2/6/2019 1:03:19 PM 74.4 56.5
2/6/2019 1:03:20 PM 74.3 56.5
2/6/2019 1:03:21 PM 74.3 56.5
2/6/2019 1:03:22 PM 74.2 56.5
2/6/2019 1:03:23 PM 74.2 56.5
2/6/2019 1:03:24 PM 74.1 56.5
2/6/2019 1:03:25 PM 74.1 56.5
2/6/2019 1:03:26 PM 74.0 56.5
2/6/2019 1:03:27 PM 74.0 56.5
2/6/2019 1:03:28 PM 74.0 56.5
2/6/2019 1:03:29 PM 73.9 56.5
2/6/2019 1:03:30 PM 73.9 56.5
2/6/2019 1:03:31 PM 73.9 56.5
2/6/2019 1:03:32 PM 73.8 56.5
2/6/2019 1:03:33 PM 73.8 56.5
2/6/2019 1:03:34 PM 73.7 56.5
2/6/2019 1:03:35 PM 73.7 56.5
2/6/2019 1:03:36 PM 73.7 56.5
2/6/2019 1:03:37 PM 73.6 56.5
2/6/2019 1:03:38 PM 73.6 56.5
2/6/2019 1:03:39 PM 73.5 56.5
2/6/2019 1:03:40 PM 73.5 56.5
2/6/2019 1:03:41 PM 73.4 56.5
2/6/2019 1:03:42 PM 73.4 56.5
2/6/2019 1:03:43 PM 73.4 56.5
2/6/2019 1:03:44 PM 73.3 56.5
2/6/2019 1:03:45 PM 73.3 56.5
2/6/2019 1:03:46 PM 73.2 56.5
2/6/2019 1:03:47 PM 73.2 56.5
2/6/2019 1:03:48 PM 73.2 56.5
2/6/2019 1:03:49 PM 73.1 56.5
2/6/2019 1:03:50 PM 73.1 56.5
2/6/2019 1:03:51 PM 73.0 56.5
2/6/2019 1:03:52 PM 73.0 56.5
2/6/2019 1:03:53 PM 72.9 56.5
2/6/2019 1:03:54 PM 72.8 56.5
2/6/2019 1:03:55 PM 72.7 56.5
2/6/2019 1:03:56 PM 72.7 56.5
2/6/2019 1:03:57 PM 72.6 56.5
2/6/2019 1:03:58 PM 72.5 56.5
2/6/2019 1:03:59 PM 72.5 56.5
2/6/2019 1:04:00 PM 72.4 56.5
2/6/2019 1:04:01 PM 72.3 56.5
2/6/2019 1:04:02 PM 72.3 56.5
2/6/2019 1:04:03 PM 72.2 56.5
2/6/2019 1:04:04 PM 72.2 56.5
2/6/2019 1:04:05 PM 72.1 56.5
2/6/2019 1:04:06 PM 72.1 56.5
2/6/2019 1:04:07 PM 72.1 56.5
2/6/2019 1:04:08 PM 72.1 56.5
2/6/2019 1:04:09 PM 72.0 56.5
2/6/2019 1:04:10 PM 72.0 56.5
2/6/2019 1:04:11 PM 72.0 56.5
2/6/2019 1:04:12 PM 72.0 56.5
2/6/2019 1:04:13 PM 71.9 56.5
2/6/2019 1:04:14 PM 71.9 56.5
2/6/2019 1:04:15 PM 71.8 56.5
2/6/2019 1:04:16 PM 71.8 56.5
2/6/2019 1:04:17 PM 71.8 56.5
2/6/2019 1:04:18 PM 71.7 56.5
2/6/2019 1:04:19 PM 71.7 56.5
2/6/2019 1:04:20 PM 71.6 56.5
2/6/2019 1:04:21 PM 71.5 56.5
2/6/2019 1:04:22 PM 71.5 56.5
2/6/2019 1:04:23 PM 71.5 56.5
2/6/2019 1:04:24 PM 71.4 56.5
2/6/2019 1:04:25 PM 71.4 56.5
2/6/2019 1:04:26 PM 71.4 56.5
2/6/2019 1:04:27 PM 71.4 56.5
2/6/2019 1:04:28 PM 71.3 56.5
2/6/2019 1:04:29 PM 71.3 56.5
2/6/2019 1:04:30 PM 71.3 56.5
2/6/2019 1:04:31 PM 71.2 56.5
2/6/2019 1:04:32 PM 71.2 56.5
2/6/2019 1:04:33 PM 71.2 56.5
Page 211 of 452 August 2019
APPENDIX E42: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
2/6/2019 1:04:34 PM 71.1 56.5
2/6/2019 1:04:35 PM 71.1 56.5
2/6/2019 1:04:36 PM 71.0 56.5
2/6/2019 1:04:37 PM 71.0 56.5
2/6/2019 1:04:38 PM 70.9 56.5
2/6/2019 1:04:39 PM 70.9 56.5
2/6/2019 1:04:40 PM 70.8 56.5
2/6/2019 1:04:41 PM 70.8 56.5
2/6/2019 1:04:42 PM 70.7 56.5
2/6/2019 1:04:43 PM 70.7 56.5
2/6/2019 1:04:44 PM 70.6 56.5
2/6/2019 1:04:45 PM 70.6 56.5
2/6/2019 1:04:46 PM 70.5 56.5
2/6/2019 1:04:47 PM 70.5 56.5
2/6/2019 1:04:48 PM 70.4 56.5
2/6/2019 1:04:49 PM 70.4 56.5
2/6/2019 1:04:50 PM 70.3 56.5
2/6/2019 1:04:51 PM 70.3 56.5
2/6/2019 1:04:52 PM 70.2 56.5
2/6/2019 1:04:53 PM 70.2 56.5
2/6/2019 1:04:54 PM 70.2 56.5
2/6/2019 1:04:55 PM 70.2 56.5
2/6/2019 1:04:56 PM 70.2 56.5
2/6/2019 1:04:57 PM 70.1 56.5
2/6/2019 1:04:58 PM 70.1 56.5
2/6/2019 1:04:59 PM 70.1 56.5
2/6/2019 1:05:00 PM 70.1 56.5
2/6/2019 1:05:01 PM 70.1 56.5
2/6/2019 1:05:02 PM 70.1 56.5
2/6/2019 1:05:03 PM 70.1 56.5
2/6/2019 1:05:04 PM 70.1 56.5
2/6/2019 1:05:05 PM 70.0 56.5
2/6/2019 1:05:06 PM 70.0 56.5
2/6/2019 1:05:07 PM 70.0 56.5
2/6/2019 1:05:08 PM 70.0 56.5
2/6/2019 1:05:09 PM 69.9 56.5
2/6/2019 1:05:10 PM 69.9 56.5
2/6/2019 1:05:11 PM 69.9 56.5
2/6/2019 1:05:12 PM 69.9 56.5
2/6/2019 1:05:13 PM 69.9 56.5
2/6/2019 1:05:14 PM 69.8 56.5
2/6/2019 1:05:15 PM 69.8 56.5
2/6/2019 1:05:16 PM 69.7 56.5
2/6/2019 1:05:17 PM 69.7 56.5
2/6/2019 1:05:18 PM 69.6 56.5
2/6/2019 1:05:19 PM 69.6 56.5
2/6/2019 1:05:20 PM 69.6 56.5
2/6/2019 1:05:21 PM 69.5 56.5
2/6/2019 1:05:22 PM 69.5 56.5
2/6/2019 1:05:23 PM 69.4 56.5
2/6/2019 1:05:24 PM 69.4 56.5
2/6/2019 1:05:25 PM 69.3 56.5
2/6/2019 1:05:26 PM 69.3 56.5
2/6/2019 1:05:27 PM 69.3 56.5
2/6/2019 1:05:28 PM 69.2 56.5
2/6/2019 1:05:29 PM 69.2 56.5
2/6/2019 1:05:30 PM 69.2 56.5
2/6/2019 1:05:31 PM 69.1 56.5
2/6/2019 1:05:32 PM 69.1 56.5
2/6/2019 1:05:33 PM 69.1 56.5
2/6/2019 1:05:34 PM 69.0 56.5
2/6/2019 1:05:35 PM 69.0 56.5
2/6/2019 1:05:36 PM 69.0 56.5
2/6/2019 1:05:37 PM 68.9 56.5
2/6/2019 1:05:38 PM 68.9 56.5
2/6/2019 1:05:39 PM 68.9 56.5
2/6/2019 1:05:40 PM 68.9 56.5
2/6/2019 1:05:41 PM 68.8 56.5
2/6/2019 1:05:42 PM 68.8 56.5
2/6/2019 1:05:43 PM 68.8 56.5
2/6/2019 1:05:44 PM 68.7 56.5
2/6/2019 1:05:45 PM 68.7 56.5
2/6/2019 1:05:46 PM 68.7 56.5
2/6/2019 1:05:47 PM 68.6 56.5
2/6/2019 1:05:48 PM 68.6 56.5
2/6/2019 1:05:49 PM 68.6 56.5
2/6/2019 1:05:50 PM 68.6 56.5
2/6/2019 1:05:51 PM 68.5 56.5
2/6/2019 1:05:52 PM 68.5 56.5
Page 212 of 452 August 2019
APPENDIX E42: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
2/6/2019 1:05:53 PM 68.5 56.5
2/6/2019 1:05:54 PM 68.5 56.5
2/6/2019 1:05:55 PM 68.5 56.5
2/6/2019 1:05:56 PM 68.4 56.5
2/6/2019 1:05:57 PM 68.4 56.5
2/6/2019 1:05:58 PM 68.4 56.5
2/6/2019 1:05:59 PM 68.4 56.5
2/6/2019 1:06:00 PM 68.3 56.5
2/6/2019 1:06:01 PM 68.3 56.5
2/6/2019 1:06:02 PM 68.3 56.5
2/6/2019 1:06:03 PM 68.3 56.5
2/6/2019 1:06:04 PM 68.2 56.5
2/6/2019 1:06:05 PM 68.2 56.5
2/6/2019 1:06:06 PM 68.2 56.5
2/6/2019 1:06:07 PM 68.1 56.5
2/6/2019 1:06:08 PM 68.1 56.5
2/6/2019 1:06:09 PM 68.1 56.5
2/6/2019 1:06:10 PM 68.1 56.5
2/6/2019 1:06:11 PM 68.1 56.5
2/6/2019 1:06:12 PM 68.0 56.5
2/6/2019 1:06:13 PM 68.0 56.5
2/6/2019 1:06:14 PM 68.0 56.5
2/6/2019 1:06:15 PM 68.0 56.5
2/6/2019 1:06:16 PM 68.0 56.5
2/6/2019 1:06:17 PM 68.0 56.5
2/6/2019 1:06:18 PM 68.0 56.5
2/6/2019 1:06:19 PM 68.0 56.5
2/6/2019 1:06:20 PM 67.9 56.5
2/6/2019 1:06:21 PM 67.9 56.5
2/6/2019 1:06:22 PM 67.9 56.5
2/6/2019 1:06:23 PM 67.8 56.5
2/6/2019 1:06:24 PM 67.8 56.5
2/6/2019 1:06:25 PM 67.8 56.5
2/6/2019 1:06:26 PM 67.7 56.5
2/6/2019 1:06:27 PM 67.7 56.5
2/6/2019 1:06:28 PM 67.7 56.5
2/6/2019 1:06:29 PM 67.6 56.5
2/6/2019 1:06:30 PM 67.6 56.5
2/6/2019 1:06:31 PM 67.6 56.5
2/6/2019 1:06:32 PM 67.6 56.5
2/6/2019 1:06:33 PM 67.5 56.5
2/6/2019 1:06:34 PM 67.5 56.5
2/6/2019 1:06:35 PM 67.5 56.5
2/6/2019 1:06:36 PM 67.4 56.5
2/6/2019 1:06:37 PM 67.4 56.5
2/6/2019 1:06:38 PM 67.4 56.5
2/6/2019 1:06:39 PM 67.4 56.5
2/6/2019 1:06:40 PM 67.3 56.5
2/6/2019 1:06:41 PM 67.3 56.5
2/6/2019 1:06:42 PM 67.3 56.5
2/6/2019 1:06:43 PM 67.3 56.5
2/6/2019 1:06:44 PM 67.3 56.5
2/6/2019 1:06:45 PM 67.2 56.5
2/6/2019 1:06:46 PM 67.2 56.5
2/6/2019 1:06:47 PM 67.2 56.5
2/6/2019 1:06:48 PM 67.2 56.5
2/6/2019 1:06:49 PM 67.2 56.5
2/6/2019 1:06:50 PM 67.2 56.5
2/6/2019 1:06:51 PM 67.2 56.5
2/6/2019 1:06:52 PM 67.1 56.5
2/6/2019 1:06:53 PM 67.1 56.5
2/6/2019 1:06:54 PM 67.1 56.5
2/6/2019 1:06:55 PM 67.1 56.5
2/6/2019 1:06:56 PM 67.1 56.5
2/6/2019 1:06:57 PM 67.1 56.5
2/6/2019 1:06:58 PM 67.1 56.5
2/6/2019 1:06:59 PM 67.1 56.5
2/6/2019 1:07:00 PM 67.0 56.5
2/6/2019 1:07:01 PM 67.0 56.5
2/6/2019 1:07:02 PM 67.0 56.5
2/6/2019 1:07:03 PM 67.0 56.5
2/6/2019 1:07:04 PM 67.0 56.5
2/6/2019 1:07:05 PM 66.9 56.5
2/6/2019 1:07:06 PM 66.9 56.5
2/6/2019 1:07:07 PM 66.9 56.5
2/6/2019 1:07:08 PM 66.9 56.5
2/6/2019 1:07:09 PM 66.9 56.5
2/6/2019 1:07:10 PM 66.9 56.5
2/6/2019 1:07:11 PM 66.8 56.5
Page 213 of 452 August 2019
APPENDIX E42: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
2/6/2019 1:07:12 PM 66.8 56.5
2/6/2019 1:07:13 PM 66.8 56.5
2/6/2019 1:07:14 PM 66.8 56.5
2/6/2019 1:07:15 PM 66.7 56.5
2/6/2019 1:07:16 PM 66.7 56.5
2/6/2019 1:07:17 PM 66.7 56.5
2/6/2019 1:07:18 PM 66.7 56.5
2/6/2019 1:07:19 PM 66.6 56.5
2/6/2019 1:07:20 PM 66.6 56.5
2/6/2019 1:07:21 PM 66.6 56.5
2/6/2019 1:07:22 PM 66.6 56.5
2/6/2019 1:07:23 PM 66.5 56.5
2/6/2019 1:07:24 PM 66.5 56.5
2/6/2019 1:07:25 PM 66.5 56.5
2/6/2019 1:07:26 PM 66.5 56.5
2/6/2019 1:07:27 PM 66.4 56.5
2/6/2019 1:07:28 PM 66.4 56.5
2/6/2019 1:07:29 PM 66.4 56.5
2/6/2019 1:07:30 PM 66.4 56.5
2/6/2019 1:07:31 PM 66.3 56.5
2/6/2019 1:07:32 PM 66.3 56.5
2/6/2019 1:07:33 PM 66.3 56.5
2/6/2019 1:07:34 PM 66.3 56.5
2/6/2019 1:07:35 PM 66.2 56.5
2/6/2019 1:07:36 PM 66.2 56.5
2/6/2019 1:07:37 PM 66.2 56.5
2/6/2019 1:07:38 PM 66.2 56.5
2/6/2019 1:07:39 PM 66.1 56.5
2/6/2019 1:07:40 PM 66.1 56.5
2/6/2019 1:07:41 PM 66.1 56.5
2/6/2019 1:07:42 PM 66.1 56.5
2/6/2019 1:07:43 PM 66.1 56.5
2/6/2019 1:07:44 PM 66.1 56.5
2/6/2019 1:07:45 PM 66.0 56.5
2/6/2019 1:07:46 PM 66.0 56.5
2/6/2019 1:07:47 PM 66.0 56.5
2/6/2019 1:07:48 PM 66.0 56.5
2/6/2019 1:07:49 PM 66.0 56.5
2/6/2019 1:07:50 PM 66.0 56.5
2/6/2019 1:07:51 PM 66.0 56.5
2/6/2019 1:07:52 PM 65.9 56.5
2/6/2019 1:07:53 PM 65.9 56.5
2/6/2019 1:07:54 PM 65.9 56.5
2/6/2019 1:07:55 PM 65.9 56.5
2/6/2019 1:07:56 PM 65.9 56.5
2/6/2019 1:07:57 PM 65.9 56.5
2/6/2019 1:07:58 PM 65.9 56.5
2/6/2019 1:07:59 PM 65.9 56.5
2/6/2019 1:08:00 PM 65.9 56.5
2/6/2019 1:08:01 PM 65.8 56.5
2/6/2019 1:08:02 PM 65.8 56.5
2/6/2019 1:08:03 PM 65.8 56.5
2/6/2019 1:08:04 PM 65.8 56.5
2/6/2019 1:08:05 PM 65.8 56.5
2/6/2019 1:08:06 PM 65.8 56.5
2/6/2019 1:08:07 PM 65.7 56.5
2/6/2019 1:08:08 PM 65.7 56.5
2/6/2019 1:08:09 PM 65.7 56.5
2/6/2019 1:08:10 PM 65.7 56.5
2/6/2019 1:08:11 PM 65.7 56.5
2/6/2019 1:08:12 PM 65.7 56.5
2/6/2019 1:08:13 PM 65.6 56.5
2/6/2019 1:08:14 PM 65.6 56.5
2/6/2019 1:08:15 PM 65.6 56.5
2/6/2019 1:08:16 PM 65.6 56.5
2/6/2019 1:08:17 PM 65.6 56.5
2/6/2019 1:08:18 PM 65.6 56.5
2/6/2019 1:08:19 PM 65.5 56.5
2/6/2019 1:08:20 PM 65.5 56.5
2/6/2019 1:08:21 PM 65.5 56.5
2/6/2019 1:08:22 PM 65.5 56.5
2/6/2019 1:08:23 PM 65.5 56.5
2/6/2019 1:08:24 PM 65.5 56.5
2/6/2019 1:08:25 PM 65.5 56.5
2/6/2019 1:08:26 PM 65.4 56.5
2/6/2019 1:08:27 PM 65.4 56.5
2/6/2019 1:08:28 PM 65.4 56.5
2/6/2019 1:08:29 PM 65.4 56.5
2/6/2019 1:08:30 PM 65.4 56.5
Page 214 of 452 August 2019
APPENDIX E42: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
2/6/2019 1:08:31 PM 65.4 56.5
2/6/2019 1:08:32 PM 65.4 56.5
2/6/2019 1:08:33 PM 65.3 56.5
2/6/2019 1:08:34 PM 65.3 56.5
2/6/2019 1:08:35 PM 65.3 56.5
2/6/2019 1:08:36 PM 65.3 56.5
2/6/2019 1:08:37 PM 65.3 56.5
2/6/2019 1:08:38 PM 65.2 56.5
2/6/2019 1:08:39 PM 65.2 56.5
2/6/2019 1:08:40 PM 65.2 56.5
2/6/2019 1:08:41 PM 65.2 56.5
2/6/2019 1:08:42 PM 65.2 56.5
2/6/2019 1:08:43 PM 65.2 56.5
2/6/2019 1:08:44 PM 65.1 56.5
2/6/2019 1:08:45 PM 65.1 56.5
2/6/2019 1:08:46 PM 65.1 56.5
2/6/2019 1:08:47 PM 65.1 56.5
2/6/2019 1:08:48 PM 65.1 56.5
2/6/2019 1:08:49 PM 65.1 56.5
2/6/2019 1:08:50 PM 65.1 56.5
2/6/2019 1:08:51 PM 65.0 56.5
2/6/2019 1:08:52 PM 65.0 56.5
2/6/2019 1:08:53 PM 65.0 56.5
2/6/2019 1:08:54 PM 65.0 56.5
2/6/2019 1:08:55 PM 65.0 56.5
2/6/2019 1:08:56 PM 65.0 56.5
2/6/2019 1:08:57 PM 64.9 56.5
2/6/2019 1:08:58 PM 64.9 56.5
2/6/2019 1:08:59 PM 64.9 56.5
2/6/2019 1:09:00 PM 64.9 56.5
2/6/2019 1:09:01 PM 64.9 56.5
2/6/2019 1:09:02 PM 64.8 56.5
2/6/2019 1:09:03 PM 64.8 56.5
2/6/2019 1:09:04 PM 64.8 56.5
2/6/2019 1:09:05 PM 64.8 56.5
2/6/2019 1:09:06 PM 64.8 56.5
2/6/2019 1:09:07 PM 64.7 56.5
2/6/2019 1:09:08 PM 64.7 56.5
2/6/2019 1:09:09 PM 64.7 56.5
2/6/2019 1:09:10 PM 64.7 56.5
2/6/2019 1:09:11 PM 64.7 56.5
2/6/2019 1:09:12 PM 64.6 56.5
2/6/2019 1:09:13 PM 64.6 56.5
2/6/2019 1:09:14 PM 64.6 56.5
2/6/2019 1:09:15 PM 64.6 56.5
2/6/2019 1:09:16 PM 64.5 56.5
2/6/2019 1:09:17 PM 64.5 56.5
2/6/2019 1:09:18 PM 64.5 56.5
2/6/2019 1:09:19 PM 64.5 56.5
2/6/2019 1:09:20 PM 64.5 56.5
2/6/2019 1:09:21 PM 64.4 56.5
2/6/2019 1:09:22 PM 64.4 56.5
2/6/2019 1:09:23 PM 64.4 56.5
2/6/2019 1:09:24 PM 64.4 56.5
2/6/2019 1:09:25 PM 64.4 56.5
2/6/2019 1:09:26 PM 64.4 56.5
2/6/2019 1:09:27 PM 64.4 56.5
2/6/2019 1:09:28 PM 64.3 56.5
2/6/2019 1:09:29 PM 64.3 56.5
2/6/2019 1:09:30 PM 64.3 56.5
2/6/2019 1:09:31 PM 64.3 56.5
2/6/2019 1:09:32 PM 64.3 56.5
2/6/2019 1:09:33 PM 64.3 56.5
2/6/2019 1:09:34 PM 64.3 56.5
2/6/2019 1:09:35 PM 64.3 56.5
2/6/2019 1:09:36 PM 64.2 56.5
2/6/2019 1:09:37 PM 64.2 56.5
2/6/2019 1:09:38 PM 64.2 56.5
2/6/2019 1:09:39 PM 64.2 56.5
2/6/2019 1:09:40 PM 64.2 56.5
2/6/2019 1:09:41 PM 64.2 56.5
2/6/2019 1:09:42 PM 64.1 56.5
2/6/2019 1:09:43 PM 64.1 56.5
2/6/2019 1:09:44 PM 64.1 56.5
2/6/2019 1:09:45 PM 64.1 56.5
2/6/2019 1:09:46 PM 64.1 56.5
2/6/2019 1:09:47 PM 64.1 56.5
2/6/2019 1:09:48 PM 64.0 56.5
2/6/2019 1:09:49 PM 64.0 56.5
Page 215 of 452 August 2019
APPENDIX E42: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
2/6/2019 1:09:50 PM 64.0 56.5
2/6/2019 1:09:51 PM 64.0 56.5
2/6/2019 1:09:52 PM 64.0 56.5
2/6/2019 1:09:53 PM 64.0 56.5
2/6/2019 1:09:54 PM 64.0 56.5
2/6/2019 1:09:55 PM 63.9 56.5
2/6/2019 1:09:56 PM 63.9 56.5
2/6/2019 1:09:57 PM 63.9 56.5
2/6/2019 1:09:58 PM 63.9 56.5
2/6/2019 1:09:59 PM 63.9 56.5
2/6/2019 1:10:00 PM 63.9 56.5
2/6/2019 1:10:01 PM 63.9 56.5
2/6/2019 1:10:02 PM 63.8 56.5
2/6/2019 1:10:03 PM 63.8 56.5
2/6/2019 1:10:04 PM 63.8 56.5
2/6/2019 1:10:05 PM 63.8 56.5
2/6/2019 1:10:06 PM 63.8 56.5
2/6/2019 1:10:07 PM 63.8 56.5
2/6/2019 1:10:08 PM 63.8 56.5
2/6/2019 1:10:09 PM 63.8 56.5
2/6/2019 1:10:10 PM 63.8 56.5
2/6/2019 1:10:11 PM 63.7 56.5
2/6/2019 1:10:12 PM 63.7 56.5
2/6/2019 1:10:13 PM 63.7 56.5
2/6/2019 1:10:14 PM 63.7 56.5
2/6/2019 1:10:15 PM 63.7 56.5
2/6/2019 1:10:16 PM 63.7 56.5
2/6/2019 1:10:17 PM 63.7 56.5
2/6/2019 1:10:18 PM 63.7 56.5
2/6/2019 1:10:19 PM 63.7 56.5
2/6/2019 1:10:20 PM 63.6 56.5
2/6/2019 1:10:21 PM 63.6 56.5
2/6/2019 1:10:22 PM 63.6 56.5
2/6/2019 1:10:23 PM 63.6 56.5
2/6/2019 1:10:24 PM 63.6 56.5
2/6/2019 1:10:25 PM 63.6 56.5
2/6/2019 1:10:26 PM 63.5 56.5
2/6/2019 1:10:27 PM 63.5 56.5
2/6/2019 1:10:28 PM 63.5 56.5
2/6/2019 1:10:29 PM 63.5 56.5
2/6/2019 1:10:30 PM 63.5 56.5
2/6/2019 1:10:31 PM 63.5 56.5
2/6/2019 1:10:32 PM 63.5 56.5
2/6/2019 1:10:33 PM 63.5 56.5
2/6/2019 1:10:34 PM 63.5 56.5
2/6/2019 1:10:35 PM 63.5 56.5
2/6/2019 1:10:36 PM 63.5 56.5
2/6/2019 1:10:37 PM 63.4 56.5
2/6/2019 1:10:38 PM 63.4 56.5
2/6/2019 1:10:39 PM 63.4 56.5
2/6/2019 1:10:40 PM 63.4 56.5
2/6/2019 1:10:41 PM 63.4 56.5
2/6/2019 1:10:42 PM 63.4 56.5
2/6/2019 1:10:43 PM 63.4 56.5
2/6/2019 1:10:44 PM 63.3 56.5
2/6/2019 1:10:45 PM 63.3 56.5
2/6/2019 1:10:46 PM 63.3 56.5
2/6/2019 1:10:47 PM 63.3 56.5
2/6/2019 1:10:48 PM 63.3 56.5
2/6/2019 1:10:49 PM 63.3 56.5
2/6/2019 1:10:50 PM 63.3 56.5
2/6/2019 1:10:51 PM 63.3 56.5
2/6/2019 1:10:52 PM 63.2 56.5
2/6/2019 1:10:53 PM 63.2 56.5
2/6/2019 1:10:54 PM 63.2 56.5
2/6/2019 1:10:55 PM 63.2 56.5
2/6/2019 1:10:56 PM 63.2 56.5
2/6/2019 1:10:57 PM 63.2 56.5
2/6/2019 1:10:58 PM 63.2 56.5
2/6/2019 1:10:59 PM 63.2 56.5
2/6/2019 1:11:00 PM 63.2 56.5
2/6/2019 1:11:01 PM 63.2 56.5
2/6/2019 1:11:02 PM 63.2 56.5
2/6/2019 1:11:03 PM 63.2 56.5
2/6/2019 1:11:04 PM 63.2 56.5
2/6/2019 1:11:05 PM 63.1 56.5
2/6/2019 1:11:06 PM 63.1 56.5
2/6/2019 1:11:07 PM 63.1 56.5
2/6/2019 1:11:08 PM 63.1 56.5
Page 216 of 452 August 2019
APPENDIX E42: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
2/6/2019 1:11:09 PM 63.1 56.5
2/6/2019 1:11:10 PM 63.1 56.5
2/6/2019 1:11:11 PM 63.1 56.5
2/6/2019 1:11:12 PM 63.1 56.5
2/6/2019 1:11:13 PM 63.1 56.5
2/6/2019 1:11:14 PM 63.1 56.5
2/6/2019 1:11:15 PM 63.1 56.5
2/6/2019 1:11:16 PM 63.0 56.5
2/6/2019 1:11:17 PM 63.0 56.5
2/6/2019 1:11:18 PM 63.0 56.5
2/6/2019 1:11:19 PM 63.0 56.5
2/6/2019 1:11:20 PM 63.0 56.5
2/6/2019 1:11:21 PM 63.0 56.5
2/6/2019 1:11:22 PM 63.0 56.5
2/6/2019 1:11:23 PM 63.0 56.5
2/6/2019 1:11:24 PM 63.0 56.5
2/6/2019 1:11:25 PM 63.0 56.5
2/6/2019 1:11:26 PM 62.9 56.5
2/6/2019 1:11:27 PM 62.9 56.5
2/6/2019 1:11:28 PM 62.9 56.5
2/6/2019 1:11:29 PM 62.9 56.5
2/6/2019 1:11:30 PM 62.9 56.5
2/6/2019 1:11:31 PM 62.9 56.5
2/6/2019 1:11:32 PM 62.9 56.5
2/6/2019 1:11:33 PM 62.9 56.5
2/6/2019 1:11:34 PM 62.9 56.5
2/6/2019 1:11:35 PM 62.9 56.5
2/6/2019 1:11:36 PM 62.9 56.5
2/6/2019 1:11:37 PM 62.9 56.5
2/6/2019 1:11:38 PM 62.8 56.5
2/6/2019 1:11:39 PM 62.8 56.5
2/6/2019 1:11:40 PM 62.8 56.5
2/6/2019 1:11:41 PM 62.8 56.5
2/6/2019 1:11:42 PM 62.8 56.5
2/6/2019 1:11:43 PM 62.8 56.5
2/6/2019 1:11:44 PM 62.8 56.5
2/6/2019 1:11:45 PM 62.8 56.5
2/6/2019 1:11:46 PM 62.8 56.5
2/6/2019 1:11:47 PM 62.8 56.5
2/6/2019 1:11:48 PM 62.8 56.5
2/6/2019 1:11:49 PM 62.8 56.5
2/6/2019 1:11:50 PM 62.8 56.5
2/6/2019 1:11:51 PM 62.8 56.5
2/6/2019 1:11:52 PM 62.8 56.5
2/6/2019 1:11:53 PM 62.8 56.5
2/6/2019 1:11:54 PM 62.8 56.5
2/6/2019 1:11:55 PM 62.8 56.5
2/6/2019 1:11:56 PM 62.8 56.5
2/6/2019 1:11:57 PM 62.8 56.5
2/6/2019 1:11:58 PM 62.7 56.5
2/6/2019 1:11:59 PM 62.7 56.5
2/6/2019 1:12:00 PM 62.7 56.5
2/6/2019 1:12:01 PM 62.7 56.5
2/6/2019 1:12:02 PM 62.7 56.5
2/6/2019 1:12:03 PM 62.7 56.5
2/6/2019 1:12:04 PM 62.7 56.5
2/6/2019 1:12:05 PM 62.7 56.5
2/6/2019 1:12:06 PM 62.7 56.5
2/6/2019 1:12:07 PM 62.7 56.5
2/6/2019 1:12:08 PM 62.6 56.5
2/6/2019 1:12:09 PM 62.6 56.5
2/6/2019 1:12:10 PM 62.6 56.5
2/6/2019 1:12:11 PM 62.6 56.5
2/6/2019 1:12:12 PM 62.6 56.5
2/6/2019 1:12:13 PM 62.6 56.5
2/6/2019 1:12:14 PM 62.5 56.5
2/6/2019 1:12:15 PM 62.5 56.5
2/6/2019 1:12:16 PM 62.5 56.5
2/6/2019 1:12:17 PM 62.5 56.5
2/6/2019 1:12:18 PM 62.5 56.5
2/6/2019 1:12:19 PM 62.5 56.5
Page 217 of 452 August 2019
APPENDIX E42: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-B2 TEST-1 1210
SEEP-B2 TEST-1 1211
SEEP-B2 TEST-1 1213
SEEP-B2 TEST-1 1215
Location EC Reading
(µS/cms)
SEEP-B2 TEST-1 83.3
SEEP-B2 TEST-1 311
SEEP-B2 TEST-1 13,770
SEEP-B2 TEST-1 107,962
q 300,200
K 1.0825
1.4
21.9
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)(°C)
Table E2 SEEP-B2 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
93.8 12.5
93.5 12.6
74.7 12.6
Table E3 SEEP-B2 TEST-1 YSI Salt Dilution Calibration DataCalibration
Concentration Temperature
87.2 12.9
Geo Mean 87.9 (µS/cms)
Average
Average (post-test)(µS/cms)
88.2
-
Average (pre-test)97.1 (µS/cms)
(mg/L)(°C)
10 11.3
100 22.5
Integral of Conductivity
Data Curve
SUM:Δt(E
Ct-ECbkg)235,823.5 (s) . (µS/cms)
1,000 21.7
10,000 22.6
Table E4 SEEP-B2 TEST-1 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Calculated Flow Rate Q
L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 218 of 452 August 2019
APPENDIX E43: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/6/2019 12:50:17 PM 56.8 -
2/6/2019 12:50:18 PM 56.8 -
2/6/2019 12:50:19 PM 56.8 -
2/6/2019 12:50:20 PM 56.8 -
2/6/2019 12:50:21 PM 56.7 -
2/6/2019 12:50:22 PM 56.7 -
2/6/2019 12:50:23 PM 56.7 -
2/6/2019 12:50:24 PM 56.7 -
2/6/2019 12:50:25 PM 56.6 -
2/6/2019 12:50:26 PM 56.6 -
2/6/2019 12:50:27 PM 56.5 -
2/6/2019 12:50:28 PM 56.5 -
2/6/2019 12:50:29 PM 56.4 -
2/6/2019 12:50:30 PM 56.4 -
2/6/2019 12:50:31 PM 56.4 -
2/6/2019 12:50:32 PM 56.4 -
2/6/2019 12:50:33 PM 56.4 -
2/6/2019 12:50:34 PM 56.4 -
2/6/2019 12:50:35 PM 56.4 -
2/6/2019 12:50:36 PM 56.4 -
2/6/2019 12:50:37 PM 56.4 -
2/6/2019 12:50:38 PM 56.4 -
2/6/2019 12:50:39 PM 56.4 -
2/6/2019 12:50:40 PM 56.4 -
2/6/2019 12:50:41 PM 56.4 -
2/6/2019 12:50:42 PM 56.4 -
2/6/2019 12:50:43 PM 56.3 -
2/6/2019 12:50:44 PM 56.3 -
2/6/2019 12:50:45 PM 56.2 -
2/6/2019 12:50:46 PM 56.2 -
2/6/2019 12:50:47 PM 56.1 -
2/6/2019 12:50:48 PM 56.1 -
2/6/2019 12:50:49 PM 56.1 -
2/6/2019 12:50:50 PM 56.1 -
2/6/2019 12:50:51 PM 56.0 -
2/6/2019 12:50:52 PM 56.0 0.5
2/6/2019 12:50:53 PM 56.0 1.1
2/6/2019 12:50:54 PM 56.0 3.0
2/6/2019 12:50:55 PM 56.0 77.7
2/6/2019 12:50:56 PM 56.0 159.2
2/6/2019 12:50:57 PM 56.0 278.1
2/6/2019 12:50:58 PM 56.0 510.9
2/6/2019 12:50:59 PM 56.0 699.0
2/6/2019 12:51:00 PM 56.0 1339.0
2/6/2019 12:51:01 PM 56.0 1780.6
2/6/2019 12:51:02 PM 56.0 2340.8
2/6/2019 12:51:03 PM 56.0 2647.9
2/6/2019 12:51:04 PM 56.0 3009.7
2/6/2019 12:51:05 PM 55.9 3627.3
2/6/2019 12:51:06 PM 55.9 4042.2
2/6/2019 12:51:07 PM 55.9 4268.9
2/6/2019 12:51:08 PM 55.9 4344.7
2/6/2019 12:51:09 PM 55.9 4769.5
2/6/2019 12:51:10 PM 55.9 4875.9
2/6/2019 12:51:11 PM 55.9 4932.9
2/6/2019 12:51:12 PM 55.9 4979.4
2/6/2019 12:51:13 PM 55.9 4980.4
2/6/2019 12:51:14 PM 55.8 4971.6
2/6/2019 12:51:15 PM 55.8 4961.0
2/6/2019 12:51:16 PM 55.8 4937.3
2/6/2019 12:51:17 PM 55.8 4903.8
2/6/2019 12:51:18 PM 55.8 4563.4
2/6/2019 12:51:19 PM 55.8 4523.4
2/6/2019 12:51:20 PM 55.8 4422.1
2/6/2019 12:51:21 PM 55.7 4321.7
2/6/2019 12:51:22 PM 55.7 4213.8
2/6/2019 12:51:23 PM 55.7 4110.0
2/6/2019 12:51:24 PM 55.7 4053.3
2/6/2019 12:51:25 PM 55.6 3649.6
2/6/2019 12:51:26 PM 55.6 3542.5
Table E1 SEEP-B2 TEST-2 Data Log
Page 219 of 452 August 2019
APPENDIX E43: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
2/6/2019 12:51:27 PM 55.6 3410.5
2/6/2019 12:51:28 PM 55.6 3348.2
2/6/2019 12:51:29 PM 55.6 3249.5
2/6/2019 12:51:30 PM 55.6 3181.6
2/6/2019 12:51:31 PM 55.6 2930.7
2/6/2019 12:51:32 PM 55.6 2835.3
2/6/2019 12:51:33 PM 55.6 2708.2
2/6/2019 12:51:34 PM 55.6 2689.4
2/6/2019 12:51:35 PM 55.6 2614.9
2/6/2019 12:51:36 PM 55.6 2566.6
2/6/2019 12:51:37 PM 55.6 2360.2
2/6/2019 12:51:38 PM 55.6 2284.8
2/6/2019 12:51:39 PM 55.7 2177.0
2/6/2019 12:51:40 PM 55.7 2136.1
2/6/2019 12:51:41 PM 55.7 2096.3
2/6/2019 12:51:42 PM 55.7 2066.9
2/6/2019 12:51:43 PM 55.7 2034.8
2/6/2019 12:51:44 PM 55.7 1880.1
2/6/2019 12:51:45 PM 55.7 1811.9
2/6/2019 12:51:46 PM 55.8 1752.2
2/6/2019 12:51:47 PM 55.8 1726.4
2/6/2019 12:51:48 PM 56.0 1697.4
2/6/2019 12:51:49 PM 56.2 1664.2
2/6/2019 12:51:50 PM 56.5 1524.5
2/6/2019 12:51:51 PM 57.1 1508.1
2/6/2019 12:51:52 PM 57.7 1443.2
2/6/2019 12:51:53 PM 58.9 1411.7
2/6/2019 12:51:54 PM 60.8 1387.6
2/6/2019 12:51:55 PM 64.1 1369.5
2/6/2019 12:51:56 PM 67.2 1355.5
2/6/2019 12:51:57 PM 71.0 1337.9
2/6/2019 12:51:58 PM 74.5 1234.2
2/6/2019 12:51:59 PM 78.3 1184.9
2/6/2019 12:52:00 PM 81.5 1156.6
2/6/2019 12:52:01 PM 84.5 1135.5
2/6/2019 12:52:02 PM 91.0 1115.5
2/6/2019 12:52:03 PM 96.4 1094.6
2/6/2019 12:52:04 PM 153.3 1078.7
2/6/2019 12:52:05 PM 176.5 996.7
2/6/2019 12:52:06 PM 184.7 972.9
2/6/2019 12:52:07 PM 183.3 946.0
2/6/2019 12:52:08 PM 179.2 923.6
2/6/2019 12:52:09 PM 178.3 904.9
2/6/2019 12:52:10 PM 181.5 886.6
2/6/2019 12:52:11 PM 183.8 868.8
2/6/2019 12:52:12 PM 186.2 806.4
2/6/2019 12:52:13 PM 263.4 785.1
2/6/2019 12:52:14 PM 326.4 760.2
2/6/2019 12:52:15 PM 350.7 751.9
2/6/2019 12:52:16 PM 351.1 740.7
2/6/2019 12:52:17 PM 360.8 730.5
2/6/2019 12:52:18 PM 369.8 663.1
2/6/2019 12:52:19 PM 439.0 642.1
2/6/2019 12:52:20 PM 447.9 619.6
2/6/2019 12:52:21 PM 434.8 609.5
2/6/2019 12:52:22 PM 480.4 600.3
2/6/2019 12:52:23 PM 567.6 596.5
2/6/2019 12:52:24 PM 579.8 528.9
2/6/2019 12:52:25 PM 651.5 544.2
2/6/2019 12:52:26 PM 789.9 534.9
2/6/2019 12:52:27 PM 824.4 532.2
2/6/2019 12:52:28 PM 755.0 527.4
2/6/2019 12:52:29 PM 752.7 519.6
2/6/2019 12:52:30 PM 762.9 511.5
2/6/2019 12:52:31 PM 920.7 505.3
2/6/2019 12:52:32 PM 948.8 499.6
2/6/2019 12:52:33 PM 1012.0 493.5
2/6/2019 12:52:34 PM 1052.5 440.3
2/6/2019 12:52:35 PM 1086.9 428.7
2/6/2019 12:52:36 PM 1227.8 421.8
2/6/2019 12:52:37 PM 1351.8 418.7
2/6/2019 12:52:38 PM 1377.3 414.2
2/6/2019 12:52:39 PM 1398.3 411.1
2/6/2019 12:52:40 PM 1406.5 403.7
2/6/2019 12:52:41 PM 1407.4 398.4
2/6/2019 12:52:42 PM 1421.0 392.5
2/6/2019 12:52:43 PM 1426.8 386.9
Page 220 of 452 August 2019
APPENDIX E43: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
2/6/2019 12:52:44 PM 1431.4 381.5
2/6/2019 12:52:45 PM 1543.6 377.0
2/6/2019 12:52:46 PM 1551.5 371.8
2/6/2019 12:52:47 PM 1550.5 367.9
2/6/2019 12:52:48 PM 1542.2 311.8
2/6/2019 12:52:49 PM 1551.4 311.4
2/6/2019 12:52:50 PM 1556.2 300.2
2/6/2019 12:52:51 PM 1560.2 299.7
2/6/2019 12:52:52 PM 1569.2 294.9
2/6/2019 12:52:53 PM 1658.4 291.1
2/6/2019 12:52:54 PM 1680.1 288.6
2/6/2019 12:52:55 PM 1692.5 285.8
2/6/2019 12:52:56 PM 1686.0 283.2
2/6/2019 12:52:57 PM 1676.3 281.3
2/6/2019 12:52:58 PM 1683.0 278.6
2/6/2019 12:52:59 PM 1812.7 275.5
2/6/2019 12:53:00 PM 1834.6 271.6
2/6/2019 12:53:01 PM 1833.1 268.1
2/6/2019 12:53:02 PM 1831.6 264.4
2/6/2019 12:53:03 PM 1840.1 261.3
2/6/2019 12:53:04 PM 1867.1 255.6
2/6/2019 12:53:05 PM 1891.0 250.0
2/6/2019 12:53:06 PM 1903.2 243.9
2/6/2019 12:53:07 PM 1910.5 238.4
2/6/2019 12:53:08 PM 1918.8 232.4
2/6/2019 12:53:09 PM 1930.0 226.5
2/6/2019 12:53:10 PM 1938.6 221.1
2/6/2019 12:53:11 PM 1946.8 215.1
2/6/2019 12:53:12 PM 1953.4 210.4
2/6/2019 12:53:13 PM 1960.5 205.4
2/6/2019 12:53:14 PM 1965.8 201.0
2/6/2019 12:53:15 PM 1975.5 196.2
2/6/2019 12:53:16 PM 1988.2 192.1
2/6/2019 12:53:17 PM 1998.0 187.7
2/6/2019 12:53:18 PM 2005.1 183.8
2/6/2019 12:53:19 PM 2012.4 179.3
2/6/2019 12:53:20 PM 2019.1 175.7
2/6/2019 12:53:21 PM 2022.8 171.6
2/6/2019 12:53:22 PM 2023.5 168.1
2/6/2019 12:53:23 PM 2023.3 164.4
2/6/2019 12:53:24 PM 2023.5 161.4
2/6/2019 12:53:25 PM 2023.0 158.2
2/6/2019 12:53:26 PM 2020.9 155.6
2/6/2019 12:53:27 PM 2018.9 152.8
2/6/2019 12:53:28 PM 2016.3 150.3
2/6/2019 12:53:29 PM 2014.1 147.6
2/6/2019 12:53:30 PM 2011.2 145.3
2/6/2019 12:53:31 PM 2008.0 142.7
2/6/2019 12:53:32 PM 2003.7 140.4
2/6/2019 12:53:33 PM 1999.5 137.8
2/6/2019 12:53:34 PM 1994.1 135.4
2/6/2019 12:53:35 PM 1988.6 132.5
2/6/2019 12:53:36 PM 1980.1 130.1
2/6/2019 12:53:37 PM 1971.3 127.5
2/6/2019 12:53:38 PM 1863.7 125.2
2/6/2019 12:53:39 PM 1863.6 122.5
2/6/2019 12:53:40 PM 1858.3 120.2
2/6/2019 12:53:41 PM 1852.2 117.8
2/6/2019 12:53:42 PM 1812.2 115.8
2/6/2019 12:53:43 PM 1792.9 113.5
2/6/2019 12:53:44 PM 1785.1 111.5
2/6/2019 12:53:45 PM 1779.0 109.5
2/6/2019 12:53:46 PM 1770.4 108.0
2/6/2019 12:53:47 PM 1764.8 106.4
2/6/2019 12:53:48 PM 1760.3 105.0
2/6/2019 12:53:49 PM 1755.8 103.2
2/6/2019 12:53:50 PM 1749.6 101.7
2/6/2019 12:53:51 PM 1636.6 100.0
2/6/2019 12:53:52 PM 1599.8 98.6
2/6/2019 12:53:53 PM 1587.5 97.1
2/6/2019 12:53:54 PM 1601.0 95.6
2/6/2019 12:53:55 PM 1605.2 94.1
2/6/2019 12:53:56 PM 1606.4 92.8
2/6/2019 12:53:57 PM 1606.2 91.4
2/6/2019 12:53:58 PM 1603.0 90.0
2/6/2019 12:53:59 PM 1592.8 88.1
2/6/2019 12:54:00 PM 1580.3 86.6
2/6/2019 12:54:01 PM 1571.2 85.1
2/6/2019 12:54:02 PM 1564.1 83.8
Page 221 of 452 August 2019
APPENDIX E43: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
2/6/2019 12:54:03 PM 1560.2 82.5
2/6/2019 12:54:04 PM 1555.2 81.2
2/6/2019 12:54:05 PM 1428.7 80.1
2/6/2019 12:54:06 PM 1425.0 79.0
2/6/2019 12:54:07 PM 1409.4 78.0
2/6/2019 12:54:08 PM 1389.7 76.9
2/6/2019 12:54:09 PM 1375.4 75.8
2/6/2019 12:54:10 PM 1376.8 74.6
2/6/2019 12:54:11 PM 1378.9 73.6
2/6/2019 12:54:12 PM 1377.7 72.6
2/6/2019 12:54:13 PM 1374.0 71.7
2/6/2019 12:54:14 PM 1371.2 70.8
2/6/2019 12:54:15 PM 1367.5 70.0
2/6/2019 12:54:16 PM 1364.1 69.1
2/6/2019 12:54:17 PM 1359.5 68.4
2/6/2019 12:54:18 PM 1355.1 67.6
2/6/2019 12:54:19 PM 1352.2 67.0
2/6/2019 12:54:20 PM 1349.8 66.3
2/6/2019 12:54:21 PM 1344.6 65.7
2/6/2019 12:54:22 PM 1261.0 65.1
2/6/2019 12:54:23 PM 1241.4 64.5
2/6/2019 12:54:24 PM 1220.5 63.8
2/6/2019 12:54:25 PM 1209.8 63.2
2/6/2019 12:54:26 PM 1190.0 62.5
2/6/2019 12:54:27 PM 1176.4 61.9
2/6/2019 12:54:28 PM 1173.1 61.1
2/6/2019 12:54:29 PM 1066.2 60.5
2/6/2019 12:54:30 PM 1060.7 59.7
2/6/2019 12:54:31 PM 1044.0 59.0
2/6/2019 12:54:32 PM 1040.0 58.2
2/6/2019 12:54:33 PM 1017.1 57.5
2/6/2019 12:54:34 PM 1003.4 56.7
2/6/2019 12:54:35 PM 1001.6 56.1
2/6/2019 12:54:36 PM 999.4 55.3
2/6/2019 12:54:37 PM 992.1 54.7
2/6/2019 12:54:38 PM 985.8 54.1
2/6/2019 12:54:39 PM 899.3 53.3
2/6/2019 12:54:40 PM 907.6 52.7
2/6/2019 12:54:41 PM 919.5 51.9
2/6/2019 12:54:42 PM 910.2 51.2
2/6/2019 12:54:43 PM 884.2 50.8
2/6/2019 12:54:44 PM 874.9 49.9
2/6/2019 12:54:45 PM 774.7 49.3
2/6/2019 12:54:46 PM 762.1 48.7
2/6/2019 12:54:47 PM 734.8 48.1
2/6/2019 12:54:48 PM 724.9 47.5
2/6/2019 12:54:49 PM 714.9 47.0
2/6/2019 12:54:50 PM 709.9 46.3
2/6/2019 12:54:51 PM 707.2 45.8
2/6/2019 12:54:52 PM 705.3 45.3
2/6/2019 12:54:53 PM 702.1 44.8
2/6/2019 12:54:54 PM 695.2 44.3
2/6/2019 12:54:55 PM 691.3 43.8
2/6/2019 12:54:56 PM 606.3 43.2
2/6/2019 12:54:57 PM 621.2 42.7
2/6/2019 12:54:58 PM 608.8 42.2
2/6/2019 12:54:59 PM 607.5 41.7
2/6/2019 12:55:00 PM 604.3 41.2
2/6/2019 12:55:01 PM 599.2 40.7
2/6/2019 12:55:02 PM 592.1 40.1
2/6/2019 12:55:03 PM 585.2 39.7
2/6/2019 12:55:04 PM 579.9 39.1
2/6/2019 12:55:05 PM 577.1 38.7
2/6/2019 12:55:06 PM 575.1 38.3
2/6/2019 12:55:07 PM 573.3 37.9
2/6/2019 12:55:08 PM 570.4 37.5
2/6/2019 12:55:09 PM 567.2 37.1
2/6/2019 12:55:10 PM 517.7 36.7
2/6/2019 12:55:11 PM 518.4 36.3
2/6/2019 12:55:12 PM 504.2 36.0
2/6/2019 12:55:13 PM 493.0 35.6
2/6/2019 12:55:14 PM 484.2 35.3
2/6/2019 12:55:15 PM 479.6 35.0
2/6/2019 12:55:16 PM 477.0 34.8
2/6/2019 12:55:17 PM 474.4 34.5
2/6/2019 12:55:18 PM 472.3 34.2
2/6/2019 12:55:19 PM 471.5 33.9
2/6/2019 12:55:20 PM 470.5 33.5
2/6/2019 12:55:21 PM 469.3 33.2
Page 222 of 452 August 2019
APPENDIX E43: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
2/6/2019 12:55:22 PM 468.2 33.0
2/6/2019 12:55:23 PM 467.9 32.7
2/6/2019 12:55:24 PM 467.4 32.4
2/6/2019 12:55:25 PM 466.8 32.1
2/6/2019 12:55:26 PM 465.8 31.9
2/6/2019 12:55:27 PM 463.2 31.6
2/6/2019 12:55:28 PM 459.7 31.3
2/6/2019 12:55:29 PM 456.2 31.0
2/6/2019 12:55:30 PM 452.0 30.7
2/6/2019 12:55:31 PM 448.3 30.5
2/6/2019 12:55:32 PM 443.6 30.2
2/6/2019 12:55:33 PM 439.1 30.0
2/6/2019 12:55:34 PM 433.9 29.8
2/6/2019 12:55:35 PM 429.7 29.5
2/6/2019 12:55:36 PM 424.3 29.2
2/6/2019 12:55:37 PM 419.4 28.9
2/6/2019 12:55:38 PM 414.2 28.7
2/6/2019 12:55:39 PM 409.3 28.4
2/6/2019 12:55:40 PM 405.1 28.2
2/6/2019 12:55:41 PM 400.0 27.9
2/6/2019 12:55:42 PM 395.8 27.7
2/6/2019 12:55:43 PM 391.2 27.5
2/6/2019 12:55:44 PM 387.1 27.3
2/6/2019 12:55:45 PM 382.1 27.0
2/6/2019 12:55:46 PM 377.7 26.8
2/6/2019 12:55:47 PM 372.5 26.6
2/6/2019 12:55:48 PM 367.5 26.4
2/6/2019 12:55:49 PM 361.6 26.1
2/6/2019 12:55:50 PM 356.5 25.9
2/6/2019 12:55:51 PM 350.2 25.7
2/6/2019 12:55:52 PM 344.6 25.5
2/6/2019 12:55:53 PM 338.9 25.3
2/6/2019 12:55:54 PM 334.6 25.1
2/6/2019 12:55:55 PM 329.6 24.8
2/6/2019 12:55:56 PM 325.2 24.6
2/6/2019 12:55:57 PM 320.2 24.4
2/6/2019 12:55:58 PM 316.1 24.2
2/6/2019 12:55:59 PM 311.7 24.0
2/6/2019 12:56:00 PM 308.3 23.8
2/6/2019 12:56:01 PM 304.6 23.6
2/6/2019 12:56:02 PM 301.6 23.4
2/6/2019 12:56:03 PM 298.4 23.3
2/6/2019 12:56:04 PM 295.8 23.1
2/6/2019 12:56:05 PM 292.9 22.9
2/6/2019 12:56:06 PM 290.1 22.7
2/6/2019 12:56:07 PM 287.2 22.5
2/6/2019 12:56:08 PM 284.8 22.3
2/6/2019 12:56:09 PM 282.1 22.1
2/6/2019 12:56:10 PM 279.7 21.9
2/6/2019 12:56:11 PM 276.9 21.7
2/6/2019 12:56:12 PM 274.1 21.5
2/6/2019 12:56:13 PM 270.8 21.3
2/6/2019 12:56:14 PM 268.0 21.1
2/6/2019 12:56:15 PM 264.8 21.0
2/6/2019 12:56:16 PM 261.9 20.8
2/6/2019 12:56:17 PM 258.7 20.6
2/6/2019 12:56:18 PM 256.0 20.5
2/6/2019 12:56:19 PM 253.8 20.3
2/6/2019 12:56:20 PM 251.6 20.2
2/6/2019 12:56:21 PM 249.7 20.1
2/6/2019 12:56:22 PM 247.6 20.0
2/6/2019 12:56:23 PM 245.8 19.8
2/6/2019 12:56:24 PM 244.1 19.7
2/6/2019 12:56:25 PM 242.7 19.6
2/6/2019 12:56:26 PM 240.8 19.5
2/6/2019 12:56:27 PM 238.7 19.4
2/6/2019 12:56:28 PM 236.1 19.3
2/6/2019 12:56:29 PM 233.8 19.2
2/6/2019 12:56:30 PM 231.1 19.1
2/6/2019 12:56:31 PM 228.5 19.0
2/6/2019 12:56:32 PM 225.4 18.8
2/6/2019 12:56:33 PM 222.7 18.7
2/6/2019 12:56:34 PM 220.0 18.6
2/6/2019 12:56:35 PM 217.9 18.5
2/6/2019 12:56:36 PM 215.7 18.4
2/6/2019 12:56:37 PM 213.8 18.3
2/6/2019 12:56:38 PM 211.9 18.2
2/6/2019 12:56:39 PM 210.5 18.1
2/6/2019 12:56:40 PM 209.1 18.0
Page 223 of 452 August 2019
APPENDIX E43: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
2/6/2019 12:56:41 PM 208.0 17.9
2/6/2019 12:56:42 PM 206.5 17.8
2/6/2019 12:56:43 PM 205.2 17.7
2/6/2019 12:56:44 PM 203.8 17.6
2/6/2019 12:56:45 PM 202.7 17.5
2/6/2019 12:56:46 PM 201.5 17.4
2/6/2019 12:56:47 PM 200.1 17.3
2/6/2019 12:56:48 PM 198.0 17.2
2/6/2019 12:56:49 PM 196.2 17.1
2/6/2019 12:56:50 PM 194.1 17.0
2/6/2019 12:56:51 PM 192.3 16.8
2/6/2019 12:56:52 PM 190.1 16.7
2/6/2019 12:56:53 PM 188.4 16.6
2/6/2019 12:56:54 PM 186.8 16.5
2/6/2019 12:56:55 PM 185.5 16.3
2/6/2019 12:56:56 PM 184.0 16.2
2/6/2019 12:56:57 PM 182.5 16.1
2/6/2019 12:56:58 PM 181.0 16.0
2/6/2019 12:56:59 PM 179.4 15.9
2/6/2019 12:57:00 PM 178.0 15.8
2/6/2019 12:57:01 PM 176.7 15.6
2/6/2019 12:57:02 PM 175.6 15.5
2/6/2019 12:57:03 PM 174.5 15.4
2/6/2019 12:57:04 PM 173.6 56.5
2/6/2019 12:57:05 PM 172.6 56.5
2/6/2019 12:57:06 PM 171.6 56.5
2/6/2019 12:57:07 PM 170.5 56.5
2/6/2019 12:57:08 PM 169.5 56.5
2/6/2019 12:57:09 PM 168.5 56.5
2/6/2019 12:57:10 PM 167.8 56.5
2/6/2019 12:57:11 PM 166.9 56.5
2/6/2019 12:57:12 PM 166.1 56.5
2/6/2019 12:57:13 PM 165.4 56.5
2/6/2019 12:57:14 PM 164.7 56.5
2/6/2019 12:57:15 PM 163.8 56.5
2/6/2019 12:57:16 PM 162.9 56.5
2/6/2019 12:57:17 PM 161.9 56.5
2/6/2019 12:57:18 PM 161.1 56.5
2/6/2019 12:57:19 PM 160.1 56.5
2/6/2019 12:57:20 PM 159.2 56.5
2/6/2019 12:57:21 PM 158.2 56.5
2/6/2019 12:57:22 PM 157.3 56.5
2/6/2019 12:57:23 PM 156.4 56.5
2/6/2019 12:57:24 PM 155.7 56.5
2/6/2019 12:57:25 PM 155.0 56.5
2/6/2019 12:57:26 PM 154.4 56.5
2/6/2019 12:57:27 PM 153.7 56.5
2/6/2019 12:57:28 PM 153.0 56.5
2/6/2019 12:57:29 PM 152.2 56.5
2/6/2019 12:57:30 PM 151.6 56.5
2/6/2019 12:57:31 PM 150.9 56.5
2/6/2019 12:57:32 PM 150.4 56.5
2/6/2019 12:57:33 PM 149.8 56.5
2/6/2019 12:57:34 PM 149.2 56.5
2/6/2019 12:57:35 PM 148.3 56.5
2/6/2019 12:57:36 PM 147.6 56.5
2/6/2019 12:57:37 PM 146.7 56.5
2/6/2019 12:57:38 PM 145.8 56.5
2/6/2019 12:57:39 PM 145.0 56.5
2/6/2019 12:57:40 PM 144.1 56.5
2/6/2019 12:57:41 PM 143.4 56.5
2/6/2019 12:57:42 PM 142.5 56.5
2/6/2019 12:57:43 PM 141.8 56.5
2/6/2019 12:57:44 PM 141.0 56.5
2/6/2019 12:57:45 PM 140.3 56.5
2/6/2019 12:57:46 PM 139.5 56.5
2/6/2019 12:57:47 PM 138.8 56.5
2/6/2019 12:57:48 PM 138.1 56.5
2/6/2019 12:57:49 PM 137.5 56.5
2/6/2019 12:57:50 PM 136.9 56.5
2/6/2019 12:57:51 PM 136.4 56.5
2/6/2019 12:57:52 PM 136.0 56.5
2/6/2019 12:57:53 PM 135.6 56.5
2/6/2019 12:57:54 PM 135.1 56.5
2/6/2019 12:57:55 PM 134.5 56.5
2/6/2019 12:57:56 PM 133.8 56.5
2/6/2019 12:57:57 PM 133.3 56.5
2/6/2019 12:57:58 PM 132.7 56.5
2/6/2019 12:57:59 PM 132.3 56.5
Page 224 of 452 August 2019
APPENDIX E43: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
2/6/2019 12:58:00 PM 131.7 56.5
2/6/2019 12:58:01 PM 130.9 56.5
2/6/2019 12:58:02 PM 130.4 56.5
2/6/2019 12:58:03 PM 129.9 56.5
2/6/2019 12:58:04 PM 129.1 56.5
2/6/2019 12:58:05 PM 128.6 56.5
2/6/2019 12:58:06 PM 128.2 56.5
2/6/2019 12:58:07 PM 127.7 56.5
2/6/2019 12:58:08 PM 127.4 56.5
2/6/2019 12:58:09 PM 127.2 56.5
2/6/2019 12:58:10 PM 126.9 56.5
2/6/2019 12:58:11 PM 126.5 56.5
2/6/2019 12:58:12 PM 126.0 56.5
2/6/2019 12:58:13 PM 125.6 56.5
2/6/2019 12:58:14 PM 125.0 56.5
2/6/2019 12:58:15 PM 124.6 56.5
2/6/2019 12:58:16 PM 124.0 56.5
2/6/2019 12:58:17 PM 123.5 56.5
2/6/2019 12:58:18 PM 123.0 56.5
2/6/2019 12:58:19 PM 122.4 56.5
2/6/2019 12:58:20 PM 121.8 56.5
2/6/2019 12:58:21 PM 121.1 56.5
2/6/2019 12:58:22 PM 120.4 56.5
2/6/2019 12:58:23 PM 119.7 56.5
2/6/2019 12:58:24 PM 119.1 56.5
2/6/2019 12:58:25 PM 118.6 56.5
2/6/2019 12:58:26 PM 118.1 56.5
2/6/2019 12:58:27 PM 117.6 56.5
2/6/2019 12:58:28 PM 117.2 56.5
2/6/2019 12:58:29 PM 116.7 56.5
2/6/2019 12:58:30 PM 116.3 56.5
2/6/2019 12:58:31 PM 115.8 56.5
2/6/2019 12:58:32 PM 115.4 56.5
2/6/2019 12:58:33 PM 115.0 56.5
2/6/2019 12:58:34 PM 114.7 56.5
2/6/2019 12:58:35 PM 114.4 56.5
2/6/2019 12:58:36 PM 114.1 56.5
2/6/2019 12:58:37 PM 113.8 56.5
2/6/2019 12:58:38 PM 113.5 56.5
2/6/2019 12:58:39 PM 113.2 56.5
2/6/2019 12:58:40 PM 113.0 56.5
2/6/2019 12:58:41 PM 112.7 56.5
2/6/2019 12:58:42 PM 112.5 56.5
2/6/2019 12:58:43 PM 112.2 56.5
2/6/2019 12:58:44 PM 112.0 56.5
2/6/2019 12:58:45 PM 111.8 56.5
2/6/2019 12:58:46 PM 111.7 56.5
2/6/2019 12:58:47 PM 111.5 56.5
2/6/2019 12:58:48 PM 111.4 56.5
2/6/2019 12:58:49 PM 111.2 56.5
2/6/2019 12:58:50 PM 111.0 56.5
2/6/2019 12:58:51 PM 110.7 56.5
2/6/2019 12:58:52 PM 110.4 56.5
2/6/2019 12:58:53 PM 110.0 56.5
2/6/2019 12:58:54 PM 109.6 56.5
2/6/2019 12:58:55 PM 109.2 56.5
2/6/2019 12:58:56 PM 108.8 56.5
2/6/2019 12:58:57 PM 108.3 56.5
2/6/2019 12:58:58 PM 107.9 56.5
2/6/2019 12:58:59 PM 107.4 56.5
2/6/2019 12:59:00 PM 107.0 56.5
2/6/2019 12:59:01 PM 106.5 56.5
2/6/2019 12:59:02 PM 106.0 56.5
2/6/2019 12:59:03 PM 105.5 56.5
2/6/2019 12:59:04 PM 105.2 56.5
2/6/2019 12:59:05 PM 104.8 56.5
2/6/2019 12:59:06 PM 104.4 56.5
2/6/2019 12:59:07 PM 104.1 56.5
2/6/2019 12:59:08 PM 103.8 56.5
2/6/2019 12:59:09 PM 103.5 56.5
2/6/2019 12:59:10 PM 103.2 56.5
2/6/2019 12:59:11 PM 103.0 56.5
2/6/2019 12:59:12 PM 102.6 56.5
2/6/2019 12:59:13 PM 102.3 56.5
2/6/2019 12:59:14 PM 102.0 56.5
2/6/2019 12:59:15 PM 101.7 56.5
2/6/2019 12:59:16 PM 101.4 56.5
2/6/2019 12:59:17 PM 101.1 56.5
2/6/2019 12:59:18 PM 100.8 56.5
Page 225 of 452 August 2019
APPENDIX E43: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
2/6/2019 12:59:19 PM 100.5 56.5
2/6/2019 12:59:20 PM 100.3 56.5
2/6/2019 12:59:21 PM 100.0 56.5
2/6/2019 12:59:22 PM 99.7 56.5
2/6/2019 12:59:23 PM 99.4 56.5
2/6/2019 12:59:24 PM 99.1 56.5
2/6/2019 12:59:25 PM 98.9 56.5
2/6/2019 12:59:26 PM 98.7 56.5
2/6/2019 12:59:27 PM 98.5 56.5
2/6/2019 12:59:28 PM 98.4 56.5
2/6/2019 12:59:29 PM 98.2 56.5
2/6/2019 12:59:30 PM 98.1 56.5
2/6/2019 12:59:31 PM 98.0 56.5
2/6/2019 12:59:32 PM 97.8 56.5
2/6/2019 12:59:33 PM 97.7 56.5
2/6/2019 12:59:34 PM 97.6 56.5
2/6/2019 12:59:35 PM 97.4 56.5
2/6/2019 12:59:36 PM 97.3 56.5
2/6/2019 12:59:37 PM 97.1 56.5
2/6/2019 12:59:38 PM 97.0 56.5
2/6/2019 12:59:39 PM 96.8 56.5
2/6/2019 12:59:40 PM 96.7 56.5
2/6/2019 12:59:41 PM 96.5 56.5
2/6/2019 12:59:42 PM 96.3 56.5
2/6/2019 12:59:43 PM 96.1 56.5
2/6/2019 12:59:44 PM 95.8 56.5
2/6/2019 12:59:45 PM 95.6 56.5
2/6/2019 12:59:46 PM 95.3 56.5
2/6/2019 12:59:47 PM 95.0 56.5
2/6/2019 12:59:48 PM 94.8 56.5
2/6/2019 12:59:49 PM 94.5 56.5
2/6/2019 12:59:50 PM 94.2 56.5
2/6/2019 12:59:51 PM 94.0 56.5
2/6/2019 12:59:52 PM 93.7 56.5
2/6/2019 12:59:53 PM 93.5 56.5
2/6/2019 12:59:54 PM 93.2 56.5
2/6/2019 12:59:55 PM 93.0 56.5
2/6/2019 12:59:56 PM 92.8 56.5
2/6/2019 12:59:57 PM 92.6 56.5
2/6/2019 12:59:58 PM 92.4 56.5
2/6/2019 12:59:59 PM 92.2 56.5
2/6/2019 1:00:00 PM 92.1 56.5
2/6/2019 1:00:01 PM 91.9 56.5
2/6/2019 1:00:02 PM 91.8 56.5
2/6/2019 1:00:03 PM 91.6 56.5
2/6/2019 1:00:04 PM 91.5 56.5
2/6/2019 1:00:05 PM 91.4 56.5
2/6/2019 1:00:06 PM 91.3 56.5
2/6/2019 1:00:07 PM 91.2 56.5
2/6/2019 1:00:08 PM 91.1 56.5
2/6/2019 1:00:09 PM 91.0 56.5
2/6/2019 1:00:10 PM 90.9 56.5
2/6/2019 1:00:11 PM 90.8 56.5
2/6/2019 1:00:12 PM 90.6 56.5
2/6/2019 1:00:13 PM 90.5 56.5
2/6/2019 1:00:14 PM 90.3 56.5
2/6/2019 1:00:15 PM 90.2 56.5
2/6/2019 1:00:16 PM 90.0 56.5
2/6/2019 1:00:17 PM 89.8 56.5
2/6/2019 1:00:18 PM 89.6 56.5
2/6/2019 1:00:19 PM 89.4 56.5
2/6/2019 1:00:20 PM 89.2 56.5
2/6/2019 1:00:21 PM 89.0 56.5
2/6/2019 1:00:22 PM 88.8 56.5
2/6/2019 1:00:23 PM 88.6 56.5
2/6/2019 1:00:24 PM 88.5 56.5
2/6/2019 1:00:25 PM 88.4 56.5
2/6/2019 1:00:26 PM 88.3 56.5
2/6/2019 1:00:27 PM 88.2 56.5
2/6/2019 1:00:28 PM 88.0 56.5
2/6/2019 1:00:29 PM 87.9 56.5
2/6/2019 1:00:30 PM 87.9 56.5
2/6/2019 1:00:31 PM 87.8 56.5
2/6/2019 1:00:32 PM 87.8 56.5
2/6/2019 1:00:33 PM 87.7 56.5
2/6/2019 1:00:34 PM 87.7 56.5
2/6/2019 1:00:35 PM 87.6 56.5
2/6/2019 1:00:36 PM 87.6 56.5
2/6/2019 1:00:37 PM 87.5 56.5
Page 226 of 452 August 2019
APPENDIX E43: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
2/6/2019 1:00:38 PM 87.5 56.5
2/6/2019 1:00:39 PM 87.4 56.5
2/6/2019 1:00:40 PM 87.4 56.5
2/6/2019 1:00:41 PM 87.3 56.5
2/6/2019 1:00:42 PM 87.2 56.5
2/6/2019 1:00:43 PM 87.1 56.5
2/6/2019 1:00:44 PM 87.0 56.5
2/6/2019 1:00:45 PM 86.9 56.5
2/6/2019 1:00:46 PM 86.8 56.5
2/6/2019 1:00:47 PM 86.7 56.5
2/6/2019 1:00:48 PM 86.5 56.5
2/6/2019 1:00:49 PM 86.4 56.5
2/6/2019 1:00:50 PM 86.2 56.5
2/6/2019 1:00:51 PM 86.1 56.5
2/6/2019 1:00:52 PM 85.9 56.5
2/6/2019 1:00:53 PM 85.8 56.5
2/6/2019 1:00:54 PM 85.6 56.5
2/6/2019 1:00:55 PM 85.5 56.5
2/6/2019 1:00:56 PM 85.4 56.5
2/6/2019 1:00:57 PM 85.2 56.5
2/6/2019 1:00:58 PM 85.1 56.5
2/6/2019 1:00:59 PM 84.9 56.5
2/6/2019 1:01:00 PM 84.8 56.5
2/6/2019 1:01:01 PM 84.6 56.5
2/6/2019 1:01:02 PM 84.5 56.5
2/6/2019 1:01:03 PM 84.4 56.5
2/6/2019 1:01:04 PM 84.3 56.5
2/6/2019 1:01:05 PM 84.2 56.5
2/6/2019 1:01:06 PM 84.1 56.5
2/6/2019 1:01:07 PM 84.0 56.5
2/6/2019 1:01:08 PM 83.9 56.5
2/6/2019 1:01:09 PM 83.8 56.5
2/6/2019 1:01:10 PM 83.7 56.5
2/6/2019 1:01:11 PM 83.6 56.5
2/6/2019 1:01:12 PM 83.5 56.5
2/6/2019 1:01:13 PM 83.4 56.5
2/6/2019 1:01:14 PM 83.3 56.5
2/6/2019 1:01:14 PM 83.2 56.5
2/6/2019 1:01:15 PM 83.1 56.5
2/6/2019 1:01:16 PM 83.0 56.5
2/6/2019 1:01:17 PM 82.9 56.5
2/6/2019 1:01:18 PM 82.7 56.5
2/6/2019 1:01:19 PM 82.6 56.5
2/6/2019 1:01:20 PM 82.5 56.5
2/6/2019 1:01:21 PM 82.4 56.5
2/6/2019 1:01:22 PM 82.3 56.5
2/6/2019 1:01:23 PM 82.2 56.5
2/6/2019 1:01:24 PM 82.1 56.5
2/6/2019 1:01:25 PM 82.0 56.5
2/6/2019 1:01:26 PM 81.9 56.5
2/6/2019 1:01:27 PM 81.8 56.5
2/6/2019 1:01:28 PM 81.7 56.5
2/6/2019 1:01:29 PM 81.6 56.5
2/6/2019 1:01:30 PM 81.5 56.5
2/6/2019 1:01:31 PM 81.4 56.5
2/6/2019 1:01:32 PM 81.4 56.5
2/6/2019 1:01:33 PM 81.3 56.5
2/6/2019 1:01:34 PM 81.2 56.5
2/6/2019 1:01:35 PM 81.1 56.5
2/6/2019 1:01:36 PM 81.0 56.5
2/6/2019 1:01:37 PM 81.0 56.5
2/6/2019 1:01:38 PM 80.9 56.5
2/6/2019 1:01:39 PM 80.8 56.5
2/6/2019 1:01:40 PM 80.7 56.5
2/6/2019 1:01:41 PM 80.6 56.5
2/6/2019 1:01:42 PM 80.5 56.5
2/6/2019 1:01:43 PM 80.4 56.5
2/6/2019 1:01:44 PM 80.3 56.5
2/6/2019 1:01:45 PM 80.2 56.5
2/6/2019 1:01:46 PM 80.1 56.5
2/6/2019 1:01:47 PM 80.0 56.5
2/6/2019 1:01:48 PM 79.9 56.5
2/6/2019 1:01:49 PM 79.8 56.5
2/6/2019 1:01:50 PM 79.8 56.5
2/6/2019 1:01:51 PM 79.7 56.5
2/6/2019 1:01:52 PM 79.6 56.5
2/6/2019 1:01:53 PM 79.6 56.5
2/6/2019 1:01:54 PM 79.5 56.5
2/6/2019 1:01:55 PM 79.4 56.5
Page 227 of 452 August 2019
APPENDIX E43: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
2/6/2019 1:01:56 PM 79.4 56.5
2/6/2019 1:01:57 PM 79.4 56.5
2/6/2019 1:01:58 PM 79.3 56.5
2/6/2019 1:01:59 PM 79.3 56.5
2/6/2019 1:02:00 PM 79.3 56.5
2/6/2019 1:02:01 PM 79.2 56.5
2/6/2019 1:02:02 PM 79.2 56.5
2/6/2019 1:02:03 PM 79.2 56.5
2/6/2019 1:02:04 PM 79.1 56.5
2/6/2019 1:02:05 PM 79.1 56.5
2/6/2019 1:02:06 PM 79.1 56.5
2/6/2019 1:02:07 PM 79.0 56.5
2/6/2019 1:02:08 PM 78.9 56.5
2/6/2019 1:02:09 PM 78.9 56.5
2/6/2019 1:02:10 PM 78.8 56.5
2/6/2019 1:02:11 PM 78.7 56.5
2/6/2019 1:02:12 PM 78.6 56.5
2/6/2019 1:02:13 PM 78.5 56.5
2/6/2019 1:02:14 PM 78.5 56.5
2/6/2019 1:02:15 PM 78.4 56.5
2/6/2019 1:02:16 PM 78.3 56.5
2/6/2019 1:02:17 PM 78.2 56.5
2/6/2019 1:02:18 PM 78.1 56.5
2/6/2019 1:02:19 PM 78.0 56.5
2/6/2019 1:02:20 PM 78.0 56.5
2/6/2019 1:02:21 PM 77.9 56.5
2/6/2019 1:02:22 PM 77.8 56.5
2/6/2019 1:02:23 PM 77.7 56.5
2/6/2019 1:02:24 PM 77.6 56.5
2/6/2019 1:02:25 PM 77.5 56.5
2/6/2019 1:02:26 PM 77.4 56.5
2/6/2019 1:02:27 PM 77.3 56.5
2/6/2019 1:02:28 PM 77.2 56.5
2/6/2019 1:02:29 PM 77.1 56.5
2/6/2019 1:02:30 PM 77.1 56.5
2/6/2019 1:02:31 PM 77.0 56.5
2/6/2019 1:02:32 PM 76.9 56.5
2/6/2019 1:02:33 PM 76.9 56.5
2/6/2019 1:02:34 PM 76.8 56.5
2/6/2019 1:02:35 PM 76.8 56.5
2/6/2019 1:02:36 PM 76.7 56.5
2/6/2019 1:02:37 PM 76.7 56.5
2/6/2019 1:02:38 PM 76.7 56.5
2/6/2019 1:02:39 PM 76.6 56.5
2/6/2019 1:02:40 PM 76.6 56.5
2/6/2019 1:02:41 PM 76.5 56.5
2/6/2019 1:02:42 PM 76.5 56.5
2/6/2019 1:02:43 PM 76.4 56.5
2/6/2019 1:02:44 PM 76.4 56.5
2/6/2019 1:02:45 PM 76.3 56.5
2/6/2019 1:02:46 PM 76.3 56.5
2/6/2019 1:02:47 PM 76.2 56.5
2/6/2019 1:02:48 PM 76.1 56.5
2/6/2019 1:02:49 PM 76.1 56.5
2/6/2019 1:02:50 PM 76.0 56.5
2/6/2019 1:02:51 PM 75.9 56.5
2/6/2019 1:02:52 PM 75.9 56.5
2/6/2019 1:02:53 PM 75.8 56.5
2/6/2019 1:02:54 PM 75.7 56.5
2/6/2019 1:02:55 PM 75.7 56.5
2/6/2019 1:02:56 PM 75.6 56.5
2/6/2019 1:02:57 PM 75.6 56.5
2/6/2019 1:02:58 PM 75.5 56.5
2/6/2019 1:02:59 PM 75.5 56.5
2/6/2019 1:03:00 PM 75.5 56.5
2/6/2019 1:03:01 PM 75.4 56.5
2/6/2019 1:03:02 PM 75.4 56.5
2/6/2019 1:03:03 PM 75.4 56.5
2/6/2019 1:03:04 PM 75.3 56.5
2/6/2019 1:03:05 PM 75.3 56.5
2/6/2019 1:03:06 PM 75.2 56.5
2/6/2019 1:03:07 PM 75.1 56.5
2/6/2019 1:03:08 PM 75.1 56.5
2/6/2019 1:03:09 PM 75.0 56.5
2/6/2019 1:03:10 PM 75.0 56.5
2/6/2019 1:03:11 PM 74.9 56.5
2/6/2019 1:03:12 PM 74.8 56.5
2/6/2019 1:03:13 PM 74.8 56.5
2/6/2019 1:03:14 PM 74.7 56.5
Page 228 of 452 August 2019
APPENDIX E43: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
2/6/2019 1:03:15 PM 74.6 56.5
2/6/2019 1:03:16 PM 74.5 56.5
2/6/2019 1:03:17 PM 74.5 56.5
2/6/2019 1:03:18 PM 74.4 56.5
2/6/2019 1:03:19 PM 74.4 56.5
2/6/2019 1:03:20 PM 74.3 56.5
2/6/2019 1:03:21 PM 74.3 56.5
2/6/2019 1:03:22 PM 74.2 56.5
2/6/2019 1:03:23 PM 74.2 56.5
2/6/2019 1:03:24 PM 74.1 56.5
2/6/2019 1:03:25 PM 74.1 56.5
2/6/2019 1:03:26 PM 74.0 56.5
2/6/2019 1:03:27 PM 74.0 56.5
2/6/2019 1:03:28 PM 74.0 56.5
2/6/2019 1:03:29 PM 73.9 56.5
2/6/2019 1:03:30 PM 73.9 56.5
2/6/2019 1:03:31 PM 73.9 56.5
2/6/2019 1:03:32 PM 73.8 56.5
2/6/2019 1:03:33 PM 73.8 56.5
2/6/2019 1:03:34 PM 73.7 56.5
2/6/2019 1:03:35 PM 73.7 56.5
2/6/2019 1:03:36 PM 73.7 56.5
2/6/2019 1:03:37 PM 73.6 56.5
2/6/2019 1:03:38 PM 73.6 56.5
2/6/2019 1:03:39 PM 73.5 56.5
2/6/2019 1:03:40 PM 73.5 56.5
2/6/2019 1:03:41 PM 73.4 56.5
2/6/2019 1:03:42 PM 73.4 56.5
2/6/2019 1:03:43 PM 73.4 56.5
2/6/2019 1:03:44 PM 73.3 56.5
2/6/2019 1:03:45 PM 73.3 56.5
2/6/2019 1:03:46 PM 73.2 56.5
2/6/2019 1:03:47 PM 73.2 56.5
2/6/2019 1:03:48 PM 73.2 56.5
2/6/2019 1:03:49 PM 73.1 56.5
2/6/2019 1:03:50 PM 73.1 56.5
2/6/2019 1:03:51 PM 73.0 56.5
2/6/2019 1:03:52 PM 73.0 56.5
2/6/2019 1:03:53 PM 72.9 56.5
2/6/2019 1:03:54 PM 72.8 56.5
2/6/2019 1:03:55 PM 72.7 56.5
2/6/2019 1:03:56 PM 72.7 56.5
2/6/2019 1:03:57 PM 72.6 56.5
2/6/2019 1:03:58 PM 72.5 56.5
2/6/2019 1:03:59 PM 72.5 56.5
2/6/2019 1:04:00 PM 72.4 56.5
2/6/2019 1:04:01 PM 72.3 56.5
2/6/2019 1:04:02 PM 72.3 56.5
2/6/2019 1:04:03 PM 72.2 56.5
2/6/2019 1:04:04 PM 72.2 56.5
2/6/2019 1:04:05 PM 72.1 56.5
2/6/2019 1:04:06 PM 72.1 56.5
2/6/2019 1:04:07 PM 72.1 56.5
2/6/2019 1:04:08 PM 72.1 56.5
2/6/2019 1:04:09 PM 72.0 56.5
2/6/2019 1:04:10 PM 72.0 56.5
2/6/2019 1:04:11 PM 72.0 56.5
2/6/2019 1:04:12 PM 72.0 56.5
2/6/2019 1:04:13 PM 71.9 56.5
2/6/2019 1:04:14 PM 71.9 56.5
2/6/2019 1:04:15 PM 71.8 56.5
2/6/2019 1:04:16 PM 71.8 56.5
2/6/2019 1:04:17 PM 71.8 56.5
2/6/2019 1:04:18 PM 71.7 56.5
2/6/2019 1:04:19 PM 71.7 56.5
2/6/2019 1:04:20 PM 71.6 56.5
2/6/2019 1:04:21 PM 71.5 56.5
2/6/2019 1:04:22 PM 71.5 56.5
2/6/2019 1:04:23 PM 71.5 56.5
2/6/2019 1:04:24 PM 71.4 56.5
2/6/2019 1:04:25 PM 71.4 56.5
2/6/2019 1:04:26 PM 71.4 56.5
2/6/2019 1:04:27 PM 71.4 56.5
2/6/2019 1:04:28 PM 71.3 56.5
2/6/2019 1:04:29 PM 71.3 56.5
2/6/2019 1:04:30 PM 71.3 56.5
2/6/2019 1:04:31 PM 71.2 56.5
2/6/2019 1:04:32 PM 71.2 56.5
2/6/2019 1:04:33 PM 71.2 56.5
Page 229 of 452 August 2019
APPENDIX E43: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
2/6/2019 1:04:34 PM 71.1 56.5
2/6/2019 1:04:35 PM 71.1 56.5
2/6/2019 1:04:36 PM 71.0 56.5
2/6/2019 1:04:37 PM 71.0 56.5
2/6/2019 1:04:38 PM 70.9 56.5
2/6/2019 1:04:39 PM 70.9 56.5
2/6/2019 1:04:40 PM 70.8 56.5
2/6/2019 1:04:41 PM 70.8 56.5
2/6/2019 1:04:42 PM 70.7 56.5
2/6/2019 1:04:43 PM 70.7 56.5
2/6/2019 1:04:44 PM 70.6 56.5
2/6/2019 1:04:45 PM 70.6 56.5
2/6/2019 1:04:46 PM 70.5 56.5
2/6/2019 1:04:47 PM 70.5 56.5
2/6/2019 1:04:48 PM 70.4 56.5
2/6/2019 1:04:49 PM 70.4 56.5
2/6/2019 1:04:50 PM 70.3 56.5
2/6/2019 1:04:51 PM 70.3 56.5
2/6/2019 1:04:52 PM 70.2 56.5
2/6/2019 1:04:53 PM 70.2 56.5
2/6/2019 1:04:54 PM 70.2 56.5
2/6/2019 1:04:55 PM 70.2 56.5
2/6/2019 1:04:56 PM 70.2 56.5
2/6/2019 1:04:57 PM 70.1 56.5
2/6/2019 1:04:58 PM 70.1 56.5
2/6/2019 1:04:59 PM 70.1 56.5
2/6/2019 1:05:00 PM 70.1 56.5
2/6/2019 1:05:01 PM 70.1 56.5
2/6/2019 1:05:02 PM 70.1 56.5
2/6/2019 1:05:03 PM 70.1 56.5
2/6/2019 1:05:04 PM 70.1 56.5
2/6/2019 1:05:05 PM 70.0 56.5
2/6/2019 1:05:06 PM 70.0 56.5
2/6/2019 1:05:07 PM 70.0 56.5
2/6/2019 1:05:08 PM 70.0 56.5
2/6/2019 1:05:09 PM 69.9 56.5
2/6/2019 1:05:10 PM 69.9 56.5
2/6/2019 1:05:11 PM 69.9 56.5
2/6/2019 1:05:12 PM 69.9 56.5
2/6/2019 1:05:13 PM 69.9 56.5
2/6/2019 1:05:14 PM 69.8 56.5
2/6/2019 1:05:15 PM 69.8 56.5
2/6/2019 1:05:16 PM 69.7 56.5
2/6/2019 1:05:17 PM 69.7 56.5
2/6/2019 1:05:18 PM 69.6 56.5
2/6/2019 1:05:19 PM 69.6 56.5
2/6/2019 1:05:20 PM 69.6 56.5
2/6/2019 1:05:21 PM 69.5 56.5
2/6/2019 1:05:22 PM 69.5 56.5
2/6/2019 1:05:23 PM 69.4 56.5
2/6/2019 1:05:24 PM 69.4 56.5
2/6/2019 1:05:25 PM 69.3 56.5
2/6/2019 1:05:26 PM 69.3 56.5
2/6/2019 1:05:27 PM 69.3 56.5
2/6/2019 1:05:28 PM 69.2 56.5
2/6/2019 1:05:29 PM 69.2 56.5
2/6/2019 1:05:30 PM 69.2 56.5
2/6/2019 1:05:31 PM 69.1 56.5
2/6/2019 1:05:32 PM 69.1 56.5
2/6/2019 1:05:33 PM 69.1 56.5
2/6/2019 1:05:34 PM 69.0 56.5
2/6/2019 1:05:35 PM 69.0 56.5
2/6/2019 1:05:36 PM 69.0 56.5
2/6/2019 1:05:37 PM 68.9 56.5
2/6/2019 1:05:38 PM 68.9 56.5
2/6/2019 1:05:39 PM 68.9 56.5
2/6/2019 1:05:40 PM 68.9 56.5
2/6/2019 1:05:41 PM 68.8 56.5
2/6/2019 1:05:42 PM 68.8 56.5
2/6/2019 1:05:43 PM 68.8 56.5
2/6/2019 1:05:44 PM 68.7 56.5
2/6/2019 1:05:45 PM 68.7 56.5
2/6/2019 1:05:46 PM 68.7 56.5
2/6/2019 1:05:47 PM 68.6 56.5
2/6/2019 1:05:48 PM 68.6 56.5
2/6/2019 1:05:49 PM 68.6 56.5
2/6/2019 1:05:50 PM 68.6 56.5
2/6/2019 1:05:51 PM 68.5 56.5
2/6/2019 1:05:52 PM 68.5 56.5
Page 230 of 452 August 2019
APPENDIX E43: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
2/6/2019 1:05:53 PM 68.5 56.5
2/6/2019 1:05:54 PM 68.5 56.5
2/6/2019 1:05:55 PM 68.5 56.5
2/6/2019 1:05:56 PM 68.4 56.5
2/6/2019 1:05:57 PM 68.4 56.5
2/6/2019 1:05:58 PM 68.4 56.5
2/6/2019 1:05:59 PM 68.4 56.5
2/6/2019 1:06:00 PM 68.3 56.5
2/6/2019 1:06:01 PM 68.3 56.5
2/6/2019 1:06:02 PM 68.3 56.5
2/6/2019 1:06:03 PM 68.3 56.5
2/6/2019 1:06:04 PM 68.2 56.5
2/6/2019 1:06:05 PM 68.2 56.5
2/6/2019 1:06:06 PM 68.2 56.5
2/6/2019 1:06:07 PM 68.1 56.5
2/6/2019 1:06:08 PM 68.1 56.5
2/6/2019 1:06:09 PM 68.1 56.5
2/6/2019 1:06:10 PM 68.1 56.5
2/6/2019 1:06:11 PM 68.1 56.5
2/6/2019 1:06:12 PM 68.0 56.5
2/6/2019 1:06:13 PM 68.0 56.5
2/6/2019 1:06:14 PM 68.0 56.5
2/6/2019 1:06:15 PM 68.0 56.5
2/6/2019 1:06:16 PM 68.0 56.5
2/6/2019 1:06:17 PM 68.0 56.5
2/6/2019 1:06:18 PM 68.0 56.5
2/6/2019 1:06:19 PM 68.0 56.5
2/6/2019 1:06:20 PM 67.9 56.5
2/6/2019 1:06:21 PM 67.9 56.5
2/6/2019 1:06:22 PM 67.9 56.5
2/6/2019 1:06:23 PM 67.8 56.5
2/6/2019 1:06:24 PM 67.8 56.5
2/6/2019 1:06:25 PM 67.8 56.5
2/6/2019 1:06:26 PM 67.7 56.5
2/6/2019 1:06:27 PM 67.7 56.5
2/6/2019 1:06:28 PM 67.7 56.5
2/6/2019 1:06:29 PM 67.6 56.5
2/6/2019 1:06:30 PM 67.6 56.5
2/6/2019 1:06:31 PM 67.6 56.5
2/6/2019 1:06:32 PM 67.6 56.5
2/6/2019 1:06:33 PM 67.5 56.5
2/6/2019 1:06:34 PM 67.5 56.5
2/6/2019 1:06:35 PM 67.5 56.5
2/6/2019 1:06:36 PM 67.4 56.5
2/6/2019 1:06:37 PM 67.4 56.5
2/6/2019 1:06:38 PM 67.4 56.5
2/6/2019 1:06:39 PM 67.4 56.5
2/6/2019 1:06:40 PM 67.3 56.5
2/6/2019 1:06:41 PM 67.3 56.5
2/6/2019 1:06:42 PM 67.3 56.5
2/6/2019 1:06:43 PM 67.3 56.5
2/6/2019 1:06:44 PM 67.3 56.5
2/6/2019 1:06:45 PM 67.2 56.5
2/6/2019 1:06:46 PM 67.2 56.5
2/6/2019 1:06:47 PM 67.2 56.5
2/6/2019 1:06:48 PM 67.2 56.5
2/6/2019 1:06:49 PM 67.2 56.5
2/6/2019 1:06:50 PM 67.2 56.5
2/6/2019 1:06:51 PM 67.2 56.5
2/6/2019 1:06:52 PM 67.1 56.5
2/6/2019 1:06:53 PM 67.1 56.5
2/6/2019 1:06:54 PM 67.1 56.5
2/6/2019 1:06:55 PM 67.1 56.5
2/6/2019 1:06:56 PM 67.1 56.5
2/6/2019 1:06:57 PM 67.1 56.5
2/6/2019 1:06:58 PM 67.1 56.5
2/6/2019 1:06:59 PM 67.1 56.5
2/6/2019 1:07:00 PM 67.0 56.5
2/6/2019 1:07:01 PM 67.0 56.5
2/6/2019 1:07:02 PM 67.0 56.5
2/6/2019 1:07:03 PM 67.0 56.5
2/6/2019 1:07:04 PM 67.0 56.5
2/6/2019 1:07:05 PM 66.9 56.5
2/6/2019 1:07:06 PM 66.9 56.5
2/6/2019 1:07:07 PM 66.9 56.5
2/6/2019 1:07:08 PM 66.9 56.5
2/6/2019 1:07:09 PM 66.9 56.5
2/6/2019 1:07:10 PM 66.9 56.5
2/6/2019 1:07:11 PM 66.8 56.5
Page 231 of 452 August 2019
APPENDIX E43: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
2/6/2019 1:07:12 PM 66.8 56.5
2/6/2019 1:07:13 PM 66.8 56.5
2/6/2019 1:07:14 PM 66.8 56.5
2/6/2019 1:07:15 PM 66.7 56.5
2/6/2019 1:07:16 PM 66.7 56.5
2/6/2019 1:07:17 PM 66.7 56.5
2/6/2019 1:07:18 PM 66.7 56.5
2/6/2019 1:07:19 PM 66.6 56.5
2/6/2019 1:07:20 PM 66.6 56.5
2/6/2019 1:07:21 PM 66.6 56.5
2/6/2019 1:07:22 PM 66.6 56.5
2/6/2019 1:07:23 PM 66.5 56.5
2/6/2019 1:07:24 PM 66.5 56.5
2/6/2019 1:07:25 PM 66.5 56.5
2/6/2019 1:07:26 PM 66.5 56.5
2/6/2019 1:07:27 PM 66.4 56.5
2/6/2019 1:07:28 PM 66.4 56.5
2/6/2019 1:07:29 PM 66.4 56.5
2/6/2019 1:07:30 PM 66.4 56.5
2/6/2019 1:07:31 PM 66.3 56.5
2/6/2019 1:07:32 PM 66.3 56.5
2/6/2019 1:07:33 PM 66.3 56.5
2/6/2019 1:07:34 PM 66.3 56.5
2/6/2019 1:07:35 PM 66.2 56.5
2/6/2019 1:07:36 PM 66.2 56.5
2/6/2019 1:07:37 PM 66.2 56.5
2/6/2019 1:07:38 PM 66.2 56.5
2/6/2019 1:07:39 PM 66.1 56.5
2/6/2019 1:07:40 PM 66.1 56.5
2/6/2019 1:07:41 PM 66.1 56.5
2/6/2019 1:07:42 PM 66.1 56.5
2/6/2019 1:07:43 PM 66.1 56.5
2/6/2019 1:07:44 PM 66.1 56.5
2/6/2019 1:07:45 PM 66.0 56.5
2/6/2019 1:07:46 PM 66.0 56.5
2/6/2019 1:07:47 PM 66.0 56.5
2/6/2019 1:07:48 PM 66.0 56.5
2/6/2019 1:07:49 PM 66.0 56.5
2/6/2019 1:07:50 PM 66.0 56.5
2/6/2019 1:07:51 PM 66.0 56.5
2/6/2019 1:07:52 PM 65.9 56.5
2/6/2019 1:07:53 PM 65.9 56.5
2/6/2019 1:07:54 PM 65.9 56.5
2/6/2019 1:07:55 PM 65.9 56.5
2/6/2019 1:07:56 PM 65.9 56.5
2/6/2019 1:07:57 PM 65.9 56.5
2/6/2019 1:07:58 PM 65.9 56.5
2/6/2019 1:07:59 PM 65.9 56.5
2/6/2019 1:08:00 PM 65.9 56.5
2/6/2019 1:08:01 PM 65.8 56.5
2/6/2019 1:08:02 PM 65.8 56.5
2/6/2019 1:08:03 PM 65.8 56.5
2/6/2019 1:08:04 PM 65.8 56.5
2/6/2019 1:08:05 PM 65.8 56.5
2/6/2019 1:08:06 PM 65.8 56.5
2/6/2019 1:08:07 PM 65.7 56.5
2/6/2019 1:08:08 PM 65.7 56.5
2/6/2019 1:08:09 PM 65.7 56.5
2/6/2019 1:08:10 PM 65.7 56.5
2/6/2019 1:08:11 PM 65.7 56.5
2/6/2019 1:08:12 PM 65.7 56.5
2/6/2019 1:08:13 PM 65.6 56.5
2/6/2019 1:08:14 PM 65.6 56.5
2/6/2019 1:08:15 PM 65.6 56.5
2/6/2019 1:08:16 PM 65.6 56.5
2/6/2019 1:08:17 PM 65.6 56.5
2/6/2019 1:08:18 PM 65.6 56.5
2/6/2019 1:08:19 PM 65.5 56.5
2/6/2019 1:08:20 PM 65.5 56.5
2/6/2019 1:08:21 PM 65.5 56.5
2/6/2019 1:08:22 PM 65.5 56.5
2/6/2019 1:08:23 PM 65.5 56.5
2/6/2019 1:08:24 PM 65.5 56.5
2/6/2019 1:08:25 PM 65.5 56.5
2/6/2019 1:08:26 PM 65.4 56.5
2/6/2019 1:08:27 PM 65.4 56.5
2/6/2019 1:08:28 PM 65.4 56.5
2/6/2019 1:08:29 PM 65.4 56.5
2/6/2019 1:08:30 PM 65.4 56.5
Page 232 of 452 August 2019
APPENDIX E43: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
2/6/2019 1:08:31 PM 65.4 56.5
2/6/2019 1:08:32 PM 65.4 56.5
2/6/2019 1:08:33 PM 65.3 56.5
2/6/2019 1:08:34 PM 65.3 56.5
2/6/2019 1:08:35 PM 65.3 56.5
2/6/2019 1:08:36 PM 65.3 56.5
2/6/2019 1:08:37 PM 65.3 56.5
2/6/2019 1:08:38 PM 65.2 56.5
2/6/2019 1:08:39 PM 65.2 56.5
2/6/2019 1:08:40 PM 65.2 56.5
2/6/2019 1:08:41 PM 65.2 56.5
2/6/2019 1:08:42 PM 65.2 56.5
2/6/2019 1:08:43 PM 65.2 56.5
2/6/2019 1:08:44 PM 65.1 56.5
2/6/2019 1:08:45 PM 65.1 56.5
2/6/2019 1:08:46 PM 65.1 56.5
2/6/2019 1:08:47 PM 65.1 56.5
2/6/2019 1:08:48 PM 65.1 56.5
2/6/2019 1:08:49 PM 65.1 56.5
2/6/2019 1:08:50 PM 65.1 56.5
2/6/2019 1:08:51 PM 65.0 56.5
2/6/2019 1:08:52 PM 65.0 56.5
2/6/2019 1:08:53 PM 65.0 56.5
2/6/2019 1:08:54 PM 65.0 56.5
2/6/2019 1:08:55 PM 65.0 56.5
2/6/2019 1:08:56 PM 65.0 56.5
2/6/2019 1:08:57 PM 64.9 56.5
2/6/2019 1:08:58 PM 64.9 56.5
2/6/2019 1:08:59 PM 64.9 56.5
2/6/2019 1:09:00 PM 64.9 56.5
2/6/2019 1:09:01 PM 64.9 56.5
2/6/2019 1:09:02 PM 64.8 56.5
2/6/2019 1:09:03 PM 64.8 56.5
2/6/2019 1:09:04 PM 64.8 56.5
2/6/2019 1:09:05 PM 64.8 56.5
2/6/2019 1:09:06 PM 64.8 56.5
2/6/2019 1:09:07 PM 64.7 56.5
2/6/2019 1:09:08 PM 64.7 56.5
2/6/2019 1:09:09 PM 64.7 56.5
2/6/2019 1:09:10 PM 64.7 56.5
2/6/2019 1:09:11 PM 64.7 56.5
2/6/2019 1:09:12 PM 64.6 56.5
2/6/2019 1:09:13 PM 64.6 56.5
2/6/2019 1:09:14 PM 64.6 56.5
2/6/2019 1:09:15 PM 64.6 56.5
2/6/2019 1:09:16 PM 64.5 56.5
2/6/2019 1:09:17 PM 64.5 56.5
2/6/2019 1:09:18 PM 64.5 56.5
2/6/2019 1:09:19 PM 64.5 56.5
2/6/2019 1:09:20 PM 64.5 56.5
2/6/2019 1:09:21 PM 64.4 56.5
2/6/2019 1:09:22 PM 64.4 56.5
2/6/2019 1:09:23 PM 64.4 56.5
2/6/2019 1:09:24 PM 64.4 56.5
2/6/2019 1:09:25 PM 64.4 56.5
2/6/2019 1:09:26 PM 64.4 56.5
2/6/2019 1:09:27 PM 64.4 56.5
2/6/2019 1:09:28 PM 64.3 56.5
2/6/2019 1:09:29 PM 64.3 56.5
2/6/2019 1:09:30 PM 64.3 56.5
2/6/2019 1:09:31 PM 64.3 56.5
2/6/2019 1:09:32 PM 64.3 56.5
2/6/2019 1:09:33 PM 64.3 56.5
2/6/2019 1:09:34 PM 64.3 56.5
2/6/2019 1:09:35 PM 64.3 56.5
2/6/2019 1:09:36 PM 64.2 56.5
2/6/2019 1:09:37 PM 64.2 56.5
2/6/2019 1:09:38 PM 64.2 56.5
2/6/2019 1:09:39 PM 64.2 56.5
2/6/2019 1:09:40 PM 64.2 56.5
2/6/2019 1:09:41 PM 64.2 56.5
2/6/2019 1:09:42 PM 64.1 56.5
2/6/2019 1:09:43 PM 64.1 56.5
2/6/2019 1:09:44 PM 64.1 56.5
2/6/2019 1:09:45 PM 64.1 56.5
2/6/2019 1:09:46 PM 64.1 56.5
2/6/2019 1:09:47 PM 64.1 56.5
2/6/2019 1:09:48 PM 64.0 56.5
2/6/2019 1:09:49 PM 64.0 56.5
Page 233 of 452 August 2019
APPENDIX E43: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
2/6/2019 1:09:50 PM 64.0 56.5
2/6/2019 1:09:51 PM 64.0 56.5
2/6/2019 1:09:52 PM 64.0 56.5
2/6/2019 1:09:53 PM 64.0 56.5
2/6/2019 1:09:54 PM 64.0 56.5
2/6/2019 1:09:55 PM 63.9 56.5
2/6/2019 1:09:56 PM 63.9 56.5
2/6/2019 1:09:57 PM 63.9 56.5
2/6/2019 1:09:58 PM 63.9 56.5
2/6/2019 1:09:59 PM 63.9 56.5
2/6/2019 1:10:00 PM 63.9 56.5
2/6/2019 1:10:01 PM 63.9 56.5
2/6/2019 1:10:02 PM 63.8 56.5
2/6/2019 1:10:03 PM 63.8 56.5
2/6/2019 1:10:04 PM 63.8 56.5
2/6/2019 1:10:05 PM 63.8 56.5
2/6/2019 1:10:06 PM 63.8 56.5
2/6/2019 1:10:07 PM 63.8 56.5
2/6/2019 1:10:08 PM 63.8 56.5
2/6/2019 1:10:09 PM 63.8 56.5
2/6/2019 1:10:10 PM 63.8 56.5
2/6/2019 1:10:11 PM 63.7 56.5
2/6/2019 1:10:12 PM 63.7 56.5
2/6/2019 1:10:13 PM 63.7 56.5
2/6/2019 1:10:14 PM 63.7 56.5
2/6/2019 1:10:15 PM 63.7 56.5
2/6/2019 1:10:16 PM 63.7 56.5
2/6/2019 1:10:17 PM 63.7 56.5
2/6/2019 1:10:18 PM 63.7 56.5
2/6/2019 1:10:19 PM 63.7 56.5
2/6/2019 1:10:20 PM 63.6 56.5
2/6/2019 1:10:21 PM 63.6 56.5
2/6/2019 1:10:22 PM 63.6 56.5
2/6/2019 1:10:23 PM 63.6 56.5
2/6/2019 1:10:24 PM 63.6 56.5
2/6/2019 1:10:25 PM 63.6 56.5
2/6/2019 1:10:26 PM 63.5 56.5
2/6/2019 1:10:27 PM 63.5 56.5
2/6/2019 1:10:28 PM 63.5 56.5
2/6/2019 1:10:29 PM 63.5 56.5
2/6/2019 1:10:30 PM 63.5 56.5
2/6/2019 1:10:31 PM 63.5 56.5
2/6/2019 1:10:32 PM 63.5 56.5
2/6/2019 1:10:33 PM 63.5 56.5
2/6/2019 1:10:34 PM 63.5 56.5
2/6/2019 1:10:35 PM 63.5 56.5
2/6/2019 1:10:36 PM 63.5 56.5
2/6/2019 1:10:37 PM 63.4 56.5
2/6/2019 1:10:38 PM 63.4 56.5
2/6/2019 1:10:39 PM 63.4 56.5
2/6/2019 1:10:40 PM 63.4 56.5
2/6/2019 1:10:41 PM 63.4 56.5
2/6/2019 1:10:42 PM 63.4 56.5
2/6/2019 1:10:43 PM 63.4 56.5
2/6/2019 1:10:44 PM 63.3 56.5
2/6/2019 1:10:45 PM 63.3 56.5
2/6/2019 1:10:46 PM 63.3 56.5
2/6/2019 1:10:47 PM 63.3 56.5
2/6/2019 1:10:48 PM 63.3 56.5
2/6/2019 1:10:49 PM 63.3 56.5
2/6/2019 1:10:50 PM 63.3 56.5
2/6/2019 1:10:51 PM 63.3 56.5
2/6/2019 1:10:52 PM 63.2 56.5
2/6/2019 1:10:53 PM 63.2 56.5
2/6/2019 1:10:54 PM 63.2 56.5
2/6/2019 1:10:55 PM 63.2 56.5
2/6/2019 1:10:56 PM 63.2 56.5
2/6/2019 1:10:57 PM 63.2 56.5
2/6/2019 1:10:58 PM 63.2 56.5
2/6/2019 1:10:59 PM 63.2 56.5
2/6/2019 1:11:00 PM 63.2 56.5
2/6/2019 1:11:01 PM 63.2 56.5
2/6/2019 1:11:02 PM 63.2 56.5
2/6/2019 1:11:03 PM 63.2 56.5
2/6/2019 1:11:04 PM 63.2 56.5
2/6/2019 1:11:05 PM 63.1 56.5
2/6/2019 1:11:06 PM 63.1 56.5
2/6/2019 1:11:07 PM 63.1 56.5
2/6/2019 1:11:08 PM 63.1 56.5
Page 234 of 452 August 2019
APPENDIX E43: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
2/6/2019 1:11:09 PM 63.1 56.5
2/6/2019 1:11:10 PM 63.1 56.5
2/6/2019 1:11:11 PM 63.1 56.5
2/6/2019 1:11:12 PM 63.1 56.5
2/6/2019 1:11:13 PM 63.1 56.5
2/6/2019 1:11:14 PM 63.1 56.5
2/6/2019 1:11:15 PM 63.1 56.5
2/6/2019 1:11:16 PM 63.0 56.5
2/6/2019 1:11:17 PM 63.0 56.5
2/6/2019 1:11:18 PM 63.0 56.5
2/6/2019 1:11:19 PM 63.0 56.5
2/6/2019 1:11:20 PM 63.0 56.5
2/6/2019 1:11:21 PM 63.0 56.5
2/6/2019 1:11:22 PM 63.0 56.5
2/6/2019 1:11:23 PM 63.0 56.5
2/6/2019 1:11:24 PM 63.0 56.5
2/6/2019 1:11:25 PM 63.0 56.5
2/6/2019 1:11:26 PM 62.9 56.5
2/6/2019 1:11:27 PM 62.9 56.5
2/6/2019 1:11:28 PM 62.9 56.5
2/6/2019 1:11:29 PM 62.9 56.5
2/6/2019 1:11:30 PM 62.9 56.5
2/6/2019 1:11:31 PM 62.9 56.5
2/6/2019 1:11:32 PM 62.9 56.5
2/6/2019 1:11:33 PM 62.9 56.5
2/6/2019 1:11:34 PM 62.9 56.5
2/6/2019 1:11:35 PM 62.9 56.5
2/6/2019 1:11:36 PM 62.9 56.5
2/6/2019 1:11:37 PM 62.9 56.5
2/6/2019 1:11:38 PM 62.8 56.5
2/6/2019 1:11:39 PM 62.8 56.5
2/6/2019 1:11:40 PM 62.8 56.5
2/6/2019 1:11:41 PM 62.8 56.5
2/6/2019 1:11:42 PM 62.8 56.5
2/6/2019 1:11:43 PM 62.8 56.5
2/6/2019 1:11:44 PM 62.8 56.5
2/6/2019 1:11:45 PM 62.8 56.5
2/6/2019 1:11:46 PM 62.8 56.5
2/6/2019 1:11:47 PM 62.8 56.5
2/6/2019 1:11:48 PM 62.8 56.5
2/6/2019 1:11:49 PM 62.8 56.5
2/6/2019 1:11:50 PM 62.8 56.5
2/6/2019 1:11:51 PM 62.8 56.5
2/6/2019 1:11:52 PM 62.8 56.5
2/6/2019 1:11:53 PM 62.8 56.5
2/6/2019 1:11:54 PM 62.8 56.5
2/6/2019 1:11:55 PM 62.8 56.5
2/6/2019 1:11:56 PM 62.8 56.5
2/6/2019 1:11:57 PM 62.8 56.5
2/6/2019 1:11:58 PM 62.7 56.5
2/6/2019 1:11:59 PM 62.7 56.5
2/6/2019 1:12:00 PM 62.7 56.5
2/6/2019 1:12:01 PM 62.7 56.5
2/6/2019 1:12:02 PM 62.7 56.5
2/6/2019 1:12:03 PM 62.7 56.5
2/6/2019 1:12:04 PM 62.7 56.5
2/6/2019 1:12:05 PM 62.7 56.5
2/6/2019 1:12:06 PM 62.7 56.5
2/6/2019 1:12:07 PM 62.7 56.5
2/6/2019 1:12:08 PM 62.6 56.5
2/6/2019 1:12:09 PM 62.6 56.5
2/6/2019 1:12:10 PM 62.6 56.5
2/6/2019 1:12:11 PM 62.6 56.5
2/6/2019 1:12:12 PM 62.6 56.5
2/6/2019 1:12:13 PM 62.6 56.5
2/6/2019 1:12:14 PM 62.5 56.5
2/6/2019 1:12:15 PM 62.5 56.5
2/6/2019 1:12:16 PM 62.5 56.5
2/6/2019 1:12:17 PM 62.5 56.5
2/6/2019 1:12:18 PM 62.5 56.5
2/6/2019 1:12:19 PM 62.5 56.5
Page 235 of 452 August 2019
APPENDIX E43: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-B2 TEST-2 1210
SEEP-B2 TEST-2 1211
SEEP-B2 TEST-2 1213
SEEP-B2 TEST-2 1215
Location EC Reading
(µS/cms)
SEEP-B2 TEST-2 40.2
SEEP-B2 TEST-2 193
SEEP-B2 TEST-2 1,593
SEEP-B2 TEST-2 13,094
SEEP-B2 TEST-2 103,212
q 299,600
K 1.0825
1.4
22.3
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)(°C)
Table E2 SEEP-B2 TEST-2 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Geometric Mean 53.5 (µS/cms)
53.7 12.5
53.5 12.6
53.6 12.6
53.3 12.9
Average 53.5 (µS/cms)
Average (pre-test)59.1 (µS/cms)
Table E3 SEEP-B2 TEST-2 YSI Salt Dilution Calibration Data
Calibration Temperature
(mg/L)(°C)
10 20.9
100 21.3
Integral of Conductivity
Data Curve
SUM:Δt(E
Ct-ECbkg)230,775.1 (s) . (µS/cms)
1,000 21.6
10,000 21.9
100,000 21.9
Table E4 SEEP-B2 TEST-2 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Calculated Flow Rate Q
L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 236 of 452 August 2019
APPENDIX E44: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-3 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/6/2019 11:25:25 AM 90.1 -
2/6/2019 11:25:26 AM 90.0 -
2/6/2019 11:25:27 AM 90.0 -
2/6/2019 11:25:28 AM 90.0 -
2/6/2019 11:25:29 AM 90.0 -
2/6/2019 11:25:30 AM 90.0 -
2/6/2019 11:25:31 AM 90.0 -
2/6/2019 11:25:32 AM 90.0 -
2/6/2019 11:25:33 AM 90.0 -
2/6/2019 11:25:34 AM 90.0 -
2/6/2019 11:25:35 AM 90.0 -
2/6/2019 11:25:36 AM 89.9 -
2/6/2019 11:25:37 AM 89.9 -
2/6/2019 11:25:38 AM 89.9 -
2/6/2019 11:25:39 AM 89.9 -
2/6/2019 11:25:40 AM 89.9 -
2/6/2019 11:25:41 AM 89.9 -
2/6/2019 11:25:42 AM 89.9 -
2/6/2019 11:25:43 AM 89.9 -
2/6/2019 11:25:44 AM 89.9 -
2/6/2019 11:25:45 AM 89.9 -
2/6/2019 11:25:46 AM 89.9 -
2/6/2019 11:25:47 AM 89.9 -
2/6/2019 11:25:48 AM 89.9 -
2/6/2019 11:25:49 AM 89.9 -
2/6/2019 11:25:50 AM 89.9 -
2/6/2019 11:25:51 AM 89.9 -
2/6/2019 11:25:52 AM 89.9 -
2/6/2019 11:25:53 AM 89.9 -
2/6/2019 11:25:54 AM 90.0 -
2/6/2019 11:25:55 AM 90.1 -
2/6/2019 11:25:56 AM 90.4 -
2/6/2019 11:25:57 AM 91.5 1.5
2/6/2019 11:25:58 AM 162.7 72.7
2/6/2019 11:25:59 AM 239.8 149.8
2/6/2019 11:26:00 AM 408.2 318.2
2/6/2019 11:26:01 AM 675.2 585.2
2/6/2019 11:26:02 AM 816.0 726.0
2/6/2019 11:26:03 AM 1456.0 1366.0
2/6/2019 11:26:04 AM 2048.6 1958.6
2/6/2019 11:26:05 AM 2439.3 2349.3
2/6/2019 11:26:06 AM 2849.4 2759.4
2/6/2019 11:26:07 AM 3371.8 3281.8
2/6/2019 11:26:08 AM 3713.8 3623.8
2/6/2019 11:26:09 AM 4190.6 4100.6
2/6/2019 11:26:10 AM 4654.9 4564.9
2/6/2019 11:26:11 AM 5025.4 4935.4
2/6/2019 11:26:12 AM 5161.8 5071.8
2/6/2019 11:26:13 AM 5283.4 5193.4
2/6/2019 11:26:14 AM 5427.7 5337.7
2/6/2019 11:26:15 AM 5508.6 5418.6
2/6/2019 11:26:16 AM 5568.0 5478.0
2/6/2019 11:26:17 AM 5602.5 5512.5
2/6/2019 11:26:18 AM 5622.7 5532.7
2/6/2019 11:26:19 AM 5623.4 5533.4
2/6/2019 11:26:20 AM 5612.2 5522.2
2/6/2019 11:26:21 AM 5595.0 5505.0
2/6/2019 11:26:22 AM 5210.1 5120.1
2/6/2019 11:26:23 AM 5048.2 4958.2
2/6/2019 11:26:24 AM 4832.6 4742.6
2/6/2019 11:26:25 AM 4685.4 4595.4
2/6/2019 11:26:26 AM 4573.5 4483.5
2/6/2019 11:26:27 AM 4215.9 4125.9
2/6/2019 11:26:28 AM 4028.3 3938.3
2/6/2019 11:26:29 AM 3874.8 3784.8
2/6/2019 11:26:30 AM 3699.2 3609.2
2/6/2019 11:26:31 AM 3646.7 3556.7
2/6/2019 11:26:32 AM 3357.5 3267.5
2/6/2019 11:26:33 AM 3214.9 3124.9
2/6/2019 11:26:34 AM 3067.6 2977.6
Table E1 SEEP-B2 TEST-3 Data Log
Page 237 of 452 August 2019
APPENDIX E44: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-3 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-3 Data Log
2/6/2019 11:26:35 AM 2931.1 2841.1
2/6/2019 11:26:36 AM 2867.0 2777.0
2/6/2019 11:26:37 AM 2782.0 2692.0
2/6/2019 11:26:38 AM 2483.4 2393.4
2/6/2019 11:26:39 AM 2378.9 2288.9
2/6/2019 11:26:40 AM 2250.6 2160.6
2/6/2019 11:26:41 AM 2213.7 2123.7
2/6/2019 11:26:42 AM 2152.0 2062.0
2/6/2019 11:26:43 AM 1966.6 1876.6
2/6/2019 11:26:44 AM 1836.4 1746.4
2/6/2019 11:26:45 AM 1752.3 1662.3
2/6/2019 11:26:46 AM 1698.7 1608.7
2/6/2019 11:26:47 AM 1663.4 1573.4
2/6/2019 11:26:48 AM 1525.8 1435.8
2/6/2019 11:26:49 AM 1460.3 1370.3
2/6/2019 11:26:50 AM 1392.2 1302.2
2/6/2019 11:26:51 AM 1345.5 1255.5
2/6/2019 11:26:52 AM 1323.3 1233.3
2/6/2019 11:26:53 AM 1300.3 1210.3
2/6/2019 11:26:54 AM 1188.6 1098.6
2/6/2019 11:26:55 AM 1140.0 1050.0
2/6/2019 11:26:56 AM 1090.8 1000.8
2/6/2019 11:26:57 AM 1076.4 986.4
2/6/2019 11:26:58 AM 1043.0 953.0
2/6/2019 11:26:59 AM 1017.3 927.3
2/6/2019 11:27:00 AM 934.1 844.1
2/6/2019 11:27:01 AM 906.9 816.9
2/6/2019 11:27:02 AM 879.7 789.7
2/6/2019 11:27:03 AM 867.1 777.1
2/6/2019 11:27:04 AM 845.6 755.6
2/6/2019 11:27:05 AM 833.9 743.9
2/6/2019 11:27:06 AM 771.4 681.4
2/6/2019 11:27:07 AM 736.4 646.4
2/6/2019 11:27:08 AM 711.7 621.7
2/6/2019 11:27:09 AM 700.4 610.4
2/6/2019 11:27:10 AM 692.3 602.3
2/6/2019 11:27:11 AM 585.1 495.1
2/6/2019 11:27:12 AM 625.2 535.2
2/6/2019 11:27:13 AM 611.3 521.3
2/6/2019 11:27:14 AM 597.4 507.4
2/6/2019 11:27:15 AM 586.8 496.8
2/6/2019 11:27:16 AM 573.3 483.3
2/6/2019 11:27:17 AM 564.0 474.0
2/6/2019 11:27:18 AM 557.0 467.0
2/6/2019 11:27:19 AM 549.0 459.0
2/6/2019 11:27:20 AM 495.2 405.2
2/6/2019 11:27:21 AM 480.8 390.8
2/6/2019 11:27:22 AM 470.2 380.2
2/6/2019 11:27:23 AM 457.4 367.4
2/6/2019 11:27:24 AM 453.4 363.4
2/6/2019 11:27:25 AM 446.2 356.2
2/6/2019 11:27:26 AM 440.5 350.5
2/6/2019 11:27:27 AM 434.8 344.8
2/6/2019 11:27:28 AM 430.2 340.2
2/6/2019 11:27:29 AM 424.7 334.7
2/6/2019 11:27:30 AM 420.2 330.2
2/6/2019 11:27:31 AM 414.9 324.9
2/6/2019 11:27:32 AM 410.6 320.6
2/6/2019 11:27:33 AM 405.9 315.9
2/6/2019 11:27:34 AM 353.3 263.3
2/6/2019 11:27:35 AM 345.8 255.8
2/6/2019 11:27:36 AM 338.4 248.4
2/6/2019 11:27:37 AM 335.0 245.0
2/6/2019 11:27:38 AM 331.2 241.2
2/6/2019 11:27:39 AM 327.7 237.7
2/6/2019 11:27:40 AM 325.1 235.1
2/6/2019 11:27:41 AM 322.0 232.0
2/6/2019 11:27:42 AM 319.2 229.2
2/6/2019 11:27:43 AM 316.0 226.0
2/6/2019 11:27:44 AM 313.2 223.2
2/6/2019 11:27:45 AM 310.2 220.2
2/6/2019 11:27:46 AM 307.7 217.7
2/6/2019 11:27:47 AM 305.0 215.0
2/6/2019 11:27:48 AM 302.7 212.7
2/6/2019 11:27:49 AM 300.0 210.0
2/6/2019 11:27:50 AM 297.3 207.3
2/6/2019 11:27:51 AM 292.0 202.0
Page 238 of 452 August 2019
APPENDIX E44: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-3 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-3 Data Log
2/6/2019 11:27:52 AM 286.7 196.7
2/6/2019 11:27:53 AM 282.0 192.0
2/6/2019 11:27:54 AM 277.0 187.0
2/6/2019 11:27:55 AM 272.8 182.8
2/6/2019 11:27:56 AM 268.3 178.3
2/6/2019 11:27:57 AM 264.5 174.5
2/6/2019 11:27:58 AM 260.3 170.3
2/6/2019 11:27:59 AM 256.6 166.6
2/6/2019 11:28:00 AM 252.4 162.4
2/6/2019 11:28:01 AM 248.9 158.9
2/6/2019 11:28:02 AM 245.1 155.1
2/6/2019 11:28:03 AM 241.8 151.8
2/6/2019 11:28:04 AM 238.1 148.1
2/6/2019 11:28:05 AM 235.0 145.0
2/6/2019 11:28:06 AM 231.5 141.5
2/6/2019 11:28:07 AM 228.4 138.4
2/6/2019 11:28:08 AM 224.9 134.9
2/6/2019 11:28:09 AM 221.9 131.9
2/6/2019 11:28:10 AM 218.4 128.4
2/6/2019 11:28:11 AM 215.5 125.5
2/6/2019 11:28:12 AM 212.2 122.2
2/6/2019 11:28:13 AM 209.5 119.5
2/6/2019 11:28:14 AM 206.5 116.5
2/6/2019 11:28:15 AM 203.9 113.9
2/6/2019 11:28:16 AM 201.0 111.0
2/6/2019 11:28:17 AM 198.6 108.6
2/6/2019 11:28:18 AM 196.0 106.0
2/6/2019 11:28:19 AM 193.9 103.9
2/6/2019 11:28:20 AM 191.8 101.8
2/6/2019 11:28:21 AM 190.0 100.0
2/6/2019 11:28:22 AM 188.0 98.0
2/6/2019 11:28:23 AM 186.4 96.4
2/6/2019 11:28:24 AM 184.7 94.7
2/6/2019 11:28:25 AM 183.3 93.3
2/6/2019 11:28:26 AM 181.7 91.7
2/6/2019 11:28:27 AM 180.3 90.3
2/6/2019 11:28:28 AM 178.8 88.8
2/6/2019 11:28:29 AM 177.5 87.5
2/6/2019 11:28:30 AM 176.1 86.1
2/6/2019 11:28:31 AM 174.7 84.7
2/6/2019 11:28:32 AM 173.5 83.5
2/6/2019 11:28:33 AM 172.0 82.0
2/6/2019 11:28:34 AM 170.7 80.7
2/6/2019 11:28:35 AM 169.2 79.2
2/6/2019 11:28:36 AM 167.9 77.9
2/6/2019 11:28:37 AM 166.6 76.6
2/6/2019 11:28:38 AM 165.4 75.4
2/6/2019 11:28:39 AM 164.0 74.0
2/6/2019 11:28:40 AM 162.8 72.8
2/6/2019 11:28:41 AM 161.5 71.5
2/6/2019 11:28:42 AM 160.4 70.4
2/6/2019 11:28:43 AM 159.1 69.1
2/6/2019 11:28:44 AM 158.0 68.0
2/6/2019 11:28:45 AM 156.8 66.8
2/6/2019 11:28:46 AM 155.8 65.8
2/6/2019 11:28:47 AM 154.6 64.6
2/6/2019 11:28:48 AM 153.7 63.7
2/6/2019 11:28:49 AM 152.6 62.6
2/6/2019 11:28:50 AM 151.7 61.7
2/6/2019 11:28:51 AM 150.6 60.6
2/6/2019 11:28:52 AM 149.6 59.6
2/6/2019 11:28:53 AM 148.5 58.5
2/6/2019 11:28:54 AM 147.6 57.6
2/6/2019 11:28:55 AM 146.4 56.4
2/6/2019 11:28:56 AM 145.4 55.4
2/6/2019 11:28:57 AM 144.2 54.2
2/6/2019 11:28:58 AM 143.3 53.3
2/6/2019 11:28:59 AM 142.2 52.2
2/6/2019 11:29:00 AM 141.2 51.2
2/6/2019 11:29:01 AM 140.1 50.1
2/6/2019 11:29:02 AM 139.1 49.1
2/6/2019 11:29:03 AM 138.0 48.0
2/6/2019 11:29:04 AM 137.1 47.1
2/6/2019 11:29:05 AM 136.1 46.1
2/6/2019 11:29:06 AM 135.1 45.1
2/6/2019 11:29:07 AM 134.1 44.1
2/6/2019 11:29:08 AM 133.3 43.3
2/6/2019 11:29:09 AM 132.4 42.4
2/6/2019 11:29:10 AM 131.6 41.6
Page 239 of 452 August 2019
APPENDIX E44: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-3 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-3 Data Log
2/6/2019 11:29:11 AM 130.8 40.8
2/6/2019 11:29:12 AM 130.0 40.0
2/6/2019 11:29:13 AM 129.3 39.3
2/6/2019 11:29:14 AM 128.5 38.5
2/6/2019 11:29:15 AM 127.9 37.9
2/6/2019 11:29:16 AM 127.1 37.1
2/6/2019 11:29:17 AM 126.5 36.5
2/6/2019 11:29:18 AM 125.8 35.8
2/6/2019 11:29:19 AM 125.3 35.3
2/6/2019 11:29:20 AM 124.6 34.6
2/6/2019 11:29:21 AM 124.1 34.1
2/6/2019 11:29:22 AM 123.5 33.5
2/6/2019 11:29:23 AM 123.1 33.1
2/6/2019 11:29:24 AM 122.5 32.5
2/6/2019 11:29:25 AM 122.0 32.0
2/6/2019 11:29:26 AM 121.4 31.4
2/6/2019 11:29:27 AM 120.9 30.9
2/6/2019 11:29:28 AM 120.4 30.4
2/6/2019 11:29:29 AM 119.9 29.9
2/6/2019 11:29:30 AM 119.4 29.4
2/6/2019 11:29:31 AM 118.9 28.9
2/6/2019 11:29:32 AM 118.4 28.4
2/6/2019 11:29:33 AM 118.0 28.0
2/6/2019 11:29:34 AM 117.5 27.5
2/6/2019 11:29:35 AM 117.0 27.0
2/6/2019 11:29:36 AM 116.6 26.6
2/6/2019 11:29:37 AM 116.2 26.2
2/6/2019 11:29:38 AM 115.7 25.7
2/6/2019 11:29:39 AM 115.3 25.3
2/6/2019 11:29:40 AM 114.9 24.9
2/6/2019 11:29:41 AM 114.5 24.5
2/6/2019 11:29:42 AM 114.1 24.1
2/6/2019 11:29:43 AM 113.8 23.8
2/6/2019 11:29:44 AM 113.5 23.5
2/6/2019 11:29:45 AM 113.2 23.2
2/6/2019 11:29:46 AM 112.8 22.8
2/6/2019 11:29:47 AM 112.5 22.5
2/6/2019 11:29:48 AM 112.2 22.2
2/6/2019 11:29:49 AM 111.9 21.9
2/6/2019 11:29:50 AM 111.6 21.6
2/6/2019 11:29:51 AM 111.2 21.2
2/6/2019 11:29:52 AM 110.9 20.9
2/6/2019 11:29:53 AM 110.5 20.5
2/6/2019 11:29:54 AM 110.2 20.2
2/6/2019 11:29:55 AM 109.9 19.9
2/6/2019 11:29:56 AM 109.6 19.6
2/6/2019 11:29:57 AM 109.2 19.2
2/6/2019 11:29:58 AM 108.9 18.9
2/6/2019 11:29:59 AM 108.5 18.5
2/6/2019 11:30:00 AM 108.1 18.1
2/6/2019 11:30:01 AM 107.8 17.8
2/6/2019 11:30:02 AM 107.5 17.5
2/6/2019 11:30:03 AM 107.2 17.2
2/6/2019 11:30:04 AM 106.9 16.9
2/6/2019 11:30:05 AM 106.6 16.6
2/6/2019 11:30:06 AM 106.3 16.3
2/6/2019 11:30:07 AM 106.0 16.0
2/6/2019 11:30:08 AM 105.7 15.7
2/6/2019 11:30:09 AM 105.4 15.4
2/6/2019 11:30:10 AM 105.2 15.2
2/6/2019 11:30:11 AM 104.9 14.9
2/6/2019 11:30:12 AM 104.7 14.7
2/6/2019 11:30:13 AM 104.4 14.4
2/6/2019 11:30:14 AM 104.2 14.2
2/6/2019 11:30:15 AM 103.9 13.9
2/6/2019 11:30:16 AM 103.6 13.6
2/6/2019 11:30:17 AM 103.4 13.4
2/6/2019 11:30:18 AM 103.2 13.2
2/6/2019 11:30:19 AM 102.9 12.9
2/6/2019 11:30:20 AM 102.7 12.7
2/6/2019 11:30:21 AM 102.5 12.5
2/6/2019 11:30:22 AM 102.3 12.3
2/6/2019 11:30:23 AM 102.0 12.0
2/6/2019 11:30:24 AM 101.8 11.8
2/6/2019 11:30:25 AM 101.5 11.5
2/6/2019 11:30:26 AM 101.3 11.3
2/6/2019 11:30:27 AM 101.0 11.0
2/6/2019 11:30:28 AM 100.8 10.8
2/6/2019 11:30:29 AM 100.5 10.5
Page 240 of 452 August 2019
APPENDIX E44: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-3 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-3 Data Log
2/6/2019 11:30:30 AM 100.3 10.3
2/6/2019 11:30:31 AM 100.0 10.0
2/6/2019 11:30:32 AM 99.8 9.8
2/6/2019 11:30:33 AM 99.6 9.6
2/6/2019 11:30:34 AM 99.4 9.4
2/6/2019 11:30:35 AM 99.2 9.2
2/6/2019 11:30:36 AM 99.1 9.1
2/6/2019 11:30:37 AM 98.9 8.9
2/6/2019 11:30:38 AM 98.8 8.8
2/6/2019 11:30:39 AM 98.7 8.7
2/6/2019 11:30:40 AM 98.5 8.5
2/6/2019 11:30:41 AM 98.4 8.4
2/6/2019 11:30:42 AM 98.3 8.3
2/6/2019 11:30:43 AM 98.2 8.2
2/6/2019 11:30:44 AM 98.0 8.0
2/6/2019 11:30:45 AM 97.9 7.9
2/6/2019 11:30:46 AM 97.7 7.7
2/6/2019 11:30:47 AM 97.6 7.6
2/6/2019 11:30:48 AM 97.4 7.4
2/6/2019 11:30:49 AM 97.3 7.3
2/6/2019 11:30:50 AM 97.1 7.1
2/6/2019 11:30:51 AM 96.9 6.9
2/6/2019 11:30:52 AM 96.7 6.7
2/6/2019 11:30:53 AM 96.6 6.6
2/6/2019 11:30:54 AM 96.4 6.4
2/6/2019 11:30:55 AM 96.2 6.2
2/6/2019 11:30:56 AM 96.0 6.0
2/6/2019 11:30:57 AM 95.8 5.8
2/6/2019 11:30:58 AM 95.6 5.6
2/6/2019 11:30:59 AM 95.5 5.5
2/6/2019 11:31:00 AM 95.3 5.3
2/6/2019 11:31:01 AM 95.1 5.1
2/6/2019 11:31:02 AM 95.0 5.0
2/6/2019 11:31:03 AM 94.8 4.8
2/6/2019 11:31:04 AM 94.7 4.7
2/6/2019 11:31:05 AM 94.6 4.6
2/6/2019 11:31:06 AM 94.4 -
2/6/2019 11:31:07 AM 94.3 -
2/6/2019 11:31:08 AM 94.2 -
2/6/2019 11:31:09 AM 94.1 -
2/6/2019 11:31:10 AM 94.0 -
2/6/2019 11:31:11 AM 93.9 -
2/6/2019 11:31:12 AM 93.7 -
2/6/2019 11:31:13 AM 93.7 -
2/6/2019 11:31:14 AM 93.5 -
2/6/2019 11:31:15 AM 93.5 -
2/6/2019 11:31:16 AM 93.4 -
2/6/2019 11:31:17 AM 93.3 -
2/6/2019 11:31:18 AM 93.2 -
2/6/2019 11:31:19 AM 93.1 -
2/6/2019 11:31:20 AM 93.0 -
2/6/2019 11:31:21 AM 92.9 -
2/6/2019 11:31:22 AM 92.8 -
2/6/2019 11:31:23 AM 92.7 -
2/6/2019 11:31:24 AM 92.7 -
2/6/2019 11:31:25 AM 92.6 -
2/6/2019 11:31:26 AM 92.5 -
2/6/2019 11:31:27 AM 92.4 -
2/6/2019 11:31:28 AM 92.3 -
2/6/2019 11:31:29 AM 92.3 -
2/6/2019 11:31:30 AM 92.2 -
2/6/2019 11:31:31 AM 92.1 -
2/6/2019 11:31:32 AM 92.0 -
2/6/2019 11:31:33 AM 92.0 -
2/6/2019 11:31:34 AM 91.9 -
2/6/2019 11:31:35 AM 91.8 -
2/6/2019 11:31:36 AM 91.7 -
2/6/2019 11:31:37 AM 91.7 -
2/6/2019 11:31:38 AM 91.6 -
2/6/2019 11:31:39 AM 91.6 -
2/6/2019 11:31:40 AM 91.5 -
2/6/2019 11:31:41 AM 91.5 -
2/6/2019 11:31:42 AM 91.5 -
2/6/2019 11:31:43 AM 91.4 -
2/6/2019 11:31:44 AM 91.4 -
2/6/2019 11:31:45 AM 91.4 -
2/6/2019 11:31:46 AM 91.4 -
2/6/2019 11:31:47 AM 91.5 -
2/6/2019 11:31:48 AM 91.5 -
Page 241 of 452 August 2019
APPENDIX E44: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-3 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-3 Data Log
2/6/2019 11:31:49 AM 91.5 -
2/6/2019 11:31:50 AM 91.5 -
2/6/2019 11:31:51 AM 91.5 -
2/6/2019 11:31:52 AM 91.5 -
2/6/2019 11:31:53 AM 91.5 -
2/6/2019 11:31:54 AM 91.4 -
2/6/2019 11:31:55 AM 91.4 -
Page 242 of 452 August 2019
APPENDIX E44: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-3 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Location Time
Background
Stream EC
Background
Stream
Temperature
(µS/cms) (°C)
SEEP-B2-TEST-3 1046 86.2 11.5
SEEP-B2-TEST-3 1048 90.1 11.4
SEEP-B2-TEST-3 1048 91 11.4
SEEP-B2-TEST-3 1049 91.4 11.4
SEEP-B2-TEST-3 1050 90.7 11.4
89.9 (µS/cms)
89.9 (µS/cms)
90.0 (µS/cms)
92.4 (µS/cms)
Location EC Reading
(µS/cms)
SEEP-B2-TEST-3 39.9
SEEP-B2-TEST-3 198
SEEP-B2-TEST-3 1,550
SEEP-B2-TEST-3 13,391
SEEP-B2-TEST-3 106,519
q 300,000
K 1.0680
1.5
24.2
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Table E2 SEEP-B2 TEST-3 Stream Background Conductivity Data
(°C)
10 20.2
100 20.8
Average
Geo Mean
Average (pre-test)
(mg/L)
Table E3 SEEP-B2 TEST-3 YSI Salt Dilution Calibration Data
Calibration Concentration Temperature
Average (post-test)
20.6
10,000 21.1
100,000 21.2
1,000
L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow Measurement
Part 2: Constant-Rate Injection.” Streamline, Watershed Management Bulletin, vol.
8, no. 1, 2004, pp. 11–15.
Table E4 SEEP-B2 TEST-3 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Integral of Conductivity Data
Curve
SUM:Δt(ECt-
ECbkg)209,827.2 (s) . (µS/cms)
Calculated Flow Rate Q
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 243 of 452 August 2019
APPENDIX E45: SALT DILUTION GAUGING SUMMARY
Seep-B2-Test-1 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
5/22/2019 3:39:14 PM 165.5 -
5/22/2019 3:39:15 PM 165.5 -
5/22/2019 3:39:16 PM 165.5 -
5/22/2019 3:39:17 PM 165.5 -
5/22/2019 3:39:18 PM 165.5 -
5/22/2019 3:39:19 PM 165.6 -
5/22/2019 3:39:20 PM 165.6 -
5/22/2019 3:39:21 PM 165.6 -
5/22/2019 3:39:22 PM 165.7 -
5/22/2019 3:39:23 PM 165.8 -
5/22/2019 3:39:24 PM 165.8 -
5/22/2019 3:39:25 PM 165.9 -
5/22/2019 3:39:26 PM 166.0 -
5/22/2019 3:39:27 PM 166.1 -
5/22/2019 3:39:28 PM 166.1 -
5/22/2019 3:39:29 PM 166.2 -
5/22/2019 3:39:30 PM 166.3 -
5/22/2019 3:39:31 PM 166.4 -
5/22/2019 3:39:32 PM 166.4 -
5/22/2019 3:39:33 PM 166.5 -
5/22/2019 3:39:34 PM 166.5 -
5/22/2019 3:39:35 PM 166.6 -
5/22/2019 3:39:36 PM 166.6 -
5/22/2019 3:39:37 PM 166.6 -
5/22/2019 3:39:38 PM 166.6 -
5/22/2019 3:39:39 PM 166.6 -
5/22/2019 3:39:40 PM 166.6 -
5/22/2019 3:39:41 PM 166.6 -
5/22/2019 3:39:42 PM 166.6 -
5/22/2019 3:39:43 PM 166.6 -
5/22/2019 3:39:44 PM 166.6 -
5/22/2019 3:39:45 PM 166.6 -
5/22/2019 3:39:46 PM 166.6 -
5/22/2019 3:39:47 PM 166.6 -
5/22/2019 3:39:48 PM 166.6 -
5/22/2019 3:39:49 PM 166.6 -
5/22/2019 3:39:50 PM 166.6 -
5/22/2019 3:39:51 PM 166.6 -
5/22/2019 3:39:52 PM 166.6 -
5/22/2019 3:39:53 PM 166.7 -
5/22/2019 3:39:54 PM 166.7 -
5/22/2019 3:39:55 PM 166.7 -
5/22/2019 3:39:56 PM 166.8 -
5/22/2019 3:39:57 PM 167.4 -
5/22/2019 3:39:58 PM 222.9 56.6
5/22/2019 3:39:59 PM 342.0 175.7
5/22/2019 3:40:00 PM 533.0 366.7
5/22/2019 3:40:01 PM 727.5 561.2
5/22/2019 3:40:02 PM 1534.5 1368.2
5/22/2019 3:40:03 PM 2414.9 2248.6
5/22/2019 3:40:04 PM 2895.1 2728.8
5/22/2019 3:40:05 PM 3880.1 3713.8
5/22/2019 3:40:06 PM 5608.4 5442.1
5/22/2019 3:40:07 PM 6454.7 6288.4
5/22/2019 3:40:08 PM 7651.2 7484.9
5/22/2019 3:40:09 PM 9169.0 9002.7
5/22/2019 3:40:10 PM 9882.8 9716.5
5/22/2019 3:40:11 PM 10495.1 10328.8
5/22/2019 3:40:12 PM 11016.6 10850.3
5/22/2019 3:40:13 PM 11366.8 11200.5
5/22/2019 3:40:14 PM 11486.0 11319.7
5/22/2019 3:40:15 PM 11588.2 11421.9
5/22/2019 3:40:16 PM 11657.9 11491.6
5/22/2019 3:40:17 PM 11730.7 11564.4
5/22/2019 3:40:18 PM 11768.6 11602.3
5/22/2019 3:40:19 PM 11782.1 11615.8
5/22/2019 3:40:20 PM 11765.5 11599.2
5/22/2019 3:40:21 PM 11722.6 11556.3
5/22/2019 3:40:22 PM 10720.5 10554.2
5/22/2019 3:40:23 PM 10749.9 10583.6
Table G1 SEEP-B2 TEST-1 Data Log
Page 244 of 452 August 2019
APPENDIX E45: SALT DILUTION GAUGING SUMMARY
Seep-B2-Test-1 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table G1 SEEP-B2 TEST-1 Data Log
5/22/2019 3:40:24 PM 10123.3 9957.0
5/22/2019 3:40:25 PM 10059.9 9893.6
5/22/2019 3:40:26 PM 9913.3 9747.0
5/22/2019 3:40:27 PM 9091.4 8925.1
5/22/2019 3:40:28 PM 8594.0 8427.7
5/22/2019 3:40:29 PM 8454.7 8288.4
5/22/2019 3:40:30 PM 8357.6 8191.3
5/22/2019 3:40:31 PM 7552.8 7386.5
5/22/2019 3:40:32 PM 7348.8 7182.5
5/22/2019 3:40:33 PM 7177.2 7010.9
5/22/2019 3:40:34 PM 6624.5 6458.2
5/22/2019 3:40:35 PM 6464.6 6298.3
5/22/2019 3:40:36 PM 5983.3 5817.0
5/22/2019 3:40:37 PM 5768.7 5602.4
5/22/2019 3:40:38 PM 5430.0 5263.7
5/22/2019 3:40:39 PM 5297.8 5131.5
5/22/2019 3:40:40 PM 5224.6 5058.3
5/22/2019 3:40:41 PM 4821.9 4655.6
5/22/2019 3:40:42 PM 4707.5 4541.2
5/22/2019 3:40:43 PM 4521.8 4355.5
5/22/2019 3:40:44 PM 4340.7 4174.4
5/22/2019 3:40:45 PM 4308.8 4142.5
5/22/2019 3:40:46 PM 4222.9 4056.6
5/22/2019 3:40:47 PM 3855.0 3688.7
5/22/2019 3:40:48 PM 3741.2 3574.9
5/22/2019 3:40:49 PM 3520.1 3353.8
5/22/2019 3:40:50 PM 3489.1 3322.8
5/22/2019 3:40:51 PM 3426.0 3259.7
5/22/2019 3:40:52 PM 3358.7 3192.4
5/22/2019 3:40:53 PM 3136.3 2970.0
5/22/2019 3:40:54 PM 2992.9 2826.6
5/22/2019 3:40:55 PM 2907.1 2740.8
5/22/2019 3:40:56 PM 2799.4 2633.1
5/22/2019 3:40:57 PM 2757.7 2591.4
5/22/2019 3:40:58 PM 2725.2 2558.9
5/22/2019 3:40:59 PM 2688.2 2521.9
5/22/2019 3:41:00 PM 2479.5 2313.2
5/22/2019 3:41:01 PM 2407.5 2241.2
5/22/2019 3:41:02 PM 2283.6 2117.3
5/22/2019 3:41:03 PM 2244.9 2078.6
5/22/2019 3:41:04 PM 2210.8 2044.5
5/22/2019 3:41:05 PM 2178.6 2012.3
5/22/2019 3:41:06 PM 2020.0 1853.7
5/22/2019 3:41:07 PM 1946.8 1780.5
5/22/2019 3:41:08 PM 1889.9 1723.6
5/22/2019 3:41:09 PM 1842.1 1675.8
5/22/2019 3:41:10 PM 1827.5 1661.2
5/22/2019 3:41:11 PM 1811.5 1645.2
5/22/2019 3:41:12 PM 1795.1 1628.8
5/22/2019 3:41:13 PM 1773.2 1606.9
5/22/2019 3:41:14 PM 1609.0 1442.7
5/22/2019 3:41:15 PM 1564.0 1397.7
5/22/2019 3:41:16 PM 1500.4 1334.1
5/22/2019 3:41:17 PM 1486.9 1320.6
5/22/2019 3:41:18 PM 1459.1 1292.8
5/22/2019 3:41:19 PM 1438.8 1272.5
5/22/2019 3:41:20 PM 1421.1 1254.8
5/22/2019 3:41:21 PM 1405.7 1239.4
5/22/2019 3:41:22 PM 1289.3 1123.0
5/22/2019 3:41:23 PM 1257.3 1091.0
5/22/2019 3:41:24 PM 1231.3 1065.0
5/22/2019 3:41:25 PM 1228.0 1061.7
5/22/2019 3:41:26 PM 1216.5 1050.2
5/22/2019 3:41:27 PM 1194.0 1027.7
5/22/2019 3:41:28 PM 1115.7 949.4
5/22/2019 3:41:29 PM 1092.7 926.4
5/22/2019 3:41:30 PM 1078.6 912.3
5/22/2019 3:41:31 PM 1060.6 894.3
5/22/2019 3:41:32 PM 1056.1 889.8
5/22/2019 3:41:33 PM 1046.8 880.5
5/22/2019 3:41:34 PM 1032.5 866.2
5/22/2019 3:41:35 PM 1020.9 854.6
5/22/2019 3:41:36 PM 957.3 791.0
5/22/2019 3:41:37 PM 932.2 765.9
5/22/2019 3:41:38 PM 924.4 758.1
5/22/2019 3:41:39 PM 901.3 735.0
5/22/2019 3:41:40 PM 886.7 720.4
Page 245 of 452 August 2019
APPENDIX E45: SALT DILUTION GAUGING SUMMARY
Seep-B2-Test-1 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table G1 SEEP-B2 TEST-1 Data Log
5/22/2019 3:41:41 PM 877.9 711.6
5/22/2019 3:41:42 PM 869.5 703.2
5/22/2019 3:41:43 PM 862.5 696.2
5/22/2019 3:41:44 PM 854.4 688.1
5/22/2019 3:41:45 PM 796.7 630.4
5/22/2019 3:41:46 PM 779.0 612.7
5/22/2019 3:41:47 PM 761.9 595.6
5/22/2019 3:41:48 PM 756.4 590.1
5/22/2019 3:41:49 PM 753.3 587.0
5/22/2019 3:41:50 PM 751.9 585.6
5/22/2019 3:41:51 PM 746.2 579.9
5/22/2019 3:41:52 PM 738.7 572.4
5/22/2019 3:41:53 PM 733.2 566.9
5/22/2019 3:41:54 PM 680.9 514.6
5/22/2019 3:41:55 PM 670.4 504.1
5/22/2019 3:41:56 PM 655.2 488.9
5/22/2019 3:41:57 PM 655.3 489.0
5/22/2019 3:41:58 PM 653.7 487.4
5/22/2019 3:41:59 PM 648.1 481.8
5/22/2019 3:42:00 PM 643.7 477.4
5/22/2019 3:42:01 PM 484.2 317.9
5/22/2019 3:42:02 PM 593.5 427.2
5/22/2019 3:42:03 PM 596.9 430.6
5/22/2019 3:42:04 PM 589.5 423.2
5/22/2019 3:42:05 PM 586.0 419.7
5/22/2019 3:42:06 PM 580.9 414.6
5/22/2019 3:42:07 PM 574.6 408.3
5/22/2019 3:42:08 PM 570.3 404.0
5/22/2019 3:42:09 PM 566.5 400.2
5/22/2019 3:42:10 PM 563.0 396.7
5/22/2019 3:42:11 PM 559.3 393.0
5/22/2019 3:42:12 PM 556.3 390.0
5/22/2019 3:42:13 PM 552.9 386.6
5/22/2019 3:42:14 PM 550.1 383.8
5/22/2019 3:42:15 PM 547.3 381.0
5/22/2019 3:42:16 PM 544.5 378.2
5/22/2019 3:42:17 PM 542.0 375.7
5/22/2019 3:42:18 PM 536.4 370.1
5/22/2019 3:42:19 PM 530.9 364.6
5/22/2019 3:42:20 PM 524.8 358.5
5/22/2019 3:42:21 PM 519.5 353.2
5/22/2019 3:42:22 PM 513.5 347.2
5/22/2019 3:42:23 PM 508.5 342.2
5/22/2019 3:42:24 PM 456.6 290.3
5/22/2019 3:42:25 PM 453.1 286.8
5/22/2019 3:42:26 PM 452.1 285.8
5/22/2019 3:42:27 PM 450.8 284.5
5/22/2019 3:42:28 PM 447.0 280.7
5/22/2019 3:42:29 PM 444.9 278.6
5/22/2019 3:42:30 PM 443.2 276.9
5/22/2019 3:42:31 PM 441.7 275.4
5/22/2019 3:42:32 PM 439.9 273.6
5/22/2019 3:42:33 PM 438.5 272.2
5/22/2019 3:42:34 PM 437.0 270.7
5/22/2019 3:42:35 PM 435.2 268.9
5/22/2019 3:42:36 PM 433.5 267.2
5/22/2019 3:42:37 PM 431.6 265.3
5/22/2019 3:42:38 PM 429.9 263.6
5/22/2019 3:42:39 PM 428.1 261.8
5/22/2019 3:42:40 PM 425.4 259.1
5/22/2019 3:42:41 PM 421.9 255.6
5/22/2019 3:42:42 PM 418.7 252.4
5/22/2019 3:42:43 PM 414.6 248.3
5/22/2019 3:42:44 PM 410.9 244.6
5/22/2019 3:42:45 PM 406.8 240.5
5/22/2019 3:42:46 PM 403.1 236.8
5/22/2019 3:42:47 PM 399.0 232.7
5/22/2019 3:42:48 PM 395.7 229.4
5/22/2019 3:42:49 PM 392.0 225.7
5/22/2019 3:42:50 PM 388.7 222.4
5/22/2019 3:42:51 PM 384.8 218.5
5/22/2019 3:42:52 PM 381.6 215.3
5/22/2019 3:42:53 PM 378.0 211.7
5/22/2019 3:42:54 PM 374.3 208.0
5/22/2019 3:42:55 PM 371.3 205.0
5/22/2019 3:42:56 PM 368.4 202.1
5/22/2019 3:42:57 PM 365.9 199.6
5/22/2019 3:42:58 PM 363.2 196.9
5/22/2019 3:42:59 PM 360.6 194.3
Page 246 of 452 August 2019
APPENDIX E45: SALT DILUTION GAUGING SUMMARY
Seep-B2-Test-1 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table G1 SEEP-B2 TEST-1 Data Log
5/22/2019 3:43:00 PM 357.6 191.3
5/22/2019 3:43:01 PM 355.1 188.8
5/22/2019 3:43:02 PM 352.4 186.1
5/22/2019 3:43:03 PM 350.0 183.7
5/22/2019 3:43:04 PM 347.3 181.0
5/22/2019 3:43:05 PM 344.8 178.5
5/22/2019 3:43:06 PM 342.0 175.7
5/22/2019 3:43:07 PM 339.6 173.3
5/22/2019 3:43:08 PM 336.9 170.6
5/22/2019 3:43:09 PM 334.4 168.1
5/22/2019 3:43:10 PM 331.6 165.3
5/22/2019 3:43:11 PM 329.3 163.0
5/22/2019 3:43:12 PM 327.1 160.8
5/22/2019 3:43:13 PM 325.1 158.8
5/22/2019 3:43:14 PM 323.2 156.9
5/22/2019 3:43:15 PM 321.1 154.8
5/22/2019 3:43:16 PM 319.4 153.1
5/22/2019 3:43:17 PM 317.7 151.4
5/22/2019 3:43:18 PM 316.3 150.0
5/22/2019 3:43:19 PM 314.9 148.6
5/22/2019 3:43:20 PM 313.7 147.4
5/22/2019 3:43:21 PM 312.3 146.0
5/22/2019 3:43:22 PM 311.0 144.7
5/22/2019 3:43:23 PM 309.5 143.2
5/22/2019 3:43:24 PM 308.0 141.7
5/22/2019 3:43:25 PM 306.3 140.0
5/22/2019 3:43:26 PM 304.9 138.6
5/22/2019 3:43:27 PM 303.4 137.1
5/22/2019 3:43:28 PM 302.3 136.0
5/22/2019 3:43:29 PM 301.1 134.8
5/22/2019 3:43:30 PM 299.8 133.5
5/22/2019 3:43:31 PM 298.5 132.2
5/22/2019 3:43:32 PM 296.9 130.6
5/22/2019 3:43:33 PM 295.6 129.3
5/22/2019 3:43:34 PM 294.4 128.1
5/22/2019 3:43:35 PM 293.4 127.1
5/22/2019 3:43:36 PM 292.2 125.9
5/22/2019 3:43:37 PM 291.2 124.9
5/22/2019 3:43:38 PM 290.0 123.7
5/22/2019 3:43:39 PM 288.7 122.4
5/22/2019 3:43:40 PM 286.9 120.6
5/22/2019 3:43:41 PM 285.3 119.0
5/22/2019 3:43:42 PM 283.3 117.0
5/22/2019 3:43:43 PM 281.8 115.5
5/22/2019 3:43:44 PM 280.1 113.8
5/22/2019 3:43:45 PM 278.7 112.4
5/22/2019 3:43:46 PM 277.0 110.7
5/22/2019 3:43:47 PM 275.6 109.3
5/22/2019 3:43:48 PM 274.3 108.0
5/22/2019 3:43:49 PM 273.0 106.7
5/22/2019 3:43:50 PM 272.0 105.7
5/22/2019 3:43:51 PM 270.8 104.5
5/22/2019 3:43:52 PM 270.0 103.7
5/22/2019 3:43:53 PM 269.0 102.7
5/22/2019 3:43:54 PM 268.2 101.9
5/22/2019 3:43:55 PM 267.3 101.0
5/22/2019 3:43:56 PM 266.5 100.2
5/22/2019 3:43:57 PM 265.6 99.3
5/22/2019 3:43:58 PM 265.0 98.7
5/22/2019 3:43:59 PM 264.2 97.9
5/22/2019 3:44:00 PM 263.6 97.3
5/22/2019 3:44:01 PM 262.8 96.5
5/22/2019 3:44:02 PM 262.0 95.7
5/22/2019 3:44:03 PM 261.1 94.8
5/22/2019 3:44:04 PM 260.4 94.1
5/22/2019 3:44:05 PM 259.4 93.1
5/22/2019 3:44:06 PM 258.7 92.4
5/22/2019 3:44:07 PM 257.9 91.6
5/22/2019 3:44:08 PM 257.2 90.9
5/22/2019 3:44:09 PM 256.6 90.3
5/22/2019 3:44:10 PM 255.9 89.6
5/22/2019 3:44:11 PM 255.2 88.9
5/22/2019 3:44:12 PM 254.5 88.2
5/22/2019 3:44:13 PM 253.8 87.5
5/22/2019 3:44:14 PM 253.0 86.7
5/22/2019 3:44:15 PM 252.3 86.0
5/22/2019 3:44:16 PM 251.6 85.3
5/22/2019 3:44:17 PM 251.0 84.7
5/22/2019 3:44:18 PM 250.4 84.1
Page 247 of 452 August 2019
APPENDIX E45: SALT DILUTION GAUGING SUMMARY
Seep-B2-Test-1 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table G1 SEEP-B2 TEST-1 Data Log
5/22/2019 3:44:19 PM 250.0 83.7
5/22/2019 3:44:20 PM 249.3 83.0
5/22/2019 3:44:21 PM 248.8 82.5
5/22/2019 3:44:22 PM 248.2 81.9
5/22/2019 3:44:23 PM 247.6 81.3
5/22/2019 3:44:24 PM 246.9 80.6
5/22/2019 3:44:25 PM 246.2 79.9
5/22/2019 3:44:26 PM 245.4 79.1
5/22/2019 3:44:27 PM 244.6 78.3
5/22/2019 3:44:28 PM 243.9 77.6
5/22/2019 3:44:29 PM 243.2 76.9
5/22/2019 3:44:30 PM 242.5 76.2
5/22/2019 3:44:31 PM 241.7 75.4
5/22/2019 3:44:32 PM 241.1 74.8
5/22/2019 3:44:33 PM 240.4 74.1
5/22/2019 3:44:34 PM 239.9 73.6
5/22/2019 3:44:35 PM 239.3 73.0
5/22/2019 3:44:36 PM 238.8 72.5
5/22/2019 3:44:37 PM 238.4 72.1
5/22/2019 3:44:38 PM 238.1 71.8
5/22/2019 3:44:39 PM 237.9 71.6
5/22/2019 3:44:40 PM 237.7 71.4
5/22/2019 3:44:41 PM 237.7 71.4
5/22/2019 3:44:42 PM 237.7 71.4
5/22/2019 3:44:43 PM 237.8 71.5
5/22/2019 3:44:44 PM 238.0 71.7
5/22/2019 3:44:45 PM 238.2 71.9
5/22/2019 3:44:46 PM 238.4 72.1
5/22/2019 3:44:47 PM 238.7 72.4
5/22/2019 3:44:48 PM 239.1 72.8
5/22/2019 3:44:49 PM 239.5 73.2
5/22/2019 3:44:50 PM 240.0 73.7
5/22/2019 3:44:51 PM 240.4 74.1
5/22/2019 3:44:52 PM 240.7 74.4
5/22/2019 3:44:53 PM 241.0 74.7
5/22/2019 3:44:54 PM 241.2 74.9
5/22/2019 3:44:55 PM 241.3 75.0
5/22/2019 3:44:56 PM 241.3 75.0
5/22/2019 3:44:57 PM 241.2 74.9
5/22/2019 3:44:58 PM 241.1 74.8
5/22/2019 3:44:59 PM 241.0 74.7
5/22/2019 3:45:00 PM 240.7 74.4
5/22/2019 3:45:01 PM 240.5 74.2
5/22/2019 3:45:02 PM 240.3 74.0
5/22/2019 3:45:03 PM 240.0 73.7
5/22/2019 3:45:04 PM 239.7 73.4
5/22/2019 3:45:05 PM 239.4 73.1
5/22/2019 3:45:06 PM 239.0 72.7
5/22/2019 3:45:07 PM 238.7 72.4
5/22/2019 3:45:08 PM 238.4 72.1
5/22/2019 3:45:09 PM 238.2 71.9
5/22/2019 3:45:10 PM 238.0 71.7
5/22/2019 3:45:11 PM 237.7 71.4
5/22/2019 3:45:12 PM 237.5 71.2
5/22/2019 3:45:13 PM 237.2 70.9
5/22/2019 3:45:14 PM 236.9 70.6
5/22/2019 3:45:15 PM 236.5 70.2
5/22/2019 3:45:16 PM 236.2 69.9
5/22/2019 3:45:17 PM 235.8 69.5
5/22/2019 3:45:18 PM 235.4 69.1
5/22/2019 3:45:19 PM 235.1 68.8
5/22/2019 3:45:20 PM 234.9 68.6
5/22/2019 3:45:21 PM 234.6 68.3
5/22/2019 3:45:22 PM 234.2 67.9
5/22/2019 3:45:23 PM 233.8 67.5
5/22/2019 3:45:24 PM 233.5 67.2
5/22/2019 3:45:25 PM 233.2 66.9
5/22/2019 3:45:26 PM 232.8 66.5
5/22/2019 3:45:27 PM 232.5 66.2
5/22/2019 3:45:28 PM 232.1 65.8
5/22/2019 3:45:29 PM 231.8 65.5
5/22/2019 3:45:30 PM 231.5 65.2
5/22/2019 3:45:31 PM 231.2 64.9
5/22/2019 3:45:32 PM 230.9 64.6
5/22/2019 3:45:33 PM 230.5 64.2
5/22/2019 3:45:34 PM 230.1 63.8
5/22/2019 3:45:35 PM 229.8 63.5
5/22/2019 3:45:36 PM 229.5 63.2
5/22/2019 3:45:37 PM 229.1 62.8
Page 248 of 452 August 2019
APPENDIX E45: SALT DILUTION GAUGING SUMMARY
Seep-B2-Test-1 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table G1 SEEP-B2 TEST-1 Data Log
5/22/2019 3:45:38 PM 228.7 62.4
5/22/2019 3:45:39 PM 228.4 62.1
5/22/2019 3:45:40 PM 228.0 61.7
5/22/2019 3:45:41 PM 227.6 61.3
5/22/2019 3:45:42 PM 227.3 61.0
5/22/2019 3:45:43 PM 227.0 60.7
5/22/2019 3:45:44 PM 226.7 60.4
5/22/2019 3:45:45 PM 226.3 60.0
5/22/2019 3:45:46 PM 226.1 59.8
5/22/2019 3:45:47 PM 225.8 59.5
5/22/2019 3:45:48 PM 225.5 59.2
5/22/2019 3:45:49 PM 225.3 59.0
5/22/2019 3:45:50 PM 225.1 58.8
5/22/2019 3:45:51 PM 224.9 58.6
5/22/2019 3:45:52 PM 224.7 58.4
5/22/2019 3:45:53 PM 224.5 58.2
5/22/2019 3:45:54 PM 224.3 58.0
5/22/2019 3:45:55 PM 224.1 57.8
5/22/2019 3:45:56 PM 223.9 57.6
5/22/2019 3:45:57 PM 223.8 57.5
5/22/2019 3:45:58 PM 223.6 57.3
5/22/2019 3:45:59 PM 223.3 57.0
5/22/2019 3:46:00 PM 223.1 56.8
5/22/2019 3:46:01 PM 222.9 56.6
5/22/2019 3:46:02 PM 222.7 56.4
5/22/2019 3:46:03 PM 222.3 56.0
5/22/2019 3:46:04 PM 222.0 55.7
5/22/2019 3:46:05 PM 221.8 55.5
5/22/2019 3:46:06 PM 221.4 55.1
5/22/2019 3:46:07 PM 221.0 54.7
5/22/2019 3:46:08 PM 220.6 54.3
5/22/2019 3:46:09 PM 220.1 53.8
5/22/2019 3:46:10 PM 219.6 53.3
5/22/2019 3:46:11 PM 219.1 52.8
5/22/2019 3:46:12 PM 218.5 52.2
5/22/2019 3:46:13 PM 218.0 51.7
5/22/2019 3:46:14 PM 217.4 51.1
5/22/2019 3:46:15 PM 216.8 50.5
5/22/2019 3:46:16 PM 216.2 49.9
5/22/2019 3:46:17 PM 215.6 49.3
5/22/2019 3:46:18 PM 215.1 48.8
5/22/2019 3:46:19 PM 214.5 48.2
5/22/2019 3:46:20 PM 213.9 47.6
5/22/2019 3:46:21 PM 213.3 47.0
5/22/2019 3:46:22 PM 212.7 46.4
5/22/2019 3:46:23 PM 212.2 45.9
5/22/2019 3:46:24 PM 211.8 45.5
5/22/2019 3:46:25 PM 211.3 45.0
5/22/2019 3:46:26 PM 210.8 44.5
5/22/2019 3:46:27 PM 210.4 44.1
5/22/2019 3:46:28 PM 210.0 43.7
5/22/2019 3:46:29 PM 209.6 43.3
5/22/2019 3:46:30 PM 209.2 42.9
5/22/2019 3:46:31 PM 208.9 42.6
5/22/2019 3:46:32 PM 208.6 42.3
5/22/2019 3:46:33 PM 208.2 41.9
5/22/2019 3:46:34 PM 207.9 41.6
5/22/2019 3:46:35 PM 207.6 41.3
5/22/2019 3:46:36 PM 207.3 41.0
5/22/2019 3:46:37 PM 207.1 40.8
5/22/2019 3:46:38 PM 206.8 40.5
5/22/2019 3:46:39 PM 206.6 40.3
5/22/2019 3:46:40 PM 206.3 40.0
5/22/2019 3:46:41 PM 206.1 39.8
5/22/2019 3:46:42 PM 205.7 39.4
5/22/2019 3:46:43 PM 205.5 39.2
5/22/2019 3:46:44 PM 205.1 38.8
5/22/2019 3:46:45 PM 205.0 38.7
5/22/2019 3:46:46 PM 204.7 38.4
5/22/2019 3:46:47 PM 204.4 38.1
5/22/2019 3:46:48 PM 204.3 38.0
5/22/2019 3:46:49 PM 204.1 37.8
5/22/2019 3:46:50 PM 203.8 37.5
5/22/2019 3:46:51 PM 203.6 37.3
5/22/2019 3:46:52 PM 203.4 37.1
5/22/2019 3:46:53 PM 203.2 36.9
5/22/2019 3:46:54 PM 203.1 36.8
5/22/2019 3:46:55 PM 202.9 36.6
5/22/2019 3:46:56 PM 202.8 36.5
Page 249 of 452 August 2019
APPENDIX E45: SALT DILUTION GAUGING SUMMARY
Seep-B2-Test-1 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table G1 SEEP-B2 TEST-1 Data Log
5/22/2019 3:46:57 PM 202.6 36.3
5/22/2019 3:46:58 PM 202.5 36.2
5/22/2019 3:46:59 PM 202.4 36.1
5/22/2019 3:47:00 PM 202.3 36.0
5/22/2019 3:47:01 PM 202.1 35.8
5/22/2019 3:47:02 PM 202.0 35.7
5/22/2019 3:47:03 PM 201.8 35.5
5/22/2019 3:47:04 PM 201.6 35.3
5/22/2019 3:47:05 PM 201.5 35.2
5/22/2019 3:47:06 PM 201.4 35.1
5/22/2019 3:47:07 PM 201.3 35.0
5/22/2019 3:47:08 PM 201.2 34.9
5/22/2019 3:47:09 PM 201.1 34.8
5/22/2019 3:47:10 PM 201.0 34.7
5/22/2019 3:47:11 PM 200.9 34.6
5/22/2019 3:47:12 PM 200.8 34.5
5/22/2019 3:47:13 PM 200.7 34.4
5/22/2019 3:47:14 PM 200.6 34.3
5/22/2019 3:47:15 PM 200.6 34.3
5/22/2019 3:47:16 PM 200.5 34.2
5/22/2019 3:47:17 PM 200.4 34.1
5/22/2019 3:47:18 PM 200.4 34.1
5/22/2019 3:47:19 PM 200.3 34.0
5/22/2019 3:47:20 PM 200.2 33.9
5/22/2019 3:47:21 PM 200.2 33.9
5/22/2019 3:47:22 PM 200.1 33.8
5/22/2019 3:47:23 PM 200.1 33.8
5/22/2019 3:47:24 PM 200.0 33.7
5/22/2019 3:47:25 PM 199.9 33.6
5/22/2019 3:47:26 PM 199.8 33.5
5/22/2019 3:47:27 PM 199.7 33.4
5/22/2019 3:47:28 PM 199.6 33.3
5/22/2019 3:47:29 PM 199.5 33.2
5/22/2019 3:47:30 PM 199.4 33.1
5/22/2019 3:47:31 PM 199.3 33.0
5/22/2019 3:47:32 PM 199.2 32.9
5/22/2019 3:47:33 PM 199.1 32.8
5/22/2019 3:47:34 PM 199.0 32.7
5/22/2019 3:47:35 PM 198.8 32.5
5/22/2019 3:47:36 PM 198.6 32.3
5/22/2019 3:47:37 PM 198.5 32.2
5/22/2019 3:47:38 PM 198.4 32.1
5/22/2019 3:47:39 PM 198.2 31.9
5/22/2019 3:47:40 PM 198.1 31.8
5/22/2019 3:47:41 PM 198.0 31.7
5/22/2019 3:47:42 PM 197.8 31.5
5/22/2019 3:47:43 PM 197.7 31.4
5/22/2019 3:47:44 PM 197.5 31.2
5/22/2019 3:47:45 PM 197.3 31.0
5/22/2019 3:47:46 PM 197.1 30.8
5/22/2019 3:47:47 PM 196.9 30.6
5/22/2019 3:47:48 PM 196.8 30.5
5/22/2019 3:47:49 PM 196.6 30.3
5/22/2019 3:47:50 PM 196.4 30.1
5/22/2019 3:47:51 PM 196.2 29.9
5/22/2019 3:47:52 PM 196.0 29.7
5/22/2019 3:47:53 PM 195.8 29.5
5/22/2019 3:47:54 PM 195.6 29.3
5/22/2019 3:47:55 PM 195.5 29.2
5/22/2019 3:47:56 PM 195.3 29.0
5/22/2019 3:47:57 PM 195.1 28.8
5/22/2019 3:47:58 PM 194.9 28.6
5/22/2019 3:47:59 PM 194.7 28.4
5/22/2019 3:48:00 PM 194.5 28.2
5/22/2019 3:48:01 PM 194.3 28.0
5/22/2019 3:48:02 PM 194.1 27.8
5/22/2019 3:48:03 PM 193.9 27.6
5/22/2019 3:48:04 PM 193.7 27.4
5/22/2019 3:48:05 PM 193.6 27.3
5/22/2019 3:48:06 PM 193.3 27.0
5/22/2019 3:48:07 PM 193.2 26.9
5/22/2019 3:48:08 PM 193.1 26.8
5/22/2019 3:48:09 PM 193.0 26.7
5/22/2019 3:48:10 PM 192.9 26.6
5/22/2019 3:48:11 PM 192.8 26.5
5/22/2019 3:48:12 PM 192.8 26.5
5/22/2019 3:48:13 PM 192.7 26.4
5/22/2019 3:48:14 PM 192.6 26.3
5/22/2019 3:48:15 PM 192.5 26.2
Page 250 of 452 August 2019
APPENDIX E45: SALT DILUTION GAUGING SUMMARY
Seep-B2-Test-1 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table G1 SEEP-B2 TEST-1 Data Log
5/22/2019 3:48:16 PM 192.4 26.1
5/22/2019 3:48:17 PM 192.2 25.9
5/22/2019 3:48:18 PM 192.1 25.8
5/22/2019 3:48:19 PM 191.9 25.6
5/22/2019 3:48:20 PM 191.7 25.4
5/22/2019 3:48:21 PM 191.5 25.2
5/22/2019 3:48:22 PM 191.2 24.9
5/22/2019 3:48:23 PM 191.0 24.7
5/22/2019 3:48:24 PM 190.8 24.5
5/22/2019 3:48:25 PM 190.6 24.3
5/22/2019 3:48:26 PM 190.4 24.1
5/22/2019 3:48:27 PM 190.3 24.0
5/22/2019 3:48:28 PM 190.1 23.8
5/22/2019 3:48:29 PM 190.0 23.7
5/22/2019 3:48:30 PM 189.9 23.6
5/22/2019 3:48:31 PM 189.8 23.5
5/22/2019 3:48:32 PM 189.7 23.4
5/22/2019 3:48:33 PM 189.6 23.3
5/22/2019 3:48:34 PM 189.6 23.3
5/22/2019 3:48:35 PM 189.5 23.2
5/22/2019 3:48:36 PM 189.4 23.1
5/22/2019 3:48:37 PM 189.4 23.1
5/22/2019 3:48:38 PM 189.3 23.0
5/22/2019 3:48:39 PM 189.3 23.0
5/22/2019 3:48:40 PM 189.2 22.9
5/22/2019 3:48:41 PM 189.2 22.9
5/22/2019 3:48:42 PM 189.1 22.8
5/22/2019 3:48:43 PM 189.1 22.8
5/22/2019 3:48:44 PM 189.0 22.7
5/22/2019 3:48:45 PM 189.0 22.7
5/22/2019 3:48:46 PM 189.0 22.7
5/22/2019 3:48:47 PM 189.0 22.7
5/22/2019 3:48:48 PM 189.0 22.7
5/22/2019 3:48:49 PM 188.9 22.6
5/22/2019 3:48:50 PM 188.9 22.6
5/22/2019 3:48:51 PM 188.9 22.6
5/22/2019 3:48:52 PM 188.9 22.6
5/22/2019 3:48:53 PM 189.0 22.7
5/22/2019 3:48:54 PM 189.0 22.7
5/22/2019 3:48:55 PM 189.0 22.7
5/22/2019 3:48:56 PM 189.0 22.7
5/22/2019 3:48:57 PM 189.0 22.7
5/22/2019 3:48:58 PM 189.0 22.7
5/22/2019 3:48:59 PM 189.0 22.7
5/22/2019 3:49:00 PM 188.9 22.6
5/22/2019 3:49:01 PM 188.9 22.6
5/22/2019 3:49:02 PM 188.9 22.6
5/22/2019 3:49:03 PM 188.8 22.5
5/22/2019 3:49:04 PM 188.8 22.5
5/22/2019 3:49:05 PM 188.7 22.4
5/22/2019 3:49:06 PM 188.6 22.3
5/22/2019 3:49:07 PM 188.6 22.3
5/22/2019 3:49:08 PM 188.5 22.2
5/22/2019 3:49:09 PM 188.4 22.1
5/22/2019 3:49:10 PM 188.4 22.1
5/22/2019 3:49:11 PM 188.3 22.0
5/22/2019 3:49:12 PM 188.3 22.0
5/22/2019 3:49:13 PM 188.2 21.9
5/22/2019 3:49:14 PM 188.1 21.8
5/22/2019 3:49:15 PM 188.0 21.7
5/22/2019 3:49:16 PM 187.9 21.6
5/22/2019 3:49:17 PM 187.8 21.5
5/22/2019 3:49:18 PM 187.7 21.4
5/22/2019 3:49:19 PM 187.6 21.3
5/22/2019 3:49:20 PM 187.5 21.2
5/22/2019 3:49:21 PM 187.4 21.1
5/22/2019 3:49:22 PM 187.3 21.0
5/22/2019 3:49:23 PM 187.2 20.9
5/22/2019 3:49:24 PM 187.0 20.7
5/22/2019 3:49:25 PM 186.9 20.6
5/22/2019 3:49:26 PM 186.8 20.5
5/22/2019 3:49:27 PM 186.7 20.4
5/22/2019 3:49:28 PM 186.6 20.3
5/22/2019 3:49:29 PM 186.5 20.2
5/22/2019 3:49:30 PM 186.4 20.1
5/22/2019 3:49:31 PM 186.4 20.1
5/22/2019 3:49:32 PM 186.3 20.0
5/22/2019 3:49:33 PM 186.2 19.9
5/22/2019 3:49:34 PM 186.1 19.8
Page 251 of 452 August 2019
APPENDIX E45: SALT DILUTION GAUGING SUMMARY
Seep-B2-Test-1 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table G1 SEEP-B2 TEST-1 Data Log
5/22/2019 3:49:35 PM 186.0 19.7
5/22/2019 3:49:36 PM 185.9 19.6
5/22/2019 3:49:37 PM 185.8 19.5
5/22/2019 3:49:38 PM 185.7 19.4
5/22/2019 3:49:39 PM 185.7 19.4
5/22/2019 3:49:40 PM 185.6 19.3
5/22/2019 3:49:41 PM 185.5 19.2
5/22/2019 3:49:42 PM 185.4 19.1
5/22/2019 3:49:43 PM 185.4 19.1
5/22/2019 3:49:44 PM 185.3 19.0
5/22/2019 3:49:45 PM 185.3 19.0
5/22/2019 3:49:46 PM 185.2 18.9
5/22/2019 3:49:47 PM 185.1 18.8
5/22/2019 3:49:48 PM 185.0 18.7
5/22/2019 3:49:49 PM 185.0 18.7
5/22/2019 3:49:50 PM 184.9 18.6
5/22/2019 3:49:51 PM 184.8 18.5
5/22/2019 3:49:52 PM 184.7 18.4
5/22/2019 3:49:53 PM 184.6 18.3
5/22/2019 3:49:54 PM 184.5 18.2
5/22/2019 3:49:55 PM 184.4 18.1
5/22/2019 3:49:56 PM 184.3 18.0
5/22/2019 3:49:57 PM 184.2 17.9
5/22/2019 3:49:58 PM 184.1 17.8
5/22/2019 3:49:59 PM 184.0 17.7
5/22/2019 3:50:00 PM 183.9 17.6
5/22/2019 3:50:01 PM 183.8 17.5
5/22/2019 3:50:02 PM 183.7 17.4
5/22/2019 3:50:03 PM 183.6 17.3
5/22/2019 3:50:04 PM 183.5 17.2
5/22/2019 3:50:05 PM 183.4 17.1
5/22/2019 3:50:06 PM 183.4 17.1
5/22/2019 3:50:07 PM 183.3 17.0
5/22/2019 3:50:08 PM 183.2 16.9
5/22/2019 3:50:09 PM 183.2 16.9
5/22/2019 3:50:10 PM 183.2 16.9
5/22/2019 3:50:11 PM 183.1 16.8
5/22/2019 3:50:12 PM 183.1 16.8
5/22/2019 3:50:13 PM 183.0 16.7
5/22/2019 3:50:14 PM 183.0 16.7
5/22/2019 3:50:15 PM 182.9 16.6
5/22/2019 3:50:16 PM 182.9 16.6
5/22/2019 3:50:17 PM 182.9 16.6
5/22/2019 3:50:18 PM 182.9 16.6
5/22/2019 3:50:19 PM 182.8 16.5
5/22/2019 3:50:20 PM 182.8 16.5
5/22/2019 3:50:21 PM 182.8 16.5
5/22/2019 3:50:22 PM 182.8 16.5
5/22/2019 3:50:23 PM 182.8 16.5
5/22/2019 3:50:24 PM 182.7 16.4
5/22/2019 3:50:25 PM 182.7 16.4
5/22/2019 3:50:26 PM 182.8 16.5
5/22/2019 3:50:27 PM 182.9 16.6
5/22/2019 3:50:28 PM 182.9 16.6
5/22/2019 3:50:29 PM 183.0 16.7
5/22/2019 3:50:30 PM 183.0 16.7
5/22/2019 3:50:31 PM 183.0 16.7
5/22/2019 3:50:32 PM 183.0 16.7
5/22/2019 3:50:33 PM 183.0 16.7
5/22/2019 3:50:34 PM 183.0 16.7
5/22/2019 3:50:35 PM 183.0 16.7
5/22/2019 3:50:36 PM 183.0 16.7
5/22/2019 3:50:37 PM 183.0 16.7
5/22/2019 3:50:38 PM 182.9 16.6
5/22/2019 3:50:39 PM 182.8 16.5
5/22/2019 3:50:40 PM 182.7 16.4
5/22/2019 3:50:41 PM 182.6 16.3
5/22/2019 3:50:42 PM 182.5 16.2
5/22/2019 3:50:43 PM 182.5 16.2
5/22/2019 3:50:44 PM 182.4 16.1
5/22/2019 3:50:45 PM 182.3 16.0
5/22/2019 3:50:46 PM 182.3 16.0
5/22/2019 3:50:47 PM 182.2 15.9
5/22/2019 3:50:48 PM 182.2 15.9
5/22/2019 3:50:49 PM 182.1 15.8
5/22/2019 3:50:50 PM 182.1 15.8
5/22/2019 3:50:51 PM 182.0 15.7
5/22/2019 3:50:52 PM 182.0 15.7
5/22/2019 3:50:53 PM 181.9 15.6
Page 252 of 452 August 2019
APPENDIX E45: SALT DILUTION GAUGING SUMMARY
Seep-B2-Test-1 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table G1 SEEP-B2 TEST-1 Data Log
5/22/2019 3:50:54 PM 181.9 15.6
5/22/2019 3:50:55 PM 181.8 15.5
5/22/2019 3:50:56 PM 181.8 15.5
5/22/2019 3:50:57 PM 181.7 15.4
5/22/2019 3:50:58 PM 181.7 15.4
5/22/2019 3:50:59 PM 181.7 15.4
5/22/2019 3:51:00 PM 181.6 15.3
5/22/2019 3:51:01 PM 181.5 15.2
5/22/2019 3:51:02 PM 181.5 15.2
5/22/2019 3:51:03 PM 181.5 15.2
5/22/2019 3:51:04 PM 181.4 15.1
5/22/2019 3:51:05 PM 181.4 15.1
5/22/2019 3:51:06 PM 181.3 15.0
5/22/2019 3:51:07 PM 181.3 15.0
5/22/2019 3:51:08 PM 181.2 14.9
5/22/2019 3:51:09 PM 181.2 14.9
5/22/2019 3:51:10 PM 181.1 14.8
5/22/2019 3:51:11 PM 181.0 14.7
5/22/2019 3:51:12 PM 180.9 14.6
5/22/2019 3:51:13 PM 180.9 14.6
5/22/2019 3:51:14 PM 180.8 14.5
5/22/2019 3:51:15 PM 180.7 14.4
5/22/2019 3:51:16 PM 180.7 14.4
5/22/2019 3:51:17 PM 180.6 14.3
5/22/2019 3:51:18 PM 180.5 14.2
5/22/2019 3:51:19 PM 180.5 14.2
5/22/2019 3:51:20 PM 180.5 14.2
5/22/2019 3:51:21 PM 180.4 14.1
5/22/2019 3:51:22 PM 180.4 14.1
5/22/2019 3:51:23 PM 180.4 14.1
5/22/2019 3:51:24 PM 180.4 14.1
5/22/2019 3:51:25 PM 180.4 14.1
5/22/2019 3:51:26 PM 180.4 14.1
5/22/2019 3:51:27 PM 180.4 14.1
5/22/2019 3:51:28 PM 180.4 14.1
5/22/2019 3:51:29 PM 180.4 14.1
5/22/2019 3:51:30 PM 180.4 14.1
5/22/2019 3:51:31 PM 180.4 14.1
5/22/2019 3:51:32 PM 180.4 14.1
5/22/2019 3:51:33 PM 180.4 14.1
5/22/2019 3:51:34 PM 180.3 14.0
5/22/2019 3:51:35 PM 180.3 14.0
5/22/2019 3:51:36 PM 180.2 13.9
5/22/2019 3:51:37 PM 180.2 13.9
5/22/2019 3:51:38 PM 180.1 13.8
5/22/2019 3:51:39 PM 180.0 13.7
5/22/2019 3:51:40 PM 180.0 13.7
5/22/2019 3:51:41 PM 179.9 13.6
5/22/2019 3:51:42 PM 179.9 13.6
5/22/2019 3:51:43 PM 179.9 13.6
5/22/2019 3:51:44 PM 179.8 13.5
5/22/2019 3:51:45 PM 179.8 13.5
5/22/2019 3:51:46 PM 179.8 13.5
5/22/2019 3:51:47 PM 179.7 13.4
5/22/2019 3:51:48 PM 179.7 13.4
5/22/2019 3:51:49 PM 179.7 13.4
5/22/2019 3:51:50 PM 179.7 13.4
5/22/2019 3:51:51 PM 179.7 13.4
5/22/2019 3:51:52 PM 179.7 13.4
5/22/2019 3:51:53 PM 179.7 13.4
5/22/2019 3:51:54 PM 179.6 13.3
5/22/2019 3:51:55 PM 179.6 13.3
5/22/2019 3:51:56 PM 179.6 13.3
5/22/2019 3:51:57 PM 179.5 13.2
5/22/2019 3:51:58 PM 179.5 13.2
5/22/2019 3:51:59 PM 179.5 13.2
5/22/2019 3:52:00 PM 179.4 13.1
5/22/2019 3:52:01 PM 179.4 13.1
5/22/2019 3:52:02 PM 179.3 13.0
5/22/2019 3:52:03 PM 179.3 13.0
5/22/2019 3:52:04 PM 179.3 13.0
5/22/2019 3:52:05 PM 179.2 12.9
5/22/2019 3:52:06 PM 179.2 12.9
5/22/2019 3:52:07 PM 179.2 12.9
5/22/2019 3:52:08 PM 179.2 12.9
5/22/2019 3:52:09 PM 179.2 12.9
5/22/2019 3:52:10 PM 179.1 12.8
5/22/2019 3:52:11 PM 179.1 12.8
5/22/2019 3:52:12 PM 179.1 12.8
Page 253 of 452 August 2019
APPENDIX E45: SALT DILUTION GAUGING SUMMARY
Seep-B2-Test-1 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table G1 SEEP-B2 TEST-1 Data Log
5/22/2019 3:52:13 PM 149.3 -17.0
5/22/2019 3:52:14 PM 133.7 -32.6
5/22/2019 3:52:15 PM 68.7 -97.6
5/22/2019 3:52:16 PM 50.6 -115.7
5/22/2019 3:52:17 PM 60.6 -105.7
5/22/2019 3:52:18 PM 168.6 2.3
5/22/2019 3:52:19 PM 177.7 11.4
5/22/2019 3:52:20 PM 178.5 12.2
5/22/2019 3:52:21 PM 178.7 12.4
5/22/2019 3:52:22 PM 178.6 12.3
5/22/2019 3:52:23 PM 178.6 12.3
5/22/2019 3:52:24 PM 178.6 12.3
5/22/2019 3:52:25 PM 178.6 12.3
5/22/2019 3:52:26 PM 178.6 12.3
5/22/2019 3:52:27 PM 178.5 12.2
5/22/2019 3:52:28 PM 178.5 12.2
5/22/2019 3:52:29 PM 178.5 12.2
5/22/2019 3:52:30 PM 178.5 12.2
5/22/2019 3:52:31 PM 178.5 12.2
5/22/2019 3:52:32 PM 178.5 12.2
5/22/2019 3:52:33 PM 178.5 12.2
5/22/2019 3:52:34 PM 178.5 12.2
5/22/2019 3:52:35 PM 178.4 12.1
5/22/2019 3:52:36 PM 178.4 12.1
5/22/2019 3:52:37 PM 178.4 12.1
5/22/2019 3:52:38 PM 178.4 12.1
5/22/2019 3:52:39 PM 178.3 12.0
5/22/2019 3:52:40 PM 178.3 12.0
5/22/2019 3:52:41 PM 178.3 12.0
5/22/2019 3:52:42 PM 178.3 12.0
5/22/2019 3:52:43 PM 178.2 11.9
5/22/2019 3:52:44 PM 178.2 11.9
5/22/2019 3:52:45 PM 178.2 11.9
5/22/2019 3:52:46 PM 178.1 11.8
5/22/2019 3:52:47 PM 178.1 11.8
5/22/2019 3:52:48 PM 178.1 11.8
5/22/2019 3:52:49 PM 178.1 11.8
5/22/2019 3:52:50 PM 178.0 11.7
5/22/2019 3:52:51 PM 178.0 11.7
5/22/2019 3:52:52 PM 178.0 11.7
5/22/2019 3:52:53 PM 178.0 11.7
5/22/2019 3:52:54 PM 178.0 11.7
5/22/2019 3:52:55 PM 178.0 11.7
5/22/2019 3:52:56 PM 178.0 11.7
5/22/2019 3:52:57 PM 178.0 11.7
5/22/2019 3:52:58 PM 178.0 11.7
5/22/2019 3:52:59 PM 178.0 11.7
5/22/2019 3:53:00 PM 177.9 11.6
5/22/2019 3:53:01 PM 177.9 11.6
5/22/2019 3:53:02 PM 177.9 11.6
5/22/2019 3:53:03 PM 177.9 11.6
5/22/2019 3:53:04 PM 177.9 11.6
5/22/2019 3:53:05 PM 177.8 11.5
5/22/2019 3:53:06 PM 177.8 11.5
5/22/2019 3:53:07 PM 177.8 11.5
5/22/2019 3:53:08 PM 177.8 11.5
5/22/2019 3:53:09 PM 177.7 11.4
5/22/2019 3:53:10 PM 177.7 11.4
Page 254 of 452 August 2019
APPENDIX E45: SALT DILUTION GAUGING SUMMARY
Seep-B2-Test-1 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-B2-TEST-1 1528
SEEP-B2-TEST-1 1532
SEEP-B2-TEST-1 1533
SEEP-B2-TEST-1 1534
Location EC Reading
(µS/cms)
SEEP-B2-TEST-1 29.9
SEEP-B2-TEST-1 167
SEEP-B2-TEST-1 426
SEEP-B2-TEST-1 3,329
SEEP-B2-TEST-1 15,499
SEEP-B2-TEST-1 127,509
q 300,100
K 1.2780
0.8
12.3
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
NR Not recorded
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Calibration
Concentration
(mg/L)
NR
NR
NR
NR
(°C)
Temperature
Table G3 SEEP-B2 TEST-1 YSI Salt Dilution Calibration Data
(µS/cms)(°C)
Table G2 SEEP-B2 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
151.5 NR
165.2 NR
167.0 NR
Average (pre-test)59.1 (µS/cms)
166.4 NR
Average 162.5 (µS/cms)
Geometric Mean 162.4 (µS/cms)
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
100,000 NR
Table G4 SEEP-B2 TEST-1 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)494,782.2 (s) . (µS/cms)
Average (post-test)7.0 (µS/cms)
Calculated Flow Rate Q
L/s
GPM
1,000
10,000 NR
1
10
100
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 255 of 452 August 2019
APPENDIX E46: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
5/22/2019 3:55:04 PM 176.6 -
5/22/2019 3:55:05 PM 176.6 -
5/22/2019 3:55:06 PM 176.6 -
5/22/2019 3:55:07 PM 176.6 -
5/22/2019 3:55:08 PM 176.6 -
5/22/2019 3:55:09 PM 176.5 -
5/22/2019 3:55:10 PM 176.5 -
5/22/2019 3:55:11 PM 176.5 -
5/22/2019 3:55:12 PM 176.4 -
5/22/2019 3:55:13 PM 176.4 -
5/22/2019 3:55:14 PM 176.4 -
5/22/2019 3:55:15 PM 176.4 -
5/22/2019 3:55:16 PM 176.3 -
5/22/2019 3:55:17 PM 176.3 -
5/22/2019 3:55:18 PM 176.2 -
5/22/2019 3:55:19 PM 176.2 -
5/22/2019 3:55:20 PM 176.2 -
5/22/2019 3:55:21 PM 176.1 -
5/22/2019 3:55:22 PM 176.1 -
5/22/2019 3:55:23 PM 176.1 -
5/22/2019 3:55:24 PM 176.0 -
5/22/2019 3:55:25 PM 176.0 -
5/22/2019 3:55:26 PM 176.0 -
5/22/2019 3:55:27 PM 175.9 -
5/22/2019 3:55:28 PM 175.9 -
5/22/2019 3:55:29 PM 175.9 -
5/22/2019 3:55:30 PM 175.9 -
5/22/2019 3:55:31 PM 175.8 -
5/22/2019 3:55:32 PM 175.8 -
5/22/2019 3:55:33 PM 175.8 -
5/22/2019 3:55:34 PM 175.8 -
5/22/2019 3:55:35 PM 175.8 -
5/22/2019 3:55:36 PM 175.8 -
5/22/2019 3:55:37 PM 175.7 -
5/22/2019 3:55:38 PM 175.7 -
5/22/2019 3:55:39 PM 175.7 -
5/22/2019 3:55:40 PM 175.7 -
5/22/2019 3:55:41 PM 175.7 -
5/22/2019 3:55:42 PM 175.7 -
5/22/2019 3:55:43 PM 176.0 -
5/22/2019 3:55:44 PM 177.3 -
5/22/2019 3:55:45 PM 236.7 60.6
5/22/2019 3:55:46 PM 250.5 74.4
5/22/2019 3:55:47 PM 341.8 165.7
5/22/2019 3:55:48 PM 371.2 195.1
5/22/2019 3:55:49 PM 556.1 380.0
5/22/2019 3:55:50 PM 723.7 547.6
5/22/2019 3:55:51 PM 1256.5 1080.4
5/22/2019 3:55:52 PM 1733.7 1557.6
5/22/2019 3:55:53 PM 3865.0 3688.9
5/22/2019 3:55:54 PM 4587.4 4411.3
5/22/2019 3:55:55 PM 5372.3 5196.2
5/22/2019 3:55:56 PM 6928.6 6752.5
5/22/2019 3:55:57 PM 7502.4 7326.3
5/22/2019 3:55:58 PM 8592.2 8416.1
5/22/2019 3:55:59 PM 9078.2 8902.1
5/22/2019 3:56:00 PM 9277.1 9101.0
5/22/2019 3:56:01 PM 10020.1 9844.0
5/22/2019 3:56:02 PM 10562.5 10386.4
5/22/2019 3:56:03 PM 10874.5 10698.4
5/22/2019 3:56:04 PM 10916.7 10740.6
5/22/2019 3:56:05 PM 10981.1 10805.0
5/22/2019 3:56:06 PM 10989.8 10813.7
5/22/2019 3:56:07 PM 10993.3 10817.2
5/22/2019 3:56:08 PM 10992.1 10816.0
5/22/2019 3:56:09 PM 10979.2 10803.1
5/22/2019 3:56:10 PM 10956.9 10780.8
5/22/2019 3:56:11 PM 10912.5 10736.4
5/22/2019 3:56:12 PM 10868.6 10692.5
5/22/2019 3:56:13 PM 10184.0 10007.9
Table E1 SEEP-B2 TEST-2 Data Log
Page 256 of 452 August 2019
APPENDIX E46: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
5/22/2019 3:56:14 PM 9657.0 9480.9
5/22/2019 3:56:15 PM 9499.4 9323.3
5/22/2019 3:56:16 PM 9403.6 9227.5
5/22/2019 3:56:17 PM 9294.9 9118.8
5/22/2019 3:56:18 PM 9179.1 9003.0
5/22/2019 3:56:19 PM 9117.7 8941.6
5/22/2019 3:56:20 PM 9011.1 8835.0
5/22/2019 3:56:21 PM 8958.6 8782.5
5/22/2019 3:56:22 PM 8166.2 7990.1
5/22/2019 3:56:23 PM 7593.3 7417.2
5/22/2019 3:56:24 PM 6996.6 6820.5
5/22/2019 3:56:25 PM 6872.9 6696.8
5/22/2019 3:56:26 PM 6805.0 6628.9
5/22/2019 3:56:27 PM 6669.0 6492.9
5/22/2019 3:56:28 PM 6584.0 6407.9
5/22/2019 3:56:29 PM 6518.4 6342.3
5/22/2019 3:56:30 PM 5840.2 5664.1
5/22/2019 3:56:31 PM 5607.9 5431.8
5/22/2019 3:56:32 PM 5471.4 5295.3
5/22/2019 3:56:33 PM 5354.4 5178.3
5/22/2019 3:56:34 PM 5233.2 5057.1
5/22/2019 3:56:35 PM 4900.8 4724.7
5/22/2019 3:56:36 PM 4750.4 4574.3
5/22/2019 3:56:37 PM 4582.0 4405.9
5/22/2019 3:56:38 PM 4552.9 4376.8
5/22/2019 3:56:39 PM 4357.8 4181.7
5/22/2019 3:56:40 PM 4262.1 4086.0
5/22/2019 3:56:41 PM 4211.6 4035.5
5/22/2019 3:56:42 PM 3818.6 3642.5
5/22/2019 3:56:43 PM 3553.7 3377.6
5/22/2019 3:56:44 PM 3446.9 3270.8
5/22/2019 3:56:45 PM 3381.8 3205.7
5/22/2019 3:56:46 PM 3336.6 3160.5
5/22/2019 3:56:47 PM 3288.2 3112.1
5/22/2019 3:56:48 PM 3250.0 3073.9
5/22/2019 3:56:49 PM 2966.8 2790.7
5/22/2019 3:56:50 PM 2945.6 2769.5
5/22/2019 3:56:51 PM 2920.0 2743.9
5/22/2019 3:56:52 PM 2917.6 2741.5
5/22/2019 3:56:53 PM 2880.6 2704.5
5/22/2019 3:56:54 PM 2837.7 2661.6
5/22/2019 3:56:55 PM 2556.3 2380.2
5/22/2019 3:56:56 PM 2463.3 2287.2
5/22/2019 3:56:57 PM 2445.9 2269.8
5/22/2019 3:56:58 PM 2428.3 2252.2
5/22/2019 3:56:59 PM 2408.8 2232.7
5/22/2019 3:57:00 PM 2399.2 2223.1
5/22/2019 3:57:01 PM 2376.7 2200.6
5/22/2019 3:57:02 PM 2146.1 1970.0
5/22/2019 3:57:03 PM 2107.5 1931.4
5/22/2019 3:57:04 PM 2086.4 1910.3
5/22/2019 3:57:05 PM 2078.7 1902.6
5/22/2019 3:57:06 PM 2024.8 1848.7
5/22/2019 3:57:07 PM 2000.3 1824.2
5/22/2019 3:57:08 PM 1975.8 1799.7
5/22/2019 3:57:09 PM 1849.3 1673.2
5/22/2019 3:57:10 PM 1782.5 1606.4
5/22/2019 3:57:11 PM 1719.3 1543.2
5/22/2019 3:57:12 PM 1695.8 1519.7
5/22/2019 3:57:13 PM 1668.1 1492.0
5/22/2019 3:57:14 PM 1641.7 1465.6
5/22/2019 3:57:15 PM 1625.4 1449.3
5/22/2019 3:57:16 PM 1615.5 1439.4
5/22/2019 3:57:17 PM 1604.8 1428.7
5/22/2019 3:57:18 PM 1597.2 1421.1
5/22/2019 3:57:19 PM 1588.1 1412.0
5/22/2019 3:57:20 PM 1464.0 1287.9
5/22/2019 3:57:21 PM 1447.3 1271.2
5/22/2019 3:57:22 PM 1437.8 1261.7
5/22/2019 3:57:23 PM 1433.8 1257.7
5/22/2019 3:57:24 PM 1423.7 1247.6
5/22/2019 3:57:25 PM 1408.5 1232.4
5/22/2019 3:57:26 PM 1318.9 1142.8
5/22/2019 3:57:27 PM 1302.3 1126.2
5/22/2019 3:57:28 PM 1277.6 1101.5
5/22/2019 3:57:29 PM 1251.0 1074.9
5/22/2019 3:57:30 PM 1248.5 1072.4
Page 257 of 452 August 2019
APPENDIX E46: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
5/22/2019 3:57:31 PM 1240.8 1064.7
5/22/2019 3:57:32 PM 1225.6 1049.5
5/22/2019 3:57:33 PM 1214.9 1038.8
5/22/2019 3:57:34 PM 1205.7 1029.6
5/22/2019 3:57:35 PM 1124.7 948.6
5/22/2019 3:57:36 PM 1109.0 932.9
5/22/2019 3:57:37 PM 1104.2 928.1
5/22/2019 3:57:38 PM 1092.4 916.3
5/22/2019 3:57:39 PM 1069.2 893.1
5/22/2019 3:57:40 PM 1054.3 878.2
5/22/2019 3:57:41 PM 1046.9 870.8
5/22/2019 3:57:42 PM 1038.2 862.1
5/22/2019 3:57:43 PM 1031.6 855.5
5/22/2019 3:57:44 PM 954.4 778.3
5/22/2019 3:57:45 PM 923.0 746.9
5/22/2019 3:57:46 PM 909.3 733.2
5/22/2019 3:57:47 PM 893.6 717.5
5/22/2019 3:57:48 PM 870.7 694.6
5/22/2019 3:57:49 PM 852.6 676.5
5/22/2019 3:57:50 PM 844.1 668.0
5/22/2019 3:57:51 PM 836.7 660.6
5/22/2019 3:57:52 PM 831.8 655.7
5/22/2019 3:57:53 PM 825.8 649.7
5/22/2019 3:57:54 PM 820.9 644.8
5/22/2019 3:57:55 PM 816.4 640.3
5/22/2019 3:57:56 PM 813.1 637.0
5/22/2019 3:57:57 PM 731.1 555.0
5/22/2019 3:57:58 PM 694.6 518.5
5/22/2019 3:57:59 PM 674.0 497.9
5/22/2019 3:58:00 PM 672.2 496.1
5/22/2019 3:58:01 PM 666.7 490.6
5/22/2019 3:58:02 PM 656.1 480.0
5/22/2019 3:58:03 PM 650.3 474.2
5/22/2019 3:58:04 PM 581.3 405.2
5/22/2019 3:58:05 PM 584.1 408.0
5/22/2019 3:58:06 PM 575.2 399.1
5/22/2019 3:58:07 PM 573.9 397.8
5/22/2019 3:58:08 PM 570.9 394.8
5/22/2019 3:58:09 PM 567.0 390.9
5/22/2019 3:58:10 PM 562.7 386.6
5/22/2019 3:58:11 PM 559.5 383.4
5/22/2019 3:58:12 PM 556.4 380.3
5/22/2019 3:58:13 PM 554.1 378.0
5/22/2019 3:58:14 PM 551.7 375.6
5/22/2019 3:58:15 PM 549.0 372.9
5/22/2019 3:58:16 PM 545.3 369.2
5/22/2019 3:58:17 PM 542.0 365.9
5/22/2019 3:58:18 PM 538.4 362.3
5/22/2019 3:58:19 PM 494.9 318.8
5/22/2019 3:58:20 PM 487.6 311.5
5/22/2019 3:58:21 PM 484.1 308.0
5/22/2019 3:58:22 PM 481.4 305.3
5/22/2019 3:58:23 PM 478.0 301.9
5/22/2019 3:58:24 PM 473.8 297.7
5/22/2019 3:58:25 PM 470.8 294.7
5/22/2019 3:58:26 PM 468.0 291.9
5/22/2019 3:58:27 PM 464.8 288.7
5/22/2019 3:58:28 PM 462.3 286.2
5/22/2019 3:58:29 PM 459.4 283.3
5/22/2019 3:58:30 PM 457.0 280.9
5/22/2019 3:58:31 PM 454.2 278.1
5/22/2019 3:58:32 PM 452.0 275.9
5/22/2019 3:58:33 PM 449.8 273.7
5/22/2019 3:58:34 PM 448.1 272.0
5/22/2019 3:58:35 PM 444.4 268.3
5/22/2019 3:58:36 PM 440.7 264.6
5/22/2019 3:58:37 PM 436.8 260.7
5/22/2019 3:58:38 PM 433.7 257.6
5/22/2019 3:58:39 PM 430.7 254.6
5/22/2019 3:58:40 PM 428.4 252.3
5/22/2019 3:58:41 PM 426.1 250.0
5/22/2019 3:58:42 PM 424.3 248.2
5/22/2019 3:58:43 PM 423.2 247.1
5/22/2019 3:58:44 PM 422.2 246.1
5/22/2019 3:58:45 PM 421.4 245.3
5/22/2019 3:58:46 PM 420.7 244.6
5/22/2019 3:58:47 PM 420.1 244.0
5/22/2019 3:58:48 PM 419.6 243.5
5/22/2019 3:58:49 PM 419.2 243.1
Page 258 of 452 August 2019
APPENDIX E46: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
5/22/2019 3:58:50 PM 418.6 242.5
5/22/2019 3:58:51 PM 418.0 241.9
5/22/2019 3:58:52 PM 417.2 241.1
5/22/2019 3:58:53 PM 416.4 240.3
5/22/2019 3:58:54 PM 415.3 239.2
5/22/2019 3:58:55 PM 414.1 238.0
5/22/2019 3:58:56 PM 412.6 236.5
5/22/2019 3:58:57 PM 411.2 235.1
5/22/2019 3:58:58 PM 409.3 233.2
5/22/2019 3:58:59 PM 407.4 231.3
5/22/2019 3:59:00 PM 405.0 228.9
5/22/2019 3:59:01 PM 403.1 227.0
5/22/2019 3:59:02 PM 400.2 224.1
5/22/2019 3:59:03 PM 397.6 221.5
5/22/2019 3:59:04 PM 395.3 219.2
5/22/2019 3:59:05 PM 392.5 216.4
5/22/2019 3:59:06 PM 390.1 214.0
5/22/2019 3:59:07 PM 387.1 211.0
5/22/2019 3:59:08 PM 384.4 208.3
5/22/2019 3:59:09 PM 381.1 205.0
5/22/2019 3:59:10 PM 378.3 202.2
5/22/2019 3:59:11 PM 375.3 199.2
5/22/2019 3:59:12 PM 372.6 196.5
5/22/2019 3:59:13 PM 369.8 193.7
5/22/2019 3:59:14 PM 367.3 191.2
5/22/2019 3:59:15 PM 364.4 188.3
5/22/2019 3:59:16 PM 361.7 185.6
5/22/2019 3:59:17 PM 358.3 182.2
5/22/2019 3:59:18 PM 356.5 180.4
5/22/2019 3:59:19 PM 353.9 177.8
5/22/2019 3:59:20 PM 351.3 175.2
5/22/2019 3:59:21 PM 349.7 173.6
5/22/2019 3:59:22 PM 347.3 171.2
5/22/2019 3:59:23 PM 345.6 169.5
5/22/2019 3:59:24 PM 343.3 167.2
5/22/2019 3:59:25 PM 341.3 165.2
5/22/2019 3:59:26 PM 339.0 162.9
5/22/2019 3:59:27 PM 336.6 160.5
5/22/2019 3:59:28 PM 335.1 159.0
5/22/2019 3:59:29 PM 332.9 156.8
5/22/2019 3:59:30 PM 331.5 155.4
5/22/2019 3:59:31 PM 329.2 153.1
5/22/2019 3:59:32 PM 327.7 151.6
5/22/2019 3:59:33 PM 325.4 149.3
5/22/2019 3:59:34 PM 323.8 147.7
5/22/2019 3:59:35 PM 322.2 146.1
5/22/2019 3:59:36 PM 320.1 144.0
5/22/2019 3:59:37 PM 319.0 142.9
5/22/2019 3:59:38 PM 317.2 141.1
5/22/2019 3:59:39 PM 315.9 139.8
5/22/2019 3:59:40 PM 314.8 138.7
5/22/2019 3:59:41 PM 313.2 137.1
5/22/2019 3:59:42 PM 312.4 136.3
5/22/2019 3:59:43 PM 310.7 134.6
5/22/2019 3:59:44 PM 309.6 133.5
5/22/2019 3:59:45 PM 308.2 132.1
5/22/2019 3:59:46 PM 307.1 131.0
5/22/2019 3:59:47 PM 305.8 129.7
5/22/2019 3:59:48 PM 304.5 128.4
5/22/2019 3:59:49 PM 303.6 127.5
5/22/2019 3:59:50 PM 302.3 126.2
5/22/2019 3:59:51 PM 301.4 125.3
5/22/2019 3:59:52 PM 300.2 124.1
5/22/2019 3:59:53 PM 298.4 122.3
5/22/2019 3:59:54 PM 297.5 121.4
5/22/2019 3:59:55 PM 296.0 119.9
5/22/2019 3:59:56 PM 294.4 118.3
5/22/2019 3:59:57 PM 293.3 117.2
5/22/2019 3:59:58 PM 292.3 116.2
5/22/2019 3:59:59 PM 291.2 115.1
5/22/2019 4:00:00 PM 289.6 113.5
5/22/2019 4:00:01 PM 288.8 112.7
5/22/2019 4:00:02 PM 287.2 111.1
5/22/2019 4:00:03 PM 286.0 109.9
5/22/2019 4:00:04 PM 284.8 108.7
5/22/2019 4:00:05 PM 283.8 107.7
5/22/2019 4:00:06 PM 282.8 106.7
5/22/2019 4:00:07 PM 282.0 105.9
5/22/2019 4:00:08 PM 281.0 104.9
Page 259 of 452 August 2019
APPENDIX E46: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
5/22/2019 4:00:09 PM 280.1 104.0
5/22/2019 4:00:10 PM 279.0 102.9
5/22/2019 4:00:11 PM 278.1 102.0
5/22/2019 4:00:12 PM 277.4 101.3
5/22/2019 4:00:13 PM 276.3 100.2
5/22/2019 4:00:14 PM 275.5 99.4
5/22/2019 4:00:15 PM 274.3 98.2
5/22/2019 4:00:16 PM 273.5 97.4
5/22/2019 4:00:17 PM 272.2 96.1
5/22/2019 4:00:18 PM 271.6 95.5
5/22/2019 4:00:19 PM 270.7 94.6
5/22/2019 4:00:20 PM 269.7 93.6
5/22/2019 4:00:21 PM 269.1 93.0
5/22/2019 4:00:22 PM 268.3 92.2
5/22/2019 4:00:23 PM 267.7 91.6
5/22/2019 4:00:24 PM 266.8 90.7
5/22/2019 4:00:25 PM 266.1 90.0
5/22/2019 4:00:26 PM 265.6 89.5
5/22/2019 4:00:27 PM 264.8 88.7
5/22/2019 4:00:28 PM 264.3 88.2
5/22/2019 4:00:29 PM 263.8 87.7
5/22/2019 4:00:30 PM 263.2 87.1
5/22/2019 4:00:31 PM 262.9 86.8
5/22/2019 4:00:32 PM 262.4 86.3
5/22/2019 4:00:33 PM 262.0 85.9
5/22/2019 4:00:34 PM 261.7 85.6
5/22/2019 4:00:35 PM 261.2 85.1
5/22/2019 4:00:36 PM 261.0 84.9
5/22/2019 4:00:37 PM 260.6 84.5
5/22/2019 4:00:38 PM 260.3 84.2
5/22/2019 4:00:39 PM 259.9 83.8
5/22/2019 4:00:40 PM 259.5 83.4
5/22/2019 4:00:41 PM 259.3 83.2
5/22/2019 4:00:42 PM 258.7 82.6
5/22/2019 4:00:43 PM 258.5 82.4
5/22/2019 4:00:44 PM 258.0 81.9
5/22/2019 4:00:45 PM 257.6 81.5
5/22/2019 4:00:46 PM 257.2 81.1
5/22/2019 4:00:47 PM 256.8 80.7
5/22/2019 4:00:48 PM 256.5 80.4
5/22/2019 4:00:49 PM 256.0 79.9
5/22/2019 4:00:50 PM 255.5 79.4
5/22/2019 4:00:51 PM 254.9 78.8
5/22/2019 4:00:52 PM 254.3 78.2
5/22/2019 4:00:53 PM 253.8 77.7
5/22/2019 4:00:54 PM 253.1 77.0
5/22/2019 4:00:55 PM 252.6 76.5
5/22/2019 4:00:56 PM 252.1 76.0
5/22/2019 4:00:57 PM 251.4 75.3
5/22/2019 4:00:58 PM 251.1 75.0
5/22/2019 4:00:59 PM 250.6 74.5
5/22/2019 4:01:00 PM 250.2 74.1
5/22/2019 4:01:01 PM 250.0 73.9
5/22/2019 4:01:02 PM 249.8 73.7
5/22/2019 4:01:03 PM 249.7 73.6
5/22/2019 4:01:04 PM 249.7 73.6
5/22/2019 4:01:05 PM 249.7 73.6
5/22/2019 4:01:06 PM 249.8 73.7
5/22/2019 4:01:07 PM 249.9 73.8
5/22/2019 4:01:08 PM 250.1 74.0
5/22/2019 4:01:09 PM 250.1 74.0
5/22/2019 4:01:10 PM 250.2 74.1
5/22/2019 4:01:11 PM 250.1 74.0
5/22/2019 4:01:12 PM 250.0 73.9
5/22/2019 4:01:13 PM 249.8 73.7
5/22/2019 4:01:14 PM 249.4 73.3
5/22/2019 4:01:15 PM 249.1 73.0
5/22/2019 4:01:16 PM 248.5 72.4
5/22/2019 4:01:17 PM 248.0 71.9
5/22/2019 4:01:18 PM 247.5 71.4
5/22/2019 4:01:19 PM 246.9 70.8
5/22/2019 4:01:20 PM 246.2 70.1
5/22/2019 4:01:21 PM 245.7 69.6
5/22/2019 4:01:22 PM 244.5 68.4
5/22/2019 4:01:23 PM 243.6 67.5
5/22/2019 4:01:24 PM 242.9 66.8
5/22/2019 4:01:25 PM 241.6 65.5
5/22/2019 4:01:26 PM 240.9 64.8
5/22/2019 4:01:27 PM 239.8 63.7
Page 260 of 452 August 2019
APPENDIX E46: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
5/22/2019 4:01:28 PM 238.8 62.7
5/22/2019 4:01:29 PM 238.2 62.1
5/22/2019 4:01:30 PM 236.8 60.7
5/22/2019 4:01:31 PM 235.8 59.7
5/22/2019 4:01:32 PM 235.0 58.9
5/22/2019 4:01:33 PM 233.9 57.8
5/22/2019 4:01:34 PM 233.0 56.9
5/22/2019 4:01:35 PM 232.4 56.3
5/22/2019 4:01:36 PM 231.6 55.5
5/22/2019 4:01:37 PM 230.9 54.8
5/22/2019 4:01:38 PM 230.5 54.4
5/22/2019 4:01:39 PM 229.6 53.5
5/22/2019 4:01:40 PM 229.0 52.9
5/22/2019 4:01:41 PM 228.5 52.4
5/22/2019 4:01:42 PM 227.9 51.8
5/22/2019 4:01:43 PM 227.5 51.4
5/22/2019 4:01:44 PM 226.9 50.8
5/22/2019 4:01:45 PM 226.5 50.4
5/22/2019 4:01:46 PM 226.0 49.9
5/22/2019 4:01:47 PM 225.2 49.1
5/22/2019 4:01:48 PM 224.9 48.8
5/22/2019 4:01:49 PM 224.3 48.2
5/22/2019 4:01:50 PM 223.7 47.6
5/22/2019 4:01:51 PM 223.1 47.0
5/22/2019 4:01:52 PM 222.8 46.7
5/22/2019 4:01:53 PM 222.2 46.1
5/22/2019 4:01:54 PM 221.9 45.8
5/22/2019 4:01:55 PM 221.5 45.4
5/22/2019 4:01:56 PM 221.0 44.9
5/22/2019 4:01:57 PM 220.7 44.6
5/22/2019 4:01:58 PM 220.4 44.3
5/22/2019 4:01:59 PM 220.1 44.0
5/22/2019 4:02:00 PM 219.8 43.7
5/22/2019 4:02:01 PM 219.6 43.5
5/22/2019 4:02:02 PM 219.3 43.2
5/22/2019 4:02:03 PM 219.2 43.1
5/22/2019 4:02:04 PM 218.9 42.8
5/22/2019 4:02:05 PM 218.7 42.6
5/22/2019 4:02:06 PM 218.5 42.4
5/22/2019 4:02:07 PM 218.3 42.2
5/22/2019 4:02:08 PM 218.1 42.0
5/22/2019 4:02:09 PM 217.9 41.8
5/22/2019 4:02:10 PM 217.8 41.7
5/22/2019 4:02:11 PM 217.5 41.4
5/22/2019 4:02:12 PM 217.3 41.2
5/22/2019 4:02:13 PM 217.0 40.9
5/22/2019 4:02:14 PM 216.7 40.6
5/22/2019 4:02:15 PM 216.4 40.3
5/22/2019 4:02:16 PM 216.2 40.1
5/22/2019 4:02:17 PM 215.9 39.8
5/22/2019 4:02:18 PM 215.7 39.6
5/22/2019 4:02:19 PM 215.3 39.2
5/22/2019 4:02:20 PM 215.0 38.9
5/22/2019 4:02:21 PM 214.8 38.7
5/22/2019 4:02:22 PM 214.4 38.3
5/22/2019 4:02:23 PM 214.2 38.1
5/22/2019 4:02:24 PM 213.9 37.8
5/22/2019 4:02:25 PM 213.7 37.6
5/22/2019 4:02:26 PM 213.4 37.3
5/22/2019 4:02:27 PM 213.1 37.0
5/22/2019 4:02:28 PM 212.8 36.7
5/22/2019 4:02:29 PM 212.6 36.5
5/22/2019 4:02:30 PM 212.3 36.2
5/22/2019 4:02:31 PM 212.1 36.0
5/22/2019 4:02:32 PM 211.9 35.8
5/22/2019 4:02:33 PM 211.7 35.6
5/22/2019 4:02:34 PM 211.4 35.3
5/22/2019 4:02:35 PM 211.1 35.0
5/22/2019 4:02:36 PM 210.9 34.8
5/22/2019 4:02:37 PM 210.6 34.5
5/22/2019 4:02:38 PM 210.4 34.3
5/22/2019 4:02:39 PM 210.3 34.2
5/22/2019 4:02:40 PM 210.1 34.0
5/22/2019 4:02:41 PM 209.9 33.8
5/22/2019 4:02:42 PM 209.7 33.6
5/22/2019 4:02:43 PM 209.4 33.3
5/22/2019 4:02:44 PM 209.2 33.1
5/22/2019 4:02:45 PM 209.0 32.9
5/22/2019 4:02:46 PM 208.7 32.6
Page 261 of 452 August 2019
APPENDIX E46: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
5/22/2019 4:02:47 PM 208.5 32.4
5/22/2019 4:02:48 PM 208.3 32.2
5/22/2019 4:02:49 PM 208.0 31.9
5/22/2019 4:02:50 PM 207.8 31.7
5/22/2019 4:02:51 PM 207.6 31.5
5/22/2019 4:02:52 PM 207.4 31.3
5/22/2019 4:02:53 PM 207.1 31.0
5/22/2019 4:02:54 PM 207.0 30.9
5/22/2019 4:02:55 PM 206.8 30.7
5/22/2019 4:02:56 PM 206.6 30.5
5/22/2019 4:02:57 PM 206.4 30.3
5/22/2019 4:02:58 PM 206.2 30.1
5/22/2019 4:02:59 PM 206.0 29.9
5/22/2019 4:03:00 PM 205.8 29.7
5/22/2019 4:03:01 PM 205.5 29.4
5/22/2019 4:03:02 PM 205.3 29.2
5/22/2019 4:03:03 PM 205.1 29.0
5/22/2019 4:03:04 PM 204.9 28.8
5/22/2019 4:03:05 PM 204.7 28.6
5/22/2019 4:03:06 PM 204.5 28.4
5/22/2019 4:03:07 PM 204.2 28.1
5/22/2019 4:03:08 PM 204.0 27.9
5/22/2019 4:03:09 PM 203.9 27.8
5/22/2019 4:03:10 PM 203.6 27.5
5/22/2019 4:03:11 PM 203.5 27.4
5/22/2019 4:03:12 PM 203.4 27.3
5/22/2019 4:03:13 PM 203.2 27.1
5/22/2019 4:03:14 PM 203.1 27.0
5/22/2019 4:03:15 PM 203.0 26.9
5/22/2019 4:03:16 PM 202.9 26.8
5/22/2019 4:03:17 PM 202.8 26.7
5/22/2019 4:03:18 PM 202.7 26.6
5/22/2019 4:03:19 PM 202.7 26.6
5/22/2019 4:03:20 PM 202.5 26.4
5/22/2019 4:03:21 PM 202.5 26.4
5/22/2019 4:03:22 PM 202.4 26.3
5/22/2019 4:03:23 PM 202.2 26.1
5/22/2019 4:03:24 PM 202.1 26.0
5/22/2019 4:03:25 PM 202.1 26.0
5/22/2019 4:03:26 PM 201.9 25.8
5/22/2019 4:03:27 PM 201.9 25.8
5/22/2019 4:03:28 PM 201.8 25.7
5/22/2019 4:03:29 PM 201.7 25.6
5/22/2019 4:03:30 PM 201.6 25.5
5/22/2019 4:03:31 PM 201.5 25.4
5/22/2019 4:03:32 PM 201.5 25.4
5/22/2019 4:03:33 PM 201.4 25.3
5/22/2019 4:03:34 PM 201.3 25.2
5/22/2019 4:03:35 PM 201.3 25.2
5/22/2019 4:03:36 PM 201.2 25.1
5/22/2019 4:03:37 PM 201.2 25.1
5/22/2019 4:03:38 PM 201.1 25.0
5/22/2019 4:03:39 PM 201.0 24.9
5/22/2019 4:03:40 PM 200.9 24.8
5/22/2019 4:03:41 PM 200.9 24.8
5/22/2019 4:03:42 PM 200.7 24.6
5/22/2019 4:03:43 PM 200.6 24.5
5/22/2019 4:03:44 PM 200.6 24.5
5/22/2019 4:03:45 PM 200.4 24.3
5/22/2019 4:03:46 PM 200.3 24.2
5/22/2019 4:03:47 PM 200.2 24.1
5/22/2019 4:03:48 PM 200.0 23.9
5/22/2019 4:03:49 PM 199.9 23.8
5/22/2019 4:03:50 PM 199.8 23.7
5/22/2019 4:03:51 PM 199.6 23.5
5/22/2019 4:03:52 PM 199.5 23.4
5/22/2019 4:03:53 PM 199.4 23.3
5/22/2019 4:03:54 PM 199.2 23.1
5/22/2019 4:03:55 PM 199.1 23.0
5/22/2019 4:03:56 PM 199.0 22.9
5/22/2019 4:03:57 PM 198.8 22.7
5/22/2019 4:03:58 PM 198.7 22.6
5/22/2019 4:03:59 PM 198.6 22.5
5/22/2019 4:04:00 PM 198.5 22.4
5/22/2019 4:04:01 PM 198.4 22.3
5/22/2019 4:04:02 PM 198.4 22.3
5/22/2019 4:04:03 PM 198.3 22.2
5/22/2019 4:04:04 PM 198.2 22.1
5/22/2019 4:04:05 PM 198.1 22.0
Page 262 of 452 August 2019
APPENDIX E46: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
5/22/2019 4:04:06 PM 198.0 21.9
5/22/2019 4:04:07 PM 197.9 21.8
5/22/2019 4:04:08 PM 197.8 21.7
5/22/2019 4:04:09 PM 197.7 21.6
5/22/2019 4:04:10 PM 197.6 21.5
5/22/2019 4:04:11 PM 197.5 21.4
5/22/2019 4:04:12 PM 197.4 21.3
5/22/2019 4:04:13 PM 197.3 21.2
5/22/2019 4:04:14 PM 197.2 21.1
5/22/2019 4:04:15 PM 197.2 21.1
5/22/2019 4:04:16 PM 197.1 21.0
5/22/2019 4:04:17 PM 197.0 20.9
5/22/2019 4:04:18 PM 196.9 20.8
5/22/2019 4:04:19 PM 196.8 20.7
5/22/2019 4:04:20 PM 196.7 20.6
5/22/2019 4:04:21 PM 196.6 20.5
5/22/2019 4:04:22 PM 196.6 20.5
5/22/2019 4:04:23 PM 196.4 20.3
5/22/2019 4:04:24 PM 196.4 20.3
5/22/2019 4:04:25 PM 196.3 20.2
5/22/2019 4:04:26 PM 196.2 20.1
5/22/2019 4:04:27 PM 196.1 20.0
5/22/2019 4:04:28 PM 196.1 20.0
5/22/2019 4:04:29 PM 196.0 19.9
5/22/2019 4:04:30 PM 196.0 19.9
5/22/2019 4:04:31 PM 196.0 19.9
5/22/2019 4:04:32 PM 195.9 19.8
5/22/2019 4:04:33 PM 195.9 19.8
5/22/2019 4:04:34 PM 195.9 19.8
5/22/2019 4:04:35 PM 195.9 19.8
5/22/2019 4:04:36 PM 195.9 19.8
5/22/2019 4:04:37 PM 195.9 19.8
5/22/2019 4:04:38 PM 195.9 19.8
5/22/2019 4:04:39 PM 195.9 19.8
5/22/2019 4:04:40 PM 196.0 19.9
5/22/2019 4:04:41 PM 196.0 19.9
5/22/2019 4:04:42 PM 195.9 19.8
5/22/2019 4:04:43 PM 195.9 19.8
5/22/2019 4:04:44 PM 195.9 19.8
5/22/2019 4:04:45 PM 195.8 19.7
5/22/2019 4:04:46 PM 195.8 19.7
5/22/2019 4:04:47 PM 195.7 19.6
5/22/2019 4:04:48 PM 195.6 19.5
5/22/2019 4:04:49 PM 195.5 19.4
5/22/2019 4:04:50 PM 195.4 19.3
5/22/2019 4:04:51 PM 195.3 19.2
5/22/2019 4:04:52 PM 195.2 19.1
5/22/2019 4:04:53 PM 195.1 19.0
5/22/2019 4:04:54 PM 195.0 18.9
5/22/2019 4:04:55 PM 194.9 18.8
5/22/2019 4:04:56 PM 194.8 18.7
5/22/2019 4:04:57 PM 194.8 18.7
5/22/2019 4:04:58 PM 194.7 18.6
5/22/2019 4:04:59 PM 194.7 18.6
5/22/2019 4:05:00 PM 194.6 18.5
5/22/2019 4:05:01 PM 194.6 18.5
5/22/2019 4:05:02 PM 194.6 18.5
5/22/2019 4:05:03 PM 194.5 18.4
5/22/2019 4:05:04 PM 194.5 18.4
5/22/2019 4:05:05 PM 194.5 18.4
5/22/2019 4:05:06 PM 194.5 18.4
5/22/2019 4:05:07 PM 194.4 18.3
5/22/2019 4:05:08 PM 194.4 18.3
5/22/2019 4:05:09 PM 194.3 18.2
5/22/2019 4:05:10 PM 194.3 18.2
5/22/2019 4:05:11 PM 194.3 18.2
5/22/2019 4:05:12 PM 194.2 18.1
5/22/2019 4:05:13 PM 194.2 18.1
5/22/2019 4:05:14 PM 194.1 18.0
5/22/2019 4:05:15 PM 194.1 18.0
5/22/2019 4:05:16 PM 194.1 18.0
5/22/2019 4:05:17 PM 194.0 17.9
5/22/2019 4:05:18 PM 194.0 17.9
5/22/2019 4:05:19 PM 194.0 17.9
5/22/2019 4:05:20 PM 194.0 17.9
5/22/2019 4:05:21 PM 193.9 17.8
5/22/2019 4:05:22 PM 193.9 17.8
5/22/2019 4:05:23 PM 193.9 17.8
5/22/2019 4:05:24 PM 193.9 17.8
Page 263 of 452 August 2019
APPENDIX E46: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
5/22/2019 4:05:25 PM 193.9 17.8
5/22/2019 4:05:26 PM 193.8 17.7
5/22/2019 4:05:27 PM 193.8 17.7
5/22/2019 4:05:28 PM 193.8 17.7
5/22/2019 4:05:29 PM 193.7 17.6
5/22/2019 4:05:30 PM 193.7 17.6
5/22/2019 4:05:31 PM 193.6 17.5
5/22/2019 4:05:32 PM 193.6 17.5
5/22/2019 4:05:33 PM 193.5 17.4
5/22/2019 4:05:34 PM 193.5 17.4
5/22/2019 4:05:35 PM 193.4 17.3
5/22/2019 4:05:36 PM 193.3 17.2
5/22/2019 4:05:37 PM 193.3 17.2
5/22/2019 4:05:38 PM 193.2 17.1
5/22/2019 4:05:39 PM 193.1 17.0
5/22/2019 4:05:40 PM 193.0 16.9
5/22/2019 4:05:41 PM 192.9 16.8
5/22/2019 4:05:42 PM 192.8 16.7
5/22/2019 4:05:43 PM 192.7 16.6
5/22/2019 4:05:44 PM 192.6 16.5
5/22/2019 4:05:45 PM 192.4 16.3
5/22/2019 4:05:46 PM 192.3 16.2
5/22/2019 4:05:47 PM 192.2 16.1
5/22/2019 4:05:48 PM 192.1 16.0
5/22/2019 4:05:49 PM 192.0 15.9
5/22/2019 4:05:50 PM 191.9 15.8
5/22/2019 4:05:51 PM 191.8 15.7
5/22/2019 4:05:52 PM 191.7 15.6
5/22/2019 4:05:53 PM 191.7 15.6
5/22/2019 4:05:54 PM 191.6 15.5
5/22/2019 4:05:55 PM 191.6 15.5
5/22/2019 4:05:56 PM 191.5 15.4
5/22/2019 4:05:57 PM 191.5 15.4
5/22/2019 4:05:58 PM 191.4 15.3
5/22/2019 4:05:59 PM 191.4 15.3
5/22/2019 4:06:00 PM 191.4 15.3
5/22/2019 4:06:01 PM 191.3 15.2
5/22/2019 4:06:02 PM 191.3 15.2
5/22/2019 4:06:03 PM 191.3 15.2
5/22/2019 4:06:04 PM 191.2 15.1
5/22/2019 4:06:05 PM 191.2 15.1
5/22/2019 4:06:06 PM 191.2 15.1
5/22/2019 4:06:07 PM 191.1 15.0
5/22/2019 4:06:08 PM 191.1 15.0
5/22/2019 4:06:09 PM 191.1 15.0
5/22/2019 4:06:10 PM 191.1 15.0
5/22/2019 4:06:11 PM 191.0 14.9
5/22/2019 4:06:12 PM 191.0 14.9
5/22/2019 4:06:13 PM 191.0 14.9
5/22/2019 4:06:14 PM 190.9 14.8
5/22/2019 4:06:15 PM 190.9 14.8
5/22/2019 4:06:16 PM 190.9 14.8
5/22/2019 4:06:17 PM 190.8 14.7
5/22/2019 4:06:18 PM 190.8 14.7
5/22/2019 4:06:19 PM 190.8 14.7
5/22/2019 4:06:20 PM 190.7 14.6
5/22/2019 4:06:21 PM 190.7 14.6
5/22/2019 4:06:22 PM 190.6 14.5
5/22/2019 4:06:23 PM 190.6 14.5
5/22/2019 4:06:24 PM 190.5 14.4
5/22/2019 4:06:25 PM 190.5 14.4
5/22/2019 4:06:26 PM 190.5 14.4
5/22/2019 4:06:27 PM 190.4 14.3
5/22/2019 4:06:28 PM 190.4 14.3
5/22/2019 4:06:29 PM 190.4 14.3
5/22/2019 4:06:30 PM 190.3 14.2
5/22/2019 4:06:31 PM 190.3 14.2
5/22/2019 4:06:32 PM 190.3 14.2
5/22/2019 4:06:33 PM 190.2 14.1
5/22/2019 4:06:34 PM 190.2 14.1
5/22/2019 4:06:35 PM 190.2 14.1
5/22/2019 4:06:36 PM 190.1 14.0
5/22/2019 4:06:37 PM 190.1 14.0
5/22/2019 4:06:38 PM 190.0 13.9
5/22/2019 4:06:39 PM 190.0 13.9
5/22/2019 4:06:40 PM 189.9 13.8
5/22/2019 4:06:41 PM 189.9 13.8
5/22/2019 4:06:42 PM 189.8 13.7
5/22/2019 4:06:43 PM 189.7 13.6
Page 264 of 452 August 2019
APPENDIX E46: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
5/22/2019 4:06:44 PM 189.7 13.6
5/22/2019 4:06:45 PM 189.6 13.5
5/22/2019 4:06:46 PM 189.5 13.4
5/22/2019 4:06:47 PM 189.5 13.4
5/22/2019 4:06:48 PM 189.4 13.3
5/22/2019 4:06:49 PM 189.3 13.2
5/22/2019 4:06:50 PM 189.3 13.2
5/22/2019 4:06:51 PM 189.3 13.2
5/22/2019 4:06:52 PM 189.2 13.1
5/22/2019 4:06:53 PM 189.2 13.1
5/22/2019 4:06:54 PM 189.1 13.0
5/22/2019 4:06:55 PM 189.1 13.0
5/22/2019 4:06:56 PM 189.0 12.9
5/22/2019 4:06:57 PM 189.0 12.9
5/22/2019 4:06:58 PM 188.9 12.8
5/22/2019 4:06:59 PM 188.9 12.8
5/22/2019 4:07:00 PM 188.9 12.8
5/22/2019 4:07:01 PM 188.8 12.7
5/22/2019 4:07:02 PM 188.8 12.7
5/22/2019 4:07:03 PM 188.8 12.7
5/22/2019 4:07:04 PM 188.7 12.6
5/22/2019 4:07:05 PM 188.7 12.6
5/22/2019 4:07:06 PM 188.7 12.6
5/22/2019 4:07:07 PM 188.6 12.5
5/22/2019 4:07:08 PM 188.6 12.5
5/22/2019 4:07:09 PM 188.6 12.5
5/22/2019 4:07:10 PM 188.5 12.4
5/22/2019 4:07:11 PM 188.5 12.4
5/22/2019 4:07:12 PM 188.5 12.4
5/22/2019 4:07:13 PM 188.4 12.3
5/22/2019 4:07:14 PM 188.4 12.3
5/22/2019 4:07:15 PM 188.4 12.3
5/22/2019 4:07:16 PM 188.3 12.2
5/22/2019 4:07:17 PM 188.3 12.2
5/22/2019 4:07:18 PM 188.3 12.2
5/22/2019 4:07:19 PM 188.2 12.1
5/22/2019 4:07:20 PM 188.2 12.1
5/22/2019 4:07:21 PM 188.2 12.1
5/22/2019 4:07:22 PM 188.1 12.0
5/22/2019 4:07:23 PM 188.0 11.9
5/22/2019 4:07:24 PM 188.0 11.9
5/22/2019 4:07:25 PM 187.9 11.8
5/22/2019 4:07:26 PM 187.9 11.8
5/22/2019 4:07:27 PM 187.8 11.7
5/22/2019 4:07:28 PM 187.8 11.7
5/22/2019 4:07:29 PM 187.7 11.6
5/22/2019 4:07:30 PM 187.7 11.6
5/22/2019 4:07:31 PM 187.6 11.5
5/22/2019 4:07:32 PM 187.6 11.5
5/22/2019 4:07:33 PM 187.6 11.5
5/22/2019 4:07:34 PM 187.5 11.4
5/22/2019 4:07:35 PM 187.5 11.4
5/22/2019 4:07:36 PM 187.5 11.4
5/22/2019 4:07:37 PM 187.5 11.4
5/22/2019 4:07:38 PM 187.4 11.3
5/22/2019 4:07:39 PM 187.4 11.3
5/22/2019 4:07:40 PM 187.4 11.3
5/22/2019 4:07:41 PM 187.4 11.3
5/22/2019 4:07:42 PM 187.3 11.2
5/22/2019 4:07:43 PM 187.3 11.2
5/22/2019 4:07:44 PM 187.2 11.1
5/22/2019 4:07:45 PM 187.2 11.1
5/22/2019 4:07:46 PM 187.1 11.0
5/22/2019 4:07:47 PM 187.0 10.9
5/22/2019 4:07:48 PM 186.9 10.8
5/22/2019 4:07:49 PM 186.8 10.7
5/22/2019 4:07:50 PM 186.7 10.6
5/22/2019 4:07:51 PM 186.6 10.5
5/22/2019 4:07:52 PM 186.6 10.5
5/22/2019 4:07:53 PM 186.5 10.4
5/22/2019 4:07:54 PM 186.4 10.3
5/22/2019 4:07:55 PM 186.3 10.2
5/22/2019 4:07:56 PM 186.2 10.1
5/22/2019 4:07:57 PM 186.2 10.1
5/22/2019 4:07:58 PM 186.1 10.0
5/22/2019 4:07:59 PM 186.1 10.0
5/22/2019 4:08:00 PM 186.1 10.0
5/22/2019 4:08:01 PM 186.1 10.0
5/22/2019 4:08:02 PM 186.1 10.0
Page 265 of 452 August 2019
APPENDIX E46: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
5/22/2019 4:08:03 PM 186.1 10.0
5/22/2019 4:08:04 PM 186.1 10.0
5/22/2019 4:08:05 PM 186.0 9.9
5/22/2019 4:08:06 PM 186.0 9.9
5/22/2019 4:08:07 PM 186.0 9.9
5/22/2019 4:08:08 PM 186.0 9.9
5/22/2019 4:08:09 PM 186.0 9.9
5/22/2019 4:08:10 PM 186.0 9.9
5/22/2019 4:08:11 PM 186.0 9.9
5/22/2019 4:08:12 PM 186.0 9.9
5/22/2019 4:08:13 PM 186.0 9.9
5/22/2019 4:08:14 PM 185.9 9.8
5/22/2019 4:08:15 PM 185.9 9.8
5/22/2019 4:08:16 PM 185.9 9.8
5/22/2019 4:08:17 PM 185.9 9.8
5/22/2019 4:08:18 PM 185.8 9.7
5/22/2019 4:08:19 PM 185.8 9.7
5/22/2019 4:08:20 PM 185.7 9.6
5/22/2019 4:08:21 PM 185.7 9.6
5/22/2019 4:08:22 PM 185.7 9.6
5/22/2019 4:08:23 PM 185.6 9.5
5/22/2019 4:08:24 PM 185.6 9.5
5/22/2019 4:08:25 PM 185.5 9.4
5/22/2019 4:08:26 PM 185.5 9.4
5/22/2019 4:08:27 PM 185.4 9.3
5/22/2019 4:08:28 PM 185.4 9.3
5/22/2019 4:08:29 PM 185.4 9.3
5/22/2019 4:08:30 PM 185.3 9.2
5/22/2019 4:08:31 PM 185.3 9.2
5/22/2019 4:08:32 PM 185.3 9.2
5/22/2019 4:08:33 PM 185.2 9.1
5/22/2019 4:08:34 PM 185.2 9.1
5/22/2019 4:08:35 PM 185.2 9.1
5/22/2019 4:08:36 PM 185.1 9.0
5/22/2019 4:08:37 PM 185.1 9.0
5/22/2019 4:08:38 PM 185.1 9.0
5/22/2019 4:08:39 PM 185.0 8.9
5/22/2019 4:08:40 PM 185.0 8.9
5/22/2019 4:08:41 PM 184.9 8.8
5/22/2019 4:08:42 PM 184.9 8.8
5/22/2019 4:08:43 PM 184.9 8.8
5/22/2019 4:08:44 PM 184.8 8.7
5/22/2019 4:08:45 PM 184.8 8.7
5/22/2019 4:08:46 PM 184.8 8.7
5/22/2019 4:08:47 PM 184.7 8.6
5/22/2019 4:08:48 PM 184.7 8.6
5/22/2019 4:08:49 PM 184.7 8.6
5/22/2019 4:08:50 PM 184.7 8.6
5/22/2019 4:08:51 PM 184.6 8.5
5/22/2019 4:08:52 PM 184.6 8.5
5/22/2019 4:08:53 PM 184.6 8.5
5/22/2019 4:08:54 PM 184.5 8.4
5/22/2019 4:08:55 PM 184.5 8.4
5/22/2019 4:08:56 PM 184.4 8.3
5/22/2019 4:08:57 PM 184.4 8.3
5/22/2019 4:08:58 PM 184.3 8.2
5/22/2019 4:08:59 PM 184.3 8.2
5/22/2019 4:09:00 PM 184.2 8.1
5/22/2019 4:09:01 PM 184.1 8.0
5/22/2019 4:09:02 PM 184.1 8.0
5/22/2019 4:09:03 PM 184.0 7.9
5/22/2019 4:09:04 PM 184.0 7.9
5/22/2019 4:09:05 PM 183.9 7.8
5/22/2019 4:09:06 PM 183.9 7.8
5/22/2019 4:09:07 PM 183.8 7.7
5/22/2019 4:09:08 PM 183.8 7.7
5/22/2019 4:09:09 PM 183.7 7.6
5/22/2019 4:09:10 PM 183.7 7.6
5/22/2019 4:09:11 PM 183.7 7.6
5/22/2019 4:09:12 PM 183.7 7.6
5/22/2019 4:09:13 PM 183.6 7.5
5/22/2019 4:09:14 PM 183.6 7.5
5/22/2019 4:09:15 PM 183.6 7.5
5/22/2019 4:09:16 PM 183.6 7.5
5/22/2019 4:09:17 PM 183.6 7.5
5/22/2019 4:09:18 PM 183.5 7.4
5/22/2019 4:09:19 PM 183.5 7.4
5/22/2019 4:09:20 PM 183.5 7.4
5/22/2019 4:09:21 PM 183.5 7.4
Page 266 of 452 August 2019
APPENDIX E46: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
5/22/2019 4:09:22 PM 183.5 7.4
5/22/2019 4:09:23 PM 183.5 7.4
5/22/2019 4:09:24 PM 183.5 7.4
5/22/2019 4:09:25 PM 183.4 7.3
5/22/2019 4:09:26 PM 183.4 7.3
5/22/2019 4:09:27 PM 183.4 7.3
5/22/2019 4:09:28 PM 183.4 7.3
5/22/2019 4:09:29 PM 183.4 7.3
5/22/2019 4:09:30 PM 183.4 7.3
5/22/2019 4:09:31 PM 183.3 7.2
5/22/2019 4:09:32 PM 183.3 7.2
5/22/2019 4:09:33 PM 183.3 7.2
5/22/2019 4:09:34 PM 183.3 7.2
5/22/2019 4:09:35 PM 183.3 7.2
5/22/2019 4:09:36 PM 183.3 7.2
5/22/2019 4:09:37 PM 183.3 7.2
5/22/2019 4:09:38 PM 183.3 7.2
5/22/2019 4:09:39 PM 183.3 7.2
5/22/2019 4:09:40 PM 183.2 7.1
5/22/2019 4:09:41 PM 183.2 7.1
5/22/2019 4:09:42 PM 183.2 7.1
5/22/2019 4:09:43 PM 183.2 7.1
5/22/2019 4:09:44 PM 183.2 7.1
5/22/2019 4:09:45 PM 183.2 7.1
5/22/2019 4:09:46 PM 183.2 7.1
5/22/2019 4:09:47 PM 183.2 7.1
5/22/2019 4:09:48 PM 183.2 7.1
5/22/2019 4:09:49 PM 183.2 7.1
5/22/2019 4:09:50 PM 183.1 7.0
5/22/2019 4:09:51 PM 183.1 7.0
5/22/2019 4:09:52 PM 183.1 7.0
5/22/2019 4:09:53 PM 183.0 6.9
5/22/2019 4:09:54 PM 183.0 6.9
5/22/2019 4:09:55 PM 182.9 6.8
5/22/2019 4:09:56 PM 182.9 6.8
5/22/2019 4:09:57 PM 182.9 6.8
5/22/2019 4:09:58 PM 182.8 6.7
5/22/2019 4:09:59 PM 182.8 6.7
5/22/2019 4:10:00 PM 182.7 6.6
5/22/2019 4:10:01 PM 182.7 6.6
5/22/2019 4:10:02 PM 182.7 6.6
5/22/2019 4:10:03 PM 182.7 6.6
5/22/2019 4:10:04 PM 182.6 6.5
5/22/2019 4:10:05 PM 182.6 6.5
5/22/2019 4:10:06 PM 182.6 6.5
5/22/2019 4:10:07 PM 182.6 6.5
5/22/2019 4:10:08 PM 182.6 6.5
5/22/2019 4:10:09 PM 182.6 6.5
5/22/2019 4:10:10 PM 182.6 6.5
5/22/2019 4:10:11 PM 182.5 6.4
5/22/2019 4:10:12 PM 182.5 6.4
5/22/2019 4:10:13 PM 182.5 6.4
5/22/2019 4:10:14 PM 182.4 6.3
5/22/2019 4:10:15 PM 182.4 6.3
5/22/2019 4:10:16 PM 182.4 6.3
5/22/2019 4:10:17 PM 182.4 6.3
5/22/2019 4:10:18 PM 182.3 6.2
5/22/2019 4:10:19 PM 182.3 6.2
5/22/2019 4:10:20 PM 182.2 6.1
5/22/2019 4:10:21 PM 182.2 6.1
5/22/2019 4:10:22 PM 182.1 6.0
5/22/2019 4:10:23 PM 182.1 6.0
5/22/2019 4:10:24 PM 182.0 5.9
5/22/2019 4:10:25 PM 182.0 5.9
5/22/2019 4:10:26 PM 182.0 5.9
5/22/2019 4:10:27 PM 181.9 5.8
5/22/2019 4:10:28 PM 181.9 5.8
5/22/2019 4:10:29 PM 181.8 5.7
5/22/2019 4:10:30 PM 181.8 5.7
5/22/2019 4:10:31 PM 181.8 5.7
5/22/2019 4:10:32 PM 181.7 5.6
5/22/2019 4:10:33 PM 181.7 5.6
5/22/2019 4:10:34 PM 181.7 5.6
5/22/2019 4:10:35 PM 181.6 5.5
5/22/2019 4:10:36 PM 181.6 5.5
5/22/2019 4:10:37 PM 181.6 5.5
5/22/2019 4:10:38 PM 181.6 5.5
5/22/2019 4:10:39 PM 181.6 5.5
5/22/2019 4:10:40 PM 181.6 5.5
Page 267 of 452 August 2019
APPENDIX E46: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
5/22/2019 4:10:41 PM 181.6 5.5
5/22/2019 4:10:42 PM 181.5 5.4
5/22/2019 4:10:43 PM 181.5 5.4
5/22/2019 4:10:44 PM 181.5 5.4
5/22/2019 4:10:45 PM 181.5 5.4
5/22/2019 4:10:46 PM 181.5 5.4
5/22/2019 4:10:47 PM 181.5 5.4
5/22/2019 4:10:48 PM 181.5 5.4
5/22/2019 4:10:49 PM 181.4 5.3
5/22/2019 4:10:50 PM 181.4 5.3
5/22/2019 4:10:51 PM 181.4 5.3
5/22/2019 4:10:52 PM 181.3 5.2
5/22/2019 4:10:53 PM 181.3 5.2
5/22/2019 4:10:54 PM 181.2 5.1
5/22/2019 4:10:55 PM 181.2 5.1
5/22/2019 4:10:56 PM 181.1 5.0
5/22/2019 4:10:57 PM 181.1 5.0
5/22/2019 4:10:58 PM 181.0 4.9
5/22/2019 4:10:59 PM 181.0 4.9
5/22/2019 4:11:00 PM 180.9 4.8
5/22/2019 4:11:01 PM 180.9 4.8
5/22/2019 4:11:02 PM 180.9 4.8
5/22/2019 4:11:03 PM 180.8 4.7
5/22/2019 4:11:04 PM 180.8 4.7
5/22/2019 4:11:05 PM 180.8 4.7
5/22/2019 4:11:06 PM 180.8 4.7
5/22/2019 4:11:07 PM 180.8 4.7
5/22/2019 4:11:08 PM 180.8 4.7
5/22/2019 4:11:09 PM 180.8 4.7
5/22/2019 4:11:10 PM 180.8 4.7
5/22/2019 4:11:11 PM 180.8 4.7
5/22/2019 4:11:12 PM 180.8 4.7
5/22/2019 4:11:13 PM 180.8 4.7
5/22/2019 4:11:14 PM 180.7 4.6
5/22/2019 4:11:15 PM 180.7 4.6
5/22/2019 4:11:16 PM 180.7 4.6
5/22/2019 4:11:17 PM 180.7 4.6
5/22/2019 4:11:18 PM 180.7 4.6
5/22/2019 4:11:19 PM 180.7 4.6
5/22/2019 4:11:20 PM 180.7 4.6
5/22/2019 4:11:21 PM 180.7 4.6
5/22/2019 4:11:22 PM 180.7 4.6
5/22/2019 4:11:23 PM 180.7 4.6
5/22/2019 4:11:24 PM 180.7 4.6
5/22/2019 4:11:25 PM 180.7 4.6
5/22/2019 4:11:26 PM 180.7 4.6
5/22/2019 4:11:27 PM 180.6 4.5
5/22/2019 4:11:28 PM 180.6 4.5
5/22/2019 4:11:29 PM 180.6 4.5
5/22/2019 4:11:30 PM 180.6 4.5
5/22/2019 4:11:31 PM 180.6 4.5
5/22/2019 4:11:32 PM 180.6 4.5
5/22/2019 4:11:33 PM 180.6 4.5
5/22/2019 4:11:34 PM 180.5 4.4
5/22/2019 4:11:35 PM 180.5 4.4
5/22/2019 4:11:36 PM 180.5 4.4
5/22/2019 4:11:37 PM 180.5 4.4
5/22/2019 4:11:38 PM 180.5 4.4
5/22/2019 4:11:39 PM 180.4 4.3
5/22/2019 4:11:40 PM 180.4 4.3
5/22/2019 4:11:41 PM 180.4 4.3
5/22/2019 4:11:42 PM 180.4 4.3
5/22/2019 4:11:43 PM 180.4 4.3
5/22/2019 4:11:44 PM 180.4 4.3
5/22/2019 4:11:45 PM 180.4 4.3
5/22/2019 4:11:46 PM 180.3 4.2
5/22/2019 4:11:47 PM 180.3 4.2
5/22/2019 4:11:48 PM 180.3 4.2
5/22/2019 4:11:49 PM 180.3 4.2
5/22/2019 4:11:50 PM 180.3 4.2
5/22/2019 4:11:51 PM 180.3 4.2
5/22/2019 4:11:52 PM 180.3 4.2
5/22/2019 4:11:53 PM 180.3 4.2
5/22/2019 4:11:54 PM 180.3 4.2
5/22/2019 4:11:55 PM 180.3 4.2
5/22/2019 4:11:56 PM 180.2 4.1
5/22/2019 4:11:57 PM 180.2 4.1
5/22/2019 4:11:58 PM 180.2 4.1
5/22/2019 4:11:59 PM 180.2 4.1
Page 268 of 452 August 2019
APPENDIX E46: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
5/22/2019 4:12:00 PM 180.1 4.0
5/22/2019 4:12:01 PM 180.1 4.0
5/22/2019 4:12:02 PM 180.1 4.0
5/22/2019 4:12:03 PM 180.1 4.0
5/22/2019 4:12:04 PM 180.0 3.9
5/22/2019 4:12:05 PM 180.0 3.9
5/22/2019 4:12:06 PM 180.0 3.9
5/22/2019 4:12:07 PM 180.0 3.9
5/22/2019 4:12:08 PM 179.9 3.8
5/22/2019 4:12:09 PM 179.9 3.8
5/22/2019 4:12:10 PM 179.9 3.8
5/22/2019 4:12:11 PM 179.9 3.8
5/22/2019 4:12:12 PM 179.9 3.8
5/22/2019 4:12:13 PM 179.8 3.7
5/22/2019 4:12:14 PM 179.8 3.7
5/22/2019 4:12:15 PM 179.8 3.7
5/22/2019 4:12:16 PM 179.8 3.7
5/22/2019 4:12:17 PM 179.8 3.7
Page 269 of 452 August 2019
APPENDIX E46: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-B2-TEST-2 1528
SEEP-B2-TEST-2 1532
SEEP-B2-TEST-2 1533
SEEP-B2-TEST-2 1534
EC Reading
(µS/cms)
SEEP-B2-TEST-2 29.9
SEEP-B2-TEST-2 167
SEEP-B2-TEST-2 426
SEEP-B2-TEST-2 3,329
SEEP-B2-TEST-2 15,499
SEEP-B2-TEST-2 127,509
q 300,200
K 1.2780
7.0
11.1
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
NR Not recorded
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Table E3 SEEP-B2 TEST-2 YSI Salt Dilution Calibration Data
(µS/cms) (°C)
Table E2 SEEP-B2 TEST-2 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Geometric Mean 162.4 (µS/cms)
151.5 NR
165.2 NR
167.0 NR
166.4 NR
Average 162.5 (µS/cms)
Average (pre-test)176.1 (µS/cms)
Average (post-test)181.1 (µS/cms)
1
10
100
1,000
10,000
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)547,402.8
100,000
Table E4 SEEP-B2 TEST-2 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
(°C)
Temperature
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
NR
NR
NR
NR
(s) . (µS/cms)
Calculated Flow Rate Q
L/s
GPM
NR
NR
Location Calibration
Concentration
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 270 of 452 August 2019
APPENDIX E47: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
5/22/2019 4:38:31 PM 178.2 -
5/22/2019 4:38:32 PM 178.1 -
5/22/2019 4:38:33 PM 178.1 -
5/22/2019 4:38:34 PM 178.1 -
5/22/2019 4:38:35 PM 178.0 -
5/22/2019 4:38:36 PM 178.0 -
5/22/2019 4:38:37 PM 178.0 -
5/22/2019 4:38:38 PM 177.9 -
5/22/2019 4:38:39 PM 177.9 -
5/22/2019 4:38:40 PM 177.9 -
5/22/2019 4:38:41 PM 177.9 -
5/22/2019 4:38:42 PM 177.9 -
5/22/2019 4:38:43 PM 177.9 -
5/22/2019 4:38:44 PM 177.8 -
5/22/2019 4:38:45 PM 177.8 -
5/22/2019 4:38:46 PM 177.8 -
5/22/2019 4:38:47 PM 177.8 -
5/22/2019 4:38:48 PM 177.7 -
5/22/2019 4:38:49 PM 177.7 -
5/22/2019 4:38:50 PM 177.7 -
5/22/2019 4:38:51 PM 177.7 -
5/22/2019 4:38:52 PM 177.6 -
5/22/2019 4:38:53 PM 177.6 -
5/22/2019 4:38:54 PM 177.6 -
5/22/2019 4:38:55 PM 177.5 -
5/22/2019 4:38:56 PM 177.5 -
5/22/2019 4:38:57 PM 177.5 -
5/22/2019 4:38:58 PM 177.5 -
5/22/2019 4:38:59 PM 177.5 -
5/22/2019 4:39:00 PM 177.4 -
5/22/2019 4:39:01 PM 177.4 -
5/22/2019 4:39:02 PM 177.4 -
5/22/2019 4:39:03 PM 177.4 -
5/22/2019 4:39:04 PM 177.4 -
5/22/2019 4:39:05 PM 177.3 -
5/22/2019 4:39:06 PM 177.3 -
5/22/2019 4:39:07 PM 177.3 -
5/22/2019 4:39:08 PM 177.3 -
5/22/2019 4:39:09 PM 177.5 -
5/22/2019 4:39:10 PM 178.6 -
5/22/2019 4:39:11 PM 239.8 62.1
5/22/2019 4:39:12 PM 298.9 121.2
5/22/2019 4:39:13 PM 411.0 233.3
5/22/2019 4:39:14 PM 501.8 324.1
5/22/2019 4:39:15 PM 744.4 566.7
5/22/2019 4:39:16 PM 1709.0 1531.3
5/22/2019 4:39:17 PM 1987.6 1809.9
5/22/2019 4:39:18 PM 2150.7 1973.0
5/22/2019 4:39:19 PM 2561.9 2384.2
5/22/2019 4:39:20 PM 3582.1 3404.4
5/22/2019 4:39:21 PM 4529.2 4351.5
5/22/2019 4:39:22 PM 5742.7 5565.0
5/22/2019 4:39:23 PM 6279.8 6102.1
5/22/2019 4:39:24 PM 7216.3 7038.6
5/22/2019 4:39:25 PM 7330.3 7152.6
5/22/2019 4:39:26 PM 8381.3 8203.6
5/22/2019 4:39:27 PM 8554.3 8376.6
5/22/2019 4:39:28 PM 8835.1 8657.4
5/22/2019 4:39:29 PM 9059.9 8882.2
5/22/2019 4:39:30 PM 9260.6 9082.9
5/22/2019 4:39:31 PM 9386.4 9208.7
5/22/2019 4:39:32 PM 9490.3 9312.6
5/22/2019 4:39:33 PM 9564.6 9386.9
5/22/2019 4:39:34 PM 9642.7 9465.0
5/22/2019 4:39:35 PM 9699.2 9521.5
5/22/2019 4:39:36 PM 9736.1 9558.4
5/22/2019 4:39:37 PM 9755.6 9577.9
5/22/2019 4:39:38 PM 9759.1 9581.4
5/22/2019 4:39:39 PM 9756.4 9578.7
5/22/2019 4:39:40 PM 9739.5 9561.8
Table E1 SEEP-B2 TEST-4 Data Log
Page 271 of 452 August 2019
APPENDIX E47: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-4 Data Log
5/22/2019 4:39:41 PM 9218.8 9041.1
5/22/2019 4:39:42 PM 9178.8 9001.1
5/22/2019 4:39:43 PM 9008.2 8830.5
5/22/2019 4:39:44 PM 8796.2 8618.5
5/22/2019 4:39:45 PM 8724.1 8546.4
5/22/2019 4:39:46 PM 8655.7 8478.0
5/22/2019 4:39:47 PM 8582.5 8404.8
5/22/2019 4:39:48 PM 8494.3 8316.6
5/22/2019 4:39:49 PM 7927.5 7749.8
5/22/2019 4:39:50 PM 7531.4 7353.7
5/22/2019 4:39:51 PM 7391.7 7214.0
5/22/2019 4:39:52 PM 7404.7 7227.0
5/22/2019 4:39:53 PM 7327.5 7149.8
5/22/2019 4:39:54 PM 7234.5 7056.8
5/22/2019 4:39:55 PM 7143.1 6965.4
5/22/2019 4:39:56 PM 6690.1 6512.4
5/22/2019 4:39:57 PM 6541.8 6364.1
5/22/2019 4:39:58 PM 6283.4 6105.7
5/22/2019 4:39:59 PM 6066.2 5888.5
5/22/2019 4:40:00 PM 6074.8 5897.1
5/22/2019 4:40:01 PM 5953.4 5775.7
5/22/2019 4:40:02 PM 5505.2 5327.5
5/22/2019 4:40:03 PM 5258.1 5080.4
5/22/2019 4:40:04 PM 5294.8 5117.1
5/22/2019 4:40:05 PM 5251.7 5074.0
5/22/2019 4:40:06 PM 4764.1 4586.4
5/22/2019 4:40:07 PM 4763.1 4585.4
5/22/2019 4:40:08 PM 4531.3 4353.6
5/22/2019 4:40:09 PM 4382.5 4204.8
5/22/2019 4:40:10 PM 4251.6 4073.9
5/22/2019 4:40:11 PM 4198.0 4020.3
5/22/2019 4:40:12 PM 4155.3 3977.6
5/22/2019 4:40:13 PM 3876.4 3698.7
5/22/2019 4:40:14 PM 3808.5 3630.8
5/22/2019 4:40:15 PM 3777.1 3599.4
5/22/2019 4:40:16 PM 3745.8 3568.1
5/22/2019 4:40:17 PM 3711.2 3533.5
5/22/2019 4:40:18 PM 3658.7 3481.0
5/22/2019 4:40:19 PM 3620.4 3442.7
5/22/2019 4:40:20 PM 3589.6 3411.9
5/22/2019 4:40:21 PM 3153.6 2975.9
5/22/2019 4:40:22 PM 3000.2 2822.5
5/22/2019 4:40:23 PM 2855.9 2678.2
5/22/2019 4:40:24 PM 2775.0 2597.3
5/22/2019 4:40:25 PM 2699.1 2521.4
5/22/2019 4:40:26 PM 2660.4 2482.7
5/22/2019 4:40:27 PM 2632.8 2455.1
5/22/2019 4:40:28 PM 2610.4 2432.7
5/22/2019 4:40:29 PM 2591.0 2413.3
5/22/2019 4:40:30 PM 2430.8 2253.1
5/22/2019 4:40:31 PM 2310.0 2132.3
5/22/2019 4:40:32 PM 2218.5 2040.8
5/22/2019 4:40:33 PM 2176.6 1998.9
5/22/2019 4:40:34 PM 2153.2 1975.5
5/22/2019 4:40:35 PM 2113.0 1935.3
5/22/2019 4:40:36 PM 2085.6 1907.9
5/22/2019 4:40:37 PM 2067.0 1889.3
5/22/2019 4:40:38 PM 2055.7 1878.0
5/22/2019 4:40:39 PM 1894.7 1717.0
5/22/2019 4:40:40 PM 1846.1 1668.4
5/22/2019 4:40:41 PM 1817.9 1640.2
5/22/2019 4:40:42 PM 1772.4 1594.7
5/22/2019 4:40:43 PM 1737.9 1560.2
5/22/2019 4:40:44 PM 1696.2 1518.5
5/22/2019 4:40:45 PM 1582.4 1404.7
5/22/2019 4:40:46 PM 1529.5 1351.8
5/22/2019 4:40:47 PM 1484.3 1306.6
5/22/2019 4:40:48 PM 1448.2 1270.5
5/22/2019 4:40:49 PM 1442.7 1265.0
5/22/2019 4:40:50 PM 1430.5 1252.8
5/22/2019 4:40:51 PM 1420.9 1243.2
5/22/2019 4:40:52 PM 1319.0 1141.3
5/22/2019 4:40:53 PM 1277.6 1099.9
5/22/2019 4:40:54 PM 1236.8 1059.1
5/22/2019 4:40:55 PM 1229.9 1052.2
5/22/2019 4:40:56 PM 1221.1 1043.4
5/22/2019 4:40:57 PM 1201.3 1023.6
Page 272 of 452 August 2019
APPENDIX E47: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-4 Data Log
5/22/2019 4:40:58 PM 1187.9 1010.2
5/22/2019 4:40:59 PM 1177.4 999.7
5/22/2019 4:41:00 PM 1108.6 930.9
5/22/2019 4:41:01 PM 1075.1 897.4
5/22/2019 4:41:02 PM 1048.9 871.2
5/22/2019 4:41:03 PM 1038.9 861.2
5/22/2019 4:41:04 PM 1029.5 851.8
5/22/2019 4:41:05 PM 1009.6 831.9
5/22/2019 4:41:06 PM 994.7 817.0
5/22/2019 4:41:07 PM 980.9 803.2
5/22/2019 4:41:08 PM 972.2 794.5
5/22/2019 4:41:09 PM 901.8 724.1
5/22/2019 4:41:10 PM 892.6 714.9
5/22/2019 4:41:11 PM 881.4 703.7
5/22/2019 4:41:12 PM 877.9 700.2
5/22/2019 4:41:13 PM 868.8 691.1
5/22/2019 4:41:14 PM 862.2 684.5
5/22/2019 4:41:15 PM 854.9 677.2
5/22/2019 4:41:16 PM 804.6 626.9
5/22/2019 4:41:17 PM 792.7 615.0
5/22/2019 4:41:18 PM 777.0 599.3
5/22/2019 4:41:19 PM 768.9 591.2
5/22/2019 4:41:20 PM 763.5 585.8
5/22/2019 4:41:21 PM 759.6 581.9
5/22/2019 4:41:22 PM 755.4 577.7
5/22/2019 4:41:23 PM 750.2 572.5
5/22/2019 4:41:24 PM 743.0 565.3
5/22/2019 4:41:25 PM 737.7 560.0
5/22/2019 4:41:26 PM 732.4 554.7
5/22/2019 4:41:27 PM 728.3 550.6
5/22/2019 4:41:28 PM 683.9 506.2
5/22/2019 4:41:29 PM 674.0 496.3
5/22/2019 4:41:30 PM 657.2 479.5
5/22/2019 4:41:31 PM 652.8 475.1
5/22/2019 4:41:32 PM 650.1 472.4
5/22/2019 4:41:33 PM 645.3 467.6
5/22/2019 4:41:34 PM 640.5 462.8
5/22/2019 4:41:35 PM 638.6 460.9
5/22/2019 4:41:36 PM 594.7 417.0
5/22/2019 4:41:37 PM 600.3 422.6
5/22/2019 4:41:38 PM 594.5 416.8
5/22/2019 4:41:39 PM 592.7 415.0
5/22/2019 4:41:40 PM 588.0 410.3
5/22/2019 4:41:41 PM 584.9 407.2
5/22/2019 4:41:42 PM 581.8 404.1
5/22/2019 4:41:43 PM 578.3 400.6
5/22/2019 4:41:44 PM 575.7 398.0
5/22/2019 4:41:45 PM 572.8 395.1
5/22/2019 4:41:46 PM 570.5 392.8
5/22/2019 4:41:47 PM 568.0 390.3
5/22/2019 4:41:48 PM 565.9 388.2
5/22/2019 4:41:49 PM 563.7 386.0
5/22/2019 4:41:50 PM 561.7 384.0
5/22/2019 4:41:51 PM 559.3 381.6
5/22/2019 4:41:52 PM 555.6 377.9
5/22/2019 4:41:53 PM 550.6 372.9
5/22/2019 4:41:54 PM 546.3 368.6
5/22/2019 4:41:55 PM 541.7 364.0
5/22/2019 4:41:56 PM 537.8 360.1
5/22/2019 4:41:57 PM 533.5 355.8
5/22/2019 4:41:58 PM 529.9 352.2
5/22/2019 4:41:59 PM 526.0 348.3
5/22/2019 4:42:00 PM 522.1 344.4
5/22/2019 4:42:01 PM 518.9 341.2
5/22/2019 4:42:02 PM 515.0 337.3
5/22/2019 4:42:03 PM 511.8 334.1
5/22/2019 4:42:04 PM 508.2 330.5
5/22/2019 4:42:05 PM 505.2 327.5
5/22/2019 4:42:06 PM 502.1 324.4
5/22/2019 4:42:07 PM 499.4 321.7
5/22/2019 4:42:08 PM 496.2 318.5
5/22/2019 4:42:09 PM 493.5 315.8
5/22/2019 4:42:10 PM 490.3 312.6
5/22/2019 4:42:11 PM 487.4 309.7
5/22/2019 4:42:12 PM 484.0 306.3
5/22/2019 4:42:13 PM 481.1 303.4
5/22/2019 4:42:14 PM 478.1 300.4
5/22/2019 4:42:15 PM 475.5 297.8
5/22/2019 4:42:16 PM 472.5 294.8
Page 273 of 452 August 2019
APPENDIX E47: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-4 Data Log
5/22/2019 4:42:17 PM 469.8 292.1
5/22/2019 4:42:18 PM 466.6 288.9
5/22/2019 4:42:19 PM 463.8 286.1
5/22/2019 4:42:20 PM 460.7 283.0
5/22/2019 4:42:21 PM 457.5 279.8
5/22/2019 4:42:22 PM 454.8 277.1
5/22/2019 4:42:23 PM 452.0 274.3
5/22/2019 4:42:24 PM 449.6 271.9
5/22/2019 4:42:25 PM 446.9 269.2
5/22/2019 4:42:26 PM 444.4 266.7
5/22/2019 4:42:27 PM 441.3 263.6
5/22/2019 4:42:28 PM 438.7 261.0
5/22/2019 4:42:29 PM 436.0 258.3
5/22/2019 4:42:30 PM 433.7 256.0
5/22/2019 4:42:31 PM 431.4 253.7
5/22/2019 4:42:32 PM 429.5 251.8
5/22/2019 4:42:33 PM 427.6 249.9
5/22/2019 4:42:34 PM 425.9 248.2
5/22/2019 4:42:35 PM 423.9 246.2
5/22/2019 4:42:36 PM 421.9 244.2
5/22/2019 4:42:37 PM 419.7 242.0
5/22/2019 4:42:38 PM 417.7 240.0
5/22/2019 4:42:39 PM 415.7 238.0
5/22/2019 4:42:40 PM 413.7 236.0
5/22/2019 4:42:41 PM 411.9 234.2
5/22/2019 4:42:42 PM 409.9 232.2
5/22/2019 4:42:43 PM 408.1 230.4
5/22/2019 4:42:44 PM 406.1 228.4
5/22/2019 4:42:45 PM 404.2 226.5
5/22/2019 4:42:46 PM 402.1 224.4
5/22/2019 4:42:47 PM 400.5 222.8
5/22/2019 4:42:48 PM 398.7 221.0
5/22/2019 4:42:49 PM 397.2 219.5
5/22/2019 4:42:50 PM 395.7 218.0
5/22/2019 4:42:51 PM 394.4 216.7
5/22/2019 4:42:52 PM 393.0 215.3
5/22/2019 4:42:53 PM 391.8 214.1
5/22/2019 4:42:54 PM 390.4 212.7
5/22/2019 4:42:55 PM 389.3 211.6
5/22/2019 4:42:56 PM 387.9 210.2
5/22/2019 4:42:57 PM 386.7 209.0
5/22/2019 4:42:58 PM 385.1 207.4
5/22/2019 4:42:59 PM 383.7 206.0
5/22/2019 4:43:00 PM 382.0 204.3
5/22/2019 4:43:01 PM 380.4 202.7
5/22/2019 4:43:02 PM 379.0 201.3
5/22/2019 4:43:03 PM 377.4 199.7
5/22/2019 4:43:04 PM 376.1 198.4
5/22/2019 4:43:05 PM 374.6 196.9
5/22/2019 4:43:06 PM 373.2 195.5
5/22/2019 4:43:07 PM 371.7 194.0
5/22/2019 4:43:08 PM 370.4 192.7
5/22/2019 4:43:09 PM 369.0 191.3
5/22/2019 4:43:10 PM 367.8 190.1
5/22/2019 4:43:11 PM 366.4 188.7
5/22/2019 4:43:12 PM 365.3 187.6
5/22/2019 4:43:13 PM 364.1 186.4
5/22/2019 4:43:14 PM 363.2 185.5
5/22/2019 4:43:15 PM 362.1 184.4
5/22/2019 4:43:16 PM 361.1 183.4
5/22/2019 4:43:17 PM 359.9 182.2
5/22/2019 4:43:18 PM 358.9 181.2
5/22/2019 4:43:19 PM 357.7 180.0
5/22/2019 4:43:20 PM 356.8 179.1
5/22/2019 4:43:21 PM 355.8 178.1
5/22/2019 4:43:22 PM 354.9 177.2
5/22/2019 4:43:23 PM 354.1 176.4
5/22/2019 4:43:24 PM 353.3 175.6
5/22/2019 4:43:25 PM 352.6 174.9
5/22/2019 4:43:26 PM 351.8 174.1
5/22/2019 4:43:27 PM 351.0 173.3
5/22/2019 4:43:28 PM 350.1 172.4
5/22/2019 4:43:29 PM 349.1 171.4
5/22/2019 4:43:30 PM 348.1 170.4
5/22/2019 4:43:31 PM 347.3 169.6
5/22/2019 4:43:32 PM 346.3 168.6
5/22/2019 4:43:33 PM 345.3 167.6
5/22/2019 4:43:34 PM 344.2 166.5
5/22/2019 4:43:35 PM 343.2 165.5
Page 274 of 452 August 2019
APPENDIX E47: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-4 Data Log
5/22/2019 4:43:36 PM 342.0 164.3
5/22/2019 4:43:37 PM 341.0 163.3
5/22/2019 4:43:38 PM 339.8 162.1
5/22/2019 4:43:39 PM 338.8 161.1
5/22/2019 4:43:40 PM 337.7 160.0
5/22/2019 4:43:41 PM 336.6 158.9
5/22/2019 4:43:42 PM 335.7 158.0
5/22/2019 4:43:43 PM 334.7 157.0
5/22/2019 4:43:44 PM 333.8 156.1
5/22/2019 4:43:45 PM 332.7 155.0
5/22/2019 4:43:46 PM 331.8 154.1
5/22/2019 4:43:47 PM 330.7 153.0
5/22/2019 4:43:48 PM 329.7 152.0
5/22/2019 4:43:49 PM 328.7 151.0
5/22/2019 4:43:50 PM 327.7 150.0
5/22/2019 4:43:51 PM 326.7 149.0
5/22/2019 4:43:52 PM 325.9 148.2
5/22/2019 4:43:53 PM 325.0 147.3
5/22/2019 4:43:54 PM 324.2 146.5
5/22/2019 4:43:55 PM 323.3 145.6
5/22/2019 4:43:56 PM 322.6 144.9
5/22/2019 4:43:57 PM 321.7 144.0
5/22/2019 4:43:58 PM 321.0 143.3
5/22/2019 4:43:59 PM 320.3 142.6
5/22/2019 4:44:00 PM 319.6 141.9
5/22/2019 4:44:01 PM 318.9 141.2
5/22/2019 4:44:02 PM 318.2 140.5
5/22/2019 4:44:03 PM 317.5 139.8
5/22/2019 4:44:04 PM 316.8 139.1
5/22/2019 4:44:05 PM 316.1 138.4
5/22/2019 4:44:06 PM 315.3 137.6
5/22/2019 4:44:07 PM 314.6 136.9
5/22/2019 4:44:08 PM 313.9 136.2
5/22/2019 4:44:09 PM 313.3 135.6
5/22/2019 4:44:10 PM 312.6 134.9
5/22/2019 4:44:11 PM 312.0 134.3
5/22/2019 4:44:12 PM 311.4 133.7
5/22/2019 4:44:13 PM 310.9 133.2
5/22/2019 4:44:14 PM 310.3 132.6
5/22/2019 4:44:15 PM 309.7 132.0
5/22/2019 4:44:16 PM 309.2 131.5
5/22/2019 4:44:17 PM 308.7 131.0
5/22/2019 4:44:18 PM 308.1 130.4
5/22/2019 4:44:19 PM 307.7 130.0
5/22/2019 4:44:20 PM 307.1 129.4
5/22/2019 4:44:21 PM 306.6 128.9
5/22/2019 4:44:22 PM 306.1 128.4
5/22/2019 4:44:23 PM 305.5 127.8
5/22/2019 4:44:24 PM 305.0 127.3
5/22/2019 4:44:25 PM 304.5 126.8
5/22/2019 4:44:26 PM 304.0 126.3
5/22/2019 4:44:27 PM 303.5 125.8
5/22/2019 4:44:28 PM 303.0 125.3
5/22/2019 4:44:29 PM 302.4 124.7
5/22/2019 4:44:30 PM 301.9 124.2
5/22/2019 4:44:31 PM 301.2 123.5
5/22/2019 4:44:32 PM 300.7 123.0
5/22/2019 4:44:33 PM 300.0 122.3
5/22/2019 4:44:34 PM 299.5 121.8
5/22/2019 4:44:35 PM 299.0 121.3
5/22/2019 4:44:36 PM 298.5 120.8
5/22/2019 4:44:37 PM 297.8 120.1
5/22/2019 4:44:38 PM 297.3 119.6
5/22/2019 4:44:39 PM 296.7 119.0
5/22/2019 4:44:40 PM 296.1 118.4
5/22/2019 4:44:41 PM 295.5 117.8
5/22/2019 4:44:42 PM 295.1 117.4
5/22/2019 4:44:43 PM 294.5 116.8
5/22/2019 4:44:44 PM 294.0 116.3
5/22/2019 4:44:45 PM 293.6 115.9
5/22/2019 4:44:46 PM 293.1 115.4
5/22/2019 4:44:47 PM 292.6 114.9
5/22/2019 4:44:48 PM 292.1 114.4
5/22/2019 4:44:49 PM 291.6 113.9
5/22/2019 4:44:50 PM 291.1 113.4
5/22/2019 4:44:51 PM 290.6 112.9
5/22/2019 4:44:52 PM 290.0 112.3
5/22/2019 4:44:53 PM 289.6 111.9
5/22/2019 4:44:54 PM 289.1 111.4
Page 275 of 452 August 2019
APPENDIX E47: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-4 Data Log
5/22/2019 4:44:55 PM 288.7 111.0
5/22/2019 4:44:56 PM 288.2 110.5
5/22/2019 4:44:57 PM 287.8 110.1
5/22/2019 4:44:58 PM 287.4 109.7
5/22/2019 4:44:59 PM 287.0 109.3
5/22/2019 4:45:00 PM 286.5 108.8
5/22/2019 4:45:01 PM 286.1 108.4
5/22/2019 4:45:02 PM 285.8 108.1
5/22/2019 4:45:03 PM 285.5 107.8
5/22/2019 4:45:04 PM 285.2 107.5
5/22/2019 4:45:05 PM 284.9 107.2
5/22/2019 4:45:06 PM 284.5 106.8
5/22/2019 4:45:07 PM 284.2 106.5
5/22/2019 4:45:08 PM 283.8 106.1
5/22/2019 4:45:09 PM 283.6 105.9
5/22/2019 4:45:10 PM 283.3 105.6
5/22/2019 4:45:11 PM 283.0 105.3
5/22/2019 4:45:12 PM 282.7 105.0
5/22/2019 4:45:13 PM 282.4 104.7
5/22/2019 4:45:14 PM 282.2 104.5
5/22/2019 4:45:15 PM 281.7 104.0
5/22/2019 4:45:16 PM 281.3 103.6
5/22/2019 4:45:17 PM 280.9 103.2
5/22/2019 4:45:18 PM 280.5 102.8
5/22/2019 4:45:19 PM 280.3 102.6
5/22/2019 4:45:20 PM 279.9 102.2
5/22/2019 4:45:21 PM 279.5 101.8
5/22/2019 4:45:22 PM 279.1 101.4
5/22/2019 4:45:23 PM 278.8 101.1
5/22/2019 4:45:24 PM 278.3 100.6
5/22/2019 4:45:25 PM 278.0 100.3
5/22/2019 4:45:26 PM 277.6 99.9
5/22/2019 4:45:27 PM 277.2 99.5
5/22/2019 4:45:28 PM 276.8 99.1
5/22/2019 4:45:29 PM 276.5 98.8
5/22/2019 4:45:30 PM 276.1 98.4
5/22/2019 4:45:31 PM 275.6 97.9
5/22/2019 4:45:32 PM 275.2 97.5
5/22/2019 4:45:33 PM 274.8 97.1
5/22/2019 4:45:34 PM 274.3 96.6
5/22/2019 4:45:35 PM 273.9 96.2
5/22/2019 4:45:36 PM 273.5 95.8
5/22/2019 4:45:37 PM 273.1 95.4
5/22/2019 4:45:38 PM 272.7 95.0
5/22/2019 4:45:39 PM 272.3 94.6
5/22/2019 4:45:40 PM 271.9 94.2
5/22/2019 4:45:41 PM 271.5 93.8
5/22/2019 4:45:42 PM 271.2 93.5
5/22/2019 4:45:43 PM 270.8 93.1
5/22/2019 4:45:44 PM 270.4 92.7
5/22/2019 4:45:45 PM 270.0 92.3
5/22/2019 4:45:46 PM 269.6 91.9
5/22/2019 4:45:47 PM 269.2 91.5
5/22/2019 4:45:48 PM 268.8 91.1
5/22/2019 4:45:49 PM 268.3 90.6
5/22/2019 4:45:50 PM 267.9 90.2
5/22/2019 4:45:51 PM 267.4 89.7
5/22/2019 4:45:52 PM 267.0 89.3
5/22/2019 4:45:53 PM 266.5 88.8
5/22/2019 4:45:54 PM 266.0 88.3
5/22/2019 4:45:55 PM 265.6 87.9
5/22/2019 4:45:56 PM 265.2 87.5
5/22/2019 4:45:57 PM 264.7 87.0
5/22/2019 4:45:58 PM 264.4 86.7
5/22/2019 4:45:59 PM 263.9 86.2
5/22/2019 4:46:00 PM 263.5 85.8
5/22/2019 4:46:01 PM 263.2 85.5
5/22/2019 4:46:02 PM 262.8 85.1
5/22/2019 4:46:03 PM 262.5 84.8
5/22/2019 4:46:04 PM 262.2 84.5
5/22/2019 4:46:05 PM 261.9 84.2
5/22/2019 4:46:06 PM 261.6 83.9
5/22/2019 4:46:07 PM 261.4 83.7
5/22/2019 4:46:08 PM 261.1 83.4
5/22/2019 4:46:09 PM 260.8 83.1
5/22/2019 4:46:10 PM 260.6 82.9
5/22/2019 4:46:11 PM 260.3 82.6
5/22/2019 4:46:12 PM 260.0 82.3
5/22/2019 4:46:13 PM 259.7 82.0
Page 276 of 452 August 2019
APPENDIX E47: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-4 Data Log
5/22/2019 4:46:14 PM 259.5 81.8
5/22/2019 4:46:15 PM 259.2 81.5
5/22/2019 4:46:16 PM 258.9 81.2
5/22/2019 4:46:17 PM 258.7 81.0
5/22/2019 4:46:18 PM 258.4 80.7
5/22/2019 4:46:19 PM 258.1 80.4
5/22/2019 4:46:20 PM 257.9 80.2
5/22/2019 4:46:21 PM 257.6 79.9
5/22/2019 4:46:22 PM 257.4 79.7
5/22/2019 4:46:23 PM 257.1 79.4
5/22/2019 4:46:24 PM 256.8 79.1
5/22/2019 4:46:25 PM 256.5 78.8
5/22/2019 4:46:26 PM 256.3 78.6
5/22/2019 4:46:27 PM 256.0 78.3
5/22/2019 4:46:28 PM 255.8 78.1
5/22/2019 4:46:29 PM 255.5 77.8
5/22/2019 4:46:30 PM 255.3 77.6
5/22/2019 4:46:31 PM 255.0 77.3
5/22/2019 4:46:32 PM 254.8 77.1
5/22/2019 4:46:33 PM 254.5 76.8
5/22/2019 4:46:34 PM 254.3 76.6
5/22/2019 4:46:35 PM 254.0 76.3
5/22/2019 4:46:36 PM 253.8 76.1
5/22/2019 4:46:37 PM 253.5 75.8
5/22/2019 4:46:38 PM 253.3 75.6
5/22/2019 4:46:39 PM 253.0 75.3
5/22/2019 4:46:40 PM 252.8 75.1
5/22/2019 4:46:41 PM 252.6 74.9
5/22/2019 4:46:42 PM 252.4 74.7
5/22/2019 4:46:43 PM 252.1 74.4
5/22/2019 4:46:44 PM 251.9 74.2
5/22/2019 4:46:45 PM 251.6 73.9
5/22/2019 4:46:46 PM 251.3 73.6
5/22/2019 4:46:47 PM 251.1 73.4
5/22/2019 4:46:48 PM 250.8 73.1
5/22/2019 4:46:49 PM 250.5 72.8
5/22/2019 4:46:50 PM 250.2 72.5
5/22/2019 4:46:51 PM 250.0 72.3
5/22/2019 4:46:52 PM 249.7 72.0
5/22/2019 4:46:53 PM 249.4 71.7
5/22/2019 4:46:54 PM 249.1 71.4
5/22/2019 4:46:55 PM 248.8 71.1
5/22/2019 4:46:56 PM 248.5 70.8
5/22/2019 4:46:57 PM 248.3 70.6
5/22/2019 4:46:58 PM 248.0 70.3
5/22/2019 4:46:59 PM 247.8 70.1
5/22/2019 4:47:00 PM 247.6 69.9
5/22/2019 4:47:01 PM 247.4 69.7
5/22/2019 4:47:02 PM 247.2 69.5
5/22/2019 4:47:03 PM 247.0 69.3
5/22/2019 4:47:04 PM 246.9 69.2
5/22/2019 4:47:05 PM 246.7 69.0
5/22/2019 4:47:06 PM 246.6 68.9
5/22/2019 4:47:07 PM 246.4 68.7
5/22/2019 4:47:08 PM 246.3 68.6
5/22/2019 4:47:09 PM 246.1 68.4
5/22/2019 4:47:10 PM 246.0 68.3
5/22/2019 4:47:11 PM 245.8 68.1
5/22/2019 4:47:12 PM 245.6 67.9
5/22/2019 4:47:13 PM 245.4 67.7
5/22/2019 4:47:14 PM 245.2 67.5
5/22/2019 4:47:15 PM 244.9 67.2
5/22/2019 4:47:16 PM 244.7 67.0
5/22/2019 4:47:17 PM 244.5 66.8
5/22/2019 4:47:18 PM 244.3 66.6
5/22/2019 4:47:19 PM 244.0 66.3
5/22/2019 4:47:20 PM 243.8 66.1
5/22/2019 4:47:21 PM 243.6 65.9
5/22/2019 4:47:22 PM 243.3 65.6
5/22/2019 4:47:23 PM 243.1 65.4
5/22/2019 4:47:24 PM 242.9 65.2
5/22/2019 4:47:25 PM 242.8 65.1
5/22/2019 4:47:26 PM 242.6 64.9
5/22/2019 4:47:27 PM 242.4 64.7
5/22/2019 4:47:28 PM 242.3 64.6
5/22/2019 4:47:29 PM 242.3 64.6
5/22/2019 4:47:30 PM 242.2 64.5
5/22/2019 4:47:31 PM 242.2 64.5
5/22/2019 4:47:32 PM 242.2 64.5
Page 277 of 452 August 2019
APPENDIX E47: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-4 Data Log
5/22/2019 4:47:33 PM 242.2 64.5
5/22/2019 4:47:34 PM 242.3 64.6
5/22/2019 4:47:35 PM 242.4 64.7
5/22/2019 4:47:36 PM 242.5 64.8
5/22/2019 4:47:37 PM 242.7 65.0
5/22/2019 4:47:38 PM 242.9 65.2
5/22/2019 4:47:39 PM 243.1 65.4
5/22/2019 4:47:40 PM 243.4 65.7
5/22/2019 4:47:41 PM 243.7 66.0
5/22/2019 4:47:42 PM 243.9 66.2
5/22/2019 4:47:43 PM 244.2 66.5
5/22/2019 4:47:44 PM 244.4 66.7
5/22/2019 4:47:45 PM 244.7 67.0
5/22/2019 4:47:46 PM 244.9 67.2
5/22/2019 4:47:47 PM 245.1 67.4
5/22/2019 4:47:48 PM 245.3 67.6
5/22/2019 4:47:49 PM 245.4 67.7
5/22/2019 4:47:50 PM 245.5 67.8
5/22/2019 4:47:51 PM 245.5 67.8
5/22/2019 4:47:52 PM 245.6 67.9
5/22/2019 4:47:53 PM 245.6 67.9
5/22/2019 4:47:54 PM 245.5 67.8
5/22/2019 4:47:55 PM 245.5 67.8
5/22/2019 4:47:56 PM 245.4 67.7
5/22/2019 4:47:57 PM 245.2 67.5
5/22/2019 4:47:58 PM 245.0 67.3
5/22/2019 4:47:59 PM 244.8 67.1
5/22/2019 4:48:00 PM 244.6 66.9
5/22/2019 4:48:01 PM 244.4 66.7
5/22/2019 4:48:02 PM 244.1 66.4
5/22/2019 4:48:03 PM 243.9 66.2
5/22/2019 4:48:04 PM 243.5 65.8
5/22/2019 4:48:05 PM 243.3 65.6
5/22/2019 4:48:06 PM 242.9 65.2
5/22/2019 4:48:07 PM 242.7 65.0
5/22/2019 4:48:08 PM 242.3 64.6
5/22/2019 4:48:09 PM 242.0 64.3
5/22/2019 4:48:10 PM 241.7 64.0
5/22/2019 4:48:11 PM 241.4 63.7
5/22/2019 4:48:12 PM 241.1 63.4
5/22/2019 4:48:13 PM 240.8 63.1
5/22/2019 4:48:14 PM 240.4 62.7
5/22/2019 4:48:15 PM 240.1 62.4
5/22/2019 4:48:16 PM 239.7 62.0
5/22/2019 4:48:17 PM 239.4 61.7
5/22/2019 4:48:18 PM 239.1 61.4
5/22/2019 4:48:19 PM 238.8 61.1
5/22/2019 4:48:20 PM 238.4 60.7
5/22/2019 4:48:21 PM 238.1 60.4
5/22/2019 4:48:22 PM 237.7 60.0
5/22/2019 4:48:23 PM 237.4 59.7
5/22/2019 4:48:24 PM 237.0 59.3
5/22/2019 4:48:25 PM 236.7 59.0
5/22/2019 4:48:26 PM 236.4 58.7
5/22/2019 4:48:27 PM 236.0 58.3
5/22/2019 4:48:28 PM 235.7 58.0
5/22/2019 4:48:29 PM 235.4 57.7
5/22/2019 4:48:30 PM 235.1 57.4
5/22/2019 4:48:31 PM 234.8 57.1
5/22/2019 4:48:32 PM 234.5 56.8
5/22/2019 4:48:33 PM 234.1 56.4
5/22/2019 4:48:34 PM 233.8 56.1
5/22/2019 4:48:35 PM 233.5 55.8
5/22/2019 4:48:36 PM 233.2 55.5
5/22/2019 4:48:37 PM 232.9 55.2
5/22/2019 4:48:38 PM 232.6 54.9
5/22/2019 4:48:39 PM 232.3 54.6
5/22/2019 4:48:40 PM 232.0 54.3
5/22/2019 4:48:41 PM 231.7 54.0
5/22/2019 4:48:42 PM 231.4 53.7
5/22/2019 4:48:43 PM 231.1 53.4
5/22/2019 4:48:44 PM 230.8 53.1
5/22/2019 4:48:45 PM 230.6 52.9
5/22/2019 4:48:46 PM 230.3 52.6
5/22/2019 4:48:47 PM 230.1 52.4
5/22/2019 4:48:48 PM 229.9 52.2
5/22/2019 4:48:49 PM 229.7 52.0
5/22/2019 4:48:50 PM 229.4 51.7
5/22/2019 4:48:51 PM 229.2 51.5
Page 278 of 452 August 2019
APPENDIX E47: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-4 Data Log
5/22/2019 4:48:52 PM 229.0 51.3
5/22/2019 4:48:53 PM 228.8 51.1
5/22/2019 4:48:54 PM 228.6 50.9
5/22/2019 4:48:55 PM 228.4 50.7
5/22/2019 4:48:56 PM 228.2 50.5
5/22/2019 4:48:57 PM 228.0 50.3
5/22/2019 4:48:58 PM 227.8 50.1
5/22/2019 4:48:59 PM 227.6 49.9
5/22/2019 4:49:00 PM 227.4 49.7
5/22/2019 4:49:01 PM 227.2 49.5
5/22/2019 4:49:02 PM 227.1 49.4
5/22/2019 4:49:03 PM 226.9 49.2
5/22/2019 4:49:04 PM 226.7 49.0
5/22/2019 4:49:05 PM 226.6 48.9
5/22/2019 4:49:06 PM 226.4 48.7
5/22/2019 4:49:07 PM 226.3 48.6
5/22/2019 4:49:08 PM 226.1 48.4
5/22/2019 4:49:09 PM 226.0 48.3
5/22/2019 4:49:10 PM 225.8 48.1
5/22/2019 4:49:11 PM 225.6 47.9
5/22/2019 4:49:12 PM 225.5 47.8
5/22/2019 4:49:13 PM 225.3 47.6
5/22/2019 4:49:14 PM 225.2 47.5
5/22/2019 4:49:15 PM 225.0 47.3
5/22/2019 4:49:16 PM 224.9 47.2
5/22/2019 4:49:17 PM 224.7 47.0
5/22/2019 4:49:18 PM 224.6 46.9
5/22/2019 4:49:19 PM 224.4 46.7
5/22/2019 4:49:20 PM 224.3 46.6
5/22/2019 4:49:21 PM 224.1 46.4
5/22/2019 4:49:22 PM 224.0 46.3
5/22/2019 4:49:23 PM 223.9 46.2
5/22/2019 4:49:24 PM 223.7 46.0
5/22/2019 4:49:25 PM 223.6 45.9
5/22/2019 4:49:26 PM 223.5 45.8
5/22/2019 4:49:27 PM 223.4 45.7
5/22/2019 4:49:28 PM 223.3 45.6
5/22/2019 4:49:29 PM 223.1 45.4
5/22/2019 4:49:30 PM 223.0 45.3
5/22/2019 4:49:31 PM 222.9 45.2
5/22/2019 4:49:32 PM 222.8 45.1
5/22/2019 4:49:33 PM 222.7 45.0
5/22/2019 4:49:34 PM 222.5 44.8
5/22/2019 4:49:35 PM 222.4 44.7
5/22/2019 4:49:36 PM 222.3 44.6
5/22/2019 4:49:37 PM 222.1 44.4
5/22/2019 4:49:38 PM 222.0 44.3
5/22/2019 4:49:39 PM 221.9 44.2
5/22/2019 4:49:40 PM 221.7 44.0
5/22/2019 4:49:41 PM 221.6 43.9
5/22/2019 4:49:42 PM 221.5 43.8
5/22/2019 4:49:43 PM 221.4 43.7
5/22/2019 4:49:44 PM 221.2 43.5
5/22/2019 4:49:45 PM 221.1 43.4
5/22/2019 4:49:46 PM 221.0 43.3
5/22/2019 4:49:47 PM 220.8 43.1
5/22/2019 4:49:48 PM 220.7 43.0
5/22/2019 4:49:49 PM 220.5 42.8
5/22/2019 4:49:50 PM 220.4 42.7
5/22/2019 4:49:51 PM 220.2 42.5
5/22/2019 4:49:52 PM 220.1 42.4
5/22/2019 4:49:53 PM 219.9 42.2
5/22/2019 4:49:54 PM 219.8 42.1
5/22/2019 4:49:55 PM 219.6 41.9
5/22/2019 4:49:56 PM 219.5 41.8
5/22/2019 4:49:57 PM 219.3 41.6
5/22/2019 4:49:58 PM 219.1 41.4
5/22/2019 4:49:59 PM 219.0 41.3
5/22/2019 4:50:00 PM 218.9 41.2
5/22/2019 4:50:01 PM 218.7 41.0
5/22/2019 4:50:02 PM 218.6 40.9
5/22/2019 4:50:03 PM 218.5 40.8
5/22/2019 4:50:04 PM 218.3 40.6
5/22/2019 4:50:05 PM 218.2 40.5
5/22/2019 4:50:06 PM 218.1 40.4
5/22/2019 4:50:07 PM 217.9 40.2
5/22/2019 4:50:08 PM 217.8 40.1
5/22/2019 4:50:09 PM 217.6 39.9
5/22/2019 4:50:10 PM 217.5 39.8
Page 279 of 452 August 2019
APPENDIX E47: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-4 Data Log
5/22/2019 4:50:11 PM 217.4 39.7
5/22/2019 4:50:12 PM 217.2 39.5
5/22/2019 4:50:13 PM 217.1 39.4
5/22/2019 4:50:14 PM 217.0 39.3
5/22/2019 4:50:15 PM 216.9 39.2
5/22/2019 4:50:16 PM 216.7 39.0
5/22/2019 4:50:17 PM 216.6 38.9
5/22/2019 4:50:18 PM 216.5 38.8
5/22/2019 4:50:19 PM 216.4 38.7
5/22/2019 4:50:20 PM 216.3 38.6
5/22/2019 4:50:21 PM 216.2 38.5
5/22/2019 4:50:22 PM 216.1 38.4
5/22/2019 4:50:23 PM 216.0 38.3
5/22/2019 4:50:24 PM 215.9 38.2
5/22/2019 4:50:25 PM 215.8 38.1
5/22/2019 4:50:26 PM 215.7 38.0
5/22/2019 4:50:27 PM 215.6 37.9
5/22/2019 4:50:28 PM 215.5 37.8
5/22/2019 4:50:29 PM 215.4 37.7
5/22/2019 4:50:30 PM 215.3 37.6
5/22/2019 4:50:31 PM 215.2 37.5
5/22/2019 4:50:32 PM 215.1 37.4
5/22/2019 4:50:33 PM 215.0 37.3
5/22/2019 4:50:34 PM 214.9 37.2
5/22/2019 4:50:35 PM 214.7 37.0
5/22/2019 4:50:36 PM 214.6 36.9
5/22/2019 4:50:37 PM 214.5 36.8
5/22/2019 4:50:38 PM 214.4 36.7
5/22/2019 4:50:39 PM 214.2 36.5
5/22/2019 4:50:40 PM 214.1 36.4
5/22/2019 4:50:41 PM 214.0 36.3
5/22/2019 4:50:42 PM 213.9 36.2
5/22/2019 4:50:43 PM 213.8 36.1
5/22/2019 4:50:44 PM 213.7 36.0
5/22/2019 4:50:45 PM 213.6 35.9
5/22/2019 4:50:46 PM 213.5 35.8
5/22/2019 4:50:47 PM 213.4 35.7
5/22/2019 4:50:48 PM 213.3 35.6
5/22/2019 4:50:49 PM 213.2 35.5
5/22/2019 4:50:50 PM 213.1 35.4
5/22/2019 4:50:51 PM 213.0 35.3
5/22/2019 4:50:52 PM 212.9 35.2
5/22/2019 4:50:53 PM 212.8 35.1
5/22/2019 4:50:54 PM 212.7 35.0
5/22/2019 4:50:55 PM 212.6 34.9
5/22/2019 4:50:56 PM 212.5 34.8
5/22/2019 4:50:57 PM 212.4 34.7
5/22/2019 4:50:58 PM 212.3 34.6
5/22/2019 4:50:59 PM 212.2 34.5
5/22/2019 4:51:00 PM 212.1 34.4
5/22/2019 4:51:01 PM 212.0 34.3
5/22/2019 4:51:02 PM 211.9 34.2
5/22/2019 4:51:03 PM 211.8 34.1
5/22/2019 4:51:04 PM 211.7 34.0
5/22/2019 4:51:05 PM 211.5 33.8
5/22/2019 4:51:06 PM 211.4 33.7
5/22/2019 4:51:07 PM 211.3 33.6
5/22/2019 4:51:08 PM 211.2 33.5
5/22/2019 4:51:09 PM 211.1 33.4
5/22/2019 4:51:10 PM 211.0 33.3
5/22/2019 4:51:11 PM 210.9 33.2
5/22/2019 4:51:12 PM 210.8 33.1
5/22/2019 4:51:13 PM 210.7 33.0
5/22/2019 4:51:14 PM 210.6 32.9
5/22/2019 4:51:15 PM 210.5 32.8
5/22/2019 4:51:16 PM 210.4 32.7
5/22/2019 4:51:17 PM 210.3 32.6
5/22/2019 4:51:18 PM 210.2 32.5
5/22/2019 4:51:19 PM 210.1 32.4
5/22/2019 4:51:20 PM 210.0 32.3
5/22/2019 4:51:21 PM 210.0 32.3
5/22/2019 4:51:22 PM 209.9 32.2
5/22/2019 4:51:23 PM 209.8 32.1
5/22/2019 4:51:24 PM 209.7 32.0
5/22/2019 4:51:25 PM 209.6 31.9
5/22/2019 4:51:26 PM 209.6 31.9
5/22/2019 4:51:27 PM 209.5 31.8
5/22/2019 4:51:28 PM 209.4 31.7
5/22/2019 4:51:29 PM 209.3 31.6
Page 280 of 452 August 2019
APPENDIX E47: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-4 Data Log
5/22/2019 4:51:30 PM 209.2 31.5
5/22/2019 4:51:31 PM 209.2 31.5
5/22/2019 4:51:32 PM 209.1 31.4
5/22/2019 4:51:33 PM 209.0 31.3
5/22/2019 4:51:34 PM 208.9 31.2
5/22/2019 4:51:35 PM 208.8 31.1
5/22/2019 4:51:36 PM 208.6 30.9
5/22/2019 4:51:37 PM 208.5 30.8
5/22/2019 4:51:38 PM 208.4 30.7
5/22/2019 4:51:39 PM 208.3 30.6
5/22/2019 4:51:40 PM 208.2 30.5
5/22/2019 4:51:41 PM 208.1 30.4
5/22/2019 4:51:42 PM 208.0 30.3
5/22/2019 4:51:43 PM 207.9 30.2
5/22/2019 4:51:44 PM 207.8 30.1
5/22/2019 4:51:45 PM 207.7 30.0
5/22/2019 4:51:46 PM 207.6 29.9
5/22/2019 4:51:47 PM 207.5 29.8
5/22/2019 4:51:48 PM 207.4 29.7
5/22/2019 4:51:49 PM 207.3 29.6
5/22/2019 4:51:50 PM 207.2 29.5
5/22/2019 4:51:51 PM 207.1 29.4
5/22/2019 4:51:52 PM 207.0 29.3
5/22/2019 4:51:53 PM 206.9 29.2
5/22/2019 4:51:54 PM 206.9 29.2
5/22/2019 4:51:55 PM 206.8 29.1
5/22/2019 4:51:56 PM 206.7 29.0
5/22/2019 4:51:57 PM 206.6 28.9
5/22/2019 4:51:58 PM 206.6 28.9
5/22/2019 4:51:59 PM 206.5 28.8
5/22/2019 4:52:00 PM 206.5 28.8
5/22/2019 4:52:01 PM 206.4 28.7
5/22/2019 4:52:02 PM 206.4 28.7
5/22/2019 4:52:03 PM 206.3 28.6
5/22/2019 4:52:04 PM 206.3 28.6
5/22/2019 4:52:05 PM 206.2 28.5
5/22/2019 4:52:06 PM 206.2 28.5
5/22/2019 4:52:07 PM 206.1 28.4
5/22/2019 4:52:08 PM 206.1 28.4
5/22/2019 4:52:09 PM 206.0 28.3
5/22/2019 4:52:10 PM 206.0 28.3
5/22/2019 4:52:11 PM 206.0 28.3
5/22/2019 4:52:12 PM 205.9 28.2
5/22/2019 4:52:13 PM 205.8 28.1
5/22/2019 4:52:14 PM 205.8 28.1
5/22/2019 4:52:15 PM 205.7 28.0
5/22/2019 4:52:16 PM 205.7 28.0
5/22/2019 4:52:17 PM 205.6 27.9
5/22/2019 4:52:18 PM 205.6 27.9
5/22/2019 4:52:19 PM 205.5 27.8
5/22/2019 4:52:20 PM 205.5 27.8
5/22/2019 4:52:21 PM 205.4 27.7
5/22/2019 4:52:22 PM 205.4 27.7
5/22/2019 4:52:23 PM 205.3 27.6
5/22/2019 4:52:24 PM 205.3 27.6
5/22/2019 4:52:25 PM 205.2 27.5
5/22/2019 4:52:26 PM 205.2 27.5
5/22/2019 4:52:27 PM 205.1 27.4
5/22/2019 4:52:28 PM 205.1 27.4
5/22/2019 4:52:29 PM 205.0 27.3
5/22/2019 4:52:30 PM 205.0 27.3
5/22/2019 4:52:31 PM 204.9 27.2
5/22/2019 4:52:32 PM 204.8 27.1
5/22/2019 4:52:33 PM 204.8 27.1
5/22/2019 4:52:34 PM 204.7 27.0
5/22/2019 4:52:35 PM 204.6 26.9
5/22/2019 4:52:36 PM 204.6 26.9
5/22/2019 4:52:37 PM 204.5 26.8
5/22/2019 4:52:38 PM 204.4 26.7
5/22/2019 4:52:39 PM 204.4 26.7
5/22/2019 4:52:40 PM 204.3 26.6
5/22/2019 4:52:41 PM 204.2 26.5
5/22/2019 4:52:42 PM 204.1 26.4
5/22/2019 4:52:43 PM 204.1 26.4
5/22/2019 4:52:44 PM 204.0 26.3
5/22/2019 4:52:45 PM 203.9 26.2
5/22/2019 4:52:46 PM 203.8 26.1
5/22/2019 4:52:47 PM 203.8 26.1
5/22/2019 4:52:48 PM 203.7 26.0
Page 281 of 452 August 2019
APPENDIX E47: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-4 Data Log
5/22/2019 4:52:49 PM 203.6 25.9
5/22/2019 4:52:50 PM 203.5 25.8
5/22/2019 4:52:51 PM 203.4 25.7
5/22/2019 4:52:52 PM 203.3 25.6
5/22/2019 4:52:53 PM 203.3 25.6
5/22/2019 4:52:54 PM 203.2 25.5
5/22/2019 4:52:55 PM 203.1 25.4
5/22/2019 4:52:56 PM 203.0 25.3
5/22/2019 4:52:57 PM 203.0 25.3
5/22/2019 4:52:58 PM 202.9 25.2
5/22/2019 4:52:59 PM 202.8 25.1
5/22/2019 4:53:00 PM 202.8 25.1
5/22/2019 4:53:01 PM 202.7 25.0
5/22/2019 4:53:02 PM 202.7 25.0
5/22/2019 4:53:03 PM 202.6 24.9
5/22/2019 4:53:04 PM 202.6 24.9
5/22/2019 4:53:05 PM 202.5 24.8
5/22/2019 4:53:06 PM 202.5 24.8
5/22/2019 4:53:07 PM 202.4 24.7
5/22/2019 4:53:08 PM 202.4 24.7
5/22/2019 4:53:09 PM 202.3 24.6
5/22/2019 4:53:10 PM 202.3 24.6
5/22/2019 4:53:11 PM 202.3 24.6
5/22/2019 4:53:12 PM 202.2 24.5
5/22/2019 4:53:13 PM 202.2 24.5
5/22/2019 4:53:14 PM 202.2 24.5
5/22/2019 4:53:15 PM 202.1 24.4
5/22/2019 4:53:16 PM 202.1 24.4
5/22/2019 4:53:17 PM 202.0 24.3
5/22/2019 4:53:18 PM 202.0 24.3
5/22/2019 4:53:19 PM 202.0 24.3
5/22/2019 4:53:20 PM 201.9 24.2
5/22/2019 4:53:21 PM 201.9 24.2
5/22/2019 4:53:22 PM 201.9 24.2
5/22/2019 4:53:23 PM 201.8 24.1
5/22/2019 4:53:24 PM 201.8 24.1
5/22/2019 4:53:25 PM 201.7 24.0
5/22/2019 4:53:26 PM 201.6 23.9
5/22/2019 4:53:27 PM 201.6 23.9
5/22/2019 4:53:28 PM 201.6 23.9
5/22/2019 4:53:29 PM 201.5 23.8
5/22/2019 4:53:30 PM 201.5 23.8
5/22/2019 4:53:31 PM 201.4 23.7
5/22/2019 4:53:32 PM 201.4 23.7
5/22/2019 4:53:33 PM 201.3 23.6
5/22/2019 4:53:34 PM 201.3 23.6
5/22/2019 4:53:35 PM 201.2 23.5
5/22/2019 4:53:36 PM 201.2 23.5
5/22/2019 4:53:37 PM 201.1 23.4
5/22/2019 4:53:38 PM 201.0 23.3
5/22/2019 4:53:39 PM 201.0 23.3
5/22/2019 4:53:40 PM 201.0 23.3
5/22/2019 4:53:41 PM 200.9 23.2
5/22/2019 4:53:42 PM 200.9 23.2
5/22/2019 4:53:43 PM 200.8 23.1
5/22/2019 4:53:44 PM 200.8 23.1
5/22/2019 4:53:45 PM 200.8 23.1
5/22/2019 4:53:46 PM 200.8 23.1
5/22/2019 4:53:47 PM 200.7 23.0
5/22/2019 4:53:48 PM 200.7 23.0
5/22/2019 4:53:49 PM 200.7 23.0
5/22/2019 4:53:50 PM 200.7 23.0
5/22/2019 4:53:51 PM 200.7 23.0
5/22/2019 4:53:52 PM 200.7 23.0
5/22/2019 4:53:53 PM 200.7 23.0
5/22/2019 4:53:54 PM 200.7 23.0
5/22/2019 4:53:55 PM 200.7 23.0
5/22/2019 4:53:56 PM 200.7 23.0
5/22/2019 4:53:57 PM 200.6 22.9
5/22/2019 4:53:58 PM 200.6 22.9
5/22/2019 4:53:59 PM 200.6 22.9
5/22/2019 4:54:00 PM 200.6 22.9
5/22/2019 4:54:01 PM 200.6 22.9
5/22/2019 4:54:02 PM 200.5 22.8
5/22/2019 4:54:03 PM 200.5 22.8
5/22/2019 4:54:04 PM 200.5 22.8
5/22/2019 4:54:05 PM 200.4 22.7
5/22/2019 4:54:06 PM 200.4 22.7
5/22/2019 4:54:07 PM 200.3 22.6
Page 282 of 452 August 2019
APPENDIX E47: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-4 Data Log
5/22/2019 4:54:08 PM 200.2 22.5
5/22/2019 4:54:09 PM 200.1 22.4
5/22/2019 4:54:10 PM 200.0 22.3
5/22/2019 4:54:11 PM 200.0 22.3
5/22/2019 4:54:12 PM 199.9 22.2
5/22/2019 4:54:13 PM 199.9 22.2
5/22/2019 4:54:14 PM 199.8 22.1
5/22/2019 4:54:15 PM 199.7 22.0
5/22/2019 4:54:16 PM 199.7 22.0
5/22/2019 4:54:17 PM 199.6 21.9
5/22/2019 4:54:18 PM 199.6 21.9
5/22/2019 4:54:19 PM 199.6 21.9
5/22/2019 4:54:20 PM 199.5 21.8
5/22/2019 4:54:21 PM 199.5 21.8
5/22/2019 4:54:22 PM 199.5 21.8
5/22/2019 4:54:23 PM 199.5 21.8
5/22/2019 4:54:24 PM 199.5 21.8
5/22/2019 4:54:25 PM 199.5 21.8
5/22/2019 4:54:26 PM 199.5 21.8
5/22/2019 4:54:27 PM 199.4 21.7
5/22/2019 4:54:28 PM 199.4 21.7
5/22/2019 4:54:29 PM 199.4 21.7
5/22/2019 4:54:30 PM 199.3 21.6
5/22/2019 4:54:31 PM 199.3 21.6
5/22/2019 4:54:32 PM 199.3 21.6
5/22/2019 4:54:33 PM 199.2 21.5
5/22/2019 4:54:34 PM 199.1 21.4
5/22/2019 4:54:35 PM 199.0 21.3
5/22/2019 4:54:36 PM 199.0 21.3
5/22/2019 4:54:37 PM 198.9 21.2
5/22/2019 4:54:38 PM 198.8 21.1
5/22/2019 4:54:39 PM 198.8 21.1
5/22/2019 4:54:40 PM 198.7 21.0
5/22/2019 4:54:41 PM 198.7 21.0
5/22/2019 4:54:42 PM 198.6 20.9
5/22/2019 4:54:43 PM 198.6 20.9
5/22/2019 4:54:44 PM 198.5 20.8
5/22/2019 4:54:45 PM 198.5 20.8
5/22/2019 4:54:46 PM 198.4 20.7
5/22/2019 4:54:47 PM 198.4 20.7
5/22/2019 4:54:48 PM 198.4 20.7
5/22/2019 4:54:49 PM 198.4 20.7
5/22/2019 4:54:50 PM 198.3 20.6
5/22/2019 4:54:51 PM 198.3 20.6
5/22/2019 4:54:52 PM 198.2 20.5
5/22/2019 4:54:53 PM 198.2 20.5
5/22/2019 4:54:54 PM 198.1 20.4
5/22/2019 4:54:55 PM 198.1 20.4
5/22/2019 4:54:56 PM 198.0 20.3
5/22/2019 4:54:57 PM 197.9 20.2
5/22/2019 4:54:58 PM 197.8 20.1
5/22/2019 4:54:59 PM 197.8 20.1
5/22/2019 4:55:00 PM 197.7 20.0
5/22/2019 4:55:01 PM 197.6 19.9
5/22/2019 4:55:02 PM 197.5 19.8
5/22/2019 4:55:03 PM 197.4 19.7
5/22/2019 4:55:04 PM 197.4 19.7
5/22/2019 4:55:05 PM 197.3 19.6
5/22/2019 4:55:06 PM 197.2 19.5
5/22/2019 4:55:07 PM 197.2 19.5
5/22/2019 4:55:08 PM 197.1 19.4
5/22/2019 4:55:09 PM 197.0 19.3
5/22/2019 4:55:10 PM 197.0 19.3
5/22/2019 4:55:11 PM 196.9 19.2
5/22/2019 4:55:12 PM 196.9 19.2
5/22/2019 4:55:13 PM 196.8 19.1
5/22/2019 4:55:14 PM 196.8 19.1
5/22/2019 4:55:15 PM 196.7 19.0
5/22/2019 4:55:16 PM 196.7 19.0
5/22/2019 4:55:17 PM 196.7 19.0
5/22/2019 4:55:18 PM 196.6 18.9
5/22/2019 4:55:19 PM 196.6 18.9
5/22/2019 4:55:20 PM 196.5 18.8
5/22/2019 4:55:21 PM 196.5 18.8
5/22/2019 4:55:22 PM 196.5 18.8
5/22/2019 4:55:23 PM 196.5 18.8
5/22/2019 4:55:24 PM 196.4 18.7
5/22/2019 4:55:25 PM 196.4 18.7
5/22/2019 4:55:26 PM 196.4 18.7
Page 283 of 452 August 2019
APPENDIX E47: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-4 Data Log
5/22/2019 4:55:27 PM 196.4 18.7
5/22/2019 4:55:28 PM 196.3 18.6
5/22/2019 4:55:29 PM 196.3 18.6
5/22/2019 4:55:30 PM 196.3 18.6
5/22/2019 4:55:31 PM 196.3 18.6
5/22/2019 4:55:32 PM 196.2 18.5
5/22/2019 4:55:33 PM 196.2 18.5
5/22/2019 4:55:34 PM 196.2 18.5
5/22/2019 4:55:35 PM 196.2 18.5
5/22/2019 4:55:36 PM 196.1 18.4
5/22/2019 4:55:37 PM 196.1 18.4
5/22/2019 4:55:38 PM 196.1 18.4
5/22/2019 4:55:39 PM 196.1 18.4
5/22/2019 4:55:40 PM 196.1 18.4
5/22/2019 4:55:41 PM 196.0 18.3
5/22/2019 4:55:42 PM 196.0 18.3
5/22/2019 4:55:43 PM 195.9 18.2
5/22/2019 4:55:44 PM 195.9 18.2
5/22/2019 4:55:45 PM 195.8 18.1
5/22/2019 4:55:46 PM 195.8 18.1
5/22/2019 4:55:47 PM 195.7 18.0
5/22/2019 4:55:48 PM 195.7 18.0
5/22/2019 4:55:49 PM 195.6 17.9
5/22/2019 4:55:50 PM 195.6 17.9
5/22/2019 4:55:51 PM 195.6 17.9
5/22/2019 4:55:52 PM 195.5 17.8
5/22/2019 4:55:53 PM 195.5 17.8
5/22/2019 4:55:54 PM 195.5 17.8
5/22/2019 4:55:55 PM 195.5 17.8
5/22/2019 4:55:56 PM 195.4 17.7
5/22/2019 4:55:57 PM 195.4 17.7
5/22/2019 4:55:58 PM 195.4 17.7
5/22/2019 4:55:59 PM 195.4 17.7
5/22/2019 4:56:00 PM 195.4 17.7
5/22/2019 4:56:01 PM 195.3 17.6
5/22/2019 4:56:02 PM 195.3 17.6
5/22/2019 4:56:03 PM 195.3 17.6
5/22/2019 4:56:04 PM 195.3 17.6
5/22/2019 4:56:05 PM 195.2 17.5
5/22/2019 4:56:06 PM 195.2 17.5
5/22/2019 4:56:07 PM 195.2 17.5
5/22/2019 4:56:08 PM 195.2 17.5
5/22/2019 4:56:09 PM 195.2 17.5
5/22/2019 4:56:10 PM 195.2 17.5
5/22/2019 4:56:11 PM 195.2 17.5
5/22/2019 4:56:12 PM 195.2 17.5
5/22/2019 4:56:13 PM 195.1 17.4
5/22/2019 4:56:14 PM 195.1 17.4
5/22/2019 4:56:15 PM 195.1 17.4
5/22/2019 4:56:16 PM 195.1 17.4
5/22/2019 4:56:17 PM 195.0 17.3
5/22/2019 4:56:18 PM 195.0 17.3
5/22/2019 4:56:19 PM 195.0 17.3
5/22/2019 4:56:20 PM 194.9 17.2
5/22/2019 4:56:21 PM 194.9 17.2
5/22/2019 4:56:22 PM 194.9 17.2
5/22/2019 4:56:23 PM 194.8 17.1
5/22/2019 4:56:24 PM 194.8 17.1
5/22/2019 4:56:25 PM 194.7 17.0
5/22/2019 4:56:26 PM 194.7 17.0
5/22/2019 4:56:27 PM 194.7 17.0
5/22/2019 4:56:28 PM 194.6 16.9
5/22/2019 4:56:29 PM 194.6 16.9
5/22/2019 4:56:30 PM 194.6 16.9
5/22/2019 4:56:31 PM 194.5 16.8
5/22/2019 4:56:32 PM 194.5 16.8
5/22/2019 4:56:33 PM 194.4 16.7
5/22/2019 4:56:34 PM 194.4 16.7
5/22/2019 4:56:35 PM 194.4 16.7
5/22/2019 4:56:36 PM 194.3 16.6
5/22/2019 4:56:37 PM 194.3 16.6
5/22/2019 4:56:38 PM 194.2 16.5
5/22/2019 4:56:39 PM 194.2 16.5
5/22/2019 4:56:40 PM 194.1 16.4
5/22/2019 4:56:41 PM 194.1 16.4
5/22/2019 4:56:42 PM 194.0 16.3
5/22/2019 4:56:43 PM 193.9 16.2
5/22/2019 4:56:44 PM 193.8 16.1
5/22/2019 4:56:45 PM 193.8 16.1
Page 284 of 452 August 2019
APPENDIX E47: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-4 Data Log
5/22/2019 4:56:46 PM 193.7 16.0
5/22/2019 4:56:47 PM 193.6 15.9
5/22/2019 4:56:48 PM 193.5 15.8
5/22/2019 4:56:49 PM 193.5 15.8
5/22/2019 4:56:50 PM 193.4 15.7
5/22/2019 4:56:51 PM 193.3 15.6
5/22/2019 4:56:52 PM 193.2 15.5
5/22/2019 4:56:53 PM 193.2 15.5
5/22/2019 4:56:54 PM 193.1 15.4
5/22/2019 4:56:55 PM 193.1 15.4
5/22/2019 4:56:56 PM 193.0 15.3
5/22/2019 4:56:57 PM 193.0 15.3
5/22/2019 4:56:58 PM 193.0 15.3
5/22/2019 4:56:59 PM 192.9 15.2
5/22/2019 4:57:00 PM 192.9 15.2
5/22/2019 4:57:01 PM 192.9 15.2
5/22/2019 4:57:02 PM 192.8 15.1
5/22/2019 4:57:03 PM 192.8 15.1
5/22/2019 4:57:04 PM 192.8 15.1
5/22/2019 4:57:05 PM 192.7 15.0
5/22/2019 4:57:06 PM 192.7 15.0
5/22/2019 4:57:07 PM 192.7 15.0
5/22/2019 4:57:08 PM 192.7 15.0
5/22/2019 4:57:09 PM 192.7 15.0
5/22/2019 4:57:10 PM 192.7 15.0
5/22/2019 4:57:11 PM 192.7 15.0
5/22/2019 4:57:12 PM 192.7 15.0
5/22/2019 4:57:13 PM 192.7 15.0
5/22/2019 4:57:14 PM 192.7 15.0
5/22/2019 4:57:15 PM 192.6 14.9
5/22/2019 4:57:16 PM 192.6 14.9
5/22/2019 4:57:17 PM 192.6 14.9
5/22/2019 4:57:18 PM 192.6 14.9
5/22/2019 4:57:19 PM 192.6 14.9
5/22/2019 4:57:20 PM 192.5 14.8
5/22/2019 4:57:21 PM 192.5 14.8
5/22/2019 4:57:22 PM 192.4 14.7
5/22/2019 4:57:23 PM 192.4 14.7
5/22/2019 4:57:24 PM 192.4 14.7
5/22/2019 4:57:25 PM 192.3 14.6
5/22/2019 4:57:26 PM 192.3 14.6
5/22/2019 4:57:27 PM 192.3 14.6
5/22/2019 4:57:28 PM 192.2 14.5
5/22/2019 4:57:29 PM 192.2 14.5
5/22/2019 4:57:30 PM 192.2 14.5
5/22/2019 4:57:31 PM 192.1 14.4
5/22/2019 4:57:32 PM 192.1 14.4
5/22/2019 4:57:33 PM 192.0 14.3
5/22/2019 4:57:34 PM 191.9 14.2
5/22/2019 4:57:35 PM 191.9 14.2
5/22/2019 4:57:36 PM 191.8 14.1
5/22/2019 4:57:37 PM 191.8 14.1
5/22/2019 4:57:38 PM 191.7 14.0
5/22/2019 4:57:39 PM 191.6 13.9
5/22/2019 4:57:40 PM 191.6 13.9
5/22/2019 4:57:41 PM 191.5 13.8
5/22/2019 4:57:42 PM 191.5 13.8
5/22/2019 4:57:43 PM 191.4 13.7
5/22/2019 4:57:44 PM 191.4 13.7
5/22/2019 4:57:45 PM 191.4 13.7
5/22/2019 4:57:46 PM 191.3 13.6
5/22/2019 4:57:47 PM 191.3 13.6
5/22/2019 4:57:48 PM 191.3 13.6
5/22/2019 4:57:49 PM 191.2 13.5
5/22/2019 4:57:50 PM 191.2 13.5
5/22/2019 4:57:51 PM 191.2 13.5
5/22/2019 4:57:52 PM 191.1 13.4
5/22/2019 4:57:53 PM 191.1 13.4
5/22/2019 4:57:54 PM 191.1 13.4
5/22/2019 4:57:55 PM 191.0 13.3
5/22/2019 4:57:56 PM 191.0 13.3
5/22/2019 4:57:57 PM 191.0 13.3
5/22/2019 4:57:58 PM 190.9 13.2
5/22/2019 4:57:59 PM 190.9 13.2
5/22/2019 4:58:00 PM 190.9 13.2
5/22/2019 4:58:01 PM 190.9 13.2
5/22/2019 4:58:02 PM 190.8 13.1
5/22/2019 4:58:03 PM 190.8 13.1
5/22/2019 4:58:04 PM 190.8 13.1
Page 285 of 452 August 2019
APPENDIX E47: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-4 Data Log
5/22/2019 4:58:05 PM 190.7 13.0
5/22/2019 4:58:06 PM 190.7 13.0
5/22/2019 4:58:07 PM 190.7 13.0
5/22/2019 4:58:08 PM 190.6 12.9
5/22/2019 4:58:09 PM 190.6 12.9
5/22/2019 4:58:10 PM 190.6 12.9
5/22/2019 4:58:11 PM 190.5 12.8
5/22/2019 4:58:12 PM 190.5 12.8
5/22/2019 4:58:13 PM 190.5 12.8
5/22/2019 4:58:14 PM 190.5 12.8
5/22/2019 4:58:15 PM 190.4 12.7
5/22/2019 4:58:16 PM 190.4 12.7
5/22/2019 4:58:17 PM 190.4 12.7
5/22/2019 4:58:18 PM 190.3 12.6
5/22/2019 4:58:19 PM 190.3 12.6
5/22/2019 4:58:20 PM 190.3 12.6
5/22/2019 4:58:21 PM 190.3 12.6
5/22/2019 4:58:22 PM 190.2 12.5
5/22/2019 4:58:23 PM 190.2 12.5
5/22/2019 4:58:24 PM 190.2 12.5
5/22/2019 4:58:25 PM 190.1 12.4
5/22/2019 4:58:26 PM 190.1 12.4
5/22/2019 4:58:27 PM 190.1 12.4
5/22/2019 4:58:28 PM 190.0 12.3
5/22/2019 4:58:29 PM 190.0 12.3
5/22/2019 4:58:30 PM 190.0 12.3
5/22/2019 4:58:31 PM 189.9 12.2
5/22/2019 4:58:32 PM 189.9 12.2
5/22/2019 4:58:33 PM 189.9 12.2
5/22/2019 4:58:34 PM 189.9 12.2
5/22/2019 4:58:35 PM 189.9 12.2
5/22/2019 4:58:36 PM 189.8 12.1
5/22/2019 4:58:37 PM 189.8 12.1
5/22/2019 4:58:38 PM 189.8 12.1
5/22/2019 4:58:39 PM 189.7 12.0
5/22/2019 4:58:40 PM 189.7 12.0
5/22/2019 4:58:41 PM 189.6 11.9
5/22/2019 4:58:42 PM 189.6 11.9
5/22/2019 4:58:43 PM 189.5 11.8
5/22/2019 4:58:44 PM 189.5 11.8
5/22/2019 4:58:45 PM 189.4 11.7
5/22/2019 4:58:46 PM 189.4 11.7
5/22/2019 4:58:47 PM 189.3 11.6
5/22/2019 4:58:48 PM 189.3 11.6
5/22/2019 4:58:49 PM 189.2 11.5
5/22/2019 4:58:50 PM 189.2 11.5
5/22/2019 4:58:51 PM 189.2 11.5
5/22/2019 4:58:52 PM 189.1 11.4
5/22/2019 4:58:53 PM 189.1 11.4
5/22/2019 4:58:54 PM 189.1 11.4
5/22/2019 4:58:55 PM 189.1 11.4
5/22/2019 4:58:56 PM 189.1 11.4
5/22/2019 4:58:57 PM 189.0 11.3
5/22/2019 4:58:58 PM 189.0 11.3
5/22/2019 4:58:59 PM 189.0 11.3
5/22/2019 4:59:00 PM 189.0 11.3
5/22/2019 4:59:01 PM 188.9 11.2
5/22/2019 4:59:02 PM 188.9 11.2
5/22/2019 4:59:03 PM 188.9 11.2
5/22/2019 4:59:04 PM 188.9 11.2
5/22/2019 4:59:05 PM 188.8 11.1
5/22/2019 4:59:06 PM 188.8 11.1
5/22/2019 4:59:07 PM 188.7 11.0
5/22/2019 4:59:08 PM 188.7 11.0
5/22/2019 4:59:09 PM 188.7 11.0
5/22/2019 4:59:10 PM 188.6 10.9
5/22/2019 4:59:11 PM 188.6 10.9
5/22/2019 4:59:12 PM 188.6 10.9
5/22/2019 4:59:13 PM 188.5 10.8
5/22/2019 4:59:14 PM 188.5 10.8
5/22/2019 4:59:15 PM 188.4 10.7
5/22/2019 4:59:16 PM 188.4 10.7
5/22/2019 4:59:17 PM 188.4 10.7
5/22/2019 4:59:18 PM 188.4 10.7
Page 286 of 452 August 2019
APPENDIX E47: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-4 May
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-B2-TEST-4 1528
SEEP-B2-TEST-4 1532
SEEP-B2-TEST-4 1533
SEEP-B2-TEST-4 1534
EC Reading
(µS/cms)
SEEP-B2-TEST-4 29.9
SEEP-B2-TEST-4 167
SEEP-B2-TEST-4 426
SEEP-B2-TEST-4 3,329
SEEP-B2-TEST-4 15,499
SEEP-B2-TEST-4 127,509
q 301,000
K 1.2780
0.7
10.5
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
NR Not recorded
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(°C)
Temperature
Table E3 SEEP-B2 TEST-4 YSI Salt Dilution Calibration Data
(µS/cms)(°C)
Table E2 SEEP-B2 TEST-4 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Geometric Mean 162.4 (µS/cms)
151.5 NR
165.2 NR
167 NR
166.4 NR
Average 162.5 (µS/cms)
Average (pre-test)178.7 (µS/cms)
Average (post-test)182.6 (µS/cms)
Location Calibration
Concentration
1 NR
10 NR
Slope of Calibration Curve (µS/cms) / (mg/L)
100 NR
1,000 NR
10,000 NR
100,000 NR
Table E4 SEEP-B2 TEST-4 Flow Calculation Summary
Mass of Salt injected mg
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline,
Watershed Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)583,874.1 (s) . (µS/cms)
Calculated Flow Rate Q
L/s
GPM
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 287 of 452 August 2019
APPENDIX E48: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 4:37:53 PM 180.3 -
6/7/2019 4:37:54 PM 180.3 -
6/7/2019 4:37:55 PM 180.3 -
6/7/2019 4:37:56 PM 180.3 -
6/7/2019 4:37:57 PM 180.3 -
6/7/2019 4:37:58 PM 180.3 -
6/7/2019 4:37:59 PM 180.3 -
6/7/2019 4:38:00 PM 180.3 -
6/7/2019 4:38:01 PM 180.3 -
6/7/2019 4:38:02 PM 180.3 -
6/7/2019 4:38:03 PM 180.3 -
6/7/2019 4:38:04 PM 180.3 -
6/7/2019 4:38:05 PM 180.3 -
6/7/2019 4:38:06 PM 180.3 -
6/7/2019 4:38:07 PM 180.3 -
6/7/2019 4:38:08 PM 180.4 -
6/7/2019 4:38:09 PM 180.4 -
6/7/2019 4:38:10 PM 180.4 -
6/7/2019 4:38:11 PM 180.4 -
6/7/2019 4:38:12 PM 180.4 -
6/7/2019 4:38:13 PM 180.4 -
6/7/2019 4:38:14 PM 180.4 -
6/7/2019 4:38:15 PM 180.4 -
6/7/2019 4:38:16 PM 180.4 -
6/7/2019 4:38:17 PM 180.4 -
6/7/2019 4:38:18 PM 180.4 -
6/7/2019 4:38:19 PM 180.5 -
6/7/2019 4:38:20 PM 180.5 -
6/7/2019 4:38:21 PM 180.6 -
6/7/2019 4:38:22 PM 180.6 -
6/7/2019 4:38:23 PM 180.7 -
6/7/2019 4:38:24 PM 180.7 -
6/7/2019 4:38:25 PM 180.7 -
6/7/2019 4:38:26 PM 180.7 -
6/7/2019 4:38:27 PM 180.8 -
6/7/2019 4:38:28 PM 180.8 -
6/7/2019 4:38:29 PM 180.8 -
6/7/2019 4:38:30 PM 180.8 -
6/7/2019 4:38:31 PM 180.8 -
6/7/2019 4:38:32 PM 180.9 -
6/7/2019 4:38:33 PM 181.9 -
6/7/2019 4:38:34 PM 271.9 91.4
6/7/2019 4:38:35 PM 403.8 223.3
6/7/2019 4:38:36 PM 561.6 381.1
6/7/2019 4:38:37 PM 3114.8 2934.3
6/7/2019 4:38:38 PM 3870.9 3690.4
6/7/2019 4:38:39 PM 6737.5 6557.0
6/7/2019 4:38:40 PM 8884.4 8703.9
6/7/2019 4:38:41 PM 15336.8 15156.3
6/7/2019 4:38:42 PM 18052.4 17871.9
6/7/2019 4:38:43 PM 19352.4 19171.9
6/7/2019 4:38:44 PM 19248.9 19068.4
6/7/2019 4:38:45 PM 19043.4 18862.9
6/7/2019 4:38:46 PM 19658.5 19478.0
6/7/2019 4:38:47 PM 19397.0 19216.5
6/7/2019 4:38:48 PM 19194.3 19013.8
6/7/2019 4:38:49 PM 18983.5 18803.0
6/7/2019 4:38:50 PM 17726.9 17546.4
6/7/2019 4:38:51 PM 16347.5 16167.0
6/7/2019 4:38:52 PM 15580.2 15399.7
6/7/2019 4:38:53 PM 14776.2 14595.7
6/7/2019 4:38:54 PM 14493.1 14312.6
6/7/2019 4:38:55 PM 12696.7 12516.2
6/7/2019 4:38:56 PM 11585.6 11405.1
6/7/2019 4:38:57 PM 10939.8 10759.3
6/7/2019 4:38:58 PM 9990.8 9810.3
6/7/2019 4:38:59 PM 9160.0 8979.5
6/7/2019 4:39:00 PM 8457.4 8276.9
6/7/2019 4:39:01 PM 7713.4 7532.9
6/7/2019 4:39:02 PM 6915.3 6734.8
Table E1 SEEP-B2 TEST-1 Data Log
Page 288 of 452 August 2019
APPENDIX E48: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
6/7/2019 4:39:03 PM 6355.6 6175.1
6/7/2019 4:39:04 PM 6150.3 5969.8
6/7/2019 4:39:05 PM 5431.3 5250.8
6/7/2019 4:39:06 PM 5250.9 5070.4
6/7/2019 4:39:07 PM 4707.2 4526.7
6/7/2019 4:39:08 PM 4443.7 4263.2
6/7/2019 4:39:09 PM 4169.9 3989.4
6/7/2019 4:39:10 PM 4032.9 3852.4
6/7/2019 4:39:11 PM 3852.7 3672.2
6/7/2019 4:39:12 PM 3286.0 3105.5
6/7/2019 4:39:13 PM 3108.4 2927.9
6/7/2019 4:39:14 PM 2642.9 2462.4
6/7/2019 4:39:15 PM 2539.7 2359.2
6/7/2019 4:39:16 PM 2491.1 2310.6
6/7/2019 4:39:17 PM 2301.8 2121.3
6/7/2019 4:39:18 PM 2200.1 2019.6
6/7/2019 4:39:19 PM 1950.9 1770.4
6/7/2019 4:39:20 PM 1931.7 1751.2
6/7/2019 4:39:21 PM 1937.1 1756.6
6/7/2019 4:39:22 PM 1753.5 1573.0
6/7/2019 4:39:23 PM 1666.3 1485.8
6/7/2019 4:39:24 PM 1569.5 1389.0
6/7/2019 4:39:25 PM 1575.7 1395.2
6/7/2019 4:39:26 PM 1593.2 1412.7
6/7/2019 4:39:27 PM 1572.3 1391.8
6/7/2019 4:39:28 PM 1387.5 1207.0
6/7/2019 4:39:29 PM 1326.2 1145.7
6/7/2019 4:39:30 PM 1292.0 1111.5
6/7/2019 4:39:31 PM 1269.0 1088.5
6/7/2019 4:39:32 PM 1138.9 958.4
6/7/2019 4:39:33 PM 1119.8 939.3
6/7/2019 4:39:34 PM 1076.9 896.4
6/7/2019 4:39:35 PM 1119.5 939.0
6/7/2019 4:39:36 PM 1130.6 950.1
6/7/2019 4:39:37 PM 1126.4 945.9
6/7/2019 4:39:38 PM 1016.4 835.9
6/7/2019 4:39:39 PM 974.4 793.9
6/7/2019 4:39:40 PM 884.9 704.4
6/7/2019 4:39:41 PM 860.1 679.6
6/7/2019 4:39:42 PM 797.8 617.3
6/7/2019 4:39:43 PM 790.2 609.7
6/7/2019 4:39:44 PM 795.1 614.6
6/7/2019 4:39:45 PM 840.1 659.6
6/7/2019 4:39:46 PM 829.3 648.8
6/7/2019 4:39:47 PM 820.3 639.8
6/7/2019 4:39:48 PM 704.3 523.8
6/7/2019 4:39:49 PM 684.0 503.5
6/7/2019 4:39:50 PM 649.4 468.9
6/7/2019 4:39:51 PM 645.2 464.7
6/7/2019 4:39:52 PM 637.3 456.8
6/7/2019 4:39:53 PM 635.7 455.2
6/7/2019 4:39:54 PM 638.5 458.0
6/7/2019 4:39:55 PM 636.9 456.4
6/7/2019 4:39:56 PM 548.7 368.2
6/7/2019 4:39:57 PM 547.1 366.6
6/7/2019 4:39:58 PM 561.0 380.5
6/7/2019 4:39:59 PM 567.5 387.0
6/7/2019 4:40:00 PM 567.5 387.0
6/7/2019 4:40:01 PM 563.4 382.9
6/7/2019 4:40:02 PM 559.6 379.1
6/7/2019 4:40:03 PM 555.2 374.7
6/7/2019 4:40:04 PM 548.6 368.1
6/7/2019 4:40:05 PM 544.2 363.7
6/7/2019 4:40:06 PM 539.8 359.3
6/7/2019 4:40:07 PM 479.8 299.3
6/7/2019 4:40:08 PM 472.7 292.2
6/7/2019 4:40:09 PM 467.0 286.5
6/7/2019 4:40:10 PM 464.3 283.8
6/7/2019 4:40:11 PM 460.2 279.7
6/7/2019 4:40:12 PM 456.8 276.3
6/7/2019 4:40:13 PM 455.5 275.0
6/7/2019 4:40:14 PM 454.0 273.5
6/7/2019 4:40:15 PM 452.9 272.4
6/7/2019 4:40:16 PM 450.6 270.1
6/7/2019 4:40:17 PM 448.1 267.6
6/7/2019 4:40:18 PM 446.2 265.7
6/7/2019 4:40:19 PM 443.9 263.4
Page 289 of 452 August 2019
APPENDIX E48: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
6/7/2019 4:40:20 PM 441.5 261.0
6/7/2019 4:40:21 PM 439.0 258.5
6/7/2019 4:40:22 PM 437.0 256.5
6/7/2019 4:40:23 PM 433.2 252.7
6/7/2019 4:40:24 PM 429.2 248.7
6/7/2019 4:40:25 PM 424.5 244.0
6/7/2019 4:40:26 PM 419.9 239.4
6/7/2019 4:40:27 PM 414.3 233.8
6/7/2019 4:40:28 PM 409.3 228.8
6/7/2019 4:40:29 PM 404.2 223.7
6/7/2019 4:40:30 PM 399.6 219.1
6/7/2019 4:40:31 PM 394.7 214.2
6/7/2019 4:40:32 PM 391.0 210.5
6/7/2019 4:40:33 PM 386.6 206.1
6/7/2019 4:40:34 PM 382.5 202.0
6/7/2019 4:40:35 PM 378.2 197.7
6/7/2019 4:40:36 PM 373.8 193.3
6/7/2019 4:40:37 PM 370.1 189.6
6/7/2019 4:40:38 PM 366.4 185.9
6/7/2019 4:40:39 PM 363.5 183.0
6/7/2019 4:40:40 PM 360.3 179.8
6/7/2019 4:40:41 PM 357.4 176.9
6/7/2019 4:40:42 PM 354.2 173.7
6/7/2019 4:40:43 PM 351.7 171.2
6/7/2019 4:40:44 PM 348.7 168.2
6/7/2019 4:40:45 PM 346.0 165.5
6/7/2019 4:40:46 PM 343.4 162.9
6/7/2019 4:40:47 PM 341.1 160.6
6/7/2019 4:40:48 PM 337.9 157.4
6/7/2019 4:40:49 PM 335.5 155.0
6/7/2019 4:40:50 PM 332.9 152.4
6/7/2019 4:40:51 PM 330.6 150.1
6/7/2019 4:40:52 PM 328.0 147.5
6/7/2019 4:40:53 PM 326.0 145.5
6/7/2019 4:40:54 PM 323.6 143.1
6/7/2019 4:40:55 PM 321.3 140.8
6/7/2019 4:40:56 PM 319.3 138.8
6/7/2019 4:40:57 PM 316.8 136.3
6/7/2019 4:40:58 PM 314.7 134.2
6/7/2019 4:40:59 PM 312.5 132.0
6/7/2019 4:41:00 PM 310.9 130.4
6/7/2019 4:41:01 PM 309.4 128.9
6/7/2019 4:41:02 PM 308.1 127.6
6/7/2019 4:41:03 PM 306.4 125.9
6/7/2019 4:41:04 PM 304.8 124.3
6/7/2019 4:41:05 PM 302.9 122.4
6/7/2019 4:41:06 PM 301.3 120.8
6/7/2019 4:41:07 PM 299.7 119.2
6/7/2019 4:41:08 PM 298.4 117.9
6/7/2019 4:41:09 PM 296.9 116.4
6/7/2019 4:41:10 PM 295.7 115.2
6/7/2019 4:41:11 PM 294.2 113.7
6/7/2019 4:41:12 PM 293.0 112.5
6/7/2019 4:41:13 PM 291.5 111.0
6/7/2019 4:41:14 PM 289.8 109.3
6/7/2019 4:41:15 PM 288.3 107.8
6/7/2019 4:41:16 PM 286.8 106.3
6/7/2019 4:41:17 PM 285.5 105.0
6/7/2019 4:41:18 PM 284.1 103.6
6/7/2019 4:41:19 PM 283.2 102.7
6/7/2019 4:41:20 PM 282.4 101.9
6/7/2019 4:41:21 PM 281.5 101.0
6/7/2019 4:41:22 PM 280.3 99.8
6/7/2019 4:41:23 PM 279.1 98.6
6/7/2019 4:41:24 PM 277.7 97.2
6/7/2019 4:41:25 PM 276.6 96.1
6/7/2019 4:41:26 PM 275.4 94.9
6/7/2019 4:41:27 PM 274.3 93.8
6/7/2019 4:41:28 PM 273.3 92.8
6/7/2019 4:41:29 PM 272.6 92.1
6/7/2019 4:41:30 PM 271.9 91.4
6/7/2019 4:41:31 PM 271.2 90.7
6/7/2019 4:41:32 PM 270.5 90.0
6/7/2019 4:41:33 PM 269.4 88.9
6/7/2019 4:41:34 PM 268.3 87.8
6/7/2019 4:41:35 PM 267.3 86.8
6/7/2019 4:41:36 PM 266.5 86.0
6/7/2019 4:41:37 PM 265.6 85.1
6/7/2019 4:41:38 PM 264.9 84.4
Page 290 of 452 August 2019
APPENDIX E48: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
6/7/2019 4:41:39 PM 264.1 83.6
6/7/2019 4:41:40 PM 263.5 83.0
6/7/2019 4:41:41 PM 262.7 82.2
6/7/2019 4:41:42 PM 261.9 81.4
6/7/2019 4:41:43 PM 260.9 80.4
6/7/2019 4:41:44 PM 260.2 79.7
6/7/2019 4:41:45 PM 259.4 78.9
6/7/2019 4:41:46 PM 258.7 78.2
6/7/2019 4:41:47 PM 258.0 77.5
6/7/2019 4:41:48 PM 257.3 76.8
6/7/2019 4:41:49 PM 256.6 76.1
6/7/2019 4:41:50 PM 255.8 75.3
6/7/2019 4:41:51 PM 255.0 74.5
6/7/2019 4:41:52 PM 254.1 73.6
6/7/2019 4:41:53 PM 253.3 72.8
6/7/2019 4:41:54 PM 252.5 72.0
6/7/2019 4:41:55 PM 251.7 71.2
6/7/2019 4:41:56 PM 250.9 70.4
6/7/2019 4:41:57 PM 250.1 69.6
6/7/2019 4:41:58 PM 249.1 68.6
6/7/2019 4:41:59 PM 248.5 68.0
6/7/2019 4:42:00 PM 247.9 67.4
6/7/2019 4:42:01 PM 247.4 66.9
6/7/2019 4:42:02 PM 246.8 66.3
6/7/2019 4:42:03 PM 246.3 65.8
6/7/2019 4:42:04 PM 245.8 65.3
6/7/2019 4:42:05 PM 245.4 64.9
6/7/2019 4:42:06 PM 245.0 64.5
6/7/2019 4:42:07 PM 244.6 64.1
6/7/2019 4:42:08 PM 244.0 63.5
6/7/2019 4:42:09 PM 243.4 62.9
6/7/2019 4:42:10 PM 242.9 62.4
6/7/2019 4:42:11 PM 242.4 61.9
6/7/2019 4:42:12 PM 241.9 61.4
6/7/2019 4:42:13 PM 241.4 60.9
6/7/2019 4:42:14 PM 241.0 60.5
6/7/2019 4:42:15 PM 240.6 60.1
6/7/2019 4:42:16 PM 240.1 59.6
6/7/2019 4:42:17 PM 239.6 59.1
6/7/2019 4:42:18 PM 239.1 58.6
6/7/2019 4:42:19 PM 238.4 57.9
6/7/2019 4:42:20 PM 237.9 57.4
6/7/2019 4:42:21 PM 237.3 56.8
6/7/2019 4:42:22 PM 236.9 56.4
6/7/2019 4:42:23 PM 236.4 55.9
6/7/2019 4:42:24 PM 236.1 55.6
6/7/2019 4:42:25 PM 235.5 55.0
6/7/2019 4:42:26 PM 235.0 54.5
6/7/2019 4:42:27 PM 234.2 53.7
6/7/2019 4:42:28 PM 233.6 53.1
6/7/2019 4:42:29 PM 233.2 52.7
6/7/2019 4:42:30 PM 232.9 52.4
6/7/2019 4:42:31 PM 232.7 52.2
6/7/2019 4:42:32 PM 232.3 51.8
6/7/2019 4:42:33 PM 232.0 51.5
6/7/2019 4:42:34 PM 231.6 51.1
6/7/2019 4:42:35 PM 231.3 50.8
6/7/2019 4:42:36 PM 231.0 50.5
6/7/2019 4:42:37 PM 230.7 50.2
6/7/2019 4:42:38 PM 230.3 49.8
6/7/2019 4:42:39 PM 230.0 49.5
6/7/2019 4:42:40 PM 229.6 49.1
6/7/2019 4:42:41 PM 229.4 48.9
6/7/2019 4:42:42 PM 229.0 48.5
6/7/2019 4:42:43 PM 228.6 48.1
6/7/2019 4:42:44 PM 228.0 47.5
6/7/2019 4:42:45 PM 227.6 47.1
6/7/2019 4:42:46 PM 227.2 46.7
6/7/2019 4:42:47 PM 226.8 46.3
6/7/2019 4:42:48 PM 226.3 45.8
6/7/2019 4:42:49 PM 225.8 45.3
6/7/2019 4:42:50 PM 225.3 44.8
6/7/2019 4:42:51 PM 224.9 44.4
6/7/2019 4:42:52 PM 224.5 44.0
6/7/2019 4:42:53 PM 224.2 43.7
6/7/2019 4:42:54 PM 223.8 43.3
6/7/2019 4:42:55 PM 223.4 42.9
6/7/2019 4:42:56 PM 223.0 42.5
6/7/2019 4:42:57 PM 222.7 42.2
Page 291 of 452 August 2019
APPENDIX E48: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
6/7/2019 4:42:58 PM 222.4 41.9
6/7/2019 4:42:59 PM 222.1 41.6
6/7/2019 4:43:00 PM 221.8 41.3
6/7/2019 4:43:01 PM 221.5 41.0
6/7/2019 4:43:02 PM 221.3 40.8
6/7/2019 4:43:03 PM 221.0 40.5
6/7/2019 4:43:04 PM 220.7 40.2
6/7/2019 4:43:05 PM 220.4 39.9
6/7/2019 4:43:06 PM 220.0 39.5
6/7/2019 4:43:07 PM 219.7 39.2
6/7/2019 4:43:08 PM 219.3 38.8
6/7/2019 4:43:09 PM 219.0 38.5
6/7/2019 4:43:10 PM 218.6 38.1
6/7/2019 4:43:11 PM 218.3 37.8
6/7/2019 4:43:12 PM 218.0 37.5
6/7/2019 4:43:13 PM 217.7 37.2
6/7/2019 4:43:14 PM 217.4 36.9
6/7/2019 4:43:15 PM 217.1 36.6
6/7/2019 4:43:16 PM 216.9 36.4
6/7/2019 4:43:17 PM 216.7 36.2
6/7/2019 4:43:18 PM 216.6 36.1
6/7/2019 4:43:19 PM 216.4 35.9
6/7/2019 4:43:20 PM 216.2 35.7
6/7/2019 4:43:21 PM 216.0 35.5
6/7/2019 4:43:22 PM 215.8 35.3
6/7/2019 4:43:23 PM 215.6 35.1
6/7/2019 4:43:24 PM 215.4 34.9
6/7/2019 4:43:25 PM 215.2 34.7
6/7/2019 4:43:26 PM 215.0 34.5
6/7/2019 4:43:27 PM 214.8 34.3
6/7/2019 4:43:28 PM 214.6 34.1
6/7/2019 4:43:29 PM 214.3 33.8
6/7/2019 4:43:30 PM 214.1 33.6
6/7/2019 4:43:31 PM 213.8 33.3
6/7/2019 4:43:32 PM 213.6 33.1
6/7/2019 4:43:33 PM 213.4 32.9
6/7/2019 4:43:34 PM 213.3 32.8
6/7/2019 4:43:35 PM 213.1 32.6
6/7/2019 4:43:36 PM 213.0 32.5
6/7/2019 4:43:37 PM 212.8 32.3
6/7/2019 4:43:38 PM 212.7 32.2
6/7/2019 4:43:39 PM 212.5 32.0
6/7/2019 4:43:40 PM 212.3 31.8
6/7/2019 4:43:41 PM 212.2 31.7
6/7/2019 4:43:42 PM 212.0 31.5
6/7/2019 4:43:43 PM 211.8 31.3
6/7/2019 4:43:44 PM 211.7 31.2
6/7/2019 4:43:45 PM 211.6 31.1
6/7/2019 4:43:46 PM 211.4 30.9
6/7/2019 4:43:47 PM 211.2 30.7
6/7/2019 4:43:48 PM 211.0 30.5
6/7/2019 4:43:49 PM 210.8 30.3
6/7/2019 4:43:50 PM 210.6 30.1
6/7/2019 4:43:51 PM 210.4 29.9
6/7/2019 4:43:52 PM 210.2 29.7
6/7/2019 4:43:53 PM 210.0 29.5
6/7/2019 4:43:54 PM 209.8 29.3
6/7/2019 4:43:55 PM 209.6 29.1
6/7/2019 4:43:56 PM 209.4 28.9
6/7/2019 4:43:57 PM 209.2 28.7
6/7/2019 4:43:58 PM 209.0 28.5
6/7/2019 4:43:59 PM 208.8 28.3
6/7/2019 4:44:00 PM 208.6 28.1
6/7/2019 4:44:01 PM 208.5 28.0
6/7/2019 4:44:02 PM 208.3 27.8
6/7/2019 4:44:03 PM 208.2 27.7
6/7/2019 4:44:04 PM 208.1 27.6
6/7/2019 4:44:05 PM 207.9 27.4
6/7/2019 4:44:06 PM 207.8 27.3
6/7/2019 4:44:07 PM 207.7 27.2
6/7/2019 4:44:08 PM 207.5 27.0
6/7/2019 4:44:09 PM 207.4 26.9
6/7/2019 4:44:10 PM 207.3 26.8
6/7/2019 4:44:11 PM 207.2 26.7
6/7/2019 4:44:12 PM 207.1 26.6
6/7/2019 4:44:13 PM 207.0 26.5
6/7/2019 4:44:14 PM 206.9 26.4
6/7/2019 4:44:15 PM 206.8 26.3
6/7/2019 4:44:16 PM 206.7 26.2
Page 292 of 452 August 2019
APPENDIX E48: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
6/7/2019 4:44:17 PM 206.6 26.1
6/7/2019 4:44:18 PM 206.5 26.0
6/7/2019 4:44:19 PM 206.3 25.8
6/7/2019 4:44:20 PM 206.2 25.7
6/7/2019 4:44:21 PM 206.1 25.6
6/7/2019 4:44:22 PM 205.9 25.4
6/7/2019 4:44:23 PM 205.8 25.3
6/7/2019 4:44:24 PM 205.6 25.1
6/7/2019 4:44:25 PM 205.4 24.9
6/7/2019 4:44:26 PM 205.2 24.7
6/7/2019 4:44:27 PM 205.1 24.6
6/7/2019 4:44:28 PM 204.9 24.4
6/7/2019 4:44:29 PM 204.8 24.3
6/7/2019 4:44:30 PM 204.6 24.1
6/7/2019 4:44:31 PM 204.5 24.0
6/7/2019 4:44:32 PM 204.5 24.0
6/7/2019 4:44:33 PM 204.6 24.1
6/7/2019 4:44:34 PM 204.6 24.1
6/7/2019 4:44:35 PM 204.5 24.0
6/7/2019 4:44:36 PM 204.4 23.9
6/7/2019 4:44:37 PM 204.2 23.7
6/7/2019 4:44:38 PM 204.1 23.6
6/7/2019 4:44:39 PM 204.0 23.5
6/7/2019 4:44:40 PM 203.9 23.4
6/7/2019 4:44:41 PM 203.7 23.2
6/7/2019 4:44:42 PM 203.6 23.1
6/7/2019 4:44:43 PM 203.5 23.0
6/7/2019 4:44:44 PM 203.3 22.8
6/7/2019 4:44:45 PM 203.0 22.5
6/7/2019 4:44:46 PM 202.7 22.2
6/7/2019 4:44:47 PM 202.5 22.0
6/7/2019 4:44:48 PM 202.3 21.8
6/7/2019 4:44:49 PM 202.2 21.7
6/7/2019 4:44:50 PM 202.1 21.6
6/7/2019 4:44:51 PM 202.0 21.5
6/7/2019 4:44:52 PM 201.8 21.3
6/7/2019 4:44:53 PM 201.7 21.2
6/7/2019 4:44:54 PM 201.6 21.1
6/7/2019 4:44:55 PM 201.5 21.0
6/7/2019 4:44:56 PM 201.4 20.9
6/7/2019 4:44:57 PM 201.3 20.8
6/7/2019 4:44:58 PM 201.2 20.7
6/7/2019 4:44:59 PM 201.1 20.6
6/7/2019 4:45:00 PM 201.0 20.5
6/7/2019 4:45:01 PM 200.9 20.4
6/7/2019 4:45:02 PM 200.7 20.2
6/7/2019 4:45:03 PM 200.6 20.1
6/7/2019 4:45:04 PM 200.5 20.0
6/7/2019 4:45:05 PM 200.4 19.9
6/7/2019 4:45:06 PM 200.3 19.8
6/7/2019 4:45:07 PM 200.2 19.7
6/7/2019 4:45:08 PM 200.1 19.6
6/7/2019 4:45:09 PM 200.0 19.5
6/7/2019 4:45:10 PM 200.0 19.5
6/7/2019 4:45:11 PM 199.9 19.4
6/7/2019 4:45:12 PM 199.8 19.3
6/7/2019 4:45:13 PM 199.8 19.3
6/7/2019 4:45:14 PM 199.7 19.2
6/7/2019 4:45:15 PM 199.7 19.2
6/7/2019 4:45:16 PM 199.6 19.1
6/7/2019 4:45:17 PM 199.6 19.1
6/7/2019 4:45:18 PM 199.6 19.1
6/7/2019 4:45:19 PM 199.5 19.0
6/7/2019 4:45:20 PM 199.5 19.0
6/7/2019 4:45:21 PM 199.4 18.9
6/7/2019 4:45:22 PM 199.4 18.9
6/7/2019 4:45:23 PM 199.3 18.8
6/7/2019 4:45:24 PM 199.3 18.8
6/7/2019 4:45:25 PM 199.2 18.7
6/7/2019 4:45:26 PM 199.1 18.6
6/7/2019 4:45:27 PM 199.0 18.5
6/7/2019 4:45:28 PM 198.9 18.4
6/7/2019 4:45:29 PM 198.8 18.3
6/7/2019 4:45:30 PM 198.8 18.3
6/7/2019 4:45:31 PM 198.7 18.2
6/7/2019 4:45:32 PM 198.6 18.1
6/7/2019 4:45:33 PM 198.4 17.9
6/7/2019 4:45:34 PM 198.3 17.8
6/7/2019 4:45:35 PM 198.2 17.7
Page 293 of 452 August 2019
APPENDIX E48: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-1 Data Log
6/7/2019 4:45:36 PM 198.1 17.6
6/7/2019 4:45:37 PM 198.0 17.5
6/7/2019 4:45:38 PM 197.9 17.4
6/7/2019 4:45:39 PM 197.8 17.3
6/7/2019 4:45:40 PM 197.7 17.2
6/7/2019 4:45:41 PM 197.6 17.1
6/7/2019 4:45:42 PM 197.5 17.0
6/7/2019 4:45:43 PM 197.4 16.9
6/7/2019 4:45:44 PM 197.3 16.8
6/7/2019 4:45:45 PM 197.2 16.7
6/7/2019 4:45:46 PM 197.2 16.7
6/7/2019 4:45:47 PM 197.1 16.6
6/7/2019 4:45:48 PM 197.0 16.5
6/7/2019 4:45:49 PM 197.0 16.5
6/7/2019 4:45:50 PM 196.9 16.4
6/7/2019 4:45:51 PM 196.8 16.3
6/7/2019 4:45:52 PM 196.8 16.3
6/7/2019 4:45:53 PM 196.7 16.2
6/7/2019 4:45:54 PM 196.7 16.2
6/7/2019 4:45:55 PM 196.6 16.1
6/7/2019 4:45:56 PM 196.6 16.1
6/7/2019 4:45:57 PM 196.5 16.0
6/7/2019 4:45:58 PM 196.5 16.0
6/7/2019 4:45:59 PM 196.5 16.0
6/7/2019 4:46:00 PM 196.5 16.0
6/7/2019 4:46:00 PM 196.4 0.0
6/7/2019 4:46:01 PM 196.4 15.9
6/7/2019 4:46:02 PM 196.3 15.8
6/7/2019 4:46:03 PM 196.3 15.8
6/7/2019 4:46:04 PM 196.2 15.7
6/7/2019 4:46:05 PM 196.2 15.7
6/7/2019 4:46:06 PM 196.1 15.6
6/7/2019 4:46:07 PM 196.0 15.5
6/7/2019 4:46:08 PM 195.9 15.4
6/7/2019 4:46:09 PM 195.9 15.4
6/7/2019 4:46:10 PM 195.7 15.2
6/7/2019 4:46:11 PM 195.6 15.1
6/7/2019 4:46:12 PM 195.5 15.0
6/7/2019 4:46:13 PM 195.4 14.9
6/7/2019 4:46:14 PM 195.4 14.9
6/7/2019 4:46:15 PM 195.3 14.8
6/7/2019 4:46:16 PM 195.3 14.8
6/7/2019 4:46:17 PM 195.2 14.7
6/7/2019 4:46:18 PM 195.2 14.7
6/7/2019 4:46:19 PM 195.1 14.6
6/7/2019 4:46:20 PM 195.1 14.6
6/7/2019 4:46:21 PM 195.0 14.5
6/7/2019 4:46:22 PM 195.0 14.5
6/7/2019 4:46:23 PM 194.9 14.4
6/7/2019 4:46:24 PM 194.9 14.4
6/7/2019 4:46:25 PM 194.8 14.3
6/7/2019 4:46:26 PM 194.8 14.3
6/7/2019 4:46:27 PM 194.8 14.3
6/7/2019 4:46:28 PM 194.7 14.2
6/7/2019 4:46:29 PM 194.7 14.2
6/7/2019 4:46:30 PM 194.7 14.2
6/7/2019 4:46:31 PM 194.6 14.1
6/7/2019 4:46:32 PM 194.5 14.0
6/7/2019 4:46:33 PM 194.5 14.0
6/7/2019 4:46:34 PM 194.4 13.9
6/7/2019 4:46:35 PM 194.3 13.8
6/7/2019 4:46:36 PM 194.2 13.7
6/7/2019 4:46:37 PM 194.2 13.7
6/7/2019 4:46:38 PM 194.1 13.6
6/7/2019 4:46:39 PM 194.0 13.5
6/7/2019 4:46:40 PM 193.9 13.4
6/7/2019 4:46:41 PM 193.8 13.3
Page 294 of 452 August 2019
APPENDIX E48: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-B2 TEST-1 1630
SEEP-B2 TEST-1 NR
SEEP-B2 TEST-1 NR
Average
Geometric Mean
Average (pre-test)
Table E3 SEEP-B2 TEST-1 YSI Salt Dilution Calibration Data
EC Reading
(µS/cms)
SEEP-B2 TEST-1 721
SEEP-B2 TEST-1 2,061
SEEP-B2 TEST-1 16,708
SEEP-B2 TEST-1 121,612
q 300,400
K 1.2207
0.8
12.5
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
NR Not recorded
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
1,000
100
(µS/cms)
(µS/cms)
(µS/cms)
180.5
174.4
174.4
24.7
24.6
(°C)
Temperature
(µS/cms) (°C)
Table E2 SEEP-B2 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Average (post-test)212.9 (µS/cms)
176.7 20.5
173.8 20.5
172.8 20.5
Slope of Calibration Curve (µS/cms) / (mg/L)
10,000 25.1
Location Calibration
Concentration
100,000 25
Table E4 SEEP-B2 TEST-1 Flow Calculation Summary
Mass of Salt injected mg
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)467,400.5 (s) . (µS/cms)
Calculated Flow Rate Q
L/s
GPM
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 295 of 452 August 2019
APPENDIX E49: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 4:53:18 PM 182.0 -
6/7/2019 4:53:19 PM 181.9 -
6/7/2019 4:53:20 PM 181.9 -
6/7/2019 4:53:21 PM 181.8 -
6/7/2019 4:53:22 PM 181.8 -
6/7/2019 4:53:23 PM 181.7 -
6/7/2019 4:53:24 PM 181.6 -
6/7/2019 4:53:25 PM 181.6 -
6/7/2019 4:53:26 PM 181.6 -
6/7/2019 4:53:27 PM 181.5 -
6/7/2019 4:53:28 PM 181.5 -
6/7/2019 4:53:29 PM 181.5 -
6/7/2019 4:53:30 PM 181.4 -
6/7/2019 4:53:31 PM 181.4 -
6/7/2019 4:53:32 PM 181.3 -
6/7/2019 4:53:33 PM 181.3 -
6/7/2019 4:53:34 PM 181.2 -
6/7/2019 4:53:35 PM 181.2 -
6/7/2019 4:53:36 PM 181.2 -
6/7/2019 4:53:37 PM 181.2 -
6/7/2019 4:53:38 PM 181.1 -
6/7/2019 4:53:39 PM 181.1 -
6/7/2019 4:53:40 PM 181.1 -
6/7/2019 4:53:41 PM 181.0 -
6/7/2019 4:53:42 PM 181.0 -
6/7/2019 4:53:43 PM 181.0 -
6/7/2019 4:53:44 PM 180.9 -
6/7/2019 4:53:45 PM 180.9 -
6/7/2019 4:53:46 PM 180.9 -
6/7/2019 4:53:47 PM 180.9 -
6/7/2019 4:53:48 PM 180.9 -
6/7/2019 4:53:49 PM 181.0 -
6/7/2019 4:53:50 PM 181.3 -
6/7/2019 4:53:51 PM 271.4 90.1
6/7/2019 4:53:52 PM 467.8 286.5
6/7/2019 4:53:53 PM 739.4 558.1
6/7/2019 4:53:54 PM 1920.4 1739.1
6/7/2019 4:53:55 PM 2501.4 2320.1
6/7/2019 4:53:56 PM 4676.4 4495.1
6/7/2019 4:53:57 PM 5800.9 5619.6
6/7/2019 4:53:58 PM 12404.1 12222.8
6/7/2019 4:53:59 PM 15439.2 15257.9
6/7/2019 4:54:00 PM 18224.6 18043.3
6/7/2019 4:54:01 PM 17808.5 17627.2
6/7/2019 4:54:02 PM 19019.7 18838.4
6/7/2019 4:54:03 PM 19526.3 19345.0
6/7/2019 4:54:04 PM 20244.4 20063.1
6/7/2019 4:54:05 PM 20142.6 19961.3
6/7/2019 4:54:06 PM 17128.5 16947.2
6/7/2019 4:54:07 PM 17414.1 17232.8
6/7/2019 4:54:08 PM 16648.1 16466.8
6/7/2019 4:54:09 PM 16367.5 16186.2
6/7/2019 4:54:10 PM 15142.8 14961.5
6/7/2019 4:54:11 PM 14202.1 14020.8
6/7/2019 4:54:12 PM 13210.7 13029.4
6/7/2019 4:54:13 PM 12102.3 11921.0
6/7/2019 4:54:14 PM 11835.1 11653.8
6/7/2019 4:54:15 PM 10454.7 10273.4
6/7/2019 4:54:16 PM 9703.9 9522.6
6/7/2019 4:54:17 PM 9010.1 8828.8
6/7/2019 4:54:18 PM 8878.5 8697.2
6/7/2019 4:54:19 PM 7732.5 7551.2
6/7/2019 4:54:20 PM 6905.1 6723.8
6/7/2019 4:54:21 PM 6366.4 6185.1
6/7/2019 4:54:22 PM 6264.4 6083.1
6/7/2019 4:54:23 PM 5697.8 5516.5
6/7/2019 4:54:24 PM 5422.0 5240.7
6/7/2019 4:54:25 PM 5049.6 4868.3
6/7/2019 4:54:26 PM 4614.3 4433.0
6/7/2019 4:54:27 PM 3942.9 3761.6
Table E1 SEEP-B2 TEST-2 Data Log
Page 296 of 452 August 2019
APPENDIX E49: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
6/7/2019 4:54:28 PM 3676.4 3495.1
6/7/2019 4:54:29 PM 3315.1 3133.8
6/7/2019 4:54:30 PM 3191.3 3010.0
6/7/2019 4:54:31 PM 2864.3 2683.0
6/7/2019 4:54:32 PM 2786.3 2605.0
6/7/2019 4:54:33 PM 2657.9 2476.6
6/7/2019 4:54:34 PM 2587.1 2405.8
6/7/2019 4:54:35 PM 2548.0 2366.7
6/7/2019 4:54:36 PM 2232.6 2051.3
6/7/2019 4:54:37 PM 2203.8 2022.5
6/7/2019 4:54:38 PM 2052.3 1871.0
6/7/2019 4:54:39 PM 1990.5 1809.2
6/7/2019 4:54:40 PM 1746.6 1565.3
6/7/2019 4:54:41 PM 1656.3 1475.0
6/7/2019 4:54:42 PM 1572.7 1391.4
6/7/2019 4:54:43 PM 1549.7 1368.4
6/7/2019 4:54:44 PM 1514.2 1332.9
6/7/2019 4:54:45 PM 1375.2 1193.9
6/7/2019 4:54:46 PM 1334.4 1153.1
6/7/2019 4:54:47 PM 1297.2 1115.9
6/7/2019 4:54:48 PM 1280.8 1099.5
6/7/2019 4:54:49 PM 1159.7 978.4
6/7/2019 4:54:50 PM 1078.3 897.0
6/7/2019 4:54:51 PM 1029.8 848.5
6/7/2019 4:54:52 PM 986.4 805.1
6/7/2019 4:54:53 PM 962.2 780.9
6/7/2019 4:54:54 PM 944.7 763.4
6/7/2019 4:54:55 PM 928.8 747.5
6/7/2019 4:54:56 PM 919.9 738.6
6/7/2019 4:54:57 PM 912.9 731.6
6/7/2019 4:54:58 PM 832.4 651.1
6/7/2019 4:54:59 PM 778.3 597.0
6/7/2019 4:55:00 PM 757.6 576.3
6/7/2019 4:55:01 PM 755.4 574.1
6/7/2019 4:55:02 PM 747.2 565.9
6/7/2019 4:55:03 PM 727.2 545.9
6/7/2019 4:55:04 PM 715.6 534.3
6/7/2019 4:55:05 PM 652.4 471.1
6/7/2019 4:55:06 PM 629.0 447.7
6/7/2019 4:55:07 PM 615.4 434.1
6/7/2019 4:55:08 PM 561.1 379.8
6/7/2019 4:55:09 PM 570.1 388.8
6/7/2019 4:55:10 PM 569.0 387.7
6/7/2019 4:55:11 PM 563.6 382.3
6/7/2019 4:55:12 PM 556.5 375.2
6/7/2019 4:55:13 PM 550.5 369.2
6/7/2019 4:55:14 PM 544.1 362.8
6/7/2019 4:55:15 PM 539.4 358.1
6/7/2019 4:55:16 PM 535.1 353.8
6/7/2019 4:55:17 PM 531.5 350.2
6/7/2019 4:55:18 PM 527.7 346.4
6/7/2019 4:55:19 PM 525.8 344.5
6/7/2019 4:55:20 PM 524.6 343.3
6/7/2019 4:55:21 PM 523.3 342.0
6/7/2019 4:55:22 PM 518.0 336.7
6/7/2019 4:55:23 PM 512.0 330.7
6/7/2019 4:55:24 PM 505.8 324.5
6/7/2019 4:55:25 PM 460.5 279.2
6/7/2019 4:55:26 PM 442.6 261.3
6/7/2019 4:55:27 PM 431.4 250.1
6/7/2019 4:55:28 PM 425.2 243.9
6/7/2019 4:55:29 PM 423.2 241.9
6/7/2019 4:55:30 PM 420.3 239.0
6/7/2019 4:55:31 PM 417.2 235.9
6/7/2019 4:55:32 PM 414.3 233.0
6/7/2019 4:55:33 PM 411.4 230.1
6/7/2019 4:55:34 PM 409.1 227.8
6/7/2019 4:55:35 PM 406.9 225.6
6/7/2019 4:55:36 PM 405.0 223.7
6/7/2019 4:55:37 PM 402.9 221.6
6/7/2019 4:55:38 PM 400.9 219.6
6/7/2019 4:55:39 PM 398.5 217.2
6/7/2019 4:55:40 PM 396.4 215.1
6/7/2019 4:55:41 PM 393.9 212.6
6/7/2019 4:55:42 PM 390.0 208.7
6/7/2019 4:55:43 PM 385.7 204.4
6/7/2019 4:55:44 PM 382.1 200.8
Page 297 of 452 August 2019
APPENDIX E49: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
6/7/2019 4:55:45 PM 378.3 197.0
6/7/2019 4:55:46 PM 375.1 193.8
6/7/2019 4:55:47 PM 371.2 189.9
6/7/2019 4:55:48 PM 367.3 186.0
6/7/2019 4:55:49 PM 363.9 182.6
6/7/2019 4:55:50 PM 360.2 178.9
6/7/2019 4:55:51 PM 357.1 175.8
6/7/2019 4:55:52 PM 353.9 172.6
6/7/2019 4:55:53 PM 351.3 170.0
6/7/2019 4:55:54 PM 348.5 167.2
6/7/2019 4:55:55 PM 346.0 164.7
6/7/2019 4:55:56 PM 342.9 161.6
6/7/2019 4:55:57 PM 340.4 159.1
6/7/2019 4:55:58 PM 337.5 156.2
6/7/2019 4:55:59 PM 335.0 153.7
6/7/2019 4:56:00 PM 332.4 151.1
6/7/2019 4:56:01 PM 330.3 149.0
6/7/2019 4:56:02 PM 327.7 146.4
6/7/2019 4:56:03 PM 325.3 144.0
6/7/2019 4:56:04 PM 322.7 141.4
6/7/2019 4:56:05 PM 320.4 139.1
6/7/2019 4:56:06 PM 317.4 136.1
6/7/2019 4:56:07 PM 314.5 133.2
6/7/2019 4:56:08 PM 312.1 130.8
6/7/2019 4:56:09 PM 309.3 128.0
6/7/2019 4:56:10 PM 306.9 125.6
6/7/2019 4:56:11 PM 304.1 122.8
6/7/2019 4:56:12 PM 301.9 120.6
6/7/2019 4:56:13 PM 299.4 118.1
6/7/2019 4:56:14 PM 297.2 115.9
6/7/2019 4:56:15 PM 295.0 113.7
6/7/2019 4:56:16 PM 293.3 112.0
6/7/2019 4:56:17 PM 291.5 110.2
6/7/2019 4:56:18 PM 290.0 108.7
6/7/2019 4:56:19 PM 288.7 107.4
6/7/2019 4:56:20 PM 287.6 106.3
6/7/2019 4:56:21 PM 286.5 105.2
6/7/2019 4:56:22 PM 285.5 104.2
6/7/2019 4:56:23 PM 284.4 103.1
6/7/2019 4:56:24 PM 283.2 101.9
6/7/2019 4:56:25 PM 282.3 101.0
6/7/2019 4:56:26 PM 281.4 100.1
6/7/2019 4:56:27 PM 280.6 99.3
6/7/2019 4:56:28 PM 279.7 98.4
6/7/2019 4:56:29 PM 278.9 97.6
6/7/2019 4:56:30 PM 277.9 96.6
6/7/2019 4:56:31 PM 277.1 95.8
6/7/2019 4:56:32 PM 276.1 94.8
6/7/2019 4:56:33 PM 275.1 93.8
6/7/2019 4:56:34 PM 274.0 92.7
6/7/2019 4:56:35 PM 273.1 91.8
6/7/2019 4:56:36 PM 272.2 90.9
6/7/2019 4:56:37 PM 271.4 90.1
6/7/2019 4:56:38 PM 270.3 89.0
6/7/2019 4:56:39 PM 269.4 88.1
6/7/2019 4:56:40 PM 268.3 87.0
6/7/2019 4:56:41 PM 267.4 86.1
6/7/2019 4:56:42 PM 266.3 85.0
6/7/2019 4:56:43 PM 265.2 83.9
6/7/2019 4:56:44 PM 264.2 82.9
6/7/2019 4:56:45 PM 263.1 81.8
6/7/2019 4:56:46 PM 262.3 81.0
6/7/2019 4:56:47 PM 261.3 80.0
6/7/2019 4:56:48 PM 260.4 79.1
6/7/2019 4:56:49 PM 259.3 78.0
6/7/2019 4:56:50 PM 258.4 77.1
6/7/2019 4:56:51 PM 257.5 76.2
6/7/2019 4:56:52 PM 256.7 75.4
6/7/2019 4:56:53 PM 255.8 74.5
6/7/2019 4:56:54 PM 255.1 73.8
6/7/2019 4:56:55 PM 254.2 72.9
6/7/2019 4:56:56 PM 253.4 72.1
6/7/2019 4:56:57 PM 252.6 71.3
6/7/2019 4:56:58 PM 251.8 70.5
6/7/2019 4:56:59 PM 250.8 69.5
6/7/2019 4:57:00 PM 250.0 68.7
6/7/2019 4:57:01 PM 249.1 67.8
6/7/2019 4:57:02 PM 248.4 67.1
6/7/2019 4:57:03 PM 247.8 66.5
Page 298 of 452 August 2019
APPENDIX E49: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
6/7/2019 4:57:04 PM 247.0 65.7
6/7/2019 4:57:05 PM 246.3 65.0
6/7/2019 4:57:06 PM 245.5 64.2
6/7/2019 4:57:07 PM 244.8 63.5
6/7/2019 4:57:08 PM 244.1 62.8
6/7/2019 4:57:09 PM 243.5 62.2
6/7/2019 4:57:10 PM 242.7 61.4
6/7/2019 4:57:11 PM 242.2 60.9
6/7/2019 4:57:12 PM 241.6 60.3
6/7/2019 4:57:13 PM 241.1 59.8
6/7/2019 4:57:14 PM 240.6 59.3
6/7/2019 4:57:15 PM 240.1 58.8
6/7/2019 4:57:16 PM 239.4 58.1
6/7/2019 4:57:17 PM 238.8 57.5
6/7/2019 4:57:18 PM 238.2 56.9
6/7/2019 4:57:19 PM 237.8 56.5
6/7/2019 4:57:20 PM 237.2 55.9
6/7/2019 4:57:21 PM 236.7 55.4
6/7/2019 4:57:22 PM 236.3 55.0
6/7/2019 4:57:23 PM 235.8 54.5
6/7/2019 4:57:24 PM 235.4 54.1
6/7/2019 4:57:25 PM 234.9 53.6
6/7/2019 4:57:26 PM 234.4 53.1
6/7/2019 4:57:27 PM 234.0 52.7
6/7/2019 4:57:28 PM 233.6 52.3
6/7/2019 4:57:29 PM 233.2 51.9
6/7/2019 4:57:30 PM 232.9 51.6
6/7/2019 4:57:31 PM 232.5 51.2
6/7/2019 4:57:32 PM 232.2 50.9
6/7/2019 4:57:33 PM 231.7 50.4
6/7/2019 4:57:34 PM 231.3 50.0
6/7/2019 4:57:35 PM 230.9 49.6
6/7/2019 4:57:36 PM 230.6 49.3
6/7/2019 4:57:37 PM 230.3 49.0
6/7/2019 4:57:38 PM 230.0 48.7
6/7/2019 4:57:39 PM 229.6 48.3
6/7/2019 4:57:40 PM 229.2 47.9
6/7/2019 4:57:41 PM 228.8 47.5
6/7/2019 4:57:42 PM 228.4 47.1
6/7/2019 4:57:43 PM 228.0 46.7
6/7/2019 4:57:44 PM 227.7 46.4
6/7/2019 4:57:45 PM 227.4 46.1
6/7/2019 4:57:46 PM 227.1 45.8
6/7/2019 4:57:47 PM 226.9 45.6
6/7/2019 4:57:48 PM 226.5 45.2
6/7/2019 4:57:49 PM 226.2 44.9
6/7/2019 4:57:50 PM 225.7 44.4
6/7/2019 4:57:51 PM 225.3 44.0
6/7/2019 4:57:52 PM 224.9 43.6
6/7/2019 4:57:53 PM 224.6 43.3
6/7/2019 4:57:54 PM 224.3 43.0
6/7/2019 4:57:55 PM 223.9 42.6
6/7/2019 4:57:56 PM 223.5 42.2
6/7/2019 4:57:57 PM 223.1 41.8
6/7/2019 4:57:58 PM 222.7 41.4
6/7/2019 4:57:59 PM 222.3 41.0
6/7/2019 4:58:00 PM 221.9 40.6
6/7/2019 4:58:01 PM 221.6 40.3
6/7/2019 4:58:02 PM 221.3 40.0
6/7/2019 4:58:03 PM 220.9 39.6
6/7/2019 4:58:04 PM 220.7 39.4
6/7/2019 4:58:05 PM 220.3 39.0
6/7/2019 4:58:06 PM 220.0 38.7
6/7/2019 4:58:07 PM 219.6 38.3
6/7/2019 4:58:08 PM 219.3 38.0
6/7/2019 4:58:09 PM 219.0 37.7
6/7/2019 4:58:10 PM 218.7 37.4
6/7/2019 4:58:11 PM 218.3 37.0
6/7/2019 4:58:12 PM 218.1 36.8
6/7/2019 4:58:13 PM 217.7 36.4
6/7/2019 4:58:14 PM 217.4 36.1
6/7/2019 4:58:15 PM 217.0 35.7
6/7/2019 4:58:16 PM 216.6 35.3
6/7/2019 4:58:17 PM 216.3 35.0
6/7/2019 4:58:18 PM 215.9 34.6
6/7/2019 4:58:19 PM 215.7 34.4
6/7/2019 4:58:20 PM 215.4 34.1
6/7/2019 4:58:21 PM 215.2 33.9
6/7/2019 4:58:22 PM 214.9 33.6
Page 299 of 452 August 2019
APPENDIX E49: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
6/7/2019 4:58:23 PM 214.7 33.4
6/7/2019 4:58:24 PM 214.5 33.2
6/7/2019 4:58:25 PM 214.3 33.0
6/7/2019 4:58:26 PM 214.2 32.9
6/7/2019 4:58:27 PM 214.2 32.9
6/7/2019 4:58:28 PM 214.1 32.8
6/7/2019 4:58:29 PM 214.0 32.7
6/7/2019 4:58:30 PM 213.9 32.6
6/7/2019 4:58:31 PM 213.8 32.5
6/7/2019 4:58:32 PM 213.7 32.4
6/7/2019 4:58:33 PM 213.5 32.2
6/7/2019 4:58:34 PM 213.3 32.0
6/7/2019 4:58:35 PM 213.1 31.8
6/7/2019 4:58:36 PM 212.9 31.6
6/7/2019 4:58:37 PM 212.7 31.4
6/7/2019 4:58:38 PM 212.4 31.1
6/7/2019 4:58:39 PM 212.0 30.7
6/7/2019 4:58:40 PM 211.7 30.4
6/7/2019 4:58:41 PM 211.4 30.1
6/7/2019 4:58:42 PM 211.2 29.9
6/7/2019 4:58:43 PM 210.9 29.6
6/7/2019 4:58:44 PM 210.7 29.4
6/7/2019 4:58:45 PM 210.5 29.2
6/7/2019 4:58:46 PM 210.3 29.0
6/7/2019 4:58:47 PM 210.0 28.7
6/7/2019 4:58:48 PM 209.8 28.5
6/7/2019 4:58:49 PM 209.6 28.3
6/7/2019 4:58:50 PM 209.4 28.1
6/7/2019 4:58:51 PM 209.2 27.9
6/7/2019 4:58:52 PM 209.0 27.7
6/7/2019 4:58:53 PM 208.8 27.5
6/7/2019 4:58:54 PM 208.6 27.3
6/7/2019 4:58:55 PM 208.4 27.1
6/7/2019 4:58:56 PM 208.2 26.9
6/7/2019 4:58:57 PM 208.1 26.8
6/7/2019 4:58:58 PM 207.9 26.6
6/7/2019 4:58:59 PM 207.7 26.4
6/7/2019 4:59:00 PM 207.5 26.2
6/7/2019 4:59:01 PM 207.4 26.1
6/7/2019 4:59:02 PM 207.2 25.9
6/7/2019 4:59:03 PM 207.0 25.7
6/7/2019 4:59:04 PM 206.8 25.5
6/7/2019 4:59:05 PM 206.7 25.4
6/7/2019 4:59:06 PM 206.5 25.2
6/7/2019 4:59:07 PM 206.4 25.1
6/7/2019 4:59:08 PM 206.2 24.9
6/7/2019 4:59:09 PM 206.1 24.8
6/7/2019 4:59:10 PM 205.9 24.6
6/7/2019 4:59:11 PM 205.7 24.4
6/7/2019 4:59:12 PM 205.5 24.2
6/7/2019 4:59:13 PM 205.3 24.0
6/7/2019 4:59:14 PM 205.2 23.9
6/7/2019 4:59:15 PM 205.0 23.7
6/7/2019 4:59:16 PM 204.9 23.6
6/7/2019 4:59:17 PM 204.8 23.5
6/7/2019 4:59:18 PM 204.7 23.4
6/7/2019 4:59:19 PM 204.5 23.2
6/7/2019 4:59:20 PM 204.3 23.0
6/7/2019 4:59:21 PM 204.1 22.8
6/7/2019 4:59:22 PM 204.0 22.7
6/7/2019 4:59:23 PM 203.8 22.5
6/7/2019 4:59:24 PM 203.6 22.3
6/7/2019 4:59:25 PM 203.4 22.1
6/7/2019 4:59:26 PM 203.3 22.0
6/7/2019 4:59:27 PM 203.1 21.8
6/7/2019 4:59:28 PM 203.0 21.7
6/7/2019 4:59:29 PM 202.8 21.5
6/7/2019 4:59:30 PM 202.6 21.3
6/7/2019 4:59:31 PM 202.5 21.2
6/7/2019 4:59:32 PM 202.4 21.1
6/7/2019 4:59:33 PM 202.3 21.0
6/7/2019 4:59:34 PM 202.2 20.9
6/7/2019 4:59:35 PM 202.2 20.9
6/7/2019 4:59:36 PM 202.1 20.8
6/7/2019 4:59:37 PM 202.0 20.7
6/7/2019 4:59:38 PM 202.0 20.7
6/7/2019 4:59:39 PM 201.9 20.6
6/7/2019 4:59:40 PM 201.9 20.6
6/7/2019 4:59:41 PM 201.8 20.5
Page 300 of 452 August 2019
APPENDIX E49: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
6/7/2019 4:59:42 PM 201.7 20.4
6/7/2019 4:59:43 PM 201.7 20.4
6/7/2019 4:59:44 PM 201.6 20.3
6/7/2019 4:59:45 PM 201.5 20.2
6/7/2019 4:59:46 PM 201.4 20.1
6/7/2019 4:59:47 PM 201.4 20.1
6/7/2019 4:59:48 PM 201.3 20.0
6/7/2019 4:59:49 PM 201.2 19.9
6/7/2019 4:59:50 PM 201.1 19.8
6/7/2019 4:59:51 PM 201.1 19.8
6/7/2019 4:59:52 PM 201.0 19.7
6/7/2019 4:59:53 PM 200.9 19.6
6/7/2019 4:59:54 PM 200.8 19.5
6/7/2019 4:59:55 PM 200.7 19.4
6/7/2019 4:59:56 PM 200.6 19.3
6/7/2019 4:59:57 PM 200.5 19.2
6/7/2019 4:59:58 PM 200.4 19.1
6/7/2019 4:59:59 PM 200.3 19.0
6/7/2019 5:00:00 PM 200.2 18.9
6/7/2019 5:00:01 PM 200.0 18.7
6/7/2019 5:00:02 PM 199.9 18.6
6/7/2019 5:00:03 PM 199.8 18.5
6/7/2019 5:00:04 PM 199.7 18.4
6/7/2019 5:00:05 PM 199.6 18.3
6/7/2019 5:00:06 PM 199.5 18.2
6/7/2019 5:00:07 PM 199.4 18.1
6/7/2019 5:00:08 PM 199.3 18.0
6/7/2019 5:00:09 PM 199.2 17.9
6/7/2019 5:00:10 PM 199.1 17.8
6/7/2019 5:00:11 PM 199.0 17.7
6/7/2019 5:00:12 PM 198.9 17.6
6/7/2019 5:00:13 PM 198.8 17.5
6/7/2019 5:00:14 PM 198.8 17.5
6/7/2019 5:00:15 PM 198.7 17.4
6/7/2019 5:00:16 PM 198.6 17.3
6/7/2019 5:00:17 PM 198.6 17.3
6/7/2019 5:00:18 PM 198.5 17.2
6/7/2019 5:00:19 PM 198.4 17.1
6/7/2019 5:00:20 PM 198.3 17.0
6/7/2019 5:00:21 PM 198.3 17.0
6/7/2019 5:00:22 PM 198.2 16.9
6/7/2019 5:00:23 PM 198.1 16.8
6/7/2019 5:00:24 PM 198.1 16.8
6/7/2019 5:00:25 PM 198.0 16.7
6/7/2019 5:00:26 PM 197.9 16.6
6/7/2019 5:00:27 PM 197.9 16.6
6/7/2019 5:00:28 PM 197.8 16.5
6/7/2019 5:00:29 PM 197.7 16.4
6/7/2019 5:00:30 PM 197.7 16.4
6/7/2019 5:00:31 PM 197.6 16.3
6/7/2019 5:00:32 PM 197.6 16.3
6/7/2019 5:00:33 PM 197.5 16.2
6/7/2019 5:00:34 PM 197.4 16.1
6/7/2019 5:00:35 PM 197.3 16.0
6/7/2019 5:00:36 PM 197.2 15.9
6/7/2019 5:00:37 PM 197.1 15.8
6/7/2019 5:00:38 PM 197.0 15.7
6/7/2019 5:00:39 PM 196.9 15.6
6/7/2019 5:00:40 PM 196.8 15.5
6/7/2019 5:00:41 PM 196.7 15.4
6/7/2019 5:00:42 PM 196.7 15.4
6/7/2019 5:00:43 PM 196.6 15.3
6/7/2019 5:00:44 PM 196.5 15.2
6/7/2019 5:00:45 PM 196.4 15.1
6/7/2019 5:00:46 PM 196.3 15.0
6/7/2019 5:00:47 PM 196.3 15.0
6/7/2019 5:00:48 PM 196.2 14.9
6/7/2019 5:00:49 PM 196.2 14.9
6/7/2019 5:00:50 PM 196.1 14.8
6/7/2019 5:00:51 PM 196.1 14.8
6/7/2019 5:00:52 PM 196.0 14.7
6/7/2019 5:00:53 PM 196.0 14.7
6/7/2019 5:00:54 PM 196.0 14.7
6/7/2019 5:00:55 PM 195.9 14.6
6/7/2019 5:00:56 PM 195.9 14.6
6/7/2019 5:00:57 PM 195.8 14.5
6/7/2019 5:00:58 PM 195.7 14.4
6/7/2019 5:00:59 PM 195.7 14.4
6/7/2019 5:01:00 PM 195.6 14.3
Page 301 of 452 August 2019
APPENDIX E49: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
6/7/2019 5:01:01 PM 195.5 14.2
6/7/2019 5:01:02 PM 195.4 14.1
6/7/2019 5:01:03 PM 195.4 14.1
6/7/2019 5:01:04 PM 195.3 14.0
6/7/2019 5:01:05 PM 195.2 13.9
6/7/2019 5:01:06 PM 195.1 13.8
6/7/2019 5:01:07 PM 195.1 13.8
6/7/2019 5:01:08 PM 195.0 13.7
6/7/2019 5:01:09 PM 194.9 13.6
6/7/2019 5:01:10 PM 194.9 13.6
6/7/2019 5:01:11 PM 194.8 13.5
6/7/2019 5:01:12 PM 194.7 13.4
6/7/2019 5:01:13 PM 194.6 13.3
6/7/2019 5:01:14 PM 194.5 13.2
6/7/2019 5:01:15 PM 194.4 13.1
6/7/2019 5:01:16 PM 194.3 13.0
6/7/2019 5:01:17 PM 194.2 12.9
6/7/2019 5:01:18 PM 194.1 12.8
6/7/2019 5:01:19 PM 194.0 12.7
6/7/2019 5:01:20 PM 193.9 12.6
6/7/2019 5:01:21 PM 193.8 12.5
6/7/2019 5:01:22 PM 193.7 12.4
6/7/2019 5:01:23 PM 193.6 12.3
6/7/2019 5:01:24 PM 193.6 12.3
6/7/2019 5:01:25 PM 193.5 12.2
6/7/2019 5:01:26 PM 193.4 12.1
6/7/2019 5:01:27 PM 193.4 12.1
6/7/2019 5:01:28 PM 193.4 12.1
6/7/2019 5:01:29 PM 193.3 12.0
6/7/2019 5:01:30 PM 193.3 12.0
6/7/2019 5:01:31 PM 193.3 12.0
6/7/2019 5:01:32 PM 193.2 11.9
6/7/2019 5:01:33 PM 193.2 11.9
6/7/2019 5:01:34 PM 193.1 11.8
6/7/2019 5:01:35 PM 193.1 11.8
6/7/2019 5:01:36 PM 193.1 11.8
6/7/2019 5:01:37 PM 193.0 11.7
6/7/2019 5:01:38 PM 193.0 11.7
6/7/2019 5:01:39 PM 193.0 11.7
6/7/2019 5:01:40 PM 192.9 11.6
6/7/2019 5:01:41 PM 192.8 11.5
6/7/2019 5:01:42 PM 192.8 11.5
6/7/2019 5:01:43 PM 192.7 11.4
6/7/2019 5:01:44 PM 192.7 11.4
6/7/2019 5:01:45 PM 192.6 11.3
6/7/2019 5:01:46 PM 192.6 11.3
6/7/2019 5:01:47 PM 192.5 11.2
6/7/2019 5:01:48 PM 192.5 11.2
6/7/2019 5:01:49 PM 192.4 11.1
6/7/2019 5:01:50 PM 192.4 11.1
6/7/2019 5:01:51 PM 192.3 11.0
6/7/2019 5:01:52 PM 192.3 11.0
6/7/2019 5:01:53 PM 192.3 11.0
6/7/2019 5:01:54 PM 192.2 10.9
6/7/2019 5:01:55 PM 192.2 10.9
6/7/2019 5:01:56 PM 192.1 10.8
6/7/2019 5:01:57 PM 192.1 10.8
6/7/2019 5:01:58 PM 192.0 10.7
6/7/2019 5:01:59 PM 192.0 10.7
6/7/2019 5:02:00 PM 191.9 10.6
6/7/2019 5:02:01 PM 191.9 10.6
6/7/2019 5:02:02 PM 191.8 10.5
6/7/2019 5:02:03 PM 191.7 10.4
6/7/2019 5:02:04 PM 191.7 10.4
6/7/2019 5:02:05 PM 191.6 10.3
6/7/2019 5:02:06 PM 191.5 10.2
6/7/2019 5:02:07 PM 191.5 10.2
6/7/2019 5:02:08 PM 191.4 10.1
6/7/2019 5:02:09 PM 191.4 10.1
6/7/2019 5:02:10 PM 191.4 10.1
6/7/2019 5:02:11 PM 191.3 10.0
6/7/2019 5:02:12 PM 191.3 10.0
6/7/2019 5:02:13 PM 191.2 9.9
6/7/2019 5:02:14 PM 191.2 9.9
6/7/2019 5:02:15 PM 191.1 9.8
6/7/2019 5:02:16 PM 191.1 9.8
6/7/2019 5:02:17 PM 191.0 9.7
6/7/2019 5:02:18 PM 190.9 9.6
6/7/2019 5:02:19 PM 190.8 9.5
Page 302 of 452 August 2019
APPENDIX E49: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B2 TEST-2 Data Log
6/7/2019 5:02:20 PM 190.8 9.5
6/7/2019 5:02:21 PM 190.7 9.4
6/7/2019 5:02:22 PM 190.6 9.3
6/7/2019 5:02:23 PM 190.5 9.2
6/7/2019 5:02:24 PM 190.4 9.1
6/7/2019 5:02:25 PM 190.4 9.1
6/7/2019 5:02:26 PM 190.3 9.0
6/7/2019 5:02:27 PM 190.2 8.9
6/7/2019 5:02:28 PM 190.2 8.9
6/7/2019 5:02:29 PM 190.1 8.8
6/7/2019 5:02:30 PM 190.1 8.8
6/7/2019 5:02:31 PM 190.0 8.7
6/7/2019 5:02:32 PM 190.0 8.7
6/7/2019 5:02:33 PM 189.9 8.6
6/7/2019 5:02:34 PM 189.9 8.6
6/7/2019 5:02:35 PM 189.8 8.5
6/7/2019 5:02:36 PM 189.8 8.5
6/7/2019 5:02:37 PM 189.7 8.4
6/7/2019 5:02:38 PM 189.7 8.4
6/7/2019 5:02:39 PM 189.6 8.3
6/7/2019 5:02:40 PM 189.6 8.3
6/7/2019 5:02:41 PM 189.5 8.2
6/7/2019 5:02:42 PM 189.5 8.2
6/7/2019 5:02:43 PM 189.4 8.1
6/7/2019 5:02:44 PM 189.4 8.1
6/7/2019 5:02:45 PM 189.4 8.1
6/7/2019 5:02:46 PM 189.3 8.0
6/7/2019 5:02:47 PM 189.3 8.0
6/7/2019 5:02:48 PM 189.3 8.0
6/7/2019 5:02:49 PM 189.3 8.0
6/7/2019 5:02:50 PM 189.2 7.9
6/7/2019 5:02:51 PM 189.2 7.9
6/7/2019 5:02:52 PM 189.1 7.8
6/7/2019 5:02:53 PM 189.1 7.8
6/7/2019 5:02:54 PM 189.0 7.7
6/7/2019 5:02:55 PM 189.0 7.7
6/7/2019 5:02:56 PM 188.9 7.6
6/7/2019 5:02:57 PM 188.9 7.6
6/7/2019 5:02:58 PM 188.8 7.5
6/7/2019 5:02:59 PM 188.7 7.4
6/7/2019 5:03:00 PM 188.7 7.4
6/7/2019 5:03:01 PM 188.6 7.3
6/7/2019 5:03:02 PM 188.6 7.3
6/7/2019 5:03:03 PM 188.5 7.2
6/7/2019 5:03:04 PM 188.5 7.2
6/7/2019 5:03:05 PM 188.4 7.1
6/7/2019 5:03:06 PM 188.4 7.1
6/7/2019 5:03:07 PM 188.4 7.1
6/7/2019 5:03:08 PM 188.3 7.0
6/7/2019 5:03:09 PM 188.3 7.0
6/7/2019 5:03:10 PM 188.3 7.0
6/7/2019 5:03:11 PM 188.2 6.9
6/7/2019 5:03:12 PM 188.2 6.9
6/7/2019 5:03:13 PM 188.2 6.9
6/7/2019 5:03:14 PM 188.1 6.8
6/7/2019 5:03:15 PM 188.0 6.7
6/7/2019 5:03:16 PM 188.0 6.7
6/7/2019 5:03:17 PM 187.9 6.6
6/7/2019 5:03:18 PM 187.9 6.6
6/7/2019 5:03:19 PM 187.8 6.5
6/7/2019 5:03:20 PM 187.8 6.5
6/7/2019 5:03:21 PM 187.8 6.5
6/7/2019 5:03:22 PM 187.7 6.4
6/7/2019 5:03:23 PM 187.7 6.4
Page 303 of 452 August 2019
APPENDIX E49: SALT DILUTION GAUGING SUMMARY
SEEP-B2 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-B2 TEST-2 1630
SEEP-B2 TEST-2 NR
SEEP-B2 TEST-2 NR
EC Reading
(µS/cms)
SEEP-B2 TEST-2 721
SEEP-B2 TEST-2 2,061
SEEP-B2 TEST-2 16,708
SEEP-B2 TEST-2 121,612
q 300,000
K 1.2207
0.8
12.7
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
NR Not recorded
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
24.7
24.6
(°C)
Temperature
(µS/cms)
(µS/cms)
(µS/cms)
Table E3 SEEP-B2 TEST-2 YSI Salt Dilution Calibration Data
(µS/cms) (°C)
Table E2 SEEP-B2 TEST-2 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
10,000 25.1
176.7 20.5
173.8 20.5
172.8 20.5
Average (post-test)190.7 (µS/cms)
Location Calibration
Concentration
GPM
100,000 25
Table E4 SEEP-B2 TEST-2 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
100
1,000
174.4
174.4
181.3
Average
Geometric Mean
Average (pre-test)
Integral of Conductivity
Data Curve
SUM:Δt(E
Ct-ECbkg)459,080.4 (s) . (µS/cms)
Calculated Flow Rate Q
L/s
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 304 of 452 August 2019
APPENDIX E50: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/6/2019 12:50:17 PM 56.8 -
2/6/2019 12:50:18 PM 56.8 -
2/6/2019 12:50:19 PM 56.8 -
2/6/2019 12:50:20 PM 56.8 -
2/6/2019 12:50:21 PM 56.7 -
2/6/2019 12:50:22 PM 56.7 -
2/6/2019 12:50:23 PM 56.7 -
2/6/2019 12:50:24 PM 56.7 -
2/6/2019 12:50:25 PM 56.6 -
2/6/2019 12:50:26 PM 56.6 -
2/6/2019 12:50:27 PM 56.5 -
2/6/2019 12:50:28 PM 56.5 -
2/6/2019 12:50:29 PM 56.4 -
2/6/2019 12:50:30 PM 56.4 -
2/6/2019 12:50:31 PM 56.4 -
2/6/2019 12:50:32 PM 56.4 -
2/6/2019 12:50:33 PM 56.4 -
2/6/2019 12:50:34 PM 56.4 -
2/6/2019 12:50:35 PM 56.4 -
2/6/2019 12:50:36 PM 56.4 -
2/6/2019 12:50:37 PM 56.4 -
2/6/2019 12:50:38 PM 56.4 -
2/6/2019 12:50:39 PM 56.4 -
2/6/2019 12:50:40 PM 56.4 -
2/6/2019 12:50:41 PM 56.4 -
2/6/2019 12:50:42 PM 56.4 -
2/6/2019 12:50:43 PM 56.3 -
2/6/2019 12:50:44 PM 56.3 -
2/6/2019 12:50:45 PM 56.2 -
2/6/2019 12:50:46 PM 56.2 -
2/6/2019 12:50:47 PM 56.1 -
2/6/2019 12:50:48 PM 56.1 -
2/6/2019 12:50:49 PM 56.1 -
2/6/2019 12:50:50 PM 56.1 -
2/6/2019 12:50:51 PM 56.0 -
2/6/2019 12:50:52 PM 56.0 -
2/6/2019 12:50:53 PM 56.0 -
2/6/2019 12:50:54 PM 56.0 -
2/6/2019 12:50:55 PM 56.0 -
2/6/2019 12:50:56 PM 56.0 -
2/6/2019 12:50:57 PM 56.0 -
2/6/2019 12:50:58 PM 56.0 -
2/6/2019 12:50:59 PM 56.0 -
2/6/2019 12:51:00 PM 56.0 -
2/6/2019 12:51:01 PM 56.0 -
2/6/2019 12:51:02 PM 56.0 -
2/6/2019 12:51:03 PM 56.0 -
2/6/2019 12:51:04 PM 56.0 -
2/6/2019 12:51:05 PM 55.9 -
2/6/2019 12:51:06 PM 55.9 -
2/6/2019 12:51:07 PM 55.9 -
2/6/2019 12:51:08 PM 55.9 -
2/6/2019 12:51:09 PM 55.9 -
2/6/2019 12:51:10 PM 55.9 -
2/6/2019 12:51:11 PM 55.9 -
2/6/2019 12:51:12 PM 55.9 -
2/6/2019 12:51:13 PM 55.9 -
2/6/2019 12:51:14 PM 55.8 -
2/6/2019 12:51:15 PM 55.8 -
2/6/2019 12:51:16 PM 55.8 -
2/6/2019 12:51:17 PM 55.8 -
2/6/2019 12:51:18 PM 55.8 -
2/6/2019 12:51:19 PM 55.8 -
2/6/2019 12:51:20 PM 55.8 -
2/6/2019 12:51:21 PM 55.7 -
2/6/2019 12:51:22 PM 55.7 -
2/6/2019 12:51:23 PM 55.7 -
2/6/2019 12:51:24 PM 55.7 -
2/6/2019 12:51:25 PM 55.6 -
2/6/2019 12:51:26 PM 55.6 -
Table E1 SEEP-B3 TEST-1 Data Log
Page 305 of 452 August 2019
APPENDIX E50: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-1 Data Log
2/6/2019 12:51:27 PM 55.6 -
2/6/2019 12:51:28 PM 55.6 -
2/6/2019 12:51:29 PM 55.6 -
2/6/2019 12:51:30 PM 55.6 -
2/6/2019 12:51:31 PM 55.6 -
2/6/2019 12:51:32 PM 55.6 -
2/6/2019 12:51:33 PM 55.6 -
2/6/2019 12:51:34 PM 55.6 -
2/6/2019 12:51:35 PM 55.6 -
2/6/2019 12:51:36 PM 55.6 -
2/6/2019 12:51:37 PM 55.6 -
2/6/2019 12:51:38 PM 55.6 -
2/6/2019 12:51:39 PM 55.7 -
2/6/2019 12:51:40 PM 55.7 -
2/6/2019 12:51:41 PM 55.7 -
2/6/2019 12:51:42 PM 55.7 -
2/6/2019 12:51:43 PM 55.7 -
2/6/2019 12:51:44 PM 55.7 -
2/6/2019 12:51:45 PM 55.7 -
2/6/2019 12:51:46 PM 55.8 -
2/6/2019 12:51:47 PM 55.8 -
2/6/2019 12:51:48 PM 56.0 -
2/6/2019 12:51:49 PM 56.2 -0.3
2/6/2019 12:51:50 PM 56.5 0.0
2/6/2019 12:51:51 PM 57.1 0.6
2/6/2019 12:51:52 PM 57.7 1.2
2/6/2019 12:51:53 PM 58.9 2.4
2/6/2019 12:51:54 PM 60.8 4.3
2/6/2019 12:51:55 PM 64.1 7.6
2/6/2019 12:51:56 PM 67.2 10.7
2/6/2019 12:51:57 PM 71.0 14.5
2/6/2019 12:51:58 PM 74.5 18.0
2/6/2019 12:51:59 PM 78.3 21.8
2/6/2019 12:52:00 PM 81.5 25.0
2/6/2019 12:52:01 PM 84.5 28.0
2/6/2019 12:52:02 PM 91.0 34.5
2/6/2019 12:52:03 PM 96.4 39.9
2/6/2019 12:52:04 PM 153.3 96.8
2/6/2019 12:52:05 PM 176.5 120.0
2/6/2019 12:52:06 PM 184.7 128.2
2/6/2019 12:52:07 PM 183.3 126.8
2/6/2019 12:52:08 PM 179.2 122.7
2/6/2019 12:52:09 PM 178.3 121.8
2/6/2019 12:52:10 PM 181.5 125.0
2/6/2019 12:52:11 PM 183.8 127.3
2/6/2019 12:52:12 PM 186.2 129.7
2/6/2019 12:52:13 PM 263.4 206.9
2/6/2019 12:52:14 PM 326.4 269.9
2/6/2019 12:52:15 PM 350.7 294.2
2/6/2019 12:52:16 PM 351.1 294.6
2/6/2019 12:52:17 PM 360.8 304.3
2/6/2019 12:52:18 PM 369.8 313.3
2/6/2019 12:52:19 PM 439.0 382.5
2/6/2019 12:52:20 PM 447.9 391.4
2/6/2019 12:52:21 PM 434.8 378.3
2/6/2019 12:52:22 PM 480.4 423.9
2/6/2019 12:52:23 PM 567.6 511.1
2/6/2019 12:52:24 PM 579.8 523.3
2/6/2019 12:52:25 PM 651.5 595.0
2/6/2019 12:52:26 PM 789.9 733.4
2/6/2019 12:52:27 PM 824.4 767.9
2/6/2019 12:52:28 PM 755.0 698.5
2/6/2019 12:52:29 PM 752.7 696.2
2/6/2019 12:52:30 PM 762.9 706.4
2/6/2019 12:52:31 PM 920.7 864.2
2/6/2019 12:52:32 PM 948.8 892.3
2/6/2019 12:52:33 PM 1012.0 955.5
2/6/2019 12:52:34 PM 1052.5 996.0
2/6/2019 12:52:35 PM 1086.9 1030.4
2/6/2019 12:52:36 PM 1227.8 1171.3
2/6/2019 12:52:37 PM 1351.8 1295.3
2/6/2019 12:52:38 PM 1377.3 1320.8
2/6/2019 12:52:39 PM 1398.3 1341.8
2/6/2019 12:52:40 PM 1406.5 1350.0
2/6/2019 12:52:41 PM 1407.4 1350.9
2/6/2019 12:52:42 PM 1421.0 1364.5
2/6/2019 12:52:43 PM 1426.8 1370.3
Page 306 of 452 August 2019
APPENDIX E50: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-1 Data Log
2/6/2019 12:52:44 PM 1431.4 1374.9
2/6/2019 12:52:45 PM 1543.6 1487.1
2/6/2019 12:52:46 PM 1551.5 1495.0
2/6/2019 12:52:47 PM 1550.5 1494.0
2/6/2019 12:52:48 PM 1542.2 1485.7
2/6/2019 12:52:49 PM 1551.4 1494.9
2/6/2019 12:52:50 PM 1556.2 1499.7
2/6/2019 12:52:51 PM 1560.2 1503.7
2/6/2019 12:52:52 PM 1569.2 1512.7
2/6/2019 12:52:53 PM 1658.4 1601.9
2/6/2019 12:52:54 PM 1680.1 1623.6
2/6/2019 12:52:55 PM 1692.5 1636.0
2/6/2019 12:52:56 PM 1686.0 1629.5
2/6/2019 12:52:57 PM 1676.3 1619.8
2/6/2019 12:52:58 PM 1683.0 1626.5
2/6/2019 12:52:59 PM 1812.7 1756.2
2/6/2019 12:53:00 PM 1834.6 1778.1
2/6/2019 12:53:01 PM 1833.1 1776.6
2/6/2019 12:53:02 PM 1831.6 1775.1
2/6/2019 12:53:03 PM 1840.1 1783.6
2/6/2019 12:53:04 PM 1867.1 1810.6
2/6/2019 12:53:05 PM 1891.0 1834.5
2/6/2019 12:53:06 PM 1903.2 1846.7
2/6/2019 12:53:07 PM 1910.5 1854.0
2/6/2019 12:53:08 PM 1918.8 1862.3
2/6/2019 12:53:09 PM 1930.0 1873.5
2/6/2019 12:53:10 PM 1938.6 1882.1
2/6/2019 12:53:11 PM 1946.8 1890.3
2/6/2019 12:53:12 PM 1953.4 1896.9
2/6/2019 12:53:13 PM 1960.5 1904.0
2/6/2019 12:53:14 PM 1965.8 1909.3
2/6/2019 12:53:15 PM 1975.5 1919.0
2/6/2019 12:53:16 PM 1988.2 1931.7
2/6/2019 12:53:17 PM 1998.0 1941.5
2/6/2019 12:53:18 PM 2005.1 1948.6
2/6/2019 12:53:19 PM 2012.4 1955.9
2/6/2019 12:53:20 PM 2019.1 1962.6
2/6/2019 12:53:21 PM 2022.8 1966.3
2/6/2019 12:53:22 PM 2023.5 1967.0
2/6/2019 12:53:23 PM 2023.3 1966.8
2/6/2019 12:53:24 PM 2023.5 1967.0
2/6/2019 12:53:25 PM 2023.0 1966.5
2/6/2019 12:53:26 PM 2020.9 1964.4
2/6/2019 12:53:27 PM 2018.9 1962.4
2/6/2019 12:53:28 PM 2016.3 1959.8
2/6/2019 12:53:29 PM 2014.1 1957.6
2/6/2019 12:53:30 PM 2011.2 1954.7
2/6/2019 12:53:31 PM 2008.0 1951.5
2/6/2019 12:53:32 PM 2003.7 1947.2
2/6/2019 12:53:33 PM 1999.5 1943.0
2/6/2019 12:53:34 PM 1994.1 1937.6
2/6/2019 12:53:35 PM 1988.6 1932.1
2/6/2019 12:53:36 PM 1980.1 1923.6
2/6/2019 12:53:37 PM 1971.3 1914.8
2/6/2019 12:53:38 PM 1863.7 1807.2
2/6/2019 12:53:39 PM 1863.6 1807.1
2/6/2019 12:53:40 PM 1858.3 1801.8
2/6/2019 12:53:41 PM 1852.2 1795.7
2/6/2019 12:53:42 PM 1812.2 1755.7
2/6/2019 12:53:43 PM 1792.9 1736.4
2/6/2019 12:53:44 PM 1785.1 1728.6
2/6/2019 12:53:45 PM 1779.0 1722.5
2/6/2019 12:53:46 PM 1770.4 1713.9
2/6/2019 12:53:47 PM 1764.8 1708.3
2/6/2019 12:53:48 PM 1760.3 1703.8
2/6/2019 12:53:49 PM 1755.8 1699.3
2/6/2019 12:53:50 PM 1749.6 1693.1
2/6/2019 12:53:51 PM 1636.6 1580.1
2/6/2019 12:53:52 PM 1599.8 1543.3
2/6/2019 12:53:53 PM 1587.5 1531.0
2/6/2019 12:53:54 PM 1601.0 1544.5
2/6/2019 12:53:55 PM 1605.2 1548.7
2/6/2019 12:53:56 PM 1606.4 1549.9
2/6/2019 12:53:57 PM 1606.2 1549.7
2/6/2019 12:53:58 PM 1603.0 1546.5
2/6/2019 12:53:59 PM 1592.8 1536.3
2/6/2019 12:54:00 PM 1580.3 1523.8
2/6/2019 12:54:01 PM 1571.2 1514.7
2/6/2019 12:54:02 PM 1564.1 1507.6
Page 307 of 452 August 2019
APPENDIX E50: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-1 Data Log
2/6/2019 12:54:03 PM 1560.2 1503.7
2/6/2019 12:54:04 PM 1555.2 1498.7
2/6/2019 12:54:05 PM 1428.7 1372.2
2/6/2019 12:54:06 PM 1425.0 1368.5
2/6/2019 12:54:07 PM 1409.4 1352.9
2/6/2019 12:54:08 PM 1389.7 1333.2
2/6/2019 12:54:09 PM 1375.4 1318.9
2/6/2019 12:54:10 PM 1376.8 1320.3
2/6/2019 12:54:11 PM 1378.9 1322.4
2/6/2019 12:54:12 PM 1377.7 1321.2
2/6/2019 12:54:13 PM 1374.0 1317.5
2/6/2019 12:54:14 PM 1371.2 1314.7
2/6/2019 12:54:15 PM 1367.5 1311.0
2/6/2019 12:54:16 PM 1364.1 1307.6
2/6/2019 12:54:17 PM 1359.5 1303.0
2/6/2019 12:54:18 PM 1355.1 1298.6
2/6/2019 12:54:19 PM 1352.2 1295.7
2/6/2019 12:54:20 PM 1349.8 1293.3
2/6/2019 12:54:21 PM 1344.6 1288.1
2/6/2019 12:54:22 PM 1261.0 1204.5
2/6/2019 12:54:23 PM 1241.4 1184.9
2/6/2019 12:54:24 PM 1220.5 1164.0
2/6/2019 12:54:25 PM 1209.8 1153.3
2/6/2019 12:54:26 PM 1190.0 1133.5
2/6/2019 12:54:27 PM 1176.4 1119.9
2/6/2019 12:54:28 PM 1173.1 1116.6
2/6/2019 12:54:29 PM 1066.2 1009.7
2/6/2019 12:54:30 PM 1060.7 1004.2
2/6/2019 12:54:31 PM 1044.0 987.5
2/6/2019 12:54:32 PM 1040.0 983.5
2/6/2019 12:54:33 PM 1017.1 960.6
2/6/2019 12:54:34 PM 1003.4 946.9
2/6/2019 12:54:35 PM 1001.6 945.1
2/6/2019 12:54:36 PM 999.4 942.9
2/6/2019 12:54:37 PM 992.1 935.6
2/6/2019 12:54:38 PM 985.8 929.3
2/6/2019 12:54:39 PM 899.3 842.8
2/6/2019 12:54:40 PM 907.6 851.1
2/6/2019 12:54:41 PM 919.5 863.0
2/6/2019 12:54:42 PM 910.2 853.7
2/6/2019 12:54:43 PM 884.2 827.7
2/6/2019 12:54:44 PM 874.9 818.4
2/6/2019 12:54:45 PM 774.7 718.2
2/6/2019 12:54:46 PM 762.1 705.6
2/6/2019 12:54:47 PM 734.8 678.3
2/6/2019 12:54:48 PM 724.9 668.4
2/6/2019 12:54:49 PM 714.9 658.4
2/6/2019 12:54:50 PM 709.9 653.4
2/6/2019 12:54:51 PM 707.2 650.7
2/6/2019 12:54:52 PM 705.3 648.8
2/6/2019 12:54:53 PM 702.1 645.6
2/6/2019 12:54:54 PM 695.2 638.7
2/6/2019 12:54:55 PM 691.3 634.8
2/6/2019 12:54:56 PM 606.3 549.8
2/6/2019 12:54:57 PM 621.2 564.7
2/6/2019 12:54:58 PM 608.8 552.3
2/6/2019 12:54:59 PM 607.5 551.0
2/6/2019 12:55:00 PM 604.3 547.8
2/6/2019 12:55:01 PM 599.2 542.7
2/6/2019 12:55:02 PM 592.1 535.6
2/6/2019 12:55:03 PM 585.2 528.7
2/6/2019 12:55:04 PM 579.9 523.4
2/6/2019 12:55:05 PM 577.1 520.6
2/6/2019 12:55:06 PM 575.1 518.6
2/6/2019 12:55:07 PM 573.3 516.8
2/6/2019 12:55:08 PM 570.4 513.9
2/6/2019 12:55:09 PM 567.2 510.7
2/6/2019 12:55:10 PM 517.7 461.2
2/6/2019 12:55:11 PM 518.4 461.9
2/6/2019 12:55:12 PM 504.2 447.7
2/6/2019 12:55:13 PM 493.0 436.5
2/6/2019 12:55:14 PM 484.2 427.7
2/6/2019 12:55:15 PM 479.6 423.1
2/6/2019 12:55:16 PM 477.0 420.5
2/6/2019 12:55:17 PM 474.4 417.9
2/6/2019 12:55:18 PM 472.3 415.8
2/6/2019 12:55:19 PM 471.5 415.0
2/6/2019 12:55:20 PM 470.5 414.0
2/6/2019 12:55:21 PM 469.3 412.8
Page 308 of 452 August 2019
APPENDIX E50: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-1 Data Log
2/6/2019 12:55:22 PM 468.2 411.7
2/6/2019 12:55:23 PM 467.9 411.4
2/6/2019 12:55:24 PM 467.4 410.9
2/6/2019 12:55:25 PM 466.8 410.3
2/6/2019 12:55:26 PM 465.8 409.3
2/6/2019 12:55:27 PM 463.2 406.7
2/6/2019 12:55:28 PM 459.7 403.2
2/6/2019 12:55:29 PM 456.2 399.7
2/6/2019 12:55:30 PM 452.0 395.5
2/6/2019 12:55:31 PM 448.3 391.8
2/6/2019 12:55:32 PM 443.6 387.1
2/6/2019 12:55:33 PM 439.1 382.6
2/6/2019 12:55:34 PM 433.9 377.4
2/6/2019 12:55:35 PM 429.7 373.2
2/6/2019 12:55:36 PM 424.3 367.8
2/6/2019 12:55:37 PM 419.4 362.9
2/6/2019 12:55:38 PM 414.2 357.7
2/6/2019 12:55:39 PM 409.3 352.8
2/6/2019 12:55:40 PM 405.1 348.6
2/6/2019 12:55:41 PM 400.0 343.5
2/6/2019 12:55:42 PM 395.8 339.3
2/6/2019 12:55:43 PM 391.2 334.7
2/6/2019 12:55:44 PM 387.1 330.6
2/6/2019 12:55:45 PM 382.1 325.6
2/6/2019 12:55:46 PM 377.7 321.2
2/6/2019 12:55:47 PM 372.5 316.0
2/6/2019 12:55:48 PM 367.5 311.0
2/6/2019 12:55:49 PM 361.6 305.1
2/6/2019 12:55:50 PM 356.5 300.0
2/6/2019 12:55:51 PM 350.2 293.7
2/6/2019 12:55:52 PM 344.6 288.1
2/6/2019 12:55:53 PM 338.9 282.4
2/6/2019 12:55:54 PM 334.6 278.1
2/6/2019 12:55:55 PM 329.6 273.1
2/6/2019 12:55:56 PM 325.2 268.7
2/6/2019 12:55:57 PM 320.2 263.7
2/6/2019 12:55:58 PM 316.1 259.6
2/6/2019 12:55:59 PM 311.7 255.2
2/6/2019 12:56:00 PM 308.3 251.8
2/6/2019 12:56:01 PM 304.6 248.1
2/6/2019 12:56:02 PM 301.6 245.1
2/6/2019 12:56:03 PM 298.4 241.9
2/6/2019 12:56:04 PM 295.8 239.3
2/6/2019 12:56:05 PM 292.9 236.4
2/6/2019 12:56:06 PM 290.1 233.6
2/6/2019 12:56:07 PM 287.2 230.7
2/6/2019 12:56:08 PM 284.8 228.3
2/6/2019 12:56:09 PM 282.1 225.6
2/6/2019 12:56:10 PM 279.7 223.2
2/6/2019 12:56:11 PM 276.9 220.4
2/6/2019 12:56:12 PM 274.1 217.6
2/6/2019 12:56:13 PM 270.8 214.3
2/6/2019 12:56:14 PM 268.0 211.5
2/6/2019 12:56:15 PM 264.8 208.3
2/6/2019 12:56:16 PM 261.9 205.4
2/6/2019 12:56:17 PM 258.7 202.2
2/6/2019 12:56:18 PM 256.0 199.5
2/6/2019 12:56:19 PM 253.8 197.3
2/6/2019 12:56:20 PM 251.6 195.1
2/6/2019 12:56:21 PM 249.7 193.2
2/6/2019 12:56:22 PM 247.6 191.1
2/6/2019 12:56:23 PM 245.8 189.3
2/6/2019 12:56:24 PM 244.1 187.6
2/6/2019 12:56:25 PM 242.7 186.2
2/6/2019 12:56:26 PM 240.8 184.3
2/6/2019 12:56:27 PM 238.7 182.2
2/6/2019 12:56:28 PM 236.1 179.6
2/6/2019 12:56:29 PM 233.8 177.3
2/6/2019 12:56:30 PM 231.1 174.6
2/6/2019 12:56:31 PM 228.5 172.0
2/6/2019 12:56:32 PM 225.4 168.9
2/6/2019 12:56:33 PM 222.7 166.2
2/6/2019 12:56:34 PM 220.0 163.5
2/6/2019 12:56:35 PM 217.9 161.4
2/6/2019 12:56:36 PM 215.7 159.2
2/6/2019 12:56:37 PM 213.8 157.3
2/6/2019 12:56:38 PM 211.9 155.4
2/6/2019 12:56:39 PM 210.5 154.0
2/6/2019 12:56:40 PM 209.1 152.6
Page 309 of 452 August 2019
APPENDIX E50: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-1 Data Log
2/6/2019 12:56:41 PM 208.0 151.5
2/6/2019 12:56:42 PM 206.5 150.0
2/6/2019 12:56:43 PM 205.2 148.7
2/6/2019 12:56:44 PM 203.8 147.3
2/6/2019 12:56:45 PM 202.7 146.2
2/6/2019 12:56:46 PM 201.5 145.0
2/6/2019 12:56:47 PM 200.1 143.6
2/6/2019 12:56:48 PM 198.0 141.5
2/6/2019 12:56:49 PM 196.2 139.7
2/6/2019 12:56:50 PM 194.1 137.6
2/6/2019 12:56:51 PM 192.3 135.8
2/6/2019 12:56:52 PM 190.1 133.6
2/6/2019 12:56:53 PM 188.4 131.9
2/6/2019 12:56:54 PM 186.8 130.3
2/6/2019 12:56:55 PM 185.5 129.0
2/6/2019 12:56:56 PM 184.0 127.5
2/6/2019 12:56:57 PM 182.5 126.0
2/6/2019 12:56:58 PM 181.0 124.5
2/6/2019 12:56:59 PM 179.4 122.9
2/6/2019 12:57:00 PM 178.0 121.5
2/6/2019 12:57:01 PM 176.7 120.2
2/6/2019 12:57:02 PM 175.6 119.1
2/6/2019 12:57:03 PM 174.5 118.0
2/6/2019 12:57:04 PM 173.6 117.1
2/6/2019 12:57:05 PM 172.6 116.1
2/6/2019 12:57:06 PM 171.6 115.1
2/6/2019 12:57:07 PM 170.5 114.0
2/6/2019 12:57:08 PM 169.5 113.0
2/6/2019 12:57:09 PM 168.5 112.0
2/6/2019 12:57:10 PM 167.8 111.3
2/6/2019 12:57:11 PM 166.9 110.4
2/6/2019 12:57:12 PM 166.1 109.6
2/6/2019 12:57:13 PM 165.4 108.9
2/6/2019 12:57:14 PM 164.7 108.2
2/6/2019 12:57:15 PM 163.8 107.3
2/6/2019 12:57:16 PM 162.9 106.4
2/6/2019 12:57:17 PM 161.9 105.4
2/6/2019 12:57:18 PM 161.1 104.6
2/6/2019 12:57:19 PM 160.1 103.6
2/6/2019 12:57:20 PM 159.2 102.7
2/6/2019 12:57:21 PM 158.2 101.7
2/6/2019 12:57:22 PM 157.3 100.8
2/6/2019 12:57:23 PM 156.4 99.9
2/6/2019 12:57:24 PM 155.7 99.2
2/6/2019 12:57:25 PM 155.0 98.5
2/6/2019 12:57:26 PM 154.4 97.9
2/6/2019 12:57:27 PM 153.7 97.2
2/6/2019 12:57:28 PM 153.0 96.5
2/6/2019 12:57:29 PM 152.2 95.7
2/6/2019 12:57:30 PM 151.6 95.1
2/6/2019 12:57:31 PM 150.9 94.4
2/6/2019 12:57:32 PM 150.4 93.9
2/6/2019 12:57:33 PM 149.8 93.3
2/6/2019 12:57:34 PM 149.2 92.7
2/6/2019 12:57:35 PM 148.3 91.8
2/6/2019 12:57:36 PM 147.6 91.1
2/6/2019 12:57:37 PM 146.7 90.2
2/6/2019 12:57:38 PM 145.8 89.3
2/6/2019 12:57:39 PM 145.0 88.5
2/6/2019 12:57:40 PM 144.1 87.6
2/6/2019 12:57:41 PM 143.4 86.9
2/6/2019 12:57:42 PM 142.5 86.0
2/6/2019 12:57:43 PM 141.8 85.3
2/6/2019 12:57:44 PM 141.0 84.5
2/6/2019 12:57:45 PM 140.3 83.8
2/6/2019 12:57:46 PM 139.5 83.0
2/6/2019 12:57:47 PM 138.8 82.3
2/6/2019 12:57:48 PM 138.1 81.6
2/6/2019 12:57:49 PM 137.5 81.0
2/6/2019 12:57:50 PM 136.9 80.4
2/6/2019 12:57:51 PM 136.4 79.9
2/6/2019 12:57:52 PM 136.0 79.5
2/6/2019 12:57:53 PM 135.6 79.1
2/6/2019 12:57:54 PM 135.1 78.6
2/6/2019 12:57:55 PM 134.5 78.0
2/6/2019 12:57:56 PM 133.8 77.3
2/6/2019 12:57:57 PM 133.3 76.8
2/6/2019 12:57:58 PM 132.7 76.2
2/6/2019 12:57:59 PM 132.3 75.8
Page 310 of 452 August 2019
APPENDIX E50: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-1 Data Log
2/6/2019 12:58:00 PM 131.7 75.2
2/6/2019 12:58:01 PM 130.9 74.4
2/6/2019 12:58:02 PM 130.4 73.9
2/6/2019 12:58:03 PM 129.9 73.4
2/6/2019 12:58:04 PM 129.1 72.6
2/6/2019 12:58:05 PM 128.6 72.1
2/6/2019 12:58:06 PM 128.2 71.7
2/6/2019 12:58:07 PM 127.7 71.2
2/6/2019 12:58:08 PM 127.4 70.9
2/6/2019 12:58:09 PM 127.2 70.7
2/6/2019 12:58:10 PM 126.9 70.4
2/6/2019 12:58:11 PM 126.5 70.0
2/6/2019 12:58:12 PM 126.0 69.5
2/6/2019 12:58:13 PM 125.6 69.1
2/6/2019 12:58:14 PM 125.0 68.5
2/6/2019 12:58:15 PM 124.6 68.1
2/6/2019 12:58:16 PM 124.0 67.5
2/6/2019 12:58:17 PM 123.5 67.0
2/6/2019 12:58:18 PM 123.0 66.5
2/6/2019 12:58:19 PM 122.4 65.9
2/6/2019 12:58:20 PM 121.8 65.3
2/6/2019 12:58:21 PM 121.1 64.6
2/6/2019 12:58:22 PM 120.4 63.9
2/6/2019 12:58:23 PM 119.7 63.2
2/6/2019 12:58:24 PM 119.1 62.6
2/6/2019 12:58:25 PM 118.6 62.1
2/6/2019 12:58:26 PM 118.1 61.6
2/6/2019 12:58:27 PM 117.6 61.1
2/6/2019 12:58:28 PM 117.2 60.7
2/6/2019 12:58:29 PM 116.7 60.2
2/6/2019 12:58:30 PM 116.3 59.8
2/6/2019 12:58:31 PM 115.8 59.3
2/6/2019 12:58:32 PM 115.4 58.9
2/6/2019 12:58:33 PM 115.0 58.5
2/6/2019 12:58:34 PM 114.7 58.2
2/6/2019 12:58:35 PM 114.4 57.9
2/6/2019 12:58:36 PM 114.1 57.6
2/6/2019 12:58:37 PM 113.8 57.3
2/6/2019 12:58:38 PM 113.5 57.0
2/6/2019 12:58:39 PM 113.2 56.7
2/6/2019 12:58:40 PM 113.0 56.5
2/6/2019 12:58:41 PM 112.7 56.2
2/6/2019 12:58:42 PM 112.5 56.0
2/6/2019 12:58:43 PM 112.2 55.7
2/6/2019 12:58:44 PM 112.0 55.5
2/6/2019 12:58:45 PM 111.8 55.3
2/6/2019 12:58:46 PM 111.7 55.2
2/6/2019 12:58:47 PM 111.5 55.0
2/6/2019 12:58:48 PM 111.4 54.9
2/6/2019 12:58:49 PM 111.2 54.7
2/6/2019 12:58:50 PM 111.0 54.5
2/6/2019 12:58:51 PM 110.7 54.2
2/6/2019 12:58:52 PM 110.4 53.9
2/6/2019 12:58:53 PM 110.0 53.5
2/6/2019 12:58:54 PM 109.6 53.1
2/6/2019 12:58:55 PM 109.2 52.7
2/6/2019 12:58:56 PM 108.8 52.3
2/6/2019 12:58:57 PM 108.3 51.8
2/6/2019 12:58:58 PM 107.9 51.4
2/6/2019 12:58:59 PM 107.4 50.9
2/6/2019 12:59:00 PM 107.0 50.5
2/6/2019 12:59:01 PM 106.5 50.0
2/6/2019 12:59:02 PM 106.0 49.5
2/6/2019 12:59:03 PM 105.5 49.0
2/6/2019 12:59:04 PM 105.2 48.7
2/6/2019 12:59:05 PM 104.8 48.3
2/6/2019 12:59:06 PM 104.4 47.9
2/6/2019 12:59:07 PM 104.1 47.6
2/6/2019 12:59:08 PM 103.8 47.3
2/6/2019 12:59:09 PM 103.5 47.0
2/6/2019 12:59:10 PM 103.2 46.7
2/6/2019 12:59:11 PM 103.0 46.5
2/6/2019 12:59:12 PM 102.6 46.1
2/6/2019 12:59:13 PM 102.3 45.8
2/6/2019 12:59:14 PM 102.0 45.5
2/6/2019 12:59:15 PM 101.7 45.2
2/6/2019 12:59:16 PM 101.4 44.9
2/6/2019 12:59:17 PM 101.1 44.6
2/6/2019 12:59:18 PM 100.8 44.3
Page 311 of 452 August 2019
APPENDIX E50: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-1 Data Log
2/6/2019 12:59:19 PM 100.5 44.0
2/6/2019 12:59:20 PM 100.3 43.8
2/6/2019 12:59:21 PM 100.0 43.5
2/6/2019 12:59:22 PM 99.7 43.2
2/6/2019 12:59:23 PM 99.4 42.9
2/6/2019 12:59:24 PM 99.1 42.6
2/6/2019 12:59:25 PM 98.9 42.4
2/6/2019 12:59:26 PM 98.7 42.2
2/6/2019 12:59:27 PM 98.5 42.0
2/6/2019 12:59:28 PM 98.4 41.9
2/6/2019 12:59:29 PM 98.2 41.7
2/6/2019 12:59:30 PM 98.1 41.6
2/6/2019 12:59:31 PM 98.0 41.5
2/6/2019 12:59:32 PM 97.8 41.3
2/6/2019 12:59:33 PM 97.7 41.2
2/6/2019 12:59:34 PM 97.6 41.1
2/6/2019 12:59:35 PM 97.4 40.9
2/6/2019 12:59:36 PM 97.3 40.8
2/6/2019 12:59:37 PM 97.1 40.6
2/6/2019 12:59:38 PM 97.0 40.5
2/6/2019 12:59:39 PM 96.8 40.3
2/6/2019 12:59:40 PM 96.7 40.2
2/6/2019 12:59:41 PM 96.5 40.0
2/6/2019 12:59:42 PM 96.3 39.8
2/6/2019 12:59:43 PM 96.1 39.6
2/6/2019 12:59:44 PM 95.8 39.3
2/6/2019 12:59:45 PM 95.6 39.1
2/6/2019 12:59:46 PM 95.3 38.8
2/6/2019 12:59:47 PM 95.0 38.5
2/6/2019 12:59:48 PM 94.8 38.3
2/6/2019 12:59:49 PM 94.5 38.0
2/6/2019 12:59:50 PM 94.2 37.7
2/6/2019 12:59:51 PM 94.0 37.5
2/6/2019 12:59:52 PM 93.7 37.2
2/6/2019 12:59:53 PM 93.5 37.0
2/6/2019 12:59:54 PM 93.2 36.7
2/6/2019 12:59:55 PM 93.0 36.5
2/6/2019 12:59:56 PM 92.8 36.3
2/6/2019 12:59:57 PM 92.6 36.1
2/6/2019 12:59:58 PM 92.4 35.9
2/6/2019 12:59:59 PM 92.2 35.7
2/6/2019 1:00:00 PM 92.1 35.6
2/6/2019 1:00:01 PM 91.9 35.4
2/6/2019 1:00:02 PM 91.8 35.3
2/6/2019 1:00:03 PM 91.6 35.1
2/6/2019 1:00:04 PM 91.5 35.0
2/6/2019 1:00:05 PM 91.4 34.9
2/6/2019 1:00:06 PM 91.3 34.8
2/6/2019 1:00:07 PM 91.2 34.7
2/6/2019 1:00:08 PM 91.1 34.6
2/6/2019 1:00:09 PM 91.0 34.5
2/6/2019 1:00:10 PM 90.9 34.4
2/6/2019 1:00:11 PM 90.8 34.3
2/6/2019 1:00:12 PM 90.6 34.1
2/6/2019 1:00:13 PM 90.5 34.0
2/6/2019 1:00:14 PM 90.3 33.8
2/6/2019 1:00:15 PM 90.2 33.7
2/6/2019 1:00:16 PM 90.0 33.5
2/6/2019 1:00:17 PM 89.8 33.3
2/6/2019 1:00:18 PM 89.6 33.1
2/6/2019 1:00:19 PM 89.4 32.9
2/6/2019 1:00:20 PM 89.2 32.7
2/6/2019 1:00:21 PM 89.0 32.5
2/6/2019 1:00:22 PM 88.8 32.3
2/6/2019 1:00:23 PM 88.6 32.1
2/6/2019 1:00:24 PM 88.5 32.0
2/6/2019 1:00:25 PM 88.4 31.9
2/6/2019 1:00:26 PM 88.3 31.8
2/6/2019 1:00:27 PM 88.2 31.7
2/6/2019 1:00:28 PM 88.0 31.5
2/6/2019 1:00:29 PM 87.9 31.4
2/6/2019 1:00:30 PM 87.9 31.4
2/6/2019 1:00:31 PM 87.8 31.3
2/6/2019 1:00:32 PM 87.8 31.3
2/6/2019 1:00:33 PM 87.7 31.2
2/6/2019 1:00:34 PM 87.7 31.2
2/6/2019 1:00:35 PM 87.6 31.1
2/6/2019 1:00:36 PM 87.6 31.1
2/6/2019 1:00:37 PM 87.5 31.0
Page 312 of 452 August 2019
APPENDIX E50: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-1 Data Log
2/6/2019 1:00:38 PM 87.5 31.0
2/6/2019 1:00:39 PM 87.4 30.9
2/6/2019 1:00:40 PM 87.4 30.9
2/6/2019 1:00:41 PM 87.3 30.8
2/6/2019 1:00:42 PM 87.2 30.7
2/6/2019 1:00:43 PM 87.1 30.6
2/6/2019 1:00:44 PM 87.0 30.5
2/6/2019 1:00:45 PM 86.9 30.4
2/6/2019 1:00:46 PM 86.8 30.3
2/6/2019 1:00:47 PM 86.7 30.2
2/6/2019 1:00:48 PM 86.5 30.0
2/6/2019 1:00:49 PM 86.4 29.9
2/6/2019 1:00:50 PM 86.2 29.7
2/6/2019 1:00:51 PM 86.1 29.6
2/6/2019 1:00:52 PM 85.9 29.4
2/6/2019 1:00:53 PM 85.8 29.3
2/6/2019 1:00:54 PM 85.6 29.1
2/6/2019 1:00:55 PM 85.5 29.0
2/6/2019 1:00:56 PM 85.4 28.9
2/6/2019 1:00:57 PM 85.2 28.7
2/6/2019 1:00:58 PM 85.1 28.6
2/6/2019 1:00:59 PM 84.9 28.4
2/6/2019 1:01:00 PM 84.8 28.3
2/6/2019 1:01:01 PM 84.6 28.1
2/6/2019 1:01:02 PM 84.5 28.0
2/6/2019 1:01:03 PM 84.4 27.9
2/6/2019 1:01:04 PM 84.3 27.8
2/6/2019 1:01:05 PM 84.2 27.7
2/6/2019 1:01:06 PM 84.1 27.6
2/6/2019 1:01:07 PM 84.0 27.5
2/6/2019 1:01:08 PM 83.9 27.4
2/6/2019 1:01:09 PM 83.8 27.3
2/6/2019 1:01:10 PM 83.7 27.2
2/6/2019 1:01:11 PM 83.6 27.1
2/6/2019 1:01:12 PM 83.5 27.0
2/6/2019 1:01:13 PM 83.4 26.9
2/6/2019 1:01:14 PM 83.3 26.8
2/6/2019 1:01:14 PM 83.2 0.0
2/6/2019 1:01:15 PM 83.1 26.6
2/6/2019 1:01:16 PM 83.0 26.5
2/6/2019 1:01:17 PM 82.9 26.4
2/6/2019 1:01:18 PM 82.7 26.2
2/6/2019 1:01:19 PM 82.6 26.1
2/6/2019 1:01:20 PM 82.5 26.0
2/6/2019 1:01:21 PM 82.4 25.9
2/6/2019 1:01:22 PM 82.3 25.8
2/6/2019 1:01:23 PM 82.2 25.7
2/6/2019 1:01:24 PM 82.1 25.6
2/6/2019 1:01:25 PM 82.0 25.5
2/6/2019 1:01:26 PM 81.9 25.4
2/6/2019 1:01:27 PM 81.8 25.3
2/6/2019 1:01:28 PM 81.7 25.2
2/6/2019 1:01:29 PM 81.6 25.1
2/6/2019 1:01:30 PM 81.5 25.0
2/6/2019 1:01:31 PM 81.4 24.9
2/6/2019 1:01:32 PM 81.4 24.9
2/6/2019 1:01:33 PM 81.3 24.8
2/6/2019 1:01:34 PM 81.2 24.7
2/6/2019 1:01:35 PM 81.1 24.6
2/6/2019 1:01:36 PM 81.0 24.5
2/6/2019 1:01:37 PM 81.0 24.5
2/6/2019 1:01:38 PM 80.9 24.4
2/6/2019 1:01:39 PM 80.8 24.3
2/6/2019 1:01:40 PM 80.7 24.2
2/6/2019 1:01:41 PM 80.6 24.1
2/6/2019 1:01:42 PM 80.5 24.0
2/6/2019 1:01:43 PM 80.4 23.9
2/6/2019 1:01:44 PM 80.3 23.8
2/6/2019 1:01:45 PM 80.2 23.7
2/6/2019 1:01:46 PM 80.1 23.6
2/6/2019 1:01:47 PM 80.0 23.5
2/6/2019 1:01:48 PM 79.9 23.4
2/6/2019 1:01:49 PM 79.8 23.3
2/6/2019 1:01:50 PM 79.8 23.3
2/6/2019 1:01:51 PM 79.7 23.2
2/6/2019 1:01:52 PM 79.6 23.1
2/6/2019 1:01:53 PM 79.6 23.1
2/6/2019 1:01:54 PM 79.5 23.0
2/6/2019 1:01:55 PM 79.4 22.9
Page 313 of 452 August 2019
APPENDIX E50: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-1 Data Log
2/6/2019 1:01:56 PM 79.4 22.9
2/6/2019 1:01:57 PM 79.4 22.9
2/6/2019 1:01:58 PM 79.3 22.8
2/6/2019 1:01:59 PM 79.3 22.8
2/6/2019 1:02:00 PM 79.3 22.8
2/6/2019 1:02:01 PM 79.2 22.7
2/6/2019 1:02:02 PM 79.2 22.7
2/6/2019 1:02:03 PM 79.2 22.7
2/6/2019 1:02:04 PM 79.1 22.6
2/6/2019 1:02:05 PM 79.1 22.6
2/6/2019 1:02:06 PM 79.1 22.6
2/6/2019 1:02:07 PM 79.0 22.5
2/6/2019 1:02:08 PM 78.9 22.4
2/6/2019 1:02:09 PM 78.9 22.4
2/6/2019 1:02:10 PM 78.8 22.3
2/6/2019 1:02:11 PM 78.7 22.2
2/6/2019 1:02:12 PM 78.6 22.1
2/6/2019 1:02:13 PM 78.5 22.0
2/6/2019 1:02:14 PM 78.5 22.0
2/6/2019 1:02:15 PM 78.4 21.9
2/6/2019 1:02:16 PM 78.3 21.8
2/6/2019 1:02:17 PM 78.2 21.7
2/6/2019 1:02:18 PM 78.1 21.6
2/6/2019 1:02:19 PM 78.0 21.5
2/6/2019 1:02:20 PM 78.0 21.5
2/6/2019 1:02:21 PM 77.9 21.4
2/6/2019 1:02:22 PM 77.8 21.3
2/6/2019 1:02:23 PM 77.7 21.2
2/6/2019 1:02:24 PM 77.6 21.1
2/6/2019 1:02:25 PM 77.5 21.0
2/6/2019 1:02:26 PM 77.4 20.9
2/6/2019 1:02:27 PM 77.3 20.8
2/6/2019 1:02:28 PM 77.2 20.7
2/6/2019 1:02:29 PM 77.1 20.6
2/6/2019 1:02:30 PM 77.1 20.6
2/6/2019 1:02:31 PM 77.0 20.5
2/6/2019 1:02:32 PM 76.9 20.4
2/6/2019 1:02:33 PM 76.9 20.4
2/6/2019 1:02:34 PM 76.8 20.3
2/6/2019 1:02:35 PM 76.8 20.3
2/6/2019 1:02:36 PM 76.7 20.2
2/6/2019 1:02:37 PM 76.7 20.2
2/6/2019 1:02:38 PM 76.7 20.2
2/6/2019 1:02:39 PM 76.6 20.1
2/6/2019 1:02:40 PM 76.6 20.1
2/6/2019 1:02:41 PM 76.5 20.0
2/6/2019 1:02:42 PM 76.5 20.0
2/6/2019 1:02:43 PM 76.4 19.9
2/6/2019 1:02:44 PM 76.4 19.9
2/6/2019 1:02:45 PM 76.3 19.8
2/6/2019 1:02:46 PM 76.3 19.8
2/6/2019 1:02:47 PM 76.2 19.7
2/6/2019 1:02:48 PM 76.1 19.6
2/6/2019 1:02:49 PM 76.1 19.6
2/6/2019 1:02:50 PM 76.0 19.5
2/6/2019 1:02:51 PM 75.9 19.4
2/6/2019 1:02:52 PM 75.9 19.4
2/6/2019 1:02:53 PM 75.8 19.3
2/6/2019 1:02:54 PM 75.7 19.2
2/6/2019 1:02:55 PM 75.7 19.2
2/6/2019 1:02:56 PM 75.6 19.1
2/6/2019 1:02:57 PM 75.6 19.1
2/6/2019 1:02:58 PM 75.5 19.0
2/6/2019 1:02:59 PM 75.5 19.0
2/6/2019 1:03:00 PM 75.5 19.0
2/6/2019 1:03:01 PM 75.4 18.9
2/6/2019 1:03:02 PM 75.4 18.9
2/6/2019 1:03:03 PM 75.4 18.9
2/6/2019 1:03:04 PM 75.3 18.8
2/6/2019 1:03:05 PM 75.3 18.8
2/6/2019 1:03:06 PM 75.2 18.7
2/6/2019 1:03:07 PM 75.1 18.6
2/6/2019 1:03:08 PM 75.1 18.6
2/6/2019 1:03:09 PM 75.0 18.5
2/6/2019 1:03:10 PM 75.0 18.5
2/6/2019 1:03:11 PM 74.9 18.4
2/6/2019 1:03:12 PM 74.8 18.3
2/6/2019 1:03:13 PM 74.8 18.3
2/6/2019 1:03:14 PM 74.7 18.2
Page 314 of 452 August 2019
APPENDIX E50: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-1 Data Log
2/6/2019 1:03:15 PM 74.6 18.1
2/6/2019 1:03:16 PM 74.5 18.0
2/6/2019 1:03:17 PM 74.5 18.0
2/6/2019 1:03:18 PM 74.4 17.9
2/6/2019 1:03:19 PM 74.4 17.9
2/6/2019 1:03:20 PM 74.3 17.8
2/6/2019 1:03:21 PM 74.3 17.8
2/6/2019 1:03:22 PM 74.2 17.7
2/6/2019 1:03:23 PM 74.2 17.7
2/6/2019 1:03:24 PM 74.1 17.6
2/6/2019 1:03:25 PM 74.1 17.6
2/6/2019 1:03:26 PM 74.0 17.5
2/6/2019 1:03:27 PM 74.0 17.5
2/6/2019 1:03:28 PM 74.0 17.5
2/6/2019 1:03:29 PM 73.9 17.4
2/6/2019 1:03:30 PM 73.9 17.4
2/6/2019 1:03:31 PM 73.9 17.4
2/6/2019 1:03:32 PM 73.8 17.3
2/6/2019 1:03:33 PM 73.8 17.3
2/6/2019 1:03:34 PM 73.7 17.2
2/6/2019 1:03:35 PM 73.7 17.2
2/6/2019 1:03:36 PM 73.7 17.2
2/6/2019 1:03:37 PM 73.6 17.1
2/6/2019 1:03:38 PM 73.6 17.1
2/6/2019 1:03:39 PM 73.5 17.0
2/6/2019 1:03:40 PM 73.5 17.0
2/6/2019 1:03:41 PM 73.4 16.9
2/6/2019 1:03:42 PM 73.4 16.9
2/6/2019 1:03:43 PM 73.4 16.9
2/6/2019 1:03:44 PM 73.3 16.8
2/6/2019 1:03:45 PM 73.3 16.8
2/6/2019 1:03:46 PM 73.2 16.7
2/6/2019 1:03:47 PM 73.2 16.7
2/6/2019 1:03:48 PM 73.2 16.7
2/6/2019 1:03:49 PM 73.1 16.6
2/6/2019 1:03:50 PM 73.1 16.6
2/6/2019 1:03:51 PM 73.0 16.5
2/6/2019 1:03:52 PM 73.0 16.5
2/6/2019 1:03:53 PM 72.9 16.4
2/6/2019 1:03:54 PM 72.8 16.3
2/6/2019 1:03:55 PM 72.7 16.2
2/6/2019 1:03:56 PM 72.7 16.2
2/6/2019 1:03:57 PM 72.6 16.1
2/6/2019 1:03:58 PM 72.5 16.0
2/6/2019 1:03:59 PM 72.5 16.0
2/6/2019 1:04:00 PM 72.4 15.9
2/6/2019 1:04:01 PM 72.3 15.8
2/6/2019 1:04:02 PM 72.3 15.8
2/6/2019 1:04:03 PM 72.2 15.7
2/6/2019 1:04:04 PM 72.2 15.7
2/6/2019 1:04:05 PM 72.1 15.6
2/6/2019 1:04:06 PM 72.1 15.6
2/6/2019 1:04:07 PM 72.1 15.6
2/6/2019 1:04:08 PM 72.1 15.6
2/6/2019 1:04:09 PM 72.0 15.5
2/6/2019 1:04:10 PM 72.0 15.5
2/6/2019 1:04:11 PM 72.0 15.5
2/6/2019 1:04:12 PM 72.0 15.5
2/6/2019 1:04:13 PM 71.9 15.4
2/6/2019 1:04:14 PM 71.9 15.4
2/6/2019 1:04:15 PM 71.8 15.3
2/6/2019 1:04:16 PM 71.8 15.3
2/6/2019 1:04:17 PM 71.8 15.3
2/6/2019 1:04:18 PM 71.7 15.2
2/6/2019 1:04:19 PM 71.7 15.2
2/6/2019 1:04:20 PM 71.6 15.1
2/6/2019 1:04:21 PM 71.5 15.0
2/6/2019 1:04:22 PM 71.5 15.0
2/6/2019 1:04:23 PM 71.5 15.0
2/6/2019 1:04:24 PM 71.4 14.9
2/6/2019 1:04:25 PM 71.4 14.9
2/6/2019 1:04:26 PM 71.4 14.9
2/6/2019 1:04:27 PM 71.4 14.9
2/6/2019 1:04:28 PM 71.3 14.8
2/6/2019 1:04:29 PM 71.3 14.8
2/6/2019 1:04:30 PM 71.3 14.8
2/6/2019 1:04:31 PM 71.2 14.7
2/6/2019 1:04:32 PM 71.2 14.7
2/6/2019 1:04:33 PM 71.2 14.7
Page 315 of 452 August 2019
APPENDIX E50: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-1 Data Log
2/6/2019 1:04:34 PM 71.1 14.6
2/6/2019 1:04:35 PM 71.1 14.6
2/6/2019 1:04:36 PM 71.0 14.5
2/6/2019 1:04:37 PM 71.0 14.5
2/6/2019 1:04:38 PM 70.9 14.4
2/6/2019 1:04:39 PM 70.9 14.4
2/6/2019 1:04:40 PM 70.8 14.3
2/6/2019 1:04:41 PM 70.8 14.3
2/6/2019 1:04:42 PM 70.7 14.2
2/6/2019 1:04:43 PM 70.7 14.2
2/6/2019 1:04:44 PM 70.6 14.1
2/6/2019 1:04:45 PM 70.6 14.1
2/6/2019 1:04:46 PM 70.5 14.0
2/6/2019 1:04:47 PM 70.5 14.0
2/6/2019 1:04:48 PM 70.4 13.9
2/6/2019 1:04:49 PM 70.4 13.9
2/6/2019 1:04:50 PM 70.3 13.8
2/6/2019 1:04:51 PM 70.3 13.8
2/6/2019 1:04:52 PM 70.2 13.7
2/6/2019 1:04:53 PM 70.2 13.7
2/6/2019 1:04:54 PM 70.2 13.7
2/6/2019 1:04:55 PM 70.2 13.7
2/6/2019 1:04:56 PM 70.2 13.7
2/6/2019 1:04:57 PM 70.1 13.6
2/6/2019 1:04:58 PM 70.1 13.6
2/6/2019 1:04:59 PM 70.1 13.6
2/6/2019 1:05:00 PM 70.1 13.6
2/6/2019 1:05:01 PM 70.1 13.6
2/6/2019 1:05:02 PM 70.1 13.6
2/6/2019 1:05:03 PM 70.1 13.6
2/6/2019 1:05:04 PM 70.1 13.6
2/6/2019 1:05:05 PM 70.0 13.5
2/6/2019 1:05:06 PM 70.0 13.5
2/6/2019 1:05:07 PM 70.0 13.5
2/6/2019 1:05:08 PM 70.0 13.5
2/6/2019 1:05:09 PM 69.9 13.4
2/6/2019 1:05:10 PM 69.9 13.4
2/6/2019 1:05:11 PM 69.9 13.4
2/6/2019 1:05:12 PM 69.9 13.4
2/6/2019 1:05:13 PM 69.9 13.4
2/6/2019 1:05:14 PM 69.8 13.3
2/6/2019 1:05:15 PM 69.8 13.3
2/6/2019 1:05:16 PM 69.7 13.2
2/6/2019 1:05:17 PM 69.7 13.2
2/6/2019 1:05:18 PM 69.6 13.1
2/6/2019 1:05:19 PM 69.6 13.1
2/6/2019 1:05:20 PM 69.6 13.1
2/6/2019 1:05:21 PM 69.5 13.0
2/6/2019 1:05:22 PM 69.5 13.0
2/6/2019 1:05:23 PM 69.4 12.9
2/6/2019 1:05:24 PM 69.4 12.9
2/6/2019 1:05:25 PM 69.3 12.8
2/6/2019 1:05:26 PM 69.3 12.8
2/6/2019 1:05:27 PM 69.3 12.8
2/6/2019 1:05:28 PM 69.2 12.7
2/6/2019 1:05:29 PM 69.2 12.7
2/6/2019 1:05:30 PM 69.2 12.7
2/6/2019 1:05:31 PM 69.1 12.6
2/6/2019 1:05:32 PM 69.1 12.6
2/6/2019 1:05:33 PM 69.1 12.6
2/6/2019 1:05:34 PM 69.0 12.5
2/6/2019 1:05:35 PM 69.0 12.5
2/6/2019 1:05:36 PM 69.0 12.5
2/6/2019 1:05:37 PM 68.9 12.4
2/6/2019 1:05:38 PM 68.9 12.4
2/6/2019 1:05:39 PM 68.9 12.4
2/6/2019 1:05:40 PM 68.9 12.4
2/6/2019 1:05:41 PM 68.8 12.3
2/6/2019 1:05:42 PM 68.8 12.3
2/6/2019 1:05:43 PM 68.8 12.3
2/6/2019 1:05:44 PM 68.7 12.2
2/6/2019 1:05:45 PM 68.7 12.2
2/6/2019 1:05:46 PM 68.7 12.2
2/6/2019 1:05:47 PM 68.6 12.1
2/6/2019 1:05:48 PM 68.6 12.1
2/6/2019 1:05:49 PM 68.6 12.1
2/6/2019 1:05:50 PM 68.6 12.1
2/6/2019 1:05:51 PM 68.5 12.0
2/6/2019 1:05:52 PM 68.5 12.0
Page 316 of 452 August 2019
APPENDIX E50: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-1 Data Log
2/6/2019 1:05:53 PM 68.5 12.0
2/6/2019 1:05:54 PM 68.5 12.0
2/6/2019 1:05:55 PM 68.5 12.0
2/6/2019 1:05:56 PM 68.4 11.9
2/6/2019 1:05:57 PM 68.4 11.9
2/6/2019 1:05:58 PM 68.4 11.9
2/6/2019 1:05:59 PM 68.4 11.9
2/6/2019 1:06:00 PM 68.3 11.8
2/6/2019 1:06:01 PM 68.3 11.8
2/6/2019 1:06:02 PM 68.3 11.8
2/6/2019 1:06:03 PM 68.3 11.8
2/6/2019 1:06:04 PM 68.2 11.7
2/6/2019 1:06:05 PM 68.2 11.7
2/6/2019 1:06:06 PM 68.2 11.7
2/6/2019 1:06:07 PM 68.1 11.6
2/6/2019 1:06:08 PM 68.1 11.6
2/6/2019 1:06:09 PM 68.1 11.6
2/6/2019 1:06:10 PM 68.1 11.6
2/6/2019 1:06:11 PM 68.1 11.6
2/6/2019 1:06:12 PM 68.0 11.5
2/6/2019 1:06:13 PM 68.0 11.5
2/6/2019 1:06:14 PM 68.0 11.5
2/6/2019 1:06:15 PM 68.0 11.5
2/6/2019 1:06:16 PM 68.0 11.5
2/6/2019 1:06:17 PM 68.0 11.5
2/6/2019 1:06:18 PM 68.0 11.5
2/6/2019 1:06:19 PM 68.0 11.5
2/6/2019 1:06:20 PM 67.9 11.4
2/6/2019 1:06:21 PM 67.9 11.4
2/6/2019 1:06:22 PM 67.9 11.4
2/6/2019 1:06:23 PM 67.8 11.3
2/6/2019 1:06:24 PM 67.8 11.3
2/6/2019 1:06:25 PM 67.8 11.3
2/6/2019 1:06:26 PM 67.7 11.2
2/6/2019 1:06:27 PM 67.7 11.2
2/6/2019 1:06:28 PM 67.7 11.2
2/6/2019 1:06:29 PM 67.6 11.1
2/6/2019 1:06:30 PM 67.6 11.1
2/6/2019 1:06:31 PM 67.6 11.1
2/6/2019 1:06:32 PM 67.6 11.1
2/6/2019 1:06:33 PM 67.5 11.0
2/6/2019 1:06:34 PM 67.5 11.0
2/6/2019 1:06:35 PM 67.5 11.0
2/6/2019 1:06:36 PM 67.4 10.9
2/6/2019 1:06:37 PM 67.4 10.9
2/6/2019 1:06:38 PM 67.4 10.9
2/6/2019 1:06:39 PM 67.4 10.9
2/6/2019 1:06:40 PM 67.3 10.8
2/6/2019 1:06:41 PM 67.3 10.8
2/6/2019 1:06:42 PM 67.3 10.8
2/6/2019 1:06:43 PM 67.3 10.8
2/6/2019 1:06:44 PM 67.3 10.8
2/6/2019 1:06:45 PM 67.2 10.7
2/6/2019 1:06:46 PM 67.2 10.7
2/6/2019 1:06:47 PM 67.2 10.7
2/6/2019 1:06:48 PM 67.2 10.7
2/6/2019 1:06:49 PM 67.2 10.7
2/6/2019 1:06:50 PM 67.2 10.7
2/6/2019 1:06:51 PM 67.2 10.7
2/6/2019 1:06:52 PM 67.1 10.6
2/6/2019 1:06:53 PM 67.1 10.6
2/6/2019 1:06:54 PM 67.1 10.6
2/6/2019 1:06:55 PM 67.1 10.6
2/6/2019 1:06:56 PM 67.1 10.6
2/6/2019 1:06:57 PM 67.1 10.6
2/6/2019 1:06:58 PM 67.1 10.6
2/6/2019 1:06:59 PM 67.1 10.6
2/6/2019 1:07:00 PM 67.0 10.5
2/6/2019 1:07:01 PM 67.0 10.5
2/6/2019 1:07:02 PM 67.0 10.5
2/6/2019 1:07:03 PM 67.0 10.5
2/6/2019 1:07:04 PM 67.0 10.5
2/6/2019 1:07:05 PM 66.9 10.4
2/6/2019 1:07:06 PM 66.9 10.4
2/6/2019 1:07:07 PM 66.9 10.4
2/6/2019 1:07:08 PM 66.9 10.4
2/6/2019 1:07:09 PM 66.9 10.4
2/6/2019 1:07:10 PM 66.9 10.4
2/6/2019 1:07:11 PM 66.8 10.3
Page 317 of 452 August 2019
APPENDIX E50: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-1 Data Log
2/6/2019 1:07:12 PM 66.8 10.3
2/6/2019 1:07:13 PM 66.8 10.3
2/6/2019 1:07:14 PM 66.8 10.3
2/6/2019 1:07:15 PM 66.7 10.2
2/6/2019 1:07:16 PM 66.7 10.2
2/6/2019 1:07:17 PM 66.7 10.2
2/6/2019 1:07:18 PM 66.7 10.2
2/6/2019 1:07:19 PM 66.6 10.1
2/6/2019 1:07:20 PM 66.6 10.1
2/6/2019 1:07:21 PM 66.6 10.1
2/6/2019 1:07:22 PM 66.6 10.1
2/6/2019 1:07:23 PM 66.5 10.0
2/6/2019 1:07:24 PM 66.5 10.0
2/6/2019 1:07:25 PM 66.5 10.0
2/6/2019 1:07:26 PM 66.5 10.0
2/6/2019 1:07:27 PM 66.4 9.9
2/6/2019 1:07:28 PM 66.4 9.9
2/6/2019 1:07:29 PM 66.4 9.9
2/6/2019 1:07:30 PM 66.4 9.9
2/6/2019 1:07:31 PM 66.3 9.8
2/6/2019 1:07:32 PM 66.3 9.8
2/6/2019 1:07:33 PM 66.3 9.8
2/6/2019 1:07:34 PM 66.3 9.8
2/6/2019 1:07:35 PM 66.2 9.7
2/6/2019 1:07:36 PM 66.2 9.7
2/6/2019 1:07:37 PM 66.2 9.7
2/6/2019 1:07:38 PM 66.2 9.7
2/6/2019 1:07:39 PM 66.1 9.6
2/6/2019 1:07:40 PM 66.1 9.6
2/6/2019 1:07:41 PM 66.1 9.6
2/6/2019 1:07:42 PM 66.1 9.6
2/6/2019 1:07:43 PM 66.1 9.6
2/6/2019 1:07:44 PM 66.1 9.6
2/6/2019 1:07:45 PM 66.0 9.5
2/6/2019 1:07:46 PM 66.0 9.5
2/6/2019 1:07:47 PM 66.0 9.5
2/6/2019 1:07:48 PM 66.0 9.5
2/6/2019 1:07:49 PM 66.0 9.5
2/6/2019 1:07:50 PM 66.0 9.5
2/6/2019 1:07:51 PM 66.0 9.5
2/6/2019 1:07:52 PM 65.9 9.4
2/6/2019 1:07:53 PM 65.9 9.4
2/6/2019 1:07:54 PM 65.9 9.4
2/6/2019 1:07:55 PM 65.9 9.4
2/6/2019 1:07:56 PM 65.9 9.4
2/6/2019 1:07:57 PM 65.9 9.4
2/6/2019 1:07:58 PM 65.9 9.4
2/6/2019 1:07:59 PM 65.9 9.4
2/6/2019 1:08:00 PM 65.9 9.4
2/6/2019 1:08:01 PM 65.8 9.3
2/6/2019 1:08:02 PM 65.8 9.3
2/6/2019 1:08:03 PM 65.8 9.3
2/6/2019 1:08:04 PM 65.8 9.3
2/6/2019 1:08:05 PM 65.8 9.3
2/6/2019 1:08:06 PM 65.8 9.3
2/6/2019 1:08:07 PM 65.7 9.2
2/6/2019 1:08:08 PM 65.7 9.2
2/6/2019 1:08:09 PM 65.7 9.2
2/6/2019 1:08:10 PM 65.7 9.2
2/6/2019 1:08:11 PM 65.7 9.2
2/6/2019 1:08:12 PM 65.7 9.2
2/6/2019 1:08:13 PM 65.6 9.1
2/6/2019 1:08:14 PM 65.6 9.1
2/6/2019 1:08:15 PM 65.6 9.1
2/6/2019 1:08:16 PM 65.6 9.1
2/6/2019 1:08:17 PM 65.6 9.1
2/6/2019 1:08:18 PM 65.6 9.1
2/6/2019 1:08:19 PM 65.5 9.0
2/6/2019 1:08:20 PM 65.5 9.0
2/6/2019 1:08:21 PM 65.5 9.0
2/6/2019 1:08:22 PM 65.5 9.0
2/6/2019 1:08:23 PM 65.5 9.0
2/6/2019 1:08:24 PM 65.5 9.0
2/6/2019 1:08:25 PM 65.5 9.0
2/6/2019 1:08:26 PM 65.4 8.9
2/6/2019 1:08:27 PM 65.4 8.9
2/6/2019 1:08:28 PM 65.4 8.9
2/6/2019 1:08:29 PM 65.4 8.9
2/6/2019 1:08:30 PM 65.4 8.9
Page 318 of 452 August 2019
APPENDIX E50: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-1 Data Log
2/6/2019 1:08:31 PM 65.4 8.9
2/6/2019 1:08:32 PM 65.4 8.9
2/6/2019 1:08:33 PM 65.3 8.8
2/6/2019 1:08:34 PM 65.3 8.8
2/6/2019 1:08:35 PM 65.3 8.8
2/6/2019 1:08:36 PM 65.3 8.8
2/6/2019 1:08:37 PM 65.3 8.8
2/6/2019 1:08:38 PM 65.2 8.7
2/6/2019 1:08:39 PM 65.2 8.7
2/6/2019 1:08:40 PM 65.2 8.7
2/6/2019 1:08:41 PM 65.2 8.7
2/6/2019 1:08:42 PM 65.2 8.7
2/6/2019 1:08:43 PM 65.2 8.7
2/6/2019 1:08:44 PM 65.1 8.6
2/6/2019 1:08:45 PM 65.1 8.6
2/6/2019 1:08:46 PM 65.1 8.6
2/6/2019 1:08:47 PM 65.1 8.6
2/6/2019 1:08:48 PM 65.1 8.6
2/6/2019 1:08:49 PM 65.1 8.6
2/6/2019 1:08:50 PM 65.1 8.6
2/6/2019 1:08:51 PM 65.0 8.5
2/6/2019 1:08:52 PM 65.0 8.5
2/6/2019 1:08:53 PM 65.0 8.5
2/6/2019 1:08:54 PM 65.0 8.5
2/6/2019 1:08:55 PM 65.0 8.5
2/6/2019 1:08:56 PM 65.0 8.5
2/6/2019 1:08:57 PM 64.9 8.4
2/6/2019 1:08:58 PM 64.9 8.4
2/6/2019 1:08:59 PM 64.9 8.4
2/6/2019 1:09:00 PM 64.9 8.4
2/6/2019 1:09:01 PM 64.9 8.4
2/6/2019 1:09:02 PM 64.8 8.3
2/6/2019 1:09:03 PM 64.8 8.3
2/6/2019 1:09:04 PM 64.8 8.3
2/6/2019 1:09:05 PM 64.8 8.3
2/6/2019 1:09:06 PM 64.8 8.3
2/6/2019 1:09:07 PM 64.7 8.2
2/6/2019 1:09:08 PM 64.7 8.2
2/6/2019 1:09:09 PM 64.7 8.2
2/6/2019 1:09:10 PM 64.7 8.2
2/6/2019 1:09:11 PM 64.7 8.2
2/6/2019 1:09:12 PM 64.6 8.1
2/6/2019 1:09:13 PM 64.6 8.1
2/6/2019 1:09:14 PM 64.6 8.1
2/6/2019 1:09:15 PM 64.6 8.1
2/6/2019 1:09:16 PM 64.5 8.0
2/6/2019 1:09:17 PM 64.5 8.0
2/6/2019 1:09:18 PM 64.5 8.0
2/6/2019 1:09:19 PM 64.5 8.0
2/6/2019 1:09:20 PM 64.5 8.0
2/6/2019 1:09:21 PM 64.4 7.9
2/6/2019 1:09:22 PM 64.4 7.9
2/6/2019 1:09:23 PM 64.4 7.9
2/6/2019 1:09:24 PM 64.4 7.9
2/6/2019 1:09:25 PM 64.4 7.9
2/6/2019 1:09:26 PM 64.4 7.9
2/6/2019 1:09:27 PM 64.4 7.9
2/6/2019 1:09:28 PM 64.3 7.8
2/6/2019 1:09:29 PM 64.3 7.8
2/6/2019 1:09:30 PM 64.3 7.8
2/6/2019 1:09:31 PM 64.3 7.8
2/6/2019 1:09:32 PM 64.3 7.8
2/6/2019 1:09:33 PM 64.3 7.8
2/6/2019 1:09:34 PM 64.3 7.8
2/6/2019 1:09:35 PM 64.3 7.8
2/6/2019 1:09:36 PM 64.2 7.7
2/6/2019 1:09:37 PM 64.2 7.7
2/6/2019 1:09:38 PM 64.2 7.7
2/6/2019 1:09:39 PM 64.2 7.7
2/6/2019 1:09:40 PM 64.2 7.7
2/6/2019 1:09:41 PM 64.2 7.7
2/6/2019 1:09:42 PM 64.1 7.6
2/6/2019 1:09:43 PM 64.1 7.6
2/6/2019 1:09:44 PM 64.1 7.6
2/6/2019 1:09:45 PM 64.1 7.6
2/6/2019 1:09:46 PM 64.1 7.6
2/6/2019 1:09:47 PM 64.1 7.6
2/6/2019 1:09:48 PM 64.0 7.5
2/6/2019 1:09:49 PM 64.0 7.5
Page 319 of 452 August 2019
APPENDIX E50: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-1 Data Log
2/6/2019 1:09:50 PM 64.0 7.5
2/6/2019 1:09:51 PM 64.0 7.5
2/6/2019 1:09:52 PM 64.0 7.5
2/6/2019 1:09:53 PM 64.0 7.5
2/6/2019 1:09:54 PM 64.0 7.5
2/6/2019 1:09:55 PM 63.9 7.4
2/6/2019 1:09:56 PM 63.9 7.4
2/6/2019 1:09:57 PM 63.9 7.4
2/6/2019 1:09:58 PM 63.9 7.4
2/6/2019 1:09:59 PM 63.9 7.4
2/6/2019 1:10:00 PM 63.9 7.4
2/6/2019 1:10:01 PM 63.9 7.4
2/6/2019 1:10:02 PM 63.8 7.3
2/6/2019 1:10:03 PM 63.8 7.3
2/6/2019 1:10:04 PM 63.8 7.3
2/6/2019 1:10:05 PM 63.8 7.3
2/6/2019 1:10:06 PM 63.8 7.3
2/6/2019 1:10:07 PM 63.8 7.3
2/6/2019 1:10:08 PM 63.8 7.3
2/6/2019 1:10:09 PM 63.8 7.3
2/6/2019 1:10:10 PM 63.8 7.3
2/6/2019 1:10:11 PM 63.7 7.2
2/6/2019 1:10:12 PM 63.7 7.2
2/6/2019 1:10:13 PM 63.7 7.2
2/6/2019 1:10:14 PM 63.7 7.2
2/6/2019 1:10:15 PM 63.7 7.2
2/6/2019 1:10:16 PM 63.7 7.2
2/6/2019 1:10:17 PM 63.7 7.2
2/6/2019 1:10:18 PM 63.7 7.2
2/6/2019 1:10:19 PM 63.7 7.2
2/6/2019 1:10:20 PM 63.6 7.1
2/6/2019 1:10:21 PM 63.6 7.1
2/6/2019 1:10:22 PM 63.6 7.1
2/6/2019 1:10:23 PM 63.6 7.1
2/6/2019 1:10:24 PM 63.6 7.1
2/6/2019 1:10:25 PM 63.6 7.1
2/6/2019 1:10:26 PM 63.5 7.0
2/6/2019 1:10:27 PM 63.5 7.0
2/6/2019 1:10:28 PM 63.5 7.0
2/6/2019 1:10:29 PM 63.5 7.0
2/6/2019 1:10:30 PM 63.5 7.0
2/6/2019 1:10:31 PM 63.5 7.0
2/6/2019 1:10:32 PM 63.5 7.0
2/6/2019 1:10:33 PM 63.5 7.0
2/6/2019 1:10:34 PM 63.5 7.0
2/6/2019 1:10:35 PM 63.5 7.0
2/6/2019 1:10:36 PM 63.5 7.0
2/6/2019 1:10:37 PM 63.4 6.9
2/6/2019 1:10:38 PM 63.4 6.9
2/6/2019 1:10:39 PM 63.4 6.9
2/6/2019 1:10:40 PM 63.4 6.9
2/6/2019 1:10:41 PM 63.4 6.9
2/6/2019 1:10:42 PM 63.4 6.9
2/6/2019 1:10:43 PM 63.4 6.9
2/6/2019 1:10:44 PM 63.3 6.8
2/6/2019 1:10:45 PM 63.3 6.8
2/6/2019 1:10:46 PM 63.3 6.8
2/6/2019 1:10:47 PM 63.3 6.8
2/6/2019 1:10:48 PM 63.3 6.8
2/6/2019 1:10:49 PM 63.3 6.8
2/6/2019 1:10:50 PM 63.3 6.8
2/6/2019 1:10:51 PM 63.3 6.8
2/6/2019 1:10:52 PM 63.2 6.7
2/6/2019 1:10:53 PM 63.2 6.7
2/6/2019 1:10:54 PM 63.2 6.7
2/6/2019 1:10:55 PM 63.2 6.7
2/6/2019 1:10:56 PM 63.2 6.7
2/6/2019 1:10:57 PM 63.2 6.7
2/6/2019 1:10:58 PM 63.2 6.7
2/6/2019 1:10:59 PM 63.2 6.7
2/6/2019 1:11:00 PM 63.2 6.7
2/6/2019 1:11:01 PM 63.2 6.7
2/6/2019 1:11:02 PM 63.2 6.7
2/6/2019 1:11:03 PM 63.2 6.7
2/6/2019 1:11:04 PM 63.2 6.7
2/6/2019 1:11:05 PM 63.1 6.6
2/6/2019 1:11:06 PM 63.1 6.6
2/6/2019 1:11:07 PM 63.1 6.6
2/6/2019 1:11:08 PM 63.1 6.6
Page 320 of 452 August 2019
APPENDIX E50: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-1 Data Log
2/6/2019 1:11:09 PM 63.1 6.6
2/6/2019 1:11:10 PM 63.1 6.6
2/6/2019 1:11:11 PM 63.1 6.6
2/6/2019 1:11:12 PM 63.1 6.6
2/6/2019 1:11:13 PM 63.1 6.6
2/6/2019 1:11:14 PM 63.1 6.6
2/6/2019 1:11:15 PM 63.1 6.6
2/6/2019 1:11:16 PM 63.0 6.5
2/6/2019 1:11:17 PM 63.0 6.5
2/6/2019 1:11:18 PM 63.0 6.5
2/6/2019 1:11:19 PM 63.0 6.5
2/6/2019 1:11:20 PM 63.0 6.5
2/6/2019 1:11:21 PM 63.0 6.5
2/6/2019 1:11:22 PM 63.0 6.5
2/6/2019 1:11:23 PM 63.0 6.5
2/6/2019 1:11:24 PM 63.0 6.5
2/6/2019 1:11:25 PM 63.0 6.5
2/6/2019 1:11:26 PM 62.9 6.4
2/6/2019 1:11:27 PM 62.9 6.4
2/6/2019 1:11:28 PM 62.9 6.4
2/6/2019 1:11:29 PM 62.9 6.4
2/6/2019 1:11:30 PM 62.9 6.4
2/6/2019 1:11:31 PM 62.9 6.4
2/6/2019 1:11:32 PM 62.9 6.4
2/6/2019 1:11:33 PM 62.9 6.4
2/6/2019 1:11:34 PM 62.9 6.4
2/6/2019 1:11:35 PM 62.9 6.4
2/6/2019 1:11:36 PM 62.9 6.4
2/6/2019 1:11:37 PM 62.9 6.4
2/6/2019 1:11:38 PM 62.8 6.3
2/6/2019 1:11:39 PM 62.8 6.3
2/6/2019 1:11:40 PM 62.8 6.3
2/6/2019 1:11:41 PM 62.8 6.3
2/6/2019 1:11:42 PM 62.8 6.3
2/6/2019 1:11:43 PM 62.8 6.3
2/6/2019 1:11:44 PM 62.8 6.3
2/6/2019 1:11:45 PM 62.8 6.3
2/6/2019 1:11:46 PM 62.8 6.3
2/6/2019 1:11:47 PM 62.8 6.3
2/6/2019 1:11:48 PM 62.8 6.3
2/6/2019 1:11:49 PM 62.8 6.3
2/6/2019 1:11:50 PM 62.8 6.3
2/6/2019 1:11:51 PM 62.8 6.3
2/6/2019 1:11:52 PM 62.8 6.3
2/6/2019 1:11:53 PM 62.8 6.3
2/6/2019 1:11:54 PM 62.8 6.3
2/6/2019 1:11:55 PM 62.8 6.3
2/6/2019 1:11:56 PM 62.8 6.3
2/6/2019 1:11:57 PM 62.8 6.3
2/6/2019 1:11:58 PM 62.7 6.2
2/6/2019 1:11:59 PM 62.7 6.2
2/6/2019 1:12:00 PM 62.7 6.2
2/6/2019 1:12:01 PM 62.7 6.2
2/6/2019 1:12:02 PM 62.7 6.2
2/6/2019 1:12:03 PM 62.7 6.2
2/6/2019 1:12:04 PM 62.7 6.2
2/6/2019 1:12:05 PM 62.7 6.2
2/6/2019 1:12:06 PM 62.7 6.2
2/6/2019 1:12:07 PM 62.7 6.2
2/6/2019 1:12:08 PM 62.6 6.1
2/6/2019 1:12:09 PM 62.6 6.1
2/6/2019 1:12:10 PM 62.6 6.1
2/6/2019 1:12:11 PM 62.6 6.1
2/6/2019 1:12:12 PM 62.6 6.1
2/6/2019 1:12:13 PM 62.6 6.1
2/6/2019 1:12:14 PM 62.5 6.0
2/6/2019 1:12:15 PM 62.5 6.0
2/6/2019 1:12:16 PM 62.5 6.0
2/6/2019 1:12:17 PM 62.5 6.0
2/6/2019 1:12:18 PM 62.5 6.0
2/6/2019 1:12:19 PM 62.5 6.0
Page 321 of 452 August 2019
APPENDIX E50: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-1 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-B3 TEST-1 1210
SEEP-B3 TEST-1 1211
SEEP-B3 TEST-1 1213
SEEP-B3 TEST-1 1215
Location EC Reading
(µS/cms)
SEEP-B3 TEST-1 40.2
SEEP-B3 TEST-1 193
SEEP-B3 TEST-1 1,593
SEEP-B3 TEST-1 13,094
SEEP-B3 TEST-1 103,212
q 300,000
K 1.0349
1.1
17.7
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)(°C)
Table E2 SEEP-B3 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
53.7 12.5
53.5 12.6
53.6 12.6
53.3 12.9
Average 53.5 (µS/cms)
100 21.3
Average (pre-test)59.1 (µS/cms)
Table E3 SEEP-B3 TEST-1 YSI Salt Dilution Calibration Data
Calibration Temperature
Slope of Calibration Curve (µS/cms) / (mg/L)
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)278,172.1 (s) . (µS/cms)
(µS/cms)53.5Geometric Mean
Table E4 SEEP-B3 TEST-1 Flow Calculation Summary
Mass of Salt injected mg
1,000 21.6
10,000 21.9
100,000 21.9
(mg/L)(°C)
10 20.9
Calculated Flow Rate Q
L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 322 of 452 August 2019
APPENDIX E51: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/6/2019 1:26:12 PM 60.2 -
2/6/2019 1:26:13 PM 60.1 -
2/6/2019 1:26:14 PM 60.1 -
2/6/2019 1:26:15 PM 60.1 -
2/6/2019 1:26:16 PM 60.0 -
2/6/2019 1:26:17 PM 60.0 -
2/6/2019 1:26:18 PM 60.0 -
2/6/2019 1:26:19 PM 60.0 -
2/6/2019 1:26:20 PM 59.9 -
2/6/2019 1:26:21 PM 59.9 -
2/6/2019 1:26:22 PM 59.9 -
2/6/2019 1:26:23 PM 59.9 -
2/6/2019 1:26:24 PM 59.8 -
2/6/2019 1:26:25 PM 59.7 -
2/6/2019 1:26:26 PM 59.7 -
2/6/2019 1:26:27 PM 59.6 -
2/6/2019 1:26:28 PM 59.6 -
2/6/2019 1:26:29 PM 59.5 -
2/6/2019 1:26:30 PM 59.5 -
2/6/2019 1:26:31 PM 59.4 -
2/6/2019 1:26:32 PM 59.4 -
2/6/2019 1:26:33 PM 59.3 -
2/6/2019 1:26:34 PM 59.3 -
2/6/2019 1:26:35 PM 59.2 -
2/6/2019 1:26:36 PM 59.1 -
2/6/2019 1:26:37 PM 59.1 -
2/6/2019 1:26:38 PM 59.1 -
2/6/2019 1:26:39 PM 59.1 -
2/6/2019 1:26:40 PM 59.0 -
2/6/2019 1:26:41 PM 59.0 -
2/6/2019 1:26:42 PM 59.0 -
2/6/2019 1:26:43 PM 59.0 -
2/6/2019 1:26:44 PM 59.0 -
2/6/2019 1:26:45 PM 58.9 -
2/6/2019 1:26:46 PM 58.9 -
2/6/2019 1:26:47 PM 58.9 -
2/6/2019 1:26:48 PM 58.9 -
2/6/2019 1:26:49 PM 58.9 -
2/6/2019 1:26:50 PM 58.9 -
2/6/2019 1:26:51 PM 58.9 -
2/6/2019 1:26:52 PM 58.8 -
2/6/2019 1:26:53 PM 58.8 -
2/6/2019 1:26:54 PM 58.8 -
2/6/2019 1:26:55 PM 58.8 -
2/6/2019 1:26:56 PM 58.8 -
2/6/2019 1:26:57 PM 58.8 -
2/6/2019 1:26:58 PM 58.7 -
2/6/2019 1:26:59 PM 58.7 -
2/6/2019 1:27:00 PM 58.7 -
2/6/2019 1:27:01 PM 58.7 -
2/6/2019 1:27:02 PM 58.7 -
2/6/2019 1:27:03 PM 58.7 -
2/6/2019 1:27:04 PM 58.7 -
2/6/2019 1:27:05 PM 58.6 -
2/6/2019 1:27:06 PM 58.6 -
2/6/2019 1:27:07 PM 58.6 -
2/6/2019 1:27:08 PM 58.6 -
2/6/2019 1:27:09 PM 58.6 -
2/6/2019 1:27:10 PM 58.6 -
2/6/2019 1:27:11 PM 58.5 -
2/6/2019 1:27:12 PM 58.5 -
2/6/2019 1:27:13 PM 58.5 -
2/6/2019 1:27:14 PM 58.5 -
2/6/2019 1:27:15 PM 58.5 -
2/6/2019 1:27:16 PM 58.5 -
2/6/2019 1:27:17 PM 58.5 -
2/6/2019 1:27:18 PM 58.5 -
2/6/2019 1:27:19 PM 58.5 -
2/6/2019 1:27:20 PM 58.5 -
2/6/2019 1:27:21 PM 58.6 -
Table E1 SEEP-B3 TEST-2 Data Log
Page 323 of 452 August 2019
APPENDIX E51: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-2 Data Log
2/6/2019 1:27:22 PM 58.7 -
2/6/2019 1:27:23 PM 58.8 -
2/6/2019 1:27:24 PM 59.0 -
2/6/2019 1:27:25 PM 59.3 -
2/6/2019 1:27:26 PM 59.8 -
2/6/2019 1:27:27 PM 60.4 1.3
2/6/2019 1:27:28 PM 61.3 2.2
2/6/2019 1:27:29 PM 62.5 3.4
2/6/2019 1:27:30 PM 64.2 5.1
2/6/2019 1:27:31 PM 65.9 6.8
2/6/2019 1:27:32 PM 68.8 9.7
2/6/2019 1:27:33 PM 71.9 12.8
2/6/2019 1:27:34 PM 76.3 17.2
2/6/2019 1:27:35 PM 135.0 75.9
2/6/2019 1:27:36 PM 148.1 89.0
2/6/2019 1:27:37 PM 167.5 108.4
2/6/2019 1:27:38 PM 181.9 122.8
2/6/2019 1:27:39 PM 196.3 137.2
2/6/2019 1:27:40 PM 206.6 147.5
2/6/2019 1:27:41 PM 267.1 208.0
2/6/2019 1:27:42 PM 305.2 246.1
2/6/2019 1:27:43 PM 347.1 288.0
2/6/2019 1:27:44 PM 375.7 316.6
2/6/2019 1:27:45 PM 384.5 325.4
2/6/2019 1:27:46 PM 407.5 348.4
2/6/2019 1:27:47 PM 502.4 443.3
2/6/2019 1:27:48 PM 543.4 484.3
2/6/2019 1:27:49 PM 605.3 546.2
2/6/2019 1:27:50 PM 624.2 565.1
2/6/2019 1:27:51 PM 639.9 580.8
2/6/2019 1:27:52 PM 726.8 667.7
2/6/2019 1:27:53 PM 785.9 726.8
2/6/2019 1:27:54 PM 862.8 803.7
2/6/2019 1:27:55 PM 898.0 838.9
2/6/2019 1:27:56 PM 925.2 866.1
2/6/2019 1:27:57 PM 1016.1 957.0
2/6/2019 1:27:58 PM 1077.7 1018.6
2/6/2019 1:27:59 PM 1163.2 1104.1
2/6/2019 1:28:00 PM 1180.4 1121.3
2/6/2019 1:28:01 PM 1288.4 1229.3
2/6/2019 1:28:02 PM 1339.2 1280.1
2/6/2019 1:28:03 PM 1395.0 1335.9
2/6/2019 1:28:04 PM 1441.2 1382.1
2/6/2019 1:28:05 PM 1477.5 1418.4
2/6/2019 1:28:06 PM 1586.5 1527.4
2/6/2019 1:28:07 PM 1637.6 1578.5
2/6/2019 1:28:08 PM 1698.9 1639.8
2/6/2019 1:28:09 PM 1743.8 1684.7
2/6/2019 1:28:10 PM 1769.4 1710.3
2/6/2019 1:28:11 PM 1809.0 1749.9
2/6/2019 1:28:12 PM 1833.0 1773.9
2/6/2019 1:28:13 PM 1854.5 1795.4
2/6/2019 1:28:14 PM 1988.1 1929.0
2/6/2019 1:28:15 PM 2033.6 1974.5
2/6/2019 1:28:16 PM 2076.4 2017.3
2/6/2019 1:28:17 PM 2093.4 2034.3
2/6/2019 1:28:18 PM 2114.6 2055.5
2/6/2019 1:28:19 PM 2131.5 2072.4
2/6/2019 1:28:20 PM 2146.2 2087.1
2/6/2019 1:28:21 PM 2161.5 2102.4
2/6/2019 1:28:22 PM 2179.9 2120.8
2/6/2019 1:28:23 PM 2194.2 2135.1
2/6/2019 1:28:24 PM 2208.6 2149.5
2/6/2019 1:28:25 PM 2220.2 2161.1
2/6/2019 1:28:26 PM 2231.7 2172.6
2/6/2019 1:28:27 PM 2240.6 2181.5
2/6/2019 1:28:28 PM 2250.9 2191.8
2/6/2019 1:28:29 PM 2259.4 2200.3
2/6/2019 1:28:30 PM 2270.0 2210.9
2/6/2019 1:28:31 PM 2287.3 2228.2
2/6/2019 1:28:32 PM 2306.1 2247.0
2/6/2019 1:28:33 PM 2319.9 2260.8
2/6/2019 1:28:34 PM 2332.7 2273.6
2/6/2019 1:28:35 PM 2341.0 2281.9
2/6/2019 1:28:36 PM 2348.5 2289.4
2/6/2019 1:28:37 PM 2353.3 2294.2
2/6/2019 1:28:38 PM 2357.0 2297.9
Page 324 of 452 August 2019
APPENDIX E51: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-2 Data Log
2/6/2019 1:28:39 PM 2359.0 2299.9
2/6/2019 1:28:40 PM 2359.7 2300.6
2/6/2019 1:28:41 PM 2358.2 2299.1
2/6/2019 1:28:42 PM 2354.4 2295.3
2/6/2019 1:28:43 PM 2349.6 2290.5
2/6/2019 1:28:44 PM 2343.2 2284.1
2/6/2019 1:28:45 PM 2335.7 2276.6
2/6/2019 1:28:46 PM 2325.7 2266.6
2/6/2019 1:28:47 PM 2315.8 2256.7
2/6/2019 1:28:48 PM 2303.1 2244.0
2/6/2019 1:28:49 PM 2291.0 2231.9
2/6/2019 1:28:50 PM 2155.0 2095.9
2/6/2019 1:28:51 PM 2139.7 2080.6
2/6/2019 1:28:52 PM 2113.8 2054.7
2/6/2019 1:28:53 PM 2090.5 2031.4
2/6/2019 1:28:54 PM 2080.7 2021.6
2/6/2019 1:28:55 PM 2069.8 2010.7
2/6/2019 1:28:56 PM 2061.0 2001.9
2/6/2019 1:28:57 PM 2052.8 1993.7
2/6/2019 1:28:58 PM 2039.1 1980.0
2/6/2019 1:28:59 PM 2027.4 1968.3
2/6/2019 1:29:00 PM 2014.6 1955.5
2/6/2019 1:29:01 PM 2001.5 1942.4
2/6/2019 1:29:02 PM 1990.8 1931.7
2/6/2019 1:29:03 PM 1873.4 1814.3
2/6/2019 1:29:04 PM 1848.6 1789.5
2/6/2019 1:29:05 PM 1808.7 1749.6
2/6/2019 1:29:06 PM 1800.6 1741.5
2/6/2019 1:29:07 PM 1790.6 1731.5
2/6/2019 1:29:08 PM 1777.1 1718.0
2/6/2019 1:29:09 PM 1764.1 1705.0
2/6/2019 1:29:10 PM 1751.7 1692.6
2/6/2019 1:29:11 PM 1736.2 1677.1
2/6/2019 1:29:12 PM 1631.0 1571.9
2/6/2019 1:29:13 PM 1618.6 1559.5
2/6/2019 1:29:14 PM 1593.5 1534.4
2/6/2019 1:29:15 PM 1570.6 1511.5
2/6/2019 1:29:16 PM 1563.7 1504.6
2/6/2019 1:29:17 PM 1546.1 1487.0
2/6/2019 1:29:18 PM 1527.5 1468.4
2/6/2019 1:29:19 PM 1509.6 1450.5
2/6/2019 1:29:20 PM 1498.5 1439.4
2/6/2019 1:29:21 PM 1487.7 1428.6
2/6/2019 1:29:22 PM 1384.1 1325.0
2/6/2019 1:29:23 PM 1378.0 1318.9
2/6/2019 1:29:24 PM 1350.8 1291.7
2/6/2019 1:29:25 PM 1333.0 1273.9
2/6/2019 1:29:26 PM 1315.6 1256.5
2/6/2019 1:29:27 PM 1307.8 1248.7
2/6/2019 1:29:28 PM 1300.6 1241.5
2/6/2019 1:29:29 PM 1288.0 1228.9
2/6/2019 1:29:30 PM 1210.0 1150.9
2/6/2019 1:29:31 PM 1191.3 1132.2
2/6/2019 1:29:32 PM 1172.0 1112.9
2/6/2019 1:29:33 PM 1151.4 1092.3
2/6/2019 1:29:34 PM 1142.3 1083.2
2/6/2019 1:29:35 PM 1132.7 1073.6
2/6/2019 1:29:36 PM 1125.2 1066.1
2/6/2019 1:29:37 PM 1114.9 1055.8
2/6/2019 1:29:38 PM 1105.2 1046.1
2/6/2019 1:29:39 PM 1096.0 1036.9
2/6/2019 1:29:40 PM 1015.4 956.3
2/6/2019 1:29:41 PM 1003.3 944.2
2/6/2019 1:29:42 PM 977.5 918.4
2/6/2019 1:29:43 PM 968.7 909.6
2/6/2019 1:29:44 PM 956.5 897.4
2/6/2019 1:29:45 PM 947.2 888.1
2/6/2019 1:29:46 PM 939.5 880.4
2/6/2019 1:29:47 PM 933.1 874.0
2/6/2019 1:29:48 PM 925.6 866.5
2/6/2019 1:29:49 PM 870.5 811.4
2/6/2019 1:29:50 PM 854.9 795.8
2/6/2019 1:29:51 PM 839.1 780.0
2/6/2019 1:29:52 PM 828.6 769.5
2/6/2019 1:29:53 PM 817.9 758.8
2/6/2019 1:29:54 PM 806.8 747.7
2/6/2019 1:29:55 PM 800.0 740.9
2/6/2019 1:29:56 PM 793.5 734.4
2/6/2019 1:29:57 PM 788.6 729.5
Page 325 of 452 August 2019
APPENDIX E51: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-2 Data Log
2/6/2019 1:29:58 PM 781.3 722.2
2/6/2019 1:29:59 PM 728.9 669.8
2/6/2019 1:30:00 PM 715.3 656.2
2/6/2019 1:30:01 PM 705.1 646.0
2/6/2019 1:30:02 PM 707.3 648.2
2/6/2019 1:30:03 PM 697.9 638.8
2/6/2019 1:30:04 PM 687.5 628.4
2/6/2019 1:30:05 PM 681.4 622.3
2/6/2019 1:30:06 PM 675.1 616.0
2/6/2019 1:30:07 PM 670.1 611.0
2/6/2019 1:30:08 PM 666.8 607.7
2/6/2019 1:30:09 PM 590.5 531.4
2/6/2019 1:30:10 PM 605.6 546.5
2/6/2019 1:30:11 PM 600.9 541.8
2/6/2019 1:30:12 PM 596.1 537.0
2/6/2019 1:30:13 PM 591.4 532.3
2/6/2019 1:30:14 PM 585.6 526.5
2/6/2019 1:30:15 PM 581.5 522.4
2/6/2019 1:30:16 PM 576.4 517.3
2/6/2019 1:30:17 PM 571.9 512.8
2/6/2019 1:30:18 PM 566.8 507.7
2/6/2019 1:30:19 PM 562.5 503.4
2/6/2019 1:30:20 PM 557.2 498.1
2/6/2019 1:30:21 PM 552.9 493.8
2/6/2019 1:30:22 PM 504.1 445.0
2/6/2019 1:30:23 PM 498.9 439.8
2/6/2019 1:30:24 PM 492.5 433.4
2/6/2019 1:30:25 PM 489.0 429.9
2/6/2019 1:30:26 PM 481.8 422.7
2/6/2019 1:30:27 PM 477.3 418.2
2/6/2019 1:30:28 PM 473.4 414.3
2/6/2019 1:30:29 PM 470.5 411.4
2/6/2019 1:30:30 PM 466.7 407.6
2/6/2019 1:30:31 PM 463.6 404.5
2/6/2019 1:30:32 PM 459.7 400.6
2/6/2019 1:30:33 PM 456.2 397.1
2/6/2019 1:30:34 PM 452.4 393.3
2/6/2019 1:30:35 PM 449.3 390.2
2/6/2019 1:30:36 PM 446.1 387.0
2/6/2019 1:30:37 PM 444.0 384.9
2/6/2019 1:30:38 PM 440.3 381.2
2/6/2019 1:30:39 PM 433.7 374.6
2/6/2019 1:30:40 PM 426.6 367.5
2/6/2019 1:30:41 PM 421.9 362.8
2/6/2019 1:30:42 PM 414.9 355.8
2/6/2019 1:30:43 PM 408.8 349.7
2/6/2019 1:30:44 PM 403.6 344.5
2/6/2019 1:30:45 PM 397.9 338.8
2/6/2019 1:30:46 PM 393.1 334.0
2/6/2019 1:30:47 PM 387.5 328.4
2/6/2019 1:30:48 PM 382.7 323.6
2/6/2019 1:30:49 PM 377.0 317.9
2/6/2019 1:30:50 PM 372.0 312.9
2/6/2019 1:30:51 PM 366.5 307.4
2/6/2019 1:30:52 PM 361.9 302.8
2/6/2019 1:30:53 PM 356.7 297.6
2/6/2019 1:30:54 PM 352.3 293.2
2/6/2019 1:30:55 PM 347.4 288.3
2/6/2019 1:30:56 PM 343.2 284.1
2/6/2019 1:30:57 PM 338.4 279.3
2/6/2019 1:30:58 PM 334.4 275.3
2/6/2019 1:30:59 PM 330.2 271.1
2/6/2019 1:31:00 PM 326.5 267.4
2/6/2019 1:31:01 PM 322.4 263.3
2/6/2019 1:31:02 PM 318.9 259.8
2/6/2019 1:31:03 PM 315.2 256.1
2/6/2019 1:31:04 PM 312.0 252.9
2/6/2019 1:31:05 PM 308.5 249.4
2/6/2019 1:31:06 PM 305.4 246.3
2/6/2019 1:31:07 PM 302.0 242.9
2/6/2019 1:31:08 PM 299.0 239.9
2/6/2019 1:31:09 PM 295.6 236.5
2/6/2019 1:31:10 PM 292.7 233.6
2/6/2019 1:31:11 PM 289.3 230.2
2/6/2019 1:31:12 PM 286.5 227.4
2/6/2019 1:31:13 PM 283.3 224.2
2/6/2019 1:31:14 PM 280.6 221.5
2/6/2019 1:31:15 PM 277.5 218.4
2/6/2019 1:31:16 PM 274.7 215.6
Page 326 of 452 August 2019
APPENDIX E51: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-2 Data Log
2/6/2019 1:31:17 PM 271.5 212.4
2/6/2019 1:31:18 PM 268.3 209.2
2/6/2019 1:31:19 PM 265.5 206.4
2/6/2019 1:31:20 PM 262.2 203.1
2/6/2019 1:31:21 PM 259.5 200.4
2/6/2019 1:31:22 PM 256.8 197.7
2/6/2019 1:31:23 PM 254.3 195.2
2/6/2019 1:31:24 PM 251.6 192.5
2/6/2019 1:31:25 PM 249.3 190.2
2/6/2019 1:31:26 PM 246.7 187.6
2/6/2019 1:31:27 PM 244.3 185.2
2/6/2019 1:31:28 PM 241.9 182.8
2/6/2019 1:31:29 PM 239.9 180.8
2/6/2019 1:31:30 PM 237.4 178.3
2/6/2019 1:31:31 PM 235.4 176.3
2/6/2019 1:31:32 PM 233.3 174.2
2/6/2019 1:31:33 PM 231.5 172.4
2/6/2019 1:31:34 PM 229.5 170.4
2/6/2019 1:31:35 PM 227.6 168.5
2/6/2019 1:31:36 PM 225.5 166.4
2/6/2019 1:31:37 PM 223.8 164.7
2/6/2019 1:31:38 PM 221.7 162.6
2/6/2019 1:31:39 PM 219.8 160.7
2/6/2019 1:31:40 PM 217.9 158.8
2/6/2019 1:31:41 PM 216.1 157.0
2/6/2019 1:31:42 PM 214.2 155.1
2/6/2019 1:31:43 PM 212.6 153.5
2/6/2019 1:31:44 PM 210.7 151.6
2/6/2019 1:31:45 PM 209.1 150.0
2/6/2019 1:31:46 PM 207.2 148.1
2/6/2019 1:31:47 PM 205.6 146.5
2/6/2019 1:31:48 PM 203.9 144.8
2/6/2019 1:31:49 PM 202.4 143.3
2/6/2019 1:31:50 PM 200.8 141.7
2/6/2019 1:31:51 PM 199.4 140.3
2/6/2019 1:31:52 PM 198.0 138.9
2/6/2019 1:31:53 PM 196.6 137.5
2/6/2019 1:31:54 PM 195.1 136.0
2/6/2019 1:31:55 PM 193.7 134.6
2/6/2019 1:31:56 PM 192.3 133.2
2/6/2019 1:31:57 PM 191.0 131.9
2/6/2019 1:31:58 PM 189.6 130.5
2/6/2019 1:31:59 PM 188.4 129.3
2/6/2019 1:32:00 PM 187.1 128.0
2/6/2019 1:32:01 PM 185.7 126.6
2/6/2019 1:32:02 PM 184.6 125.5
2/6/2019 1:32:03 PM 183.3 124.2
2/6/2019 1:32:04 PM 182.1 123.0
2/6/2019 1:32:05 PM 180.8 121.7
2/6/2019 1:32:06 PM 179.7 120.6
2/6/2019 1:32:07 PM 178.5 119.4
2/6/2019 1:32:08 PM 177.4 118.3
2/6/2019 1:32:09 PM 176.1 117.0
2/6/2019 1:32:10 PM 175.1 116.0
2/6/2019 1:32:11 PM 173.9 114.8
2/6/2019 1:32:12 PM 172.9 113.8
2/6/2019 1:32:13 PM 171.8 112.7
2/6/2019 1:32:14 PM 170.8 111.7
2/6/2019 1:32:15 PM 169.7 110.6
2/6/2019 1:32:16 PM 168.8 109.7
2/6/2019 1:32:17 PM 167.7 108.6
2/6/2019 1:32:18 PM 166.8 107.7
2/6/2019 1:32:19 PM 165.8 106.7
2/6/2019 1:32:20 PM 164.9 105.8
2/6/2019 1:32:21 PM 164.0 104.9
2/6/2019 1:32:22 PM 163.2 104.1
2/6/2019 1:32:23 PM 162.2 103.1
2/6/2019 1:32:24 PM 161.4 102.3
2/6/2019 1:32:25 PM 160.4 101.3
2/6/2019 1:32:26 PM 159.6 100.5
2/6/2019 1:32:27 PM 158.6 99.5
2/6/2019 1:32:28 PM 157.8 98.7
2/6/2019 1:32:29 PM 156.9 97.8
2/6/2019 1:32:30 PM 156.2 97.1
2/6/2019 1:32:31 PM 155.4 96.3
2/6/2019 1:32:32 PM 154.6 95.5
2/6/2019 1:32:33 PM 153.8 94.7
2/6/2019 1:32:34 PM 153.0 93.9
2/6/2019 1:32:35 PM 152.3 93.2
Page 327 of 452 August 2019
APPENDIX E51: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-2 Data Log
2/6/2019 1:32:36 PM 151.6 92.5
2/6/2019 1:32:37 PM 150.8 91.7
2/6/2019 1:32:38 PM 150.2 91.1
2/6/2019 1:32:39 PM 149.5 90.4
2/6/2019 1:32:40 PM 148.8 89.7
2/6/2019 1:32:41 PM 148.1 89.0
2/6/2019 1:32:42 PM 147.4 88.3
2/6/2019 1:32:43 PM 146.8 87.7
2/6/2019 1:32:44 PM 146.2 87.1
2/6/2019 1:32:45 PM 145.6 86.5
2/6/2019 1:32:46 PM 145.0 85.9
2/6/2019 1:32:47 PM 144.5 85.4
2/6/2019 1:32:48 PM 143.9 84.8
2/6/2019 1:32:49 PM 143.4 84.3
2/6/2019 1:32:50 PM 142.7 83.6
2/6/2019 1:32:51 PM 142.2 83.1
2/6/2019 1:32:52 PM 141.7 82.6
2/6/2019 1:32:53 PM 141.2 82.1
2/6/2019 1:32:54 PM 140.6 81.5
2/6/2019 1:32:55 PM 140.2 81.1
2/6/2019 1:32:56 PM 139.6 80.5
2/6/2019 1:32:57 PM 139.2 80.1
2/6/2019 1:32:58 PM 138.6 79.5
2/6/2019 1:32:59 PM 138.1 79.0
2/6/2019 1:33:00 PM 137.5 78.4
2/6/2019 1:33:01 PM 137.0 77.9
2/6/2019 1:33:02 PM 136.5 77.4
2/6/2019 1:33:03 PM 136.0 76.9
2/6/2019 1:33:04 PM 135.6 76.5
2/6/2019 1:33:05 PM 135.2 76.1
2/6/2019 1:33:06 PM 134.7 75.6
2/6/2019 1:33:07 PM 134.3 75.2
2/6/2019 1:33:08 PM 133.9 74.8
2/6/2019 1:33:09 PM 133.5 74.4
2/6/2019 1:33:10 PM 133.0 73.9
2/6/2019 1:33:11 PM 132.7 73.6
2/6/2019 1:33:12 PM 132.4 73.3
2/6/2019 1:33:13 PM 132.1 73.0
2/6/2019 1:33:14 PM 131.7 72.6
2/6/2019 1:33:15 PM 131.4 72.3
2/6/2019 1:33:16 PM 131.0 71.9
2/6/2019 1:33:17 PM 130.7 71.6
2/6/2019 1:33:18 PM 130.3 71.2
2/6/2019 1:33:19 PM 130.0 70.9
2/6/2019 1:33:20 PM 129.6 70.5
2/6/2019 1:33:21 PM 129.3 70.2
2/6/2019 1:33:22 PM 129.0 69.9
2/6/2019 1:33:23 PM 128.7 69.6
2/6/2019 1:33:24 PM 128.4 69.3
2/6/2019 1:33:25 PM 128.0 68.9
2/6/2019 1:33:26 PM 127.7 68.6
2/6/2019 1:33:27 PM 127.4 68.3
2/6/2019 1:33:28 PM 127.1 68.0
2/6/2019 1:33:29 PM 126.7 67.6
2/6/2019 1:33:30 PM 126.4 67.3
2/6/2019 1:33:31 PM 126.0 66.9
2/6/2019 1:33:32 PM 125.7 66.6
2/6/2019 1:33:33 PM 125.3 66.2
2/6/2019 1:33:34 PM 125.1 66.0
2/6/2019 1:33:35 PM 124.8 65.7
2/6/2019 1:33:36 PM 124.5 65.4
2/6/2019 1:33:37 PM 124.2 65.1
2/6/2019 1:33:38 PM 123.9 64.8
2/6/2019 1:33:39 PM 123.5 64.4
2/6/2019 1:33:40 PM 123.2 64.1
2/6/2019 1:33:41 PM 122.9 63.8
2/6/2019 1:33:42 PM 122.5 63.4
2/6/2019 1:33:43 PM 122.3 63.2
2/6/2019 1:33:44 PM 121.9 62.8
2/6/2019 1:33:45 PM 121.6 62.5
2/6/2019 1:33:46 PM 121.3 62.2
2/6/2019 1:33:47 PM 120.9 61.8
2/6/2019 1:33:48 PM 120.6 61.5
2/6/2019 1:33:49 PM 120.2 61.1
2/6/2019 1:33:50 PM 119.9 60.8
2/6/2019 1:33:51 PM 119.6 60.5
2/6/2019 1:33:52 PM 119.3 60.2
2/6/2019 1:33:53 PM 119.0 59.9
2/6/2019 1:33:54 PM 118.7 59.6
Page 328 of 452 August 2019
APPENDIX E51: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-2 Data Log
2/6/2019 1:33:55 PM 118.4 59.3
2/6/2019 1:33:56 PM 118.1 59.0
2/6/2019 1:33:57 PM 117.8 58.7
2/6/2019 1:33:58 PM 117.5 58.4
2/6/2019 1:33:59 PM 117.2 58.1
2/6/2019 1:34:00 PM 116.9 57.8
2/6/2019 1:34:01 PM 116.5 57.4
2/6/2019 1:34:02 PM 116.2 57.1
2/6/2019 1:34:03 PM 115.9 56.8
2/6/2019 1:34:04 PM 115.5 56.4
2/6/2019 1:34:05 PM 115.2 56.1
2/6/2019 1:34:06 PM 114.9 55.8
2/6/2019 1:34:07 PM 114.5 55.4
2/6/2019 1:34:08 PM 114.2 55.1
2/6/2019 1:34:09 PM 113.8 54.7
2/6/2019 1:34:10 PM 113.5 54.4
2/6/2019 1:34:11 PM 113.2 54.1
2/6/2019 1:34:12 PM 112.9 53.8
2/6/2019 1:34:13 PM 112.5 53.4
2/6/2019 1:34:14 PM 112.2 53.1
2/6/2019 1:34:15 PM 111.9 52.8
2/6/2019 1:34:16 PM 111.6 52.5
2/6/2019 1:34:17 PM 111.3 52.2
2/6/2019 1:34:18 PM 111.0 51.9
2/6/2019 1:34:19 PM 110.7 51.6
2/6/2019 1:34:20 PM 110.3 51.2
2/6/2019 1:34:21 PM 110.0 50.9
2/6/2019 1:34:22 PM 109.7 50.6
2/6/2019 1:34:23 PM 109.4 50.3
2/6/2019 1:34:24 PM 109.1 50.0
2/6/2019 1:34:25 PM 108.8 49.7
2/6/2019 1:34:26 PM 108.4 49.3
2/6/2019 1:34:27 PM 108.1 49.0
2/6/2019 1:34:28 PM 107.8 48.7
2/6/2019 1:34:29 PM 107.5 48.4
2/6/2019 1:34:30 PM 107.2 48.1
2/6/2019 1:34:31 PM 106.9 47.8
2/6/2019 1:34:32 PM 106.7 47.6
2/6/2019 1:34:33 PM 106.4 47.3
2/6/2019 1:34:34 PM 106.1 47.0
2/6/2019 1:34:35 PM 105.9 46.8
2/6/2019 1:34:36 PM 105.6 46.5
2/6/2019 1:34:37 PM 105.4 46.3
2/6/2019 1:34:38 PM 105.1 46.0
2/6/2019 1:34:39 PM 104.9 45.8
2/6/2019 1:34:40 PM 104.7 45.6
2/6/2019 1:34:41 PM 104.4 45.3
2/6/2019 1:34:42 PM 104.2 45.1
2/6/2019 1:34:43 PM 103.9 44.8
2/6/2019 1:34:44 PM 103.7 44.6
2/6/2019 1:34:45 PM 103.5 44.4
2/6/2019 1:34:46 PM 103.2 44.1
2/6/2019 1:34:47 PM 103.0 43.9
2/6/2019 1:34:48 PM 102.8 43.7
2/6/2019 1:34:49 PM 102.6 43.5
2/6/2019 1:34:50 PM 102.4 43.3
2/6/2019 1:34:51 PM 102.2 43.1
2/6/2019 1:34:52 PM 102.0 42.9
2/6/2019 1:34:53 PM 101.8 42.7
2/6/2019 1:34:54 PM 101.6 42.5
2/6/2019 1:34:55 PM 101.4 42.3
2/6/2019 1:34:56 PM 101.2 42.1
2/6/2019 1:34:57 PM 101.0 41.9
2/6/2019 1:34:58 PM 100.8 41.7
2/6/2019 1:34:59 PM 100.6 41.5
2/6/2019 1:35:00 PM 100.4 41.3
2/6/2019 1:35:01 PM 100.2 41.1
2/6/2019 1:35:02 PM 100.0 40.9
2/6/2019 1:35:03 PM 99.8 40.7
2/6/2019 1:35:04 PM 99.6 40.5
2/6/2019 1:35:05 PM 99.4 40.3
2/6/2019 1:35:06 PM 99.3 40.2
2/6/2019 1:35:07 PM 99.1 40.0
2/6/2019 1:35:08 PM 98.9 39.8
2/6/2019 1:35:09 PM 98.7 39.6
2/6/2019 1:35:10 PM 98.6 39.5
2/6/2019 1:35:11 PM 98.4 39.3
2/6/2019 1:35:12 PM 98.2 39.1
2/6/2019 1:35:13 PM 98.0 38.9
Page 329 of 452 August 2019
APPENDIX E51: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-2 Data Log
2/6/2019 1:35:14 PM 97.9 38.8
2/6/2019 1:35:15 PM 97.7 38.6
2/6/2019 1:35:16 PM 97.6 38.5
2/6/2019 1:35:17 PM 97.4 38.3
2/6/2019 1:35:18 PM 97.2 38.1
2/6/2019 1:35:19 PM 97.0 37.9
2/6/2019 1:35:20 PM 96.9 37.8
2/6/2019 1:35:21 PM 96.7 37.6
2/6/2019 1:35:22 PM 96.5 37.4
2/6/2019 1:35:23 PM 96.4 37.3
2/6/2019 1:35:24 PM 96.2 37.1
2/6/2019 1:35:25 PM 96.1 37.0
2/6/2019 1:35:26 PM 96.0 36.9
2/6/2019 1:35:27 PM 95.8 36.7
2/6/2019 1:35:28 PM 95.7 36.6
2/6/2019 1:35:29 PM 95.5 36.4
2/6/2019 1:35:30 PM 95.4 36.3
2/6/2019 1:35:31 PM 95.2 36.1
2/6/2019 1:35:32 PM 95.1 36.0
2/6/2019 1:35:33 PM 95.0 35.9
2/6/2019 1:35:34 PM 94.9 35.8
2/6/2019 1:35:35 PM 94.7 35.6
2/6/2019 1:35:36 PM 94.6 35.5
2/6/2019 1:35:37 PM 94.4 35.3
2/6/2019 1:35:38 PM 94.2 35.1
2/6/2019 1:35:39 PM 94.1 35.0
2/6/2019 1:35:40 PM 93.9 34.8
2/6/2019 1:35:41 PM 93.8 34.7
2/6/2019 1:35:42 PM 93.6 34.5
2/6/2019 1:35:43 PM 93.5 34.4
2/6/2019 1:35:44 PM 93.3 34.2
2/6/2019 1:35:45 PM 93.1 34.0
2/6/2019 1:35:46 PM 93.0 33.9
2/6/2019 1:35:47 PM 92.8 33.7
2/6/2019 1:35:48 PM 92.7 33.6
2/6/2019 1:35:49 PM 92.5 33.4
2/6/2019 1:35:50 PM 92.4 33.3
2/6/2019 1:35:51 PM 92.2 33.1
2/6/2019 1:35:52 PM 92.1 33.0
2/6/2019 1:35:53 PM 92.0 32.9
2/6/2019 1:35:54 PM 91.8 32.7
2/6/2019 1:35:55 PM 91.7 32.6
2/6/2019 1:35:56 PM 91.6 32.5
2/6/2019 1:35:57 PM 91.5 32.4
2/6/2019 1:35:58 PM 91.3 32.2
2/6/2019 1:35:59 PM 91.2 32.1
2/6/2019 1:36:00 PM 91.1 32.0
2/6/2019 1:36:01 PM 90.9 31.8
2/6/2019 1:36:02 PM 90.8 31.7
2/6/2019 1:36:03 PM 90.7 31.6
2/6/2019 1:36:04 PM 90.6 31.5
2/6/2019 1:36:05 PM 90.5 31.4
2/6/2019 1:36:06 PM 90.3 31.2
2/6/2019 1:36:07 PM 90.2 31.1
2/6/2019 1:36:08 PM 90.1 31.0
2/6/2019 1:36:09 PM 89.9 30.8
2/6/2019 1:36:10 PM 89.8 30.7
2/6/2019 1:36:11 PM 89.7 30.6
2/6/2019 1:36:12 PM 89.5 30.4
2/6/2019 1:36:13 PM 89.4 30.3
2/6/2019 1:36:14 PM 89.3 30.2
2/6/2019 1:36:15 PM 89.1 30.0
2/6/2019 1:36:16 PM 89.0 29.9
2/6/2019 1:36:17 PM 88.9 29.8
2/6/2019 1:36:18 PM 88.7 29.6
2/6/2019 1:36:19 PM 88.6 29.5
2/6/2019 1:36:20 PM 88.5 29.4
2/6/2019 1:36:21 PM 88.4 29.3
2/6/2019 1:36:22 PM 88.3 29.2
2/6/2019 1:36:23 PM 88.2 29.1
2/6/2019 1:36:24 PM 88.1 29.0
2/6/2019 1:36:25 PM 87.9 28.8
2/6/2019 1:36:26 PM 87.8 28.7
2/6/2019 1:36:27 PM 87.7 28.6
2/6/2019 1:36:28 PM 87.6 28.5
2/6/2019 1:36:29 PM 87.5 28.4
2/6/2019 1:36:30 PM 87.4 28.3
2/6/2019 1:36:31 PM 87.2 28.1
2/6/2019 1:36:32 PM 87.1 28.0
Page 330 of 452 August 2019
APPENDIX E51: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-2 Data Log
2/6/2019 1:36:33 PM 87.0 27.9
2/6/2019 1:36:34 PM 86.9 27.8
2/6/2019 1:36:35 PM 86.7 27.6
2/6/2019 1:36:36 PM 86.6 27.5
2/6/2019 1:36:37 PM 86.5 27.4
2/6/2019 1:36:38 PM 86.3 27.2
2/6/2019 1:36:39 PM 86.2 27.1
2/6/2019 1:36:40 PM 86.1 27.0
2/6/2019 1:36:41 PM 85.9 26.8
2/6/2019 1:36:42 PM 85.8 26.7
2/6/2019 1:36:43 PM 85.7 26.6
2/6/2019 1:36:44 PM 85.5 26.4
2/6/2019 1:36:45 PM 85.4 26.3
2/6/2019 1:36:46 PM 85.3 26.2
2/6/2019 1:36:47 PM 85.2 26.1
2/6/2019 1:36:48 PM 85.1 26.0
2/6/2019 1:36:49 PM 85.0 25.9
2/6/2019 1:36:50 PM 84.9 25.8
2/6/2019 1:36:51 PM 84.8 25.7
2/6/2019 1:36:52 PM 84.7 25.6
2/6/2019 1:36:53 PM 84.5 25.4
2/6/2019 1:36:54 PM 84.4 25.3
2/6/2019 1:36:55 PM 84.3 25.2
2/6/2019 1:36:56 PM 84.2 25.1
2/6/2019 1:36:57 PM 84.1 25.0
2/6/2019 1:36:58 PM 84.0 24.9
2/6/2019 1:36:59 PM 83.9 24.8
2/6/2019 1:37:00 PM 83.9 24.8
2/6/2019 1:37:01 PM 83.7 24.6
2/6/2019 1:37:02 PM 83.7 24.6
2/6/2019 1:37:03 PM 83.6 24.5
2/6/2019 1:37:04 PM 83.5 24.4
2/6/2019 1:37:05 PM 83.4 24.3
2/6/2019 1:37:06 PM 83.3 24.2
2/6/2019 1:37:07 PM 83.2 24.1
2/6/2019 1:37:08 PM 83.2 24.1
2/6/2019 1:37:09 PM 83.1 24.0
2/6/2019 1:37:10 PM 83.0 23.9
2/6/2019 1:37:11 PM 82.9 23.8
2/6/2019 1:37:12 PM 82.8 23.7
2/6/2019 1:37:13 PM 82.8 23.7
2/6/2019 1:37:14 PM 82.7 23.6
2/6/2019 1:37:15 PM 82.6 23.5
2/6/2019 1:37:16 PM 82.5 23.4
2/6/2019 1:37:17 PM 82.4 23.3
2/6/2019 1:37:18 PM 82.3 23.2
2/6/2019 1:37:19 PM 82.2 23.1
2/6/2019 1:37:20 PM 82.1 23.0
2/6/2019 1:37:21 PM 82.1 23.0
2/6/2019 1:37:22 PM 82.0 22.9
2/6/2019 1:37:23 PM 81.9 22.8
2/6/2019 1:37:24 PM 81.8 22.7
2/6/2019 1:37:25 PM 81.7 22.6
2/6/2019 1:37:26 PM 81.7 22.6
2/6/2019 1:37:27 PM 81.6 22.5
2/6/2019 1:37:28 PM 81.5 22.4
2/6/2019 1:37:29 PM 81.4 22.3
2/6/2019 1:37:30 PM 81.4 22.3
2/6/2019 1:37:31 PM 81.3 22.2
2/6/2019 1:37:32 PM 81.2 22.1
2/6/2019 1:37:33 PM 81.2 22.1
2/6/2019 1:37:34 PM 81.1 22.0
2/6/2019 1:37:35 PM 81.0 21.9
2/6/2019 1:37:36 PM 80.9 21.8
2/6/2019 1:37:37 PM 80.9 21.8
2/6/2019 1:37:38 PM 80.8 21.7
2/6/2019 1:37:39 PM 80.8 21.7
2/6/2019 1:37:40 PM 80.7 21.6
2/6/2019 1:37:41 PM 80.7 21.6
2/6/2019 1:37:42 PM 80.6 21.5
2/6/2019 1:37:43 PM 80.6 21.5
2/6/2019 1:37:44 PM 80.5 21.4
2/6/2019 1:37:45 PM 80.5 21.4
2/6/2019 1:37:46 PM 80.4 21.3
2/6/2019 1:37:47 PM 80.4 21.3
2/6/2019 1:37:48 PM 80.3 21.2
2/6/2019 1:37:49 PM 80.3 21.2
2/6/2019 1:37:50 PM 80.2 21.1
2/6/2019 1:37:51 PM 80.1 21.0
Page 331 of 452 August 2019
APPENDIX E51: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-2 Data Log
2/6/2019 1:37:52 PM 80.1 21.0
2/6/2019 1:37:53 PM 80.0 20.9
2/6/2019 1:37:54 PM 80.0 20.9
2/6/2019 1:37:55 PM 79.9 20.8
2/6/2019 1:37:56 PM 79.9 20.8
2/6/2019 1:37:57 PM 79.8 20.7
2/6/2019 1:37:58 PM 79.7 20.6
2/6/2019 1:37:59 PM 79.7 20.6
2/6/2019 1:38:00 PM 79.6 20.5
2/6/2019 1:38:01 PM 79.6 20.5
2/6/2019 1:38:02 PM 79.5 20.4
2/6/2019 1:38:03 PM 79.5 20.4
2/6/2019 1:38:04 PM 79.4 20.3
2/6/2019 1:38:05 PM 79.4 20.3
2/6/2019 1:38:06 PM 79.3 20.2
2/6/2019 1:38:07 PM 79.2 20.1
2/6/2019 1:38:08 PM 79.2 20.1
2/6/2019 1:38:09 PM 79.1 20.0
2/6/2019 1:38:10 PM 79.1 20.0
2/6/2019 1:38:11 PM 79.0 19.9
2/6/2019 1:38:12 PM 79.0 19.9
2/6/2019 1:38:13 PM 78.9 19.8
2/6/2019 1:38:14 PM 78.9 19.8
2/6/2019 1:38:15 PM 78.8 19.7
2/6/2019 1:38:16 PM 78.8 19.7
2/6/2019 1:38:17 PM 78.7 19.6
2/6/2019 1:38:18 PM 78.7 19.6
2/6/2019 1:38:19 PM 78.6 19.5
2/6/2019 1:38:20 PM 78.6 19.5
2/6/2019 1:38:21 PM 78.5 19.4
2/6/2019 1:38:22 PM 78.5 19.4
2/6/2019 1:38:23 PM 78.4 19.3
2/6/2019 1:38:24 PM 78.3 19.2
2/6/2019 1:38:25 PM 78.3 19.2
2/6/2019 1:38:26 PM 78.2 19.1
2/6/2019 1:38:27 PM 78.1 19.0
2/6/2019 1:38:28 PM 78.1 19.0
2/6/2019 1:38:29 PM 78.0 18.9
2/6/2019 1:38:30 PM 77.9 18.8
2/6/2019 1:38:31 PM 77.9 18.8
2/6/2019 1:38:32 PM 77.8 18.7
2/6/2019 1:38:33 PM 77.7 18.6
2/6/2019 1:38:34 PM 77.7 18.6
2/6/2019 1:38:35 PM 77.6 18.5
2/6/2019 1:38:36 PM 77.6 18.5
2/6/2019 1:38:37 PM 77.5 18.4
2/6/2019 1:38:38 PM 77.4 18.3
2/6/2019 1:38:39 PM 77.4 18.3
2/6/2019 1:38:40 PM 77.3 18.2
2/6/2019 1:38:41 PM 77.3 18.2
2/6/2019 1:38:42 PM 77.2 18.1
2/6/2019 1:38:43 PM 77.2 18.1
2/6/2019 1:38:44 PM 77.1 18.0
2/6/2019 1:38:45 PM 77.0 17.9
2/6/2019 1:38:46 PM 77.0 17.9
2/6/2019 1:38:47 PM 76.9 17.8
2/6/2019 1:38:48 PM 76.8 17.7
2/6/2019 1:38:49 PM 76.8 17.7
2/6/2019 1:38:50 PM 76.7 17.6
2/6/2019 1:38:51 PM 76.7 17.6
2/6/2019 1:38:52 PM 76.6 17.5
2/6/2019 1:38:53 PM 76.6 17.5
2/6/2019 1:38:54 PM 76.5 17.4
2/6/2019 1:38:55 PM 76.4 17.3
2/6/2019 1:38:56 PM 76.4 17.3
2/6/2019 1:38:57 PM 76.3 17.2
2/6/2019 1:38:58 PM 76.3 17.2
2/6/2019 1:38:59 PM 76.2 17.1
2/6/2019 1:39:00 PM 76.2 17.1
2/6/2019 1:39:01 PM 76.2 17.1
2/6/2019 1:39:02 PM 76.1 17.0
2/6/2019 1:39:03 PM 76.1 17.0
2/6/2019 1:39:04 PM 76.0 16.9
2/6/2019 1:39:05 PM 76.0 16.9
2/6/2019 1:39:06 PM 75.9 16.8
2/6/2019 1:39:07 PM 75.9 16.8
2/6/2019 1:39:08 PM 75.8 16.7
2/6/2019 1:39:09 PM 75.8 16.7
2/6/2019 1:39:10 PM 75.7 16.6
Page 332 of 452 August 2019
APPENDIX E51: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-2 Data Log
2/6/2019 1:39:11 PM 75.7 16.6
2/6/2019 1:39:12 PM 75.6 16.5
2/6/2019 1:39:13 PM 75.6 16.5
2/6/2019 1:39:14 PM 75.5 16.4
2/6/2019 1:39:15 PM 75.5 16.4
2/6/2019 1:39:16 PM 75.4 16.3
2/6/2019 1:39:17 PM 75.4 16.3
2/6/2019 1:39:18 PM 75.4 16.3
2/6/2019 1:39:19 PM 75.3 16.2
2/6/2019 1:39:20 PM 75.3 16.2
2/6/2019 1:39:21 PM 75.3 16.2
2/6/2019 1:39:22 PM 75.2 16.1
2/6/2019 1:39:23 PM 75.2 16.1
2/6/2019 1:39:24 PM 75.1 16.0
2/6/2019 1:39:25 PM 75.1 16.0
2/6/2019 1:39:26 PM 75.1 16.0
2/6/2019 1:39:27 PM 75.0 15.9
2/6/2019 1:39:28 PM 75.0 15.9
2/6/2019 1:39:29 PM 74.9 15.8
2/6/2019 1:39:30 PM 74.9 15.8
2/6/2019 1:39:31 PM 74.8 15.7
2/6/2019 1:39:32 PM 74.8 15.7
2/6/2019 1:39:33 PM 74.8 15.7
2/6/2019 1:39:34 PM 74.8 15.7
2/6/2019 1:39:35 PM 74.7 15.6
2/6/2019 1:39:36 PM 74.7 15.6
2/6/2019 1:39:37 PM 74.7 15.6
2/6/2019 1:39:38 PM 74.6 15.5
2/6/2019 1:39:39 PM 74.6 15.5
2/6/2019 1:39:40 PM 74.6 15.5
2/6/2019 1:39:41 PM 74.6 15.5
2/6/2019 1:39:42 PM 74.5 15.4
2/6/2019 1:39:43 PM 74.5 15.4
2/6/2019 1:39:44 PM 74.5 15.4
2/6/2019 1:39:45 PM 74.4 15.3
2/6/2019 1:39:46 PM 74.4 15.3
2/6/2019 1:39:47 PM 74.3 15.2
2/6/2019 1:39:48 PM 74.3 15.2
2/6/2019 1:39:49 PM 74.2 15.1
2/6/2019 1:39:50 PM 74.2 15.1
2/6/2019 1:39:51 PM 74.1 15.0
2/6/2019 1:39:52 PM 74.1 15.0
2/6/2019 1:39:53 PM 74.1 15.0
2/6/2019 1:39:54 PM 74.0 14.9
2/6/2019 1:39:55 PM 74.0 14.9
2/6/2019 1:39:56 PM 73.9 14.8
2/6/2019 1:39:57 PM 73.9 14.8
2/6/2019 1:39:58 PM 73.8 14.7
2/6/2019 1:39:59 PM 73.8 14.7
2/6/2019 1:40:00 PM 73.7 14.6
2/6/2019 1:40:01 PM 73.7 14.6
2/6/2019 1:40:02 PM 73.7 14.6
2/6/2019 1:40:03 PM 73.6 14.5
2/6/2019 1:40:04 PM 73.6 14.5
2/6/2019 1:40:05 PM 73.5 14.4
2/6/2019 1:40:06 PM 73.5 14.4
2/6/2019 1:40:07 PM 73.4 14.3
2/6/2019 1:40:08 PM 73.4 14.3
2/6/2019 1:40:09 PM 73.4 14.3
2/6/2019 1:40:10 PM 73.3 14.2
2/6/2019 1:40:11 PM 73.3 14.2
2/6/2019 1:40:12 PM 73.2 14.1
2/6/2019 1:40:13 PM 73.2 14.1
2/6/2019 1:40:14 PM 73.2 14.1
2/6/2019 1:40:15 PM 73.1 14.0
2/6/2019 1:40:16 PM 73.1 14.0
2/6/2019 1:40:17 PM 73.0 13.9
2/6/2019 1:40:18 PM 73.0 13.9
2/6/2019 1:40:19 PM 72.9 13.8
2/6/2019 1:40:20 PM 72.9 13.8
2/6/2019 1:40:21 PM 72.9 13.8
2/6/2019 1:40:22 PM 72.8 13.7
2/6/2019 1:40:23 PM 72.8 13.7
2/6/2019 1:40:24 PM 72.7 13.6
2/6/2019 1:40:25 PM 72.7 13.6
2/6/2019 1:40:26 PM 72.7 13.6
2/6/2019 1:40:27 PM 72.6 13.5
2/6/2019 1:40:28 PM 72.6 13.5
2/6/2019 1:40:29 PM 72.6 13.5
Page 333 of 452 August 2019
APPENDIX E51: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B3 TEST-2 Data Log
2/6/2019 1:40:30 PM 72.5 13.4
2/6/2019 1:40:31 PM 72.5 13.4
2/6/2019 1:40:32 PM 72.4 13.3
2/6/2019 1:40:33 PM 72.4 13.3
2/6/2019 1:40:34 PM 72.4 13.3
2/6/2019 1:40:35 PM 72.3 13.2
2/6/2019 1:40:36 PM 72.3 13.2
2/6/2019 1:40:37 PM 72.2 13.1
2/6/2019 1:40:38 PM 72.2 13.1
2/6/2019 1:40:39 PM 72.2 13.1
2/6/2019 1:40:40 PM 72.1 13.0
2/6/2019 1:40:41 PM 72.1 13.0
2/6/2019 1:40:42 PM 72.1 13.0
2/6/2019 1:40:43 PM 72.0 12.9
2/6/2019 1:40:44 PM 72.0 12.9
2/6/2019 1:40:45 PM 72.0 12.9
2/6/2019 1:40:46 PM 71.9 12.8
2/6/2019 1:40:47 PM 71.9 12.8
2/6/2019 1:40:48 PM 71.9 12.8
2/6/2019 1:40:49 PM 71.8 12.7
2/6/2019 1:40:50 PM 71.8 12.7
2/6/2019 1:40:51 PM 71.7 12.6
2/6/2019 1:40:52 PM 71.7 12.6
2/6/2019 1:40:53 PM 71.7 12.6
2/6/2019 1:40:54 PM 71.6 12.5
2/6/2019 1:40:55 PM 71.6 12.5
2/6/2019 1:40:56 PM 71.6 12.5
2/6/2019 1:40:57 PM 71.5 12.4
2/6/2019 1:40:58 PM 71.5 12.4
2/6/2019 1:40:59 PM 71.5 12.4
2/6/2019 1:41:00 PM 71.4 12.3
2/6/2019 1:41:01 PM 71.4 12.3
2/6/2019 1:41:02 PM 71.4 12.3
2/6/2019 1:41:03 PM 71.3 12.2
2/6/2019 1:41:04 PM 71.3 12.2
2/6/2019 1:41:05 PM 71.3 12.2
2/6/2019 1:41:06 PM 71.2 12.1
2/6/2019 1:41:07 PM 71.2 12.1
2/6/2019 1:41:08 PM 71.1 12.0
2/6/2019 1:41:09 PM 71.1 12.0
2/6/2019 1:41:10 PM 71.1 12.0
2/6/2019 1:41:11 PM 71.0 11.9
2/6/2019 1:41:12 PM 71.0 11.9
2/6/2019 1:41:13 PM 70.9 11.8
2/6/2019 1:41:14 PM 70.9 11.8
2/6/2019 1:41:15 PM 70.9 11.8
2/6/2019 1:41:16 PM 70.8 11.7
2/6/2019 1:41:17 PM 70.8 11.7
2/6/2019 1:41:18 PM 70.8 11.7
2/6/2019 1:41:19 PM 70.7 11.6
2/6/2019 1:41:20 PM 70.7 11.6
2/6/2019 1:41:21 PM 70.7 11.6
2/6/2019 1:41:22 PM 70.7 11.6
2/6/2019 1:41:23 PM 70.6 11.5
2/6/2019 1:41:24 PM 70.6 11.5
2/6/2019 1:41:25 PM 70.6 11.5
2/6/2019 1:41:26 PM 70.5 11.4
2/6/2019 1:41:27 PM 70.5 11.4
2/6/2019 1:41:28 PM 70.5 11.4
2/6/2019 1:41:29 PM 70.5 11.4
2/6/2019 1:41:30 PM 70.4 11.3
2/6/2019 1:41:31 PM 70.4 11.3
2/6/2019 1:41:32 PM 70.4 11.3
Page 334 of 452 August 2019
APPENDIX E51: SALT DILUTION GAUGING SUMMARY
SEEP-B3 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-B3 TEST-2 1210
SEEP-B3 TEST-2 1211
SEEP-B3 TEST-2 1213
SEEP-B3 TEST-2 1215
Location EC Reading
(µS/cms)
SEEP-B3 TEST-2 40.2
SEEP-B3 TEST-2 193
SEEP-B3 TEST-2 1,593
SEEP-B3 TEST-2 13,094
SEEP-B3 TEST-2 103,212
q 300,000
K 1.0349
1.2
18.6
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)(°C)
Table E2 SEEP-B3 TEST-2 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Geometric Mean 53.5 (µS/cms)
53.7 12.5
53.5 12.6
53.6 12.6
53.3 12.9
Average 53.5 (µS/cms)
10 20.9
Average (pre-test)59.1 (µS/cms)
Table E3 SEEP-B3 TEST-2 YSI Salt Dilution Calibration Data
Calibration Temperature
(mg/L)(°C)
Slope of Calibration Curve (µS/cms) / (mg/L)
100 21.3
1,000 21.6
10,000 21.9
100,000 21.9
Table E4 SEEP-B3 TEST-2 Flow Calculation Summary
Mass of Salt injected mg
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)265,173.5 (s) . (µS/cms)
Calculated Flow Rate Q
L/s
GPM
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 335 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
6/7/2019 3:09:30 PM 170.0 -
6/7/2019 3:09:31 PM 170.0 -
6/7/2019 3:09:32 PM 169.9 -
6/7/2019 3:09:33 PM 169.9 -
6/7/2019 3:09:34 PM 169.8 -
6/7/2019 3:09:35 PM 169.8 -
6/7/2019 3:09:36 PM 169.7 -
6/7/2019 3:09:37 PM 169.6 -
6/7/2019 3:09:38 PM 169.6 -
6/7/2019 3:09:39 PM 169.5 -
6/7/2019 3:09:40 PM 169.5 -
6/7/2019 3:09:41 PM 169.4 -
6/7/2019 3:09:42 PM 169.4 -
6/7/2019 3:09:43 PM 169.3 -
6/7/2019 3:09:44 PM 169.2 -
6/7/2019 3:09:45 PM 169.2 -
6/7/2019 3:09:46 PM 169.1 -
6/7/2019 3:09:47 PM 169.1 -
6/7/2019 3:09:48 PM 169.0 -
6/7/2019 3:09:49 PM 169.0 -
6/7/2019 3:09:50 PM 168.9 -
6/7/2019 3:09:51 PM 168.9 -
6/7/2019 3:09:52 PM 168.8 -
6/7/2019 3:09:53 PM 168.8 -
6/7/2019 3:09:54 PM 168.8 -
6/7/2019 3:09:55 PM 168.7 -
6/7/2019 3:09:56 PM 168.7 -
6/7/2019 3:09:57 PM 168.6 -
6/7/2019 3:09:58 PM 168.6 -
6/7/2019 3:09:59 PM 168.6 -
6/7/2019 3:10:00 PM 168.6 -
6/7/2019 3:10:01 PM 168.6 -
6/7/2019 3:10:02 PM 168.6 -
6/7/2019 3:10:03 PM 168.5 -
6/7/2019 3:10:04 PM 168.5 -
6/7/2019 3:10:05 PM 168.5 -
6/7/2019 3:10:06 PM 168.5 -
6/7/2019 3:10:07 PM 168.5 -
6/7/2019 3:10:08 PM 168.5 -
6/7/2019 3:10:09 PM 168.5 -
6/7/2019 3:10:10 PM 168.4 -
6/7/2019 3:10:11 PM 168.4 -
6/7/2019 3:10:12 PM 168.4 -
6/7/2019 3:10:13 PM 168.4 -
6/7/2019 3:10:14 PM 168.4 -
6/7/2019 3:10:15 PM 168.3 -
6/7/2019 3:10:16 PM 168.3 -
6/7/2019 3:10:17 PM 168.3 -
6/7/2019 3:10:18 PM 168.3 -
6/7/2019 3:10:19 PM 168.3 -
6/7/2019 3:10:20 PM 168.2 -
6/7/2019 3:10:21 PM 168.2 -
6/7/2019 3:10:22 PM 168.2 -
6/7/2019 3:10:23 PM 168.2 -
6/7/2019 3:10:24 PM 168.1 -
6/7/2019 3:10:25 PM 168.1 -
6/7/2019 3:10:26 PM 168.1 -
6/7/2019 3:10:27 PM 168.1 -
6/7/2019 3:10:28 PM 168.1 -
6/7/2019 3:10:29 PM 168.1 -
6/7/2019 3:10:30 PM 168.1 -
6/7/2019 3:10:31 PM 168.1 -
6/7/2019 3:10:32 PM 168.1 -
6/7/2019 3:10:33 PM 168.0 -
6/7/2019 3:10:34 PM 168.0 -
6/7/2019 3:10:35 PM 168.0 -
6/7/2019 3:10:36 PM 168.0 -
6/7/2019 3:10:37 PM 168.0 -
6/7/2019 3:10:38 PM 168.1 -
6/7/2019 3:10:39 PM 168.3 -
6/7/2019 3:10:40 PM 168.7 -
6/7/2019 3:10:41 PM 169.4 -
6/7/2019 3:10:42 PM 170.6 -
6/7/2019 3:10:43 PM 172.8 -
6/7/2019 3:10:44 PM 224.5 55.7
6/7/2019 3:10:45 PM 249.2 80.4
6/7/2019 3:10:46 PM 288.3 119.5
6/7/2019 3:10:47 PM 323.3 154.5
6/7/2019 3:10:48 PM 347.1 178.3
6/7/2019 3:10:49 PM 457.1 288.3
6/7/2019 3:10:50 PM 524.1 355.3
6/7/2019 3:10:51 PM 655.7 486.9
Table E1 SEEP-B-TR-2 Test-1 Data Log
Page 336 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:10:52 PM 749.9 581.1
6/7/2019 3:10:53 PM 971.0 802.2
6/7/2019 3:10:54 PM 1094.7 925.9
6/7/2019 3:10:55 PM 1279.3 1110.5
6/7/2019 3:10:56 PM 1485.3 1316.5
6/7/2019 3:10:57 PM 1681.4 1512.6
6/7/2019 3:10:58 PM 1866.0 1697.2
6/7/2019 3:10:59 PM 2144.3 1975.5
6/7/2019 3:11:00 PM 2448.2 2279.4
6/7/2019 3:11:01 PM 2762.5 2593.7
6/7/2019 3:11:02 PM 3068.2 2899.4
6/7/2019 3:11:03 PM 3451.9 3283.1
6/7/2019 3:11:04 PM 3799.2 3630.4
6/7/2019 3:11:05 PM 4110.7 3941.9
6/7/2019 3:11:06 PM 4313.8 4145.0
6/7/2019 3:11:07 PM 4823.8 4655.0
6/7/2019 3:11:08 PM 5256.4 5087.6
6/7/2019 3:11:09 PM 5726.8 5558.0
6/7/2019 3:11:10 PM 6014.7 5845.9
6/7/2019 3:11:11 PM 6167.4 5998.6
6/7/2019 3:11:12 PM 6960.4 6791.6
6/7/2019 3:11:13 PM 7561.9 7393.1
6/7/2019 3:11:14 PM 8032.9 7864.1
6/7/2019 3:11:15 PM 8335.6 8166.8
6/7/2019 3:11:16 PM 8579.8 8411.0
6/7/2019 3:11:17 PM 9317.5 9148.7
6/7/2019 3:11:18 PM 9819.7 9650.9
6/7/2019 3:11:19 PM 10219.7 10050.9
6/7/2019 3:11:20 PM 10441.5 10272.7
6/7/2019 3:11:21 PM 10694.7 10525.9
6/7/2019 3:11:22 PM 10951.9 10783.1
6/7/2019 3:11:23 PM 11776.6 11607.8
6/7/2019 3:11:24 PM 12087.9 11919.1
6/7/2019 3:11:25 PM 12474.2 12305.4
6/7/2019 3:11:26 PM 12582.5 12413.7
6/7/2019 3:11:27 PM 12724.8 12556.0
6/7/2019 3:11:28 PM 12835.3 12666.5
6/7/2019 3:11:29 PM 12970.7 12801.9
6/7/2019 3:11:30 PM 13078.9 12910.1
6/7/2019 3:11:31 PM 13193.2 13024.4
6/7/2019 3:11:32 PM 13286.7 13117.9
6/7/2019 3:11:33 PM 13382.4 13213.6
6/7/2019 3:11:34 PM 14130.2 13961.4
6/7/2019 3:11:35 PM 14209.3 14040.5
6/7/2019 3:11:36 PM 14244.7 14075.9
6/7/2019 3:11:37 PM 14264.4 14095.6
6/7/2019 3:11:38 PM 14270.7 14101.9
6/7/2019 3:11:39 PM 14281.8 14113.0
6/7/2019 3:11:40 PM 14283.8 14115.0
6/7/2019 3:11:41 PM 14277.9 14109.1
6/7/2019 3:11:42 PM 14264.9 14096.1
6/7/2019 3:11:43 PM 14245.8 14077.0
6/7/2019 3:11:44 PM 14218.8 14050.0
6/7/2019 3:11:45 PM 14192.3 14023.5
6/7/2019 3:11:46 PM 14156.8 13988.0
6/7/2019 3:11:47 PM 14122.5 13953.7
6/7/2019 3:11:48 PM 14080.1 13911.3
6/7/2019 3:11:49 PM 14040.3 13871.5
6/7/2019 3:11:50 PM 13991.0 13822.2
6/7/2019 3:11:51 PM 13217.4 13048.6
6/7/2019 3:11:52 PM 13088.2 12919.4
6/7/2019 3:11:53 PM 12930.6 12761.8
6/7/2019 3:11:54 PM 12797.1 12628.3
6/7/2019 3:11:55 PM 12749.4 12580.6
6/7/2019 3:11:56 PM 12663.8 12495.0
6/7/2019 3:11:57 PM 12598.5 12429.7
6/7/2019 3:11:58 PM 12520.1 12351.3
6/7/2019 3:11:59 PM 12442.8 12274.0
6/7/2019 3:12:00 PM 12355.4 12186.6
6/7/2019 3:12:01 PM 11644.9 11476.1
6/7/2019 3:12:02 PM 11458.7 11289.9
6/7/2019 3:12:03 PM 11257.6 11088.8
6/7/2019 3:12:04 PM 11143.8 10975.0
6/7/2019 3:12:05 PM 11059.8 10891.0
6/7/2019 3:12:06 PM 10971.2 10802.4
6/7/2019 3:12:07 PM 10891.4 10722.6
6/7/2019 3:12:08 PM 10817.1 10648.3
6/7/2019 3:12:09 PM 10722.4 10553.6
6/7/2019 3:12:10 PM 10644.5 10475.7
6/7/2019 3:12:11 PM 10005.6 9836.8
6/7/2019 3:12:12 PM 9881.4 9712.6
6/7/2019 3:12:13 PM 9680.0 9511.2
6/7/2019 3:12:14 PM 9551.3 9382.5
6/7/2019 3:12:15 PM 9484.5 9315.7
6/7/2019 3:12:16 PM 9405.0 9236.2
6/7/2019 3:12:17 PM 9322.9 9154.1
6/7/2019 3:12:18 PM 9258.9 9090.1
6/7/2019 3:12:19 PM 9187.4 9018.6
6/7/2019 3:12:20 PM 9121.6 8952.8
6/7/2019 3:12:21 PM 9046.3 8877.5
6/7/2019 3:12:22 PM 8424.2 8255.4
6/7/2019 3:12:23 PM 8281.4 8112.6
Page 337 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:12:24 PM 8146.9 7978.1
6/7/2019 3:12:25 PM 8100.0 7931.2
6/7/2019 3:12:26 PM 8022.8 7854.0
6/7/2019 3:12:27 PM 7966.0 7797.2
6/7/2019 3:12:28 PM 7900.1 7731.3
6/7/2019 3:12:29 PM 7840.4 7671.6
6/7/2019 3:12:30 PM 7782.7 7613.9
6/7/2019 3:12:31 PM 7733.8 7565.0
6/7/2019 3:12:32 PM 7216.0 7047.2
6/7/2019 3:12:33 PM 7107.0 6938.2
6/7/2019 3:12:34 PM 6986.2 6817.4
6/7/2019 3:12:35 PM 6930.1 6761.3
6/7/2019 3:12:36 PM 6860.8 6692.0
6/7/2019 3:12:37 PM 6804.4 6635.6
6/7/2019 3:12:38 PM 6752.7 6583.9
6/7/2019 3:12:39 PM 6708.3 6539.5
6/7/2019 3:12:40 PM 6657.1 6488.3
6/7/2019 3:12:41 PM 6612.6 6443.8
6/7/2019 3:12:42 PM 6163.6 5994.8
6/7/2019 3:12:43 PM 6000.6 5831.8
6/7/2019 3:12:44 PM 6021.4 5852.6
6/7/2019 3:12:45 PM 5951.7 5782.9
6/7/2019 3:12:46 PM 5926.0 5757.2
6/7/2019 3:12:47 PM 5864.5 5695.7
6/7/2019 3:12:48 PM 5810.4 5641.6
6/7/2019 3:12:49 PM 5759.8 5591.0
6/7/2019 3:12:50 PM 5722.3 5553.5
6/7/2019 3:12:51 PM 5679.8 5511.0
6/7/2019 3:12:52 PM 5641.0 5472.2
6/7/2019 3:12:53 PM 5268.9 5100.1
6/7/2019 3:12:54 PM 5188.8 5020.0
6/7/2019 3:12:55 PM 5096.5 4927.7
6/7/2019 3:12:56 PM 5076.8 4908.0
6/7/2019 3:12:57 PM 5042.9 4874.1
6/7/2019 3:12:58 PM 5011.9 4843.1
6/7/2019 3:12:59 PM 4967.9 4799.1
6/7/2019 3:13:00 PM 4932.9 4764.1
6/7/2019 3:13:01 PM 4893.0 4724.2
6/7/2019 3:13:02 PM 4858.7 4689.9
6/7/2019 3:13:03 PM 4551.9 4383.1
6/7/2019 3:13:04 PM 4489.4 4320.6
6/7/2019 3:13:05 PM 4437.4 4268.6
6/7/2019 3:13:06 PM 4417.8 4249.0
6/7/2019 3:13:07 PM 4378.6 4209.8
6/7/2019 3:13:08 PM 4339.1 4170.3
6/7/2019 3:13:09 PM 4307.1 4138.3
6/7/2019 3:13:10 PM 4271.4 4102.6
6/7/2019 3:13:11 PM 4243.4 4074.6
6/7/2019 3:13:12 PM 4213.8 4045.0
6/7/2019 3:13:13 PM 3962.5 3793.7
6/7/2019 3:13:14 PM 3902.3 3733.5
6/7/2019 3:13:15 PM 3856.4 3687.6
6/7/2019 3:13:16 PM 3818.1 3649.3
6/7/2019 3:13:17 PM 3777.0 3608.2
6/7/2019 3:13:18 PM 3740.1 3571.3
6/7/2019 3:13:19 PM 3716.6 3547.8
6/7/2019 3:13:20 PM 3688.9 3520.1
6/7/2019 3:13:21 PM 3665.3 3496.5
6/7/2019 3:13:22 PM 3638.7 3469.9
6/7/2019 3:13:23 PM 3616.6 3447.8
6/7/2019 3:13:24 PM 3409.0 3240.2
6/7/2019 3:13:25 PM 3368.1 3199.3
6/7/2019 3:13:26 PM 3320.6 3151.8
6/7/2019 3:13:27 PM 3281.6 3112.8
6/7/2019 3:13:28 PM 3260.1 3091.3
6/7/2019 3:13:29 PM 3230.3 3061.5
6/7/2019 3:13:30 PM 3208.2 3039.4
6/7/2019 3:13:31 PM 3183.8 3015.0
6/7/2019 3:13:32 PM 3164.8 2996.0
6/7/2019 3:13:33 PM 3144.0 2975.2
6/7/2019 3:13:34 PM 3125.0 2956.2
6/7/2019 3:13:35 PM 2948.9 2780.1
6/7/2019 3:13:36 PM 2907.7 2738.9
6/7/2019 3:13:37 PM 2865.8 2697.0
6/7/2019 3:13:38 PM 2839.8 2671.0
6/7/2019 3:13:39 PM 2819.5 2650.7
6/7/2019 3:13:40 PM 2797.5 2628.7
6/7/2019 3:13:41 PM 2778.7 2609.9
6/7/2019 3:13:42 PM 2762.6 2593.8
6/7/2019 3:13:43 PM 2745.1 2576.3
6/7/2019 3:13:44 PM 2729.9 2561.1
6/7/2019 3:13:45 PM 2712.6 2543.8
6/7/2019 3:13:46 PM 2556.8 2388.0
6/7/2019 3:13:47 PM 2522.7 2353.9
6/7/2019 3:13:48 PM 2493.4 2324.6
6/7/2019 3:13:49 PM 2469.5 2300.7
6/7/2019 3:13:50 PM 2455.6 2286.8
6/7/2019 3:13:51 PM 2438.3 2269.5
6/7/2019 3:13:52 PM 2423.7 2254.9
6/7/2019 3:13:53 PM 2411.0 2242.2
6/7/2019 3:13:54 PM 2397.2 2228.4
6/7/2019 3:13:55 PM 2384.7 2215.9
Page 338 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:13:56 PM 2370.7 2201.9
6/7/2019 3:13:57 PM 2358.2 2189.4
6/7/2019 3:13:58 PM 2344.5 2175.7
6/7/2019 3:13:59 PM 2207.7 2038.9
6/7/2019 3:14:00 PM 2178.7 2009.9
6/7/2019 3:14:01 PM 2160.3 1991.5
6/7/2019 3:14:02 PM 2151.6 1982.8
6/7/2019 3:14:03 PM 2132.7 1963.9
6/7/2019 3:14:04 PM 2116.8 1948.0
6/7/2019 3:14:05 PM 2107.3 1938.5
6/7/2019 3:14:06 PM 2094.9 1926.1
6/7/2019 3:14:07 PM 2084.8 1916.0
6/7/2019 3:14:08 PM 2074.2 1905.4
6/7/2019 3:14:09 PM 2063.8 1895.0
6/7/2019 3:14:10 PM 2054.0 1885.2
6/7/2019 3:14:11 PM 2043.0 1874.2
6/7/2019 3:14:12 PM 1930.8 1762.0
6/7/2019 3:14:13 PM 1909.4 1740.6
6/7/2019 3:14:14 PM 1893.7 1724.9
6/7/2019 3:14:15 PM 1874.3 1705.5
6/7/2019 3:14:16 PM 1866.9 1698.1
6/7/2019 3:14:17 PM 1856.6 1687.8
6/7/2019 3:14:18 PM 1848.9 1680.1
6/7/2019 3:14:19 PM 1840.8 1672.0
6/7/2019 3:14:20 PM 1834.2 1665.4
6/7/2019 3:14:21 PM 1825.4 1656.6
6/7/2019 3:14:22 PM 1817.7 1648.9
6/7/2019 3:14:23 PM 1809.3 1640.5
6/7/2019 3:14:24 PM 1802.6 1633.8
6/7/2019 3:14:25 PM 1794.3 1625.5
6/7/2019 3:14:26 PM 1787.0 1618.2
6/7/2019 3:14:27 PM 1687.0 1518.2
6/7/2019 3:14:28 PM 1676.7 1507.9
6/7/2019 3:14:29 PM 1659.1 1490.3
6/7/2019 3:14:30 PM 1647.3 1478.5
6/7/2019 3:14:31 PM 1639.2 1470.4
6/7/2019 3:14:32 PM 1629.2 1460.4
6/7/2019 3:14:33 PM 1621.8 1453.0
6/7/2019 3:14:34 PM 1613.7 1444.9
6/7/2019 3:14:35 PM 1606.9 1438.1
6/7/2019 3:14:36 PM 1598.9 1430.1
6/7/2019 3:14:37 PM 1593.0 1424.2
6/7/2019 3:14:38 PM 1586.1 1417.3
6/7/2019 3:14:39 PM 1580.4 1411.6
6/7/2019 3:14:40 PM 1573.4 1404.6
6/7/2019 3:14:41 PM 1567.4 1398.6
6/7/2019 3:14:42 PM 1560.7 1391.9
6/7/2019 3:14:43 PM 1468.7 1299.9
6/7/2019 3:14:44 PM 1461.8 1293.0
6/7/2019 3:14:45 PM 1451.8 1283.0
6/7/2019 3:14:46 PM 1447.8 1279.0
6/7/2019 3:14:47 PM 1439.5 1270.7
6/7/2019 3:14:48 PM 1431.5 1262.7
6/7/2019 3:14:49 PM 1425.5 1256.7
6/7/2019 3:14:50 PM 1419.1 1250.3
6/7/2019 3:14:51 PM 1413.2 1244.4
6/7/2019 3:14:52 PM 1407.9 1239.1
6/7/2019 3:14:53 PM 1401.8 1233.0
6/7/2019 3:14:54 PM 1396.6 1227.8
6/7/2019 3:14:55 PM 1390.8 1222.0
6/7/2019 3:14:56 PM 1385.8 1217.0
6/7/2019 3:14:57 PM 1380.2 1211.4
6/7/2019 3:14:58 PM 1375.3 1206.5
6/7/2019 3:14:59 PM 1300.3 1131.5
6/7/2019 3:15:00 PM 1290.8 1122.0
6/7/2019 3:15:01 PM 1280.0 1111.2
6/7/2019 3:15:02 PM 1274.8 1106.0
6/7/2019 3:15:03 PM 1268.0 1099.2
6/7/2019 3:15:04 PM 1262.6 1093.8
6/7/2019 3:15:05 PM 1256.8 1088.0
6/7/2019 3:15:06 PM 1252.7 1083.9
6/7/2019 3:15:07 PM 1248.3 1079.5
6/7/2019 3:15:08 PM 1244.5 1075.7
6/7/2019 3:15:09 PM 1239.8 1071.0
6/7/2019 3:15:10 PM 1235.0 1066.2
6/7/2019 3:15:11 PM 1230.9 1062.1
6/7/2019 3:15:12 PM 1226.4 1057.6
6/7/2019 3:15:13 PM 1222.7 1053.9
6/7/2019 3:15:14 PM 1218.4 1049.6
6/7/2019 3:15:15 PM 1214.0 1045.2
6/7/2019 3:15:16 PM 1205.2 1036.4
6/7/2019 3:15:17 PM 1197.5 1028.7
6/7/2019 3:15:18 PM 1188.7 1019.9
6/7/2019 3:15:19 PM 1180.9 1012.1
6/7/2019 3:15:20 PM 1172.2 1003.4
6/7/2019 3:15:21 PM 1164.7 995.9
6/7/2019 3:15:22 PM 1156.2 987.4
6/7/2019 3:15:23 PM 1148.9 980.1
6/7/2019 3:15:24 PM 1140.5 971.7
6/7/2019 3:15:25 PM 1133.0 964.2
6/7/2019 3:15:26 PM 1124.3 955.5
6/7/2019 3:15:27 PM 1116.7 947.9
Page 339 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:15:28 PM 1108.3 939.5
6/7/2019 3:15:29 PM 1100.9 932.1
6/7/2019 3:15:30 PM 1092.8 924.0
6/7/2019 3:15:31 PM 1085.0 916.2
6/7/2019 3:15:32 PM 1078.2 909.4
6/7/2019 3:15:33 PM 1070.4 901.6
6/7/2019 3:15:34 PM 1063.7 894.9
6/7/2019 3:15:35 PM 1056.1 887.3
6/7/2019 3:15:36 PM 1049.6 880.8
6/7/2019 3:15:37 PM 1042.5 873.7
6/7/2019 3:15:38 PM 1036.3 867.5
6/7/2019 3:15:39 PM 1029.4 860.6
6/7/2019 3:15:40 PM 1023.5 854.7
6/7/2019 3:15:41 PM 1016.6 847.8
6/7/2019 3:15:42 PM 1010.5 841.7
6/7/2019 3:15:43 PM 1003.8 835.0
6/7/2019 3:15:44 PM 997.9 829.1
6/7/2019 3:15:45 PM 991.0 822.2
6/7/2019 3:15:46 PM 985.1 816.3
6/7/2019 3:15:47 PM 978.5 809.7
6/7/2019 3:15:48 PM 972.9 804.1
6/7/2019 3:15:49 PM 966.5 797.7
6/7/2019 3:15:50 PM 960.7 791.9
6/7/2019 3:15:51 PM 954.3 785.5
6/7/2019 3:15:52 PM 948.0 779.2
6/7/2019 3:15:53 PM 942.6 773.8
6/7/2019 3:15:54 PM 936.5 767.7
6/7/2019 3:15:55 PM 931.2 762.4
6/7/2019 3:15:56 PM 925.1 756.3
6/7/2019 3:15:57 PM 920.0 751.2
6/7/2019 3:15:58 PM 914.3 745.5
6/7/2019 3:15:59 PM 909.2 740.4
6/7/2019 3:16:00 PM 903.5 734.7
6/7/2019 3:16:01 PM 898.5 729.7
6/7/2019 3:16:02 PM 893.0 724.2
6/7/2019 3:16:03 PM 888.2 719.4
6/7/2019 3:16:04 PM 882.8 714.0
6/7/2019 3:16:05 PM 878.1 709.3
6/7/2019 3:16:06 PM 872.7 703.9
6/7/2019 3:16:07 PM 868.0 699.2
6/7/2019 3:16:08 PM 862.8 694.0
6/7/2019 3:16:09 PM 858.3 689.5
6/7/2019 3:16:10 PM 853.3 684.5
6/7/2019 3:16:11 PM 848.9 680.1
6/7/2019 3:16:12 PM 844.0 675.2
6/7/2019 3:16:13 PM 839.1 670.3
6/7/2019 3:16:14 PM 834.8 666.0
6/7/2019 3:16:15 PM 830.0 661.2
6/7/2019 3:16:16 PM 825.8 657.0
6/7/2019 3:16:17 PM 821.2 652.4
6/7/2019 3:16:18 PM 817.1 648.3
6/7/2019 3:16:19 PM 812.7 643.9
6/7/2019 3:16:20 PM 808.8 640.0
6/7/2019 3:16:21 PM 804.4 635.6
6/7/2019 3:16:22 PM 800.5 631.7
6/7/2019 3:16:23 PM 796.1 627.3
6/7/2019 3:16:24 PM 792.2 623.4
6/7/2019 3:16:25 PM 787.9 619.1
6/7/2019 3:16:26 PM 784.1 615.3
6/7/2019 3:16:27 PM 779.9 611.1
6/7/2019 3:16:28 PM 776.2 607.4
6/7/2019 3:16:29 PM 772.0 603.2
6/7/2019 3:16:30 PM 768.4 599.6
6/7/2019 3:16:31 PM 764.2 595.4
6/7/2019 3:16:32 PM 760.5 591.7
6/7/2019 3:16:33 PM 756.4 587.6
6/7/2019 3:16:34 PM 752.5 583.7
6/7/2019 3:16:35 PM 749.0 580.2
6/7/2019 3:16:36 PM 745.0 576.2
6/7/2019 3:16:37 PM 741.6 572.8
6/7/2019 3:16:38 PM 737.7 568.9
6/7/2019 3:16:39 PM 734.3 565.5
6/7/2019 3:16:40 PM 730.5 561.7
6/7/2019 3:16:41 PM 727.2 558.4
6/7/2019 3:16:42 PM 723.4 554.6
6/7/2019 3:16:43 PM 720.2 551.4
6/7/2019 3:16:44 PM 716.6 547.8
6/7/2019 3:16:45 PM 713.5 544.7
6/7/2019 3:16:46 PM 709.9 541.1
6/7/2019 3:16:47 PM 706.7 537.9
6/7/2019 3:16:48 PM 703.2 534.4
6/7/2019 3:16:49 PM 700.3 531.5
6/7/2019 3:16:50 PM 696.9 528.1
6/7/2019 3:16:51 PM 694.1 525.3
6/7/2019 3:16:52 PM 690.9 522.1
6/7/2019 3:16:53 PM 688.1 519.3
6/7/2019 3:16:54 PM 685.8 517.0
6/7/2019 3:16:55 PM 682.1 513.3
6/7/2019 3:16:56 PM 679.4 510.6
6/7/2019 3:16:57 PM 676.5 507.7
6/7/2019 3:16:58 PM 674.0 505.2
6/7/2019 3:16:59 PM 671.2 502.4
Page 340 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:17:00 PM 668.9 500.1
6/7/2019 3:17:01 PM 666.2 497.4
6/7/2019 3:17:02 PM 663.8 495.0
6/7/2019 3:17:03 PM 661.1 492.3
6/7/2019 3:17:04 PM 658.7 489.9
6/7/2019 3:17:05 PM 656.0 487.2
6/7/2019 3:17:06 PM 653.6 484.8
6/7/2019 3:17:07 PM 650.8 482.0
6/7/2019 3:17:08 PM 648.5 479.7
6/7/2019 3:17:09 PM 645.8 477.0
6/7/2019 3:17:10 PM 643.5 474.7
6/7/2019 3:17:11 PM 640.7 471.9
6/7/2019 3:17:12 PM 638.3 469.5
6/7/2019 3:17:13 PM 635.6 466.8
6/7/2019 3:17:14 PM 633.3 464.5
6/7/2019 3:17:15 PM 631.3 462.5
6/7/2019 3:17:16 PM 564.3 395.5
6/7/2019 3:17:17 PM 603.8 435.0
6/7/2019 3:17:18 PM 606.4 437.6
6/7/2019 3:17:19 PM 605.8 437.0
6/7/2019 3:17:20 PM 604.8 436.0
6/7/2019 3:17:21 PM 604.1 435.3
6/7/2019 3:17:22 PM 603.2 434.4
6/7/2019 3:17:23 PM 602.6 433.8
6/7/2019 3:17:24 PM 601.8 433.0
6/7/2019 3:17:25 PM 601.2 432.4
6/7/2019 3:17:26 PM 600.5 431.7
6/7/2019 3:17:27 PM 600.0 431.2
6/7/2019 3:17:28 PM 599.5 430.7
6/7/2019 3:17:29 PM 599.1 430.3
6/7/2019 3:17:30 PM 598.7 429.9
6/7/2019 3:17:31 PM 598.4 429.6
6/7/2019 3:17:32 PM 597.8 429.0
6/7/2019 3:17:33 PM 597.3 428.5
6/7/2019 3:17:34 PM 596.9 428.1
6/7/2019 3:17:35 PM 596.7 427.9
6/7/2019 3:17:36 PM 596.6 427.8
6/7/2019 3:17:37 PM 596.7 427.9
6/7/2019 3:17:38 PM 597.0 428.2
6/7/2019 3:17:39 PM 597.4 428.6
6/7/2019 3:17:40 PM 598.2 429.4
6/7/2019 3:17:41 PM 598.8 430.0
6/7/2019 3:17:42 PM 600.0 431.2
6/7/2019 3:17:43 PM 601.2 432.4
6/7/2019 3:17:44 PM 602.4 433.6
6/7/2019 3:17:45 PM 603.9 435.1
6/7/2019 3:17:46 PM 604.9 436.1
6/7/2019 3:17:47 PM 607.0 438.2
6/7/2019 3:17:48 PM 608.6 439.8
6/7/2019 3:17:49 PM 610.4 441.6
6/7/2019 3:17:50 PM 612.0 443.2
6/7/2019 3:17:51 PM 613.9 445.1
6/7/2019 3:17:52 PM 615.4 446.6
6/7/2019 3:17:53 PM 617.6 448.8
6/7/2019 3:17:54 PM 619.1 450.3
6/7/2019 3:17:55 PM 620.7 451.9
6/7/2019 3:17:56 PM 622.5 453.7
6/7/2019 3:17:57 PM 624.1 455.3
6/7/2019 3:17:58 PM 625.7 456.9
6/7/2019 3:17:59 PM 627.1 458.3
6/7/2019 3:18:00 PM 628.6 459.8
6/7/2019 3:18:01 PM 629.8 461.0
6/7/2019 3:18:02 PM 631.0 462.2
6/7/2019 3:18:03 PM 632.3 463.5
6/7/2019 3:18:04 PM 633.0 464.2
6/7/2019 3:18:05 PM 633.9 465.1
6/7/2019 3:18:06 PM 634.4 465.6
6/7/2019 3:18:07 PM 634.8 466.0
6/7/2019 3:18:08 PM 635.3 466.5
6/7/2019 3:18:09 PM 635.4 466.6
6/7/2019 3:18:10 PM 635.5 466.7
6/7/2019 3:18:11 PM 635.5 466.7
6/7/2019 3:18:12 PM 635.3 466.5
6/7/2019 3:18:13 PM 635.0 466.2
6/7/2019 3:18:14 PM 634.6 465.8
6/7/2019 3:18:15 PM 633.8 465.0
6/7/2019 3:18:16 PM 633.3 464.5
6/7/2019 3:18:17 PM 632.4 463.6
6/7/2019 3:18:18 PM 631.5 462.7
6/7/2019 3:18:19 PM 630.4 461.6
6/7/2019 3:18:20 PM 629.3 460.5
6/7/2019 3:18:21 PM 628.0 459.2
6/7/2019 3:18:22 PM 626.7 457.9
6/7/2019 3:18:23 PM 625.3 456.5
6/7/2019 3:18:24 PM 623.9 455.1
6/7/2019 3:18:25 PM 622.2 453.4
6/7/2019 3:18:26 PM 620.7 451.9
6/7/2019 3:18:27 PM 618.9 450.1
6/7/2019 3:18:28 PM 617.3 448.5
6/7/2019 3:18:29 PM 615.5 446.7
6/7/2019 3:18:30 PM 613.8 445.0
6/7/2019 3:18:31 PM 612.0 443.2
Page 341 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:18:32 PM 610.0 441.2
6/7/2019 3:18:33 PM 608.3 439.5
6/7/2019 3:18:34 PM 606.3 437.5
6/7/2019 3:18:35 PM 604.5 435.7
6/7/2019 3:18:36 PM 602.4 433.6
6/7/2019 3:18:37 PM 600.6 431.8
6/7/2019 3:18:38 PM 598.6 429.8
6/7/2019 3:18:39 PM 596.8 428.0
6/7/2019 3:18:40 PM 594.7 425.9
6/7/2019 3:18:41 PM 592.8 424.0
6/7/2019 3:18:42 PM 590.7 421.9
6/7/2019 3:18:43 PM 588.8 420.0
6/7/2019 3:18:44 PM 586.7 417.9
6/7/2019 3:18:45 PM 584.8 416.0
6/7/2019 3:18:46 PM 582.7 413.9
6/7/2019 3:18:47 PM 580.9 412.1
6/7/2019 3:18:48 PM 578.8 410.0
6/7/2019 3:18:49 PM 576.9 408.1
6/7/2019 3:18:50 PM 574.8 406.0
6/7/2019 3:18:51 PM 573.0 404.2
6/7/2019 3:18:52 PM 570.9 402.1
6/7/2019 3:18:53 PM 568.8 400.0
6/7/2019 3:18:54 PM 567.0 398.2
6/7/2019 3:18:55 PM 564.9 396.1
6/7/2019 3:18:56 PM 563.1 394.3
6/7/2019 3:18:57 PM 561.0 392.2
6/7/2019 3:18:58 PM 559.2 390.4
6/7/2019 3:18:59 PM 557.1 388.3
6/7/2019 3:19:00 PM 555.3 386.5
6/7/2019 3:19:01 PM 553.2 384.4
6/7/2019 3:19:02 PM 551.4 382.6
6/7/2019 3:19:03 PM 549.3 380.5
6/7/2019 3:19:04 PM 547.5 378.7
6/7/2019 3:19:05 PM 545.4 376.6
6/7/2019 3:19:06 PM 543.6 374.8
6/7/2019 3:19:07 PM 541.5 372.7
6/7/2019 3:19:08 PM 539.7 370.9
6/7/2019 3:19:09 PM 537.6 368.8
6/7/2019 3:19:10 PM 535.9 367.1
6/7/2019 3:19:11 PM 533.8 365.0
6/7/2019 3:19:12 PM 531.8 363.0
6/7/2019 3:19:13 PM 530.1 361.3
6/7/2019 3:19:14 PM 528.0 359.2
6/7/2019 3:19:15 PM 526.3 357.5
6/7/2019 3:19:16 PM 524.4 355.6
6/7/2019 3:19:17 PM 522.7 353.9
6/7/2019 3:19:18 PM 520.7 351.9
6/7/2019 3:19:19 PM 519.0 350.2
6/7/2019 3:19:20 PM 517.1 348.3
6/7/2019 3:19:21 PM 515.4 346.6
6/7/2019 3:19:22 PM 513.4 344.6
6/7/2019 3:19:23 PM 511.7 342.9
6/7/2019 3:19:24 PM 509.8 341.0
6/7/2019 3:19:25 PM 508.2 339.4
6/7/2019 3:19:26 PM 506.3 337.5
6/7/2019 3:19:27 PM 504.6 335.8
6/7/2019 3:19:28 PM 502.7 333.9
6/7/2019 3:19:29 PM 501.0 332.2
6/7/2019 3:19:30 PM 499.1 330.3
6/7/2019 3:19:31 PM 497.4 328.6
6/7/2019 3:19:32 PM 495.6 326.8
6/7/2019 3:19:33 PM 493.7 324.9
6/7/2019 3:19:34 PM 492.1 323.3
6/7/2019 3:19:35 PM 490.2 321.4
6/7/2019 3:19:36 PM 488.6 319.8
6/7/2019 3:19:37 PM 486.8 318.0
6/7/2019 3:19:38 PM 485.2 316.4
6/7/2019 3:19:39 PM 483.4 314.6
6/7/2019 3:19:40 PM 481.8 313.0
6/7/2019 3:19:41 PM 480.1 311.3
6/7/2019 3:19:42 PM 478.6 309.8
6/7/2019 3:19:43 PM 476.9 308.1
6/7/2019 3:19:44 PM 475.4 306.6
6/7/2019 3:19:45 PM 473.7 304.9
6/7/2019 3:19:46 PM 472.2 303.4
6/7/2019 3:19:47 PM 470.5 301.7
6/7/2019 3:19:48 PM 469.1 300.3
6/7/2019 3:19:49 PM 467.5 298.7
6/7/2019 3:19:50 PM 466.0 297.2
6/7/2019 3:19:51 PM 464.4 295.6
6/7/2019 3:19:52 PM 463.0 294.2
6/7/2019 3:19:53 PM 461.4 292.6
6/7/2019 3:19:54 PM 459.8 291.0
6/7/2019 3:19:55 PM 458.4 289.6
6/7/2019 3:19:56 PM 456.9 288.1
6/7/2019 3:19:57 PM 455.5 286.7
6/7/2019 3:19:58 PM 454.0 285.2
6/7/2019 3:19:59 PM 452.7 283.9
6/7/2019 3:20:00 PM 451.2 282.4
6/7/2019 3:20:01 PM 450.0 281.2
6/7/2019 3:20:02 PM 448.6 279.8
6/7/2019 3:20:03 PM 447.3 278.5
Page 342 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:20:04 PM 446.0 277.2
6/7/2019 3:20:05 PM 444.8 276.0
6/7/2019 3:20:06 PM 443.4 274.6
6/7/2019 3:20:07 PM 442.2 273.4
6/7/2019 3:20:08 PM 440.8 272.0
6/7/2019 3:20:09 PM 439.7 270.9
6/7/2019 3:20:10 PM 438.3 269.5
6/7/2019 3:20:11 PM 437.2 268.4
6/7/2019 3:20:12 PM 435.8 267.0
6/7/2019 3:20:13 PM 434.5 265.7
6/7/2019 3:20:14 PM 433.4 264.6
6/7/2019 3:20:15 PM 432.1 263.3
6/7/2019 3:20:16 PM 430.9 262.1
6/7/2019 3:20:17 PM 429.7 260.9
6/7/2019 3:20:18 PM 428.6 259.8
6/7/2019 3:20:19 PM 427.3 258.5
6/7/2019 3:20:20 PM 426.3 257.5
6/7/2019 3:20:21 PM 425.0 256.2
6/7/2019 3:20:22 PM 424.0 255.2
6/7/2019 3:20:23 PM 422.9 254.1
6/7/2019 3:20:24 PM 421.9 253.1
6/7/2019 3:20:25 PM 420.7 251.9
6/7/2019 3:20:26 PM 419.7 250.9
6/7/2019 3:20:27 PM 418.6 249.8
6/7/2019 3:20:28 PM 417.6 248.8
6/7/2019 3:20:29 PM 416.5 247.7
6/7/2019 3:20:30 PM 415.5 246.7
6/7/2019 3:20:31 PM 414.4 245.6
6/7/2019 3:20:32 PM 413.5 244.7
6/7/2019 3:20:33 PM 412.4 243.6
6/7/2019 3:20:34 PM 411.2 242.4
6/7/2019 3:20:35 PM 410.3 241.5
6/7/2019 3:20:36 PM 409.2 240.4
6/7/2019 3:20:37 PM 408.2 239.4
6/7/2019 3:20:38 PM 407.1 238.3
6/7/2019 3:20:39 PM 406.2 237.4
6/7/2019 3:20:40 PM 405.1 236.3
6/7/2019 3:20:41 PM 404.2 235.4
6/7/2019 3:20:42 PM 403.1 234.3
6/7/2019 3:20:43 PM 402.2 233.4
6/7/2019 3:20:44 PM 401.2 232.4
6/7/2019 3:20:45 PM 400.3 231.5
6/7/2019 3:20:46 PM 399.2 230.4
6/7/2019 3:20:47 PM 398.3 229.5
6/7/2019 3:20:48 PM 397.3 228.5
6/7/2019 3:20:49 PM 396.4 227.6
6/7/2019 3:20:50 PM 395.4 226.6
6/7/2019 3:20:51 PM 394.5 225.7
6/7/2019 3:20:52 PM 393.5 224.7
6/7/2019 3:20:53 PM 392.6 223.8
6/7/2019 3:20:54 PM 391.6 222.8
6/7/2019 3:20:55 PM 390.6 221.8
6/7/2019 3:20:56 PM 389.8 221.0
6/7/2019 3:20:57 PM 388.8 220.0
6/7/2019 3:20:58 PM 387.9 219.1
6/7/2019 3:20:59 PM 386.9 218.1
6/7/2019 3:21:00 PM 386.1 217.3
6/7/2019 3:21:01 PM 385.1 216.3
6/7/2019 3:21:02 PM 384.2 215.4
6/7/2019 3:21:03 PM 383.3 214.5
6/7/2019 3:21:04 PM 382.4 213.6
6/7/2019 3:21:05 PM 381.5 212.7
6/7/2019 3:21:06 PM 380.6 211.8
6/7/2019 3:21:07 PM 379.7 210.9
6/7/2019 3:21:08 PM 378.8 210.0
6/7/2019 3:21:09 PM 377.8 209.0
6/7/2019 3:21:10 PM 377.0 208.2
6/7/2019 3:21:11 PM 376.0 207.2
6/7/2019 3:21:12 PM 375.2 206.4
6/7/2019 3:21:13 PM 374.2 205.4
6/7/2019 3:21:14 PM 373.3 204.5
6/7/2019 3:21:15 PM 372.5 203.7
6/7/2019 3:21:16 PM 371.6 202.8
6/7/2019 3:21:17 PM 370.8 202.0
6/7/2019 3:21:18 PM 369.9 201.1
6/7/2019 3:21:19 PM 369.1 200.3
6/7/2019 3:21:20 PM 368.2 199.4
6/7/2019 3:21:21 PM 367.5 198.7
6/7/2019 3:21:22 PM 366.6 197.8
6/7/2019 3:21:23 PM 365.9 197.1
6/7/2019 3:21:24 PM 365.0 196.2
6/7/2019 3:21:25 PM 364.3 195.5
6/7/2019 3:21:26 PM 363.5 194.7
6/7/2019 3:21:27 PM 362.7 193.9
6/7/2019 3:21:28 PM 361.9 193.1
6/7/2019 3:21:29 PM 361.2 192.4
6/7/2019 3:21:30 PM 360.4 191.6
6/7/2019 3:21:31 PM 359.7 190.9
6/7/2019 3:21:32 PM 358.9 190.1
6/7/2019 3:21:33 PM 358.1 189.3
6/7/2019 3:21:34 PM 357.3 188.5
6/7/2019 3:21:35 PM 356.5 187.7
Page 343 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:21:36 PM 355.8 187.0
6/7/2019 3:21:37 PM 355.0 186.2
6/7/2019 3:21:38 PM 354.3 185.5
6/7/2019 3:21:39 PM 353.5 184.7
6/7/2019 3:21:40 PM 352.8 184.0
6/7/2019 3:21:41 PM 352.1 183.3
6/7/2019 3:21:42 PM 351.4 182.6
6/7/2019 3:21:43 PM 350.6 181.8
6/7/2019 3:21:44 PM 349.9 181.1
6/7/2019 3:21:45 PM 349.2 180.4
6/7/2019 3:21:46 PM 348.5 179.7
6/7/2019 3:21:47 PM 347.8 179.0
6/7/2019 3:21:48 PM 347.2 178.4
6/7/2019 3:21:49 PM 346.4 177.6
6/7/2019 3:21:50 PM 345.8 177.0
6/7/2019 3:21:51 PM 345.1 176.3
6/7/2019 3:21:52 PM 344.5 175.7
6/7/2019 3:21:53 PM 343.8 175.0
6/7/2019 3:21:54 PM 343.2 174.4
6/7/2019 3:21:55 PM 342.5 173.7
6/7/2019 3:21:56 PM 341.8 173.0
6/7/2019 3:21:57 PM 341.3 172.5
6/7/2019 3:21:58 PM 340.6 171.8
6/7/2019 3:21:59 PM 340.1 171.3
6/7/2019 3:22:00 PM 339.4 170.6
6/7/2019 3:22:01 PM 338.9 170.1
6/7/2019 3:22:02 PM 338.3 169.5
6/7/2019 3:22:03 PM 337.8 169.0
6/7/2019 3:22:04 PM 337.2 168.4
6/7/2019 3:22:05 PM 336.7 167.9
6/7/2019 3:22:06 PM 336.1 167.3
6/7/2019 3:22:07 PM 335.6 166.8
6/7/2019 3:22:08 PM 335.1 166.3
6/7/2019 3:22:09 PM 334.6 165.8
6/7/2019 3:22:10 PM 334.1 165.3
6/7/2019 3:22:11 PM 333.6 164.8
6/7/2019 3:22:12 PM 333.1 164.3
6/7/2019 3:22:13 PM 332.7 163.9
6/7/2019 3:22:14 PM 332.2 163.4
6/7/2019 3:22:15 PM 331.7 162.9
6/7/2019 3:22:16 PM 331.3 162.5
6/7/2019 3:22:17 PM 330.8 162.0
6/7/2019 3:22:18 PM 330.4 161.6
6/7/2019 3:22:19 PM 329.9 161.1
6/7/2019 3:22:20 PM 329.5 160.7
6/7/2019 3:22:21 PM 329.0 160.2
6/7/2019 3:22:22 PM 328.6 159.8
6/7/2019 3:22:23 PM 328.2 159.4
6/7/2019 3:22:24 PM 327.8 159.0
6/7/2019 3:22:25 PM 327.3 158.5
6/7/2019 3:22:26 PM 326.9 158.1
6/7/2019 3:22:27 PM 326.5 157.7
6/7/2019 3:22:28 PM 326.1 157.3
6/7/2019 3:22:29 PM 325.6 156.8
6/7/2019 3:22:30 PM 325.2 156.4
6/7/2019 3:22:31 PM 324.8 156.0
6/7/2019 3:22:32 PM 324.4 155.6
6/7/2019 3:22:33 PM 324.0 155.2
6/7/2019 3:22:34 PM 323.6 154.8
6/7/2019 3:22:35 PM 323.1 154.3
6/7/2019 3:22:36 PM 322.7 153.9
6/7/2019 3:22:37 PM 322.3 153.5
6/7/2019 3:22:38 PM 321.9 153.1
6/7/2019 3:22:39 PM 321.5 152.7
6/7/2019 3:22:40 PM 321.1 152.3
6/7/2019 3:22:41 PM 320.7 151.9
6/7/2019 3:22:42 PM 320.3 151.5
6/7/2019 3:22:43 PM 319.9 151.1
6/7/2019 3:22:44 PM 319.5 150.7
6/7/2019 3:22:45 PM 319.1 150.3
6/7/2019 3:22:46 PM 318.7 149.9
6/7/2019 3:22:47 PM 318.3 149.5
6/7/2019 3:22:48 PM 317.9 149.1
6/7/2019 3:22:49 PM 317.5 148.7
6/7/2019 3:22:50 PM 317.1 148.3
6/7/2019 3:22:51 PM 316.7 147.9
6/7/2019 3:22:52 PM 316.3 147.5
6/7/2019 3:22:53 PM 316.0 147.2
6/7/2019 3:22:54 PM 315.6 146.8
6/7/2019 3:22:55 PM 315.3 146.5
6/7/2019 3:22:56 PM 314.9 146.1
6/7/2019 3:22:57 PM 314.5 145.7
6/7/2019 3:22:58 PM 314.2 145.4
6/7/2019 3:22:59 PM 313.8 145.0
6/7/2019 3:23:00 PM 313.5 144.7
6/7/2019 3:23:01 PM 313.2 144.4
6/7/2019 3:23:02 PM 312.9 144.1
6/7/2019 3:23:03 PM 312.5 143.7
6/7/2019 3:23:04 PM 312.2 143.4
6/7/2019 3:23:05 PM 311.8 143.0
6/7/2019 3:23:06 PM 311.5 142.7
6/7/2019 3:23:07 PM 311.1 142.3
Page 344 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:23:08 PM 310.7 141.9
6/7/2019 3:23:09 PM 310.4 141.6
6/7/2019 3:23:10 PM 310.1 141.3
6/7/2019 3:23:11 PM 309.7 140.9
6/7/2019 3:23:12 PM 309.4 140.6
6/7/2019 3:23:13 PM 309.0 140.2
6/7/2019 3:23:14 PM 308.7 139.9
6/7/2019 3:23:15 PM 308.4 139.6
6/7/2019 3:23:16 PM 308.0 139.2
6/7/2019 3:23:17 PM 307.7 138.9
6/7/2019 3:23:18 PM 307.4 138.6
6/7/2019 3:23:19 PM 307.1 138.3
6/7/2019 3:23:20 PM 306.8 138.0
6/7/2019 3:23:21 PM 306.5 137.7
6/7/2019 3:23:22 PM 306.2 137.4
6/7/2019 3:23:23 PM 305.9 137.1
6/7/2019 3:23:24 PM 305.6 136.8
6/7/2019 3:23:25 PM 305.3 136.5
6/7/2019 3:23:26 PM 305.0 136.2
6/7/2019 3:23:27 PM 304.7 135.9
6/7/2019 3:23:28 PM 304.4 135.6
6/7/2019 3:23:29 PM 304.2 135.4
6/7/2019 3:23:30 PM 303.9 135.1
6/7/2019 3:23:31 PM 303.6 134.8
6/7/2019 3:23:32 PM 303.3 134.5
6/7/2019 3:23:33 PM 303.0 134.2
6/7/2019 3:23:34 PM 302.7 133.9
6/7/2019 3:23:35 PM 302.4 133.6
6/7/2019 3:23:36 PM 302.1 133.3
6/7/2019 3:23:37 PM 301.8 133.0
6/7/2019 3:23:38 PM 301.5 132.7
6/7/2019 3:23:39 PM 301.1 132.3
6/7/2019 3:23:40 PM 300.8 132.0
6/7/2019 3:23:41 PM 300.4 131.6
6/7/2019 3:23:42 PM 300.1 131.3
6/7/2019 3:23:43 PM 299.7 130.9
6/7/2019 3:23:44 PM 299.4 130.6
6/7/2019 3:23:45 PM 299.1 130.3
6/7/2019 3:23:46 PM 298.7 129.9
6/7/2019 3:23:47 PM 298.4 129.6
6/7/2019 3:23:48 PM 298.0 129.2
6/7/2019 3:23:49 PM 297.6 128.8
6/7/2019 3:23:50 PM 297.3 128.5
6/7/2019 3:23:51 PM 296.9 128.1
6/7/2019 3:23:52 PM 296.6 127.8
6/7/2019 3:23:53 PM 296.2 127.4
6/7/2019 3:23:54 PM 295.9 127.1
6/7/2019 3:23:55 PM 295.6 126.8
6/7/2019 3:23:56 PM 295.2 126.4
6/7/2019 3:23:57 PM 294.8 126.0
6/7/2019 3:23:58 PM 294.5 125.7
6/7/2019 3:23:59 PM 294.1 125.3
6/7/2019 3:24:00 PM 293.8 125.0
6/7/2019 3:24:01 PM 293.4 124.6
6/7/2019 3:24:02 PM 293.1 124.3
6/7/2019 3:24:03 PM 292.8 124.0
6/7/2019 3:24:04 PM 292.4 123.6
6/7/2019 3:24:05 PM 292.1 123.3
6/7/2019 3:24:06 PM 291.7 122.9
6/7/2019 3:24:07 PM 291.4 122.6
6/7/2019 3:24:08 PM 291.0 122.2
6/7/2019 3:24:09 PM 290.7 121.9
6/7/2019 3:24:10 PM 290.4 121.6
6/7/2019 3:24:11 PM 290.1 121.3
6/7/2019 3:24:12 PM 289.7 120.9
6/7/2019 3:24:13 PM 289.4 120.6
6/7/2019 3:24:14 PM 289.1 120.3
6/7/2019 3:24:15 PM 288.8 120.0
6/7/2019 3:24:16 PM 288.4 119.6
6/7/2019 3:24:17 PM 288.2 119.4
6/7/2019 3:24:18 PM 287.8 119.0
6/7/2019 3:24:19 PM 287.5 118.7
6/7/2019 3:24:20 PM 287.3 118.5
6/7/2019 3:24:21 PM 287.0 118.2
6/7/2019 3:24:22 PM 286.7 117.9
6/7/2019 3:24:23 PM 286.4 117.6
6/7/2019 3:24:24 PM 286.2 117.4
6/7/2019 3:24:25 PM 285.9 117.1
6/7/2019 3:24:26 PM 285.7 116.9
6/7/2019 3:24:27 PM 285.5 116.7
6/7/2019 3:24:28 PM 285.2 116.4
6/7/2019 3:24:29 PM 285.0 116.2
6/7/2019 3:24:30 PM 284.8 116.0
6/7/2019 3:24:31 PM 284.6 115.8
6/7/2019 3:24:32 PM 284.4 115.6
6/7/2019 3:24:33 PM 284.2 115.4
6/7/2019 3:24:34 PM 284.0 115.2
6/7/2019 3:24:35 PM 283.7 114.9
6/7/2019 3:24:36 PM 283.6 114.8
6/7/2019 3:24:37 PM 283.3 114.5
6/7/2019 3:24:38 PM 283.1 114.3
6/7/2019 3:24:39 PM 282.9 114.1
Page 345 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:24:40 PM 282.7 113.9
6/7/2019 3:24:41 PM 282.5 113.7
6/7/2019 3:24:42 PM 282.2 113.4
6/7/2019 3:24:43 PM 282.0 113.2
6/7/2019 3:24:44 PM 281.8 113.0
6/7/2019 3:24:45 PM 281.6 112.8
6/7/2019 3:24:46 PM 281.3 112.5
6/7/2019 3:24:47 PM 281.1 112.3
6/7/2019 3:24:48 PM 280.9 112.1
6/7/2019 3:24:49 PM 280.6 111.8
6/7/2019 3:24:50 PM 280.4 111.6
6/7/2019 3:24:51 PM 280.1 111.3
6/7/2019 3:24:52 PM 279.9 111.1
6/7/2019 3:24:53 PM 279.6 110.8
6/7/2019 3:24:54 PM 279.4 110.6
6/7/2019 3:24:55 PM 279.2 110.4
6/7/2019 3:24:56 PM 278.9 110.1
6/7/2019 3:24:57 PM 278.7 109.9
6/7/2019 3:24:58 PM 278.4 109.6
6/7/2019 3:24:59 PM 278.1 109.3
6/7/2019 3:25:00 PM 277.9 109.1
6/7/2019 3:25:01 PM 277.6 108.8
6/7/2019 3:25:02 PM 277.4 108.6
6/7/2019 3:25:03 PM 277.1 108.3
6/7/2019 3:25:04 PM 276.9 108.1
6/7/2019 3:25:05 PM 276.6 107.8
6/7/2019 3:25:06 PM 276.4 107.6
6/7/2019 3:25:07 PM 276.1 107.3
6/7/2019 3:25:08 PM 275.8 107.0
6/7/2019 3:25:09 PM 275.6 106.8
6/7/2019 3:25:10 PM 275.3 106.5
6/7/2019 3:25:11 PM 275.0 106.2
6/7/2019 3:25:12 PM 274.8 106.0
6/7/2019 3:25:13 PM 274.5 105.7
6/7/2019 3:25:14 PM 274.2 105.4
6/7/2019 3:25:15 PM 274.0 105.2
6/7/2019 3:25:16 PM 273.7 104.9
6/7/2019 3:25:17 PM 273.4 104.6
6/7/2019 3:25:18 PM 273.2 104.4
6/7/2019 3:25:19 PM 273.0 104.2
6/7/2019 3:25:20 PM 272.7 103.9
6/7/2019 3:25:21 PM 272.5 103.7
6/7/2019 3:25:22 PM 272.3 103.5
6/7/2019 3:25:23 PM 272.1 103.3
6/7/2019 3:25:24 PM 271.9 103.1
6/7/2019 3:25:25 PM 271.7 102.9
6/7/2019 3:25:26 PM 271.5 102.7
6/7/2019 3:25:27 PM 271.3 102.5
6/7/2019 3:25:28 PM 271.2 102.4
6/7/2019 3:25:29 PM 271.0 102.2
6/7/2019 3:25:30 PM 270.9 102.1
6/7/2019 3:25:31 PM 270.7 101.9
6/7/2019 3:25:32 PM 270.6 101.8
6/7/2019 3:25:33 PM 270.4 101.6
6/7/2019 3:25:34 PM 270.3 101.5
6/7/2019 3:25:35 PM 270.2 101.4
6/7/2019 3:25:36 PM 270.1 101.3
6/7/2019 3:25:37 PM 269.9 101.1
6/7/2019 3:25:38 PM 269.8 101.0
6/7/2019 3:25:39 PM 269.7 100.9
6/7/2019 3:25:40 PM 269.5 100.7
6/7/2019 3:25:41 PM 269.4 100.6
6/7/2019 3:25:42 PM 269.3 100.5
6/7/2019 3:25:43 PM 269.1 100.3
6/7/2019 3:25:44 PM 269.0 100.2
6/7/2019 3:25:45 PM 268.8 100.0
6/7/2019 3:25:46 PM 268.7 99.9
6/7/2019 3:25:47 PM 268.5 99.7
6/7/2019 3:25:48 PM 268.4 99.6
6/7/2019 3:25:49 PM 268.2 99.4
6/7/2019 3:25:50 PM 268.1 99.3
6/7/2019 3:25:51 PM 267.9 99.1
6/7/2019 3:25:52 PM 267.7 98.9
6/7/2019 3:25:53 PM 267.5 98.7
6/7/2019 3:25:54 PM 267.4 98.6
6/7/2019 3:25:55 PM 267.2 98.4
6/7/2019 3:25:56 PM 267.0 98.2
6/7/2019 3:25:57 PM 266.8 98.0
6/7/2019 3:25:58 PM 266.6 97.8
6/7/2019 3:25:59 PM 266.4 97.6
6/7/2019 3:26:00 PM 266.1 97.3
6/7/2019 3:26:01 PM 265.9 97.1
6/7/2019 3:26:02 PM 265.7 96.9
6/7/2019 3:26:03 PM 265.5 96.7
6/7/2019 3:26:04 PM 265.2 96.4
6/7/2019 3:26:05 PM 265.0 96.2
6/7/2019 3:26:06 PM 264.8 96.0
6/7/2019 3:26:07 PM 264.5 95.7
6/7/2019 3:26:08 PM 264.2 95.4
6/7/2019 3:26:09 PM 264.0 95.2
6/7/2019 3:26:10 PM 263.7 94.9
6/7/2019 3:26:11 PM 263.5 94.7
Page 346 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:26:12 PM 263.2 94.4
6/7/2019 3:26:13 PM 263.0 94.2
6/7/2019 3:26:14 PM 262.7 93.9
6/7/2019 3:26:15 PM 262.4 93.6
6/7/2019 3:26:16 PM 262.2 93.4
6/7/2019 3:26:17 PM 261.9 93.1
6/7/2019 3:26:18 PM 261.7 92.9
6/7/2019 3:26:19 PM 261.4 92.6
6/7/2019 3:26:20 PM 261.2 92.4
6/7/2019 3:26:21 PM 260.9 92.1
6/7/2019 3:26:22 PM 260.7 91.9
6/7/2019 3:26:23 PM 260.5 91.7
6/7/2019 3:26:24 PM 260.3 91.5
6/7/2019 3:26:25 PM 260.1 91.3
6/7/2019 3:26:26 PM 259.9 91.1
6/7/2019 3:26:27 PM 259.6 90.8
6/7/2019 3:26:28 PM 259.5 90.7
6/7/2019 3:26:29 PM 259.3 90.5
6/7/2019 3:26:30 PM 259.1 90.3
6/7/2019 3:26:31 PM 258.9 90.1
6/7/2019 3:26:32 PM 258.7 89.9
6/7/2019 3:26:33 PM 258.5 89.7
6/7/2019 3:26:34 PM 258.4 89.6
6/7/2019 3:26:35 PM 258.2 89.4
6/7/2019 3:26:36 PM 258.1 89.3
6/7/2019 3:26:37 PM 257.9 89.1
6/7/2019 3:26:38 PM 257.7 88.9
6/7/2019 3:26:39 PM 257.6 88.8
6/7/2019 3:26:40 PM 257.4 88.6
6/7/2019 3:26:41 PM 257.3 88.5
6/7/2019 3:26:42 PM 257.1 88.3
6/7/2019 3:26:43 PM 257.0 88.2
6/7/2019 3:26:44 PM 256.8 88.0
6/7/2019 3:26:45 PM 256.6 87.8
6/7/2019 3:26:46 PM 256.5 87.7
6/7/2019 3:26:47 PM 256.3 87.5
6/7/2019 3:26:48 PM 256.1 87.3
6/7/2019 3:26:49 PM 256.0 87.2
6/7/2019 3:26:50 PM 255.8 87.0
6/7/2019 3:26:51 PM 255.7 86.9
6/7/2019 3:26:52 PM 255.5 86.7
6/7/2019 3:26:53 PM 255.4 86.6
6/7/2019 3:26:54 PM 255.2 86.4
6/7/2019 3:26:55 PM 255.1 86.3
6/7/2019 3:26:56 PM 254.9 86.1
6/7/2019 3:26:57 PM 254.7 85.9
6/7/2019 3:26:58 PM 254.6 85.8
6/7/2019 3:26:59 PM 254.4 85.6
6/7/2019 3:27:00 PM 254.3 85.5
6/7/2019 3:27:01 PM 254.1 85.3
6/7/2019 3:27:02 PM 254.0 85.2
6/7/2019 3:27:03 PM 253.9 85.1
6/7/2019 3:27:04 PM 253.7 84.9
6/7/2019 3:27:05 PM 253.5 84.7
6/7/2019 3:27:06 PM 253.4 84.6
6/7/2019 3:27:07 PM 253.2 84.4
6/7/2019 3:27:08 PM 253.1 84.3
6/7/2019 3:27:09 PM 252.9 84.1
6/7/2019 3:27:10 PM 252.8 84.0
6/7/2019 3:27:11 PM 252.6 83.8
6/7/2019 3:27:12 PM 252.4 83.6
6/7/2019 3:27:13 PM 252.3 83.5
6/7/2019 3:27:14 PM 252.1 83.3
6/7/2019 3:27:15 PM 251.9 83.1
6/7/2019 3:27:16 PM 251.8 83.0
6/7/2019 3:27:17 PM 251.6 82.8
6/7/2019 3:27:18 PM 251.5 82.7
6/7/2019 3:27:19 PM 251.3 82.5
6/7/2019 3:27:20 PM 251.2 82.4
6/7/2019 3:27:21 PM 251.0 82.2
6/7/2019 3:27:22 PM 250.8 82.0
6/7/2019 3:27:23 PM 250.7 81.9
6/7/2019 3:27:24 PM 250.5 81.7
6/7/2019 3:27:25 PM 250.4 81.6
6/7/2019 3:27:26 PM 250.2 81.4
6/7/2019 3:27:27 PM 250.1 81.3
6/7/2019 3:27:28 PM 249.9 81.1
6/7/2019 3:27:29 PM 249.8 81.0
6/7/2019 3:27:30 PM 249.6 80.8
6/7/2019 3:27:31 PM 249.5 80.7
6/7/2019 3:27:32 PM 249.3 80.5
6/7/2019 3:27:33 PM 249.2 80.4
6/7/2019 3:27:34 PM 249.0 80.2
6/7/2019 3:27:35 PM 248.8 80.0
6/7/2019 3:27:36 PM 248.7 79.9
6/7/2019 3:27:37 PM 248.5 79.7
6/7/2019 3:27:38 PM 248.4 79.6
6/7/2019 3:27:39 PM 248.2 79.4
6/7/2019 3:27:40 PM 248.0 79.2
6/7/2019 3:27:41 PM 247.9 79.1
6/7/2019 3:27:42 PM 247.7 78.9
6/7/2019 3:27:43 PM 247.5 78.7
Page 347 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:27:44 PM 247.4 78.6
6/7/2019 3:27:45 PM 247.2 78.4
6/7/2019 3:27:46 PM 247.0 78.2
6/7/2019 3:27:47 PM 246.8 78.0
6/7/2019 3:27:48 PM 246.7 77.9
6/7/2019 3:27:49 PM 246.5 77.7
6/7/2019 3:27:50 PM 246.3 77.5
6/7/2019 3:27:51 PM 246.1 77.3
6/7/2019 3:27:52 PM 246.0 77.2
6/7/2019 3:27:53 PM 245.8 77.0
6/7/2019 3:27:54 PM 245.6 76.8
6/7/2019 3:27:55 PM 245.5 76.7
6/7/2019 3:27:56 PM 245.3 76.5
6/7/2019 3:27:57 PM 245.2 76.4
6/7/2019 3:27:58 PM 245.0 76.2
6/7/2019 3:27:59 PM 244.9 76.1
6/7/2019 3:28:00 PM 244.7 75.9
6/7/2019 3:28:01 PM 244.6 75.8
6/7/2019 3:28:02 PM 244.5 75.7
6/7/2019 3:28:03 PM 244.3 75.5
6/7/2019 3:28:04 PM 244.2 75.4
6/7/2019 3:28:05 PM 244.1 75.3
6/7/2019 3:28:06 PM 244.0 75.2
6/7/2019 3:28:07 PM 243.8 75.0
6/7/2019 3:28:08 PM 243.7 74.9
6/7/2019 3:28:09 PM 243.6 74.8
6/7/2019 3:28:10 PM 243.5 74.7
6/7/2019 3:28:11 PM 243.4 74.6
6/7/2019 3:28:12 PM 243.3 74.5
6/7/2019 3:28:13 PM 243.2 74.4
6/7/2019 3:28:14 PM 243.1 74.3
6/7/2019 3:28:15 PM 243.0 74.2
6/7/2019 3:28:16 PM 242.9 74.1
6/7/2019 3:28:17 PM 242.8 74.0
6/7/2019 3:28:18 PM 242.7 73.9
6/7/2019 3:28:19 PM 242.6 73.8
6/7/2019 3:28:20 PM 242.5 73.7
6/7/2019 3:28:21 PM 242.4 73.6
6/7/2019 3:28:22 PM 242.3 73.5
6/7/2019 3:28:23 PM 242.2 73.4
6/7/2019 3:28:24 PM 242.1 73.3
6/7/2019 3:28:25 PM 242.0 73.2
6/7/2019 3:28:26 PM 241.9 73.1
6/7/2019 3:28:27 PM 241.8 73.0
6/7/2019 3:28:28 PM 241.8 73.0
6/7/2019 3:28:29 PM 241.7 72.9
6/7/2019 3:28:30 PM 241.6 72.8
6/7/2019 3:28:31 PM 241.5 72.7
6/7/2019 3:28:32 PM 241.4 72.6
6/7/2019 3:28:33 PM 241.3 72.5
6/7/2019 3:28:34 PM 241.2 72.4
6/7/2019 3:28:35 PM 241.0 72.2
6/7/2019 3:28:36 PM 240.9 72.1
6/7/2019 3:28:37 PM 240.8 72.0
6/7/2019 3:28:38 PM 240.7 71.9
6/7/2019 3:28:39 PM 240.6 71.8
6/7/2019 3:28:40 PM 240.4 71.6
6/7/2019 3:28:41 PM 240.3 71.5
6/7/2019 3:28:42 PM 240.2 71.4
6/7/2019 3:28:43 PM 240.0 71.2
6/7/2019 3:28:44 PM 239.9 71.1
6/7/2019 3:28:45 PM 239.7 70.9
6/7/2019 3:28:46 PM 239.6 70.8
6/7/2019 3:28:47 PM 239.5 70.7
6/7/2019 3:28:48 PM 239.3 70.5
6/7/2019 3:28:49 PM 239.2 70.4
6/7/2019 3:28:50 PM 239.0 70.2
6/7/2019 3:28:51 PM 238.9 70.1
6/7/2019 3:28:52 PM 238.7 69.9
6/7/2019 3:28:53 PM 238.6 69.8
6/7/2019 3:28:54 PM 238.4 69.6
6/7/2019 3:28:55 PM 238.3 69.5
6/7/2019 3:28:56 PM 238.1 69.3
6/7/2019 3:28:57 PM 238.0 69.2
6/7/2019 3:28:58 PM 237.8 69.0
6/7/2019 3:28:59 PM 237.6 68.8
6/7/2019 3:29:00 PM 237.4 68.6
6/7/2019 3:29:01 PM 237.3 68.5
6/7/2019 3:29:02 PM 237.1 68.3
6/7/2019 3:29:03 PM 236.9 68.1
6/7/2019 3:29:04 PM 236.8 68.0
6/7/2019 3:29:05 PM 236.6 67.8
6/7/2019 3:29:06 PM 236.4 67.6
6/7/2019 3:29:07 PM 236.2 67.4
6/7/2019 3:29:08 PM 236.1 67.3
6/7/2019 3:29:09 PM 235.9 67.1
6/7/2019 3:29:10 PM 235.7 66.9
6/7/2019 3:29:11 PM 235.5 66.7
6/7/2019 3:29:12 PM 235.3 66.5
6/7/2019 3:29:13 PM 235.1 66.3
6/7/2019 3:29:14 PM 235.0 66.2
6/7/2019 3:29:15 PM 234.8 66.0
Page 348 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:29:16 PM 234.6 65.8
6/7/2019 3:29:17 PM 234.4 65.6
6/7/2019 3:29:18 PM 234.2 65.4
6/7/2019 3:29:19 PM 234.0 65.2
6/7/2019 3:29:20 PM 233.9 65.1
6/7/2019 3:29:21 PM 233.7 64.9
6/7/2019 3:29:22 PM 233.5 64.7
6/7/2019 3:29:23 PM 233.3 64.5
6/7/2019 3:29:24 PM 233.1 64.3
6/7/2019 3:29:25 PM 233.0 64.2
6/7/2019 3:29:26 PM 232.8 64.0
6/7/2019 3:29:27 PM 232.7 63.9
6/7/2019 3:29:28 PM 232.5 63.7
6/7/2019 3:29:29 PM 232.3 63.5
6/7/2019 3:29:30 PM 232.2 63.4
6/7/2019 3:29:31 PM 232.0 63.2
6/7/2019 3:29:32 PM 231.9 63.1
6/7/2019 3:29:33 PM 231.7 62.9
6/7/2019 3:29:34 PM 231.6 62.8
6/7/2019 3:29:35 PM 231.4 62.6
6/7/2019 3:29:36 PM 231.2 62.4
6/7/2019 3:29:37 PM 231.1 62.3
6/7/2019 3:29:38 PM 231.0 62.2
6/7/2019 3:29:39 PM 230.8 62.0
6/7/2019 3:29:40 PM 230.7 61.9
6/7/2019 3:29:41 PM 230.5 61.7
6/7/2019 3:29:42 PM 230.4 61.6
6/7/2019 3:29:43 PM 230.2 61.4
6/7/2019 3:29:44 PM 230.1 61.3
6/7/2019 3:29:45 PM 229.9 61.1
6/7/2019 3:29:46 PM 229.8 61.0
6/7/2019 3:29:47 PM 229.6 60.8
6/7/2019 3:29:48 PM 229.5 60.7
6/7/2019 3:29:49 PM 229.4 60.6
6/7/2019 3:29:50 PM 229.3 60.5
6/7/2019 3:29:51 PM 229.1 60.3
6/7/2019 3:29:52 PM 229.0 60.2
6/7/2019 3:29:53 PM 228.9 60.1
6/7/2019 3:29:54 PM 228.8 60.0
6/7/2019 3:29:55 PM 228.6 59.8
6/7/2019 3:29:56 PM 228.5 59.7
6/7/2019 3:29:57 PM 228.4 59.6
6/7/2019 3:29:58 PM 228.2 59.4
6/7/2019 3:29:59 PM 228.1 59.3
6/7/2019 3:30:00 PM 228.0 59.2
6/7/2019 3:30:01 PM 227.8 59.0
6/7/2019 3:30:02 PM 227.7 58.9
6/7/2019 3:30:03 PM 227.5 58.7
6/7/2019 3:30:04 PM 227.4 58.6
6/7/2019 3:30:05 PM 227.3 58.5
6/7/2019 3:30:06 PM 227.1 58.3
6/7/2019 3:30:07 PM 227.0 58.2
6/7/2019 3:30:08 PM 226.8 58.0
6/7/2019 3:30:09 PM 226.7 57.9
6/7/2019 3:30:10 PM 226.5 57.7
6/7/2019 3:30:11 PM 226.4 57.6
6/7/2019 3:30:12 PM 226.3 57.5
6/7/2019 3:30:13 PM 226.1 57.3
6/7/2019 3:30:14 PM 226.0 57.2
6/7/2019 3:30:15 PM 225.8 57.0
6/7/2019 3:30:16 PM 225.7 56.9
6/7/2019 3:30:17 PM 225.6 56.8
6/7/2019 3:30:18 PM 225.4 56.6
6/7/2019 3:30:19 PM 225.3 56.5
6/7/2019 3:30:20 PM 225.2 56.4
6/7/2019 3:30:21 PM 225.0 56.2
6/7/2019 3:30:22 PM 224.9 56.1
6/7/2019 3:30:23 PM 224.7 55.9
6/7/2019 3:30:24 PM 224.6 55.8
6/7/2019 3:30:25 PM 224.5 55.7
6/7/2019 3:30:26 PM 224.3 55.5
6/7/2019 3:30:27 PM 224.2 55.4
6/7/2019 3:30:28 PM 224.1 55.3
6/7/2019 3:30:29 PM 224.0 55.2
6/7/2019 3:30:30 PM 223.9 55.1
6/7/2019 3:30:31 PM 223.8 55.0
6/7/2019 3:30:32 PM 223.7 54.9
6/7/2019 3:30:33 PM 223.5 54.7
6/7/2019 3:30:34 PM 223.5 54.7
6/7/2019 3:30:35 PM 223.4 54.6
6/7/2019 3:30:36 PM 223.3 54.5
6/7/2019 3:30:37 PM 223.2 54.4
6/7/2019 3:30:38 PM 223.1 54.3
6/7/2019 3:30:39 PM 223.1 54.3
6/7/2019 3:30:40 PM 223.0 54.2
6/7/2019 3:30:41 PM 222.9 54.1
6/7/2019 3:30:42 PM 222.9 54.1
6/7/2019 3:30:43 PM 222.8 54.0
6/7/2019 3:30:44 PM 222.8 54.0
6/7/2019 3:30:45 PM 222.8 54.0
6/7/2019 3:30:46 PM 222.7 53.9
6/7/2019 3:30:47 PM 222.7 53.9
Page 349 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:30:48 PM 222.6 53.8
6/7/2019 3:30:49 PM 222.6 53.8
6/7/2019 3:30:50 PM 222.5 53.7
6/7/2019 3:30:51 PM 222.5 53.7
6/7/2019 3:30:52 PM 222.4 53.6
6/7/2019 3:30:53 PM 222.4 53.6
6/7/2019 3:30:54 PM 222.3 53.5
6/7/2019 3:30:55 PM 222.3 53.5
6/7/2019 3:30:56 PM 222.2 53.4
6/7/2019 3:30:57 PM 222.2 53.4
6/7/2019 3:30:58 PM 222.1 53.3
6/7/2019 3:30:59 PM 222.1 53.3
6/7/2019 3:31:00 PM 222.0 53.2
6/7/2019 3:31:01 PM 222.0 53.2
6/7/2019 3:31:02 PM 221.9 53.1
6/7/2019 3:31:03 PM 221.9 53.1
6/7/2019 3:31:04 PM 221.8 53.0
6/7/2019 3:31:05 PM 221.8 53.0
6/7/2019 3:31:06 PM 221.7 52.9
6/7/2019 3:31:07 PM 221.7 52.9
6/7/2019 3:31:08 PM 221.6 52.8
6/7/2019 3:31:09 PM 221.6 52.8
6/7/2019 3:31:10 PM 221.5 52.7
6/7/2019 3:31:11 PM 221.4 52.6
6/7/2019 3:31:12 PM 221.4 52.6
6/7/2019 3:31:13 PM 221.3 52.5
6/7/2019 3:31:14 PM 221.3 52.5
6/7/2019 3:31:15 PM 221.2 52.4
6/7/2019 3:31:16 PM 221.2 52.4
6/7/2019 3:31:17 PM 221.1 52.3
6/7/2019 3:31:18 PM 221.1 52.3
6/7/2019 3:31:19 PM 221.0 52.2
6/7/2019 3:31:20 PM 220.9 52.1
6/7/2019 3:31:21 PM 220.9 52.1
6/7/2019 3:31:22 PM 220.8 52.0
6/7/2019 3:31:23 PM 220.7 51.9
6/7/2019 3:31:24 PM 220.6 51.8
6/7/2019 3:31:25 PM 220.6 51.8
6/7/2019 3:31:26 PM 220.5 51.7
6/7/2019 3:31:27 PM 220.4 51.6
6/7/2019 3:31:28 PM 220.3 51.5
6/7/2019 3:31:29 PM 220.2 51.4
6/7/2019 3:31:30 PM 220.2 51.4
6/7/2019 3:31:31 PM 220.1 51.3
6/7/2019 3:31:32 PM 220.0 51.2
6/7/2019 3:31:33 PM 219.9 51.1
6/7/2019 3:31:34 PM 219.8 51.0
6/7/2019 3:31:35 PM 219.7 50.9
6/7/2019 3:31:36 PM 219.6 50.8
6/7/2019 3:31:37 PM 219.5 50.7
6/7/2019 3:31:38 PM 219.4 50.6
6/7/2019 3:31:39 PM 219.3 50.5
6/7/2019 3:31:40 PM 219.2 50.4
6/7/2019 3:31:41 PM 219.1 50.3
6/7/2019 3:31:42 PM 219.0 50.2
6/7/2019 3:31:43 PM 218.9 50.1
6/7/2019 3:31:44 PM 218.7 49.9
6/7/2019 3:31:45 PM 218.6 49.8
6/7/2019 3:31:46 PM 218.5 49.7
6/7/2019 3:31:47 PM 218.4 49.6
6/7/2019 3:31:48 PM 218.3 49.5
6/7/2019 3:31:49 PM 218.2 49.4
6/7/2019 3:31:50 PM 218.0 49.2
6/7/2019 3:31:51 PM 217.9 49.1
6/7/2019 3:31:52 PM 217.8 49.0
6/7/2019 3:31:53 PM 217.7 48.9
6/7/2019 3:31:54 PM 217.6 48.8
6/7/2019 3:31:55 PM 217.4 48.6
6/7/2019 3:31:56 PM 217.3 48.5
6/7/2019 3:31:57 PM 217.2 48.4
6/7/2019 3:31:58 PM 217.1 48.3
6/7/2019 3:31:59 PM 217.0 48.2
6/7/2019 3:32:00 PM 216.9 48.1
6/7/2019 3:32:01 PM 216.7 47.9
6/7/2019 3:32:02 PM 216.6 47.8
6/7/2019 3:32:03 PM 216.5 47.7
6/7/2019 3:32:04 PM 216.4 47.6
6/7/2019 3:32:05 PM 216.3 47.5
6/7/2019 3:32:06 PM 216.2 47.4
6/7/2019 3:32:07 PM 216.1 47.3
6/7/2019 3:32:08 PM 216.0 47.2
6/7/2019 3:32:09 PM 215.9 47.1
6/7/2019 3:32:10 PM 215.7 46.9
6/7/2019 3:32:11 PM 215.6 46.8
6/7/2019 3:32:12 PM 215.5 46.7
6/7/2019 3:32:13 PM 215.4 46.6
6/7/2019 3:32:14 PM 215.3 46.5
6/7/2019 3:32:15 PM 215.2 46.4
6/7/2019 3:32:16 PM 215.0 46.2
6/7/2019 3:32:17 PM 214.9 46.1
6/7/2019 3:32:18 PM 214.8 46.0
6/7/2019 3:32:19 PM 214.7 45.9
Page 350 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:32:20 PM 214.6 45.8
6/7/2019 3:32:21 PM 214.5 45.7
6/7/2019 3:32:22 PM 214.3 45.5
6/7/2019 3:32:23 PM 214.2 45.4
6/7/2019 3:32:24 PM 214.1 45.3
6/7/2019 3:32:25 PM 214.0 45.2
6/7/2019 3:32:26 PM 213.9 45.1
6/7/2019 3:32:27 PM 213.8 45.0
6/7/2019 3:32:28 PM 213.7 44.9
6/7/2019 3:32:29 PM 213.6 44.8
6/7/2019 3:32:30 PM 213.5 44.7
6/7/2019 3:32:31 PM 213.4 44.6
6/7/2019 3:32:32 PM 213.3 44.5
6/7/2019 3:32:33 PM 213.2 44.4
6/7/2019 3:32:34 PM 213.1 44.3
6/7/2019 3:32:35 PM 213.1 44.3
6/7/2019 3:32:36 PM 213.0 44.2
6/7/2019 3:32:37 PM 212.9 44.1
6/7/2019 3:32:38 PM 212.8 44.0
6/7/2019 3:32:39 PM 212.7 43.9
6/7/2019 3:32:40 PM 212.7 43.9
6/7/2019 3:32:41 PM 212.6 43.8
6/7/2019 3:32:42 PM 212.5 43.7
6/7/2019 3:32:43 PM 212.4 43.6
6/7/2019 3:32:44 PM 212.3 43.5
6/7/2019 3:32:45 PM 212.2 43.4
6/7/2019 3:32:46 PM 212.1 43.3
6/7/2019 3:32:47 PM 212.0 43.2
6/7/2019 3:32:48 PM 211.9 43.1
6/7/2019 3:32:49 PM 211.8 43.0
6/7/2019 3:32:50 PM 211.7 42.9
6/7/2019 3:32:51 PM 211.6 42.8
6/7/2019 3:32:52 PM 211.5 42.7
6/7/2019 3:32:53 PM 211.4 42.6
6/7/2019 3:32:54 PM 211.3 42.5
6/7/2019 3:32:55 PM 211.2 42.4
6/7/2019 3:32:56 PM 211.2 42.4
6/7/2019 3:32:57 PM 211.1 42.3
6/7/2019 3:32:58 PM 211.0 42.2
6/7/2019 3:32:59 PM 210.9 42.1
6/7/2019 3:33:00 PM 210.8 42.0
6/7/2019 3:33:01 PM 210.7 41.9
6/7/2019 3:33:02 PM 210.6 41.8
6/7/2019 3:33:03 PM 210.6 41.8
6/7/2019 3:33:04 PM 210.5 41.7
6/7/2019 3:33:05 PM 210.4 41.6
6/7/2019 3:33:06 PM 210.3 41.5
6/7/2019 3:33:07 PM 210.3 41.5
6/7/2019 3:33:08 PM 210.2 41.4
6/7/2019 3:33:09 PM 210.1 41.3
6/7/2019 3:33:10 PM 210.0 41.2
6/7/2019 3:33:11 PM 209.9 41.1
6/7/2019 3:33:12 PM 209.9 41.1
6/7/2019 3:33:13 PM 209.8 41.0
6/7/2019 3:33:14 PM 209.7 40.9
6/7/2019 3:33:15 PM 209.7 40.9
6/7/2019 3:33:16 PM 209.6 40.8
6/7/2019 3:33:17 PM 209.6 40.8
6/7/2019 3:33:18 PM 209.5 40.7
6/7/2019 3:33:19 PM 209.5 40.7
6/7/2019 3:33:20 PM 209.5 40.7
6/7/2019 3:33:21 PM 209.4 40.6
6/7/2019 3:33:22 PM 209.4 40.6
6/7/2019 3:33:23 PM 209.3 40.5
6/7/2019 3:33:24 PM 209.3 40.5
6/7/2019 3:33:25 PM 209.3 40.5
6/7/2019 3:33:26 PM 209.3 40.5
6/7/2019 3:33:27 PM 209.2 40.4
6/7/2019 3:33:28 PM 209.2 40.4
6/7/2019 3:33:29 PM 209.2 40.4
6/7/2019 3:33:30 PM 209.2 40.4
6/7/2019 3:33:31 PM 209.1 40.3
6/7/2019 3:33:32 PM 209.1 40.3
6/7/2019 3:33:33 PM 209.1 40.3
6/7/2019 3:33:34 PM 209.0 40.2
6/7/2019 3:33:35 PM 209.0 40.2
6/7/2019 3:33:36 PM 209.0 40.2
6/7/2019 3:33:37 PM 209.0 40.2
6/7/2019 3:33:38 PM 209.0 40.2
6/7/2019 3:33:39 PM 208.9 40.1
6/7/2019 3:33:40 PM 208.9 40.1
6/7/2019 3:33:41 PM 208.9 40.1
6/7/2019 3:33:42 PM 208.8 40.0
6/7/2019 3:33:43 PM 208.8 40.0
6/7/2019 3:33:44 PM 208.8 40.0
6/7/2019 3:33:45 PM 208.7 39.9
6/7/2019 3:33:46 PM 208.7 39.9
6/7/2019 3:33:47 PM 208.6 39.8
6/7/2019 3:33:48 PM 208.6 39.8
6/7/2019 3:33:49 PM 208.6 39.8
6/7/2019 3:33:50 PM 208.5 39.7
6/7/2019 3:33:51 PM 208.5 39.7
Page 351 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:33:52 PM 208.4 39.6
6/7/2019 3:33:53 PM 208.4 39.6
6/7/2019 3:33:54 PM 208.3 39.5
6/7/2019 3:33:55 PM 208.3 39.5
6/7/2019 3:33:56 PM 208.2 39.4
6/7/2019 3:33:57 PM 208.2 39.4
6/7/2019 3:33:58 PM 208.1 39.3
6/7/2019 3:33:59 PM 208.1 39.3
6/7/2019 3:34:00 PM 208.0 39.2
6/7/2019 3:34:01 PM 207.9 39.1
6/7/2019 3:34:02 PM 207.9 39.1
6/7/2019 3:34:03 PM 207.8 39.0
6/7/2019 3:34:04 PM 207.8 39.0
6/7/2019 3:34:05 PM 207.7 38.9
6/7/2019 3:34:06 PM 207.6 38.8
6/7/2019 3:34:07 PM 207.6 38.8
6/7/2019 3:34:08 PM 207.5 38.7
6/7/2019 3:34:09 PM 207.4 38.6
6/7/2019 3:34:10 PM 207.4 38.6
6/7/2019 3:34:11 PM 207.3 38.5
6/7/2019 3:34:12 PM 207.3 38.5
6/7/2019 3:34:13 PM 207.2 38.4
6/7/2019 3:34:14 PM 207.1 38.3
6/7/2019 3:34:15 PM 207.1 38.3
6/7/2019 3:34:16 PM 207.0 38.2
6/7/2019 3:34:17 PM 206.9 38.1
6/7/2019 3:34:18 PM 206.8 38.0
6/7/2019 3:34:19 PM 206.8 38.0
6/7/2019 3:34:20 PM 206.7 37.9
6/7/2019 3:34:21 PM 206.6 37.8
6/7/2019 3:34:22 PM 206.5 37.7
6/7/2019 3:34:23 PM 206.4 37.6
6/7/2019 3:34:24 PM 206.4 37.6
6/7/2019 3:34:25 PM 206.3 37.5
6/7/2019 3:34:26 PM 206.2 37.4
6/7/2019 3:34:27 PM 206.1 37.3
6/7/2019 3:34:28 PM 206.1 37.3
6/7/2019 3:34:29 PM 206.0 37.2
6/7/2019 3:34:30 PM 205.9 37.1
6/7/2019 3:34:31 PM 205.8 37.0
6/7/2019 3:34:32 PM 205.8 37.0
6/7/2019 3:34:33 PM 205.7 36.9
6/7/2019 3:34:34 PM 205.6 36.8
6/7/2019 3:34:35 PM 205.5 36.7
6/7/2019 3:34:36 PM 205.5 36.7
6/7/2019 3:34:37 PM 205.4 36.6
6/7/2019 3:34:38 PM 205.3 36.5
6/7/2019 3:34:39 PM 205.2 36.4
6/7/2019 3:34:40 PM 205.2 36.4
6/7/2019 3:34:41 PM 205.1 36.3
6/7/2019 3:34:42 PM 205.0 36.2
6/7/2019 3:34:43 PM 204.9 36.1
6/7/2019 3:34:44 PM 204.8 36.0
6/7/2019 3:34:45 PM 204.7 35.9
6/7/2019 3:34:46 PM 204.6 35.8
6/7/2019 3:34:47 PM 204.5 35.7
6/7/2019 3:34:48 PM 204.4 35.6
6/7/2019 3:34:49 PM 204.4 35.6
6/7/2019 3:34:50 PM 204.2 35.4
6/7/2019 3:34:51 PM 204.2 35.4
6/7/2019 3:34:52 PM 204.1 35.3
6/7/2019 3:34:53 PM 204.0 35.2
6/7/2019 3:34:54 PM 203.9 35.1
6/7/2019 3:34:55 PM 203.8 35.0
6/7/2019 3:34:56 PM 203.7 34.9
6/7/2019 3:34:57 PM 203.6 34.8
6/7/2019 3:34:58 PM 203.5 34.7
6/7/2019 3:34:59 PM 203.5 34.7
6/7/2019 3:35:00 PM 203.4 34.6
6/7/2019 3:35:01 PM 203.3 34.5
6/7/2019 3:35:02 PM 203.2 34.4
6/7/2019 3:35:03 PM 203.1 34.3
6/7/2019 3:35:04 PM 203.0 34.2
6/7/2019 3:35:05 PM 202.9 34.1
6/7/2019 3:35:06 PM 202.8 34.0
6/7/2019 3:35:07 PM 202.7 33.9
6/7/2019 3:35:08 PM 202.6 33.8
6/7/2019 3:35:09 PM 202.5 33.7
6/7/2019 3:35:10 PM 202.4 33.6
6/7/2019 3:35:11 PM 202.3 33.5
6/7/2019 3:35:12 PM 202.3 33.5
6/7/2019 3:35:13 PM 202.2 33.4
6/7/2019 3:35:14 PM 202.1 33.3
6/7/2019 3:35:15 PM 202.0 33.2
6/7/2019 3:35:16 PM 201.9 33.1
6/7/2019 3:35:17 PM 201.9 33.1
6/7/2019 3:35:18 PM 201.8 33.0
6/7/2019 3:35:19 PM 201.7 32.9
6/7/2019 3:35:20 PM 201.6 32.8
6/7/2019 3:35:21 PM 201.5 32.7
6/7/2019 3:35:22 PM 201.5 32.7
6/7/2019 3:35:23 PM 201.4 32.6
Page 352 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:35:24 PM 201.3 32.5
6/7/2019 3:35:25 PM 201.2 32.4
6/7/2019 3:35:26 PM 201.1 32.3
6/7/2019 3:35:27 PM 201.0 32.2
6/7/2019 3:35:28 PM 200.9 32.1
6/7/2019 3:35:29 PM 200.9 32.1
6/7/2019 3:35:30 PM 200.8 32.0
6/7/2019 3:35:31 PM 200.7 31.9
6/7/2019 3:35:32 PM 200.6 31.8
6/7/2019 3:35:33 PM 200.5 31.7
6/7/2019 3:35:34 PM 200.4 31.6
6/7/2019 3:35:35 PM 200.4 31.6
6/7/2019 3:35:36 PM 200.3 31.5
6/7/2019 3:35:37 PM 200.2 31.4
6/7/2019 3:35:38 PM 200.1 31.3
6/7/2019 3:35:39 PM 200.0 31.2
6/7/2019 3:35:40 PM 200.0 31.2
6/7/2019 3:35:41 PM 199.9 31.1
6/7/2019 3:35:42 PM 199.8 31.0
6/7/2019 3:35:43 PM 199.7 30.9
6/7/2019 3:35:44 PM 199.7 30.9
6/7/2019 3:35:45 PM 199.6 30.8
6/7/2019 3:35:46 PM 199.5 30.7
6/7/2019 3:35:47 PM 199.4 30.6
6/7/2019 3:35:48 PM 199.4 30.6
6/7/2019 3:35:49 PM 199.3 30.5
6/7/2019 3:35:50 PM 199.3 30.5
6/7/2019 3:35:51 PM 199.2 30.4
6/7/2019 3:35:52 PM 199.1 30.3
6/7/2019 3:35:53 PM 199.1 30.3
6/7/2019 3:35:54 PM 199.0 30.2
6/7/2019 3:35:55 PM 199.0 30.2
6/7/2019 3:35:56 PM 198.9 30.1
6/7/2019 3:35:57 PM 198.9 30.1
6/7/2019 3:35:58 PM 198.8 30.0
6/7/2019 3:35:59 PM 198.8 30.0
6/7/2019 3:36:00 PM 198.7 29.9
6/7/2019 3:36:01 PM 198.7 29.9
6/7/2019 3:36:02 PM 198.7 29.9
6/7/2019 3:36:03 PM 198.6 29.8
6/7/2019 3:36:04 PM 198.6 29.8
6/7/2019 3:36:05 PM 198.5 29.7
6/7/2019 3:36:06 PM 198.5 29.7
6/7/2019 3:36:07 PM 198.5 29.7
6/7/2019 3:36:08 PM 198.4 29.6
6/7/2019 3:36:09 PM 198.4 29.6
6/7/2019 3:36:10 PM 198.4 29.6
6/7/2019 3:36:11 PM 198.3 29.5
6/7/2019 3:36:12 PM 198.3 29.5
6/7/2019 3:36:13 PM 198.3 29.5
6/7/2019 3:36:14 PM 198.2 29.4
6/7/2019 3:36:15 PM 198.2 29.4
6/7/2019 3:36:16 PM 198.2 29.4
6/7/2019 3:36:17 PM 198.1 29.3
6/7/2019 3:36:18 PM 198.1 29.3
6/7/2019 3:36:19 PM 198.1 29.3
6/7/2019 3:36:20 PM 198.0 29.2
6/7/2019 3:36:21 PM 198.0 29.2
6/7/2019 3:36:22 PM 197.9 29.1
6/7/2019 3:36:23 PM 197.9 29.1
6/7/2019 3:36:24 PM 197.9 29.1
6/7/2019 3:36:25 PM 197.9 29.1
6/7/2019 3:36:26 PM 197.8 29.0
6/7/2019 3:36:27 PM 197.8 29.0
6/7/2019 3:36:28 PM 197.8 29.0
6/7/2019 3:36:29 PM 197.7 28.9
6/7/2019 3:36:30 PM 197.7 28.9
6/7/2019 3:36:31 PM 197.7 28.9
6/7/2019 3:36:32 PM 197.6 28.8
6/7/2019 3:36:33 PM 197.6 28.8
6/7/2019 3:36:34 PM 197.6 28.8
6/7/2019 3:36:35 PM 197.6 28.8
6/7/2019 3:36:36 PM 197.5 28.7
6/7/2019 3:36:37 PM 197.5 28.7
6/7/2019 3:36:38 PM 197.4 28.6
6/7/2019 3:36:39 PM 197.4 28.6
6/7/2019 3:36:40 PM 197.4 28.6
6/7/2019 3:36:41 PM 197.3 28.5
6/7/2019 3:36:42 PM 197.3 28.5
6/7/2019 3:36:43 PM 197.2 28.4
6/7/2019 3:36:44 PM 197.2 28.4
6/7/2019 3:36:45 PM 197.1 28.3
6/7/2019 3:36:46 PM 197.1 28.3
6/7/2019 3:36:47 PM 197.0 28.2
6/7/2019 3:36:48 PM 197.0 28.2
6/7/2019 3:36:49 PM 196.9 28.1
6/7/2019 3:36:50 PM 196.9 28.1
6/7/2019 3:36:51 PM 196.9 28.1
6/7/2019 3:36:52 PM 196.8 28.0
6/7/2019 3:36:53 PM 196.8 28.0
6/7/2019 3:36:54 PM 196.7 27.9
6/7/2019 3:36:55 PM 196.7 27.9
Page 353 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:36:56 PM 196.7 27.9
6/7/2019 3:36:57 PM 196.6 27.8
6/7/2019 3:36:58 PM 196.6 27.8
6/7/2019 3:36:59 PM 196.6 27.8
6/7/2019 3:37:00 PM 196.5 27.7
6/7/2019 3:37:01 PM 196.5 27.7
6/7/2019 3:37:02 PM 196.5 27.7
6/7/2019 3:37:03 PM 196.4 27.6
6/7/2019 3:37:04 PM 196.4 27.6
6/7/2019 3:37:05 PM 196.4 27.6
6/7/2019 3:37:06 PM 196.4 27.6
6/7/2019 3:37:07 PM 196.4 27.6
6/7/2019 3:37:08 PM 196.3 27.5
6/7/2019 3:37:09 PM 196.3 27.5
6/7/2019 3:37:10 PM 196.3 27.5
6/7/2019 3:37:11 PM 196.3 27.5
6/7/2019 3:37:12 PM 196.3 27.5
6/7/2019 3:37:13 PM 196.2 27.4
6/7/2019 3:37:14 PM 196.2 27.4
6/7/2019 3:37:15 PM 196.2 27.4
6/7/2019 3:37:16 PM 196.2 27.4
6/7/2019 3:37:17 PM 196.2 27.4
6/7/2019 3:37:18 PM 196.1 27.3
6/7/2019 3:37:19 PM 196.1 27.3
6/7/2019 3:37:20 PM 196.1 27.3
6/7/2019 3:37:21 PM 196.1 27.3
6/7/2019 3:37:22 PM 196.1 27.3
6/7/2019 3:37:23 PM 196.0 27.2
6/7/2019 3:37:24 PM 196.0 27.2
6/7/2019 3:37:25 PM 196.0 27.2
6/7/2019 3:37:26 PM 195.9 27.1
6/7/2019 3:37:27 PM 195.9 27.1
6/7/2019 3:37:28 PM 195.9 27.1
6/7/2019 3:37:29 PM 195.9 27.1
6/7/2019 3:37:30 PM 195.8 27.0
6/7/2019 3:37:31 PM 195.8 27.0
6/7/2019 3:37:32 PM 195.8 27.0
6/7/2019 3:37:33 PM 195.7 26.9
6/7/2019 3:37:34 PM 195.7 26.9
6/7/2019 3:37:35 PM 195.7 26.9
6/7/2019 3:37:36 PM 195.6 26.8
6/7/2019 3:37:37 PM 195.6 26.8
6/7/2019 3:37:38 PM 195.6 26.8
6/7/2019 3:37:39 PM 195.5 26.7
6/7/2019 3:37:40 PM 195.5 26.7
6/7/2019 3:37:41 PM 195.5 26.7
6/7/2019 3:37:42 PM 195.4 26.6
6/7/2019 3:37:43 PM 195.4 26.6
6/7/2019 3:37:44 PM 195.3 26.5
6/7/2019 3:37:45 PM 195.3 26.5
6/7/2019 3:37:46 PM 195.2 26.4
6/7/2019 3:37:47 PM 195.2 26.4
6/7/2019 3:37:48 PM 195.2 26.4
6/7/2019 3:37:49 PM 195.1 26.3
6/7/2019 3:37:50 PM 195.0 26.2
6/7/2019 3:37:51 PM 195.0 26.2
6/7/2019 3:37:52 PM 194.9 26.1
6/7/2019 3:37:53 PM 194.9 26.1
6/7/2019 3:37:54 PM 194.8 26.0
6/7/2019 3:37:55 PM 194.8 26.0
6/7/2019 3:37:56 PM 194.7 25.9
6/7/2019 3:37:57 PM 194.7 25.9
6/7/2019 3:37:58 PM 194.6 25.8
6/7/2019 3:37:59 PM 194.6 25.8
6/7/2019 3:38:00 PM 194.5 25.7
6/7/2019 3:38:01 PM 194.5 25.7
6/7/2019 3:38:02 PM 194.4 25.6
6/7/2019 3:38:03 PM 194.3 25.5
6/7/2019 3:38:04 PM 194.3 25.5
6/7/2019 3:38:05 PM 194.2 25.4
6/7/2019 3:38:06 PM 194.2 25.4
6/7/2019 3:38:07 PM 194.1 25.3
6/7/2019 3:38:08 PM 194.1 25.3
6/7/2019 3:38:09 PM 194.0 25.2
6/7/2019 3:38:10 PM 194.0 25.2
6/7/2019 3:38:11 PM 193.9 25.1
6/7/2019 3:38:12 PM 193.9 25.1
6/7/2019 3:38:13 PM 193.9 25.1
6/7/2019 3:38:14 PM 193.9 25.1
6/7/2019 3:38:15 PM 193.9 25.1
6/7/2019 3:38:16 PM 193.9 25.1
6/7/2019 3:38:17 PM 193.8 25.0
6/7/2019 3:38:18 PM 193.8 25.0
6/7/2019 3:38:19 PM 193.8 25.0
6/7/2019 3:38:20 PM 193.8 25.0
6/7/2019 3:38:21 PM 193.8 25.0
6/7/2019 3:38:22 PM 193.8 25.0
6/7/2019 3:38:23 PM 193.8 25.0
6/7/2019 3:38:24 PM 193.8 25.0
6/7/2019 3:38:25 PM 193.7 24.9
6/7/2019 3:38:26 PM 193.7 24.9
6/7/2019 3:38:27 PM 193.7 24.9
Page 354 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:38:28 PM 193.7 24.9
6/7/2019 3:38:29 PM 193.7 24.9
6/7/2019 3:38:30 PM 193.7 24.9
6/7/2019 3:38:31 PM 193.6 24.8
6/7/2019 3:38:32 PM 193.6 24.8
6/7/2019 3:38:33 PM 193.6 24.8
6/7/2019 3:38:34 PM 193.6 24.8
6/7/2019 3:38:35 PM 193.6 24.8
6/7/2019 3:38:36 PM 193.6 24.8
6/7/2019 3:38:37 PM 193.5 24.7
6/7/2019 3:38:38 PM 193.5 24.7
6/7/2019 3:38:39 PM 193.5 24.7
6/7/2019 3:38:40 PM 193.5 24.7
6/7/2019 3:38:41 PM 193.4 24.6
6/7/2019 3:38:42 PM 193.4 24.6
6/7/2019 3:38:43 PM 193.3 24.5
6/7/2019 3:38:44 PM 193.3 24.5
6/7/2019 3:38:45 PM 193.3 24.5
6/7/2019 3:38:46 PM 193.2 24.4
6/7/2019 3:38:47 PM 193.2 24.4
6/7/2019 3:38:48 PM 193.1 24.3
6/7/2019 3:38:49 PM 193.1 24.3
6/7/2019 3:38:50 PM 193.0 24.2
6/7/2019 3:38:51 PM 192.9 24.1
6/7/2019 3:38:52 PM 192.9 24.1
6/7/2019 3:38:53 PM 192.8 24.0
6/7/2019 3:38:54 PM 192.8 24.0
6/7/2019 3:38:55 PM 192.7 23.9
6/7/2019 3:38:56 PM 192.7 23.9
6/7/2019 3:38:57 PM 192.6 23.8
6/7/2019 3:38:58 PM 192.5 23.7
6/7/2019 3:38:59 PM 192.5 23.7
6/7/2019 3:39:00 PM 192.4 23.6
6/7/2019 3:39:01 PM 192.4 23.6
6/7/2019 3:39:02 PM 192.3 23.5
6/7/2019 3:39:03 PM 192.2 23.4
6/7/2019 3:39:04 PM 192.2 23.4
6/7/2019 3:39:05 PM 192.1 23.3
6/7/2019 3:39:06 PM 192.0 23.2
6/7/2019 3:39:07 PM 192.0 23.2
6/7/2019 3:39:08 PM 191.9 23.1
6/7/2019 3:39:09 PM 191.8 23.0
6/7/2019 3:39:10 PM 191.8 23.0
6/7/2019 3:39:11 PM 191.7 22.9
6/7/2019 3:39:12 PM 191.6 22.8
6/7/2019 3:39:13 PM 191.6 22.8
6/7/2019 3:39:14 PM 191.5 22.7
6/7/2019 3:39:15 PM 191.4 22.6
6/7/2019 3:39:16 PM 191.4 22.6
6/7/2019 3:39:17 PM 191.3 22.5
6/7/2019 3:39:18 PM 191.3 22.5
6/7/2019 3:39:19 PM 191.2 22.4
6/7/2019 3:39:20 PM 191.1 22.3
6/7/2019 3:39:21 PM 191.1 22.3
6/7/2019 3:39:22 PM 191.0 22.2
6/7/2019 3:39:23 PM 191.0 22.2
6/7/2019 3:39:24 PM 190.9 22.1
6/7/2019 3:39:25 PM 190.9 22.1
6/7/2019 3:39:26 PM 190.8 22.0
6/7/2019 3:39:27 PM 190.8 22.0
6/7/2019 3:39:28 PM 190.7 21.9
6/7/2019 3:39:29 PM 190.7 21.9
6/7/2019 3:39:30 PM 190.6 21.8
6/7/2019 3:39:31 PM 190.6 21.8
6/7/2019 3:39:32 PM 190.5 21.7
6/7/2019 3:39:33 PM 190.5 21.7
6/7/2019 3:39:34 PM 190.4 21.6
6/7/2019 3:39:35 PM 190.4 21.6
6/7/2019 3:39:36 PM 190.4 21.6
6/7/2019 3:39:37 PM 190.3 21.5
6/7/2019 3:39:38 PM 190.3 21.5
6/7/2019 3:39:39 PM 190.2 21.4
6/7/2019 3:39:40 PM 190.2 21.4
6/7/2019 3:39:41 PM 190.2 21.4
6/7/2019 3:39:42 PM 190.1 21.3
6/7/2019 3:39:43 PM 190.1 21.3
6/7/2019 3:39:44 PM 190.1 21.3
6/7/2019 3:39:45 PM 190.0 21.2
6/7/2019 3:39:46 PM 190.0 21.2
6/7/2019 3:39:47 PM 190.0 21.2
6/7/2019 3:39:48 PM 189.9 21.1
6/7/2019 3:39:49 PM 189.9 21.1
6/7/2019 3:39:50 PM 189.8 21.0
6/7/2019 3:39:51 PM 189.8 21.0
6/7/2019 3:39:52 PM 189.8 21.0
6/7/2019 3:39:53 PM 189.7 20.9
6/7/2019 3:39:54 PM 189.7 20.9
6/7/2019 3:39:55 PM 189.7 20.9
6/7/2019 3:39:56 PM 189.6 20.8
6/7/2019 3:39:57 PM 189.6 20.8
6/7/2019 3:39:58 PM 189.6 20.8
6/7/2019 3:39:59 PM 189.6 20.8
Page 355 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:40:00 PM 189.5 20.7
6/7/2019 3:40:01 PM 189.5 20.7
6/7/2019 3:40:02 PM 189.5 20.7
6/7/2019 3:40:03 PM 189.4 20.6
6/7/2019 3:40:04 PM 189.4 20.6
6/7/2019 3:40:05 PM 189.4 20.6
6/7/2019 3:40:06 PM 189.4 20.6
6/7/2019 3:40:07 PM 189.3 20.5
6/7/2019 3:40:08 PM 189.3 20.5
6/7/2019 3:40:09 PM 189.3 20.5
6/7/2019 3:40:10 PM 189.3 20.5
6/7/2019 3:40:11 PM 189.2 20.4
6/7/2019 3:40:12 PM 189.2 20.4
6/7/2019 3:40:13 PM 189.2 20.4
6/7/2019 3:40:14 PM 189.2 20.4
6/7/2019 3:40:15 PM 189.1 20.3
6/7/2019 3:40:16 PM 189.1 20.3
6/7/2019 3:40:17 PM 189.1 20.3
6/7/2019 3:40:18 PM 189.1 20.3
6/7/2019 3:40:19 PM 189.0 20.2
6/7/2019 3:40:20 PM 189.0 20.2
6/7/2019 3:40:21 PM 189.0 20.2
6/7/2019 3:40:22 PM 188.9 20.1
6/7/2019 3:40:23 PM 188.9 20.1
6/7/2019 3:40:24 PM 188.9 20.1
6/7/2019 3:40:25 PM 188.8 20.0
6/7/2019 3:40:26 PM 188.8 20.0
6/7/2019 3:40:27 PM 188.8 20.0
6/7/2019 3:40:28 PM 188.7 19.9
6/7/2019 3:40:29 PM 188.7 19.9
6/7/2019 3:40:30 PM 188.6 19.8
6/7/2019 3:40:31 PM 188.6 19.8
6/7/2019 3:40:32 PM 188.6 19.8
6/7/2019 3:40:33 PM 188.5 19.7
6/7/2019 3:40:34 PM 188.5 19.7
6/7/2019 3:40:35 PM 188.5 19.7
6/7/2019 3:40:36 PM 188.4 19.6
6/7/2019 3:40:37 PM 188.4 19.6
6/7/2019 3:40:38 PM 188.4 19.6
6/7/2019 3:40:39 PM 188.3 19.5
6/7/2019 3:40:40 PM 188.3 19.5
6/7/2019 3:40:41 PM 188.3 19.5
6/7/2019 3:40:42 PM 188.2 19.4
6/7/2019 3:40:43 PM 188.2 19.4
6/7/2019 3:40:44 PM 188.2 19.4
6/7/2019 3:40:45 PM 188.1 19.3
6/7/2019 3:40:46 PM 188.1 19.3
6/7/2019 3:40:47 PM 188.1 19.3
6/7/2019 3:40:48 PM 188.1 19.3
6/7/2019 3:40:49 PM 188.0 19.2
6/7/2019 3:40:50 PM 188.0 19.2
6/7/2019 3:40:51 PM 188.0 19.2
6/7/2019 3:40:52 PM 188.0 19.2
6/7/2019 3:40:53 PM 188.0 19.2
6/7/2019 3:40:54 PM 188.0 19.2
6/7/2019 3:40:55 PM 187.9 19.1
6/7/2019 3:40:56 PM 187.9 19.1
6/7/2019 3:40:57 PM 187.9 19.1
6/7/2019 3:40:58 PM 187.9 19.1
6/7/2019 3:40:59 PM 187.9 19.1
6/7/2019 3:41:00 PM 187.9 19.1
6/7/2019 3:41:01 PM 187.9 19.1
6/7/2019 3:41:02 PM 187.9 19.1
6/7/2019 3:41:03 PM 187.9 19.1
6/7/2019 3:41:04 PM 187.9 19.1
6/7/2019 3:41:05 PM 187.9 19.1
6/7/2019 3:41:06 PM 188.0 19.2
6/7/2019 3:41:07 PM 188.0 19.2
6/7/2019 3:41:08 PM 188.0 19.2
6/7/2019 3:41:09 PM 188.0 19.2
6/7/2019 3:41:10 PM 188.0 19.2
6/7/2019 3:41:11 PM 188.0 19.2
6/7/2019 3:41:12 PM 188.0 19.2
6/7/2019 3:41:13 PM 188.0 19.2
6/7/2019 3:41:14 PM 188.0 19.2
6/7/2019 3:41:15 PM 188.0 19.2
6/7/2019 3:41:16 PM 188.0 19.2
6/7/2019 3:41:17 PM 188.1 19.3
6/7/2019 3:41:18 PM 188.1 19.3
6/7/2019 3:41:19 PM 188.1 19.3
6/7/2019 3:41:20 PM 188.1 19.3
6/7/2019 3:41:21 PM 188.1 19.3
6/7/2019 3:41:22 PM 188.1 19.3
6/7/2019 3:41:23 PM 188.1 19.3
6/7/2019 3:41:24 PM 188.0 19.2
6/7/2019 3:41:25 PM 188.0 19.2
6/7/2019 3:41:26 PM 188.0 19.2
6/7/2019 3:41:27 PM 188.0 19.2
6/7/2019 3:41:28 PM 188.0 19.2
6/7/2019 3:41:29 PM 188.0 19.2
6/7/2019 3:41:30 PM 188.0 19.2
6/7/2019 3:41:31 PM 188.0 19.2
Page 356 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:41:32 PM 188.0 19.2
6/7/2019 3:41:33 PM 187.9 19.1
6/7/2019 3:41:34 PM 187.9 19.1
6/7/2019 3:41:35 PM 187.9 19.1
6/7/2019 3:41:36 PM 187.9 19.1
6/7/2019 3:41:37 PM 187.8 19.0
6/7/2019 3:41:38 PM 187.8 19.0
6/7/2019 3:41:39 PM 187.8 19.0
6/7/2019 3:41:40 PM 187.7 18.9
6/7/2019 3:41:41 PM 187.7 18.9
6/7/2019 3:41:42 PM 187.6 18.8
6/7/2019 3:41:43 PM 187.6 18.8
6/7/2019 3:41:44 PM 187.5 18.7
6/7/2019 3:41:45 PM 187.5 18.7
6/7/2019 3:41:46 PM 187.4 18.6
6/7/2019 3:41:47 PM 187.3 18.5
6/7/2019 3:41:48 PM 187.3 18.5
6/7/2019 3:41:49 PM 187.2 18.4
6/7/2019 3:41:50 PM 187.1 18.3
6/7/2019 3:41:51 PM 187.1 18.3
6/7/2019 3:41:52 PM 187.0 18.2
6/7/2019 3:41:53 PM 186.9 18.1
6/7/2019 3:41:54 PM 186.9 18.1
6/7/2019 3:41:55 PM 186.8 18.0
6/7/2019 3:41:56 PM 186.7 17.9
6/7/2019 3:41:57 PM 186.7 17.9
6/7/2019 3:41:58 PM 186.6 17.8
6/7/2019 3:41:59 PM 186.5 17.7
6/7/2019 3:42:00 PM 186.5 17.7
6/7/2019 3:42:01 PM 186.4 17.6
6/7/2019 3:42:02 PM 186.4 17.6
6/7/2019 3:42:03 PM 186.4 17.6
6/7/2019 3:42:04 PM 186.3 17.5
6/7/2019 3:42:05 PM 186.3 17.5
6/7/2019 3:42:06 PM 186.2 17.4
6/7/2019 3:42:07 PM 186.2 17.4
6/7/2019 3:42:08 PM 186.2 17.4
6/7/2019 3:42:09 PM 186.1 17.3
6/7/2019 3:42:10 PM 186.1 17.3
6/7/2019 3:42:11 PM 186.1 17.3
6/7/2019 3:42:12 PM 186.0 17.2
6/7/2019 3:42:13 PM 186.0 17.2
6/7/2019 3:42:14 PM 186.0 17.2
6/7/2019 3:42:15 PM 185.9 17.1
6/7/2019 3:42:16 PM 185.9 17.1
6/7/2019 3:42:17 PM 185.9 17.1
6/7/2019 3:42:18 PM 185.8 17.0
6/7/2019 3:42:19 PM 185.8 17.0
6/7/2019 3:42:20 PM 185.8 17.0
6/7/2019 3:42:21 PM 185.7 16.9
6/7/2019 3:42:22 PM 185.7 16.9
6/7/2019 3:42:23 PM 185.7 16.9
6/7/2019 3:42:24 PM 185.6 16.8
6/7/2019 3:42:25 PM 185.6 16.8
6/7/2019 3:42:26 PM 185.6 16.8
6/7/2019 3:42:27 PM 185.5 16.7
6/7/2019 3:42:28 PM 185.5 16.7
6/7/2019 3:42:29 PM 185.5 16.7
6/7/2019 3:42:30 PM 185.4 16.6
6/7/2019 3:42:31 PM 185.4 16.6
6/7/2019 3:42:32 PM 185.4 16.6
6/7/2019 3:42:33 PM 185.3 16.5
6/7/2019 3:42:34 PM 185.3 16.5
6/7/2019 3:42:35 PM 185.3 16.5
6/7/2019 3:42:36 PM 185.3 16.5
6/7/2019 3:42:37 PM 185.2 16.4
6/7/2019 3:42:38 PM 185.2 16.4
6/7/2019 3:42:39 PM 185.2 16.4
6/7/2019 3:42:40 PM 185.1 16.3
6/7/2019 3:42:41 PM 185.1 16.3
6/7/2019 3:42:42 PM 185.1 16.3
6/7/2019 3:42:43 PM 185.1 16.3
6/7/2019 3:42:44 PM 185.1 16.3
6/7/2019 3:42:45 PM 185.1 16.3
6/7/2019 3:42:46 PM 185.1 16.3
6/7/2019 3:42:47 PM 185.0 16.2
6/7/2019 3:42:48 PM 185.0 16.2
6/7/2019 3:42:49 PM 185.0 16.2
6/7/2019 3:42:50 PM 185.0 16.2
6/7/2019 3:42:51 PM 185.0 16.2
6/7/2019 3:42:52 PM 185.0 16.2
6/7/2019 3:42:53 PM 185.0 16.2
6/7/2019 3:42:54 PM 185.0 16.2
6/7/2019 3:42:55 PM 185.0 16.2
6/7/2019 3:42:56 PM 185.0 16.2
6/7/2019 3:42:57 PM 185.0 16.2
6/7/2019 3:42:58 PM 185.0 16.2
6/7/2019 3:42:59 PM 185.0 16.2
6/7/2019 3:43:00 PM 185.0 16.2
6/7/2019 3:43:01 PM 185.0 16.2
6/7/2019 3:43:02 PM 185.0 16.2
6/7/2019 3:43:03 PM 185.0 16.2
Page 357 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:43:04 PM 185.0 16.2
6/7/2019 3:43:05 PM 185.0 16.2
6/7/2019 3:43:06 PM 185.0 16.2
6/7/2019 3:43:07 PM 185.0 16.2
6/7/2019 3:43:08 PM 185.0 16.2
6/7/2019 3:43:09 PM 184.9 16.1
6/7/2019 3:43:10 PM 184.9 16.1
6/7/2019 3:43:11 PM 184.9 16.1
6/7/2019 3:43:12 PM 184.9 16.1
6/7/2019 3:43:13 PM 184.8 16.0
6/7/2019 3:43:14 PM 184.8 16.0
6/7/2019 3:43:15 PM 184.8 16.0
6/7/2019 3:43:16 PM 184.8 16.0
6/7/2019 3:43:17 PM 184.7 15.9
6/7/2019 3:43:18 PM 184.7 15.9
6/7/2019 3:43:19 PM 184.7 15.9
6/7/2019 3:43:20 PM 184.6 15.8
6/7/2019 3:43:21 PM 184.6 15.8
6/7/2019 3:43:22 PM 184.6 15.8
6/7/2019 3:43:23 PM 184.5 15.7
6/7/2019 3:43:24 PM 184.5 15.7
6/7/2019 3:43:25 PM 184.4 15.6
6/7/2019 3:43:26 PM 184.4 15.6
6/7/2019 3:43:27 PM 184.4 15.6
6/7/2019 3:43:28 PM 184.3 15.5
6/7/2019 3:43:29 PM 184.3 15.5
6/7/2019 3:43:30 PM 184.2 15.4
6/7/2019 3:43:31 PM 184.2 15.4
6/7/2019 3:43:32 PM 184.1 15.3
6/7/2019 3:43:33 PM 184.1 15.3
6/7/2019 3:43:34 PM 184.0 15.2
6/7/2019 3:43:35 PM 184.0 15.2
6/7/2019 3:43:36 PM 183.9 15.1
6/7/2019 3:43:37 PM 183.9 15.1
6/7/2019 3:43:38 PM 183.9 15.1
6/7/2019 3:43:39 PM 183.8 15.0
6/7/2019 3:43:40 PM 183.8 15.0
6/7/2019 3:43:41 PM 183.7 14.9
6/7/2019 3:43:42 PM 183.7 14.9
6/7/2019 3:43:43 PM 183.7 14.9
6/7/2019 3:43:44 PM 183.6 14.8
6/7/2019 3:43:45 PM 183.6 14.8
6/7/2019 3:43:46 PM 183.5 14.7
6/7/2019 3:43:47 PM 183.5 14.7
6/7/2019 3:43:48 PM 183.5 14.7
6/7/2019 3:43:49 PM 183.4 14.6
6/7/2019 3:43:50 PM 183.4 14.6
6/7/2019 3:43:51 PM 183.4 14.6
6/7/2019 3:43:52 PM 183.4 14.6
6/7/2019 3:43:53 PM 183.3 14.5
6/7/2019 3:43:54 PM 183.3 14.5
6/7/2019 3:43:55 PM 183.3 14.5
6/7/2019 3:43:56 PM 183.3 14.5
6/7/2019 3:43:57 PM 183.3 14.5
6/7/2019 3:43:58 PM 183.3 14.5
6/7/2019 3:43:59 PM 183.3 14.5
6/7/2019 3:44:00 PM 183.3 14.5
6/7/2019 3:44:01 PM 183.3 14.5
6/7/2019 3:44:02 PM 183.3 14.5
6/7/2019 3:44:03 PM 183.3 14.5
6/7/2019 3:44:04 PM 183.3 14.5
6/7/2019 3:44:05 PM 183.3 14.5
6/7/2019 3:44:06 PM 183.3 14.5
6/7/2019 3:44:07 PM 183.4 14.6
6/7/2019 3:44:08 PM 183.4 14.6
6/7/2019 3:44:09 PM 183.4 14.6
6/7/2019 3:44:10 PM 183.4 14.6
6/7/2019 3:44:11 PM 183.4 14.6
6/7/2019 3:44:12 PM 183.4 14.6
6/7/2019 3:44:13 PM 183.4 14.6
6/7/2019 3:44:14 PM 183.4 14.6
6/7/2019 3:44:15 PM 183.4 14.6
6/7/2019 3:44:16 PM 183.4 14.6
6/7/2019 3:44:17 PM 183.5 14.7
6/7/2019 3:44:18 PM 183.5 14.7
6/7/2019 3:44:19 PM 183.5 14.7
6/7/2019 3:44:20 PM 183.5 14.7
6/7/2019 3:44:21 PM 183.5 14.7
6/7/2019 3:44:22 PM 183.5 14.7
6/7/2019 3:44:23 PM 183.5 14.7
6/7/2019 3:44:24 PM 183.5 14.7
6/7/2019 3:44:25 PM 183.4 14.6
6/7/2019 3:44:26 PM 183.4 14.6
6/7/2019 3:44:27 PM 183.4 14.6
6/7/2019 3:44:28 PM 183.4 14.6
6/7/2019 3:44:29 PM 183.4 14.6
6/7/2019 3:44:30 PM 183.4 14.6
6/7/2019 3:44:31 PM 183.3 14.5
6/7/2019 3:44:32 PM 183.3 14.5
6/7/2019 3:44:33 PM 183.3 14.5
6/7/2019 3:44:34 PM 183.2 14.4
6/7/2019 3:44:35 PM 183.2 14.4
Page 358 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:44:36 PM 183.2 14.4
6/7/2019 3:44:37 PM 183.1 14.3
6/7/2019 3:44:38 PM 183.1 14.3
6/7/2019 3:44:39 PM 183.1 14.3
6/7/2019 3:44:40 PM 183.0 14.2
6/7/2019 3:44:41 PM 183.0 14.2
6/7/2019 3:44:42 PM 182.9 14.1
6/7/2019 3:44:43 PM 182.9 14.1
6/7/2019 3:44:44 PM 182.9 14.1
6/7/2019 3:44:45 PM 182.8 14.0
6/7/2019 3:44:46 PM 182.8 14.0
6/7/2019 3:44:47 PM 182.7 13.9
6/7/2019 3:44:48 PM 182.7 13.9
6/7/2019 3:44:49 PM 182.6 13.8
6/7/2019 3:44:50 PM 182.6 13.8
6/7/2019 3:44:51 PM 182.5 13.7
6/7/2019 3:44:52 PM 182.4 13.6
6/7/2019 3:44:53 PM 182.4 13.6
6/7/2019 3:44:54 PM 182.3 13.5
6/7/2019 3:44:55 PM 182.3 13.5
6/7/2019 3:44:56 PM 182.2 13.4
6/7/2019 3:44:57 PM 182.2 13.4
6/7/2019 3:44:58 PM 182.1 13.3
6/7/2019 3:44:59 PM 182.0 13.2
6/7/2019 3:45:00 PM 182.0 13.2
6/7/2019 3:45:01 PM 181.9 13.1
6/7/2019 3:45:02 PM 181.9 13.1
6/7/2019 3:45:03 PM 181.8 13.0
6/7/2019 3:45:04 PM 181.8 13.0
6/7/2019 3:45:05 PM 181.7 12.9
6/7/2019 3:45:06 PM 181.7 12.9
6/7/2019 3:45:07 PM 181.6 12.8
6/7/2019 3:45:08 PM 181.5 12.7
6/7/2019 3:45:09 PM 181.5 12.7
6/7/2019 3:45:10 PM 181.4 12.6
6/7/2019 3:45:11 PM 181.4 12.6
6/7/2019 3:45:12 PM 181.3 12.5
6/7/2019 3:45:13 PM 181.3 12.5
6/7/2019 3:45:14 PM 181.2 12.4
6/7/2019 3:45:15 PM 181.2 12.4
6/7/2019 3:45:16 PM 181.1 12.3
6/7/2019 3:45:17 PM 181.1 12.3
6/7/2019 3:45:18 PM 181.0 12.2
6/7/2019 3:45:19 PM 181.0 12.2
6/7/2019 3:45:20 PM 180.9 12.1
6/7/2019 3:45:21 PM 180.9 12.1
6/7/2019 3:45:22 PM 180.8 12.0
6/7/2019 3:45:23 PM 180.8 12.0
6/7/2019 3:45:24 PM 180.8 12.0
6/7/2019 3:45:25 PM 180.7 11.9
6/7/2019 3:45:26 PM 180.7 11.9
6/7/2019 3:45:27 PM 180.7 11.9
6/7/2019 3:45:28 PM 180.6 11.8
6/7/2019 3:45:29 PM 180.6 11.8
6/7/2019 3:45:30 PM 180.6 11.8
6/7/2019 3:45:31 PM 180.5 11.7
6/7/2019 3:45:32 PM 180.5 11.7
6/7/2019 3:45:33 PM 180.5 11.7
6/7/2019 3:45:34 PM 180.5 11.7
6/7/2019 3:45:35 PM 180.5 11.7
6/7/2019 3:45:36 PM 180.4 11.6
6/7/2019 3:45:37 PM 180.4 11.6
6/7/2019 3:45:38 PM 180.4 11.6
6/7/2019 3:45:39 PM 180.4 11.6
6/7/2019 3:45:40 PM 180.4 11.6
6/7/2019 3:45:41 PM 180.4 11.6
6/7/2019 3:45:42 PM 180.4 11.6
6/7/2019 3:45:43 PM 180.4 11.6
6/7/2019 3:45:44 PM 180.3 11.5
6/7/2019 3:45:45 PM 180.3 11.5
6/7/2019 3:45:46 PM 180.3 11.5
6/7/2019 3:45:47 PM 180.3 11.5
6/7/2019 3:45:48 PM 180.3 11.5
6/7/2019 3:45:49 PM 180.3 11.5
6/7/2019 3:45:50 PM 180.3 11.5
6/7/2019 3:45:51 PM 180.3 11.5
6/7/2019 3:45:52 PM 180.2 11.4
6/7/2019 3:45:53 PM 180.2 11.4
6/7/2019 3:45:54 PM 180.2 11.4
6/7/2019 3:45:55 PM 180.2 11.4
6/7/2019 3:45:56 PM 180.2 11.4
6/7/2019 3:45:57 PM 180.2 11.4
6/7/2019 3:45:58 PM 180.2 11.4
6/7/2019 3:45:59 PM 180.1 11.3
6/7/2019 3:46:00 PM 180.1 11.3
6/7/2019 3:46:01 PM 180.1 11.3
6/7/2019 3:46:02 PM 180.1 11.3
6/7/2019 3:46:03 PM 180.1 11.3
6/7/2019 3:46:04 PM 180.1 11.3
6/7/2019 3:46:05 PM 180.1 11.3
6/7/2019 3:46:06 PM 180.1 11.3
6/7/2019 3:46:07 PM 180.0 11.2
Page 359 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:46:08 PM 180.0 11.2
6/7/2019 3:46:09 PM 180.0 11.2
6/7/2019 3:46:10 PM 180.0 11.2
6/7/2019 3:46:11 PM 179.9 11.1
6/7/2019 3:46:12 PM 179.9 11.1
6/7/2019 3:46:13 PM 179.9 11.1
6/7/2019 3:46:14 PM 179.9 11.1
6/7/2019 3:46:15 PM 179.9 11.1
6/7/2019 3:46:16 PM 179.9 11.1
6/7/2019 3:46:17 PM 179.8 11.0
6/7/2019 3:46:18 PM 179.8 11.0
6/7/2019 3:46:19 PM 179.8 11.0
6/7/2019 3:46:20 PM 179.8 11.0
6/7/2019 3:46:21 PM 179.8 11.0
6/7/2019 3:46:22 PM 179.8 11.0
6/7/2019 3:46:23 PM 179.8 11.0
6/7/2019 3:46:24 PM 179.8 11.0
6/7/2019 3:46:25 PM 179.7 10.9
6/7/2019 3:46:26 PM 179.7 10.9
6/7/2019 3:46:27 PM 179.7 10.9
6/7/2019 3:46:28 PM 179.7 10.9
6/7/2019 3:46:29 PM 179.7 10.9
6/7/2019 3:46:30 PM 179.7 10.9
6/7/2019 3:46:31 PM 179.7 10.9
6/7/2019 3:46:32 PM 179.7 10.9
6/7/2019 3:46:33 PM 179.6 10.8
6/7/2019 3:46:34 PM 179.6 10.8
6/7/2019 3:46:35 PM 179.6 10.8
6/7/2019 3:46:36 PM 179.6 10.8
6/7/2019 3:46:37 PM 179.6 10.8
6/7/2019 3:46:38 PM 179.6 10.8
6/7/2019 3:46:39 PM 179.6 10.8
6/7/2019 3:46:40 PM 179.6 10.8
6/7/2019 3:46:41 PM 179.5 10.7
6/7/2019 3:46:42 PM 179.5 10.7
6/7/2019 3:46:43 PM 179.5 10.7
6/7/2019 3:46:44 PM 179.5 10.7
6/7/2019 3:46:45 PM 179.5 10.7
6/7/2019 3:46:46 PM 179.5 10.7
6/7/2019 3:46:47 PM 179.5 10.7
6/7/2019 3:46:48 PM 179.5 10.7
6/7/2019 3:46:49 PM 179.5 10.7
6/7/2019 3:46:50 PM 179.5 10.7
6/7/2019 3:46:51 PM 179.5 10.7
6/7/2019 3:46:52 PM 179.5 10.7
6/7/2019 3:46:53 PM 179.5 10.7
6/7/2019 3:46:54 PM 179.5 10.7
6/7/2019 3:46:55 PM 179.5 10.7
6/7/2019 3:46:56 PM 179.5 10.7
6/7/2019 3:46:57 PM 179.5 10.7
6/7/2019 3:46:58 PM 179.5 10.7
6/7/2019 3:46:59 PM 179.5 10.7
6/7/2019 3:47:00 PM 179.5 10.7
6/7/2019 3:47:01 PM 179.5 10.7
6/7/2019 3:47:02 PM 179.5 10.7
6/7/2019 3:47:03 PM 179.5 10.7
6/7/2019 3:47:04 PM 179.5 10.7
6/7/2019 3:47:05 PM 179.5 10.7
6/7/2019 3:47:06 PM 179.5 10.7
6/7/2019 3:47:07 PM 179.5 10.7
6/7/2019 3:47:08 PM 179.5 10.7
6/7/2019 3:47:09 PM 179.5 10.7
6/7/2019 3:47:10 PM 179.5 10.7
6/7/2019 3:47:11 PM 179.5 10.7
6/7/2019 3:47:12 PM 179.5 10.7
6/7/2019 3:47:13 PM 179.5 10.7
6/7/2019 3:47:14 PM 179.5 10.7
6/7/2019 3:47:15 PM 179.5 10.7
6/7/2019 3:47:16 PM 179.5 10.7
6/7/2019 3:47:17 PM 179.5 10.7
6/7/2019 3:47:18 PM 179.5 10.7
6/7/2019 3:47:19 PM 179.5 10.7
6/7/2019 3:47:20 PM 179.5 10.7
6/7/2019 3:47:21 PM 179.4 10.6
6/7/2019 3:47:22 PM 179.4 10.6
6/7/2019 3:47:23 PM 179.4 10.6
6/7/2019 3:47:24 PM 179.4 10.6
6/7/2019 3:47:25 PM 179.4 10.6
6/7/2019 3:47:26 PM 179.4 10.6
6/7/2019 3:47:27 PM 179.4 10.6
6/7/2019 3:47:28 PM 179.4 10.6
6/7/2019 3:47:29 PM 179.4 10.6
6/7/2019 3:47:30 PM 179.3 10.5
6/7/2019 3:47:31 PM 179.3 10.5
6/7/2019 3:47:32 PM 179.3 10.5
6/7/2019 3:47:33 PM 179.3 10.5
6/7/2019 3:47:34 PM 179.3 10.5
6/7/2019 3:47:35 PM 179.3 10.5
6/7/2019 3:47:36 PM 179.3 10.5
6/7/2019 3:47:37 PM 179.2 10.4
6/7/2019 3:47:38 PM 179.2 10.4
6/7/2019 3:47:39 PM 179.2 10.4
Page 360 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:47:40 PM 179.2 10.4
6/7/2019 3:47:41 PM 179.2 10.4
6/7/2019 3:47:42 PM 179.2 10.4
6/7/2019 3:47:43 PM 179.2 10.4
6/7/2019 3:47:44 PM 179.1 10.3
6/7/2019 3:47:45 PM 179.1 10.3
6/7/2019 3:47:46 PM 179.1 10.3
6/7/2019 3:47:47 PM 179.1 10.3
6/7/2019 3:47:48 PM 179.1 10.3
6/7/2019 3:47:49 PM 179.1 10.3
6/7/2019 3:47:50 PM 179.1 10.3
6/7/2019 3:47:51 PM 179.0 10.2
6/7/2019 3:47:52 PM 179.0 10.2
6/7/2019 3:47:53 PM 179.0 10.2
6/7/2019 3:47:54 PM 179.0 10.2
6/7/2019 3:47:55 PM 179.0 10.2
6/7/2019 3:47:56 PM 179.0 10.2
6/7/2019 3:47:57 PM 179.0 10.2
6/7/2019 3:47:58 PM 179.0 10.2
6/7/2019 3:47:59 PM 179.0 10.2
6/7/2019 3:48:00 PM 178.9 10.1
6/7/2019 3:48:01 PM 178.9 10.1
6/7/2019 3:48:02 PM 178.9 10.1
6/7/2019 3:48:03 PM 178.9 10.1
6/7/2019 3:48:04 PM 178.9 10.1
6/7/2019 3:48:05 PM 178.9 10.1
6/7/2019 3:48:06 PM 178.8 10.0
6/7/2019 3:48:07 PM 178.8 10.0
6/7/2019 3:48:08 PM 178.8 10.0
6/7/2019 3:48:09 PM 178.8 10.0
6/7/2019 3:48:10 PM 178.8 10.0
6/7/2019 3:48:11 PM 178.7 9.9
6/7/2019 3:48:12 PM 178.7 9.9
6/7/2019 3:48:13 PM 178.7 9.9
6/7/2019 3:48:14 PM 178.7 9.9
6/7/2019 3:48:15 PM 178.6 9.8
6/7/2019 3:48:16 PM 178.6 9.8
6/7/2019 3:48:17 PM 178.6 9.8
6/7/2019 3:48:18 PM 178.6 9.8
6/7/2019 3:48:19 PM 178.6 9.8
6/7/2019 3:48:20 PM 178.5 9.7
6/7/2019 3:48:21 PM 178.5 9.7
6/7/2019 3:48:22 PM 178.5 9.7
6/7/2019 3:48:23 PM 178.5 9.7
6/7/2019 3:48:24 PM 178.5 9.7
6/7/2019 3:48:25 PM 178.4 9.6
6/7/2019 3:48:26 PM 178.4 9.6
6/7/2019 3:48:27 PM 178.4 9.6
6/7/2019 3:48:28 PM 178.4 9.6
6/7/2019 3:48:29 PM 178.4 9.6
6/7/2019 3:48:30 PM 178.4 9.6
6/7/2019 3:48:31 PM 178.4 9.6
6/7/2019 3:48:32 PM 178.3 9.5
6/7/2019 3:48:33 PM 178.3 9.5
6/7/2019 3:48:34 PM 178.3 9.5
6/7/2019 3:48:35 PM 178.3 9.5
6/7/2019 3:48:36 PM 178.3 9.5
6/7/2019 3:48:37 PM 178.3 9.5
6/7/2019 3:48:38 PM 178.3 9.5
6/7/2019 3:48:39 PM 178.3 9.5
6/7/2019 3:48:40 PM 178.3 9.5
6/7/2019 3:48:41 PM 178.3 9.5
6/7/2019 3:48:42 PM 178.3 9.5
6/7/2019 3:48:43 PM 178.3 9.5
6/7/2019 3:48:44 PM 178.3 9.5
6/7/2019 3:48:45 PM 178.3 9.5
6/7/2019 3:48:46 PM 178.3 9.5
6/7/2019 3:48:47 PM 178.3 9.5
6/7/2019 3:48:48 PM 178.3 9.5
6/7/2019 3:48:49 PM 178.3 9.5
6/7/2019 3:48:50 PM 178.3 9.5
6/7/2019 3:48:51 PM 178.3 9.5
6/7/2019 3:48:52 PM 178.3 9.5
6/7/2019 3:48:53 PM 178.3 9.5
6/7/2019 3:48:54 PM 178.3 9.5
6/7/2019 3:48:55 PM 178.3 9.5
6/7/2019 3:48:56 PM 178.3 9.5
6/7/2019 3:48:57 PM 178.3 9.5
6/7/2019 3:48:58 PM 178.3 9.5
6/7/2019 3:48:59 PM 178.3 9.5
6/7/2019 3:49:00 PM 178.3 9.5
6/7/2019 3:49:01 PM 178.3 9.5
6/7/2019 3:49:02 PM 178.3 9.5
6/7/2019 3:49:03 PM 178.4 9.6
6/7/2019 3:49:04 PM 178.4 9.6
6/7/2019 3:49:05 PM 178.4 9.6
6/7/2019 3:49:06 PM 178.4 9.6
6/7/2019 3:49:07 PM 178.4 9.6
6/7/2019 3:49:08 PM 178.4 9.6
6/7/2019 3:49:09 PM 178.4 9.6
6/7/2019 3:49:10 PM 178.4 9.6
6/7/2019 3:49:11 PM 178.4 9.6
Page 361 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:49:12 PM 178.4 9.6
6/7/2019 3:49:13 PM 178.4 9.6
6/7/2019 3:49:14 PM 178.5 9.7
6/7/2019 3:49:15 PM 178.5 9.7
6/7/2019 3:49:16 PM 178.5 9.7
6/7/2019 3:49:17 PM 178.5 9.7
6/7/2019 3:49:18 PM 178.5 9.7
6/7/2019 3:49:19 PM 178.5 9.7
6/7/2019 3:49:20 PM 178.5 9.7
6/7/2019 3:49:21 PM 178.5 9.7
6/7/2019 3:49:22 PM 178.5 9.7
6/7/2019 3:49:23 PM 178.5 9.7
6/7/2019 3:49:24 PM 178.5 9.7
6/7/2019 3:49:25 PM 178.5 9.7
6/7/2019 3:49:26 PM 178.5 9.7
6/7/2019 3:49:27 PM 178.5 9.7
6/7/2019 3:49:28 PM 178.5 9.7
6/7/2019 3:49:29 PM 178.5 9.7
6/7/2019 3:49:30 PM 178.5 9.7
6/7/2019 3:49:31 PM 178.5 9.7
6/7/2019 3:49:32 PM 178.4 9.6
6/7/2019 3:49:33 PM 178.4 9.6
6/7/2019 3:49:34 PM 178.4 9.6
6/7/2019 3:49:35 PM 178.4 9.6
6/7/2019 3:49:36 PM 178.3 9.5
6/7/2019 3:49:37 PM 178.3 9.5
6/7/2019 3:49:38 PM 178.3 9.5
6/7/2019 3:49:39 PM 178.3 9.5
6/7/2019 3:49:40 PM 178.2 9.4
6/7/2019 3:49:41 PM 178.2 9.4
6/7/2019 3:49:42 PM 178.2 9.4
6/7/2019 3:49:43 PM 178.1 9.3
6/7/2019 3:49:44 PM 178.1 9.3
6/7/2019 3:49:45 PM 178.0 9.2
6/7/2019 3:49:46 PM 178.0 9.2
6/7/2019 3:49:47 PM 177.9 9.1
6/7/2019 3:49:48 PM 177.9 9.1
6/7/2019 3:49:49 PM 177.9 9.1
6/7/2019 3:49:50 PM 177.8 9.0
6/7/2019 3:49:51 PM 177.8 9.0
6/7/2019 3:49:52 PM 177.8 9.0
6/7/2019 3:49:53 PM 177.7 8.9
6/7/2019 3:49:54 PM 177.7 8.9
6/7/2019 3:49:55 PM 177.6 8.8
6/7/2019 3:49:56 PM 177.6 8.8
6/7/2019 3:49:57 PM 177.6 8.8
6/7/2019 3:49:58 PM 177.6 8.8
6/7/2019 3:49:59 PM 177.6 8.8
6/7/2019 3:50:00 PM 177.5 8.7
6/7/2019 3:50:01 PM 177.5 8.7
6/7/2019 3:50:02 PM 177.5 8.7
6/7/2019 3:50:03 PM 177.6 8.8
6/7/2019 3:50:04 PM 177.6 8.8
6/7/2019 3:50:05 PM 177.6 8.8
6/7/2019 3:50:06 PM 177.6 8.8
6/7/2019 3:50:07 PM 177.7 8.9
6/7/2019 3:50:08 PM 177.7 8.9
6/7/2019 3:50:09 PM 177.8 9.0
6/7/2019 3:50:10 PM 177.9 9.1
6/7/2019 3:50:11 PM 178.0 9.2
6/7/2019 3:50:12 PM 178.0 9.2
6/7/2019 3:50:13 PM 178.1 9.3
6/7/2019 3:50:14 PM 178.2 9.4
6/7/2019 3:50:15 PM 178.4 9.6
6/7/2019 3:50:16 PM 178.5 9.7
6/7/2019 3:50:17 PM 178.6 9.8
6/7/2019 3:50:18 PM 178.8 10.0
6/7/2019 3:50:19 PM 178.9 10.1
6/7/2019 3:50:20 PM 179.1 10.3
6/7/2019 3:50:21 PM 179.2 10.4
6/7/2019 3:50:22 PM 179.4 10.6
6/7/2019 3:50:23 PM 179.6 10.8
6/7/2019 3:50:24 PM 179.7 10.9
6/7/2019 3:50:25 PM 179.9 11.1
6/7/2019 3:50:26 PM 180.1 11.3
6/7/2019 3:50:27 PM 180.3 11.5
6/7/2019 3:50:28 PM 180.5 11.7
6/7/2019 3:50:29 PM 180.7 11.9
6/7/2019 3:50:30 PM 180.9 12.1
6/7/2019 3:50:31 PM 181.1 12.3
6/7/2019 3:50:32 PM 181.3 12.5
6/7/2019 3:50:33 PM 181.5 12.7
6/7/2019 3:50:34 PM 181.7 12.9
6/7/2019 3:50:35 PM 181.8 13.0
6/7/2019 3:50:36 PM 182.1 13.3
6/7/2019 3:50:37 PM 182.3 13.5
6/7/2019 3:50:38 PM 182.4 13.6
6/7/2019 3:50:39 PM 182.6 13.8
6/7/2019 3:50:40 PM 182.8 14.0
6/7/2019 3:50:41 PM 183.0 14.2
6/7/2019 3:50:42 PM 183.2 14.4
6/7/2019 3:50:43 PM 183.4 14.6
Page 362 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:50:44 PM 183.6 14.8
6/7/2019 3:50:45 PM 183.8 15.0
6/7/2019 3:50:46 PM 184.0 15.2
6/7/2019 3:50:47 PM 184.2 15.4
6/7/2019 3:50:48 PM 184.3 15.5
6/7/2019 3:50:49 PM 184.5 15.7
6/7/2019 3:50:50 PM 184.7 15.9
6/7/2019 3:50:51 PM 184.9 16.1
6/7/2019 3:50:52 PM 185.0 16.2
6/7/2019 3:50:53 PM 185.2 16.4
6/7/2019 3:50:54 PM 185.3 16.5
6/7/2019 3:50:55 PM 185.5 16.7
6/7/2019 3:50:56 PM 185.7 16.9
6/7/2019 3:50:57 PM 185.8 17.0
6/7/2019 3:50:58 PM 185.9 17.1
6/7/2019 3:50:59 PM 186.1 17.3
6/7/2019 3:51:00 PM 186.2 17.4
6/7/2019 3:51:01 PM 186.3 17.5
6/7/2019 3:51:02 PM 186.4 17.6
6/7/2019 3:51:03 PM 186.5 17.7
6/7/2019 3:51:04 PM 186.6 17.8
6/7/2019 3:51:05 PM 186.7 17.9
6/7/2019 3:51:06 PM 186.8 18.0
6/7/2019 3:51:07 PM 186.9 18.1
6/7/2019 3:51:08 PM 187.0 18.2
6/7/2019 3:51:09 PM 187.1 18.3
6/7/2019 3:51:10 PM 187.1 18.3
6/7/2019 3:51:11 PM 187.2 18.4
6/7/2019 3:51:12 PM 187.3 18.5
6/7/2019 3:51:13 PM 187.3 18.5
6/7/2019 3:51:14 PM 187.4 18.6
6/7/2019 3:51:15 PM 187.4 18.6
6/7/2019 3:51:16 PM 187.4 18.6
6/7/2019 3:51:17 PM 187.5 18.7
6/7/2019 3:51:18 PM 187.5 18.7
6/7/2019 3:51:19 PM 187.5 18.7
6/7/2019 3:51:20 PM 187.6 18.8
6/7/2019 3:51:21 PM 187.6 18.8
6/7/2019 3:51:22 PM 187.6 18.8
6/7/2019 3:51:23 PM 187.6 18.8
6/7/2019 3:51:24 PM 187.6 18.8
6/7/2019 3:51:25 PM 187.6 18.8
6/7/2019 3:51:26 PM 187.6 18.8
6/7/2019 3:51:27 PM 187.5 18.7
6/7/2019 3:51:28 PM 187.5 18.7
6/7/2019 3:51:29 PM 187.5 18.7
6/7/2019 3:51:30 PM 187.5 18.7
6/7/2019 3:51:31 PM 187.4 18.6
6/7/2019 3:51:32 PM 187.4 18.6
6/7/2019 3:51:33 PM 187.4 18.6
6/7/2019 3:51:34 PM 187.3 18.5
6/7/2019 3:51:35 PM 187.3 18.5
6/7/2019 3:51:36 PM 187.2 18.4
6/7/2019 3:51:37 PM 187.2 18.4
6/7/2019 3:51:38 PM 187.1 18.3
6/7/2019 3:51:39 PM 187.1 18.3
6/7/2019 3:51:40 PM 187.0 18.2
6/7/2019 3:51:41 PM 186.9 18.1
6/7/2019 3:51:42 PM 186.9 18.1
6/7/2019 3:51:43 PM 186.8 18.0
6/7/2019 3:51:44 PM 186.8 18.0
6/7/2019 3:51:45 PM 186.7 17.9
6/7/2019 3:51:46 PM 186.7 17.9
6/7/2019 3:51:47 PM 186.6 17.8
6/7/2019 3:51:48 PM 186.6 17.8
6/7/2019 3:51:49 PM 186.5 17.7
6/7/2019 3:51:50 PM 186.5 17.7
6/7/2019 3:51:51 PM 186.4 17.6
6/7/2019 3:51:52 PM 186.4 17.6
6/7/2019 3:51:53 PM 186.3 17.5
6/7/2019 3:51:54 PM 186.3 17.5
6/7/2019 3:51:55 PM 186.2 17.4
6/7/2019 3:51:56 PM 186.2 17.4
6/7/2019 3:51:57 PM 186.2 17.4
6/7/2019 3:51:58 PM 186.1 17.3
6/7/2019 3:51:59 PM 186.1 17.3
6/7/2019 3:52:00 PM 186.0 17.2
6/7/2019 3:52:01 PM 186.0 17.2
6/7/2019 3:52:02 PM 185.9 17.1
6/7/2019 3:52:03 PM 185.9 17.1
6/7/2019 3:52:04 PM 185.9 17.1
6/7/2019 3:52:05 PM 185.8 17.0
6/7/2019 3:52:06 PM 185.8 17.0
6/7/2019 3:52:07 PM 185.7 16.9
6/7/2019 3:52:08 PM 185.7 16.9
6/7/2019 3:52:09 PM 185.7 16.9
6/7/2019 3:52:10 PM 185.6 16.8
6/7/2019 3:52:11 PM 185.6 16.8
6/7/2019 3:52:12 PM 185.6 16.8
6/7/2019 3:52:13 PM 185.5 16.7
6/7/2019 3:52:14 PM 185.5 16.7
6/7/2019 3:52:15 PM 185.4 16.6
Page 363 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:52:16 PM 185.4 16.6
6/7/2019 3:52:17 PM 185.4 16.6
6/7/2019 3:52:18 PM 185.3 16.5
6/7/2019 3:52:19 PM 185.3 16.5
6/7/2019 3:52:20 PM 185.2 16.4
6/7/2019 3:52:21 PM 185.2 16.4
6/7/2019 3:52:22 PM 185.2 16.4
6/7/2019 3:52:23 PM 185.1 16.3
6/7/2019 3:52:24 PM 185.1 16.3
6/7/2019 3:52:25 PM 185.0 16.2
6/7/2019 3:52:26 PM 185.0 16.2
6/7/2019 3:52:27 PM 185.0 16.2
6/7/2019 3:52:28 PM 184.9 16.1
6/7/2019 3:52:29 PM 184.9 16.1
6/7/2019 3:52:30 PM 184.8 16.0
6/7/2019 3:52:31 PM 184.8 16.0
6/7/2019 3:52:32 PM 184.8 16.0
6/7/2019 3:52:33 PM 184.7 15.9
6/7/2019 3:52:34 PM 184.7 15.9
6/7/2019 3:52:35 PM 184.7 15.9
6/7/2019 3:52:36 PM 184.6 15.8
6/7/2019 3:52:37 PM 184.6 15.8
6/7/2019 3:52:38 PM 184.6 15.8
6/7/2019 3:52:39 PM 184.6 15.8
6/7/2019 3:52:40 PM 184.5 15.7
6/7/2019 3:52:41 PM 184.5 15.7
6/7/2019 3:52:42 PM 184.5 15.7
6/7/2019 3:52:43 PM 184.5 15.7
6/7/2019 3:52:44 PM 184.4 15.6
6/7/2019 3:52:45 PM 184.4 15.6
6/7/2019 3:52:46 PM 184.4 15.6
6/7/2019 3:52:47 PM 184.4 15.6
6/7/2019 3:52:48 PM 184.4 15.6
6/7/2019 3:52:49 PM 184.3 15.5
6/7/2019 3:52:50 PM 184.3 15.5
6/7/2019 3:52:51 PM 184.3 15.5
6/7/2019 3:52:52 PM 184.2 15.4
6/7/2019 3:52:53 PM 184.2 15.4
6/7/2019 3:52:54 PM 184.2 15.4
6/7/2019 3:52:55 PM 184.2 15.4
6/7/2019 3:52:56 PM 184.1 15.3
6/7/2019 3:52:57 PM 184.1 15.3
6/7/2019 3:52:58 PM 184.1 15.3
6/7/2019 3:52:59 PM 184.0 15.2
6/7/2019 3:53:00 PM 184.0 15.2
6/7/2019 3:53:01 PM 183.9 15.1
6/7/2019 3:53:02 PM 183.9 15.1
6/7/2019 3:53:03 PM 183.8 15.0
6/7/2019 3:53:04 PM 183.8 15.0
6/7/2019 3:53:05 PM 183.8 15.0
6/7/2019 3:53:06 PM 183.7 14.9
6/7/2019 3:53:07 PM 183.6 14.8
6/7/2019 3:53:08 PM 183.6 14.8
6/7/2019 3:53:09 PM 183.5 14.7
6/7/2019 3:53:10 PM 183.4 14.6
6/7/2019 3:53:11 PM 183.4 14.6
6/7/2019 3:53:12 PM 183.3 14.5
6/7/2019 3:53:13 PM 183.2 14.4
6/7/2019 3:53:14 PM 183.2 14.4
6/7/2019 3:53:15 PM 183.1 14.3
6/7/2019 3:53:16 PM 183.0 14.2
6/7/2019 3:53:17 PM 183.0 14.2
6/7/2019 3:53:18 PM 182.9 14.1
6/7/2019 3:53:19 PM 182.8 14.0
6/7/2019 3:53:20 PM 182.7 13.9
6/7/2019 3:53:21 PM 182.7 13.9
6/7/2019 3:53:22 PM 182.6 13.8
6/7/2019 3:53:23 PM 182.5 13.7
6/7/2019 3:53:24 PM 182.5 13.7
6/7/2019 3:53:25 PM 182.4 13.6
6/7/2019 3:53:26 PM 182.3 13.5
6/7/2019 3:53:27 PM 182.2 13.4
6/7/2019 3:53:28 PM 182.2 13.4
6/7/2019 3:53:29 PM 182.1 13.3
6/7/2019 3:53:30 PM 182.0 13.2
6/7/2019 3:53:31 PM 181.9 13.1
6/7/2019 3:53:32 PM 181.9 13.1
6/7/2019 3:53:33 PM 181.8 13.0
6/7/2019 3:53:34 PM 181.8 13.0
6/7/2019 3:53:35 PM 181.7 12.9
6/7/2019 3:53:36 PM 181.6 12.8
6/7/2019 3:53:37 PM 181.6 12.8
6/7/2019 3:53:38 PM 181.5 12.7
6/7/2019 3:53:39 PM 181.5 12.7
6/7/2019 3:53:40 PM 181.4 12.6
6/7/2019 3:53:41 PM 181.4 12.6
6/7/2019 3:53:42 PM 181.3 12.5
6/7/2019 3:53:43 PM 181.3 12.5
6/7/2019 3:53:44 PM 181.2 12.4
6/7/2019 3:53:45 PM 181.2 12.4
6/7/2019 3:53:46 PM 181.2 12.4
6/7/2019 3:53:47 PM 181.1 12.3
Page 364 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:53:48 PM 181.1 12.3
6/7/2019 3:53:49 PM 181.1 12.3
6/7/2019 3:53:50 PM 181.0 12.2
6/7/2019 3:53:51 PM 181.0 12.2
6/7/2019 3:53:52 PM 181.0 12.2
6/7/2019 3:53:53 PM 181.0 12.2
6/7/2019 3:53:54 PM 180.9 12.1
6/7/2019 3:53:55 PM 180.9 12.1
6/7/2019 3:53:56 PM 180.9 12.1
6/7/2019 3:53:57 PM 180.9 12.1
6/7/2019 3:53:58 PM 180.9 12.1
6/7/2019 3:53:59 PM 180.8 12.0
6/7/2019 3:54:00 PM 180.8 12.0
6/7/2019 3:54:01 PM 180.8 12.0
6/7/2019 3:54:02 PM 180.8 12.0
6/7/2019 3:54:03 PM 180.8 12.0
6/7/2019 3:54:04 PM 180.8 12.0
6/7/2019 3:54:05 PM 180.8 12.0
6/7/2019 3:54:06 PM 180.7 11.9
6/7/2019 3:54:07 PM 180.7 11.9
6/7/2019 3:54:08 PM 180.7 11.9
6/7/2019 3:54:09 PM 180.7 11.9
6/7/2019 3:54:10 PM 180.7 11.9
6/7/2019 3:54:11 PM 180.6 11.8
6/7/2019 3:54:12 PM 180.6 11.8
6/7/2019 3:54:13 PM 180.6 11.8
6/7/2019 3:54:14 PM 180.6 11.8
6/7/2019 3:54:15 PM 180.5 11.7
6/7/2019 3:54:16 PM 180.5 11.7
6/7/2019 3:54:17 PM 180.5 11.7
6/7/2019 3:54:18 PM 180.5 11.7
6/7/2019 3:54:19 PM 180.5 11.7
6/7/2019 3:54:20 PM 180.4 11.6
6/7/2019 3:54:21 PM 180.4 11.6
6/7/2019 3:54:22 PM 180.4 11.6
6/7/2019 3:54:23 PM 180.4 11.6
6/7/2019 3:54:24 PM 180.4 11.6
6/7/2019 3:54:25 PM 180.3 11.5
6/7/2019 3:54:26 PM 180.3 11.5
6/7/2019 3:54:27 PM 180.3 11.5
6/7/2019 3:54:28 PM 180.3 11.5
6/7/2019 3:54:29 PM 180.3 11.5
6/7/2019 3:54:30 PM 180.2 11.4
6/7/2019 3:54:31 PM 180.2 11.4
6/7/2019 3:54:32 PM 180.2 11.4
6/7/2019 3:54:33 PM 180.2 11.4
6/7/2019 3:54:34 PM 180.1 11.3
6/7/2019 3:54:35 PM 180.1 11.3
6/7/2019 3:54:36 PM 180.1 11.3
6/7/2019 3:54:37 PM 180.1 11.3
6/7/2019 3:54:38 PM 180.0 11.2
6/7/2019 3:54:39 PM 180.0 11.2
6/7/2019 3:54:40 PM 180.0 11.2
6/7/2019 3:54:41 PM 180.0 11.2
6/7/2019 3:54:42 PM 179.9 11.1
6/7/2019 3:54:43 PM 179.9 11.1
6/7/2019 3:54:44 PM 179.9 11.1
6/7/2019 3:54:45 PM 179.9 11.1
6/7/2019 3:54:46 PM 179.9 11.1
6/7/2019 3:54:47 PM 179.8 11.0
6/7/2019 3:54:48 PM 179.8 11.0
6/7/2019 3:54:49 PM 179.8 11.0
6/7/2019 3:54:50 PM 179.8 11.0
6/7/2019 3:54:51 PM 179.8 11.0
6/7/2019 3:54:52 PM 179.8 11.0
6/7/2019 3:54:53 PM 179.7 10.9
6/7/2019 3:54:54 PM 179.7 10.9
6/7/2019 3:54:55 PM 179.7 10.9
6/7/2019 3:54:56 PM 179.7 10.9
6/7/2019 3:54:57 PM 179.7 10.9
6/7/2019 3:54:58 PM 179.7 10.9
6/7/2019 3:54:59 PM 179.7 10.9
6/7/2019 3:55:00 PM 179.7 10.9
6/7/2019 3:55:01 PM 179.7 10.9
6/7/2019 3:55:02 PM 179.6 10.8
6/7/2019 3:55:03 PM 179.6 10.8
6/7/2019 3:55:04 PM 179.6 10.8
6/7/2019 3:55:05 PM 179.6 10.8
6/7/2019 3:55:06 PM 179.6 10.8
6/7/2019 3:55:07 PM 179.6 10.8
6/7/2019 3:55:08 PM 179.6 10.8
6/7/2019 3:55:09 PM 179.5 10.7
6/7/2019 3:55:10 PM 179.5 10.7
6/7/2019 3:55:11 PM 179.5 10.7
6/7/2019 3:55:12 PM 179.5 10.7
6/7/2019 3:55:13 PM 179.5 10.7
6/7/2019 3:55:14 PM 179.5 10.7
6/7/2019 3:55:15 PM 179.5 10.7
6/7/2019 3:55:16 PM 179.5 10.7
6/7/2019 3:55:17 PM 179.5 10.7
6/7/2019 3:55:18 PM 179.5 10.7
6/7/2019 3:55:19 PM 179.4 10.6
Page 365 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:55:20 PM 179.4 10.6
6/7/2019 3:55:21 PM 179.4 10.6
6/7/2019 3:55:22 PM 179.4 10.6
6/7/2019 3:55:23 PM 179.4 10.6
6/7/2019 3:55:24 PM 179.4 10.6
6/7/2019 3:55:25 PM 179.4 10.6
6/7/2019 3:55:26 PM 179.4 10.6
6/7/2019 3:55:27 PM 179.3 10.5
6/7/2019 3:55:28 PM 179.3 10.5
6/7/2019 3:55:29 PM 179.3 10.5
6/7/2019 3:55:30 PM 179.3 10.5
6/7/2019 3:55:31 PM 179.2 10.4
6/7/2019 3:55:32 PM 179.2 10.4
6/7/2019 3:55:33 PM 179.2 10.4
6/7/2019 3:55:34 PM 179.1 10.3
6/7/2019 3:55:35 PM 179.1 10.3
6/7/2019 3:55:36 PM 179.1 10.3
6/7/2019 3:55:37 PM 179.0 10.2
6/7/2019 3:55:38 PM 179.0 10.2
6/7/2019 3:55:39 PM 179.0 10.2
6/7/2019 3:55:40 PM 179.0 10.2
6/7/2019 3:55:41 PM 179.0 10.2
6/7/2019 3:55:42 PM 178.9 10.1
6/7/2019 3:55:43 PM 178.9 10.1
6/7/2019 3:55:44 PM 178.9 10.1
6/7/2019 3:55:45 PM 178.9 10.1
6/7/2019 3:55:46 PM 178.9 10.1
6/7/2019 3:55:47 PM 178.9 10.1
6/7/2019 3:55:48 PM 178.8 10.0
6/7/2019 3:55:49 PM 178.8 10.0
6/7/2019 3:55:50 PM 178.8 10.0
6/7/2019 3:55:51 PM 178.8 10.0
6/7/2019 3:55:52 PM 178.8 10.0
6/7/2019 3:55:53 PM 178.8 10.0
6/7/2019 3:55:54 PM 178.8 10.0
6/7/2019 3:55:55 PM 178.7 9.9
6/7/2019 3:55:56 PM 178.7 9.9
6/7/2019 3:55:57 PM 178.7 9.9
6/7/2019 3:55:58 PM 178.7 9.9
6/7/2019 3:55:59 PM 178.7 9.9
6/7/2019 3:56:00 PM 178.7 9.9
6/7/2019 3:56:01 PM 178.6 9.8
6/7/2019 3:56:02 PM 178.6 9.8
6/7/2019 3:56:03 PM 178.6 9.8
6/7/2019 3:56:04 PM 178.6 9.8
6/7/2019 3:56:05 PM 178.6 9.8
6/7/2019 3:56:06 PM 178.5 9.7
6/7/2019 3:56:07 PM 178.5 9.7
6/7/2019 3:56:08 PM 178.5 9.7
6/7/2019 3:56:09 PM 178.5 9.7
6/7/2019 3:56:10 PM 178.4 9.6
6/7/2019 3:56:11 PM 178.4 9.6
6/7/2019 3:56:12 PM 178.4 9.6
6/7/2019 3:56:13 PM 178.4 9.6
6/7/2019 3:56:14 PM 178.4 9.6
6/7/2019 3:56:15 PM 178.4 9.6
6/7/2019 3:56:16 PM 178.3 9.5
6/7/2019 3:56:17 PM 178.3 9.5
6/7/2019 3:56:18 PM 178.3 9.5
6/7/2019 3:56:19 PM 178.3 9.5
6/7/2019 3:56:20 PM 178.3 9.5
6/7/2019 3:56:21 PM 178.2 9.4
6/7/2019 3:56:22 PM 178.2 9.4
6/7/2019 3:56:23 PM 178.2 9.4
6/7/2019 3:56:24 PM 178.1 9.3
6/7/2019 3:56:25 PM 178.1 9.3
6/7/2019 3:56:26 PM 178.1 9.3
6/7/2019 3:56:27 PM 178.0 9.2
6/7/2019 3:56:28 PM 178.0 9.2
6/7/2019 3:56:29 PM 178.0 9.2
6/7/2019 3:56:30 PM 177.9 9.1
6/7/2019 3:56:31 PM 177.9 9.1
6/7/2019 3:56:32 PM 177.9 9.1
6/7/2019 3:56:33 PM 177.8 9.0
6/7/2019 3:56:34 PM 177.8 9.0
6/7/2019 3:56:35 PM 177.7 8.9
6/7/2019 3:56:36 PM 177.7 8.9
6/7/2019 3:56:37 PM 177.7 8.9
6/7/2019 3:56:38 PM 177.6 8.8
6/7/2019 3:56:39 PM 177.6 8.8
6/7/2019 3:56:40 PM 177.6 8.8
6/7/2019 3:56:41 PM 177.5 8.7
6/7/2019 3:56:42 PM 177.5 8.7
6/7/2019 3:56:43 PM 177.5 8.7
6/7/2019 3:56:44 PM 177.4 8.6
6/7/2019 3:56:45 PM 177.4 8.6
6/7/2019 3:56:46 PM 177.4 8.6
6/7/2019 3:56:47 PM 177.3 8.5
6/7/2019 3:56:48 PM 177.3 8.5
6/7/2019 3:56:49 PM 177.3 8.5
6/7/2019 3:56:50 PM 177.2 8.4
6/7/2019 3:56:51 PM 177.2 8.4
Page 366 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:56:52 PM 177.2 8.4
6/7/2019 3:56:53 PM 177.1 8.3
6/7/2019 3:56:54 PM 177.1 8.3
6/7/2019 3:56:55 PM 177.0 8.2
6/7/2019 3:56:56 PM 177.0 8.2
6/7/2019 3:56:57 PM 176.9 8.1
6/7/2019 3:56:58 PM 176.9 8.1
6/7/2019 3:56:59 PM 176.8 8.0
6/7/2019 3:57:00 PM 176.8 8.0
6/7/2019 3:57:01 PM 176.7 7.9
6/7/2019 3:57:02 PM 176.7 7.9
6/7/2019 3:57:03 PM 176.7 7.9
6/7/2019 3:57:04 PM 176.6 7.8
6/7/2019 3:57:05 PM 176.6 7.8
6/7/2019 3:57:06 PM 176.5 7.7
6/7/2019 3:57:07 PM 176.5 7.7
6/7/2019 3:57:08 PM 176.5 7.7
6/7/2019 3:57:09 PM 176.4 7.6
6/7/2019 3:57:10 PM 176.4 7.6
6/7/2019 3:57:11 PM 176.4 7.6
6/7/2019 3:57:12 PM 176.3 7.5
6/7/2019 3:57:13 PM 176.3 7.5
6/7/2019 3:57:14 PM 176.3 7.5
6/7/2019 3:57:15 PM 176.2 7.4
6/7/2019 3:57:16 PM 176.2 7.4
6/7/2019 3:57:17 PM 176.2 7.4
6/7/2019 3:57:18 PM 176.2 7.4
6/7/2019 3:57:19 PM 176.1 7.3
6/7/2019 3:57:20 PM 176.1 7.3
6/7/2019 3:57:21 PM 176.1 7.3
6/7/2019 3:57:22 PM 176.1 7.3
6/7/2019 3:57:23 PM 176.0 7.2
6/7/2019 3:57:24 PM 176.0 7.2
6/7/2019 3:57:25 PM 176.0 7.2
6/7/2019 3:57:26 PM 176.0 7.2
6/7/2019 3:57:27 PM 176.0 7.2
6/7/2019 3:57:28 PM 176.0 7.2
6/7/2019 3:57:29 PM 176.0 7.2
6/7/2019 3:57:30 PM 175.9 7.1
6/7/2019 3:57:31 PM 175.9 7.1
6/7/2019 3:57:32 PM 175.9 7.1
6/7/2019 3:57:33 PM 175.9 7.1
6/7/2019 3:57:34 PM 175.9 7.1
6/7/2019 3:57:35 PM 175.9 7.1
6/7/2019 3:57:36 PM 175.8 7.0
6/7/2019 3:57:37 PM 175.8 7.0
6/7/2019 3:57:38 PM 175.8 7.0
6/7/2019 3:57:39 PM 175.8 7.0
6/7/2019 3:57:40 PM 175.8 7.0
6/7/2019 3:57:41 PM 175.7 6.9
6/7/2019 3:57:42 PM 175.7 6.9
6/7/2019 3:57:43 PM 175.7 6.9
6/7/2019 3:57:44 PM 175.7 6.9
6/7/2019 3:57:45 PM 175.6 6.8
6/7/2019 3:57:46 PM 175.6 6.8
6/7/2019 3:57:47 PM 175.6 6.8
6/7/2019 3:57:48 PM 175.5 6.7
6/7/2019 3:57:49 PM 175.5 6.7
6/7/2019 3:57:50 PM 175.4 6.6
6/7/2019 3:57:51 PM 175.4 6.6
6/7/2019 3:57:52 PM 175.4 6.6
6/7/2019 3:57:53 PM 175.3 6.5
6/7/2019 3:57:54 PM 175.3 6.5
6/7/2019 3:57:55 PM 175.2 6.4
6/7/2019 3:57:56 PM 175.2 6.4
6/7/2019 3:57:57 PM 175.2 6.4
6/7/2019 3:57:58 PM 175.1 6.3
6/7/2019 3:57:59 PM 175.1 6.3
6/7/2019 3:58:00 PM 175.1 6.3
6/7/2019 3:58:01 PM 175.0 6.2
6/7/2019 3:58:02 PM 175.0 6.2
6/7/2019 3:58:03 PM 175.0 6.2
6/7/2019 3:58:04 PM 174.9 6.1
6/7/2019 3:58:05 PM 174.9 6.1
6/7/2019 3:58:06 PM 174.9 6.1
6/7/2019 3:58:07 PM 174.8 6.0
6/7/2019 3:58:08 PM 174.8 6.0
6/7/2019 3:58:09 PM 174.8 6.0
6/7/2019 3:58:10 PM 174.7 5.9
6/7/2019 3:58:11 PM 174.7 5.9
6/7/2019 3:58:12 PM 174.7 5.9
6/7/2019 3:58:13 PM 174.7 5.9
6/7/2019 3:58:14 PM 174.7 5.9
6/7/2019 3:58:15 PM 174.6 5.8
6/7/2019 3:58:16 PM 174.6 5.8
6/7/2019 3:58:17 PM 174.6 5.8
6/7/2019 3:58:18 PM 174.6 5.8
6/7/2019 3:58:19 PM 174.5 5.7
6/7/2019 3:58:20 PM 174.5 5.7
6/7/2019 3:58:21 PM 174.5 5.7
6/7/2019 3:58:22 PM 174.5 5.7
6/7/2019 3:58:23 PM 174.5 5.7
Page 367 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:58:24 PM 174.4 5.6
6/7/2019 3:58:25 PM 174.4 5.6
6/7/2019 3:58:26 PM 174.4 5.6
6/7/2019 3:58:27 PM 174.4 5.6
6/7/2019 3:58:28 PM 174.3 5.5
6/7/2019 3:58:29 PM 174.3 5.5
6/7/2019 3:58:30 PM 174.3 5.5
6/7/2019 3:58:31 PM 174.3 5.5
6/7/2019 3:58:32 PM 174.2 5.4
6/7/2019 3:58:33 PM 174.2 5.4
6/7/2019 3:58:34 PM 174.2 5.4
6/7/2019 3:58:35 PM 174.2 5.4
6/7/2019 3:58:36 PM 174.1 5.3
6/7/2019 3:58:37 PM 174.1 5.3
6/7/2019 3:58:38 PM 174.1 5.3
6/7/2019 3:58:39 PM 174.1 5.3
6/7/2019 3:58:40 PM 174.1 5.3
6/7/2019 3:58:41 PM 174.0 5.2
6/7/2019 3:58:42 PM 174.0 5.2
6/7/2019 3:58:43 PM 174.0 5.2
6/7/2019 3:58:44 PM 174.0 5.2
6/7/2019 3:58:45 PM 174.0 5.2
6/7/2019 3:58:46 PM 173.9 5.1
6/7/2019 3:58:47 PM 173.9 5.1
6/7/2019 3:58:48 PM 173.9 5.1
6/7/2019 3:58:49 PM 173.9 5.1
6/7/2019 3:58:50 PM 173.9 5.1
6/7/2019 3:58:51 PM 173.9 5.1
6/7/2019 3:58:52 PM 173.9 5.1
6/7/2019 3:58:53 PM 173.8 5.0
6/7/2019 3:58:54 PM 173.8 5.0
6/7/2019 3:58:55 PM 173.8 5.0
6/7/2019 3:58:56 PM 173.8 5.0
6/7/2019 3:58:57 PM 173.8 5.0
6/7/2019 3:58:58 PM 173.8 5.0
6/7/2019 3:58:59 PM 173.8 5.0
6/7/2019 3:59:00 PM 173.8 5.0
6/7/2019 3:59:01 PM 173.7 4.9
6/7/2019 3:59:02 PM 173.7 4.9
6/7/2019 3:59:03 PM 173.7 4.9
6/7/2019 3:59:04 PM 173.7 4.9
6/7/2019 3:59:05 PM 173.7 4.9
6/7/2019 3:59:06 PM 173.7 4.9
6/7/2019 3:59:07 PM 173.7 4.9
6/7/2019 3:59:08 PM 173.7 4.9
6/7/2019 3:59:09 PM 173.7 4.9
6/7/2019 3:59:10 PM 173.7 4.9
6/7/2019 3:59:11 PM 173.7 4.9
6/7/2019 3:59:12 PM 173.6 4.8
6/7/2019 3:59:13 PM 173.6 4.8
6/7/2019 3:59:14 PM 173.6 4.8
6/7/2019 3:59:15 PM 173.6 4.8
6/7/2019 3:59:16 PM 173.6 4.8
6/7/2019 3:59:17 PM 173.6 4.8
6/7/2019 3:59:18 PM 173.5 4.7
6/7/2019 3:59:19 PM 173.5 4.7
6/7/2019 3:59:20 PM 173.5 4.7
6/7/2019 3:59:21 PM 173.5 4.7
6/7/2019 3:59:22 PM 173.4 4.6
6/7/2019 3:59:23 PM 173.4 4.6
6/7/2019 3:59:24 PM 173.4 4.6
6/7/2019 3:59:25 PM 173.4 4.6
6/7/2019 3:59:26 PM 173.3 4.5
6/7/2019 3:59:27 PM 173.3 4.5
6/7/2019 3:59:28 PM 173.3 4.5
6/7/2019 3:59:29 PM 173.3 4.5
6/7/2019 3:59:30 PM 173.3 4.5
6/7/2019 3:59:31 PM 173.2 4.4
6/7/2019 3:59:32 PM 173.2 4.4
6/7/2019 3:59:33 PM 173.2 4.4
6/7/2019 3:59:34 PM 173.2 4.4
6/7/2019 3:59:35 PM 173.2 4.4
6/7/2019 3:59:36 PM 173.2 4.4
6/7/2019 3:59:37 PM 173.2 4.4
6/7/2019 3:59:38 PM 173.1 4.3
6/7/2019 3:59:39 PM 173.1 4.3
6/7/2019 3:59:40 PM 173.1 4.3
6/7/2019 3:59:41 PM 173.1 4.3
6/7/2019 3:59:42 PM 173.1 4.3
6/7/2019 3:59:43 PM 173.1 4.3
6/7/2019 3:59:44 PM 173.1 4.3
6/7/2019 3:59:45 PM 173.1 4.3
6/7/2019 3:59:46 PM 173.1 4.3
6/7/2019 3:59:47 PM 173.1 4.3
6/7/2019 3:59:48 PM 173.1 4.3
6/7/2019 3:59:49 PM 173.1 4.3
6/7/2019 3:59:50 PM 173.1 4.3
6/7/2019 3:59:51 PM 173.1 4.3
6/7/2019 3:59:52 PM 173.1 4.3
6/7/2019 3:59:53 PM 173.1 4.3
6/7/2019 3:59:54 PM 173.1 4.3
6/7/2019 3:59:55 PM 173.1 4.3
Page 368 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 3:59:56 PM 173.0 4.2
6/7/2019 3:59:57 PM 173.0 4.2
6/7/2019 3:59:58 PM 173.0 4.2
6/7/2019 3:59:59 PM 173.0 4.2
6/7/2019 4:00:00 PM 173.0 4.2
6/7/2019 4:00:01 PM 173.0 4.2
6/7/2019 4:00:02 PM 173.0 4.2
6/7/2019 4:00:03 PM 173.0 4.2
6/7/2019 4:00:04 PM 173.0 4.2
6/7/2019 4:00:05 PM 172.9 4.1
6/7/2019 4:00:06 PM 172.9 4.1
6/7/2019 4:00:07 PM 172.9 4.1
6/7/2019 4:00:08 PM 172.9 4.1
6/7/2019 4:00:09 PM 172.9 4.1
6/7/2019 4:00:10 PM 172.8 4.0
6/7/2019 4:00:11 PM 172.8 4.0
6/7/2019 4:00:12 PM 172.8 4.0
6/7/2019 4:00:13 PM 172.8 4.0
6/7/2019 4:00:14 PM 172.7 3.9
6/7/2019 4:00:15 PM 172.7 3.9
6/7/2019 4:00:16 PM 172.7 3.9
6/7/2019 4:00:17 PM 172.7 3.9
6/7/2019 4:00:18 PM 172.6 3.8
6/7/2019 4:00:19 PM 172.6 3.8
6/7/2019 4:00:20 PM 172.6 3.8
6/7/2019 4:00:21 PM 172.6 3.8
6/7/2019 4:00:22 PM 172.5 3.7
6/7/2019 4:00:23 PM 172.5 3.7
6/7/2019 4:00:24 PM 172.5 3.7
6/7/2019 4:00:25 PM 172.5 3.7
6/7/2019 4:00:26 PM 172.4 3.6
6/7/2019 4:00:27 PM 172.4 3.6
6/7/2019 4:00:28 PM 172.4 3.6
6/7/2019 4:00:29 PM 172.4 3.6
6/7/2019 4:00:30 PM 172.4 3.6
6/7/2019 4:00:31 PM 172.3 3.5
6/7/2019 4:00:32 PM 172.3 3.5
6/7/2019 4:00:33 PM 172.3 3.5
6/7/2019 4:00:34 PM 172.3 3.5
6/7/2019 4:00:35 PM 172.3 3.5
6/7/2019 4:00:36 PM 172.3 3.5
6/7/2019 4:00:37 PM 172.2 3.4
6/7/2019 4:00:38 PM 172.2 3.4
6/7/2019 4:00:39 PM 172.2 3.4
6/7/2019 4:00:40 PM 172.2 3.4
6/7/2019 4:00:41 PM 172.2 3.4
6/7/2019 4:00:42 PM 172.2 3.4
6/7/2019 4:00:43 PM 172.2 3.4
6/7/2019 4:00:44 PM 172.2 3.4
6/7/2019 4:00:45 PM 172.1 3.3
6/7/2019 4:00:46 PM 172.1 3.3
6/7/2019 4:00:47 PM 172.1 3.3
6/7/2019 4:00:48 PM 172.1 3.3
6/7/2019 4:00:49 PM 172.1 3.3
6/7/2019 4:00:50 PM 172.1 3.3
6/7/2019 4:00:51 PM 172.1 3.3
6/7/2019 4:00:52 PM 172.1 3.3
6/7/2019 4:00:53 PM 172.0 3.2
6/7/2019 4:00:54 PM 172.0 3.2
6/7/2019 4:00:55 PM 172.0 3.2
6/7/2019 4:00:56 PM 172.0 3.2
6/7/2019 4:00:57 PM 172.0 3.2
6/7/2019 4:00:58 PM 172.0 3.2
6/7/2019 4:00:59 PM 172.0 3.2
6/7/2019 4:01:00 PM 172.0 3.2
6/7/2019 4:01:01 PM 172.0 3.2
6/7/2019 4:01:02 PM 171.9 3.1
6/7/2019 4:01:03 PM 171.9 3.1
6/7/2019 4:01:04 PM 171.9 3.1
6/7/2019 4:01:05 PM 171.9 3.1
6/7/2019 4:01:06 PM 171.9 3.1
6/7/2019 4:01:07 PM 171.9 3.1
6/7/2019 4:01:08 PM 171.9 3.1
6/7/2019 4:01:09 PM 171.8 3.0
6/7/2019 4:01:10 PM 171.8 3.0
6/7/2019 4:01:11 PM 171.8 3.0
6/7/2019 4:01:12 PM 171.8 3.0
6/7/2019 4:01:13 PM 171.8 3.0
6/7/2019 4:01:14 PM 171.8 3.0
6/7/2019 4:01:15 PM 171.8 3.0
6/7/2019 4:01:16 PM 171.8 3.0
6/7/2019 4:01:17 PM 171.7 2.9
6/7/2019 4:01:18 PM 171.7 2.9
6/7/2019 4:01:19 PM 171.7 2.9
6/7/2019 4:01:20 PM 171.7 2.9
6/7/2019 4:01:21 PM 171.7 2.9
6/7/2019 4:01:22 PM 171.7 2.9
6/7/2019 4:01:23 PM 171.7 2.9
6/7/2019 4:01:24 PM 171.7 2.9
6/7/2019 4:01:25 PM 171.7 2.9
6/7/2019 4:01:26 PM 171.6 2.8
6/7/2019 4:01:27 PM 171.6 2.8
Page 369 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 4:01:28 PM 171.6 2.8
6/7/2019 4:01:29 PM 171.6 2.8
6/7/2019 4:01:30 PM 171.6 2.8
6/7/2019 4:01:31 PM 171.6 2.8
6/7/2019 4:01:32 PM 171.6 2.8
6/7/2019 4:01:33 PM 171.5 2.7
6/7/2019 4:01:34 PM 171.5 2.7
6/7/2019 4:01:35 PM 171.5 2.7
6/7/2019 4:01:36 PM 171.5 2.7
6/7/2019 4:01:37 PM 171.5 2.7
6/7/2019 4:01:38 PM 171.5 2.7
6/7/2019 4:01:38 PM 171.4 0.0
6/7/2019 4:01:39 PM 171.4 2.6
6/7/2019 4:01:40 PM 171.4 2.6
6/7/2019 4:01:41 PM 171.4 2.6
6/7/2019 4:01:42 PM 171.4 2.6
6/7/2019 4:01:43 PM 171.4 2.6
6/7/2019 4:01:44 PM 171.3 2.5
6/7/2019 4:01:45 PM 171.3 2.5
6/7/2019 4:01:46 PM 171.3 2.5
6/7/2019 4:01:47 PM 171.3 2.5
6/7/2019 4:01:48 PM 171.3 2.5
6/7/2019 4:01:49 PM 171.3 2.5
6/7/2019 4:01:50 PM 171.2 2.4
6/7/2019 4:01:51 PM 171.2 2.4
6/7/2019 4:01:52 PM 171.2 2.4
6/7/2019 4:01:53 PM 171.2 2.4
6/7/2019 4:01:54 PM 171.2 2.4
6/7/2019 4:01:55 PM 171.2 2.4
6/7/2019 4:01:56 PM 171.2 2.4
6/7/2019 4:01:57 PM 171.1 2.3
6/7/2019 4:01:58 PM 171.1 2.3
6/7/2019 4:01:59 PM 171.1 2.3
6/7/2019 4:02:00 PM 171.1 2.3
6/7/2019 4:02:01 PM 171.1 2.3
6/7/2019 4:02:02 PM 171.1 2.3
6/7/2019 4:02:03 PM 171.1 2.3
6/7/2019 4:02:04 PM 171.1 2.3
6/7/2019 4:02:05 PM 171.1 2.3
6/7/2019 4:02:06 PM 171.1 2.3
6/7/2019 4:02:07 PM 171.1 2.3
6/7/2019 4:02:08 PM 171.1 2.3
6/7/2019 4:02:09 PM 171.2 2.4
6/7/2019 4:02:10 PM 171.2 2.4
6/7/2019 4:02:11 PM 171.2 2.4
6/7/2019 4:02:12 PM 171.2 2.4
6/7/2019 4:02:13 PM 171.2 2.4
6/7/2019 4:02:14 PM 171.2 2.4
6/7/2019 4:02:15 PM 171.2 2.4
6/7/2019 4:02:16 PM 171.2 2.4
6/7/2019 4:02:17 PM 171.2 2.4
6/7/2019 4:02:18 PM 171.2 2.4
6/7/2019 4:02:19 PM 171.2 2.4
6/7/2019 4:02:20 PM 171.2 2.4
6/7/2019 4:02:21 PM 171.2 2.4
6/7/2019 4:02:22 PM 171.2 2.4
6/7/2019 4:02:23 PM 171.2 2.4
6/7/2019 4:02:24 PM 171.2 2.4
6/7/2019 4:02:25 PM 171.2 2.4
6/7/2019 4:02:26 PM 171.2 2.4
6/7/2019 4:02:27 PM 171.2 2.4
6/7/2019 4:02:28 PM 171.2 2.4
6/7/2019 4:02:29 PM 171.2 2.4
6/7/2019 4:02:30 PM 171.2 2.4
6/7/2019 4:02:31 PM 171.2 2.4
6/7/2019 4:02:32 PM 171.2 2.4
6/7/2019 4:02:33 PM 171.2 2.4
6/7/2019 4:02:34 PM 171.1 2.3
6/7/2019 4:02:35 PM 171.2 2.4
6/7/2019 4:02:36 PM 171.1 2.3
6/7/2019 4:02:37 PM 171.1 2.3
6/7/2019 4:02:38 PM 171.1 2.3
6/7/2019 4:02:39 PM 171.1 2.3
6/7/2019 4:02:40 PM 171.1 2.3
6/7/2019 4:02:41 PM 171.1 2.3
6/7/2019 4:02:42 PM 171.1 2.3
6/7/2019 4:02:43 PM 171.1 2.3
6/7/2019 4:02:44 PM 171.1 2.3
6/7/2019 4:02:45 PM 171.1 2.3
6/7/2019 4:02:46 PM 171.1 2.3
6/7/2019 4:02:47 PM 171.1 2.3
6/7/2019 4:02:48 PM 171.1 2.3
6/7/2019 4:02:49 PM 171.1 2.3
6/7/2019 4:02:50 PM 171.1 2.3
6/7/2019 4:02:51 PM 171.1 2.3
6/7/2019 4:02:52 PM 171.0 2.2
6/7/2019 4:02:53 PM 171.0 2.2
6/7/2019 4:02:54 PM 171.0 2.2
6/7/2019 4:02:55 PM 171.0 2.2
6/7/2019 4:02:56 PM 171.0 2.2
6/7/2019 4:02:57 PM 171.0 2.2
6/7/2019 4:02:58 PM 171.0 2.2
Page 370 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 4:02:59 PM 171.0 2.2
6/7/2019 4:03:00 PM 171.0 2.2
6/7/2019 4:03:01 PM 171.0 2.2
6/7/2019 4:03:02 PM 171.0 2.2
6/7/2019 4:03:03 PM 171.0 2.2
6/7/2019 4:03:04 PM 171.0 2.2
6/7/2019 4:03:05 PM 171.0 2.2
6/7/2019 4:03:06 PM 171.0 2.2
6/7/2019 4:03:07 PM 171.0 2.2
6/7/2019 4:03:08 PM 171.1 2.3
6/7/2019 4:03:09 PM 171.1 2.3
6/7/2019 4:03:10 PM 171.1 2.3
6/7/2019 4:03:11 PM 171.1 2.3
6/7/2019 4:03:12 PM 171.1 2.3
6/7/2019 4:03:13 PM 171.1 2.3
6/7/2019 4:03:14 PM 171.1 2.3
6/7/2019 4:03:15 PM 171.1 2.3
6/7/2019 4:03:16 PM 171.2 2.4
6/7/2019 4:03:17 PM 171.2 2.4
6/7/2019 4:03:18 PM 171.2 2.4
6/7/2019 4:03:19 PM 171.2 2.4
6/7/2019 4:03:20 PM 171.2 2.4
6/7/2019 4:03:21 PM 171.2 2.4
6/7/2019 4:03:22 PM 171.3 2.5
6/7/2019 4:03:23 PM 171.3 2.5
6/7/2019 4:03:24 PM 171.3 2.5
6/7/2019 4:03:25 PM 171.3 2.5
6/7/2019 4:03:26 PM 171.3 2.5
6/7/2019 4:03:27 PM 171.3 2.5
6/7/2019 4:03:28 PM 171.3 2.5
6/7/2019 4:03:29 PM 171.3 2.5
6/7/2019 4:03:30 PM 171.3 2.5
6/7/2019 4:03:31 PM 171.3 2.5
6/7/2019 4:03:32 PM 171.3 2.5
6/7/2019 4:03:33 PM 171.3 2.5
6/7/2019 4:03:34 PM 171.3 2.5
6/7/2019 4:03:35 PM 171.3 2.5
6/7/2019 4:03:36 PM 171.3 2.5
6/7/2019 4:03:37 PM 171.3 2.5
6/7/2019 4:03:38 PM 171.3 2.5
6/7/2019 4:03:39 PM 171.2 2.4
6/7/2019 4:03:40 PM 171.2 2.4
6/7/2019 4:03:41 PM 171.2 2.4
6/7/2019 4:03:42 PM 171.2 2.4
6/7/2019 4:03:43 PM 171.2 2.4
6/7/2019 4:03:44 PM 171.1 2.3
6/7/2019 4:03:45 PM 171.1 2.3
6/7/2019 4:03:46 PM 171.1 2.3
6/7/2019 4:03:47 PM 171.1 2.3
6/7/2019 4:03:48 PM 171.0 2.2
6/7/2019 4:03:49 PM 171.0 2.2
6/7/2019 4:03:50 PM 171.0 2.2
6/7/2019 4:03:51 PM 170.9 2.1
6/7/2019 4:03:52 PM 170.9 2.1
6/7/2019 4:03:53 PM 170.8 2.0
6/7/2019 4:03:54 PM 170.8 2.0
6/7/2019 4:03:55 PM 170.8 2.0
6/7/2019 4:03:56 PM 170.7 1.9
6/7/2019 4:03:57 PM 170.7 1.9
6/7/2019 4:03:58 PM 170.6 1.8
6/7/2019 4:03:59 PM 170.6 1.8
6/7/2019 4:04:00 PM 170.5 1.7
6/7/2019 4:04:01 PM 170.5 1.7
6/7/2019 4:04:02 PM 170.4 1.6
6/7/2019 4:04:03 PM 170.4 1.6
6/7/2019 4:04:04 PM 170.3 1.5
6/7/2019 4:04:05 PM 170.3 1.5
6/7/2019 4:04:06 PM 170.2 1.4
6/7/2019 4:04:07 PM 170.2 1.4
6/7/2019 4:04:08 PM 170.1 1.3
6/7/2019 4:04:09 PM 170.1 1.3
6/7/2019 4:04:10 PM 170.1 1.3
6/7/2019 4:04:11 PM 170.0 1.2
6/7/2019 4:04:12 PM 170.0 1.2
6/7/2019 4:04:13 PM 169.9 1.1
6/7/2019 4:04:14 PM 169.9 1.1
6/7/2019 4:04:15 PM 169.8 1.0
6/7/2019 4:04:16 PM 169.8 1.0
6/7/2019 4:04:17 PM 169.8 1.0
6/7/2019 4:04:18 PM 169.7 0.9
6/7/2019 4:04:19 PM 169.7 0.9
6/7/2019 4:04:20 PM 169.7 0.9
6/7/2019 4:04:21 PM 169.6 0.8
6/7/2019 4:04:22 PM 169.6 0.8
6/7/2019 4:04:23 PM 169.6 0.8
6/7/2019 4:04:24 PM 169.6 0.8
6/7/2019 4:04:25 PM 169.5 0.7
6/7/2019 4:04:26 PM 169.5 0.7
6/7/2019 4:04:27 PM 169.5 0.7
6/7/2019 4:04:28 PM 169.5 0.7
6/7/2019 4:04:29 PM 169.5 0.7
6/7/2019 4:04:30 PM 169.5 0.7
Page 371 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 4:04:31 PM 169.4 0.6
6/7/2019 4:04:32 PM 169.4 0.6
6/7/2019 4:04:33 PM 169.4 0.6
6/7/2019 4:04:34 PM 169.4 0.6
6/7/2019 4:04:35 PM 169.4 0.6
6/7/2019 4:04:36 PM 169.4 0.6
6/7/2019 4:04:37 PM 169.4 0.6
6/7/2019 4:04:38 PM 169.4 0.6
6/7/2019 4:04:39 PM 169.4 0.6
6/7/2019 4:04:40 PM 169.4 0.6
6/7/2019 4:04:41 PM 169.4 0.6
6/7/2019 4:04:42 PM 169.4 0.6
6/7/2019 4:04:43 PM 169.4 0.6
6/7/2019 4:04:44 PM 169.4 0.6
6/7/2019 4:04:45 PM 169.4 0.6
6/7/2019 4:04:46 PM 169.4 0.6
6/7/2019 4:04:47 PM 169.4 0.6
6/7/2019 4:04:48 PM 169.4 0.6
6/7/2019 4:04:49 PM 169.5 0.7
6/7/2019 4:04:50 PM 169.5 0.7
6/7/2019 4:04:51 PM 169.5 0.7
6/7/2019 4:04:52 PM 169.5 0.7
6/7/2019 4:04:53 PM 169.5 0.7
6/7/2019 4:04:54 PM 169.5 0.7
6/7/2019 4:04:55 PM 169.5 0.7
6/7/2019 4:04:56 PM 169.5 0.7
6/7/2019 4:04:57 PM 169.5 0.7
6/7/2019 4:04:58 PM 169.5 0.7
6/7/2019 4:04:59 PM 169.5 0.7
6/7/2019 4:05:00 PM 169.5 0.7
6/7/2019 4:05:01 PM 169.5 0.7
6/7/2019 4:05:02 PM 169.5 0.7
6/7/2019 4:05:03 PM 169.5 0.7
6/7/2019 4:05:04 PM 169.4 0.6
6/7/2019 4:05:05 PM 169.4 0.6
6/7/2019 4:05:06 PM 169.4 0.6
6/7/2019 4:05:07 PM 169.4 0.6
6/7/2019 4:05:08 PM 169.4 0.6
6/7/2019 4:05:09 PM 169.4 0.6
6/7/2019 4:05:10 PM 169.4 0.6
6/7/2019 4:05:11 PM 169.4 0.6
6/7/2019 4:05:12 PM 169.4 0.6
6/7/2019 4:05:13 PM 169.4 0.6
6/7/2019 4:05:14 PM 169.4 0.6
6/7/2019 4:05:15 PM 169.4 0.6
6/7/2019 4:05:16 PM 169.4 0.6
6/7/2019 4:05:17 PM 169.4 0.6
6/7/2019 4:05:18 PM 169.4 0.6
6/7/2019 4:05:19 PM 169.4 0.6
6/7/2019 4:05:20 PM 169.4 0.6
6/7/2019 4:05:21 PM 169.4 0.6
6/7/2019 4:05:22 PM 169.4 0.6
6/7/2019 4:05:23 PM 169.4 0.6
6/7/2019 4:05:24 PM 169.4 0.6
6/7/2019 4:05:25 PM 169.4 0.6
6/7/2019 4:05:26 PM 169.4 0.6
6/7/2019 4:05:27 PM 169.4 0.6
6/7/2019 4:05:28 PM 169.4 0.6
6/7/2019 4:05:29 PM 169.4 0.6
6/7/2019 4:05:30 PM 169.4 0.6
6/7/2019 4:05:31 PM 169.3 0.5
6/7/2019 4:05:32 PM 169.3 0.5
6/7/2019 4:05:33 PM 169.3 0.5
6/7/2019 4:05:34 PM 169.3 0.5
6/7/2019 4:05:35 PM 169.2 0.4
6/7/2019 4:05:36 PM 169.2 0.4
6/7/2019 4:05:37 PM 169.2 0.4
6/7/2019 4:05:38 PM 169.1 0.3
6/7/2019 4:05:39 PM 169.1 0.3
6/7/2019 4:05:40 PM 169.1 0.3
6/7/2019 4:05:41 PM 169.0 0.2
6/7/2019 4:05:42 PM 169.0 0.2
6/7/2019 4:05:43 PM 168.9 0.1
6/7/2019 4:05:44 PM 168.9 0.1
6/7/2019 4:05:45 PM 168.9 0.1
6/7/2019 4:05:46 PM 168.8 0.0
6/7/2019 4:05:47 PM 168.8 0.0
6/7/2019 4:05:48 PM 168.7 -0.1
6/7/2019 4:05:49 PM 168.7 -0.1
6/7/2019 4:05:50 PM 168.6 -0.2
6/7/2019 4:05:51 PM 168.6 -0.2
6/7/2019 4:05:52 PM 168.6 -0.2
6/7/2019 4:05:53 PM 168.5 -0.3
6/7/2019 4:05:54 PM 168.5 -0.3
6/7/2019 4:05:55 PM 168.4 -0.4
6/7/2019 4:05:56 PM 168.4 -0.4
6/7/2019 4:05:57 PM 168.3 -0.5
6/7/2019 4:05:58 PM 168.3 -0.5
6/7/2019 4:05:59 PM 168.2 -0.6
6/7/2019 4:06:00 PM 168.2 -0.6
6/7/2019 4:06:01 PM 168.2 -0.6
6/7/2019 4:06:02 PM 168.1 -0.7
Page 372 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 4:06:03 PM 168.1 -0.7
6/7/2019 4:06:04 PM 168.1 -0.7
6/7/2019 4:06:05 PM 168.0 -0.8
6/7/2019 4:06:06 PM 168.0 -0.8
6/7/2019 4:06:07 PM 168.0 -0.8
6/7/2019 4:06:08 PM 167.9 -0.9
6/7/2019 4:06:09 PM 167.9 -0.9
6/7/2019 4:06:10 PM 167.9 -0.9
6/7/2019 4:06:11 PM 167.8 -1.0
6/7/2019 4:06:12 PM 167.8 -1.0
6/7/2019 4:06:13 PM 167.8 -1.0
6/7/2019 4:06:14 PM 167.8 -1.0
6/7/2019 4:06:15 PM 167.8 -1.0
6/7/2019 4:06:16 PM 167.8 -1.0
6/7/2019 4:06:17 PM 167.8 -1.0
6/7/2019 4:06:18 PM 167.8 -1.0
6/7/2019 4:06:19 PM 167.8 -1.0
6/7/2019 4:06:20 PM 167.7 -1.1
6/7/2019 4:06:21 PM 167.7 -1.1
6/7/2019 4:06:22 PM 167.8 -1.0
6/7/2019 4:06:23 PM 167.8 -1.0
6/7/2019 4:06:24 PM 167.8 -1.0
6/7/2019 4:06:25 PM 167.8 -1.0
6/7/2019 4:06:26 PM 167.8 -1.0
6/7/2019 4:06:27 PM 167.8 -1.0
6/7/2019 4:06:28 PM 167.8 -1.0
6/7/2019 4:06:29 PM 167.8 -1.0
6/7/2019 4:06:30 PM 167.8 -1.0
6/7/2019 4:06:31 PM 167.9 -0.9
6/7/2019 4:06:32 PM 167.9 -0.9
6/7/2019 4:06:33 PM 167.9 -0.9
6/7/2019 4:06:34 PM 167.9 -0.9
6/7/2019 4:06:35 PM 167.9 -0.9
6/7/2019 4:06:36 PM 167.9 -0.9
6/7/2019 4:06:37 PM 168.0 -0.8
6/7/2019 4:06:38 PM 168.0 -0.8
6/7/2019 4:06:39 PM 168.0 -0.8
6/7/2019 4:06:40 PM 168.0 -0.8
6/7/2019 4:06:41 PM 168.1 -0.7
6/7/2019 4:06:42 PM 168.1 -0.7
6/7/2019 4:06:43 PM 168.1 -0.7
6/7/2019 4:06:44 PM 168.1 -0.7
6/7/2019 4:06:45 PM 168.1 -0.7
6/7/2019 4:06:46 PM 168.1 -0.7
6/7/2019 4:06:47 PM 168.2 -0.6
6/7/2019 4:06:48 PM 168.2 -0.6
6/7/2019 4:06:49 PM 168.2 -0.6
6/7/2019 4:06:50 PM 168.2 -0.6
6/7/2019 4:06:51 PM 168.2 -0.6
6/7/2019 4:06:52 PM 168.2 -0.6
6/7/2019 4:06:53 PM 168.2 -0.6
6/7/2019 4:06:54 PM 168.2 -0.6
6/7/2019 4:06:55 PM 168.2 -0.6
6/7/2019 4:06:56 PM 168.3 -0.5
6/7/2019 4:06:57 PM 168.3 -0.5
6/7/2019 4:06:58 PM 168.3 -0.5
6/7/2019 4:06:59 PM 168.3 -0.5
6/7/2019 4:07:00 PM 168.3 -0.5
6/7/2019 4:07:01 PM 168.3 -0.5
6/7/2019 4:07:02 PM 168.3 -0.5
6/7/2019 4:07:03 PM 168.4 -0.4
6/7/2019 4:07:04 PM 168.4 -0.4
6/7/2019 4:07:05 PM 168.4 -0.4
6/7/2019 4:07:06 PM 168.4 -0.4
6/7/2019 4:07:07 PM 168.4 -0.4
6/7/2019 4:07:08 PM 168.4 -0.4
6/7/2019 4:07:09 PM 168.4 -0.4
6/7/2019 4:07:10 PM 168.4 -0.4
6/7/2019 4:07:11 PM 168.4 -0.4
6/7/2019 4:07:12 PM 168.5 -0.3
6/7/2019 4:07:13 PM 168.5 -0.3
6/7/2019 4:07:14 PM 168.5 -0.3
6/7/2019 4:07:15 PM 168.5 -0.3
6/7/2019 4:07:16 PM 168.5 -0.3
6/7/2019 4:07:17 PM 168.5 -0.3
6/7/2019 4:07:18 PM 168.5 -0.3
6/7/2019 4:07:19 PM 168.5 -0.3
6/7/2019 4:07:20 PM 168.5 -0.3
6/7/2019 4:07:21 PM 168.5 -0.3
6/7/2019 4:07:22 PM 168.5 -0.3
6/7/2019 4:07:23 PM 168.5 -0.3
6/7/2019 4:07:24 PM 168.4 -0.4
6/7/2019 4:07:25 PM 168.4 -0.4
6/7/2019 4:07:26 PM 168.4 -0.4
6/7/2019 4:07:27 PM 168.4 -0.4
6/7/2019 4:07:28 PM 168.4 -0.4
6/7/2019 4:07:29 PM 168.4 -0.4
6/7/2019 4:07:30 PM 168.4 -0.4
6/7/2019 4:07:31 PM 168.4 -0.4
6/7/2019 4:07:32 PM 168.4 -0.4
6/7/2019 4:07:33 PM 168.4 -0.4
6/7/2019 4:07:34 PM 168.4 -0.4
Page 373 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 4:07:35 PM 168.4 -0.4
6/7/2019 4:07:36 PM 168.4 -0.4
6/7/2019 4:07:37 PM 168.4 -0.4
6/7/2019 4:07:38 PM 168.3 -0.5
6/7/2019 4:07:39 PM 168.3 -0.5
6/7/2019 4:07:40 PM 168.3 -0.5
6/7/2019 4:07:41 PM 168.3 -0.5
6/7/2019 4:07:42 PM 168.3 -0.5
6/7/2019 4:07:43 PM 168.3 -0.5
6/7/2019 4:07:44 PM 168.3 -0.5
6/7/2019 4:07:45 PM 168.3 -0.5
6/7/2019 4:07:46 PM 168.2 -0.6
6/7/2019 4:07:47 PM 168.2 -0.6
6/7/2019 4:07:48 PM 168.2 -0.6
6/7/2019 4:07:49 PM 168.2 -0.6
6/7/2019 4:07:50 PM 168.2 -0.6
6/7/2019 4:07:51 PM 168.2 -0.6
6/7/2019 4:07:52 PM 168.1 -0.7
6/7/2019 4:07:53 PM 168.1 -0.7
6/7/2019 4:07:54 PM 168.1 -0.7
6/7/2019 4:07:55 PM 168.1 -0.7
6/7/2019 4:07:56 PM 168.1 -0.7
6/7/2019 4:07:57 PM 168.1 -0.7
6/7/2019 4:07:58 PM 168.1 -0.7
6/7/2019 4:07:59 PM 168.0 -0.8
6/7/2019 4:08:00 PM 168.0 -0.8
6/7/2019 4:08:01 PM 168.0 -0.8
6/7/2019 4:08:02 PM 168.0 -0.8
6/7/2019 4:08:03 PM 168.0 -0.8
6/7/2019 4:08:04 PM 168.0 -0.8
6/7/2019 4:08:05 PM 168.0 -0.8
6/7/2019 4:08:06 PM 168.0 -0.8
6/7/2019 4:08:07 PM 168.0 -0.8
6/7/2019 4:08:08 PM 168.0 -0.8
6/7/2019 4:08:09 PM 168.0 -0.8
6/7/2019 4:08:10 PM 168.0 -0.8
6/7/2019 4:08:11 PM 168.0 -0.8
6/7/2019 4:08:12 PM 168.0 -0.8
6/7/2019 4:08:13 PM 168.0 -0.8
6/7/2019 4:08:14 PM 168.0 -0.8
6/7/2019 4:08:15 PM 168.0 -0.8
6/7/2019 4:08:16 PM 168.0 -0.8
6/7/2019 4:08:17 PM 168.0 -0.8
6/7/2019 4:08:18 PM 168.1 -0.7
6/7/2019 4:08:19 PM 168.1 -0.7
6/7/2019 4:08:20 PM 168.1 -0.7
6/7/2019 4:08:21 PM 168.1 -0.7
6/7/2019 4:08:22 PM 168.1 -0.7
6/7/2019 4:08:23 PM 168.1 -0.7
6/7/2019 4:08:24 PM 168.1 -0.7
6/7/2019 4:08:25 PM 168.1 -0.7
6/7/2019 4:08:26 PM 168.2 -0.6
6/7/2019 4:08:27 PM 168.2 -0.6
6/7/2019 4:08:28 PM 168.2 -0.6
6/7/2019 4:08:29 PM 168.2 -0.6
6/7/2019 4:08:30 PM 168.2 -0.6
6/7/2019 4:08:31 PM 168.2 -0.6
6/7/2019 4:08:32 PM 168.2 -0.6
6/7/2019 4:08:33 PM 168.2 -0.6
6/7/2019 4:08:34 PM 168.2 -0.6
6/7/2019 4:08:35 PM 168.2 -0.6
6/7/2019 4:08:36 PM 168.2 -0.6
6/7/2019 4:08:37 PM 168.2 -0.6
6/7/2019 4:08:38 PM 168.2 -0.6
6/7/2019 4:08:39 PM 168.2 -0.6
6/7/2019 4:08:40 PM 168.2 -0.6
6/7/2019 4:08:41 PM 168.3 -0.5
6/7/2019 4:08:42 PM 168.3 -0.5
6/7/2019 4:08:43 PM 168.3 -0.5
6/7/2019 4:08:44 PM 168.3 -0.5
6/7/2019 4:08:45 PM 168.3 -0.5
6/7/2019 4:08:46 PM 168.3 -0.5
6/7/2019 4:08:47 PM 168.3 -0.5
6/7/2019 4:08:48 PM 168.2 -0.6
6/7/2019 4:08:49 PM 168.2 -0.6
6/7/2019 4:08:50 PM 168.2 -0.6
6/7/2019 4:08:51 PM 168.2 -0.6
6/7/2019 4:08:52 PM 168.2 -0.6
6/7/2019 4:08:53 PM 168.2 -0.6
6/7/2019 4:08:54 PM 168.2 -0.6
6/7/2019 4:08:55 PM 168.1 -0.7
6/7/2019 4:08:56 PM 168.1 -0.7
6/7/2019 4:08:57 PM 168.1 -0.7
6/7/2019 4:08:58 PM 168.1 -0.7
6/7/2019 4:08:59 PM 168.0 -0.8
6/7/2019 4:09:00 PM 168.0 -0.8
6/7/2019 4:09:01 PM 168.0 -0.8
6/7/2019 4:09:02 PM 167.9 -0.9
6/7/2019 4:09:03 PM 167.9 -0.9
6/7/2019 4:09:04 PM 167.8 -1.0
6/7/2019 4:09:05 PM 167.8 -1.0
6/7/2019 4:09:06 PM 167.8 -1.0
Page 374 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 4:09:07 PM 167.7 -1.1
6/7/2019 4:09:08 PM 167.7 -1.1
6/7/2019 4:09:09 PM 167.7 -1.1
6/7/2019 4:09:10 PM 167.6 -1.2
6/7/2019 4:09:11 PM 167.6 -1.2
6/7/2019 4:09:12 PM 167.6 -1.2
6/7/2019 4:09:13 PM 167.5 -1.3
6/7/2019 4:09:14 PM 167.5 -1.3
6/7/2019 4:09:15 PM 167.5 -1.3
6/7/2019 4:09:16 PM 167.4 -1.4
6/7/2019 4:09:17 PM 167.4 -1.4
6/7/2019 4:09:18 PM 167.4 -1.4
6/7/2019 4:09:19 PM 167.3 -1.5
6/7/2019 4:09:20 PM 167.3 -1.5
6/7/2019 4:09:21 PM 167.2 -1.6
6/7/2019 4:09:22 PM 167.2 -1.6
6/7/2019 4:09:23 PM 167.2 -1.6
6/7/2019 4:09:24 PM 167.1 -1.7
6/7/2019 4:09:25 PM 167.1 -1.7
6/7/2019 4:09:26 PM 167.1 -1.7
6/7/2019 4:09:27 PM 167.1 -1.7
6/7/2019 4:09:28 PM 167.0 -1.8
6/7/2019 4:09:29 PM 167.0 -1.8
6/7/2019 4:09:30 PM 167.0 -1.8
6/7/2019 4:09:31 PM 167.0 -1.8
6/7/2019 4:09:32 PM 166.9 -1.9
6/7/2019 4:09:33 PM 166.9 -1.9
6/7/2019 4:09:34 PM 166.9 -1.9
6/7/2019 4:09:35 PM 166.9 -1.9
6/7/2019 4:09:36 PM 166.8 -2.0
6/7/2019 4:09:37 PM 166.8 -2.0
6/7/2019 4:09:38 PM 166.8 -2.0
6/7/2019 4:09:39 PM 166.8 -2.0
6/7/2019 4:09:40 PM 166.8 -2.0
6/7/2019 4:09:41 PM 166.8 -2.0
6/7/2019 4:09:42 PM 166.8 -2.0
6/7/2019 4:09:43 PM 166.8 -2.0
6/7/2019 4:09:44 PM 166.8 -2.0
6/7/2019 4:09:45 PM 166.8 -2.0
6/7/2019 4:09:46 PM 166.8 -2.0
6/7/2019 4:09:47 PM 166.8 -2.0
6/7/2019 4:09:48 PM 166.8 -2.0
6/7/2019 4:09:49 PM 166.8 -2.0
6/7/2019 4:09:50 PM 166.8 -2.0
6/7/2019 4:09:51 PM 166.8 -2.0
6/7/2019 4:09:52 PM 166.8 -2.0
6/7/2019 4:09:53 PM 166.8 -2.0
6/7/2019 4:09:54 PM 166.8 -2.0
6/7/2019 4:09:55 PM 166.8 -2.0
6/7/2019 4:09:56 PM 166.8 -2.0
6/7/2019 4:09:57 PM 166.8 -2.0
6/7/2019 4:09:58 PM 166.8 -2.0
6/7/2019 4:09:59 PM 166.8 -2.0
6/7/2019 4:10:00 PM 166.8 -2.0
6/7/2019 4:10:01 PM 166.8 -2.0
6/7/2019 4:10:02 PM 166.8 -2.0
6/7/2019 4:10:03 PM 166.8 -2.0
6/7/2019 4:10:04 PM 166.8 -2.0
6/7/2019 4:10:05 PM 166.8 -2.0
6/7/2019 4:10:06 PM 166.8 -2.0
6/7/2019 4:10:07 PM 166.8 -2.0
6/7/2019 4:10:08 PM 166.8 -2.0
6/7/2019 4:10:09 PM 166.8 -2.0
6/7/2019 4:10:10 PM 166.8 -2.0
6/7/2019 4:10:11 PM 166.8 -2.0
6/7/2019 4:10:12 PM 166.8 -2.0
6/7/2019 4:10:13 PM 166.8 -2.0
6/7/2019 4:10:14 PM 166.8 -2.0
6/7/2019 4:10:15 PM 166.8 -2.0
6/7/2019 4:10:16 PM 166.8 -2.0
6/7/2019 4:10:17 PM 166.8 -2.0
6/7/2019 4:10:18 PM 166.8 -2.0
6/7/2019 4:10:19 PM 166.8 -2.0
6/7/2019 4:10:20 PM 166.8 -2.0
6/7/2019 4:10:21 PM 166.8 -2.0
6/7/2019 4:10:22 PM 166.8 -2.0
6/7/2019 4:10:23 PM 166.8 -2.0
6/7/2019 4:10:24 PM 166.8 -2.0
6/7/2019 4:10:25 PM 166.8 -2.0
6/7/2019 4:10:26 PM 166.8 -2.0
6/7/2019 4:10:27 PM 166.8 -2.0
6/7/2019 4:10:28 PM 166.8 -2.0
6/7/2019 4:10:29 PM 166.7 -2.1
6/7/2019 4:10:30 PM 166.7 -2.1
6/7/2019 4:10:31 PM 166.7 -2.1
6/7/2019 4:10:32 PM 166.7 -2.1
6/7/2019 4:10:33 PM 166.7 -2.1
6/7/2019 4:10:34 PM 166.7 -2.1
6/7/2019 4:10:35 PM 166.6 -2.2
6/7/2019 4:10:36 PM 166.6 -2.2
6/7/2019 4:10:37 PM 166.6 -2.2
6/7/2019 4:10:38 PM 166.6 -2.2
Page 375 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 4:10:39 PM 166.6 -2.2
6/7/2019 4:10:40 PM 166.5 -2.3
6/7/2019 4:10:41 PM 166.5 -2.3
6/7/2019 4:10:42 PM 166.5 -2.3
6/7/2019 4:10:43 PM 166.5 -2.3
6/7/2019 4:10:44 PM 166.5 -2.3
6/7/2019 4:10:45 PM 166.5 -2.3
6/7/2019 4:10:46 PM 166.5 -2.3
6/7/2019 4:10:47 PM 166.5 -2.3
6/7/2019 4:10:48 PM 166.5 -2.3
6/7/2019 4:10:49 PM 166.4 -2.4
6/7/2019 4:10:50 PM 166.4 -2.4
6/7/2019 4:10:51 PM 166.4 -2.4
6/7/2019 4:10:52 PM 166.4 -2.4
6/7/2019 4:10:53 PM 166.4 -2.4
6/7/2019 4:10:54 PM 166.4 -2.4
6/7/2019 4:10:55 PM 166.4 -2.4
6/7/2019 4:10:56 PM 166.4 -2.4
6/7/2019 4:10:57 PM 166.4 -2.4
6/7/2019 4:10:58 PM 166.4 -2.4
6/7/2019 4:10:59 PM 166.4 -2.4
6/7/2019 4:11:00 PM 166.4 -2.4
6/7/2019 4:11:01 PM 166.4 -2.4
6/7/2019 4:11:02 PM 166.4 -2.4
6/7/2019 4:11:03 PM 166.4 -2.4
6/7/2019 4:11:04 PM 166.4 -2.4
6/7/2019 4:11:05 PM 166.4 -2.4
6/7/2019 4:11:06 PM 166.5 -2.3
6/7/2019 4:11:07 PM 166.5 -2.3
6/7/2019 4:11:08 PM 166.5 -2.3
6/7/2019 4:11:09 PM 166.5 -2.3
6/7/2019 4:11:10 PM 166.5 -2.3
6/7/2019 4:11:11 PM 166.5 -2.3
6/7/2019 4:11:12 PM 166.5 -2.3
6/7/2019 4:11:13 PM 166.5 -2.3
6/7/2019 4:11:14 PM 166.5 -2.3
6/7/2019 4:11:15 PM 166.5 -2.3
6/7/2019 4:11:16 PM 166.5 -2.3
6/7/2019 4:11:17 PM 166.5 -2.3
6/7/2019 4:11:18 PM 166.5 -2.3
6/7/2019 4:11:19 PM 166.5 -2.3
6/7/2019 4:11:20 PM 166.5 -2.3
6/7/2019 4:11:21 PM 166.5 -2.3
6/7/2019 4:11:22 PM 166.5 -2.3
6/7/2019 4:11:23 PM 166.5 -2.3
6/7/2019 4:11:24 PM 166.5 -2.3
6/7/2019 4:11:25 PM 166.5 -2.3
6/7/2019 4:11:26 PM 166.5 -2.3
6/7/2019 4:11:27 PM 166.5 -2.3
6/7/2019 4:11:28 PM 166.5 -2.3
6/7/2019 4:11:29 PM 166.5 -2.3
6/7/2019 4:11:30 PM 166.5 -2.3
6/7/2019 4:11:31 PM 166.5 -2.3
6/7/2019 4:11:32 PM 166.5 -2.3
6/7/2019 4:11:33 PM 166.5 -2.3
6/7/2019 4:11:34 PM 166.5 -2.3
6/7/2019 4:11:35 PM 166.5 -2.3
6/7/2019 4:11:36 PM 166.5 -2.3
6/7/2019 4:11:37 PM 166.5 -2.3
6/7/2019 4:11:38 PM 166.5 -2.3
6/7/2019 4:11:39 PM 166.5 -2.3
6/7/2019 4:11:40 PM 166.5 -2.3
6/7/2019 4:11:41 PM 166.5 -2.3
6/7/2019 4:11:42 PM 166.5 -2.3
6/7/2019 4:11:43 PM 166.5 -2.3
6/7/2019 4:11:44 PM 166.5 -2.3
6/7/2019 4:11:45 PM 166.5 -2.3
6/7/2019 4:11:46 PM 166.6 -2.2
6/7/2019 4:11:47 PM 166.6 -2.2
6/7/2019 4:11:48 PM 166.6 -2.2
6/7/2019 4:11:49 PM 166.6 -2.2
6/7/2019 4:11:50 PM 166.5 -2.3
6/7/2019 4:11:51 PM 166.5 -2.3
6/7/2019 4:11:52 PM 166.5 -2.3
6/7/2019 4:11:53 PM 166.5 -2.3
6/7/2019 4:11:54 PM 166.5 -2.3
6/7/2019 4:11:55 PM 166.5 -2.3
6/7/2019 4:11:56 PM 166.5 -2.3
6/7/2019 4:11:57 PM 166.5 -2.3
6/7/2019 4:11:58 PM 166.5 -2.3
6/7/2019 4:11:59 PM 166.5 -2.3
6/7/2019 4:12:00 PM 166.5 -2.3
6/7/2019 4:12:01 PM 166.5 -2.3
6/7/2019 4:12:02 PM 166.5 -2.3
6/7/2019 4:12:03 PM 166.5 -2.3
6/7/2019 4:12:04 PM 166.5 -2.3
6/7/2019 4:12:05 PM 166.5 -2.3
6/7/2019 4:12:06 PM 166.5 -2.3
6/7/2019 4:12:07 PM 166.5 -2.3
6/7/2019 4:12:08 PM 166.5 -2.3
6/7/2019 4:12:09 PM 166.4 -2.4
6/7/2019 4:12:10 PM 166.4 -2.4
Page 376 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 4:12:11 PM 166.4 -2.4
6/7/2019 4:12:12 PM 166.4 -2.4
6/7/2019 4:12:13 PM 166.4 -2.4
6/7/2019 4:12:14 PM 166.4 -2.4
6/7/2019 4:12:15 PM 166.4 -2.4
6/7/2019 4:12:16 PM 166.4 -2.4
6/7/2019 4:12:17 PM 166.3 -2.5
6/7/2019 4:12:18 PM 166.3 -2.5
6/7/2019 4:12:19 PM 166.3 -2.5
6/7/2019 4:12:20 PM 166.3 -2.5
6/7/2019 4:12:21 PM 166.3 -2.5
6/7/2019 4:12:22 PM 166.3 -2.5
6/7/2019 4:12:23 PM 166.3 -2.5
6/7/2019 4:12:24 PM 166.3 -2.5
6/7/2019 4:12:25 PM 166.2 -2.6
6/7/2019 4:12:26 PM 166.2 -2.6
6/7/2019 4:12:27 PM 166.2 -2.6
6/7/2019 4:12:28 PM 166.2 -2.6
6/7/2019 4:12:29 PM 166.2 -2.6
6/7/2019 4:12:30 PM 166.2 -2.6
6/7/2019 4:12:31 PM 166.2 -2.6
6/7/2019 4:12:32 PM 166.1 -2.7
6/7/2019 4:12:33 PM 166.1 -2.7
6/7/2019 4:12:34 PM 166.1 -2.7
6/7/2019 4:12:35 PM 166.1 -2.7
6/7/2019 4:12:36 PM 166.1 -2.7
6/7/2019 4:12:37 PM 166.0 -2.8
6/7/2019 4:12:38 PM 166.0 -2.8
6/7/2019 4:12:39 PM 166.0 -2.8
6/7/2019 4:12:40 PM 166.0 -2.8
6/7/2019 4:12:41 PM 165.9 -2.9
6/7/2019 4:12:42 PM 165.9 -2.9
6/7/2019 4:12:43 PM 165.9 -2.9
6/7/2019 4:12:44 PM 165.9 -2.9
6/7/2019 4:12:45 PM 165.8 -3.0
6/7/2019 4:12:46 PM 165.8 -3.0
6/7/2019 4:12:47 PM 165.8 -3.0
6/7/2019 4:12:48 PM 165.8 -3.0
6/7/2019 4:12:49 PM 165.7 -3.1
6/7/2019 4:12:50 PM 165.7 -3.1
6/7/2019 4:12:51 PM 165.7 -3.1
6/7/2019 4:12:52 PM 165.7 -3.1
6/7/2019 4:12:53 PM 165.7 -3.1
6/7/2019 4:12:54 PM 165.6 -3.2
6/7/2019 4:12:55 PM 165.6 -3.2
6/7/2019 4:12:56 PM 165.6 -3.2
6/7/2019 4:12:57 PM 165.6 -3.2
6/7/2019 4:12:58 PM 165.6 -3.2
6/7/2019 4:12:59 PM 165.6 -3.2
6/7/2019 4:13:00 PM 165.5 -3.3
6/7/2019 4:13:01 PM 165.5 -3.3
6/7/2019 4:13:02 PM 165.5 -3.3
6/7/2019 4:13:03 PM 165.5 -3.3
6/7/2019 4:13:04 PM 165.5 -3.3
6/7/2019 4:13:05 PM 165.4 -3.4
6/7/2019 4:13:06 PM 165.4 -3.4
6/7/2019 4:13:07 PM 165.4 -3.4
6/7/2019 4:13:08 PM 165.4 -3.4
6/7/2019 4:13:09 PM 165.4 -3.4
6/7/2019 4:13:10 PM 165.3 -3.5
6/7/2019 4:13:11 PM 165.3 -3.5
6/7/2019 4:13:12 PM 165.3 -3.5
6/7/2019 4:13:13 PM 165.3 -3.5
6/7/2019 4:13:14 PM 165.3 -3.5
6/7/2019 4:13:15 PM 165.3 -3.5
6/7/2019 4:13:16 PM 165.2 -3.6
6/7/2019 4:13:17 PM 165.2 -3.6
6/7/2019 4:13:18 PM 165.2 -3.6
6/7/2019 4:13:19 PM 165.2 -3.6
6/7/2019 4:13:20 PM 165.2 -3.6
6/7/2019 4:13:21 PM 165.1 -3.7
6/7/2019 4:13:22 PM 165.1 -3.7
6/7/2019 4:13:23 PM 165.1 -3.7
6/7/2019 4:13:24 PM 165.1 -3.7
6/7/2019 4:13:25 PM 165.0 -3.8
6/7/2019 4:13:26 PM 165.0 -3.8
6/7/2019 4:13:27 PM 165.0 -3.8
6/7/2019 4:13:28 PM 164.9 -3.9
6/7/2019 4:13:29 PM 164.9 -3.9
6/7/2019 4:13:30 PM 164.9 -3.9
6/7/2019 4:13:31 PM 164.9 -3.9
6/7/2019 4:13:32 PM 164.8 -4.0
6/7/2019 4:13:33 PM 164.8 -4.0
6/7/2019 4:13:34 PM 164.8 -4.0
6/7/2019 4:13:35 PM 164.8 -4.0
6/7/2019 4:13:36 PM 164.7 -4.1
6/7/2019 4:13:37 PM 164.7 -4.1
6/7/2019 4:13:38 PM 164.7 -4.1
6/7/2019 4:13:39 PM 164.7 -4.1
6/7/2019 4:13:40 PM 164.7 -4.1
6/7/2019 4:13:41 PM 164.6 -4.2
6/7/2019 4:13:42 PM 164.6 -4.2
Page 377 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity (µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-B-TR-2 Test-1 Data Log
6/7/2019 4:13:43 PM 164.6 -4.2
6/7/2019 4:13:44 PM 164.6 -4.2
6/7/2019 4:13:45 PM 164.6 -4.2
6/7/2019 4:13:46 PM 164.6 -4.2
6/7/2019 4:13:47 PM 164.6 -4.2
6/7/2019 4:13:48 PM 164.5 -4.3
6/7/2019 4:13:49 PM 164.5 -4.3
6/7/2019 4:13:50 PM 164.5 -4.3
6/7/2019 4:13:51 PM 164.5 -4.3
6/7/2019 4:13:52 PM 164.5 -4.3
6/7/2019 4:13:53 PM 164.5 -4.3
6/7/2019 4:13:54 PM 164.5 -4.3
6/7/2019 4:13:55 PM 164.5 -4.3
6/7/2019 4:13:56 PM 164.5 -4.3
6/7/2019 4:13:57 PM 164.5 -4.3
6/7/2019 4:13:58 PM 164.5 -4.3
6/7/2019 4:13:59 PM 164.5 -4.3
6/7/2019 4:14:00 PM 164.5 -4.3
6/7/2019 4:14:01 PM 164.6 -4.2
Page 378 of 452 August 2019
APPENDIX E52: SALT DILUTION GAUGING SUMMARY
SEEP-B-TR-2 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-B-TR-2 1445
SEEP-B-TR-2 1452
SEEP-B-TR-2 1454
Location EC Reading
(µS/cms)
SEEP-B-TR-2 256
SEEP-B-TR-2 2,107
SEEP-B-TR-2 17,409
SEEP-B-TR-2 128,835
q 300,300
K 1.2919
0.2
3.7
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
25.1
24.7
24.6
(µS/cms) (°C)
Table E2 SEEP-B-TR-2 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
151 18.7
142.4 18.5
167 18.5
153.5 (µS/cms)
Geometric Mean 153.1 (µS/cms)
Average
Average (pre-test)168.8 (µS/cms)
Table E3 SEEP-B-TR-2 TEST-1 YSI Salt Dilution Calibration Data
Calibration Temperature
Average (post-test)172.8 (µS/cms)
Table E4 SEEP-B-TR-2 TEST-1 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
100
1,000
(mg/L)(°C)
Calculated Flow Rate Q
L/s
GPM
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)1,677,106.1 (s) . (µS/cms)
10,000
100,000 25
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 379 of 452 August 2019
APPENDIX E53: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 4:33:32 PM 185.9 -
6/7/2019 4:33:33 PM 182.8 -
6/7/2019 4:33:34 PM 180.7 -
6/7/2019 4:33:35 PM 179.0 -
6/7/2019 4:33:36 PM 177.3 -
6/7/2019 4:33:37 PM 176.4 -
6/7/2019 4:33:38 PM 175.0 -
6/7/2019 4:33:39 PM 173.9 -
6/7/2019 4:33:40 PM 172.6 -
6/7/2019 4:33:41 PM 171.7 -
6/7/2019 4:33:42 PM 170.0 -
6/7/2019 4:33:43 PM 167.9 -
6/7/2019 4:33:44 PM 166.5 -
6/7/2019 4:33:45 PM 165.2 -
6/7/2019 4:33:46 PM 163.8 -
6/7/2019 4:33:47 PM 162.5 -
6/7/2019 4:33:48 PM 161.6 -
6/7/2019 4:33:49 PM 161.1 -
6/7/2019 4:33:50 PM 160.4 -
6/7/2019 4:33:51 PM 159.7 -
6/7/2019 4:33:52 PM 159.2 -
6/7/2019 4:33:53 PM 158.9 -
6/7/2019 4:33:54 PM 158.4 -
6/7/2019 4:33:55 PM 158.1 -
6/7/2019 4:33:56 PM 157.7 -
6/7/2019 4:33:57 PM 157.4 -
6/7/2019 4:33:58 PM 157.1 -
6/7/2019 4:33:59 PM 156.8 -
6/7/2019 4:34:00 PM 156.6 -
6/7/2019 4:34:01 PM 156.4 -
6/7/2019 4:34:02 PM 156.2 -
6/7/2019 4:34:03 PM 156.0 -
6/7/2019 4:34:04 PM 155.8 -
6/7/2019 4:34:05 PM 155.7 -
6/7/2019 4:34:06 PM 155.5 -
6/7/2019 4:34:07 PM 155.3 -
6/7/2019 4:34:08 PM 155.1 -
6/7/2019 4:34:09 PM 155.0 -
6/7/2019 4:34:10 PM 154.8 -
6/7/2019 4:34:11 PM 154.7 -
6/7/2019 4:34:12 PM 154.6 -
6/7/2019 4:34:13 PM 154.5 -
6/7/2019 4:34:14 PM 154.3 -
6/7/2019 4:34:15 PM 154.2 -
6/7/2019 4:34:16 PM 154.1 -
6/7/2019 4:34:17 PM 153.9 -
6/7/2019 4:34:18 PM 153.8 -
6/7/2019 4:34:19 PM 153.6 -
6/7/2019 4:34:20 PM 153.5 -
6/7/2019 4:34:21 PM 153.4 -
6/7/2019 4:34:22 PM 153.3 -
6/7/2019 4:34:23 PM 153.2 -
6/7/2019 4:34:24 PM 153.2 -
6/7/2019 4:34:25 PM 153.2 -
6/7/2019 4:34:26 PM 153.4 -
6/7/2019 4:34:27 PM 154.2 -
6/7/2019 4:34:28 PM 155.4 -
6/7/2019 4:34:29 PM 157.3 -
6/7/2019 4:34:30 PM 236.3 75.6
6/7/2019 4:34:31 PM 293.4 132.7
6/7/2019 4:34:32 PM 371.2 210.5
6/7/2019 4:34:33 PM 473.2 312.5
6/7/2019 4:34:34 PM 559.7 399.0
6/7/2019 4:34:35 PM 716.1 555.4
6/7/2019 4:34:36 PM 997.9 837.2
6/7/2019 4:34:37 PM 1279.3 1118.6
6/7/2019 4:34:38 PM 1566.0 1405.3
6/7/2019 4:34:39 PM 2024.8 1864.1
6/7/2019 4:34:40 PM 2317.8 2157.1
6/7/2019 4:34:41 PM 2672.2 2511.5
Table E1 SEEP-C1 TEST-1 Data Log
Page 380 of 452 August 2019
APPENDIX E53: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-1 Data Log
6/7/2019 4:34:42 PM 2981.2 2820.5
6/7/2019 4:34:43 PM 3312.8 3152.1
6/7/2019 4:34:44 PM 3924.2 3763.5
6/7/2019 4:34:45 PM 4334.2 4173.5
6/7/2019 4:34:46 PM 4694.9 4534.2
6/7/2019 4:34:47 PM 5136.8 4976.1
6/7/2019 4:34:48 PM 5576.2 5415.5
6/7/2019 4:34:49 PM 5910.9 5750.2
6/7/2019 4:34:50 PM 6270.7 6110.0
6/7/2019 4:34:51 PM 6424.2 6263.5
6/7/2019 4:34:52 PM 6569.4 6408.7
6/7/2019 4:34:53 PM 7061.0 6900.3
6/7/2019 4:34:54 PM 7287.0 7126.3
6/7/2019 4:34:55 PM 7484.4 7323.7
6/7/2019 4:34:56 PM 7616.0 7455.3
6/7/2019 4:34:57 PM 7683.0 7522.3
6/7/2019 4:34:58 PM 7715.0 7554.3
6/7/2019 4:34:59 PM 7722.6 7561.9
6/7/2019 4:35:00 PM 7717.5 7556.8
6/7/2019 4:35:01 PM 7696.8 7536.1
6/7/2019 4:35:02 PM 7669.1 7508.4
6/7/2019 4:35:03 PM 7642.5 7481.8
6/7/2019 4:35:04 PM 7607.0 7446.3
6/7/2019 4:35:05 PM 7161.2 7000.5
6/7/2019 4:35:06 PM 7033.0 6872.3
6/7/2019 4:35:07 PM 6898.3 6737.6
6/7/2019 4:35:08 PM 6772.0 6611.3
6/7/2019 4:35:09 PM 6701.8 6541.1
6/7/2019 4:35:10 PM 6553.4 6392.7
6/7/2019 4:35:11 PM 6456.1 6295.4
6/7/2019 4:35:12 PM 5964.9 5804.2
6/7/2019 4:35:13 PM 5769.9 5609.2
6/7/2019 4:35:14 PM 5631.0 5470.3
6/7/2019 4:35:15 PM 5499.4 5338.7
6/7/2019 4:35:16 PM 5403.3 5242.6
6/7/2019 4:35:17 PM 5309.3 5148.6
6/7/2019 4:35:18 PM 5209.3 5048.6
6/7/2019 4:35:19 PM 4844.5 4683.8
6/7/2019 4:35:20 PM 4685.2 4524.5
6/7/2019 4:35:21 PM 4514.8 4354.1
6/7/2019 4:35:22 PM 4395.3 4234.6
6/7/2019 4:35:23 PM 4315.1 4154.4
6/7/2019 4:35:24 PM 4223.2 4062.5
6/7/2019 4:35:25 PM 3901.4 3740.7
6/7/2019 4:35:26 PM 3784.0 3623.3
6/7/2019 4:35:27 PM 3660.2 3499.5
6/7/2019 4:35:28 PM 3566.0 3405.3
6/7/2019 4:35:29 PM 3512.8 3352.1
6/7/2019 4:35:30 PM 3451.4 3290.7
6/7/2019 4:35:31 PM 3407.1 3246.4
6/7/2019 4:35:32 PM 3103.7 2943.0
6/7/2019 4:35:33 PM 3027.1 2866.4
6/7/2019 4:35:34 PM 2935.0 2774.3
6/7/2019 4:35:35 PM 2906.5 2745.8
6/7/2019 4:35:36 PM 2861.5 2700.8
6/7/2019 4:35:37 PM 2829.0 2668.3
6/7/2019 4:35:38 PM 2790.8 2630.1
6/7/2019 4:35:39 PM 2603.9 2443.2
6/7/2019 4:35:40 PM 2524.9 2364.2
6/7/2019 4:35:41 PM 2461.1 2300.4
6/7/2019 4:35:42 PM 2421.9 2261.2
6/7/2019 4:35:43 PM 2393.0 2232.3
6/7/2019 4:35:44 PM 2363.3 2202.6
6/7/2019 4:35:45 PM 2330.8 2170.1
6/7/2019 4:35:46 PM 2164.1 2003.4
6/7/2019 4:35:47 PM 2093.7 1933.0
6/7/2019 4:35:48 PM 2052.0 1891.3
6/7/2019 4:35:49 PM 2028.6 1867.9
6/7/2019 4:35:50 PM 2001.3 1840.6
6/7/2019 4:35:51 PM 1976.3 1815.6
6/7/2019 4:35:52 PM 1954.5 1793.8
6/7/2019 4:35:53 PM 1931.1 1770.4
6/7/2019 4:35:54 PM 1810.4 1649.7
6/7/2019 4:35:55 PM 1756.7 1596.0
6/7/2019 4:35:56 PM 1720.3 1559.6
6/7/2019 4:35:57 PM 1696.2 1535.5
6/7/2019 4:35:58 PM 1681.5 1520.8
Page 381 of 452 August 2019
APPENDIX E53: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-1 Data Log
6/7/2019 4:35:59 PM 1663.4 1502.7
6/7/2019 4:36:00 PM 1651.0 1490.3
6/7/2019 4:36:01 PM 1637.3 1476.6
6/7/2019 4:36:02 PM 1623.2 1462.5
6/7/2019 4:36:03 PM 1507.6 1346.9
6/7/2019 4:36:04 PM 1482.2 1321.5
6/7/2019 4:36:05 PM 1453.7 1293.0
6/7/2019 4:36:06 PM 1447.2 1286.5
6/7/2019 4:36:07 PM 1432.3 1271.6
6/7/2019 4:36:08 PM 1420.2 1259.5
6/7/2019 4:36:09 PM 1406.1 1245.4
6/7/2019 4:36:10 PM 1394.5 1233.8
6/7/2019 4:36:11 PM 1301.9 1141.2
6/7/2019 4:36:12 PM 1288.6 1127.9
6/7/2019 4:36:13 PM 1259.7 1099.0
6/7/2019 4:36:14 PM 1242.9 1082.2
6/7/2019 4:36:15 PM 1227.2 1066.5
6/7/2019 4:36:16 PM 1217.6 1056.9
6/7/2019 4:36:17 PM 1208.4 1047.7
6/7/2019 4:36:18 PM 1199.5 1038.8
6/7/2019 4:36:19 PM 1127.5 966.8
6/7/2019 4:36:20 PM 1110.6 949.9
6/7/2019 4:36:21 PM 1093.1 932.4
6/7/2019 4:36:22 PM 1079.8 919.1
6/7/2019 4:36:23 PM 1074.6 913.9
6/7/2019 4:36:24 PM 1064.3 903.6
6/7/2019 4:36:25 PM 1055.3 894.6
6/7/2019 4:36:26 PM 1045.3 884.6
6/7/2019 4:36:27 PM 1036.3 875.6
6/7/2019 4:36:28 PM 1026.5 865.8
6/7/2019 4:36:29 PM 967.5 806.8
6/7/2019 4:36:30 PM 954.7 794.0
6/7/2019 4:36:31 PM 936.5 775.8
6/7/2019 4:36:32 PM 925.5 764.8
6/7/2019 4:36:33 PM 920.2 759.5
6/7/2019 4:36:34 PM 911.4 750.7
6/7/2019 4:36:35 PM 905.0 744.3
6/7/2019 4:36:36 PM 897.3 736.6
6/7/2019 4:36:37 PM 892.0 731.3
6/7/2019 4:36:38 PM 885.3 724.6
6/7/2019 4:36:39 PM 879.9 719.2
6/7/2019 4:36:40 PM 825.3 664.6
6/7/2019 4:36:41 PM 820.9 660.2
6/7/2019 4:36:42 PM 812.1 651.4
6/7/2019 4:36:43 PM 806.1 645.4
6/7/2019 4:36:44 PM 801.4 640.7
6/7/2019 4:36:45 PM 797.2 636.5
6/7/2019 4:36:46 PM 792.2 631.5
6/7/2019 4:36:47 PM 786.1 625.4
6/7/2019 4:36:48 PM 780.2 619.5
6/7/2019 4:36:49 PM 775.6 614.9
6/7/2019 4:36:50 PM 770.2 609.5
6/7/2019 4:36:51 PM 765.8 605.1
6/7/2019 4:36:52 PM 715.5 554.8
6/7/2019 4:36:53 PM 709.3 548.6
6/7/2019 4:36:54 PM 700.1 539.4
6/7/2019 4:36:55 PM 695.2 534.5
6/7/2019 4:36:56 PM 689.9 529.2
6/7/2019 4:36:57 PM 684.3 523.6
6/7/2019 4:36:58 PM 680.4 519.7
6/7/2019 4:36:59 PM 677.7 517.0
6/7/2019 4:37:00 PM 674.4 513.7
6/7/2019 4:37:01 PM 671.5 510.8
6/7/2019 4:37:02 PM 668.8 508.1
6/7/2019 4:37:03 PM 664.7 504.0
6/7/2019 4:37:04 PM 661.4 500.7
6/7/2019 4:37:05 PM 658.9 498.2
6/7/2019 4:37:06 PM 655.6 494.9
6/7/2019 4:37:07 PM 611.7 451.0
6/7/2019 4:37:08 PM 607.6 446.9
6/7/2019 4:37:09 PM 605.2 444.5
6/7/2019 4:37:10 PM 597.4 436.7
6/7/2019 4:37:11 PM 515.1 354.4
6/7/2019 4:37:12 PM 579.2 418.5
6/7/2019 4:37:13 PM 577.5 416.8
6/7/2019 4:37:14 PM 570.7 410.0
6/7/2019 4:37:15 PM 568.6 407.9
6/7/2019 4:37:16 PM 566.3 405.6
6/7/2019 4:37:17 PM 564.3 403.6
Page 382 of 452 August 2019
APPENDIX E53: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-1 Data Log
6/7/2019 4:37:18 PM 562.2 401.5
6/7/2019 4:37:19 PM 560.0 399.3
6/7/2019 4:37:20 PM 558.1 397.4
6/7/2019 4:37:21 PM 555.7 395.0
6/7/2019 4:37:22 PM 553.8 393.1
6/7/2019 4:37:23 PM 551.7 391.0
6/7/2019 4:37:24 PM 549.9 389.2
6/7/2019 4:37:25 PM 547.9 387.2
6/7/2019 4:37:26 PM 546.2 385.5
6/7/2019 4:37:27 PM 544.3 383.6
6/7/2019 4:37:28 PM 541.8 381.1
6/7/2019 4:37:29 PM 537.9 377.2
6/7/2019 4:37:30 PM 534.7 374.0
6/7/2019 4:37:31 PM 530.8 370.1
6/7/2019 4:37:32 PM 527.5 366.8
6/7/2019 4:37:33 PM 523.7 363.0
6/7/2019 4:37:34 PM 520.5 359.8
6/7/2019 4:37:35 PM 516.6 355.9
6/7/2019 4:37:36 PM 513.1 352.4
6/7/2019 4:37:37 PM 509.1 348.4
6/7/2019 4:37:38 PM 505.6 344.9
6/7/2019 4:37:39 PM 501.7 341.0
6/7/2019 4:37:40 PM 498.1 337.4
6/7/2019 4:37:41 PM 494.0 333.3
6/7/2019 4:37:42 PM 490.3 329.6
6/7/2019 4:37:43 PM 485.9 325.2
6/7/2019 4:37:44 PM 482.1 321.4
6/7/2019 4:37:45 PM 477.9 317.2
6/7/2019 4:37:46 PM 474.2 313.5
6/7/2019 4:37:47 PM 470.0 309.3
6/7/2019 4:37:48 PM 466.5 305.8
6/7/2019 4:37:49 PM 462.5 301.8
6/7/2019 4:37:50 PM 459.0 298.3
6/7/2019 4:37:51 PM 455.1 294.4
6/7/2019 4:37:52 PM 451.7 291.0
6/7/2019 4:37:53 PM 448.0 287.3
6/7/2019 4:37:54 PM 444.8 284.1
6/7/2019 4:37:55 PM 441.3 280.6
6/7/2019 4:37:56 PM 438.3 277.6
6/7/2019 4:37:57 PM 435.1 274.4
6/7/2019 4:37:58 PM 432.3 271.6
6/7/2019 4:37:59 PM 429.2 268.5
6/7/2019 4:38:00 PM 426.2 265.5
6/7/2019 4:38:01 PM 423.6 262.9
6/7/2019 4:38:02 PM 420.8 260.1
6/7/2019 4:38:03 PM 418.5 257.8
6/7/2019 4:38:04 PM 415.8 255.1
6/7/2019 4:38:05 PM 413.6 252.9
6/7/2019 4:38:06 PM 411.1 250.4
6/7/2019 4:38:07 PM 409.0 248.3
6/7/2019 4:38:08 PM 406.5 245.8
6/7/2019 4:38:09 PM 404.4 243.7
6/7/2019 4:38:10 PM 402.1 241.4
6/7/2019 4:38:11 PM 400.2 239.5
6/7/2019 4:38:12 PM 397.9 237.2
6/7/2019 4:38:13 PM 396.0 235.3
6/7/2019 4:38:14 PM 394.0 233.3
6/7/2019 4:38:15 PM 392.1 231.4
6/7/2019 4:38:16 PM 390.0 229.3
6/7/2019 4:38:17 PM 388.2 227.5
6/7/2019 4:38:18 PM 386.1 225.4
6/7/2019 4:38:19 PM 384.4 223.7
6/7/2019 4:38:20 PM 382.4 221.7
6/7/2019 4:38:21 PM 380.7 220.0
6/7/2019 4:38:22 PM 378.8 218.1
6/7/2019 4:38:23 PM 377.1 216.4
6/7/2019 4:38:24 PM 375.2 214.5
6/7/2019 4:38:25 PM 373.6 212.9
6/7/2019 4:38:26 PM 371.6 210.9
6/7/2019 4:38:27 PM 369.9 209.2
6/7/2019 4:38:28 PM 368.0 207.3
6/7/2019 4:38:29 PM 366.3 205.6
6/7/2019 4:38:30 PM 364.3 203.6
6/7/2019 4:38:31 PM 362.6 201.9
6/7/2019 4:38:32 PM 360.7 200.0
6/7/2019 4:38:33 PM 359.0 198.3
6/7/2019 4:38:34 PM 357.1 196.4
6/7/2019 4:38:35 PM 355.4 194.7
6/7/2019 4:38:36 PM 353.4 192.7
Page 383 of 452 August 2019
APPENDIX E53: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-1 Data Log
6/7/2019 4:38:37 PM 351.6 190.9
6/7/2019 4:38:38 PM 349.6 188.9
6/7/2019 4:38:39 PM 348.0 187.3
6/7/2019 4:38:40 PM 346.1 185.4
6/7/2019 4:38:41 PM 344.3 183.6
6/7/2019 4:38:42 PM 342.8 182.1
6/7/2019 4:38:43 PM 341.1 180.4
6/7/2019 4:38:44 PM 339.6 178.9
6/7/2019 4:38:45 PM 337.9 177.2
6/7/2019 4:38:46 PM 336.5 175.8
6/7/2019 4:38:47 PM 334.9 174.2
6/7/2019 4:38:48 PM 333.6 172.9
6/7/2019 4:38:49 PM 332.2 171.5
6/7/2019 4:38:50 PM 330.9 170.2
6/7/2019 4:38:51 PM 329.5 168.8
6/7/2019 4:38:52 PM 328.3 167.6
6/7/2019 4:38:53 PM 326.9 166.2
6/7/2019 4:38:54 PM 325.8 165.1
6/7/2019 4:38:55 PM 324.5 163.8
6/7/2019 4:38:56 PM 323.4 162.7
6/7/2019 4:38:57 PM 322.1 161.4
6/7/2019 4:38:58 PM 321.0 160.3
6/7/2019 4:38:59 PM 319.7 159.0
6/7/2019 4:39:00 PM 318.6 157.9
6/7/2019 4:39:01 PM 317.5 156.8
6/7/2019 4:39:02 PM 316.4 155.7
6/7/2019 4:39:03 PM 315.2 154.5
6/7/2019 4:39:04 PM 314.3 153.6
6/7/2019 4:39:05 PM 313.1 152.4
6/7/2019 4:39:06 PM 312.1 151.4
6/7/2019 4:39:07 PM 310.9 150.2
6/7/2019 4:39:08 PM 309.9 149.2
6/7/2019 4:39:09 PM 308.8 148.1
6/7/2019 4:39:10 PM 307.9 147.2
6/7/2019 4:39:11 PM 306.9 146.2
6/7/2019 4:39:12 PM 306.0 145.3
6/7/2019 4:39:13 PM 304.9 144.2
6/7/2019 4:39:14 PM 303.9 143.2
6/7/2019 4:39:15 PM 302.9 142.2
6/7/2019 4:39:16 PM 302.0 141.3
6/7/2019 4:39:17 PM 301.0 140.3
6/7/2019 4:39:18 PM 300.2 139.5
6/7/2019 4:39:19 PM 299.2 138.5
6/7/2019 4:39:20 PM 298.5 137.8
6/7/2019 4:39:21 PM 297.6 136.9
6/7/2019 4:39:22 PM 296.8 136.1
6/7/2019 4:39:23 PM 295.9 135.2
6/7/2019 4:39:24 PM 295.0 134.3
6/7/2019 4:39:25 PM 294.3 133.6
6/7/2019 4:39:26 PM 293.5 132.8
6/7/2019 4:39:27 PM 292.7 132.0
6/7/2019 4:39:28 PM 291.9 131.2
6/7/2019 4:39:29 PM 291.2 130.5
6/7/2019 4:39:30 PM 290.4 129.7
6/7/2019 4:39:31 PM 289.7 129.0
6/7/2019 4:39:32 PM 288.9 128.2
6/7/2019 4:39:33 PM 288.1 127.4
6/7/2019 4:39:34 PM 287.3 126.6
6/7/2019 4:39:35 PM 286.5 125.8
6/7/2019 4:39:36 PM 285.6 124.9
6/7/2019 4:39:37 PM 284.8 124.1
6/7/2019 4:39:38 PM 283.9 123.2
6/7/2019 4:39:39 PM 283.2 122.5
6/7/2019 4:39:40 PM 282.3 121.6
6/7/2019 4:39:41 PM 281.6 120.9
6/7/2019 4:39:42 PM 280.7 120.0
6/7/2019 4:39:43 PM 280.0 119.3
6/7/2019 4:39:44 PM 279.2 118.5
6/7/2019 4:39:45 PM 278.5 117.8
6/7/2019 4:39:46 PM 277.7 117.0
6/7/2019 4:39:47 PM 277.0 116.3
6/7/2019 4:39:48 PM 276.3 115.6
6/7/2019 4:39:49 PM 275.6 114.9
6/7/2019 4:39:50 PM 275.0 114.3
6/7/2019 4:39:51 PM 274.5 113.8
6/7/2019 4:39:52 PM 273.8 113.1
6/7/2019 4:39:53 PM 273.3 112.6
6/7/2019 4:39:54 PM 272.8 112.1
6/7/2019 4:39:55 PM 272.3 111.6
Page 384 of 452 August 2019
APPENDIX E53: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-1 Data Log
6/7/2019 4:39:56 PM 271.7 111.0
6/7/2019 4:39:57 PM 271.2 110.5
6/7/2019 4:39:58 PM 270.4 109.7
6/7/2019 4:39:59 PM 270.0 109.3
6/7/2019 4:40:00 PM 269.2 108.5
6/7/2019 4:40:01 PM 268.7 108.0
6/7/2019 4:40:02 PM 268.2 107.5
6/7/2019 4:40:03 PM 267.6 106.9
6/7/2019 4:40:04 PM 267.0 106.3
6/7/2019 4:40:05 PM 266.5 105.8
6/7/2019 4:40:06 PM 265.9 105.2
6/7/2019 4:40:07 PM 265.4 104.7
6/7/2019 4:40:08 PM 264.9 104.2
6/7/2019 4:40:09 PM 264.4 103.7
6/7/2019 4:40:10 PM 263.9 103.2
6/7/2019 4:40:11 PM 263.4 102.7
6/7/2019 4:40:12 PM 262.9 102.2
6/7/2019 4:40:13 PM 262.5 101.8
6/7/2019 4:40:14 PM 262.0 101.3
6/7/2019 4:40:15 PM 261.5 100.8
6/7/2019 4:40:16 PM 261.1 100.4
6/7/2019 4:40:17 PM 260.7 100.0
6/7/2019 4:40:18 PM 260.1 99.4
6/7/2019 4:40:19 PM 259.7 99.0
6/7/2019 4:40:20 PM 259.2 98.5
6/7/2019 4:40:21 PM 258.7 98.0
6/7/2019 4:40:22 PM 258.3 97.6
6/7/2019 4:40:23 PM 257.8 97.1
6/7/2019 4:40:24 PM 257.3 96.6
6/7/2019 4:40:25 PM 256.8 96.1
6/7/2019 4:40:26 PM 256.3 95.6
6/7/2019 4:40:27 PM 255.7 95.0
6/7/2019 4:40:28 PM 255.3 94.6
6/7/2019 4:40:29 PM 254.7 94.0
6/7/2019 4:40:30 PM 254.3 93.6
6/7/2019 4:40:31 PM 253.8 93.1
6/7/2019 4:40:32 PM 253.3 92.6
6/7/2019 4:40:33 PM 252.9 92.2
6/7/2019 4:40:34 PM 252.4 91.7
6/7/2019 4:40:35 PM 252.0 91.3
6/7/2019 4:40:36 PM 251.6 90.9
6/7/2019 4:40:37 PM 251.1 90.4
6/7/2019 4:40:38 PM 250.8 90.1
6/7/2019 4:40:39 PM 250.4 89.7
6/7/2019 4:40:40 PM 250.0 89.3
6/7/2019 4:40:41 PM 249.7 89.0
6/7/2019 4:40:42 PM 249.3 88.6
6/7/2019 4:40:43 PM 248.9 88.2
6/7/2019 4:40:44 PM 248.4 87.7
6/7/2019 4:40:45 PM 248.0 87.3
6/7/2019 4:40:46 PM 247.6 86.9
6/7/2019 4:40:47 PM 247.3 86.6
6/7/2019 4:40:48 PM 247.0 86.3
6/7/2019 4:40:49 PM 246.6 85.9
6/7/2019 4:40:50 PM 246.2 85.5
6/7/2019 4:40:51 PM 245.8 85.1
6/7/2019 4:40:52 PM 245.5 84.8
6/7/2019 4:40:53 PM 245.1 84.4
6/7/2019 4:40:54 PM 244.8 84.1
6/7/2019 4:40:55 PM 244.5 83.8
6/7/2019 4:40:56 PM 244.2 83.5
6/7/2019 4:40:57 PM 243.8 83.1
6/7/2019 4:40:58 PM 243.4 82.7
6/7/2019 4:40:59 PM 243.0 82.3
6/7/2019 4:41:00 PM 242.7 82.0
6/7/2019 4:41:01 PM 242.4 81.7
6/7/2019 4:41:02 PM 242.1 81.4
6/7/2019 4:41:03 PM 241.7 81.0
6/7/2019 4:41:04 PM 241.3 80.6
6/7/2019 4:41:05 PM 240.9 80.2
6/7/2019 4:41:06 PM 240.6 79.9
6/7/2019 4:41:07 PM 240.2 79.5
6/7/2019 4:41:08 PM 240.0 79.3
6/7/2019 4:41:09 PM 239.7 79.0
6/7/2019 4:41:10 PM 239.3 78.6
6/7/2019 4:41:11 PM 238.9 78.2
6/7/2019 4:41:12 PM 238.6 77.9
6/7/2019 4:41:13 PM 238.3 77.6
6/7/2019 4:41:14 PM 237.9 77.2
Page 385 of 452 August 2019
APPENDIX E53: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-1 Data Log
6/7/2019 4:41:15 PM 237.7 77.0
6/7/2019 4:41:16 PM 237.3 76.6
6/7/2019 4:41:17 PM 237.1 76.4
6/7/2019 4:41:18 PM 236.6 75.9
6/7/2019 4:41:19 PM 236.3 75.6
6/7/2019 4:41:20 PM 236.0 75.3
6/7/2019 4:41:21 PM 235.7 75.0
6/7/2019 4:41:22 PM 235.4 74.7
6/7/2019 4:41:23 PM 235.1 74.4
6/7/2019 4:41:24 PM 234.7 74.0
6/7/2019 4:41:25 PM 234.3 73.6
6/7/2019 4:41:26 PM 233.9 73.2
6/7/2019 4:41:27 PM 233.6 72.9
6/7/2019 4:41:28 PM 233.3 72.6
6/7/2019 4:41:29 PM 233.0 72.3
6/7/2019 4:41:30 PM 232.7 72.0
6/7/2019 4:41:31 PM 232.4 71.7
6/7/2019 4:41:32 PM 232.0 71.3
6/7/2019 4:41:33 PM 231.7 71.0
6/7/2019 4:41:34 PM 231.4 70.7
6/7/2019 4:41:35 PM 231.2 70.5
6/7/2019 4:41:36 PM 230.9 70.2
6/7/2019 4:41:37 PM 230.7 70.0
6/7/2019 4:41:38 PM 230.4 69.7
6/7/2019 4:41:39 PM 230.2 69.5
6/7/2019 4:41:40 PM 229.9 69.2
6/7/2019 4:41:41 PM 229.7 69.0
6/7/2019 4:41:42 PM 229.4 68.7
6/7/2019 4:41:43 PM 229.2 68.5
6/7/2019 4:41:44 PM 229.0 68.3
6/7/2019 4:41:45 PM 228.7 68.0
6/7/2019 4:41:46 PM 228.4 67.7
6/7/2019 4:41:47 PM 228.1 67.4
6/7/2019 4:41:48 PM 227.8 67.1
6/7/2019 4:41:49 PM 227.5 66.8
6/7/2019 4:41:50 PM 227.3 66.6
6/7/2019 4:41:51 PM 227.1 66.4
6/7/2019 4:41:52 PM 226.8 66.1
6/7/2019 4:41:53 PM 226.5 65.8
6/7/2019 4:41:54 PM 226.3 65.6
6/7/2019 4:41:55 PM 226.1 65.4
6/7/2019 4:41:56 PM 225.9 65.2
6/7/2019 4:41:57 PM 225.8 65.1
6/7/2019 4:41:58 PM 225.6 64.9
6/7/2019 4:41:59 PM 225.5 64.8
6/7/2019 4:42:00 PM 225.3 64.6
6/7/2019 4:42:01 PM 225.1 64.4
6/7/2019 4:42:02 PM 225.0 64.3
6/7/2019 4:42:03 PM 224.9 64.2
6/7/2019 4:42:04 PM 224.8 64.1
6/7/2019 4:42:05 PM 224.6 63.9
6/7/2019 4:42:06 PM 224.4 63.7
6/7/2019 4:42:07 PM 224.2 63.5
6/7/2019 4:42:08 PM 224.0 63.3
6/7/2019 4:42:09 PM 223.9 63.2
6/7/2019 4:42:10 PM 223.7 63.0
6/7/2019 4:42:11 PM 223.4 62.7
6/7/2019 4:42:12 PM 223.2 62.5
6/7/2019 4:42:13 PM 222.9 62.2
6/7/2019 4:42:14 PM 222.7 62.0
6/7/2019 4:42:15 PM 222.5 61.8
6/7/2019 4:42:16 PM 222.2 61.5
6/7/2019 4:42:17 PM 222.0 61.3
6/7/2019 4:42:18 PM 221.8 61.1
6/7/2019 4:42:19 PM 221.6 60.9
6/7/2019 4:42:20 PM 221.4 60.7
6/7/2019 4:42:21 PM 221.2 60.5
6/7/2019 4:42:22 PM 220.9 60.2
6/7/2019 4:42:23 PM 220.7 60.0
6/7/2019 4:42:24 PM 220.5 59.8
6/7/2019 4:42:25 PM 220.3 59.6
6/7/2019 4:42:26 PM 220.1 59.4
6/7/2019 4:42:27 PM 219.9 59.2
6/7/2019 4:42:28 PM 219.6 58.9
6/7/2019 4:42:29 PM 219.5 58.8
6/7/2019 4:42:30 PM 219.3 58.6
6/7/2019 4:42:31 PM 219.0 58.3
6/7/2019 4:42:32 PM 218.8 58.1
6/7/2019 4:42:33 PM 218.6 57.9
Page 386 of 452 August 2019
APPENDIX E53: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-1 Data Log
6/7/2019 4:42:34 PM 218.5 57.8
6/7/2019 4:42:35 PM 218.2 57.5
6/7/2019 4:42:36 PM 218.1 57.4
6/7/2019 4:42:37 PM 217.9 57.2
6/7/2019 4:42:38 PM 217.7 57.0
6/7/2019 4:42:39 PM 217.6 56.9
6/7/2019 4:42:40 PM 217.4 56.7
6/7/2019 4:42:41 PM 217.2 56.5
6/7/2019 4:42:42 PM 217.0 56.3
6/7/2019 4:42:43 PM 216.9 56.2
6/7/2019 4:42:44 PM 216.8 56.1
6/7/2019 4:42:45 PM 216.7 56.0
6/7/2019 4:42:46 PM 216.4 55.7
6/7/2019 4:42:47 PM 216.3 55.6
6/7/2019 4:42:48 PM 216.2 55.5
6/7/2019 4:42:49 PM 216.0 55.3
6/7/2019 4:42:50 PM 215.8 55.1
6/7/2019 4:42:51 PM 215.7 55.0
6/7/2019 4:42:52 PM 215.6 54.9
6/7/2019 4:42:53 PM 215.5 54.8
6/7/2019 4:42:54 PM 215.3 54.6
6/7/2019 4:42:55 PM 215.2 54.5
6/7/2019 4:42:56 PM 215.1 54.4
6/7/2019 4:42:57 PM 215.0 54.3
6/7/2019 4:42:58 PM 214.8 54.1
6/7/2019 4:42:59 PM 214.7 54.0
6/7/2019 4:43:00 PM 214.7 54.0
6/7/2019 4:43:01 PM 214.6 53.9
6/7/2019 4:43:02 PM 214.6 53.9
6/7/2019 4:43:03 PM 214.5 53.8
6/7/2019 4:43:04 PM 214.5 53.8
6/7/2019 4:43:05 PM 214.4 53.7
6/7/2019 4:43:06 PM 214.4 53.7
6/7/2019 4:43:07 PM 214.4 53.7
6/7/2019 4:43:08 PM 214.4 53.7
6/7/2019 4:43:09 PM 214.3 53.6
6/7/2019 4:43:10 PM 214.3 53.6
6/7/2019 4:43:11 PM 214.3 53.6
6/7/2019 4:43:12 PM 214.3 53.6
6/7/2019 4:43:13 PM 214.4 53.7
6/7/2019 4:43:14 PM 214.4 53.7
6/7/2019 4:43:15 PM 214.4 53.7
6/7/2019 4:43:16 PM 214.4 53.7
6/7/2019 4:43:17 PM 214.4 53.7
6/7/2019 4:43:18 PM 214.4 53.7
6/7/2019 4:43:19 PM 214.5 53.8
6/7/2019 4:43:20 PM 214.5 53.8
6/7/2019 4:43:21 PM 214.6 53.9
6/7/2019 4:43:22 PM 214.6 53.9
6/7/2019 4:43:23 PM 214.7 54.0
6/7/2019 4:43:24 PM 214.7 54.0
6/7/2019 4:43:25 PM 214.8 54.1
6/7/2019 4:43:26 PM 214.8 54.1
6/7/2019 4:43:27 PM 214.9 54.2
6/7/2019 4:43:28 PM 214.9 54.2
6/7/2019 4:43:29 PM 215.0 54.3
6/7/2019 4:43:30 PM 215.0 54.3
6/7/2019 4:43:31 PM 215.1 54.4
Page 387 of 452 August 2019
APPENDIX E53: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-C1 TEST-1 1625
SEEP-C1 TEST-1 1626
SEEP-C1 TEST-1 1627
SEEP-C1 TEST-1 1628
Location EC Reading
(µS/cms)
SEEP-C1 1,115
SEEP-C1 2,150
SEEP-C1 16,651
SEEP-C1 132,589
q 299,700
K 1.3293
0.9
13.8
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)
(µS/cms)
(µS/cms)
24.1
24.2
24.2
(µS/cms) (°C)
Table E2 SEEP-C1 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Average 145.4 (µS/cms)
142.9 21.4
141.8 21.8
142.6 21.4
154.3 21.7
(mg/L) (°C)
100
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)458,382.1 (s) . (µS/cms)
1,000
10,000
100,000 24.1
Table E4 SEEP-C1 TEST-1 Flow Calculation Summary
Mass of Salt injected mg
L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Geometric Mean 145.3
Average (pre-test)160.7
Calculated Flow Rate Q
Average (post-test)216.7
Slope of Calibration Curve (µS/cms) / (mg/L)
Table E3 SEEP-C1 TEST-1 YSI Salt Dilution Calibration Data
Calibration Temperature
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 388 of 452 August 2019
APPENDIX E54: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 4:51:14 PM 159.6 -
6/7/2019 4:51:15 PM 159.5 -
6/7/2019 4:51:16 PM 159.5 -
6/7/2019 4:51:17 PM 159.5 -
6/7/2019 4:51:18 PM 159.5 -
6/7/2019 4:51:19 PM 159.5 -
6/7/2019 4:51:20 PM 159.5 -
6/7/2019 4:51:21 PM 159.5 -
6/7/2019 4:51:22 PM 159.4 -
6/7/2019 4:51:23 PM 159.4 -
6/7/2019 4:51:24 PM 159.4 -
6/7/2019 4:51:25 PM 159.4 -
6/7/2019 4:51:26 PM 159.3 -
6/7/2019 4:51:27 PM 159.3 -
6/7/2019 4:51:28 PM 159.3 -
6/7/2019 4:51:29 PM 159.2 -
6/7/2019 4:51:30 PM 159.2 -
6/7/2019 4:51:31 PM 159.2 -
6/7/2019 4:51:32 PM 159.1 -
6/7/2019 4:51:33 PM 159.1 -
6/7/2019 4:51:34 PM 159.1 -
6/7/2019 4:51:35 PM 159.0 -
6/7/2019 4:51:36 PM 159.0 -
6/7/2019 4:51:37 PM 159.0 -
6/7/2019 4:51:38 PM 159.0 -
6/7/2019 4:51:39 PM 158.9 -
6/7/2019 4:51:40 PM 158.9 -
6/7/2019 4:51:41 PM 158.9 -
6/7/2019 4:51:42 PM 158.8 -
6/7/2019 4:51:43 PM 158.8 -
6/7/2019 4:51:44 PM 158.8 -
6/7/2019 4:51:45 PM 158.8 -
6/7/2019 4:51:46 PM 158.7 -
6/7/2019 4:51:47 PM 158.7 -
6/7/2019 4:51:48 PM 158.7 -
6/7/2019 4:51:49 PM 158.7 -
6/7/2019 4:51:50 PM 158.7 -
6/7/2019 4:51:51 PM 158.7 -
6/7/2019 4:51:52 PM 158.6 -
6/7/2019 4:51:53 PM 158.6 -
6/7/2019 4:51:54 PM 158.6 -
6/7/2019 4:51:55 PM 158.6 -
6/7/2019 4:51:56 PM 158.6 -
6/7/2019 4:51:57 PM 158.6 -
6/7/2019 4:51:58 PM 158.6 -
6/7/2019 4:51:59 PM 158.5 -
6/7/2019 4:52:00 PM 158.5 -
6/7/2019 4:52:01 PM 158.5 -
6/7/2019 4:52:02 PM 158.5 -
6/7/2019 4:52:03 PM 158.4 -
6/7/2019 4:52:04 PM 158.4 -
6/7/2019 4:52:05 PM 158.4 -
6/7/2019 4:52:06 PM 158.3 -
6/7/2019 4:52:07 PM 158.3 -
6/7/2019 4:52:08 PM 158.3 -
6/7/2019 4:52:09 PM 158.2 -
6/7/2019 4:52:10 PM 158.2 -
6/7/2019 4:52:11 PM 158.2 -
6/7/2019 4:52:12 PM 158.1 -
6/7/2019 4:52:13 PM 158.1 -
6/7/2019 4:52:14 PM 158.1 -
6/7/2019 4:52:15 PM 158.1 -
6/7/2019 4:52:16 PM 158.2 -
6/7/2019 4:52:17 PM 158.4 -
6/7/2019 4:52:18 PM 159.0 -
6/7/2019 4:52:19 PM 160.2 -
6/7/2019 4:52:20 PM 227.1 68.3
6/7/2019 4:52:21 PM 265.2 106.4
6/7/2019 4:52:22 PM 325.8 167.0
6/7/2019 4:52:23 PM 362.7 203.9
Table E1 SEEP-C1 TEST-2 Data Log
Page 389 of 452 August 2019
APPENDIX E54: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-2 Data Log
6/7/2019 4:52:24 PM 570.2 411.4
6/7/2019 4:52:25 PM 724.1 565.3
6/7/2019 4:52:26 PM 1080.1 921.3
6/7/2019 4:52:27 PM 1337.4 1178.6
6/7/2019 4:52:28 PM 1759.0 1600.2
6/7/2019 4:52:29 PM 2193.1 2034.3
6/7/2019 4:52:30 PM 2559.0 2400.2
6/7/2019 4:52:31 PM 2984.2 2825.4
6/7/2019 4:52:32 PM 3471.3 3312.5
6/7/2019 4:52:33 PM 3911.9 3753.1
6/7/2019 4:52:34 PM 4510.3 4351.5
6/7/2019 4:52:35 PM 5397.9 5239.1
6/7/2019 4:52:36 PM 5823.2 5664.4
6/7/2019 4:52:37 PM 6262.7 6103.9
6/7/2019 4:52:38 PM 6305.5 6146.7
6/7/2019 4:52:39 PM 7122.3 6963.5
6/7/2019 4:52:40 PM 7585.9 7427.1
6/7/2019 4:52:41 PM 7736.4 7577.6
6/7/2019 4:52:42 PM 7966.6 7807.8
6/7/2019 4:52:43 PM 8167.7 8008.9
6/7/2019 4:52:44 PM 8275.3 8116.5
6/7/2019 4:52:45 PM 8401.0 8242.2
6/7/2019 4:52:46 PM 8470.7 8311.9
6/7/2019 4:52:47 PM 8542.9 8384.1
6/7/2019 4:52:48 PM 8577.5 8418.7
6/7/2019 4:52:49 PM 8601.3 8442.5
6/7/2019 4:52:50 PM 8612.3 8453.5
6/7/2019 4:52:51 PM 8613.7 8454.9
6/7/2019 4:52:52 PM 8605.9 8447.1
6/7/2019 4:52:53 PM 8585.6 8426.8
6/7/2019 4:52:54 PM 8104.4 7945.6
6/7/2019 4:52:55 PM 7856.1 7697.3
6/7/2019 4:52:56 PM 7724.0 7565.2
6/7/2019 4:52:57 PM 7536.0 7377.2
6/7/2019 4:52:58 PM 7486.3 7327.5
6/7/2019 4:52:59 PM 7339.9 7181.1
6/7/2019 4:53:00 PM 7221.2 7062.4
6/7/2019 4:53:01 PM 6640.0 6481.2
6/7/2019 4:53:02 PM 6406.1 6247.3
6/7/2019 4:53:03 PM 6177.9 6019.1
6/7/2019 4:53:04 PM 6136.6 5977.8
6/7/2019 4:53:05 PM 6084.3 5925.5
6/7/2019 4:53:06 PM 5629.0 5470.2
6/7/2019 4:53:07 PM 5377.2 5218.4
6/7/2019 4:53:08 PM 5185.3 5026.5
6/7/2019 4:53:09 PM 5125.5 4966.7
6/7/2019 4:53:10 PM 5032.5 4873.7
6/7/2019 4:53:11 PM 4595.0 4436.2
6/7/2019 4:53:12 PM 4454.1 4295.3
6/7/2019 4:53:13 PM 4329.0 4170.2
6/7/2019 4:53:14 PM 4214.3 4055.5
6/7/2019 4:53:15 PM 4069.5 3910.7
6/7/2019 4:53:16 PM 3997.7 3838.9
6/7/2019 4:53:17 PM 3711.6 3552.8
6/7/2019 4:53:18 PM 3551.1 3392.3
6/7/2019 4:53:19 PM 3414.8 3256.0
6/7/2019 4:53:20 PM 3317.9 3159.1
6/7/2019 4:53:21 PM 3267.4 3108.6
6/7/2019 4:53:22 PM 3173.1 3014.3
6/7/2019 4:53:23 PM 2919.5 2760.7
6/7/2019 4:53:24 PM 2832.9 2674.1
6/7/2019 4:53:25 PM 2754.2 2595.4
6/7/2019 4:53:26 PM 2686.5 2527.7
6/7/2019 4:53:27 PM 2651.0 2492.2
6/7/2019 4:53:28 PM 2440.7 2281.9
6/7/2019 4:53:29 PM 2394.9 2236.1
6/7/2019 4:53:30 PM 2312.3 2153.5
6/7/2019 4:53:31 PM 2293.9 2135.1
6/7/2019 4:53:32 PM 2259.8 2101.0
6/7/2019 4:53:33 PM 2206.2 2047.4
6/7/2019 4:53:34 PM 2054.5 1895.7
6/7/2019 4:53:35 PM 1980.8 1822.0
6/7/2019 4:53:36 PM 1927.9 1769.1
6/7/2019 4:53:37 PM 1911.3 1752.5
6/7/2019 4:53:38 PM 1874.8 1716.0
6/7/2019 4:53:39 PM 1848.7 1689.9
6/7/2019 4:53:40 PM 1815.9 1657.1
Page 390 of 452 August 2019
APPENDIX E54: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-2 Data Log
6/7/2019 4:53:41 PM 1668.2 1509.4
6/7/2019 4:53:42 PM 1642.9 1484.1
6/7/2019 4:53:43 PM 1603.2 1444.4
6/7/2019 4:53:44 PM 1591.5 1432.7
6/7/2019 4:53:45 PM 1579.9 1421.1
6/7/2019 4:53:46 PM 1466.9 1308.1
6/7/2019 4:53:47 PM 1422.3 1263.5
6/7/2019 4:53:48 PM 1382.8 1224.0
6/7/2019 4:53:49 PM 1362.4 1203.6
6/7/2019 4:53:50 PM 1338.6 1179.8
6/7/2019 4:53:51 PM 1318.5 1159.7
6/7/2019 4:53:52 PM 1305.4 1146.6
6/7/2019 4:53:53 PM 1290.6 1131.8
6/7/2019 4:53:54 PM 1210.3 1051.5
6/7/2019 4:53:55 PM 1181.6 1022.8
6/7/2019 4:53:56 PM 1149.2 990.4
6/7/2019 4:53:57 PM 1137.8 979.0
6/7/2019 4:53:58 PM 1126.8 968.0
6/7/2019 4:53:59 PM 1111.2 952.4
6/7/2019 4:54:00 PM 1098.5 939.7
6/7/2019 4:54:01 PM 1087.8 929.0
6/7/2019 4:54:02 PM 1015.6 856.8
6/7/2019 4:54:03 PM 1001.1 842.3
6/7/2019 4:54:04 PM 991.0 832.2
6/7/2019 4:54:05 PM 968.2 809.4
6/7/2019 4:54:06 PM 958.7 799.9
6/7/2019 4:54:07 PM 948.0 789.2
6/7/2019 4:54:08 PM 941.3 782.5
6/7/2019 4:54:09 PM 934.3 775.5
6/7/2019 4:54:10 PM 929.9 771.1
6/7/2019 4:54:11 PM 922.9 764.1
6/7/2019 4:54:12 PM 866.0 707.2
6/7/2019 4:54:13 PM 847.2 688.4
6/7/2019 4:54:14 PM 839.9 681.1
6/7/2019 4:54:15 PM 833.6 674.8
6/7/2019 4:54:16 PM 823.0 664.2
6/7/2019 4:54:17 PM 815.1 656.3
6/7/2019 4:54:18 PM 809.7 650.9
6/7/2019 4:54:19 PM 804.3 645.5
6/7/2019 4:54:20 PM 800.7 641.9
6/7/2019 4:54:21 PM 795.1 636.3
6/7/2019 4:54:22 PM 745.2 586.4
6/7/2019 4:54:23 PM 735.7 576.9
6/7/2019 4:54:24 PM 732.1 573.3
6/7/2019 4:54:25 PM 725.1 566.3
6/7/2019 4:54:26 PM 719.1 560.3
6/7/2019 4:54:27 PM 714.5 555.7
6/7/2019 4:54:28 PM 710.2 551.4
6/7/2019 4:54:29 PM 706.7 547.9
6/7/2019 4:54:30 PM 702.9 544.1
6/7/2019 4:54:31 PM 698.4 539.6
6/7/2019 4:54:32 PM 695.1 536.3
6/7/2019 4:54:33 PM 691.4 532.6
6/7/2019 4:54:34 PM 689.2 530.4
6/7/2019 4:54:35 PM 685.3 526.5
6/7/2019 4:54:36 PM 681.1 522.3
6/7/2019 4:54:37 PM 634.3 475.5
6/7/2019 4:54:38 PM 627.8 469.0
6/7/2019 4:54:39 PM 621.7 462.9
6/7/2019 4:54:40 PM 616.9 458.1
6/7/2019 4:54:41 PM 612.0 453.2
6/7/2019 4:54:42 PM 608.5 449.7
6/7/2019 4:54:43 PM 607.3 448.5
6/7/2019 4:54:44 PM 572.3 413.5
6/7/2019 4:54:45 PM 580.8 422.0
6/7/2019 4:54:46 PM 579.5 420.7
6/7/2019 4:54:47 PM 576.4 417.6
6/7/2019 4:54:48 PM 572.3 413.5
6/7/2019 4:54:49 PM 570.1 411.3
6/7/2019 4:54:50 PM 567.6 408.8
6/7/2019 4:54:51 PM 564.8 406.0
6/7/2019 4:54:52 PM 562.0 403.2
6/7/2019 4:54:53 PM 560.1 401.3
6/7/2019 4:54:54 PM 558.1 399.3
6/7/2019 4:54:55 PM 554.6 395.8
6/7/2019 4:54:56 PM 552.4 393.6
6/7/2019 4:54:57 PM 550.7 391.9
6/7/2019 4:54:58 PM 548.2 389.4
6/7/2019 4:54:59 PM 546.2 387.4
Page 391 of 452 August 2019
APPENDIX E54: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-2 Data Log
6/7/2019 4:55:00 PM 542.2 383.4
6/7/2019 4:55:01 PM 538.0 379.2
6/7/2019 4:55:02 PM 533.3 374.5
6/7/2019 4:55:03 PM 529.1 370.3
6/7/2019 4:55:04 PM 523.2 364.4
6/7/2019 4:55:05 PM 519.2 360.4
6/7/2019 4:55:06 PM 515.8 357.0
6/7/2019 4:55:07 PM 511.0 352.2
6/7/2019 4:55:08 PM 506.7 347.9
6/7/2019 4:55:09 PM 503.1 344.3
6/7/2019 4:55:10 PM 500.0 341.2
6/7/2019 4:55:11 PM 495.4 336.6
6/7/2019 4:55:12 PM 492.3 333.5
6/7/2019 4:55:13 PM 488.9 330.1
6/7/2019 4:55:14 PM 485.2 326.4
6/7/2019 4:55:15 PM 481.1 322.3
6/7/2019 4:55:16 PM 478.4 319.6
6/7/2019 4:55:17 PM 475.5 316.7
6/7/2019 4:55:18 PM 472.2 313.4
6/7/2019 4:55:19 PM 468.6 309.8
6/7/2019 4:55:20 PM 465.4 306.6
6/7/2019 4:55:21 PM 463.4 304.6
6/7/2019 4:55:22 PM 460.3 301.5
6/7/2019 4:55:23 PM 456.8 298.0
6/7/2019 4:55:24 PM 453.8 295.0
6/7/2019 4:55:25 PM 451.3 292.5
6/7/2019 4:55:26 PM 449.2 290.4
6/7/2019 4:55:27 PM 446.7 287.9
6/7/2019 4:55:28 PM 443.8 285.0
6/7/2019 4:55:29 PM 440.7 281.9
6/7/2019 4:55:30 PM 437.9 279.1
6/7/2019 4:55:31 PM 435.6 276.8
6/7/2019 4:55:32 PM 433.6 274.8
6/7/2019 4:55:33 PM 430.9 272.1
6/7/2019 4:55:34 PM 428.5 269.7
6/7/2019 4:55:35 PM 425.6 266.8
6/7/2019 4:55:36 PM 423.1 264.3
6/7/2019 4:55:37 PM 420.9 262.1
6/7/2019 4:55:38 PM 418.4 259.6
6/7/2019 4:55:39 PM 416.5 257.7
6/7/2019 4:55:40 PM 414.3 255.5
6/7/2019 4:55:41 PM 411.8 253.0
6/7/2019 4:55:42 PM 409.0 250.2
6/7/2019 4:55:43 PM 406.5 247.7
6/7/2019 4:55:44 PM 404.3 245.5
6/7/2019 4:55:45 PM 401.8 243.0
6/7/2019 4:55:46 PM 400.3 241.5
6/7/2019 4:55:47 PM 398.0 239.2
6/7/2019 4:55:48 PM 396.0 237.2
6/7/2019 4:55:49 PM 393.4 234.6
6/7/2019 4:55:50 PM 391.6 232.8
6/7/2019 4:55:51 PM 389.6 230.8
6/7/2019 4:55:52 PM 387.8 229.0
6/7/2019 4:55:53 PM 386.4 227.6
6/7/2019 4:55:54 PM 384.9 226.1
6/7/2019 4:55:55 PM 383.1 224.3
6/7/2019 4:55:56 PM 381.1 222.3
6/7/2019 4:55:57 PM 379.5 220.7
6/7/2019 4:55:58 PM 378.0 219.2
6/7/2019 4:55:59 PM 376.4 217.6
6/7/2019 4:56:00 PM 375.3 216.5
6/7/2019 4:56:01 PM 373.7 214.9
6/7/2019 4:56:02 PM 372.2 213.4
6/7/2019 4:56:03 PM 370.1 211.3
6/7/2019 4:56:04 PM 368.7 209.9
6/7/2019 4:56:05 PM 367.1 208.3
6/7/2019 4:56:06 PM 366.1 207.3
6/7/2019 4:56:07 PM 364.5 205.7
6/7/2019 4:56:08 PM 363.0 204.2
6/7/2019 4:56:09 PM 361.4 202.6
6/7/2019 4:56:10 PM 359.7 200.9
6/7/2019 4:56:11 PM 358.2 199.4
6/7/2019 4:56:12 PM 356.8 198.0
6/7/2019 4:56:13 PM 355.7 196.9
6/7/2019 4:56:14 PM 354.1 195.3
6/7/2019 4:56:15 PM 352.8 194.0
6/7/2019 4:56:16 PM 351.1 192.3
6/7/2019 4:56:17 PM 349.6 190.8
6/7/2019 4:56:18 PM 348.3 189.5
Page 392 of 452 August 2019
APPENDIX E54: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-2 Data Log
6/7/2019 4:56:19 PM 346.8 188.0
6/7/2019 4:56:20 PM 345.7 186.9
6/7/2019 4:56:21 PM 344.4 185.6
6/7/2019 4:56:22 PM 343.0 184.2
6/7/2019 4:56:23 PM 341.4 182.6
6/7/2019 4:56:24 PM 340.1 181.3
6/7/2019 4:56:25 PM 338.9 180.1
6/7/2019 4:56:26 PM 338.0 179.2
6/7/2019 4:56:27 PM 336.9 178.1
6/7/2019 4:56:28 PM 335.6 176.8
6/7/2019 4:56:29 PM 334.5 175.7
6/7/2019 4:56:30 PM 333.0 174.2
6/7/2019 4:56:31 PM 331.9 173.1
6/7/2019 4:56:32 PM 330.8 172.0
6/7/2019 4:56:33 PM 330.2 171.4
6/7/2019 4:56:34 PM 329.2 170.4
6/7/2019 4:56:35 PM 328.3 169.5
6/7/2019 4:56:36 PM 326.9 168.1
6/7/2019 4:56:37 PM 325.9 167.1
6/7/2019 4:56:38 PM 324.8 166.0
6/7/2019 4:56:39 PM 323.8 165.0
6/7/2019 4:56:40 PM 323.1 164.3
6/7/2019 4:56:41 PM 322.2 163.4
6/7/2019 4:56:42 PM 321.2 162.4
6/7/2019 4:56:43 PM 320.0 161.2
6/7/2019 4:56:44 PM 319.0 160.2
6/7/2019 4:56:45 PM 318.2 159.4
6/7/2019 4:56:46 PM 317.1 158.3
6/7/2019 4:56:47 PM 316.5 157.7
6/7/2019 4:56:48 PM 315.6 156.8
6/7/2019 4:56:49 PM 314.6 155.8
6/7/2019 4:56:50 PM 313.7 154.9
6/7/2019 4:56:51 PM 312.9 154.1
6/7/2019 4:56:52 PM 312.2 153.4
6/7/2019 4:56:53 PM 311.5 152.7
6/7/2019 4:56:54 PM 310.6 151.8
6/7/2019 4:56:55 PM 309.6 150.8
6/7/2019 4:56:56 PM 308.7 149.9
6/7/2019 4:56:57 PM 307.9 149.1
6/7/2019 4:56:58 PM 307.3 148.5
6/7/2019 4:56:59 PM 306.4 147.6
6/7/2019 4:57:00 PM 305.7 146.9
6/7/2019 4:57:01 PM 304.8 146.0
6/7/2019 4:57:02 PM 303.9 145.1
6/7/2019 4:57:03 PM 303.2 144.4
6/7/2019 4:57:04 PM 302.6 143.8
6/7/2019 4:57:05 PM 301.9 143.1
6/7/2019 4:57:06 PM 301.0 142.2
6/7/2019 4:57:07 PM 300.2 141.4
6/7/2019 4:57:08 PM 299.6 140.8
6/7/2019 4:57:09 PM 299.0 140.2
6/7/2019 4:57:10 PM 298.4 139.6
6/7/2019 4:57:11 PM 297.6 138.8
6/7/2019 4:57:12 PM 296.8 138.0
6/7/2019 4:57:13 PM 296.2 137.4
6/7/2019 4:57:14 PM 295.4 136.6
6/7/2019 4:57:15 PM 294.7 135.9
6/7/2019 4:57:16 PM 294.2 135.4
6/7/2019 4:57:17 PM 293.5 134.7
6/7/2019 4:57:18 PM 292.9 134.1
6/7/2019 4:57:19 PM 292.0 133.2
6/7/2019 4:57:20 PM 291.4 132.6
6/7/2019 4:57:21 PM 290.8 132.0
6/7/2019 4:57:22 PM 290.2 131.4
6/7/2019 4:57:23 PM 289.5 130.7
6/7/2019 4:57:24 PM 288.7 129.9
6/7/2019 4:57:25 PM 287.9 129.1
6/7/2019 4:57:26 PM 287.5 128.7
6/7/2019 4:57:27 PM 286.8 128.0
6/7/2019 4:57:28 PM 286.0 127.2
6/7/2019 4:57:29 PM 285.3 126.5
6/7/2019 4:57:30 PM 284.7 125.9
6/7/2019 4:57:31 PM 284.2 125.4
6/7/2019 4:57:32 PM 283.4 124.6
6/7/2019 4:57:33 PM 282.9 124.1
6/7/2019 4:57:34 PM 282.2 123.4
6/7/2019 4:57:35 PM 281.5 122.7
6/7/2019 4:57:36 PM 281.1 122.3
6/7/2019 4:57:37 PM 280.3 121.5
Page 393 of 452 August 2019
APPENDIX E54: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-2 Data Log
6/7/2019 4:57:38 PM 279.8 121.0
6/7/2019 4:57:39 PM 279.2 120.4
6/7/2019 4:57:40 PM 278.7 119.9
6/7/2019 4:57:41 PM 278.2 119.4
6/7/2019 4:57:42 PM 277.6 118.8
6/7/2019 4:57:43 PM 277.1 118.3
6/7/2019 4:57:44 PM 276.5 117.7
6/7/2019 4:57:45 PM 275.8 117.0
6/7/2019 4:57:46 PM 275.4 116.6
6/7/2019 4:57:47 PM 274.8 116.0
6/7/2019 4:57:48 PM 274.3 115.5
6/7/2019 4:57:49 PM 273.7 114.9
6/7/2019 4:57:50 PM 273.4 114.6
6/7/2019 4:57:51 PM 273.0 114.2
6/7/2019 4:57:52 PM 272.3 113.5
6/7/2019 4:57:53 PM 271.8 113.0
6/7/2019 4:57:54 PM 271.6 112.8
6/7/2019 4:57:55 PM 271.1 112.3
6/7/2019 4:57:56 PM 270.5 111.7
6/7/2019 4:57:57 PM 270.2 111.4
6/7/2019 4:57:58 PM 269.7 110.9
6/7/2019 4:57:59 PM 269.3 110.5
6/7/2019 4:58:00 PM 268.8 110.0
6/7/2019 4:58:01 PM 268.4 109.6
6/7/2019 4:58:02 PM 268.0 109.2
6/7/2019 4:58:03 PM 267.5 108.7
6/7/2019 4:58:04 PM 267.0 108.2
6/7/2019 4:58:05 PM 266.6 107.8
6/7/2019 4:58:06 PM 266.3 107.5
6/7/2019 4:58:07 PM 265.9 107.1
6/7/2019 4:58:08 PM 265.3 106.5
6/7/2019 4:58:09 PM 264.9 106.1
6/7/2019 4:58:10 PM 264.6 105.8
6/7/2019 4:58:11 PM 264.1 105.3
6/7/2019 4:58:12 PM 263.7 104.9
6/7/2019 4:58:13 PM 263.4 104.6
6/7/2019 4:58:14 PM 263.0 104.2
6/7/2019 4:58:15 PM 262.5 103.7
6/7/2019 4:58:16 PM 262.1 103.3
6/7/2019 4:58:17 PM 261.7 102.9
6/7/2019 4:58:18 PM 261.4 102.6
6/7/2019 4:58:19 PM 261.0 102.2
6/7/2019 4:58:20 PM 260.4 101.6
6/7/2019 4:58:21 PM 260.0 101.2
6/7/2019 4:58:22 PM 259.7 100.9
6/7/2019 4:58:23 PM 259.3 100.5
6/7/2019 4:58:24 PM 258.9 100.1
6/7/2019 4:58:25 PM 258.3 99.5
6/7/2019 4:58:26 PM 257.9 99.1
6/7/2019 4:58:27 PM 257.5 98.7
6/7/2019 4:58:28 PM 257.1 98.3
6/7/2019 4:58:29 PM 256.7 97.9
6/7/2019 4:58:30 PM 256.2 97.4
6/7/2019 4:58:31 PM 255.6 96.8
6/7/2019 4:58:32 PM 255.2 96.4
6/7/2019 4:58:33 PM 254.8 96.0
6/7/2019 4:58:34 PM 254.3 95.5
6/7/2019 4:58:35 PM 254.0 95.2
6/7/2019 4:58:36 PM 253.6 94.8
6/7/2019 4:58:37 PM 253.2 94.4
6/7/2019 4:58:38 PM 252.7 93.9
6/7/2019 4:58:39 PM 252.4 93.6
6/7/2019 4:58:40 PM 252.0 93.2
6/7/2019 4:58:41 PM 251.7 92.9
6/7/2019 4:58:42 PM 251.4 92.6
6/7/2019 4:58:43 PM 251.0 92.2
6/7/2019 4:58:44 PM 250.6 91.8
6/7/2019 4:58:45 PM 250.2 91.4
6/7/2019 4:58:46 PM 249.8 91.0
6/7/2019 4:58:47 PM 249.4 90.6
6/7/2019 4:58:48 PM 249.2 90.4
6/7/2019 4:58:49 PM 248.8 90.0
6/7/2019 4:58:50 PM 248.4 89.6
6/7/2019 4:58:51 PM 247.9 89.1
6/7/2019 4:58:52 PM 247.6 88.8
6/7/2019 4:58:53 PM 247.2 88.4
6/7/2019 4:58:54 PM 246.8 88.0
6/7/2019 4:58:55 PM 246.5 87.7
6/7/2019 4:58:56 PM 246.2 87.4
Page 394 of 452 August 2019
APPENDIX E54: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-2 Data Log
6/7/2019 4:58:57 PM 245.8 87.0
6/7/2019 4:58:58 PM 245.4 86.6
6/7/2019 4:58:59 PM 245.1 86.3
6/7/2019 4:59:00 PM 244.8 86.0
6/7/2019 4:59:01 PM 244.5 85.7
6/7/2019 4:59:02 PM 244.2 85.4
6/7/2019 4:59:03 PM 243.9 85.1
6/7/2019 4:59:04 PM 243.6 84.8
6/7/2019 4:59:05 PM 243.2 84.4
6/7/2019 4:59:06 PM 242.9 84.1
6/7/2019 4:59:07 PM 242.6 83.8
6/7/2019 4:59:08 PM 242.4 83.6
6/7/2019 4:59:09 PM 242.1 83.3
6/7/2019 4:59:10 PM 241.8 83.0
6/7/2019 4:59:11 PM 241.4 82.6
6/7/2019 4:59:12 PM 241.2 82.4
6/7/2019 4:59:13 PM 240.9 82.1
6/7/2019 4:59:14 PM 240.7 81.9
6/7/2019 4:59:15 PM 240.4 81.6
6/7/2019 4:59:16 PM 240.1 81.3
6/7/2019 4:59:17 PM 239.8 81.0
6/7/2019 4:59:18 PM 239.5 80.7
6/7/2019 4:59:19 PM 239.2 80.4
6/7/2019 4:59:20 PM 239.0 80.2
6/7/2019 4:59:21 PM 238.7 79.9
6/7/2019 4:59:22 PM 238.4 79.6
6/7/2019 4:59:23 PM 238.1 79.3
6/7/2019 4:59:24 PM 237.8 79.0
6/7/2019 4:59:25 PM 237.5 78.7
6/7/2019 4:59:26 PM 237.2 78.4
6/7/2019 4:59:27 PM 236.9 78.1
6/7/2019 4:59:28 PM 236.6 77.8
6/7/2019 4:59:29 PM 236.4 77.6
6/7/2019 4:59:30 PM 236.0 77.2
6/7/2019 4:59:31 PM 235.8 77.0
6/7/2019 4:59:32 PM 235.4 76.6
6/7/2019 4:59:33 PM 235.1 76.3
6/7/2019 4:59:34 PM 234.7 75.9
6/7/2019 4:59:35 PM 234.5 75.7
6/7/2019 4:59:36 PM 234.2 75.4
6/7/2019 4:59:37 PM 233.9 75.1
6/7/2019 4:59:38 PM 233.6 74.8
6/7/2019 4:59:39 PM 233.2 74.4
6/7/2019 4:59:40 PM 232.9 74.1
6/7/2019 4:59:41 PM 232.6 73.8
6/7/2019 4:59:42 PM 232.3 73.5
6/7/2019 4:59:43 PM 232.1 73.3
6/7/2019 4:59:44 PM 231.7 72.9
6/7/2019 4:59:45 PM 231.4 72.6
6/7/2019 4:59:46 PM 231.0 72.2
6/7/2019 4:59:47 PM 230.7 71.9
6/7/2019 4:59:48 PM 230.4 71.6
6/7/2019 4:59:49 PM 230.2 71.4
6/7/2019 4:59:50 PM 229.9 71.1
6/7/2019 4:59:51 PM 229.6 70.8
6/7/2019 4:59:52 PM 229.2 70.4
6/7/2019 4:59:53 PM 229.0 70.2
6/7/2019 4:59:54 PM 228.7 69.9
6/7/2019 4:59:55 PM 228.5 69.7
6/7/2019 4:59:56 PM 228.3 69.5
6/7/2019 4:59:57 PM 228.0 69.2
6/7/2019 4:59:58 PM 227.7 68.9
6/7/2019 4:59:59 PM 227.5 68.7
6/7/2019 5:00:00 PM 227.3 68.5
6/7/2019 5:00:01 PM 227.0 68.2
6/7/2019 5:00:02 PM 226.7 67.9
6/7/2019 5:00:03 PM 226.5 67.7
6/7/2019 5:00:04 PM 226.2 67.4
6/7/2019 5:00:05 PM 226.0 67.2
6/7/2019 5:00:06 PM 225.8 67.0
6/7/2019 5:00:07 PM 225.6 66.8
6/7/2019 5:00:08 PM 225.3 66.5
6/7/2019 5:00:09 PM 225.0 66.2
6/7/2019 5:00:10 PM 224.8 66.0
6/7/2019 5:00:11 PM 224.7 65.9
6/7/2019 5:00:12 PM 224.5 65.7
6/7/2019 5:00:13 PM 224.2 65.4
6/7/2019 5:00:14 PM 224.0 65.2
6/7/2019 5:00:15 PM 223.8 65.0
Page 395 of 452 August 2019
APPENDIX E54: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-2 Data Log
6/7/2019 5:00:16 PM 223.6 64.8
6/7/2019 5:00:17 PM 223.4 64.6
6/7/2019 5:00:18 PM 223.2 64.4
6/7/2019 5:00:19 PM 222.9 64.1
6/7/2019 5:00:20 PM 222.7 63.9
6/7/2019 5:00:21 PM 222.6 63.8
6/7/2019 5:00:22 PM 222.4 63.6
6/7/2019 5:00:23 PM 222.1 63.3
6/7/2019 5:00:24 PM 221.9 63.1
6/7/2019 5:00:25 PM 221.8 63.0
6/7/2019 5:00:26 PM 221.6 62.8
6/7/2019 5:00:27 PM 221.3 62.5
6/7/2019 5:00:28 PM 221.1 62.3
6/7/2019 5:00:29 PM 220.9 62.1
6/7/2019 5:00:30 PM 220.8 62.0
6/7/2019 5:00:31 PM 220.6 61.8
6/7/2019 5:00:32 PM 220.4 61.6
6/7/2019 5:00:33 PM 220.2 61.4
6/7/2019 5:00:34 PM 220.0 61.2
6/7/2019 5:00:35 PM 219.8 61.0
6/7/2019 5:00:36 PM 219.6 60.8
6/7/2019 5:00:37 PM 219.4 60.6
6/7/2019 5:00:38 PM 219.2 60.4
6/7/2019 5:00:39 PM 219.1 60.3
6/7/2019 5:00:40 PM 218.9 60.1
6/7/2019 5:00:41 PM 218.7 59.9
6/7/2019 5:00:42 PM 218.5 59.7
6/7/2019 5:00:43 PM 218.4 59.6
6/7/2019 5:00:44 PM 218.2 59.4
6/7/2019 5:00:45 PM 218.0 59.2
6/7/2019 5:00:46 PM 217.9 59.1
6/7/2019 5:00:47 PM 217.7 58.9
6/7/2019 5:00:48 PM 217.5 58.7
6/7/2019 5:00:49 PM 217.3 58.5
6/7/2019 5:00:50 PM 217.2 58.4
6/7/2019 5:00:51 PM 217.0 58.2
6/7/2019 5:00:52 PM 216.8 58.0
6/7/2019 5:00:53 PM 216.6 57.8
6/7/2019 5:00:54 PM 216.4 57.6
6/7/2019 5:00:55 PM 216.2 57.4
6/7/2019 5:00:56 PM 216.0 57.2
6/7/2019 5:00:57 PM 215.8 57.0
6/7/2019 5:00:58 PM 215.6 56.8
6/7/2019 5:00:59 PM 215.5 56.7
6/7/2019 5:01:00 PM 215.2 56.4
6/7/2019 5:01:01 PM 215.1 56.3
6/7/2019 5:01:02 PM 214.9 56.1
6/7/2019 5:01:03 PM 214.6 55.8
6/7/2019 5:01:04 PM 214.4 55.6
6/7/2019 5:01:05 PM 214.3 55.5
6/7/2019 5:01:06 PM 214.1 55.3
6/7/2019 5:01:07 PM 213.9 55.1
6/7/2019 5:01:08 PM 213.7 54.9
6/7/2019 5:01:09 PM 213.6 54.8
6/7/2019 5:01:10 PM 213.4 54.6
6/7/2019 5:01:11 PM 213.2 54.4
6/7/2019 5:01:12 PM 213.1 54.3
6/7/2019 5:01:13 PM 212.9 54.1
6/7/2019 5:01:14 PM 212.8 54.0
6/7/2019 5:01:15 PM 212.6 53.8
6/7/2019 5:01:16 PM 212.4 53.6
6/7/2019 5:01:17 PM 212.3 53.5
6/7/2019 5:01:18 PM 212.1 53.3
6/7/2019 5:01:19 PM 211.9 53.1
6/7/2019 5:01:20 PM 211.8 53.0
6/7/2019 5:01:21 PM 211.6 52.8
6/7/2019 5:01:22 PM 211.4 52.6
6/7/2019 5:01:23 PM 211.2 52.4
6/7/2019 5:01:24 PM 211.0 52.2
6/7/2019 5:01:25 PM 210.9 52.1
6/7/2019 5:01:26 PM 210.7 51.9
6/7/2019 5:01:27 PM 210.5 51.7
6/7/2019 5:01:28 PM 210.3 51.5
6/7/2019 5:01:29 PM 210.2 51.4
6/7/2019 5:01:30 PM 210.0 51.2
6/7/2019 5:01:31 PM 209.9 51.1
6/7/2019 5:01:32 PM 209.7 50.9
6/7/2019 5:01:33 PM 209.6 50.8
6/7/2019 5:01:34 PM 209.4 50.6
Page 396 of 452 August 2019
APPENDIX E54: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-2 Data Log
6/7/2019 5:01:35 PM 209.2 50.4
6/7/2019 5:01:36 PM 209.1 50.3
6/7/2019 5:01:37 PM 208.9 50.1
6/7/2019 5:01:38 PM 208.8 50.0
6/7/2019 5:01:39 PM 208.7 49.9
6/7/2019 5:01:40 PM 208.6 49.8
6/7/2019 5:01:41 PM 208.4 49.6
6/7/2019 5:01:42 PM 208.3 49.5
6/7/2019 5:01:43 PM 208.1 49.3
6/7/2019 5:01:44 PM 208.0 49.2
6/7/2019 5:01:45 PM 207.9 49.1
6/7/2019 5:01:46 PM 207.8 49.0
6/7/2019 5:01:47 PM 207.7 48.9
6/7/2019 5:01:48 PM 207.6 48.8
6/7/2019 5:01:49 PM 207.5 48.7
6/7/2019 5:01:50 PM 207.4 48.6
6/7/2019 5:01:51 PM 207.3 48.5
6/7/2019 5:01:52 PM 207.2 48.4
6/7/2019 5:01:53 PM 207.1 48.3
6/7/2019 5:01:54 PM 206.9 48.1
6/7/2019 5:01:55 PM 206.8 48.0
6/7/2019 5:01:56 PM 206.7 47.9
6/7/2019 5:01:57 PM 206.5 47.7
6/7/2019 5:01:58 PM 206.4 47.6
6/7/2019 5:01:59 PM 206.3 47.5
6/7/2019 5:02:00 PM 206.2 47.4
6/7/2019 5:02:01 PM 206.0 47.2
6/7/2019 5:02:02 PM 205.9 47.1
6/7/2019 5:02:03 PM 205.7 46.9
6/7/2019 5:02:04 PM 205.6 46.8
6/7/2019 5:02:05 PM 205.4 46.6
6/7/2019 5:02:06 PM 205.3 46.5
6/7/2019 5:02:07 PM 205.1 46.3
6/7/2019 5:02:08 PM 205.0 46.2
6/7/2019 5:02:09 PM 204.8 46.0
6/7/2019 5:02:10 PM 204.6 45.8
6/7/2019 5:02:11 PM 204.4 45.6
6/7/2019 5:02:12 PM 204.3 45.5
6/7/2019 5:02:13 PM 204.2 45.4
6/7/2019 5:02:14 PM 204.0 45.2
6/7/2019 5:02:15 PM 203.8 45.0
6/7/2019 5:02:16 PM 203.7 44.9
6/7/2019 5:02:17 PM 203.5 44.7
6/7/2019 5:02:18 PM 203.3 44.5
6/7/2019 5:02:19 PM 203.2 44.4
6/7/2019 5:02:20 PM 203.0 44.2
6/7/2019 5:02:21 PM 202.9 44.1
6/7/2019 5:02:22 PM 202.7 43.9
6/7/2019 5:02:23 PM 202.5 43.7
6/7/2019 5:02:24 PM 202.4 43.6
6/7/2019 5:02:25 PM 202.2 43.4
6/7/2019 5:02:26 PM 202.1 43.3
6/7/2019 5:02:27 PM 201.9 43.1
6/7/2019 5:02:28 PM 201.8 43.0
6/7/2019 5:02:29 PM 201.6 42.8
6/7/2019 5:02:30 PM 201.4 42.6
6/7/2019 5:02:31 PM 201.3 42.5
6/7/2019 5:02:32 PM 201.1 42.3
6/7/2019 5:02:33 PM 201.0 42.2
6/7/2019 5:02:34 PM 200.9 42.1
6/7/2019 5:02:35 PM 200.8 42.0
6/7/2019 5:02:36 PM 200.6 41.8
6/7/2019 5:02:37 PM 200.4 41.6
6/7/2019 5:02:38 PM 200.3 41.5
6/7/2019 5:02:39 PM 200.2 41.4
6/7/2019 5:02:40 PM 200.1 41.3
6/7/2019 5:02:41 PM 199.9 41.1
6/7/2019 5:02:42 PM 199.8 41.0
6/7/2019 5:02:43 PM 199.7 40.9
6/7/2019 5:02:44 PM 199.5 40.7
6/7/2019 5:02:45 PM 199.4 40.6
6/7/2019 5:02:46 PM 199.3 40.5
6/7/2019 5:02:47 PM 199.2 40.4
6/7/2019 5:02:48 PM 199.1 40.3
6/7/2019 5:02:49 PM 199.0 40.2
6/7/2019 5:02:50 PM 198.9 40.1
6/7/2019 5:02:51 PM 198.8 40.0
6/7/2019 5:02:52 PM 198.7 39.9
6/7/2019 5:02:53 PM 198.6 39.8
Page 397 of 452 August 2019
APPENDIX E54: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-2 Data Log
6/7/2019 5:02:54 PM 198.6 39.8
6/7/2019 5:02:55 PM 198.5 39.7
6/7/2019 5:02:56 PM 198.5 39.7
6/7/2019 5:02:57 PM 198.4 39.6
6/7/2019 5:02:58 PM 198.4 39.6
6/7/2019 5:02:59 PM 198.4 39.6
6/7/2019 5:03:00 PM 198.4 39.6
6/7/2019 5:03:01 PM 198.4 39.6
6/7/2019 5:03:02 PM 198.5 39.7
6/7/2019 5:03:03 PM 198.5 39.7
6/7/2019 5:03:04 PM 198.6 39.8
6/7/2019 5:03:05 PM 198.7 39.9
6/7/2019 5:03:06 PM 198.7 39.9
6/7/2019 5:03:07 PM 198.8 40.0
6/7/2019 5:03:08 PM 198.9 40.1
6/7/2019 5:03:09 PM 198.9 40.1
6/7/2019 5:03:10 PM 199.0 40.2
6/7/2019 5:03:11 PM 199.1 40.3
6/7/2019 5:03:12 PM 199.1 40.3
6/7/2019 5:03:13 PM 199.1 40.3
6/7/2019 5:03:14 PM 199.2 40.4
6/7/2019 5:03:15 PM 199.2 40.4
6/7/2019 5:03:16 PM 199.2 40.4
6/7/2019 5:03:17 PM 199.1 40.3
6/7/2019 5:03:18 PM 199.1 40.3
6/7/2019 5:03:19 PM 199.0 40.2
6/7/2019 5:03:20 PM 199.0 40.2
6/7/2019 5:03:21 PM 198.9 40.1
6/7/2019 5:03:22 PM 198.8 40.0
6/7/2019 5:03:23 PM 198.7 39.9
6/7/2019 5:03:24 PM 198.5 39.7
6/7/2019 5:03:25 PM 198.4 39.6
6/7/2019 5:03:26 PM 198.3 39.5
6/7/2019 5:03:27 PM 198.1 39.3
6/7/2019 5:03:28 PM 198.0 39.2
6/7/2019 5:03:29 PM 197.8 39.0
6/7/2019 5:03:30 PM 197.7 38.9
6/7/2019 5:03:31 PM 197.5 38.7
6/7/2019 5:03:32 PM 197.3 38.5
6/7/2019 5:03:33 PM 197.1 38.3
6/7/2019 5:03:34 PM 196.9 38.1
6/7/2019 5:03:35 PM 196.7 37.9
6/7/2019 5:03:36 PM 196.6 37.8
6/7/2019 5:03:37 PM 196.3 37.5
6/7/2019 5:03:38 PM 196.1 37.3
6/7/2019 5:03:39 PM 196.0 37.2
6/7/2019 5:03:40 PM 195.8 37.0
6/7/2019 5:03:41 PM 195.7 36.9
6/7/2019 5:03:42 PM 195.5 36.7
6/7/2019 5:03:43 PM 195.3 36.5
6/7/2019 5:03:44 PM 195.2 36.4
6/7/2019 5:03:45 PM 195.1 36.3
6/7/2019 5:03:46 PM 194.9 36.1
6/7/2019 5:03:47 PM 194.8 36.0
6/7/2019 5:03:48 PM 194.7 35.9
6/7/2019 5:03:49 PM 194.6 35.8
6/7/2019 5:03:50 PM 194.5 35.7
6/7/2019 5:03:51 PM 194.4 35.6
6/7/2019 5:03:52 PM 194.2 35.4
6/7/2019 5:03:53 PM 194.1 35.3
6/7/2019 5:03:54 PM 194.1 35.3
6/7/2019 5:03:55 PM 193.9 35.1
6/7/2019 5:03:56 PM 193.8 35.0
6/7/2019 5:03:57 PM 193.7 34.9
6/7/2019 5:03:58 PM 193.6 34.8
6/7/2019 5:03:59 PM 193.4 34.6
6/7/2019 5:04:00 PM 193.3 34.5
6/7/2019 5:04:01 PM 193.2 34.4
6/7/2019 5:04:02 PM 193.1 34.3
6/7/2019 5:04:03 PM 193.0 34.2
6/7/2019 5:04:04 PM 192.9 34.1
6/7/2019 5:04:05 PM 192.8 34.0
6/7/2019 5:04:06 PM 192.6 33.8
6/7/2019 5:04:07 PM 192.5 33.7
6/7/2019 5:04:08 PM 192.4 33.6
6/7/2019 5:04:09 PM 192.3 33.5
6/7/2019 5:04:10 PM 192.2 33.4
6/7/2019 5:04:11 PM 192.1 33.3
6/7/2019 5:04:12 PM 192.0 33.2
Page 398 of 452 August 2019
APPENDIX E54: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-2 Data Log
6/7/2019 5:04:13 PM 192.0 33.2
6/7/2019 5:04:14 PM 191.8 33.0
6/7/2019 5:04:15 PM 191.8 33.0
6/7/2019 5:04:16 PM 191.7 32.9
6/7/2019 5:04:17 PM 191.6 32.8
6/7/2019 5:04:18 PM 191.5 32.7
6/7/2019 5:04:19 PM 191.4 32.6
6/7/2019 5:04:20 PM 191.3 32.5
6/7/2019 5:04:21 PM 191.3 32.5
6/7/2019 5:04:22 PM 191.2 32.4
6/7/2019 5:04:23 PM 191.1 32.3
6/7/2019 5:04:24 PM 191.0 32.2
6/7/2019 5:04:25 PM 190.9 32.1
6/7/2019 5:04:26 PM 190.8 32.0
6/7/2019 5:04:27 PM 190.8 32.0
6/7/2019 5:04:28 PM 190.7 31.9
6/7/2019 5:04:29 PM 190.6 31.8
6/7/2019 5:04:30 PM 190.5 31.7
6/7/2019 5:04:31 PM 190.4 31.6
6/7/2019 5:04:32 PM 190.3 31.5
6/7/2019 5:04:33 PM 190.2 31.4
6/7/2019 5:04:34 PM 190.2 31.4
6/7/2019 5:04:35 PM 190.1 31.3
6/7/2019 5:04:36 PM 190.0 31.2
6/7/2019 5:04:37 PM 189.9 31.1
6/7/2019 5:04:38 PM 189.8 31.0
6/7/2019 5:04:39 PM 189.7 30.9
6/7/2019 5:04:40 PM 189.6 30.8
6/7/2019 5:04:41 PM 189.5 30.7
6/7/2019 5:04:42 PM 189.4 30.6
6/7/2019 5:04:43 PM 189.3 30.5
6/7/2019 5:04:44 PM 189.2 30.4
6/7/2019 5:04:45 PM 189.1 30.3
6/7/2019 5:04:46 PM 189.1 30.3
6/7/2019 5:04:47 PM 188.9 30.1
6/7/2019 5:04:48 PM 188.8 30.0
6/7/2019 5:04:49 PM 188.7 29.9
6/7/2019 5:04:50 PM 188.6 29.8
6/7/2019 5:04:51 PM 188.5 29.7
6/7/2019 5:04:52 PM 188.4 29.6
6/7/2019 5:04:53 PM 188.3 29.5
6/7/2019 5:04:54 PM 188.2 29.4
6/7/2019 5:04:55 PM 188.1 29.3
6/7/2019 5:04:56 PM 188.0 29.2
6/7/2019 5:04:57 PM 187.9 29.1
6/7/2019 5:04:58 PM 187.8 29.0
6/7/2019 5:04:59 PM 187.7 28.9
6/7/2019 5:05:00 PM 187.6 28.8
6/7/2019 5:05:01 PM 187.5 28.7
6/7/2019 5:05:02 PM 187.4 28.6
6/7/2019 5:05:03 PM 187.3 28.5
6/7/2019 5:05:04 PM 187.2 28.4
6/7/2019 5:05:05 PM 187.1 28.3
6/7/2019 5:05:06 PM 187.0 28.2
6/7/2019 5:05:07 PM 186.9 28.1
6/7/2019 5:05:08 PM 186.8 28.0
6/7/2019 5:05:09 PM 186.7 27.9
6/7/2019 5:05:10 PM 186.7 27.9
6/7/2019 5:05:11 PM 186.6 27.8
6/7/2019 5:05:12 PM 186.5 27.7
6/7/2019 5:05:13 PM 186.4 27.6
6/7/2019 5:05:14 PM 186.4 27.6
6/7/2019 5:05:15 PM 186.3 27.5
6/7/2019 5:05:16 PM 186.2 27.4
6/7/2019 5:05:17 PM 186.2 27.4
6/7/2019 5:05:18 PM 186.1 27.3
6/7/2019 5:05:19 PM 186.0 27.2
6/7/2019 5:05:20 PM 186.0 27.2
6/7/2019 5:05:21 PM 185.9 27.1
6/7/2019 5:05:22 PM 185.9 27.1
6/7/2019 5:05:23 PM 185.8 27.0
6/7/2019 5:05:24 PM 185.7 26.9
6/7/2019 5:05:25 PM 185.7 26.9
6/7/2019 5:05:26 PM 185.6 26.8
6/7/2019 5:05:27 PM 185.6 26.8
6/7/2019 5:05:28 PM 185.5 26.7
6/7/2019 5:05:29 PM 185.4 26.6
6/7/2019 5:05:30 PM 185.4 26.6
Page 399 of 452 August 2019
APPENDIX E54: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-C1 TEST-2 1625
SEEP-C1 TEST-2 1626
SEEP-C1 TEST-2 1627
SEEP-C1 TEST-2 1628
Location EC Reading
(µS/cms)
SEEP-C1 TEST-2 1,115
SEEP-C1 TEST-2 2,150
SEEP-C1 TEST-2 16,651
SEEP-C1 TEST-2 132,589
q 300,300
K 1.3293
0.8
13.3
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)
(µS/cms)
(µS/cms)
24.1
24.2
24.2
(µS/cms)(°C)
Table E2 SEEP-C1 TEST-2 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
142.9 21.4
141.8 21.8
142.6 21.4
Calibration Temperature
154.3 21.7
Average 145.4 (µS/cms)
Geometric Mean 145.3
Average (pre-test)158.8
Average (post-test)187.2
Table E3 SEEP-C1 TEST-2 YSI Salt Dilution Calibration Data
Integral of Conductivity
Data Curve
SUM:Δt(E
Ct-ECbkg)477,164.5 (s) . (µS/cms)
(mg/L)(°C)
100
1,000
10,000
100,000 24.1
Table E4 SEEP-C1 TEST-2 Flow Calculation Summary
Mass of Salt injected mg
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline,
Watershed Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Slope of Calibration Curve (µS/cms) / (mg/L)
Calculated Flow Rate Q
L/s
GPM
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 400 of 452 August 2019
APPENDIX E55: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 5:12:23 PM 164.0 -
6/7/2019 5:12:24 PM 164.0 -
6/7/2019 5:12:25 PM 164.0 -
6/7/2019 5:12:26 PM 163.9 -
6/7/2019 5:12:27 PM 163.9 -
6/7/2019 5:12:28 PM 163.9 -
6/7/2019 5:12:29 PM 163.8 -
6/7/2019 5:12:30 PM 163.8 -
6/7/2019 5:12:31 PM 163.7 -
6/7/2019 5:12:32 PM 163.7 -
6/7/2019 5:12:33 PM 163.6 -
6/7/2019 5:12:34 PM 163.5 -
6/7/2019 5:12:35 PM 163.5 -
6/7/2019 5:12:36 PM 163.4 -
6/7/2019 5:12:37 PM 163.3 -
6/7/2019 5:12:38 PM 163.3 -
6/7/2019 5:12:39 PM 163.3 -
6/7/2019 5:12:40 PM 163.2 -
6/7/2019 5:12:41 PM 163.2 -
6/7/2019 5:12:42 PM 163.2 -
6/7/2019 5:12:43 PM 163.2 -
6/7/2019 5:12:44 PM 163.2 -
6/7/2019 5:12:45 PM 163.2 -
6/7/2019 5:12:46 PM 163.2 -
6/7/2019 5:12:47 PM 163.2 -
6/7/2019 5:12:48 PM 163.2 -
6/7/2019 5:12:49 PM 163.2 -
6/7/2019 5:12:50 PM 163.2 -
6/7/2019 5:12:51 PM 163.2 -
6/7/2019 5:12:52 PM 163.2 -
6/7/2019 5:12:53 PM 163.1 -
6/7/2019 5:12:54 PM 163.1 -
6/7/2019 5:12:55 PM 163.1 -
6/7/2019 5:12:56 PM 163.1 -
6/7/2019 5:12:57 PM 163.0 -
6/7/2019 5:12:58 PM 163.0 -
6/7/2019 5:12:59 PM 163.0 -
6/7/2019 5:13:00 PM 163.0 -
6/7/2019 5:13:01 PM 162.9 -
6/7/2019 5:13:02 PM 162.9 -
6/7/2019 5:13:03 PM 163.0 -
6/7/2019 5:13:04 PM 163.1 -
6/7/2019 5:13:05 PM 163.7 -
6/7/2019 5:13:06 PM 164.9 -
6/7/2019 5:13:07 PM 218.5 55.1
6/7/2019 5:13:08 PM 265.9 102.5
6/7/2019 5:13:09 PM 372.2 208.8
6/7/2019 5:13:10 PM 498.2 334.8
6/7/2019 5:13:11 PM 686.7 523.3
6/7/2019 5:13:12 PM 1152.7 989.3
6/7/2019 5:13:13 PM 1387.1 1223.7
6/7/2019 5:13:14 PM 1922.3 1758.9
6/7/2019 5:13:15 PM 2488.5 2325.1
6/7/2019 5:13:16 PM 3161.7 2998.3
6/7/2019 5:13:17 PM 3964.7 3801.3
6/7/2019 5:13:18 PM 4662.6 4499.2
6/7/2019 5:13:19 PM 5445.5 5282.1
6/7/2019 5:13:20 PM 6736.9 6573.5
6/7/2019 5:13:21 PM 7032.4 6869.0
6/7/2019 5:13:22 PM 8457.9 8294.5
6/7/2019 5:13:23 PM 9345.7 9182.3
6/7/2019 5:13:24 PM 9740.9 9577.5
6/7/2019 5:13:25 PM 10228.9 10065.5
6/7/2019 5:13:26 PM 10445.5 10282.1
6/7/2019 5:13:27 PM 10630.8 10467.4
6/7/2019 5:13:28 PM 11474.4 11311.0
6/7/2019 5:13:29 PM 11593.4 11430.0
6/7/2019 5:13:30 PM 11651.7 11488.3
6/7/2019 5:13:31 PM 11668.3 11504.9
6/7/2019 5:13:32 PM 11662.4 11499.0
Table E1 SEEP-C1 TEST-3 Data Log
Page 401 of 452 August 2019
APPENDIX E55: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-3 Data Log
6/7/2019 5:13:33 PM 11632.3 11468.9
6/7/2019 5:13:34 PM 11576.9 11413.5
6/7/2019 5:13:35 PM 11500.0 11336.6
6/7/2019 5:13:36 PM 11412.7 11249.3
6/7/2019 5:13:37 PM 10517.0 10353.6
6/7/2019 5:13:38 PM 10256.3 10092.9
6/7/2019 5:13:39 PM 9859.0 9695.6
6/7/2019 5:13:40 PM 9743.6 9580.2
6/7/2019 5:13:41 PM 9482.2 9318.8
6/7/2019 5:13:42 PM 8784.0 8620.6
6/7/2019 5:13:43 PM 8472.1 8308.7
6/7/2019 5:13:44 PM 7978.5 7815.1
6/7/2019 5:13:45 PM 7600.1 7436.7
6/7/2019 5:13:46 PM 7536.2 7372.8
6/7/2019 5:13:47 PM 7385.5 7222.1
6/7/2019 5:13:48 PM 6685.6 6522.2
6/7/2019 5:13:49 PM 6296.2 6132.8
6/7/2019 5:13:50 PM 6006.7 5843.3
6/7/2019 5:13:51 PM 5682.1 5518.7
6/7/2019 5:13:52 PM 5592.0 5428.6
6/7/2019 5:13:53 PM 5065.0 4901.6
6/7/2019 5:13:54 PM 4854.4 4691.0
6/7/2019 5:13:55 PM 4636.3 4472.9
6/7/2019 5:13:56 PM 4390.6 4227.2
6/7/2019 5:13:57 PM 4265.2 4101.8
6/7/2019 5:13:58 PM 4145.8 3982.4
6/7/2019 5:13:59 PM 3732.2 3568.8
6/7/2019 5:14:00 PM 3563.9 3400.5
6/7/2019 5:14:01 PM 3344.4 3181.0
6/7/2019 5:14:02 PM 3262.7 3099.3
6/7/2019 5:14:03 PM 3181.8 3018.4
6/7/2019 5:14:04 PM 2929.9 2766.5
6/7/2019 5:14:05 PM 2785.3 2621.9
6/7/2019 5:14:06 PM 2584.3 2420.9
6/7/2019 5:14:07 PM 2472.0 2308.6
6/7/2019 5:14:08 PM 2448.7 2285.3
6/7/2019 5:14:09 PM 2384.3 2220.9
6/7/2019 5:14:10 PM 2125.6 1962.2
6/7/2019 5:14:11 PM 2053.6 1890.2
6/7/2019 5:14:12 PM 1956.1 1792.7
6/7/2019 5:14:13 PM 1943.5 1780.1
6/7/2019 5:14:14 PM 1773.9 1610.5
6/7/2019 5:14:15 PM 1706.1 1542.7
6/7/2019 5:14:16 PM 1644.1 1480.7
6/7/2019 5:14:17 PM 1611.6 1448.2
6/7/2019 5:14:18 PM 1578.0 1414.6
6/7/2019 5:14:19 PM 1543.7 1380.3
6/7/2019 5:14:20 PM 1510.4 1347.0
6/7/2019 5:14:21 PM 1388.0 1224.6
6/7/2019 5:14:22 PM 1325.9 1162.5
6/7/2019 5:14:23 PM 1277.5 1114.1
6/7/2019 5:14:24 PM 1250.9 1087.5
6/7/2019 5:14:25 PM 1230.8 1067.4
6/7/2019 5:14:26 PM 1139.0 975.6
6/7/2019 5:14:27 PM 1114.6 951.2
6/7/2019 5:14:28 PM 1083.0 919.6
6/7/2019 5:14:29 PM 1052.0 888.6
6/7/2019 5:14:30 PM 1038.7 875.3
6/7/2019 5:14:31 PM 1023.0 859.6
6/7/2019 5:14:32 PM 1005.7 842.3
6/7/2019 5:14:33 PM 993.3 829.9
6/7/2019 5:14:34 PM 916.6 753.2
6/7/2019 5:14:35 PM 888.1 724.7
6/7/2019 5:14:36 PM 866.4 703.0
6/7/2019 5:14:37 PM 860.5 697.1
6/7/2019 5:14:38 PM 848.2 684.8
6/7/2019 5:14:39 PM 837.6 674.2
6/7/2019 5:14:40 PM 826.6 663.2
6/7/2019 5:14:41 PM 817.7 654.3
6/7/2019 5:14:42 PM 763.2 599.8
6/7/2019 5:14:43 PM 747.2 583.8
6/7/2019 5:14:44 PM 732.5 569.1
6/7/2019 5:14:45 PM 729.5 566.1
6/7/2019 5:14:46 PM 718.1 554.7
6/7/2019 5:14:47 PM 710.5 547.1
6/7/2019 5:14:48 PM 704.2 540.8
6/7/2019 5:14:49 PM 697.4 534.0
Page 402 of 452 August 2019
APPENDIX E55: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-3 Data Log
6/7/2019 5:14:50 PM 691.4 528.0
6/7/2019 5:14:51 PM 685.2 521.8
6/7/2019 5:14:52 PM 636.5 473.1
6/7/2019 5:14:53 PM 623.4 460.0
6/7/2019 5:14:54 PM 612.9 449.5
6/7/2019 5:14:55 PM 607.5 444.1
6/7/2019 5:14:56 PM 605.1 441.7
6/7/2019 5:14:57 PM 545.1 381.7
6/7/2019 5:14:58 PM 577.3 413.9
6/7/2019 5:14:59 PM 574.0 410.6
6/7/2019 5:15:00 PM 569.6 406.2
6/7/2019 5:15:01 PM 564.8 401.4
6/7/2019 5:15:02 PM 559.5 396.1
6/7/2019 5:15:03 PM 555.3 391.9
6/7/2019 5:15:04 PM 552.2 388.8
6/7/2019 5:15:05 PM 548.7 385.3
6/7/2019 5:15:06 PM 545.4 382.0
6/7/2019 5:15:07 PM 541.8 378.4
6/7/2019 5:15:08 PM 538.6 375.2
6/7/2019 5:15:09 PM 535.1 371.7
6/7/2019 5:15:10 PM 532.0 368.6
6/7/2019 5:15:11 PM 528.7 365.3
6/7/2019 5:15:12 PM 525.9 362.5
6/7/2019 5:15:13 PM 522.1 358.7
6/7/2019 5:15:14 PM 516.3 352.9
6/7/2019 5:15:15 PM 510.0 346.6
6/7/2019 5:15:16 PM 504.4 341.0
6/7/2019 5:15:17 PM 498.1 334.7
6/7/2019 5:15:18 PM 492.8 329.4
6/7/2019 5:15:19 PM 487.1 323.7
6/7/2019 5:15:20 PM 482.2 318.8
6/7/2019 5:15:21 PM 476.8 313.4
6/7/2019 5:15:22 PM 472.1 308.7
6/7/2019 5:15:23 PM 466.9 303.5
6/7/2019 5:15:24 PM 462.4 299.0
6/7/2019 5:15:25 PM 457.5 294.1
6/7/2019 5:15:26 PM 453.3 289.9
6/7/2019 5:15:27 PM 448.6 285.2
6/7/2019 5:15:28 PM 444.8 281.4
6/7/2019 5:15:29 PM 440.6 277.2
6/7/2019 5:15:30 PM 437.2 273.8
6/7/2019 5:15:31 PM 433.5 270.1
6/7/2019 5:15:32 PM 430.2 266.8
6/7/2019 5:15:33 PM 426.6 263.2
6/7/2019 5:15:34 PM 423.6 260.2
6/7/2019 5:15:35 PM 420.3 256.9
6/7/2019 5:15:36 PM 417.1 253.7
6/7/2019 5:15:37 PM 414.3 250.9
6/7/2019 5:15:38 PM 411.1 247.7
6/7/2019 5:15:39 PM 408.4 245.0
6/7/2019 5:15:40 PM 405.4 242.0
6/7/2019 5:15:41 PM 402.8 239.4
6/7/2019 5:15:42 PM 399.8 236.4
6/7/2019 5:15:43 PM 397.1 233.7
6/7/2019 5:15:44 PM 393.9 230.5
6/7/2019 5:15:45 PM 391.3 227.9
6/7/2019 5:15:46 PM 388.3 224.9
6/7/2019 5:15:47 PM 385.7 222.3
6/7/2019 5:15:48 PM 382.8 219.4
6/7/2019 5:15:49 PM 380.3 216.9
6/7/2019 5:15:50 PM 377.6 214.2
6/7/2019 5:15:51 PM 375.2 211.8
6/7/2019 5:15:52 PM 372.5 209.1
6/7/2019 5:15:53 PM 370.3 206.9
6/7/2019 5:15:54 PM 367.8 204.4
6/7/2019 5:15:55 PM 365.7 202.3
6/7/2019 5:15:56 PM 363.3 199.9
6/7/2019 5:15:57 PM 361.1 197.7
6/7/2019 5:15:58 PM 358.8 195.4
6/7/2019 5:15:59 PM 356.9 193.5
6/7/2019 5:16:00 PM 354.8 191.4
6/7/2019 5:16:01 PM 353.0 189.6
6/7/2019 5:16:02 PM 351.0 187.6
6/7/2019 5:16:03 PM 349.2 185.8
6/7/2019 5:16:04 PM 347.3 183.9
6/7/2019 5:16:05 PM 345.5 182.1
6/7/2019 5:16:06 PM 343.4 180.0
6/7/2019 5:16:07 PM 341.1 177.7
6/7/2019 5:16:08 PM 339.7 176.3
Page 403 of 452 August 2019
APPENDIX E55: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-3 Data Log
6/7/2019 5:16:09 PM 338.0 174.6
6/7/2019 5:16:10 PM 336.2 172.8
6/7/2019 5:16:11 PM 334.5 171.1
6/7/2019 5:16:12 PM 332.1 168.7
6/7/2019 5:16:13 PM 330.9 167.5
6/7/2019 5:16:14 PM 329.0 165.6
6/7/2019 5:16:15 PM 327.3 163.9
6/7/2019 5:16:16 PM 325.5 162.1
6/7/2019 5:16:17 PM 323.7 160.3
6/7/2019 5:16:18 PM 322.5 159.1
6/7/2019 5:16:19 PM 320.6 157.2
6/7/2019 5:16:20 PM 319.5 156.1
6/7/2019 5:16:21 PM 317.7 154.3
6/7/2019 5:16:22 PM 316.1 152.7
6/7/2019 5:16:23 PM 314.9 151.5
6/7/2019 5:16:24 PM 313.3 149.9
6/7/2019 5:16:25 PM 312.0 148.6
6/7/2019 5:16:26 PM 310.6 147.2
6/7/2019 5:16:27 PM 309.4 146.0
6/7/2019 5:16:28 PM 308.0 144.6
6/7/2019 5:16:29 PM 306.8 143.4
6/7/2019 5:16:30 PM 305.5 142.1
6/7/2019 5:16:31 PM 304.4 141.0
6/7/2019 5:16:32 PM 303.1 139.7
6/7/2019 5:16:33 PM 301.9 138.5
6/7/2019 5:16:34 PM 300.6 137.2
6/7/2019 5:16:35 PM 299.7 136.3
6/7/2019 5:16:36 PM 298.3 134.9
6/7/2019 5:16:37 PM 297.2 133.8
6/7/2019 5:16:38 PM 296.2 132.8
6/7/2019 5:16:39 PM 295.1 131.7
6/7/2019 5:16:40 PM 294.2 130.8
6/7/2019 5:16:41 PM 293.1 129.7
6/7/2019 5:16:42 PM 292.1 128.7
6/7/2019 5:16:43 PM 291.0 127.6
6/7/2019 5:16:44 PM 290.1 126.7
6/7/2019 5:16:45 PM 289.1 125.7
6/7/2019 5:16:46 PM 288.2 124.8
6/7/2019 5:16:47 PM 287.1 123.7
6/7/2019 5:16:48 PM 286.2 122.8
6/7/2019 5:16:49 PM 285.1 121.7
6/7/2019 5:16:50 PM 284.1 120.7
6/7/2019 5:16:51 PM 283.0 119.6
6/7/2019 5:16:52 PM 282.1 118.7
6/7/2019 5:16:53 PM 281.0 117.6
6/7/2019 5:16:54 PM 280.1 116.7
6/7/2019 5:16:55 PM 279.1 115.7
6/7/2019 5:16:56 PM 278.2 114.8
6/7/2019 5:16:57 PM 277.2 113.8
6/7/2019 5:16:58 PM 276.3 112.9
6/7/2019 5:16:59 PM 275.4 112.0
6/7/2019 5:17:00 PM 274.7 111.3
6/7/2019 5:17:01 PM 273.8 110.4
6/7/2019 5:17:02 PM 273.1 109.7
6/7/2019 5:17:03 PM 272.3 108.9
6/7/2019 5:17:04 PM 271.5 108.1
6/7/2019 5:17:05 PM 270.7 107.3
6/7/2019 5:17:06 PM 270.0 106.6
6/7/2019 5:17:07 PM 269.1 105.7
6/7/2019 5:17:08 PM 268.4 105.0
6/7/2019 5:17:09 PM 267.7 104.3
6/7/2019 5:17:10 PM 267.0 103.6
6/7/2019 5:17:11 PM 266.2 102.8
6/7/2019 5:17:12 PM 265.5 102.1
6/7/2019 5:17:13 PM 264.8 101.4
6/7/2019 5:17:14 PM 264.1 100.7
6/7/2019 5:17:15 PM 263.4 100.0
6/7/2019 5:17:16 PM 262.7 99.3
6/7/2019 5:17:17 PM 261.9 98.5
6/7/2019 5:17:18 PM 261.3 97.9
6/7/2019 5:17:19 PM 260.7 97.3
6/7/2019 5:17:20 PM 260.1 96.7
6/7/2019 5:17:21 PM 259.4 96.0
6/7/2019 5:17:22 PM 258.8 95.4
6/7/2019 5:17:23 PM 258.2 94.8
6/7/2019 5:17:24 PM 257.5 94.1
6/7/2019 5:17:25 PM 256.9 93.5
6/7/2019 5:17:26 PM 256.3 92.9
6/7/2019 5:17:27 PM 255.7 92.3
Page 404 of 452 August 2019
APPENDIX E55: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-3 Data Log
6/7/2019 5:17:28 PM 255.2 91.8
6/7/2019 5:17:29 PM 254.7 91.3
6/7/2019 5:17:30 PM 254.2 90.8
6/7/2019 5:17:31 PM 253.7 90.3
6/7/2019 5:17:32 PM 253.2 89.8
6/7/2019 5:17:33 PM 252.7 89.3
6/7/2019 5:17:34 PM 252.1 88.7
6/7/2019 5:17:35 PM 251.6 88.2
6/7/2019 5:17:36 PM 251.1 87.7
6/7/2019 5:17:37 PM 250.6 87.2
6/7/2019 5:17:38 PM 250.1 86.7
6/7/2019 5:17:39 PM 249.6 86.2
6/7/2019 5:17:40 PM 249.0 85.6
6/7/2019 5:17:41 PM 248.5 85.1
6/7/2019 5:17:42 PM 247.9 84.5
6/7/2019 5:17:43 PM 247.5 84.1
6/7/2019 5:17:44 PM 246.9 83.5
6/7/2019 5:17:45 PM 246.4 83.0
6/7/2019 5:17:46 PM 245.8 82.4
6/7/2019 5:17:47 PM 245.4 82.0
6/7/2019 5:17:48 PM 244.9 81.5
6/7/2019 5:17:49 PM 244.4 81.0
6/7/2019 5:17:50 PM 243.9 80.5
6/7/2019 5:17:51 PM 243.5 80.1
6/7/2019 5:17:52 PM 243.0 79.6
6/7/2019 5:17:53 PM 242.6 79.2
6/7/2019 5:17:54 PM 242.1 78.7
6/7/2019 5:17:55 PM 241.6 78.2
6/7/2019 5:17:56 PM 241.2 77.8
6/7/2019 5:17:57 PM 240.7 77.3
6/7/2019 5:17:58 PM 240.3 76.9
6/7/2019 5:17:59 PM 239.9 76.5
6/7/2019 5:18:00 PM 239.4 76.0
6/7/2019 5:18:01 PM 239.0 75.6
6/7/2019 5:18:02 PM 238.6 75.2
6/7/2019 5:18:03 PM 238.2 74.8
6/7/2019 5:18:04 PM 237.8 74.4
6/7/2019 5:18:05 PM 237.4 74.0
6/7/2019 5:18:06 PM 236.9 73.5
6/7/2019 5:18:07 PM 236.6 73.2
6/7/2019 5:18:08 PM 236.1 72.7
6/7/2019 5:18:09 PM 235.8 72.4
6/7/2019 5:18:10 PM 235.3 71.9
6/7/2019 5:18:11 PM 234.9 71.5
6/7/2019 5:18:12 PM 234.5 71.1
6/7/2019 5:18:13 PM 234.1 70.7
6/7/2019 5:18:14 PM 233.7 70.3
6/7/2019 5:18:15 PM 233.3 69.9
6/7/2019 5:18:16 PM 232.9 69.5
6/7/2019 5:18:17 PM 232.5 69.1
6/7/2019 5:18:18 PM 232.2 68.8
6/7/2019 5:18:19 PM 231.8 68.4
6/7/2019 5:18:20 PM 231.4 68.0
6/7/2019 5:18:21 PM 231.0 67.6
6/7/2019 5:18:22 PM 230.6 67.2
6/7/2019 5:18:23 PM 230.2 66.8
6/7/2019 5:18:24 PM 229.8 66.4
6/7/2019 5:18:25 PM 229.5 66.1
6/7/2019 5:18:26 PM 229.1 65.7
6/7/2019 5:18:27 PM 228.7 65.3
6/7/2019 5:18:28 PM 228.4 65.0
6/7/2019 5:18:29 PM 228.0 64.6
6/7/2019 5:18:30 PM 227.7 64.3
6/7/2019 5:18:31 PM 227.3 63.9
6/7/2019 5:18:32 PM 227.0 63.6
6/7/2019 5:18:33 PM 226.6 63.2
6/7/2019 5:18:34 PM 226.3 62.9
6/7/2019 5:18:35 PM 226.0 62.6
6/7/2019 5:18:36 PM 225.7 62.3
6/7/2019 5:18:37 PM 225.3 61.9
6/7/2019 5:18:38 PM 225.0 61.6
6/7/2019 5:18:39 PM 224.7 61.3
6/7/2019 5:18:40 PM 224.4 61.0
6/7/2019 5:18:41 PM 224.1 60.7
6/7/2019 5:18:42 PM 223.8 60.4
6/7/2019 5:18:43 PM 223.5 60.1
6/7/2019 5:18:44 PM 223.2 59.8
6/7/2019 5:18:45 PM 222.9 59.5
6/7/2019 5:18:46 PM 222.7 59.3
Page 405 of 452 August 2019
APPENDIX E55: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-3 Data Log
6/7/2019 5:18:47 PM 222.4 59.0
6/7/2019 5:18:48 PM 222.1 58.7
6/7/2019 5:18:49 PM 221.9 58.5
6/7/2019 5:18:50 PM 221.6 58.2
6/7/2019 5:18:51 PM 221.3 57.9
6/7/2019 5:18:52 PM 221.1 57.7
6/7/2019 5:18:53 PM 220.8 57.4
6/7/2019 5:18:54 PM 220.5 57.1
6/7/2019 5:18:55 PM 220.2 56.8
6/7/2019 5:18:56 PM 220.0 56.6
6/7/2019 5:18:57 PM 219.7 56.3
6/7/2019 5:18:58 PM 219.4 56.0
6/7/2019 5:18:59 PM 219.1 55.7
6/7/2019 5:19:00 PM 218.8 55.4
6/7/2019 5:19:01 PM 218.6 55.2
6/7/2019 5:19:02 PM 218.3 54.9
6/7/2019 5:19:03 PM 218.1 54.7
6/7/2019 5:19:04 PM 217.8 54.4
6/7/2019 5:19:05 PM 217.6 54.2
6/7/2019 5:19:06 PM 217.4 54.0
6/7/2019 5:19:07 PM 217.1 53.7
6/7/2019 5:19:08 PM 217.0 53.6
6/7/2019 5:19:09 PM 216.8 53.4
6/7/2019 5:19:10 PM 216.6 53.2
6/7/2019 5:19:11 PM 216.4 53.0
6/7/2019 5:19:12 PM 216.2 52.8
6/7/2019 5:19:13 PM 216.1 52.7
6/7/2019 5:19:14 PM 215.9 52.5
6/7/2019 5:19:15 PM 215.7 52.3
6/7/2019 5:19:16 PM 215.4 52.0
6/7/2019 5:19:17 PM 215.2 51.8
6/7/2019 5:19:18 PM 215.0 51.6
6/7/2019 5:19:19 PM 214.8 51.4
6/7/2019 5:19:20 PM 214.6 51.2
6/7/2019 5:19:21 PM 214.4 51.0
6/7/2019 5:19:22 PM 214.0 50.6
6/7/2019 5:19:23 PM 213.8 50.4
6/7/2019 5:19:24 PM 213.6 50.2
6/7/2019 5:19:25 PM 213.3 49.9
6/7/2019 5:19:26 PM 213.0 49.6
6/7/2019 5:19:27 PM 212.7 49.3
6/7/2019 5:19:28 PM 212.5 49.1
6/7/2019 5:19:29 PM 212.2 48.8
6/7/2019 5:19:30 PM 212.0 48.6
6/7/2019 5:19:31 PM 211.7 48.3
6/7/2019 5:19:32 PM 211.4 48.0
6/7/2019 5:19:33 PM 211.1 47.7
6/7/2019 5:19:34 PM 210.8 47.4
6/7/2019 5:19:35 PM 210.6 47.2
6/7/2019 5:19:36 PM 210.3 46.9
6/7/2019 5:19:37 PM 210.0 46.6
6/7/2019 5:19:38 PM 209.8 46.4
6/7/2019 5:19:39 PM 209.5 46.1
6/7/2019 5:19:40 PM 209.3 45.9
6/7/2019 5:19:41 PM 209.1 45.7
6/7/2019 5:19:42 PM 208.8 45.4
6/7/2019 5:19:43 PM 208.7 45.3
6/7/2019 5:19:44 PM 208.5 45.1
6/7/2019 5:19:45 PM 208.3 44.9
6/7/2019 5:19:46 PM 208.1 44.7
6/7/2019 5:19:47 PM 208.0 44.6
6/7/2019 5:19:48 PM 207.8 44.4
6/7/2019 5:19:49 PM 207.7 44.3
6/7/2019 5:19:50 PM 207.6 44.2
6/7/2019 5:19:51 PM 207.4 44.0
6/7/2019 5:19:52 PM 207.3 43.9
6/7/2019 5:19:53 PM 207.2 43.8
6/7/2019 5:19:54 PM 207.0 43.6
6/7/2019 5:19:55 PM 206.9 43.5
6/7/2019 5:19:56 PM 206.7 43.3
6/7/2019 5:19:57 PM 206.6 43.2
6/7/2019 5:19:58 PM 206.5 43.1
6/7/2019 5:19:59 PM 206.3 42.9
6/7/2019 5:20:00 PM 206.2 42.8
6/7/2019 5:20:01 PM 206.0 42.6
6/7/2019 5:20:02 PM 205.8 42.4
6/7/2019 5:20:03 PM 205.6 42.2
6/7/2019 5:20:04 PM 205.5 42.1
6/7/2019 5:20:05 PM 205.2 41.8
Page 406 of 452 August 2019
APPENDIX E55: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-3 Data Log
6/7/2019 5:20:06 PM 205.0 41.6
6/7/2019 5:20:07 PM 204.8 41.4
6/7/2019 5:20:08 PM 204.6 41.2
6/7/2019 5:20:09 PM 204.4 41.0
6/7/2019 5:20:10 PM 204.1 40.7
6/7/2019 5:20:11 PM 203.9 40.5
6/7/2019 5:20:12 PM 203.6 40.2
6/7/2019 5:20:13 PM 203.4 40.0
6/7/2019 5:20:14 PM 203.2 39.8
6/7/2019 5:20:15 PM 202.9 39.5
6/7/2019 5:20:16 PM 202.7 39.3
6/7/2019 5:20:17 PM 202.5 39.1
6/7/2019 5:20:18 PM 202.3 38.9
6/7/2019 5:20:19 PM 202.1 38.7
6/7/2019 5:20:20 PM 202.0 38.6
6/7/2019 5:20:21 PM 201.8 38.4
6/7/2019 5:20:22 PM 201.7 38.3
6/7/2019 5:20:23 PM 201.5 38.1
6/7/2019 5:20:24 PM 201.4 38.0
6/7/2019 5:20:25 PM 201.3 37.9
6/7/2019 5:20:26 PM 201.1 37.7
6/7/2019 5:20:27 PM 201.0 37.6
6/7/2019 5:20:28 PM 200.9 37.5
6/7/2019 5:20:29 PM 200.8 37.4
6/7/2019 5:20:30 PM 200.6 37.2
6/7/2019 5:20:31 PM 200.5 37.1
6/7/2019 5:20:32 PM 200.4 37.0
6/7/2019 5:20:33 PM 200.3 36.9
6/7/2019 5:20:34 PM 200.2 36.8
6/7/2019 5:20:35 PM 200.0 36.6
6/7/2019 5:20:36 PM 199.9 36.5
6/7/2019 5:20:37 PM 199.8 36.4
6/7/2019 5:20:38 PM 199.6 36.2
6/7/2019 5:20:39 PM 199.5 36.1
6/7/2019 5:20:40 PM 199.3 35.9
6/7/2019 5:20:41 PM 199.2 35.8
6/7/2019 5:20:42 PM 199.1 35.7
6/7/2019 5:20:43 PM 198.9 35.5
6/7/2019 5:20:44 PM 198.7 35.3
6/7/2019 5:20:45 PM 198.6 35.2
6/7/2019 5:20:46 PM 198.4 35.0
6/7/2019 5:20:47 PM 198.3 34.9
6/7/2019 5:20:48 PM 198.1 34.7
6/7/2019 5:20:49 PM 198.0 34.6
6/7/2019 5:20:50 PM 197.9 34.5
6/7/2019 5:20:51 PM 197.7 34.3
6/7/2019 5:20:52 PM 197.6 34.2
6/7/2019 5:20:53 PM 197.5 34.1
6/7/2019 5:20:54 PM 197.3 33.9
6/7/2019 5:20:55 PM 197.2 33.8
6/7/2019 5:20:56 PM 197.1 33.7
6/7/2019 5:20:57 PM 197.0 33.6
6/7/2019 5:20:58 PM 196.9 33.5
6/7/2019 5:20:59 PM 196.9 33.5
6/7/2019 5:21:00 PM 196.8 33.4
6/7/2019 5:21:01 PM 196.7 33.3
6/7/2019 5:21:02 PM 196.6 33.2
6/7/2019 5:21:03 PM 196.5 33.1
6/7/2019 5:21:04 PM 196.4 33.0
6/7/2019 5:21:05 PM 196.3 32.9
6/7/2019 5:21:06 PM 196.2 32.8
6/7/2019 5:21:07 PM 196.1 32.7
6/7/2019 5:21:08 PM 196.0 32.6
6/7/2019 5:21:09 PM 196.0 32.6
6/7/2019 5:21:10 PM 195.9 32.5
6/7/2019 5:21:11 PM 195.8 32.4
6/7/2019 5:21:12 PM 195.7 32.3
6/7/2019 5:21:13 PM 195.6 32.2
6/7/2019 5:21:14 PM 195.4 32.0
6/7/2019 5:21:15 PM 195.3 31.9
6/7/2019 5:21:16 PM 195.2 31.8
6/7/2019 5:21:17 PM 195.1 31.7
6/7/2019 5:21:18 PM 195.0 31.6
6/7/2019 5:21:19 PM 194.9 31.5
6/7/2019 5:21:20 PM 194.8 31.4
6/7/2019 5:21:21 PM 194.7 31.3
6/7/2019 5:21:22 PM 194.5 31.1
6/7/2019 5:21:23 PM 194.4 31.0
6/7/2019 5:21:24 PM 194.3 30.9
Page 407 of 452 August 2019
APPENDIX E55: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-3 Data Log
6/7/2019 5:21:25 PM 194.1 30.7
6/7/2019 5:21:26 PM 194.0 30.6
6/7/2019 5:21:27 PM 193.9 30.5
6/7/2019 5:21:28 PM 193.7 30.3
6/7/2019 5:21:29 PM 193.6 30.2
6/7/2019 5:21:30 PM 193.4 30.0
6/7/2019 5:21:31 PM 193.2 29.8
6/7/2019 5:21:32 PM 193.1 29.7
6/7/2019 5:21:33 PM 192.9 29.5
6/7/2019 5:21:34 PM 192.7 29.3
6/7/2019 5:21:35 PM 192.6 29.2
6/7/2019 5:21:36 PM 192.4 29.0
6/7/2019 5:21:37 PM 192.2 28.8
6/7/2019 5:21:38 PM 192.1 28.7
6/7/2019 5:21:39 PM 191.9 28.5
6/7/2019 5:21:40 PM 191.7 28.3
6/7/2019 5:21:41 PM 191.6 28.2
6/7/2019 5:21:42 PM 191.4 28.0
6/7/2019 5:21:43 PM 191.3 27.9
6/7/2019 5:21:44 PM 191.2 27.8
6/7/2019 5:21:45 PM 191.1 27.7
6/7/2019 5:21:46 PM 191.0 27.6
6/7/2019 5:21:47 PM 190.9 27.5
6/7/2019 5:21:48 PM 190.8 27.4
6/7/2019 5:21:49 PM 190.8 27.4
6/7/2019 5:21:50 PM 190.7 27.3
6/7/2019 5:21:51 PM 190.6 27.2
6/7/2019 5:21:52 PM 190.5 27.1
6/7/2019 5:21:53 PM 190.5 27.1
6/7/2019 5:21:54 PM 190.4 27.0
6/7/2019 5:21:55 PM 190.3 26.9
6/7/2019 5:21:56 PM 190.2 26.8
6/7/2019 5:21:57 PM 190.1 26.7
6/7/2019 5:21:58 PM 190.1 26.7
6/7/2019 5:21:59 PM 189.9 26.5
6/7/2019 5:22:00 PM 189.9 26.5
6/7/2019 5:22:01 PM 189.8 26.4
6/7/2019 5:22:02 PM 189.6 26.2
6/7/2019 5:22:03 PM 189.6 26.2
6/7/2019 5:22:04 PM 189.5 26.1
6/7/2019 5:22:05 PM 189.4 26.0
6/7/2019 5:22:06 PM 189.3 25.9
6/7/2019 5:22:07 PM 189.1 25.7
6/7/2019 5:22:08 PM 189.1 25.7
6/7/2019 5:22:09 PM 189.0 25.6
6/7/2019 5:22:10 PM 188.9 25.5
6/7/2019 5:22:11 PM 188.8 25.4
6/7/2019 5:22:12 PM 188.7 25.3
6/7/2019 5:22:13 PM 188.5 25.1
6/7/2019 5:22:14 PM 188.5 25.1
6/7/2019 5:22:15 PM 188.3 24.9
6/7/2019 5:22:16 PM 188.2 24.8
6/7/2019 5:22:17 PM 188.1 24.7
6/7/2019 5:22:18 PM 187.9 24.5
6/7/2019 5:22:19 PM 187.8 24.4
6/7/2019 5:22:20 PM 187.7 24.3
6/7/2019 5:22:21 PM 187.6 24.2
6/7/2019 5:22:22 PM 187.5 24.1
6/7/2019 5:22:23 PM 187.3 23.9
6/7/2019 5:22:24 PM 187.2 23.8
6/7/2019 5:22:25 PM 187.1 23.7
6/7/2019 5:22:26 PM 187.0 23.6
6/7/2019 5:22:27 PM 186.9 23.5
6/7/2019 5:22:28 PM 186.9 23.5
6/7/2019 5:22:29 PM 186.8 23.4
6/7/2019 5:22:30 PM 186.7 23.3
6/7/2019 5:22:31 PM 186.6 23.2
6/7/2019 5:22:32 PM 186.6 23.2
6/7/2019 5:22:33 PM 186.5 23.1
6/7/2019 5:22:34 PM 186.5 23.1
6/7/2019 5:22:35 PM 186.4 23.0
6/7/2019 5:22:36 PM 186.4 23.0
6/7/2019 5:22:37 PM 186.3 22.9
6/7/2019 5:22:38 PM 186.3 22.9
6/7/2019 5:22:39 PM 186.2 22.8
6/7/2019 5:22:40 PM 186.2 22.8
6/7/2019 5:22:41 PM 186.1 22.7
6/7/2019 5:22:42 PM 186.1 22.7
6/7/2019 5:22:43 PM 186.1 22.7
Page 408 of 452 August 2019
APPENDIX E55: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-3 Data Log
6/7/2019 5:22:44 PM 186.0 22.6
6/7/2019 5:22:45 PM 186.0 22.6
6/7/2019 5:22:46 PM 186.0 22.6
6/7/2019 5:22:47 PM 185.9 22.5
6/7/2019 5:22:48 PM 185.9 22.5
6/7/2019 5:22:49 PM 185.8 22.4
6/7/2019 5:22:50 PM 185.8 22.4
6/7/2019 5:22:51 PM 185.8 22.4
6/7/2019 5:22:52 PM 185.7 22.3
6/7/2019 5:22:53 PM 185.7 22.3
6/7/2019 5:22:54 PM 185.7 22.3
6/7/2019 5:22:55 PM 185.6 22.2
6/7/2019 5:22:56 PM 185.6 22.2
6/7/2019 5:22:57 PM 185.6 22.2
6/7/2019 5:22:58 PM 185.5 22.1
6/7/2019 5:22:59 PM 185.4 22.0
6/7/2019 5:23:00 PM 185.4 22.0
6/7/2019 5:23:01 PM 185.3 21.9
6/7/2019 5:23:02 PM 185.3 21.9
6/7/2019 5:23:03 PM 185.2 21.8
6/7/2019 5:23:04 PM 185.1 21.7
6/7/2019 5:23:05 PM 185.0 21.6
6/7/2019 5:23:06 PM 184.9 21.5
6/7/2019 5:23:07 PM 184.8 21.4
6/7/2019 5:23:08 PM 184.7 21.3
6/7/2019 5:23:09 PM 184.6 21.2
6/7/2019 5:23:10 PM 184.5 21.1
6/7/2019 5:23:11 PM 184.4 21.0
6/7/2019 5:23:12 PM 184.2 20.8
6/7/2019 5:23:13 PM 184.1 20.7
6/7/2019 5:23:14 PM 184.0 20.6
6/7/2019 5:23:15 PM 183.9 20.5
6/7/2019 5:23:16 PM 183.8 20.4
6/7/2019 5:23:17 PM 183.7 20.3
6/7/2019 5:23:18 PM 183.5 20.1
6/7/2019 5:23:19 PM 183.4 20.0
6/7/2019 5:23:20 PM 183.3 19.9
6/7/2019 5:23:21 PM 183.2 19.8
6/7/2019 5:23:22 PM 183.1 19.7
6/7/2019 5:23:23 PM 183.1 19.7
6/7/2019 5:23:24 PM 183.0 19.6
6/7/2019 5:23:25 PM 182.9 19.5
6/7/2019 5:23:26 PM 182.9 19.5
6/7/2019 5:23:27 PM 182.8 19.4
6/7/2019 5:23:28 PM 182.7 19.3
6/7/2019 5:23:29 PM 182.7 19.3
6/7/2019 5:23:30 PM 182.6 19.2
6/7/2019 5:23:31 PM 182.6 19.2
6/7/2019 5:23:32 PM 182.5 19.1
6/7/2019 5:23:33 PM 182.5 19.1
6/7/2019 5:23:34 PM 182.4 19.0
6/7/2019 5:23:35 PM 182.4 19.0
6/7/2019 5:23:36 PM 182.3 18.9
6/7/2019 5:23:37 PM 182.2 18.8
6/7/2019 5:23:38 PM 182.2 18.8
6/7/2019 5:23:39 PM 182.1 18.7
6/7/2019 5:23:40 PM 182.0 18.6
6/7/2019 5:23:41 PM 181.9 18.5
6/7/2019 5:23:42 PM 181.9 18.5
6/7/2019 5:23:43 PM 181.8 18.4
6/7/2019 5:23:44 PM 181.7 18.3
6/7/2019 5:23:45 PM 181.6 18.2
6/7/2019 5:23:46 PM 181.5 18.1
6/7/2019 5:23:47 PM 181.4 18.0
6/7/2019 5:23:48 PM 181.3 17.9
6/7/2019 5:23:49 PM 181.2 17.8
6/7/2019 5:23:50 PM 181.1 17.7
6/7/2019 5:23:51 PM 181.0 17.6
6/7/2019 5:23:52 PM 180.9 17.5
6/7/2019 5:23:53 PM 180.8 17.4
6/7/2019 5:23:54 PM 180.7 17.3
6/7/2019 5:23:55 PM 180.6 17.2
6/7/2019 5:23:56 PM 180.5 17.1
6/7/2019 5:23:57 PM 180.5 17.1
6/7/2019 5:23:58 PM 180.4 17.0
6/7/2019 5:23:59 PM 180.3 16.9
6/7/2019 5:24:00 PM 180.2 16.8
6/7/2019 5:24:01 PM 180.1 16.7
6/7/2019 5:24:02 PM 180.1 16.7
Page 409 of 452 August 2019
APPENDIX E55: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-3 Data Log
6/7/2019 5:24:03 PM 180.0 16.6
6/7/2019 5:24:04 PM 180.0 16.6
6/7/2019 5:24:05 PM 179.9 16.5
6/7/2019 5:24:06 PM 179.9 16.5
6/7/2019 5:24:07 PM 179.8 16.4
6/7/2019 5:24:08 PM 179.8 16.4
6/7/2019 5:24:09 PM 179.8 16.4
6/7/2019 5:24:10 PM 179.7 16.3
6/7/2019 5:24:11 PM 179.7 16.3
6/7/2019 5:24:12 PM 179.7 16.3
6/7/2019 5:24:13 PM 179.6 16.2
6/7/2019 5:24:14 PM 179.6 16.2
6/7/2019 5:24:15 PM 179.6 16.2
6/7/2019 5:24:16 PM 179.6 16.2
6/7/2019 5:24:17 PM 179.5 16.1
6/7/2019 5:24:18 PM 179.5 16.1
6/7/2019 5:24:19 PM 179.5 16.1
6/7/2019 5:24:20 PM 179.4 16.0
6/7/2019 5:24:21 PM 179.4 16.0
6/7/2019 5:24:22 PM 179.4 16.0
6/7/2019 5:24:23 PM 179.3 15.9
6/7/2019 5:24:24 PM 179.3 15.9
6/7/2019 5:24:25 PM 179.3 15.9
6/7/2019 5:24:26 PM 179.2 15.8
6/7/2019 5:24:27 PM 179.2 15.8
6/7/2019 5:24:28 PM 179.1 15.7
6/7/2019 5:24:29 PM 179.1 15.7
6/7/2019 5:24:30 PM 179.0 15.6
6/7/2019 5:24:31 PM 179.0 15.6
6/7/2019 5:24:32 PM 178.9 15.5
6/7/2019 5:24:33 PM 178.9 15.5
6/7/2019 5:24:34 PM 178.9 15.5
6/7/2019 5:24:35 PM 178.8 15.4
6/7/2019 5:24:36 PM 178.8 15.4
6/7/2019 5:24:37 PM 178.7 15.3
6/7/2019 5:24:38 PM 178.7 15.3
6/7/2019 5:24:39 PM 178.7 15.3
6/7/2019 5:24:40 PM 178.6 15.2
6/7/2019 5:24:41 PM 178.6 15.2
6/7/2019 5:24:42 PM 178.6 15.2
6/7/2019 5:24:43 PM 178.5 15.1
6/7/2019 5:24:44 PM 178.5 15.1
6/7/2019 5:24:45 PM 178.4 15.0
6/7/2019 5:24:46 PM 178.4 15.0
6/7/2019 5:24:47 PM 178.4 15.0
6/7/2019 5:24:48 PM 178.3 14.9
6/7/2019 5:24:49 PM 178.3 14.9
6/7/2019 5:24:50 PM 178.2 14.8
6/7/2019 5:24:51 PM 178.2 14.8
6/7/2019 5:24:52 PM 178.1 14.7
6/7/2019 5:24:53 PM 178.1 14.7
6/7/2019 5:24:54 PM 178.0 14.6
6/7/2019 5:24:55 PM 178.0 14.6
6/7/2019 5:24:56 PM 177.9 14.5
6/7/2019 5:24:57 PM 177.9 14.5
6/7/2019 5:24:58 PM 177.8 14.4
6/7/2019 5:24:59 PM 177.8 14.4
6/7/2019 5:25:00 PM 177.7 14.3
6/7/2019 5:25:01 PM 177.7 14.3
6/7/2019 5:25:02 PM 177.6 14.2
Page 410 of 452 August 2019
APPENDIX E55: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-C1 TEST-3 1625
SEEP-C1 TEST-3 1626
SEEP-C1 TEST-3 1627
SEEP-C1 TEST-3 1628
Location EC Reading
(µS/cms)
SEEP-C1 TEST-3 1,115
SEEP-C1 TEST-3 2,150
SEEP-C1 TEST-3 16,651
SEEP-C1 TEST-3 132,589
q 299,800
K 1.3293
0.8
13.4
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)
(µS/cms)
(µS/cms)
24.1
24.2
24.2
(µS/cms) (°C)
Table E2 SEEP-C1 TEST-3 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
142.9 21.4
141.8 21.8
142.6 21.4
Calibration Temperature
154.3 21.7
Average 145.4 (µS/cms)
Geometric Mean 145.3
Average (pre-test)163.4
Average (post-test)182.6
Table E3 SEEP-C1 TEST-3 YSI Salt Dilution Calibration Data
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)471,658.4 (s) . (µS/cms)
(mg/L)(°C)
100
1,000
10,000
100,000 24.1
Table E4 SEEP-C1 TEST-3 Flow Calculation Summary
Mass of Salt injected mg
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Slope of Calibration Curve (µS/cms) / (mg/L)
Calculated Flow Rate Q
L/s
GPM
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 411 of 452 August 2019
APPENDIX E56: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 5:34:33 PM 165.5 -
6/7/2019 5:34:34 PM 165.5 -
6/7/2019 5:34:35 PM 165.4 -
6/7/2019 5:34:36 PM 165.4 -
6/7/2019 5:34:37 PM 165.4 -
6/7/2019 5:34:38 PM 165.4 -
6/7/2019 5:34:39 PM 165.4 -
6/7/2019 5:34:40 PM 165.4 -
6/7/2019 5:34:41 PM 165.3 -
6/7/2019 5:34:42 PM 165.3 -
6/7/2019 5:34:43 PM 165.3 -
6/7/2019 5:34:44 PM 165.3 -
6/7/2019 5:34:45 PM 165.3 -
6/7/2019 5:34:46 PM 165.3 -
6/7/2019 5:34:47 PM 165.3 -
6/7/2019 5:34:48 PM 165.3 -
6/7/2019 5:34:49 PM 165.2 -
6/7/2019 5:34:50 PM 165.2 -
6/7/2019 5:34:51 PM 165.2 -
6/7/2019 5:34:52 PM 165.2 -
6/7/2019 5:34:53 PM 165.2 -
6/7/2019 5:34:54 PM 165.2 -
6/7/2019 5:34:55 PM 165.1 -
6/7/2019 5:34:56 PM 165.1 -
6/7/2019 5:34:57 PM 165.1 -
6/7/2019 5:34:58 PM 165.1 -
6/7/2019 5:34:59 PM 165.1 -
6/7/2019 5:35:00 PM 165.0 -
6/7/2019 5:35:01 PM 165.0 -
6/7/2019 5:35:02 PM 165.0 -
6/7/2019 5:35:03 PM 165.0 -
6/7/2019 5:35:04 PM 165.0 -
6/7/2019 5:35:05 PM 165.0 -
6/7/2019 5:35:06 PM 165.1 -
6/7/2019 5:35:07 PM 165.1 -
6/7/2019 5:35:08 PM 165.1 -
6/7/2019 5:35:09 PM 165.2 -
6/7/2019 5:35:10 PM 165.2 -
6/7/2019 5:35:11 PM 165.2 -
6/7/2019 5:35:12 PM 165.2 -
6/7/2019 5:35:13 PM 165.2 -
6/7/2019 5:35:14 PM 165.1 -
6/7/2019 5:35:15 PM 165.1 -
6/7/2019 5:35:16 PM 165.0 -
6/7/2019 5:35:17 PM 164.9 -
6/7/2019 5:35:18 PM 164.8 -
6/7/2019 5:35:19 PM 164.8 -
6/7/2019 5:35:20 PM 164.6 -
6/7/2019 5:35:21 PM 164.5 -
6/7/2019 5:35:22 PM 164.4 -
6/7/2019 5:35:23 PM 164.3 -
6/7/2019 5:35:24 PM 164.3 -
6/7/2019 5:35:25 PM 164.2 -
6/7/2019 5:35:26 PM 164.2 -
6/7/2019 5:35:27 PM 164.2 -
6/7/2019 5:35:28 PM 164.2 -
6/7/2019 5:35:29 PM 164.2 -
6/7/2019 5:35:30 PM 164.2 -
6/7/2019 5:35:31 PM 164.2 -
6/7/2019 5:35:32 PM 164.2 -
6/7/2019 5:35:33 PM 164.2 -
6/7/2019 5:35:34 PM 164.2 -
6/7/2019 5:35:35 PM 164.2 -
6/7/2019 5:35:36 PM 164.2 -
6/7/2019 5:35:37 PM 164.4 -
6/7/2019 5:35:38 PM 164.7 -
6/7/2019 5:35:39 PM 165.4 -
6/7/2019 5:35:40 PM 167.1 -
6/7/2019 5:35:41 PM 225.3 60.3
6/7/2019 5:35:42 PM 265.9 100.9
Table E1 SEEP-C1 TEST-4 Data Log
Page 412 of 452 August 2019
APPENDIX E56: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-4 Data Log
6/7/2019 5:35:43 PM 334.3 169.3
6/7/2019 5:35:44 PM 406.7 241.7
6/7/2019 5:35:45 PM 566.5 401.5
6/7/2019 5:35:46 PM 716.2 551.2
6/7/2019 5:35:47 PM 1003.6 838.6
6/7/2019 5:35:48 PM 1219.6 1054.6
6/7/2019 5:35:49 PM 1753.0 1588.0
6/7/2019 5:35:50 PM 2195.5 2030.5
6/7/2019 5:35:51 PM 2630.5 2465.5
6/7/2019 5:35:52 PM 3226.0 3061.0
6/7/2019 5:35:53 PM 3826.7 3661.7
6/7/2019 5:35:54 PM 4677.7 4512.7
6/7/2019 5:35:55 PM 5345.2 5180.2
6/7/2019 5:35:56 PM 6048.7 5883.7
6/7/2019 5:35:57 PM 6875.6 6710.6
6/7/2019 5:35:58 PM 7376.4 7211.4
6/7/2019 5:35:59 PM 8052.9 7887.9
6/7/2019 5:36:00 PM 8876.7 8711.7
6/7/2019 5:36:01 PM 9473.3 9308.3
6/7/2019 5:36:02 PM 10064.3 9899.3
6/7/2019 5:36:03 PM 10322.1 10157.1
6/7/2019 5:36:04 PM 10553.7 10388.7
6/7/2019 5:36:05 PM 10740.2 10575.2
6/7/2019 5:36:06 PM 10873.8 10708.8
6/7/2019 5:36:07 PM 11001.6 10836.6
6/7/2019 5:36:08 PM 11092.0 10927.0
6/7/2019 5:36:09 PM 11165.4 11000.4
6/7/2019 5:36:10 PM 11204.2 11039.2
6/7/2019 5:36:11 PM 11225.4 11060.4
6/7/2019 5:36:12 PM 11224.4 11059.4
6/7/2019 5:36:13 PM 11203.5 11038.5
6/7/2019 5:36:14 PM 11167.3 11002.3
6/7/2019 5:36:15 PM 10352.3 10187.3
6/7/2019 5:36:16 PM 10118.0 9953.0
6/7/2019 5:36:17 PM 9788.1 9623.1
6/7/2019 5:36:18 PM 9674.4 9509.4
6/7/2019 5:36:19 PM 9450.1 9285.1
6/7/2019 5:36:20 PM 9272.4 9107.4
6/7/2019 5:36:21 PM 8449.0 8284.0
6/7/2019 5:36:22 PM 8181.3 8016.3
6/7/2019 5:36:23 PM 7833.0 7668.0
6/7/2019 5:36:24 PM 7734.6 7569.6
6/7/2019 5:36:25 PM 7502.6 7337.6
6/7/2019 5:36:26 PM 6840.3 6675.3
6/7/2019 5:36:27 PM 6585.0 6420.0
6/7/2019 5:36:28 PM 6265.1 6100.1
6/7/2019 5:36:29 PM 6142.6 5977.6
6/7/2019 5:36:30 PM 5733.9 5568.9
6/7/2019 5:36:31 PM 5487.3 5322.3
6/7/2019 5:36:32 PM 5249.4 5084.4
6/7/2019 5:36:33 PM 5041.4 4876.4
6/7/2019 5:36:34 PM 4931.0 4766.0
6/7/2019 5:36:35 PM 4530.3 4365.3
6/7/2019 5:36:36 PM 4318.1 4153.1
6/7/2019 5:36:37 PM 4113.2 3948.2
6/7/2019 5:36:38 PM 3975.4 3810.4
6/7/2019 5:36:39 PM 3872.6 3707.6
6/7/2019 5:36:40 PM 3559.1 3394.1
6/7/2019 5:36:41 PM 3393.8 3228.8
6/7/2019 5:36:42 PM 3273.6 3108.6
6/7/2019 5:36:43 PM 3157.3 2992.3
6/7/2019 5:36:44 PM 3090.9 2925.9
6/7/2019 5:36:45 PM 3004.4 2839.4
6/7/2019 5:36:46 PM 2751.6 2586.6
6/7/2019 5:36:47 PM 2607.7 2442.7
6/7/2019 5:36:48 PM 2508.1 2343.1
6/7/2019 5:36:49 PM 2428.3 2263.3
6/7/2019 5:36:50 PM 2373.7 2208.7
6/7/2019 5:36:51 PM 2315.7 2150.7
6/7/2019 5:36:52 PM 2107.3 1942.3
6/7/2019 5:36:53 PM 2044.5 1879.5
6/7/2019 5:36:54 PM 1962.0 1797.0
6/7/2019 5:36:55 PM 1935.0 1770.0
6/7/2019 5:36:56 PM 1893.6 1728.6
6/7/2019 5:36:57 PM 1860.3 1695.3
6/7/2019 5:36:58 PM 1700.5 1535.5
6/7/2019 5:36:59 PM 1661.2 1496.2
Page 413 of 452 August 2019
APPENDIX E56: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-4 Data Log
6/7/2019 5:37:00 PM 1595.0 1430.0
6/7/2019 5:37:01 PM 1573.7 1408.7
6/7/2019 5:37:02 PM 1538.0 1373.0
6/7/2019 5:37:03 PM 1513.8 1348.8
6/7/2019 5:37:04 PM 1407.5 1242.5
6/7/2019 5:37:05 PM 1361.0 1196.0
6/7/2019 5:37:06 PM 1315.7 1150.7
6/7/2019 5:37:07 PM 1292.4 1127.4
6/7/2019 5:37:08 PM 1272.1 1107.1
6/7/2019 5:37:09 PM 1251.8 1086.8
6/7/2019 5:37:10 PM 1231.7 1066.7
6/7/2019 5:37:11 PM 1217.3 1052.3
6/7/2019 5:37:12 PM 1128.7 963.7
6/7/2019 5:37:13 PM 1098.6 933.6
6/7/2019 5:37:14 PM 1073.5 908.5
6/7/2019 5:37:15 PM 1056.5 891.5
6/7/2019 5:37:16 PM 1041.2 876.2
6/7/2019 5:37:17 PM 1027.7 862.7
6/7/2019 5:37:18 PM 1015.7 850.7
6/7/2019 5:37:19 PM 1004.7 839.7
6/7/2019 5:37:20 PM 935.3 770.3
6/7/2019 5:37:21 PM 920.6 755.6
6/7/2019 5:37:22 PM 902.6 737.6
6/7/2019 5:37:23 PM 892.2 727.2
6/7/2019 5:37:24 PM 879.3 714.3
6/7/2019 5:37:25 PM 868.8 703.8
6/7/2019 5:37:26 PM 859.9 694.9
6/7/2019 5:37:27 PM 852.3 687.3
6/7/2019 5:37:28 PM 844.0 679.0
6/7/2019 5:37:29 PM 793.6 628.6
6/7/2019 5:37:30 PM 780.7 615.7
6/7/2019 5:37:31 PM 769.3 604.3
6/7/2019 5:37:32 PM 760.4 595.4
6/7/2019 5:37:33 PM 755.4 590.4
6/7/2019 5:37:34 PM 747.2 582.2
6/7/2019 5:37:35 PM 742.1 577.1
6/7/2019 5:37:36 PM 736.1 571.1
6/7/2019 5:37:37 PM 729.5 564.5
6/7/2019 5:37:38 PM 725.1 560.1
6/7/2019 5:37:39 PM 720.2 555.2
6/7/2019 5:37:40 PM 714.5 549.5
6/7/2019 5:37:41 PM 668.2 503.2
6/7/2019 5:37:42 PM 654.6 489.6
6/7/2019 5:37:43 PM 650.7 485.7
6/7/2019 5:37:44 PM 644.7 479.7
6/7/2019 5:37:45 PM 640.2 475.2
6/7/2019 5:37:46 PM 636.1 471.1
6/7/2019 5:37:47 PM 631.5 466.5
6/7/2019 5:37:48 PM 628.9 463.9
6/7/2019 5:37:49 PM 625.2 460.2
6/7/2019 5:37:50 PM 621.9 456.9
6/7/2019 5:37:51 PM 508.6 343.6
6/7/2019 5:37:52 PM 578.8 413.8
6/7/2019 5:37:53 PM 580.2 415.2
6/7/2019 5:37:54 PM 575.6 410.6
6/7/2019 5:37:55 PM 573.6 408.6
6/7/2019 5:37:56 PM 568.8 403.8
6/7/2019 5:37:57 PM 565.5 400.5
6/7/2019 5:37:58 PM 564.0 399.0
6/7/2019 5:37:59 PM 561.7 396.7
6/7/2019 5:38:00 PM 559.6 394.6
6/7/2019 5:38:01 PM 557.2 392.2
6/7/2019 5:38:02 PM 554.4 389.4
6/7/2019 5:38:03 PM 552.5 387.5
6/7/2019 5:38:04 PM 549.8 384.8
6/7/2019 5:38:05 PM 547.5 382.5
6/7/2019 5:38:06 PM 545.5 380.5
6/7/2019 5:38:07 PM 543.2 378.2
6/7/2019 5:38:08 PM 539.0 374.0
6/7/2019 5:38:09 PM 534.4 369.4
6/7/2019 5:38:10 PM 530.3 365.3
6/7/2019 5:38:11 PM 525.6 360.6
6/7/2019 5:38:12 PM 521.5 356.5
6/7/2019 5:38:13 PM 516.8 351.8
6/7/2019 5:38:14 PM 512.8 347.8
6/7/2019 5:38:15 PM 508.3 343.3
6/7/2019 5:38:16 PM 504.7 339.7
6/7/2019 5:38:17 PM 500.5 335.5
6/7/2019 5:38:18 PM 496.7 331.7
Page 414 of 452 August 2019
APPENDIX E56: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-4 Data Log
6/7/2019 5:38:19 PM 492.5 327.5
6/7/2019 5:38:20 PM 488.9 323.9
6/7/2019 5:38:21 PM 484.9 319.9
6/7/2019 5:38:22 PM 481.6 316.6
6/7/2019 5:38:23 PM 477.9 312.9
6/7/2019 5:38:24 PM 474.8 309.8
6/7/2019 5:38:25 PM 471.2 306.2
6/7/2019 5:38:26 PM 468.1 303.1
6/7/2019 5:38:27 PM 464.8 299.8
6/7/2019 5:38:28 PM 462.0 297.0
6/7/2019 5:38:29 PM 458.7 293.7
6/7/2019 5:38:30 PM 455.8 290.8
6/7/2019 5:38:31 PM 452.6 287.6
6/7/2019 5:38:32 PM 449.8 284.8
6/7/2019 5:38:33 PM 446.7 281.7
6/7/2019 5:38:34 PM 443.9 278.9
6/7/2019 5:38:35 PM 440.8 275.8
6/7/2019 5:38:36 PM 438.2 273.2
6/7/2019 5:38:37 PM 435.3 270.3
6/7/2019 5:38:38 PM 432.9 267.9
6/7/2019 5:38:39 PM 430.2 265.2
6/7/2019 5:38:40 PM 427.7 262.7
6/7/2019 5:38:41 PM 424.8 259.8
6/7/2019 5:38:42 PM 422.3 257.3
6/7/2019 5:38:43 PM 419.6 254.6
6/7/2019 5:38:44 PM 417.2 252.2
6/7/2019 5:38:45 PM 414.6 249.6
6/7/2019 5:38:46 PM 412.3 247.3
6/7/2019 5:38:47 PM 409.8 244.8
6/7/2019 5:38:48 PM 407.3 242.3
6/7/2019 5:38:49 PM 405.1 240.1
6/7/2019 5:38:50 PM 402.6 237.6
6/7/2019 5:38:51 PM 400.5 235.5
6/7/2019 5:38:52 PM 398.1 233.1
6/7/2019 5:38:53 PM 396.0 231.0
6/7/2019 5:38:54 PM 393.7 228.7
6/7/2019 5:38:55 PM 391.6 226.6
6/7/2019 5:38:56 PM 389.2 224.2
6/7/2019 5:38:57 PM 387.2 222.2
6/7/2019 5:38:58 PM 385.0 220.0
6/7/2019 5:38:59 PM 383.2 218.2
6/7/2019 5:39:00 PM 381.1 216.1
6/7/2019 5:39:01 PM 379.4 214.4
6/7/2019 5:39:02 PM 377.6 212.6
6/7/2019 5:39:03 PM 376.0 211.0
6/7/2019 5:39:04 PM 374.1 209.1
6/7/2019 5:39:05 PM 372.4 207.4
6/7/2019 5:39:06 PM 370.5 205.5
6/7/2019 5:39:07 PM 369.0 204.0
6/7/2019 5:39:08 PM 367.4 202.4
6/7/2019 5:39:09 PM 365.9 200.9
6/7/2019 5:39:10 PM 364.3 199.3
6/7/2019 5:39:11 PM 362.8 197.8
6/7/2019 5:39:12 PM 361.1 196.1
6/7/2019 5:39:13 PM 359.5 194.5
6/7/2019 5:39:14 PM 357.7 192.7
6/7/2019 5:39:15 PM 356.1 191.1
6/7/2019 5:39:16 PM 354.3 189.3
6/7/2019 5:39:17 PM 352.9 187.9
6/7/2019 5:39:18 PM 351.3 186.3
6/7/2019 5:39:19 PM 350.0 185.0
6/7/2019 5:39:20 PM 348.4 183.4
6/7/2019 5:39:21 PM 347.0 182.0
6/7/2019 5:39:22 PM 345.5 180.5
6/7/2019 5:39:23 PM 344.2 179.2
6/7/2019 5:39:24 PM 342.6 177.6
6/7/2019 5:39:25 PM 341.3 176.3
6/7/2019 5:39:26 PM 339.8 174.8
6/7/2019 5:39:27 PM 338.4 173.4
6/7/2019 5:39:28 PM 336.9 171.9
6/7/2019 5:39:29 PM 335.6 170.6
6/7/2019 5:39:30 PM 334.2 169.2
6/7/2019 5:39:31 PM 333.0 168.0
6/7/2019 5:39:32 PM 331.6 166.6
6/7/2019 5:39:33 PM 330.4 165.4
6/7/2019 5:39:34 PM 329.0 164.0
6/7/2019 5:39:35 PM 327.8 162.8
6/7/2019 5:39:36 PM 326.5 161.5
6/7/2019 5:39:37 PM 325.5 160.5
Page 415 of 452 August 2019
APPENDIX E56: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-4 Data Log
6/7/2019 5:39:38 PM 324.4 159.4
6/7/2019 5:39:39 PM 323.3 158.3
6/7/2019 5:39:40 PM 322.4 157.4
6/7/2019 5:39:41 PM 321.3 156.3
6/7/2019 5:39:42 PM 320.3 155.3
6/7/2019 5:39:43 PM 319.2 154.2
6/7/2019 5:39:44 PM 318.3 153.3
6/7/2019 5:39:45 PM 317.2 152.2
6/7/2019 5:39:46 PM 316.2 151.2
6/7/2019 5:39:47 PM 315.2 150.2
6/7/2019 5:39:48 PM 314.2 149.2
6/7/2019 5:39:49 PM 313.1 148.1
6/7/2019 5:39:50 PM 312.1 147.1
6/7/2019 5:39:51 PM 311.1 146.1
6/7/2019 5:39:52 PM 310.1 145.1
6/7/2019 5:39:53 PM 309.0 144.0
6/7/2019 5:39:54 PM 308.1 143.1
6/7/2019 5:39:55 PM 307.1 142.1
6/7/2019 5:39:56 PM 306.3 141.3
6/7/2019 5:39:57 PM 305.3 140.3
6/7/2019 5:39:58 PM 304.5 139.5
6/7/2019 5:39:59 PM 303.6 138.6
6/7/2019 5:40:00 PM 302.9 137.9
6/7/2019 5:40:01 PM 302.1 137.1
6/7/2019 5:40:02 PM 301.4 136.4
6/7/2019 5:40:03 PM 300.5 135.5
6/7/2019 5:40:04 PM 299.7 134.7
6/7/2019 5:40:05 PM 298.9 133.9
6/7/2019 5:40:06 PM 298.1 133.1
6/7/2019 5:40:07 PM 297.2 132.2
6/7/2019 5:40:08 PM 296.4 131.4
6/7/2019 5:40:09 PM 295.5 130.5
6/7/2019 5:40:10 PM 294.6 129.6
6/7/2019 5:40:11 PM 293.7 128.7
6/7/2019 5:40:12 PM 292.9 127.9
6/7/2019 5:40:13 PM 292.0 127.0
6/7/2019 5:40:14 PM 291.2 126.2
6/7/2019 5:40:15 PM 290.4 125.4
6/7/2019 5:40:16 PM 289.6 124.6
6/7/2019 5:40:17 PM 288.8 123.8
6/7/2019 5:40:18 PM 288.2 123.2
6/7/2019 5:40:19 PM 287.4 122.4
6/7/2019 5:40:20 PM 286.7 121.7
6/7/2019 5:40:21 PM 286.0 121.0
6/7/2019 5:40:22 PM 285.4 120.4
6/7/2019 5:40:23 PM 284.8 119.8
6/7/2019 5:40:24 PM 284.2 119.2
6/7/2019 5:40:25 PM 283.6 118.6
6/7/2019 5:40:26 PM 283.1 118.1
6/7/2019 5:40:27 PM 282.5 117.5
6/7/2019 5:40:28 PM 282.0 117.0
6/7/2019 5:40:29 PM 281.4 116.4
6/7/2019 5:40:30 PM 280.8 115.8
6/7/2019 5:40:31 PM 280.3 115.3
6/7/2019 5:40:32 PM 279.8 114.8
6/7/2019 5:40:33 PM 279.3 114.3
6/7/2019 5:40:34 PM 278.8 113.8
6/7/2019 5:40:35 PM 278.3 113.3
6/7/2019 5:40:36 PM 277.7 112.7
6/7/2019 5:40:37 PM 277.3 112.3
6/7/2019 5:40:38 PM 276.7 111.7
6/7/2019 5:40:39 PM 276.3 111.3
6/7/2019 5:40:40 PM 275.7 110.7
6/7/2019 5:40:41 PM 275.3 110.3
6/7/2019 5:40:42 PM 274.8 109.8
6/7/2019 5:40:43 PM 274.3 109.3
6/7/2019 5:40:44 PM 273.8 108.8
6/7/2019 5:40:45 PM 273.4 108.4
6/7/2019 5:40:46 PM 272.9 107.9
6/7/2019 5:40:47 PM 272.4 107.4
6/7/2019 5:40:48 PM 272.0 107.0
6/7/2019 5:40:49 PM 271.6 106.6
6/7/2019 5:40:50 PM 271.2 106.2
6/7/2019 5:40:51 PM 270.8 105.8
6/7/2019 5:40:52 PM 270.3 105.3
6/7/2019 5:40:53 PM 270.0 105.0
6/7/2019 5:40:54 PM 269.5 104.5
6/7/2019 5:40:55 PM 268.9 103.9
6/7/2019 5:40:56 PM 268.6 103.6
Page 416 of 452 August 2019
APPENDIX E56: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-4 Data Log
6/7/2019 5:40:57 PM 268.0 103.0
6/7/2019 5:40:58 PM 267.6 102.6
6/7/2019 5:40:59 PM 267.0 102.0
6/7/2019 5:41:00 PM 266.4 101.4
6/7/2019 5:41:01 PM 266.0 101.0
6/7/2019 5:41:02 PM 265.4 100.4
6/7/2019 5:41:03 PM 264.9 99.9
6/7/2019 5:41:04 PM 264.4 99.4
6/7/2019 5:41:05 PM 263.9 98.9
6/7/2019 5:41:06 PM 263.4 98.4
6/7/2019 5:41:07 PM 263.0 98.0
6/7/2019 5:41:08 PM 262.4 97.4
6/7/2019 5:41:09 PM 261.9 96.9
6/7/2019 5:41:10 PM 261.4 96.4
6/7/2019 5:41:11 PM 260.9 95.9
6/7/2019 5:41:12 PM 260.4 95.4
6/7/2019 5:41:13 PM 260.0 95.0
6/7/2019 5:41:14 PM 259.5 94.5
6/7/2019 5:41:15 PM 259.0 94.0
6/7/2019 5:41:16 PM 258.5 93.5
6/7/2019 5:41:17 PM 258.1 93.1
6/7/2019 5:41:18 PM 257.7 92.7
6/7/2019 5:41:19 PM 257.2 92.2
6/7/2019 5:41:20 PM 256.8 91.8
6/7/2019 5:41:21 PM 256.4 91.4
6/7/2019 5:41:22 PM 255.9 90.9
6/7/2019 5:41:23 PM 255.6 90.6
6/7/2019 5:41:24 PM 255.1 90.1
6/7/2019 5:41:25 PM 254.8 89.8
6/7/2019 5:41:26 PM 254.4 89.4
6/7/2019 5:41:27 PM 254.0 89.0
6/7/2019 5:41:28 PM 253.5 88.5
6/7/2019 5:41:29 PM 253.1 88.1
6/7/2019 5:41:30 PM 252.7 87.7
6/7/2019 5:41:31 PM 252.3 87.3
6/7/2019 5:41:32 PM 251.8 86.8
6/7/2019 5:41:33 PM 251.4 86.4
6/7/2019 5:41:34 PM 251.0 86.0
6/7/2019 5:41:35 PM 250.5 85.5
6/7/2019 5:41:36 PM 250.1 85.1
6/7/2019 5:41:37 PM 249.7 84.7
6/7/2019 5:41:38 PM 249.2 84.2
6/7/2019 5:41:39 PM 248.8 83.8
6/7/2019 5:41:40 PM 248.4 83.4
6/7/2019 5:41:41 PM 248.0 83.0
6/7/2019 5:41:42 PM 247.6 82.6
6/7/2019 5:41:43 PM 247.2 82.2
6/7/2019 5:41:44 PM 246.9 81.9
6/7/2019 5:41:45 PM 246.5 81.5
6/7/2019 5:41:46 PM 246.2 81.2
6/7/2019 5:41:47 PM 245.9 80.9
6/7/2019 5:41:48 PM 245.6 80.6
6/7/2019 5:41:49 PM 245.3 80.3
6/7/2019 5:41:50 PM 245.1 80.1
6/7/2019 5:41:51 PM 244.7 79.7
6/7/2019 5:41:52 PM 244.5 79.5
6/7/2019 5:41:53 PM 244.1 79.1
6/7/2019 5:41:54 PM 243.8 78.8
6/7/2019 5:41:55 PM 243.5 78.5
6/7/2019 5:41:56 PM 243.2 78.2
6/7/2019 5:41:57 PM 242.9 77.9
6/7/2019 5:41:58 PM 242.5 77.5
6/7/2019 5:41:59 PM 242.2 77.2
6/7/2019 5:42:00 PM 241.9 76.9
6/7/2019 5:42:01 PM 241.5 76.5
6/7/2019 5:42:02 PM 241.2 76.2
6/7/2019 5:42:03 PM 240.9 75.9
6/7/2019 5:42:04 PM 240.6 75.6
6/7/2019 5:42:05 PM 240.2 75.2
6/7/2019 5:42:06 PM 240.0 75.0
6/7/2019 5:42:07 PM 239.7 74.7
6/7/2019 5:42:08 PM 239.5 74.5
6/7/2019 5:42:09 PM 239.2 74.2
6/7/2019 5:42:10 PM 238.9 73.9
6/7/2019 5:42:11 PM 238.6 73.6
6/7/2019 5:42:12 PM 238.4 73.4
6/7/2019 5:42:13 PM 238.1 73.1
6/7/2019 5:42:14 PM 237.9 72.9
6/7/2019 5:42:15 PM 237.6 72.6
Page 417 of 452 August 2019
APPENDIX E56: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-4 Data Log
6/7/2019 5:42:16 PM 237.4 72.4
6/7/2019 5:42:17 PM 237.2 72.2
6/7/2019 5:42:18 PM 237.0 72.0
6/7/2019 5:42:19 PM 236.7 71.7
6/7/2019 5:42:20 PM 236.5 71.5
6/7/2019 5:42:21 PM 236.2 71.2
6/7/2019 5:42:22 PM 236.0 71.0
6/7/2019 5:42:23 PM 235.7 70.7
6/7/2019 5:42:24 PM 235.5 70.5
6/7/2019 5:42:25 PM 235.2 70.2
6/7/2019 5:42:26 PM 235.0 70.0
6/7/2019 5:42:27 PM 234.8 69.8
6/7/2019 5:42:28 PM 234.5 69.5
6/7/2019 5:42:29 PM 234.2 69.2
6/7/2019 5:42:30 PM 234.0 69.0
6/7/2019 5:42:31 PM 233.8 68.8
6/7/2019 5:42:32 PM 233.5 68.5
6/7/2019 5:42:33 PM 233.3 68.3
6/7/2019 5:42:34 PM 233.0 68.0
6/7/2019 5:42:35 PM 232.8 67.8
6/7/2019 5:42:36 PM 232.6 67.6
6/7/2019 5:42:37 PM 232.4 67.4
6/7/2019 5:42:38 PM 232.1 67.1
6/7/2019 5:42:39 PM 231.9 66.9
6/7/2019 5:42:40 PM 231.7 66.7
6/7/2019 5:42:41 PM 231.5 66.5
6/7/2019 5:42:42 PM 231.2 66.2
6/7/2019 5:42:43 PM 231.0 66.0
6/7/2019 5:42:44 PM 230.8 65.8
6/7/2019 5:42:45 PM 230.6 65.6
6/7/2019 5:42:46 PM 230.3 65.3
6/7/2019 5:42:47 PM 230.1 65.1
6/7/2019 5:42:48 PM 229.9 64.9
6/7/2019 5:42:49 PM 229.7 64.7
6/7/2019 5:42:50 PM 229.5 64.5
6/7/2019 5:42:51 PM 229.3 64.3
6/7/2019 5:42:52 PM 229.0 64.0
6/7/2019 5:42:53 PM 228.8 63.8
6/7/2019 5:42:54 PM 228.6 63.6
6/7/2019 5:42:55 PM 228.4 63.4
6/7/2019 5:42:56 PM 228.2 63.2
6/7/2019 5:42:57 PM 228.0 63.0
6/7/2019 5:42:58 PM 227.8 62.8
6/7/2019 5:42:59 PM 227.6 62.6
6/7/2019 5:43:00 PM 227.3 62.3
6/7/2019 5:43:01 PM 227.1 62.1
6/7/2019 5:43:02 PM 226.9 61.9
6/7/2019 5:43:03 PM 226.7 61.7
6/7/2019 5:43:04 PM 226.5 61.5
6/7/2019 5:43:05 PM 226.3 61.3
6/7/2019 5:43:06 PM 226.1 61.1
6/7/2019 5:43:07 PM 225.9 60.9
6/7/2019 5:43:08 PM 225.7 60.7
6/7/2019 5:43:09 PM 225.4 60.4
6/7/2019 5:43:10 PM 225.2 60.2
6/7/2019 5:43:11 PM 225.0 60.0
6/7/2019 5:43:12 PM 224.8 59.8
6/7/2019 5:43:13 PM 224.6 59.6
6/7/2019 5:43:14 PM 224.4 59.4
6/7/2019 5:43:15 PM 224.2 59.2
6/7/2019 5:43:16 PM 224.0 59.0
6/7/2019 5:43:17 PM 223.8 58.8
6/7/2019 5:43:18 PM 223.6 58.6
6/7/2019 5:43:19 PM 223.4 58.4
6/7/2019 5:43:20 PM 223.2 58.2
6/7/2019 5:43:21 PM 223.0 58.0
6/7/2019 5:43:22 PM 222.9 57.9
6/7/2019 5:43:23 PM 222.6 57.6
6/7/2019 5:43:24 PM 222.5 57.5
6/7/2019 5:43:25 PM 222.2 57.2
6/7/2019 5:43:26 PM 222.1 57.1
6/7/2019 5:43:27 PM 221.9 56.9
6/7/2019 5:43:28 PM 221.7 56.7
6/7/2019 5:43:29 PM 221.5 56.5
6/7/2019 5:43:30 PM 221.3 56.3
6/7/2019 5:43:31 PM 221.2 56.2
6/7/2019 5:43:32 PM 221.0 56.0
6/7/2019 5:43:33 PM 220.9 55.9
6/7/2019 5:43:34 PM 220.7 55.7
Page 418 of 452 August 2019
APPENDIX E56: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-4 Data Log
6/7/2019 5:43:35 PM 220.5 55.5
6/7/2019 5:43:36 PM 220.4 55.4
6/7/2019 5:43:37 PM 220.3 55.3
6/7/2019 5:43:38 PM 220.2 55.2
6/7/2019 5:43:39 PM 220.0 55.0
6/7/2019 5:43:40 PM 219.9 54.9
6/7/2019 5:43:41 PM 219.7 54.7
6/7/2019 5:43:42 PM 219.6 54.6
6/7/2019 5:43:43 PM 219.5 54.5
6/7/2019 5:43:44 PM 219.4 54.4
6/7/2019 5:43:45 PM 219.2 54.2
6/7/2019 5:43:46 PM 219.1 54.1
6/7/2019 5:43:47 PM 219.0 54.0
6/7/2019 5:43:48 PM 218.9 53.9
6/7/2019 5:43:49 PM 218.7 53.7
6/7/2019 5:43:50 PM 218.7 53.7
6/7/2019 5:43:51 PM 218.6 53.6
6/7/2019 5:43:52 PM 218.5 53.5
6/7/2019 5:43:53 PM 218.3 53.3
6/7/2019 5:43:54 PM 218.3 53.3
6/7/2019 5:43:55 PM 218.1 53.1
6/7/2019 5:43:56 PM 218.0 53.0
6/7/2019 5:43:57 PM 217.9 52.9
6/7/2019 5:43:58 PM 217.8 52.8
6/7/2019 5:43:59 PM 217.6 52.6
6/7/2019 5:44:00 PM 217.5 52.5
6/7/2019 5:44:01 PM 217.4 52.4
6/7/2019 5:44:02 PM 217.2 52.2
6/7/2019 5:44:03 PM 217.1 52.1
6/7/2019 5:44:04 PM 216.9 51.9
6/7/2019 5:44:05 PM 216.7 51.7
6/7/2019 5:44:06 PM 216.6 51.6
6/7/2019 5:44:07 PM 216.4 51.4
6/7/2019 5:44:08 PM 216.3 51.3
6/7/2019 5:44:09 PM 216.2 51.2
6/7/2019 5:44:10 PM 216.1 51.1
6/7/2019 5:44:11 PM 215.9 50.9
6/7/2019 5:44:12 PM 215.8 50.8
6/7/2019 5:44:13 PM 215.7 50.7
6/7/2019 5:44:14 PM 215.6 50.6
6/7/2019 5:44:15 PM 215.5 50.5
6/7/2019 5:44:16 PM 215.5 50.5
6/7/2019 5:44:17 PM 215.4 50.4
6/7/2019 5:44:18 PM 215.3 50.3
6/7/2019 5:44:19 PM 215.3 50.3
6/7/2019 5:44:20 PM 215.2 50.2
6/7/2019 5:44:21 PM 215.1 50.1
6/7/2019 5:44:22 PM 215.1 50.1
6/7/2019 5:44:23 PM 215.0 50.0
6/7/2019 5:44:24 PM 214.9 49.9
6/7/2019 5:44:25 PM 214.9 49.9
6/7/2019 5:44:26 PM 214.9 49.9
6/7/2019 5:44:27 PM 214.9 49.9
6/7/2019 5:44:28 PM 214.8 49.8
6/7/2019 5:44:29 PM 214.8 49.8
6/7/2019 5:44:30 PM 214.8 49.8
6/7/2019 5:44:31 PM 214.7 49.7
6/7/2019 5:44:32 PM 214.7 49.7
6/7/2019 5:44:33 PM 214.6 49.6
6/7/2019 5:44:34 PM 214.6 49.6
6/7/2019 5:44:35 PM 214.5 49.5
6/7/2019 5:44:36 PM 214.5 49.5
6/7/2019 5:44:37 PM 214.4 49.4
6/7/2019 5:44:38 PM 214.3 49.3
6/7/2019 5:44:39 PM 214.2 49.2
6/7/2019 5:44:40 PM 214.1 49.1
6/7/2019 5:44:41 PM 214.0 49.0
6/7/2019 5:44:42 PM 213.8 48.8
6/7/2019 5:44:43 PM 213.7 48.7
6/7/2019 5:44:44 PM 213.6 48.6
6/7/2019 5:44:45 PM 213.5 48.5
6/7/2019 5:44:46 PM 213.3 48.3
6/7/2019 5:44:47 PM 213.2 48.2
6/7/2019 5:44:48 PM 213.1 48.1
6/7/2019 5:44:49 PM 213.0 48.0
6/7/2019 5:44:50 PM 212.9 47.9
6/7/2019 5:44:51 PM 212.8 47.8
6/7/2019 5:44:52 PM 212.7 47.7
6/7/2019 5:44:53 PM 212.6 47.6
Page 419 of 452 August 2019
APPENDIX E56: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-4 Data Log
6/7/2019 5:44:54 PM 212.4 47.4
6/7/2019 5:44:55 PM 212.3 47.3
6/7/2019 5:44:56 PM 212.2 47.2
6/7/2019 5:44:57 PM 212.1 47.1
6/7/2019 5:44:58 PM 212.0 47.0
6/7/2019 5:44:59 PM 211.8 46.8
6/7/2019 5:45:00 PM 211.7 46.7
6/7/2019 5:45:01 PM 211.5 46.5
6/7/2019 5:45:02 PM 211.4 46.4
6/7/2019 5:45:03 PM 211.2 46.2
6/7/2019 5:45:04 PM 211.1 46.1
6/7/2019 5:45:05 PM 210.9 45.9
6/7/2019 5:45:06 PM 210.8 45.8
6/7/2019 5:45:07 PM 210.6 45.6
6/7/2019 5:45:08 PM 210.4 45.4
6/7/2019 5:45:09 PM 210.2 45.2
6/7/2019 5:45:10 PM 210.1 45.1
6/7/2019 5:45:11 PM 209.9 44.9
6/7/2019 5:45:12 PM 209.7 44.7
6/7/2019 5:45:13 PM 209.6 44.6
6/7/2019 5:45:14 PM 209.4 44.4
6/7/2019 5:45:15 PM 209.2 44.2
6/7/2019 5:45:16 PM 209.1 44.1
6/7/2019 5:45:17 PM 208.9 43.9
6/7/2019 5:45:18 PM 208.8 43.8
6/7/2019 5:45:19 PM 208.6 43.6
6/7/2019 5:45:20 PM 208.5 43.5
6/7/2019 5:45:21 PM 208.4 43.4
6/7/2019 5:45:22 PM 208.3 43.3
6/7/2019 5:45:23 PM 208.1 43.1
6/7/2019 5:45:24 PM 208.0 43.0
6/7/2019 5:45:25 PM 207.8 42.8
6/7/2019 5:45:26 PM 207.7 42.7
6/7/2019 5:45:27 PM 207.6 42.6
6/7/2019 5:45:28 PM 207.5 42.5
6/7/2019 5:45:29 PM 207.3 42.3
6/7/2019 5:45:30 PM 207.2 42.2
6/7/2019 5:45:31 PM 207.1 42.1
6/7/2019 5:45:32 PM 206.9 41.9
6/7/2019 5:45:33 PM 206.8 41.8
6/7/2019 5:45:34 PM 206.7 41.7
6/7/2019 5:45:35 PM 206.6 41.6
6/7/2019 5:45:36 PM 206.4 41.4
6/7/2019 5:45:37 PM 206.3 41.3
6/7/2019 5:45:38 PM 206.2 41.2
6/7/2019 5:45:39 PM 206.1 41.1
6/7/2019 5:45:40 PM 206.0 41.0
6/7/2019 5:45:41 PM 205.8 40.8
6/7/2019 5:45:42 PM 205.7 40.7
6/7/2019 5:45:43 PM 205.6 40.6
6/7/2019 5:45:44 PM 205.5 40.5
6/7/2019 5:45:45 PM 205.4 40.4
6/7/2019 5:45:46 PM 205.4 40.4
6/7/2019 5:45:47 PM 205.3 40.3
6/7/2019 5:45:48 PM 205.2 40.2
6/7/2019 5:45:49 PM 205.1 40.1
6/7/2019 5:45:50 PM 205.0 40.0
6/7/2019 5:45:51 PM 204.9 39.9
6/7/2019 5:45:52 PM 204.8 39.8
6/7/2019 5:45:53 PM 204.7 39.7
6/7/2019 5:45:54 PM 204.7 39.7
6/7/2019 5:45:55 PM 204.6 39.6
6/7/2019 5:45:56 PM 204.5 39.5
6/7/2019 5:45:57 PM 204.4 39.4
6/7/2019 5:45:58 PM 204.3 39.3
6/7/2019 5:45:59 PM 204.1 39.1
6/7/2019 5:46:00 PM 204.0 39.0
6/7/2019 5:46:01 PM 203.9 38.9
6/7/2019 5:46:02 PM 203.8 38.8
6/7/2019 5:46:03 PM 203.7 38.7
6/7/2019 5:46:04 PM 203.6 38.6
6/7/2019 5:46:05 PM 203.5 38.5
6/7/2019 5:46:06 PM 203.4 38.4
6/7/2019 5:46:07 PM 203.3 38.3
6/7/2019 5:46:08 PM 203.2 38.2
6/7/2019 5:46:09 PM 203.1 38.1
6/7/2019 5:46:10 PM 203.0 38.0
6/7/2019 5:46:11 PM 202.9 37.9
6/7/2019 5:46:12 PM 202.8 37.8
Page 420 of 452 August 2019
APPENDIX E56: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-4 Data Log
6/7/2019 5:46:13 PM 202.7 37.7
6/7/2019 5:46:14 PM 202.5 37.5
6/7/2019 5:46:15 PM 202.4 37.4
6/7/2019 5:46:16 PM 202.3 37.3
6/7/2019 5:46:17 PM 202.2 37.2
6/7/2019 5:46:18 PM 202.1 37.1
6/7/2019 5:46:19 PM 202.0 37.0
6/7/2019 5:46:20 PM 201.9 36.9
6/7/2019 5:46:21 PM 201.8 36.8
6/7/2019 5:46:22 PM 201.8 36.8
6/7/2019 5:46:23 PM 201.7 36.7
6/7/2019 5:46:24 PM 201.6 36.6
6/7/2019 5:46:25 PM 201.5 36.5
6/7/2019 5:46:26 PM 201.4 36.4
6/7/2019 5:46:27 PM 201.3 36.3
6/7/2019 5:46:28 PM 201.2 36.2
6/7/2019 5:46:29 PM 201.1 36.1
6/7/2019 5:46:30 PM 201.0 36.0
6/7/2019 5:46:31 PM 200.9 35.9
6/7/2019 5:46:32 PM 200.8 35.8
6/7/2019 5:46:33 PM 200.7 35.7
6/7/2019 5:46:34 PM 200.6 35.6
6/7/2019 5:46:35 PM 200.5 35.5
6/7/2019 5:46:36 PM 200.4 35.4
6/7/2019 5:46:37 PM 200.2 35.2
6/7/2019 5:46:38 PM 200.1 35.1
6/7/2019 5:46:39 PM 200.0 35.0
6/7/2019 5:46:40 PM 199.9 34.9
6/7/2019 5:46:41 PM 199.8 34.8
6/7/2019 5:46:42 PM 199.6 34.6
6/7/2019 5:46:43 PM 199.6 34.6
6/7/2019 5:46:44 PM 199.5 34.5
6/7/2019 5:46:45 PM 199.3 34.3
6/7/2019 5:46:46 PM 199.2 34.2
6/7/2019 5:46:47 PM 199.1 34.1
6/7/2019 5:46:48 PM 199.1 34.1
6/7/2019 5:46:49 PM 199.0 34.0
6/7/2019 5:46:50 PM 198.9 33.9
6/7/2019 5:46:51 PM 198.8 33.8
6/7/2019 5:46:52 PM 198.7 33.7
6/7/2019 5:46:53 PM 198.7 33.7
6/7/2019 5:46:54 PM 198.7 33.7
6/7/2019 5:46:55 PM 198.6 33.6
6/7/2019 5:46:56 PM 198.6 33.6
6/7/2019 5:46:57 PM 198.5 33.5
6/7/2019 5:46:58 PM 198.5 33.5
6/7/2019 5:46:59 PM 198.5 33.5
6/7/2019 5:47:00 PM 198.4 33.4
6/7/2019 5:47:01 PM 198.4 33.4
6/7/2019 5:47:02 PM 198.3 33.3
6/7/2019 5:47:03 PM 198.3 33.3
6/7/2019 5:47:04 PM 198.2 33.2
6/7/2019 5:47:05 PM 198.2 33.2
6/7/2019 5:47:06 PM 198.1 33.1
6/7/2019 5:47:07 PM 198.1 33.1
6/7/2019 5:47:08 PM 198.0 33.0
6/7/2019 5:47:09 PM 198.0 33.0
6/7/2019 5:47:10 PM 197.9 32.9
6/7/2019 5:47:11 PM 197.8 32.8
6/7/2019 5:47:12 PM 197.8 32.8
6/7/2019 5:47:13 PM 197.7 32.7
6/7/2019 5:47:14 PM 197.6 32.6
6/7/2019 5:47:15 PM 197.5 32.5
6/7/2019 5:47:16 PM 197.4 32.4
6/7/2019 5:47:17 PM 197.3 32.3
6/7/2019 5:47:18 PM 197.3 32.3
6/7/2019 5:47:19 PM 197.2 32.2
6/7/2019 5:47:20 PM 197.1 32.1
6/7/2019 5:47:21 PM 197.0 32.0
6/7/2019 5:47:22 PM 196.9 31.9
6/7/2019 5:47:23 PM 196.8 31.8
6/7/2019 5:47:24 PM 196.7 31.7
6/7/2019 5:47:25 PM 196.7 31.7
6/7/2019 5:47:26 PM 196.6 31.6
6/7/2019 5:47:27 PM 196.5 31.5
6/7/2019 5:47:28 PM 196.5 31.5
6/7/2019 5:47:29 PM 196.4 31.4
6/7/2019 5:47:30 PM 196.4 31.4
6/7/2019 5:47:31 PM 196.3 31.3
Page 421 of 452 August 2019
APPENDIX E56: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-4 Data Log
6/7/2019 5:47:32 PM 196.3 31.3
6/7/2019 5:47:33 PM 196.2 31.2
6/7/2019 5:47:34 PM 196.2 31.2
6/7/2019 5:47:35 PM 196.1 31.1
6/7/2019 5:47:36 PM 196.1 31.1
6/7/2019 5:47:37 PM 196.0 31.0
6/7/2019 5:47:38 PM 196.0 31.0
6/7/2019 5:47:39 PM 195.9 30.9
6/7/2019 5:47:40 PM 195.9 30.9
6/7/2019 5:47:41 PM 195.8 30.8
6/7/2019 5:47:42 PM 195.8 30.8
6/7/2019 5:47:43 PM 195.7 30.7
6/7/2019 5:47:44 PM 195.7 30.7
6/7/2019 5:47:45 PM 195.6 30.6
6/7/2019 5:47:46 PM 195.6 30.6
6/7/2019 5:47:47 PM 195.5 30.5
6/7/2019 5:47:48 PM 195.5 30.5
6/7/2019 5:47:49 PM 195.4 30.4
6/7/2019 5:47:50 PM 195.4 30.4
6/7/2019 5:47:51 PM 195.4 30.4
6/7/2019 5:47:52 PM 195.3 30.3
6/7/2019 5:47:53 PM 195.3 30.3
6/7/2019 5:47:54 PM 195.3 30.3
6/7/2019 5:47:55 PM 195.3 30.3
6/7/2019 5:47:56 PM 195.3 30.3
6/7/2019 5:47:57 PM 195.3 30.3
6/7/2019 5:47:58 PM 195.2 30.2
6/7/2019 5:47:59 PM 195.2 30.2
6/7/2019 5:48:00 PM 195.2 30.2
6/7/2019 5:48:01 PM 195.2 30.2
6/7/2019 5:48:02 PM 195.1 30.1
6/7/2019 5:48:03 PM 195.1 30.1
6/7/2019 5:48:04 PM 195.1 30.1
6/7/2019 5:48:05 PM 195.1 30.1
6/7/2019 5:48:06 PM 195.0 30.0
6/7/2019 5:48:07 PM 195.0 30.0
6/7/2019 5:48:08 PM 195.0 30.0
6/7/2019 5:48:09 PM 194.9 29.9
6/7/2019 5:48:10 PM 194.9 29.9
6/7/2019 5:48:11 PM 194.8 29.8
6/7/2019 5:48:12 PM 194.8 29.8
6/7/2019 5:48:13 PM 194.7 29.7
6/7/2019 5:48:14 PM 194.7 29.7
6/7/2019 5:48:15 PM 194.6 29.6
6/7/2019 5:48:16 PM 194.6 29.6
6/7/2019 5:48:17 PM 194.5 29.5
6/7/2019 5:48:18 PM 194.4 29.4
6/7/2019 5:48:19 PM 194.4 29.4
6/7/2019 5:48:20 PM 194.3 29.3
6/7/2019 5:48:21 PM 194.2 29.2
6/7/2019 5:48:22 PM 194.2 29.2
6/7/2019 5:48:23 PM 194.1 29.1
6/7/2019 5:48:24 PM 194.0 29.0
6/7/2019 5:48:25 PM 194.0 29.0
6/7/2019 5:48:26 PM 193.9 28.9
6/7/2019 5:48:27 PM 193.8 28.8
6/7/2019 5:48:28 PM 193.7 28.7
6/7/2019 5:48:29 PM 193.7 28.7
6/7/2019 5:48:30 PM 193.6 28.6
6/7/2019 5:48:31 PM 193.5 28.5
6/7/2019 5:48:32 PM 193.4 28.4
6/7/2019 5:48:33 PM 193.4 28.4
6/7/2019 5:48:34 PM 193.3 28.3
6/7/2019 5:48:35 PM 193.2 28.2
6/7/2019 5:48:36 PM 193.1 28.1
6/7/2019 5:48:37 PM 193.1 28.1
6/7/2019 5:48:38 PM 193.0 28.0
6/7/2019 5:48:39 PM 192.9 27.9
6/7/2019 5:48:40 PM 192.8 27.8
6/7/2019 5:48:41 PM 192.7 27.7
6/7/2019 5:48:42 PM 192.6 27.6
6/7/2019 5:48:43 PM 192.6 27.6
6/7/2019 5:48:44 PM 192.5 27.5
6/7/2019 5:48:45 PM 192.4 27.4
6/7/2019 5:48:46 PM 192.3 27.3
6/7/2019 5:48:47 PM 192.2 27.2
6/7/2019 5:48:48 PM 192.1 27.1
6/7/2019 5:48:49 PM 192.0 27.0
6/7/2019 5:48:50 PM 191.9 26.9
Page 422 of 452 August 2019
APPENDIX E56: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-4 Data Log
6/7/2019 5:48:51 PM 191.8 26.8
6/7/2019 5:48:52 PM 191.7 26.7
6/7/2019 5:48:53 PM 191.6 26.6
6/7/2019 5:48:54 PM 191.5 26.5
6/7/2019 5:48:55 PM 191.3 26.3
6/7/2019 5:48:56 PM 191.2 26.2
6/7/2019 5:48:57 PM 191.1 26.1
6/7/2019 5:48:58 PM 191.0 26.0
6/7/2019 5:48:59 PM 190.9 25.9
6/7/2019 5:49:00 PM 190.8 25.8
6/7/2019 5:49:01 PM 190.7 25.7
6/7/2019 5:49:02 PM 190.6 25.6
6/7/2019 5:49:03 PM 190.5 25.5
6/7/2019 5:49:04 PM 190.4 25.4
6/7/2019 5:49:05 PM 190.3 25.3
6/7/2019 5:49:06 PM 190.3 25.3
6/7/2019 5:49:07 PM 190.2 25.2
6/7/2019 5:49:08 PM 190.1 25.1
6/7/2019 5:49:09 PM 190.0 25.0
6/7/2019 5:49:10 PM 190.0 25.0
6/7/2019 5:49:11 PM 189.9 24.9
6/7/2019 5:49:12 PM 189.8 24.8
6/7/2019 5:49:13 PM 189.8 24.8
6/7/2019 5:49:14 PM 189.7 24.7
6/7/2019 5:49:15 PM 189.7 24.7
6/7/2019 5:49:16 PM 189.6 24.6
6/7/2019 5:49:17 PM 189.6 24.6
6/7/2019 5:49:18 PM 189.5 24.5
6/7/2019 5:49:19 PM 189.5 24.5
6/7/2019 5:49:20 PM 189.4 24.4
6/7/2019 5:49:21 PM 189.4 24.4
6/7/2019 5:49:22 PM 189.3 24.3
6/7/2019 5:49:23 PM 189.3 24.3
6/7/2019 5:49:24 PM 189.2 24.2
6/7/2019 5:49:25 PM 189.2 24.2
6/7/2019 5:49:26 PM 189.1 24.1
6/7/2019 5:49:27 PM 189.1 24.1
6/7/2019 5:49:28 PM 189.0 24.0
6/7/2019 5:49:29 PM 189.0 24.0
6/7/2019 5:49:30 PM 188.9 23.9
6/7/2019 5:49:31 PM 188.9 23.9
6/7/2019 5:49:32 PM 188.8 23.8
6/7/2019 5:49:33 PM 188.8 23.8
6/7/2019 5:49:34 PM 188.7 23.7
6/7/2019 5:49:35 PM 188.7 23.7
6/7/2019 5:49:36 PM 188.6 23.6
6/7/2019 5:49:37 PM 188.6 23.6
6/7/2019 5:49:38 PM 188.5 23.5
6/7/2019 5:49:39 PM 188.5 23.5
6/7/2019 5:49:40 PM 188.4 23.4
6/7/2019 5:49:41 PM 188.4 23.4
6/7/2019 5:49:42 PM 188.3 23.3
6/7/2019 5:49:43 PM 188.3 23.3
6/7/2019 5:49:44 PM 188.2 23.2
6/7/2019 5:49:45 PM 188.2 23.2
6/7/2019 5:49:46 PM 188.1 23.1
6/7/2019 5:49:47 PM 188.0 23.0
6/7/2019 5:49:48 PM 188.0 23.0
6/7/2019 5:49:49 PM 188.0 23.0
6/7/2019 5:49:50 PM 187.9 22.9
6/7/2019 5:49:51 PM 187.9 22.9
6/7/2019 5:49:52 PM 187.9 22.9
6/7/2019 5:49:53 PM 187.9 22.9
6/7/2019 5:49:54 PM 187.9 22.9
6/7/2019 5:49:55 PM 187.9 22.9
6/7/2019 5:49:56 PM 187.9 22.9
6/7/2019 5:49:57 PM 188.0 23.0
6/7/2019 5:49:58 PM 188.0 23.0
6/7/2019 5:49:59 PM 188.1 23.1
6/7/2019 5:50:00 PM 188.1 23.1
6/7/2019 5:50:01 PM 188.2 23.2
6/7/2019 5:50:02 PM 188.2 23.2
6/7/2019 5:50:03 PM 188.2 23.2
6/7/2019 5:50:04 PM 188.3 23.3
6/7/2019 5:50:05 PM 188.3 23.3
6/7/2019 5:50:06 PM 188.4 23.4
6/7/2019 5:50:07 PM 188.4 23.4
6/7/2019 5:50:08 PM 188.4 23.4
6/7/2019 5:50:09 PM 188.4 23.4
Page 423 of 452 August 2019
APPENDIX E56: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-C1 TEST-4 Data Log
6/7/2019 5:50:10 PM 188.4 23.4
6/7/2019 5:50:11 PM 188.4 23.4
6/7/2019 5:50:12 PM 188.4 23.4
6/7/2019 5:50:13 PM 188.3 23.3
6/7/2019 5:50:14 PM 188.3 23.3
6/7/2019 5:50:15 PM 188.3 23.3
6/7/2019 5:50:16 PM 188.2 23.2
6/7/2019 5:50:17 PM 188.2 23.2
6/7/2019 5:50:18 PM 188.1 23.1
6/7/2019 5:50:19 PM 188.1 23.1
6/7/2019 5:50:20 PM 188.0 23.0
6/7/2019 5:50:21 PM 188.0 23.0
6/7/2019 5:50:22 PM 187.9 22.9
6/7/2019 5:50:23 PM 187.9 22.9
6/7/2019 5:50:24 PM 187.8 22.8
6/7/2019 5:50:25 PM 187.8 22.8
6/7/2019 5:50:26 PM 187.7 22.7
6/7/2019 5:50:27 PM 187.7 22.7
6/7/2019 5:50:28 PM 187.6 22.6
6/7/2019 5:50:29 PM 187.6 22.6
6/7/2019 5:50:30 PM 187.5 22.5
6/7/2019 5:50:31 PM 187.5 22.5
6/7/2019 5:50:32 PM 187.4 22.4
6/7/2019 5:50:33 PM 187.4 22.4
6/7/2019 5:50:34 PM 187.3 22.3
6/7/2019 5:50:35 PM 187.3 22.3
6/7/2019 5:50:36 PM 187.3 22.3
6/7/2019 5:50:37 PM 187.2 22.2
6/7/2019 5:50:38 PM 187.2 22.2
6/7/2019 5:50:39 PM 187.2 22.2
6/7/2019 5:50:40 PM 187.2 22.2
6/7/2019 5:50:41 PM 187.1 22.1
6/7/2019 5:50:42 PM 187.1 22.1
6/7/2019 5:50:43 PM 187.1 22.1
6/7/2019 5:50:44 PM 187.1 22.1
6/7/2019 5:50:45 PM 187.0 22.0
6/7/2019 5:50:46 PM 187.0 22.0
6/7/2019 5:50:47 PM 187.0 22.0
6/7/2019 5:50:48 PM 187.0 22.0
6/7/2019 5:50:49 PM 187.0 22.0
6/7/2019 5:50:50 PM 187.0 22.0
6/7/2019 5:50:51 PM 187.0 22.0
6/7/2019 5:50:52 PM 187.0 22.0
6/7/2019 5:50:53 PM 187.0 22.0
6/7/2019 5:50:54 PM 187.0 22.0
6/7/2019 5:50:55 PM 187.0 22.0
6/7/2019 5:50:56 PM 187.0 22.0
6/7/2019 5:50:57 PM 187.0 22.0
6/7/2019 5:50:58 PM 187.0 22.0
6/7/2019 5:50:59 PM 187.0 22.0
6/7/2019 5:51:00 PM 187.0 22.0
Page 424 of 452 August 2019
APPENDIX E56: SALT DILUTION GAUGING SUMMARY
SEEP-C1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-C1 TEST-4 1625
SEEP-C1 TEST-4 1626
SEEP-C1 TEST-4 1627
SEEP-C1 TEST-4 1628
Location EC Reading
(µS/cms)
SEEP-C1 TEST-4 1,115
SEEP-C1 TEST-4 2,150
SEEP-C1 TEST-4 16,651
SEEP-C1 TEST-4 132,589
q 300,200
K 1.3293
0.8
11.9
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)
(µS/cms)
(µS/cms)
24.1
24.2
24.2
(µS/cms)(°C)
Table E2 SEEP-C1 TEST-4 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
142.9 21.4
141.8 21.8
142.6 21.4
Calibration Temperature
154.3 21.7
Average 145.4 (µS/cms)
Geometric Mean 145.3
Average (pre-test)165.0
Average (post-test)190.9
Table E3 SEEP-C1 TEST-4 YSI Salt Dilution Calibration Data
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)530,862.5 (s) . (µS/cms)
(mg/L)(°C)
100
1,000
10,000
100,000 24.1
Table E4 SEEP-C1 TEST-4 Flow Calculation Summary
Mass of Salt injected mg
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Slope of Calibration Curve (µS/cms) / (mg/L)
Calculated Flow Rate Q
L/s
GPM
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 425 of 452 August 2019
APPENDIX E57: SALT DILUTION GAUGING SUMMARY
SEEP-D1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 3:31:43 PM 183.7 -
6/7/2019 3:31:44 PM 183.7 -
6/7/2019 3:31:45 PM 183.7 -
6/7/2019 3:31:46 PM 183.8 -
6/7/2019 3:31:47 PM 183.8 -
6/7/2019 3:31:48 PM 183.7 -
6/7/2019 3:31:49 PM 183.7 -
6/7/2019 3:31:50 PM 183.7 -
6/7/2019 3:31:51 PM 183.7 -
6/7/2019 3:31:52 PM 183.7 -
6/7/2019 3:31:53 PM 183.7 -
6/7/2019 3:31:54 PM 183.7 -
6/7/2019 3:31:55 PM 183.7 -
6/7/2019 3:31:56 PM 183.6 -
6/7/2019 3:31:57 PM 183.6 -
6/7/2019 3:31:58 PM 183.5 -
6/7/2019 3:31:59 PM 183.5 -
6/7/2019 3:32:00 PM 183.4 -
6/7/2019 3:32:01 PM 183.5 -
6/7/2019 3:32:02 PM 236.9 53.2
6/7/2019 3:32:03 PM 461.3 277.6
6/7/2019 3:32:04 PM 2222.0 2038.3
6/7/2019 3:32:05 PM 4353.0 4169.3
6/7/2019 3:32:06 PM 6225.2 6041.5
6/7/2019 3:32:07 PM 7492.9 7309.2
6/7/2019 3:32:08 PM 9474.1 9290.4
6/7/2019 3:32:09 PM 10104.2 9920.5
6/7/2019 3:32:10 PM 10155.4 9971.7
6/7/2019 3:32:11 PM 10038.3 9854.6
6/7/2019 3:32:12 PM 8994.5 8810.8
6/7/2019 3:32:13 PM 8306.9 8123.2
6/7/2019 3:32:14 PM 7528.3 7344.6
6/7/2019 3:32:15 PM 6617.8 6434.1
6/7/2019 3:32:16 PM 5471.7 5288.0
6/7/2019 3:32:17 PM 5131.1 4947.4
6/7/2019 3:32:18 PM 4224.8 4041.1
6/7/2019 3:32:19 PM 3776.9 3593.2
6/7/2019 3:32:20 PM 3326.0 3142.3
6/7/2019 3:32:21 PM 2893.8 2710.1
6/7/2019 3:32:22 PM 2542.4 2358.7
6/7/2019 3:32:23 PM 2240.3 2056.6
6/7/2019 3:32:24 PM 1871.1 1687.4
6/7/2019 3:32:25 PM 1587.0 1403.3
6/7/2019 3:32:26 PM 1487.4 1303.7
6/7/2019 3:32:27 PM 1191.2 1007.5
6/7/2019 3:32:28 PM 1056.3 872.6
6/7/2019 3:32:29 PM 933.0 749.3
6/7/2019 3:32:30 PM 891.5 707.8
6/7/2019 3:32:31 PM 765.8 582.1
6/7/2019 3:32:32 PM 704.1 520.4
6/7/2019 3:32:33 PM 641.9 458.2
6/7/2019 3:32:34 PM 639.7 456.0
6/7/2019 3:32:35 PM 506.7 323.0
6/7/2019 3:32:36 PM 505.6 321.9
6/7/2019 3:32:37 PM 489.8 306.1
6/7/2019 3:32:38 PM 468.8 285.1
6/7/2019 3:32:39 PM 445.4 261.7
6/7/2019 3:32:40 PM 428.0 244.3
6/7/2019 3:32:41 PM 416.1 232.4
6/7/2019 3:32:42 PM 408.6 224.9
6/7/2019 3:32:43 PM 354.2 170.5
6/7/2019 3:32:44 PM 340.8 157.1
6/7/2019 3:32:45 PM 332.6 148.9
6/7/2019 3:32:46 PM 326.1 142.4
6/7/2019 3:32:47 PM 320.4 136.7
6/7/2019 3:32:48 PM 316.0 132.3
6/7/2019 3:32:49 PM 311.8 128.1
6/7/2019 3:32:50 PM 308.4 124.7
6/7/2019 3:32:51 PM 304.5 120.8
6/7/2019 3:32:52 PM 301.4 117.7
Table E1 SEEP-D1 TEST-1 Data Log
Page 426 of 452 August 2019
APPENDIX E57: SALT DILUTION GAUGING SUMMARY
SEEP-D1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-D1 TEST-1 Data Log
6/7/2019 3:32:53 PM 297.8 114.1
6/7/2019 3:32:54 PM 294.6 110.9
6/7/2019 3:32:55 PM 291.4 107.7
6/7/2019 3:32:56 PM 288.5 104.8
6/7/2019 3:32:57 PM 285.5 101.8
6/7/2019 3:32:58 PM 283.3 99.6
6/7/2019 3:32:59 PM 280.4 96.7
6/7/2019 3:33:00 PM 274.9 91.2
6/7/2019 3:33:01 PM 269.0 85.3
6/7/2019 3:33:02 PM 264.2 80.5
6/7/2019 3:33:03 PM 258.9 75.2
6/7/2019 3:33:04 PM 254.5 70.8
6/7/2019 3:33:05 PM 249.7 66.0
6/7/2019 3:33:06 PM 245.9 62.2
6/7/2019 3:33:07 PM 241.8 58.1
6/7/2019 3:33:08 PM 238.3 54.6
6/7/2019 3:33:09 PM 234.7 51.0
6/7/2019 3:33:10 PM 231.1 47.4
6/7/2019 3:33:11 PM 227.8 44.1
6/7/2019 3:33:12 PM 224.7 41.0
6/7/2019 3:33:13 PM 222.1 38.4
6/7/2019 3:33:14 PM 219.2 35.5
6/7/2019 3:33:15 PM 216.8 33.1
6/7/2019 3:33:16 PM 214.3 30.6
6/7/2019 3:33:17 PM 212.3 28.6
6/7/2019 3:33:18 PM 210.1 26.4
6/7/2019 3:33:19 PM 208.1 24.4
6/7/2019 3:33:20 PM 206.0 22.3
6/7/2019 3:33:21 PM 204.3 20.6
6/7/2019 3:33:22 PM 202.5 18.8
6/7/2019 3:33:23 PM 201.0 17.3
6/7/2019 3:33:24 PM 199.5 15.8
6/7/2019 3:33:25 PM 198.2 14.5
6/7/2019 3:33:26 PM 196.9 13.2
6/7/2019 3:33:27 PM 195.9 12.2
6/7/2019 3:33:28 PM 194.9 11.2
6/7/2019 3:33:29 PM 194.1 10.4
6/7/2019 3:33:30 PM 193.3 9.6
6/7/2019 3:33:31 PM 192.7 9.0
6/7/2019 3:33:32 PM 192.1 8.4
6/7/2019 3:33:33 PM 191.7 8.0
6/7/2019 3:33:34 PM 191.3 7.6
6/7/2019 3:33:35 PM 190.9 7.2
6/7/2019 3:33:36 PM 190.6 6.9
6/7/2019 3:33:37 PM 190.4 6.7
6/7/2019 3:33:38 PM 190.2 6.5
6/7/2019 3:33:39 PM 190.0 6.3
6/7/2019 3:33:40 PM 189.8 6.1
6/7/2019 3:33:41 PM 189.7 6.0
6/7/2019 3:33:42 PM 189.6 5.9
6/7/2019 3:33:43 PM 189.5 5.8
6/7/2019 3:33:44 PM 189.3 5.6
6/7/2019 3:33:45 PM 189.2 5.5
6/7/2019 3:33:46 PM 189.0 5.3
6/7/2019 3:33:47 PM 188.9 5.2
6/7/2019 3:33:48 PM 188.8 5.1
6/7/2019 3:33:49 PM 188.7 5.0
6/7/2019 3:33:50 PM 188.6 4.9
6/7/2019 3:33:51 PM 188.5 4.8
Page 427 of 452 August 2019
APPENDIX E57: SALT DILUTION GAUGING SUMMARY
SEEP-D1 TEST-1 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-D1 TEST-1 1520
SEEP-D1 TEST-1 1521
SEEP-D1 TEST-1 1522
SEEP-D1 TEST-1 1524
Location EC Reading
(µS/cms)
SEEP-D1 TEST-1 1,130
SEEP-D1 TEST-1 2,147
SEEP-D1 TEST-1 17,118
SEEP-D1 TEST-1 135,213
q 300,200
K 1.3558
3.1
48.5
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)
(µS/cms)
(µS/cms)
27.1
27.2
27.1
(µS/cms) (°C)
Table E2 SEEP-D1 TEST-1 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
182.9 19.6
184.1 19.4
185.2 19.1
Calibration Temperature
185.2 19.4
Average 184.4 (µS/cms)
Geometric Mean 184.3
Average (pre-test)183.7
Average (post-test)190.0
Table E3 SEEP-D1 TEST-1 YSI Salt Dilution Calibration Data
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)133,186.2 (s) . (µS/cms)
(mg/L)(°C)
100
1,000
10,000
100,000 27
Table E4 SEEP-D1 TEST-1 Flow Calculation Summary
Mass of Salt injected mg
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Slope of Calibration Curve (µS/cms) / (mg/L)
Calculated Flow Rate Q
L/s
GPM
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 428 of 452 August 2019
APPENDIX E58: SALT DILUTION GAUGING SUMMARY
SEEP-D1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 3:39:47 PM 179.5 -
6/7/2019 3:39:48 PM 179.3 -
6/7/2019 3:39:49 PM 179.2 -
6/7/2019 3:39:50 PM 179.2 -
6/7/2019 3:39:51 PM 179.1 -
6/7/2019 3:39:52 PM 179.0 -
6/7/2019 3:39:53 PM 179.0 -
6/7/2019 3:39:54 PM 179.0 -
6/7/2019 3:39:55 PM 179.0 -
6/7/2019 3:39:56 PM 179.0 -
6/7/2019 3:39:57 PM 179.0 -
6/7/2019 3:39:58 PM 179.0 -
6/7/2019 3:39:59 PM 179.1 -
6/7/2019 3:40:00 PM 179.3 -
6/7/2019 3:40:01 PM 179.4 -
6/7/2019 3:40:02 PM 179.5 -
6/7/2019 3:40:03 PM 179.6 -
6/7/2019 3:40:04 PM 179.7 -
6/7/2019 3:40:05 PM 179.8 -
6/7/2019 3:40:06 PM 179.9 -
6/7/2019 3:40:07 PM 180.1 -
6/7/2019 3:40:08 PM 180.5 -
6/7/2019 3:40:09 PM 308.5 129.1
6/7/2019 3:40:10 PM 668.7 489.3
6/7/2019 3:40:11 PM 1924.7 1745.3
6/7/2019 3:40:12 PM 3249.7 3070.3
6/7/2019 3:40:13 PM 4203.8 4024.4
6/7/2019 3:40:14 PM 5468.0 5288.6
6/7/2019 3:40:15 PM 6179.0 5999.6
6/7/2019 3:40:16 PM 6697.1 6517.7
6/7/2019 3:40:17 PM 6867.5 6688.1
6/7/2019 3:40:18 PM 6949.9 6770.5
6/7/2019 3:40:19 PM 6953.2 6773.8
6/7/2019 3:40:20 PM 6545.4 6366.0
6/7/2019 3:40:21 PM 6201.1 6021.7
6/7/2019 3:40:22 PM 5535.0 5355.6
6/7/2019 3:40:23 PM 5072.0 4892.6
6/7/2019 3:40:24 PM 4526.7 4347.3
6/7/2019 3:40:25 PM 4181.4 4002.0
6/7/2019 3:40:26 PM 3615.5 3436.1
6/7/2019 3:40:27 PM 3482.4 3303.0
6/7/2019 3:40:28 PM 3119.1 2939.7
6/7/2019 3:40:29 PM 2741.2 2561.8
6/7/2019 3:40:30 PM 2474.8 2295.4
6/7/2019 3:40:31 PM 2245.3 2065.9
6/7/2019 3:40:32 PM 1997.2 1817.8
6/7/2019 3:40:33 PM 1819.8 1640.4
6/7/2019 3:40:34 PM 1634.3 1454.9
6/7/2019 3:40:35 PM 1491.4 1312.0
6/7/2019 3:40:36 PM 1352.8 1173.4
6/7/2019 3:40:37 PM 1224.1 1044.7
6/7/2019 3:40:38 PM 1217.1 1037.7
6/7/2019 3:40:39 PM 1066.5 887.1
6/7/2019 3:40:40 PM 1038.2 858.8
6/7/2019 3:40:41 PM 962.7 783.3
6/7/2019 3:40:42 PM 901.5 722.1
6/7/2019 3:40:43 PM 863.7 684.3
6/7/2019 3:40:44 PM 788.3 608.9
6/7/2019 3:40:45 PM 703.2 523.8
6/7/2019 3:40:46 PM 716.6 537.2
6/7/2019 3:40:47 PM 681.9 502.5
6/7/2019 3:40:48 PM 671.0 491.6
6/7/2019 3:40:49 PM 659.2 479.8
6/7/2019 3:40:50 PM 655.5 476.1
6/7/2019 3:40:51 PM 572.7 393.3
6/7/2019 3:40:52 PM 576.8 397.4
6/7/2019 3:40:53 PM 547.3 367.9
6/7/2019 3:40:54 PM 533.6 354.2
6/7/2019 3:40:55 PM 524.3 344.9
6/7/2019 3:40:56 PM 511.0 331.6
Table E1 SEEP-D1 TEST-2 Data Log
Page 429 of 452 August 2019
APPENDIX E58: SALT DILUTION GAUGING SUMMARY
SEEP-D1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-D1 TEST-2 Data Log
6/7/2019 3:40:57 PM 502.1 322.7
6/7/2019 3:40:58 PM 497.5 318.1
6/7/2019 3:40:59 PM 491.1 311.7
6/7/2019 3:41:00 PM 440.9 261.5
6/7/2019 3:41:01 PM 432.0 252.6
6/7/2019 3:41:02 PM 419.6 240.2
6/7/2019 3:41:03 PM 401.2 221.8
6/7/2019 3:41:04 PM 400.3 220.9
6/7/2019 3:41:05 PM 396.6 217.2
6/7/2019 3:41:06 PM 392.7 213.3
6/7/2019 3:41:07 PM 386.8 207.4
6/7/2019 3:41:08 PM 381.3 201.9
6/7/2019 3:41:09 PM 376.4 197.0
6/7/2019 3:41:10 PM 372.9 193.5
6/7/2019 3:41:11 PM 368.0 188.6
6/7/2019 3:41:12 PM 365.9 186.5
6/7/2019 3:41:13 PM 361.8 182.4
6/7/2019 3:41:14 PM 358.9 179.5
6/7/2019 3:41:15 PM 355.5 176.1
6/7/2019 3:41:16 PM 352.6 173.2
6/7/2019 3:41:17 PM 345.4 166.0
6/7/2019 3:41:18 PM 339.5 160.1
6/7/2019 3:41:19 PM 333.1 153.7
6/7/2019 3:41:20 PM 328.6 149.2
6/7/2019 3:41:21 PM 323.5 144.1
6/7/2019 3:41:22 PM 318.9 139.5
6/7/2019 3:41:23 PM 314.1 134.7
6/7/2019 3:41:24 PM 309.7 130.3
6/7/2019 3:41:25 PM 304.6 125.2
6/7/2019 3:41:26 PM 300.2 120.8
6/7/2019 3:41:27 PM 295.5 116.1
6/7/2019 3:41:28 PM 291.6 112.2
6/7/2019 3:41:29 PM 287.2 107.8
6/7/2019 3:41:30 PM 283.0 103.6
6/7/2019 3:41:31 PM 279.4 100.0
6/7/2019 3:41:32 PM 275.4 96.0
6/7/2019 3:41:33 PM 272.2 92.8
6/7/2019 3:41:34 PM 268.6 89.2
6/7/2019 3:41:35 PM 265.6 86.2
6/7/2019 3:41:36 PM 262.4 83.0
6/7/2019 3:41:37 PM 259.9 80.5
6/7/2019 3:41:38 PM 257.1 77.7
6/7/2019 3:41:39 PM 254.7 75.3
6/7/2019 3:41:40 PM 252.0 72.6
6/7/2019 3:41:41 PM 249.9 70.5
6/7/2019 3:41:42 PM 247.6 68.2
6/7/2019 3:41:43 PM 245.7 66.3
6/7/2019 3:41:44 PM 243.6 64.2
6/7/2019 3:41:45 PM 241.7 62.3
6/7/2019 3:41:46 PM 239.6 60.2
6/7/2019 3:41:47 PM 238.0 58.6
6/7/2019 3:41:48 PM 236.3 56.9
6/7/2019 3:41:49 PM 234.9 55.5
6/7/2019 3:41:50 PM 233.4 54.0
6/7/2019 3:41:51 PM 232.3 52.9
6/7/2019 3:41:52 PM 231.3 51.9
6/7/2019 3:41:53 PM 230.4 51.0
6/7/2019 3:41:54 PM 229.6 50.2
6/7/2019 3:41:55 PM 228.9 49.5
6/7/2019 3:41:56 PM 228.2 48.8
6/7/2019 3:41:57 PM 227.7 48.3
6/7/2019 3:41:58 PM 226.9 47.5
6/7/2019 3:41:59 PM 226.3 46.9
6/7/2019 3:42:00 PM 225.6 46.2
6/7/2019 3:42:01 PM 224.9 45.5
6/7/2019 3:42:02 PM 224.2 44.8
6/7/2019 3:42:03 PM 223.6 44.2
6/7/2019 3:42:04 PM 223.0 43.6
6/7/2019 3:42:05 PM 222.5 43.1
6/7/2019 3:42:06 PM 222.0 42.6
6/7/2019 3:42:07 PM 221.5 42.1
6/7/2019 3:42:08 PM 221.0 41.6
6/7/2019 3:42:09 PM 220.4 41.0
6/7/2019 3:42:10 PM 219.7 40.3
6/7/2019 3:42:11 PM 219.2 39.8
6/7/2019 3:42:12 PM 218.5 39.1
6/7/2019 3:42:13 PM 217.8 38.4
Page 430 of 452 August 2019
APPENDIX E58: SALT DILUTION GAUGING SUMMARY
SEEP-D1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-D1 TEST-2 Data Log
6/7/2019 3:42:14 PM 217.1 37.7
6/7/2019 3:42:15 PM 216.3 36.9
6/7/2019 3:42:16 PM 215.5 36.1
6/7/2019 3:42:17 PM 214.5 35.1
6/7/2019 3:42:18 PM 213.7 34.3
6/7/2019 3:42:19 PM 212.7 33.3
6/7/2019 3:42:20 PM 211.8 32.4
6/7/2019 3:42:21 PM 210.9 31.5
6/7/2019 3:42:22 PM 210.1 30.7
6/7/2019 3:42:23 PM 209.2 29.8
6/7/2019 3:42:24 PM 208.6 29.2
6/7/2019 3:42:25 PM 207.9 28.5
6/7/2019 3:42:26 PM 207.4 28.0
6/7/2019 3:42:27 PM 206.8 27.4
6/7/2019 3:42:28 PM 206.4 27.0
6/7/2019 3:42:29 PM 205.9 26.5
6/7/2019 3:42:30 PM 205.6 26.2
6/7/2019 3:42:31 PM 205.2 25.8
6/7/2019 3:42:32 PM 204.9 25.5
6/7/2019 3:42:33 PM 204.6 25.2
6/7/2019 3:42:34 PM 204.4 25.0
6/7/2019 3:42:35 PM 204.1 24.7
6/7/2019 3:42:36 PM 203.9 24.5
6/7/2019 3:42:37 PM 203.8 24.4
6/7/2019 3:42:38 PM 203.6 24.2
6/7/2019 3:42:39 PM 203.5 24.1
6/7/2019 3:42:40 PM 203.3 23.9
6/7/2019 3:42:41 PM 203.2 23.8
6/7/2019 3:42:42 PM 203.1 23.7
6/7/2019 3:42:43 PM 203.0 23.6
6/7/2019 3:42:44 PM 202.9 23.5
6/7/2019 3:42:45 PM 202.8 23.4
6/7/2019 3:42:46 PM 202.7 23.3
6/7/2019 3:42:47 PM 202.7 23.3
6/7/2019 3:42:48 PM 202.7 23.3
6/7/2019 3:42:49 PM 202.7 23.3
6/7/2019 3:42:50 PM 202.6 23.2
6/7/2019 3:42:51 PM 202.6 23.2
6/7/2019 3:42:52 PM 202.5 23.1
6/7/2019 3:42:53 PM 202.5 23.1
6/7/2019 3:42:54 PM 202.4 23.0
6/7/2019 3:42:55 PM 202.4 23.0
6/7/2019 3:42:56 PM 202.3 22.9
6/7/2019 3:42:57 PM 202.3 22.9
6/7/2019 3:42:58 PM 202.3 22.9
6/7/2019 3:42:59 PM 202.1 22.7
6/7/2019 3:43:00 PM 202.0 22.6
6/7/2019 3:43:01 PM 201.8 22.4
6/7/2019 3:43:02 PM 201.6 22.2
6/7/2019 3:43:03 PM 201.5 22.1
6/7/2019 3:43:04 PM 201.3 21.9
6/7/2019 3:43:05 PM 201.1 21.7
6/7/2019 3:43:06 PM 200.9 21.5
6/7/2019 3:43:07 PM 200.8 21.4
6/7/2019 3:43:08 PM 200.5 21.1
6/7/2019 3:43:09 PM 200.4 21.0
6/7/2019 3:43:10 PM 200.2 20.8
6/7/2019 3:43:11 PM 200.0 20.6
6/7/2019 3:43:12 PM 199.8 20.4
6/7/2019 3:43:13 PM 199.7 20.3
6/7/2019 3:43:14 PM 199.6 20.2
6/7/2019 3:43:15 PM 199.5 20.1
6/7/2019 3:43:16 PM 199.3 19.9
6/7/2019 3:43:17 PM 199.2 19.8
6/7/2019 3:43:18 PM 199.1 19.7
6/7/2019 3:43:19 PM 199.0 19.6
6/7/2019 3:43:20 PM 198.8 19.4
6/7/2019 3:43:21 PM 198.7 19.3
6/7/2019 3:43:22 PM 198.6 19.2
6/7/2019 3:43:23 PM 198.4 19.0
6/7/2019 3:43:24 PM 198.2 18.8
6/7/2019 3:43:25 PM 198.1 18.7
6/7/2019 3:43:26 PM 198.0 18.6
6/7/2019 3:43:27 PM 197.8 18.4
6/7/2019 3:43:28 PM 197.7 18.3
6/7/2019 3:43:29 PM 197.5 18.1
6/7/2019 3:43:30 PM 197.2 17.8
6/7/2019 3:43:31 PM 197.0 17.6
6/7/2019 3:43:32 PM 196.7 17.3
Page 431 of 452 August 2019
APPENDIX E58: SALT DILUTION GAUGING SUMMARY
SEEP-D1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-D1 TEST-2 Data Log
6/7/2019 3:43:33 PM 196.4 17.0
6/7/2019 3:43:34 PM 196.0 16.6
6/7/2019 3:43:35 PM 195.7 16.3
6/7/2019 3:43:36 PM 195.3 15.9
6/7/2019 3:43:37 PM 194.9 15.5
6/7/2019 3:43:38 PM 194.5 15.1
6/7/2019 3:43:39 PM 194.1 14.7
6/7/2019 3:43:40 PM 193.7 14.3
6/7/2019 3:43:41 PM 193.4 14.0
6/7/2019 3:43:42 PM 193.0 13.6
6/7/2019 3:43:43 PM 192.7 13.3
6/7/2019 3:43:44 PM 192.4 13.0
6/7/2019 3:43:45 PM 192.2 12.8
6/7/2019 3:43:46 PM 192.0 12.6
6/7/2019 3:43:47 PM 191.9 12.5
6/7/2019 3:43:48 PM 191.8 12.4
6/7/2019 3:43:49 PM 191.7 12.3
6/7/2019 3:43:50 PM 191.6 12.2
6/7/2019 3:43:51 PM 191.5 12.1
6/7/2019 3:43:52 PM 191.5 12.1
6/7/2019 3:43:53 PM 191.5 12.1
6/7/2019 3:43:54 PM 191.4 12.0
6/7/2019 3:43:55 PM 191.4 12.0
6/7/2019 3:43:56 PM 191.4 12.0
6/7/2019 3:43:57 PM 191.4 12.0
6/7/2019 3:43:58 PM 191.5 12.1
6/7/2019 3:43:59 PM 191.6 12.2
6/7/2019 3:44:00 PM 191.7 12.3
6/7/2019 3:44:01 PM 191.9 12.5
6/7/2019 3:44:02 PM 192.0 12.6
6/7/2019 3:44:03 PM 192.2 12.8
6/7/2019 3:44:04 PM 192.4 13.0
6/7/2019 3:44:05 PM 192.7 13.3
6/7/2019 3:44:06 PM 192.9 13.5
6/7/2019 3:44:07 PM 193.1 13.7
6/7/2019 3:44:08 PM 193.3 13.9
6/7/2019 3:44:09 PM 193.4 14.0
6/7/2019 3:44:10 PM 193.5 14.1
6/7/2019 3:44:11 PM 193.6 14.2
6/7/2019 3:44:12 PM 193.6 14.2
6/7/2019 3:44:13 PM 193.6 14.2
6/7/2019 3:44:14 PM 193.5 14.1
6/7/2019 3:44:15 PM 193.4 14.0
6/7/2019 3:44:16 PM 193.3 13.9
6/7/2019 3:44:17 PM 193.2 13.8
6/7/2019 3:44:18 PM 193.0 13.6
6/7/2019 3:44:19 PM 192.7 13.3
6/7/2019 3:44:20 PM 192.4 13.0
6/7/2019 3:44:21 PM 192.1 12.7
6/7/2019 3:44:22 PM 191.9 12.5
6/7/2019 3:44:23 PM 191.6 12.2
6/7/2019 3:44:24 PM 191.4 12.0
6/7/2019 3:44:25 PM 191.1 11.7
6/7/2019 3:44:26 PM 190.9 11.5
6/7/2019 3:44:27 PM 190.7 11.3
6/7/2019 3:44:28 PM 190.5 11.1
6/7/2019 3:44:29 PM 190.4 11.0
6/7/2019 3:44:30 PM 190.2 10.8
6/7/2019 3:44:31 PM 190.2 10.8
6/7/2019 3:44:32 PM 190.1 10.7
6/7/2019 3:44:33 PM 190.1 10.7
6/7/2019 3:44:34 PM 190.1 10.7
6/7/2019 3:44:35 PM 190.2 10.8
6/7/2019 3:44:36 PM 190.2 10.8
6/7/2019 3:44:37 PM 190.3 10.9
Page 432 of 452 August 2019
APPENDIX E58: SALT DILUTION GAUGING SUMMARY
SEEP-D1 TEST-2 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-D1 TEST-2 1520
SEEP-D1 TEST-2 1521
SEEP-D1 TEST-2 1522
SEEP-D1 TEST-2 1524
Location EC Reading
(µS/cms)
SEEP-D1 TEST-2 1,130
SEEP-D1 TEST-2 2,147
SEEP-D1 TEST-2 17,118
SEEP-D1 TEST-2 135,213
q 300,200
K 1.3558
3.2
51.3
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)
(µS/cms)
(µS/cms)
(µS/cms)(°C)
Table E2 SEEP-D1 TEST-2 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
182.9 19.6
184.1 19.4
185.2 19.1
Calibration Temperature
185.2 19.4
Average 184.4 (µS/cms)
Geometric Mean 184.3
Average (pre-test)183.7
Average (post-test)190.0
Table E3 SEEP-D1 TEST-2 YSI Salt Dilution Calibration Data
(mg/L)(°C)
100
1,000
10,000 27.1
27.2
27.1
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)125,873.3 (s) . (µS/cms)
Calculated Flow Rate Q
L/s
GPM
Slope of Calibration Curve (µS/cms) / (mg/L)
100,000 27
Table E4 SEEP-D1 TEST-2 Flow Calculation Summary
Mass of Salt injected mg
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 433 of 452 August 2019
APPENDIX E59: SALT DILUTION GAUGING SUMMARY
SEEP-D1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 3:49:09 PM 180.1 -
6/7/2019 3:49:10 PM 179.9 -
6/7/2019 3:49:11 PM 179.6 -
6/7/2019 3:49:12 PM 179.4 -
6/7/2019 3:49:13 PM 179.3 -
6/7/2019 3:49:14 PM 179.3 -
6/7/2019 3:49:15 PM 179.3 -
6/7/2019 3:49:16 PM 179.3 -
6/7/2019 3:49:17 PM 179.4 -
6/7/2019 3:49:18 PM 179.4 -
6/7/2019 3:49:19 PM 179.4 -
6/7/2019 3:49:20 PM 179.5 -
6/7/2019 3:49:21 PM 179.6 -
6/7/2019 3:49:22 PM 179.6 -
6/7/2019 3:49:23 PM 179.7 -
6/7/2019 3:49:24 PM 179.9 -
6/7/2019 3:49:25 PM 180.0 -
6/7/2019 3:49:26 PM 180.0 -
6/7/2019 3:49:27 PM 180.0 -
6/7/2019 3:49:28 PM 180.0 -
6/7/2019 3:49:29 PM 180.0 -
6/7/2019 3:49:30 PM 180.2 -
6/7/2019 3:49:31 PM 180.8 -
6/7/2019 3:49:32 PM 256.2 76.5
6/7/2019 3:49:33 PM 422.1 242.4
6/7/2019 3:49:34 PM 691.8 512.1
6/7/2019 3:49:35 PM 1178.5 998.8
6/7/2019 3:49:36 PM 2045.8 1866.1
6/7/2019 3:49:37 PM 4015.7 3836.0
6/7/2019 3:49:38 PM 5447.8 5268.1
6/7/2019 3:49:39 PM 6202.0 6022.3
6/7/2019 3:49:40 PM 7228.0 7048.3
6/7/2019 3:49:41 PM 7513.7 7334.0
6/7/2019 3:49:42 PM 7722.5 7542.8
6/7/2019 3:49:43 PM 7792.4 7612.7
6/7/2019 3:49:44 PM 7747.6 7567.9
6/7/2019 3:49:45 PM 7185.2 7005.5
6/7/2019 3:49:46 PM 6761.9 6582.2
6/7/2019 3:49:47 PM 6315.4 6135.7
6/7/2019 3:49:48 PM 5370.4 5190.7
6/7/2019 3:49:49 PM 5221.0 5041.3
6/7/2019 3:49:50 PM 4772.0 4592.3
6/7/2019 3:49:51 PM 4308.3 4128.6
6/7/2019 3:49:52 PM 4102.8 3923.1
6/7/2019 3:49:53 PM 3806.8 3627.1
6/7/2019 3:49:54 PM 3366.0 3186.3
6/7/2019 3:49:55 PM 2997.3 2817.6
6/7/2019 3:49:56 PM 2744.0 2564.3
6/7/2019 3:49:57 PM 2587.4 2407.7
6/7/2019 3:49:58 PM 2290.8 2111.1
6/7/2019 3:49:59 PM 2035.3 1855.6
6/7/2019 3:50:00 PM 1912.6 1732.9
6/7/2019 3:50:01 PM 1737.3 1557.6
6/7/2019 3:50:02 PM 1573.4 1393.7
6/7/2019 3:50:03 PM 1434.0 1254.3
6/7/2019 3:50:04 PM 1271.7 1092.0
6/7/2019 3:50:05 PM 1164.0 984.3
6/7/2019 3:50:06 PM 1134.0 954.3
6/7/2019 3:50:07 PM 1020.0 840.3
6/7/2019 3:50:08 PM 944.9 765.2
6/7/2019 3:50:09 PM 869.9 690.2
6/7/2019 3:50:10 PM 816.7 637.0
6/7/2019 3:50:11 PM 789.2 609.5
6/7/2019 3:50:12 PM 692.1 512.4
6/7/2019 3:50:13 PM 669.6 489.9
6/7/2019 3:50:14 PM 620.8 441.1
6/7/2019 3:50:15 PM 469.5 289.8
6/7/2019 3:50:16 PM 553.4 373.7
6/7/2019 3:50:17 PM 543.9 364.2
6/7/2019 3:50:18 PM 514.3 334.6
Table E1 SEEP-D1 TEST-3 Data Log
Page 434 of 452 August 2019
APPENDIX E59: SALT DILUTION GAUGING SUMMARY
SEEP-D1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-D1 TEST-3 Data Log
6/7/2019 3:50:19 PM 507.2 327.5
6/7/2019 3:50:20 PM 491.8 312.1
6/7/2019 3:50:21 PM 479.9 300.2
6/7/2019 3:50:22 PM 473.2 293.5
6/7/2019 3:50:23 PM 465.8 286.1
6/7/2019 3:50:24 PM 408.0 228.3
6/7/2019 3:50:25 PM 397.5 217.8
6/7/2019 3:50:26 PM 385.4 205.7
6/7/2019 3:50:27 PM 382.0 202.3
6/7/2019 3:50:28 PM 375.8 196.1
6/7/2019 3:50:29 PM 372.7 193.0
6/7/2019 3:50:30 PM 368.4 188.7
6/7/2019 3:50:31 PM 363.1 183.4
6/7/2019 3:50:32 PM 358.3 178.6
6/7/2019 3:50:33 PM 355.7 176.0
6/7/2019 3:50:34 PM 350.8 171.1
6/7/2019 3:50:35 PM 347.7 168.0
6/7/2019 3:50:36 PM 344.1 164.4
6/7/2019 3:50:37 PM 341.2 161.5
6/7/2019 3:50:38 PM 338.2 158.5
6/7/2019 3:50:39 PM 335.6 155.9
6/7/2019 3:50:40 PM 331.1 151.4
6/7/2019 3:50:41 PM 325.6 145.9
6/7/2019 3:50:42 PM 319.7 140.0
6/7/2019 3:50:43 PM 315.1 135.4
6/7/2019 3:50:44 PM 310.3 130.6
6/7/2019 3:50:45 PM 306.6 126.9
6/7/2019 3:50:46 PM 302.5 122.8
6/7/2019 3:50:47 PM 299.6 119.9
6/7/2019 3:50:48 PM 295.6 115.9
6/7/2019 3:50:49 PM 292.3 112.6
6/7/2019 3:50:50 PM 289.6 109.9
6/7/2019 3:50:51 PM 286.7 107.0
6/7/2019 3:50:52 PM 284.2 104.5
6/7/2019 3:50:53 PM 281.6 101.9
6/7/2019 3:50:54 PM 279.4 99.7
6/7/2019 3:50:55 PM 276.9 97.2
6/7/2019 3:50:56 PM 274.8 95.1
6/7/2019 3:50:57 PM 272.6 92.9
6/7/2019 3:50:58 PM 270.6 90.9
6/7/2019 3:50:59 PM 268.5 88.8
6/7/2019 3:51:00 PM 266.7 87.0
6/7/2019 3:51:01 PM 264.7 85.0
6/7/2019 3:51:02 PM 263.1 83.4
6/7/2019 3:51:03 PM 261.1 81.4
6/7/2019 3:51:04 PM 259.5 79.8
6/7/2019 3:51:05 PM 257.7 78.0
6/7/2019 3:51:06 PM 256.2 76.5
6/7/2019 3:51:07 PM 254.6 74.9
6/7/2019 3:51:08 PM 253.3 73.6
6/7/2019 3:51:09 PM 251.8 72.1
6/7/2019 3:51:10 PM 250.5 70.8
6/7/2019 3:51:11 PM 249.1 69.4
6/7/2019 3:51:12 PM 247.9 68.2
6/7/2019 3:51:13 PM 246.7 67.0
6/7/2019 3:51:14 PM 245.6 65.9
6/7/2019 3:51:15 PM 244.4 64.7
6/7/2019 3:51:16 PM 243.4 63.7
6/7/2019 3:51:17 PM 242.3 62.6
6/7/2019 3:51:18 PM 241.4 61.7
6/7/2019 3:51:19 PM 240.5 60.8
6/7/2019 3:51:20 PM 239.7 60.0
6/7/2019 3:51:21 PM 238.8 59.1
6/7/2019 3:51:22 PM 238.1 58.4
6/7/2019 3:51:23 PM 237.4 57.7
6/7/2019 3:51:24 PM 236.8 57.1
6/7/2019 3:51:25 PM 236.1 56.4
6/7/2019 3:51:26 PM 235.5 55.8
6/7/2019 3:51:27 PM 234.8 55.1
6/7/2019 3:51:28 PM 234.2 54.5
6/7/2019 3:51:29 PM 233.6 53.9
6/7/2019 3:51:30 PM 232.9 53.2
6/7/2019 3:51:31 PM 232.3 52.6
6/7/2019 3:51:32 PM 231.5 51.8
6/7/2019 3:51:33 PM 230.9 51.2
6/7/2019 3:51:34 PM 230.1 50.4
6/7/2019 3:51:35 PM 229.3 49.6
Page 435 of 452 August 2019
APPENDIX E59: SALT DILUTION GAUGING SUMMARY
SEEP-D1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-D1 TEST-3 Data Log
6/7/2019 3:51:36 PM 228.3 48.6
6/7/2019 3:51:37 PM 227.4 47.7
6/7/2019 3:51:38 PM 226.3 46.6
6/7/2019 3:51:39 PM 225.2 45.5
6/7/2019 3:51:40 PM 224.1 44.4
6/7/2019 3:51:41 PM 223.1 43.4
6/7/2019 3:51:42 PM 221.7 42.0
6/7/2019 3:51:43 PM 220.4 40.7
6/7/2019 3:51:44 PM 218.5 38.8
6/7/2019 3:51:45 PM 216.9 37.2
6/7/2019 3:51:46 PM 214.9 35.2
6/7/2019 3:51:47 PM 213.3 33.6
6/7/2019 3:51:48 PM 211.5 31.8
6/7/2019 3:51:49 PM 209.9 30.2
6/7/2019 3:51:50 PM 208.2 28.5
6/7/2019 3:51:51 PM 206.8 27.1
6/7/2019 3:51:52 PM 205.2 25.5
6/7/2019 3:51:53 PM 203.9 24.2
6/7/2019 3:51:54 PM 202.5 22.8
6/7/2019 3:51:55 PM 201.4 21.7
6/7/2019 3:51:56 PM 200.6 20.9
6/7/2019 3:51:57 PM 200.1 20.4
6/7/2019 3:51:58 PM 199.7 20.0
6/7/2019 3:51:59 PM 199.3 19.6
6/7/2019 3:52:00 PM 198.8 19.1
6/7/2019 3:52:01 PM 198.4 18.7
6/7/2019 3:52:02 PM 197.9 18.2
6/7/2019 3:52:03 PM 197.5 17.8
6/7/2019 3:52:04 PM 197.0 17.3
6/7/2019 3:52:05 PM 196.6 16.9
6/7/2019 3:52:06 PM 196.1 16.4
6/7/2019 3:52:07 PM 195.6 15.9
6/7/2019 3:52:08 PM 195.0 15.3
6/7/2019 3:52:09 PM 194.3 14.6
6/7/2019 3:52:10 PM 193.7 14.0
6/7/2019 3:52:11 PM 193.0 13.3
6/7/2019 3:52:12 PM 192.5 12.8
6/7/2019 3:52:13 PM 192.0 12.3
6/7/2019 3:52:14 PM 191.6 11.9
6/7/2019 3:52:15 PM 191.2 11.5
6/7/2019 3:52:16 PM 190.9 11.2
6/7/2019 3:52:17 PM 190.7 11.0
6/7/2019 3:52:18 PM 190.4 10.7
6/7/2019 3:52:19 PM 190.2 10.5
6/7/2019 3:52:20 PM 190.0 10.3
6/7/2019 3:52:21 PM 189.8 10.1
6/7/2019 3:52:22 PM 189.6 9.9
6/7/2019 3:52:23 PM 189.3 9.6
6/7/2019 3:52:24 PM 189.1 9.4
6/7/2019 3:52:25 PM 188.9 9.2
6/7/2019 3:52:26 PM 188.8 9.1
6/7/2019 3:52:27 PM 188.6 8.9
6/7/2019 3:52:28 PM 188.5 8.8
6/7/2019 3:52:29 PM 188.3 8.6
6/7/2019 3:52:30 PM 188.2 8.5
6/7/2019 3:52:31 PM 188.1 8.4
6/7/2019 3:52:32 PM 188.0 8.3
6/7/2019 3:52:33 PM 187.9 8.2
6/7/2019 3:52:34 PM 187.9 8.2
6/7/2019 3:52:35 PM 187.9 8.2
6/7/2019 3:52:36 PM 188.0 8.3
6/7/2019 3:52:37 PM 188.0 8.3
6/7/2019 3:52:38 PM 188.0 8.3
6/7/2019 3:52:39 PM 188.0 8.3
6/7/2019 3:52:40 PM 188.0 8.3
6/7/2019 3:52:41 PM 188.0 8.3
6/7/2019 3:52:42 PM 188.0 8.3
6/7/2019 3:52:43 PM 188.0 8.3
6/7/2019 3:52:44 PM 188.1 8.4
Page 436 of 452 August 2019
APPENDIX E59: SALT DILUTION GAUGING SUMMARY
SEEP-D1 TEST-3 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-D1 TEST-3 1520
SEEP-D1 TEST-3 1521
SEEP-D1 TEST-3 1522
SEEP-D1 TEST-3 1524
Location EC Reading
(µS/cms)
SEEP-D1 TEST-3 1,130
SEEP-D1 TEST-3 2,147
SEEP-D1 TEST-3 17,118
SEEP-D1 TEST-3 135,213
q 300,200
K 1.3558
2.9
45.2
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)
(µS/cms)
(µS/cms)
27.1
27.1
27.2
(µS/cms) (°C)
Table E2 SEEP-D1 TEST-3 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
182.9 19.6
184.1 19.4
185.2 19.1
Calibration Temperature
185.2 19.4
Average 184.4 (µS/cms)
Geometric Mean 184.3
Average (pre-test)179.7
Average (post-test)189.2
Table E3 SEEP-D1 TEST-3 YSI Salt Dilution Calibration Data
Integral of Conductivity
Data Curve
SUM:Δt(E
Ct-ECbkg)142,794.7 (s) . (µS/cms)
(mg/L)(°C)
100
1,000
10,000
100,000 27
Table E4 SEEP-D1 TEST-3 Flow Calculation Summary
Mass of Salt injected mg
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Slope of Calibration Curve (µS/cms) / (mg/L)
Calculated Flow Rate Q
L/s
GPM
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 437 of 452 August 2019
APPENDIX E60: SALT DILUTION GAUGING SUMMARY
SEEP-D1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
6/7/2019 3:57:21 PM 184.5 -
6/7/2019 3:57:22 PM 184.5 -
6/7/2019 3:57:23 PM 184.5 -
6/7/2019 3:57:24 PM 184.5 -
6/7/2019 3:57:25 PM 184.5 -
6/7/2019 3:57:26 PM 184.5 -
6/7/2019 3:57:27 PM 184.5 -
6/7/2019 3:57:28 PM 184.5 -
6/7/2019 3:57:29 PM 184.5 -
6/7/2019 3:57:30 PM 184.5 -
6/7/2019 3:57:31 PM 184.5 -
6/7/2019 3:57:32 PM 184.5 -
6/7/2019 3:57:33 PM 184.6 -
6/7/2019 3:57:34 PM 184.6 -
6/7/2019 3:57:35 PM 184.7 -
6/7/2019 3:57:36 PM 184.8 -
6/7/2019 3:57:37 PM 184.8 -
6/7/2019 3:57:38 PM 185.0 -
6/7/2019 3:57:39 PM 185.2 -
6/7/2019 3:57:40 PM 185.3 -
6/7/2019 3:57:41 PM 185.5 -
6/7/2019 3:57:42 PM 185.7 -
6/7/2019 3:57:43 PM 185.8 -
6/7/2019 3:57:44 PM 186.0 -
6/7/2019 3:57:45 PM 186.1 -
6/7/2019 3:57:46 PM 186.2 -
6/7/2019 3:57:47 PM 186.3 -
6/7/2019 3:57:48 PM 186.6 -
6/7/2019 3:57:49 PM 187.7 -
6/7/2019 3:57:50 PM 428.0 242.9
6/7/2019 3:57:51 PM 709.3 524.2
6/7/2019 3:57:52 PM 2066.6 1881.5
6/7/2019 3:57:53 PM 3110.7 2925.6
6/7/2019 3:57:54 PM 4608.4 4423.3
6/7/2019 3:57:55 PM 6135.0 5949.9
6/7/2019 3:57:56 PM 6688.8 6503.7
6/7/2019 3:57:57 PM 6997.8 6812.7
6/7/2019 3:57:58 PM 7162.1 6977.0
6/7/2019 3:57:59 PM 7230.5 7045.4
6/7/2019 3:58:00 PM 7192.8 7007.7
6/7/2019 3:58:01 PM 6467.4 6282.3
6/7/2019 3:58:02 PM 6039.1 5854.0
6/7/2019 3:58:03 PM 5437.9 5252.8
6/7/2019 3:58:04 PM 5177.2 4992.1
6/7/2019 3:58:05 PM 4407.9 4222.8
6/7/2019 3:58:06 PM 4082.7 3897.6
6/7/2019 3:58:07 PM 3578.9 3393.8
6/7/2019 3:58:08 PM 3408.5 3223.4
6/7/2019 3:58:09 PM 3091.1 2906.0
6/7/2019 3:58:10 PM 2801.1 2616.0
6/7/2019 3:58:11 PM 2532.3 2347.2
6/7/2019 3:58:12 PM 2423.7 2238.6
6/7/2019 3:58:13 PM 2117.1 1932.0
6/7/2019 3:58:14 PM 2010.5 1825.4
6/7/2019 3:58:15 PM 1825.6 1640.5
6/7/2019 3:58:16 PM 1781.8 1596.7
6/7/2019 3:58:17 PM 1609.2 1424.1
6/7/2019 3:58:18 PM 1434.9 1249.8
6/7/2019 3:58:19 PM 1332.9 1147.8
6/7/2019 3:58:20 PM 1269.0 1083.9
6/7/2019 3:58:21 PM 1170.1 985.0
6/7/2019 3:58:22 PM 1099.0 913.9
6/7/2019 3:58:23 PM 1068.1 883.0
6/7/2019 3:58:24 PM 1005.6 820.5
6/7/2019 3:58:25 PM 911.1 726.0
6/7/2019 3:58:26 PM 903.4 718.3
6/7/2019 3:58:27 PM 821.0 635.9
6/7/2019 3:58:28 PM 774.3 589.2
6/7/2019 3:58:29 PM 711.6 526.5
6/7/2019 3:58:30 PM 716.7 531.6
Table E1 SEEP-D1 TEST-4 Data Log
Page 438 of 452 August 2019
APPENDIX E60: SALT DILUTION GAUGING SUMMARY
SEEP-D1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-D1 TEST-4 Data Log
6/7/2019 3:58:31 PM 655.3 470.2
6/7/2019 3:58:32 PM 647.7 462.6
6/7/2019 3:58:33 PM 634.8 449.7
6/7/2019 3:58:34 PM 626.1 441.0
6/7/2019 3:58:35 PM 517.2 332.1
6/7/2019 3:58:36 PM 546.4 361.3
6/7/2019 3:58:37 PM 534.1 349.0
6/7/2019 3:58:38 PM 527.5 342.4
6/7/2019 3:58:39 PM 519.8 334.7
6/7/2019 3:58:40 PM 508.7 323.6
6/7/2019 3:58:41 PM 495.4 310.3
6/7/2019 3:58:42 PM 485.3 300.2
6/7/2019 3:58:43 PM 434.2 249.1
6/7/2019 3:58:44 PM 427.6 242.5
6/7/2019 3:58:45 PM 409.9 224.8
6/7/2019 3:58:46 PM 397.3 212.2
6/7/2019 3:58:47 PM 388.3 203.2
6/7/2019 3:58:48 PM 380.8 195.7
6/7/2019 3:58:49 PM 378.1 193.0
6/7/2019 3:58:50 PM 375.2 190.1
6/7/2019 3:58:51 PM 372.1 187.0
6/7/2019 3:58:52 PM 368.3 183.2
6/7/2019 3:58:53 PM 364.4 179.3
6/7/2019 3:58:54 PM 359.9 174.8
6/7/2019 3:58:55 PM 356.7 171.6
6/7/2019 3:58:56 PM 353.0 167.9
6/7/2019 3:58:57 PM 349.9 164.8
6/7/2019 3:58:58 PM 346.2 161.1
6/7/2019 3:58:59 PM 343.1 158.0
6/7/2019 3:59:00 PM 336.7 151.6
6/7/2019 3:59:01 PM 330.7 145.6
6/7/2019 3:59:02 PM 323.7 138.6
6/7/2019 3:59:03 PM 317.7 132.6
6/7/2019 3:59:04 PM 311.2 126.1
6/7/2019 3:59:05 PM 305.9 120.8
6/7/2019 3:59:06 PM 300.8 115.7
6/7/2019 3:59:07 PM 296.5 111.4
6/7/2019 3:59:08 PM 291.6 106.5
6/7/2019 3:59:09 PM 287.7 102.6
6/7/2019 3:59:10 PM 283.4 98.3
6/7/2019 3:59:11 PM 280.2 95.1
6/7/2019 3:59:12 PM 276.6 91.5
6/7/2019 3:59:13 PM 273.7 88.6
6/7/2019 3:59:14 PM 270.7 85.6
6/7/2019 3:59:15 PM 268.4 83.3
6/7/2019 3:59:16 PM 266.1 81.0
6/7/2019 3:59:17 PM 264.2 79.1
6/7/2019 3:59:18 PM 262.3 77.2
6/7/2019 3:59:19 PM 260.6 75.5
6/7/2019 3:59:20 PM 258.7 73.6
6/7/2019 3:59:21 PM 257.1 72.0
6/7/2019 3:59:22 PM 255.3 70.2
6/7/2019 3:59:23 PM 253.9 68.8
6/7/2019 3:59:24 PM 252.1 67.0
6/7/2019 3:59:25 PM 250.4 65.3
6/7/2019 3:59:26 PM 248.9 63.8
6/7/2019 3:59:27 PM 247.2 62.1
6/7/2019 3:59:28 PM 245.7 60.6
6/7/2019 3:59:29 PM 243.8 58.7
6/7/2019 3:59:30 PM 242.1 57.0
6/7/2019 3:59:31 PM 240.2 55.1
6/7/2019 3:59:32 PM 238.7 53.6
6/7/2019 3:59:33 PM 236.9 51.8
6/7/2019 3:59:34 PM 235.5 50.4
6/7/2019 3:59:35 PM 233.9 48.8
6/7/2019 3:59:36 PM 232.5 47.4
6/7/2019 3:59:37 PM 231.0 45.9
6/7/2019 3:59:38 PM 229.8 44.7
6/7/2019 3:59:39 PM 228.4 43.3
6/7/2019 3:59:40 PM 227.3 42.2
6/7/2019 3:59:41 PM 226.3 41.2
6/7/2019 3:59:42 PM 225.4 40.3
6/7/2019 3:59:43 PM 224.3 39.2
6/7/2019 3:59:44 PM 223.4 38.3
6/7/2019 3:59:45 PM 222.3 37.2
6/7/2019 3:59:46 PM 221.4 36.3
6/7/2019 3:59:47 PM 220.4 35.3
Page 439 of 452 August 2019
APPENDIX E60: SALT DILUTION GAUGING SUMMARY
SEEP-D1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-D1 TEST-4 Data Log
6/7/2019 3:59:48 PM 219.5 34.4
6/7/2019 3:59:49 PM 218.5 33.4
6/7/2019 3:59:50 PM 217.7 32.6
6/7/2019 3:59:51 PM 216.8 31.7
6/7/2019 3:59:52 PM 216.1 31.0
6/7/2019 3:59:53 PM 215.2 30.1
6/7/2019 3:59:54 PM 214.5 29.4
6/7/2019 3:59:55 PM 213.7 28.6
6/7/2019 3:59:56 PM 213.1 28.0
6/7/2019 3:59:57 PM 212.5 27.4
6/7/2019 3:59:58 PM 211.9 26.8
6/7/2019 3:59:59 PM 211.4 26.3
6/7/2019 4:00:00 PM 210.9 25.8
6/7/2019 4:00:01 PM 210.5 25.4
6/7/2019 4:00:02 PM 210.1 25.0
6/7/2019 4:00:03 PM 209.6 24.5
6/7/2019 4:00:04 PM 209.3 24.2
6/7/2019 4:00:05 PM 208.9 23.8
6/7/2019 4:00:06 PM 208.5 23.4
6/7/2019 4:00:07 PM 208.1 23.0
6/7/2019 4:00:08 PM 207.7 22.6
6/7/2019 4:00:09 PM 207.3 22.2
6/7/2019 4:00:10 PM 206.9 21.8
6/7/2019 4:00:11 PM 206.5 21.4
6/7/2019 4:00:12 PM 206.0 20.9
6/7/2019 4:00:13 PM 205.6 20.5
6/7/2019 4:00:14 PM 205.1 20.0
6/7/2019 4:00:15 PM 204.7 19.6
6/7/2019 4:00:16 PM 204.3 19.2
6/7/2019 4:00:17 PM 203.9 18.8
6/7/2019 4:00:18 PM 203.5 18.4
6/7/2019 4:00:19 PM 203.2 18.1
6/7/2019 4:00:20 PM 202.9 17.8
6/7/2019 4:00:21 PM 202.7 17.6
6/7/2019 4:00:22 PM 202.5 17.4
6/7/2019 4:00:23 PM 202.3 17.2
6/7/2019 4:00:24 PM 202.1 17.0
6/7/2019 4:00:25 PM 201.9 16.8
6/7/2019 4:00:26 PM 201.8 16.7
6/7/2019 4:00:27 PM 201.6 16.5
6/7/2019 4:00:28 PM 201.6 16.5
6/7/2019 4:00:29 PM 201.5 16.4
6/7/2019 4:00:30 PM 201.4 16.3
6/7/2019 4:00:31 PM 201.3 16.2
6/7/2019 4:00:32 PM 201.3 16.2
6/7/2019 4:00:33 PM 201.2 16.1
6/7/2019 4:00:34 PM 201.1 16.0
6/7/2019 4:00:35 PM 201.0 15.9
6/7/2019 4:00:36 PM 200.9 15.8
6/7/2019 4:00:37 PM 200.9 15.8
6/7/2019 4:00:38 PM 200.8 15.7
6/7/2019 4:00:39 PM 200.7 15.6
6/7/2019 4:00:40 PM 200.6 15.5
6/7/2019 4:00:41 PM 200.5 15.4
6/7/2019 4:00:42 PM 200.3 15.2
6/7/2019 4:00:43 PM 200.1 15.0
6/7/2019 4:00:44 PM 199.9 14.8
6/7/2019 4:00:45 PM 199.8 14.7
6/7/2019 4:00:46 PM 199.6 14.5
6/7/2019 4:00:47 PM 199.4 14.3
6/7/2019 4:00:48 PM 199.3 14.2
6/7/2019 4:00:49 PM 199.1 14.0
6/7/2019 4:00:50 PM 199.0 13.9
6/7/2019 4:00:51 PM 198.8 13.7
6/7/2019 4:00:52 PM 198.6 13.5
6/7/2019 4:00:53 PM 198.5 13.4
6/7/2019 4:00:54 PM 198.3 13.2
6/7/2019 4:00:55 PM 198.2 13.1
6/7/2019 4:00:56 PM 198.0 12.9
6/7/2019 4:00:57 PM 197.9 12.8
6/7/2019 4:00:58 PM 197.8 12.7
6/7/2019 4:00:59 PM 197.6 12.5
6/7/2019 4:01:00 PM 197.5 12.4
6/7/2019 4:01:01 PM 197.3 12.2
6/7/2019 4:01:02 PM 197.2 12.1
6/7/2019 4:01:03 PM 197.1 12.0
6/7/2019 4:01:04 PM 197.0 11.9
6/7/2019 4:01:05 PM 197.0 11.9
6/7/2019 4:01:06 PM 197.0 11.9
Page 440 of 452 August 2019
APPENDIX E60: SALT DILUTION GAUGING SUMMARY
SEEP-D1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-D1 TEST-4 Data Log
6/7/2019 4:01:07 PM 197.0 11.9
6/7/2019 4:01:08 PM 197.0 11.9
6/7/2019 4:01:09 PM 197.0 11.9
6/7/2019 4:01:10 PM 197.1 12.0
6/7/2019 4:01:11 PM 197.3 12.2
6/7/2019 4:01:12 PM 197.4 12.3
6/7/2019 4:01:13 PM 197.6 12.5
6/7/2019 4:01:14 PM 197.7 12.6
6/7/2019 4:01:15 PM 197.9 12.8
6/7/2019 4:01:16 PM 198.0 12.9
6/7/2019 4:01:17 PM 198.1 13.0
6/7/2019 4:01:18 PM 198.2 13.1
6/7/2019 4:01:19 PM 198.3 13.2
6/7/2019 4:01:20 PM 198.3 13.2
6/7/2019 4:01:21 PM 198.3 13.2
6/7/2019 4:01:22 PM 198.2 13.1
6/7/2019 4:01:23 PM 198.1 13.0
6/7/2019 4:01:24 PM 198.0 12.9
6/7/2019 4:01:25 PM 197.8 12.7
6/7/2019 4:01:26 PM 197.6 12.5
6/7/2019 4:01:27 PM 197.4 12.3
6/7/2019 4:01:28 PM 197.2 12.1
6/7/2019 4:01:29 PM 196.9 11.8
6/7/2019 4:01:30 PM 196.7 11.6
6/7/2019 4:01:31 PM 196.5 11.4
6/7/2019 4:01:32 PM 196.3 11.2
6/7/2019 4:01:33 PM 196.0 10.9
6/7/2019 4:01:34 PM 195.9 10.8
6/7/2019 4:01:35 PM 195.6 10.5
6/7/2019 4:01:36 PM 195.4 10.3
6/7/2019 4:01:37 PM 195.3 10.2
6/7/2019 4:01:38 PM 195.1 10.0
6/7/2019 4:01:39 PM 194.9 9.8
6/7/2019 4:01:40 PM 194.7 9.6
6/7/2019 4:01:41 PM 194.6 9.5
6/7/2019 4:01:42 PM 194.4 9.3
6/7/2019 4:01:43 PM 194.3 9.2
6/7/2019 4:01:44 PM 194.1 9.0
6/7/2019 4:01:45 PM 194.0 8.9
6/7/2019 4:01:46 PM 193.9 8.8
6/7/2019 4:01:47 PM 193.7 8.6
6/7/2019 4:01:48 PM 193.6 8.5
6/7/2019 4:01:49 PM 193.5 8.4
6/7/2019 4:01:50 PM 193.4 8.3
6/7/2019 4:01:51 PM 193.3 8.2
6/7/2019 4:01:52 PM 193.2 8.1
6/7/2019 4:01:53 PM 193.0 7.9
6/7/2019 4:01:54 PM 192.9 7.8
6/7/2019 4:01:55 PM 192.8 7.7
6/7/2019 4:01:56 PM 192.7 7.6
6/7/2019 4:01:57 PM 192.6 7.5
6/7/2019 4:01:58 PM 192.5 7.4
6/7/2019 4:01:59 PM 192.4 7.3
6/7/2019 4:02:00 PM 192.3 7.2
6/7/2019 4:02:01 PM 192.3 7.2
6/7/2019 4:02:02 PM 192.2 7.1
6/7/2019 4:02:03 PM 192.1 7.0
6/7/2019 4:02:04 PM 192.0 6.9
6/7/2019 4:02:05 PM 191.9 6.8
6/7/2019 4:02:06 PM 191.8 6.7
6/7/2019 4:02:07 PM 191.7 6.6
6/7/2019 4:02:08 PM 191.6 6.5
6/7/2019 4:02:09 PM 191.5 6.4
6/7/2019 4:02:10 PM 191.3 6.2
6/7/2019 4:02:11 PM 191.2 6.1
6/7/2019 4:02:12 PM 191.1 6.0
6/7/2019 4:02:13 PM 191.0 5.9
6/7/2019 4:02:14 PM 190.9 5.8
6/7/2019 4:02:15 PM 190.8 5.7
6/7/2019 4:02:16 PM 190.7 5.6
6/7/2019 4:02:17 PM 190.6 5.5
6/7/2019 4:02:18 PM 190.5 5.4
6/7/2019 4:02:19 PM 190.4 5.3
6/7/2019 4:02:20 PM 190.3 5.2
6/7/2019 4:02:21 PM 190.3 5.2
6/7/2019 4:02:22 PM 190.2 5.1
6/7/2019 4:02:23 PM 190.2 5.1
6/7/2019 4:02:24 PM 190.1 5.0
6/7/2019 4:02:25 PM 190.1 5.0
Page 441 of 452 August 2019
APPENDIX E60: SALT DILUTION GAUGING SUMMARY
SEEP-D1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 SEEP-D1 TEST-4 Data Log
6/7/2019 4:02:26 PM 190.0 4.9
6/7/2019 4:02:27 PM 189.9 4.8
6/7/2019 4:02:28 PM 189.9 4.8
6/7/2019 4:02:29 PM 189.8 4.7
6/7/2019 4:02:30 PM 189.8 4.7
6/7/2019 4:02:31 PM 189.8 4.7
6/7/2019 4:02:32 PM 189.7 4.6
6/7/2019 4:02:33 PM 189.7 4.6
6/7/2019 4:02:34 PM 189.6 4.5
6/7/2019 4:02:35 PM 189.6 4.5
6/7/2019 4:02:36 PM 189.6 4.5
6/7/2019 4:02:37 PM 189.6 4.5
6/7/2019 4:02:38 PM 189.5 4.4
6/7/2019 4:02:39 PM 189.5 4.4
6/7/2019 4:02:40 PM 189.5 4.4
6/7/2019 4:02:41 PM 189.4 4.3
6/7/2019 4:02:42 PM 189.4 4.3
6/7/2019 4:02:43 PM 189.3 4.2
6/7/2019 4:02:44 PM 189.3 4.2
6/7/2019 4:02:45 PM 189.3 4.2
6/7/2019 4:02:46 PM 189.2 4.1
6/7/2019 4:02:47 PM 189.2 4.1
6/7/2019 4:02:48 PM 189.1 4.0
6/7/2019 4:02:49 PM 189.1 4.0
6/7/2019 4:02:50 PM 189.1 4.0
6/7/2019 4:02:51 PM 189.1 4.0
6/7/2019 4:02:52 PM 189.1 4.0
6/7/2019 4:02:53 PM 189.1 4.0
6/7/2019 4:02:54 PM 189.1 4.0
6/7/2019 4:02:55 PM 189.1 4.0
Page 442 of 452 August 2019
APPENDIX E60: SALT DILUTION GAUGING SUMMARY
SEEP-D1 TEST-4 JUNE
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
SEEP-D1 TEST-4 1520
SEEP-D1 TEST-4 1521
SEEP-D1 TEST-4 1522
SEEP-D1 TEST-4 1524
Location EC Reading
(µS/cms)
SEEP-D1 TEST-4 1,130
SEEP-D1 TEST-4 2,147
SEEP-D1 TEST-4 17,118
SEEP-D1 TEST-4 135,213
q 300,900
K 1.3558
3.1
49.7
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)
(µS/cms)
(µS/cms)
27.1
27.2
27.1
(µS/cms)(°C)
Table E2 SEEP-D1 TEST-4 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
182.9 19.6
184.1 19.4
185.2 19.1
Calibration Temperature
185.2 19.4
Average 184.4 (µS/cms)
Geometric Mean 184.3
Average (pre-test)185.1
Average (post-test)190.7
Table E3 SEEP-D1 TEST-4 YSI Salt Dilution Calibration Data
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)130,394.1 (s) . (µS/cms)
(mg/L)(°C)
100
1,000
10,000
100,000 27.0
Table E4 SEEP-D1 TEST-4 Flow Calculation Summary
Mass of Salt injected mg
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Slope of Calibration Curve (µS/cms) / (mg/L)
Calculated Flow Rate Q
L/s
GPM
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ
಼
Page 443 of 452 August 2019
APPENDIX E61: SALT DILUTION GAUGING SUMMARY
WC-1 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/7/2019 10:10:03 AM 90.9 -
2/7/2019 10:10:04 AM 90.9 -
2/7/2019 10:10:05 AM 90.9 -
2/7/2019 10:10:06 AM 90.9 -
2/7/2019 10:10:07 AM 90.9 -
2/7/2019 10:10:08 AM 90.9 -
2/7/2019 10:10:09 AM 90.8 -
2/7/2019 10:10:10 AM 90.8 -
2/7/2019 10:10:11 AM 90.8 -
2/7/2019 10:10:12 AM 90.9 -
2/7/2019 10:10:13 AM 91.0 -
2/7/2019 10:10:14 AM 91.0 -
2/7/2019 10:10:15 AM 91.0 -
2/7/2019 10:10:16 AM 91.0 -
2/7/2019 10:10:17 AM 91.0 -
2/7/2019 10:10:18 AM 91.0 -
2/7/2019 10:10:19 AM 91.0 -
2/7/2019 10:10:20 AM 91.0 -
2/7/2019 10:10:21 AM 91.0 -
2/7/2019 10:10:22 AM 91.0 -
2/7/2019 10:10:23 AM 91.0 -
2/7/2019 10:10:24 AM 91.0 -
2/7/2019 10:10:25 AM 91.0 -
2/7/2019 10:10:26 AM 90.9 -
2/7/2019 10:10:27 AM 90.8 -
2/7/2019 10:10:28 AM 90.8 -
2/7/2019 10:10:29 AM 90.8 -
2/7/2019 10:10:30 AM 90.8 -
2/7/2019 10:10:31 AM 90.8 -
2/7/2019 10:10:32 AM 90.9 -
2/7/2019 10:10:33 AM 90.9 -
2/7/2019 10:10:34 AM 90.9 -
2/7/2019 10:10:35 AM 90.9 -
2/7/2019 10:10:36 AM 90.9 -
2/7/2019 10:10:37 AM 90.8 -
2/7/2019 10:10:38 AM 90.8 -
2/7/2019 10:10:39 AM 90.9 -
2/7/2019 10:10:40 AM 90.9 -
2/7/2019 10:10:41 AM 91.0 0.1
2/7/2019 10:10:42 AM 91.1 0.2
2/7/2019 10:10:43 AM 91.2 0.3
2/7/2019 10:10:44 AM 91.5 0.6
2/7/2019 10:10:45 AM 92.3 1.4
2/7/2019 10:10:46 AM 93.8 2.9
2/7/2019 10:10:47 AM 96.6 5.7
2/7/2019 10:10:48 AM 99.3 8.4
2/7/2019 10:10:49 AM 152.4 61.5
2/7/2019 10:10:50 AM 153.8 62.9
2/7/2019 10:10:51 AM 158.9 68.0
2/7/2019 10:10:52 AM 159.9 69.0
2/7/2019 10:10:53 AM 161.1 70.2
2/7/2019 10:10:54 AM 162.0 71.1
2/7/2019 10:10:55 AM 162.6 71.7
2/7/2019 10:10:56 AM 162.8 71.9
2/7/2019 10:10:57 AM 162.8 71.9
2/7/2019 10:10:58 AM 162.5 71.6
2/7/2019 10:10:59 AM 162.2 71.3
2/7/2019 10:11:00 AM 162.0 71.1
2/7/2019 10:11:01 AM 161.7 70.8
2/7/2019 10:11:02 AM 161.5 70.6
2/7/2019 10:11:03 AM 161.1 70.2
2/7/2019 10:11:04 AM 160.7 69.8
2/7/2019 10:11:05 AM 159.8 68.9
2/7/2019 10:11:06 AM 158.9 68.0
2/7/2019 10:11:07 AM 157.5 66.6
2/7/2019 10:11:08 AM 156.0 65.1
2/7/2019 10:11:09 AM 154.8 63.9
2/7/2019 10:11:10 AM 153.3 62.4
2/7/2019 10:11:11 AM 151.3 60.4
2/7/2019 10:11:12 AM 148.8 57.9
Table E1 WC-1 TEST-2 Data Log
Page 444 of 452 August 2019
APPENDIX E61: SALT DILUTION GAUGING SUMMARY
WC-1 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 WC-1 TEST-2 Data Log
2/7/2019 10:11:13 AM 146.3 55.4
2/7/2019 10:11:14 AM 143.9 53.0
2/7/2019 10:11:15 AM 141.6 50.7
2/7/2019 10:11:16 AM 138.6 47.7
2/7/2019 10:11:17 AM 135.3 44.4
2/7/2019 10:11:18 AM 131.9 41.0
2/7/2019 10:11:19 AM 129.1 38.2
2/7/2019 10:11:20 AM 126.6 35.7
2/7/2019 10:11:21 AM 123.8 32.9
2/7/2019 10:11:22 AM 121.8 30.9
2/7/2019 10:11:23 AM 119.5 28.6
2/7/2019 10:11:24 AM 116.9 26.0
2/7/2019 10:11:25 AM 114.2 23.3
2/7/2019 10:11:26 AM 112.2 21.3
2/7/2019 10:11:27 AM 110.4 19.5
2/7/2019 10:11:28 AM 109.3 18.4
2/7/2019 10:11:29 AM 108.2 17.3
2/7/2019 10:11:30 AM 106.8 15.9
2/7/2019 10:11:31 AM 105.2 14.3
2/7/2019 10:11:32 AM 103.9 13.0
2/7/2019 10:11:33 AM 102.9 12.0
2/7/2019 10:11:34 AM 101.8 10.9
2/7/2019 10:11:35 AM 101.1 10.2
2/7/2019 10:11:36 AM 100.1 9.2
2/7/2019 10:11:37 AM 99.1 8.2
2/7/2019 10:11:38 AM 98.5 7.6
2/7/2019 10:11:39 AM 98.0 7.1
2/7/2019 10:11:40 AM 97.4 6.5
2/7/2019 10:11:41 AM 97.0 6.1
2/7/2019 10:11:42 AM 96.5 5.6
2/7/2019 10:11:43 AM 96.1 5.2
2/7/2019 10:11:44 AM 95.6 4.7
2/7/2019 10:11:45 AM 95.4 4.5
2/7/2019 10:11:46 AM 95.0 4.1
2/7/2019 10:11:47 AM 94.8 3.9
2/7/2019 10:11:48 AM 94.4 3.5
2/7/2019 10:11:49 AM 94.2 3.3
2/7/2019 10:11:50 AM 93.8 2.9
2/7/2019 10:11:51 AM 93.5 2.6
2/7/2019 10:11:52 AM 93.2 2.3
2/7/2019 10:11:53 AM 93.1 2.2
2/7/2019 10:11:54 AM 92.9 2.0
2/7/2019 10:11:55 AM 92.7 1.8
2/7/2019 10:11:56 AM 92.5 1.6
2/7/2019 10:11:57 AM 92.4 1.5
2/7/2019 10:11:58 AM 92.3 1.4
2/7/2019 10:11:59 AM 92.2 1.3
2/7/2019 10:12:00 AM 92.0 1.1
2/7/2019 10:12:01 AM 91.9 1.0
2/7/2019 10:12:02 AM 91.8 0.9
2/7/2019 10:12:03 AM 91.8 0.9
2/7/2019 10:12:04 AM 91.8 0.9
2/7/2019 10:12:05 AM 91.8 0.9
2/7/2019 10:12:06 AM 91.8 0.9
2/7/2019 10:12:07 AM 91.8 0.9
2/7/2019 10:12:08 AM 91.8 0.9
2/7/2019 10:12:09 AM 91.8 0.9
2/7/2019 10:12:10 AM 91.8 0.9
2/7/2019 10:12:11 AM 91.8 0.9
2/7/2019 10:12:12 AM 91.8 0.9
2/7/2019 10:12:13 AM 91.8 0.9
2/7/2019 10:12:14 AM 91.7 0.8
2/7/2019 10:12:15 AM 91.7 0.8
2/7/2019 10:12:16 AM 91.7 0.8
2/7/2019 10:12:17 AM 91.7 0.8
2/7/2019 10:12:18 AM 91.7 0.8
2/7/2019 10:12:19 AM 91.6 0.7
2/7/2019 10:12:20 AM 91.6 0.7
2/7/2019 10:12:21 AM 91.6 0.7
2/7/2019 10:12:22 AM 91.5 0.6
2/7/2019 10:12:23 AM 91.5 0.6
2/7/2019 10:12:24 AM 91.5 0.6
2/7/2019 10:12:25 AM 91.5 0.6
2/7/2019 10:12:26 AM 91.5 0.6
2/7/2019 10:12:27 AM 91.5 0.6
2/7/2019 10:12:28 AM 91.5 0.6
2/7/2019 10:12:29 AM 91.5 0.6
2/7/2019 10:12:30 AM 91.5 0.6
Page 445 of 452 August 2019
APPENDIX E61: SALT DILUTION GAUGING SUMMARY
WC-1 TEST-2 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
WC-1 TEST-2 921
WC-1 TEST-2 923
WC-1 TEST-2 925
WC-1 TEST-2 929
Location EC Reading
(µS/cms)
WC-1 TEST-2 145.8
WC-1 TEST-2 196
WC-1 TEST-2 1,554
WC-1 TEST-2 12,382
WC-1 TEST-2 99,950
q 449,500
K 1.0019
185.4
2,942.3
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms) (°C)
Table E2 WC-1 TEST-2 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
Geometric Mean 73.4 (µS/cms)
89.9 13.8
90.2 13.6
59.9 13.6
59.9 13.6
Average 75.0 (µS/cms)
10 20.3
Average (pre-test) 90.6 (µS/cms)
Average (post-test) 90.5 (µS/cms)
Table E3 WC-1 TEST-2 YSI Salt Dilution Calibration Data
Calibration
Concentration Temperature
(mg/L)(°C)
Slope of Calibration Curve (µS/cms) / (mg/L)
100 20.9
1,000 20.9
10,000 21.1
100,000 21
Table E4 WC-1 TEST-2 Flow Calculation Summary
Mass of Salt injected mg
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline,
Watershed Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)2,429.6 (s) . (µS/cms)
Calculated Flow Rate Q
L/s
GPM
Qൌ ௤
∑ಶ಴೟షಶ಴್೒ ∗∆೟೙೔సభ಼
Page 446 of 452 August 2019
APPENDIX E62: SALT DILUTION GAUGING SUMMARY
WC-1 TEST-3 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/7/2019 10:21:34 AM 90.7 -
2/7/2019 10:21:35 AM 90.7 -
2/7/2019 10:21:36 AM 90.7 -
2/7/2019 10:21:37 AM 90.7 -
2/7/2019 10:21:38 AM 90.7 -
2/7/2019 10:21:39 AM 90.7 -
2/7/2019 10:21:40 AM 90.7 -
2/7/2019 10:21:41 AM 90.7 -
2/7/2019 10:21:42 AM 90.7 -
2/7/2019 10:21:43 AM 90.7 -
2/7/2019 10:21:44 AM 90.7 -
2/7/2019 10:21:45 AM 90.7 -
2/7/2019 10:21:46 AM 90.7 -
2/7/2019 10:21:47 AM 90.7 -
2/7/2019 10:21:48 AM 90.6 -
2/7/2019 10:21:49 AM 90.6 -
2/7/2019 10:21:50 AM 90.6 -
2/7/2019 10:21:51 AM 90.6 -
2/7/2019 10:21:52 AM 90.6 -
2/7/2019 10:21:53 AM 90.6 -
2/7/2019 10:21:54 AM 90.6 -
2/7/2019 10:21:55 AM 90.6 -
2/7/2019 10:21:56 AM 90.6 -
2/7/2019 10:21:57 AM 90.6 -
2/7/2019 10:21:58 AM 90.6 -
2/7/2019 10:21:59 AM 90.6 -
2/7/2019 10:22:00 AM 90.6 -
2/7/2019 10:22:01 AM 90.6 -
2/7/2019 10:22:02 AM 90.5 -
2/7/2019 10:22:03 AM 90.5 -
2/7/2019 10:22:04 AM 90.5 -
2/7/2019 10:22:05 AM 90.5 -
2/7/2019 10:22:06 AM 90.5 -
2/7/2019 10:22:07 AM 90.5 -
2/7/2019 10:22:08 AM 90.5 -
2/7/2019 10:22:09 AM 90.5 -
2/7/2019 10:22:10 AM 90.5 -
2/7/2019 10:22:11 AM 90.6 -
2/7/2019 10:22:12 AM 90.6 -
2/7/2019 10:22:13 AM 90.8 -
2/7/2019 10:22:14 AM 91.1 0.5
2/7/2019 10:22:15 AM 91.6 1.0
2/7/2019 10:22:16 AM 93.3 2.7
2/7/2019 10:22:17 AM 95.9 5.3
2/7/2019 10:22:18 AM 99.1 8.5
2/7/2019 10:22:19 AM 102.3 11.7
2/7/2019 10:22:20 AM 106.1 15.5
2/7/2019 10:22:21 AM 109.9 19.3
2/7/2019 10:22:22 AM 158.8 68.2
2/7/2019 10:22:23 AM 161.8 71.2
2/7/2019 10:22:24 AM 175.2 84.6
2/7/2019 10:22:25 AM 178.0 87.4
2/7/2019 10:22:26 AM 180.2 89.6
2/7/2019 10:22:27 AM 181.1 90.5
2/7/2019 10:22:28 AM 181.9 91.3
2/7/2019 10:22:29 AM 182.7 92.1
2/7/2019 10:22:30 AM 184.0 93.4
2/7/2019 10:22:31 AM 185.2 94.6
2/7/2019 10:22:32 AM 186.1 95.5
2/7/2019 10:22:33 AM 186.1 95.5
2/7/2019 10:22:34 AM 185.0 94.4
2/7/2019 10:22:35 AM 183.9 93.3
2/7/2019 10:22:36 AM 182.8 92.2
2/7/2019 10:22:37 AM 181.9 91.3
2/7/2019 10:22:38 AM 181.2 90.6
2/7/2019 10:22:39 AM 180.4 89.8
2/7/2019 10:22:40 AM 179.2 88.6
2/7/2019 10:22:41 AM 178.0 87.4
2/7/2019 10:22:42 AM 176.5 85.9
2/7/2019 10:22:43 AM 174.8 84.2
Table E1 WC-1 TEST-3 Data Log
Page 447 of 452 August 2019
APPENDIX E62: SALT DILUTION GAUGING SUMMARY
WC-1 TEST-3 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 WC-1 TEST-3 Data Log
2/7/2019 10:22:44 AM 172.1 81.5
2/7/2019 10:22:45 AM 168.3 77.7
2/7/2019 10:22:46 AM 165.1 74.5
2/7/2019 10:22:47 AM 162.2 71.6
2/7/2019 10:22:48 AM 159.9 69.3
2/7/2019 10:22:49 AM 157.1 66.5
2/7/2019 10:22:50 AM 154.6 64.0
2/7/2019 10:22:51 AM 151.3 60.7
2/7/2019 10:22:52 AM 148.8 58.2
2/7/2019 10:22:53 AM 145.9 55.3
2/7/2019 10:22:54 AM 142.7 52.1
2/7/2019 10:22:55 AM 138.7 48.1
2/7/2019 10:22:56 AM 135.3 44.7
2/7/2019 10:22:57 AM 132.0 41.4
2/7/2019 10:22:58 AM 129.6 39.0
2/7/2019 10:22:59 AM 126.9 36.3
2/7/2019 10:23:00 AM 124.2 33.6
2/7/2019 10:23:01 AM 121.1 30.5
2/7/2019 10:23:02 AM 118.4 27.8
2/7/2019 10:23:03 AM 115.5 24.9
2/7/2019 10:23:04 AM 113.1 22.5
2/7/2019 10:23:05 AM 110.3 19.7
2/7/2019 10:23:06 AM 108.0 17.4
2/7/2019 10:23:07 AM 106.1 15.5
2/7/2019 10:23:08 AM 104.7 14.1
2/7/2019 10:23:09 AM 103.1 12.5
2/7/2019 10:23:10 AM 102.0 11.4
2/7/2019 10:23:11 AM 100.9 10.3
2/7/2019 10:23:12 AM 100.1 9.5
2/7/2019 10:23:13 AM 99.3 8.7
2/7/2019 10:23:14 AM 98.7 8.1
2/7/2019 10:23:15 AM 98.2 7.6
2/7/2019 10:23:16 AM 97.7 7.1
2/7/2019 10:23:17 AM 97.2 6.6
2/7/2019 10:23:18 AM 96.7 6.1
2/7/2019 10:23:19 AM 96.2 5.6
2/7/2019 10:23:20 AM 95.8 5.2
2/7/2019 10:23:21 AM 95.3 4.7
2/7/2019 10:23:22 AM 94.8 4.2
2/7/2019 10:23:23 AM 94.3 3.7
2/7/2019 10:23:24 AM 93.8 3.2
2/7/2019 10:23:25 AM 93.4 2.8
2/7/2019 10:23:26 AM 93.2 2.6
2/7/2019 10:23:27 AM 93.0 2.4
2/7/2019 10:23:28 AM 92.8 2.2
2/7/2019 10:23:29 AM 92.5 1.9
2/7/2019 10:23:30 AM 92.3 1.7
2/7/2019 10:23:31 AM 92.2 1.6
2/7/2019 10:23:32 AM 92.0 1.4
2/7/2019 10:23:33 AM 91.9 1.3
2/7/2019 10:23:34 AM 91.8 1.2
2/7/2019 10:23:35 AM 91.6 1.0
2/7/2019 10:23:36 AM 91.6 1.0
2/7/2019 10:23:37 AM 91.5 0.9
2/7/2019 10:23:38 AM 91.4 0.8
2/7/2019 10:23:39 AM 91.4 0.8
2/7/2019 10:23:40 AM 91.3 0.7
2/7/2019 10:23:41 AM 91.2 0.6
2/7/2019 10:23:42 AM 91.2 0.6
2/7/2019 10:23:43 AM 91.1 0.5
2/7/2019 10:23:44 AM 91.0 0.4
2/7/2019 10:23:45 AM 91.0 0.4
2/7/2019 10:23:46 AM 90.9 0.3
2/7/2019 10:23:47 AM 90.9 0.3
2/7/2019 10:23:48 AM 90.9 0.3
2/7/2019 10:23:49 AM 90.9 0.3
2/7/2019 10:23:50 AM 90.9 0.3
2/7/2019 10:23:51 AM 90.9 0.3
2/7/2019 10:23:52 AM 90.9 0.3
2/7/2019 10:23:53 AM 90.9 0.3
2/7/2019 10:23:54 AM 90.9 0.3
2/7/2019 10:23:55 AM 90.9 0.3
2/7/2019 10:23:56 AM 90.9 0.3
2/7/2019 10:23:57 AM 90.9 0.3
2/7/2019 10:23:58 AM 90.9 0.3
2/7/2019 10:23:59 AM 90.9 0.3
2/7/2019 10:24:00 AM 90.8 0.2
Page 448 of 452 August 2019
APPENDIX E62: SALT DILUTION GAUGING SUMMARY
WC-1 TEST-3 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
Table E1 WC-1 TEST-3 Data Log
2/7/2019 10:24:01 AM 90.8 0.2
2/7/2019 10:24:02 AM 90.8 0.2
2/7/2019 10:24:03 AM 90.8 0.2
2/7/2019 10:24:04 AM 90.8 0.2
2/7/2019 10:24:05 AM 90.7 -
2/7/2019 10:24:06 AM 90.7 -
2/7/2019 10:24:07 AM 90.7 -
2/7/2019 10:24:08 AM 90.6 -
2/7/2019 10:24:09 AM 90.6 -
2/7/2019 10:24:10 AM 90.6 -
2/7/2019 10:24:11 AM 90.6 -
2/7/2019 10:24:12 AM 90.5 -
2/7/2019 10:24:13 AM 90.5 -
2/7/2019 10:24:14 AM 90.5 -
2/7/2019 10:24:15 AM 90.5 -
2/7/2019 10:24:16 AM 90.5 -
2/7/2019 10:24:17 AM 90.5 -
2/7/2019 10:24:18 AM 90.5 -
2/7/2019 10:24:19 AM 90.5 -
2/7/2019 10:24:20 AM 90.5 -
2/7/2019 10:24:21 AM 90.5 -
2/7/2019 10:24:22 AM 90.5 -
2/7/2019 10:24:23 AM 90.5 -
2/7/2019 10:24:24 AM 90.5 -
2/7/2019 10:24:25 AM 90.5 -
2/7/2019 10:24:26 AM 90.5 -
2/7/2019 10:24:27 AM 90.5 -
2/7/2019 10:24:28 AM 90.5 -
2/7/2019 10:24:29 AM 90.5 -
2/7/2019 10:24:30 AM 90.5 -
2/7/2019 10:24:31 AM 90.5 -
2/7/2019 10:24:32 AM 90.5 -
2/7/2019 10:24:33 AM 90.5 -
2/7/2019 10:24:34 AM 90.5 -
2/7/2019 10:24:35 AM 90.5 -
2/7/2019 10:24:36 AM 90.5 -
2/7/2019 10:24:37 AM 90.5 -
Page 449 of 452 August 2019
APPENDIX E62: SALT DILUTION GAUGING SUMMARY
WC-1 TEST-3 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
WC-1 TEST-3 921
WC-1 TEST-3 923
WC-1 TEST-3 925
WC-1 TEST-3 929
Location EC Reading
(µS/cms)
WC-1 TEST-3 145.8
WC-1 TEST-3 196
WC-1 TEST-3 1,554
WC-1 TEST-3 12,382
WC-1 TEST-3 99,950
q 600,600
K 1.0019
181.9
2,887.8
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
Table E2 WC-1 TEST-3 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
(µS/cms)(°C)
89.9 13.8
90.2 13.6
59.9 13.6
59.9 13.6
Average 75.0 (µS/cms)
Geometric Mean 73.4 (µS/cms)
Average (pre-test)90.6 (µS/cms)
Average (post-test)90.5 (µS/cms)
Table E3 WC-1 TEST-3 YSI Salt Dilution Calibration Data
Calibration
Concentration Temperature
(mg/L)(°C)
10 20.3
100 20.9
Integral of Conductivity
Data Curve
SUM:Δt(E
Ct-ECbkg)3,307.6 (s) . (µS/cms)
1,000 20.9
10,000 21.1
100,000 21.0
Table E4 WC-1 TEST-3 Flow Calculation Summary
Mass of Salt injected mg
Slope of Calibration Curve (µS/cms) / (mg/L)
Calculated Flow Rate Q
L/s
GPM
Moore, Dan. “Introduction to Salt Dilution Gauging for
Streamflow Measurement Part 2: Constant-Rate Injection.”
Streamline, Watershed Management Bulletin, vol. 8, no. 1, 2004,
pp. 11–15.
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Page 450 of 452 August 2019
APPENDIX E63: SALT DILUTION GAUGING SUMMARY
WC-5 TEST-3 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
Date Time
Conductivity
(µS/cms)Δt(ECt-ECbkg)
2/7/2019 2:25:56 PM 82.8 -
2/7/2019 2:25:57 PM 82.7 -
2/7/2019 2:25:58 PM 82.7 -
2/7/2019 2:25:59 PM 82.7 -
2/7/2019 2:26:00 PM 82.6 -
2/7/2019 2:26:01 PM 82.6 -
2/7/2019 2:26:02 PM 82.5 -
2/7/2019 2:26:03 PM 82.5 -
2/7/2019 2:26:04 PM 82.5 -
2/7/2019 2:26:05 PM 82.4 -
2/7/2019 2:26:06 PM 82.4 -
2/7/2019 2:26:07 PM 82.4 -
2/7/2019 2:26:08 PM 82.4 -
2/7/2019 2:26:09 PM 82.4 -
2/7/2019 2:26:10 PM 82.3 -
2/7/2019 2:26:11 PM 82.3 -
2/7/2019 2:26:12 PM 82.3 -
2/7/2019 2:26:13 PM 82.4 -
2/7/2019 2:26:14 PM 143.9 61.4
2/7/2019 2:26:15 PM 296.3 213.8
2/7/2019 2:26:16 PM 323.6 241.1
2/7/2019 2:26:17 PM 342.9 260.4
2/7/2019 2:26:18 PM 342.0 259.5
2/7/2019 2:26:19 PM 269.0 186.5
2/7/2019 2:26:20 PM 252.9 170.4
2/7/2019 2:26:21 PM 196.3 113.8
2/7/2019 2:26:22 PM 167.7 85.2
2/7/2019 2:26:23 PM 150.3 67.8
2/7/2019 2:26:24 PM 141.9 59.4
2/7/2019 2:26:25 PM 135.4 52.9
2/7/2019 2:26:26 PM 129.0 46.5
2/7/2019 2:26:27 PM 122.1 39.6
2/7/2019 2:26:28 PM 117.6 35.1
2/7/2019 2:26:29 PM 113.3 30.8
2/7/2019 2:26:30 PM 110.2 27.7
2/7/2019 2:26:31 PM 107.2 24.7
2/7/2019 2:26:32 PM 105.0 22.5
2/7/2019 2:26:33 PM 102.9 20.4
2/7/2019 2:26:34 PM 101.3 18.8
2/7/2019 2:26:35 PM 98.7 16.2
2/7/2019 2:26:36 PM 94.3 11.8
2/7/2019 2:26:37 PM 90.1 7.6
2/7/2019 2:26:38 PM 87.4 4.9
2/7/2019 2:26:39 PM 85.5 -
2/7/2019 2:26:40 PM 84.6 -
2/7/2019 2:26:41 PM 83.7 -
2/7/2019 2:26:42 PM 83.2 -
2/7/2019 2:26:43 PM 82.9 -
2/7/2019 2:26:44 PM 82.7 -
2/7/2019 2:26:45 PM 82.6 -
2/7/2019 2:26:46 PM 82.5 -
2/7/2019 2:26:47 PM 82.5 -
2/7/2019 2:26:48 PM 82.4 -
2/7/2019 2:26:49 PM 82.3 -
2/7/2019 2:26:50 PM 82.3 -
2/7/2019 2:26:51 PM 82.2 -
2/7/2019 2:26:52 PM 82.2 -
2/7/2019 2:26:53 PM 82.2 -
2/7/2019 2:26:54 PM 82.2 -
2/7/2019 2:26:55 PM 82.2 -
Table E1 WC-5 TEST-3 Data Log
Page 451 of 452 August 2019
APPENDIX E63: SALT DILUTION GAUGING SUMMARY
WC-5 TEST-3 FEBRUARY
Chemours Fayettevile Works, North Carolina
Geosyntec Consultants of NC P.C.
WC-5 TEST-3 1346
WC-5 TEST-3 1347
WC-5 TEST-3 1348
WC-5 TEST-3 1349
Location EC Reading
(µS/cms)
WC-5 TEST-3 163.4
WC-5 TEST-3 186
WC-5 TEST-3 1,432
WC-5 TEST-3 11,787
WC-5 TEST-3 94,424
q 300,000
K 0.9466
136.6
2,168.3
Notes:
EC Electrical conductivity
°C degrees celsius
mg miligrams
L liter
µS/cms microSiemens per centimeter second
GPM gallons per minute
s second
Ect raw electronic conductivty during test
Ecbkg background electronic conductivity value
Δt time interval between conductivity readings (1 second)
Equation for flow calculation derived from:
(µS/cms)(°C)
81.6 16.2
Table E2 WC-5 TEST-3 Stream Background Conductivity Data
Location Time Background Stream EC
Background Stream
Temperature
81.2 16.2
82.0 16.2
81.9 16.3
Average 81.7 (µS/cms)
Geometric Mean 81.7 (µS/cms)
Average (pre-test)82.5 (µS/cms)
Average (post-test)82.8 (µS/cms)
Table E3 WC-5 TEST-3 YSI Salt Dilution Calibration Data
Calibration
Concentration Temperature
mg
(mg/L)(°C)
10 23.8
100 24.2
1,000 24.4
10,000 23.9
Table E4 WC-5 TEST-3 Flow Calculation Summary
100,000 24.3
Calculated Flow Rate Q
L/s
GPM
Mass of Salt injected
Moore, Dan. “Introduction to Salt Dilution Gauging for Streamflow
Measurement Part 2: Constant-Rate Injection.” Streamline, Watershed
Management Bulletin, vol. 8, no. 1, 2004, pp. 11–15.
Slope of Calibration Curve (µS/cms) / (mg/L)
Integral of Conductivity Data
Curve
SUM:Δt(E
Ct-ECbkg)2,078.9 (s) . (µS/cms)
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಼
Page 452 of 452 August 2019

APPENDIX F
Temporary Weir Installation Summary

TABLE F1TEMPORARY WEIR INSTALLATION SUMMARYChemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC P.C.Measurement Location Ha (ft) Hw (ft) H (ft) GPMWeir Plate 1Flow Estimate 2SEEP A-11.4 1.1 0.33045-degree V NotchGPM = 464.5 x H 2.5SEEP A-50.7 0.6 0.10.3622.5-degree V NotchGPM = 223.1 x H 2.5Graduated cylinder0.85GPMSEEP A-TR1-10.9 0.6 0.21245-degree V NotchGPM = 464.5 x H 2.5Graduated cylinder9.5GPMSEEP A-31.1 0.8 0.32545-degree V NotchGPM = 464.5 x H 2.5Graduated cylinder15GPMSEEP A-40.7 0.6 0.00.1045-degree V NotchGPM = 464.5 x H 2.5Graduated cylinder3.1GPMSEEP B-21.3 1.3 0.0N/S22.5-degree V NotchGPM = 223.1 x H 2.5Graduated cylinder2.6GPMSEEP B-TR21.0 0.9 0.10.3322.5-degree V NotchGPM = 464.5 x H 2.5Graduated cylinder4.0GPMSEEP C-11.0 0.7 0.42022.5-degree V NotchGPM = 223.1 x H 2.5Graduated cylinder6.5GPMSEEP D-11.4 1.1 0.21445-degree V Notch GPM = 464.5 x H 2.5Graduated cylinder32GPMOLD OUTFALL 0022.0 1.4 0.6700Cipolleti V NotchGPM = 1511 x H 1.5Flow Velocity Meter Measurement670GPMNotes: Ha = Water column height, upstream of weir plate.Hw = Weir plate notch height from downstream creek bed.H = Calculated thickness of water at notch of weir plate.GPM = Gallons per minute.N/S = Value not sufficient due to discrepancy in Hw measurement.1 - Weir plate was selected based on flow rate. 22.5-degree V Notch was used for low flow, 45-degree V notch for medium flow, and Cipolleti V notch for high flow.2 - Flow estimate was selected according to the weir plate used.Other flow measurements recordedHaHwHAugust 2019
APPENDIX G
Laboratory Reports & DVM Report
Note: Laboratory Reports provided separately
ADQM Data Review Narrative - FAY SURFACE WATER 0219.doc 1 of 3
ADQM DATA REVIEW NARRATIVE
Site Chemours FAY – Fayetteville Project SURFACE WATER 02/19 Project Reviewer Michael Aucoin, AECOM as a Chemours contractor Sampling Dates February 1-2 and 4-7, 2019 Analytical Protocol Laboratory Analytical Method Parameter(s)
Eurofins Lancaster (ELLE) 537 Modified PFAS1
TestAmerica - Sacramento Cl. Spec. Table 3 Compound SOP Table 3+ compounds
ELLE SW-846 8260C Volatiles
ELLE SW-846 8270D Semivolatiles
ELLE EPA 200.7 Rev. 4.4 Total Metals
ELLE EPA 300 Chloride, Nitrate, Nitrite, Sulfate
ELLE EPA 350.1 Ammonia
ELLE EPA 365.1 Phosphate
ELLE 2320 B-1997 Alkalinity
ELLE 2540 C-1997 TDS
ELLE 2540 D-1997 TSS
ELLE 5310 C-2000 TOC

1 Perfluoroalkylsubstances including HFPO-DA. Sample Receipt The following items are noted for this data set:
• All samples were received in satisfactory condition and within EPA temperature guidelines on February 2 and 5-8, 2019.
• Samples were submitted to Eurofins Lancaster and later transferred to TestAmerica Sacramento
for Table 3+ analysis. Data Review The electronic data submitted for this project was reviewed via the Data Verification Module (DVM) process. Overall the data is acceptable for use without qualification, except as noted below:
ADQM Data Review Narrative - FAY SURFACE WATER 0219.doc 2 of 3
• A non-detect result for 2-Chloroethyl Vinyl Ether in one field sample was qualified R and is considered to be unusable due to a very poor matrix spike recovery.
• PFO5DA and other parameter results in some field samples were qualified B and may be biased high, or may be false positives, due to a comparable concentration in the associated field blank.
• Table 3+ sample results were qualified J as estimated, and non-detect results were qualified UJ, and the reporting limit may be biased low, because the lab established holding time was exceeded.
• Several analytical results have been qualified J as estimated, and non-detect results qualified UJ indicating an estimated reporting limit, due to lab control sample, matrix spike or surrogate recovery outside criteria, and; poor lab replicate precision. Various non-pfas sample results reported between the MDL and PQL were qualified J as estimated. See the Data Verification
Module (DVM) Narrative Report for which samples were qualified, the specific reasons for qualification, and potential bias in reported results.
Attachments The DVM Narrative report is attached. The lab reports due to a large page count are stored on an AECOM network shared drive and are available to be posted on external shared drives, or on a flash drive.

ADQM Data Review Narrative - FAY SURFACE WATER 0219.doc 3 of 3
Data Verification Module (DVM)
The DVM is an internal review process used by the ADQM group to assist with the determination of data usability. The electronic data deliverables received from the laboratory are loaded into the Locus EIM™ database and processed through a series of data quality checks, which are a combination of software (Locus EIM™ database Data Verification Module (DVM)) and manual reviewer evaluations. The data is evaluated against the following data usability checks:
• Field and laboratory blank contamination
• US EPA hold time criteria
• Missing Quality Control (QC) samples
• Matrix spike(MS)/matrix spike duplicate (MSD) recoveries and the relative percent differences
(RPDs) between these spikes
• Laboratory control sample(LCS)/control sample duplicate (LCSD) recoveries and the RPD
between these spikes
• Surrogate spike recoveries for organic analyses
• RPD between field duplicate sample pairs
• RPD between laboratory replicates for inorganic analyses
• Difference / percent difference between total and dissolved sample pairs. There are two qualifier fields in EIM: Lab Qualifier is the qualifier assigned by the lab and may not reflect the usability of the data. This qualifier may have many different meanings and can vary between labs and over time within the same lab. Please refer to the laboratory report for a description of the lab qualifiers. As they are lab descriptors they are not to be used when evaluating the data. Validation Qualifier is the 3rd party formal validation qualifier if this was performed. Otherwise this field contains the qualifier resulting from the ADQM DVM review process. This qualifier assesses the usability of the data and may not equal the lab qualifier. The DVM applies the following data
evaluation qualifiers to analysis results, as warranted: Qualifier Definition B Not detected substantially above the level reported in the laboratory or field blanks. R Unusable result. Analyte may or may not be present in the sample.
J Analyte present. Reported value may not be accurate or precise.
UJ Not detected. Reporting limit may not be accurate or precise.

The Validation Status Code field is set to “DVM” if the ADQM DVM process has been performed. If the DVM has not been run, the field will be blank.
If the DVM has been run (Validation Status Code equals “DVM”), use the Validation Qualifier.
DVM Narrative ReportAssociated MS and/or MSD analysis had relative percent recovery (RPR) values less than the data rejection level. The reported non-detect result isunusable.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-4-02061902/06/2019 99817022-Chloroethyl VinylEther0.2 UG/L0.28260CR5030C10MDLPage 1 of 150
Contamination detected in Field Blank(s). Sample result does not differ significantly from the analyte concentration detected in the associated fieldblank(s).LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-4-02061902/06/2019 9981702Sulfate6.5 MG/L1.5300.0B5.0MDLFAY-SW-SEEP-B-4-02061902/06/2019 9981702Chloride10.8 MG/L1.0300.0B2.0MDLFAY-SW-SEEP-B-3-E4-02061902/06/2019 9981701Sulfate10.8 MG/L1.5300.0B5.0MDLFAY-SW-SEEP-B-3-E4-02061902/06/2019 9981701Chloride7.5 MG/L1.0300.0B2.0MDLFAY-SW-SEEP-B-3-A1-02061902/06/2019 9981698Chloride16.2 MG/L1.0300.0B2.0MDLFAY-SW-SEEP-B-3-02061902/06/2019 9981695Sulfate8.5 MG/L1.5300.0B5.0MDLFAY-SW-SEEP-B-3-A1-02061902/06/2019 9981698Sulfate18.6 MG/L1.5300.0B5.0MDLFAY-SW-SEEP-B-3-02061902/06/2019 9981695Chloride9.0 MG/L1.0300.0B2.0MDLFAY-SW-SEEP-B-4-A3-02061902/06/2019 9981703Chloride14.5 MG/L1.0300.0B2.0MDLFAY-SW-SEEP-B-4-A3-02061902/06/2019 9981703Sulfate5.2 MG/L1.5300.0B5.0MDLFAY-SW-OLDOF-1-02011902/01/2019 9978962PFO5DA0.67 ug/LCl. Spec. Table 3Compound SOPB0.10PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PFO5DA0.97 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.034PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PFO5DA0.86 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.034PQLFAY-SW-OLDOF-1-02011902/01/2019 9978952Ammonia0.60 MG/L0.050350.1B0.10MDLFAY-SW-OLDOF-2-02011902/01/2019 9978966PFO5DA0.82 ug/LCl. Spec. Table 3Compound SOPB0.10PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PFO5DA0.95 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.034PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PFO5DA1.0 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.034PQLFAY-SW-OLDOF-2-S-02011902/01/2019 9978954Chloride6.6 MG/L1.0300.0B2.0MDLFAY-SW-OLDOF-1-S-02011902/01/2019 9978951Chloride59100 MG/L4000300.0B8000MDLFAY-SW-OLDOF-2-02011902/01/2019 9978955Ammonia0.48 MG/L0.050350.1B0.10MDLPage 2 of 150
Contamination detected in Field Blank(s). Sample result does not differ significantly from the analyte concentration detected in the associated fieldblank(s).LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-4-02061902/06/2019 9981702Selenium0.0248 MG/L0.02106010BB3005A0.0500MDLPage 3 of 150
Only one surrogate has relative percent recovery (RPR) values outside control limits and the parameter is a PFC (Nondetects).LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-WC-1-020719 02/07/2019 9982641F-53B Major0.00085 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.00085PQLFAY-SW-WC-1-020719 02/07/2019 9982641F-53B Minor0.0017 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0017PQLFAY-SW-WC-1-020719 02/07/2019 9982641ADONA0.00085 UG/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.00085PQLFAY-SW-WC-3-020719 02/07/2019 9982649F-53B Major0.00086 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.00086PQLFAY-SW-WC-3-020719 02/07/2019 9982649F-53B Minor0.0017 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0017PQLFAY-SW-WC-3-020719 02/07/2019 9982649ADONA0.00086 UG/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.00086PQLFAY-SW-OLDOF-1-02011902/01/2019 9978959F-53B Major0.00086 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.00086PQLFAY-SW-OLDOF-1-02011902/01/2019 9978959F-53B Minor0.0017 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0017PQLFAY-SW-OLDOF-1-02011902/01/2019 9978959ADONA0.00086 UG/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.00086PQLFAY-SW-CFR-RM-76-02021902/04/2019 9979948F-53B Major0.00087 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.00087PQLFAY-SW-CFR-RM-76-02021902/04/2019 9979948F-53B Minor0.0017 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0017PQLFAY-SW-CFR-RM-76-02021902/04/2019 9979948ADONA0.00087 UG/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.00087PQLFAY-SW-SEEP-A-1-02071902/07/2019 9982593F-53B Major0.00085 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.00085PQLFAY-SW-SEEP-A-1-02071902/07/2019 9982593F-53B Minor0.0017 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0017PQLFAY-SW-SEEP-A-1-02071902/07/2019 9982593ADONA0.00085 UG/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.00085PQLFAY-SW-SEEP-A-3-02071902/07/2019 9982601F-53B Minor0.0018 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0018PQLFAY-SW-SEEP-A-3-02071902/07/2019 9982601ADONA0.0009 UG/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0009PQLFAY-SW-SEEP-A-3-02071902/07/2019 9982601F-53B Major0.0009 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0009PQLPage 4 of 150
Associated LCS and/or LCSD analysis had relative percent recovery (RPR) values less than the lower control limit but above 10%. The actual detectionlimits may be higher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFB-02061902/06/2019 9981760Hfpo Dimer Acid0.0018 UG/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0018PQLFB-02071902/07/2019 99826611H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)0.0027 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0027PQLFB-S-02051902/05/2019 9980837Hfpo Dimer Acid0.0018 UG/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0018PQLPage 5 of 150
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit. The actual detection limits may behigher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-C-1-02051902/05/2019 9980788Butyl Benzyl Phthalate2 UG/L28270DUJ3510C5MDLFAY-SW-SEEP-C-1-02051902/05/2019 99807882,4-Dimethylphenol3 UG/L38270DUJ3510C10MDLFAY-SW-SEEP-C-1-02051902/05/2019 9980788Alkalinity, Total1.7 MG/L1.72320 B-1997UJ5MDLFAY-SW-SEEP-B-1-02051902/05/2019 9980784Alkalinity, Total1.7 MG/L1.72320 B-1997UJ5MDLFB-02041902/04/2019 9979907Chloride0.20 MG/L0.20300.0UJ0.40MDLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 N-ethylperfluoro-1-octanesulfonamide0.19 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.19PQLFAY-SW-SEEP-A-2-02071902/07/2019 9982570Nitrate0.25 MG/L0.25300.0UJ0.50MDLFAY-SW-SEEP-A-3-02071902/07/2019 9982571Nitrate0.25 MG/L0.25300.0UJ0.50MDLFAY-SW-SEEP-A-4-02071902/07/2019 9982572Nitrate0.25 MG/L0.25300.0UJ0.50MDLFAY-SW-SEEP-A-5-02071902/07/2019 9982573Nitrate0.25 MG/L0.25300.0UJ0.50MDLFAY-SW-SEEP-A-6-02071902/07/2019 9982574Nitrate0.25 MG/L0.25300.0UJ0.50MDLFAY-SW-SEEP-A-7-02071902/07/2019 9982575Nitrate0.25 MG/L0.25300.0UJ0.50MDLFAY-SW-SEEP-A-8-02071902/07/2019 9982576Nitrate0.25 MG/L0.25300.0UJ0.50MDLPage 6 of 150
One or more surrogates had relative percent recovery (RPR) values less than the data rejection level. The reporting limit is consid-ered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-WC-1-020719 02/07/2019 99826412-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0026 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0026PQLFAY-SW-WC-1-020719 02/07/2019 99826412-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0026 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0026PQLFAY-SW-WC-1-020719 02/07/2019 9982641N-methyl perfluoro-1-octanesulfonamide0.0077 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0077PQLFAY-SW-WC-1-020719 02/07/2019 9982641N-ethylperfluoro-1-octanesulfonamide0.0077 UG/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0077PQLFAY-SW-WC-3-020719 02/07/2019 99826492-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0026 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0026PQLFAY-SW-WC-3-020719 02/07/2019 99826492-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0026 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0026PQLFAY-SW-WC-3-020719 02/07/2019 9982649N-methyl perfluoro-1-octanesulfonamide0.0077 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0077PQLFAY-SW-WC-3-020719 02/07/2019 9982649N-ethylperfluoro-1-octanesulfonamide0.0077 UG/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0077PQLFAY-SW-OLDOF-1-02011902/01/2019 9978959N-ethylperfluoro-1-octanesulfonamide0.0078 UG/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0078PQLFAY-SW-CFR-RM-76-02021902/04/2019 9979948N-ethylperfluoro-1-octanesulfonamide0.0079 UG/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0079PQLFAY-SW-CFR-RM-84-02021902/04/2019 9979952N-methyl perfluoro-1-octanesulfonamide0.008 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.008PQLFAY-SW-CFR-RM-76-02021902/04/2019 9979948N-methyl perfluoro-1-octanesulfonamide0.0079 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0079PQLFAY-SW-CFR-RM-84-02021902/04/2019 9979952N-ethylperfluoro-1-octanesulfonamide0.008 UG/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.008PQLFAY-SW-OLDOF-1-02011902/01/2019 9978959N-methyl perfluoro-1-octanesulfonamide0.0078 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0078PQLFAY-SW-SEEP-A-1-02071902/07/2019 9982593N-methyl perfluoro-1-octanesulfonamide0.0076 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0076PQLFAY-SW-SEEP-A-1-02071902/07/2019 9982593N-ethylperfluoro-1-octanesulfonamide0.0076 UG/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0076PQLPage 7 of 150
One or more surrogates had relative percent recovery (RPR) values less than the data rejection level. The reporting limit is consid-ered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-3-02071902/07/2019 99826012-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0027 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0027PQLFAY-SW-SEEP-A-3-02071902/07/2019 99826012-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0027 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0027PQLFAY-SW-SEEP-A-3-02071902/07/2019 9982601N-methyl perfluoro-1-octanesulfonamide0.0081 ug/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0081PQLFAY-SW-SEEP-A-3-02071902/07/2019 9982601N-ethylperfluoro-1-octanesulfonamide0.0081 UG/LEPA 537 Rev.1.1 modifiedUJ537_Prep0.0081PQLPage 8 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-4-02061902/06/2019 9981755PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLPage 9 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value..LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PFECA B0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PFECA B0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 N-ethylperfluoro-1-octanesulfonamide0.075 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.075PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 N-ethylperfluoro-1-octanesulfonamide0.075 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.075PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.12 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.12 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.22 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.22PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.22 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.22PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 EVE Acid0.049 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.049PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 EVE Acid0.049 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.049PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980828PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLPage 10 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-C-1-02051902/05/2019 9980832PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PFECA-G0.082 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.082PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PFECA-G0.082 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.082PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 9981759PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PES0.092 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.092PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PES0.092 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.092PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980828PFESA-BP10.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980832PFESA-BP10.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PFESA-BP10.053 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.053PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PFESA-BP10.053 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.053PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 N-methyl perfluoro-1-octanesulfonamide0.069 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.069PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 N-methyl perfluoro-1-octanesulfonamide0.069 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.069PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 Byproduct 60.031 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.031PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 Byproduct 60.031 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.031PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLPage 11 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 9980836PFESA-BP10.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLPage 12 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 9980836PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-WC-1-020719 02/07/2019 9982644PFESA-BP10.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLPage 13 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value..LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-WC-1-020719 02/07/2019 320-51045-25 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-WC-1-020719 02/07/2019 9982644PFESA-BP20.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-WC-1-020719 02/07/2019 9982644PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-WC-1-020719 02/07/2019 9982644PFO4DA0.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLPage 14 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLPage 15 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-B-2-02051902/05/2019 9980824PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLPage 16 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-9-02071902/07/2019 9982628PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 2-(N-methyl perfluoro-1-0.11 ug/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.11PQLPage 17 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitoctanesulfonamido)-ethanolSOPFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-1-02051902/05/2019 9980820PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 9981747PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLPage 18 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-B-3-02061902/06/2019 9981743PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLPage 19 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 9981751PFESA-BP10.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 20 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 9981751PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLPage 21 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFB-02011902/01/2019 320-51031-9 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFB-02011902/01/2019 320-51031-9 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFB-02011902/01/2019 9978970PFMOAA0.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02011902/01/2019 320-51031-9 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLFB-02011902/01/2019 320-51031-9 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLFB-02011902/01/2019 320-51031-9 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFB-02011902/01/2019 320-51031-9 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFB-02011902/01/2019 9978970PFESA-BP20.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02011902/01/2019 320-51031-9 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFB-02011902/01/2019 320-51031-9 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFB-02011902/01/2019 320-51031-9 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFB-02011902/01/2019 320-51031-9 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFB-02011902/01/2019 9978970PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02011902/01/2019 320-51031-9 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFB-02011902/01/2019 320-51031-9 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFB-02011902/01/2019 320-51031-9 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFB-02011902/01/2019 320-51031-9 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLPage 22 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFB-02011902/01/2019 320-51031-9 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLFB-02011902/01/2019 320-51031-9 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLFB-02011902/01/2019 320-51031-9 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB-02011902/01/2019 320-51031-9 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB-02011902/01/2019 320-51031-9 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFB-02011902/01/2019 320-51031-9 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFB-02021902/02/2019 320-51031-6 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLFB-02021902/02/2019 320-51031-6 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLFB-02021902/02/2019 320-51031-6 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFB-02021902/02/2019 320-51031-6 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFB-02021902/02/2019 9979939PMPA0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02021902/02/2019 320-51031-6 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLFB-02021902/02/2019 320-51031-6 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLFB-02021902/02/2019 320-51031-6 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFB-02021902/02/2019 320-51031-6 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFB-02021902/02/2019 320-51031-6 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 23 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFB-02021902/02/2019 320-51031-6 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFB-02021902/02/2019 320-51031-6 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFB-02021902/02/2019 320-51031-6 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFB-02021902/02/2019 9979939PEPA0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02021902/02/2019 320-51031-6 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFB-02021902/02/2019 320-51031-6 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFB-02021902/02/2019 9979939PFESA-BP10.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02021902/02/2019 320-51031-6 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFB-02021902/02/2019 320-51031-6 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFB-02021902/02/2019 320-51031-6 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFB-02021902/02/2019 320-51031-6 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFB-02021902/02/2019 9979939PFO2HxA0.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02021902/02/2019 320-51031-6 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLFB-02021902/02/2019 320-51031-6 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLFB-02021902/02/2019 9979939PFO3OA0.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02021902/02/2019 320-51031-6 PFO3OA0.058 ug/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.058PQLPage 24 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPFB-02021902/02/2019 320-51031-6 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB-02021902/02/2019 9979939PFO4DA0.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02021902/02/2019 320-51031-6 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLFB-02021902/02/2019 320-51031-6 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLFB-02021902/02/2019 9979939PFO5DA0.10 ug/LCl. Spec. Table 3Compound SOPUJ0.10PQLFB-02021902/02/2019 320-51031-6 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLFB-02021902/02/2019 320-51031-6 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLFB-02021902/02/2019 320-51031-6 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFB-02021902/02/2019 320-51031-6 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFB-02021902/02/2019 9979939PFMOAA0.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02021902/02/2019 320-51031-6 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLFB-02021902/02/2019 320-51031-6 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLFB-02021902/02/2019 320-51031-6 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFB-02021902/02/2019 320-51031-6 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFB-02021902/02/2019 9979939PFESA-BP20.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02021902/02/2019 320-51031-6 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLPage 25 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFB-02021902/02/2019 320-51031-6 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFB-02021902/02/2019 320-51031-6 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFB-02021902/02/2019 320-51031-6 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFB-02021902/02/2019 9979939PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02021902/02/2019 320-51031-6 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFB-02021902/02/2019 320-51031-6 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFB-02021902/02/2019 320-51031-6 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFB-02021902/02/2019 320-51031-6 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFB-02021902/02/2019 320-51031-6 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLFB-02021902/02/2019 320-51031-6 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLFB-02021902/02/2019 320-51031-6 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB-02021902/02/2019 320-51031-6 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB-02021902/02/2019 320-51031-6 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFB-02021902/02/2019 320-51031-6 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFB-02051902/05/2019 320-51045-11 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLFB-02051902/05/2019 320-51045-11 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLFB-02051902/05/2019 320-51045-11 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLPage 26 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFB-02051902/05/2019 320-51045-11 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFB-02051902/05/2019 320-51045-11 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLFB-02051902/05/2019 320-51045-11 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLFB-02051902/05/2019 320-51045-11 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFB-02051902/05/2019 320-51045-11 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFB-02051902/05/2019 320-51045-11 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFB-02051902/05/2019 320-51045-11 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFB-02051902/05/2019 320-51045-11 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFB-02051902/05/2019 320-51045-11 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFB-02051902/05/2019 320-51045-11 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFB-02051902/05/2019 320-51045-11 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFB-02051902/05/2019 320-51045-11 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFB-02051902/05/2019 320-51045-11 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFB-02051902/05/2019 320-51045-11 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFB-02051902/05/2019 320-51045-11 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLPage 27 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFB-02051902/05/2019 320-51045-11 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLFB-02051902/05/2019 320-51045-11 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLFB-02051902/05/2019 320-51045-11 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB-02051902/05/2019 320-51045-11 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB-02051902/05/2019 320-51045-11 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLFB-02051902/05/2019 320-51045-11 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLFB-02051902/05/2019 320-51045-11 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLFB-02051902/05/2019 320-51045-11 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLFB-02051902/05/2019 320-51045-11 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFB-02051902/05/2019 320-51045-11 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFB-02051902/05/2019 320-51045-11 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLFB-02051902/05/2019 320-51045-11 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLFB-02051902/05/2019 320-51045-11 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFB-02051902/05/2019 320-51045-11 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFB-02011902/01/2019 320-51031-9 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFB-02011902/01/2019 320-51031-9 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 28 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFB-02011902/01/2019 320-51031-9 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFB-02011902/01/2019 320-51031-9 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFB-02011902/01/2019 9978970PEPA0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02011902/01/2019 320-51031-9 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFB-02011902/01/2019 320-51031-9 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFB-02011902/01/2019 9978970PFESA-BP10.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02011902/01/2019 320-51031-9 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFB-02011902/01/2019 320-51031-9 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFB-02011902/01/2019 320-51031-9 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFB-02011902/01/2019 320-51031-9 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFB-02011902/01/2019 9978970PFO2HxA0.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02011902/01/2019 320-51031-9 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLFB-02011902/01/2019 320-51031-9 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLFB-02011902/01/2019 9978970PFO3OA0.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02011902/01/2019 320-51031-9 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB-02011902/01/2019 320-51031-9 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLPage 29 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFB-02011902/01/2019 9978970PFO4DA0.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02011902/01/2019 320-51031-9 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLFB-02011902/01/2019 320-51031-9 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLFB-02011902/01/2019 320-51031-9 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLFB-02011902/01/2019 320-51031-9 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLFB-02011902/01/2019 320-51031-9 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFB-02011902/01/2019 320-51031-9 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFB-02011902/01/2019 9978970PMPA0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02011902/01/2019 320-51031-9 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLFB-02011902/01/2019 320-51031-9 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLFB-02011902/01/2019 320-51031-9 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFB-02011902/01/2019 320-51031-9 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFB-02051902/05/2019 320-51045-11 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFB-02051902/05/2019 320-51045-11 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFB-02051902/05/2019 320-51045-11 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFB-02051902/05/2019 320-51045-11 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFB-02051902/05/2019 320-51045-11 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLPage 30 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFB-02051902/05/2019 320-51045-11 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFB-02051902/05/2019 320-51045-11 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFB-02051902/05/2019 320-51045-11 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFB-02051902/05/2019 320-51045-11 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLFB-02051902/05/2019 320-51045-11 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLFB-02051902/05/2019 320-51045-11 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFB-02051902/05/2019 320-51045-11 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFB-02061902/06/2019 320-51045-12 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLFB-02061902/06/2019 320-51045-12 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLFB-02061902/06/2019 320-51045-12 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFB-02061902/06/2019 320-51045-12 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFB-02061902/06/2019 9981763PMPA0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02061902/06/2019 320-51045-12 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLFB-02061902/06/2019 320-51045-12 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLFB-02061902/06/2019 320-51045-12 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFB-02061902/06/2019 320-51045-12 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFB-02061902/06/2019 320-51045-12 2-(N-ethyl perfluoro-1-octanesulfonamido)0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 31 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnit-ethanolFB-02061902/06/2019 320-51045-12 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFB-02061902/06/2019 320-51045-12 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFB-02061902/06/2019 320-51045-12 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFB-02061902/06/2019 9981763PEPA0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02061902/06/2019 320-51045-12 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFB-02061902/06/2019 320-51045-12 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFB-02061902/06/2019 9981763PFESA-BP10.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02061902/06/2019 320-51045-12 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFB-02061902/06/2019 320-51045-12 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFB-02061902/06/2019 320-51045-12 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFB-02061902/06/2019 320-51045-12 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFB-02061902/06/2019 9981763PFO2HxA0.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02061902/06/2019 320-51045-12 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLFB-02061902/06/2019 320-51045-12 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLFB-02061902/06/2019 9981763PFO3OA0.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLPage 32 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFB-02061902/06/2019 320-51045-12 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB-02061902/06/2019 320-51045-12 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB-02061902/06/2019 9981763PFO4DA0.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02061902/06/2019 320-51045-12 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLFB-02061902/06/2019 320-51045-12 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLFB-02061902/06/2019 9981763PFO5DA0.10 ug/LCl. Spec. Table 3Compound SOPUJ0.10PQLFB-02061902/06/2019 320-51045-12 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLFB-02061902/06/2019 320-51045-12 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLFB-02061902/06/2019 320-51045-12 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFB-02061902/06/2019 320-51045-12 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFB-02061902/06/2019 9981763PFMOAA0.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02061902/06/2019 320-51045-12 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLFB-02061902/06/2019 320-51045-12 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLFB-02061902/06/2019 320-51045-12 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFB-02061902/06/2019 320-51045-12 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFB-02061902/06/2019 9981763PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02061902/06/2019 320-51045-12 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLPage 33 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFB-02061902/06/2019 320-51045-12 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFB-02061902/06/2019 320-51045-12 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFB-02061902/06/2019 320-51045-12 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFB-02061902/06/2019 320-51045-12 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLFB-02061902/06/2019 320-51045-12 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLFB-02061902/06/2019 320-51045-12 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB-02061902/06/2019 320-51045-12 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB-02061902/06/2019 320-51045-12 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFB-02061902/06/2019 320-51045-12 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFB-02061902/06/2019 9981763PFESA-BP20.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLFB-02061902/06/2019 320-51045-12 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFB-02061902/06/2019 320-51045-12 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFB-02061902/06/2019 320-51045-12 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFB-02061902/06/2019 320-51045-12 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-2J-02021902/02/2019 9979923PFO4DA0.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLPage 34 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-2J-02021902/02/2019 9979923PFESA-BP10.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLPage 35 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-2J-02021902/02/2019 9979923PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLPage 36 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-OLDOF-2-02011902/01/2019 9978966PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 37 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-1-02011902/01/2019 9978962PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLEB-02041902/04/2019 320-51024-5 NVHOS0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 NVHOS0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 9979959PMPA0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLEB-02041902/04/2019 320-51024-5 PMPA0.010 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.010PQLPage 38 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitEB-02041902/04/2019 320-51024-5 PMPA0.010 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.010PQLEB-02041902/04/2019 320-51024-5 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 9979959PEPA0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLEB-02041902/04/2019 320-51024-5 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLEB-02041902/04/2019 320-51024-5 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLEB-02041902/04/2019 9979959PFESA-BP10.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLEB-02041902/04/2019 320-51024-5 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 39 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitEB-02041902/04/2019 9979959PFO2HxA0.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLEB-02041902/04/2019 320-51024-5 PFO2HxA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 PFO2HxA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 9979959PFO3OA0.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLEB-02041902/04/2019 320-51024-5 PFO3OA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 PFO3OA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 9979959PFO4DA0.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLEB-02041902/04/2019 320-51024-5 PFO4DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 PFO4DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 9979959PFO5DA0.10 ug/LCl. Spec. Table 3Compound SOPUJ0.10PQLEB-02041902/04/2019 320-51024-5 PFO5DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 PFO5DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 9979959PFMOAA0.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLEB-02041902/04/2019 320-51024-5 PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLEB-02041902/04/2019 320-51024-5 PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLPage 40 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value..LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitEB-02041902/04/2019 320-51024-5 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 9979959PFESA-BP20.050 ug/LCl. Spec. Table 3Compound SOPUJ0.050PQLEB-02041902/04/2019 320-51024-5 PFESA-BP20.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 PFESA-BP20.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 9979959PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLEB-02041902/04/2019 320-51024-5 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 R-EVE0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 R-EVE0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 Byproduct 40.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 Byproduct 40.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 Byproduct 50.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 Byproduct 50.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLEB-02041902/04/2019 320-51024-5 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 41 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitEB-02041902/04/2019 320-51024-5 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 42 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PFO3OA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PFO3OA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PFO4DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PFO4DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PFO5DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PFO5DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PFESA-BP20.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PFESA-BP20.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 43 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 R-EVE0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 R-EVE0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 Byproduct 40.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 Byproduct 40.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 Byproduct 50.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 Byproduct 50.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 44 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value..LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PFO4DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PFO4DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PFO5DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PFO5DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PFESA-BP20.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 45 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PFESA-BP20.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 R-EVE0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 R-EVE0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 2-(N-methyl perfluoro-1-octanesulfonamido)0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLPage 46 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnit-ethanolFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-OLDOF-2L-02021902/02/2019 9979927PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLPage 47 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLPage 48 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-3-02021902/02/2019 9979931PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLPage 49 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-OLDOF-4-02021902/02/2019 9979935PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 50 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-5-02021902/02/2019 9979943PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-OLDOF-5K-02021902/02/2019 9979947PFESA-BP10.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLPage 51 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-5K-02021902/02/2019 9979947PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 52 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value..LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLPage 53 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 54 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-1-02071902/07/2019 9982569Nitrate0.25 MG/L0.25300.0UJ0.50MDLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-1-02071902/07/2019 9982596PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PES0.23 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.23PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PES0.23 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.23PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 2-(N-ethyl perfluoro-1-octanesulfonamido)0.30 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.30PQLPage 55 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnit-ethanolFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.30 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.30PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.55 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.55PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.55 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.55PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 N-methyl perfluoro-1-octanesulfonamide0.17 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.17PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 N-methyl perfluoro-1-octanesulfonamide0.17 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.17PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 N-ethylperfluoro-1-octanesulfonamide0.19 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.19PQLFAY-SW-SEEP-A-10-02071902/07/2019 9982632PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PFECA-G0.20 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.20PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PFECA-G0.20 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.20PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PES0.23 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.23PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PES0.23 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.23PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.30 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.30PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.30 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.30PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.55 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.55PQLPage 56 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.55 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.55PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 N-methyl perfluoro-1-octanesulfonamide0.17 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.17PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 N-methyl perfluoro-1-octanesulfonamide0.17 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.17PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 N-ethylperfluoro-1-octanesulfonamide0.19 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.19PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 N-ethylperfluoro-1-octanesulfonamide0.19 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.19PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PFECA B0.30 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.30PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PFECA B0.30 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.30PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PFECA B0.30 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.30PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PFECA B0.30 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.30PQLFAY-SW-SEEP-A-11-02071902/07/2019 9982636PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PFECA-G0.20 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.20PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PFECA-G0.20 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.20PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 57 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-12-02071902/07/2019 9982640PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 58 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-2-02071902/07/2019 9982600PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 59 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-3-02071902/07/2019 9982604PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 2-(N-ethyl perfluoro-1-octanesulfonamido)0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 60 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnit-ethanolFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-4-02071902/07/2019 9982608PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 61 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-5-02071902/07/2019 9982612PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 2-(N-ethyl perfluoro-1-octanesulfonamido)0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 62 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnit-ethanolFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-6-02071902/07/2019 9982616PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 63 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-7-02071902/07/2019 9982620PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 2-(N-ethyl perfluoro-1-octanesulfonamido)0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 64 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnit-ethanolFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-8-02071902/07/2019 9982624PFECA-G0.050 UG/LCl. Spec. Table 3Compound SOPUJ0.050PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLPage 65 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLPage 66 of 150
Associated LCS and/or LCSD analysis had relative percent recovery (RPR) values below the data rejection level. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFB-02071902/07/2019 9982590Benzidine20 UG/L208270DUJ3510C60MDLFAY-SW-SEEP-A-1-02071902/07/2019 9982569Benzidine20 UG/L208270DUJ3510C60MDLFAY-SW-SEEP-A-11-02071902/07/2019 9982579Benzidine20 UG/L208270DUJ3510C60MDLPage 67 of 150
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the data rejection level. The reporting limit is considered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-C-1-02051902/05/2019 9980788Benzidine21 UG/L218270DUJ3510C62MDLFAY-SW-SEEP-C-1-02051902/05/2019 99807882-Chloroethyl VinylEther0.2 UG/L0.28260CUJ5030C10MDLPage 68 of 150
Associated MS and/or MSD analysis had relative percent recovery (RPR) values higher than the upper control limit. The reported result may be biasedhigh.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-TR-1-1-A-02021902/02/2019 9979890Chloride5.2 MG/L1.0300.0J2.0MDLFAY-SW-OLDOF-TR-1-1-S-02021902/02/2019 9979891Chloride27500 MG/L2000300.0J4000MDLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PFO4DA0.16 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PFO4DA0.18 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-OLDOF-5-A-02021902/02/2019 9979908Chloride14.1 MG/L1.0300.0J2.0MDLFAY-SW-OLDOF-5-S-02021902/02/2019 9979909Chloride62700 MG/L4000300.0J8000MDLFAY-SW-OLDOF-5-02021902/02/2019 9979943PFO5DA4.2 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PFO5DA4.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PFO5DA3.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-OLDOF-4-02021902/02/2019 9979935PFO3OA9.0 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PFO3OA7.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PFO3OA6.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PFO4DA2.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-OLDOF-4-02021902/02/2019 9979935PFO5DA1.1 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PFO5DA1.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PFO5DA1.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-OLDOF-3-A-02021902/02/2019 9979898Chloride7.8 MG/L1.0300.0J2.0MDLFAY-SW-OLDOF-3-S-02021902/02/2019 9979899Chloride58000 MG/L4000300.0J8000MDLPage 69 of 150
Associated MS and/or MSD analysis had relative percent recovery (RPR) values higher than the upper control limit. The reported result may be biasedhigh.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-2L-02021902/02/2019 9979927PFESA-BP20.35 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2L-02021902/02/2019 9979924PFESA-BP20.36 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PFESA-BP20.35 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-OLDOF-2L-02021902/02/2019 9979927PEPA2.1 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2L-02021902/02/2019 9979924PEPA2.1 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PEPA2.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-OLDOF-2L-02021902/02/2019 9979927PFO4DA2.1 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2L-02021902/02/2019 9979924PFO4DA2.1 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PFO4DA1.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PFO4DA2.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-OLDOF-2L-02021902/02/2019 9979927PFO5DA0.81 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-OLDOF-2L-02021902/02/2019 9979924PFO5DA0.82 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PFO5DA0.87 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 Byproduct 40.0083 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 Byproduct 40.0074 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 Byproduct 50.014 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 Byproduct 50.013 UG/LCl. Spec. Table 3CompoundJPFAS_DI_Prep0.0020PQLPage 70 of 150
Associated MS and/or MSD analysis had relative percent recovery (RPR) values higher than the upper control limit. The reported result may be biasedhigh.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PFO5DA0.055 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFB-02011902/01/2019 320-51031-9 PFO5DA0.37 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFB-02011902/01/2019 320-51031-9 PFO5DA0.45 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 R-EVE13 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 R-EVE12.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-B-2-02051902/05/2019 9980785Chloride6.2 MG/L1.0300.0J2.0MDLFAY-SW-SEEP-B-2-02051902/05/2019 9980785Sulfate13.0 MG/L1.5300.0J5.0MDLFAY-SW-WC-5-020719 02/07/2019 9982587Nitrate0.96 MG/L0.25300.0J0.50MDLFAY-SW-WC-4-020719 02/07/2019 9982586Nitrate0.93 MG/L0.25300.0J0.50MDLFAY-SW-WC-3-020719 02/07/2019 9982585Nitrate0.88 MG/L0.25300.0J0.50MDLFAY-SW-WC-2-020719 02/07/2019 9982584Nitrate0.83 MG/L0.25300.0J0.50MDLFAY-SW-SEEP-C-1-E2-02051902/05/2019 9980793Chloride11.9 MG/L1.0300.0J2.0MDLFAY-SW-SEEP-C-1-E2-02051902/05/2019 9980793Sulfate13.6 MG/L1.5300.0J5.0MDLFAY-SW-SEEP-C-1-020519-D02/05/2019 9980792Sulfate24.6 MG/L1.5300.0J5.0MDLFAY-SW-SEEP-C-1-020519-D02/05/2019 9980792Chloride10.9 MG/L1.0300.0J2.0MDLFAY-SW-SEEP-C-1-02051902/05/2019 9980788Sulfate24.7 MG/L1.5300.0J5.0MDLFAY-SW-SEEP-C-1-02051902/05/2019 9980788Aluminum1.45 MG/L0.153200.7 Rev. 4.4J200.70.300MDLFAY-SW-SEEP-C-1-02051902/05/2019 9980788Iron3.82 MG/L0.0400200.7 Rev. 4.4J200.70.200MDLPage 71 of 150
Associated MS and/or MSD analysis had relative percent recovery (RPR) values higher than the upper control limit. The reported result may be biasedhigh.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-C-1-02051902/05/2019 9980828PFESA-BP20.59 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980825PFESA-BP20.59 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980832PFESA-BP20.50 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980829PFESA-BP20.49 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PFESA-BP20.59 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.061PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980788Chloride10.5 MG/L1.0300.0J2.0MDLFAY-SW-SEEP-B-4-02061902/06/2019 9989189Aluminum0.478 MG/L0.153200.7 Rev. 4.4J200.70.300MDLFAY-SW-OLDOF-5-02041902/04/2019 9979911Ammonia0.053 MG/L0.050350.1J0.10MDLPage 72 of 150
Only one surrogate has relative percent recovery (RPR) values outside control limits and the parameter is a PFC (Detects).LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-3-02071902/07/2019 9982601PerfluorobutaneSulfonic Acid0.0016 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep0.0009PQLFAY-SW-SEEP-A-3-02071902/07/2019 9982601Hfpo Dimer Acid13 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep0.18PQLFAY-SW-SEEP-A-1-02071902/07/2019 9982593Hfpo Dimer Acid10 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep0.17PQLFAY-SW-OLDOF-1-02011902/01/2019 9978959PerfluorobutaneSulfonic Acid0.0014 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep0.00086PQLFAY-SW-OLDOF-1-02011902/01/2019 9978959Hfpo Dimer Acid4.8 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep0.17PQLFAY-SW-CFR-RM-76-02021902/04/2019 9979948PerfluorobutaneSulfonic Acid0.002 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep0.00087PQLFAY-SW-CFR-RM-84-02021902/04/2019 9979952PerfluorobutaneSulfonic Acid0.0022 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep0.00089PQLFAY-SW-CFR-RM-76-02021902/04/2019 9979948Hfpo Dimer Acid0.0029 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep0.0017PQLFAY-SW-WC-3-020719 02/07/2019 9982649Hfpo Dimer Acid0.12 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep0.0017PQLFAY-SW-WC-1-020719 02/07/2019 9982641Hfpo Dimer Acid0.29 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep0.0017PQLPage 73 of 150
Quality review criteria exceeded between the REP (laboratory replicate) and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-8-02071902/07/2019 9982576Total SuspendedSolids712 MG/L40.02540 D-1997J120MDLFAY-SW-SEEP-A-8-02071902/07/2019 9982576Chloride4.7 MG/L1.0300.0J2.0MDLFAY-SW-SEEP-A-7-02071902/07/2019 9982575Chloride6.6 MG/L1.0300.0J2.0MDLFAY-SW-SEEP-A-6-02071902/07/2019 9982574Chloride4.5 MG/L1.0300.0J2.0MDLFAY-SW-SEEP-A-5-02071902/07/2019 9982573Chloride5.5 MG/L1.0300.0J2.0MDLFAY-SW-SEEP-A-4-02071902/07/2019 9982572Chloride10.4 MG/L1.0300.0J2.0MDLFAY-SW-SEEP-A-3-02071902/07/2019 9982571Chloride11.5 MG/L1.0300.0J2.0MDLFAY-SW-SEEP-A-2-02071902/07/2019 9982570Chloride11.2 MG/L1.0300.0J2.0MDLFAY-SW-SEEP-A-12-02071902/07/2019 9982580Total SuspendedSolids7.40 MG/L1.002540 D-1997J3.00MDLFAY-SW-SEEP-A-12-02071902/07/2019 9982640PFO5DA2.5 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PFO5DA4.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PFO5DA3.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-A-12-02071902/07/2019 9982640PFESA-BP10.098 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PFESA-BP10.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PFESA-BP10.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-10-02071902/07/2019 9982578Chloride9.0 MG/L1.0300.0J2.0MDLFAY-SW-SEEP-A-1-02071902/07/2019 9982569Chloride9.0 MG/L1.0300.0J2.0MDLFAY-SW-OLDOF-4-02021902/02/2019 9979935PFO4DA2.8 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PFO4DA2.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLPage 74 of 150
Quality review criteria exceeded between the REP (laboratory replicate) and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-3-02021902/02/2019 9979931PFO4DA2.2 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PFO4DA1.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PFO4DA2.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-OLDOF-2L-02021902/02/2019 9979927PFESA-BP10.24 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2L-02021902/02/2019 9979924PFESA-BP10.21 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PFESA-BP10.25 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PFESA-BP10.28 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PFO5DA1.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-WC-5-020719 02/07/2019 9982587Total SuspendedSolids9.10 MG/L1.002540 D-1997J3.00MDLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 Byproduct 50.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 Byproduct 50.21 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-1-02051902/05/2019 9980784Total SuspendedSolids236 MG/L10.02540 D-1997J30.0MDLFAY-SW-SEEP-A-9-02071902/07/2019 9982577Total SuspendedSolids3740 MG/L1002540 D-1997J300MDLFAY-SW-SEEP-B-2-02051902/05/2019 9980785Total SuspendedSolids11.0 MG/L1.002540 D-1997J3.00MDLFAY-SW-WC-4-020719 02/07/2019 9982586Total SuspendedSolids12.0 MG/L2.002540 D-1997J6.00MDLFAY-SW-WC-1-020719 02/07/2019 9982583Chloride10.8 MG/L1.0300.0J2.0MDLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PFO5DA0.11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLPage 75 of 150
Quality review criteria exceeded between the REP (laboratory replicate) and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-WC-1-020719 02/07/2019 9982644PEPA0.13 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PEPA0.19 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PEPA0.23 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 Byproduct 41.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 Byproduct 41.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 Byproduct 51.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 Byproduct 51.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 9980793Total SuspendedSolids28.1 MG/L1.002540 D-1997J3.00MDLFAY-SW-SEEP-C-1-020519-D02/05/2019 9980792Total SuspendedSolids14.6 MG/L1.002540 D-1997J3.00MDLFAY-SW-SEEP-C-1-02051902/05/2019 9980788Total SuspendedSolids24.5 MG/L1.002540 D-1997J3.00MDLFB-02051902/05/2019 9980794Total SuspendedSolids1.34 MG/L1.002540 D-1997J3.00MDLPage 76 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-9-02071902/07/2019 9982628PFO3OA24 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PFO3OA24 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PFO3OA24.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-9-02071902/07/2019 9982628PFO4DA19 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PFO4DA21 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PFO4DA22.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-A-9-02071902/07/2019 9982628PFO5DA15 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PFO5DA17 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PFO5DA17.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-A-9-02071902/07/2019 9982628PEPA18 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PEPA22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PEPA22.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 R-EVE0.80 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 R-EVE0.77 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 Byproduct 41.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 Byproduct 41.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 Byproduct 56.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 77 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 Byproduct 55.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 Byproduct 60.037 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 Byproduct 60.039 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 NVHOS3.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 NVHOS3.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 Hydro-EVE Acid0.86 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 Hydro-EVE Acid0.87 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 Hydro-EVE Acid1.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 Hydro-EVE Acid1.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-A-8-02071902/07/2019 9982624PFMOAA17 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PFMOAA17 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PFMOAA17.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 EVE Acid0.54 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 EVE Acid0.53 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-A-8-02071902/07/2019 9982624PFESA-BP21.4 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PFESA-BP21.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PFESA-BP21.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLPage 78 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-8-02071902/07/2019 9982624PFO2HxA18 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PFO2HxA20 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PFO2HxA20.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-A-8-02071902/07/2019 9982624PFO3OA5.8 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PFO3OA6.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PFO3OA6.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-8-02071902/07/2019 9982624PFO4DA5.3 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PFO4DA6.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PFO4DA6.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-A-8-02071902/07/2019 9982624PFO5DA4.2 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PFO5DA6.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PFO5DA6.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-A-8-02071902/07/2019 9982624PEPA15 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PEPA19 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PEPA19.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-A-8-02071902/07/2019 9982624PFESA-BP12.8 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PFESA-BP11.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLPage 79 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PFESA-BP11.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-8-02071902/07/2019 9982624PMPA34 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PMPA38 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 PMPA38.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-A-7-02071902/07/2019 9982620PFMOAA41 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PFMOAA43 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PFMOAA43.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 EVE Acid0.56 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 EVE Acid0.55 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-A-7-02071902/07/2019 9982620PFESA-BP21.3 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PFESA-BP21.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PFESA-BP21.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 Hydro-EVE Acid1.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 Hydro-EVE Acid1.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 R-EVE1.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 R-EVE1.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 Byproduct 42.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLPage 80 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 Byproduct 42.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 Byproduct 513 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 Byproduct 513.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 Byproduct 60.051 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 Byproduct 60.051 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 NVHOS0.38 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-8-02071902/07/2019 320-51045-20 NVHOS0.38 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-7-02071902/07/2019 9982620PFO2HxA31 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PFO2HxA35 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PFO2HxA34.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-A-7-02071902/07/2019 9982620PFO3OA9.8 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PFO3OA11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PFO3OA11.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-7-02071902/07/2019 9982620PFO4DA6.2 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PFO4DA8.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PFO4DA8.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-A-7-02071902/07/2019 9982620PFO5DA4.2 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLPage 81 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PFO5DA5.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PFO5DA5.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-A-7-02071902/07/2019 9982620PEPA17 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PEPA22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PEPA22.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-A-7-02071902/07/2019 9982620PFESA-BP10.99 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PFESA-BP11.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PFESA-BP11.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-7-02071902/07/2019 9982620PMPA39 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PMPA46 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 PMPA46.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 Byproduct 60.031 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 Byproduct 60.032 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 NVHOS0.88 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-7-02071902/07/2019 320-51045-19 NVHOS0.88 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 EVE Acid0.67 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 EVE Acid0.68 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLPage 82 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-6-02071902/07/2019 9982616PFESA-BP21.2 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PFESA-BP21.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PFESA-BP21.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 Hydro-EVE Acid1.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 Hydro-EVE Acid1.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-A-6-02071902/07/2019 9982616PFO3OA6.0 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PFO3OA6.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PFO3OA6.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-6-02071902/07/2019 9982616PFO4DA5.0 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PFO4DA5.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PFO4DA6.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-A-6-02071902/07/2019 9982616PFO5DA3.8 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PFO5DA4.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PFO5DA4.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-A-6-02071902/07/2019 9982616PEPA14 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PEPA18 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PEPA19.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLPage 83 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-6-02071902/07/2019 9982616PFESA-BP11.5 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PFESA-BP11.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PFESA-BP11.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 R-EVE1.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 R-EVE1.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 Byproduct 42.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 Byproduct 42.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 Byproduct 59.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 Byproduct 510.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 Byproduct 60.040 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 Byproduct 60.037 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 NVHOS0.38 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 NVHOS0.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-5-02071902/07/2019 9982612PFMOAA25 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PFMOAA30 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PFMOAA29.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 EVE Acid0.52 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLPage 84 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 EVE Acid0.53 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-A-5-02071902/07/2019 9982612PFESA-BP21.1 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PFESA-BP21.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PFESA-BP21.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 Hydro-EVE Acid1.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 Hydro-EVE Acid1.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-A-5-02071902/07/2019 9982612PFO2HxA23 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PFO2HxA28 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PFO2HxA27.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-A-5-02071902/07/2019 9982612PFO3OA8.0 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PFO3OA8.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PFO3OA8.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-5-02071902/07/2019 9982612PFO4DA5.6 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PFO4DA6.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PFO4DA6.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-A-5-02071902/07/2019 9982612PFO5DA3.8 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PFO5DA4.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLPage 85 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PFO5DA4.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-A-5-02071902/07/2019 9982612PEPA15 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PEPA20 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PEPA20.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-A-5-02071902/07/2019 9982612PFESA-BP11.3 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PFESA-BP11.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PFESA-BP11.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-5-02071902/07/2019 9982612PMPA31 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PMPA42 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 PMPA42.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 R-EVE0.77 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 R-EVE0.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 Byproduct 41.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 Byproduct 41.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 Byproduct 56.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 Byproduct 56.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 Byproduct 60.026 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLPage 86 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 Byproduct 60.025 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 NVHOS0.61 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-5-02071902/07/2019 320-51045-17 NVHOS0.62 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-4-02071902/07/2019 9982608PFMOAA42 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PFMOAA49 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PFMOAA49.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 EVE Acid0.24 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 EVE Acid0.25 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-A-4-02071902/07/2019 9982608PFESA-BP20.77 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PFESA-BP20.83 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PFESA-BP20.83 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-A-4-02071902/07/2019 9982608PFO2HxA27 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PFO2HxA28 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PFO2HxA28.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-A-4-02071902/07/2019 9982608PFO3OA8.1 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PFO3OA8.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PFO3OA8.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 87 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-4-02071902/07/2019 9982608PFO4DA4.1 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PFO4DA4.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PFO4DA4.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-A-4-02071902/07/2019 9982608PFO5DA3.6 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PFO5DA4.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PFO5DA4.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-A-4-02071902/07/2019 9982608PEPA9.3 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PEPA12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PEPA12.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-A-4-02071902/07/2019 9982608PFESA-BP10.70 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PFESA-BP10.56 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PFESA-BP10.56 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-4-02071902/07/2019 9982608PMPA23 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PMPA28 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 PMPA28.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-A-3-02071902/07/2019 9982604PFESA-BP21.0 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PFESA-BP21.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLPage 88 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PFESA-BP21.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 Hydro-EVE Acid1.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 Hydro-EVE Acid1.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 R-EVE1.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 R-EVE1.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 Byproduct 42.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 Byproduct 42.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 Byproduct 523 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 Byproduct 525.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 Byproduct 60.045 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 Byproduct 60.048 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 NVHOS0.64 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-4-02071902/07/2019 320-51045-16 NVHOS0.72 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-3-02071902/07/2019 9982604PFMOAA69 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PFMOAA79 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PFMOAA83.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 EVE Acid0.93 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLPage 89 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 EVE Acid1.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-A-3-02071902/07/2019 9982604PFO2HxA36 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PFO2HxA38 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PFO2HxA40.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-A-3-02071902/07/2019 9982604PFO3OA14 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PFO3OA13 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PFO3OA14.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-3-02071902/07/2019 9982604PFO4DA7.3 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PFO4DA7.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PFO4DA8.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-A-3-02071902/07/2019 9982604PFO5DA4.8 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PFO5DA5.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PFO5DA6.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-A-3-02071902/07/2019 9982604PEPA6.7 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PEPA8.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PEPA8.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-A-3-02071902/07/2019 9982604PFESA-BP14.5 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLPage 90 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PFESA-BP13.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PFESA-BP14.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-3-02071902/07/2019 9982604PMPA18 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PMPA22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 PMPA23.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 R-EVE1.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 R-EVE1.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 Byproduct 42.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 Byproduct 42.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 Byproduct 523 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 Byproduct 523.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 Byproduct 60.047 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 Byproduct 60.046 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 NVHOS0.91 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-3-02071902/07/2019 320-51045-15 NVHOS0.96 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-2-02071902/07/2019 9982600PFMOAA68 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PFMOAA82 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLPage 91 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PFMOAA82.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 EVE Acid0.83 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 EVE Acid0.84 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-A-2-02071902/07/2019 9982600PFESA-BP20.99 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PFESA-BP21.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PFESA-BP21.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 Hydro-EVE Acid1.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 Hydro-EVE Acid1.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-A-2-02071902/07/2019 9982600PFO2HxA36 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PFO2HxA40 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PFO2HxA40.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-A-2-02071902/07/2019 9982600PFO3OA14 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PFO3OA14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PFO3OA14.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-2-02071902/07/2019 9982600PFO4DA7.2 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PFO4DA7.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PFO4DA7.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLPage 92 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-2-02071902/07/2019 9982600PFO5DA4.6 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PFO5DA5.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PFO5DA6.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-A-2-02071902/07/2019 9982600PEPA6.9 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PEPA8.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PEPA8.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-A-2-02071902/07/2019 9982600PFESA-BP14.1 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PFESA-BP13.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PFESA-BP13.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-2-02071902/07/2019 9982600PMPA19 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PMPA23 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 PMPA23.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 R-EVE0.89 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 R-EVE0.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 Byproduct 42.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 Byproduct 42.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 Byproduct 50.49 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 93 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 Byproduct 50.48 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 Byproduct 60.026 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 Byproduct 60.026 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 NVHOS1.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-2-02071902/07/2019 320-51045-14 NVHOS0.98 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-12-02071902/07/2019 9982640PFESA-BP21.3 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PFESA-BP21.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PFESA-BP21.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 Hydro-EVE Acid0.31 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 Hydro-EVE Acid0.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-A-12-02071902/07/2019 9982640PFMOAA15 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PFMOAA16 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PFMOAA17.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 EVE Acid0.039 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 EVE Acid0.03 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-A-12-02071902/07/2019 9982640PFO2HxA30 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PFO2HxA30 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLPage 94 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PFO2HxA30.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-A-12-02071902/07/2019 9982640PFO3OA4.8 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PFO3OA5.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PFO3OA5.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-12-02071902/07/2019 9982640PFO4DA4.2 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PFO4DA4.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PFO4DA4.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-A-12-02071902/07/2019 9982640PEPA7.4 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PEPA8.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PEPA8.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 Hydro-EVE Acid10 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.14PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 Hydro-EVE Acid10.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.14PQLFAY-SW-SEEP-A-12-02071902/07/2019 9982640PMPA20 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PMPA22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 PMPA21.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 R-EVE4.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.35PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 R-EVE4.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.35PQLPage 95 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 Byproduct 46.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.79PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 Byproduct 46.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.79PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 Byproduct 574 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.29PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 Byproduct 573.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.29PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 Byproduct 60.24 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.077PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 Byproduct 60.25 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.077PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 NVHOS0.57 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-12-02071902/07/2019 320-51045-24 NVHOS0.56 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-11-02071902/07/2019 9982636PFESA-BP26.1 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PFESA-BP27.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.15PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PFESA-BP27.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.15PQLFAY-SW-SEEP-A-11-02071902/07/2019 9982636PFMOAA76 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PFMOAA90 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep1.1PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PFMOAA90.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep1.1PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 EVE Acid24 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 EVE Acid24.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLFAY-SW-SEEP-A-11-02071902/07/2019 9982636PFO2HxA62 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLPage 96 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PFO2HxA67 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.41PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PFO2HxA67.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.41PQLFAY-SW-SEEP-A-11-02071902/07/2019 9982636PFO3OA26 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PFO3OA26 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.29PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PFO3OA26.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.29PQLFAY-SW-SEEP-A-11-02071902/07/2019 9982636PFO4DA20 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PFO4DA22 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.39PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PFO4DA21.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.39PQLFAY-SW-SEEP-A-11-02071902/07/2019 9982636PFO5DA16 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PFO5DA24 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.17PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PFO5DA24.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.17PQLFAY-SW-SEEP-A-11-02071902/07/2019 9982636PEPA18 UG/LCl. Spec. Table 3Compound SOPJ0.50PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PEPA22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.23PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PEPA22.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.23PQLFAY-SW-SEEP-A-11-02071902/07/2019 9982636PFESA-BP151 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PFESA-BP154 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.13PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PFESA-BP153.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.13PQLPage 97 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-11-02071902/07/2019 9982636PMPA46 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PMPA51 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep2.8PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 PMPA50.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep2.8PQLFAY-SW-SEEP-A-10-02071902/07/2019 9982632PFESA-BP26.1 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PFESA-BP26.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.15PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PFESA-BP26.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.15PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 Hydro-EVE Acid9.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.14PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 Hydro-EVE Acid9.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.14PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 R-EVE4.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.35PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 R-EVE4.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.35PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 Byproduct 46.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.79PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 Byproduct 46.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.79PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 Byproduct 570 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.29PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 Byproduct 568.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.29PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 Byproduct 60.24 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.077PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 Byproduct 60.24 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.077PQLFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 NVHOS3.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.27PQLPage 98 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-11-02071902/07/2019 320-51045-23 NVHOS3.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.27PQLFAY-SW-SEEP-A-10-02071902/07/2019 9982632PFMOAA75 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PFMOAA84 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep1.1PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PFMOAA83.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep1.1PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 EVE Acid24 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 EVE Acid23.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLFAY-SW-SEEP-A-10-02071902/07/2019 9982632PFO2HxA59 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PFO2HxA65 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.41PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PFO2HxA63.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.41PQLFAY-SW-SEEP-A-10-02071902/07/2019 9982632PFO3OA25 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PFO3OA25 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.29PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PFO3OA25.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.29PQLFAY-SW-SEEP-A-10-02071902/07/2019 9982632PFO4DA19 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PFO4DA21 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.39PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PFO4DA20.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.39PQLFAY-SW-SEEP-A-10-02071902/07/2019 9982632PFO5DA17 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PFO5DA25 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.17PQLPage 99 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PFO5DA24.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.17PQLFAY-SW-SEEP-A-10-02071902/07/2019 9982632PEPA19 UG/LCl. Spec. Table 3Compound SOPJ0.50PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PEPA22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.23PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PEPA22.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.23PQLFAY-SW-SEEP-A-10-02071902/07/2019 9982632PFESA-BP149 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PFESA-BP150 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.13PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PFESA-BP149.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.13PQLFAY-SW-SEEP-A-10-02071902/07/2019 9982632PMPA48 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PMPA52 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep2.8PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 PMPA51.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep2.8PQLFAY-SW-SEEP-A-1-02071902/07/2019 9982596PFESA-BP21.2 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PFESA-BP21.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PFESA-BP21.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 Hydro-EVE Acid1.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 Hydro-EVE Acid1.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 R-EVE1.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 R-EVE1.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLPage 100 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 Byproduct 42.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 Byproduct 42.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 Byproduct 523 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 Byproduct 524.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 Byproduct 60.047 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 Byproduct 60.048 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 NVHOS3.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.27PQLFAY-SW-SEEP-A-10-02071902/07/2019 320-51045-22 NVHOS3.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.27PQLFAY-SW-SEEP-A-1-02071902/07/2019 9982569Sulfate30.3 MG/L6.0300.0J20.0MDLFAY-SW-SEEP-A-1-02071902/07/2019 9982596PFMOAA62 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PFMOAA84 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PFMOAA86.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 EVE Acid0.96 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 EVE Acid1.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-A-1-02071902/07/2019 9982596PFO2HxA35 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PFO2HxA41 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PFO2HxA41.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLPage 101 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-1-02071902/07/2019 9982596PFO3OA12 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PFO3OA14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PFO3OA14.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-1-02071902/07/2019 9982596PFO4DA6.8 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PFO4DA8.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PFO4DA7.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-A-1-02071902/07/2019 9982596PFO5DA6.3 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PFO5DA5.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PFO5DA5.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-A-1-02071902/07/2019 9982596PEPA7.1 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PEPA9.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PEPA10.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-A-1-02071902/07/2019 9982596PFESA-BP14.3 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PFESA-BP14.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PFESA-BP14.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-1-02071902/07/2019 9982596PMPA19 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PMPA25 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLPage 102 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 PMPA25.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PFESA-BP20.11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PFESA-BP20.11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 NVHOS0.98 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-1-02071902/07/2019 320-51045-13 NVHOS1.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PFMOAA0.34 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PFMOAA0.25 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PMPA3.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PMPA3.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PFO2HxA1.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PFO2HxA1.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PFO3OA0.27 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PFO3OA0.26 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PFO5DA0.25 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PFO5DA0.27 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PEPA1.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-OLDOF-TR1-1-02021902/02/2019 320-51031-1 PEPA1.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLPage 103 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 Byproduct 60.016 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 R-EVE0.21 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 R-EVE0.23 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 Byproduct 40.35 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 Byproduct 40.35 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-OLDOF-5K-02021902/02/2019 9979947PFMOAA18 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PFMOAA16 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PFMOAA16.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 EVE Acid0.031 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 EVE Acid0.033 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-OLDOF-5K-02021902/02/2019 9979947PFESA-BP20.54 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PFESA-BP20.50 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PFESA-BP20.51 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 Hydro-EVE Acid0.20 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 Hydro-EVE Acid0.21 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-5K-02021902/02/2019 9979947PEPA1.9 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLPage 104 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PEPA1.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PEPA1.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-OLDOF-5K-02021902/02/2019 9979947PFO2HxA6.6 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PFO2HxA5.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PFO2HxA5.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-5K-02021902/02/2019 9979947PFO3OA1.7 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PFO3OA1.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PFO3OA1.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-5K-02021902/02/2019 9979947PFO4DA1.7 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PFO4DA1.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PFO4DA1.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-OLDOF-5K-02021902/02/2019 9979947PFO5DA0.59 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PFO5DA0.58 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PFO5DA0.58 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-OLDOF-5K-02021902/02/2019 9979947PMPA5.4 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PMPA4.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 PMPA4.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLPage 105 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 NVHOS0.21 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-OLDOF-5K-02021902/02/2019 320-51024-2 NVHOS0.21 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 R-EVE0.31 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 R-EVE0.31 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 Byproduct 40.80 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 Byproduct 40.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 Byproduct 53.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 Byproduct 53.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 Byproduct 60.032 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 Byproduct 60.033 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-OLDOF-5-02021902/02/2019 9979943PFMOAA190 ug/LCl. Spec. Table 3Compound SOPJ0.50PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PFMOAA200 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PFMOAA200.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 EVE Acid0.37 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 EVE Acid0.37 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-OLDOF-5-02021902/02/2019 9979943PFESA-BP20.99 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PFESA-BP20.99 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLPage 106 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PFESA-BP20.99 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 Hydro-EVE Acid0.55 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 Hydro-EVE Acid0.53 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-5-02021902/02/2019 9979943PFO2HxA43 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PFO2HxA37 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PFO2HxA36.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-5-02021902/02/2019 9979943PFO3OA14 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PFO3OA11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PFO3OA10.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-5-02021902/02/2019 9979943PFO4DA5.2 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PFO4DA4.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PFO4DA4.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-OLDOF-5-02021902/02/2019 9979943PEPA2.7 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PEPA2.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PEPA2.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-OLDOF-5-02021902/02/2019 9979943PFESA-BP14.6 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PFESA-BP13.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLPage 107 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PFESA-BP13.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-OLDOF-5-02021902/02/2019 9979943PMPA8.6 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PMPA8.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 PMPA8.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 NVHOS1.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 NVHOS1.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 NVHOS1.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-OLDOF-5-02021902/02/2019 320-51024-1 NVHOS1.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-OLDOF-4-02021902/02/2019 9979935PFESA-BP20.48 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PFESA-BP20.47 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PFESA-BP20.48 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 Hydro-EVE Acid0.31 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 Hydro-EVE Acid0.31 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 R-EVE0.24 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 R-EVE0.24 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 Byproduct 40.62 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 Byproduct 40.65 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLPage 108 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 Byproduct 51.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 Byproduct 51.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 Byproduct 60.019 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 Byproduct 60.017 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-OLDOF-4-02021902/02/2019 9979935PFMOAA140 ug/LCl. Spec. Table 3Compound SOPJ0.50PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PFMOAA140 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PFMOAA140.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-4-02021902/02/2019 9979935PMPA7.3 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PMPA7.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PMPA6.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-OLDOF-4-02021902/02/2019 9979935PFO2HxA31 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PFO2HxA25 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PFO2HxA24.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-4-02021902/02/2019 9979935PEPA2.4 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PEPA2.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PEPA2.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-OLDOF-4-02021902/02/2019 9979935PFESA-BP10.23 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLPage 109 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PFESA-BP10.24 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 PFESA-BP10.25 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-OLDOF-3-02021902/02/2019 9979931PFESA-BP20.40 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PFESA-BP20.42 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PFESA-BP20.43 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 Hydro-EVE Acid0.24 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 Hydro-EVE Acid0.26 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 NVHOS1.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-OLDOF-4-02021902/02/2019 320-51031-5 NVHOS1.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 R-EVE0.22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 R-EVE0.23 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 Byproduct 40.56 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 Byproduct 40.57 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 Byproduct 51.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 Byproduct 51.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 Byproduct 60.018 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 Byproduct 60.019 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLPage 110 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-3-02021902/02/2019 9979931PFMOAA110 ug/LCl. Spec. Table 3Compound SOPJ0.50PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PFMOAA109 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PFMOAA110.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-3-02021902/02/2019 9979931PMPA6.6 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PMPA6.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PMPA6.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-OLDOF-3-02021902/02/2019 9979931PFO2HxA25 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PFO2HxA23 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PFO2HxA24.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-3-02021902/02/2019 9979931PFO3OA7.4 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PFO3OA5.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PFO3OA5.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-3-02021902/02/2019 9979931PFO5DA0.85 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PFO5DA0.79 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PFO5DA0.88 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-OLDOF-3-02021902/02/2019 9979931PEPA2.2 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PEPA2.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLPage 111 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PEPA2.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-OLDOF-3-02021902/02/2019 9979931PFESA-BP10.10 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PFESA-BP10.17 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-OLDOF-3-02021902/02/2019 320-51031-4 PFESA-BP10.17 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-OLDOF-2L-02021902/02/2019 9979927PFMOAA99 ug/LCl. Spec. Table 3Compound SOPJ0.50PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PFMOAA104 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PFMOAA100.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 R-EVE0.19 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 R-EVE0.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 Byproduct 40.49 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 Byproduct 40.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 Byproduct 51.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 Byproduct 51.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PFESA-BP20.36 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 Hydro-EVE Acid0.22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 Hydro-EVE Acid0.22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PEPA2.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLPage 112 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-2L-02021902/02/2019 9979927PFO3OA6.9 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PFO3OA5.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PFO3OA5.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-1-02011902/01/2019 9978962PFO2HxA21 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PFO2HxA17 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PFO2HxA18.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-1-02011902/01/2019 9978962PFO3OA6.4 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PFO3OA5.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PFO3OA5.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-1-02011902/01/2019 9978962PFO4DA1.7 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PFO4DA1.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PFO4DA1.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-OLDOF-1-02011902/01/2019 9978962PEPA1.9 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PEPA1.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PEPA2.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-OLDOF-1-02011902/01/2019 9978962PFESA-BP10.26 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PFESA-BP10.19 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLPage 113 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PFESA-BP10.21 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-OLDOF-1-02011902/01/2019 9978962PMPA5.6 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PMPA5.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PMPA6.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 NVHOS0.75 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 NVHOS0.77 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PFMOAA0.055 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PFMOAA0.055 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PMPA0.031 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PMPA0.032 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 NVHOS0.0029 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 NVHOS0.0029 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PFO2HxA0.017 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PFO2HxA0.018 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PFO3OA0.0036 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-84-02041902/04/2019 320-51024-4 PFO3OA0.0039 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PFO2HxA0.0020 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 114 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PFO2HxA0.002 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PMPA0.011 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 PMPA0.011 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 NVHOS0.0022 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-02041902/04/2019 320-51024-3 NVHOS0.0021 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 R-EVE0.19 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 R-EVE0.19 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 Byproduct 40.45 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 Byproduct 40.46 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 Byproduct 51.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 Byproduct 51.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-1-02011902/01/2019 9978962PFMOAA83 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PFMOAA93 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PFMOAA94.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-2-02011902/01/2019 9978966PEPA1.9 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PEPA2.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PEPA2.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLPage 115 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-2-02011902/01/2019 9978966PFESA-BP10.18 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PFESA-BP10.14 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PFESA-BP10.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-OLDOF-1-02011902/01/2019 9978962PFESA-BP20.30 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PFESA-BP20.31 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 PFESA-BP20.31 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 Hydro-EVE Acid0.20 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-1-02011902/01/2019 320-51031-7 Hydro-EVE Acid0.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 R-EVE0.19 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 R-EVE0.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 Byproduct 40.42 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 Byproduct 40.43 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 Byproduct 51.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 Byproduct 51.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-2-02011902/01/2019 9978966PFESA-BP20.33 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PFESA-BP20.34 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PFESA-BP20.34 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLPage 116 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-2-02011902/01/2019 9978966PMPA5.8 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PMPA6.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PMPA5.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-OLDOF-2-02011902/01/2019 9978966PFO2HxA22 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PFO2HxA18 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PFO2HxA18.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-2-02011902/01/2019 9978966PFO3OA6.4 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PFO3OA5.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PFO3OA5.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-2-02011902/01/2019 9978966PFO4DA1.8 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PFO4DA1.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PFO4DA1.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-OLDOF-2-02011902/01/2019 9978966PFMOAA83 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PFMOAA92 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 PFMOAA90.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-2L-02021902/02/2019 9979927PMPA6.2 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PMPA6.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLPage 117 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PMPA6.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 NVHOS0.89 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 NVHOS0.85 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 R-EVE0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 R-EVE0.13 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 Byproduct 40.18 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PFESA-BP20.071 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PFESA-BP20.07 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-OLDOF-2J-02021902/02/2019 9979923PFMOAA0.63 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PFMOAA0.49 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PFMOAA0.49 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-2J-02021902/02/2019 9979923PEPA1.4 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PEPA1.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PEPA1.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-OLDOF-2J-02021902/02/2019 9979923PMPA3.7 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PMPA3.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLPage 118 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PMPA3.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-OLDOF-2J-02021902/02/2019 9979923PFO2HxA1.7 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PFO2HxA1.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PFO2HxA1.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-2J-02021902/02/2019 9979923PFO3OA0.40 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PFO3OA0.29 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-2J-02021902/02/2019 320-51031-3 PFO3OA0.27 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 Hydro-EVE Acid0.20 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 Hydro-EVE Acid0.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 NVHOS0.80 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-OLDOF-2-02011902/01/2019 320-51031-8 NVHOS0.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFB-02051902/05/2019 320-51045-11 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFB-02051902/05/2019 320-51045-11 Byproduct 50.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-4-02061902/06/2019 9981755PMPA120 UG/LCl. Spec. Table 3Compound SOPJ0.50PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PMPA111 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PMPA110.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 NVHOS13 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLPage 119 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 NVHOS13.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-B-4-02061902/06/2019 9981755PEPA60 UG/LCl. Spec. Table 3Compound SOPJ0.50PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PEPA61 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PEPA61.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-B-4-02061902/06/2019 9981755PFESA-BP169 UG/LCl. Spec. Table 3Compound SOPJ0.50PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PFESA-BP151 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PFESA-BP151.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 R-EVE0.64 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 R-EVE0.63 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 Byproduct 40.73 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 Byproduct 40.72 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 9981751PFESA-BP20.25 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PFESA-BP20.30 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PFESA-BP20.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 Hydro-EVE Acid0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 Hydro-EVE Acid0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 9981751PFO2HxA5.4 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLPage 120 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PFO2HxA5.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PFO2HxA5.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 9981751PFO3OA0.98 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PFO3OA1.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PFO3OA1.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 9981751PFO4DA0.99 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PFO4DA1.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PFO4DA1.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 9981751PFO5DA0.39 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PFO5DA0.61 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PFO5DA0.62 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 9981751PFMOAA1.6 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PFMOAA1.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PFMOAA1.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 9981751PMPA13 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PMPA16 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PMPA16.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLPage 121 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-3-E4-02061902/06/2019 9981751PEPA4.8 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PEPA6.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 PEPA6.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-B-3-02061902/06/2019 9981743PFMOAA5.0 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PFMOAA5.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PFMOAA4.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 EVE Acid34 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 EVE Acid33.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-B-3-02061902/06/2019 9981743PFESA-BP23.5 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PFESA-BP23.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PFESA-BP23.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 Hydro-EVE Acid9.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 Hydro-EVE Acid8.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 Byproduct 414 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 Byproduct 413.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 Byproduct 599 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 Byproduct 593.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 122 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 Byproduct 60.28 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 Byproduct 60.27 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 NVHOS8.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 NVHOS8.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 9981747PFESA-BP131 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PFESA-BP130 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PFESA-BP131.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 9981747PFO2HxA18 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PFO2HxA17 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PFO2HxA17.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 9981747PFO3OA3.7 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PFO3OA3.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PFO3OA3.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 9981747PFO4DA2.9 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PFO4DA2.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PFO4DA2.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 9981747PFO5DA1.9 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLPage 123 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PFO5DA1.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PFO5DA1.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 N-ethylperfluoro-1-octanesulfonamide0.042 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 9981747PFMOAA4.8 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PFMOAA5.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PFMOAA5.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 9981747PFESA-BP24.1 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PFESA-BP24.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PFESA-BP25.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 Hydro-EVE Acid11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 Hydro-EVE Acid11.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 R-EVE13 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 R-EVE13.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 Byproduct 416 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 Byproduct 416.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 Byproduct 5119 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 124 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 Byproduct 5120.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 Byproduct 60.34 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 Byproduct 60.36 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 NVHOS0.075 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 320-51045-8 NVHOS0.076 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 R-EVE3.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 R-EVE3.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 Byproduct 44.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 Byproduct 44.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 Byproduct 538 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 Byproduct 537.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 Byproduct 60.084 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 Byproduct 60.081 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 Hydro-EVE Acid2.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 Hydro-EVE Acid2.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-B-1-02051902/05/2019 9980820PMPA38 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PMPA42 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLPage 125 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PMPA40.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-B-1-02051902/05/2019 9980820PFMOAA150 ug/LCl. Spec. Table 3Compound SOPJ0.50PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PFMOAA148 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PFMOAA140.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 EVE Acid6.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 EVE Acid5.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-B-1-02051902/05/2019 9980820PFESA-BP21.1 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PFESA-BP21.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PFESA-BP21.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-B-1-02051902/05/2019 9980820PFO2HxA43 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PFO2HxA43 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PFO2HxA42.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-B-1-02051902/05/2019 9980820PFO3OA11 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PFO3OA9.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PFO3OA9.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-1-02051902/05/2019 9980820PFO4DA2.0 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PFO4DA1.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLPage 126 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PFO4DA1.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-B-1-02051902/05/2019 9980820PFO5DA0.46 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PFO5DA0.53 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PFO5DA0.54 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-B-1-02051902/05/2019 9980820PEPA15 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PEPA17 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PEPA17.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-B-1-02051902/05/2019 9980820PFESA-BP14.6 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PFESA-BP13.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 PFESA-BP13.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 R-EVE5.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 R-EVE5.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 Byproduct 48.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 Byproduct 48.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 Byproduct 584 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 Byproduct 583.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 Byproduct 60.20 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLPage 127 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 Byproduct 60.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 NVHOS3.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-B-1-02051902/05/2019 320-51045-1 NVHOS3.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-A-9-02071902/07/2019 9982628PFESA-BP25.6 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PFESA-BP26.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PFESA-BP26.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 Hydro-EVE Acid8.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 Hydro-EVE Acid8.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-B-2-02051902/05/2019 9980824PFMOAA9.2 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PFMOAA8.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PFMOAA8.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 EVE Acid24 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 EVE Acid25.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-B-2-02051902/05/2019 9980824PFESA-BP23.2 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PFESA-BP23.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PFESA-BP23.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 Hydro-EVE Acid7.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLPage 128 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 Hydro-EVE Acid7.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-B-2-02051902/05/2019 9980824PFO2HxA19 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PFO2HxA16 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PFO2HxA16.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-B-2-02051902/05/2019 9980824PFO3OA4.5 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PFO3OA3.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PFO3OA3.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-2-02051902/05/2019 9980824PFO4DA2.8 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PFO4DA2.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PFO4DA2.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-B-2-02051902/05/2019 9980824PFO5DA1.3 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PFO5DA1.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PFO5DA1.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-B-2-02051902/05/2019 9980824PEPA34 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PEPA32 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PEPA33.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-B-2-02051902/05/2019 9980824PFESA-BP119 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLPage 129 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PFESA-BP114 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PFESA-BP114.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 NVHOS6.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 NVHOS6.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-B-2-02051902/05/2019 9980824PMPA66 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PMPA61 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 PMPA63.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-B-3-02061902/06/2019 9981743PMPA66 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PMPA72 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PMPA69.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 R-EVE9.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 R-EVE10.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 Byproduct 411 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 Byproduct 412.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 Byproduct 577 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 Byproduct 583.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 Byproduct 60.23 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLPage 130 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-2-02051902/05/2019 320-51045-2 Byproduct 60.23 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 NVHOS7.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 NVHOS7.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-B-3-02061902/06/2019 9981743PFO2HxA17 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PFO2HxA16 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PFO2HxA15.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-B-3-02061902/06/2019 9981743PFO3OA3.8 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PFO3OA3.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PFO3OA3.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-3-02061902/06/2019 9981743PFO4DA2.7 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PFO4DA2.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PFO4DA2.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-B-3-02061902/06/2019 9981743PFO5DA1.7 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PFO5DA1.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PFO5DA1.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-B-3-02061902/06/2019 9981743PEPA35 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PEPA38 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLPage 131 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PEPA37.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-B-3-02061902/06/2019 9981743PFESA-BP123 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PFESA-BP122 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-B-3-02061902/06/2019 320-51045-3 PFESA-BP121.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 Byproduct 50.091 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 Byproduct 50.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-WC-1-020719 02/07/2019 9982644PFO2HxA0.31 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PFO2HxA0.33 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PFO2HxA0.34 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-WC-1-020719 02/07/2019 9982644PFO3OA0.052 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PFO3OA0.062 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-WC-1-020719 02/07/2019 9982644PMPA0.44 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PMPA1.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-WC-1-020719 02/07/2019 320-51045-25 PMPA1.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 R-EVE0.99 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 R-EVE1.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLPage 132 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 Byproduct 60.017 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 Byproduct 60.018 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 9980836PFESA-BP20.26 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PFESA-BP20.25 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PFESA-BP20.27 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 Hydro-EVE Acid0.58 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 Hydro-EVE Acid0.58 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 9980836PFMOAA180 ug/LCl. Spec. Table 3Compound SOPJ0.50PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PFMOAA164 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PFMOAA170.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 9980836PEPA4.6 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PEPA4.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PEPA4.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 9980836PFO2HxA46 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PFO2HxA40 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PFO2HxA42.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 9980836PFO3OA13 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLPage 133 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PFO3OA9.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PFO3OA9.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 9980836PFO4DA2.6 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PFO4DA2.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PFO4DA2.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PFO5DA0.092 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PFO5DA0.082 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 Hydro-EVE Acid2.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.056PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 Hydro-EVE Acid2.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.056PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 9980836PMPA14 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PMPA12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 PMPA13.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 NVHOS1.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 320-51045-5 NVHOS1.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980828PFO2HxA62 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980832PFO2HxA62 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PFO2HxA64 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLPage 134 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PFO2HxA62.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980828PFO3OA21 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980832PFO3OA22 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PFO3OA20 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PFO3OA20.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980828PFO4DA4.5 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980832PFO4DA4.4 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PFO4DA4.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PFO4DA4.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PFO5DA0.089 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.067PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PFO5DA0.09 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.067PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980828PMPA16 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980832PMPA15 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PMPA16 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep1.1PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PMPA15.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep1.1PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 NVHOS2.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 NVHOS1.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.11PQLPage 135 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 R-EVE1.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.14PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 R-EVE1.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.14PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 Byproduct 41.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.32PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 Byproduct 41.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.32PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 Byproduct 53.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 Byproduct 52.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PFESA-BP20.59 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.061PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980828PEPA4.7 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980832PEPA4.7 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PEPA5.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.093PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PEPA4.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.093PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980828PFMOAA200 ug/LCl. Spec. Table 3Compound SOPJ0.50PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980832PFMOAA200 ug/LCl. Spec. Table 3Compound SOPJ0.50PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PFMOAA196 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.42PQLFAY-SW-SEEP-C-1-02051902/05/2019 320-51045-4 PFMOAA190.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.42PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 9981759PFMOAA4.9 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PFMOAA5.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLPage 136 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PFMOAA5.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 EVE Acid64 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 EVE Acid62.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 9981759PFESA-BP24.0 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PFESA-BP24.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PFESA-BP24.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 Hydro-EVE Acid9.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 Hydro-EVE Acid8.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 R-EVE16 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 R-EVE16.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 Byproduct 418 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 Byproduct 417.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 Byproduct 596 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 Byproduct 589.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 Byproduct 60.29 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 Byproduct 60.28 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 9981759PFO2HxA18 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLPage 137 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PFO2HxA17 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PFO2HxA17.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 9981759PFO3OA4.9 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PFO3OA4.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PFO3OA3.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 9981759PFO4DA3.7 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PFO4DA3.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PFO4DA3.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 9981759PFO5DA2.8 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PFO5DA2.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PFO5DA2.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 9981759PEPA33 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PEPA36 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PEPA35.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 9981759PFESA-BP142 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PFESA-BP140 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PFESA-BP137.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLPage 138 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-4-02061902/06/2019 9981755PFMOAA6.7 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PFMOAA6.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PFMOAA6.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-B-4-02061902/06/2019 9981755PFESA-BP26.2 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PFESA-BP26.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PFESA-BP26.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 Hydro-EVE Acid16 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 Hydro-EVE Acid16.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-B-4-02061902/06/2019 9981755PFO2HxA24 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PFO2HxA22 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PFO2HxA22.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-B-4-02061902/06/2019 9981755PFO3OA5.0 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PFO3OA4.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PFO3OA4.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-4-02061902/06/2019 9981755PFO4DA3.8 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PFO4DA3.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PFO4DA3.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLPage 139 of 150
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-4-02061902/06/2019 9981755PFO5DA2.6 ug/LCl. Spec. Table 3Compound SOPJ0.10PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PFO5DA2.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 PFO5DA2.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 9981759PMPA66 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PMPA71 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 PMPA69.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 R-EVE21 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 R-EVE21.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 Byproduct 424 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 Byproduct 423.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 Byproduct 5171 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 Byproduct 5170.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 Byproduct 60.50 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 Byproduct 60.51 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 NVHOS6.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 320-51045-10 NVHOS6.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLPage 140 of 150
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-8-02071902/07/2019 9982576Total Dissolved Solids113 MG/L20.02540 C-1997J60.0MDLFAY-SW-SEEP-A-2-02071902/07/2019 9982570Total Dissolved Solids88.0 MG/L20.02540 C-1997J60.0MDLPage 141 of 150
Associated LCS and/or LCSD analysis had relative percent recovery (RPR) values less than the lower control limit. The reported result may be biasedlow.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-8-02071902/07/2019 9982621Hfpo Dimer Acid13 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.9PQLFAY-SW-SEEP-A-7-02071902/07/2019 9982617Hfpo Dimer Acid28 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.7PQLFAY-SW-SEEP-A-6-02071902/07/2019 9982613Hfpo Dimer Acid18 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.7PQLFAY-SW-SEEP-A-5-02071902/07/2019 9982609Hfpo Dimer Acid18 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.8PQLFAY-SW-SEEP-A-4-02071902/07/2019 9982605Hfpo Dimer Acid17 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.8PQLFAY-SW-SEEP-A-2-02071902/07/2019 9982597Hfpo Dimer Acid27 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.8PQLFAY-SW-SEEP-A-12-02071902/07/2019 9982637Hfpo Dimer Acid20 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.8PQLFAY-SW-SEEP-A-11-02071902/07/2019 9982633Hfpo Dimer Acid55 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.7PQLFAY-SW-SEEP-A-10-02071902/07/2019 9982629Hfpo Dimer Acid61 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.8PQLFB-02071902/07/2019 9982661Hfpo Dimer Acid0.0022 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep0.0018PQLFAY-SW-SEEP-B-4-02061902/06/2019 9981752Hfpo Dimer Acid82 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.8PQLFAY-SW-SEEP-B-3-E4-02061902/06/2019 9981748Hfpo Dimer Acid10 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.9PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 9981744Hfpo Dimer Acid58 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.8PQLFAY-SW-SEEP-B-1-02051902/05/2019 9980817Hfpo Dimer Acid24 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.8PQLFAY-SW-SEEP-A-9-02071902/07/2019 9982625Hfpo Dimer Acid57 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.8PQLFAY-SW-SEEP-B-2-02051902/05/2019 9980821Hfpo Dimer Acid38 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.8PQLFAY-SW-SEEP-B-3-02061902/06/2019 9981740Hfpo Dimer Acid40 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.7PQLFAY-SW-WC-5-020719 02/07/2019 9982657Hfpo Dimer Acid0.033 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep0.0017PQLFAY-SW-WC-4-020719 02/07/2019 9982653Hfpo Dimer Acid0.051 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep0.0017PQLFAY-SW-WC-2-020719 02/07/2019 9982645Hfpo Dimer Acid0.13 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep0.0017PQLFAY-SW-SEEP-C-1-E2-02051902/05/2019 9980833Hfpo Dimer Acid17 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.8PQLFAY-SW-SEEP-C-1-02051902/05/2019 9980825Hfpo Dimer Acid27 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.8PQLPage 142 of 150
Associated LCS and/or LCSD analysis had relative percent recovery (RPR) values less than the lower control limit. The reported result may be biasedlow.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-C-1-02051902/05/2019 9980829Hfpo Dimer Acid27 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.7PQLFAY-SW-SEEP-B-4-A3-02061902/06/2019 9981756Hfpo Dimer Acid32 UG/LEPA 537 Rev.1.1 modifiedJ537_Prep1.9PQLPage 143 of 150
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit but above the rejection limit. Thereported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-9-02071902/07/2019 9982628PFO2HxA58 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PFO2HxA63 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PFO2HxA63.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-A-9-02071902/07/2019 9982628PFESA-BP146 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PFESA-BP143 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PFESA-BP143.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 R-EVE0.87 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 R-EVE0.96 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 Byproduct 41.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 Byproduct 41.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 Byproduct 56.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 Byproduct 57.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-6-02071902/07/2019 9982616PFMOAA15 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PFMOAA17 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PFMOAA18.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-A-6-02071902/07/2019 9982616PFO2HxA18 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLPage 144 of 150
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit but above the rejection limit. Thereported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PFO2HxA20 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PFO2HxA21.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-A-6-02071902/07/2019 9982616PMPA29 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PMPA38 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-A-6-02071902/07/2019 320-51045-18 PMPA39.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-A-12-02071902/07/2019 9982580Chloride7.0 MG/L1.0300.0J2.0MDLFAY-SW-SEEP-A-11-02071902/07/2019 9982579Chloride9.6 MG/L1.0300.0J2.0MDLFAY-SW-OLDOF-4-02041902/04/2019 9979903Chloride9.1 MG/L1.0300.0J2.0MDLFAY-SW-OLDOF-2L-02021902/02/2019 9979927PFO2HxA23 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PFO2HxA21 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-2L-02021902/02/2019 320-51031-2 PFO2HxA21.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-2J-02041902/04/2019 9979895Chloride3.6 MG/L1.0300.0J2.0MDLFAY-SW-SEEP-B-3-A1-02061902/06/2019 9981747PMPA70 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PMPA79 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PMPA80.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 9981747PEPA36 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PEPA42 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 PEPA43.0 UG/LCl. Spec. Table 3CompoundJPFAS_DI_Prep0.047PQLPage 145 of 150
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit but above the rejection limit. Thereported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 EVE Acid46 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-B-3-A1-02061902/06/2019 320-51045-7 EVE Acid46.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-A-9-02071902/07/2019 9982577Chloride8.8 MG/L1.0300.0J2.0MDLFAY-SW-SEEP-A-9-02071902/07/2019 9982628PMPA47 UG/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PMPA50 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PMPA50.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-A-9-02071902/07/2019 9982628PFMOAA73 ug/LCl. Spec. Table 3Compound SOPJ0.050PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PFMOAA75 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 PFMOAA76.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 EVE Acid22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-A-9-02071902/07/2019 320-51045-21 EVE Acid22.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-WC-5-020719 02/07/2019 9982587Chloride10.7 MG/L1.0300.0J2.0MDLFAY-SW-WC-4-020719 02/07/2019 9982586Chloride10.2 MG/L1.0300.0J2.0MDLFAY-SW-WC-3-020719 02/07/2019 9982585Chloride9.9 MG/L1.0300.0J2.0MDLFAY-SW-WC-2-020719 02/07/2019 9982584Chloride9.8 MG/L1.0300.0J2.0MDLFAY-SW-WC-1-020719 02/07/2019 9982583Nitrate0.89 MG/L0.25300.0J0.50MDLFAY-SW-SEEP-C-1-A-02051902/05/2019 9980787Chloride11.3 MG/L1.0300.0J2.0MDLFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 EVE Acid75 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLPage 146 of 150
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit but above the rejection limit. Thereported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-4-02061902/06/2019 320-51045-9 EVE Acid75.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-A-10-02071902/07/2019 9982578Nitrate0.48 MG/L0.25300.0J0.50MDLPage 147 of 150
The result is estimated since the concentration is between the method detection limit and practical quantitation limit.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-4-02061902/06/2019 9981702Total Dissolved Solids50.0 MG/L20.02540 C-1997J60.0MDLFAY-SW-SEEP-B-4-A3-02061902/06/2019 9981703Alkalinity, Total2.4 MG/L1.72320 B-1997J5MDLFAY-SW-SEEP-C-1-02051902/05/2019 9980788Ammonia0.088 MG/L0.050350.1J0.10MDLFAY-SW-SEEP-B-4-A3-02061902/06/2019 9981703Total Dissolved Solids57.5 MG/L20.02540 C-1997J60.0MDLFAY-SW-SEEP-C-1-020519-D02/05/2019 9980792Ammonia0.088 MG/L0.050350.1J0.10MDLFAY-SW-SEEP-C-1-E2-02051902/05/2019 9980793Total Dissolved Solids52.5 MG/L20.02540 C-1997J60.0MDLFAY-SW-WC-1-020719 02/07/2019 9982583Total Dissolved Solids56.5 MG/L20.02540 C-1997J60.0MDLFAY-SW-WC-1-020719 02/07/2019 9982583Ammonia0.085 MG/L0.050350.1J0.10MDLFAY-SW-WC-2-020719 02/07/2019 9982584Ammonia0.062 MG/L0.050350.1J0.10MDLFAY-SW-WC-2-020719 02/07/2019 9982584Total Dissolved Solids46.5 MG/L20.02540 C-1997J60.0MDLFAY-SW-WC-4-020719 02/07/2019 9982586Ammonia0.060 MG/L0.050350.1J0.10MDLFAY-SW-WC-3-020719 02/07/2019 9982585Ammonia0.059 MG/L0.050350.1J0.10MDLFAY-SW-WC-5-020719 02/07/2019 9982587Manganese0.0184 MG/L0.0011200.7 Rev. 4.4J200.70.0200MDLFAY-SW-WC-5-020719 02/07/2019 9982587Ammonia0.058 MG/L0.050350.1J0.10MDLFAY-SW-WC-4-020719 02/07/2019 9982586Total Dissolved Solids50.0 MG/L20.02540 C-1997J60.0MDLFAY-SW-WC-3-020719 02/07/2019 9982585Total Dissolved Solids53.5 MG/L20.02540 C-1997J60.0MDLFAY-SW-SEEP-B-2-02051902/05/2019 9980785Total Dissolved Solids49.0 MG/L20.02540 C-1997J60.0MDLFAY-SW-SEEP-A-9-02071902/07/2019 9982577Manganese0.0114 MG/L0.0011200.7 Rev. 4.4J200.70.0200MDLFAY-SW-SEEP-B-1-02051902/05/2019 9980784Ammonia0.079 MG/L0.050350.1J0.10MDLFAY-SW-SEEP-B-3-A1-02061902/06/2019 9981698Total Dissolved Solids42.5 MG/L20.02540 C-1997J60.0MDLFAY-SW-SEEP-B-3-02061902/06/2019 9981695Total Dissolved Solids44.5 MG/L20.02540 C-1997J60.0MDLFB-02011902/01/2019 9978958Chloride0.23 MG/L0.20300.0J0.40MDLFB-02051902/05/2019 9980794Calcium0.0711 MG/L0.0330200.7 Rev. 4.4J200.70.500MDLPage 148 of 150
The result is estimated since the concentration is between the method detection limit and practical quantitation limit.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFB-02021902/02/2019 9979906Magnesium0.0328 MG/L0.0190200.7 Rev. 4.4J200.70.100MDLFB-02021902/02/2019 9979906Calcium0.0871 MG/L0.0330200.7 Rev. 4.4J200.70.500MDLFB-02071902/07/2019 9982590Sodium0.426 MG/L0.326200.7 Rev. 4.4J200.71.00MDLFB-02071902/07/2019 9982590Calcium0.0542 MG/L0.0330200.7 Rev. 4.4J200.70.500MDLFAY-SW-WC-5-020719 02/07/2019 9982587Total Dissolved Solids47.5 MG/L20.02540 C-1997J60.0MDLFB-02061902/06/2019 9981706Selenium0.0250 MG/L0.02106010BJ3005A0.0500MDLFB-02061902/06/2019 9987495Sodium0.374 MG/L0.326200.7 Rev. 4.4J200.71.00MDLFB-02061902/06/2019 9987495Calcium0.0817 MG/L0.0330200.7 Rev. 4.4J200.70.500MDLFAY-SW-OLDOF-2J-02041902/04/2019 9979895Manganese0.0783 MG/L0.0055200.7 Rev. 4.4J200.70.100MDLFAY-SW-OLDOF-2J-02041902/04/2019 9979895Sodium2.34 MG/L1.63200.7 Rev. 4.4J200.75.00MDLFAY-SW-OLDOF-2J-02041902/04/2019 9979895Calcium1.41 MG/L0.165200.7 Rev. 4.4J200.72.50MDLFAY-SW-OLDOF-2J-02041902/04/2019 9979895Ammonia0.076 MG/L0.050350.1J0.10MDLFAY-SW-OLDOF-2L-02041902/04/2019 9979897Nitrate0.44 MG/L0.25300.0J0.50MDLFAY-SW-OLDOF-2L-02041902/04/2019 9979897Ammonia0.060 MG/L0.050350.1J0.10MDLFAY-SW-OLDOF-3-02041902/04/2019 9979901Nitrate0.41 MG/L0.25300.0J0.50MDLFAY-SW-OLDOF-3-02041902/04/2019 9979901Ammonia0.052 MG/L0.050350.1J0.10MDLFAY-SW-OLDOF-4-02041902/04/2019 9979903Ammonia0.055 MG/L0.050350.1J0.10MDLFAY-SW-OLDOF-4-02021902/02/2019 9979902Total Organic Carbon0.98 MG/L0.505310 C-2000J1.0MDLFAY-SW-OLDOF-5K-02041902/04/2019 9979913Aluminum0.227 MG/L0.153200.7 Rev. 4.4J200.70.300MDLFAY-SW-OLDOF-TR-1-1-02021902/02/2019 9979892Total SuspendedSolids2.69 MG/L1.002540 D-1997J3.00MDLFAY-SW-OLDOF-TR-1-1-02041902/04/2019 9979893Ammonia0.065 MG/L0.050350.1J0.10MDLFAY-SW-SEEP-A-1-02071902/07/2019 9987515Nickel0.0040 MG/L0.00316010BJ3005A0.0100MDLFAY-SW-SEEP-A-1-02071902/07/2019 9987515Zinc0.0181 MG/L0.00306010BJ3005A0.0200MDLPage 149 of 150
The result is estimated since the concentration is between the method detection limit and practical quantitation limit.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingSURFACE WATER 02/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-10-02071902/07/2019 9982578Manganese0.0095 MG/L0.0011200.7 Rev. 4.4J200.70.0200MDLFAY-SW-SEEP-A-11-02071902/07/2019 9982579Manganese0.0162 MG/L0.0011200.7 Rev. 4.4J200.70.0200MDLFAY-SW-SEEP-A-11-02071902/07/2019 9987516Zinc0.0173 MG/L0.00306010BJ3005A0.0200MDLFAY-SW-SEEP-A-11-02071902/07/2019 9982579Ammonia0.061 MG/L0.050350.1J0.10MDLFAY-SW-SEEP-A-12-02071902/07/2019 9982580Manganese0.0157 MG/L0.0011200.7 Rev. 4.4J200.70.0200MDLFAY-SW-SEEP-A-12-02071902/07/2019 9982580Total Dissolved Solids48.5 MG/L20.02540 C-1997J60.0MDLFAY-SW-SEEP-A-4-02071902/07/2019 9982572Ammonia0.087 MG/L0.050350.1J0.10MDLFAY-SW-SEEP-A-4-02071902/07/2019 9982572Total Dissolved Solids58.0 MG/L20.02540 C-1997J60.0MDLFAY-SW-SEEP-A-5-02071902/07/2019 9982573Total Dissolved Solids44.0 MG/L20.02540 C-1997J60.0MDLFAY-SW-SEEP-A-6-02071902/07/2019 9982574Total Dissolved Solids39.5 MG/L20.02540 C-1997J60.0MDLFAY-SW-SEEP-A-7-02071902/07/2019 9982575Total Dissolved Solids57.0 MG/L20.02540 C-1997J60.0MDLFAY-SW-SEEP-A-8-02071902/07/2019 9982576Ammonia0.056 MG/L0.050350.1J0.10MDLPage 150 of 150
ADQM Data Review Narrative - FAY Creeks Seeps Old Outfall 002 FI 519.doc 1 of 3
ADQM DATA REVIEW NARRATIVE
Site Chemours FAY – Fayetteville Project Creeks Seeps Old Outfall 002 FI 5/19 Project Reviewer Michael Aucoin, AECOM as a Chemours contractor Sampling Dates May 20-24, May 29-30, June 7, 2019 Analytical Protocol Laboratory Analytical Method Parameter(s)
TestAmerica - Sacramento 537 Modified PFAS1
TestAmerica - Sacramento Cl. Spec. Table 3 Compound SOP Table 3+ compounds
TestAmerica - Sacramento EPA 300 Fluoride
1 Perfluoroalkylsubstances including HFPO-DA. Sample Receipt The following items are noted for this data set:
• All samples were received in satisfactory condition and within EPA temperature guidelines on May 22-24, May 29-30, June 1, and June 11, 2019.
Data Review The electronic data submitted for this project was reviewed via the Data Verification Module (DVM)
process. Overall the data is acceptable for use without qualification, except as noted below:

• PFO5DA results in some field samples were qualified B and may be biased high, or may be false positives, due to a comparable concentration in the associated field blank.
• Table 3+ sample results were qualified J as estimated, and non-detect results were qualified UJ, and the reporting limit may be biased low, because the lab established holding time was exceeded.
• Several analytical results have been qualified J as estimated, and non-detect results qualified UJ indicating an estimated reporting limit, due to matrix spike recovery outside criteria, and; poor field duplicate, lab replicate, or LCSD precision. Fluoride sample results between the MDL and PQL were qualified J as estimated. See the Data Verification Module (DVM) Narrative Report for which samples were qualified, the specific reasons for qualification, and potential bias in reported results.
ADQM Data Review Narrative - FAY Creeks Seeps Old Outfall 002 FI 519.doc 2 of 3
Attachments The DVM Narrative report is attached. The lab reports due to a large page count are stored on an AECOM network shared drive and are available to be posted on external shared drives, or on a flash drive.

ADQM Data Review Narrative - FAY Creeks Seeps Old Outfall 002 FI 519.doc 3 of 3
Data Verification Module (DVM)
The DVM is an internal review process used by the ADQM group to assist with the determination of data usability. The electronic data deliverables received from the laboratory are loaded into the Locus EIM™ database and processed through a series of data quality checks, which are a combination of software (Locus EIM™ database Data Verification Module (DVM)) and manual reviewer evaluations. The data is evaluated against the following data usability checks:
• Field and laboratory blank contamination
• US EPA hold time criteria
• Missing Quality Control (QC) samples
• Matrix spike(MS)/matrix spike duplicate (MSD) recoveries and the relative percent differences
(RPDs) between these spikes
• Laboratory control sample(LCS)/control sample duplicate (LCSD) recoveries and the RPD
between these spikes
• Surrogate spike recoveries for organic analyses
• RPD between field duplicate sample pairs
• RPD between laboratory replicates for inorganic analyses
• Difference / percent difference between total and dissolved sample pairs. There are two qualifier fields in EIM: Lab Qualifier is the qualifier assigned by the lab and may not reflect the usability of the data. This qualifier may have many different meanings and can vary between labs and over time within the same lab. Please refer to the laboratory report for a description of the lab qualifiers. As they are lab descriptors they are not to be used when evaluating the data. Validation Qualifier is the 3rd party formal validation qualifier if this was performed. Otherwise this field contains the qualifier resulting from the ADQM DVM review process. This qualifier assesses the usability of the data and may not equal the lab qualifier. The DVM applies the following data
evaluation qualifiers to analysis results, as warranted: Qualifier Definition B Not detected substantially above the level reported in the laboratory or field blanks. R Unusable result. Analyte may or may not be present in the sample.
J Analyte present. Reported value may not be accurate or precise.
UJ Not detected. Reporting limit may not be accurate or precise.

The Validation Status Code field is set to “DVM” if the ADQM DVM process has been performed. If the DVM has not been run, the field will be blank.
If the DVM has been run (Validation Status Code equals “DVM”), use the Validation Qualifier.
DVM Narrative ReportContamination detected in Field Blank(s). Sample result does not differ significantly from the analyte concentration detected in the associated fieldblank(s).LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PFO5DA0.15 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.034PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PFO5DA0.15 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.034PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PFO5DA0.15 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.034PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PFO5DA0.14 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.034PQLFAY-SW-SEEPA-5-D1-2-05211905/21/2019 280-124212-4 PFO5DA0.36 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.034PQLFAY-SW-SEEPA-5-D1-2-05211905/21/2019 280-124212-4 PFO5DA0.36 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.034PQLFAY-SW-SEEPA-TR1-05211905/21/2019 280-124212-7 PFO5DA0.23 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.034PQLFAY-SW-SEEPA-TR1-05211905/21/2019 280-124212-7 PFO5DA0.22 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.034PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PFO5DA0.045 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.034PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PFO5DA0.048 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.034PQLPage 1 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-WC-1-053019 05/30/2019 280-124599-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLPage 2 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-WC-1-053019 05/30/2019 280-124599-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 N-ethylperfluoro-1-octanesulfonamide0.0075 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0075PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 N-ethylperfluoro-1-octanesulfonamide0.0075 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0075PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 EVE Acid0.0049 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0049PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 EVE Acid0.0049 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0049PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PFECA-G0.0082 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0082PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PFECA-G0.0082 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0082PQLPage 3 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PES0.0092 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0092PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PES0.0092 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0092PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PFECA B0.012 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.012PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PFECA B0.012 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.012PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.012 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.012PQLPage 4 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.012 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.012PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.022 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.022PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.022 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.022PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PFESA-BP10.0053 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0053PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PFESA-BP10.0053 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0053PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 N-methyl perfluoro-1-octanesulfonamide0.0069 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0069PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 N-methyl perfluoro-1-octanesulfonamide0.0069 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0069PQLFB7-05301905/30/2019 280-124599-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLFB7-05301905/30/2019 280-124599-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLFB7-05301905/30/2019 280-124599-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFB7-05301905/30/2019 280-124599-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFB7-05301905/30/2019 280-124599-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLFB7-05301905/30/2019 280-124599-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLFB7-05301905/30/2019 280-124599-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFB7-05301905/30/2019 280-124599-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFB7-05301905/30/2019 280-124599-4 2-(N-ethyl perfluoro-1-0.060 ug/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.060PQLPage 5 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitoctanesulfonamido)-ethanolSOPFB7-05301905/30/2019 280-124599-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFB7-05301905/30/2019 280-124599-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFB7-05301905/30/2019 280-124599-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFB7-05301905/30/2019 280-124599-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFB7-05301905/30/2019 280-124599-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFB7-05301905/30/2019 280-124599-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFB7-05301905/30/2019 280-124599-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFB7-05301905/30/2019 280-124599-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFB7-05301905/30/2019 280-124599-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFB7-05301905/30/2019 280-124599-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLFB7-05301905/30/2019 280-124599-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLFB7-05301905/30/2019 280-124599-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB7-05301905/30/2019 280-124599-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB7-05301905/30/2019 280-124599-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLFB7-05301905/30/2019 280-124599-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLPage 6 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFB7-05301905/30/2019 280-124599-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLFB7-05301905/30/2019 280-124599-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLFB7-05301905/30/2019 280-124599-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFB7-05301905/30/2019 280-124599-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFB7-05301905/30/2019 280-124599-4 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFB7-05301905/30/2019 280-124599-4 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFB7-05301905/30/2019 280-124599-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFB7-05301905/30/2019 280-124599-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFB7-05301905/30/2019 280-124599-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLPage 7 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFB7-05301905/30/2019 280-124599-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFB7-05301905/30/2019 280-124599-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFB7-05301905/30/2019 280-124599-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFB7-05301905/30/2019 280-124599-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLFB7-05301905/30/2019 280-124599-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLFB7-05301905/30/2019 280-124599-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB7-05301905/30/2019 280-124599-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB7-05301905/30/2019 280-124599-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFB7-05301905/30/2019 280-124599-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PES0.0046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0046PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PES0.0046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0046PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PMPA0.057 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.057PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PMPA0.057 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.057PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PFECA B0.0060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0060PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PFECA B0.0060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0060PQLPage 8 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0060PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0060PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.011 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.011PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.011 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.011PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 N-methyl perfluoro-1-octanesulfonamide0.0035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0035PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 N-methyl perfluoro-1-octanesulfonamide0.0035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0035PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 N-ethylperfluoro-1-octanesulfonamide0.0037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0037PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 N-ethylperfluoro-1-octanesulfonamide0.0037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0037PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PFECA-G0.0041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0041PQLPage 9 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PFECA-G0.0041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0041PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLPage 10 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLPage 11 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PFECA B0.045 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.045PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PFECA B0.045 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.045PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.045 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.045PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.045 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.045PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.082 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.082PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.082 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.082PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 N-methyl perfluoro-1-octanesulfonamide0.026 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.026PQLPage 12 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 N-methyl perfluoro-1-octanesulfonamide0.026 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.026PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 N-ethylperfluoro-1-octanesulfonamide0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 N-ethylperfluoro-1-octanesulfonamide0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PFECA-G0.031 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.031PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PFECA-G0.031 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.031PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PFECA B0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PFECA B0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.12 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.12 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.22 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.22PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.22 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.22PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PFESA-BP10.053 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.053PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PFESA-BP10.053 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.053PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 N-methyl perfluoro-1-octanesulfonamide0.069 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.069PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 N-methyl perfluoro-1-octanesulfonamide0.069 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.069PQLPage 13 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PES0.092 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.092PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PES0.092 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.092PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PFO5DA0.067 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.067PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PFO5DA0.067 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.067PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 N-ethylperfluoro-1-octanesulfonamide0.075 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.075PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 N-ethylperfluoro-1-octanesulfonamide0.075 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.075PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PFECA-G0.082 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.082PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PFECA-G0.082 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.082PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 EVE Acid0.049 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.049PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 EVE Acid0.049 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.049PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 14 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 15 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFO5DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 16 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFO5DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFESA-BP20.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFESA-BP20.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLPage 17 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLPage 18 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFO3OA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFO3OA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFO4DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFO4DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFO5DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFO5DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLPage 19 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFESA-BP20.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFESA-BP20.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 20 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 R-EVE0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 R-EVE0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PMPA0.010 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.010PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PMPA0.010 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.010PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 2-(N-methyl perfluoro-1-0.11 ug/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.11PQLPage 21 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitoctanesulfonamido)-ethanolSOPFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFO2HxA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFO2HxA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLPage 22 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFO3OA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFO3OA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFO4DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFO4DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFO5DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFO5DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 23 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFESA-BP20.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFESA-BP20.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 R-EVE0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 R-EVE0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 24 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PMPA0.010 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.010PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PMPA0.010 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.010PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 2-(N-ethyl perfluoro-1-octanesulfonamido)0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 25 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnit-ethanolFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFO3OA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFO3OA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 26 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFO4DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFO4DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFO5DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFO5DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFESA-BP20.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 27 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFESA-BP20.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 R-EVE0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 R-EVE0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 Byproduct 40.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 Byproduct 40.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 28 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLPage 29 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 30 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PES0.023 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.023PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PES0.023 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.023PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PFECA B0.030 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PFECA B0.030 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 2-(N-ethyl perfluoro-1-0.030 ug/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.030PQLPage 31 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitoctanesulfonamido)-ethanolSOPFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.055 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.055PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.055 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.055PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 N-methyl perfluoro-1-octanesulfonamide0.017 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.017PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 N-methyl perfluoro-1-octanesulfonamide0.017 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.017PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 N-ethylperfluoro-1-octanesulfonamide0.019 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.019PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 N-ethylperfluoro-1-octanesulfonamide0.019 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.019PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PFECA-G0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PFECA-G0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PFECA B0.0060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0060PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PFECA B0.0060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0060PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0060PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0060PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.011 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.011PQLPage 32 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.011 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.011PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 N-methyl perfluoro-1-octanesulfonamide0.0035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0035PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 N-methyl perfluoro-1-octanesulfonamide0.0035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0035PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PES0.0046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0046PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PES0.0046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0046PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 EVE Acid0.0024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0024PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 EVE Acid0.0024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0024PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PFECA-G0.0041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0041PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PFECA-G0.0041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0041PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 2-(N-methyl perfluoro-1-0.11 ug/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.11PQLPage 33 of 87
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitoctanesulfonamido)-ethanolSOPFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PES0.034 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PES0.034 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLPage 34 of 87
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit. The actual detection limits may behigher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-WC-1-053019 05/30/2019 280-124599-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEPA-TR1-05211905/21/2019 280-124212-7 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEPA-TR1-05211905/21/2019 280-124212-7 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEPA-5-D1-2-05211905/21/2019 280-124212-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEPA-5-D1-2-05211905/21/2019 280-124212-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEPA-TR1-05211905/21/2019 280-124212-7 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEPA-TR1-05211905/21/2019 280-124212-7 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEPA-5-D1-2-05211905/21/2019 280-124212-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEPA-5-D1-2-05211905/21/2019 280-124212-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEPA-5-B-1-052119-D05/21/2019 280-124212-6 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEPA-5-B-1-052119-D05/21/2019 280-124212-6 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEPA-5-B-1-052119-D05/21/2019 280-124212-6 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEPA-5-B-1-052119-D05/21/2019 280-124212-6 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEPA-5-05211905/21/2019 280-124212-9 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEPA-5-05211905/21/2019 280-124212-9 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEPA-5-B-1-05211905/21/2019 280-124212-5 Perfluorooctadecanoicacid0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLPage 35 of 87
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit. The actual detection limits may behigher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEPA-5-B-1-05211905/21/2019 280-124212-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEPA-5-B-1-05211905/21/2019 280-124212-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEPA-5-B-1-05211905/21/2019 280-124212-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEPA-5-B-1-05211905/21/2019 280-124212-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEPA-10-05201905/20/2019 280-124212-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEPA-10-05201905/20/2019 280-124212-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEPA-4-05211905/21/2019 280-124212-8 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEPA-4-05211905/21/2019 280-124212-8 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEPA-4-05211905/21/2019 280-124212-8 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEPA-4-05211905/21/2019 280-124212-8 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEPA-5-05211905/21/2019 280-124212-9 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEPA-5-05211905/21/2019 280-124212-9 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-WC-1-TR1-05211905/21/2019 280-124212-10 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-WC-1-TR1-05211905/21/2019 280-124212-10 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-WC-1-TR1-05211905/21/2019 280-124212-10 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-WC-1-TR1-05211905/21/2019 280-124212-10 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-WC-1-TR2-05221905/22/2019 280-124323-2 Byproduct 50.058 UG/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.058PQLPage 36 of 87
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit. The actual detection limits may behigher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPFAY-SW-WC-1-TR2-05221905/22/2019 280-124323-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFAY-SW-WC-3-TR2-05231905/23/2019 280-124323-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFAY-SW-WC-3-TR2-05231905/23/2019 280-124323-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFAY-SW-WC-3-TR3-05231905/23/2019 280-124323-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFAY-SW-WC-3-TR3-05231905/23/2019 280-124323-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFAY-SW-WC-4-TR1-05221905/22/2019 280-124323-5 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFAY-SW-WC-4-TR1-05221905/22/2019 280-124323-5 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFAY-SW-WC-4-TR1-05221905/22/2019 280-124323-6 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFAY-SW-WC-4-TR1-05221905/22/2019 280-124323-6 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB1-05201905/20/2019 280-124212-13 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFB1-05201905/20/2019 280-124212-13 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFB1-05201905/20/2019 280-124212-13 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFB1-05201905/20/2019 280-124212-13 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFB2-05211905/21/2019 280-124222-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFB2-05211905/21/2019 280-124222-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFB2-05211905/21/2019 280-124222-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLPage 37 of 87
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit. The actual detection limits may behigher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFB2-05211905/21/2019 280-124222-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFB4-05231905/23/2019 280-124323-1 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB4-05231905/23/2019 280-124323-1 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB5-05241905/24/2019 280-124472-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFB5-05241905/24/2019 280-124472-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFB6-05291905/29/2019 280-124472-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFB6-05291905/29/2019 280-124472-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFB6-05291905/29/2019 280-124472-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB6-05291905/29/2019 280-124472-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFB7-05301905/30/2019 280-124599-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFB7-05301905/30/2019 280-124599-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEPA-1-05201905/20/2019 280-124212-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEPA-1-05201905/20/2019 280-124212-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEPA-1-05201905/20/2019 280-124212-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEPA-1-05201905/20/2019 280-124212-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEPA-1-052019-D05/20/2019 280-124212-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEPA-1-052019-D05/20/2019 280-124212-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.037PQLPage 38 of 87
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit. The actual detection limits may behigher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPFAY-SW-SEEPA-10-05201905/20/2019 280-124212-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEPA-10-05201905/20/2019 280-124212-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEPA-3-05211905/21/2019 280-124212-14 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEPA-3-05211905/21/2019 280-124212-14 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEPA-3-05211905/21/2019 280-124212-14 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEPA-3-05211905/21/2019 280-124212-14 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-TR2-1-05211905/21/2019 280-124222-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-TR2-1-05211905/21/2019 280-124222-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-TR2-1-05211905/21/2019 280-124222-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-TR2-1-05211905/21/2019 280-124222-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-TR3-1-05211905/21/2019 280-124222-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-TR3-1-05211905/21/2019 280-124222-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-TR3-1-05211905/21/2019 280-124222-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-TR3-1-05211905/21/2019 280-124222-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLPage 39 of 87
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit. The actual detection limits may behigher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-A-TR4-1-05211905/21/2019 280-124222-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-TR4-1-05211905/21/2019 280-124222-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-SEEP-A-TR4-1-05211905/21/2019 280-124222-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-SEEP-A-TR4-1-05211905/21/2019 280-124222-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-EXCESS RIVERWATER-05201905/20/2019 280-124212-11 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-EXCESS RIVERWATER-05201905/20/2019 280-124212-11 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-EXCESS RIVERWATER-05201905/20/2019 280-124212-11 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-EXCESS RIVERWATER-05201905/20/2019 280-124212-11 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-OUTFALL 002-05201905/20/2019 280-124212-12 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-OUTFALL 002-05201905/20/2019 280-124212-12 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-OUTFALL 002-05201905/20/2019 280-124212-12 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-OUTFALL 002-05201905/20/2019 280-124212-12 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-CFR-KINGS-05231905/23/2019 280-124325-2 Perfluorooctadecanoicacid0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLFAY-SW-CFR-RM-56-06071906/07/2019 280-124971-10 PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLFAY-SW-CFR-RM-56-06071906/07/2019 280-124971-10 PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLPage 40 of 87
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit. The actual detection limits may behigher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-RM-56-060719-D06/07/2019 280-124971-11 PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLFAY-SW-CFR-RM-56-060719-D06/07/2019 280-124971-11 PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLFAY-SW-GBC-2-052919 05/29/2019 280-124472-5 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-SW-GBC-2-052919 05/29/2019 280-124472-5 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-SW-GBC-TR2-1-05291905/29/2019 280-124472-8 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-SW-GBC-TR2-1-05291905/29/2019 280-124472-8 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-SW-GBC-TR2-1-05291905/29/2019 280-124472-8 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLFAY-SW-GBC-TR2-1-05291905/29/2019 280-124472-8 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLPage 41 of 87
Associated MS and/or MSD analysis had relative percent recovery (RPR) values higher than the upper control limit. The reported result may be biasedhigh.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-RM-56-060719-D06/07/2019 280-124971-11 Byproduct 40.0020 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-060719-D06/07/2019 280-124971-11 Byproduct 40.0081 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-06071906/07/2019 280-124971-21 R-EVE0.0020 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-06071906/07/2019 280-124971-21 R-EVE0.004 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-GBC-1-060719 06/07/2019 280-124971-4 R-EVE0.024 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-GBC-1-060719 06/07/2019 280-124971-4 R-EVE0.023 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-GBC-1-060719 06/07/2019 280-124971-4 Byproduct 40.049 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-GBC-1-060719 06/07/2019 280-124971-4 Byproduct 40.05 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 Byproduct 50.0052 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 Byproduct 50.0057 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 Byproduct 40.0020 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 Byproduct 40.004 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 Byproduct 50.012 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 Byproduct 50.011 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 Byproduct 40.0049 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 Byproduct 40.0046 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 42 of 87
Associated MS and/or MSD analysis had relative percent recovery (RPR) values higher than the upper control limit. The reported result may be biasedhigh.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-KINGS-052319-D05/23/2019 280-124325-3 Byproduct 50.0083 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-KINGS-052319-D05/23/2019 280-124325-3 Byproduct 50.0085 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-KINGS-06071906/07/2019 280-124971-23 R-EVE0.0083 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-KINGS-06071906/07/2019 280-124971-23 R-EVE0.009 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-KINGS-06071906/07/2019 280-124971-23 Byproduct 40.019 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-KINGS-06071906/07/2019 280-124971-23 Byproduct 40.02 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-KINGS-06071906/07/2019 280-124971-23 Byproduct 50.082 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-KINGS-06071906/07/2019 280-124971-23 Byproduct 50.084 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-06071906/07/2019 280-124971-22 R-EVE0.0063 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-06071906/07/2019 280-124971-22 R-EVE0.0064 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-06071906/07/2019 280-124971-22 Byproduct 40.019 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-06071906/07/2019 280-124971-22 Byproduct 40.019 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-06071906/07/2019 280-124971-22 Byproduct 50.069 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-06071906/07/2019 280-124971-22 Byproduct 50.065 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 R-EVE0.0040 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 R-EVE0.0042 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 Byproduct 50.031 UG/LCl. Spec. Table 3CompoundJPFAS_DI_Prep0.0020PQLPage 43 of 87
Associated MS and/or MSD analysis had relative percent recovery (RPR) values higher than the upper control limit. The reported result may be biasedhigh.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 Byproduct 50.032 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-SEEP-A-TR4-1-05211905/21/2019 280-124222-4 Byproduct 40.54 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-TR4-1-05211905/21/2019 280-124222-4 Byproduct 40.59 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-TR3-1-05211905/21/2019 280-124222-1 R-EVE0.60 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-TR3-1-05211905/21/2019 280-124222-1 R-EVE0.64 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-TR3-1-05211905/21/2019 280-124222-1 Byproduct 41.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-TR3-1-05211905/21/2019 280-124222-1 Byproduct 41.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-TR3-1-05211905/21/2019 280-124222-1 Byproduct 50.98 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-TR3-1-05211905/21/2019 280-124222-1 Byproduct 50.99 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-TR2-1-05211905/21/2019 280-124222-3 R-EVE0.57 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-TR2-1-05211905/21/2019 280-124222-3 R-EVE0.62 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-TR2-1-05211905/21/2019 280-124222-3 Byproduct 40.96 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-TR2-1-05211905/21/2019 280-124222-3 Byproduct 40.99 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-A-TR2-1-05211905/21/2019 280-124222-3 Byproduct 51.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-A-TR2-1-05211905/21/2019 280-124222-3 Byproduct 51.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEPA-10-05201905/20/2019 280-124212-3 R-EVE5.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLPage 44 of 87
Associated MS and/or MSD analysis had relative percent recovery (RPR) values higher than the upper control limit. The reported result may be biasedhigh.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEPA-10-05201905/20/2019 280-124212-3 R-EVE5.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEPA-10-05201905/20/2019 280-124212-3 Byproduct 47.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEPA-10-05201905/20/2019 280-124212-3 Byproduct 48.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEPA-10-05201905/20/2019 280-124212-3 Byproduct 571 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEPA-10-05201905/20/2019 280-124212-3 Byproduct 570.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEPA-10-05201905/20/2019 280-124212-3 PMPA61 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEPA-10-05201905/20/2019 280-124212-3 PMPA60.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEPA-1-05201905/20/2019 280-124212-1 PMPA24 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEPA-1-05201905/20/2019 280-124212-1 PMPA24.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEPA-1-05201905/20/2019 280-124212-1 PFMOAA103 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEPA-1-05201905/20/2019 280-124212-1 PFMOAA100.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEPA-1-052019-D05/20/2019 280-124212-2 PMPA25 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEPA-1-052019-D05/20/2019 280-124212-2 PMPA24.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 R-EVE0.028 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 R-EVE0.03 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 Byproduct 40.041 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 Byproduct 40.042 UG/LCl. Spec. Table 3CompoundJPFAS_DI_Prep0.0020PQLPage 45 of 87
Associated MS and/or MSD analysis had relative percent recovery (RPR) values higher than the upper control limit. The reported result may be biasedhigh.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPFAY-SW-WC-1-060719 06/07/2019 280-124971-3 Byproduct 50.27 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 Byproduct 50.26 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLWSTW-EXCESS RIVERWATER-06071906/07/2019 280-124971-12 R-EVE0.0020 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLWSTW-EXCESS RIVERWATER-06071906/07/2019 280-124971-12 R-EVE0.0039 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLWSTW-EXCESS RIVERWATER-06071906/07/2019 280-124971-12 Byproduct 40.013 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLWSTW-EXCESS RIVERWATER-06071906/07/2019 280-124971-12 Byproduct 40.013 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLWSTW-EXCESS RIVERWATER-06071906/07/2019 280-124971-12 Byproduct 50.0056 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLWSTW-EXCESS RIVERWATER-06071906/07/2019 280-124971-12 Byproduct 50.0053 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-SEEPA-5-05211905/21/2019 280-124212-9 R-EVE1.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEPA-5-05211905/21/2019 280-124212-9 R-EVE0.94 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEPA-5-05211905/21/2019 280-124212-9 Byproduct 41.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEPA-5-05211905/21/2019 280-124212-9 Byproduct 41.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEPA-5-05211905/21/2019 280-124212-9 Byproduct 56.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEPA-5-05211905/21/2019 280-124212-9 Byproduct 56.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEPA-5-05211905/21/2019 280-124212-9 PMPA38 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEPA-5-05211905/21/2019 280-124212-9 PMPA39.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLPage 46 of 87
Associated MS and/or MSD analysis had relative percent recovery (RPR) values higher than the upper control limit. The reported result may be biasedhigh.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEPA-10-05201905/20/2019 280-124212-3 PFO3OA14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEPA-10-05201905/20/2019 280-124212-3 PFO3OA14.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEPA-5-05211905/21/2019 280-124212-9 PFO3OA7.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEPA-5-05211905/21/2019 280-124212-9 PFO3OA7.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 47 of 87
High relative percent difference (RPD) observed between field duplicate and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-GBC-5-052919-D05/29/2019 280-124472-10 PMPA1.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-GBC-5-052919-D05/29/2019 280-124472-10 PMPA1.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-GBC-5-052919-D05/29/2019 280-124472-10 PEPA0.49 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-GBC-5-052919-D05/29/2019 280-124472-10 PEPA0.48 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-GBC-5-052919-D05/29/2019 280-124472-10 PFO2HxA0.69 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-GBC-5-052919-D05/29/2019 280-124472-10 PFO2HxA0.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-GBC-5-052919-D05/29/2019 280-124472-10 PFO3OA0.13 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-GBC-5-052919-D05/29/2019 280-124472-10 PFO3OA0.13 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-CFR-RM-56-060719-D06/07/2019 280-124971-11 Byproduct 50.0045 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-060719-D06/07/2019 280-124971-11 Byproduct 50.005 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-GBC-1-052919 05/29/2019 280-124472-4 PMPA1.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-GBC-1-052919 05/29/2019 280-124472-4 PMPA1.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-GBC-1-052919 05/29/2019 280-124472-4 PEPA0.30 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-GBC-1-052919 05/29/2019 280-124472-4 PEPA0.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-GBC-1-052919 05/29/2019 280-124472-4 PFO2HxA0.42 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-GBC-1-052919 05/29/2019 280-124472-4 PFO2HxA0.41 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-CFR-RM-56-06071906/07/2019 280-124971-10 Byproduct 40.0020 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 48 of 87
High relative percent difference (RPD) observed between field duplicate and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-RM-56-06071906/07/2019 280-124971-10 Byproduct 40.0085 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-06071906/07/2019 280-124971-10 Byproduct 50.0020 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-06071906/07/2019 280-124971-10 Byproduct 50.0081 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-KINGS-05231905/23/2019 280-124325-2 R-EVE0.010 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-KINGS-05231905/23/2019 280-124325-2 R-EVE0.01 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-KINGS-05231905/23/2019 280-124325-2 Byproduct 40.020 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-KINGS-05231905/23/2019 280-124325-2 Byproduct 40.021 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-KINGS-05231905/23/2019 280-124325-2 NVHOS0.0062 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-KINGS-05231905/23/2019 280-124325-2 NVHOS0.0069 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 Hfpo Dimer Acid15.0 UG/L537 ModifiedJ3535_PFC0.0070PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 Hfpo Dimer Acid19.0 UG/L537 ModifiedJ3535_PFC0.0071PQLFAY-SW-SEEPA-1-05201905/20/2019 280-124212-1 Hfpo Dimer Acid24.0 UG/L537 ModifiedJ3535_PFC0.0071PQLFAY-SW-SEEPA-1-052019-D05/20/2019 280-124212-2 Hfpo Dimer Acid30.0 UG/L537 ModifiedJ3535_PFC0.0073PQLPage 49 of 87
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PFO5DA0.11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0034PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PFO5DA0.11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0034PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 N-ethylperfluoro-1-octanesulfonamide0.0037 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0037PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 N-ethylperfluoro-1-octanesulfonamide0.0045 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0037PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PFO5DA2.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.017PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PFO5DA2.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.017PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PFO5DA8.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PFO5DA7.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PFO5DA4.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PFO5DA4.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PFO5DA0.57 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PFO5DA0.59 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-GBC-1-060719 06/07/2019 280-124971-4 PFO5DA0.0020 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-GBC-1-060719 06/07/2019 280-124971-4 PFO5DA0.0027 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PFO5DA0.12 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PFO5DA0.12 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEPA-4-05211905/21/2019 280-124212-8 Hfpo Dimer Acid20.0 UG/L537 ModifiedJ3535_PFC0.0040PQLPage 50 of 87
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEPA-10-05201905/20/2019 280-124212-3 Hfpo Dimer Acid48.0 UG/L537 ModifiedJ3535_PFC0.0071PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PFO5DA0.061 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0034PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PFO5DA0.057 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0034PQLFAY-SW-WC-1-TR1-05211905/21/2019 280-124212-10 Hfpo Dimer Acid0.062 UG/L537 ModifiedJ3535_PFC0.0040PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PFO5DA0.0040 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PFO5DA0.0039 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-SEEPA-5-B-1-05211905/21/2019 280-124212-5 Hfpo Dimer Acid0.042 UG/L537 ModifiedJ3535_PFC0.0040PQLFAY-SW-SEEPA-5-05211905/21/2019 280-124212-9 Hfpo Dimer Acid29.0 UG/L537 ModifiedJ3535_PFC0.0040PQLFAY-SW-SEEPA-5-B-1-052119-D05/21/2019 280-124212-6 Hfpo Dimer Acid0.038 UG/L537 ModifiedJ3535_PFC0.0040PQLFAY-SW-SEEPA-5-D1-2-05211905/21/2019 280-124212-4 Hfpo Dimer Acid12.0 UG/L537 ModifiedJ3535_PFC0.0040PQLFAY-SW-SEEPA-TR1-05211905/21/2019 280-124212-7 Hfpo Dimer Acid12.0 UG/L537 ModifiedJ3535_PFC0.0040PQLPage 51 of 87
Quality review criteria exceeded between the REP (laboratory replicate) and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PES0.046 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.046PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PES0.21 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.046PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.060PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PFECA B0.17 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.060PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.060PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.17 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.060PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.035PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 N-methyl perfluoro-1-octanesulfonamide0.14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.035PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.037PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 N-ethylperfluoro-1-octanesulfonamide0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.037PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.041PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PFECA-G0.21 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.041PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 Byproduct 60.38 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 Byproduct 60.47 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-GBC-5-052919 05/29/2019 280-124472-9 PMPA1.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-GBC-5-052919 05/29/2019 280-124472-9 PMPA2.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLPage 52 of 87
Quality review criteria exceeded between the REP (laboratory replicate) and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-RM-68-06071906/07/2019 280-124971-20 R-EVE0.023 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-68-06071906/07/2019 280-124971-20 R-EVE0.038 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-68-06071906/07/2019 280-124971-20 Byproduct 40.020 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-68-06071906/07/2019 280-124971-20 Byproduct 40.027 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-68-06071906/07/2019 280-124971-20 Byproduct 50.32 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-68-06071906/07/2019 280-124971-20 Byproduct 50.53 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-06071906/07/2019 280-124971-21 Byproduct 40.0079 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-06071906/07/2019 280-124971-21 Byproduct 40.0095 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-06071906/07/2019 280-124971-21 Byproduct 50.023 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-06071906/07/2019 280-124971-21 Byproduct 50.03 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-GBC-1-060719 06/07/2019 280-124971-4 PFMOAA0.14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLFAY-SW-GBC-1-060719 06/07/2019 280-124971-4 PFMOAA0.16 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PMPA0.010 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PMPA0.021 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 Byproduct 50.0079 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 Byproduct 50.0094 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-KINGS-05231905/23/2019 280-124325-2 Byproduct 50.0076 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 53 of 87
Quality review criteria exceeded between the REP (laboratory replicate) and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-KINGS-05231905/23/2019 280-124325-2 Byproduct 50.0086 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 NVHOS0.0076 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 NVHOS0.012 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 Byproduct 40.0096 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 Byproduct 40.0084 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-SEEP-A-TR4-1-05211905/21/2019 280-124222-4 R-EVE0.26 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-A-TR4-1-05211905/21/2019 280-124222-4 R-EVE0.32 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-B-1-05211905/21/2019 280-124257-1 R-EVE2.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-B-1-05211905/21/2019 280-124257-1 R-EVE1.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-B-1-05211905/21/2019 280-124257-1 Byproduct 42.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-B-1-05211905/21/2019 280-124257-1 Byproduct 42.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-B-1-05211905/21/2019 280-124257-1 Byproduct 521 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-1-05211905/21/2019 280-124257-1 Byproduct 516.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-2 -05211905/21/2019 280-124257-2 PFMOAA11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-B-2 -05211905/21/2019 280-124257-2 PFMOAA12.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-B-2 -05211905/21/2019 280-124257-2 Byproduct 556 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-B-2 -05211905/21/2019 280-124257-2 Byproduct 547.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 54 of 87
Quality review criteria exceeded between the REP (laboratory replicate) and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-B-2 -05211905/21/2019 280-124257-2 Byproduct 60.25 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-B-2 -05211905/21/2019 280-124257-2 Byproduct 60.29 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-C-1-05231905/23/2019 280-124325-4 PFO5DA0.097 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.050PQLFAY-SW-SEEP-C-1-05231905/23/2019 280-124325-4 PFO5DA0.07 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.050PQLFAY-SW-SEEP-C-1-05231905/23/2019 280-124325-4 Byproduct 60.052 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.023PQLFAY-SW-SEEP-C-1-05231905/23/2019 280-124325-4 Byproduct 60.035 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.023PQLFAY-SW-SEEPA-3-05211905/21/2019 280-124212-14 R-EVE1.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEPA-3-05211905/21/2019 280-124212-14 R-EVE1.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEPA-3-05211905/21/2019 280-124212-14 Byproduct 43.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEPA-3-05211905/21/2019 280-124212-14 Byproduct 42.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEPA-3-05211905/21/2019 280-124212-14 Byproduct 537 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEPA-3-05211905/21/2019 280-124212-14 Byproduct 529.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEPA-TR1-05211905/21/2019 280-124212-7 NVHOS0.28 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEPA-TR1-05211905/21/2019 280-124212-7 NVHOS0.21 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEPB-TR1-05211905/21/2019 280-124257-3 R-EVE0.50 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEPB-TR1-05211905/21/2019 280-124257-3 R-EVE0.34 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEPB-TR1-05211905/21/2019 280-124257-3 Byproduct 40.88 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLPage 55 of 87
Quality review criteria exceeded between the REP (laboratory replicate) and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEPB-TR1-05211905/21/2019 280-124257-3 Byproduct 40.62 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEPB-TR1-05211905/21/2019 280-124257-3 Byproduct 51.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEPB-TR1-05211905/21/2019 280-124257-3 Byproduct 50.79 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEPB-TR2-05211905/21/2019 280-124257-4 Byproduct 46.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEPB-TR2-05211905/21/2019 280-124257-4 Byproduct 45.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEPB-TR2-05211905/21/2019 280-124257-4 Byproduct 534 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEPB-TR2-05211905/21/2019 280-124257-4 Byproduct 528.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 Byproduct 50.22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 Byproduct 50.26 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 56 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PMPA37 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.43PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PMPA35.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.43PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 Hfpo Dimer Acid40 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.064PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PMPA35 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PMPA35.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PFMOAA157 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PFMOAA150.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 EVE Acid4.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 EVE Acid4.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PFESA-BP20.94 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PFESA-BP20.93 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 Hydro-EVE Acid2.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 Hydro-EVE Acid2.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PFO2HxA39 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PFO2HxA39.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PFO3OA8.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PFO3OA8.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 57 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PFO4DA1.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PFO4DA1.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PFO5DA0.27 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PFO5DA0.26 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PEPA15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PEPA15.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PFESA-BP12.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 PFESA-BP12.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 R-EVE3.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 R-EVE3.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 Byproduct 43.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 Byproduct 43.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 Byproduct 534 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 Byproduct 532.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 Byproduct 60.078 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 Byproduct 60.074 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 NVHOS7.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLPage 58 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 NVHOS8.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PMPA87 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PMPA87.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 Hfpo Dimer Acid85 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.086PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.11PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.18 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.11PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PEPA50 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PEPA49.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PFESA-BP117 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PFESA-BP117.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PFO2HxA18 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PFO2HxA18.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PFO3OA4.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PFO3OA4.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PFO4DA2.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PFO4DA2.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLPage 59 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PFO5DA1.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PFO5DA1.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PFMOAA13 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PFMOAA12.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 EVE Acid24 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 EVE Acid26.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PFESA-BP23.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 PFESA-BP23.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 Hydro-EVE Acid8.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 Hydro-EVE Acid9.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 Hfpo Dimer Acid (trial)84.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.086PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 R-EVE11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 R-EVE11.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 Byproduct 412 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 Byproduct 412.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 Byproduct 574 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP B-2-06071906/07/2019 280-124971-19 Byproduct 572.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 60 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 NVHOS4.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.040PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 NVHOS4.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.040PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 Hfpo Dimer Acid (trial)4.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0086PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 R-EVE0.17 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0070PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 R-EVE0.16 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0070PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 Byproduct 40.29 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.016PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 Byproduct 40.27 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.016PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 Byproduct 50.30 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0058PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 Byproduct 50.29 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0058PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 Byproduct 60.0052 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 Byproduct 60.0049 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 NVHOS3.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP B-1-06071906/07/2019 280-124971-16 NVHOS3.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PFESA-BP20.14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0030PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PFESA-BP20.13 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0030PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 Hydro-EVE Acid0.062 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0028PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 Hydro-EVE Acid0.059 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0028PQLPage 61 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PMPA5.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.057PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PMPA5.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.057PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 Hfpo Dimer Acid5.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0086PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PFO2HxA5.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0081PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PFO2HxA5.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0081PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PFO3OA1.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0058PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PFO3OA1.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0058PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PFO4DA0.47 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0079PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PFO4DA0.43 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0079PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PFMOAA7.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.021PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PFMOAA7.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.021PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PEPA1.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PEPA1.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PFESA-BP10.0055 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0027PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 PFESA-BP10.0047 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0027PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 Hfpo Dimer Acid (trial)19.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.043PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 R-EVE0.95 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.035PQLPage 62 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 R-EVE0.93 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.035PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 Byproduct 41.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 Byproduct 41.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 Byproduct 56.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.029PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 Byproduct 56.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.029PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 Byproduct 60.029 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0077PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 Byproduct 60.031 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0077PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 NVHOS0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0054PQLFAY-SW-SEEP A-TR1-1-06071906/07/2019 280-124971-8 NVHOS0.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0054PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PFMOAA59 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.11PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PFMOAA61.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.11PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 EVE Acid0.087 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.012PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 EVE Acid0.092 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.012PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PFESA-BP20.77 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PFESA-BP20.77 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 Hydro-EVE Acid0.70 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.014PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 Hydro-EVE Acid0.73 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.014PQLPage 63 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PFO2HxA25 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.041PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PFO2HxA26.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.041PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PFO3OA6.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.029PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PFO3OA7.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.029PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PFO4DA2.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.039PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PFO4DA2.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.039PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PEPA11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.023PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PEPA11.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.023PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PFESA-BP10.38 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.013PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PFESA-BP10.37 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.013PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PMPA25 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.28PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 PMPA26.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.28PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 Hfpo Dimer Acid19 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.043PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PMPA25 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PMPA25.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 Hfpo Dimer Acid34 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.086PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 Hfpo Dimer Acid (trial)34.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.086PQLPage 64 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 R-EVE1.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 R-EVE1.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 Byproduct 43.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 Byproduct 42.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 Byproduct 533 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 Byproduct 533.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 Byproduct 60.088 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 Byproduct 60.088 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 NVHOS0.76 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP A-4-06071906/07/2019 280-124971-9 NVHOS0.79 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PFMOAA122 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PFMOAA120.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 EVE Acid1.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 EVE Acid1.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PFESA-BP22.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PFESA-BP22.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 Hydro-EVE Acid2.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLPage 65 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 Hydro-EVE Acid2.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PFO2HxA48 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PFO2HxA47.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PFO3OA17 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PFO3OA17.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PFO4DA8.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PFO4DA8.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PEPA9.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PEPA9.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PFESA-BP111 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 PFESA-BP111.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 R-EVE1.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 R-EVE1.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 Byproduct 41.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 Byproduct 41.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 Byproduct 518 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 Byproduct 517.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 66 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 Byproduct 60.050 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 Byproduct 60.05 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 NVHOS1.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP A-3-06071906/07/2019 280-124971-7 NVHOS1.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PFMOAA72 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PFMOAA72.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 EVE Acid0.97 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 EVE Acid0.97 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PFESA-BP21.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PFESA-BP21.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 Hydro-EVE Acid1.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 Hydro-EVE Acid1.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PFO2HxA30 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PFO2HxA29.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PFO3OA11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PFO3OA11.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PFO4DA5.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLPage 67 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PFO4DA5.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PEPA6.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PEPA6.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PFESA-BP15.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PFESA-BP15.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PMPA17 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 PMPA17.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PMPA5.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PMPA5.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 R-EVE0.20 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 R-EVE0.22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 Byproduct 40.39 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 Byproduct 40.39 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 Byproduct 51.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 Byproduct 51.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLPage 68 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 NVHOS1.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP A-1-06071906/07/2019 280-124971-6 NVHOS1.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PFMOAA91 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PFMOAA93.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 EVE Acid0.025 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PFESA-BP20.35 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PFESA-BP20.36 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 Hydro-EVE Acid0.20 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 Hydro-EVE Acid0.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PFO2HxA18 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PFO2HxA18.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PFO3OA4.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PFO3OA4.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PFO4DA1.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PFO4DA1.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PEPA1.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLPage 69 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PEPA1.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PFESA-BP10.30 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 PFESA-BP10.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 NVHOS0.90 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-OLDOF-2-06071906/07/2019 280-124971-2 NVHOS0.92 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 NVHOS0.0041 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 NVHOS0.004 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFO2HxA0.0035 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-76-05221905/22/2019 280-124268-3 PFO2HxA0.0029 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 NVHOS0.0028 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-56-05221905/22/2019 280-124268-1 NVHOS0.0027 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFO2HxA0.0020 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-RM-08-05221905/22/2019 280-124268-2 PFO2HxA0.0028 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PMPA0.031 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PMPA0.032 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFMOAA0.13 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFMOAA0.14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLPage 70 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 NVHOS0.0061 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 NVHOS0.0063 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFO2HxA0.040 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFO2HxA0.041 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFO3OA0.0099 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFO3OA0.01 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFO4DA0.0035 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-CFR-BLADEN-05221905/22/2019 280-124268-4 PFO4DA0.0036 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 NVHOS0.81 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 NVHOS0.81 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PFESA-BP20.39 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PFESA-BP20.38 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 Hydro-EVE Acid1.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 Hydro-EVE Acid1.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PFMOAA90 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PFMOAA86.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PFO2HxA24 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLPage 71 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PFO2HxA24.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PFO3OA7.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PFO3OA7.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PFO4DA1.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PFO4DA1.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PEPA2.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PEPA2.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PMPA7.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 PMPA7.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PFESA-BP20.66 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.061PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PFESA-BP20.62 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.061PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 Hydro-EVE Acid2.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.056PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 Hydro-EVE Acid2.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.056PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 R-EVE1.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.14PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 R-EVE2.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.14PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 Byproduct 41.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.32PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 Byproduct 41.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.32PQLPage 72 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 Byproduct 53.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 Byproduct 52.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 Byproduct 60.040 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.031PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 Byproduct 60.041 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.031PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 NVHOS0.90 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 NVHOS0.86 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PFMOAA199 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.42PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PFMOAA190.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.42PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PMPA13 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep1.1PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PMPA12.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep1.1PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PFO2HxA56 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PFO2HxA54.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PFO3OA17 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PFO3OA17.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PFO4DA3.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PFO4DA3.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PEPA4.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.093PQLPage 73 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 PEPA3.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.093PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 Hfpo Dimer Acid (trial)38.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.064PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 R-EVE5.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.053PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 R-EVE5.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.053PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 Byproduct 46.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 Byproduct 45.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 Byproduct 537 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.044PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 Byproduct 535.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.044PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 Byproduct 60.13 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.012PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 Byproduct 60.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.012PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 NVHOS2.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.11PQLFAY-SW-SEEP C-1-06071906/07/2019 280-124971-1 NVHOS2.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.11PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PFMOAA82 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PFMOAA77.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 EVE Acid2.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.018PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 EVE Acid1.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.018PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PFESA-BP21.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.023PQLPage 74 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PFESA-BP21.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.023PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 Hydro-EVE Acid3.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.021PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 Hydro-EVE Acid3.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.021PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PFO2HxA27 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.061PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PFO2HxA25.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.061PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PFO3OA4.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.044PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PFO3OA4.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.044PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PFO4DA1.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.059PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PFO4DA1.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.059PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PFO5DA0.38 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.025PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PFO5DA0.34 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.025PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PEPA19 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.035PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PEPA18.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.035PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PFESA-BP12.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLFAY-SW-SEEP B-TR2-06071906/07/2019 280-124971-18 PFESA-BP12.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PEPA2.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PEPA2.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLPage 75 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 R-EVE1.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 R-EVE0.97 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 Byproduct 40.84 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 Byproduct 40.83 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 Byproduct 52.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 Byproduct 52.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 Byproduct 60.017 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP D-1-06071906/07/2019 280-124971-5 Byproduct 60.017 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PMPA9.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PMPA8.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PFESA-BP20.32 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PFESA-BP20.32 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 Hydro-EVE Acid1.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 Hydro-EVE Acid1.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 R-EVE1.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 R-EVE1.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 Byproduct 40.97 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLPage 76 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 Byproduct 40.91 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 Byproduct 52.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 Byproduct 52.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 NVHOS0.80 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 NVHOS0.77 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PFO2HxA29 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PFO2HxA29.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PFO3OA7.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PFO3OA7.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PFO4DA2.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PFO4DA2.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PMPA9.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PMPA9.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PFMOAA91 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-D-1-05301905/30/2019 280-124599-1 PFMOAA90.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLPage 77 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PFO2HxA29 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PFO2HxA28.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PFO3OA8.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PFO3OA7.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PFO4DA2.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PFO4DA2.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PEPA3.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PEPA2.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 R-EVE1.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 R-EVE1.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 Byproduct 41.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 Byproduct 41.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 Byproduct 52.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 Byproduct 52.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PFESA-BP20.34 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PFESA-BP20.32 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 Hydro-EVE Acid1.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLPage 78 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 Hydro-EVE Acid1.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PFMOAA91 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEP-D-1-053019-D05/30/2019 280-124599-2 PFMOAA88.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 R-EVE0.015 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0070PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 R-EVE0.014 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0070PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 Byproduct 40.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.016PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 Byproduct 40.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.016PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 Byproduct 50.56 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0058PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 Byproduct 50.55 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0058PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 Byproduct 60.0040 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 Byproduct 60.0039 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PFMOAA0.48 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.021PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PFMOAA0.47 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.021PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 EVE Acid0.0028 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0024PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 EVE Acid0.0024 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0024PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PFESA-BP20.21 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0030PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PFESA-BP20.21 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0030PQLPage 79 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 Hydro-EVE Acid0.0045 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0028PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 Hydro-EVE Acid0.0041 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0028PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PFO2HxA0.11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0081PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PFO2HxA0.11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0081PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PFO3OA0.055 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0058PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PFO3OA0.053 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0058PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PFO4DA0.046 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0079PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PFO4DA0.044 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0079PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PFESA-BP10.014 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0027PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 PFESA-BP10.014 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0027PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 NVHOS0.042 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0054PQLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 NVHOS0.041 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0054PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PFESA-BP20.017 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PFESA-BP20.017 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 Hydro-EVE Acid0.0054 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 Hydro-EVE Acid0.0053 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PFMOAA0.81 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLPage 80 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PFMOAA0.82 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PFO3OA0.067 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PFO3OA0.066 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PFO4DA0.016 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PFO4DA0.016 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFB7-05301905/30/2019 280-124599-4 PFO5DA0.037 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFB7-05301905/30/2019 280-124599-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PFO2HxA15 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.016PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PFO2HxA15.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.016PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PFO3OA3.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.012PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PFO3OA3.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.012PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PFO4DA1.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.016PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PFO4DA1.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.016PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PFO5DA0.16 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0067PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PFO5DA0.16 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0067PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PEPA16 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PEPA16.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLPage 81 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PMPA34 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.11PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PMPA35.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.11PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 Hfpo Dimer Acid19 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.017PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 NVHOS0.21 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.011PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 NVHOS0.21 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.011PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PFO2HxA0.73 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PFO2HxA0.75 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PFO3OA0.12 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PFO3OA0.12 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PEPA0.24 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PEPA0.23 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 Hfpo Dimer Acid (trial)19.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.017PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 R-EVE0.82 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.014PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 R-EVE0.81 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.014PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 Byproduct 41.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.032PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 Byproduct 41.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.032PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 Byproduct 50.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.012PQLPage 82 of 87
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 Byproduct 50.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.012PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 Byproduct 60.0086 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0031PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 Byproduct 60.0088 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0031PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PFESA-BP20.18 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0061PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PFESA-BP20.18 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0061PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 Hydro-EVE Acid0.083 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0056PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 Hydro-EVE Acid0.08 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0056PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PFMOAA17 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.042PQLFAY-SW-SEEPB-TR1-06071906/07/2019 280-124971-17 PFMOAA17.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.042PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PEPA0.14 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PEPA0.14 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 NVHOS0.014 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 NVHOS0.014 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PMPA1.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PMPA1.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PFMOAA1.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-WC-1-053019 05/30/2019 280-124599-3 PFMOAA1.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLPage 83 of 87
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit but above the rejection limit. Thereported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-OLDOF-2-05241905/24/2019 280-124472-2 R-EVE0.17 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-OLDOF-2-05241905/24/2019 280-124472-2 R-EVE0.17 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-CFR-KINGS-05231905/23/2019 280-124325-2 PFMOAA0.0078 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLFAY-SW-CFR-KINGS-05231905/23/2019 280-124325-2 PFMOAA0.0081 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLFAY-SW-CFR-KINGS-06071906/07/2019 280-124971-23 PFMOAA0.23 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLFAY-SW-CFR-KINGS-06071906/07/2019 280-124971-23 PFMOAA0.24 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLFAY-SW-SEEP-B-3A-05211905/21/2019 280-124257-5 PFESA-BP158 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.13PQLFAY-SW-SEEP-B-3A-05211905/21/2019 280-124257-5 PFESA-BP161.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.13PQLFAY-SW-SEEP-B-3A-05211905/21/2019 280-124257-5 R-EVE19 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.35PQLFAY-SW-SEEP-B-3A-05211905/21/2019 280-124257-5 R-EVE19.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.35PQLFAY-SW-SEEP-B-3A-05211905/21/2019 280-124257-5 Byproduct 422 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.79PQLFAY-SW-SEEP-B-3A-05211905/21/2019 280-124257-5 Byproduct 423.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.79PQLFAY-SW-SEEPA-3-05211905/21/2019 280-124212-14 PFMOAA118 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEPA-3-05211905/21/2019 280-124212-14 PFMOAA120.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PFO2HxA0.42 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PFO2HxA0.42 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 84 of 87
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit but above the rejection limit. Thereported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-SEEPB-TR1-05211905/21/2019 280-124257-3 PFMOAA38 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-SEEPB-TR1-05211905/21/2019 280-124257-3 PFMOAA42.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PMPA0.54 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLFAY-SW-WC-1-060719 06/07/2019 280-124971-3 PMPA0.54 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLPage 85 of 87
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the rejection level. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-CFR-KINGS-052319-D05/23/2019 280-124325-3 PFMOAA0.0084 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLFAY-SW-CFR-KINGS-052319-D05/23/2019 280-124325-3 PFMOAA0.0085 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLPage 86 of 87
The result is estimated since the concentration is between the method detection limit and practical quantitation limit.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingCreeks Seeps Old Outfall 002 FI 5/19AnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitWSTW-EXCESS RIVERWATER-06071906/07/2019 280-124971-12 Fluoride0.12 MG/L0.060300.0J0.50MDLWSTW-OUTFALL 002-06071906/07/2019 280-124971-13 Fluoride0.15 MG/L0.060300.0J0.50MDLFAY-SW-CFR-BLADEN-06071906/07/2019 280-124971-22 Fluoride0.12 MG/L0.060300.0J0.50MDLFAY-SW-CFR-RM-56-060719-D06/07/2019 280-124971-11 Fluoride0.13 MG/L0.060300.0J0.50MDLFAY-SW-CFR-RM-56-06071906/07/2019 280-124971-10 Fluoride0.14 MG/L0.060300.0J0.50MDLFAY-SW-CFR-RM-68-06071906/07/2019 280-124971-20 Fluoride0.13 MG/L0.060300.0J0.50MDLFAY-SW-CFR-RM-76-06071906/07/2019 280-124971-21 Fluoride0.13 MG/L0.060300.0J0.50MDLPage 87 of 87
ATTACHMENT 3:
Assessment of HFPO-DA and PFMOAA in
Outfall 002 Discharge and Evaluation of
Potential Control Options

ASSESSMENT OF
HFPO-DA AND PFMOAA IN OUTFALL
002 DISCHARGE AND EVALUATION
OF POTENTIAL CONTROL OPTIONS
Chemours Fayetteville Works, NC
Prepared for
The Chemours Company FC, LLC 22828 NC-87
Fayetteville, NC 28306

Prepared by
Geosyntec Consultants of NC, P.C.
2501 Blue Ridge Road, Suite 430
Raleigh, NC 27607
Geosyntec Project Number TR0795
August 2019

Outfall 002 Assessment i August 26, 2019
TABLE OF CONTENTS
1 INTRODUCTION AND OBJECTIVES .............................................................. 5
2 DESCRIPTION OF OUTFALL 002 AND SITE CONVEYANCE NETWORK 6
3 HFPO-DA AND PFMOAA DATA ASSESSMENT ........................................... 8
3.1 HFPO-DA and PFMOAA Temporal Trends ............................................... 8
3.2 HFPO-DA and PFMOAA Calendar Year 2018 – Mass Loading ............... 9
3.3 Paragraph 11(c) Bimonthly Sampling ....................................................... 12
3.4 Stormwater Sampling ................................................................................ 15
3.5 Supplemental Wastewater Treatment Plant Sampling .............................. 17
3.6 Supplemental Conveyance Network Sediment Sampling (Dry Weather) . 19
3.7 Supplemental Outfall Channel Sampling (Dry Weather) .......................... 20
3.8 Observations from Data Assessment ......................................................... 21
3.9 Data Needs and On-going Assessment Activities ..................................... 21
4 POTENTIAL CONTROL APPROACHES ....................................................... 22
4.1 Investigate and Control Dry Weather Sources to the Cooling Water
Channel ............................................................................................................... 22
4.2 Targeted Sediment Removal ..................................................................... 22
4.3 Assess Potential for Groundwater Intrusion .............................................. 23
4.4 Decommission and Replace the Remaining Portion of the Terracotta Pipe
24
4.5 Continue Air Abatement Measures ........................................................... 24
4.6 Implement Targeted Stormwater Source Control and/or Treatment ......... 25
4.7 Treat Stormwater End of Pipe ................................................................... 25
4.8 Stormwater Pollution Prevention Plan (SWPPP) ...................................... 26
4.9 Treat All Flows End of Pipe ...................................................................... 26
4.10 Summary of Potential Control Approaches ............................................... 27
5 SUMMARY ........................................................................................................ 31
6 REFERENCES ................................................................................................... 32

Outfall 002 Assessment ii August 26, 2019
LIST OF TABLES
Table 1: Outfall 002 HFPO-DA Concentrations (June 2017 – July 2019)
Table 2: Outfall 002 PFMOAA Concentrations (June 2017 – July 2019)
Table 3: River Intake HFPO-DA Concentrations (June 2017 – July 2019)
Table 4: River Intake PFMOAA Concentrations (June 2017 – July 2019)
Table 5: Total Daily Precipitation (June 2017 – July 2019)
Table 6: Bimonthly Sample Locations – Paragraph 11(c)
Table 7: Analytical Results – April 2019 Paragraph 11(c) Sampling Event
Table 8: Analytical Results – June 2019 Paragraph 11(c) Sampling Event
Table 9: Loading Estimates to Outfall 002 Added Throughout the Site Conveyance
Network during Dry Weather (for HFPO-DA)
Table 10: Analytical Results – Stormwater Sampling
Table 11: Analytical Results – Wastewater Treatment Plant
Table 12: Analytical Results – Cooling Water Channel Sediments
Table 13: Analytical Results – Additional Outfall 002 Samples
Table 14: Potential Control Approaches and Estimated Load Reductions

Outfall 002 Assessment iii August 26, 2019
LIST OF FIGURES
Figure 1: Facility Production Areas and Site Conveyance Network
Figure 2: Conceptual Schematic of Site Water Balance
Figure 3: Site Conveyance Network
Figure 4: Precipitation Data and Outfall 002 HFPO-DA Concentrations (June 2017 –
July 2019)
Figure 5: Precipitation Data and Outfall 002 HFPO-DA Concentrations (August 2017
– July 2019)
Figure 6: Precipitation Data and Outfall 002 PFMOAA Concentrations (May 2018 –
July 2019)
Figure 7: Calendar Year 2018 HFPO-DA Concentrations at Outfall 002
Figure 8: Calendar Year 2018 PFMOAA Concentrations at Outfall 002
Figure 9: Calendar Year 2018 Outfall 002 Flow and Precipitation
Figure 10: Calendar Year 2018 HFPO-DA Loading at Outfall 002
Figure 11: Calendar Year 2018 PFMOAA Loading at Outfall 002
Figure 12: Paragraph 11(b) Sample Locations
Figure 13: HFPO-DA and PFMOAA Concentrations – April 2019 Dry Event
Figure 14: HFPO-DA and PFMOAA Concentrations - June 2019 Dry Event
Figure 15: Stormwater Sampling Locations
Figure 16: HFPO-DA and PFMOAA Concentrations – June 2019 Storm Event
Figure 17: Wastewater Treatment Plant Sampling Locations
Figure 18: HFPO-DA and PFMOAA Concentrations Wastewater Treatment Plant
Sampling
Figure 19: Composite Sediment Sample Locations
Figure 20: Results of Deionized Water Added to Composite Sediment Samples
Figure 21: Additional Outfall 002 Sample Locations
Figure 22: HFPO-DA and PFMOAA Concentrations - Additional Outfall 002 Samples
- May 2019 Event

Outfall 002 Assessment iv August 26, 2019
LIST OF APPENDICES
Appendix A: Laboratory Reports & Data Verification Module Reports

Outfall 002 Assessment v August 26, 2019
ACRONYMS AND ABBREVIATIONS
HDPE High Density Polyethylene
HFPO-DA Hexafluoropropylene oxide dimer acid
IXM Ion Exchange Membrane
ng/L Nanograms per Liter
NCCW Non-contact Cooling Water
NCDEQ The North Carolina Department of Environmental Quality
PFAS Per- and polyfluoroalkyl substances
PFMOAA perfluoro-2-methoxyacetic acid
PPA Polymer Processing Aid
SOP Standard Operating Procedure
SWMM Stormwater Management Model
SWPPP Stormwater Pollution Prevention Plan
TSS Total Suspended Solids
WWTP Wastewater Treatment Plant
VEN Vinyl Ethers North

Outfall 002 Assessment vi August 26, 2019
This report has been prepared under the direction of a North Carolina Licensed Engineer,
subject to limitations of currently available data in an ongoing site investigation.
Geosyntec Consultants of NC, PC is licensed to practice geology in North Carolina. The
certification number (Firm’s License Number) is C-295. Geosyntec Consultants of NC,
PC is licensed to practice engineering in North Carolina. The certification number
(Firm’s License Number) is C-3500.
Not considered final until all signatures have been applied.
8/26/2019

Outfall 002 Assessment 1 August 26, 2019
EXECUTIVE SUMMARY
Geosyntec Consultants of NC, P.C. (Geosyntec) has prepared this report for The
Chemours Company FC, LLC (Chemours) to provide an assessment of
hexafluoropropylene oxide dimer acid (HFPO-DA) and perfluoro-2-methoxyacetic acid
(PFMOAA) detected at Outfall 002 at Chemours Fayetteville Works (the Site). This
report is one of four supporting attachments to the Cape Fear River PFAS Loading
Reduction Plan (Reduction Plan; Geosyntec, 2019a) required by Paragraph 12 of the
Consent Order among Chemours, the North Carolina Department of Environmental
Quality (NCDEQ) and Cape Fear River Watch. This report has been prepared to present
data and a technical analysis related to Outfall 002 to support actions Chemours is
proposing in the Reduction Plan along with an evaluation of Consent Order Paragraph
12(d) requirements to assess the potential to reduce HFPO-DA and PFMOAA.
The Site is adjacent to the Cape Fear River and draws water from the Cape Fear River,
the majority of which is used as non-contact cooling water (NCCW) and is then
transported through the Site Conveyance Network and returned to the river via Outfall
002. Prior to June 2017, Outfall 002 represented the primary transport pathway by which
per- and polyfluoroalkyl substances (PFAS) originating from the Facility reached the
river. Actions taken by Chemours to divert process wastewater flows away from Outfall
002 reduced HFPO-DA loads to the river by over 95% from pre-June 2017 to 2019, as
presented in the Reduction Plan. At present, under normal operating conditions, Outfall
002 contributes between 1% and 4% of the loads of HFPO-DA and PFMOAA observed
in the Cape Fear River (Geosyntec, 2019b). The remaining fraction is predominantly the
result of historical air deposition. Chemours is implementing air emissions controls to
reduce facility-wide PFAS air emissions by 99%. Over time this action, in addition to the
actions proposed in the Reduction Plan, will further reduce PFAS at Outfall 002.
Chemours is conducting bimonthly sampling of the Site Conveyance Network pursuant
to Consent Order Paragraph 11(c) to assess sources of loading and variability over time
in the conveyance network. Chemours has also conducted stormwater sampling at 24
locations during one rainfall event to characterize distributions of HFPO-DA and
PFMOAA in stormwater. Chemours is planning to conduct two more stormwater
sampling events to further characterize stormwater loads and sources.
Results to date indicate HFPO-DA and PFMOAA loads to Outfall 002 are dominated by
three general source categories:
 river intake loading – loading of HFPO-DA and PFMOAA in water drawn from
the Cape Fear River;

Outfall 002 Assessment 2 August 26, 2019
• dry weather loading – additional loading contributed to flows passing through the
Site Conveyance Network;
• stormwater loading – loading added, during wet weather only, from stormwater
runoff entering the Site Conveyance Network.
Estimated load percentages of the total load attributable to each category, for the 2018
calendar year, are shown in the table that follows. The process for deriving these estimates
based on measured flows and concentrations from the intake and Outfall 002 is described
in the report.
Loading Type HFPO-DA PFMOAA
River Intake 11% 48%
Dry Weather 44% 21%
Stormwater 45% 31%

The two bimonthly, dry weather sampling events performed to date indicate dry weather
loads primarily originate from the open section of the Cooling Water Channel in the
Chemours Monomers Ion Exchange Membrane (IXM) manufacturing area and the Open
Channel to Outfall 002 near the DuPont Area. Loads from the Chemours Monomers IXM
Manufacturing Area may potentially be added from sediments in the Cooling Water
Channel and/or other unknown sources. Loads from the Open Channel to Outfall 002
near the DuPont Area may potentially be added by sediments in the channel and/or
potential groundwater intrusion. Estimated facility-based loading from these two sources
(river intake loads excluded) along with loads from the Wood Lined Trench that transmits
NCCW and Wastewater Treatment Plant (WWTP) effluent, are presented for the two
2019 dry weather sampling events in the table below.
April Event June Event
Facility HFPO-DA Dry Weather Loading Source
Load1 (lbs/day)
% of Total Load at
Outfall 002
Load1 (lbs/day)
% of Total Load at
Outfall 002
Wood Lined Trench 0 0% 0.00031 5%
Cooling Water Channel 0.0020 24% 0.0031 48%
Wastewater Treatment Plant Effluent 0.00058 7% 0.00055 9%
Open Channel to Outfall 002 0.0057 69% 0.0025 38%
1 Loads are calculated based on concentrations measured during the dry weather sampling events and estimated flows
on the day sampling occurred from each loading source (using measured flow at Outfall 002 on the day sampling
occurred and typical flows from the various loading sources, based on data from December 2017 through May 2019).

Outfall 002 Assessment 3 August 26, 2019
Stormwater grab sampling results indicated the highest stormwater concentrations were
associated with areas in the Chemours Monomers IXM Area, the Chemours Polymer
Processing Aid (PPA) Area and near the WWTP. Detailed stormwater modeling analyses
and additional sampling events are underway to determine the relative loadings associated
with stormwater from different areas onsite.
Existing abatement of air emissions are expected to further reduce both dry weather and
stormwater loads to the Site Conveyance Network. In addition to air abatement actions,
eight other potential control approaches that are expected to be capable of reducing
loadings at Outfall 002 have been identified in this report. The possible timelines to
implement these approaches and estimates of their potential load reduction benefits, for
those that can be estimated, are presented. These potential approaches include the
following:
• Remove targeted sediments, which could contain PFAS from historical aerial
deposition, along the open section of the Cooling Water Channel and in the Open
Channel to Outfall 002.
• Investigate, locate, and control other (non-sediment) dry weather sources to the
Cooling Water Channel.
• Assess the potential for groundwater intrusion of perched zone groundwater
containing HFPO-DA infiltrating into the Open Channel to Outfall 002 and
reduce, if occurring.
• Decommission the remaining portion of the terracotta pipe to the WWTP to
prevent transport of PFAS that are potentially still present in the pipe or adhered
to remnant sediments.
• Continue air abatement measures to reduce PFAS loading to the land surface and
over time reduce concentrations in surface soils and on surfaces that are then
flushed through the environment.
• Implement targeted stormwater source control and/or treatment, including
covering/sealing of certain areas, replacement of materials, sweeping or
washing/rinsing, or targeted collection and treatment with carbon filtration or ion
exchange.
• Treat stormwater end of pipe, up to a given design flowrate, by constructing a
separate collection system for either stormwater or NCCW to segregate these
flows and provide treatment of the stormwater.

Outfall 002 Assessment 4 August 26, 2019
• Develop and implement an Industrial Stormwater Pollution Prevention Plan
(SWPPP) to reduce the potential for stormwater contamination from industrial
activities and other sources such as impacted soils or active construction.
• Diversion and treatment of all flows (i.e., stormwater and dry weather flows) end
of pipe (at Outfall 002) using carbon filtration, up to a given design flowrate.
Similar alternatives include treatment of dry weather flow only (NCCW and
WWTP effluent) end of pipe or treatment of stormwater only end of pipe; these
alternatives would require collection system separation.
These approaches provide differing levels of potential reductions, time to implement, and
cost effectiveness for benefit achieved. The approaches Chemours propose to implement
are presented in the Cape Fear River PFAS Loading Reduction Plan (Geosyntec, 2019a).

Outfall 002 Assessment 5 August 26, 2019
1 INTRODUCTION AND OBJECTIVES
Geosyntec Consultants of NC, P.C. (Geosyntec) has prepared this report for The
Chemours Company FC, LLC (Chemours) to provide an assessment of
hexafluoropropylene oxide dimer acid (HFPO-DA) and perfluoro-2-methoxyacetic acid
(PFMOAA) detected at Outfall 002 at Chemours Fayetteville Works (the Site). This
report is one of four supporting attachments to the Cape Fear River PFAS Loading
Reduction Plan (“Reduction Plan”; Geosyntec, 2019a) required by Paragraph 12 of the
Consent Order among Chemours, the North Carolina Department of Environmental
Quality (NCDEQ) and Cape Fear River Watch which was entered into court on February
25, 2019. This report has been prepared to present data and a technical analysis related to
Outfall 002 pursuant to requirements of Consent Order Paragraph 12(d). Paragraph 12(d)
states:
The burden is on Chemours to demonstrate that the concentrations of
GenX and perfluoro-1-methoxyacetic acid (PFMOAA) detected in Outfall
002 cannot be reduced by at least 80% from baseline levels, including
after measurable storm events, as defined in 40 C.F.R. 122.21(g)(7)(ii),
within 2 years.
This document presents an assessment of HFPO-DA and PFMOAA concentrations at
Outfall 002, including past concentrations and areas, activities and processes contributing
to detections of these two compounds at Outfall 002. The assessment also presents
potential control approaches to reduce concentrations and loadings of HFPO-DA and
PFMOAA and evaluates the potential benefits, challenges, and timelines associated with
the potential control approaches. Proposed commitments to potential control approaches
and an assessment if 80% reductions can be accomplished in two years are presented in
the Reduction Plan (Geosyntec, 2019a).
The remainder of this document is organized as follows:
• Section 2 – Description of Outfall 002 and Site Conveyance Network. This
section presents a description of flows and areas that contribute to the Outfall 002
discharge.
• Section 3 – HFPO-DA and PFMOAA Data Assessment. This section presents
a description of observed temporal trends in HFPO-DA and PFMOAA
concentrations at Outfall 002, calculation of 2018 calendar year loading at Outfall
002, and a description of recent sampling activities and results.

Outfall 002 Assessment 6 August 26, 2019
• Section 4 – Potential Control Approaches. This section presents a description
of potential control approaches for reducing loading to Outfall 002, including
estimated potential reductions at Outfall 002 for each approach, potential
timelines, and implementation considerations.
• Section 5 – Summary. This section presents a summary of Outfall 002 HFPO-
DA and PFMOAA data presented in this document and potential control
approaches to reduce loading of Site-related HFPO-DA and PFMOAA at Outfall
002.
2 DESCRIPTION OF OUTFALL 002 AND SITE CONVEYANCE NETWORK
This section presents an overview of the Site Conveyance Network, including the
different flows that contribute to water discharged at Outfall 002. This discussion
addresses current flows and does not include potential future flows scenarios at the Site.
The Facility is adjacent to the Cape Fear River and draws water from the river. The
Facility returns over 95% of this water via Outfall 002 after being used primarily as non-
contact cooling water (NCCW). Rainfall at the Facility that does not infiltrate to
groundwater runs off through a series of storm drains and ditches.
The Facility has four chemical production areas, shown in Figure 1 and listed below:
• Chemours Monomers Ion Exchange Membrane (IXM) Area;
• Chemours Polymer Processing Aid (PPA) Area;
• Kuraray America northern and southern leased areas (Kuraray America Leased
Areas); and
• DuPont leased area (DuPont Area).
A portion of the intake water from the river is used for process water by Chemours, and
the resulting process wastewater is then collected and transported offsite for disposal.
Therefore, this process wastewater is not discharged back to the river via Outfall 002.
Some intake river water is also used as non-process water, by Chemours and other Site
tenants, and is sent via pipe to the onsite wastewater treatment plant (WWTP). A small
amount of purchased potable water used for sanitary facilities is also sent to the WWTP.
The WWTP also receives and treats process water from Kuraray and DuPont. Treated
WWTP effluent is discharged through Outfall 001, which then combines with flow in the
Open Channel to Outfall 002. The specific operations contributing flow to Outfall 001 to
the Open Channel include the following:
• Kuraray Americas Inc. – Trosifol® Manufacturing Process

Outfall 002 Assessment 7 August 26, 2019
• Kuraray Americas Inc. – SentryGlas® Manufacturing Process
• DuPont Company – Polyvinyl Fluoride Manufacturing Processes
• Stormwater from Kuraray and DuPont Process Areas
• Sanitary (Domestic) Wastewater
• Demineralized Water Regenerate Flow
• Air Compressor Cooling Water
A large portion of river intake water is used as NCCW throughout the Site, which is
transported through the Site Conveyance Network to Outfall 002 and discharged into the
river, as shown in Figure 2.
NCCW from the Chemours PPA Area and Kuraray America Leased Areas are discharged
into the Wood Lined Trench that flows through the western portion of the Site from north
to south. The Wood Lined Trench discharges into the concrete-lined Open Channel to
Outfall 002, just upstream of where the WWTP discharge combines with the Open
Channel. NCCW from the Chemours Monomers IXM area (northeast portion of the
Facility) is conveyed via an open channel/ditch, until it is conveyed underground via a
pipe on the eastern portion of the Site (starting just upstream of the sediment basins). The
NCCW conveyed underground (from north to south) combines with the Open Channel to
Outfall 002, downstream of where the WWTP discharges into the channel.
Open, unlined ditches convey NCCW and steam condensate from the DuPont Area (in
the southeast portion of the Facility), and these ditches ultimately drain into the lined
Open Channel to Outfall 002. However, since the DuPont ditches are not lined, flow in
these ditches has been observed to infiltrate before reaching where the ditches combine
with the channel to Outfall 002. The Open Channel to Outfall 002 flows along the
southern portion of the Site, from west to east, and is discharged to the river through a
pipe. The Site Conveyance Network is illustrated in Figure 3.
Non-process stormwater runoff throughout the Site is conveyed via small ditches,
stormdrain pipes, roof gutters, and downspouts into the Site Conveyance Network and
ultimately discharged via Outfall 002. Operations contributing flow to Outfall 002
include the following:
• River sediment basin water overflow;
• Stormwater from non-process areas;
• Boiler blowdown and condensate;

Outfall 002 Assessment 8 August 26, 2019
• Chemours fluoroproducts manufacturing processes NCCW;
• Kuraray Trosifol® manufacturing process NCCW;
• Kuraray SentryGlas® manufacturing process NCCW;
• DuPont polyvinyl fluoride resin processes NCCW;
• DuPont polyvinyl fluoride resin processes reverse osmosis/capacitive
deionization reject water;
• Outfall 001 effluent;
• Non-contact river water once-through cooling water;
• Steam condensate; and
• Excess river water.
3 HFPO-DA AND PFMOAA DATA ASSESSMENT
This section presents results from sampling activities at the Site that support assessment
of concentration trends and sources for HFPO-DA and PFMOAA detected at Outfall 002.
3.1 HFPO-DA and PFMOAA Temporal Trends
HFPO-DA and PFMOAA analytical results from samples collected from Outfall 002 and
from the Cape Fear River (at a location representing the river intake) were evaluated.
Reported Outfall 002 concentrations for HFPO-DA and PFMOAA between June 2017
and July 2019 are provided in Table 1 and Table 2, respectively. Reported river intake
concentrations for HFPO-DA and PFMOAA between June 2017 and July 2019 are
provided in Table 3 and Table 4, respectively. Daily precipitation data from a nearby
United States Geological Survey rain gauge are provided in Table 5. HFPO-DA
concentrations from June 2017 through July 2019 from samples collected from Outfall
002 are shown in Figure 4. On June 21, 2017, Chemours diverted six process wastewater
types from going to the WWTP and containerized and shipped them for offsite disposal.
Subsequently, between June and July 2017, HFPO-DA concentrations at Outfall 002
decreased by over 99% [from approximately 80,000 nanograms per liter (ng/L) to 120
ng/L from Outfall samples collected on June 14, 2017 and July 27, 2017].
HFPO-DA concentrations at Outfall 002 from August 2017 through July 2019 are shown
in Figure 5. There were several notable events during this period. From October 2017
until June 2018, concentrations at Outfall 002 increased after rainfall and other
precipitation events following the October 2017 scrubber upset and subsequent

Outfall 002 Assessment 9 August 26, 2019
mobilization of HFPO-DA deposited on the soil due to air deposition to the Site
Conveyance Network. Air abatement efforts began in May 2018, and Cooling Water
Channel, sediment basin lining and discharge of water from dewatered excavated
sediment from the previous sediment ponds to the newly lined sediment ponds occurred
in late 2018. Additionally, Thermal Oxidizer construction began in late 2018. Hurricane
Florence occurred in mid-September 2018, which resulted in over seven inches of rainfall
in a single day to the area.
As shown in Figures 4 and 5, although HFPO-DA concentrations measured at Outfall 002
are variable, there is a general downward trend over time. Additionally, despite the
variability in HFPO-DA concentrations, concentrations generally increase during wet
weather, indicating that stormwater is a source of HFPO-DA loading to Outfall 002.
However, even during dry weather, Outfall 002 concentrations are consistently higher
than river intake concentrations, suggesting that the Site Conveyance Network is also
contributing HFPO-DA loading.
PFMOAA concentrations from May 2018 through June 2019 are shown in Figure 6.
There are limited data available for PFMOAA at Outfall 002, and many of the sample
results were non-detects where the detection limit was 210 ng/L. These samples are being
reanalyzed at lower detection limits by the laboratories. Although PFMOAA
concentrations were frequently below the detection limit, several elevated concentrations
were observed at Outfall 002 during 2019. The highest PFMOAA observations at Outfall
002 and the intake sampling location occurred between late May and early June 2019
(Geosyntec, 2019c), which were associated with the use of supplemental rental pumps.
The limited number of available PFMOAA sampling results and the frequency of non-
detect results contribute to uncertainty in PFMOAA loading analyses.
3.2 HFPO-DA and PFMOAA Calendar Year 2018 – Mass Loading
The 2018 calendar year was established as the period for comparison with recent loadings
at Outfall 002 and potential control approaches for this report. Before 2018, all process
water had been diverted from Outfall 002.1
To calculate mass loading over the 2018 calendar year, measured concentration data for
HFPO-DA and PFMOAA were used, in combination with measured flows at Outfall 002.

1 Process wastewater diversion occurred between June 21, 2017 and November 29, 2017. Subsequent to November 29, 2017, process wastewaters from the Chemours Monomers IXM Area have been sent for offsite disposal.

Outfall 002 Assessment 10 August 26, 2019
HFPO-DA and PFMOAA concentrations at Outfall 002 during 2018 are shown in Figure
7 and Figure 8, respectively. Additionally, measured flows from Outfall 001 (the WWTP
effluent) and Outfall 002 are shown in Figure 9. During 2018, there were a total of 100
sample results for HFPO-DA and 12 sample results for PFMOAA. All of the HFPO-DA
results had detected concentrations while half, i.e. six, of the PFMOAA results were non-
detects (detection limit was 210 ng/L).
To calculate loading at Outfall 002, the measured concentrations and flows were
multiplied (with unit conversion factors) to determine the mass loading. To enable
comparative analysis of loading from different sources of flow (to support evaluation of
intervention options), the total loading from Outfall 002 was separated into loads from
stormwater versus loading occurring during dry weather flows. Dry weather loading
encompasses all flows except for stormwater, which includes the WWTP effluent,
NCCW, demineralized water regenerate flow water, river sediment basin water overflow,
and boiler blowdown and condensate. Additionally, because the majority of dry weather
flow, not including WWTP effluent, is NCCW, this contribution is referred to as “NCCW
in the Site Conveyance Network”. The Site Conveyance network is illustrated in Figure
1 and Figure 3.
For baseflow load apportionment, flow data for each day was designated as “wet” or
“dry” based on the total precipitation depth measured on that day and the two preceding
days, with wet days defined as greater than 0.2 inches of precipitation (below this
approximate rainfall threshold, minimal stormwater runoff generation is expected). On
dry days, flow measured at Outfall 002 was subdivided as follows: 𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂 002 𝐹𝐹𝑂𝑂𝐹𝐹𝐹𝐹 = 𝑁𝑁𝑁𝑁𝑁𝑁𝑁𝑁 𝑂𝑂𝑂𝑂𝐹𝐹𝐹𝐹+𝑁𝑁𝑁𝑁𝑊𝑊𝑊𝑊 𝑒𝑒𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑒𝑒𝑒𝑒𝑂𝑂 (𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂 001) 𝑂𝑂𝑂𝑂𝐹𝐹𝐹𝐹
On wet days, NCCW flows in the Site Conveyance Network were assumed to be of
similar flow volumes to NCCW flows on dry days. Therefore, any flow in addition to
WWTP effluent and NCCW in the Site Conveyance Network flows was assumed to be
attributed to stormwater, as shown below: 𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂 002 𝐹𝐹𝑂𝑂𝐹𝐹𝐹𝐹 = 𝑁𝑁𝑁𝑁𝑁𝑁𝑁𝑁 𝑂𝑂𝑂𝑂𝐹𝐹𝐹𝐹+𝑁𝑁𝑁𝑁𝑊𝑊𝑊𝑊 𝑒𝑒𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑒𝑒𝑒𝑒𝑂𝑂 (𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂𝑂 001) +𝑆𝑆𝑂𝑂𝐹𝐹𝑆𝑆𝑆𝑆𝐹𝐹𝑂𝑂𝑂𝑂𝑒𝑒𝑆𝑆
Based on these assumptions, the flow at Outfall 002 from NCCW in the Site Conveyance
Network, WWTP effluent, and stormwater was estimated for each day in the 2018
calendar year, as shown in Figure 9. The 2018 calendar year is in the 97th percentile of
total annual rainfall depth including the record rainfall experienced during Hurricane
Florence in mid-September 2018. Excluding the record rainfall that occurred during the
hurricane, the 2018 calendar year would be in the 44th percentile of total annual rainfall
depth, which is close to a median (50th percentile) rainfall year.

Outfall 002 Assessment 11 August 26, 2019
HFPO-DA and PFMOAA concentrations measured on both dry and wet days were used
to estimate the concentrations that could be attributed to dry weather flows (WWTP
effluent and NCCW in the Site Conveyance Network) and wet weather flows.
Concentrations were estimated based on the equations shown below.
Where,
𝑁𝑁𝑑𝑑 = dry day concentration
𝑁𝑁𝑠𝑠= stormwater concentration
𝑁𝑁𝑤𝑤 = wet day concentration
𝑅𝑅𝑠𝑠𝑑𝑑 = ratio of stormwater to dry weather concentration
𝑉𝑉𝑠𝑠 = portion of Outfall 002 flow that is stormwater
𝑉𝑉𝑑𝑑 = portion of Outfall 002 flow that is from dry weather
• Average stormwater concentration:
𝑁𝑁𝑤𝑤 𝑚𝑚𝑚𝑚𝑚𝑚𝑚𝑚=𝑁𝑁𝑑𝑑 𝑚𝑚𝑚𝑚𝑚𝑚𝑚𝑚𝑉𝑉𝑑𝑑 𝑚𝑚𝑚𝑚𝑚𝑚𝑚𝑚+𝑁𝑁𝑠𝑠 𝑚𝑚𝑚𝑚𝑚𝑚𝑚𝑚𝑉𝑉𝑠𝑠 𝑚𝑚𝑚𝑚𝑚𝑚𝑚𝑚
𝑁𝑁𝑠𝑠 𝑚𝑚𝑚𝑚𝑚𝑚𝑚𝑚 = (𝑁𝑁𝑤𝑤 𝑚𝑚𝑚𝑚𝑚𝑚𝑚𝑚-𝑁𝑁𝑑𝑑 𝑚𝑚𝑚𝑚𝑚𝑚𝑚𝑚 𝑉𝑉𝑑𝑑 𝑚𝑚𝑚𝑚𝑚𝑚𝑚𝑚)/ 𝑉𝑉𝑠𝑠 𝑚𝑚𝑚𝑚𝑚𝑚𝑚𝑚
• Ratio of the stormwater concentration to the average dry day concentration:
𝑅𝑅𝑠𝑠𝑑𝑑=𝑁𝑁𝑠𝑠 𝑚𝑚𝑚𝑚𝑚𝑚𝑚𝑚 /𝑁𝑁𝑑𝑑 𝑚𝑚𝑚𝑚𝑚𝑚𝑚𝑚
• The ratio was used to calculate the stormwater and dry weather concentrations for
each day (where V is based on the day of and two preceding days):
𝑁𝑁𝑑𝑑 = 𝑁𝑁/(𝑅𝑅𝑠𝑠𝑑𝑑 𝑉𝑉𝑠𝑠+ 𝑉𝑉𝑑𝑑)
𝑁𝑁𝑠𝑠 = C/(𝑉𝑉𝑠𝑠+ (
1𝑅𝑅𝑠𝑠𝑠𝑠 )𝑉𝑉𝑑𝑑)
For wet days, the measured flows and concentrations at Outfall 002 were translated into
estimated flows and concentrations from stormwater, NCCW in the Site Conveyance
Network, and the WWTP effluent, while dry days were translated into flows and
concentrations for NCCW in the Site Conveyance Network and the WWTP effluent.
The flows and concentrations discussed above were used to calculate total loading at
Outfall 002 during the 2018 calendar year, subdivided by the estimated contributions
from stormwater and dry weather flows (NCCW in the Site Conveyance Network and the
WWTP effluent). Figure 10 and Figure 11 show loading at Outfall 002 for the 2018
calendar year for HFPO-DA and PFMOAA, respectively. The approximate loading
present in the river intake water (and then subsequently discharged to Outfall 002) is also
illustrated.

Outfall 002 Assessment 12 August 26, 2019
In mid-September, a record rainfall occurred during Hurricane Florence. There was 17.3
inches of rainfall from September 14-16, 2018, which represents 28% of the total annual
rainfall in 2018. The measured flows were estimated to represent 1.4% of the annual
flows to Outfall 002, and the loading from September 14-16 accounts for 2.3% of the
total 2018 loading (for HFPO-DA). This assumes a concentration of 333 ng/L for HFPO-
DA at Outfall 002 during this event, since it was not possible to collect a sample at Outfall
002 during the hurricane2.
In the time period evaluated, stormwater is a relatively small contribution to Outfall 002
in terms of flow. However, Figures 10 and 11 show that it is a significant contribution to
loading (due to its relatively higher concentrations), representing approximately 45% and
31% of HFPO-DA and PFMOAA loading at Outfall 002, respectively. Although
concentrations from the WWTP effluent (Outfall 001) were generally higher than
concentrations measured at Outfall 002, the WWTP effluent is estimated to contribute a
relatively smaller load due to the low flows representing 2% of HFPO-DA loading at
Outfall 002.
3.3 Paragraph 11(c) Bimonthly Sampling
Paragraph 11(c) of the executed Consent Order requires that Chemours submit quarterly
reports to NCDEQ identifying Per- and polyfluoroalkyl substances (PFAS) constituents
and concentrations in all process and non-process wastewater and stormwater at the
Facility. To conduct this evaluation, Chemours began conducting bimonthly sampling
events in April 2019 to characterize PFAS in these water types. The second bimonthly
sampling event occurred in June 2019, and further sampling events will occur bimonthly
for up to eighteen months.
Samples collected under Paragraph 11(c) include the raw water intake, process
wastewater, non-process wastewater, and stormwater, including water that is discharged
through Outfall 002. The proposed sample locations for each sampling event are shown
in Figure 12 and are described in the PFAS Characterization Sampling Plan (Geosyntec,
2019d). Samples collected are listed in Table 6. Details on general field methods,

2 Based on the average concentration measured at Outfall 002 during wet weather in the 2018 calendar year.

Outfall 002 Assessment 13 August 26, 2019
sampling methods, and field quality assurance/quality control procedures conducted
during the bimonthly sampling events are described in the First Quarterly Report for
PFAS Characterization (Geosyntec, 2019e).
During the April 2019 and June 2019 sampling events, some sample locations identified
in the PFAS Characterization Sampling Plan (Geosyntec, 2019d) were unable to be
sampled (Table 6) as these locations were dry during the sampling event. There was no
precipitation in the 72 hours leading up to sample collection.3
Concentrations of HFPO-DA and PFMOAA in samples collected during the April 2019
and June 2019 sampling events are presented in Figure 13 and Figure 14, respectively.
Sample results for all PFAS reported under Table 3+ Laboratory Standard Operating
Procedure (SOP) and EPA Method 537 Mod for the April 2019 and June 2019 sampling
events are provided in Table 7 and Table 8, respectively. PFAS results for samples
collected from Chemours wastewater locations (Locations 16, 17A, and 17B) are not
included, because water from these locations is shipped offsite for disposal and is not
discharged through Outfall 002. The data review narrative package and the associated
laboratory reports for these samples, and for other samples discussed in this document,
are provided in Appendix A. Further details on the data review process can be found in
the Seeps and Creeks Investigation Report (Geosyntec, 2019f).
The following observations were made for HFPO-DA and PFMOAA concentrations in
the April 2019 and June 2019 dry events:
• HFPO-DA was detected at Location 1, the intake water from the Cape Fear River,
at 14 ng/L in April and 18 ng/L in June.4
• Samples from non-process wastewater locations (6A, 6B, 24A, 24B, and 24C)
contained low levels of HFPO-DA (ranging from 13 to 66 ng/L) and were non-
detect for PFMOAA. All HFPO-DA concentrations for Chemours non-process
wastewater samples were within 8 ng/L of the concurrent sample of intake water
at Location 1.

3 The April sampling event occurred on 4/24/2019; there was 0.46 inches on 4/19/2019 and 0.02 inches of precipitation on 4/20/2019. The June sampling event occurred on 6/27/2019; there was 0.23 inches of precipitation on 6/22/2019. 4 PFMOAA was not detected at Location 1 during either dry weather sampling event (the detection limit was 210 ng/L for the April event and 5 ng/L for the June event).

Outfall 002 Assessment 14 August 26, 2019
• The highest non-process wastewater-related HFPO-DA concentration during the
April event was in the sample collected at Location 10 (320 ng/L), a Chemours
Monomers IXM Stormwater Discharge area. This section of the channel receives
stormwater from roof drainage and has sediment present in the drainage ditch.
This location was dry during the June event.
• Elevated HFPO-DA and PFMOAA concentrations were observed at locations
23A (April and June) and 23B (June). These locations and the combined influent
to the WWTP (Location 22) were further evaluated through additional sample
collection, and possible sources of the elevated HFPO-DA and PFMOAA
concentrations are discussed further below in Section 3.5.
• The samples collected at Location 20 (Outfall 002) had detectable concentrations
of HFPO-DA (61 ng/L in April and 50 ng/L in June). In April, PFMOAA in the
sample collected at Location 20 was non-detect above the reporting limit (210
ng/L), while in June, PFMOAA was detected at 48 ng/L.
The 2018 loading estimate plots (Section 3.2) show a loading of 44% for HFPO-DA to
Outfall 002 is contributed through dry weather flows, because the loading estimated due
to dry weather flows (NCCW in the Site Conveyance Network and the WWTP effluent)
is higher than the estimated river intake loading. Based on the data collected during the
April and June sampling events, in addition to typical flows contributed to the Site
Conveyance Network from different parts of the Facility, the total loading to Outfall 002
from NCCW in the Site Conveyance Network was separated into the major components
of the network (Figure 3 illustrates the major components). As shown in Table 9, the
Cooling Water Channel (in the northeast portion of the Facility) and the Open Channel
to Outfall 002 (located along the southern border of the Facility5) are estimated to
contribute the most load to Outfall 002, based on available data. These data show
variability in the percent loading from each section of the Site Conveyance Network,
suggesting that load reduction estimates of control measures that target particular sections
(reported later) will have uncertainty that is proportionate to these ranges.

5 The Open Channel to Outfall 002 begins where the Wood Lined Trench terminates and flows until Outfall 002. Flows from the WWTP effluent and the Cooling Water Channel also discharge into this channel.

Outfall 002 Assessment 15 August 26, 2019
Table 9. Loading Estimates to Outfall 002 Added Throughout the Site Conveyance Network during Dry Weather (for HFPO-DA); Intake contributions are not counted in these values.
Location1,2,3
Approximate HFPO-DA Loading Added to Outfall 002
(through Site Conveyance Network)
4/24/2019 6/27/2019 Average
Load (lb/day)
% of Total Load
Load (lb/day)
% of Total Load
Load (lb/day)
% of Total Load
Wood Lined Trench 0 0% 0.00031 5% 0.00015 2%
Cooling Water Channel 0.0020 24% 0.0031 48% 0.0026 36%
Wastewater Treatment Plant Effluent 0.00058 7% 0.00055 9% 0.00056 8%
Open Channel to Outfall 002 0.0057 69% 0.0025 38% 0.0041 53%
1 This assessment assumes flow in the ditches from the DuPont Area are infiltrated and no flow discharges into the
Open Channel to Outfall 002

2 The intake loading represented 29% of the total HFPO-DA load exiting Outfall 002 in the April 2019 event and
55% of the total HFPO-DA load exiting Outfall 002 in the June 2019 event.

3 Loads are calculated based on concentrations measured during the dry weather sampling events and estimated flows
on the day sampling occurred from each loading source (using measured flow at Outfall 002 on the day
sampled).occurred and typical flows from the various loading sources, based on data from December 2017 through
May 2019).

3.4 Stormwater Sampling
Concentrations of HFPO-DA and PFMOAA in stormwater runoff are needed to consider
the effectiveness of potential stormwater control measures. A stormwater sampling event
was therefore conducted to collect and analyze grab samples of stormwater throughout
the Site (i.e., from drainage ditches or channels before stormwater enters the Site
Conveyance Network and mixes with dry weather flows). Sampling was planned for
storms having these forecasted characteristics: at least 70% chance of rain predicted to
last at least 4 hours, at least 0.5 inches of rainfall, and an antecedent dry period lasting at
least 72 hours. Grab sample collection started once 0.1 inches of rain had fallen and when
runoff was observed to occur. Samples were also analyzed for total and dissolved PFAS,
total suspended solids (TSS), and particle size distribution. Additionally, six pressure
transducers (micro-divers) were installed in defined channels/ditches collecting

Outfall 002 Assessment 16 August 26, 2019
stormwater only in order to collect continuous measurement of pressure/depth6
throughout sampling period to support estimates of stormwater flows.
Stormwater samples were collected on June 5, 2019. The proposed sample locations are
shown in Figure 15. Not all locations planned for sampling were successfully sampled
due to lack of flow at some locations and time limitations during the relatively short rain
event. Concentrations of HFPO-DA and PFMOAA in samples collected during the June
2019 stormwater sampling event are presented in Figure 16. Sample results for all PFAS
reported under Table 3+ Laboratory SOP and EPA Method 537 Mod are provided in
Table 10. Additional stormwater sampling events are planned to further assess
stormwater PFAS levels and contributing areas within the Facility to potentially support
reduction actions.
The following observations were made for HFPO-DA and PFMOAA concentrations in
the June 2019 stormwater sampling event:
• Stormwater concentrations were generally higher than those measured at Outfall
002, particularly during dry weather. The median concentration of HFPO-DA
measured at Outfall 002 during dry weather (in 2018 and 2019) was 87 ng/L, and
the median concentration of HFPO-DA during wet weather was 235 ng/L
(additionally, data has shown that concentrations are higher at Outfall 002 during
large storm events vs. small storm events). The median stormwater concentration
of HFPO-DA measured during the June 2019 stormwater sampling event was 370
ng/L, confirming that stormwater concentrations are higher than other dry weather
flow sources to Outfall 002.
• Stormwater concentrations were spatially variable throughout the Facility, with
certain sample clusters indicating potential areas of higher loading. If these spatial
patterns are corroborated in future sampling events, targeted stormwater treatment
could potentially be prioritized in these areas to measurably reduce loading to
Outfall 002 during wet weather.
• Both HFPO-DA and PFMOAA were elevated at sampling Location 42 (46,000
ng/L for HFPO-DA, 105,000 ng/L for PFMOAA, 5,400 ng/L for HFPO-DA, and
42,000 ng/L for PFMOAA). These samples represent runoff from rooftop gutters

6 Two pressure transducers (micro-divers) were also installed to represent atmospheric pressure.

Outfall 002 Assessment 17 August 26, 2019
(from the Chemours Monomers IXM area) going to the Site Conveyance
Network.
• Location 10 was also elevated (3,500 ng/L for HFPO-DA and 2,200 ng/L for
PFMOAA). This sampling location represents stormwater discharge from the
Chemours Monomers area. Water mixed with sediment sample results were also
elevated in the Chemours Monomers IXM area (discussed in Section 3.6),
compared to limited results from other sampling locations.
• Locations 2 and 3 were relatively elevated for HFPO-DA (940 ng/L for Location
2 and 1,800 ng/L for Location 3). These locations drain the northwest corner of
the Facility.
• Dissolved PFAS and TSS concentrations in stormwater samples were also
analyzed, to understand pollutant form and treatability. Samples were filtered at
the laboratory prior to analysis. In these samples, and sample preparation
sequence, dissolved concentrations were generally equivalent to total
concentrations, indicating that these chemicals are predominantly in dissolved
form, which may limit the potential effectiveness of traditional stormwater source
control measures (e.g., soil tackifiers and other erosion and sediment controls that
focus on holding surface soils in place) and treatment control measures (which
more effectively reduce particulate-associated pollutants).
• Additionally, there was no relationship between TSS for either total or dissolved
PFAS concentrations. This suggests that the mobilization pathway for PFAS in
stormwater is via a land surface wash-off process that occurs without associated
particulate wash-off (i.e., a colloidal or salt-like, soluble form of the pollutant may
exist on the land surface and is rinsed into suspension during rainfall-runoff).
3.5 Supplemental Wastewater Treatment Plant Sampling
Supplemental wastewater samples were collected on July 16-18, 2019, from locations
along the terracotta pipe upstream and downstream of the WWTP to gather additional
data on PFAS concentrations in water that is processed at the WWTP before reaching
Outfall 001 and then Outfall 002. Simultaneous 24-hour composite samples were
collected at the following locations (Figure 17):
• Location 1 (excess river water)
• Location 18 (Kuraray Trosifol® process wastewater)
• Location 23A-1 (Kuraray SentryGlas® process wastewater)

Outfall 002 Assessment 18 August 26, 2019
• Location 23A-2 (Kuraray laboratory process wastewater).
• Location 23A (combined process wastewater from Kuraray SentryGlas® and
laboratory)
• Location 22 (WWTP combined influent) – during sample collection at this
location, sediment caused a blockage in the autosampler tubing, so the sample
was composited over approximately 8 hours instead of 24 hours. The sediment
may have affected the sample results as described below.
• Location 8 (WWTP effluent at Outfall 001) – this sample was collected one day
later than the other samples over 24 hours. One day represents the estimated
hydraulic residence time of water flowing through the WWTP.
The samples were sent to the Chemours onsite laboratory and TestAmerica Sacramento
(TestAmerica) for Table 3+ Laboratory SOP analysis. Results reported here are from the
onsite laboratory and are being used for indicative purposes, as results from TestAmerica
are pending at the time of report submission. Concentrations of HFPO-DA and PFMOAA
in samples collected upstream and downstream of the WWTP are shown in Figure 18.
Sample results for all PFAS reported under Table 3+ Laboratory SOP are provided in
Table 11. Below are observations from this sampling event:
• Elevated HFPO-DA and PFMOAA concentrations at Location 22 do not
correspond to similar levels directly upstream (Location 23A) or in the effluent
(Location 8). The autosampler at this location became clogged with sediment
roughly 8 hours into the integration time. The sediment clogging of the sampler,
and direct upstream samples having lower concentrations suggests that the
elevated PFAS concentrations observed in the sample at Location 22 are affected
by sediment.
• Elevated HFPO-DA (9,395 ng/L) was observed at Location 23A-1 (Kuraray
SentryGlas® process wastewater) and at Location 22 (2,637 ng/L, the WWTP
combined influent). A lower concentration was observed at Location 8 (53.7 ng/L,
the WWTP effluent).
• Elevated PFMOAA was observed at Location 23A (597 ng/L, combined Kuraray
process water) and at Location 22 (1,589 ng/L, the WWTP combined influent).
PFMOAA was non-detect above the reporting limit (10.6 ng/L) in the WWTP
effluent (Location 8).
• The elevated HFPO-DA observed in the sample collected from Location 23A-1
(9,395 ng/L) does not appear represent a significant source of mass loading to
downstream Location 23A where the HFPO-DA concentration was 65.9 ng/L.

Outfall 002 Assessment 19 August 26, 2019

3.6 Supplemental Conveyance Network Sediment Sampling (Dry Weather)
Supplemental dry weather sampling was conducted on July 3, 2019 where sediment
samples were collected from Cooling Water Channel locations with sediment
accumulation. Sample collection was attempted in the Open Channel to Outfall 002, but
the sediment had too many fines to be able to collect the sample through the existing
water column and flow. The samples were collected to evaluate the potential for
desorption from these sediments to contribute to observed PFAS concentrations at Outfall
002. Composite samples were created from sediment grab samples. The locations of these
samples are show in in Figure 19 and are listed below:
• Sediment Location C (SD-DNSS-C, Cooling Water Channel; immediately before
joining with the Open Channel to Outfall 002)
• Sediment Location F (SD-DNSS-F, Cooling Water Channel; south of Chemours
Monomers IXM Area)
• Sediment Location G (SD-DNSS-G, Cooling Water Channel; north and west of
Chemours Monomers IXM Area)
These samples were collected before a Table 3+ solids method had been developed by
external laboratories. To facilitate an assessment of the potential presence of Table 3+
PFAS associated with the Site, equal masses of deionized water and sediment
(approximately 100-g each) were combined together in a high-density polyethylene
(HDPE) bottle and mixed together. The sediment-water mixture samples were sent to the
Chemours onsite laboratory and TestAmerica for Table 3+ Laboratory SOP analysis.
Results discussed here are from the onsite laboratory since results from TestAmerica are
pending. The overlying water was extracted from the samples and analyzed to semi-
quantitatively assess the PFAS levels in the samples. Aqueous HFPO-DA and PFMOAA
reported results from these analyses are shown in Figure 20. Sample results for all PFAS
reported under Table 3+ Laboratory SOP are provided in Table 12.
Reported HFPO-DA and PFMOAA levels were highest at Sediment Location G (1,400
ng/L and 560 ng/L, respectively). Sediment Location F was observed to have HFPO-DA
detected at 3,120 ng/L while PFMOAA was non-detect at reporting limit of 11 ng/L.
Sediment Location C was observed to have the lowest HFPO-DA concentration at 26
ng/L and PFMOAA was non-detect at a reporting limit of 11 ng/L. These results suggest
that sediments present in the Cooling Water Channel around Monomers IXM Area may
represent a source of PFAS that can originate from the sediment and contribute to Outfall
002.

Outfall 002 Assessment 20 August 26, 2019
3.7 Supplemental Outfall Channel Sampling (Dry Weather)
Supplemental dry weather water samples were collected on May 30, 2019 along the Open
Channel to Outfall 002 to evaluate whether possible groundwater infiltration was
affecting the variability of PFAS concentrations in the Open Channel. The samples were
collected from along the Open Channel to Outfall 002 after the last conveyance network
tributary joins the channel (Figure 21). Samples at Locations 20B, 20C, and 20D were
collected as spatial composite samples, where three grab samples were collected from
just below the water surface using a dip rod at three points along the width of the open
channel, then composited together in a stainless-steel vessel and poured into HDPE
bottles. Downstream of Location 20D, the sample at Location 20E was collected from
within the sump at Outfall 002 as a grab sample using the autosampler at that location.
Concentrations of HFPO-DA and PFMOAA in the supplemental outfall channel samples
are presented in Figure 22. Sample results for all PFAS reported under Table 3+
Laboratory SOP and EPA Method 537 Mod are provided in Table 13.
HFPO-DA concentrations in samples collected along the Open Channel, upstream of
Outfall 002 (Locations 20B, 20C, and 20D) were either non-detect (reporting limit 86
ng/L) or were detected between 89 ng/L and 130 ng/L. The sample collected at Location
20E, downstream of Outfall 002 in the sump, similarly had detectable HFPO-DA at 110
ng/L.
Each of the supplemental outfall samples had elevated PFMOAA compared to results for
Location 20 (2,400 ng/L to 2,800 ng/L), along with several other PFAS that are non-
detect or detected at much lower concentrations at Location 20. In addition, temporal
composite samples collected around the same time (May 28-31, 2019) from Outfall 002
had elevated concentrations of several PFAS compared to results earlier in 2019 including
PFMOAA (Figure 8). These observations are discussed in more detail in the Observations
of Elevated PFAS Concentrations at the Cape Fear River Intake and Outfall 002 Sample
Locations in May and June 2019 (Geosyntec, 2019c).
The primary sample at Location 20B, along with the samples at 20C, 20D, and 20E, show
an increase in HFPO-DA concentrations upstream to downstream along the Open
Channel to Outfall 002 consistent with the April and June 2019 bimonthly sampling event
observations. The duplicate sample collected at Location 20B, however, shows an HFPO-
DA concentration similar to downstream Location 20E which is inconsistent with earlier
observations provided by the same laboratory (TestAmerica). Future bimonthly sampling
data will be evaluated to determine if the observations from the April and June events
occur again. The Cape Fear River PFAS Loading Reduction Plan (Geosyntec, 2019a)
also outlines additional assessment activities to first remove any sediment from this

Outfall 002 Assessment 21 August 26, 2019
portion of the channel and second to examine if the potential for groundwater intrusion
exists.
3.8 Observations from Data Assessment
The 2018 calendar year loading for HFPO-DA and PFMOAA to Outfall 002, as presented
in Section 3.2, shows that stormwater and dry weather flows are both significant
contributions to the Outfall 002 total 2018 loading. Stormwater is approximately 45% of
the total loading and dry weather flows are approximately 55% of the total loading.
NCCW in the Site Conveyance Network is approximately 53% of the total loading. The
WWTP effluent does not contribute significant loading to Outfall 002, due to the
relatively small effluent flows. There is, however, a significant difference between the
total loading contributed to Outfall 002 from NCCW in the Site Conveyance Network
and estimated loading from the river intake, significant loading is being added along the
Site Conveyance Network.
Stormwater sampling results show that stormwater concentrations are higher than dry
weather concentrations measured at Outfall 002 and along the Site Conveyance Network.
This confirms the hypothesis that stormwater runoff contributes significant loading to
Outfall 002, even though it is a relatively small volume contribution compared to other
dry weather sources of flow (i.e., NCCW). Additionally, there were several sampling
location clusters throughout the Site with elevated concentrations in stormwater.
3.9 Data Needs and On-going Assessment Activities
Critical data gaps related to this assessment were identified, and Chemours is committed
to continuing efforts to fill these data gaps. Further data are needed to assess spatial
patterns of stormwater and dry weather concentrations of HFPO-DA and PFMOAA
throughout the Site. Additional stormwater data will assist in confirming or identifying
additional areas with relatively higher stormwater loads and what reduction might be
yielded from capturing and treating stormwater from these areas. Additionally, dry
weather data will contribute to the understanding of dry weather concentration increases
observed along the Cooling Water Channel and Open Channel to Outfall 002 and what
control approaches addressing the Site Conveyance Network may potentially yield.
Chemours is committed to continuing these sampling campaigns and source
investigations to answer key questions and inform the selection and design of future
control measures.

Outfall 002 Assessment 22 August 26, 2019
4 POTENTIAL CONTROL APPROACHES
This section presents nine potential control approaches and their rationale. Estimated
benefits (i.e. reductions in loading from Outfall 002) are also provided.
As shown in Section 3.2, the 2018 calendar year loading to Outfall 002 includes
contributions from both stormwater and dry weather sources. In evaluating the ability to
potentially achieve the reduction targets for HFPO-DA or PFMOAA, given that neither
stormwater nor NCCW in the Site Conveyance Network alone contribute 80% of the load,
there is a need for control approaches that address each of these sources. The following
subsections outline details of the potential control approaches, and Table 14 summarizes
the different control approaches (organized based on their potential to reduce dry weather
vs. wet weather [i.e., stormwater] loading) and their potential to reduce HFPO-DA and
PFMOAA loading to Outfall 002.
4.1 Investigate and Control Dry Weather Sources to the Cooling Water Channel
Characterization data from the Site Conveyance Network indicate increasing PFAS
concentrations along the Cooling Water Channel. The Cooling Water Channel is an open
channel around Monomers IXM but then becomes an underground pipe that emerges
around the DuPont Area. By investigating, locating, and controlling other (non-sediment)
dry weather sources to the Cooling Water Channel, any ongoing source inputs (e.g.,
existing sediments, new windblown soils, groundwater, stormwater) would be prevented.
Presumably, concentrations along this section of the Site Conveyance Network would
remain around river intake levels, thereby reducing a source estimated to contribute
between 24% to 48% of the dry weather HFPO-DA load from the Site Conveyance
Network to Outfall 002. The other actions that would reduce Cooling Water Channel
loads are targeted sediment removal (Section 4.2), targeted stormwater source control and
treatment (Section 4.6), and a Stormwater Pollution Prevention Plan (SWPPP; Section
4.8)
4.2 Targeted Sediment Removal
Soils onsite contain PFAS from historical aerial deposition. If soils from the Site enter
the Site Conveyance Network becoming sediments, they can potential contribute to PFAS
loads detected at Outfall 002. Analyses of sediment samples from the Cooling Water
Channel demonstrated that PFAS from sediments can enter water, therefore existing
sediments along the Conveyance Network have the potential to contribute to PFAS
detected at Outfall 002, particularly during conditions when sufficient contact time allows
such diffusion processes to occur (e.g., during slower, shallower dry weather flows).
Characterization data along certain sections of the Site Conveyance Network and two

Outfall 002 Assessment 23 August 26, 2019
dry-weather bimonthly characterization events indicate increases in PFAS concentrations
that could potentially be from existing sediments along the Cooling Water Channel and
in the Open Channel to Outfall 002.
This potential action involves removing sediment present along sections of the Site
Conveyance Network where sediments may have contributed to PFAS loading at Outfall
002: the open section of the Cooling Water Channel and the Open Channel to Outfall
002. This action could potentially be performed by Chemours during the yearly
turnaround (next scheduled for October 2019) when the Site pauses activities, including
passing water through the Site Conveyance Network, to perform yearly preventative
maintenance.
At present, the expected reductions in PFAS loading to Outfall 002 from removing these
sediments cannot be accurately quantified.
4.3 Assess Potential for Groundwater Intrusion
Along a portion of the Open Channel to Outfall 002 near the DuPont Area during dry
weather, concentrations have been observed to increase along this section of open
channel, without observable point source inputs. This suggests a diffuse source along this
section of the Open Channel. The source of these increased HFPO-DA concentrations
has not been determined but may be potentially related to:
• Sediments in the channel. Sediment samples in the Open Channel were too fine
and could not be reliably collected during normal operating periods. These
sediments can be removed as per the action described in Section 4.2, and samples
of the removed sediment would be sent for analysis of PFAS concentrations; and
• Potentially perched zone groundwater containing HFPO-DA infiltrates into the
Open Channel to Outfall 002. Perched zone groundwater levels along the Open
Channel near the DuPont Area may potentially be higher than water levels in the
Outfall Channel, and groundwater in this area contains HFPO-DA at
concentrations higher than in Outfall 002 (66,000 ng/L at PZ-24). The Outfall
Channel is lined with a grout-filled revetment mat and underlain with Geotextile
to limit connectivity with the surrounding environment. If groundwater levels are
higher than water levels in the Open Channel, then groundwater intrusion is
possible in principle but may be limited by the materials from which the channel
is constructed.

Outfall 002 Assessment 24 August 26, 2019
4.4 Decommission and Replace the Remaining Portion of the Terracotta Pipe
A terracotta pipe was used prior to June 21, 2017 to transmit Chemours process
wastewater from the Monomers IXM Area to the WWTP. The terracotta pipe is presently
still being used to transmit process and some NCCW from Kuraray operations and filter
wash water stream from the Power Area to the WWTP. On November 29, 2019,
Chemours severed the connection from the Monomers IXM area to the terracotta pipe. In
February 2019, Chemours grouted the east-west section of the terracotta pipe to limit the
potential for stormwater or groundwater to enter this section of the pipe and then be
transmitted to the Cape Fear River via the terracotta pipe and WWTP (Geosyntec, 2019g).
Sampling conducted in April, June, and July 2019 of locations along the terracotta pipe
indicate that PFAS are still present in the pipe, potentially adhered to remnant sediments
or potentially infused onto/into the clay pipe itself as described in Sections 3.3 and 3.5
this report. Kuraray and Chemours are planning to decommission the terracotta pipe and
replace it with an above ground pipe.
4.5 Continue Air Abatement Measures
Pursuant to the Consent Order, Chemours is implementing air abatement measures which
will “reduce Facility-wide annual air emissions of GenX Compounds by at least 99%
from 2017 Total Reported Emissions,” including the installation by the end of this year
of a Thermal Oxidizer that will control all PFAS routed to it at an efficiency of 99.99%.
Chemours has already completed implementation of the following air emissions control
measures: enhanced leak detection and repair controls, carbon bed for Vinyl Ethers North
(VEN) indoor air fugitives, and carbon bed for PPA indoor air fugitives and scrubber exit
(completed by May 2018); installation of secondary scrubber (completed by November
2018); routing of secondary scrubber to the VEN carbon adsorption unit (completed by
December 2018); and carbon bed for Vinyl Ethers South indoor air and scrubber exit
(completed by June 2019). Pursuant to the Consent Order, Chemours will complete
installation of the Thermal Oxidizer by December 2019.
These emissions reductions have and will continue to reduce PFAS loading to the land
surface and over time reduce concentrations of PFAS in surface soils and on surfaces as
PFAS are flushed through the environment. These reductions will lead to reductions in
stormwater concentrations as surface runoff will encounter and mobilize less PFAS on
soils and surfaces (and rainfall that contacts the Site will contain less PFAS). At present,
it is not possible to accurately estimate the degree of stormwater runoff PFAS reductions
that will be achieved in a two- to five-year timeframe. This is due to uncertainties in the
fate and transport interactions of all PFAS at the Site with Site soils and surfaces, and a
lack of reference sites with similar chemicals and dynamics to provide indicative

Outfall 002 Assessment 25 August 26, 2019
estimates of the rate of reduction over time. However, reductions in estimated stormwater
concentrations have been observed since 2018 and are believed to be due in part from
these air abatement measures.
4.6 Implement Targeted Stormwater Source Control and/or Treatment
Results from the stormwater sampling event indicated areas of elevated PFAS
concentrations in stormwater. This suggests that some combination of targeted source
control and stormwater collection and treatment could achieve mass loading reductions.
At present, only one high resolution stormwater grab sampling event has been possible
due to rainfall patterns since April 2019. Consequently, additional data are still being
collected to develop a better understanding of stormwater levels and spatial patterns
throughout the Site (two additional stormwater grab sampling events remain planned).
Potential targeted source control could include capping of certain areas or replacement of
materials. Targeted treatment could also consist of either carbon filtration or ion
exchange, new stormwater collection systems (e.g., drain inlets or catch basins), pump
stations, local storage and pretreatment (as needed), and piping to discharge treated flows
back into the Site Conveyance Network.
Additionally, a long-term continuous simulation hydrologic model is being developed for
the site, using EPA’s Stormwater Management Model (SWMM). The model is based on
a local rain gauge data, local hydrologic soil type data, onsite drainage plans, and onsite
imperviousness data. The model will be calibrated using onsite flow measurements to
determine candidate areas for cost-effective storage and treatment sizing ranges, and the
resulting percent runoff volume capture (as required for load reduction estimation).
4.7 Treat Stormwater End of Pipe
A potential control approach involves treating stormwater flows “end of pipe” (i.e., at
Outfall 002), up to a given design flowrate. Currently, dry weather flows and stormwater
are conveyed to Outfall 002 via a combined network. A potential approach involves
constructing a separate collection system for either stormwater or NCCW to achieve
segregation of these flows. This would allow for treatment of either the stormwater or dry
weather flows end of pipe. Presumably this treatment would prioritize stormwater, given
its higher concentrations, so that greater load reduction would be achieved for the same

Outfall 002 Assessment 26 August 26, 2019
treatment system design flowrate and cost.7 Collection system separation and treatment
of stormwater from the entire Site would require significant cost and time to plan, design,
permit and construct, and significant cost to operate and maintain given the expected
required pace of carbon replacement or regeneration.
This option could possibly reduce most of the stormwater load, with the reduction
determined based on the proposed storage volume and treatment system design flowrate,
which can be translated to a percent of annual stormwater volume that is treated using the
SWMM continuous hydrologic model. The required storage volume and treatment
flowrate for this scenario would be very large, and the cost is expected to be similarly
extremely high relative to other potential control options and to the benefits that would
be realized, given the already low contribution of Outfall 002 to river loadings.
4.8 Stormwater Pollution Prevention Plan (SWPPP)
Industrial SWPPPs provide facility-specific guidance on stormwater best management
practices, such as good housekeeping practices, exposure minimization, and erosion
controls. Implementation of the SWPPP reduces the potential for stormwater
contamination from industrial activities and known sources, such as impacted soils or
active construction or soil stockpiling.
Based on the one stormwater sampling event, PFAS concentrations were not elevated
near construction areas or soil stockpiles. These data also did not indicate any relationship
between PFAS and TSS. The presence of sediment in the Cooling Water Channel with
PFAS detections, however, suggests that reducing sediment entering and residing in the
Site Conveyance Network is a best practice that may limit the potential for PFAS
contributions to Outfall 002.
4.9 Treat All Flows End of Pipe
A potential control approach involves treating all flows (i.e., stormwater and dry weather
flows) end of pipe (at Outfall 002), up to a given design flowrate. This option would not
require collection system separation; therefore, the existing Site Conveyance Network
could remain. This would require a new diversion structure above Outfall 002, a new

7 When little or no stormwater is present, dry weather flows could be pumped to the treatment system as needed, if there is benefit to make constant and maximal use of the treatment system capacity. This dry flow could be drawn from near Outfall 002, or particular, higher concentration sections of the Site Conveyance Network (e.g., the Cooling Water Channel) to “optimize” the load reduction achieved by the treatment system.

Outfall 002 Assessment 27 August 26, 2019
pump station, a new storage tank, and a new treatment system similar to that described in
the Treat Stormwater End of Pipe control approach (discussed in Section 4.7). Treated
flows would be discharged back into the Open Channel above Outfall 002.
It would be possible for this option to achieve the 80% load reduction target, with a design
flowrate and storage volume that achieves 100% dry weather flow capture and significant
stormwater flow capture (73% of stormwater flow, in the 2018 calendar year). The
required storage volume and treatment flowrate for this scenario would be extremely
large, and the cost would also be extreme relative to other potential control options and
to the benefits that would be realized, given the already low contribution of Outfall 002
to river loadings.
.
4.10 Summary of Potential Control Approaches
Table 14 includes a summary of potential control actions, including estimated potential
reductions to Outfall 002.

Outfall 002 Assessment 28 August 26, 2019
Table 14. Potential Control Approaches and Estimated Load Reductions
Action # Category Potential Actions
Potential Completion Date
Potential Load Reduction to Cape Fear River Loading (for HFPO-DA, compared to 2018)1
Lower Estimate of Potential Reductions (for HFPO-DA) as compared to 20182, 3, 4
Best Estimate of Potential Reductions (for HFPO-DA) as compared to 20182, 3, 4
Notes on Estimated Reduction
0
DRY interventions that could be expected to appreciably reduce load
Completed (Dry Weather) Interventions Since the End of 2018
End of 2018 0.3% - 8%
Based on observed reductions in dry weather loading since 2018 (calculated from measured flows and concentrations at Outfall 002 in 2018 and 2019. 2019 loads were scaled to represent a full year to compare with 2018 loads).
1
Investigate and Control Dry Weather Sources to the Cooling Water Channel
2-4 years 0.4% 4% 8%
NCCW in the Site Conveyance Network is estimated to contribute 53% of the total 2018 loading to Outfall 002 (of HFPO-DA), although approximately 11% of this is from the river intake water. Therefore, 42% of the Outfall 002 load is generated or added within the Site Conveyance Network (Cooling Water Channel, Wood Lined Trench, Open Channel to Outfall 002). Based on the estimates in Table 9 (which used the [average] observed difference in concentration between the intake and at the bottom of the Cooling Water Channel [Location 15] from both the May and June sampling events), the Cooling Water Channel is assumed to contribute 36% of the loading added to Outfall 002 from the Site Conveyance Network (including the WWTP effluent) during dry weather. The low and "best" estimates for potential reductions assume 25% and 50% reduction of all of the load from the Cooling Water Channel, respectively.
2 Targeted Sediment Removal 1 year NQ NQ NQ
Not quantifiable at this time. Sediments do contribute some
loading in the cooling water channel based on analysis results for PFAS in water contacting these sediments, but it is not possible to accurately estimate the degree this contributes to dry weather loading.

Outfall 002 Assessment 29 August 26, 2019
Action # Category Potential Actions
Potential Completion Date
Potential Load Reduction to Cape Fear River Loading (for HFPO-DA, compared to 2018)1
Lower Estimate of Potential Reductions (for HFPO-DA) as compared to 20182, 3, 4
Best Estimate of Potential Reductions (for HFPO-DA) as compared to 20182, 3, 4
Notes on Estimated Reduction
3
Assess Potential for Groundwater Intrusion (Open Channel to Outfall 002)
3-5 years 0.5% 6% 13%
Loading contributions from the Open Channel to Outfall 002 may be attributable in part to sediments present in the channel, potential groundwater entering the channel, or another mechanism not yet identified. Based on the estimates in Table 9 (which used the [average] observed difference in concentration between locations in the Open Channel to Outfall 002 [Locations 7B and 15] and Outfall 002 [Location 20] from both the May and June sampling events), the Open Channel to Outfall 002 is assumed to contribute 53% of the loading added to Outfall 002 from the Site Conveyance Network (including the WWTP effluent) during dry weather. The low and "best" estimates for potential reductions assume 25% and 50% reduction of all of the load from the Open Channel to Outfall 002, respectively.
4 Decommission Terracotta Pipe 2 years 0.1% 1% 2%
The loading from Outfall 001 (WWTP effluent) was estimated to only be 2% of the total Outfall 002 loading (in 2018). Assuming sediment in the pipes is contributing all of the load to the WWTP, 2% reduction would be achieved.
5
WET interventions that could be expected to appreciably reduce load
Continue Air Abatement Measures End of 2019 - - -
Not quantifiable at this time. A longer time period is needed to evaluate long-term effects of these measures. Over time this will reduce stormwater loading as HFPO-DA and PFMOAA aerial deposition rates are being reduced by 99%.
6
Implement Targeted Stormwater Source Control and Treatment
4 years 1% 16% 30%
Used the long-term continuous hydrologic model of the Site (including drainage areas to the targeted subareas) to determine best management practices capture volume (approximately 80% of long-term average) and percent of site-wide volume that is from potential targeted areas, then multiplied these by average stormwater concentrations to estimate percent of site-wide load that could be reduced. Assumed 99% concentration reduction of captured stormwater flows.

Outfall 002 Assessment 30 August 26, 2019
Action # Category Potential Actions
Potential Completion Date
Potential Load Reduction to Cape Fear River Loading (for HFPO-DA, compared to 2018)1
Lower Estimate of Potential Reductions (for HFPO-DA) as compared to 20182, 3, 4
Best Estimate of Potential Reductions (for HFPO-DA) as compared to 20182, 3, 4
Notes on Estimated Reduction
7 Treat Stormwater End of Pipe 5 years 2% 31% 40%
Assumed 90% capture of stormwater flows (in 2018) for the best estimate of potential reduction (and 70% capture for the low estimate) and assumed 99% concentration reduction in captured flows.
8
WET interventions that would NOT be expected to appreciably reduce load
Stormwater Pollution Prevention Plan (SWPPP)
1 year - - -
SWPPP development and implementation will focus on good housekeeping practices, exposure minimization, and erosion control, which are designed to control stormwater pollutant sources from existing industrial activities, materials, and equipment and soils. However, these sources are not believed to be contributing PFAS in stormwater runoff at the site (for example, concentrations of PFAS in stormwater at the site were not associated with TSS), therefore this action is not expected to yield significant reduction of stormwater loads, and no reduction quantification was possible at this time. However, it may be possible that reducing soil erosion in wet weather will reduce sediment accumulation along the Site Conveyance Network, which could then reduce sediment contribution to overlying water during dry weather.
9 Comprehensive DRY + WET intervention
Treat All Flows End of Pipe 3 years 3% - 80% Assumed treatment of all dry weather and stormwater flows up to a design flowrate that achieves a load reduction at the 80% target. Assumed 99% concentration removal by treatment.
1 Assumes that the Outfall 002 load contribution is 4.2% of the river load.
2 Calculations are based on the 2018 calendar year loading being approximately 45% contributions from stormwater and 55% contributions from dry weather flow.
These ratios will vary based on the amount of rainfall in future years.
3 While many of these reductions were estimated using 2019 concentration data (which would more closely represent percent reductions from 2019 loads), reductions
are shown consistent across all the control measures (from the 2018 calendar year) for simplicity.
4 Estimated reductions are only shown for HFPO-DA; The amount of PFMOAA data is too limited to make reduction estimates at present.

Outfall 002 Assessment 31 August 26, 2019

5 SUMMARY
The loading estimates for HFPO-DA and PFMOAA to Outfall 002 for the 2018 calendar
year show that stormwater and NCCW in the Site Conveyance Network are the primary
contributors to the Outfall 002 loading, estimated to comprise 45% and 53% of the 2018
calendar year loading, respectively. The river intake is estimated to contribute
approximately 11% of the Outfall 002 loading in 2018. Therefore, approximately 42% of
the total Outfall 002 loading is added from NCCW in the Site Conveyance Network. The
WWTP effluent (at 2%) does not contribute significant loading to Outfall 002, due to the
relatively small effluent flows. The sampling results from within the Site Conveyance
Network during dry weather show that the majority of the dry weather load to Outfall 002
appears to be added in the Cooling Water Channel and the Open Channel to Outfall 002.
A number of possible diffuse source inputs could potentially explain these increases, and
potential control measures are identified to address these. Several of these measures were
evaluated and found to potentially significantly reduce dry weather loading to Outfall
002.
Stormwater sampling results show that stormwater concentrations are higher than typical
concentrations measured at Outfall 002, confirming that stormwater contributes
significant loading to Outfall 002, even though it contributes a relatively small volume
compared to dry weather flow sources (in particular, NCCW). Additionally, there were
several areas throughout the site with elevated concentrations in stormwater.
Nine potential control approaches were presented. These approaches provide differing
levels of reductions, time to implement, and cost effectiveness for benefit achieved.
Additional Site stormwater investigations are presently being performed to refine the
selection and implementation of control approaches. The Reduction Plan (Geosyntec,
2019a) outlines the proposed reduction actions pursuant to Consent Order Paragraph 12
and an assessment of Consent Order Paragraph 12(d) relating to Outfall 002 reductions
of HFPO-DA and PFMOAA.

Outfall 002 Assessment 32 August 26, 2019

6 REFERENCES
Geosyntec, 2019a. Cape Fear River PFAS Loading Reduction Plan. Chemours
Fayetteville Works. August 26, 2019.
Geosyntec, 2019b: Cape Fear River PFAS Mass Loading Model Assessment and
Paragraph 11.1 Characterization of PFAS at Intakes. Chemours Fayetteville
Works. August 26, 2019.
Geosyntec, 2019c. Observations of Elevated PFAS Concentrations at the Cape Fear River
Intake and Outfall 002 Sample Locations in May and June 2019. August, 2019.
Geosyntec, 2019d. PFAS Characterization Sampling Plan. May, 2019.
Geosyntec, 2019e. Quarterly Report #1. Characterization of PFAS in Process and Non-
Process Wastewater and Stormwater. July, 2019.
Geosyntec, 2019f. Seeps and Creeks Investigation Report. August, 2019.
Geosyntec 2019g. Summary of Grouting of East-West Section of Terracotta Pipe from
Chemours Monomers IXM Area. Chemours Fayetteville Works. August 26,
2019.

TABLES

TABLE 1OUTFALL 002 HFPO-DA CONCENTRATIONS (JUNE 2017 - JULY 2019)Chemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC P.C.Field Sample IDSample DateQA/QC Concentrations (ng/L)DA0617-7061406/14/2017--80,000 JDA0617-7061506/15/2017--44,000 JChemours Outfall 002-061917 06/19/2017--39,000 DA0617-7061906/19/2017--42,000 DA0617-7062006/20/2017--37,000 JDA0617-70620A06/21/2017--45,000 DA0617-SE7062106/22/2017--24,000 Chemours Outfall 002-62606/26/2017--19,000 DA0617-SE7062606/27/2017--41,000 DA0617-SE7062706/28/2017--27,000 DA0617-SE7062806/29/2017--15,000 Chemours Outfall 002-070317 07/03/2017--30,000 JDA0717-SE7070307/04/2017--27,000 DA0717-SE7070407/05/2017--17,000 DA0717-SE7070507/06/2017--12,000 DA0717-SE7071007/11/2017--4,100 Chemours Outfall 002-071217 07/12/2017--3,300 DA0717-SE7071107/12/2017--4,500 DA0717-SE7071207/13/2017--3,000 Chemours Outfall 002-071717 07/17/2017--830 DA0717-SE7071707/18/2017--960 DA0717-SE7071807/19/2017--880 DA0717-SE7071907/20/2017--550 Chemours Outfall 002-072417 07/24/2017--150 DA0717-SE7072407/25/2017--170 DA0717-SE7072507/26/2017--130 DA0717-SE7072607/27/2017--120 GW0817-OUTFALL08/01/2017--110 O7080108/01/2017--68 DA0717-SE7073108/01/2017--82 O7080208/02/2017--66 O7080308/03/2017--65 O7080408/04/2017--59 O7080708/07/2017--57 O7080808/08/2017--190 O7080908/09/2017--230 O7081008/10/2017--120 O7081108/11/2017--140 SE7081408/15/2017--170 O7081608/16/2017--140 SE7081508/16/2017--220 O7081708/17/2017--100 O7081808/18/2017--140 O7082108/21/2017--87 O7082208/22/2017--95 O7082308/23/2017--140 O7082408/24/2017--210 O7082508/25/2017--130 O7082808/28/2017--77 O7082908/29/2017--120 O7083008/30/2017--91 O7083108/31/2017--62 O7090109/01/2017--180 O7090509/05/2017--70 O7090609/06/2017--250 O7090709/07/2017--140 O7090809/08/2017--69 O7091109/11/2017--67 J002-09111709/11/2017--64 JO7091209/12/2017--420 O7091309/13/2017--88 O7091409/14/2017--58 O7091509/15/2017--330 JO7091809/18/2017--79 O7091909/19/2017--50 O7092009/20/2017--68 O7092109/21/2017--110 O7092209/22/2017--110 O7092509/25/2017--20 O7092609/26/2017--51 Fay-D-outfall09/27/2017--35 Fay-D-outfall-D09/27/2017Duplicate36 O7092709/27/2017--55 O7092809/28/2017--43 O7092909/29/2017--51 O7100210/02/2017--35 Page 1 of 4August 2019
TABLE 1OUTFALL 002 HFPO-DA CONCENTRATIONS (JUNE 2017 - JULY 2019)Chemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC P.C.Field Sample IDSample DateQA/QC Concentrations (ng/L)O7100310/03/2017--65 O7100410/04/2017--210 O7100510/05/2017--69 O7100610/06/2017--250 Outfall 002-7100910/09/2017--3,700 Outfall 002-7101210/12/2017--740 Outfall 002-7101610/16/2017--390 Outfall 002-7103010/30/2017--2,400 JOutfall 002-7110211/02/2017--290 Outfall 002-7110611/06/2017--86 Outfall 002-7110911/09/2017--130 JOutfalll 002-7111311/13/2017--160 SE7111411/15/2017--59 Outfall 002-7111611/16/2017--130 JSE7111511/16/2017--38 JSE7111611/17/2017--65 JOutfall 002-7112011/20/2017--95 SE7111911/20/2017--88 SE7112011/21/2017--37 Outfall 002-7112211/22/2017--77 SE7112111/22/2017--70 SE7112211/23/2017--72 SE7112311/24/2017--50 Outfall 002-7112711/27/2017--130 SE7112611/27/2017--45 SE7112711/28/2017--34 JSE7112811/29/2017--50 Outfall 002-7113011/30/2017--110 SE7112911/30/2017--96 SE7113012/01/2017--50 Outfall 002-7120412/04/2017--120 SE7120312/04/2017--76 SE7120412/05/2017--160 SE7120512/06/2017--150 Outfall 002-7120712/07/2017--240 SE7120612/07/2017--280 SE7120712/08/2017--290 Outfall 002-7121112/11/2017--2,100 Outfall 002-7121412/14/2017--120 Outfall 002-7121812/18/2017--78 SE7122012/21/2017--740 Outfall002-7122212/22/2017--470 Outfall 002-7122812/28/2017--190 Outfall 002-8010201/02/2018--96 Outfall 002-8010501/05/2018--130 Outfall 002-8010801/08/2018--98 Outfall 002-8011101/11/2018--320 Outfall 002-8011601/16/2018--370 Outfall 002-8011801/18/2018--360 Outfall 002-8012201/22/2018--1,500 SE8012501/26/2018--86 Outfall 002-8012901/29/2018--960 Outfall 002-8020102/01/2018--410 080205-Outfall 00202/05/2018--600 080208-Outfall 00202/08/2018--340 O80212-Outfall 00202/12/2018--420 JO80215-Outfall 00202/15/2018--120 JO80219-Outfall 00202/19/2018--88 O80222-Outfall 00202/22/2018--83 O80226-Outfall 00202/26/2018--140 O80301-Outfall 00203/01/2018--450 O80305-Outfall 00203/05/2018--230 JO80308-Outfall 00203/08/2018--220 O80312 - Outfall 00203/12/2018--150 O80315 - Outfall 00203/15/2018--240 O80319-Outfall 00203/19/2018--140 O80322-Outfall 00203/22/2018--300 O80326 - Outfall 00203/26/2018--380 O80329 - Outfall 00203/29/2018--140 O80402 - Outfall 00204/02/2018--91 O80405 - Outfall 00204/05/2018--91 O80409 - Outfall 00204/09/2018--1,300 O80412 - Outfall 00204/12/2018--120 JO80416 - Outfall 00204/16/2018--690 O80419 - Outfall 00204/19/2018--46 JO80423 - Outfall 00204/23/2018--280 JPage 2 of 4August 2019
TABLE 1OUTFALL 002 HFPO-DA CONCENTRATIONS (JUNE 2017 - JULY 2019)Chemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC P.C.Field Sample IDSample DateQA/QC Concentrations (ng/L)O80426 - Outfall 00204/26/2018--1,100 O80430 - Outfall 00204/30/2018--190 O80503 - Outfall 00205/03/2018--90 O80507 - Outfall 00205/07/2018--85 FAY-SW-002-1-05091805/09/2018--45 80510 - Outfall 00205/10/2018--68 O80514 - Outfall 00205/14/2018--110 O80517 - Outfall 00205/17/2018--110 O50821 - Outfall 00205/21/2018--370 O50824 - Outfall 00205/24/2018--90 O80529 - Outfall 00205/29/2018--300 O80531 - Outfall 00205/31/2018--120 O80604 - Outfall 00206/04/2018--66 O80607 - Outfall 00206/07/2018--59 O80611 - Outfall 00206/11/2018--54 JO80614 - Outfall 00206/14/2018--220 JO80618 - Outfall 00206/18/2018--71 JO80621 - Outfall 00206/21/2018--120 O80625 - Outfall 00206/25/2018--46 JO80628 - Outfall 00206/28/2018--150 JO80702 - Outfall 00207/02/2018--43 O80705 - Outfall 00207/05/2018--38 O80709 - Outfall 00207/09/2018--110 O80712 - Outfall 00207/12/2018--33 O80716 - Outfall 00207/16/2018--53 O80719 - Outfall 00207/19/2018--39 O80723 - Outfall 00207/23/2018--24 O80726 - Outfall 00207/26/2018--38 O80730 - Outfall 00207/30/2018--39 O80802 - Outfall 00208/02/2018--210 O80806 - Outfall 00208/06/2018--230 O80809 - Outfall 00208/09/2018--50 O80813 - Outfall 00208/13/2018--140 O80816 - Outfall 00208/16/2018--83 O80820 - Outfall 00208/20/2018--56 O80823 - Outfall 00208/23/2018--110 O80827 - Outfall 00208/27/2018--36 O80830 - Outfall 00208/30/2018--34 O80904 - Outfall 00209/04/2018--34 O80906 - Outfall 00209/06/2018--26 O80910 - Outfall 00209/10/2018--27 O80920 - Outfall 00209/20/2018--310 O80924 - Outfall 00209/24/2018--87 O80927 - Outfall 00209/27/2018--120 O81001 - Outfall 00210/01/2018--74 O8100410/04/2018--60 O81008 - Outfall 00210/08/2018--58 JO8101110/11/2018--80 O81015 - Outfall 00210/15/2018--400 O81025 - Outfall 00210/25/2018--57 O81029 -Outfall 00210/29/2018--340 O81101 - Outfall 00211/01/2018--53 O81105 - Outfall 00211/05/2018--280 O81108 - Outfall 00211/08/2018--270 O81113-OUTFALL00211/13/2018--390 JO81115-OUTFALL00211/15/2018--390 O81119-OUTFALL 00211/19/2018--190 PF1018-Outfall-00211/20/2018--70 O81126-Outfall 00211/26/2018--350 O81203-Outfall 00212/03/2018--560 O81206-Outfall 00212/06/2018--72 O81210-Outfall 00212/10/2018--710 O81213-Outfall 00212/13/2018--200 O81217-Outfall 00212/17/2018--440 O81221 - Outfall 00212/21/2018--330 O81227 - Outfall 00212/27/2018--120 O81231 OUTFALL 00212/31/2018--430 O90103 - OUTFALL 00201/03/2019--190 O90107 - OUTFALL 00201/07/2019--340 O90110 - OUTFALL 00201/10/2019--110 O90114 - Outfall 00201/14/2019--240 O90117 - Outfall 00201/17/2019--92 O90122 - OUTFALL 00201/22/2019--190 O90125 - OUTFALL 00201/25/2019--340 O90128-OUTFALL 00201/28/2019--85 O90201-OUTFALL 00202/01/2019--88 Page 3 of 4August 2019
TABLE 1OUTFALL 002 HFPO-DA CONCENTRATIONS (JUNE 2017 - JULY 2019)Chemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC P.C.Field Sample IDSample DateQA/QC Concentrations (ng/L)O90204-Outfall 00202/04/2019--91 O90207-Outfall 00202/07/2019--88 O90211-OUTFALL 00202/11/2019--90 O90214-OUTFALL 00202/14/2019--240 O90218-Outfall 00202/18/2019--170 O90221-Outfall 00202/18/2019--130 O90225-Outfall 00202/25/2019--350 90228-outfall 00202/28/2019--54 O90304 - Outfall 00203/04/2019--290 O90307 - Outfall 00203/07/2019--62 O90311 - OUTFALL 00203/11/2019--110 O90314 - Outfall 00203/14/2019--49 O90318-Outfall 00203/18/2019--120 O90321-Outfall 00203/21/2019--72 O90325 - Outfall 00203/25/2019--87 O90328 - Outfall 00203/28/2019--110 090401-Outfall 00204/01/2019--68 090405-Outfall 00204/05/2019--350 SW2019-OUTFALL02-040819 04/08/2019--48 O90409 - Outfall 00204/09/2019--240 O90412 - Outfall 00204/12/2019--73 O90416-OUTFALL 00204/16/2019--140 O90418-OUTFALL 00204/18/2019--48 O90423-Outfall 00204/23/2019--140 O90426- Outfall 00204/26/2019--59 O90430-Outfall 00204/30/2019--58 O90503-Outfall 00205/03/2019--56 O090507-Outfall 00205/07/2019--190 O90509-Outfall 00205/09/2019--290 O90514-Outfall 00205/14/2019--83 O90517- Outfall 00205/17/2019--47 O90528 - Outfall 00205/28/2019--76 O90531 - Outfall 00205/31/2019--68 O90611 - Outfall 00206/11/2019--250 O90614 - Outfall 00206/14/2019--72 O9061806/18/2019--27 O9062006/20/2019--33 O9062506/25/2019--44 O9062706/28/2019--28 O9070107/01/2019--33 O9070307/03/2019--42 O9070807/08/2019--320 O9071207/12/2019--68 Notes:Bold - Analyte detected above associated reporting limitHFPO-DA - hexafluoropropylene oxide dimer acidID - identifierJ - Analyte detected. Reported value may not be accurate or preciseng/L - nanograms per literQA/QC - Quality assurance/ quality control-- - no corresponding QA/QC samplePage 4 of 4August 2019
TABLE 2
OUTFALL 002 PFMOAA CONCENTRATIONS (JUNE 2017 - JULY 2019)
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Sample ID Sample Date Concentrations (ng/L)
080503 OUTFALL 002 05/03/2018 310
FAY-SW-002-1-050918 05/09/2018 340
080524 OUTFALL 002 05/24/2018 370
172250 OUTFALL 002 06/04/2018 700
180567 OUTFALL 002 06/14/2018 260
195273 OUTFALL 002 07/02/2018 <200
207436 OUTFALL 002 07/16/2018 <200
218736 OUTFALL 002 08/02/2018 <200
240652 OUTFALL 002 08/30/2018 <200
249022 OUTFALL 002 09/10/2018 <200
269059 OUTFALL 002 10/04/2018 230
PF1018-Outfall-002 11/20/2018 <200
O90204-Outfall 002 02/04/2019 <210
O90207-Outfall 002 02/07/2019 <210
O90211-OUTFALL 002 02/11/2019 <210
O90214-OUTFALL 002 02/14/2019 <210
O90218-Outfall 002 02/18/2019 <210
O90221-Outfall 002 02/21/2019 <210
O90225-Outfall 002 02/25/2019 <210
90228-outfall 002 02/28/2019 <210
O90304 - Outfall 002 03/04/2019 1,300
O90307 - Outfall 002 03/07/2019 720
O90311 - OUTFALL 002 03/11/2019 <210
O90314 - Outfall 002 03/14/2019 <210
O90318-Outfall 002 03/18/2019 <210
O90321-Outfall 002 03/21/2019 <210
O90325 - Outfall 002 03/25/2019 <210
O90328 - Outfall 002 03/28/2019 <210
090401-Outfall 002 04/01/2019 <210
090405-Outfall 002 04/05/2019 <210
SW2019-OUTFALL02-040819 04/08/2019 <210
O90409 - Outfall 002 04/09/2019 <210
O90412 - Outfall 002 04/12/2019 <210
O90416-OUTFALL 002 04/16/2019 <210
O90418-OUTFALL 002 04/18/2019 <210
O90423 - Outfall 002 04/23/2019 120
O90426 - Outfall 002 04/26/2019 70
O90430-Outfall 002 04/30/2019 <210
O90503-Outfall 002 05/03/2019 <210
O090507-Outfall 002 05/07/2019 <210
O90509-Outfall 002 05/09/2019 <210
O90514-Outfall 002 05/14/2019 <210
O90517- Outfall 002 05/17/2019 <210
DSTW-OUTFALL 002-052019 05/20/2019 <210
O90528 - Outfall 002 05/28/2019 5,500
FAY-DSTW-OUTFALL002-053019 05/30/2019 2,500
O90531 - Outfall 002 05/31/2019 2,100
O90611 - Outfall 002 06/11/2019 <210
O90614 - Outfall 002 06/14/2019 <210
Notes:
Bold - Analyte detected above associated reporting limit
ID - identifier
ng/L - nanograms per liter
PFMOAA - perfluoro-2-methoxyaceticacid
QA/QC - Quality assurance/ quality control
< - Analyte not detected above associated reporting limit.
Page 1 of 1 August 2019
TABLE 3
RIVER INTAKE HFPO-DA CONCENTRATIONS (JUNE 2017 - JULY 2019)
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Sample ID Sample Date Concentrations (ng/L)
DA0717-RW70706 07/06/2017 5,300
River Water Influent-071917 07/19/2017 330
24 River Water Influent-726 07/26/2017 17
GW0817-INTAKE 08/01/2017 11
24 River Water Influent-70802 08/02/2017 15
RW70808 08/08/2017 47
RW70815 08/15/2017 17
RW70823 08/23/2017 74
RW70829 08/29/2017 37
RW70905 09/05/2017 <10
RW70914 09/14/2017 78
RW70920 09/20/2017 14
RW70926 09/26/2017 14
RW71003 10/03/2017 <10
RW71011 10/11/2017 11
RW71016 10/16/2017 65
RW71103 11/03/2017 25
RW71110 11/10/2017 110
RW71115 11/15/2017 11
RW71122 11/22/2017 81
RW71201 12/01/2017 63
RW71208 12/08/2017 25
RW71213 12/13/2017 17
RW71218 12/18/2017 44
RW71228 12/28/2017 82
RW80105 01/05/2018 42
RW80108 01/08/2018 20
RW80117 01/17/2018 43
RW80124 01/24/2018 54
RW80202 02/02/2018 29
RW80207 02/07/2018 <10
RW80214 02/14/2018 21 J
R80221 02/21/2018 12
R80301 03/01/2018 41
R80307 03/07/2018 26
R80314 03/14/2018 <10
R80315 03/15/2018 <10
R80320 03/20/2018 16
R80328 03/28/2018 <10
R80403 04/03/2018 <10
R80411 04/11/2018 60 J
R80419 04/19/2018 160 J
R80426 04/26/2018 <10
R80503 05/03/2018 10
FAY-D-XRIV-H2O-050918 05/09/2018 12
R80509 05/09/2018 20
R80514 05/14/2018 20
R80524 05/24/2018 22
R80530 05/30/2018 15
R80607 06/07/2018 39
R80614 06/14/2018 36 J
River-Water-Intake-062018 06/20/2018 9.3000
R80621 06/21/2018 52
R80626 06/26/2018 20 J
R80706 07/06/2018 27
R80711 07/11/2018 <10
R80718 07/18/2018 39
R80725 07/25/2018 <10
R80802 08/02/2018 <10
R80808 08/08/2018 <10
R80815 08/15/2018 23
R80822 08/22/2018 33
R80830 08/30/2018 17
R80905 09/05/2018 13
R80912 09/12/2018 <10
R80920 09/20/2018 24
R80927 09/27/2018 13
R81004 10/04/2018 <10
R81010 10/10/2018 12
R81018 10/18/2018 <10
R81024 10/24/2018 <10
R81031 10/31/2018 11
R81107 11/07/2018 <10
R81114 11/14/2018 <10
PF1018-Excess River Water 11/19/2018 12 B
R81120 11/20/2018 30
R81127 11/27/2018 <10
Page 1 of 2 August 2019
TABLE 3
RIVER INTAKE HFPO-DA CONCENTRATIONS (JUNE 2017 - JULY 2019)
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Sample ID Sample Date Concentrations (ng/L)
R81205 12/05/2018 32
R81213 12/13/2018 16
R81219 12/19/2018 12
R81227 12/27/2018 18
R90102 01/02/2019 10
R90108 01/08/2019 <10
R90118 01/18/2019 82
R90125 01/25/2019 11
R90128 01/28/2019 15
R90207 02/07/2019 19
R90214 02/14/2019 12
R90218 02/18/2019 10
R90225 02/25/2019 11
R90306 03/06/2019 21
R90312 03/12/2019 10
R90320 03/20/2019 16
R90327 03/27/2019 20
R90404 04/04/2019 19
SW2019-EXCESSRIVER-040819 04/08/2019 23
SW2019-INTAKE-040819 04/08/2019 19
R90410 04/10/2019 <10
R90415 04/15/2019 <4.0
R90423 04/23/2019 <10
DSTW-LOC1-042419 04/24/2019 14
R90429 04/29/2019 28
R90508 05/08/2019 13
R90516 05/16/2019 10
R90529 05/29/2019 <10
R90606 06/06/2019 150
R90612 6/12/2019 <10
R90619 6/19/2019 <10
R90627 6/27/2019 <10
R90703 7/3/2019 22
R90710 7/10/2019 14
Notes:
Bold - Analyte detected above associated reporting limit
B - Analyte detected in associated blank.
HFPO-DA - hexafluoropropylene oxide dimer acid
ID - identifier
J - Analyte detected. Reported value may not be accurate or precise
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
UJ – Analyte not detected. Reporting limit may not be accurate or precise
< - Analyte not detected above associated reporting limit.
Page 2 of 2 August 2019
TABLE 4
RIVER INTAKE PFMOAA CONCENTRATIONS (JUNE 2017 - JULY 2019)
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Field Sample ID Sample Date Concentrations (ng/L)
FAY-D-XRIV-H2O-050918 05/09/2018 <100
River-Water-Intake-062018 06/20/2018 <95
PF1018-Excess River Water 11/19/2018 <200 UJ
R90207 02/07/2019 <210
R90214 02/14/2019 <210
R90218 02/18/2019 <210
R90225 02/25/2019 <210
R90306 03/06/2019 <210
R90312 03/12/2019 <210
R90320 03/20/2019 <210
R90327 03/27/2019 <210
R90404 04/04/2019 <210
SW2019-EXCESSRIVER-040819 04/08/2019 <210
SW2019-INTAKE-040819 04/08/2019 <210
R90410 04/10/2019 <210
R90415 04/15/2019 <210
R90423 04/23/2019 10
DSTW-LOC1-042419 04/24/2019 <210 UJ
R90429 04/29/2019 <210
R90508 05/08/2019 <210
R90516 05/16/2019 <210
DSTW-EXCESS RIVER WATER-052019 05/20/2019 <210
R90529 05/29/2019 <210
R90606 06/06/2019 14,000
R90612 6/12/2019 <210
Notes:
Bold - Analyte detected above associated reporting limit
ID - identifier
ng/L - nanograms per liter
PFMOAA - perfluoro-2-methoxyaceticacid
QA/QC - Quality assurance/ quality control
UJ – Analyte not detected. Reporting limit may not be accurate or precise
< - Analyte not detected above associated reporting limit.
Page 1 of 1 August 2019
TABLE 5
TOTAL DAILY PRECIPITATION (JUNE 2017 - JULY 2019)
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Date
Total
Precipitation (inches)Date
Total
Precipitation (inches)Date
Total
Precipitation (inches)
6/1/2017 --7/23/2017 0.13 9/13/2017 --
6/2/2017 --7/24/2017 --9/14/2017 --
6/3/2017 0.13 7/25/2017 --9/15/2017 --
6/4/2017 --7/26/2017 --9/16/2017 --
6/5/2017 1.66 7/27/2017 --9/17/2017 --
6/6/2017 --7/28/2017 --9/18/2017 --
6/7/2017 --7/29/2017 0.44 9/19/2017 --
6/8/2017 0.02 7/30/2017 --9/20/2017 0.28
6/9/2017 --7/31/2017 --9/21/2017 --
6/10/2017 --8/1/2017 --9/22/2017 --
6/11/2017 --8/2/2017 --9/23/2017 --
6/12/2017 --8/3/2017 --9/24/2017 --
6/13/2017 --8/4/2017 0.02 9/25/2017 --
6/14/2017 0.96 8/5/2017 --9/26/2017 --
6/15/2017 0.03 8/6/2017 --9/27/2017 --
6/16/2017 0.04 8/7/2017 0.12 9/28/2017 --
6/17/2017 0.03 8/8/2017 1.4 9/29/2017 --
6/18/2017 --8/9/2017 0.11 9/30/2017 --
6/19/2017 --8/10/2017 --10/1/2017 --
6/20/2017 0.74 8/11/2017 0.01 10/2/2017 --
6/21/2017 0.12 8/12/2017 0.47 10/3/2017 --
6/22/2017 0.4 8/13/2017 1.72 10/4/2017 --
6/23/2017 --8/14/2017 0.01 10/5/2017 --
6/24/2017 1.93 8/15/2017 0.05 10/6/2017 --
6/25/2017 0.01 8/16/2017 --10/7/2017 1.86
6/26/2017 --8/17/2017 0.24 10/8/2017 1.14
6/27/2017 --8/18/2017 --10/9/2017 0.08
6/28/2017 --8/19/2017 --10/10/2017 --
6/29/2017 --8/20/2017 --10/11/2017 --
6/30/2017 1.84 8/21/2017 --10/12/2017 --
7/1/2017 0.01 8/22/2017 --10/13/2017 --
7/2/2017 --8/23/2017 1.02 10/14/2017 --
7/3/2017 0.2 8/24/2017 --10/15/2017 --
7/4/2017 0.03 8/25/2017 --10/16/2017 0.09
7/5/2017 --8/26/2017 --10/17/2017 0.01
7/6/2017 --8/27/2017 --10/18/2017 --
7/7/2017 --8/28/2017 0.22 10/19/2017 --
7/8/2017 --8/29/2017 0.01 10/20/2017 --
7/9/2017 --8/30/2017 --10/21/2017 --
7/10/2017 0.82 8/31/2017 0.29 10/22/2017 --
7/11/2017 --9/1/2017 0.93 10/23/2017 0.15
7/12/2017 --9/2/2017 0.05 10/24/2017 0.01
7/13/2017 --9/3/2017 --10/25/2017 --
7/14/2017 --9/4/2017 --10/26/2017 --
7/15/2017 0.33 9/5/2017 0.05 10/27/2017 --
7/16/2017 0.12 9/6/2017 0.57 10/28/2017 0.73
7/17/2017 0.05 9/7/2017 --10/29/2017 0.03
7/18/2017 0.31 9/8/2017 --10/30/2017 --
7/19/2017 --9/9/2017 --10/31/2017 --
7/20/2017 --9/10/2017 --11/1/2017 --
7/21/2017 --9/11/2017 0.05 11/2/2017 --
7/22/2017 --9/12/2017 0.96 11/3/2017 --
Page 1 of 5 August 2019
TABLE 5
TOTAL DAILY PRECIPITATION (JUNE 2017 - JULY 2019)
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Date
Total
Precipitation (inches)Date
Total
Precipitation (inches)Date
Total
Precipitation (inches)
11/4/2017 --12/26/2017 --2/16/2018 --
11/5/2017 --12/27/2017 0.15 2/17/2018 --
11/6/2017 --12/28/2017 --2/18/2018 --
11/7/2017 --12/29/2017 --2/19/2018 0.04
11/8/2017 0.03 12/30/2017 --2/20/2018 0.01
11/9/2017 0.22 12/31/2017 --2/21/2018 --
11/10/2017 0.01 1/1/2018 --2/22/2018 --
11/11/2017 --1/2/2018 --2/23/2018 --
11/12/2017 --1/3/2018 --2/24/2018 --
11/13/2017 0.14 1/4/2018 0.01 2/25/2018 --
11/14/2017 --1/5/2018 --2/26/2018 0.22
11/15/2017 --1/6/2018 --2/27/2018 0.01
11/16/2017 --1/7/2018 --2/28/2018 0.07
11/17/2017 --1/8/2018 --3/1/2018 0.9
11/18/2017 --1/9/2018 --3/2/2018 --
11/19/2017 0.06 1/10/2018 --3/3/2018 --
11/20/2017 --1/11/2018 0.09 3/4/2018 --
11/21/2017 --1/12/2018 0.22 3/5/2018 --
11/22/2017 0.03 1/13/2018 --3/6/2018 0.26
11/23/2017 --1/14/2018 --3/7/2018 0.02
11/24/2017 --1/15/2018 --3/8/2018 --
11/25/2017 --1/16/2018 --3/9/2018 --
11/26/2017 --1/17/2018 0.2 3/10/2018 --
11/27/2017 --1/18/2018 0.07 3/11/2018 0.02
11/28/2017 --1/19/2018 0.01 3/12/2018 0.63
11/29/2017 --1/20/2018 --3/13/2018 0.01
11/30/2017 --1/21/2018 --3/14/2018 --
12/1/2017 --1/22/2018 --3/15/2018 --
12/2/2017 0.09 1/23/2018 0.08 3/16/2018 --
12/3/2017 0.01 1/24/2018 --3/17/2018 --
12/4/2017 --1/25/2018 --3/18/2018 --
12/5/2017 --1/26/2018 --3/19/2018 0.01
12/6/2017 0.24 1/27/2018 --3/20/2018 0.57
12/7/2017 0.07 1/28/2018 1.04 3/21/2018 0.1
12/8/2017 2.43 1/29/2018 1.04 3/22/2018 --
12/9/2017 0.3 1/30/2018 0.03 3/23/2018 --
12/10/2017 --1/31/2018 --3/24/2018 0.43
12/11/2017 --2/1/2018 --3/25/2018 0.21
12/12/2017 --2/2/2018 0.18 3/26/2018 --
12/13/2017 --2/3/2018 --3/27/2018 0.01
12/14/2017 --2/4/2018 1.12 3/28/2018 --
12/15/2017 --2/5/2018 --3/29/2018 --
12/16/2017 --2/6/2018 --3/30/2018 --
12/17/2017 --2/7/2018 0.08 3/31/2018 --
12/18/2017 --2/8/2018 0.03 4/1/2018 --
12/19/2017 --2/9/2018 --4/2/2018 --
12/20/2017 0.57 2/10/2018 0.21 4/3/2018 --
12/21/2017 --2/11/2018 --4/4/2018 --
12/22/2017 --2/12/2018 0.01 4/5/2018 --
12/23/2017 --2/13/2018 --4/6/2018 --
12/24/2017 0.03 2/14/2018 --4/7/2018 0.68
12/25/2017 0.01 2/15/2018 --4/8/2018 0.25
Page 2 of 5 August 2019
TABLE 5
TOTAL DAILY PRECIPITATION (JUNE 2017 - JULY 2019)
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Date
Total
Precipitation (inches)Date
Total
Precipitation (inches)Date
Total
Precipitation (inches)
4/9/2018 0.04 5/31/2018 --7/22/2018 0.01
4/10/2018 --6/1/2018 --7/23/2018 --
4/11/2018 --6/2/2018 --7/24/2018 0.02
4/12/2018 --6/3/2018 --7/25/2018 0.09
4/13/2018 --6/4/2018 --7/26/2018 --
4/14/2018 --6/5/2018 --7/27/2018 --
4/15/2018 1.06 6/6/2018 --7/28/2018 1.96
4/16/2018 --6/7/2018 --7/29/2018 0.06
4/17/2018 --6/8/2018 --7/30/2018 0.78
4/18/2018 --6/9/2018 0.02 7/31/2018 0.19
4/19/2018 --6/10/2018 --8/1/2018 0.43
4/20/2018 --6/11/2018 1.81 8/2/2018 0.66
4/21/2018 --6/12/2018 0.73 8/3/2018 0.46
4/22/2018 --6/13/2018 --8/4/2018 0.59
4/23/2018 0.23 6/14/2018 --8/5/2018 0.08
4/24/2018 1.18 6/15/2018 --8/6/2018 0.01
4/25/2018 --6/16/2018 --8/7/2018 --
4/26/2018 --6/17/2018 --8/8/2018 0.11
4/27/2018 0.13 6/18/2018 0.35 8/9/2018 --
4/28/2018 --6/19/2018 --8/10/2018 0.12
4/29/2018 --6/20/2018 --8/11/2018 0.01
4/30/2018 --6/21/2018 --8/12/2018 0.73
5/1/2018 --6/22/2018 --8/13/2018 0.43
5/2/2018 --6/23/2018 --8/14/2018 --
5/3/2018 --6/24/2018 0.07 8/15/2018 --
5/4/2018 --6/25/2018 0.45 8/16/2018 --
5/5/2018 --6/26/2018 0.76 8/17/2018 0.27
5/6/2018 0.04 6/27/2018 0.01 8/18/2018 0.16
5/7/2018 --6/28/2018 --8/19/2018 0.17
5/8/2018 --6/29/2018 --8/20/2018 0.55
5/9/2018 --6/30/2018 --8/21/2018 0.01
5/10/2018 0.08 7/1/2018 --8/22/2018 --
5/11/2018 --7/2/2018 --8/23/2018 --
5/12/2018 --7/3/2018 --8/24/2018 --
5/13/2018 --7/4/2018 --8/25/2018 --
5/14/2018 --7/5/2018 0.38 8/26/2018 --
5/15/2018 --7/6/2018 0.01 8/27/2018 --
5/16/2018 0.25 7/7/2018 0.16 8/28/2018 --
5/17/2018 0.8 7/8/2018 --8/29/2018 --
5/18/2018 0.01 7/9/2018 --8/30/2018 --
5/19/2018 0.23 7/10/2018 --8/31/2018 --
5/20/2018 --7/11/2018 --9/1/2018 --
5/21/2018 --7/12/2018 0.12 9/2/2018 --
5/22/2018 --7/13/2018 --9/3/2018 --
5/23/2018 0.07 7/14/2018 --9/4/2018 --
5/24/2018 1.86 7/15/2018 --9/5/2018 --
5/25/2018 --7/16/2018 --9/6/2018 --
5/26/2018 0.02 7/17/2018 0.07 9/7/2018 --
5/27/2018 --7/18/2018 --9/8/2018 --
5/28/2018 0.58 7/19/2018 --9/9/2018 --
5/29/2018 0.13 7/20/2018 0.01 9/10/2018 --
5/30/2018 --7/21/2018 0.01 9/11/2018 --
Page 3 of 5 August 2019
TABLE 5
TOTAL DAILY PRECIPITATION (JUNE 2017 - JULY 2019)
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Date
Total
Precipitation (inches)Date
Total
Precipitation (inches)Date
Total
Precipitation (inches)
9/12/2018 --11/3/2018 --12/25/2018 --
9/13/2018*0.68 11/4/2018 0.08 12/26/2018 --
9/14/2018*5.6 11/5/2018 0.18 12/27/2018 0.05
9/15/2018*7 11/6/2018 0.04 12/28/2018 0.6
9/16/2018*4.66 11/7/2018 0.05 12/29/2018 0.01
9/17/2018 --11/8/2018 0.3 12/30/2018 0.2
9/18/2018 --11/9/2018 0.04 12/31/2018 --
9/19/2018 --11/10/2018 0.01 1/1/2019 0.01
9/20/2018 --11/11/2018 --1/2/2019 --
9/21/2018 --11/12/2018 1.5 1/3/2019 0.22
9/22/2018 --11/13/2018 1.57 1/4/2019 0.76
9/23/2018 --11/14/2018 0.07 1/5/2019 --
9/24/2018 --11/15/2018 0.64 1/6/2019 --
9/25/2018 --11/16/2018 --1/7/2019 --
9/26/2018 0.35 11/17/2018 --1/8/2019 --
9/27/2018 0.13 11/18/2018 --1/9/2019 --
9/28/2018 0.28 11/19/2018 0.11 1/10/2019 --
9/29/2018 --11/20/2018 --1/11/2019 --
9/30/2018 --11/21/2018 --1/12/2019 --
10/1/2018 --11/22/2018 --1/13/2019 0.7
10/2/2018 --11/23/2018 --1/14/2019 --
10/3/2018 --11/24/2018 1.09 1/15/2019 --
10/4/2018 --11/25/2018 --1/16/2019 --
10/5/2018 --11/26/2018 --1/17/2019 0.17
10/6/2018 --11/27/2018 --1/18/2019 --
10/7/2018 --11/28/2018 --1/19/2019 --
10/8/2018 --11/29/2018 --1/20/2019 0.5
10/9/2018 --11/30/2018 --1/21/2019 --
10/10/2018 0.07 12/1/2018 1.11 1/22/2019 --
10/11/2018 0.67 12/2/2018 0.01 1/23/2019 --
10/12/2018 --12/3/2018 --1/24/2019 0.83
10/13/2018 --12/4/2018 --1/25/2019 --
10/14/2018 --12/5/2018 --1/26/2019 --
10/15/2018 --12/6/2018 --1/27/2019 --
10/16/2018 0.24 12/7/2018 --1/28/2019 --
10/17/2018 0.03 12/8/2018 0.39 1/29/2019 0.09
10/18/2018 --12/9/2018 1.56 1/30/2019 --
10/19/2018 --12/10/2018 0.35 1/31/2019 --
10/20/2018 --12/11/2018 0.02 2/1/2019 --
10/21/2018 --12/12/2018 --2/2/2019 --
10/22/2018 --12/13/2018 --2/3/2019 --
10/23/2018 --12/14/2018 1.49 2/4/2019 --
10/24/2018 --12/15/2018 0.43 2/5/2019 --
10/25/2018 --12/16/2018 0.01 2/6/2019 --
10/26/2018 1.05 12/17/2018 --2/7/2019 --
10/27/2018 0.02 12/18/2018 --2/8/2019 --
10/28/2018 --12/19/2018 --2/9/2019 --
10/29/2018 --12/20/2018 0.39 2/10/2019 --
10/30/2018 --12/21/2018 0.15 2/11/2019 0.25
10/31/2018 --12/22/2018 --2/12/2019 0.25
11/1/2018 0.11 12/23/2018 --2/13/2019 0.02
11/2/2018 0.04 12/24/2018 --2/14/2019 --
Page 4 of 5 August 2019
TABLE 5
TOTAL DAILY PRECIPITATION (JUNE 2017 - JULY 2019)
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Date
Total
Precipitation (inches)Date
Total
Precipitation (inches)Date
Total
Precipitation (inches)
2/15/2019 --4/8/2019 --5/30/2019 --
2/16/2019 0.6 4/9/2019 0.03 5/31/2019 0.1
2/17/2019 0.04 4/10/2019 --6/1/2019 --
2/18/2019 0.12 4/11/2019 --6/2/2019 --
2/19/2019 0.11 4/12/2019 1.1 6/3/2019 --
2/20/2019 0.19 4/13/2019 1.18 6/4/2019 --
2/21/2019 0.16 4/14/2019 0.23 6/5/2019 0.84
2/22/2019 0.28 4/15/2019 --6/6/2019 0.01
2/23/2019 0.46 4/16/2019 --6/7/2019 --
2/24/2019 0.01 4/17/2019 --6/8/2019 0.01
2/25/2019 --4/18/2019 --6/9/2019 2.19
2/26/2019 --4/19/2019 0.48 6/10/2019 0.79
2/27/2019 --4/20/2019 --6/11/2019 0.06
2/28/2019 --4/21/2019 --6/12/2019 0.39
3/1/2019 0.68 4/22/2019 --6/13/2019 0.02
3/2/2019 0.01 4/23/2019 --6/14/2019 --
3/3/2019 1.04 4/24/2019 --6/15/2019 --
3/4/2019 0.14 4/25/2019 --6/16/2019 --
3/5/2019 --4/26/2019 0.05 6/17/2019 --
3/6/2019 --4/27/2019 --6/18/2019 --
3/7/2019 --4/28/2019 --6/19/2019 --
3/8/2019 0.51 4/29/2019 --6/20/2019 0.08
3/9/2019 0.07 4/30/2019 --6/21/2019 --
3/10/2019 --5/1/2019 --6/22/2019 0.23
3/11/2019 --5/2/2019 --6/23/2019 --
3/12/2019 --5/3/2019 --6/24/2019 --
3/13/2019 --5/4/2019 0.16 6/25/2019 --
3/14/2019 --5/5/2019 0.39 6/26/2019 --
3/15/2019 0.7 5/6/2019 --6/27/2019 --
3/16/2019 --5/7/2019 --6/28/2019 --
3/17/2019 --5/8/2019 --6/29/2019 --
3/18/2019 --5/9/2019 --6/30/2019 --
3/19/2019 --5/10/2019 --7/1/2019 --
3/20/2019 0.19 5/11/2019 --7/2/2019 0.03
3/21/2019 0.15 5/12/2019 0.13 7/3/2019 --
3/22/2019 0.01 5/13/2019 --7/4/2019 1.72
3/23/2019 --5/14/2019 --7/5/2019 --
3/24/2019 --5/15/2019 --7/6/2019 --
3/25/2019 0.53 5/16/2019 --7/7/2019 --
3/26/2019 0.07 5/17/2019 --7/8/2019 0.43
3/27/2019 --5/18/2019 --7/9/2019 --
3/28/2019 --5/19/2019 --7/10/2019 0.01
3/29/2019 --5/20/2019 0.24 7/11/2019 --
3/30/2019 --5/21/2019 --7/12/2019 0.15
3/31/2019 --5/22/2019 --7/13/2019 --
4/1/2019 --5/23/2019 --7/14/2019 --
4/2/2019 1.02 5/24/2019 --
4/3/2019 --5/25/2019 --
4/4/2019 --5/26/2019 --
4/5/2019 1.03 5/27/2019 --
4/6/2019 --5/28/2019 --
4/7/2019 --5/29/2019 --
Notes:
-- - below USGS measurement threshold
USGS - United States Geological
Precipitation data obtained from USGS rain gauge at W.O. Huske Dam.
* - The USGS rain gauge did not collect data during Hurricane Florence. Precipitation data for September 13-16, 2018 was obtained
from the onsite rain gauge.
Page 5 of 5 August 2019
TABLE 6BIMONTHLY SAMPLE LOCATIONS - PARAGRAPH 11C Chemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC P.C.Intake/ OutfallProcess waterNon-process wastewater Stormwater April June1Discharge point of excess river water (i.e., water drawn from the Cape Fear River, but not used as process water or NCCW) to characterize background levels of PFASTemporal Composite Intake2 Kuraray northern leased area stormwater dischargeTemporal Composite----3 Chemours PPA area stormwater dischargeTemporal Composite----4 Combined stormwater discharge from Kuraray northern leased area and Chemours PPA areaTemporal Composite----5 Kuraray southern leased area stormwater Temporal Composite----6A Kuraray southern leased area NCCW discharge - Vacuum CondenserGrab6B Kuraray southern leased area NCCW discharge - Resins AreaGrab7A Combined stormwater and NCCW discharge from western portion of the FacilityTemporal Composite7BCombined stormwater and NCCW discharge from western portion of the Facility and treated discharge from WWTPGrab*8 Outfall 001 treated non-Chemours process wastewater discharge to open channel to Outfall 002 Temporal Composite9Chemours Monomers IXM NCCW and stormwater discharge including stormwater from Vinyl Ethers South and Vinyl Ethers NorthTemporal Composite10 Chemours Monomers IXM area stormwater dischargeTemporal Composite--11 Stormwater discharge from portion of grassy field to north of decommissioned Chemours Teflon area. Temporal Composite----12 DuPont area southern drainage ditch stormwater discharge and NCCWTemporal Composite----13 DuPont area northern drainage ditch stormwater discharge and NCCWTemporal Composite----14 DuPont area southeast stormwater and NCCW discharge Temporal Composite15 Combined stormwater and NCCW discharge from eastern portion of the FacilityTemporal Composite18 Kuraray process wastewater Grab19A DuPont process wastewater, Plant 1Grab19B DuPont process wastewater, Plant 2Grab20 Outfall 002 pipe to Cape Fear River upstream of sumpTemporal Composite Outfall21A Sediment Basin SouthGrab21B Sediment Basin NorthGrab----22 WWTP combined influentGrab23A Kuraray northern leased area combined process wastewater and NCCW; manhole on Terra Cotta Pipe Grab23B Kuraray laboratory process wastewaterGrab--24A Chemours Monomers IXM Vinyl Ethers South NCCWGrab24B Chemours Monomers IXM Line 3 and Line 4 Extruder NCCWGrab24C Chemours Monomers IXM Water Return Header NCCWGrabNotesSample numbers refer to locations identified in Figure 2.Temporal composite samples were integrated over 4 hours.Locations 2, 3, 4, 5, 11, 12, and 13 were not sampled in April or June because they were dry. Location 10 was not sampled in June because it was dry.Location 21B was not sampled in April or June because this sediment pond was not in use at the time of sampling.Location 23B was added to the Sampling Plan after April 2019. A sample was not collected in April.-- - sample not collected* - Location 7B was collected as a grab sample in April and June due to limited autosampler availability.IXM - ion exchange membraneNCCW - non-contact cooling waterPFAS - per- and polyfluoroalkyl substances PPA - polymer processing aid WWTP - Wastewater treatment plantSample CollectedSampling MethodSample Location DescriptionSample NumberSample CategoryAugust 2019
TABLE 7
ANALYTICAL RESULTS - APRIL 2019
PARAGRAPH 11C SAMPLING EVENT
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID 1 6A 6B 7A 7B
Field Sample ID DSTW-LOC1-042419 DSTW-LOC6A-042419 DSTW-LOC6B-042419 DSTW-LOC7A-042419 DSTW-LOC7B-042419
Date Sampled 04/24/2019 04/24/2019 04/24/2019 04/24/2019 04/24/2019
QA/QC----------
Table 3+ Lab SOP (ng/L)
PEPA <47 <47 <47 <47 <47
PFECA-G <41 <41 <41 <41 <41
PFMOAA <210 UJ <210 <210 <210 UJ <210
PFO2HxA <81 <81 <81 <81 <81
PFO3OA <58 <58 <58 <58 <58
PFO4DA <79 <79 <79 <79 <79
PMPA <570 <570 <570 <570 <570
Hydro-EVE Acid <28 <28 <28 <28 <28
EVE Acid <24 <24 <24 <24 <24
PFECA B <60 <60 <60 <60 <60
R-EVE <70 <70 <70 <70 <70
PFO5DA <34 <34 <34 <34 <34
Byproduct 4 <160 <160 <160 <160 <160
Byproduct 5 <58 <58 <58 <58 <58
Byproduct 6 <15 <15 <15 <15 <15
NVHOS <54 <54 <54 <54 <54
PES <46 <46 <46 <46 <46
PFESA-BP1 <27 <27 <27 <27 <27
PFESA-BP2 <30 <30 <30 <30 <30
EPA Method 537 Mod (ng/L)
HFPO-DA 14 13 41 14 21
Perfluorobutanoic Acid 7.1 7.6 7.1 7 5.2
Perfluorodecanoic Acid <2.0 <2.0 <2.0 <2.0 <2.0
Perfluorododecanoic Acid <2.0 <2.0 <2.0 <2.0 <2.0
Perfluoroheptanoic Acid 7 7.4 7.4 7.4 7
Perfluorononanoic Acid <2.0 <2.0 <2.0 <2.0 <2.0
Perfluorooctanoic acid 8.1 8.6 9.3 8.8 7.9
Perfluorohexanoic Acid 9.2 9.2 9.3 8.3 8.2
Perfluoropentanoic Acid 7 7.4 7.2 6.5 7.2
Perfluorotetradecanoic Acid <2.0 <2.0 <2.0 <2.0 <2.0
Perfluorotridecanoic Acid <2.0 <2.0 <2.0 <2.0 <2.0
Perfluoroundecanoic Acid <2.0 <2.0 <2.0 <2.0 <2.0
Perfluorobutane Sulfonic Acid 2.3 2.4 2.3 2.3 2.3
Perfluorodecane Sulfonic Acid <2.0 <2.0 <2.0 <2.0 <2.0
Perfluoroheptane sulfonic acid (PFHpS)<2.0 <2.0 <2.0 <2.0 <2.0
Perfluorohexane Sulfonic Acid 3.3 3.7 3.6 3.4 3.5
Perfluorononanesulfonic acid <2.0 <2.0 <2.0 <2.0 <2.0
Perfluorooctanesulfonic acid 12 14 14 14 14
Perfluoropentane sulfonic acid (PFPeS)<2.0 <2.0 <2.0 <2.0 <2.0
10:2 Fluorotelomer sulfonate <2.0 <2.0 <2.0 <2.0 <2.0
8:2 Fluorotelomersulfonic acid <20 <20 <20 <20 <20
6:2 Fluorotelomer sulfonate <20 <20 <20 <20 <20
4:2 Fluorotelomersulfonic acid <20 <20 <20 <20 <20
N-ethyl perfluorooctane sulfonamidoacetic acid <20 <20 <20 <20 <20
N-ethylperfluoro-1-octanesulfonamide <37 <37 UJ <37 UJ <37 <37 UJ
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol <60 <60 <60 <60 900 J
N-methyl perfluorooctane sulfonamidoacetic acid <20 <20 <20 <20 <20
N-methyl perfluoro-1-octanesulfonamide <35 <35 UJ <35 UJ <35 <35
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol <110 <110 <110 <110 <110
Perfluorododecane sulfonic acid (PFDoS)<2.0 <2.0 <2.0 <2.0 <2.0
Perfluorohexadecanoic acid (PFHxDA)<2.0 <2.0 <2.0 <2.0 <2.0
Perfluorooctadecanoic acid <2.0 <2.0 <2.0 2 <2.0
Perfluorooctane Sulfonamide <2.0 <2.0 <2.0 <2.0 <2.0
ADONA <2.1 <2.1 <2.1 <2.1 <2.1
NaDONA <2.1 <2.1 <2.1 <2.1 <2.1
F-53B Major <2.0 <2.0 <2.0 <2.0 <2.0
F-53B Minor <2.0 <2.0 <2.0 <2.0 <2.0
Notes:
Bold - Analyte detected above associated reporting limit
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
Page 1 of 6 August 2019
TABLE 7
ANALYTICAL RESULTS - APRIL 2019
PARAGRAPH 11C SAMPLING EVENT
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
8:2 Fluorotelomersulfonic acid
6:2 Fluorotelomer sulfonate
4:2 Fluorotelomersulfonic acid
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
NaDONA
F-53B Major
F-53B Minor
8 9 10 14 15
DSTW-LOC8-042419 DSTW-LOC9-042419 DSTW-LOC10-042419 DSTW-LOC14-042419 DSTW-LOC15-042419
04/24/2019 04/24/2019 04/24/2019 04/24/2019 04/24/2019
----------
<47 <47 47 <47 <47
<41 <41 <41 <41 <41
1,200 J <210 UJ <210 UJ <210 UJ <210 UJ
480 <81 94 <81 <81
150 <58 <58 <58 <58
<79 <79 <79 <79 <79
<570 <570 570 <570 <570
<28 <28 <28 <28 <28
<24 <24 <24 <24 <24
<60 <60 <60 <60 <60
<70 <70 70 <70 UJ <70
51 <34 <34 <34 34
<160 <160 <160 <160 UJ <160
690 <58 92 <58 UJ <58
<15 <15 <15 <15 <15
<54 <54 <54 <54 <54
<46 <46 <46 <46 <46
<27 <27 84 <27 <27
240 <30 <30 <30 <30
120 29 320 12 34
5.7 6.9 10 4.7 6.5
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
3.7 7.5 8.4 3.1 7.5
<2.0 <2.0 <2.0 <2.0 <2.0
8.2 8.9 10 5.8 8.5
4.9 9 9.3 4.4 7.9
4.2 8.6 17 3.8 8.2
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
2.4 2.2 2.1 <2.0 2.3
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
3.1 3.3 3.5 3 3.5
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 14 12 11 14
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<37 <37 <37 <37 <37
<60 <60 <60 <60 <60
<20 <20 <20 <20 <20
<35 <35 <35 <35 <35
<110 <110 <110 <110 <110
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1 <2.1
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
Notes:
Bold - Analyte detected above associated reporting limit
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
Page 2 of 6 August 2019
TABLE 7
ANALYTICAL RESULTS - APRIL 2019
PARAGRAPH 11C SAMPLING EVENT
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
8:2 Fluorotelomersulfonic acid
6:2 Fluorotelomer sulfonate
4:2 Fluorotelomersulfonic acid
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
NaDONA
F-53B Major
F-53B Minor
16 17A 17B 18 19A
DSTW-LOC16-042419 DSTW-LOC17A-042419 DSTW-LOC17B-042419 DSTW-LOC18-042419 DSTW-LOC19A-042419
04/24/2019 04/24/2019 04/24/2019 04/24/2019 04/24/2019
----------
<35,000 110,000 47,000 <47 <47
<31,000 <41,000 <41,000 <41 <41
160,000 <210,000 1,770,000 <210 <210
133,000 <81,000 <81,000 <81 <81
44,000 <58,000 <58,000 <58 <58
<59,000 <79,000 <79,000 <79 <79
539,000 <570,000 <570,000 <570 <570
95,000 <28,000 <28,000 <28 <28
787,000 <24,000 <24,000 <24 <24
<45,000 <60,000 <60,000 <60 <60
1,590,000 <70,000 <70,000 <70 <70
<25,000 <34,000 <34,000 <34 <34
2,410,000 <160,000 <160,000 <160 <160
330,000 <58,000 <58,000 <58 <58
54,000 <15,000 <15,000 <15 <15
259,000 <54,000 <54,000 <54 <54
<34,000 <46,000 <46,000 <46 <46
1,445,000 <27,000 <27,000 <27 <27
248,000 <30,000 <30,000 <30 <30
2,100,000 860,000,000 550,000,000 59 30 J
30,000 <4,400,000 <8,800 5.3 4.3 J
240 <3,900,000 28,000 <2.0 <2.0 UJ
<51 <6,900,000 <14,000 <2.0 <2.0 UJ
13,000 <3,100,000 <6,300 3 <2.0 UJ
7,500 <3,400,000 <6,800 <2.0 <2.0 UJ
440 <11,000,000 1,800,000 6.7 2.6 J
1,700 <7,300,000 <15,000 4.3 <2.0 UJ
53,000 <6,100,000 <12,000 3.7 2.6 J
<27 <3,600,000 <7,300 <2.0 <2.0 UJ
300 <16,000,000 <33,000 <2.0 <2.0 UJ
1,900 <14,000,000 <28,000 <2.0 <2.0 UJ
<18 <2,500,000 <5,000 <2.0 <2.0 UJ
<29 <4,000,000 <8,000 <2.0 <2.0 UJ
<18 <2,400,000 <4,800 <2.0 <2.0 UJ
<16 4,100,000 <4,300 2.1 <2.0 UJ
<15 <2,000,000 <4,000 <2.0 <2.0 UJ
<50 <6,800,000 <14,000 7.3 <2.0 UJ
<28 <3,800,000 <7,500 <2.0 <2.0 UJ
170 <2,400,000 <4,800 <2.0 <2.0
<480 <65,000,000 <130,000 <20 <20
<370 <25,000,000 <50,000 <20 <20 UJ
<370 <25,000,000 <50,000 <20 <20
<180 <24,000,000 <48,000 <20 <20
<28,000 <37,000 <37,000 <37 UJ <37 UJ
<45,000 <60,000 <60,000 <60 <60
<290 <39,000,000 <78,000 <20 <20
<26,000 <35,000 <35,000 <35 UJ <35 UJ
<82,000 <110,000 <110,000 <110 <110
<41 <5,600,000 <11,000 <2.0 <2.0 UJ
<82 <11,000,000 <22,000 <2.0 <2.0 UJ
<42 <5,800,000 <12,000 <2.0 <2.0 UJ
<32 <4,400,000 <8,800 <2.0 <2.0 UJ
<18 <2,400,000 <4,800 <2.1 <2.1 UJ
<18 <2,400,000 <4,800 <2.1 <2.1 UJ
900 <3,000,000 <6,000 <2.0 <2.0 UJ
<29 <4,000,000 <8,000 <2.0 <2.0 UJ
Notes:
Bold - Analyte detected above associated reporting limit
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
Page 3 of 6 August 2019
TABLE 7
ANALYTICAL RESULTS - APRIL 2019
PARAGRAPH 11C SAMPLING EVENT
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
8:2 Fluorotelomersulfonic acid
6:2 Fluorotelomer sulfonate
4:2 Fluorotelomersulfonic acid
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
NaDONA
F-53B Major
F-53B Minor
19B 20 20 21A 22
DSTW-LOC19B-042419 DSTW-LOC20-042419 DSTW-LOC20-042419-D DSTW-LOC21A-042419 DSTW-LOC22-042419
04/24/2019 04/24/2019 04/24/2019 04/24/2019 04/24/2019
----Blind Field Duplicate ----
<47 <47 <47 <47 <47
<41 <41 <41 <41 <41
<210 <210 UJ <210 UJ <210 <210
<81 <81 <81 <81 <81
<58 <58 <58 <58 <58
<79 <79 <79 <79 <79
<570 <570 <570 <570 <570
<28 <28 <28 <28 <28
<24 <24 <24 <24 <24
<60 <60 <60 <60 <60
<70 <70 <70 <70 UJ <70 UJ
<34 <34 <34 <34 <34
<160 <160 <160 <160 <160
<58 <58 <58 <58 UJ <58 UJ
<15 <15 <15 <15 <15
<54 <54 <54 <54 <54
<46 <46 <46 <46 <46
<27 <27 <27 <27 <27
<30 <30 <30 <30 <30
22 61 63 33 170
4.4 6.5 5.9 5 <3.5 UJ
<2.0 <2.0 <2.0 <2.0 <3.1
<2.0 <2.0 <2.0 <2.0 <5.5
2.2 7.1 7 3 7.1
<2.0 <2.0 <2.0 <2.0 <2.7
4.9 8.7 8.5 5.6 <8.5
3.4 7.8 7.7 4.4 <5.8
3.6 6.7 7.6 4.8 20
<2.0 <2.0 <2.0 <2.0 2.9
<2.0 <2.0 <2.0 <2.0 <13
<2.0 <2.0 <2.0 <2.0 <11
<2.0 2.2 2.2 2 <2.0
<2.0 <2.0 <2.0 <2.0 <3.2
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 3.5 3.5 3 4.5
<2.0 <2.0 <2.0 <2.0 <2.0
3.2 13 13 9.1 <5.4
<2.0 <2.0 <2.0 <2.0 <3.0
<2.0 <2.0 <2.0 <2.0 <2.0
<20 <20 <20 <20 <52
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<37 UJ <37 <37 <37 UJ <37 UJ
<60 <60 <60 <60 <60
<20 <20 <20 <20 <31
<35 UJ <35 <35 <35 UJ <35 UJ
<110 <110 <110 <110 <110
<2.0 <2.0 <2.0 <2.0 <4.5
<2.0 <2.0 <2.0 <2.0 <8.9
<2.0 <2.0 UJ <2.0 <2.0 <4.6
<2.0 <2.0 <2.0 <2.0 <3.5
<2.1 <2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1 <2.1
<2.0 <2.0 <2.0 <2.0 <2.4
<2.0 <2.0 <2.0 <2.0 <3.2
Notes:
Bold - Analyte detected above associated reporting limit
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
Page 4 of 6 August 2019
TABLE 7
ANALYTICAL RESULTS - APRIL 2019
PARAGRAPH 11C SAMPLING EVENT
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
8:2 Fluorotelomersulfonic acid
6:2 Fluorotelomer sulfonate
4:2 Fluorotelomersulfonic acid
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
NaDONA
F-53B Major
F-53B Minor
23A 24A 24A 24B 24C
DSTW-LOC23A-042419 DSTW-LOC24A-042419 D DSTW-LOC24B-042419 DSTW-LOC24C-042419
04/24/2019 04/24/2019 04/24/2019 04/24/2019 04/24/2019
----Blind Field Duplicate ----
<47 <47 <47 <47 <47
<41 <41 <41 <41 <41
1,300 <210 <210 <210 UJ <210 UJ
480 <81 <81 <81 <81
140 <58 <58 <58 <58
<79 <79 <79 <79 <79
700 <570 <570 <570 <570
32 <28 <28 <28 <28
65 <24 <24 <24 <24
<60 <60 <60 <60 <60
<70 <70 UJ <70 <70 <70
<34 <34 <34 <34 <34
180 <160 <160 <160 <160
2,200 <58 UJ <58 UJ <58 <58
<15 <15 <15 <15 <15
<54 <54 <54 <54 <54
<46 <46 <46 <46 <46
2,700 <27 <27 <27 35
140 <30 <30 <30 <30
270 16 J 14 14 19
160 6.3 5.8 5.5 4.7
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <16 <2.0 <2.0 <2.0
3.6 7 7.3 6 5.9
<2.0 2 <2.0 <2.0 <2.0
20 9.5 9.7 7.7 7.3
6.6 8.5 8.8 8 7
13 7 6.7 6.2 6.4
<2.0 <5.9 <2.0 <2.0 <2.0
<2.0 <14 <2.0 <2.0 <2.0
<2.0 <2 <2.0 <2.0 <2.0
<2.0 2.3 2.3 2.2 2
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
2 3.9 3.8 3.3 3.4
<2.0 <2.0 <2.0 <2.0 <2.0
2.925211215
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<37 <37 UJ <37 UJ <37 <37
<60 <60 <60 <60 <60
<20 <20 <20 <20 <20
<35 <35 UJ <35 UJ <35 <35
<110 <110 <110 <110 <110
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1 <2.1
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
Notes:
Bold - Analyte detected above associated reporting limit
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
Page 5 of 6 August 2019
TABLE 7
ANALYTICAL RESULTS - APRIL 2019
PARAGRAPH 11C SAMPLING EVENT
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
Perfluorooctanoic acid
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
Perfluorooctanesulfonic acid
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
8:2 Fluorotelomersulfonic acid
6:2 Fluorotelomer sulfonate
4:2 Fluorotelomersulfonic acid
N-ethyl perfluorooctane sulfonamidoacetic acid
N-ethylperfluoro-1-octanesulfonamide
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
N-methyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluoro-1-octanesulfonamide
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
NaDONA
F-53B Major
F-53B Minor
EQBLK EQBLK EQBLK FBLK TBLK
DSTW-EB-01-042419 DSTW-EB-02-042419 DSTW-EB-03-042419 DSTW-FB-042419 DSTW-TB-042519
04/24/2019 04/24/2019 04/24/2019 04/24/2019 04/25/2019
Equipment Blank - Dip Rod Equipment Blank - Peristaltic Pump
Equipment Blank -
Autosampler Field Blank Trip Blank
<47 <47 <47 <47 <47
<41 <41 <41 <41 <41
<210 <210 <210 <210 UJ <210
<81 <81 <81 <81 <81
<58 <58 <58 <58 <58
<79 <79 <79 <79 <79
<570 <570 <570 <570 <570
<28 <28 <28 <28 <28
<24 <24 <24 <24 <24
<60 <60 <60 <60 <60
<70 <70 <70 <70 <70
<34 <34 <34 <34 <34
<160 <160 <160 <160 <160
<58 <58 <58 <58 <58
<15 <15 <15 <15 <15
<54 <54 <54 <54 <54
<46 <46 <46 <46 <46
<27 <27 <27 <27 <27
<30 <30 <30 <30 <30
<4.0 <4.0 <4.0 <4.0 <4.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<37 UJ <37 UJ <37 <37 <37
820 J 850 J 780 J <60 <60
<20 <20 <20 <20 <20
<35 <35 <35 <35 <35
<110 <110 <110 <110 <110
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1 <2.1
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
Notes:
Bold - Analyte detected above associated reporting limit
EPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or precise
ng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedure
UJ – Analyte not detected. Reporting limit may not be accurate or precise.
-- - No data reported
< - Analyte not detected above associated reporting limit.
Page 6 of 6 August 2019
TABLE 8
ANALYTICAL RESULTS - JUNE 2019
PARAGRAPH 11 C SAMPLING EVENT
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID LOC1 LOC6A LOC6B LOC7A LOC7B
Field Sample ID STW-LOC1-062819 STW-LOC-6A-062719 STW-LOC-6B-062719 STW-LOC7A-062819 STW-LOC7B-062719
Date Sampled 06/28/2019 06/27/2019 06/27/2019 06/28/2019 06/27/2019
QA/QC ----------
Table 3+ Lab SOP (ng/L)
PEPA <20 <47 <47 <20 <20
PFECA-G <2.0 <41 <41 <2.0 <2.0
PFMOAA <5.0 <210 <210 <5.0 69
PFO2HxA 14 <81 <81 14 25
PFO3OA 2.5 <58 <58 2.2 10
PFO4DA <2.0 <79 <79 <2.0 9.7
PMPA 23 <570 <570 22 21
Hydro-EVE Acid ----------
EVE Acid ----------
PFECA B ----------
R-EVE ----------
PFO5DA <2.0 <34 UJ <34 UJ <2.0 24
Byproduct 4 ----------
Byproduct 5 ----------
Byproduct 6 ----------
NVHOS ----------
PES ----------
PFESA-BP1 <2.0 <27 <27 <2.0 <2.0
PFESA-BP2 <2.0 <30 <30 <2.0 120
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol <2.0 <60 <60 <2.0 <2.0
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol <2.0 <110 <110 <2.0 <2.0
N-ethylperfluoro-1-octanesulfonamide 2 <37 <37 <2.0 <2.0
N-methyl perfluoro-1-octanesulfonamide <2.0 <35 <35 <2.0 <2.0
EPA Method 537 Mod (ng/L)
HFPO-DA 18 66 24 22 18
Perfluorobutanoic Acid 8.3 11 9.2 8.8 8.9
Perfluorodecanoic Acid <2.0 <2.0 <2.0 <2.0 <2.0
Perfluorododecanoic Acid <2.0 <2.0 <2.0 <2.0 <2.0
Perfluoroheptanoic Acid 14 13 13 14 14
Perfluorononanoic Acid <2.0 <2.0 <2.0 <2.0 <2.0
PFOA 8.5 8.3 9.6 9.4 8.9
Perfluorohexanoic Acid 21 22 20 20 21
Perfluoropentanoic Acid 17 18 17 19 18
Perfluorotetradecanoic Acid <2.0 <2.0 <2.0 <2.0 <2.0
Perfluorotridecanoic Acid <2.0 <2.0 <2.0 <2.0 <2.0
Perfluoroundecanoic Acid <2.0 <2.0 <2.0 <2.0 <2.0
Perfluorobutane Sulfonic Acid 3.7 3.6 3.6 3.6 3.4
Perfluorodecane Sulfonic Acid <2.0 <2.0 <2.0 <2.0 <2.0
Perfluoroheptane sulfonic acid (PFHpS)<2.0 <2.0 <2.0 <2.0 <2.0
Perfluorohexane Sulfonic Acid 5 5.3 5.6 5.2 5.4
Perfluorononanesulfonic acid <2.0 <2.0 <2.0 <2.0 <2.0
PFOS 11 14 16 15 15
Perfluoropentane sulfonic acid (PFPeS)<2.0 <2.0 <2.0 <2.0 <2.0
10:2 Fluorotelomer sulfonate <2.0 <2.0 <2.0 <2.0 <2.0
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)<20 <20 <20 <20 <20
6:2 Fluorotelomer sulfonate <20 <20 <20 <20 <20
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)<20 <20 <20 <20 <20
N-ethyl perfluorooctane sulfonamidoacetic acid <20 <20 <20 <20 <20
N-methyl perfluorooctane sulfonamidoacetic acid <20 <20 <20 <20 <20
Perfluorododecane sulfonic acid (PFDoS)<2.0 <2.0 <2.0 <2.0 <2.0
Perfluorohexadecanoic acid (PFHxDA)<2.0 <2.0 <2.0 <2.0 <2.0
Perfluorooctadecanoic acid <2.0 <2.0 <2.0 <2.0 <2.0
Perfluorooctane Sulfonamide <2.0 <2.0 <2.0 <2.0 <2.0
ADONA <2.1 <2.1 <2.1 <2.1 <2.1
NaDONA <2.1 <2.1 <2.1 <2.1 <2.1
Notes:
Bold - Analyte detected above associated reporting limit
EPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality controlSOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
Page 1 of 5 August 2019
TABLE 8
ANALYTICAL RESULTS - JUNE 2019
PARAGRAPH 11 C SAMPLING EVENT
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
NaDONA
Notes:
Bold - Analyte detected above associated reporting limit
EPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality controlSOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
LOC7B LOC8 LOC9 LOC14 LOC15
STW-LOC7B-062719-D STW-LOC8-062819 STW-LOC9-062819 STW-LOC14-062819 STW-LOC15-062819
06/27/2019 06/28/2019 06/28/2019 06/28/2019 06/28/2019
Field Duplicate --------
<20 34 <20 <20 <20
<2.0 <4.1 <4.1 <2.0 <2.0
65 <21 <21 <5.0 12
25 360 20 15 16
10 200 <5.8 2.5 3.2
10 210 <7.9 <2.0 <2.0
19 <57 <57 22 25
----------
----------
----------
----------
26 520 <3.4 <2.0 <2.0
----------
----------
----------
----------
----------
<2.0 37 2,300 <2.0 880
130 2,600 120 <2.0 41
<2.0 <6.0 <6.0 <2.0 <2.0
<2.0 <11 <11 <2.0 <2.0
<2.0 <3.7 <3.7 <2.0 <2.0
<2.0 <3.5 <3.5 <2.0 <2.0
18 100 77 22 45
8.7 18 9.2 13 9.4
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
15 16 13 24 14
<2.0 4.8 2 2.3 <2.0
9.3 12 9.3 14 9.5
21 25 21 36 22
17 22 19 28 18
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
3.7 4.3 3.7 5.7 3.7
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
5.5 4.7 5.5 7.9 5.7
<2.0 <2.0 <2.0 <2.0 <2.0
16 2.9 15 22 15
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1 <2.1
Page 2 of 5 August 2019
TABLE 8
ANALYTICAL RESULTS - JUNE 2019
PARAGRAPH 11 C SAMPLING EVENT
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
NaDONA
Notes:
Bold - Analyte detected above associated reporting limit
EPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality controlSOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
LOC18 LOC19A LOC19B LOC20 LOC21A
STW-LOC-18-062719 STW-LOC-19A-062719 STW-LOC-19B-062719 STW-LOC20-062819 STW-LOC-21A-062719
06/27/2019 06/27/2019 06/27/2019 06/28/2019 06/27/2019
----------
<47 <47 <47 <20 <47
<41 <41 <41 <2.0 <41
<210 <210 <210 48 <210
<81 <81 <81 28 <81
<58 <58 <58 9.3 <58
<79 <79 <79 8.7 <79
<570 <570 <570 30 <570
----------
----------
----------
----------
<34 UJ <34 UJ <34 UJ 20 <34 UJ
----------
----------
----------
----------
----------
27 27 <27 260 <27
<30 <30 <30 110 <30
<60 <60 <60 <2.0 <60
<110 <110 <110 <2.0 <110
<37 <37 <37 <2.0 <37
<35 <35 <35 <2.0 <35
4.1 4.5 J 9.6 50 40
<3.3 2.4 J 3 8.8 9.8
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
2.4 3.3 J 4 15 14
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 3.1 J 3.1 9.3 9.8
3.5 6.1 J 6.8 23 23
3.6 5.3 6 17 21
<2.0 <2.0 UJ <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 3.8 4
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 5.8 6.2
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 2.2 15 14
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<20 <20 <20 <20 <20
<20 <20 UJ <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 UJ <2.0 UJ <2.0 UJ <2.0 <2.0
<2.0 UJ <2.0 UJ <2.0 UJ <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.1 <2.1 UJ <2.1 <2.1 <2.1
<2.1 <2.1 UJ <2.1 <2.1 <2.1
Page 3 of 5 August 2019
TABLE 8
ANALYTICAL RESULTS - JUNE 2019
PARAGRAPH 11 C SAMPLING EVENT
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
NaDONA
Notes:
Bold - Analyte detected above associated reporting limit
EPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality controlSOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
LOC22 LOC23A LOC23B LOC24A LOC24A
STW-LOC-22-062719 STW-LOC-23A-062719 STW-LOC-23B-062719 STW-LOC-24A-062719 STW-LOC-24A-062719-D
06/27/2019 06/27/2019 06/27/2019 06/27/2019 06/27/2019
--------Field Duplicate
310 560 9,200 <47 <47
<41 <41 <41 <41 <41
<210 320 <210 <210 <210
<81 240 200 <81 <81
<58 87 78 <58 <58
<79 <79 79 <79 <79
780 1,300 21,000 <570 <570
----------
----------
----------
----------
<34 UJ <34 UJ 98 J <34 UJ <34 UJ
----------
----------
----------
----------
----------
1,400 17,000 210 <27 <27
130 740 130 <30 <30
<60 <60 <60 <60 <60
<110 <110 <110 <110 <110
<37 <37 <37 <37 <37
<35 <35 <35 <35 <35
130 J 170 3,200 26 26
37 J 70 580 9.7 9.4
2.4 2.8 <2.0 <2.0 2.2
<2.0 6.9 <2.0 <2.0 <2.0
12 14 10 13 13
2.3 2.9 2.5 <2.0 2.7
9.8 30 29 8.8 J 11 J
21 J241221 21
22 29 68 17 17
<2.0 30 <2.0 UJ <2.0 <2.0
<2.0 16 <2.0 <2.0 <2.0
<2.0 4.3 <2.0 <2.0 <2.0
3.4 3.8 2.5 3.5 3.4
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
5.6 5.8 <2.0 5.3 6
<2.0 <2.0 <2.0 <2.0 <2.0
18 19 5.0 17 J 30 J
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <3.5 <2.0 <2.0
<20 <20 <37 <20 <20
<20 <20 20 J <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 42 <2.0 UJ <2.0 <2.0
<2.0 21 <2.0 UJ <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.1 UJ <2.1 <2.1 <2.1 <2.1
<2.1 UJ <2.1 <2.1 <2.1 <2.1
Page 4 of 5 August 2019
TABLE 8
ANALYTICAL RESULTS - JUNE 2019
PARAGRAPH 11 C SAMPLING EVENT
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
ADONA
NaDONA
Notes:
Bold - Analyte detected above associated reporting limit
EPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality controlSOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
LOC24B LOC24C TBLK EQBLK EQBLK FBLK
STW-LOC24B-062719 STW-LOC24C-062719 STW-TBLK-1 STW-EQBLK-1 STW-EQBLK-2 STW-LOC-FBLK-1
06/27/2019 06/27/2019 06/28/2019 06/28/2019 06/27/2019 06/27/2019
----Trip Blank Equipment Blank Equipment Blank Field Blank
<20 <20 <20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
<5.0 <5.0 <5.0 <5.0 <5.0 <5.0
8.1 8.6 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
17 14 <10 <10 <10 <10
------------
------------
------------
------------
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
------------
------------
------------
------------
------------
77 3.5 <2.0 <2.0 <2.0 <2.0
3.3 <2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
<2.0 2 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
10 16 <4.0 <4.0 <4.0 <4.0
9.6 8 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
13 13 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
8.3 7.9 <2.0 <2.0 <2.0 <2.0
19 21 <2.0 <2.0 <2.0 <2.0
17 17 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
3.5 3.8 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
55.1<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
14 15 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
<20 <20 <20 <20 <20 <20
<20 <20 <20 <20 <20 <20
<20 <20 <20 <20 <20 <20
<20 <20 <20 <20 <20 <20
<20 <20 <20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1 <2.1 <2.1
Page 5 of 5 August 2019
TABLE 10ANALYTICAL RESULTS - STORMWATER SAMPLING
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID LOC2 LOC2 LOC3 LOC3
Field Sample ID ASTW-LOC2-060519 ASTW-LOC2-060519-Z ASTW-LOC3-060519 ASTW-LOC3-060519-Z
Date Sampled 06/05/2019 06/05/2019 06/05/2019 06/05/2019
Total/ Dissolved Total Dissolved Total Dissolved
QA/QC --------
Table 3+ Lab SOP (ng/L)
PEPA 160 J 150 J <47 UJ 23 J
PFECA-G <41 UJ <2.0 UJ <41 UJ <2.0 UJ
PFMOAA <210 UJ 32 J <210 UJ 28 J
PFO2HxA 110 J 87 J <81 UJ 24 J
PFO3OA <58 UJ 16 J <58 UJ 7.0 J
PFO4DA <79 UJ 13 J <79 UJ 5.5 J
PMPA 650 J 430 J <570 UJ 79 J
Hydro-EVE Acid <28 UJ 2.4 J <28 UJ <2.0 UJ
EVE Acid <24 UJ <2.0 UJ <24 UJ <2.0 UJ
PFECA B <60 UJ <2.0 UJ <60 UJ <2.0 UJ
R-EVE <70 UJ 95 J <70 UJ 13 J
PFO5DA <34 UJ 8.6 J <34 UJ 3.7 J
Byproduct 4 <160 UJ 190 J <160 UJ 39 J
Byproduct 5 <58 UJ 170 J <58 UJ 9.1 J
Byproduct 6 <15 UJ <2.0 UJ <15 UJ <2.0 UJ
NVHOS <54 UJ 8.9 J <54 UJ 3.2 J
PES <46 UJ <2.0 UJ <46 UJ <2.0 UJ
PFESA-BP1 <27 UJ 23 J <27 UJ <2.0 UJ
PFESA-BP2 <30 UJ 17 J <30 UJ 4.0 J
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol <60 UJ <2.0 UJ <60 UJ <2.0 UJ
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol <110 UJ <2.0 UJ <110 UJ <2.0 UJ
N-ethylperfluoro-1-octanesulfonamide <37 UJ <2.0 UJ <37 UJ <2.0 UJ
N-methyl perfluoro-1-octanesulfonamide <35 UJ <2.0 UJ <35 UJ <2.0 UJ
EPA Method 537 Mod (ng/L)
HFPO-DA 940 1,100 1,800 1,400
Perfluorobutanoic Acid 12 11 2.1 3.3
Perfluorodecanoic Acid <2.0 <2.0 <2.0 <2.0
Perfluorododecanoic Acid <2.0 <2.0 <2.0 <2.0
Perfluoroheptanoic Acid 2.5 2.6 2.2 <2.0
Perfluorononanoic Acid <2.0 <2.0 <2.0 <2.0
PFOA 16 17 19 15
Perfluorohexanoic Acid 2.9 2.6 <2.0 <2.0
Perfluoropentanoic Acid 4.7 4.8 <2.0 2.4
Perfluorotetradecanoic Acid <2.0 <2.0 <2.0 <2.0
Perfluorotridecanoic Acid <2.0 <2.0 <2.0 <2.0
Perfluoroundecanoic Acid <2.0 <2.0 <2.0 <2.0
Perfluorobutane Sulfonic Acid <2.0 <2.0 <2.0 <2.0
Perfluorodecane Sulfonic Acid <2.0 <2.0 <2.0 <2.0
Perfluoroheptane sulfonic acid (PFHpS)<2.0 <2.0 <2.0 <2.0
Perfluorohexane Sulfonic Acid <2.0 <2.0 <2.0 <2.0
Perfluorononanesulfonic acid <2.0 <2.0 <2.0 <2.0
PFOS <2.0 <2.0 2.3 2.4
Perfluoropentane sulfonic acid (PFPeS)<2.0 <2.0 <2.0 <2.0
10:2 Fluorotelomer sulfonate <2.0 <2.0 <2.0 <2.0
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)<51 <50 <47 <51
6:2 Fluorotelomer sulfonate <20 <20 <20 <20
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)<20 <20 <20 <20
N-ethyl perfluorooctane sulfonamidoacetic acid <20 <20 <20 <20
N-methyl perfluorooctane sulfonamidoacetic acid <20 <20 <20 <20
Perfluorododecane sulfonic acid (PFDoS)<2.0 <2.0 <2.0 <2.0
Perfluorohexadecanoic acid (PFHxDA)<2.0 <2.0 <2.0 <2.0
Perfluorooctadecanoic acid <2.0 <2.0 <2.0 <2.0
Perfluorooctane Sulfonamide <2.0 <2.0 <2.0 <2.0
11Cl-PF3OUdS <2.0 <2.0 <2.0 <2.0
9Cl-PF3ONS <2.0 <2.0 <2.0 <2.0
ADONA <2.1 <2.1 <2.1 <2.1
NaDONA <2.1 <2.1 <2.1 <2.1
Total Suspended Solids (ng/L)18,000,000 J --9,200,000 J --
Notes:Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality control
SOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
Page 1 of 19 August 2019
TABLE 10ANALYTICAL RESULTS - STORMWATER SAMPLING
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
Total/ Dissolved
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
11Cl-PF3OUdS
9Cl-PF3ONS
ADONA
NaDONA
Total Suspended Solids (ng/L)
Notes:Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality control
SOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
LOC5 LOC5 LOC10 LOC10
ASTW-LOC5-060519 ASTW-LOC5-060519-Z ASTW-LOC10-060519 ASTW-LOC10-060519-Z
06/05/2019 06/05/2019 06/05/2019 06/05/2019
Total Dissolved Total Dissolved
--------
<47 UJ 58 J 1,500 J 1,300 J
<41 UJ <2.0 UJ <41 UJ <41 UJ
<210 UJ 7.4 J 2,200 J 2,500 J
<81 UJ 22 J 1,400 J 1,500 J
<58 UJ 2.7 J 660 J 500 J
<79 UJ 2.7 J 380 J 420 J
<570 UJ 190 J 3,700 J 2,900 J
<28 UJ <2.0 UJ 75 J 80 J
<24 UJ <2.0 UJ <24 UJ <24 UJ
<60 UJ <2.0 UJ <60 UJ <60 UJ
<70 UJ 11 J 340 J 330 J
<34 UJ 4.6 J 420 J 390 J
<160 UJ 100 J 940 J 980 J
<58 UJ 24 J 620 J 640 J
<15 UJ <2.0 UJ 26 J 29 J
<54 UJ 2.5 J 320 J 310 J
<46 UJ <2.0 UJ <46 UJ <46 UJ
<27 UJ 9.1 J 820 J 660 J
<30 UJ 4.2 J 630 J 550 J
<60 UJ <2.0 UJ <60 UJ <60 UJ
<110 UJ <2.0 UJ <110 UJ <110 UJ
<37 UJ <2.0 UJ <37 UJ <37 UJ
<35 UJ <2.0 UJ <35 UJ <35 UJ
160 140 3,500 5,100
4.4 5.9 99 95
<2.0 <2.0 4.3 3.5
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 24 23
<2.0 <2.0 8.9 8.2
3.9 3 26 25
2.6 2.5 23 21
<2.0 <2.0 100 110
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 3.6 3.2
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 2.3 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1
26,000,000 J --24,000,000 J --
Page 2 of 19 August 2019
TABLE 10ANALYTICAL RESULTS - STORMWATER SAMPLING
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
Total/ Dissolved
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
11Cl-PF3OUdS
9Cl-PF3ONS
ADONA
NaDONA
Total Suspended Solids (ng/L)
Notes:Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality control
SOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
LOC26 LOC26 LOC27 LOC27
ASTW-LOC26-060519 ASTW-LOC26-060519-Z ASTW-LOC27-060519 ASTW-LOC27-060519-Z
06/05/2019 06/05/2019 06/05/2019 06/05/2019
Total Dissolved Total Dissolved
--------
<47 UJ <20 UJ 47 J 30 J
<41 UJ <2.0 UJ <41 UJ <2.0 UJ
<210 UJ <5.0 UJ <210 UJ 40 J
<81 UJ 3.8 J <81 UJ 34 J
<58 UJ <2.0 UJ <58 UJ 7.9 J
<79 UJ <2.0 UJ <79 UJ 4.7 J
<570 UJ 30 J <570 UJ 120 J
<28 UJ <2.0 UJ <28 UJ <2.0 UJ
<24 UJ <2.0 UJ <24 UJ <2.0 UJ
<60 UJ <2.0 UJ <60 UJ <2.0 UJ
<70 UJ 3.1 J <70 UJ 20 J
<34 UJ <2.0 UJ <34 UJ 6.2 J
<160 UJ 8.9 J <160 UJ 110 J
<58 UJ 4.1 J <58 UJ 28 J
<15 UJ <2.0 UJ <15 UJ <2.0 UJ
<54 UJ <2.0 UJ <54 UJ 4.8 J
<46 UJ <2.0 UJ <46 UJ <2.0 UJ
<27 UJ 2.7 J <27 UJ 2.8 J
<30 UJ <2.0 UJ <30 UJ 5.8 J
<60 UJ <2.0 UJ <60 UJ <2.0 UJ
<110 UJ <2.0 UJ <110 UJ <2.0 UJ
<37 UJ <2.0 UJ <37 UJ <2.0 UJ
<35 UJ <2.0 UJ <35 UJ <2.0 UJ
46 B 41 170 200
<2.0 2.6 4.9 6.6
<2.0 <2.0 11 10
<2.0 <2.0 8 6.1
<2.0 <2.0 4.2 3.8
<2.0 <2.0 4.5 3.8
<2.0 <2.0 11 10
<2.0 <2.0 8.8 6.5
<2.0 <2.0 5.1 6.2
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 2 <2.0
<2.0 <2.0 6.7 4.8
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 6.7 6.1
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 84 69
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 9 J 9.2
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1
5,600,000 J --50,000,000 J --
Page 3 of 19 August 2019
TABLE 10ANALYTICAL RESULTS - STORMWATER SAMPLING
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
Total/ Dissolved
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
11Cl-PF3OUdS
9Cl-PF3ONS
ADONA
NaDONA
Total Suspended Solids (ng/L)
Notes:Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality control
SOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
LOC28 LOC28 LOC30 LOC30
ASTW-LOC28-060519 ASTW-LOC28-060519-Z ASTW-LOC30-060519 ASTW-LOC30-060519-Z
06/05/2019 06/05/2019 06/05/2019 06/05/2019
Total Dissolved Total Dissolved
--------
<47 UJ 32 J 210 J 210 J
<41 UJ <2.0 UJ <41 UJ <41 UJ
<210 UJ 11 J <210 UJ <210 UJ
<81 UJ 17 J 190 J 200 J
<58 UJ 2.3 J 100 J 110 J
<79 UJ 2.5 J 79 J 84 J
790 B 110 J 650 J 650 J
<28 UJ <2.0 UJ <28 UJ <28 UJ
<24 UJ <2.0 UJ <24 UJ <24 UJ
<60 UJ <2.0 UJ <60 UJ <60 UJ
<70 UJ 9.0 J <70 UJ <70 UJ
<34 UJ 4.5 J 100 J 100 J
<160 UJ 40 J <160 UJ 160 J
<58 UJ 15 J 100 J 130 J
<15 UJ <2.0 UJ <15 UJ <15 UJ
<54 UJ 3.0 J <54 UJ 59 J
<46 UJ <2.0 UJ <46 UJ <46 UJ
<27 UJ 3.5 J <27 UJ <27 UJ
<30 UJ 4.8 J 90 J 73 J
<60 UJ <2.0 UJ <60 UJ <60 UJ
<110 UJ <2.0 UJ <110 UJ <110 UJ
<37 UJ <2.0 UJ <37 UJ <37 UJ
<35 UJ <2.0 UJ <35 UJ <35 UJ
140 160 830 760
2.2 5.1 20 21
3.4 2.4 <2.0 <2.0
2 <2.0 <2.0 <2.0
<2.0 <2.0 4.3 4.4
<2.0 <2.0 <2.0 <2.0
6.1 5.5 6 5.6
<2.0 2.7 4.8 4.3
<2.0 2.3 13 15
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
2 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<20 <20 <46 <50
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1
36,000,000 J --28,000,000 J --
Page 4 of 19 August 2019
TABLE 10ANALYTICAL RESULTS - STORMWATER SAMPLING
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
Total/ Dissolved
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
11Cl-PF3OUdS
9Cl-PF3ONS
ADONA
NaDONA
Total Suspended Solids (ng/L)
Notes:Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality control
SOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
LOC31 LOC31 LOC31 LOC31
ASTW-LOC31-060519 ASTW-LOC31-060519-D ASTW-LOC31-060519-Z ASTW-LOC31-060519-Z-D
06/05/2019 06/05/2019 06/05/2019 06/05/2019
Total Total Dissolved Dissolved
--Field Duplicate --Field Duplicate
<47 UJ <47 UJ <47 UJ <47 UJ
<41 UJ <41 UJ <41 UJ <41 UJ
<210 UJ <210 UJ <210 UJ <210 UJ
<81 UJ <81 UJ <81 UJ <81 UJ
<58 UJ <58 UJ <58 UJ <58 UJ
<79 UJ <79 UJ <79 UJ <79 UJ
<570 UJ <570 UJ <570 UJ <570 UJ
<28 UJ <28 UJ <28 UJ <28 UJ
<24 UJ <24 UJ <24 UJ <24 UJ
<60 UJ <60 UJ <60 UJ <60 UJ
<70 UJ <70 UJ <70 UJ <70 UJ
<34 UJ <34 UJ <34 UJ <34 UJ
<160 UJ <160 UJ <160 UJ <160 UJ
<58 UJ <58 UJ <58 UJ <58 UJ
<15 UJ <15 UJ <15 UJ <15 UJ
<54 UJ <54 UJ <54 UJ <54 UJ
<46 UJ <46 UJ <46 UJ <46 UJ
<27 UJ <27 UJ <27 UJ <27 UJ
<30 UJ <30 UJ <30 UJ <30 UJ
<60 UJ <60 UJ <60 UJ <60 UJ
<110 UJ <110 UJ <110 UJ <110 UJ
37 J <37 UJ <37 UJ <37 UJ
<35 UJ <35 UJ <35 UJ <35 UJ
54 J 50 43 48
3.5 3.6 3.5 3.5
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 3.4 4.2
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 2.7 2.2
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<2.0 UJ <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 UJ <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1
6,800,000 J <5,000,000 R ----
Page 5 of 19 August 2019
TABLE 10ANALYTICAL RESULTS - STORMWATER SAMPLING
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
Total/ Dissolved
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
11Cl-PF3OUdS
9Cl-PF3ONS
ADONA
NaDONA
Total Suspended Solids (ng/L)
Notes:Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality control
SOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
LOC32 LOC32 LOC33 LOC33
ASTW-LOC32-060519 ASTW-LOC32-060519-Z ASTW-LOC33-060519 ASTW-LOC33-060519-Z
06/05/2019 06/05/2019 06/05/2019 06/05/2019
Total Dissolved Total Dissolved
--------
<47 UJ 130 J 590 J 540 J
<41 UJ <41 UJ <41 UJ <41 UJ
<210 UJ <210 UJ <210 UJ <210 UJ
<81 UJ <81 UJ 220 J 240 J
<58 UJ <58 UJ <58 UJ 81 J
<79 UJ <79 UJ 130 J 97 J
690 J <570 UJ 1,800 J 1,500 J
<28 UJ <28 UJ 28 J 39 J
<24 UJ <24 UJ <24 UJ <24 UJ
<60 UJ <60 UJ <60 UJ <60 UJ
<70 UJ <70 UJ <70 UJ 110 J
180 J 81 J 480 J 400 J
<160 UJ <160 UJ 160 J 190 J
<58 UJ 66 J 150 J 180 J
<15 UJ <15 UJ <15 UJ <15 UJ
<54 UJ <54 UJ 100 J 86 J
<46 UJ <46 UJ <46 UJ <46 UJ
27 J 27 J 140 J 130 J
190 J 170 J 320 J 290 J
<60 UJ <60 UJ <60 UJ <60 UJ
<110 UJ <110 UJ <110 UJ <110 UJ
<37 UJ <37 UJ <37 UJ <37 UJ
<35 UJ <35 UJ <35 UJ <35 UJ
320 300 880 890
12 12 46 47
2.2 2.3 5.7 5.1
<2.0 2.3 2.9 2.3
5.9 5.7 8.5 8.5
5.6 6.3 7.3 6.3
22 22 91 81
2.4 2.5 9.3 9.2
28 32 35 37
<2.0 <2.0 <2.0 <2.0
<2.0 2.3 2.7 2
5.9 8.5 5.4 6.1
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
4.3 5 10 12
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<20 <20 <20 <50
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1
300,000,000 J --210,000,000 J --
Page 6 of 19 August 2019
TABLE 10ANALYTICAL RESULTS - STORMWATER SAMPLING
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
Total/ Dissolved
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
11Cl-PF3OUdS
9Cl-PF3ONS
ADONA
NaDONA
Total Suspended Solids (ng/L)
Notes:Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality control
SOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
LOC34 LOC34 LOC35 LOC35
ASTW-LOC34-060519 ASTW-LOC34-060519-Z ASTW-LOC35-1-060519 ASTW-LOC35-1-060519-D
06/05/2019 06/05/2019 06/05/2019 06/05/2019
Total Dissolved Total Total
------Field Duplicate
<47 UJ 190 J 140 J <47 UJ
<41 UJ <41 UJ <41 UJ <41 UJ
210 J 350 J <210 UJ 12,000 J
180 J 160 J 180 J 2,400 J
<58 UJ 58 J 58 J 1,300 J
<79 UJ <79 UJ <79 UJ 1,000 J
910 J 640 J <570 UJ 570 J
<28 UJ <28 UJ <28 UJ 53 J
<24 UJ <24 UJ <24 UJ <24 UJ
<60 UJ <60 UJ <60 UJ <60 UJ
<70 UJ <70 UJ <70 UJ <70 UJ
800 J 460 J 95 J 700 J
<160 UJ <160 UJ <160 UJ <160 UJ
<58 UJ 78 J 380 J 620 J
<15 UJ <15 UJ <15 UJ 29 J
<54 UJ <54 UJ <54 UJ 380 J
<46 UJ <46 UJ <46 UJ <46 UJ
59 J 44 J 27 J 87 J
130 J 100 J 230 J 1,700 J
<60 UJ <60 UJ <60 UJ <60 UJ
<110 UJ <110 UJ <110 UJ <110 UJ
<37 UJ <37 UJ <37 UJ <37 UJ
<35 UJ <35 UJ <35 UJ <35 UJ
360 330 200 J 120 J
21 20 16 17
11 10 3.4 <2.0
14 15 <2.0 <2.0
3.9 3.6 <2 2.4
3.9 5 2.8 4.3
67 72 3.7 3.9
3.5 3.5 3.8 4.2
12 13 6.7 7.5
3.9 J 3.3 <2.0 <2.0
23 32 <2.0 <2.0
58 60 6.3 J 5.6
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
25 31 2.5 <2.0
<2.0 <2.0 <2.0 <2.0
4.6 5.9 2.4 <2.0
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 UJ <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1
810,000,000 J --23,000,000 J 22,000,000 J
Page 7 of 19 August 2019
TABLE 10ANALYTICAL RESULTS - STORMWATER SAMPLING
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
Total/ Dissolved
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
11Cl-PF3OUdS
9Cl-PF3ONS
ADONA
NaDONA
Total Suspended Solids (ng/L)
Notes:Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality control
SOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
LOC35 LOC35 LOC35 LOC35
ASTW-LOC35-1-060519-Z ASTW-LOC35-1-060519-Z-D ASTW-LOC35-2-060519 ASTW-LOC35-2-060519-Z
06/05/2019 06/05/2019 06/05/2019 06/05/2019
Dissolved Dissolved Total Dissolved
--Field Duplicate ----
150 J 81 J 97 J 100 J
<41 UJ <41 UJ <41 UJ <41 UJ
380 J 10,000 J 10,000 J 8,900 J
130 J 2,400 J 2,300 J 2,100 J
<58 UJ 1,100 J 1,000 J 910 J
<79 UJ 880 J 780 J 680 J
<570 UJ <570 UJ <570 UJ <570 UJ
<28 UJ 48 J 56 J 44 J
<24 UJ <24 UJ <24 UJ <24 UJ
<60 UJ <60 UJ <60 UJ <60 UJ
<70 UJ <70 UJ <70 UJ <70 UJ
100 J 560 J 580 J 420 J
<160 UJ <160 UJ <160 UJ 160 J
330 J 660 J 730 J 520 J
<15 UJ 28 J 29 J 26 J
<54 UJ 370 J 380 J 350 J
<46 UJ <46 UJ <46 UJ <46 UJ
38 J 110 J 99 J 83 J
220 J 1,500 J 1,600 J 1,400 J
<60 UJ <60 UJ <60 UJ <60 UJ
<110 UJ <110 UJ <110 UJ <110 UJ
<37 UJ <37 UJ <37 UJ <37 UJ
<35 UJ <35 UJ <35 UJ <35 UJ
150 J 100 J 130 110
15 16 19 17
3.5 <2.0 2.4 <2.0
2.3 <2.0 <2.0 <2.0
2.2 2.2 2.6 2.3
2.8 3.4 3.6 3.4
3.5 3.5 4.1 3.4
3.9 4 5.5 4.8
7.8 7.3 8.6 7.6
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
6.6 J 4.3 J 5.3 3.5
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 2.1 <2.0
<2.0 <2.0 <2.0 <2.0
3.5 <2.0 3.9 <2.0
<2.0 <2.0 <2.0 <2.0
2.8 <2.0 <2.0 <2.0
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 UJ <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1
----16,000,000 J --
Page 8 of 19 August 2019
TABLE 10ANALYTICAL RESULTS - STORMWATER SAMPLING
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
Total/ Dissolved
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
11Cl-PF3OUdS
9Cl-PF3ONS
ADONA
NaDONA
Total Suspended Solids (ng/L)
Notes:Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality control
SOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
LOC36 LOC36 LOC36 LOC36
ASTW-LOC36-060519 ASTW-LOC36-060519-D ASTW-LOC36-060519-Z ASTW-LOC36-060519-Z-D
06/05/2019 06/05/2019 06/05/2019 06/05/2019
Total Total Dissolved Dissolved
--Field Duplicate --Field Duplicate
140 J 130 J 130 J 150 J
<41 UJ <41 UJ <2.0 UJ <2.0 UJ
<210 UJ <210 UJ 38 J 96 J
170 J 180 J 72 J 230 J
<58 UJ <58 UJ 17 J 65 J
<79 UJ <79 UJ 16 J 40 J
660 J <570 UJ 290 J 380 J
<28 UJ <28 UJ 4.4 J 15 J
<24 UJ <24 UJ <2.0 UJ 3.5 J
<60 UJ <60 UJ <2.0 UJ <2.0 UJ
<70 UJ <70 UJ 20 J 65 J
79 J 88 J 39 J 110 J
<160 UJ <160 UJ 99 J 290 J
150 J 130 J 120 J 540 J
<15 UJ <15 UJ <2.0 UJ 2.2 J
<54 UJ <54 UJ 7.4 J 19 J
<46 UJ <46 UJ <2.0 UJ <2.0 UJ
<27 UJ <27 UJ 4.2 J 16 J
49 J 48 J 23 J 52 J
60 J <60 UJ <2.0 UJ <2.0 UJ
<110 UJ <110 UJ <2.0 UJ <2.0 UJ
<37 UJ <37 UJ <2.0 UJ <2.0 UJ
<35 UJ <35 UJ <2.0 UJ <2.0 UJ
310 J 300 280 J 390 J
13 J 14 11 J 20 J
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.9 2.1 <2.0 3.6
<2.0 <2.0 <2.0 2.1
<3.7 2.9 <2.6 4.3
<3.7 <2.0 <2.0 2.1
61 J 84 J 54 J 140 J
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2 2.3 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<5.2 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<11 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 UJ <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1
23,000,000 J 80,000,000 J ----
Page 9 of 19 August 2019
TABLE 10ANALYTICAL RESULTS - STORMWATER SAMPLING
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
Total/ Dissolved
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
11Cl-PF3OUdS
9Cl-PF3ONS
ADONA
NaDONA
Total Suspended Solids (ng/L)
Notes:Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality control
SOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
LOC37 LOC37 LOC38 LOC38
ASTW-LOC37-060519 ASTW-LOC37-060519-Z ASTW-LOC38-1-060519 ASTW-LOC38-1-060519-Z
06/05/2019 06/05/2019 06/05/2019 06/05/2019
Total Dissolved Total Dissolved
--------
340 J 340 J 730 J 530 J
<41 UJ <2.0 UJ <41 UJ <2.0 UJ
240 J 180 J 280 J 220 J
240 J 210 J 170 J 140 J
<58 UJ 31 J <58 UJ 34 J
<79 UJ 31 J <79 UJ 17 J
1,200 J 1,000 J 2,200 J 2,000 J
<28 UJ 5.3 J <28 UJ 11 J
<24 UJ <2.0 UJ <24 UJ 9.4 J
<60 UJ <2.0 UJ <60 UJ 11 J
<70 UJ 55 J 140 J 210 J
100 J 64 J 47 J 16 J
<160 UJ 340 J 250 J 770 J
<58 UJ 53 J 58 J 160 J
<15 UJ <2.0 UJ <15 UJ <2.0 UJ
<54 UJ 7.6 J <54 UJ 56 J
<46 UJ <2.0 UJ <46 UJ <2.3 UJ
<27 UJ 22 J 260 J 280 J
31 J 26 J 66 J 65 J
<60 UJ <2.0 UJ <60 UJ <3.0 UJ
<110 UJ <2.0 UJ <110 UJ <5.5 UJ
<37 UJ <2.0 UJ <37 UJ <2.0 UJ
<35 UJ <2.0 UJ <35 UJ <2.0 UJ
380 480 940 850
20 21 51 49
<2.0 <2.0 3.4 3.7
<2.0 <2.0 3.7 2.4
3.1 3 5 4.3
2.1 2.4 7.9 7.6
3.3 3.4 6.5 5.9
4.3 4.7 5.1 4.7
14 12 14 14
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 3.7 <2.0
2.2 2.3 8.9 7.7
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
3.3 2.7 5.3 5.9
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<20 <20 <51 <50
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1
63,000,000 J --22,000,000 J --
Page 10 of 19 August 2019
TABLE 10ANALYTICAL RESULTS - STORMWATER SAMPLING
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
Total/ Dissolved
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
11Cl-PF3OUdS
9Cl-PF3ONS
ADONA
NaDONA
Total Suspended Solids (ng/L)
Notes:Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality control
SOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
LOC38 LOC38 LOC39 LOC39
ASTW-LOC38-2-060519 ASTW-LOC38-2-060519-Z ASTW-LOC39-1-060519 ASTW-LOC39-1-060519-Z
06/05/2019 06/05/2019 06/05/2019 06/05/2019
Total Dissolved Total Dissolved
--------
520 J 370 J 500 J 430 J
<41 UJ <2.0 UJ <41 UJ <2.0 UJ
<210 UJ 84 J <210 UJ 48 J
160 J 100 J 100 J 74 J
<58 UJ 19 J <58 UJ 20 J
<79 UJ 12 J <79 UJ 16 J
1,500 J 1,000 J 1,500 J 1,000 J
<28 UJ 6.5 J <28 UJ 9.3 J
<24 UJ 9.8 J <24 UJ 3.7 J
<60 UJ <2.0 UJ <60 UJ <2.0 UJ
<70 UJ 26 J <70 UJ 110 J
53 J 20 J <34 UJ 17 J
<160 UJ 69 J <160 UJ 270 J
<58 UJ 50 J <58 UJ 110 J
<15 UJ <2.0 UJ <15 UJ <2.0 UJ
<54 UJ 9.3 J <54 UJ 13 J
<46 UJ <2.0 UJ <46 UJ <2.0 UJ
75 J 96 J 41 J 34 J
49 J 32 J 44 J 29 J
<60 UJ <2.0 UJ <60 UJ <2.0 UJ
<110 UJ <2.0 UJ <110 UJ <2.0 UJ
<37 UJ <2.0 UJ <37 UJ <2.0 UJ
<35 UJ <2.0 UJ <35 UJ <2.0 UJ
590 560 470 600
26 23 23 22
<2.0 <2.0 3.8 2.8
<2.0 <2.0 <2.0 <2.0
3.1 2.5 5.8 5.4
<2.0 <2.0 8.5 7.5
3.6 3.4 12 10
5.4 4.4 5.3 4.8
13 7.3 11 11
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 3.6 2.2
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 2.7 2.4
<2.0 <2.0 <2.0 <2.0
5.6 3.1 21 18
<2.0 <2.0 <2.8 <2.0
<2.0 <2.0 <2.0 <2.0
<20 <20 <20 <45
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1
20,000,000 J --160,000,000 J --
Page 11 of 19 August 2019
TABLE 10ANALYTICAL RESULTS - STORMWATER SAMPLING
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
Total/ Dissolved
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
11Cl-PF3OUdS
9Cl-PF3ONS
ADONA
NaDONA
Total Suspended Solids (ng/L)
Notes:Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality control
SOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
LOC39 LOC39 LOC40 LOC40
ASTW-LOC39-2-060519 ASTW-LOC39-2-060519-Z ASTW-LOC40-060519 ASTW-LOC40-060519-Z
06/05/2019 06/05/2019 06/05/2019 06/05/2019
Total Dissolved Total Dissolved
--------
720 J 590 J 130 J 110 J
<41 UJ <2.0 UJ <41 UJ <2.0 UJ
<210 UJ 66 J <210 UJ 32 J
130 J 100 J 81 J 51 J
<58 UJ 30 J <58 UJ 9.0 J
<79 UJ 16 J <79 UJ 8.6 J
1,800 J 1,400 J 730 J 350 J
<28 UJ 12 J <28 UJ <2.0 UJ
<24 UJ 5.2 J <24 UJ <2.0 UJ
<60 UJ <2.0 UJ <60 UJ <2.0 UJ
<70 UJ 110 J <70 UJ 11 J
42 J 19 J <34 UJ 11 J
<160 UJ 170 J <160 UJ 85 J
<58 UJ 120 J 120 J 270 J
<15 UJ <2.0 UJ <15 UJ <2.0 UJ
<54 UJ 17 J <54 UJ 6.3 J
<46 UJ <2.0 UJ <46 UJ <2.0 UJ
45 J 48 J <27 UJ 19 J
49 J 44 J <30 UJ 15 J
<60 UJ <2.0 UJ <60 UJ <2.0 UJ
<110 UJ <2.0 UJ <110 UJ <2.0 UJ
<37 UJ <2.0 UJ <37 UJ <2.0 UJ
<35 UJ <2.0 UJ <35 UJ <2.0 UJ
660 860 250 230
36 36 7.1 7.1
7.5 5.8 <2.0 <2.0
3.1 2.4 <2.0 <2.0
9.7 10 <2.0 <2.0
11 11 <2.0 <2.0
15 15 3.6 2.8
10 9.8 2.3 2.3
17 17 3.3 3.2
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
9.1 6.6 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
4.3 4.3 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
40 34 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1
20,000,000 J --<5,000,000 UJ --
Page 12 of 19 August 2019
TABLE 10ANALYTICAL RESULTS - STORMWATER SAMPLING
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
Total/ Dissolved
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
11Cl-PF3OUdS
9Cl-PF3ONS
ADONA
NaDONA
Total Suspended Solids (ng/L)
Notes:Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality control
SOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
LOC41 LOC41 LOC42 LOC42
ASTW-LOC41-060519 ASTW-LOC41-060519-Z ASTW-LOC42-1-060519 ASTW-LOC42-1-060519-Z
06/05/2019 06/05/2019 06/05/2019 06/05/2019
Total Dissolved Total Dissolved
--------
140 J 110 J 1,600 J 1,500 J
<41 UJ <2.0 UJ <41 UJ <41 UJ
<210 UJ 34 J 105,000 J 108,000 J
81 J 56 J 30,000 J 31,000 J
<58 UJ 11 J 12,000 J 13,000 J
<79 UJ 7.1 J 8,000 J 9,900 J
900 J 370 J 4,400 J 4,300 J
<28 UJ 2.2 J 1,500 J 1,500 J
<24 UJ <2.0 UJ 86 J 71 J
<60 UJ <2.0 UJ <60 UJ <60 UJ
<70 UJ 12 J 1,700 J 1,800 J
<34 UJ 12 J 4,900 J 5,100 J
<160 UJ 95 J 3,300 J 3,400 J
150 J 410 J 1,400 J 1,300 J
<15 UJ <2.0 UJ 390 J 410 J
<54 UJ 6.9 J 4,300 J 4,400 J
<46 UJ <2.0 UJ <46 UJ <46 UJ
<27 UJ 25 J 1,900 J 1,700 J
<30 UJ 18 J 7,200 J 6,900 J
<60 UJ <2.0 UJ <60 UJ <60 UJ
<110 UJ <2.0 UJ <110 UJ <110 UJ
<37 UJ <2.0 UJ <37 UJ <37 UJ
<35 UJ <2.0 UJ <35 UJ <35 UJ
290 250 46,000 54,000
7.6 7.9 390 390
<2.0 <2.0 12 12
<2.0 <2.0 6.7 6.1
<2.0 <2.0 420 450
<2.0 <2.0 160 160
4.2 4 33 32
2.6 3.1 100 100
3.4 3.1 1,400 1,400
<2.0 2.2 2 <2.0
<2.0 <2.0 11 7.7
<2.0 <2.0 55 44
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 2.8
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<20 <20 <20 <20
<20 <20 <200 <190
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0
<2.0 2.8 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1
6,800,000 J --21,000,000 J --
Page 13 of 19 August 2019
TABLE 10ANALYTICAL RESULTS - STORMWATER SAMPLING
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
Total/ Dissolved
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
11Cl-PF3OUdS
9Cl-PF3ONS
ADONA
NaDONA
Total Suspended Solids (ng/L)
Notes:Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality control
SOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
LOC42 LOC42 LOC43 LOC43
ASTW-LOC42-2-060519 ASTW-LOC42-2-060519-Z ASTW-LOC43-060519 ASTW-LOC43-060519-Z
06/05/2019 06/05/2019 06/05/2019 06/05/2019
Total Dissolved Total Dissolved
--------
750 J 680 J 580 J 640 J
<41 UJ <41 UJ <41 UJ <41 UJ
42,000 J 46,000 J 26,000 J 30,000 J
13,000 J 12,000 J 7,300 J 8,700 J
8,400 J 7,800 J 3,800 J 4,400 J
7,900 J 5,800 J 3,300 J 4,200 J
1,900 J 1,700 J 1,700 J 1,400 J
160 J 150 J 170 J 210 J
33 J 28 J 31 J 35 J
<60 UJ <60 UJ <60 UJ <60 UJ
430 J 430 J 270 J 320 J
4,200 J 3,300 J 2,500 J 2,800 J
710 J 630 J 890 J 940 J
970 J 890 J 1,600 J 1,700 J
40 J 43 J 28 J 38 J
400 J 470 J 420 J 500 J
<46 UJ <46 UJ <46 UJ <46 UJ
1,500 J 1,500 J 1,100 J 1,200 J
940 J 910 J 770 J 800 J
<60 UJ <60 UJ <60 UJ <60 UJ
<110 UJ <110 UJ <110 UJ <110 UJ
<37 UJ <37 UJ <37 UJ <37 UJ
<35 UJ <35 UJ <35 UJ <35 UJ
5,400 4,500 4,800 5,900
110 110 140 130
3 2.3 2.3 2.5
<2.0 <2.0 4.2 5.5
50 50 37 36
24 22 13 13
6.1 7.2 12 10
22 20 23 25
150 140 150 150
<2.0 <2.0 <2.0 3.3
<2.0 <2.0 3.7 7.2
8.6 7.1 5.3 5.2
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<20 <470 <530 <510
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1
10,000,000 J --14,000,000 J --
Page 14 of 19 August 2019
TABLE 10ANALYTICAL RESULTS - STORMWATER SAMPLING
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
Total/ Dissolved
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
11Cl-PF3OUdS
9Cl-PF3ONS
ADONA
NaDONA
Total Suspended Solids (ng/L)
Notes:Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality control
SOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
LOC52 LOC52 LOC53 LOC53
ASTW-LOC52-060519 ASTW-LOC52-060519-Z ASTW-LOC53-060519 ASTW-LOC53-060519-Z
06/05/2019 06/05/2019 06/05/2019 06/05/2019
Total Dissolved Total Dissolved
--------
4,100 J 4,700 J 180 J 120 J
<41 UJ 4.1 J <41 UJ <2.0 UJ
490 J 1,200 J 520 J 630 J
1,400 J 2,100 J 360 J 270 J
360 J 440 J 170 J 110 J
250 J 370 J 91 J 55 J
9,400 J 11,000 J 1,100 J 390 J
55 J 69 J <28 UJ 2.5 J
<24 UJ 16 J <24 UJ <2.0 UJ
<60 UJ <6.0 UJ <60 UJ <2.0 UJ
310 J 450 J <70 UJ 83 J
190 J 130 J <34 UJ 25 J
1,400 J 2,100 J <160 UJ 760 J
650 J 1,000 J <58 UJ 77 J
<15 UJ 14 J <15 UJ 4.4 J
220 J 330 J <54 UJ 26 J
<46 UJ <4.6 UJ <46 UJ <2.0 UJ
540 J 580 J 27 J 16 J
650 J 600 J 74 J 64 J
<60 UJ <6.0 UJ <60 UJ <2.0 UJ
<110 UJ <11 UJ <110 UJ <2.0 UJ
<37 UJ <3.7 UJ <37 UJ <2.0 UJ
<35 UJ <3.5 UJ <35 UJ <2.0 UJ
16,000 14,000 490 440
110 120 4.1 9.7
3.1 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
17 20 3 2.6
4.8 4.1 <2.0 <2.0
16 15 2.6 2.4
17 19 <2.0 <2.0
57 62 7.9 14
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 2 2.1 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<20 <20 <25 <45
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1
78,000,000 J --17,000,000 J --
Page 15 of 19 August 2019
TABLE 10ANALYTICAL RESULTS - STORMWATER SAMPLING
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
Total/ Dissolved
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
11Cl-PF3OUdS
9Cl-PF3ONS
ADONA
NaDONA
Total Suspended Solids (ng/L)
Notes:Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality control
SOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
LOC55 LOC55 TB TB TB
ASTW-LOC55-060519 ASTW-LOC55-060519-Z TB-1-060519 TB-10-060519 TB-11-060519
06/05/2019 06/05/2019 06/05/2019 06/05/2019 06/05/2019
Total Dissolved Total Total Total
----Trip Blank Trip Blank Trip Blank
110 J 85 J --<47 UJ <47 UJ
<41 UJ <2.0 UJ --<41 UJ <41 UJ
<210 UJ 28 J --<210 UJ <210 UJ
<81 UJ 32 J --<81 UJ <81 UJ
<58 UJ 5.8 J --<58 UJ <58 UJ
<79 UJ 16 J --<79 UJ <79 UJ
730 J 260 J --<570 UJ <570 UJ
<28 UJ 8.7 J --<28 UJ <28 UJ
<24 UJ <2.0 UJ --<24 UJ <24 UJ
<60 UJ <2.0 UJ --<60 UJ <60 UJ
<70 UJ 76 J --<70 UJ <70 UJ
170 J 92 J --<34 UJ <34 UJ
<160 UJ 210 J --<160 UJ <160 UJ
<58 UJ 37 J --<58 UJ <58 UJ
<15 UJ 2.6 J --<15 UJ <15 UJ
<54 UJ 6.8 J --<54 UJ <54 UJ
<46 UJ <2.0 UJ --<46 UJ <46 UJ
<27 UJ 13 J --<27 UJ <27 UJ
87 J 76 J --<30 UJ <30 UJ
<60 UJ <2.0 UJ --<60 UJ <60 UJ
<110 UJ <2.0 UJ --<110 UJ <110 UJ
<37 UJ <2.0 UJ --<37 UJ <37 UJ
<35 UJ <2.0 UJ --<35 UJ <35 UJ
160 140 <15 <4.0 <4.0
15 14 <3.5 <2.0 <2.0
4.7 3.1 <3.1 <2.0 <2.0
<2.0 <2.0 <5.5 <2.0 <2.0
2 <2.0 <2.5 <2.0 <2.0
5.6 4.6 <2.7 <2.0 <2.0
33 33 <8.5 <2.0 <2.0
2.1 <2.0 <5.8 <2.0 <2.0
3.5 4.5 <4.9 <2.0 <2.0
<2.0 <2.0 <2.9 <2.0 <2.0
<2.0 <2.0 <13 <2.0 <2.0
3.4 2.2 <11 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <3.2 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 3.6 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
6.9 5.5 <5.4 <2.0 <2.0
<2.0 <2.0 <3.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<20 <20 <52 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <31 <20 <20
<2.0 <2.0 <4.5 <2.0 <2.0
<2.0 <2.0 <8.9 <2.0 <2.0
<2.0 <2.0 <4.6 <2.0 <2.0
<2.0 <2.0 <3.5 <2.0 <2.0
<2.0 <2.0 <3.2 <2.0 <2.0
<2.0 <2.0 <2.4 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1 <2.1
290,000,000 J --<5,000,000 UJ ----
Page 16 of 19 August 2019
TABLE 10ANALYTICAL RESULTS - STORMWATER SAMPLING
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
Total/ Dissolved
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
11Cl-PF3OUdS
9Cl-PF3ONS
ADONA
NaDONA
Total Suspended Solids (ng/L)
Notes:Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality control
SOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
TB TB TB TB TB
TB-12-060519 TB-13-060519 TB-14-060519 TB-15-060519 TB-3-060519
06/05/2019 06/05/2019 06/05/2019 06/05/2019 06/05/2019
Total Total Total Total Total
Trip Blank Trip Blank Trip Blank Trip Blank Trip Blank
<47 UJ <47 UJ <47 UJ <47 UJ --
<41 UJ <41 UJ <41 UJ <41 UJ --
<210 UJ <210 UJ <210 UJ <210 UJ --
<81 UJ <81 UJ <81 UJ <81 UJ --
<58 UJ <58 UJ <58 UJ <58 UJ --
<79 UJ <79 UJ <79 UJ <79 UJ --
<570 UJ <570 UJ <570 UJ <570 UJ --
<28 UJ <28 UJ <28 UJ <28 UJ --
<24 UJ <24 UJ <24 UJ <24 UJ --
<60 UJ <60 UJ <60 UJ <60 UJ --
<70 UJ <70 UJ <70 UJ <70 UJ --
<34 UJ <34 UJ <34 UJ <34 UJ --
<160 UJ <160 UJ <160 UJ <160 UJ --
<58 UJ <58 UJ <58 UJ <58 UJ --
<15 UJ <15 UJ <15 UJ <15 UJ --
<54 UJ <54 UJ <54 UJ <54 UJ --
<46 UJ <46 UJ <46 UJ <46 UJ --
<27 UJ <27 UJ <27 UJ <27 UJ --
<30 UJ <30 UJ <30 UJ <30 UJ --
<60 UJ <60 UJ <60 UJ <60 UJ --
<110 UJ <110 UJ <110 UJ <110 UJ --
<37 UJ <37 UJ <37 UJ <37 UJ --
<35 UJ <35 UJ <35 UJ <35 UJ --
10 <4.0 <4.0 <4.0 10
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.1
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1 <2.1
--------<10,000,000 UJ
Page 17 of 19 August 2019
TABLE 10ANALYTICAL RESULTS - STORMWATER SAMPLING
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
Total/ Dissolved
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
11Cl-PF3OUdS
9Cl-PF3ONS
ADONA
NaDONA
Total Suspended Solids (ng/L)
Notes:Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality control
SOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
TB TB TB TB TB
TB-4-060519 TB-5-060519 TB-6-060519 TB-7-060519 TB-8-060519
06/05/2019 06/05/2019 06/05/2019 06/05/2019 06/05/2019
Total Total Total Total Total
Trip Blank Trip Blank Trip Blank Trip Blank Trip Blank
<47 UJ <47 UJ --<47 UJ <47 UJ
<41 UJ <41 UJ --<41 UJ <41 UJ
<210 UJ <210 UJ --<210 UJ <210 UJ
<81 UJ <81 UJ --<81 UJ <81 UJ
<58 UJ <58 UJ --<58 UJ <58 UJ
<79 UJ <79 UJ --<79 UJ <79 UJ
590 J <570 UJ --<570 UJ <570 UJ
<28 UJ <28 UJ --<28 UJ <28 UJ
<24 UJ <24 UJ --<24 UJ <24 UJ
<60 UJ <60 UJ --<60 UJ <60 UJ
<70 UJ <70 UJ --<70 UJ <70 UJ
<34 UJ <34 UJ --<34 UJ <34 UJ
<160 UJ <160 UJ --<160 UJ <160 UJ
<58 UJ <58 UJ --<58 UJ <58 UJ
<15 UJ <15 UJ --<15 UJ <15 UJ
<54 UJ <54 UJ --<54 UJ <54 UJ
<46 UJ <46 UJ --<46 UJ <46 UJ
<27 UJ <27 UJ --<27 UJ <27 UJ
<30 UJ <30 UJ --<30 UJ <30 UJ
<60 UJ <60 UJ --<60 UJ <60 UJ
<110 UJ <110 UJ --<110 UJ <110 UJ
<37 UJ <37 UJ --<37 UJ <37 UJ
<35 UJ <35 UJ --<35 UJ <35 UJ
25 <4.0 <4.0 <4.0 <4.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
3.9 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<20 <20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0 <2.0
3.7 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1 <2.1
----------
Page 18 of 19 August 2019
TABLE 10ANALYTICAL RESULTS - STORMWATER SAMPLING
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
Total/ Dissolved
QA/QC
Table 3+ Lab SOP (ng/L)
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic Acid
Perfluorodecanoic Acid
Perfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic Acid
PFOA
Perfluorohexanoic Acid
Perfluoropentanoic Acid
Perfluorotetradecanoic Acid
Perfluorotridecanoic Acid
Perfluoroundecanoic Acid
Perfluorobutane Sulfonic Acid
Perfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)
Perfluorohexane Sulfonic Acid
Perfluorononanesulfonic acid
PFOS
Perfluoropentane sulfonic acid (PFPeS)
10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)
6:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acid
Perfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acid
Perfluorooctane Sulfonamide
11Cl-PF3OUdS
9Cl-PF3ONS
ADONA
NaDONA
Total Suspended Solids (ng/L)
Notes:Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
ng/L - nanograms per literQA/QC - Quality assurance/ quality control
SOP - standard operating procedure
-- - No data reported
< - Analyte not detected above associated reporting limit.
J - Analyte detected. Reported value may not be accurate or precise
UJ – Analyte not detected. Reporting limit may not be accurate or
precise.
TB TBLK FBLK FBLK
TB-9-060519 TB-2-060519 ASTW-FB-060519 ASTW-FB-060519-Z
06/05/2019 06/05/2019 06/05/2019 06/05/2019
Total Total Total Dissolved
Trip Blank Trip Blank Field Blank Field Blank
<47 UJ --<47 UJ <20 UJ
<41 UJ --<41 UJ <2.0 UJ
<210 UJ --<210 UJ <5.0 UJ
<81 UJ --<81 UJ <2.0 UJ
<58 UJ --<58 UJ <2.0 UJ
<79 UJ --<79 UJ <2.0 UJ
<570 UJ --<570 UJ <10 UJ
<28 UJ --<28 UJ <2.0 UJ
<24 UJ --<24 UJ <2.0 UJ
<60 UJ --<60 UJ <2.0 UJ
<70 UJ --<70 UJ <2.0 UJ
<34 UJ --<34 UJ <2.0 UJ
<160 UJ --<160 UJ <2.0 UJ
<58 UJ --<58 UJ <2.0 UJ
<15 UJ --<15 UJ <2.0 UJ
<54 UJ --<54 UJ <2.0 UJ
<46 UJ --<46 UJ <2.0 UJ
<27 UJ --<27 UJ <2.0 UJ
<30 UJ --<30 UJ <2.0 UJ
<60 UJ --<60 UJ <2.0 UJ
<110 UJ --<110 UJ <2.0 UJ
<37 UJ --<37 UJ <2.0 UJ
<35 UJ --<35 UJ <2.0 UJ
<4.0 <4.0 <4.0 <4.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<20 <20 <20 <20
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.0 <2.0 <2.0 <2.0
<2.1 <2.1 <2.1 <2.1
<2.1 <2.1 <2.1 <2.1
----<5,000,000 R --
Page 19 of 19 August 2019
TABLE 11ANALYTICAL RESULTS - WASTEWATER TREATMENT PLANT Chemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC P.C.Location ID181822Field Sample ID WWTP_LOC1_071619.d WWTP_LOC8_071819.d WWTP_LOC18_071619.d WWTP_LOC22_071619.dDate Sampled 7/16/20197/18/20197/16/20197/16/2019QA/QC--------Table 3+ Lab SOP (ng/L)HFPO-DA<11.753.7<11.72,637PEPA<23.5 <23.5 <23.5684PFECA G<6.2<6.2<6.2<6.2PFMOAA<10.6<10.6<10.61,589PFO2HxA9.31485.32,213PFO3OA<9.269.7<9.22,602PFO4DA<8.266.4<8.212,459PMPA<4.8<4.8<4.8886Hydro-EVE Acid<28.7<21,194EVE Acid<5.2<5.2<5.22,902PFECA B<3.5<3.5<3.5<3.5R-EVE<10.7<10.7<10.715.8PFO5DA<7134<722,912Byproduct 4<7.3<7.3<7.360.2Byproduct 5<6.711.1<6.7268Byproduct 61.322.01.4439NVHOS<11.4141<11.48,598PES<1.2<1.2<1.24.6Byproduct 1<9.410.7<9.4591Byproduct 2<7.31,207<7.311,843PFPA156<16.3<16.32,213Notes:Bold - Analyte detected above associated reporting limitng/L - nanograms per literQA/QC - Quality assurance/ quality controlSOP - standard operating procedure< - Analyte not detected above associated reporting limit.Page 1 of 2August 2019
TABLE 11ANALYTICAL RESULTS - WASTEWATER TREATMENT PLANT Chemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC P.C.Location IDField Sample IDDate SampledQA/QCTable 3+ Lab SOP (ng/L)HFPO-DAPEPAPFECA GPFMOAAPFO2HxAPFO3OAPFO4DAPMPAHydro-EVE AcidEVE AcidPFECA BR-EVEPFO5DAByproduct 4Byproduct 5Byproduct 6NVHOSPESByproduct 1Byproduct 2PFPA2323A123A2EQBLKWWTP_LOC23_071619.d WWTP_LOC23A1_071619.d WWTP_LOC23A2_071619.d WWTP_LOCEB_071819.d7/16/2019 7/16/2019 7/16/2019 7/18/2019-- -- -- Equipment Blank65.9 9,394 12.7<11.7<23.5 <23.5 <23.5 <23.5<6.2 <6.2 <6.2 <6.2597<10.6 <10.6 <10.6214 22.0 10.9<4.859.6<9.2 <9.2 <9.223.7<8.2 <8.2 <8.2<4.86.0<4.8 <4.825.7 4.6<2 <274.4<5.2 <5.2 <5.2<3.5 <3.5 <3.5 <3.5<10.7 <10.7 <10.7 <10.711.7<7 <7 <727.1<7.3 <7.3 <7.31,419<6.7 <6.7 <6.72.5 1.3 1.3 1.341.9<11.4 <11.4 <11.4<1.2 <1.2 <1.2 <1.27,007<9.4 <9.4 <9.4315 14.6<7.3 <7.3118 79.8<16.3 <16.3Notes:Bold - Analyte detected above associated reporting limitng/L - nanograms per literQA/QC - Quality assurance/ quality controlSOP - standard operating procedure< - Analyte not detected above associated reporting limit.Page 2 of 2August 2019
TABLE 12ANALYTICAL RESULTS - COOLING WATER CHANNEL SEDIMENTS Chemours Fayetteville Works, North CarolinaGeosyntec Consultants of NC P.C.Location ID SD-CSD-FSD-GSD-GSD-GField Sample IDSD-DNSS-C-070319 SD-DNSS-F-070319 SD-DNSS-G-070319-1 SD-DNSS-G-070319-2 SD-DNSS-G-070219-DDate Sampled7/3/2019 7/3/2019 7/3/2019 7/3/2019 7/3/2019QA/QC-- -- -- -- Field DuplicateTable 3+ Lab SOP (ng/L)HFPO-DA26.5 317 1,130 1,194 1,383PEPA <23.5 <23.528.0 28.5 30.9PFECA G0.6 0.6 1.3 0.8 0.7PFMOAA <10.6 <10.6682 563 559PFO2HxA8.3 65.3 2,596 2,314 2,485PFO3OA2.9 26.7 1,871 1,744 1,962PFO4DA4.8 20.3 1,960 1,809 2,054PMPA <4.8 <4.828.0 29.4 32.8Hydro-EVE Acid4.6 7.6 152 164 205EVE Acid10.8 25.3 24.5 20.7 26.8PFECA B <3.5 <3.5 <3.5 <3.5 <3.5R-EVE0.4 0.3 4.0 2.1 2.4PFO5DA7.0 26.1 746 708 871Byproduct 45.6 11.1 27.9 26.4 28.5Byproduct 5105 176 137 137 145Byproduct 63.0 11.3 46.4 49.5 59.4NVHOS1.1 6.7 771 846 1,030PES0.5 0.5 0.7 0.5 0.7Byproduct 11,779 4,573 219 188 263Byproduct 2143 120 2,054 2,176 2,897Notes:Bold - Analyte detected above associated reporting limitng/L - nanograms per literQA/QC - Quality assurance/ quality controlSOP - standard operating procedure< - Analyte not detected above associated reporting limit.August 2019
TABLE 13
ANALYTICAL RESULTS - ADDITIONAL OUTFALL 002 SAMPLES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID 20B 20B 20C 20D
Field Sample ID FAY-SW-20B-053019 FAY-SW-DUP-053019 FAY-SW-20C-053019 FAY-SW-20D-053019
Date Sampled 05/30/2019 05/30/2019 05/30/2019 05/30/2019
QA/QC --Field Duplicate ----
Table 3+ Lab SOP (ng/L)
HFPO-DA <86 130 <86 89
PEPA <47 UJ <47 UJ <47 UJ <47 UJ
PFECA-G <41 UJ <41 UJ <41 UJ <41 UJ
PFMOAA 2,400 J 2,500 J 2,800 J 2,600 J
PFO2HxA 640 J 680 J 680 J 660 J
PFO3OA 300 J 320 J 340 J 320 J
PFO4DA 220 J 220 J 250 J 230 J
PMPA <570 UJ <570 UJ 570 J <570 UJ
Hydro-EVE Acid <28 UJ <28 UJ <28 UJ <28 UJ
EVE Acid <24 UJ <24 UJ <24 UJ <24 UJ
PFECA B <60 UJ <60 UJ <60 UJ <60 UJ
R-EVE <70 UJ 70 J <70 UJ <70 UJ
PFO5DA 140 J 140 J 160 J 150 J
Byproduct 4 210 J 280 J 220 J 240 J
Byproduct 5 1,300 J 1,500 J 1,700 J 1,300 J
Byproduct 6 <15 UJ <15 UJ <15 UJ <15 UJ
NVHOS 110 J 110 J 140 J 110 J
PES <46 UJ <46 UJ <46 UJ <46 UJ
PFESA-BP1 <27 UJ <27 UJ 36 J 32 J
PFESA-BP2 200 J 200 J 210 J 210 J
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol <60 UJ <60 UJ <60 UJ <60 UJ
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol <110 UJ <110 UJ <110 UJ <110 UJ
N-ethylperfluoro-1-octanesulfonamide <37 UJ <37 UJ <37 UJ <37 UJ
N-methyl perfluoro-1-octanesulfonamide <35 UJ <35 UJ <35 UJ <35 UJ
EPA Method 537 Mod (ng/L)
HFPO-DA --------
Perfluorobutanoic Acid --------Perfluorodecanoic Acid --------Perfluorododecanoic Acid --------
Perfluoroheptanoic Acid --------
Perfluorononanoic Acid --------PFOA --------
Perfluorohexanoic Acid --------
Perfluoropentanoic Acid --------Perfluorotetradecanoic Acid --------Perfluorotridecanoic Acid --------
Perfluoroundecanoic Acid --------Perfluorobutane Sulfonic Acid --------Perfluorodecane Sulfonic Acid --------
Perfluoroheptane sulfonic acid (PFHpS)--------Perfluorohexane Sulfonic Acid --------Perfluorononanesulfonic acid --------
PFOS --------Perfluoropentane sulfonic acid (PFPeS)--------10:2 Fluorotelomer sulfonate --------
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)--------6:2 Fluorotelomer sulfonate --------1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)--------
N-ethyl perfluorooctane sulfonamidoacetic acid --------
N-methyl perfluorooctane sulfonamidoacetic acid --------Perfluorododecane sulfonic acid (PFDoS)--------
Perfluorohexadecanoic acid (PFHxDA)--------
Perfluorooctadecanoic acid --------Perfluorooctane Sulfonamide --------
Notes:
Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or preciseng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedureUJ – Analyte not detected. Reporting limit may not be accurate or
precise
-- - No data reported< - Analyte not detected above associated reporting limit.
Page 1 of 2 August 2019
TABLE 13
ANALYTICAL RESULTS - ADDITIONAL OUTFALL 002 SAMPLES
Chemours Fayetteville Works, North Carolina
Geosyntec Consultants of NC P.C.
Location ID
Field Sample ID
Date Sampled
QA/QC
Table 3+ Lab SOP (ng/L)
HFPO-DA
PEPA
PFECA-G
PFMOAA
PFO2HxA
PFO3OA
PFO4DA
PMPA
Hydro-EVE Acid
EVE Acid
PFECA B
R-EVE
PFO5DA
Byproduct 4
Byproduct 5
Byproduct 6
NVHOS
PES
PFESA-BP1
PFESA-BP2
2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol
2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol
N-ethylperfluoro-1-octanesulfonamide
N-methyl perfluoro-1-octanesulfonamide
EPA Method 537 Mod (ng/L)
HFPO-DA
Perfluorobutanoic AcidPerfluorodecanoic AcidPerfluorododecanoic Acid
Perfluoroheptanoic Acid
Perfluorononanoic AcidPFOA
Perfluorohexanoic Acid
Perfluoropentanoic AcidPerfluorotetradecanoic AcidPerfluorotridecanoic Acid
Perfluoroundecanoic AcidPerfluorobutane Sulfonic AcidPerfluorodecane Sulfonic Acid
Perfluoroheptane sulfonic acid (PFHpS)Perfluorohexane Sulfonic AcidPerfluorononanesulfonic acid
PFOSPerfluoropentane sulfonic acid (PFPeS)10:2 Fluorotelomer sulfonate
1H,1H,2H,2H-perfluorohexanesulfonate (4:2 FTS)6:2 Fluorotelomer sulfonate1H,1H,2H,2H-perfluorodecanesulfonate (8:2 FTS)
N-ethyl perfluorooctane sulfonamidoacetic acid
N-methyl perfluorooctane sulfonamidoacetic acidPerfluorododecane sulfonic acid (PFDoS)
Perfluorohexadecanoic acid (PFHxDA)
Perfluorooctadecanoic acidPerfluorooctane Sulfonamide
Notes:
Bold - Analyte detected above associated reporting limitEPA - Environmental Protection Agency
J - Analyte detected. Reported value may not be accurate or preciseng/L - nanograms per liter
QA/QC - Quality assurance/ quality control
SOP - standard operating procedureUJ – Analyte not detected. Reporting limit may not be accurate or
precise
-- - No data reported< - Analyte not detected above associated reporting limit.
20E EQBLK FBLK
053019 EB3-053019 FB7-053019
05/30/2019 05/30/2019 05/30/2019
--Equipment Blank Field Blank
110 <86 --
<47 UJ <47 UJ <47 UJ
<41 UJ <41 UJ <41 UJ
2,500 J <210 UJ <210 UJ
640 J <81 UJ <81 UJ
320 J <58 UJ <58 UJ
220 J <79 UJ <79 UJ
640 J <570 UJ <570 UJ
<28 UJ <28 UJ <28 UJ
<24 UJ <24 UJ <24 UJ
<60 UJ <60 UJ <60 UJ
<70 UJ <70 UJ <70 UJ
140 J <34 UJ 37 J
230 J <160 UJ <160 UJ
1,300 J <58 UJ <58 UJ
<15 UJ <15 UJ <15 UJ
100 J <54 UJ <54 UJ
<46 UJ <46 UJ <46 UJ
30 J <27 UJ <27 UJ
190 J <30 UJ <30 UJ
<60 UJ <60 UJ <60 UJ
<110 UJ <110 UJ <110 UJ
<37 UJ <37 UJ <37 UJ
<35 UJ <35 UJ <35 UJ
----<4.0
----<2.0----<2.0----<2.0
----<2.0
----<2.0----<2.0
----<2.0
----<2.0----<2.0
----<2.0
----<2.0----<2.0----<2.0
----<2.0----<2.0----<2.0
----<2.0----<2.0----<2.0
----<20----<20----<20
----<20----<20----<2.0
----<2.0
----<2.0----<2.0
Page 2 of 2 August 2019
FIGURES
")
")
")
")
")Cape Fear RiverKuraray America
Leased Areas
Chemours
PPA Area
Chemours Monomers IXM Area
WastewaterTreatment
Plant
DuPont
Leased Area
Former DuPont
PMDF ProductionArea
Outfall 002
Sampling Point
Site DrainageNetwork
Outfall 002
W.O. Huske Dam
Old Outfall Channel Mouth
Site River Water Intake
Willis Creek Mouth
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS,AeroGRID, IGN, and the GIS User Community
Facility Production Areas and Site Conveyance Network
Chemours Fayetteville Works, North Carolina
Figure
1Raleigh
500 0 500250 Feet
³
August 2019
Legend
")Site Features
Cape Fear River
Nearby Tributaries
Observed Seep (Natural Drainage)
Drainage Network
Site Boundary
Notes:Basemap Sources: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the GIS User Community
Areas at Site
Chemours Monomers Ion Exchange Membrance(IXM) Area
Chemours Polymer Processing Aid (PPA) Area
DuPont Leased Area
Former DuPont PMDF Production Area
Kuraray America Leased Areas
Wastewater Treatment Plant
1
2
3
4
5
1 Chemours Process Water Users
2 Chemours Non-Process Water Users
3 Tenant Water Users
4 Non-Contact Cooling Water Users
5 Wastewater Treatment Plant
Outfall 001
Outfall 002
Drainag
e
N
et
w
or
k
Intake
Process WastewaterDisposed Off-Site
Cape Fe
a
r
Ri
v
er
Stormw
at
er
Runoff
Outfall 002 SamplingPoint

Raleigh, NC August 2019
Figure
2
Conceptual Schematic of Site Water Balance
Chemours Fayetteville Works, North Carolina
Note: Figure not to scale
Waste Water Treatment Plant Discharge
Du Po nt A r eaWoodLinedTrench
O p en Ch a n ne l t o O ut fa ll 0 02
C o o l i ng Wat er Ch an ne l
Site Conveyance Network
Chemours Fayetteville Works, North Carolina
Figure
3Raleigh
500 0 500250 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Legend
Wood Lined Trench
Wastewater Treatment Plant Discharge
Cooling Water Channel
Open Channel to Outfall 002
DuPont Area Ditches
Notes: Precipitation Data and Outfall 002 HFPO-DA Concentrations(June 2017 - July 2019)Chemours Fayetteville Works, North CarolinaFigure4RaleighAugust 2019- Outfall 002 samples are a combination of 1-day and 3-day composite and grab samples.- Precipitation data plotted is the 24-hour rainfall amount for each day.- Precipitation data obtained from USGS rain gauge at W.O. Huske Dam. Precipitation datafor September 13-16, 2018 obtained from onsite rain gauge, since USGS rain gauge did notcollect data during Hurricane Florence.Acronyms: - HFPO-DA - Hexafluoropropylene oxide dimer acid-ng / L: nanograms per liter-USGS: United States Geological Survey010,00020,00030,00040,00050,00060,00070,00080,00090,00000.511.522.53HFPO‐DA Concentration (ng/L)Daily Precipitation (inches)HFPO‐DAPrecipitationOutfall 002 DetectsOutfall 002 Non‐DetectsRiver Intake DetectsRiver Intake Non‐Detects
Notes: Precipitation Data and Outfall 002 HFPO-DA Concentrations(August 2017 - July 2019)Chemours Fayetteville Works, North CarolinaFigure5RaleighAugust 2019- Outfall 002 samples are a combination of 1-day and 3-day composite and grab samples.- Precipitation data plotted is the 24-hour rainfall amount for each day.- Precipitation data obtained from USGS rain gauge at W.O. Huske Dam. Precipitation datafor September 13-16, 2018 obtained from onsite rain gauge, since USGS rain gauge did notcollect data during Hurricane Florence.Acronyms: - HFPO-DA - Hexafluoropropylene oxide dimer acid- ng / L: nanograms per liter- USGS: United States Geological Survey05001,0001,5002,0002,5003,0003,5004,00000.511.522.53HFPO‐DA Concentration (ng/L)Daily Precipitation (inches)HFPO‐DAPrecipitationOutfall 002 DetectsOutfall 002 Non‐DetectsRiver Intake DetectsRiver Intake Non‐Detects
Notes: Precipitation Data and Outfall 002 PFMOAA Concentrations(May 2018 - July 2019)Chemours Fayetteville Works, North CarolinaFigure6RaleighAugust 2019- Outfall 002 samples are a combination of 1-day and 3-day composite and grab samples.-Precipitation data plotted is the 24-hour rainfall amount for each day.-Precipitation data obtained from USGS rain gauge at W.O. Huske Dam. Precipitation datafor September 13-16, 2018 obtained from onsite rain gauge, since USGS rain gauge did notcollect data during Hurricane Florence.-Intake and Outfall 002 PFMOAA concentrations in late May and early June 2019 aredescribed in the Observations of Elevated PFAS Concentrations at the Cape Fear RiverIntake and Outfall 002 Sample Locations in May and June 2019 Memorandum (Geosyntec,2019B)Acronyms:-ng / L: nanograms per liter-PFMOAA - Perfluoro-2-methoxyaceticacid-USGS: United States Geological Survey02,0004,0006,0008,00010,00012,00014,00016,00000.511.522.53PFMOAA Concentration (ng/L)Daily Precipitation (inches)PFMOAAPrecipitationOutfall 002 DetectsOutfall 002 Non‐DetectsRiver Intake DetectsRiver Intake Non‐Detects
Notes: Calendar Year 2018 HFPO-DA Concentrations at Outfall 002 Chemours Fayetteville Works, North CarolinaFigure7RaleighAugust 2019- Outfall 002 samples are a combination of 1-day and 3-day composite and grab samples.-Precipitation data plotted is the 24-hour rainfall amount for each day.-Precipitation data obtained from USGS rain gauge at W.O. Huske Dam. Precipitation datafor September 13-16, 2018 obtained from onsite rain gauge, since USGS rain gauge did notcollect data during Hurricane Florence.Acronyms:-HFPO-DA - Hexafluoropropylene oxide dimer acid-ng / L: nanograms per liter-USGS: United States Geological Survey05001,0001,5002,0002,5003,00000.511.522.53HFPO‐DA Concentration (ng/L)Daily Precipitation (inches)HFPO‐DAPrecipitationOutfall 002 DetectsOutfall 002 Non‐DetectsRiver Intake DetectsRiver Intake Non‐Detects
Notes: Calendar Year 2018 PFMOAA Concentrations at Outfall 002 Chemours Fayetteville Works, North CarolinaFigure8RaleighAugust 2019- Outfall 002 samples are a combination of 1-day and 3-day composite and grab samples.-Precipitation data plotted is the 24-hour rainfall amount for each day.-Precipitation data obtained from USGS rain gauge at W.O. Huske Dam. Precipitation datafor September 13-16, 2018 obtained from onsite rain gauge, since USGS rain gauge did notcollect data during Hurricane Florence.Acronyms:-ng / L: nanograms per liter-PFMOAA - Perfluoro-2-methoxyaceticacid-USGS: United States Geological Survey05001,0001,5002,0002,5003,00000.511.522.53PFMOAA Concentration (ng/L)Daily Precipitation (inches)PFMOAAPrecipitationOutfall 002 DetectsOutfall 002 Non‐DetectsRiver Intake DetectsRiver Intake Non‐Detects
Acronyms: Calendar Year 2018 Outfall 002 Flow and Precipitation
Chemours Fayetteville Works, North Carolina
Figure
9RaleighAugust 2019
- MGD - millions of gallons per day
- in - inches
- NCCW - non-contact cooling water
- WWTP - wastewater treatment plant
0
2
4
6
8
10
12
14
16
18
20
0
5
10
15
20
25
30
35
40
45
50
Precipitation (day of and two preceding days) (inches)Outfall 002 Flow (MGD)NCCW in Site Conveyance Network Flow (MGD)
WWTP Effluent (OF 001) Flow (MGD)
OF 002 Approximate Stormwater Flow (MGD)
Precipitation (day of + 2 preceding days) (in)
Acronyms: Calendar Year 2018 HFPO-DA Loading at Outfall 002
Chemours Fayetteville Works, North Carolina- HFPO-DA - Hexafluoropropylene oxide dimer acid
- lbs - pounds
Figure
10RaleighAugust 2019
5.7 lbs, 45%
1.4 lbs, 11%
5.6 lbs, 44%
Dry Stormwater
River
Intake
Acronyms: Calendar Year 2018 PFMOAA Loading at Outfall 002
Chemours Fayetteville Works, North Carolina- lbs - pounds
- PFMOAA - Perfluoro-2-methoxyaceticacid
Figure
11RaleighAugust 2019
2.4 lbs, 27%
Dry
Stormwater
3.6 lbs, 39%
River Intake
5.5 lbs, 61%
")")
")
")
")
")
")")
")
")")
")@@@@@@Waste Water Treatment Plant Discharge
Du Po nt A r e aWoodLinedTrench
Op en

C
h a nn el t o O ut fa ll 0 02
C oo l i n g Wat er C h an ne l
21A
22
23A
16
17A
17B
18
19A
19B
23B
6A 6B
24B
24A24C1
2 3
4
5
7A
8
910
11
12
13
14
15
20
7B
Paragraph 11(b) Sample Locations
Chemours Fayetteville Works, North Carolina
Figure
12Raleigh
500 0 500250 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Legend
!(Temporal Composite Sample
")Grab Sample
Sample Location Category
Intake
Stormwater
Discharge Areas
Wood Lined Trench
Cooling Water Channel
Open Channel to Outfall 002
Non-process wastewater
DuPont Area Ditches
Process wastewater
Outfall 002
Wastewater Treatment Plant Discharge
")")
")
")
")")@@@@@@Du Po nt A r e aWoodLinedTrench
Op en

C
h a nn el t o O ut fa ll 0 02
C oo l i n g Wat er C h an n e l
HFPO-DA and PFMOAA ConcentrationsApril 2019 Dry Event
Chemours Fayetteville Works, North Carolina
Figure
13Raleigh
500 0 500250 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Notes:Samples collected on April 24, 2019.All concentrations are in nanograms per liter.Location 20 collected from channel upstream of sump.Temporal composite samples collected over 4 hour interval.J – estimated valueUJ - Estimated reporting limitHFPO-DA - Hexafluoropropylene oxide dimer acidPFMOAA - Perfluoro-2-methoxyacetic acid
Legend
!(Temporal Composite Sample
")Grab Sample
Sample Location Category
Intake
Stormwater if present
Ditch Types
Wood Lined Trench
Cooling Water Channel
Open Channel to Outfall 002
Non-process wastewater
DuPont Area Ditches
Process wastewater
Outfall 002
Wastewater Treatment Plant Discharge
")")
WastewaterTreatmentPlant Discharge
WastewaterTreatmentPlant Discharge
* detained stormwater
18
23A
6A 6B
24B
24A
24C
921A
10
1
19A19B 22
7A
8 157B
14 20
HFPO-DA 14
PFMOAA <210 UJ
HFPO-DA 270
PFMOAA 1,300
HFPO-DA 13
PFMOAA <210
HFPO-DA 41
PFMOAA <210
HFPO-DA 59
PFMOAA <210
HFPO-DA 33
PFMOAA <210
HFPO-DA 320
PFMOAA <210 UJ
HFPO-DA 29
PFMOAA <210 UJ
HFPO-DA 16 J
PFMOAA <210
HFPO-DA 61
PFMOAA <210 UJ
HFPO-DA 14
PFMOAA <210 UJ
HFPO-DA 30 J
PFMOAA <210
HFPO-DA 22
PFMOAA <210
HFPO-DA 170
PFMOAA <210
HFPO-DA 120
PFMOAA 1,200 J
HFPO-DA 21
PFMOAA <210
HFPO-DA 34
PFMOAA <210 UJ
HFPO-DA 12
PFMOAA <210 UJ
HFPO-DA 14
PFMOAA <210 UJ
HFPO-DA 19
PFMOAA <210 UJ
HFPO-DA 33
PFMOAA <210
Cons tuent Result (ng/L)
**
**
")")
")
")
")
")
")")
")@@@@@@Du Po nt A r e aWoodLinedTrench
Op en

C
h a nn el t o O ut fa ll 0 02
C oo l i n g Wat er C h an n e l
23B
HFPO-DA and PFMOAA ConcentrationsJune 2019 Dry Event
Chemours Fayetteville Works, North Carolina
Figure
14Raleigh
500 0 500250 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Notes:Samples collected on June 27, 2019.All concentrations are in nanograms per liter.Temporal composite samples collected over 4 hour interval.J - estimated valueHFPO-DA - Hexafluoropropylene oxide dimer acidPFMOAA - Perfluoro-2-methoxyacetic acid
Legend
!(Temporal Composite Sample
")Grab Sample
Sample Location Category
Intake
Stormwater if present
Ditch Types
Wood Lined Trench
Cooling Water Channel
Open Channel to Outfall 002
Non-process wastewater
DuPont Area Ditches
Process wastewater
Outfall 002
Wastewater Treatment Plant Discharge
WastewaterTreatmentPlant Discharge
WastewaterTreatmentPlant Discharge
* detained stormwater
HFPO-DA 16
PFMOAA <5
HFPO-DA 10
PFMOAA <5
HFPO-DA 26
PFMOAA <210
HFPO-DA 3200
PFMOAA <210
HFPO-DA 170
PFMOAA 320
HFPO-DA 130 J
PFMOAA <210
HFPO-DA 40
PFMOAA <210
HFPO-DA 50
PFMOAA 48
HFPO-DA 9.6
PFMOAA <210
HFPO-DA 4.5 J
PFMOAA <210
HFPO-DA 4.1
PFMOAA <210
HFPO-DA 22
PFMOAA <5
HFPO-DA 45
PFMOAA 12
HFPO-DA 77
PFMOAA <21
HFPO-DA 100
PFMOAA <21
HFPO-DA 18
PFMOAA 69
HFPO-DA 22
PFMOAA <5
HFPO-DA 24
PFMOAA <210
HFPO-DA 66
PFMOAA <210
HFPO-DA 18
PFMOAA <5
Constituent Result (ng/L)
HFPO-DA 12.7
PFMOAA <10.6
**18
23A
6A 6B
24B
24A
24C
921A1
19A19B 22
7A
8 157B
14 20
")
")")
")
")")
")")
")")
")
")")
")")
")
")
")
")
")")
")
")")
")
")")")
Waste Water Treatment Plant Discharge
Du P o nt A r eaWoodLinedTrench
O p en Ch a n ne l t o O ut fa ll 0 02
C o o l i ng Wat er Ch an ne l
26
27
28
30
33
55
37
38-1
41
40
52
53
10
2 3
5
38-2
43
3435-1
39-1
35-2
39-2
3132
42-1
36
42-2
Stormwater Sampling Locations
Chemours Fayetteville Works, North Carolina
Figure
15Raleigh
500 0 500250 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Discharge Areas
Wood Lined Trench
Waste Water Treatment Plant Discharge
Cooling Water Channel
Open Channel to Outfall 002
DuPont Area Ditches
Legend
")Grab Sample
Sample Location Category
Stormwater
")
")")
")
")")
")")
")")
")
")")
")")
")
")
")
")
")")
")
")")
")
")")")
Waste Water Treatment Plant Discharge
Du P o nt A r eaWoodLinedTrench
O p en Ch a n ne l t o O ut fa ll 0 02
C o o l i ng Wat er Ch an ne l
26
27
28
30
33
55
37
38-1
41
40
52
53
10
2 3
5
38-2
43
3435-1
39-1
35-2
39-2
3132
42-1
36
42-2
HFPO-DA and PFMOAA ConcentrationsJune 2019 Storm Event
Chemours Fayetteville Works, North Carolina
Figure
16Raleigh
500 0 500250 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Legend
")Stormwater Grab Sample Location
Discharge Areas
Wood Lined Trench
Waste Water Treatment Plant Discharge
Cooling Water Channel
Open Channel to Outfall 002
DuPont Area Ditches
Notes:ng/L - nanograms per literB - detection in associated blankJ - estimated valueUJ - estimated reporting limitHFPO-DA - Hexafluoropropylene oxide dimer acidPFMOAA - Perfluoro-2-methoxyacetic acid
HFPO-DA 940
PFMOAA <210 UJ HFPO-DA 1800
PFMOAA <210 UJ
HFPO-DA 46 B
PFMOAA <210 UJ
HFPO-DA 170
PFMOAA <210 UJ
HFPO-DA 140
PFMOAA <210 UJ
HFPO-DA 160
PFMOAA <210 UJ
HFPO-DA 160
PFMOAA <210 UJ
HFPO-DA 54 J
PFMOAA <210 UJ
HFPO-DA 320
PFMOAA <210 UJ
HFPO-DA 490
PFMOAA 520 J
HFPO-DA 16000
PFMOAA 490 JHFPO-DA 4800
PFMOAA 26000 J HFPO-DA 46000
PFMOAA 105000 J
HFPO-DA 5400
PFMOAA 42000 J
HFPO-DA 880
PFMOAA <210 UJ
HFPO-DA 360
PFMOAA 210 J
HFPO-DA 940
PFMOAA 280 JHFPO-DA 590
PFMOAA <210 UJ
HFPO-DA 380
PFMOAA 240 JHFPO-DA 200 J
PFMOAA <210 UJ
HFPO-DA 470
PFMOAA <210 UJ
HFPO-DA 660
PFMOAA <210 UJ
HFPO-DA 3500
PFMOAA 2200 J
HFPO-DA 830
PFMOAA <210 UJ
HFPO-DA 250
PFMOAA <210 UJ
HFPO-DA 290
PFMOAA <210 UJ
HFPO-DA 130
PFMOAA 10000 J
HFPO-DA 310 J
PFMOAA <210 UJ
Constituent Result (ng/L)
HFPO-DA 490
PFMOAA 520
1
8
18
22*
23A
23A-1
23A-2
Wastewater Treatment Plant Sampling Locations
Chemours Fayetteville Works, North Carolina
Figure
17Raleigh
500 0 500250 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Notes:Samples were collected as 24-hr composite samples.All samples were collected simultaneously except Location 8,which was collected 1 hydraulic residence time after the otherlocations.* Due to a sediment blockage, sample was only collected over 8hours. Results may potentially be influenced by presence ofsediment.Aerial imagery provided by Esri basemaps (2017).
Sample Location Category
Intake
Process wastewater
Non-process wastewater
Legend
Pipe Connection to Facility
Terracotta Pipe and Piping Connected to Terracotta Pipe
Grouted Pipe Section
!(Temporal Composite Sample
Site Areas
Chemours Monomer IXM Area
Kuraray Trosifol® Manufacturing Operations
Kuraray Laboratory
Kuraray SentryGlas® Manufacturing Operations
Power - Filtered and Demineralized Water Production
Wastewater Treatment Plant
1
8
18
22*
23A
23A-1
23A-2
HFPO-DA and PFMOAA ConcentrationsWastewater Treatment Plant Sampling
Chemours Fayetteville Works, North Carolina
Figure
18Raleigh
500 0 500250 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Notes:Samples were collected as 24-hr composite samples.All samples were collected simultaneously except Location 8, whichwas collected 1 hydraulic residence time after the other locations.Data reported here are from the Fayetteville Works onsitelaboratory. Sample results from TestAmerica were still pending attime of report preparation.* Due to a sediment blockage, sample was only collected over 8hours. Results may potentially be influenced by presence of
sediment.ng/L - nanograms per literAerial imagery provided by Esri basemaps (2017).
Sample Location Category
Intake
Process wastewater
Non-process wastewater
Legend
Pipe Connection to Facility
Terracotta Pipe and Piping Connected to Terracotta Pipe
Grouted Pipe Section
!(Temporal Composite Sample
Site Areas
Chemours Monomer IXM Area
Kuraray Trosifol® Manufacturing Operations
Kuraray Laboratory
Kuraray SentryGlas® Manufacturing Operations
Power - Filtered and Demineralized Water Production
Wastewater Treatment Plant
HFPO-DA <12
PFMOAA <11
HFPO-DA 54
PFMOAA <11
HFPO-DA <12
PFMOAA <11
HFPO-DA 2600*
PFMOAA 1600*
HFPO-DA 9400
PFMOAA <11
HFPO-DA 13
PFMOAA <11
Cons tuent Result (ng/L)
HFPO-DA 13
PFMOAA <11
HFPO-DA 66
PFMOAA 600
!(!(!(
!(!(
!(!(!(
DuPont Area Ditche
s Cool
ing
Water ChannelWood Lined Trench
Open Cha nn el t o Out fall 0 02
SD-DNSS-G-070319
SD-DNSS-F-070319
SD-DNSS-C-070319
Composite Sediment Sample Locations
Chemours Fayetteville Works, North Carolina
Figure
19Raleigh
500 0 500250 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Notes:
1. Sediment samples collected July 3, 2019.2. Samples were collected from individual locations thencomposited for analysis.3. Basemap source: Esri, DigitalGlobe, GeoEye, EarthstarGeographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, andthe GIS User Community
Legend
!(Composite Sediment Sample Location
Ditch Types
Wood Lined Trench
Wastewater Treatment Plant Discharge
Cooling Water Channel
Open Channel to Outfall 002
DuPont Area Ditches
!(!(!(
!(!(
!(!(!(
DuPont Area Ditche
s Cool
ing Water Channe
lWood Lined Trench
Open Cha nn el t o Out fall 0 02
SD-DNSS-G-070319-D
SD-DNSS-F-070319
SD-DNSS-C-070319
Results of Deionized Water Added to Composite Sediment Samples
Chemours Fayetteville Works, North Carolina
Figure
20Raleigh
500 0 500250 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Notes:ng/L - nanograms per liter
1. Sediment samples collected July 3, 2019.2. Duplicate results for Location SD-DNSS-G-070319 are reportedhere since parent sample was analyzed as separate samplesinstead of being composited from all locations. All results areprovided in Table X.3. Data reported here are from the Fayetteville Works onsitelaboratory. Sample results from TestAmerica were still pending attime of report preparation.4. Equal masses of deionized water and sediment (approximately100-g each) were combined together in a high-density polyethylene(HDPE) bottle and mixed together. The resulting overlying waterwas then analyzed.5. Basemap source: Esri, DigitalGlobe, GeoEye, EarthstarGeographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, andthe GIS User Community
Legend
!(Composite Sediment Sample Location
Ditch Types
Wood Lined Trench
Wastewater Treatment Plant Discharge
Cooling Water Channel
Open Channel to Outfall 002
DuPont Area Ditches
HFPO-DA 27
PFMOAA <11
HFPO-DA 320
PFMOAA <11
HFPO-DA 1400
PFMOAA 560
Cons tuent Result (ng/L)
HFPO-DA 1400
PFMOAA 560
#*
#*
#*")D u P o n t A r e a
O p en C h a n ne l t o O u t f al l 0 0 2
WastewaterTreatement
Plant Discharge
20E*20B
20C
20D
Additional Outfall 002 Sample Locations
Chemours Fayetteville Works, North Carolina
Figure
21Raleigh
400 0 400200 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Notes:Spatial composite samples collected as three grab samples alongchannel cross section then composited together.Samples collected 30 May 2019.* Location 20E was collected from the sump at the end of theOpen Channel.
Legend
")Grab Sample
#*Spatial Composite Sample
Sample Location Category
Non-process wastewater
Outfall 002
Stormwater
Process wastewater
Ditch Types
Wood Lined Trench
Cooling Water Channel
Open Channel to Outfall 002
DuPont Area Ditches
Wastewater Treatment Plant Discharge
#*
#*
#*")D u P o n t A r e a
O p en C h a n ne l t o O u t f al l 0 0 2
WastewaterTreatement
Plant Discharge
20E*20B
20C
20D
HFPO-DA and PFMOAA Concentrations – Additional Outfall 002 Samples - May 2019 Event
Chemours Fayetteville Works, North Carolina
Figure
22Raleigh
400 0 400200 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Notes:J - estimated valueAll concentrations are in nanograms per liter.Spatial composite samples collected as three grab samples alongchannel cross section then composited together.Samples collected 30 May 2019.Intake and Outfall 002 PFMOAA concentrations in late May andearly June 2019 are described in the Observations of ElevatedPFAS Concentrations at the Cape Fear River Intake and Outfall002 Sample Locations in May and June 2019 Memorandum(Geosyntec, 2019B).* Location 20E was collected from the sump at the end of theOpen Channel.
Legend
")Grab Sample
#*Spatial Composite Sample
Sample Location Category
Non-process wastewater
Outfall 002
Stormwater
Process wastewater
Ditch Types
Wood Lined Trench
Cooling Water Channel
Open Channel to Outfall 002
DuPont Area Ditches
Wastewater Treatment Plant Discharge
HFPO-DA 89
PFMOAA 2,600 J
HFPO-DA 110
PFMOAA 2,500 J
HFPO-DA <86
PFMOAA 2,800 J
HFPO-DA <86
PFMOAA 2,400 J
130
2,500 J
DuplicatePrimary
APPENDIX A
Laboratory Reports & DVM Report
Note: Laboratory Reports provided separately
ADQM Data Review Narrative - FAY 2019 Additional Samp.doc 1 of 3
ADQM DATA REVIEW NARRATIVE
Site Chemours FAY – Fayetteville
Project 2019 Additional Sampling
Project Reviewer Michael Aucoin, AECOM as a Chemours contractor
Sampling Dates June 5, 2019
Analytical Protocol
Laboratory Analytical Method Parameter(s)
TestAmerica - Sacramento 537 Modified PFAS1
TestAmerica - Sacramento Cl. Spec. Table 3 Compound SOP Table 3+ compounds
TestAmerica - Sacramento SM 2540 D-1997 TSS
1 Perfluoroalkylsubstances, a list of 33 compounds including HFPO-DA.
Sample Receipt
The following items are noted for this data set:
•All samples were received in satisfactory condition and within EPA temperature guidelines onJune 8, 2019.
•Field sample IDs ending with -Z were submitted for lab filtration to provide dissolved pfas andTable 3+ results.
Data Review
The electronic data submitted for this project was reviewed via the Data Verification Module (DVM) process.
Overall the data is acceptable for use without qualification, except as noted below:
•Non-detect results for TSS in one sample and one field blank were qualified R and are consideredto be unusable due to analysis greater than two times the analytical hold time.
•The HFPO-DA result in one field sample and PMPA results in two field samples were qualified Band may be biased high, or may be false positives, due to a comparable concentration in theassociated trip (travel) blank.
•Table 3+ sample results were qualified J as estimated, and non-detect results were qualified UJ,and the reporting limit may be biased low, because the lab established holding time wasexceeded.
•Several analytical results have been qualified J as estimated, and non-detect results qualified UJ
indicating an estimated reporting limit, due to matrix spike or surrogate recovery outside criteria,and; poor field duplicate, lab replicate, or LCSD precision. See the Data Verification Module
ADQM Data Review Narrative - FAY 2019 Additional Samp.doc 2 of 3
(DVM) Narrative Report for which samples were qualified, the specific reasons for qualification, and potential bias in reported results.
Attachments The DVM Narrative report is attached. The lab reports due to a large page count are stored on an AECOM network shared drive and are available to be posted on external shared drives, or on a flash
drive.

ADQM Data Review Narrative - FAY 2019 Additional Samp.doc 3 of 3
Data Verification Module (DVM)
The DVM is an internal review process used by the ADQM group to assist with the determination of data usability. The electronic data deliverables received from the laboratory are loaded into the Locus EIM™ database and processed through a series of data quality checks, which are a combination of software (Locus EIM™ database Data Verification Module (DVM)) and manual reviewer evaluations. The data is evaluated against the following data usability checks:
• Field and laboratory blank contamination
• US EPA hold time criteria
• Missing Quality Control (QC) samples
• Matrix spike(MS)/matrix spike duplicate (MSD) recoveries and the relative percent differences
(RPDs) between these spikes
• Laboratory control sample(LCS)/control sample duplicate (LCSD) recoveries and the RPD
between these spikes
• Surrogate spike recoveries for organic analyses
• RPD between field duplicate sample pairs
• RPD between laboratory replicates for inorganic analyses
• Difference / percent difference between total and dissolved sample pairs. There are two qualifier fields in EIM: Lab Qualifier is the qualifier assigned by the lab and may not reflect the usability of the data. This qualifier may have many different meanings and can vary between labs and over time within the same lab. Please refer to the laboratory report for a description of the lab qualifiers. As they are lab descriptors they are not to be used when evaluating the data. Validation Qualifier is the 3rd party formal validation qualifier if this was performed. Otherwise this field contains the qualifier resulting from the ADQM DVM review process. This qualifier assesses the usability of the data and may not equal the lab qualifier. The DVM applies the following data
evaluation qualifiers to analysis results, as warranted: Qualifier Definition B Not detected substantially above the level reported in the laboratory or field blanks. R Unusable result. Analyte may or may not be present in the sample.
J Analyte present. Reported value may not be accurate or precise.
UJ Not detected. Reporting limit may not be accurate or precise.

The Validation Status Code field is set to “DVM” if the ADQM DVM process has been performed. If the DVM has not been run, the field will be blank.
If the DVM has been run (Validation Status Code equals “DVM”), use the Validation Qualifier.
DVM Narrative ReportThe analysis hold time for this sample was exceeded by a factor of 2. The reported non-detect result is unusable.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-FB-060519 06/05/2019 320-51141-2 Total SuspendedSolids5.0 MG/L5.02540 D-1997R5.0MDLASTW-LOC31-060519-D 06/05/2019 320-51215-3 Total SuspendedSolids5.0 MG/L5.02540 D-1997R5.0MDLPage 1 of 223
Contamination detected in trip blank(s). Sample result does not differ significantly from the analyte concentration detected in the associated trip blank(s).LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC26-060519 06/05/2019 320-51135-1 Hfpo Dimer Acid0.046 UG/L537 ModifiedB3535_PFC0.0040PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PMPA0.79 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.57PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PMPA0.72 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.57PQLPage 2 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC28-060519 06/05/2019 320-51135-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC28-060519 06/05/2019 320-51135-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC28-060519 06/05/2019 320-51135-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC28-060519 06/05/2019 320-51135-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC28-060519 06/05/2019 320-51135-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC28-060519 06/05/2019 320-51135-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC28-060519 06/05/2019 320-51135-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLPage 3 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC28-060519 06/05/2019 320-51135-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC28-060519 06/05/2019 320-51135-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC28-060519 06/05/2019 320-51135-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC28-060519 06/05/2019 320-51135-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC28-060519 06/05/2019 320-51135-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC28-060519 06/05/2019 320-51135-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC28-060519 06/05/2019 320-51135-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLPage 4 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC26-060519-Z 06/05/2019 320-51274-1 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519 06/05/2019 320-51135-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC27-060519 06/05/2019 320-51135-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 5 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC27-060519-Z 06/05/2019 320-51274-2 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 6 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC26-060519-Z 06/05/2019 320-51274-1 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PFO3OA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PFO3OA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PFO4DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PFO4DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PFO5DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PFO5DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PFESA-BP20.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PFESA-BP20.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 7 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC26-060519-Z 06/05/2019 320-51274-1 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC27-060519 06/05/2019 320-51135-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC27-060519 06/05/2019 320-51135-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC27-060519 06/05/2019 320-51135-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC27-060519 06/05/2019 320-51135-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLPage 8 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC27-060519 06/05/2019 320-51135-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC27-060519 06/05/2019 320-51135-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC27-060519 06/05/2019 320-51135-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC27-060519 06/05/2019 320-51135-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC27-060519 06/05/2019 320-51135-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC27-060519 06/05/2019 320-51135-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC27-060519 06/05/2019 320-51135-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC27-060519 06/05/2019 320-51135-2 2-(N-methyl perfluoro-1-0.11 ug/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.11PQLPage 9 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitoctanesulfonamido)-ethanolSOPASTW-LOC27-060519 06/05/2019 320-51135-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC27-060519 06/05/2019 320-51135-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC27-060519 06/05/2019 320-51135-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC27-060519 06/05/2019 320-51135-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC27-060519 06/05/2019 320-51135-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC27-060519 06/05/2019 320-51135-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC27-060519 06/05/2019 320-51135-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC27-060519 06/05/2019 320-51135-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519 06/05/2019 320-51135-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC28-060519 06/05/2019 320-51135-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC28-060519 06/05/2019 320-51135-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC28-060519 06/05/2019 320-51135-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC28-060519 06/05/2019 320-51135-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC28-060519 06/05/2019 320-51135-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLPage 10 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC28-060519 06/05/2019 320-51135-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC28-060519 06/05/2019 320-51135-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519 06/05/2019 320-51135-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC28-060519 06/05/2019 320-51135-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC28-060519 06/05/2019 320-51135-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 2-(N-methyl perfluoro-1-0.0020 ug/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.0020PQLPage 11 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitoctanesulfonamido)-ethanolSOPASTW-LOC28-060519-Z 06/05/2019 320-51274-3 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519 06/05/2019 320-51128-1 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC3-060519 06/05/2019 320-51128-1 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC3-060519 06/05/2019 320-51128-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC3-060519 06/05/2019 320-51128-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC3-060519 06/05/2019 320-51128-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC3-060519 06/05/2019 320-51128-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PEPA0.047 UG/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.047PQLPage 12 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPASTW-LOC3-060519 06/05/2019 320-51128-1 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC3-060519 06/05/2019 320-51128-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC3-060519 06/05/2019 320-51128-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC3-060519 06/05/2019 320-51128-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC3-060519 06/05/2019 320-51128-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC3-060519 06/05/2019 320-51128-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLPage 13 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC3-060519 06/05/2019 320-51128-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC3-060519 06/05/2019 320-51128-1 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC3-060519 06/05/2019 320-51128-1 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 14 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC3-060519 06/05/2019 320-51128-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC3-060519 06/05/2019 320-51128-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC3-060519 06/05/2019 320-51128-1 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC3-060519 06/05/2019 320-51128-1 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC3-060519 06/05/2019 320-51128-1 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC3-060519 06/05/2019 320-51128-1 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC3-060519 06/05/2019 320-51128-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC3-060519 06/05/2019 320-51128-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 15 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC26-060519 06/05/2019 320-51135-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC26-060519 06/05/2019 320-51135-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC26-060519 06/05/2019 320-51135-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC26-060519 06/05/2019 320-51135-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLPage 16 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC26-060519 06/05/2019 320-51135-1 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC26-060519 06/05/2019 320-51135-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC26-060519 06/05/2019 320-51135-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC26-060519 06/05/2019 320-51135-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC26-060519 06/05/2019 320-51135-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLPage 17 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC26-060519 06/05/2019 320-51135-1 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC26-060519 06/05/2019 320-51135-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC26-060519 06/05/2019 320-51135-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC26-060519 06/05/2019 320-51135-1 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC26-060519 06/05/2019 320-51135-1 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 18 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC26-060519 06/05/2019 320-51135-1 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC26-060519 06/05/2019 320-51135-1 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC26-060519 06/05/2019 320-51135-1 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC26-060519 06/05/2019 320-51135-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC26-060519 06/05/2019 320-51135-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC26-060519 06/05/2019 320-51135-1 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC26-060519 06/05/2019 320-51135-1 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC26-060519 06/05/2019 320-51135-1 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC26-060519 06/05/2019 320-51135-1 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC26-060519 06/05/2019 320-51135-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC26-060519 06/05/2019 320-51135-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 NVHOS0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 NVHOS0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 19 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC2-060519 06/05/2019 320-51140-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC2-060519 06/05/2019 320-51140-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC2-060519 06/05/2019 320-51140-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC2-060519 06/05/2019 320-51140-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLPage 20 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC2-060519 06/05/2019 320-51140-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC2-060519 06/05/2019 320-51140-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC2-060519 06/05/2019 320-51140-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC2-060519 06/05/2019 320-51140-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC2-060519 06/05/2019 320-51140-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC2-060519 06/05/2019 320-51140-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC2-060519 06/05/2019 320-51140-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC2-060519 06/05/2019 320-51140-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLPage 21 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC2-060519 06/05/2019 320-51140-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC2-060519 06/05/2019 320-51140-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC2-060519 06/05/2019 320-51140-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC2-060519 06/05/2019 320-51140-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC2-060519 06/05/2019 320-51140-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC2-060519 06/05/2019 320-51140-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC2-060519 06/05/2019 320-51140-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC2-060519 06/05/2019 320-51140-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC2-060519 06/05/2019 320-51140-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC2-060519 06/05/2019 320-51140-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC2-060519 06/05/2019 320-51140-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 2-(N-methyl perfluoro-1-octanesulfonamido)0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 22 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnit-ethanolASTW-LOC2-060519-Z 06/05/2019 320-51243-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519 06/05/2019 320-51141-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-FB-060519 06/05/2019 320-51141-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-FB-060519 06/05/2019 320-51141-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-FB-060519 06/05/2019 320-51141-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-FB-060519 06/05/2019 320-51141-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-FB-060519 06/05/2019 320-51141-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-FB-060519 06/05/2019 320-51141-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-FB-060519 06/05/2019 320-51141-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 NVHOS0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 NVHOS0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PMPA0.010 UG/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.010PQLPage 23 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPASTW-FB-060519-Z 06/05/2019 320-51275-2 PMPA0.010 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.010PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PEPA0.020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PFESA-BP10.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PFO2HxA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PFO2HxA0.0020 ug/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.0020PQLPage 24 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPASTW-FB-060519-Z 06/05/2019 320-51275-2 PFO3OA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PFO3OA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PFO4DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PFO4DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PFO5DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PFO5DA0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PFMOAA0.0050 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0050PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PFESA-BP20.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PFESA-BP20.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 25 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-FB-060519-Z 06/05/2019 320-51275-2 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 R-EVE0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 R-EVE0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 Byproduct 40.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 Byproduct 40.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 Byproduct 50.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 Byproduct 50.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519-Z 06/05/2019 320-51275-2 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-FB-060519 06/05/2019 320-51141-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-FB-060519 06/05/2019 320-51141-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-FB-060519 06/05/2019 320-51141-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-FB-060519 06/05/2019 320-51141-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-FB-060519 06/05/2019 320-51141-2 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-FB-060519 06/05/2019 320-51141-2 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-FB-060519 06/05/2019 320-51141-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 26 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-FB-060519 06/05/2019 320-51141-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-FB-060519 06/05/2019 320-51141-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-FB-060519 06/05/2019 320-51141-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-FB-060519 06/05/2019 320-51141-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-FB-060519 06/05/2019 320-51141-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-FB-060519 06/05/2019 320-51141-2 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLASTW-FB-060519 06/05/2019 320-51141-2 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLASTW-FB-060519 06/05/2019 320-51141-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-FB-060519 06/05/2019 320-51141-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-FB-060519 06/05/2019 320-51141-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-FB-060519 06/05/2019 320-51141-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-FB-060519 06/05/2019 320-51141-2 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-FB-060519 06/05/2019 320-51141-2 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-FB-060519 06/05/2019 320-51141-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-FB-060519 06/05/2019 320-51141-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLPage 27 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-FB-060519 06/05/2019 320-51141-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-FB-060519 06/05/2019 320-51141-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-FB-060519 06/05/2019 320-51141-2 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-FB-060519 06/05/2019 320-51141-2 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-FB-060519 06/05/2019 320-51141-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-FB-060519 06/05/2019 320-51141-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-FB-060519 06/05/2019 320-51141-2 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-FB-060519 06/05/2019 320-51141-2 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-FB-060519 06/05/2019 320-51141-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-FB-060519 06/05/2019 320-51141-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-FB-060519 06/05/2019 320-51141-2 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-FB-060519 06/05/2019 320-51141-2 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-FB-060519 06/05/2019 320-51141-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-FB-060519 06/05/2019 320-51141-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-FB-060519 06/05/2019 320-51141-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-FB-060519 06/05/2019 320-51141-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 28 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC10-060519 06/05/2019 320-51128-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC10-060519 06/05/2019 320-51128-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC10-060519 06/05/2019 320-51128-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC10-060519 06/05/2019 320-51128-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC10-060519 06/05/2019 320-51128-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC10-060519 06/05/2019 320-51128-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC10-060519 06/05/2019 320-51128-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC10-060519 06/05/2019 320-51128-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC10-060519 06/05/2019 320-51128-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC10-060519 06/05/2019 320-51128-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC10-060519 06/05/2019 320-51128-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLPage 29 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLPage 30 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC31-060519-D 06/05/2019 320-51215-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 31 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC31-060519-Z 06/05/2019 320-51220-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PFO5DA0.034 ug/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.034PQLPage 32 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLPage 33 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC31-060519-Z 06/05/2019 320-51220-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 2-(N-methyl perfluoro-1-octanesulfonamido)0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLPage 34 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnit-ethanolASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.037PQLPage 35 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLPage 36 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC31-060519-Z-D06/05/2019 320-51220-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC32-060519 06/05/2019 320-51215-5 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC32-060519 06/05/2019 320-51215-5 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC31-060519 06/05/2019 320-51215-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC31-060519 06/05/2019 320-51215-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLPage 37 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC31-060519 06/05/2019 320-51215-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC31-060519 06/05/2019 320-51215-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC31-060519 06/05/2019 320-51215-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC31-060519 06/05/2019 320-51215-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC32-060519 06/05/2019 320-51215-5 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC32-060519 06/05/2019 320-51215-5 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC32-060519 06/05/2019 320-51215-5 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC32-060519 06/05/2019 320-51215-5 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLPage 38 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC32-060519 06/05/2019 320-51215-5 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLASTW-LOC32-060519 06/05/2019 320-51215-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC32-060519 06/05/2019 320-51215-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC32-060519 06/05/2019 320-51215-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC32-060519 06/05/2019 320-51215-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC32-060519 06/05/2019 320-51215-5 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC32-060519 06/05/2019 320-51215-5 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLPage 39 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC32-060519 06/05/2019 320-51215-5 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC32-060519 06/05/2019 320-51215-5 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC32-060519 06/05/2019 320-51215-5 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC32-060519 06/05/2019 320-51215-5 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC32-060519 06/05/2019 320-51215-5 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC32-060519 06/05/2019 320-51215-5 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC32-060519 06/05/2019 320-51215-5 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC32-060519 06/05/2019 320-51215-5 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC32-060519 06/05/2019 320-51215-5 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC32-060519 06/05/2019 320-51215-5 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLPage 40 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC30-060519 06/05/2019 320-51215-1 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC30-060519 06/05/2019 320-51215-1 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 41 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC30-060519 06/05/2019 320-51215-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC30-060519 06/05/2019 320-51215-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC30-060519 06/05/2019 320-51215-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC30-060519 06/05/2019 320-51215-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC30-060519 06/05/2019 320-51215-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC30-060519 06/05/2019 320-51215-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC30-060519 06/05/2019 320-51215-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC30-060519 06/05/2019 320-51215-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC30-060519 06/05/2019 320-51215-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC30-060519 06/05/2019 320-51215-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 42 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC3-060519-Z 06/05/2019 320-51271-1 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC30-060519 06/05/2019 320-51215-1 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC30-060519 06/05/2019 320-51215-1 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC30-060519 06/05/2019 320-51215-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC30-060519 06/05/2019 320-51215-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC30-060519 06/05/2019 320-51215-1 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC30-060519 06/05/2019 320-51215-1 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC30-060519 06/05/2019 320-51215-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC30-060519 06/05/2019 320-51215-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 2-(N-methyl perfluoro-1-octanesulfonamido)0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLPage 43 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnit-ethanolASTW-LOC30-060519-Z 06/05/2019 320-51220-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 R-EVE0.070 UG/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.070PQLPage 44 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPASTW-LOC30-060519-Z 06/05/2019 320-51220-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC31-060519 06/05/2019 320-51215-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC31-060519 06/05/2019 320-51215-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC31-060519 06/05/2019 320-51215-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC31-060519 06/05/2019 320-51215-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC31-060519 06/05/2019 320-51215-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC31-060519 06/05/2019 320-51215-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PFO2HxA0.081 ug/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.081PQLPage 45 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPASTW-LOC31-060519 06/05/2019 320-51215-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC31-060519 06/05/2019 320-51215-2 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC31-060519 06/05/2019 320-51215-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC31-060519 06/05/2019 320-51215-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC31-060519 06/05/2019 320-51215-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC31-060519 06/05/2019 320-51215-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC31-060519 06/05/2019 320-51215-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC31-060519 06/05/2019 320-51215-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC31-060519 06/05/2019 320-51215-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC31-060519 06/05/2019 320-51215-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLPage 46 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC31-060519-D 06/05/2019 320-51215-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLPage 47 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC31-060519-D 06/05/2019 320-51215-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLPage 48 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC31-060519-D 06/05/2019 320-51215-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC31-060519-D 06/05/2019 320-51215-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLPage 49 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC32-060519-Z 06/05/2019 320-51220-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC33-060519 06/05/2019 320-51089-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 50 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC33-060519 06/05/2019 320-51089-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC33-060519 06/05/2019 320-51089-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC33-060519 06/05/2019 320-51089-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC33-060519 06/05/2019 320-51089-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC33-060519 06/05/2019 320-51089-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC33-060519 06/05/2019 320-51089-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC33-060519 06/05/2019 320-51089-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC33-060519 06/05/2019 320-51089-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC33-060519 06/05/2019 320-51089-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC33-060519 06/05/2019 320-51089-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC33-060519 06/05/2019 320-51089-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC33-060519 06/05/2019 320-51089-1 Byproduct 60.015 UG/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.015PQLPage 51 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPASTW-LOC33-060519 06/05/2019 320-51089-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 EVE Acid0.024 UG/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.024PQLPage 52 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC34-060519 06/05/2019 320-51089-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC34-060519 06/05/2019 320-51089-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC34-060519 06/05/2019 320-51089-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC34-060519 06/05/2019 320-51089-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC34-060519 06/05/2019 320-51089-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC34-060519 06/05/2019 320-51089-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC34-060519 06/05/2019 320-51089-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC34-060519 06/05/2019 320-51089-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC34-060519 06/05/2019 320-51089-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC34-060519 06/05/2019 320-51089-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC34-060519 06/05/2019 320-51089-2 PEPA0.047 UG/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.047PQLPage 53 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPASTW-LOC34-060519 06/05/2019 320-51089-2 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC34-060519 06/05/2019 320-51089-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC34-060519 06/05/2019 320-51089-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC34-060519 06/05/2019 320-51089-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC34-060519 06/05/2019 320-51089-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC34-060519 06/05/2019 320-51089-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC34-060519 06/05/2019 320-51089-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC34-060519 06/05/2019 320-51089-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC34-060519 06/05/2019 320-51089-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC34-060519 06/05/2019 320-51089-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC34-060519 06/05/2019 320-51089-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC34-060519 06/05/2019 320-51089-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC34-060519 06/05/2019 320-51089-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC34-060519 06/05/2019 320-51089-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLPage 54 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC34-060519 06/05/2019 320-51089-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC34-060519 06/05/2019 320-51089-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC34-060519 06/05/2019 320-51089-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC34-060519 06/05/2019 320-51089-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC34-060519 06/05/2019 320-51089-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC34-060519 06/05/2019 320-51089-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC34-060519 06/05/2019 320-51089-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC34-060519 06/05/2019 320-51089-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC34-060519 06/05/2019 320-51089-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 55 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC34-060519-Z 06/05/2019 320-51232-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 R-EVE0.070 UG/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.070PQLPage 56 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPASTW-LOC34-060519-Z 06/05/2019 320-51232-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 57 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC35-1-060519 06/05/2019 320-51089-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLPage 58 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC35-1-060519 06/05/2019 320-51089-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLPage 59 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLPage 60 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLPage 61 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLPage 62 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLPage 63 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLPage 64 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC35-2-060519 06/05/2019 320-51136-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 2-(N-ethyl perfluoro-1-octanesulfonamido)0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 65 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnit-ethanolASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC36-060519 06/05/2019 320-51139-1 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC36-060519 06/05/2019 320-51139-1 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLPage 66 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC36-060519 06/05/2019 320-51139-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC36-060519 06/05/2019 320-51139-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC36-060519 06/05/2019 320-51139-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC36-060519 06/05/2019 320-51139-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC36-060519 06/05/2019 320-51139-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC36-060519 06/05/2019 320-51139-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC36-060519 06/05/2019 320-51139-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC36-060519 06/05/2019 320-51139-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC36-060519 06/05/2019 320-51139-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLPage 67 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC36-060519 06/05/2019 320-51139-1 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC36-060519 06/05/2019 320-51139-1 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC36-060519 06/05/2019 320-51139-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC36-060519 06/05/2019 320-51139-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 68 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC36-060519-D 06/05/2019 320-51139-5 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC36-060519 06/05/2019 320-51139-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC36-060519 06/05/2019 320-51139-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC36-060519 06/05/2019 320-51139-1 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC36-060519 06/05/2019 320-51139-1 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLPage 69 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC36-060519-D 06/05/2019 320-51139-5 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLPage 70 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC36-060519-D 06/05/2019 320-51139-5 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 71 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC36-060519-Z 06/05/2019 320-51251-1 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 72 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC37-060519 06/05/2019 320-51139-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC37-060519 06/05/2019 320-51139-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC37-060519 06/05/2019 320-51139-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC37-060519 06/05/2019 320-51139-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC37-060519 06/05/2019 320-51139-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC37-060519 06/05/2019 320-51139-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC37-060519 06/05/2019 320-51139-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC37-060519 06/05/2019 320-51139-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLPage 73 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC37-060519 06/05/2019 320-51139-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC37-060519 06/05/2019 320-51139-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC37-060519 06/05/2019 320-51139-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC37-060519 06/05/2019 320-51139-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC37-060519 06/05/2019 320-51139-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC37-060519 06/05/2019 320-51139-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC37-060519 06/05/2019 320-51139-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC37-060519 06/05/2019 320-51139-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC37-060519 06/05/2019 320-51139-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC37-060519 06/05/2019 320-51139-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC37-060519 06/05/2019 320-51139-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC37-060519 06/05/2019 320-51139-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLPage 74 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC37-060519 06/05/2019 320-51139-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC37-060519 06/05/2019 320-51139-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC37-060519 06/05/2019 320-51139-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 75 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC37-060519-Z 06/05/2019 320-51251-2 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLPage 76 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC38-1-060519 06/05/2019 320-51139-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0030PQLPage 77 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0030PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0055 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0055PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0055 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0055PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PFECA B0.060 UG/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.060PQLPage 78 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPASTW-LOC38-2-060519 06/05/2019 320-51136-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PES0.0023 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0023PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PES0.0023 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0023PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 EVE Acid0.024 UG/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.024PQLPage 79 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPASTW-LOC38-2-060519 06/05/2019 320-51136-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLPage 80 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLPage 81 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC39-1-060519 06/05/2019 320-51134-1 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLPage 82 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC39-1-060519 06/05/2019 320-51134-1 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLPage 83 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC39-1-060519 06/05/2019 320-51134-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 84 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 2-(N-methyl perfluoro-1-0.11 ug/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.11PQLPage 85 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitoctanesulfonamido)-ethanolSOPASTW-LOC39-2-060519 06/05/2019 320-51136-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLPage 86 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC39-2-060519 06/05/2019 320-51136-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 2-(N-methyl perfluoro-1-0.0020 ug/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.0020PQLPage 87 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitoctanesulfonamido)-ethanolSOPASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519 06/05/2019 320-51134-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC40-060519 06/05/2019 320-51134-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLPage 88 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC40-060519 06/05/2019 320-51134-2 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC40-060519 06/05/2019 320-51134-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC40-060519 06/05/2019 320-51134-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC40-060519 06/05/2019 320-51134-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC40-060519 06/05/2019 320-51134-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC40-060519 06/05/2019 320-51134-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC40-060519 06/05/2019 320-51134-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC40-060519 06/05/2019 320-51134-2 Total SuspendedSolids5.0 MG/L5.02540 D-1997UJ5.0MDLASTW-LOC40-060519 06/05/2019 320-51134-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC40-060519 06/05/2019 320-51134-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLPage 89 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC40-060519 06/05/2019 320-51134-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC40-060519 06/05/2019 320-51134-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC40-060519 06/05/2019 320-51134-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC40-060519 06/05/2019 320-51134-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC40-060519 06/05/2019 320-51134-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC40-060519 06/05/2019 320-51134-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC40-060519 06/05/2019 320-51134-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC40-060519 06/05/2019 320-51134-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC40-060519 06/05/2019 320-51134-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC40-060519 06/05/2019 320-51134-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 90 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 91 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC40-060519-Z 06/05/2019 320-51276-2 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519 06/05/2019 320-51134-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC41-060519 06/05/2019 320-51134-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC41-060519 06/05/2019 320-51134-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC41-060519 06/05/2019 320-51134-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC41-060519 06/05/2019 320-51134-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC41-060519 06/05/2019 320-51134-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLPage 92 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC41-060519 06/05/2019 320-51134-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC41-060519 06/05/2019 320-51134-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC41-060519 06/05/2019 320-51134-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC41-060519 06/05/2019 320-51134-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC41-060519 06/05/2019 320-51134-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC41-060519 06/05/2019 320-51134-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC41-060519 06/05/2019 320-51134-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 93 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC41-060519 06/05/2019 320-51134-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC41-060519 06/05/2019 320-51134-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC41-060519 06/05/2019 320-51134-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC41-060519 06/05/2019 320-51134-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC41-060519 06/05/2019 320-51134-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC41-060519 06/05/2019 320-51134-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC41-060519 06/05/2019 320-51134-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC41-060519 06/05/2019 320-51134-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC41-060519 06/05/2019 320-51134-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 2-(N-methyl perfluoro-1-0.0020 ug/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.0020PQLPage 94 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitoctanesulfonamido)-ethanolSOPASTW-LOC41-060519-Z 06/05/2019 320-51276-3 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLPage 95 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC42-1-060519 06/05/2019 320-51140-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 96 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 2-(N-ethyl perfluoro-1-0.060 ug/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.060PQLPage 97 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitoctanesulfonamido)-ethanolSOPASTW-LOC42-2-060519 06/05/2019 320-51141-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLPage 98 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC43-060519 06/05/2019 320-51140-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC43-060519 06/05/2019 320-51140-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC43-060519 06/05/2019 320-51140-2 2-(N-methyl perfluoro-1-0.11 ug/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.11PQLPage 99 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitoctanesulfonamido)-ethanolSOPASTW-LOC43-060519 06/05/2019 320-51140-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC43-060519 06/05/2019 320-51140-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC43-060519 06/05/2019 320-51140-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC43-060519 06/05/2019 320-51140-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC43-060519 06/05/2019 320-51140-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLPage 100 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC43-060519-Z 06/05/2019 320-51243-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC5-060519 06/05/2019 320-51128-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC5-060519 06/05/2019 320-51128-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC5-060519 06/05/2019 320-51128-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC5-060519 06/05/2019 320-51128-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC5-060519 06/05/2019 320-51128-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC5-060519 06/05/2019 320-51128-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLPage 101 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC5-060519 06/05/2019 320-51128-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC5-060519 06/05/2019 320-51128-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC5-060519 06/05/2019 320-51128-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC5-060519 06/05/2019 320-51128-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC5-060519 06/05/2019 320-51128-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC5-060519 06/05/2019 320-51128-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLPage 102 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC5-060519 06/05/2019 320-51128-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLASTW-LOC5-060519 06/05/2019 320-51128-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC5-060519 06/05/2019 320-51128-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC5-060519 06/05/2019 320-51128-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC5-060519 06/05/2019 320-51128-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC5-060519 06/05/2019 320-51128-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC5-060519 06/05/2019 320-51128-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC5-060519 06/05/2019 320-51128-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC5-060519 06/05/2019 320-51128-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC5-060519 06/05/2019 320-51128-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLPage 103 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC5-060519 06/05/2019 320-51128-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC5-060519 06/05/2019 320-51128-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 104 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC5-060519-Z 06/05/2019 320-51271-2 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 Hydro-EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 Byproduct 60.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC52-060519 06/05/2019 320-51133-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC52-060519 06/05/2019 320-51133-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC52-060519 06/05/2019 320-51133-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC52-060519 06/05/2019 320-51133-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLPage 105 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC52-060519 06/05/2019 320-51133-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC52-060519 06/05/2019 320-51133-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC52-060519 06/05/2019 320-51133-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC52-060519 06/05/2019 320-51133-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC52-060519 06/05/2019 320-51133-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC52-060519 06/05/2019 320-51133-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC52-060519 06/05/2019 320-51133-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC52-060519 06/05/2019 320-51133-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PES0.0046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0046PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PES0.0046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0046PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PFECA B0.0060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0060PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PFECA B0.0060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0060PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0060PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0060PQLPage 106 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC52-060519-Z 06/05/2019 320-51278-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.011 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.011PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.011 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.011PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 N-methyl perfluoro-1-octanesulfonamide0.0035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0035PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 N-methyl perfluoro-1-octanesulfonamide0.0035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0035PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 N-ethylperfluoro-1-octanesulfonamide0.0037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0037PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 N-ethylperfluoro-1-octanesulfonamide0.0037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0037PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC53-060519 06/05/2019 320-51133-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC53-060519 06/05/2019 320-51133-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC53-060519 06/05/2019 320-51133-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC53-060519 06/05/2019 320-51133-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC53-060519 06/05/2019 320-51133-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC53-060519 06/05/2019 320-51133-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC53-060519 06/05/2019 320-51133-2 NVHOS0.054 UG/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.054PQLPage 107 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPASTW-LOC53-060519 06/05/2019 320-51133-2 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC53-060519 06/05/2019 320-51133-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC53-060519 06/05/2019 320-51133-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC53-060519 06/05/2019 320-51133-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC53-060519 06/05/2019 320-51133-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC53-060519 06/05/2019 320-51133-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC53-060519 06/05/2019 320-51133-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC53-060519 06/05/2019 320-51133-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC53-060519 06/05/2019 320-51133-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC53-060519 06/05/2019 320-51133-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLPage 108 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC53-060519 06/05/2019 320-51133-2 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC53-060519 06/05/2019 320-51133-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC53-060519 06/05/2019 320-51133-2 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC53-060519 06/05/2019 320-51133-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC53-060519 06/05/2019 320-51133-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 109 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC53-060519-Z 06/05/2019 320-51278-2 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519 06/05/2019 320-51133-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC55-060519 06/05/2019 320-51133-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC55-060519 06/05/2019 320-51133-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC55-060519 06/05/2019 320-51133-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLASTW-LOC55-060519 06/05/2019 320-51133-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLASTW-LOC55-060519 06/05/2019 320-51133-3 2-(N-methyl perfluoro-1-0.11 ug/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.11PQLPage 110 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitoctanesulfonamido)-ethanolSOPASTW-LOC55-060519 06/05/2019 320-51133-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLASTW-LOC55-060519 06/05/2019 320-51133-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC55-060519 06/05/2019 320-51133-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLASTW-LOC55-060519 06/05/2019 320-51133-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC55-060519 06/05/2019 320-51133-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLASTW-LOC55-060519 06/05/2019 320-51133-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLASTW-LOC55-060519 06/05/2019 320-51133-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLPage 111 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC55-060519 06/05/2019 320-51133-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC55-060519 06/05/2019 320-51133-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLASTW-LOC55-060519 06/05/2019 320-51133-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC55-060519 06/05/2019 320-51133-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLASTW-LOC55-060519 06/05/2019 320-51133-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC55-060519 06/05/2019 320-51133-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLASTW-LOC55-060519 06/05/2019 320-51133-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC55-060519 06/05/2019 320-51133-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC55-060519 06/05/2019 320-51133-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC55-060519 06/05/2019 320-51133-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PES0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PFECA B0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 2-(N-ethyl perfluoro-1-octanesulfonamido)0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 112 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnit-ethanolASTW-LOC55-060519-Z 06/05/2019 320-51278-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 N-methyl perfluoro-1-octanesulfonamide0.0020 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 N-ethylperfluoro-1-octanesulfonamide0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 EVE Acid0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLTB-1-06051906/05/2019 320-51089-4 Total SuspendedSolids5.0 MG/L5.02540 D-1997UJ5.0MDLTB-10-06051906/05/2019 320-51128-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-10-06051906/05/2019 320-51128-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-10-06051906/05/2019 320-51128-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-10-06051906/05/2019 320-51128-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-10-06051906/05/2019 320-51128-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLPage 113 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-10-06051906/05/2019 320-51128-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLTB-10-06051906/05/2019 320-51128-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-10-06051906/05/2019 320-51128-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-10-06051906/05/2019 320-51128-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-10-06051906/05/2019 320-51128-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-10-06051906/05/2019 320-51128-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLTB-10-06051906/05/2019 320-51128-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLTB-10-06051906/05/2019 320-51128-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-10-06051906/05/2019 320-51128-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-10-06051906/05/2019 320-51128-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-10-06051906/05/2019 320-51128-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-10-06051906/05/2019 320-51128-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-10-06051906/05/2019 320-51128-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-10-06051906/05/2019 320-51128-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-10-06051906/05/2019 320-51128-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLPage 114 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-10-06051906/05/2019 320-51128-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-10-06051906/05/2019 320-51128-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-10-06051906/05/2019 320-51128-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-10-06051906/05/2019 320-51128-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-10-06051906/05/2019 320-51128-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-10-06051906/05/2019 320-51128-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-10-06051906/05/2019 320-51128-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-10-06051906/05/2019 320-51128-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-10-06051906/05/2019 320-51128-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-10-06051906/05/2019 320-51128-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-10-06051906/05/2019 320-51128-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-10-06051906/05/2019 320-51128-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-10-06051906/05/2019 320-51128-4 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-10-06051906/05/2019 320-51128-4 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-10-06051906/05/2019 320-51128-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-10-06051906/05/2019 320-51128-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-10-06051906/05/2019 320-51128-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLPage 115 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-10-06051906/05/2019 320-51128-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-10-06051906/05/2019 320-51128-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-10-06051906/05/2019 320-51128-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-10-06051906/05/2019 320-51128-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-10-06051906/05/2019 320-51128-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-10-06051906/05/2019 320-51128-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-10-06051906/05/2019 320-51128-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-10-06051906/05/2019 320-51128-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLTB-10-06051906/05/2019 320-51128-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLTB-11-06051906/05/2019 320-51133-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-11-06051906/05/2019 320-51133-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-11-06051906/05/2019 320-51133-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-11-06051906/05/2019 320-51133-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-11-06051906/05/2019 320-51133-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLTB-11-06051906/05/2019 320-51133-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLTB-11-06051906/05/2019 320-51133-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-11-06051906/05/2019 320-51133-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 116 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-11-06051906/05/2019 320-51133-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-11-06051906/05/2019 320-51133-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-11-06051906/05/2019 320-51133-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLTB-11-06051906/05/2019 320-51133-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLTB-11-06051906/05/2019 320-51133-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-11-06051906/05/2019 320-51133-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-11-06051906/05/2019 320-51133-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-11-06051906/05/2019 320-51133-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-11-06051906/05/2019 320-51133-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-11-06051906/05/2019 320-51133-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-11-06051906/05/2019 320-51133-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-11-06051906/05/2019 320-51133-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-11-06051906/05/2019 320-51133-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-11-06051906/05/2019 320-51133-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-11-06051906/05/2019 320-51133-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLPage 117 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-11-06051906/05/2019 320-51133-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-11-06051906/05/2019 320-51133-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-11-06051906/05/2019 320-51133-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-11-06051906/05/2019 320-51133-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-11-06051906/05/2019 320-51133-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-11-06051906/05/2019 320-51133-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-11-06051906/05/2019 320-51133-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-11-06051906/05/2019 320-51133-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-11-06051906/05/2019 320-51133-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-11-06051906/05/2019 320-51133-4 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-11-06051906/05/2019 320-51133-4 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-11-06051906/05/2019 320-51133-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-11-06051906/05/2019 320-51133-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-11-06051906/05/2019 320-51133-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-11-06051906/05/2019 320-51133-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-11-06051906/05/2019 320-51133-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-11-06051906/05/2019 320-51133-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLPage 118 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-11-06051906/05/2019 320-51133-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-11-06051906/05/2019 320-51133-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-11-06051906/05/2019 320-51133-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-11-06051906/05/2019 320-51133-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-11-06051906/05/2019 320-51133-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLTB-11-06051906/05/2019 320-51133-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLTB-12-06051906/05/2019 320-51134-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-12-06051906/05/2019 320-51134-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-12-06051906/05/2019 320-51134-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-12-06051906/05/2019 320-51134-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-12-06051906/05/2019 320-51134-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLTB-12-06051906/05/2019 320-51134-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLTB-12-06051906/05/2019 320-51134-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-12-06051906/05/2019 320-51134-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-12-06051906/05/2019 320-51134-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-12-06051906/05/2019 320-51134-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 119 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-12-06051906/05/2019 320-51134-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLTB-12-06051906/05/2019 320-51134-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLTB-12-06051906/05/2019 320-51134-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-12-06051906/05/2019 320-51134-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-12-06051906/05/2019 320-51134-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-12-06051906/05/2019 320-51134-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-12-06051906/05/2019 320-51134-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-12-06051906/05/2019 320-51134-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-12-06051906/05/2019 320-51134-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-12-06051906/05/2019 320-51134-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-12-06051906/05/2019 320-51134-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-12-06051906/05/2019 320-51134-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-12-06051906/05/2019 320-51134-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-12-06051906/05/2019 320-51134-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-12-06051906/05/2019 320-51134-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-12-06051906/05/2019 320-51134-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLPage 120 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-12-06051906/05/2019 320-51134-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-12-06051906/05/2019 320-51134-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-12-06051906/05/2019 320-51134-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-12-06051906/05/2019 320-51134-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-12-06051906/05/2019 320-51134-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-12-06051906/05/2019 320-51134-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-12-06051906/05/2019 320-51134-4 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-12-06051906/05/2019 320-51134-4 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-12-06051906/05/2019 320-51134-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-12-06051906/05/2019 320-51134-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-12-06051906/05/2019 320-51134-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-12-06051906/05/2019 320-51134-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-12-06051906/05/2019 320-51134-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-12-06051906/05/2019 320-51134-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-12-06051906/05/2019 320-51134-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-12-06051906/05/2019 320-51134-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-12-06051906/05/2019 320-51134-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLPage 121 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-12-06051906/05/2019 320-51134-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-12-06051906/05/2019 320-51134-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLTB-12-06051906/05/2019 320-51134-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLTB-13-06051906/05/2019 320-51139-6 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-13-06051906/05/2019 320-51139-6 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-13-06051906/05/2019 320-51139-6 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-13-06051906/05/2019 320-51139-6 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-13-06051906/05/2019 320-51139-6 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLTB-13-06051906/05/2019 320-51139-6 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLTB-13-06051906/05/2019 320-51139-6 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-13-06051906/05/2019 320-51139-6 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-13-06051906/05/2019 320-51139-6 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-13-06051906/05/2019 320-51139-6 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-13-06051906/05/2019 320-51139-6 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLTB-13-06051906/05/2019 320-51139-6 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLPage 122 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-13-06051906/05/2019 320-51139-6 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-13-06051906/05/2019 320-51139-6 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-13-06051906/05/2019 320-51139-6 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-13-06051906/05/2019 320-51139-6 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-13-06051906/05/2019 320-51139-6 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-13-06051906/05/2019 320-51139-6 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-13-06051906/05/2019 320-51139-6 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-13-06051906/05/2019 320-51139-6 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-13-06051906/05/2019 320-51139-6 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-13-06051906/05/2019 320-51139-6 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-13-06051906/05/2019 320-51139-6 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-13-06051906/05/2019 320-51139-6 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-13-06051906/05/2019 320-51139-6 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-13-06051906/05/2019 320-51139-6 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-13-06051906/05/2019 320-51139-6 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-13-06051906/05/2019 320-51139-6 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-13-06051906/05/2019 320-51139-6 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLPage 123 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-13-06051906/05/2019 320-51139-6 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-13-06051906/05/2019 320-51139-6 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-13-06051906/05/2019 320-51139-6 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-13-06051906/05/2019 320-51139-6 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-13-06051906/05/2019 320-51139-6 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-13-06051906/05/2019 320-51139-6 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-13-06051906/05/2019 320-51139-6 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-13-06051906/05/2019 320-51139-6 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-13-06051906/05/2019 320-51139-6 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-13-06051906/05/2019 320-51139-6 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-13-06051906/05/2019 320-51139-6 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-13-06051906/05/2019 320-51139-6 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-13-06051906/05/2019 320-51139-6 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-13-06051906/05/2019 320-51139-6 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-13-06051906/05/2019 320-51139-6 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-13-06051906/05/2019 320-51139-6 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLTB-13-06051906/05/2019 320-51139-6 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLPage 124 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-14-06051906/05/2019 320-51140-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-14-06051906/05/2019 320-51140-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-14-06051906/05/2019 320-51140-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-14-06051906/05/2019 320-51140-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-14-06051906/05/2019 320-51140-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLTB-14-06051906/05/2019 320-51140-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLTB-14-06051906/05/2019 320-51140-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-14-06051906/05/2019 320-51140-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-14-06051906/05/2019 320-51140-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-14-06051906/05/2019 320-51140-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-14-06051906/05/2019 320-51140-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLTB-14-06051906/05/2019 320-51140-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLTB-14-06051906/05/2019 320-51140-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-14-06051906/05/2019 320-51140-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-14-06051906/05/2019 320-51140-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLPage 125 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-14-06051906/05/2019 320-51140-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-14-06051906/05/2019 320-51140-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-14-06051906/05/2019 320-51140-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-14-06051906/05/2019 320-51140-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-14-06051906/05/2019 320-51140-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-14-06051906/05/2019 320-51140-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-14-06051906/05/2019 320-51140-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-14-06051906/05/2019 320-51140-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-14-06051906/05/2019 320-51140-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-14-06051906/05/2019 320-51140-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-14-06051906/05/2019 320-51140-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-14-06051906/05/2019 320-51140-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-14-06051906/05/2019 320-51140-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-14-06051906/05/2019 320-51140-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-14-06051906/05/2019 320-51140-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-14-06051906/05/2019 320-51140-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-14-06051906/05/2019 320-51140-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLPage 126 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-14-06051906/05/2019 320-51140-4 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-14-06051906/05/2019 320-51140-4 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-14-06051906/05/2019 320-51140-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-14-06051906/05/2019 320-51140-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-14-06051906/05/2019 320-51140-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-14-06051906/05/2019 320-51140-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-14-06051906/05/2019 320-51140-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-14-06051906/05/2019 320-51140-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-14-06051906/05/2019 320-51140-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-14-06051906/05/2019 320-51140-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-14-06051906/05/2019 320-51140-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-14-06051906/05/2019 320-51140-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-14-06051906/05/2019 320-51140-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLTB-14-06051906/05/2019 320-51140-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLTB-15-06051906/05/2019 320-51139-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-15-06051906/05/2019 320-51139-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-15-06051906/05/2019 320-51139-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLPage 127 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-15-06051906/05/2019 320-51139-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-15-06051906/05/2019 320-51139-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLTB-15-06051906/05/2019 320-51139-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLTB-15-06051906/05/2019 320-51139-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-15-06051906/05/2019 320-51139-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-15-06051906/05/2019 320-51139-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-15-06051906/05/2019 320-51139-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-15-06051906/05/2019 320-51139-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLTB-15-06051906/05/2019 320-51139-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLTB-15-06051906/05/2019 320-51139-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-15-06051906/05/2019 320-51139-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-15-06051906/05/2019 320-51139-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-15-06051906/05/2019 320-51139-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-15-06051906/05/2019 320-51139-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-15-06051906/05/2019 320-51139-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLPage 128 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-15-06051906/05/2019 320-51139-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-15-06051906/05/2019 320-51139-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-15-06051906/05/2019 320-51139-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-15-06051906/05/2019 320-51139-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-15-06051906/05/2019 320-51139-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-15-06051906/05/2019 320-51139-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-15-06051906/05/2019 320-51139-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-15-06051906/05/2019 320-51139-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-15-06051906/05/2019 320-51139-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-15-06051906/05/2019 320-51139-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-15-06051906/05/2019 320-51139-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-15-06051906/05/2019 320-51139-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-15-06051906/05/2019 320-51139-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-15-06051906/05/2019 320-51139-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-15-06051906/05/2019 320-51139-4 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-15-06051906/05/2019 320-51139-4 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-15-06051906/05/2019 320-51139-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLPage 129 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-15-06051906/05/2019 320-51139-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-15-06051906/05/2019 320-51139-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-15-06051906/05/2019 320-51139-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-15-06051906/05/2019 320-51139-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-15-06051906/05/2019 320-51139-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-15-06051906/05/2019 320-51139-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-15-06051906/05/2019 320-51139-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-15-06051906/05/2019 320-51139-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-15-06051906/05/2019 320-51139-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-15-06051906/05/2019 320-51139-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLTB-15-06051906/05/2019 320-51139-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLTB-3-06051906/05/2019 320-51089-6 Total SuspendedSolids10 MG/L102540 D-1997UJ10MDLTB-4-06051906/05/2019 320-51135-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-4-06051906/05/2019 320-51135-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-4-06051906/05/2019 320-51135-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-4-06051906/05/2019 320-51135-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-4-06051906/05/2019 320-51135-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 130 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-4-06051906/05/2019 320-51135-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-4-06051906/05/2019 320-51135-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-4-06051906/05/2019 320-51135-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-4-06051906/05/2019 320-51135-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLTB-4-06051906/05/2019 320-51135-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLTB-4-06051906/05/2019 320-51135-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-4-06051906/05/2019 320-51135-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-4-06051906/05/2019 320-51135-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-4-06051906/05/2019 320-51135-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-4-06051906/05/2019 320-51135-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-4-06051906/05/2019 320-51135-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-4-06051906/05/2019 320-51135-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-4-06051906/05/2019 320-51135-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-4-06051906/05/2019 320-51135-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-4-06051906/05/2019 320-51135-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLPage 131 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-4-06051906/05/2019 320-51135-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-4-06051906/05/2019 320-51135-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-4-06051906/05/2019 320-51135-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-4-06051906/05/2019 320-51135-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-4-06051906/05/2019 320-51135-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-4-06051906/05/2019 320-51135-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-4-06051906/05/2019 320-51135-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-4-06051906/05/2019 320-51135-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-4-06051906/05/2019 320-51135-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-4-06051906/05/2019 320-51135-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-4-06051906/05/2019 320-51135-4 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-4-06051906/05/2019 320-51135-4 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-4-06051906/05/2019 320-51135-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-4-06051906/05/2019 320-51135-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-4-06051906/05/2019 320-51135-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-4-06051906/05/2019 320-51135-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-4-06051906/05/2019 320-51135-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLPage 132 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-4-06051906/05/2019 320-51135-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-4-06051906/05/2019 320-51135-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-4-06051906/05/2019 320-51135-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-4-06051906/05/2019 320-51135-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-4-06051906/05/2019 320-51135-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-4-06051906/05/2019 320-51135-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLTB-4-06051906/05/2019 320-51135-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLTB-5-06051906/05/2019 320-51141-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-5-06051906/05/2019 320-51141-3 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-5-06051906/05/2019 320-51141-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-5-06051906/05/2019 320-51141-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-5-06051906/05/2019 320-51141-3 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLTB-5-06051906/05/2019 320-51141-3 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLTB-5-06051906/05/2019 320-51141-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-5-06051906/05/2019 320-51141-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-5-06051906/05/2019 320-51141-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 133 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-5-06051906/05/2019 320-51141-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-5-06051906/05/2019 320-51141-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLTB-5-06051906/05/2019 320-51141-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLTB-5-06051906/05/2019 320-51141-3 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-5-06051906/05/2019 320-51141-3 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-5-06051906/05/2019 320-51141-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-5-06051906/05/2019 320-51141-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-5-06051906/05/2019 320-51141-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-5-06051906/05/2019 320-51141-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-5-06051906/05/2019 320-51141-3 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-5-06051906/05/2019 320-51141-3 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-5-06051906/05/2019 320-51141-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-5-06051906/05/2019 320-51141-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-5-06051906/05/2019 320-51141-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-5-06051906/05/2019 320-51141-3 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-5-06051906/05/2019 320-51141-3 PFO5DA0.034 ug/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.034PQLPage 134 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPTB-5-06051906/05/2019 320-51141-3 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-5-06051906/05/2019 320-51141-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-5-06051906/05/2019 320-51141-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-5-06051906/05/2019 320-51141-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-5-06051906/05/2019 320-51141-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-5-06051906/05/2019 320-51141-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-5-06051906/05/2019 320-51141-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-5-06051906/05/2019 320-51141-3 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-5-06051906/05/2019 320-51141-3 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-5-06051906/05/2019 320-51141-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-5-06051906/05/2019 320-51141-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-5-06051906/05/2019 320-51141-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-5-06051906/05/2019 320-51141-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-5-06051906/05/2019 320-51141-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-5-06051906/05/2019 320-51141-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-5-06051906/05/2019 320-51141-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLPage 135 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-5-06051906/05/2019 320-51141-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-5-06051906/05/2019 320-51141-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-5-06051906/05/2019 320-51141-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-5-06051906/05/2019 320-51141-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLTB-5-06051906/05/2019 320-51141-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLTB-7-06051906/05/2019 320-51141-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-7-06051906/05/2019 320-51141-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-7-06051906/05/2019 320-51141-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-7-06051906/05/2019 320-51141-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-7-06051906/05/2019 320-51141-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLTB-7-06051906/05/2019 320-51141-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLTB-7-06051906/05/2019 320-51141-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-7-06051906/05/2019 320-51141-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-7-06051906/05/2019 320-51141-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-7-06051906/05/2019 320-51141-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-7-06051906/05/2019 320-51141-4 2-(N-methyl perfluoro-1-octanesulfonamido)0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLPage 136 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnit-ethanolTB-7-06051906/05/2019 320-51141-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLTB-7-06051906/05/2019 320-51141-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-7-06051906/05/2019 320-51141-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-7-06051906/05/2019 320-51141-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-7-06051906/05/2019 320-51141-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-7-06051906/05/2019 320-51141-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-7-06051906/05/2019 320-51141-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-7-06051906/05/2019 320-51141-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-7-06051906/05/2019 320-51141-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-7-06051906/05/2019 320-51141-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-7-06051906/05/2019 320-51141-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-7-06051906/05/2019 320-51141-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-7-06051906/05/2019 320-51141-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-7-06051906/05/2019 320-51141-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-7-06051906/05/2019 320-51141-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-7-06051906/05/2019 320-51141-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.037PQLPage 137 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPTB-7-06051906/05/2019 320-51141-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-7-06051906/05/2019 320-51141-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-7-06051906/05/2019 320-51141-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-7-06051906/05/2019 320-51141-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-7-06051906/05/2019 320-51141-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-7-06051906/05/2019 320-51141-4 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-7-06051906/05/2019 320-51141-4 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-7-06051906/05/2019 320-51141-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-7-06051906/05/2019 320-51141-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-7-06051906/05/2019 320-51141-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-7-06051906/05/2019 320-51141-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-7-06051906/05/2019 320-51141-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-7-06051906/05/2019 320-51141-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-7-06051906/05/2019 320-51141-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-7-06051906/05/2019 320-51141-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-7-06051906/05/2019 320-51141-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLPage 138 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-7-06051906/05/2019 320-51141-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-7-06051906/05/2019 320-51141-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLTB-7-06051906/05/2019 320-51141-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLTB-8-06051906/05/2019 320-51141-5 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-8-06051906/05/2019 320-51141-5 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-8-06051906/05/2019 320-51141-5 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-8-06051906/05/2019 320-51141-5 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-8-06051906/05/2019 320-51141-5 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLTB-8-06051906/05/2019 320-51141-5 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLTB-8-06051906/05/2019 320-51141-5 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-8-06051906/05/2019 320-51141-5 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-8-06051906/05/2019 320-51141-5 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-8-06051906/05/2019 320-51141-5 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-8-06051906/05/2019 320-51141-5 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLTB-8-06051906/05/2019 320-51141-5 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLPage 139 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-8-06051906/05/2019 320-51141-5 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-8-06051906/05/2019 320-51141-5 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-8-06051906/05/2019 320-51141-5 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-8-06051906/05/2019 320-51141-5 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-8-06051906/05/2019 320-51141-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-8-06051906/05/2019 320-51141-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-8-06051906/05/2019 320-51141-5 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-8-06051906/05/2019 320-51141-5 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-8-06051906/05/2019 320-51141-5 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-8-06051906/05/2019 320-51141-5 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-8-06051906/05/2019 320-51141-5 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-8-06051906/05/2019 320-51141-5 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-8-06051906/05/2019 320-51141-5 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-8-06051906/05/2019 320-51141-5 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-8-06051906/05/2019 320-51141-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-8-06051906/05/2019 320-51141-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-8-06051906/05/2019 320-51141-5 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLPage 140 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-8-06051906/05/2019 320-51141-5 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-8-06051906/05/2019 320-51141-5 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-8-06051906/05/2019 320-51141-5 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-8-06051906/05/2019 320-51141-5 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-8-06051906/05/2019 320-51141-5 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-8-06051906/05/2019 320-51141-5 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-8-06051906/05/2019 320-51141-5 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-8-06051906/05/2019 320-51141-5 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-8-06051906/05/2019 320-51141-5 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-8-06051906/05/2019 320-51141-5 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-8-06051906/05/2019 320-51141-5 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-8-06051906/05/2019 320-51141-5 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-8-06051906/05/2019 320-51141-5 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-8-06051906/05/2019 320-51141-5 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-8-06051906/05/2019 320-51141-5 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-8-06051906/05/2019 320-51141-5 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLTB-8-06051906/05/2019 320-51141-5 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLPage 141 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-9-06051906/05/2019 320-51136-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-9-06051906/05/2019 320-51136-4 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLTB-9-06051906/05/2019 320-51136-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-9-06051906/05/2019 320-51136-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLTB-9-06051906/05/2019 320-51136-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLTB-9-06051906/05/2019 320-51136-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLTB-9-06051906/05/2019 320-51136-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-9-06051906/05/2019 320-51136-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-9-06051906/05/2019 320-51136-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-9-06051906/05/2019 320-51136-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLTB-9-06051906/05/2019 320-51136-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLTB-9-06051906/05/2019 320-51136-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLTB-9-06051906/05/2019 320-51136-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-9-06051906/05/2019 320-51136-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLTB-9-06051906/05/2019 320-51136-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLPage 142 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-9-06051906/05/2019 320-51136-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLTB-9-06051906/05/2019 320-51136-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-9-06051906/05/2019 320-51136-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLTB-9-06051906/05/2019 320-51136-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-9-06051906/05/2019 320-51136-4 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLTB-9-06051906/05/2019 320-51136-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-9-06051906/05/2019 320-51136-4 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-9-06051906/05/2019 320-51136-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-9-06051906/05/2019 320-51136-4 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLTB-9-06051906/05/2019 320-51136-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-9-06051906/05/2019 320-51136-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLTB-9-06051906/05/2019 320-51136-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-9-06051906/05/2019 320-51136-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLTB-9-06051906/05/2019 320-51136-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-9-06051906/05/2019 320-51136-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLTB-9-06051906/05/2019 320-51136-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLTB-9-06051906/05/2019 320-51136-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLPage 143 of 223
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitTB-9-06051906/05/2019 320-51136-4 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-9-06051906/05/2019 320-51136-4 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLTB-9-06051906/05/2019 320-51136-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-9-06051906/05/2019 320-51136-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLTB-9-06051906/05/2019 320-51136-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-9-06051906/05/2019 320-51136-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLTB-9-06051906/05/2019 320-51136-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-9-06051906/05/2019 320-51136-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLTB-9-06051906/05/2019 320-51136-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-9-06051906/05/2019 320-51136-4 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLTB-9-06051906/05/2019 320-51136-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-9-06051906/05/2019 320-51136-4 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLTB-9-06051906/05/2019 320-51136-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLTB-9-06051906/05/2019 320-51136-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 144 of 223
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit. The actual detection limits may behigher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC3-060519 06/05/2019 320-51128-1 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC31-060519-Z 06/05/2019 320-51220-2 Perfluorooctadecanoicacid0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLASTW-LOC31-060519 06/05/2019 320-51215-2 Perfluorododecanesulfonic acid (PFDoS)0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 Perfluorooctadecanoicacid0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 Perfluorooctadecanoicacid0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLASTW-LOC36-060519 06/05/2019 320-51139-1 Perfluorooctadecanoicacid0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 145 of 223
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit. The actual detection limits may behigher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PFECA-G0.0020 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.0020PQLPage 146 of 223
Associated MS and/or MSD analysis had relative percent recovery (RPR) values higher than the upper control limit. The reported result may be biasedhigh.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 R-EVE0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 R-EVE0.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 Byproduct 40.17 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 Byproduct 50.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 Byproduct 50.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 Byproduct 50.050 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 Byproduct 50.053 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC31-060519 06/05/2019 320-51215-2 Hfpo Dimer Acid0.054 UG/L537 ModifiedJ3535_PFC0.0040PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 R-EVE0.0090 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 R-EVE0.0083 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 Byproduct 40.040 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 Byproduct 40.038 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 Byproduct 50.015 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 Byproduct 50.015 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PFO3OA0.17 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PFO3OA0.17 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 147 of 223
High relative percent difference (RPD) observed between field duplicate and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 R-EVE0.065 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 R-EVE0.064 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 Byproduct 40.29 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 Byproduct 40.29 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 Byproduct 50.54 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 Byproduct 50.54 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PFMOAA0.096 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PFMOAA0.094 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PFESA-BP20.052 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PFESA-BP20.052 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 Hydro-EVE Acid0.015 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 Hydro-EVE Acid0.015 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 Perfluorobutanoic Acid0.02 UG/L537 ModifiedJ3535_PFC0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PFO2HxA0.23 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PFO2HxA0.24 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PFO3OA0.065 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PFO3OA0.064 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 148 of 223
High relative percent difference (RPD) observed between field duplicate and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PFO4DA0.040 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PFO4DA0.041 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PFO5DA0.11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PFO5DA0.12 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PerfluoropentanoicAcid0.14 UG/L537 ModifiedJ3535_PFC0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PFESA-BP10.016 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PFESA-BP10.015 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 Hfpo Dimer Acid0.39 UG/L537 ModifiedJ3535_PFC0.0040PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 NVHOS0.019 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 NVHOS0.019 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 R-EVE0.020 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 R-EVE0.021 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 Byproduct 40.099 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 Byproduct 40.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 Byproduct 50.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 Byproduct 50.13 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PFESA-BP20.023 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 149 of 223
High relative percent difference (RPD) observed between field duplicate and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PFESA-BP20.024 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 Hydro-EVE Acid0.0044 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 Hydro-EVE Acid0.0045 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PFMOAA0.038 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PFMOAA0.038 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 Perfluorobutanoic Acid0.011 UG/L537 ModifiedJ3535_PFC0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PFO2HxA0.072 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PFO2HxA0.076 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PFO3OA0.017 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PFO3OA0.017 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PFO4DA0.016 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PFO4DA0.016 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PFO5DA0.039 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PFO5DA0.041 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PerfluoropentanoicAcid0.054 UG/L537 ModifiedJ3535_PFC0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PFESA-BP10.0042 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PFESA-BP10.0044 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 150 of 223
High relative percent difference (RPD) observed between field duplicate and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC36-060519-Z 06/05/2019 320-51251-1 Hfpo Dimer Acid0.28 UG/L537 ModifiedJ3535_PFC0.0040PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 NVHOS0.0074 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 NVHOS0.008 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 Total SuspendedSolids80 MG/L5.02540 D-1997J5.0MDLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PerfluoropentanoicAcid0.084 UG/L537 ModifiedJ3535_PFC0.0020PQLASTW-LOC36-060519 06/05/2019 320-51139-1 Total SuspendedSolids23 MG/L5.02540 D-1997J5.0MDLASTW-LOC36-060519 06/05/2019 320-51139-1 PerfluoropentanoicAcid0.061 UG/L537 ModifiedJ3535_PFC0.0020PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 Byproduct 50.66 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 Byproduct 50.67 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PFESA-BP21.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PFESA-BP21.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PFMOAA10 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PFMOAA10.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PFO2HxA2.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PFO2HxA2.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PFO3OA1.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PFO3OA1.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PFO4DA0.88 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLPage 151 of 223
High relative percent difference (RPD) observed between field duplicate and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PFO4DA0.86 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PFO5DA0.56 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PFO5DA0.57 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PEPA0.081 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PEPA0.089 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PFESA-BP10.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PFESA-BP10.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 PerfluoroundecanoicAcid0.0043 UG/L537 ModifiedJ3535_PFC0.0020PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 Hfpo Dimer Acid0.1 UG/L537 ModifiedJ3535_PFC0.0040PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 NVHOS0.37 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 NVHOS0.36 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 Byproduct 50.33 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 Byproduct 50.34 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PFESA-BP20.22 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PFESA-BP20.22 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PFMOAA0.38 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PFMOAA0.35 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLPage 152 of 223
High relative percent difference (RPD) observed between field duplicate and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PFO5DA0.10 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PFO5DA0.11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PFO2HxA0.13 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PFO2HxA0.14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PEPA0.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PEPA0.16 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PFESA-BP10.038 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PFESA-BP10.039 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PerfluoroundecanoicAcid0.0066 UG/L537 ModifiedJ3535_PFC0.0020PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 Hfpo Dimer Acid0.15 UG/L537 ModifiedJ3535_PFC0.0040PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 Byproduct 50.62 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 Byproduct 50.63 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PFESA-BP21.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PFESA-BP21.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PFMOAA12 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PFMOAA12.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PFO2HxA2.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLPage 153 of 223
High relative percent difference (RPD) observed between field duplicate and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PFO2HxA2.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PFO3OA1.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PFO3OA1.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PFO4DA1.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PFO4DA1.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PFO5DA0.70 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PFO5DA0.69 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PFESA-BP10.087 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PFESA-BP10.086 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 Hfpo Dimer Acid0.12 UG/L537 ModifiedJ3535_PFC0.0040PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 NVHOS0.38 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 NVHOS0.37 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 Byproduct 50.38 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 Byproduct 50.39 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PFESA-BP20.23 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PFESA-BP20.24 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PFO5DA0.095 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLPage 154 of 223
High relative percent difference (RPD) observed between field duplicate and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC35-1-060519 06/05/2019 320-51089-3 PFO5DA0.098 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PFO2HxA0.18 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PFO2HxA0.18 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PFO3OA0.065 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PEPA0.14 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PEPA0.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 Hfpo Dimer Acid0.2 UG/L537 ModifiedJ3535_PFC0.0040PQLASTW-LOC31-060519 06/05/2019 320-51215-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.037PQLASTW-LOC31-060519 06/05/2019 320-51215-2 N-ethylperfluoro-1-octanesulfonamide0.17 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.037PQLPage 155 of 223
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PFESA-BP20.018 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PFESA-BP20.018 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 Hydro-EVE Acid0.0022 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 Hydro-EVE Acid0.0022 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 Byproduct 50.41 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 Byproduct 50.44 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PFMOAA0.034 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PFMOAA0.036 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PFESA-BP10.025 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PFESA-BP10.026 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 NVHOS0.0069 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 NVHOS0.0073 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 R-EVE0.011 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 R-EVE0.011 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 Byproduct 40.085 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 Byproduct 40.081 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 Byproduct 50.27 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 156 of 223
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC40-060519-Z 06/05/2019 320-51276-2 Byproduct 50.26 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PFMOAA0.032 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PFMOAA0.031 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PFESA-BP10.019 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PFESA-BP10.017 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 NVHOS0.0063 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 NVHOS0.0063 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 R-EVE0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 R-EVE0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 Byproduct 40.27 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 Byproduct 40.27 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 Byproduct 50.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 Byproduct 50.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PFMOAA0.048 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PFMOAA0.048 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 EVE Acid0.0037 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 EVE Acid0.0037 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 157 of 223
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 Hydro-EVE Acid0.0093 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 Hydro-EVE Acid0.0092 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PFESA-BP10.034 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PFESA-BP10.031 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 NVHOS0.013 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 NVHOS0.013 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 R-EVE0.21 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0035PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 R-EVE0.22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0035PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 Byproduct 40.77 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0079PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 Byproduct 40.82 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0079PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 Byproduct 50.16 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0029PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 Byproduct 50.17 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0029PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PFMOAA0.22 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.011PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PFMOAA0.23 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.011PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 EVE Acid0.0094 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 EVE Acid0.0096 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PFESA-BP20.065 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 158 of 223
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PFESA-BP20.065 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 Hydro-EVE Acid0.011 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 Hydro-EVE Acid0.011 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PFO5DA0.016 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PFO5DA0.016 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PFESA-BP10.28 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PFESA-BP10.27 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 NVHOS0.056 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0027PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 NVHOS0.056 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0027PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PFESA-BP20.026 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PFESA-BP20.026 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 Hydro-EVE Acid0.0053 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 Hydro-EVE Acid0.0052 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 R-EVE0.055 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 R-EVE0.052 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 Byproduct 40.34 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 Byproduct 40.32 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 159 of 223
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC37-060519-Z 06/05/2019 320-51251-2 Byproduct 50.053 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 Byproduct 50.052 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PFMOAA0.18 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PFMOAA0.18 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PFO5DA0.064 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PFO5DA0.066 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PFESA-BP10.022 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PFESA-BP10.022 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 NVHOS0.0076 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 NVHOS0.0075 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 Byproduct 60.0022 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 Byproduct 60.0022 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 EVE Acid0.0035 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 EVE Acid0.0034 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PFESA-BP20.0040 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PFESA-BP20.0038 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PFESA-BP20.55 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLPage 160 of 223
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PFESA-BP20.51 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 Hydro-EVE Acid0.080 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 Hydro-EVE Acid0.077 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PFMOAA2.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PFMOAA2.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PFO5DA0.39 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PFO5DA0.38 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PFESA-BP10.66 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PFESA-BP10.64 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 NVHOS0.31 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 NVHOS0.32 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PFO5DA0.0086 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PFO5DA0.0092 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PFESA-BP10.023 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PFESA-BP10.023 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 NVHOS0.0089 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 NVHOS0.0089 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 161 of 223
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC10-060519-Z 06/05/2019 320-51271-3 R-EVE0.33 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 R-EVE0.32 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 Byproduct 40.98 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 Byproduct 40.95 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 Byproduct 50.64 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 Byproduct 50.64 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 Byproduct 60.029 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 Byproduct 60.029 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 R-EVE0.095 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 R-EVE0.091 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 Byproduct 40.19 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 Byproduct 40.19 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 Byproduct 50.17 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 Byproduct 50.17 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PFMOAA0.032 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PFMOAA0.032 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 R-EVE0.013 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 162 of 223
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC3-060519-Z 06/05/2019 320-51271-1 R-EVE0.013 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 Byproduct 40.039 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 Byproduct 40.038 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 Byproduct 50.0091 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 Byproduct 50.0089 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PFMOAA0.028 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PFMOAA0.029 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PFO5DA0.0037 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PFO5DA0.0029 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 NVHOS0.0032 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 NVHOS0.0032 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PFO4DA0.0025 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PFO4DA0.0026 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 R-EVE0.020 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 R-EVE0.019 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 Byproduct 40.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 Byproduct 40.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 163 of 223
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC27-060519-Z 06/05/2019 320-51274-2 Byproduct 50.028 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 Byproduct 50.029 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 NVHOS0.0048 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 NVHOS0.005 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 R-EVE0.0031 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 R-EVE0.0027 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 Byproduct 50.0041 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 Byproduct 50.0038 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PFESA-BP20.017 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PFESA-BP20.016 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 Hydro-EVE Acid0.0024 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 Hydro-EVE Acid0.0024 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PFESA-BP10.0027 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PFESA-BP10.0026 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PFESA-BP20.0058 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PFESA-BP20.0059 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PFMOAA0.040 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLPage 164 of 223
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PFMOAA0.04 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PFO5DA0.0062 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PFO5DA0.0062 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PFESA-BP10.0028 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PFESA-BP10.003 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 R-EVE0.076 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 R-EVE0.081 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 Byproduct 40.21 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 Byproduct 40.22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 Byproduct 50.037 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 Byproduct 50.038 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 Byproduct 60.0026 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 Byproduct 60.0025 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PFESA-BP20.076 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PFESA-BP20.075 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 Hydro-EVE Acid0.0087 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 Hydro-EVE Acid0.0088 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 165 of 223
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PFMOAA0.028 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PFMOAA0.026 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PFO5DA0.092 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PFO5DA0.086 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PFESA-BP10.013 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PFESA-BP10.013 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 NVHOS0.0068 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 NVHOS0.0069 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PFESA-BP20.064 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PFESA-BP20.066 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 Hydro-EVE Acid0.0025 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 Hydro-EVE Acid0.0025 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 R-EVE0.083 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 R-EVE0.081 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 Byproduct 40.76 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 Byproduct 40.75 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 Byproduct 50.077 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 166 of 223
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC53-060519-Z 06/05/2019 320-51278-2 Byproduct 50.077 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 Byproduct 60.0044 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 Byproduct 60.0045 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PFMOAA0.63 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PFMOAA0.64 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PFESA-BP10.016 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PFESA-BP10.017 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 NVHOS0.026 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 NVHOS0.026 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PFMOAA1.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.021PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PFMOAA1.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.021PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 EVE Acid0.016 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0024PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 EVE Acid0.015 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0024PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PFESA-BP20.60 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0030PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PFESA-BP20.59 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0030PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 Hydro-EVE Acid0.069 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0028PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 Hydro-EVE Acid0.067 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0028PQLPage 167 of 223
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PFECA-G0.0041 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0041PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PFECA-G0.0041 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0041PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 R-EVE0.45 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0070PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 R-EVE0.43 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0070PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 Byproduct 42.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.016PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 Byproduct 42.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.016PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 Byproduct 51.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0058PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 Byproduct 50.99 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0058PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 Byproduct 60.014 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 Byproduct 60.014 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PFO5DA0.13 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0034PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PFO5DA0.13 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0034PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PFESA-BP10.58 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0027PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PFESA-BP10.54 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0027PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 NVHOS0.33 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0054PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 NVHOS0.33 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0054PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 R-EVE0.011 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 168 of 223
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC5-060519-Z 06/05/2019 320-51271-2 R-EVE0.011 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 Byproduct 40.10 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 Byproduct 40.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 Byproduct 50.024 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 Byproduct 50.025 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PFESA-BP20.0042 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PFESA-BP20.0041 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PFMOAA0.0074 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PFMOAA0.0074 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PFO5DA0.0046 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PFO5DA0.0041 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PFESA-BP10.0091 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PFESA-BP10.009 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 NVHOS0.0025 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 NVHOS0.0026 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 R-EVE0.32 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 R-EVE0.33 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLPage 169 of 223
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC43-060519-Z 06/05/2019 320-51243-2 Byproduct 40.94 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 Byproduct 40.93 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 Byproduct 51.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 Byproduct 51.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 Byproduct 60.038 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 Byproduct 60.038 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PFMOAA30 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PFMOAA31.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 EVE Acid0.035 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 EVE Acid0.037 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PFESA-BP20.80 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PFESA-BP20.81 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 Hydro-EVE Acid0.21 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 Hydro-EVE Acid0.21 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PFESA-BP11.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PFESA-BP11.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 NVHOS0.50 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLPage 170 of 223
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC43-060519-Z 06/05/2019 320-51243-2 NVHOS0.51 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 R-EVE1.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 R-EVE1.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 Byproduct 43.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 Byproduct 43.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 Byproduct 51.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 Byproduct 51.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 Byproduct 60.41 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 Byproduct 60.41 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PFMOAA108 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PFMOAA110.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 EVE Acid0.071 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 EVE Acid0.075 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PFESA-BP26.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PFESA-BP26.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 Hydro-EVE Acid1.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 Hydro-EVE Acid1.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLPage 171 of 223
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PFESA-BP11.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PFESA-BP11.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 NVHOS4.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 NVHOS4.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLPage 172 of 223
Only one surrogate has relative percent recovery (RPR) values outside control limits and the parameter is a PFC (Detects).LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC34-060519 06/05/2019 320-51089-2 PerfluorotetradecanoicAcid0.0039 UG/L537 ModifiedJ3535_PFC0.0020PQLASTW-LOC27-060519 06/05/2019 320-51135-2 10:2 Fluorotelomersulfonate0.009 ug/L537 ModifiedJ3535_PFC0.0020PQLPage 173 of 223
Quality review criteria exceeded between the REP (laboratory replicate) and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC41-060519-Z 06/05/2019 320-51276-3 R-EVE0.012 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 R-EVE0.014 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 Byproduct 40.095 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 Byproduct 40.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PFO5DA0.012 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PFO5DA0.01 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PFESA-BP20.015 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PFESA-BP20.012 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PFO4DA0.0086 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PFO4DA0.0069 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PFO5DA0.011 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PFO5DA0.0092 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519 06/05/2019 320-51134-2 Byproduct 50.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC40-060519 06/05/2019 320-51134-2 Byproduct 50.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PFESA-BP20.029 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PFESA-BP20.025 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PFO5DA0.017 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 174 of 223
Quality review criteria exceeded between the REP (laboratory replicate) and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PFO5DA0.015 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PFO4DA0.017 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0039PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PFO4DA0.014 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0039PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 Total SuspendedSolids22 MG/L5.02540 D-1997J5.0MDLASTW-LOC37-060519 06/05/2019 320-51139-2 Total SuspendedSolids63 MG/L102540 D-1997J10MDLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 Perfluorobutanoic Acid(trial)0.0066 UG/L537 ModifiedJ3535_PFC0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PerfluoropentanoicAcid (trial)0.021 UG/L537 ModifiedJ3535_PFC0.0020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 Hfpo Dimer Acid (trial)0.19 UG/L537 ModifiedJ3535_PFC0.0040PQLASTW-LOC36-060519 06/05/2019 320-51139-1 Perfluorobutanoic Acid(trial)0.0075 UG/L537 ModifiedJ3535_PFC0.0020PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PerfluoropentanoicAcid (trial)0.027 UG/L537 ModifiedJ3535_PFC0.0020PQLASTW-LOC36-060519 06/05/2019 320-51139-1 Hfpo Dimer Acid (trial)0.19 UG/L537 ModifiedJ3535_PFC0.0040PQLASTW-LOC36-060519 06/05/2019 320-51139-1 Perfluorobutanoic Acid0.013 UG/L537 ModifiedJ3535_PFC0.0020PQLASTW-LOC36-060519 06/05/2019 320-51139-1 Hfpo Dimer Acid0.31 UG/L537 ModifiedJ3535_PFC0.0040PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PFESA-BP10.083 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PFESA-BP10.068 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 PerfluoroundecanoicAcid (trial)0.0066 UG/L537 ModifiedJ3535_PFC0.0020PQLASTW-LOC35-1-060519-Z06/05/2019 320-51232-3 Hfpo Dimer Acid (trial)0.15 UG/L537 ModifiedJ3535_PFC0.0040PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PerfluoroundecanoicAcid (trial)0.0063 UG/L537 ModifiedJ3535_PFC0.0020PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 Hfpo Dimer Acid (trial)0.2 UG/L537 ModifiedJ3535_PFC0.0040PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 PerfluoroundecanoicAcid0.0063 UG/L537 ModifiedJ3535_PFC0.0020PQLASTW-LOC34-060519 06/05/2019 320-51089-2 PFO5DA0.80 ug/LCl. Spec. Table 3CompoundJPFAS_DI_Prep0.034PQLPage 175 of 223
Quality review criteria exceeded between the REP (laboratory replicate) and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPASTW-LOC34-060519 06/05/2019 320-51089-2 PFO5DA0.96 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC30-060519 06/05/2019 320-51215-1 Total SuspendedSolids28 MG/L5.02540 D-1997J5.0MDLASTW-LOC30-060519 06/05/2019 320-51215-1 PEPA0.21 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PEPA0.23 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC32-060519 06/05/2019 320-51215-5 Total SuspendedSolids300 MG/L102540 D-1997J10MDLASTW-LOC32-060519 06/05/2019 320-51215-5 PFO5DA0.18 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PFO5DA0.23 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC31-060519 06/05/2019 320-51215-2 Total SuspendedSolids6.8 MG/L5.02540 D-1997J5.0MDLASTW-LOC10-060519 06/05/2019 320-51128-3 PFO5DA0.42 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PFO5DA0.37 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 Byproduct 40.0089 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 Byproduct 40.0077 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PFO5DA0.17 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PFO5DA0.11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PFO5DA0.025 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PFO5DA0.03 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PFO4DA0.25 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLPage 176 of 223
Quality review criteria exceeded between the REP (laboratory replicate) and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC52-060519 06/05/2019 320-51133-1 PFO4DA0.31 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PFO4DA4.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PFO4DA4.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PFO5DA2.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PFO5DA3.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PFESA-BP20.91 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PFESA-BP20.74 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PFO5DA3.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PFO5DA2.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PFO5DA5.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PFO5DA3.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLPage 177 of 223
The analysis hold time for this sample was exceeded by a factor of 2. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC42-2-060519 06/05/2019 320-51141-1 Total SuspendedSolids10 MG/L5.02540 D-1997J5.0MDLPage 178 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC35-2-060519 06/05/2019 320-51136-1 Total SuspendedSolids16 MG/L5.02540 D-1997J5.0MDLASTW-LOC42-1-060519 06/05/2019 320-51140-1 NVHOS4.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 NVHOS4.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PMPA0.37 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PMPA0.39 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PFO2HxA0.056 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PFO2HxA0.057 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PFO3OA0.011 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PFO3OA0.012 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PFO4DA0.0071 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PFO4DA0.0078 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PEPA0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC41-060519-Z 06/05/2019 320-51276-3 PEPA0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC41-060519 06/05/2019 320-51134-3 Byproduct 50.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC41-060519 06/05/2019 320-51134-3 Byproduct 50.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PFO2HxA0.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLPage 179 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC41-060519 06/05/2019 320-51134-3 Total SuspendedSolids6.8 MG/L5.02540 D-1997J5.0MDLASTW-LOC41-060519 06/05/2019 320-51134-3 PEPA0.14 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PEPA0.14 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PMPA0.90 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC41-060519 06/05/2019 320-51134-3 PMPA0.93 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PMPA0.35 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PMPA0.35 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PFO2HxA0.051 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PFO2HxA0.048 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PFO3OA0.0090 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PFO3OA0.0086 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PEPA0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC40-060519-Z 06/05/2019 320-51276-2 PEPA0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PFO2HxA0.087 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PEPA0.13 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PEPA0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLPage 180 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC40-060519 06/05/2019 320-51134-2 PMPA0.73 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC40-060519 06/05/2019 320-51134-2 PMPA0.72 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PFMOAA0.066 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PFMOAA0.065 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 EVE Acid0.0052 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 EVE Acid0.0051 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PFESA-BP20.044 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PFESA-BP20.043 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 Hydro-EVE Acid0.012 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 Hydro-EVE Acid0.011 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PFO2HxA0.10 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PFO2HxA0.098 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PFO3OA0.030 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PFO3OA0.029 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PFO4DA0.016 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PFO4DA0.015 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PFO5DA0.019 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 181 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PFO5DA0.017 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PEPA0.59 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PEPA0.58 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PFESA-BP10.048 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PFESA-BP10.046 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PMPA1.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 PMPA1.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 Total SuspendedSolids20 MG/L5.02540 D-1997J5.0MDLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 NVHOS0.017 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519-Z06/05/2019 320-51241-3 NVHOS0.016 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PFESA-BP20.049 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PFESA-BP20.047 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PFO5DA0.042 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PFO5DA0.045 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PFO2HxA0.13 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PFO2HxA0.12 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PEPA0.72 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLPage 182 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC39-2-060519 06/05/2019 320-51136-3 PEPA0.74 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PFESA-BP10.045 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PFESA-BP10.042 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PMPA1.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC39-2-060519 06/05/2019 320-51136-3 PMPA1.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PFO2HxA0.074 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PFO2HxA0.074 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PFO3OA0.020 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PFO3OA0.019 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PFO4DA0.016 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PFO4DA0.015 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PEPA0.43 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PEPA0.44 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PMPA1.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC39-1-060519-Z06/05/2019 320-51276-1 PMPA1.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 Total SuspendedSolids160 MG/L252540 D-1997J25MDLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PFESA-BP20.044 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLPage 183 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC39-1-060519 06/05/2019 320-51134-1 PFESA-BP20.041 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PFO2HxA0.10 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PFO2HxA0.097 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PMPA1.00 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PMPA1.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PEPA0.50 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PEPA0.53 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PFESA-BP10.041 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PFESA-BP10.046 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PMPA1.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC39-1-060519 06/05/2019 320-51134-1 PMPA1.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 R-EVE0.026 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 R-EVE0.028 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 Byproduct 40.069 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 Byproduct 40.07 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PFMOAA0.084 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PFMOAA0.084 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLPage 184 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 EVE Acid0.0098 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 EVE Acid0.01 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PFESA-BP20.032 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PFESA-BP20.032 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 Hydro-EVE Acid0.0065 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 Hydro-EVE Acid0.0067 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PFO2HxA0.100 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PFO2HxA0.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PFO3OA0.019 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PFO3OA0.02 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PFO4DA0.012 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PFO4DA0.013 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PFO5DA0.020 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PFO5DA0.021 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PEPA0.37 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PEPA0.38 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PFESA-BP10.096 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 185 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 PFESA-BP10.099 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 NVHOS0.0093 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519-Z06/05/2019 320-51241-2 NVHOS0.0094 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 Total SuspendedSolids20 MG/L5.02540 D-1997J5.0MDLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PFO5DA0.053 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PFO5DA0.051 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PFESA-BP20.049 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PFESA-BP20.044 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PFO2HxA0.16 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PFO2HxA0.14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PMPA2.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PMPA2.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PFECA B0.011 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0030PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PFECA B0.011 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0030PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PEPA0.52 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PEPA0.49 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PFESA-BP10.075 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLPage 186 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC38-2-060519 06/05/2019 320-51136-2 PFESA-BP10.062 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PMPA1.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC38-2-060519 06/05/2019 320-51136-2 PMPA1.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PFO2HxA0.14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0041PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PFO2HxA0.14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0041PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PFO3OA0.034 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0029PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PFO3OA0.034 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0029PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PEPA0.53 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC38-1-060519-Z06/05/2019 320-51251-3 PEPA0.52 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PFESA-BP20.066 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PFESA-BP20.061 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 R-EVE0.14 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 R-EVE0.14 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 Byproduct 40.25 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 Byproduct 40.27 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 Byproduct 50.064 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 187 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC38-1-060519 06/05/2019 320-51139-3 PFMOAA0.28 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PFMOAA0.33 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PFO5DA0.047 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PFO5DA0.047 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PFO2HxA0.17 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PFO2HxA0.18 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PEPA0.73 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PEPA0.78 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PFESA-BP10.26 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PFESA-BP10.28 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PMPA2.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC38-1-060519 06/05/2019 320-51139-3 PMPA2.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PMPA1.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PMPA1.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PFO3OA0.031 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PFO3OA0.034 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PFO4DA0.031 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 188 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PFO4DA0.031 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PEPA0.34 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PEPA0.34 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PFESA-BP20.031 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PFESA-BP20.03 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PFMOAA0.24 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PFMOAA0.25 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PFO5DA0.10 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PFO5DA0.11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PFO2HxA0.24 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PFO2HxA0.24 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PMPA1.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PMPA1.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PEPA0.34 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC37-060519 06/05/2019 320-51139-2 PEPA0.34 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PEPA0.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PEPA0.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLPage 189 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PMPA0.38 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC36-060519-Z-D06/05/2019 320-51251-4 PMPA0.38 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PEPA0.13 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PEPA0.13 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PMPA0.29 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC36-060519-Z 06/05/2019 320-51251-1 PMPA0.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 Byproduct 50.13 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 Byproduct 50.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PFESA-BP20.048 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PFESA-BP20.046 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PFO5DA0.088 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PFO5DA0.091 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PFO2HxA0.18 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PFO2HxA0.17 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC36-060519 06/05/2019 320-51139-1 Byproduct 50.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC36-060519 06/05/2019 320-51139-1 Byproduct 50.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PFO5DA0.079 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLPage 190 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC36-060519 06/05/2019 320-51139-1 PFO5DA0.074 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PEPA0.13 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC36-060519-D 06/05/2019 320-51139-5 PEPA0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PFESA-BP20.049 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PFESA-BP20.047 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PFO2HxA0.17 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PFO2HxA0.18 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PEPA0.14 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PEPA0.13 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC36-060519 06/05/2019 320-51139-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.060PQLASTW-LOC36-060519 06/05/2019 320-51139-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.074 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.060PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PMPA0.66 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC36-060519 06/05/2019 320-51139-1 PMPA0.61 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 Byproduct 50.52 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 191 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 Byproduct 50.49 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 Byproduct 60.026 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 Byproduct 60.025 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PFESA-BP21.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PFESA-BP21.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 Hydro-EVE Acid0.044 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 Hydro-EVE Acid0.043 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PFMOAA8.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PFMOAA8.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PFO2HxA2.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PFO2HxA2.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PFO3OA0.91 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PFO3OA0.91 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PFO4DA0.68 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PFO4DA0.68 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PFO5DA0.42 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PFO5DA0.38 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLPage 192 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PEPA0.100 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 PEPA0.082 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 Byproduct 50.73 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 Byproduct 50.77 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 Byproduct 60.029 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 Byproduct 60.03 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 NVHOS0.35 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC35-2-060519-Z06/05/2019 320-51241-1 NVHOS0.33 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PFESA-BP21.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PFESA-BP21.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 Hydro-EVE Acid0.056 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 Hydro-EVE Acid0.062 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PFMOAA10 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PFMOAA10.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PFO2HxA2.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PFO2HxA2.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PFO3OA1.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 193 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC35-2-060519 06/05/2019 320-51136-1 PFO3OA1.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PFO4DA0.78 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PFO4DA0.74 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PFO5DA0.58 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PFO5DA0.58 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PEPA0.097 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PEPA0.093 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PFESA-BP10.099 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 PFESA-BP10.089 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 Byproduct 60.028 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 Byproduct 60.028 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 NVHOS0.38 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC35-2-060519 06/05/2019 320-51136-1 NVHOS0.39 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 Hydro-EVE Acid0.048 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC35-1-060519-Z-D06/05/2019 320-51232-4 Hydro-EVE Acid0.05 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 Total SuspendedSolids22 MG/L5.02540 D-1997J5.0MDLASTW-LOC33-060519 06/05/2019 320-51089-1 Total SuspendedSolids210 MG/L102540 D-1997J10MDLPage 194 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC35-1-060519-D06/05/2019 320-51089-5 Byproduct 60.029 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 Byproduct 60.03 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 Hydro-EVE Acid0.053 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 Hydro-EVE Acid0.055 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC35-1-060519-D06/05/2019 320-51089-5 PMPA0.58 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC35-1-060519 06/05/2019 320-51089-3 Total SuspendedSolids23 MG/L5.02540 D-1997J5.0MDLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 Byproduct 50.078 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 Byproduct 50.083 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PFESA-BP20.10 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PFESA-BP20.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PFMOAA0.35 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PFMOAA0.32 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PFO5DA0.46 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PFO5DA0.45 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PFO2HxA0.16 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PFO2HxA0.16 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLPage 195 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PFO3OA0.06 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PEPA0.19 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PEPA0.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PFESA-BP10.044 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PFESA-BP10.037 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PMPA0.64 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC34-060519-Z 06/05/2019 320-51232-2 PMPA0.63 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC34-060519 06/05/2019 320-51089-2 Total SuspendedSolids810 MG/L502540 D-1997J50MDLASTW-LOC34-060519 06/05/2019 320-51089-2 PFESA-BP20.13 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC34-060519 06/05/2019 320-51089-2 PFESA-BP20.12 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC34-060519 06/05/2019 320-51089-2 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC34-060519 06/05/2019 320-51089-2 PFMOAA0.24 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC34-060519 06/05/2019 320-51089-2 PFO2HxA0.18 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC34-060519 06/05/2019 320-51089-2 PFO2HxA0.18 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PMPA1.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PMPA1.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLPage 196 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC34-060519 06/05/2019 320-51089-2 PFESA-BP10.059 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC34-060519 06/05/2019 320-51089-2 PFESA-BP10.053 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC34-060519 06/05/2019 320-51089-2 PMPA0.91 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC34-060519 06/05/2019 320-51089-2 PMPA0.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 R-EVE0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 R-EVE0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 Byproduct 40.19 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 Byproduct 40.22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 Byproduct 50.18 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 Byproduct 50.19 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PFESA-BP20.29 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PFESA-BP20.29 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 Hydro-EVE Acid0.039 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 Hydro-EVE Acid0.038 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PFO2HxA0.24 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PFO2HxA0.25 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PFO3OA0.081 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 197 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PFO3OA0.076 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PFO4DA0.097 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PFO4DA0.096 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PFO5DA0.40 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PFO5DA0.43 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PEPA0.54 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PEPA0.55 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PFESA-BP10.13 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 PFESA-BP10.13 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 NVHOS0.086 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC33-060519-Z 06/05/2019 320-51232-1 NVHOS0.093 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC33-060519 06/05/2019 320-51089-1 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC33-060519 06/05/2019 320-51089-1 Byproduct 40.17 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC33-060519 06/05/2019 320-51089-1 Byproduct 50.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC33-060519 06/05/2019 320-51089-1 Byproduct 50.16 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PFESA-BP20.32 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PFESA-BP20.33 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLPage 198 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC33-060519 06/05/2019 320-51089-1 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC33-060519 06/05/2019 320-51089-1 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PFO4DA0.13 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PFO4DA0.14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PFO5DA0.48 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PFO5DA0.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PFO2HxA0.22 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PFO2HxA0.22 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PEPA0.59 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PEPA0.65 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PFESA-BP10.14 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PFESA-BP10.14 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PMPA1.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC33-060519 06/05/2019 320-51089-1 PMPA2.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC33-060519 06/05/2019 320-51089-1 NVHOS0.100 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC33-060519 06/05/2019 320-51089-1 NVHOS0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 Byproduct 50.066 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 199 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC32-060519-Z 06/05/2019 320-51220-4 Byproduct 50.071 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PFESA-BP20.17 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PFESA-BP20.18 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PFO5DA0.081 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PFO5DA0.087 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 Byproduct 40.18 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 Byproduct 50.13 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 Byproduct 50.14 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PFESA-BP20.073 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PFESA-BP20.073 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PFO2HxA0.20 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PFO2HxA0.19 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PFO3OA0.11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PFO3OA0.12 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PFO4DA0.084 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLPage 200 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PFO5DA0.10 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PFO5DA0.11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PEPA0.21 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PEPA0.22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 NVHOS0.059 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 NVHOS0.063 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC30-060519 06/05/2019 320-51215-1 Byproduct 50.10 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC30-060519 06/05/2019 320-51215-1 Byproduct 50.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PFESA-BP20.090 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PFESA-BP20.09 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PFO2HxA0.19 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PFO2HxA0.19 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PFO3OA0.10 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PFO3OA0.11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PFO4DA0.082 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PFO5DA0.10 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLPage 201 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC30-060519 06/05/2019 320-51215-1 PFO5DA0.11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PMPA0.65 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC30-060519 06/05/2019 320-51215-1 PMPA0.65 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PEPA0.13 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PEPA0.13 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC32-060519-Z 06/05/2019 320-51220-4 PFESA-BP10.033 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PMPA0.65 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC30-060519-Z 06/05/2019 320-51220-1 PMPA0.65 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PFESA-BP20.19 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PFESA-BP20.18 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PFESA-BP10.03 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PMPA0.69 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC32-060519 06/05/2019 320-51215-5 PMPA0.78 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PFO2HxA1.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PFO2HxA1.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLPage 202 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PFO3OA0.50 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PFO3OA0.49 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PFO4DA0.42 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PFO4DA0.39 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PEPA1.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PEPA1.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PMPA2.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC10-060519-Z 06/05/2019 320-51271-3 PMPA2.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PFESA-BP20.63 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PFESA-BP20.65 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC10-060519 06/05/2019 320-51128-3 Hydro-EVE Acid0.075 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC10-060519 06/05/2019 320-51128-3 Hydro-EVE Acid0.079 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC10-060519 06/05/2019 320-51128-3 Total SuspendedSolids24 MG/L5.02540 D-1997J5.0MDLASTW-LOC10-060519 06/05/2019 320-51128-3 R-EVE0.34 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC10-060519 06/05/2019 320-51128-3 R-EVE0.36 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC10-060519 06/05/2019 320-51128-3 Byproduct 40.94 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC10-060519 06/05/2019 320-51128-3 Byproduct 41.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLPage 203 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC10-060519 06/05/2019 320-51128-3 Byproduct 50.62 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC10-060519 06/05/2019 320-51128-3 Byproduct 50.67 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC10-060519 06/05/2019 320-51128-3 Byproduct 60.026 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC10-060519 06/05/2019 320-51128-3 Byproduct 60.027 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PFMOAA2.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PFMOAA2.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PMPA3.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PMPA3.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PFO2HxA1.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PFO2HxA1.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PFO3OA0.66 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PFO3OA0.72 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PFO4DA0.38 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PFO4DA0.36 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PEPA1.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PEPA1.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC10-060519 06/05/2019 320-51128-3 PFESA-BP10.82 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLPage 204 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC10-060519 06/05/2019 320-51128-3 PFESA-BP10.85 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC10-060519 06/05/2019 320-51128-3 NVHOS0.32 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC10-060519 06/05/2019 320-51128-3 NVHOS0.33 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PFO2HxA0.087 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PFO2HxA0.085 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PFO3OA0.016 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PFO3OA0.017 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PFO4DA0.013 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PFO4DA0.013 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PEPA0.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PEPA0.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PFO2HxA0.11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PFO2HxA0.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PMPA0.65 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC2-060519 06/05/2019 320-51140-3 PMPA0.63 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC2-060519 06/05/2019 320-51140-3 Total SuspendedSolids18 MG/L5.02540 D-1997J5.0MDLASTW-LOC2-060519 06/05/2019 320-51140-3 PEPA0.16 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLPage 205 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC2-060519 06/05/2019 320-51140-3 PEPA0.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PMPA0.030 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PMPA0.029 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PMPA0.43 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC2-060519-Z 06/05/2019 320-51243-3 PMPA0.44 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC26-060519 06/05/2019 320-51135-1 Total SuspendedSolids5.6 MG/L5.02540 D-1997J5.0MDLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PMPA0.079 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PMPA0.077 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PFO2HxA0.024 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PFO2HxA0.023 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PFO3OA0.0070 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PFO3OA0.0075 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PFO4DA0.0055 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PFO4DA0.0051 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PEPA0.023 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC3-060519-Z 06/05/2019 320-51271-1 PEPA0.023 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PFESA-BP20.0048 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 206 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PFESA-BP20.0048 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PFMOAA0.011 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PFMOAA0.011 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0050PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PFO2HxA0.017 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PFO2HxA0.017 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PFO3OA0.0023 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PFO3OA0.0023 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PFO5DA0.0045 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PFO5DA0.0051 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC3-060519 06/05/2019 320-51128-1 Total SuspendedSolids9.2 MG/L5.02540 D-1997J5.0MDLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PEPA0.032 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PEPA0.031 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PFESA-BP10.0035 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PFESA-BP10.0035 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PMPA0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 PMPA0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC28-060519-Z 06/05/2019 320-51274-3 NVHOS0.0030 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 207 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC28-060519-Z 06/05/2019 320-51274-3 NVHOS0.003 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC27-060519 06/05/2019 320-51135-2 PEPA0.069 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC27-060519 06/05/2019 320-51135-2 Total SuspendedSolids50 MG/L5.02540 D-1997J5.0MDLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PFO2HxA0.0038 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC26-060519-Z 06/05/2019 320-51274-1 PFO2HxA0.0038 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PFO2HxA0.034 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PFO2HxA0.032 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PFO3OA0.0079 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PFO3OA0.0077 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PFO4DA0.0047 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PFO4DA0.0046 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PEPA0.030 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PEPA0.03 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PMPA0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC27-060519-Z 06/05/2019 320-51274-2 PMPA0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC28-060519 06/05/2019 320-51135-3 Total SuspendedSolids36 MG/L5.02540 D-1997J5.0MDLPage 208 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC42-1-060519 06/05/2019 320-51140-1 PMPA4.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PMPA4.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLTB-4-06051906/05/2019 320-51135-4 PMPA0.59 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLTB-4-06051906/05/2019 320-51135-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PFO2HxA0.032 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PFO2HxA0.032 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PFO3OA0.0058 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PFO3OA0.0058 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PFO4DA0.016 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PFO4DA0.017 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PEPA0.085 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PEPA0.084 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PMPA0.26 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC55-060519-Z 06/05/2019 320-51278-3 PMPA0.26 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC55-060519 06/05/2019 320-51133-3 Total SuspendedSolids290 MG/L502540 D-1997J50MDLASTW-LOC55-060519 06/05/2019 320-51133-3 PFESA-BP20.087 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PFESA-BP20.085 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLPage 209 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC55-060519 06/05/2019 320-51133-3 PEPA0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PEPA0.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PMPA0.73 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC55-060519 06/05/2019 320-51133-3 PMPA0.69 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PMPA0.39 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PMPA0.38 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PFO2HxA0.27 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PFO2HxA0.27 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PFO3OA0.11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PFO3OA0.11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PFO4DA0.055 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PFO4DA0.058 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PEPA0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC53-060519-Z 06/05/2019 320-51278-2 PEPA0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC53-060519 06/05/2019 320-51133-2 Total SuspendedSolids17 MG/L5.02540 D-1997J5.0MDLASTW-LOC53-060519 06/05/2019 320-51133-2 PFESA-BP20.074 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PFESA-BP20.071 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLPage 210 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC53-060519 06/05/2019 320-51133-2 PFMOAA0.52 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PFMOAA0.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PMPA1.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PMPA1.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PFO2HxA0.36 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PFO2HxA0.36 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PFO4DA0.091 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PFO4DA0.094 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PEPA0.18 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PEPA0.19 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC53-060519 06/05/2019 320-51133-2 PFESA-BP10.029 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PFO2HxA2.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0081PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PFO2HxA2.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0081PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PFO3OA0.44 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0058PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PFO3OA0.39 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0058PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PFO4DA0.37 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0079PQLPage 211 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PFO4DA0.35 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0079PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PEPA4.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PEPA4.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PMPA11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.057PQLASTW-LOC52-060519-Z 06/05/2019 320-51278-1 PMPA11.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.057PQLASTW-LOC52-060519 06/05/2019 320-51133-1 Total SuspendedSolids78 MG/L5.02540 D-1997J5.0MDLASTW-LOC52-060519 06/05/2019 320-51133-1 R-EVE0.31 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC52-060519 06/05/2019 320-51133-1 R-EVE0.31 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC52-060519 06/05/2019 320-51133-1 Byproduct 41.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC52-060519 06/05/2019 320-51133-1 Byproduct 41.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC52-060519 06/05/2019 320-51133-1 Byproduct 50.65 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC52-060519 06/05/2019 320-51133-1 Byproduct 50.66 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PFESA-BP20.65 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PFESA-BP20.68 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC52-060519 06/05/2019 320-51133-1 Hydro-EVE Acid0.055 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC52-060519 06/05/2019 320-51133-1 Hydro-EVE Acid0.05 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PFMOAA0.49 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLPage 212 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC52-060519 06/05/2019 320-51133-1 PFMOAA0.51 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PFO2HxA1.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PFO2HxA1.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PFO3OA0.36 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PFO3OA0.35 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PFO5DA0.19 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PFO5DA0.17 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PEPA4.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PEPA4.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PFESA-BP10.54 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PFESA-BP10.58 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PMPA9.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC52-060519 06/05/2019 320-51133-1 PMPA9.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC52-060519 06/05/2019 320-51133-1 NVHOS0.22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC52-060519 06/05/2019 320-51133-1 NVHOS0.22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PFO2HxA0.022 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PFO2HxA0.021 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 213 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PFO3OA0.0027 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PFO3OA0.0026 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PFO4DA0.0027 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PFO4DA0.003 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PEPA0.058 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PEPA0.059 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.020PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PMPA0.19 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC5-060519-Z 06/05/2019 320-51271-2 PMPA0.18 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.010PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PMPA1.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PMPA1.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC5-060519 06/05/2019 320-51128-2 Total SuspendedSolids26 MG/L5.02540 D-1997J5.0MDLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PFO2HxA8.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PFO2HxA8.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PFO3OA4.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PFO3OA4.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PEPA0.64 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC43-060519-Z 06/05/2019 320-51243-2 PEPA0.64 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLPage 214 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC43-060519 06/05/2019 320-51140-2 Total SuspendedSolids14 MG/L5.02540 D-1997J5.0MDLASTW-LOC43-060519 06/05/2019 320-51140-2 R-EVE0.27 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC43-060519 06/05/2019 320-51140-2 R-EVE0.24 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC43-060519 06/05/2019 320-51140-2 Byproduct 40.89 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC43-060519 06/05/2019 320-51140-2 Byproduct 40.81 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC43-060519 06/05/2019 320-51140-2 Byproduct 51.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC43-060519 06/05/2019 320-51140-2 Byproduct 51.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC43-060519 06/05/2019 320-51140-2 Byproduct 60.028 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC43-060519 06/05/2019 320-51140-2 Byproduct 60.029 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PFMOAA26 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PFMOAA26.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC43-060519 06/05/2019 320-51140-2 EVE Acid0.031 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLASTW-LOC43-060519 06/05/2019 320-51140-2 EVE Acid0.03 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PFESA-BP20.77 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PFESA-BP20.77 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC43-060519 06/05/2019 320-51140-2 Hydro-EVE Acid0.17 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC43-060519 06/05/2019 320-51140-2 Hydro-EVE Acid0.18 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLPage 215 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC43-060519 06/05/2019 320-51140-2 PFO2HxA7.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PFO2HxA7.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PFO3OA3.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PFO3OA3.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PFO4DA3.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PFO4DA3.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PFO5DA2.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PFO5DA2.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PEPA0.58 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PEPA0.58 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PFESA-BP11.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PFESA-BP11.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PMPA1.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC43-060519 06/05/2019 320-51140-2 PMPA1.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PMPA1.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PMPA1.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 R-EVE0.43 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLPage 216 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 R-EVE0.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 Byproduct 40.63 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 Byproduct 40.59 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 Byproduct 50.89 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 Byproduct 50.85 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 Byproduct 60.043 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 Byproduct 60.038 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC43-060519 06/05/2019 320-51140-2 NVHOS0.42 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC43-060519 06/05/2019 320-51140-2 NVHOS0.43 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PFMOAA46 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PFMOAA44.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 Hydro-EVE Acid0.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 Hydro-EVE Acid0.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PFO2HxA12 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PFO2HxA11.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLPage 217 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PFO3OA7.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PFO3OA7.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PFO4DA5.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PFO4DA5.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PEPA0.68 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PEPA0.66 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PFESA-BP11.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 PFESA-BP11.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 R-EVE0.43 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 R-EVE0.42 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 Byproduct 40.71 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 Byproduct 40.75 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 Byproduct 50.97 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 Byproduct 51.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 Byproduct 60.040 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 Byproduct 60.041 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 NVHOS0.47 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLPage 218 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC42-2-060519-Z06/05/2019 320-51275-1 NVHOS0.45 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PFMOAA42 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PFMOAA44.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 EVE Acid0.033 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 EVE Acid0.034 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PFESA-BP20.94 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PFESA-BP20.94 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 Hydro-EVE Acid0.16 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 Hydro-EVE Acid0.15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PFO2HxA13 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PFO2HxA13.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PFO3OA8.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PFO3OA8.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PFO4DA7.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PFO4DA8.1 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PFO5DA4.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PFO5DA4.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLPage 219 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC42-2-060519 06/05/2019 320-51141-1 PEPA0.75 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PEPA0.79 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PFESA-BP11.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PFESA-BP11.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PMPA1.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 PMPA2.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PMPA4.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PMPA4.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 NVHOS0.40 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC42-2-060519 06/05/2019 320-51141-1 NVHOS0.41 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PFO2HxA31 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PFO2HxA31.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PFO3OA13 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PFO3OA13.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PFO4DA9.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PFO4DA11.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PEPA1.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLPage 220 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC42-1-060519-Z06/05/2019 320-51243-1 PEPA1.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 Total SuspendedSolids21 MG/L102540 D-1997J10MDLASTW-LOC42-1-060519 06/05/2019 320-51140-1 R-EVE1.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 R-EVE1.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 Byproduct 43.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 Byproduct 43.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 Byproduct 51.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 Byproduct 51.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 Byproduct 60.39 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 Byproduct 60.42 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.015PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PFMOAA105 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PFMOAA110.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 EVE Acid0.086 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 EVE Acid0.091 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PFESA-BP27.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PFESA-BP27.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 Hydro-EVE Acid1.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLPage 221 of 223
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC42-1-060519 06/05/2019 320-51140-1 Hydro-EVE Acid1.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PFO2HxA30 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PFO2HxA32.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PFO3OA12 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PFO3OA13.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PFO4DA8.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PFO4DA8.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PFO5DA4.9 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PFO5DA5.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PEPA1.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PEPA1.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PFESA-BP11.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLASTW-LOC42-1-060519 06/05/2019 320-51140-1 PFESA-BP12.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLPage 222 of 223
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit but above the rejection limit. Thereported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Additional SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PFO2HxA0.21 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLASTW-LOC37-060519-Z 06/05/2019 320-51251-2 PFO2HxA0.21 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.0020PQLPage 223 of 223
ADQM Data Review Narrative - FAY 2019 Dry Stormwater Samp rev2.doc 1 of 3
ADQM DATA REVIEW NARRATIVE
Site Chemours FAY – Fayetteville Project 2019 Dry Stormwater Sampling Project Reviewer Michael Aucoin, AECOM as a Chemours contractor Sampling Dates April 24 - 25, 2019 Analytical Protocol Laboratory Analytical Method Parameter(s)
TestAmerica - Sacramento 537 Modified PFAS1
TestAmerica - Sacramento Cl. Spec. Table 3 Compound SOP Table 3+ compounds

1 Perfluoroalkylsubstances, a list of 33 compounds including HFPO-DA. Sample Receipt
The following items are noted for this data set:
• All samples were received in satisfactory condition and within EPA temperature guidelines on April 26, 2019, except for a waste acid sample (LOC17A) received on May 17, 2019. Data Review The electronic data submitted for this project was reviewed via the Data Verification Module (DVM) process. Overall the data is acceptable for use without qualification, except as noted below:
• Non-detect results for PPF Acid in one sample were qualified R and are considered to be unusable due to very poor matrix spike (MS) relative percent recoveries (RPR). The lab revised reports to apply a Z qualifier for four Table 3+ compounds (DFSA, MMF, MTP, PPF Acid), indicating poor performance in the presence of matrix effects, including inconsistent sample results. The data reviewer qualified these analytical results J as estimated, and non-detect results were qualified UJ indicating an estimated reporting limit, unless the DVM had already applied a B or R qualifier. Subsequently DFSA, MMF, MTP, and PPF Acid were dropped from the method. These compounds were not reported for the waste acid sample.
• Professional judgement was used to overwrite R qualifiers, indicating an unusable result, that were assigned by the DVM due to very poor matrix recoveries for PFMOAA and MTP in one sample. The qualifiers were updated to UJ, indicating an estimated reporting limit, because the surrogate compound was a measurable labeled isotope compound, which is used for quantitation and provides a sample specific recovery correction of the sample results.
ADQM Data Review Narrative - FAY 2019 Dry Stormwater Samp rev2.doc 2 of 3
• Some of the analytical results have been qualified B, and may be biased high, or may be a false positive, because an associated field or equipment blank contained a comparable concentration.
• Several analytical results have been qualified J as estimated, and non-detect results qualified UJ indicating an estimated reporting limit, due to poor recovery of surrogate, laboratory blank spike, or matrix spike compounds; sample preparation and/or analysis which exceeded the laboratory hold times; and poor laboratory blank spike, matrix spike, field duplicate or lab replicate precision. See the Data Verification Module (DVM) Narrative Report for which samples were qualified, the specific reasons for qualification, and potential bias in reported results.
Attachments The DVM Narrative report is attached. The lab reports due to a large page count are stored on an AECOM network shared drive and are available to be posted on external shared drives, or on a flash drive.

ADQM Data Review Narrative - FAY 2019 Dry Stormwater Samp rev2.doc 3 of 3
Data Verification Module (DVM)
The DVM is an internal review process used by the ADQM group to assist with the determination of data usability. The electronic data deliverables received from the laboratory are loaded into the Locus EIM™ database and processed through a series of data quality checks, which are a combination of software (Locus EIM™ database Data Verification Module (DVM)) and manual reviewer evaluations. The data is evaluated against the following data usability checks:
• Field and laboratory blank contamination
• US EPA hold time criteria
• Missing Quality Control (QC) samples
• Matrix spike(MS)/matrix spike duplicate (MSD) recoveries and the relative percent differences
(RPDs) between these spikes
• Laboratory control sample(LCS)/control sample duplicate (LCSD) recoveries and the RPD
between these spikes
• Surrogate spike recoveries for organic analyses
• RPD between field duplicate sample pairs
• RPD between laboratory replicates for inorganic analyses
• Difference / percent difference between total and dissolved sample pairs. There are two qualifier fields in EIM: Lab Qualifier is the qualifier assigned by the lab and may not reflect the usability of the data. This qualifier may have many different meanings and can vary between labs and over time within the same lab. Please refer to the laboratory report for a description of the lab qualifiers. As they are lab descriptors they are not to be used when evaluating the data. Validation Qualifier is the 3rd party formal validation qualifier if this was performed. Otherwise this field contains the qualifier resulting from the ADQM DVM review process. This qualifier assesses the usability of the data and may not equal the lab qualifier. The DVM applies the following data
evaluation qualifiers to analysis results, as warranted: Qualifier Definition B Not detected substantially above the level reported in the laboratory or field blanks. R Unusable result. Analyte may or may not be present in the sample.
J Analyte present. Reported value may not be accurate or precise.
UJ Not detected. Reporting limit may not be accurate or precise.

The Validation Status Code field is set to “DVM” if the ADQM DVM process has been performed. If the DVM has not been run, the field will be blank.
If the DVM has been run (Validation Status Code equals “DVM”), use the Validation Qualifier.
DVM Narrative ReportAssociated MS and/or MSD analysis had relative percent recovery (RPR) values less than the data rejection level. The reported non-detect result isunusable.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC14-042419 04/24/2019 320-49620-8 PPF Acid0.38 UG/LCl. Spec. Table 3Compound SOPRPFAS_DI_Prep0.38PQLDSTW-LOC14-042419 04/24/2019 320-49620-8 PPF Acid0.38 UG/LCl. Spec. Table 3Compound SOPRPFAS_DI_Prep0.38PQLPage 1 of 37
Contamination detected in equipment blank(s). Sample result does not differ significantly from the analyte concentration detected in the associatedequipment blank(s).LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC7B-042419 04/24/2019 320-49623-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.90 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.060PQLDSTW-LOC7B-042419 04/24/2019 320-49623-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.79 ug/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.060PQLPage 2 of 37
Contamination detected in Field Blank(s). Sample result does not differ significantly from the analyte concentration detected in the associated fieldblank(s).LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC10-042419 04/24/2019 320-49620-7 PPF Acid1.1 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.38PQLDSTW-LOC10-042419 04/24/2019 320-49620-7 PPF Acid0.93 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.38PQLDSTW-LOC1-042419 04/24/2019 320-49620-3 PPF Acid0.82 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.38PQLDSTW-LOC1-042419 04/24/2019 320-49620-3 PPF Acid0.72 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.38PQLDSTW-LOC15-042419 04/24/2019 320-49620-9 PPF Acid1.1 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.38PQLDSTW-LOC15-042419 04/24/2019 320-49620-9 PPF Acid1.1 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.38PQLDSTW-LOC20-042419 04/24/2019 320-49620-11 PPF Acid0.85 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.38PQLDSTW-LOC20-042419 04/24/2019 320-49620-11 PPF Acid0.88 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.38PQLDSTW-LOC20-042419-D 04/24/2019 320-49620-12 PPF Acid0.89 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.38PQLDSTW-LOC20-042419-D 04/24/2019 320-49620-12 PPF Acid0.96 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.38PQLDSTW-LOC24B-042419 04/24/2019 320-49620-1 PPF Acid0.79 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.38PQLDSTW-LOC24B-042419 04/24/2019 320-49620-1 PPF Acid0.56 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.38PQLDSTW-LOC24C-042419 04/24/2019 320-49620-2 PPF Acid0.53 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.38PQLDSTW-LOC24C-042419 04/24/2019 320-49620-2 PPF Acid0.59 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.38PQLDSTW-LOC7A-042419 04/24/2019 320-49620-4 PPF Acid0.96 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.38PQLDSTW-LOC7A-042419 04/24/2019 320-49620-4 PPF Acid0.82 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.38PQLPage 3 of 37
Contamination detected in Field Blank(s). Sample result does not differ significantly from the analyte concentration detected in the associated fieldblank(s).LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC9-042419 04/24/2019 320-49620-6 PPF Acid0.82 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.38PQLDSTW-LOC9-042419 04/24/2019 320-49620-6 PPF Acid0.79 UG/LCl. Spec. Table 3Compound SOPBPFAS_DI_Prep0.38PQLPage 4 of 37
Only one surrogate has relative percent recovery (RPR) values outside control limits and the parameter is a PFC (Nondetects).LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC22-042419 04/24/2019 320-49624-9 Perfluorobutanoic Acid0.0035 UG/L537 ModifiedUJ3535_PFC0.0035PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 PerfluorodecanoicAcid0.0020 UG/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 PerfluorodecaneSulfonic Acid0.0020 UG/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 PerfluorohexaneSulfonic Acid0.0020 UG/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 ADONA0.0021 UG/L537 ModifiedUJ3535_PFC0.0021PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 NaDONA0.0021 ug/L537 ModifiedUJ3535_PFC0.0021PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 Perfluorooctadecanoicacid0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 PFOS0.0020 UG/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 PerfluoroundecanoicAcid0.0020 UG/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 Perfluoropentanesulfonic acid (PFPeS)0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 6:2 Fluorotelomersulfonate0.020 ug/L537 ModifiedUJ3535_PFC0.020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 PerfluorohexanoicAcid0.0020 UG/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 PerfluorododecanoicAcid0.0020 UG/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 PerfluorobutaneSulfonic Acid0.0020 UG/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 PerfluoroheptanoicAcid0.0020 UG/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 Perfluoroheptanesulfonic acid (PFHpS)0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 PerfluorononanoicAcid0.0020 UG/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 PerfluorotetradecanoicAcid0.0020 UG/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 Perfluorohexadecanoicacid (PFHxDA)0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 Perfluorononanesulfonic acid0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 PerfluorotridecanoicAcid0.0020 UG/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 F-53B Major0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLPage 5 of 37
Only one surrogate has relative percent recovery (RPR) values outside control limits and the parameter is a PFC (Nondetects).LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC19A-042419 04/24/2019 320-49624-6 PerfluorooctaneSulfonamide0.0020 UG/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 Perfluorododecanesulfonic acid (PFDoS)0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 F-53B Minor0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLPage 6 of 37
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC23A-042419 04/24/2019 320-49624-10 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 7 of 37
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC23A-042419 04/24/2019 320-49624-10 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 NVHOS54 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep54PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 NVHOS54 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep54PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PES46 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep46PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PES46 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep46PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PMPA570 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep570PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PMPA570 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep570PQLPage 8 of 37
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC17A-042419 04/24/2019 320-50472-1 PFECA B60 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep60PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PFECA B60 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep60PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol60 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep60PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol60 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep60PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol110 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep110PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol110 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep110PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 N-methyl perfluoro-1-octanesulfonamide26 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep26PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 N-methyl perfluoro-1-octanesulfonamide26 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep26PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 DFSA3100 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep3100PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 DFSA3100 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep3100PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 EVE Acid24 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep24PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 EVE Acid24 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep24PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PFESA-BP230 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep30PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PFESA-BP230 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep30PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 Hydro-EVE Acid28 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep28PQLPage 9 of 37
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC17B-042419 04/24/2019 320-49624-4 Hydro-EVE Acid28 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep28PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PFECA-G41 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep41PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PFECA-G41 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep41PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 R-EVE70 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep70PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 R-EVE70 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep70PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 Byproduct 4160 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep160PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 Byproduct 4160 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep160PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 Byproduct 558 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep58PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 Byproduct 558 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep58PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 Byproduct 615 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep15PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 Byproduct 615 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep15PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PES34 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep34PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PES34 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep34PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PFO4DA59 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep59PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PFO4DA59 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep59PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PFO5DA25 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep25PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PFO5DA25 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep25PQLPage 10 of 37
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC16-042419 04/24/2019 320-49624-3 N-ethylperfluoro-1-octanesulfonamide28 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep28PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 N-ethylperfluoro-1-octanesulfonamide28 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep28PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PFESA-BP127 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep27PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PFESA-BP127 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep27PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 N-methyl perfluoro-1-octanesulfonamide35 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep35PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 N-methyl perfluoro-1-octanesulfonamide35 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep35PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PFO2HxA81 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep81PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PFO2HxA81 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep81PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PFO3OA58 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep58PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PFO3OA58 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep58PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PFO4DA79 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep79PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PFO4DA79 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep79PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PFO5DA34 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep34PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PFO5DA34 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep34PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 N-ethylperfluoro-1-octanesulfonamide37 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep37PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 N-ethylperfluoro-1-octanesulfonamide37 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep37PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PFMOAA210 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep210PQLPage 11 of 37
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC17A-042419 04/24/2019 320-50472-1 PFMOAA210 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep210PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 EVE Acid24 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep24PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 EVE Acid24 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep24PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PFESA-BP230 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep30PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PFESA-BP230 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep30PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 Hydro-EVE Acid28 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep28PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 Hydro-EVE Acid28 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep28PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PFECA-G41 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep41PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PFECA-G41 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep41PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 R-EVE70 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep70PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 R-EVE70 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep70PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 Byproduct 4160 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep160PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 Byproduct 4160 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep160PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 Byproduct 558 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep58PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 Byproduct 558 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep58PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 Byproduct 615 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep15PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 Byproduct 615 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep15PQLPage 12 of 37
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC17B-042419 04/24/2019 320-49624-4 NVHOS54 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep54PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 NVHOS54 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep54PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PES46 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep46PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PES46 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep46PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PMPA570 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep570PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PMPA570 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep570PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 MMF3600 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep3600PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 MMF3600 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep3600PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PFECA B60 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep60PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PFECA B60 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep60PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol60 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep60PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol60 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep60PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol110 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep110PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol110 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep110PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 MMF2700 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep2700PQLPage 13 of 37
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC16-042419 04/24/2019 320-49624-3 MMF2700 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep2700PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PFECA B45 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep45PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PFECA B45 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep45PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol45 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep45PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol45 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep45PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol82 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep82PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol82 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep82PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PEPA35 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep35PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PEPA35 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep35PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PFECA-G31 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep31PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PFECA-G31 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep31PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PFESA-BP127 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep27PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PFESA-BP127 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep27PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 N-methyl perfluoro-1-octanesulfonamide35 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep35PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 N-methyl perfluoro-1-octanesulfonamide35 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep35PQLPage 14 of 37
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC17B-042419 04/24/2019 320-49624-4 PFO2HxA81 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep81PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PFO2HxA81 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep81PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PFO3OA58 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep58PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PFO3OA58 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep58PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PFO4DA79 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep79PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PFO4DA79 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep79PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PFO5DA34 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep34PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PFO5DA34 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep34PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 N-ethylperfluoro-1-octanesulfonamide37 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep37PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 N-ethylperfluoro-1-octanesulfonamide37 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep37PQLPage 15 of 37
Associated LCS and/or LCSD analysis had relative percent recovery (RPR) values less than the lower control limit but above 10%. The actual detectionlimits may be higher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC9-042419 04/24/2019 320-49620-6 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-LOC9-042419 04/24/2019 320-49620-6 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-LOC9-042419 04/24/2019 320-49620-6 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC9-042419 04/24/2019 320-49620-6 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC8-042419 04/24/2019 320-49620-5 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC8-042419 04/24/2019 320-49620-5 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC8-042419 04/24/2019 320-49620-5 PPF Acid0.38 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.38PQLDSTW-LOC8-042419 04/24/2019 320-49620-5 PPF Acid0.38 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.38PQLDSTW-LOC7A-042419 04/24/2019 320-49620-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-LOC7A-042419 04/24/2019 320-49620-4 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-LOC7A-042419 04/24/2019 320-49620-4 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC7A-042419 04/24/2019 320-49620-4 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC6B-042419 04/24/2019 320-49624-2 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC6B-042419 04/24/2019 320-49624-2 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC24C-042419 04/24/2019 320-49620-2 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-LOC24C-042419 04/24/2019 320-49620-2 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLPage 16 of 37
Associated LCS and/or LCSD analysis had relative percent recovery (RPR) values less than the lower control limit but above 10%. The actual detectionlimits may be higher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC24C-042419 04/24/2019 320-49620-2 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC24C-042419 04/24/2019 320-49620-2 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC24B-042419 04/24/2019 320-49620-1 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-LOC24B-042419 04/24/2019 320-49620-1 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-LOC24B-042419 04/24/2019 320-49620-1 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC24B-042419 04/24/2019 320-49620-1 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC24A-042419 04/24/2019 320-49624-11 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC24A-042419 04/24/2019 320-49624-11 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC20-042419-D 04/24/2019 320-49620-12 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-LOC20-042419-D 04/24/2019 320-49620-12 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-LOC20-042419-D 04/24/2019 320-49620-12 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC20-042419-D 04/24/2019 320-49620-12 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC21A-042419 04/24/2019 320-49624-8 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC21A-042419 04/24/2019 320-49624-8 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC20-042419 04/24/2019 320-49620-11 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-LOC20-042419 04/24/2019 320-49620-11 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-LOC20-042419 04/24/2019 320-49620-11 MTP0.12 UG/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.12PQLPage 17 of 37
Associated LCS and/or LCSD analysis had relative percent recovery (RPR) values less than the lower control limit but above 10%. The actual detectionlimits may be higher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPDSTW-LOC20-042419 04/24/2019 320-49620-11 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 MTP120 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep120PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 MTP120 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep120PQLDSTW-LOC18-042419 04/24/2019 320-49624-5 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC18-042419 04/24/2019 320-49624-5 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC15-042419 04/24/2019 320-49620-9 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-LOC15-042419 04/24/2019 320-49620-9 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-LOC15-042419 04/24/2019 320-49620-9 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC15-042419 04/24/2019 320-49620-9 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-FB-042419 04/24/2019 320-49620-10 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-FB-042419 04/24/2019 320-49620-10 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-FB-042419 04/24/2019 320-49620-10 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-FB-042419 04/24/2019 320-49620-10 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC1-042419 04/24/2019 320-49620-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-LOC1-042419 04/24/2019 320-49620-3 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-LOC1-042419 04/24/2019 320-49620-3 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLPage 18 of 37
Associated LCS and/or LCSD analysis had relative percent recovery (RPR) values less than the lower control limit but above 10%. The actual detectionlimits may be higher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC1-042419 04/24/2019 320-49620-3 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC10-042419 04/24/2019 320-49620-7 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-LOC10-042419 04/24/2019 320-49620-7 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-LOC10-042419 04/24/2019 320-49620-7 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC10-042419 04/24/2019 320-49620-7 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 MTP91 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep91PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 MTP91 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep91PQLPage 19 of 37
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit. The actual detection limits may behigher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC20-042419 04/24/2019 320-49620-11 Perfluorooctadecanoicacid0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLDSTW-LOC7B-042419 04/24/2019 320-49623-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC7B-042419 04/24/2019 320-49623-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC6B-042419 04/24/2019 320-49624-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC6B-042419 04/24/2019 320-49624-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC6B-042419 04/24/2019 320-49624-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC6B-042419 04/24/2019 320-49624-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC6A-042419 04/24/2019 320-49624-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC6A-042419 04/24/2019 320-49624-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC6A-042419 04/24/2019 320-49624-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC6A-042419 04/24/2019 320-49624-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC24A-042419-D 04/24/2019 320-49624-12 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLDSTW-LOC24A-042419-D 04/24/2019 320-49624-12 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLDSTW-LOC22-042419 04/24/2019 320-49624-9 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC22-042419 04/24/2019 320-49624-9 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC22-042419 04/24/2019 320-49624-9 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC22-042419 04/24/2019 320-49624-9 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLPage 20 of 37
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit. The actual detection limits may behigher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC23A-042419 04/24/2019 320-49624-10 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC24A-042419 04/24/2019 320-49624-11 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC24A-042419 04/24/2019 320-49624-11 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC24A-042419 04/24/2019 320-49624-11 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC24A-042419 04/24/2019 320-49624-11 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC24A-042419 04/24/2019 320-49624-11 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLDSTW-LOC24A-042419 04/24/2019 320-49624-11 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLDSTW-LOC24A-042419 04/24/2019 320-49624-11 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLDSTW-LOC24A-042419 04/24/2019 320-49624-11 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLDSTW-LOC24A-042419-D 04/24/2019 320-49624-12 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC24A-042419-D 04/24/2019 320-49624-12 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC24A-042419-D 04/24/2019 320-49624-12 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC24A-042419-D 04/24/2019 320-49624-12 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC21A-042419 04/24/2019 320-49624-8 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC21A-042419 04/24/2019 320-49624-8 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC21A-042419 04/24/2019 320-49624-8 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.037PQLPage 21 of 37
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit. The actual detection limits may behigher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPDSTW-LOC21A-042419 04/24/2019 320-49624-8 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC21A-042419 04/24/2019 320-49624-8 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLDSTW-LOC21A-042419 04/24/2019 320-49624-8 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLDSTW-LOC21A-042419 04/24/2019 320-49624-8 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLDSTW-LOC21A-042419 04/24/2019 320-49624-8 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLDSTW-LOC19B-042419 04/24/2019 320-49624-7 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC19B-042419 04/24/2019 320-49624-7 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC19B-042419 04/24/2019 320-49624-7 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC19B-042419 04/24/2019 320-49624-7 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC22-042419 04/24/2019 320-49624-9 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLDSTW-LOC22-042419 04/24/2019 320-49624-9 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLDSTW-LOC22-042419 04/24/2019 320-49624-9 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLDSTW-LOC22-042419 04/24/2019 320-49624-9 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PPF Acid0.38 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.38PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PPF Acid0.38 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.38PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 DFSA3.1 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep3.1PQLPage 22 of 37
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit. The actual detection limits may behigher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC23A-042419 04/24/2019 320-49624-10 DFSA3.1 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep3.1PQLDSTW-LOC18-042419 04/24/2019 320-49624-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC18-042419 04/24/2019 320-49624-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC18-042419 04/24/2019 320-49624-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC18-042419 04/24/2019 320-49624-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-EB-01-042419 04/24/2019 320-49623-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-EB-01-042419 04/24/2019 320-49623-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-EB-02-042419 04/24/2019 320-49623-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-EB-02-042419 04/24/2019 320-49623-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLDSTW-LOC14-042419 04/24/2019 320-49620-8 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLDSTW-LOC14-042419 04/24/2019 320-49620-8 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLDSTW-LOC14-042419 04/24/2019 320-49620-8 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLDSTW-LOC14-042419 04/24/2019 320-49620-8 Byproduct 40.16 UG/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.16PQLPage 23 of 37
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit. The actual detection limits may behigher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSOPDSTW-LOC14-042419 04/24/2019 320-49620-8 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLDSTW-LOC14-042419 04/24/2019 320-49620-8 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLPage 24 of 37
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the data rejection level. The reported non-detect result isconsidered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC14-042419 04/24/2019 320-49620-8 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-LOC14-042419 04/24/2019 320-49620-8 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLDSTW-LOC14-042419 04/24/2019 320-49620-8 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLDSTW-LOC14-042419 04/24/2019 320-49620-8 MTP0.12 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.12PQLPage 25 of 37
Associated LCS and/or LCSD analysis had relative percent recovery (RPR) values higher than the upper control limit. The reported result may bebiased high.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC23A-042419 04/24/2019 320-49624-10 MMF7.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 MMF5.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLPage 26 of 37
Associated MS and/or MSD analysis had relative percent recovery (RPR) values higher than the upper control limit. The reported result may be biasedhigh.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC19A-042419 04/24/2019 320-49624-6 MMF17 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLDSTW-LOC18-042419 04/24/2019 320-49624-5 MMF15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLDSTW-LOC18-042419 04/24/2019 320-49624-5 MMF13.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLDSTW-LOC19B-042419 04/24/2019 320-49624-7 MMF12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLDSTW-LOC19B-042419 04/24/2019 320-49624-7 MMF11.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLDSTW-LOC21A-042419 04/24/2019 320-49624-8 MMF19 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLDSTW-LOC24A-042419 04/24/2019 320-49624-11 Hfpo Dimer Acid0.016 UG/L537 ModifiedJ3535_PFC0.0040PQLDSTW-LOC8-042419 04/24/2019 320-49620-5 DFSA8.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.1PQLPage 27 of 37
High relative percent difference (RPD) observed between field duplicate and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC24A-042419 04/24/2019 320-49624-11 MMF14.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLDSTW-LOC24A-042419-D 04/24/2019 320-49624-12 MMF9.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLDSTW-LOC24A-042419-D 04/24/2019 320-49624-12 MMF8.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLPage 28 of 37
High relative percent difference (RPD) observed between LCS and LCSD samples. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC14-042419 04/24/2019 320-49620-8 MMF3.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLDSTW-LOC14-042419 04/24/2019 320-49620-8 MMF4.9 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLPage 29 of 37
Only one surrogate has relative percent recovery (RPR) values outside control limits and the parameter is a PFC (Detects).LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC19A-042419 04/24/2019 320-49624-6 PFOA0.0026 UG/L537 ModifiedJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 PerfluoropentanoicAcid0.0026 UG/L537 ModifiedJ3535_PFC0.0020PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 Hfpo Dimer Acid0.03 UG/L537 ModifiedJ3535_PFC0.0040PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 Perfluorobutanoic Acid0.0043 UG/L537 ModifiedJ3535_PFC0.0020PQLPage 30 of 37
Quality review criteria exceeded between the REP (laboratory replicate) and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC17B-042419 04/24/2019 320-49624-4 PEPA47 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep47PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PEPA180.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep47PQLDSTW-LOC10-042419 04/24/2019 320-49620-7 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLDSTW-LOC10-042419 04/24/2019 320-49620-7 PEPA0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.047PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 MMF15.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLDSTW-LOC21A-042419 04/24/2019 320-49624-8 MMF15.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLDSTW-LOC6B-042419 04/24/2019 320-49624-2 MMF19.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLDSTW-LOC8-042419 04/24/2019 320-49620-5 DFSA4.8 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.1PQLDSTW-LOC8-042419 04/24/2019 320-49620-5 PFMOAA1.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLPage 31 of 37
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC17B-042419 04/24/2019 320-49624-4 PPF Acid48750 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep380PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PPF Acid49000.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep380PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 R-EVE1590 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep53PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 R-EVE1700.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep53PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 Byproduct 42410 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep120PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 Byproduct 42500.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep120PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 Byproduct 5330 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep44PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 Byproduct 5360.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep44PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 Byproduct 654 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep12PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 Byproduct 655.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep12PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PFESA-BP11445 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep20PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PFESA-BP11500.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep20PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PPF Acid353 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep280PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PPF Acid390.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep280PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 DFSA50100 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep2300PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 DFSA56000.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep2300PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PFMOAA160 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep160PQLPage 32 of 37
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC16-042419 04/24/2019 320-49624-3 PFMOAA170.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep160PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 EVE Acid787 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep18PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 EVE Acid820.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep18PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PFESA-BP2248 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep23PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PFESA-BP2250.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep23PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 Hydro-EVE Acid95 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep21PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 Hydro-EVE Acid99.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep21PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PMPA539 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep430PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PMPA600.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep430PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 NVHOS259 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep40PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 NVHOS270.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep40PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PFMOAA1770 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep210PQLDSTW-LOC17B-042419 04/24/2019 320-49624-4 PFMOAA2000.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep210PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PFO2HxA133 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep61PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PFO2HxA140.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep61PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PFO3OA44 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep44PQLDSTW-LOC16-042419 04/24/2019 320-49624-3 PFO3OA53.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep44PQLPage 33 of 37
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC17A-042419 04/24/2019 320-50472-1 PEPA110 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep47PQLDSTW-LOC17A-042419 04/24/2019 320-50472-1 PEPA110.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep47PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PFMOAA1.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PFMOAA1.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 EVE Acid0.065 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 EVE Acid0.063 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.024PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PFESA-BP20.14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PFESA-BP20.13 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 Hydro-EVE Acid0.032 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 Hydro-EVE Acid0.03 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.028PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PFESA-BP12.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PFESA-BP12.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PMPA0.70 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PMPA0.59 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 Byproduct 40.18 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 Byproduct 40.18 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 Byproduct 52.2 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 34 of 37
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-LOC23A-042419 04/24/2019 320-49624-10 Byproduct 52.1 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PFO2HxA0.48 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PFO2HxA0.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PFO3OA0.14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLDSTW-LOC23A-042419 04/24/2019 320-49624-10 PFO3OA0.14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 35 of 37
Associated LCS and/or LCSD analysis had relative percent recovery (RPR) values less than the lower control limit. The reported result may be biasedlow.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-FB-042419 04/24/2019 320-49620-10 PPF Acid0.72 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.38PQLDSTW-FB-042419 04/24/2019 320-49620-10 PPF Acid0.94 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.38PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 MTP0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLDSTW-LOC19A-042419 04/24/2019 320-49624-6 MTP0.13 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLDSTW-LOC19B-042419 04/24/2019 320-49624-7 MTP0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLDSTW-LOC19B-042419 04/24/2019 320-49624-7 MTP0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLDSTW-LOC24A-042419-D 04/24/2019 320-49624-12 MTP0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLDSTW-LOC24A-042419-D 04/24/2019 320-49624-12 MTP0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLDSTW-LOC22-042419 04/24/2019 320-49624-9 MTP0.14 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLDSTW-LOC22-042419 04/24/2019 320-49624-9 MTP0.14 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLDSTW-LOC6A-042419 04/24/2019 320-49624-1 MTP0.20 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLDSTW-LOC6A-042419 04/24/2019 320-49624-1 MTP0.22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.12PQLDSTW-LOC8-042419 04/24/2019 320-49620-5 PFMOAA1.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLPage 36 of 37
Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit but above the rejection limit. Thereported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Dry Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitDSTW-EB-03-042419 04/24/2019 320-49623-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.78 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.060PQLDSTW-EB-03-042419 04/24/2019 320-49623-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.86 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.060PQLDSTW-EB-02-042419 04/24/2019 320-49623-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.85 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.060PQLDSTW-EB-02-042419 04/24/2019 320-49623-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.82 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.060PQLDSTW-LOC22-042419 04/24/2019 320-49624-9 MMF7.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLDSTW-LOC22-042419 04/24/2019 320-49624-9 MMF6.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLDSTW-LOC24A-042419 04/24/2019 320-49624-11 MMF15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLDSTW-EB-01-042419 04/24/2019 320-49623-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.82 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.060PQLDSTW-EB-01-042419 04/24/2019 320-49623-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.82 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.060PQLDSTW-LOC6B-042419 04/24/2019 320-49624-2 MMF15 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep3.6PQLPage 37 of 37
ADQM Data Review Narrative - FAY 2019 Stormwater Samp.doc 1 of 2
ADQM DATA REVIEW NARRATIVE
Site Chemours FAY – Fayetteville Project 2019 Stormwater Sampling Project Reviewer Michael Aucoin, AECOM as a Chemours contractor Sampling Dates June 27 - 28, 2019 Analytical Protocol Laboratory Analytical Method Parameter(s)
TestAmerica - Sacramento 537 Modified PFAS1
TestAmerica - Sacramento Cl. Spec. Table 3 Compound SOP Table 3+ compounds

1 Perfluoroalkylsubstances, a list of 33 compounds including HFPO-DA. Sample Receipt
The following items are noted for this data set:
• All samples were received in satisfactory condition and within EPA temperature guidelines on July 2, 11, and 16, 2019. Data Review The electronic data submitted for this project was reviewed via the Data Verification Module (DVM) process. Overall the data is acceptable for use without qualification, except as noted below:
• Several analytical results have been qualified J as estimated, and non-detect results qualified UJ indicating an estimated reporting limit, due to poor or very poor recovery of a surrogate or laboratory blank spike; sample analysis which exceeded the laboratory hold time; and poor field duplicate or lab replicate precision. See the Data Verification Module (DVM) Narrative Report for which samples were qualified, the specific reasons for qualification, and potential bias in reported results. Attachments The DVM Narrative report is attached. The lab reports due to a large page count are stored on an AECOM network shared drive and are available to be posted on external shared drives, or on a flash drive.
ADQM Data Review Narrative - FAY 2019 Stormwater Samp.doc 2 of 2
Data Verification Module (DVM)
The DVM is an internal review process used by the ADQM group to assist with the determination of data usability. The electronic data deliverables received from the laboratory are loaded into the Locus EIM™ database and processed through a series of data quality checks, which are a combination of software (Locus EIM™ database Data Verification Module (DVM)) and manual reviewer evaluations. The data is evaluated against the following data usability checks:
• Field and laboratory blank contamination
• US EPA hold time criteria
• Missing Quality Control (QC) samples
• Matrix spike(MS)/matrix spike duplicate (MSD) recoveries and the relative percent differences
(RPDs) between these spikes
• Laboratory control sample(LCS)/control sample duplicate (LCSD) recoveries and the RPD
between these spikes
• Surrogate spike recoveries for organic analyses
• RPD between field duplicate sample pairs
• RPD between laboratory replicates for inorganic analyses
• Difference / percent difference between total and dissolved sample pairs. There are two qualifier fields in EIM: Lab Qualifier is the qualifier assigned by the lab and may not reflect the usability of the data. This qualifier may have many different meanings and can vary between labs and over time within the same lab. Please refer to the laboratory report for a description of the lab qualifiers. As they are lab descriptors they are not to be used when evaluating the data. Validation Qualifier is the 3rd party formal validation qualifier if this was performed. Otherwise this field contains the qualifier resulting from the ADQM DVM review process. This qualifier assesses the usability of the data and may not equal the lab qualifier. The DVM applies the following data
evaluation qualifiers to analysis results, as warranted: Qualifier Definition B Not detected substantially above the level reported in the laboratory or field blanks. R Unusable result. Analyte may or may not be present in the sample.
J Analyte present. Reported value may not be accurate or precise.
UJ Not detected. Reporting limit may not be accurate or precise.

The Validation Status Code field is set to “DVM” if the ADQM DVM process has been performed. If the DVM has not been run, the field will be blank.
If the DVM has been run (Validation Status Code equals “DVM”), use the Validation Qualifier.
DVM Narrative ReportOnly one surrogate has relative percent recovery (RPR) values outside control limits and the parameter is a PFC (Nondetects).LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSTW-LOC-18-062719 06/27/2019 320-51907-4 Perfluorooctadecanoicacid0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLSTW-LOC-18-062719 06/27/2019 320-51907-4 Perfluorohexadecanoicacid (PFHxDA)0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLSTW-LOC-19A-062719 06/27/2019 320-51907-5 6:2 Fluorotelomersulfonate0.020 ug/L537 ModifiedUJ3535_PFC0.020PQLSTW-LOC-19A-062719 06/27/2019 320-51907-5 PerfluorotetradecanoicAcid0.0020 UG/L537 ModifiedUJ3535_PFC0.0020PQLSTW-LOC-19A-062719 06/27/2019 320-51907-5 ADONA0.0021 UG/L537 ModifiedUJ3535_PFC0.0021PQLSTW-LOC-19A-062719 06/27/2019 320-51907-5 NaDONA0.0021 ug/L537 ModifiedUJ3535_PFC0.0021PQLSTW-LOC-22-062719 06/27/2019 320-51907-8 ADONA0.0021 UG/L537 ModifiedUJ3535_PFC0.0021PQLSTW-LOC-22-062719 06/27/2019 320-51907-8 NaDONA0.0021 ug/L537 ModifiedUJ3535_PFC0.0021PQLSTW-LOC-23B-062719 06/27/2019 320-51907-10 Perfluorooctadecanoicacid0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLSTW-LOC-23B-062719 06/27/2019 320-51907-10 PerfluorotetradecanoicAcid0.0020 UG/L537 ModifiedUJ3535_PFC0.0020PQLSTW-LOC-23B-062719 06/27/2019 320-51907-10 Perfluorohexadecanoicacid (PFHxDA)0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLPage 1 of 13
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSTW-LOC17A-062719 06/27/2019 320-52169-1 NVHOS54 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep54PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 PES46 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep46PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 PMPA570 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep570PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 PFECA B60 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep60PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol60 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep60PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol110 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep110PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 PEPA47 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep47PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 PFESA-BP127 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep27PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 N-methyl perfluoro-1-octanesulfonamide35 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep35PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 PFO2HxA81 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep81PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 PFO3OA58 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep58PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 PFO4DA79 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep79PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 PFO5DA34 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep34PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 PFMOAA210 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep210PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 EVE Acid24 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep24PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 PFESA-BP230 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep30PQLPage 2 of 13
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSTW-LOC17A-062719 06/27/2019 320-52169-1 Hydro-EVE Acid28 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep28PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 PFECA-G41 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep41PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 R-EVE70 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep70PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 Byproduct 4160 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep160PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 Byproduct 558 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep58PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 Byproduct 615 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep15PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 NVHOS21 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep21PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 PES18 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep18PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 PMPA230 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep230PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 PFECA B24 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep24PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol24 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep24PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol44 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep44PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 PFESA-BP111 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep11PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 N-methyl perfluoro-1-octanesulfonamide14 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep14PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 PFO2HxA32 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep32PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 PFO3OA23 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep23PQLPage 3 of 13
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSTW-LOC17B-062719 06/27/2019 320-52276-1 PFO4DA31 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep31PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 PFO5DA13 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep13PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 N-ethylperfluoro-1-octanesulfonamide15 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep15PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 PFMOAA85 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep85PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 EVE Acid9.7 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep9.7PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 PFESA-BP212 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep12PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 Hydro-EVE Acid11 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep11PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 PFECA-G16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep16PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 R-EVE28 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep28PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 Byproduct 463 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep63PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 Byproduct 523 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep23PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 Byproduct 66.2 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep6.2PQLPage 4 of 13
Associated LCS and/or LCSD analysis had relative percent recovery (RPR) values less than the lower control limit but above 10%. The actual detectionlimits may be higher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSTW-LOC-18-062719 06/27/2019 320-51907-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLSTW-LOC-18-062719 06/27/2019 320-51907-4 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLSTW-LOC-19A-062719 06/27/2019 320-51907-5 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLSTW-LOC-19A-062719 06/27/2019 320-51907-5 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLSTW-LOC-19B-062719 06/27/2019 320-51907-6 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLSTW-LOC-19B-062719 06/27/2019 320-51907-6 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLSTW-LOC-21A-062719 06/27/2019 320-51907-7 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLSTW-LOC-21A-062719 06/27/2019 320-51907-7 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLSTW-LOC-22-062719 06/27/2019 320-51907-8 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLSTW-LOC-22-062719 06/27/2019 320-51907-8 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLSTW-LOC-23A-062719 06/27/2019 320-51907-9 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLSTW-LOC-23A-062719 06/27/2019 320-51907-9 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLSTW-LOC-24A-062719 06/27/2019 320-51907-11 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLSTW-LOC-24A-062719 06/27/2019 320-51907-11 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLSTW-LOC-24A-062719-D 06/27/2019 320-51907-12 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLSTW-LOC-24A-062719-D 06/27/2019 320-51907-12 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLPage 5 of 13
Associated LCS and/or LCSD analysis had relative percent recovery (RPR) values less than the lower control limit but above 10%. The actual detectionlimits may be higher than reported.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSTW-LOC-6A-062719 06/27/2019 320-51907-1 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLSTW-LOC-6A-062719 06/27/2019 320-51907-1 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLSTW-LOC-6B-062719 06/27/2019 320-51907-2 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLSTW-LOC-6B-062719 06/27/2019 320-51907-2 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLPage 6 of 13
One or more surrogates had relative percent recovery (RPR) values less than the data rejection level. The reporting limit is consid-ered to be an estimated value.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSTW-LOC-19A-062719 06/27/2019 320-51907-5 Perfluorooctadecanoicacid0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLSTW-LOC-19A-062719 06/27/2019 320-51907-5 Perfluorohexadecanoicacid (PFHxDA)0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLSTW-LOC-19B-062719 06/27/2019 320-51907-6 Perfluorooctadecanoicacid0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLSTW-LOC-19B-062719 06/27/2019 320-51907-6 Perfluorohexadecanoicacid (PFHxDA)0.0020 ug/L537 ModifiedUJ3535_PFC0.0020PQLPage 7 of 13
High relative percent difference (RPD) observed between field duplicate and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSTW-LOC-24A-062719 06/27/2019 320-51907-11 PFOS0.017 UG/L537 ModifiedJ3535_PFC0.0020PQLSTW-LOC-24A-062719 06/27/2019 320-51907-11 PFOA0.0088 UG/L537 ModifiedJ3535_PFC0.0020PQLSTW-LOC-24A-062719-D 06/27/2019 320-51907-12 PFOS0.03 UG/L537 ModifiedJ3535_PFC0.0020PQLSTW-LOC-24A-062719-D 06/27/2019 320-51907-12 PFOA0.011 UG/L537 ModifiedJ3535_PFC0.0020PQLPage 8 of 13
Only one surrogate has relative percent recovery (RPR) values outside control limits and the parameter is a PFC (Detects).LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSTW-LOC-23B-062719 06/27/2019 320-51907-10 6:2 Fluorotelomersulfonate0.02 ug/L537 ModifiedJ3535_PFC0.020PQLSTW-LOC-22-062719 06/27/2019 320-51907-8 Hfpo Dimer Acid0.13 UG/L537 ModifiedJ3535_PFC0.0040PQLSTW-LOC-22-062719 06/27/2019 320-51907-8 PerfluorohexanoicAcid0.021 UG/L537 ModifiedJ3535_PFC0.0020PQLSTW-LOC-19A-062719 06/27/2019 320-51907-5 PerfluorohexanoicAcid0.0061 UG/L537 ModifiedJ3535_PFC0.0020PQLSTW-LOC-19A-062719 06/27/2019 320-51907-5 PFOA0.0031 UG/L537 ModifiedJ3535_PFC0.0020PQLSTW-LOC-19A-062719 06/27/2019 320-51907-5 Perfluorobutanoic Acid0.0024 UG/L537 ModifiedJ3535_PFC0.0020PQLSTW-LOC-19A-062719 06/27/2019 320-51907-5 PerfluoroheptanoicAcid0.0033 UG/L537 ModifiedJ3535_PFC0.0020PQLSTW-LOC-19A-062719 06/27/2019 320-51907-5 Hfpo Dimer Acid0.0045 UG/L537 ModifiedJ3535_PFC0.0040PQLPage 9 of 13
Quality review criteria exceeded between the REP (laboratory replicate) and parent sample. The reported result may be imprecise.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSTW-LOC-16-062819 06/28/2019 320-51907-3 PFO5DA14.0 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.34PQLSTW-LOC-22-062719 06/27/2019 320-51907-8 PFESA-BP20.13 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLSTW-LOC-22-062719 06/27/2019 320-51907-8 PFESA-BP20.15 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLPage 10 of 13
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSTW-LOC17B-062719 06/27/2019 320-52276-1 Hfpo Dimer Acid (trial) 370000.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep34PQLSTW-LOC17B-062719 06/27/2019 320-52276-1 PEPA66.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep19PQLSTW-LOC17A-062719 06/27/2019 320-52169-1 N-ethylperfluoro-1-octanesulfonamide52.0 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep37PQLPage 11 of 13
Associated LCS and/or LCSD analysis had relative percent recovery (RPR) values less than the lower control limit. The reported result may be biasedlow.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSTW-LOC-23B-062719 06/27/2019 320-51907-10 PFO5DA0.098 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLSTW-LOC-23B-062719 06/27/2019 320-51907-10 PFO5DA0.082 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLSTW-LOC-16-062819 06/28/2019 320-51907-3 PFO5DA11 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.34PQLPage 12 of 13
One or more surrogates had relative percent recovery (RPR) values less than the data rejection level. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:Sampling2019 Stormwater SamplingAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitSTW-LOC-22-062719 06/27/2019 320-51907-8 Perfluorobutanoic Acid0.037 UG/L537 ModifiedJ3535_PFC0.0035PQLPage 13 of 13
ADQM Data Review Narrative - FAY Additional Outfall Samples.doc 1 of 2
ADQM DATA REVIEW NARRATIVE
Site Chemours FAY – Fayetteville Project Additional Outfall Samples Project Reviewer Michael Aucoin, AECOM as a Chemours contractor Sampling Dates May 30, 2019 Analytical Protocol Laboratory Analytical Method Parameter(s)
TestAmerica - Sacramento Cl. Spec. Table 3 Compound SOP Table 3+ compounds

Sample Receipt The following items are noted for this data set:

• All samples were received in satisfactory condition and within EPA temperature guidelines on June 1, 2019.
Data Review The electronic data submitted for this project was reviewed via the Data Verification Module (DVM)
process. Overall the data is acceptable for use without qualification, except as noted below:

• All of the Table 3+ analytical results have been qualified J as estimated, and non-detect results qualified UJ indicating an estimated reporting limit, due to analysis which exceeded the laboratory established hold time. The result for Byproduct 5 in one sample was qualified J, and may be biased high, due to an MS RPR that exceeded criteria. See the Data Verification Module
(DVM) Narrative Report for which samples were qualified, the specific reasons for qualification, and potential bias in reported results.
Attachments The DVM Narrative report is attached. The lab report due to a large page count is stored on an AECOMnetwork shared drive and is available to be posted on external shared drives, or on a flash drive.

ADQM Data Review Narrative - FAY Additional Outfall Samples.doc 2 of 2
Data Verification Module (DVM)
The DVM is an internal review process used by the ADQM group to assist with the determination of data usability. The electronic data deliverables received from the laboratory are loaded into the Locus EIM™ database and processed through a series of data quality checks, which are a combination of software (Locus EIM™ database Data Verification Module (DVM)) and manual reviewer evaluations. The data is evaluated against the following data usability checks:
• Field and laboratory blank contamination
• US EPA hold time criteria
• Missing Quality Control (QC) samples
• Matrix spike(MS)/matrix spike duplicate (MSD) recoveries and the relative percent differences
(RPDs) between these spikes
• Laboratory control sample(LCS)/control sample duplicate (LCSD) recoveries and the RPD
between these spikes
• Surrogate spike recoveries for organic analyses
• RPD between field duplicate sample pairs
• RPD between laboratory replicates for inorganic analyses
• Difference / percent difference between total and dissolved sample pairs. There are two qualifier fields in EIM: Lab Qualifier is the qualifier assigned by the lab and may not reflect the usability of the data. This qualifier may have many different meanings and can vary between labs and over time within the same lab. Please refer to the laboratory report for a description of the lab qualifiers. As they are lab descriptors they are not to be used when evaluating the data. Validation Qualifier is the 3rd party formal validation qualifier if this was performed. Otherwise this field contains the qualifier resulting from the ADQM DVM review process. This qualifier assesses the usability of the data and may not equal the lab qualifier. The DVM applies the following data
evaluation qualifiers to analysis results, as warranted: Qualifier Definition B Not detected substantially above the level reported in the laboratory or field blanks. R Unusable result. Analyte may or may not be present in the sample.
J Analyte present. Reported value may not be accurate or precise.
UJ Not detected. Reporting limit may not be accurate or precise.

The Validation Status Code field is set to “DVM” if the ADQM DVM process has been performed. If the DVM has not been run, the field will be blank.
If the DVM has been run (Validation Status Code equals “DVM”), use the Validation Qualifier.
DVM Narrative ReportThe analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingAdditional Outfall SamplesAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitEB3-05301905/30/2019 280-124597-5 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLEB3-05301905/30/2019 280-124597-5 NVHOS0.054 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.054PQLEB3-05301905/30/2019 280-124597-5 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLEB3-05301905/30/2019 280-124597-5 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLEB3-05301905/30/2019 280-124597-5 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLEB3-05301905/30/2019 280-124597-5 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLEB3-05301905/30/2019 280-124597-5 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLEB3-05301905/30/2019 280-124597-5 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLEB3-05301905/30/2019 280-124597-5 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLEB3-05301905/30/2019 280-124597-5 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLEB3-05301905/30/2019 280-124597-5 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLEB3-05301905/30/2019 280-124597-5 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLEB3-05301905/30/2019 280-124597-5 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLEB3-05301905/30/2019 280-124597-5 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLPage 1 of 19
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingAdditional Outfall SamplesAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitEB3-05301905/30/2019 280-124597-5 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLEB3-05301905/30/2019 280-124597-5 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLEB3-05301905/30/2019 280-124597-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLEB3-05301905/30/2019 280-124597-5 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLEB3-05301905/30/2019 280-124597-5 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLEB3-05301905/30/2019 280-124597-5 PFO2HxA0.081 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.081PQLEB3-05301905/30/2019 280-124597-5 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLEB3-05301905/30/2019 280-124597-5 PFO3OA0.058 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLEB3-05301905/30/2019 280-124597-5 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLEB3-05301905/30/2019 280-124597-5 PFO4DA0.079 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.079PQLEB3-05301905/30/2019 280-124597-5 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLEB3-05301905/30/2019 280-124597-5 PFO5DA0.034 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.034PQLEB3-05301905/30/2019 280-124597-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLEB3-05301905/30/2019 280-124597-5 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLEB3-05301905/30/2019 280-124597-5 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLEB3-05301905/30/2019 280-124597-5 PFMOAA0.21 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.21PQLEB3-05301905/30/2019 280-124597-5 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLPage 2 of 19
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingAdditional Outfall SamplesAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitEB3-05301905/30/2019 280-124597-5 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLEB3-05301905/30/2019 280-124597-5 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLEB3-05301905/30/2019 280-124597-5 PFESA-BP20.030 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.030PQLEB3-05301905/30/2019 280-124597-5 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLEB3-05301905/30/2019 280-124597-5 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLEB3-05301905/30/2019 280-124597-5 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLEB3-05301905/30/2019 280-124597-5 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLEB3-05301905/30/2019 280-124597-5 Hfpo Dimer Acid (trial)0.086 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.086PQLEB3-05301905/30/2019 280-124597-5 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLEB3-05301905/30/2019 280-124597-5 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLEB3-05301905/30/2019 280-124597-5 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLEB3-05301905/30/2019 280-124597-5 Byproduct 40.16 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.16PQLEB3-05301905/30/2019 280-124597-5 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLEB3-05301905/30/2019 280-124597-5 Byproduct 50.058 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.058PQLEB3-05301905/30/2019 280-124597-5 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLEB3-05301905/30/2019 280-124597-5 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLPage 3 of 19
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingAdditional Outfall SamplesAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLPage 4 of 19
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingAdditional Outfall SamplesAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLPage 5 of 19
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingAdditional Outfall SamplesAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-20B-053019 05/30/2019 280-124597-2 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLPage 6 of 19
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingAdditional Outfall SamplesAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-20B-053019 05/30/2019 280-124597-2 Hfpo Dimer Acid (trial)0.086 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.086PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLPage 7 of 19
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingAdditional Outfall SamplesAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-20C-053019 05/30/2019 280-124597-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 Hfpo Dimer Acid (trial)0.086 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.086PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLPage 8 of 19
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingAdditional Outfall SamplesAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-20D-053019 05/30/2019 280-124597-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLPage 9 of 19
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingAdditional Outfall SamplesAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-20D-053019 05/30/2019 280-124597-4 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 Hfpo Dimer Acid (trial)0.086 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.086PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.070PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PES0.046 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.046PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.57PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PFECA B0.060 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 2-(N-ethyl perfluoro-1-octanesulfonamido)-ethanol0.060 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.060PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 2-(N-methyl perfluoro-1-octanesulfonamido)-ethanol0.11 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.11PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 2-(N-methyl perfluoro-1-0.11 ug/LCl. Spec. Table 3CompoundUJPFAS_DI_Prep0.11PQLPage 10 of 19
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingAdditional Outfall SamplesAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitoctanesulfonamido)-ethanolSOPFAY-SW-DUP-053019 05/30/2019 280-124597-7 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PEPA0.047 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.047PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.027PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 N-methyl perfluoro-1-octanesulfonamide0.035 ug/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.035PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 N-ethylperfluoro-1-octanesulfonamide0.037 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.037PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 EVE Acid0.024 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.024PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 Hydro-EVE Acid0.028 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.028PQLPage 11 of 19
The analysis hold time for this sample was exceeded. The reporting limit may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingAdditional Outfall SamplesAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-DUP-053019 05/30/2019 280-124597-7 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PFECA-G0.041 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.041PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 Byproduct 60.015 UG/LCl. Spec. Table 3Compound SOPUJPFAS_DI_Prep0.015PQLPage 12 of 19
Associated MS and/or MSD analysis had relative percent recovery (RPR) values higher than the upper control limit. The reported result may be biasedhigh.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingAdditional Outfall SamplesAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 Byproduct 51.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 Byproduct 51.4 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 13 of 19
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingAdditional Outfall SamplesAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-DUP-053019 05/30/2019 280-124597-7 Hfpo Dimer Acid (trial)0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.086PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 R-EVE0.070 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 R-EVE0.087 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.070PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 Byproduct 40.28 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 Byproduct 40.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 Byproduct 51.5 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 Byproduct 51.6 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PFESA-BP20.20 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PFESA-BP20.21 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PFMOAA2.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PFMOAA2.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 NVHOS0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 NVHOS0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PFESA-BP20.21 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PFESA-BP20.21 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PFO2HxA0.68 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PFO2HxA0.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLPage 14 of 19
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingAdditional Outfall SamplesAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-DUP-053019 05/30/2019 280-124597-7 PFO3OA0.32 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PFO3OA0.33 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PFO4DA0.22 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PFO4DA0.24 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PFO5DA0.14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-DUP-053019 05/30/2019 280-124597-7 PFO5DA0.14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 Byproduct 40.24 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 Byproduct 40.26 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 Byproduct 51.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 Byproduct 51.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PFMOAA2.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PFMOAA2.7 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 NVHOS0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 NVHOS0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PFO2HxA0.66 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PFO2HxA0.66 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PFO3OA0.32 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLPage 15 of 19
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingAdditional Outfall SamplesAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-20D-053019 05/30/2019 280-124597-4 PFO3OA0.32 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PFO4DA0.23 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PFO4DA0.24 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PFO5DA0.15 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PFO5DA0.15 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PFESA-BP10.032 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-20D-053019 05/30/2019 280-124597-4 PFESA-BP10.036 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 Byproduct 40.22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 Byproduct 40.23 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 Byproduct 51.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 Byproduct 51.7 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PFESA-BP20.21 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PFESA-BP20.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PFMOAA2.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PFMOAA2.8 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PFO2HxA0.68 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PFO2HxA0.67 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLPage 16 of 19
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingAdditional Outfall SamplesAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-20C-053019 05/30/2019 280-124597-1 PFO3OA0.34 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PFO3OA0.34 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PFO4DA0.25 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PFO4DA0.26 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PFO5DA0.16 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PFO5DA0.16 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PFESA-BP10.036 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PFESA-BP10.04 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PMPA0.57 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 PMPA0.66 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 NVHOS0.14 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-20C-053019 05/30/2019 280-124597-1 NVHOS0.12 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 Byproduct 40.21 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 Byproduct 40.22 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 Byproduct 51.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 Byproduct 51.3 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PFESA-BP20.20 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLPage 17 of 19
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingAdditional Outfall SamplesAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-SW-20B-053019 05/30/2019 280-124597-2 PFESA-BP20.19 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PFMOAA2.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PFMOAA2.4 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 NVHOS0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 NVHOS0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 Byproduct 40.23 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 Byproduct 40.28 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.16PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PFO2HxA0.64 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PFO2HxA0.66 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PFO3OA0.30 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PFO3OA0.29 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PFO4DA0.22 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PFO4DA0.23 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PFO5DA0.14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-SW-20B-053019 05/30/2019 280-124597-2 PFO5DA0.14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 Hfpo Dimer Acid (trial)0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.086PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PFESA-BP20.19 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLPage 18 of 19
The analysis hold time for this sample was exceeded. The reported result may be biased low.LABSTATSValidationValidation ReasonFayettevilleSite:SamplingAdditional Outfall SamplesAnalyticalMethodAnalyteDateSamplePQLValidationLab SamplePre-prepMDLResult TypField Sample IDPrepUnitFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PFESA-BP20.2 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.030PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PFMOAA2.5 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PFMOAA2.6 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.21PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PMPA0.64 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PMPA0.67 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.57PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PFO2HxA0.64 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PFO2HxA0.62 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.081PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PFO3OA0.32 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PFO3OA0.3 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.058PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PFO4DA0.22 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PFO4DA0.21 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.079PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PFO5DA0.14 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PFO5DA0.13 ug/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.034PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PFESA-BP10.030 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 PFESA-BP10.027 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.027PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 NVHOS0.10 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLFAY-DSTW-OUTFALL002-05301905/30/2019 280-124597-3 NVHOS0.11 UG/LCl. Spec. Table 3Compound SOPJPFAS_DI_Prep0.054PQLPage 19 of 19

DECOMMISSIONING SUMMARY OF
GROUTING OF EAST-WEST SECTION
OF TERRACOTTA PIPE FROM
CHEMOURS MONOMERS IXM AREA

Chemours Fayetteville Works, NC

Prepared for
The Chemours Company
1007 Market Street
PO Box 2047
Wilmington, DE 19899
Prepared by
Geosyntec Consultants of NC, P.C.
2501 Blue Ridge Road, Suite 430
Raleigh, NC 27607
Geosyntec Project Number TR0795
August 2019

i 2019.08.26
TABLE OF CONTENTS
1. INTRODUCTION AND OBJECTIVES .............................................................. 1
2. TERRACOTTA PIPE GROUTING ACTIVITIES .............................................. 2
3. SUMMARY .......................................................................................................... 2
4. REFERENCES ..................................................................................................... 3

ii 2019.08.26
LIST OF FIGURES
Figure 1: Terracotta Pipe Location
Figure 2: Terracotta Grouted Pipe Section and Manhole Locations

ACRONYMS AND ABBREVIATIONS
% Percent
Chemours The Chemours Company FC, LLC
Geosyntec Geosyntec Consultants of NC, P.C.
IXM Ion Exchange Membrane
Kuraray Kuraray America Inc.
PFAS per- and polyfluoroalkyl substances
the Site Chemours Fayetteville Works Facility
WWTP Wastewater treatment plant

TR0795 1 2019.08.26
1. INTRODUCTION AND OBJECTIVES
Geosyntec Consultants of NC, P.C. (Geosyntec) has prepared this memorandum for The
Chemours Company FC, LLC (Chemours) to summarize grouting performed by G.A.
West & Co., Inc. and supervised by Chemours of the east-west section of the terracotta
pipe that originates in the Chemours Monomers Ion Exchange Membrane (IXM) Area at
the Chemours Fayetteville Works Site (the Site) that occurred in February 2019. This
grouting represents continued action by Chemours to mitigate the potential for PFAS
originating from the terracotta pipe to be transmitted to the Cape Fear River via transit
through the pipe to the Wastewater Treatment Plant (WWTP) and then to Outfall 002.
Chemours intends by Fall 2021 to fully decommission the terracotta pipe and transmit
existing flows through the terracotta pipe to the Wastewater Treatment Plant using new,
aboveground piping.
The terracotta pipe was designed to convey wastewaters from the various manufacturing
areas on the Site to the wastewater treatment plant (WWTP) (Figure 1). The table below
summarizes inputs of wastewaters transmitted via the terracotta pipe.

Wastewater Contributions to Terracotta Pipe Contribution Status
Kuraray SentryGlas® Process Wastewater Active
Kuraray Laboratory Wastewater Active
Kuraray Trosifol® Process Wastewater Active
Site Demineralized Water Production Wastewater Active
Chemours Monomers IXM Process Wastewater Discontinued Nov-2017

The two Kuraray America, Inc. (Kuraray) Areas, SentryGlas® and Trosifol®, and the
Site demineralized water production operations located in the “Power” Area actively
transmit water to the WWTP via the terracotta pipe. Neither Kuraray or the water
production activities use or produce per- and polyfluoroalkyl substances (PFAS). Prior to
June 21, 2017 Chemours transmitted PFAS containing process wastewater to the WWTP
from the “Monomers IXM Area” via the terracotta pipe. Between June 21, 2017 and
November 29, 2017 Chemours diverted all process wastewater flows from the Chemours
Monomers IXM Area from the WWTP and presently sends them for offsite disposal. On
November 29, 2017 Chemours severed the terracotta pipe connection from the Chemours
Monomers IXM Area to prevent the potential for aqueous process wastewater to be
conveyed by the terracotta pipe. While there have been no known contributions of process
water from the Monomers IXM Area transmitted to the WWTP via the terracotta pipe

TR0795 2 2019.08.26
since November 29, 2017, there was the possibility that perched groundwater could enter
the east-west section of the terracotta pipe after heavy rain events (Parsons, 2018). Heavy
rain events could lead to groundwater levels higher than the bottom of the terracotta pipe
near Monomers IXM. This water could then be transmitted to the WWTP and Outfall 002
and the Cape Fear River. To mitigate this possibility Chemours grouted the presently
unused east-west section of the terracotta pipe that formerly connected the Monomers
IXM Area with the main north-south running section of the terracotta pipe. This grouted
portion of the pipe (Figure 1), is referred to as the “east-west” section of the terracotta
pipe.
2. TERRACOTTA PIPE GROUTING ACTIVITIES
The east-west portion of the terracotta pipe was grouted by G.A. West & Co., Inc. during
the week of February 21, 2019, with oversight by Chemours. Forty (40) cubic yards of
flowable fill grout (a mixture of cement, sand and water) were applied under gravity to
fill sections of the east-west portion of the terracotta pipe and associated manholes. Pipe
vents were installed to vent trapped air and were also used as observation points.
There were eight manholes along the east-west section of terracotta pipe from Chemours
Monomers IXM Area. These manholes and the connecting pipe sections between them
have been fully grouted (Figure 2). Manholes were used as access points for grouting the
pipe. After the pipe sections were filled with grout, the continual addition of grout filled
in the manholes. Figure 2 shows photographs of the manholes post grouting. Therefore,
this section of the terracotta pipe is expected to be unable to either receive or transmit any
type of water (e.g. groundwater, stormwater, process water, etc.,). The section of pipe
between Manhole 8 and Manhole 9 had approximately 70 percent (%) of its volume
grouted. Kuraray process waters flow through Manhole 9, and consequently this manhole
was not filled with grout. The grouting activities mitigate and are intended to prevent
transmission of any waters through this section of the terracotta pipe, including waters
from upstream pipe or any potentially infiltrating stormwater or groundwater.
3. SUMMARY
In summary, the February 2019 grouting of the east-west section of the terracotta pipe
that formerly conveyed process wastewater from the Chemours Monomers IXM Area
mitigates the possibility of either groundwater or stormwater entering this section of the
pipe and being transmitted to the WWTP and subsequently Outfall 002 and the Cape Fear
River. This action represents continued action by Chemours to mitigate potential
contributions of PFAS to the WWTP and ultimately through outfall 002 and into the Cape
Fear River via the terracotta pipe. By Fall 2021 Chemours intends to fully decommission

TR0795 3 2019.08.26
remaining terracotta pipe sections connected to the WWTP. The present flows through
the terracotta pipe to the WWTP (flows from Kuraray and Power) will be transmitted
through new aboveground piping.
4. REFERENCES
Terracotta Sewer Pipe Area Investigation Report, Parsons, December 2018.

FIGURES
Chemours Monomers
IXM Area
Kuraray Trosifol®
Manufacturing Operations
Wastewater Treatment Plant
Power - Filtered and
Demineralized
Water Production
Kuraray SentryGlas®
Manufacturing Operations
Kuraray Laboratory
Terracotta Pipe Location
Chemours Fayetteville Works, North Carolina
Figure
1Raleigh
500 0 500250 Feet
³
August 2019
Projection: NAD 1983 StatePlane North Carolina FIPS 3200 Feet; Units in Foot US
Legend
Pipe Connection to Facility
Terracotta Pipe and PipingConnected to Terracotta Pipe
Grouted Pipe Section
!?
!?
!?
!?!?!?
!?
!?
!?
MH #6
MH #1
MH #2
MH #3
MH #4MH #5
MH #7
MH #8
MH #9
Terracotta Gouted Pipe Section and Manhole Locations
Chemours Fayetteville Works, North Carolina
Figure
2Raleigh
200 0 200100 Feet
³
August 2019
Projection: WGS 1984 Web Mercator Auxiliary Sphere; Units in Meter
Legend
!?Manhole (MH)
Pipe Connection to Facility
Terracotta Pipe and Piping
Connected to Terracotta Pipe
Grouted Pipe Section
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Reduction Plan Attachment 5 HFPO-DA Loadings Reductions Estimate
1 August 2019
ATTACHMENT 5
HFPO-DA LOADING REDUCTIONS ESTIMATE
This document presents an analysis supporting the Cape Fear River PFAS Loading
Reduction Plan (the Reduction Plan). This assessment was completed to understand the
range of HFPO-DA loading reductions achieved since June 2017. Specifically, this
document presents estimates of the following reductions in PFAS loading:
 HFPO-DA loading reductions to Outfall 002;
 HFPO-DA loading reductions to the Cape Fear River; and
 HFPO-DA loading reductions to the environment.
HFPO-DA Loading Reductions to Outfall 002
Actions taken by Chemours reduced HFPO-DA loading to Outfall 002 by over 99%
throughout 2018 when compared to pre-June and mid-June 2017. This assessment was
performed by calculating the mass loading at Outfall 002 for June 14 and 15, 2017. At
that time Chemours had not yet begun diverting process wastewater from the Monomers
IXM Area away from the Wastewater Treatment Plant (WWTP) whereupon they were
discharged to Outfall 002. These samples are used as an approximation of pre-June 2017
loadings. The reported concentration of HFPO-DA from these two samples (80,000 and
44,000 nanograms per liter [ng/L] respectively) were then combined with the Outfall 002
flow rates on these dates, 22.12 and 24.255 million gallons per day (MGD). These daily
mass loading rates were then prorated to provide estimates of pre-June 2017 potential
yearly mass loadings of 3,251 to 5,390 pounds per year (lbs/yr; values not rounded to
preserve calculation accuracy).
The estimated pre-June 2017 yearly mass loadings were then combined with the
estimated 2018 HFPO-DA load of 12.7 lbs (equivalent to 12.7 lbs/yr) presented in the
“Outfall 002 Assessment” – Assessment of HFPO-DA and PFMOAA in Outfall 002
Discharge and Evaluation of Potential Control Options (Attachment 3). The calculated
reduction in loadings for 2018 compared to mid-June and pre-June 2017 were 99.6% and
99.8% (Table 1).

Reduction Plan Attachment 5 HFPO-DA Loadings Reductions Estimate
2 August 2019

Table 1: Calculated Pre-June 2017 to 2019 Outfall 002 HFPO-DA Loading Reductions
Location
Chemours Fayetteville Works
Outfall 002
Date 6/14/2017 6/15/2017
Laboratory TA TA
HFPO-DA (ng/L) 80,000 44,000
Outfall 002 Discharge Rate (MGD) 22.1 24.3
Outfall 002 Discharge (L/s) 969 1,063
Outfall 002 Mass Loading (mg/s) 78 47
Prorated Estimate of pre-June 2017
Outfall 002 HFPO-DA Loading (lbs/yr) 5,390 3,251
Estimated 2018 HFPO-DA
Outfall 002 Load 12.7 12.7
Calculated Percent Reduction in
HFPO-DA Loading Pre-June 2017 to 2019 99.8% 99.6%
- Outfall 002 flow rates were provided by the Fayetteville Works Site (22.12 and 24.255 million gallons
per day - MGD).
lbs/yr – pounds per year MGD – Million Gallons per Day
L/s – Liters per Second ng/L – nanograms per liter
mg/s – milligrams per second TA - TestAmerica Laboratories, Inc.

Reduction Plan Attachment 5 HFPO-DA Loadings Reductions Estimate
3 August 2019
HFPO-DA Loading Reductions to the Cape Fear River
Actions taken by Chemours have reduced HFPO-DA loading reductions to the Cape Fear
River by over 95% by 2019 compared to pre-June and mid-June 2017. This assessment
was performed by first estimating 2019 Cape Fear River HFPO-DA mass loading and
then comparing the highest estimated 2019 HFPO-DA Cape Fear River mid-June and
pre-June 2017 HFPO-DA Cape Fear River loadings.
The Cape Fear River 2019 HFPO-DA load was calculated by combining HFPO-DA
concentrations reported in the Seeps and Creeks Investigation Report (Attachment 2) with
Cape Fear River discharge rates reported at two USGS flow gauging stations. These
estimates, presented in Table 2, estimated that the observed loads in the Cape Fear River
during the Seeps and Creeks Investigation ranged from between 64 and 129 (lbs/yr) on a
prorated basis. The 129 (lbs/yr) value was advanced for calculating the estimated
reductions since June 2017.
Table 2: 2019 Calculated Cape Fear River HFPO-DA Loading Reductions
Location Bladen Bluffs1 Kings Bluff2
Sample Date 5/22/2019 6/7/2019 5/23/2019 6/7/2019
HFPO-DA (ng/L) 28 57 17 37
River Discharge (cfs) 1,820 1,150 1,920 1,360
River Discharge (L/s) 51,537 32,564 54,368 38,511
Mass Loading (mg/s) 1.44 1.86 0.92 1.42
Prorated Estimate of 2019
HFPO-DA Loading (lbs/yr) 100 129 64 99
1 - To account for the approximate 1 day of travel time between the W.O. Huske Dam (USGS Station No. 02105500) and Bladen Bluffs the mean discharge rates from May 21, 2019 and June 6, 2019 were used. 2 - The mean discharge rate from the Cape Fear Lock and Dam Number 1 (USGS Station No. 02105769) on the same date the location was sampled was used for Kings Bluff calculations. cfs - Cubic Feet Per Second mg/s - Miligrams per Second L/s - Liters per Second ng/L – Nanogram per Liter lbs/yr - Pounds per Year To estimate HFPO-DA loading reductions since mid-June 2017 and pre-June 2017
publicly available HFPO-DA concentrations in the river reported by the North Carolina
Department of Environmental Quality (NCDEQ) and Brunswick County sampled
between June 14 - 22, 2017 were combined with Cape Fear River discharge values as
measured by the USGS flow gauging station at Lock and Dam Number 1 on the Cape
Fear River. The prorated loads ranged from 3,147 to 14,336 (lbs/yr; Table 3). Comparing
these values to the maximum 129 lbs/yr estimated for 2019 yielded HFPO-DA Cape Fear
River loading reductions estimated to be between 95.9% and 99.1
Reduction Plan Attachment 5 HFPO-DA Loadings Reductions Estimate 4 August 2019 Table 3: Calculated Pre-June 2017 to 2019 Cape Fear River HFPO-DA Loading Reductions -Non-Outfall 002 HFPO-DA data taken from publicly accessible websites https://www.ncwater.org/basins/Cape_Fear/GenXDataspreadsheet.pdf and http://www.brunswickcountync.gov/genx/. - Flow rates used were the mean flow rates at Cape Fear Lock and Dam Number 1 (USGS Station No. 02105769) on the same date the location was sampled. Kings Bluff Intake Canal is immediately upstream of this USGS Station. - Outfall 002 flow rates were provided by the Fayetteville Works Site (22.12 and 24.255 million gallons per day - MGD). EPA - RTP NC - United States Environmental Protection Agency, Research Triangle Park, North Carolina TA - TestAmerica Laboratories, Inc. cfs - Cubic Feet Per Second L/s - Liters per Second lbs/yr - Pounds per Year mg/s - Miligrams per Second ng/L – Nanogram per LiteLocationDate6/22/2017 6/22/2017 6/22/2017 6/22/2017 6/19/2017 6/19/2017 6/14/20176/15/2017LaboratoryEPA RTP NCTAEPA RTP NCTAEPA RTP NCTA TA TAHFPO-DA (ng/L)726 1,100 629 830 695 910 80,000 44,000 River / Outfall 002 Discharge (cfs)6,620 6,620 6,620 6,620 2,300 2,300 34 38 River / Outfall 002 Discharge (L/s)187,457 187,457 187,457 187,457 65,129 65,129 969 1,063 Mass Loading (mg/s)136 206 118 156 45 59 78 47 Prorated Estimate of pre-June 2017 HFPO-DA Loading (lbs/yr)9,462 14,336 8,198 10,817 3,147 4,121 5,390 3,251 Maximum Estimated Prorated2019 HFPO-DA Loading (lbs/yr)129 129 129 129 129 129 129 129 Calculated Percent Reduction in HFPO-DA Loading Pre-June 2017 to 201998.6% 99.1% 98.4% 98.8% 95.9% 96.9% 97.6% 96.0%CFPUA Sweeney FinishedKings Bluff IntakeRaw WaterWater Treatment Plant FinishedChemours Fayetteville Works Outfall 002
Reduction Plan Attachment 5
HFPO-DA Loadings Reductions Estimate
5 August 2019

HFPO-DA Loading Reductions to the Environment
Actions taken by Chemours have reduced HFPO-DA loading to the environment by upwards of
5,150 lbs/yr. This value was calculated by combining the reductions in air emissions and the
minimum estimated reduction in Cape Fear River HFPO-DA loading. The July 2019 monthly
emissions report (Chemours, 2019) reported air emission reduction of 2,150 pounds. The
reductions to the Cape Fear River was based on the minimum estimated 2017 load of 3,147 lbs/yr
(Table 3) minus the maximum 2019 loading of 129 lbs/yr (Table 2) – a reduction of 3,018.
Combining these two reductions yields a total estimated reduction of HFPO-DA loading to the
environment since mid-June 2017 of 5,150 lbs/yr or greater.

REFERENCES
Chemours 2019: Monthly Emissions Report Pursuant to Consent Order Paragraph 8. Chemours
Fayetteville Works. July 22, 2019.

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