3902_Granville_Butner_MSWLF_Aug21GW_FID1627138_20211215

GARRETT ■
& MOORE�
Engineering for the Power and Waste Industries
December 14, 2021
Ms. Jaclynne Drummond
Department. of Environmental Quality
Solid Waste Section
Asheville Regional Office
2090 US Highway 70
Swannanoa, North Carolina 28778
0aclynne.drummond(a)ncdenr.gov
RE: Water Quality Monitoring Report — August 2021 Event
Granville County Butner Landfill
Butner, North Carolina
Permit # 39-02
Dear Jackie:
On behalf of Granville County, please find attached the Water Quality Monitoring Report for the
Butner Landfill for the 2nd semi-annual sampling event of 2021. If you have any questions or
require further assistance regarding this matter, please do not hesitate to call me at 919-792-
1903.
Sincerely,
Garrett & Moore, Inc.
Stefan Bray, P.E.
Cc: Jason Falls, Granville County
1029 West South Street • Raleigh, North Carolina 27 • O: 919-792-1900 • F: 866-311-7206

DENR USE ONLY ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #:
NC DENR Environmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Garrett & Moore, Inc.
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Stefan Bray Phone: [phone]
E-mail: [e-mail]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Granville County State Road 1004 39-02 .1600 August 19, 2021
Butner Landfill Butner, NC 27565
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring ❑ Detection Monitoring ❑X Assessment Monitoring Corrective Action
Tie of data submitted: (Check all that apply)
X Groundwater monitoring data from monitoring wells Methane gas monitoring data
Groundwater monitoring data from private water supply wells ❑X Corrective action data (specify) MNA Parameters
Leachate monitoring data
X Surface water monitoring data Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Brian Boutin, PG Consltant for Facility 919-791-8903
Facility Representative Name (Print) Title (Area Code) Telephone Number
Brian S . Boutin Digitai,ned by Brian S. 6outin Affix NC Licensed/ Professional Geologist Seal
-Brianian S.
Boutin, email= [e-mail] 12/14/2021 9
Date: 2021.12.14 1114:37 EST
Signature Date
1029 West South St., Raleigh, NC 27603
Facility Representative Address
C-2910
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009

Granville County Butner landfill
Permit No. 39-02
Water Quality Monitoring Report
December 2021
Prepared By:
GARRETT
Z)!2P21�E
Engineering for the Power and Waste Industries
1029 W South Street
Raleigh, North Carolina 27603 • O: 919-792-1900 • F: 866-311-7206
NC FIRM C-2910

Water Quality Monitoring Report — December 2021
Granville County Butner Landfill — Permit No. 39-02
Contents
1 - INTRODUCTION.................................................................................................................................1
2 - GROUNDWATER GAUGING AND WATER SAMPLE COLLECTION................................................1
3 - RESULTS OF GROUNDWATER AND SURFACE WATER ANALYSIS.............................................3
4 - CORRECTIVE ACTION EVALUATION...............................................................................................4
5 - CONCLUSIONS..................................................................................................................................5
FIGURES
TABLES
.::
APPENDIX A - FIELD DATA LOGS
APPENDIX B - LABORATORY ANALYTICAL REPORTS
APPENDIX C - HISTORICAL GROUNDWATER ELEVATIONS
APPENDIX D - HISTORICAL CONSTITUENTS IN GROUNDWATER
APPENDIX E - HISTORICAL CONSTITUENTS IN SURFACE WATER
APPENDIX F - HISTORICAL MONITORING NATURAL ATTENUATION PARAMETERS
GAMM rU ZAP
& MOORE'A
Engineering for the Power and Waste Industries

Water Quality Monitoring Report — December 2021
Granville County Butner Landfill — Permit No. 39-02
1 INTRODUCTION
Site Information
The Butner Landfill is a closed municipal solid waste (MSW) landfill, located off State Route 1004 near the
town of Butner, in Granville County, North Carolina (Figure 1). The Butner facility started receiving solid
waste prior to May 1973. Permit Number 39- 02 was issued by the State of North Carolina on March 3,
1982. The facility stopped receiving solid waste in August 1998. At the present, a small recycling center
and transfer station are operated by the County of Granville at the entrance of the closed landfill.
Regulatory Status
The site is currently in Assessment Monitoring and a Corrective Action Monitoring Program. Groundwater
samples are collected semiannually and analyzed in accordance with the approved Corrective Action
Plan. Surface water samples are collected and sampled for Appendix I of 40 CFR Part 258, from here on
known as North Carolina Appendix I list of constituents during each sampling event.
The Butner Landfill entered an Assessment Monitoring Program in December of 1997 because of
detections of volatile organic compounds and pesticides above the North Carolina 2L (NC2L) Groundwater
Standards. An Assessment of Corrective Measures (ACM) was initiated in 2003, and then suspended by
NCDEQ since there had been no more NC2L exceedances. The Nature and Extent Study (NES) and ACM
were recommenced in 2007 when apparent volatile organic compound (VOC) exceedances of the NC2L
Standards began to appear; however, they were again suspended when it was determined that the
apparent exceedances were not statistically significant increases (SSTs) above background. An ACM was
reinitiated after an exceedance of benzene in monitoring well MW-2R in December 2012 and was
submitted to NCDENR in May 2013. Approval of the ACM was granted in a letter from NCDEQ dated June
27, 2013. A Corrective Action Plan (CAP) for monitored natural attenuation (MNA) plus phytoremediation
was submitted to NCDEQ on May 23, 2014, and was approved by NCDEQ on June 18, 2014.
Groundwater Monitoring Program
The groundwater monitoring program at the Butner Landfill consists of the following seven monitoring
wells: MW- 1 R (facility background well), MW- 2R, MW- 3R, MW-4, MW- 5, MW- 6, and NES-1. The
locations of the groundwater monitoring wells, and other site features are identified on Figure 2. A
summary of well construction details is provided in Table 1.
Surface Water Monitoring Program
The surface monitoring program at the Butner Landfill consists of two surface water sampling points, SW-
1 and SW-2, which are located respectively upstream and downstream of the facility, along an unnamed
tributary of Picture Creek. The locations of the surface monitoring points are identified on Figure 2.
2 GROUNDWATER GAUGING AND WATER SAMPLE COLLECTION
Groundwater levels were gauged in groundwater monitoring wells MW- 1 R, MW- 2R, MW- 3R, MW-4,
MW- 5, MW- 6, and NES-1 on August 19, 2021, as part of the site monitoring. Depths to groundwater
were measured using an electronic interface probe that was thoroughly decontaminated between wells
with a non -phosphate soap and water wash followed in order by multiple rinses with distilled water, an
isopropyl alcohol rinse, and multiple distilled water rinses. Depth to water measurements were made after
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Water Quality Monitoring Report — December 2021
Granville County Butner Landfill — Permit No. 39-02
the wells were opened for a sufficient period of time to allow water levels to equilibrate with atmospheric
pressure. Groundwater elevations collected on August 19, 2021, are presented in Table 2.
Groundwater samples were collected from the downgradient site monitoring wells on August 19, 2021, for
laboratory analysis to monitor the quality of groundwater at the site with respect to the 40 CFR Part 258
Appendix II List of Hazardous Inorganic and Organic Constituents. The groundwater samples were
collected and handled in accordance with the sampling protocols included in the site Water Quality
Monitoring Plan as well as the SWS Groundwater Monitoring Guidance Document. It is noted that
monitoring well MW-1 R serves as the upgradient, natural background well for the facility, and monitoring
wells MW-2R, MW- 2R, MW- 3R, MW-4, MW- 5, MW- 6, and NES-1serving as the downgradient
monitoring wells. All reusable sampling equipment was properly decontaminated between sampling
locations with a non -phosphate soap and water wash, followed by multiple rinses with distilled water. New
disposable nitrile or latex gloves were worn during all sampling activities. Disposable sampling
equipment/material was discarded after each use.
Prior to groundwater sampling, the monitoring wells were purged of a minimum of six well volumes of
water using a peristaltic pump under low flow (<_200 ml/min.) conditions. During purging, measurements
were made in the field of the pH, temperature, specific conductance oxygen reduction potential (ORP),
dissolved oxygen and turbidity of the groundwater collected from the monitoring wells. The results of the
field analyses of these parameters are presented in Table 3. Copies of Groundwater Sampling Forms
containing pertinent information recorded in the field during purging and sampling at each groundwater
monitoring well are presented in Appendix A.
The results of the field -measured water -quality parameters indicate that the values measured in
groundwater collected from the site monitoring wells were generally within applicable stabilization criteria
(± 10%; see Groundwater Sampling Forms). Groundwater at the site is acidic based on the pH values
measured in the field (4.94 to 6.60). Specific conductance values ranged from 125 (NES-1) to 2,062 (MW-
2R) pS/cm in groundwater at the monitoring wells. Turbidity values ranged from 0.02 (MW-2R, 3R) to
22.1 (MW-1 R) NTUs. After field parameters had stabilized over three consecutive recording intervals,
groundwater samples were collected using the same tubing that was used to purge the well. The samples
were decanted directly into laboratory prepared containers, which were then placed into ice -filled coolers
and shipped under proper chain -of -custody to Pace Analytical Services, Inc. (Pace) for analysis.
Surface water samples were collected from sampling locations SW-1 and SW-2 (Figure 2). New
disposable nitrile or latex gloves were worn during all sampling activities. All surface water samples were
collected in accordance with the protocol presented in the SWS Groundwater Monitoring Guidance
Document. Field Logs are included in Appendix A and field parameters are summarized in Table 3.
Following collection, the samples were placed into ice -filled coolers and shipped under proper chain -of -
custody to Pace for analysis.
Laboratory Analyses
Pace Analytical Services, Inc. analyzed the August 2021 groundwater and surface water samples under
chain -of -custody control.
The groundwater samples from monitoring wells MW- 1 R, MW- 2R, and MW-3R were analyzed for the
NC Appendix II list of constituents, plus 1,4-dioxane. Groundwater samples from monitoring wells MW-
1 R, MW-2R, MW-3R and NES- 1 were also analyzed for MNA parameters. Additionally, groundwater from
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Water Quality Monitoring Report — December 2021
Granville County Butner Landfill — Permit No. 39-02
monitoring well NES- 1 was analyzed for benzene, cobalt, and vanadium as constituents of concern. The
groundwater samples from monitoring wells MW-4, MW-5, and MW- 6 were analyzed for the NC Appendix
I list of constituents plus 1,4-dioxane.
The surface water samples from SW-1 and SW- 2 were analyzed for NC Appendix I constituents plus 1,4-
dioxane and hardness during the August 2021 event.
The complete laboratory analytical reports and the chains -of -custody from the August 2021 Sampling
Event are included in Appendix B. The historical groundwater elevation data are presented in Appendix
C. Historical analytical results for groundwater and surface water are presented in Appendix D and
Appendix E, respectively.
3 RESULTS OF GROUNDWATER AND SURFACE WATER ANALYSIS
Groundwater flow direction, average hydraulic gradient, and average interstitial flow velocity were derived
from water -level measurements recorded during the sampling event. A water -table elevation contour map
derived from the groundwater elevation measurements recorded on August 19, 2021, is presented as
Figure 3. The water -table elevation contours indicate that the direction of shallow groundwater flow is
generally to the southeast.
The hydraulic gradient in the vicinity of each well was derived by dividing the elevation difference between
water table elevations measured at the monitoring wells and proximal water -table elevation contour lines,
by the perpendicular horizontal distance between the wells and contours (Figure 3 and Table 4). The
water -table elevation contours indicate an average hydraulic gradient of approximately 0.058 ft./ft. Results
of in -situ slug testing reported by others (LaBella, 2021) indicate an average hydraulic conductivity value
in the shallow surficial aquifer of 2.18 x 10-5 cm/s (approximately 6.18 x 10-2 ft/day). Using the horizontal
hydraulic gradient measurements, the individual estimate of hydraulic conductivity, and an assumed
effective porosity of 0.18 (LaBella, 2021), the range of average interstitial groundwater flow velocities for
the shallow surficial aquifer was calculated using the following formula:
vX = (K/ne) x dh/dl
Where:
vX = average interstitial groundwater flow velocity
K = hydraulic conductivity
ne = effective porosity
dh/dl = horizontal hydraulic gradient
Average linear flow velocities are estimated to range between approximately 3.58 to 9.50 feet/year (0.0098
to 0.026 feet/day), with a geometric mean of 7.3 feet/year (0.02 feet/day). Table 4 summarizes the data
used to calculate the average interstitial groundwater flow velocity in the vicinity of each monitoring well.
Analytical Results for Groundwater and Comparisons to Standards
Inorganic Analyses
The following inorganic constituents were detected at quantified concentrations above the method
reportable limit (MRL) or practical quantitation limit (PQL) in one or more wells during the August 2021
Sampling Event:
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Water Quality Monitoring Report — December 2021
Granville County Butner Landfill — Permit No. 39-02
• barium, cadmium, cobalt, copper, lead, nickel, vanadium, tin, and zinc.
Table 5 summarizes all of the detections from the August 2021 sampling event.
Cobalt was detected in exceedance of the IMAC in MW-2R and MW-5. Vanadium was detected in
exceedance of the IMAC in MW- 2. The results for cobalt in MW- 2R and MW- 5 are consistent with
historical data. Exceedances of groundwater standards from the August 2021 sampling event are
summarized in Table 6.
No other inorganic constituents were detected above their NC2L/IMAC during the August 2021 sampling
event.
Organic Analyses
The following organic constituents were detected at quantified concentrations above the method
reportable limit (MRL) or practical quantitation limit (PQL) in one or more wells during the August 2021
Sampling Event:
• Chlorobenzene, chloroethane, 1,2-dichlorobenzene, 1,4-dichlorobenzene, 2-butanone (MEK), 1,4-
dioxane, benzene, naphthalene, tetra hydrofuran, vinyl chloride and xylene.
Table 5 summarizes all of the detections from the August 2021 sampling event.
Concentrations of 1,4-dioxane in exceedance of the NC21- standard were reported in monitoring wells
MW- 2R, MW- 3R, MW-4 and MW-5. Benzene was detected above the NC21- Standard in MW- 2R. The
benzene in MW- 2R is consistent with historical data and has been addressed in the ACM, approved in
June 2013, and the CAP, approved in June 2014. Exceedances of groundwater standards from the August
2021 sampling event are summarized in Table 6.
No other organic constituents were detected above the corresponding GPS during the August 2021
sampling event.
Analytical Results for Surface Water and Comparisons to Standards
Surface water points SW-1 and SW-2 were sampled during the August 2021 sampling event. Three
Appendix I constituents were detected above the MRL in the SW-2 samples. Barium (also detected in
SW-1 sample), nickel and 1,4-dioxane were detected but were below applicable surface water standards.
The detections in surface water samples are included in Table 5.
4 CORRECTIVE ACTION EVALUATION
Monitored Natural Attenuation Parameters
Monitoring wells MW- 2R and MW-3R were analyzed for the following MNA parameters during the August
2021 sampling event:
• MNA Field Parameters: Temperature, pH, conductivity, oxidation reduction potential, turbidity, and
dissolved oxygen. (Dissolved carbon dioxide is analyzed every 3rd year)
• MNA Laboratory Parameters: Alkalinity, sulfide, sulfate, nitrate, chloride, biological oxygen
demand (BOD), chemical oxygen demand (COD), and total organic carbon (TOC), methane,
ethane, ethane and dissolved hydrogen.
The current MNA parameter data are presented in Table 7.
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Water Quality Monitoring Report — December 2021
Granville County Butner Landfill — Permit No. 39-02
Based on the January 13, 2021, response from NCSWMR to the Corrective Action Evaluation Report
(CAER) dated December 21, 2020, the following parameters will be analyzed for two events every five
years, corresponding to the two events immediately preceding each Corrective Action Evaluation Report:
• Dissolved carbon dioxide,
• dissolved hydrogen,
• sulfide,
• volatile fatty acids,
• dissolved methane,
• ethene, and
• ethane.
The next Corrective Action Evaluation Report is due after the second semiannual sampling event of 2025.
Evaluation of Plume Stability and Trends
Chart 1 presents a plot of the benzene concentrations versus time in all monitoring wells where it has
been detected (MW-2R, MW-3R and MW-4). There were no benzene detections prior to December 2006;
however, from December 2006 to present, benzene in MW- 2R has fluctuated generally between 1 lag/L
and 2 lag/L and showed a slight downward trend overall prior to the last few years; the results of the last
few monitoring events indicate a recent slight upward trend in benzene concentrations. Benzene in MW-
3R initially fluctuated between 0. 3 lag/ L and 0.7 lag/ with a slight downward trend followed by a recent
trend of concentrations alternating between about 0.5 lag/ L and non -detects. Benzene in MW-4 has
fluctuated between non -detect and 0.4 lag/L and also shows a slight downward trend. Over the last two
years, benzene in MW-4 has not been detected. Also, the chart suggests that there is seasonal fluctuation
of the benzene concentrations. It should be noted that for non -detect concentrations in Chart 1, the
laboratory minimum detection level at the time was used as the event concentration (i.e., 0.25 lag/ up until
2018, and 0.15 lag/ since).
The benzene concentrations from the August 2021 Sampling Event are within the range of historical
fluctuations. Since there have been no detections of benzene in either the surface water or sentinel well
NES-1, there is no indication that the plume is migrating toward the property boundary. Based on the
available site data the plume appears to be stable.
Chart 2 presents a plot of the cobalt concentrations versus time in the monitoring wells where it has been
detected in exceedance of the GPS (MW-2R and MW-5). Cobalt in MW-2R has ranged between non -
detect and 38.0 lag/L but has been consistently between 7.4 and 11.3 lag/L since August 2014. Cobalt in
MW- 5 has fluctuated between non -detect and 251 lag/L, with large fluctuations that appear to have a
seasonal component (lower in winter and higher in summer); however, there are inconsistencies (the
highest historical concentration was in June 2002). There is no apparent increasing or decreasing trend
for cobalt in either well.
5 CONCLUSIONS
The groundwater flow regime is consistent with previous events and the groundwater monitoring network
remains adequate to monitor the site.
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Water Quality Monitoring Report — December 2021
Granville County Butner Landfill — Permit No. 39-02
Benzene was detected above the NC21- in MW-2R during the August 2021 sampling event. Review of
MNA parameter data, plume stability, and benzene trends indicate that the selected remedies of natural
attenuation and phytoremediation are adequately controlling the plume.
Cobalt was detected in MW-2R and MW-5 above its corresponding Interim maximum allowable
concentration (IMAC). This exceedance is consistent with historical detections.
Vanadium was detected above the IMAC in MW-2. The exceedance is consistent with historical
detections. Vanadium was not detected in any other wells during the August 2021 sampling event. An
Alternate Source Demonstration (ASD) to determine the statistical background for vanadium is
recommended. If the vanadium in MW-2 is above the statistical background, it should be added to the
COC list.
Analyte 1,4-dioxane was detected above the NC21- standard in MW-2R, MW-3R, MW-4 and MW-5.
Analyte 1,4-dioxane has been added to the COC list. The facility will remain in Assessment Monitoring
and Corrective Action.
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Figures

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Tables

TABLE 1
WELL CONSTRUCTION DETAILS
Monitoring
Well
Latitude
Longitude
Ground
Elevation
Ft-AMSLI
TOC
Elevation
Ft-AMSLI
Top of
Casing
Ft-AGS
Top of
Screen
Ft-BTOC
Bottom of
Screen
Ft-BTOC
Total Well
Depth
Ft-BTOC
Depth to
Bedrock
Ft-BTOC
Geologic
Unit
MW-1 R
N36 ° 09' 55.49"
W78 ° 45' 37.80"
461.01
461.01
0.00
41.00
56.00
56.00
30.00
Fractured Bedrock
MW-2 R
N36° 09' 38.57"
W78° 45' 34 .97"
326.60
328.94
2.34
3.85
18.85
18.85
13.00
Weathered
Bedrock
MW-3 R
N36° 09' 38.58"
W78° 45' 34.85"
328.77
330.95
2.18
25.83
35.83
35.83
13.00
Fractured Bedrock
MW-4
N36° 09' 38.93"
W78 '45' 30.15"
338.97
340.92
1.95
16.43
31.43
31.43
13.00
Fractured Bedrock
MW-5
N36° 09' 39.35 "
W78'45' 23.77"
341.88
344.00
2.12
8.52
23.52
23.52
17.00
Fractured Bedrock
MW-6
N36 ° 09' 47.00 "
W78° 45' 25.47"
360.80
362.80
2.00
17.63
32.63
32.63
21.20
Fractured Bedrock
NES-1
N36 ° 09' 35.65"
W78 ° 45' 31.59"
326.22
328.72
2.50
15.00
30.00
30.00
26.00
Fractured Bedrock

TABLE 2
GROUNDWATER ELEVATIONS
WELL
TOC ELEVATION
Ft- AMSL
DEPTH TO GW
8/19/2021
Ft- BTOC
WELL DEPTH
Ft-BTOC
GROUNDWATER
ELEVATION
Ft-AMSL
MW-1 R
460.51
40.29
56.00
420.22
MW-2R
331.60
2.10
18.85
329.50
MW-3R
330.96
2.25
35.83
328.71
MW-4
340.80
7.13
31.43
333.67
MW-5
343.88
13.75
23.52
330.13
MW-6
362.53
10.69
32.63
351.84
NES-1
328.40
18.11
32.80
310.29
Notes TOC = Top of Casing
Ft-BTOC = Feet below Top of Casing Ft-AMSL= Feet above mean sea level

TABLE 3
FIELD PARAMETERS
WELL ID
PARAMETER
RESULTS
UNITS
SAMPLE DATE
Groundwater
MW-1 R
pH
5.52
S.0
8/19/21
Temperature
19.70
°C
Conductivity
127.40
pS/cm
Turbidity
22.11
NTU
Dissolved Oxygen
0.68
mg.IL
Oxidation Reduction Potential
112.30
my
Static Water Level
40.29
ft
Well Depth
56.00
ft
MW-2R
pH
6.27
S.0
8/19/21
Temperature
19.40
°C
Conductivity
Turbidity
206.20
pS/cm
0.02
NTU
Dissolved Oxygen
3.55
mg.IL
Oxidation Reduction Potential
Static Water Level
65.00
my
2.10
ft
Well Depth
18.85
ft
MW-3R
pH
6.59
S.0
8/19/21
Temperature
19.90
°C
Conductivity
1568.00
pS/cm
Turbidity
0.02
NTU
Dissolved Oxygen
1.02
mg.IL
Oxidation Reduction Potential
79.90
my
Static Water Level
2.25
ft
Well Depth
35.83
ft
MW-4
pH
6.36
S.0
8/19/21
Temperature
25.30
°C
Conductivity
1658.00
ps/cm
Turbidity
1.40
NTU
m g.IL
Dissolved Oxygen
0.31
Oxidation Reduction Potential
58.70
my
Static Water Level
7.13
ft
Well Depth
31.43
ft
MW-5
pH
6.52
S.0
8/19/21
Temperature
19.30
°C
Conductivity
1044.00
pS/cm
Turbidity
8.48
NTU
Dissolved Oxygen
0.19
mg/L
Oxidation Reduction Potential
52.50
my
Static Water Level
13.75
ft
Well Depth
24.80
ft

TABLE 3
FIELD PARAMETERS
WELL ID
PARAMETER
RESULTS
UNITS
SAMPLE DATE
MW-6
pH
6.60
S.Ll
8/19/21
Temperature
22.30
°C
Conductivity
630.00
PS/CM
Turbidity
2.51
NTU
Dissolved Oxygen
1.88
mg/L
Oxidation Reduction Potential
125.00
my
Static Water Level
10.69
ft
Well Depth
31.85
ft
NES-1
pH
4.94
S.Ll
8/19/21
Temperature
17.70
°C
Conductivity
125.60
PS/CM
Turbidity
8.92
NTU
Dissolved Oxygen
2.07
mg/L
Oxidation Reduction Potential
42.30
my
Static Water Level
18.11
ft
Well Depth
36.10
ft
Surface
Water
SW-1
pH
7.14
S.Ll
8/19/21
Temperature
23.60
°C
Conductivity
285.60
PS/CM
Turbidity
7.82
NT U
Dissolved Oxygen
2.31
mg/L
Oxidation Reduction Potential
94.40
my
SW-2
pH
7.35
S.Ll
8/19/21
Temperature
24.60
°C
Conductivity
1231.00
PS/CM
Turbidity
3.02
NT U
Dissolved Oxygen
4.82
mg/L
Oxidation Reduction Potential
40.10
my

TABLE 4
GROUNDWATER FLOW
Well
No.
Hydraulic Conductivity (k)
ft/day
Grd. Water
Elevation*
Reference
Elevation*
delta-Elev.
in feet
Map Length
in feet
Hydraulic
Gradient (1)
Effective
Porosity (n)
GW Velocity
(V), ft/day
GW Velocity
(V), ft/year
MW-1R
6.18E-02
420.22
410.00
10.22
177.60
0.058
0.180
0.0198
7.21
MW-2R
6.18E-02
329.50
350.00
20.50
317.36
0.065
0.180
0.022
8.09
MW-3R
6.18E-02
328.71
350.00
21.29
320.71
0.066
0.180
0.023
8.32
MW-4
6.18E-02
333.67
330.00
3.67
52.21
0.070
0.180
0.024
8.81
MW-5
6.18E-02
330.13
340.00
9.87
344.97
0.029
0.180
0.010
3.59
MW-6
6.18E-02
351.84
360.00
8.16
135.11
0.060
0.180
0.021
7.57
NES-1
6.18E-02
310.29
320.00
9.71
128.12
0.076
0.180
0.026
9.50
Minimum
0.029
0.0098
3.5855
Maximum
0.076
0.026
9.498
Geometric Mean
0.058
0.020
7.298

TABLE 5
SUMMARY OF DETECTIONS
WELL ID
PARAMETER
RESULT
UNITS
QUALIFIER
METHOD
MDL
[MRL
STANDARD
FSOURCE
UNITS
COLLECT
DATE
Groundwater
Barium
6.2
pg/L
EPA 60100
3.5
5
700
NC 2L
pg/L
9/1/2021
MW-1 R
Copper
13.7
p /L
J
EPA 60100
4.3
5
1000
NC 2L
p /L
9/1/2021
Nickel
3.5
pg/L
EPA 60100
3.5
5
100
NC 2L
pg/L
9/1/2021
Zinc
44.2
pg/L
EPA 60100
9.5
10
1000
NC 2L
pg/L
9/1/2021
1,2-Dichlorobenzene
1.1
pg/L
EPA 8260D
0.29
1
20
NC 2L
pg/L
8/20/2021
1,4-Dichlorobenzene
2.0
p /L
EPA 8260D
0.33
1
6
NC 2L
p /L
8/20/2021
2-Butanone (MEK)
4.9
pg/L
J
EPA 8260D
4.0
5
4000
NC 2L
pg/L
8/20/2021
1,4-Dioxane
89.7
p /L
EPA 8260D
1.20
2
3
NC 2L
p /L
8/20/2021
Barium
119.0
pg/L
EPA 60100
3.5
5
700
NC 2L
pg/L
9/1/2021
Benzene
2.1
p /L
EPA 8260D
0.15
1
1
NC 2L
p /L
8/20/2021
Chlorobenzene
15.4
pg/L
EPA 8260D
0.23
1
50
NC 2L
pg/L
8/20/2021
MW-2R
Chloroethane
0.9
p /L
EPA 8260D
0.49
1
3000
NC 2L
p /L
8/20/2021
Cobalt
11.1
pg/L
EPA 60100
3.6
5
1
IMAC
pg/L
9/1/2021
Lead
4.7
p /L
J
EPA 60100
4.5
5
15
NC 2L
p /L
9/1/2021
Nickel
100.0
pg/L
EPA 60100
3.5
5
100
NC 2L
pg/L
9/1/2021
Tetrah drofuran
32.2
p /L
EPA 8260D
3.50
10
2000
IMAC
p /L
8/20/2021
Tin
26.2
pg/L
EPA 60100
4.7
5
2,000
IMAC
pg/L
9/1/2021
Vanadium
4.8
p /L
J
EPA 60100
3.9
5
0.3
IMAC
p /L
9/1/2021
Xylene (Total)
0.8
pg/L
J
EPA 8260D
0.34
1
500
NC 2L
pg/L
8/20/2021
112-Dichlorobenzene
1.1
p /L
EPA 8260D
0.29
1
20
NC 2L
p /L
8/21/2021
1,4-Dichlorobenzene
1.1
pg/L
EPA 8260D
0.33
1
6
NC 2L
pg/L
8/21/2021
Barium
72.7
p /L
EPA 60100
3.5
5
700
NC 2L
p /L
9/1/2021
Benzene
0.5
pg/L
J
EPA 8260D
0.3
1
1
NC 2L
pg/L
8/21/2021
Chlorobenzene
15.7
p /L
EPA 8260D
0.3
1
50
NC 2L
p /L
8/21/2021
MW-3R
Chloroethane
1.4
pg/L
EPA 8260D
0.7
1
3000
NC 2L
pg/L
8/21/2021
Nickel
24.8
p /L
EPA 60100
3.5
5
100
NC 2L
p /L
9/1/2021
Tetrahydrofuran
9.3
pg/L
J
EPA 8260D
3.5
10
2,000
IMAC
pg/L
8/21/2021
Tin
6.5
p /L
EPA 60100
4.7
5
2,000
IMAC
p /L
9/1/2021
1,4-Dioxane
52.8
pg/L
EPA 8260D
1.0
2
3
NC 2L
pg/L
8/21/2021
Vinyl chloride
0.8
p /L
J
EPA 8260D
0.39
1
0.03
NC 2L
p /L
8/21/2021
Chlorobenzene
4.2
pg/L
EPA 8260D
0.28
1
50
NC 2L
pg/L
8/21/2021
MW-4
Chloroethane
1.2
p /L
EPA 8260D
0.65
1
3000
NC 2L
p /L
8/21/2021
Nickel
15.1
pg/L
EPA 8260D
3.5
5
100
NC 2L
pg/L
9/1/2021
1,4-Dioxane
39.8
p /L
EPA 8260D
1.0
2
3
NC 2L
p /L
8/21/2021
Barium
131.0
pg/L
EPA 60100
3.5
5
700
NC 2L
pg/L
9/1/2021
Benzene
0.4
p /L
J
EPA 8260D
0.3
1
1
NC 2L
p /L
8/27/2021
MW-5
Cobalt
91.0
pg/L
EPA 60100
3.6
1 5
1
IMAC
pg/L
9/1/2021
Nickel
15.9
p /L
J
EPA 60100
3.5
5
100
NC 2L
p /L
9/1/2021
1,4-Dioxane
5.2
pg/L
EPA 8260D
1.0
2
3
NC 2L
pg/L
8/27/2021
MW-6
X lene Total
0.4
p /L
J
EPA 8260D
0.3
1
500
NC 2L
p /L
8/20/2021
NES-1
Barium
72.3
pg/L
J
EPA 60100
3.5
5
700
NC 2L
pg/L
9/1/2021
Nickel
7.1
p /L
EPA 60100
3.5
5
100
NC 2L
p /L
9/1/2021

TABLE 5
SUMMARY OF DETECTIONS
WELL ID
PARAMETER
RESULT
UNITS
QUALIFIER
METHOD
MDL
MRL
STANDARD
SOURCE
UNITS
COLLECT
DATE
Surface Water
SW-1
Barium
45.1
lag/L
EPA 60100
3.5
5
21000
ISTV
lag/L
9/1/2021
Barium
91.9
u /L
EPA 60100
3.5
5
21000
ISTV
la /L
9/1/2021
SW-2
Nickel
25.1
lag/L
J
EPA 60100
3.5
5
13274
NC 2L
Ng/L
9/1/2021
1,4-Dioxane
26.0
N /L
EPA 8260D
1
2
80
ISTV
N /L
8/20/2021

TABLE 6
SUMMARY OF EXCEEDANCES
WELL ID
PARAMETER
RESULT
UNITS
QUALIFIER
METHOD
MDL
MRL
STANDARD
SOURCE
UNITS
COLLECT
DATE
Groundwater
1,4-Dioxane
89.7
fag/L
EPA 8260D
1.20
2
3
NC 2L
lag/L
8/20/2021
MW 2
Benzene
2.1
N /L
EPA 8260D
0.15
1
1
NC 2L
N /L
8/20/2021
Cobalt
11.1
lag/L
EPA 60100
3.6
5
1
IMAC
Ng/L
9/1/2021
Vanadium
4.8
N /L
J
EPA 60100
3.9
5
0.3
IMAC
N /L
9/1/2021
MW-3
1,4-Dioxane
52.8
fag/L
EPA 8260D
1.0
2
3
NC 2L
lag/L
8/21/2021
Vinyl chloride
0.8
N /L
J
EPA 8260D
0.39
1
0.03
NC 2L
u /L
8/21/2021
MW-4
1,4-Dioxane
39.8
fag/L
EPA 8260D
1.0
2
3
NC 2L
Ng/L
8/21/2021
MW-5
Cobalt
91.0
N /L
EPA 60100
3.6
5
1
IMAC
N /L
9/1/2021
1,4-Dioxane
5.2
fag/L
EPA 8260D
1.0
2
3
NC 2L
lag/L
8/27/2021

TABLE 7
MONITORED NATURAL ATTENUATION PARAMETERS
Well ID
Parameter
Result
Units
Method
MDL
MRL
Collect Date
MW-1R
Chloride
NS
µg/L
EPA 300.0 Rev 2.11993
600
1,000
8/19/21
MW-2R
Chloride
217
µg/L
EPA 300.0 Rev 2.11993
2,400
4,000
8/19/21
MW-3R
Chloride
157
µg/L
EPA 300.0 Rev 2.11993
1,800
3,000
8/19/21
NES-1
Chloride
NS
µg/L
EPA 300.0 Rev 2.11993
600
1,000
8/19/21
MW-1R
Sulfate
NS
µg/L
EPA 300.0 Rev 2.11993
500
1,000
8/19/21
MW-2R
Sulfate
ND
µg/L
EPA 300.0 Rev 2.11993
500
1,000
8/19/21
MW-3R
Sulfate
ND
µg/L
EPA 300.0 Rev 2.11993
500
1,000
8/19/21
NES-1
Sulfate
NS
µg/L
EPA 300.0 Rev 2.11993
500
1,000
8/19/21
MW-1R
Nitrogen, Nitrate
NS
µg/L
EPA 353.2 Rev 2.0 1993
10
40
8/19/21
MW-2R
Nitrogen, Nitrate
ND
µg/L
EPA 353.2 Rev 2.0 1993
10
40
8/19/21
MW-3R
Nitrogen, Nitrate
ND
µg/L
EPA 353.2 Rev 2.0 1993
10
40
8/19/21
NES-1
Nitrogen, Nitrate
NS
µg/L
EPA 353.2 Rev 2.0 1993
50
200
8/19/21
MW-1R
Ethane
NS
µg/L
RSK 175 Modified
1
10
8/19/21
MW-2R
Ethane
NS
µg/L
RSK 175 Modified
1
10
8/19/21
MW-3R
Ethane
NS
µg/L
RSK 175 Modified
1
10
8/19/21
NES-1
Ethane
NS
µg/L
RSK 175 Modified
1
10
8/19/21
MW-1R
Ethene
NS
µg/L
RSK 175 Modified
1
10
8/19/21
MW-2R
Ethene
NS
µg/L
RSK 175 Modified
1
10
8/19/21
MW-3R
Ethene
NS
µg/L
RSK 175 Modified
1
10
8/19/21
NES-1
Ethene
NS
µg/L
RSK 175 Modified
1
10
8/19/21
MW-1R
Methane
NS
µg/L
RSK 175 Modified
3
10
8/19/21
MW-2R
Methane
7,210
µg/L
RSK 175 Modified
3
10
8/19/21
MW-3R
Methane
603
µg/L
RSK 175 Modified
3
10
8/19/21
NES-1
Methane
NS
µg/L
RSK 175 Modified
3
10
8/19/21
MW-1R
Alkalinity, Total as CaCO3
NS
µg/L
SM 2320B-2011
5,000
5,000
8/19/21
MW-2R
Alkalinity, Total as CaCO3
914,000
µg/L
SM 2320B-2011
5,000
5,000
8/19/21
MW-3R
Alkalinity, Total as CaCO3
636,000
µg/L
SM 2320B-2011
5,000
5,000
8/19/21
NES-1
Alkalinity, Total as CaCO3
NS
µg/L
SM 2320B-2011
5,000
5,000
8/19/21
MW-1R
Sulfide
NS
µg/L
SM 4500-S2D-2011
50
100
8/19/21
MW-2R
Sulfide
NS
µg/L
SM 4500-S2D-2011
50
100
8/19/21
MW-3R
Sulfide
NS
µg/L
SM 4500-S2D-2011
50
100
8/19/21
NES-1
Sulfide
NS
µg/L
SM 4500-S2D-2011
50
100
8/19/21
MW-1R
BOD, 5 day
NS
µg/L
SM 521OB-2011
2,000
2,000
8/19/21
MW-2R
BOD, 5 day
6,380
µg/L
SM 521OB-2011
2,000
2,000
8/19/21
MW-3R
BOD, 5 day
ND
µg/L
SM 521OB-2011
2,000
2,000
8/19/21
NES-1
BOD, 5 day
NS
µg/L
SM 521OB-2011
2,000
2,000
8/19/21

TABLE 7
MONITORED NATURAL ATTENUATION PARAMETERS
Well ID
Parameter
Result
Units
Method
MDL
MRL
Collect Date
MW-1R
Chemical Oxygen Demand
NS
µg/L
SM 5220D-2011
12,500
25,000
8/19/21
MW-2R
I Chemical Oxygen Demand
121,000
µg/L
SM 5220D-2011
12,500
25,000
8/19/21
MW-3R
Chemical Oxygen Demand
48,200
µg/L
SM 5220D-2011
12,500
25,000
8/19/21
NES-1
Chemical Oxygen Demand
NS
µg/L
SM 5220D-2011
12,500
25,000
8/19/21
MW-1R
Total Organic Carbon
NS
µg/L
SM 531OB-2011
500
1,000
8/19/21
MW-2R
Total Organic Carbon
28,200
µg/L
SM 531OB-2011
500
1,000
8/19/21
MW-3R
Total Organic Carbon
7,690
µg/L
SM 531OB-2011
500
1,000
8/19/21
NES-1
Total Organic Carbon
NS
µg/L
SM 531OB-2011
500
1,000
8/19/21

Charts

2.5
2
1.5
1
0.5
C
Chart 1
Benzene Concentrations (µg/L) vs. Time
MW-2R, MW-3R, & MW-4
lD I� n 00 00 Ol Ol M O O -1 -1 -1 N N M M -It :t I;t Ln Ln w w w I- n 00 00 M M M O O -1 �--�
.--I
N L\f1 O M W a\ -I w -1 -Zt M N rl N L 1 O M W -1 W\-I It 00) N n N Ln O M 0000 r-I W -4 ':t a) N n
a --I r-I -i ci r-I ci r-I ci r-I
BMW-2R MW-3R MW-4

Chart 2
Cobalt Concentrations (µg/L) vs. Tlme
MW-2R & MW-5
300 -
PVII
200
150
100
1 50
C
��� y�\��Cl XCI��\�XCI �\��Cl -�� o yy�oti�\��o�yo��o�%a�\��yo��\��ti��\��titi�\��ti��\��tiy�\��ti��\��ti��\��ti�
MW-2R MW-5

Appendix A
Field Data Logs

EQUIPI ENT CALIBRATION FORM
Client: project #: _ ` F
`
INSTRUMENT: � PN+
SERIAL NO.:
Date
ro
Time
Parameter
M
1 400
_ 7.00
10;00V
Calibration
Readin
Calibration Recorded
LEx : dV
Lot# Ex : o
Lot# D6ji f Fyn
ll Specific ConductIv.
Lot# $x:
ORP
LA 93
�
Dissolved:O en
T 70
���
.
Ambient Air Pressure
. I
INSTRUMENT:
SERIAL NO.: w 0-1
Date
r
Time
Parameter
4.00
7.00
Calibration
Readin
r
Calibration Recorded B 77 14
tot# Ex
Lot# Exp:
Lot# Ex , .
Specific Conductivft
W 1701S
Lot# Ij Ex :
ORP
Dissolved Oxygen
�Co
Turbid'
061
Temperature
Ambient Air Pressure

ECM,PMENT Cp►L1BRATiON;. FORM
client'.Q Project #: 1. CJ1�17 l�
tNSTRuME PN4 Q
SERIAL. NO.: S " Iota Z T of j
Calibration
�I P
fir'
a �, 3 , �►—
a ;
�i .� 6 .; •. a �:.e ® ��r

WELL NO.:/
►TER SAMPLE
ON RECORD PERMIT NO.:
Project No.:
Project Name: Butner Landfill Permit#
Weather Conditions:
1. WATER LEVEL DATA (measured
a. Depth to LNAPL:
C. Depth to DNAPL:
C. LNAPL Thickness: (a-b)
g. Length of Water Column:
h. Well Volume: INA
2. WELL PURGE DATA
a. Purge Method: Surface
b. Field Testing Equipment:
C. Required Total Purge Volume
d. Total Volume and Number
Client: Garrett and Moore
39-02 Project Location: Granville County
I Sampling Date: 8/ l /2021
from top of inner well casing)
I NA (ft) b. Depth to Water: NA (ft)
I NA (ft) d. Total Well Depth: NA 00
NA (ft) f. DNAPL Thickness: (c-d) NA 00
NA (ft) (a-d)
(gal) Conversion Factors
(a x cf = h)
Water Well LD. Conv. Fact. (cf)
I YSI PRO+; Hach 2100 1 0.041
(If x 2c) (gals.): NA 2 0.163
of Well Volumes Removed: NA 4 0.653
SW-
Sw
Sample
Point
-0wrw
Temp
(deg. C)
(±10%)
pH
(0.1s.u.)
(±0.1)
Spec. Cond.
(0.1uS/cm)
(±10%)
Eh/ORP
(1.OmV)
(±10mV)
Diss 02
(0.1mg/L)
(±10%)
TURB
(LONTU)
(<IONTU)
Color
Odor
Sample
Time
,3
C' 231
f l
2
Af
1510
SW-
. l b
J,
H
I
1,5
NO
, 40
4
^�
j
i
i
i
3. SAMPLE COLLECTION DATA Sampling Personnel:
Sampling Method(s) & Equip: Grab
Sample Analytical Parameters/Method:
HACH s/n: �A`{ ; YSI s/n: MlCA�2�i1
Sample Start Time: End SampleTime:
COMMENTS:

WELLNO.: 3
GROUNDWATER SAMPLE �q ®,.
COLLECTION RECORD PERMIT No.: 1
Project No.: Client:
Garrett and Moore
Project Name: Butner Landfill Permit# 39-02 Project Location:
Granville County
Weather Conditions: SIAu t VO.S Sampling Date: 8/ 141 /2021
1. WATER LEVEL DATA (measured trom top of inner well casing)
a. Depth to LNAPL: NA (ft) b. Depth to Water: t`�,�(ft)
i�
C. Depth to DNAPL: NA (ft) d. Total Well Depths, (ft)
e. LNAPL Thickness: (a-b) NA (ft) f. DNAPL Thickness:
(c-d) NA (ft)
g. Length of Water Column: (ft) (a-d)
h. Well Volume: (gal)
Conversion Factors
2. WELL PURGE DATA
(a x cf = h)
a. Purge Method: Qeristlalfi Subm um /Bailer(3 volume)
well I.D. Conv. Fact. (cf)
b. Field Testing Equipment: YSI PRO+;1 -ft60
1 0.041
C. Required Total Purge Volume (1f x 2c) (gals.):
0> 0.163
d. Total Volume and Nu berlof Well Volumes Removed:
4 0.653
e. - Begin Purge Time: Q 1-S End Purge Time: N 570
6 1.470
Lapse
Purge
Temp- pH,.
Spec. Cond.
Eh/ORP
Diss 02
TURB
Water
Read
Time
Rate
(deg. C) (0.1s.u.)
(O.IuS/cm)
(1.0mv)
(0.1mg/L)
(LONTU)
Color
Odor
Level
No.
(min.)
(ml/min)
(±10%) (±0.1)
(±1.0%)
(±10mv)
(±10%)
(<IONTU)
(ft)
$J
NR
n
P
4
jots
1, 4,qq � � 7 2
., a„ 4
�.,y'-�
a �01.,
CWa-
1,71
f
rza
106
11, S�
,0
,6
a
t � � 3
, 4 -L
40
J,b 2-
13,
1 oc)
11. (a
.3 z
S it
- Sri.
ILZ.
o,5
�
Lf
1-7
too
0:7
6s
fs7
- �,.�,
, 0
6P,03
3,
.a-.
0
' .Y
6. �
(T
- &I.Z
1,05
0,0'
64O&J
(4.®
late
v,�
t 5(a
--M-5
t, 42
AJO
,*9
t
i
3. SAMPLE COLLECTION DATA Sampling Personnel: -
Sampling Method(s) & Equip:
Sample I.D. (Name, Date, Time):'
Sample Analytical Parameters/Method:
04111t,Lk mOX0,W340A
ieok4&I'ts�• /n: 00 YSI s/n:
Fe+2= hDn j mg/1
Sample Start Time: l S!, End SampleTime:
to Za
COMMENTS:

ELL W NO.:
GROUNDWATER SAMPLE
PF.RA41T Nn
uuhEhu l 1UN Kh;uu"
Project No.: I
Client: Garrett and Moore
Project Name: Butner Landfill Permit# 39-02 Project Location:
Granville County
;
Weather Conditions:
Sampling Date: 8/ J /2021
L WATER LEVEL DATA (measu ed from top of inner well casing)
b.
a. Depth to LNAPL: NA
(ft) Depth toWater:
(ft)
C. Depth to DNAPL: NA (ft) d. Total Well Depth: S, r00 (ft)
e. LNAPL Thickness: (a-1i)
NA (ft) f. DNAPL Thickness:
(c-d) NA (ft)
g. Length of Water Column:
!ye, zi i (ft) (a-d)
h. Well Volume: �,
(gal)
Conversion Factors
2. WELL PURGE DATA
(a x cf = h)
a. Purge Method: Peristalti
ubm pump ailer(3 volume)
Well I.D. Conv. Fact. (cf)
b. Field Testing Equipment: 1
YSI PRO+; Hach 2100
1 0.041
C. Required Total Purge Volume (If x 2c):(gals.):
2 0:163
d. Total Volume and Number of Well Volumes Removed:
4 0.653
e. Begin Purge Time:
End Purge Time:
6 1.470
Lapse
Purge
Temp
pH
Spec. Cond.
Eh/ORP
Diss 02
TURB
Water
Read
Time
Rate
(deg. C)
I
(0.1s.u.)
(0.1uS/cm)
(1.0mV)
(0.1mg/L)
(LONTU)
Color
Odor
Level
No.
(min.)
(MI/Min)
(±10%)
(±0.>)
(±10%)
(±10mV)
(±10%)
(<loNTIJ)
(ft)
ISO
Q S'
AlaqAJ
f
34,
Z;
FO
I
too
Y
k0
d3�
3
15-
tee
%
0 -3
01
-3
t
(11[� ,
10 `
Ol ZY
, 0
Af,b
I 4b3
W
coo
Ky
S
f-3 [
r lo, I
2` .` fdAa
I
Z 33
66P
�,G
b
00.11
fti0.;
O 13
UA
C
40 3
I````��,
IVY
P`�'
�!T
r�ll ,�
n/�
' C V�s
�1
,' ' t, ,
��j f� r
//V�
X1b
'50
ran
c !� ..
°
' C��1�7t�1
G
7,
✓
�.
60
AJ
s dc`z
Z�� �F
3
0.�
i a
3. SAMPLE COLLECTION DATA Sampling Personnel:
Sampling Method(s) & Equip: CIA
Sample I.D. (Name, Date, Time): 3 IA1j P 0 1101so 1 p
Sample Analytical Parameters/Method: /vC -+-Mt, f' xf Y.
HACH s/n: T C(< ; YSLs/n: JIGo i I
Fe+2= rV Mg/1
Sample Start Time: tUj
COMMENTS:
End SampleTime:

i
WELL NO.: Kw -9—V ,
i
GROUNDWATER SAMPLE PERMIT NO.:
COLLECTION RECORD
Project No.: Client: Garrett and Moore
Project Name: Butner Landfill Permit# 39-02 Project Location: Granville County
Weather Conditions: Sampling Dated 8/ /2021
1. WATER LEVEL DATA (measured from top of inner well casing)
a. Depth to LNAPL: NA (ft) . b. Depth to Water: ! U (ft)
C. Depth to DNAPL: NA (ft) d. Total Well Depth: � (fo
e. LNAPL Thickness: (a-bl NA (ft) f. DNAPL Thickness: (c-d) NA (ft)
g. Length of Water Column:`S (ft) (a-d)
h. Well Volume: 2-. 7 3 (gal) Conversion Factors
2. WELL PURGE DATA ''�', (a x cf = h)
a. Purge Method: tic/Subm um /Bailer(3 volume) well I.D. Conv. Fact. ('cf)
b. Field Testing Equipment: YSI PRO+; HMIrZT00 4U 1 0.041
C. Required Total Purge Volume (1f x 2c) (gals.): 0.163
d. Total Volume and Number lof Well Volumes Removed: a 0.653
e. Begin Purge Time: 40%-7j End Purge Time: 1 6 1.470
Lapse Purge Temp pH! Spec. Cond. Eh/ORP Diss 02. TURB Water
Read Time Rate (deg. C) (0.1s.u.) (0.1uS/cm) (1.0mv) (0.1mg/L) , (LONTU) Color Odor Level
No. (min.) (ml/min) (±10%) (#0.11) (±10%) (±10mv) (±lo%)' (<1DNTU) (ft)
2-80
r
r�r e
&,Z� SO 7` -q3, . 37' &K, ftjt�> 2, L'7
. y 6,zt v s ss.s- 3, 0 to
n 100 'L0.3 &-tt W 7 -U-5 ,S o2 ciar Am2�Z8'
(� 2, ZP0 Z -&5-6 3' 55' 0Y07— 7-;-,
i
I
3. SAMPLE COLLECTION DATA Sampling Personnel: -}
Sampling Method(s) & Equip: t �u,.
Sample I.D. (Name, Date, Time):
Sample Analytical Parameters/Method:
H222& IP, Q S ; YSI 's/n:. C-, Wt9
Fe+2= (. mg/1
Sample Start Time: �,�'1. j End SampleTime: l t
COMMENTS:

WELL NO.:iLl�."C{
GROUNDWATER SAMPLE
COLLECTION RECORD PERMIT NO.:
Project No.:I Client: Garrett and Moore
/
Project Name: Butner Landfill Permit# 39-02 Project Location: Granville County "
Weather Conditions: ,�,�,,,, zi�t7OS Sampling Date: 8/ /2021
1. WATER LEVEL DATA (measui
f om top of inner well easing)
a. Depth to LNAPL:
j NA (ft) b. Depth to Water: -7 /
00
C. Depth to DNAPL:
NA (ft) d. Total Well Depth: 3 1, 43
(ft)
e. LNAPL Thickness: (a-b)
NA (ft) f. DNAPL Thickness: (c-d) NA
(ft)
g. Length of Water Column:
(ft) (a-d)
h. Well Volume:
(gal)
Conversion Factors
2. WELL PURGE DATA
(Peristaltic-
(a x cf = h)
a. Purge Method:
ubm um /Bailer(3 volume)
Well I.D. Conv. Fact: (co
b. Field Testing Equipment:
YSI PRO+; Hach 2100
1 0.041
C. Required Total Purge Volume
(1f x 2c) (gals.):
2 0.163
d. Total Volume and Number
of Well Volumes Removed:
4 0.653
e. Begin Purge;:Time:
0 �- 'L-
End Purge Time: 1311,
6 1.470
Lapse
Purge
Temp
pH,I
Spec. Cond.
Eh/ORP
Diss 02 '
TURB
Water
Read
Time
Rate
(deg.C)
(O.ISA.)
(OAUS/cm)
(1:0mv)
(0.1mg/L)
(IANTU)
'Color
Odor
Level
No.
(min.)
(ml/min)
(#10%)
(±0.1,)
(#10%)
(±10mv)
(±10%0)
(<IONTU)
(ft)
o
?-..3
(p,z,3
[c q'
7 r
Xb
`71
y.
a I,.�-
�T-
1,111111
z
16
too
G-30
03
16s,2
01
1
loa
L 7
Zd
100
�
4
`�
® 37
'
� '
r�
`Z q�
z�
Z �
i 7
," 3
rz
cam/
J,
%q
j
i
m
3. SAMPLE COLLECTION DATA S mpling Personnel:
Sampling Method(s) & Equip: �U
Sample I.D. (Name, Date, Time): J20 Z- y Z
Sample Analyticca/ll Parameters/Method:
HACH s/n: ­�1-C ; YSI s7n: 0V - 7
Fe+2= 84 mg/1
Sample Start Time: i 3 VZj End SampleTime: 13,Ll.
COMMENTS:

i
WELL NO.: M 1/\/`' J
GROUNDWATER SAMPLE PERMIT NO.: 37Q
COLLECTION RECORD
Project No.: Client:
Garrett and Moore
Project Name: Butner Landfill Permit# 39-02 Project Location:
Granville County
Weather Conditions: n 0 ` Sampling Date: 8/
/2021
1. WATER LEVEL DATA (measurell from top of inner well casing)
a. Depth to LNAPL: NA (ft) b. Depth to Water:
C. Depth to DNAPL: NA (ft) d. Total Well Depth: a t9 (ft)
e. LNAPL Thickness: (a-b) NA (ft) f. DNAPL Thickness: (c-d)
NA (ft)
g. Length of Water Column: I t1 01' - (ft) (a-d)
h. Well Volume: (so (gal)
Conversion Factors
2. WELL PURGE DATA
(a x cf = h)
a. Purge Method: Pe salt /Subm pump/Bailer(3 volume)
Well I.D.
Conv. Fact. (ct)
b. Field Testing Equipment: YSI PRO+; Hach 2100
1
0.041
C. Required Total Purge Volume (If x 2c) (gals.):
(0'
0.163
d. Total Volume and Number of Well Volumes Removed:
4
0.653
e. Begin Purge Time: QJ r End Purge Time: (
6
1.470
Lapse
Purge
Temp
pHI
Spec. Cond.
Eh/ORP
Diss 02
TURB
Water
Read
Time
Rate
(deg. C)
(0.1s.u.)
(0.1uS/cm)
(1.OmV)
(O.lmg/L)
(LONTU)
Color
Odor
Level
No.
(min.)
(ml/min)
(#10%)
(t0.1I)
(#10%)
(±IOmv)
(#10%)
(<IONTU)
(ft)
ME�
H11All
�
;P
a-
10
p 0
do
� ��.�
� I
-�
�,
r I
dtw
b
too
00
(;.-1
3 (
114
� `-
log 10
/&, d
s
po
�b
IS2
p.�-o
S �c4c
C V
M
A 0
-1
To
kbo
(o
-s
0,c
,
c6
r1.a-
b197
s ,a
c
-
NO
IQ9, a
�Q-
Io
-5:a.,:
0,1��LaT
i
3. SAMPLE COLLECTION DATALSampling Personnel:
p g
/�
Sampling Method(s) & Equip:l� ✓Jse'F(°v�
f�iC ^^
Sample I.D. (Name, Date, Time);
Sample Analytical Parameters/Method: vbG5
Sto
ova
HACH s/n: 5-'Trd ; Ysll s/n: ITO(ci c r
Fe+2= jy A, mg/1
Sample Start Time:
End SampleTime:
COMMENTS:

WELL NO.: tAvi
GROUNDWATER SAMPLE
.COLLECTION RECORD PERMIT No 1p2
Project No.: Client:
Gaxrett and Moore'
Project Name: Butner Landfill Permit'# 39-02 Project Location:
Granville County
Weather Conditions: S (A/1A4L §30 Sampling Date: 8/ /2021
1. WATER LEVEL DATA (meas red from top of inner well casing)
a. Depth to LNAPL: NA (ft) b. Depth to Water:
C. Depth to DNAPL: NA (ft) d. Total Well Depth:
3 S (ft)
e. LNAPL Thickness: (a-b; NA (ft) f. DNAPL Thickness:
(c-d) NA (ft)
g. Length of Water Column: I i i6 (ft) (a-d)
h. Well Volume: 'fl�" (gal)
Conversion Factors
2. WELL PURGE DATA
(a x cf = h)
a. Purge Method: Pnris�alis/Subm umpBailer(3 volume)
Well I.D. Conv. Fact. (co
b. Field Testing Equipmeht, YSI PRO+; Hach 2100
1 0.041
C. Required Total Purge Volume (lf x 2c) (gals.): 01
n 0.163
d. Total Volume and Numberlof Well Volumes Removed: /�
4 0.6�
e. Begin Purge Time: C�11O l End Purge Time::
6 1.470
Lapse
Purge
Temp
pH,
Spec. Cond.
Eh/ORP
Diss 02
TURB
Water
Read
Time
Rate
(deg. C)
(O.ls.u.)
(O.luS/cm)
(1.0mV)
(O.lmg/L)
(IANTU)
Color
Odor
Level
No.
(min.)
(ml/min)
(±10%)
(±0.1)
(±10%)
(±10mv)
(±10%)
(<lONTU)
(ft)
.i.NFU
3f1'_.
itPo,�gdE �ri
!
a�J'
�,.4,
ko©
,3
7• 1
gas
t3 t�
a
�.Ctow
ei
lath i
g
9
�00
1q-3
13y
1�'q
709
G 6�
NO
0
11,70
`7
s"
00
Pilo
LA
jb.
►��,'�
C.�w
No
a
i
(19 t9 .
�
a�.
z 0
(DrVr
d�,
�-b4-
2-
oo
aa_a
r�
a
s I _
��
- a. r
470
,as -.a
)A
- (
N%
s
3. SAMPLE COLLECTION DATA,,Sampling Personnel:
Sampling Method(s) &,Equip: `C(vv 3C W
rl
Sample I.D. (Name, Date, Time): p 41 Lt7 a
S-
Sample Analytical Parameters/Method: VoG
HACH s/n: d' I ; YSI s/n: 19 (0(p '7
Fe+2= mg/1
Sample Start Time: d�s-' End SampleTime:
l �O
COMMENTS:

WELL NO.:S'
GROUNDWATER SAMPLE G
� PERMIT NO.:
COLLECTION RECORD
Project No.: Client: Garrett and Moore
Project Name: Butner Landfill Permit# 39-02 Project Location: Granville County
Weather Conditions: Sampling Date: 8/ l: /2021
1. WATER LEVEL DATA (measured from top of inner well casing)
a. Depth to LNAPL: NA (ft) b. Depth to Water: �, (�
(ft)
C. Depth to DNAPL: j NA (ft) d. Total Well Depth:
(ft)
e. LNAPL Thickness: (a-b) NA (ft) f. DNAPL Thickness: (c-d) NA (ft)
g. Length of Water Column: f ,�� (ft) (a-d) _
h. Well Volume: 'L t-1 (gal) Conversion Factors
2. WELL PURGE DATA (a x cf = h)
a. Purge Method: is a tic bm um /Bailer(3 volume) Well I.D. Conv. Fact. (cf)
b. Field Testing Equipment: YSI PRO+; Iaeh-2-MO G,0, ", 1 0.041
C. Required Total Purge Volu a (1f x 2c) (gals.): 0.163
d. Total Volume and Numberlof Well Volumes Removed: 4 0.653
-Ai4
e. Begin Purge Time: End Purge Time: 6 1.470
Lapse
Purge
Temp
pH
Spec. Cond..
Eh/ORP
Diss 02
TURB
Water
e"'ii
Rad
Time
RateO.ls.u.
C (deg. )
( )
O.IuS/cm
( )
1.OmV
( )
Oam L
( g/)
1.ONTU
( )
Color
Odor
Level
No.
(min.)
(ml/min)
(#10%)
(#0-t)
(#10%)
(#lOmV)
(±10%)
(<1,ONTU)
(ft)
n
V.
.N2,
(,
ud)
,�Z
11�,�.-
t t
i
i
i
i
3. SAMPLE COLLECTION DATA Sampling Personnel:
Sampling Method(s) & Equip: 11 C6t.J
Sample I.D. (Name, Date, Time): l�s ZI
Sample Ana ytical Parameters/Method:
lekavwls' ; YSI s/n:It G100A3
Fe+2= mg/1
Sample Start Time: End SampleTime:
COMMENTS:

Appendix B
Laboratory Analytical Reports

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
September 13, 2021
Stefan Bray, PE
Garrett & Moore
1029 West South Street
Raleigh, NC 27603
RE: Project: Butner Landfill Compliance
Pace Project No.: 92556832
Dear Stefan Bray, PE:
Enclosed are the analytical results for sample(s) received by the laboratory on August 19, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Eden
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Butner Landfill Compliance
92556832
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92556832001
3902-MW1R
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92556832002
3902-MW4
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92556832003
3902-MW3R
EPA 353.2 Rev 2.0 1993
AMI
1
PASI-E
SM 521OB-2011
DAW
1
PASI-E
RSK 175 Modified
MAD
1
PASI-C
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
SM 4500-CI-E-2011
KDF1
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
SM 531OB-2011
MDW
1
PASI-A
92556832004
3902-MW2R
EPA 353.2 Rev 2.0 1993
AMI
1
PASI-E
SM 521OB-2011
DAW
1
PASI-E
RSK 175 Modified
MAD
1
PASI-C
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
SM 4500-CI-E-2011
KDF1
1
PASI-A
SM 5220D-2011
JP1
1
PASI-A
SM 531OB-2011
MDW
1
PASI-A
92556832005
3902-MW5
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
SAS
50
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92556832006
3902-MW6
EPA 601OD
SH1
15
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Butner Landfill Compliance
Pace Project No.:
92556832
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92556832007
3902-NES1
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92556832008
3902-Field Blank
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92556832009
3902-SW1
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92556832010
3902-SW2
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
NSCQ
51
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92556832011
3902-Trip Blank
EPA 8260D
NSCQ
51
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-E = Pace Analytical Services - Eden
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-MW1R Lab ID: 92556832001 Collected: 08/19/21 11:05 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/01/2112:55
09/02/2104:52
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/01/2112:55
09/02/2104:52
7440-38-2
Barium
6.2
ug/L
5.0
1
09/01/2112:55
09/02/2104:52
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/01/2112:55
09/02/2104:52
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/01/2112:55
09/02/2104:52
7440-43-9
Chromium
ND
ug/L
5.0
1
09/01/2112:55
09/02/2104:52
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/01/2112:55
09/02/2104:52
7440-48-4
Copper
13.7
ug/L
5.0
1
09/01/2112:55
09/02/2104:52
7440-50-8
Lead
ND
ug/L
5.0
1
09/01/2112:55
09/02/2104:52
7439-92-1
Nickel
3.5J
ug/L
5.0
1
09/01/2112:55
09/02/2104:52
7440-02-0
Selenium
ND
ug/L
10.0
1
09/01/2112:55
09/02/2104:52
7782-49-2
Silver
ND
ug/L
5.0
1
09/01/2112:55
09/02/2104:52
7440-22-4
Tin
ND
ug/L
5.0
1
09/01/2112:55
09/02/2104:52
7440-31-5
Vanadium
ND
ug/L
5.0
1
09/01/2112:55
09/02/2104:52
7440-62-2
Zinc
44.2
ug/L
10.0
1
09/01/2112:55
09/02/2104:52
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/07/21 09:57
09/10/2101:57
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
08/20/21 23:08
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
08/20/21 23:08
107-13-1
Benzene
ND
ug/L
1.0
1
08/20/21 23:08
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
08/20/21 23:08
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
08/20/21 23:08
75-27-4
Bromoform
ND
ug/L
1.0
1
08/20/21 23:08
75-25-2
Bromomethane
ND
ug/L
2.0
1
08/20/21 23:08
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
08/20/21 23:08
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
08/20/21 23:08
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
08/20/21 23:08
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
08/20/21 23:08
108-90-7
Chloroethane
ND
ug/L
1.0
1
08/20/21 23:08
75-00-3
Chloroform
ND
ug/L
1.0
1
08/20/21 23:08
67-66-3
Chloromethane
ND
ug/L
1.0
1
08/20/21 23:08
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
08/20/21 23:08
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
08/20/21 23:08
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
08/20/21 23:08
106-93-4
Dibromomethane
ND
ug/L
1.0
1
08/20/21 23:08
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
08/20/21 23:08
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
08/20/21 23:08
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
08/20/21 23:08
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
08/20/21 23:08
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
08/20/21 23:08
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
L1,v1
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-MW1R Lab ID: 92556832001 Collected: 08/19/21 11:05 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
08/20/21 23:08
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
08/20/21 23:08
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
08/20/21 23:08
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
08/20/21 23:08
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
08/20/21 23:08
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
08/20/21 23:08
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
08/20/21 23:08
100-41-4
2-Hexanone
ND
ug/L
5.0
1
08/20/21 23:08
591-78-6
lodomethane
ND
ug/L
20.0
1
08/20/21 23:08
74-88-4 L2,v2
Methylene Chloride
ND
ug/L
5.0
1
08/20/21 23:08
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
08/20/21 23:08
108-10-1
Styrene
ND
ug/L
1.0
1
08/20/21 23:08
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
08/20/21 23:08
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
08/20/21 23:08
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
08/20/21 23:08
127-18-4
Tetrahydrofuran
ND
ug/L
10.0
1
08/20/21 23:08
109-99-9
Toluene
ND
ug/L
1.0
1
08/20/21 23:08
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
08/20/21 23:08
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
08/20/21 23:08
79-00-5
Trichloroethene
ND
ug/L
1.0
1
08/20/21 23:08
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
08/20/21 23:08
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
08/20/21 23:08
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
08/20/21 23:08
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
08/20/21 23:08
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
08/20/21 23:08
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
08/20/21 23:08
460-00-4
1,2-Dichloroethane-d4 (S)
101
%
70-130
1
08/20/21 23:08
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
08/20/21 23:08
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
08/20/21 16:40
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
08/20/21 16:40
17060-07-0
Toluene-d8 (S)
97
%
66-133
1
08/20/21 16:40
2037-26-5
Date: 09/13/2021 01:03 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-MW4 Lab ID: 92556832002 Collected: 08/19/21 13:12 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:05
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:05
7440-38-2
Barium
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:05
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/01/2112:55
09/02/2105:05
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/01/2112:55
09/02/2105:05
7440-43-9
Chromium
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:05
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:05
7440-48-4
Copper
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:05
7440-50-8
Lead
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:05
7439-92-1
Nickel
15.1
ug/L
5.0
1
09/01/2112:55
09/02/2105:05
7440-02-0
Selenium
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:05
7782-49-2
Silver
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:05
7440-22-4
Tin
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:05
7440-31-5
Vanadium
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:05
7440-62-2
Zinc
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:05
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
2.4
5
09/07/21 09:57
09/10/2102:02
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
08/20/21 23:26
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
08/20/21 23:26
107-13-1
Benzene
ND
ug/L
1.0
1
08/20/21 23:26
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
08/20/21 23:26
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
08/20/21 23:26
75-27-4
Bromoform
ND
ug/L
1.0
1
08/20/21 23:26
75-25-2
Bromomethane
ND
ug/L
2.0
1
08/20/21 23:26
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
08/20/21 23:26
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
08/20/21 23:26
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
08/20/21 23:26
56-23-5
Chlorobenzene
4.2
ug/L
1.0
1
08/20/21 23:26
108-90-7
Chloroethane
1.2
ug/L
1.0
1
08/20/21 23:26
75-00-3
Chloroform
ND
ug/L
1.0
1
08/20/21 23:26
67-66-3
Chloromethane
ND
ug/L
1.0
1
08/20/21 23:26
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
08/20/21 23:26
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
08/20/21 23:26
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
08/20/21 23:26
106-93-4
Dibromomethane
ND
ug/L
1.0
1
08/20/21 23:26
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
08/20/21 23:26
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
08/20/21 23:26
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
08/20/21 23:26
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
08/20/21 23:26
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
08/20/21 23:26
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
L1,v1
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-MW4 Lab ID: 92556832002 Collected: 08/19/21 13:12 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
08/20/21 23:26
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
08/20/21 23:26
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
08/20/21 23:26
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
08/20/21 23:26
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
08/20/21 23:26
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
08/20/21 23:26
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
08/20/21 23:26
100-41-4
2-Hexanone
ND
ug/L
5.0
1
08/20/21 23:26
591-78-6
lodomethane
ND
ug/L
20.0
1
08/20/21 23:26
74-88-4 L2,v2
Methylene Chloride
ND
ug/L
5.0
1
08/20/21 23:26
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
08/20/21 23:26
108-10-1
Styrene
ND
ug/L
1.0
1
08/20/21 23:26
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
08/20/21 23:26
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
08/20/21 23:26
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
08/20/21 23:26
127-18-4
Tetrahydrofuran
ND
ug/L
10.0
1
08/20/21 23:26
109-99-9
Toluene
ND
ug/L
1.0
1
08/20/21 23:26
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
08/20/21 23:26
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
08/20/21 23:26
79-00-5
Trichloroethene
ND
ug/L
1.0
1
08/20/21 23:26
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
08/20/21 23:26
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
08/20/21 23:26
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
08/20/21 23:26
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
08/20/21 23:26
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
08/20/21 23:26
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
08/20/21 23:26
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
08/20/21 23:26
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
08/20/21 23:26
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
39.8
ug/L
2.0
1
08/20/21 17:00
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
08/20/21 17:00
17060-07-0
Toluene-d8 (S)
97
%
66-133
1
08/20/21 17:00
2037-26-5
Date: 09/13/2021 01:03 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 62

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-MW3R
Lab ID: 92556832003 Collected:
08/19/21
09:50
Received: 08/19/21 15:40 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services - Eden
Nitrogen, Nitrate
ND mg/L
0.040
1
08/20/21 15:42
14797-55-8
5210B BOD, 5 day EDN
Analytical Method: SM 521OB-2011 Preparation
Method: SM 521 OB-2011
Pace Analytical Services - Eden
BOD, 5 day
ND ug/L
2000
1
08/20/21 17:33
08/25/21 14:00
B2
RSK 175 Headspace
Analytical Method: RSK 175 Modified
Pace Analytical Services - Charlotte
Methane
603 ug/L
10.0
1
08/24/21 16:50
74-82-8
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND ug/L
5.0
1
09/01/2112:55
09/02/2105:15
7440-36-0
Arsenic
ND ug/L
10.0
1
09/01/2112:55
09/02/2105:15
7440-38-2
Barium
72.7 ug/L
5.0
1
09/01/2112:55
09/02/2105:15
7440-39-3
Beryllium
ND ug/L
1.0
1
09/01/2112:55
09/02/2105:15
7440-41-7
Cadmium
ND ug/L
1.0
1
09/01/2112:55
09/02/2105:15
7440-43-9
Chromium
ND ug/L
5.0
1
09/01/2112:55
09/02/2105:15
7440-47-3
Cobalt
ND ug/L
5.0
1
09/01/2112:55
09/02/2105:15
7440-48-4
Copper
ND ug/L
5.0
1
09/01/2112:55
09/02/2105:15
7440-50-8
Lead
ND ug/L
5.0
1
09/01/2112:55
09/02/2105:15
7439-92-1
Nickel
24.8 ug/L
5.0
1
09/01/2112:55
09/02/2105:15
7440-02-0
Selenium
ND ug/L
10.0
1
09/01/2112:55
09/02/2105:15
7782-49-2
Silver
ND ug/L
5.0
1
09/01/2112:55
09/02/2105:15
7440-22-4
Tin
6.5 ug/L
5.0
1
09/01/2112:55
09/02/2105:15
7440-31-5
Vanadium
ND ug/L
5.0
1
09/01/2112:55
09/02/2105:15
7440-62-2
Zinc
ND ug/L
10.0
1
09/01/2112:55
09/02/2105:15
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical Services -Asheville
Thallium
ND ug/L
0.47
1
09/07/21 09:57
09/10/2102:07
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
1
08/21/21 00:02
67-64-1
Acrylonitrile
ND ug/L
10.0
1
08/21/21 00:02
107-13-1
Benzene
0.49J ug/L
1.0
1
08/21/21 00:02
71-43-2
Bromochloromethane
ND ug/L
1.0
1
08/21/21 00:02
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
08/21/21 00:02
75-27-4
Bromoform
ND ug/L
1.0
1
08/21/21 00:02
75-25-2
Bromomethane
ND ug/L
2.0
1
08/21/21 00:02
74-83-9 v2
2-Butanone (MEK)
ND ug/L
5.0
1
08/21/21 00:02
78-93-3
Carbon disulfide
ND ug/L
2.0
1
08/21/21 00:02
75-15-0
Carbon tetrachloride
ND ug/L
1.0
1
08/21/21 00:02
56-23-5
Chlorobenzene
15.7 ug/L
1.0
1
08/21/21 00:02
108-90-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 62

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-MW3R Lab ID: 92556832003 Collected: 08/19/21 09:50 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Date: 09/13/2021 01:03 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1.4
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
1.1
ug/L
1.1
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
9.3J
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
0.84J
ug/L
ND
ug/L
97 %
99 %
99 %
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
52.8 ug/L
1.0
1
08/21 /21 00:02
75-00-3
1.0
1
08/21 /21 00:02
67-66-3
1.0
1
08/21 /21 00:02
74-87-3
2.0
1
08/21 /21 00:02
96-12-8
1.0
1
08/21 /21 00:02
124-48-1
1.0
1
08/21 /21 00:02
106-93-4
1.0
1
08/21 /21 00:02
74-95-3
1.0
1
08/21 /21 00:02
95-50-1
1.0
1
08/21 /21 00:02
106-46-7
1.0
1
08/21 /21 00:02
110-57-6
1.0
1
08/21 /21 00:02
75-34-3
1.0
1
08/21 /21 00:02
107-06-2
1.0
1
08/21 /21 00:02
75-35-4
1.0
1
08/21 /21 00:02
156-59-2
1.0
1
08/21 /21 00:02
156-60-5
1.0
1
08/21 /21 00:02
78-87-5
1.0
1
08/21 /21 00:02
10061-01-5
1.0
1
08/21 /21 00:02
10061-02-6
1.0
1
08/21 /21 00:02
100-41-4
5.0
1
08/21 /21 00:02
591-78-6
20.0
1
08/21 /21 00:02
74-88-4
5.0
1
08/21 /21 00:02
75-09-2
5.0
1
08/21 /21 00:02
108-10-1
1.0
1
08/21 /21 00:02
100-42-5
1.0
1
08/21 /21 00:02
630-20-6
1.0
1
08/21 /21 00:02
79-34-5
1.0
1
08/21 /21 00:02
127-18-4
10.0
1
08/21 /21 00:02
109-99-9
1.0
1
08/21 /21 00:02
108-88-3
1.0
1
08/21 /21 00:02
71-55-6
1.0
1
08/21 /21 00:02
79-00-5
1.0
1
08/21 /21 00:02
79-01-6
1.0
1
08/21 /21 00:02
75-69-4
1.0
1
08/21 /21 00:02
96-18-4
2.0
1
08/21 /21 00:02
108-05-4
1.0
1
08/21 /21 00:02
75-01-4
1.0
1
08/21 /21 00:02
1330-20-7
70-130 1
70-130 1
70-130 1
2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
08/21 /21 00:02 460-00-4
08/21 /21 00:02 17060-07-0
08/21 /21 00:02 2037-26-5
08/20/21 17:20 123-91-1
L1,v1
L2,v2
Page 10 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-MW3R Lab ID: 92556832003 Collected: 08/19/21 09:50 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV SIM
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
2320B Alkalinity
Alkalinity, Total as CaCO3
300.0 IC Anions 28 Days
Sulfate
4500 Chloride
Chloride
5220D COD
Chemical Oxygen Demand
5310B TOC
Total Organic Carbon
Date: 09/13/2021 01:03 PM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
100 %
70-130
1
08/20/2117:20
17060-07-0
97 %
66-133
1
08/20/21 17:20
2037-26-5
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
636000 ug/L
5000
1
08/31/2117:21
Analytical Method: EPA 300.0 Rev 2.1
1993
Pace Analytical Services -Asheville
ND ug/L
1000
1
08/26/2107:32
14808-79-8
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
157 mg/L
10.0
10
09/02/2111:29
16887-00-6
Analytical Method: SM 5220D-2011
Preparation
Method:
SM 5220D-2011
Pace Analytical Services -Asheville
48200 ug/L
25000
1
09/01/2101:27 09/01/2105:20
Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
7690 ug/L
1000
1
08/23/21 19:42
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 62

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-MW2R Lab ID: 92556832004 Collected: 08/19/21 11:25 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
353.2 NO2/NO3 unpres EDN
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Eden
Nitrogen, Nitrate
ND mg/L
0.040
1
08/20/21 15:46
14797-55-8
5210B BOD, 5 day EDN
Analytical Method: SM 521OB-2011 Preparation
Method:
SM 521 OB-2011
Pace Analytical Services - Eden
BOD, 5 day
6380 ug/L
2000
1
08/20/21 17:33
08/25/21 14:08
RSK 175 Headspace
Analytical Method: RSK 175 Modified
Pace Analytical Services - Charlotte
Methane
7210 ug/L
10.0
1
08/24/21 17:06
74-82-8
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Antimony
ND ug/L
5.0
1
09/01/2112:55
09/02/2105:18
7440-36-0
Arsenic
ND ug/L
10.0
1
09/01/2112:55
09/02/2105:18
7440-38-2
Barium
119 ug/L
5.0
1
09/01/2112:55
09/02/2105:18
7440-39-3
Beryllium
ND ug/L
1.0
1
09/01/2112:55
09/02/2105:18
7440-41-7
Cadmium
ND ug/L
1.0
1
09/01/2112:55
09/02/2105:18
7440-43-9
Chromium
ND ug/L
5.0
1
09/01/2112:55
09/02/2105:18
7440-47-3
Cobalt
11.1 ug/L
5.0
1
09/01/2112:55
09/02/2105:18
7440-48-4
Copper
ND ug/L
5.0
1
09/01/2112:55
09/02/2105:18
7440-50-8
Lead
4.7J ug/L
5.0
1
09/01/2112:55
09/02/2105:18
7439-92-1
Nickel
100 ug/L
5.0
1
09/01/2112:55
09/02/2105:18
7440-02-0
Selenium
ND ug/L
10.0
1
09/01/2112:55
09/02/2105:18
7782-49-2
Silver
ND ug/L
5.0
1
09/01/2112:55
09/02/2105:18
7440-22-4
Tin
26.2 ug/L
5.0
1
09/01/2112:55
09/02/2105:18
7440-31-5
Vanadium
4.8J ug/L
5.0
1
09/01/2112:55
09/02/2105:18
7440-62-2
Zinc
ND ug/L
10.0
1
09/01/2112:55
09/02/2105:18
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Thallium
ND ug/L
0.47
1
09/07/21 09:57
09/10/2102:11
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
1
08/20/21 22:13
67-64-1
Acrylonitrile
ND ug/L
10.0
1
08/20/21 22:13
107-13-1
Benzene
2.1 ug/L
1.0
1
08/20/21 22:13
71-43-2
Bromochloromethane
ND ug/L
1.0
1
08/20/21 22:13
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
08/20/21 22:13
75-27-4
Bromoform
ND ug/L
1.0
1
08/20/21 22:13
75-25-2
Bromomethane
ND ug/L
2.0
1
08/20/21 22:13
74-83-9
2-Butanone (MEK)
4.9J ug/L
5.0
1
08/20/21 22:13
78-93-3
Carbon disulfide
ND ug/L
2.0
1
08/20/21 22:13
75-15-0
Carbon tetrachloride
ND ug/L
1.0
1
08/20/21 22:13
56-23-5
Chlorobenzene
15.4 ug/L
1.0
1
08/20/21 22:13
108-90-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC.
v2
Page 12 of 62

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-MW2R Lab ID: 92556832004 Collected: 08/19/21 11:25 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Date: 09/13/2021 01:03 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
0.92J
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
1.1
ug/L
2.0
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
32.2
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
0.82J
ug/L
97 %
99 %
98 %
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
89.7 ug/L
1.0
1
08/20/21 22:13
75-00-3
1.0
1
08/20/21 22:13
67-66-3
1.0
1
08/20/21 22:13
74-87-3
2.0
1
08/20/21 22:13
96-12-8
1.0
1
08/20/21 22:13
124-48-1
1.0
1
08/20/21 22:13
106-93-4
1.0
1
08/20/21 22:13
74-95-3
1.0
1
08/20/21 22:13
95-50-1
1.0
1
08/20/21 22:13
106-46-7
1.0
1
08/20/21 22:13
110-57-6
1.0
1
08/20/21 22:13
75-34-3
1.0
1
08/20/21 22:13
107-06-2
1.0
1
08/20/21 22:13
75-35-4
1.0
1
08/20/21 22:13
156-59-2
1.0
1
08/20/21 22:13
156-60-5
1.0
1
08/20/21 22:13
78-87-5
1.0
1
08/20/21 22:13
10061-01-5
1.0
1
08/20/21 22:13
10061-02-6
1.0
1
08/20/21 22:13
100-41-4
5.0
1
08/20/21 22:13
591-78-6
20.0
1
08/20/21 22:13
74-88-4
5.0
1
08/20/21 22:13
75-09-2
5.0
1
08/20/21 22:13
108-10-1
1.0
1
08/20/21 22:13
100-42-5
1.0
1
08/20/21 22:13
630-20-6
1.0
1
08/20/21 22:13
79-34-5
1.0
1
08/20/21 22:13
127-18-4
10.0
1
08/20/21 22:13
109-99-9
1.0
1
08/20/21 22:13
108-88-3
1.0
1
08/20/21 22:13
71-55-6
1.0
1
08/20/21 22:13
79-00-5
1.0
1
08/20/21 22:13
79-01-6
1.0
1
08/20/21 22:13
75-69-4
1.0
1
08/20/21 22:13
96-18-4
2.0
1
08/20/21 22:13
108-05-4
1.0
1
08/20/21 22:13
75-01-4
1.0
1
08/20/21 22:13
1330-20-7
70-130 1
70-130 1
70-130 1
2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
08/20/21 22:13 460-00-4
08/20/21 22:13 17060-07-0
08/20/21 22:13 2037-26-5
08/24/21 14:17 123-91-1
L1,v1
L2,v2
Page 13 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-MW2R Lab ID: 92556832004 Collected: 08/19/21 11:25 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV SIM
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
2320B Alkalinity
Alkalinity, Total as CaCO3
300.0 IC Anions 28 Days
Sulfate
4500 Chloride
Chloride
5220D COD
Chemical Oxygen Demand
5310B TOC
Total Organic Carbon
Date: 09/13/2021 01:03 PM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
98 %
70-130
1
08/24/2114:17
17060-07-0
91 %
66-133
1
08/24/21 14:17
2037-26-5
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
914000 ug/L
5000
1
08/31/2103:41
Analytical Method: EPA 300.0 Rev 2.1
1993
Pace Analytical Services -Asheville
ND ug/L
1000
1
08/26/2107:48
14808-79-8
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
217 mg/L
10.0
10
09/02/2111:30
16887-00-6
Analytical Method: SM 5220D-2011
Preparation
Method:
SM 5220D-2011
Pace Analytical Services -Asheville
121000 ug/L
25000
1
09/02/2102:41 09/02/2106:08
Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
28200 ug/L
1000
1
08/23/21 19:58
7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-MW5 Lab ID: 92556832005 Collected: 08/19/21 11:26 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:21
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:21
7440-38-2
Barium
131
ug/L
5.0
1
09/01/2112:55
09/02/2105:21
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/01/2112:55
09/02/2105:21
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/01/2112:55
09/02/2105:21
7440-43-9
Chromium
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:21
7440-47-3
Cobalt
91.0
ug/L
5.0
1
09/01/2112:55
09/02/2105:21
7440-48-4
Copper
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:21
7440-50-8
Lead
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:21
7439-92-1
Nickel
15.9
ug/L
5.0
1
09/01/2112:55
09/02/2105:21
7440-02-0
Selenium
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:21
7782-49-2
Silver
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:21
7440-22-4
Vanadium
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:21
7440-62-2
Zinc
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:21
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020B Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/07/21 09:57
09/10/2102:16
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
08/27/21 19:40
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
08/27/21 19:40
107-13-1
Benzene
0.38J
ug/L
1.0
1
08/27/21 19:40
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
08/27/21 19:40
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
08/27/21 19:40
75-27-4
Bromoform
ND
ug/L
1.0
1
08/27/21 19:40
75-25-2
Bromomethane
ND
ug/L
2.0
1
08/27/21 19:40
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
08/27/21 19:40
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
08/27/21 19:40
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
08/27/21 19:40
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
08/27/21 19:40
108-90-7
Chloroethane
ND
ug/L
1.0
1
08/27/21 19:40
75-00-3
Chloroform
ND
ug/L
1.0
1
08/27/21 19:40
67-66-3
Chloromethane
ND
ug/L
1.0
1
08/27/21 19:40
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
08/27/21 19:40
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
08/27/21 19:40
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
08/27/21 19:40
106-93-4
Dibromomethane
ND
ug/L
1.0
1
08/27/21 19:40
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
08/27/21 19:40
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
08/27/21 19:40
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
08/27/21 19:40
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
08/27/21 19:40
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
08/27/21 19:40
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
08/27/21 19:40
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-MW5 Lab ID: 92556832005 Collected: 08/19/21 11:26 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
08/27/21 19:40
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
08/27/21 19:40
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
08/27/21 19:40
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
08/27/21 19:40
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
08/27/21 19:40
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
08/27/21 19:40
100-41-4
2-Hexanone
ND
ug/L
5.0
1
08/27/21 19:40
591-78-6
lodomethane
ND
ug/L
20.0
1
08/27/21 19:40
74-88-4 L1,v1
Methylene Chloride
ND
ug/L
5.0
1
08/27/21 19:40
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
08/27/21 19:40
108-10-1
Styrene
ND
ug/L
1.0
1
08/27/21 19:40
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
08/27/21 19:40
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
08/27/21 19:40
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
08/27/21 19:40
127-18-4
Toluene
ND
ug/L
1.0
1
08/27/21 19:40
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
08/27/21 19:40
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
08/27/21 19:40
79-00-5
Trichloroethene
ND
ug/L
1.0
1
08/27/21 19:40
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
08/27/21 19:40
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
08/27/21 19:40
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
08/27/21 19:40
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
08/27/21 19:40
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
08/27/21 19:40
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
96
%
70-130
1
08/27/21 19:40
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
08/27/21 19:40
17060-07-0
Toluene-d8 (S)
98
%
70-130
1
08/27/21 19:40
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
5.2
ug/L
2.0
1
08/26/21 14:56
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
08/26/21 14:56
17060-07-0
Toluene-d8(S)
102
%
66-133
1
08/26/21 14:56
2037-26-5
Date: 09/13/2021 01:03 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-MW6 Lab ID: 92556832006 Collected: 08/19/21 09:51 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:25
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:25
7440-38-2
Barium
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:25
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/01/2112:55
09/02/2105:25
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/01/2112:55
09/02/2105:25
7440-43-9
Chromium
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:25
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:25
7440-48-4
Copper
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:25
7440-50-8
Lead
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:25
7439-92-1
Nickel
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:25
7440-02-0
Selenium
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:25
7782-49-2
Silver
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:25
7440-22-4
Tin
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:25
7440-31-5
Vanadium
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:25
7440-62-2
Zinc
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:25
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/07/21 09:57
09/10/2102:21
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
08/20/21 22:31
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
08/20/21 22:31
107-13-1
Benzene
ND
ug/L
1.0
1
08/20/21 22:31
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
08/20/21 22:31
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
08/20/21 22:31
75-27-4
Bromoform
ND
ug/L
1.0
1
08/20/21 22:31
75-25-2
Bromomethane
ND
ug/L
2.0
1
08/20/21 22:31
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
08/20/21 22:31
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
08/20/21 22:31
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
08/20/21 22:31
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
08/20/21 22:31
108-90-7
Chloroethane
ND
ug/L
1.0
1
08/20/21 22:31
75-00-3
Chloroform
ND
ug/L
1.0
1
08/20/21 22:31
67-66-3
Chloromethane
ND
ug/L
1.0
1
08/20/21 22:31
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
08/20/21 22:31
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
08/20/21 22:31
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
08/20/21 22:31
106-93-4
Dibromomethane
ND
ug/L
1.0
1
08/20/21 22:31
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
08/20/21 22:31
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
08/20/21 22:31
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
08/20/21 22:31
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
08/20/21 22:31
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
08/20/21 22:31
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
L1.v1
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-MW6 Lab ID: 92556832006 Collected: 08/19/21 09:51 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/13/2021 01:03 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
0.35J
ug/L
100
%
100
%
99
%
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L
103 %
86 %
1.0
1
08/20/21 22:31
75-35-4
1.0
1
08/20/21 22:31
156-59-2
1.0
1
08/20/21 22:31
156-60-5
1.0
1
08/20/21 22:31
78-87-5
1.0
1
08/20/21 22:31
10061-01-5
1.0
1
08/20/21 22:31
10061-02-6
1.0
1
08/20/21 22:31
100-41-4
5.0
1
08/20/21 22:31
591-78-6
20.0
1
08/20/21 22:31
74-88-4 L2,v2
5.0
1
08/20/21 22:31
75-09-2
5.0
1
08/20/21 22:31
108-10-1
1.0
1
08/20/21 22:31
100-42-5
1.0
1
08/20/21 22:31
630-20-6
1.0
1
08/20/21 22:31
79-34-5
1.0
1
08/20/21 22:31
127-18-4
10.0
1
08/20/21 22:31
109-99-9
1.0
1
08/20/21 22:31
108-88-3
1.0
1
08/20/21 22:31
71-55-6
1.0
1
08/20/21 22:31
79-00-5
1.0
1
08/20/21 22:31
79-01-6
1.0
1
08/20/21 22:31
75-69-4
1.0
1
08/20/21 22:31
96-18-4
2.0
1
08/20/21 22:31
108-05-4
1.0
1
08/20/21 22:31
75-01-4
1.0
1
08/20/21 22:31
1330-20-7
70-130 1
70-130 1
70-130 1
2.0 1
70-130 1
66-133 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
08/20/21 22:31 460-00-4
08/20/21 22:31 17060-07-0
08/20/21 22:31 2037-26-5
08/20/21 16:07 123-91-1
08/20/21 16:07 17060-07-0
08/20/21 16:07 2037-26-5
Page 18 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-NES1 Lab ID: 92556832007 Collected: 08/19/21 12:53 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:28
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:28
7440-38-2
Barium
72.3
ug/L
5.0
1
09/01/2112:55
09/02/2105:28
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/01/2112:55
09/02/2105:28
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/01/2112:55
09/02/2105:28
7440-43-9
Chromium
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:28
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:28
7440-48-4
Copper
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:28
7440-50-8
Lead
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:28
7439-92-1
Nickel
7.1
ug/L
5.0
1
09/01/2112:55
09/02/2105:28
7440-02-0
Selenium
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:28
7782-49-2
Silver
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:28
7440-22-4
Vanadium
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:28
7440-62-2
Zinc
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:28
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020B Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
0.069J
ug/L
0.47
1
09/02/21 13:58
09/03/2123:29
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
08/20/21 22:50
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
08/20/21 22:50
107-13-1
Benzene
ND
ug/L
1.0
1
08/20/21 22:50
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
08/20/21 22:50
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
08/20/21 22:50
75-27-4
Bromoform
ND
ug/L
1.0
1
08/20/21 22:50
75-25-2
Bromomethane
ND
ug/L
2.0
1
08/20/21 22:50
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
08/20/21 22:50
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
08/20/21 22:50
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
08/20/21 22:50
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
08/20/21 22:50
108-90-7
Chloroethane
ND
ug/L
1.0
1
08/20/21 22:50
75-00-3
Chloroform
ND
ug/L
1.0
1
08/20/21 22:50
67-66-3
Chloromethane
ND
ug/L
1.0
1
08/20/21 22:50
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
08/20/21 22:50
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
08/20/21 22:50
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
08/20/21 22:50
106-93-4
Dibromomethane
ND
ug/L
1.0
1
08/20/21 22:50
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
08/20/21 22:50
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
08/20/21 22:50
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
08/20/21 22:50
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
08/20/21 22:50
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
08/20/21 22:50
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
08/20/21 22:50
75-35-4
REPORT OF LABORATORY ANALYSIS
v2
L1,v1
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-NES1 Lab ID: 92556832007 Collected: 08/19/21 12:53 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/13/2021 01:03 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
99
%
102
%
99
%
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L
105 %
92 %
1.0
1
08/20/21 22:50
156-59-2
1.0
1
08/20/21 22:50
156-60-5
1.0
1
08/20/21 22:50
78-87-5
1.0
1
08/20/21 22:50
10061-01-5
1.0
1
08/20/21 22:50
10061-02-6
1.0
1
08/20/21 22:50
100-41-4
5.0
1
08/20/21 22:50
591-78-6
20.0
1
08/20/21 22:50
74-88-4 L2,v2
5.0
1
08/20/21 22:50
75-09-2
5.0
1
08/20/21 22:50
108-10-1
1.0
1
08/20/21 22:50
100-42-5
1.0
1
08/20/21 22:50
630-20-6
1.0
1
08/20/21 22:50
79-34-5
1.0
1
08/20/21 22:50
127-18-4
10.0
1
08/20/21 22:50
109-99-9
1.0
1
08/20/21 22:50
108-88-3
1.0
1
08/20/21 22:50
71-55-6
1.0
1
08/20/21 22:50
79-00-5
1.0
1
08/20/21 22:50
79-01-6
1.0
1
08/20/21 22:50
75-69-4
1.0
1
08/20/21 22:50
96-18-4
2.0
1
08/20/21 22:50
108-05-4
1.0
1
08/20/21 22:50
75-01-4
1.0
1
08/20/21 22:50
1330-20-7
70-130 1
70-130 1
70-130 1
2.0 1
70-130 1
66-133 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
08/20/21 22:50 460-00-4
08/20/21 22:50 17060-07-0
08/20/21 22:50 2037-26-5
08/20/21 16:26 123-91-1
08/20/21 16:26 17060-07-0
08/20/21 16:26 2037-26-5
Page 20 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-Field Blank Lab ID: 92556832008 Collected: 08/19/21 13:30 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:31
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:31
7440-38-2
Barium
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:31
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/01/2112:55
09/02/2105:31
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/01/2112:55
09/02/2105:31
7440-43-9
Chromium
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:31
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:31
7440-48-4
Copper
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:31
7440-50-8
Lead
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:31
7439-92-1
Nickel
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:31
7440-02-0
Selenium
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:31
7782-49-2
Silver
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:31
7440-22-4
Tin
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:31
7440-31-5
Vanadium
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:31
7440-62-2
Zinc
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:31
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/02/21 13:58
09/03/2123:51
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
08/20/21 21:19
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
08/20/21 21:19
107-13-1
Benzene
ND
ug/L
1.0
1
08/20/21 21:19
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
08/20/21 21:19
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
08/20/21 21:19
75-27-4
Bromoform
ND
ug/L
1.0
1
08/20/21 21:19
75-25-2
Bromomethane
ND
ug/L
2.0
1
08/20/21 21:19
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
08/20/21 21:19
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
08/20/21 21:19
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
08/20/21 21:19
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
08/20/21 21:19
108-90-7
Chloroethane
ND
ug/L
1.0
1
08/20/21 21:19
75-00-3
Chloroform
ND
ug/L
1.0
1
08/20/21 21:19
67-66-3
Chloromethane
ND
ug/L
1.0
1
08/20/21 21:19
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
08/20/21 21:19
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
08/20/21 21:19
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
08/20/21 21:19
106-93-4
Dibromomethane
ND
ug/L
1.0
1
08/20/21 21:19
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
08/20/21 21:19
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
08/20/21 21:19
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
08/20/21 21:19
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
08/20/21 21:19
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
08/20/21 21:19
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
L1,v1
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-Field Blank Lab ID: 92556832008 Collected: 08/19/21 13:30 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/13/2021 01:03 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
12.9
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
99
%
99
%
98
%
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L
100 %
99 %
1.0
1
08/20/21 21:19
75-35-4
1.0
1
08/20/21 21:19
156-59-2
1.0
1
08/20/21 21:19
156-60-5
1.0
1
08/20/21 21:19
78-87-5
1.0
1
08/20/21 21:19
10061-01-5
1.0
1
08/20/21 21:19
10061-02-6
1.0
1
08/20/21 21:19
100-41-4
5.0
1
08/20/21 21:19
591-78-6
20.0
1
08/20/21 21:19
74-88-4 L2,v2
5.0
1
08/20/21 21:19
75-09-2
5.0
1
08/20/21 21:19
108-10-1
1.0
1
08/20/21 21:19
100-42-5
1.0
1
08/20/21 21:19
630-20-6
1.0
1
08/20/21 21:19
79-34-5
1.0
1
08/20/21 21:19
127-18-4
10.0
1
08/20/21 21:19
109-99-9
1.0
1
08/20/21 21:19
108-88-3
1.0
1
08/20/21 21:19
71-55-6
1.0
1
08/20/21 21:19
79-00-5
1.0
1
08/20/21 21:19
79-01-6
1.0
1
08/20/21 21:19
75-69-4
1.0
1
08/20/21 21:19
96-18-4
2.0
1
08/20/21 21:19
108-05-4
1.0
1
08/20/21 21:19
75-01-4
1.0
1
08/20/21 21:19
1330-20-7
70-130 1
70-130 1
70-130 1
2.0 1
70-130 1
66-133 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
08/20/21 21:19 460-00-4
08/20/21 21:19 17060-07-0
08/20/21 21:19 2037-26-5
08/20/21 15:40 123-91-1
08/20/21 15:40 17060-07-0
08/20/21 15:40 2037-26-5
Page 22 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-SW1 Lab ID: 92556832009 Collected: 08/19/21 13:40 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:35
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:35
7440-38-2
Barium
45.1
ug/L
5.0
1
09/01/2112:55
09/02/2105:35
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/01/2112:55
09/02/2105:35
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/01/2112:55
09/02/2105:35
7440-43-9
Chromium
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:35
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:35
7440-48-4
Copper
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:35
7440-50-8
Lead
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:35
7439-92-1
Nickel
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:35
7440-02-0
Selenium
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:35
7782-49-2
Silver
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:35
7440-22-4
Vanadium
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:35
7440-62-2
Zinc
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:35
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020B Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/02/21 13:58
09/03/2123:56
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
08/20/21 21:37
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
08/20/21 21:37
107-13-1
Benzene
ND
ug/L
1.0
1
08/20/21 21:37
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
08/20/21 21:37
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
08/20/21 21:37
75-27-4
Bromoform
ND
ug/L
1.0
1
08/20/21 21:37
75-25-2
Bromomethane
ND
ug/L
2.0
1
08/20/21 21:37
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
08/20/21 21:37
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
08/20/21 21:37
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
08/20/21 21:37
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
08/20/21 21:37
108-90-7
Chloroethane
ND
ug/L
1.0
1
08/20/21 21:37
75-00-3
Chloroform
ND
ug/L
1.0
1
08/20/21 21:37
67-66-3
Chloromethane
ND
ug/L
1.0
1
08/20/21 21:37
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
08/20/21 21:37
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
08/20/21 21:37
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
08/20/21 21:37
106-93-4
Dibromomethane
ND
ug/L
1.0
1
08/20/21 21:37
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
08/20/21 21:37
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
08/20/21 21:37
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
08/20/21 21:37
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
08/20/21 21:37
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
08/20/21 21:37
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
08/20/21 21:37
75-35-4
REPORT OF LABORATORY ANALYSIS
v2
L1,v1
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-SW1 Lab ID: 92556832009 Collected: 08/19/21 13:40 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/13/2021 01:03 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
98
%
100
%
99
%
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
ND ug/L
102 %
90 %
1.0
1
08/20/21 21:37
156-59-2
1.0
1
08/20/21 21:37
156-60-5
1.0
1
08/20/21 21:37
78-87-5
1.0
1
08/20/21 21:37
10061-01-5
1.0
1
08/20/21 21:37
10061-02-6
1.0
1
08/20/21 21:37
100-41-4
5.0
1
08/20/21 21:37
591-78-6
20.0
1
08/20/21 21:37
74-88-4 L2,v2
5.0
1
08/20/21 21:37
75-09-2
5.0
1
08/20/21 21:37
108-10-1
1.0
1
08/20/21 21:37
100-42-5
1.0
1
08/20/21 21:37
630-20-6
1.0
1
08/20/21 21:37
79-34-5
1.0
1
08/20/21 21:37
127-18-4
10.0
1
08/20/21 21:37
109-99-9
1.0
1
08/20/21 21:37
108-88-3
1.0
1
08/20/21 21:37
71-55-6
1.0
1
08/20/21 21:37
79-00-5
1.0
1
08/20/21 21:37
79-01-6
1.0
1
08/20/21 21:37
75-69-4
1.0
1
08/20/21 21:37
96-18-4
2.0
1
08/20/21 21:37
108-05-4
1.0
1
08/20/21 21:37
75-01-4
1.0
1
08/20/21 21:37
1330-20-7
70-130 1
70-130 1
70-130 1
2.0 1
70-130 1
66-133 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
08/20/21 21:37 460-00-4
08/20/21 21:37 17060-07-0
08/20/21 21:37 2037-26-5
08/20/21 16:45 123-91-1
08/20/21 16:45 17060-07-0
08/20/21 16:45 2037-26-5
Page 24 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-SW2 Lab ID: 92556832010 Collected: 08/19/21 13:10 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:38
7440-36-0
Arsenic
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:38
7440-38-2
Barium
91.9
ug/L
5.0
1
09/01/2112:55
09/02/2105:38
7440-39-3
Beryllium
ND
ug/L
1.0
1
09/01/2112:55
09/02/2105:38
7440-41-7
Cadmium
ND
ug/L
1.0
1
09/01/2112:55
09/02/2105:38
7440-43-9
Chromium
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:38
7440-47-3
Cobalt
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:38
7440-48-4
Copper
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:38
7440-50-8
Lead
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:38
7439-92-1
Nickel
25.1
ug/L
5.0
1
09/01/2112:55
09/02/2105:38
7440-02-0
Selenium
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:38
7782-49-2
Silver
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:38
7440-22-4
Vanadium
ND
ug/L
5.0
1
09/01/2112:55
09/02/2105:38
7440-62-2
Zinc
ND
ug/L
10.0
1
09/01/2112:55
09/02/2105:38
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020B Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.47
1
09/02/21 13:58
09/04/2100:00
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
08/20/21 21:55
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
08/20/21 21:55
107-13-1
Benzene
ND
ug/L
1.0
1
08/20/21 21:55
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
08/20/21 21:55
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
08/20/21 21:55
75-27-4
Bromoform
ND
ug/L
1.0
1
08/20/21 21:55
75-25-2
Bromomethane
ND
ug/L
2.0
1
08/20/21 21:55
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
08/20/21 21:55
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
08/20/21 21:55
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
08/20/21 21:55
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
08/20/21 21:55
108-90-7
Chloroethane
ND
ug/L
1.0
1
08/20/21 21:55
75-00-3
Chloroform
ND
ug/L
1.0
1
08/20/21 21:55
67-66-3
Chloromethane
ND
ug/L
1.0
1
08/20/21 21:55
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
08/20/21 21:55
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
08/20/21 21:55
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
08/20/21 21:55
106-93-4
Dibromomethane
ND
ug/L
1.0
1
08/20/21 21:55
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
08/20/21 21:55
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
08/20/21 21:55
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
08/20/21 21:55
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
08/20/21 21:55
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
08/20/21 21:55
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
08/20/21 21:55
75-35-4
REPORT OF LABORATORY ANALYSIS
v2
L1,v1
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-SW2 Lab ID: 92556832010 Collected: 08/19/21 13:10 Received: 08/19/21 15:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/13/2021 01:03 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
96
%
100
%
100
%
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
26.0 ug/L
102 %
89 %
1.0
1
08/20/21 21:55
156-59-2
1.0
1
08/20/21 21:55
156-60-5
1.0
1
08/20/21 21:55
78-87-5
1.0
1
08/20/21 21:55
10061-01-5
1.0
1
08/20/21 21:55
10061-02-6
1.0
1
08/20/21 21:55
100-41-4
5.0
1
08/20/21 21:55
591-78-6
20.0
1
08/20/21 21:55
74-88-4 L2,v2
5.0
1
08/20/21 21:55
75-09-2
5.0
1
08/20/21 21:55
108-10-1
1.0
1
08/20/21 21:55
100-42-5
1.0
1
08/20/21 21:55
630-20-6
1.0
1
08/20/21 21:55
79-34-5
1.0
1
08/20/21 21:55
127-18-4
10.0
1
08/20/21 21:55
109-99-9
1.0
1
08/20/21 21:55
108-88-3
1.0
1
08/20/21 21:55
71-55-6
1.0
1
08/20/21 21:55
79-00-5
1.0
1
08/20/21 21:55
79-01-6
1.0
1
08/20/21 21:55
75-69-4
1.0
1
08/20/21 21:55
96-18-4
2.0
1
08/20/21 21:55
108-05-4
1.0
1
08/20/21 21:55
75-01-4
1.0
1
08/20/21 21:55
1330-20-7
70-130 1
70-130 1
70-130 1
2.0 1
70-130 1
66-133 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
08/20/21 21:55 460-00-4
08/20/21 21:55 17060-07-0
08/20/21 21:55 2037-26-5
08/20/21 17:04 123-91-1
08/20/21 17:04 17060-07-0
08/20/21 17:04 2037-26-5
Page 26 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-Trip Blank
Lab ID: 92556832011 Collected:
08/19/21
00:00
Received: 08/19/21 15:40 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
08/20/21 20:43
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
08/20/21 20:43
107-13-1
Benzene
ND
ug/L
1.0
1
08/20/21 20:43
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
08/20/21 20:43
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
08/20/21 20:43
75-27-4
Bromoform
ND
ug/L
1.0
1
08/20/21 20:43
75-25-2
Bromomethane
ND
ug/L
2.0
1
08/20/21 20:43
74-83-9 v2
2-Butanone (MEK)
ND
ug/L
5.0
1
08/20/21 20:43
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
08/20/21 20:43
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
08/20/21 20:43
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
08/20/21 20:43
108-90-7
Chloroethane
ND
ug/L
1.0
1
08/20/21 20:43
75-00-3
Chloroform
ND
ug/L
1.0
1
08/20/21 20:43
67-66-3
Chloromethane
ND
ug/L
1.0
1
08/20/21 20:43
74-87-3 L1,v1
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
08/20/21 20:43
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
08/20/21 20:43
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
08/20/21 20:43
106-93-4
Dibromomethane
ND
ug/L
1.0
1
08/20/21 20:43
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
08/20/21 20:43
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
08/20/21 20:43
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
08/20/21 20:43
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
08/20/21 20:43
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
08/20/21 20:43
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
08/20/21 20:43
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
08/20/21 20:43
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
08/20/21 20:43
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
08/20/21 20:43
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
08/20/21 20:43
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
08/20/21 20:43
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
08/20/21 20:43
100-41-4
2-Hexanone
ND
ug/L
5.0
1
08/20/21 20:43
591-78-6
lodomethane
ND
ug/L
20.0
1
08/20/21 20:43
74-88-4 L2,v2
Methylene Chloride
13.0
ug/L
5.0
1
08/20/21 20:43
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
08/20/21 20:43
108-10-1
Styrene
ND
ug/L
1.0
1
08/20/21 20:43
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
08/20/21 20:43
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
08/20/21 20:43
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
08/20/21 20:43
127-18-4
Tetrahydrofuran
ND
ug/L
10.0
1
08/20/21 20:43
109-99-9
Toluene
ND
ug/L
1.0
1
08/20/21 20:43
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
08/20/21 20:43
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
08/20/21 20:43
79-00-5
Trichloroethene
ND
ug/L
1.0
1
08/20/21 20:43
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
08/20/21 20:43
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
08/20/21 20:43
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
08/20/21 20:43
108-05-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 62

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Sample: 3902-Trip Blank
Parameters
Lab ID: 92556832011 Collected: 08/19/21 00:00
Results Units Report Limit DF
Received: 08/19/21 15:40 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Vinyl chloride
ND ug/L
1.0
1
08/20/21 20:43
75-01-4
Xylene (Total)
ND ug/L
1.0
1
08/20/21 20:43
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
08/20/21 20:43
460-00-4
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
08/20/21 20:43
17060-07-0
Toluene-d8 (S)
100 %
70-130
1
08/20/21 20:43
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L
2.0
1
08/20/21 16:00
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
08/20/21 16:00
17060-07-0
Toluene-d8 (S)
97 %
66-133
1
08/20/21 16:00
2037-26-5
Date: 09/13/2021 01:03 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 28 of 62

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
QC Batch: 642036 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92556832003, 92556832004
METHOD BLANK: 3369692
Matrix:
Water
Associated Lab Samples: 92556832003, 92556832004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg/L
ND
0.040
08/20/21 15:38
LABORATORY CONTROL SAMPLE:
3369693
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Nitrogen, Nitrate
mg/L
1.5
1.5
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3369694 3369695
MS MSD
92556832003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate mg/L ND 1.5 1.5 1.5 1.5 99 98 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC.
Page 29 of 62

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
QC Batch: 642092 Analysis Method: SM 521 OB-2011
QC Batch Method: SM 521OB-2011 Analysis Description: 5210E BOD, 5 day Final EDN
Laboratory: Pace Analytical Services - Eden
Associated Lab Samples: 92556832003, 92556832004
METHOD BLANK: 3370068
Matrix:
Water
Associated Lab Samples: 92556832003, 92556832004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
BOD, 5 day
ug/L
ND
2000
08/25/21 13:51
LABORATORY CONTROL SAMPLE:
3370069
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
BOD, 5 day
ug/L
198000
174000
88 84.6-115.4
SAMPLE DUPLICATE: 3370071
92556832003 Dup
Parameter Units Result Result RPD Qualifiers
BOD, 5 day ug/L ND ND B2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 62

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
QC Batch: 642636 Analysis Method: RSK 175 Modified
QC Batch Method: RSK 175 Modified Analysis Description: RSK 175 HEADSPACE
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92556832003, 92556832004
METHOD BLANK: 3372564 Matrix: Water
Associated Lab Samples: 92556832003, 92556832004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Methane ug/L ND 10.0 08/24/2115:49
LABORATORY CONTROL SAMPLE: 3372565
Spike LCS
LCS
% Rec
Parameter Units
Conc. Result
% Rec
Limits
Qualifiers
Methane ug/L
396 393
99
70-130
MATRIX SPIKE SAMPLE: 3374759
92556832003 Spike
MS
MS
% Rec
Parameter Units
Result Conc.
Result
% Rec
Limits Qualifiers
Methane ug/L
603 396
974
94
70-130
SAMPLE DUPLICATE: 3374758
92556487003 Dup
Parameter Units Result Result RPD Qualifiers
Methane ug/L 91.9 82.8 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 62

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
QC Batch: 644216 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92556832001, 92556832002, 92556832003, 92556832004, 92556832005, 92556832006, 92556832007,
92556832008,92556832009,92556832010
METHOD BLANK: 3380012 Matrix: Water
Associated Lab Samples: 92556832001, 92556832002, 92556832003, 92556832004, 92556832005, 92556832006, 92556832007,
92556832008,92556832009,92556832010
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Antimony
ug/L
ND
5.0
09/02/2104:45
Arsenic
ug/L
ND
10.0
09/02/2104:45
Barium
ug/L
ND
5.0
09/02/2104:45
Beryllium
ug/L
ND
1.0
09/02/2104:45
Cadmium
ug/L
ND
1.0
09/02/2104:45
Chromium
ug/L
ND
5.0
09/02/2104:45
Cobalt
ug/L
ND
5.0
09/02/2104:45
Copper
ug/L
ND
5.0
09/02/2104:45
Lead
ug/L
ND
5.0
09/02/2104:45
Nickel
ug/L
ND
5.0
09/02/2104:45
Selenium
ug/L
ND
10.0
09/02/2104:45
Silver
ug/L
ND
5.0
09/02/2104:45
Tin
ug/L
ND
5.0
09/02/2104:45
Vanadium
ug/L
ND
5.0
09/02/2104:45
Zinc
ug/L
ND
10.0
09/02/2104:45
LABORATORY CONTROL SAMPLE:
Parameter
3380013
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
508
102
80-120
Arsenic
ug/L
500
479
96
80-120
Barium
ug/L
500
492
98
80-120
Beryllium
ug/L
500
486
97
80-120
Cadmium
ug/L
500
474
95
80-120
Chromium
ug/L
500
445
89
80-120
Cobalt
ug/L
500
472
94
80-120
Copper
ug/L
500
492
98
80-120
Lead
ug/L
500
480
96
80-120
Nickel
ug/L
500
480
96
80-120
Selenium
ug/L
500
475
95
80-120
Silver
ug/L
250
234
94
80-120
Tin
ug/L
500
495
99
80-120
Vanadium
ug/L
500
464
93
80-120
Zinc
ug/L
500
451
90
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 62

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Butner Landfill Compliance
92556832
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3380014
3380015
MS
MSD
92556832001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
520
536
104
107
75-125
3
Arsenic
ug/L
ND
500
500
492
504
98
101
75-125
2
Barium
ug/L
6.2
500
500
509
526
101
104
75-125
3
Beryllium
ug/L
ND
500
500
490
512
98
102
75-125
4
Cadmium
ug/L
ND
500
500
491
506
98
101
75-125
3
Chromium
ug/L
ND
500
500
455
475
91
95
75-125
4
Cobalt
ug/L
ND
500
500
477
492
95
98
75-125
3
Copper
ug/L
13.7
500
500
513
535
100
104
75-125
4
Lead
ug/L
ND
500
500
488
502
97
100
75-125
3
Nickel
ug/L
3.5J
500
500
489
506
97
101
75-125
4
Selenium
ug/L
ND
500
500
512
527
102
105
75-125
3
Silver
ug/L
ND
250
250
239
249
95
100
75-125
4
Tin
ug/L
ND
500
500
495
514
99
103
75-125
4
Vanadium
ug/L
ND
500
500
475
494
95
98
75-125
4
Zinc
ug/L
44.2
500
500
513
525
94
96
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
QC Batch: 644733 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92556832001, 92556832002, 92556832003, 92556832004, 92556832005, 92556832006
METHOD BLANK: 3382401
Matrix:
Water
Associated Lab Samples: 92556832001, 92556832002, 92556832003, 92556832004, 92556832005, 92556832006
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
0.47
09/10/2100:09
LABORATORY CONTROL SAMPLE:
3382402
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
25
23.7
95 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3382403 3382404
MS MSD
92556487002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 25 25 24.4 23.9 98 95 75-125 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC.
Page 34 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
QC Batch: 644743 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92556832007, 92556832008, 92556832009, 92556832010
METHOD BLANK: 3382433
Matrix:
Water
Associated Lab Samples: 92556832007, 92556832008, 92556832009, 92556832010
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
0.47
09/03/2122:58
LABORATORY CONTROL SAMPLE:
3382434
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
25
25.0
100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3382435 3382436
MS MSD
92556832007 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L 0.069J 25 25 25.0 25.2 100 101 75-125 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC.
Page 35 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
QC Batch: 642049 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92556832001, 92556832002, 92556832003, 92556832004, 92556832006, 92556832007, 92556832008,
92556832009,92556832010,92556832011
METHOD BLANK: 3369810 Matrix: Water
Associated Lab Samples: 92556832001, 92556832002, 92556832003, 92556832004, 92556832006, 92556832007, 92556832008,
92556832009,92556832010,92556832011
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
08/20/21 19:49
1,1,1-Trichloroethane
ug/L
ND
1.0
08/20/21 19:49
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
08/20/21 19:49
1,1,2-Trichloroethane
ug/L
ND
1.0
08/20/21 19:49
1,1-Dichloroethane
ug/L
ND
1.0
08/20/21 19:49
1,1-Dichloroethene
ug/L
ND
1.0
08/20/21 19:49
1,2,3-Trichloropropane
ug/L
ND
1.0
08/20/21 19:49
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
08/20/21 19:49
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
08/20/21 19:49
1,2-Dichlorobenzene
ug/L
ND
1.0
08/20/21 19:49
1,2-Dichloroethane
ug/L
ND
1.0
08/20/21 19:49
1,2-Dichloropropane
ug/L
ND
1.0
08/20/21 19:49
1,4-Dichlorobenzene
ug/L
ND
1.0
08/20/21 19:49
2-Butanone (MEK)
ug/L
ND
5.0
08/20/21 19:49
2-Hexanone
ug/L
ND
5.0
08/20/21 19:49
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
08/20/21 19:49
Acetone
ug/L
ND
25.0
08/20/21 19:49
Acrylonitrile
ug/L
ND
10.0
08/20/21 19:49
Benzene
ug/L
ND
1.0
08/20/21 19:49
Bromochloromethane
ug/L
ND
1.0
08/20/21 19:49
Bromodichloromethane
ug/L
ND
1.0
08/20/21 19:49
Bromoform
ug/L
ND
1.0
08/20/21 19:49
Bromomethane
ug/L
ND
2.0
08/20/21 19:49
Carbon disulfide
ug/L
ND
2.0
08/20/21 19:49
Carbon tetrachloride
ug/L
ND
1.0
08/20/21 19:49
Chlorobenzene
ug/L
ND
1.0
08/20/21 19:49
Chloroethane
ug/L
ND
1.0
08/20/21 19:49
Chloroform
ug/L
0.59J
1.0
08/20/21 19:49
Chloromethane
ug/L
ND
1.0
08/20/21 19:49
cis-1,2-Dichloroethene
ug/L
ND
1.0
08/20/21 19:49
cis-1,3-Dichloropropene
ug/L
ND
1.0
08/20/21 19:49
Dibromochloromethane
ug/L
ND
1.0
08/20/21 19:49
Dibromomethane
ug/L
ND
1.0
08/20/21 19:49
Ethylbenzene
ug/L
ND
1.0
08/20/21 19:49
lodomethane
ug/L
ND
20.0
08/20/21 19:49
Methylene Chloride
ug/L
ND
5.0
08/20/21 19:49
Styrene
ug/L
ND
1.0
08/20/21 19:49
Tetrachloroethene
ug/L
ND
1.0
08/20/21 19:49
Tetrahydrofuran
ug/L
ND
10.0
08/20/21 19:49
v2
v1
v2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 62

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
METHOD BLANK: 3369810 Matrix: Water
Associated Lab Samples: 92556832001, 92556832002, 92556832003, 92556832004, 92556832006, 92556832007, 92556832008,
92556832009,92556832010,92556832011
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Toluene
ug/L
ND
1.0
08/20/21 19:49
trans-1,2-Dichloroethene
ug/L
ND
1.0
08/20/21 19:49
trans- 1,3-Dichloropropene
ug/L
ND
1.0
08/20/21 19:49
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
08/20/21 19:49
Trichloroethene
ug/L
ND
1.0
08/20/21 19:49
Trichlorofluoromethane
ug/L
ND
1.0
08/20/21 19:49
Vinyl acetate
ug/L
ND
2.0
08/20/21 19:49
Vinyl chloride
ug/L
ND
1.0
08/20/21 19:49
Xylene (Total)
ug/L
ND
1.0
08/20/21 19:49
1,2-Dichloroethane-d4 (S)
%
98
70-130
08/20/21 19:49
4-Bromofluorobenzene (S)
%
98
70-130
08/20/21 19:49
Toluene-d8 (S)
%
99
70-130
08/20/21 19:49
LABORATORY CONTROL SAMPLE:
Parameter
3369811
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
51.6
103
70-130
1,1,1-Trichloroethane
ug/L
50
52.5
105
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
55.3
111
70-130
1,1,2-Trichloroethane
ug/L
50
52.9
106
70-130
1,1-Dichloroethane
ug/L
50
56.6
113
70-130
1,1-Dichloroethene
ug/L
50
55.6
111
70-132
1,2,3-Trichloropropane
ug/L
50
53.0
106
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
57.9
116
70-132
1,2-Dibromoethane (EDB)
ug/L
50
53.4
107
70-130
1,2-Dichlorobenzene
ug/L
50
52.9
106
70-130
1,2-Dichloroethane
ug/L
50
50.8
102
70-130
1,2-Dichloropropane
ug/L
50
56.0
112
70-130
1,4-Dichlorobenzene
ug/L
50
53.2
106
70-130
2-Butanone (MEK)
ug/L
100
114
114
70-133
2-Hexanone
ug/L
100
126
126
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
122
122
70-130
Acetone
ug/L
100
116
116
70-144
Acrylonitrile
ug/L
250
295
118
70-130
Benzene
ug/L
50
53.4
107
70-130
Bromochloromethane
ug/L
50
51.0
102
70-130
Bromodichloromethane
ug/L
50
52.5
105
70-130
Bromoform
ug/L
50
51.4
103
70-131
Bromomethane
ug/L
50
33.0
66
30-177 v2
Carbon disulfide
ug/L
50
54.7
109
70-133
Carbon tetrachloride
ug/L
50
52.2
104
70-130
Chlorobenzene
ug/L
50
52.8
106
70-130
Chloroethane
ug/L
50
50.9
102
46-131
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 62

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
LABORATORY CONTROL SAMPLE:
Parameter
3369811
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Chloroform
ug/L
50
51.1
102
70-130
Chloromethane
ug/L
50
75.3
151
49-130 L1,v1
cis-1,2-Dichloroethene
ug/L
50
55.1
110
70-130
cis-1,3-Dichloropropene
ug/L
50
54.2
108
70-130
Dibromochloromethane
ug/L
50
53.6
107
70-130
Dibromomethane
ug/L
50
53.3
107
70-130
Ethylbenzene
ug/L
50
52.5
105
70-130
lodomethane
ug/L
100
45.9
46
47-140 L2,v2
Methylene Chloride
ug/L
50
54.8
110
68-130
Styrene
ug/L
50
55.0
110
70-130
Tetrachloroethene
ug/L
50
51.4
103
70-130
Tetrahydrofuran
ug/L
500
602
120
70-130
Toluene
ug/L
50
53.4
107
70-130
trans-1,2-Dichloroethene
ug/L
50
55.7
111
70-130
trans- 1,3-Dichloropropene
ug/L
50
52.9
106
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
61.8
124
25-200
Trichloroethene
ug/L
50
51.3
103
70-130
Trichlorofluoromethane
ug/L
50
46.0
92
61-130
Vinyl acetate
ug/L
100
117
117
70-140
Vinyl chloride
ug/L
50
54.8
110
59-142
Xylene (Total)
ug/L
150
157
105
70-130
1,2-Dichloroethane-d4 (S)
%
91
70-130
4-Bromofluorobenzene (S)
%
98
70-130
Toluene-d8 (S)
%
102
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3369812
MS
92556832009 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3369813
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.9
20.9
110
104
70-135
5
1,1,1-Trichloroethane
ug/L
ND
20
20
21.8
20.9
109
104
70-148
4
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.1
21.1
110
106
70-131
4
1,1,2-Trichloroethane
ug/L
ND
20
20
21.9
20.8
110
104
70-136
5
1,1-Dichloroethane
ug/L
ND
20
20
23.7
22.2
119
111
70-147
6
1,1-Dichloroethene
ug/L
ND
20
20
23.4
22.4
117
112
70-158
4
1,2,3-Trichloropropane
ug/L
ND
20
20
22.0
20.6
110
103
67-137
6
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
24.6
24.0
123
120
69-136
2
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.4
21.3
112
107
70-137
5
1,2-Dichlorobenzene
ug/L
ND
20
20
22.3
21.9
112
110
70-133
2
1,2-Dichloroethane
ug/L
ND
20
20
20.3
19.4
102
97
67-138
4
1,2-Dichloropropane
ug/L
ND
20
20
22.8
21.9
114
109
70-138
4
1,4-Dichlorobenzene
ug/L
ND
20
20
22.5
21.9
112
109
70-133
3
2-Butanone (MEK)
ug/L
ND
40
40
45.6
44.3
114
111
61-147
3
2-Hexanone
ug/L
ND
40
40
49.1
46.3
123
116
67-139
6
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
45.7
43.7
114
109
67-136
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3369812
MS
92556832009 Spike
Parameter Units Result Conc.
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Ethylbenzene
lodomethane
Methylene Chloride
Styrene
Tetrachloroethene
Tetrahydrofuran
Toluene
trans-1,2-Dichloroethene
trans- 1,3-Dichloropropene
trans-1,4-Dichloro-2-butene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Xylene (Total)
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
ug/L ND
40
100
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
40
20
20
20
200
20
20
20
20
20
20
40
20
60
MSD
Spike
Conc.
40
100
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
40
20
20
20
200
20
20
20
20
20
20
40
20
60
3369813
MS
Result
46.1
120
22.8
22.4
21.6
21.9
18.6
23.3
21.3
22.6
22.7
21.6
24.1
23.3
21.9
22.9
22.1
22.3
29.2
22.2
22.3
22.7
237
22.0
23.6
21.7
21.8
22.0
19.4
46.6
24.6
66.8
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
43.6
115
109
55-159
113
120
113
68-140
21.4
114
107
67-150
21.5
112
107
70-146
20.2
108
101
70-138
20.5
110
103
57-138
18.2
93
91
10-200
22.5
116
112
70-152
21.0
107
105
70-147
21.4
113
107
70-137
21.7
114
109
51-166
20.4
108
102
70-144
22.1
121
110
24-161
21.9
117
110
67-148
20.7
110
103
70-142
21.5
114
108
68-138
21.3
111
106
70-134
21.5
112
108
68-143
28.6
73
71
20-161
20.6
111
103
64-148
21.9
111
109
70-136
21.7
113
108
70-139
222
119
111
65-145
21.1
110
106
47-157
22.5
118
113
70-149
20.3
108
102
70-138
20.8
109
104
31-145
21.4
110
107
70-149
18.9
97
94
61-154
43.7
117
109
48-156
23.3
123
117
55-172
64.2
111
107
66-145
92
94
70-130
97
97
70-130
99
99
70-130
RPD Qual
5
6
6
4
7
7
2
3
2
5
4
6
9
6
6
6
4
4
2 v2
7
2
5
7
4
5
7
5
2
3
7
5
4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC.
Page 39 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
QC Batch: 643524 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92556832005
METHOD BLANK: 3376615
Associated Lab Samples: 92556832005
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
08/27/21 11:50
1,1,1-Trichloroethane
ug/L
ND
1.0
08/27/21 11:50
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
08/27/21 11:50
1,1,2-Trichloroethane
ug/L
ND
1.0
08/27/21 11:50
1,1-Dichloroethane
ug/L
ND
1.0
08/27/21 11:50
1,1-Dichloroethene
ug/L
ND
1.0
08/27/21 11:50
1,2,3-Trichloropropane
ug/L
ND
1.0
08/27/21 11:50
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
08/27/21 11:50
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
08/27/21 11:50
1,2-Dichlorobenzene
ug/L
ND
1.0
08/27/21 11:50
1,2-Dichloroethane
ug/L
ND
1.0
08/27/21 11:50
1,2-Dichloropropane
ug/L
ND
1.0
08/27/21 11:50
1,4-Dichlorobenzene
ug/L
ND
1.0
08/27/21 11:50
2-Butanone (MEK)
ug/L
ND
5.0
08/27/21 11:50
2-Hexanone
ug/L
ND
5.0
08/27/21 11:50
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
08/27/21 11:50
Acetone
ug/L
ND
25.0
08/27/21 11:50
Acrylonitrile
ug/L
ND
10.0
08/27/21 11:50
Benzene
ug/L
ND
1.0
08/27/21 11:50
Bromochloromethane
ug/L
ND
1.0
08/27/21 11:50
Bromodichloromethane
ug/L
ND
1.0
08/27/21 11:50
Bromoform
ug/L
ND
1.0
08/27/21 11:50
Bromomethane
ug/L
ND
2.0
08/27/21 11:50
Carbon disulfide
ug/L
ND
2.0
08/27/21 11:50
Carbon tetrachloride
ug/L
ND
1.0
08/27/21 11:50
Chlorobenzene
ug/L
ND
1.0
08/27/21 11:50
Chloroethane
ug/L
ND
1.0
08/27/21 11:50
Chloroform
ug/L
0.45J
1.0
08/27/21 11:50
Chloromethane
ug/L
ND
1.0
08/27/21 11:50
cis-1,2-Dichloroethene
ug/L
ND
1.0
08/27/21 11:50
cis-1,3-Dichloropropene
ug/L
ND
1.0
08/27/21 11:50
Dibromochloromethane
ug/L
ND
1.0
08/27/21 11:50
Dibromomethane
ug/L
ND
1.0
08/27/21 11:50
Ethylbenzene
ug/L
ND
1.0
08/27/21 11:50
lodomethane
ug/L
ND
20.0
08/27/21 11:50 v1
Methylene Chloride
ug/L
ND
5.0
08/27/21 11:50
Styrene
ug/L
ND
1.0
08/27/21 11:50
Tetrachloroethene
ug/L
ND
1.0
08/27/21 11:50
Toluene
ug/L
ND
1.0
08/27/21 11:50
trans-1,2-Dichloroethene
ug/L
ND
1.0
08/27/21 11:50
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC.
Page 40 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
METHOD BLANK: 3376615
Associated Lab Samples: 92556832005
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
trans- 1,3-Dichloropropene
ug/L
ND
1.0
08/27/21 11:50
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
08/27/21 11:50
Trichloroethene
ug/L
ND
1.0
08/27/21 11:50
Trichlorofluoromethane
ug/L
ND
1.0
08/27/21 11:50
Vinyl acetate
ug/L
ND
2.0
08/27/21 11:50
Vinyl chloride
ug/L
ND
1.0
08/27/21 11:50
Xylene (Total)
ug/L
ND
1.0
08/27/21 11:50
1,2-Dichloroethane-d4 (S)
%
96
70-130
08/27/21 11:50
4-Bromofluorobenzene (S)
%
97
70-130
08/27/21 11:50
Toluene-d8 (S)
%
100
70-130
08/27/21 11:50
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3376616
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
49.3
99
70-130
1,1,1-Trichloroethane
ug/L
50
49.1
98
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
48.0
96
70-130
1,1,2-Trichloroethane
ug/L
50
48.0
96
70-130
1,1-Dichloroethane
ug/L
50
48.3
97
70-130
1,1-Dichloroethene
ug/L
50
50.6
101
70-132
1,2,3-Trichloropropane
ug/L
50
47.0
94
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
49.5
99
70-132
1,2-Dibromoethane (EDB)
ug/L
50
50.0
100
70-130
1,2-Dichlorobenzene
ug/L
50
50.6
101
70-130
1,2-Dichloroethane
ug/L
50
46.6
93
70-130
1,2-Dichloropropane
ug/L
50
48.5
97
70-130
1,4-Dichlorobenzene
ug/L
50
51.3
103
70-130
2-Butanone (MEK)
ug/L
100
86.4
86
70-133
2-Hexanone
ug/L
100
87.5
88
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
90.1
90
70-130
Acetone
ug/L
100
91.5
92
70-144
Acrylonitrile
ug/L
250
233
93
70-130
Benzene
ug/L
50
48.6
97
70-130
Bromochloromethane
ug/L
50
51.6
103
70-130
Bromodichloromethane
ug/L
50
49.5
99
70-130
Bromoform
ug/L
50
50.2
100
70-131
Bromomethane
ug/L
50
62.8
126
30-177
Carbon disulfide
ug/L
50
51.5
103
70-133
Carbon tetrachloride
ug/L
50
50.0
100
70-130
Chlorobenzene
ug/L
50
49.9
100
70-130
Chloroethane
ug/L
50
45.7
91
46-131
Chloroform
ug/L
50
47.1
94
70-130
Chloromethane
ug/L
50
45.4
91
49-130
cis-1,2-Dichloroethene
ug/L
50
47.9
96
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 62

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
LABORATORY CONTROL SAMPLE:
Parameter
3376616
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
cis-1,3-Dichloropropene
ug/L
50
48.8
98
70-130
Dibromochloromethane
ug/L
50
50.9
102
70-130
Dibromomethane
ug/L
50
50.3
101
70-130
Ethylbenzene
ug/L
50
49.6
99
70-130
lodomethane
ug/L
100
146
146
47-140 L1,v1
Methylene Chloride
ug/L
50
45.0
90
68-130
Styrene
ug/L
50
51.1
102
70-130
Tetrachloroethene
ug/L
50
49.8
100
70-130
Toluene
ug/L
50
48.9
98
70-130
trans-1,2-Dichloroethene
ug/L
50
48.3
97
70-130
trans- 1,3-Dichloropropene
ug/L
50
49.2
98
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
42.9
86
25-200
Trichloroethene
ug/L
50
49.8
100
70-130
Trichlorofluoromethane
ug/L
50
47.7
95
61-130
Vinyl acetate
ug/L
100
93.5
94
70-140
Vinyl chloride
ug/L
50
49.3
99
59-142
Xylene (Total)
ug/L
150
148
99
70-130
1,2-Dichloroethane-d4 (S)
%
98
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3376617
MS
92557975014 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3376618
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
22.4
21.7
112
108
70-135
3
1,1,1-Trichloroethane
ug/L
ND
20
20
22.8
23.0
114
115
70-148
1
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
20.8
20.9
104
105
70-131
1
1,1,2-Trichloroethane
ug/L
ND
20
20
21.2
21.6
106
108
70-136
2
1,1-Dichloroethane
ug/L
ND
20
20
22.2
22.1
111
110
70-147
0
1,1-Dichloroethene
ug/L
ND
20
20
23.7
24.2
118
121
70-158
2
1,2,3-Trichloropropane
ug/L
ND
20
20
20.1
20.3
100
102
67-137
1
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
20.0
21.9
100
109
69-136
9
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.3
21.6
107
108
70-137
1
1,2-Dichlorobenzene
ug/L
ND
20
20
21.0
21.3
105
107
70-133
1
1,2-Dichloroethane
ug/L
ND
20
20
20.8
20.9
104
104
67-138
0
1,2-Dichloropropane
ug/L
ND
20
20
22.0
21.6
110
108
70-138
2
1,4-Dichlorobenzene
ug/L
ND
20
20
21.4
21.9
107
109
70-133
2
2-Butanone (MEK)
ug/L
ND
40
40
38.5
41.3
96
103
61-147
7
2-Hexanone
ug/L
ND
40
40
37.7
39.0
94
98
67-139
4
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
37.7
39.9
94
100
67-136
6
Acetone
ug/L
ND
40
40
38.4
41.8
96
105
55-159
9
Acrylonitrile
ug/L
ND
100
100
101
105
101
105
68-140
4
Benzene
ug/L
ND
20
20
21.7
22.3
108
111
67-150
3
Bromochloromethane
ug/L
ND
20
20
22.6
22.8
113
114
70-146
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC.
Page 42 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3376617
3376618
MS
MSD
92557975014
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Bromodichloromethane
ug/L
ND
20
20
21.3
21.7
106
108
70-138
2
Bromoform
ug/L
ND
20
20
19.8
20.2
99
101
57-138
2
Bromomethane
ug/L
ND
20
20
25.5
26.2
127
131
10-200
3
Carbon disulfide
ug/L
ND
20
20
21.9
22.7
109
113
70-152
4
Carbon tetrachloride
ug/L
ND
20
20
23.1
23.0
116
115
70-147
0
Chlorobenzene
ug/L
ND
20
20
22.3
22.2
111
111
70-137
0
Chloroethane
ug/L
ND
20
20
24.5
24.9
122
125
51-166
2
Chloroform
ug/L
ND
20
20
21.3
21.5
107
108
70-144
1
Chloromethane
ug/L
ND
20
20
17.0
17.2
85
86
24-161
1
cis-1,2-Dichloroethene
ug/L
ND
20
20
21.7
22.2
108
111
67-148
2
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.0
20.6
105
103
70-142
2
Dibromochloromethane
ug/L
ND
20
20
21.0
21.4
105
107
68-138
2
Dibromomethane
ug/L
ND
20
20
21.8
22.3
109
111
70-134
2
Ethylbenzene
ug/L
ND
20
20
21.9
22.1
110
110
68-143
1
lodomethane
ug/L
ND
40
40
57.6
57.2
144
143
20-161
1 v1
Methylene Chloride
ug/L
ND
20
20
20.7
20.7
103
103
64-148
0
Styrene
ug/L
ND
20
20
21.4
21.4
107
107
70-136
0
Tetrachloroethene
ug/L
ND
20
20
21.4
22.4
107
112
70-139
4
Toluene
ug/L
ND
20
20
22.1
22.2
110
111
47-157
1
trans-1,2-Dichloroethene
ug/L
ND
20
20
22.2
21.9
111
110
70-149
2
trans- 1,3-Dichloropropene
ug/L
ND
20
20
20.2
20.3
101
101
70-138
0
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
20.0
20.4
100
102
31-145
2
Trichloroethene
ug/L
ND
20
20
22.0
22.9
110
115
70-149
4
Trichlorofluoromethane
ug/L
ND
20
20
23.2
23.5
116
118
61-154
1
Vinyl acetate
ug/L
ND
40
40
35.7
37.1
89
93
48-156
4
Vinyl chloride
ug/L
ND
20
20
22.2
22.1
111
111
55-172
0
Xylene (Total)
ug/L
ND
60
60
65.2
65.3
109
109
66-145
0
1,2-Dichloroethane-d4 (S)
%
96
97
70-130
4-Bromofluorobenzene (S)
%
98
97
70-130
Toluene-d8(S)
%
99
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC.
Page 43 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
QC Batch: 641871 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92556832006, 92556832007, 92556832009, 92556832010
METHOD BLANK: 3368639
Matrix:
Water
Associated Lab Samples:
92556832006, 92556832007, 92556832009, 92556832010
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
08/20/21 10:42
1,2-Dichloroethane-d4 (S)
%
102
70-130
08/20/21 10:42
Toluene-d8 (S)
%
93
66-133
08/20/21 10:42
LABORATORY CONTROL SAMPLE: 3368640
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 17.3 86 70-130
1,2-Dichloroethane-d4 (S) % 102 70-130
Toluene-d8(S) % 94 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3368641
3368642
MS
MSD
92556487001 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 17.2
17.5 86
88
64-141 1
1,2-Dichloroethane-d4 (S)
%
100
101
70-130
Toluene-d8(S)
%
91
88
66-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
QC Batch: 641872 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92556832001, 92556832002, 92556832003, 92556832008, 92556832011
METHOD BLANK: 3368643
Matrix:
Water
Associated Lab Samples:
92556832001, 92556832002, 92556832003, 92556832008, 92556832011
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
08/20/21 10:45
1,2-Dichloroethane-d4 (S)
%
99
70-130
08/20/21 10:45
Toluene-d8 (S)
%
96
66-133
08/20/21 10:45
LABORATORY CONTROL SAMPLE: 3368644
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 19.7 99 70-130
1,2-Dichloroethane-d4 (S) % 96 70-130
Toluene-d8 (S) % 96 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3368645
3368646
MS
MSD
92556603001 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 21.9
21.2 107
104
64-141 3
1,2-Dichloroethane-d4 (S)
%
99
101
70-130
Toluene-d8(S)
%
97
97
66-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
QC Batch: 642553 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92556832004
METHOD BLANK: 3372112
Matrix:
Water
Associated Lab Samples: 92556832004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
08/24/21 13:39
1,2-Dichloroethane-d4 (S)
%
102
70-130
08/24/21 13:39
Toluene-d8 (S)
%
93
66-133
08/24/21 13:39
LABORATORY CONTROL SAMPLE: 3372113
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 17.9 90 70-130
1,2-Dichloroethane-d4 (S) % 103 70-130
Toluene-d8 (S) % 92 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3372114
3372115
MS
MSD
92557097001 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L 6.1 20
20 24.1
23.7 90
88
64-141 2
1,2-Dichloroethane-d4 (S)
%
95
94
70-130
Toluene-d8(S)
%
90
93
66-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
QC Batch: 643279 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92556832005
METHOD BLANK: 3375476
Matrix:
Water
Associated Lab Samples: 92556832005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
08/26/21 12:17
1,2-Dichloroethane-d4 (S)
%
96
70-130
08/26/21 12:17
Toluene-d8 (S)
%
102
66-133
08/26/21 12:17
LABORATORY CONTROL SAMPLE: 3375477
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 20.6 103 70-130
1,2-Dichloroethane-d4 (S) % 97 70-130
Toluene-d8(S) % 102 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3375478
3375479
MS
MSD
92556832005 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 5.2 20
20 27.0
27.3 109
110
64-141 1
1,2-Dichloroethane-d4 (S)
%
100
97
70-130
Toluene-d8(S)
%
101
102
66-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
QC Batch: 643833 Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92556832003, 92556832004
METHOD BLANK: 3377949
Matrix:
Water
Associated Lab Samples: 92556832003, 92556832004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Alkalinity, Total as CaCO3
ug/L
ND
5000
08/30/21 22:08
LABORATORY CONTROL SAMPLE:
3377950
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Alkalinity, Total as CaCO3
ug/L
50000
50000
100 80-120
LABORATORY CONTROL SAMPLE: 3377951
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Alkalinity, Total as CaCO3 ug/L 50000 52800 106 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3377952 3377953
MS MSD
92557682017 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 ug/L 146 50000 50000 194000 201000 96 110 80-120 4
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3377954 3377955
MS MSD
92556487003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 ug/L 179000 50000 50000 235000 237000 110 116 80-120 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC.
Page 48 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Butner Landfill Compliance
Pace Project No.: 92556832
QC Batch: 642990
QC Batch Method: EPA 300.0 Rev 2.1 1993
Associated Lab Samples: 92556832003, 92556832004
METHOD BLANK: 3374032
Associated Lab Samples: 92556832003, 92556832004
Parameter Units
Sulfate ug/L
LABORATORY CONTROL SAMPLE: 3374033
Parameter Units
Sulfate ug/L
QUALITY CONTROL DATA
Analysis Method: EPA 300.0 Rev 2.1 1993
Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services -Asheville
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1000 08/26/21 00:53
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
50000 48400 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3374034 3374035
MS MSD
92557349005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate ug/L 1040 50000 50000 1040000 1090000 -16 89 90-110 5 M1
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3374036 3374037
MS MSD
92555945011 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate ug/L 219 50000 50000 321000 254000 204 68 90-110 24 M1,R1
mg/L
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC.
Page 49 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
QC Batch: 644613 Analysis Method: SM 4500-CI-E-2011
QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92556832003, 92556832004
METHOD BLANK: 3381960
Matrix:
Water
Associated Lab Samples: 92556832003, 92556832004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Chloride
mg/L
ND
1.0
09/02/2111:04
LABORATORY CONTROL SAMPLE:
3381961
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Chloride
mg/L
20
20.4
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3381962 3381963
MS MSD
92557313001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L 18.9 10 10 29.4 29.3 105 104 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3381964 3381965
MS MSD
92557313003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L 19.0 10 10 29.0 28.8 100 98 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC.
Page 50 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
QC Batch: 644349 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92556832003
METHOD BLANK: 3380766
Associated Lab Samples: 92556832003
Parameter Units
Chemical Oxygen Demand ug/L
LABORATORY CONTROL SAMPLE: 3380767
Parameter Units
Chemical Oxygen Demand ug/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25000 09/01 /21 05:18
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
750000 754000 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3380768 3380769
MS MSD
92556543001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand ug/L 31.8 100000 100000 125000 127000 93 96 90-110 2
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3380770 3380771
MS MSD
92556556001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand ug/L 31.8 100000 100000 141000 139000 110 107 90-110 2
mg/L
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC.
Page 51 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Butner Landfill Compliance
Pace Project No.: 92556832
QC Batch: 644686 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92556832004
METHOD BLANK: 3382287
Associated Lab Samples: 92556832004
Parameter Units
Chemical Oxygen Demand ug/L
LABORATORY CONTROL SAMPLE: 3382288
Parameter Units
Chemical Oxygen Demand ug/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25000 09/02/2106:07
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
750000 794000 106 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3382291 3382292
MS MSD
92557864001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand ug/L 12900 100000 100000 1320000 1290000 359 0 90-110 3 M1
mg/L 0 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3382320 3382321
MS MSD
92556832004 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand ug/L 121000 100000 100000 228000 224000 108 103 90-110 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC.
Page 52 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Butner Landfill Compliance
Pace Project No.: 92556832
QC Batch: 642316
QC Batch Method: SM 531OB-2011
Associated Lab Samples: 92556832003, 92556832004
METHOD BLANK: 3371123
Associated Lab Samples: 92556832003, 92556832004
Parameter Units
Total Organic Carbon ug/L
LABORATORY CONTROL SAMPLE: 3371124
Parameter Units
Total Organic Carbon ug/L
QUALITY CONTROL DATA
Analysis Method: SM 531 OB-2011
Analysis Description: 5310E TOC
Laboratory: Pace Analytical Services -Asheville
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1000 08/23/21 19:07
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
25000 23400 94 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3371125 3371126
MS MSD
92555701001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon ug/L 19.8 25000 25000 43400 43300 94 94 90-110 0
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3371127 3371128
MS MSD
92555701002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon ug/L 19.2 25000 25000 42900 43300 95 97 90-110 1
mg/L
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC.
Page 53 of 62

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: Butner Landfill Compliance
Pace Project No.: 92556832
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
B2 Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 54 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Butner Landfill Compliance
Pace Project No.: 92556832
Lab ID
92556832003
92556832004
92556832003
92556832004
92556832003
92556832004
92556832001
92556832002
92556832003
92556832004
92556832005
92556832006
92556832007
92556832008
92556832009
92556832010
92556832001
92556832002
92556832003
92556832004
92556832005
92556832006
92556832007
92556832008
92556832009
92556832010
92556832001
92556832002
92556832003
92556832004
92556832005
92556832006
92556832007
92556832008
92556832009
92556832010
92556832011
92556832001
92556832002
92556832003
92556832004
92556832005
92556832006
Sample ID
3902-MW3R
3902-MW2R
3902-MW3R
3902-MW2R
3902-MW3R
3902-MW2R
3902-MW1 R
3902-MW4
3902-MW3R
3902-MW2R
3902-MW5
3902-MW6
3902-N ES1
3902-Field Blank
3902-SW1
3902-SW2
3902-MW1 R
3902-MW4
3902-MW3R
3902-MW2R
3902-MW5
3902-MW6
3902-N ES1
3902-Field Blank
3902-SW1
3902-SW2
3902-MW1 R
3902-MW4
3902-MW3R
3902-MW2R
3902-MW5
3902-MW6
3902-NES1
3902-Field Blank
3902-SW1
3902-SW2
3902-Trip Blank
3902-MW1 R
3902-MW4
3902-MW3R
rI Iwzz� kyffmN
3902-MW5
3902-MW6
Date: 09/13/2021 01:03 PM
QC Batch Method
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
SM 5210B-2011
SM 5210B-2011
RSK 175 Modified
RSK 175 Modified
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 8260D
EPA 8260D
EPA 8260D
EPA 8260D
EPA 8260D
EPA 8260D
EPA 8260D
EPA 8260D
EPA 8260D
EPA 8260D
EPA 8260D
EPA 8260D Mod.
EPA 8260D Mod.
EPA 8260D Mod.
EPA 8260D Mod
EPA 8260D Mod
EPA 8260D Mod
QC Batch Analytical Method
642036
642036
642092
642092
642636
642636
644216
644216
644216
644216
644216
644216
644216
644216
644216
644216
644733
644733
644733
644733
644733
644733
644743
644743
644743
644743
642049
642049
642049
642049
643524
642049
642049
642049
642049
642049
642049
641872
641872
641872
642553
643279
641871
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
SM 5210B-2011
SM 5210B-2011
EPA6010D
EPA6010D
EPA6010D
EPA6010D
EPA6010D
EPA6010D
EPA6010D
EPA6010D
EPA6010D
EPA6010D
EPA 6020B
EPA 6020B
EPA 6020B
EPA 6020B
EPA 6020B
EPA 6020B
EPA 6020B
EPA 6020B
EPA 6020B
EPA 6020B
Analytical
Batch
642097
642097
644578
644578
644578
644578
644578
644578
644578
644578
644578
644578
645553
645553
645553
645553
645553
645553
644912
644912
644912
644912
Page 55 of 62

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Butner Landfill Compliance
92556832
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92556832007
3902-NES1
EPA 8260D Mod.
641871
92556832008
3902-Field Blank
EPA 8260D Mod.
641872
92556832009
3902-SW1
EPA 8260D Mod.
641871
92556832010
3902-SW2
EPA 8260D Mod.
641871
92556832011
3902-Trip Blank
EPA 8260D Mod.
641872
92556832003
3902-MW3R
SM 2320B-2011
643833
92556832004
3902-MW2R
SM 2320B-2011
643833
92556832003
3902-MW3R
EPA 300.0 Rev 2.1 1993
642990
92556832004
3902-MW2R
EPA 300.0 Rev 2.1 1993
642990
92556832003
3902-MW3R
SM 4500-CI-E-2011
644613
92556832004
3902-MW2R
SM 4500-CI-E-2011
644613
92556832003
3902-MW3R
SM 5220D-2011
644349
SM 5220D-2011
644361
92556832004
3902-MW2R
SM 5220D-2011
644686
SM 5220D-2011
644704
92556832003
3902-MW3R
SM 5310B-2011
642316
92556832004
3902-MW2R
SM 5310B-2011
642316
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/13/2021 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 56 of 62

Document Name:
Document Revised: October 28, 2020
aceAnalytical ^
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
F-CAR-CS-033-Rev.07
issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ HuntersvllleQ/ Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersvillerl
Sample Condition Client Name:
Upon Receipt Project #:
Courier: ❑Fed Ex ❑UPS — ❑USPS ❑Client
❑ Commercial q ce [I]Other:
Custody Seal Present? [-]Yes Q#o seals Intact? Oyes ❑Afe�
Wo# : 92556832
11111111111111
32
Date/initials Person Examining Contents: I�/L I
Packing Material: ❑Bubble Wrapble Bags ❑None ❑ Other Blolagical Tissue F oxen?
Thermometer: Eyes ❑No �/A
a4 r ,,� rn• r � -r cr r1 r _ic q1et ❑Blue ❑None
ype OT ice:
II Correction Factor;
Cooler Temp: 1 ' l Add/Subtract ('Q Temp should be above freezing to G°C
[]Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected {'C,�! l has begun
USDA Regulated Soil 7 N/A, water sample)
Did fs-amples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)7 Did samples originate from a foreign source (internationally,
-7
I Ym f-INn i—I... 7i— W--ii —A G..n M-11 mv— nrin
Comments/Discrepancy:
Chain of Custody Present?
` _/
y--dY//es
No
NIA
1.
Sam les Arrived within Hold Time?
'Ekes
❑No
❑N/A
2.
Short -Hold Time Analysis <72 hr.)?
'Yes
ONO
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
E3J/O
❑N/A
4.
Sufficient Volume?
es
El No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
' Yes
Q41
[IN.,
❑No
❑N/A
❑N/A
6.
Containers Intact?
❑Yes
a,
❑N/A
7. _
(bv tA/(j7ln�
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
'EXIA
S.
Sample Labels Match COC7 N\fD W2JDJZ1 .--,EJrns
-Includes Date/Time/ID/Analysis Matrix:
V&
❑N/A
9. Qi�
Covv�lMft v��t
Headspace in VOA Vials (>5-limm)?
Yes
��//
'MNo
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
e$
es
ONO
ONO
❑N/A
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY
Field Data Required? ❑Yes ❑No
1_�g�U W ; �,�1i�� S w -Z otrr'.►rer� �,,f et�.>`i._aG�
2 CS J1 �,-TS77YV� il'YAty1 '�r (Oe►- nvy� ' �O2-AAW4-- -t 11 1 I\AW 7-V
C
Lot ID of split containers:
CLIENT
-Pe
Project Manager SCURF Review: Hate:
Project Manager SRF Review:
Date:
Page 57 of 62

Document Name:
Document Revised: October 28, 2020
e
ceAnalytical
Sample Condition Upon RecelptiSCUR)
Page 2 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.07
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination Is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, ORO/8015 (water) DOC, LLHS
**Bottom half of box is to list number of bottles
Project a wog : 92556832
PM: AMB Due Data: 09/02/21
CLIENT: 92—Garratt
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Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot p
Noie:-W h e neve rt here-is-a-discre pe n cy-affecti ng-No rth-C-aro lina- corn p li a nee-s a mples,-a-eopy-of-this-form-wi I Lbe-sent-t e-the-No r-th-Carolina-QSH NR-C orti Flcation-Off ice-ii.e
Out of hold, Incorrect preservative, out of temp, incorrect containers.
Page 58 of 62

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Q Page 59 of 62
.a .s.

Document Name: Document Revised: October 29, 2020
Sample Condition Upon Receipt(SCUR) Page S of 2
aceAnaly idal Document No,: Issuing Authority:
F-CAR-CS-033-Rev.07 Pace Carolinas Quality Office
Laboratory rece ng samples:
KEden❑ ❑ Huntersville ❑ Raleigh❑
Mechanicsville❑ Atlanta❑ Kernersville❑
Asheville Greenwood
WO# : 92556832
SaryiplL.condition Client name:
Up on ReceiptProjectg: pM; AMB Due Date: 09/02/21
:2- CC Tr
Courier: ❑Fed Ex ❑UPS ❑USPS ❑Client
CLIENT: 92-Garrett
19 Cornmercia( ace ❑Other:
L
Custody Seal Present? ❑Yes J2V—b Seals Intact? ❑Yes 1_4;N0
Date/initials Person Exansining Cantents:_ ` r
1
Packing Material: 21r.bble Wrap ❑Bubble Bags []None ❑ Other
Biological Tissue Frozen?
❑Yes ❑No ❑N/A
H� et ❑slue
Thermornete 431171
IR Gun fD: l 13�j 7 Type of Ice:
❑NonTe
Correction Factor:
Cooler Temp: 3 - y Add/Subtract ('C) �
Temp should he above freezing to 6"C
❑Samples out of temp critzna. Saissples an ice, cooling Process
CoelerTemp Corrected ('C): 3 .c.)
nasbcgun
USDA Regulated Soil ( A, water sample)
Did samples originate i aqua rantine zone within the United States: CA, NY, or SC (check maps)?
Did samples originate from a foreign source (internationally.
❑No
❑Yes ❑Na
indudingHawaii and Puerto Rica)? []Yes
Comm ents/Discrepancy:
Chain of Custody Present?
Sarnoles Arrived within Hold Time?
Short Hold Time Analysis (02 hr.]?
Rush Turn Around Time Requested?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis: Samples Field Filtered?
Sample labels Match COC?
-Includes Date%Time/ID/Analysis Matrix
Headspace in VOA Vials (>5-6mm)?
Trip Blank Present?
Trip Blank Custody Seals Present?
COMMENTS/SAMPLES �DISCREPANCY
CLIENT NOTIHCATION/ RESOLUTION
Person contacted:
Project iYlanager SCURF Review:
Project Manager SRF Review:
R'rrs
❑PIo
❑N/A
1-
es
❑Plo
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❑N/A
S.
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❑P!/A
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❑N-
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❑Yes❑
No
NIA
g•
❑NIA
No
9.❑es
❑Peso
❑NJA
10.
❑Yes ❑PIo 1/A
bate/Time:
Lot 10 or split containers;
Date:
Date:
Field Data Required? ❑Yes ❑NO
Page 60 of 62

*Check mark top half of box if pH and/or dechiorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 iwater) DOC, LLHS
"Bottom half of box Is to list number of bottles
Document Name: Document Revised: October 28, 2020
Sample Condition Upon Receipt(SCUR) Page 2 of 2
cICC�ilFc3�JItICr7i+6 Document No.: Issuing Authority;
F-CAR-CS-033-Rev.07 Pace Carolinas Quality Office
92556832
Project # WO#
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Page 62 of 62
i
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Appendix C
Historic Groundwater Elevations
(from LaBella, 2021)

APPENDIX C
HISTORICAL GROUNDWATER ELEVATIONS
Well ID:
Background
Downgradient
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Well TOC Elev.:
460.51
331.60
330.96
340.80
343.88
362.53
328.40
Well Depth:
56.00
18.85
35.83
31.43
23.52
32.63
32.80
8/21/99
418.68
329.13
328.06
330.50
330.83
352.10
NI
11/16/99
419.75
325.38
324.51
331.53
334.33
352.97
NI
5/10/00
424.53
329.60
328.83
334.15
334.49
355.72
NI
10/26/00
419.21
329.26
328.15
331.33
330.94
352.78
NI
4/18/01
418.76
329.42
328.63
333.57
334.36
354.22
NI
10/26/01
412.53
329.04
327.94
330.57
330.23
350.92
NI
6/13/02
413.70
328.38
327.41
330.21
330.29
351.04
NI
11/19/02
413.40
329.25
328.35
331.57
337.17
350.94
NI
06/27/03
423.61
329.57
328.93
334.24
333.99
355.21
NI
12/29/03
420.23
329.70
329.11
334.49
334.78
354.92
NI
06/30/04
418.81
329.38
328.48
332.26
331.39
353.10
NI
12/28/04
418.02
329.50
328.91
333.45
334.14
355.14
NI
06/29/05
418.81
329.10
329.26
331.62
330.90
352.76
NI
12/29/05
413.38
329.29
328.71
332.78
334.27
351.52
NI
06/27/06
414.75
329.17
328.40
332.18
333.56
353.43
NI
12/28/06
415.54
329.40
328.86
333.57
335.24
354.02
NI
07/12/07
438.64
328.69
327.97
331.31
330.52
352.30
NI
12/18/07
412.59
328.94
328.08
330.32
327.92
347.90
306.54
07/08/08
414.52
329.20
326.00
331.46
330.85
351.03
NM
12/17/08
412.79
329.39
328.84
333.15
335.03
350.82
NM
07/09/09
417.16
329.17
329.48
332.30
331.36
352.17
310.12
12/16/29
418.11
329.55
329.09
334.57
336.94
352.87
NM
06/24/10
422.42
329.41
328.77
333.65
333.15
353.62
NM
12/13/10
415.96
329.49
328.85
332.81
330.34
350.08
NM
06/20/11
416.00
328.95
328.18
336.77
331.38
351.83
NM
12/05/11
412.94
329.31
328.65
332.32
329.51
349.87
NM
06/12/11
414.56
329.10
328.35
332.52
331.33
351.75
312.50
12/12/12
412.83
329.19
328.36
331.67
330.35
349.48
NM
05/01/13
415.69
329.65
329.13
334.49
335.15
353.63
317.11
08/05/13
417.97
329.02
328.41
333.32
332.83
353.01
NM
02/24/14
415.81
329.68
329.17
334.48
331.63
351.78
316.15
08/11/14
416.23
329.38
328.48
332.04
329.08
350.08
310.93
03/10/15
417.09
329.87
329.45
335.07
336.42
353.13
317.55
08/17/15
417.71
328.65
327.81
331.05
327.73
347.63
308.80
02/17/16
418.51
330.10
329.71
335.05
337.53
353.44
317.87
08/09/16
418.59
329.50
328.61
332.95
330.95
352.03
312.65
02/13/17
415.21
329.45
328.96
333.10
333.03
350.83
313.45
08/22/17
414.68
328.55
327.61
331.60
329.78
350.38
310.55
02/05/18
412.31
329.41
328.21
332.07
328.87
348.18
317.10
08/14/18
415.86
328.96
327.96
331.97
329.68
350.12
312.51
02/04/19
420.86
329.67
329.28
335.62
335.42
355.30
316.02
08/06/19
420.05
329.35
328.37
332.98
329.73
351.46
310.34
02/12/20
417.43
329.75
329.30
335.65
336.08
352.38
317.67
08/27/20
418.84
329.18
328.55
333.42
330.48
351.34
310.90
02/11/21
421.71
329.93
329.62
336.59
336.17
355.52
318.10
08/19/21
420.22
329.50
328.71
333.67
330.13
351.84
310.29

Appendix D
Historical Constituents in Groundwater
(from LaBella, 2021)

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
INORGANICS
Antimony
8-Sep-94
---
30
ND
ND
ND
ND
ND
ND
---
---
1-Dec-94
---
30
ND
ND
ND
ND
ND
ND
---
---
9-Feb-95
---
30
ND
ND
ND
ND
ND
ND
---
---
2-M a r-95
---
30
ND
ND
ND
ND
ND
ND
---
---
15-Nov-95
---
30
ND
ND
ND
ND
ND
ND
---
---
28-May-96
---
30
ND
ND
ND
ND
ND
ND
---
---
22-Nov-96
---
30
ND
ND
ND
ND
ND
ND
---
---
17-Jun-97
---
30
ND
ND
ND
ND
ND
ND
---
---
1-Dec-97
---
30
ND
ND
ND
ND
ND
ND
---
---
20-May-98
---
30
ND
ND
ND
ND
ND
ND
---
---
19-N ov-98
---
30
ND
ND
ND
ND
ND
ND
---
---
21-J u 1-99
---
30
ND
ND
ND
ND
ND
ND
---
---
16-N ov-99
---
30
ND
ND
ND
ND
ND
ND
---
---
10-May-00
---
30
ND
80.0
38.0
32.0
33.0
31.0
---
---
26-Oct-00
---
30
30.0
ND
ND
ND
ND
ND
---
---
18-A p r-01
---
30
ND
ND
ND
ND
ND
ND
---
---
27-Oct-01
---
30
ND
ND
ND
ND
ND
ND
---
---
13-Jun-02
---
30
ND
ND
ND
ND
ND
ND
---
---
19-N ov-02
---
30
ND
ND
ND
ND
ND
ND
---
---
27-Jun-03
---
30
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
30
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
30
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
30
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
30
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
30
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
30
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
6
ND
ND
ND
ND
ND
ND
---
ND
12-Jul-07
---
6
ND
ND
ND
ND
ND
ND
---
ND
IMAC = 1.4 pg/L (10/23/07)
19-Dec-07
---
6
ND
ND
ND
ND
ND
ND
ND
ND
8-Ju1-08
---
6
ND
ND
ND
ND
ND
ND
---
ND
17-Dec-08
2.6
6.0
ND
ND
ND
ND
ND
ND
---
ND
9-Jul-09
2.6
6.0
ND
ND
ND
ND
ND
ND
ND
ND
16-Dec-09
2.6
6.0
ND
ND
ND
ND
ND
ND
---
ND
24-Jun-10
2.6
6.0
ND
ND
ND
2.9 J
ND
ND
---
ND
IMAC = 1 pg/L (8/1/10)
13-Dec-10
2.6
6.0
ND
ND
3.0 J
ND
2.8 J
ND
---
ND
20-Jun-11
5.0
6.0
ND
ND
ND
ND
6.0
ND
---
ND
5-Dec-11
5.0
6.0
ND
ND
ND
ND
ND
ND
---
ND
11-Jun-12
5.0
6.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
5.0
6.0
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
5.0
6.0
ND
ND
ND
ND
ND
ND
ND
ND
5-Aug-13
5.0
6.0
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
5.0
6.0
8.8
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
5.0
6.0
ND
10.5
8.0
ND
ND
ND
---
ND
10-Mar-15
3.8
6.0
ND
7.1
6.5
3.9 J
ND
ND
---
ND
18-Aug-15
3.8
6.0
ND
6.2
4.8 J
4.1 J
ND
ND
---
ND
16-Feb-16
3.8
6.0
ND
9.9
6.5
4.3 J
ND
ND
---
ND
9-Aug-16
3.8
6.0
ND
7.7
ND
ND
ND
ND
---
ND
13-Feb-17
3.9
6.0
ND
ND
ND
ND
ND
ND
---
ND
22-Aug-17
3.9
6.0
ND
ND
ND
ND
ND
ND
---
ND
5-Feb-18
3.9
6.0
ND
ND
ND
ND
ND
ND
---
ND
13-Aug-18
3.9
6.0
ND
ND
ND
ND
ND
ND
---
ND
4-Feb-19
3.9
5.0
ND
ND
ND
ND
ND
ND
---
ND
7-Aug-19
3.0
5.0
ND
ND
ND
ND
ND
ND
---
ND
12-Feb-20
3.0
5.0
ND
ND
ND
ND
ND
ND
---
ND
27-Aug-20
3.0
5.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
3.0
5.0
ND
ND
ND
ND
ND
ND
---
ND
Arsenic
8-Sep-94
---
10
ND
ND
ND
ND
ND
ND
---
---
1-Dec-94
---
10
ND
ND
ND
ND
ND
ND
---
---
9-Feb-95
---
10
ND
ND
ND
ND
ND
ND
---
---
2-M a r-95
---
10
ND
ND
ND
ND
ND
ND
---
---
15-N ov-95
---
10
ND
ND
ND
ND
ND
ND
---
---
28-May-96
---
10
ND
ND
ND
ND
ND
ND
---
---
22-Nov-96
---
10
ND
ND
ND
ND
ND
ND
---
---
17-J u n-97
---
10
6.0 J
15.0
ND
ND
ND
ND
---
---
1-Dec-97
---
10
ND
5.0 J
ND
ND
ND
ND
---
---
20-May-98
---
10
ND
ND
ND
ND
ND
ND
---
---
19-N ov-98
---
10
ND
ND
ND
ND
ND
ND
---
---
21-J u 1-99
---
10
N D
N D
N D
N D
N D
N D
---
---
16-N ov-99
---
10
N D
N D
N D
N D
N D
N D
---
---
10-May-00
---
10
N D
N D
N D
N D
N D
N D
---
---
26-Oct-00
---
10
N D
N D
N D
N D
N D
N D
---
---
18-Apr-01
---
10
N D
N D
N D
N D
N D
N D
---
---
27-Oct-01
---
10
N D
N D
N D
N D
N D
N D
---
---
13-Jun-02
---
10
ND
ND
ND
ND
ND
ND
---
---
19-N ov-02
---
10
N D
N D
N D
N D
N D
N D
---
---
27-Jun-03
---
10
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
10
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
10
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
10
2.0 J
ND
ND
ND
ND
ND
---
ND
12-Jul-07
---
10
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = 50 pg/L (10/23/07)
19-Dec-07
---
10
ND
4.1 J
ND
ND
ND
ND
ND
ND
8-Ju1-08
---
10
ND
4.9 J
ND
ND
ND
ND
---
ND
17-Dec-08
2.7
10.0
ND
ND
ND
ND
ND
ND
---
ND
9-Jul-09
2.7
10.0
ND
13.5
10.9
5.6 J
ND
4.0 J
ND
ND
16-Dec-09
2.7
10.0
ND
10.6
6.4 J
5.0 J
ND
3.6 J
---
ND
NC 2L = 10 pg/L (02/05/10)
24-Jun-10
2.7
10.0
ND
11.8
8.1 J
8.2 J
3.3 J
3.1 J
---
ND
Resample >
12-Aug-10
2.7
10.0
---
---
7.2 J
---
---
---
---
ND
Resample >
31-Aug-10
2.7
10.0
---
15.4
---
---
---
---
---
ND
13-Dec-10
2.7
10.0
ND
4.9 J
2.7 J
5.4 J
ND
ND
---
ND
20-Jun-11
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
11-Jun-12
5.0
10.0
ND
5.4 J
ND
ND
ND
ND
ND
ND
12-Dec-12
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
5.0
10.0
ND
ND
ND
ND
ND
ND
ND
ND
5-Aug-13
5.0
10.0
ND
ND
5.6 J
ND
ND
ND
---
ND
24-Feb-14
5.0
10.0
ND
6.4 J
ND
ND
ND
ND
ND
ND
12-Aug-14
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
10-Mar-15
2.5
10.0
4.1 J
5.4 J
ND
ND
3.1 J
3.2 J
---
3.0 J
18-Aug-15
2.5
10.0
ND
5.1 J
ND
ND
ND
ND
---
ND
16-Feb-16
2.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
9-Aug-16
2.5
10.0
ND
ND
ND
ND
ND
ND
---
5.1 J
13-Feb-17
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
22-Aug-17
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Feb-18
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
13-Aug-18
5.0
10.0
ND
5.4 J
ND
ND
ND
ND
---
ND
4-Feb-19
5.0
10.0
ND
5.7 J
ND
ND
ND
ND
---
ND
7-Aug-19
4.7
10.0
ND
ND
ND
ND
ND
ND
---
ND
12-Feb-20
4.7
10.0
ND
ND
ND
ND
ND
ND
---
ND
27-Aug-20
4.7
10.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
4.7
10.0
4.9 J
10.0 J
ND
ND
ND
ND
---
ND

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
Barium
8-Sep-94
---
500
ND
270
ND
ND
830
860
---
---
1-Dec-94
---
500
ND
ND
ND
N D
ND
ND
---
---
9-Feb-95
---
500
ND
ND
ND
ND
510
ND
---
---
2-Mar-95
---
500
ND
ND
ND
ND
ND
ND
---
---
15-Nov-95
---
500
ND
ND
ND
ND
ND
ND
---
---
28-May-96
---
500
ND
ND
ND
ND
ND
ND
---
---
22-Nov-96
---
500
ND
82.0
30.0
ND
15.0
ND
---
---
17-Jun-97
---
500
200
320
37.0
17.0
210
31.0
---
---
1-Dec-97
---
500
61.0
180
43.0
46.0
220
33.0
---
---
20-May-98
---
500
30.0
150
45.0
13.0
180
22.0
---
---
19-Nov-98
---
500
48.0
120
42.0
ND
380
12.0
---
---
21-J u 1-99
---
500
ND
ND
ND
N D
ND
ND
---
---
16-Nov-99
---
500
ND
ND
ND
ND
ND
ND
---
---
10-May-00
---
500
ND
ND
ND
ND
ND
ND
---
---
26-Oct-00
---
500
ND
ND
ND
N D
ND
ND
---
---
18-Apr-01
---
500
ND
ND
ND
N D
ND
ND
---
---
27-Oct-01
---
500
ND
ND
ND
N D
ND
ND
---
---
13-Jun-02
---
500
ND
ND
ND
ND
ND
ND
---
---
19-N ov-02
---
500
ND
ND
ND
N D
ND
ND
---
---
27-Jun-03
---
500
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
500
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
500
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
500
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
500
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
500
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
500
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
500
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
100
5.2 J
120
64.9
1.5 J
64.1
1.8 J
---
0.20 J
12-Jul-07
---
100
2.5 J
129
65.7 J
1.1 J
77.0 J
1.3 J
---
ND
INC 2L = 2,000 pg/L (10/23/07)
19-Dec-07
---
100
2.8 B
99.2
50.0 B
1.4 B
49.6 B
1.7 B
87.8
11.7
8-J u 1-08
---
100
5.8 J
102
58.4 J
1.1 B
57.9 J
1.2 B
---
0.29 J
17-Dec-08
0.20
100
2.7 B
92.9 J
53.1 B
1.2 B
55.5 J
1.1 B
---
10.7 J
9-Jul-09
0.20
100
4.6 B
121
63.4 B
0.37 B
81.4 B
0.94 B
72.4 B
17.6 J
16-Dec-09
0.20
100
2.9 B
108
62.8 B
0.61 B
56.8 B
0.87 B
---
17.1 J
INC 2L = 700 pg/L (02/05/10)
24-Jun-10
0.20
100
2.5 B
115 B
61.1 B
1.6 B
93.5 B
1.4 B
---
27.3 J
13-Dec-10
0.20
100
4.3 B
122
67.9 J
1.3 B
90.6 J
1.5 B
---
12.1 J
20-Jun-11
5.0
100
ND
108
70.7 J
ND
84.7 J
ND
---
ND
5-Dec-11
5.0
100
ND
118
73.0 J
ND
90.6 J
ND
---
ND
11-Jun-12
5.0
100
ND
138
65.2 J
ND
76.4 J
ND
61.3 J
ND
12-Dec-12
5.0
100
ND
113
64.7 J
ND
73.6 J
ND
---
ND
1-May-13
5.0
100
ND
118
69.1 J
ND
84.2 J
ND
81.2 J
ND
5-Aug-13
5.0
100
ND
111
65.1 J
ND
95.6 J
ND
---
ND
24-Feb-14
5.0
100
ND
93.8 J
44.8 J
ND
139
ND
ND
ND
12-Aug-14
5.0
100
ND
125
66.4 J
ND
121
ND
---
ND
10-Mar-15
2.5
100
3.0 J
109
61.8 J
ND
116
ND
---
ND
18-Aug-15
2.5
100
4.4 J
119
63.1 J
ND
81.3 J
ND
---
ND
16-Feb-16
2.5
100
5.2 J
123
72.7 J
3.0 J
126
ND
---
ND
9-Aug-16
2.5
100
4.5 J
123
73.3 J
ND
109
ND
---
ND
13-Feb-17
2.5
100
7.8 J
112
68.3 J
ND
151
5.6 J
---
ND
22-Aug-17
2.5
100
ND
102
64.5 J
ND
99.9 J
ND
---
ND
5-Feb-18
2.5
100
8.0 J
117
73.5 J
ND
161
ND
---
ND
13-Aug-18
2.5
100
3.8 J
116
67.6 J
ND
103
ND
---
ND
4-Feb-19
2.5
5.0
ND
104
44.3
ND
110
ND
---
ND
7-Aug-19
1.0
5.0
5.4
113
73.8
1.2 J
95.1
1.9 J
---
ND
12-Feb-20
1.0
5.0
3.6 J
110
56.2
2.5 J
147
1.6 J
---
ND
27-Aug-20
3.5
5.0
4.5 J
127
83.2
ND
128
ND
---
ND
11-Feb-21
3.5
5.0
5.3
116
74.4
ND
161
ND
---
ND
Beryllium
8-Sep-94
---
2
ND
ND
ND
ND
ND
ND
---
---
1-Dec-94
---
2
ND
ND
ND
N D
4.0
ND
---
---
9-Feb-95
---
2
ND
ND
ND
ND
ND
ND
---
---
2-Mar-95
---
2
ND
ND
ND
ND
2.0
ND
---
---
15-N ov-95
---
2
ND
ND
ND
N D
ND
ND
---
---
28-May-96
---
2
ND
ND
ND
ND
6.0
ND
---
---
22-Nov-96
---
2
ND
ND
ND
ND
3.0
ND
---
---
17-J u n-97
---
2
2.0
3.0
ND
N D
1.0
ND
---
---
1-Dec-97
---
2
ND
ND
ND
N D
ND
ND
---
---
20-May-98
---
2
ND
ND
ND
ND
ND
ND
---
---
19-N ov-98
---
2
ND
ND
ND
N D
2.0
ND
---
---
21-J u 1-99
---
2
N D
N D
N D
N D
N D
N D
---
---
16-N ov-99
---
2
N D
N D
N D
N D
N D
N D
---
---
10-May-00
---
2
N D
N D
N D
N D
N D
N D
---
---
26-Oct-00
---
2
N D
N D
N D
N D
N D
N D
---
---
18-Apr-01
---
2
N D
12.0
N D
N D
N D
N D
---
---
27-Oct-01
---
2
N D
N D
N D
N D
N D
N D
---
---
13-Jun-02
---
2
ND
ND
ND
ND
ND
ND
---
---
19-N ov-02
---
2
N D
N D
N D
N D
N D
N D
---
---
27-Jun-03
---
2
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
2
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
2
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
2
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
2
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
2
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
2
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
2
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
1
ND
ND
ND
ND
ND
ND
---
ND
12-Jul-07
---
1
ND
ND
ND
ND
ND
ND
---
ND
IMAC = 4 pg/L (10/23/07)
19-Dec-07
---
1
ND
ND
ND
ND
ND
ND
ND
ND
8-Ju1-08
---
1
ND
ND
ND
ND
ND
ND
---
ND
17-Dec-08
0.10
1.0
ND
ND
ND
ND
0.14 J
ND
---
ND
9-Jul-09
0.10
1.0
ND
0.18 J
0.22 J
0.17 J
ND
ND
0.23 J
ND
16-Dec-09
0.10
1.0
ND
0.15 J
0.17 J
0.15 J
0.25 J
ND
---
ND
24-Jun-10
0.10
1.0
ND
ND
0.27 J
0.16 J
ND
ND
---
ND
13-Dec-10
0.10
1.0
ND
ND
ND
ND
ND
ND
---
ND
20-Jun-11
1.0
1.0
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
1.0
1.0
ND
ND
ND
ND
ND
ND
---
ND
11-Jun-12
1.0
1.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
1.0
1.0
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
1.0
1.0
ND
ND
ND
ND
ND
ND
ND
ND
5-Aug-13
1.0
1.0
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
1.0
1.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
1.0
1.0
ND
ND
ND
ND
ND
ND
---
ND
10-Mar-15
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
18-Aug-15
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
16-Feb-16
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
9-Aug-16
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
13-Feb-17
0.50
1.0
ND
ND
ND
ND
0.57 J
ND
---
ND
22-Aug-17
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
5-Feb-18
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
13-Aug-18
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
4-Feb-19
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
7-Aug-19
0.20
1.0
ND
ND
ND
ND
ND
ND
---
ND
12-Feb-20
0.20
1.0
0.27 J
ND
ND
ND
ND
0.21 J
---
ND
27-Aug-20
0.70
1.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
0.70
1.0
ND
ND
ND
ND
ND
ND
---
ND

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
Cadmium
8-Sep-94
---
1
ND
ND
ND
ND
ND
4.0
---
---
1-Dec-94
---
1
ND
ND
ND
ND
ND
ND
---
---
9-Feb-95
---
1
ND
ND
ND
ND
ND
ND
---
---
2-M a r-95
---
1
ND
ND
ND
ND
ND
ND
---
---
15-N ov-95
---
1
ND
ND
ND
ND
ND
ND
---
---
28-May-96
---
1
ND
ND
ND
ND
ND
ND
---
---
22-Nov-96
---
1
ND
ND
ND
ND
ND
ND
---
---
17-J u n-97
---
1
ND
3.0
1.0
ND
ND
ND
---
---
1-Dec-97
---
1
ND
2.0
ND
ND
ND
ND
---
---
20-May-98
---
1
ND
ND
ND
ND
ND
ND
---
---
19-N ov-98
---
1
ND
ND
ND
ND
ND
ND
---
---
21-J u 1-99
---
1
ND
ND
ND
ND
ND
ND
---
---
16-N ov-99
---
1
ND
3.0
3.0
ND
2.0
ND
---
---
10-May-00
---
1
5.0
ND
ND
ND
ND
ND
---
---
26-Oct-00
---
1
ND
2.0
ND
ND
ND
ND
---
---
18-A p r-01
---
1
ND
11.0
ND
ND
ND
ND
---
---
27-Oct-01
---
1
ND
ND
ND
ND
ND
ND
---
---
13-J u n-02
---
1
ND
2.0
ND
ND
ND
ND
---
---
19-N ov-02
---
1
2.0
2.0
ND
ND
2.0
ND
---
---
27-Jun-03
---
1
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
1
ND
1.0
ND
ND
ND
ND
---
ND
30-Jun-04
---
1
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
1
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
1
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
1
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
1
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
1
ND
ND
ND
ND
ND
ND
---
ND
12-Jul-07
---
1
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = 1.75 pg/L (10/23/07)
19-Dec-07
---
1
ND
ND
ND
ND
ND
ND
ND
ND
8-Ju1-08
---
1
ND
ND
ND
ND
ND
ND
---
ND
17-Dec-08
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
9-Jul-09
0.50
1.0
ND
1.4
ND
ND
ND
ND
ND
ND
16-Dec-09
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = 2 pg/L (02/05/10)
24-Jun-10
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
13-Dec-10
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
20-Jun-11
1.0
1.0
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
1.0
1.0
ND
ND
ND
ND
ND
ND
---
ND
11-Jun-12
1.0
1.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
1.0
1.0
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
1.0
1.0
ND
ND
ND
ND
ND
ND
ND
ND
5-Aug-13
1.0
1.0
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
1.0
1.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
1.0
1.0
ND
ND
ND
ND
ND
ND
---
ND
10-Mar-15
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
18-Aug-15
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
16-Feb-16
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
9-Aug-16
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
13-Feb-17
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
22-Aug-17
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
5-Feb-18
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
13-Aug-18
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
4-Feb-19
0.50
1.0
ND
ND
ND
ND
ND
ND
---
ND
7-Aug-19
0.40
1.0
ND
ND
ND
0.48 J
ND
ND
---
ND
12-Feb-20
0.40
1.0
ND
ND
ND
0.69 J
ND
ND
---
ND
27-Aug-20
0.40
1.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
0.40
1.0
ND
0.7 J
0.7 J
1.10
ND
ND
---
ND
Chromium
8-Sep-94
---
10
8.0
44.0
ND
6.0
48.0
80.0
---
---
1-Dec-94
---
10
14.0
ND
ND
ND
18.0
ND
---
---
9-Feb-95
---
10
14.0
ND
ND
10.0
ND
ND
---
---
2-M a r-95
---
10
ND
ND
ND
ND
ND
ND
---
---
15-N ov-95
---
10
13.0
13.0
ND
ND
ND
ND
---
---
28-May-96
---
10
33.0
ND
ND
ND
ND
ND
---
---
22-Nov-96
---
10
3.0
ND
ND
ND
ND
3.0
---
---
17-J u n-97
---
10
57.0
43.0
ND
3.0
2.0
6.0
---
---
1-Dec-97
---
10
29.0
ND
ND
ND
ND
ND
---
---
20-May-98
---
10
10.0
3.0
ND
ND
12.0
ND
---
---
19-N ov-98
---
10
17.0
3.0
ND
ND
5.0
ND
---
---
21-J u 1-99
---
10
N D
N D
N D
N D
N D
N D
---
---
16-N ov-99
---
10
N D
N D
N D
N D
N D
N D
---
---
10-May-00
---
10
N D
N D
N D
N D
N D
N D
---
---
26-Oct-00
---
10
N D
N D
N D
N D
N D
N D
---
---
18-A p r-01
---
10
N D
12.0
N D
N D
N D
N D
---
---
27-Oct-01
---
10
N D
N D
N D
N D
N D
N D
---
---
13-Jun-02
---
10
ND
ND
ND
ND
ND
ND
---
---
19-N ov-02
---
10
N D
N D
N D
N D
N D
N D
---
---
27-Jun-03
---
10
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
10
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
10
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
10
ND
ND
ND
ND
ND
ND
---
ND
12-Jul-07
---
10
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = 50 pg/L (10/23/07)
19-Dec-07
---
10
ND
2.0 B
ND
ND
ND
ND
1.1 B
1.4 J
8-J u 1-08
---
10
N D
0.54 J
0.58 J
N D
N D
N D
---
N D
17-Dec-08
0.40
10.0
0.73 J
1.8 J
0.96 J
ND
0.96 J
0.70 J
---
ND
9-J u 1-09
0.40
10.0
1.2 J
2.4 J
1.1 J
1.6 J
0.68 J
0.53 J
4.8 J
N D
16-Dec-09
0.40
10.0
1.3 J
ND
ND
ND
0.95 J
ND
---
ND
NC 2L = 10 pg/L (02/05/10)
24-Jun-10
0.40
10.0
1.1 B
3.5 B
2.8 B
2.4 B
1.2 B
1.4 B
---
0.71 J
13-Dec-10
0.40
10.0
2.5 J
1.3 J
1.8 J
0.69 J
0.57 J
1.2 J
---
ND
20-Jun-11
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
11-Jun-12
5.0
10.0
ND
8.6 J
ND
ND
ND
ND
ND
ND
12-Dec-12
5.0
10.0
ND
5.2 J
ND
ND
ND
ND
---
ND
1-May-13
5.0
10.0
ND
ND
ND
ND
ND
ND
ND
ND
5-Aug-13
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
5.0
10.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
10-Mar-15
2.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
18-Aug-15
2.5
10.0
ND
2.7 J
ND
ND
ND
6.7 J
---
ND
16-Feb-16
2.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
9-Aug-16
2.5
10.0
2.8 B
2.8 B
ND
ND
ND
ND
---
2.9 J
13-Feb-17
2.5
10.0
ND
2.6 J
ND
ND
ND
ND
---
ND
22-Aug-17
2.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Feb-18
2.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
13-Aug-18
2.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
4-Feb-19
2.5
5.0
ND
ND
ND
ND
ND
ND
---
ND
7-Aug-19
1.0
5.0
ND
ND
ND
ND
ND
ND
---
ND
12-Feb-20
1.0
5.0
1.5 J
ND
ND
1.1 J
ND
ND
---
ND
27-Aug-20
3.7
5.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
3.7
5.0
4.1 J
4 1
ND
ND
ND
ND
---
ND

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
Cobalt
8-Sep-94
---
10
ND
ND
ND
ND
ND
ND
---
---
1-Dec-94
---
10
11.0
ND
13.0
16.0
22.0
ND
---
---
9-Feb-95
---
10
20.0
14.0
ND
48.0
39.0
ND
---
---
2-Mar-95
---
10
16.0
21.0
ND
29.0
121.0
ND
---
---
15-Nov-95
---
10
20.0
21.0
ND
ND
27.0
ND
---
---
28-May-96
---
10
30.0
16.0
ND
ND
122
ND
---
---
22-Nov-96
---
10
6.0
13.0
ND
4.7
93.0
ND
---
---
17-J u n-97
---
10
130
38.0
ND
6.0
45.0
3.0
---
---
1-Dec-97
---
10
32.0
21.0
ND
12.0
36.0
4.0
---
---
20-May-98
---
10
15.0
16.0
2.0
9.0
100
3.0
---
---
19-Nov-98
---
10
21.0
16.0
2.0
7.0
180
3.0
---
---
21-J u 1-99
---
10
ND
16.0
ND
N D
100
ND
---
---
16-N ov-99
---
10
ND
15.0
ND
N D
38.0
ND
---
---
10-May-00
---
10
ND
17.0
ND
N D
61.0
ND
---
---
26-Oct-00
---
10
ND
15.0
ND
N D
ND
ND
---
---
18-Apr-01
---
10
ND
27.0
ND
N D
74.0
ND
---
---
27-Oct-01
---
10
ND
12.0
ND
N D
47.0
ND
---
---
13-J u n-02
---
10
ND
14.0
ND
N D
251
ND
---
---
19-Nov-02
---
10
ND
10.0
ND
ND
57.0
ND
---
---
27-Jun-03
---
10
ND
15.0
ND
ND
75.0
ND
---
---
30-Dec-03
---
10
ND
17.0
ND
ND
52.0
ND
---
ND
30-Jun-04
---
10
ND
16.0
ND
ND
31.0
ND
---
ND
29-Dec-04
---
10
ND
11.0
ND
ND
46.0
ND
---
ND
29-Jun-05
---
10
ND
11.0
ND
ND
43.0
ND
---
ND
29-Dec-05
---
10
ND
12.0
ND
ND
30.0
ND
---
ND
28-Jun-06
---
10
ND
ND
ND
ND
72.5
ND
---
ND
29-Dec-06
---
10
ND
11.4
ND
ND
37.5
ND
---
ND
12-Jul-07
---
10
ND
11.8
ND
2.7
58.4
ND
---
ND
IMAC = 70 pg/L (10/23/07)
19-Dec-07
---
10
2.5 B
ND
ND
2.0 B
103
2.6 B
8.0 B
1.8 J
8-J u 1-08
---
10
10.3 B
12.1 B
2.0 B
9.0 B
130
4.8 B
---
6.2 J
17-Dec-08
0.60
10.0
2.1 B
11.8 B
2.3 B
3.6 B
43.7
1.6 B
---
2.5 J
9-Jul-09
0.60
10.0
ND
6.2 J
ND
ND
100
ND
2.2 J
ND
16-Dec-09
0.60
10.0
ND
4.7 J
ND
ND
6.6 J
ND
---
ND
24-Jun-10
0.60
10.0
ND
16.3
ND
ND
25.0
ND
---
ND
IMAC = 1 pg/L (2/05/10)
13-Dec-10
0.60
10.0
2.5 B
15.5
ND
ND
{129)
(ND)
---
1.6 (1.0 J) J
20-Jun-11
5.0
10.0
ND
14.2
ND
ND
81.8
ND
---
ND
5-Dec-11
5.0
10.0
ND
12.7
ND
ND
146
ND
---
ND
Resample >
25-Jan-12
5.0
10.0
---
---
---
---
47.5
---
---
ND
11-Jun-12
5.0
10.0
ND
14.2
ND
ND
101
ND
ND
ND
12-Dec-12
5.0
10.0
ND
11.3
ND
ND
113
ND
---
ND
1-May-13
5.0
10.0
ND
24.3
ND
ND
34.0
ND
ND
ND
5-Aug-13
5.0
10.0
ND
24.7
ND
ND
50.9
ND
---
ND
24-Feb-14
5.0
10.0
ND
18.4
ND
ND
9.6 J
ND
ND
ND
12-Aug-14
5.0
10.0
ND
9.4 J
ND
ND
46.3
ND
---
ND
10-Mar-15
2.5
10.0
ND
8.7 J
ND
ND
39.2
ND
---
ND
18-Aug-15
2.5
10.0
ND
9.3 J
ND
ND
116
ND
---
ND
16-Feb-16
2.5
10.0
ND
10.0
ND
ND
13.1
ND
---
ND
9-Aug-16
2.5
10.0
ND
10.0 J
ND
ND
144
ND
---
ND
13-Feb-17
2.5
10.0
ND
8.3 J
ND
ND
78.7
ND
---
ND
22-Aug-17
2.5
10.0
ND
7.4 J
ND
ND
51.1
ND
---
ND
5-Feb-18
2.5
10.0
ND
8.3 J
ND
ND
172
ND
---
ND
13-Aug-18
2.5
10.0
ND
10.7
ND
ND
97.7
ND
---
ND
4-Feb-19
2.5
5.0
ND
9.9
ND
ND
24.0
ND
---
ND
7-Aug-19
1.1
5.0
ND
11.3
ND
ND
127
ND
ND
ND
12-Feb-20
1.1
5.0
ND
7.5
ND
ND
11.4
ND
1.1 J
ND
27-Aug-20
3.6
5.0
ND
9.7
ND
ND
88.7
ND
ND
ND
11-Feb-21
3.6
5.0
ND
10.8
ND
ND
18.6
ND
3.8 J
ND
Copper
8-Sep-94
---
200
ND
ND
ND
ND
ND
660
---
---
1-Dec-94
---
200
ND
ND
ND
N D
ND
ND
---
---
9-Feb-95
---
200
ND
ND
ND
ND
ND
ND
---
---
2-Mar-95
---
200
ND
ND
ND
ND
ND
ND
---
---
15-Nov-95
---
200
ND
ND
ND
ND
ND
ND
---
---
28-May-96
---
200
ND
ND
ND
ND
ND
ND
---
---
22-Nov-96
---
200
ND
ND
32.0
13.0
100
ND
---
---
17-Jun-97
---
200
34.0
350
13.0
37.0
28.0
77.0
---
---
1-Dec-97
---
200
19.0
72.0
14.0
88.0
15.0
34.0
---
---
20-May-98
---
200
12.0
48.0
380
41.0
53.0
28.0
---
---
19-Nov-98
---
200
10.0
ND
410
28.0
53.0
14.0
---
---
21-J u 1-99
---
200
N D
N D
N D
N D
N D
N D
---
---
16-Nov-99
---
200
ND
ND
ND
ND
ND
ND
---
---
10-May-00
---
200
ND
ND
ND
ND
ND
ND
---
---
26-Oct-00
---
200
N D
N D
N D
N D
N D
N D
---
---
18-Apr-01
---
200
N D
N D
N D
N D
N D
N D
---
---
27-Oct-01
---
200
ND
ND
ND
ND
ND
ND
---
---
13-Jun-02
---
200
ND
ND
ND
ND
ND
ND
---
---
19-Nov-02
---
200
ND
ND
ND
ND
ND
ND
---
---
27-Jun-03
---
200
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
200
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
200
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
200
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
200
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
200
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
200
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
10
N D
N D
11.3
5.50 J
10.4
1.90 B
---
0.60 J
12-Jul-07
---
10
ND
ND
13.4
7.90
2.6 J
ND
---
ND
INC 2L = 1,000 pg/L (10/23/07)
19-Dec-07
---
10
2.0 B
ND
8.6 B
3.8 B
7.0 B
0.73 B
5.8 B
9.8
8-J u 1-08
---
10
0.64 J
N D
12.1
3.7 J
8.5 J
N D
---
N D
17-Dec-08
0.30
10.0
0.80 J
13.6
10.2
3.9 J
11.9
0.37 J
---
N D
9-Jul-09
0.30
10.0
ND
ND
6.3 J
ND
5.7 J
ND
8.8 J
ND
16-Dec-09
0.30
10.0
N D
N D
9.2 J
1.6 J
5.7 J
N D
---
N D
24-Jun-10
0.30
10.0
ND
ND
10
1.2 J
5.1 J
ND
---
ND
13-Dec-10
0.30
10.0
1.1 B
N D
13.6
5.8 J
5.6 J
0.59 B
---
0.49 J
20-Jun-11
5.0
10.0
ND
ND
15.3
8.1 J
8.7 J
ND
---
ND
5-Dec-11
5.0
10.0
ND
ND
16.9
10.0 J
7.6 J
ND
---
ND
11-Jun-12
5.0
10.0
ND
10.7
12.2
6.3 J
7.4 J
ND
ND
ND
12-Dec-12
5.0
10.0
ND
ND
11.6
8.5 J
10.4
ND
---
ND
1-May-13
5.0
10.0
ND
ND
13.6
5.8 J
9.6 J
ND
ND
ND
5-Aug-13
5.0
10.0
ND
ND
14.3
ND
10.2
ND
---
ND
24-Feb-14
5.0
10.0
ND
ND
12.2
ND
5.1 J
ND
ND
ND
12-Aug-14
5.0
10.0
ND
ND
10.5
ND
ND
ND
---
ND
10-Mar-15
2.5
10.0
ND
ND
8.7 J
ND
15.5
ND
---
ND
18-Aug-15
2.5
10.0
ND
ND
6.7 J
5.6 J
10.1
ND
---
ND
INC 2L = 50 pg/L (06/01/2016)
16-Feb-16
2.5
10.0
ND
ND
7.8 J
ND
5.1 J
ND
---
ND
9-Aug-16
2.5
10.0
ND
ND
5.4 J
ND
7.8 J
ND
---
ND
13-Feb-17
2.5
10.0
ND
ND
6.8 J
4.3 J
14.5
9.4 J
---
ND
22-Aug-17
2.5
10.0
ND
ND
6.5 J
ND
5.7 J
4.4 J
---
ND
5-Feb-18
2.5
10.0
ND
6.5 J
9.0 J
5.5 J
12.4
2.6 J
---
ND
13-Aug-18
2.5
10.0
ND
5.5 J
12.2
3.7 J
48.8
ND
---
ND
4-Feb-19
2.5
5.0
ND
3.0 J
5.4
8.0
4.3 J
ND
---
ND
7-Aug-19
2.1
5.0
ND
3.5 J
6.0
7.2
4.4 J
2.3 J
---
ND
12-Feb-20
2.1
5.0
ND
ND
9.8
12.7
3.3 J
ND
---
ND
27-Aug-20
4.3
5.0
ND
ND
5.3
13.5
5.6
ND
---
ND
11-Feb-21
4.3
5.0
ND
ND
84.8
9.6
ND
ND
---
ND

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
Lead
8-Sep-94
---
10
ND
13.0
ND
ND
30.0
36.0
---
---
1-Dec-94
---
10
11.0
ND
ND
ND
36.0
ND
---
---
9-Feb-95
---
10
ND
ND
ND
10.0
37.0
ND
---
---
2-M a r-95
---
10
ND
ND
ND
ND
44.0
ND
---
---
15-N ov-95
---
10
ND
ND
ND
ND
ND
ND
---
---
28-May-96
---
10
ND
ND
ND
ND
42.0
ND
---
---
22-Nov-96
---
10
ND
ND
ND
ND
13.0
ND
---
---
17-J u n-97
---
10
20.0
29.0
ND
ND
13.0
ND
---
---
1-Dec-97
---
10
8.0
14.0
ND
5.0
14.0
ND
---
---
20-May-98
---
10
ND
6.0
ND
6.0
21.0
ND
---
---
19-N ov-98
---
10
5.0
ND
ND
ND
58.0
ND
---
---
21-J u l-99
---
10
ND
12.0
14.0
ND
ND
ND
---
---
16-N ov-99
---
10
ND
ND
ND
ND
ND
ND
---
---
10-May-00
---
10
ND
ND
ND
ND
ND
ND
---
---
26-Oct-00
---
10
ND
ND
ND
ND
ND
ND
---
---
18-A p r-01
---
10
ND
ND
ND
ND
ND
ND
---
---
27-Oct-01
---
10
ND
ND
ND
ND
ND
ND
---
---
13-J u n-02
---
10
11.0
ND
ND
ND
ND
ND
---
---
19-N ov-02
---
10
ND
ND
ND
ND
12.0
ND
---
---
27-Jun-03
---
10
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
10
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
10
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
10
ND
ND
ND
ND
ND
2.1 J
---
ND
12-Jul-07
---
10
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = 15 pg/L (10/23/07)
19-Dec-07
---
10
ND
ND
ND
ND
ND
ND
ND
ND
8-Ju1-08
---
10
ND
ND
ND
ND
ND
ND
---
ND
17-Dec-08
4.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
9-Jul-09
4.0
10.0
ND
ND
ND
ND
ND
ND
ND
ND
16-Dec-09
4.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
24-Jun-10
4.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
13-Dec-10
4.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
20-Jun-11
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
11-Jun-12
5.0
10.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
5.0
10.0
ND
ND
ND
ND
ND
ND
ND
ND
5-Aug-13
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
5.0
10.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
10-Mar-15
2.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
18-Aug-15
2.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
16-Feb-16
2.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
9-Aug-16
2.5
10.0
ND
5.1 J
ND
ND
ND
ND
---
ND
13-Feb-17
2.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
22-Aug-17
2.5
10.0
ND
2.8 J
ND
ND
ND
ND
---
ND
5-Feb-18
2.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
13-Aug-18
2.5
10.0
ND
ND
ND
ND
4.6 J
ND
---
ND
4-Feb-19
2.5
5.0
ND
ND
ND
ND
ND
ND
---
ND
7-Aug-19
1.6
5.0
ND
2.0 J
ND
ND
ND
ND
---
ND
12-Feb-20
1.6
5.0
1.9 J
2.1 J
2.1 J
2.8 J
3.1 J
2.3 J
---
ND
27-Aug-20
4.5
5.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
4.5
5.0
ND
ND
ND
ND
ND
ND
---
ND
Mercury
1-Dec-97
---
0.5
ND
ND
ND
ND
ND
ND
---
---
19-N ov-98
---
0.5
N D
N D
N D
N D
N D
N D
---
---
16-Nov-99
---
0.5
N D
0.59
0.65
0.65
0.76
N D
---
---
10-May-00
---
0.5
---
N D
N D
N D
N D
---
---
---
26-Oct-00
---
0.5
---
N D
N D
N D
N D
---
---
---
18-A p r-01
---
0.5
---
N D
N D
N D
N D
---
---
---
13-J u n-02
---
0.5
---
N D
N D
N D
N D
---
---
---
2 7-Jun-03
---
0.5
---
N D
N D
N D
N D
---
---
---
30-Dec-03
---
0.5
---
---
---
---
---
---
---
30-Jun-04
---
0.5
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
---
---
---
---
---
---
---
---
---
29-Jun-05
---
0.5
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
---
---
---
---
---
---
---
---
---
28-Jun-06
---
2.0
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
---
---
---
---
---
---
---
---
---
12-Jul-07
---
0.2
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = 1.05 pg/L (10/23/07)
19-Dec-07
---
---
---
---
---
---
---
---
ND
---
8-Ju1-08
---
0.2
ND
ND
ND
ND
ND
ND
---
ND
17-Dec-08
---
---
---
---
---
---
---
---
---
---
9-Jul-09
0.070
0.2
ND
ND
ND
ND
ND
ND
---
ND
16-Dec-09
---
---
---
---
---
---
---
---
---
---
NC 2L = 1 pg/L (02/05/10)
24-Jun-10
0.070
0.20
ND
ND
ND
ND
ND
0.098 J
---
ND
13-Dec-10
---
---
---
---
---
---
---
---
---
---
20-Jun-11
0.10
0.20
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
---
---
---
---
---
---
---
---
---
---
11-Jun-12
0.10
0.20
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
---
---
---
---
---
---
1-May-13
0.10
0.20
ND
ND
ND
ND
ND
ND
---
ND
5-Aug-
---
---
---
---
---
---
24-Feb-14
0.10
0.20
ND
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
---
---
---
---
---
---
---
---
---
---
10-M a r-15
0.10
0.20
ND
ND
ND
---
---
---
---
ND
16-Feb-16
0.10
0.20
ND
ND
ND
---
---
---
---
ND
13-Feb-17
0.10
0.20
ND
ND
ND
---
---
---
---
ND
22-Aug-17
0.10
0.20
ND
ND
ND
---
---
---
---
ND
5-Feb-18
0.10
0.20
ND
ND
ND
---
---
---
---
ND
4-Feb-19
0.10
0.20
ND
ND
ND
---
---
---
---
ND
11-Feb-21
0.12
0.20
ND
ND
ND
---
---
---
---
---

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
Nickel
8-Sep-94
---
50
ND
ND
ND
ND
ND
ND
---
---
1-Dec-94
---
50
ND
ND
ND
N D
ND
ND
---
---
9-Feb-95
---
50
ND
72
ND
ND
ND
ND
---
---
2-Mar-95
---
50
ND
100
ND
ND
ND
ND
---
---
15-Nov-95
---
50
ND
61.0
ND
ND
ND
ND
---
---
28-May-96
---
50
ND
85.0
ND
ND
ND
ND
---
---
22-Nov-96
---
50
ND
72.0
ND
ND
ND
ND
---
---
17-Jun-97
---
50
75
98.0
ND
ND
ND
ND
---
---
1-Dec-97
---
50
ND
89.0
ND
ND
ND
ND
---
---
20-May-98
---
50
ND
91.0
ND
ND
ND
ND
---
---
19-N ov-98
---
50
ND
83.0
ND
N D
N D
ND
---
---
21-J u 1-99
---
50
ND
109
ND
N D
ND
ND
---
---
16-Nov-99
---
50
ND
122
ND
ND
ND
ND
---
---
10-May-00
---
50
N D
104
ND
N D
ND
ND
---
---
26-Oct-00
---
50
ND
93.0
ND
N D
ND
ND
---
---
18-Apr-01
---
50
N D
107
ND
N D
ND
ND
---
---
27-Oct-01
---
50
N D
92.0
ND
N D
N D
ND
---
---
13-J u n-02
---
50
N D
98.0
ND
N D
ND
ND
---
---
19-N ov-02
---
50
ND
74.0
ND
N D
ND
ND
---
---
27-Jun-03
---
50
ND
85.0
ND
ND
ND
ND
---
---
30-Dec-03
---
50
ND
100
ND
ND
ND
ND
---
ND
30-Jun-04
---
50
ND
120 (81.0)
ND
ND
ND
ND
---
ND
29-Dec-04
---
50
ND
100
ND
ND
ND
ND
---
ND
29-Jun-05
---
50
ND
150
ND
ND
ND
ND
---
ND
29-Dec-05
---
50
ND
96.0
ND
ND
ND
ND
---
ND
28-Jun-06
---
50
ND
88.7
ND
ND
ND
ND
---
ND
29-Dec-06
---
50
ND
94.7
30.1
14.2
8.9 J
ND
---
ND
12-Jul-07
---
50
ND
99.0
30.6 J
13.9 J
13.7 J
ND
---
ND
NC 2L = 100 pg/L (10/23/07)
19-Dec-07
---
50
ND
83.4
23.7
11.0
18.3
ND
11.4
ND
8-Ju1-08
---
50
ND
76.0
28.1 J
11.5 J
27.0 J
ND
---
ND
17-Dec-08
1.7
50.0
ND
75.5
27.8 J
12.2 J
11.0 B
ND
---
2.4 J
9-J u 1-09
1.7
50.0
2.2 J
93.5
29.4 J
11.7 J
23.2 J
N D
13.1 J
N D
16-Dec-09
1.7
50.0
N D
81.2
28.2 J
11.8 B
2.6 B
N D
---
3.0 J
24-Jun-10
1.7
50.0
ND
76.3
19.7 J
9.0 J
7.0 J
4.5 J
---
ND
13-Dec-10
1.7
50.0
N D
83.0
23.5 J
6.8 B
20.7 J
N D
---
2.7 J
20-Jun-11
5.0
50.0
ND
78.8
30.1 J
11.2 J
15.3 J
ND
---
ND
5-Dec-11
5.0
50.0
N D
89.1
32.8 J
11.7 J
24.3 J
N D
---
N D
11-Jun-12
5.0
50.0
ND
91.8
28.9 J
10.0 J
17.3 J
ND
ND
ND
12-Dec-12
5.0
50.0
N D
91.8
29.2 J
9.3 J
21.1 J
N D
---
N D
1-May-13
5.0
50.0
ND
89.6
31.9 J
10.4 J
5.7 J
ND
ND
ND
5-Aug-13
5.0
50.0
ND
87.9
28.1 J
9.0 J
8.4 J
ND
---
ND
24-Feb-14
5.0
50.0
ND
83.1
16.7 J
10.4 J
ND
ND
ND
ND
12-Aug-14
5.0
50.0
ND
97.9
29 J
12.9 J
13.2 J
ND
---
ND
10-Mar-15
2.5
50.0
ND
91.9
32.9 J
12.3 J
8.2 J
ND
---
ND
18-Aug-15
2.5
50.0
N D
98.0
28.0 J
11.9 J
26.2 J
5.4 J
---
N D
16-Feb-16
2.5
50.0
ND
92.0
35.4 J
12.7 J
3.7 J
ND
---
ND
9-Aug-16
2.5
50.0
3.3 J
88.9
29.0 J
12.2 J
30.7 J
N D
---
N D
13-Feb-17
2.5
50.0
N D
89.6
30.4 J
13.5 J
16.2 J
N D
---
N D
22-Aug-17
2.5
50.0
ND
84.2
28.2 J
12.3 J
13.5 J
ND
---
ND
5-Feb-18
2.5
50.0
N D
87.6
29.8 J
11.7 J
28.5 J
N D
---
N D
13-Aug-18
2.5
50.0
ND
88.9
29.0 J
12.3 J
21.9 J
ND
---
ND
4-Feb-19
2.5
5.0
ND
85.7
17.4
10.7
5.5
ND
---
ND
7-Aug-19
0.90
5.0
ND
92.6
27.8
11.7
18.7
ND
---
ND
12-Feb-20
0.90
5.0
1.1 J
89.9
20.5
13.2
3.4 J
N D
---
N D
27-Aug-20
3.50
5.0
ND
99.1
19.5
12.2
18.1
ND
---
ND
11-Feb-21
3.50
5.0
ND
91.8
21.4
13.5
3.9 J
ND
---
ND
Selenium
8-Sep-94
---
20
ND
ND
ND
ND
ND
ND
---
---
1-Dec-94
---
20
N D
N D
N D
N D
N D
N D
---
---
9-Feb-95
---
20
ND
ND
ND
ND
ND
ND
---
---
2-Mar-95
---
20
ND
ND
ND
ND
ND
ND
---
---
15-N ov-95
---
20
N D
N D
N D
N D
N D
N D
---
---
28-May-96
---
20
ND
ND
ND
ND
ND
ND
---
---
22-Nov-96
---
20
ND
ND
ND
ND
ND
ND
---
---
17-Jun-97
---
20
ND
ND
ND
ND
ND
ND
---
---
1-Dec-97
---
20
ND
ND
ND
ND
ND
ND
---
---
20-May-98
---
20
ND
ND
ND
ND
ND
ND
---
---
19-N ov-98
---
20
N D
N D
N D
N D
N D
N D
---
---
21-J u 1-99
---
20
N D
N D
N D
N D
36.0
N D
---
---
16-N ov-99
---
20
N D
N D
N D
N D
N D
N D
---
---
10-May-00
---
20
N D
N D
N D
N D
N D
N D
---
---
26-Oct-00
---
20
N D
N D
N D
N D
N D
N D
---
---
18-Apr-01
---
20
N D
N D
N D
N D
N D
N D
---
---
27-Oct-01
---
20
N D
N D
N D
N D
N D
N D
---
---
13-Jun-02
---
20
ND
ND
ND
ND
ND
ND
---
---
19-N ov-02
---
20
N D
N D
N D
N D
N D
N D
---
---
27-Jun-03
---
20
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
20
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
20
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
20
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
20
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
20
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
20
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
10
ND
ND
ND
ND
ND
ND
---
ND
12-Jul-07
---
10
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = 50 pg/L (10/23/07)
19-Dec-07
---
10
ND
11.5
ND
ND
ND
ND
ND
ND
8-Ju1-08
---
10
ND
ND
ND
ND
ND
ND
---
ND
17-Dec-08
3.8
10
4.8 B
5.1 B
4.8 B
ND
ND
ND
---
4.9 J
9-Jul-09
3.8
10
ND
ND
4.2 J
ND
ND
ND
ND
ND
16-Dec-09
3.8
10
ND
ND
ND
5.1 J
ND
ND
---
ND
NC 2L = 20 pg/L (02/05/10)
24-Jun-10
3.8
10
ND
ND
ND
ND
ND
ND
---
ND
13-Dec-10
3.8
10
ND
ND
ND
ND
ND
ND
---
ND
20-Jun-11
10.0
10
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
10.0
10
ND
ND
ND
ND
ND
ND
---
ND
11-Jun-12
10.0
10
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
10.0
10
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
10.0
10
ND
ND
ND
ND
ND
ND
ND
ND
5-Aug-13
10.0
10
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
10.0
10
ND
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
10.0
10
ND
ND
ND
ND
ND
ND
---
ND
10-Mar-15
5.0
10
ND
ND
ND
ND
ND
ND
---
ND
18-Aug-15
5.0
10
ND
ND
ND
ND
ND
ND
---
ND
16-Feb-16
5.0
10
ND
ND
ND
ND
ND
ND
---
ND
9-Aug-16
5.0
10
ND
ND
ND
ND
ND
ND
---
ND
13-Feb-17
5.0
10
ND
ND
ND
ND
ND
ND
---
ND
22-Aug-17
5.0
10
ND
ND
ND
ND
ND
ND
---
ND
5-Feb-18
5.0
10
ND
ND
ND
ND
ND
ND
---
ND
13-Aug-18
5.0
10
ND
ND
ND
ND
ND
ND
---
ND
4-Feb-19
5.0
10
ND
ND
ND
ND
ND
ND
---
ND
7-Aug-19
4.7
10.0
ND
ND
ND
ND
ND
ND
---
ND
12-Feb-20
4.7
10.0
ND
ND
ND
ND
ND
ND
---
ND
27-Aug-20
4.7
10.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
4.7
10.0
ND
ND
ND
ND
ND
ND
---
ND

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
Silver
8-Sep-94
---
10
ND
ND
ND
ND
ND
ND
---
---
1-Dec-94
---
10
ND
ND
ND
N D
ND
ND
---
---
9-Feb-95
---
10
ND
ND
ND
N D
ND
ND
---
---
2-M a r-95
---
10
ND
ND
ND
N D
ND
ND
---
---
15-N ov-95
---
10
ND
ND
ND
N D
ND
ND
---
---
28-May-96
---
10
ND
ND
ND
ND
ND
ND
---
---
22-Nov-96
---
10
ND
ND
ND
ND
ND
ND
---
---
17-Jun-97
---
10
ND
ND
ND
ND
ND
ND
---
---
1-Dec-97
---
10
ND
8.0
ND
N D
ND
3.0
---
---
20-May-98
---
10
ND
ND
ND
ND
ND
ND
---
---
19-N ov-98
---
10
ND
ND
ND
N D
ND
ND
---
---
21-J u 1-99
---
10
ND
ND
ND
N D
ND
ND
---
---
16-N ov-99
---
10
ND
ND
ND
N D
ND
ND
---
---
10-May-00
---
10
ND
ND
ND
N D
ND
ND
---
---
26-Oct-00
---
10
ND
ND
ND
N D
ND
ND
---
---
18-A p r-01
---
10
ND
15.0
ND
N D
ND
ND
---
---
27-Oct-01
---
10
ND
ND
ND
N D
ND
ND
---
---
13-Jun-02
---
10
ND
ND
ND
ND
ND
ND
---
---
19-N ov-02
---
10
ND
ND
ND
N D
ND
ND
---
---
27-Jun-03
---
10
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
10
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
10
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
10
ND
ND
ND
ND
ND
ND
---
ND
12-Jul-07
---
10
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = 17.5 pg/L (10/23/07)
19-Dec-07
---
10
ND
0.57 J
0.60 J
0.55 J
ND
0.33 J
ND
ND
8-J u 1-08
---
10
N D
2.7 J
2.3 J
1.1 J
0.22 J
0.69 J
---
0.12 J
17-Dec-08
0.10
10.0
0.13 J
1.8 J
1.4 J
0.85 J
0.12 J
0.51 J
---
N D
9-Jul-09
0.10
10.0
ND
0.84 J
0.63 J
0.45 J
ND
0.11 J
ND
ND
16-Dec-09
0.10
10.0
0.12 J
2.0 J
1.6 J
1.0 J
0.12 J
0.52 J
---
N D
NC 2L = 20 pg/L (02/05/10)
24-Jun-10
0.10
10.0
ND
0.38 J
0.33 J
0.35 J
ND
ND
---
ND
13-Dec-10
0.10
10.0
0.15 B
1.3 J
0.99 J
0.45 B
{ND)
(ND)
---
6.21 {0.19 J J
20-Jun-11
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
11-Jun-12
5.0
10.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
5.0
10.0
ND
ND
ND
ND
ND
ND
ND
ND
5-Aug-13
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
5.0
10.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
10-Mar-15
2.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
18-Aug-15
2.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
16-Feb-16
2.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
9-Aug-16
2.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
13-Feb-17
2.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
22-Aug-17
2.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Feb-18
2.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
13-Aug-18
2.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
4-Feb-19
2.5
5.0
ND
ND
ND
ND
ND
ND
---
ND
7-Aug-19
2.5
5.0
ND
ND
ND
ND
ND
ND
---
ND
12-Feb-20
2.5
5.0
ND
ND
ND
ND
ND
ND
---
ND
27-Aug-20
2.5
5.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
2.5
5.0
ND
ND
ND
ND
ND
ND
---
ND
Thallium
8-Sep-94
---
10
ND
ND
ND
ND
ND
ND
---
---
1-Dec-94
---
10
ND
ND
ND
N D
ND
ND
---
---
9-Feb-95
---
10
ND
ND
ND
ND
ND
ND
---
---
2-M a r-95
---
10
ND
ND
ND
ND
ND
ND
---
---
15-N ov-95
---
10
ND
ND
ND
ND
ND
ND
---
---
28-May-96
---
10
ND
ND
ND
ND
ND
ND
---
---
22-Nov-96
---
10
ND
ND
ND
ND
ND
ND
---
---
17-J u n-97
---
10
ND
3.0
ND
N D
ND
ND
---
---
1-Dec-97
---
10
ND
ND
ND
N D
ND
ND
---
---
20-May-98
---
10
ND
ND
ND
ND
ND
ND
---
---
19-N ov-98
---
10
ND
ND
ND
N D
ND
ND
---
---
21-J u 1-99
---
10
N D
N D
N D
N D
N D
N D
---
---
16-N ov-99
---
10
N D
N D
N D
N D
N D
N D
---
---
10-May-00
---
10
N D
N D
N D
N D
N D
N D
---
---
26-Oct-00
---
10
N D
N D
N D
N D
N D
N D
---
---
18-Apr-01
---
10
N D
N D
N D
N D
N D
N D
---
---
27-Oct-01
---
10
N D
N D
N D
N D
N D
N D
---
---
13-Jun-02
---
10
ND
ND
ND
ND
ND
ND
---
---
19-N ov-02
---
10
N D
N D
N D
N D
N D
N D
---
---
27-Jun-03
---
10
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
10
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
10
ND
10.0 J
ND
ND
ND
ND
---
ND
29-Jun-05
---
10
ND
22.0
13.0
ND
ND
ND
---
ND
29-Dec-05
---
10
ND
23.0
20.0
ND
ND
ND
---
ND
28-Jun-06
---
10
ND
25.7
12.6
ND
ND
ND
---
ND
29-Dec-06
---
6
ND
ND
ND
ND
ND
ND
---
ND
12-Jul-07
---
5.5
ND
ND
ND
ND
ND
ND
---
ND
IMAC = 0.28 pg/L (10/23/07)
19-Dec-07
---
5.5
ND
4.0 J
ND
ND
ND
ND
ND
ND
8-Ju1-08
---
5.5
ND
ND
ND
ND
ND
ND
---
ND
17-Dec-08
3.0
5.5
ND
3.2 J
3.2 J
ND
ND
ND
---
ND
9-Jul-09
3.0
5.5
ND
ND
ND
4.1 J
ND
ND
ND
ND
16-Dec-09
3.0
5.5
ND
ND
ND
ND
ND
ND
---
ND
24-Jun-10
3.0
5.5
ND
ND
5.2 J
3.1 J
ND
ND
---
ND
IMAC = 0.2 pg/L (10/1/10)
13-Dec-10
3.0
5.5
ND
ND
7.7
ND
ND
ND
---
ND
20-Jun-11
5.4
5.5
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
5.4
5.5
ND
ND
ND
ND
ND
ND
---
ND
11-Jun-12
5.4
5.5
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
5.4
5.5
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
5.4
5.5
ND
ND
ND
ND
ND
ND
ND
ND
5-Aug-13
5.4
5.5
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
5.4
5.5
ND
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
5.4
5.5
ND
ND
ND
ND
ND
ND
---
ND
10-Mar-15
5.0
5.5
ND
ND
ND
ND
ND
ND
---
ND
18-Aug-15
5.0
5.5
ND
ND
ND
ND
ND
ND
---
ND
16-Feb-16
5.0
5.5
ND
ND
ND
ND
ND
ND
---
ND
9-Aug-16
5.0
5.5
ND
ND
ND
ND
ND
ND
---
ND
13-Feb-17
0.02
5.5
0.023 J
0.040 J
ND
ND
0.035 J
ND
---
ND
22-Aug-17
0.02
5.5
ND
ND
ND
ND
0.033 J
ND
---
ND
5-Feb-18
0.03
0.1
ND
ND
ND
ND
0.047 J
ND
---
ND
13-Aug-18
0.02
5.5
ND
ND
ND
ND
0.037 J
ND
---
ND
4-Feb-19
0.06
0.1
ND
ND
ND
ND
ND
ND
---
ND
7-Aug-19
0.060
0.10
ND
ND
ND
ND
ND
ND
---
ND
12-Feb-20
0.060
0.10
ND
ND
ND
ND
ND
ND
---
ND
27-Aug-20
0.050
0.10
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
0.050
0.10
ND
ND
ND
ND
ND
ND
---
ND

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
Tin
1-Dec-97
---
100
ND
ND
ND
ND
ND
ND
---
---
19-N ov-98
---
100
ND
ND
ND
ND
ND
ND
---
---
16-N ov-99
---
100
ND
ND
ND
ND
ND
ND
---
---
26-Oct-00
---
100
---
ND
ND
ND
ND
---
---
---
18-A p r-01
---
100
---
ND
ND
ND
ND
---
---
---
27-Oct-01
---
100
---
---
---
---
---
---
---
---
13-Jun-02
---
100
ND
ND
ND
ND
ND
ND
---
---
19-Nov-02
---
100
---
---
---
---
---
---
---
---
27-Jun-03
---
100
ND
149
127
ND
ND
ND
---
---
30-Dec-03
---
100
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
100
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
100
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
100
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
100
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
100
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
100
ND
41.1
14.4
3.2 J
ND
ND
---
ND
12-Jul-07
---
100
ND
35.2 J
13.9 J
5.2 J
ND
ND
---
ND
19-Dec-07
---
100
ND
33.6
7.4
ND
ND
ND
ND
ND
8-J u 1-08
---
100
4.4 J
28.6 J
15.1 J
5.4 J
3.0 J
3.6 J
---
N D
17-Dec-08
1.8
100
ND
22.5 J
9.2 J
ND
ND
ND
---
ND
9-Jul-09
1.8
100
ND
21.4 J
8.6 J
ND
ND
ND
---
ND
16-Dec-09
1.8
100
ND
26.3 J
10.7 J
ND
ND
ND
---
ND
IMAC = 2100 pg/L (02/05/10)
24-Jun-10
1.8
100
ND
23.4 J
10.7 J
3.2 J
2.2 J
1.9 J
---
ND
13-Dec-10
1.8
100
ND
30.3 J
12.1 J
5.8 J
ND
ND
---
ND
20-Jun-11
5.0
100
ND
26.8 J
13.8 J
ND
ND
ND
---
ND
5-Dec-11
5.0
100
ND
25.8 J
13.9 J
ND
ND
ND
---
ND
11-Jun-12
5.0
100
ND
22.2 J
9.0 J
ND
ND
ND
ND
ND
12-Dec-12
5.0
100
ND
30.0 J
13.2 J
ND
ND
ND
---
ND
1-May-13
5.0
100
ND
25.8 J
12.2 J
ND
ND
ND
---
ND
5-Aug-13
5.0
100
ND
22.7 J
12.5 J
ND
ND
ND
---
ND
24-Feb-14
5.0
100
ND
26.7 J
11.7 J
9.8 J
ND
ND
ND
ND
12-Aug-14
5.0
100
ND
30.7 J
8.2 J
ND
ND
ND
---
ND
10-Mar-15
2.5
100
ND
28.7 J
11.1 J
ND
ND
ND
---
ND
18-Aug-15
2.5
100
ND
27.7 J
7.5 J
ND
ND
ND
---
ND
16-Feb-16
2.5
100
ND
28.6 J
10.4 J
---
---
---
---
ND
9-Aug-16
2.5
100
ND
20.9 J
5.4 J
---
---
---
---
ND
13-Feb-17
2.5
100
ND
25.5 B
7.8 B
---
---
---
---
3.6 J,
22-Aug-17
2.5
100
ND
17.2 J
5.3 J
---
---
---
---
ND
5-Feb-18
2.5
100
ND
20.3 J
9.5 J
---
---
---
---
ND
13-Aug-18
2.5
100
ND
22.2 J
7.4 J
---
---
ND
---
ND
4-Feb-19
2.5
5.0
ND
24.8
5.5
---
---
---
---
ND
7-Aug-19
1.6
5.0
ND
29.3
9.7
---
---
---
---
ND
12-Feb-20
1.6
5.0
ND
26.0
5.8
---
---
---
---
ND
27-Aug-20
4.7
5.0
ND
27.6
5.1
---
---
---
---
ND
11-Feb-21
4.7
5.0
ND
30.1
8.0
---
---
---
---
---
Vanadium
8-Sep-94
---
40
ND
ND
ND
ND
ND
130
---
---
1-Dec-94
---
40
63.0
ND
ND
45.0
ND
ND
---
---
9-Feb-95
---
40
ND
ND
ND
ND
ND
ND
---
---
2-M a r-95
---
40
41.0
ND
ND
45.0
ND
ND
---
---
15-N ov-95
---
40
ND
ND
ND
ND
ND
ND
---
---
28-May-96
---
40
83.0
ND
ND
ND
ND
ND
---
---
22-N ov-96
---
40
7.0
17
ND
21.0
ND
ND
---
---
17-Jun-97
---
40
450
560
ND
19.0
ND
ND
---
---
1-Dec-97
---
40
62.0
88.0
ND
41.0
ND
10.0
---
---
20-May-98
---
40
25.0
15.0
ND
10.0
5.0
ND
---
---
19-Nov-98
---
40
33.0
29.0
5.0
16.0
9.0
5.0
---
---
21-J u 1-99
---
40
N D
N D
N D
N D
N D
N D
---
---
16-N ov-99
---
40
N D
N D
N D
N D
N D
N D
---
---
10-May-00
---
40
N D
N D
N D
N D
N D
N D
---
---
26-Oct-00
---
40
N D
N D
N D
N D
N D
N D
---
---
18-Apr-01
---
40
N D
N D
N D
N D
N D
N D
---
---
27-Oct-01
---
40
N D
N D
N D
N D
N D
N D
---
---
13-Jun-02
---
40
ND
ND
ND
ND
ND
ND
---
---
19-N ov-02
---
40
N D
N D
N D
N D
N D
N D
---
---
27-Jun-03
---
40
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
40
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
40
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
40
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
40
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
40
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
40
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
25
2.7 J
N D
N D
14.5
N D
1.0 J
---
N D
12-Jul-07
---
25
ND
ND
ND
19.4 J
ND
ND
---
ND
IMAC = 3.5 pg/L (10/23/07)
19-Dec-07
---
25
2.2 B
2.2 B
ND
15.7 J
3.0 B
1.2 B
4.0 J
0.62 J
8-Ju1-08
---
25
2.6 J
2.4 J
ND
14.6 J
1.4 J
1.2 J
---
0.20 J
17-Dec-08
0.20
25.0
1.9 B
2.3 B
N D
13.9 J
2.5 B
1.2 B
---
0.76 J
9-Jul-09
0.20
25.0
3.9 B
9.7 J
2.5 B
18.4 J
2.9 B
2.2 B
8.5 J
1.30 J
16-Dec-09
0.20
25.0
2.0 B
4.4 J
1.3 B
14.0 J
2.2 B
1.5 B
---
0.53 J
24-Jun-10
0.20
25.0
1.8 J
4.4 J
1.5 J
13.3 J
2.2 J
1.3 J
---
ND
IMAC = 0.3 pg/L (10/1/10)
13-Dec-10
0.20
25.0
3.2 J
3.6 J
0.35 B
16.6 J
1.8 B
1.0 B
---
0.36 J
20-Jun-11
5.0
25.0
ND
ND
ND
14.5 J
ND
ND
---
ND
5-Dec-11
5.0
25.0
ND
ND
ND
13.5 J
ND
ND
---
ND
11-Jun-12
5.0
25.0
ND
18.0 J
ND
12.3 J
ND
ND
ND
ND
12-Dec-12
5.0
25.0
ND
ND
ND
13.6 J
ND
ND
---
ND
1-May-13
5.0
25.0
ND
ND
ND
6.3 J
ND
ND
ND
ND
5-Aug-13
5.0
25.0
ND
ND
ND
10.2 J
ND
ND
---
ND
24-Feb-14
5.0
25.0
ND
ND
ND
12.9 J
ND
ND
ND
ND
12-Aug-14
5.0
25.0
ND
ND
ND
18.6 J
ND
ND
---
ND
10-Mar-15
2.5
25.0
3.1 J
11.6 J
6.2 J
13.4 J
ND
ND
---
ND
18-Aug-15
2.5
25.0
3.4 J
6.8 J
3.6 J
19.6 J
2.8 J
ND
---
ND
16-Feb-16
2.5
25.0
2.7 J
3.3 J
ND
14.4 J
ND
ND
---
ND
9-Aug-16
2.5
25.0
2.5 J
3.5 J
ND
21.2 J
ND
ND
---
ND
13-Feb-17
2.5
25.0
4.4 J
4.1 J
ND
18.4 J
3.0 J
2.9 J
---
ND
22-Aug-17
2.5
25.0
ND
6.6 J
ND
20.6 J
2.6 J
ND
---
ND
5-Feb-18
2.5
25.0
3.6 J
4.4 J
ND
17.6 J
ND
2.5 J
---
ND
13-Aug-18
2.5
25.0
ND
5.3 J
ND
20.4 J
2.9 J
ND
---
ND
4-Feb-19
2.5
5.0
ND
3.5 J
ND
12.0
ND
ND
---
ND
7-Aug-19
1.3
5.0
2.6 J
4.1 J
1.9 J
22.1
1.7 J
2.4 J
---
ND
12-Feb-20
1.3
5.0
ND
ND
ND
17.0
ND
1.4 J
---
ND
27-Aug-20
3.9
5.0
ND
ND
ND
21.1
ND
ND
6.8
ND
11-Feb-21
3.9
5.0
ND
ND
ND
13.4
ND
ND
7.2
ND

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
Zinc
8-Sep-94
---
50
110
160
ND
ND
320
430
---
---
1-Dec-94
---
50
132
ND
ND
70
164
ND
---
---
9-Feb-95
---
50
144
89
ND
91
79
74
---
---
2-Mar-95
---
50
67
ND
ND
ND
111
ND
---
---
15-Nov-95
---
50
ND
50
ND
ND
ND
ND
---
---
28-May-96
---
50
136
ND
ND
ND
122
ND
---
---
22-Nov-96
---
50
79.0
48.0
28.0
ND
38.0
ND
---
---
17-Jun-97
---
50
370
410
33.0
39.0
36.0
69.0
---
---
1-Dec-97
---
50
140
110
11.0
45.0
34.0
30.0
---
---
20-May-98
---
50
70.0
63.0
23.0
31.0
47.0
34.0
---
---
19-Nov-98
---
50
61.0
33.0
21.0
17.0
53.0
10.0
---
---
21-J u 1-99
---
50
ND
ND
ND
ND
ND
ND
---
---
16-N ov-99
---
50
ND
ND
ND
ND
ND
ND
---
---
10-May-00
---
50
ND
ND
ND
ND
ND
ND
---
---
26-Oct-00
---
50
ND
ND
ND
ND
ND
ND
---
---
18-A p r-01
---
50
ND
ND
ND
ND
ND
ND
---
---
27-Oct-01
---
50
ND
ND
ND
ND
ND
ND
---
---
13-J u n-02
---
50
ND
ND
ND
ND
382
ND
---
---
19-N ov-02
---
50
ND
ND
ND
ND
ND
ND
---
---
27-Jun-03
---
50
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
50
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
50
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
50
ND
ND
ND
66.0
ND
ND
---
ND
29-Jun-05
---
50
ND
54.0
56.0
ND
ND
ND
---
ND
29-Dec-05
---
50
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
50
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
50
8.0 J
ND
ND
4.1 J
4.3 J
4.1 J
---
ND
12-Jul-07
---
10
9.6 J
ND
ND
ND
ND
ND
---
ND
NC 2L = 1,050 pg/L (10/23/07)
19-Dec-07
---
10
4.3 B
14.3 B
6.3 B
ND
ND
ND
2.4 B
102
8-J u 1-08
---
10
5.9 B
N D
N D
N D
4.1 B
N D
---
1.2 J
17-Dec-08
0.40
10.0
2.4 B
6.3 J
ND
ND
4.6 J
0.60 B
---
0.49 J
9-Jul-09
0.40
10.0
3.4 B
ND
ND
ND
ND
ND
6.1 B
1.6 J
16-Dec-09
0.40
10.0
4.6 B
ND
ND
ND
7.4 B
ND
---
7.7 J
NC 2L = 1,000 pg/L (02/05/10)
24-Jun-10
0.40
10.0
0.58 J
ND
ND
ND
ND
1.3 J
---
ND
13-Dec-10
0.40
10.0
4.5 B
ND
ND
ND
ND
ND
---
6.7 J
20-Jun-11
10.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
10.0
10.0
ND
ND
ND
ND
ND
ND
---
12.4
11-Jun-12
10.0
10.0
ND
20.9
ND
ND
ND
ND
ND
ND
12-Dec-12
10.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
10.0
10.0
ND
ND
ND
ND
11.8
ND
10.0
ND
5-Aug-13
10.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
10.0
10.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
10.0
10.0
ND
ND
ND
ND
16.9
ND
---
ND
18-Aug-15
5.0
10.0
7.4 J
ND
ND
ND
5.2 J
ND
---
ND
16-Feb-16
5.0
10.0
14.5
16.7
17.8
46.1
5.9 J
ND
---
ND
9-Aug-16
5.0
10.0
12.0
7.7 J
ND
ND
ND
ND
---
ND
13-Feb-17
5.0
10.0
12.3
ND
ND
ND
9.8 J
6.0 J
---
ND
22-Aug-17
5.0
10.0
ND
6.3 J
ND
ND
ND
ND
---
ND
5-Feb-18
5.0
10.0
6.7 J
17.9
ND
ND
ND
ND
---
ND
13-Aug-18
5.0
10.0
ND
ND
ND
ND
8.1 J
ND
---
ND
4-Feb-19
5.0
10.0
6.8 J
ND
5.0 J
ND
ND
ND
---
ND
7-Aug-19
3.9
10.0
8.3 J
ND
ND
ND
ND
ND
---
ND
12-Feb-20
3.9
10.0
4.3 J
ND
ND
ND
4.5 J
ND
---
ND
27-Aug-20
9.5
10.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
9.5
10.0
12.9
ND
ND
ND
ND
ND
---
ND
Cyanide
9-Ju1-09
5.0
10
ND
ND
ND
ND
46.9
ND
ND
ND
Resample >
28-Sep-09
5.0
10
---
---
---
---
ND
---
---
ND
NC 2 L = 70 pg/ L (10/23/07)
16-Dec-09
---
---
---
---
---
---
---
---
---
---
24-Jun-10
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
13-Dec-10
---
---
---
---
---
---
Resample >
20-Jun-11
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
---
---
---
---
---
---
---
---
---
---
11-Jun-12
5.0
10.0
ND
6.4 J
ND
ND
8.7 J
ND
---
ND
12-Dec-12
---
---
---
---
---
---
---
---
---
---
1-May-13
5.0
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Aug-13
---
---
---
---
---
---
---
---
---
---
24-Feb-14
5.0
10.0
ND
ND
ND
ND
ND
ND
ND
5.5 J
12-Aug-14
5.0
10.0
ND
ND
ND
ND
ND
ND
ND
ND
10-Mar-15
5.0
10.0
9.5 B
7.5 B
8.5 B
8.8 B
11.8 B
6.6 B
---
5.6 J
16-Feb-16
4.0
10.0
ND
ND
ND
---
---
---
---
ND
13-Feb-17
4.0
10.0
ND
ND
ND
---
---
---
---
ND
2 2-Aug-17
4.0
10.0
ND
ND
ND
---
---
---
---
ND
5-Feb-18
4.0
10.0
ND
ND
ND
---
---
---
---
ND
4-Feb-19
6.0
8.0
ND
ND
ND
---
---
---
---
ND

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
ORGANICS
Acetone
27-Oct-01
---
100
244 B
109 B
ND
130 B
128 B
476 B
---
479
13-Jun-02
---
100
ND
ND
ND
ND
ND
ND
---
---
13-Jun-02
---
100
ND
ND
ND
ND
ND
ND
---
---
19-N ov-02
---
100
ND
ND
ND
ND
ND
ND
---
---
27-Jun-03
---
100
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
100
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
100
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
100
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
100
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
100
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
100
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
100
ND
ND
ND
ND
ND
ND
---
ND
12-Jul-07
---
100
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = 700 pg/L (10/23/07)
19-Dec-07
---
100
ND
ND
ND
ND
ND
ND
ND
4.5 J
8-Ju1-08
---
100
ND
ND
ND
ND
ND
ND
---
ND
17-Dec-08
20.0
100
ND
ND
ND
ND
ND
ND
---
ND
9-Jul-09
20.0
100
ND
ND
ND
ND
ND
ND
ND
ND
16-Dec-09
2.2
100
ND
ND
ND
ND
ND
ND
---
2.8 J
NC 2L = 6,000 pg/L (02/05/10)
24-Jun-10
2.2
100
ND
18.5 B
6.5 B
ND
2.2 B
ND
---
7.7 J
13-Dec-10
2.2
100
ND
ND
ND
ND
ND
ND
---
ND
20-Jun-11
2.2
100
ND
ND
ND
ND
ND
2.4 B
---
3.9 J
5-Dec-11
2.2
100
ND
2.3 B
ND
ND
ND
ND
---
8.8 J
11-Jun-12
2.2
100
ND
3.5 B
ND
ND
ND
ND
ND
4.7 J
12-Dec-12
10.0
100
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
10.0
100
ND
ND
ND
ND
ND
ND
ND
14.6 J
5-Aug-13
10.0
100
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
10.0
100
ND
ND
ND
ND
ND
ND
ND
25.7 J
12-Aug-14
10.0
100
ND
ND
ND
ND
ND
ND
ND
22.0 J
10-Mar-15
10.0
100
ND
ND
ND
ND
ND
ND
ND
ND
18-Aug-15
10.0
100
ND
ND
ND
ND
ND
ND
ND
ND
16-Feb-16
10.0
100
ND
ND
ND
ND
ND
ND
ND
ND
9-Aug-16
10.0
100
ND
ND
ND
ND
ND
ND
---
ND
13-Feb-17
10.0
100
ND
ND
ND
ND
ND
ND
---
ND
22-Aug-17
10.0
100
ND
ND
ND
ND
ND
ND
---
ND
5-Feb-18
10.0
100
ND
ND
ND
ND
ND
ND
---
ND
13-Aug-18
10.0
100
ND
ND
ND
ND
ND
ND
---
ND
4-Feb-19
6.2
25
ND
ND
ND
ND
ND
ND
---
ND
14-Aug-19 for MW-6 >
7-Aug-19
6.2
25.0
ND
ND
ND
ND
ND
ND
---
ND
12-Feb-20
6.2
25.0
ND
ND
ND
ND
ND
ND
---
ND
27-Aug-20
6.2
25.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
6.2
25.0
ND
ND
ND
ND
ND
ND
---
ND
Benzene
8-Sep-94
---
5
ND
ND
ND
ND
ND
ND
---
---
1-Dec-94
---
5
ND
ND
ND
ND
ND
ND
---
---
9-Feb-95
---
5
ND
ND
ND
ND
ND
ND
---
---
2-Mar-95
---
5
ND
ND
ND
ND
ND
ND
---
---
15-N ov-95
---
5
ND
ND
ND
ND
ND
ND
---
---
28-May-96
---
5
ND
ND
ND
ND
ND
ND
---
---
22-Nov-96
---
5
ND
ND
ND
ND
ND
ND
---
---
17-Jun-97
---
5
ND
ND
ND
ND
ND
ND
---
---
1-Dec-97
---
5
ND
ND
ND
ND
ND
ND
---
---
20-May-98
---
5
ND
ND
ND
ND
ND
ND
---
---
19-N ov-98
---
5
ND
ND
ND
ND
ND
ND
---
---
21-J u l-99
---
5
ND
ND
ND
ND
ND
ND
---
---
16-N ov-99
---
5
ND
ND
ND
ND
ND
ND
---
---
10-May-00
---
5
ND
ND
ND
ND
ND
ND
---
---
26-Oct-00
---
5
ND
ND
ND
ND
ND
ND
---
---
18-A p r-01
---
5
ND
ND
ND
ND
ND
ND
---
---
27-Oct-01
---
5
ND
ND
ND
ND
ND
ND
---
---
13-Jun-02
---
5
ND
ND
ND
ND
ND
ND
---
---
19-N ov-02
---
5
ND
ND
ND
ND
ND
ND
---
---
27-Jun-03
---
5
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
5
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
5
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
3
ND
1.5
ND
ND
ND
ND
---
ND
Resample >
23-Feb-07
---
3
---
1.2
---
---
---
---
---
ND
12-Jul-07
---
1
ND
1.9
ND
ND
ND
ND
---
ND
NC 2L = 1 pg/L (10/23/07)
19-Dec-07
---
1
ND
1.8
0.48 J
0.26 J
ND
ND
ND
ND
8-Ju1-08
---
1
ND
1.4
0.51 J
0.32 J
ND
ND
---
ND
17-Dec-08
0.25
1.0
ND
1.7
0.54 J
ND
ND
ND
---
ND
9-Ju1-09
0.25
1.0
ND
1.7
0.34 J
ND
ND
ND
ND
ND
16-Dec-09
0.25
1.0
ND
1.7
0.60 J
0.29 J
ND
ND
---
ND
24-Jun-10
0.25
1.0
ND
0.77 J
0.49 J
0.33 J
ND
ND
---
ND
13-Dec-10
0.25
1.0
ND
1.8
0.59 J
0.37 J
ND
ND
---
ND
Resample >
8-Feb-11
0.25
1.0
---
1.4
---
---
---
---
---
ND
20-Jun-11
0.25
1.0
ND
1.7
0.60 J
0.39 J
ND
ND
---
ND
5-Dec-11
0.25
1.0
ND
1.4
0.69 J
0.40 J
ND
ND
---
ND
11-Jun-12
0.25
1.0
ND
ND
0.51 J
ND
ND
ND
ND
ND
12-Dec-12
0.25
1.0
ND
1.6
0.73 J
0.32 J
ND
ND
---
ND
Resample >
10-Jan-13
0.25
1.0
ND
1.4
---
---
---
---
ND
ND
1-May-13
0.25
1.0
ND
1.3
0.56 J
0.27 J
ND
ND
ND
ND
5-Aug-13
0.25
1.0
ND
1.6
0.64 J
0.44 J
ND
ND
---
ND
24-Feb-14
0.25
1.0
ND
1.4
ND
ND
ND
ND
ND
ND
12-Aug-14
0.25
1.0
ND
1.7
0.61 J
0.25 J
ND
ND
ND
ND
10-Mar-15
0.25
1.0
ND
1.3
0.54 J
ND
ND
ND
ND
ND
18-Aug-15
0.25
1.0
ND
1.5
0.66 J
0.32 J
ND
ND
---
ND
16-Feb-16
0.25
1.0
ND
1.3
0.56 J
ND
ND
ND
ND
ND
9-Aug-16
0.25
1.0
ND
1.4
0.53 J
0.29 J
ND
ND
ND
ND
13-Feb-17
0.25
1.0
ND
1.2
0.61 J
ND
ND
ND
ND
ND
22-Aug-17
0.25
1.0
ND
1.3
0.54 J
ND
ND
ND
ND
ND
5-Feb-18
0.25
1.0
ND
1.2
0.67 J
ND
ND
ND
ND
ND
13-Aug-18
0.25
1.0
ND
1.3
0.61 J
0.29 J
ND
ND
ND
ND
4-Feb-19
0.15
1.0
ND
1.6
ND
ND
ND
ND
ND
ND
14-Aug-19 for MW-6 >
7-Aug-19
0.15
1.0
ND
1.7
0.54 J
0.30 J
ND
ND
ND
ND
12-Feb-20
0.15
1.0
ND
1.5
ND
ND
ND
ND
ND
ND
27-Aug-20
0.15
1.0
ND
1.9
0.49 J
ND
ND
ND
ND
ND
11-Feb-21
0.15
1.0
ND
1.8
ND
ND
ND
ND
---
ND

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
Bromomethane
17-Dec-08
0.29
10.0
ND
ND
0.58 J
ND
ND
ND
---
ND
9-Jul-09
0.29
10.0
ND
ND
ND
ND
ND
ND
ND
ND
16-Dec-09
0.29
10.0
ND
ND
ND
ND
ND
ND
---
ND
24-Jun-10
0.29
10.0
ND
ND
ND
ND
ND
ND
---
ND
IMAC = 10 pg/L (8/1/10)
13-Dec-10
0.29
10.0
ND
ND
ND
ND
ND
ND
---
ND
20-Jun-11
0.29
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
0.29
10.0
ND
ND
ND
ND
ND
ND
ND
ND
11-Jun-12
0.29
10.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
0.29
10.0
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
0.29
10.0
ND
ND
ND
ND
ND
ND
ND
ND
5-Aug-13
0.29
10.0
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
0.29
10.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
0.29
10.0
ND
ND
ND
ND
ND
ND
ND
ND
10-Mar-15
0.29
10.0
ND
ND
ND
ND
ND
ND
ND
ND
18-Aug-15
0.29
10.0
ND
ND
ND
ND
ND
ND
---
ND
16-Feb-16
0.29
10.0
ND
ND
ND
ND
ND
ND
ND
ND
9-Aug-16
0.29
10.0
ND
ND
ND
ND
ND
ND
---
ND
13-Feb-17
0.29
10.0
ND
ND
ND
ND
ND
ND
---
ND
22-Aug-17
0.29
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Feb-18
0.29
10.0
ND
ND
ND
ND
ND
ND
---
ND
13-Aug-18
0.29
10.0
ND
ND
ND
ND
ND
ND
---
ND
4-Feb-19
0.62
2.0
ND
ND
ND
ND
ND
ND
---
ND
14-Aug-19 for MW-6 >
7-Aug-19
0.62
2.0
N D
N D
N D
ND
N D
N D
---
N D
12-Feb-20
0.62
2.0
ND
ND
ND
ND
ND
ND
---
ND
27-Aug-20
0.62
2.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
0.62
2.0
ND
ND
ND
ND
ND
ND
---
ND
2-Butanone (MEK)
17-Dec-08
0.96
100
ND
ND
ND
ND
1.2 J
ND
---
ND
NC 2L = 4,200 pg/L (10/23/07)
9-Jul-09
0.96
100
ND
ND
ND
ND
ND
ND
ND
ND
16-Dec-09
0.96
100
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = 4,000 pg/L (02/05/10)
24-Jun-10
0.96
100
ND
ND
ND
ND
ND
ND
---
ND
13-Dec-10
0.96
100
ND
ND
ND
ND
ND
ND
---
ND
20-Jun-11
0.96
100
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
0.96
100
ND
ND
ND
ND
ND
ND
---
ND
11-Jun-12
0.96
100
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
0.96
100
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
0.96
100
ND
ND
ND
ND
ND
ND
ND
ND
8-May-13
0.96
100
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
0.96
100
ND
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
0.96
100
ND
ND
ND
ND
ND
ND
ND
ND
10-Mar-15
0.96
100
ND
ND
ND
ND
ND
ND
ND
ND
18-Aug-15
0.96
100
ND
ND
ND
ND
ND
ND
---
ND
16-Feb-16
0.96
100
ND
ND
ND
ND
ND
ND
ND
ND
9-Aug-16
0.96
100
ND
ND
ND
ND
ND
ND
---
ND
13-Feb-17
0.96
100
ND
ND
ND
ND
ND
ND
---
ND
22-Aug-17
0.96
100
ND
ND
ND
ND
ND
ND
---
ND
5-Feb-18
0.96
100
ND
ND
ND
ND
ND
ND
---
ND
13-Aug-18
0.96
100
ND
ND
ND
ND
ND
ND
---
ND
4-Feb-19
3.30
5
ND
ND
ND
ND
ND
ND
---
ND
14-Aug 19 for MW-6 ->
7-Aug-19
3.3
5.0
N D
N D
N D
ND
N D
N D
---
N D
12-Feb-20
3.3
5.0
ND
ND
ND
ND
ND
ND
---
ND
27-Aug-20
3.3
5.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
3.3
5.0
ND
ND
ND
ND
ND
ND
---
ND
Carbon Disulfide
17-Jun-97
---
100
ND
64.0
ND
ND
ND
ND
---
---
1-Dec-97
---
100
ND
5.0
8.0
ND
ND
ND
---
---
20-May-98
---
100
ND
7.5
6.2
ND
ND
ND
---
---
19-N ov-98
---
100
ND
ND
ND
ND
ND
ND
---
---
21-J u 1-99
---
100
N D
N D
N D
N D
N D
N D
---
---
16-N ov-99
---
100
N D
N D
N D
N D
N D
N D
---
---
10-May-00
---
100
N D
N D
N D
N D
N D
N D
---
---
26-Oct-00
---
100
N D
N D
N D
N D
N D
N D
---
---
18-A p r-01
---
100
N D
N D
N D
N D
N D
N D
---
---
27-Oct-01
---
100
N D
N D
N D
N D
N D
N D
---
---
13-Jun-02
---
5
ND
ND
ND
ND
ND
ND
---
---
19-N ov-02
---
100
N D
N D
N D
N D
N D
N D
---
---
27-Jun-03
---
100
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
100
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
100
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
100
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
100
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
100
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
100
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
100
ND
ND
ND
ND
ND
ND
---
ND
12-Jul-07
---
100
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = 700 pg/L (10/23/07)
19-Dec-07
---
100
ND
ND
ND
ND
ND
ND
ND
ND
8-Ju1-08
---
100
ND
ND
ND
ND
ND
ND
---
ND
17-Dec-08
1.2
100
ND
ND
ND
ND
ND
ND
---
ND
9-Jul-09
1.2
100
ND
ND
ND
ND
ND
ND
ND
ND
16-Dec-09
1.2
100
ND
ND
ND
ND
ND
ND
---
ND
24-Jun-10
1.2
100
ND
ND
ND
ND
ND
ND
---
ND
13-Dec-10
1.2
100
ND
ND
ND
ND
ND
ND
---
ND
20-Jun-11
1.2
100
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
1.2
100
ND
ND
ND
ND
ND
ND
---
ND
11-Jun-12
1.2
100
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
1.2
100
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
1.2
100
ND
ND
ND
ND
ND
ND
ND
ND
5-Aug-13
1.2
100
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
1.2
100
ND
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
1.2
100
ND
ND
ND
ND
ND
ND
ND
ND
10-Mar-15
1.2
100
ND
ND
ND
ND
ND
ND
ND
ND
18-Aug-15
1.2
100
ND
ND
ND
ND
ND
ND
---
ND
16-Feb-16
1.2
100
ND
ND
ND
ND
ND
ND
ND
ND
9-Aug-16
1.2
100
ND
ND
ND
ND
ND
ND
---
ND
13-Feb-17
1.2
100
ND
ND
ND
ND
ND
ND
---
ND
22-Aug-17
1.2
100
ND
ND
ND
ND
ND
ND
---
ND
5-Feb-18
1.2
100
ND
ND
ND
ND
ND
ND
---
ND
13-Aug-18
1.2
100
ND
ND
ND
ND
ND
ND
---
ND
4-Feb-19
0.4
2
ND
ND
ND
ND
ND
ND
---
ND
14-Aug-19 for MW-6 >
7-Aug-19
0.40
2.0
N D
N D
N D
N D
N D
N D
---
N D
12-Feb-20
0.40
2.0
ND
ND
ND
ND
ND
ND
---
ND
27-Aug-20
0.40
2.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
0.40
2.0
ND
ND
ND
ND
ND
ND
---
ND

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
Chlorobenzene
8-Sep-94
---
5
ND
10.0
7.0
ND
ND
ND
---
---
1-Dec-94
---
5
ND
ND
7.0
ND
ND
ND
---
---
9-Feb-95
---
5
ND
13.0
8.0
6.0
ND
ND
---
---
2-M a r-95
---
5
ND
12.0
9.0
ND
ND
ND
---
---
15-N ov-95
---
5
ND
14.0
8.0
9.0
ND
ND
---
---
28-May-96
---
5
ND
15.0
9.0
10.0
ND
ND
---
---
22-N ov-96
---
5
ND
15.0
ND
11.0
ND
ND
---
---
17-J u n-97
---
5
ND
19.0
11.0
14.0
ND
ND
---
---
1-Dec-97
---
5
ND
17.0
9.0
14.0
ND
ND
---
---
20-May-98
---
5
ND
20.0
8.6
12.0
ND
ND
---
---
19-N ov-98
---
5
ND
17.2
9.2
10.0
ND
ND
---
---
21-J u 1-99
---
5
ND
14.0
10.0
11.0
ND
ND
---
---
16-N ov-99
---
5
ND
16.0
10.0
8.0
ND
ND
---
---
10-May-00
---
5
ND
17.0
11.0
10.0
ND
ND
---
---
26-Oct-00
---
5
ND
16.0
12.0
9.0
ND
ND
---
---
18-A p r-01
---
5
ND
16.0
13.0
6.0
ND
ND
---
---
27-Oct-01
---
0.5
ND
17.0
12.0
9.0
ND
ND
---
---
13-J u n-02
---
0.5
ND
16.0
11.0
8.0
ND
ND
---
---
19-N ov-02
---
0.5
ND
18.0
15.0
9.0
ND
ND
---
---
27-Jun-03
---
0.5
ND
17.7
13.3
7.4
ND
ND
---
ND
30-Dec-03
---
5
ND
20.0
15.0
6.1
ND
ND
---
ND
30-Jun-04
---
5
ND
18.0
15.0
9.9
ND
ND
---
ND
29-Dec-04
---
5
ND
19.0
16.0
9.4
ND
ND
---
ND
29-Jun-05
---
5
ND
15.0
13.0
8.0
ND
ND
---
ND
29-Dec-05
---
5
ND
18.0
16.0
5.0
ND
ND
---
ND
28-Jun-06
---
5
ND
16.5
10.8
7.8
ND
ND
---
ND
29-Dec-06
---
3
ND
17.0
17.0
4.2
ND
ND
---
ND
12-Jul-07
---
3
ND
17.0
16.0
ND
ND
ND
---
ND
NC 2L = 50 pg/L (10/23/07)
19-Dec-07
---
3
ND
17.3
16.9
4.7
ND
ND
ND
ND
8-J u 1-08
---
3
N D
17.2
17.4
6.5
N D
N D
---
N D
17-Dec-08
0.23
3.0
ND
15.9
15.6
2.6 J
ND
ND
---
ND
9-Jul-09
0.23
3.0
ND
16.1
17.2
6.1
ND
ND
ND
ND
16-Dec-09
0.23
3.0
ND
15.5
17.7
4.8
ND
ND
---
ND
24-Jun-10
0.23
3.0
ND
8.3
15.7
6.3
ND
ND
---
ND
13-Dec-10
0.23
3.0
N D
17.7
18.2
6.4
N D
N D
---
0.28 J
20-Jun-11
0.23
3.0
ND
16.3
17.2
6.7
ND
ND
---
ND
5-Dec-11
0.23
3.0
ND
14.2
17.0
5.8
ND
ND
---
ND
11-Jun-12
0.23
3.0
ND
12.0
14.8
4.4
ND
ND
ND
ND
12-Dec-12
0.23
3.0
ND
15.8
17.9
4.5
ND
ND
---
ND
1-May-13
0.23
3.0
ND
14.0
16.6
3.0 J
ND
ND
ND
ND
5-Aug-13
0.23
3.0
ND
14.4
15.9
4.6
ND
ND
---
ND
24-Feb-14
0.23
3.0
ND
16.3
2.5 J
1.4 J
ND
ND
ND
ND
12-Aug-14
0.23
3.0
ND
15.6
18.3
3.6
ND
ND
ND
ND
10-Mar-15
0.23
3.0
ND
16.0
17.0
2.1 J
ND
ND
ND
ND
18-Aug-15
0.23
3.0
ND
12.8
17.6
4.3
ND
ND
---
ND
16-Feb-16
0.23
3.0
ND
13.5
16.4
1.5 J
ND
ND
ND
ND
9-Aug-16
0.23
3.0
ND
13.5
16.9
4.2
ND
ND
---
ND
13-Feb-17
0.23
3.0
ND
13.6
18.0
1.3 J
ND
ND
---
ND
22-Aug-17
0.23
3.0
ND
14.2
19.9
4.2
ND
ND
---
ND
5-Feb-18
0.23
3.0
ND
13.5
17.3
0.54 J
ND
ND
---
ND
13-Aug-18
0.23
3.0
ND
14.5
22.2
3.4
ND
ND
---
ND
4-Feb-19
0.23
1.0
ND
13.6
0.35 J
1.3
ND
ND
---
ND
14-Aug-19 for MW-6 >
7-Aug-19
0.23
1.0
N D
10.2
16.9
N D
N D
N D
---
N D
12-Feb-20
0.23
1.0
ND
ND
ND
2.0
ND
ND
---
ND
27-Aug-20
0.23
1.0
ND
16.1
17.5
4.1
0.32 J
ND
---
ND
11-Feb-21
0.23
1.0
ND
15.1
7.3
2.2
ND
ND
---
ND
Chloroethane
1-Dec-97
---
10
ND
5.0
2.0
2.0
ND
ND
---
---
20-May-98
---
10
ND
ND
ND
ND
ND
ND
---
---
19-N ov-98
---
10
N D
N D
N D
N D
N D
N D
---
---
21-J u 1-99
---
10
N D
N D
N D
N D
N D
N D
---
---
16-N ov-99
---
10
N D
N D
N D
N D
N D
N D
---
---
10-May-00
---
10
N D
N D
N D
N D
N D
N D
---
---
26-Oct-00
---
10
N D
N D
N D
N D
N D
N D
---
---
18-A p r-01
---
10
N D
N D
N D
N D
N D
N D
---
---
27-Oct-01
---
10
N D
N D
N D
N D
N D
N D
---
---
13-Jun-02
---
10
ND
ND
ND
ND
ND
ND
---
---
19-N ov-02
---
10
N D
N D
N D
N D
N D
N D
---
---
27-Jun-03
---
10
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
10
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
10
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
10
ND
2.2
1.9
ND
ND
ND
---
ND
12-Jul-07
---
10
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = 2,800 pg/L (10/23/07)
19-Dec-07
---
10
ND
1.9
1.9
1.5
ND
ND
ND
ND
8-J u 1-08
---
10
N D
2.2 J
2.5 J
1.8 J
N D
N D
---
N D
17-Dec-08
0.54
10.0
N D
1.6 J
N D
N D
N D
N D
---
N D
9-Jul-09
0.54
10.0
ND
ND
ND
3.8 J
ND
ND
ND
ND
16-Dec-09
0.54
10.0
ND
ND
2.2 J
2.0 J
ND
ND
---
ND
NC 2L = 3,000 pg/L (02/05/10)
24-Jun-10
0.54
10.0
ND
ND
2.1 J
2.0 J
ND
ND
---
ND
13-Dec-10
0.54
10.0
ND
1.8 J
2.0 J
1.7 J
ND
ND
---
ND
20-Jun-11
0.54
10.0
ND
1.2 J
2.2 J
2.0 J
ND
ND
---
ND
5-Dec-11
0.54
10.0
ND
1.3 J
2.0 J
1.7 J
ND
ND
---
ND
11-Jun-12
0.54
10.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
0.54
10.0
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
0.54
10.0
ND
ND
1.9 J
2.7 J
ND
ND
ND
ND
5-Aug-13
0.54
10.0
ND
ND
2.0 J
2.2 J
ND
ND
---
ND
24-Feb-14
0.54
10.0
ND
1.1 J
0.82 J
ND
ND
ND
ND
ND
12-Aug-14
0.54
10.0
ND
1.1 J
1.50 J
1.1 J
ND
ND
ND
ND
10-Mar-15
0.54
10.0
ND
1.0 J
1.80 J
0.81 J
ND
ND
ND
ND
18-Aug-15
0.54
10.0
ND
1.2 J
2.0 J
3.7 J
ND
ND
---
ND
16-Feb-16
0.54
10.0
ND
1.1 J
1.8 J
0.79 J
ND
ND
ND
ND
9-Aug-16
0.54
10.0
ND
0.68 J
2.4 J
1.5 J
ND
ND
---
ND
13-Feb-17
0.54
10.0
ND
0.76 J
1.6 J
1.1 J
ND
ND
---
ND
22-Aug-17
0.54
10.0
ND
1.3 J
2.0 J
1.6 J
ND
ND
---
ND
5-Feb-18
0.54
10.0
ND
1.7 J
1.7 J
0.68 J
ND
ND
---
ND
13-Aug-18
0.54
10.0
ND
1.2 J
2.4 J
1.40 J
ND
ND
---
ND
4-Feb-19
0.49
1.0
ND
1.3
ND
0.79 J
ND
ND
---
ND
14-Aug-19 for MW-6 >
7-Aug-19
0.49
1.0
ND
0.94 J
1.9
1.3
ND
ND
---
ND
12-Feb-20
0.49
1.0
ND
1.6
1.3
1.5
ND
ND
---
ND
27-Aug-20
0.49
1.0
ND
0.87 J
1.5
1.1
ND
ND
---
ND
11-Feb-21
0.49
1.0
ND
1.2
1.0 I,v
1.3 v1
ND
ND
---
ND

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
Chloromethane
9-Jul-09
0.11
1.0
ND
ND
ND
ND
ND
ND
ND
ND
NC 2L = 2.6 pg/L (10/23/07)
16-Dec-09
0.11
1.0
ND
ND
ND
ND
ND
ND
---
ND
24-Jun-10
0.11
1.0
ND
ND
ND
ND
ND
0.11 J
---
ND
NC 2L = 3 pg/L (02/05/10)
13-Dec-10
0.11
1.0
ND
ND
ND
ND
ND
ND
---
ND
20-Jun-11
0.11
1.0
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
0.11
1.0
ND
ND
ND
ND
ND
ND
---
ND
11-Jun-12
0.11
1.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
0.11
1.0
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
0.11
1.0
ND
ND
ND
ND
ND
ND
ND
ND
5-Aug-13
0.11
1.0
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
0.11
1.0
ND
ND
ND
ND
ND
ND
ND
0.25 J
12-Aug-14
0.11
1.0
ND
ND
ND
ND
ND
ND
ND
ND
10-Mar-15
0.11
1.0
ND
ND
ND
ND
ND
ND
ND
ND
18-Aug-15
0.11
1.0
ND
ND
ND
ND
ND
ND
---
ND
16-Feb-16
0.11
1.0
ND
ND
ND
ND
ND
ND
ND
ND
9-Aug-16
0.11
1.0
ND
ND
ND
ND
ND
ND
---
ND
13-Feb-17
0.11
1.0
0.20 B
ND
0.22 B
0.23 B
0.19 B
0.32 B
---
0.18 J
22-Aug-17
0.11
1.0
ND
ND
ND
ND
ND
ND
---
ND
5-Feb-18
0.11
1.0
ND
ND
ND
ND
ND
ND
---
ND
13-Aug-18
0.11
1.0
ND
ND
ND
ND
ND
ND
---
ND
4-Feb-19
0.39
1.0
ND
ND
ND
ND
ND
ND
---
ND
14-Aug-19 for MW-6 >
7-Aug-19
0.39
1.0
ND
ND
ND
ND
ND
ND
---
ND
12-Feb-20
0.39
1.0
ND
ND
ND
ND
ND
ND
---
ND
27-Aug-20
0.39
1.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
0.39
1.0
ND
ND
ND
ND
ND
ND
---
ND
1,2-Dichlorobenzene
1-Dec-97
---
5
ND
3.0
2.0
1.0
ND
ND
---
---
20-May-98
---
5
ND
ND
ND
ND
ND
ND
---
---
19-N ov-98
---
5
ND
2.4
2.3
ND
ND
ND
---
---
21-J u 1-99
---
5
ND
ND
ND
ND
ND
ND
---
---
16-N ov-99
---
5
ND
ND
ND
ND
ND
ND
---
---
10-May-00
---
5
ND
ND
ND
ND
ND
ND
---
---
26-Oct-00
---
5
ND
ND
ND
ND
ND
ND
---
---
18-A p r-01
---
5
ND
ND
ND
ND
ND
ND
---
---
27-Oct-01
---
5
ND
ND
ND
ND
ND
ND
---
---
13-Jun-02
---
5
ND
ND
ND
ND
ND
ND
---
---
19-N ov-02
---
5
ND
ND
ND
ND
ND
ND
---
---
27-Jun-03
---
5
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
5
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
5
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
5
ND
1.5
2.3
ND
ND
ND
---
ND
12-Jul-07
---
5
ND
1.4 J
1.7 J
0.31 J
ND
ND
---
ND
NC 2L = 24 pg/L (10/23/07)
19-Dec-07
---
5
ND
1.6
2.0
0.37 J
ND
ND
ND
ND
8-J u 1-08
---
5
N D
1.6 J
2.0 J
0.39 J
N D
N D
---
N D
17-Dec-08
0.30
5.0
ND
1.4 J
1.9 J
ND
ND
ND
---
ND
9-Jul-09
0.30
5.0
ND
1.6 J
2.0 J
0.36 J
ND
ND
ND
ND
16-Dec-09
0.30
5.0
N D
1.6 J
2.0 J
0.33 J
N D
N D
---
N D
NC 2L = 20 pg/L (02/05/10)
24-Jun-10
0.30
5.0
ND
0.96 J
1.7 J
0.31 J
ND
ND
---
ND
13-Dec-10
0.30
5.0
ND
1.9 J
1.9 J
0.43 J
ND
ND
---
ND
20-Jun-11
0.30
5.0
ND
1.5 J
1.7 J
0.37 J
ND
ND
---
ND
5-Dec-11
0.30
5.0
ND
1.3 J
1.6 J
ND
ND
ND
---
ND
11-Jun-12
0.30
5.0
ND
1.0 J
1.5 J
ND
ND
ND
ND
ND
12-Dec-12
0.30
5.0
ND
1.3 J
1.7 J
ND
ND
ND
---
ND
1-May-13
0.30
5.0
ND
1.2 J
1.6 J
ND
ND
ND
ND
ND
5-Aug-13
0.30
5.0
ND
1.2 J
1.6 J
0.30 J
ND
ND
---
ND
24-Feb-14
0.30
5.0
ND
1.4 J
0.64 J
ND
ND
ND
ND
ND
12-Aug-14
0.30
5.0
ND
1.2 J
1.5 J
ND
ND
ND
ND
ND
10-Mar-15
0.30
5.0
ND
1.1 J
1.1 J
ND
ND
ND
ND
ND
18-Aug-15
0.30
5.0
ND
0.88 J
1.3 J
ND
ND
ND
---
ND
16-Feb-16
0.30
5.0
ND
1.1 J
1.4 J
ND
ND
ND
ND
ND
9-Aug-16
0.30
5.0
ND
1.2 J
1.4 J
ND
ND
ND
---
ND
13-Feb-17
0.30
5.0
ND
1.2 J
1.4 J
ND
ND
ND
---
ND
22-Aug-17
0.30
5.0
ND
1.2 J
1.5 J
ND
ND
ND
---
ND
5-Feb-18
0.30
5.0
ND
1.0 J
1.4 J
ND
ND
ND
---
ND
13-Aug-18
0.30
5.0
ND
1.2 J
1.6 J
ND
ND
ND
---
ND
4-Feb-19
0.29
1.0
ND
1.0 J
ND
ND
ND
ND
---
ND
14-Aug-19 for MW-6 >
7-Aug-19
0.29
1.0
ND
0.62 J
1.2
ND
ND
ND
---
ND
12-Feb-20
0.29
1.0
ND
0.82 J
0.71 J
ND
ND
ND
---
ND
27-Aug-20
0.29
1.0
ND
1.20
1.3
ND
ND
ND
---
ND
11-Feb-21
0.29
1.0
ND
1.10
0.83 J
ND
ND
ND
---
ND

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
1,4-Dichlorobenzene
8-Sep-94
---
5
ND
ND
5.0
ND
ND
ND
---
---
1-Dec-94
---
5
ND
ND
5.0
ND
ND
ND
---
---
9-Feb-95
---
5
ND
8.0
6.0
ND
ND
ND
---
---
2-M a r-95
---
5
ND
7.0
6.0
ND
ND
ND
---
---
15-N ov-95
---
5
ND
7.0
6.0
ND
ND
ND
---
---
28-May-96
---
5
ND
ND
ND
ND
ND
ND
---
---
22-Nov-96
---
5
ND
ND
ND
ND
ND
ND
---
---
17-J u n-97
---
5
ND
7.6
6.2
ND
ND
ND
---
---
1-Dec-97
---
5
ND
6.0
5.0
4.0
ND
ND
---
---
20-May-98
---
5
ND
7.6
ND
ND
ND
ND
---
---
19-N ov-98
---
5
ND
3.7
2.8
ND
ND
ND
---
---
21-J u 1-99
---
5
ND
ND
ND
ND
ND
ND
---
---
16-N ov-99
---
5
ND
ND
ND
ND
ND
ND
---
---
10-May-00
---
5
ND
ND
ND
ND
ND
ND
---
---
26-Oct-00
---
5
ND
5.0
6.0
ND
ND
ND
---
---
18-A p r-01
---
5
ND
ND
5.0
6.0
ND
ND
---
---
27-Oct-01
---
5
ND
ND
ND
ND
ND
ND
---
---
13-Jun-02
---
5
ND
ND
ND
ND
ND
ND
---
---
19-N ov-02
---
5
ND
ND
ND
ND
ND
ND
---
---
27-Jun-03
---
5
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
5
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
5
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
3
ND
3.0
3.3
ND
ND
ND
---
ND
Resample >
23-Feb-07
---
3
---
3.2
3.3
---
---
---
---
ND
12-Jul-07
---
1
ND
3.3
2.9
0.31 J
ND
ND
---
ND
NC 2L = 1.4 pg/L (10/23/07)
19-Dec-07
---
1
ND
3.0
2.7
ND
ND
ND
ND
ND
8-Ju1-08
---
1
ND
3.0
2.4
ND
ND
ND
---
ND
17-Dec-08
0.33
1.0
ND
2.9
2.5
ND
ND
ND
---
ND
9-Jul-09
0.33
1.0
ND
ND
ND
ND
ND
ND
ND
ND
16-Dec-09
0.33
1.0
ND
2.8
2.2
ND
ND
ND
---
ND
NC 2L = 6 pg/L (02/05/10)
24-Jun-10
0.33
1.0
ND
1.6
ND
ND
ND
ND
---
ND
13-Dec-10
0.33
1.0
ND
3.1
1.9
ND
ND
ND
---
ND
20-Jun-11
0.33
1.0
ND
2.7
1.6
ND
ND
ND
---
ND
5-Dec-11
0.33
1.0
ND
2.2
1.4
ND
ND
ND
---
ND
11-Jun-12
0.33
1.0
ND
1.8
1.4
ND
ND
ND
ND
ND
12-Dec-12
0.33
1.0
ND
2.4
1.3
ND
ND
ND
---
ND
1-May-13
0.33
1.0
ND
2.1
1.2
ND
ND
ND
ND
ND
5-Aug-13
0.33
1.0
ND
2.0
1.3
ND
ND
ND
---
ND
24-Feb-14
0.33
1.0
ND
2.2
1.8
ND
ND
ND
ND
ND
12-Aug-14
0.33
1.0
ND
2.4
1.3
ND
ND
ND
ND
ND
10-Mar-15
0.33
1.0
ND
2.2
1.1
ND
ND
ND
ND
ND
18-Aug-15
0.33
1.0
ND
1.5
1.1
ND
ND
ND
---
ND
16-Feb-16
0.33
1.0
ND
2.0
1.0
ND
ND
ND
ND
ND
9-Aug-16
0.33
1.0
ND
1.9
1.0
ND
ND
ND
---
ND
13-Feb-17
0.33
1.0
ND
1.9
0.90 J
ND
ND
ND
---
ND
22-Aug-17
0.33
1.0
ND
1.9
0.96 J
ND
ND
ND
---
ND
5-Feb-18
0.33
1.0
ND
1.6
1.1
ND
ND
ND
---
ND
13-Aug-18
0.33
1.0
ND
1.9
1.1
ND
ND
ND
---
ND
4-Feb-19
0.26
1.0
ND
ND
ND
ND
ND
ND
---
ND
14-Aug-19 for MW-6 >
7-Aug-19
0.26
1.0
ND
ND
ND
ND
ND
ND
---
ND
12-Feb-20
0.26
1.0
ND
ND
ND
ND
ND
ND
---
ND
27-Aug-20
0.26
1.0
ND
2.1
1.4
ND
ND
ND
---
ND
11-Feb-21
0.26
1.0
ND
1.9
0.8 J
ND
ND
ND
---
ND
Trans-1,4-Dichloro-2-Butene
20-May-98
---
100
ND
ND
5.1
ND
ND
ND
---
---
19-N ov-98
---
100
ND
ND
ND
ND
ND
ND
---
---
21-J u 1-99
---
100
N D
N D
N D
N D
N D
N D
---
---
16-N ov-99
---
100
N D
N D
N D
N D
N D
N D
---
---
10-May-00
---
100
N D
N D
N D
N D
N D
N D
---
---
26-Oct-00
---
100
N D
N D
N D
N D
N D
N D
---
---
18-A p r-01
---
100
N D
N D
N D
N D
N D
N D
---
---
27-Oct-01
---
100
N D
N D
N D
N D
N D
N D
---
---
19-Nov-02
---
100
ND
ND
ND
ND
ND
ND
---
---
27-Jun-03
---
100
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
100
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
100
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
100
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
100
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
100
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
100
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
100
ND
ND
ND
ND
ND
ND
---
ND
12-Jul-07
---
100
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = NE pg/L
19-Dec-07
---
100
ND
ND
ND
ND
ND
ND
ND
ND
8-Ju1-08
---
100
ND
ND
ND
ND
ND
ND
---
ND
17-Dec-08
1.0
100
ND
ND
ND
ND
ND
ND
---
ND
9-Jul-09
1.0
100
ND
ND
ND
ND
ND
ND
ND
ND
16-Dec-09
1.0
100
ND
ND
ND
ND
ND
ND
---
ND
24-Jun-10
1.0
100
ND
ND
ND
ND
ND
ND
---
ND
13-Dec-10
1.0
100
ND
ND
ND
ND
ND
ND
---
ND
20-Jun-11
1.0
100
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
1.0
100
ND
ND
ND
ND
ND
ND
---
ND
11-Jun-12
1.0
100
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
1.0
100
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
1.0
100
ND
ND
ND
ND
ND
ND
ND
ND
5-Aug-13
1.0
100
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
1.0
100
ND
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
1.0
100
ND
ND
ND
ND
ND
ND
ND
ND
10-Mar-15
1.0
100
ND
ND
ND
ND
ND
ND
ND
ND
18-Aug-15
1.0
100
ND
ND
ND
ND
ND
ND
---
ND
16-Feb-16
1.0
100
ND
ND
ND
ND
ND
ND
ND
ND
9-Aug-16
1.0
100
ND
ND
ND
ND
ND
ND
---
ND
13-Feb-17
1.0
100
ND
ND
ND
ND
ND
ND
---
ND
22-Aug-17
1.0
100
ND
ND
ND
ND
ND
ND
---
ND
5-Feb-18
1.0
100
ND
ND
ND
ND
ND
ND
---
ND
13-Aug-18
1.0
100
ND
ND
ND
ND
ND
ND
---
ND
4-Feb-19
0.5
1
ND
ND
ND
ND
ND
ND
---
ND
14-Aug-19 for MW-6 >
7-Aug-19
0.54
1.0
N D
N D
N D
N D
N D
N D
---
N D
12-Feb-20
0.54
1.0
ND
ND
ND
ND
ND
ND
---
ND
27-Aug-20
0.54
1.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
0.54
1.0
ND
ND
ND
ND
ND
ND
---
ND
1,4-Dioxane (p-Dioxane)
13-Aug-18
1.9
10
ND
88.0
53.1
40.7
2.0 J
ND
---
ND
NC 2L = 3 pg/L (2017)
4-Feb-19
1.9
2
ND
132
49.6
49.8
ND
ND
ND
ND
14-Aug-19 for MW-6 >
7-Aug-19
1.2
2.0
N D
98.1
51.7
32.7
3.1
N D
---
N D
12-Feb-20
1.2
2.0
N D
98.2
44.4
36.0
N D
N D
---
N D
27-Aug-20
1.2
2.0
ND
113
50.0
39.3
3.0
ND
ND
ND
11-Feb-21
1.2
2.0
N D
118
53.1
40.6
1.8 J
N D
---
N D

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
1,1-Dichloroethane
1-Dec-97
---
5
ND
ND
1.0
ND
ND
ND
---
---
20-May-98
---
5
ND
ND
ND
ND
ND
ND
---
---
19-N ov-98
---
5
ND
ND
ND
ND
ND
ND
---
---
21-J u 1-99
---
5
N D
N D
N D
N D
N D
N D
---
---
16-N ov-99
---
5
N D
N D
N D
N D
N D
N D
---
---
10-May-00
---
5
N D
N D
N D
N D
N D
N D
---
---
26-Oct-00
---
5
N D
N D
N D
N D
N D
N D
---
---
18-A p r-01
---
5
N D
N D
N D
N D
N D
N D
---
---
27-Oct-01
---
5
N D
N D
N D
N D
N D
N D
---
---
13-Jun-02
---
5
ND
ND
ND
ND
ND
ND
---
---
19-N ov-02
---
5
N D
N D
N D
N D
N D
N D
---
---
27-Jun-03
---
5
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
5
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
5
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
5
ND
ND
ND
ND
ND
ND
---
ND
12-Jul-07
---
5
ND
ND
0.36 J
0.52 J
ND
ND
---
ND
NC 2L = 70 pg/L (10/23/07)
19-Dec-07
---
5
ND
ND
ND
0.57 J
ND
ND
ND
ND
8-Ju1-08
---
5
ND
ND
ND
0.60 J
ND
ND
---
ND
17-Dec-08
0.32
5.0
ND
ND
ND
0.51 J
ND
ND
---
ND
9-Jul-09
0.32
5.0
ND
ND
ND
0.84 J
ND
ND
ND
ND
16-Dec-09
0.32
5.0
ND
ND
ND
0.73 J
ND
ND
---
ND
NC 2L = 6 pg/L (02/05/10)
24-Jun-10
0.32
5.0
ND
ND
ND
0.53 J
ND
ND
---
ND
13-Dec-10
0.32
5.0
ND
ND
ND
0.60 J
ND
ND
---
ND
20-Jun-11
0.32
5.0
ND
ND
ND
0.63 J
ND
ND
---
ND
5-Dec-11
0.32
5.0
ND
ND
ND
0.67 J
ND
ND
---
ND
11-Jun-12
0.32
5.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
0.32
5.0
ND
ND
ND
0.61 J
ND
ND
---
ND
1-May-13
0.32
5.0
ND
ND
ND
0.62 J
ND
ND
ND
ND
8-May-13
0.32
5.0
ND
ND
ND
0.53 J
ND
ND
---
ND
24-Feb-14
0.32
5.0
ND
ND
ND
0.50 J
ND
ND
ND
ND
12-Aug-14
0.32
5.0
ND
ND
ND
0.47 J
ND
ND
ND
ND
10-Mar-15
0.32
5.0
ND
ND
ND
0.50 J
ND
ND
ND
ND
18-Aug-15
0.32
5.0
ND
ND
ND
0.49 J
ND
ND
---
ND
16-Feb-16
0.32
5.0
ND
ND
ND
0.45 J
ND
ND
ND
ND
9-Aug-16
0.32
5.0
ND
ND
ND
0.34 J
ND
ND
---
ND
13-Feb-17
0.32
5.0
ND
ND
ND
0.33 J
ND
ND
---
ND
22-Aug-17
0.32
5.0
ND
ND
ND
0.37 J
ND
ND
---
ND
5-Feb-18
0.32
5.0
ND
ND
ND
0.38 J
ND
ND
---
ND
13-Aug-18
0.32
5.0
ND
ND
ND
0.37 J
ND
ND
---
ND
4-Feb-19
0.27
1.0
ND
ND
ND
0.36 J
ND
ND
---
ND
14-Aug-19 for MW-6 >
7-Aug-19
0.27
1.0
ND
ND
ND
ND
ND
ND
---
ND
12-Feb-20
0.27
1.0
ND
ND
ND
0.33 J
ND
ND
---
ND
27-Aug-20
0.27
1.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
0.27
1.0
ND
ND
ND
ND
ND
ND
---
ND
1,2-Dichloroethane
17-Dec-08
0.12
1.0
ND
ND
0.15 J
ND
ND
ND
---
ND
NC 2L = 0.38 pg/L (10/23/07)
9-Jul-09
0.12
1.0
ND
ND
ND
ND
ND
ND
ND
0.19 J
16-Dec-09
0.12
1.0
ND
ND
0.14 J
ND
ND
ND
---
ND
NC 2L = 0.4 pg/L (02/05/10)
24-Jun-10
0.12
1.0
ND
ND
ND
ND
ND
ND
---
ND
13-Dec-10
0.12
1.0
ND
ND
ND
ND
ND
ND
---
ND
20-Jun-11
0.12
1.0
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
0.12
1.0
ND
ND
ND
ND
0.18 J
ND
---
ND
11-Jun-12
0.12
1.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
0.12
1.0
ND
ND
ND
ND
-0.20 J
ND
---
0.20 (ND) J
1-May-13
0.12
1.0
ND
ND
ND
ND
ND
ND
ND
ND
5-Aug-13
0.12
1.0
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
0.12
1.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
0.12
1.0
ND
ND
ND
ND
ND
ND
ND
ND
10-Mar-15
0.12
1.0
ND
ND
ND
ND
ND
ND
ND
ND
18-Aug-15
0.24
1.0
ND
ND
0.33 J
0.29 J
0.36 J
ND
---
---
16-Feb-16
0.24
1.0
ND
ND
ND
ND
ND
ND
ND
ND
9-Aug-16
0.24
1.0
ND
ND
ND
ND
ND
ND
---
ND
13-Feb-17
0.24
1.0
ND
ND
ND
ND
ND
ND
---
ND
22-Aug-17
0.24
1.0
ND
ND
ND
ND
ND
ND
---
ND
5-Feb-18
0.24
1.0
0.25 J
ND
0.37 J
ND
0.43 J
ND
---
ND
13-Aug-18
0.24
1.0
ND
ND
ND
ND
ND
ND
---
ND
4-Feb-19
0.34
1.0
ND
ND
ND
ND
ND
ND
---
ND
14-Aug-19 for MW-6 >
7-Aug-19
0.34
1.0
N D
N D
N D
ND
N D
N D
---
N D
12-Feb-20
0.34
1.0
ND
ND
ND
ND
ND
ND
---
ND
27-Aug-20
0.34
1.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
0.34
1.0
ND
ND
ND
ND
ND
ND
---
ND
Ethylbenzene
17-Dec-08
0.30
1.0
ND
0.31 J
ND
ND
ND
ND
---
ND
NC 2L = 550 pg/L (10/23/07)
9-Jul-09
0.30
1.0
ND
ND
ND
ND
ND
ND
ND
ND
16-Dec-09
0.30
1.0
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = 600 pg/L (02/05/10)
24-Jun-10
0.30
1.0
ND
ND
ND
ND
ND
ND
---
ND
13-Dec-10
0.30
1.0
ND
ND
ND
ND
ND
ND
---
ND
20-Jun-11
0.30
1.0
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
0.30
1.0
ND
ND
ND
ND
ND
ND
---
ND
11-Jun-12
0.30
1.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
0.30
1.0
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
0.30
1.0
ND
ND
ND
ND
ND
ND
ND
ND
5-Aug-13
0.30
1.0
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
0.30
1.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
0.30
1.0
ND
ND
ND
ND
ND
ND
ND
ND
10-Mar-15
0.30
1.0
ND
ND
ND
ND
ND
ND
ND
ND
18-Aug-15
0.30
1.0
ND
ND
ND
ND
ND
ND
---
ND
16-Feb-16
0.30
1.0
ND
ND
ND
ND
ND
ND
ND
ND
9-Aug-16
0.30
1.0
ND
ND
ND
ND
ND
ND
---
ND
13-Feb-17
0.30
1.0
ND
ND
ND
ND
ND
ND
---
ND
22-Aug-17
0.30
1.0
ND
ND
ND
ND
ND
ND
---
ND
5-Feb-18
0.30
1.0
ND
ND
ND
ND
ND
ND
---
ND
13-Aug-18
0.30
1.0
ND
ND
ND
ND
ND
ND
---
ND
4-Feb-19
0.26
1.0
ND
ND
ND
ND
ND
ND
---
ND
14-Aug-19 for MW-6 >
7-Aug-19
0.26
1.0
ND
ND
ND
ND
ND
ND
---
ND
12-Feb-20
0.26
1.0
ND
ND
ND
ND
ND
ND
---
ND
27-Aug-20
0.26
1.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
0.26
1.0
ND
ND
ND
ND
ND
ND
---
ND

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
Isobutanol
24-Jun-10
35.0
100
ND
59.0 J
ND
ND
ND
ND
---
ND
NC 2 L = NE p g/ L (02/05/10)
13-Dec-10
---
---
---
---
---
---
---
---
---
---
20-Jun-11
35.0
100
ND
39.5 J
ND
ND
ND
ND
---
ND
5-Dec-11
---
---
---
---
---
---
---
---
---
---
11-Jun-12
35.0
100.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
---
---
---
---
---
---
---
---
---
---
1-May-13
35.0
100
ND
ND
ND
ND
ND
ND
---
ND
5-Aug-13
---
---
---
---
---
---
---
---
---
---
24-Feb-14
35.0
100
ND
ND
ND
ND
ND
ND
---
ND
12-Aug-14
35.0
100
ND
ND
ND
ND
ND
ND
---
ND
10-Mar-15
35.0
100
ND
ND
ND
---
---
---
---
ND
16-Feb-16
35.0
100
N D
42.5 J
ND
---
---
---
---
ND
13-Feb-17
35.0
100
N D
ND
ND
---
---
---
---
ND
22-Aug-17
35.0
100
ND
ND
ND
---
---
---
---
ND
5-Feb-18
35.0
100
ND
ND
ND
---
---
---
---
ND
4-Feb-19
66.4
100
ND
ND
ND
---
---
---
---
ND
11-Feb-21
66.4
100
ND
ND
ND
---
---
---
---
---
Methylene Chloride
9-Jul-09
0.97
2.0
ND
ND
ND
ND
ND
ND
ND
9.6
NC 2L = 4.3 pg/L (10/23/07)
16-Dec-09
0.97
2.0
ND
ND
ND
ND
ND
ND
---
ND
24-Jun-10
0.97
1.0
ND
19.0
ND
ND
ND
ND
---
ND
Resample >
12-Aug-10
0.97
1.0
---
ND
---
---
---
---
---
ND
NC 2L = 5 pg/L (02/05/10)
13-Dec-10
0.97
1.0
ND
ND
ND
ND
ND
ND
---
ND
20-Jun-11
0.97
1.0
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
0.97
1.0
ND
ND
ND
ND
ND
ND
---
ND
11-Jun-12
0.97
1.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
0.97
1.0
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
0.97
1.0
ND
ND
ND
ND
ND
ND
ND
ND
5-Aug-13
0.97
1.0
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
0.97
1.0
1.0
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
0.97
1.0
ND
ND
ND
ND
ND
ND
ND
ND
10-Mar-15
0.97
1.0
ND
ND
ND
ND
ND
ND
ND
ND
18-Aug-15
0.97
1.0
1.3
1.1
1.6
ND
ND
ND
ND
ND
16-Feb-16
0.97
1.0
ND
ND
ND
ND
ND
ND
ND
ND
9-Aug-16
0.97
1.0
ND
ND
1.0 B
ND
ND
ND
---
2.2 B
13-Feb-17
0.97
1.0
ND
ND
ND
ND
ND
ND
---
ND
22-Aug-17
0.97
1.0
ND
ND
ND
ND
ND
ND
---
1.4 C
5-Feb-18
0.97
1.0
ND
ND
ND
ND
ND
ND
---
ND
13-Aug-18
0.97
1.0
ND
ND
ND
ND
ND
ND
---
6.6
4-Feb-19
3.70
5.0
ND
ND
ND
ND
ND
ND
---
ND
14-Aug-19 for MW-6 >
7-Aug-19
3.7
5.0
ND
ND
ND
N D
ND
N D
---
ND
12-Feb-20
3.7
5.0
ND
ND
ND
ND
ND
ND
---
ND
27-Aug-20
3.7
5.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
3.7
5.0
ND
ND
ND
ND
ND
ND
---
ND
Naphthalene
8-Ju1-08
---
10
ND
3.8 J
ND
ND
ND
ND
---
ND
NC 2 L = 21 p g/ L (10/ 2 3/ 0 7)
17-Dec-08
---
---
---
---
---
---
---
---
---
---
9-Jul-09
0.24
10.0
ND
2.4 J
ND
ND
ND
ND
---
ND
16-Dec-09
---
---
---
---
---
---
---
---
---
---
NC 2L = 6 pg/L (02/05/10)
24-Jun-10
0.24
10.0
ND
7.4 J
ND
ND
ND
ND
---
ND
13-Dec-10
---
---
---
---
---
---
---
---
---
---
20-Jun-11
0.24
10.0
ND
4.6 J
ND
ND
ND
ND
---
0.39 J
5-Dec-11
---
---
---
---
---
---
---
---
---
---
11-Jun-12
0.2
10.0
ND
4.6 J
ND
ND
ND
ND
ND
ND
12-Dec-12
---
---
---
---
---
---
1-May-13
0.24
10.0
ND
5.1 J
ND
ND
ND
ND
---
ND
5-Aug-
---
---
---
---
---
---
24-Feb-14
0.24
10.0
ND
5.8 J
ND
ND
ND
ND
---
ND
12-Aug-14
---
---
---
---
---
---
---
---
---
---
10-M a r-15
0.2
10
ND
5.4 J
ND
---
---
---
---
ND
16-Feb-16
0.2
10
ND
5.7 J
ND
---
---
---
---
ND
13-Feb-17
0.2
10
ND
6.1 J
ND
---
---
---
---
ND
22-Aug-17
0.2
10
ND
7.0 J
0.45 J
---
---
---
---
ND
5-Feb-18
0.2
10
ND
5.7 J
ND
---
---
---
---
ND
4-Feb-19
0.4
1
ND
4.2
ND
---
---
---
---
ND
11-Feb-21
0.4
1
ND
3.7
ND
---
---
---
---
---

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
Toluene
20-May-98
---
5
ND
ND
8.1
ND
ND
ND
---
---
19-N ov-98
---
5
ND
ND
ND
N D
ND
ND
---
---
21-J u l-99
---
5
ND
ND
ND
N D
ND
ND
---
---
16-N ov-99
---
5
ND
ND
ND
N D
ND
ND
---
---
10-May-00
---
5
ND
ND
ND
N D
ND
ND
---
---
26-Oct-00
---
5
ND
ND
ND
N D
ND
ND
---
---
18-A p r-01
---
5
ND
ND
ND
N D
ND
ND
---
---
27-Oct-01
---
5
ND
ND
ND
N D
ND
ND
---
---
13-Jun-02
---
5
ND
ND
ND
ND
ND
ND
---
---
19-N ov-02
---
5
ND
ND
ND
N D
ND
ND
---
---
27-Jun-03
---
5
ND
ND
ND
ND
ND
ND
---
-
30-Dec-03
---
5
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
5
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
5
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
5
ND
ND
ND
ND
ND
ND
---
ND
12-Jul-07
---
1
ND
0.49 B
ND
ND
ND
ND
---
0.34 J
NC 2L = 1,000 pg/L (10/23/07)
19-Dec-07
---
1
ND
0.51 J
ND
ND
ND
ND
ND
ND
8-Ju1-08
---
1
ND
0.39 J
ND
ND
1.3
ND
---
ND
17-Dec-08
0.26
1.0
1.4
1.6
ND
ND
11.7
ND
---
ND
9-Jul-09
0.26
1.0
ND
0.46 J
ND
ND
ND
ND
ND
ND
16-Dec-09
0.26
1.0
ND
0.42 J
ND
ND
ND
ND
---
ND
NC 2L = 600 pg/L (02/05/10)
24-Jun-10
0.26
1.0
ND
ND
ND
ND
ND
ND
---
ND
13-Dec-10
0.26
1.0
ND
0.54 J
ND
ND
ND
ND
---
ND
20-Jun-11
0.26
1.0
ND
0.34 J
ND
ND
ND
ND
---
ND
5-Dec-11
0.26
1.0
ND
0.28 J
ND
ND
0.30 J
ND
---
ND
11-Jun-12
0.26
1.0
ND
0.28 J
ND
ND
ND
ND
ND
ND
12-Dec-12
0.26
1.0
ND
0.29 J
ND
ND
0.36 J
ND
---
ND
1-May-13
0.26
1.0
ND
ND
ND
ND
ND
ND
ND
ND
5-Aug-13
0.26
1.0
ND
0.29 J
ND
ND
ND
ND
---
ND
24-Feb-14
0.26
1.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
0.26
1.0
ND
ND
ND
ND
ND
ND
ND
ND
10-Mar-15
0.26
1.0
ND
ND
ND
ND
ND
ND
ND
ND
18-Aug-15
0.26
1.0
ND
ND
ND
ND
ND
ND
---
ND
16-Feb-16
0.26
1.0
ND
ND
ND
ND
ND
ND
ND
ND
9-Aug-16
0.26
1.0
ND
0.33 J
ND
ND
ND
ND
---
ND
13-Feb-17
0.26
1.0
ND
ND
ND
ND
ND
ND
---
ND
22-Aug-17
0.26
1.0
ND
ND
ND
ND
ND
ND
---
ND
5-Feb-18
0.26
1.0
ND
ND
ND
ND
ND
ND
---
ND
13-Aug-18
0.26
1.0
ND
ND
ND
ND
0.44 J
ND
---
ND
4-Feb-19
0.24
1.0
ND
ND
ND
ND
ND
ND
---
ND
14-Aug-19 for MW-6 >
7-Aug-19
0.24
1.0
ND
ND
ND
ND
ND
ND
---
ND
12-Feb-20
0.24
1.0
ND
ND
ND
ND
ND
ND
---
ND
27-Aug-20
0.24
1.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
0.24
1.0
ND
ND
ND
ND
ND
ND
---
ND

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
Vinyl Chloride
8-Sep-94
---
10
ND
ND
12.0
ND
ND
ND
---
---
1-Dec-94
---
10
ND
ND
13.0
ND
ND
ND
---
---
9-Feb-95
---
10
ND
ND
15.0
ND
ND
ND
---
---
2-M a r-95
---
10
ND
ND
14.0
N D
ND
ND
---
---
15-N ov-95
---
10
ND
ND
11.0
N D
ND
ND
---
---
28-May-96
---
10
ND
ND
ND
ND
ND
ND
---
---
22-Nov-96
---
10
ND
ND
ND
ND
ND
ND
---
---
17-Jun-97
---
10
ND
ND
ND
ND
ND
ND
---
---
1-Dec-97
---
10
ND
ND
7.0
4.0
ND
ND
---
---
20-May-98
---
10
ND
ND
ND
ND
ND
ND
---
---
19-N ov-98
---
10
ND
ND
ND
N D
ND
ND
---
---
21-J u l-99
---
10
ND
ND
ND
N D
ND
ND
---
---
16-N ov-99
---
10
ND
ND
ND
N D
ND
ND
---
---
10-May-00
---
10
ND
ND
ND
N D
ND
ND
---
---
26-Oct-00
---
10
ND
ND
ND
N D
ND
ND
---
---
18-A p r-01
---
10
ND
ND
ND
N D
ND
ND
---
---
27-Oct-01
---
10
ND
ND
ND
N D
ND
ND
---
---
13-Jun-02
---
10
ND
ND
ND
ND
ND
ND
---
---
19-N ov-02
---
10
ND
ND
ND
N D
ND
ND
---
---
27-Jun-03
---
10
ND
ND
ND
ND
ND
ND
---
---
30-Dec-03
---
10
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
10
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
5.5
ND
ND
0.98 J
ND
ND
ND
---
ND
Resample >
23-Feb-07
---
5.5
---
---
1.0
---
---
---
---
ND
12-Jul-07
---
1
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = 0.015 pg/L (10/23/07)
19-Dec-07
---
1
ND
ND
ND
ND
ND
ND
ND
ND
8-Ju1-08
---
1
ND
ND
0.76 J
ND
ND
ND
---
ND
17-Dec-08
0.62
1.0
ND
ND
0.76 J
ND
ND
ND
---
ND
9-Jul-09
0.62
1.0
ND
ND
0.99 J
ND
ND
ND
ND
ND
16-Dec-09
0.62
1.0
ND
ND
0.81 J
ND
ND
ND
---
ND
NC 2L = 0.03 pg/L (02/05/10)
24-Jun-10
0.62
1.0
ND
ND
0.77 J
ND
ND
ND
---
ND
13-Dec-10
0.62
1.0
ND
ND
ND
ND
ND
ND
---
ND
20-Jun-11
0.62
1.0
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
0.62
1.0
ND
ND
ND
ND
ND
ND
---
ND
11-Jun-12
0.62
1.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Dec-12
0.62
1.0
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
0.62
1.0
ND
ND
ND
ND
ND
ND
ND
ND
5-Aug-13
0.62
1.0
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
0.62
1.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
0.62
1.0
ND
ND
ND
ND
ND
ND
ND
ND
10-Mar-15
0.62
1.0
ND
ND
ND
ND
ND
ND
ND
ND
18-Aug-15
0.62
1.0
ND
ND
ND
ND
ND
ND
---
ND
16-Feb-16
0.62
1.0
ND
ND
ND
ND
ND
ND
ND
ND
9-Aug-16
0.62
1.0
ND
ND
ND
ND
ND
ND
---
ND
13-Feb-17
0.62
1.0
ND
ND
ND
ND
ND
ND
---
ND
22-Aug-17
0.62
1.0
ND
ND
ND
ND
ND
ND
---
ND
5-Feb-18
0.62
1.0
ND
ND
0.63 J
ND
ND
ND
---
ND
13-Aug-18
0.62
1.0
ND
ND
0.72 J
ND
ND
ND
---
ND
4-Feb-19
0.24
1.0
ND
ND
ND
ND
ND
ND
---
ND
14-Aug-19 for MW-6 >
7-Aug-19
0.24
1.0
ND
ND
1.1
N D
ND
ND
---
ND
Resample >
4-Sep-19
0.24
1.0
--
--
ND
--
--
--
---
ND
12-Feb-20
0.24
1.0
ND
ND
ND
ND
ND
ND
---
ND
27-Aug-20
0.24
1.0
ND
ND
1.1
ND
ND
ND
---
ND
Resample >
30-Sep-20
0.24
1.0
---
---
ND
---
---
---
---
ND
11-Feb-21
0.24
1.0
ND
ND
0.53 J
ND
ND
ND
---
ND
Xylene (Total)
29-Dec-06
---
5
ND
1.4
ND
ND
ND
ND
---
ND
12-Jul-07
---
4
ND
1.2 J
ND
ND
ND
ND
---
ND
INC 2L = 530 pg/L (10/23/07)
19-Dec-07
---
4
ND
2.0
ND
ND
ND
ND
ND
ND
8-Ju1-08
---
4
ND
1.1 J
ND
ND
ND
ND
---
ND
17-Dec-08
0.66
2.0
1.4 J
2.7
ND
ND
ND
ND
---
ND
9-Jul-09
0.66
2.0
ND
1.5 J
ND
ND
ND
ND
ND
ND
16-Dec-09
0.66
2.0
ND
2.2
ND
ND
ND
ND
---
ND
INC 2L = 500 pg/L (02/05/10)
24-Jun-10
0.66
2.0
ND
0.73 J
ND
ND
ND
ND
---
ND
13-Dec-10
0.66
2.0
ND
2.0
ND
ND
ND
ND
---
ND
20-Jun-11
0.66
2.0
ND
1.4 J
ND
ND
ND
ND
---
ND
5-Dec-11
0.66
2.0
ND
1.1 J
ND
ND
ND
ND
---
ND
11-Jun-12
0.66
2.0
ND
0.91 J
ND
ND
ND
ND
ND
ND
12-Dec-12
0.66
5.0
ND
0.97 J
ND
ND
ND
ND
---
ND
1-May-13
0.66
5.0
ND
0.68 J
ND
ND
ND
ND
ND
ND
5-Aug-13
0.66
5.0
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
0.66
5.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
0.66
5.0
ND
ND
ND
ND
ND
ND
ND
ND
10-Mar-15
0.66
5.0
ND
ND
ND
ND
ND
ND
ND
ND
18-Aug-15
0.66
5.0
ND
ND
ND
ND
ND
ND
---
ND
16-Feb-16
0.66
5.0
ND
ND
ND
ND
ND
ND
ND
ND
9-Aug-16
0.66
5.0
ND
ND
ND
ND
ND
ND
---
ND
13-Feb-17
0.66
5.0
ND
ND
ND
ND
ND
ND
---
ND
22-Aug-17
0.66
5.0
ND
ND
ND
ND
ND
ND
---
ND
5-Feb-18
0.66
5.0
ND
ND
ND
ND
ND
ND
---
ND
13-Aug-18
0.66
5.0
ND
ND
ND
ND
ND
ND
---
ND
4-Feb-19
0.63
1.0
ND
ND
ND
ND
ND
ND
---
ND
14-Aug-19 for MW-6 >
7-Aug-19
0.63
1.0
ND
ND
ND
N D
ND
ND
---
ND
12-Feb-20
0.63
1.0
ND
ND
ND
ND
ND
ND
---
ND
27-Aug-20
0.63
1.0
ND
ND
ND
ND
ND
ND
---
ND
11-Feb-21
0.63
1.0
ND
ND
ND
ND
ND
ND
---
ND
Bis(2-Ethylhexyl)phthalate
24-Feb-14
0.79
15.0
2.6 J
ND
ND
ND
ND
ND
ND
ND
INC 2L = 3 pg/L (2/5/10)
15-Apr-14
0.79
15.0
ND
ND
ND
ND
ND
ND
ND
ND
12-Aug-14
---
---
---
---
---
---
---
---
---
---
10-M a r-15
0.5
15.0
ND
ND
ND
---
---
---
---
ND
16-Feb-16
0.9
15.0
ND
ND
ND
---
---
---
---
ND
13-Feb-17
0.9
15.0
ND
ND
ND
---
---
---
---
ND
2 2-Aug-17
2.3
15.0
ND
ND
ND
---
---
---
---
ND
5-Feb-18
2.4
15.6
ND
ND
ND
---
---
---
---
ND
4-Feb-19
1.4
6.0
ND
ND
ND
---
---
---
---
ND
N-Nitroso-di-n-butylamine
24-Feb-14
7.5
10.0
ND
ND
ND
8.6 J
ND
ND
ND
ND
12-Aug-14
---
---
---
---
---
---
---
---
---
---
10-M a r-15
1.3
10
ND
ND
ND
---
---
---
---
ND
16-Feb-16
2.2
10
ND
ND
ND
---
---
---
---
ND
13-Feb-17
2.2
10
ND
ND
ND
---
---
---
---
ND
22-Aug-17
1.6
10
ND
ND
ND
---
---
---
---
ND
5-Feb-18
1.6
10
ND
ND
ND
---
---
---
---
ND
4-Feb-19
2.2
10
ND
ND
ND
---
---
---
---
ND

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
Benzo(g,h,i)perylene
20-Jun-11
0.4
10.0
ND
ND
ND
ND
ND
1.4 J
---
ND
NC 2 L = 200 p g/ L (2/ 5/ 10)
5-Dec-11
---
---
---
---
---
---
---
---
---
---
11-Jun-12
0.38
10.0
ND
ND
ND
ND
ND
ND
---
ND
12-Dec-12
---
---
---
---
---
---
---
---
---
---
1-May-13
0.38
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Aug-13
---
---
---
---
---
---
---
---
---
---
24-Feb-14
0.38
10.0
ND
ND
ND
ND
ND
ND
---
ND
12-Aug-14
---
---
---
---
---
---
---
---
---
---
10- M a r-15
0.5
10.0
ND
ND
ND
---
---
---
---
ND
16-Feb-16
0.4
10.0
ND
ND
ND
---
---
---
---
ND
13-Feb-17
0.4
10.0
ND
ND
ND
---
---
---
---
ND
22-Aug-17
2.1
10.0
ND
ND
ND
---
---
---
---
ND
5-Feb-18
2.2
10.4
ND
ND
ND
---
---
---
---
ND
4-Feb-19
1.8
10.0
ND
ND
ND
---
---
---
---
ND
Dibenz(a,h)anthracene
20-Jun-11
0.55
10.0
ND
ND
ND
ND
ND
1.5 J
---
ND
NC 2 L = 0.005 p g/ L (2/5/ 10)
5-Dec-11
---
---
---
---
---
---
---
---
---
---
11-Jun-12
0.55
10.0
ND
ND
ND
ND
ND
ND
---
ND
12-Dec-12
---
---
---
---
---
---
---
---
---
---
1-May-13
0.55
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Aug-
---
---
---
---
---
---
24-Feb-14
0.55
10.0
ND
ND
ND
ND
ND
ND
---
ND
12-Aug-14
---
---
---
---
---
---
---
---
---
---
10- M a r-15
0.5
10.0
ND
ND
ND
---
---
---
---
ND
16-Feb-16
0.6
10.0
ND
ND
ND
---
---
---
---
ND
13-Feb-17
0.6
10.0
ND
ND
ND
---
---
---
---
ND
22-Aug-17
2.0
10.0
ND
ND
ND
---
---
---
---
ND
5-Feb-18
2.1
10.4
ND
ND
ND
---
---
---
---
ND
4-Feb-19
1.9
10.0
ND
ND
ND
---
---
---
---
ND
Fluorene
24-Jun-10
3.8
12.2
ND
4.3 J
ND
ND
ND
ND
---
ND
Resample >
12-Aug-10
3.1
10.0
---
ND
---
---
---
---
---
ND
NC 2 L = 300 pg/ L (2/ 5/ 10)
13-Dec-10
---
---
---
---
---
---
---
---
---
---
20-Jun-11
0.2
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
---
---
---
---
---
---
---
---
---
---
11-Jun-12
0.21
10.0
ND
ND
ND
ND
ND
ND
---
ND
12-Dec-12
---
---
---
---
---
---
---
---
---
---
1-May-13
0.21
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Aug-13
---
---
---
---
---
---
---
---
---
---
24-Feb-14
0.21
10.0
ND
ND
ND
ND
ND
ND
---
ND
12-Aug-14
---
---
---
---
---
---
---
---
---
---
10-M a r-15
1.0
10.0
ND
ND
ND
---
---
---
---
ND
16-Feb-16
0.2
10.0
ND
ND
ND
---
---
---
---
ND
13-Feb-17
0.2
10.0
ND
ND
ND
---
---
---
---
ND
2 2-Aug-17
1.6
10.0
ND
ND
ND
---
---
---
---
ND
5-Feb-18
1.6
10.4
ND
ND
ND
---
---
---
---
ND
4-Feb-19
3.0
10.0
ND
ND
ND
---
---
---
---
ND
Indeno(1,2,3-cd)pyrene
20-Jun-11
0.29
10.0
ND
ND
ND
ND
ND
1.3 J
---
ND
NC 2 L = 0.05 p g/ L (2/5/ 10)
5-Dec-11
---
---
---
---
---
---
---
---
---
---
11-Jun-12
0.29
10.0
ND
ND
ND
ND
ND
ND
---
ND
12-Dec-12
---
---
---
---
---
---
---
---
---
---
1-May-13
0.29
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Aug-
---
---
---
---
---
---
24-Feb-14
0.29
10.0
ND
ND
ND
ND
ND
ND
---
ND
12-Aug-14
---
---
---
---
---
---
---
---
---
---
10-M a r-15
0.5
10.0
ND
ND
ND
---
---
---
---
ND
16-Feb-16
0.3
10.0
ND
ND
ND
---
---
---
---
ND
13-Feb-17
0.3
10.0
ND
ND
ND
---
---
---
---
ND
22-Aug-17
2.0
10.0
ND
ND
ND
---
---
---
---
ND
5-Feb-18
2.1
10.4
ND
ND
ND
---
---
---
---
ND
4-Feb-19
1.7
10.0
ND
ND
ND
---
---
---
---
ND
2-Methylnaphthalene
24-Jun-10
5.1
12.2
ND
38.9
ND
ND
ND
ND
---
ND
Resample>
12-Aug-10
4.2
10
---
ND
---
---
---
---
---
ND
NC 2L = 30 pg/L (02/05/10)
13-Dec-10
---
---
---
---
---
---
---
---
---
---
20-Jun-11
0.3
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
---
---
---
---
---
---
---
---
---
---
11-Jun-12
0.28
10.0
ND
ND
ND
ND
ND
ND
---
ND
12-Dec-12
---
---
---
---
---
---
---
---
---
---
1-May-13
0.28
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Aug-13
---
---
---
---
---
---
---
---
---
---
24-Feb-14
0.28
10.0
ND
ND
ND
ND
ND
ND
---
ND
12-Aug-14
---
---
---
---
---
---
---
---
---
---
10- M a r-15
1.0
10.0
ND
ND
ND
---
---
---
---
ND
16-Feb-16
0.3
10.0
ND
ND
ND
---
---
---
---
ND
13-Feb-17
0.3
10.0
ND
ND
ND
---
---
---
---
ND
22-Aug-17
1.4
10.0
ND
ND
ND
---
---
---
---
ND
5-Feb-18
1.5
10.4
ND
ND
ND
---
---
---
---
ND
4-Feb-19
2.8
10.0
ND
ND
ND
---
---
---
---
ND
Phorate
18-Apr-01
---
10
---
3.2
ND
ND
ND
---
---
---
27-Oct-01
---
5
ND
8.1
ND
ND
ND
ND
---
---
27-Oct-01
---
0.5
---
8.1
1.3
ND
ND
---
---
---
13-Jun-02
---
5
ND
ND
ND
ND
ND
ND
---
---
13-J u n-02
---
0.5
---
ND
ND
ND
ND
---
---
---
19-N ov-02
---
5
ND
ND
ND
ND
ND
ND
---
---
27-Jun-03
---
5
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
---
---
---
---
---
28-Jun-06
---
10
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
---
---
---
---
---
12-Jul-07
---
10
ND
ND
ND
ND
ND
ND
---
ND
NC 2 L = 1.4 p g/ L (10/23/07)
19-Dec-07
---
---
---
---
---
---
---
---
ND
---
8-Ju1-08
---
10
ND
ND
ND
ND
ND
ND
---
ND
17-Dec-08
---
---
---
---
---
---
---
---
---
---
9-Jul-09
6.6
22.2
ND
ND
ND
ND
ND
ND
---
ND
16-Dec-09
---
---
---
---
---
---
---
---
---
---
NC 2L = 1 pg/L (02/05/10)
24-Jun-10
6.5
24.1
ND
ND
ND
ND
ND
ND
---
ND
13-Dec-10
---
---
---
---
---
---
---
---
---
---
20-Jun-11
5.4
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
---
---
---
---
---
---
---
---
---
---
11-Jun-12
5.4
10.0
ND
ND
ND
ND
ND
ND
---
ND
12-Dec-12
---
---
---
---
---
---
---
---
---
---
1-May-13
5.4
10.0
ND
ND
ND
ND
ND
ND
---
ND
5-Aug-13
---
---
---
---
---
---
---
---
---
---
24-Feb-14
5.4
10.0
ND
ND
ND
ND
ND
ND
---
ND
12-Aug-14
---
---
---
---
---
---
---
---
---
---
10- M a r-15
0.8
10.0
ND
ND
ND
---
---
---
---
ND
16-Feb-16
1.1
10.0
ND
ND
ND
---
---
---
---
ND
13-Feb-17
1.1
10.0
ND
ND
ND
---
---
---
---
ND
2 2-Aug-17
1.7
10.0
ND
ND
ND
---
---
---
---
ND
5-Feb-18
1.8
10.4
ND
ND
ND
---
---
---
---
ND
4-Feb-19
1.1
10.0
ND
ND
ND
---
---
---
---
ND

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
Beta-BHC
11-Jun-12
0.050
0.050
ND
ND
0.16
ND
ND
ND
---
ND
NC 2L = 0.019 pg/L (10/23/07)
19-Jul-12
0.050
0.050
---
---
ND
---
---
---
---
---
12-Dec-12
---
---
---
---
---
---
---
---
---
---
1-May-13
0.050
0.050
ND
ND
ND
ND
ND
ND
---
ND
5-Aug-13
---
---
---
---
---
---
---
---
---
---
24-Fe b-14
0.050
0.050
ND
0.052
ND
ND
ND
ND
---
ND
Resample >
15-Apr-14
0.050
0.050
---
ND
---
---
---
---
---
ND
12-Aug-14
---
---
---
---
---
---
---
---
---
---
10-M a r-15
0.1
0.1
ND
ND
ND
---
---
---
---
ND
16-Feb-16
0.1
0.1
ND
ND
ND
---
---
---
---
ND
13-Feb-17
0.1
0.1
ND
ND
ND
---
---
---
---
ND
5-Feb-18
0.1
0.1
ND
ND
ND
---
---
---
---
ND
4-Feb-19
0.1
0.1
ND
ND
ND
---
---
---
---
ND
Delta-BHC
11-Jun-12
0.050
0.050
ND
ND
0.090
ND
ND
ND
---
ND
NC 2L = 0.019 pg/L (10/23/07)
19-Jul-12
0.050
0.050
---
---
ND
---
---
---
---
---
12-Dec-12
---
---
---
---
---
---
---
---
---
---
1-May-13
0.050
0.050
ND
ND
ND
ND
ND
ND
---
ND
5-Aug-13
---
---
---
---
---
---
---
---
---
---
24-Feb-14
0.050
0.050
ND
ND
ND
ND
ND
ND
---
ND
12-Aug-14
---
---
---
---
---
---
---
---
---
---
10-M a r-15
0.050
0.050
ND
ND
ND
---
---
---
---
ND
16-Feb-16
0.050
0.050
ND
ND
ND
---
---
---
---
ND
13-Feb-17
0.050
0.050
ND
ND
ND
---
---
---
---
ND
5-Feb-18
0.052
0.052
ND
ND
ND
---
---
---
---
ND
4-Feb-19
0.050
0.050
ND
ND
ND
---
---
---
---
ND
gamma-BHC (Lindane)
27-Jun-03
---
1.05
ND
0.085
ND
ND
ND
ND
---
ND
30-Dec-03
---
0.05
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
0.05
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
0.05
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
0.05
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
0.05
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
0.05
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
0.05
ND
ND
ND
ND
ND
ND
---
ND
12-Jul-07
---
0.05
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = 0.2 pg/L (10/23/07)
19-Dec-07
---
0.05
ND
ND
ND
ND
ND
ND
ND
ND
8-Ju1-08
---
0.50
ND
ND
ND
ND
ND
ND
---
ND
17-Dec-08
0.050
0.050
ND
ND
ND
ND
ND
ND
---
ND
9-Jul-09
0.050
0.050
ND
ND
ND
ND
ND
ND
---
ND
16-Dec-09
0.01
0.1
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = 0.03 pg/L (02/05/10)
24-Jun-10
0.00021
0.010
ND
ND
0.052
ND
ND
ND
---
ND
Resample >
12-Aug-10
0.00020
0.010
---
---
ND
---
---
---
---
ND
13-Dec-10
0.00020
0.050
ND
ND
0.013 J
ND
ND
ND
---
ND
20-Jun-11
0.00020
0.050
ND
ND
0.066
ND
ND
ND
---
ND
Resample >
28-Jul-11
0.00020
0.010
---
---
ND
---
---
---
---
ND
5-Dec-11
0.050
0.050
ND
ND
ND
ND
ND
ND
---
ND
11-Jun-12
0.050
0.050
ND
ND
ND
ND
ND
ND
---
ND
12-Dec-12
0.050
0.050
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
0.050
0.050
ND
ND
ND
ND
ND
ND
---
ND
5-Aug-13
0.050
0.050
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
0.050
0.050
ND
ND
ND
ND
ND
ND
---
ND
12-Aug-14
0.050
0.050
ND
ND
ND
---
---
---
---
ND
10-Mar-15
0.050
0.050
ND
ND
ND
---
---
---
---
ND
18-Aug-15
0.050
0.050
ND
ND
ND
---
---
---
---
ND
16-Feb-16
0.050
0.050
ND
ND
ND
---
---
---
---
ND
9-Aug-16
0.050
0.050
ND
ND
ND
---
---
---
---
ND
13-Feb-17
0.050
0.050
ND
ND
ND
---
---
---
---
ND
5-Feb-18
0.052
0.052
ND
ND
ND
---
---
---
---
ND
4-Feb-19
0.050
0.050
ND
ND
ND
---
---
---
---
ND
Heptachlor
27-Jun-03
---
1.05
ND
0.03
0.17
ND
ND
ND
---
ND
30-Dec-03
---
0.05
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
0.05
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
0.05
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
0.05
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
0.05
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
0.05
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
0.05
ND
ND
ND
ND
ND
ND
---
ND
12-Jul-07
---
0.05
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = 0.0078 pg/L (10/23/07)
19-Dec-07
---
0.05
ND
ND
ND
ND
ND
ND
ND
ND
8-Ju1-08
---
0.05
ND
ND
ND
ND
ND
ND
---
ND
17-Dec-08
0.050
0.050
ND
ND
ND
ND
ND
ND
---
ND
9-Ju1-09
0.050
0.050
ND
ND
ND
ND
ND
ND
---
ND
16-Dec-09
0.02
0.1
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = 0.008 pg/L (02/05/10)
24-Jun-10
0.0015
0.010
ND
ND
ND
ND
ND
ND
---
ND
13-Dec-10
0.0500
0.0015
ND
ND
ND
ND
ND
ND
---
ND
20-Jun-11
0.050
0.0015
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
0.050
0.056
ND
0.062
ND
ND
ND
ND
---
ND
Resample >
25-Jan-12
0.050
0.0500
---
ND
---
---
---
---
---
ND
11-Jun-12
0.050
0.050
ND
ND
ND
ND
ND
ND
---
ND
12-Dec-12
0.050
0.050
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
0.050
0.050
ND
ND
ND
ND
ND
ND
---
ND
5-Aug-13
0.050
0.050
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
0.050
0.050
ND
ND
ND
ND
ND
ND
---
ND
12-Aug-14
0.050
0.050
ND
ND
ND
---
---
---
---
ND
10-Mar-15
0.050
0.050
ND
ND
ND
---
---
---
---
ND
18-Aug-15
0.050
0.050
ND
ND
ND
---
---
---
---
ND
16-Feb-16
0.050
0.050
ND
ND
ND
---
---
---
---
ND
9-Aug-16
0.050
0.050
ND
ND
ND
---
---
---
---
ND
13-Feb-17
0.050
0.050
ND
ND
ND
---
---
---
---
ND
5-Feb-18
0.052
0.052
ND
ND
ND
---
---
---
---
ND
4-Feb-19
0.050
0.050
ND
ND
ND
---
---
---
---
ND

Analyte
Sample Date
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Blanks
2,4-D
27-Jun-03
---
3
---
5.9
ND
ND
ND
---
---
---
30-Dec-03
---
2
ND
ND
ND
ND
ND
ND
---
ND
30-Jun-04
---
2
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-04
---
2
ND
ND
ND
ND
ND
ND
---
ND
29-Jun-05
---
2
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-05
---
2
ND
ND
ND
ND
ND
ND
---
ND
28-Jun-06
---
2
ND
ND
ND
ND
ND
ND
---
ND
29-Dec-06
---
2
ND
ND
ND
ND
ND
ND
---
ND
12-Jul-07
---
2
ND
ND
ND
ND
ND
ND
---
ND
NC 2L = 70 pg/L (10/23/07)
19-Dec-07
---
2
ND
ND
ND
ND
ND
ND
ND
ND
8-Apr-08
---
2
ND
ND
ND
ND
ND
ND
---
ND
17-Dec-08
---
2.0
ND
ND
ND
ND
ND
ND
---
ND
9-Ju1-09
---
2.0
ND
ND
ND
ND
ND
ND
---
ND
16-Dec-09
0.11
5.0
ND
ND
ND
ND
ND
ND
---
ND
24-Jun-10
0.23
2.1
ND
ND
ND
ND
ND
ND
---
ND
10-Dec-10
0.22
2.0
ND
ND
ND
ND
ND
ND
---
ND
20-Jun-11
0.22
2.0
ND
ND
ND
ND
ND
ND
---
ND
5-Dec-11
0.22
2.0
ND
ND
ND
ND
ND
ND
---
ND
11-Jun-12
0.22
2.0
ND
ND
ND
ND
ND
ND
---
ND
12-Dec-12
0.22
2.0
ND
ND
ND
ND
ND
ND
---
ND
1-May-13
0.22
2.0
ND
ND
ND
ND
ND
ND
---
ND
5-Aug-13
0.22
2.0
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
0.22
2.0
ND
ND
ND
ND
ND
ND
---
ND
12-Aug-14
0.22
2.0
N D
N D
N D
---
---
---
---
N D
10-Mar-15
0.24
2.1
N D
N D
N D
---
---
---
---
N D
18-Aug-15
0.24
2.1
N D
N D
N D
---
---
---
---
N D
16-Feb-16
0.23
1.0
N D
N D
N D
---
---
---
---
N D
9-Aug-16
0.24
1.0
N D
N D
N D
---
---
---
---
N D
13-Feb-17
0.22
0.9
N D
N D
N D
---
---
---
---
N D
22-Aug-17
0.24
1.0
N D
N D
N D
---
---
---
---
N D
5-Feb-18
0.24
1.0
N D
N D
N D
---
---
---
---
N D
4-Feb-19
1.60
5.0
N D
N D
N D
---
---
---
---
N D
4,4'-DDD
11-Jun-12
0.05
0.05
ND
ND
0.13
ND
ND
ND
---
ND
Resample>
19-Jul-12
0.05
0.10
---
---
ND
---
---
---
---
---
NC 2L = 0.1 p g/ L (2/5/ 10)
12-Dec-12
---
---
---
---
---
---
---
---
---
---
1-May-13
0.050
0.10
ND
ND
ND
ND
ND
ND
---
ND
5-Aug-13
---
---
---
---
---
---
---
---
---
---
24-Feb-14
0.050
0.10
ND
ND
ND
ND
ND
ND
---
ND
12-Aug-14
---
---
---
---
---
---
---
---
---
---
10-Ma r-15
0.050
0.10
N D
ND
ND
---
---
---
---
ND
16-Feb-16
0.050
0.10
ND
ND
ND
---
---
---
---
ND
13-Feb-17
0.050
0.10
N D
ND
ND
---
---
---
---
ND
5-Feb-18
0.052
0.10
N D
ND
ND
---
---
---
---
ND
4-Feb-19
0.050
0.05
N D
ND
ND
---
---
---
---
ND
4,4'-DDT
11-Jun-12
0.05
0.05
ND
ND
0.10
ND
ND
ND
---
ND
Resample>
19-Jul-12
0.05
0.10
---
---
0.063 J
---
---
---
---
---
NC 2L = 0.1 p g/ L (2/5/ 10)
12-Dec-12
---
---
---
---
---
---
---
---
---
---
1-May-13
0.050
0.10
ND
ND
ND
ND
ND
ND
---
ND
5-Aug-13
---
---
---
---
---
---
---
---
---
---
24-Feb-14
0.050
0.10
ND
ND
ND
ND
ND
ND
---
ND
12-Aug-14
---
---
---
---
---
---
---
---
---
---
10-M a r-15
0.050
0.10
ND
ND
ND
---
---
---
---
ND
16-Feb-16
0.050
0.10
ND
ND
ND
---
---
---
---
ND
13-Feb-17
0.050
0.10
ND
ND
ND
---
---
---
---
ND
5-Feb-18
0.052
0.10
ND
ND
ND
---
---
---
---
ND
4-Feb-19
0.050
0.05
ND
ND
ND
---
---
---
---
ND
Dinoseb
10-Mar-15
0.061
1.1
ND
ND
0.11 J
---
---
---
---
ND
16-Feb-16
0.058
0.19
ND
ND
ND
---
---
---
---
ND
13-Feb-17
0.057
0.19
ND
ND
ND
---
---
---
---
ND
22-Aug-17
0.062
0.20
ND
ND
ND
---
---
---
---
ND
5-Feb-18
0.061
0.20
ND
ND
ND
---
---
---
---
ND
4-Feb-19
1.200
5.00
ND
ND
ND
---
---
---
---
ND
Endrin aldehyde
11-Jun-12
0.050
0.050
ND
ND
0.14
ND
ND
ND
---
---
NC 2L= 2 (2/5/10)
12-Dec-12
0.050
0.10
ND
ND
ND
ND
ND
ND
---
---
1-May-13
0.050
0.10
ND
ND
ND
ND
ND
ND
---
ND
5-Aug-13
0.050
0.10
ND
ND
ND
ND
ND
ND
---
ND
24-Feb-14
0.050
0.10
ND
ND
ND
ND
ND
ND
---
ND
12-Aug-14
0.050
0.10
N D
ND
N D
---
---
---
---
ND
10-Mar-15
0.050
0.10
N D
ND
N D
---
---
---
---
ND
18-Aug-15
0.050
0.10
N D
ND
N D
---
---
---
---
ND
16-Feb-16
0.050
0.10
N D
ND
N D
---
---
---
---
ND
9-Aug-16
0.050
0.10
N D
ND
N D
---
---
---
---
ND
13-Feb-17
0.050
0.10
N D
ND
N D
---
---
---
---
ND
5-Feb-18
0.052
0.10
ND
ND
N D
---
---
---
---
ND
4-Feb-19
0.050
0.05
ND
ND
N D
---
---
---
---
ND
Diethyl phthalate
4-Feb-19
2.00
10.00
ND
7.1 J
ND
---
---
---
---
ND
Endosulfan I
4-Feb-19
0.05
0.05
---
0.078
0.19
---
---
---
---
---
Dichlorodifluoromethane
5-Feb-18
0.21
5.0
ND
0.36 J
ND
---
---
---
---
ND
4-Feb-19
0.23
1.0
ND
ND
ND
---
---
---
---
ND
11-Feb-21
0.23
1.0
ND
ND
ND
---
---
---
---
---
Notes:
All concentrations are in micrograms per liter (pg/L).
RL = Reporting Limit (SWSL for December 2006 - present).
DL = Laboratory detection limit.
J = Estimated value between the DL and the RL.
B = Blank -qualified data; result is expected to be biased high based on concentrations in the blanks.
ND = Not detected above laboratory reporting limit.
NC 2L = North Carolina Groundwater Standards from 15A NCAC 2L.0202.
IMAC = Interim Maximum Allowable Concetration (for constituents with no NC2L).
Bold values for groundwater are above the NC 2L Standards or IMAC.
--- = Well was not monitored and/or not reported.

Appendix E
Historical Constituents in Surface Water
(from LaBella, 2021)

Analytes
Sample Date
EPA Method
DL
RL
SW-1
SW-2
Blanks
INORGANICS
Arsenic
06/24/10
2.7
10.00
4.30 J
2.90 J
ND
NC2B = 10 pg/L (03/28/08)
12/13/10
2.7
10.0
ND
ND
ND
06/20/11
5.0
10.0
ND
ND
ND
12/05/11
5.0
10.0
ND
ND
ND
06/11/12
5.0
10.0
ND
ND
ND
12/12/12
5.0
10.0
ND
ND
ND
05/01/13
5.0
10.0
ND
ND
ND
08/05/13
5.0
10.0
ND
ND
ND
02/24/14
5.0
10.0
ND
ND
ND
08/12/14
EPA 6010
5.0
10.0
---
ND
ND
03/10/15
EPA 6010
2.5
10.0
ND
ND
3.0 J
08/18/15
---
---
Dry
Dry
---
02/16/16
EPA 6010
2.5
10.0
ND
ND
ND
08/09/16
EPA 6010
2.5
10.0
3.10 B
ND
5.1 J
02/13/17
EPA 6010
5.0
10.0
ND
ND
ND
08/22/17
EPA 6010
5.0
10.0
ND
ND
ND
02/05/18
EPA 6010
5.0
10.0
ND
ND
ND
08/13/18
EPA 6010D
5.0
10.0
ND
ND
ND
02/04/19
EPA 6010D
5.0
10.0
ND
ND
---
08/07/19
EPA 6010D
4.7
10.0
ND
ND
ND
02/12/20
EPA 6010D
4.7
10.0
ND
ND
ND
08/27/20
---
---
Dry
Dry
---
02/11/21
EPA 6010D
4.7
10.0
---
ND
---
Barium
11/22/96
---
500
37.0
37.0
---
06/17/97
---
500
37.0
62.0
---
12/01/97
---
500
53.0
45.0
---
05/20/98
---
500
24.0
69.0
---
11/19/98
---
500
ND
100.0
---
07/21/99
---
500
ND
ND
---
11/16/99
---
500
ND
ND
---
05/10/00
---
500
ND
ND
---
10/26/00
---
500
ND
ND
---
04/18/01
---
500
ND
ND
---
10/27/01
---
500
ND
ND
---
06/13/02
---
500
---
---
---
11/19/02
---
500
ND
ND
---
06/27/03
---
500
ND
ND
---
12/30/03
---
500
ND
ND
ND
06/30/04
---
500
ND
ND
ND
12/29/04
---
500
ND
ND
ND
12/29/04
---
500
ND
ND
ND
06/29/05
---
500
ND
ND
ND
12/29/05
---
500
ND
ND
ND
06/28/06
---
500
ND
ND
ND
12/29/06
---
100
37.5
40.6
0.20 J
07/12/07
---
100
33.3 J
---
ND
12/19/07
---
100
52.6 B
149.0
11.7
07/08/08
---
100
33.8 J
161.0
0.3 J
12/17/08
0.2
100
30.2 B
33.5 B
10.7 J
07/09/09
0.2
100
36.8 B
78.4 B
17.6 J
12/16/09
0.2
100
31.2 B
36.2 B
17.1 J
06/24/10
0.2
100
34.5 B
71.3 B
27.3 J
12/13/10
0.2
100
36.1 B
91.0 J
12.1 J
06/20/11
5.0
100
40.3 J
93.0 J
ND
12/05/11
5.0
100
32.9 J
59.0 J
ND
06/11/12
5.0
100
40.0 J
95.6 J
ND
12/12/12
5.0
100
45.0 J
97.8 J
ND
05/01/13
5.0
100
32.7 J
43.1 J
ND
08/05/13
5.0
100
49.9 J
79.8 J
ND
02/24/14
5.0
100
29.0 J
30.4 J
ND
08/12/14
EPA 6010
5.0
100
---
121
ND
03/10/15
EPA 6010
2.5
100
29.0 J
32.1 J
ND
08/18/15
---
---
Dry
Dry
---
02/16/16
EPA 6010
2.5
100
33.1 J
33.5 J
ND
08/09/16
EPA 6010
2.5
100
43.3 J
105
ND
02/13/17
EPA 6010
2.5
100
45.3 J
60.4 J
ND
08/22/17
EPA 6010
2.5
100
39.7 J
88.7 J
ND
02/05/18
EPA 6010
2.5
100
32.5 J
29.1 J
ND
08/13/18
EPA 6010D
2.5
100
70.0 J
86.6 J
ND
02/04/19
EPA 6010D
2.5
5
29.1
33.1
---
ISTV = 21,000 pg/L
08/07/19
EPA 6010D
1.0
5.0
70.0
94.4
ND
02/12/20
EPA 6010D
1.0
5.0
27.6
30.3
ND
08/27/20
---
---
Dry
Dry
---
02/11/21
EPA 6010D
3.5
5.0
---
31.20
---

Analytes
Sample Date
EPA Method
DL
RL
SW-1
SW-2
Blanks
Beryllium
07/08/08
---
1.0
0.32 J
ND
ND
12/17/08
0.1
1.0
ND
ND
ND
07/09/09
0.1
1.0
ND
ND
ND
12/16/09
0.1
1.0
0.12 J
ND
ND
NC2B = 6.5 pg/L (02/05/10)
06/24/10
0.1
1.0
ND
ND
ND
12/13/10
0.1
1.0
ND
ND
ND
06/20/11
1.0
1.0
ND
ND
ND
12/05/11
1.0
1.0
ND
ND
ND
06/11/12
1.0
1.0
ND
ND
ND
12/12/12
1.0
1.0
ND
ND
ND
05/01/13
1.0
1.0
ND
ND
ND
08/05/13
1.0
1.0
ND
ND
ND
02/24/14
1.0
1.0
ND
ND
ND
08/12/14
EPA 6010
1.0
1.0
---
ND
ND
03/10/15
EPA 6010
0.50
1.0
ND
ND
ND
08/18/15
---
---
Dry
Dry
---
02/16/16
EPA 6010
0.50
1.0
ND
ND
ND
08/09/16
EPA 6010
0.50
1.0
ND
ND
ND
02/13/17
EPA 6010
0.50
1.0
ND
ND
ND
08/22/17
EPA 6010
0.50
1.0
ND
ND
ND
NC213 = Hardness Dependant
02/05/18
EPA 6010
0.50
1.0
ND
ND
ND
08/13/18
EPA 6010D
0.50
1.0
ND
ND
ND
02/04/19
EPA 6010D
0.50
1.0
ND
ND
---
08/07/19
EPA 6010D
0.20
1.0
ND
ND
ND
02/12/20
EPA 6010D
0.20
1.0
0.21 J
0.25 J
ND
08/27/20
---
---
Dry
Dry
---
02/11/21
EPA 6010D
0.7
1.0
---
ND
---
Chromium
06/17/97
---
10.0
ND
3.00
---
12/01/97
---
10.0
ND
ND
---
05/20/98
---
10.0
ND
ND
---
11/19/98
---
10.0
ND
ND
---
07/21/99
---
10.0
ND
ND
---
11/ 16/99
---
10.0
ND
ND
---
05/ 10/00
---
10.0
ND
ND
---
10/26/00
---
10.0
ND
ND
---
04/ 18/ 01
---
10.0
ND
ND
---
10/27/01
---
10.0
ND
ND
---
06/13/02
---
10.0
---
---
---
11/19/02
---
10.0
ND
ND
---
06/27/03
---
10.0
ND
ND
---
12/30/03
---
10.0
ND
ND
ND
06/30/04
---
10.0
ND
ND
ND
12/29/04
---
10.0
ND
ND
ND
06/29/05
---
10.0
ND
ND
ND
12/29/05
---
10.0
ND
ND
ND
06/28/06
---
10.0
ND
ND
ND
12/29/06
---
10.0
ND
ND
ND
07/12/07
---
10.0
ND
---
ND
12/19/07
---
10.0
2.20 B
2.60 B
1.40 J
NC2B = 50 pg/L (03/28/08)
07/08/08
---
10.0
2.50 J
2.20 J
ND
12/17/08
0.4
10.0
1.40 J
2.60 J
ND
07/09/09
0.4
10.0
2.6 J
1.2 J
ND
12/16/09
0.4
10.0
4.1 J
3.4 J
ND
06/24/10
0.4
10.0
3.3 B
7.3 J
0.71 J
12/13/10
0.4
10.0
1.4 J
1.5 J
ND
06/20/11
5.0
10.0
ND
ND
ND
12/05/11
5.0
10.0
ND
ND
ND
06/11/12
5.0
10.0
ND
7.2 J
ND
12/12/12
5.0
10.0
ND
8.2 J
ND
05/01/13
5.0
10.0
5.7 J
ND
ND
08/05/13
5.0
10.0
ND
ND
ND
02/24/14
5.0
10.0
ND
ND
ND
08/12/14
EPA 6010
5.0
10.0
---
ND
ND
03/10/15
EPA 6010
2.5
10.0
4.4 J
3.6 J
ND
08/18/15
---
---
Dry
Dry
---
02/16/16
EPA 6010
2.5
10.0
4.6 J
6.8 J
ND
08/09/16
EPA 6010
2.5
10.0
ND
ND
2.90 J
02/13/17
EPA 6010
2.5
10.0
ND
ND
ND
08/22/17
EPA 6010
2.5
10.0
ND
ND
ND
02/05/18
EPA 6010
2.5
10.0
6.9 J
7.9 J
ND
NC2B = Hardness Dependant
08/13/18
EPA 6010D
2.5
10.0
5.9 J
ND
ND
02/04/19
EPA 6010D
2.5
5.0
ND
ND
---
08/07/19
EPA 6010D
1.0
5.0
ND
ND
ND
02/12/20
EPA 6010D
1.0
5.0
5.3
4.7 J
ND
08/27/20
---
---
Dry
Dry
---
02/11/21
EPA 6010D
3.7
5.0
---
4.00 1
---

Analytes
Sample Date
EPA Method
DL
RL
SW-1
SW-2
Blanks
Cobalt
05/20/98
---
10
2.0
2.0
---
11/19/98
---
10
ND
3.0
---
07/21/99
---
10
ND
ND
---
11/ 16/99
---
10
ND
ND
---
05/ 10/00
---
10
ND
ND
---
10/26/00
---
10
ND
ND
---
04/18/01
---
10
ND
ND
---
10/27/01
---
10.0
ND
22.0
---
06/13/02
---
10.0
---
---
---
11/19/02
---
10.0
ND
ND
---
06/27/03
---
10.0
ND
10.0
---
12/30/03
---
10.0
ND
ND
ND
06/30/04
---
10.0
ND
ND
ND
12/29/04
---
10.0
ND
ND
ND
06/29/05
---
10.0
ND
ND
ND
12/29/05
---
10.0
ND
ND
ND
06/28/06
---
10.0
ND
ND
ND
12/29/06
---
10.0
ND
ND
ND
07/12/07
---
10.0
ND
---
ND
12/19/07
---
10.0
4.2 B
1.20 B
1.8 J
07/08/08
---
10.0
4.80 B
10.5 B
6.20 J
12/17/08
0.6
10.0
1.70 B
1.1 B
2.50 J
07/09/09
0.6
10.0
ND
ND
ND
12/16/09
0.6
10.0
ND
1.0 J
ND
NC2B = NE pg/L (03/24/10)
06/24/10
0.6
10.0
ND
ND
ND
12/13/10
0.6
10.0
{4.4} B
{ND}
1.6 {1.0 J} J
06/20/11
5.0
10.0
ND
ND
ND
12/05/11
5.0
10.0
ND
ND
ND
Resample >
01/25/12
5.0
10.0
---
---
ND
06/11/12
5.0
10.0
ND
5.10 J
ND
12/12/12
5.0
10.0
ND
ND
ND
05/01/13
5.0
10.0
ND
ND
ND
08/05/13
5.0
10.0
ND
ND
ND
02/24/14
5.0
10.0
ND
ND
ND
08/12/14
EPA 6010
5.0
10.0
---
ND
ND
03/10/15
EPA 6010
2.5
10.0
ND
ND
ND
08/18/15
---
---
Dry
Dry
---
02/16/16
EPA 6010
2.5
10.0
ND
ND
ND
08/09/16
EPA 6010
2.5
10.0
ND
ND
ND
02/13/17
EPA 6010
2.5
10.0
ND
ND
ND
08/22/17
EPA 6010
2.5
10.0
ND
ND
ND
02/05/18
EPA 6010
2.5
10.0
ND
ND
ND
08/13/18
EPA 6010D
2.5
10.0
6.0 J
ND
ND
02/04/19
EPA 6010D
2.5
5.0
ND
ND
---
ISTV = 4 pg/L
08/07/19
EPA 6010D
1.1
5.0
2.5 J
ND
ND
02/12/20
EPA 6010D
1.1
5.0
ND
ND
ND
08/27/20
---
---
Dry
Dry
---
02/11/21
EPA 6010D
3.6
5.0
---
ND
---
Copper
12/29/06
---
10.0
1.3 B
1.10 B
0.60 J
07/12/07
---
10.0
ND
---
ND
12/19/07
---
10.0
5.3 B
ND
9.8
NC2B = 7 pg/L (03/28/08)
07/08/08
---
10.0
1.7 J
4.20 J
ND
12/17/08
0.3
10.0
1.40 J
1.50 J
ND
07/09/09
0.3
10.0
ND
ND
ND
12/16/09
0.3
10.0
1.90 J
2.00 J
ND
06/24/10
0.3
10.0
ND
3.10 J
ND
12/ 13/ 10
0.3
10.0
0.31 B
N D
0.49 J
06/20/11
5.0
10.0
ND
ND
ND
12/05/11
5.0
10.0
ND
ND
ND
06/11/12
5.0
10.0
ND
5.50 J
ND
12/12/12
5.0
10.0
ND
ND
ND
05/01/13
5.0
10.0
ND
ND
ND
08/05/13
5.0
10.0
ND
ND
ND
02/24/14
5.0
10.0
ND
ND
ND
08/12/14
EPA 6010
5.0
10.0
---
ND
ND
03/10/15
EPA 6010
2.5
10.0
ND
ND
ND
08/18/15
---
---
Dry
Dry
---
02/16/16
EPA 6010
2.5
10.0
2.90 J
3.40 J
ND
08/09/16
EPA 6010
2.5
10.0
ND
ND
ND
02/13/17
EPA 6010
2.5
10.0
ND
ND
ND
08/22/17
EPA 6010
2.5
10.0
ND
ND
ND
NC2B = Hardness Dependant
02/05/18
EPA 6010
2.5
10.0
3.8 J
3.8 J
ND
08/13/18
EPA 6010D
2.5
10.0
4.1 J
ND
ND
02/04/19
EPA 6010D
2.5
5.0
ND
ND
---
08/07/19
EPA 6010D
2.1
5.0
3.2 J
3.3 J
ND
02/12/20
EPA 6010D
2.1
5.0
3.9 J
3.4 J
ND
08/27/20
---
---
Dry
Dry
---
02/11/21
EPA 6010D
4.3
5.0
---
ND
---

Analytes
Sample Date
EPA Method
DL
RL
SW-1
SW-2
Blanks
Lead
05/20/98
---
10.0
ND
8.00
---
11/19/98
---
10.0
ND
ND
---
07/21/99
---
10.0
ND
10.0
---
11/ 16/99
---
10.0
ND
ND
---
05/ 10/00
---
10.0
ND
ND
---
10/26/00
---
10.0
ND
ND
---
04/18/01
---
10.0
ND
ND
---
10/27/01
---
10.0
ND
ND
---
06/13/02
---
10.0
---
---
---
11/19/02
---
10.0
ND
ND
---
06/27/03
---
10.0
ND
ND
---
12/30/03
---
10.0
ND
ND
ND
06/30/04
---
10.0
ND
ND
ND
12/29/04
---
10.0
ND
ND
ND
06/29/05
---
10.0
ND
ND
ND
12/29/05
---
10.0
ND
ND
ND
06/28/06
---
10.0
ND
ND
ND
12/29/06
---
10.0
ND
ND
ND
07/12/07
---
10.0
ND
---
ND
12/19/07
---
10.0
ND
ND
ND
NC213 = 25 pg/L (03/28/08)
07/08/08
---
10.0
ND
ND
ND
12/17/08
4.0
10.0
ND
ND
ND
07/09/09
4.0
10.0
ND
ND
ND
12/16/09
4.0
10.0
ND
ND
ND
06/24/10
4.0
10.0
ND
ND
ND
12/13/10
4.0
10.0
ND
ND
ND
06/20/11
5.0
10.0
ND
ND
ND
12/05/11
5.0
10.0
ND
ND
ND
06/11/12
5.0
10.0
ND
ND
ND
12/12/12
5.0
10.0
ND
ND
ND
05/01/13
5.0
10.0
ND
ND
ND
08/05/13
5.0
10.0
ND
ND
ND
02/24/14
5.0
10.0
ND
ND
ND
08/12/14
EPA 6010
5.0
10.0
---
ND
ND
03/10/15
EPA 6010
2.5
10.0
ND
ND
ND
08/18/15
---
---
Dry
Dry
---
02/16/16
EPA 6010
2.5
10.0
ND
ND
ND
08/09/16
EPA 6010
2.5
10.0
ND
ND
ND
02/13/17
EPA 6010
2.5
10.0
ND
ND
ND
08/22/17
EPA 6010
2.5
10.0
ND
ND
ND
NC2B = Hardness Dependant
02/05/18
EPA 6010
2.5
10.0
ND
ND
ND
08/13/18
EPA 6010D
2.5
10.0
ND
ND
ND
02/04/19
EPA 6010D
2.5
5.0
ND
ND
---
08/07/19
EPA 6010D
1.6
5.0
2.2 J
ND
ND
02/12/20
EPA 6010D
1.6
5.0
ND
ND
ND
08/27/20
---
---
Dry
Dry
---
02/11/21
EPA 6010D
4.5
5.0
---
ND
---
Nickel
12/29/04
---
50.0
ND
50.0 (ND)
ND
06/29/05
---
50.0
ND
ND
ND
12/29/05
---
50.0
ND
ND
ND
06/28/06
---
50.0
ND
ND
ND
12/29/06
---
50.0
ND
2.9 J
ND
07/12/07
---
50.0
3.8 J
---
ND
12/19/07
---
50.0
6.0
31.5
ND
NC2B = 25 pg/L (03/28/08)
07/08/08
---
50.0
3.2 J
29.8 J
ND
12/17/08
1.7
50.0
2.4 B
4.0 B
2.4 J
07/09/09
1.7
50.0
4.1 J
12.3 J
ND
12/16/09
1.7
50.0
3.8 B
4.4 B
3.0 J
06/24/10
1.7
50.0
ND
2.0 J
ND
12/13/10
1.7
50.0
ND
14.2 J
2.7 J
06/20/11
5.0
50.0
ND
7.8 J
ND
12/05/11
5.0
50.0
ND
5.3 J
ND
06/11/12
5.0
50.0
ND
11.0 J
ND
12/12/12
5.0
50.0
ND
13.8 J
ND
05/01/13
5.0
50.0
ND
ND
ND
08/05/13
5.0
50.0
ND
5.6 J
ND
02/24/14
5.0
50.0
ND
ND
ND
08/12/14
EPA 6010
5.0
50.0
---
20.3 J
ND
03/10/15
EPA 6010
2.5
50.0
3.0 J
3.8 J
ND
08/18/15
---
---
Dry
Dry
---
02/16/16
EPA 6010
2.5
50.0
2.9 J
4.7 J
ND
08/09/16
EPA 6010
2.5
50.0
3.3 J
15.2 J
ND
02/13/17
EPA 6010
2.5
50.0
ND
7.3 J
ND
08/22/17
EPA 6010
2.5
50.0
ND
16.3 J
ND
NC2B = Hardness Dependant
02/05/18
EPA 6010
2.5
50.0
5.3 J
4.4 J
ND
08/13/18
EPA 6010D
2.5
50.0
7.3 J
12.4 J
ND
02/04/19
EPA 6010D
2.5
5.0
ND
2.7 J
---
08/07/19
EPA 6010D
0.90
5.0
8.8
14.8
ND
02/12/20
EPA 6010D
0.90
5.0
3.1 J
4.6 J
ND
08/27/20
---
---
Dry
Dry
---
02/11/21
EPA 6010D
3.5
5.0
---
4.40 1
---

Analytes
Sample Date
EPA Method
DL
RL
SW-1
SW-2
Blanks
Silver
07/12/07
---
10.0
2.20 J
---
ND
12/19/07
---
10.0
ND
0.34 J
ND
NC2B = 0.06 pg/L (03/28/08)
07/08/08
---
10.0
0.35 B
1.00 J
0.12 J
12/17/08
0.1
10.0
ND
ND
ND
07/09/09
0.1
10.0
ND
0.10 J
ND
12/16/09
0.1
10.0
ND
0.16 J
ND
06/24/10
0.1
10.0
ND
0.26 J
ND
12/13/10
0.1
10.0
(ND)
{0.28) B
0.21 {0.19 J) J
06/20/11
5.0
10.0
ND
ND
ND
12/05/11
5.0
10.0
ND
ND
ND
06/11/12
5.0
10.0
ND
ND
ND
12/12/12
5.0
10.0
ND
ND
ND
05/01/13
5.0
10.0
ND
ND
ND
08/05/13
5.0
10.0
ND
ND
ND
02/24/14
5.0
10.0
ND
ND
ND
08/12/14
EPA 6010
5.0
10.0
---
ND
ND
03/10/15
EPA 6010
2.5
10.0
ND
ND
ND
08/18/15
---
---
Dry
Dry
---
02/16/16
EPA 6010
2.5
10.0
ND
ND
ND
08/09/16
EPA 6010
2.5
10.0
ND
ND
ND
02/13/17
EPA 6010
2.5
10.0
ND
ND
ND
08/22/17
EPA 6010
2.5
10.0
ND
ND
ND
NC2B = Hardness Dependant
02/05/18
EPA 6010
2.5
10.0
ND
ND
ND
08/13/18
EPA 6010D
2.5
10.0
ND
ND
ND
02/04/19
EPA 6010D
2.5
5.0
ND
ND
---
08/07/19
EPA 6010D
2.5
5.0
ND
ND
ND
02/12/20
EPA 6010D
2.5
5.0
ND
ND
ND
08/27/20
---
---
Dry
Dry
---
02/11/21
EPA 6010D
2.5
5.0
---
ND
---
Thallium
12/29/04
---
10.0
ND
10.0 (ND)
ND
06/29/05
---
10.0
ND
ND
ND
12/29/05
---
10.0
ND
ND
ND
06/28/06
---
10.0
ND
ND
ND
12/29/06
---
6.00
ND
ND
ND
07/12/07
---
5.5
ND
---
ND
12/19/07
---
5.5
3.60 J
ND
ND
07/08/08
---
5.5
3.40 J
ND
ND
12/17/08
3.0
5.5
ND
ND
ND
07/09/09
3.0
5.5
ND
ND
ND
12/16/09
3.0
5.5
ND
ND
ND
NC2B = NE (03/24/10)
06/24/10
3.0
5.5
ND
ND
ND
12/13/10
3.0
5.5
3.80 J
ND
ND
06/20/11
5.4
5.5
ND
ND
ND
12/05/11
5.4
5.5
ND
ND
ND
06/11/12
5.4
5.5
ND
ND
ND
12/12/12
5.4
5.5
ND
ND
ND
05/01/13
5.4
5.5
ND
ND
ND
08/05/13
5.4
5.5
ND
ND
ND
02/24/14
5.4
5.5
ND
ND
ND
08/12/14
EPA 6010
5.4
5.5
---
ND
ND
03/10/15
EPA 6010
5.0
5.5
ND
ND
ND
08/18/15
---
---
Dry
Dry
---
02/16/16
EPA 6010
5.0
5.5
ND
ND
ND
08/09/16
EPA 6010
5.0
5.5
ND
ND
ND
02/13/17
EPA 6020B
0.020
5.5
ND
ND
ND
08/22/17
EPA 6020B
0.020
5.5
ND
ND
ND
02/05/18
EPA 6020B
0.028
0.10
ND
ND
ND
08/13/18
EPA 6020B
0.020
5.50
ND
ND
ND
02/04/19
EPA 6020B
0.060
0.10
ND
ND
---
08/07/19
EPA 6020B
0.060
0.10
ND
ND
ND
02/12/20
EPA 6020B
0.060
0.10
ND
ND
ND
08/27/20
---
---
Dry
Dry
---
02/11/21
EPA 6020B
0.1
0.1
---
ND
---

Analytes
Sample Date
EPA Method
DL
RL
SW-1
SW-2
Blanks
Vanadium
12/29/06
---
25.0
1.60 J
2.00 J
ND
07/12/07
---
25.0
4.60 J
---
ND
12/19/07
---
25.0
3.30 J
1.40 B
0.62 J
NC2B = NE pg/L (03/28/08)
07/08/08
---
25.0
5.20 J
2.30 J
0.20 J
12/17/08
0.2
25.0
1.80 B
2.70 B
0.76 J
07/09/09
0.2
25.0
5.00 B
3.40 B
1.30 J
12/16/09
0.2
25.0
3.60 J
3.50 J
0.53 J
06/24/10
0.2
25.0
5.80 J
2.60 J
ND
12/13/10
0.2
25.0
1.60 B
0.67 B
0.36 J
06/20/11
5.0
25.0
ND
ND
ND
12/05/11
5.0
25.0
ND
ND
ND
06/11/12
5.0
25.0
ND
11.50 J
ND
12/12/12
5.0
25.0
ND
ND
ND
05/01/13
5.0
25.0
ND
ND
ND
08/05/13
5.0
25.0
ND
ND
ND
02/24/14
5.0
25.0
ND
ND
ND
08/12/14
EPA 6010
5.0
25.0
---
ND
ND
03/10/15
EPA 6010
2.5
25.0
3.9 J
4.7 J
ND
08/18/15
---
---
Dry
Dry
---
02/16/16
EPA 6010
2.5
25.0
4.1 J
5.8 J
ND
08/09/16
EPA 6010
2.5
25.0
2.9 J
2.8 J
ND
02/13/17
EPA 6010
2.5
25.0
ND
ND
ND
08/22/17
EPA 6010
2.5
25.0
2.8 J
ND
ND
02/05/18
EPA 6010
2.5
25.0
6.6 J
5.9 J
ND
08/13/18
EPA 6010D
2.5
25.0
8.3 J
3.1 J
ND
02/04/19
EPA 6010D
2.5
5.0
2.9 J
2.7 J
---
08/07/19
EPA 6010D
1.3
5.0
1.4 J
2.3 J
ND
02/12/20
EPA 6010D
1.3
5.0
4.5 J
5.0
ND
08/27/20
---
---
Dry
Dry
---
02/11/21
EPA 6010D
3.9
5.0
---
ND
---
Zinc
11/22/96
---
50.0
11.0
ND
---
06/17/97
---
50.0
ND
ND
---
12/01/97
---
50.0
20.0
ND
---
05/20/98
---
50.0
20.0
28.0
---
11/19/98
---
50.0
ND
ND
---
07/21/99
---
50.0
ND
ND
---
11/16/99
---
50.0
ND
ND
---
05/10/00
---
50.0
ND
ND
---
10/26/00
---
50.0
ND
ND
---
04/18/01
---
50.0
ND
ND
---
10/27/01
---
50.0
ND
ND
---
06/13/02
---
50.0
---
---
---
11/19/02
---
50.0
ND
ND
---
06/27/03
---
50.0
ND
ND
---
12/30/03
---
50.0
ND
ND
ND
06/30/04
---
50.0
ND
ND
ND
12/29/04
---
50.0
ND
ND
ND
06/29/05
---
50.0
ND
ND
ND
12/29/05
---
50.0
ND
ND
ND
06/28/06
---
50.0
ND
ND
ND
12/29/06
---
50.0
ND
ND
ND
07/12/07
---
10.0
ND
---
ND
12/19/07
---
10.0
24.6 B
ND
102
NC2B = 50 pg/L (03/28/08)
07/08/08
---
10.0
ND
ND
1.20 J
12/17/08
0.4
10.0
ND
0.89 B
0.49 J
07/09/09
0.4
10.0
ND
4.90 B
1.60 J
12/16/09
0.4
10.0
2.60 B
2.60 B
7.70 J
06/24/10
0.4
10.0
ND
14.9
ND
12/13/10
0.4
10.0
ND
9.80 B
6.70 J
06/20/11
10.0
10.0
ND
ND
ND
12/05/11
10.0
10.0
ND
ND
12.4
06/11/12
10.0
10.0
ND
ND
ND
12/12/12
10.0
10.0
ND
ND
ND
05/01/13
10.0
10.0
ND
16.80
ND
08/05/13
10.0
10.0
ND
ND
ND
02/24/14
10.0
10.0
ND
ND
ND
08/12/14
EPA 6010
10.0
10.0
---
ND
ND
03/10/15
EPA 6010
5.0
10.0
7.7 B
7.8 B
5.6 J
08/18/15
---
---
Dry
Dry
---
02/16/16
EPA 6010
5.0
10.0
7.0 J
ND
ND
08/09/16
EPA 6010
5.0
10.0
ND
ND
ND
02/13/17
EPA 6010
5.0
10.0
ND
5.2 J
ND
08/22/17
EPA 6010
5.0
10.0
ND
ND
ND
NC2B = Hardness Dependant
02/05/18
EPA 6010
5.0
10.0
ND
ND
ND
08/13/18
EPA 6010D
5.0
10.0
6.0 J
ND
ND
02/04/19
EPA 6010D
5.0
10.0
ND
ND
---
08/07/19
EPA 6010D
3.9
10.0
ND
ND
ND
02/12/20
EPA 6010D
3.9
10.0
ND
ND
ND
08/27/20
---
---
Dry
Dry
---
02/11/21
EPA 6010D
9.5
10.0
---
ND
---
Hardness, Total(SM 2340B)
02/04/19
EPA 6010D
662
662
57.1
85.3
---
08/07/19
EPA 6010D
131
662
316
460
ND
02/12/20
EPA 6010D
131
662
18300
60200
---
08/27/20
---
---
Dry
Dry
---
02/11/21
EPA 6010D
131.0
662.0
---
70000.00
---

Analytes
Sample Date
EPA Method
DL
RL
SW-1
SW-2
Blanks
ORGANICS
Acetone
10/27/01
---
100
168.0 B
337.0 B
479.0
06/13/02
---
100
---
---
---
06/13/02
---
100
---
---
---
11/19/02
---
100
ND
ND
---
06/27/03
---
100
ND
ND
---
12/30/03
---
100
ND
ND
ND
06/30/04
---
100
ND
ND
ND
12/29/04
---
100
ND
ND
ND
06/29/05
---
100
ND
ND
ND
12/29/05
---
100
ND
ND
ND
06/28/06
---
100
ND
ND
ND
12/29/06
---
100
ND
ND
ND
07/12/07
---
100
ND
---
ND
12/19/07
---
100
12.70 B
ND
4.50 J
NC2B = 2,000 pg/L (03/28/08)
07/08/08
---
100
ND
ND
ND
12/17/08
20
100
ND
ND
ND
07/09/09
20
100
ND
ND
ND
NC2B = NE (03/24/10)
12/16/09
2.2
100
ND
ND
2.80 J
06/24/10
2.2
100
2.80 B
ND
7.70 J
12/13/10
2.2
100
ND
3.00 J
ND
06/20/11
2.2
100
ND
3.80 B
3.90 J
12/05/11
2.2
100
ND
7.20 B
8.80 J
06/11/12
2.2
100
ND
5.50 B
4.70 J
12/12/12
10.0
100
ND
ND
ND
05/01/13
10.0
100
ND
ND
14.6 J
08/05/13
10.0
100
ND
ND
ND
02/24/14
10.0
100
ND
ND
25.7 J
08/12/14
EPA 8260
10.0
100
---
ND
22.0 J
03/10/15
EPA 8260
10.0
100
ND
ND
ND
08/18/15
---
---
Dry
Dry
---
02/16/16
EPA 8260
10.0
100
ND
ND
ND
08/09/16
EPA 8260
10.0
100
ND
ND
ND
02/13/17
EPA 8260
10.0
100
ND
ND
ND
08/22/17
EPA 8260
10.0
100
ND
ND
ND
02/05/18
EPA 8260
10.0
100
ND
ND
ND
08/13/18
EPA 8260B
10.0
100
ND
ND
ND
02/04/19
EPA 8260B
6.2
25
ND
ND
---
ISTV = 2000 pg/L
08/07/19
EPA 8260D
6.2
25.0
ND
ND
ND
02/12/20
EPA 8260D
6.2
25.0
ND
ND
ND
08/27/20
---
---
Dry
Dry
---
02/11/21
EPA 8260D
6.2
25.0
---
ND
---
Chlorobenzene
06/27/03
---
5.0
ND
7.20
ND
12/30/03
---
5.0
ND
ND
ND
06/30/04
---
5.0
ND
ND
ND
12/29/04
---
5.0
ND
ND
ND
06/29/05
---
5.0
ND
ND
ND
12/29/05
---
5.0
ND
ND
ND
06/28/06
---
5.0
ND
ND
ND
12/29/06
---
3.0
ND
ND
ND
07/12/07
---
3.0
ND
---
ND
12/19/07
---
3.0
ND
ND
ND
NC2B = 130 pg/L (03/28/08)
07/08/08
---
3.0
ND
ND
ND
12/17/08
0.23
3.0
ND
ND
ND
07/09/09
0.23
3.0
ND
ND
ND
12/16/09
0.23
3.0
ND
ND
ND
06/24/10
0.23
3.0
ND
ND
ND
12/13/10
0.23
3.0
ND
ND
0.28 J
06/20/11
0.23
3.0
ND
ND
ND
12/05/11
0.23
3.0
ND
ND
ND
06/11/12
0.23
3.0
ND
ND
ND
12/12/12
0.23
3.0
ND
ND
ND
05/01/13
0.23
3.0
ND
ND
ND
08/05/13
0.23
3.0
ND
ND
ND
02/24/14
0.23
3.0
ND
ND
ND
08/12/14
EPA 8260
0.23
3.0
---
ND
ND
03/10/15
EPA 8260
0.23
3.0
ND
ND
ND
08/18/15
---
---
Dry
Dry
---
02/16/16
EPA 8260
0.23
3.0
ND
ND
ND
08/09/16
EPA 8260
0.23
3.0
ND
ND
ND
02/13/17
EPA 8260
0.23
3.0
ND
ND
ND
08/22/17
EPA 8260
0.23
3.0
ND
ND
ND
02/05/18
EPA 8260
0.23
3.0
ND
ND
ND
08/13/18
EPA 8260B
0.23
3.0
ND
ND
ND
02/04/19
EPA 8260B
0.23
1.0
ND
ND
---
08/07/19
EPA 8260D
0.23
1.0
ND
ND
ND
02/12/20
EPA 8260D
0.23
1.0
ND
ND
ND
08/27/20
---
---
Dry
Dry
---
02/11/21
EPA 8260D
0.2
1.0
---
ND
---

Analytes
Sample Date
EPA Method
DL
RL
SW-1
SW-2
Blanks
Chloromethane
07/09/09
0.11
1.0
ND
0.19 J
ND
12/16/09
0.11
1.0
ND
ND
ND
NC213 = NE (03/24/10)
06/24/10
0.11
1.0
ND
ND
ND
12/13/10
0.11
1.0
ND
ND
ND
06/20/11
0.11
1.0
ND
ND
ND
12/05/11
0.11
1.0
ND
ND
ND
06/11/12
0.11
1.0
ND
ND
ND
12/12/12
0.11
1.0
ND
ND
ND
05/01/13
0.11
1.0
ND
ND
ND
08/05/13
0.11
1.0
ND
ND
ND
02/24/14
0.11
1.0
ND
ND
0.25 J
08/12/14
EPA 8260
0.11
1.0
---
ND
ND
03/10/15
EPA 8260
0.11
1.0
ND
ND
ND
08/18/15
---
---
Dry
Dry
---
02/16/16
EPA 8260
0.11
1.0
ND
ND
ND
08/09/16
EPA 8260
0.11
1.0
ND
ND
ND
02/13/17
EPA 8260
0.11
1.0
0.17 J
0.19 J
0.18 J
08/22/17
EPA 8260
0.11
1.0
ND
ND
ND
02/05/18
EPA 8260
0.11
1.0
ND
ND
ND
08/13/18
EPA 8260B
0.11
1.0
ND
ND
ND
02/04/19
EPA 8260B
0.39
1.0
ND
ND
---
08/07/19
EPA 8260D
0.39
1.0
ND
ND
ND
02/12/20
EPA 8260D
0.39
1.0
ND
ND
ND
08/27/20
---
---
Dry
Dry
---
02/11/21
EPA 8260D
0.4
1.0
---
ND
---
1,4-Dioxane (p-Dioxane)
08/13/18
EPA 8260B Mod.
1.9
2.0
ND
14.1
ND
02/04/19
EPA 8260B Mod.
1.9
2.0
ND
ND
---
ISTV = 80 pg/L
08/07/19
EPA 8260D Mod.
1.2
2.0
10.50
22.3
ND
02/12/20
EPA 8260D Mod.
1.2
2.0
ND
1.2 J
ND
08/27/20
---
---
Dry
Dry
---
02/11/21
EPA 8260D Mod.
1.2
2.0
---
3.00
---
Methylene Chloride
08/09/16
EPA 8260
0.97
1.0
ND
ND
2.20 J
02/13/17
EPA 8260
0.97
1.0
ND
ND
ND
NC 2L = 5 pg/L (2/5/10)
08/22/17
EPA 8260
0.97
1.0
ND
ND
1.4 C9
02/05/18
EPA 8260
0.97
1.0
ND
ND
ND
08/13/18
EPA 8260B
0.97
1.0
ND
ND
6.60
02/04/19
EPA 8260B
3.7
5.0
ND
ND
---
ISTV = 11,000 pg/L
08/07/19
EPA 8260D
3.7
5.0
ND
ND
ND
02/12/20
EPA 8260D
3.7
5.0
ND
ND
ND
08/27/20
---
---
Dry
Dry
---
02/11/21
EPA 8260D
3.7
5.0
---
ND
---
Notes:
All concentrations are in micrograms per liter (pg/L).
RL = Reporting Limit (SWSL for December 2006 - present).
DL = Laboratory detection limit.
J = Estimated value between the DL and the RL.
B = Blank -qualified data; result is expected to be biased high based on concentrations in the blanks.
ND = Not detected above laboratory reporting limit.
NS = Not sampled.
NR = Not Reported.
Dry =Surface water point considered to be dry.
NC2B = North Carolina Surface Water Standards from 15A NCAC 2B.0101
ISTV = NC In -stream Target Values (for constituents with no NC2B).
NE = Not established.

Appendix F
Historical Monitoring Natural Attenuation Parameters
(from LaBella, 2021)

Parameter
Date
Units
DL RL
MW-1R
MW-2R MW-3R MW-4 MW-5 MW-6
NES-1
Temperature
12/30/03
°C
- -
15.4
11.1 11.2 12.5 13.6 14.2
-
(FP)
12/19/07
°C
- -
12.3
12.5 13.1 14.4 14.9 14.4
13.3
05/01/13
°C
- -
15.7
13.7 15.1 14.4 14.2 14.2
12.5
08/14/14
°C
- -
17.8
18.0 19.2 19.4 16.8 17.2
16.0
03/10/15
°C
- -
17.3
16.0 15.9 13.8 13.3 13.7
16.1
08/18/15
°C
- -
16.43
17.78 17.79 17.25 16.47 16.64
16.05
02/16/16
°C
- -
14.6
13.8 14.4 14.0 12.0 13.4
13.1
08/09/16
°C
- -
16.4
17.3 19.4 18.2 17.1 16.8
17.9
02/13/17
°C
- -
14.8
14.4 14.9 15.7 14.1 15.3
15.2
08/22/17
°C
- -
17.4
17.9 17.9 17.5 17.4 16.6
17.8
02/05/18
°C
- -
13.06
11.66 13.05 14.46 13.83 14.53
12.25
08/13/18
°C
- -
17.4
21.1 18.2 19.3 20.6 18.4
16.6
02/04/19
°C
- -
13.2
15.5 16.5 14.9 14.5 15.4
13.7
08/06/19
°C
- -
17.0
22.7 17.6 19.9 17.3 18.2
16.0
Resample -->
08/14/19
°C
- -
-
- - - - 24.3
-
02/12/20
°C
- -
17.2
14.3 14.8 16.5 15.1 16.4
14.8
08/27/20
°C
- -
17.2
18.9 19.9 22.2 20.3 21.1
20.1
Resample -->
09/30/20
°C
- -
-
- 19.3 - - -
-
02/11/21
°C
- -
15.1
12.4 13.6 11.8 11.5 11.3
14.0
pH
12/30/03
SU
- -
7.31
6.54 6.81 6.90 7.24 7.29
-
(FP)
12/19/07
SU
- -
6.89
6.90 7.07 6.87 7.39 6.67
7.64
05/01/13
SU
- -
7.32
6.37 6.61 6.42 6.92 7.13
6.10
08/14/14
SU
- -
5.84
6.36 6.96 6.79 7.00 6.48
5.59
03/10/15
SU
- -
6.11
6.37 6.56 6.30 6.25 6.55
5.68
08/18/15
SU
- -
5.12
6.68 6.48 6.76 7.03 6.78
4.94
02/16/16
SU
- -
6.15
6.15 6.61 6.69 7.14 6.10
6.52
08/09/16
SU
- -
4.79
5.05 5.30 5.06 4.41 5.75
6.46
02/13/17
SU
- -
6.10
6.55 6.76 6.78 6.24 7.37
6.23
08/22/17
SU
- -
6.58
6.46 6.45 6.98 7.53 7.16
7.16
02/05/18
SU
- -
7.11
6.80 7.01 7.33 7.22 7.54
5.53
08/13/18
SU
- -
6.30
6.45 6.64 6.38 7.15 7.03
5.54
02/04/19
SU
- -
6.17
6.44 7.16 6.87 6.07 7.02
5.13
08/06/19
SU
- -
8.84
6.17 6.49 6.69 7.44 7.49
6.79
Resample -->
08/14/19
SU
- -
-
- - - - 6.47
-
02/12/20
SU
- -
5.63
4.88 6.30 6.73 6.27 7.10
8.72
08/27/20
SU
- -
5.08
6.13 6.42 6.45 6.71 6.73
5.48
Resample -->
09/30/20
SU
- -
-
- 6.57 - - -
-
02/11/21
SU
- -
5.65
6.13 6.45 5.94 6.30 6.15
4.38
Conductivity
12/19/07
pS/cm
- -
96
1,964 1,591 1,245 - -
510
(FP)
05/01/13
pS/cm
- -
111
1,587 1,357 1,150 195 594
69.6
08/14/14
pS/cm
- -
231
1,897 1,534 1,413 522 565
172.6
03/10/15
pS/cm
- -
90
996 1,277 1,186 106 504
114
08/18/15
pS/cm
- -
134
1,630 1,680 1,244 617 534
83
02/16/16
pS/cm
- -
72.4
1,611 1,369 1,234 164 474
78.2
08/09/16
pS/cm
- -
100.7
1,924 1,535 1,475 660 600
95.6
02/13/17
pS/cm
- -
68.0
1,535 1,314 1,155 272 508
89.6
08/22/17
pS/cm
- -
77.1
1,752 1,350 1,446 755 560
175
02/05/18
pS/cm
- -
80.0
1,460 1,247 1,230 676 633
50.0
08/13/18
pS/cm
- -
101.2
2,013 1,608 1,569 870 620
131.2
02/04/19
pS/cm
- -
107.9
1,692 1,266 1,364 276.1 546.0
91.6
08/06/19
pS/cm
- -
113.4
1,719 1,307 1,287 775.0 545.3
98.5
Resample -->
08/14/19
pS/cm
- -
-
- - - - 559
-
02/12/20
pS/cm
- -
94.8
1,946 1,475 1,471 276.9 588.3
95.5
08/27/20
pS/cm
- -
82.4
1,601 1,217 1,335 773.0 577.0
140.5
Resample -->
09/30/20
pS/cm
- -
-
- 1,409 - - -
-
02/11/21
pS/cm
- -
85.2
1,251.0 1,004.0 838.0 211.3 323.8
65.9

Parameter
Date
Units
DL RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5
MW-6
NES-1
Redox Potential
12/30/03
mV
- -
257.2
76.2
207.6
212.7
187.3
123.6
-
ORP
12/19/07
mV
- -
146
45.0
142
134
-
-
138
(FP)
05/01/13
mV
- -
111.7
-26.7
55.2
120.5
-
-
227.1
08/14/14
mV
- -
115.8
-37.2
86.9
-
-
-
-
03/10/15
mV
- -
87.0
0.8
56.3
-
-
-
96.7
08/18/15
mV
- -
134.7
-96.3
-68.8
-33.9
-49.9
-
182.8
02/16/16
mV
- -
111.7
-47.3
16.9
-
-
-
173.4
08/09/16
mV
- -
56.0
-43.1
-6.9
-
-
-
-
02/13/17
mV
- -
87.4
0.8
-16.5
-
-
-
-
08/22/17
mV
- -
102.9
-37.1
87.0
-
-
-
116.7
02/05/18
mV
- -
57.1
29.5
49.4
-
-
-
109.2
08/13/18
mV
- -
117.9
-60.5
-49.3
-
-
64.4
28.4
02/04/19
mV
- -
197.7
-64.3
132.2
-
9.6
-
281.2
08/06/19
mV
- -
164.7
-69.3
-33.7
171.6
188.6
232.6
231.8
Resample -->
08/14/19
mV
- -
-
-
-
-
-
237.6
-
02/12/20
mV
- -
336.5
33.4
22.4
254.5
299.9
282.0
245.6
08/27/20
mV
- -
242.7
-10.8
12.4
190.3
196.5
188.0
240.6
Resample -->
09/30/20
mV
- -
-
-
232.3
-
-
-
-
02/11/21
mV
- -
166.8
4.1
34.8
197.4
-
278.8
284.5
Dissolved Oxygen
12/30/03
mg/L
- -
9.49
4.84
-
-
-
-
-
DO
12/19/07
mg/L
- -
-
1.88
1.44
3.21
-
-
0.70
(FP)
05/01/13
mg/L
- -
4.40
1.37
1.79
4.65
-
-
2.90
08/14/14
mg/L
- -
4.44
3.26
2.48
-
-
-
2.80
03/10/15
mg/L
- -
3.84
1.47
1.80
-
-
-
1.85
08/18/15
mg/L
- -
4.95
5.75
1.30
-
3.79
-
1.77
02/16/16
mg/L
- -
4.45
3.66
2.51
-
-
-
3.72
08/09/16
mg/L
- -
3.17
2.87
2.29
-
-
-
-
02/13/17
mg/L
- -
5.37
3.16
2.14
-
-
-
-
08/22/17
mg/L
- -
5.43
2.24
4.02
-
-
-
5.86
02/05/18
mg/L
- -
8.08
6.61
9.16
-
-
-
8.36
08/13/18
mg/L
- -
6.31
3.20
2.35
-
-
4.80
3.91
02/04/19
mg/L
- -
1.26
1.82
4.17
-
4.17
-
1.63
08/06/19
mg/L
- -
3.77
0.32
0.26
4.55
5.30
2.76
3.04
Resample -->
08/14/19
mg/L
- -
-
-
-
-
-
1.95
-
02/12/20
mg/L
- -
5.11
0.65
1.36
4.30
3.48
2.44
6.37
08/27/20
mg/L
- -
0.63
0.22
0.48
5.04
6.22
4.14
3.16
Resample -->
09/30/20
mg/L
- -
-
-
2.00
-
-
-
-
02/11/21
mg/L
- -
1.75
1.05
0.40
7.40
5.41
3.23
2.18
Dissolved CO2
12/19/07
mg/L
- -
25.0
365
175
295
-
-
60
(FP)
05/01/13
mg/L
- -
30.0
245
125
225
-
-
45
08/14/14
mg/L
- -
60.0
390
185
-
-
-
75
03/10/15
mg/L
- -
50.0
110
75
-
-
-
50
08/18/15
mg/L
- -
30.0
275
125
-
-
-
60
02/16/16
mg/L
- -
30.0
210
230
-
-
-
20
08/09/16
mg/L
- -
-
185
210
-
-
-
-
02/13/17
mg/L
- -
-
-
-
-
-
-
-
08/22/17
mg/L
- -
-
-
-
-
-
-
-
02/05/18
mg/L
- -
-
-
-
-
-
-
-
08/13/18
mg/L
- -
-
-
-
-
-
-
-
02/04/19
mg/L
- -
75.0
-
130.0
-
-
-
-
08/06/19
mg/L
- -
-
475.0
250.0
-
-
-
-
02/12/20
mg/L
- -
-
260.0
-
-
-
-
-
08/27/20
mg/L
- -
-
-
-
-
-
-
-
02/11/21
mg/L
- -
-
-
-
-
-
-
-

Parameter
Date
Units
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5 MW-6
NES-1
Fe, Ferrous (+2)
12/30/03
mg/L
-
-
ND
1.5
ND
ND
0.22 ND
-
(FP)
12/19/07
mg/L
-
-
ND
7.2
ND
ND
- -
0.2
05/01/13
mg/L
-
-
ND
1.0
ND
ND
- -
ND
08/14/14
mg/L
-
-
ND
2.5
ND
-
- -
ND
03/10/15
mg/L
-
-
ND
5.3
ND
-
- -
ND
08/18/15
mg/L
-
-
ND
4.5
1.0
-
- -
ND
02/16/16
mg/L
-
-
ND
4.0
1.3
-
- -
ND
08/09/16
mg/L
-
-
-
3.1
1.0
-
- -
-
02/13/17
mg/L
-
-
ND
3.0
1.5
-
- -
-
08/22/17
mg/L
-
-
ND
3.5
1.5
-
- -
ND
02/05/18
mg/L
-
-
ND
4.0
0.5
-
- -
ND
08/13/18
mg/L
-
-
ND
5.5
0.2
-
- -
-
02/04/19
mg/L
-
-
ND
-
ND
-
- -
-
08/06/19
mg/L
-
-
-
3.5
0.5
-
- -
-
02/12/20
mg/L
-
-
-
1.0
0.5
-
- -
-
08/27/20
mg/L
-
-
-
4.5
1.0
-
- -
-
02/11/21
mg/L
-
-
0
1.5
0.5
-
- -
0.0
Alkalinity (as CaCO3)
12/30/03
mg/L
9.00
10.0
37.0
800
690
640
68.0 350
-
12/19/07
mg/L
-
5.00
39.0
763
726
619
- -
190
05/01/13
mg/L
1.00
5.00
43.4
757
660
645
- -
10.4
08/14/14
mg/L
1.00
5.00
41.1
784
661
-
- -
14.5
03/10/15
mg/L
1.00
5.00
38.0
744
653
-
- -
8.8
08/18/15
mg/L
1.00
5.00
37.8
772
664
-
- -
10.3
02/16/16
mg/L
1.00
5.00
41.2
792
741
-
- -
8.73
08/09/16
mg/L
1.00
5.00
-
783
629
-
- -
-
02/13/17
mg/L
1.00
5.00
37.9
753
654
-
- -
8.79
08/22/17
mg/L
1.00
5.00
42.4
766
678
-
- -
10.2
02/05/18
mg/L
1.00
5.00
44.4
821
752
-
- -
7.52
08/13/18
mg/L
1.00
5.00
-
768
722
-
- -
-
02/04/19
mg/L
1.00
5.00
62.0
856
638
-
- -
7.02
08/06/19
mg/L
5.00
5.00
-
839
754
-
- -
-
02/02/20
mg/L
5.00
5.00
-
818
646
-
- -
-
08/27/20
mg/L
5.00
5.00
47.6
909
735
-
- -
-
02/11/21
mg/L
5.00
5.00
53.9
875
724
-
- -
ND
Chloride
12/30/03
mg/L
0.200
1.00
3.50
280
170
82.0
13.0 44.0
-
12/19/07
mg/L
-
5.00
ND
13.1
297
89.1
- -
7.90
NC 2L = 250,000 pg/L
05/01/13
mg/L
0.50
1.00
3.54
258
180
123
- -
2.85
(250 mg/L)
08/14/14
mg/L
0.50
1.00
5.53
264
144
-
- -
5.00
03/10/15
mg/L
0.50
1.00
3.80
266
194
-
- -
4.09
08/18/15
mg/L
0.50
1.00
4.69
267
178
-
- -
3.90
02/16/16
mg/L
0.50
1.00
3.92
274
186
-
- -
3.24
08/09/16
mg/L
0.50
1.00
-
269
191
-
- -
-
02/13/17
mg/L
0.50
1.00
3.45
309
215
-
- -
5.09
08/22/17
mg/L
0.50
1.00
3.73
318
214
-
- -
5.86
02/05/18
mg/L
0.50
1.00
3.92
280
205
-
- -
2.52
08/13/18
mg/L
0.50
1.00
-
221
165
-
- -
-
02/04/19
mg/L
0.50
1.00
3.42
221
147
-
- -
4.52
08/06/19
mg/L
2.40
4.00
-
203
154
-
- -
-
02/12/20
mg/L
2.40
4.00
-
224
153
-
- -
-
08/27/20
mg/L
2.40
4.00
3.84
208
148
-
- -
5.33
02/11/21
mg/L
2.40
4.00
3.67
201
148
-
- -
4.06

Parameter
Date
Units
DL RL
MW-1R
MW-2R MW-3R MW-4 MW-5 MW-6
NES-1
Dissolved Hydrogen
05/01/13
nM
0.074 0.60
0.400
0.630 0.610 0.500 - -
0.470
08/14/14
nM
0.13 0.60
1.4
1.6 5.4 - - -
1.4
03/10/15
nM
0.13 0.60
1.2
1.4 1.4 1.0 - -
1.4
08/18/15
nM
0.13 0.60
1.7
2.2 1.7 - - -
1.5
02/16/16
nM
0.13 0.60
2.0
1.7 1.9 - - -
1.5
08/09/16
nM
0.13 0.60
-
1.5 1.6 - - -
-
02/13/17
nM
- -
-
- - - - -
-
08/22/17
nM
- -
-
- - - - -
-
02/05/18
nM
- -
-
- - - - -
-
08/13/18
nM
- -
-
- - - - -
-
02/04/19
nM
0.65 1.0
6.7
7.6 7.4 - - -
6.8
08/06/19
nM
0.75 1.0
-
2.0 5.4 - - -
-
02/12/20
nM
- -
-
5.8 2.7 - - -
-
08/27/20
nM
0.49 0.49
-
1.0 J 1.2 J - - -
-
Resample -->
09/10/20
nM
0.49 1.9
1.8
- - - - -
2.4
02/11/21
nM
- -
-
- - - - -
-
Nitrate-N
12/30/03
mg/L
0.020 0.050
0.120
ND ND ND ND 0.13
-
12/19/07
mg/L
- 0.100
ND
ND ND ND - -
13.0
05/01/13
mg/L
0.001 10.0
0.163
ND ND ND - -
3.58
08/14/14
mg/L
0.001 10.0
0.115 J
ND ND - - -
2.02 J
03/10/15
mg/L
0.001 10.0
0.252 J
ND ND - - -
2.56 J
08/18/15
mg/L
0.001 10.0
0.124 J
ND ND - - -
3.27 J
02/16/16
mg/L
0.001 10.0
0.36 J
ND ND - - -
2.54 J
08/09/16
mg/L
0.001 10.0
-
ND ND - - -
-
02/13/17
mg/L
0.001 10.0
0.248 J
0.189 J ND - - -
2.63 J
08/22/17
mg/L
0.001 10.0
0.118 J
0.0186 J 0.0451 J - - -
4.06 J
02/05/18
mg/L
0.010 10.0
0.310 J
ND 0.0120 J - - -
1.15 J
08/13/18
mg/L
0.050 0.1
-
ND ND - - -
-
02/04/19
mg/L
0.050 0.1
0.196
ND 0.113 - - -
6.5
08/06/19
mg/L
0.010 0.0
-
ND ND - - -
-
02/12/20
mg/L
0.010 0.0
-
0.069 0.362 - - -
-
08/27/20
mg/L
0.050 0.1
ND
ND ND - - -
6.34
02/11/21
mg/L
0.01 0.04
0.0565
ND 0.0587 - - -
4.65
Sulfate
12/30/03
mg/L
0.0600 2.00
ND
ND ND 2.60 9.60 9.00
-
12/19/07
mg/L
- 5.00
ND
ND ND ND - -
36.8
NC 2L = 250,000 pg/L
05/01/13
mg/L
1.00 250
ND
ND ND 4.69 - -
10.7
(250 mg/L)
08/14/14
mg/L
1.00 250
1.08 J
1.2 J ND - - -
5.84 J
03/10/15
mg/L
1.00 250
1.52 J
1.13 J 1.52 J - - -
7.04 J
08/18/15
mg/L
1.00 250
1.56 J
1.31 J 2.49 J - - -
524 J
02/16/16
mg/L
1.0 250
1.5 J
1.7 J 1.8 J - - -
10.0 J
08/09/16
mg/L
1.00 250
-
1.22 J 1.75 J - - -
-
02/13/17
mg/L
1.00 250
1.53 J
1.59 J 1.78 J - - -
11.9 J
08/22/17
mg/L
1.00 250
ND
ND 0.626 J - - -
11.2 J
02/05/18
mg/L
0.500 250
ND
ND 0.627 J - - -
7.48 J
08/13/18
mg/L
0.500 250
ND
ND 0.630 J - - -
-
02/04/19
mg/L
0.500 250
1.15
ND 1.10 - - -
6.75
08/06/19
mg/L
0.500 1
-
ND 0.711 J - - -
-
02/12/20
mg/L
0.500 1
-
ND 0.58 J - - -
-
08/27/20
mg/L
0.500 1
ND
ND ND - - -
5.21
02/11/21
mg/L
0.500 1
1.41
ND 0.819 - - -
5.92

Parameter
Date
Units
DL RL
MW-1R
MW-2R MW-3R MW-4 MW-5 MW-6
NES-1
Sulfide
08/14/14
mg/L
0.05 1.00
ND
ND ND - - -
ND
03/10/15
mg/L
0.05 1.00
ND
ND ND - - -
ND
08/18/15
mg/L
0.05 1.00
ND
ND ND - - -
1.0
02/16/16
mg/L
0.05 1.00
ND
ND ND - - -
ND
08/09/16
mg/L
0.05 1.00
-
ND ND - - -
-
02/13/17
mg/L
0.05 1.00
ND
ND ND - - -
-
08/22/17
mg/L
0.05 1.00
ND
ND ND - - -
-
02/05/18
mg/L
- -
-
- - - - -
-
08/13/18
mg/L
- -
-
- - - - -
-
02/04/19
mg/L
0.05 1
ND
ND ND - - -
ND
08/06/19
mg/L
0.05 0.1
-
ND ND - - -
-
02/12/20
mg/L
0.05 0.1
-
0.083 J ND - - -
-
08/27/20
mg/L
0.05 0.1
ND
ND ND - - -
ND
02/11/21
mg/L
- -
-
- - - - -
-
Total Organic Carbon
12/19/07
mg/L
- 1.0 *
2.9
54.3 23.2 17.2 - -
7.20
05/01/13
mg/L
0.50 1.00
2.24
29.5 30.0 19.4 - -
5.74
08/14/14
mg/L
0.50 1.00
ND
229 25.5 - - -
8.39
03/10/15
mg/L
0.50 1.00
0.781J
34.8 9.54 - - -
1.88
08/18/15
mg/L
0.50 1.00
0.917J
32.9 9.86 - - -
27.80
02/16/16
mg/L
0.50 1.00
1.500
27.6 8.46 - - -
40.90
08/09/16
mg/L
0.50 1.00
-
29.4 9.53 - - -
-
02/13/17
mg/L
0.50 1.00
ND
28.5 9.72 - - -
1.36
08/22/17
mg/L
0.50 1.00
ND
29.1 9.92 - - -
1.71
02/05/18
mg/L
0.50 1.00
ND
25.9 11.4 - - -
4.24
08/13/18
mg/L
0.50 1.00
ND
25.8 10.2 - - -
ND
02/04/19
mg/L
0.50 1.00
ND
27.9 8.02 - - -
1.6
08/06/19
mg/L
2.50 5.00
-
33.3 15.1 - - -
-
02/12/20
mg/L
2.50 5.00
-
25.4 7.46 - - -
-
08/27/20
mg/L
0.50 1.00
0.689 J
29.8 8.19 - - -
0.916 J
02/11/21
mg/L
0.50 1.00
ND
28.2 7.68 - - -
1.61
Biochemical Oxygen Demand
08/14/14
mg/L
2.00 2.00
ND
83.4 2.49 - - -
-
BOD (5-day)
03/10/15
mg/L
2.00 2.00
2.55
10.6 ND - - -
ND
08/18/15
mg/L
2.00 2.00
2.22
11.8 2.0 - - -
2.00
02/16/16
mg/L
2.00 2.00
ND
60.0 6.6 - - -
ND
08/09/16
mg/L
2.00 2.00
-
11.6 ND - - -
-
02/13/17
mg/L
2.00 2.00
ND
9.50 J ND - - -
ND
08/22/17
mg/L
2.00 2.00
ND
ND ND - - -
ND
02/05/18
mg/L
2.00 2.00
ND
5.6 ND - - -
ND
08/13/18
mg/L
2.00 2.00
ND
71.8 3.56 - - -
ND
02/04/19
mg/L
2.00 2.00
ND
7.5 ND - - -
ND
08/06/19
mg/L
2.00 2.00
-
8.0 ND - - -
-
02/12/20
mg/L
2.00 2.00
-
6.3 ND - - -
-
08/27/20
mg/L
2.00 2.00
ND
9.45 ND - - -
ND
02/11/21
mg/L
2.00 2.00
ND
9.87 ND - - -
ND

Parameter
Date
Units
DL
RL
MW-1R
MW-2R
MW-3R
MW-4
MW-5 MW-6
NES-1
Chemical Oxygen Demand
08/14/14
mg/L
12.5
25.0
ND
132.0
ND
-
- -
50.00
COD
03/10/15
mg/L
12.5
25.0
15.0J
235.0
96.0
-
- -
ND
08/18/15
mg/L
12.5
25.0
25.0
110.0
756.0
-
- -
25.00
02/16/16
mg/L
12.5
25.0
ND
295.0
50.0
-
- -
ND
08/09/16
mg/L
12.5
25.0
-
131.0
50.0
-
- -
-
02/13/17
mg/L
12.5
25.0
17.0 J
119.0
43.0
-
- -
22.0 J
08/22/17
mg/L
12.5
25.0
ND
121.0
74.0
-
- -
16.0 J
02/05/18
mg/L
12.5
25.0
ND
113.0
51.0
-
- -
46.0
08/13/18
mg/L
12.5
25.0
ND
112.0
73.9
-
- -
ND
02/04/19
mg/L
12.5
25.0
ND
101.0
26.5
-
- -
ND
08/06/19
mg/L
12.5
25.0
-
123.0
45.5
-
- -
-
02/12/20
mg/L
12.5
25.0
-
160.0
36.1
-
- -
-
08/27/20
mg/L
12.5
25.0
ND
112.00
35.9
-
- -
ND
02/11/21
mg/L
12.5
25.0
ND
108
38.0
-
- -
ND
Dissolved Ethane
12/30/03
mg/L
0.0002
0.0010
ND
ND
ND
ND
ND ND
-
12/19/07
mg/L
-
20.0
ND
ND
ND
ND
- -
ND
05/01/13
mg/L
0.0031
0.0062
ND
ND
ND
ND
- -
ND
08/14/14
mg/L
0.0031
0.0062
ND
ND
0.0036 J
-
- -
ND
03/10/15
mg/L
0.0031
0.0062
ND
ND
ND
-
- -
ND
08/18/15
mg/L
0.0031
0.0062
0.01
0.01
0.01
-
- -
0.01
02/16/16
mg/L
0.0031
0.0062
ND
ND
ND
-
- -
ND
08/09/16
mg/L
0.0031
0.0062
-
1.6 J
2.6 J
-
- -
-
02/13/17
mg/L
-
-
-
-
-
-
- -
-
08/22/17
mg/L
-
-
-
-
-
-
- -
-
02/05/18
mg/L
-
-
-
-
-
-
- -
-
08/13/18
mg/L
-
-
-
-
-
-
- -
-
02/04/19
mg/L
0.001
0.0010
ND
ND
ND
ND
ND ND
ND
08/06/19
mg/L
0.0012
0.0100
ND
2.0 J
.0041 J
-
- -
ND
02/12/20
mg/L
0.0012
0.0100
ND
0.0026 J
0.0026 J
-
- -
ND
08/27/20
mg/L
0.001
0.0100
ND
ND
ND
-
- -
ND
02/11/21
mg/L
-
-
-
-
-
-
- -
-
Dissolved Ethene
12/01/03
mg/L
0.0003
0.0010
ND
ND
ND
ND
ND ND
-
12/19/07
mg/L
-
20.0
ND
ND
ND
ND
- -
ND
05/01/13
mg/L
0.0031
0.0062
ND
ND
0.0017
ND
- -
ND
08/14/14
mg/L
0.0031
0.0062
ND
ND
ND
-
- -
ND
03/10/15
mg/L
0.0031
0.0062
ND
ND
ND
-
- -
ND
08/18/15
mg/L
0.0031
0.0062
0.01
0.01
0.01
-
- -
0.01
02/16/16
mg/L
0.0031
0.0062
ND
ND
ND
-
- -
ND
08/09/16
mg/L
0.0031
0.0062
-
ND
ND
-
- -
-
02/13/17
mg/L
-
-
-
-
-
-
- -
-
08/22/17
mg/L
-
-
-
-
-
-
- -
-
02/05/18
mg/L
-
-
-
-
-
-
- -
-
08/13/18
mg/L
-
-
-
-
-
-
- -
-
02/04/19
mg/L
0.001
0.001
ND
ND
ND
ND
ND ND
ND
08/06/19
mg/L
0.0012
0.01
ND
ND
.0016 J
-
- -
ND
02/12/20
mg/L
0.0012
0.01
ND
0.0027 J
ND
-
- -
ND
08/27/20
mg/L
0.001
0.01
ND
ND
ND
-
- -
ND
02/11/21
mg/L
-
-
-
-
-
-
- -
-

Parameter
Date
Units
DL RL
MW-1R
MW-2R MW-3R MW-4 MW-5 MW-6
NES-1
Dissolved Methane
12/30/03
mg/L
0.0002 0.0010
ND
0.660 0.130 0.0099 0.0010 ND
-
12/19/07
mg/L
- 10.0
ND
0.116 0.186 ND - -
ND
05/01/13
mg/L
0.0033 0.0066
ND
0.0379 0.100 0.0337 - -
ND
08/14/14
mg/L
0.0033 0.0066
ND
1.29 0.284 - - -
ND
03/10/15
mg/L
0.0033 0.0066
0.0072
0.996 0.158 - - -
ND
08/18/15
mg/L
0.0033 0.0066
0.0027
2.16 0.316 - - -
0.0013
02/16/16
mg/L
0.0033 0.0066
0.007 J
0.87 0.098 - - -
0.0016 J
08/09/16
mg/L
0.0033 0.0066
-
1.85 0.206 - - -
-
02/13/17
mg/L
- -
-
- - - - -
-
08/22/17
mg/L
- -
-
- - - - -
-
02/05/18
mg/L
- -
-
- - - - -
-
08/13/18
mg/L
- -
-
- - - - -
-
02/04/19
mg/L
0.001 0.0010
ND
27.2 ND ND ND ND
ND
08/06/19
mg/L
0.0034 0.0100
ND
5.0 0.486 - - -
ND
02/12/20
mg/L
0.0034 0.0100
ND
4.5 0.376 - - -
ND
08/27/20
mg/L
0.0034 0.0100
ND
6.0 0.497 - - -
ND
02/11/21
mg/L
0.0034 0.0100
ND
6.66 0.519 - - -
ND
Pyruvic Acid
12/19/07
mg/L
- -
2.50
ND 1.50 2.00 - -
1.20
05/01/13
mg/L
2 10
ND
ND ND ND - -
ND
08/14/14
mg/L
0.77 10
ND
ND ND - - -
ND
03/10/15
m g/ L
0.77 10
0.41J
0.41J 0.41J - - -
0.41J
08/18/15
mg/L
0.77 10
ND
ND ND - - -
ND
02/16/16
mg/L
0.77 10
ND
ND ND - - -
ND
08/09/16
mg/L
0.77 10
-
ND ND - - -
-
02/13/17
mg/L
- -
-
- - - - -
-
08/22/17
mg/L
- -
-
- - - - -
-
02/05/18
mg/L
- -
-
- - - - -
-
08/13/18
mg/L
- -
-
- - - - -
-
02/04/19
mg/L
- -
-
- - - - -
-
08/06/19
mg/L
- -
ND
ND ND - - -
ND
02/12/20
mg/L
- -
-
- - - - -
-
08/27/20
mg/L
0.06 0.06
ND
ND ND - - -
ND
02/11/21
mg/L
- -
-
- - - - -
-
Lactic Acid
12/19/07
mg/L
ND
5.40 11.9 3.10 - -
ND
05/01/13
mg/L
2.3 25
ND
ND ND ND - -
ND
08/14/14
mg/L
2.5 25
4.2 J
ND ND - - -
ND
03/10/15
mg/L
2.5 25
ND
ND ND - - -
ND
08/18/15
mg/L
2.5 25
ND
ND ND - - -
ND
02/16/16
mg/L
2.5 25
ND
ND ND - - -
ND
08/09/16
mg/L
2.5 25
-
ND ND - - -
-
02/13/17
mg/L
- -
-
- - - - -
-
08/22/17
mg/L
- -
-
- - - - -
-
02/05/18
mg/L
- -
-
- - - - -
-
08/13/18
mg/L
- -
-
- - - - -
-
02/04/19
mg/L
- -
-
- - - - -
-
08/06/19
mg/L
0.043 0.20
ND
ND 0.087 J - - -
ND
02/12/20
mg/L
- -
-
- - - - -
-
08/27/20
mg/L
0.053 0.053
ND
ND ND - - -
ND
02/11/21
mg/L
- -
-
- - - - -
-

Parameter
Date
Units
DL RL
MW-1R
MW-2R MW-3R MW-4 MW-5 MW-6
NES-1
Acetic Acid
12/19/07
mg/L
ND
ND ND ND - -
ND
05/01/13
mg/L
1.8 5
ND
ND ND ND - -
ND
08/14/14
mg/L
0.81 5.0
ND
ND ND - - -
ND
03/10/15
mg/L
0.81 5.0
ND
ND ND - - -
ND
08/18/15
mg/L
0.81 5.0
ND
ND 0.97 J - - -
ND
02/16/16
mg/L
0.81 5.0
ND
ND ND - - -
ND
08/09/16
mg/L
0.81 5.0
-
ND ND - - -
-
02/13/17
mg/L
- -
-
- - - - -
-
08/22/17
mg/L
- -
-
- - - - -
-
02/05/18
mg/L
- -
-
- - - - -
-
08/13/18
mg/L
- -
-
- - - - -
-
02/04/19
mg/L
- -
-
- - - - -
-
08/06/19
mg/L
0.028 0.10
ND
0.097 J 0.34 - - -
ND
02/12/20
mg/L
- -
-
- - - - -
-
08/27/20
mg/L
0.12 0.12
0.530
4.7 J 0.53 - - -
0.56
02/11/21
mg/L
- -
-
- - - - -
-
Propionic Acid
12/19/07
mg/L
ND
63.7 38.3 12.8 - -
ND
05/01/13
mg/L
1 5
ND
ND ND ND - -
ND
08/14/14
mg/L
0.66 5.0
ND
ND ND - - -
ND
03/10/15
mg/L
0.66 5.0
ND
ND ND - - -
ND
08/18/15
mg/L
0.66 5.0
ND
ND ND - - -
ND
02/16/16
mg/L
0.66 5.0
ND
ND ND - - -
ND
08/09/16
mg/L
0.66 5.0
-
ND ND - - -
-
08/22/17
mg/L
- -
-
- - - - -
-
02/13/17
mg/L
- -
-
- - - - -
-
08/22/17
mg/L
- -
-
- - - - -
-
02/05/18
mg/L
- -
-
- - - - -
-
08/13/18
mg/L
- -
-
- - - - -
-
02/04/19
mg/L
- -
-
- - - - -
-
08/06/19
mg/L
0.004 0.10
-
0.0058 J 0.0045 J - - -
-
02/12/20
mg/L
- -
-
- - - - -
-
08/27/20
mg/L
0.053 0.053
ND
ND ND - - -
ND
02/11/21
mg/L
- -
-
- - - - -
-
Butyric Acid
12/19/07
mg/L
ND
ND ND ND - -
ND
05/01/13
mg/L
0.87 5
ND
ND ND ND - -
ND
08/14/14
mg/L
0.70 5.0
ND
ND ND - - -
ND
03/10/15
mg/L
0.70 5.0
ND
ND ND - - -
ND
08/18/15
mg/L
0.70 5.0
ND
ND ND - - -
ND
02/16/16
mg/L
0.70 5.0
ND
ND ND - - -
ND
08/09/16
mg/L
0.70 5.0
-
ND ND - - -
02/13/17
mg/L
- -
-
- - - - -
-
08/22/17
mg/L
- -
-
- - - - -
-
02/05/18
mg/L
- -
-
- - - - -
-
08/13/18
mg/L
- -
-
- - - - -
-
02/04/19
mg/L
- -
-
- - - - -
-
08/06/19
mg/L
0.011 0.10
-
0.22 ND - - -
-
02/12/20
mg/L
- -
-
- - - - -
-
08/27/20
mg/L
0.058 0.058
ND
ND 0.066 J - - -
ND
02/11/21
mg/L
- -
-
- - - - -
-
Formic Acid
08/06/19
mg/L
0.086 0.50
-
1.10 1.60 - - -
-
02/12/20
mg/L
- -
-
- - - - -
-
08/27/20
mg/L
0.055 0.055
4.9
45.0 4.8 - - -
5.1
02/11/21
mg/L
- -
-
- - - - -
-

Parameter
Date
Units
DL RL
MW-1R
MW-2R MW-3R MW-4 MW-5 MW-6
NES-1
Total Volatile Fatty Acids
12/19/07
mg/L
- -
2.50
69.10 51.70 17.90 - -
1.20
(sum of above 6 acids)
05/01/13
mg/L
- -
ND
ND ND - - -
ND
08/14/14
mg/L
- -
4.2 J
ND ND - - -
ND
03/10/15
mg/L
- -
ND
ND ND - - -
ND
08/18/15
mg/L
- -
ND
ND 0.97 J - - -
ND
02/16/16
mg/L
- -
ND
ND ND - - -
ND
08/09/16
mg/L
- -
-
ND ND - - -
-
02/13/17
mg/L
- -
-
- - - - -
-
08/22/17
mg/L
- -
-
- - - - -
-
02/05/18
mg/L
- -
-
- - - - -
-
08/13/18
mg/L
- -
-
- - - - -
-
02/04/19
mg/L
- -
-
- - - - -
-
08/06/19
mg/L
- -
-
1.32 1.94 - - -
-
02/12/20
mg/L
- -
-
- - -
-
08/27/20
mg/L
- -
5.43
49.70 5.40 - - -
5.66
02/11/21
mg/L
- -
-
- - - - -
-
NOTES:
DL = laboratory detection limit.
RL = laboratory reporting limit.
ND = not detected above detection limit.
J = estimated concentration between the DL and the RL.
- = not analyzed or not applicable.
mg/L = milligrams per liter
my = millivolt
SU = standard unit
nM = nano -Molar
°C = degress Celcius
pS/cm = micro-Siemen per centimeter
ntu = nephelometric turbidity units