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HomeMy WebLinkAbout4101_Guilford_HighPoint_MSWLF_Seaboard_2021AnnualGW_FID1628542_2021120Environmental Compliance and Remediation Babb & Associates, PA. December 20, 2021 Mr. Eric B. Aufderhaar, P.G., Environmental Program Consultant Ms. Jackie Drummond, Hydrogeologist NC Division of Waste Management 1646 Mail Service Center Raleigh, North Carolina 27699-1646 Re: 2021 Annual Water Quality Monitoring Report Former Seaboard Chemical/Riverdale Drive Landfill Site Jamestown, North Carolina EPA ID No. NCD 071 574 164 NC DEQ Landfill Permit No. 41-01 Dear Eric and Jackie: Please find attached the 2021 Annual Water Quality Monitoring Report for the former Seaboard Chemical/Riverdale Drive Landfill Site in Jamestown, North Carolina. If there are any questions or comments regarding this report, please contact the undersigned at (919) 605-4719. Respectfully, Babb & Associates, P.A. Gary D. Babb, P.G. President Enclosure Cc: Robby Stone Craig Coslette Mike Spencer Electronic Data - Email CD (data loaded: Yes / No ) Doc/Event #: NC DENR I IEnvironmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). • Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. • Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). • Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Manitolriag Dat Sub6iitt4l lnfor'mAion.; ; .. . Name of entity submitting data (laboratory, consultant, facility owner): Babb & Associates, P.A. Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Gary D. Babb E-mail: gdbabb@gmail.com Phone: 919/605-4719 NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006) Closed Riverdale Drive Landfill SR 1145 41-01 .0500 October 21-28, 2021 High Point, NC Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring ❑ Detection Monitoring of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells Groundwater monitoring data from private water supply wells Leachate monitoring data Siirface water monitoring data F El ❑ Assessment Monitoring ❑X Corrective Action Methane gas monitoring data Corrective action data (specify) Annual Monitoring Other(specify) No tification attached? No. No groundwater or surface water standards were exceeded. Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. ❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true ana correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Gary D. Babb Licensed Geologist 919/605-4719 Facility Rsentative,�Jary�(Pri t�j Title (Area Code) Telephone Number r // l/ �/ November 23, 2021 Affix NC Licensed/ Professional Geologist Seal Signat re / , Date Babb & Associates, P.A., 5506 Bradford Pear Ct., Raleigh, NC 27606 Facility Representative Address NC PE Firm License Number (if applicable effective May 1, 2009) °f EAL 488 C'-'0 L o G\��;���,as •,,��%�,�' ............ • Pip f ��"tillI it uNNN% Water Quality Monitoring Report Former Seaboard Chemical/Riverdale Drive Landfill 5899 Riverdale Drive Jamestown, North Carolina Permit No. 41-01 NCD 071 574 164 Prepared for: Seaboard Group II and City of High Point High Point, NC Prepared by: Babb & Associates, P.A. 5506 Bradford Pear Court Raleigh, North Carolina 27606 October 2021 Gary D. Babb, Licensed Geologist o. rzr SEAL i 488 Cj ti Babb & Associates, P.A. Table of Contents 1.0 Introduction 1.1 Site Information 1.2 Site Geology 1.3 Site Hydrogeology 2.0 Water Quality Monitoring Program 2.1 Groundwater Monitoring Network 2.2 Surface Water Monitoring Network 3.0 Water Quality Sample Collection 3.1 Field Sample Procedures 3.2 Field Quality Assurance 3.3 Sample Delivery/Chain-of-Custody 4.0 Laboratory Analysis 5.0 Hydrogeological Conditions 6.0 Laboratory Analytical Results 6.1 Groundwater Analytical Results 6.2 Surface Water Analytical Results 6.3 Quality Control Samples 7.0 Conclusions Figure 1 Site Location Map Figure 2 Groundwater Potentiometric Map Figure 3 1,2-Dichloroethane Isoconcentration Map Figure 4 Vinyl Chloride Isoconcentration Map Figure 5 Chlorobenzene Isoconcentration Map Figure 6 1,4-Dioxane Isoconcentration Map Figure 7 Total Volatile Organic Compound Isoconcentration Map Table 1 Monitoring Well Construction/Groundwater Elevations Table 2 Groundwater VOC Concentrations Table 3 Surface Water VOC Concentrations Table 4 Field Parameters Table 5 Monitoring Well Lat/Long and Elevations Appendix A ENCO Laboratory Analytical Report 1 6 8 11 12 13 18 1.0 Introduction 1.1 Site Information The former Seaboard Chemical/Riverdale Drive Landfill Site (the Site) is located approximately five miles east-southeast of High Point, NC near the intersection of Riverdale Drive and Interstate 85 (Figure 1). The Site consists of two properties, the facility where the former Seaboard Chemical Corporation (Seaboard) conducted operations and the closed municipal Riverdale Drive Landfill (Landfill), as shown on Figure 2. The former Seaboard Facility is located at 5899 Riverdale Drive, Jamestown, NC and consists of approximately 13 acres. Between 1974 and 1989, Seaboard operated solvent recovery and fuel blending processes at the facility. The corporation declared bankruptcy in 1989 and was not able to fund the cost of performing the necessary site closure and remediation. Removal activities were conducted during 1990 and 1992 to remove all remaining waste materials and certain tanks and equipment from the former Seaboard Facility. The removal was conducted by Seaboard Group I which was formed by parties that may have used the services of Seaboard in the past. The adjacent Landfill, a closed unlined municipal solid waste facility, consists of approximately 150 acres and bounds the former Seaboard Facility on two sides. The Landfill was operated from the 1950's until October 1993. The Landfill was permitted by the North Carolina DEQ Solid Waste Section in 1979. During Landfill operations, sections of the two tributary streams that cross the landfill property were piped and solid waste was used to fill the drainage valleys. The two streams are referred to as the Southern Intermittent Stream and the Northern Intermittent Stream. During filling of the Southern Intermittent Stream valley, a leachate collection system was installed adjacent to the stream channel to collect leachate migrating from the overlying solid waste. In Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report October 2021 Page 1 1989, a leachate collection system was added to control surface seeps (leachate leaks) along the slopes of the Landfill. From approximately 1966 to 1970, Landfill operations also included the disposal and open burning of spent solvents in shallow pits located just north of the former Landfill scale house (Figure 2). Periodically, these burn pits were cleaned of residue that accumulated in a mound to the south of the burn pits. Presently, this mound consists of approximately 600 cubic yards of contaminated residue capped by a synthetic liner and is referred to as the "soil residue mound". The Landfill is now capped and maintained under an approved post -closure plan. Seaboard Group II was formed in 1994 and entered into an agreement with the City of High Point (the City) to jointly perform a remedial investigation and prepare a baseline risk assessment and feasibility study for the Site, including both the former Seaboard Facility and closed Landfill properties. The Seaboard Group II and the City then entered into an Administrative Order on Consent (AOC) dated January 30, 1996 with NC DEQ to perform the remedial investigation. The feasibility study was conducted under a separate AOC dated July 22, 1997. Remedial investigations conducted at the Site have documented the presence of chlorinated and non -chlorinated volatile organic compounds (VOCs) in soils, leachate, groundwater, and surface water. The results from the remedial investigation indicate that the VOC-affected groundwater had migrated toward Randleman Lake, which adjoins the Site along the northern and eastern property boundary of the Landfill. The Randleman Lake was created by the impoundment of the Deep River in 2006 by the Randleman Lake Dam, which is located approximately 11.5 miles downstream of the Site. The Remedial Recommendation Document (February 2005) presented a remedial strategy for the impacted media at the Site based on the results of the remedial investigation, baseline risk assessment, and feasibility study. The remedial design consisted of groundwater extraction and treatment in combination with institutional controls including site access control, recorded land use restrictions, and restriction of water Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report October 2021 Page 2 supply well construction. The groundwater and surface water monitoring program is designed to evaluate the effectiveness of the remedy. The Remedial Recommendation Document was conditionally approved by the NC DEQ in September 2005. Seaboard Group II and the City entered into a Remedial Action Settlement Agreement (RASA) with NC DEQ on December 29, 2008. The RASA provides for the design and implementation of the approved remedial action program for the Site as well as completion and reporting of annual groundwater and surface water monitoring activities. 1.2 Site Geology The Site is located in the central Piedmont Physiographic Province in the northern portion of the Carolina Slate Belt. Granite is the predominant rock type in the area and outcrops are observed along the creeks and within the Site. The geology of the Site consists of fractured granitic gneiss which has been intruded by mafic dikes. The mafic dikes are generally oriented N20°E and are sub -vertical, dipping to both the northwest and the southeast. The mafic dikes generally do not occur as single massive tabular bodies but normally occur as a swarm of thinner tabular and/or irregular dikes within larger fracture zones within the granitic gneiss. The thickness of individual mafic dikes ranges from less than one foot to more than 30 feet. Smaller mafic dikes that are not associated with fracture zones are disseminated throughout the granitic gneiss. Several prominent geologic structures have been identified and mapped at the Site, including these significant geologic features: Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report October 2021 Page 3 Southern Intermittent Stream Fault — N80°E oriented fracture zone/fault that parallels the Southern Intermittent Stream. Based on an on -site outcrop measurement and fracture orientation data from the PW-31) core, the fracture zone is believed to dip 43' to the south; Seaboard Dike — N20°E oriented mafic dike that extends from the Seaboard Facility to the vicinity of monitoring well PW-13I and north of the Deep River; PW-5D Dike/Fault — N200E oriented diabase dike/fault that extends northward from the east side of the Seaboard Facility near PW-8S to the vicinity of monitoring well PW-5D north of the Deep River. The PW-51) Fault has an inferred connection with the Southern Intermittent Stream Fault beneath the Landfill; Regional Fault/Dike — major regional fault/mafic dike that extends N20°E near PW-6I/6D and extends north of the Deep River; and Deep River Fault — southward -dipping fault that forms the east -west segment of the Deep River. Based on an on -site outcrop measurement and fracture orientation data from the PW-5D core, the fracture zone is believed to dip 50' to the south. 1.3 Site Hydrogeology The Site hydrogeology is characteristic of the regional piedmont aquifer system and consists of three aquifer units: the saprolite and partially weathered rock (PWR) aquifer, shallow bedrock aquifer, and deep bedrock aquifer. The saprolite/PWR aquifer is the uppermost aquifer across much of the Site, but is locally absent where the water table occurs below the top of bedrock. The thickness of the saprolite/PWR aquifer, where present, is generally less than 20 feet but extends to depths of 90 feet in limited areas Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report October 2021 Page 4 (PW-13I). The shallow bedrock aquifer extends from the top of competent bedrock to a depth where groundwater flow becomes limited due to the lack of open fractures. The base of the shallow bedrock zone at the Site is variable but generally believed to occur at depths of 200 to 400 feet. The deep bedrock aquifer extends downward from the base of the shallow bedrock aquifer and is characterized by low permeability and limited groundwater flow. The primary zone of groundwater movement at the Site is considered to occur within the saprolite/PWR and shallow bedrock aquifer zones. The saprolite/PWR and shallow bedrock aquifers are hydraulically connected. The potentiometric surface of shallow groundwater in the saprolite/PWR aquifer is generally a subdued replica of the original topography of the Site. The saprolite/PWR aquifer is locally absent where the water table occurs below the top of bedrock (generally beneath the topographic highs). Groundwater flow within the shallow bedrock aquifer is primarily through fractures in the bedrock and is strongly controlled by subsurface geologic structures such as faults, fracture zones, and mafic dikes. Two constant rate discharge tests were conducted in August and September 1997. The calculated bulk hydraulic conductivity values at the Site range from 0.5 to 3 feet/day in the saprolite/PWR aquifer and 0.1 to 0.6 feet/day in the shallow bedrock aquifer. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report October 2021 Page 5 2.0 Water Quality Monitoring Program The water quality monitoring network at the Site is evaluated on an annual basis. The locations of the groundwater and surface water samples collected during the annual monitoring event are shown on the attached Figure 2. The primary objectives of the annual groundwater and surface water monitoring program are: • Monitor VOC concentrations and migration of the VOC-affected groundwater; • Monitor groundwater elevations, hydraulic gradients and flow directions; • Monitor surface water quality in Randleman Lake, Northern Intermittent Stream, and Southern Intermittent Stream to assess impacts from groundwater discharge. The 2021 annual groundwater and surface water monitoring activities were conducted at the Site during the period of October 21-28, 2021. Groundwater level gauging was conducted at the monitoring wells to be sampled to evaluate groundwater flow patterns at the Site (Figure 2). Surface water sampling was conducted at nine surface water stations which included; four stations along Randleman Lake (SW-6, SW-7, SW-DRP-2, and SW-DRP-11), three stations on the Southern Intermittent Stream (SW-3, SW-4, and SW-5), and two monitoring stations on the Northern Intermittent Stream (SW-1 and SW-2). Please note that surface water monitoring stations SW-1 and SW-2 were dry during this sampling event. 2.1 Groundwater Monitoring Network The existing groundwater monitoring network consists of 25 monitoring wells which have been selected to evaluate the lateral and vertical extent of the contaminant plume as well as the effectiveness of the groundwater extraction system. The 25 monitoring wells sampled for subsequent laboratory analysis include: Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report October 2021 Page 6 MW-1 (background) MW-3C MW-6 MW-10 MW-1 2A MW-12B MW-12D MW-15A OW-DR2 OW-LFS2 PW-31) PW-4I PW-5D PW-6I PW-61) PW-10I PW-1 OD PW-12I PW-13I PW-14D PW-15D PW-16D PW-18 PW-SF1 W-4A Monitoring well construction information and groundwater elevations for the monitoring wells at the Site are provided on Table 1. 2.2 Surface Water Monitoring Network The current surface water monitoring network consists of nine monitoring stations as shown on Figure 2. The surface water monitoring stations are located along the Northern Intermittent Stream, Southern Intermittent Stream, and on Randleman Lake. The nine surface water stations sampled for the water quality monitoring program include: SW-1 SW-3 SW-5 SW-7 SW-DRP-11 SW-2 SW-4 SW-6 SW-DRP-2 * The surface water samples collected from the Randleman Lake are collected at two discrete depths, 1' below the surface and l' above the bottom of the lake. Seaboard Chemical/Riverdale Drive Landfill October 2021 Water Quality Monitoring Report Page 7 3.0 Water Quality Sample Collection Samples of groundwater and surface water were collected in accordance with the approved Annual Monitoring Plan — 2010 dated March 17, 2010. A brief description of the sample collection procedure is provided below. The 2021 annual groundwater and surface water monitoring activities were conducted at the Site during the period of October 21-28, 2021. 3.1 Field Sample Procedures Prior to groundwater sampling, water levels were obtained from each well using an electric water level meter capable of measuring the depth to water to the nearest 0.01 feet. This information was later used to determine the elevation of the water table in each monitoring well relative to surveyed datum (Table 1). The groundwater elevations are used to develop a potentiometric map of the shallow water table (Figure 2). The monitoring wells were sampled using low -flow purge and sample procedures. The groundwater samples were collected using either a peristaltic pump or Grunfos pump with disposable poly tubing. The depth of the intake tubing is positioned at the mid -point of the well screen and the pumping rate is adjusted to match recharge and minimize drawdown in the well. Multiple field parameters, including pH, specific conductivity, temperature, dissolved oxygen, and ORP, are constantly monitored using a flow cell. The turbidity of the influent groundwater is periodically evaluated using a field meter capable of measuring turbidity to +0.01 NTU. Low -flow purging of the well continues until the field parameters have stabilized and the NTU concentration is <10 NTUs, at which time the sample is collected. The samples are collected in the following order: • VOCs and 1,4-dioxane • Field parameters (pH, conductivity, temperature, dissolved oxygen) Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report October 2021 Page 8 The samples were collected directly in the laboratory -supplied containers which had been pre -filled with the appropriate preservative. No filtering of the samples was performed either in the field or laboratory. After collection, the samples were placed in a cooler on ice for overnight shipment to the analytical laboratory. Surface water samples were collected directly into the laboratory -supplied containers as grab samples. Sampling personnel wore new disposable nitrile gloves for each surface water sample collected. The surface water samples collected from the four stations along the Randleman Lake were collected at two discrete intervals: a shallow sample collected one foot below the surface, and a deeper sample collected one foot above the bottom of the Lake. The Randleman Lake water samples were collected using a stainless steel discrete -interval Kemmerer water sampler. The actual depths of the shallow and deeper Randleman Lake surface water samples are provided in Table 4. As with the groundwater samples, these samples were stored in a cooler on ice prior to overnight delivery to the analytical laboratory. 3.2 Field Quality Assurance Two trip blank samples were prepared by the analytical laboratory and accompanied the sample shipments until receipt by the laboratory. The trip blank samples were analyzed for VOCs. Temperature blanks were also provided with the sample shipments to assure the proper temperature was maintained until delivery to the analytical laboratory. 3.3 Sample Delivery/Chain of Custody All groundwater and surface water samples were stored in coolers on ice immediately after collection. Individual sample containers for each monitoring well or surface water sample were placed in zip lock plastic bags to reduce the potential for cross contamination between sample locations. Chain -of -Custody control documents were prepared and shipped with each cooler. Custody seals were also used for each cooler to Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report October 2021 Page 9 maintain sample integrity until delivery to the analytical laboratory. The sample coolers were shipped via Federal Express for next morning delivery to the analytical laboratory. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report October 2021 Page 10 4.0 Laboratory Analysis The groundwater and surface water samples were analyzed for VOCs by EPA Method 8260D and 1,4-dioxane by EPA Method 8260D SIM. The laboratory performing the water quality analysis is Environmental Conservation Laboratories, Inc. (ENCO) of Cary, North Carolina, which is a NC Certified Laboratory. Internal quality control samples, including matrix spikes/matrix spike duplicates, were performed by ENCO for each set of samples. The ENCO laboratory reports, including internal quality control samples, are provided with this report in Appendix A. Field parameters (pH, specific conductivity, temperature, dissolved oxygen) were also measured by the sampling personnel for each groundwater and surface water sample using calibrated meters. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report October 2021 Page 11 5.0 Hydrogeological Conditions The depth to groundwater was measured in the 25 compliance monitoring wells during the October 2021 monitoring event. The groundwater elevations were calculated relative to the surveyed measuring point (top of casing) for each monitoring well. A groundwater potentiometric map is provided as Figure 2. This potentiometric map primarily represents groundwater flow in the uppermost aquifer. The groundwater depths and elevation data for the Site are summarized in Table 1. In the bedrock aquifer, the general groundwater flow direction across the Site is northeastward toward Randleman Lake. The vertical hydraulic gradient in the shallow bedrock aquifer, as measured between monitoring wells MW-3C and OW-DR2 during the October 2021 monitoring event, was 0.010 feet/feet downward. An Extraction Rate/Capture Zone Test was conducted by ERM NC, PC in August 2002. This test used well PW-DR1 as the primary extraction point to determine the potential capture zone using various pumping rates. The results of this test indicated pumping at a relatively low rate of 10 - 20 gallons per minute from PW-DR1 effectively contains the contaminant plume. A pumping rate of 9 — 14 gallons per minute from PW-DR1 during operation of the system has demonstrated a drawdown of approximately 24 feet which creates an effective capture zone. The filling of Randleman Lake began in 2006 and the lake level reached normal pool elevation (682 feet msl) in 2008. Consistent with prior gauging events, and confirmed with the data collected during the October 2021 monitoring event, groundwater levels at monitoring wells located adjacent to the lake have risen 10 - 12 feet as compared to pre -lake water level conditions. Inland from the lake, groundwater levels at wells located on the western portion of the Site have risen approximately 4 feet due to the lake impoundment. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report October 2021 Page 12 6.0 Laboratory Analytical Results The complete analytical results for the samples collected during the period of October 21-28, 2021 were received from the laboratory on November 8 and November 22, 2021. A summary of the analytical results are provided for groundwater (Table 2), surface water (Table 3), and field parameters (Table 4). 6.1 Groundwater Analytical Results The analytical results for selected groundwater contaminants collected during the October 2021 monitoring event are shown in a series of figures. Groundwater quality maps representing the bedrock aquifer are provided for 1,2-dichloroethane (Figure 3), vinyl chloride (Figure 4), chlorobenzene (Figure 5), 1,4-dioxane (Figure 6), and total VOCs (Figure 7). The historical groundwater analytical results for specific VOCs, including the 2020 data, are summarized in Table 2 and the ENCO laboratory reports are provided in Appendix A. Measurements of pH, temperature, and specific conductance as determined in the field during sample collection are provided in Table 4. Additional monitoring well information including the latitude/longitude of each well location is provided in Table 5. The main mass of VOC impacted groundwater generally extends northeastward across the Site to the Randleman Lake basin. As shown on Figure 7, the highest levels of VOCs are present in the vicinity of the northeast corner of the Seaboard Facility near the location of three former surface impoundments. Prior to their closure and capping between 1984 and 1986, the area of the former impoundments served as a primary source area of VOC releases to the groundwater at the Seaboard Facility. Additionally, elevated VOC concentrations in groundwater are also present in the area of the soil residue mound, a contaminant source area located at the Landfill which has also been closed and capped with a synthetic liner. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report October 2021 Page 13 During this monitoring event, VOCs were detected in a limited area across Randleman Lake to the northeast of the Site. Minor concentrations of VOCs at levels above the North Carolina 2L Groundwater Quality Standards were detected at off -site bedrock monitoring wells PW-15D and PW-16D. These bedrock monitoring wells are located on the north side of the Randleman Lake basin from the Site. The extent of the VOC contaminant plume on the north side of Randleman Lake appears to be limited primarily to property encompassed by the Lake's buffer zone, which is maintained and regulated by the Piedmont Triad Regional Water Authority (PTRWA). Please note that a sample was not collected from monitoring well PW-18 during this monitoring event. Monitoring well PW-18 is located on the Crutchfield property on the north side of Randleman Lake from the Site. After numerous attempts to contact the property owner (written and verbal), permission to access the PW-18 location was not granted. Overall, the October 2021 groundwater analytical results and the general distribution of VOCs in the Site's groundwater are consistent with the historical groundwater quality monitoring results. A historical reduction in contaminant concentrations in the monitoring wells on the north side of Randleman Lake from the Site is evident from the groundwater VOC data collected during this monitoring event. 6.2 Surface Water Analytical Results Surface water sampling was conducted at the Southern Intermittent Stream, Northern Intermittent Stream, and at various locations and depths in Randleman Lake. The surface water results for VOCs and 1,4-dioxane are summarized in Table 3 and the ENCO laboratory report is provided in Appendix A. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report October 2021 Page 14 Randleman Lake The Randleman Lake surface water sampling stations include: • SW-6 — Upstream and background sample location for the Site, • SW-DRP-2 — Adjacent to the Site near Lift Station 1 and PW-DR1, • SW-7 — Downstream of the Site at the I-85 bridge, and • SW-DRP-11 —Downstream (-1 mile) at Richland Creek confluence. The laboratory analytical data indicated no VOCs or 1,4-dioxane concentrations above the laboratory practical quantitation limits in any of Randleman Lake surface water samples. The locations of the surface water monitoring stations are shown on Figure 2 and a summary of the Randleman Lake surface water analytical results are provided in Table 3. Based on field observations during the October 2021 monitoring activities, the Randleman Lake was at or near the normal pool elevation of 682 feet msl. Southern Intermittent Stream The Southern Intermittent Stream surface water sampling stations include: • SW-5 — Upstream of Seaboard Facility and downstream of City MRF, • SW-3 — Downstream of Seaboard Facility and upstream of Landfill, and • SW- 4 — Downstream of both Seaboard Facility and Landfill. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report October 2021 Page 15 The compound 1,4-dioxane was reported in all three of the Southern Intermittent Stream surface water monitoring stations. The upstream surface water monitoring station (SW-5) reported a 1,4-dioxane concentration of 2.2 ug/l. Both of the downstream surface water monitoring stations on the Southern Intermittent Stream, SW-3 and SW-4, reported detectable 1,4-dioxane concentrations of 4.6 ug/l and 1,500 ug/l, respectively. No other Site VOCs were reported above the laboratory reporting limits in the samples collected from surface water monitoring station SW-5. Only one VOC (cis-1,2-dichloroethene — 2.6 ug/1) was reported in surface water sample SW-3 at a concentration well below the regulatory standard of 330 ug/l. In addition to the reported concentration of 1,4-dioxane in the sample collected from surface water monitoring station SW-4, numerous Site VOCs were also reported above the regulatory standards in this sample. A summary of the analytical data for the Southern Intermittent Stream samples is provided in Table 3. Northern Intermittent Stream The Northern Intermittent Stream surface water sampling stations include: • SW-1 Surface Water Station —Upstream of the Landfill, and • SW-2 Surface Water Station — Downstream of the Landfill. The flow path of the Northern Intermittent Stream was re-routed in 2011 and no longer passes through a pipe beneath the Landfill. Due to a limited watershed area, these two surface water monitoring stations are typically dry except during periods of heavy rainfall. Both surface water monitoring stations for the Northern Intermittent Stream were dry during the October 2021 monitoring event. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report October 2021 Page 16 A summary of the laboratory analytical results for October 2020 surface water monitoring event is provided on Table 3. A copy of the ENCO laboratory analytical report for the surface water samples is provided with Appendix A. 6.3 Quality Control Samples Two trip blanks were submitted and analyzed for quality assurance purposes. No VOCs were detected at a concentration equaling or exceeding its laboratory quantitation limit in either of the trip blanks. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report October 2021 Page 17 7.0 Conclusions The major findings of the annual groundwater and surface water monitoring activities for October 2021 monitoring event at the Site include the following: • The overall groundwater flow pattern at the Site continues to be toward Randleman Lake on both sides of the Lake basin (Figure 2). Operation of the extraction well PW-DR1 over the past year indicates a significant capture zone for monitoring wells along the northern section of the Landfill adjacent to Randleman Lake. The observed capture zone also extends to the bedrock wells on the north side of Randleman Lake. The capture zone can be maintained by pumping extraction well PW-DR1 at a rate of approximately 10 - 15 gallons per minute. An operational extraction rate of 9 — 14 gallons per minute from PW-DR1 during this monitoring period has demonstrated a drawdown of approximately 24 feet which creates an effective capture zone. Based on the October 2021 monitoring results and historical data, the main VOC plume extends from the Site through the Southern Intermittent Stream valley northeastward to Randleman Lake. The minor concentrations of VOCs detected on the north side of the Randleman Lake in monitoring wells PW-15D and PW- 16D represents the northern extent of the VOC plume. Based on historical groundwater analytical results, the northern extent of Site VOCs in the groundwater north of Randleman Lake is likely restricted to the Piedmont Triad Regional Water Authority regulated buffer. • During the October 2021 monitoring event, concentrations of 1,4-dioxane above the laboratory practical quantitation limit was reported at three of the nine surface water monitoring locations. The three surface water samples collected from the Southern Intermittent Stream exceeded the laboratory quantitation limit and the established regulatory standard. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report October 2021 Page 18 • The October 2021 monitoring data indicated that groundwater levels at monitoring wells located adjacent to the Randleman Lake have risen approximately 10 to 12 feet compared to pre -lake water level conditions. Inland from the lake, the October 2021 groundwater levels at wells located on the western portion of the Site are approximately 4 feet higher compared to pre -lake water level conditions. • Overall, the October 2021 groundwater monitoring results are generally consistent with historical monitoring data. The geometry and migration of VOC-affected groundwater at the Site have not been substantially altered by the filling of Randleman Lake to normal pool. Pumping of extraction well PW-DR1 at a rate of 9 - 14 gallons per minute has demonstrated a significant capture zone created by the drawdown on both sides of Randleman Lake. A historical reduction in contaminant concentrations in the monitoring wells on the north side of Randleman Lake from the Site is evident from the groundwater VOC data collected during this monitoring event. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report October 2021 Page 19 FIGURES TIRE: Site Location leap Seaboard/Riverdale LF Site Jamestown, North Carolina Babb & Associates, P.A. MGM W. W"..• PAWECT NO. Figure 1 1 "= 8000' CHECKM ■r. AU*W or- WE G. Babb 2/10/11 . SW-2�/ SW-6 LOCATED AT UPSTREAM PW-18 SIDE OF KIVETT DRIVE BRIDGE -------------- SW-� -- 1. Ij - ii D —NIs, j i RW-NIS .I I I W-12 681.87 682. M 12 _ � - I /! RIVERDALE DRIVE LANDFILL 690/ 1 PW 19 i I P W-14 D 680.59 P WrT� D� w 5 I P J71 623.1964 L P W-145 T \I A !%r PW-15D*w-,5s SW t, 6D �.. a I I FORMER BURN - - \ - / M W 1 \� 1 / I I PITS AREA 681.36 763.60� I-����' I I ��• -13 w a i,l l it II \ T 1.32 OW-DR4 OW— R2 M678.81 e �,. W-38 678 81 - . \ i -- --� WAY I � R1 -'" � ` I\ • REcove --- �` - M WSCA— 3C _ 4 �\ 677.50 DR1 w - ' \ 'Cp 679.90 ® S 7HERN_��/� - `-... \�� 0 `I � • • Y CITY �\ RW-SISI IN RMI T7ENT/: GARAGE ��_ O-DRSREAMj / �\�l ,I • \ I• \ , Ti `\ MRF-1 Y � I I i SOIL SIDUE \ W15 A OND 738.78 V J Mw-,se 51 a \V I MATERIAL �-2C 1 �\ I -- RECYCLING -211. FACILITY Y \� I C� r� V i RW-SIS2 /Rw-s, liW—L JL SW-3 I , 7 I W- 4A� SW-5 q UINERN INTERMITTENT _ iREAM 6� \ \ \ A�so w-zo OW W MW-9 owasls2 W ­5 D \ z�ai � w-sI \. \\ MRF-2 a * — W— 41 OW-SF1 MW 8e 696 88\ \ •I� 701 00 I / HOUSE eW-18 W 5 �A�M1/"/i 7B �'"' °� M W 1.01 PRAYER W 676.3z 675. 1 .I II 680.85 o _jw-zs $W-29 III 710 �. . • §v RIVERDALE DRIVE LANDFILL '�Y ' `\ Opp 31b1 I I I , • e\ , J.'Z ail 720 FORMER SEABOARD \`=-____-- -- CHEMICAL \` ' CORPORA PON II Q w-25 I r V A m' Aso I RIVERDALE DRIVE _ i i 4 � 2� N � I I 1 730 SW-bRP-11 LOC TE A A _ DOWNSTREAM A ' �' Ib /T P W 5121 EAST sroE ONFLUENCE Wl $ -7 / wREAME T CHLAND CREE Rw-17 o ��------ TREATMENT RLa,vr ... . � SCALE IN FEET 6 II LC T 0 75 150 300 oBASE MAP FROM BBL REMEDIAL INVESTIGATION LEGEND FIGURE o REPORT, MARCH 1999. g MONITORING WELL (SAPROLTE/PWR) OCTOBER 2021 GROUNDWATER POTENTIOMETRIC MAP I WELLS TO BE SAMPLED SHOWN ®RECOVERY WELL SAPROL TESB GROUNDWATER AND SURFACE WATER SAMPLE LOCATIONS N ENLARGED TYPE ( / ) pb� FORMER SEABOARD CHEMICAL/RIVERDALE DRIVE LF Q A SURFACE WATER MONITORING STATION Babb & Associates, P.A. JAMESTOWN, NORTH CAROLINA I BASE MAP FROM BBL REMEDIAL INVESTIGATION NOTE: WELLS TO BE SAMPLED SHOWN REPORT, MARCH 1999. IN ENLARGED TYPE F� * PW-18 r�t0 LEGEND MONITORING WELL (BEDROCK) ® RECOVERY WELL (SAPROLITE/SB) (64.6) CONCENTRATION IN PPB 0 CONCEN�]FONS GREATER THAN 1 L,�11 l000 `'q 0 CONCENTRATIONS G EATER THAN 100 ug/ g-QNCENTONS GREATER THAN 10 ug/L t N SCALE IN FEET 75 150 300 +PW-18 wE. r710 D iFORMER BURN M W-1 PITS AREA (BqL) REOU Y WAY � A� \ O CITY- MAINTENANCE GARAGE MW-12A� (BQL) MW-12B (BQL) MW-12 (BQL) j/ PW-14D PW-16 JJ (BQL) (3.6) _. PW-15 . (i.i) / . . . . . . . . . . . . . . . ,//. . . . . . PW-6D� . . . . . . - . . . . . W— 61 (22) 1 �PW-131 / / M W �23( ) P W— \� �/ SOIL RESIDUE / \ MW-1/ (BQL) MOUND / RECYMM a / I FACR/TY f V 3D1 / / Z�'*P Wt 41 Nd/5£ 1 / (1 3a) OF PRAYER \ I 20 it FaIMER I I i I i �I II SEABOARD j C"aaaa M/ i CORPORA Y i - �50 W // — RDALE f740 so _73� I i PW-121 (BQL) PLANT T BASE MAP FROM BBL REMEDIAL INVESTIGATION REPORT, MARCH 1999. LEGEND MONITORING WELL (BEDROCK) ® ECOVERY WELL (SAPROLITE/SB) ss2 C NCENTRATION IN PPB CONCEf TIONS GREATER THAN 500 u 0 QONCENTRATIONS G EATER THAN ug/ 7J Z m. Z. m. W-0. (BQL) . . . . . L 1 SCALE IN FEET 0 75 150 300 PW-18 �I a 0 0 i HOUSE a, PRAYER BASE MAP FROM BBL REMEDIAL INVESTIGATION REPORT. MARCH 1999. .E MW-12A-,L (5.8) MW-12B (7.7) MW-12 FORMER BURN PITS AREA vv crrr /! : y (180 -.7NANCE� GARAGE / —4- SOIL RESIDUE ` I , .:. �':...... FORIAER SEABOARD CORPORA7Kw o PWW-121 EAST(BQL) WAS7ESADE W47ER MEAIM NT PLANT IW-DR3 1i LEGEND MONITORING WELL (BEDROCK) ® ECOVERY WELL (SAPROLITE/SB) (662) CONCENTRATION IN PPB CONCENTRATIONS GREATER THAN 1,000 ug/L 0 CONCENTRATIONS G EATER THAN 100 ug/L CONCENTRATIONS GREATER THAN 10 ug/L \ V N SCALE IN FEET 0 75 150 300 FORMER BURN PITS AREA S�A�E HWM OF PRAYER BASE MAP FROM BBL REMEDIAL INVESTIGATION REPORT. MARCH 1999. •E PW-18 ,Zo I / t 720 M W—'12 A 1 7180) . . . . r / 730 Mw>1� r...... /; taw=r12 i I .... 7,0 PW-14D� F''O%16 I I (e0L) LEGEND MONITORING WELL (BEDROCK) I . a ECOVERY WELL (SAPROLITE/SB) 2V- 15 1 t �(sa) ��� I (662) C NCENTRATION IN PPB � �� ' — PWoD © CONCENTRATIONS GREATER THAN . ... / 00 ug/ �� (70) 3 I / CONCENTRATIONS G EATER THAN t / (250) -low—� ^ 10 0 u g / MW-3C I �� /COI NTRATIONS GREATER THAN P(W� 5 OW—DRz I ` 10 ug/L cirr� I�� I (400) MAINTENANC --,\ ...... .. GARAGE ... \PN d1 E;� 1 ZU � \ SCALE IN FEET 0 75 150 300 PW-18 ,I i �I II iFORMER BURN M W-1 P175 AREA J (BQL) I war _ � r �j lio sc /76R� AWMAL RECYMM FALYUTY HOUSE OF PRAYER e BASE MAP FROM BBL REMEDIAL INVESTIGATION REPORT, MARCH 1999. M W-112A /(m) Mit— 129 / (12p) / MW-t12 l I (3) � I I i�l I /..::... I RIMERDALE IDRIVWE LAJ✓DFlLL I II I 1 I / I MW 6)3C / I PA -)a rr I 1 —SOIL MO. MVO .15A � . 513) \ ........ p �:..: ................ FORMER SEABOARDCHOACAL OaeF014 im RIVERDALE DRIVE LAMMLL '��icf:F:F:°:4i: i:'�:'.;�:cr ..........::::::::::::::::::::::::::'::' PW-121 (BQL) Babb & Associates, P.A. *\ MONITORING WELL (BEDROCK) (662) CONCENTRATION I PPB CONCENTRATIONS EATER THAN 10,000 ug/L CONCENTRATIO GREATER THAN 16Y/ 1 1,000 ug/L \ 0 CONCENTRATIONS\GREATER THAN 1 100 ug/L GROUND WATER QUALITY -BEDROCK AQUIFER TOTAL VOCS-OCTOBER 2021 FORMER SEABOARD CHEMICAL/RIVERDALE DRIVE LF JAMESTOWN, NORTH CAROLINA ATER THAN N SCALE IN FEET 0 75 150 300 FIGURE 7 TABLES TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 1 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-1 57.71 47.71-57.71 743.98-733.98 789.40 791.69 11/14/2000 27.28 764.41 9/4/2001 27.99 763.70 9/17/2002 29.55 762.14 9/11/2003 23.86 767.83 8/16/2004 25.70 765.99 12/19/2005 25.55 766.14 8/21/2006 25.97 765.72 9/24/2007 26.33 765.36 2/23/2009 25.35 766.14 3/29/2010 24.89 765.72 11/1/2011 27.69 764.00 11/16/2012 27.23 764.46 12/9/2013 28.36 763.33 12/8/2014 28.54 763.15 New Survey 788.85 790.46 10/26/2015 27.99 763.47 11/14/2016 27.50 762.96 10/11/2017 28.43 762.03 11/1/2018 29.70 760.76 9/10/2019 24.78 765.68 10/13/2020 27.67 761.18 10/26/2021 26.86 763.60 MW-2A 19 4-19 709.9-694.9 711.80 713.90 11/14/2000 13.46 700.44 9/4/2001 17.43 696.47 9/17/2002 10.25 703.65 9/11/2003 10.60 703.30 8/16/2004 7.83 706.07 8/21 /2006 13.04 700.86 9/24/2007 14.17 699.73 2/23/2009 10.67 703.23 3/29/2010 6.11 707.79 11/1/2011 8.18 705.72 11/16/2012 12.90 701.00 MW-213 30 30 681.0 711.00 712.57 11/14/2000 12.78 699.79 9/4/2001 13.01 699.56 9/17/2002 10.61 701.96 9/11/2003 10.62 701.95 8/16/2004 7.75 704.82 8/21 /2006 12.25 700.32 9/24/2007 14.64 697.93 2/23/2009 10.35 702.22 3/29/2010 6.05 706.52 11/1/2011 9.16 703.41 1 /16/2012 12.21 700.36 MW-2C 48 28-48 685.56-665.56 711.40 713.56 11/14/2000 16.12 697.44 9/4/2001 14.02 699.54 9/17/2002 18.41 695.15 9/11/2003 12.78 700.78 8/16/2004 14.80 698.76 12/19/2005 NM NM 8/21 /2006 17.53 696.03 9/24/2007 16.86 696.70 2/23/2009 14.25 699.31 3/29/2010 10.97 702.59 11/1/2011 14.55 699.01 11/16/2012 15.82 697.74 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 2 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-3A 27 12-27 682.4-667.4 692.74 694.40 11/14/2000 19.62 674.78 9/4/2001 21.03 673.37 9/17/2002 20.22 674.18 9/11/2003 16.74 677.66 8/16/2004 18.60 675.80 12/19/2005 18.54 675.86 8/21/2006 20.32 674.08 9/24/2007 17.18 677.22 2/23/2009 11.00 683.40 3/29/2010 10.92 683.48 11 /1 /2011 12.34 682.06 11/16/2012 11.87 682.53 MW-36 38.83 28.83-38.83 664.76-654.76 692.32 693.59 11/14/2000 19.46 674.13 9/4/2001 21.00 672.59 9/17/2002 20.00 673.59 9/11/2003 16.32 677.27 8/16/2004 NM NM 12/19/2005 18.81 674.78 8/21/2006 20.33 673.26 9/24/2007 16.59 677.00 2/23/2009 8.48 685.11 3/29/2010 8.04 685.55 11 /1 /2011 11.27 682.32 11/16/2012 11.00 682.59 MW-3C 57 47-57 647.22-637.22 691.90 694.22 11/14/2000 19.51 674.71 9/4/2001 21.12 673.10 8/19/2002 20.57 673.65 9/16/2002 20.00 674.22 9/11/2003 16.47 677.75 8/16/2004 18.46 675.13 12/19/2005 18.96 674.63 8/21/2006 20.56 673.03 9/24/2007 16.50 677.72 2/23/2009 10.15 683.44 3/29/2010 7.86 685.73 11 /1 /2011 10.33 683.89 11/16/2012 10.88 683.34 12/11/2013 10.54 683.68 12/11/2014 20.74 673.48 New Survey 692.50 692.74 10/27/2015 17.68 675.06 11/14/2016 9.90 682.84 10/9/2017 20.46 672.28 11 /2/2018 18.31 674.43 9/11/2019 18.00 674.74 10/13/2020 17.54 674.96 10/26/2021 15.24 677.50 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 3 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-4 30 20-30 664.72-654.72 683.20 684.72 11/14/2000 12.22 672.50 9/4/2001 14.18 670.54 9/ 16/2002 12.71 672.01 9/11/2003 10.62 674.10 8/16/2004 11.91 672.81 12/19/2005 17.55 667.17 8/21/2006 NM NM 9/24/2007 13.22 671.50 New TOC elevation 683.87 687.29 2/23/2009 8.02 679.27 3/29/2010 6.25 681.04 11/1/2011 6.48 680.81 11/16/2012 7.01 680.28 MW-5 30 20-30 664.4-654.4 682.00 684.40 11/14/2000 12.89 671.51 9/4/2001 14.69 669.71 9/ 16/2002 13.81 670.59 9/11/2003 9.23 675.17 8/16/2004 12.05 672.35 12/19/2005 16.59 667.81 8/21/2006 NM NM 9/24/2007 13.98 670.42 New TOC elevation; survey data pending 2/23/2009 5.82 NA 3/29/2010 4.63 NA 11/1/2011 6.18 NA 11/16/2012 6.61 NA MW-6 110 100-110 661.73-651.73 759.60 761.73 11/14/2000 65.92 695.81 9/4/2001 66.49 695.24 9/17/2002 67.21 694.52 9/11/2003 59.32 702.41 8/16/2004 63.47 698.26 12/19/2005 65.83 695.90 8/21/2006 66.46 695.27 9/24/2007 67.11 694.62 2/23/2009 62.58 699.15 3/29/2010 60.55 701.18 11/1/2011 64.36 697.37 11/16/2012 64.60 697.13 12/11/2013 64.88 696.85 12/12/2014 65.80 695.93 New Survey 759.74 761.47 10/30/2015 64.89 696.58 11/17/2016 64.38 697.09 10/10/2017 65.03 696.44 11 /2/2018 61.20 700.27 9/12/2019 62.28 699.19 10/14/2020 63.00 696.74 10/28/2021 65.11 696.36 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 4 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-7A 35 15-35 726.64-706.64 739.42 741.64 11/14/2000 31.10 710.54 9/4/2001 32.34 709.30 9/17/2002 35.73 705.91 9/11/2003 22.61 719.03 8/16/2004 29.02 712.62 12/19/2005 31.13 710.51 8/21 /2006 31.19 710.45 9/24/2007 30.55 711.09 2/23/2009 28.23 713.41 3/29/2010 23.65 717.99 11/1/2011 30.61 711.03 11/16/2012 30.60 711.04 MW-713 68 58-68 682.16-672.16 738.50 740.16 11/14/2000 33.90 706.26 9/4/2001 33.15 707.01 9/17/2002 38.12 702.04 9/11/2003 24.53 715.63 8/16/2004 31.80 708.36 12/19/2005 33.74 706.42 8/21 /2006 33.36 706.80 9/24/2007 33.31 706.85 2/23/2009 30.18 709.98 3/29/2010 25.67 714.49 11/1/2011 27.93 712.23 11/16/2012 30.00 710.16 MW-8 33 13-33 721.16-701.16 731.80 734.16 11/14/2000 >30.70 - 9/4/2001 >30.70 9/17/2002 >30.70 - 9/11/2003 20.49 719.67 8/16/2004 28.35 711.81 12/19/2005 20.22 719.94 8/21 /2006 30.81 709.35 9/24/2007 32.89 701.27 2/23/2009 26.39 713.77 3/29/2010 20.51 719.65 11/1/2011 28.85 705.31 11/16/2012 30.96 703.20 MW-9 32 12-32 676.95-656.95 685.95 688.95 11/14/2000 12.36 9/4/2001 13.53 675.42 9/16/2002 13.48 675.47 9/11/2003 8.15 680.80 8/16/2004 10.78 678.17 12/19/2005 11.43 677.52 8/21 /2006 21.35 667.60 9/24/2007 NM NM 2/23/2009 5.37 683.58 3/29/2010 4.22 684.73 11/1/2011 5.97 682.98 11/16/2012 6.26 682.69 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 5 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-10 28 8-28 687.62-667.62 693.60 695.62 11/14/2000 16.91 678.71 9/4/2001 18.61 677.01 9/16/2002 17.64 677.98 9/11/2003 13.78 681.84 8/16/2004 15.06 680.56 12/19/2005 14.47 681.15 8/21 /2006 16.80 678.82 9/24/2007 17.29 678.33 2/23/2009 11.92 683.70 3/29/2010 10.57 685.05 11 /1 /2011 12.96 682.66 11/16/2012 13.18 682.44 12/10/2013 12.97 682.65 12/10/2014 13.97 681.65 New Survey 693.24 695.01 10/26/2015 12.59 682.42 11/14/2016 12.86 682.15 10/9/2017 12.95 682.06 10/31 /2018 11.53 683.48 9/10/2019 13.40 681.61 10/12/2020 14.96 678.28 10/26/2021 19.50 675.51 MW-11 68 53-68 695.42-680.42 746.26 748.42 11/14/2000 38.24 710.18 9/4/2001 38.50 709.92 8/19/2002 41.06 707.36 9/16/2002 40.65 707.77 9/11/2003 28.97 719.45 8/16/2004 36.81 711.61 12/19/2005 38.51 709.91 8/21 /2006 32.91 715.51 9/24/2007 37.29 711.13 2/23/2009 28.91 719.51 3/29/2010 26.02 722.40 11/1/2011 31.13 717.29 11/16/2012 34.87 713.55 MW-12A 20 5-20 688.96-673.96 691.12 693.96 11/14/2000 15.66 678.30 9/4/2001 15.87 678.09 9/16/2002 15.62 678.34 9/11/2003 11.08 682.88 8/16/2004 14.15 679.81 12/19/2005 11.31 682.65 8/21 /2006 14.67 679.29 9/24/2007 13.92 680.04 2/23/2009 11.11 682.85 3/29/2010 9.99 683.97 11 /1 /2011 9.26 684.70 11/16/2012 11.13 682.83 12/10/2013 9.07 684.89 12/11/2014 11.58 682.38 New Survey 690.21 693.07 10/27/2015 11.15 681.92 11 /14/2016 11.01 682.06 10/9/2017 10.98 682.09 11/1/2018 10.19 682.88 9/ 10/2019 10.41 682.66 10/13/2020 10.34 679.87 10/26/2021 11.20 681.87 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 6 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-12B 58 48-58 647-637 691.70 695.00 11/14/2000 16.49 678.51 9/4/2001 16.92 678.08 9/16/2002 16.65 678.35 9/11/2003 12.72 682.28 8/16/2004 15.03 679.97 12/19/2005 14.12 680.88 8/21/2006 NM NM 9/24/2007 NM NM 2/23/2009 10.95 684.05 3/29/2010 NM NM 11/1/2011 10.25 684.75 11/16/2012 10.81 684.19 12/10/2013 11.55 683.45 12/11/2014 11.65 683.35 New Survey 690.75 693.86 10/27/2015 10.67 683.19 11/14/2016 10.23 683.63 10/ 10/2017 11.21 682.65 11 /1 /2018 10.22 683.64 9/11/2019 10.76 683.10 10/13/2020 10.35 680.40 10/26/2021 11.51 682.35 MW-12D 202 187-202 507.93-492.93 691.81 694.93 11/14/2000 >101.50 <593 9/4/2001 48.12 646.81 9/16/2002 47.59 647.34 9/11/2003 46.06 648.87 8/16/2004 NM NM 12/19/2005 20.80 674.13 8/21/2006 NM NM 9/24/2007 14.24 680.69 2/23/2009 9.43 685.50 3/29/2010 12.62 682.31 11/1/2011 13.88 681.05 11/16/2012 43.06 651.87 12/10/2013 25.34 669.59 12/11/2014 43.02 651.91 New Survey 691.19 694.21 10/29/2015 21.96 672.25 11/18/2016 24.12 670.09 10/11/2017 53.41 640.80 11 /1 /2018 26.84 667.37 9/12/2019 3.25 690.96 10/13/2020 2.97 688.22 10/26/2021 3.90 690.31 MW-14 35 20-35 746.22-731.22 763.80 766.22 11/14/2000 28.42 737.80 9/4/2001 29.33 736.89 9/17/2002 NM NM 9/11/2003 25.38 740.84 8/16/2004 26.16 740.06 8/21/2006 27.98 738.24 2/23/2009 27.27 738.95 3/29/2010 25.71 740.51 11/1/2011 27.86 738.36 11/16/2012 27.61 738.61 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 7 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-15A 34 19-34 731.34-746.34 762.5 765.34 9/4/2001 26.70 738.64 9/17/2002 21.40 743.94 9/11/2003 NM NM 8/16/2004 22.72 742.62 12/19/2005 24.31 741.03 8/21/2006 NM NM 2/23/2009 15.21 750.13 3/29/2010 22.06 743.28 11/1/2011 25.19 740.15 11/16/2012 24.75 740.59 12/10/2013 24.69 740.65 12/8/2014 25.64 739.70 New Survey 762.57 764.33 10/27/2015 24.46 739.87 11/14/2016 27.01 737.32 10/11/2017 27.90 736.43 10/31/2018 22.72 741.61 9/10/2019 22.58 741.75 10/9/2020 22.43 740.14 10/28/2021 25.55 738.78 MW-16 45 30-45 749.13-734.13 779.00 779.13 11/14/2000 34.18 744.95 9/4/2001 NM NM 9/17/2002 NM NM 9/11/2003 NM NM 8/16/2004 NM NM 12/19/2005 NM NM 8/21/2006 NM NM 2/23/2009 NM NM 11/16/2012 NM NM MW-17 (WSW-1) 250 230-250 12/19/2005 68.09 8/21/2006 NM NM 2/23/2009 66.04 3/29/2010 64.30 11 /1 /2011 66.88 11/16/2012 67.34 NM MRF-1 43.5 28.5-43.5 723.31-708.31 752.10 751.81 11/14/2000 8.45 743.36 9/4/2001 8.48 743.33 9/17/2002 8.56 743.25 9/11/2003 7.40 744.41 8/16/2004 7.59 744.22 12/19/2005 7.63 744.18 8/21/2006 8.25 743.56 9/24/2007 8.87 742.94 2/23/2009 7.56 744.25 3/29/2010 7.55 744.26 11 /1 /2011 8.01 743.80 11/16/2012 7.98 743.83 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 8 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MRF-2 41.5 26.5-41.5 724.23-709.23 751.00 750.73 11/14/2000 26.06 724.67 9/4/2001 26.18 724.55 9/17/2002 26.10 724.63 9/11/2003 24.28 726.45 8/16/2004 24.10 726.63 12/19/2005 24.35 726.38 8/21/2006 25.69 725.04 9/24/2007 25.69 725.04 2/23/2009 25.22 725.51 3/29/2010 24.73 726.00 11/1/2011 25.18 725.55 11/16/2012 25.30 725.43 OW-DR1 165 49-165 648.95-532.95 695.39 697.95 11/14/2000 23.21 674.74 9/4/2001 24.72 673.23 9/16/2002 23.80 674.15 9/11/2003 20.21 677.74 8/16/2004 22.23 675.72 12/19/2005 22.91 675.04 8/21/2006 24.40 673.55 9/24/2007 20.16 677.79 2/23/2009 13.77 684.18 3/29/2010 11.42 686.53 11 /1 /2011 13.95 684.00 11/16/2012 14.64 683.31 OW-DR2 186 176-186 518.4-508.4 692.61 694.40 11/14/2000 19.72 674.68 9/4/2001 21.33 673.07 8/19/2002 20.75 673.65 9/16/2002 20.25 674.15 9/11/2003 16.60 677.80 8/16/2004 18.62 675.78 12/19/2005 19.34 675.06 8/21/2006 20.79 673.61 9/24/2007 16.52 677.88 2/23/2009 10.13 684.27 3/29/2010 7.97 686.43 11 /1 /2011 10.32 684.08 11/16/2012 10.90 683.50 12/10/2013 10.55 683.85 12/12/2014 27.31 667.09 New Survey 692.22 695.87 10/30/2015 13.53 682.34 11/18/2016 14.28 681.59 10/ 10/2017 16.31 679.56 11 /2/2018 19.59 676.28 9/11/2019 20.24 675.63 10/13/2020 19.76 672.46 10/28/2021 17.06 678.81 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 9 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) OW-DR3 160 77-160 626.52-543.52 703.52 704.75 8/19/2002 30.79 663.61 9/16/2002 30.40 664.00 9/11/2003 27.80 666.60 8/16/2004 29.02 665.38 12/19/2005 30.29 664.11 8/21 /2006 31.17 663.23 9/24/2007 26.32 678.43 2/23/2009 20.17 684.58 3/29/2010 18.61 686.14 11/1/2011 20.45 684.30 11/16/2012 20.75 684.00 12/10/2013 20.99 683.76 OW-DR4 165 45 - 165 667.70-547.70 712.70 713.85 8/19/2002 40.15 673.70 9/16/2002 39.72 674.13 9/11/2003 36.25 677.60 8/16/2004 38.23 675.62 12/19/2005 38.91 674.94 8/21 /2006 40.34 673.51 9/24/2007 35.99 677.86 2/23/2009 29.64 684.21 3/29/2010 22.30 691.55 11/1/2011 29.83 684.02 11/16/2012 30.30 683.55 OW-DR5 40 20-40 12/19/2005 10.50 -- 2/23/2009 NM 3/29/2010 NM 11/1/2011 NM 11/16/2012 NM NM OW-NIS1 40 25-40 12/19/2005 10.91 2/23/2009 8.40 3/29/2010 7.59 11/1/2011 6.40 11/16/2012 7.54 OW-SIS1 39 20-39 12/19/2005 24.05 8/21 /2006 24.08 9/24/2007 23.89 2/23/2009 20.89 3/29/2010 17.69 11/1/2011 22.98 11/16/2012 22.99 OW-SIS2 40 20-40 12/19/2005 5.32 2/23/2009 4.32 3/29/2010 3.29 11/1/2011 3.74 11/16/2012 7.63 OW-SIS3 45 15-45 12/19/2005 5.80 2/23/2009 5.67 3/29/2010 3.61 11/1/2011 5.22 11/16/2012 7.00 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 10 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) OW-SF1 120 95-120 638.15-613.15 731.06 731.06 12/19/2005 26.15 704.91 8/21/2006 26.00 705.06 9/24/2007 25.84 705.22 2/23/2009 23.03 708.03 3/29/2010 18.64 712.42 11/1/2011 25.39 705.67 11/16/2012 25.22 705.84 OW-SF2 120 80-120 651.05-611.05 728.87 731.05 8/21/2006 NM NM 9/24/2007 20.44 710.61 2/23/2009 18.47 -- 3/29/2010 14.27 716.78 11/1/2011 20.46 710.59 11/16/2012 20.68 710.37 OW-LFS1 50 30-50 698.74 12/19/2005 17.15 681.59 2/23/2009 14.45 684.29 3/29/2010 13.28 685.46 11/1/2011 14.90 683.84 11/16/2012 15.88 682.86 OW-LFS2 50 30-50 700.08 12/19/2005 21.97 678.11 2/23/2009 15.81 684.27 3/29/2010 14.66 685.42 11/1/2011 16.34 683.74 11/16/2012 16.61 683.47 12/11/2013 16.82 683.26 12/12/2014 17.44 682.64 New Survey 696.69 699.45 10/26/2015 16.48 682.97 11/14/2016 20.12 679.33 10/9/2017 25.57 673.88 10/31/2018 38.96 660.49 9/12/2019 17.20 682.25 10/12/2020 32.22 664.47 10/28/2021 16.05 683.40 PW-DR1 185 38-185 657.21-510.21 693.62 695.21 11/14/2000 20.51 674.70 9/4/2001 21.90 673.31 8/19/2002 21.48 673.73 9/16/2002 21.02 674.19 9/11 /2003 17.51 677.70 8/16/2004 19.55 675.66 12/19/2005 NM -- 8/21/2006 NM 9/24/2007 NM 2/23/2009 NM 3/29/2010 NM 11/1/2011 NM 11/16/2012 NM TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 11 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-SF1 120 95-120 638.15-613.15 732.14 733.15 8/21/2006 25.98 707.17 9/24/2007 25.60 707.55 2/23/2009 22.96 710.19 3/29/2010 18.62 714.53 11 /1 /2011 25.31 707.84 11/16/2012 25.50 707.64 12/9/2013 21.00 712.15 12/8/2014 26.65 706.50 New Survey 731.13 732.19 10/27/2015 26.78 705.41 11/17/2016 24.45 707.74 10/11/2017 28.21 703.98 10/31 /2018 22.17 710.02 9/10/2019 20.50 711.69 10/9/2020 21.66 709.47 10/27/2021 23.76 708.43 PW-SIS1 39 19-39 695.21 8/16/2004 NM -- 12/19/2005 12.20 683.01 8/21/2006 13.95 681.26 9/24/2007 15.43 679.78 2/23/2009 12.73 682.48 3/29/2010 11.31 683.90 11 /1 /2011 13.01 682.20 11/16/2012 13.63 681.58 PW-1D 81.5 66.5-81.5 717.18-702.18 781.90 783.68 11/14/2000 54.92 728.76 9/4/2001 54.60 729.08 9/17/2002 54.65 729.03 9/11/2003 47.49 736.19 8/16/2004 NM -- 12/19/2005 51.82 731.86 8/21/2006 NM -- 2/23/2009 49.60 734.08 3/29/2010 47.86 735.82 11 /1 /2011 50.18 733.50 11/16/2012 50.30 733.38 PW-2D 101 80-100 700.55-680.55 778.80 780.55 11/14/2000 45.43 735.12 9/4/2001 45.16 735.39 9/17/2002 NM -- 9/11/2003 NM -- 8/16/2004 43.45 737.10 12/19/2005 43.94 736.61 8/21/2006 42.75 737.80 9/24/2007 44.20 736.35 2/23/2009 41.43 739.12 3/29/2010 39.30 741.25 11 /1 /2011 42.62 737.93 11/16/2012 42.20 738.35 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 12 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-3D 209.5 179.5-209.5 578.84-548.84 756.60 758.34 11/14/2000 56.60 701.74 9/4/2001 NM -- 9/16/2002 58.62 699.72 9/11/2003 NM -- 8/16/2004 55.55 702.79 12/19/2005 NM -- 8/21/2006 56.75 701.59 2/23/2009 50.02 708.32 3/29/2010 48.12 710.22 11 /1 /2011 50.52 707.82 11/16/2012 47.90 710.44 12/17/2013 48.81 709.53 12/11/2014 49.51 708.83 New Survey 737.63 738.60 10/29/2015 48.91 689.69 11/16/2016 52.42 686.18 10/11/2017 43.99 694.61 11 /2/2018 50.71 687.89 9/11/2019 52.02 686.58 10/14/2020 51.76 685.87 10/27/2021 51.39 687.21 PW-41 122 112-122 625.67-615.67 735.17 737.67 11/14/2000 43.39 694.28 9/4/2001 44.73 692.94 9/17/2002 45.94 691.73 9/11/2003 36.04 701.63 8/16/2004 42.31 695.36 12/19/2005 43.27 694.40 8/21 /2006 43.11 712.03 2/23/2009 39.35 698.32 3/29/2010 35.56 719.58 11 /1 /2011 41.23 696.44 11/16/2012 41.49 696.18 12/17/2013 42.03 695.64 12/8/2014 42.62 695.05 New Survey 732.04 737.59 10/29/2015 42.10 695.49 Corrected elevation after well repair. Removed 2.59' of casing. 735.00 11/17/2016 40.78 694.22 10/11/2017 43.80 691.20 11 /2/2018 34.04 700.96 9/11/2019 35.52 699.48 10/14/2020 36.42 695.62 10/27/2021 38.12 696.88 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 13 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-5D 306.5 272-282 425.87-415.87 695.07 697.87 11/14/2000 23.52 674.35 9/4/2001 24.04 673.83 8/19/2002 24.54 673.33 9/16/2002 23.86 674.01 9/11/2003 20.37 677.50 8/16/2004 22.45 675.42 12/19/2005 23.21 674.66 8/21 /2006 24.68 673.19 9/24/2007 20.31 677.56 2/23/2009 13.85 684.02 3/29/2010 10.85 687.02 11 /1 /2011 13.98 683.89 11/16/2012 12.92 684.95 12/16/2013 10.54 687.33 12/11/2014 21.86 676.01 New Survey 693.96 696.27 10/30/2015 13.80 682.47 11/18/2016 13.73 682.54 10/ 10/2017 17.41 678.86 11 /2/2018 17.31 678.96 9/11/2019 17.42 678.85 10/13/2020 17.72 678.55 10/28/2021 16.37 679.90 PW-61 76 65-76 619.19-608.19 682.27 684.19 11/14/2000 11.80 672.39 9/4/2001 13.98 670.21 8/ 19/2002 12.81 671.38 9/16/2002 12.35 671.84 9/11/2003 11.20 672.99 8/16/2004 12.00 672.19 12/19/2005 16.14 668.05 8/21/2006 NM -- 9/24/007 NM -- New TOC elevation 693.57 696.15 2/23/2009 14.75 681.40 3/29/2010 11.76 684.39 11/1/2011 13.98 682.17 11/16/2012 14.26 669.93 12/16/2013 14.29 681.86 New well 12/10/2014 17.43 679.98 New Survey 100 90-100 695.12 697.41 10/27/2015 16.15 681.26 11/17/2016 16.54 680.87 10/10/2017 17.38 680.03 11/1/2018 15.47 681.94 9/12/2019 16.00 681.41 10/13/2020 15.27 679.85 10/28/2021 16.05 681.36 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 14 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-6D 275 260-275 424.77-409.77 682.22 684.77 11/14/2000 11.01 673.76 9/4/2001 12.58 672.19 8/19/2002 12.07 672.70 9/16/2002 11.57 673.20 9/11/2003 7.87 676.90 8/16/2004 9.95 674.82 12/19/2005 13.24 671.53 8/21/2006 NM -- 9/24/2007 NM -- New TOC elevation 691.53 696.33 3/12/2009 13.05 683.28 3/29/2010 11.84 684.49 11 /1 /2011 13.34 682.99 11/16/2012 14.03 682.30 12/16/2013 NA NA New well 12/10/2014 23.56 673.23 New Survey 300 270-300 695.02 696.79 10/30/2015 14.53 682.26 11/17/2016 15.02 681.77 10/10/2017 21.65 675.14 11 /1 /2018 17.33 679.46 9/12/2019 18.44 678.35 10/12/2020 16.75 678.27 10/28/2021 16.68 680.11 PW-71 101 90-100 594.92-584.92 683.42 684.92 11/14/2000 12.90 672.02 9/4/2001 14.58 670.34 6/ 16/2002 12.81 672.11 8/19/2002 13.28 671.64 9/ 16/2002 12.81 672.11 9/11/2003 11.69 673.23 8/16/2004 12.92 672.00 12/19/2005 11.41 673.51 8/21 /2006 14.38 670.54 9/24/2007 9.11 675.81 New TOC elevation; survey data pending 2/23/2009 2.34 NA 3/29/2010 1.89 NA 11/1/2011 1.85 NA 11/16/2012 2.99 NA PW-8S 48 35-45 728.13-718.13 761.23 763.13 11/14/2000 42.30 720.83 9/4/2001 45.10 718.03 9/17/2002 47.33 715.80 9/11/2003 38.95 724.18 8/16/2004 40.70 722.43 12/19/2005 42.80 720.33 8/21 /2006 43.39 719.74 9/24/2007 44.57 718.56 2/23/2009 41.66 721.47 3/29/2010 27.22 735.91 11 /1 /2011 40.58 722.55 11/16/2012 40.96 722.17 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 15 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-91 100 80-100 619.07-599.07 698.07 699.07 11/14/2000 21.80 677.27 9/4/2001 22.95 676.12 9/16/2002 22.74 676.33 9/11/2003 18.04 681.03 8/16/2004 20.50 678.57 12/19/2005 20.79 678.28 8/21 /2006 11.75 687.32 9/24/2007 21.14 677.93 2/23/2009 14.18 684.89 3/29/2010 13.50 685.57 11 /1 /2011 14.61 684.46 11/16/2012 15.18 683.89 PW-101 100 80-100 616.44-596.44 695.34 696.44 11/14/2000 17.24 679.20 9/4/2001 19.08 677.36 9/16/2002 18.30 678.14 9/11/2003 14.57 681.87 8/16/2004 16.05 680.39 12/19/2005 15.53 680.91 8/21 /2006 17.68 678.76 9/24/2007 17.44 679.00 2/23/2009 12.06 684.38 3/29/2010 10.62 685.82 11/1/2011 12.32 684.12 11/16/2012 13.37 683.07 12/11/2013 13.10 683.34 12/ 10/2014 14.21 682.23 New Survey 694.63 695.97 10/29/2015 12.43 683.54 11/17/2016 13.46 682.51 10/9/2017 14.19 681.78 11 /1 /2018 11.68 684.29 9/12/2019 13.20 682.77 10/12/2020 16.82 677.81 10/26/2021 19.63 676.34 PW-1OD 200 185-200 512.75-497.75 695.48 697.96 11/14/2000 >101.50 - 9/4/2001 39.20 658.76 9/16/2002 46.45 651.51 9/11/2003 NM NM 8/16/2004 48.04 649.92 12/19/2005 29.01 668.95 8/21 /2006 32.60 665.36 9/24/2007 18.42 679.54 2/23/2009 14.51 683.45 3/29/2010 26.38 671.58 11 /1 /2011 17.01 680.95 11/16/2012 43.21 654.75 12/11/2013 42.25 655.71 12/10/2014 34.50 663.46 New Survey 695.13 697.26 11/3/2015 35.32 661.94 11/17/2016 25.33 671.93 10/10/2017 49.55 647.71 10/31 /2018 26.28 670.98 9/12/2019 45.70 651.56 10/12/2020 22.75 672.38 10/26/2021 16.41 680.85 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 16 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-111 90 75-90 710.45-695.45 784.38 785.45 11/14/2000 57.55 727.90 9/4/2001 58.00 727.45 9/17/2002 58.77 726.68 9/11/2003 53.81 731.64 8/16/2004 56.23 729.22 12/19/2005 56.65 728.80 8/21 /2006 56.73 728.72 9/24/2007 57.25 728.20 2/23/2009 55.90 729.55 3/29/2010 52.60 732.85 11 /1 /2011 55.01 730.44 11/16/2012 54.90 730.55 PW-121 105 90-105 660.54-645.54 748.07 750.54 11/14/2000 29.09 721.45 9/4/2001 32.36 718.18 2/16/2002 36.25 714.29 9/16/2002 36.25 714.29 9/11/2003 26.18 724.36 8/16/2004 27.41 723.13 12/19/2005 29.55 720.99 8/23/2006 30.15 720.39 9/24/2007 28.55 721.99 2/23/2009 28.93 721.61 3/29/2010 24.62 725.92 11/1/2011 28.18 722.36 11/16/2012 27.73 722.81 12/16/2013 28.17 722.37 12/12/2014 28.70 721.84 New Survey 746.99 749.48 10/30/2015 28.82 720.66 11/21/2016 35.73 713.75 10/11/2017 28.55 720.93 11/6/2018 29.51 719.97 9/11/2019 21.83 727.65 10/14/2020 22.94 724.05 10/28/2021 23.95 725.53 PW-131 250 235-250 504.9-489.9 736.58 739.90 11/14/2000 67.65 672.25 9/4/2001 69.68 670.22 8/19/2002 68.50 671.40 9/17/2002 68.12 671.78 9/11/2003 66.59 673.31 8/16/2004 67.52 672.38 12/19/2005 68.51 671.39 8/21/2006 69.64 670.26 9/24/2007 64.70 675.20 2/23/2009 57.31 682.59 3/29/2010 54.65 685.25 11 /1 /2011 57.33 682.57 11/16/2012 58.05 681.85 12/16/2013 57.20 682.70 12/12/2014 59.52 680.38 New Survey 736.23 739.01 10/26/2015 37.69 701.32 11/18/2016 58.24 680.77 10/11/2017 58.97 680.04 10/31/2018 57.15 681.86 9/11/2019 51.68 687.33 10/13/2020 56.93 679.30 10/28/2021 57.69 681.32 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 17 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-14D 198.8 183.8-198.8 505.33-490.33 686.38 689.13 10/31/2000 16.24 672.89 12/20/2000 > 150 - 9/5/2001 76.98 612.15 9/17/2002 64.16 624.97 9/11/2003 6.51 682.62 8/16/2004 56.01 633.12 12/19/2005 67.27 621.86 8/21/2006 37.29 651.84 9/24/2007 62.45 626.68 3/11/2009 37.90 651.23 3/29/2010 29.41 659.72 11/1/2011 17.63 671.50 11/16/2012 32.37 656.76 12/12/2013 56.60 632.53 12/9/2014 63.29 625.84 New Survey 685.27 686.50 11/3/2015 72.59 613.91 11/16/2016 46.02 640.48 10/12/2017 9.42 677.08 11 /5/2018 39.62 646.88 9/17/2019 87.88 598.62 10/14/2020 62.08 623.19 10/27/2021 37.36 649.14 PW-14S 21.5 11.5-21.5 677.09-667.09 685.96 688.59 10/30/2000 13.19 675.40 12/20/2000 13.47 675.12 9/5/2001 14.28 674.31 9/17/2002 14.55 674.04 9/11/2003 14.92 673.67 8/16/2004 10.26 678.33 12/19/2005 11.54 677.05 8/21 /2006 13.45 675.14 3/11/2009 4.34 684.25 3/29/2010 2.13 686.46 11/1/2011 4.27 684.32 11/16/2012 5.30 683.29 PW-15D 163.5 153.5-163.5 533.93-523.93 684.85 687.43 10/31/2000 13.25 674.18 12/20/2000 13.32 674.11 9/5/2001 14.79 672.64 9/17/2002 13.81 673.62 9/11/2003 10.13 677.30 8/16/2004 12.24 675.19 12/19/2005 13.03 674.40 8/21 /2006 15.80 671.63 9/24/2007 9.93 677.50 3/11/2009 3.20 684.23 3/29/2010 2.02 685.41 11/1/2011 3.25 684.18 11/16/2012 4.39 683.04 12/12/2013 4.50 682.93 12/9/2014 8.14 679.29 New Survey 684.05 685.80 10/28/2015 4.11 681.69 11/15/2016 4.54 681.26 10/12/2017 10.15 675.65 11 /5/2018 4.95 680.85 9/17/2019 6.60 679.20 10/14/2020 5.95 678.10 10/27/2021 5.38 680.42 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 18 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-15S 21.5 11.5-21.5 676.71-666.71 685.88 688.21 10/30/2000 14.87 673.34 12/20/2000 14.91 673.30 9/5/2001 16.26 671.95 9/17/2002 15.42 672.79 9/11/2003 11.61 676.60 8/16/2004 13.89 674.32 12/19/2005 14.14 674.07 8/21 /2006 14.32 673.89 9/24/2007 9.75 678.46 3/11/2009 4.65 683.56 3/29/2010 3.09 685.12 11/1/2011 4.58 683.63 11/16/2012 5.89 682.32 PW-16D 179 169-179 515.98-505.98 681.46 684.98 10/31/2000 10.94 674.04 12/20/2000 10.95 674.03 9/5/2001 12.43 672.55 9/17/2002 11.51 673.47 9/11/2003 7.88 677.10 8/16/2004 9.91 675.07 12/19/2005 10.80 674.18 8/21 /2006 12.09 672.89 9/24/2007 11.21 673.77 New TOC elevation; survey data pending 3/11/2009 4.38 NA 3/29/2010 3.23 NA 11/1/2011 4.45 NA 11/16/2012 5.65 NA 12/12/2013 5.22 NA 12/9/2014 7.10 NA New Survey 684.07 686.68 10/28/2015 4.84 681.84 11/15/2016 5.31 681.37 10/12/2017 8.89 677.79 11 /5/2018 4.70 681.98 9/17/2019 6.77 679.91 10/14/2020 6.31 677.76 10/27/2021 6.09 680.59 PW-16S 12.5 5.5-12.5 677.67-670.67 680.97 683.17 10/30/2000 8.00 675.17 12/20/2000 7.39 675.78 9/5/2001 9.82 673.35 9/17/2002 9.65 673.52 9/11/2003 6.56 676.61 8/16/2004 6.79 676.38 12/19/2005 6.21 676.96 8/21 /2006 8.44 674.73 9/24/2007 11.83 671.34 New TOC elevation; survey data pending 3/11/2009 4.93 NA 3/29/2010 4.10 NA 11/1/2011 4.64 NA 11/16/2012 5.96 NA TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 19 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-17 100 85 - 100 686.0 - 671.0 771.0 774.7 11/14/2000 43.25 731.45 12/20/2000 43.96 730.74 9/5/2001 45.55 729.15 9/16/2002 49.34 725.36 9/11/2003 37.64 737.06 8/16/2004 39.42 735.28 12/19/2005 21.09 753.61 8/21 /2006 43.19 731.51 9/24/2007 42.02 732.68 2/23/2009 42.50 732.20 3/29/2010 38.20 736.50 11/1/2011 43.50 731.20 11/16/2012 42.40 732.30 PW-18 225 210 - 225 525.4 - 510.4 735.4 737.8 11/9/2000 110.06 627.74 12/7/2000 57.23 680.57 12/14/2000 57.28 680.52 12/20/2000 57.27 680.53 9/5/2001 58.50 679.30 9/17/2002 NM NM 9/11/2003 86.31? Suspect data 8/16/2004 53.18 684.62 12/19/2005 NM NM 8/21 /2006 39.32 698.48 9/24/2007 34.56 703.24 3/11/2009 37.43 700.37 3/29/2010 30.22 707.58 11/1/2011 36.15 701.65 11/16/2012 35.04 702.76 12/12/2013 34.75 703.05 12/9/2014 33.80 704.00 New Survey 734.02 736.44 10/26/2015 36.68 699.76 11/15/2016 30.73 705.71 10/16/2017 33.24 703.20 11 /7/2018 32.70 703.74 NM NM NM PW-19 260 235-250 516.6 - 501.6 751.6 754.1 11/5/2001 75.70 678.40 9/17/2002 60.16 693.94 9/11/2003 94.56? Suspect data 9/11/2003 52.75 701.35 8/16/2004 53.18 700.92 12/19/2005 54.11 699.99 8/21 /2006 54.50 699.60 9/24/007 54.15 699.95 2/25/2009 52.18 701.92 3/29/2010 50.65 703.45 11/1/2011 NM 11/16/2012 NM TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 20 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) W-1 64.7 53.7-64.7 719.05-708.05 772.20 772.75 11/14/2000 42.08 730.67 9/4/2001 24.12 748.63 9/17/2002 48.07 724.68 9/11/2003 36.39 736.36 8/16/2004 38.00 734.75 12/19/2005 40.78 731.97 8/21 /2006 41.87 730.88 2/23/2009 41.63 731.12 3/29/2010 37.13 735.62 11/1/2011 41.53 731.22 11/16/2012 41.00 731.75 W-2 35 23-35 703-691 723.30 726.00 11/14/2000 16.51 709.49 9/4/2001 17.33 708.67 9/17/2002 18.35 707.65 9/11/2003 12.62 713.38 8/16/2004 14.05 711.95 8/21 /2006 18.56 707.44 9/224/07 16.30 709.70 2/23/2009 15.54 710.46 3/29/2010 14.75 711.25 11 /1 /2011 16.43 709.57 11/16/2012 18.10 707.90 W-4 19 9-19 703.64-693.64 710.30 712.64 11/14/2000 9.49 703.15 9/4/2001 9.84 702.80 9/17/2002 8.57 704.07 9/11/2003 6.71 705.93 8/16/2004 6.28 706.36 12/19/2005 7.74 704.90 8/21 /2006 9.09 703.55 9/24/2007 9.94 702.70 2/23/2009 6.22 706.42 3/29/2010 5.80 706.84 11 /1 /2011 6.69 705.95 11/16/2012 9.35 703.29 W-4A 38.5 28.5-38.5 684.75-674.75 712.00 713.25 11/14/2000 9.77 703.48 9/4/2001 10.12 703.13 9/17/2002 9.00 704.25 9/11/2003 7.58 705.67 8/16/2004 6.87 706.38 12/19/2005 6.91 706.34 8/21 /2006 9.49 703.76 9/24/2007 10.08 703.17 2/23/2009 6.92 706.33 3/29/2010 5.83 707.42 11 /1 /2011 6.82 706.43 11/16/2012 9.57 703.68 12/17/2013 7.39 705.86 12./8/2014 14.76 698.49 New Survey 709.86 712.64 10/27/2015 9.93 702.71 11/16/2016 11.07 701.57 10/11/2017 12.93 699.71 10/31 /2018 6.72 705.92 9/11/2019 17.60 695.04 10/9/2020 15.57 694.29 10/27/2021 15.62 697.02 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 21 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) W-413 50 52.7 711.70 713.93 11/14/2000 10.71 703.22 9/4/2001 11.11 702.82 9/17/2002 10.27 703.66 9/11/2003 NM NM 8/16/2004 7.90 706.03 12/19/2005 7.79 706.14 8/21 /2006 10.59 703.34 9/24/2007 11.00 702.93 2/23/2009 6.50 707.43 3/29/2010 5.78 708.15 11/1/2011 7.58 706.35 11/16/2012 10.50 703.43 W-5 60 50-60 702.06-692.06 750.86 752.06 11/14/2000 32.28 719.78 9/4/2001 33.84 718.22 9/17/2002 38.61 713.45 9/11/2003 26.85 725.21 8/16/2004 29.64 722.42 12/19/2005 32.30 719.76 8/21 /2006 33.11 718.95 9/24/2007 32.50 719.56 2/23/2009 31.97 720.09 3/29/2010 27.64 724.42 11/1/2011 32.63 719.43 11/16/2012 32.35 719.71 W-6 57 42-57 701.8-686.8 742.17 743.80 11/14/2000 30.43 713.37 9/4/2001 31.59 712.21 9/17/2002 35.47 708.33 9/11/2003 22.78 721.02 8/16/2004 27.95 715.85 12/19/2005 30.36 713.44 8/21 /2006 30.81 712.99 9/24/2007 29.86 713.94 2/23/2009 28.53 715.27 3/29/2010 24.32 719.48 11/1/2011 30.13 713.67 11/16/2012 30.15 713.65 W-6A 90 80-90 664.9-654.9 742.91 744.90 11/14/2000 32.45 712.45 9/4/2001 33.70 711.20 9/17/2002 36.67 708.23 9/11/2003 24.62 720.28 8/16/2004 30.20 714.70 12/19/2005 32.51 712.39 8/21 /2006 32.85 712.05 9/24/2007 32.15 712.75 2/23/2009 30.39 714.51 3/29/2010 26.17 718.73 11/1/2011 32.99 711.91 11/16/2012 33.17 711.73 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 22 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) W-613 35 20-35 724.39-709.39 743.13 744.39 11/14/2000 29.75 714.64 9/4/2001 30.98 713.41 9/17/2002 33.71 710.68 9/11/2003 22.34 722.05 8/16/2004 27.00 717.39 12/19/2005 29.44 714.95 8/21/2006 29.97 714.42 9/24/2007 28.86 715.53 2/23/2009 27.99 716.40 3/29/2010 23.70 720.69 11/1/2011 28.03 716.36 11/16/2012 27.33 717.06 W-12 60 50-60 685.84-675.84 734.14 735.84 12/19/2005 21.65 714.19 8/21/2006 NM NM 9/24/2007 20.96 714.88 2/23/2009 19.83 716.01 3/29/2010 15.45 720.39 11/1/2011 21.26 714.58 11/16/2012 21.30 714.54 W-12A 25 10-25 725.74-710.74 733.62 735.74 12/19/2005 21.61 714.13 8/21/2006 NM NM 9/24/2007 NM NM 2/23/2009 20.19 715.55 3/29/2010 15.93 719.81 11/1/2011 21.71 714.03 11/16/2012 21.50 714.24 W-13 20 10-20 744.4-734.7 752.40 754.70 11/14/2000 DRY -- 9/4/2001 DRY 9/17/2002 DRY -- 9/11/2003 24.25 730.45 8/16/2004 14.30 740.40 8/21/2006 DRY -- 2/23/2009 35.97 718.73 3/29/2010 4.30 750.40 11/1/2011 18.61 736.09 11/16/2012 dry W-14 23 8-23 715.9-700.9 721.3 723.90 12/19/2005 16.68 707.22 8/21/2006 NM NM 9/24/2007 13.32 710.58 2/23/2009 3.52 720.38 3/29/2010 2.56 721.34 11/1/2011 11.72 712.18 11/16/2012 12.52 711.38 W-15 55 35-55 727.36-707.36 760.0 762.36 8/21/2006 NM NM 2/23/2009 NM NM 3/29/2010 NM NM 11/1/2011 40.96 721.40 11/16/2012 40.27 722.09 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 23 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) W-16 38 28-38 714.01-704.01 739.8 742.01 9/17/2002 29.73 712.28 9/11/2003 NM NM 8/16/2004 NM NM 8/21/2006 NM NM 2/23/2009 22.53 719.48 3/29/2010 18.42 723.59 11/1/2011 23.69 718.32 11/16/2012 23.62 718.39 W-17 20.5 23 687.44 708.4 710.44 12/19/2005 6.97 703.47 8/21/2006 9.40 701.04 9/24/2007 11.00 699.44 2/23/2009 7.80 702.64 3/29/2010 4.62 705.82 11/1/2011 9.86 700.58 11/16/2012 10.20 700.24 W-18 41.5 31.5-41.5 722.21-712.21 751.4 753.71 12/19/2005 35.01 718.70 8/21/2006 36.45 717.26 9/24/2007 37.10 716.61 2/23/2009 36.08 717.63 3/29/2010 33.81 719.90 11/1/2011 36.69 717.02 11/16/2012 37.55 716.16 W-19 40 30-40 717.33-707.33 744.3 747.33 8/21/2006 NM NM 9/24/2007 29.14 718.19 2/23/2009 28.75 718.58 3/29/2010 24.68 722.65 11/1/2011 29.22 718.11 11/16/2012 29.00 718.33 W-20 10 5-10 712.24-707.24 715.14 717.24 12/19/2005 5.14 712.10 8/21/2006 6.65 710.59 9/24/2007 7.10 710.14 2/23/2009 4.59 712.65 3/29/2010 4.05 713.19 11/1/2011 7.01 710.23 11/16/2012 7.61 709.63 W-21 33.4 33.4 684.78 716.00 718.18 11/14/2000 15.73 702.45 9/4/2001 16.41 701.77 9/17/2002 17.15 701.03 9/11/2003 14.00 704.18 8/16/2004 14.94 703.24 12/19/2005 14.18 704.00 8/21/2006 15.59 702.59 9/24/2007 15.91 702.27 2/23/2009 14.60 703.58 3/29/2010 9.48 708.70 11/1/2011 15.02 703.16 11/16/2012 15.70 702.48 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 24 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) W-23A 75 65-75 707.66-697.66 770.18 772.66 11/14/2000 41.41 731.25 9/4/2001 42.91 729.75 9/17/2002 45.30 727.36 9/11/2003 31.29 741.37 8/16/2004 38.17 734.49 12/19/2005 42.06 730.60 8/21/2006 40.94 731.72 9/24/2007 42.30 730.36 2/23/2009 40.10 732.56 3/29/2010 36.44 736.22 11/1/2011 41.74 730.92 11/16/2012 41.65 731.01 W-23B 55 40-55 731.89-716.89 769.60 771.89 11/14/2000 41.00 730.89 9/4/2001 42.37 729.52 9/17/2002 44.54 727.35 9/11/2003 31.29 740.60 8/16/2004 37.45 734.44 12/19/2005 41.29 730.60 8/21/2006 40.42 731.47 9/24/2007 42.57 729.32 2/23/2009 39.55 732.34 3/29/2010 35.74 736.15 11/1/2011 41.01 730.88 11/16/2012 41.40 730.49 W-24 60 45-60 721.14-706.14 765.80 766.14 11/14/2000 40.45 725.69 9/4/2001 42.61 723.53 9/17/2002 NM -- 9/11/2003 NM 8/16/2004 NM 12/19/2005 NM 8/21/2006 NM 2/23/2009 NM 3/29/2010 NM 11/1/2011 NM 11/16/2012 NM NM W-25 58 43-58 727.27-712.27 770.80 770.27 11/14/2000 40.58 729.69 9/4/2001 42.47 727.80 9/17/2002 46.25 724.02 9/11/2003 35.75 734.52 8/16/2004 NM NM 12/19/2005 NM NM 8/21/2006 NM NM 2/23/2009 NM NM 3/29/2010 NM NM 11/1/2011 NM NM 11/16/2012 NM NM TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 25 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) W-26 53 38-53 721.65-706.65 759.20 759.65 11/14/2000 NM NM 9/4/2001 NM NM 9/17/2002 40.62 719.03 9/11/2003 NM NM 8/16/2004 NM NM 8/21/2006 NM NM 2/23/2009 NM NM 3/29/2010 NM NM 11/1/2011 NM NM 11/16/2012 NM NM W-27 58.5 43.5-58.5 721.7-706.7 765.50 765.20 11/14/2000 39.86 725.34 9/4/2001 41.37 723.83 9/17/02 NM NM 9/11/2003 NM NM 8/16/2004 NM NM 8/21/2006 NM NM 2/23/2009 NM NM 3/29/2010 NM NM 11/1/2011 39.05 726.15 11/16/2012 37.61 727.59 W-29 49.5 34.5-49.5 715.69-700.69 750.74 750.19 11/14/2000 28.22 721.97 9/4/2001 29.68 720.51 9/17/2002 28.01 722.18 9/11/2003 NM NM 8/16/2004 NM NM 8/21/2006 NM NM 2/23/2009 NM NM 3/29/2010 NM NM 11/1/2011 NM NM 11/16/2012 NM NM W-30 53 38-53 722.77-707.77 761.00 760.77 11/14/2000 34.47 726.30 9/4/2001 36.59 724.18 9/17/2002 40.16 720.61 9/11/2003 30.37 730.40 8/16/2004 NM NM 12/19/2005 NM NM 8/21/2006 34.92 725.85 9/24/2007 33.67 727.10 2/23/2009 32.79 727.98 3/29/2010 28.64 732.13 11/1/2011 33.73 727.04 11/16/2012 33.58 727.19 RW-NIS1 40 20-40 12/19/2005 10.51 -- 2/23/2009 9.43 -- 3/29/2010 8.72 -- 11/1/2011 3.79 -- 11/16/2012 5.57 RW-SIS1 50 30-50 12/19/2005 11.59 2/23/2009 NM -- 3/29/2010 NM -- 11/1/2011 NM -- 11/16/2012 NM TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 26 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) RW-SIS2 40 20-40 12/19/2005 6.48 2/23/2009 7.47 -- 3/29/2010 6.98 -- 11/1/2011 6.11 -- 11/16/2012 8.84 RW-SIS3 40 20-40 713.60 12/19/2005 6.67 706.93 2/23/2009 5.15 708.45 3/29/2010 4.05 709.55 11/1/2011 4.82 708.78 11/16/2012 5.43 708.17 RW-SIS4 45 1545 713.16 12/19/2005 4.38 708.78 2/23/2009 9.99 703.17 3/29/2010 2.51 710.65 11/1/2011 4.27 708.89 11/16/2012 4.00 709.16 RW-SIS5 12/19/2005 9.22 -- 2/23/2009 9.22 3/29/2010 5.50 11/1/2011 9.56 11/16/2012 8.50 RW-SIS6 12/19/2005 5.28 2/23/2009 6.15 3/29/2010 4.70 11/1/2011 5.73 -- 11/16/2012 6.70 RW-LFS1 50 30-50 696.44 12/19/2005 14.71 681.73 2/23/2009 12.09 684.35 3/29/2010 10.97 685.47 11/1/2011 11.88 684.56 11/16/2012 11.74 684.70 RW-LFS2 50 30-50 697.48 12/19/2005 19.39 678.09 2/23/2009 13.16 684.32 3/29/2010 12.05 685.43 11/1/2011 13.49 683.99 11/16/2012 12.96 684.52 NM = Not measured BGL = Below ground level MSL = Mean sea level BTOC = Below top of well casing TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 1 of 15 VOLATILE ORGANIC COMPOUNDS (ug/L) i i 0 c> y su °1 y Sample i i N b o ^' CD ^' Sample I.D. Date �. �. b 0 q 0 b 0 a 3 3 n n n 3 b c, m c, 0 S 0 S S S S i (D O S O S 3 F 0 S S_ 0 S 3 O O O O O O A y 0 O S 0 O `G fD O O O 3 S v O' 0 O' 0 0 'a W 0 a 0 a n 0 0 n m N 0 fD .. fD .. (D .fD. .Oi O _ O 0 (D O 3 S M 3 M .. O M fD 3 S (DD �+ O_ (DD .* (DD �+ S_ M < O S S S S S -a x .+ N O S �+ O S S N O S C S S O O O 0 v 3 0) 3 a) 3 (D 3 a) 3 a) 3 N 3 O 3 (D 3 0: CND 3 a) 3 c) 3 CD 3 CD 3 M CD 3 M 3 fD 3 CD 3 O. m n fp CD CD fD fD fD fD fD CD fD M fD fD fD fD fD fD CD M fD M fD to NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 MW-1 1/28/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3/5/2009 17 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 15.3 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.1 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 3/31/2010 0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11/2/2011 0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <3.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 11/20/2012 54 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 54.4 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 1/21/2013 ND <2.0 12/9/2013 ND <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 ND 12/8/2014 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/26/2015 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 11/14/2016 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/11/2017 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 11/1/2018 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 9/10/2019 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/13/2020 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 10/26/2021 ND <1 <1 <1 <1 <1 I <1 <2 I <20 <1 <1 I <1 <1 <1 <1 <1 <1 <1 <1 I <1 <1 <1 <1 <2 ND MW-2A 1/24/1997 4 4 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND MW-2C 1/24/1997 620 160 ND 260 98.0 30.0 ND ND ND 7 J ND 3 J 10 J ND ND ND ND 6 J ND ND 13.0 31.0 ND 2.0 7/15/1998 600 ND 100 290 D 140 ND ND ND ND 5.0 ND ND ND ND ND ND ND 6.0 ND ND 9.0 50.0 ND ND 2/24/2009 102 <1.0 <1.0 41.1 <1.0 2.8 <1.0 49 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.8 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 4.9 <2.0 ND MW-3A 8/6/1996 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1/29/1997 24 ND ND ND ND ND ND ND ND 3 J ND 15 ND ND ND ND ND ND ND ND ND ND ND 6 MW-3B 7/15/1998 139 ND ND ND ND ND ND 120 J ND 3 J 14 2 J ND ND ND ND ND ND ND ND ND ND ND 9/26/2000 186 <5 <5 <5 <5 <5 <5 160 NA <5 26 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 139 <5 <5 <5 <5 <5 <5 126 <10 <5 12.6 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND MW-3C 8/6/1996 273 11 ND 150 31 5.0 ND ND 6 37 ND ND ND ND 2 J 4J ND ND 14 13 ND ND 1/28/1997 197 6 ND 92 21 3.0 ND ND ND ND 41 14 ND NA ND 1 J ND ND ND 9 10.0 ND ND 9/26/2000 138 <5 <5 41 7.2 <5 <5 <100 NA <5 32 <10 <5 21 <5 <5 <5 37 <5 <5 <10 <10 ND 9/5/2001 178 <5 <5 22.6 <5 <5 <5 117 <10 <5 24.2 <10 <5 14.6 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/18/2002 152 <5 <5 18.4 <5 <5 <5 94.6 <10 <5 27.3 <10 <5 12 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2003 103 <5 <5 <5 <5 <5 <5 90 <10 <5 13.4 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/17/2004 132 <5 <5 19.4 <5 <5 <5 71 <10 <5 30.0 <10 <5 12.4 <5 <5 <5 <5 <5 <5 <10 <5 ND 2/27/2009 589 <1.0 <1.0 104 20.3 4.4 <1.0 160 <5.0 3.0 <1.0 151 32.7 <1.0 <1.0 70.1 <1.0 <1.0 1.9 <1.0 <1.0 2.5 39.4 <2.0 ND 3/30/2010 863 <1.0 <1.0 161 32.4 6.31 <1.0 186 <5.0 3.92 <1.0 249 45.7 <1.0 <1.0 108 <1.0 4.87 1.71 <1.0 <1.0 2.71 61 ND ND 11/1/2011 1,861 29.1 <0.5 396 144 14 <0.5 80 <0.5 9.94 <0.5 459 192 <0.5 <0.5 364 <0.5 <0.5 3.09 <0.5 1.15 8.74 157 <0.5 3.26 11 /20/2012 1,798 28.5 <0.5 361 106 <0.5 <0.5 268 <0.5 8.73 <0.5 386 150 <0.5 <0.5 314 <0.5 4.30 3.83 1.26 1.40 8.36 146 0.7 10.31 12/11/2013 2,268 18.6 <5 383 107 15 <5 549 <50 9 <5 559 137 <5 <5 318 <5 <5 <5 <5 <5 <5 173 <5 ND 12/11/2014 2,051 100 <1 290 170 <1 <1 311 <5.0 12 17.0 330 60 <1 <1 620 <1 <1 <1 <1 <1 11 130 <3 ND 10/27/2015 1,262 66 <1 210 100 <1 <1 308 >50 10 <1 350 40 <1 <1 410 <1 <1 <1 <1 <1 9.4 J 67 <30 ND 11/14/2016 872 67 <10 94 56 <10 <10 190 <10 5.4 J 12.0 150 <10 <10 <10 270 <10 <10 <10 <10 <10 6.0 27 <30 ND 10/10/2017 402 15 <1 57 22 1.8 <1 120 <20 2.2 <1 49 6.2 J <1 <1 100 <1 <1 0.81 J <1 0.73 J 2.0 31 <3 1.70 11/2/2018 414 6 <1 54 30 1.9 <1 110 <20 3.2 <1 66 6.3 <1 <1 110 <1 <1 0.62 J <1 0.61 J 2.3 22 <3 2.60 9/11/2019 288 <10 <10 41 17 <10 <10 94 <200 <10 <10 50 <10 <10 <10 72 <10 <10 <10 <10 <10 <10 14 <30 ND 10/13/2020 246 1.7 <1 38 13 1.5 <1 64 <20 1.6 <1 50 5.4 <1 <1 46 <1 <1 <1 0.57 J 0.55 J 1.4 23 <2 ND 10/26/2021 156 <1 <1 37 2 1.4 <1 67 <20 0.93 J <1 36 2.8 <1 <1 9.8 <1 <1 <1 <1 0.53 J <1 21 <2 ND MW-4 1/27/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 2 of 15 n v; Sample iv N b p N CD N Sample I.D. �. �. b q b F 3 n n v 3 v Date 0 0 0 0 0 3- n 3 c, m F 0 c, 0 S S 3- 3- 3- p 3- O 3- S S S_ 3' 3 Q O O O O O O A y p O S O O K fD O O O 3 S C) 0 0 O' 0 0 0 W 0 a 0 0 a n 0 0 /� ♦/ N fD N .. fD .. (D O a O O (D O 3 S O 3 (DD O M O 3 S fOD a O_ fOD .. fOD .. S_ : C O S S S S S -a x .r N O N S O S S N O S C S S O O O 0 D) 3 D) 3 N 3 M 3 a) 3 a) 3 D) 3 O 3 (D 3 0: fD 3 N 3 D) 3 fD 3 fD 3 a CD 3 M 3 fD 3 M 3 3 O. m 0 fp fD CD fD M fD fD M M fD M fD fD fD fD fD CD M M fD M (D U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 MW-5 2/24/2009 19 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 18.6 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND MW-6 1/27/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND NA ND ND ND ND ND ND ND ND ND 9/26/2000 ND <5 <5 <5 <5 <5 <5 <100 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 40 <5 <5 <5 <5 <5 <5 40.2 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 24 <5 <5 <5 <5 <5 <5 24.4 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/22/2003 16 <5 <5 <5 <5 <5 <5 15.8 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/18/2004 14 <5 <5 <5 <5 <5 <5 13.8 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/3/2009 75 <1.0 <1.0 5.9 <1.0 <1.0 <1.0 36.8 16.2 <1.0 <1.0 1.0 <1.0 <1.0 <1.0 6.3 <1.0 2.4 2.9 <1.0 <1.0 1.6 2.0 <2.0 ND 3/30/2010 73 <1.0 <1.0 7.99 <1.0 <1.0 <1.0 47.9 <5.0 <1.0 <1.0 1.21 <1.0 <1.0 <1.0 7.47 <1.0 2.51 1.86 <1.0 <1.0 1.44 2.13 ND ND 11/1/2011 57 <0.5 <0.5 12.9 1.84 <0.5 <0.5 18.0 <0.5 <0.5 <0.5 3.86 2.58 <0.5 <0.5 11 <0.5 <0.5 0.52 <0.5 <0.5 1.92 3.66 <0.5 0.63 11/19/2012 58 <0.5 <0.5 13.2 <0.5 <0.5 <0.5 19.7 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 14 <0.5 <0.5 1.86 <0.5 0.68 2.46 4.87 <0.5 0.76 12/11/2013 48 <5 <5 13.8 <5 <5 <5 12.3 <50 <5 <5 6.50 <5 <5 <5 16 <5 <5 <5 <5 <5 <5 <5 <10 ND 12/12/2014 101 <1 <1 13 0.47 J <1 <1 58.4 <5 0.96 J <1 2.2 3.8 <1 <1 14 <1 <1 1.9 <1 0.65 J 1.7 4.7 <3 1.2 10/30/2015 69 <1 <1 10 <1 <1 <1 44.8 <5 0.63 J <1 2.0 J 2.2 J <1 <1 8.3 <1 <1 0.99 J <1 <1 1.2 3.2 <3 1.5 11/17/2016 90 <1 <1 12 <1 <1 <1 59 <20 0.74 J <1 1.9 J 2.1 J <1 <1 11 <1 <1 1.6 <1 0.56 J 1.6 3.2 <3 1.4 10/10/2017 53 <1 <1 7 <1 <1 <1 34 <20 15 J <1 1.7 J <1 <1 <1 6 <1 <1 <1 <1 <1 4.2 2.0 <3 ND 11/2/2018 118 <1 <1 12 <1 <1 <1 82 <20 0.63 J <1 2.7 2.1 <1 <1 13 <1 <1 0.79 J <1 0.54 J 1.1 3.3 <3 1.6 9/12/2019 67 <1 <1 5.4 <1 <1 <1 29 27.0 0.45 J <1 <1 <1 <1 <1 4.2 <1 <1 <1 <1 <1 <1 1.1 <3 ND 10/14/2020 76 <1 <1 12.0 <1 <1 <1 43 <20 0.75 J <1 2.8 2.0 <1 <1 10.0 <1 <1 0.81 J <1 0.51 J 1.7 3.0 <2 1.9 10/28/2021 51 <1 <1 7.2 <1 <1 <1 24 <20 0.63 J <1 3.2 1.8 <1 <1 8.8 <1 <1 0.85 J <1 0.41 J 2.0 2.2 <2 1.7 MW-7B 3/3/2009 244,324 2,630 <100X 25,800 10,100 9,760 <100X 28,900 12,000 <100X <100X 39,500 2,450 <100X <100X 36,100 181 48,100 522 6,020 <100X 251 15,800 1,740 4,470 MW-8 1/28/1997 119 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2 J 96 4.0 3/5/2009 47 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 10.8 15.2 6.6 <1.0 10.8 <1.0 <1.0 <1.0 <1.0 <1.0 3.3 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND MW-9 1/28/1997 1 ND ND ND ND ND ND ND ND 1 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND DUP-1 (MW-9) 1/28/1997 2 ND ND ND ND ND ND ND ND 2 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2/26/2009 182 <1.0 <1.0 1.5 <1.0 <1.0 <1.0 168 6.0 <1.0 <1.0 2.7 2.0 <1.0 <1.0 2.1 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND MW-10 1/27/1997 126 ND ND 6 ND ND ND 120 ND 2 J ND ND ND ND ND ND ND ND 1 J ND ND ND 7/14/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/26/2000 258 <5 <5 7.6 <5 <5 <5 250 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 335 <5 <5 <5 <5 <5 <5 335 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 234 <5 <5 <5 <5 <5 <5 234 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 221 <5 <5 <5 <5 <5 <5 221 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/19/2004 198 <5 <5 <5 <5 <5 <5 198 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/6/2009 176 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 162 6.4 1.1 <1.0 4.1 <1.0 <1.0 <1.0 <1.0 <1.0 2.2 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 3/29/2010 184 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 166 10.6 <1.0 <1.0 3.82 1.26 <1.0 <1.0 <1.0 <1.0 2.31 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11/1/2011 56 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 47 <0.5 <0.5 <0.5 3.99 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 6.45 11/19/2012 148 <5 74 <5 <5 <5 <5 74.4 <50 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 ND 12/10/2013 33 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 28.1 <5 <0.5 <0.5 2.27 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 2.7 12/10/2014 137 <1 <1 <1 <1 <1 <1 133 <5 <1 <1 2.6 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 1.2 10/26/2015 104 <1 <1 <1 <1 <1 <1 103 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 1.1 11/14/2016 130 <1 <1 <1 <1 <1 <1 130 <20 0.78 J <1 2.8 J <1 <1 <1 0.41 J <1 <1 <1 <1 <1 <1 <1 <3 ND 10/10/2017 150 <1 <1 <1 <1 <1 <1 150 <20 <1 <1 <1 1.8 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/31/2018 160 <1 <1 <1 <1 <1 <1 160 <20 <1 <1 0.93 J 1.1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 9/10/2019 74 <1 <1 <1 <1 <1 <1 72 <20 <1 <1 1.5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/12/2020 14 <1 <1 <1 <1 <1 <1 14 <20 <1 <1 0.46 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 10/26/2021 10 <1 <1 <1 <1 <1 <1 10 <20 <1 <1 0.46 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL SITE Page 3 of 15 j � 0 N z N Sample z N M s N <7 O p N „O.' rt N) Sample I.D. b q b S 0 n 0 < Date c) 0 S 0 S s s 0 S m 0 S 0 � p s (D p S_ 0 O S_ >. 3 3 S_ 3 3 N 0 O O O O O O A v p O S p O `G N O O O 3 co A tS S 0ii N C fD fD lD fD lD 0 cb 3 S 3 N 0O O O S_ O O_ lD fD S C 0 S 3 S 3 S -0 X N O N S M O S S N O S C S 3 O O 0 0 0) 3 0) 7 w 3 (D 7 0) 3 0) 3 0) 3 O 3 M 3 M a (D 3 0) 3 I 0) 3 fD 3 N 3 a CD 7 CD 7 (D 3 CD 7 a G) 0 U) lD CD fD fD M CD CD M fD CD fD CD 9 CD /D M CD CD CD (D CD M V) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 - MW-11 1/23/1997 84 5 J ND 4 J 3 J ND ND ND ND 4 J 9 ND ND NA 10 ND ND ND ND ND ND 2 J 47 9/28/2000 298 <5 <5 <5 <5 <5 <5 270 NA 8.6 12 <10 <5 <5 <5 7.7 <5 <5 <5 <5 <10 <10 ND 9/10/2001 314 <5 <5 <5 <5 <5 <5 288 <10 10.6 15.3 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/18/2002 434 <5 <5 <5 <5 <5 <5 283 <10 11.1 13.7 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 126 9/19/2003 118 <5 <5 <5 <5 <5 <5 94.2 <10 7.4 16.8 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/17/2004 120 <5 <5 <5 <5 <5 <5 94.1 <10 11.5 14.4 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/4/2009 74 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 39.8 11.6 5.4 <1.0 15.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.7 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND MW-12A 1/23/1997 11 2 J ND ND 3 J ND ND ND ND 2 J ND ND ND ND ND ND 2 J ND 2 J ND ND ND 7/10/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/30/2000 ND <5 <5 <5 <5 <5 <5 <100 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 12 <5 <5 <5 <5 <5 <5 <10 12.3 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/20/2002 27 <5 <5 <5 <5 <5 <5 11.7 14.9 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 28 <5 <5 <5 <5 <5 <5 11.9 15.6 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/18/2004 44 <5 <5 <5 <5 <5 <5 <10 43.7 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/6/2009 40 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 38.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.9 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 4/1/2010 6 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.50 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.09 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11/2/2011 38 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 29.0 <5 <0.5 <0.5 8.04 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.61 11/19/2012 203 <5 <5 <5 <5 <5 <5 203 <50 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 ND 12/10/2013 210 <5 <5 <5 <5 <5 <5 210 <50 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 ND 12/11/2014 226 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 210 8.3 <1.0 <1.0 5.6 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <3 1.7 10/27/2015 213 <1 <1 <1 <1 <1 <1 200 <5 <1 <1 11 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 2.2 11/14/2016 207 <1 <1 <1 <1 <1 <1 200 191 <1 <1 5.9 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 1.5 10/10/2017 273 <1 <1 <1 <1 <1 <1 260 <20 <1 <1 11 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 1.7 11/1/2018 93 <1 <1 <1 <1 <1 <1 79 <20 <1 <1 11 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 2.9 9/10/2019 189 <1 <1 <1 <1 <1 <1 180 16 J <1 <1 6.2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 2.9 10/13/2020 34 <1 <1 <1 <1 <1 <1 31 <20 <1 <1 1.0 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 2.0 10/26/2021 188 <1 <1 <1 <1 <1 <1 180 <20 <1 <1 5.8 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 1.7 MW-12B 1/23/1997 16 6 ND 2 J ND ND ND ND ND ND 8.0 ND ND ND ND ND ND ND ND ND ND ND 7/10/1998 11 ND ND ND ND ND ND ND ND ND 11 ND ND ND ND ND ND ND ND ND ND ND 9/28/2000 567 <5 <5 <5 <5 <5 <5 510 <5 18 <10 <5 11.0 <5 28 <5 <5 <5 <5 <10 <10 ND 9/6/2001 371 <5 <5 <5 <5 <5 <5 359 <10 <5 12 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/20/2002 221 <5 <5 <5 <5 <5 <5 211 <10 <5 10.2 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 262 <5 <5 <5 <5 <5 <5 250 <10 <5 12.4 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/18/2004 196 <5 <5 <5 <5 <5 <5 182 <10 <5 13.7 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/4/2009 224 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 199 17.6 <1.0 <1.0 5.8 <1.0 <1.0 <1.0 <1.0 <1.0 1.5 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 4/9/2010 191 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 176 12.6 <1.0 <1.0 2.50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11/2/2011 62 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 43 <5 <0.5 <0.5 13.0 <0.5 <0.5 <0.5 3.6 <0.5 <0.5 <0.5 <0.5 <0.5 1.5 <0.5 <0.5 1.1 11/19/2012 69 <10 <10 <10 <10 <10 <10 68.5 <100 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 ND 12/10/2013 83 <5 <5 <5 <5 <5 <5 71.4 <50 <5 <5 11.3 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 ND 12/11/2014 158 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 132 6.3 0.64 J <1.0 12.0 <1.0 <1.0 <1.0 3.4 <1.0 <1.0 <1.0 <1.0 <1.0 0.73 J <1.0 <3 4.2 10/27/2015 123 <1 <1 <1 <1 <1 <1 117 <5 <1 <1 4.7 <1 <1 <1 1.11 <1 <1 <1 <1 <1 <1 <1 <3 ND 11/14/2016 164 <1 <1 <1 <1 <1 <1 150 <20 0.5 J <1 11.0 <1 <1 <1 2.7 J <1 <1 <1 <1 <1 0.58 J <1 <3 3.4 10/10/2017 181 <1 <1 <1 <1 <1 <1 170 <20 0.94 J <1 8.3 <1 <1 <1 2.3 J <1 <1 <1 <1 <1 0.61 J <1 <3 2.7 11/1/2018 112 <1 <1 <1 <1 <1 <1 95 <20 0.51 J <1 11 <1 <1 <1 2.7 <1 <1 <1 <1 <1 <1 <1 <3 3.1 9/11/2019 133 <1 <1 <1 <1 <1 <1 120 <20 0.48 J <1 10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 3.1 10/13/2020 125 <1 <1 <1 <1 <1 <1 110 <20 0.75 J <1 9.5 <1 <1 <1 2.8 <1 <1 <1 <1 <1 <1 <1 <2 3.0 10/26/2021 120 <1 <1 <1 <1 <1 <1 110 <20 0.75 J <1 7.7 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 2.2 TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 4 of 15 �'71_ n v; Sample iv N b p N CDN Sample I.D. �. �. b q b F 3 n n v 3 v Date o n 0 0 0 3- n 3 c, m F n c, n S S 3- 3- 3- p 3- O 3- S S S_ 3' 3 O O O O O O 3A y p O' O S C 0 0 O o o n Do 0 a ' a n � O O O 0 N CD (D a O O (D O S O 3 (D O M O a O _ : CS -a x N N O S N O C S OO O O 0 D) 3 D) 3 N 3 M 3 a) 3 a) 3 D) 3 O 3 (D 3 CL fD 3 N 3 D) 3 fD 3 fD 3 a CD 3 M 3 fD 3 M 3 3 O. m n fA fD CD fD M fD fD CD I M fD fD I fD fD fD fD fD CD M M fD M (D U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 MW-12D 9/10/1998 ND ND ND ND ND ND ND ND ND ND ND NA NA ND ND ND NA ND ND ND ND 9/29/2000 132 <5 <5 <5 <5 <5 <5 120 NA <5 <5 <10 <5 <5 <5 12 <5 <5 <5 <5 <10 <10 ND 9/12/2001 54 <5 <5 <5 <5 <5 <5 14.4 39.6 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/20/2002 31 <5 <5 <5 <5 <5 <5 <10 21.9 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 9.5 10/22/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/5/2009 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 4/1/2010 6 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.58 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.15 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11/3/2011 11 <0.5 <0.5 0.99 <0.5 <0.5 <0.5 3.0 <5 <0.5 <0.5 2.22 <0.5 <0.5 <0.5 1.42 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 11/23/2012 79 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 77.6 <5 <0.5 <0.5 1.30 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 12/12/2013 ND <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 12/11/2014 1740 41 2.2 29 41 770 <1.0 5.3 5.3 12 6.3 480 <1.0 <1.0 <1.0 5 <1.0 66 47 32 <1.0 180 2.2 7.1 8.6 10/25/2015 ND <1 <1 <1 <1 <1 <1 4.29 J <5 <1 <1 1.1 J <1 <1 <1 0.49 J <1 <1 <1 <1 <1 0.56 J <1 <3 ND 11/18/2016 ND <1 <1 0.48 J 0.41 J <1 <1 4.9 J <20 <1 <1 0.76 J <1 <1 <1 0.79 J <1 <1 <1 <1 <1 <1 <1 <3 ND 10/11/2017 8 <1 <1 <1 <1 <1 <1 8.2 J <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 11/1/2018 16 <1 <1 0.82 J 1.4 <1 <1 7.2 <20 <1 <1 0.95 J <1 <1 <1 4.1 <1 <1 <1 <1 <1 1.8 1.5 <3 ND 9/11/2019 4 <10 <10 <10 <10 <10 <10 3.7 <200 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <30 ND 10/13/2020 3 <1 <1 <1 <1 <1 <1 3.1 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 10/26/2021 3 <1 <1 <1 <1 <1 <1 2.9 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND MW-14 8/6/1996 147 ND ND ND ND ND ND ND ND ND 140 ND ND ND ND ND ND ND ND 7 J ND ND 1/29/1997 2,118 ND ND 1 J ND ND ND 1,700 J ND 2 J ND 180 ND ND ND ND ND ND ND ND 3 J 7 J 1 J 46 MW-15A 1/30/1997 2,266 ND ND ND ND ND ND 1,700 ND 9 J ND 520 ND ND ND ND ND ND ND ND ND ND ND 37.0 9/5/2001 3,157 <5 <5 <5 <5 <5 <5 2,640 <10 <5 517 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/18/2002 2,140 <5 <5 <5 <5 <5 <5 1,500 <10 <5 635 <10 <5 5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/17/2003 2,424 <25 <25 <25 <25 <25 <25 1,910 <50 <25 514 <50 <25 <25 <25 <25 <25 <25 <25 <25 <50 <25 ND 8/18/2004 3,209 <25 <25 <25 <25 <25 <25 2,720 <50 <25 489 <50 <25 <25 <25 <25 <25 <25 <25 <25 <50 <25 ND 3/6/2009 2,238 <1.0 <1.0 <1.0 <1.0 <1.0 1.2 1,900 <5.0 <1.0 <1.0 335 <1.0 <1.0 <1.0 1.8 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 3/31/2010 1,211 <1.0 <1.0 <1.0 <1.0 <1.0 1.26 1,170 <5.0 <1.0 <1.0 32.7 <1.0 <1.0 <1.0 7.48 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11 /2/2011 940 <0.5 <0.5 <0.5 <0.5 <0.5 1.23 480 <5 1.27 <0.5 430 <0.5 <0.5 <0.5 1.64 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.92 14.96 11/19/2012 2,324 <10 <10 <10 <10 <10 <10 1,920 <100 <10 <10 404 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 ND 12/10/2013 3,308 <5 <5 <5 <5 <5 <5 2,950 <50 <5 <5 350 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 8.2 12/9/2014 2,405 <5 <5 <5 <5 <5 <5 1,970 <25 <5 <5 430 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <15 4.6 10/27/2015 2,159 <5 <5 <5 <5 <5 <5 1,740 <25 <5 <5 410 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <15 9.0 11/14/2016 2,334 <1 <1 <1 <1 <1 1.4 2,200 <20 0.49 J <1 110 <1 <1 <1 5.3 <1 <1 <1 <1 <1 0.45 J 0.93 J <3 17.3 10/11/2017 2,734 <1 <1 <1 <1 <1 1.8 2,600 <20 0.51 J <1 110 <1 <1 <1 5.8 <1 <1 <1 <1 <1 0.43 J 0.69 J <3 16.1 10/31/2018 1,796 <1 <1 <1 <1 <1 0.42 J 1,600 <20 0.67J <1 190 <1 <1 <1 0.45J <1 <1 <1 <1 <1 <1 <1 <3 6.2 9/10/2019 1,590 <5 <5 <5 <5 <5 <5 1,400 <100 <5 <5 190 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <15 ND 10/8/2020 1,449 <2 <2 7.7 9.9 <2 <2 1,100 <40 0.92 J <2 300 <2 <2 <2 17.0 <2 <2 <2 2.6 <2 <2 5.4 <4 9.0 10/28/2021 1,262 <1 <1 <1 <1 <1 <1 1,200 <20 <1 <1 60 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 1.9 MW-15B 1/30/1997 330 ND ND ND ND ND ND 210 J ND 1 J ND 110 ND ND ND ND ND ND ND ND ND ND ND 9.0 MW-16 1/21/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND MW-17 3/5/2009 305 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 258 30.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 5.8 <1.0 <1.0 1.7 <1.0 <1.0 5.9 3.2 <2.0 ND MRF-1 1/21/1997 63 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 63.0 ND ND ND 7/13/1998 53 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 53.0 ND ND ND 2/24/2009 65 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 28.3 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 6.9 <1.0 <1.0 <1.0 <1.0 <1.0 29.9 <1.0 <2.0 ND FM-F-2 1/21/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 5 of 15 �'71_ n v; Sample N N b 0 N N Sample I.D. Date �. 0 �. 0 b 0 q 0 b 0 F 3 n 3- n n 3 v c, m 3 ,� 0 v c, 0 S S 3- 3- 3- p 3- O S S F S S_ 3' 3 Q O O O O O O A y p O S O O K fD O O O 7 S C) 0 0 O' 0 0 0 W 0 a 0 0 a n 0 0 /� ♦/ N fD G N .. fD .. (D O a O O M O 3 S O 3 (DD O M O 3 S fOD a O_ fOD .. fOD .. S_ : C O S D) S D) S N S fD S a) -a a) x D) .r O N M O N N S N O S D) S N N M O S CD C M S N S M O 3 O O 0 3 3 3 3 3 3 3 3 3 0: 3 3 3 3 3 a 3 3 3 3 CL m 0 fA (D CD I M M N I N M M M M M M M M M CD M M N M M U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 OW -NISI 3/10/2009 214 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 180 9.9 <1.0 <1.0 20.6 <1.0 <1.0 <1.0 <1.0 <1.0 3.4 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND OW-DR1 9/28/2000 26,291 360 <5 4,300 1,000 150 <5 2,900 150 6,600 3,300 <5 4,100 33 310 18 420 26 14 2,400 210 ND OW-DR2 7/21/1998 11,612 400 J 1,500 D 480 J ND 3,400 J ND 150 2,900 D 1,100 D ND 40 J 460 J 22 ND 250 J 910 9/26/2000 25,240 460 <5 4,200 1,400 220 <5 4,900 NA 170 5,600 1,300 <5 3,500 25 120 19 260 77 28 2,800 161 ND 9/10/2001 27,394 695 <5 4,950 1,330 208 <5 3,450 <10 145 5,980 1,380 <5 5,700 27 107 36 271 11.3 27.8 2,880 196 ND 2/27/2009 25,306 1,230 7.3 3,550 1,580 141 1.3 4,180 46.8 113 <1.0 5,380 1,030 4.3 41.4 6,320 21.1 41.4 47.2 201 17.4 29.5 1,190 120 13.6 3/30/2010 24,982 1,330 <1.0 3,330 1,790 123 <5.0 3,910 <5.0 127 <1.0 5,510 1,090 <1.0 <1.0 6,400 <1.0 <1.0 <1.0 182 <1.0 <1.0 1,190 ND ND 11/1/2011 22,265 1,910 <25 3,000 2,050 121 <25 990 <250 101 <25 4,130 2,350 <25 <25 6,290 <25 <25 <25 153 <25 <25 1,100 38 32.0 11/23/2012 19,775 1,620 <50 2,230 1,430 <50 <50 2,180 <500 <50 <50 4,810 1,760 <50 <50 4,650 <50 <50 <50 177 <50 <50 918 <50 ND 12/11/2013 24,766 1,920 <50 2,730 1,920 120 <50 3,130 <500 154 <50 4,800 1,890 <50 <50 6,600 <50 <50 <50 172 <50 <50 1,330 <100 ND 12/12/2014 6,977 11 <100 19 15 3 <100 2,160 <5 1.1 1.8 4,500 <1.0 <1.0 <1.0 45 <100 <1.0 <100 160 <1.0 <100 13 48 ND 10/30/2015 12,595 720 <20 1,300 800 71 <20 1,630 <100 79 <20 3,400 480 <20 <20 3,200 <20 <20 24 95 14 J 22 750 24 J ND 11/18/2016 11,740 830 <20 1,300 860 150 <20 1,800 <400 65 <20 2,800 340 8.8 J <20 2,800 9.4 J <20 19 J 65 12 J 20 710 21 J ND 10/10/2017 4,103 100 <5 590 290 48 <5 990 <50 23 <100 920 45 <5 <5 840 <5 <5 5.9 5.4 4.7 J 5.4 240 4.5 J ND 11/2/2018 1,882 20 <10 250 110 16 <10 560 <200 8.9 J <10 380 13 <10 <10 430 <10 <10 <10 <10 <10 <10 94 <30 ND 9/11/2019 1,178 12 <5 200 84 11 <5 250 <100 7 <5 260 12 <5 <5 290 <5 <5 <5 <5 <5 <5 52 <15 ND 10/13/2020 1,060 10 <5 220 86 15 <5 280 <100 <5 <5 71 15 <5 <5 310 <5 <5 2.3 J <5 2.6 J <5 53 <10 ND 10/28/2021 742 5.2 <5 130 54 6 <5 250 <100 <5 <5 36 11 <5 <5 230 <5 <5 <5 <5 <5 <5 20 <10 ND OW-DR3 9/20/2002 3,989 <5 <5 221 <5 15.4 <5 1,050 <10 11.3 1,840 778 <5 8.9 <5 29.5 <5 <5 <5 <5 35.3 <5 ND 9/19/2003 2,815 <5 <5 201 <5 14.7 <5 690 <10 6.1 1,390 455 <5 11.1 <5 12 <5 <5 <5 <5 35.5 <5 ND 8/24/2004 4,403 <50 <50 452 <50 <50 <50 1,260 <100 <50 1,910 675 <50 <50 <50 <50 <50 <50 <50 <50 106 <50 ND 10/12/2004 3,438 <5 <5 353 <5 14.2 <5 916 <10 6.9 1,480 553 <5 26.2 <5 11.5 <5 <5 <5 <5 77.1 <5 ND 3/4/2009 2,184 <1.0 <1.0 251 5.3 25.1 <1.0 552 <5.0 3.3 <1.0 984 267 <1.0 5.8 38.7 <1.0 5.0 1.3 2.4 <1.0 2.6 40.6 <2.0 ND 11/26/2012 2,352 <0.5 <0.5 226 J 14.7 23.3 <0.5 471 <5 <0.5 <0.5 1,020 359 <0.5 <0.5 73.4 <0.5 5.5 2.06 2.16 1.21 6.55 92.8 0.61 279.57 12/10/2013 2,757 <5 <5 374 43.6 26.4 <5 793 <50 <5 <5 1,060 249 <5 <5 112.0 <5 <5 <5 <5 <5 7.70 85.3 <10 6.30 OW-DR4 9/23/2002 20,502 1,860 <5 4,320 2,010 226 <5 1,570 <10 121 323 282 <5 7,630 5.4 27.6 55.3 27.3 11.7 66.1 1,880 86.7 ND 9/22/2003 22,030 1,350 <50 4,850 1,860 181 <50 2,200 <100 107 562 311 <50 8,960 <50 <50 <50 <50 <50 65.4 1,530 53.5 ND 8/24/2004 20,516 1,840 <250 4,630 2,100 298 <250 1,480 <500 <250 608 <250 <250 7,880 <250 <250 <250 <250 <250 <250 1,680 <250 ND 10/12/2004 9,067 810 <5 3,110 1,230 167 <5 2,190 <10 77 353 <10 <5 <5 <5 <5 35.3 <5 18.8 39.3 987 50.0 ND 10/20/2004 20,733 1,700 <250 4,480 2,240 <250 <250 2,120 <500 <250 522 <500 <250 8,030 <250 <250 <250 <250 <250 <250 1,590 51.0 ND 2/25/2009 15,223 1,490 6.2 2,570 1,510 156 <1.0 1,300 56.0 96.4 <1.0 659 127 7.1 3.9 6,350 4.3 <1.0 44.9 12.9 17.7 96.3 677 38.5 ND OW-SIS-1 8/17/2004 9,885 1,770 6.0 768 1,580 201 <5 811 <10 95 111 <10 18.3 3,150 <5 160 215 <5 <5 774 213 12.8 ND 3/9/2009 16,834 2,820 11.6 1,280 2,950 256 <10.OX 1,360 107 180 <10.OX 179 54.1 29.6 <10.OX 5,200 <10.OX 146 412 <10.OX <10.OX 1,540 288 20.9 ND OW-SIS-2 2/24/2009 3,111 79.8 <1.0 579 277 26 <1.0 418 17.8 38.2 <1.0 29 14.8 <1.0 <1.0 1,030 4.9 356 3.8 36.1 2.1 3.9 167 28.2 ND OW-SIS-3 3/4/2009 41,840 9,110 14.4 4,320 4,640 172 2.7 2,540 158 167 <1.0 147 23.5 34.9 <1.0 13,600 46.2 3,330 103 132 72.6 1,620 1,400 207 ND OW-SF1 3/9/2009 57,440 2,920 48.4 4,980 5,530 1,860 <10.OX 6,670 242 89.6 <10.OX 2,160 1,840 194 <10.OX 20,400 15.7 680 437 618 40.2 1,290 7,240 185 ND OW-LFS-1 2/26/2009 782 <1.0 <1.0 1.5 <1.0 <1.0 <1.0 723 12.8 4.5 <1.0 1 20.8 12.0 <1.0 <1.0 4.3 2.4 <1.0 <1.0 1.1 <1.0 <1.0 <1.0 <2.0 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 6 of 15 n v; Sample iv N b p N CD N Sample I.D. Date �. �. b 0 q 0 b 0 F 3 n 3- n n 3 v c, m 3 v c, 0 S 0 S 3- 3- 3- p 3- O 3- S F 0 S S_ 0 3' 3 O O O O O O 3A y p O S O O K fD O O O S C) 0 0 O' 0 0 0 W 0 a 0 0 a n 0 0 /� ♦/ N CD C N .. fD .. K CD ,. fD ,. O O �p O 3 S M 3 (D O M fD 3 S fOD a O_ fOD .+ fOD .. S_ G O S S S 3 S -a x .r N O N S O S S N O S C S S O O O 0 D) 3 D) 3 N 3 M 3 a) 3 a) 3 a) 3 O 3 (D 3 0: fD 3 N 3 c) 3 fD 3 fD 3 a CD 3 M 3 fD 3 CD 3 3 O. m n fp fD CD fD M fD fD M M fD fD I fD fD fD fD I fD CD M M fD M (D U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 OW-LFS-2 2/26/2009 363 <1.0 <1.0 1.9 <1.0 <1.0 <1.0 329 9.0 2.4 <1.0 9.4 3.5 <1.0 <1.0 7.1 <1.0 <1.0 <1.0 <1.0 <1.0 1.1 <1.0 <2.0 ND 3/30/2010 281 <1.0 <1.0 2.33 <1.0 <1.0 <1.0 251 <5.0 2.17 <1.0 9.92 2.74 <1.0 <1.0 11.8 <1.0 <1.0 <1.0 <1.0 <1.0 1.15 <1.0 ND ND 11 /1 /2011 110 <0.5 <0.5 3.23 <0.5 <0.5 <0.5 65 <5 4.52 <0.5 10.1 1.90 <0.5 <0.5 20.7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.3 <0.5 3.5 11/19/2012 276 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 274 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2.12 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 12/11/2013 421 <5 <5 <5 <5 <5 <5 391 <50 <5 <5 <5 <5 <5 <5 29.6 <5 <5 <5 <5 <5 <5 <5 <10 ND 12/12/2014 306 <1.0 <1.0 1.9 <1.0 <1.0 <1.0 255 8.1 6.2 <1.0 15 3.8 <1.0 <1.0 12 <1.0 <1.0 <1.0 0.48 J <1.0 0.54 J 1.7 0.75 J 3.7 10/26/2015 285 <1.0 <1.0 1.8 J <1.0 <1.0 <1.0 253 <5 4.5 <1.0 11 <1.0 <1.0 <1.0 13 <1.0 <1.0 <1.0 <1.0 <1.0 0.93 J <1.0 0.45 J 3.4 11/14/2016 276 <1.0 <1.0 1.2 J <1.0 <1.0 <1.0 250 12 J 2.4 <1.0 11 0.76 J <1.0 <1.0 9 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <3 3.2 10/10/2017 248 <1 <1 1.1 J <1 <1 <1 240 <20 1.4 <1 4.6 1.5 J <1 <1 4.6 J <1 <1 <1 <1 <1 <1 <3 0.50 J 2.0 10/31/2018 404 <1 <1 <1 <1 <1 <1 360 <20 32.0 <1 9.3 1.3 <1 <1 0.80 J <1 <1 <1 <1 <1 <1 <1 <3 1.2 9/12/2019 213 <1 <1 0.8 J <1 <1 <1 210 <20 0.48 J <1 3.1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/12/2020 153 <1 <1 0.74 J <1 <1 <1 150 <20 1.2 <1 2.0 0.53 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 10/28/2021 284 <1 <1 0.79 J <1 <1 <1 270 <20 7.0 <1 3.8 1.3 <1 <1 <1 <1 <1 <1 <1 <1 <1 1.4 <2 ND PW-1 D 1/24/1997 659 ND ND 1 J 1 J ND ND 530 J ND ND 7 ND ND ND ND ND ND ND ND ND 120 ND ND ND 7/15/1998 110 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 110 ND ND ND PW-2D 2/7/1997 28 ND ND 10 ND ND ND ND 10 J ND ND ND 4 J ND ND ND 4 J ND ND ND ND ND ND ND 7/18/1998 11 ND ND 9 ND ND ND ND ND ND ND ND ND ND ND ND 2 J ND ND ND ND ND ND ND 2/26/2009 21 <1.0 <1.0 1 1.3 <1.0 <1.0 I <1.0 19.5 <5.0 I <1.0 <1.0 <1.0 I <1.0 <1.0 <1.0 I <1.0 <1.0 <1.0 I <1.0 <1.0 <1.0 I <1.0 <1.0 <2.0 ND PW-3D 2/7/1997 42,680 4,100 ND 370 J 790 15,000 ND ND ND 260 J ND 16,000 ND ND ND ND 1,300 990 740 ND 3,600 ND ND 160 7/17/1998 21,462 ND 650 D ND 520 J 8,100 D ND ND ND 160 ND 8,600 3 J 2 J ND 13 680 610 D ND ND 2,000 D 54.0 49.0 21.0 4/9/2010 22,149 <1.0 <1.0 393 82.5 8,840 <1.0 39.8 18.4 5.46 <1.0 174 <1.0 <1.0 <1.0 36.1 <1.0 99.1 137.0 7.72 <1.0 419 11.6 ND ND 11/3/2011 damaged 11/27/2012 8,532 54 <50 293 203 4,830 <50 55 <500 <50 <50 2,150 <50 <50 <50 54.0 <50 <50 222 82 <50 589 <50 <50 ND 12/17/2013 27,696 993 9.0 491 1,180 12,800 <5 19.5 <50 137 <5 7,250 <5 <5 <5 59.4 <5 979 723 338 <5 2,540 58.4 12.3 106.5 12/11/2014 73,348 1,500 <200 610 2,800 14,000 <200 67.6 <100 310 240 32,000 <200 <200 <200 100 <200 1,100 8,900 1,300 <200 9,300 150 180 790 10/29/2015 67,602 2,300 <200 660 2,100 17,000 <200 112 <1000 350 <200 32,000 <200 <200 <200 380 86 J 1,000 3,300 1,400 <200 7,000 120 J >600 160 J 11/16/2016 45,170 970 <100 400 870 20,000 <100 120 <2000 190 <100 16,000 <100 <100 <100 110 <100 1,100 1,300 610 <100 3,500 <100 <300 470 J 10/11/2017 70,050 1,700 <200 730 2,000 20,000 <200 180 <4000 330 <200 31,000 <200 <200 <200 280 <200 1,700 3,700 1,200 <200 7,100 120 J 130 760 J 11/2/2018 61,400 1,600 <200 660 2,000 17,000 <200 170 <4000 320 <200 27,000 <200 <200 <200 510 <200 1,400 3,100 1,100 <200 6,100 130 J 100 J 1101 9/11/2019 31,290 860 <200 480 1,100 14,000 <200 140 <200 190 J <200 11,000 <200 <200 <200 350 <200 1,300 620 470 <200 <200 <200 <600 780 J 10/14/2020 76,030 1,700 <200 800 2,900 20,000 <200 160 <4000 450 <200 32,000 <200 <200 <200 540 <200 1,800 4,800 1,300 <200 8,400 190 210 780 10/27/2021 1 42,540 890 <500 660 1,500 17,000 <500 1 160 1 <10000 280 <500 18,000 <500 <500 I <500 1 380 1 <500 1 1,800 1 1,200 1 670 1 <500 1 4,200 1 <500 1 <1500 1 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 7 of 15 n v; Sample N N b 0 N N Sample I.D. �. �. b q b F 3 n n v 3 ,� v Date 0 0 0 0 0 3- n 3 c, m F 0 c, 0 S S 3- 3- 3- p 3- O S S S S_ 3' 3 Q O O O O O O A y p O S O O K fD O O O 7 S C) 0 0 O' 0 0 0 W 0 a 0 0 a n 0 0 /� ♦/ N fD N .. fD .. (D O a O O M O 3 S O 3 (DD O M O 3 S fOD a O_ fOD .. fOD .. S_ : C O S S S S S -a x .r N O N S O S S N O S C S S O O O 0 D) 3 D) 3 N 3 fD 3 a) 3 a) 3 D) 3 O 3 M 3 0: N 3 N 3 D) 3 N 3 M 3 a CD 3 M 3 N 3 M 3 3 CL m 0 fp (D CD I M M N N fD I M M M M M M M M CD M M N M M U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 PW-41 1/29/1997 1,086 19.0 ND 440 19.0 280 ND ND ND 3 J 210 101 ND ND ND 4 J 4 J ND 7 J 100 4 J ND 7/13/1998 1,012 ND ND 240 D 26 J 200 D ND ND ND 3 J 110 J ND ND 140 J ND ND 101 2 J ND 111 130 DJ ND 140 9/26/2000 1,063 37.0 <5 290 28.0 200 <5 <100 <5 160 <10 <5 190 <5 <5 8 <5 <5 30 120 <10 ND 9/12/2001 1,532 47.8 <5 378 49.2 256 <5 108 <10 <5 211 <10 <5 277 <5 <5 30.6 <5 <5 47.4 127 <5 ND 9/19/2002 1,861 55.8 <15 451 64 306 <15 156 <30 <15 253 <30 <15 336 <15 <15 33.7 <15 <15 53.1 152 <15 ND 10/22/2003 1,781 95.3 <5 340 84 247 <5 232 <10 <5 228 <10 <5 361 <5 <5 18.7 <5 <5 27.5 147 <5 ND 8/26/2004 1,997 78.1 <20 359 78.9 409 <20 215 <40 <20 266 <40 <20 357 <20 <20 39.9 <20 <20 50.6 143 <20 ND 3/5/2009 1,441 45.2 <2.OX 227 66.5 192 <2.OX 204 15.4 <2.OX <2.OX 172 6.4 <2.OX <2.OX 288 <2.OX <2.OX 51.4 <2.OX <2.OX 67.2 106 <4.OX ND 4/2/2010 1,143 <1.0 <1.0 220 38.8 178 <1.0 224 8.12 2.32 <1.0 132 3.78 <1.0 <1.0 195 <1.0 3.19 21.3 <1.0 <1.0 28.5 87.6 ND ND 11/2/2011 1,077 456 <5 8.84 48.7 101 <5 44 <50 <5 <5 74.2 <5 <5 <5 204 <5 <5 17.3 <5 <5 118 4.99 <5 ND 11/20/2012 1,086 28.9 <0.5 122 65.5 135 <0.5 175 <50 <5 <5 84.3 <5 <5 <5 276 <5 <5 30 <5 <5 87.8 81.3 <5 ND 12/17/2013 1,276 62.2 <5 134 67.1 139 <5 143 <50 <5 <5 82.4 <5 <5 <5 406 <5 <5 9.4 <5 <5 110 123 <10 ND 12/8/2014 864 35 <5 73 48 87 <5 196 <25 <5 <5 63 3.1 J <5 <5 210 <5 <5 28 <5 <5 74 50 <15 ND 10/29/2015 942 33 <2 75 43 55 <2 206 <10 2.0 <2 88 <2 <2 <2 240 <2 <2 44 <2 1.3 J 95 57 <6 3.9 11/17/2016 933 59 <2 75 51 74 <2 210 <40 2.0 <2 71 <2 <2 <2 230 <2 <2 31 <2 1.5 J 80 47 <6 3.3 10/11/2017 906 46 <2 72 42 49 <2 240 <40 2.0 <2 77 3.5 J <2 <2 230 <2 <2 30 <2 1.7 J 70 45 <6 2.9 11/2/2018 853 46 <2 57 42 36 <2 220 <40 1.6 J <2 78 2.8 <2 <2 230 <2 <2 26 <2 1.3 J 64 46 <6 2.7 9/11/2019 720 32 <5 69 37 36 <5 200 <100 <5 <5 60 <5 <5 <5 230 <5 <5 13 <5 <5 <5 43 <15 ND 10/14/2020 789 30 <5 62 41 37 <5 160 <100 2.8 J <5 100 <5 <5 <5 220 <5 <5 32 2.0 J <5 65 42 <10 3.5 10/27/2021 585 26 <5 43 32 22 <5 180 <100 2.1 J <5 60 <5 <5 <5 170 <5 2.2 J 12 2.0 J <5 41 33 <10 2.6 PW-5D 1/30/1997 426 ND ND 20.0 ND 2.0 ND ND 76.0 2 J 140 33.0 8.0 NA ND 26 ND 10 ND ND 18 ND 91 7/14/1998 6,293 96 J ND 550 D ND 38.0 ND 1,300 ND 61 J 3,800 ND ND 22.0 19 J ND 9 J 260 D 3 J 5 J ND 99 J 31 9/26/2000 13,327 360 <5 2,400 500 150 <5 2,300 110 4,300 220 <5 1,600 21 6.3 17 180 31 28 1,000 104 ND 9/10/2001 13,445 437 <5 2,310 534 168 <5 1,680 <10 90.6 4,110 156 <5 2,280 19.3 11.1 31.7 205 6.6 30.8 1,270 105 ND 9/23/2002 14,201 552 <5 2,500 694 211 <5 1,920 <10 90.1 3,460 190 <5 2,900 16.9 6 27.6 169 7.5 26.2 1,330 101 ND 9/19/2003 753 <5 <5 57.6 <5 <5 <5 412 110.0 <5 164 <10 <5 9 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/18/2004 12,945 534 <5 2,360 757 177 <5 1,260 <10 78.0 3,240 <10 <5 2,980 15.6 <5 32.1 131 <5 15.7 1,280 85 ND 10/12/2004 6,457 166 <5 842 235 57.4 <5 2,420 33.4 31.6 1,240 <10 <5 921 5.7 <5 9.5 44.0 <5 5.8 417 28.4 ND 2/27/2009 14,465 638 5.7 1,900 885 178 <1.0 2,390 36.4 83.4 <1.0 3,110 119 3.5 22.8 4,120 14.8 <1.0 38.3 131 12.1 26.4 672 78.7 ND 3/30/2010 12,428 481 <20.0 1,760 771 102 <20.0 2,170 <100 71.4 <20 3,070 210 <20.0 <20.0 3,040 <20.0 <20.0 <20.0 109 <20.0 <20.0 644 ND ND 11/3/2011 11,290 895 <50 1,760 925 103 <50 580 <500 <50 <50 2,440 488 <50 <50 3,450 <50 <50 <50 <50 <50 <50 649 <50 ND 11/23/2012 11,845 792 <5 1,290 896 109 <5 1,710 <50 51.9 <5 2,000 302 <5 <5 3,850 <5 <5 21.5 101 <5 22.2 602 49.8 47.6 12/16/2013 19,821 1,550 <5 2,200 2,200 181 <5 3,760 <50 121 <5 2,960 509 7.2 <5 5,300 <5 <5 <5 <5 29.7 <5 920 57.6 25.5 12/10/2014 18,168 860 <100 1,800 1,700 340 <100 1,740 <100 100 120 5,200 350 <100 <100 4,400 <100 <100 100 <100 160 <100 1,000 58 240 10/30/2015 7,514 280 <20 870 490 61 <20 1,390 <100 46 <20 2,000 52 <20 <20 1,900 <20 <20 14 J 45 8.8 J 9.2 J 380 13 J ND 11/18/2016 11,941 830 <50 1,400 960 190 <50 1,600 <1000 65 <50 3,000 240 <50 <50 2,900 <50 <50 28 J 66 <50 28 J 690 22 J ND 10/10/2017 4,536 120 <10 640 300 57 <10 1,100 <200 23 <10 830 36 <10 <10 1,200 <10 <10 5.0 J 4.0 J <10 5.1 J 230 4.1 J ND 11/2/2018 2,010 20 <10 280 110 15 <10 560 <200 11 <10 450 14 <10 <10 440 <10 <10 <10 <10 <10 <10 110 <30 ND 9/11/2019 940 7 <5 170 55 8 <5 240 <100 4.4 J <5 220 <5 <5 <5 180 <5 <5 <5 <5 <5 <5 56 <15 ND 10/13/2020 1,272 25 <5 370 21 26 <5 460 <100 9.2 <5 280 7.8 <5 <5 44 <5 <5 3.1 J 3.4 J 2.4 J <5 29 <10 ND 10/28/2021 834 7.6 <5 200 4 15 <5 400 <100 5.4 <5 180 <5 <5 <5 12 <5 <5 <5 <5 <5 <5 10 <10 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 8 of 15 n v; Sample N N b 0 N N Sample I.D. �. �. b q b F 3 n n v 3 ,� v Date 0 0 0 0 0 3- n 3 c, m F 0 c, 0 S S 3- 3- 3- p 3- O 3- S S S_ 3' 3 Q O O O O O O A y p O S O O K fD O O O 3 S C) 0 0 O' 0 0 0 W 0 a 0 0 a n 0 0 /� ♦/ N CD N .. fD .. (D O a O O M O 3 S O 3 (DD O M O 3 S fOD a O_ fOD .. fOD .. S_ : C O S S S S S -a x .r N O N S O S S N O S C S S O O O 0 D) 3 D) 3 N 3 M 3 a) 3 a) 3 D) 3 O 3 M 3 0: N 3 N 3 D) 3 N 3 M 3 a CD 3 M 3 N 3 M 3 3 O. m n fp (D CD M M N N CD M M M M M M M M CD M M N M M U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 PW-6D 7/21/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/2/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/12/2001 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/20/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/25/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/18/2009 3.8 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.8 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 3/31/2010 31.3 <1.0 <1.0 4.9 <1.0 <1.0 <1.0 5.70 <5.0 <1.0 <1.0 15.5 <1.0 <1.0 <1.0 3.24 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.0 ND ND 11/3/2011 damaged 11/21/2012 damaged 12/10/2013 damaged new well 12/10/2014 266 3.2 <1 41 16 <1 <1 43.2 <5 1.7 <1 90 <1 <1 <1 48 <1 <1 0.53J 1.1 <1 <1 20.0 1.5 ND 10/30/2015 116 2.7 <1 20 8.6 <1 <1 8.85 J <5 0.9 J <1 46 3.0 J <1 <1 31 <1 <1 <1 <1 <1 <1 7.9 <3 ND 11/17/2016 935 14.0 <5 140 59.0 5.2 <5 190 <100 5.4 <5 260 12.0 <5 <5 210 <5 <5 <5 <5 <5 <5 39 <15 ND 12/28/2016 13 NA NA NA NA NA NA 13 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/1/2017 600 NA NA NA NA NA NA 600 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 10/10/2017 1,626 19.0 <2 270 95 12.0 <2 450 <40 7.3 <2 320 20.0 <2 <2 370 <2 <2 1.5 <2 1.4 J 1.4 J 61 <6 ND 11/1/2018 996 7.4 <2 130 50 6.5 <2 320 <40 2.7 <2 230 6.1 <2 <2 210 <2 <2 1.3 <2 <2 1.1 J 31 <6 ND 9/12/2019 492 4.5 <1 120 42 4.7 <1 100 <20 1.4 <1 120 7.0 <1 <1 150 <1 0.84 J 0.84 J <1 1.6 <1 25 <3 ND 10/12/2020 210 <1 <1 47 1.1 3.2 <1 120 <20 0.92 J <1 27 2.3 <1 <1 6.7 <1 <1 <1 0.99 J <1 <1 3.1 <2 ND 10/28/2021 620 3.4 <5 110 38 5.3 <5 190 <100 2.2 J <5 93 5.6 <5 <5 150 <5 <5 <5 <5 <5 <5 22 <15 ND PW-61 1/28/1997 33 ND ND 11 ND 1 J ND ND ND ND 14 4 J ND ND 1 J ND ND ND 2 J ND ND ND 7/14/1998 46 ND ND 10 ND ND ND ND ND ND 14 4 J ND 5 ND ND 5 ND ND 3 J ND ND 5 9/26/2000 29 <5 <5 12 <5 <5 <5 <100 <5 8.4 <10 <5 8.3 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/12/2001 28 <5 <5 10.7 <5 <5 <5 <10 <10 <5 7.2 <10 <5 9.9 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 31 <5 <5 12.2 <5 <5 <5 <10 <10 <5 9.0 <10 <5 9.8 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/20/2003 47 <5 <5 12.1 <5 <5 <5 11.6 <10 <5 9.9 <10 <5 13 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/25/2004 42 <5 <5 10.6 <5 <5 <5 11.7 <10 <5 6.2 <10 <5 13.0 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/4/2009 8.2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.0 <1.0 2.4 <1.0 3.8 <1.0 <1.0 <1.0 <2.0 ND 3/31/2010 143.1 <1.0 <1.0 32 1.63 3.47 <1.0 22.5 <5.0 <1.0 <1.0 35.7 10.3 <1.0 <1.0 25.2 <1.0 <1.0 1.56 <1.0 <1.0 2.81 7.88 ND ND 11/3/2011 damaged 11/21/2012 damaged 12/10/2013 damaged new well 12/10/2014 115 0.41 J <1 26 2.2 <1 <1 47.9 <5 <1 <1 2.2 <1 <1 <1 24 <1 1.1 0.7 J 0.7 J <1 1.1 3.3 4.8 1.9 10/27/2015 98 <1 <1 20 1.1 J 3 <1 46.7 <5 <1 <1 7.6 <1 <1 <1 18 <1 <1 0.74 J <1 <1 1.4 <1 <3 1.1 11/17/2016 132 <1 <1 19 1.1 J 11 <1 56 <20 0.47 J <1 21 <1 <1 <1 18 <1 0.53 J 1.0 <1 <1 2.5 3.6 <3 3.89 J 10/10/2017 148 <1 <1 25 0.92 J 3.6 <1 71 <20 0.52 J <1 19 <1 <1 <1 25 <1 <1 0.42 J <1 <1 1.1 3.0 <3 1.4 11/1/2018 128 <1 <1 17 1.1 3.2 0.4 J 60 <20 0.58 J <1 14 <1 <1 <1 24 <1 <1 0.8 J <1 <1 1.7 4.7 <3 1.8 9/12/2019 148 <1 <1 19 1.0 2.9 <1 79 <20 0.74 J <1 13 <1 <1 <1 26 <1 <1 0.42 J <1 <1 <1 5.3 <3 1.8 10/13/2020 137 <1 <1 20 1.4 3.3 <1 63 <20 0.74 J <1 15 <1 <1 <1 26 <1 <1 0.52 J <1 0.43 J 1.6 4.5 <2 1.8 10/28/2021 115 <1 <1 11 0.74 J 2.1 <1 69 <20 0.62 J <1 9.6 <1 <1 <1 18 <1 <1 0.50 J <1 <1 <1 3.2 <2 2.0 PW-71 2/6/1997 11 ND ND 2 J ND ND ND ND 7 J ND 1 J ND ND ND ND ND ND ND 1 J ND ND ND 7/17/1998 443 86 ND 16 37 23 ND ND ND 2 J 77 ND ND 50 ND ND 65 9 ND 21 4 J 3 J 50 9/28/2000 99 <5 <5 9.2 15 7.2 <5 <100 NA <5 18 <10 <5 36 <5 14 <5 <5 <5 <5 <10 <10 ND 9/12/2001 158 <5 <5 <5 <5 <5 <5 150 <10 <5 8.1 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/20/2002 139 <5 <5 <5 <5 <5 <5 126 <10 <5 7.7 <10 <5 5 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/22/2003 161 <5 <5 <5 <5 <5 <5 144 <10 <5 9.8 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 6.8 8/25/2004 199 <5 <5 <5 <5 <5 <5 191 <10 <5 8.4 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/4/2009 75 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 50.5 6.8 <1.0 <1.0 11.8 <1.0 <1.0 <1.0 2.6 <1.0 <1.0 <1.0 <1.0 <1.0 1.4 <1.0 1.8 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 9 of 15 n v; Sample N N b 0 N N Sample I.D. �. �. b q b F 3 n n v 3 ,� v Date 0 0 0 0 0 3- n 3 c, m F 0 c, 0 S S 3- 3- 3- p 3- O S S S S_ 3' 3 Q O O O O O O A y p O S O O K fD O O O 3 S C) 0 0 O' 0 0 0 W 0 a 0 0 a n 0 0 /� ♦/ N fD N .. fD .. (D O a O O M O 3 S O 3 (DD O M O 3 S fOD a O_ fOD .. fOD .. S_ : C O S S S S S -a x .r N O N S O S S N O S C S S O O O 0 D) 3 D) 3 N 3 fD 3 a) 3 a) 3 D) 3 O 3 M 3 0: N 3 N 3 D) 3 N 3 M 3 a CD 3 M 3 N 3 M 3 3 O. m 0 fp (D CD M M N N CD I M M fD I M M M fD I M CD CD M N M fD 1 U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 PW-8S 1/28/1997 670 ND ND ND ND ND ND ND 670 J ND ND ND ND ND ND ND ND ND ND ND ND ND 7/13/1998 17 ND ND ND ND ND ND ND ND ND ND ND ND 7 ND ND ND ND ND ND ND ND 10 9/27/2000 7.7 <5 <5 <5 <5 <5 <5 <100 <5 <5 <10 <5 7.7 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 37 <5 <5 <5 <5 <5 <5 14.5 <10 <5 6.1 <10 <5 8.1 <5 <5 <5 <5 <5 <5 <10 <5 8.7 9/17/2003 180 <5 <5 <5 <5 <5 <5 <10 163 <5 11.3 <10 <5 6.0 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/17/2004 7.7 <5 <5 <5 <5 <5 <5 <10 <10 <5 7.7 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND PW-91 1/30/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 7/17/1998 50 ND ND ND ND ND ND ND 50 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3/12/2009 97 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 95.2 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND PW-10D 9/10/1998 15.0 ND ND 6.0 ND ND ND ND ND ND ND 9 J NA NA NA ND ND ND ND ND ND ND 9/26/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/12/2001 11 <5 <5 <5 <5 <5 <5 10.8 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 10.4 <5 <5 <5 <5 <5 <5 <10 10.4 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/17/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 2/26/2009 31 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.6 <1.0 <1.0 <1.0 <2.0 29.0 3/29/2010 2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.37 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11/1/2011 2 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <3.0 <5 <0.5 <0.5 1.56 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.72 <0.5 <0.5 <0.5 <0.5 ND 11 /21 /2012 ND <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 12/11/2013 ND <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 ND 12/10/2014 ND <1 <1 <1 <1 <1 <1 1.7 J <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 1.8 J ND 11/3/2015 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 11/17/2016 15 1.5 <1 2.3 J 4.9 J <1 <1 <1 <20 <1 <1 2.6 J <1 <1 <1 7.8 <1 <1 0.60 J 0.49 J <1 2.4 3.3 <3 ND 10/10/2017 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/31/2018 20 0.96 J <1 1.6 2.3 <1 <1 <2 <20 <1 <1 1.1 <1 <1 <1 8.6 <1 <1 <1 0.5 J <1 2.7 3.2 <3 ND 9/12/2019 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/12/2020 ND <1 <1 <1 <1 <1 <1 <1 <20 <1 <1 0.85 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 10/26/2021 ND <1 <1 <1 <1 <1 <1 <1 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND PW-101 1/27/1997 7.0 ND ND 6 ND ND ND ND ND ND ND ND ND ND 1 J ND ND ND ND ND ND ND 7/10/1998 8.0 ND ND 8 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/26/2000 14 <5 <5 14 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/11/2001 44 <5 <5 12.9 <5 <5 <5 31.4 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 39 <5 <5 <5 <5 <5 <5 14.7 24.6 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/18/2003 126 <5 <5 17 <5 <5 <5 109 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/17/2004 83 <5 <5 16.7 <5 <5 <5 61.3 <10 <5 <5 <10 <5 5.0 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/12/2009 150 <1.0 <1.0 12.7 <1.0 <1.0 <1.0 115 13.8 <1.0 <1.0 <1.0 1.5 <1.0 <1.0 5.2 <1.0 1.1 <1.0 <1.0 <1.0 1.1 <1.0 <2.0 ND 3/29/2010 229 <1.0 <1.0 12.6 <1.0 <1.0 <1.0 206 <5.0 <1.0 <1.0 1.38 1.96 <1.0 <1.0 4.86 <1.0 1.49 <1.0 <1.0 <1.0 <1.0 1.14 ND ND 11/1/2011 78 <0.5 <0.5 21.7 1.65 <0.5 <0.5 36 <5 <0.5 <0.5 1.95 3.73 <0.5 <0.5 8.64 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 3.18 <0.5 1.45 11/19/2012 440 220 <5 25.9 <5 <5 <5 183 <50 <5 <5 <5 <5 <5 <5 11.4 <5 <5 <5 <5 <5 <5 <5 <5 ND 12/11/2013 276 <5 <5 19.5 <5 <5 <5 249 <50 <5 <5 <5 <5 <5 <5 7.7 <5 <5 <5 <5 <5 <5 <5 <10 ND 12/10/2014 243 <1 <1 18 0.55 J <1 <1 205 <5 0.45 J <1 2.3 5.1 <1 <1 6.2 <1 <1 <1 <1 <1 <1 4.4 <3 1.6 10/29/2015 22 <1 <1 16 <1 <1 <1 222 <5 0.57 J <1 2.7 J 3.3 J <1 <1 4.2 J <1 <1 <1 <1 <1 <1 3.9 <3 2.3 11/17/2016 270 <1 <1 18 0.41 J <1 <1 240 <20 0.85 J <1 3.0 2.6 J <1 <1 5.2 <1 <1 <1 <1 0.45 J <1 4.1 <3 2.93 J 10/10/2017 226 <1 <1 5.7 <1 <1 <1 220 <20 <1 <1 <1 <1 <1 <1 1.4 J <1 <1 <1 <1 <1 <1 0.51 J <3 0.44 J 11/1/2018 319 <1 <1 13 <1 <1 <1 290 <20 0.96 J <1 2.5 3.7 <1 <1 4.2 <1 <1 <1 <1 <1 <1 3.4 <3 2.0 9/12/2019 292 <1 <1 12 <1 <1 <1 260 <20 1.0 <1 2.6 <1 <1 5.9 4.2 <1 <1 <1 <1 <1 <1 3.7 <3 2.4 10/12/2020 281 <1 <1 11 <1 <1 <1 250 <20 1.4 <1 2.9 4.0 <1 <1 4.5 <1 1.1 <1 <1 <1 <1 3.2 <2 2.7 10/26/2021 327 <1 <1 7 <1 <1 <1 310 <20 1.2 <1 2.2 2.9 <1 <1 <1 <1 <1 <1 <1 <1 <1 1.9 <2 1.7 TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 10of15 �'71_ n v; Sample N N b o N N Sample I.D. �. �. b q b � 3 n n v 3 ,� �,M. v x Date o n 0 0 0 3- n 3 c, m n c, n _<, S S 3- 3- 3- p 3- O S S S S_ 3' 3 O O O O O O 3A y p O S O O K fD O O O 7 S C) 0 0 O' o o n W n a ' ' a n ' 0 /� ♦/ N :D N .. fD .. K CD ,. fD ,. O O M O 3 S M 3 (D O M fD 3 S fOD a O_ fOD a fOD .. 3- : C O S S S S S -a x .r N O N S O S S N O S C S S O O O 0 C) 3 D) 3 N 3 M 3 a) 3 a) 3 D) 3 O 3 M 3 CL N 3 N 3 D) 3 N 3 M 3 a CD 3 M 3 N 3 CD 3 3 a m n fp (D CD M M N N CD M M M M M M N I M CD CD M N M N U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 PW-111 7/22/1997 458 ND ND ND ND ND 8 J ND ND ND ND ND ND ND ND ND ND ND 450 ND ND ND 7/16/1998 354 ND ND ND ND ND ND ND ND ND ND ND ND 47 ND ND ND ND ND 260 D ND ND 47 9/29/2000 156 <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 26 <5 <5 <5 <5 <5 130 <10 <10 ND 9/11/2001 254 <5 <5 <5 <5 <5 <5 14.3 <10 <5 <5 <10 <5 34.8 <5 <5 <5 <5 <5 205 <10 <5 ND 9/18/2002 274 <5 <5 <5 <5 <5 <5 22.3 <10 <5 <5 <10 <5 38.1 <5 <5 <5 <5 <5 214 <10 <5 ND 9/23/2003 516 <10 <10 <10 <10 <10 <10 50.3 <20 <10 <10 <20 <10 87.3 <10 <10 <10 <10 <10 378 <20 <10 ND 8/25/2004 365 <10 <10 21.5 <10 <10 <10 31.3 <20 <10 <10 <20 <10 82.7 <10 <10 <10 <10 <10 229 <20 <10 ND 3/5/2009 224 <1.0 <1.0 <1.0 <1.0 <1.0 1.7 13.2 8.4 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 36.2 <1.0 2.5 <1.0 <1.0 <1.0 162 <1.0 <5.0 ND PW-121 7/22/1997 8.0 ND ND ND ND ND ND ND 6 J ND ND ND ND ND 2 J ND ND ND ND ND ND ND 7/16/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/2/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/12/2001 1.0 <5 <5 <5 <5 <5 <5 1.0 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/22/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/17/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 9/27/2007 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/3/2009 6.7 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 6.7 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 3/31/2010 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11/2/2011 1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <3.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.69 <0.5 <0.5 <0.5 <0.5 ND 11/20/2012 9 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 8.55 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.22 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 1/21/2013 ND <2.0 12/17/2013 ND <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 ND 12/12/2014 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/30/2015 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 1.3 J <1 <1 <1 0.70 J <1 <1 <1 <1 <1 <1 <1 <3 ND 11/21/2016 ND <1 <1 <1 <1 <1 <1 <1 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/11/2017 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 11/6/2018 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 9/11/2019 ND <1 <1 <1 <1 <1 <1 1.2 J <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/14/2020 ND <1 <1 <1 <1 <1 <1 <1 <20 <1 <1 0.63 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 10/28/2021 ND <1 <1 <1 <1 <1 <1 <1 <20 <1 <1 0.63 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND PW-131 7/22/1998 295 16/14 NA 77176 35/26 ND/ND NA ND/ND ND/ND 2 J/2 J 6/6 ND/4 J NA ND/ND 3 J / 2 J 8/8 NA 4 J / 4 J 34/36 ND/ND 110/110 9/29/2000 754 27 <5 240 120 12 <5 <100 NA 8.2 11.0 11.0 <5 220 <5 <5 <5 <5 5.4 6.2 93 <10 ND 9/12/2001 892 16.4 <5 275 89.0 14.1 <5 70.9 <10 7.8 10.4 10.9 <5 305 <5 <5 <5 <5 <5 5.2 87.6 <5 ND 9/20/2002 799 <15 <15 243 67.4 <15 <15 128 <30 <15 <15 <30 <15 270 <15 <15 <15 <15 <15 <15 91 <15 ND 9/23/2003 1,027 11.7 <10 321 92.2 14.3 <10 118 <20 <10 21.7 <20 <10 358 <10 <10 <10 <10 <10 <10 90.4 <10 ND 8/25/2004 1,285 <5 <5 353 116 22.2 <5 166 <10 10.7 47.0 13.4 <5 405 <5 <5 5.6 <5 <5 8.4 138 <5 ND 3/4/2009 520 <1.0 <1.0 175 39.3 8.9 <1.0 78.0 <5.0 5.6 <1.0 18.1 4.1 <1.0 <1.0 133 <1.0 <1.0 1.8 <1.0 <1.0 2.6 53.9 <2.0 ND 3/31/2010 581 <1.0 <1.0 192 41.6 8.8 <1.0 92.4 <5.0 4.96 <1.0 14.5 3.66 <1.0 <1.0 158 <1.0 <1.0 1.07 <1.0 <1.0 2.08 62 ND ND 11/3/2011 784 6.18 <0.5 214 121 11.8 <0.5 27.0 <5 8.05 <0.5 31.4 7.27 <0.5 <0.5 243 <0.5 <0.5 <0.5 <0.5 <0.5 6.26 107 <0.5 0.87 11 /23/2012 779 2.10 <0.5 137 58.5 <0.5 <0.5 332 <5 2.21 <0.5 23.1 4.98 <0.5 <0.5 147 <0.5 <0.5 1.64 <0.5 <0.5 3.26 62.1 <0.5 5.21 12/16/2013 743 <5 <5 197 56.3 11.0 <5 139 <50 <5 <5 <5 <5 <5 <5 236 <5 <5 <5 <5 <5 <5 104 <10 ND 12/12/2014 564 <2 <2 150 53 11.0 <2 91.6 <10 4.0 <2 22 <2 <2 <2 160 <2 <2 1.5 <2 <2 2.8 69 <6 2.1 10/26/2015 419 <1 <1 120 28 4.6 <1 88.6 <5 3.2 <1 18 2.0 J <1 <1 110 <1 <1 1.2 <1 <1 2.1 41 <3 2.2 11/18/2016 433 <1 <1 120 34 5.0 <1 89 <20 2.9 <1 17 1.6 J <1 <1 120 <1 <1 1.3 <1 <1 2.3 40 <3 1.9 10/11/2017 350 <1 <1 100 20 4.8 <1 88 <20 2.5 <1 11 1.7 J <1 <1 80 <1 <1 0.83 J <1 <1 1.6 40 <3 1.9 10/31/2018 322 <1 <1 82 20 4.1 <1 81 <20 2.3 <1 12 1.3 <1 <1 84 <1 <1 0.86 J <1 <1 1.7 32 <3 1.5 9/11/2019 282 <1 <1 94 18 3.6 <1 44 <20 2.4 <1 8.9 1.4 <1 <1 72 <1 <1 0.72 J <1 0.44 J <1 38 <3 ND 10/13/2020 146 <1 <1 110 1.6 4.0 <1 68 <20 2.7 <1 11.0 2.5 <1 <1 7.8 <1 <1 <1 0.65 J <1 0.51 J 6.1 <2 0.93 J 10/28/2021 171 <1 <1 87 <1 1.2 <1 70 <20 2.3 <1 9.4 1.2 <1 <1 <1 <1 <1 <1 0.53 J <1 <1 0.94 J <2 0.74 J TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 11 of 15 �'71_ n v; Sample N N b 0 N N Sample I.D. �. �. b q b � 3 n n v 3 ,� �, v x Date 0 0 0 0 0 3- n 3 c, m 0 c, 0 _<, S S 3- 3- 3- p 3- O 3- S S S_ 3' 3 O O O O O O 3A y 0 O S O O K fD O O O S C) 0 0 O' 0 0 0 W 0 a 0 0 a n 0 0 /� ♦/ N :D N .. fD .. (D O a O O M O 3 3 O 3 (DD O M O 3 S fOD a O_ .+ .' 3 : C O S -a x .+ N O N S O S S N O S C S S O O O 0 C) 3 D) 3 a) 3 M 3 a) 3 a) 3 a) 3 O 3 M 3 0: N 3 N 3 D) 3 N 3 M 3 a CD 3 M 3 N 3 M 3 3 a m n fp (D CD N M N N M CD M M M M M N M CD CD M N M N U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 PW-14D 7/22/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/31/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/10/2001 81 <5 <5 <5 <5 <5 <5 <10 73.1 <5 <5 <10 <5 <5 <5 7.6 <5 <5 <5 <5 <10 <5 ND 9/17/2003 71 <5 <5 <5 <5 <5 <5 <10 70.7 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/17/2004 25 <5 <5 <5 <5 <5 <5 <10 25.2 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 16 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <2/<2 16.3/18.1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <2/<2 ND 7/26/2007 13 <1 <1 <1 <1 <1 <1 <2 12.6 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/11/2009 14 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 13.4 <1.0 <1.0 1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 3/31/2010 21 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 21.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11 /7/2011 23 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <3.0 13.6 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 9.2 11/27/2012 40 <0.5 <0.5 1.1 <0.5 <0.5 <0.5 35.4 <5 <0.5 <0.5 1.72 <0.5 <0.5 <0.5 2.18 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 12/12/2013 690 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 690 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 ND 12/9/2014 236 8.9 <1 25 17 <1 <1 28.7 16.0 1.9 1.2 75.0 6.9 <1 <1 44 <1 <1 0.41 J 1.1 <1 <1 10 2.9 J ND 11/3/2015 10 0.53 J <1 4.2 J 1.0 J <1 <1 8.33 J 8.5 J <1 <1 4.0 <1 <1 <1 5.9 <1 <1 <1 <1 <1 <1 <1 <3 ND 11/16/2016 9 0.64 J <1 3.1 J 0.96 J <1 <1 7.6 J <20 <1 <1 4.4 <1 <1 <1 5 <1 <1 <1 <1 <1 <1 0.89 J <3 ND 10/12/2017 972 5.9 <1 100 24 0.63 J <1 640 <20 1.7 <1 83.0 4.7 J <1 <1 110 <1 <1 0.87 J <1 <1 0.59 J 7.8 <3 ND 11/5/2018 153 <1 <1 0.91 J <1 <1 <1 2.4 <20 0.71 J <1 1.5 <1 <1 <1 1.6 7.7 <1 <1 23 <1 <1 <1 59 ND 9/17/2019 19 <1 <1 0.55 J <1 <1 <1 <2 10 J <1 <1 1.4 <1 <1 <1 0.89 J 1.6 <1 <1 5.2 <1 <1 <1 11 ND 10/15/2020 16 <1 <1 0.44 J <1 <1 <1 <2 <20 <1 <1 1.4 <1 <1 <1 0.99 J 0.90 J <1 <1 2.7 <1 <1 <1 5.7 ND 10/27/2021 10 <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 0.80 J <1 <1 <1 0.76 J 0.67 J <1 <1 1.7 <1 <1 <1 4.2 ND PW-14S 7/23/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/30/2000 ND <5 <5 <5 <5 <5 <5 <100 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/19/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 7/28/2007 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/10/2009 28 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 28.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND PW-15D 7/21/1998 841 ND 150 ND 8 320 J ND ND 14.0 220 D 75.0 3 J ND 3 J 38.0 ND 10.0 10/31/2000 9,042 46.0 <5 710 57 19 <5 1,800 NA 73.0 5,100 690 <5 220 <5 68.0 <5 25.0 5.4 6.5 200 22.0 ND 9/6/2001 12,582 <5 <5 1,150 <5 <5 <5 3,650 <10 <5 5,930 813 <5 653 <5 <5 <5 <5 <5 <5 386 <5 ND 9/16/2003 2,467 24.0 <5 349 78.2 14.1 <5 622 <10 <10 728 162 <5 352 <5 20.1 <5 <5 <5 <5 118 <5 ND 8/19/2004 507 <5 <5 105 19.7 <5 <5 126 <10 <10 107 27.0 <5 104 <5 <5 <5 <5 <5 <5 17.8 <5 ND 8/29/2006 8,571 234 <10 1,450 507 65.2 <10 1,650 <50 57.3 1,910 200 <10 1,920 <10 16.9 10.1 <10 <10 <10 550 <20 ND 9/26/2007 1.8 <1 <1 1.8 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/11/2009 11,715 426 3.6 1,840 740 83.6 <1.0 1,990 37.1 69.3 <1.0 2,890 254 1.7 <1.0 2,530 1.9 7.4 20.2 31.6 8.4 7.1 713 52.2 7.4 3/30/2010 14,028 466 3.37 2,120 876 83.0 <1.0 2,230 40.1 82.1 <1.0 3,660 273 1.65 <1.0 3,360 <1.0 8.21 15.9 19.1 9.47 8.0 772 ND ND 11/7/2011 196 10.1 <5 39.4 <5 <5 <5 8 <50 <5 <5 61.9 <5 <5 <5 58.4 <5 <5 <5 <5 <5 <5 18.5 <5 ND 11/26/2012 6,608 424 1.89 1,160 612 64.6 0.59 1,180 <5 73.9 <0.5 812 J 351 <0.5 <0.5 2,070 6.56 7.23 12.0 53.2 12.0 7.48 483 37.5 50.63 12/12/2013 11,775 591 <5 1,440 593 70.5 <5 1,770 <50 67.3 88.4 2,920 536 <5 <5 2,920 <5 <5 <5 51.8 <5 <5 676 32.7 18.2 12/9/2014 12,358 520 <50 1,400 920 82.0 <50 1,930 <250 66.0 <50 3,600 470 <50 <50 2,700 <50 <50 <50 23.0 <50 <50 670 <150 ND 10/28/2015 4,734 68 <50 570 220 <50 <50 1,280 <250 28.0 <50 1,300 <50 <50 96 1,000 <50 <50 <50 <50 <50 <50 200 <150 ND 11/15/2016 3,812 63 <10 430 170 24 <10 1,300 <200 16.0 <10 910 99 <10 <10 690 <10 <10 <10 <10 <10 <10 110 <30 ND 10/12/2017 1,321 12 <1 200 66 7.9 <1 510 <20 4.2 <1 190 12 <1 <1 280 <1 <1 1.5 J <1 1.1 J 1.0 J 39 <3 ND 11/5/2018 572 3.1 <2 81 27 2.2 <2 240 <40 1.1 J <2 79 5.3 <2 <2 120 <2 <2 1.2 J <2 1.1 J <2 11 <6 ND 9/17/2019 176 <5 <5 30 8.9 <5 <5 91 <100 <5 <5 7.4 <5 <5 <5 39 <5 <5 <5 <5 <5 <5 <5 <15 ND 10/14/2020 36 <1 <1 3 6.2 <1 <1 <2 <20 <1 <1 4.7 <1 <1 <1 20 <1 <1 <1 <1 <1 <1 2.5 <2 ND 10/27/2021 106 <1 <1 18 5.2 0.53 J <1 53 <20 <1 <1 2.0 <1 <1 <1 27 <1 <1 <1 <1 <1 <1 1.1 <2 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 12 of 15 �'71_ n v; Sample N N b o N N Sample I.D. Date �. �. b 0 q 0 b 0 F 3 n 3- n n 3 v c, m 3 ,� v c, o S n S 3- 3- 3- p 3- O S S F n n Q O O O O O O 3y p O O O SO C 0 0 O o o n Do n a ' a n O O O / fCD (D O O M O 3 O 3 (D O M Oa a O _ S -a K N N O S N O C S OO O O 0 D) 3 D) 3 a) 3 M 3 a) 3 a) 3 D) 3 O 3 M 3 CL N 3 N 3 D) 3 N 3 M 3 a CD 3 M 3 N 3 M 3 3 a m 0 fp (D CD I N M N N CD I M M M M M M N I M CD CD M N M N 1 U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 PW-15S 7/21/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/30/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 11 <5 <5 <5 <5 <5 <5 11.0 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 25 <5 <5 <5 <5 <5 <5 24.6 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/19/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 9/25/2007 1.5 <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 1.5 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/11/2009 78 <1.0 <1.0 1 18.6 4.8 <1.0 <1.0 1 6.6 13.4 1 <1.0 <1.0 <1.0 1 4.5 <1.0 I <1.0 1 26.5 <1.0 3.9 1 <1.0 <1.0 <1.0 <1.0 I <1.0 <2.0 ND PW-16D 7/22/1998 786 ND 130 ND 6.0 87.0 ND 7.0 380 140 ND 3 J ND 6.0 16.0 ND 11.0 11/2/2000 1,610 <120 <120 210 <120 <120 <120 <2,500 <120 1,400 <250 <120 <120 <120 <120 <120 <120 <120 <120 <250 <250 ND 9/6/2001 4,184 10.6 <5 355 12.3 8.9 <5 788 <10 29.3 2,580 250 <5 71.5 <5 22.7 <5 <5 <5 <5 55.2 <5 ND 9/17/2003 4,324 <100 <100 501 <100 <100 <100 858 <200 <100 2,680 <200 <100 285 <100 <100 <100 <100 <100 <100 <200 <100 ND 8/19/2004 2,722 <50 <50 353 <50 <50 <50 729 <100 <50 1,200 119 <50 215 <50 <50 <50 <50 <50 <50 106 <50 ND 8/29/2006 4,357 71.8 <10 732 178 31.5 <10 889 <50 31.1 1,370 78 <10 709 <10 <10 <10 <10 <10 <10 266 <20 ND 9/25/2007 5,130 <20 <20 844 247 36.5 <20 882 <100 36.8 1,700 75.5 <20 957 <20 <20 <20 <20 <20 <20 351 <40 ND 3/11/2009 6,570 110 1.5 1,160 372 50.5 <1.0 890 15.9 42.6 <1.0 1,950 93.5 <1.0 <1.0 1,400 <1.0 4.9 11.1 3.4 4.2 4.5 442 10.5 3.3 3/30/2010 6,295 88.2 <1.0 1,180 329 48.2 <1.0 1,080 27.2 39.9 <1.0 1,780 80.8 <1.0 <1.0 1,240 <1.0 4.85 4.97 1.50 3.03 3.59 384 ND ND 11/7/2011 7,345 232.0 <5 1,380 732 62.5 <5 260 <50 55.9 <5 1,770 405 <5 <5 1,740 <5 <5 <5 <5 <5 11.7 655 7.9 8.0 11/26/2012 7,820 165 1.01 1,090 543 50.4 0.52 1,260 <5 48.7 <0.5 2,100 229 <0.5 <0.5 1,680 <0.5 4.57 8.59 3.30 6.72 5.5 601 <0.5 23.1 12/12/2013 7,988 251 <5 1,360 688 65.9 <5 1,330 <50 55.2 37 1,870 245 <5 <5 1,700 <5 <5 <5 <5 <5 <5 368 5.7 12.0 12/9/2014 6,745 180 <20 920 490 60 <20 1,150 <100 36 <20 1,900 150 <20 <20 1,500 <20 <20 9.2 <20 <20 <20 350 <60 ND 10/28/2015 3,527 51 <20 480 190 18 <20 772 <100 22 <20 1,000 44 <20 <20 790 <20 <20 <20 <20 <20 <20 160 <60 ND 11/15/2016 2,461 46 <10 390 180 23 <10 650 <200 12 <10 520 <10 <10 <10 540 <10 <10 3.2 J <10 <10 2.1 J 100 <30 ND 10/12/2017 4 <1 <1 1.5 J 0.47 J <1 <1 3.9 J 13 J <1 <1 2.4 J <1 <1 <1 2.5 J <1 <1 <1 <1 <1 <1 0.66 J <3 ND 11/29/2017 2,284 21 <5 340 76 16 <5 870 <100 14 <5 490 14 <5 <5 370 <5 <5 2.4 J <5 <5 <5 73 <15 ND 11/5/2018 195 1.5 <1 40 12 0.96 J <1 84 <20 <1 <1 2.3 <1 <1 <1 53 <1 <1 <1 <1 <1 0.46 J 1.8 <3 ND 9/17/2019 99 0.51 J <1 20 4.5 <1 <1 28 <20 0.45 J <1 22 3.3 <1 <1 20 <1 <1 <1 <1 <1 <1 1.3 <3 ND 10/14/2020 68 <1 <1 4.6 9.1 <1 <1 <2 <20 <1 <1 17 1.2 <1 <1 30 <1 <1 <1 <1 <1 <1 5.8 <2 ND 10/27/2021 127 <1 <1 20.0 7.1 <1 <1 23 <20 <1 <1 40 1.5 <1 <1 32 <1 <1 <1 <1 <1 <1 3.6 <2 ND PW-16S 7/22/1998 ND ND NA ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/30/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/17/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/19/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 6.5 <1 <1 <1 <1 <1 <1 <2 6.5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 9/26/2007 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND PW-17 11/3/2000 160 <5 <5 <5 <5 <5 <5 160 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 12/20/2000 ND <5/<2 <5/<2 <5/<2 <5/<2 <5/NA <5/<10 <100/<100 NA/<100 <5/<2 <5/<10 <10/<10 <5/<2 <5/<2 <5/<2 <5/<10 <5/<2 <5/<2 <5/<2 <5/<2 <10/<2 <10/<5 ND 9/12/2001 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/22/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/25/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 8.8 <1 <1 <1 <1 <1 <1 <2 8.8 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 9/27/2007 6.3 <1 <1 <1 <1 <1 <1 <2 6.3 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/5/2009 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 13 of 15 n v; Sample N N b 0 N N Sample I.D. �. �. b q b F n n v 3 ,� v Date 0 0 0 0 0 3- n c, m F 0 a 0 S S 3- 3- 3- p 3- O 3- S S S_ 3' 3 Q O O O O O O A y p O S O O K fD O O O 3 S v 0 0 O' 0 0 'a 0 W 0 a a 0 0 0 m N m C N .. fD .. (D O a O _ O M O 3 S O 3 (D O M O 3 S fOD a O_ fOD fOD S_ O S S S S S -a x .r N O N S O S S N O S C S S O O O 0 Cl 3 D) 3 N 3 m 3 C) 3 C) 3 d 3 O 3 m 3 0: m 3 N 3 D) 3 m 3 m 3 a CD 3 M 3 m 3 M 3 3 O. Iv 0 fp (D CD M M N I N CD I M M fD I M M M M M CD M M N M M U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 PW-18 11/7/2000 19 <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 19.0 <5 <5 <10 <10 ND 12/20/2000 ND <5/<2 <5/<2 <5/<2 <5/<2 <5/NA <5/<10 <100/<100 NA/<100 <5/<2 <5/<10 <10/<10 <5/<2 <5/<2 <5/<2 <5/<10 <5/<2 <5/<2 <5/<2 <5/<2 <10/<2 <10/<5 ND 9/11/2001 24 <5 <5 <5 <5 <5 <5 <10 24.3 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 204 <5 <5 <5 <5 <5 <5 <10 195 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 8.9 ND 8/19/2004 149 <5 <5 <5 <5 <5 <5 22.8 119 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 6.8 ND 10/1/2004 27 <5 <5 <5 <5 <5 <5 <10 27.4 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 264 <1 <1 <1 <1 <1 <1 <2 151 <1 <1 <1 < <1 1.7 <1 <1 1.2 <1 <1 <1 16.3 93.8 9/26/2007 194 <1 <1 <1 <1 <1 <1 <2 108 <1 <1 <1 < <1 1.3 <1 <1 1.2 <1 <1 <1 12.0 71.1 3/12/2009 203 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 125 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.1 3.5 <1.0 <1.0 <1.0 <1.0 <1.0 9.8 63.7 3/31/2010 86 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 85.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.26 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11 /7/2011 143 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <3.0 92.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2.94 48.43 11 /26/2012 91 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 36.0 30.8 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.86 <0.5 <0.5 0.6 <0.5 <0.5 <0.5 6.73 24.5 1/21/2013 ND <2.0 12/12/2013 31 <5 <5 <5 <5 <5 <0.5 5.05 <50 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 25.6 2/25/2014 ND <2 12/9/2014 96 <1 <1 <1 <1 <1 <1 9.17 55 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 1 <1 <1 <1 6 30.7 1/29/2015 58 <1 <1 <1 <1 <1 <1 <2 35 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 4.9 18 10/26/2015 ND <1 <1 <1 <1 <1 <1 <2 40 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 0.65 J <1 <1 <1 1.2 J 19 11/15/2016 ND <10 <10 <10 <10 <10 <10 <10 <200 <10 <10 <10 <10 8.3 J <10 <10 <10 <10 <10 <10 <10 <10 <10 <30 ND 10/16/2017 ND <1 <1 <1 <1 <1 <1 <2 20 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 6.7 J 11/7/20018 35 <1 <1 0.65 J 0.91 J <1 <1 <2 20 <1 <1 0.42 J <1 <1 <1 2.8 <1 <1 <1 <1 <1 1.3 <1 0.58 J 7.3 1/10/2019 24 J <1 <1 0.65 J <1 <1 <1 <2 17 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 1.3 J 5.2 J 9/17/2019 Not Sampled 10/14/2020 Not Sampled 10/27/2021 Not Sampled PW-19 11/6/2001 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/18/2004 98 <5 <5 <5 <5 <5 <5 97.8 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/1/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 3.7 <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 3.7 9/27/2007 5.0 <1 <1 <1 <1 <1 <1 <2 5.0 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/11/2009 91 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 87.3 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.8 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 1/29/2015 <1 <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 0.57 J <1 <3 ND PW-DR-1 9/8/2004 248 <5 <5 10.7 <5 <5 <5 164 <10 <5 40.2 16.6 <5 16.4 <5 <5 <5 <5 <5 <5 <5 <5 ND 9/23/2004 268 <5 <5 5.6 <5 <5 <5 209 <10 <5 31.3 13.6 <5 8.3 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/8/2004 249 <5 <5 5.6 <5 <5 <5 213 <10 <5 30.8 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 2/25/2009 1,848 54.4 <1.0 213 98.8 7.7 <1.0 579 7.5 11.8 <1.0 400 58.3 <1.0 <1.0 314 2.2 <1.0 3.5 23.8 1.2 1.3 <1.0 71.2 ND PW-SIS1 8/25/2004 12,848 201 <5 3,370 765 223 <5 2,500 <10 69.5 39.0 <10 <5 5,060 <5 110 49.9 <5 <5 69.8 376 15.1 ND 3/9/2009 9,940 473 3.7 1,990 1,310 139 1.4 1,230 37.7 97.4 <1.0 68.1 38.8 3.7 <1.0 3,510 1 <1.0 6.0 121 3.2 49.0 263 555 39.9 ND W-1 1/29/1997 3 ND ND ND ND ND ND ND ND ND ND ND 3 J NA ND ND ND ND ND ND ND ND ND 9/27/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/10/2001 <5 <5 <5 <5 <5 <5 12.4 <10 <5 <5 <10 <5 <5 <5 <5 8.4 <5 <5 <5 <10 <5 ND 9/18/2002 20 <5 <5 <5 <5 <5 <5 11.5 <10 <5 <5 <10 <5 <5 <5 <5 8.2 <5 <5 <5 <10 <5 ND 9/17/2003 86 <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 76.4 <5 <5 9.7 <10 <5 ND 8/17/2004 43 <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 33.7 <5 <5 9.3 <10 <5 ND 3/3/2009 25 <1.0 <1.0 <1.0 3.3 <1.0 <1.0 <2.0 7.7 <1.0 <1.0 <1.0 <1.0 1.1 <1.0 <1.0 <1.0 <1.0 11.1 <1.0 <1.0 1.9 <1.0 <2.0 ND W-2 1/30/1997 87,240 30,000 ND 12,000 11,000 960 J ND ND 2,200 J 410 J ND ND 1,500 J ND ND ND 20,000 970 J 1,200 ND 1,200 5,300 500 J ND DUP-3(W-2) 1/28/1997 79,260 27,000 ND 11,000 9,500 930 J ND ND 2,300 J 410 J ND ND 1,400 J ND ND ND 19,000 910 1 1,200 ND 1,100 4,300 210 J ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 14of15 �'71_ n v; Sample N N b 0 N 3 N Sample I.D. Date �. �. b 0 q 0 b 0 � 3 n 3- n n 3 v c, m ,� �, v c, x 0 S 0 S 3- 3- 3- p 3- O S S 0 S S_ 0 3' _<, 3 Q O O O O O O A y p O S O O K fD O O O 7 S C) 0 0 O' 0 0 0 W 0 a 0 0 a n 0 0 /� ♦/ N fD N .. fD .. (D O a O O M O 3 S O 3 (DD O M O 3 S fOD a O_ fOD fOD S_ O S D) S D) S N S fD S O -a O K D) .r O N M O N N S N O S D) S N N M O S CD C M S N S M O 3 O O 0 3 3 3 3 3 3 3 3 3 0: 3 3 3 3 3 a 3 3 3 3 CL m 0 fp (D CD I M M N N CD M M M M M M M M CD CD M N M M U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 - W-4 2/6/1997 1,624 47.0 ND 640 86.0 23 J ND ND 6 J 30.0 8 J 35 J ND NA 7 J ND ND 7 J ND ND 280 5 J 450 9/27/2000 525 14.0 <5 200 57.0 8.4 <5 <100 NA 8.7 <5 <10 <5 170 <5 <5 <5 <5 6.7 <5 60.0 <10 ND 9/10/2001 49 <5 32.7 <5 <5 <5 <5 16.5 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/17/2002 18 <5 <5 <5 <5 <5 <5 18.2 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/17/2003 694 27.9 <5 135 56.9 10.9 <5 162 <10 <5 <5 <10 <5 248 <5 <5 <5 <5 <5 8.1 45.2 <5 ND 8/17/2004 3,157 136 <10 432 331 35.2 <10 547 <20 17.0 14.5 <20 <10 1,010 <10 <10 13.0 <10 <10 10.4 91.2 <10 ND W-4A 1/28/1997 75,370 13,000 ND 11,000 5,700 540 ND ND ND 890 J ND ND ND NA ND 39,000 ND 1,300 ND ND 2,600 280 J 1,060 9/27/2000 15,940 380 <5 4,300 1,500 160 <5 2,100 NA 230 67 50 <5 4,500 12.0 1,300 38.0 57 260 42.0 870 66.0 8.3 9/10/2001 37,215 619 <5 10,400 3,560 316 <5 2,770 <10 <5 125 111 <5 12,400 40.4 4,350 52.6 126 19.3 43.8 2,100 169 13.1 9/17/2002 31,439 515 <5 9,120 2,490 207 <5 1,950 <10 273 105 95.7 <5 10,500 24.4 3,570 38.5 59.4 10.9 28.5 2,330 122 ND 9/17/2003 5,351 83 <5 1,350 544 68.1 <5 1,090 <10 73 29.1 18.5 <5 1,740 <5 <5 16.8 15.1 <5 16 286 22.4 ND 8/17/2004 19,357 <100 <100 5,390 2,070 182 <100 1,870 <200 225 111 <100 <100 7,330 <100 831 <100 <100 <100 <100 1,230 118 ND 2/27/2009 6,307 73.4 <1.0 1,240 541 57.9 <1.0 942 13.4 98.4 <1.0 67.4 163 <1.0 3.3 2,260 7.3 78.8 8.3 11.3 6.5 12 686 36.8 ND 3/31/2010 10,920 401 <1.0 1,880 995 73.6 1.19 1,010 32.7 129 <1.0 91.9 238 <1.0 1.98 3,590 16.1 918 43.5 72.5 6.26 89 1,330 ND ND 11/2/2011 41,390 216 <50 5,340 3,750 363 <50 520 <500 861 <50 469 7,290 <50 <50 10,300 <50 1,130 <50 307 <50 83 11,000 281 ND 11/19/2012 4,144 28.7 <0.5 335 296 21.9 <0.5 1,600 <5 65.3 3.77 30 241 <0.5 0.95 693 3.28 155 1.48 16 2.87 4.27 622 20.11 3.74 12/17/2013 59,696 513 <50 7,580 3,260 318 <50 1,270 <500 843 <50 332 6,790 <50 <50 14,400 <50 15,300 <50 249 <50 <50 8,580 261 ND 12/8/2014 37,661 430 <100 4,700 2,700 360 <100 2,100 <100 560 <100 270 3,600 <100 <100 8,800 <100 6,300 <100 220 41 140 7,000 220 220 10/27/2015 8,952 270 <100 1,400 640 <100 <100 962 <500 210 <100 110 540 <100 <100 2,500 <100 <100 <100 120 <100 76 J 2,200 <300 ND 11/16/2016 9,410 380 <100 2,000 690 67 <100 660 <2000 260 <100 140 560 <100 <100 2,400 <100 220 <100 72 J <100 92 J 2,100 <300 ND 10/11/2017 2,832 24 <10 440 190 36 <10 630 <200 40 <10 39 66 <10 <10 570 <10 <10 4.3 J <10 <10 5.3 780 12 ND 10/31/2018 1,400 33 <5 260 110 7.6 <5 210 <100 14 <5 11 30 <5 <5 500 <5 <5 3.4 J <5 2.4 J 28 190 <15 ND 9/11/2019 435 12 <1 83 33 2.8 <1 54 <20 7.5 <1 4.4 13 <1 <1 130 <1 0.45 J 0.81 J <1 1.3 6 88 <3 ND 10/9/2020 344 13 <2 74 35 2.3 <2 30 <40 3.1 <2 6.7 4 <2 <2 120 <2 <2 <2 1.7 J 0.88 J 5.5 50 <4 ND 10/27/2021 513 24 <5 110 43 2.8 <5 54 <100 6.6 <5 <5 4.5 J <5 <5 170 <5 <5 <5 <5 <5 <5 98 <15 ND W-4B 2/4/1997 117,470 20,000 ND 13,000 8,700 810 J ND ND 4,500 J 1,200 J ND ND ND ND ND ND 61,000 550 J 2,800 ND ND 4,200 710 J ND W-5 8/7/1996 467,000 110,000 ND 27,000 21,000 ND ND 19,000 2,100 J 1,700 9,400 J ND ND ND 140,000 6,900 13,000 ND ND 36,000 3,900 J 77,000 2/24/1997 415,300 98,000 ND 26,000 19,000 2,000 ND ND 34,000 2,200 J 1,800 9,100 J ND ND 1,100 J 130,000 5,600 15,000 ND 24,000 33,000 5,200 9,300 10/30/2000 402,208 95,000 91.0 22,000 31,000 1,100 17.0 24,000 NA 1,000 1,200 2,200 190 72,000 760 100,000 3,500 8,900 340 11,000 25,000 2,540 370 9/10/2001 378,680 144,000 <5 14,000 33,300 <5 <5 13,800 <10 <5 <5 <10 <5 53,900 <5 63,200 7,710 9,270 <5 27,000 12,500 <5 ND 9/19/2002 672,790 121,000 <5,000 45,400 122,000 <5,000 <5,000 14,300 <10,000 7,780 11,100 <10,000 <5,000 74,300 5,880 93,100 28,900 35,300 <5,000 38,300 39,500 28,400 7,530 9/17/2003 367,940 135,000 <5,000 9,220 31,800 <5,000 <5,000 11,300 <10,000 <5,000 <5,000 <10,000 <5,000 56,400 <5,000 81,900 6,340 7,580 <5,000 28,400 <10,000 <5,000 ND 8/18/2004 375,700 177,000 <5000 5,290 36,600 <5000 <5,000 4,110 <10,000 <5,000 <5,000 <10,000 <5,000 41,400 <5,000 48,900 10,800 10,400 <5,000 41,200 <10,000 <5,000 ND 3/3/2009 170,238 66,700 75.8 3,720 15,500 289 <50.OX 1,860 1,380 1,420 <50 1,000 111 121 <50.OX 30,800 <50.OX 10,900 3,700 3,400 70.0 25,900 1,040 1,940 311.0 W-6 2/5/1997 123,360 23,000 ND 14,000 8,500 20,000 ND ND 3,400 J ND ND 15,000 ND ND ND ND 260 J 19,000 2,700 3,000 ND 2,400 5,100 1,400 2,800 DUP-1 (W-6 8/7/1996 143,900 27,000 ND 16,000 10,000 23,000 ND 2,800 ND ND 18,000 ND ND ND ND ND 21,000 6,200 3,300 ND 4,000 6,500 1,600 4,500 W-6A 2/5/1997 739,000 10,000 ND 65,000 16,000 48,000 ND ND 150,000 ND 21,000 ND ND ND ND 310,000 3,200 J 12,000 ND ND 6,800 J ND 97,000 9/28/2000 838,040 31,000 280 69,000 24,000 71,000 <5 81,000 <5 17,000 940 160 100,000 550 410,000 3,200 14,000 660 3,100 9,900 1,950 300 W-6B 2/5/1997 238,400 59,000 ND 23,000 14,000 19,000 ND ND 14,000 ND ND 18,000 ND ND ND ND 55,000 4,700 5,700 ND 11,000 1,000 J 1,000 J 13,000 W-13A 1/31/1997 1,688 66.0 ND 230 110 6 J ND 990 120 ND ND ND 5J ND ND ND 27.0 90 ND ND 30 14J ND ND W-18 2/3/1997 6,781 500 ND 820 930 960 ND ND ND ND ND ND ND 71 J ND ND 610 1,500 ND ND 930 460 ND ND 3/5/2009 9,932 60.0 3 741 396 17.4 <1.0 1,350 19.5 9.9 7.2 4.4 11.7 77.9 <1.0 4,050 <1.0 7.2 490 <1.0 13.5 1,850 819 3.8 ND W-20 1/31/1997 19.0 4 J ND 4 J 4 J ND ND ND ND ND ND ND ND ND ND ND ND 5 ND ND 2 J ND ND ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 15of15 �'71_ n v; Sample N N b o N N Sample I.D. �. �. b q b � 3 n n v 3 ,� �, vM. x Date 0 n 0 0 0 3- n c, m n a n _< S S 3- 3- =r p 3- O S S S S_ 3' 3 Q O O O O O O A y p O S O O K fD O O O 3 S C) 0 0 O' o o n W n rr ' ' a n ' 0 /� ♦/ N fD N a fD .. M O a O O M O 3 3 O 3 M O M O 3 S fOD a O_ fOD .. fOD .. 3- : C O S S S S S -a x .r N O N S O S S N O S C S S O O O 0 C) 3 D) 3 N 3 fD 3 a) 3 a) 3 D) 3 O 3 M 3 CL N 3 N 3 D) 3 N 3 M 3 a CD 3 M 3 N 3 M 3 3 a m 0 fp M CD M M N I N CD M M M M M M N I M CD CD M N M N U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 W-21 1/31/1997 1,232 340 ND 130 210 110 ND 240 J ND ND ND 18 J 3 J ND ND 3 J 47.0 ND ND 54.0 77.0 ND ND 9/28/2000 1,494 190 <5 120 140 74.0 <5 520 NA <5 <5 <10 <5 220 <5 <5 97.0 <5 <5 73.0 60.0 <10 ND 9/10/2001 1,336 129 <5 101 140 57.8 <5 407 <10 <5 <5 <10 <5 271 <5 <5 116 <5 <5 72.7 41.4 <5 ND 9/17/2002 1,775 127 <5 188 163 36.2 <5 458 <10 5.2 <5 <10 <5 498 <5 <5 102 <5 <5 98.0 100 <5 ND 9/17/2003 1,890 106 <5 140 151 44.6 <5 743 <10 <5 <5 <10 <5 384 <5 <5 140 <5 <5 105 76.7 <5 ND 8/17/2004 1,761 71.2 <10 114 124 47.4 <10 821 <20 <10 <10 <20 <10 333 <10 <10 95.2 <10 <10 81.5 73.5 <10 ND 9/24/2009 3,701 313 1.2 1 518 390 38.9 1 <1.0 678 16.0 12.6 <1.0 1 9.8 4.9 5.3 1 <1.0 1,210 1 <1.0 <1.0 108 <1.0 1 3.3 170 222 <2.0 ND W-23A 1/30/1997 4,600 ND ND ND ND ND ND ND 4,600 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 7/17/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3/4/2009 115 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 106 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.4 <1.0 <1.0 3.1 <1.0 <1.0 2.6 <1.0 <2.0 ND W-23B 1/22/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND W-24 1/31/1997 2,109 200 ND 190 330 ND ND ND ND ND ND ND ND 11 J ND ND 54 440 ND ND 710 160 14 J ND UP-2 (W-2 1/31/1997 1,921 180 ND 180 310 ND ND ND ND ND ND ND ND 10 J ND ND 49 400 ND ND 630 150 12 J ND 7/16/1998 1,943 ND 100 J 160 240 D ND ND ND ND 3 J ND ND ND 8 ND ND 12 520 D ND ND 690 D 190 20.0 ND W-25 8/7/1996 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1/27/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND W-29 2/5/1997 1,688,000 120,000 ND 7,400 J 29,000 580,000 ND ND 240,000 ND ND 49,000 ND ND ND ND 290,000 13,000 J 10,000 J ND 150,000 ND ND 230,000 BD-1 3/29/2010 235 <1.0 <1.0 14.7 <1.0 <1.0 <5.0 208 <5.0 <1.0 <1.0 1.74 2.28 <1.0 <1.0 5.72 <1.0 1.48 <1.0 <1.0 <1.0 <1.0 1.34 ND ND DUP-02 3/31/2010 148 <1.0 <1.0 31.0 1.60 3.45 <1.0 28.6 <5.0 <1.0 <1.0 35.4 9.90 <1.0 <1.0 24.1 <1.0 2.00 1.55 <1.0 <1.0 2.87 7.67 ND ND LCHT-COMP 3/30/2010 904 <2.0 <2.0 82.2 34.4 8.87 <2.0 416 32.4 8.00 <2.0 136 24.7 <2.0 <2.0 95.8 2.60 5.09 <2.0 6.24 <2.0 6.69 44.9 ND ND PW-SF1 4/2/2010 11,985 <2.0 <2.0 114 <2.0 <2.0 <2.0 8,410 247 20 <2.0 1,190 1,340 <2.0 <2.0 2.4 11 175 <2.0 447 4 <2.0 25 ND ND 11/3/2011 34,627 1,840 32.6 2,990 3,670 1,240 <5 1,300 57.2 32.5 <5 1,450 1,580 250 <5 13,100 <5 251 211 1,070 23.3 1,410 3,920 54.0 145.7 11/20/2012 8,577 136 <50 480 5.7 135 <50 4,310 <500 <50 <50 298 <50 <50 <50 2,230 <50 <50 <50 110 <50 123 749 <50 ND 12/9/2013 46,400 1,250 <50 3,700 6,190 1,060 <50 3,940 <500 <50 <50 1,710 1,130 276 19,900 <50 <50 <50 700 <50 1,470 4,920 <100 154 12/8/2014 43,302 1,100 <200 3,500 4,200 1,300 <200 3,510 <1000 <200 <200 2,000 1,200 200 <200 19,000 <200 <200 320 680 <200 1,700 4,500 <600 92 10/27/2015 41,479 1,100 <100 3,200 3,600 780 <100 3,550 <500 <100 <100 2,100 790 160 <100 18,000 <100 <100 420 800 <100 2,200 4,700 <300 79 J 11/17/2016 48,530 1,800 <500 4,400 4,900 780 <500 3,600 <10000 <500 <500 2,200 450 J 280 J <500 22,000 <500 <500 660 690 <500 2,800 4,700 <1500 ND 10/11/2017 43,254 1,300 <100 3,900 4,000 880 <100 3,600 <2000 <100 <100 1,900 340 180 <100 19,000 <100 <100 650 530 <100 2,900 4,000 43 J 74 10/30/2018 40,063 1,200 <100 3,400 3,600 660 <100 2,800 <2000 <100 <100 2,100 <100 110 <100 18,000 <100 <100 680 660 <100 3,100 3,600 45 J 63 J 9/10/2019 43,240 3,100 <200 3,500 4,100 600 <200 3,200 <4000 <200 <200 1,800 <200 120 <200 20,000 <200 160 830 530 <200 2,900 2,400 <600 ND 10/9/2020 42,870 130 J <200 6,400 4,300 <200 <200 2,400 <4000 <200 <200 1,900 970 <200 <200 14,000 <200 260 <200 640 <200 <200 12,000 <600 ND 10/27/2021 61,780 3,300 <500 6,200 5,300 <500 <500 2,300 <10000 <500 <500 2,100 <500 <500 <500 38,000 <500 260 J <500 720 <500 <500 3,200 <1500 400 EB-1 4/2/2010 19 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 1 15.5 <1.0 <1.0 I <1.0 <1.0 <1.0 I <1.0 <1.0 <1.0 3.15 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND FB-1 4/2/2010 25 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 21.4 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.55 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND Grutchfield (potable well 12/1/1998' ND <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA <2.0 <0.5 <0.5 <0.5 <2.0 <0.5 <2.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA <0.5 ND 3/11/2009 2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND ug/l = micrograms per liter Bold type indicates value exceeds NC 2L ground water standard J = Estimated value Values separated by slash 0 indicate split sample results ND = Not detected NA = Not Analyzed NC 2L Standard = North Carolina 2L ground water quality standard TABLE 3 Pege2 f4 SURFACE WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RFVERDALE DRIVE LANDFILL SITE Sample Date o 0 0 0 > a o ' - 'm o g o n m Descriptlon p 0 10 O _ _ y Y 10 u /I ue/I ue/I u /I u /I ue/I uq/I uq/I ue/I u /I ue/I ue/I u /I u /I u /I u /I u /I ue/I NC 213 Std. WS-I 2500 6700 330 0.38 3.1 2000 1.19 130 12 NE -JAL 330 2.6 0.7 11 140 2.5 0.025 670 20,000 Northam Intermittent $roam SW-1 4/30/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 11/2/2000 <5 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND 9/14/2001 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/02 Dry _ _ _. __ _ _ _ _ ND _ _ _ _. _ _ _ _ _ 9/16/2003 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/23/2004 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 Dry - - -- -- - - - - -- -- - - -- 8/29/2006 Dry 9/27/2007 Dry - - -- -- - - - - -- -- 5/13/2009 Dry 12/13/2013 Dry - - -- -- - - - - -- -- - - -- 12/8/2014 Dry 10/2212015 Dry - - -- -- - - - - -- -- - - -- 11/17/2016 Dry 2/1/2017 Dry - - -- -- - - - - -- -- - - -- 10/13/2017 Dry 11/29/2017 Dry - - -- -- - - - - -- -- - - -- 11/7/2018 <1 <1 <1 <1 12 <20 <l <1 <1 <l <1 <1 <l <1 <1 <1 <1 <3 <5 1/10/2019 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 9/18/2019 Dry 10/2212020 Dry 1012112021 Dry SW-2 4/30/1997 ND ND ND ND ND ND SJ 8 ND ND ND ND ND ND ND ND ND ND ND 7/15/1998 ND ND ND ND ND ND 6 12 ND ND ND ND ND ND ND ND ND ND ND 11/2/2000 <5 <5 <5 <5 420 NA <5 10 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND 9/14/2001 <5 <5 <5 <5 353 <10 <5 7.6 <l0 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 258 <10 <5 7.7 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA 293 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 <5 <5 <5 SOS <10 <5 9.6 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/16/2004 <5 <5 <5 <5 233 <10 <5 8.7 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 <5 <5 <5 <5 64 14.7 <5 6.2 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <1 <l <1 <1 218 <5 <1 9.1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND Spit(8270) 8/29/2006 NA NA NA NA 390 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/27/2007 <l <7 <7 <1 176 <5 <7 9.4 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND 5/13/2009 <1 <t <t ,1 17.1 7.1 <1 3.8 <1 <t <1 <1 <t <1 <1 <1 <1 <t <5 4/1/2010 <7.0 <l.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 11/3/2011 <0.5 <0.5 <0.5 <0.5 6.2 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 11/20/2012 Dry - - -- - - - - - -- -- - - -- -- -- -- -- - 12/13/2013 Dry - - -- - - - - - -- -- - - -- 12/8/2014 Dry - - -- - - p8i7u6 - - -- - - -- -- -- -- -- - 10/22/2015 Dry - - -- - - - - - -- -- - - -- 11/17/2016 Dry - - -- - - - - - -- - - -- -- -- -- -- - 2/1/2017 Dry - - -- - - - - - -- -- - - -- 10/13/2017 <1 <7 <l <1 <2 <20 <l <1 <1 <l <1 <1 <l <1 <1 <1 11 <3 <5 11/29/2017 Dry - - -- -- - - - - -- -- - - -- 11/7/2018 <1 <1 <1 <1 22 <20 <7 <1 <1 <7 <1 <1 <l <1 <1 <1 <1 <3 <5 1/10/2019 <1 <1 <1 <1 15 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 9/18/2019 Dry 10/22/2020 Dry 10/21'2021 Dry Southem mtarmlttant Sheam SW-3 4/30/1997 66 73 33 6 ND ND 3J ND 5J ND ND 110 4J 4J ND 2J 19 ND ND 7/15/1998 ND 5 ND ND NA ND ND ND ND ND 4J ND ND ND ND ND ND ND ND 11/2/2000 24 38 14 <5 6008 NA <5 <5 <70 ND 45 10 <5 <5 <5 <5 <10 <10 ND 9/14/2001 <5 <5 <5 <5 281 00 <5 <5 <70 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 14.6 5.1 <5 69.7 <10 <5 <5 <10 ND 17.0 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA 151 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/16/2003 13 42.4 16.8 <5 202 <10 <5 <5 <10 ND 50.4 7.2 <5 <5 <5 <5 <10 <5 <10 8/23/2004 <5 13.3 <5 <5 546 00 <5 8.7 16.4 ND 6.9 <5 <5 <5 <5 <5 <10 <5 <10 8/25/2004 <5 31.7 9 <5 115 <10 <5 <5 <10 ND 33.6 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 39.1 96.3 50 <5 26.3 <10 <5 <5 <10 ND 182 111 <5 <5 <5 <5 211.7 <5 <10 8/29/2006 11.8 59.3 24 3.5 327 <5 <t <1 3.2 ND 88.6 5.2 1.1 <1 <1 1.7 7.4 <2 ND 9/27/2007 Dry _ _ _. 5/13/2009 32.3 84.1 52.4 4.1 1" 10.2 2.5 1.4 10.5 <1 178 7.6 2.1 <1.0 <1.0 7.8 28.5 <1 <5 4/1/2010 21.7 52.6 36.6 <1.0 66.9 8.01 1.69 1.01 11.2 <1.0 127 51 1.32 <1.0 <1.0 5.58 23.7 ND <5.0 11/3/2011 20.6 37.3 24 1.58 38 <5 <0.5 <0.5 19.9 <0.5 76.5 4.79 <0.5 <0.5 <0.5 10.6 25 <0.5 <5 11/20/2012 27.1 50.7 29.3 <0.5 115 <5 <0.5 0.62 19 <0.5 105 1.31 2.62 <0.5 0.58 14 23.2 <0.5 <5 12/11/2013 28.7 26.6 33.2 0.74 10 <5 1.83 0.73 10.4 <0.5 85.1 <0.5 1A <0.5 0.75 14.6 18.8 <0.5 <5 12/8/2014 8.2 22 10 <1 96.8 <5 <l <1 8.8 <7 42 15 1.2 <1 <1 4.8 11 <3 <5 10/22/2015 27 81 37 2.7 104 <5 0.88 J <1 24 <1 140 81 4.8 <1 0.87 J 19 28 <3 <5 11/17,2016 <7 <l <1 <1 16 28 J <1 <1 <1 <l 0.44 J <1 <l <1 <1 <1 <1 <3 <5 2/1/2017 NA NA NA NA 12 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 10/1312017 <7 <l <1 <1 9.7 J <20 <l <1 <1 <1 <1 <1 <l <1 <1 <1 <1 <3 <5 11/29/2017 NA NA NA NA 15 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 11/7/2018 <1 1.2 <1 <1 13 <20 <1 <1 <1 <1 2.3 <1 <1 <1 <1 <1 <1 <3 <5 9/18/2019 <i <t <t <1 1.7 <20 <t <1 <1 <t <1 <1 <t <1 <1 <1 <1 <3 <t 10/22/2020 <7 0.89 J <l <1 3.9 <20 <1 <1 <1 1.6 <1 <1 <1 <1 <1 <1 <2 <7 10/21/2021 0.951 2.1 <t <1 4.6 <20 <t <1 <1 2.6 <1 <t <1 <1 <1 <1 <2 <t SW-4 4/30/1997 4J/5J 30/34 3J/3J 3J/4J ND/ND 12J/23J 1J/1J 62/69 15J/16J ND NDMD 10111 ND/ND NDMD NDMD NDMD 8J/9J ND/ND ND/ND 7/20/1998 ND 16 ND 4J NA ND ND 77 36 ND ND ND ND ND ND ND ND ND ND 11/2/2000 <5 <5 <5 <5 1100 NA <5 48 34 ND <5 <5 <5 <5 <5 <5 <10 <10 ND 9/14/2001 <5 <5 <5 <5 806 <10 <5 16.5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 480 <70 <5 19.3 <70 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA 448 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 7.7 <5 <5 118 11 <5 12.2 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/25/2004 <5 <5 <5 <5 592 <10 <5 38.0 18.2 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 6.4 24.9 7.3 <5 172 17.3 <5 22.4 <10 ND 36.5 5.8 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <1 1.2 <1 <1 1040 <5 <1 9.5 8.1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND Split (8270) 8/29/2006 NA NA NA NA 1200 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/27/2007 <1 <1 <1 <1 24.1 <5 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND 5/13/2009 <1 <l <l <1 8A 8.4 <l <1 <1 1.7 <1 <1 <l <1 <1 <1 <1 <7 <5 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 11/3/2011 72 443 126 32.6 110 10.6 14.2 358 141 <0.5 440 1.21 3.24 0.74 <0.5 13.5 371 4.93 <5 11/20/2012 <0.5 2.1 <0.5 <0.5 22.7 <5 <0.5 5.9 <0.5 <0.5 1.56 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 12/13/2013 <0.5 <0.5 <0.5 <0.5 Q.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 12/8/2014 <1 <1 <1 <1 3.3 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 10/22/2015 <7 <7 <7 <1 4.1 J <5 <1 0.82 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 11/21/2016 <i <t <t <1 18 <10 <t 1.3 J 0.70 J <t <1 <1 <t <1 <1 <1 <1 <3 <5 2/1/2017 NA NA NA NA Q.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 10/13/2017 86 710 280 63 1700 <200 20 840 120 <10 1100 <10 6.7 J 4.8 J 4.3 J 4.1 J 1000 9.1 <50 11129,2017 120 770 370 58 1500 <200 24 950 65 <10 1400 <10 15 6.7 4.1 22 970 14 <50 11/7/2018 <1 25 13 2.5 48 <20 <1 23 2.4 <1 40 <1 <1 <1 <1 <1 45 <3 <5 9/18/2019 51 400 120 34 1800 <200 <10 820 250 <10 540 <10 4A 4.9 J 7.1 J <1 420 7.7 J <50 10/22/2020 7.7 52 27 4.7 79 <20 0.41 J 6 6.6 <1 100 <1 1 <1 <1 <1 73 0.47 J <5 10/21/2021 170 1100 670 120 1500 QO 0.41 J 1700 100 <1 3300 <1 16 11 <1 <1 1500 <7 <5 TABLE 3 P^gee f4 SURFACE WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RI VERDALE DRIVE LANDFILL SITE Sample Date o 0 0 0 > a o ' - 'm o g o n m Descriptlon p n 0 m 0 u /I un/I un/I u /I u /I un/I un/I un/I un/I u /I ti /I _ un/I un/I u /I u /I u /I _ u /I u /I un/I NC 2B Std. WS-I 2500 6700 330 0.38 3.1 2000 1.19 130 12 NE 330 2.6 0.7 11 140 2.5 0.025 670 20,000 SW-5 4/30/1997 ND ND ND ND ND 81 ND ND ND ND ND ND ND ND ND ND ND ND ND 11/2/2000 <5 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 c5 <5 <5 <10 <10 ND 9/14/2001 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 <10 <70 <5 <5 <70 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/16/2003 <5 <5 <5 <5 12A <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/25/2004 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <1 <1 <1 <1 <2 51.7 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND 9/27/2007 <1 <1 <7 <1 <2 <5 <7 <1 <1 ND <1 <1 <7 <1 <1 <1 <1 <2 ND 5/13/2009 8.7 8.6 6.4 <1 25A 5.3 <7 <1 <1 <7 39.4 <1 3.3 <1 <1 9.0 8.2 <1 <5 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 11/3/2011 <0.5 <0.5 <0.5 <0.5 <3.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 11/20/2012 <0.5 <0.5 <0.5 <0.5 6.97 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 12/16/2013 <0.5 <0.5 <0.5 <0.5 13.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 12/8/2014 <1 <1 <1 <1 2.26 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 10/22/2015 <1 <7 <7 <1 1.8 J <5 <7 <1 <1 <7 <1 <1 <7 <1 <1 <1 <1 <3 <5 11/17/2016 <1 <1 <1 <1 3.1J <10 <7 <1 <1 <7 <1 <1 <1 <1 <1 <1 <1 <3 <5 2/1/2017 NA NA NA NA 8.3 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 10/13/2017 <1 <1 <1 <1 14.0 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 11/29/2017 NA NA NA NA 8.6 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 11/7/2018 <1 <7 <7 <1 23.0 <20 <1 <1 <1 <7 <1 <1 <7 <1 <1 <1 <1 <3 <5 9/18/2019 <1 <7 <7 <1 5.8 <20 <1 <1 <1 <1 0.63 J <1 <7 <1 <1 <1 0.46 J <3 <5 10/22/2020 <1 <1 <1 <1 3.5 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 10/21/2021 0 0 0 <1 2.2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Randleman Laker -I ma owp RIwI SW-6 5/1/1997 ND ND ND ND ND 6J ND ND ND ND ND ND ND ND ND ND ND ND ND 11/2/2000 <5 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND 9/14/2001 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 11.5 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/16/2003 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/25/2004 <5 <5 <5 <5 133 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 <5 <5 <5 <5 11.4 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <7 <7 <7 <1 Q <5 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND Spit(8270) 8/29/2006 NA NA NA NA <3.3 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/27/2007 <1 <1 <1 <1 <2 <5 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND Upper 2/25/2009 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND Mid 2/25/2009 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND Mid 5/13/2009 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5 Upper 5/13/2009 <1.0 <1.0 <1.0 <1.0 <2.0 8.1 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.1 <1.0 <1.0 <1.0 <5 Surface 4/1/2010 <7.0 <7.0 <7.0 <1.0 <2.0 <5.0 <7.0 <1.0 <1.0 <7.0 <1.0 <1.0 <7.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Bottom 4/1/2010 <1.0 <1.0 <1.0 <00 4.02 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Surface 11/3/2011 <0.5 <0.5 <0.5 <0.5 <3.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Surface 11/21/2012 <0.5 <0.5 <0.5 <0.5 3.73 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Bottom 11/21/2012 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Surface 12/1312013 <0.5 <0.5 <0.5 <0.5 9.29 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Bottom 1113/2013 <0.5 <0.5 <0.5 <0.5 <2.90 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Surface 12/15/2014 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 12/15/2014 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 10/22/2015 <i <1 <1 <1 <2 <5 <1 <1 <1 <i <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 10/22/2015 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 11/21/2016 <i <i <i <1 <2 <10 <i <1 <1 <i <1 <1 <i <1 <1 <1 <1 <3 <5 Bottom 11/21/2016 <1 <1 <1 <1 <2 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 2/1/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 2/1/2017 NA NA NA NA Q NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 10/1312017 <i <t <t <1 13.0 <20 <t <1 <1 <i <1 <1 <t <1 <1 <1 <1 <3 <5 Bottom 10/13/2017 <7 <7 <7 <1 14.0 <20 <7 <1 <1 <7 <1 <1 <7 <1 <1 <1 <1 <3 <5 Surface 11/29/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 11/29/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 11/7/2018 <i <t <t <1 <2 <20 <t <1 <1 <t <1 <1 <t <1 <1 <1 <1 <3 <5 Bottom 11/7/2018 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 9/18/2019 <i <t <t <1 1.6J <20 <t <1 <1 <t <1 <1 <t <1 <1 <1 <1 <3 <5 Bottom 9/18/2019 <7 <7 <7 <1 <2 <20 <7 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 10/22/2020 <i <t <t <1 <2 <20 <t <1 <1 <t <1 <1 <t <1 <1 <1 <1 <2 <5 Bottom 10/22/2020 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Surface 10/21/2021 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Bottom 10/21/2021 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 SW-7 5/2/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 11/3/2000 <5 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND 9/13/2001 <5 <5 <5 <5 40.5 <10 <5 <5 23 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/23/2004 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 <5 <5 <5 <5 <10 10.7 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <1 <1 <1 <1 4.3 <5 <1 2 <1 ND <1 <1 <1 <1 <1 <1 <1 Q ND 9-27-200 <1 <1 <1 <1 23.2 5.0 <1 2 <1 ND <1 <1 <1 <1 <1 <1 <1 Q ND Upper 2/25/2009 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND Mid 2/25/2009 <7.0 <7.0 <7.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 ND <1.0 <1.0 <7.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND Mid 5/13/2009 <1.0 <1.0 <1.0 <1.0 <2.0 5.3 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5 Upper 5/13/2009 <7.0 <7.0 <7.0 <1.0 <2.0 7.0 <7.0 <1.0 <1.0 <7.0 <1.0 <1.0 <7.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5 Surface 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Bottom 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Surface 11/3/2011 <0.5 <0.5 <0.5 <0.5 <3.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Surface 11/21/2012 <0.5 <0.5 0.88 <0.5 9.10 <5 <0.5 1.11 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Bottom 11/21/2012 <0.5 <0.5 <0.5 <0.5 8.88 <5 <0.5 0.94 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Surface 12/13/2013 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Bottom 12/13/2013 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Surface 12/15/2014 <7 <7 <1 <1 2.38 <5 <1 1.3 <1 <1 0.42 J <1 <1 <1 <1 <1 <1 <3 <5 Bottom 12/15/2014 <1 <1 <t <1 <2 <5 <t 1.3 <1 <t <1 <1 <t <1 <1 <1 <1 <3 <5 Surface 10/22/2015 <7 <7 <7 <1 1.43J <5 <7 <1 <1 <1 <1 <1 <7 <1 <1 <1 <1 <3 <5 Bottom 10/2212015 <1 <1 <1 <1 1.10 J <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 11/21/2016 <1 <1 <7 <1 27 <10 <1 <1 <1 <1 <1 <1 <7 <1 <1 <1 <1 <3 <5 Bottom 11/21/2016 <1 <1 <1 <1 28 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 12/28/2016 NA NA NA NA 10 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 2/1/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 2/1/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 10/1312017 <t <t <t <1 26.0 <20 <t <1 <1 <i <1 <1 <t <1 <1 <1 <1 <3 <5 Bottom 10/13/2017 <7 <1 <1 <1 20.0 <20 <7 <1 <1 <7 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 11/2912017 NA NA NA NA 8.9 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 11/29/2017 NA NA NA NA 9.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 11/7/2018 <i <t <t <1 <2 <20 <t <1 <1 <t <1 <1 <t <1 <1 <1 <1 <3 <5 Bottom 11/7/2018 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 9/18/2019 <i <t <t <1 <2 <20 <t <1 <1 <t <1 <1 <t <1 <1 <1 <1 <3 <5 Bottom 9/18/2019 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 10/22/2020 <i <1 <t <1 <2 <20 <t <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Bottom 10/22/2020 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Surface 10,2112021 <1 <1 <1 <1 <2 <20 <1 <1 <1 <t <1 <1 <t <1 <1 <1 <1 <2 <5 Bottom 10/21/2021 <1 <1 11 <1 12 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 TABLE 3 Pege3 F4 SURFACE WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RI VERDALE DRIVE LANDFILL SITE Sample Sample Date 2: o E 0 E 0 0 > a o ' - 'm o g o n m Descriptlon p N 0 m 0 u /I ue/I ue/I u /I u /I ue/I uq/I uq/I ue/I u /I ti /I _ ju/I ue/I u /I u /I u /I _ u /I(!!2/1) u /I ue/I NC 2B Std. WS-I 2500 6700 330 0.38 3.1 2000 1.19 130 12 NE 330 2.6 0.7 11 140 2.5 0.025 670 20,000 SW-DRP-2 11/3/2000 <5 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND EAST 9/14/2001 <5 6.3 <5 <5 15.3 <10 <5 5.8 <10 ND 5.7 <5 <5 <5 <5 <5 <10 <5 ND WEST 9/14/2001 <5 29.5 <5 <5 42.8 <10 <5 61.5 30.5 ND 26.4 <5 <5 <5 <5 <5 21.7 <5 ND 9/24/2002 6.6 47.0 11.8 <5 39.2 <10 <5 62.3 20.5 ND 60.3 <5 <5 <5 <5 <5 28.1 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/23/2004 <5 <5 7.1 <5 145 <10 5.4 189 48.6 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 14.2 80.3 33.8 <5 82.1 <10 <5 66.4 17.7 ND 140 <5 <5 <5 <5 <5 36.1 <5 <10 8/29/2006 <7 2 <7 <1 <2 <5 <7 <1 <1 ND 3.1 <1 <7 <1 <1 <1 <1 <2 ND Spit(8270) 8/29/2006 NA NA NA NA <3 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/27/2007 <1 <1 <1 <1 23.3 <5 <1 2 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND Upper 2/25/2009 <1.0 <1.0 3.0 1.9 <2.0 8.0 <1.0 1.4 <1.0 ND 7.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND Mid 2/25/2009 <1.0 <1.0 <1.0 <1.0 <2.0 9.2 <1.0 <1.0 <1.0 ND <1.0 <1.0 <1.0 1.4 <1.0 <1.0 <1.0 <2.0 ND Mid 5/13/2009 <1.0 <1.0 <1.0 <1.0 <2.0 8.6 <7.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Q.0 <5 Upper 5/13/2009 <1.0 <1.0 <1.0 <1.0 <2.0 6.9 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5 Surface 4/1/2010 <7.0 <7.0 <7.0 <1.0 <2.0 <5.0 <7.0 <1.0 <1.0 :1.0 <1.l) <1.0 :1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Bottom 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Surface 11/21/2012 <0.5 <0.5 <0.5 <0.5 7.27 <5 <0.5 2.75 <0.5 <0.5 1.19 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Bottom 11/21/2012 <0.5 1.86 1.4 <0.5 11A <5 <0.5 6.26 6.36 <0.5 2.26 <0.5 <0.5 <0.5 <0.5 <0.5 2.54 <0.5 <0.5 Surface 12/13/2013 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Bottom 12/13/2013 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Surface 12/15/2014 <1 <1 <1 <1 1.2 J <5 <1 <1 <1 <7 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 12/15/2014 <1 <1 <t <1 1.62 J <5 <t <1 <1 <1 <1 <1 <t <1 <1 <1 <1 <3 <5 Surface 10/22/2015 <7 <7 <7 <1 3.02 J <5 0 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 10/2212015 <i <t <t <1 3.11 J <5 <1 0.47 J <1 <1 <1 <1 <t <1 <1 <1 <1 <3 <5 Surface 11/21/2016 <1 <1 <1 <1 18 <10 <7 1.3 J 0.59 J <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 11/21/2016 <i <t <t <1 18 <10 <t 1.3J <1 <i <1 <1 <t <1 <1 <1 <1 <3 <5 Bottom 12/28/2016 NA NA NA NA 7.2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 2/1/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 2/1/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 10/1312017 <t <t <t <1 19.0 <20 <t <1 <1 <i <1 <1 <t <1 <1 <1 <1 <3 <5 Bottom 10/13/2017 <7 <7 <7 <1 21.0 <20 <1 0.53 J <1 <7 <1 <1 <7 <1 <1 <1 <1 <3 <5 Surface 11/29/2017 NA NA NA NA 3A NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 11/29/2017 NA NA NA NA 3A NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 11/7/2018 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 11/7/2018 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 9/18/2019 <1 <t <t <1 1.4J <20 <t <1 <1 <1 <1 <1 <t <1 <1 <1 <1 <3 <5 Bottom 9/8/2019 <7 <7 <7 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 10/22/2020 <i <t <t <1 0.83 J <20 <t <1 <1 <t <1 <1 <1 <1 <1 <1 <1 <2 <5 Bottom 10/22/2020 <1 <1 <7 <1 <2 <20 <7 <1 <1 <7 <1 <1 <7 <1 <1 <1 <1 <2 <5 Surface 10/21/2021 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Bottom 10121 0121/2021 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 SW-DRPA 11/2/2000 <5 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND EAST 9/14/2001 <5 9.1 <5 <5 44 <10 <5 101 51.5 ND 8 <5 <5 <5 <5 <5 <10 <5 ND WEST 9/14/2001 <5 8.5 <5 <5 30.2 <10 <5 69.4 33.3 ND 7.4 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/24/2004 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2 06 <1 <1 <1 <1 Q <5 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND 9/27/2007 <7 <7 <7 <1 24.9 <5 <1 <1 <1 ND <1 <1 <7 <1 <1 <1 <1 Q ND SW-DRP-10 11/2/2000 <5 7.5 <5 <5 <100 NA <5 14 17 ND 5.7 <5 <5 <5 <5 <5 <10 <10 ND EAST 9/13/2001 <5 6 <5 <5 43.8 00 <5 14.4 27.7 ND <5 <5 <5 <5 <5 <5 <10 <5 ND WEST 9/13/2001 <5 6.3 <5 <5 43.5 <10 <5 19.2 30.9 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 12.6 <70 <5 7.2 7.5 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/23/2004 <5 <5 <5 <5 12 <10 <5 9.1 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 <5 <5 <5 <5 <10 <70 <5 <10 <70 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <1 <1 <1 <1 4.1 <5 <1 2.9 1.1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND 9/27/2007 <1 <7 <7 <1 22A <5 <7 <1 <1 ND <1 <1 <7 <1 <1 <1 <1 Q ND TABLE 3 SURFACE WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RI VERDALE DRIVE LANDFILL SITE rage s of 4 Deacrlptlon Sample Date o n 0 ugn 0 u n 0 n > p un 0 jun uqn a uqn o ugn ' uen - !!%n 'm O _ juaill o jusa _0 n g urn o jun _ _ n n y n m Y 0 ugn NC 2B Std. S4 2500 6700 330 0.38 3.1 2000 1.19 130 12 NE 330 2.6 0.7 11 140 2.5 0.025 670 20,000 SW-DRP-11 11/2/2000 <5 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND 9/13/2001 <5 <5 <5 <5 10.2 <10 <5 <5 <70 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 109 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 50n UPS-11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 <5 <5 <5 53.5 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/23/2004 <5 <5 <5 <5 20A <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <1 <1 <1 <1 3.5 5.2 <1 1.1 <1 ND <1 <1 <1 <1 <1 <1 <1 Q ND 9/27/2007 <l <l <1 <1 17.9 <5 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 Q ND Upper 2/25/2009 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND Mld 2/25/2009 <7.0 <7.0 <7.0 <1.0 <2.0 <5.0 <7.0 <1.0 <1.0 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND Mid 5/13/2009 <1.0 <1.0 <1.0 <1.0 <2.0 10.4 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5 Upper 5/13/2009 <7.0 <7.0 <7.0 <1.0 <2.0 <5 <7.0 <1.0 <1.0 <7.0 <1.0 <1.0 <7.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5 Surface 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Bottom 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <7.0 <1.0 <1.0 <7.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Surface 11/21/2012 <0.5 <0.5 <0.5 <0.5 10.2 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Bottom 11/21/2012 <0.5 <0.5 <0.5 <0.5 9.93 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Surface 12/16/2013 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Bottom 12/16/2013 <0.5 <0.5 <0.5 <0.5 14.4 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Surface 51014 <1 <1 <1 <1 1.55J <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom Ill 1115/2014 <1 <1 <1 <1 1.53 J <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 10/22/2015 <1 <1 <t <1 <2 <5 <t <1 <1 <t <1 <1 <t <1 <1 <1 <1 <3 <5 Bottom 10/22/2015 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 11/21/2016 <1 <t <t <1 19 <10 <t <1 <1 <1 <1 <1 <t <1 <1 <1 <1 <3 <5 Bottom 11/21/2016 <1 <1 <1 <1 17 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 2/1/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 2/1/2017 NA NA NA NA 1.4J NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 10/1312017 <1 <t <t <1 31.0 <20 <t <1 <1 <1 <1 <1 <t <1 <1 <1 <1 <3 <5 Bottom 10/13/2017 <1 <1 <1 <1 31.0 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 11/2912017 NA NA NA NA 20.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 11/29/2017 NA NA NA NA 20.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 11/7/2018 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 11/7/2018 <7 <7 <7 <1 <2 < 0 <7 <1 <1 <7 <1 <1 <7 <1 <1 <1 <1 <3 <5 Surface 9/18/2019 <1 <t <t <1 1.3 J <20 <t <1 <1 <t <1 <1 <t <1 <1 <1 <1 <3 <5 Bottom 9/18/2019 <7 <7 <7 <1 <2 <20 <7 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 10/22/2020 <1 <t <t <1 <2 <20 <t <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Bottom 10/22/2020 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <5 Surface 10/2112021 <1 <1 <t <1 1.4 J <20 <t <1 <1 <t <1 <1 <t <1 <1 <1 <1 <2 <5 Bottom 1012112 021 <7 <7 <7 <1 1.2 J <20 <7 <1 <1 <7 <1 <1 <7 <1 <1 <1 <1 <2 <5 - J=Estimated value NE =Not Established B = Analyte detected in method blank as well as sample NA = Not Analyzed Bold type indicates value exceeds NC 213 surface water quality ston&,d(WS-IV) NC 2B Std. (4VS-IV)= North Carolina 213 surface water quality standardfor Class WS-IV waters Values separated by slash 0 indicates split sample results TABLE 4 Page 1 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification Ground Water = MRF-1 2/24/2009 17.0 6.1 900 MW-1 3/5/2009 14.8 3.9 194 3/31/2010 16.5 6.6 2840 11/2/2011 14.2 8.2 9.7 228 11/20/2012 13.6 9.4 3.5 458 12/9/2013 13.5 12.0 3.6 3 12/8/2014 12.1 7.8 4.6 352 10/26/2015 13.7 8.0 3.5 0 11/14/2016 14.5 7.3 3.4 287 10/11/2017 19.9 7.2 4.7 262 11/1/2018 17.8 8.1 10.5 324 9/10/2019 22.8 6.6 585 10/13/2020 19.7 7.4 196 10/26/2021 15.7 5.7 1.3 337 MW-2C 2/24/2009 14.4 6.6 688 MW-313 9/26/2000 15.7 6.2 2000 9/5/2001 17.8 6.4 1930 MW-3C 9/26/2000 15.4 6.3 1520 9/5/2001 17.6 6.5 1570 9/18/2002 16.9 6.8 1820 8/17/2004 18.2 6.6 1461 2/27/2009 15.7 6.4 686 3/30/2010 17.5 7.7 2370 11/1/2011 16.4 7.8 8.3 971 11/20/2012 14.8 7.9 2.9 648 12/11/2013 11.1 6.9 19.5 4 12/11/2014 15.7 6.7 4.4 1915 10/27/2015 15.3 6.5 1.9 1284 11/14/2016 17.2 7.3 2.7 1221 10/10/2017 23.9 6.2 4.2 1096 11/2/2018 17.3 6.8 3.3 1123 9/11/2019 31.1 6.5 1555 10/13/2020 18.1 6.4 665 10/26/2021 16.6 5.5 1.2 1042 MW-5 2/24/2009 10.5 5.2 544 MW-6 9/26/2000 15.3 6.0 559 9/6/2001 17.5 6.2 472 9/19/2002 18.1 6.5 538 8/18/2004 -- -- -- 3/3/2009 14.6 7.5 900 3/30/2010 17.4 6.9 2730 11/1/2011 17.6 8.9 7.3 40 11/19/2012 20.6 7.3 2.9 1036 12/11/2013 11.3 6.5 11.7 113 12/12/2014 14.7 6.6 3.2 1163 10/30/2015 16.0 7.1 1.3 719 11/17/2016 20.1 6.5 1.7 751 10/10/2017 22.0 7.6 3.6 692 11/2/2018 19.5 6.6 4.6 993 9/12/2019 26.7 6.9 1245 10/14/2020 19.7 6.2 579 10/28/2021 19.2 6.4 0.3 955 MW-713 3/3/2009 16.2 5.9 4220 MW-8 3/5/2009 16.9 5.1 990 MW-9 9/26/2000 14.9 5.8 1.17 2/26/2009 12.4 8.0 1840 MW-10 9/26/2000 15.4 6.3 2.51 9/6/2001 16.0 6.3 2480 9/19/2002 16.1 6.7 2740 9/16/2003 17.0 6.7 1940 8/17/2004 16.0 6.4 2200 3/6/2009 14.9 6.2 932 3/29/2010 16.6 8.8 4510 11/1/2011 16.9 7.1 9.4 1058 11/19/2012 15.8 7.4 2.0 154 12/10/2013 12.8 6.5 7.9 302 12/10/2014 13.1 6.5 4.1 257 10/26/2015 15.9 7.0 1.8 1523 11/14/2016 16.6 6.7 2.3 1194 10/10/2017 20.2 6.0 3.9 905 10/31/2018 17.6 6.8 3.6 1591 9/10/2019 24.5 6.2 31 10/12/2020 19.1 6.4 307 10/26/2021 18.7 4.6 0.9 355 TABLE 4 Page 2 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification MW-11 9/28/2000 17.2 6.5 5950 9/10/2001 17.3 6.7 5860 9/18/2002 16.5 7.0 5350 8/17/2004 -- -- -- 3/4/2009 14.0 6.8 2990 MW-12A 9/28/2000 17.9 6.2 747 10/30/2000 17.7 6.4 899 9/6/2001 18.7 6.5 506 9/20/2002 18.8 6.4 766 9/16/2003 21.3 6.6 521 8/18/2004 23.0 7.0 425 3/6/2009 12.1 5.0 150 4/1/2010 17.0 7.4 6660 11/2/2011 10.9 9.6 1.1 1601 11/19/2012 15.8 7.7 2.8 539 12/10/2013 12.3 6.8 7.7 317 12/11/2014 14.1 6.8 4.6 564 10/27/2015 14.7 6.8 1.6 1948 11/14/2016 16.4 7.5 3.1 1530 10/10/2017 22.2 6.4 4.4 1558 11/1/2018 18.2 6.1 1.7 1720 9/10/2019 26.7 6.5 1500 10/13/2020 19.5 6.5 1180 10/26/2021 18.6 5.9 0.8 1856 MW-12B 9/28/2000 16.9 6.2 2620 9/6/2001 17.7 6.4 2570 9/20/2002 18.1 6.3 2930 9/16/2003 18.3 6.7 2500 8/18/2004 -- -- -- 3/4/2009 11.9 7.8 2990 4/9/2010 16.6 6.2 412 11/2/2011 16.4 9.0 2.7 1418 11/19/2012 15.0 7.4 2.8 39 12/10/2013 14.8 6.4 18.5 295 12/11/2014 14.3 6.5 3.5 868 10/27/2015 14.0 6.5 1.7 1475 11/14/2016 15.3 6.6 2.9 1682 10/10/2017 22.4 6.5 3.5 1699 11/1/2018 22.1 6.7 7.8 990 9/11/2019 25.0 6.5 1695 10/13/2020 18.9 6.5 1230 10/26/2021 17.4 5.6 0.7 1965 MW-12D 9/29/2000 15.8 6.8 1110 9/12/2001 16.2 7.8 949 9/20/2002 19.5 7.6 520 3/5/2009 13.4 11.9 208 4/1/2010 19.6 9.6 91100 11/2/2011 11.2 8.4 11.5 293 11/23/2012 18.0 9.1 1.9 27 12/11/2013 12.8 7.9 18.8 379 12/11/2014 17.3 7.7 6.0 609 10/25/2015 19.3 6.7 1.8 1210 11/18/2016 14.8 8.3 3.7 358 10/11/2017 20.5 7.3 6.2 382 11/1/2018 22.2 8.7 4.7 412 9/12/2019 21.0 7.1 275 10/13/2020 18.8 7.7 113 10/26/2021 17.7 6.3 0.6 279 MW-15A 9/5/2001 17.5 6.3 942 9/18/2002 15.8 6.7 1150 9/17/2003 15.8 5.9 932 8/18/2004 -- -- -- 3/6/2009 15.1 6.3 427 3/31/2010 17.7 7.7 4940 11/2/2011 14.7 7.8 7.8 265 11/19/2012 14.8 7.6 2.7 237 12/10/2013 14.9 6.1 6.9 873 12/8/2014 11.6 6.6 4.9 768 10/27/2015 14.7 6.6 1.8 478 11/14/2016 14.1 6.6 2.8 760 10/11/2017 22.9 6.6 4.7 739 10/31/2018 16.3 6.8 11.2 246 9/10/2019 24.8 6.6 1515 10/9/2020 17.9 6.3 289 10/28/2021 15.7 7.1 0.5 508 MW-16 MW-17 3/5/2009 18.7 10.0 357 OW-DR1 9/27/2000 19.0 6.3 2120 TABLE 4 Page 3 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification OW-DR2 9/26/2000 16.0 6.3 1850 9/10/2001 15.6 6.5 1900 2/27/2009 16.2 9.9 1760 3/30/2010 17.1 8.2 4960 11/1/2011 17.0 8.4 6.3 1060 11/23/2012 14.7 7.7 1.9 789 12/11/2013 13.2 8.4 2.9 837 12/12/2014 14.4 7.0 3.1 1918 10/30/2015 12.7 9.7 0.9 1388 11/18/2016 17.0 6.9 1.0 987 10/10/2017 20.6 6.4 3.3 1500 11/2/2018 17.1 7.6 0.8 1600 9/11/2019 23.3 7.6 900 10/13/2020 18.1 7.2 372 10/28/2021 16.2 7.5 0.3 627 OW-DR3 9/20/2002 16.7 6.3 2520 8/24/2004 17.6 6.7 643 3/4/2009 12.7 3.7 2460 11/26/2012 17.5 6.1 2.5 1713 12/10/2013 13.7 6.3 4.1 254 OW-DR4 9/23/2002 17.9 6.6 1720 8/24/2004 17.5 6.3 1288 2/25/2009 17.5 6.2 762 OW-LFS1 2/26/2009 15.2 6.0 3730 OW-LFS2 2/26/2009 14.5 5.4 3100 3/30/2010 17.3 8.2 9990 11/1/2011 16.9 7.7 6.2 141 11/19/2012 17.4 7.6 2.7 367 12/11/2013 12.2 6.4 8.4 668 12/12/2014 14.7 6.5 4.6 1722 10/26/2015 16.2 6.6 2.2 1302 11/14/2016 18.9 6.5 2.5 2036 10/10/2017 21.6 6.5 4.5 2093 10/31/2018 17.9 6.6 9.5 1403 9/12/2019 20.2 6.7 830 10/12/2020 20.4 6.5 1440 10/28/2021 17.2 6.5 0.3 2827 OW-NIS1 3/10/2009 20.3 4.4 2650 OW-SF1 3/9/2009 18.0 3.8 802 OW-SIS1 8/17/2004 16.2 5.8 656.4 3/9/2009 18.0 4.2 579 OW-SIS2 2/24/2009 16.0 6.1 155 OW-SIS3 3/4/2009 13.6 6.0 392 PW-2D 3/3/2009 15.2 7.8 1930 PW-3D 11/27/2012 9.3 10.0 5.0 375 12/17/2013 8.6 12.7 18.7 128 12/11/2014 14.1 8.6 1.8 572 10/25/2015 18.8 6.3 0.6 397 11/16/2016 18.1 8.5 3.7 358 10/11/2017 21.4 7.5 1.7 377 11/2/2018 19.1 7.5 1.5 457 9/11/2019 23.6 8.0 762 10/27/2021 17.0 6.9 0.4 461 PW-41 9/28/2000 21.8 6.3 2010 9/11/2001 19.7 6.4 1710 9/19/2002 20.8 6.5 1890 8/23/2004 20.4 3.1 1719 3/5/2009 17.5 4.4 2160 4/2/2010 16.6 7.6 1860 11/2/2011 24.4 8.0 0.2 1017 11/20/2012 18.9 7.2 2.0 920 12/17/2013 12.1 6.7 19.6 807 12/8/2014 13.9 6.3 1.5 1516 10/29/2015 20.5 6.8 0.8 1675 11/17/2016 21.1 6.0 1.6 1399 10/11/2017 22.7 6.4 1.5 857 11/2/2018 21.5 6.5 1.9 1686 9/11/2019 24.2 6.4 1857 10/14/2020 21.6 6.2 1120 10/27/2021 18.3 6.9 0.3 1944 TABLE 4 Page 4 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification PW-5D 9/26/2000 15.8 6.4 1620 9/10/2001 16.0 6.7 1590 9/23/2002 16.3 6.8 1610 8/18/2004 16.5 6.4 1293 3/27/2009 16.3 6.3 797 3/30/2010 17.2 8.4 1690 11/3/2011 17.3 8.4 8.3 1044 11/23/2012 15.8 8.2 1.9 790 12/16/2013 10.4 6.8 18.3 995 12/11/2014 14.9 7.0 2.8 1609 10/30/2015 15.8 7.8 1.3 955 11/18/2016 15.3 6.9 1.1 927 10/10/2017 20.3 6.8 2.4 1335 11/2/2018 17.6 7.8 2.9 1658 9/11/2019 25.6 7.6 920 10/13/2020 18.0 7.4 455 10/28/2021 16.5 7.5 0.4 757 PW-6D 10/2/2000 16.5 7.7 320 9/12/2001 15.4 8.0 472 9/19/2002 15.9 8.1 356 8/25/2004 15.7 7.9 276 3/18/2009 16.7 7.3 363 3/31/2010 17.4 7.4 408 New Well 12/10/2014 13.1 8.2 4.6 564 10/30/2015 20.5 8.2 1.2 263 11/17/2016 17.6 7.7 1.4 410 10/10/2017 19.0 7.3 4.3 1100 11/1/2018 16.6 7.6 7.1 918 9/12/2019 25.2 7.5 904 10/12/2020 17.9 8.0 241 10/28/2021 15.9 6.1 0.4 780 PW-61 10/2/2000 15.9 6.2 573 9/12/2001 14.5 6.2 816 9/19/2002 15.3 6.3 631 8/25/2004 15.1 6.3 544 3/4/2009 13.5 6.2 404 3/31/2010 17.9 6.0 1020 New Well 12/10/2014 11.0 7.6 3.5 1521 10/27/2015 14.7 6.7 1.5 1201 11/17/2016 14.6 6.8 1.9 1155 10/10/2017 22.1 6.4 3.6 1178 11/1/2018 17.3 6.5 0.7 1157 9/12/2019 21.8 6.0 1517 10/13/2020 17.4 6.3 761 10/28/2021 15.9 6.0 0.4 1303 PW-71 9/28/2000 19.3 6.9 2230 9/12/2001 16.6 6.6 3190 9/20/2002 16.2 6.7 3250 8/20/2004 19.6 6.6 2666 3/4/2009 13.8 5.2 3010 PW-8S 9/27/2000 15.5 6.3 1130 9/6/2001 19.0 6.5 1040 9/17/2003 17.4 6.2 2080 8/17/2004 20.0 6.3 1628 3/3/2009 14.1 9.7 1670 PW-91 9/27/2000 19.2 7.0 1860 3/12/2009 19.0 5.4 1410 PW-10D 9/26/2000 15.1 8.3 703 9/11/2001 15.5 6.9 769 9/18/2002 19.8 9.8 354 8/17/2004 18.0 9.3 235 3/29/2010 18.1 9.9 920 11/1/2011 19.3 7.7 6.8 53 11/21/2012 14.3 12.8 4.7 103 12/11/2013 13.3 12.0 4.6 120 12/10/2014 13.6 9.8 4.6 342 11/3/2015 17.7 7.1 2.7 1225 11/17/2016 17.5 9.9 2.1 259 10/10/2017 21.3 7.3 4.6 285 10/31/2018 23.3 9.9 4.9 250 9/12/2019 24.9 9.9 298 10/12/2020 19.2 10.3 130 10/26/2021 17.4 7.0 0.9 220 TABLE 4 Page 5 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification PW-101 9/26/2000 16.7 6.1 787 9/11/2001 15.6 6.2 1080 9/18/2002 16.0 6.4 1210 8/17/2004 15.9 6.3 1192 3/12/2009 16.5 3.7 2110 3/29/2010 15.6 7.7 3960 11/1/2011 17.4 7.9 6.1 1123 11/19/2012 15.0 7.3 1.9 1693 12/11/2013 11.9 6.5 7.2 973 12/10/2014 14.3 6.4 2.7 214 10/29/2015 19.7 8.1 2.5 1356 11/17/2016 17.3 6.2 1.7 1529 10/10/2017 22.5 6.9 2.8 930 11/1/2018 16.3 7.3 11.8 62 9/12/2019 22.2 6.2 2000 10/12/2020 17.7 6.2 1150 10/26/2021 17.5 5.3 0.9 2254 PW-111 9/29/2000 16.3 6.9 649 9/11/2001 17.2 7.2 722 9/18/2002 19.1 8.1 618 8/25/2004 19.1 7.8 294 3/5/2009 16.1 5.2 929 PW-121 10/2/2000 23.1 7.1 659 9/11/2001 15.9 6.5 554 9/19/2002 17.6 6.7 689 8/17/2004 17.3 5.8 525 8/22/2006 16.9 5.5 90 3/3/2009 13.9 6.1 752 3/31/2010 17.0 6.4 634 11/2/2011 21.3 8.9 1.5 47 11/20/2012 16.3 8.1 3.4 152 12/17/2013 11.8 7.0 8.8 160 12/12/2014 11.7 7.1 9.2 880 10/30/2015 15.8 7.2 2.9 650 11/21/2016 16.1 6.7 2.7 597 10/11/2017 21.3 6.5 8.9 660 11/6/2018 19.1 7.2 3.4 816 9/11/2019 25.5 6.3 1022 10/14/2020 18.0 6.4 446 10/28/2021 17.1 6.3 0.4 852 PW-131 9/29/2000 17.5 6.7 1100 9/12/2001 18.3 6.9 937 9/20/2002 18.4 7.2 999 9/23/2003 17.8 6.3 890 8/25/2004 17.8 7.0 896 3/4/2009 16.5 6.7 483 3/31/2010 18.5 8.1 1640 11/3/2011 12.1 9.5 6.3 780 11/23/2012 19.2 8.4 1.7 1323 12/16/2013 13.1 6.8 8.7 319 12/12/2014 17.5 6.9 2.9 1450 10/26/2015 16.9 6.9 1.0 1701 11/18/2016 18.0 6.9 1.3 976 10/11/2017 19.8 6.8 3.0 791 10/31/2018 17.7 7.1 10.1 1003 9/11/2019 24.7 6.9 1247 10/13/2020 18.3 7.0 571 10/28/2021 16.2 6.9 0.4 1007 PW-14D 10/31/2000 23.0 12.2 6.91 9/10/2001 19.3 12.7 6,720 8/19/2004 19.2 12.2 4941 8/22/2006 20.5 12.8 613 3/11/2009 18.9 9.7 6400 3/31/2010 16.0 12.0 6640 11/7/2011 14.8 9.6 7.5 1253 11/27/2012 13.3 12.7 2.8 1776 12/12/2013 9.5 7.0 2.6 629 12/9/2014 16.8 12.1 5.2 381 11/3/2015 18.1 9.1 1.7 340 11/16/2016 15.6 13.1 2.0 3999 10/12/2017 18.8 6.9 5.1 612 11/5/2018 19.2 12.7 2.0 4246 9/17/2019 26.0 12.5 365 10/14/2020 19.7 12.1 3370 10/27/2021 15.9 10.0 0.0 5677 PW-14S 10/30/2000 17.7 6.0 130 9/6/2001 17.8 6.3 185 8/19/2004 16.8 5.9 95 8/22/2006 16.8 5.1 185 3/10/2009 15.7 4.0 68 TABLE 4 Page 6 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification PW-15D 10/31/2000 15.5 6.8 1.46 9/6/2001 16.8 6.7 1.68 9/16/2003 16.3 7.5 730 8/19/2004 -- -- -- 8/23/2006 16.0 6.3 1.6 3/11/2009 19.0 4.0 79 3/30/2010 15.9 6.2 1950 11/7/2011 11.1 6.3 8.1 95 11/26/2012 17.3 6.3 1.1 1204 12/12/2013 9.4 6.9 7.0 727 12/9/2014 16.1 7.0 2.8 1628 10/28/2015 18.7 7.1 1.0 966 11/15/2016 17.3 7.8 2.4 867 10/12/2017 18.1 6.9 2.8 738 11/5/2018 15.9 7.5 0.7 1360 9/17/2019 21.1 7.2 920 10/14/2020 19.6 6.4 34 10/27/2021 15.2 6.0 0.4 784 PW-15S 10/30/2000 16.7 6.4 467 9/6/2001 16.3 7.2 648 8/19/2004 -- -- -- 8/23/2006 17.9 6.5 604 3/11/2009 17.6 4.5 432 PW-16D 11/2/2000 17.1 7.4 85.7 9/6/2001 15.7 7.3 96 8/19/2004 16.5 7.2 845 8/23/2006 15.8 6.7 125 3/11/2009 19.1 3.8 633 3/30/2010 15.4 6.6 1280 11/7/2011 16.8 8.2 6.1 460 11/26/2012 19.8 6.8 1.6 926 12/12/2013 8.4 7.8 9.7 365 12/9/2014 15.2 7.7 2.9 1327 10/28/2015 18.6 7.1 0.8 815 11/15/2016 18.0 8.4 1.7 709 10/12/2017 18.8 7.8 3.2 1364 11/5/2018 16.3 7.4 2.4 619 9/12/2019 22.5 7.2 689 10/14/2020 18.4 6.2 45 10/27/2021 16.1 6.5 0.4 604 PW-16S 10/30/2000 17.4 6.3 347 9/6/2001 17.6 6.3 499 8/19/2004 17.2 6.3 291 8/23/2006 18.6 6.8 416 PW-17 11/3/2000 18.8 6.4 44.4 9/12/2001 18.3 6.5 364 9/18/2002 16.8 6.6 424 8/19/2004 17.3 6.6 447 3/5/2009 15.9 7.4 242 PW-18 11/3/2000 15.6 10.3 44.2 9/10/2001 17.3 11.2 853 9/16/2003 16.8 12.9 9040 8/19/2004 -- -- -- 8/22/2006 18.5 13.1 121 3/11/2009 20.3 8.7 1310 3/31 /2010 17.7 12.2 12200 11/8/2011 7.7 6.1 9.6 954 11/26/2012 15.1 12.0 3.1 393 12/12/2013 10.6 12.5 8.7 66 12/9/2014 14.1 12.2 7.6 1134 10/26/2015 15.5 12.7 4.3 1102 11/15/2016 17.2 13.5 7.3 3999 10/16/2017 16.7 12.8 7.9 1217 11/7/2018 17.5 12.7 4.8 1210 9/17/2019 Not Sampled 10/14/2020 Not Sampled 10/27/2021 Not Sampled PW-19 11/6/2001 15.3 7.2 268 9/18/2002 18.6 7.5 387 9/16/2003 11.8 8.9 483 8/17/2004 16.2 7.8 450 3/10/2009 17.1 9.2 299 PW-DR1 2/25/2009 13.6 6.2 1950 PW-SIS1 8/19/2004 15.7 6.8 536 3/9/2009 17.2 5.8 210 TABLE 4 Page 7 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification PW-SF1 4/2/2010 17.6 8.8 3960 11/3/2011 18.6 8.7 3.4 896 11/20/2012 14.9 7.6 1.8 147 12/9/2013 14.9 6.8 11.3 39 12/8/2014 14.5 6.7 3.4 1272 10/27/2015 14.1 6.8 3.1 1656 11/17/2016 15.9 6.9 1.6 845 10/11/2017 18.3 6.4 3.3 819 10/31/2018 17.2 6.4 0.5 392 9/10/2019 24.6 6.0 218 10/9/2020 17.5 7.1 676 10/27/2021 15.6 6.3 0.5 1091 RW-LFS1 2/26/2009 14.8 6.0 3010 RW-LFS2 2/26/2009 15.7 6.2 2460 RW-NIS1 3/6/2009 15.0 5.1 3190 RW-SIS2 3/9/2009 17.7 3.8 160 RW-SIS3 3/4/2009 15.6 6.0 681 RW-SIS4 3/4/2009 12.7 6.1 97 RW-SISS 3/4/2009 12.5 6.7 425 RW-SIS6 3/4/2009 15.2 6.3 322 W-1 9/27/2000 16.2 6.5 330 9/10/2001 17.5 6.6 296 9/18/2002 17.1 6.6 307 9/17/2003 17.6 6.3 448 8/17/2004 17.1 6.8 390 3/3/2009 16.4 6.9 484 W-4 9/27/2000 14.9 6.5 267 9/10/2001 16.0 6.6 263 9/17/2002 18.4 6.9 342 9/17/2003 16.5 6.1 290 8/17/2004 18.4 6.0 248 W-4A 9/27/2000 14.7 6.5 612 9/10/2001 15.1 6.5 773 9/14/2002 15.5 6.4 653 9/17/2003 14.5 6.1 434 8/17/2004 15.5 6.4 475 2/27/2009 18.6 6.2 223 3/31/2010 15.6 7.6 52100 11/2/2011 14.7 9.0 1.0 695 11/19/2012 14.5 7.6 3.4 32 12/17/2013 10.8 6.5 9.5 546 12/8/2014 12.5 6.6 4.2 1006 10/27/2015 14.3 6.7 1.8 234 11/16/2016 16.3 7.6 1.3 356 10/11/2017 21.9 6.6 4.1 383 10/31/2018 17.3 6.6 10.0 13 9/11/2019 23.2 7.1 337 10/9/2020 19.7 6.2 144 10/27/2021 15.3 6.0 0.4 270 W-5 9/27/2000 15.7 6.4 2530 10/30/2000 15.3 6.3 2580 9/10/2001 15.9 6.4 2170 9/18/2002 16.1 6.9 2060 8/18/2004 -- -- -- 3/3/2009 14.1 6.3 556 W-6A 9/28/2000 17.1 5.9 4950 W-18 3/5/2009 14.6 6.1 361 W-21 9/28/2000 14.3 6.0 343 9/10/2001 14.8 6.6 310 9/17/2002 15.5 6.7 342 9/17/2003 14.9 6.1 360 8/17/2004 16.8 6.5 292 2/24/2009 13.4 6.6 900 W-23A 3/4/2009 11.8 6.4 426 W-24 3/5/2009 TABLE 4 Page 8 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification Surface Water = 175 SW-1 11/2/2000 10.4 6.7 9/14/2001 20.1 6.4 153 9/24/2002 Dry -- -- 9/16/2003 19.9 6.8 119 8/23/2004 20.2 7.4 59 10/22/2015 Dry 11/21/2016 Dry 10/13/2017 Dry 11/7/2018 12.8 7.9 6.7 177 9/18/2019 Dry 10/22/2020 Dry 10/21/2021 Dry SW-2 11/2/2000 16.6 7.2 2070 9/14/2001 21.2 7.1 1640 9/24/2002 20.9 5.8 1870 9/15/2003 21.8 7.2 2160 8/23/2004 24.8 7.3 98 8/22/2006 20.8 7.0 226 4/1/2010 15.3 7.5 103 11/3/2011 14.3 8.4 378 11/20/2012 Dry 12/11/2013 Dry 12/8/2014 Dry 10/22/2015 Dry 11/21/2016 Dry 10/13/2017 21.7 7.8 5.3 112 11/7/2018 14.7 7.7 7.1 251 9/18/2019 Dry 10/22/2020 Dry 10/21/2021 Dry SW-3 11/2/2000 11.0 8.0 359 9/14/2001 20.1 7.3 199 9/24/2002 19.3 6.7 3450 9/16/2003 19.7 7.3 244 8/25/2004 23.1 8.1 133 8/22/2006 23.2 7.5 480 4/1/2010 15.6 7.6 6850 11/3/2011 10.6 8.9 11.1 261 11/20/2012 11.1 9.1 6.0 35 12/11/2013 5.5 9.0 1.6 144 12/8/2014 10.2 8.4 16.2 108 10/22/2015 16.6 7.5 4.8 224 11/17/2016 12.7 7.7 2.2 1577 10/13/2017 19.1 7.4 2.2 246 11/7/2018 19.2 7.9 6.6 298 9/18/2019 21.8 7.7 323 10/22/2020 20.8 8.4 4.5 281 10/21/2021 11.6 4.9 2.7 312 SW-3A 8/25/2004 21.9 8.1 126 SW-313 8/25/2004 21.9 7.7 123 SW-4 11/2/2000 12.8 6.9 964 9/14/2001 19.9 7.2 771 9/15/2003 25.0 7.5 473 8/25/2004 22.9 7.5 452 8/22/2006 22.2 7.3 112 4/1/2010 14.9 7.7 102 11/3/2011 14.5 7.7 6.1 671 11/20/2012 11.5 9.1 5.6 22 12/13/2013 4.2 8.8 9.5 1 12/8/2014 7.2 8.3 17.4 147 10/22/2015 15.8 8.4 4.8 0 11/21/2016 9.8 8.1 4.0 206 10/13/2017 19.9 6.3 8.8 878 11/7/2018 19.5 8.1 6.3 252 9/18/2019 21.2 6.5 1285 10/22/2020 20.5 8.3 2.5 108 10/21/2021 15.0 4.7 2.1 1546 TABLE 4 Page 9 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification SW-5 11/2/2000 14.7 6.9 415 9/14/2001 19.7 6.7 295 9/24/2002 19.7 6.7 295 9/16/2003 20.6 7.0 300 8/25/2004 21.1 7.5 168 8/22/2006 22.2 7.5 540 4/1/2010 17.1 7.4 6760 11/3/2011 11.9 9.6 9.9 212 11/20/2012 11.5 9.1 5.6 22 12/16/2013 8.7 8.5 9.7 78 12/8/2014 7.7 10.1 11.0 229 10/22/2015 16.3 7.3 4.9 199 11/17/2016 10.2 7.8 4.8 320 10/13/2017 19.0 7.4 9.2 314 11/7/2018 14.9 7.8 6.1 217 9/18/2019 22.0 9.1 311 10/22/2020 19.5 8.1 3.8 301 10/21/2021 13.3 6.1 4.1 438 SW-6 11/2/2000 11.4 7.5 215 9/14/2001 22.4 6.9 133 9/24/2002 22.4 7.5 168 9/16/2003 21.5 7.4 117 8/25/2004 26.4 8.2 82 8/22/2006 25.7 7.7 168 4/1/2010 14.3 8.3 103 11/3/2011 14.5 10.3 6.8 326 shallow-1' 11/21/2012 8.1 9.0 5.4 8 deep-8.5' 11/21/2012 8.7 9.3 5.2 79 shallow - 1' 12/13/2013 5.2 8.2 9.8 45 deep - 11' 12/13/2013 5.6 8.3 9.5 26 shallow - 1' 12/15/2014 9.0 8.6 13.9 212 deep - 8.6' 12/15/2014 9.1 8.7 13.3 279 shallow - 1' 10/22/2015 21.6 7.5 3.9 127 deep - 8.6' 10/22/2015 20.3 7.4 4.1 97 shallow-1' 11/21/2016 12.2 8.0 4.4 154 deep-8.5' 11/21/2016 11.9 7.9 4.2 151 shallow - 1' 10/13/2017 22.5 9.4 13.6 303 deep - 10.2' 10/13/2017 22.0 9.2 13.3 293 shallow - 1' 11/7/2018 18.1 9.9 7.3 197 deep - 11.0' 11/7/2018 17.8 9.5 7.3 100 shallow - 1' 9/18/2019 24.4 8.1 177 deep - 10' 9/18/2019 24.6 8.6 163 shallow - 1' 10/22/2020 21.8 5.9 4.8 56 deep - 11' 10/22/2020 22.3 4.8 5.7 69 shallow - 1' 10/21/2021 16.0 5.7 2.0 150 deep - 15.3' 10/21/2021 16.2 5.3 1.7 124 SW-7 11/3/2000 9.0 6.3 319 9/13/2001 20.3 6.8 220 9/24/2002 21.8 6.6 263 9/15/2003 23.8 7.0 156 8/23/2004 25.5 7.2 85 4/1/2010 13.4 7.4 103 11/3/2011 11.8 9.0 13.3 84 shallow-1' 11/21/2012 10.5 9.1 6.4 58 deep -11.5' 11/21/2012 10.7 9.0 6.8 319 shallow - 1' 12/13/2013 6.6 8.2 9.1 18 deep - 13' 12/13/2013 6.4 8.2 9.6 4 shallow - 1' 12/15/2014 10.5 8.6 13.4 186 deep - 12.3' 12/15/2014 11.1 8.4 13.8 179 shallow - 1' 10/22/2015 18.6 8.6 5.4 75 deep - 12.1' 10/22/2015 18.3 8.6 5.5 64 shallow-1' 11/21/2016 10.5 8.0 4.4 262 deep -12' 11/21/2016 9.7 9.2 5.7 276 shallow - 1' 10/13/2017 23.3 8.6 13.8 338 deep - 13.0' 10/13/2017 22.3 8.3 13.5 318 shallow - 1' 11/7/2018 17.8 8.7 6.9 82 deep - 16.0' 11/7/2018 17.8 8.7 6.4 80 shallow - 1' 9/18/2019 26.2 8.5 216 deep - 19.5' 9/18/2019 24.7 8.2 169 shallow - 1' 10/22/2020 23.0 8.2 6.4 144 deep - 11' 10/22/2020 21.6 8.2 5.2 89 shallow - 1' 10/21/2021 18.1 5.4 1.0 116 deep - 14' 10/21/2021 17.9 5.3 1.0 111 TABLE 4 Page 10 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date (degrees Celsius) pH (Std. Units) Oxygen (mg/1) (US/cm) Sample Identification SW-DRP-2 11/3/2000 13.5 6.5 1870 East 9/14/2001 20.3 7.0 224 West 9/14/2001 20.5 6.9 239 9/15/2003 23.1 7.1 150 8/23/2004 22.0 3.7 386 4/1/2010 14.1 7.8 102 11/3/2011 11.5 8.8 10.9 140 shallow-1' 11/21/2012 10.2 8.9 5.9 43 deep - 12.5' 11/21/2012 9.9 9.1 5.6 67 shallow - 1' 12/13/2013 5.8 8.2 9.4 10 deep - 10' 12/13/2013 5.7 6.9 9.9 28 shallow - 1' 12/15/2014 10.2 8.7 16.5 176 deep - 12.3' 12/15/2014 10.2 8.5 16.3 176 shallow - 1' 10/22/2015 15.9 8.1 6.3 0 deep - 12.3' 10/22/2015 16.0 8.1 6.4 0 shallow-1' 11/21/2016 9.7 8.1 3.7 203 deep-12' 11/21/2016 9.6 7.9 6.6 206 shallow - 1' 10/13/2017 23.3 8.5 16.5 324 deep - 14.2' 10/13/2017 21.7 8.6 16.3 334 shallow - 1' 11/7/2018 18.9 9.1 6.7 97 deep - 12.0' 11/7/2018 17.9 8.8 6.5 83 shallow - 1' 9/18/2019 24.8 7.7 300 deep -10' 9/18/2019 25.0 8.3 159 shallow - 1' 10/22/2020 25.3 8.6 5.3 119 deep - 12' 10/22/2020 24.6 8.6 4.6 89 shallow - 1' 10/21/2021 17.8 6.2 1.9 124 deep - 11.5' 10/21/2021 17.7 5.9 1.8 113 SW-DRP-4 11/3/2000 13.1 6.3 544 East 9/14/2001 18.8 6.1 286 West 9/14/2001 17.7 6.8 237 9/15/2003 23.4 7.1 182 SW-DRP-10 11/2/2000 12.6 6.9 306 East 9/13/2001 21.9 7.6 214 West 9/13/2001 21.4 7.2 215 9/15/2003 23.5 7.1 154 SW-DRP-11 11/2/2000 16.5 6.4 559 9/13/2001 20.4 6.4 343 9/24/2002 23.6 6.3 527 9/15/2003 25.4 6.8 357 8/23/2004 15.7 7.9 276 4/1/2010 14.0 7.3 104 11/3/2011 13.5 9.1 12.2 58 shallow-1' 11/21/2012 9.2 11.0 8.2 27 deep -9' 11/21/2012 10.3 9.3 8.3 26 shallow - 1' 12/16/2013 5.6 8.5 9.7 1 deep - 12' 12/16/2013 5.4 8.7 9.2 34 shallow - 1' 12/15/2014 7.5 8.9 16.4 164 deep - 11.6' 12/15/2014 9.3 8.8 16.9 198 shallow - 1' 10/22/2015 18.4 7.9 5.6 0 deep - 11.7' 10/22/2015 18.0 7.6 6.0 0 shallow-1' 11/21/2016 11.0 8.2 7.0 362 deep-12' 11/21/2016 11.2 8.2 2.7 398 shallow - 1' 10/13/2017 23.0 7.7 16.4 357 deep - 12.5' 10/13/2017 21.9 7.9 16.7 342 shallow - 1' 11/7/2018 17.9 8.7 6.4 87 deep - 11.5' 11/7/2018 17.8 8.9 6.7 167 shallow - 1' 9/18/2019 26.8 8.3 230 deep - 5' 9/18/2019 28.6 7.7 224 shallow - 1' 10/22/2020 23.9 8.1 6.3 195 deep - 10' 10/22/2020 23.0 7.5 4.3 149 shallow - 1' 10/21/2021 20.0 6.4 0.7 223 deep - 6.5' 10/21/2021 18.9 6.3 0.7 190 SWT-40 East @ 1' ^ 9/13/2001 21.9 7.0 219 East @ 3.25' ^ 9/13/2001 22.0 7.0 219 West @ 0.5' ^ 9/13/2001 21.8 7.0 217 SWT-50 East @ 1' ^ 9/13/2001 21.0 7.5 217 East @ 3' ^ 9/13/2001 22.1 7.0 216 West @ 1' " 9/13/2001 21.6 7.0 216 SWT-70 East 9/13/2001 22.0 7.1 216 West 9/13/2001 20.8 7.2 216 RCP-1 11/2/2000 15.3 6.6 277 RCP-2 11/2/2000 15.4 6.6 248 TABLE 5 MONITORING WELL LATITUDE/LONGITUDE, DEPTHS AND ELEVATIONS SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Facility Name Seaboard Chemical/Riverdale Drive Landfill EPA ID Number NCD 071 574 164 Well ID Type Well Use Northing Easting Reference Source of Information TOC Elevation Well Depth MW-1 well monitoring 801318.45 1729231.88 state plane coord Jamestown Engineering 790.46 57.7 MW-3C well monitoring 801265.20 1731350.08 state plane coord Jamestown Engineering 692.74 57 MW-6 well monitoring 799702.65 1731990.93 state plane coord Jamestown Engineering 761.47 110 MW-10 well monitoring 800464.20 1732378.92 state plane coord Jamestown Engineering 695.01 28 MW-12A well monitoring 801788.63 1730912.94 state plane coord Jamestown Engineering 693.07 20 MW-12B well monitoring 801780.30 1730911.77 state plane coord Jamestown Engineering 693.86 58 MW-12D well monitoring 801770.20 1730908.12 state plane coord Jamestown Engineering 694.21 202 MW-15A well monitoring 800903.23 1730181.46 state plane coord Jamestown Engineering 764.33 34 OW-DR2 well monitoring 801266.66 1731357.68 state plane coord Jamestown Engineering 695.87 186 OW-DR3 well monitoring 801185.56 1731735.15 state plane coord Jamestown Engineering 702.93 160 OW-LFS-2 well monitoring 800674.15 1732093.91 state plane coord Jamestown Engineering 699.45 50 PW-3D well monitoring 800603.04 1730831.13 state plane coord Jamestown Engineering 738.60 209.5 PW-41 well monitoring 800545.88 1731099.56 state plane coord Jamestown Engineering 735.00 ** 122 PW-5D well monitoring 801164.35 1731363.53 state plane coord Jamestown Engineering 696.27 306.5 PW-6D well monitoring 801425.12 1732032.71 state plane coord Jamestown Engineering 696.79 275 PW-61 well monitoring 801415.38 1732022.44 state plane coord Jamestown Engineering 697.41 75 PW-10D well monitoring 800446.73 1732384.15 state plane coord Jamestown Engineering 697.26 200 PW-101 well monitoring 800456.28 1732373.34 state plane coord Jamestown Engineering 695.97 100 PW-121 well monitoring 799844.10 1730816.38 state plane coord Jamestown Engineering 749.48 105 PW-131 well monitoring 801310.27 1730977.69 state plane coord Jamestown Engineering 739.01 250 PW-14D well monitoring 801653.66 1731389.41 state plane coord Jamestown Engineering 686.50 * 198.8 PW-15D well monitoring 801544.36 1731748.91 state plane coord Jamestown Engineering 685.80 163.5 PW-16D well monitoring 801711.36 1732067.64 state plane coord Jamestown Engineering 686.68 179 W-4A well monitoring 1800667.98 11730625.66 state plane coord iJamestown Engineering 1712.64 138.5 I * Elevation corrected for repairs performed on PW-14D during October 2015 monitoring event. ** Elevation corrected for repairs performed on PW-41 during November 2016 monitoring event. APPENDIX A Laboratory Report 2�SQ pCCgF ENCO Laboratories 9e0 Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Monday, November 22, 2021 Babb & Associates (BA024) Attn: Gary Babb 5506 Bradford Pear Court Raleigh, NC 27606 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Seaboard/Riverdale Landfill ENCO Workorder(s): CE13949 Dear Gary Babb, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, October 29, 2021. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, 4P 0 ee Bill Scott Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 of H 1 PROJECT NARRATIVE Client: Babb & Associates (BA024) Project: Seaboard/Riverdale Landfill Lab ID: CE13949-Rev Overview (� �Eo www.encolabs.com This report is an amendment to the original report dated 111221 for this work order. This report was revised to correct sample ID CE13949-18 from MW-1 to MW-121. Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in the QC Remarks section below. Quality Control Samples No Comments Quality Control Remarks No Comments Other Comments The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of the report. Released By: Environmental Conservation Laboratories, Inc. Bill Scott Project Manager FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 2 of 81 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 4401-MW3 Lab ID: CE13949-01 Sampled: 10/26/21 08:30 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/09/21 11/02/21 11:26 11/02/21 18:19 EPA 8260D EPA 503013_MS 11/09/21 11/04/21 18:41 11/05/21 13:23 Client ID: 4401-MW3C Lab ID: CE13949-02 Sampled: 10/26/21 09:30 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/09/21 11/02/21 11:26 11/02/21 18:45 EPA 8260D EPA 503013_MS 11/09/21 11/04/21 18:41 11/05/21 13:53 Client ID: 4401-MW3C Lab ID: CE13949-02RE2 Sampled: 10/26/21 09:30 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/09/21 11/09/21 16:12 11/09/21 22:25 Client ID: 4401-MW6 Lab ID: CE13949-03 Sampled: 10/28/21 12:50 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 11/11/21 11/02/21 11:26 11/02/21 19:11 EPA 8260D EPA 503013_MS 11/11/21 11/09/21 16:12 11/10/21 01:12 Client ID: 4401-MW10 Lab ID: CE13949-04 Sampled: 10/26/21 10:20 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/09/21 11/02/21 11:26 11/02/21 19:36 EPA 8260D EPA 503013_MS 11/09/21 11/04/21 18:41 11/05/21 14:22 Client ID: 4401-MW12A Lab ID: CE13949-05 Sampled: 10/26/21 13:10 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/09/21 11/02/21 11:26 11/02/21 20:02 EPA 8260D EPA 503013_MS 11/09/21 11/04/21 18:41 11/05/21 14:52 Client ID: 4401-MW12B Lab ID: CE13949-06 Sampled: 10/26/21 14:10 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 11/09/21 11/02/21 11:26 11/02/21 20:28 EPA 8260D EPA 503013_MS 11/09/21 11/04/21 18:41 11/05/21 15:21 Client ID: 4401-MW12D Lab ID: CE13949-07 Sampled: 10/26/21 14:40 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/09/21 11/02/21 11:26 11/02/21 20:53 EPA 8260D EPA 503013_MS 11/09/21 11/04/21 18:41 11/05/21 15:51 Client ID: 4401-MW15A Lab ID: CE13949-08 Sampled: 10/28/21 08:25 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/11/21 11/02/21 13:32 11/03/21 02:01 Client ID: 4401-MW15A Lab ID: CE13949-08RE1 Sampled: 10/28/21 08:25 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/11/21 11/10/21 13:59 11/11/21 03:17 Client ID: 4401-OWDR2 Lab ID: CE13949-09 Sampled: 10/28/21 09:45 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 11/11/21 11/02/21 13:32 11/03/21 02:26 EPA 8260D EPA 5030B_MIS 11/11/21 11/09/21 16:12 11/10/21 02:08 Client ID: 4401-OWLFS2 Lab ID: CE13949-10 Sampled: 10/28/21 12:15 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(sl EPA 8260D EPA 503013_MS 11/11/21 11/02/21 13:32 11/03/21 02:52 EPA 8260D EPA 503013_MS 11/11/21 11/09/21 16:12 11/10/21 02:35 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 Of 81 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 4401-PW3D Lab ID: CE13949-11 Sampled: 10/27/21 14:15 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/10/21 11/02/21 13:32 11/03/21 03:18 EPA 8260D EPA 503013_MS 11/10/21 11/05/21 17:42 11/06/21 18:40 Client ID: 4401-PW3D Lab ID: CE13949-11RE1 Sampled: 10/27/21 14:15 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/10/21 11/09/21 16:12 11/10/21 00:44 Client ID: 4401-PW5D Lab ID: CE13949-12 Sampled: 10/28/21 10:40 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/11/21 11/02/21 13:32 11/03/21 03:44 EPA 8260D EPA 503013_MS 11/11/21 11/09/21 16:12 11/10/21 03:03 Client ID: 4401-PW4I Lab ID: CE13949-13 Sampled: 10/27/21 15:05 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 11/10/21 11/02/21 13:32 11/03/21 04:09 EPA 8260D EPA 503013_MS 11/10/21 11/05/21 17:42 11/06/21 19:09 Client ID: 4401-PW4I Lab ID: CE13949-13RE1 Sampled: 10/27/21 15:05 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/10/21 11/09/21 16:12 11/10/21 00:16 Client ID: 4401-PW6I Lab ID: CE13949-14 Sampled: 10/28/21 11:45 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/11/21 11/02/21 13:32 11/03/21 04:35 EPA 8260D EPA 503013_MS 11/11/21 11/09/21 16:12 11/10/21 03:31 Client ID: 4401-PW6D Lab ID: CE13949-15 Sampled: 10/28/21 11:15 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/11/21 11/02/21 13:32 11/03/21 05:01 EPA 8260D EPA 5030B_MS 11/11/21 11/09/21 16:12 11/10/21 03:59 Client ID: 4401-PWSOI Lab ID: CE13949-16 Sampled: 10/26/21 12:00 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MIS 11/09/21 11/02/21 13:32 11/03/21 05:26 EPA 8260D EPA 503013_MS 11/09/21 11/04/21 18:41 11/05/21 16:20 Client ID: 4401-PW10D Lab ID: CE13949-17 Sampled: 10/26/21 11:10 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/09/21 11/02/21 13:32 11/03/21 01:35 EPA 8260D EPA 503013_MS 11/09/21 11/04/21 18:41 11/05/21 16:49 Client ID: 4401-MW12I Lab ID: CE13949-18 Sampled: 10/28/21 13:25 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/11/21 11/02/21 13:32 11/03/21 05:52 EPA 8260D EPA 5030B_MS 11/11/21 11/09/21 16:12 11/10/21 04:27 Client ID: 4401-PW13I Lab ID: CE13949-19 Sampled: 10/28/21 09:00 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MIS 11/11/21 11/02/21 13:32 11/03/21 06:18 EPA 8260D EPA 503013_MS 11/11/21 11/09/21 16:12 11/10/21 04:55 Client ID: 4401-PW14D Lab ID: CE13949-20 Sampled: 10/27/21 11:00 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/10/21 11/02/21 13:32 11/03/21 06:43 EPA 8260D EPA 503013_MS 11/10/21 11/03/21 16:23 11/03/21 22:24 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 4 Of 81 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 4401-PW15D Lab ID: CE13949-21 Sampled: 10/27/21 10:20 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/10/21 11/02/21 13:32 11/03/21 07:09 EPA 8260D EPA 503013_MS 11/10/21 11/03/21 16:23 11/03/21 22:53 Client ID: 4401-PWSSD Lab ID: CE13949-21RE1 Sampled: 10/27/21 10:20 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/10/21 11/05/21 17:42 11/06/21 17:12 Client ID: 4401-PW16D Lab ID: CE13949-22 Sampled: 10/27/21 09:10 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/10/21 11/02/21 13:32 11/03/21 07:35 EPA 8260D EPA 503013_MS 11/10/21 11/03/21 16:23 11/03/21 23:22 Client ID: 4401-PW16D Lab ID: CE13949-22RE1 Sampled: 10/27/21 09:10 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 11/10/21 11/05/21 17:42 11/06/21 17:42 Client ID: 4401-PWSF1 Lab ID: CE13949-23 Sampled: 10/27/21 13:05 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MIS 11/10/21 11/02/21 13:32 11/03/21 08:00 EPA 8260D EPA 503013_MS 11/10/21 11/05/21 17:42 11/06/21 19:38 Client ID: 4401-W4A Lab ID: CE13949-24 Sampled: 10/27/21 12:35 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/10/21 11/02/21 13:32 11/03/21 08:27 EPA 8260D EPA 503013_MS 11/10/21 11/08/21 17:00 11/08/21 20:29 Client ID: 4401-TripBlank Lab ID: CE13949-25 Sampled: 10/26/21 08:30 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/09/21 11/02/21 13:32 11/03/21 08:53 EPA 8260D EPA 5030B_MS 11/09/21 11/04/21 18:41 11/05/21 11:55 Client ID: 4401-TripBlank Lab ID: CE13949-26 Sampled: 10/26/21 08:30 Received: 10/29/21 10:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MIS 11/09/21 11/02/21 13:32 11/03/21 09:18 EPA 8260D EPA 503013_MS 11/09/21 11/04/21 18:41 11/05/21 12:24 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 5 Of H 1 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 4401-MW3C Lab ID: CE13949-02 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 37 0.13 1.0 ug/L EPA 8260D 1,2-Dichloroethane 1.4 0.21 1.0 ug/L EPA 8260D 1,4-Dioxane 67 0.80 2.0 ug/L EPA 8260D Benzene 0.93 J 0.15 1.0 ug/L EPA 8260D Chlorobenzene 36 0.17 1.0 ug/L EPA 8260D Chloroethane 2.8 0.23 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 9.8 0.15 1.0 ug/L EPA 8260D trans-1,2-Dichloroethene 0.53 J 0.21 1.0 ug/L EPA 8260D Vinyl chloride 21 0.32 1.0 uq/L EPA 8260D I Client ID: 4401-MW3C Lab ID: CE33949-02RE2 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethene 2.0 0.21 1.0 ug/L EPA 8260D Client ID: 4401-MW6 Lab ID: CE13949-03 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 7.2 0.13 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 1.7 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 24 0.80 2.0 ug/L EPA 8260D Benzene 0.63 J 0.15 1.0 ug/L EPA 8260D Chlorobenzene 3.2 0.17 1.0 ug/L EPA 8260D Chloroethane 1.8 0.23 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 8.8 0.15 1.0 ug/L EPA 8260D Tetrachloroethene 0.85 J 0.17 1.0 ug/L EPA 8260D trans-1,2-Dichloroethene 0.41 J 0.21 1.0 ug/L EPA 8260D Trichloroethene 2.0 0.15 1.0 ug/L EPA 8260D Vinyl chloride 2.2 0.32 1.0 ug/L EPA 8260D Client ID: 4401-MW30 Lab ID: CE13949-04 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 6.6 0.80 2.0 uq/L EPA 8260D Client ID: 4401-MW12A Lab ID: CE13949-05 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dichlorobenzene 1.7 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 180 D 4.0 10 ug/L EPA 8260D Chlorobenzene 5.8 0.17 1.0 ug/L EPA 8260D Client ID: 4401-MW12B Lab ID: CE13949-06 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dichlorobenzene 2.2 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 110 D 4.0 10 ug/L EPA 8260D Chlorobenzene 7.7 0.17 1.0 ug/L EPA 8260D Client ID: 4401-MW12D Lab ID: CE13949-07 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 2.9 0.80 2.0 ug/L EPA 8260D Client ID: 4401-MW15A Lab ID: CE13949-08 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 1200 D 80 200 uq/L EPA 8260D Client ID: 4401-MW15A Lab ID: CE13949-0BRE3 Analvte Results Flag MDL PQL Units Method Notes 1,2-Dichlorobenzene 0.68 J 0.19 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 1.9 0.19 1.0 ug/L EPA 8260D Chlorobenzene 60 0.17 1.0 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 6 Of 81 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 4401-OWDR2 Lab ID: CE13949-09 Analvte Results Flag MDL Q Units Method Notes 1,1,1-Trichloroethane 5.2 D 0.60 5.0 ug/L EPA 8260D 1,1-Dichloroethane 130 D 0.65 5.0 ug/L EPA 8260D 1,1-Dichloroethene 54 D 1.0 5.0 ug/L EPA 8260D 1,2-Dichloroethane 6.0 D 1.0 5.0 ug/L EPA 8260D 1,4-Dioxane 250 D 20 50 ug/L EPA 8260D Chlorobenzene 36 D 0.85 5.0 ug/L EPA 8260D Chloroethane 11 D 1.2 5.0 ug/L EPA 8260D cis-1,2-Dichloroethene 230 D 0.75 5.0 ug/L EPA 8260D Vinyl chloride 20 D 1.6 5.0 uq/L EPA 8260D I Client ID: 4401-OWLFS2 Lab ID: CE13949-10 Analvte Results Flag MDL Q Units Method Notes 1,1-Dichloroethane 0.79 J 0.13 1.0 ug/L EPA 8260D 1,4-Dioxane 270 D 8.0 20 ug/L EPA 8260D Benzene 7.0 0.15 1.0 ug/L EPA 8260D Chlorobenzene 3.8 0.17 1.0 ug/L EPA 8260D Chloroethane 1.3 0.23 1.0 ug/L EPA 8260D Vinyl chloride 1.4 0.32 1.0 ug/L EPA 8260D Client ID: 4401-PW3D Lab ID: CE13949-11 Analvte Results Flag MDL Q Units Method Notes 1,1,1-Trichloroethane 890 D 60 500 ug/L EPA 8260D 1,1-Dichloroethane 660 D 65 500 ug/L EPA 8260D 1,1-Dichloroethene 1500 D 100 500 ug/L EPA 8260D 1,2-Dichloroethane 17000 D 100 500 ug/L EPA 8260D 1,4-Dioxane 160 D 4.0 10 ug/L EPA 8260D Benzene 280 JD 75 500 ug/L EPA 8260D Chlorobenzene 18000 D 85 500 ug/L EPA 8260D cis-1,2-Dichloroethene 380 JD 75 500 ug/L EPA 8260D Methylene chloride 1800 D 120 500 ug/L EPA 8260D Tetrachloroethene 1200 D 85 500 ug/L EPA 8260D Toluene 670 D 70 500 ug/L EPA 8260D Client ID: 4401-PW3D Lab ID: CE13949-11RE1 Analvte Results Flag MDL PQL Units Method Notes Trichloroethene 4200 D 75 500 ug/L EPA 8260D Client ID: 4401-PW5D Lab ID: CE13949-12 Analvte Results Flag MDL PQL Units Method Notes 1,1,1-Trichloroethane 7.6 JD 1.2 10 ug/L EPA 8260D 1,1-Dichloroethane 200 D 1.3 10 ug/L EPA 8260D 1,1-Dichloroethene 4.3 JD 2.1 10 ug/L EPA 8260D 1,2-Dichloroethane 15 D 2.1 10 ug/L EPA 8260D 1,4-Dioxane 400 D 40 100 ug/L EPA 8260D Benzene 5.4 JD 1.5 10 ug/L EPA 8260D Chlorobenzene 180 D 1.7 10 ug/L EPA 8260D cis-1,2-Dichloroethene 12 D 1.5 10 ug/L EPA 8260D Vinyl chloride 9.5 JD 3.2 10 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 7 Of H 1 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 4401-PW13I Lab ID: CE13949-19 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 87 0.13 1.0 ug/L EPA 8260D 1,2-Dichloroethane 1.2 0.21 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 0.74 J 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 70 0.80 2.0 ug/L EPA 8260D Benzene 2.3 0.15 1.0 ug/L EPA 8260D Chlorobenzene 9.4 0.17 1.0 ug/L EPA 8260D Chloroethane 1.2 0.23 1.0 ug/L EPA 8260D Toluene 0.53 J 0.14 1.0 ug/L EPA 8260D Vinyl chloride 0.94 J 0.32 1.0 uq/L EPA 8260D Client ID: 4401-PW14D Lab ID: CE13949-20 Analvte Results Flag MDL PQL Units Method Notes Chlorobenzene 0.80 J 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 0.76 J 0.15 1.0 ug/L EPA 8260D Ethylbenzene 0.67 J 0.13 1.0 ug/L EPA 8260D m,p-Xylenes 2.8 0.17 2.0 ug/L EPA 8260D o-Xylene 1.4 0.065 1.0 ug/L EPA 8260D Toluene 1.7 0.14 1.0 ug/L EPA 8260D Xylenes (Total) 4.2 0.45 3.0 ug/L EPA 8260D Client ID: 4401-PW1SD Lab ID: CE13949-21 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 18 0.13 1.0 ug/L EPA 8260D 1,2-Dichloroethane 0.53 1 0.21 1.0 ug/L EPA 8260D 1,4-Dioxane 53 0.80 2.0 ug/L EPA 8260D Chlorobenzene 2.0 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 27 0.15 1.0 ug/L EPA 8260D Vinyl chloride 1.1 0.32 1.0 ug/L EPA 8260D Client ID: 4401-PW1SD Lab ID: CE13949-21RE3 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethene 5.2 0.21 1.0 ug/L EPA 8260D Client ID: 4401-PW16D Lab ID: CE13949-22 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 20 0.13 1.0 ug/L EPA 8260D 1,4-Dioxane 23 0.80 2.0 ug/L EPA 8260D Chlorobenzene 40 0.17 1.0 ug/L EPA 8260D Chloroethane 1.5 0.23 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 32 0.15 1.0 ug/L EPA 8260D Vinyl chloride 3.6 0.32 1.0 uq/L EPA 8260D I Client ID: 4401-PW16D Lab ID: CE13949-22RE3 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethene 7.1 0.21 1.0 ug/L EPA 8260D Client ID: 4401-PWSF1 Lab ID: CE13949-23 Analvte Results Flag MDL PQL Units Method Notes 1,1,1-Trichloroethane 3300 D 60 500 ug/L EPA 8260D 1,1-Dichloroethane 6200 D 65 500 ug/L EPA 8260D 1,1-Dichloroethene 5300 D 100 500 ug/L EPA 8260D 1,4-Dioxane 2300 D 80 200 ug/L EPA 8260D Chlorobenzene 2100 D 85 500 ug/L EPA 8260D cis-1,2-Dichloroethene 38000 D 75 500 ug/L EPA 8260D Methylene chloride 260 ]D 120 500 ug/L EPA 8260D Toluene 720 D 70 500 ug/L EPA 8260D Trichlorofluoromethane 400 ]D 120 500 ug/L EPA 8260D Vinyl chloride 3200 D 160 500 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 9 Of H 1 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 4401-W4A Lab ID: CE13949-24 Analvte Results Flag MDL PQL Units Method Notes 1,1,1-Trichloroethane 24 D 0.60 5.0 ug/L EPA 8260D 1,1-Dichloroethane 110 D 0.65 5.0 ug/L EPA 8260D 1,1-Dichloroethene 43 D 1.0 5.0 ug/L EPA 8260D 1,2-Dichloroethane 2.8 ]D 1.0 5.0 ug/L EPA 8260D 1,4-Dioxane 54 0.80 2.0 ug/L EPA 8260D Benzene 6.6 D 0.75 5.0 ug/L EPA 8260D Chloroethane 4.6 ]D 1.2 5.0 ug/L EPA 8260D cis-1,2-Dichloroethene 170 D 0.75 5.0 ug/L EPA 8260D Vinyl chloride 98 D 1.6 5.0 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 10 Of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW1 Lab Sample ID:CE13949-01 Received: 10/29/21 10:45 Matrix: Water Sampled: 10/26/2108:30 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY QV-01 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1K04051 EPA 8260D 11/05/21 13:23 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1K04051 EPA 8260D 11/05/21 13:23 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 1K04051 EPA 8260D 11/05/21 13:23 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1K04051 EPA 8260D 11/05/21 13:23 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Chlorobenzene[108-90-7]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Ethylbenzene[100-41-4]A 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1K04051 EPA 8260D 11/05/21 13:23 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY o-Xylene [95-47-6]A 0.065 u ug/L 1 0.065 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Styrene[100-42-5]A 0.11 u ug/L 1 0.11 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Vinyl acetate [108-05-4]A 0.95 Ll ug/L 1 0.95 5.0 1K04051 EPA 8260D 11/05/21 13:23 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 11 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW1 Lab Sample ID:CE13949-01 Received: 10/29/21 10:45 Matrix: Water Sampled: 10/26/2108:30 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K04051 EPA 8260D 11/05/21 13:23 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 49 1 50.0 98 % 53-136 IK04051 EPA 6260D 11/05/21 13:23 RKY Dibromofluoromethane 50 1 50.0 100 % 67-129 IK04051 EPA 6260D 11105121 13:23 RKY Toluene-d8 48 1 50.0 96 % 59-134 IK04051 EPA 6260D 11105121 13:23 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1K02027 EPA 8260D 11/02/21 18:19 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 5.3 1 5.00 107 % 75-125 1K02027 EPA 8260D 11102121 18:19 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 12 of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW3C Lab Sample ID:CE13949-02 Received: 10/29/21 10:45 Matrix: Water Sampled: 10/26/2109:30 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY 1,1-Dichloroethane [75-34-3]A 37 ug/L 1 0.13 1.0 IK04051 EPA 8260D 11/05/21 13:53 RKY 1,1-Dichloroethene [75-35-4]A 2.0 ug/L 1 0.21 1.0 IK09032 EPA 8260D 11/09/21 22:25 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY 1,2-Dichloroethane [107-06-2]A 1.4 ug/L 1 0.21 1.0 IK04051 EPA 8260D 11/05/21 13:53 RKY 1,2-Dichloropropane [78-87-5]A 0.10 U ug/L 1 0.10 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 1K04051 EPA 8260D 11/05/21 13:53 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 1K04051 EPA 8260D 11/05/21 13:53 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Acetone [67-64-1]A 10 U ug/L 1 10 20 1K04051 EPA 8260D 11/05/21 13:53 RKY Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 1K04051 EPA 8260D 11/05/21 13:53 RKY Benzene [71-43-2]A 0.93 J ug/L 1 0.15 1.0 IK04051 EPA 8260D 11/05/21 13:53 RKY Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Bromodichloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Chlorobenzene [108-90-7]A 36 ug/L 1 0.17 1.0 IK04051 EPA 8260D 11/05/21 13:53 RKY Chloroethane [75-00-3]A 2.8 ug/L 1 0.23 1.0 IK04051 EPA 8260D 11/05/21 13:53 RKY Chloroform [67-66-3]A 0.18 U ug/L 1 0.18 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY cis-1,2-Dichloroethene [156-59-2]A 9.8 ug/L 1 0.15 1.0 IK04051 EPA 8260D 11/05/21 13:53 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Ethylbenzene[100-41-4]A 0.13 U ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 1K04051 EPA 8260D 11/05/21 13:53 RKY m,p-Xylenes[108-38-3/106-42-3]A 0.17 U ug/L 1 0.17 2.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY o-Xylene [95-47-6]A 0.065 U ug/L 1 0.065 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Styrene[100-42-5]A 0.11 U ug/L 1 0.11 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY trans-1,2-Dichloroethene [156-60-5]A 0.53 J ug/L 1 0.21 1.0 IK04051 EPA 8260D 11/05/21 13:53 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 1K04051 EPA 8260D 11/05/21 13:53 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 13 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW3C Lab Sample ID:CE13949-02 Received: 10/29/21 10:45 Matrix: Water Sampled: 10/26/2109:30 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 21 ug/L 1 0.32 1.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K04051 EPA 8260D 11/05/21 13:53 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 50 1 50.0 100 % 53-136 IK04051 EPA 6260D 11105121 13:53 RKY 4-Bromofluorobenzene 60 1 50.0 121 % 53-136 IK09032 EPA 6260D 11109121 22:25 RKY Dibromofluoromethane 51 1 50.0 102 % 67-129 IK04051 EPA 8260D 11105121 13:53 RKY Dibromofluoromethane 55 1 50.0 110 % 67-129 IK09032 EPA 8260D 11109121 22:25 RKY Toluene-d8 49 1 50.0 98 % 59-134 IK04051 EPA 6260D 11105121 13:53 RKY Toluene-d8 61 1 50.0 121 % 59-134 IK09032 EPA 6260D 11109121 22:25 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed gy Notes 1,4-Dioxane [123-91-1]^ 67 ug/L 1 0.80 2.0 1K02027 EPA 8260D 11/02/21 18:45 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed By Notes Toluene-d8 5.2 1 5.00 105 % 75-125 1K02027 EPA 8260D 11102121 18:45 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 14 of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW6 Lab Sample ID:CE13949-03 Received: 10/29/21 10:45 Matrix: Water Sampled:10/28/21 12:50 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY 1,1-Dichloroethane [75-34-3]A 7.2 ug/L 1 0.13 1.0 IK09032 EPA 8260D 11/10/21 01:12 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY 1,4-Dichlorobenzene [306-46-7]^ 1.7 ug/L 1 0.19 1.0 IK09032 EPA 8260D 11/10/21 01:12 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 1K09032 EPA 8260D 11/10/21 01:12 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 1K09032 EPA 8260D 11/10/21 01:12 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 1K09032 EPA 8260D 11/10/21 01:12 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 1K09032 EPA 8260D 11/10/21 01:12 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 1K09032 EPA 8260D 11/10/21 01:12 RKY Benzene [71-43-2]A 0.63 J ug/L 1 0.15 1.0 IK09032 EPA 8260D 11/10/21 01:12 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 1K09032 EPA 8260D 11/10/21 01:12 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY Chlorobenzene [108-90-7]A 3.2 ug/L 1 0.17 1.0 IK09032 EPA 8260D 11/10/21 01:12 RKY Chloroethane [75-00-3]A 1.8 ug/L 1 0.23 1.0 IK09032 EPA 8260D 11/10/21 01:12 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY cis-1,2-Dichloroethene [156-59-2]A 8.8 ug/L 1 0.15 1.0 IK09032 EPA 8260D 11/10/21 01:12 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY Ethylbenzene [500-41-4]^ 0.13 U ug/L 1 0.13 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 1K09032 EPA 8260D 11/10/21 01:12 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 1K09032 EPA 8260D 11/10/21 01:12 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY Tetrachloroethene [127-18-4]A 0.85 J ug/L 1 0.17 1.0 IK09032 EPA 8260D 11/10/21 01:12 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.41 J ug/L 1 0.21 1.0 IK09032 EPA 8260D 11/10/21 01:12 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY trans- l,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY Trichloroethene [79-01-6]A 2.0 ug/L 1 0.15 1.0 IK09032 EPA 8260D 11/10/21 01:12 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1K09032 EPA 8260D 11/10/21 01:12 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 15 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW6 Lab Sample ID:CE13949-03 Received: 10/29/21 10:45 Matrix: Water Sampled:10/28/21 12:50 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 2.2 ug/L 1 0.32 1.0 1K09032 EPA 8260D 11/10/21 01:12 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K09032 EPA 8260D 11/10/21 01:12 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 59 1 50.0 118 % 53-136 IK09032 EPA 6260D 11110121 01:12 RKY Dibromofluoromethane 55 1 50.0 110 % 67-129 IK09032 EPA 6260D 11110121 01:12 RKY Toluene-d8 61 1 50.0 121 % 59-134 IK09032 EPA 8260D 11110121 01:12 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 24 ug/L 1 0.80 2.0 1K02027 EPA 8260D 11/02/21 19:11 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 5.0 1 5.00 101 % 75-125 1K02027 EPA 8260D 11102121 19:11 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 16 of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW10 Lab Sample ID:CE13949-04 Received: 10/29/21 10:45 Matrix: Water Sampled:10/26/21 10:20 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY QV-01 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1K04051 EPA 8260D 11/05/21 14:22 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1K04051 EPA 8260D 11/05/21 14:22 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 1K04051 EPA 8260D 11/05/21 14:22 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1K04051 EPA 8260D 11/05/21 14:22 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Chlorobenzene[108-90-7]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Ethylbenzene[100-41-4]A 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1K04051 EPA 8260D 11/05/21 14:22 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY o-Xylene [95-47-6]A 0.065 u ug/L 1 0.065 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Styrene[100-42-5]A 0.11 u ug/L 1 0.11 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Vinyl acetate [108-05-4]A 0.95 Ll ug/L 1 0.95 5.0 1K04051 EPA 8260D 11/05/21 14:22 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 17 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW10 Lab Sample ID:CE13949-04 Received: 10/29/21 10:45 Matrix: Water Sampled:10/26/21 10:20 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K04051 EPA 8260D 11/05/21 14:22 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 50 1 50.0 100 % 53-136 1KO4051 EPA 6260D 11105121 14:22 RKY Dibromofluoromethane 50 1 50.0 99 % 67-129 IK04051 EPA 6260D 11105121 14:22 RKY Toluene-d8 49 1 50.0 98 % 59-134 IK04051 EPA 6260D 11105121 14:22 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 6.6 ug/L 1 0.80 2.0 1K02027 EPA 8260D 11/02/21 19:36 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 5.5 1 5.00 110 % 75-125 1K02027 EPA 8260D 11102121 19:36 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 18 of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW12A Lab Sample ID:CE13949-05 Received: 10/29/21 10:45 Matrix: Water Sampled:10/26/21 13:10 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY QV-01 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY 1,4-Dichlorobenzene [306-46-7]^ 1.7 ug/L 1 0.19 1.0 IK04051 EPA 8260D 11/05/21 14:52 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 1K04051 EPA 8260D 11/05/21 14:52 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 1K04051 EPA 8260D 11/05/21 14:52 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 1K04051 EPA 8260D 11/05/21 14:52 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 1K04051 EPA 8260D 11/05/21 14:52 RKY Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Chlorobenzene [108-90-7]^ 5.8 ug/L 1 0.17 1.0 IK04051 EPA 8260D 11/05/21 14:52 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Ethylbenzene[100-41-4]^ 0.13 U ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 1K04051 EPA 8260D 11/05/21 14:52 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Styrene[100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1K04051 EPA 8260D 11/05/21 14:52 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 19 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW12A Lab Sample ID:CE13949-05 Received: 10/29/21 10:45 Matrix: Water Sampled:10/26/21 13:10 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K04051 EPA 8260D 11/05/21 14:52 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 51 1 50.0 102 % 53-136 1KO4051 EPA 6260D 11105121 14:52 RKY Dibromofluoromethane 51 1 50.0 103 % 67-129 IK04051 EPA 6260D 11105121 14:52 RKY Toluene-d8 49 1 50.0 98 % 59-134 IK04051 EPA 6260D 11105121 14:52 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 180 D ug/L 5 4.0 10 1K02027 EPA 8260D 11/02/21 20:02 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 5.4 1 5.00 108 % 75-125 1K02027 EPA 8260D 11102121 20:02 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 20 of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW12B Lab Sample ID:CE13949-06 Received: 10/29/21 10:45 Matrix: Water Sampled:10/26/21 14:10 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 u ug/L 1 0.12 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 u ug/L 1 0.28 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY QV-01 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY 1,4-Dichlorobenzene [306-46-7]^ 2.2 ug/L 1 0.19 1.0 IK04051 EPA 8260D 11/05/21 15:21 RKY 2-Butanone [78-93-3]^ 1.3 u ug/L 1 1.3 5.0 1K04051 EPA 8260D 11/05/21 15:21 RKY 2-Hexanone [591-78-6]^ 0.88 u ug/L 1 0.88 5.0 1K04051 EPA 8260D 11/05/21 15:21 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Acetone [67-64-1]^ 10 u ug/L 1 10 20 1K04051 EPA 8260D 11/05/21 15:21 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1K04051 EPA 8260D 11/05/21 15:21 RKY Benzene[71-43-2]^ 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Bromochloromethane [74-97-5]^ 0.48 u ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Bromomethane [74-83-9]^ 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Carbon disulfide [75-15-0]^ 1.5 u ug/L 1 1.5 5.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Carbon tetrachloride [56-23-5]^ 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Chlorobenzene [108-90-7]^ 7.7 ug/L 1 0.17 1.0 IK04051 EPA 8260D 11/05/21 15:21 RKY Chloroethane [75-00-3]^ 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Chloromethane [74-87-3]^ 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 u ug/L 1 0.20 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Dibromochloromethane [124-48-1]^ 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Dibromomethane [74-95-3]^ 0.27 u ug/L 1 0.27 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Ethylbenzene[100-41-4]^ 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1K04051 EPA 8260D 11/05/21 15:21 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Methylene chloride [75-09-2]^ 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY o-Xylene [95-47-6]^ 0.065 u ug/L 1 0.065 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Styrene[100-42-5]^ 0.11 u ug/L 1 0.11 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Tetrachloroethene [127-18-4]^ 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 u ug/L 1 0.70 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Vinyl acetate [108-05-4]^ 0.95 Ll ug/L 1 0.95 5.0 1K04051 EPA 8260D 11/05/21 15:21 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 21 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW12B Lab Sample ID:CE13949-06 Received: 10/29/21 10:45 Matrix: Water Sampled:10/26/21 14:10 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K04051 EPA 8260D 11/05/21 15:21 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 50 1 50.0 101 % 53-136 IK04051 EPA 6260D 11/05/21 15:21 RKY Dibromofluoromethane 51 1 50.0 103 % 67-129 IK04051 EPA 6260D 11105121 15:21 RKY Toluene-d8 54 1 50.0 108 % 59-134 IK04051 EPA 8260D 11105121 15:21 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 110 D ug/L 5 4.0 10 1K02027 EPA 8260D 11/02/21 20:28 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 5.4 1 5.00 108 % 75-125 1K02027 EPA 8260D 11102121 20:28 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 22 of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW12D Lab Sample ID:CE13949-07 Received: 10/29/21 10:45 Matrix: Water Sampled:10/26/21 14:40 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY QV-01 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1K04051 EPA 8260D 11/05/21 15:51 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1K04051 EPA 8260D 11/05/21 15:51 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 1K04051 EPA 8260D 11/05/21 15:51 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1K04051 EPA 8260D 11/05/21 15:51 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Chlorobenzene[108-90-7]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Ethylbenzene[100-41-4]A 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1K04051 EPA 8260D 11/05/21 15:51 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY o-Xylene [95-47-6]A 0.065 u ug/L 1 0.065 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Styrene[100-42-5]A 0.11 u ug/L 1 0.11 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Vinyl acetate [108-05-4]A 0.95 Ll ug/L 1 0.95 5.0 1K04051 EPA 8260D 11/05/21 15:51 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 23 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW12D Lab Sample ID:CE13949-07 Received: 10/29/21 10:45 Matrix: Water Sampled:10/26/21 14:40 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K04051 EPA 8260D 11/05/21 15:51 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 50 1 50.0 99 % 53-136 1KO4051 EPA 6260D 11/05/21 15:51 RKY Dibromofluoromethane 52 1 50.0 103 % 67-129 IK04051 EPA 6260D 11105121 15:51 RKY Toluene-d8 50 1 50.0 100 % 59-134 IK04051 EPA 6260D 11105121 15:51 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 2.9 ug/L 1 0.80 2.0 1K02027 EPA 8260D 11/02/21 20:53 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.4 1 5.00 107 % 75-125 1K02027 EPA 8260D 11102121 20:53 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 24 of 81 00� www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW15A Lab Sample ID:CE13949-08 Received: 10/29/21 10:45 Matrix: Water Sampled: 10/28/2108:25 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 u ug/L 1 0.17 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 u ug/L 1 0.12 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 u ug/L 1 0.28 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 u ug/L 1 0.14 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.68 J ug/L 1 0.19 1.0 IK10033 EPA 8260D 11/11/21 03:17 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY 1,4-Dichlorobenzene [306-46-7]^ 1.9 ug/L 1 0.19 1.0 IK10033 EPA 8260D 11/11/21 03:17 RKY 2-Butanone [78-93-3]^ 1.3 u ug/L 1 1.3 5.0 lK10033 EPA 8260D 11/11/21 03:17 RKY 2-Hexanone [591-78-6]^ 0.88 u ug/L 1 0.88 5.0 lK10033 EPA 8260D 11/11/21 03:17 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Acetone [67-64-1]^ 10 u ug/L 1 10 20 lK10033 EPA 8260D 11/11/21 03:17 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 lK10033 EPA 8260D 11/11/21 03:17 RKY Benzene[71-43-2]^ 0.15 u ug/L 1 0.15 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Bromochloromethane [74-97-5]^ 0.48 u ug/L 1 0.48 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Bromomethane [74-83-9]^ 0.14 u ug/L 1 0.14 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Carbon disulfide [75-15-0]^ 1.5 u ug/L 1 1.5 5.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Carbon tetrachloride [56-23-5]^ 0.17 u ug/L 1 0.17 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Chlorobenzene [108-90-7]^ 60 ug/L 1 0.17 1.0 IK10033 EPA 8260D 11/11/21 03:17 RKY Chloroethane [75-00-3]^ 0.23 u ug/L 1 0.23 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Chloromethane [74-87-3]^ 0.13 u ug/L 1 0.13 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 u ug/L 1 0.20 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Dibromochloromethane [124-48-1]^ 0.17 u ug/L 1 0.17 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Dibromomethane [74-95-3]^ 0.27 u ug/L 1 0.27 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Ethylbenzene [100-41-4]^ 0.13 u ug/L 1 0.13 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 lK10033 EPA 8260D 11/11/21 03:17 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Methylene chloride [75-09-2]^ 0.23 u ug/L 1 0.23 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY o-Xylene [95-47-6]^ 0.065 u ug/L 1 0.065 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Styrene[100-42-5]^ 0.11 u ug/L 1 0.11 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Tetrachloroethene [127-18-4]^ 0.17 u ug/L 1 0.17 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 u ug/L 1 0.15 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 u ug/L 1 0.70 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 lK10033 EPA 8260D 11/11/21 03:17 RKY Vinyl acetate [108-05-4]^ 0.95 Ll ug/L 1 0.95 5.0 lK10033 EPA 8260D 11/11/21 03:17 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 25 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW15A Lab Sample ID:CE13949-08 Received: 10/29/21 10:45 Matrix: Water Sampled: 10/28/2108:25 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K10033 EPA 8260D 11/11/21 03:17 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K10033 EPA 8260D 11/11/21 03:17 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 58 1 50.0 116 % 53-136 IK10033 EPA 6260D 11111121 03:17 RKY Dibromofluoromethane 54 1 50.0 109 % 67-129 IK10033 EPA 6260D 11111121 03:17 RKY Toluene-d8 60 1 50.0 120 % 59-134 IK10033 EPA 8260D 11111121 03:17 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1200 D ug/L 100 80 200 1K02042 EPA 8260D 11/03/21 02:01 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 5.1 1 5.00 103 % 75-125 1K02042 EPA 8260D 11103121 02:01 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 26 of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-OWDR2 Lab Sample ID:CE13949-09 Received: 10/29/21 10:45 Matrix: Water Sampled: 10/28/2109:45 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.85 LID ug/L 5 0.85 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY 1,1,1-Trichloroethane [71-55-6]A 5.2 D ug/L 5 0.60 5.0 IK09032 EPA 8260D 11/10/21 02:08 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 1.4 LID ug/L 5 1.4 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY 1,1,2-Trichloroethane [79-00-5]A 0.70 LID ug/L 5 0.70 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY 1.1-Dichloroethane [75-34-3]A 130 D ug/L 5 0.65 5.0 IK09032 EPA 8260D 11/10/21 02:08 RKY 1.1-Dichloroethene [75-35-4]A 54 D ug/L 5 1.0 5.0 IK09032 EPA 8260D 11/10/21 02:08 RKY 1,2,3-Trichloropropane [96-18-4]A 1.2 LID ug/L 5 1.2 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 2.4 LID ug/L 5 2.4 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY 1,2-Dibromoethane [106-93-4]A 3.3 LID ug/L 5 3.3 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY 1,2-Dichlorobenzene [95-50-1]A 0.95 LID ug/L 5 0.95 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY 1.2-Dichloroethane [107-06-2]A 6.0 D ug/L 5 1.0 5.0 IK09032 EPA 8260D 11/10/21 02:08 RKY 1,2-Dichloropropane [78-87-5]A 0.50 LID ug/L 5 0.50 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY 1,4-Dichlorobenzene [106-46-7]A 0.95 LID ug/L 5 0.95 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY 2-Butanone [78-93-3]A 6.5 LID ug/L 5 6.5 25 1K09032 EPA 8260D 11/10/21 02:08 RKY 2-Hexanone [591-78-6]A 4.4 LID ug/L 5 4.4 25 1K09032 EPA 8260D 11/10/21 02:08 RKY 4-Methyl-2-pentanone [108-10-1]A 5.5 LID ug/L 5 5.5 25 1K09032 EPA 8260D 11/10/21 02:08 RKY Acetone [67-64-1]A 50 LID ug/L 5 50 100 1K09032 EPA 8260D 11/10/21 02:08 RKY Acrylonitrile [107-13-1]A 18 LID ug/L 5 18 50 1K09032 EPA 8260D 11/10/21 02:08 RKY Benzene[71-43-2]A 0.75 LID ug/L 5 0.75 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY Bromochloromethane [74-97-5]A 2.4 LID ug/L 5 2.4 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY Bromodichloromethane [75-27-4]A 0.85 LID ug/L 5 0.85 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY Bromoform [75-25-2]A 1.1 LID ug/L 5 1.1 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY Bromomethane [74-83-9]A 0.70 LID ug/L 5 0.70 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY Carbon disulfide [75-15-0]A 7.5 LID ug/L 5 7.5 25 1K09032 EPA 8260D 11/10/21 02:08 RKY Carbon tetrachloride [56-23-5]A 0.85 LID ug/L 5 0.85 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY Chlorobenzene [108-90-7]A 36 D ug/L 5 0.85 5.0 IK09032 EPA 8260D 11/10/21 02:08 RKY Chloroethane [75-00-3]A 11 D ug/L 5 1.2 5.0 IK09032 EPA 8260D 11/10/21 02:08 RKY Chloroform [67-66-3]A 0.90 LID ug/L 5 0.90 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY Chloromethane [74-87-3]A 0.65 LID ug/L 5 0.65 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY cis-1,2-Dichloroethene [156-59-2]A 230 D ug/L 5 0.75 5.0 IK09032 EPA 8260D 11/10/21 02:08 RKY cis-1,3-Dichloropropene [10061-01-5]A 1.0 LID ug/L 5 1.0 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY Dibromochloromethane [124-48-1]A 0.85 LID ug/L 5 0.85 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY Dibromomethane [74-95-3]A 1.4 LID ug/L 5 1.4 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY Ethylbenzene [100-41-4]A 0.65 LID ug/L 5 0.65 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY Iodomethane[74-88-4]A 8.5 LID ug/L 5 8.5 25 1K09032 EPA 8260D 11/10/21 02:08 RKY m,p-Xylenes[108-38-3/106-42-3]A 0.85 LID ug/L 5 0.85 10 1K09032 EPA 8260D 11/10/21 02:08 RKY Methylene chloride [75-09-2]A 1.2 LID ug/L 5 1.2 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY o-Xylene [95-47-6]A 0.32 LID ug/L 5 0.32 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY Styrene[100-42-5]A 0.55 LID ug/L 5 0.55 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY Tetrachloroethene [127-18-4]A 0.85 LID ug/L 5 0.85 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY Toluene [108-88-3]A 0.70 LID ug/L 5 0.70 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY trans-1,2-Dichloroethene [156-60-5]A 1.0 LID ug/L 5 1.0 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.75 LID ug/L 5 0.75 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 3.5 LID ug/L 5 3.5 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY Trichloroethene [79-01-6]A 0.75 LID ug/L 5 0.75 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY Trichlorofluoromethane [75-69-4]A 1.2 LID ug/L 5 1.2 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY Vinyl acetate [108-05-4]A 4.8 LID ug/L 5 4.8 25 1K09032 EPA 8260D 11/10/21 02:08 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 27 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-OWDR2 Lab Sample ID:CE13949-09 Received: 10/29/21 10:45 Matrix: Water Sampled: 10/28/2109:45 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 20 D ug/L 5 1.6 5.0 1K09032 EPA 8260D 11/10/21 02:08 RKY Xylenes (Total) [1330-20-7]^ 2.2 UD ug/L 5 2.2 15 1K09032 EPA 8260D 11/10/21 02:08 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 60 1 50.0 119 % 53-136 IK09032 EPA 6260D 11110121 02:08 RKY Dibromofluoromethane 55 1 50.0 110 % 67-129 IK09032 EPA 6260D 11110121 02:08 RKY Toluene-d8 61 1 50.0 122 % 59-134 IK09032 EPA 8260D 11110121 02:08 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 250 D ug/L 25 20 50 1K02042 EPA 8260D 11/03/21 02:26 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 5.3 1 5.00 106 % 75-125 1K02042 EPA 8260D 11103121 02:26 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 28 Of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-OWLFS2 Lab Sample ID:CE13949-10 Received: 10/29/21 10:45 Matrix: Water Sampled:10/28/21 12:15 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 u ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 u ug/L 1 0.12 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 u ug/L 1 0.28 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 u ug/L 1 0.14 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY 1,1-Dichloroethane [75-34-3]A 0.79 J ug/L 1 0.13 1.0 IK09032 EPA 8260D 11/10/21 02:35 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY 2-Butanone [78-93-3]^ 1.3 u ug/L 1 1.3 5.0 1K09032 EPA 8260D 11/10/21 02:35 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1K09032 EPA 8260D 11/10/21 02:35 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Acetone [67-64-1]^ 10 u ug/L 1 10 20 1K09032 EPA 8260D 11/10/21 02:35 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1K09032 EPA 8260D 11/10/21 02:35 RKY Benzene [71-43-2]A 7.0 ug/L 1 0.15 1.0 IK09032 EPA 8260D 11/10/21 02:35 RKY Bromochloromethane [74-97-5]^ 0.48 u ug/L 1 0.48 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Bromomethane [74-83-9]^ 0.14 u ug/L 1 0.14 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Carbon tetrachloride [56-23-5]^ 0.17 u ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Chlorobenzene [108-90-7]A 3.8 ug/L 1 0.17 1.0 IK09032 EPA 8260D 11/10/21 02:35 RKY Chloroethane [75-00-3]A 1.3 ug/L 1 0.23 1.0 IK09032 EPA 8260D 11/10/21 02:35 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Chloromethane [74-87-3]^ 0.13 u ug/L 1 0.13 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Dibromochloromethane [124-48-1]^ 0.17 u ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Dibromomethane [74-95-3]^ 0.27 u ug/L 1 0.27 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Ethylbenzene[100-41-4]^ 0.13 u ug/L 1 0.13 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1K09032 EPA 8260D 11/10/21 02:35 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY o-Xylene [95-47-6]A 0.065 u ug/L 1 0.065 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Styrene[100-42-5]^ 0.11 u ug/L 1 0.11 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Tetrachloroethene [127-18-4]^ 0.17 u ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 u ug/L 1 0.70 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Vinyl acetate [108-05-4]^ 0.95 Ll ug/L 1 0.95 5.0 1K09032 EPA 8260D 11/10/21 02:35 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 29 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-OWLFS2 Lab Sample ID:CE13949-10 Received: 10/29/21 10:45 Matrix: Water Sampled:10/28/21 12:15 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 1.4 ug/L 1 0.32 1.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K09032 EPA 8260D 11/10/21 02:35 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 61 1 50.0 122 % 53-136 IK09032 EPA 6260D 11110121 02:35 RKY Dibromofluoromethane 56 1 50.0 113 % 67-129 IK09032 EPA 6260D 11110121 02:35 RKY Toluene-d8 62 1 50.0 124 % 59-134 IK09032 EPA 8260D 11110121 02:35 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 270 D ug/L 10 8.0 20 1K02042 EPA 8260D 11/03/21 02:52 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.4 1 5.00 107 % 75-125 1K02042 EPA 8260D 11103121 02:52 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 30 Of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW3D Lab Sample ID:CE13949-11 Received: 10/29/21 10:45 Matrix: Water Sampled:10/27/21 14:15 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 85 LID ug/L 500 85 500 1KO5042 EPA 8260D 11/06/21 18:40 RKY 1,1,1-Trichloroethane [71-55-6]A 890 D ug/L 500 60 500 IK05042 EPA 8260D 11/06/21 18:40 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 140 LID ug/L 500 140 500 1KO5042 EPA 8260D 11/06/21 18:40 RKY 1,1,2-Trichloroethane [79-00-5]^ 70 LID ug/L 500 70 500 1KO5042 EPA 8260D 11/06/21 18:40 RKY 1,1-Dichloroethane [75-34-3]A 660 D ug/L 500 65 500 IK05042 EPA 8260D 11/06/21 18:40 RKY 1,1-Dichloroethene [75-35-4]A 1500 D ug/L 500 100 500 IK05042 EPA 8260D 11/06/21 18:40 RKY 1,2,3-Trichloropropane [96-18-4]^ 120 LID ug/L 500 120 500 1KO5042 EPA 8260D 11/06/21 18:40 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 240 LID ug/L 500 240 500 1K05042 EPA 8260D 11/06/21 18:40 RKY 1,2-Dibromoethane[106-93-4]^ 330 LID ug/L 500 330 500 1K05042 EPA 8260D 11/06/21 18:40 RKY 1,2-Dichlorobenzene [95-50-1]^ 95 LID ug/L 500 95 500 1KO5042 EPA 8260D 11/06/21 18:40 RKY 1,2-Dichloroethane [107-06-2]A 17000 D ug/L 500 100 500 IK05042 EPA 8260D 11/06/21 18:40 RKY 1,2-Dichloropropane [78-87-5]^ 50 LID ug/L 500 50 500 1KO5042 EPA 8260D 11/06/21 18:40 RKY 1,4-Dichlorobenzene [106-46-7]^ 95 LID ug/L 500 95 500 1K05042 EPA 8260D 11/06/21 18:40 RKY 2-Butanone [78-93-3]^ 650 LID ug/L 500 650 2500 1K05042 EPA 8260D 11/06/21 18:40 RKY 2-Hexanone [591-78-6]^ 440 LID ug/L 500 440 2500 1K05042 EPA 8260D 11/06/21 18:40 RKY 4-Methyl-2-pentanone [108-10-1]^ 550 LID ug/L 500 550 2500 1K05042 EPA 8260D 11/06/21 18:40 RKY Acetone [67-64-1]^ 5000 LID ug/L 500 5000 10000 1K05042 EPA 8260D 11/06/21 18:40 RKY Acrylonitrile [107-13-1]^ 1800 LID ug/L 500 1800 5000 1K05042 EPA 8260D 11/06/21 18:40 RKY Benzene [71-43-2]A 280 ]D ug/L 500 75 500 IK05042 EPA 8260D 11/06/21 18:40 RKY Bromochloromethane [74-97-5]^ 240 LID ug/L 500 240 500 1K05042 EPA 8260D 11/06/21 18:40 RKY QV-01 Bromodichloromethane [75-27-4]^ 85 LID ug/L 500 85 500 1K05042 EPA 8260D 11/06/21 18:40 RKY Bromoform [75-25-2]^ 110 LID ug/L 500 110 500 1K05042 EPA 8260D 11/06/21 18:40 RKY Bromomethane[74-83-9]^ 70 LID ug/L 500 70 500 1K05042 EPA 8260D 11/06/21 18:40 RKY Carbon disulfide [75-15-0]^ 750 LID ug/L 500 750 2500 1K05042 EPA 8260D 11/06/21 18:40 RKY Carbon tetrachloride [56-23-5]^ 85 LID ug/L 500 85 500 1K05042 EPA 8260D 11/06/21 18:40 RKY QV-01 Chlorobenzene [108-90-7]A 18000 D ug/L 500 85 500 IK05042 EPA 8260D 11/06/21 18:40 RKY Chloroethane [75-00-3]^ 120 UD ug/L 500 120 500 1K05042 EPA 8260D 11/06/21 18:40 RKY Chloroform [67-66-3]^ 90 LID ug/L 500 90 500 1KO5042 EPA 8260D 11/06/21 18:40 RKY Chloromethane [74-87-3]^ 65 LID ug/L 500 65 500 1KO5042 EPA 8260D 11/06/21 18:40 RKY cis-1,2-Dichloroethene [156-59-2]A 380 JD ug/L 500 75 500 IK05042 EPA 8260D 11/06/21 18:40 RKY cis-1,3-Dichloropropene [10061-01-5]^ 100 LID ug/L 500 100 500 1K05042 EPA 8260D 11/06/21 18:40 RKY Dibromochloromethane [124-48-1]^ 85 LID ug/L 500 85 500 1K05042 EPA 8260D 11/06/21 18:40 RKY Dibromomethane [74-95-3]^ 140 LID ug/L 500 140 500 1K05042 EPA 8260D 11/06/21 18:40 RKY Ethylbenzene[100-41-4]^ 65 LID ug/L 500 65 500 1K05042 EPA 8260D 11/06/21 18:40 RKY Iodomethane[74-88-4]^ 850 LID ug/L 500 850 2500 1K05042 EPA 8260D 11/06/21 18:40 RKY m,p-Xylenes[108-38-3/106-42-3]^ 85 LID ug/L 500 85 1000 1K05042 EPA 8260D 11/06/21 18:40 RKY Methylene chloride [75-09-2]^ 1800 D ug/L 500 120 500 1K05042 EPA 8260D 11/06/21 18:40 RKY o-Xylene [95-47-6]^ 32 LID ug/L 500 32 500 1K05042 EPA 8260D 11/06/21 18:40 RKY Styrene [100-42-5]^ 55 LID ug/L 500 55 500 1K05042 EPA 8260D 11/06/21 18:40 RKY Tetrachloroethene [127-18-4]^ 1200 D ug/L 500 85 500 IK05042 EPA 8260D 11/06/21 18:40 RKY Toluene [108-88-3]A 670 D ug/L 500 70 500 IK05042 EPA 8260D 11/06/21 18:40 RKY trans-1,2-Dichloroethene [156-60-5]^ 100 LID ug/L 500 100 500 1KO5042 EPA 8260D 11/06/21 18:40 RKY trans-1,3-Dichloropropene [10061-02-6]^ 75 LID ug/L 500 75 500 1KO5042 EPA 8260D 11/06/21 18:40 RKY trans- l,4-Dichloro-2-butene [110-57-6]^ 350 LID ug/L 500 350 500 1KO5042 EPA 8260D 11/06/21 18:40 RKY Trichloroethene [79-01-6]A 4200 D ug/L 500 75 500 IK09032 EPA 8260D 11/10/21 00:44 RKY Trichlorofluoromethane [75-69-4]^ 120 LID ug/L 500 120 500 1K05042 EPA 8260D 11/06/21 18:40 RKY Vinyl acetate[108-05-4]^ 480 LID ug/L 500 480 2500 1K05042 EPA 8260D 11/06/21 18:40 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 31 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW3D Lab Sample ID:CE13949-11 Received: 10/29/21 10:45 Matrix: Water Sampled:10/27/21 14:15 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 160 UD ug/L 500 160 500 1K05042 EPA 8260D 11/06/21 18:40 RKY Xylenes (Total) [1330-20-7]^ 220 UD ug/L 500 220 1500 1K05042 EPA 8260D 11/06/21 18:40 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 50 1 50.0 99 % 53-136 IK05042 EPA 6260D 11106121 16:40 RKY 4-Bromofluorobenzene 59 1 50.0 118 % 53-136 IK09032 EPA 6260D 11110121 00:44 RKY Dibromofluoromethane 48 1 50.0 96 % 67-129 IK05042 EPA 6260D 11106121 16:40 RKY Dibromofluoromethane 54 1 50.0 108 % 67-129 IK09032 EPA 6260D 11110121 00:44 RKY Toluene-d8 49 1 50.0 98 % 59-134 IK05042 EPA 8260D 11106121 16:40 RKY Toluene-d8 60 1 50.0 119 % 59-134 IK09032 EPA 6260D 11110121 00:44 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed gy Notes 1,4-Dioxane [123-91-1]^ 160 D ug/L 5 4.0 10 1K02042 EPA 8260D 11/03/21 03:18 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed By Notes Toluene-d8 6.1 1 5.00 121 % 75-125 1K02042 EPA 8260D 11103121 03:18 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 32 of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW5D Lab Sample ID:CE13949-12 Received: 10/29/21 10:45 Matrix: Water Sampled:10/28/21 10:40 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 1.7 LID ug/L 10 1.7 10 1K09032 EPA 8260D 11/10/21 03:03 RKY 1,1,1-Trichloroethane [71-55-6]A 7.6 ID ug/L 10 1.2 10 IK09032 EPA 8260D 11/10/21 03:03 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 2.8 LID ug/L 10 2.8 10 1K09032 EPA 8260D 11/10/21 03:03 RKY 1,1,2-Trichloroethane [79-00-5]A 1.4 LID ug/L 10 1.4 10 1K09032 EPA 8260D 11/10/21 03:03 RKY 1.1-Dichloroethane [75-34-3]A 200 D ug/L 10 1.3 10 IK09032 EPA 8260D 11/10/21 03:03 RKY 1.1-Dichloroethene [75-35-4]A 4.3 ID ug/L 10 2.1 10 IK09032 EPA 8260D 11/10/21 03:03 RKY 1,2,3-Trichloropropane [96-18-4]A 2.3 LID ug/L 10 2.3 10 1K09032 EPA 8260D 11/10/21 03:03 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 4.8 LID ug/L 10 4.8 10 1K09032 EPA 8260D 11/10/21 03:03 RKY 1,2-Dibromoethane [106-93-4]A 6.6 LID ug/L 10 6.6 10 1K09032 EPA 8260D 11/10/21 03:03 RKY 1,2-Dichlorobenzene [95-50-1]A 1.9 LID ug/L 10 1.9 10 1K09032 EPA 8260D 11/10/21 03:03 RKY 1,2-Dichloroethane [107-06-2]A 15 D ug/L 10 2.1 10 IK09032 EPA 8260D 11/10/21 03:03 RKY 1,2-Dichloropropane [78-87-5]A 1.0 LID ug/L 10 1.0 10 1K09032 EPA 8260D 11/10/21 03:03 RKY 1,4-Dichlorobenzene [106-46-7]A 1.9 LID ug/L 10 1.9 10 1K09032 EPA 8260D 11/10/21 03:03 RKY 2-Butanone [78-93-3]A 13 LID ug/L 10 13 50 1K09032 EPA 8260D 11/10/21 03:03 RKY 2-Hexanone [591-78-6]A 8.8 LID ug/L 10 8.8 50 1K09032 EPA 8260D 11/10/21 03:03 RKY 4-Methyl-2-pentanone [108-10-1]A 11 LID ug/L 10 11 50 1K09032 EPA 8260D 11/10/21 03:03 RKY Acetone [67-64-1]A 100 LID ug/L 10 100 200 1K09032 EPA 8260D 11/10/21 03:03 RKY Acrylonitrile [107-13-1]A 35 LID ug/L 10 35 100 1K09032 EPA 8260D 11/10/21 03:03 RKY Benzene [71-43-2]A 5.4 ID ug/L 10 1.5 10 IK09032 EPA 8260D 11/10/21 03:03 RKY Bromochloromethane [74-97-5]A 4.8 LID ug/L 10 4.8 10 1K09032 EPA 8260D 11/10/21 03:03 RKY Bromodichloromethane [75-27-4]A 1.7 LID ug/L 10 1.7 10 1K09032 EPA 8260D 11/10/21 03:03 RKY Bromoform [75-25-2]A 2.2 LID ug/L 10 2.2 10 1K09032 EPA 8260D 11/10/21 03:03 RKY Bromomethane [74-83-9]A 1.4 LID ug/L 10 1.4 10 1K09032 EPA 8260D 11/10/21 03:03 RKY Carbon disulfide [75-15-0]A 15 LID ug/L 10 15 50 1K09032 EPA 8260D 11/10/21 03:03 RKY Carbon tetrachloride [56-23-5]A 1.7 LID ug/L 10 1.7 10 1K09032 EPA 8260D 11/10/21 03:03 RKY Chlorobenzene [108-90-7]A 180 D ug/L 10 1.7 10 IK09032 EPA 8260D 11/10/21 03:03 RKY Chloroethane [75-00-3]A 2.3 LID ug/L 10 2.3 10 1K09032 EPA 8260D 11/10/21 03:03 RKY Chloroform [67-66-3]A 1.8 LID ug/L 10 1.8 10 1K09032 EPA 8260D 11/10/21 03:03 RKY Chloromethane [74-87-3]A 1.3 LID ug/L 10 1.3 10 1K09032 EPA 8260D 11/10/21 03:03 RKY cis-1,2-Dichloroethene [156-59-2]A 12 D ug/L 10 1.5 10 1K09032 EPA 8260D 11/10/21 03:03 RKY cis-1,3-Dichloropropene [10061-01-5]A 2.0 LID ug/L 10 2.0 10 1K09032 EPA 8260D 11/10/21 03:03 RKY Dibromochloromethane [124-48-1]A 1.7 LID ug/L 10 1.7 10 1K09032 EPA 8260D 11/10/21 03:03 RKY Dibromomethane [74-95-3]A 2.7 LID ug/L 10 2.7 10 1K09032 EPA 8260D 11/10/21 03:03 RKY Ethylbenzene [100-41-4]A 1.3 LID ug/L 10 1.3 10 1K09032 EPA 8260D 11/10/21 03:03 RKY Iodomethane[74-88-4]A 17 LID ug/L 10 17 50 1K09032 EPA 8260D 11/10/21 03:03 RKY m,p-Xylenes[108-38-3/106-42-3]A 1.7 LID ug/L 10 1.7 20 1K09032 EPA 8260D 11/10/21 03:03 RKY Methylene chloride [75-09-2]A 2.3 LID ug/L 10 2.3 10 1K09032 EPA 8260D 11/10/21 03:03 RKY o-Xylene [95-47-6]A 0.65 LID ug/L 10 0.65 10 1K09032 EPA 8260D 11/10/21 03:03 RKY Styrene[100-42-5]A 1.1 LID ug/L 10 1.1 10 1K09032 EPA 8260D 11/10/21 03:03 RKY Tetrachloroethene [127-18-4]A 1.7 LID ug/L 10 1.7 10 1K09032 EPA 8260D 11/10/21 03:03 RKY Toluene [108-88-3]A 1.4 LID ug/L 10 1.4 10 1K09032 EPA 8260D 11/10/21 03:03 RKY trans-1,2-Dichloroethene [156-60-5]A 2.1 LID ug/L 10 2.1 10 1K09032 EPA 8260D 11/10/21 03:03 RKY trans-1,3-Dichloropropene [10061-02-6]A 1.5 LID ug/L 10 1.5 10 1K09032 EPA 8260D 11/10/21 03:03 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 7.0 LID ug/L 10 7.0 10 1K09032 EPA 8260D 11/10/21 03:03 RKY Trichloroethene [79-01-6]A 1.5 LID ug/L 10 1.5 10 1K09032 EPA 8260D 11/10/21 03:03 RKY Trichlorofluoromethane [75-69-4]A 2.4 LID ug/L 10 2.4 10 1K09032 EPA 8260D 11/10/21 03:03 RKY Vinyl acetate [108-05-4]A 9.5 LID ug/L 10 9.5 50 1K09032 EPA 8260D 11/10/21 03:03 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 33 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW5D Lab Sample ID:CE13949-12 Received: 10/29/21 10:45 Matrix: Water Sampled:10/28/21 10:40 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 9.5 JD ug/L 10 3.2 10 1K09032 EPA 8260D 11/10/21 03:03 RKY Xylenes (Total) [1330-20-7]^ 4.5 UD ug/L 10 4.5 30 1K09032 EPA 8260D 11/10/21 03:03 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 59 1 50.0 118 % 53-136 1KO9032 EPA 6260D 11110121 03:03 RKY Dibromofluoromethane 55 1 50.0 110 % 67-129 IK09032 EPA 6260D 11110121 03:03 RKY Toluene-d8 62 1 50.0 123 % 59-134 IK09032 EPA 8260D 11110121 03:03 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 400 D ug/L 50 40 100 1K02042 EPA 8260D 11/03/21 03:44 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 5.0 1 5.00 100 % 75-125 1K02042 EPA 8260D 11103121 03:44 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 34 of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW4I Lab Sample ID:CE13949-13 Received: 10/29/21 10:45 Matrix: Water Sampled:10/27/21 15:05 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.85 LID ug/L 5 0.85 5.0 1KO5042 EPA 8260D 11/06/21 19:09 RKY 1,1,1-Trichloroethane [71-55-6]A 26 D ug/L 5 0.60 5.0 IK05042 EPA 8260D 11/06/21 19:09 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 1.4 LID ug/L 5 1.4 5.0 1KO5042 EPA 8260D 11/06/21 19:09 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.70 LID ug/L 5 0.70 5.0 1KO5042 EPA 8260D 11/06/21 19:09 RKY 1.1-Dichloroethane [75-34-3]A 43 D ug/L 5 0.65 5.0 IK05042 EPA 8260D 11/06/21 19:09 RKY 1.1-Dichloroethene [75-35-4]A 32 D ug/L 5 1.0 5.0 IK05042 EPA 8260D 11/06/21 19:09 RKY 1,2,3-Trichloropropane [96-18-4]^ 1.2 LID ug/L 5 1.2 5.0 1KO5042 EPA 8260D 11/06/21 19:09 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 2.4 LID ug/L 5 2.4 5.0 1K05042 EPA 8260D 11/06/21 19:09 RKY 1,2-Dibromoethane [106-93-4]^ 3.3 LID ug/L 5 3.3 5.0 1K05042 EPA 8260D 11/06/21 19:09 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.95 LID ug/L 5 0.95 5.0 1KO5042 EPA 8260D 11/06/21 19:09 RKY 1.2-Dichloroethane [107-06-2]A 22 D ug/L 5 1.0 5.0 IK05042 EPA 8260D 11/06/21 19:09 RKY 1,2-Dichloropropane [78-87-5]^ 0.50 LID ug/L 5 0.50 5.0 1KO5042 EPA 8260D 11/06/21 19:09 RKY 1.4-Dichlorobenzene [106-46-7]A 2.6 ID ug/L 5 0.95 5.0 IK05042 EPA 8260D 11/06/21 19:09 RKY 2-Butanone [78-93-3]^ 6.5 LID ug/L 5 6.5 25 1K05042 EPA 8260D 11/06/21 19:09 RKY 2-Hexanone [591-78-6]^ 4.4 LID ug/L 5 4.4 25 1K05042 EPA 8260D 11/06/21 19:09 RKY 4-Methyl-2-pentanone [108-10-1]^ 5.5 LID ug/L 5 5.5 25 1K05042 EPA 8260D 11/06/21 19:09 RKY Acetone [67-64-1]^ 50 LID ug/L 5 50 100 1K05042 EPA 8260D 11/06/21 19:09 RKY Acrylonitrile [107-13-1]^ 18 LID ug/L 5 18 50 1K05042 EPA 8260D 11/06/21 19:09 RKY Benzene [71-43-2]A 2.1 ID ug/L 5 0.75 5.0 IK05042 EPA 8260D 11/06/21 19:09 RKY Bromochloromethane [74-97-5]^ 2.4 LID ug/L 5 2.4 5.0 1K05042 EPA 8260D 11/06/21 19:09 RKY QV-01 Bromodichloromethane [75-27-4]^ 0.85 LID ug/L 5 0.85 5.0 1K05042 EPA 8260D 11/06/21 19:09 RKY Bromoform [75-25-2]^ 1.1 LID ug/L 5 1.1 5.0 1K05042 EPA 8260D 11/06/21 19:09 RKY Bromomethane [74-83-9]^ 0.70 LID ug/L 5 0.70 5.0 1K05042 EPA 8260D 11/06/21 19:09 RKY Carbon disulfide [75-15-0]^ 7.5 LID ug/L 5 7.5 25 1K05042 EPA 8260D 11/06/21 19:09 RKY Carbon tetrachloride [56-23-5]^ 0.85 LID ug/L 5 0.85 5.0 1K05042 EPA 8260D 11/06/21 19:09 RKY QV-01 Chlorobenzene [108-90-7]A 60 D ug/L 5 0.85 5.0 IK05042 EPA 8260D 11/06/21 19:09 RKY Chloroethane [75-00-3]^ 1.2 LID ug/L 5 1.2 5.0 1K05042 EPA 8260D 11/06/21 19:09 RKY Chloroform [67-66-3]^ 0.90 LID ug/L 5 0.90 5.0 1KO5042 EPA 8260D 11/06/21 19:09 RKY Chloromethane [74-87-3]^ 0.65 LID ug/L 5 0.65 5.0 1KO5042 EPA 8260D 11/06/21 19:09 RKY cis-1,2-Dichloroethene [156-59-2]A 170 D ug/L 5 0.75 5.0 IK05042 EPA 8260D 11/06/21 19:09 RKY cis-1,3-Dichloropropene [10061-01-5]^ 1.0 LID ug/L 5 1.0 5.0 1K05042 EPA 8260D 11/06/21 19:09 RKY Dibromochloromethane [124-48-1]^ 0.85 LID ug/L 5 0.85 5.0 1K05042 EPA 8260D 11/06/21 19:09 RKY Dibromomethane [74-95-3]^ 1.4 LID ug/L 5 1.4 5.0 1K05042 EPA 8260D 11/06/21 19:09 RKY Ethylbenzene [100-41-4]^ 0.65 LID ug/L 5 0.65 5.0 1K05042 EPA 8260D 11/06/21 19:09 RKY Iodomethane[74-88-4]^ 8.5 LID ug/L 5 8.5 25 1K05042 EPA 8260D 11/06/21 19:09 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.85 LID ug/L 5 0.85 10 1K05042 EPA 8260D 11/06/21 19:09 RKY Methylene chloride [75-09-2]^ 2.2 ID ug/L 5 1.2 5.0 IK05042 EPA 8260D 11/06/21 19:09 RKY o-Xylene [95-47-6]^ 0.32 LID ug/L 5 0.32 5.0 1K05042 EPA 8260D 11/06/21 19:09 RKY Styrene[100-42-5]^ 0.55 LID ug/L 5 0.55 5.0 1KO5042 EPA 8260D 11/06/21 19:09 RKY Tetrachloroethene [127-18-4]A 12 D ug/L 5 0.85 5.0 IK05042 EPA 8260D 11/06/21 19:09 RKY Toluene [108-88-3]^ 0.70 LID ug/L 5 0.70 5.0 1K05042 EPA 8260D 11/06/21 19:09 RKY trans-1,2-Dichloroethene [156-60-5]^ 1.0 LID ug/L 5 1.0 5.0 1K05042 EPA 8260D 11/06/21 19:09 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.75 LID ug/L 5 0.75 5.0 1K05042 EPA 8260D 11/06/21 19:09 RKY trans- l,4-Dichloro-2-butene [110-57-6]^ 3.5 LID ug/L 5 3.5 5.0 1K05042 EPA 8260D 11/06/21 19:09 RKY Trichloroethene [79-01-6]A 41 D ug/L 5 0.75 5.0 IK09032 EPA 8260D 11/10/21 00:16 RKY Trichlorofluoromethane [75-69-4]^ 1.2 LID ug/L 5 1.2 5.0 1K05042 EPA 8260D 11/06/21 19:09 RKY Vinyl acetate [108-05-4]^ 4.8 LID ug/L 5 4.8 25 1K05042 EPA 8260D 11/06/21 19:09 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 35 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW4I Lab Sample ID:CE13949-13 Received: 10/29/21 10:45 Matrix: Water Sampled:10/27/21 15:05 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 33 D ug/L 5 1.6 5.0 1K05042 EPA 8260D 11/06/21 19:09 RKY Xylenes (Total) [1330-20-7]^ 2.2 UD ug/L 5 2.2 15 1K05042 EPA 8260D 11/06/21 19:09 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 50 1 50.0 101 % 53-136 IK05042 EPA 6260D 11106121 19:09 RKY 4-Bromofluorobenzene 60 1 50.0 120 % 53-136 IK09032 EPA 6260D 11110121 00:16 RKY Dibromofluoromethane 50 1 50.0 100 % 67-129 IK05042 EPA 8260D 11106121 19:09 RKY Dibromofluoromethane 55 1 50.0 110 % 67-129 IK09032 EPA 8260D 11110121 00:16 RKY Toluene-d8 48 1 50.0 96 % 59-134 IK05042 EPA 6260D 11106121 19:09 RKY Toluene-d8 61 1 50.0 122 % 59-134 IK09032 EPA 6260D 11110121 00:16 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed gy Notes 1,4-Dioxane [123-91-1]^ 160 D ug/L 10 8.0 20 1K02042 EPA 8260D 11/03/21 04:09 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed By Notes Toluene-d8 5.1 1 5.00 102 % 75-125 1K02042 EPA 8260D 11103121 04:09 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 36 of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW6I Lab Sample ID:CE13949-14 Received: 10/29/21 10:45 Matrix: Water Sampled:10/28/21 11:45 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY 1,1-Dichloroethane [75-34-3]A 11 ug/L 1 0.13 1.0 IK09032 EPA 8260D 11/10/21 03:31 RKY 1,1-Dichloroethene [75-35-4]A 0.74 J ug/L 1 0.21 1.0 IK09032 EPA 8260D 11/10/21 03:31 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY 1,2-Dichloroethane [107-06-2]A 2.1 ug/L 1 0.21 1.0 IK09032 EPA 8260D 11/10/21 03:31 RKY 1,2-Dichloropropane [78-87-5]A 0.10 U ug/L 1 0.10 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY 1,4-Dichlorobenzene [106-46-7]A 2.0 ug/L 1 0.19 1.0 IK09032 EPA 8260D 11/10/21 03:31 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 1K09032 EPA 8260D 11/10/21 03:31 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 1K09032 EPA 8260D 11/10/21 03:31 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Acetone [67-64-1]A 10 U ug/L 1 10 20 1K09032 EPA 8260D 11/10/21 03:31 RKY Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 1K09032 EPA 8260D 11/10/21 03:31 RKY Benzene [71-43-2]A 0.62 J ug/L 1 0.15 1.0 IK09032 EPA 8260D 11/10/21 03:31 RKY Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Bromodichloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Chlorobenzene [108-90-7]A 9.6 ug/L 1 0.17 1.0 IK09032 EPA 8260D 11/10/21 03:31 RKY Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Chloroform [67-66-3]A 0.18 U ug/L 1 0.18 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY cis-1,2-Dichloroethene [156-59-2]A 18 ug/L 1 0.15 1.0 IK09032 EPA 8260D 11/10/21 03:31 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Ethylbenzene[100-41-4]A 0.13 U ug/L 1 0.13 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 1K09032 EPA 8260D 11/10/21 03:31 RKY m,p-Xylenes[108-38-3/106-42-3]A 0.17 U ug/L 1 0.17 2.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY o-Xylene [95-47-6]A 0.065 U ug/L 1 0.065 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Styrene[100-42-5]A 0.11 U ug/L 1 0.11 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Tetrachloroethene [127-18-4]A 0.50 J ug/L 1 0.17 1.0 IK09032 EPA 8260D 11/10/21 03:31 RKY Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 1K09032 EPA 8260D 11/10/21 03:31 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 37 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW6I Lab Sample ID:CE13949-14 Received: 10/29/21 10:45 Matrix: Water Sampled:10/28/21 11:45 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 3.2 ug/L 1 0.32 1.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K09032 EPA 8260D 11/10/21 03:31 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 59 1 50.0 118 % 53-136 1KO9032 EPA 6260D 11110121 03:31 RKY Dibromofluoromethane 55 1 50.0 110 % 67-129 IK09032 EPA 6260D 11110121 03:31 RKY Toluene-d8 62 1 50.0 123 % 59-134 IK09032 EPA 8260D 11110121 03:31 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 69 ug/L 1 0.80 2.0 1K02042 EPA 8260D 11/03/21 04:35 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 5.0 1 5.00 101 % 75-125 1K02042 EPA 8260D 11103121 0425 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 38 of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW6D Lab Sample ID:CE13949-15 Received: 10/29/21 10:45 Matrix: Water Sampled:10/28/21 11:15 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.85 LID ug/L 5 0.85 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY 1,1,1-Trichloroethane [71-55-6]A 3.4 ID ug/L 5 0.60 5.0 IK09032 EPA 8260D 11/10/21 03:59 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 1.4 LID ug/L 5 1.4 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY 1,1,2-Trichloroethane [79-00-5]A 0.70 LID ug/L 5 0.70 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY 1.1-Dichloroethane [75-34-3]A 110 D ug/L 5 0.65 5.0 IK09032 EPA 8260D 11/10/21 03:59 RKY 1.1-Dichloroethene [75-35-4]A 38 D ug/L 5 1.0 5.0 IK09032 EPA 8260D 11/10/21 03:59 RKY 1,2,3-Trichloropropane [96-18-4]A 1.2 LID ug/L 5 1.2 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 2.4 LID ug/L 5 2.4 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY 1,2-Dibromoethane [106-93-4]A 3.3 LID ug/L 5 3.3 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY 1,2-Dichlorobenzene [95-50-1]A 0.95 LID ug/L 5 0.95 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY 1.2-Dichloroethane [107-06-2]A 5.3 D ug/L 5 1.0 5.0 IK09032 EPA 8260D 11/10/21 03:59 RKY 1,2-Dichloropropane [78-87-5]A 0.50 LID ug/L 5 0.50 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY 1,4-Dichlorobenzene [106-46-7]A 0.95 LID ug/L 5 0.95 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY 2-Butanone [78-93-3]A 6.5 LID ug/L 5 6.5 25 1K09032 EPA 8260D 11/10/21 03:59 RKY 2-Hexanone [591-78-6]A 4.4 LID ug/L 5 4.4 25 1K09032 EPA 8260D 11/10/21 03:59 RKY 4-Methyl-2-pentanone [108-10-1]A 5.5 LID ug/L 5 5.5 25 1K09032 EPA 8260D 11/10/21 03:59 RKY Acetone [67-64-1]A 50 LID ug/L 5 50 100 1K09032 EPA 8260D 11/10/21 03:59 RKY Acrylonitrile [107-13-1]A 18 LID ug/L 5 18 50 1K09032 EPA 8260D 11/10/21 03:59 RKY Benzene [71-43-2]A 2.2 ID ug/L 5 0.75 5.0 IK09032 EPA 8260D 11/10/21 03:59 RKY Bromochloromethane [74-97-5]A 2.4 LID ug/L 5 2.4 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY Bromodichloromethane [75-27-4]A 0.85 LID ug/L 5 0.85 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY Bromoform [75-25-2]A 1.1 LID ug/L 5 1.1 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY Bromomethane [74-83-9]A 0.70 LID ug/L 5 0.70 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY Carbon disulfide [75-15-0]A 7.5 LID ug/L 5 7.5 25 1K09032 EPA 8260D 11/10/21 03:59 RKY Carbon tetrachloride [56-23-5]A 0.85 LID ug/L 5 0.85 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY Chlorobenzene [108-90-7]A 93 D ug/L 5 0.85 5.0 IK09032 EPA 8260D 11/10/21 03:59 RKY Chloroethane [75-00-3]A 5.6 D ug/L 5 1.2 5.0 IK09032 EPA 8260D 11/10/21 03:59 RKY Chloroform [67-66-3]A 0.90 LID ug/L 5 0.90 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY Chloromethane [74-87-3]A 0.65 LID ug/L 5 0.65 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY cis-1,2-Dichloroethene [156-59-2]A 150 D ug/L 5 0.75 5.0 IK09032 EPA 8260D 11/10/21 03:59 RKY cis-1,3-Dichloropropene [10061-01-5]A 1.0 LID ug/L 5 1.0 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY Dibromochloromethane [124-48-1]A 0.85 LID ug/L 5 0.85 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY Dibromomethane [74-95-3]A 1.4 LID ug/L 5 1.4 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY Ethylbenzene [100-41-4]A 0.65 LID ug/L 5 0.65 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY Iodomethane[74-88-4]A 8.5 LID ug/L 5 8.5 25 1K09032 EPA 8260D 11/10/21 03:59 RKY m,p-Xylenes[108-38-3/106-42-3]A 0.85 LID ug/L 5 0.85 10 1K09032 EPA 8260D 11/10/21 03:59 RKY Methylene chloride [75-09-2]A 1.2 LID ug/L 5 1.2 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY o-Xylene [95-47-6]A 0.32 LID ug/L 5 0.32 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY Styrene[100-42-5]A 0.55 LID ug/L 5 0.55 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY Tetrachloroethene [127-18-4]A 0.85 LID ug/L 5 0.85 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY Toluene [108-88-3]A 0.70 LID ug/L 5 0.70 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY trans-1,2-Dichloroethene [156-60-5]A 1.0 LID ug/L 5 1.0 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.75 LID ug/L 5 0.75 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 3.5 LID ug/L 5 3.5 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY Trichloroethene [79-01-6]A 0.75 LID ug/L 5 0.75 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY Trichlorofluoromethane [75-69-4]A 1.2 LID ug/L 5 1.2 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY Vinyl acetate [108-05-4]A 4.8 LID ug/L 5 4.8 25 1K09032 EPA 8260D 11/10/21 03:59 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 39 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW6D Lab Sample ID:CE13949-15 Received: 10/29/21 10:45 Matrix: Water Sampled:10/28/21 11:15 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 22 D ug/L 5 1.6 5.0 1K09032 EPA 8260D 11/10/21 03:59 RKY Xylenes (Total) [1330-20-7]^ 2.2 UD ug/L 5 2.2 15 1K09032 EPA 8260D 11/10/21 03:59 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 60 1 50.0 119 % 53-136 IK09032 EPA 6260D 11110121 03:59 RKY Dibromofluoromethane 56 1 50.0 112 % 67-129 IK09032 EPA 6260D 11110121 03:59 RKY Toluene-d8 62 1 50.0 125 % 59-134 IK09032 EPA 8260D 11110121 03:59 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 190 D ug/L 10 8.0 20 1K02042 EPA 8260D 11/03/21 05:01 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.1 1 5.00 102 % 75-125 1K02042 EPA 8260D 11103121 05:01 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 40 of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW10I Lab Sample ID:CE13949-16 Received: 10/29/21 10:45 Matrix: Water Sampled:10/26/21 12:00 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY 1,1-Dichloroethane [75-34-3]A 7.0 ug/L 1 0.13 1.0 IK04051 EPA 8260D 11/05/21 16:20 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY QV-01 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY 1,4-Dichlorobenzene [306-46-7]^ 1.7 ug/L 1 0.19 1.0 IK04051 EPA 8260D 11/05/21 16:20 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 1K04051 EPA 8260D 11/05/21 16:20 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 1K04051 EPA 8260D 11/05/21 16:20 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 1K04051 EPA 8260D 11/05/21 16:20 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 1K04051 EPA 8260D 11/05/21 16:20 RKY Benzene [71-43-2]A 1.2 ug/L 1 0.15 1.0 IK04051 EPA 8260D 11/05/21 16:20 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Chlorobenzene [108-90-7]A 2.2 ug/L 1 0.17 1.0 IK04051 EPA 8260D 11/05/21 16:20 RKY Chloroethane [75-00-3]A 2.9 ug/L 1 0.23 1.0 IK04051 EPA 8260D 11/05/21 16:20 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Ethylbenzene[100-41-4]^ 0.13 U ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 1K04051 EPA 8260D 11/05/21 16:20 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Styrene[100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1K04051 EPA 8260D 11/05/21 16:20 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 41 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW10I Lab Sample ID:CE13949-16 Received: 10/29/21 10:45 Matrix: Water Sampled:10/26/21 12:00 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 1.9 ug/L 1 0.32 1.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K04051 EPA 8260D 11/05/21 16:20 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 49 1 50.0 98 % 53-136 IK04051 EPA 6260D 11105121 16:20 RKY Dibromofluoromethane 50 1 50.0 101 % 67-129 IK04051 EPA 6260D 11105121 16:20 RKY Toluene-d8 49 1 50.0 98 % 59-134 IK04051 EPA 6260D 11105121 16:20 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 310 D ug/L 10 8.0 20 1K02042 EPA 8260D 11/03/21 05:26 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.4 1 5.00 108 % 75-125 1K02042 EPA 8260D 11103121 05:26 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 42 of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW10D Lab Sample ID:CE13949-17 Received: 10/29/21 10:45 Matrix: Water Sampled:10/26/21 11:10 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY QV-01 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1K04051 EPA 8260D 11/05/21 16:49 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1K04051 EPA 8260D 11/05/21 16:49 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 1K04051 EPA 8260D 11/05/21 16:49 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1K04051 EPA 8260D 11/05/21 16:49 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Chlorobenzene[108-90-7]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Ethylbenzene[100-41-4]A 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1K04051 EPA 8260D 11/05/21 16:49 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY o-Xylene [95-47-6]A 0.065 u ug/L 1 0.065 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Styrene[100-42-5]A 0.11 u ug/L 1 0.11 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Vinyl acetate [108-05-4]A 0.95 Ll ug/L 1 0.95 5.0 1K04051 EPA 8260D 11/05/21 16:49 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 43 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW10D Lab Sample ID:CE13949-17 Received: 10/29/21 10:45 Matrix: Water Sampled:10/26/21 11:10 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K04051 EPA 8260D 11/05/21 16:49 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 50 1 50.0 101 % 53-136 1KO4051 EPA 6260D 11105121 16:49 RKY Dibromofluoromethane 50 1 50.0 101 % 67-129 IK04051 EPA 6260D 11105121 16:49 RKY Toluene-d8 49 1 50.0 99 % 59-134 IK04051 EPA 6260D 11105121 16:49 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1K02042 EPA 8260D 11/03/21 01:35 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 5.5 1 5.00 110 % 75-125 1K02042 EPA 8260D 11103121 01:35 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 44 of 81 00� www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW12I Lab Sample ID:CE13949-18 Received: 10/29/21 10:45 Matrix: Water Sampled:10/28/21 13:25 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1K09032 EPA 8260D 11/10/21 04:27 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1K09032 EPA 8260D 11/10/21 04:27 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 1K09032 EPA 8260D 11/10/21 04:27 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1K09032 EPA 8260D 11/10/21 04:27 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Chlorobenzene[108-90-7]A 0.17 u ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Ethylbenzene[100-41-4]A 0.13 u ug/L 1 0.13 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1K09032 EPA 8260D 11/10/21 04:27 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY o-Xylene [95-47-6]A 0.065 u ug/L 1 0.065 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Styrene[100-42-5]A 0.11 u ug/L 1 0.11 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Vinyl acetate [108-05-4]A 0.95 Ll ug/L 1 0.95 5.0 1K09032 EPA 8260D 11/10/21 04:27 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 45 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW12I Lab Sample ID:CE13949-18 Received: 10/29/21 10:45 Matrix: Water Sampled:10/28/21 13:25 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K09032 EPA 8260D 11/10/21 04:27 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 59 1 50.0 118 % 53-136 IK09032 EPA 6260D 11110121 04:27 RKY Dibromofluoromethane 54 1 50.0 109 % 67-129 IK09032 EPA 6260D 11110121 04:27 RKY Toluene-d8 62 1 50.0 123 % 59-134 IK09032 EPA 8260D 11110121 04:27 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1K02042 EPA 8260D 11/03/21 05:52 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.0 1 5.00 99 % 75-125 1K02042 EPA 8260D 11103121 05:52 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 46 of 81 00� www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW13I Lab Sample ID:CE13949-19 Received: 10/29/21 10:45 Matrix: Water Sampled: 10/28/2109:00 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY 1,1-Dichloroethane [75-34-3]A 87 ug/L 1 0.13 1.0 IK09032 EPA 8260D 11/10/21 04:55 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY 1,2-Dichloroethane [107-06-2]A 1.2 ug/L 1 0.21 1.0 IK09032 EPA 8260D 11/10/21 04:55 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY 1,4-Dichlorobenzene [106-46-7]A 0.74 J ug/L 1 0.19 1.0 IK09032 EPA 8260D 11/10/21 04:55 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 1K09032 EPA 8260D 11/10/21 04:55 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 1K09032 EPA 8260D 11/10/21 04:55 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 1K09032 EPA 8260D 11/10/21 04:55 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 1K09032 EPA 8260D 11/10/21 04:55 RKY Benzene [71-43-2]A 2.3 ug/L 1 0.15 1.0 IK09032 EPA 8260D 11/10/21 04:55 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Chlorobenzene [108-90-7]A 9.4 ug/L 1 0.17 1.0 IK09032 EPA 8260D 11/10/21 04:55 RKY Chloroethane [75-00-3]A 1.2 ug/L 1 0.23 1.0 IK09032 EPA 8260D 11/10/21 04:55 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Ethylbenzene[100-41-4]^ 0.13 U ug/L 1 0.13 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 1K09032 EPA 8260D 11/10/21 04:55 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY o-Xylene [95-47-6]A 0.065 U ug/L 1 0.065 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Styrene[100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Toluene [108-88-3]A 0.53 J ug/L 1 0.14 1.0 IK09032 EPA 8260D 11/10/21 04:55 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1K09032 EPA 8260D 11/10/21 04:55 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 47 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW13I Lab Sample ID:CE13949-19 Received: 10/29/21 10:45 Matrix: Water Sampled: 10/28/2109:00 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.94 J ug/L 1 0.32 1.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K09032 EPA 8260D 11/10/21 04:55 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 60 1 50.0 120 % 53-136 IK09032 EPA 6260D 11110121 04:55 RKY Dibromofluoromethane 55 1 50.0 111 % 67-129 IK09032 EPA 6260D 11110121 04:55 RKY Toluene-d8 61 1 50.0 122 % 59-134 IK09032 EPA 8260D 11110121 04:55 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 70 ug/L 1 0.80 2.0 1K02042 EPA 8260D 11/03/21 06:18 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.1 1 5.00 102 % 75-125 1K02042 EPA 8260D 11103121 06:16 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 48 of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW14D Lab Sample ID:CE13949-20 Received: 10/29/21 10:45 Matrix: Water Sampled:10/27/21 11:00 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY 1,1-Dichloroethane [75-34-3]A 0.13 U ug/L 1 0.13 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY 1,1-Dichloroethene [75-35-4]A 0.21 U ug/L 1 0.21 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY QV-01 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY 1,2-Dichloroethane [107-06-2]A 0.21 U ug/L 1 0.21 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY 1,2-Dichloropropane [78-87-5]A 0.10 U ug/L 1 0.10 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 1K03032 EPA 8260D 11/03/21 22:24 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 1K03032 EPA 8260D 11/03/21 22:24 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 1K03032 EPA 8260D 11/03/21 22:24 RKY Acetone [67-64-1]A 10 U ug/L 1 10 20 1K03032 EPA 8260D 11/03/21 22:24 RKY Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 1K03032 EPA 8260D 11/03/21 22:24 RKY Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY QV-01 Bromodichloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 1K03032 EPA 8260D 11/03/21 22:24 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY QV-01 Chlorobenzene [108-90-7]A 0.80 J ug/L 1 0.17 1.0 IK03032 EPA 8260D 11/03/21 22:24 RKY Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY Chloroform [67-66-3]A 0.18 U ug/L 1 0.18 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY cis-1,2-Dichloroethene [156-59-2]A 0.76 J ug/L 1 0.15 1.0 IK03032 EPA 8260D 11/03/21 22:24 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY Ethylbenzene [100-41-4]A 0.67 J ug/L 1 0.13 1.0 IK03032 EPA 8260D 11/03/21 22:24 RKY Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 1K03032 EPA 8260D 11/03/21 22:24 RKY m,p-Xylenes[108-38-3/306-42-3]A 2.8 ug/L 1 0.17 2.0 IK03032 EPA 8260D 11/03/21 22:24 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY o-Xylene [95-47-6]A 1.4 ug/L 1 0.065 1.0 IK03032 EPA 8260D 11/03/21 22:24 RKY Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY Toluene [108-88-3]A 1.7 ug/L 1 0.14 1.0 IK03032 EPA 8260D 11/03/21 22:24 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 1K03032 EPA 8260D 11/03/21 22:24 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 49 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW14D Lab Sample ID:CE13949-20 Received: 10/29/21 10:45 Matrix: Water Sampled:10/27/21 11:00 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K03032 EPA 8260D 11/03/21 22:24 RKY Xylenes (Total) [1330-20-7]^ 4.2 ug/L 1 0.45 3.0 1K03032 EPA 8260D 11/03/21 22:24 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 50 1 50.0 99 % 53-136 1KO3032 EPA 6260D 11103121 22:24 RKY Dibromofluoromethane 51 1 50.0 101 % 67-129 IK03032 EPA 6260D 11103121 22:24 RKY Toluene-d8 49 1 50.0 98 % 59-134 IK03032 EPA 6260D 11103121 22:24 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1K02042 EPA 8260D 11/03/21 06:43 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 5.1 1 5.00 102 % 75-125 1K02042 EPA 8260D 11103121 06:43 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 50 of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW15D Lab Sample ID:CE13949-21 Received: 10/29/21 10:45 Matrix: Water Sampled:10/27/21 10:20 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY 1,1-Dichloroethane [75-34-3]A 18 ug/L 1 0.13 1.0 IK03032 EPA 8260D 11/03/21 22:53 RKY 1,1-Dichloroethene [75-35-4]A 5.2 ug/L 1 0.21 1.0 IK05042 EPA 8260D 11/06/21 17:12 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY 1,2-Dichloroethane [107-06-2]A 0.53 J ug/L 1 0.21 1.0 IK03032 EPA 8260D 11/03/21 22:53 RKY 1,2-Dichloropropane [78-87-5]A 0.10 U ug/L 1 0.10 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 1K03032 EPA 8260D 11/03/21 22:53 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 1K03032 EPA 8260D 11/03/21 22:53 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Acetone [67-64-1]A 10 U ug/L 1 10 20 1K03032 EPA 8260D 11/03/21 22:53 RKY Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 1K03032 EPA 8260D 11/03/21 22:53 RKY Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY QV-01 Bromodichloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY QV-01 Chlorobenzene [108-90-7]A 2.0 ug/L 1 0.17 1.0 IK03032 EPA 8260D 11/03/21 22:53 RKY Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Chloroform [67-66-3]A 0.18 U ug/L 1 0.18 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY cis-1,2-Dichloroethene [156-59-2]A 27 ug/L 1 0.15 1.0 IK03032 EPA 8260D 11/03/21 22:53 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Ethylbenzene[100-41-4]A 0.13 U ug/L 1 0.13 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 1K03032 EPA 8260D 11/03/21 22:53 RKY m,p-Xylenes[108-38-3/106-42-3]A 0.17 U ug/L 1 0.17 2.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY o-Xylene [95-47-6]A 0.065 U ug/L 1 0.065 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Styrene[100-42-5]A 0.11 U ug/L 1 0.11 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 1K03032 EPA 8260D 11/03/21 22:53 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 51 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW15D Lab Sample ID:CE13949-21 Received: 10/29/21 10:45 Matrix: Water Sampled:10/27/21 10:20 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 1.1 ug/L 1 0.32 1.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K03032 EPA 8260D 11/03/21 22:53 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 50 1 50.0 100 % 53-136 IK03032 EPA 6260D 11103121 22:53 RKY 4-Bromofluorobenzene 50 1 50.0 99 % 53-136 IK05042 EPA 6260D 11106121 17:12 RKY Dibromofluoromethane 50 1 50.0 99 % 67-129 IK03032 EPA 6260D 11103121 22:53 RKY Dibromofluoromethane 49 1 50.0 98 % 67-129 IK05042 EPA 6260D 11106121 17:12 RKY Toluene-d8 49 1 50.0 98 % 59-134 IK03032 EPA 6260D 11103121 22:53 RKY Toluene-d8 48 1 50.0 95 % 59-134 IK05042 EPA 6260D 11106121 17:12 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed gy Notes 1,4-Dioxane [123-91-1]^ 53 ug/L 1 0.80 2.0 1K02042 EPA 8260D 11/03/21 07:09 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed By Notes Toluene-d8 5.4 1 5.00 109 % 75-125 1K02042 EPA 8260D 11103121 07:09 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 52 of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW16D Lab Sample ID:CE13949-22 Received: 10/29/21 10:45 Matrix: Water Sampled: 10/27/2109:10 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY 1,1-Dichloroethane [75-34-3]A 20 ug/L 1 0.13 1.0 IK03032 EPA 8260D 11/03/21 23:22 RKY 1,1-Dichloroethene [75-35-4]A 7.1 ug/L 1 0.21 1.0 IK05042 EPA 8260D 11/06/21 17:42 RKY 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY 1,2-Dichloroethane [107-06-2]A 0.21 U ug/L 1 0.21 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY 1,2-Dichloropropane [78-87-5]A 0.10 U ug/L 1 0.10 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 1K03032 EPA 8260D 11/03/21 23:22 RKY 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 1K03032 EPA 8260D 11/03/21 23:22 RKY 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Acetone [67-64-1]A 10 U ug/L 1 10 20 1K03032 EPA 8260D 11/03/21 23:22 RKY Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 1K03032 EPA 8260D 11/03/21 23:22 RKY Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY QV-01 Bromodichloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY QV-01 Chlorobenzene [108-90-7]A 40 ug/L 1 0.17 1.0 IK03032 EPA 8260D 11/03/21 23:22 RKY Chloroethane [75-00-3]A 1.5 ug/L 1 0.23 1.0 IK03032 EPA 8260D 11/03/21 23:22 RKY Chloroform [67-66-3]A 0.18 U ug/L 1 0.18 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY cis-1,2-Dichloroethene [156-59-2]A 32 ug/L 1 0.15 1.0 IK03032 EPA 8260D 11/03/21 23:22 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Ethylbenzene[100-41-4]A 0.13 U ug/L 1 0.13 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 1K03032 EPA 8260D 11/03/21 23:22 RKY m,p-Xylenes[108-38-3/106-42-3]A 0.17 U ug/L 1 0.17 2.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY o-Xylene [95-47-6]A 0.065 U ug/L 1 0.065 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Styrene[100-42-5]A 0.11 U ug/L 1 0.11 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 1K03032 EPA 8260D 11/03/21 23:22 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 53 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW16D Lab Sample ID:CE13949-22 Received: 10/29/21 10:45 Matrix: Water Sampled: 10/27/2109:10 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 3.6 ug/L 1 0.32 1.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K03032 EPA 8260D 11/03/21 23:22 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 50 1 50.0 100 % 53-136 IK03032 EPA 6260D 11103121 23:22 RKY 4-Bromofluorobenzene 50 1 50.0 100 % 53-136 IK05042 EPA 6260D 11106121 17:42 RKY Dibromofluoromethane 50 1 50.0 100 % 67-129 IK03032 EPA 8260D 11103121 23:22 RKY Dibromofluoromethane 49 1 50.0 98 % 67-129 IK05042 EPA 8260D 11106121 17:42 RKY Toluene-d8 49 1 50.0 98 % 59-134 IK03032 EPA 6260D 11103121 23:22 RKY Toluene-d8 47 1 50.0 94 % 59-134 IK05042 EPA 6260D 11106121 17:42 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed gy Notes 1,4-Dioxane [123-91-1]^ 23 ug/L 1 0.80 2.0 1K02042 EPA 8260D 11/03/21 07:35 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.3 1 5.00 106 % 75-125 1K02042 EPA 8260D 11103121 0735 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 54 of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PWSF1 Lab Sample ID:CE13949-23 Received: 10/29/21 10:45 Matrix: Water Sampled:10/27/21 13:05 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 85 UD ug/L 500 85 500 1K05042 EPA 8260D 11/06/21 19:38 RKY 1,1,1-Trichloroethane [71-55-6]^ 3300 D ug/L 500 60 500 1KO5042 EPA 8260D 11/06/21 19:38 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 140 UD ug/L 500 140 500 1K05042 EPA 8260D 11/06/21 19:38 RKY 1,1,2-Trichloroethane [79-00-5]^ 70 UD ug/L 500 70 500 1K05042 EPA 8260D 11/06/21 19:38 RKY 1,1-Dichloroethane [75-34-3]^ 6200 D ug/L 500 65 500 1KO5042 EPA 8260D 11/06/21 19:38 RKY 1,1-Dichloroethene [75-35-4]^ 5300 D ug/L 500 100 500 1KO5042 EPA 8260D 11/06/21 19:38 RKY 1,2,3-Trichloropropane [96-18-4]^ 120 UD ug/L 500 120 500 1K05042 EPA 8260D 11/06/21 19:38 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 240 UD ug/L 500 240 500 1K05042 EPA 8260D 11/06/21 19:38 RKY 1,2-Dibromoethane[106-93-4]^ 330 UD ug/L 500 330 500 1K05042 EPA 8260D 11/06/21 19:38 RKY 1,2-Dichlorobenzene [95-50-1]^ 95 UD ug/L 500 95 500 1K05042 EPA 8260D 11/06/21 19:38 RKY 1,2-Dichloroethane [107-06-2]^ 100 UD ug/L 500 100 500 1K05042 EPA 8260D 11/06/21 19:38 RKY 1,2-Dichloropropane [78-87-5]^ 50 UD ug/L 500 50 500 1K05042 EPA 8260D 11/06/21 19:38 RKY 1,4-Dichlorobenzene [106-46-7]^ 95 UD ug/L 500 95 500 1K05042 EPA 8260D 11/06/21 19:38 RKY 2-Butanone [78-93-3]^ 650 UD ug/L 500 650 2500 1K05042 EPA 8260D 11/06/21 19:38 RKY 2-Hexanone [591-78-6]^ 440 UD ug/L 500 440 2500 1K05042 EPA 8260D 11/06/21 19:38 RKY 4-Methyl-2-pentanone[108-10-1]^ 550 UD ug/L 500 550 2500 1K05042 EPA 8260D 11/06/21 19:38 RKY Acetone [67-64-1]^ 5000 UD ug/L 500 5000 10000 1K05042 EPA 8260D 11/06/21 19:38 RKY Acrylonitrile [107-13-1]^ 1800 UD ug/L 500 1800 5000 1K05042 EPA 8260D 11/06/21 19:38 RKY Benzene [71-43-2]^ 75 UD ug/L 500 75 500 1K05042 EPA 8260D 11/06/21 19:38 RKY Bromochloromethane [74-97-5]^ 240 UD ug/L 500 240 500 1K05042 EPA 8260D 11/06/21 19:38 RKY QV-01 Bromodichloromethane [75-27-4]^ 85 UD ug/L 500 85 500 1K05042 EPA 8260D 11/06/21 19:38 RKY Bromoform [75-25-2]^ 110 UD ug/L 500 110 500 1K05042 EPA 8260D 11/06/21 19:38 RKY Bromomethane [74-83-9]^ 70 UD ug/L 500 70 500 1K05042 EPA 8260D 11/06/21 19:38 RKY Carbon disulfide [75-15-0]^ 750 UD ug/L 500 750 2500 1K05042 EPA 8260D 11/06/21 19:38 RKY Carbon tetrachloride [56-23-5]^ 85 UD ug/L 500 85 500 1K05042 EPA 8260D 11/06/21 19:38 RKY QV-01 Chlorobenzene [308-90-7]^ 2100 D ug/L 500 85 500 1K05042 EPA 8260D 11/06/21 19:38 RKY Chloroethane [75-00-3]^ 120 UD ug/L 500 120 500 1K05042 EPA 8260D 11/06/21 19:38 RKY Chloroform [67-66-3]^ 90 UD ug/L 500 90 500 1K05042 EPA 8260D 11/06/21 19:38 RKY Chloromethane [74-87-3]^ 65 UD ug/L 500 65 500 1K05042 EPA 8260D 11/06/21 19:38 RKY cis- 1,2-Dichloroethene [156-59-2]^ 38000 D ug/L 500 75 500 1K05042 EPA 8260D 11/06/21 19:38 RKY cis- 1,3-Dichloropropene [10061-01-5]^ 100 UD ug/L 500 100 500 1K05042 EPA 8260D 11/06/21 19:38 RKY Dibromochloromethane [124-48-1]^ 85 UD ug/L 500 85 500 1K05042 EPA 8260D 11/06/21 19:38 RKY Dibromomethane [74-95-3]^ 140 UD ug/L 500 140 500 1K05042 EPA 8260D 11/06/21 19:38 RKY Ethylbenzene [100-41-4]^ 65 UD ug/L 500 65 500 1K05042 EPA 8260D 11/06/21 19:38 RKY Iodomethane[74-88-4]^ 850 UD ug/L 500 850 2500 1K05042 EPA 8260D 11/06/21 19:38 RKY m,p-Xylenes[108-38-3/106-42-3]^ 85 UD ug/L 500 85 1000 1K05042 EPA 8260D 11/06/21 19:38 RKY Methylene chloride [75-09-2]^ 260 JD ug/L 500 120 500 1K05042 EPA 8260D 11/06/21 19:38 RKY o-Xylene [95-47-6]^ 32 UD ug/L 500 32 500 1K05042 EPA 8260D 11/06/21 19:38 RKY Styrene [100-42-5]^ 55 UD ug/L 500 55 500 1K05042 EPA 8260D 11/06/21 19:38 RKY Tetrachloroethene [127-18-4]^ 85 UD ug/L 500 85 500 1K05042 EPA 8260D 11/06/21 19:38 RKY Toluene [308-88-3]^ 720 D ug/L 500 70 500 1K05042 EPA 8260D 11/06/21 19:38 RKY trans-1,2-Dichloroethene [156-60-5]^ 100 UD ug/L 500 100 500 1K05042 EPA 8260D 11/06/21 19:38 RKY trans-1,3-Dichloropropene [10061-02-6]^ 75 UD ug/L 500 75 500 1K05042 EPA 8260D 11/06/21 19:38 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 350 UD ug/L 500 350 500 1K05042 EPA 8260D 11/06/21 19:38 RKY Trichloroethene [79-01-6]^ 75 UD ug/L 500 75 500 1K05042 EPA 8260D 11/06/21 19:38 RKY QL-02, QV-01 Trichlorofluoromethane [75-69-4]^ 400 JD ug/L 500 120 500 1K05042 EPA 8260D 11/06/21 19:38 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 55 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PWSF1 Lab Sample ID:CE13949-23 Received: 10/29/21 10:45 Matrix: Water Sampled:10/27/21 13:05 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl acetate [108-05-4]^ 480 UD ug/L 500 480 2500 1K05042 EPA 8260D 11/06/21 19:38 RKY Vinyl chloride [75-01-4]^ 3200 D ug/L 500 160 500 1K05042 EPA 8260D 11/06/21 19:38 RKY Xylenes(Total)[1330-20-7]^ 220 UD ug/L 500 220 1500 1K05042 EPA 8260D 11/06/21 19:38 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 49 1 50.0 99 % 53-136 IK05042 EPA 6260D 11106121 19:38 RKY Dibromofluoromethane 50 1 50.0 99 % 67-129 IK05042 EPA 6260D 11106121 19:38 RKY Toluene-d8 49 1 50.0 98 % 59-134 IK05042 EPA 6260D 11106121 19:38 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 2300 D ug/L 100 80 200 1K02042 EPA 8260D 11/03/21 08:00 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.3 1 5.00 107 % 75-125 1K02042 EPA 8260D 11103121 08:00 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 56 of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-W4A Lab Sample ID:CE13949-24 Received: 10/29/21 10:45 Matrix: Water Sampled:10/27/21 12:35 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.85 LID ug/L 5 0.85 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY 1,1,1-Trichloroethane [71-55-6]A 24 D ug/L 5 0.60 5.0 IK08031 EPA 8260D 11/08/21 20:29 RKY 1,1,2,2-Tetrachloroethane [79-34-5]A 1.4 LID ug/L 5 1.4 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY 1,1,2-Trichloroethane [79-00-5]A 0.70 LID ug/L 5 0.70 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY 1.1-Dichloroethane [75-34-3]A 110 D ug/L 5 0.65 5.0 IK08031 EPA 8260D 11/08/21 20:29 RKY 1.1-Dichloroethene [75-35-4]A 43 D ug/L 5 1.0 5.0 IK08031 EPA 8260D 11/08/21 20:29 RKY 1,2,3-Trichloropropane [96-18-4]A 1.2 LID ug/L 5 1.2 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY 1,2-Dibromo-3-chloropropane [96-12-8]A 2.4 LID ug/L 5 2.4 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY 1,2-Dibromoethane [106-93-4]A 3.3 LID ug/L 5 3.3 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY 1,2-Dichlorobenzene [95-50-1]A 0.95 LID ug/L 5 0.95 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY 1.2-Dichloroethane [107-06-2]A 2.8 ID ug/L 5 1.0 5.0 IK08031 EPA 8260D 11/08/21 20:29 RKY 1,2-Dichloropropane [78-87-5]A 0.50 LID ug/L 5 0.50 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY 1,4-Dichlorobenzene [106-46-7]A 0.95 LID ug/L 5 0.95 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY 2-Butanone [78-93-3]A 6.5 LID ug/L 5 6.5 25 1KO8031 EPA 8260D 11/08/21 20:29 RKY 2-Hexanone [591-78-6]A 4.4 LID ug/L 5 4.4 25 1KO8031 EPA 8260D 11/08/21 20:29 RKY 4-Methyl-2-pentanone [108-10-1]A 5.5 LID ug/L 5 5.5 25 1KO8031 EPA 8260D 11/08/21 20:29 RKY Acetone [67-64-1]A 50 LID ug/L 5 50 100 1KO8031 EPA 8260D 11/08/21 20:29 RKY Acrylonitrile [107-13-1]A 18 LID ug/L 5 18 50 1KO8031 EPA 8260D 11/08/21 20:29 RKY Benzene [71-43-2]A 6.6 D ug/L 5 0.75 5.0 IK08031 EPA 8260D 11/08/21 20:29 RKY Bromochloromethane [74-97-5]A 2.4 LID ug/L 5 2.4 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY Bromodichloromethane [75-27-4]A 0.85 LID ug/L 5 0.85 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY Bromoform [75-25-2]A 1.1 LID ug/L 5 1.1 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY Bromomethane [74-83-9]A 0.70 LID ug/L 5 0.70 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY Carbon disulfide [75-15-0]A 7.5 LID ug/L 5 7.5 25 1KO8031 EPA 8260D 11/08/21 20:29 RKY Carbon tetrachloride [56-23-5]A 0.85 LID ug/L 5 0.85 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY Chlorobenzene [108-90-7]A 0.85 LID ug/L 5 0.85 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY Chloroethane [75-00-3]A 4.6 ID ug/L 5 1.2 5.0 IK08031 EPA 8260D 11/08/21 20:29 RKY Chloroform [67-66-3]A 0.90 LID ug/L 5 0.90 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY Chloromethane [74-87-3]A 0.65 LID ug/L 5 0.65 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY cis-1,2-Dichloroethene [156-59-2]A 170 D ug/L 5 0.75 5.0 IK08031 EPA 8260D 11/08/21 20:29 RKY cis-1,3-Dichloropropene [10061-01-5]A 1.0 LID ug/L 5 1.0 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY Dibromochloromethane [124-48-1]A 0.85 LID ug/L 5 0.85 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY Dibromomethane [74-95-3]A 1.4 LID ug/L 5 1.4 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY Ethylbenzene [100-41-4]A 0.65 LID ug/L 5 0.65 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY Iodomethane[74-88-4]A 8.5 LID ug/L 5 8.5 25 1KO8031 EPA 8260D 11/08/21 20:29 RKY m,p-Xylenes[108-38-3/106-42-3]A 0.85 LID ug/L 5 0.85 10 1KO8031 EPA 8260D 11/08/21 20:29 RKY Methylene chloride [75-09-2]A 1.2 LID ug/L 5 1.2 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY o-Xylene [95-47-6]A 0.32 LID ug/L 5 0.32 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY Styrene[100-42-5]A 0.55 LID ug/L 5 0.55 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY Tetrachloroethene [127-18-4]A 0.85 LID ug/L 5 0.85 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY Toluene [108-88-3]A 0.70 LID ug/L 5 0.70 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY trans-1,2-Dichloroethene [156-60-5]A 1.0 LID ug/L 5 1.0 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.75 LID ug/L 5 0.75 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 3.5 LID ug/L 5 3.5 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY Trichloroethene [79-01-6]A 0.75 LID ug/L 5 0.75 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY Trichlorofluoromethane [75-69-4]A 1.2 LID ug/L 5 1.2 5.0 1KO8031 EPA 8260D 11/08/21 20:29 RKY Vinyl acetate [108-05-4]A 4.8 LID ug/L 5 4.8 25 1KO8031 EPA 8260D 11/08/21 20:29 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 57 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-W4A Lab Sample ID:CE13949-24 Received: 10/29/21 10:45 Matrix: Water Sampled:10/27/21 12:35 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 98 D ug/L 5 1.6 5.0 1K08031 EPA 8260D 11/08/21 20:29 RKY Xylenes (Total) [1330-20-7]^ 2.2 UD ug/L 5 2.2 15 1K08031 EPA 8260D 11/08/21 20:29 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 63 1 50.0 125 % 53-136 IK08031 EPA 6260D 11108121 20:29 RKY Dibromofluoromethane 61 1 50.0 121 % 67-129 IK08031 EPA 6260D 11106121 20:29 RKY Toluene-d8 62 1 50.0 124 % 59-134 IK08031 EPA 8260D 11106121 20:29 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 54 ug/L 1 0.80 2.0 1K02042 EPA 8260D 11/03/21 08:27 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.0 1 5.00 99 % 75-125 1K02042 EPA 8260D 11103121 08:27 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 58 of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-TripBlank Lab Sample ID:CE13949-25 Received: 10/29/21 10:45 Matrix: Water Sampled: 10/26/2108:30 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY QV-01 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1K04051 EPA 8260D 11/05/21 11:55 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1K04051 EPA 8260D 11/05/21 11:55 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 1K04051 EPA 8260D 11/05/21 11:55 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1K04051 EPA 8260D 11/05/21 11:55 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Chlorobenzene[108-90-7]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Ethylbenzene[100-41-4]A 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1K04051 EPA 8260D 11/05/21 11:55 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY o-Xylene [95-47-6]A 0.065 u ug/L 1 0.065 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Styrene[100-42-5]A 0.11 u ug/L 1 0.11 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Vinyl acetate [108-05-4]A 0.95 Ll ug/L 1 0.95 5.0 1K04051 EPA 8260D 11/05/21 11:55 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 59 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-TripBlank Lab Sample ID:CE13949-25 Received: 10/29/21 10:45 Matrix: Water Sampled: 10/26/2108:30 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K04051 EPA 8260D 11/05/21 11:55 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 49 1 50.0 99 % 53-136 IK04051 EPA 6260D 11105121 11:55 RKY Dibromofluoromethane 50 1 50.0 99 % 67-129 IK04051 EPA 6260D 11105121 11:55 RKY Toluene-d8 47 1 50.0 95 % 59-134 IK04051 EPA 6260D 11105121 11:55 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1K02042 EPA 8260D 11/03/21 08:53 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed & Notes Toluene-d8 5.2 1 5.00 105 % 75-125 1K02042 EPA 8260D 11103121 08:53 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 60 Of 81 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-TripBlank Lab Sample ID:CE13949-26 Received: 10/29/21 10:45 Matrix: Water Sampled: 10/26/2108:30 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY QV-01 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY 2-Butanone [78-93-3]A 1.3 u ug/L 1 1.3 5.0 1K04051 EPA 8260D 11/05/21 12:24 RKY 2-Hexanone [591-78-6]A 0.88 u ug/L 1 0.88 5.0 1K04051 EPA 8260D 11/05/21 12:24 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Acetone [67-64-1]A 10 u ug/L 1 10 20 1K04051 EPA 8260D 11/05/21 12:24 RKY Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 1K04051 EPA 8260D 11/05/21 12:24 RKY Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Bromomethane [74-83-9]A 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Chlorobenzene[108-90-7]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Ethylbenzene[100-41-4]A 0.13 u ug/L 1 0.13 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 1K04051 EPA 8260D 11/05/21 12:24 RKY m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Methylene chloride [75-09-2]A 0.23 u ug/L 1 0.23 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY o-Xylene [95-47-6]A 0.065 u ug/L 1 0.065 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Styrene[100-42-5]A 0.11 u ug/L 1 0.11 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY trans-1,3-Dichloropropene [10061-02-6]A 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 u ug/L 1 0.70 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Vinyl acetate [108-05-4]A 0.95 Ll ug/L 1 0.95 5.0 1K04051 EPA 8260D 11/05/21 12:24 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 61 Of 81 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-TripBlank Lab Sample ID:CE13949-26 Received: 10/29/21 10:45 Matrix: Water Sampled: 10/26/2108:30 Work Order: CE13949 Project: Seaboard/Riverdale Landfill Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K04051 EPA 8260D 11/05/21 12:24 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 50 1 50.0 100 % 53-136 1KO4051 EPA 6260D 11105121 12:24 RKY Dibromofluoromethane 49 1 50.0 98 % 67-129 IK04051 EPA 6260D 11105121 12:24 RKY Toluene-d8 48 1 50.0 97 % 59-134 IK04051 EPA 6260D 11105121 12:24 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1K02042 EPA 8260D 11/03/21 09:18 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 5.2 1 5.00 103 % 75-125 1K02042 EPA 8260D 11103121 09:18 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 62 Of 81 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IK03032 - EPA 5030E MS Blank (lK03032-BLKS) Prepared: 11/03/2021 16:23 Analyzed: 11/03/2021 20:27 Analvte Result Flaq POL Units 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC Level Result %REC Limits RPD RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 63 Of 81 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IK03032 - EPA 5030B MS - Continued Blank (SK03032-BLKS) Continued Prepared: 11/03/2021 16:23 Analyzed: 11/03/2021 20:27 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 49 u9/L 50.0 99 53-136 Dibromofluoromethane 48 u9/L 50.0 96 67-129 Toluene-d8 47 u91L 50.0 95 59-134 LCS (11(03032-BS1) Prepared: 11/03/2021 16:23 Analyzed: 11/03/2021 18:31 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 23 1.0 ug/L 20.0 113 75-133 Benzene 22 1.0 ug/L 20.0 111 80-134 Chlorobenzene 19 1.0 ug/L 20.0 94 80-120 Toluene 18 1.0 ug/L 20.0 88 71-120 Trichloroethene 23 1.0 ug/L 20.0 116 74-120 4-Bromofluorobenzene 50 u91L 50.0 100 53-136 Dibromofluoromethane 50 u91L 50.0 99 67-129 Toluene-d8 48 u9/L 50.0 95 59-134 Matrix Spike (1K03032-MS1) Prepared: 11/03/2021 16:23 Analyzed: 11/03/2021 19:00 Source: CE16709-03 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 23 1.0 ug/L 20.0 0.21 U 114 75-133 Benzene 21 1.0 ug/L 20.0 0.15 U 107 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 94 80-120 Toluene 17 1.0 ug/L 20.0 0.14 U 87 71-120 Trichloroethene 23 1.0 ug/L 20.0 0.15 U 114 74-120 4-Bromofluorobenzene 49 u9/L 50.0 99 53-136 Dibromofluoromethane 50 u9/L 50.0 100 67-129 Toluene-d8 47 u91L 50.0 95 59-134 Matrix Spike Dup (1K03032-MSD1) Prepared: 11/03/2021 16:23 Analyzed: 11/03/2021 19:29 Source: CE16709-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 0.21 U 104 75-133 9 20 Benzene 20 1.0 ug/L 20.0 0.15 U 101 80-134 5 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 93 80-120 1 16 Toluene 17 1.0 ug/L 20.0 0.14 U 84 71-120 3 17 Trichloroethene 22 1.0 ug/L 20.0 0.15 U 110 74-120 3 22 4-Bromofluorobenzene 50 u9/L 50.0 99 53-136 Dibromofluoromethane 48 u91L 50.0 97 67-129 Toluene-d8 46 u9/L 50.0 93 59-134 Batch ZK04051 - EPA 5030E MS Blank (1K04051-BLK1) Prepared: 11/04/2021 18:41 Analyzed: 11/05/2021 11:26 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 64 Of 81 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IK04051 - EPA 5030B MS - Continued Blank (SK04051-BLKS) Continued Prepared: 11/04/2021 18:41 Analyzed: 11/05/2021 11:26 Analvte Result Flaq POL Units 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 49 u91L 50.0 98 53-136 Dibromofluoromethane 50 u91L 50.0 99 67-129 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 65 Of 81 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IK04051 - EPA 5030B MS - Continued Blank (SK04051-BLKS) Continued Prepared: 11/04/2021 18:41 Analyzed: 11/05/2021 11:26 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Toluene-d8 47 u91L 50.0 95 59-134 LCS (1K04051-BS1) Prepared: 11/04/2021 18:41 Analyzed: 11/05/2021 09:28 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 107 75-133 Benzene 20 1.0 ug/L 20.0 100 80-134 Chlorobenzene 17 1.0 ug/L 20.0 85 80-120 Toluene 16 1.0 ug/L 20.0 80 71-120 Trichloroethene 22 1.0 ug/L 20.0 108 74-120 4-Bromofluorobenzene 50 u91L 50.0 100 53-136 Dibromofluoromethane 50 u91L 50.0 99 67-129 Toluene-d8 49 u91L 50.0 98 59-134 Matrix Spike (1K04051-MS1) Prepared: 11/04/2021 18:41 Analyzed: 11/05/2021 09:58 Source: CE16709-05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 24 1.0 ug/L 20.0 0.21 U 120 75-133 Benzene 24 1.0 ug/L 20.0 0.15 U 119 80-134 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 98 80-120 Toluene 19 1.0 ug/L 20.0 0.14 U 95 71-120 Trichloroethene 27 1.0 ug/L 20.0 0.15 U 133 74-120 QM-07 4-Bromofluorobenzene 50 u91L 50.0 101 53-136 Dibromofluoromethane 50 u91L 50.0 100 67-129 Toluene-d8 48 u91L 50.0 96 59-134 Matrix Spike Dup (1K04051-MSD1) Prepared: 11/04/2021 18:41 Analyzed: 11/05/2021 10:27 Source: CE16709-05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 0.21 U 105 75-133 14 20 Benzene 21 1.0 ug/L 20.0 0.15 U 105 80-134 12 17 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 90 80-120 9 16 Toluene 17 1.0 ug/L 20.0 0.14 U 83 71-120 13 17 Trichloroethene 24 1.0 ug/L 20.0 0.15 U 120 74-120 10 22 4-Bromofluorobenzene 49 u91L 50.0 99 53-136 Dibromofluoromethane 49 u91L 50.0 96 67-129 Toluene-& 48 u91L 50.0 96 59-134 Batch IK05042 - EPA 5030B MS Blank (1K05042-BLKi) Prepared: 11/05/2021 17:42 Analyzed: 11/06/2021 13:18 Spike Source %REC Analvte Result Flaq POL Units Level Result %REC Limits 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L RPD RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full Page 66 of 81 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IK05042 - EPA 5030B MS - Continued Blank (SK05042-BLKS) Continued Prepared: 11/05/2021 17:42 Analyzed: 11/06/2021 13:18 Analvte Result Flaq POL Units 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 47 u9/L 50.0 95 53-136 Dibromofluoromethane 46 u9/L 50.0 91 67-129 Toluene-d8 45 u9/L 50.0 89 59-134 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 67 Of 81 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1K05042 - EPA 5030B MS - Continued LCS (1K05042-BS1) Prepared: 11/05/2021 17:42 Analyzed: 11/06/2021 11:21 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 106 75-133 Benzene 20 1.0 ug/L 20.0 102 80-134 Chlorobenzene 18 1.0 ug/L 20.0 91 80-120 Toluene 16 1.0 ug/L 20.0 79 71-120 Trichloroethene 25 1.0 ug/L 20.0 124 74-120 QL-02 4-Bromofluorobenzene 46 u91L 50.0 92 53-136 Dibromofluoromethane 47 u91L 50.0 93 67-129 Toluene-d8 46 u91L 50.0 91 59-134 Matrix Spike (1K05042-MS1) Prepared: 11/05/2021 17:42 Analyzed: 11/06/2021 11:50 Source: CE17193-04 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 23 1.0 ug/L 20.0 0.21 U 113 75-133 Benzene 22 1.0 ug/L 20.0 0.15 U 112 80-134 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 100 80-120 Toluene 17 1.0 ug/L 20.0 0.14 U 87 71-120 Trichloroethene 29 1.0 ug/L 20.0 0.15 U 146 74-120 QM-07 4-Bromofluorobenzene 47 u91L 50.0 95 53-136 Dibromofluoromethane 46 u91L 50.0 91 67-129 Toluene-d8 45 u91L 50.0 90 59-134 Matrix Spike Dup (1K05042-MSD1) Prepared: 11/05/2021 17:42 Analyzed: 11/06/2021 12:20 Source: CE17193-04 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 0.21 U 101 75-133 12 20 Benzene 20 1.0 ug/L 20.0 0.15 U 100 80-134 11 17 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 90 80-120 11 16 Toluene 15 1.0 ug/L 20.0 0.14 U 76 71-120 13 17 Trichloroethene 26 1.0 ug/L 20.0 0.15 U 131 74-120 11 22 QM-07 4-Bromofluorobenzene 47 u91L 50.0 94 53-136 Dibromofluoromethane 46 u91L 50.0 92 67-129 Toluene-d8 45 u91L 50.0 90 59-134 Batch IK08031 - EPA 5030E MS Blank (1K08031-BLK1) Prepared: 11/08/2021 17:00 Analyzed: 11/08/2021 20:02 Spike Source %REC Analvte Result Flaq POL Units Level Result %REC Limits 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. RPD RPD Limit Notes Page 68 of 81 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IKOB031 - EPA 5030B MS - Continued Blank (SK08031-BLKS) Continued Prepared: 11/08/2021 17:00 Analyzed: 11/08/2021 20:02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromofluorobenzene 62 ug/L 50.0 123 53-136 Dibromofluoromethane 60 ug/L 50.0 120 67-129 Toluene-d8 61 ug/L 50.0 122 59-134 LCS (IK08031-BSI) Prepared: 11/08/2021 17:00 Analyzed: 11/08/2021 18:12 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 99 75-133 Benzene 19 1.0 ug/L 20.0 96 80-134 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 69 Of 81 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IKOB031 - EPA 5030B MS - Continued LCS (1K08031-BS3) Continued Prepared: 11/08/2021 17:00 Analyzed: 11/08/2021 18:12 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chlorobenzene 20 1.0 ug/L 20.0 99 80-120 Toluene 20 1.0 ug/L 20.0 100 71-120 Trichloroethene 20 1.0 ug/L 20.0 102 74-120 4-Bromofluorobenzene 62 ug/L 50.0 124 53-136 Dibromofluoromethane 60 u91L 50.0 119 67-129 Toluene-d8 61 u91L 50.0 122 59-134 Matrix Spike (1K08031-MS1) Prepared: 11/08/2021 17:00 Analyzed: 11/08/2021 18:40 Source: CE17193-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 0.21 U 102 75-133 Benzene 20 1.0 ug/L 20.0 0.15 U 98 80-134 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 101 80-120 Toluene 20 1.0 ug/L 20.0 0.14 U 102 71-120 Trichloroethene 21 1.0 ug/L 20.0 0.15 U 104 74-120 4-Bromofluorobenzene 62 ug/L 50.0 125 53-136 Dibromofluoromethane 61 ug/L 50.0 121 67-129 Toluene-d8 62 u91L 50.0 123 59-134 Matrix Spike Dup (1K08031-MSD1) Prepared: 11/08/2021 17:00 Analyzed: 11/08/2021 19:07 Source: CE17193-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 0.21 U 98 75-133 4 20 Benzene 19 1.0 ug/L 20.0 0.15 U 96 80-134 2 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 96 80-120 5 16 Toluene 19 1.0 ug/L 20.0 0.14 U 97 71-120 5 17 Trichloroethene 20 1.0 ug/L 20.0 0.15 U 102 74-120 2 22 4-Bromofluorobenzene 61 u91L 50.0 123 53-136 Dibromofluoromethane 61 u91L 50.0 122 67-129 Toluene-d8 61 u91L 50.0 123 59-134 Batch IK08033 - EPA 5030B MS Blank (1K08033-BLK1) Prepared: 11/08/2021 21:22 Analyzed: 11/09/2021 08:38 Analvte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1, 2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dich loroethane 1,1-Dichloroethene 1, 2, 3-Trich I o rop ropa ne 1,2-Di bromo-3-ch loropropane 1,2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane FINAL Spike Source %REC Result Flaq POL Units Level Result %REC Limits 0.17 U 1.0 ug/L 0.12 U 1.0 ug/L 0.28 U 1.0 ug/L 0.14 U 1.0 ug/L 0.13 U 1.0 ug/L 0.21 U 1.0 ug/L 0.23 U 1.0 ug/L 0.48 U 1.0 ug/L 0.66 U 1.0 ug/L 0.19 U 1.0 ug/L 0.21 U 1.0 ug/L 0.10 U 1.0 ug/L This report relates only to the sample as received by the laboratory, and may only be reproduced in full. RPD RPD Limit Notes Page 70 of 81 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IKOB033 - EPA 5030B MS - Continued Blank (SK08033-BLKS) Continued Prepared: 11/08/2021 21:22 Analyzed: 11/09/2021 08:38 Analvte Result Flaq POL Units 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 47 u91L 50.0 94 53-136 Dibromofluoromethane 48 u91L 50.0 96 67-129 Toluene-d8 46 u91L 50.0 92 59-134 LCS (1K08033-BS1) Prepared: 11/08/2021 21:22 Analyzed: 11/09/2021 06:42 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 22 1.0 ug/L 20.0 108 75-133 Benzene 21 1.0 ug/L 20.0 107 80-134 Chlorobenzene 19 1.0 ug/L 20.0 96 80-120 Toluene 17 1.0 ug/L 20.0 86 71-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 71 of 81 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IKOB033 - EPA 5030B MS - Continued LCS (1K08033-BS3) Continued Prepared: 11/08/2021 21:22 Analyzed: 11/09/2021 06:42 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Trichloroethene 25 1.0 ug/L 20.0 126 74-120 4-Bromofluorobenzene 49 u91L 50.0 96 53-136 Dibromofluoromethane 48 u91L 50.0 96 67-129 Toluene-d8 46 u91L 50.0 92 59-134 Matrix Spike (11(08033-MS1) Prepared: 11/08/2021 21:22 Analyzed: 11/09/2021 07:11 Source: CE17198-04 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 23 1.0 ug/L 20.0 0.21 U 113 75-133 Benzene 22 1.0 ug/L 20.0 0.15 U 110 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 97 80-120 Toluene 17 1.0 ug/L 20.0 0.14 U 86 71-120 Trichloroethene 26 1.0 ug/L 20.0 0.15 U 130 74-120 4-Bromofluorobenzene 48 u91L 50.0 95 53-136 Dibromofluoromethane 47 u91L 50.0 94 67-129 Toluene-d8 46 u91L 50.0 92 59-134 Matrix Spike Dup (1K08033-MSD1) Prepared: 11/08/2021 21:22 Analyzed: 11/09/2021 07:40 Source: CE17198-04 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 22 1.0 ug/L 20.0 0.21 U 108 75-133 5 20 Benzene 21 1.0 ug/L 20.0 0.15 U 105 80-134 4 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 95 80-120 3 16 Toluene 17 1.0 ug/L 20.0 0.14 U 84 71-120 3 17 Trichloroethene 25 1.0 ug/L 20.0 0.15 U 125 74-120 4 22 4-Bromofluorobenzene 46 u91L 50.0 96 53-136 Dibromofluoromethane 47 u91L 50.0 94 67-129 Toluene-d8 47 u91L 50.0 94 59-134 Batch IK09032 - EPA 5030B MS Blank (lK09032-BLKS) Prepared: 11/09/2021 16:12 Analyzed: 11/09/2021 21:58 Analvte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,2,3-Trichloropropane 1,2-Di bromo-3-ch loropropane 1,2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,4-Dichlorobenzene 2-Butanone FINAL Spike Source %REC Result Flaq POL Units Level Result %REC Limits 0.17 U 1.0 ug/L 0.12 U 1.0 ug/L 0.28 U 1.0 ug/L 0.14 U 1.0 ug/L 0.13 U 1.0 ug/L 0.21 U 1.0 ug/L 0.23 U 1.0 ug/L 0.48 U 1.0 ug/L 0.66 U 1.0 ug/L 0.19 U 1.0 ug/L 0.21 U 1.0 ug/L 0.10 U 1.0 ug/L 0.19 U 1.0 ug/L 1.3 U 5.0 ug/L This report relates only to the sample as received by the laboratory, and may only be reproduced in full. RPD RPD Limit Notes Page 72 of 81 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IK09032 - EPA 5030B MS - Continued Blank (SK09032-BLKS) Continued Prepared: 11/09/2021 16:12 Analyzed: 11/09/2021 21:58 Analvte Result Flaq POL Units 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 61 u91L 50.0 121 53-136 Dibromofluoromethane 55 u91L 50.0 111 67-129 Toluene-d8 61 u91L 50.0 122 59-134 LCS (lK09032-BS1) Prepared: 11/09/2021 16:12 Analyzed: 11/09/2021 20:06 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 93 75-133 Benzene 19 1.0 ug/L 20.0 94 80-134 Chlorobenzene 19 1.0 ug/L 20.0 94 80-120 Toluene 19 1.0 ug/L 20.0 95 71-120 Trichloroethene 19 1.0 ug/L 20.0 96 74-120 4-Bromofluorobenzene 60 u91L 50.0 120 53-136 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 73 Of 81 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IK09032 - EPA 5030B MS - Continued LCS (1K09032-BS3) Continued Prepared: 11/09/2021 16:12 Analyzed: 11/09/2021 20:06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Dibromofluoromethane 57 u9/L 50.0 113 67-129 Toluene-& 60 ug/L 50.0 121 59-134 Matrix Spike (1K09032-MS1) Prepared: 11/09/2021 16:12 Analyzed: 11/09/2021 20:34 Source: CE17193-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 0.21 U 96 75-133 Benzene 19 1.0 ug/L 20.0 0.15 U 97 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 97 80-120 Toluene 20 1.0 ug/L 20.0 0.14 U 99 71-120 Trichloroethene 20 1.0 ug/L 20.0 0.15 U 99 74-120 4-Bromofluorobenzene 60 ug/L 50.0 121 53-136 Dibromofluoromethane 56 ug/L 50.0 113 67-129 Toluene-d8 60 u91L 50.0 121 59-134 Matrix Spike Dup (1K09032-MSD1) Prepared: 11/09/2021 16:12 Analyzed: 11/09/2021 21:02 Source: CE17193-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 1.0 ug/L 20.0 0.21 U 92 75-133 4 20 Benzene 19 1.0 ug/L 20.0 0.15 U 94 80-134 3 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 95 80-120 2 16 Toluene 19 1.0 ug/L 20.0 0.14 U 97 71-120 2 17 Trichloroethene 19 1.0 ug/L 20.0 0.15 U 96 74-120 2 22 4-Bromofluorobenzene 61 u91L 50.0 122 53-136 Dibromofluoromethane 57 u9/L 50.0 114 67-129 Toluene-d8 60 u9/L 50.0 121 59-134 Batch IK10033 - EPA 5030E MS Blank (1K10033-BLK1) Prepared: 11/10/2021 13:59 Analyzed: 11/11/2021 00:31 Analvte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1, 2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dich loroethane 1,1-Dichloroethene 1,2,3-Trichloropropane 1,2-Di bromo-3-ch loropropane 1,2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,4-Dichlorobenzene 2-Butanone 2-Hexanone 4-Methyl-2-pentanone FINAL Result Flaa Q Units 0.17 U 1.0 ug/L 0.12 U 1.0 ug/L 0.28 U 1.0 ug/L 0.14 U 1.0 ug/L 0.13 U 1.0 ug/L 0.21 U 1.0 ug/L 0.23 U 1.0 ug/L 0.48 U 1.0 ug/L 0.66 U 1.0 ug/L 0.19 U 1.0 ug/L 0.21 U 1.0 ug/L 0.10 U 1.0 ug/L 0.19 U 1.0 ug/L 1.3 U 5.0 ug/L 0.88 U 5.0 ug/L 1.1 U 5.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 74 Of 81 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IK10033 - EPA 5030B MS - Continued Blank (1K10033-BLK1) Continued Prepared: 11/10/2021 13:59 Analyzed: 11/11/2021 00:31 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromofluorobenzene 58 ug/L 50.0 116 53-136 Dibromofluoromethane 53 ug/L 50.0 106 67-129 Toluene-d8 60 u91L 50.0 120 59-134 LCS (IK10033-BSI) Prepared: 11/10/2021 13:59 Analyzed: 11/10/2021 22:40 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 1.0 ug/L 20.0 90 75-133 Benzene 18 1.0 ug/L 20.0 92 80-134 Chlorobenzene 18 1.0 ug/L 20.0 89 80-120 Toluene 18 1.0 ug/L 20.0 92 71-120 Trichloroethene 18 1.0 ug/L 20.0 89 74-120 4-Bromofluorobenzene 58 ug/L 50.0 115 53-136 Dibromofluoromethane 56 u91L 50.0 112 67-129 Toluene-d8 60 u91L 50.0 119 59-134 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 75 Of 81 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IK10033 - EPA 5030B MS - Continued Matrix Spike (1K30033-MS1) Prepared: 11/10/2021 13:59 Analyzed: 11/10/2021 23:08 Source: CE16371-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 22 1.0 ug/L 20.0 0.21 U 109 75-133 Benzene 21 1.0 ug/L 20.0 0.15 U 105 80-134 Chlorobenzene 24 1.0 ug/L 20.0 3.8 102 80-120 Toluene 21 1.0 ug/L 20.0 0.14 U 106 71-120 Trichloroethene 22 1.0 ug/L 20.0 0.15 U 109 74-120 4-Bromofluorobenzene 58 u91L 50.0 116 53-136 Dibromofluoromethane 56 u91L 50.0 111 67-129 Toluene-d8 59 u91L 50.0 118 59-134 Matrix Spike Dup (1K10033-MSD1) Prepared: 11/10/2021 13:59 Analyzed: 11/10/2021 23:36 Source: CE16371-01 Spike Source %REC RPD Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 22 1.0 ug/L 20.0 0.21 U 109 75-133 0.4 20 Benzene 21 1.0 ug/L 20.0 0.15 U 105 80-134 0.2 17 Chlorobenzene 25 1.0 ug/L 20.0 3.8 104 80-120 1 16 Toluene 22 1.0 ug/L 20.0 0.14 U 109 71-120 2 17 Trichloroethene 22 1.0 ug/L 20.0 0.15 U 108 74-120 0.6 22 4-Bromofluorobenzene 59 u91L 50.0 118 53-136 Dibromofluoromethane 56 u91L 50.0 112 67-129 Toluene-d8 58 u91L 50.0 117 59-134 Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch IK02027 - EPA 50305 MS Blank (1K02027-BLK1) Prepared: 11/02/2021 00:00 Analyzed: 11/02/2021 12:02 Spike Source %REC RPD Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 0.80 U 2.0 ug/L Toluene-& 5.5 u91L 5.00 110 75-125 LCS (1K02027-BS1) Prepared: 11/02/2021 00:00 Analyzed: 11/02/2021 11:37 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 25 2.0 ug/L 25.0 102 80-133 Toluene-d8 5.1 u91L 5.00 103 75-125 Matrix Spike (1K02027-MS1) Prepared: 11/02/2021 00:00 Analyzed: 11/02/2021 21:19 Source: AE08658-12 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 26 2.0 ug/L 25.0 0.80 U 104 80-133 Toluene-d8 5.4 u91L 5.00 108 75-125 Matrix Spike Dup (11(02027-MSD1) Prepared: 11/02/2021 00:00 Analyzed: 11/02/2021 21:44 Source: AE08658-12 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 25 2.0 ug/L 25.0 0.80 U 102 80-133 2 19 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 76 Of 81 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 1 K02027 - EPA 5030B MS - Continued Matrix Spike Dup (1K02027-MSD1) Continued Prepared: 11/02/2021 00:00 Analyzed: 11/02/2021 21:44 Source: AE08658-12 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Toluene-d8 5.5 u91L 5.00 110 75-125 Batch IK02042 - EPA 5030B MS Blank (lK02042-BLK1) Prepared: 11/02/2021 13:32 Analyzed: 11/03/2021 00:44 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 0.80 U 2.0 ug/L Toluene-& 5.5 u91L 5.00 109 75-125 LCS (1K02042-B51) Prepared: 11/02/2021 13:32 Analyzed: 11/02/2021 23:01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 25 2.0 ug/L 25.0 100 80-133 Toluene-& 5.3 u91L 5.00 106 75-125 Matrix Spike (1K02042-MS1) Prepared: 11/02/2021 13:32 Analyzed: 11/02/2021 23:27 Source: CE13949-17 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 27 2.0 ug/L 25.0 0.80 U 109 80-133 Toluene-d8 5.4 u91L 5.00 108 75-125 Matrix Spike Dup (1K02042-MSD1) Prepared: 11/02/2021 13:32 Analyzed: 11/02/2021 23:52 Source: CE13949-17 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 27 2.0 uo/L 25.0 0.80 U 108 80-133 0.9 19 Toluene-d8 5.1 u91L 5.00 103 75-125 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 77 Of S1 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there is no impact. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 78 of 81 E U) O N ~Q a UI C) v z i � O 09 W U) z 0 V J LU o O N Z a N c 0 ..i N D W z o LLJ '(I m 'O O C _0 O C ro m 70 _ N TJ .. C' EO C Q mh ym x � E m 9E N (n E1J LD �Y E� a m _ m w cc d �U o n o J a U 1 Q C D U F V C m p m jn a W m = m da"i O � m Z m m m Z m V m a• m = y6� 0 1` x CL N' a U E E E fi 6 m m� - - m a � //'�{{ w ��[j �y} / � y� /''� p /''�/��p a WiS LdHC4s'peMua�'�.i Voqu'a s x x x x x x x x x X x x v V y O � V D G tip o CD CD CD w to CD 0 CD W 0 W (D Lr- p � �° �ta�aaaaaaada a� CD a V Q m C } 2 m m 9T 4 N N J O E [] rS Q�i m _o c ^ o v 4 U uzi o mft ' cc C v � n N ny N !v N L x m C D D L m r C (!} D + U ^ s E rw�t a m❑ d f!] a E ,�} c `2 r C*7 LLB r V- LL LL a M �S EL z a ? c3 � a d a Page 79 of 81 U CQ u7 ¢ M i3 IY Css r +✓ m n ro � y - w V a U 0 V IA 0 V 3 cc 0 V W cc 0 V. 0 Z Q 2 U U) W_ Q O a O m Q z O tiJ CA z 0 U LJ r z Lil 2 z O z LLI M NjI U m I 0 Ul ro Q ro C 1 m 9 N ro was r !JCL J N W o t r E N w c� o Y E m m a m tl cr z fl a v o Q � r c o S C U E m c m � ro c m Z � 0 A p 4 U m P-2 y S r 0 _ 0 ° ¢ ¢ ¢ p = N f9 ❑ ` ❑ O 1 N o QI YVl6 CMZO*PWL Jx3 ❑09Z8'U08Z6 7C �C X x iC X 7{ x ?t X X )C v �sC ` (D tD tp CD (D (D iD CD to (O tD (D E c E c Lo e E m- � a L Q a a a¢ a ¢¢ 2a 2Q Cc 0 N e a Ttl a v a 16 j c J (}[�� n m E U b 'Lf aC W C C m Z G U to m r( U S E_ ARQk E 3i ErJ c o �} ►� _ N N �p ^�,� h E P4 s 0 = ti m Nz v ((S�nJj"hjjJj to to C = d (6 L a.Ti h LT1 C C a w a, N � N r- IL c IV I 0 z a m ? a— E 0 5 r 25 e-- N r- F V- e- w V- 0 e- dD r � g ¢ a n m c co E� r m z CD t[3 m E a m E E Page 80 of 81 U 4 U h U1 0 G y U E 3 0 cc �2 0 �q rid M — 4 cc } � m .c ,0 ny L L/ O m U U zv lLavrn 0 z Q i U m_ c i £ m e N o ~ E a A cv °- �- � v CDcr U m co cr z � C N N m py C_ l6 p c U b¢ W N N O � U � y `o ro a � 0 U f7 a m UE ms a4gz9'PBPL"x3 aogzg,amz$ X X X X !C X t° J o RS cO d' q1t cn w to rop n C E F L7 (n E EC z z) a` EL I a m m U rj Y 1A N O F ri [� ca IN o I�i V 9 IL m a m m ry E a"ar h H 9 .n C7 Q U F- 0 co co � t7 m U C d E E E m m o is n m n Q d ro sn m c V D m } m ¢ s ICE Q � E m E v E m v � s Q 0 N 0. m m N m a (A m m N h Q c ¢Q c Q S y ` V W C 0 m m y � a m � N W Page 81 of £ C� U 3 2�SQ pCCgF ENCO Laboratories 9e0 Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Monday, November 8, 2021 Babb & Associates (BA024) Attn: Gary Babb 5506 Bradford Pear Court Raleigh, NC 27606 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Seaboard/Riverdale Landfill- SW Sampling ENCO Workorder(s): CE13951 Dear Gary Babb, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, October 22, 2021. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, 4P 0 ee Bill Scott Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 of 4O (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 4401-SW3 Lab ID: CE13951-01 Sampled: 10/21/21 09:20 Received: 10/22/21 10:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/04/21 10/28/21 11:10 10/28/21 14:58 EPA 8260D EPA 503013_MS 11/04/21 11/02/21 09:27 11/02/21 21:02 Client ID: 4401-SW4 Lab ID: CE13951-02 Sampled: 10/21/21 09:35 Received: 10/22/21 10:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/04/21 11/01/21 20:16 11/02/21 08:35 Client ID: 4401-SW4 Lab ID: CE13951-02RE1 Sampled: 10/21/21 09:35 Received: 10/22/21 10:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/04/21 10/29/21 11:05 10/29/21 21:33 EPA 8260D EPA 503013_MS 11/04/21 11/02/21 19:29 11/03/21 16:02 Client ID: 4401-SW5 Lab ID: CE13951-03 Sampled: 10/21/21 09:10 Received: 10/22/21 10:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 11/04/21 11/01/21 20:16 11/02/21 09:02 Client ID: 4401-SW5 Lab ID: CE13951-03RE1 Sampled: 10/21/21 09:10 Received: 10/22/21 10:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MIS 11/04/21 10/29/21 11:05 10/29/21 13:24 EPA 8260D EPA 503013_MS 11/04/21 11/02/21 16:29 11/02/21 22:57 Client ID: 4401-SW6Surface Lab ID: CE13951-04 Sampled: 10/21/21 10:10 Received: 10/22/21 10:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/04/21 10/28/21 11:10 10/28/21 16:15 EPA 8260D EPA 503013_MS 11/04/21 11/01/21 20:16 11/02/21 09:30 Client ID: 4401-SW6Bottom Lab ID: CE13951-05 Sampled: 10/21/21 10:20 Received: 10/22/21 10:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/04/21 10/28/21 11:10 10/28/21 16:40 EPA 8260D EPA 5030B_MS 11/04/21 11/01/21 20:16 11/02/21 09:57 Client ID: 4401-SW7Bottom Lab ID: CE13951-06 Sampled: 10/21/21 11:55 Received: 10/22/21 10:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MIS 11/04/21 10/28/21 11:10 10/28/21 17:06 EPA 8260D EPA 503013_MS 11/04/21 11/01/21 20:16 11/02/21 10:25 Client ID: 4401-SW7Surface Lab ID: CE13951-07 Sampled: 10/21/21 11:50 Received: 10/22/21 10:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/04/21 10/28/21 11:10 10/28/21 17:32 EPA 8260D EPA 503013_MS 11/04/21 11/01/21 20:16 11/02/21 10:52 Client ID: 4401-SWDRP2Bottom Lab ID: CE13951-08 Sampled: 10/21/21 11:30 Received: 10/22/21 10:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/04/21 10/28/21 11:10 10/28/21 17:58 EPA 8260D EPA 5030B_MS 11/04/21 11/01/21 20:16 11/02/21 11:20 Client ID: 4401-SWDRP2Surface Lab ID: CE13951-09 Sampled: 10/21/21 11:15 Received: 10/22/21 10:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MIS 11/04/21 10/28/21 11:10 10/28/21 18:23 EPA 8260D EPA 503013_MS 11/04/21 11/01/21 20:16 11/02/21 11:47 Client ID: 4401-SWDRP11Surface Lab ID: CE13951-10 Sampled: 10/21/21 12:30 Received: 10/22/21 10:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/04/21 10/28/21 11:10 10/28/21 18:49 EPA 8260D EPA 503013_MS 11/04/21 11/01/21 20:16 11/02/21 12:15 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 2 Of 40 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 4401-SWDRP11Bottom Lab ID: CE13951-11 Sampled: 10/21/21 12:40 Received: 10/22/21 10:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/04/21 10/28/21 11:10 10/28/21 19:15 EPA 8260D EPA 503013_MS 11/04/21 11/01/21 20:16 11/02/21 12:42 Client ID: 4401-TripBlank Lab ID: CE13951-12 Sampled: 10/21/21 09:10 Received: 10/22/21 10:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 11/04/21 10/28/21 11:10 10/28/21 19:40 EPA 8260D EPA 503013_MS 11/04/21 11/01/21 20:16 11/02/21 08:07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 Of 40 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 4401-SW3 Lab ID: CE13951-01 Analvte Results Flag MDL Q Units Method Notes 1,1,1-Trichloroethane 0.95 J 0.12 1.0 ug/L EPA 8260D 1,1-Dichloroethane 2.1 0.13 1.0 ug/L EPA 8260D 1,4-Dioxane 4.6 0.80 2.0 ug/L EPA 8260D cis-1,2-Dichloroethene 2.6 0.15 1.0 ug/L EPA 8260D Client ID: 4401-SW4 Lab ID: CE13951-02 Analvte Results Flag MDL PQL Units Method Notes 1,1,1-Trichloroethane 170 D 1.2 10 ug/L EPA 8260D 1,1-Dichloroethane 1100 D 1.3 10 ug/L EPA 8260D 1,1-Dichloroethene 670 D 2.1 10 ug/L EPA 8260D 1,2-Dichlorobenzene 9.3 ]D 1.9 10 ug/L EPA 8260D 1,2-Dichloroethane 120 D 2.1 10 ug/L EPA 8260D Chlorobenzene 1700 D 1.7 10 ug/L EPA 8260D Chloroethane 100 D 2.3 10 ug/L EPA 8260D Tetrachloroethene 18 D 1.7 10 ug/L EPA 8260D Toluene 11 D 1.4 10 ug/L EPA 8260D Client ID: 4401-SW4 Lab ID: CE13951-02RE3 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 1500 D 40 100 ug/L EPA 8260D cis-1,2-Dichloroethene 3300 D 7.5 50 ug/L EPA 8260D Vinyl chloride 1500 D 16 50 ug/L EPA 8260D Client ID: 4401-SWS Lab ID: CE13951-03RE3 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 2.2 0.80 2.0 ug/L EPA 8260D Client ID: 4401-SWDRP11Surface Lab ID: CE13951-10 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 1.4 J 0.80 2.0 ug/L EPA 8260D Client ID: 4401-SWDRP11Bottom Lab ID: CE13951-11 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 1.2 J 0.80 2.0 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 4 Of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW3 Lab Sample ID:CE13951-01 Received: 10/22/21 10:30 Matrix: Water Sampled: 10/21/2109:20 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref 1,1,1-Trichloroethane [71-55-6]^ 0.95 J ug/L 1 0.12 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref 1,1-Dichloroethane [75-34-3]^ 2.1 ug/L 1 0.13 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 1K02007 EPA 8260D 11/02/21 21:02 ref 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 1K02007 EPA 8260D 11/02/21 21:02 ref 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 1K02007 EPA 8260D 11/02/21 21:02 ref Acetone [67-64-1]^ 10 U ug/L 1 10 20 1K02007 EPA 8260D 11/02/21 21:02 ref Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 1K02007 EPA 8260D 11/02/21 21:02 ref Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 1K02007 EPA 8260D 11/02/21 21:02 ref Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref cis- 1,2-Dichloroethene [156-59-2]^ 2.6 ug/L 1 0.15 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 1K02007 EPA 8260D 11/02/21 21:02 ref m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 1K02007 EPA 8260D 11/02/21 21:02 ref Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 5 Of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW3 Lab Sample ID:CE13951-01 Received: 10/22/21 10:30 Matrix: Water Sampled: 10/21/2109:20 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1K02007 EPA 8260D 11/02/21 21:02 ref Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K02007 EPA 8260D 11/02/21 21:02 ref Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K02007 EPA 8260D 11/02/21 21:02 ref Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 53 1 50.0 105 % 53-136 IKO2007 EPA 8260D 11102121 21:02 ref Dlbromofluoromethane 57 1 50.0 115 % 67-129 IK02007 EPA 6260D 11102121 21:02 ref Toluene-& 58 1 50.0 116 % 59-134 IK02007 EPA 6260D 11102121 21:02 ref Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 4.6 ug/L 1 0.80 2.0 1128029 EPA 8260D 10/28/21 14:58 KKW Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 5.0 1 5.00 100 % 75-125 IJ28029 EPA 8260D 10128121 14:58 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 6 Of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW4 Lab Sample ID:CE13951-02 Received: 10/22/21 10:30 Matrix: Water Sampled: 10/21/2109:35 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 1.7 UD ug/L 10 1.7 10 1K01045 EPA 8260D 11/02/21 08:35 RKY 1,1,1-Trichloroethane [71-55-6]^ 170 D ug/L 10 1.2 10 1KO1045 EPA 8260D 11/02/21 08:35 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 2.8 UD ug/L 10 2.8 10 1K01045 EPA 8260D 11/02/21 08:35 RKY 1,1,2-Trichloroethane [79-00-5]^ 1.4 UD ug/L 10 1.4 10 1K01045 EPA 8260D 11/02/21 08:35 RKY 1,1-Dichloroethane [75-34-3]^ 1100 D ug/L 10 1.3 10 1KO1045 EPA 8260D 11/02/21 08:35 RKY 1,1-Dichloroethene [75-35-4]^ 670 D ug/L 10 2.1 10 1KO1045 EPA 8260D 11/02/21 08:35 RKY 1,2,3-Trichloropropane [96-18-4]^ 2.3 UD ug/L 10 2.3 10 1K01045 EPA 8260D 11/02/21 08:35 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 4.8 UD ug/L 10 4.8 10 1K01045 EPA 8260D 11/02/21 08:35 RKY 1,2-Dibromoethane [106-93-4]^ 6.6 UD ug/L 10 6.6 10 1K01045 EPA 8260D 11/02/21 08:35 RKY 1,2-Dichlorobenzene [95-50-1]^ 9.3 ]D ug/L 10 1.9 10 1KO1045 EPA 8260D 11/02/21 08:35 RKY 1,2-Dichloroethane [107-06-2]^ 120 D ug/L 10 2.1 10 1KO1045 EPA 8260D 11/02/21 08:35 RKY 1,2-Dichloropropane [78-87-5]^ 1.0 UD ug/L 10 1.0 10 1K01045 EPA 8260D 11/02/21 08:35 RKY 1,4-Dichlorobenzene [106-46-7]^ 1.9 UD ug/L 10 1.9 10 1K01045 EPA 8260D 11/02/21 08:35 RKY 2-Butanone [78-93-3]^ 13 UD ug/L 10 13 50 1K01045 EPA 8260D 11/02/21 08:35 RKY 2-Hexanone [591-78-6]^ 8.8 UD ug/L 10 8.8 50 1K01045 EPA 8260D 11/02/21 08:35 RKY 4-Methyl-2-pentanone[108-10-1]^ 11 UD ug/L 10 11 50 1K01045 EPA 8260D 11/02/21 08:35 RKY Acetone[67-64-1]^ 100 UD ug/L 10 100 200 1K01045 EPA 8260D 11/02/21 08:35 RKY Acrylonitrile [107-13-1]^ 35 UD ug/L 10 35 100 1K01045 EPA 8260D 11/02/21 08:35 RKY Benzene [71-43-2]^ 1.5 UD ug/L 10 1.5 10 1K01045 EPA 8260D 11/02/21 08:35 RKY Bromochloromethane [74-97-5]^ 4.8 UD ug/L 10 4.8 10 1K01045 EPA 8260D 11/02/21 08:35 RKY Bromodichloromethane [75-27-4]^ 1.7 UD ug/L 10 1.7 10 1K01045 EPA 8260D 11/02/21 08:35 RKY Bromoform [75-25-2]^ 2.2 UD ug/L 10 2.2 10 1K01045 EPA 8260D 11/02/21 08:35 RKY Bromomethane [74-83-9]^ 1.4 UD ug/L 10 1.4 10 1K01045 EPA 8260D 11/02/21 08:35 RKY Carbon disulfide [75-15-0]^ 15 UD ug/L 10 15 50 1K01045 EPA 8260D 11/02/21 08:35 RKY Carbon tetrachloride [56-23-5]^ 1.7 UD ug/L 10 1.7 10 1K01045 EPA 8260D 11/02/21 08:35 RKY Chlorobenzene [108-90-7]^ 1700 D ug/L 10 1.7 10 1KO1045 EPA 8260D 11/02/21 08:35 RKY Chloroethane [75-00-3]^ 100 D ug/L 10 2.3 10 1KO1045 EPA 8260D 11/02/21 08:35 RKY Chloroform [67-66-3]^ 1.8 UD ug/L 10 1.8 10 1K01045 EPA 8260D 11/02/21 08:35 RKY Chloromethane [74-87-3]^ 1.3 UD ug/L 10 1.3 10 1K01045 EPA 8260D 11/02/21 08:35 RKY cis- 1,2-Dichloroethene [156-59-2]^ 3300 D ug/L 50 7.5 50 1K02032 EPA 8260D 11/03/21 16:02 RKY cis- 1,3-Dichloropropene [10061-01-5]^ 2.0 UD ug/L 10 2.0 10 1K01045 EPA 8260D 11/02/21 08:35 RKY Dibromochloromethane [124-48-1]^ 1.7 UD ug/L 10 1.7 10 1K01045 EPA 8260D 11/02/21 08:35 RKY Dibromomethane [74-95-3]^ 2.7 UD ug/L 10 2.7 10 1K01045 EPA 8260D 11/02/21 08:35 RKY Ethylbenzene [100-41-4]^ 1.3 UD ug/L 10 1.3 10 1K01045 EPA 8260D 11/02/21 08:35 RKY Iodomethane[74-88-4]^ 17 UD ug/L 10 17 50 1K01045 EPA 8260D 11/02/21 08:35 RKY m,p-Xylenes [108-38-3/106-42-3]^ 1.7 UD ug/L 10 1.7 20 1K01045 EPA 8260D 11/02/21 08:35 RKY Methylene chloride [75-09-2]^ 2.3 UD ug/L 10 2.3 10 1K01045 EPA 8260D 11/02/21 08:35 RKY o-Xylene [95-47-6]^ 0.65 UD ug/L 10 0.65 10 1K01045 EPA 8260D 11/02/21 08:35 RKY Styrene [100-42-5]^ 1.1 UD ug/L 10 1.1 10 1K01045 EPA 8260D 11/02/21 08:35 RKY Tetrachloroethene [127-18-4]^ 18 D ug/L 10 1.7 10 1KO1045 EPA 8260D 11/02/21 08:35 RKY Toluene [108-88-3]^ 11 D ug/L 10 1.4 10 1KO1045 EPA 8260D 11/02/21 08:35 RKY trans-1,2-Dichloroethene [156-60-5]^ 2.1 UD ug/L 10 2.1 10 1K01045 EPA 8260D 11/02/21 08:35 RKY trans-1,3-Dichloropropene [10061-02-6]^ 1.5 UD ug/L 10 1.5 10 1K01045 EPA 8260D 11/02/21 08:35 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 7.0 UD ug/L 10 7.0 10 1K01045 EPA 8260D 11/02/21 08:35 RKY Trichloroethene [79-01-6]^ 1.5 UD ug/L 10 1.5 10 1K01045 EPA 8260D 11/02/21 08:35 RKY Trichlorofluoromethane [75-69-4]^ 2.4 UD ug/L 10 2.4 10 1K01045 EPA 8260D 11/02/21 08:35 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 7 Of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW4 Lab Sample ID:CE13951-02 Received: 10/22/21 10:30 Matrix: Water Sampled: 10/21/2109:35 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]^ 9.5 UD ug/L 10 9.5 50 1K01045 EPA 8260D 11/02/21 08:35 RKY Vinyl chloride [75-01-4]^ 1500 D ug/L 50 16 50 1K02032 EPA 8260D 11/03/21 16:02 RKY Xylenes (Total) [1330-20-7]^ 4.5 UD ug/L 10 4.5 30 1K01045 EPA 8260D 11/02/21 08:35 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 60 1 50.0 120 % 53-136 IKO1045 EPA 8260D 11102121 0825 RKY 4-Bromofluorobenzene 51 1 50.0 101 % 53-136 IK02032 EPA 6260D 11103121 16:02 RKY Dibromofluoromethane 47 1 50.0 95 % 67-129 IK01045 EPA 6260D 11102121 0625 RKY Dibromofluoromethane 51 1 50.0 102 % 67-129 IK02032 EPA 6260D 11103121 16:02 RKY Toluene-d8 50 1 50.0 100 % 59-134 IK01045 EPA 8260D 11102121 0625 RKY Toluene-d8 49 1 50.0 97 % 59-134 1KO2032 EPA 8260D 11103121 16:02 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1500 D ug/L 50 40 100 1129022 EPA 8260D 10/29/21 21:33 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 5.4 1 5.00 107 % 75-125 IJ29022 EPA 8260D 10129121 21:33 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 8 Of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW5 Lab Sample ID:CE13951-03 Received: 10/22/21 10:30 Matrix: Water Sampled: 10/21/2109:10 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 1K01045 EPA 8260D 11/02/21 09:02 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 1K01045 EPA 8260D 11/02/21 09:02 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 1K01045 EPA 8260D 11/02/21 09:02 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 1K01045 EPA 8260D 11/02/21 09:02 RKY Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY cis- 1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 1K02031 EPA 8260D 11/02/21 22:57 RKY cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 1K01045 EPA 8260D 11/02/21 09:02 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 9 Of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW5 Lab Sample ID:CE13951-03 Received: 10/22/21 10:30 Matrix: Water Sampled: 10/21/2109:10 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K01045 EPA 8260D 11/02/21 09:02 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 61 1 50.0 123 % 53-136 IKO1045 EPA 8260D 11102121 09:02 RKY 4-Bromofluorobenzene 66 1 50.0 131 % 53-136 IK02031 EPA 6260D 11102121 22:57 RKY Dibromofluoromethane 50 1 50.0 99 % 67-129 IK01045 EPA 6260D 11102121 09:02 RKY Dibromofluoromethane 57 1 50.0 114 % 67-129 IK02031 EPA 6260D 11102121 22:57 RKY Toluene-d8 52 1 50.0 103 % 59-134 IK01045 EPA 8260D 11102121 09:02 RKY Toluene-d8 61 1 50.0 121 % 59-134 IK02031 EPA 8260D 11102121 22:57 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 2.2 ug/L 1 0.80 2.0 1129022 EPA 8260D 10/29/21 13:24 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 5.1 1 5.00 101 % 75-125 IJ29022 EPA 8260D 10129121 13:24 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 10 of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW6Surface Lab Sample ID:CE13951-04 Received: 10/22/21 10:30 Matrix: Water Sampled:10/21/21 10: 10 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 1K01045 EPA 8260D 11/02/21 09:30 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 1K01045 EPA 8260D 11/02/21 09:30 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 1K01045 EPA 8260D 11/02/21 09:30 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 1K01045 EPA 8260D 11/02/21 09:30 RKY Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY cis- 1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 1K01045 EPA 8260D 11/02/21 09:30 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 11 of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW6Surface Lab Sample ID:CE13951-04 Received: 10/22/21 10:30 Matrix: Water Sampled:10/21/21 10:10 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K01045 EPA 8260D 11/02/21 09:30 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 57 1 50.0 114 % 53-136 IKO1045 EPA 8260D 11102121 09:30 RKY Dlbromofluoromethane 49 1 50.0 97 % 67-129 IKO1045 EPA 8260D 11102121 09:30 RKY Toluene-& 52 1 50.0 103 % 59-134 IK01045 EPA 6260D 11102121 09:30 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1J28029 EPA 8260D 10/28/21 16:15 KKW Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 5.2 1 5.00 103 % 75-125 IJ28029 EPA 8260D 10128121 16:15 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 12 of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW6Bottom Lab Sample ID:CE13951-05 Received: 10/22/21 10:30 Matrix: Water Sampled:10/21/21 10:20 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 1K01045 EPA 8260D 11/02/21 09:57 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 1K01045 EPA 8260D 11/02/21 09:57 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 1K01045 EPA 8260D 11/02/21 09:57 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 1K01045 EPA 8260D 11/02/21 09:57 RKY Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY cis- 1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 1K01045 EPA 8260D 11/02/21 09:57 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 13 Of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW6Bottom Lab Sample ID:CE13951-05 Received: 10/22/21 10:30 Matrix: Water Sampled:10/21/21 10:20 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K01045 EPA 8260D 11/02/21 09:57 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 61 1 50.0 122 % 53-136 IKO1045 EPA 8260D 11102121 09:57 RKY Dlbromofluoromethane 54 1 50.0 109 % 67-129 IK01045 EPA 6260D 11102121 09:57 RKY Toluene-& 52 1 50.0 105 % 59-134 IK01045 EPA 6260D 11102121 09:57 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1J28029 EPA 8260D 10/28/21 16:40 KKW Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 4.7 1 5.00 95 % 75-125 IJ28029 EPA 6260D 10128121 16:40 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 14 of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW7Bottom Lab Sample ID:CE13951-06 Received: 10/22/21 10:30 Matrix: Water Sampled:10/21/21 11:55 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 1K01045 EPA 8260D 11/02/21 10:25 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 1K01045 EPA 8260D 11/02/21 10:25 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 1K01045 EPA 8260D 11/02/21 10:25 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 1K01045 EPA 8260D 11/02/21 10:25 RKY Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY cis- 1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 1K01045 EPA 8260D 11/02/21 10:25 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 15 Of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW7Bottom Lab Sample ID:CE13951-06 Received: 10/22/21 10:30 Matrix: Water Sampled:10/21/21 11:55 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K01045 EPA 8260D 11/02/21 10:25 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 61 1 50.0 122 % 53-136 IKO1045 EPA 8260D 11102121 10:25 RKY Dlbromofluoromethane 57 1 50.0 115 % 67-129 IK01045 EPA 6260D 11102121 10:25 RKY Toluene-& 53 1 50.0 106 % 59-134 IK01045 EPA 6260D 11102121 10:25 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1J28029 EPA 8260D 10/28/21 17:06 KKW Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 5.2 1 5.00 104 % 75-125 IJ28029 EPA 8260D 10128121 17:06 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 16 of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW7Surface Lab Sample ID:CE13951-07 Received: 10/22/21 10:30 Matrix: Water Sampled:10/21/21 11:50 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 1K01045 EPA 8260D 11/02/21 10:52 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 1K01045 EPA 8260D 11/02/21 10:52 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 1K01045 EPA 8260D 11/02/21 10:52 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 1K01045 EPA 8260D 11/02/21 10:52 RKY Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY cis- 1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 1K01045 EPA 8260D 11/02/21 10:52 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 17 of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW7Surface Lab Sample ID:CE13951-07 Received: 10/22/21 10:30 Matrix: Water Sampled:10/21/21 11:50 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K01045 EPA 8260D 11/02/21 10:52 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 62 1 50.0 125 % 53-136 IKO1045 EPA 8260D 11102121 10:52 RKY Dlbromofluoromethane 49 1 50.0 98 % 67-129 IKO1045 EPA 8260D 11102121 10:52 RKY Toluene-& 51 1 50.0 103 % 59-134 IK01045 EPA 6260D 11102121 10:52 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1J28029 EPA 8260D 10/28/21 17:32 KKW Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 5.0 1 5.00 101 % 75-125 IJ28029 EPA 8260D 10128121 1732 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 18 of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SWDRP2Bottom Lab Sample ID:CE13951-08 Received: 10/22/21 10:30 Matrix: Water Sampled:10/21/21 11:30 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 1K01045 EPA 8260D 11/02/21 11:20 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 1K01045 EPA 8260D 11/02/21 11:20 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 1K01045 EPA 8260D 11/02/21 11:20 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 1K01045 EPA 8260D 11/02/21 11:20 RKY Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY cis- 1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 1K01045 EPA 8260D 11/02/21 11:20 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 19 of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SWDRP2Bottom Lab Sample ID:CE13951-08 Received: 10/22/21 10:30 Matrix: Water Sampled:10/21/21 11:30 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K01045 EPA 8260D 11/02/21 11:20 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 65 1 50.0 129 % 53-136 IKO1045 EPA 8260D 11102121 11:20 RKY Dlbromofluoromethane 55 1 50.0 ill % 67-129 IK01045 EPA 6260D 11102121 11:20 RKY Toluene-& 54 1 50.0 109 % 59-134 IK01045 EPA 6260D 11102121 11:20 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1J28029 EPA 8260D 10/28/21 17:58 KKW Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 5.4 1 5.00 107 % 75-125 IJ28029 EPA 8260D 10128121 17:58 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 20 of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SWDRP2Surface Lab Sample ID:CE13951-09 Received: 10/22/21 10:30 Matrix: Water Sampled:10/21/21 11:15 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 1K01045 EPA 8260D 11/02/21 11:47 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 1K01045 EPA 8260D 11/02/21 11:47 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 1K01045 EPA 8260D 11/02/21 11:47 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 1K01045 EPA 8260D 11/02/21 11:47 RKY Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY cis- 1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 1K01045 EPA 8260D 11/02/21 11:47 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 21 of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SWDRP2Surface Lab Sample ID:CE13951-09 Received: 10/22/21 10:30 Matrix: Water Sampled:10/21/21 11:15 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K01045 EPA 8260D 11/02/21 11:47 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 66 1 50.0 132 % 53-136 IKO1045 EPA 8260D 11102121 11:47 RKY Dlbromofluoromethane 53 1 50.0 106 % 67-129 IK01045 EPA 6260D 11102121 11:47 RKY Toluene-& 56 1 50.0 112 % 59-134 IK01045 EPA 6260D 11102121 11:47 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1J28029 EPA 8260D 10/28/21 18:23 KKW Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 5.0 1 5.00 101 % 75-125 IJ28029 EPA 8260D 10128121 18:23 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 22 of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SWDRP11Surface Lab Sample ID:CE13951-10 Received: 10/22/21 10:30 Matrix: Water Sampled:10/21/21 12:30 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 1K01045 EPA 8260D 11/02/21 12:15 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 1K01045 EPA 8260D 11/02/21 12:15 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 1K01045 EPA 8260D 11/02/21 12:15 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 1K01045 EPA 8260D 11/02/21 12:15 RKY Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY cis- 1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 1K01045 EPA 8260D 11/02/21 12:15 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 23 of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SWDRPllSurface Lab Sample ID:CE13951-10 Received: 10/22/21 10:30 Matrix: Water Sampled:10/21/21 12:30 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K01045 EPA 8260D 11/02/21 12:15 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 64 1 50.0 128 % 53-136 IKO1045 EPA 8260D 11102121 12:15 RKY Dlbromofluoromethane 53 1 50.0 107 % 67-129 IK01045 EPA 6260D 11102121 12:15 RKY Toluene-& 56 1 50.0 ill % 59-134 IK01045 EPA 6260D 11102121 12:15 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.4 1 ug/L 1 0.80 2.0 1128029 EPA 8260D 10/28/21 18:49 KKW Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 5.1 1 5.00 103 % 75-125 IJ28029 EPA 8260D 10128121 18:49 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 24 of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SWDRP11Bottom Lab Sample ID:CE13951-11 Received: 10/22/21 10:30 Matrix: Water Sampled:10/21/21 12:40 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 1K01045 EPA 8260D 11/02/21 12:42 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 1K01045 EPA 8260D 11/02/21 12:42 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 1K01045 EPA 8260D 11/02/21 12:42 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 1K01045 EPA 8260D 11/02/21 12:42 RKY Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY cis- 1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 1K01045 EPA 8260D 11/02/21 12:42 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 25 Of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SWDRP11Bottom Lab Sample ID:CE13951-11 Received: 10/22/21 10:30 Matrix: Water Sampled:10/21/21 12:40 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K01045 EPA 8260D 11/02/21 12:42 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 62 1 50.0 125 % 53-136 IKO1045 EPA 8260D 11102121 12:42 RKY Dlbromofluoromethane 54 1 50.0 108 % 67-129 IK01045 EPA 6260D 11102121 12:42 RKY Toluene-& 56 1 50.0 ill % 59-134 IK01045 EPA 6260D 11102121 12:42 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.2 1 ug/L 1 0.80 2.0 1128029 EPA 8260D 10/28/21 19:15 KKW Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 5.1 1 5.00 103 % 75-125 IJ28029 EPA 8260D 10128121 19:15 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 26 of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-Trip Blank Lab Sample ID:CE13951-12 Received: 10/22/21 10:30 Matrix: Water Sampled: 10/21/2109:10 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 1K01045 EPA 8260D 11/02/21 08:07 RKY 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 1K01045 EPA 8260D 11/02/21 08:07 RKY 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Acetone [67-64-1]^ 10 U ug/L 1 10 20 1K01045 EPA 8260D 11/02/21 08:07 RKY Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 1K01045 EPA 8260D 11/02/21 08:07 RKY Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY cis- 1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 1K01045 EPA 8260D 11/02/21 08:07 RKY m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 27 Of 40 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-TripBlank Lab Sample ID:CE13951-12 Received: 10/22/21 10:30 Matrix: Water Sampled: 10/21/2109:10 Work Order: CE13951 Project: Seaboard/Riverdale Landfill- SW Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 1K01045 EPA 8260D 11/02/21 08:07 RKY Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 62 1 50.0 124 % 53-136 IKO1045 EPA 8260D 11102121 06:07 RKY Dlbromofluoromethane 48 1 50.0 95 % 67-129 IKO1045 EPA 8260D 11102121 06:07 RKY Toluene-& 50 1 50.0 100 % 59-134 IK01045 EPA 6260D 11102121 06:07 RKY Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 1J28029 EPA 8260D 10/28/21 19:40 KKW Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 5.4 1 5.00 109 % 75-125 IJ28029 EPA 8260D 10128121 19:40 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 28 Of 40 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1K01045 - EPA 5030E M5 Blank (1K03045-BLKS) Prepared: 11/01/2021 20:16 Analyzed: 11/02/2021 07:40 Analvte Result Flaq POL Units 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC Level Result %REC Limits RPD RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 29 Of 40 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1 K01045 - EPA 5030B MS - Continued Blank (SK03045-BLKS) Continued Prepared: 11/01/2021 20:16 Analyzed: 11/02/2021 07:40 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 64 u91L 50.0 128 53-136 Dibromofluoromethane 51 u91L 50.0 102 67-129 Toluene-d8 51 u91L 50.0 102 59-134 LCS (11(01045-BS1) Prepared: 11/01/2021 20:16 Analyzed: 11/02/2021 05:50 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 17 1.0 ug/L 20.0 85 75-133 Benzene 17 1.0 ug/L 20.0 85 80-134 Chlorobenzene 18 1.0 ug/L 20.0 91 80-120 Toluene 22 1.0 ug/L 20.0 108 71-120 Trichloroethene 21 1.0 ug/L 20.0 106 74-120 4-Bromofluorobenzene 61 u91L 50.0 122 53-136 Dibromofluoromethane 48 u91L 50.0 96 67-129 Toluene-d8 51 u91L 50.0 103 59-134 Matrix Spike (1K01045-MS1) Prepared: 11/01/2021 20:16 Analyzed: 11/02/2021 06:17 Source: CE16545-10 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 22 1.0 ug/L 20.0 0.21 U 109 75-133 Benzene 18 1.0 ug/L 20.0 0.15 U 92 80-134 Chlorobenzene 21 1.0 ug/L 20.0 0.17 U 103 80-120 Toluene 24 1.0 ug/L 20.0 0.14 U 121 71-120 QM-07 Trichloroethene 21 1.0 ug/L 20.0 0.15 U 103 74-120 4-Bromofluorobenzene 60 u91L 50.0 120 53-136 Dibromofluoromethane 46 u91L 50.0 93 67-129 Toluene-d8 50 u91L 50.0 99 59-134 Matrix Spike Dup (1K03045-MSD1) Prepared: 11/01/2021 20:16 Analyzed: 11/02/2021 06:45 Source: CE16545-10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 17 1.0 ug/L 20.0 0.21 U 84 75-133 26 20 QM-11 Benzene 16 1.0 ug/L 20.0 0.15 U 80 80-134 13 17 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 88 80-120 16 16 Toluene 20 1.0 ug/L 20.0 0.14 U 102 71-120 17 17 Trichloroethene 18 1.0 ug/L 20.0 0.15 U 88 74-120 16 22 4-Bromofluorobenzene 62 u91L 50.0 124 53-136 Dibromofluoromethane 47 u91L 50.0 95 67-129 Toluene-d8 50 u91L 50.0 100 59-134 Batch ZK02007 -EPA 5030B MS Blank (lK02007-BLK1) Prepared: 11/02/2021 09:27 Analyzed: 11/02/2021 17:52 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 30 Of 40 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1 K02007 - EPA 5030B MS - Continued Blank (SK02007-BLKS) Continued Prepared: 11/02/2021 09:27 Analyzed: 11/02/2021 17:52 Analvte Result Flaq POL Units 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 53 u9/L 50.0 106 53-136 Dibromofluoromethane 55 u9/L 50.0 110 67-129 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 31 of 40 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1 K02007 - EPA 5030B MS - Continued Blank (SK02007-BLKS) Continued Prepared: 11/02/2021 09:27 Analyzed: 11/02/2021 17:52 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Toluene-d8 56 u91L 50.0 115 59-134 LCS (1K02007-BS1) Prepared: 11/02/2021 09:27 Analyzed: 11/02/2021 16:03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 102 75-133 Benzene 20 1.0 ug/L 20.0 100 80-134 Chlorobenzene 18 1.0 ug/L 20.0 92 80-120 Toluene 18 1.0 ug/L 20.0 92 71-120 Trichloroethene 21 1.0 ug/L 20.0 104 74-120 4-Bromofluorobenzene 55 ug/L 50.0 109 53-136 Dibromofluoromethane 55 ug/L 50.0 110 67-129 Toluene-d8 57 ug/L 50.0 115 59-134 Matrix Spike (1K02007-MS1) Prepared: 11/02/2021 09:27 Analyzed: 11/02/2021 16:30 Source: CE16545-05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 23 1.0 ug/L 20.0 0.21 U 113 75-133 Benzene 22 1.0 ug/L 20.0 0.15 U 108 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 96 80-120 Toluene 20 1.0 ug/L 20.0 0.14 U 100 71-120 Trichloroethene 22 1.0 ug/L 20.0 0.15 U 108 74-120 4-Bromofluorobenzene 55 ug/L 50.0 109 53-136 Dibromofluoromethane 56 ug/L 50.0 111 67-129 Toluene-d8 58 u91L 50.0 116 59-134 Matrix Spike Dup (1K02007-MSD1) Prepared: 11/02/2021 09:27 Analyzed: 11/02/2021 16:58 Source: CE16545-05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 0.21 U 104 75-133 8 20 Benzene 21 1.0 ug/L 20.0 0.15 U 104 80-134 4 17 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 91 80-120 6 16 Toluene 19 1.0 ug/L 20.0 0.14 U 94 71-120 6 17 Trichloroethene 22 1.0 ug/L 20.0 0.15 U 109 74-120 0.4 22 4-Bromofluorobenzene 55 u91L 50.0 110 53-136 Dibromofluoromethane 55 u91L 50.0 110 67-129 Toluene-& 56 u91L 50.0 112 59-134 Batch IK02031 - EPA 5030B MS Blank (lK02031-BLKI) Prepared: 11/02/2021 16:29 Analyzed: 11/02/2021 20:40 Spike Source %REC Analvte Result Flaq POL Units Level Result %REC Limits 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L RPD RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full Page 32 of 40 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IK02031 - EPA 5030B MS - Continued Blank (SK02031-BLKS) Continued Prepared: 11/02/2021 16:29 Analyzed: 11/02/2021 20:40 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromofluorobenzene 69 u91L 50.0 138 53-136 QS-03 Dibromofluoromethane 59 u91L 50.0 118 67-129 Toluene-d8 62 u91L 50.0 124 59-134 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 33 Of 40 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IK02031 - EPA 5030B MS - Continued LCS (1K02031-BS1) Prepared: 11/02/2021 16:29 Analyzed: 11/02/2021 18:50 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 1.0 ug/L 20.0 91 75-133 Benzene 17 1.0 ug/L 20.0 83 80-134 Chlorobenzene 19 1.0 ug/L 20.0 95 80-120 Toluene 21 1.0 ug/L 20.0 107 71-120 Trichloroethene 17 1.0 ug/L 20.0 85 74-120 4-Bromofluorobenzene 65 ug/L 50.0 130 53-136 Dibromofluoromethane 60 u91L 50.0 120 67-129 Toluene-d8 61 u91L 50.0 122 59-134 Matrix Spike (1K02031-MS1) Prepared: 11/02/2021 16:29 Analyzed: 11/02/2021 19:17 Source: CE16545-07 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 1.0 ug/L 20.0 0.21 U 88 75-133 Benzene 17 1.0 ug/L 20.0 0.15 U 87 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 96 80-120 Toluene 22 1.0 ug/L 20.0 0.14 U 112 71-120 Trichloroethene 19 1.0 ug/L 20.0 0.15 U 95 74-120 4-Bromofluorobenzene 66 ug/L 50.0 133 53-136 Dibromofluoromethane 56 u91L 50.0 113 67-129 Toluene-d8 61 ug/L 50.0 122 59-134 Matrix Spike Dup (1K02031-MSD1) Prepared: 11/02/2021 16:29 Analyzed: 11/02/2021 19:45 Source: CE16545-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 1.0 ug/L 20.0 0.21 U 89 75-133 0.2 20 Benzene 18 1.0 ug/L 20.0 0.15 U 89 80-134 2 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 96 80-120 0 16 Toluene 23 1.0 ug/L 20.0 0.14 U 113 71-120 1 17 Trichloroethene 18 1.0 ug/L 20.0 0.15 U 91 74-120 4 22 4-Bromofluorobenzene 67 u91L 50.0 134 53-136 Dibromofluoromethane 54 u91L 50.0 108 67-129 Toluene-d8 61 u91L 50.0 122 59-134 Batch IK02032 -EPA 5030E MS Blank (1K02032-BLK1) Prepared: 11/02/2021 19:29 Analyzed: 11/03/2021 07:41 Spike Source %REC Analvte Result Flaq POL Units Level Result %REC Limits 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. RPD RPD Limit Notes Page 34 of 40 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch IK02032 - EPA 5030B MS - Continued Blank (SK02032-BLKS) Continued Prepared: 11/02/2021 19:29 Analyzed: 11/03/2021 07:41 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromofluorobenzene 48 u9/L 50.0 97 53-136 Dibromofluoromethane 47 u9/L 50.0 93 67-129 Toluene-d8 46 u9/L 50.0 91 59-134 LCS (IK02032-BSI) Prepared: 11/02/2021 19:29 Analyzed: 11/03/2021 05:44 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 102 75-133 Benzene 20 1.0 ug/L 20.0 102 80-134 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 35 Of 40 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 1K02032 - EPA 5030B MS - Continued LCS (1K02032-BS3) Continued Prepared: 11/02/2021 19:29 Analyzed: 11/03/2021 05:44 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chlorobenzene 15 1.0 ug/L 20.0 75 80-120 A-07 Toluene 19 1.0 ug/L 20.0 94 71-120 Trichloroethene 25 1.0 ug/L 20.0 126 74-120 QL-02 4-Bromofluorobenzene 55 u91L 50.0 110 53-136 Dibromofluoromethane 46 u91L 50.0 96 67-129 Toluene-d8 46 u91L 50.0 93 59-134 Matrix Spike (1K02032-MS1) Prepared: 11/02/2021 19:29 Analyzed: 11/03/2021 06:14 Source: CE15679-16 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 23 1.0 ug/L 20.0 0.21 U 114 75-133 Benzene 21 1.0 ug/L 20.0 0.15 U 103 80-134 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 92 80-120 Toluene 16 1.0 ug/L 20.0 0.14 U 82 71-120 Trichloroethene 23 1.0 ug/L 20.0 0.15 U 116 74-120 4-Bromofluorobenzene 49 u91L 50.0 98 53-136 Dibromofluoromethane 47 u91L 50.0 94 67-129 Toluene-d8 46 u91L 50.0 91 59-134 Matrix Spike Dup (1K02032-MSD1) Prepared: 11/02/2021 19:29 Analyzed: 11/03/2021 06:43 Source: CE15679-16 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 24 1.0 ug/L 20.0 0.21 U 122 75-133 7 20 Benzene 23 1.0 ug/L 20.0 0.15 U 115 80-134 11 17 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 99 80-120 8 16 Toluene 18 1.0 ug/L 20.0 0.14 U 88 71-120 6 17 Trichloroethene 26 1.0 ug/L 20.0 0.15 U 128 74-120 10 22 QM-07 4-Bromofluorobenzene 48 u91L 50.0 95 53-136 Dibromofluoromethane 47 u91L 50.0 95 67-129 Toluene-d8 46 u91L 50.0 92 59-134 Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch IJ28029 - EPA 5030E MS Blank (1328029-BLK3) Prepared: 10/28/2021 00:00 Analyzed: 10/28/2021 12:17 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 0.80 U 2.0 ug/L Toluene-d8 5.0 u91L 5.00 101 75-125 LCS (1328029-BSI) Prepared: 10/28/2021 00:00 Analyzed: 10/28/2021 11:51 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 26 2.0 ug/L 25.0 104 80-133 Toluene-d8 5.2 u91L 5.00 103 75-125 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 36 Of 40 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 1128029 - EPA 5030B MS - Continued Matrix Spike (1328029-MS3) Prepared: 10/28/2021 00:00 Analyzed: 10/28/2021 21:23 Source: AE08570-01 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 26 2.0 ug/L 25.0 0.80 U 103 80-133 Toluene-& 5.3 ug/L 5.00 107 75-125 Matrix Spike Dup (1728029-MSD1) Prepared: 10/28/2021 00:00 Analyzed: 10/28/2021 21:48 Source: AE08570-01 Analvte 1.4-Dioxane Spike Result Flag POL Units Level 26 2.0 ug/L 25.0 Source %REC RPD Result %REC Limits RPD Limit Notes 0.80 U 104 80-133 0.4 19 Toluene-d8 5.1 ug/L 5.00 101 75-125 Batch 1129022 - EPA 5030E MS Blank (1329022-BLK3) Prepared: 10/29/2021 00:00 Analyzed: 10/29/2021 11:35 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 0.80 U 2.0 ug/L Toluene-d8 5.2 u91L 5.00 104 75-125 LCS (1729022-BS1) Prepared: 10/29/2021 00:00 Analyzed: 10/29/2021 11:09 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 24 2.0 ug/L 25.0 96 80-133 Toluene-d8 5.5 ug/L 5.00 109 75-125 Matrix Spike (1329022-MS1) Prepared: 10/29/2021 00:00 Analyzed: 10/29/2021 21:58 Source: AE08586-02 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 30 2.0 ug/L 25.0 5.8 97 80-133 Toluene-d8 5.0 u91L 5.00 101 75-125 Matrix Spike Dup (1729022-MSD1) Prepared: 10/29/2021 00:00 Analyzed: 10/29/2021 22:24 Source: AE08586-02 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 30 2.0 ug/L 25.0 5.8 98 80-133 0.2 19 Toluene-d8 5.1 ug/L 5.00 101 75-125 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 37 Of 4O (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. A-07 Analyte biased low in LCS but detected in the reporting limit standard. Since the analyte in the associated sample was not detected, there is no impact on data quality. QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits. QS-03 Surrogate recovery outside acceptance limits QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there is no impact. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 38 of 4O i I 0 G E N �L E o C a O E a x CD N~ h LLJ q W a a:V Z � D m � o e U d � m m N O S fA a E' m a � O U 0 4 al W15 aoWS' l XIPueddtf (logn X x X x V O U �yT Ln' od K V a N�Y O EC E.8 ZO z" m r(D �� W C a a cc m m a U 44 co i�O i j 0 r G b co IL cr) FS N Z co Z� - U v D U U C4 E r � E E m ono Cl Q U O U O U 1 = a j } j .m cc a E m E F E F o d m c C O m i m LL m a m �N cr Q 0 U d� W O C� �Ir cc c m m Q c cc n a E Page 39 of 4 U! U O LU It 0 0 N Q m � p U m z ti O 5 v aL a u p w to z O U LU 5z Ifi ❑ � v z �_ N OWN cc U d m a z f- o W�o`v 0 C: CY) w "' C w v u v1 w E o m m g X ro I m c W cr W v aC z a o w m m Q a ayi N a cn e Z `y C a � U 0 st al wis aaazs' L xipuaddd aooza x x x x x x x x x x x x v 8 V C W M W CD W Cc M c CD co � m S. o 1 U � y CD m m 0 E o L E � c� = m �N" z z m o rn 1 VJ - a` a` a ¢ m in m ❑ w a N 777 \ _4 co 0 + _ y U) M i _ Q wJ W LL M E ~� M ti ti❑❑ C7 n N t]i N N co co to co co to tq to to th U! z �(.y�yj 15 W ml' U C U Fv rn in ro r3 ..r a U G m `� E \ k w ' E m m E m 0 0 0 m Q $ a rr (D U f0i Q O a c C U A 0 @ In m a � V yy V m � m Ir N w r E E � w ro o w E k m � E E m ro 5 m .� m c a m � EE 9 .8 y w , ? y D a C a s l m 0 Q m m c a m m m E a_ Y C E Page 40 of 4 U) U