6001_Mecklenburg_Harrisburg_MSWLF_Dec21GW_FID1628622_20210104

DENR USE ONLY: I I ❑Paper Report ❑Electronic
NC DENR
Division of Waste Management - Solid Waste
_Email CD (data loaded: Yes / No
Doc/Event #:
Environmental Monitoring
Reaortina Form
Notice: This
form and
any
information attached
to it are "Public Records"
as defined in NC
General Statute 132-1. As such, these documents are
available for
inspection
and
examination by any
person upon request (NC
General Statute 132-6).
Instructions:
• Prepare one form for each individually monitored unit.
• Please type or print legibly.
• Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
• Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
• Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646,
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Mecklenburg County Solid Waste Services
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Amber R. Grzymski, P.G. Phone: [phone]
E-mail: [e-mail]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Harrisburg Road Landfill 7817 Harrisburg Road, Charlotte 60-01 .0500 December 1-2,14, 2021
Environmental Status: (Check all that apply)
Initial/Background Monitoring Q Detection Monitoring Assessment Monitoring Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells Q
Groundwater monitoring data from private water supply wells
Leachate monitoring data El
water monitoring data
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface wafer
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Amber R. Grzymski, P.G.
2145 Suttle Ave, Charlotte, NC 28208
Facility Representative Address
Project Manager
NC PE Firm License Number (if applicable effective May 1, 2009)
980-314-3855
(Area c.oaev ieiepnone ivumoer
Affix NC Licensed/ Professional Geologist Seal
Revised 6/2009

4ECKLEN13URU COUNTY
Land Use and Environmental Services Agency
Solid Waste Services
January 4, 2022
Jaclynne Drummond
North Carolina Department of Environment
and Natural Resources
Division of Waste Management - Solid Waste Section
2090 US Highway 70
Swannanoa, NC 28778
Subject: Water Quality Monitoring Report December 2021
Harrisburg Road Landfill, Permit 60-01
Dear Ms. Drummond:
Mecklenburg County conducted semi-annual water quality monitoring at the closed
Harrisburg Road Landfill December 1.2, 2021, in accordance with the approved revised
sample and analysis plan dated May 11, 2004. Samples were collected from seven
monitoring wells (HB W-12B, HB W-14, HB W-17B, HB W-20, HB W-21, HB W-22 and
background well HBW-28) and three surface -water sampling locations (14132006,
HB2008 and, HB2010). Laboratory analytical data, field -measured data, and a table of
results exceeding water quality standards along with a preliminary explanation of the
cause and significance are included on the electronic data deliverable (EDD) submittal.
The EDD containing the monitoring data are labeled to reflect the units that are used for
reporting. Detection levels and applicable standards have been included for all sampling
locations. Surface water standards listed are the water quality standards established for
freshwater classification for aquatic life as outlined in 15A NCAC 2B "Classification and
Water Quality Standards Applicable to Surface Waters of North Carolina". Groundwater
standards listed are the standards outlined in 15A NCAC 2L "Classification of Water
Quality Standards applicable to the Groundwaters of North Carolina". If the sample is
reported in parts per billion, then the standard is also reported in parts per billion.
Surface -water samples:
PEOPLE • PRIDE • PROGRESS •PARTNERSHIP
2145 Suttle Ave •Charlotte, NC 28208-5237 • [phone] •FAX [phone]
www. wip e outwaste 0 co m

Page 2
Barium was detected in HB 2006, HB 2008 and HB 2010 at 28.2 ppb, 24.2 ppb and 37.8
ppb, respectively. No other analytes were detected in the surface water samples. Field -
measured parameters for surface -water samples were within the range of established
standards and are summarized in the table below.
Location
Temperature
PH
Specific
Conductivity
Dissolved
Oxveen
HB2006
8.5° C
7.7
265.3 µs/cm
10.75 mg/l
HB2008
9.50 C
7.5
278.6 µs/cm
8.29 mg/l
HB2010
7.40 C
7.4
264.8 µs/cm
8.26 mg/l
Groundwater samples:
Multiple metals were detected above 2L standards. The table below summarizes metals
detections in groundwater samples.
Well ID
Ba
ug/1
Be
ug/1
Cd
ug/1
Cr
ug/l
Co
ug/l
Cu
ug/1
Ni
ug/1
Pb
ug/1
Th
ug/1
Vn
ug/l
Zn
ug/l
HBW12B
53.2
-----
-----
-----
------
14.4
-----
5.5
------
30.8
-----
HBW1481.3
-----
-----
-----
-----
8.7
-----
-----
------
-----
-----
HB W 17B
71.7
-----
------
-----
20.7
19.7
-----
-----
-----
6.6
18.1
HBW-20
15.2
-----
-----
-----
-----
8.7
-----
-----
------
16.6
-----
HB W-21
15.2
-----
-----
-----
-----
10.8
-----
-----
------
13.2
-----
HB W-22
61.2
-----
-----
94.1
-----
18.3
15.3
-----
-----
8.4
24.0
HBW-28*
62.0
-----
-----
-----
70.5
74.5
7.7
-----
------
30.2
-----
2L Std. ug/1
700
4
2.0
10
1
15000
100
15
0.2
0.3
1,000
Note: Bolded results exceed 2L Standard, *Background Well
The following volatile organic compounds ("VOCs") were detected in the sample
collected from well H13W-1711:
VOC
Sam le Result u /1
2L Standard u /1
Benzene
8.9
1
Tetrachloroeth lene
26.8
0.7
Trichloroeth lene
22.7
2.8
1,1-Dichloroethane
6.1
6
1,2-Dichloro ro ane
9.8
0.6
cis-1,2 Dichloroethene
123
70
trans-1,2 Dichloroethene
1.0
100
1,4-Dichlorobenzene
1.2
6
X lens total
10.7
500
Vinyl Chloride
1.8
0.03
Note: Bolded results exceed 2L Standard

Page 3
The pH was measured to be more acidic than the standard in the samples collected from
HBW17B, HBW-20, HBW-21, HBW-22 and background monitoring well HBW-28.
Field -measured parameters for groundwater samples are summarized in the following
table:
Location
Tem erature
pH
Conductivity
HBW12B
16.4
°C
6,5
379.4
µs/cm
HBW14
16.3
°C
6.5
215.0
µs/cm
HBW17B
16.6
°C
5.2
58.8
is/cm
HBW-20
16.7
°C
6.3
143.6
µs/cm
HBW-21
16.3
°C
6.1
192.9
µs/cm
HBW-22
17.7
°C
6.0
64.8
µs/cm
*HBW-28
16.6
°C
5.6
76.5
µs/cm
Note: Bolded results are outside of the 6.5 to 8.5 S.U. range 2L Standard
*Background Well
Please call me at [phone], if you have any questions concerning this report.
-_ 1�7i
" "Fto
" 967Qo400ec
Sincerely,
Amber R. Grzymski, P.G.
Project Manager
LUESA Solid Waste Services

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Landfill Gas Monitoring Data Form
Facility Name: Harrisburg Road Landfill
Permit Number: 60-01
Date of Sampling: _12/14/2021 NC Landfill Rule (.0500 or .1600): .0500
Name and Position of Sample Collector: David E. Coleman, Enviromnental Specialist
Type and Serial Number of Gas Meter: Gem 5000 #G507530
Calibration Date of Gas Meter: 4/26/2021 Date and Time of Field Calibration: 12/14/2021 13:15
Type of Field Calibration Gas (15/15 or 35/50): 35/50
Expiration Date of Field Calibration Gas Canister: February 2026
Pump Rate of Gas Meter: 120 Seconds Ambient Air Temperature: 65 De rees
Barometric Pressure: 29.57 General Weather Conditions: Sunny, Winds E7
Sam le ID
Time
% LEL
% CH4
% CO2
% 02
Comments
MP-1
14:11
>100
62.7
37.3
0
Methane Extraction System
MP-2
14:05
>100
57.5
29.5
2.5
Methane Extraction System
MP-3
13:57
0
0
0.2
20.4
Methane Extraction System
MP4
13:53
>100
1900
1205
14.0
Methane Extraction System
MP-5
15:00
0
0
2.7
18.8
MP-6
15:06
0
0
3.7
17.3
MP-7
15:13
0
0
5.0
17.4
MP-8
15:18
0
0
5.1
17.8
MP-9A
15:25
0
0
0.8
20.6
MP-913
15:31
0
0
3.8
18.1
MP-11
13:30
>100
7.3
9.4
12.3
MP42
13:40
0
0
6.4
15.6
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and
attachments are true and correct. I am aware that there are significant penalties for making any false
statement, representation, or certification including the possibility of a fine and imprisonment.
SIGNATURE
TITLE

60-01 Harrisbura Rd Landfill Methane Wells
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leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
December 10, 2021
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: HARRISBURG RD LANDFILL (PERMIT
Pace Project No.: 92575182
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on December 01, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 21

lacmnalyfical'f'
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: HARRISBURG RD LANDFILL (PERMIT
Pace Project No.: 92575182
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: HARRISBURG RD LANDFILL (PERMIT
Pace Project No.: 92575182
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92575182001 6001-HBW28
EPA 601OD
CBV, JOR
15
PASI-A
EPA 6020E
CRW
1
PASI-A
EPA 8260D
CL
52
PASI-C
92575182002 6001-HBW20
EPA 601OD
CBV, JOR
15
PASI-A
EPA 6020E
CRW
1
PASI-A
EPA 8260D
CL
52
PASI-C
92575182003 6001-HBW14
EPA 601OD
CBV, JOR
15
PASI-A
EPA 6020E
CRW
1
PASI-A
EPA 8260D
CL
52
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 21

Pace Analytical Services, LLC
ceAnalyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL (PERMIT
Pace Project No.: 92575182
Sample: 6001-HBW28 Lab ID: 92575182001 Collected: 12/01/21 10:55 Received: 12/01/21 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2106:59
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/07/21 13:43
12/09/2106:59
7440-38-2
Barium
62.0
ug/L
5.0
1
12/07/21 13:43
12/09/2106:59
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/07/21 13:43
12/09/2106:59
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/07/21 13:43
12/09/2106:59
7440-43-9
Chromium
ND
ug/L
5.0
1
12/07/21 13:43
12/09/21 17:04
7440-47-3
Cobalt
70.5
ug/L
5.0
1
12/07/21 13:43
12/09/2106:59
7440-48-4
Copper
74.5
ug/L
5.0
1
12/07/21 13:43
12/09/21 17:04
7440-50-8
Lead
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2106:59
7439-92-1
Nickel
7.7
ug/L
5.0
1
12/07/21 13:43
12/09/2106:59
7440-02-0
Selenium
ND
ug/L
10.0
1
12/07/21 13:43
12/09/2106:59
7782-49-2
Silver
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2106:59
7440-22-4
Thallium
ND
ug/L
10.0
1
12/07/21 13:43
12/09/2106:59
7440-28-0
Vanadium
30.2
ug/L
5.0
1
12/07/21 13:43
12/09/21 17:04
7440-62-2
Zinc
ND
ug/L
10.0
1
12/07/21 13:43
12/09/2106:59
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
12/07/2111:50
12/07/2123:22
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/04/21 12:50
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/04/21 12:50
107-13-1
Benzene
ND
ug/L
1.0
1
12/04/21 12:50
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/04/21 12:50
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/04/21 12:50
75-27-4
Bromoform
ND
ug/L
1.0
1
12/04/21 12:50
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/04/21 12:50
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/04/21 12:50
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/04/21 12:50
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/04/21 12:50
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/04/21 12:50
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/04/21 12:50
75-00-3
Chloroform
ND
ug/L
1.0
1
12/04/21 12:50
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/04/21 12:50
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/04/21 12:50
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/04/21 12:50
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/04/21 12:50
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/04/21 12:50
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 12:50
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 12:50
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/04/21 12:50
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/04/21 12:50
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/04/21 12:50
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL (PERMIT
Pace Project No.: 92575182
Sample: 6001-HBW28 Lab ID: 92575182001 Collected: 12/01/21 10:55 Received: 12/01/21 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/04/21 12:50
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 12:50
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 12:50
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/04/21 12:50
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/04/21 12:50
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/04/21 12:50
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/04/21 12:50
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/04/21 12:50
591-78-6
lodomethane
ND
ug/L
20.0
1
12/04/21 12:50
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/04/21 12:50
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/04/21 12:50
108-10-1
Styrene
ND
ug/L
1.0
1
12/04/21 12:50
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/04/21 12:50
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/04/21 12:50
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/04/21 12:50
127-18-4
Toluene
ND
ug/L
1.0
1
12/04/21 12:50
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/04/21 12:50
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/04/21 12:50
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/04/21 12:50
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/04/21 12:50
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/04/21 12:50
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/04/21 12:50
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/04/21 12:50
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/04/21 12:50
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/04/21 12:50
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/04/21 12:50
95-47-6
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
12/04/21 12:50
460-00-4
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
12/04/21 12:50
17060-07-0
Toluene-d8(S)
101
%
70-130
1
12/04/21 12:50
2037-26-5
Date: 12/10/2021 04:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 21

Pace Analytical Services, LLC
ceAnalyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL (PERMIT
Pace Project No.: 92575182
Sample: 6001-HBW20 Lab ID: 92575182002 Collected: 12/01/21 11:40 Received: 12/01/21 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2107:02
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/07/21 13:43
12/09/2107:02
7440-38-2
Barium
15.2
ug/L
5.0
1
12/07/21 13:43
12/09/2107:02
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/07/21 13:43
12/09/2107:02
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/07/21 13:43
12/09/2107:02
7440-43-9
Chromium
ND
ug/L
5.0
1
12/07/21 13:43
12/09/21 17:08
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2107:02
7440-48-4
Copper
8.7
ug/L
5.0
1
12/07/21 13:43
12/09/21 17:08
7440-50-8
Lead
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2107:02
7439-92-1
Nickel
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2107:02
7440-02-0
Selenium
ND
ug/L
10.0
1
12/07/21 13:43
12/09/2107:02
7782-49-2
Silver
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2107:02
7440-22-4
Thallium
ND
ug/L
10.0
1
12/07/21 13:43
12/09/2107:02
7440-28-0
Vanadium
16.6
ug/L
5.0
1
12/07/21 13:43
12/09/21 17:08
7440-62-2
Zinc
ND
ug/L
10.0
1
12/07/21 13:43
12/09/2107:02
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
12/07/2111:50
12/07/2123:25
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/04/21 13:09
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/04/21 13:09
107-13-1
Benzene
ND
ug/L
1.0
1
12/04/21 13:09
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/04/21 13:09
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/04/21 13:09
75-27-4
Bromoform
ND
ug/L
1.0
1
12/04/21 13:09
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/04/21 13:09
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/04/21 13:09
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/04/21 13:09
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/04/21 13:09
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/04/21 13:09
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/04/21 13:09
75-00-3
Chloroform
ND
ug/L
1.0
1
12/04/21 13:09
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/04/21 13:09
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/04/21 13:09
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/04/21 13:09
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/04/21 13:09
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/04/21 13:09
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 13:09
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 13:09
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/04/21 13:09
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/04/21 13:09
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/04/21 13:09
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL (PERMIT
Pace Project No.: 92575182
Sample: 6001-HBW20 Lab ID: 92575182002 Collected: 12/01/21 11:40 Received: 12/01/21 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/04/21 13:09
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 13:09
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 13:09
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/04/21 13:09
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/04/21 13:09
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/04/21 13:09
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/04/21 13:09
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/04/21 13:09
591-78-6
lodomethane
ND
ug/L
20.0
1
12/04/21 13:09
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/04/21 13:09
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/04/21 13:09
108-10-1
Styrene
ND
ug/L
1.0
1
12/04/21 13:09
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/04/21 13:09
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/04/21 13:09
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/04/21 13:09
127-18-4
Toluene
ND
ug/L
1.0
1
12/04/21 13:09
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/04/21 13:09
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/04/21 13:09
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/04/21 13:09
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/04/21 13:09
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/04/21 13:09
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/04/21 13:09
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/04/21 13:09
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/04/21 13:09
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/04/21 13:09
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/04/21 13:09
95-47-6
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
12/04/21 13:09
460-00-4
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
12/04/21 13:09
17060-07-0
Toluene-d8(S)
100
%
70-130
1
12/04/21 13:09
2037-26-5
Date: 12/10/2021 04:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 21

Pace Analytical Services, LLC
ceAnalyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL (PERMIT
Pace Project No.: 92575182
Sample: 6001-HBW14 Lab ID: 92575182003 Collected: 12/01/21 12:00 Received: 12/01/21 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
12/07/2113:43
12/09/2107:05
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/07/2113:43
12/09/2107:05
7440-38-2
Barium
81.3
ug/L
5.0
1
12/07/2113:43
12/09/2107:05
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/07/2113:43
12/09/2107:05
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/07/2113:43
12/09/2107:05
7440-43-9
Chromium
ND
ug/L
5.0
1
12/07/2113:43
12/09/2117:11
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/07/2113:43
12/09/2107:05
7440-48-4
Copper
8.7
ug/L
5.0
1
12/07/2113:43
12/09/2117:11
7440-50-8
Lead
ND
ug/L
5.0
1
12/07/2113:43
12/09/2107:05
7439-92-1
Nickel
ND
ug/L
5.0
1
12/07/2113:43
12/09/2107:05
7440-02-0
Selenium
ND
ug/L
10.0
1
12/07/2113:43
12/09/2107:05
7782-49-2
Silver
ND
ug/L
5.0
1
12/07/2113:43
12/09/2107:05
7440-22-4
Thallium
ND
ug/L
10.0
1
12/07/2113:43
12/09/2107:05
7440-28-0
Vanadium
ND
ug/L
5.0
1
12/07/2113:43
12/09/2117:11
7440-62-2
Zinc
ND
ug/L
10.0
1
12/07/2113:43
12/09/2107:05
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
12/07/2111:50
12/07/2123:36
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/04/21 13:27
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/04/21 13:27
107-13-1
Benzene
ND
ug/L
1.0
1
12/04/21 13:27
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/04/21 13:27
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/04/21 13:27
75-27-4
Bromoform
ND
ug/L
1.0
1
12/04/21 13:27
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/04/21 13:27
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/04/21 13:27
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/04/21 13:27
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/04/21 13:27
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/04/21 13:27
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/04/21 13:27
75-00-3
Chloroform
ND
ug/L
1.0
1
12/04/21 13:27
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/04/21 13:27
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/04/21 13:27
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/04/21 13:27
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/04/21 13:27
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/04/21 13:27
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 13:27
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 13:27
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/04/21 13:27
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/04/21 13:27
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/04/21 13:27
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL (PERMIT
Pace Project No.: 92575182
Sample: 6001-HBW14 Lab ID: 92575182003 Collected: 12/01/21 12:00 Received: 12/01/21 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/04/21 13:27
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 13:27
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 13:27
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/04/21 13:27
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/04/21 13:27
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/04/21 13:27
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/04/21 13:27
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/04/21 13:27
591-78-6
lodomethane
ND
ug/L
20.0
1
12/04/21 13:27
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/04/21 13:27
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/04/21 13:27
108-10-1
Styrene
ND
ug/L
1.0
1
12/04/21 13:27
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/04/21 13:27
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/04/21 13:27
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/04/21 13:27
127-18-4
Toluene
ND
ug/L
1.0
1
12/04/21 13:27
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/04/21 13:27
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/04/21 13:27
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/04/21 13:27
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/04/21 13:27
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/04/21 13:27
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/04/21 13:27
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/04/21 13:27
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/04/21 13:27
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/04/21 13:27
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/04/21 13:27
95-47-6
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
12/04/21 13:27
460-00-4
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
12/04/21 13:27
17060-07-0
Toluene-d8(S)
100
%
70-130
1
12/04/21 13:27
2037-26-5
Date: 12/10/2021 04:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL (PERMIT
Pace Project No.: 92575182
QC Batch: 664332 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92575182001, 92575182002, 92575182003
METHOD BLANK: 3479656 Matrix: Water
Associated Lab Samples: 92575182001, 92575182002, 92575182003
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
5.0 12/09/21 05:38
10.0 12/09/21 05:38
5.0 12/09/21 05:38
1.0 12/09/21 05:38
1.0 12/09/21 05:38
5.0 12/09/21 05:38
5.0 12/09/21 05:38
5.0 12/09/21 05:38
5.0 12/09/21 05:38
5.0 12/09/21 05:38
10.0 12/09/21 05:38
5.0 12/09/21 05:38
10.0 12/09/21 05:38
5.0 12/09/21 05:38
10.0 12/09/21 05:38
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3479657
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
549
110
80-120
Arsenic
ug/L
500
493
99
80-120
Barium
ug/L
500
540
108
80-120
Beryllium
ug/L
500
529
106
80-120
Cadmium
ug/L
500
505
101
80-120
Chromium
ug/L
500
485
97
80-120
Cobalt
ug/L
500
506
101
80-120
Copper
ug/L
500
494
99
80-120
Lead
ug/L
500
516
103
80-120
Nickel
ug/L
500
508
102
80-120
Selenium
ug/L
500
521
104
80-120
Silver
ug/L
250
256
102
80-120
Thallium
ug/L
500
500
100
80-120
Vanadium
ug/L
500
500
100
80-120
Zinc
ug/L
500
511
102
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 21

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
HARRISBURG RD LANDFILL (PERMIT
92575182
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3479658
3479659
MS
MSD
92575770012
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
560
552
112
110
75-125
1
Arsenic
ug/L
ND
500
500
477
467
95
93
75-125
2
Barium
ug/L
34.2
500
500
534
532
100
100
75-125
0
Beryllium
ug/L
ND
500
500
492
490
98
98
75-125
0
Cadmium
ug/L
ND
500
500
484
481
97
96
75-125
1
Chromium
ug/L
ND
500
500
456
455
91
91
75-125
0 E
Cobalt
ug/L
ND
500
500
469
466
94
93
75-125
1
Copper
ug/L
ND
500
500
462
460
92
92
75-125
0 E
Lead
ug/L
ND
500
500
486
481
97
96
75-125
1
Nickel
ug/L
ND
500
500
474
471
95
94
75-125
1
Selenium
ug/L
9.11
500
500
519
510
102
100
75-125
2
Silver
ug/L
ND
250
250
258
257
103
103
75-125
1
Thallium
ug/L
ND
500
500
460
458
92
91
75-125
0
Vanadium
ug/L
ND
500
500
474
479
95
96
75-125
1
Zinc
ug/L
14.5
500
500
502
500
98
97
75-125
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 21

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL (PERMIT
Pace Project No.: 92575182
QC Batch: 664324 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92575182001, 92575182002, 92575182003
METHOD BLANK: 3479628
Matrix:
Water
Associated Lab Samples: 92575182001, 92575182002, 92575182003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
0.47
12/07/2118:15
LABORATORY CONTROL SAMPLE:
3479629
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
25
23.9
95 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3480738 3480739
MS MSD
92573625015 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 25 25 24.5 24.9 98 100 75-125 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL (PERMIT
Pace Project No.: 92575182
QC Batch: 663872 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92575182001, 92575182002, 92575182003
METHOD BLANK: 3477583 Matrix:
Associated Lab Samples: 92575182001, 92575182002, 92575182003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
12/04/21 06:29
1,1,1-Trichloroethane
ug/L
ND
1.0
12/04/21 06:29
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/04/21 06:29
1,1,2-Trichloroethane
ug/L
ND
1.0
12/04/21 06:29
1,1-Dichloroethane
ug/L
ND
1.0
12/04/21 06:29
1,1-Dichloroethene
ug/L
ND
1.0
12/04/21 06:29
1,2,3-Trichloropropane
ug/L
ND
1.0
12/04/21 06:29
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
12/04/21 06:29
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/04/21 06:29
1,2-Dichlorobenzene
ug/L
ND
1.0
12/04/21 06:29
1,2-Dichloroethane
ug/L
ND
1.0
12/04/21 06:29
1,2-Dichloropropane
ug/L
ND
1.0
12/04/21 06:29
1,4-Dichlorobenzene
ug/L
ND
1.0
12/04/21 06:29
2-Butanone (MEK)
ug/L
ND
5.0
12/04/21 06:29
2-Hexanone
ug/L
ND
5.0
12/04/21 06:29
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/04/21 06:29
Acetone
ug/L
ND
25.0
12/04/21 06:29
Acrylonitrile
ug/L
ND
10.0
12/04/21 06:29
Benzene
ug/L
ND
1.0
12/04/21 06:29
Bromochloromethane
ug/L
ND
1.0
12/04/21 06:29
Bromodichloromethane
ug/L
ND
1.0
12/04/21 06:29
Bromoform
ug/L
ND
1.0
12/04/21 06:29
Bromomethane
ug/L
ND
2.0
12/04/21 06:29
Carbon disulfide
ug/L
ND
2.0
12/04/21 06:29
Carbon tetrachloride
ug/L
ND
1.0
12/04/21 06:29
Chlorobenzene
ug/L
ND
1.0
12/04/21 06:29
Chloroethane
ug/L
ND
1.0
12/04/21 06:29
Chloroform
ug/L
ND
1.0
12/04/21 06:29
Chloromethane
ug/L
ND
1.0
12/04/21 06:29
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/04/21 06:29
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/04/21 06:29
Dibromochloromethane
ug/L
ND
1.0
12/04/21 06:29
Dibromomethane
ug/L
ND
1.0
12/04/21 06:29
Ethylbenzene
ug/L
ND
1.0
12/04/21 06:29
lodomethane
ug/L
ND
20.0
12/04/21 06:29
m&p-Xylene
ug/L
ND
2.0
12/04/21 06:29
Methylene Chloride
ug/L
ND
5.0
12/04/21 06:29
o-Xylene
ug/L
ND
1.0
12/04/21 06:29
Styrene
ug/L
ND
1.0
12/04/21 06:29
Tetrachloroethene
ug/L
ND
1.0
12/04/21 06:29
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL (PERMIT
Pace Project No.: 92575182
METHOD BLANK: 3477583 Matrix:
Associated Lab Samples: 92575182001, 92575182002, 92575182003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
Toluene
ug/L
ND
1.0
12/04/21 06:29
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/04/21 06:29
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/04/21 06:29
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
12/04/21 06:29
Trichloroethene
ug/L
ND
1.0
12/04/21 06:29
Trichlorofluoromethane
ug/L
ND
1.0
12/04/21 06:29
Vinyl acetate
ug/L
ND
2.0
12/04/21 06:29
Vinyl chloride
ug/L
ND
1.0
12/04/21 06:29
Xylene (Total)
ug/L
ND
1.0
12/04/21 06:29
1,2-Dichloroethane-d4 (S)
%
96
70-130
12/04/21 06:29
4-Bromofluorobenzene (S)
%
100
70-130
12/04/21 06:29
Toluene-d8 (S)
%
100
70-130
12/04/21 06:29
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3477584
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.0
102
70-130
1,1,1-Trichloroethane
ug/L
50
49.3
99
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.9
102
70-130
1,1,2-Trichloroethane
ug/L
50
48.9
98
70-130
1,1-Dichloroethane
ug/L
50
49.1
98
70-130
1,1-Dichloroethene
ug/L
50
49.5
99
70-132
1,2,3-Trichloropropane
ug/L
50
50.1
100
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
55.1
110
70-132
1,2-Dibromoethane (EDB)
ug/L
50
50.7
101
70-130
1,2-Dichlorobenzene
ug/L
50
50.5
101
70-130
1,2-Dichloroethane
ug/L
50
49.0
98
70-130
1,2-Dichloropropane
ug/L
50
50.4
101
70-130
1,4-Dichlorobenzene
ug/L
50
50.7
101
70-130
2-Butanone (MEK)
ug/L
100
94.7
95
70-133
2-Hexanone
ug/L
100
104
104
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
101
101
70-130
Acetone
ug/L
100
96.2
96
70-144
Acrylonitrile
ug/L
250
233
93
70-130
Benzene
ug/L
50
48.6
97
70-130
Bromochloromethane
ug/L
50
48.9
98
70-130
Bromodichloromethane
ug/L
50
50.5
101
70-130
Bromoform
ug/L
50
51.3
103
70-131
Bromomethane
ug/L
50
57.6
115
30-177
Carbon disulfide
ug/L
50
49.9
100
70-133
Carbon tetrachloride
ug/L
50
50.5
101
70-130
Chlorobenzene
ug/L
50
50.6
101
70-130
Chloroethane
ug/L
50
43.1
86
46-131
Chloroform
ug/L
50
48.3
97
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL (PERMIT
Pace Project No.: 92575182
LABORATORY CONTROL SAMPLE:
Parameter
3477584
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Chloromethane
ug/L
50
50.0
100
49-130
cis-1,2-Dichloroethene
ug/L
50
49.2
98
70-130
cis-1,3-Dichloropropene
ug/L
50
49.4
99
70-130
Dibromochloromethane
ug/L
50
52.2
104
70-130
Dibromomethane
ug/L
50
48.8
98
70-130
Ethylbenzene
ug/L
50
51.2
102
70-130
lodomethane
ug/L
100
111
111
47-140
m&p-Xylene
ug/L
100
104
104
70-130
Methylene Chloride
ug/L
50
47.8
96
68-130
o-Xylene
ug/L
50
51.4
103
70-130
Styrene
ug/L
50
52.5
105
70-130
Tetrachloroethene
ug/L
50
49.7
99
70-130
Toluene
ug/L
50
49.0
98
70-130
trans-1,2-Dichloroethene
ug/L
50
49.6
99
70-130
trans- 1,3-Dichloropropene
ug/L
50
49.3
99
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
60.7
121
25-200
Trichloroethene
ug/L
50
49.5
99
70-130
Trichlorofluoromethane
ug/L
50
47.7
95
61-130
Vinyl acetate
ug/L
100
99.3
99
70-140
Vinyl chloride
ug/L
50
52.3
105
59-142
Xylene (Total)
ug/L
150
155
103
70-130
1,2-Dichloroethane-d4 (S)
%
96
70-130
4-Bromofluorobenzene (S)
%
102
70-130
Toluene-d8 (S)
%
100
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3477585
MS
92575083005 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3477586
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
24.1
22.6
121
113
70-135
7
1,1,1-Trichloroethane
ug/L
ND
20
20
20.4
19.4
102
97
70-148
5
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
23.5
22.3
118
111
70-131
5
1,1,2-Trichloroethane
ug/L
ND
20
20
22.4
21.2
112
106
70-136
5
1,1-Dichloroethane
ug/L
ND
20
20
19.6
19.0
98
95
70-147
3
1,1-Dichloroethene
ug/L
ND
20
20
18.1
17.7
90
89
70-158
2
1,2,3-Trichloropropane
ug/L
ND
20
20
22.2
21.1
111
106
67-137
5
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
25.8
24.7
129
124
69-136
4
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
23.5
22.3
117
112
70-137
5
1,2-Dichlorobenzene
ug/L
ND
20
20
23.8
22.6
119
113
70-133
5
1,2-Dichloroethane
ug/L
ND
20
20
19.5
18.6
97
93
67-138
5
1,2-Dichloropropane
ug/L
ND
20
20
21.6
20.4
108
102
70-138
6
1,4-Dichlorobenzene
ug/L
ND
20
20
23.9
22.6
120
113
70-133
6
2-Butanone (MEK)
ug/L
ND
40
40
39.2
38.6
98
96
61-147
2
2-Hexanone
ug/L
ND
40
40
44.7
43.6
112
109
67-139
3
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
41.9
40.6
105
101
67-136
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL (PERMIT
Pace Project No.: 92575182
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3477585
MS
92575083005 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3477586
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
36.5
35.6
91
89
55-159
3
Acrylonitrile
ug/L
ND
100
100
92.6
91.1
93
91
68-140
2
Benzene
ug/L
ND
20
20
20.5
19.6
102
98
67-150
4
Bromochloromethane
ug/L
ND
20
20
20.8
20.1
104
101
70-146
3
Bromodichloromethane
ug/L
ND
20
20
22.1
20.5
110
103
70-138
7
Bromoform
ug/L
ND
20
20
23.3
22.1
116
111
57-138
5
Bromomethane
ug/L
ND
20
20
16.0
16.1
80
80
10-200
0 v3
Carbon disulfide
ug/L
ND
20
20
18.1
17.4
91
87
70-152
4
Carbon tetrachloride
ug/L
ND
20
20
21.0
20.6
105
103
70-147
2
Chlorobenzene
ug/L
ND
20
20
23.3
22.1
116
111
70-137
5
Chloroethane
ug/L
ND
20
20
16.9
15.9
85
79
51-166
6 v3
Chloroform
ug/L
ND
20
20
19.7
19.0
98
95
70-144
4
Chloromethane
ug/L
ND
20
20
16.4
16.0
82
80
24-161
3
cis-1,2-Dichloroethene
ug/L
ND
20
20
20.1
19.2
101
96
67-148
5
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.8
20.4
109
102
70-142
7
Dibromochloromethane
ug/L
ND
20
20
23.9
22.3
120
111
68-138
7
Dibromomethane
ug/L
ND
20
20
22.3
21.1
112
106
70-134
6
Ethylbenzene
ug/L
ND
20
20
22.9
22.0
115
110
68-143
4
lodomethane
ug/L
ND
40
40
39.3
37.0
98
93
20-161
6
m&p-Xylene
ug/L
ND
40
40
45.9
44.1
115
110
53-157
4
Methylene Chloride
ug/L
ND
20
20
18.9
17.9
95
89
64-148
6
o-Xylene
ug/L
ND
20
20
23.2
22.0
116
110
68-143
6
Styrene
ug/L
ND
20
20
23.1
22.0
116
110
70-136
5
Tetrachloroethene
ug/L
ND
20
20
22.1
21.7
111
108
70-139
2
Toluene
ug/L
ND
20
20
21.2
20.4
106
102
47-157
4
trans-1,2-Dichloroethene
ug/L
ND
20
20
19.8
18.2
99
91
70-149
8
trans- 1,3-Dichloropropene
ug/L
ND
20
20
21.8
20.0
109
100
70-138
9
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
20.2
16.3
101
81
31-145
22
Trichloroethene
ug/L
ND
20
20
21.4
20.6
107
103
70-149
4
Trichlorofluoromethane
ug/L
ND
20
20
15.9
15.3
80
77
61-154
4 v3
Vinyl acetate
ug/L
ND
40
40
42.6
40.1
106
100
48-156
6
Vinyl chloride
ug/L
ND
20
20
17.8
17.1
89
85
55-172
4
Xylene (Total)
ug/L
ND
60
60
69.2
66.1
115
110
66-145
5
1,2-Dichloroethane-d4 (S)
%
91
88
70-130
4-Bromofluorobenzene (S)
%
100
100
70-130
Toluene-d8(S)
%
98
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 21

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: HARRISBURG RD LANDFILL (PERMIT
Pace Project No.: 92575182
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
E Analyte concentration exceeded the calibration range. The reported result is estimated.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: HARRISBURG RD LANDFILL (PERMIT
Pace Project No.: 92575182
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92575182001
6001-HBW28
EPA 3010A
664332
EPA6010D
664507
92575182002
6001-HBW20
EPA 3010A
664332
EPA6010D
664507
92575182003
6001-HBW14
EPA 3010A
664332
EPA6010D
664507
92575182001
6001-HBW28
EPA 3010A
664324
EPA6020B
664495
92575182002
6001-HBW20
EPA 3010A
664324
EPA6020B
664495
92575182003
6001-HBW14
EPA 3010A
664324
EPA6020B
664495
92575182001
6001-HBW28
EPA 8260D
663872
92575182002
6001-HBW20
EPA8260D
663872
92575182003
6001-HBW14
EPA8260D
663872
Date: 12/10/2021 04:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 21

Document Name:
Document Revised: November 15, 2021
aeeAnaoical d
Sample Condition Upon Recelpt (SCUR)
Page 1 of 2
Document No,:
Issuing Authority:
F•CAR-CS-033-Rev.08
Pace Carolinas Quality office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ HuntersvilleQ Raleigh[] Mechanicsville❑ Atlanta❑ Kernersville❑
• 11 Client Na Im- of :�� f } Project WQI# ' 9,2575182
Courier: ❑Fed Ex ❑UP5 ❑U5P5 ❑Cli—en t
❑ Commercial ©Pace ❑Other: IIII I 11 I
92575182
Custody Seal Present? Dyes ®No Seats intact? ❑Yes QNo
Date/Initlals Person Examining Contents:
Packing Materlal: []Bubble Wrap QBubble Bags ❑None ❑ Other Biological Tissue frozen?
Thermometer []Yes ❑No ON/A
IR Gun ID: Tug U{ Type of tee; �GVet []Blue ❑None
Correction Factor -
Cooler Temp: Add/Subtract VQ Temp should be above freezing to 5'C
Eaoler-Temp@onected f=C},
Dimples cut of temp criteria. Samples on ice, cooling process
ass egun
USDA Regulated Soll ('EIN/A, water.sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Mel samples originate from a fa -Win source iintemationaay,
nYes I7No , r-r,. r -.
Comments/Discrepancy:
Chain of Custody Present?
hiles
❑No
❑N/A
1.
Samples Arrived within Hold Time?
Short Hold Time Analysls (<72 hr.)?
'Qr YeS
❑Yes
❑Na
J - No
❑N/A
N/A
2.
3.
Rush Tarn Around Time Requested?
[-]Yes
'QNo
❑N/A
4.
Sufficient Volume?
'fqVes
[]No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
t2Yes
OYes
❑No
[]No
[)WA
❑N/A
6.
Containers Intact?
ItYeS
❑No
JJNJA
7.
Dissolved analysis: Samples Feld Filtered?
❑Yes
[:)No
❑N/A
8.
Sample Labels Match COC?
-IncludesDate/Time/ID/Analysis Matrlx:
Yes
UT
❑No
❑N/A
9.
Headspace in VOA Vials (>5.6mm)?
❑Yes
Mo
❑N/A
10.
Trip Blank?resent?
Trip Blank Custody Seals Present?
[]Yes
[]Yes
'®No
[-]No
❑N/A
N/A
COMMEN75/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person C9ntacted:
Project Manager SCURF Review:
Project Manager:SRF Review-
Date/Time:
Lot ID of spit containers:
Date:
Date:
Field Data Required? []Yes ❑No
Page 19 of 21

Document Name:
Document Revised: November 15, 2021
o
Sample Conditlon Upon Recelpt (SCUR)
Page 2 of 2
Document No.:
issuing Authority:
2GEAfldlylCal.
F•CAR•CS-033-Rev.08
Pace Carolinas Quality Office
*Check mark top half of box If pH and/or dechlorination is Project # r
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottles
WO,# : 9r2575182
PM: MWB Due Date: 12/15/21
CLIENT: 92—MECK CO
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PA

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
December 10, 2021
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on December 01, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 25

lacmnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92575188001 6001-HBW21
EPA 601OD
CBV, JOR
15
PASI-A
EPA 6020E
CRW
1
PASI-A
EPA 8260D
CL
52
PASI-C
92575188002 6001-HBW22
EPA 601OD
CBV, JOR
15
PASI-A
EPA 6020E
CRW
1
PASI-A
EPA 8260D
CL
52
PASI-C
92575188003 6001-HBW12B
EPA 601OD
CBV, JOR
15
PASI-A
EPA 6020E
CRW
1
PASI-A
EPA 8260D
CL
52
PASI-C
92575188004 6001-HBW17B
EPA 601OD
CBV, JOR
15
PASI-A
EPA 6020E
CRW
1
PASI-A
EPA 8260D
CL
52
PASI-C
92575188005 TRIP BLANK
EPA 8260D
CL
52
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 25

Pace Analytical Services, LLC
ceAnalyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
Sample: 6001-HBW21 Lab ID: 92575188001 Collected: 12/01/21 13:50 Received: 12/01/21 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2107:08
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/07/21 13:43
12/09/2107:08
7440-38-2
Barium
15.2
ug/L
5.0
1
12/07/21 13:43
12/09/2107:08
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/07/21 13:43
12/09/2107:08
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/07/21 13:43
12/09/2107:08
7440-43-9
Chromium
ND
ug/L
5.0
1
12/07/21 13:43
12/09/21 17:14
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2107:08
7440-48-4
Copper
10.8
ug/L
5.0
1
12/07/21 13:43
12/09/21 17:14
7440-50-8
Lead
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2107:08
7439-92-1
Nickel
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2107:08
7440-02-0
Selenium
ND
ug/L
10.0
1
12/07/21 13:43
12/09/2107:08
7782-49-2
Silver
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2107:08
7440-22-4
Thallium
ND
ug/L
10.0
1
12/07/21 13:43
12/09/2107:08
7440-28-0
Vanadium
13.2
ug/L
5.0
1
12/07/21 13:43
12/09/21 17:14
7440-62-2
Zinc
ND
ug/L
10.0
1
12/07/21 13:43
12/09/2107:08
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
12/07/2111:50
12/07/2123:39
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/04/21 13:45
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/04/21 13:45
107-13-1
Benzene
ND
ug/L
1.0
1
12/04/21 13:45
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/04/21 13:45
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/04/21 13:45
75-27-4
Bromoform
ND
ug/L
1.0
1
12/04/21 13:45
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/04/21 13:45
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/04/21 13:45
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/04/21 13:45
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/04/21 13:45
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/04/21 13:45
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/04/21 13:45
75-00-3
Chloroform
ND
ug/L
1.0
1
12/04/21 13:45
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/04/21 13:45
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/04/21 13:45
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/04/21 13:45
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/04/21 13:45
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/04/21 13:45
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 13:45
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 13:45
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/04/21 13:45
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/04/21 13:45
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/04/21 13:45
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
Sample: 6001-HBW21 Lab ID: 92575188001 Collected: 12/01/21 13:50 Received: 12/01/21 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/04/21 13:45
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 13:45
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 13:45
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/04/21 13:45
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/04/21 13:45
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/04/21 13:45
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/04/21 13:45
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/04/21 13:45
591-78-6
lodomethane
ND
ug/L
20.0
1
12/04/21 13:45
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/04/21 13:45
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/04/21 13:45
108-10-1
Styrene
ND
ug/L
1.0
1
12/04/21 13:45
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/04/21 13:45
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/04/21 13:45
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/04/21 13:45
127-18-4
Toluene
ND
ug/L
1.0
1
12/04/21 13:45
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/04/21 13:45
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/04/21 13:45
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/04/21 13:45
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/04/21 13:45
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/04/21 13:45
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/04/21 13:45
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/04/21 13:45
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/04/21 13:45
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/04/21 13:45
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/04/21 13:45
95-47-6
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
12/04/21 13:45
460-00-4
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
12/04/21 13:45
17060-07-0
Toluene-d8(S)
101
%
70-130
1
12/04/21 13:45
2037-26-5
Date: 12/10/2021 04:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 25

Pace Analytical Services, LLC
ceAnalyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
Sample: 6001-HBW22 Lab ID: 92575188002 Collected: 12/01/21 13:25 Received: 12/01/21 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2107:12
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/07/21 13:43
12/09/2107:12
7440-38-2
Barium
61.2
ug/L
5.0
1
12/07/21 13:43
12/09/2107:12
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/07/21 13:43
12/09/2107:12
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/07/21 13:43
12/09/2107:12
7440-43-9
Chromium
94.1
ug/L
5.0
1
12/07/21 13:43
12/09/21 17:17
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2107:12
7440-48-4
Copper
18.3
ug/L
5.0
1
12/07/21 13:43
12/09/21 17:17
7440-50-8
Lead
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2107:12
7439-92-1
Nickel
15.3
ug/L
5.0
1
12/07/21 13:43
12/09/2107:12
7440-02-0
Selenium
ND
ug/L
10.0
1
12/07/21 13:43
12/09/2107:12
7782-49-2
Silver
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2107:12
7440-22-4
Thallium
ND
ug/L
10.0
1
12/07/21 13:43
12/09/2107:12
7440-28-0
Vanadium
8.4
ug/L
5.0
1
12/07/21 13:43
12/09/21 17:17
7440-62-2
Zinc
24.0
ug/L
10.0
1
12/07/21 13:43
12/09/2107:12
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
12/07/2111:50
12/07/2123:43
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/04/21 14:03
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/04/21 14:03
107-13-1
Benzene
ND
ug/L
1.0
1
12/04/21 14:03
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/04/21 14:03
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/04/21 14:03
75-27-4
Bromoform
ND
ug/L
1.0
1
12/04/21 14:03
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/04/21 14:03
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/04/21 14:03
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/04/21 14:03
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/04/21 14:03
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/04/21 14:03
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/04/21 14:03
75-00-3
Chloroform
ND
ug/L
1.0
1
12/04/21 14:03
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/04/21 14:03
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/04/21 14:03
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/04/21 14:03
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/04/21 14:03
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/04/21 14:03
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 14:03
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 14:03
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/04/21 14:03
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/04/21 14:03
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/04/21 14:03
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
Sample: 6001-HBW22 Lab ID: 92575188002 Collected: 12/01/21 13:25 Received: 12/01/21 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/04/21 14:03
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 14:03
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 14:03
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/04/21 14:03
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/04/21 14:03
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/04/21 14:03
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/04/21 14:03
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/04/21 14:03
591-78-6
lodomethane
ND
ug/L
20.0
1
12/04/21 14:03
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/04/21 14:03
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/04/21 14:03
108-10-1
Styrene
ND
ug/L
1.0
1
12/04/21 14:03
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/04/21 14:03
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/04/21 14:03
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/04/21 14:03
127-18-4
Toluene
ND
ug/L
1.0
1
12/04/21 14:03
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/04/21 14:03
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/04/21 14:03
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/04/21 14:03
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/04/21 14:03
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/04/21 14:03
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/04/21 14:03
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/04/21 14:03
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/04/21 14:03
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/04/21 14:03
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/04/21 14:03
95-47-6
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
12/04/21 14:03
460-00-4
1,2-Dichloroethane-d4 (S)
95
%
70-130
1
12/04/21 14:03
17060-07-0
Toluene-d8(S)
100
%
70-130
1
12/04/21 14:03
2037-26-5
Date: 12/10/2021 04:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 25

Pace Analytical Services, LLC
ceAnalyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
Sample: 6001-HBW12B Lab ID: 92575188003 Collected: 12/01/21 14:05 Received: 12/01/21 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
12/07/2113:43
12/09/2107:15
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/07/2113:43
12/09/2107:15
7440-38-2
Barium
53.2
ug/L
5.0
1
12/07/2113:43
12/09/2107:15
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/07/2113:43
12/09/2107:15
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/07/2113:43
12/09/2107:15
7440-43-9
Chromium
ND
ug/L
5.0
1
12/07/2113:43
12/09/2117:21
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/07/2113:43
12/09/2107:15
7440-48-4
Copper
14.4
ug/L
5.0
1
12/07/2113:43
12/09/2117:21
7440-50-8
Lead
5.5
ug/L
5.0
1
12/07/21 13:43
12/09/2107:15
7439-92-1
Nickel
ND
ug/L
5.0
1
12/07/2113:43
12/09/2107:15
7440-02-0
Selenium
ND
ug/L
10.0
1
12/07/2113:43
12/09/2107:15
7782-49-2
Silver
ND
ug/L
5.0
1
12/07/2113:43
12/09/2107:15
7440-22-4
Thallium
ND
ug/L
10.0
1
12/07/2113:43
12/09/2107:15
7440-28-0
Vanadium
30.8
ug/L
5.0
1
12/07/2113:43
12/09/2117:21
7440-62-2
Zinc
ND
ug/L
10.0
1
12/07/2113:43
12/09/2107:15
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
12/07/2111:50
12/07/2123:46
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/04/21 14:21
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/04/21 14:21
107-13-1
Benzene
ND
ug/L
1.0
1
12/04/21 14:21
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/04/21 14:21
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/04/21 14:21
75-27-4
Bromoform
ND
ug/L
1.0
1
12/04/21 14:21
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/04/21 14:21
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/04/21 14:21
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/04/21 14:21
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/04/21 14:21
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/04/21 14:21
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/04/21 14:21
75-00-3
Chloroform
ND
ug/L
1.0
1
12/04/21 14:21
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/04/21 14:21
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/04/21 14:21
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/04/21 14:21
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/04/21 14:21
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/04/21 14:21
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 14:21
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 14:21
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/04/21 14:21
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/04/21 14:21
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/04/21 14:21
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
Sample: 6001-HBW12B Lab ID: 92575188003 Collected: 12/01/21 14:05 Received: 12/01/21 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/04/21 14:21
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 14:21
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 14:21
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/04/21 14:21
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/04/21 14:21
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/04/21 14:21
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/04/21 14:21
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/04/21 14:21
591-78-6
lodomethane
ND
ug/L
20.0
1
12/04/21 14:21
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/04/21 14:21
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/04/21 14:21
108-10-1
Styrene
ND
ug/L
1.0
1
12/04/21 14:21
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/04/21 14:21
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/04/21 14:21
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/04/21 14:21
127-18-4
Toluene
ND
ug/L
1.0
1
12/04/21 14:21
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/04/21 14:21
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/04/21 14:21
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/04/21 14:21
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/04/21 14:21
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/04/21 14:21
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/04/21 14:21
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/04/21 14:21
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/04/21 14:21
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/04/21 14:21
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/04/21 14:21
95-47-6
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
12/04/21 14:21
460-00-4
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
12/04/21 14:21
17060-07-0
Toluene-d8(S)
100
%
70-130
1
12/04/21 14:21
2037-26-5
Date: 12/10/2021 04:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 25

Pace Analytical Services, LLC
ceAnalyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
Sample: 6001-HBW17B Lab ID: 92575188004 Collected: 12/01/21 14:35 Received: 12/01/21 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2107:18
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/07/21 13:43
12/09/2107:18
7440-38-2
Barium
71.7
ug/L
5.0
1
12/07/21 13:43
12/09/2107:18
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/07/21 13:43
12/09/2107:18
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/07/21 13:43
12/09/2107:18
7440-43-9
Chromium
ND
ug/L
5.0
1
12/07/21 13:43
12/09/21 17:24
7440-47-3
Cobalt
20.7
ug/L
5.0
1
12/07/21 13:43
12/09/2107:18
7440-48-4
Copper
19.7
ug/L
5.0
1
12/07/21 13:43
12/09/21 17:24
7440-50-8
Lead
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2107:18
7439-92-1
Nickel
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2107:18
7440-02-0
Selenium
ND
ug/L
10.0
1
12/07/21 13:43
12/09/2107:18
7782-49-2
Silver
ND
ug/L
5.0
1
12/07/21 13:43
12/09/2107:18
7440-22-4
Thallium
ND
ug/L
10.0
1
12/07/21 13:43
12/09/2107:18
7440-28-0
Vanadium
6.6
ug/L
5.0
1
12/07/21 13:43
12/09/21 17:24
7440-62-2
Zinc
18.1
ug/L
10.0
1
12/07/21 13:43
12/09/2107:18
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
12/07/2111:50
12/07/2123:50
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/04/21 14:39
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/04/21 14:39
107-13-1
Benzene
8.9
ug/L
1.0
1
12/04/21 14:39
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/04/21 14:39
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/04/21 14:39
75-27-4
Bromoform
ND
ug/L
1.0
1
12/04/21 14:39
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/04/21 14:39
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/04/21 14:39
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/04/21 14:39
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/04/21 14:39
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/04/21 14:39
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/04/21 14:39
75-00-3
Chloroform
ND
ug/L
1.0
1
12/04/21 14:39
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/04/21 14:39
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/04/21 14:39
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/04/21 14:39
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/04/21 14:39
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/04/21 14:39
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 14:39
95-50-1
1,4-Dichlorobenzene
1.2
ug/L
1.0
1
12/04/21 14:39
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/04/21 14:39
110-57-6
1,1-Dichloroethane
6.1
ug/L
1.0
1
12/04/21 14:39
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/04/21 14:39
107-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
Sample: 6001-HBW17B Lab ID: 92575188004 Collected: 12/01/21 14:35 Received: 12/01/21 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 12/10/2021 04:46 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
123
ug/L
1.0
ug/L
9.8
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
26.8
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
22.7
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
1.8
ug/L
10.7
ug/L
ND
ug/L
10.7
ug/L
98
%
95
%
100
%
1.0
1
12/04/21 14:39
75-35-4
1.0
1
12/04/21 14:39
156-59-2
1.0
1
12/04/21 14:39
156-60-5
1.0
1
12/04/21 14:39
78-87-5
1.0
1
12/04/21 14:39
10061-01-5
1.0
1
12/04/21 14:39
10061-02-6
1.0
1
12/04/21 14:39
100-41-4
5.0
1
12/04/21 14:39
591-78-6
20.0
1
12/04/21 14:39
74-88-4
5.0
1
12/04/21 14:39
75-09-2
5.0
1
12/04/21 14:39
108-10-1
1.0
1
12/04/21 14:39
100-42-5
1.0
1
12/04/21 14:39
630-20-6
1.0
1
12/04/21 14:39
79-34-5
1.0
1
12/04/21 14:39
127-18-4
1.0
1
12/04/21 14:39
108-88-3
1.0
1
12/04/21 14:39
71-55-6
1.0
1
12/04/21 14:39
79-00-5
1.0
1
12/04/21 14:39
79-01-6
1.0
1
12/04/21 14:39
75-69-4
1.0
1
12/04/21 14:39
96-18-4
2.0
1
12/04/21 14:39
108-05-4
1.0
1
12/04/21 14:39
75-01-4
1.0
1
12/04/21 14:39
1330-20-7
2.0
1
12/04/21 14:39
179601-23-1
1.0
1
12/04/21 14:39
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
12/04/21 14:39 460-00-4
12/04/21 14:39 17060-07-0
12/04/21 14:39 2037-26-5
Page 11 of 25

Pace Analytical Services, LLC
ceAnalyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
Sample: TRIP BLANK Lab ID: 92575188005 Collected: 12/01/21 10:50 Received: 12/01/21 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/04/21 07:24
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/04/21 07:24
107-13-1
Benzene
ND
ug/L
1.0
1
12/04/21 07:24
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/04/21 07:24
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/04/21 07:24
75-27-4
Bromoform
ND
ug/L
1.0
1
12/04/21 07:24
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/04/21 07:24
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/04/21 07:24
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/04/21 07:24
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/04/21 07:24
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/04/21 07:24
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/04/21 07:24
75-00-3
Chloroform
ND
ug/L
1.0
1
12/04/21 07:24
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/04/21 07:24
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/04/21 07:24
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/04/21 07:24
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/04/21 07:24
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/04/21 07:24
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 07:24
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 07:24
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/04/21 07:24
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/04/21 07:24
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/04/21 07:24
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/04/21 07:24
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 07:24
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 07:24
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/04/21 07:24
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/04/21 07:24
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/04/21 07:24
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/04/21 07:24
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/04/21 07:24
591-78-6
lodomethane
ND
ug/L
20.0
1
12/04/21 07:24
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/04/21 07:24
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/04/21 07:24
108-10-1
Styrene
ND
ug/L
1.0
1
12/04/21 07:24
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/04/21 07:24
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/04/21 07:24
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/04/21 07:24
127-18-4
Toluene
ND
ug/L
1.0
1
12/04/21 07:24
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/04/21 07:24
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/04/21 07:24
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/04/21 07:24
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/04/21 07:24
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/04/21 07:24
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/04/21 07:24
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/04/21 07:24
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
Sample: TRIP BLANK
Parameters
Lab ID: 92575188005 Collected: 12/01/21 10:50
Results Units Report Limit DF
Received: 12/01/21 15:45 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
12/04/21 07:24
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
12/04/21 07:24
179601-23-1
o-Xylene
ND ug/L
1.0
1
12/04/21 07:24
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99 %
70-130
1
12/04/21 07:24
460-00-4
1,2-Dichloroethane-d4 (S)
98 %
70-130
1
12/04/21 07:24
17060-07-0
Toluene-d8(S)
100 %
70-130
1
12/04/21 07:24
2037-26-5
Date: 12/10/2021 04:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
QC Batch: 664332 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92575188001, 92575188002, 92575188003, 92575188004
METHOD BLANK: 3479656 Matrix: Water
Associated Lab Samples: 92575188001, 92575188002, 92575188003, 92575188004
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
5.0 12/09/21 05:38
10.0 12/09/21 05:38
5.0 12/09/21 05:38
1.0 12/09/21 05:38
1.0 12/09/21 05:38
5.0 12/09/21 05:38
5.0 12/09/21 05:38
5.0 12/09/21 05:38
5.0 12/09/21 05:38
5.0 12/09/21 05:38
10.0 12/09/21 05:38
5.0 12/09/21 05:38
10.0 12/09/21 05:38
5.0 12/09/21 05:38
10.0 12/09/21 05:38
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3479657
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
549
110
80-120
Arsenic
ug/L
500
493
99
80-120
Barium
ug/L
500
540
108
80-120
Beryllium
ug/L
500
529
106
80-120
Cadmium
ug/L
500
505
101
80-120
Chromium
ug/L
500
485
97
80-120
Cobalt
ug/L
500
506
101
80-120
Copper
ug/L
500
494
99
80-120
Lead
ug/L
500
516
103
80-120
Nickel
ug/L
500
508
102
80-120
Selenium
ug/L
500
521
104
80-120
Silver
ug/L
250
256
102
80-120
Thallium
ug/L
500
500
100
80-120
Vanadium
ug/L
500
500
100
80-120
Zinc
ug/L
500
511
102
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
HARRISBURG RD LANDFILL PERMIT
92575188
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3479658
3479659
MS
MSD
92575770012
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
560
552
112
110
75-125
1
Arsenic
ug/L
ND
500
500
477
467
95
93
75-125
2
Barium
ug/L
34.2
500
500
534
532
100
100
75-125
0
Beryllium
ug/L
ND
500
500
492
490
98
98
75-125
0
Cadmium
ug/L
ND
500
500
484
481
97
96
75-125
1
Chromium
ug/L
ND
500
500
456
455
91
91
75-125
0 E
Cobalt
ug/L
ND
500
500
469
466
94
93
75-125
1
Copper
ug/L
ND
500
500
462
460
92
92
75-125
0 E
Lead
ug/L
ND
500
500
486
481
97
96
75-125
1
Nickel
ug/L
ND
500
500
474
471
95
94
75-125
1
Selenium
ug/L
9.11
500
500
519
510
102
100
75-125
2
Silver
ug/L
ND
250
250
258
257
103
103
75-125
1
Thallium
ug/L
ND
500
500
460
458
92
91
75-125
0
Vanadium
ug/L
ND
500
500
474
479
95
96
75-125
1
Zinc
ug/L
14.5
500
500
502
500
98
97
75-125
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 25

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
QC Batch: 664324 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92575188001, 92575188002, 92575188003, 92575188004
METHOD BLANK: 3479628
Matrix:
Water
Associated Lab Samples: 92575188001, 92575188002, 92575188003, 92575188004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
0.47
12/07/2118:15
LABORATORY CONTROL SAMPLE:
3479629
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
25
23.9
95 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3480738 3480739
MS MSD
92573625015 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 25 25 24.5 24.9 98 100 75-125 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
QC Batch: 663869 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92575188001, 92575188002, 92575188003, 92575188004, 92575188005
METHOD BLANK: 3477561 Matrix: Water
Associated Lab Samples: 92575188001, 92575188002, 92575188003, 92575188004, 92575188005
Blank Reporting
Parameter Units Result Limit Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
12/04/21 06:11
1,1,1-Trichloroethane
ug/L
ND
1.0
12/04/21 06:11
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/04/21 06:11
1,1,2-Trichloroethane
ug/L
ND
1.0
12/04/21 06:11
1,1-Dichloroethane
ug/L
ND
1.0
12/04/21 06:11
1,1-Dichloroethene
ug/L
ND
1.0
12/04/21 06:11
1,2,3-Trichloropropane
ug/L
ND
1.0
12/04/21 06:11
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
12/04/21 06:11
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/04/21 06:11
1,2-Dichlorobenzene
ug/L
ND
1.0
12/04/21 06:11
1,2-Dichloroethane
ug/L
ND
1.0
12/04/21 06:11
1,2-Dichloropropane
ug/L
ND
1.0
12/04/21 06:11
1,4-Dichlorobenzene
ug/L
ND
1.0
12/04/21 06:11
2-Butanone (MEK)
ug/L
ND
5.0
12/04/21 06:11
2-Hexanone
ug/L
ND
5.0
12/04/21 06:11
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/04/21 06:11
Acetone
ug/L
ND
25.0
12/04/21 06:11
Acrylonitrile
ug/L
ND
10.0
12/04/21 06:11
Benzene
ug/L
ND
1.0
12/04/21 06:11
Bromochloromethane
ug/L
ND
1.0
12/04/21 06:11
Bromodichloromethane
ug/L
ND
1.0
12/04/21 06:11
Bromoform
ug/L
ND
1.0
12/04/21 06:11
Bromomethane
ug/L
ND
2.0
12/04/21 06:11
Carbon disulfide
ug/L
ND
2.0
12/04/21 06:11
Carbon tetrachloride
ug/L
ND
1.0
12/04/21 06:11
Chlorobenzene
ug/L
ND
1.0
12/04/21 06:11
Chloroethane
ug/L
ND
1.0
12/04/21 06:11
Chloroform
ug/L
ND
1.0
12/04/21 06:11
Chloromethane
ug/L
ND
1.0
12/04/21 06:11
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/04/21 06:11
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/04/21 06:11
Dibromochloromethane
ug/L
ND
1.0
12/04/21 06:11
Dibromomethane
ug/L
ND
1.0
12/04/21 06:11
Ethylbenzene
ug/L
ND
1.0
12/04/21 06:11
lodomethane
ug/L
ND
20.0
12/04/21 06:11
m&p-Xylene
ug/L
ND
2.0
12/04/21 06:11
Methylene Chloride
ug/L
ND
5.0
12/04/21 06:11
o-Xylene
ug/L
ND
1.0
12/04/21 06:11
Styrene
ug/L
ND
1.0
12/04/21 06:11
Tetrachloroethene
ug/L
ND
1.0
12/04/21 06:11
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
METHOD BLANK: 3477561 Matrix: Water
Associated Lab Samples: 92575188001, 92575188002, 92575188003, 92575188004, 92575188005
Blank Reporting
Parameter Units Result Limit Analyzed
Toluene
ug/L
ND
1.0
12/04/21 06:11
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/04/21 06:11
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/04/21 06:11
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
12/04/21 06:11
Trichloroethene
ug/L
ND
1.0
12/04/21 06:11
Trichlorofluoromethane
ug/L
ND
1.0
12/04/21 06:11
Vinyl acetate
ug/L
ND
2.0
12/04/21 06:11
Vinyl chloride
ug/L
ND
1.0
12/04/21 06:11
Xylene (Total)
ug/L
ND
1.0
12/04/21 06:11
1,2-Dichloroethane-d4 (S)
%
96
70-130
12/04/21 06:11
4-Bromofluorobenzene (S)
%
100
70-130
12/04/21 06:11
Toluene-d8 (S)
%
99
70-130
12/04/21 06:11
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3477562
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
50.3
101
70-130
1,1,1-Trichloroethane
ug/L
50
48.0
96
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
51.7
103
70-130
1,1,2-Trichloroethane
ug/L
50
49.2
98
70-130
1,1-Dichloroethane
ug/L
50
47.7
95
70-130
1,1-Dichloroethene
ug/L
50
47.2
94
70-132
1,2,3-Trichloropropane
ug/L
50
51.1
102
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
57.7
115
70-132
1,2-Dibromoethane (EDB)
ug/L
50
51.8
104
70-130
1,2-Dichlorobenzene
ug/L
50
51.0
102
70-130
1,2-Dichloroethane
ug/L
50
48.1
96
70-130
1,2-Dichloropropane
ug/L
50
49.7
99
70-130
1,4-Dichlorobenzene
ug/L
50
51.4
103
70-130
2-Butanone (MEK)
ug/L
100
98.7
99
70-133
2-Hexanone
ug/L
100
109
109
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
106
106
70-130
Acetone
ug/L
100
101
101
70-144
Acrylonitrile
ug/L
250
239
95
70-130
Benzene
ug/L
50
48.0
96
70-130
Bromochloromethane
ug/L
50
48.0
96
70-130
Bromodichloromethane
ug/L
50
50.0
100
70-130
Bromoform
ug/L
50
52.3
105
70-131
Bromomethane
ug/L
50
59.0
118
30-177
Carbon disulfide
ug/L
50
49.1
98
70-133
Carbon tetrachloride
ug/L
50
49.8
100
70-130
Chlorobenzene
ug/L
50
50.2
100
70-130
Chloroethane
ug/L
50
38.7
77
46-131
Chloroform
ug/L
50
47.6
95
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
LABORATORY CONTROL SAMPLE:
Parameter
3477562
Units
Spike LCS
Conc. Result
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Ethylbenzene
ug/L
50
lodomethane
ug/L
100
m&p-Xylene
ug/L
100
Methylene Chloride
ug/L
50
o-Xylene
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
trans-1,4-Dichloro-2-butene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits
48.0
96
49-130
47.9
96
70-130
48.8
98
70-130
53.1
106
70-130
48.5
97
70-130
50.7
101
70-130
104
104
47-140
103
103
70-130
46.9
94
68-130
50.8
102
70-130
52.5
105
70-130
49.0
98
70-130
48.4
97
70-130
48.3
97
70-130
49.3
99
70-130
62.6
125
25-200
48.1
96
70-130
46.4
93
61-130
99.8
100
70-140
50.9
102
59-142
154
102
70-130
93
70-130
103
70-130
100
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3477563
MS
92575418001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3477564
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
22.6
22.9
113
114
70-135
1
1,1,1-Trichloroethane
ug/L
ND
20
20
19.9
19.8
99
99
70-148
0
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
21.9
22.1
110
111
70-131
1
1,1,2-Trichloroethane
ug/L
ND
20
20
21.1
21.0
105
105
70-136
0
1,1-Dichloroethane
ug/L
ND
20
20
19.2
19.0
96
95
70-147
1
1,1-Dichloroethene
ug/L
ND
20
20
17.8
17.6
89
88
70-158
1
1,2,3-Trichloropropane
ug/L
ND
20
20
20.6
21.0
103
105
67-137
2
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
23.8
24.3
119
121
69-136
2
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.0
21.8
110
109
70-137
1
1,2-Dichlorobenzene
ug/L
ND
20
20
22.8
22.4
114
112
70-133
2
1,2-Dichloroethane
ug/L
ND
20
20
18.5
18.4
93
92
67-138
1
1,2-Dichloropropane
ug/L
ND
20
20
20.6
20.4
103
102
70-138
1
1,4-Dichlorobenzene
ug/L
ND
20
20
23.0
22.6
115
113
70-133
2
2-Butanone (MEK)
ug/L
ND
40
40
36.7
36.8
92
92
61-147
0
2-Hexanone
ug/L
ND
40
40
41.1
41.5
103
104
67-139
1
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
39.1
38.6
98
97
67-136
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3477563
MS
92575418001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3477564
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
33.8
34.1
85
85
55-159
1
Acrylonitrile
ug/L
ND
100
100
86.7
88.0
87
88
68-140
1
Benzene
ug/L
ND
20
20
19.7
19.7
98
98
67-150
0
Bromochloromethane
ug/L
ND
20
20
20.0
20.1
100
101
70-146
1
Bromodichloromethane
ug/L
ND
20
20
20.7
20.6
104
103
70-138
1
Bromoform
ug/L
ND
20
20
21.7
21.8
108
109
57-138
1
Bromomethane
ug/L
ND
20
20
16.4
16.7
82
83
10-200
2 v3
Carbon disulfide
ug/L
ND
20
20
17.6
17.5
88
87
70-152
1
Carbon tetrachloride
ug/L
ND
20
20
20.6
20.8
103
104
70-147
1
Chlorobenzene
ug/L
ND
20
20
21.9
22.4
109
112
70-137
2
Chloroethane
ug/L
ND
20
20
16.1
15.9
81
80
51-166
1 v3
Chloroform
ug/L
ND
20
20
18.9
19.0
95
95
70-144
0
Chloromethane
ug/L
ND
20
20
16.0
16.0
80
80
24-161
0
cis-1,2-Dichloroethene
ug/L
ND
20
20
19.2
19.3
96
96
67-148
0
cis-1,3-Dichloropropene
ug/L
ND
20
20
20.5
20.3
103
101
70-142
1
Dibromochloromethane
ug/L
ND
20
20
22.2
22.4
111
112
68-138
1
Dibromomethane
ug/L
ND
20
20
21.1
20.6
106
103
70-134
3
Ethylbenzene
ug/L
ND
20
20
21.8
22.1
109
111
68-143
2
lodomethane
ug/L
ND
40
40
37.6
37.8
94
95
20-161
0
m&p-Xylene
ug/L
ND
40
40
43.8
44.4
110
111
53-157
1
Methylene Chloride
ug/L
ND
20
20
18.1
17.9
90
89
64-148
1
o-Xylene
ug/L
ND
20
20
21.9
22.0
109
110
68-143
1
Styrene
ug/L
ND
20
20
21.9
22.0
109
110
70-136
0
Tetrachloroethene
ug/L
ND
20
20
21.6
22.0
108
110
70-139
2
Toluene
ug/L
ND
20
20
20.2
20.6
101
103
47-157
2
trans-1,2-Dichloroethene
ug/L
ND
20
20
19.2
18.4
96
92
70-149
4
trans- 1,3-Dichloropropene
ug/L
ND
20
20
20.4
20.3
102
102
70-138
1
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
15.5
18.8
77
94
31-145
20
Trichloroethene
ug/L
ND
20
20
20.9
20.7
105
104
70-149
1
Trichlorofluoromethane
ug/L
ND
20
20
15.8
15.6
79
78
61-154
2 v3
Vinyl acetate
ug/L
ND
40
40
39.2
39.1
98
98
48-156
0
Vinyl chloride
ug/L
ND
20
20
17.2
17.1
86
86
55-172
1
Xylene (Total)
ug/L
ND
60
60
65.7
66.4
110
111
66-145
1
1,2-Dichloroethane-d4 (S)
%
90
87
70-130
4-Bromofluorobenzene (S)
%
98
100
70-130
Toluene-d8(S)
%
98
97
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 25

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92575188
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
E Analyte concentration exceeded the calibration range. The reported result is estimated.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/10/2021 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 25

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
HARRISBURG RD LANDFILL PERMIT
92575188
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92575188001
6001-HBW21
EPA 3010A
664332
EPA6010D
664507
92575188002
6001-HBW22
EPA 3010A
664332
EPA6010D
664507
92575188003
6001-HBW12B
EPA 3010A
664332
EPA6010D
664507
92575188004
6001-HBW17B
EPA 3010A
664332
EPA6010D
664507
92575188001
6001-HBW21
EPA 3010A
664324
EPA6020B
664495
92575188002
6001-HBW22
EPA 3010A
664324
EPA6020B
664495
92575188003
6001-HBW12B
EPA 3010A
664324
EPA6020B
664495
92575188004
6001-HBW17B
EPA 3010A
664324
EPA6020B
664495
92575188001
6001-H BW21
EPA 8260D
663869
92575188002
6001-HBW22
EPA 8260D
663869
92575188003
6001-HBW12B
EPA 8260D
663869
92575188004
6001-HBW17B
EPA 8260D
663869
92575188005
TRIP BLANK
EPA 8260D
663869
Date: 12/10/2021 04:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 22 of 25

Document Name:
Document Revised: November 15, 2021
el
aCBArr�lyflC31
Sample Condition Upon Receipt (SCUR)
Page i of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev,09
Pace Carolinas Quality Office
Laboratory receiving samples: =
Asheville ❑ Eden[] Greenwood ❑ HuntersvilleRl Raleigh❑ Mechanicsville[] Atlanta❑ Kernersville❑
Siimple Condition I Client Name:Upon WQ'#� * 9 2575188
. � - Project •
Couriee ❑Fed Ex ❑UPS ❑USPS ❑Client
❑ Commercial 'QPace []Other: I f I r I
92575188
Custody Seal Present? ❑Yes 'DNo Seals Intact? ❑Yes ❑No
Oate/lnitiaLsPersanEMaminingContents: �C
Packing Material: ❑Bubble Wrap `OBubble Bags []None ❑' Other Biological Tissue Frozen?
Thermornieterr. []Yes❑NO ©N/A
Q IR Gun ID: T( �rWet ❑91ve ❑Nont
✓'�" Type Of ice:
Correction Factor:
CoolerTemp: Add/Subtract('ClP= [ (/ Temp should be above freezing to 6°C
❑5imples out of temp criteria. Samples On ice, cooling process
Eoaler�emp Conected�'H• " -tias be tin
USDA Regulated Soil (E] N/A, water sample]
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? DId samples originate from a foreign source linternationally,
r1yes FINn nrli. V Row„u�i �h� o, an Ri n flu°� flu
Comments/Discrepancy:
Chain of Custody Present?
(1Yes
❑Na
❑NIA
1.
Samples Arrived within Hold Time?
❑r Yes
[]No
❑N/A
2.
Short Hold Tlme Analysis (<72 hr.)?
❑Yes
"j]No
N/A
3.
Rush Turn Around Tlme Requested?
[]Yes
MNo
❑N/A
4.
Sufficient Volume?
n"Yes
❑No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
'OYes
' yes
❑No
[]NO
[-]N/A
❑N/A
6.
Containers Intact?
l_]Yes
[]No
N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
[]No
'0N/A
a.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
Mies
, V
[]No
❑N/A
9.
Headspace in VOA Vials (>S-6mm)?
Yes
©Nn
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
E [Yes
❑Yes
❑No
No
❑N/A
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of spit containers:
CLIENT NOTIFICAVON/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Field Data Requlred? []Yes ❑No
Da te:
I
1
i
Date: j
1
Page 23 of 25
]
i

Document Name: Oocument Revised: November 15, 2021
A Sample Condition Upon Receipt (SCUR) Page 2 of 2
Analytical . ' Document Nn.: Issuing Authority:
F•CAR•CS•033•Rev.06 n..o rnrnIinas Ouality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Caliform,TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to fist number of bottles
Project WO# : 9,2575188
PM: MWB Due Dale: 12/15/21
CLIENT: 92—MECK CO
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leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
December 14, 2021
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: HARRISBURG RD LANDFILL
Pace Project No.: 92575493
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on December 02, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 22

lacmnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: HARRISBURG RD LANDFILL
Pace Project No.: 92575493
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: HARRISBURG RD LANDFILL
Pace Project No.: 92575493
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92575493001 6001-HB2006
EPA 6010D
IDS, RDT
15
PASI-A
EPA 8260D
CL
52
PASI-C
92575493002 6001-HB2008
EPA 6010D
IDS, RDT
15
PASI-A
EPA 8260D
CL
52
PASI-C
92575493003 6001-HB2010
EPA 6010D
IDS, RDT
15
PASI-A
EPA 8260D
CL
52
PASI-C
92575493004 TRIP BLANK
EPA 8260D
CL
52
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL
Pace Project No.: 92575493
Sample: 6001-HB2006
Lab ID: 92575493001 Collected:
12/02/21 10:45
Received: 12/02/21 13:02 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical Method:
EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:46
7440-36-0
L2
Arsenic
ND
ug/L
10.0
1
12/08/2113:19
12/13/2118:46
7440-38-2
L2
Barium
28.2
ug/L
5.0
1
12/08/2113:19
12/13/2118:46
7440-39-3
L2
Beryllium
ND
ug/L
1.0
1
12/08/2113:19
12/13/2118:46
7440-41-7
L2
Cadmium
ND
ug/L
1.0
1
12/08/2113:19
12/13/2118:46
7440-43-9
L2
Chromium
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:46
7440-47-3
L2
Cobalt
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:46
7440-48-4
L2
Copper
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:46
7440-50-8
L2
Lead
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:46
7439-92-1
L2
Nickel
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:46
7440-02-0
L2
Selenium
ND
ug/L
10.0
1
12/08/2113:19
12/13/2118:46
7782-49-2
L2
Silver
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:46
7440-22-4
L2
Thallium
ND
ug/L
10.0
1
12/08/2113:19
12/13/2118:46
7440-28-0
L2
Vanadium
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:46
7440-62-2
L2
Zinc
ND
ug/L
10.0
1
12/08/2113:19
12/13/2118:46
7440-66-6
L2
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/04/21 11:01
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/04/21 11:01
107-13-1
Benzene
ND
ug/L
1.0
1
12/04/21 11:01
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/04/21 11:01
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/04/21 11:01
75-27-4
Bromoform
ND
ug/L
1.0
1
12/04/21 11:01
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/04/21 11:01
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/04/21 11:01
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/04/21 11:01
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/04/21 11:01
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/04/21 11:01
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/04/21 11:01
75-00-3
Chloroform
ND
ug/L
1.0
1
12/04/21 11:01
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/04/21 11:01
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/04/21 11:01
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/04/21 11:01
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/04/21 11:01
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/04/21 11:01
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 11:01
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 11:01
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/04/21 11:01
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/04/21 11:01
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/04/21 11:01
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/04/21 11:01
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 11:01
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 11:01
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
1
12/04/21 11:01
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/04/21 11:01
10061-01-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:45 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL
Pace Project No.: 92575493
Sample: 6001-HB2006 Lab ID: 92575493001 Collected: 12/02/21 10:45 Received: 12/02/21 13:02 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 12/14/2021 04:45 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
1.0
1
12/04/2111:01
10061-02-6
ND
ug/L
1.0
1
12/04/2111:01
100-41-4
ND
ug/L
5.0
1
12/04/2111:01
591-78-6
ND
ug/L
20.0
1
12/04/2111:01
74-88-4
ND
ug/L
5.0
1
12/04/2111:01
75-09-2
ND
ug/L
5.0
1
12/04/2111:01
108-10-1
ND
ug/L
1.0
1
12/04/2111:01
100-42-5
ND
ug/L
1.0
1
12/04/2111:01
630-20-6
ND
ug/L
1.0
1
12/04/2111:01
79-34-5
ND
ug/L
1.0
1
12/04/2111:01
127-18-4
ND
ug/L
1.0
1
12/04/2111:01
108-88-3
ND
ug/L
1.0
1
12/04/2111:01
71-55-6
ND
ug/L
1.0
1
12/04/2111:01
79-00-5
ND
ug/L
1.0
1
12/04/2111:01
79-01-6
ND
ug/L
1.0
1
12/04/2111:01
75-69-4
ND
ug/L
1.0
1
12/04/2111:01
96-18-4
ND
ug/L
2.0
1
12/04/2111:01
108-05-4
ND
ug/L
1.0
1
12/04/2111:01
75-01-4
ND
ug/L
1.0
1
12/04/2111:01
1330-20-7
ND
ug/L
2.0
1
12/04/2111:01
179601-23-1
ND
ug/L
1.0
1
12/04/2111:01
95-47-6
100
%
70-130
1
12/04/2111:01
460-00-4
97
%
70-130
1
12/04/2111:01
17060-07-0
100
%
70-130
1
12/04/2111:01
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL
Pace Project No.: 92575493
Sample: 6001-HB2008
Lab ID: 92575493002 Collected:
12/02/21 11:00
Received: 12/02/21 13:02 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical Method:
EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:49
7440-36-0
L2
Arsenic
ND
ug/L
10.0
1
12/08/2113:19
12/13/2118:49
7440-38-2
L2
Barium
24.2
ug/L
5.0
1
12/08/2113:19
12/13/2118:49
7440-39-3
L2
Beryllium
ND
ug/L
1.0
1
12/08/2113:19
12/13/2118:49
7440-41-7
L2
Cadmium
ND
ug/L
1.0
1
12/08/2113:19
12/13/2118:49
7440-43-9
L2
Chromium
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:49
7440-47-3
L2
Cobalt
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:49
7440-48-4
L2
Copper
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:49
7440-50-8
L2
Lead
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:49
7439-92-1
L2
Nickel
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:49
7440-02-0
L2
Selenium
ND
ug/L
10.0
1
12/08/2113:19
12/13/2118:49
7782-49-2
L2
Silver
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:49
7440-22-4
L2
Thallium
ND
ug/L
10.0
1
12/08/2113:19
12/13/2118:49
7440-28-0
L2
Vanadium
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:49
7440-62-2
L2
Zinc
ND
ug/L
10.0
1
12/08/2113:19
12/13/2118:49
7440-66-6
L2
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/04/21 11:20
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/04/21 11:20
107-13-1
Benzene
ND
ug/L
1.0
1
12/04/21 11:20
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/04/21 11:20
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/04/21 11:20
75-27-4
Bromoform
ND
ug/L
1.0
1
12/04/21 11:20
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/04/21 11:20
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/04/21 11:20
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/04/21 11:20
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/04/21 11:20
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/04/21 11:20
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/04/21 11:20
75-00-3
Chloroform
ND
ug/L
1.0
1
12/04/21 11:20
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/04/21 11:20
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/04/21 11:20
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/04/21 11:20
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/04/21 11:20
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/04/21 11:20
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 11:20
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 11:20
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/04/21 11:20
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/04/21 11:20
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/04/21 11:20
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/04/21 11:20
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 11:20
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 11:20
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
1
12/04/21 11:20
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/04/21 11:20
10061-01-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:45 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL
Pace Project No.: 92575493
Sample: 6001-HB2008 Lab ID: 92575493002 Collected: 12/02/21 11:00 Received: 12/02/21 13:02 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 12/14/2021 04:45 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
1.0
1
12/04/2111:20
10061-02-6
ND
ug/L
1.0
1
12/04/2111:20
100-41-4
ND
ug/L
5.0
1
12/04/2111:20
591-78-6
ND
ug/L
20.0
1
12/04/2111:20
74-88-4
ND
ug/L
5.0
1
12/04/2111:20
75-09-2
ND
ug/L
5.0
1
12/04/2111:20
108-10-1
ND
ug/L
1.0
1
12/04/2111:20
100-42-5
ND
ug/L
1.0
1
12/04/2111:20
630-20-6
ND
ug/L
1.0
1
12/04/2111:20
79-34-5
ND
ug/L
1.0
1
12/04/2111:20
127-18-4
ND
ug/L
1.0
1
12/04/2111:20
108-88-3
ND
ug/L
1.0
1
12/04/2111:20
71-55-6
ND
ug/L
1.0
1
12/04/2111:20
79-00-5
ND
ug/L
1.0
1
12/04/2111:20
79-01-6
ND
ug/L
1.0
1
12/04/2111:20
75-69-4
ND
ug/L
1.0
1
12/04/2111:20
96-18-4
ND
ug/L
2.0
1
12/04/2111:20
108-05-4
ND
ug/L
1.0
1
12/04/2111:20
75-01-4
ND
ug/L
1.0
1
12/04/2111:20
1330-20-7
ND
ug/L
2.0
1
12/04/2111:20
179601-23-1
ND
ug/L
1.0
1
12/04/2111:20
95-47-6
99
%
70-130
1
12/04/2111:20
460-00-4
99
%
70-130
1
12/04/2111:20
17060-07-0
100
%
70-130
1
12/04/2111:20
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL
Pace Project No.: 92575493
Sample: 6001-HB2010
Lab ID: 92575493003 Collected:
12/02/21 09:50
Received: 12/02/21 13:02 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical Method:
EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:53
7440-36-0
L2
Arsenic
ND
ug/L
10.0
1
12/08/2113:19
12/13/2118:53
7440-38-2
L2
Barium
37.8
ug/L
5.0
1
12/08/2113:19
12/13/2118:53
7440-39-3
L2
Beryllium
ND
ug/L
1.0
1
12/08/2113:19
12/13/2118:53
7440-41-7
L2
Cadmium
ND
ug/L
1.0
1
12/08/2113:19
12/13/2118:53
7440-43-9
L2
Chromium
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:53
7440-47-3
L2
Cobalt
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:53
7440-48-4
L2
Copper
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:53
7440-50-8
L2
Lead
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:53
7439-92-1
L2
Nickel
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:53
7440-02-0
L2
Selenium
ND
ug/L
10.0
1
12/08/2113:19
12/13/2118:53
7782-49-2
L2
Silver
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:53
7440-22-4
L2
Thallium
ND
ug/L
10.0
1
12/08/2113:19
12/13/2118:53
7440-28-0
L2
Vanadium
ND
ug/L
5.0
1
12/08/2113:19
12/13/2118:53
7440-62-2
L2
Zinc
ND
ug/L
10.0
1
12/08/2113:19
12/13/2118:53
7440-66-6
L2
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/04/21 11:38
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/04/21 11:38
107-13-1
Benzene
ND
ug/L
1.0
1
12/04/21 11:38
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/04/21 11:38
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/04/21 11:38
75-27-4
Bromoform
ND
ug/L
1.0
1
12/04/21 11:38
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/04/21 11:38
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/04/21 11:38
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/04/21 11:38
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/04/21 11:38
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/04/21 11:38
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/04/21 11:38
75-00-3
Chloroform
ND
ug/L
1.0
1
12/04/21 11:38
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/04/21 11:38
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/04/21 11:38
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/04/21 11:38
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/04/21 11:38
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/04/21 11:38
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 11:38
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 11:38
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/04/21 11:38
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/04/21 11:38
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/04/21 11:38
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/04/21 11:38
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 11:38
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 11:38
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
1
12/04/21 11:38
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/04/21 11:38
10061-01-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:45 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL
Pace Project No.: 92575493
Sample: 6001-HB2010 Lab ID: 92575493003 Collected: 12/02/21 09:50 Received: 12/02/21 13:02 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 12/14/2021 04:45 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
1.0
1
12/04/2111:38
10061-02-6
ND
ug/L
1.0
1
12/04/2111:38
100-41-4
ND
ug/L
5.0
1
12/04/2111:38
591-78-6
ND
ug/L
20.0
1
12/04/2111:38
74-88-4
ND
ug/L
5.0
1
12/04/2111:38
75-09-2
ND
ug/L
5.0
1
12/04/2111:38
108-10-1
ND
ug/L
1.0
1
12/04/2111:38
100-42-5
ND
ug/L
1.0
1
12/04/2111:38
630-20-6
ND
ug/L
1.0
1
12/04/2111:38
79-34-5
ND
ug/L
1.0
1
12/04/2111:38
127-18-4
ND
ug/L
1.0
1
12/04/2111:38
108-88-3
ND
ug/L
1.0
1
12/04/2111:38
71-55-6
ND
ug/L
1.0
1
12/04/2111:38
79-00-5
ND
ug/L
1.0
1
12/04/2111:38
79-01-6
ND
ug/L
1.0
1
12/04/2111:38
75-69-4
ND
ug/L
1.0
1
12/04/2111:38
96-18-4
ND
ug/L
2.0
1
12/04/2111:38
108-05-4
ND
ug/L
1.0
1
12/04/2111:38
75-01-4
ND
ug/L
1.0
1
12/04/2111:38
1330-20-7
ND
ug/L
2.0
1
12/04/2111:38
179601-23-1
ND
ug/L
1.0
1
12/04/2111:38
95-47-6
99
%
70-130
1
12/04/2111:38
460-00-4
96
%
70-130
1
12/04/2111:38
17060-07-0
101
%
70-130
1
12/04/2111:38
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL
Pace Project No.: 92575493
Sample: TRIP BLANK Lab ID: 92575493004 Collected: 12/02/21 10:15 Received: 12/02/21 13:02 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/04/21 08:18
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/04/21 08:18
107-13-1
Benzene
ND
ug/L
1.0
1
12/04/21 08:18
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/04/21 08:18
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/04/21 08:18
75-27-4
Bromoform
ND
ug/L
1.0
1
12/04/21 08:18
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/04/21 08:18
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/04/21 08:18
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/04/21 08:18
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/04/21 08:18
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/04/21 08:18
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/04/21 08:18
75-00-3
Chloroform
ND
ug/L
1.0
1
12/04/21 08:18
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/04/21 08:18
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/04/21 08:18
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/04/21 08:18
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/04/21 08:18
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/04/21 08:18
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 08:18
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/04/21 08:18
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/04/21 08:18
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/04/21 08:18
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/04/21 08:18
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/04/21 08:18
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 08:18
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/04/21 08:18
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/04/21 08:18
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/04/21 08:18
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/04/21 08:18
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/04/21 08:18
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/04/21 08:18
591-78-6
lodomethane
ND
ug/L
20.0
1
12/04/21 08:18
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/04/21 08:18
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/04/21 08:18
108-10-1
Styrene
ND
ug/L
1.0
1
12/04/21 08:18
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/04/21 08:18
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/04/21 08:18
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/04/21 08:18
127-18-4
Toluene
ND
ug/L
1.0
1
12/04/21 08:18
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/04/21 08:18
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/04/21 08:18
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/04/21 08:18
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/04/21 08:18
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/04/21 08:18
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/04/21 08:18
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/04/21 08:18
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:45 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 22

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ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL
Pace Project No.: 92575493
Sample: TRIP BLANK
Parameters
Lab ID: 92575493004 Collected: 12/02/21 10:15
Results Units Report Limit DF
Received: 12/02/21 13:02 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
12/04/21 08:18
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
12/04/21 08:18
179601-23-1
o-Xylene
ND ug/L
1.0
1
12/04/21 08:18
95-47-6
Surrogates
4-Bromofluorobenzene (S)
100 %
70-130
1
12/04/21 08:18
460-00-4
1,2-Dichloroethane-d4 (S)
97 %
70-130
1
12/04/21 08:18
17060-07-0
Toluene-d8(S)
99 %
70-130
1
12/04/21 08:18
2037-26-5
Date: 12/14/2021 04:45 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 22

leAnalyiical
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9800 Kincey Ave. Suite 100
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QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL
Pace Project No.: 92575493
QC Batch: 664667 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92575493001, 92575493002, 92575493003
METHOD BLANK: 3481424 Matrix: Water
Associated Lab Samples: 92575493001, 92575493002, 92575493003
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
5.0 12/13/21 07:59
10.0 12/13/21 18:16
5.0 12/13/21 07:59
1.0 12/13/21 07:59
1.0 12/13/21 07:59
5.0 12/13/21 07:59
5.0 12/13/21 07:59
5.0 12/13/21 07:59
5.0 12/13/21 07:59
5.0 12/13/21 07:59
10.0 12/13/21 18:16
5.0 12/13/21 07:59
10.0 12/13/21 07:59
5.0 12/13/21 07:59
10.0 12/13/21 07:59
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3481425
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
549
110
80-120
Arsenic
ug/L
500
506
101
80-120
Barium
ug/L
500
534
107
80-120
Beryllium
ug/L
500
527
105
80-120
Cadmium
ug/L
500
514
103
80-120
Chromium
ug/L
500
495
99
80-120
Cobalt
ug/L
500
517
103
80-120
Copper
ug/L
500
530
106
80-120
Lead
ug/L
500
536
107
80-120
Nickel
ug/L
500
517
103
80-120
Selenium
ug/L
500
495
99
80-120
Silver
ug/L
250
253
101
80-120
Thallium
ug/L
500
514
103
80-120
Vanadium
ug/L
500
505
101
80-120
Zinc
ug/L
500
524
105
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:45 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 22

leAnalyiical
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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
HARRISBURG RD LANDFILL
92575493
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3481426
3481427
MS
MSD
92574998010
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
457
495
91
99
75-125
8
Arsenic
ug/L
ND
500
500
441
484
88
97
75-125
9
Barium
ug/L
17.1
500
500
470
476
91
92
75-125
1
Beryllium
ug/L
ND
500
500
451
458
90
91
75-125
1
Cadmium
ug/L
ND
500
500
455
487
91
97
75-125
7
Chromium
ug/L
ND
500
500
445
481
89
96
75-125
8
Cobalt
ug/L
ND
500
500
438
470
87
94
75-125
7
Copper
ug/L
ND
500
500
453
490
91
98
75-125
8
Lead
ug/L
ND
500
500
454
487
90
97
75-125
7
Nickel
ug/L
ND
500
500
451
483
90
96
75-125
7
Selenium
ug/L
ND
500
500
459
500
92
100
75-125
9
Silver
ug/L
ND
250
250
222
239
89
96
75-125
7
Thallium
ug/L
ND
500
500
447
483
89
97
75-125
8
Vanadium
ug/L
ND
500
500
440
480
88
96
75-125
9
Zinc
ug/L
ND
500
500
450
484
89
96
75-125
7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:45 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 22

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL
Pace Project No.: 92575493
QC Batch: 663872 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92575493001, 92575493002, 92575493003, 92575493004
METHOD BLANK: 3477583 Matrix: Water
Associated Lab Samples: 92575493001, 92575493002, 92575493003, 92575493004
Blank Reporting
Parameter Units Result Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
12/04/21 06:29
1,1,1-Trichloroethane
ug/L
ND
1.0
12/04/21 06:29
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/04/21 06:29
1,1,2-Trichloroethane
ug/L
ND
1.0
12/04/21 06:29
1,1-Dichloroethane
ug/L
ND
1.0
12/04/21 06:29
1,1-Dichloroethene
ug/L
ND
1.0
12/04/21 06:29
1,2,3-Trichloropropane
ug/L
ND
1.0
12/04/21 06:29
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
12/04/21 06:29
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/04/21 06:29
1,2-Dichlorobenzene
ug/L
ND
1.0
12/04/21 06:29
1,2-Dichloroethane
ug/L
ND
1.0
12/04/21 06:29
1,2-Dichloropropane
ug/L
ND
1.0
12/04/21 06:29
1,4-Dichlorobenzene
ug/L
ND
1.0
12/04/21 06:29
2-Butanone (MEK)
ug/L
ND
5.0
12/04/21 06:29
2-Hexanone
ug/L
ND
5.0
12/04/21 06:29
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/04/21 06:29
Acetone
ug/L
ND
25.0
12/04/21 06:29
Acrylonitrile
ug/L
ND
10.0
12/04/21 06:29
Benzene
ug/L
ND
1.0
12/04/21 06:29
Bromochloromethane
ug/L
ND
1.0
12/04/21 06:29
Bromodichloromethane
ug/L
ND
1.0
12/04/21 06:29
Bromoform
ug/L
ND
1.0
12/04/21 06:29
Bromomethane
ug/L
ND
2.0
12/04/21 06:29
Carbon disulfide
ug/L
ND
2.0
12/04/21 06:29
Carbon tetrachloride
ug/L
ND
1.0
12/04/21 06:29
Chlorobenzene
ug/L
ND
1.0
12/04/21 06:29
Chloroethane
ug/L
ND
1.0
12/04/21 06:29
Chloroform
ug/L
ND
1.0
12/04/21 06:29
Chloromethane
ug/L
ND
1.0
12/04/21 06:29
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/04/21 06:29
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/04/21 06:29
Dibromochloromethane
ug/L
ND
1.0
12/04/21 06:29
Dibromomethane
ug/L
ND
1.0
12/04/21 06:29
Ethylbenzene
ug/L
ND
1.0
12/04/21 06:29
lodomethane
ug/L
ND
20.0
12/04/21 06:29
m&p-Xylene
ug/L
ND
2.0
12/04/21 06:29
Methylene Chloride
ug/L
ND
5.0
12/04/21 06:29
o-Xylene
ug/L
ND
1.0
12/04/21 06:29
Styrene
ug/L
ND
1.0
12/04/21 06:29
Tetrachloroethene
ug/L
ND
1.0
12/04/21 06:29
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:45 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 22

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL
Pace Project No.: 92575493
METHOD BLANK: 3477583 Matrix: Water
Associated Lab Samples: 92575493001, 92575493002, 92575493003, 92575493004
Blank Reporting
Parameter Units Result Limit
Analyzed
Toluene
ug/L
ND
1.0
12/04/21 06:29
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/04/21 06:29
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/04/21 06:29
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
12/04/21 06:29
Trichloroethene
ug/L
ND
1.0
12/04/21 06:29
Trichlorofluoromethane
ug/L
ND
1.0
12/04/21 06:29
Vinyl acetate
ug/L
ND
2.0
12/04/21 06:29
Vinyl chloride
ug/L
ND
1.0
12/04/21 06:29
Xylene (Total)
ug/L
ND
1.0
12/04/21 06:29
1,2-Dichloroethane-d4 (S)
%
96
70-130
12/04/21 06:29
4-Bromofluorobenzene (S)
%
100
70-130
12/04/21 06:29
Toluene-d8 (S)
%
100
70-130
12/04/21 06:29
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3477584
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.0
102
70-130
1,1,1-Trichloroethane
ug/L
50
49.3
99
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.9
102
70-130
1,1,2-Trichloroethane
ug/L
50
48.9
98
70-130
1,1-Dichloroethane
ug/L
50
49.1
98
70-130
1,1-Dichloroethene
ug/L
50
49.5
99
70-132
1,2,3-Trichloropropane
ug/L
50
50.1
100
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
55.1
110
70-132
1,2-Dibromoethane (EDB)
ug/L
50
50.7
101
70-130
1,2-Dichlorobenzene
ug/L
50
50.5
101
70-130
1,2-Dichloroethane
ug/L
50
49.0
98
70-130
1,2-Dichloropropane
ug/L
50
50.4
101
70-130
1,4-Dichlorobenzene
ug/L
50
50.7
101
70-130
2-Butanone (MEK)
ug/L
100
94.7
95
70-133
2-Hexanone
ug/L
100
104
104
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
101
101
70-130
Acetone
ug/L
100
96.2
96
70-144
Acrylonitrile
ug/L
250
233
93
70-130
Benzene
ug/L
50
48.6
97
70-130
Bromochloromethane
ug/L
50
48.9
98
70-130
Bromodichloromethane
ug/L
50
50.5
101
70-130
Bromoform
ug/L
50
51.3
103
70-131
Bromomethane
ug/L
50
57.6
115
30-177
Carbon disulfide
ug/L
50
49.9
100
70-133
Carbon tetrachloride
ug/L
50
50.5
101
70-130
Chlorobenzene
ug/L
50
50.6
101
70-130
Chloroethane
ug/L
50
43.1
86
46-131
Chloroform
ug/L
50
48.3
97
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:45 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 22

leAnalyiical
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QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL
Pace Project No.: 92575493
LABORATORY CONTROL SAMPLE:
Parameter
3477584
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Chloromethane
ug/L
50
50.0
100
49-130
cis-1,2-Dichloroethene
ug/L
50
49.2
98
70-130
cis-1,3-Dichloropropene
ug/L
50
49.4
99
70-130
Dibromochloromethane
ug/L
50
52.2
104
70-130
Dibromomethane
ug/L
50
48.8
98
70-130
Ethylbenzene
ug/L
50
51.2
102
70-130
lodomethane
ug/L
100
111
111
47-140
m&p-Xylene
ug/L
100
104
104
70-130
Methylene Chloride
ug/L
50
47.8
96
68-130
o-Xylene
ug/L
50
51.4
103
70-130
Styrene
ug/L
50
52.5
105
70-130
Tetrachloroethene
ug/L
50
49.7
99
70-130
Toluene
ug/L
50
49.0
98
70-130
trans-1,2-Dichloroethene
ug/L
50
49.6
99
70-130
trans- 1,3-Dichloropropene
ug/L
50
49.3
99
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
60.7
121
25-200
Trichloroethene
ug/L
50
49.5
99
70-130
Trichlorofluoromethane
ug/L
50
47.7
95
61-130
Vinyl acetate
ug/L
100
99.3
99
70-140
Vinyl chloride
ug/L
50
52.3
105
59-142
Xylene (Total)
ug/L
150
155
103
70-130
1,2-Dichloroethane-d4 (S)
%
96
70-130
4-Bromofluorobenzene (S)
%
102
70-130
Toluene-d8 (S)
%
100
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3477585
MS
92575083005 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3477586
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
24.1
22.6
121
113
70-135
7
1,1,1-Trichloroethane
ug/L
ND
20
20
20.4
19.4
102
97
70-148
5
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
23.5
22.3
118
111
70-131
5
1,1,2-Trichloroethane
ug/L
ND
20
20
22.4
21.2
112
106
70-136
5
1,1-Dichloroethane
ug/L
ND
20
20
19.6
19.0
98
95
70-147
3
1,1-Dichloroethene
ug/L
ND
20
20
18.1
17.7
90
89
70-158
2
1,2,3-Trichloropropane
ug/L
ND
20
20
22.2
21.1
111
106
67-137
5
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
25.8
24.7
129
124
69-136
4
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
23.5
22.3
117
112
70-137
5
1,2-Dichlorobenzene
ug/L
ND
20
20
23.8
22.6
119
113
70-133
5
1,2-Dichloroethane
ug/L
ND
20
20
19.5
18.6
97
93
67-138
5
1,2-Dichloropropane
ug/L
ND
20
20
21.6
20.4
108
102
70-138
6
1,4-Dichlorobenzene
ug/L
ND
20
20
23.9
22.6
120
113
70-133
6
2-Butanone (MEK)
ug/L
ND
40
40
39.2
38.6
98
96
61-147
2
2-Hexanone
ug/L
ND
40
40
44.7
43.6
112
109
67-139
3
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
41.9
40.6
105
101
67-136
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:45 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL
Pace Project No.: 92575493
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3477585
MS
92575083005 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3477586
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
36.5
35.6
91
89
55-159
3
Acrylonitrile
ug/L
ND
100
100
92.6
91.1
93
91
68-140
2
Benzene
ug/L
ND
20
20
20.5
19.6
102
98
67-150
4
Bromochloromethane
ug/L
ND
20
20
20.8
20.1
104
101
70-146
3
Bromodichloromethane
ug/L
ND
20
20
22.1
20.5
110
103
70-138
7
Bromoform
ug/L
ND
20
20
23.3
22.1
116
111
57-138
5
Bromomethane
ug/L
ND
20
20
16.0
16.1
80
80
10-200
0 v3
Carbon disulfide
ug/L
ND
20
20
18.1
17.4
91
87
70-152
4
Carbon tetrachloride
ug/L
ND
20
20
21.0
20.6
105
103
70-147
2
Chlorobenzene
ug/L
ND
20
20
23.3
22.1
116
111
70-137
5
Chloroethane
ug/L
ND
20
20
16.9
15.9
85
79
51-166
6 v3
Chloroform
ug/L
ND
20
20
19.7
19.0
98
95
70-144
4
Chloromethane
ug/L
ND
20
20
16.4
16.0
82
80
24-161
3
cis-1,2-Dichloroethene
ug/L
ND
20
20
20.1
19.2
101
96
67-148
5
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.8
20.4
109
102
70-142
7
Dibromochloromethane
ug/L
ND
20
20
23.9
22.3
120
111
68-138
7
Dibromomethane
ug/L
ND
20
20
22.3
21.1
112
106
70-134
6
Ethylbenzene
ug/L
ND
20
20
22.9
22.0
115
110
68-143
4
lodomethane
ug/L
ND
40
40
39.3
37.0
98
93
20-161
6
m&p-Xylene
ug/L
ND
40
40
45.9
44.1
115
110
53-157
4
Methylene Chloride
ug/L
ND
20
20
18.9
17.9
95
89
64-148
6
o-Xylene
ug/L
ND
20
20
23.2
22.0
116
110
68-143
6
Styrene
ug/L
ND
20
20
23.1
22.0
116
110
70-136
5
Tetrachloroethene
ug/L
ND
20
20
22.1
21.7
111
108
70-139
2
Toluene
ug/L
ND
20
20
21.2
20.4
106
102
47-157
4
trans-1,2-Dichloroethene
ug/L
ND
20
20
19.8
18.2
99
91
70-149
8
trans- 1,3-Dichloropropene
ug/L
ND
20
20
21.8
20.0
109
100
70-138
9
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
20.2
16.3
101
81
31-145
22
Trichloroethene
ug/L
ND
20
20
21.4
20.6
107
103
70-149
4
Trichlorofluoromethane
ug/L
ND
20
20
15.9
15.3
80
77
61-154
4 v3
Vinyl acetate
ug/L
ND
40
40
42.6
40.1
106
100
48-156
6
Vinyl chloride
ug/L
ND
20
20
17.8
17.1
89
85
55-172
4
Xylene (Total)
ug/L
ND
60
60
69.2
66.1
115
110
66-145
5
1,2-Dichloroethane-d4 (S)
%
91
88
70-130
4-Bromofluorobenzene (S)
%
100
100
70-130
Toluene-d8(S)
%
98
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:45 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 22

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: HARRISBURG RD LANDFILL
Pace Project No.: 92575493
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2021 04:45 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 22

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: HARRISBURG RD LANDFILL
Pace Project No.: 92575493
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92575493001
6001-HB2006
EPA 3010A
664667
EPA6010D
664812
92575493002
6001-HB2008
EPA 3010A
664667
EPA6010D
664812
92575493003
6001-HB2010
EPA 3010A
664667
EPA6010D
664812
92575493001
6001-HB2006
EPA 8260D
663872
92575493002
6001-HB2008
EPA 8260D
663872
92575493003
6001-HB2010
EPA 8260D
663872
92575493004
TRIP BLANK
EPA 8260D
663872
Date: 12/14/2021 04:45 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 22

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