8002_Rowan_NeedmoreRoad_CelaneseFibers_Indus_May2020GW_Nov2020GW_FID1584693_20210603

AECOM Environment Prepared for:
CNA Holdings LLC
Irving, Texas
2020 Annual Report
Needmore Road Landfill
Salisbury, North Carolina
Prepared by:
AECOM
Atlanta, GA
60633967
May 2021

A=COM Environment Prepared for:
CNA Holdings LLC
Irving, Texas
2020 Annual Report
Needmore Road Landfill
Salisbury, North Carolina
L
Prepared By
Ishita Mathur
\ y 4 C AR
SEAL
046063
GINE. �.
',lz//NG+Z\AO
Reviewed By
Jing Zhou, Ph.D., P.E.
Prepared by:
AECOM
Atlanta, GA
60633967
May 2021

AECOM Environment i
Contents
1.0 Introduction.................................................................................................................1-1
1.1 Site Background................................................................................................................1-1
2.0 Summary of Monitoring Activities............................................................................2-1
3.0 Summary of May 2020 and November 2020 Monitoring Results ........................... 3-1
3.1 Groundwater Sampling Results.......................................................................................3-1
3.2 Groundwater Sampling Results.......................................................................................3-1
3.2.1 Ethylene Glycol..................................................................................................3-1
3.2.2 1,4-Dioxane........................................................................................................ 3-2
3.2.3 DowTherm ATM.................................................................................................. 3-2
3.3 Surface Water Sampling Results.....................................................................................3-3
3.4 Intermittent Seep Sampling Results.................................................................................3-3
3.5 Phytoremediation System and Landfill Cover Inspections..............................................3-3
4.0 Conclusions................................................................................................................4-1
List of Tables
Table 1 May Groundwater and Surface Water Sampling Plan
Table 2 November Groundwater and Surface Water Sampling Plan
Table 3 Groundwater Elevations
Table 4 Groundwater Analytical Summary
Table 5 Surface Water Analytical Summary
Table 6 Intermittent Seep Water Analytical Summary
Table 7 Summary of Detected Constituents in Groundwater
Table 8 Time vs. Concentration Plots — Ethylene Glycol
Table 9 Time vs. Concentration Plots — 1,4-Dioxane
Table 10 Time vs. Concentration Plots — Diphenyl Ether
May 2021

AECOM
Environment ii
List of Figures
Figure 1 Site Location Map
Figure 2 Site Layout Map
Figure 3 Sample Location Map — May 2020
Figure 4 Sample Location Map — November 2020
Figure 5 Groundwater Elevation Data — November 2020
Figure 6
Ethylene Glycol Map — May 2020
Figure 7
Ethylene Glycol Map — November 2020
Figure 8
1,4-Dioxane Map — May 2020
Figure 9 1,4-Dioxane Map — November 2020
Figure 10 1,1-Biphenyl Map — November 2020
Figure 11 Diphenyl Ether Map — November 2020
List of Appendices
Appendix A May 2020 and November 2020 Laboratory Analytical Reports
Appendix B Completed Inspection Forms for Landfill Cap and Phytoremediation System
May 2021

AECOM
Environment
List of Acronyms
CAP Corrective Action Plan
IMAC Interim Maximum Allowable Concentrations
mg/L milligrams per liter
MNA monitored natural attenuation
MSL mean sea level
NC 2L North Carolina Administrative Code, Title 15A, Subchapter 2L
NCDEQ North Carolina Department of Environmental Quality
NPDES National Pollutant Discharge Elimination System
NRLF Needmore Road Landfill
VFA Volatile Fatty Acid
May 2021

AECOM
Environment 1-1
1.0 Introduction
This annual report has been prepared to present activities completed between January 2020 and
December 2020, and the sampling results for the May and November monitoring events for the
Needmore Road Landfill (NRLF) site. This report includes an updated summary of data and
findings at the site and presents the status of the monitored natural attenuation (MNA) and
phytoremediation programs established in the Corrective Action Plan (CAP).
1.1 Site Background
The NRLF site, located at 345 Messick Farm Road, Woodleaf, Rowan County, North Carolina, was
used until 1990 to dispose of by-products of polyester resin manufacturing from the former Hoechst
Celanese plant located on U.S. Route 70 near Salisbury, North Carolina. These by-products
primarily included waste materials containing ethylene glycol with some other impurities, including
1,4-dioxane, 1,1-biphenyl, and diphenyl ether. There were four main disposal areas at this site, and
they were referred to as Taylor's Pit (0.6 acre), the 14-Acre Site, the 16-Acre Site, and the
Secondary Site (2.6 acres). Taylor's Pit was consolidated into the main part of the landfill prior to
final landfill closure. The site consists of an approximately 243-acre tract of land that is bounded by
the South Yadkin River to the east. The current North Carolina Department of Environmental
Quality (NCDEQ) status of the site is "closed." A site location map is included as Figure 1, and a
site layout map is included as Figure 2.
The landfill lies within the central portion of the Charlotte Metamorphic Belt of the Piedmont
Physiographic Province. Bedrock in this area is composed of a complex series of meta -
sedimentary, meta -volcanic, and igneous intrusive rock types. This geologic matrix has undergone
repeated cycles of folding, faulting, metamorphism, and intrusions, which have resulted in regional
northeasterly strike and southeasterly dip directions.
A basic understanding of the geology at the landfill has been established during several phases of
work, during which numerous monitoring and extraction wells were installed. Based on an
evaluation of the subsurface boring logs, the site is underlain by diorite, gabbro, and granite
bedrock. Some localized gneissic and schistose metamorphism has been noted in several of the
borings drilled at the site. These profiles are generally well -weathered and occur in the zone above
the competent rock.
Historic remedial activities at the landfill include the installation of an impermeable cover on the
landfill, regrading of the surface of the landfill (to improve surface drainage), and the installation of
groundwater extraction wells. Groundwater was extracted and treated by a UV/peroxide oxidation
process and discharged under a National Pollutant Discharge Elimination System (NPDES) permit.
Groundwater extraction was suspended in June 2002 with NCDEQ approval. In 2004,
modifications were made to the drainage system and a phytoremediation system was initiated to
address seepage at the toe of the landfill. The phytoremediation system is positioned downgradient
of the landfill face and upgradient of the intermittent seep location.
Groundwater monitoring data in the reports submitted semiannually from November 2004 until 2007
demonstrated that the existing groundwater impact had been generally contained and was not
expanding. As such, a final CAP was established in 2007 defining a combination of MNA and
May 2021

AECOM
Environment 1-2
phytoremediation as the site remedy. Subsequent monitoring events have reported similarly
successful results.
Biological degradation has been a significant component of natural attenuation of ethylene glycol
and DowTherm ATM components at the site. The original MNA parameters supplemented with the
additional sampling requested by NCDEQ indicate that biological degradation is occurring at the site
to control the ethylene glycol and DowTherm ATM plume. Phytoremediation is currently being
utilized to supplement the MNA, treat the 1,4-dioxane plume through evapotranspiration, and to
provide additional hydraulic control.
Groundwater monitoring, surface water monitoring, intermittent seep monitoring, and regular
inspections of the phytoremediation system and landfill cap have been ongoing at the site in
accordance with the schedule detailed in the CAP and were revised in early 2009. Based on the
site understanding and long-term data, the levels of impact in groundwater are not anticipated to
exceed surface water quality standards nor pose an unacceptable risk to the receptors. Based on
these data, the reports support continued MNA with phytoremediation as a viable remedy, as
described in the CAP.
Because the primary constituents at the site have generally remained stable since 2007, and
because the MNA and phytoremediation systems have remained effective as designed, AECOM
recommended in the semiannual report submitted to NCDEQ in May 2014 that the monitoring
continue to be conducted semiannually in May and November and the reporting frequency be
reduced from semiannual to annual. The NCDEQ approved the reduction of the reporting
frequency in a letter dated September 10, 2014, and an annual site report has been prepared each
year since May 2015.
May 2021

AECOM
Environment 2.1
2.0 Summary of Monitoring Activities
The ongoing MNA/phytoremediation activities for the NRLF site include:
• semiannual groundwater sampling and analysis;
• semiannual surface water sampling and analysis;
• semiannual sampling and analysis of intermittent seep at toe of landfill;
• continued ongoing maintenance and monthly inspection of the landfill cap; and
• continued ongoing maintenance and monthly inspections of the phytoremediation tree farm.
The May and November sampling events were conducted using methodologies detailed in the CAP.
A reduced scope plan for the May events was approved in 2009 and is shown in Table 1. The
November events include the full sampling plan originally presented in the CAP, and the plan is
shown in Table 2. Prior to sampling, depths to groundwater were measured at the wells to be
sampled. These data are shown in Table 3 and are resolved to the groundwater elevations used to
plot the site potentiometric maps.
The replacement of a Volatile Fatty Acids (VFAs) analysis with an acetic acid analysis was
approved by NCDEQ in 2010.
Sample location maps for the May and November sampling events are included as Figure 3 and
Figure 4, respectively. Laboratory analytical reports are included in Appendix A.
Completed monthly inspection forms for the phytoremediation system and landfill cap for January
through December 2020 are included in Appendix B.
May 2021

AECOM
Environment 3-1
3.0 Summary of May 2020 and November 2020 Monitoring
Results
Nine groundwater monitoring wells, one surface water location, and one intermittent seep location
were sampled during the May monitoring event. Fourteen groundwater monitoring wells, four
surface water locations, and two intermittent seep locations were sampled during the November
monitoring event. No sample was collected from intermittent seep location CSW-2 in May 2020
due to the location being dry during the sampling. Laboratory analytical results are summarized in
Table 4 (groundwater), Table 5 (surface water), and Table 6 (intermittent seep). Complete
analytical reports are included as Appendix A. Previous reports identified that the primary
constituents in groundwater are ethylene glycol, 1,4-dioxane, 1,1-biphenyl, and diphenyl ether.
Monitoring updates for these constituents are presented in the following sections.
3.1 Groundwater Sampling Results
During the May 2020 sampling event, groundwater elevations ranged from approximately 655.08
feet above mean sea level (MSL) at B-24A to approximately 705.98 feet above MSL at B-10.
During the November 2020 sampling event, groundwater elevations ranged from approximately
656.02 feet above mean sea level (MSL) at B-24A to 714.16 feet above MSL at B-32B. The
groundwater elevation data are presented in Table 3. The groundwater elevations in 2020 appear
to be consistent with typical measurements from the previous years.
The May 2020 and November 2020 groundwater elevation data are consistent with the
groundwater flow patterns established in the CAP (October 2007), which indicated that
groundwater under the site generally flows northeast toward the South Yadkin River. Groundwater
elevations collected during the November 2020 event were used to develop the potentiometric
surface presented on Figure 5.
3.2 Groundwater Sampling Results
3.2.1 Ethylene Glycol
Historically, ethylene glycol remained below analytical reporting limits (non -detect) in samples
collected from 2007 to November 2012. Fluctuating detections have been noted at several wells
since May 2013, including B-01, B-09C, B-10, B-23A, and B-23B, and some detections were above
the North Carolina Administrative Code, Title 15A, Subchapter 2L (NC 2L) standard of 10 milligrams
per liter (mg/L). During both the May 2020 sampling event and November 2020 sampling event,
ethylene glycol was not detected from any of the wells sampled.
The low or non-existent detections in the wells from 2007 to 2012 support the ethylene glycol
natural attenuation conclusions presented in the 2007 CAP. The landfill cap has significantly
reduced or eliminated the transport of ethylene glycol from the landfill into groundwater, and the
concentrations of ethylene glycol which had entered the groundwater prior to the installation of the
cap, were decreased or attenuated (CAP, 2007). Since ethylene glycol is fully miscible in water and
mobile, ongoing occasional detections were anticipated in the 2007 CAP. Future fluctuations
between detections within historical ranges and non -detect results are expected as the remaining
material migrates and rapidly degrades. Detections do not suggest a deficiency in the landfill cover,
May 2021

AECOM Environment 3-2
and the fluctuations back to non -detect continue to confirm MNA as an ongoing remedy. Ethylene
glycol will continue to be monitored.
Historic data summaries for ethylene glycol and other site parameters are presented in Table 7.
Selected trend plots of ethylene glycol concentrations over time are presented in Table 8. Ethylene
glycol concentrations are included on Figure 6 for the May 2020 sampling event and Figure 7 for
the November 2020 sampling event.
3.2.2 1,4-Dioxane
1,4-Dioxane has been historically detected in wells near the four former disposal sites. During the
May 2020 and November 2020 sampling event, every well sampled exhibited a 1,4-dioxane
concentration higher than the NC 2L standard of 0.003 mg/L. The concentration trend plots
presented in Table 9 indicate that 1,4-dioxane concentrations in most wells are generally either
stable or declining.
Data used to generate the plots in Table 9 can be found in Table 7. Plume maps for 1,4-dioxane
are included as Figure 8 for the May sampling event and Figure 9 for the November sampling
event.
3.2.3 DowTherm ATM
1,1-Biphenyl
1,1-Biphenyl results are presented in Table 4, and the 1,1-biphenyl plume map for the November
2020 event is shown on Figure 10.
Since 2005, 1,1-biphenyl has only been consistently detected in samples collected from monitoring
well B-10. The result from B-10 was estimated ("J") to be 0.0711 mg/L in May 2020 (duplicate
0.113 J mg/L) and 0.0694 mg/L in November 2020, similar to the recent sampling results and below
the NC 2L standard of 0.40 mg/L. Historic data for 1,1-biphenyl at B-10 have typically remained
below the 0.40 mg/L level but has occasionally exceeded this level. The historic maximum was
0.461 mg/L, which was reported in 1999. 1,1-Biphenyl was not detected in other wells in 2020.
Diphenyl Ether
NCDEQ has not developed a 2L standard for diphenyl ether, therefore, the Interim Maximum
Allowable Concentration (IMAC) (0.10 mg/L, effective since April 2011) is used as the screening
criteria for this constituent at the site. Diphenyl ether has been historically detected at several wells
located near the former disposal sites and at the downgradient wells. Historically, diphenyl ether
ranged from approximately 1.1 to 4.5 mg/L, and wells have demonstrated a decreasing trend since
December 2009. The May 2020 and November 2020 diphenyl ether data are presented in Table 4.
Diphenyl ether was detected in well B-10 in May and in wells B-01, B-09C, B-10, B-22B, B-23A,
B-23B, and B-24B in November. Throughout the 2020 sampling events, concentrations ranged
from 0.0104 mg/L in B-24B to 1.01 J mg/L (duplicate) in B-10. B-10 consistently has the highest
diphenyl ether concentrations; however, the concentrations demonstrate a decreasing trend since
2009. Selected diphenyl ether trends are shown in Table 10 and on Figure 11.
The data continue to indicate that migration of 1,1-biphenyl and diphenyl ether is being controlled
by the landfill cap and through natural attenuation mechanisms.
May 2021

AECOM
Environment 3-3
3.3 Surface Water Sampling Results
Surface water monitoring was conducted at one location (SW-5) during the May 2020 sampling
event and at four locations (SW-3, SW-5, SW-7, and SW-8) during the November 2020 event. The
surface water results are summarized in Table 5.
During both the May 2020 and November 2020 sampling events, no detections of
1,4-dioxane, ethylene glycol, diphenyl ether, or 1,1-biphenyl were noted at the surface water
monitoring locations.
3.4 Intermittent Seep Sampling Results
CSW-1 and CSW-2 are monitoring locations associated with the intermittent seep, and both
locations have been dry for a substantial number of sampling events since the phytoremediation
program was initiated. CSW-1 is located at the initial discharge point of the seep, and CSW-2 is
located downstream in the creek bed fed by the seep.
Intermittent seep monitoring was conducted at one location (CSW-1) during the May 2020 sampling
event and 1,4-Dioxane was detected = with a concentration of 0.58 mg/L. Intermittent seep
monitoring was conducted at two locations (CSW-1 and CSW-2) during the November 2020
sampling event. 1,4-Dioxane was detected at location CSW-1 with a concentration of 0.368 mg/L
and at location CSW-2 with a concentration of 0.279 mg/L. The intermittent seep water results are
summarized in Table 6.
For CSW-1 and CSW-2, monitoring events prior to construction of the phytoremediation system
indicated concentrations of 1,4-dioxane at CSW-1 of approximately 0.5 mg/L and lower
concentrations at downgradient CSW-2. The 1,4-dioxane concentrations decreased after the
construction of the phytoremediation system and maintained below 0.2 mg/L from 2012-2019,
indicating that the phytoremediation continues to provide control of the 1,4-dioxane mass in the
treatment area. During the 2020 sampling events, the 1,4-dioxane concentration in CSW-1 and
CSW-2 were higher than recent sampling results, however, considering that the concentration in
CSW-1 in November 2020 decreased by 40% from May 2020, the elevated 1,4-dioxane
concentrations in the intermittent seep locations may be temporary, and we will continue monitoring
1,4-dioxane in future sampling event and evaluate the concentration trend.
3.5 Phytoremediation System and Landfill Cover Inspections
Monthly inspections of the phytoremediation system and landfill cap were conducted for the period
of January through December 2020 and are presented in Appendix B. Based on these inspections,
most of the trees remained in good health during this reporting period.
The phytoremediation system was originally installed in 2004. A supplemental new tree planting
event was conducted in 2012, including the removal of dead trees and planting of 30 new trees and
20 whips. Since the 2012 planting, some poplar trees were lost. The phytoremediation system
status was evaluated in 2019, and another supplemental new tree planting was conducted at the
site in February and March 2020. A total of 12 dead poplar trees were removed by mobile crane in
February 2020. A total of 100 black willow 4-foot whips were planted in March 2020. The trees
were planted in 6-inch diameter by 12-inch deep holes, and the holes were backfilled with compost
followed by fertilization. Most of the newly planted trees are in good health through 2020.
May 2021

AECOM
Environment 3-4
The landfill cap has remained in good condition and permanent edge -of -waste markers were
installed during this reporting period per NCDEQ request.
The landfill cover has been in place since the early 1990s. The phytoremediation system was first
implemented in 2004 and has been upgraded and maintained consistently since that time.
Groundwater monitoring has consistently demonstrated that these systems remain effective and
along with MNA maintain stable to improving conditions.
Routine mowing and cover service will continue. Maintenance of the phytoremediation system will
also be continued. The maintenance will include periodic removal of trees based on damage, age,
or overcrowding, and additional trees will be installed as needed to continue meeting the objectives
of the CAP.
May 2021

AECOM
Environment 4-1
4.0 Conclusions
The CAP was submitted in November 2007, and subsequent semiannual and annual reports
describe stabilized or declining concentrations and present the extent of the various plumes within
the Needmore Road Landfill. This report includes the field activities from January to December
2020 and the analytical results of the May 2020 and November 2020 sampling events. Semiannual
monitoring and monthly inspections of the phytoremediation system were conducted during this
reporting period.
Ethylene glycol was not detected from any wells sampled in 2020.
1,4-dioxane continues to be detected above the NC 2L standard and concentrations remain stable
or declining in most wells.
1,1-Biphenyl has only been consistently detected at monitoring well B-10, and historical data for this
well indicate a decreasing trend since 2008. Diphenyl ether concentrations in the former disposal
areas have decreased or stabilized over time due to the natural attenuation processes.
The phytoremediation system and landfill cap remain in good condition. A total of 100 black willow
4-foot whips were planted in March 2020. Future maintenance of the phytoremediation system,
including pruning, removal, and/or installation of new trees, will be continued as described in the
CAP.
The monitoring of groundwater, surface water, and the intermittent seep will be continued in May
and November as shown in Tables 1 and 2, respectively, and the next annual report will be
submitted in May 2022.
May 2021

Tables

Table 1
May Groundwater and Surface Water Sampling Plan
CNA Holdings LLC — Needmore Road Landfill
AECOM Project No. 60633967
Location
1,4-Dioxane
DowTherm ATM
Ethylene
Glycol
VOCs*
MNA**
B-01
X
X
X
B-09C
X
X
X
B-10
X
I X
X
X
B-12
X
X
X
B-17C
X
I
X
B-22B
X
X
B-23A
X
I
X
X
B-23B
X
X
X
B-24A
X
X
SW-5
X
X
X
CSW-1
X
CSW-2
X
Notes:
* VOCs to be analyzed annually (November only; revised from CAP schedule of May only)
** MNA: alkalinity, nitrate, phosphate, sulfate, DO, ORP, and ferrous iron
Page 1 of 25 5/28/2021

Table 2
November Groundwater and Surface Water Sampling Plan
CNA Holdings LLC — Needmore Road Landfill
AECOM Project No. 60633967
Location
1,4-Dioxane
DowTherm
A—
Ethylene
Glycol
VOCs*
MNA**
Expanded
MNA***
B-01
X
X
X
X
X
X
B-09C
X
X
X
X
X
B-10
X
X
X
X
X
X
B-12
X
X
X
B-17B
X
X
X
X
B-17C
X
X
X
X
B-21 B
X
X
B-22A
X
X
X
X
X
B-22B
X
X
X
X
X
B-23A
X
X
X
X
X
X
B-23B
X
X
X
X
X
X
B-24A
X
X
X
X
B-24B
X
X
X
X
B-32B
X
X
X
X
X
CSW-1
X
CSW-2
X
SW-3
X
X
X
SW-5
X
X
X
SW-7
X
X
X
SW-8
X
X
X
Notes:
* VOCs to be analyzed annually (November only; revised from CAP schedule of May only)
** MNA: alkalinity, nitrate, phosphate, sulfate, DO, ORP, and ferrous iron
*** Expanded MNA: TOC, ethane, ethene, methane, carbon dioxide, hydrogen, and acetic acid
Page 2 of 25 5/28/2021

Table 3
Groundwater Elevations
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
Well ID
Date
Gauged
Top of
Casing (TOC)
Depth to
Water
Groundwater
Elevation
MSL
Feet below
TOC
MSL
B-01
5/18/2020
756.55
57.86
698.69
11/3/2020
57.21
699.34
B-09C
5/18/2020
713.44
35.02
678.42
11 /2/2020
35.54
677.90
B-10
5/18/2020
751.78
45.80
705.98
11/3/2020
45.72
706.06
B-12
5/18/2020
677.11
18.03
659.08
11/3/2020
18.55
658.56
B-17B
11/3/2020
678.32
15.41
662.91
B-17C
5/18/2020
677.06
15.80
661.26
11/3/2020
15.90
661.16
B-21 B
11 /2/2020
676.73
10.47
666.26
B-22A
11/3/2020
661.66
2.53
659.13
B 22B
5/18/2020
660.15
0.62
659.53
11/3/2020
0.52
659.63
B-23A
5/18/2020
665.73
8.20
657.53
11 /2/2020
6.49
659.24
B 23B
5/18/2020
665.74
7.71
658.03
11 /2/2020
6.67
659.07
B-24A
5/18/2020
659.10
4.02
655.08
11 /2/2020
3.08
656.02
B-24B
11 /2/2020
659.19
2.27
656.92
B-32B
11/3/2020
744.27
30.11
714.16
Notes:
MSL - mean sea level
TOC - top of casing
Page 3 of 25 5/28/2021

Table 4
Groundwater Analytical Summary
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
Location
B-01
5/18/2020
B-01-051820
B-01
11/3/2020
B-01-110320
B-09C
5/18/2020
B-09C-051820
B-09C
11/2/2020
B-09C-110220
B-09C
11/2/2020
B-99C-110220
B-10
5/18/2020
B-10-051820
B-10
5/18/2020
B-99-051820
B-10
11/3/2020
B-10-110320
B-12
5/18/2020
B-12-051820
B-12
11/2/2020
B-12-110320
Collection Date
Sample Name
Chemical Units INC 2L Standard
Organic Compounds
1,1'-Biphenyl
mg/L
0.4
<0.0100
<0.0100
<0.0100
0.0711 J
0.113 J
0.0694
<0.0100
<0.0100
Diphenyl ether
mg/L
0.1
0.0300
0.0255
0.0244
0.643 J
1.01 J
0.698
<0.0100
<0.0100
Ethylene Glycol
m /L
10
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
1,4-Dioxane
mg/L
0.003
1.51
1.51
0.756
0.743
0.686
0.219
0.179
0.197
2.13 J
2.4
Acetone
mg/L
6
0.635
2.66
2.68
<0.0250
2-Butanone
mg/L
4
0.371
0.451
0.453
<0.0050
Chlorobenzene
mg/L
0.05
<0.0025
<0.0125
<0.0100
<0.0010
Chloroethane
mg/L
3
0.0192
<0.0125
<0.0100
0.0526
1,1-Dichloroethane
mg/L
0.006
0.0158
<0.0125
<0.0100
0.0216
1,1-Dichloroethene
mg/L
0.35
<0.0025
<0.0125
<0.0100
<0.0010
4-Methyl-2-Pentanone
mg/L
0.0248
0.0875
0.0885
<0.0050
1,4-Dichlorobenzene
mg/L
<0.0025
<0.0125
<0.0100
0.0050
Toluene
mg/L
0.0041
<0.0125
<0.0100
<0.0010
Vinyl chloride
mg/L
<0.0025
<0.0125
<0.0100
0.0019
MINA Parameters
Alkalinity
mg/L
1390
1380
2420
2790
410
512
504
360
391
Nitrate -as -nitrogen
mg/L
10
<0.040
<0.040 UJ
<0.040
<0.040
<0.040 UJ
<0.040
<0.040
<0.040
<0.040
Nitrite -as -nitrogen
mg/L
1
0.19
0.22 J-
0.072
0.18
0.076
0.078
0.057
<0.040
<0.040
Orthophosphate
mg/L
0.73
<0.25
0.12
<0.25
0.17 J
0.39 J
0.32 J-
0.064
0.25 J-
Sulfate
mg/L
250
6.9
9.2
<1.0
1.2
<1.0
<1.0
<1.0
1.1
1.3 J+
Total Organic Carbon 1
mg/L
884
20.4
Total Organic Carbon 2
mg/L
900
20.7
Total Organic Carbon 3
mg/L
914
20.7
Total Organic Carbon 4
mg/L
908
21.0
Total organic carbon average
mg/L
901
20.7
Acetic Acid
mg/L
<5.0
1.6
Methane
mg/L
35
35
Ethane
mg/L
<0.0010
<0.0010
Ethene
mg/L
<0.0010
<0.0010
Carbon Dioxide
mg/L
293
195
Hydrogen
nM
<1.9
<1.9
Field Parameters
Dissolved Oxygen
mg/L
0.04
0.04
0.02
0.01
0.10
0.19
0.97
0.69
Iron, Ferrous
mg/L
5.2
4.2
6.2
4.8
3.4
2.9
0.0
0.8
ORP
mV
-90.2
-174.7
-82.2
-154.7
-31.7
-112.2
126.0
-9.7
pH
SU
6.24
6.59
6.42
6.74
6.29
6.56
6.45
6.77
Specific Conductance
umhos/cm
3142
2063
3893
2825
918
710
703
538.9
Temperature
degrees C
21.60
18.80
17.80
16.10
17.60
17.30
17.90
15.00
Turbidity
NTU
20.6
22.9
6.9
6.4
2.1
7.0
2.9
5.6
Notes:
IMAC - Interim Maximum Allowable Concentration
site -specific target chemical
-- no standard specified under 15A NCAC 2L.0202
mg/L - milligrams per liter
my - millivolts
SU - standard units
umhos/cm - micromhos per centimeter
degrees C - degrees Celsius
NTU - Nephelometric Turbidity Units
NA - Not Analyzed
Bold - Analyte detected by the laboratory
Bold and shaded - Concentration exceeds the INC 2L limit
J: The analyte was positively identified. The associated numerical value
is the approximate concentration of the analyte in the sample.
J+: The analyte was positively identified. The associated numerical value
is the approximate concentration of the analyte in the sample biased high.
J-: The analyte was positively identified. The associated numerical value
is the approximate concentration of the analyte in the sample biased low.
UJ: The analyte was not detected; however, the reported quantitation limit is
approximated and may be inaccurate or imprecise.
Page 4 of 25 5/28/2021

Table 4
Groundwater Analytical Summary
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
Location
B-17B
11/3/2020
B-17B-110320
B-17C
5/18/2020
B-17C-051820
B-17C
11/3/2020
B-17C-110320
B-21B
11/2/2020
B-21B-110220
B-22A
11/3/2020
B-22A-110320
B-22B
5/18/2020
13-2213-051820
B-22B
11/3/2020
13-2213-110320
B-23A
5/18/2020
B-23A-051820
B-23A
11/2/2020
B-23A-110220
B-23B
5/18/2020
13-2313-051820
B-23B
11/2/2020
13-2313-110220
Collection Date
Sample Name
Chemical Units NC 2L Standard
Organic Compounds
1,1'-Biphenyl
mg/L
0.4
<0.0100
<0.0100
<0.0100
<0.0100
<0.0100
<0.0100
Diphenyl ether
mg/L
0.1
<0.0100
<0.0100
<0.0100
0.0312
0.0431
0.0696
Ethylene Glycol
m /L
10
<50.0
<50.0
<50.0
<50.0
1,4-Dioxane
mg/L
0.003
0.0786
1.32
1.64
0.0357
1.27
1.33
1.35
2.92
3.47
2.63
3.15
Acetone
mg/L
6
<0.0250
<0.0250
5.55
5.07
2-Butanone
mg/L
4
<0.0050
<0.0050
0.846
0.708
Chlorobenzene
mg/L
0.05
0.0055
0.0104
<0.0250
<0.0250
Chloroethane
mg/L
3
<0.0010
0.0167
<0.0250
0.0296
1,1-Dichloroethane
mg/L
0.006
0.0042
<0.0010
0.0396
<0.0250
1,1-Dichloroethene
mg/L
0.35
0.0023
<0.0010
<0.0250
<0.0250
4-Methyl-2-Pentanone
mg/L
<0.0050
<0.0050
<0.125
<0.125
1,4-Dichlorobenzene
mg/L
<0.0010
<0.0010
<0.0250
<0.0250
Toluene
mg/ L
<0.0010
<0.0010
<0.0250
<0.0250
Vinyl chloride
mg/L
0.0011
<0.0010
<0.0250
<0.0250
MINA Parameters
Alkalinity
mg/L
217
367
417
239
564
833
939
3060
3290
2300
2450
Nitrate -as -nitrogen
mg/L
10
0.044
<0.040
<0.040
<0.040
<0.040
<0.040
<0.040
<0.040 UJ
<0.040 UJ
<0.040
<0.040
Nitrite -as -nitrogen
mg/L
1
<0.040
<0.040
<0.040
<0.040
0.11
<0.040
0.049
0.041 J-
0.046
0.099
0.16
Orthophosphate
mg/L
0.22 J-
0.10
0.24 J-
0.10 J-
<0.25
<0.050
0.14 J-
0.67
0.34 J
0.54
<0.25 UJ
Sulfate
mg/L
250
2.6
1.2
1.2
18.6
<1.0
<1.0
<1.0
4.6
5.1 J+
4.3
4.7
Total Organic Carbon 1
mg/L
1.8
3.2
3.9
6.3
2410
1890
Total Organic Carbon 2
mg/L
1.6
3.3
4.0
6.0
2390
1910
Total Organic Carbon 3
mg/L
1.5
3.2
4.0
6.1
2400
1920
Total Organic Carbon 4
mg/L
1.6
3.2
4.0
6.0
2390
1950
Total organic carbon average
mg/L
1.6
3.2
4.0
6.1
2400
1920
Acetic Acid
mg/L
0.52
0.52
6.1
1.1
2700
2200
Methane
mg/ L
0.2
0.096
0.1
42
12
16
Ethane
mg/L
<0.0010
0.0011
0.0043
0.0027
0.0026
0.0012
Ethene
mg/L
<0.0010
<0.0010
0.0013
<0.0010
0.0061
0.0023
Carbon Dioxide
mg/L
98.1
89.2
168
160
335
301
Hydrogen
nM
<1.9
1.9
<1.9
<1.9
<1.9
<1.9
Field Parameters
Dissolved Oxygen
mg/L
0.05
0.42
0.56
1.28
0.06
0.03
0.02
0.45
0.09
0.36
0.03
Iron, Ferrous
mg/L
1.8
0.0
1.4
1.0
4.6
4.8
3.2
3.0
2.8
3.4
3.8
ORP
mV
-93.4
101.8
-42.0
9.0
-138.7
-69.3
-140.9
-118.7
9.6
-89.5
-117.8
pH
SU
6.60
6.50
6.93
6.98
6.86
6.53
6.86
6.29
6.46
6.50
6.53
Specific Conductance
umhos/cm
332.1
704
560.9
487
774
1340
1057
6122
3368
4673
2915
Temperatur
1 degrees C
1
1 14.70
1 16.40
1 15.10
1 16.00
1 12.30
1 16.10
1 14.70
1 18.90
1 13.10
1 17.80
1 14.80
Turbidity
I NTU
1
1 7.7
1 2.9
1 6.2
1 2.7
1 5.1
1 4.2
1 4.8
1 5.5
1 4.5
1 16.9
1 6.0
Notes:
IMAC - Interim Maximum Allowable Concentration
site -specific target chemical
-- no standard specified under 15A NCAC 2L.0202
mg/L - milligrams per liter
mV - millivolts
SU - standard units
umhos/cm - micromhos per centimeter
degrees C - degrees Celsius
NTU - Nephelometric Turbidity Units
NA - Not Analyzed
Bold - Analyte detected by the laboratory
Bold and shaded - Concentration exceeds the NC 2L limit
J: The analyte was positively identified. The associated numerical value
is the approximate concentration of the analyte in the sample.
J+: The analyte was positively identified. The associated numerical value
is the approximate concentration of the analyte in the sample biased high.
J-: The analyte was positively identified. The associated numerical value
is the approximate concentration of the analyte in the sample biased low.
UJ: The analyte was not detected; however, the reported quantitation limit is
approximated and may be inaccurate or imprecise.
Page 5 of 25 5/28/2021

Table 4
Groundwater Analytical Summary
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
Location
B-24A
5/18/2020
B-24A-051820
B-24A
11/2/2020
B-24A-110220
B-24B
11/2/2020
13-2413-110220
B-32B
11/3/2020
13-3213-110320
Collection Date
Sample Name
Chemical Units INC 2L Standard
Organic Compounds
1,1'-Biphenyl
mg/L
0.4
<0.0100
<0.0100
<0.0100
Diphenyl ether
mg/L
0.1
<0.0100
0.0104
<0.0100
Ethylene Glycol
m /L
10
<5.0
1,4-Dioxane
mg/L
0.003
0.162
0.182
0.103
0.0034
Acetone
mg/L
6
<0.0250
<0.0250
2-Butanone
mg/L
4
<0.0050
<0.0050
Chlorobenzene
mg/L
0.05
<0.0010
<0.0010
Chloroethane
mg/L
3
0.0011
0.0041
1,1-Dichloroethane
mg/L
0.006
0.0103
<0.0010
1,1-Dichloroethene
mg/L
0.35
0.0019
<0.0010
4-Methyl-2-Pentanone
mg/L
<0.0050
<0.0050
1,4-Dichlorobenzene
mg/L
<0.0010
<0.0010
Toluene
mg/L
<0.0010
<0.0010
Vinyl chloride
mg/L
<0.0010
<0.0010
MINA Parameters
Alkalinity
mg/L
347
390
428
129
Nitrate -as -nitrogen
mg/L
10
<0.040
<0.040
<0.040
0.068
Nitrite -as -nitrogen
mg/L
1
<0.040
<0.040
<0.040
<0.040
Orthophosphate
mg/L
0.11
0.16 J-
0.064 J-
<0.050 UJ
Sulfate
mg/L
250
<1.0
<1.0
<1.0
<1.0
Total Organic Carbon 1
mg/L
2.4
Total Organic Carbon 2
mg/L
2.3
Total Organic Carbon 3
mg/L
2.3
Total Organic Carbon 4
mg/L
2.4
Total organic carbon average
mg/L
2.4
Acetic Acid
mg/L
1.0
Methane
mg/L
3.1
Ethane
mg/L
<0.0010
Ethene
mg/L
<0.0010
Carbon Dioxide
mg/L
37.1
Hydrogen
nM
<1.9
Field Parameters
Dissolved Oxygen
mg/L
0.43
0.72
0.72
0.44
Iron, Ferrous
mg/L
2.6
3.6
3.2
3.4
ORP
mV
-30.4
-36.9
-72.9
-77.9
pH
SU
6.48
6.80
6.87
6.86
Specific Conductance
umhos/cm
624
636
701
196.1
Temperature
degrees C
17.90
12.60
12.50
16.90
Turbidity
NTU
3.1
3.6
4.0
7.2
Notes:
IMAC - Interim Maximum Allowable Concentration
site -specific target chemical
-- no standard specified under 15A NCAC 2L.0202
mg/L - milligrams per liter
my - millivolts
SU - standard units
umhos/cm - micromhos per centimeter
degrees C - degrees Celsius
NTU - Nephelometric Turbidity Units
NA - Not Analyzed
Bold - Analyte detected by the laboratory
Bold and shaded - Concentration exceeds the NC 2L limit
J: The analyte was positively identified. The associated numerical value
is the approximate concentration of the analyte in the sample.
J+: The analyte was positively identified. The associated numerical value
is the approximate concentration of the analyte in the sample biased high.
J-: The analyte was positively identified. The associated numerical value
is the approximate concentration of the analyte in the sample biased low.
UJ: The analyte was not detected; however, the reported quantitation limit is
approximated and may be inaccurate or imprecise.
Page 6 of 25 5/28/2021

Table 5
Surface Water Analytical Summary
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
Location ID
SW-3
11/2/2020
SW-3-110220
SW-5
5/18/2020
SW-5-051820
SW-5
11/2/2020
SW-5-110220
SW-7
11/2/2020
SW-7-110220
SW-8
11/2/2020
SW-8-110220
Collection Date
Sample Name
Chemical Units
Organic Compounds
1,1'-Biphenyl
m /L
<0.0100
<0.0100
<0.0100
<0.0100
<0.0100
Di hen I ether
m /L
<0.0100
<0.0100
<0.0100
<0.0100
<0.0100
Ethylene Glycol
m /L
<5.0
<5.0
<5.0
<5.0
<5.0
1,4-Dioxane
m /L
<0.0020
<0.0020
<0.0020
<0.0020
<0.0020
Field Parameters
Dissolved Oxygen
m /L
7.61
7.05
7.73
7.88
8.66
ORP
mV
84.2
82.3
91.6
92.9
-70.8
pH
SU
7.48
7.74
7.56
7.73
8.23
Specific Conductance
umhos/cm
64.6
198
70.8
157.3
64.4
Temperature
degrees C
13.50
19.70
13.00
13.00
12.60
Turbidity
NTU
37.0
16.3
34.0
37.0
24.8
Notes:
mg/L - milligrams per liter
mV - millivolts
SU - standard units
umhos/cm - micromhos per centimeter
degrees C - degrees Celsius
NTU - Nephelometric Turbidity Units
Page 7 of 25 5/28/2021

Table 6
Intermittent Seep Water Analytical Summary
CNA Holdings LLC — Needmore Road Landfill
AECOM Project No. 60633967
Location ID
CSW-1
5/18/2020
CSW-1-051820
Collection Date
Sample Name
Chemical
Units
Organic Compounds
1,4-Dioxane
mg/L
0.58
Field Parameters
Dissolved Oxygen
m /L
6.81
ORP
mV
57.0
pH
SU
7.04
Specific Conductance
umhos/cm
354
Temperature
degrees C
15.20
Turbidity
NTU
6.9
Notes:
mg/L — milligrams per liter
mV — millivolts
SU — standard units
umhos/cm — micromhos per centimeter
degrees C — degrees Celsius
NTU — Nephelometric Turbidity Units
Page 8 of 25 5/28/2021

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-01
Jun-04
<0.05
4.07
<28
0.0723
Nov-04
<0.01
0.202
492
0.0211
May-05
<2.5
2.93
1160
<2.5
Nov-05
<0.01
3.69
<70
0.02
May-06
<0.02
2.75
93.9
0.0419
Nov-06
<0.01
4.68
2000
0.0446
May-07
<0.01
3.43
<140
0.0716
Nov-07
<0.04
3.01
<7
0.0662
May-08
<0.04
2.15
<7
0.0635
Nov-08
<0.01
3.31
<7
0.0565
May-09
NA
2.26
<7
NA
Dec-09
<0.01
3.54
<35
0.0423
May-10
NA
3.56
<35
NA
Nov-10
<0.01
3.24
<35
0.0811
May-11
NA
2.15
NA
NA
Nov-11
<0.01
3.25
<35
0.083
May-12
NA
3.85
NA
NA
Nov-12
<1
3.41
<14
<1
May-13
NA
3.07
254
NA
Nov-13
<0.1
2.74
38.5
<0.1
May-14
NA
1.96
796
NA
Nov-14
<0.01
3.27
648
0.0858
May-15
NA
2.89
<5.0
NA
Nov-15
<0.01
2.64
<50
0.122
May-16
NA
2.37
<50
NA
Nov-16
<0.1
2.18
751
<0.1
May-17
NA
0.242
266
NA
Nov-17
0.0101
1.86
198
0.132
May-18
NA
1.93
<10.0
NA
Nov-18
<0.0100
2.13
51.9
0.0223
May-19
NA
1.81
<5.0
NA
Nov-19
<0.0100
1.55
<50.0
0
May-20
N/A
1.51
<5.0
N/A
Nov-20
<0.0100
1.51
<5.0
0.0300
Page 9 of 25 5/28/2021

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-09C
Jun-04
<0.5
0.791
<70
<0.5
Nov-04
<0.05
1.04
1420
0.0545
May-05
<0.2
0.776
<70
<0.2
Nov-05
<0.01
1.31
363
0.0324
May-06
<0.02
0.668
85.8
0.0492
Nov-06
<0.01
1.29
2020
<0.01
May-07
<0.01
1.11
<140
0.0377
Nov-07
<0.01
0.995
<7
0.0352
May-08
<0.01
0.486
<7
0.0312
Nov-08
<0.01
1.11
<7
0.0438
May-09
NA
0.873
<7
NA
Dec-09
<0.01
1.15
<35
0.0581
May-10
NA
1.03
<35
NA
Nov-10
<0.01
0.951
<35
0.0542
May-11
NA
0.782
NA
NA
Nov-11
<0.01
1.1
<35
0.0451
May-12
NA
1.46
NA
NA
Nov-12
<0.01
1.15
<14
0.0255
May-13
NA
0.803
448
NA
Nov-13
<0.01
0.766
77
0.0272
May-14
NA
0.86
288
NA
Nov-14
<0.01
0.893
406
0.029
May-15
NA
0.972
<5.0
NA
Nov-15
<0.01
0.909
<500
0.0106
May-16
NA
0.954
<50
NA
Nov-16
<0.01
0.796
330
0.0157
May-17
NA
0.56
192
NA
Nov-17
<0.0100
0.906
122
0.0269
Nov-17
<0.0100
0.81
NA
0.026
May-18
NA
0.689
<10.0
NA
Nov-18
<0.0100
0.935
197
<0.0100
Nov-18
<0.0100
0.964
NA
<0.0100
May-19
NA
0.85
<5.0
NA
Nov-19
<0.0100
0.886
<50.0
0
Nov-19
<0.0100
0.848
NA
0
May-20
NA
0.756
<5.0
NA
Nov-20
<0.0100
0.743
<5.0
0.0255
Nov-20
I <0.0100
1 0.686
1 NA
0.0244
Page 10 of 25 5/28/2021

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-10
Jun-04
<1
0.723
<28
4.63
Nov-04
<0.4
0.592
354
3.33
May-05
0.02
0.419
647
0.193
Nov-05
0.31
0.62
57.5
3.62
May-06
0.29
0.328
<7
3.01
Nov-06
0.28
0.509
284
3.12
May-07
0.28
0.564
<28
3.26
Nov-07
0.31
0.413
<7
3.46
May-08
0.405
0.461
<7
3.22
Nov-08
0.352
0.481
<7
3.12
May-09
0.319
0.412
<7
3.09
Dec-09
0.391
0.649
<14
4.58
May-10
0.288
0.417
<14
2.91
Nov-10
0.25
0.39
<14
2.55
May-11
0.328
0.553
NA
3.34
Nov-11
0.3
0.306
<14
2.53
May-12
0.157
0.484
NA
1.45
Nov-12
0.165
0.546
<14
1.82
May-13
0.106
0.421
252
1.12
Nov-13
0.157
0.47
<35
1.69
May-14
0.0728
0.599
<10
0.73
Nov-14
0.169
0.508
<10
1.84
May-15
0.0828
0.511
<5.0
1.09
Nov-15
0.192
0.404
<50
2.11
May-16
0.0888
0.42
<50
1.16
Nov-16
0.104
0.33
403
1.08
May-17
0.137 J
0.275
<5
1.4 J
May-17
0.070 J
0.257
<5
0.735 J
Nov-17
0.231 J
0.327
<5.0
1.44
May-18
0.146
0.243
<10.0
1.46
May-18
0.178 J
0.261
<10.0
1.57
Nov-18
0.0321
0.267
41.3
0.31
May-19
0
0.328
<5.0
1
May-19
0
0.312
<5.0
1
Nov-19
0
0.222
<50.0
1
May-20
0.0711 J
0.219
<5.0
0.643 J
May-20
0.113 J
0.179
<5.0
1.01 J
Nov-20
1 0.0694
1 0.197
1 <5.0
1 0.698
Page 11 of 25 5/28/2021

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-12
Feb-04
<0.01
0.315
<7
<0.01
May-04
<0.01
0.521
<7
<0.01
Jun-04
<0.01
0.775
<7
0.0102
Nov-04
<0.01
0.942
<7
0.0115
May-05
<0.01
0.222
<7
0.0108
Nov-05
<0.01
0.165
<7
<0.01
May-06
<0.01
0.151
NA
<0.01
Nov-06
<0.01
0.216
NA
<0.01
May-07
<0.01
0.118
NA
<0.01
Nov-07
<0.01
0.169
NA
<0.01
May-08
<0.01
0.121
<7
<0.01
Nov-08
<0.01
0.102
NA
<0.01
May-09
<0.01
0.105
NA
0.0108
Dec-09
<0.01
0.128
NA
0.0119
May-10
<0.01
0.11
NA
<0.01
Nov-10
<0.01
0.0946
NA
<0.01
May-11
<0.01
0.11
NA
<0.01
Nov-11
<0.01
0.0761
NA
<0.01
May-12
<0.01
0.13
NA
<0.01
May-12
<0.01
0.132
NA
<0.01
Nov-12
<0.01
3.68
NA
<0.01
May-13
<0.01
3.44
NA
<0.01
Nov-13
<0.01
3.24
NA
<0.01
May-14
<0.01
2.59
NA
<0.01
Nov-14
<0.01
3.27
NA
<0.01
May-15
<0.01
3.09
NA
<0.01
Nov-15
<0.01
2.9
NA
<0.01
May-16
<0.01
2.81
NA
<0.01
Nov-16
<0.01
2.91
NA
<0.01
May-17
<0.01
2.71
NA
<0.01
Nov-17
<0.0100
2.76
NA
<0.0100
May-18
<0.0100 UJ
2.89
NA
<0.0100 UJ
Nov-18
<0.0100
3.09
NA
<0.0100
May-19
<0.0100
2.5
NA
<0.0100
Nov-19
<0.0100
2.3
NA
<0.0100
May-20
<0.0100
2.13
NA
<0.0100
Nov-20
<0.0100
2.4
NA
<0.0100
Page 12 of 25 5/28/2021

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-17B
Feb-04
<0.01
2.98
<7
<0.01
May-04
<0.01
2.33
<7
0.0125
Jun-04
<0.01
4.96
<7
<0.01
Nov-04
<0.01
3.11
<7
<0.01
May-05
<0.01
2.83
<7
0.0102
Nov-05
<0.01
1.87
<7
0.0107
May-06
<0.01
2.42
NA
<0.01
Nov-06
<0.01
2.84
NA
<0.01
May-07
<0.01
2.62
NA
<0.01
Nov-07
<0.01
3.33
NA
<0.01
May-08
<0.01
3.52
<7
<0.01
Nov-08
<0.01
2.35
NA
<0.01
Dec-09
<0.01
2.54
NA
<0.01
Nov-10
<0.01
2.75
NA
<0.01
Nov-11
<0.01
2.59
NA
<0.01
Nov-12
<0.01
0.291
NA
<0.01
Nov-13
<0.01
0.113
NA
<0.01
Nov-14
<0.01
0.271
NA
<0.01
Nov-15
<0.01
0.135
NA
<0.01
Nov-16
<0.01
1.93
NA
<0.01
Nov-17
<0.0100
0.128
NA
<0.0100
Nov-18
I <0.0100
0.0722
NA
<0.0100
Nov-19
<0.0100
0.259
NA
<0.0100
Nov-20
<0.0100
0.0786
NA
<0.0100
Page 13 of 25 5/28/2021

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-17C
Feb-04
<0.01
3.29
<7
<0.01
May-04
<0.01
2.21
<7
<0.01
Jun-04
<0.01
3.01
<7
<0.01
Nov-04
<0.01
3.22
<7
0.0117
May-05
<0.01
2.51
<8.5
<0.01
Nov-05
<0.01
2.44
<7
<0.01
May-06
<0.01
2.68
NA
<0.01
Nov-06
<0.01
2.92
NA
<0.01
May-07
<0.01
2.93
NA
<0.01
Nov-07
<0.01
3.06
NA
<0.01
May-08
<0.01
2.90
<7
<0.01
Nov-08
<0.01
2.10
NA
<0.01
Dec-09
<0.01
2.40
NA
<0.01
May-10
NA
1.95
NA
NA
Nov-10
<0.01
2.39
NA
<0.01
May-11
NA
2.02
NA
NA
Nov-11
<0.01
2.15
NA
<0.01
May-12
NA
2.47
NA
NA
Nov-12
<0.01
3.18
NA
<0.01
May-13
NA
3.61
NA
NA
Nov-13
<0.01
3.1
NA
<0.01
May-14
NA
3.71
NA
NA
Nov-14
<0.01
2.42
NA
<0.01
May-15
NA
2.9
NA
NA
Nov-15
<0.01
1.81
NA
<0.01
May-16
<0.01
0.177
NA
<0.01
Nov-16
<0.01
0.177
NA
<0.01
May-17
NA
2.51
NA
NA
Nov-17
<0.0100
1.68
NA
<0.0100
May-18
NA
2.09
NA
NA
Nov-18
<0.0100
1.97
NA
<0.0100
May-19
NA
1.97
NA
NA
Nov-19
<0.0100
1.51
NA
<0.0100
May-20
I NA
1 1.32
1 NA
I NA
Nov-20
I <0.0100
1 1.64
1 NA
I <0.0100
Page 14 of 25 5/28/2021

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC — Needmore Road Landfill
AECOM Project No. 60633967
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-21 B
Jun-04
<0.01
0.0391
<7
<0.01
Nov-04
<0.01
0.047
<7
<0.01
May-05
<0.01
0.0338
<7
<0.01
Nov-05
<0.01
0.0477
<7
<0.01
May-06
NA
0.0348
NA
NA
Nov-06
NA
0.0507
NA
NA
May-07
NA
0.0511
NA
NA
Nov-07
NA
0.0686
NA
NA
May-08
NA
0.0557
<7
NA
Nov-08
NA
0.0598
NA
NA
Dec-09
NA
0.0698
NA
NA
Nov-10
NA
0.0534
NA
NA
Nov-11
NA
0.0573
NA
NA
Nov-12
NA
0.0811
NA
NA
Nov-13
NA
0.0665
NA
NA
Nov-14
NA
0.0832
NA
NA
Nov-15
NA
0.092
NA
NA
Nov-16
NA
0.0685
NA
NA
Nov-17
NA
0.071
NA
NA
Nov-18
NA
0.0703
NA
NA
Nov-19
NA
0
NA
NA
Nov-20
NA
0.0357
NA
I NA
Page 15 of 25 5/28/2021

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-22A
Feb-04
<0.01
0.67
<7
0.0634
May-04
<0.01
0.322
<7
0.0514
Jun-04
<0.01
1.06
<7
0.0449
Nov-04
<0.01
0.895
<7
0.0427
May-05
<0.01
0.722
<7.9
0.0284
Nov-05
<0.01
0.572
<7
0.0268
May-06
<0.01
0.949
NA
0.025
Nov-06
<0.01
1.12
NA
0.0259
May-07
<0.01
1.13
NA
0.0186
Nov-07
<0.01
1.3
NA
0.0213
May-08
<0.01
1.18
<7
0.0242
Nov-08
<0.01
1.04
NA
0.0214
Dec-09
<0.01
1.25
NA
0.0141
Nov-10
<0.01
1.74
NA
<0.01
Nov-11
<0.01
1.22
NA
<0.01
Nov-12
<0.01
2.05
NA
<0.01
Nov-13
<0.01
1.71
NA
<0.01
Nov-14
<0.01
1.64
NA
<0.01
Nov-15
<0.01
1.69
NA
<0.01
Nov-16
<0.01
1.48
NA
<0.01
Nov-17
<0.0100
1.35
NA
<0.0100
Nov-18
<0.0100
0.767
NA
I <0.0100
Nov-19
<0.0100
1.44
NA
<0.0100
Nov-20
<0.0100
1.27
NA
<0.0100
Page 16 of 25 5/28/2021

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-22B
Feb-04
<0.01
2.64
<7
0.0323
May-04
<0.01
1.9
<7
0.0346
Jun-04
<0.01
2.78
<7
0.033
Nov-04
<0.01
2.72
<7
0.0362
May-05
<0.01
2.32
<10.8
0.0351
Nov-05
<0.01
1.22
<7
0.0365
May-06
<0.01
2.46
NA
0.0329
Nov-06
<0.01
2.33
NA
0.028
May-07
<0.01
2.79
NA
0.0284
Nov-07
<0.01
2.62
NA
0.0295
May-08
<0.01
2.42
<7
0.023
Nov-08
<0.01
1.87
NA
0.0236
May-09
NA
2.39
NA
NA
Dec-09
<0.01
2.14
NA
0.0265
May-10
NA
2.01
NA
NA
Nov-10
<0.01
2.14
NA
0.0316
May-11
NA
1.75
NA
NA
Nov-11
<0.01
1.5
NA
0.0251
May-12
NA
1.95
NA
NA
Nov-12
<0.01
2.08
NA
0.0243
Nov-12
<0.01
2.2
NA
0.0227
May-13
NA
1.88
NA
NA
Nov-13
<0.01
1.69
NA
0.0222
May-14
NA
2.05
NA
NA
Nov-14
<0.01
2.8
NA
0.0202
May-15
NA
1.73
NA
NA
Nov-15
<0.01
1.72
NA
0.0117
May-16
<0.01
1.39
NA
0.0119
Nov-16
NA
1.62
NA
NA
May-17
NA
1.87
NA
NA
Nov-17
<0.0100
1.62
NA
0.0367
May-18
NA
1.63
NA
NA
Nov-18
<0.0100
1.51
NA
0.0163
May-19
NA
1.71
NA
NA
Nov-19
<0.0100
1.41
NA
0
Nov-20
NA
1.33
NA
NA
May-20
<0.0100
1.35
NA
0.0312
Page 17 of 25 5/28/2021

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-23A
Feb-04
<0.01
1.5
<7
0.115
May-04
<0.01
1.21
<7
0.0928
Jun-04
<0.01
2.03
<7
0.0911
Nov-04
<0.01
1.45
227
0.0769
May-05
<0.01
1.41
278
0.0108
Nov-05
<0.01
1.29
<70
0.0919
May-06
<0.01
0.711
286
0.0823
Nov-06
<0.01
2.01
255
0.0791
May-07
<0.01
1.51
<70
0.0768
Nov-07
<0.01
1.45
<7
0.112
May-08
<0.01
1.91
NA
0.0936
Nov-08
<0.01
1.97
<7
0.0711
May-09
NA
1.34
<7
NA
Dec-09
<0.01
1.84
<7
0.131
May-10
NA
1.96
<7
NA
Nov-10
<0.01
1.81
<7
0.1
May-11
NA
1.3
NA
NA
Nov-11
<0.01
2.41
<7
0.0884
May-12
NA
2.45
NA
NA
Nov-12
<0.01
3.35
<7
0.0772
May-13
NA
2.82
120
NA
Nov-13
<0.01
2.76
146
0.0755
May-14
NA
3.06
<100
NA
Nov-14
<0.01
3.54
329
0.0708
May-15
NA
3.24
<5.0
NA
Nov-15
<0.1
3.35
<50
<0.1
May-16
NA
3.11
<50
NA
Nov-16
<0.01
2.52
189
0.0349
May-17
NA
3.04
393
NA
Nov-17
<0.0100 UJ
2.99
244
0.0696 J
May-18
NA
2.76
<50.0
NA
Nov-18
<0.0100
3.54
192
0.0257
May-19
NA
2.65
<5.0
NA
Nov-19
<0.0100
1 3.09
1 <50.0
1 0
May-20
NA
2.92
<50.0
NA
Nov-20
<0.0100
3.47
<50.0
0.0431
Page 18 of 25 5/28/2021

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-23B
Feb-04
<0.01
1.67
594
0.124
May-04
<0.01
1.14
<7
0.115
Jun-04
<0.01
1.76
<35
0.101
Nov-04
<0.01
1.82
393
0.0857
May-05
<0.2
1.29
<35
<0.2
Nov-05
<0.01
1.33
<35
0.129
May-06
<0.01
0.891
51.9
0.116
Nov-06
<0.02
1.7
907
0.128
May-07
<0.02
2.29
<70
0.0973
Nov-07
<0.01
1.94
<7
0.128
May-08
<0.01
2.31
<7
0.123
Nov-08
<0.01
2.54
<7
0.112
May-09
NA
1.77
<7
NA
Dec-09
<0.01
2.46
<7
0.183
May-10
NA
2.14
<7
NA
Nov-10
<0.01
2.02
<7
0.0768
May-11
NA
2.15
NA
NA
Nov-11
<0.01
2.49
<7
0.0982
May-12
NA
2.39
NA
NA
Nov-12
<0.01
3.52
<7
0.0811
May-13
NA
2.72
120
NA
Nov-13
<0.01
2.88
82.3
0.0759
May-14
NA
3.01
381
NA
Nov-14
<0.0111
3.4
542
0.103
May-15
NA
2.78
<5.0
NA
Nov-15
<0.01
3.33
<50
<0.01
May-16
NA
2.73
<50
NA
Nov-16
<0.01
2.71
516
0.0275
May-17
NA
2.62
512
NA
Nov-17
<0.0100
2.63
<5.0
0.103
May-18
NA
2.53
<50.0
NA
Nov-18
<0.0100
3.04
74
0.0322
May-19
NA
3.4
<5.0
NA
Nov-19
I <0.0100
1 3.08
1 <50.0
1 0
May-20
NA
2.63
<50.0
NA
Nov-20
<0.0100
3.15
<50.0
0.0696
Page 19 of 25 5/28/2021

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-24A
Feb-04
<0.01
0.0548
7.8
<0.01
May-04
<0.01
0.022
<7
<0.01
Jun-04
<0.01
0.0625
<7
<0.01
Nov-04
<0.01
0.0796
<7
<0.01
May-05
<0.01
0.0885
<7
<0.01
Nov-05
<0.01
0.0726
<7
0.0111
May-06
<0.01
0.105
NA
0.0102
Nov-06
<0.01
0.158
NA
0.0126
May-07
<0.01
0.141
NA
<0.01
Nov-07
<0.01
0.161
NA
0.0124
May-08
<0.01
0.159
<7
<0.01
Nov-08
<0.01
0.125
NA
0.0124
May-09
NA
0.113
NA
NA
Dec-09
<0.01
0.15
NA
0.0169
May-10
NA
0.135
NA
NA
Nov-10
<0.01
0.133
NA
0.01
May-11
NA
0.102
NA
NA
Nov-11
<0.01
0.132
NA
0.0118
Nov-12
<0.01
0.218
NA
0.011
May-13
NA
0.126
NA
NA
Nov-13
<0.01
0.158
NA
<0.01
May-14
NA
0.189
NA
NA
Nov-14
<0.01
0.23
NA
0.0124
May-15
NA
0.103
NA
NA
Nov-15
NA
NA
NA
NA
May-16
<0.01
0.188
NA
<0.01
Nov-16
<0.01
0.155
NA
<0.01
Ma -17
NA
0.0437
NA
NA
Nov-17
<0.0100
0.198
NA
0.013
Ma -18
NA
0.158
NA
NA
Nov-18
<0.0100
0.0313
NA
<0.0100
Ma -19
NA
0.231
NA
NA
Nov-19
<0.0100
0.214
NA
<0.0100
May-20
NA
0.162
NA
NA
Nov-20
<0.0100
0.182
NA
<0.0100
Page 20 of 25 5/28/2021

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-24B
Feb-04
<0.01
0.0586
<7
0.0184
Ma -04
<0.01
0.0439
<7
0.0178
Jun-04
<0.01
0.0892
<7
0.0146
Nov-04
<0.01
0.082
<7
0.0181
May-05
<0.01
0.0722
<7
0.0194
Nov-05
<0.01
0.0591
<7
0.0165
May-06
<0.01
0.0746
NA
0.0178
Nov-06
<0.01
0.101
NA
0.018
May-07
<0.01
0.0962
NA
0.015
Nov-07
<0.01
0.102
NA
0.0158
May-08
<0.01
0.113
<7
0.0151
Nov-08
<0.01
0.0877
NA
0.0178
Dec-09
<0.01
0.0931
NA
0.0226
Nov-10
<0.01
0.0896
NA
0.0151
Nov-11
<0.01
0.0874
NA
0.0144
Ma -12
NA
0.103
NA
NA
Nov-12
<0.01
0.118
NA
0.0136
Nov-13
<0.01
0.0918
NA
<0.01
Nov-14
<0.01
0.103
NA
0.0101
Nov-15
NA
NA
NA
NA
May-16
<0.01
0.0998
NA
<0.01
Nov-16
<0.01
0.122
NA
0.0102
Nov-17
<0.0100
0.104
NA
0.0178
Nov-18
<0.0100
0.0485
NA
<0.0100
Nov-19
<0.0100
0
NA
0
Nov-20
<0.0100
0.103
NA
0.0104
Page 21 of 25 5/28/2021

Table 7
Summary of Detected Constituents in Groundwater
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
Parameter
1,1-Biphenyl
1,4-Dioxane
Ethylene
Glycol
Diphenyl
Ether
Units
mg/L
mg/L
mg/L
mg/L
NC 2L Standard
0.4
0.003
14
PQL
B-32 B
Jun-04
<0.01
0.176
<28
0.0577
Nov-04
<0.01
0.198
162
0.0575
May-05
<0.2
0.115
<14
<0.2
Nov-05
<0.01
0.072
<14
0.0416
May-06
<0.01
0.0818
27.6
0.0617
Nov-06
<0.01
0.0996
344
0.0558
May-07
<0.01
0.149
<35
0.0414
Nov-07
<0.01
0.117
<7
0.0816
May-08
<0.01
0.0796
<7
0.0329
Nov-08
<0.01
0.173
<7
0.0816
Dec-09
<0.01
0.104
<7
0.0621
Nov-10
<0.01
0.144
<7
0.0566
Nov-11
<0.01
0.0988
<7
0.0399
Nov-12
<0.01
0.0755
<7
<0.01
Nov-13
<0.01
0.0275
<7
0.0106
Nov-14
<0.01
0.0178
<10
<0.01
Nov-15
<0.01
0.0183
<50
<0.01
Nov-16
<0.01
0.0123
<5
<0.01
Nov-17
<0.0100
0.0152
246
<0.0100
Nov-18
<0.0100
0.0033
<50.0
<0.0100
Nov-19
<0.0100
0.0041
<5.0
<0.0100
Nov-20
<0.0100
0.0034
<5.0
<0.0100
Notes:
mg/L - milligrams per liter
NA - Not Analyzed
PQL - Practical Quantitation Limit
Page 22 of 25 5/28/2021

Ethylene Glycol(B-01)
ab
m
c
C
c
U°
06. 5P _O(o 01 _00 _00 ^O _^^ ^p
10 40 40 40
Date
B-01 f NC 2L Standard
Table 8
Time vs. Concentration Plots - Ethylene Glycol
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
Ethylene Glycol (B-09C)
2500
E 2000
0 1500
1000
w
c 500
0
U 0
,0 ^0 ^1 0 ^0 'L°
sf Sacs saw
Date
�B-09C tNC2LStandard
Ethylene Glycol (B-23A)
_ 450
7
rn 400
� 350
300
C 250
200
y 150
� 100
tj 50
0
�c �c �c lac lac ��c ��c lac lac ��c
Date
tB-23A tNC 21. Standard
Ethylene Glycol (B-10)
J 1000
E aoo
O 600
C 400
d
c 200
V
0
Date
tB-10 tNC2LStandard
Ethylene Glycol (13-236)
l000
J
� 800
O 600
400
d
c 200
O
U
0
I.
Sao' dad sae sae 0ao 0ao Sao Sao Sao 0ao 0a� �a� �a� �a� �a� Sao'
Date
—0--B-23B tNC 2L Standard
Page 23 of 25 5/28/2021

1,4-Dioxane (B-01)
5
4
3
2
1
0
Date
-*-B-01 fNC2LStandard
1,4-Dioxane (B-12)
J 5
E 4
3
.O
2
O
c 1
U O
o
U
Date
B-12 t NC 2L Standard
1,4-Dioxane (B-23A)
5
4
3
2
1
0
.yo
�Jc I'll IJc "I IJc I., I., �Jc IJc
Date
B-23A t NC 2L Standard
Table 9
Time vs. Concentration Plots — 1,4-Dioxane
CNA Holdings LLC — Needmore Road Landfill
AECOM Project No. 60633967
1,4-Dioxane (B-09C)
5
4
3
2
A------ J
0
a 5
£ 4
� 3
.O
- 2
m
c 1
cO 0�p,
5
a
3
2
1
0
Date
-4-B-09C fNC2LStandar7d
1,4-Dioxane (B-17C)
Date
B-17C f NC 2L Standard
1,4-Dioxane (B-23B)
Date
t B-23B t NC 2L Standard
5
4
3
2
1
0
1,4-Dioxane (B-10)
Date
-B-10 fNC2LStandard
1,4-Dioxane (B-22B)
s
J
6 4
E 3
C
O 2
c 1
cdi 0
O
U �Jc �Jc �Jc �Jc �Jc �Jc �Jc �Jc �Jc �Jc �Jc �Jc �Jc �Jc �Jc �Jc �Jc
Date
-0-B-22B fNC2LStandard
1,4-Dioxane (B-24A)
0.25
0.2
0.15
0.1
0.05
0
^I ^°
�Jp �Jp �Jp �Jp �Jc �Jc �Jc �Jc ,3Jc
Date
-B-24A fNC2LStandard
Page 24 of 25 5/28/2021

Diphenyl Ether(B-01)
0.5
J
E 0.4
0.3
O
- 0.2
0.1
m
U p
O °b Oh 00 °A 00 °O NO ^�. ^0, ^'S ^b ^5 ^° ^'1 ^0 0 ry0
) ) ) ) ) ) ) ) ) ) ) ) ) ) ) ) )
Date
t B-01 t NC 2L Standard
J 0.5
E 0.4
c 0.3
O
«. 0.2
M
Table 10
Time vs. Concentration Plots - Diphenyl Ether
CNA Holdings LLC - Needmore Road Landfill
AECOM Project No. 60633967
J 0.12
I 0.1
-- 0.03
O 0.06
` 0.04
m 0.02
U 0
Diphenyl Ether (B-23A)
Diphenyl Ether (B-12)
Date
t B-12 t NC 2L Standard
C 0.1
41
O 0
c
�s �s �s �s �s �s �- �., �., '0 '0 '0 'fit' '0 1§1
Date
+B-23A tNC 2L Standard
J 0.5
m 0.4
E
c 0.3
O
0.2
Diphenyl Ether (B-10)
5
J
4
c 3
O
2
c
d
O 0
c 10c 10c sic ��c ��c ��c ��c ��c ��c ��c ��c ��c ��c ssc �Is� �,
Diphenyl Ether (B-23B)
Date
+B-10 tNC 2L Standard
c 0.1
d
O 0
c
U °a oy °o ^o- N5 No NAN.,�0 ,yo
777777
Date
+B-23B t NC 2L Standard
Page 25 of 25 5/28/2021

Figures

t
1
I
J
r—�
�
1
is r
Needmore Rd
0 1,000 2,000
= Feet
4,000
N
W E.
S DAVIE
'ROWAN
I J -
1 r Cooleemee
Need,,,, Rd
Junction
Way
Fob 1
f �
/ 1 �
1
1
/ I
/ 1
J
/ x
/ F
2
i Needmore Rd
I
Or 1 ' 796 d
E d
t 1 )ade Chickadee �° c
`' 1 =
"'MP Cv
1 NP
1 hid eOno�
d S mp CraQpntr Wrhams Rd IQ
I �arxe' Rd m
I
I
a�eG
I CNhJ'r'nsn ��5
Sources: Esri, HERE, Garmin, Intermap, increment P Corp., GEBCO, USGS,
FAO, NPS, NRCAN, GeoBase, IGN, Kadaster NL, Ordnance Survey, Esri Japan,
METI, Esri China (Hong Kong), swisstopo, © OpenStreetMap contributors, and
the GIS User Community
�0� 13Peachtree NE
At
� Atlanta, GA 3030309
T. [phone]
FIGURE 1
SITE LOCATION MAP
NEEDMORE ROAD LANDFILL - CNA HOLDINGS
SALISBURY, NORTH CAROLINA
MAY 2021 60313404

r'
o�
a
S NDAR
SITE
2.6 ACR
\ TAYLOR'S
PIT
i \ (0.6 ACRE)
� J
PHYTOREM IATION
16-ACRE SITE
8
14-ACRE SITE j
L=com
N
01 400' 800'
SCALE
FIGURE 2
SITE LAYOUT MAP
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
6031340
C:\Users\splawnm\Desktop\Projects\Salisbury\60313404_012 Site Layout Map_May202l.dwg, 3/23/2021 10:12:10 AM, Splawnm

1 Q `^
a
b
B-09C ° e9
J
°
B-1
OR
J
CSW-2*
CSW-1
B-22B
° B-23B
° s
2 A
m
B-24A
0
B-01
a
L=COM
LEGEND
0 MONITORING WELL LOCATION
SURFACE WATER SAMPLING LOCATIONS
INTERMITTENT SEEP SAMPLING LOCATION
*: CSW-2 WAS DRY AND THEREFORE NOT SAMPLED.
7 ld�w
I
N
,70
I
ti I
01 400' 800'
1
SCALE
FIGURE 3
SAMPLE LOCATION MAP
MAY 2020
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
MAY 2021 60313404
C:\Users\splawnm\Desktop\Projects\Salisbury\60313404_013 Sample Location Map_May202O.dwg, 3/23/2021 10:14:31 AM, Splawr

I Q
B-09C
J
1ti
J
SW-3 SLIGHTLY UPSTREAM
OF CONFLUENCE WITH
BEAVERDAM BRANCH
Q
A
O
V
® J
LEGEND
O MONITORING WELL LOCATION
SURFACE WATER SAMPLING
LOCATIONS
INTERMITTENT SEEP SAMPLING LOCATIONS
-17 S'W-5
o B-22B \�
1 -22A
B-23B \ ± 1000 FT DOWN STREAM
M
OF COOLEEMEE WEIR
2 A
B-24B
m
B-24A
SW-7
0
B-01 ® `�
I
I`J
01
,70
I
ti I
01 400' 800'
1
SCALE
FIGURE 4
SAMPLE LOCATION MAP
NOVEMBER 2020
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
MAY 2021 60313404
C:\Users\splawnm\Desktop\Projects\Salisbury\60313404_014 Sample Location Map_Nov202O.dwg, 3/23/2021 10:15:57 AM, SpIE

70
71
6�
��6) mob' �\
13-09C
(677.90) • / B-21 I
6 7 (666.2jBl
•
(662.91)
69 \ \ \
\
� B-01
(699.34)0
\\V
706
'' ----�� B-10
(706.06)
711----`/,
• B-32B
(714.16)
B-17C
(661.16)
B-22B
(659.63)
'B-22A
659.13)
B-23B
(659.07)
B-23A
(659.24)
B-24B
-2)
24A
EB
VX�
LEGEND
• MONITORING WELL LOCATION
GROUNDWATER CONTOUR
(DASHED WHERE INFERRED)
• � 18 �b \ 69
0 200 400 800
SCALE IN FEET
L=com
FIGURE 5
GROUNDWATER ELEVATION DATA
NOVEMBER 2020
NEEDMORE ROAD LANDFILL - CNA HOLDINGS
SALISBURY, NORTH CAROLINA
MAY 2021
60313404
C:\Users\splawnm\Desktop\Projects\Salisbury\60313404_015 GW Potentiometric Map_Nov202O.dwg, 3/30/2021 3:07:08 PM, Splawnm

1 Q `^
a
1 b
Q o B-09C
• oe
J
0
1ti
J
a�vv El -
B-23B
0
<50.0 \
-23A
<50.0
m
0
B-01
<5.0
B-10
<5.0 /
P"=COM
LEGEND
® MONITORING WELL LOCATION
SURFACE WATER SAMPLING LOCATION
<5.0 ETHYLENE GLYCOL CONCENTRATION (mg/L)
NOTE: Locations not sampled or analyzed for ethylene
glycol are not shown.
I
N
o7
I
ti I
01 400' 800'
1
SCALE
FIGURE 6
ETHYLENE GLYCOL MAP
MAY 2020
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
MAY 2021 60313404
C:\Users\splawnm\Desktop\Projects\Salisbury\60313404_016 Ethylene Glycol Map_May2020 Data.dwg, 3/23/2021 10:58:59 AM, Splawr

i
SW-3 <5.0
SLIGHTLY UPSTREAM
OF CONFLUENCE WITH
BEAVERDAM BRANCH
� sao
LEGEND
® MONITORING WELL LOCATION
0 SURFACE WATER SAMPLING LOCATION
0 B-09C <5.0 ETHYLENE GLYCOL CONCENTRATION (mg/L)
a9 NOTE: Locations not sampled or analyzed for ethylene
/ I glycol are not shown.
°� ®SW 5
1ti
o
B-23B
70 <50.0
ss
'4 -23A
<50.0
a� 72 /
m
s� SW-7
—____,,,5.0
\ B-01
<5.0
o � I75
�\ q\ AB
<j1 0 1
L=COM
SW-8 <5.0
± 1000 FT DOWN STREAM
OF COOLEEMEE WEIR
N
J 01 400' 800'
I( SCALE
FIGURE 7
ETHYLENE GLYCOL MAP
NOVEMBER 2020
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
60313404
C:\Users\splawnm\Desktop\Projects\Salisbury\60313404_017 Ethylene Glycol Map_Nov2020 Data.dwg, 3/30/2021 3:12:41 PM, Splay

I Q B-09C
bF0 0.7
• oe
LEGEND
® MONITORING WELL LOCATION
SURFACE WATER SAMPLING LOCATION
INTERMITTENT SEEP SAMPLING LOCATION
1.51 1,4-DIOXANE CONCENTRATION (mg/L)
® NOTES:
1. Locations not sampled or analyzed for 1,4-dioxane are not shown.
2. J - Estimated Value
"SW-1
)0.58
W-5
®< .0020
B-226
1.33
B-63 B
o \
B-23A
.92
m
B-24A
.162
0
B-01
® 1.51
B-10
0.219
P"=COM
7 ld�w
I
N
a
I
ti I
01 400' 800'
1
SCALE
FIGURE 8
1,4-DIOXANE MAP
MAY 2020
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
MAY 2021
60313404
C:\Users\splawnm\Desktop\Projects\Salisbury\60313404_0181-4 Dioxane Map_May202O Data.dwg, 3/30/2021 3:18:34 PM, Splawi

SW-3 <0.0020
SLIGHTLY UPSTREAM
OF CONFLUENCE WITH
BEAVERDAM BRANCH
LEGEND
J O MONITORING WELL LOCATION
® SURFACE WATER SAMPLING LOCATION
INTERMITTENT SEEP SAMPLING LOCATIONS
1.51 1,4-DIOXANE CONCENTRATION (mg/L)
CSW-2
0.279
e9 CSW-1
B-21 B 0.368 NOTE: Locations not sampled or analyzed for 1,4-dioxane
�0.035M7�9ZA S 5
I
64 are not shown.
B-22B < .0020
1.35
2A
1.
1.27
o B-23B
3.15 \
s
23A
.47
B.14 B
s� B 182 SW-7
<0 20
SW-8 <0.0020
000 FT DOWN STREAM
F COOLEEMEE WEIR
gg o
®1.51
B-10
0.197 1°
1 6
® 70 -
❑ 6A I
71
� I
V
% 6 01 400' 800'
�z a
SCALE
FIGURE 9
1,4-DIOXANE MAP
P"=COM NOVEMBER 2020
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
MAY 2021 60313404
C:\Users\splawnm\Desktop\Projects\Salisbury\60313404_019 id Dionne Map_Nov202O Data.dwg, 3/23/2021 11:14:13 AM, Splawn

1 Q `^
a
b
Q o
<0.01 6A
J
0
1ti B-1
a
SW-3 <0.01
SLIGHTLY UPSTREAM
OF CONFLUENCE WITH
BEAVERDAM BRANCH
LEGEND
® MONITORING WELL LOCATION
0 SURFACE WATER SAMPLING LOCATION
J<0.01 1,1-BIPHENYL CONCENTRATION (mg/L)
NOTE:
Locations not sampled or analyzed for 1,1-biphenyl are not shown.
I S -5
t 1 < .01
B 11
0.01 <
<0.01
\ m o
o s <0.011 \
s
- 3A
001
B-24B
<0.01
B-24A
0.01 SW-7
® B0�01
0.0694
L=COM
SW-8 <0.01
1000 FT DOWN STREAM
DF COOLEEMEE WEIR
,d d I
01
,70
I
ti I
01 400' 800'
1
SCALE
FIGURE 10
1,1-BIPHENYL MAP
NOVEMBER 2020
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
MAY 2021 60313404
C:\Usem\splawnm\Desktop\Projects\Salisbury\60313404_020 1-1 Biphenyl Map_Nov202O Data.dwg, 3/23/2021 11:18:21 AM, Splawnn

0
We
X
ISW-3 <0.01
SLIGHTLY UPSTREAM
OF CONFLUENCE WITH
BEAVERDAM BRANCH
LEGEND
® MONITORING WELL LOCATION
® J SURFACE WATER SAMPLING LOCATION
1 O 6�' 0.03 DIPHENYL ETHER CONCENTRATION (mg/L)
NOTES:
e 1. Locations not sampled or analyzed for diphenyl ether
are not shown.
. 0.71 °� 001 2. J - Estimated Value
0
6.03 2
B-.01
<001
o B-23B
0.0696 \
- 3A
431
B-24 B
0.0104
B-24A
0.01 SV�/-7
SW-8 <0.01
1000 FT DOWN STREAM
OF COOLEEMEE WEIR
ggp0o
gg 75 I N
0.698 1° 1
1 6
® 70
❑ 6A I
71
� I
V
6 12 01 400' 800'
a %
SCALE
FIGURE 11
DIPHENYL ETHER MAP
NOVEMBER 2020
NEEDMORE ROAD LANDFILL - CNA HOLDINGS LLC
SALISBURY, NORTH CAROLINA
MAY 2021 60313404
C:\Users\splawnm\Desktop\Projects\Salisbury\60313404_021 Diphenyl Ether Map_Nov202O Data.dwg, 3/23/2021 11:23:23 AM, Splawn

Appendix A
May 2020 and November 2020
Laboratory Analytical Reports

AECOM
Memorandum
AECOM
One Midtown Plaza
1360 Peachtree St. N.E.
Suite 500
Atlanta, GA 30309
To Jing Zhou — AECOM Atlanta
CC
Subject Level 2 Data Validation for Needmore Road Landfill
From Robert Davis — AECOM Atlanta
Date March 16, 2021
404.965.9600
404.965.9605
Page
tel
fax
1 of 6
Limited validation of the analytical data for the water samples was performed on one data package
received from Pace Analytical Services, Inc. in Greenwood, South Carolina. The samples were
collected on November 2-3, 2020, at the Needmore Road Landfill in North Carolina.
The data were reviewed for conformance to method specifications and the project guidance
document: Supplemental Characterization and Long -Term Monitoring (AECOM, July 2010 Revision
2). Data qualifiers were applied in accordance with the validation criteria set forth in USEPA
Contract Laboratory Program (CLP) National Functional Guidelines for Organic Superfund Methods
Data Review, EPA-540-R-2017-002, January 2017 and USEPA Contract Laboratory Program
National Functional Guidelines for Inorganic Superfund Methods Data Review, EPA-540-R-2017-
001, January 2017, as they apply to the analytical methods employed.
Field duplicate relative percent difference (RPD) review and applicable control limits were taken
from the USEPA Region I, New England Data Validation Functional Guidelines for Evaluating
Environmental Analyses, December 1996.
The following methods were requested on the chain -of -custody (COC) records:
• Method 8260D —
Volatiles by Gas Chromatography/Mass Spectrometry (GC/MS);
• Method 8260D SIM — Volatiles by GC/MS in SIM mode;
• Method 8270E —
Semivolatiles by GC/MS;
• Method 8015M
— Ethylene Glycol by GC;
• Method 2320B —
Alkalinity;
• Method 353.2 —
Nitrate and Nitrite;
• SM450OP-E — Orthophosphate;
• Method 9056A —
Sulfate by Ion Chromatography (IC);
• Method AM23G
— Volatile Fatty Acids;
• Method AM20GAX — Hydrogen;

AECOM
2
• Method AM20GAX — Dissolved Gases (MEE); and
• Method RSK-175 —Carbon Dioxide.
REVIEW ELEMENTS
Sample data were reviewed for the following quality control (QC) parameters:
• Agreement of analyses conducted with COC requests;
• Holding times and sample preservation;
• GC/MS hardware tunes, initial and continuing calibrations;
• Method blanks/trip blanks;
• Surrogate recoveries;
• Laboratory control sample (LCS) recoveries;
• Matrix spike/matrix spike duplicate (MS/MSD) recoveries; and
• Field duplicate precision results.
Samples
Environmental Field Management (EFM) personnel collected the following water samples from the
Needmore Road Landfill in North Carolina, as reported under the Pace Analytical Services, Inc. job
number:
nncngcro
Lab ID
Sample ID
Lab ID
Sample ID
92503658001
B-23A-110220
92503658012
CSW-1-110220
92503658002
B-2313-110220
92503658013
CSW-2-110220
92503658003
B-2413-110220
92503658014
B-22A-110320
92503658004
B-24A-110220
92503658015
B-2213-110320
92503658005
B-21B-110220
92503658016
B-17C-110320
92503658006
B-09C-110220
92503658017
B-1713-110320
92503658007
B-99C-110220
92503658018
B-12-110320
92503658008
SW-7-110220
92503658019
B-3213-110320
92503658009
SW-5-110220
92503658020
B-01-110320
92503658010
SW-3-110220
92503658021
B-10-110320
92503658011
SW-8-110220
ANALYTICAL RESULTS
In general, the data results are valid as reported and may be used for decision -making purposes.
Sample data were qualified with either "J" (estimated) or "UX (the analyte was not detected;
however, the reporting limit is approximate and may be inaccurate or imprecise). See Table 1.

AECOM
DISCUSSION
Agreement of Analyses Conducted with Chain -of -Custody Requests
Sample reports were checked to verify agreement with the COC request. No discrepancies were
noted.
Holding Times and Sample Preservation
All samples were analyzed within the holding times required by the methods with the following
exception:
• Method SM4500P-E: All samples were outside of the holding time for orthophosphate,
because they were not filtered within 15 minutes of collection. The orthophosphate results
were qualified. See Table 1.
All coolers were received within the optimal range of 4±2 degrees Celsius (°C).
All samples were properly preserved as specified by the methods.
GC/MS Tunes, Initial and Continuing Calibrations
GC/MS tuning and calibration summaries were not submitted for validation in this Level II data
package.
Method Blanks/Trip Blanks
No analytes were detected at concentrations exceeding the reporting limits for the method blanks
with the following exceptions:
• Method AM20GAX: The method blank associated with batch 697069 had detection for
methane. All of the associated samples had methane detections greater than five times the
method blank concentration. Data qualification was not required.
• Trip blanks were not submitted with the sample set. Contamination picked up in storage or
transit could not be evaluated.
Surrogate Recoveries
The surrogate recoveries were acceptable for all analyses.
Laboratory Control Sample Recoveries
LCS recoveries for all analyses were within the QC limits.
Matrix Spike/Matrix Spike Duplicate Recoveries
MS/MSDs that were performed on non -project samples were not evaluated because matrix
similarity to project samples could not be assumed.

AECOM
The MS/MSD recoveries on client samples were all within the advisory limits with the following
exceptions:
• Method 2320B: The alkalinity MS/MSD recoveries were outside of the QC limits in samples
B-2313-110220 and B-10-110320. The spike amounts were less than 25% of the sample
concentrations; therefore, data qualification was not required.
• Method 353.2: The nitrate MS/MSD recoveries were outside of the QC limits biased low in
sample B-23A-110220. The nitrate result in sample B-23A-110220 was qualified. See
Table 1.
• Method 353.2: The nitrate and nitrite MS/MSD recoveries were outside of the QC limits
biased low in sample B-01-110320. The nitrate and nitrite results in sample B-01-110320
were qualified. See Table 1.
• Method SM 4500P-E: The orthophosphate MS/MSD recoveries were outside of the QC
limits biased high in sample B-23A-110220. The orthophosphate result in sample
B-23A-110220 was qualified. See Table 1.
• Method 9056A: The sulfate MSD recovery was outside of the QC limits biased high in
sample B-23A-110220. The sulfate result in sample B-23A-110220 was qualified. See
Table 1.
• Method 9056A: The sulfate MS/MSD recoveries were outside of the QC limits biased high
in sample B-12-110320. The sulfate result in sample B-12-110320 was qualified. See
Table 1.
• Method 906OA: The Total Organic Carbon (TOC) MS/MSD recoveries were outside of the
QC limits in sample B-23A-110220. The spike amounts were less than 25% of the sample
concentrations; therefore, data qualification was not required.
Field Duplicate Precision Results
A field duplicate was collected on sample B-09C-110220. See Table 2 for the calculated RPDs for
all compounds for which there were detections. The RPDs between the original and field duplicate
were all within the advisory limits of 0-30%. Field sampling/laboratory precision and sample
homogeneity were acceptable. No data qualifications were required.

AECOM
Table 1
Qualified Analytical Data
Sample ID
Method
Analyte
Lab
Result
Lab
Qual
Validated
Result
Validation
Qualifier'
Units
Reason
Codes'
B-23A-110220
353.2
Nitrate
ND
0.040
UJ
mg/L
MS
B-23A-110220
SM450OP-E
Orthophosphate
0.34
0.34
J
mg/L
MS HT
B-23A-110220
9056
Sulfate
5.1
5.1
J+
mg/L
MS
B-2313-110220
SM450OP-E
Orthophosphate
ND
0.25
UJ
mg/L
HT
B-2413-110220
SM450OP-E
Orthophosphate
0.064
0.064
J-
mg/L
HT
B-24A-110220
SM450OP-E
Orthophosphate
0.16
0.16
J-
mg/L
HT
B-21 B-110220
SM450OP-E
Orthophosphate
0.10
0.10
J-
mg/L
HT
B-09C-110220
SM450OP-E
Orthophosphate
ND
0.25
UJ
mg/L
HT
B-22A-110320
SM450OP-E
Orthophosphate
ND
0.25
UJ
mg/L
HT
B-2213-110320
SM450OP-E
Orthophosphate
0.14
0.14
J-
mg/L
HT
B-17C-110320
SM450OP-E
Orthophosphate
0.24
0.24
J-
mg/L
HT
B-1713-110320
SM450OP-E
Orthophosphate
0.22
0.22
J-
mg/L
HT
B-12-110320
SM450OP-E
Orthophosphate
0.25
0.25
J-
mg/L
HT
B-12-110320
9056
Sulfate
1.3
1.3
J+
mg/L
MS
13-3213-110320
SM450OP-E
Orthophosphate
ND
0.050
UJ
mg/L
HT
B-01-110320
SM450OP-E
Orthophosphate
ND
0.25
UJ
mg/L
HT
B-01-110320
353.2
Nitrate
ND
0.040
UJ
mg/L
MS
B-01-110320
353.2
Nitrite
0.22
0.22
J-
mg/L
MS
B-10-110320
SM450OP-E
Orthophosphate
0.32
0.32
J-
mg/L
HT
Notes:
mg/L: milligrams per liter
ND: not detected
': USEPA-defined data validation qualifiers applied in this data evaluation:
J: The associated numerical value is the approximate concentration of the compound in the sample.
J-: The associated numerical value is the approximate concentration of the compound in the sample biased low.
J+: The associated numerical value is the approximate concentration of the compound in the sample biased high.
UJ: The analyte was not detected; however, the reported quantitation limit is approximated and may be inaccurate or
imprecise.
': Reason Codes:
HT: The holding time was exceeded.
MS: The matrix spike recovery was outside of the advisory limits.

AECOM
Table 2
Field Precision
Method
Compound
B-09C-110220
I B-99C-110220
Units
% RPD
8270E
Diphenyl ether
25.5
24.4
pg/L
4.4
8260D
Acetone
2660
2680
pg/L
0.75
8260D
2-Butanone
451
453
pg/L
0.44
8260D
MIBK
87.5
88.5
pg/L
1.1
8260D
1,4-Dioxane
743
686
pg/L
8.0
Notes:
% RPD: Relative percent difference between the primary sample result and the sample duplicate result
pg/L: micrograms per liter

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
November 19, 2020
Jing Zhou
AECOM
1000 Abernathy Road
Building 400, Suite 900
Atlanta, GA 30328
RE: Project: NRLF
Pace Project No.: 92503658
Dear Jing Zhou:
Enclosed are the analytical results for sample(s) received by the laboratory between November 03, 2020 and November
04, 2020. The results relate only to the samples included in this report. Results reported herein conform to the applicable
TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the
report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Gulf Coast
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Indianapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
c
Kevin Godwin
[e-mail]
1(704)875-9092
Project Manager
Enclosures
cc: Rob Davis. AECOM
?4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 104

lacieAnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Project: NRLF
Pace Project No.: 92503658
Pace Analytical Services Indianapolis
7726 Moller Road, Indianapolis, IN 46268
Illinois Accreditation #: 200074
Indiana Drinking Water Laboratory #: C-49-06
Kansas/TNI Certification #: E-10177
Kentucky UST Agency Interest #: 80226
Kentucky WW Laboratory ID #: 98019
Michigan Drinking Water Laboratory #9050
CERTIFICATIONS
Ohio VAP Certified Laboratory #: CL0065
Oklahoma Laboratory #: 9204
Texas Certification #: T104704355
West Virginia Certification #: 330
Wisconsin Laboratory #: 999788130
USDA Soil Permit #: P330-19-00257
Pace Analytical Gulf Coast
7979 Innovation Park Drive, Baton Rouge, LA 70820
North Dakota Certification #: R-195
Arkansas Certification #: 88-0655
Oklahoma Certification #: 2019-101
DoD ELAP Certification #: L18-597
South Carolina Certification #: 73006001
Florida Certification #: E87854
Texas Certification #: T104704178-19-11
Illinois Certification #: 004585
USDA Soil Permit # P330-19-00209
Kansas Certification #: E-10354
Virginia Certification #: 460215
Louisiana/LELAP Certification #: 01955
Washington Certification #: C929
North Carolina Certification #: 618
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
North Carolina Drinking Water Certification M 37712
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
SAMPLE ANALYTE COUNT
Project: NRLF
Pace Project No.: 92503658
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92503658001
B-23A-110220
AM20GAX
AWE
1
GCLA
AM20GAX
JCK2
3
GCLA
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
RSK-175
BMR
1
GCLA
EPA 8270E
PKS
5
PASI-C
EPA 8260D
CL
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
CJL
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
EPA 9060A
ECH
5
PASI-A
AM23G
MOS
1
GCLA
92503658002
13-2313-110220
AM20GAX
AWE
1
GCLA
AM20GAX
JCK2
3
GCLA
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
RSK-175
BMR
1
GCLA
EPA 8270E
PKS
5
PASI-C
EPA 8260D
CL
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
CJL
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
EPA 9060A
ECH
5
PASI-A
AM23G
MOS
1
GCLA
92503658003
13-2413-110220
EPA 8270E
PKS
5
PASI-C
EPA 8260D
CL
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
CJL
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92503658004
B-24A-110220
EPA 8270E
PKS
5
PASI-C
EPA 8260D
CL
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
SAMPLE ANALYTE COUNT
Project:
NRLF
Pace Project No.:
92503658
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
EPA 353.2 Rev 2.0 1993
CJL
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92503658005
B-21 B-110220
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
CJL
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92503658006
B-09C-110220
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D
CL
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
CJL
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92503658007
B-99C-110220
EPA 8270E
PKS
5
PASI-C
EPA 8260D
CL
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92503658008
SW-7-110220
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92503658009
SW-5-110220
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92503658010
SW-3-110220
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92503658011
SW-8-110220
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92503658012
CSW-1-110220
EPA 8260DMod.
LMB
3
PASI-C
92503658013
CSW-2-110220
EPA 8260D Mod.
LMB
3
PASI-C
92503658014
B-22A-110320
AM20GAX
AWE
1
GCLA
AM20GAX
JCK2
3
GCLA
RSK-175
BMR
1
GCLA
EPA 8270E
PKS
5
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
SAMPLE ANALYTE COUNT
Project: NRLF
Pace Project No.: 92503658
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
EPA 8260D
CL
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
CJL
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
EPA 9060A
ECH
5
PASI-A
AM23G
MOS
1
GCLA
92503658015
13-2213-110320
AM20GAX
AWE
1
GCLA
AM20GAX
JCK2
3
GCLA
RSK-175
BMR
1
GCLA
EPA 8270E
PKS
5
PASI-C
EPA 8260D
CL
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
CJL
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
EPA 9060A
ECH
5
PASI-A
AM23G
MOS
1
GCLA
92503658016
B-17C-110320
AM20GAX
AWE
1
GCLA
AM20GAX
JCK2
3
GCLA
RSK-175
BMR
1
GCLA
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
CJL
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
EPA 9060A
ECH
5
PASI-A
AM23G
MOS
1
GCLA
92503658017
B-17B-110320
AM20GAX
AWE
1
GCLA
AM20GAX
JCK2
3
GCLA
RSK-175
BMR
1
GCLA
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
NRLF
92503658
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
EPA 353.2 Rev 2.0 1993
CJL
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
EPA 9060A
ECH
5
PASI-A
AM23G
MOS
1
GCLA
92503658018
B-12-110320
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
CJL
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92503658019
13-3213-110320
AM20GAX
AWE
1
GCLA
AM20GAX
JCK2
3
GCLA
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
RSK-175
BMR
1
GCLA
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
CJL
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
EPA 9060A
ECH
5
PASI-A
AM23G
MOS
1
GCLA
92503658020
B-01-110320
AM20GAX
AWE
1
GCLA
AM20GAX
JCK2
3
GCLA
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
RSK-175
BMR
1
GCLA
EPA 8270E
PKS
5
PASI-C
EPA 8260D
CL
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
JKG
2
PASI-A
SM 4500-P E-2011
NAL
1
PASI-A
EPA 9056A
BRJ
1
PASI-A
EPA 9060A
ECH
5
PASI-A
AM23G
MOS
1
GCLA
92503658021
B-10-110320
AM20GAX
AWE
1
GCLA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
SAMPLE ANALYTE COUNT
Project: NRLF
Pace Project No.: 92503658
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
AM20GAX
JCK2
3
GCLA
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
RSK-175
BMR
1
GCLA
EPA 8270E
PKS
5
PASI-C
EPA 8260D
CL
53
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
JKG
2
PASI-A
SM 4500-P E-2011
NAL
1
PASI-A
EPA 9056A
BRJ
1
PASI-A
EPA 9060A
ECH
5
PASI-A
AM23G
MOS
1
GCLA
GCLA = Pace Analytical Gulf Coast
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-I = Pace Analytical Services - Indianapolis
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 7 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-23A-110220 Lab ID: 92503658001 Collected: 11/02/20 10:10 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen
ND nM
1.9
1
11/17/2011:50
1333-74-0
Indicator Gases Water LHC
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Ethane
2.6 ug/L
1.0
1
11/15/2015:31
74-84-0
Ethene
6.1 ug/L
1.0
1
11/15/2015:31
74-85-1
Methane
12000 ug/L
5.0
1
11/15/2015:31
74-82-8
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L
50.0
10
11/08/20 13:36
107-21-1 ED
EPA RSK-175
Analytical Method: RSK-175
Pace Analytical Gulf Coast
Carbon dioxide
335000 ug/L
45000
50
11/11/20 15:58
124-38-9
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
ND ug/L
10.0
1
11/05/20 09:50
11/06/20 16:30
92-52-4
Diphenyl ether (Phenyl ether)
43.1 ug/L
10.0
1
11/05/20 09:50
11/06/20 16:30
101-84-8
Surrogates
Nitrobenzene-d5(S)
47 %
10-144
1
11/05/20 09:50
11/06/20 16:30
4165-60-0
2-Fluorobiphenyl (S)
91 %
10-130
1
11/05/20 09:50
11/06/20 16:30
321-60-8
Terphenyl-d14 (S)
80 %
34-163
1
11/05/20 09:50
11/06/20 16:30
1718-51-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
5550 ug/L
625
25
11/05/20 01:07
67-64-1
Benzene
ND ug/L
25.0
25
11/05/20 01:07
71-43-2
Bromochloromethane
ND ug/L
25.0
25
11/05/20 01:07
74-97-5
Bromodichloromethane
ND ug/L
25.0
25
11/05/20 01:07
75-27-4
Bromoform
ND ug/L
25.0
25
11/05/20 01:07
75-25-2
Bromomethane
ND ug/L
50.0
25
11/05/20 01:07
74-83-9 v2
2-Butanone (MEK)
846 ug/L
125
25
11/05/20 01:07
78-93-3
Carbon disulfide
ND ug/L
50.0
25
11/05/20 01:07
75-15-0
Carbon tetrachloride
ND ug/L
25.0
25
11/05/20 01:07
56-23-5
Chlorobenzene
ND ug/L
25.0
25
11/05/20 01:07
108-90-7
Chloroethane
ND ug/L
25.0
25
11/05/20 01:07
75-00-3 v2
Chloroform
ND ug/L
125
25
11/05/20 01:07
67-66-3
Chloromethane
ND ug/L
25.0
25
11/05/20 01:07
74-87-3
Cyclohexane
ND ug/L
25.0
25
11/05/20 01:07
110-82-7
1,2-Dibromo-3-chloropropane
ND ug/L
125
25
11/05/20 01:07
96-12-8
Dibromochloromethane
ND ug/L
25.0
25
11/05/20 01:07
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
25.0
25
11/05/20 01:07
106-93-4
1,2-Dichlorobenzene
ND ug/L
25.0
25
11/05/20 01:07
95-50-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-23A-110220 Lab ID: 92503658001 Collected: 11/02/20 10:10 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,3-Dichlorobenzene
ND
ug/L
25.0
25
11/05/20 01:07
541-73-1
1,4-Dichlorobenzene
ND
ug/L
25.0
25
11/05/20 01:07
106-46-7
Dichlorodifluoromethane
ND
ug/L
25.0
25
11/05/20 01:07
75-71-8
1,1-Dichloroethane
39.6
ug/L
25.0
25
11/05/20 01:07
75-34-3
1,2-Dichloroethane
ND
ug/L
25.0
25
11/05/20 01:07
107-06-2
1,1-Dichloroethene
ND
ug/L
25.0
25
11/05/20 01:07
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
25.0
25
11/05/20 01:07
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
25.0
25
11/05/20 01:07
156-60-5
1,2-Dichloropropene
ND
ug/L
25.0
25
11/05/20 01:07
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
25.0
25
11/05/20 01:07
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
25.0
25
11/05/20 01:07
10061-02-6
Ethylbenzene
ND
ug/L
25.0
25
11/05/20 01:07
100-41-4
2-Hexanone
ND
ug/L
125
25
11/05/20 01:07
591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
25.0
25
11/05/20 01:07
98-82-8
Methyl acetate
ND
ug/L
250
25
11/05/20 01:07
79-20-9
Methylcyclohexane
ND
ug/L
250
25
11/05/20 01:07
108-87-2
Methylene Chloride
ND
ug/L
125
25
11/05/20 01:07
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
125
25
11/05/20 01:07
108-10-1
Methyl-tert-butyl ether
ND
ug/L
25.0
25
11/05/20 01:07
1634-04-4
Styrene
ND
ug/L
25.0
25
11/05/20 01:07
100-42-5
1,1,2,2-Tetrachloroethane
ND
ug/L
25.0
25
11/05/20 01:07
79-34-5
Tetrachloroethene
ND
ug/L
25.0
25
11/05/20 01:07
127-18-4
Toluene
ND
ug/L
25.0
25
11/05/20 01:07
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
25.0
25
11/05/20 01:07
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
25.0
25
11/05/20 01:07
120-82-1
1,1,1-Trichloroethane
ND
ug/L
25.0
25
11/05/20 01:07
71-55-6
1,1,2-Trichloroethane
ND
ug/L
25.0
25
11/05/20 01:07
79-00-5
Trichloroethene
ND
ug/L
25.0
25
11/05/20 01:07
79-01-6
Trichlorofluoromethane
ND
ug/L
25.0
25
11/05/20 01:07
75-69-4
1,1,2-Trichlorotrifluoroethane
ND
ug/L
25.0
25
11/05/20 01:07
76-13-1
Vinyl chloride
ND
ug/L
25.0
25
11/05/20 01:07
75-01-4
Xylene (Total)
ND
ug/L
25.0
25
11/05/20 01:07
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
25
11/05/20 01:07
460-00-4
1,2-Dichloroethane-d4 (S)
102
%
70-130
25
11/05/20 01:07
17060-07-0
Toluene-d8 (S)
99
%
70-130
25
11/05/20 01:07
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
3470
ug/L
100
50
11/04/20 19:17
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
99
%
70-130
50
11/04/20 19:17
17060-07-0
Toluene-d8 (S)
91
%
66-133
50
11/04/20 19:17
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-23A-110220
Lab ID: 92503658001 Collected:
11/02/20
10:10
Received: 11/03/20 17:24 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No.
Qual
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
3290 mg/L
5.0
1
11/11/20 15:23
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
11/03/20 23:38
14797-55-8
Nitrogen, Nitrite
0.046 mg/L
0.040
1
11/03/20 23:38
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.34 mg/L
0.25
5
11/04/20 08:31
F6,M1
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
5.1 mg/L
1.0
1
11/06/20 00:11
14808-79-8
M1
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
2410 mg/L
250
250
11/16/20 11:35
7440-44-0
M6
Total Organic Carbon
2390 mg/L
250
250
11/16/20 11:35
7440-44-0
M6
Total Organic Carbon
2400 mg/L
250
250
11/16/20 11:35
7440-44-0
M6
Total Organic Carbon
2390 mg/L
250
250
11/16/20 11:35
7440-44-0
M6
Mean Total Organic Carbon
2400 mg/L
250
250
11/16/20 11:35
7440-44-0
M6
Low Level Volatile Fatty Acids
Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid
2700 mg/L
250
500
11/18/20 06:34
64-19-7
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-2313-110220 Lab ID: 92503658002 Collected: 11/02/20 14:56 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen
ND nM
1.9
1
11/17/2012:02
1333-74-0
Indicator Gases Water LHC
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Ethane
1.2 ug/L
1.0
1
11/15/2015:43
74-84-0
Ethene
2.3 ug/L
1.0
1
11/15/2015:43
74-85-1
Methane
16000 ug/L
5.0
1
11/15/2015:43
74-82-8
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L
50.0
10
11/08/20 13:45
107-21-1 ED
EPA RSK-175
Analytical Method: RSK-175
Pace Analytical Gulf Coast
Carbon dioxide
301000 ug/L
45000
50
11/11/20 16:03
124-38-9
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
ND ug/L
10.0
1
11/05/20 09:50
11/06/20 16:55
92-52-4
Diphenyl ether (Phenyl ether)
69.6 ug/L
10.0
1
11/05/20 09:50
11/06/20 16:55
101-84-8
Surrogates
Nitrobenzene-d5(S)
76 %
10-144
1
11/05/20 09:50
11/06/20 16:55
4165-60-0
2-Fluorobiphenyl (S)
59 %
10-130
1
11/05/20 09:50
11/06/20 16:55
321-60-8
Terphenyl-d14 (S)
94 %
34-163
1
11/05/20 09:50
11/06/20 16:55
1718-51-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
5070 ug/L
625
25
11/05/20 01:25
67-64-1
Benzene
ND ug/L
25.0
25
11/05/20 01:25
71-43-2
Bromochloromethane
ND ug/L
25.0
25
11/05/20 01:25
74-97-5
Bromodichloromethane
ND ug/L
25.0
25
11/05/20 01:25
75-27-4
Bromoform
ND ug/L
25.0
25
11/05/20 01:25
75-25-2
Bromomethane
ND ug/L
50.0
25
11/05/20 01:25
74-83-9 v2
2-Butanone (MEK)
708 ug/L
125
25
11/05/20 01:25
78-93-3
Carbon disulfide
ND ug/L
50.0
25
11/05/20 01:25
75-15-0
Carbon tetrachloride
ND ug/L
25.0
25
11/05/20 01:25
56-23-5
Chlorobenzene
ND ug/L
25.0
25
11/05/20 01:25
108-90-7
Chloroethane
29.6 ug/L
25.0
25
11/05/20 01:25
75-00-3 v2
Chloroform
ND ug/L
125
25
11/05/20 01:25
67-66-3
Chloromethane
ND ug/L
25.0
25
11/05/20 01:25
74-87-3
Cyclohexane
ND ug/L
25.0
25
11/05/20 01:25
110-82-7
1,2-Dibromo-3-chloropropane
ND ug/L
125
25
11/05/20 01:25
96-12-8
Dibromochloromethane
ND ug/L
25.0
25
11/05/20 01:25
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
25.0
25
11/05/20 01:25
106-93-4
1,2-Dichlorobenzene
ND ug/L
25.0
25
11/05/20 01:25
95-50-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: 13-2313-110220 Lab ID: 92503658002 Collected: 11/02/20 14:56 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,3-Dichlorobenzene
ND
ug/L
25.0
25
11/05/20 01:25
541-73-1
1,4-Dichlorobenzene
ND
ug/L
25.0
25
11/05/20 01:25
106-46-7
Dichlorodifluoromethane
ND
ug/L
25.0
25
11/05/20 01:25
75-71-8
1,1-Dichloroethane
ND
ug/L
25.0
25
11/05/20 01:25
75-34-3
1,2-Dichloroethane
ND
ug/L
25.0
25
11/05/20 01:25
107-06-2
1,1-Dichloroethene
ND
ug/L
25.0
25
11/05/20 01:25
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
25.0
25
11/05/20 01:25
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
25.0
25
11/05/20 01:25
156-60-5
1,2-Dichloropropene
ND
ug/L
25.0
25
11/05/20 01:25
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
25.0
25
11/05/20 01:25
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
25.0
25
11/05/20 01:25
10061-02-6
Ethylbenzene
ND
ug/L
25.0
25
11/05/20 01:25
100-41-4
2-Hexanone
ND
ug/L
125
25
11/05/20 01:25
591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
25.0
25
11/05/20 01:25
98-82-8
Methyl acetate
ND
ug/L
250
25
11/05/20 01:25
79-20-9
Methylcyclohexane
ND
ug/L
250
25
11/05/20 01:25
108-87-2
Methylene Chloride
ND
ug/L
125
25
11/05/20 01:25
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
125
25
11/05/20 01:25
108-10-1
Methyl-tert-butyl ether
ND
ug/L
25.0
25
11/05/20 01:25
1634-04-4
Styrene
ND
ug/L
25.0
25
11/05/20 01:25
100-42-5
1,1,2,2-Tetrachloroethane
ND
ug/L
25.0
25
11/05/20 01:25
79-34-5
Tetrachloroethene
ND
ug/L
25.0
25
11/05/20 01:25
127-18-4
Toluene
ND
ug/L
25.0
25
11/05/20 01:25
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
25.0
25
11/05/20 01:25
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
25.0
25
11/05/20 01:25
120-82-1
1,1,1-Trichloroethane
ND
ug/L
25.0
25
11/05/20 01:25
71-55-6
1,1,2-Trichloroethane
ND
ug/L
25.0
25
11/05/20 01:25
79-00-5
Trichloroethene
ND
ug/L
25.0
25
11/05/20 01:25
79-01-6
Trichlorofluoromethane
ND
ug/L
25.0
25
11/05/20 01:25
75-69-4
1,1,2-Trichlorotrifluoroethane
ND
ug/L
25.0
25
11/05/20 01:25
76-13-1
Vinyl chloride
ND
ug/L
25.0
25
11/05/20 01:25
75-01-4
Xylene (Total)
ND
ug/L
25.0
25
11/05/20 01:25
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
25
11/05/20 01:25
460-00-4
1,2-Dichloroethane-d4 (S)
103
%
70-130
25
11/05/20 01:25
17060-07-0
Toluene-d8 (S)
99
%
70-130
25
11/05/20 01:25
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
3150
ug/L
100
50
11/04/20 19:37
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
99
%
70-130
50
11/04/20 19:37
17060-07-0
Toluene-d8 (S)
91
%
66-133
50
11/04/20 19:37
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: 13-2313-110220
Lab ID: 92503658002 Collected:
11/02/20 14:56
Received: 11/03/20 17:24 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
2450 mg/L
5.0
1
11/11/20 16:40
M1
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
11/03/20 23:46
14797-55-8
Nitrogen, Nitrite
0.16 mg/L
0.040
1
11/03/20 23:46
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
ND mg/L
0.25
5
11/04/20 08:36
F6
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
4.7 mg/L
1.0
1
11/06/20 00:56
14808-79-8
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
1890 mg/L
250
250
11/16/20 12:29
7440-44-0
Total Organic Carbon
1910 mg/L
250
250
11/16/20 12:29
7440-44-0
Total Organic Carbon
1920 mg/L
250
250
11/16/20 12:29
7440-44-0
Total Organic Carbon
1950 mg/L
250
250
11/16/20 12:29
7440-44-0
Mean Total Organic Carbon
1920 mg/L
250
250
11/16/20 12:29
7440-44-0
Low Level Volatile Fatty Acids
Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid
2200 mg/L
250
500
11/18/20 07:28
64-19-7
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-24B-110220 Lab ID: 92503658003 Collected: 11/02/20 10:22 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
Biphenyl (Diphenyl)
ND
ug/L
10.0
1
11/05/20 09:50
11/06/20 17:20
92-52-4
Diphenyl ether (Phenyl ether)
10.4
ug/L
10.0
1
11/05/20 09:50
11/06/20 17:20
101-84-8
Surrogates
Nitrobenzene-d5(S)
71
%
10-144
1
11/05/20 09:50
11/06/20 17:20
4165-60-0
2-Fluorobiphenyl (S)
32
%
10-130
1
11/05/20 09:50
11/06/20 17:20
321-60-8
Terphenyl-d14 (S)
117
%
34-163
1
11/05/20 09:50
11/06/20 17:20
1718-51-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
11/04/20 22:59
67-64-1
Benzene
ND
ug/L
1.0
1
11/04/20 22:59
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
11/04/20 22:59
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
11/04/20 22:59
75-27-4
Bromoform
ND
ug/L
1.0
1
11/04/20 22:59
75-25-2
Bromomethane
ND
ug/L
2.0
1
11/04/20 22:59
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
11/04/20 22:59
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
11/04/20 22:59
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
11/04/20 22:59
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
11/04/20 22:59
108-90-7
Chloroethane
4.1
ug/L
1.0
1
11/04/20 22:59
75-00-3
Chloroform
ND
ug/L
5.0
1
11/04/20 22:59
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/04/20 22:59
74-87-3
Cyclohexane
ND
ug/L
1.0
1
11/04/20 22:59
110-82-7
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
11/04/20 22:59
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
11/04/20 22:59
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
11/04/20 22:59
106-93-4
1,2-Dichlorobenzene
ND
ug/L
1.0
1
11/04/20 22:59
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
1
11/04/20 22:59
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
11/04/20 22:59
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
1
11/04/20 22:59
75-71-8
1,1-Dichloroethane
ND
ug/L
1.0
1
11/04/20 22:59
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
11/04/20 22:59
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
11/04/20 22:59
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
11/04/20 22:59
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
11/04/20 22:59
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
1
11/04/20 22:59
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
11/04/20 22:59
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
11/04/20 22:59
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
11/04/20 22:59
100-41-4
2-Hexanone
ND
ug/L
5.0
1
11/04/20 22:59
591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
1.0
1
11/04/20 22:59
98-82-8
Methyl acetate
ND
ug/L
10.0
1
11/04/20 22:59
79-20-9
Methylcyclohexane
ND
ug/L
10.0
1
11/04/20 22:59
108-87-2
Methylene Chloride
ND
ug/L
5.0
1
11/04/20 22:59
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
11/04/20 22:59
108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
1
11/04/20 22:59
1634-04-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
v2
v2
Page 14 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-2413-110220 Lab ID: 92503658003 Collected: 11/02/20 10:22 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
2320B Alkalinity
Alkalinity, Total as CaCO3
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
9056 IC anions 28 Days
Sulfate
Date: 11/19/2020 04:25 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
98 %
70-130
102 %
70-130
99 %
70-130
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
103 ug/L
4.0
97 %
70-130
91 %
66-133
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
428 mg/L
5.0
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
ND mg/L
0.040
ND mg/L
0.040
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
0.064 mg/L
0.050
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
ND mg/L
1.0
1 11/04/20 22:59
100-42-5
1 11/04/20 22:59
79-34-5
1 11/04/20 22:59
127-18-4
1 11/04/20 22:59
108-88-3
1 11/04/20 22:59
87-61-6
1 11/04/20 22:59
120-82-1
1 11/04/20 22:59
71-55-6
1 11/04/20 22:59
79-00-5
1 11/04/20 22:59
79-01-6
1 11/04/20 22:59
75-69-4
1 11/04/20 22:59
76-13-1
1 11/04/20 22:59
75-01-4
1 11/04/20 22:59
1330-20-7
1 11/04/20 22:59
460-00-4
1 11/04/20 22:59
17060-07-0
1 11/04/20 22:59
2037-26-5
2 11/04/20 18:58
123-91-1
2 11/04/20 18:58 17060-07-0
2 11/04/20 18:58 2037-26-5
1 11 /12/20 13:54
1 11/03/20 23:41 14797-55-8
1 11/03/20 23:41 14797-65-0
1 11/04/20 08:33
1 11 /06/20 01:11 14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
F6
Page 15 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-24A-110220 Lab ID: 92503658004 Collected: 11/02/20 11:17 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
Biphenyl (Diphenyl)
ND
ug/L
10.0
1
11/05/20 09:50
11/06/20 17:45
92-52-4
Diphenyl ether (Phenyl ether)
ND
ug/L
10.0
1
11/05/20 09:50
11/06/20 17:45
101-84-8
Surrogates
Nitrobenzene-d5(S)
99
%
10-144
1
11/05/20 09:50
11/06/20 17:45
4165-60-0
2-Fluorobiphenyl (S)
61
%
10-130
1
11/05/20 09:50
11/06/20 17:45
321-60-8
Terphenyl-d14 (S)
116
%
34-163
1
11/05/20 09:50
11/06/20 17:45
1718-51-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
11/04/20 23:17
67-64-1
Benzene
ND
ug/L
1.0
1
11/04/20 23:17
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
11/04/20 23:17
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
11/04/20 23:17
75-27-4
Bromoform
ND
ug/L
1.0
1
11/04/20 23:17
75-25-2
Bromomethane
ND
ug/L
2.0
1
11/04/20 23:17
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
11/04/20 23:17
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
11/04/20 23:17
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
11/04/20 23:17
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
11/04/20 23:17
108-90-7
Chloroethane
1.1
ug/L
1.0
1
11/04/20 23:17
75-00-3
Chloroform
ND
ug/L
5.0
1
11/04/20 23:17
67-66-3
Chloromethane
ND
ug/L
1.0
1
11/04/20 23:17
74-87-3
Cyclohexane
ND
ug/L
1.0
1
11/04/20 23:17
110-82-7
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
11/04/20 23:17
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
11/04/20 23:17
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
11/04/20 23:17
106-93-4
1,2-Dichlorobenzene
ND
ug/L
1.0
1
11/04/20 23:17
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
1
11/04/20 23:17
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
11/04/20 23:17
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
1
11/04/20 23:17
75-71-8
1,1-Dichloroethane
10.3
ug/L
1.0
1
11/04/20 23:17
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
11/04/20 23:17
107-06-2
1,1-Dichloroethene
1.9
ug/L
1.0
1
11/04/20 23:17
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
11/04/20 23:17
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
11/04/20 23:17
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
1
11/04/20 23:17
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
11/04/20 23:17
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
11/04/20 23:17
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
11/04/20 23:17
100-41-4
2-Hexanone
ND
ug/L
5.0
1
11/04/20 23:17
591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
1.0
1
11/04/20 23:17
98-82-8
Methyl acetate
ND
ug/L
10.0
1
11/04/20 23:17
79-20-9
Methylcyclohexane
ND
ug/L
10.0
1
11/04/20 23:17
108-87-2
Methylene Chloride
ND
ug/L
5.0
1
11/04/20 23:17
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
11/04/20 23:17
108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
1
11/04/20 23:17
1634-04-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
v2
v2
Page 16 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-24A-110220 Lab ID: 92503658004 Collected: 11/02/20 11:17 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
2320B Alkalinity
Alkalinity, Total as CaCO3
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
9056 IC anions 28 Days
Sulfate
Date: 11/19/2020 04:25 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
ND ug/L
1.0
99 %
70-130
99 %
70-130
101 %
70-130
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
182 ug/L
5.0
98 %
70-130
91 %
66-133
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
390 mg/L
5.0
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
ND mg/L
0.040
ND mg/L
0.040
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
0.16 mg/L
0.050
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
ND mg/L
1.0
1 11/04/20 23:17
100-42-5
1 11/04/20 23:17
79-34-5
1 11/04/20 23:17
127-18-4
1 11/04/20 23:17
108-88-3
1 11/04/20 23:17
87-61-6
1 11/04/20 23:17
120-82-1
1 11/04/20 23:17
71-55-6
1 11/04/20 23:17
79-00-5
1 11/04/20 23:17
79-01-6
1 11/04/20 23:17
75-69-4
1 11/04/20 23:17
76-13-1
1 11/04/20 23:17
75-01-4
1 11/04/20 23:17
1330-20-7
1
11/04/20 23:17
460-00-4
1
11/04/20 23:17
17060-07-0
1
11/04/20 23:17
2037-26-5
2.5
11/04/20 19:56
123-91-1
2.5 11/04/20 19:56 17060-07-0
2.5 11/04/20 19:56 2037-26-5
1 11 /12/20 14:04
1 11/03/20 23:44 14797-55-8
1 11/03/20 23:44 14797-65-0
1 11/04/20 08:35
1 11 /06/20 01:26 14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
F6
Page 17 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: 13-2113-110220
Lab ID: 92503658005 Collected:
11/02/20 15:00
Received: 11/03/20 17:24 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
35.7 ug/L
2.0
1
11/04/20 17:40
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
96 %
70-130
1
11/04/20 17:40
17060-07-0
Toluene-d8 (S)
91 %
66-133
1
11/04/20 17:40
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
239 mg/L
5.0
1
11/12/20 14:13
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
11/03/20 23:49
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
11/03/20 23:49
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.10 mg/L
0.050
1
11/04/20 08:38
F6
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
18.6 mg/L
1.0
1
11/06/20 02:11
14808-79-8
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-09C-110220 Lab ID: 92503658006 Collected: 11/02/20 16:58 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical
Services - Indianapolis
Ethylene glycol
ND
mg/L
5.0
1
11/08/20 13:17
107-21-1
8270E RVE
Analytical Method:
EPA 8270E Preparation Method: EPA
3510C
Pace Analytical
Services - Charlotte
Biphenyl (Diphenyl)
ND
ug/L
10.0
1
11/05/20 09:50
11/06/20 18:10
92-52-4
Diphenyl ether (Phenyl ether)
25.5
ug/L
10.0
1
11/05/20 09:50
11/06/20 18:10
101-84-8
Surrogates
Nitrobenzene-d5(S)
101
%
10-144
1
11/05/20 09:50
11/06/20 18:10
4165-60-0
2-Fluorobiphenyl (S)
62
%
10-130
1
11/05/20 09:50
11/06/20 18:10
321-60-8
Terphenyl-d14 (S)
94
%
34-163
1
11/05/20 09:50
11/06/20 18:10
1718-51-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
2660
ug/L
312
12.5
11/05/20 00:49
67-64-1
Benzene
ND
ug/L
12.5
12.5
11/05/20 00:49
71-43-2
Bromochloromethane
ND
ug/L
12.5
12.5
11/05/20 00:49
74-97-5
Bromodichloromethane
ND
ug/L
12.5
12.5
11/05/20 00:49
75-27-4
Bromoform
ND
ug/L
12.5
12.5
11/05/20 00:49
75-25-2
Bromomethane
ND
ug/L
25.0
12.5
11/05/20 00:49
74-83-9
2-Butanone (MEK)
451
ug/L
62.5
12.5
11/05/20 00:49
78-93-3
Carbon disulfide
ND
ug/L
25.0
12.5
11/05/20 00:49
75-15-0
Carbon tetrachloride
ND
ug/L
12.5
12.5
11/05/20 00:49
56-23-5
Chlorobenzene
ND
ug/L
12.5
12.5
11/05/20 00:49
108-90-7
Chloroethane
ND
ug/L
12.5
12.5
11/05/20 00:49
75-00-3
Chloroform
ND
ug/L
62.5
12.5
11/05/20 00:49
67-66-3
Chloromethane
ND
ug/L
12.5
12.5
11/05/20 00:49
74-87-3
Cyclohexane
ND
ug/L
12.5
12.5
11/05/20 00:49
110-82-7
1,2-Dibromo-3-chloropropane
ND
ug/L
62.5
12.5
11/05/20 00:49
96-12-8
Dibromochloromethane
ND
ug/L
12.5
12.5
11/05/20 00:49
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
12.5
12.5
11/05/20 00:49
106-93-4
1,2-Dichlorobenzene
ND
ug/L
12.5
12.5
11/05/20 00:49
95-50-1
1,3-Dichlorobenzene
ND
ug/L
12.5
12.5
11/05/20 00:49
541-73-1
1,4-Dichlorobenzene
ND
ug/L
12.5
12.5
11/05/20 00:49
106-46-7
Dichlorodifluoromethane
ND
ug/L
12.5
12.5
11/05/20 00:49
75-71-8
1,1-Dichloroethane
ND
ug/L
12.5
12.5
11/05/20 00:49
75-34-3
1,2-Dichloroethane
ND
ug/L
12.5
12.5
11/05/20 00:49
107-06-2
1,1-Dichloroethene
ND
ug/L
12.5
12.5
11/05/20 00:49
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
12.5
12.5
11/05/20 00:49
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
12.5
12.5
11/05/20 00:49
156-60-5
1,2-Dichloropropane
ND
ug/L
12.5
12.5
11/05/20 00:49
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
12.5
12.5
11/05/20 00:49
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
12.5
12.5
11/05/20 00:49
10061-02-6
Ethylbenzene
ND
ug/L
12.5
12.5
11/05/20 00:49
100-41-4
2-Hexanone
ND
ug/L
62.5
12.5
11/05/20 00:49
591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
12.5
12.5
11/05/20 00:49
98-82-8
Methyl acetate
ND
ug/L
125
12.5
11/05/20 00:49
79-20-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
v2
v2
Page 19 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-09C-110220 Lab ID: 92503658006 Collected: 11/02/20 16:58 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Methylcyclohexane
ND ug/L
125
12.5
11/05/20 00:49
108-87-2
Methylene Chloride
ND ug/L
62.5
12.5
11/05/20 00:49
75-09-2
4-Methyl-2-pentanone (MIBK)
87.5 ug/L
62.5
12.5
11/05/20 00:49
108-10-1
Methyl-tert-butyl ether
ND ug/L
12.5
12.5
11/05/20 00:49
1634-04-4
Styrene
ND ug/L
12.5
12.5
11/05/20 00:49
100-42-5
1,1,2,2-Tetrachloroethane
ND ug/L
12.5
12.5
11/05/20 00:49
79-34-5
Tetrachloroethene
ND ug/L
12.5
12.5
11/05/20 00:49
127-18-4
Toluene
ND ug/L
12.5
12.5
11/05/20 00:49
108-88-3
1,2,3-Trichlorobenzene
ND ug/L
12.5
12.5
11/05/20 00:49
87-61-6
1,2,4-Trichlorobenzene
ND ug/L
12.5
12.5
11/05/20 00:49
120-82-1
1,1,1-Trichloroethane
ND ug/L
12.5
12.5
11/05/20 00:49
71-55-6
1,1,2-Trichloroethane
ND ug/L
12.5
12.5
11/05/20 00:49
79-00-5
Trichloroethene
ND ug/L
12.5
12.5
11/05/20 00:49
79-01-6
Trichlorofluoromethane
ND ug/L
12.5
12.5
11/05/20 00:49
75-69-4
1,1,2-Trichlorotrifluoroethane
ND ug/L
12.5
12.5
11/05/20 00:49
76-13-1
Vinyl chloride
ND ug/L
12.5
12.5
11/05/20 00:49
75-01-4
Xylene (Total)
ND ug/L
12.5
12.5
11/05/20 00:49
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
97 %
70-130
12.5
11/05/20 00:49
460-00-4
1,2-Dichloroethane-d4 (S)
104 %
70-130
12.5
11/05/20 00:49
17060-07-0
Toluene-d8 (S)
100 %
70-130
12.5
11/05/20 00:49
2037-26-5
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
743 ug/L
20.0
10
11/04/20 20:15
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
97 %
70-130
10
11/04/20 20:15
17060-07-0
Toluene-d8 (S)
91 %
66-133
10
11/04/20 20:15
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
2790 mg/L
5.0
1
11/11/20 20:09
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
11/03/20 23:50
14797-55-8
Nitrogen, Nitrite
0.18 mg/L
0.040
1
11/03/20 23:50
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
ND mg/L
0.25
5
11/04/20 08:39
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
1.2 mg/L
1.0
1
11/06/20 02:26
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
D3,F6
Page 20 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-99C-110220 Lab ID: 92503658007 Collected: 11/02/20 17:10 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical
Services - Charlotte
Biphenyl (Diphenyl)
ND
ug/L
10.0
1
11/05/20 09:50
11/06/20 18:36
92-52-4
Diphenyl ether (Phenyl ether)
24.4
ug/L
10.0
1
11/05/20 09:50
11/06/20 18:36
101-84-8
Surrogates
Nitrobenzene-d5(S)
112
%
10-144
1
11/05/20 09:50
11/06/20 18:36
4165-60-0
2-Fluorobiphenyl (S)
78
%
10-130
1
11/05/20 09:50
11/06/20 18:36
321-60-8
Terphenyl-d14 (S)
104
%
34-163
1
11/05/20 09:50
11/06/20 18:36
1718-51-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
2680
ug/L
250
10
11/05/20 00:30
67-64-1
Benzene
ND
ug/L
10.0
10
11/05/20 00:30
71-43-2
Bromochloromethane
ND
ug/L
10.0
10
11/05/20 00:30
74-97-5
Bromodichloromethane
ND
ug/L
10.0
10
11/05/20 00:30
75-27-4
Bromoform
ND
ug/L
10.0
10
11/05/20 00:30
75-25-2
Bromomethane
ND
ug/L
20.0
10
11/05/20 00:30
74-83-9
2-Butanone (MEK)
453
ug/L
50.0
10
11/05/20 00:30
78-93-3
Carbon disulfide
ND
ug/L
20.0
10
11/05/20 00:30
75-15-0
Carbon tetrachloride
ND
ug/L
10.0
10
11/05/20 00:30
56-23-5
Chlorobenzene
ND
ug/L
10.0
10
11/05/20 00:30
108-90-7
Chloroethane
ND
ug/L
10.0
10
11/05/20 00:30
75-00-3
Chloroform
ND
ug/L
50.0
10
11/05/20 00:30
67-66-3
Chloromethane
ND
ug/L
10.0
10
11/05/20 00:30
74-87-3
Cyclohexane
ND
ug/L
10.0
10
11/05/20 00:30
110-82-7
1,2-Dibromo-3-chloropropane
ND
ug/L
50.0
10
11/05/20 00:30
96-12-8
Dibromochloromethane
ND
ug/L
10.0
10
11/05/20 00:30
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
10.0
10
11/05/20 00:30
106-93-4
1,2-Dichlorobenzene
ND
ug/L
10.0
10
11/05/20 00:30
95-50-1
1,3-Dichlorobenzene
ND
ug/L
10.0
10
11/05/20 00:30
541-73-1
1,4-Dichlorobenzene
ND
ug/L
10.0
10
11/05/20 00:30
106-46-7
Dichlorodifluoromethane
ND
ug/L
10.0
10
11/05/20 00:30
75-71-8
1,1-Dichloroethane
ND
ug/L
10.0
10
11/05/20 00:30
75-34-3
1,2-Dichloroethane
ND
ug/L
10.0
10
11/05/20 00:30
107-06-2
1,1-Dichloroethene
ND
ug/L
10.0
10
11/05/20 00:30
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
10.0
10
11/05/20 00:30
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
10.0
10
11/05/20 00:30
156-60-5
1,2-Dichloropropane
ND
ug/L
10.0
10
11/05/20 00:30
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
10.0
10
11/05/20 00:30
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
10.0
10
11/05/20 00:30
10061-02-6
Ethylbenzene
ND
ug/L
10.0
10
11/05/20 00:30
100-41-4
2-Hexanone
ND
ug/L
50.0
10
11/05/20 00:30
591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
10.0
10
11/05/20 00:30
98-82-8
Methyl acetate
ND
ug/L
100
10
11/05/20 00:30
79-20-9
Methylcyclohexane
ND
ug/L
100
10
11/05/20 00:30
108-87-2
Methylene Chloride
ND
ug/L
50.0
10
11/05/20 00:30
75-09-2
4-Methyl-2-pentanone (MIBK)
88.5
ug/L
50.0
10
11/05/20 00:30
108-10-1
Methyl-tert-butyl ether
ND
ug/L
10.0
10
11/05/20 00:30
1634-04-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
v2
v2
Page 21 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-99C-110220 Lab ID: 92503658007 Collected: 11/02/20 17:10 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 11/19/2020 04:25 PM
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
ND
ug/L
10.0
10
11/05/20 00:30
100-42-5
ND
ug/L
10.0
10
11/05/20 00:30
79-34-5
ND
ug/L
10.0
10
11/05/20 00:30
127-18-4
ND
ug/L
10.0
10
11/05/20 00:30
108-88-3
ND
ug/L
10.0
10
11/05/20 00:30
87-61-6
ND
ug/L
10.0
10
11/05/20 00:30
120-82-1
ND
ug/L
10.0
10
11/05/20 00:30
71-55-6
ND
ug/L
10.0
10
11/05/20 00:30
79-00-5
ND
ug/L
10.0
10
11/05/20 00:30
79-01-6
ND
ug/L
10.0
10
11/05/20 00:30
75-69-4
ND
ug/L
10.0
10
11/05/20 00:30
76-13-1
ND
ug/L
10.0
10
11/05/20 00:30
75-01-4
ND
ug/L
10.0
10
11/05/20 00:30
1330-20-7
99
%
70-130
10
11/05/20 00:30
460-00-4
106
%
70-130
10
11/05/20 00:30
17060-07-0
99
%
70-130
10
11/05/20 00:30
2037-26-5
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
686
ug/L
25.0
12.5
11/04/20 20:35
123-91-1
100
%
70-130
12.5
11/04/20 20:35
17060-07-0
92
%
66-133
12.5
11/04/20 20:35
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 22 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: SW-7-110220
Lab ID: 92503658008 Collected: 11/02/20 13:00
Received: 11/03/20 17:24 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
11/09/20 23:42
107-21-1
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (biphenyl)
ND ug/L 10.0
1
11/05/20 09:50
11/06/20 19:01
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L 10.0
1
11/05/20 09:50
11/06/20 19:01
101-84-8
Surrogates
Nitrobenzene-d5(S)
48 % 10-144
1
11/05/20 09:50
11/06/20 19:01
4165-60-0
2-Fluorobiphenyl (S)
21 % 10-130
1
11/05/20 09:50
11/06/20 19:01
321-60-8
Terphenyl-d14 (S)
82 % 34-163
1
11/05/20 09:50
11/06/20 19:01
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
1
11/04/20 16:23
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
97 % 70-130
1
11/04/20 16:23
17060-07-0
Toluene-d8 (S)
90 % 66-133
1
11/04/20 16:23
2037-26-5
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 23 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: SW-5-110220
Lab ID: 92503658009 Collected: 11/02/20 13:12
Received: 11/03/20 17:24 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
11/09/20 23:57
107-21-1
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (biphenyl)
ND ug/L 10.0
1
11/06/20 08:53
11/07/20 12:29
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L 10.0
1
11/06/20 08:53
11/07/20 12:29
101-84-8
Surrogates
Nitrobenzene-d5 (S)
46 % 10-144
1
11/06/20 08:53
11/07/20 12:29
4165-60-0
2-Fluorobiphenyl (S)
36 % 10-130
1
11/06/20 08:53
11/07/20 12:29
321-60-8
Terphenyl-d14 (S)
74 % 34-163
1
11/06/20 08:53
11/07/20 12:29
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
1
11/04/20 16:42
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
97 % 70-130
1
11/04/20 16:42
17060-07-0
Toluene-d8 (S)
90 % 66-133
1
11/04/20 16:42
2037-26-5
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 24 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: SW-3-110220
Lab ID: 92503658010 Collected: 11/02/20 13:25
Received: 11/03/20 17:24 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
11/10/20 00:06
107-21-1
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (biphenyl)
ND ug/L 10.0
1
11/06/20 08:53
11/07/20 12:58
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L 10.0
1
11/06/20 08:53
11/07/20 12:58
101-84-8
Surrogates
Nitrobenzene-d5(S)
71 % 10-144
1
11/06/20 08:53
11/07/20 12:58
4165-60-0
2-Fluorobiphenyl (S)
50 % 10-130
1
11/06/20 08:53
11/07/20 12:58
321-60-8
Terphenyl-d14 (S)
106 % 34-163
1
11/06/20 08:53
11/07/20 12:58
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
1
11/04/20 17:01
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
97 % 70-130
1
11/04/20 17:01
17060-07-0
Toluene-d8 (S)
91 % 66-133
1
11/04/20 17:01
2037-26-5
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 25 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: SW-8-110220
Lab ID: 92503658011 Collected: 11/02/20 14:00
Received: 11/03/20 17:24 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
11/10/20 18:22
107-21-1
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (biphenyl)
ND ug/L 10.0
1
11/06/20 08:53
11/07/20 13:27
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L 10.0
1
11/06/20 08:53
11/07/20 13:27
101-84-8
Surrogates
Nitrobenzene-d5(S)
51 % 10-144
1
11/06/20 08:53
11/07/20 13:27
4165-60-0
2-Fluorobiphenyl (S)
26 % 10-130
1
11/06/20 08:53
11/07/20 13:27
321-60-8
Terphenyl-d14 (S)
98 % 34-163
1
11/06/20 08:53
11/07/20 13:27
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
1
11/04/20 17:21
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
98 % 70-130
1
11/04/20 17:21
17060-07-0
Toluene-d8 (S)
92 % 66-133
1
11/04/20 17:21
2037-26-5
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 26 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: CSW-1-110220
Lab ID: 92503658012 Collected:
11/02/20 16:08
Received: 11/03/20 17:24 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
368 ug/L
20.0
10
11/04/20 20:54
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
98 %
70-130
10
11/04/20 20:54
17060-07-0
Toluene-d8(S)
92 %
66-133
10
11/04/20 20:54
2037-26-5
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 27 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: CSW-2-110220
Lab ID: 92503658013 Collected:
11/02/20 16:20
Received: 11/03/20 17:24 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
279 ug/L
10.0
5
11/05/20 11:49
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
86 %
70-130
5
11/05/20 11:49
17060-07-0
Toluene-d8 (S)
95 %
66-133
5
11/05/20 11:49
2037-26-5
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 28 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-22A-110320 Lab ID: 92503658014 Collected: 11/03/20 08:00 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2
Hydrogen
Indicator Gases Water LHC
Ethane
Ethene
Methane
EPA RSK-175
Carbon dioxide
8270E RVE
Biphenyl (Diphenyl)
Diphenyl ether (Phenyl ether)
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
8260D MSV Low Level Landfill
Acetone
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
Date: 11/19/2020 04:25 PM
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
ND nM
1.9
1
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
4.3 ug/L
1.0
1
1.3 ug/L
1.0
1
100 ug/L
5.0
1
Analytical Method: RSK-175
Pace Analytical Gulf Coast
168000 ug/L
18000
20
Analytical Method: EPA 8270E Preparation
Method: EPA 3510C
Pace Analytical Services - Charlotte
11 /17/20 12:15 1333-74-0
11/15/2015:55 74-84-0
11/15/2015:55 74-85-1
11/15/2015:55 74-82-8
11 /13/20 11:57 124-38-9
ND
ug/L
10.0
1
11/06/20 08:53
11/07/20 13:56
92-52-4
ND
ug/L
10.0
1
11/06/20 08:53
11/07/20 13:56
101-84-8
70
%
10-144
1
11/06/20 08:53
11/07/20 13:56
4165-60-0
53
%
10-130
1
11/06/20 08:53
11/07/20 13:56
321-60-8
94
%
34-163
1
11/06/20 08:53
11/07/20 13:56
1718-51-0
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
25.0
1
11/04/20 23:36
67-64-1
ND
ug/L
1.0
1
11/04/20 23:36
71-43-2
ND
ug/L
1.0
1
11/04/20 23:36
74-97-5
ND
ug/L
1.0
1
11/04/20 23:36
75-27-4
ND
ug/L
1.0
1
11/04/20 23:36
75-25-2
ND
ug/L
2.0
1
11/04/20 23:36
74-83-9
ND
ug/L
5.0
1
11/04/20 23:36
78-93-3
ND
ug/L
2.0
1
11/04/20 23:36
75-15-0
ND
ug/L
1.0
1
11/04/20 23:36
56-23-5
5.5
ug/L
1.0
1
11/04/20 23:36
108-90-7
ND
ug/L
1.0
1
11/04/20 23:36
75-00-3
ND
ug/L
5.0
1
11/04/20 23:36
67-66-3
ND
ug/L
1.0
1
11/04/20 23:36
74-87-3
ND
ug/L
1.0
1
11/04/20 23:36
110-82-7
ND
ug/L
5.0
1
11/04/20 23:36
96-12-8
ND
ug/L
1.0
1
11/04/20 23:36
124-48-1
ND
ug/L
1.0
1
11/04/20 23:36
106-93-4
ND
ug/L
1.0
1
11/04/20 23:36
95-50-1
ND
ug/L
1.0
1
11/04/20 23:36
541-73-1
ND
ug/L
1.0
1
11/04/20 23:36
106-46-7
ND
ug/L
1.0
1
11/04/20 23:36
75-71-8
4.2
ug/L
1.0
1
11/04/20 23:36
75-34-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v2
v2
Page 29 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-22A-110320 Lab ID: 92503658014 Collected: 11/03/20 08:00 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene (Cumene)
Methyl acetate
Methylcyclohexane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
2320B Alkalinity
Alkalinity, Total as CaCO3
Date: 11/19/2020 04:25 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
2.3
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
1.1
ug/L
ND
ug/L
99
%
103
%
101
%
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1270
ug/L
97
%
91
%
Analytical Method:
SM 2320B-2011
Pace Analytical
Services -Asheville
564
mg/L
1.0
1
11/04/20 23:36
107-06-2
1.0
1
11/04/20 23:36
75-35-4
1.0
1
11/04/20 23:36
156-59-2
1.0
1
11/04/20 23:36
156-60-5
1.0
1
11/04/20 23:36
78-87-5
1.0
1
11/04/20 23:36
10061-01-5
1.0
1
11/04/20 23:36
10061-02-6
1.0
1
11/04/20 23:36
100-41-4
5.0
1
11/04/20 23:36
591-78-6
1.0
1
11/04/20 23:36
98-82-8
10.0
1
11/04/20 23:36
79-20-9
10.0
1
11/04/20 23:36
108-87-2
5.0
1
11/04/20 23:36
75-09-2
5.0
1
11/04/20 23:36
108-10-1
1.0
1
11/04/20 23:36
1634-04-4
1.0
1
11/04/20 23:36
100-42-5
1.0
1
11/04/20 23:36
79-34-5
1.0
1
11/04/20 23:36
127-18-4
1.0
1
11/04/20 23:36
108-88-3
1.0
1
11/04/20 23:36
87-61-6
1.0
1
11/04/20 23:36
120-82-1
1.0
1
11/04/20 23:36
71-55-6
1.0
1
11/04/20 23:36
79-00-5
1.0
1
11/04/20 23:36
79-01-6
1.0
1
11/04/20 23:36
75-69-4
1.0
1
11/04/20 23:36
76-13-1
1.0
1
11/04/20 23:36
75-01-4
1.0
1
11/04/20 23:36
1330-20-7
70-130 1
70-130 1
70-130 1
40.0 20
70-130 20
66-133 20
5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
11/04/20 23:36 460-00-4
11/04/20 23:36 17060-07-0
11/04/20 23:36 2037-26-5
11 /04/20 21:13 123-91-1
11/04/20 21:13 17060-07-0
11/04/20 21:13 2037-26-5
11 /11 /20 20:52
Page 30 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-22A-110320
Lab ID: 92503658014 Collected:
11/03/20 08:00
Received: 11/03/20 17:24 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
11/03/20 23:51
14797-55-8
Nitrogen, Nitrite
0.11 mg/L
0.040
1
11/03/20 23:51
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
ND mg/L
0.25
5
11/04/20 08:40
D3,F6
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
11/06/20 02:41
14808-79-8
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
3.9 mg/L
1.0
1
11/16/20 12:46
7440-44-0
Total Organic Carbon
4.0 mg/L
1.0
1
11/16/20 12:46
7440-44-0
Total Organic Carbon
4.0 mg/L
1.0
1
11/16/20 12:46
7440-44-0
Total Organic Carbon
4.0 mg/L
1.0
1
11/16/20 12:46
7440-44-0
Mean Total Organic Carbon
4.0 mg/L
1.0
1
11/16/20 12:46
7440-44-0
Low Level Volatile Fatty Acids
Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid
6.1 mg/L
5.0
10
11/13/2011:35
64-19-7
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 31 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-2213-110320 Lab ID: 92503658015 Collected: 11/03/20 09:28 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2
Hydrogen
Indicator Gases Water LHC
Methane
Ethane
Ethene
EPA RSK-175
Carbon dioxide
8270E RVE
Biphenyl (Diphenyl)
Diphenyl ether (Phenyl ether)
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
8260D MSV Low Level Landfill
Acetone
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
Date: 11/19/2020 04:25 PM
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
ND nM
1.9
1
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
42000 ug/L
20
4
2.7 ug/L
1.0
1
ND ug/L
1.0
1
Analytical Method: RSK-175
Pace Analytical Gulf Coast
160000 ug/L
18000
20
Analytical Method: EPA 8270E Preparation
Method: EPA 3510C
Pace Analytical Services - Charlotte
11 /17/20 12:32 1333-74-0
11/17/20 03:02 74-82-8
11/15/2016:07 74-84-0
11/15/2016:07 74-85-1
11 /13/20 12:04 124-38-9
ND
ug/L
10.0
1
11/06/20 08:53
11/07/20 14:25
92-52-4
31.2
ug/L
10.0
1
11/06/20 08:53
11/07/20 14:25
101-84-8
46
%
10-144
1
11/06/20 08:53
11/07/20 14:25
4165-60-0
25
%
10-130
1
11/06/20 08:53
11/07/20 14:25
321-60-8
92
%
34-163
1
11/06/20 08:53
11/07/20 14:25
1718-51-0
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
25.0
1
11/04/20 23:54
67-64-1
ND
ug/L
1.0
1
11/04/20 23:54
71-43-2
ND
ug/L
1.0
1
11/04/20 23:54
74-97-5
ND
ug/L
1.0
1
11/04/20 23:54
75-27-4
ND
ug/L
1.0
1
11/04/20 23:54
75-25-2
ND
ug/L
2.0
1
11/04/20 23:54
74-83-9
ND
ug/L
5.0
1
11/04/20 23:54
78-93-3
ND
ug/L
2.0
1
11/04/20 23:54
75-15-0
ND
ug/L
1.0
1
11/04/20 23:54
56-23-5
10.4
ug/L
1.0
1
11/04/20 23:54
108-90-7
16.7
ug/L
1.0
1
11/04/20 23:54
75-00-3
ND
ug/L
5.0
1
11/04/20 23:54
67-66-3
ND
ug/L
1.0
1
11/04/20 23:54
74-87-3
ND
ug/L
1.0
1
11/04/20 23:54
110-82-7
ND
ug/L
5.0
1
11/04/20 23:54
96-12-8
ND
ug/L
1.0
1
11/04/20 23:54
124-48-1
ND
ug/L
1.0
1
11/04/20 23:54
106-93-4
ND
ug/L
1.0
1
11/04/20 23:54
95-50-1
ND
ug/L
1.0
1
11/04/20 23:54
541-73-1
ND
ug/L
1.0
1
11/04/20 23:54
106-46-7
ND
ug/L
1.0
1
11/04/20 23:54
75-71-8
ND
ug/L
1.0
1
11/04/20 23:54
75-34-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v2
v2
Page 32 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: 13-2213-110320 Lab ID: 92503658015 Collected: 11/03/20 09:28 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
Isopropylbenzene (Cumene)
Methyl acetate
Methylcyclohexane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
2320B Alkalinity
Alkalinity, Total as CaCO3
Date: 11/19/2020 04:25 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
100
%
101
%
100
%
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1350
ug/L
99
%
91
%
Analytical Method:
SM 2320B-2011
Pace Analytical
Services -Asheville
939
mg/L
1.0
1
11/04/20 23:54
107-06-2
1.0
1
11/04/20 23:54
75-35-4
1.0
1
11/04/20 23:54
156-59-2
1.0
1
11/04/20 23:54
156-60-5
1.0
1
11/04/20 23:54
78-87-5
1.0
1
11/04/20 23:54
10061-01-5
1.0
1
11/04/20 23:54
10061-02-6
1.0
1
11/04/20 23:54
100-41-4
5.0
1
11/04/20 23:54
591-78-6
1.0
1
11/04/20 23:54
98-82-8
10.0
1
11/04/20 23:54
79-20-9
10.0
1
11/04/20 23:54
108-87-2
5.0
1
11/04/20 23:54
75-09-2
5.0
1
11/04/20 23:54
108-10-1
1.0
1
11/04/20 23:54
1634-04-4
1.0
1
11/04/20 23:54
100-42-5
1.0
1
11/04/20 23:54
79-34-5
1.0
1
11/04/20 23:54
127-18-4
1.0
1
11/04/20 23:54
108-88-3
1.0
1
11/04/20 23:54
87-61-6
1.0
1
11/04/20 23:54
120-82-1
1.0
1
11/04/20 23:54
71-55-6
1.0
1
11/04/20 23:54
79-00-5
1.0
1
11/04/20 23:54
79-01-6
1.0
1
11/04/20 23:54
75-69-4
1.0
1
11/04/20 23:54
76-13-1
1.0
1
11/04/20 23:54
75-01-4
1.0
1
11/04/20 23:54
1330-20-7
70-130 1
70-130 1
70-130 1
40.0 20
70-130 20
66-133 20
5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
11/04/20 23:54 460-00-4
11/04/20 23:54 17060-07-0
11/04/20 23:54 2037-26-5
11 /04/20 21:32 123-91-1
11/04/20 21:32 17060-07-0
11/04/20 21:32 2037-26-5
11 /12/20 14:22
Page 33 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: 13-2213-110320
Lab ID: 92503658015 Collected:
11/03/20 09:28
Received: 11/03/20 17:24 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
11/03/20 23:52
14797-55-8
Nitrogen, Nitrite
0.049 mg/L
0.040
1
11/03/20 23:52
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.14 mg/L
0.050
1
11/04/20 08:41
F6
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
11/06/20 02:56
14808-79-8
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
6.3 mg/L
1.0
1
11/16/20 13:04
7440-44-0
Total Organic Carbon
6.0 mg/L
1.0
1
11/16/20 13:04
7440-44-0
Total Organic Carbon
6.1 mg/L
1.0
1
11/16/20 13:04
7440-44-0
Total Organic Carbon
6.0 mg/L
1.0
1
11/16/20 13:04
7440-44-0
Mean Total Organic Carbon
6.1 mg/L
1.0
1
11/16/20 13:04
7440-44-0
Low Level Volatile Fatty Acids
Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid
1.1 mg/L
1.0
2
11/13/2012:28
64-19-7
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 34 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-17C-110320 Lab ID: 92503658016 Collected: 11/03/20 10:44 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen
1.9 nM
1.9
1
11/17/2012:44
1333-74-0
Indicator Gases Water LHC
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Ethane
1.1 ug/L
1.0
1
11/15/2016:19
74-84-0
Ethene
ND ug/L
1.0
1
11/15/2016:19
74-85-1
Methane
96 ug/L
5.0
1
11/15/2016:19
74-82-8
EPA RSK-175
Analytical Method: RSK-175
Pace Analytical Gulf Coast
Carbon dioxide
89200 ug/L
18000
20
11/13/20 12:11
124-38-9
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
ND ug/L
10.0
1
11/06/20 08:53
11/07/20 14:53
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L
10.0
1
11/06/20 08:53
11/07/20 14:53
101-84-8
Surrogates
Nitrobenzene-d5(S)
39 %
10-144
1
11/06/20 08:53
11/07/20 14:53
4165-60-0
2-Fluorobiphenyl (S)
22 %
10-130
1
11/06/20 08:53
11/07/20 14:53
321-60-8
Terphenyl-d14 (S)
74 %
34-163
1
11/06/20 08:53
11/07/20 14:53
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
1640 ug/L
50.0
25
11/04/20 21:51
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
98 %
70-130
25
11/04/20 21:51
17060-07-0
Toluene-d8 (S)
91 %
66-133
25
11/04/20 21:51
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
417 mg/L
5.0
1
11/12/20 14:33
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
11/03/20 23:53
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
11/03/20 23:53
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.24 mg/L
0.050
1
11/04/20 08:42
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
1.2 mg/L
1.0
1
11/06/20 03:11
14808-79-8
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
F6
Page 35 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-17C-110320
Parameters
Lab ID: 92503658016 Collected: 11/03/20 10:44
Results Units Report Limit DF
Received: 11/03/20 17:24 Matrix: Water
Prepared Analyzed CAS No. Qual
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
3.2 mg/L
1.0
1
11/12/20 22:38
7440-44-0
Total Organic Carbon
3.3 mg/L
1.0
1
11/12/20 22:38
7440-44-0
Total Organic Carbon
3.2 mg/L
1.0
1
11/12/20 22:38
7440-44-0
Total Organic Carbon
3.2 mg/L
1.0
1
11/12/20 22:38
7440-44-0
Mean Total Organic Carbon
3.2 mg/L
1.0
1
11/12/20 22:38
7440-44-0
Low Level Volatile Fatty Acids
Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid
0.52 mg/L
0.50
1
11/13/2013:21
64-19-7
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 36 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: 13-1713-110320 Lab ID: 92503658017 Collected: 11/03/20 11:44 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen
ND nM
1.9
1
11/17/2012:56
1333-74-0
Indicator Gases Water LHC
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Ethane
ND ug/L
1.0
1
11/15/2016:30
74-84-0
Ethene
ND ug/L
1.0
1
11/15/2016:30
74-85-1
Methane
200 ug/L
5.0
1
11/15/2016:30
74-82-8
EPA RSK-175
Analytical Method: RSK-175
Pace Analytical Gulf Coast
Carbon dioxide
98100 ug/L
18000
20
11/13/20 12:19
124-38-9
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
ND ug/L
10.0
1
11/06/20 08:53
11/07/20 15:22
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L
10.0
1
11/06/20 08:53
11/07/20 15:22
101-84-8
Surrogates
Nitrobenzene-d5(S)
43 %
10-144
1
11/06/20 08:53
11/07/20 15:22
4165-60-0
2-Fluorobiphenyl (S)
25 %
10-130
1
11/06/20 08:53
11/07/20 15:22
321-60-8
Terphenyl-d14 (S)
86 %
34-163
1
11/06/20 08:53
11/07/20 15:22
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
78.6 ug/L
2.0
1
11/05/20 11:11
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
86 %
70-130
1
11/05/20 11:11
17060-07-0
Toluene-d8 (S)
91 %
66-133
1
11/05/20 11:11
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
217 mg/L
5.0
1
11/11/20 21:16
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
0.044 mg/L
0.040
1
11/03/20 23:55
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
11/03/20 23:55
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.22 mg/L
0.050
1
11/04/20 08:43
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
2.6 mg/L
1.0
1
11/06/20 03:26
14808-79-8
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
F6
Page 37 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: 13-1713-110320
Parameters
Lab ID: 92503658017 Collected: 11/03/20 11:44
Results Units Report Limit DF
Received: 11/03/20 17:24 Matrix: Water
Prepared Analyzed CAS No. Qual
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
1.8 mg/L
1.0
1
11/12/20 22:56
7440-44-0
Total Organic Carbon
1.6 mg/L
1.0
1
11/12/20 22:56
7440-44-0
Total Organic Carbon
1.5 mg/L
1.0
1
11/12/20 22:56
7440-44-0
Total Organic Carbon
1.6 mg/L
1.0
1
11/12/20 22:56
7440-44-0
Mean Total Organic Carbon
1.6 mg/L
1.0
1
11/12/20 22:56
7440-44-0
Low Level Volatile Fatty Acids
Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid
0.52 mg/L
0.50
1
11/13/2014:15
64-19-7
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 38 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-12-110320 Lab ID: 92503658018 Collected: 11/03/20 12:57 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E RVE
Biphenyl (Diphenyl)
Diphenyl ether (Phenyl ether)
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
2320B Alkalinity
Alkalinity, Total as CaCO3
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
9056 IC anions 28 Days
Sulfate
Date: 11/19/2020 04:25 PM
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND ug/L
10.0
1
11/06/20 08:53
11/07/20 15:51
92-52-4
ND ug/L
10.0
1
11/06/20 08:53
11/07/20 15:51
101-84-8
66 %
10-144
1
11/06/20 08:53
11/07/20 15:51
4165-60-0
46 %
10-130
1
11/06/20 08:53
11/07/20 15:51
321-60-8
92 %
34-163
1
11/06/20 08:53
11/07/20 15:51
1718-51-0
Analytical Method: EPA 8260D Mod
Pace Analytical Services - Charlotte
2400 ug/L
100
50
81 %
70-130
50
91 %
66-133
50
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
391 mg/L
5.0
1
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
ND mg/L
0.040
1
ND mg/L
0.040
1
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
0.25 mg/L
0.050
1
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
1.3 mg/L
1.0
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
11 /05/20 12:07 123-91-1
11 /05/20 12:07 17060-07-0
11 /05/20 12:07 2037-26-5
11 /12/20 14:42
11/03/20 23:56 14797-55-8
11/03/20 23:56 14797-65-0
11/04/20 08:43 F6
11/06/20 03:40 14808-79-8 M 1
Page 39 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: 13-3213-110320 Lab ID: 92503658019 Collected: 11/03/20 13:53 Received: 11/03/20 17:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2
Hydrogen
Indicator Gases Water LHC
Ethane
Ethene
Methane
8015M Glycols in water
Ethylene glycol
EPA RSK-175
Carbon dioxide
8270E RVE
Biphenyl (Diphenyl)
Diphenyl ether (Phenyl ether)
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
2320B Alkalinity
Alkalinity, Total as CaCO3
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
Date: 11/19/2020 04:25 PM
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
ND nM
1.9
1
11/17/2013:08
1333-74-0
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
ND ug/L
1.0
1
11/15/2016:43
74-84-0
ND ug/L
1.0
1
11/15/2016:43
74-85-1
3100 ug/L
5.0
1
11/15/2016:43
74-82-8
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
ND mg/L
5.0
1
11/10/20 20:26
107-21-1
Analytical Method: RSK-175
Pace Analytical Gulf Coast
37100 ug/L
18000
20
11 /13/20 12:26
124-38-9
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
ND ug/L
10.0
1
11/06/20 08:53
11/07/20 16:20
92-52-4
ND ug/L
10.0
1
11/06/20 08:53
11/07/20 16:20
101-84-8
45 %
10-144
1
11/06/20 08:53
11/07/20 16:20
4165-60-0
26 %
10-130
1
11/06/20 08:53
11/07/20 16:20
321-60-8
74 %
34-163
1
11/06/20 08:53
11/07/20 16:20
1718-51-0
Analytical Method: EPA 8260D Mod
Pace Analytical Services - Charlotte
3.4 ug/L
2.0
1
97 %
70-130
1
91 %
66-133
1
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
129 mg/L
5.0
1
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
0.068 mg/L
0.040
1
ND mg/L
0.040
1
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
ND mg/L
0.050
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
11 /04/20 18:00 123-91-1
11 /04/20 18:00 17060-07-0
11 /04/20 18:00 2037-26-5
11/11/20 21:46
11/03/20 23:57 14797-55-8
11/03/20 23:57 14797-65-0
11/04/20 08:44 F6
Page 40 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: 13-3213-110320
Lab ID: 92503658019 Collected:
11/03/20 13:53
Received: 11/03/20 17:24 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
11/06/20 04:25
14808-79-8
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
2.4 mg/L
1.0
1
11/12/20 23:13
7440-44-0
Total Organic Carbon
2.3 mg/L
1.0
1
11/12/20 23:13
7440-44-0
Total Organic Carbon
2.3 mg/L
1.0
1
11/12/20 23:13
7440-44-0
Total Organic Carbon
2.4 mg/L
1.0
1
11/12/20 23:13
7440-44-0
Mean Total Organic Carbon
2.4 mg/L
1.0
1
11/12/20 23:13
7440-44-0
Low Level Volatile Fatty Acids
Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid
1.0 mg/L
1.0
2
11/13/2015:08
64-19-7
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 41 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-01-110320 Lab ID: 92503658020 Collected: 11/03/20 15:14 Received: 11/04/20 12:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen
ND nM
1.9
1
11/17/2011:23
1333-74-0
Indicator Gases Water LHC
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Ethane
ND ug/L
1.0
1
11/11/20 23:43
74-84-0
Methane
35000 ug/L
20
4
11/12/20 20:07
74-82-8
Ethene
ND ug/L
1.0
1
11/11/20 23:43
74-85-1
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L
5.0
1
11/10/20 20:50
107-21-1
EPA RSK-175
Analytical Method: RSK-175
Pace Analytical Gulf Coast
Carbon dioxide
293000 ug/L
45000
50
11/13/20 11:46
124-38-9
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
ND ug/L
10.0
1
11/06/20 08:53
11/07/20 16:49
92-52-4
Diphenyl ether (Phenyl ether)
30.0 ug/L
10.0
1
11/06/20 08:53
11/07/20 16:49
101-84-8
Surrogates
Nitrobenzene-d5 (S)
41 %
10-144
1
11/06/20 08:53
11/07/20 16:49
4165-60-0
2-Fluorobiphenyl (S)
23 %
10-130
1
11/06/20 08:53
11/07/20 16:49
321-60-8
Terphenyl-d14 (S)
67 %
34-163
1
11/06/20 08:53
11/07/20 16:49
1718-51-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
635 ug/L
62.5
2.5
11/06/20 14:51
67-64-1
Benzene
ND ug/L
2.5
2.5
11/06/20 14:51
71-43-2
Bromochloromethane
ND ug/L
2.5
2.5
11/06/20 14:51
74-97-5
Bromodichloromethane
ND ug/L
2.5
2.5
11/06/20 14:51
75-27-4
Bromoform
ND ug/L
2.5
2.5
11/06/20 14:51
75-25-2
Bromomethane
ND ug/L
5.0
2.5
11/06/20 14:51
74-83-9
2-Butanone (MEK)
371 ug/L
12.5
2.5
11/06/20 14:51
78-93-3
Carbon disulfide
ND ug/L
5.0
2.5
11/06/20 14:51
75-15-0
Carbon tetrachloride
ND ug/L
2.5
2.5
11/06/20 14:51
56-23-5
Chlorobenzene
ND ug/L
2.5
2.5
11/06/20 14:51
108-90-7
Chloroethane
19.2 ug/L
2.5
2.5
11/06/20 14:51
75-00-3
Chloroform
ND ug/L
12.5
2.5
11/06/20 14:51
67-66-3
Chloromethane
ND ug/L
2.5
2.5
11/06/20 14:51
74-87-3
Cyclohexane
ND ug/L
2.5
2.5
11/06/20 14:51
110-82-7
1,2-Dibromo-3-chloropropane
ND ug/L
12.5
2.5
11/06/20 14:51
96-12-8
Dibromochloromethane
ND ug/L
2.5
2.5
11/06/20 14:51
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
2.5
2.5
11/06/20 14:51
106-93-4
1,2-Dichlorobenzene
ND ug/L
2.5
2.5
11/06/20 14:51
95-50-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
v2
Page 42 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-01-110320 Lab ID: 92503658020 Collected: 11/03/20 15:14 Received: 11/04/20 12:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,3-Dichlorobenzene
ND
ug/L
2.5
2.5
11/06/20 14:51
541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.5
2.5
11/06/20 14:51
106-46-7
Dichlorodifluoromethane
ND
ug/L
2.5
2.5
11/06/20 14:51
75-71-8
1,1-Dichloroethane
15.8
ug/L
2.5
2.5
11/06/20 14:51
75-34-3
1,2-Dichloroethane
ND
ug/L
2.5
2.5
11/06/20 14:51
107-06-2
1,1-Dichloroethene
ND
ug/L
2.5
2.5
11/06/20 14:51
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
2.5
2.5
11/06/20 14:51
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
2.5
2.5
11/06/20 14:51
156-60-5
1,2-Dichloropropene
ND
ug/L
2.5
2.5
11/06/20 14:51
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
2.5
2.5
11/06/20 14:51
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
2.5
2.5
11/06/20 14:51
10061-02-6
Ethylbenzene
ND
ug/L
2.5
2.5
11/06/20 14:51
100-41-4
2-Hexanone
ND
ug/L
12.5
2.5
11/06/20 14:51
591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
2.5
2.5
11/06/20 14:51
98-82-8
Methyl acetate
ND
ug/L
25.0
2.5
11/06/20 14:51
79-20-9
Methylcyclohexane
ND
ug/L
25.0
2.5
11/06/20 14:51
108-87-2
Methylene Chloride
ND
ug/L
12.5
2.5
11/06/20 14:51
75-09-2
4-Methyl-2-pentanone (MIBK)
24.8
ug/L
12.5
2.5
11/06/20 14:51
108-10-1
Methyl-tert-butyl ether
ND
ug/L
2.5
2.5
11/06/20 14:51
1634-04-4
Styrene
ND
ug/L
2.5
2.5
11/06/20 14:51
100-42-5
1,1,2,2-Tetrachloroethane
ND
ug/L
2.5
2.5
11/06/20 14:51
79-34-5
Tetrachloroethene
ND
ug/L
2.5
2.5
11/06/20 14:51
127-18-4
Toluene
4.1
ug/L
2.5
2.5
11/06/20 14:51
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.5
2.5
11/06/20 14:51
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.5
2.5
11/06/20 14:51
120-82-1
1,1,1-Trichloroethane
ND
ug/L
2.5
2.5
11/06/20 14:51
71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.5
2.5
11/06/20 14:51
79-00-5
Trichloroethene
ND
ug/L
2.5
2.5
11/06/20 14:51
79-01-6
Trichlorofluoromethane
ND
ug/L
2.5
2.5
11/06/20 14:51
75-69-4
1,1,2-Trichlorotrifluoroethane
ND
ug/L
2.5
2.5
11/06/20 14:51
76-13-1
Vinyl chloride
ND
ug/L
2.5
2.5
11/06/20 14:51
75-01-4
Xylene (Total)
ND
ug/L
2.5
2.5
11/06/20 14:51
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
2.5
11/06/20 14:51
460-00-4
1,2-Dichloroethane-d4 (S)
94
%
70-130
2.5
11/06/20 14:51
17060-07-0
Toluene-d8 (S)
96
%
70-130
2.5
11/06/20 14:51
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
1510
ug/L
50.0
25
11/06/20 01:36
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
81
%
70-130
25
11/06/20 01:36
17060-07-0
Toluene-d8(S)
97
%
66-133
25
11/06/20 01:36
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-01-110320
Lab ID: 92503658020 Collected:
11/03/20 15:14
Received: 11/04/20 12:35 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
1380 mg/L
5.0
1
11/11/20 23:21
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
11/05/20 11:59
14797-55-8
Nitrogen, Nitrite
0.22 mg/L
0.040
1
11/05/20 11:59
14797-65-0 M1
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
ND mg/L
0.25
5
11/05/20 11:52
D3,F6
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
9.2 mg/L
1.0
1
11/07/20 04:18
14808-79-8
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
884 mg/L
25.0
25
11/12/20 23:30
7440-44-0
Total Organic Carbon
900 mg/L
25.0
25
11/12/20 23:30
7440-44-0
Total Organic Carbon
914 mg/L
25.0
25
11/12/20 23:30
7440-44-0
Total Organic Carbon
908 mg/L
25.0
25
11/12/20 23:30
7440-44-0
Mean Total Organic Carbon
901 mg/L
25.0
25
11/12/20 23:30
7440-44-0
Low Level Volatile Fatty Acids
Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid
ND mg/L
5.0
10
11/13/20 05:21
64-19-7
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 44 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-10-110320 Lab ID: 92503658021 Collected: 11/03/20 16:41 Received: 11/04/20 12:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Indicator Gases Bubblestrip H2
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Hydrogen
ND nM
1.9
1
11/17/2011:35
1333-74-0
Indicator Gases Water LHC
Analytical Method: AM20GAX
Pace Analytical Gulf Coast
Methane
35000 ug/L
20
4
11/12/20 20:19
74-82-8
Ethane
ND ug/L
1.0
1
11/11/20 23:55
74-84-0
Ethene
ND ug/L
1.0
1
11/11/20 23:55
74-85-1
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L
5.0
1
11/08/20 13:27
107-21-1
EPA RSK-175
Analytical Method: RSK-175
Pace Analytical Gulf Coast
Carbon dioxide
195000 ug/L
45000
50
11/13/20 11:51
124-38-9
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
69.4 ug/L
10.0
1
11/06/20 08:53
11/07/20 17:18
92-52-4
Diphenyl ether (Phenyl ether)
698 ug/L
100
10
11/06/20 08:53
11/09/20 18:23
101-84-8
Surrogates
Nitrobenzene-d5 (S)
38 %
10-144
1
11/06/20 08:53
11/07/20 17:18
4165-60-0
2-Fluorobiphenyl (S)
17 %
10-130
1
11/06/20 08:53
11/07/20 17:18
321-60-8
Terphenyl-d14 (S)
87 %
34-163
1
11/06/20 08:53
11/07/20 17:18
1718-51-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND ug/L
25.0
1
11/06/20 12:14
67-64-1
Benzene
ND ug/L
1.0
1
11/06/20 12:14
71-43-2
Bromochloromethane
ND ug/L
1.0
1
11/06/20 12:14
74-97-5
Bromodichloromethane
ND ug/L
1.0
1
11/06/20 12:14
75-27-4
Bromoform
ND ug/L
1.0
1
11/06/20 12:14
75-25-2
Bromomethane
ND ug/L
2.0
1
11/06/20 12:14
74-83-9
2-Butanone (MEK)
ND ug/L
5.0
1
11/06/20 12:14
78-93-3
Carbon disulfide
ND ug/L
2.0
1
11/06/20 12:14
75-15-0
Carbon tetrachloride
ND ug/L
1.0
1
11/06/20 12:14
56-23-5
Chlorobenzene
ND ug/L
1.0
1
11/06/20 12:14
108-90-7
Chloroethane
52.6 ug/L
1.0
1
11/06/20 12:14
75-00-3
Chloroform
ND ug/L
5.0
1
11/06/20 12:14
67-66-3
Chloromethane
ND ug/L
1.0
1
11/06/20 12:14
74-87-3
Cyclohexane
ND ug/L
1.0
1
11/06/20 12:14
110-82-7
1,2-Dibromo-3-chloropropane
ND ug/L
5.0
1
11/06/20 12:14
96-12-8
Dibromochloromethane
ND ug/L
1.0
1
11/06/20 12:14
124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
1
11/06/20 12:14
106-93-4
1,2-Dichlorobenzene
ND ug/L
1.0
1
11/06/20 12:14
95-50-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
v2
Page 45 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-10-110320 Lab ID: 92503658021 Collected: 11/03/20 16:41 Received: 11/04/20 12:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,3-Dichlorobenzene
ND
ug/L
1.0
1
11/06/20 12:14
541-73-1
1,4-Dichlorobenzene
5.0
ug/L
1.0
1
11/06/20 12:14
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
1
11/06/20 12:14
75-71-8
1,1-Dichloroethane
21.6
ug/L
1.0
1
11/06/20 12:14
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
11/06/20 12:14
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
11/06/20 12:14
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
11/06/20 12:14
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
11/06/20 12:14
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
11/06/20 12:14
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
11/06/20 12:14
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
11/06/20 12:14
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
11/06/20 12:14
100-41-4
2-Hexanone
ND
ug/L
5.0
1
11/06/20 12:14
591-78-6
Isopropylbenzene (Cumene)
ND
ug/L
1.0
1
11/06/20 12:14
98-82-8
Methyl acetate
ND
ug/L
10.0
1
11/06/20 12:14
79-20-9
Methylcyclohexane
ND
ug/L
10.0
1
11/06/20 12:14
108-87-2
Methylene Chloride
ND
ug/L
5.0
1
11/06/20 12:14
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
11/06/20 12:14
108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
1
11/06/20 12:14
1634-04-4
Styrene
ND
ug/L
1.0
1
11/06/20 12:14
100-42-5
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
11/06/20 12:14
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
11/06/20 12:14
127-18-4
Toluene
ND
ug/L
1.0
1
11/06/20 12:14
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
1.0
1
11/06/20 12:14
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
1.0
1
11/06/20 12:14
120-82-1
1,1,1-Trichloroethane
ND
ug/L
1.0
1
11/06/20 12:14
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
11/06/20 12:14
79-00-5
Trichloroethene
ND
ug/L
1.0
1
11/06/20 12:14
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
11/06/20 12:14
75-69-4
1,1,2-Trichlorotrifluoroethane
ND
ug/L
1.0
1
11/06/20 12:14
76-13-1
Vinyl chloride
1.9
ug/L
1.0
1
11/06/20 12:14
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
11/06/20 12:14
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
11/06/20 12:14
460-00-4
1,2-Dichloroethane-d4 (S)
108
%
70-130
1
11/06/20 12:14
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
11/06/20 12:14
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
Pace Analytical
Services - Charlotte
1,4-Dioxane (p-Dioxane)
197
ug/L
10.0
5
11/06/20 01:17
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
86
%
70-130
5
11/06/20 01:17
17060-07-0
Toluene-d8 (S)
86
%
66-133
5
11/06/20 01:17
2037-26-5
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 46 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92503658
Sample: B-10-110320
Lab ID: 92503658021 Collected:
11/03/20 16:41
Received: 11/04/20 12:35 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
504 mg/L
5.0
1
11/12/20 00:06
M1
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
11/05/20 12:04
14797-55-8
Nitrogen, Nitrite
0.057 mg/L
0.040
1
11/05/20 12:04
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.32 mg/L
0.25
5
11/05/20 11:53
F6
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
11/07/20 05:02
14808-79-8
Total Organic Carbon,Asheville
Analytical Method: EPA 9060A
Pace Analytical Services -Asheville
Total Organic Carbon
20.4 mg/L
1.0
1
11/12/20 23:49
7440-44-0
Total Organic Carbon
20.7 mg/L
1.0
1
11/12/20 23:49
7440-44-0
Total Organic Carbon
20.7 mg/L
1.0
1
11/12/20 23:49
7440-44-0
Total Organic Carbon
21.0 mg/L
1.0
1
11/12/20 23:49
7440-44-0
Mean Total Organic Carbon
20.7 mg/L
1.0
1
11/12/20 23:49
7440-44-0
Low Level Volatile Fatty Acids
Analytical Method: AM23G
Pace Analytical Gulf Coast
Acetic Acid
1.6 mg/L
1.0
2
11/13/20 06:14
64-19-7
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 47 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 697515 Analysis Method: AM20GAX
QC Batch Method: AM20GAX Analysis Description: Indicator Gases Bubble Strip H2
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92503658001, 92503658002, 92503658014, 92503658015, 92503658016, 92503658017, 92503658019,
92503658020,92503658021
METHOD BLANK: 2112018 Matrix: Air
Associated Lab Samples: 92503658001, 92503658002, 92503658014, 92503658015, 92503658016, 92503658017, 92503658019,
92503658020,92503658021
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Hydrogen nM ND 1.9 11/17/2011:10
LABORATORY CONTROL SAMPLE & LCSD: 2112019 2112020
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Hydrogen nM 12 11 12 97 100 70-130 3 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 48 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 697069 Analysis Method: AM20GAX
QC Batch Method: AM20GAX Analysis Description: Indicator Gases Water LHC
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92503658020, 92503658021
METHOD BLANK: 2109860
Associated Lab Samples: 92503658020, 92503658021
Parameter Units
Ethane ug/L
Ethene ug/L
Methane ug/L
Matrix: Water
Blank Reporting
Result Limit Analyzed
ND 1.0 11/11/20 20:07
ND 1.0 11/11/20 20:07
5.7 5.0 11/11/20 20:07
Qualifiers
LABORATORY CONTROL SAMPLE & LCSD:
2109861
2109862
Spike
LCS
LCSD
LCS LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec % Rec
Limits RPD RPD Qualifiers
Ethane
ug/L
100
100
120
100 120
70-130 18 20
Ethene
ug/L
140
140
160
100 115
70-130 14 20
Methane
ug/L
490
480
560
98 114
70-130 15 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 49 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Project: NRLF
Pace Project No.: 92503658
QC Batch: 697207
QC Batch Method: AM20GAX
Associated Lab Samples: 92503658020, 92503658021
METHOD BLANK: 2110643
Associated Lab Samples: 92503658020, 92503658021
Parameter Units
Methane ug/L
QUALITY CONTROL DATA
Analysis Method: AM20GAX
Analysis Description: Indicator Gases Water LHC
Laboratory: Pace Analytical Gulf Coast
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 11/12/2018:17 BO
LABORATORY CONTROL SAMPLE & LCSD: 2110644 2110645
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Methane ug/L 490 480 400 98 82 70-130 17 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 50 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 697358 Analysis Method: AM20GAX
QC Batch Method: AM20GAX Analysis Description: Indicator Gases Water LHC
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92503658001, 92503658002, 92503658014, 92503658015, 92503658016, 92503658017, 92503658019
METHOD BLANK: 2111532
Matrix: Water
Associated Lab Samples:
92503658001, 92503658002, 92503658014, 92503658015, 92503658016,
92503658017, 92503658019
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Ethane
ug/L
ND 1.0
11/15/2011:23
Ethene
ug/L
ND 1.0
11/15/2011:23
Methane
ug/L
ND 5.0
11/15/2011:23
LABORATORY CONTROL SAMPLE & LCSD:
2111533
2111534
Spike
LCS LCSD
LCS LCSD
% Rec Max
Parameter
Units
Conc.
Result Result
% Rec % Rec
Limits RPD RPD Qualifiers
Ethane
ug/L
100
110 120
109 124
70-130 13 20
Ethene
ug/L
140
150 170
108 121
70-130 12 20
Methane
ug/L
490
470 530
96 107
70-130 12 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 51 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 697477 Analysis Method: AM20GAX
QC Batch Method: AM20GAX Analysis Description: Indicator Gases Water LHC
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92503658015
METHOD BLANK: 2111917
Associated Lab Samples: 92503658015
Parameter Units
Methane ug/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 11 /16/20 23:37
LABORATORY CONTROL SAMPLE & LCSD: 2111918 2111919
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Methane ug/L 490 400 500 82 103 70-130 22 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 52 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 591658 Analysis Method: EPA 8015 Alcohol -Glycol
QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified
Laboratory: Pace Analytical Services - Indianapolis
Associated Lab Samples: 92503658001, 92503658002, 92503658006, 92503658021
METHOD BLANK: 2730118
Matrix:
Water
Associated Lab Samples: 92503658001, 92503658002, 92503658006, 92503658021
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Ethylene glycol
mg/L
ND
5.0
11/08/20 10:07
LABORATORY CONTROL SAMPLE:
2730119
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Ethylene glycol
mg/L
25
12.2
49 47-167
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2730120 2730121
MS MSD
5254917001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Ethylene glycol mg/L ND 25 25 46.6 30.9 179 117 31-179 41 R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 53 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 591908 Analysis Method: EPA 8015 Alcohol -Glycol
QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified
Laboratory: Pace Analytical Services - Indianapolis
Associated Lab Samples: 92503658008, 92503658009, 92503658010
METHOD BLANK: 2730886
Matrix:
Water
Associated Lab Samples: 92503658008, 92503658009, 92503658010
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Ethylene glycol
mg/L
ND
5.0
11/09/20 18:22
LABORATORY CONTROL SAMPLE:
2730887
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Ethylene glycol
mg/L
25
25.5
102 47-167
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2730942 2730943
MS MSD
92504020007 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Ethylene glycol mg/L <5.0 25 25 23.9 29.6 93 115 31-179 21 R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 54 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 592184 Analysis Method: EPA 8015 Alcohol -Glycol
QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified
Laboratory: Pace Analytical Services - Indianapolis
Associated Lab Samples: 92503658011, 92503658019, 92503658020
METHOD BLANK: 2732066
Matrix:
Water
Associated Lab Samples: 92503658011, 92503658019,
92503658020
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Ethylene glycol
mg/L
ND
5.0
11/10/20 18:13
LABORATORY CONTROL SAMPLE:
2732067
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Ethylene glycol
mg/L
25
16.2
65 47-167
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2732068 2732069
MS MSD
92503658011 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Ethylene glycol mg/L ND 25 25 25.2 22.7 97 87 31-179 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 55 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 697027 Analysis Method: RSK-175
QC Batch Method: RSK-175 Analysis Description: EPA RSK 175
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples:
METHOD BLANK: 2109603 Matrix: Water
Associated Lab Samples: 92503658001, 92503658002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Carbon dioxide ug/L ND 900 11/11/20 12:55
LABORATORY CONTROL SAMPLE & LCSD: 2109604 2109605
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Carbon dioxide ug/L 8700 8380 8680 96 100 38-147 4 40
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 56 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 697246 Analysis Method: RSK-175
QC Batch Method: RSK-175 Analysis Description: EPA RSK 175
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples:
METHOD BLANK: 2110789 Matrix: Water
Associated Lab Samples: 92503658014, 92503658015, 92503658016, 92503658017, 92503658019, 92503658020, 92503658021
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Carbon dioxide ug/L ND 900 11/13/20 08:59
LABORATORY CONTROL SAMPLE & LCSD: 2110790 2110791
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Carbon dioxide ug/L 8700 8290 8490 95 98 38-147 2 40
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 57 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 577974 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92503658003
METHOD BLANK: 3057780
Associated Lab Samples: 92503658003
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1-Trichloroethane
ug/L
ND
1.0
11/04/20 16:52
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
11/04/20 16:52
1,1,2-Trichloroethane
ug/L
ND
1.0
11/04/20 16:52
1,1,2-Trichlorotrifluoroethane
ug/L
ND
1.0
11/04/20 16:52
1,1-Dichloroethane
ug/L
ND
1.0
11/04/20 16:52
1,1-Dichloroethene
ug/L
ND
1.0
11/04/20 16:52
1,2,3-Trichlorobenzene
ug/L
ND
1.0
11/04/20 16:52
1,2,4-Trichlorobenzene
ug/L
ND
1.0
11/04/20 16:52
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
11/04/20 16:52
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
11/04/20 16:52
1,2-Dichlorobenzene
ug/L
ND
1.0
11/04/20 16:52
1,2-Dichloroethane
ug/L
ND
1.0
11/04/20 16:52
1,2-Dichloropropane
ug/L
ND
1.0
11/04/20 16:52
1,3-Dichlorobenzene
ug/L
ND
1.0
11/04/20 16:52
1,4-Dichlorobenzene
ug/L
ND
1.0
11/04/20 16:52
2-Butanone (MEK)
ug/L
ND
5.0
11/04/20 16:52
2-Hexanone
ug/L
ND
5.0
11/04/20 16:52
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
11/04/20 16:52
Acetone
ug/L
ND
25.0
11/04/20 16:52
Benzene
ug/L
ND
1.0
11/04/20 16:52
Bromochloromethane
ug/L
ND
1.0
11/04/20 16:52
Bromodichloromethane
ug/L
ND
1.0
11/04/20 16:52
Bromoform
ug/L
ND
1.0
11/04/20 16:52
Bromomethane
ug/L
ND
2.0
11/04/20 16:52
Carbon disulfide
ug/L
ND
2.0
11/04/20 16:52
Carbon tetrachloride
ug/L
ND
1.0
11/04/20 16:52
Chlorobenzene
ug/L
ND
1.0
11/04/20 16:52
Chloroethane
ug/L
ND
1.0
11/04/20 16:52
Chloroform
ug/L
ND
5.0
11/04/20 16:52
Chloromethane
ug/L
ND
1.0
11/04/20 16:52
cis-1,2-Dichloroethene
ug/L
ND
1.0
11/04/20 16:52
cis-1,3-Dichloropropene
ug/L
ND
1.0
11/04/20 16:52
Cyclohexane
ug/L
ND
1.0
11/04/20 16:52
Dibromochloromethane
ug/L
ND
1.0
11/04/20 16:52
Dichlorodifluoromethane
ug/L
ND
1.0
11/04/20 16:52
Ethylbenzene
ug/L
ND
1.0
11/04/20 16:52
Isopropylbenzene (Cumene)
ug/L
ND
1.0
11/04/20 16:52
Methyl acetate
ug/L
ND
10.0
11/04/20 16:52
Methyl-tert-butyl ether
ug/L
ND
1.0
11/04/20 16:52
Methylcyclohexane
ug/L
ND
10.0
11/04/20 16:52
v2
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC. Page 58 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
METHOD BLANK: 3057780
Associated Lab Samples: 92503658003
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed Qualifiers
Methylene Chloride
ug/L
ND
5.0
11/04/20 16:52
Styrene
ug/L
ND
1.0
11/04/20 16:52
Tetrachloroethene
ug/L
ND
1.0
11/04/20 16:52
Toluene
ug/L
ND
1.0
11/04/20 16:52
trans-1,2-Dichloroethene
ug/L
ND
1.0
11/04/20 16:52
trans- 1,3-Dichloropropene
ug/L
ND
1.0
11/04/20 16:52
Trichloroethene
ug/L
ND
1.0
11/04/20 16:52
Trichlorofluoromethane
ug/L
ND
1.0
11/04/20 16:52
Vinyl chloride
ug/L
ND
1.0
11/04/20 16:52
Xylene (Total)
ug/L
ND
1.0
11/04/20 16:52
1,2-Dichloroethane-d4 (S)
%
94
70-130
11/04/20 16:52
4-Bromofluorobenzene (S)
%
98
70-130
11/04/20 16:52
Toluene-d8 (S)
%
101
70-130
11/04/20 16:52
LABORATORY CONTROL SAMPLE:
Parameter
3057781
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1-Trichloroethane
ug/L
50
47.6
95
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
52.3
105
70-130
1,1,2-Trichloroethane
ug/L
50
52.5
105
70-130
1,1,2-Trichlorotrifluoroethane
ug/L
50
53.1
106
70-130
1,1-Dichloroethane
ug/L
50
49.6
99
70-130
1,1-Dichloroethene
ug/L
50
51.3
103
70-132
1,2,3-Trichlorobenzene
ug/L
50
51.5
103
70-134
1,2,4-Trichlorobenzene
ug/L
50
52.0
104
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
53.7
107
70-132
1,2-Dibromoethane (EDB)
ug/L
50
51.0
102
70-130
1,2-Dichlorobenzene
ug/L
50
51.3
103
70-130
1,2-Dichloroethane
ug/L
50
46.1
92
70-130
1,2-Dichloropropane
ug/L
50
51.1
102
70-130
1,3-Dichlorobenzene
ug/L
50
51.7
103
70-130
1,4-Dichlorobenzene
ug/L
50
51.3
103
70-130
2-Butanone (MEK)
ug/L
100
102
102
70-133
2-Hexanone
ug/L
100
104
104
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
102
102
70-130
Acetone
ug/L
100
113
113
70-144
Benzene
ug/L
50
50.9
102
70-130
Bromochloromethane
ug/L
50
48.1
96
70-130
Bromodichloromethane
ug/L
50
48.4
97
70-130
Bromoform
ug/L
50
49.8
100
70-131
Bromomethane
ug/L
50
32.9
66
30-177 v3
Carbon disulfide
ug/L
50
52.8
106
70-133
Carbon tetrachloride
ug/L
50
49.9
100
70-130
Chlorobenzene
ug/L
50
51.5
103
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC. Page 59 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
LABORATORY CONTROL SAMPLE:
Parameter
3057781
Units
Spike
Conc.
LCS LCS
Result % Rec
Chloroethane
ug/L
50
39.6
Chloroform
ug/L
50
46.5
Chloromethane
ug/L
50
44.5
cis-1,2-Dichloroethene
ug/L
50
48.8
cis-1,3-Dichloropropene
ug/L
50
52.6
Cyclohexane
ug/L
50
49.7
Dibromochloromethane
ug/L
50
51.4
Dichlorodifluoromethane
ug/L
50
47.2
Ethylbenzene
ug/L
50
50.9
Isopropylbenzene (Cumene)
ug/L
50
50.8
Methyl acetate
ug/L
50
53.2
Methyl-tert-butyl ether
ug/L
50
49.4
Methylcyclohexane
ug/L
50
49.9
Methylene Chloride
ug/L
50
47.7
Styrene
ug/L
50
50.7
Tetrachloroethene
ug/L
50
49.7
Toluene
ug/L
50
51.8
trans-1,2-Dichloroethene
ug/L
50
51.1
trans- 1,3-Dichloropropene
ug/L
50
51.4
Trichloroethene
ug/L
50
51.2
Trichlorofluoromethane
ug/L
50
40.5
Vinyl chloride
ug/L
50
46.7
Xylene (Total)
ug/L
150
153
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
% Rec
Limits Qualifiers
79
46-131 v3
93
70-130
89
49-130
98
70-130
105
70-130
99
70-131
103
70-130
94
52-134
102
70-130
102
70-130
106
70-131
99
70-130
100
70-130
95
68-130
101
70-130
99
70-130
104
70-130
102
70-130
103
70-130
102
70-130
81
61-130
93
59-142
102
70-130
89
70-130
101
70-130
100
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3057782
MS
92503436014 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3057783
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1-Trichloroethane
ug/L
ND
20
20
22.4
23.1
112
115
70-148
3
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.1
23.4
110
117
70-131
6
1,1,2-Trichloroethane
ug/L
ND
20
20
22.5
23.2
112
116
70-136
3
1,1,2-Trichlorotrifluoroethane
ug/L
ND
20
20
23.1
23.6
116
118
70-154
2
1,1-Dichloroethane
ug/L
ND
20
20
22.4
23.1
112
116
70-147
3
1,1-Dichloroethene
ug/L
ND
20
20
24.6
25.6
123
128
70-158
4
1,2,3-Trichlorobenzene
ug/L
ND
20
20
21.6
23.0
108
115
68-140
6
1,2,4-Trichlorobenzene
ug/L
ND
20
20
22.1
23.8
110
119
70-139
8
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
20.9
22.8
105
114
69-136
8
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.0
23.7
110
118
70-137
7
1,2-Dichlorobenzene
ug/L
ND
20
20
23.3
24.1
116
121
70-133
3
1,2-Dichloroethane
ug/L
ND
20
20
20.0
20.8
100
104
67-138
4
1,2-Dichloropropane
ug/L
ND
20
20
23.1
24.2
115
121
70-138
5
1,3-Dichlorobenzene
ug/L
ND
20
20
22.9
25.1
115
126
70-133
9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 60 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3057782
3057783
MS
MSD
92503436014
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,4-Dichlorobenzene
ug/L
ND
20
20
23.2
24.4
116
122
70-133
5
2-Butanone (MEK)
ug/L
ND
40
40
37.7
38.9
94
97
61-147
3
2-Hexanone
ug/L
ND
40
40
43.5
45.0
109
113
67-139
3
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
41.7
43.2
104
108
67-136
4
Acetone
ug/L
ND
40
40
40.4
40.9
101
102
55-159
1
Benzene
ug/L
ND
20
20
22.9
24.0
114
120
67-150
5
Bromochloromethane
ug/L
ND
20
20
21.9
22.6
109
113
70-146
3
Bromodichloromethane
ug/L
ND
20
20
21.4
22.3
107
112
70-138
4
Bromoform
ug/L
ND
20
20
19.8
21.1
99
105
57-138
6
Bromomethane
ug/L
ND
20
20
13.6
16.0
68
80
10-200
16 v3
Carbon disulfide
ug/L
ND
20
20
23.9
25.4
119
127
70-152
6
Carbon tetrachloride
ug/L
ND
20
20
24.5
25.0
122
125
70-147
2
Chlorobenzene
ug/L
ND
20
20
24.7
26.0
124
130
70-137
5
Chloroethane
ug/L
ND
20
20
21.9
22.1
109
111
51-166
1
Chloroform
ug/L
ND
20
20
20.8
21.1
104
105
70-144
1
Chloromethane
ug/L
ND
20
20
16.5
16.2
82
81
24-161
2
cis-1,2-Dichloroethene
ug/L
ND
20
20
21.0
22.0
105
110
67-148
5
cis-1,3-Dichloropropene
ug/L
ND
20
20
22.6
23.8
113
119
70-142
5
Cyclohexane
ug/L
ND
20
20
25.2
25.7
126
128
70-151
2
Dibromochloromethane
ug/L
ND
20
20
21.9
23.6
110
118
68-138
7
Dichlorodifluoromethane
ug/L
ND
20
20
19.5
19.9
98
100
43-155
2
Ethylbenzene
ug/L
ND
20
20
24.7
25.6
124
128
68-143
3
Isopropylbenzene (Cumene)
ug/L
ND
20
20
24.5
26.0
122
130
70-136
6
Methyl acetate
ug/L
ND
20
20
19.9
19.9
99
100
55-149
0
Methyl-tert-butyl ether
ug/L
0.41 J
20
20
20.4
21.0
100
103
59-156
3
Methylcyclohexane
ug/L
ND
20
20
23.0
24.0
115
120
70-142
4
Methylene Chloride
ug/L
ND
20
20
20.0
20.7
100
103
64-148
3
Styrene
ug/L
ND
20
20
24.1
25.1
120
126
70-136
4
Tetrachloroethene
ug/L
ND
20
20
21.6
22.9
108
114
70-139
6
Toluene
ug/L
ND
20
20
23.6
24.5
118
122
47-157
4
trans-1,2-Dichloroethene
ug/L
ND
20
20
22.6
23.5
113
118
70-149
4
trans- 1,3-Dichloropropene
ug/L
ND
20
20
21.5
21.9
108
109
70-138
2
Trichloroethene
ug/L
ND
20
20
25.0
25.4
125
127
70-149
1
Trichlorofluoromethane
ug/L
ND
20
20
21.5
21.8
108
109
61-154
2
Vinyl chloride
ug/L
ND
20
20
19.9
20.3
100
102
55-172
2
Xylene (Total)
ug/L
ND
60
60
73.8
76.7
123
128
66-145
4
1,2-Dichloroethane-d4 (S)
%
89
90
70-130
4-Bromofluorobenzene (S)
%
100
101
70-130
Toluene-d8(S)
%
98
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 61 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 577978 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92503658001, 92503658002, 92503658004, 92503658006, 92503658007, 92503658014, 92503658015
METHOD BLANK: 3057787 Matrix: Water
Associated Lab Samples: 92503658001, 92503658002, 92503658004, 92503658006, 92503658007, 92503658014, 92503658015
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1-Trichloroethane
ug/L
ND
1.0
11/04/20 16:34
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
11/04/20 16:34
1,1,2-Trichloroethane
ug/L
ND
1.0
11/04/20 16:34
1,1,2-Trichlorotrifluoroethane
ug/L
ND
1.0
11/04/20 16:34
1,1-Dichloroethane
ug/L
ND
1.0
11/04/20 16:34
1,1-Dichloroethene
ug/L
ND
1.0
11/04/20 16:34
1,2,3-Trichlorobenzene
ug/L
ND
1.0
11/04/20 16:34
1,2,4-Trichlorobenzene
ug/L
ND
1.0
11/04/20 16:34
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
11/04/20 16:34
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
11/04/20 16:34
1,2-Dichlorobenzene
ug/L
ND
1.0
11/04/20 16:34
1,2-Dichloroethane
ug/L
ND
1.0
11/04/20 16:34
1,2-Dichloropropane
ug/L
ND
1.0
11/04/20 16:34
1,3-Dichlorobenzene
ug/L
ND
1.0
11/04/20 16:34
1,4-Dichlorobenzene
ug/L
ND
1.0
11/04/20 16:34
2-Butanone (MEK)
ug/L
ND
5.0
11/04/20 16:34
2-Hexanone
ug/L
ND
5.0
11/04/20 16:34
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
11/04/20 16:34
Acetone
ug/L
ND
25.0
11/04/20 16:34
Benzene
ug/L
ND
1.0
11/04/20 16:34
Bromochloromethane
ug/L
ND
1.0
11/04/20 16:34
Bromodichloromethane
ug/L
ND
1.0
11/04/20 16:34
Bromoform
ug/L
ND
1.0
11/04/20 16:34
Bromomethane
ug/L
ND
2.0
11/04/20 16:34
Carbon disulfide
ug/L
ND
2.0
11/04/20 16:34
Carbon tetrachloride
ug/L
ND
1.0
11/04/20 16:34
Chlorobenzene
ug/L
ND
1.0
11/04/20 16:34
Chloroethane
ug/L
ND
1.0
11/04/20 16:34
Chloroform
ug/L
ND
5.0
11/04/20 16:34
Chloromethane
ug/L
ND
1.0
11/04/20 16:34
cis-1,2-Dichloroethene
ug/L
ND
1.0
11/04/20 16:34
cis-1,3-Dichloropropene
ug/L
ND
1.0
11/04/20 16:34
Cyclohexane
ug/L
ND
1.0
11/04/20 16:34
Dibromochloromethane
ug/L
ND
1.0
11/04/20 16:34
Dichlorodifluoromethane
ug/L
ND
1.0
11/04/20 16:34
Ethylbenzene
ug/L
ND
1.0
11/04/20 16:34
Isopropylbenzene (Cumene)
ug/L
ND
1.0
11/04/20 16:34
Methyl acetate
ug/L
ND
10.0
11/04/20 16:34
Methyl-tert-butyl ether
ug/L
ND
1.0
11/04/20 16:34
Methylcyclohexane
ug/L
ND
10.0
11/04/20 16:34
v2
v2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC. Page 62 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
METHOD BLANK: 3057787 Matrix: Water
Associated Lab Samples: 92503658001, 92503658002, 92503658004, 92503658006, 92503658007, 92503658014, 92503658015
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Methylene Chloride
ug/L
ND
5.0
11/04/20 16:34
Styrene
ug/L
ND
1.0
11/04/20 16:34
Tetrachloroethene
ug/L
ND
1.0
11/04/20 16:34
Toluene
ug/L
ND
1.0
11/04/20 16:34
trans-1,2-Dichloroethene
ug/L
ND
1.0
11/04/20 16:34
trans- 1,3-Dichloropropene
ug/L
ND
1.0
11/04/20 16:34
Trichloroethene
ug/L
ND
1.0
11/04/20 16:34
Trichlorofluoromethane
ug/L
ND
1.0
11/04/20 16:34
Vinyl chloride
ug/L
ND
1.0
11/04/20 16:34
Xylene (Total)
ug/L
ND
1.0
11/04/20 16:34
1,2-Dichloroethane-d4 (S)
%
97
70-130
11/04/20 16:34
4-Bromofluorobenzene (S)
%
100
70-130
11/04/20 16:34
Toluene-d8 (S)
%
103
70-130
11/04/20 16:34
LABORATORY CONTROL SAMPLE:
Parameter
3057788
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1-Trichloroethane
ug/L
50
48.8
98
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
52.9
106
70-130
1,1,2-Trichloroethane
ug/L
50
52.7
105
70-130
1,1,2-Trichlorotrifluoroethane
ug/L
50
54.3
109
70-130
1,1-Dichloroethane
ug/L
50
50.5
101
70-130
1,1-Dichloroethene
ug/L
50
53.2
106
70-132
1,2,3-Trichlorobenzene
ug/L
50
50.8
102
70-134
1,2,4-Trichlorobenzene
ug/L
50
51.2
102
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
53.1
106
70-132
1,2-Dibromoethane (EDB)
ug/L
50
50.8
102
70-130
1,2-Dichlorobenzene
ug/L
50
50.4
101
70-130
1,2-Dichloroethane
ug/L
50
46.7
93
70-130
1,2-Dichloropropane
ug/L
50
52.0
104
70-130
1,3-Dichlorobenzene
ug/L
50
51.0
102
70-130
1,4-Dichlorobenzene
ug/L
50
50.5
101
70-130
2-Butanone (MEK)
ug/L
100
103
103
70-133
2-Hexanone
ug/L
100
102
102
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
99.2
99
70-130
Acetone
ug/L
100
112
112
70-144
Benzene
ug/L
50
51.0
102
70-130
Bromochloromethane
ug/L
50
51.3
103
70-130
Bromodichloromethane
ug/L
50
47.7
95
70-130
Bromoform
ug/L
50
49.9
100
70-131
Bromomethane
ug/L
50
39.4
79
30-177 v3
Carbon disulfide
ug/L
50
53.8
108
70-133
Carbon tetrachloride
ug/L
50
49.3
99
70-130
Chlorobenzene
ug/L
50
51.5
103
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC. Page 63 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
LABORATORY CONTROL SAMPLE:
Parameter
3057788
Units
Spike
Conc.
LCS LCS
Result % Rec
Chloroethane
ug/L
50
38.1
Chloroform
ug/L
50
47.4
Chloromethane
ug/L
50
45.9
cis-1,2-Dichloroethene
ug/L
50
50.0
cis-1,3-Dichloropropene
ug/L
50
52.0
Cyclohexane
ug/L
50
51.8
Dibromochloromethane
ug/L
50
52.5
Dichlorodifluoromethane
ug/L
50
49.4
Ethylbenzene
ug/L
50
50.7
Isopropylbenzene (Cumene)
ug/L
50
51.0
Methyl acetate
ug/L
50
51.7
Methyl-tert-butyl ether
ug/L
50
50.8
Methylcyclohexane
ug/L
50
51.4
Methylene Chloride
ug/L
50
48.9
Styrene
ug/L
50
51.0
Tetrachloroethene
ug/L
50
50.1
Toluene
ug/L
50
51.4
trans-1,2-Dichloroethene
ug/L
50
52.4
trans- 1,3-Dichloropropene
ug/L
50
51.4
Trichloroethene
ug/L
50
50.8
Trichlorofluoromethane
ug/L
50
42.3
Vinyl chloride
ug/L
50
48.4
Xylene (Total)
ug/L
150
153
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
% Rec
Limits Qualifiers
76
46-131 v3
95
70-130
92
49-130
100
70-130
104
70-130
104
70-131
105
70-130
99
52-134
101
70-130
102
70-130
103
70-131
102
70-130
103
70-130
98
68-130
102
70-130
100
70-130
103
70-130
105
70-130
103
70-130
102
70-130
85
61-130
97
59-142
102
70-130
92
70-130
102
70-130
101
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3057789
MS
92503658002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3057790
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1-Trichloroethane
ug/L
ND
500
500
594
568
119
114
70-148
5
1,1,2,2-Tetrachloroethane
ug/L
ND
500
500
618
546
124
109
70-131
12
1,1,2-Trichloroethane
ug/L
ND
500
500
603
553
121
111
70-136
9
1,1,2-Trichlorotrifluoroethane
ug/L
ND
500
500
648
616
130
123
70-154
5
1,1-Dichloroethane
ug/L
ND
500
500
614
586
120
114
70-147
5
1,1-Dichloroethene
ug/L
ND
500
500
645
607
129
121
70-158
6
1,2,3-Trichlorobenzene
ug/L
ND
500
500
601
552
120
110
68-140
8
1,2,4-Trichlorobenzene
ug/L
ND
500
500
601
548
120
110
70-139
9
1,2-Dibromo-3-chloropropane
ug/L
ND
500
500
666
580
133
116
69-136
14
1,2-Dibromoethane (EDB)
ug/L
ND
500
500
592
536
118
107
70-137
10
1,2-Dichlorobenzene
ug/L
ND
500
500
625
568
125
114
70-133
9
1,2-Dichloroethane
ug/L
ND
500
500
557
525
111
105
67-138
6
1,2-Dichloropropane
ug/L
ND
500
500
600
557
120
111
70-138
7
1,3-Dichlorobenzene
ug/L
ND
500
500
627
577
125
115
70-133
8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 64 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3057789
3057790
MS
MSD
92503658002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,4-Dichlorobenzene
ug/L
ND
500
500
619
560
124
112
70-133
10
2-Butanone (MEK)
ug/L
708
1000
1000
1930
1840
122
113
61-147
4
2-Hexanone
ug/L
ND
1000
1000
1240
1090
119
104
67-139
13
4-Methyl-2-pentanone (MIBK)
ug/L
ND
1000
1000
1240
1080
119
104
67-136
14
Acetone
ug/L
5070
1000
1000
6350
6180
128
111
55-159
3
Benzene
ug/L
ND
500
500
610
556
122
111
67-150
9
Bromochloromethane
ug/L
ND
500
500
602
567
120
113
70-146
6
Bromodichloromethane
ug/L
ND
500
500
562
533
112
107
70-138
5
Bromoform
ug/L
ND
500
500
578
528
116
106
57-138
9
Bromomethane
ug/L
ND
500
500
396
435
79
87
10-200
9 v3
Carbon disulfide
ug/L
ND
500
500
579
568
116
114
70-152
2
Carbon tetrachloride
ug/L
ND
500
500
613
577
123
115
70-147
6
Chlorobenzene
ug/L
ND
500
500
603
550
121
110
70-137
9
Chloroethane
ug/L
29.6
500
500
515
561
97
106
51-166
9 v3
Chloroform
ug/L
ND
500
500
587
522
117
104
70-144
12
Chloromethane
ug/L
ND
500
500
512
506
102
101
24-161
1
cis-1,2-Dichloroethene
ug/L
ND
500
500
576
538
115
108
67-148
7
cis-1,3-Dichloropropene
ug/L
ND
500
500
590
531
118
106
70-142
11
Cyclohexane
ug/L
ND
500
500
595
577
119
115
70-151
3
Dibromochloromethane
ug/L
ND
500
500
604
550
121
110
68-138
9
Dichlorodifluoromethane
ug/L
ND
500
500
550
525
110
105
43-155
5
Ethylbenzene
ug/L
ND
500
500
600
552
120
110
68-143
8
Isopropylbenzene (Cumene)
ug/L
ND
500
500
594
549
119
110
70-136
8
Methyl acetate
ug/L
ND
500
500
594
554
119
111
55-149
7
Methyl-tert-butyl ether
ug/L
ND
500
500
563
525
113
105
59-156
7
Methylcyclohexane
ug/L
ND
500
500
612
556
122
111
70-142
10
Methylene Chloride
ug/L
ND
500
500
648
597
130
119
64-148
8
Styrene
ug/L
ND
500
500
591
535
118
107
70-136
10
Tetrachloroethene
ug/L
ND
500
500
585
540
117
108
70-139
8
Toluene
ug/L
ND
500
500
607
548
120
108
47-157
10
trans-1,2-Dichloroethene
ug/L
ND
500
500
611
577
122
115
70-149
6
trans- 1,3-Dichloropropene
ug/L
ND
500
500
573
519
115
104
70-138
10
Trichloroethene
ug/L
ND
500
500
600
551
120
110
70-149
8
Trichlorofluoromethane
ug/L
ND
500
500
575
568
115
114
61-154
1
Vinyl chloride
ug/L
ND
500
500
531
514
106
103
55-172
3
Xylene (Total)
ug/L
ND
1500
1500
1800
1630
120
109
66-145
10
1,2-Dichloroethane-d4 (S)
%
100
101
70-130
4-Bromofluorobenzene (S)
%
98
97
70-130
Toluene-d8(S)
%
100
97
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 65 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 578305 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92503658020
METHOD BLANK: 3059679
Associated Lab Samples: 92503658020
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1-Trichloroethane
ug/L
ND
1.0
11/06/20 06:04
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
11/06/20 06:04
1,1,2-Trichloroethane
ug/L
ND
1.0
11/06/20 06:04
1,1,2-Trichlorotrifluoroethane
ug/L
ND
1.0
11/06/20 06:04
1,1-Dichloroethane
ug/L
ND
1.0
11/06/20 06:04
1,1-Dichloroethene
ug/L
ND
1.0
11/06/20 06:04
1,2,3-Trichlorobenzene
ug/L
ND
1.0
11/06/20 06:04
1,2,4-Trichlorobenzene
ug/L
ND
1.0
11/06/20 06:04
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
11/06/20 06:04
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
11/06/20 06:04
1,2-Dichlorobenzene
ug/L
ND
1.0
11/06/20 06:04
1,2-Dichloroethane
ug/L
ND
1.0
11/06/20 06:04
1,2-Dichloropropane
ug/L
ND
1.0
11/06/20 06:04
1,3-Dichlorobenzene
ug/L
ND
1.0
11/06/20 06:04
1,4-Dichlorobenzene
ug/L
ND
1.0
11/06/20 06:04
2-Butanone (MEK)
ug/L
ND
5.0
11/06/20 06:04
2-Hexanone
ug/L
ND
5.0
11/06/20 06:04
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
11/06/20 06:04
Acetone
ug/L
ND
25.0
11/06/20 06:04
Benzene
ug/L
ND
1.0
11/06/20 06:04
Bromochloromethane
ug/L
ND
1.0
11/06/20 06:04
Bromodichloromethane
ug/L
ND
1.0
11/06/20 06:04
Bromoform
ug/L
ND
1.0
11/06/20 06:04
Bromomethane
ug/L
ND
2.0
11/06/20 06:04
Carbon disulfide
ug/L
ND
2.0
11/06/20 06:04
Carbon tetrachloride
ug/L
ND
1.0
11/06/20 06:04
Chlorobenzene
ug/L
ND
1.0
11/06/20 06:04
Chloroethane
ug/L
ND
1.0
11/06/20 06:04
Chloroform
ug/L
ND
5.0
11/06/20 06:04
Chloromethane
ug/L
ND
1.0
11/06/20 06:04
cis-1,2-Dichloroethene
ug/L
ND
1.0
11/06/20 06:04
cis-1,3-Dichloropropene
ug/L
ND
1.0
11/06/20 06:04
Cyclohexane
ug/L
ND
1.0
11/06/20 06:04
Dibromochloromethane
ug/L
ND
1.0
11/06/20 06:04
Dichlorodifluoromethane
ug/L
ND
1.0
11/06/20 06:04
Ethylbenzene
ug/L
ND
1.0
11/06/20 06:04
Isopropylbenzene (Cumene)
ug/L
ND
1.0
11/06/20 06:04
Methyl acetate
ug/L
ND
10.0
11/06/20 06:04
Methyl-tert-butyl ether
ug/L
ND
1.0
11/06/20 06:04
Methylcyclohexane
ug/L
ND
10.0
11/06/20 06:04
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC. Page 66 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
METHOD BLANK: 3059679
Associated Lab Samples: 92503658020
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed Qualifiers
Methylene Chloride
ug/L
ND
5.0
11/06/20 06:04
Styrene
ug/L
ND
1.0
11/06/20 06:04
Tetrachloroethene
ug/L
ND
1.0
11/06/20 06:04
Toluene
ug/L
ND
1.0
11/06/20 06:04
trans-1,2-Dichloroethene
ug/L
ND
1.0
11/06/20 06:04
trans- 1,3-Dichloropropene
ug/L
ND
1.0
11/06/20 06:04
Trichloroethene
ug/L
ND
1.0
11/06/20 06:04
Trichlorofluoromethane
ug/L
ND
1.0
11/06/20 06:04
Vinyl chloride
ug/L
ND
1.0
11/06/20 06:04
Xylene (Total)
ug/L
ND
1.0
11/06/20 06:04
1,2-Dichloroethane-d4 (S)
%
94
70-130
11/06/20 06:04
4-Bromofluorobenzene (S)
%
100
70-130
11/06/20 06:04
Toluene-d8 (S)
%
96
70-130
11/06/20 06:04
LABORATORY CONTROL SAMPLE:
Parameter
3059680
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1-Trichloroethane
ug/L
50
47.4
95
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
48.8
98
70-130
1,1,2-Trichloroethane
ug/L
50
48.8
98
70-130
1,1,2-Trichlorotrifluoroethane
ug/L
50
46.0
92
70-130
1,1-Dichloroethane
ug/L
50
49.1
98
70-130
1,1-Dichloroethene
ug/L
50
52.0
104
70-132
1,2,3-Trichlorobenzene
ug/L
50
50.6
101
70-134
1,2,4-Trichlorobenzene
ug/L
50
50.4
101
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
49.6
99
70-132
1,2-Dibromoethane (EDB)
ug/L
50
48.3
97
70-130
1,2-Dichlorobenzene
ug/L
50
50.5
101
70-130
1,2-Dichloroethane
ug/L
50
44.9
90
70-130
1,2-Dichloropropane
ug/L
50
49.8
100
70-130
1,3-Dichlorobenzene
ug/L
50
51.9
104
70-130
1,4-Dichlorobenzene
ug/L
50
51.6
103
70-130
2-Butanone (MEK)
ug/L
100
89.3
89
70-133
2-Hexanone
ug/L
100
99.4
99
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
94.9
95
70-130
Acetone
ug/L
100
104
104
70-144
Benzene
ug/L
50
49.4
99
70-130
Bromochloromethane
ug/L
50
48.8
98
70-130
Bromodichloromethane
ug/L
50
48.9
98
70-130
Bromoform
ug/L
50
48.7
97
70-131
Bromomethane
ug/L
50
37.0
74
30-177 v3
Carbon disulfide
ug/L
50
52.3
105
70-133
Carbon tetrachloride
ug/L
50
51.7
103
70-130
Chlorobenzene
ug/L
50
53.4
107
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC. Page 67 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
LABORATORY CONTROL SAMPLE:
Parameter
3059680
Units
Spike LCS
Conc. Result
Chloroethane
ug/L
50
Chloroform
ug/L
50
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Cyclohexane
ug/L
50
Dibromochloromethane
ug/L
50
Dichlorodifluoromethane
ug/L
50
Ethylbenzene
ug/L
50
Isopropylbenzene (Cumene)
ug/L
50
Methyl acetate
ug/L
50
Methyl-tert-butyl ether
ug/L
50
Methylcyclohexane
ug/L
50
Methylene Chloride
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
% Rec
% Rec
Limits
44.9
90
46-131
45.1
90
70-130
40.4
81
49-130
47.0
94
70-130
50.2
100
70-130
51.4
103
70-131
52.9
106
70-130
41.3
83
52-134
52.0
104
70-130
51.9
104
70-130
44.0
88
70-131
44.4
89
70-130
47.2
94
70-130
45.5
91
68-130
52.1
104
70-130
44.3
89
70-130
50.6
101
70-130
48.3
97
70-130
49.2
98
70-130
52.0
104
70-130
43.4
87
61-130
36.8
74
59-142
156
104
70-130
94
70-130
102
70-130
99
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3059681
MS
7348180008 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3059682
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1-Trichloroethane
ug/L
ND
20
20
22.2
24.6
111
123
70-148
10
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
21.3
24.5
107
122
70-131
14
1,1,2-Trichloroethane
ug/L
ND
20
20
21.0
24.0
105
120
70-136
14
1,1,2-Trichlorotrifluoroethane
ug/L
ND
20
20
24.0
26.2
120
131
70-154
9
1,1-Dichloroethane
ug/L
ND
20
20
22.8
25.5
114
128
70-147
11
1,1-Dichloroethene
ug/L
ND
20
20
24.1
26.8
121
134
70-158
11
1,2,3-Trichlorobenzene
ug/L
ND
20
20
15.8
17.2
79
86
68-140
9
1,2,4-Trichlorobenzene
ug/L
ND
20
20
16.0
17.7
80
88
70-139
10
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
21.7
24.3
109
121
69-136
11
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.5
23.9
107
120
70-137
11
1,2-Dichlorobenzene
ug/L
ND
20
20
20.7
23.1
104
116
70-133
11
1,2-Dichloroethane
ug/L
ND
20
20
20.3
22.4
102
112
67-138
10
1,2-Dichloropropane
ug/L
ND
20
20
21.7
24.1
108
120
70-138
10
1,3-Dichlorobenzene
ug/L
ND
20
20
21.0
23.2
105
116
70-133
10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 68 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3059681
3059682
MS
MSD
7348180008
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,4-Dichlorobenzene
ug/L
ND
20
20
20.8
23.1
104
116
70-133
10
2-Butanone (MEK)
ug/L
ND
40
40
41.5
46.7
104
117
61-147
12
2-Hexanone
ug/L
ND
40
40
40.8
47.9
102
120
67-139
16
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
38.6
43.9
96
110
67-136
13
Acetone
ug/L
ND
40
40
43.6
48.8
109
122
55-159
11
Benzene
ug/L
ND
20
20
21.9
25.4
110
127
67-150
15
Bromochloromethane
ug/L
ND
20
20
21.8
24.1
109
121
70-146
10
Bromodichloromethane
ug/L
ND
20
20
19.9
22.6
99
113
70-138
13
Bromoform
ug/L
ND
20
20
19.0
22.0
95
110
57-138
15
Bromomethane
ug/L
ND
20
20
21.2
22.3
106
112
10-200
5 v3
Carbon disulfide
ug/L
ND
20
20
23.3
26.4
117
132
70-152
12
Carbon tetrachloride
ug/L
ND
20
20
22.0
24.6
110
123
70-147
11
Chlorobenzene
ug/L
ND
20
20
21.8
25.3
109
126
70-137
15
Chloroethane
ug/L
ND
20
20
21.2
24.6
106
123
51-166
15
Chloroform
ug/L
ND
20
20
21.3
22.0
106
110
70-144
3
Chloromethane
ug/L
ND
20
20
22.0
24.4
110
122
24-161
11
cis-1,2-Dichloroethene
ug/L
ND
20
20
22.8
25.1
110
121
67-148
10
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.4
24.0
107
120
70-142
11
Cyclohexane
ug/L
ND
20
20
21.9
24.3
110
121
70-151
10
Dibromochloromethane
ug/L
ND
20
20
20.6
23.9
103
120
68-138
15
Dichlorodifluoromethane
ug/L
ND
20
20
22.0
23.7
110
119
43-155
8
Ethylbenzene
ug/L
ND
20
20
21.6
24.6
108
123
68-143
13
Isopropylbenzene (Cumene)
ug/L
ND
20
20
20.0
23.2
100
116
70-136
15
Methyl acetate
ug/L
ND
20
20
20.8
22.6
104
113
55-149
8
Methyl-tert-butyl ether
ug/L
ND
20
20
20.2
23.0
101
115
59-156
13
Methylcyclohexane
ug/L
ND
20
20
17.7
20.2
88
101
70-142
13
Methylene Chloride
ug/L
ND
20
20
21.3
23.5
107
118
64-148
10
Styrene
ug/L
ND
20
20
17.5
20.7
88
104
70-136
17
Tetrachloroethene
ug/L
ND
20
20
20.6
23.5
103
117
70-139
13
Toluene
ug/L
ND
20
20
21.5
24.5
108
122
47-157
13
trans-1,2-Dichloroethene
ug/L
ND
20
20
23.5
25.6
118
128
70-149
8
trans- 1,3-Dichloropropene
ug/L
ND
20
20
20.4
22.7
102
114
70-138
11
Trichloroethene
ug/L
ND
20
20
21.8
25.1
109
126
70-149
14
Trichlorofluoromethane
ug/L
ND
20
20
21.0
23.2
105
116
61-154
10
Vinyl chloride
ug/L
ND
20
20
22.2
23.9
111
120
55-172
7
Xylene (Total)
ug/L
ND
60
60
63.7
73.1
106
122
66-145
14
1,2-Dichloroethane-d4 (S)
%
95
93
70-130
4-Bromofluorobenzene (S)
%
97
99
70-130
Toluene-d8(S)
%
98
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 69 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 578368 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92503658021
METHOD BLANK: 3060053
Associated Lab Samples: 92503658021
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1-Trichloroethane
ug/L
ND
1.0
11/06/20 02:43
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
11/06/20 02:43
1,1,2-Trichloroethane
ug/L
ND
1.0
11/06/20 02:43
1,1,2-Trichlorotrifluoroethane
ug/L
ND
1.0
11/06/20 02:43
1,1-Dichloroethane
ug/L
ND
1.0
11/06/20 02:43
1,1-Dichloroethene
ug/L
ND
1.0
11/06/20 02:43
1,2,3-Trichlorobenzene
ug/L
ND
1.0
11/06/20 02:43
1,2,4-Trichlorobenzene
ug/L
ND
1.0
11/06/20 02:43
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
11/06/20 02:43
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
11/06/20 02:43
1,2-Dichlorobenzene
ug/L
ND
1.0
11/06/20 02:43
1,2-Dichloroethane
ug/L
ND
1.0
11/06/20 02:43
1,2-Dichloropropane
ug/L
ND
1.0
11/06/20 02:43
1,3-Dichlorobenzene
ug/L
ND
1.0
11/06/20 02:43
1,4-Dichlorobenzene
ug/L
ND
1.0
11/06/20 02:43
2-Butanone (MEK)
ug/L
ND
5.0
11/06/20 02:43
2-Hexanone
ug/L
ND
5.0
11/06/20 02:43
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
11/06/20 02:43
Acetone
ug/L
ND
25.0
11/06/20 02:43
Benzene
ug/L
ND
1.0
11/06/20 02:43
Bromochloromethane
ug/L
ND
1.0
11/06/20 02:43
Bromodichloromethane
ug/L
ND
1.0
11/06/20 02:43
Bromoform
ug/L
ND
1.0
11/06/20 02:43
Bromomethane
ug/L
ND
2.0
11/06/20 02:43
Carbon disulfide
ug/L
ND
2.0
11/06/20 02:43
Carbon tetrachloride
ug/L
ND
1.0
11/06/20 02:43
Chlorobenzene
ug/L
ND
1.0
11/06/20 02:43
Chloroethane
ug/L
ND
1.0
11/06/20 02:43
Chloroform
ug/L
ND
5.0
11/06/20 02:43
Chloromethane
ug/L
ND
1.0
11/06/20 02:43
cis-1,2-Dichloroethene
ug/L
ND
1.0
11/06/20 02:43
cis-1,3-Dichloropropene
ug/L
ND
1.0
11/06/20 02:43
Cyclohexane
ug/L
ND
1.0
11/06/20 02:43
Dibromochloromethane
ug/L
ND
1.0
11/06/20 02:43
Dichlorodifluoromethane
ug/L
ND
1.0
11/06/20 02:43
Ethylbenzene
ug/L
ND
1.0
11/06/20 02:43
Isopropylbenzene (Cumene)
ug/L
ND
1.0
11/06/20 02:43
Methyl acetate
ug/L
ND
10.0
11/06/20 02:43
Methyl-tert-butyl ether
ug/L
ND
1.0
11/06/20 02:43
Methylcyclohexane
ug/L
ND
10.0
11/06/20 02:43
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC. Page 70 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
METHOD BLANK: 3060053
Associated Lab Samples: 92503658021
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed Qualifiers
Methylene Chloride
ug/L
ND
5.0
11/06/20 02:43
Styrene
ug/L
ND
1.0
11/06/20 02:43
Tetrachloroethene
ug/L
ND
1.0
11/06/20 02:43
Toluene
ug/L
ND
1.0
11/06/20 02:43
trans-1,2-Dichloroethene
ug/L
ND
1.0
11/06/20 02:43
trans- 1,3-Dichloropropene
ug/L
ND
1.0
11/06/20 02:43
Trichloroethene
ug/L
ND
1.0
11/06/20 02:43
Trichlorofluoromethane
ug/L
ND
1.0
11/06/20 02:43
Vinyl chloride
ug/L
ND
1.0
11/06/20 02:43
Xylene (Total)
ug/L
ND
1.0
11/06/20 02:43
1,2-Dichloroethane-d4 (S)
%
104
70-130
11/06/20 02:43
4-Bromofluorobenzene (S)
%
98
70-130
11/06/20 02:43
Toluene-d8 (S)
%
102
70-130
11/06/20 02:43
LABORATORY CONTROL SAMPLE:
Parameter
3060054
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1-Trichloroethane
ug/L
50
47.1
94
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
51.8
104
70-130
1,1,2-Trichloroethane
ug/L
50
50.4
101
70-130
1,1,2-Trichlorotrifluoroethane
ug/L
50
50.5
101
70-130
1,1-Dichloroethane
ug/L
50
49.5
99
70-130
1,1-Dichloroethene
ug/L
50
51.1
102
70-132
1,2,3-Trichlorobenzene
ug/L
50
49.4
99
70-134
1,2,4-Trichlorobenzene
ug/L
50
50.2
100
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
54.3
109
70-132
1,2-Dibromoethane (EDB)
ug/L
50
50.9
102
70-130
1,2-Dichlorobenzene
ug/L
50
50.1
100
70-130
1,2-Dichloroethane
ug/L
50
47.0
94
70-130
1,2-Dichloropropane
ug/L
50
48.5
97
70-130
1,3-Dichlorobenzene
ug/L
50
50.9
102
70-130
1,4-Dichlorobenzene
ug/L
50
50.2
100
70-130
2-Butanone (MEK)
ug/L
100
104
104
70-133
2-Hexanone
ug/L
100
109
109
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
101
101
70-130
Acetone
ug/L
100
125
125
70-144
Benzene
ug/L
50
48.1
96
70-130
Bromochloromethane
ug/L
50
45.7
91
70-130
Bromodichloromethane
ug/L
50
46.2
92
70-130
Bromoform
ug/L
50
49.8
100
70-131
Bromomethane
ug/L
50
40.0
80
30-177 v3
Carbon disulfide
ug/L
50
50.7
101
70-133
Carbon tetrachloride
ug/L
50
46.9
94
70-130
Chlorobenzene
ug/L
50
50.8
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC. Page 71 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
LABORATORY CONTROL SAMPLE:
Parameter
3060054
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Chloroethane
ug/L
50
35.8
72
46-131
Chloroform
ug/L
50
43.5
87
70-130
Chloromethane
ug/L
50
45.3
91
49-130
cis-1,2-Dichloroethene
ug/L
50
47.7
95
70-130
cis-1,3-Dichloropropene
ug/L
50
48.2
96
70-130
Cyclohexane
ug/L
50
46.9
94
70-131
Dibromochloromethane
ug/L
50
51.5
103
70-130
Dichlorodifluoromethane
ug/L
50
46.3
93
52-134
Ethylbenzene
ug/L
50
49.6
99
70-130
Isopropylbenzene (Cumene)
ug/L
50
49.4
99
70-130
Methyl acetate
ug/L
50
52.2
104
70-131
Methyl-tert-butyl ether
ug/L
50
48.1
96
70-130
Methylcyclohexane
ug/L
50
46.7
93
70-130
Methylene Chloride
ug/L
50
47.8
96
68-130
Styrene
ug/L
50
49.7
99
70-130
Tetrachloroethene
ug/L
50
48.6
97
70-130
Toluene
ug/L
50
48.3
97
70-130
trans-1,2-Dichloroethene
ug/L
50
49.3
99
70-130
trans- 1,3-Dichloropropene
ug/L
50
48.1
96
70-130
Trichloroethene
ug/L
50
48.0
96
70-130
Trichlorofluoromethane
ug/L
50
41.5
83
61-130
Vinyl chloride
ug/L
50
44.7
89
59-142
Xylene (Total)
ug/L
150
151
100
70-130
1,2-Dichloroethane-d4 (S)
%
98
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
98
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3060055
MS
7348141005 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3060056
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1-Trichloroethane
ug/L
ND
20
20
21.2
25.5
106
128
70-148
19
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
20.4
24.8
102
124
70-131
19
1,1,2-Trichloroethane
ug/L
ND
20
20
20.2
24.0
101
120
70-136
17
1,1,2-Trichlorotrifluoroethane
ug/L
ND
20
20
23.5
27.6
117
138
70-154
16
1,1-Dichloroethane
ug/L
ND
20
20
21.0
25.4
105
127
70-147
19
1,1-Dichloroethene
ug/L
ND
20
20
23.2
27.5
116
138
70-158
17
1,2,3-Trichlorobenzene
ug/L
ND
20
20
18.1
20.7
90
103
68-140
13
1,2,4-Trichlorobenzene
ug/L
ND
20
20
18.3
20.6
91
103
70-139
12
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
21.0
24.5
105
123
69-136
15
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
20.2
24.3
101
121
70-137
19
1,2-Dichlorobenzene
ug/L
ND
20
20
20.7
24.3
104
122
70-133
16
1,2-Dichloroethane
ug/L
ND
20
20
19.3
22.8
96
114
67-138
17
1,2-Dichloropropane
ug/L
ND
20
20
20.5
25.2
103
126
70-138
20
1,3-Dichlorobenzene
ug/L
ND
20
20
21.2
24.6
106
123
70-133
14
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 72 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3060055
3060056
MS
MSD
7348141005
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,4-Dichlorobenzene
ug/L
ND
20
20
20.8
24.2
104
121
70-133
15
2-Butanone (MEK)
ug/L
ND
40
40
40.6
48.4
102
121
61-147
18
2-Hexanone
ug/L
ND
40
40
40.7
49.9
102
125
67-139
20
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
37.6
45.5
94
114
67-136
19
Acetone
ug/L
ND
40
40
42.4
51.6
106
129
55-159
19
Benzene
ug/L
ND
20
20
21.1
25.4
105
127
67-150
19
Bromochloromethane
ug/L
ND
20
20
21.0
24.6
105
123
70-146
16
Bromodichloromethane
ug/L
ND
20
20
19.3
23.1
96
116
70-138
18
Bromoform
ug/L
ND
20
20
18.5
23.0
93
115
57-138
21
Bromomethane
ug/L
ND
20
20
19.0
22.3
95
111
10-200
16 v3
Carbon disulfide
ug/L
ND
20
20
20.9
24.5
105
123
70-152
16
Carbon tetrachloride
ug/L
ND
20
20
21.6
25.8
108
129
70-147
18
Chlorobenzene
ug/L
ND
20
20
20.9
25.2
104
126
70-137
19
Chloroethane
ug/L
ND
20
20
19.6
21.6
98
108
51-166
10
Chloroform
ug/L
ND
20
20
19.0
24.1
95
121
70-144
24
Chloromethane
ug/L
ND
20
20
20.8
22.0
104
110
24-161
6
cis-1,2-Dichloroethene
ug/L
ND
20
20
20.9
24.6
104
123
67-148
16
cis-1,3-Dichloropropene
ug/L
ND
20
20
20.1
24.4
100
122
70-142
19
Cyclohexane
ug/L
ND
20
20
22.1
25.4
111
127
70-151
14
Dibromochloromethane
ug/L
ND
20
20
19.9
24.3
99
121
68-138
20
Dichlorodifluoromethane
ug/L
ND
20
20
21.1
25.3
105
127
43-155
18
Ethylbenzene
ug/L
ND
20
20
20.8
25.4
104
127
68-143
20
Isopropylbenzene (Cumene)
ug/L
ND
20
20
20.4
24.4
102
122
70-136
18
Methyl acetate
ug/L
ND
20
20
19.3
24.6
97
123
55-149
24
Methyl-tert-butyl ether
ug/L
ND
20
20
19.0
23.1
95
115
59-156
19
Methylcyclohexane
ug/L
ND
20
20
20.1
23.0
100
115
70-142
14
Methylene Chloride
ug/L
ND
20
20
20.8
24.3
104
122
64-148
16
Styrene
ug/L
ND
20
20
19.3
23.8
96
119
70-136
21
Tetrachloroethene
ug/L
ND
20
20
21.0
24.6
105
123
70-139
16
Toluene
ug/L
ND
20
20
20.4
24.8
102
124
47-157
20
trans-1,2-Dichloroethene
ug/L
ND
20
20
23.0
26.5
115
133
70-149
14
trans- 1,3-Dichloropropene
ug/L
ND
20
20
20.1
23.9
100
119
70-138
17
Trichloroethene
ug/L
ND
20
20
21.2
25.2
106
126
70-149
18
Trichlorofluoromethane
ug/L
ND
20
20
20.8
24.5
104
123
61-154
17
Vinyl chloride
ug/L
ND
20
20
20.5
23.5
102
118
55-172
14
Xylene (Total)
ug/L
ND
60
60
61.6
74.8
103
125
66-145
19
1,2-Dichloroethane-d4 (S)
%
96
97
70-130
4-Bromofluorobenzene (S)
%
99
101
70-130
Toluene-d8(S)
%
98
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 73 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3060057
3060058
MS
MSD
7348171008
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
1,1,1-Trichloroethane
ug/L
ND
20
20
23.9
23.3
120
116
70-148
3
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.6
22.2
113
111
70-131
2
1,1,2-Trichloroethane
ug/L
ND
20
20
23.1
21.7
116
109
70-136
6
1,1,2-Trichlorotrifluoroethane
ug/L
ND
20
20
25.6
24.8
128
124
70-154
3
1,1-Dichloroethane
ug/L
ND
20
20
24.3
24.9
119
122
70-147
2
1,1-Dichloroethene
ug/L
ND
20
20
25.7
25.0
129
125
70-158
3
1,2,3-Trichlorobenzene
ug/L
ND
20
20
20.2
19.9
101
100
68-140
1
1,2,4-Trichlorobenzene
ug/L
ND
20
20
21.1
20.4
106
102
70-139
4
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
22.8
23.3
114
116
69-136
2
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.4
23.0
112
115
70-137
3
1,2-Dichlorobenzene
ug/L
6.7
20
20
29.5
29.4
114
114
70-133
0
1,2-Dichloroethane
ug/L
ND
20
20
21.3
20.7
106
104
67-138
3
1,2-Dichloropropane
ug/L
ND
20
20
23.0
22.2
115
111
70-138
3
1,3-Dichlorobenzene
ug/L
ND
20
20
23.8
23.4
116
114
70-133
2
1,4-Dichlorobenzene
ug/L
4.7
20
20
27.9
27.6
116
114
70-133
1
2-Butanone (MEK)
ug/L
ND
40
40
44.2
45.4
110
113
61-147
3
2-Hexanone
ug/L
ND
40
40
44.1
44.3
110
111
67-139
0
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
42.0
40.8
105
102
67-136
3
Acetone
ug/L
ND
40
40
45.8
48.3
114
121
55-159
5
Benzene
ug/L
2.1
20
20
25.8
24.5
119
112
67-150
5
Bromochloromethane
ug/L
ND
20
20
23.2
22.8
116
114
70-146
2
Bromodichloromethane
ug/L
ND
20
20
21.5
20.5
107
103
70-138
4
Bromoform
ug/L
ND
20
20
21.0
20.5
105
103
57-138
2
Bromomethane
ug/L
ND
20
20
20.7
20.8
104
104
10-200
0 v3
Carbon disulfide
ug/L
ND
20
20
24.8
24.3
124
121
70-152
2
Carbon tetrachloride
ug/L
ND
20
20
23.7
22.7
118
114
70-147
4
Chlorobenzene
ug/L
26.5
20
20
50.5
49.7
120
116
70-137
2
Chloroethane
ug/L
ND
20
20
22.1
22.1
111
111
51-166
0
Chloroform
ug/L
ND
20
20
21.2
20.9
106
105
70-144
1
Chloromethane
ug/L
ND
20
20
23.4
20.2
117
101
24-161
15
cis-1,2-Dichloroethene
ug/L
5.4
20
20
28.7
28.7
117
116
67-148
0
cis-1,3-Dichloropropene
ug/L
ND
20
20
22.6
21.5
113
108
70-142
5
Cyclohexane
ug/L
ND
20
20
24.2
24.1
121
120
70-151
1
Dibromochloromethane
ug/L
ND
20
20
21.8
21.9
109
109
68-138
0
Dichlorodifluoromethane
ug/L
ND
20
20
23.9
22.8
119
114
43-155
4
Ethylbenzene
ug/L
ND
20
20
23.6
22.5
118
113
68-143
5
Isopropylbenzene(Cumene)
ug/L
1.8
20
20
25.5
24.5
119
114
70-136
4
Methyl acetate
ug/L
ND
20
20
21.9
22.3
110
112
55-149
2 v3
Methyl-tert-butyl ether
ug/L
1.3
20
20
22.7
22.7
107
107
59-156
0
Methylcyclohexane
ug/L
ND
20
20
23.0
22.1
115
111
70-142
4
Methylene Chloride
ug/L
ND
20
20
21.1
22.4
105
112
64-148
6
Styrene
ug/L
ND
20
20
22.9
22.1
115
111
70-136
4
Tetrachloroethene
ug/L
ND
20
20
23.2
22.5
116
113
70-139
3
Toluene
ug/L
ND
20
20
22.8
22.5
114
112
47-157
2
trans-1,2-Dichloroethene
ug/L
ND
20
20
24.0
24.1
120
120
70-149
0
trans- 1,3-Dichloropropene
ug/L
ND
20
20
21.8
21.2
109
106
70-138
3
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 74 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3060057
3060058
MS
MSD
7348171008 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Trichloroethene
ug/L
ND 20
20
23.7
23.1
118
116
70-149
2
Trichlorofluoromethane
ug/L
ND 20
20
23.1
22.3
116
111
61-154
4
Vinyl chloride
ug/L
ND 20
20
22.2
22.0
111
110
55-172
1
Xylene (Total)
ug/L
ND 60
60
69.7
68.2
116
114
66-145
2
1,2-Dichloroethane-d4 (S)
%
96
99
70-130
4-Bromofluorobenzene (S)
%
98
97
70-130
Toluene-d8(S)
%
99
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 75 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 577993 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92503658001, 92503658002, 92503658003, 92503658004, 92503658005, 92503658006, 92503658007,
92503658008,92503658009,92503658010,92503658011,92503658012,92503658014,92503658015,
92503658016,92503658019
METHOD BLANK: 3057904 Matrix: Water
Associated Lab Samples: 92503658001, 92503658002, 92503658003, 92503658004, 92503658005, 92503658006, 92503658007,
92503658008,92503658009,92503658010,92503658011,92503658012,92503658014,92503658015,
92503658016,92503658019
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,4-Dioxane (p-Dioxane) ug/L ND 2.0 11/04/20 15:06
1,2-Dichloroethane-d4 (S) % 96 70-130 11/04/20 15:06
Toluene-d8 (S) % 89 66-133 11/04/20 15:06
LABORATORY CONTROL SAMPLE: 3057905
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 19.0 95 70-130
1,2-Dichloroethane-d4 (S) % 95 70-130
Toluene-d8 (S) % 88 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3057906 3057907
Parameter
1,4-Dioxane (p-Dioxane)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
MS
92503436012 Spike
Units Result Conc.
ug/L 1.6J 20
MSD
Spike MS
Conc. Result
20 21.5
MSD MS
Result % Rec
22.7 100
99
91
MSD % Rec
% Rec Limits RPD
106 64-141 5
98 70-130
91 66-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Qual
Page 76 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 578204 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92503658013, 92503658017, 92503658018
METHOD BLANK: 3058919
Matrix:
Water
Associated Lab Samples:
92503658013, 92503658017, 92503658018
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
11/05/20 10:33
1,2-Dichloroethane-d4 (S)
%
88
70-130
11/05/20 10:33
Toluene-d8 (S)
%
90
66-133
11/05/20 10:33
LABORATORY CONTROL SAMPLE: 3058920
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 17.5 88 70-130
1,2-Dichloroethane-d4 (S) % 85 70-130
Toluene-d8 (S) % 91 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3058921
3058922
MS
MSD
92502848005 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L 20.0 20
20 39.5
39.1 98
95
64-141 1
1,2-Dichloroethane-d4 (S)
%
87
87
70-130
Toluene-d8(S)
%
84
90
66-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 77 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 578313 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92503658020, 92503658021
METHOD BLANK: 3059759
Associated Lab Samples: 92503658020, 92503658021
Parameter Units
1,4-Dioxane (p-Dioxane) ug/L
1,2-Dichloroethane-d4 (S) %
Toluene-d8 (S) %
Matrix: Water
Blank Reporting
Result Limit Analyzed
ND 2.0 11/05/20 20:34
86 70-130 11/05/20 20:34
94 66-133 11/05/20 20:34
Qualifiers
LABORATORY CONTROL SAMPLE: 3059760
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 17.3 86 70-130
1,2-Dichloroethane-d4 (S) % 95 70-130
Toluene-d8 (S) % 95 66-133
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3059761
3059762
MS
MSD
7348180008 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 20.0
19.2 100
96
64-141 5
1,2-Dichloroethane-d4 (S)
%
98
98
70-130
Toluene-d8(S)
%
85
85
66-133
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 78 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 578132 Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92503658001, 92503658002, 92503658003, 92503658004, 92503658006, 92503658007, 92503658008
METHOD BLANK: 3058603 Matrix: Water
Associated Lab Samples: 92503658001, 92503658002, 92503658003, 92503658004, 92503658006, 92503658007, 92503658008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Biphenyl (Diphenyl)
ug/L
ND
10.0
11/05/20 15:47
Diphenyl ether (Phenyl ether)
ug/L
ND
10.0
11/05/20 15:47
2,4,6-Tribromophenol (S)
%
108
10-144
11/05/20 15:47
2-Fluorobiphenyl (S)
%
70
10-130
11/05/20 15:47
2-Fluorophenol (S)
%
63
10-130
11/05/20 15:47
Nitrobenzene-d5 (S)
%
90
10-144
11/05/20 15:47
Phenol-d6 (S)
%
49
10-130
11/05/20 15:47
Terphenyl-d14 (S)
%
125
34-163
11/05/20 15:47
LABORATORY CONTROL SAMPLE:
Parameter
3058604
Units
Spike LCS LCS
Conc. Result % Rec
% Rec
Limits Qualifiers
Biphenyl (Diphenyl)
ug/L
50 37.7 75
31-130
Diphenyl ether (Phenyl ether)
ug/L
50 38.0 76
25-130
2,4,6-Tribromophenol (S)
%
122
10-144
2-Fluorobiphenyl (S)
%
77
10-130
2-Fluorophenol(S)
%
65
10-130
Nitrobenzene-d5 (S)
%
97
10-144
Phenol-d6 (S)
%
50
10-130
Terphenyl-d14 (S)
%
108
34-163
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3058605 3058606
Parameter
Biphenyl (Diphenyl)
Diphenyl ether (Phenyl ether)
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
MS
92503950007 Spike
Units Result Conc.
ug/L ND 50
ug/L ND 50
MSD
Spike MS
Conc. Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits RPD
50 28.7
26.0
57
52
17-130 10
50 29.3
26.5
59
53
16-130 10
75
59
10-144
43
40
10-130
44
40
10-130
55
50
10-144
38
34
10-130
88
80
34-163
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Qual
Page 79 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 578463 Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92503658009,92503658010,92503658011,92503658014,92503658015,92503658016,92503658017,
92503658018,92503658019,92503658020,92503658021
METHOD BLANK: 3060461 Matrix: Water
Associated Lab Samples: 92503658009,92503658010,92503658011,92503658014,92503658015,92503658016,92503658017,
92503658018,92503658019,92503658020,92503658021
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Biphenyl (Diphenyl)
ug/L
ND
10.0
11/06/20 13:48
Diphenyl ether (Phenyl ether)
ug/L
ND
10.0
11/06/20 13:48
2,4,6-Tribromophenol (S)
%
60
10-144
11/06/20 13:48
2-Fluorobiphenyl (S)
%
39
10-130
11/06/20 13:48
2-Fluorophenol(S)
%
35
10-130
11/06/20 13:48
Nitrobenzene-d5 (S)
%
50
10-144
11/06/20 13:48
Phenol-d6 (S)
%
23
10-130
11/06/20 13:48
Terphenyl-d14 (S)
%
104
34-163
11/06/20 13:48
LABORATORY CONTROL SAMPLE:
Parameter
3060462
Units
Spike LCS LCS
Conc. Result % Rec
% Rec
Limits Qualifiers
Biphenyl (Diphenyl)
ug/L
50 29.4 59
31-130
Diphenyl ether (Phenyl ether)
ug/L
50 30.6 61
25-130
2,4,6-Tribromophenol (S)
%
85
10-144
2-Fluorobiphenyl (S)
%
61
10-130
2-Fluorophenol(S)
%
47
10-130
Nitrobenzene-d5 (S)
%
72
10-144
Phenol-d6 (S)
%
34
10-130
Terphenyl-d14 (S)
%
91
34-163
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3060463 3060464
Parameter
Biphenyl (Diphenyl)
Diphenyl ether (Phenyl ether)
2-Fluorobiphenyl (S)
Nitrobenzene-d5 (S)
Terphenyl-d14 (S)
MS
92494245017 Spike
Units Result Conc.
ug/L ND 50
ug/L ND 50
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
50
23.5
17.2
47
34
17-130 31 R1
50
22.2
16.2
44
32
16-130 31 R1
35
31
10-130
49
36
10-144
87
62
34-163
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 80 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 579479 Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92503658001, 92503658002, 92503658003, 92503658004, 92503658005, 92503658006, 92503658014,
92503658015,92503658016,92503658017,92503658018
METHOD BLANK: 3065568 Matrix: Water
Associated Lab Samples: 92503658001, 92503658002, 92503658003, 92503658004, 92503658005, 92503658006, 92503658014,
92503658015,92503658016,92503658017,92503658018
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Alkalinity, Total as CaCO3 mg/L ND 5.0 11/11/20 13:26
LABORATORY CONTROL SAMPLE: 3065569
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Alkalinity, Total as CaCO3 mg/L 50 53.6 107 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3065570 3065571
MS MSD
92503186004 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 77100 50 50 124 127 93 99 80-120 2
ug/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3065572 3065573
MS MSD
92503658002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 2450 50 50 2440 2400 -12 -92 80-120 2 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 81 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 579481 Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92503658019, 92503658020, 92503658021
METHOD BLANK: 3065579
Matrix:
Water
Associated Lab Samples: 92503658019, 92503658020, 92503658021
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Alkalinity, Total as CaCO3
mg/L
ND
5.0
11/11/20 21:36
LABORATORY CONTROL SAMPLE:
3065580
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Alkalinity, Total as CaCO3
mg/L
50
53.4
107 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3065581 3065582
MS MSD
92503658019 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 129 50 50 177 177 97 97 80-120 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3065583 3065584
MS MSD
92503658021 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 504 50 50 528 517 49 27 80-120 2 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 82 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 577740 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92503658001, 92503658002, 92503658003, 92503658004, 92503658005, 92503658006, 92503658014,
92503658015,92503658016,92503658017,92503658018,92503658019
METHOD BLANK: 3056880 Matrix: Water
Associated Lab Samples: 92503658001, 92503658002, 92503658003, 92503658004, 92503658005, 92503658006, 92503658014,
92503658015,92503658016,92503658017,92503658018,92503658019
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L ND 0.040 11/03/20 23:35
Nitrogen, Nitrite mg/L ND 0.040 11/03/20 23:35
LABORATORY CONTROL SAMPLE: 3056881
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 1.5 1.6 104 90-110
Nitrogen, Nitrite mg/L 1 1.0 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3056882
3056883
MS
MSD
92503658001 Spike
Spike MS
MSD MS
MSD % Rec
Parameter
Units
Result Conc.
Conc. Result
Result % Rec
% Rec Limits RPD Qual
Nitrogen, Nitrate
mg/L
ND 1.5
1.5 1.3
1.3 85
84 90-110 1
Nitrogen, Nitrite
mg/L
0.046 1
1 0.99
0.98 94
94 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3056884
3056885
MS
MSD
92503658003 Spike
Spike MS
MSD MS MSD % Rec
Parameter
Units
Result Conc.
Conc. Result
Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate
mg/L
ND 1.5
1.5 1.5
1.5 98 99 90-110 1
Nitrogen, Nitrite
mg/L
ND 1
1 1.0
1.0 100 102 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 83 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 578222
Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993
Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92503658020, 92503658021
METHOD BLANK: 3059077
Matrix: Water
Associated Lab Samples: 92503658020, 92503658021
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L
ND 0.040 11/05/20 11:57
Nitrogen, Nitrite mg/L
ND 0.040 11/05/20 11:57
LABORATORY CONTROL SAMPLE: 3059078
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L
1.5 1.5 99 90-110
Nitrogen, Nitrite mg/L
1 0.99 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3059079 3059080
MS MSD
92503658020
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Nitrogen, Nitrate mg/L ND
1.5 1.5 0.45 0.44 30 30
90-110 0
Nitrogen, Nitrite mg/L 0.22
1 1 0.93 0.94 70 71
90-110 1 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 84 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 577790 Analysis Method: SM 4500-P E-2011
QC Batch Method: SM 4500-P E-2011 Analysis Description: SM450OP-E Phosphorus, Ortho
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92503658001, 92503658002, 92503658003, 92503658004, 92503658005, 92503658006, 92503658014,
92503658015,92503658016,92503658017,92503658018,92503658019
METHOD BLANK: 3057002 Matrix: Water
Associated Lab Samples: 92503658001, 92503658002, 92503658003, 92503658004, 92503658005, 92503658006, 92503658014,
92503658015,92503658016,92503658017,92503658018,92503658019
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Orthophosphate as P mg/L ND 0.050 11/04/20 08:30
LABORATORY CONTROL SAMPLE: 3057003
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Orthophosphate as P mg/L 0.25 0.25 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3057004 3057005
MS MSD
92503658001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Orthophosphate as P mg/L 0.34 0.25 0.25 1.9 1.9 620 621 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3057006 3057007
MS MSD
92503658003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Orthophosphate as P mg/L 0.064 0.25 0.25 0.30 0.30 95 95 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 85 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 578202 Analysis Method: SM 4500-P E-2011
QC Batch Method: SM 4500-P E-2011 Analysis Description: SM450OP-E Phosphorus, Ortho
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92503658020, 92503658021
METHOD BLANK: 3058914 Matrix: Water
Associated Lab Samples: 92503658020, 92503658021
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Orthophosphate as P mg/L ND 0.050 11/05/20 11:50
LABORATORY CONTROL SAMPLE & LCSD: 3058915 3058916
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Orthophosphate as P mg/L 0.25 0.25 0.25 102 102 90-110 0 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 86 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 578170 Analysis Method: EPA 9056A
QC Batch Method: EPA 9056A Analysis Description: 9056 IC anions 28 Days
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92503658001, 92503658002, 92503658003, 92503658004, 92503658005, 92503658006, 92503658014,
92503658015,92503658016,92503658017,92503658018,92503658019
METHOD BLANK: 3058701 Matrix: Water
Associated Lab Samples: 92503658001, 92503658002, 92503658003, 92503658004, 92503658005, 92503658006, 92503658014,
92503658015,92503658016,92503658017,92503658018,92503658019
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfate mg/L ND 1.0 11/05/20 23:41
LABORATORY CONTROL SAMPLE: 3058702
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Sulfate mg/L 50 53.3 107 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3058703 3058704
MS MSD
92503658001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 5.1 50 50 60.0 61.1 110 112 90-110 2 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3058705 3058706
MS MSD
92503658018 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 1.3 50 50 59.9 60.5 117 118 90-110 1 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 87 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 578495 Analysis Method: EPA 9056A
QC Batch Method: EPA 9056A Analysis Description: 9056 IC anions 28 Days
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92503658020, 92503658021
METHOD BLANK: 3060538
Matrix:
Water
Associated Lab Samples: 92503658020, 92503658021
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Sulfate
mg/L
ND
1.0
11/07/20 03:49
LABORATORY CONTROL SAMPLE:
3060539
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Sulfate
mg/L
50
49.7
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3060540 3060541
MS MSD
92503658020 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 9.2 50 50 54.8 55.1 91 92 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3060542 3060543
MS MSD
92504334007 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 22700 50 50 74.0 74.7 103 104 90-110 1
ug/L
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 88 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 580000 Analysis Method: EPA 9060A
QC Batch Method: EPA 9060A Analysis Description: 9060 TOC, AVL
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92503658001, 92503658002, 92503658014, 92503658015, 92503658016, 92503658017, 92503658019,
92503658020,92503658021
METHOD BLANK: 3068098
Matrix:
Water
Associated Lab Samples:
92503658001, 92503658002, 92503658014,
92503658015, 92503658016,
92503658017, 92503658019,
92503658020,92503658021
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Mean Total Organic Carbon
mg/L
ND
1.0
11/12/20 19:07
Total Organic Carbon
mg/L
ND
1.0
11/12/20 19:07
Total Organic Carbon
mg/L
ND
1.0
11/12/20 19:07
Total Organic Carbon
mg/L
ND
1.0
11/12/20 19:07
Total Organic Carbon
mg/L
ND
1.0
11/12/20 19:07
LABORATORY CONTROL SAMPLE:
3068099
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Mean Total Organic Carbon
mg/L
25
23.7
95
75-125
Total Organic Carbon
mg/L
25
23.7
95
75-125
Total Organic Carbon
mg/L
25
23.7
95
75-125
Total Organic Carbon
mg/L
25
23.3
93
75-125
Total Organic Carbon
mg/L
25
24.0
96
75-125
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3068100
3068101
MS
MSD
92503658001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Mean Total Organic Carbon
mg/L
2400
25
25
2290
2340
-437
-208
75-125
2 M6
Total Organic Carbon
mg/L
2390
25
25
2280
2330
-426
-218
75-125
2 M6
Total Organic Carbon
mg/L
2390
25
25
2310
2370
-336
-84
75-125
3 M6
Total Organic Carbon
mg/L
2410
25
25
2230
2300
-704
-432
75-125
3 M6
Total Organic Carbon
mg/L
2400
25
25
2330
2370
-281
-96
75-125
2 M6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 89 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 696989 Analysis Method: AM23G
QC Batch Method: AM23G Analysis Description: Low Level Volatile Fatty Acids
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92503658014, 92503658015, 92503658016, 92503658017, 92503658019, 92503658020, 92503658021
METHOD BLANK: 2109389 Matrix: Water
Associated Lab Samples: 92503658001, 92503658002, 92503658014, 92503658015, 92503658016, 92503658017, 92503658019,
92503658020,92503658021
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Acetic Acid mg/L ND 0.50 11/12/2022:14
LABORATORY CONTROL SAMPLE & LCSD: 2109390 2109391
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Acetic Acid mg/L 2 2.3 2.3 114 114 70-130 0 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 90 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92503658
QC Batch: 697678 Analysis Method: AM23G
QC Batch Method: AM23G Analysis Description: Low Level Volatile Fatty Acids
Laboratory: Pace Analytical Gulf Coast
Associated Lab Samples: 92503658001, 92503658002
METHOD BLANK: 2112976 Matrix: Water
Associated Lab Samples: 92503658001, 92503658002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Acetic Acid mg/L ND 0.50 11/18/2002:07
LABORATORY CONTROL SAMPLE & LCSD: 2112977 2112978
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Acetic Acid mg/L 2 2.0 2.0 101 101 70-130 0 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC.
Page 91 of 104

Pace Analytical Services, LLC
leac,yficalAnal816 DurstAvenue East
Greenwood, SC 29649
www.pacelabs.com [phone]
QUALIFIERS
Project: NRLF
Pace Project No.: 92503658
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
WORKORDER QUALIFIERS
WO: 92503658
[11 In the AM20GAX analysis for analytical batch 697477, the LC/LCSD RPD is above the control limit for Methane. All
recoveries are acceptable.
Ill QC has a methane hit in the blank but all hits in samples are at least 10x larger than the hit in Method Blank.
ANALYTE QUALIFIERS
BO Analyte was detected in an associated blank at a concentration greater than the MDL.
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
ED Due to the extract's physical characteristics, the analysis was performed at dilution.
F6 Sample was not filtered within 15 minutes of collection and does not meet sampling and/or regulatory requirements.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
R1 RPD value was outside control limits.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC. Page 92 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
NRLF
92503658
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92503658001
B-23A-110220
AM20GAX
697515
92503658002
B-23B-110220
AM20GAX
697515
92503658014
B-22A-110320
AM20GAX
697515
92503658015
B-22B-110320
AM20GAX
697515
92503658016
B-17C-110320
AM20GAX
697515
92503658017
B-17B-110320
AM20GAX
697515
92503658019
B-32B-110320
AM20GAX
697515
92503658020
B-01-110320
AM20GAX
697515
92503658021
B-10-110320
AM20GAX
697515
92503658001
B-23A-110220
AM20GAX
697358
92503658002
B-23B-110220
AM20GAX
697358
92503658014
B-22A-110320
AM20GAX
697358
92503658015
B-22B-110320
AM20GAX
697358
92503658015
B-22B-110320
AM20GAX
697477
92503658016
B-17C-110320
AM20GAX
697358
92503658017
B-17B-110320
AM20GAX
697358
92503658019
B-32B-110320
AM20GAX
697358
92503658020
B-01-110320
AM20GAX
697069
92503658020
B-01-110320
AM20GAX
697207
92503658021
B-10-110320
AM20GAX
697069
92503658021
B-10-110320
AM20GAX
697207
92503658001
B-23A-110220
EPA 8015 Alcohol -Glycol
591658
92503658002
B-23B-110220
EPA 8015 Alcohol -Glycol
591658
92503658006
B-09C-110220
EPA 8015 Alcohol -Glycol
591658
92503658008
SW-7-110220
EPA 8015 Alcohol -Glycol
591908
92503658009
SW-5-110220
EPA 8015 Alcohol -Glycol
591908
92503658010
SW-3-110220
EPA 8015 Alcohol -Glycol
591908
92503658011
SW-8-110220
EPA 8015 Alcohol -Glycol
592184
92503658019
B-32B-110320
EPA 8015 Alcohol -Glycol
592184
92503658020
B-01-110320
EPA 8015 Alcohol -Glycol
592184
92503658021
B-10-110320
EPA 8015 Alcohol -Glycol
591658
92503658001
B-23A-110220
RSK-175
697027
92503658002
B-23B-110220
RSK-175
697027
92503658014
B-22A-110320
RSK-175
697246
92503658015
B-22B-110320
RSK-175
697246
92503658016
B-17C-110320
RSK-175
697246
92503658017
B-17B-110320
RSK-175
697246
92503658019
B-32B-110320
RSK-175
697246
92503658020
B-01-110320
RSK-175
697246
92503658021
B-10-110320
RSK-175
697246
92503658001
B-23A-110220
EPA 3510C
578132 EPA 8270E
578384
92503658002
B-23B-110220
EPA 3510C
578132 EPA 8270E
578384
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except
in full,
Date: 11 /19/2020 04:25
PM
without the written consent of Pace Analytical Services, LLC.
Page 93 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
NRLF
92503658
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92503658003
B-24B-110220
EPA 3510C
578132
EPA 8270E
578384
92503658004
B-24A-110220
EPA 3510C
578132
EPA 8270E
578384
92503658006
B-09C-110220
EPA 3510C
578132
EPA 8270E
578384
92503658007
B-99C-110220
EPA 3510C
578132
EPA 8270E
578384
92503658008
SW-7-110220
EPA 3510C
578132
EPA 8270E
578384
92503658009
SW-5-110220
EPA 3510C
578463
EPA 8270E
578603
92503658010
SW-3-110220
EPA 3510C
578463
EPA 8270E
578603
92503658011
SW-8-110220
EPA 3510C
578463
EPA 8270E
578603
92503658014
B-22A-110320
EPA 3510C
578463
EPA 8270E
578603
92503658015
B-22B-110320
EPA 3510C
578463
EPA 8270E
578603
92503658016
B-17C-110320
EPA 3510C
578463
EPA 8270E
578603
92503658017
B-17B-110320
EPA 3510C
578463
EPA 8270E
578603
92503658018
B-12-110320
EPA 3510C
578463
EPA 8270E
578603
92503658019
B-32B-110320
EPA 3510C
578463
EPA 8270E
578603
92503658020
B-01-110320
EPA 3510C
578463
EPA 8270E
578603
92503658021
B-10-110320
EPA 3510C
578463
EPA 8270E
578603
92503658001
B-23A-110220
EPA 8260D
577978
92503658002
B-23B-110220
EPA 8260D
577978
92503658003
B-24B-110220
EPA 8260D
577974
92503658004
B-24A-110220
EPA 8260D
577978
92503658006
B-09C-110220
EPA 8260D
577978
92503658007
B-99C-110220
EPA 8260D
577978
92503658014
B-22A-110320
EPA 8260D
577978
92503658015
B-22B-110320
EPA 8260D
577978
92503658020
B-01-110320
EPA 8260D
578305
92503658021
B-10-110320
EPA 8260D
578368
92503658001
B-23A-110220
EPA 8260D Mod.
577993
92503658002
B-23B-110220
EPA 8260D Mod.
577993
92503658003
B-24B-110220
EPA 8260D Mod.
577993
92503658004
B-24A-110220
EPA 8260D Mod.
577993
92503658005
B-21 B-110220
EPA 8260D Mod.
577993
92503658006
B-09C-110220
EPA 8260D Mod.
577993
92503658007
B-99C-110220
EPA 8260D Mod.
577993
92503658008
SW-7-110220
EPA 8260D Mod.
577993
92503658009
SW-5-110220
EPA 8260D Mod.
577993
92503658010
SW-3-110220
EPA 8260D Mod.
577993
92503658011
SW-8-110220
EPA 8260D Mod.
577993
92503658012
CSW-1-110220
EPA 8260D Mod.
577993
92503658013
CSW-2-110220
EPA 8260D Mod.
578204
92503658014
B-22A-110320
EPA 8260D Mod.
577993
92503658015
B-22B-110320
EPA 8260D Mod.
577993
92503658016
B-17C-110320
EPA 8260D Mod.
577993
92503658017
B-17B-110320
EPA 8260D Mod.
578204
92503658018
B-12-110320
EPA 8260D Mod.
578204
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 11 /19/2020 04:25
PM
without the written consent of Pace Analytical Services, LLC.
Page 94 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NRLF
Pace Project No.: 92503658
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92503658019
B-32B-110320
EPA 8260D Mod.
577993
92503658020
B-01-110320
EPA 8260D Mod.
578313
92503658021
B-10-110320
EPA 8260D Mod.
578313
92503658001
B-23A-110220
SM 2320B-2011
579479
92503658002
B-23B-110220
SM 2320B-2011
579479
92503658003
B-24B-110220
SM 2320B-2011
579479
92503658004
B-24A-110220
SM 2320B-2011
579479
92503658005
B-21B-110220
SM 2320B-2011
579479
92503658006
B-09C-110220
SM 2320B-2011
579479
92503658014
B-22A-110320
SM 2320B-2011
579479
92503658015
B-22B-110320
SM 2320B-2011
579479
92503658016
B-17C-110320
SM 2320B-2011
579479
92503658017
B-17B-110320
SM 2320B-2011
579479
92503658018
B-12-110320
SM 2320B-2011
579479
92503658019
B-32B-110320
SM 2320B-2011
579481
92503658020
B-01-110320
SM 2320B-2011
579481
92503658021
B-10-110320
SM 2320B-2011
579481
92503658001
B-23A-110220
EPA 353.2 Rev 2.0 1993
577740
92503658002
B-23B-110220
EPA 353.2 Rev 2.0 1993
577740
92503658003
B-24B-110220
EPA 353.2 Rev 2.0 1993
577740
92503658004
B-24A-110220
EPA 353.2 Rev 2.0 1993
577740
92503658005
B-21 B-110220
EPA 353.2 Rev 2.0 1993
577740
92503658006
B-09C-110220
EPA 353.2 Rev 2.0 1993
577740
92503658014
B-22A-110320
EPA 353.2 Rev 2.0 1993
577740
92503658015
B-22B-110320
EPA 353.2 Rev 2.0 1993
577740
92503658016
B-17C-110320
EPA 353.2 Rev 2.0 1993
577740
92503658017
B-17B-110320
EPA 353.2 Rev 2.0 1993
577740
92503658018
B-12-110320
EPA 353.2 Rev 2.0 1993
577740
92503658019
B-32B-110320
EPA 353.2 Rev 2.0 1993
577740
92503658020
B-01-110320
EPA 353.2 Rev 2.0 1993
578222
92503658021
B-10-110320
EPA 353.2 Rev 2.0 1993
578222
92503658001
B-23A-110220
SM 4500-P E-2011
577790
92503658002
B-23B-110220
SM 4500-P E-2011
577790
92503658003
B-24B-110220
SM 4500-P E-2011
577790
92503658004
B-24A-110220
SM 4500-P E-2011
577790
92503658005
B-21B-110220
SM 4500-P E-2011
577790
92503658006
B-09C-110220
SM 4500-P E-2011
577790
92503658014
B-22A-110320
SM 4500-P E-2011
577790
92503658015
B-22B-110320
SM 4500-P E-2011
577790
92503658016
B-17C-110320
SM 4500-P E-2011
577790
92503658017
B-17B-110320
SM 4500-P E-2011
577790
92503658018
B-12-110320
SM 4500-P E-2011
577790
92503658019
B-32B-110320
SM 4500-P E-2011
577790
92503658020
B-01-110320
SM 4500-P E-2011
578202
92503658021
B-10-110320
SM 4500-P E-2011
578202
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2020 04:25 PM without the written consent of Pace Analytical Services, LLC. Page 95 of 104

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NRLF
Pace Project No.: 92503658
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92503658001
B-23A-110220
EPA 9056A
578170
92503658002
B-23B-110220
EPA 9056A
578170
92503658003
B-24B-110220
EPA 9056A
578170
92503658004
B-24A-110220
EPA 9056A
578170
92503658005
B-21B-110220
EPA 9056A
578170
92503658006
B-09C-110220
EPA 9056A
578170
92503658014
B-22A-110320
EPA 9056A
578170
92503658015
B-22B-110320
EPA 9056A
578170
92503658016
B-17C-110320
EPA 9056A
578170
92503658017
B-17B-110320
EPA 9056A
578170
92503658018
B-12-110320
EPA 9056A
578170
92503658019
B-32B-110320
EPA 9056A
578170
92503658020
B-01-110320
EPA 9056A
578495
92503658021
B-10-110320
EPA 9056A
578495
92503658001
B-23A-110220
EPA 9060A
580000
92503658002
B-23B-110220
EPA 9060A
580000
92503658014
B-22A-110320
EPA 9060A
580000
92503658015
B-22B-110320
EPA 9060A
580000
92503658016
B-17C-110320
EPA 9060A
580000
92503658017
B-17B-110320
EPA 9060A
580000
92503658019
B-32B-110320
EPA 9060A
580000
92503658020
B-01-110320
EPA 9060A
580000
92503658021
B-10-110320
EPA 9060A
580000
92503658001
B-23A-110220
AM23G
697678
92503658002
B-23B-110220
AM23G
697678
92503658014
B-22A-110320
AM23G
696989
92503658015
B-22B-110320
AM23G
696989
92503658016
B-17C-110320
AM23G
696989
92503658017
B-17B-110320
AM23G
696989
92503658019
B-32B-110320
AM23G
696989
92503658020
B-01-110320
AM23G
696989
92503658021
B-10-110320
AM23G
696989
Date: 11/19/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 96 of 104

Document Name:
Document Revised: October 28, 2020
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
1�
i c?GeAnaI34ical DocumentNa.:
Issuing Authority:
F-CAR-CS-033-Rev.07
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville [ Raleigh[]
Mechanicsville❑ Atlanta❑ Kernersville❑
Sample Condition Client Name:
Project
WV# : 92503658
p. Receipt
EcO A+}e
;
Courier: ❑FUPS ❑Client
1111111111111111111111
❑ commercial ace ❑Othr:
92503658
Custody Seal Present? ❑Yes No Seals Intact? ❑Yes B10
Dale/Initials Person Examining Contents. I f f3 A-C,
Packing Material: Bubble Wrap ubbie Bags ❑None Other
Biological Tissue Fr n?
Thermometer et ❑Blue
❑Yes ONO N/A
❑None
IR Gun ID: 92TO61 Type of Ice:
Correction Factor:
Cooler Temp: Add/Subtract ('C) 0.0
Temp should be above freezing to 6°C
�1
L.-
❑samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected i°C`
has begun
USDA Regulated Soil ( NIA, water sample)
g
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
Did samples originate From a foreign source {internationally,
inel—linaWnwaii and PuprM RirnP MYPS FINo
Comments/Discrepancy: .
Chain of Custody Present?
es
No
❑NIA
1.
Sam les Arrived within Hold Time?
Yes
❑No
N/A
2•
Short Hold Time Analysis (02 hr.)?
❑Yes
o
N/A
3.
Rush Turn Around Time Requested?
Yes
No
❑N/A
4.
Sufficient Volume?
lqoYes
[-]NO
[]N/A
S.
Correct Containers Used?
-Pace Containers Used?
R<
es
[]No
No
❑NIA
❑NIA
6.
Containers Intact?
Yes
[]No .,,
-[]N/A
7.
Dissolved analysis: Samples Field Filtered?
❑v
Co
❑NIA
8.
Sample Labels Match COC?
-Includes Date/Time/1D/Analysis Matrix:
Yes
[:]No
[-]N/A
9.
Headspace in VOA Vials >5-6mm)?
❑yes
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
o
OKI,
❑N/A
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY
SfIO1 n110_ -10 ?� R
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
01
Date/Time:
Lot ID of split containers:
Date:
Date:
Field Data Required? []Yes ❑No
Page 97 of 104

Analytical A
Document Name:
Sample Condition Upon Recei
Document No.:
F-CAR-CS-033-Rev.07
Document Revised: October 28, 2020
_ Page 2 of 2
Issuing Authority:
Pace Carolinas duality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions; VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottles
Project # �WQ# : 92543658
P
� PM: KRG Due Dale: 11/12/20
CLIENT: 97-CNA
2
U
0
a
v
u
=
�
z
Z
a
a
o
z
z
Z
Q
V
ry
N
I
y
C
z
G
v
`
z
O
Mcc
I
47
is
is
N
f'
01
V
=
V
=
2
=
=
N
�
;"
aV
N
2
2
Y
x
Z
Q
?
Y
Q
q
Z
Cl
_
9J
v
`G
@
-a+
�
V
H
`7.
Z
�
�[
�
Z
�
�
rC
N
Iz
7
a
7
ii
v
C-
N
0
z
Q
z
0
'�
c
-_
u
0
0
ry
z
4
z
0
w
?
a
v
ii
o
w
@
a
=
z
c
0
c
•�
a
j
r
d
a
a
/o
Q
"
a
E
E
4
d
�
O
p
O
O
c.
e
N
in
a
Q
U
C
J
E
J
E
J
E
O-
O.
J
E
-1
E
d
J
E
J
E
E
v
Q
v
¢
iu
�,
E
`a
E
,
m
>
E
>
-'
E
>
E
>
E
n
f 0
a
�°
J
£
J
E
--I
E
Ln
E
E
IN-1
N
Ln
,°!
I -I
�
pN
N
eN-0
Ln
ri
—
}
�
eq
rl
o
N
=
�.:1
!off
N
�
V
�
�
�
�
>
v
ei
N
o
In
E
M
N
.�i
M
IN IN
6
ei
2
N
r"
tl'I
I"1
14
M
M
n1
T
GI
T
l7
0
0
UI
N
N
I
M
�7
M
C7
_
0)
0.
0.
�.
0.
a
a
d
l7
a
C7
Q
U'
Q
19
a
l7
a
t'�
Q
l7
c
l7
>
C7
>
O
>
>
>
In
vi
m
4
4
s71
7
O
m
m
m
m
I.
m
m
m
1N,
2-1
\\I
6
3
Z
�2—L
N\\\�
4
N2
3
g
2
5
2-
6
I
2
Z—
e
3
9
2-
10
N
\\3
��
11
3
12
pH Adjustment Log for Preserved Samples
Sample iD
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
Amount of Preservative
Lot q
adjusted
added
Note: Whenever there is a discrepancy atrecting Noun Larouna compuance sdIIIIJI a, c LL,Ny VI LI 113 1UI III YYIII MV aC 11L LV LI It IwmI L-dI V1111tl VLIl1YR bCl LIIIWLIUII V-- kh G•
Out of hold, incorrect preservative, out of ternp, incorrect containers.
Page 98 of 104

hd� a
c7CBl�fl8ij�1Cc7�
Document Name:
Sample Condition Upon Recel t SCURI
Document Revised: February 7, 2018
Page 1 of 2
Document No.:
Issuing Authority:
..Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination Is Project # + �O ���03658
verified and within the acceptance range for preservation III
samples. Pfl: KRG Due Date: 11/12/20
Exceptions: VOA, Conform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHS CLIENT • 97-CNA
"*Bottom half of box Is to list number of bottle
1
u
_
_
U
1
2
?
T
N
.Z_..
z
za
Z
n
a
Z
q
a�!
Q
d
a
W
L
.4.
Y
ai
c
u�
c
c
3i
Z
O
to
a
Z
CA
2
$
7
7y
7
a
=
Z
V
�,
u
=
5
e
7
y
it
Y
'CN
+a
•P
.N
H
�^
'N
5
a
o
N
aE
E
9,
�.
L
EE
o
Z
p
d
.0
°
E
a
d
a
E
E
E
E
E
c
d
E
E
E
E
E
>7
E
E
E
8
E
E
y�
N
N
YOI
in
O
IA
�
1Q/�
^
N
LL��
S
L
N
Ln
N
-1
N
Q
N
NI
IV
ry
a
r1
,rNi,
�r71
84
CJ
$
m
m
3
4
a
O
S
?
a°d
m
m
1
�
2I'\\\
\N\J�\NZ
2
1
.3
2—
rr
evi
Z1
N�Nl
S
2
N\
�s
j
7\[\
2
2-1
2-
3
33
9-1
NN
I
A
\\\d
\N1
pH Adjustment Log for Preserved Samples
Sample 10 Type of Preservative pH upon receipt Dote preservation adjusted Time preservation Amount of Preservative Lot p
edJwted added
•_ t___ ...rrr s...__�...,._
s,��s. r..�ss.,. n[unsn rnwiR�reHww
Af4ire li e
Note: whenever there is a discrepancy affecting North Carolina comPciance 3dmpieb, a ,.Uwr U, �r"� •� ^ • �_ �_•�_ 1^= �� • • ��
Out of hold, incorrect preservative, out of temp, Incorrect containers.
Page 99 of 104

ITEM #
'3
01
(P
CL
'aPxa0
(A
(A
W
C
o
1 P
N
0
wow A
3 3
S CD
rn
0
CP
9 0
Cr
z
-n
m
0 ;U x
93
3 0
T
a
MATRIXCODE (see valid codes to left)
lip
SAMPLETYPE (G=rRAB C=CIOMP)
z
m
0
0
G)
M
M
;a
m
m
z
m
k
Z4
E
'U
V
M
rn
I
I
SAMPLE TEMP AT COLLECTION
OF CONTAINERS
8
9) or
FP
0
3 2.
3. 0
M
' n
IM
MQJ
kA
0)
VI
Unpmearved
H2SO4
HNO3
HCI
CD
0
.7,-
r '
tJ�
V3
luo
U'j
-G-
y
'j
k
NaOH
Al"34Sri
LY
;3
Other
V') I t,4 k,3 W JU4 1
8260 SIM 1,4-Dioxane
3
�J
4aP
8270 COW Therm A
"Q
UJ
Ethylene Glycol
M
(OPT
826D
n
Alkalinity, Sulfate
Nitrate (48 hr)
Orthophosphate (48 hr)
"9
Ul
TOC
MIE/E, CO2
Hydrogen
N
Acetic Acid AM23G
TEMP in G
--------
Residual Chlorine (Y/N)
z
rs
Received on
tee
(Y)N)
A
0
Sealed
Cooler
(YIN )
V�
V\
Samples
Intact
I
!
1R3
(YIN)
,
Page 100 of 104

;U
-0 m
0
ITEM #
C
D
C
N
>
m
8
0
ED
0
-;ji
z
m
R
?c
k5
�*V
MATRIX CODE (see valid codes to left)
z
N
SAMPLE TYPE (G-GRAB C=GOMP)
X
0
m
Ln
m
z
z
m
m
m
m
z
Zi
m
rn
m
9
ON
SAMPLE TEMP AT COLLECTION
tO
era
# Or CONTAINERS
3
U1
Unpresery ed
I
-U
A
A
N,
H2SO4
0
HNO3
R 3
HCI
m-fD
NaOH
a)
Ui
w
U13
3
ID
to
s.
Id
Q')
V%�
Uj
..Vj
o
~,—ALQ% .. lkc lj
V
Other L
4 J
W Vi LN 1A
826C SIM 1,4-Dioxene
NJ
8270 DOW Therm A
m
w
Ethylene Glycol
to
8260
A
AlkWinily, Sulfate
ar:
HUH
Nitrate (48 hrJ
Orthophosphate (48 hr)
—V,- ji,
TOC
En
MOE, CO2
Hydrcgon
Q,
AcstIcAcIcIAM23G
A�
TEMP in C
r
---------
Residual Chlorine (YIN
Received an
f
Z
0
r
Si
ice
(YIN)
V11
75-8-to-CFY
Sealed
Cooler
(YIN)
Samples
(YIN)
:!'- " (:`' Page 101 of 104

Document Name: Document Revised: October 28, 2020
Condition Upon Receipt(SCUR) Page 1 of 2
Document No.: Issuing Authority:
F-CAR-CS-033-Rey.07 Pace Carolinas Quality Office
Laboratory receiving samples;
Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Raleigh;9 Mechanicsville❑ Atlanta❑ Kernersville❑
Condition Upon Receipt Client Name: �Project I!:WO# : 92503658
Courier: QFed Ex ❑UPS USPS []Client PM: KRG Due Date; 11/12/20
El Commercial ❑Other: Commercial CLIENT: 97-CNA
Custody Seal Present? Dyes Nlo Seals Intact? ❑Yes rlo
Lzli
Packing Material: ❑Bubble Wrap t9Aubble Bags XNone
Thermometer:
(R Gun ID: 9et
-j O65 Type of Ice:
Correcto or:
GoolerTemp; �� Ad ubtract C)
Date/Initials Person Examining Contents:W D
Other Biological Tissue �rozen?
[]Yes ❑No III "T �V/A
❑Blue []None
Temp should be above freezing to 6°C
Cooler Temp Corrected (°C). f _ ❑Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil (,93)N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
❑Yes [:]No
including Hawaii and Puerto Rico)? nYes hlNn
Chain of Custody Present?
Samples Arrived within Hold Time?
Short Hold Time Analysis {<72 hr.)?
Rush Turn Around Time Requested?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis: Samples Field Filtered?
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis
Headspace in VOA Vials (>S-6mm)?
Trip Blank Present?
Trip Blank Custody Seals Present?
COMMENTS/SAMPLE DISCREPANCY
LJNo
LJI
❑ND
❑❑No
❑9M-
❑
❑No
❑N/A
5.
[:]No
❑N/A
6.
_KYes j_JNo ❑N/A 7,
)! s []No ❑N/A 8.
Mc res ❑No ❑N/A 9.
LUyes No LIN/A 1 10.
❑Yes ❑No ,®N/A 11.
CLIENT NOTIFICATION/RESOLUTION Lot !D of split containers:
Person contacted:
Date/Time:
Field Data Required? ❑Yes ❑No
Project Manager SCURF Review: Date.:
Project Manager SRF Review: Page 102 of 104
Date;

Document Name:
aCBAnalytical' sampie Condition Upon Recei
s 1 Document No.:
F-CAR-CS-033-Rev.07
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottles
21
n Q
z z z ¢ m �' Q z
z N N Z 'a N Z
V V 06 A � y N V �
Z
2 x
Q. a. .M `V a xe. z
m a
a m o O ¢ a a CL v 0 -0
G N z Z O 0 in N E
U U U = U U Z v �. i .¢_I
mIntl IyV' N W j d W A
w m E E o
E E E E a a a N
Ln a 0 °f E E E „w m E `m E Q
r1 N In e-I Ln N N N c-I ri N O 0
E N
p,+ a a a a a a a a a a 4 Q
m off m m m m m R Q
1 �
2
�
3
4
5
6
7�
8
9
10
11
12
Document Revised: October 28, 2o20
Page 2 of 2
Issuing Authority:
Pace Carolinas Quality mffice
Project I WO# : 92503658
PM: KRG Due Dale: 11/12/20
CLIENT: 97-CNA
z
�
`
Z
x
zv
z
m
0
z
p
>
E
d'
>
Q
Z
>
E
4
>
�
z
d'
O
p
>
E
i#
fl
z
Y
en
r�1
`m
a
.4
"'
7
0
Y
a
a
0F
R
M
3
v
n
E
Fq
ai
ca
•''
v
n
E
Ln N
#A
A%
`�s
V
\
��U�
�
C.
N
N
c
a
E
�
en
m
w
a
2
71
Q7
`y
E
Q
O
0
¢
z
m
G
c
NLM .
>
Z
y
N
a
E
G
33
r
PH Adjustment Log for Preserved Samples
Sample in Type of Preservative pH upon receipt Date preservation adjusted Tigd
Amount of Preservative Lot #
added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this fororth Carolina r]EHNR Certification Office {i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 103 of 104

21
HE
I? 'a
w
-U m
0v.
3
oil
1" #4
P�,'
ITEM
r
j.
>
c
CD
N
0
U
0
cc
>
m
-0
&
C, W
M
(D
Cj
CD
h y
n
0) V
3
'n
z
m
2 �4 2. T m?
0
-U
ao
-V
CD
CD
0
I
I
P
I
I
I
0
R a
MATRIKOODE (see valid codes to left)
M
o
SAMPLETYPE (Q.-GRAB C=COMP)
E-n
m
D
Cn
V
Ali!
M
m
z
z
z
ir
T
m
m
rn
z
all
m
t
-SAMPLE TEMP AT COLLECTION
w
ib 0a
0
# OF CONTAINERS
—A
3 3 or.
Unpreserved
A
H2SO4
z 0
w F
HNO3
it
3
HCI
CD
Na0H
w
NNN@98 A 0
ID
rn
V'j
A d
Othar%Ak
VA
Y4
W
W
8260 SIM 1,4-Dioxane
8270 DOW Therm A
m
w
Lu
Ethylene Glycol
8260
Alkalinity, Sulfate
Nitrate (48 hr)
Iza
Orthophosphate (48 hr)
-Y
0
TOC
V)
MUE, CO2
Hydrogen
Acetic Acid AM23G
M&
TEMP in G
p
Residual Chlorine (YIN)
Received on
ra
ice
(YIN)
VVTUSIOCTY
Sealed
Cooler
/N
V\
Samples
Intact
ry
(YIN}
Q v
N Page 104 of 104

AECOM
Memorandum
AECOM
One Midtown Plaza
1360 Peachtree St. N.E.
Suite 500
Atlanta, GA 30309
To Jing Zhou — AECOM Atlanta
CC
Subject Level 2 Data Validation for Needmore Road Landfill
From Robert Davis — AECOM Atlanta
Date September 3, 2020
404.965.9600
404.965.9605
Page
tel
fax
1 of 5
Limited validation of the analytical data for the water samples was performed on one data package
received from Pace Analytical Services, Inc. in Greenwood, South Carolina. The samples were
collected on May 18, 2020, at the Needmore Road Landfill in North Carolina.
The data were reviewed for conformance to method specifications and the project guidance
document: Supplemental Characterization and Long -Term Monitoring (AECOM, July 2010 Revision
2). Data qualifiers were applied in accordance with the validation criteria set forth in USEPA
Contract Laboratory Program (CLP) National Functional Guidelines for Organic Superfund Methods
Data Review, EPA-540-R-2017-002, January 2017 and USEPA Contract Laboratory Program
National Functional Guidelines for Inorganic Superfund Methods Data Review, EPA-540-R-2017-
001, January 2017, as they apply to the analytical methods employed.
Field duplicate relative percent difference (RPD) review and applicable control limits were taken
from the USEPA Region I, New England Data Validation Functional Guidelines for Evaluating
Environmental Analyses, December 1996.
The following methods were requested on the chain -of -custody (COC) records:
• Method 8260D SIM — Volatiles by Gas Chromatography/Mass Spectrometry (GC/MS) in
SIM mode;
• Method 8270E — Semivolatiles by GC/MS;
• Method 8015M — Ethylene Glycol by GC;
• Method 2320B — Alkalinity;
• Method 353.2 — Nitrate and Nitrite;
• SM450OP-E — Orthophosphate; and
• Method 9056A — Sulfate by Ion Chromatography (IC).

AECOM
2
REVIEW ELEMENTS
Sample data were reviewed for the following quality control (QC) parameters:
• Agreement of analyses conducted with COC requests;
• Holding times and sample preservation;
• GC/MS hardware tunes, initial and continuing calibrations;
• Method blanks/trip blanks;
• Surrogate recoveries;
• Laboratory control sample (LCS) recoveries;
• Matrix spike/matrix spike duplicate (MS/MSD) recoveries; and
• Field duplicate precision results.
Samples
Environmental Field Management (EFM) personnel collected the following water samples from the
Needmore Road Landfill in North Carolina, as reported under the Pace Analytical Services, Inc. job
number:
92478230
Lab ID
Sample ID
Lab ID
Sample ID
92478230001
B-01-051820
92478230007
B-23A-051820
92478230002
B-09C-051820
92478230008
B-2313-051820
92478230003
B-10-051820
92478230009
B-24A-051820
92478230004
B-12-051820
92478230010
SW-5-051820
92478230005
B-17C-051820
92478230011
CSW-1-051820
92478230006
B-2213-051820
92478230012
B-99-051820
ANALYTICAL RESULTS
In general, the data results are valid as reported and may be used for decision -making purposes.
Sample data were qualified with either "J" (estimated) or "UX (the analyte was not detected;
however, the reporting limit is approximate and may be inaccurate or imprecise). See Table 1.
DISCUSSION
Agreement of Analyses Conducted with Chain -of -Custody Requests
Sample reports were checked to verify agreement with the COC request. No discrepancies were
noted.
Holding Times and Sample Preservation
All samples were analyzed within the holding times required by the methods.
All coolers were received within the optimal range of 4±2 degrees Celsius (°C).
All samples were properly preserved as specified by the methods.

AECOM
GUMS Tunes, Initial and Continuing Calibrations
GC/MS tuning and calibration summaries were not submitted for validation in this Level II data
package.
Method Blanks/Trip Blanks
No analytes were detected at concentrations exceeding the reporting limits for the method blanks.
Trip blanks were not submitted with sample set. Contamination picked up in storage or transit could
not be evaluated.
Surrogate Recoveries
The surrogate recoveries were acceptable for all analyses.
Laboratory Control Sample Recoveries
LCS recoveries for all of the analyses were within the QC limits.
Matrix Spike/Matrix Spike Duplicate Recoveries
MS/MSDs that were performed on non -project samples were not evaluated because matrix
similarity to project samples could not be assumed.
The MS/MSD recoveries on client samples were all within the advisory limits with the following
exceptions:
• Method 8260D SIM: The 1,4-dioxane MSD recovery was outside of the QC limits biased
low in sample B-12-051820. The 1,4-dioxane result in sample B-12-051820 was qualified.
See Table 1.
• Method 353.2: The nitrate and nitrite MS/MSD recoveries were outside of the QC limits
biased low in sample B-23A-051820. The nitrate and nitrite results in sample
B-23A-051820 were qualified. See Table 1.
• Method 353.2: The nitrate MS/MSD recoveries were outside of the QC limits biased low in
sample B-10-051820. The nitrate result in sample B-10-051820 was qualified. See
Table 1.
Field Duplicate Precision Results
A field duplicate was collected on sample B-10-051820. See Table 2 for the calculated RPDs for all
compounds for which there were detections. The RPDs between the original and field duplicate
results that were outside the acceptance criteria of 0-30% are in bold text in Table 2 and qualified in
Table 1.

AECOM
Table 1
Qualified Analytical Data
Sample ID
Method
Analyte
Lab
Result
Lab
Qual
Validated
Result
Validation
Qualifier'
Units
Reason
Codes'
B-10-051820
8270E
Biphenyl
71.1
71.1
J
pg/L
FD
B-10-051820
8270E
Diphenyl ether
643
643
J
pg/L
FD
B-10-051820
SM450OP-E
Orthophosphate
0.17
0.17
J
mg/L
FD
B-10-051820
353.2
Nitrate
ND
0.040
UJ
mg/L
MS
B-12-051020
8260D SIM
1,4-Dioxane
2130
2130
J
pg/L
MS
B-23A-051820
353.2
Nitrate
ND
0.040
UJ
mg/L
MS
B-23A-051820
353.2
Nitrite
0.041
0.041
J-
mg/L
MS
B-99-051820
8270E
Biphenyl
113
113
J
pg/L
FD
B-99-051820
8270E
Diphenyl ether
1010
1010
J
pg/L
FD
B-99-051820
SM450OP-E
Orthophosphate
0.39
0.39
J
mg/L
FD
Notes:
pg/L: micrograms per liter
mg/L: milligrams per liter
ND: not detected
': USEPA-defined data validation qualifiers applied in this data evaluation:
J: The associated numerical value is the approximate concentration of the compound in the sample.
J-: The associated numerical value is the approximate concentration of the compound in the sample biased low.
UJ: The analyte was not detected; however, the reported quantitation limit is approximated and may be inaccurate or
imprecise.
2: Reason Codes:
FD: The % RPD was outside of the QC limits.
MS: The matrix spike recovery was outside of the advisory limits.

AECOM
Table 2
Field Precision
Method
Compound
B-10-051820
I B-99-051820
Units
% RPD
8270E
Biphenyl
71.1
113
pg/L
46
8270E
Diphenyl ether
643
1010
pg/L
44
8260D
1,4-Dioxane
219
179
pg/L
20
2320B
Alkalinity
410
512
mg/L
22
353.2
Nitrite
0.076
0.078
mg/L
2.6
SM4500P-E
Orthophosphate
0.17
0.39
mg/L
79
Notes:
% RPD: Relative percent difference between the primary sample result and the sample duplicate result.
pg/L: micrograms per liter
Bold text indicates RPDs between original and field duplicate results were outside acceptance criteria of 0-30%.

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
May 28, 2020
Jing Zhou
AECOM
1000 Abernathy Road
Building 400, Suite 900
Atlanta, GA 30328
RE: Project: NRLF
Pace Project No.: 92478230
Dear Jing Zhou:
Enclosed are the analytical results for sample(s) received by the laboratory on May 19, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Indianapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
1(704)875-9092
Project Manager
Enclosures
cc: Rob Davis, AECOM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
Project: NRLF
Pace Project No.: 92478230
Pace Analytical Services Indianapolis
7726 Moller Road, Indianapolis, IN 46268
Illinois Accreditation #: 200074
Indiana Drinking Water Laboratory #: C-49-06
Kansas/TNI Certification #: E-10177
Kentucky UST Agency Interest #: 80226
Kentucky WW Laboratory ID #: 98019
Michigan Drinking Water Laboratory #9050
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Ohio VAP Certified Laboratory #: CL0065
Oklahoma Laboratory #: 9204
Texas Certification #: T104704355
West Virginia Certification #: 330
Wisconsin Laboratory #: 999788130
USDA Soil Permit #: P330-19-00257
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
NRLF
92478230
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92478230001
B-01-051820
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
LMS1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92478230002
B-09C-051820
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
LMS1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92478230003
B-10-051820
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
LMS1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92478230004
B-12-051820
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
LMS1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92478230005
B-17C-051820
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
LMS1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92478230006
13-2213-051820
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
LMS1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92478230007
B-23A-051820
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8260D Mod.
LMB
3
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
SAMPLE ANALYTE COUNT
Project: NRLF
Pace Project No.: 92478230
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
LMS1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92478230008
13-2313-051820
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
LMS1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92478230009
B-24A-051820
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
LMS1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
92478230010
SW-5-051820
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
92478230011
CSW-1-051820
EPA 8260DMod.
LMB
3
PASI-C
92478230012
B-99-051820
EPA 8015 Alcohol -Glycol
CPH
1
PASI-I
EPA 8270E
PKS
5
PASI-C
EPA 8260D Mod.
LMB
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
LMS1
1
PASI-A
EPA 9056A
CDC
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-I = Pace Analytical Services - Indianapolis
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92478230
Sample: B-01-051820
Lab ID: 92478230001 Collected: 05/18/20
15:12
Received: 05/19/20 08:10 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
05/22/20 17:39
107-21-1
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
1510 ug/L 50.0
25
05/22/20 06:57
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
122 % 50-150
25
05/22/20 06:57
17060-07-0
Toluene-d8(S)
118 % 50-150
25
05/22/20 06:57
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
1390 mg/L 5.0
1
05/26/20 16:21
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L 0.040
1
05/20/20 01:07
14797-55-8
Nitrogen, Nitrite
0.19 mg/L 0.040
1
05/20/20 01:07
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.73 mg/L 0.25
5
05/19/20 22:47
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
6.9 mg/L 1.0
1
05/20/20 20:44
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2020 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92478230
Sample: B-09C-051820
Lab ID: 92478230002 Collected: 05/18/20
14:08
Received: 05/19/20 08:10 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
05/22/20 17:14
107-21-1
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
756 ug/L 20.0
10
05/22/20 07:17
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
124 % 50-150
10
05/22/20 07:17
17060-07-0
Toluene-d8 (S)
118 % 50-150
10
05/22/20 07:17
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
2420 mg/L 5.0
1
05/26/20 17:05
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L 0.040
1
05/20/20 01:05
14797-55-8
Nitrogen, Nitrite
0.072 mg/L 0.040
1
05/20/20 01:05
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.12 mg/L 0.10
2
05/19/20 23:03
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L 1.0
1
05/20/20 20:59
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2020 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92478230
Sample: B-10-051820 Lab ID: 92478230003 Collected: 05/18/20 16:00 Received: 05/19/20 08:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L
5.0
1
05/21/20 23:30
107-21-1
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
71.1 ug/L
10.0
1
05/20/20 12:49
05/22/20 22:05
92-52-4
Diphenyl ether (Phenyl ether)
643 ug/L
100
10
05/20/20 12:49
05/23/20 16:48
101-84-8
Surrogates
Nitrobenzene-d5 (S)
70 %
13-130
1
05/20/20 12:49
05/22/20 22:05
4165-60-0
2-Fluorobiphenyl (S)
53 %
13-130
1
05/20/20 12:49
05/22/20 22:05
321-60-8
Terphenyl-d14 (S)
88 %
25-130
1
05/20/20 12:49
05/22/20 22:05
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
219 ug/L
10.0
5
05/22/20 07:37
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
123 %
50-150
5
05/22/20 07:37
17060-07-0
Toluene-d8 (S)
119 %
50-150
5
05/22/20 07:37
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
410 mg/L
5.0
1
05/26/20 17:42
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
05/20/20 01:10
14797-55-8
Nitrogen, Nitrite
0.076 mg/L
0.040
1
05/20/20 01:10
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.17 mg/L
0.10
2
05/19/20 23:03
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
05/20/20 21:15
14808-79-8
Date: 05/28/2020 05:02 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92478230
Sample: B-12-051820 Lab ID: 92478230004 Collected: 05/18/20 12:24 Received: 05/19/20 08:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
ND ug/L
10.0
1
05/20/20 12:49
05/22/20 22:30
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L
10.0
1
05/20/20 12:49
05/22/20 22:30
101-84-8
Surrogates
Nitrobenzene-d5 (S)
71 %
13-130
1
05/20/20 12:49
05/22/20 22:30
4165-60-0
2-Fluorobiphenyl (S)
51 %
13-130
1
05/20/20 12:49
05/22/20 22:30
321-60-8
Terphenyl-d14 (S)
104 %
25-130
1
05/20/20 12:49
05/22/20 22:30
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
2130 ug/L
100
50
05/22/20 07:57
123-91-1 M1
Surrogates
1,2-Dichloroethane-d4 (S)
121 %
50-150
50
05/22/20 07:57
17060-07-0
Toluene-d8(S)
116 %
50-150
50
05/22/20 07:57
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
360 mg/L
5.0
1
05/22/20 23:04
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
05/20/20 01:01
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
05/20/20 01:01
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.064 mg/L
0.050
1
05/19/20 22:40
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
1.1 mg/L
1.0
1
05/20/20 22:01
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2020 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92478230
Sample: B-17C-051820
Lab ID: 92478230005 Collected:
05/18/20
13:04
Received: 05/19/20 08:10 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
1320 ug/L
50.0
25
05/22/20 08:17
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
120 %
50-150
25
05/22/20 08:17
17060-07-0
Toluene-d8 (S)
117 %
50-150
25
05/22/20 08:17
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
367 mg/L
5.0
1
05/22/20 23:23
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
05/20/20 01:04
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
05/20/20 01:04
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.10 mg/L
0.050
1
05/19/20 22:41
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
1.2 mg/L
1.0
1
05/20/20 22:17
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2020 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92478230
Sample: 13-2213-051820
Lab ID: 92478230006 Collected:
05/18/20 11:40
Received: 05/19/20 08:10 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
1330 ug/L
40.0
20
05/22/20 08:37
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
124 %
50-150
20
05/22/20 08:37
17060-07-0
Toluene-d8 (S)
120 %
50-150
20
05/22/20 08:37
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
833 mg/L
5.0
1
05/26/20 17:51
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
05/20/20 01:00
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
05/20/20 01:00
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
ND mg/L
0.050
1
05/19/20 22:42
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
05/20/20 23:19
14808-79-8
Date: 05/28/2020 05:02 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92478230
Sample: B-23A-051820
Lab ID: 92478230007 Collected: 05/18/20 10:46
Received: 05/19/20 08:10 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 50.0
10
05/21/20 22:54
107-21-1 D3
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
2920 ug/L 100
50
05/22/20 08:57
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
129 % 50-150
50
05/22/20 08:57
17060-07-0
Toluene-d8(S)
121 % 50-150
50
05/22/20 08:57
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
3060 mg/L 5.0
1
05/26/20 18:01
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
05/20/20 00:54 14797-55-8
Nitrogen, Nitrite
0.041 mg/L
0.040
1
05/20/20 00:54 14797-65-0 M1
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.67 mg/L
0.10
2
05/19/20 23:04
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
4.6 mg/L
1.0
1
05/20/20 23:34 14808-79-8
Date: 05/28/2020 05:02 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92478230
Sample: 13-2313-051820
Lab ID: 92478230008 Collected: 05/18/20 11:30
Received: 05/19/20 08:10 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 50.0
10
05/21/20 23:40
107-21-1 D3
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
2630 ug/L 100
50
05/22/20 09:16
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
126 % 50-150
50
05/22/20 09:16
17060-07-0
Toluene-d8 (S)
120 % 50-150
50
05/22/20 09:16
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
2300 mg/L 5.0
1
05/26/20 19:10
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L 0.040
1
05/20/20 00:59
14797-55-8
Nitrogen, Nitrite
0.099 mg/L 0.040
1
05/20/20 00:59
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.54 mg/L 0.10
2
05/19/20 23:04
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
4.3 mg/L 1.0
1
05/20/20 23:50
14808-79-8
Date: 05/28/2020 05:02 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92478230
Sample: B-24A-051820
Lab ID: 92478230009 Collected:
05/18/20 10:52
Received: 05/19/20 08:10 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
162 ug/L
5.0
2.5
05/26/20 19:58
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
103 %
50-150
2.5
05/26/20 19:58
17060-07-0
Toluene-d8 (S)
101 %
50-150
2.5
05/26/20 19:58
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
347 mg/L
5.0
1
05/23/20 00:17
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
05/20/20 00:57
14797-55-8
Nitrogen, Nitrite
ND mg/L
0.040
1
05/20/20 00:57
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.11 mg/L
0.050
1
05/19/20 22:44
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
05/21/20 00:05
14808-79-8
Date: 05/28/2020 05:02 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92478230
Sample: SW-5-051820
Lab ID: 92478230010 Collected: 05/18/20
09:12
Received: 05/19/20 08:10 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L 5.0
1
05/21/20 22:11
107-21-1
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (biphenyl)
ND ug/L 10.0
1
05/20/20 12:49
05/22/20 22:56
92-52-4
Diphenyl ether (Phenyl ether)
ND ug/L 10.0
1
05/20/20 12:49
05/22/20 22:56
101-84-8
Surrogates
Nitrobenzene-d5 (S)
54 % 13-130
1
05/20/20 12:49
05/22/20 22:56
4165-60-0
2-Fluorobiphenyl (S)
35 % 13-130
1
05/20/20 12:49
05/22/20 22:56
321-60-8
Terphenyl-d14 (S)
91 % 25-130
1
05/20/20 12:49
05/22/20 22:56
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
ND ug/L 2.0
1
05/22/20 01:42
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
110 % 50-150
1
05/22/20 01:42
17060-07-0
Toluene-d8 (S)
113 % 50-150
1
05/22/20 01:42
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2020 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92478230
Sample: CSW-1-051820
Lab ID: 92478230011 Collected:
05/18/20
10:05
Received: 05/19/20 08:10 Matrix: Water
Parameters
Results Units Report
Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
580 ug/L
20.0
10
05/27/20 11:22
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
104 %
50-150
10
05/27/20 11:22
17060-07-0
Toluene-d8(S)
146 %
50-150
10
05/27/20 11:22
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2020 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
ANALYTICAL RESULTS
Project: NRLF
Pace Project No.: 92478230
Sample: B-99-051820 Lab ID: 92478230012 Collected: 05/18/20 16:10 Received: 05/19/20 08:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015M Glycols in water
Analytical Method: EPA 8015 Alcohol -Glycol
Pace Analytical Services - Indianapolis
Ethylene glycol
ND mg/L
5.0
1
05/21/20 22:22
107-21-1
8270E RVE
Analytical Method: EPA 8270E Preparation Method:
EPA 3510C
Pace Analytical Services - Charlotte
Biphenyl (Diphenyl)
113 ug/L
10.0
1
05/20/20 12:49
05/22/20 23:21
92-52-4
Diphenyl ether (Phenyl ether)
1010 ug/L
100
10
05/20/20 12:49
05/23/20 17:14
101-84-8
Surrogates
Nitrobenzene-d5 (S)
71 %
13-130
1
05/20/20 12:49
05/22/20 23:21
4165-60-0
2-Fluorobiphenyl (S)
65 %
13-130
1
05/20/20 12:49
05/22/20 23:21
321-60-8
Terphenyl-d14 (S)
88 %
25-130
1
05/20/20 12:49
05/22/20 23:21
1718-51-0
8260D MSV SIM
Analytical Method: EPA 8260D Mod.
Pace Analytical Services - Charlotte
1,4-Dioxane (p-Dioxane)
179 ug/L
10.0
5
05/22/20 10:15
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
133 %
50-150
5
05/22/20 10:15
17060-07-0
Toluene-d8 (S)
123 %
50-150
5
05/22/20 10:15
2037-26-5
2320B Alkalinity
Analytical Method: SM 2320B-2011
Pace Analytical Services -Asheville
Alkalinity, Total as CaCO3
512 mg/L
5.0
1
05/26/20 20:08
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L
0.040
1
05/20/20 01:13
14797-55-8
Nitrogen, Nitrite
0.078 mg/L
0.040
1
05/20/20 01:13
14797-65-0
SM4500P-E, Phosphate, Ortho
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
Orthophosphate as P
0.39 mg/L
0.050
1
05/19/20 22:45
9056 IC anions 28 Days
Analytical Method: EPA 9056A
Pace Analytical Services -Asheville
Sulfate
ND mg/L
1.0
1
05/21/20 00:21
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2020 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92478230
QC Batch: 563213 Analysis Method: EPA 8015 Alcohol -Glycol
QC Batch Method: EPA 8015 Alcohol -Glycol Analysis Description: EPA 8015 Modified
Laboratory: Pace Analytical Services - Indianapolis
Associated Lab Samples: 92478230001, 92478230002, 92478230003, 92478230007, 92478230008, 92478230010, 92478230012
METHOD BLANK: 2598188 Matrix: Water
Associated Lab Samples: 92478230001, 92478230002, 92478230003, 92478230007, 92478230008, 92478230010, 92478230012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Ethylene glycol mg/L ND 5.0 05/21/20 21:51
LABORATORY CONTROL SAMPLE: 2598189
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Ethylene glycol mg/L 25 28.8 115 47-167
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2598199 2598200
MS MSD
92478230010 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Ethylene glycol mg/L ND 25 25 25.3 21.9 98 85 31-179 14
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2020 05:02 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92478230
QC Batch: 542984 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92478230001, 92478230002, 92478230003, 92478230010
METHOD BLANK: 2892634
Matrix:
Water
Associated Lab Samples:
92478230001, 92478230002, 92478230003, 92478230010
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
05/22/20 00:43
1,2-Dichloroethane-d4 (S)
%
101
50-150
05/22/20 00:43
Toluene-d8 (S)
%
107
50-150
05/22/20 00:43
LABORATORY CONTROL SAMPLE: 2892635
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 17.1 86 70-130
1,2-Dichloroethane-d4 (S) % 96 50-150
Toluene-d8(S) % 102 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2892636
2892637
MS
MSD
92478230010 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 16.7
15.9 81
77
50-150 5
1,2-Dichloroethane-d4 (S)
%
132
132
50-150
Toluene-d8(S)
%
123
122
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2020 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92478230
QC Batch: 542985 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92478230004, 92478230005, 92478230006, 92478230007, 92478230008, 92478230012
METHOD BLANK: 2892638
Matrix:
Water
Associated Lab Samples:
92478230004, 92478230005, 92478230006, 92478230007, 92478230008,
92478230012
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
05/22/20 01:03
1,2-Dichloroethane-d4 (S)
%
110
50-150
05/22/20 01:03
Toluene-d8 (S)
%
115
50-150
05/22/20 01:03
LABORATORY CONTROL SAMPLE: 2892639
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 18.2 91 70-130
1,2-Dichloroethane-d4 (S) % 103 50-150
Toluene-d8(S) % 110 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2892640
2892641
MS
MSD
92478230004 Spike
Spike
MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc.
Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 2130 1000
1000
2630
2560 50
43
50-150 3 M1
1,2-Dichloroethane-d4 (S)
%
140
128
50-150
Toluene-d8(S)
%
121
122
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2020 05:02 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92478230
QC Batch: 543516 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92478230009
METHOD BLANK: 2894937
Matrix:
Water
Associated Lab Samples: 92478230009
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
05/26/20 18:19
1,2-Dichloroethane-d4 (S)
%
101
50-150
05/26/20 18:19
Toluene-d8 (S)
%
101
50-150
05/26/20 18:19
LABORATORY CONTROL SAMPLE: 2894938
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 19.4 97 70-130
1,2-Dichloroethane-d4 (S) % 101 50-150
Toluene-d8 (S) % 103 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2894939
2894940
MS
MSD
92478613001 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 20.1
20.6 100
103
50-150 2
1,2-Dichloroethane-d4 (S)
%
100
106
50-150
Toluene-d8(S)
%
103
104
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2020 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92478230
QC Batch: 543519 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92478230011
METHOD BLANK: 2894960
Matrix:
Water
Associated Lab Samples: 92478230011
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
05/27/20 03:29
1,2-Dichloroethane-d4 (S)
%
102
50-150
05/27/20 03:29
Toluene-d8 (S)
%
104
50-150
05/27/20 03:29
LABORATORY CONTROL SAMPLE: 2894961
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 20.4 102 70-130
1,2-Dichloroethane-d4 (S) % 102 50-150
Toluene-d8(S) % 102 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2894962
2894963
MS
MSD
7328261014 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 20.0 20
20 39.2
42.0 96
110
50-150 7
1,2-Dichloroethane-d4 (S)
%
104
100
50-150
Toluene-d8(S)
%
105
104
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2020 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92478230
QC Batch: 542537 Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92478230003, 92478230004, 92478230010, 92478230012
METHOD BLANK: 2890472
Matrix:
Water
Associated Lab Samples: 92478230003, 92478230004, 92478230010, 92478230012
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Biphenyl (Diphenyl)
ug/L
ND
10.0
05/21/20 03:18
Diphenyl ether (Phenyl ether)
ug/L
ND
10.0
05/21/20 03:18
2,4,6-Tribromophenol (S)
%
71
10-137
05/21/20 03:18
2-Fluorobiphenyl (S)
%
72
13-130
05/21/20 03:18
2-Fluorophenol (S)
%
62
10-130
05/21/20 03:18
Nitrobenzene-d5 (S)
%
86
13-130
05/21/20 03:18
Phenol-d6 (S)
%
48
10-130
05/21/20 03:18
Terphenyl-d14 (S)
%
94
25-130
05/21/20 03:18
LABORATORY CONTROL SAMPLE:
Parameter
2890473
Units
Spike LCS LCS
Conc. Result % Rec
% Rec
Limits Qualifiers
Biphenyl (Diphenyl)
ug/L
50 43.9 88
20-130
Diphenyl ether (Phenyl ether)
ug/L
50 44.4 89
20-130
2,4,6-Tribromophenol (S)
%
80
10-137
2-Fluorobiphenyl (S)
%
80
13-130
2-Fluorophenol(S)
%
68
10-130
Nitrobenzene-d5(S)
%
94
13-130
Phenol-d6 (S)
%
54
10-130
Terphenyl-d14 (S)
%
98
25-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2890474 2890475
Parameter
Biphenyl (Diphenyl)
Diphenyl ether (Phenyl ether)
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol(S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
MS
92471460017 Spike
Units Result Conc.
ug/L ND 50
ug/L ND 50
MSD
Spike MS
Conc. Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits RPD
50 31.8
33.3
64
67
20-130 4
50 31.4
32.9
63
66
20-130 4
89
51
10-137
62
65
13-130
52
23
10-130
76
66
13-130
40
31
10-130
119
119
25-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2020 05:02 PM without the written consent of Pace Analytical Services, LLC.
Qual
Page 22 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92478230
QC Batch: 543081 Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92478230004, 92478230005, 92478230009
METHOD BLANK: 2892906
Matrix:
Water
Associated Lab Samples: 92478230004, 92478230005, 92478230009
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Alkalinity, Total as CaCO3
mg/L
ND
5.0
05/22/20 20:50
LABORATORY CONTROL SAMPLE:
2892907
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Alkalinity, Total as CaCO3
mg/L
50
52.5
105 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2892908 2892909
MS MSD
92477714012 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 148 50 50 198 199 100 101 80-120 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2893700 2893701
MS MSD
92478704001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 13400 50 50 62.3 62.8 98 99 80-120 1
ug/L
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2020 05:02 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92478230
QC Batch: 543371 Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92478230001, 92478230002, 92478230003, 92478230006, 92478230007, 92478230008, 92478230012
METHOD BLANK: 2894118 Matrix: Water
Associated Lab Samples: 92478230001, 92478230002, 92478230003, 92478230006, 92478230007, 92478230008, 92478230012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Alkalinity, Total as CaCO3 mg/L ND 5.0 05/26/20 12:22
LABORATORY CONTROL SAMPLE: 2894119
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Alkalinity, Total as CaCO3 mg/L 50 52.5 105 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2894120 2894121
MS MSD
2632085001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 1670 50 50 1650 1640 -33 -45 80-120 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2894122 2894123
MS MSD
2632100025 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 50.8 50 50 105 106 109 111 80-120 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2020 05:02 PM without the written consent of Pace Analytical Services, LLC.
Page 24 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92478230
QC Batch: 542465 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92478230001, 92478230002, 92478230003, 92478230004, 92478230005, 92478230006, 92478230007,
92478230008,92478230009,92478230012
METHOD BLANK: 2890268 Matrix: Water
Associated Lab Samples: 92478230001, 92478230002, 92478230003, 92478230004, 92478230005, 92478230006, 92478230007,
92478230008,92478230009,92478230012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/L ND 0.040 05/20/20 00:52
Nitrogen, Nitrite mg/L ND 0.040 05/20/20 00:52
LABORATORY CONTROL SAMPLE: 2890269
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 1.5 1.5 101 90-110
Nitrogen, Nitrite mg/L 1 0.99 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2890270
2890271
MS
MSD
92478230007 Spike
Spike MS
MSD MS
MSD % Rec
Parameter
Units
Result Conc.
Conc. Result
Result % Rec
% Rec Limits RPD Qual
Nitrogen, Nitrate
mg/L
ND 1.5
1.5 1.2
1.2 82
82 90-110 1
Nitrogen, Nitrite
mg/L
0.041 1
1 0.93
0.91 88
87 90-110 2 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2890272
2890273
MS
MSD
92478230003 Spike
Spike MS
MSD MS MSD % Rec
Parameter
Units
Result Conc.
Conc. Result
Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate
mg/L
ND 1.5
1.5 1.3
1.2 84 83 90-110 0
Nitrogen, Nitrite
mg/L
0.076 1
1 1.0
1.0 92 93 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2020 05:02 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92478230
QC Batch: 542448 Analysis Method: SM 4500-P E-2011
QC Batch Method: SM 4500-P E-2011 Analysis Description: SM450OP-E Phosphorus, Ortho
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92478230001, 92478230002, 92478230003, 92478230004, 92478230005, 92478230006, 92478230007,
92478230008,92478230009,92478230012
METHOD BLANK: 2890215 Matrix: Water
Associated Lab Samples: 92478230001, 92478230002, 92478230003, 92478230004, 92478230005, 92478230006, 92478230007,
92478230008,92478230009,92478230012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Orthophosphate as P mg/L ND 0.050 05/19/20 22:20
LABORATORY CONTROL SAMPLE & LCSD: 2890216 2890217
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Orthophosphate as P mg/L 0.25 0.27 0.26 107 106 90-110 1 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2020 05:02 PM without the written consent of Pace Analytical Services, LLC.
Page 26 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA
Project: NRLF
Pace Project No.: 92478230
QC Batch: 542528 Analysis Method: EPA 9056A
QC Batch Method: EPA 9056A Analysis Description: 9056 IC anions 28 Days
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92478230001, 92478230002, 92478230003, 92478230004, 92478230005, 92478230006, 92478230007,
92478230008,92478230009,92478230012
METHOD BLANK: 2890438 Matrix: Water
Associated Lab Samples: 92478230001, 92478230002, 92478230003, 92478230004, 92478230005, 92478230006, 92478230007,
92478230008,92478230009,92478230012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfate mg/L ND 1.0 05/20/2016:51
LABORATORY CONTROL SAMPLE: 2890439
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Sulfate mg/L 50 50.0 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2890440 2890441
MS MSD
2631951001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L 10.7 50 50 62.2 62.0 103 103 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2890442 2890443
MS MSD
92478230003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg/L ND 50 50 51.5 51.7 103 103 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2020 05:02 PM without the written consent of Pace Analytical Services, LLC.
Page 27 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALIFIERS
Project: NRLF
Pace Project No.: 92478230
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/28/2020 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
NRLF
92478230
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method Batch
92478230001
B-01-051820
EPA 8015 Alcohol -Glycol
563213
92478230002
B-09C-051820
EPA 8015 Alcohol -Glycol
563213
92478230003
B-10-051820
EPA 8015 Alcohol -Glycol
563213
92478230007
B-23A-051820
EPA 8015 Alcohol -Glycol
563213
92478230008
B-23B-051820
EPA 8015 Alcohol -Glycol
563213
92478230010
SW-5-051820
EPA 8015 Alcohol -Glycol
563213
92478230012
B-99-051820
EPA 8015 Alcohol -Glycol
563213
92478230003
B-10-051820
EPA 3510C
542537
EPA 8270E 542743
92478230004
B-12-051820
EPA 3510C
542537
EPA 8270E 542743
92478230010
SW-5-051820
EPA 3510C
542537
EPA 8270E 542743
92478230012
B-99-051820
EPA 3510C
542537
EPA 8270E 542743
92478230001
B-01-051820
EPA 8260D Mod.
542984
92478230002
B-09C-051820
EPA 8260D Mod.
542984
92478230003
B-10-051820
EPA 8260D Mod.
542984
92478230004
B-12-051820
EPA 8260D Mod.
542985
92478230005
B-17C-051820
EPA 8260D Mod.
542985
92478230006
B-22B-051820
EPA 8260D Mod.
542985
92478230007
B-23A-051820
EPA 8260D Mod.
542985
92478230008
B-23B-051820
EPA 8260D Mod.
542985
92478230009
B-24A-051820
EPA 8260D Mod.
543516
92478230010
SW-5-051820
EPA 8260D Mod.
542984
92478230011
CSW-1-051820
EPA 8260D Mod.
543519
92478230012
B-99-051820
EPA 8260D Mod.
542985
92478230001
B-01-051820
SM 2320B-2011
543371
92478230002
B-09C-051820
SM 2320B-2011
543371
92478230003
B-10-051820
SM 2320B-2011
543371
92478230004
B-12-051820
SM 2320B-2011
543081
92478230005
B-17C-051820
SM 2320B-2011
543081
92478230006
B-22B-051820
SM 2320B-2011
543371
92478230007
B-23A-051820
SM 2320B-2011
543371
92478230008
B-23B-051820
SM 2320B-2011
543371
92478230009
B-24A-051820
SM 2320B-2011
543081
92478230012
B-99-051820
SM 2320B-2011
543371
92478230001
B-01-051820
EPA 353.2 Rev 2.0 1993
542465
92478230002
B-09C-051820
EPA 353.2 Rev 2.0 1993
542465
92478230003
B-10-051820
EPA 353.2 Rev 2.0 1993
542465
92478230004
B-12-051820
EPA 353.2 Rev 2.0 1993
542465
92478230005
B-17C-051820
EPA 353.2 Rev 2.0 1993
542465
92478230006
B-22B-051820
EPA 353.2 Rev 2.0 1993
542465
92478230007
B-23A-051820
EPA 353.2 Rev 2.0 1993
542465
92478230008
B-23B-051820
EPA 353.2 Rev 2.0 1993
542465
92478230009
B-24A-051820
EPA 353.2 Rev 2.0 1993
542465
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except
in full,
Date: 05/28/2020 05:02 PM
without the written consent of Pace Analytical Services, LLC.
Page 29 of 33

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
816 Durst Avenue East
Greenwood, SC 29649
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NRLF
Pace Project No.: 92478230
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92478230012
B-99-051820
EPA 353.2 Rev 2.0 1993
542465
92478230001
B-01-051820
SM 4500-P
E-2011
542448
92478230002
B-09C-051820
SM 4500-P
E-2011
542448
92478230003
B-10-051820
SM 4500-P
E-2011
542448
92478230004
B-12-051820
SM 4500-P
E-2011
542448
92478230005
B-17C-051820
SM 4500-P
E-2011
542448
92478230006
B-22B-051820
SM 4500-P
E-2011
542448
92478230007
B-23A-051820
SM 4500-P
E-2011
542448
92478230008
B-23B-051820
SM 4500-P
E-2011
542448
92478230009
B-24A-051820
SM 4500-P
E-2011
542448
92478230012
B-99-051820
SM 4500-P
E-2011
542448
92478230001
B-01-051820
EPA 9056A
542528
92478230002
B-09C-051820
EPA 9056A
542528
92478230003
B-10-051820
EPA 9056A
542528
92478230004
B-12-051820
EPA 9056A
542528
92478230005
B-17C-051820
EPA 9056A
542528
92478230006
B-22B-051820
EPA 9056A
542528
92478230007
B-23A-051820
EPA 9056A
542528
92478230008
B-23B-051820
EPA 9056A
542528
92478230009
B-24A-051820
EPA 9056A
542528
92478230012
B-99-051820
EPA 9056A
542528
Date: 05/28/2020 05:02 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
Page 30 of 33

Document Name:
Document Revised: February 7, 2018
m
/�alceAnalytical
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS•033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville E� Raleigh❑ Mechanicsville❑
Sample Condition
Upon Receipt Client Name: Project #:WQ# : 92478230
—� Courfer; ❑F d Ex []UPSUPS ❑LISPS ❑Client
❑ Commercial b ace [:]Other:_ 1111111111111111111111111
92478230
Custody Seal Present? Oyes 2]`N�, Seals intact? Oyes El to
Date/Initlals Person Examintng Contents:
Packing Material: []Bubble Wrap " Bubble Sags [-]None ❑ Other Biological Tissue Fr en?
Thermometer � [:]Yes[]NO❑N/A
92TO61 Type of Ice: E]Wet ❑Blue [:]NoneIR Gun IA: 11
Cooler Temp (°C): - �— LCorrection Factor: Add/Subtract (°Cj t0.1
I Ate'. �' % •' V � Temp should be above freezing to VCCaDler Temp Corrected ('C):� L� `X ❑Samples out of temp criteria. Samples an Ice, coaling process
has begun
USDA Regulated Soil ( N/A, water samples
Did samples origin to in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (intern onally,
Flyer rye inrl,,dinu Hawnli and Puarrn Rirnt7 FIYas Nn
Comments/Discrepancy:
Chain of Custody Present?
(Yes
❑No
❑N/A
I.
Samples Arrived wlthlr Hold Time?
Yes
No
❑N/A
2,
Short Hold Time Analysis (02 hr.)?
N/A
3,
Rush Turn Around Time Requested?
❑Yes
Cl<o
❑N/A
4.
Sufficient Volume?
= res
ON.
[]N/A
5.
Correct Containers Used?
-Pace Containers Used?
04es
dYes
[:]No
❑No
❑N/A
[]N/A
6.
Containers Intact?
-
- es
[jNo
ON/A
?.
Dissolved analysis: Samples Field Filtered? ❑Y
❑No
ENJA
R.
Samnle Labels Match COC?
We s
Nv
N A
9.
-Includes Date/Time/ID/Analysts
1l
Matrix: tJ-T-
Heads ace in VOA Vials (>S-6mm)?
❑yes
2LN.
❑ A
lo.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
[]Yes
[]No
❑No
QI(/A
COMMENTS/SAMPLE DISCREPANCY
Lot 10 of split Containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Date:
Date;
field Data Required? ❑Yes ❑No
Page 31 of 33

Document Name:
Document Revised: February 7, 2018
ti
aceArialytrcal
Sample Condjtian Upon Recellt{SCURi
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS.033-Rev.06
Pace Carolinas Quallty Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLH8
*"Bottom half of box is to list number of bottle
Project # lO# : 924782r30
PM: KRIS Due Date: 05/29/20
CLIENT: 97—CNA
w
a
m
\
a
v
v
Z
06
N
N
n
�
v
U
v
ry
v
N
V
J
_
U
a
_
C
\
2
2
H,
Y
2
I
I
4
rM
Oi
v
\
2
a
y
Z
ai
a
2
N
o.
t
a
ni
x
4
q
ry
x
a
O
i
°
4
Z
z
TO
�°
m
y
u
d
C
^�
a
4
a
7
x
O
N
a
O
2
z
4
2
?
N
2
G
pv
Y
o
Q
l7
a
?
Z
`^
vaty
G
c
N
d
n
u
A
a
_
o
a
7
d
c
,
s
=
n
J
�!
n
N
u
a
J
U
a
J
di`a
a
E
a
a
=
4
`w
E
a
E
a
E
a
J
E
o
N
z
4
Z
q
O
G
¢
ti.
S
¢
4
y
a
Y
n
�-°
6�N.
a
'
m
'A
=
m
a
a
E
¢
E
c
n
¢
E
ry
rl
7
a
E
N
M
a
E
o
t�1
>
a
a
=
ell
>
a
E
r�
"�.��
v1
a
E
z
a
E
M
r4
d
E
N
a
w
5�
3
w
ti
e+
t7
.,
.4
U
E
o
`^
m
W
m
—
ri
n
to
E
Ln
N
M
0
f
0
M
ko
E
C
�$
0�
ld7
E
a
v
7
E
o
Q1
]
E
q
Ch
0
1O
>
W
d
7
'U
5
E
N
ri
in
a.
E
vai
N
N
E
o
"�
N
eaa5
m
v
1
O
Q
E
N
>
E
O
Ol
a
.d.
m
m
m
m
as
m
m
m
a
a
a
a
a
a
vai
1
\f\
5
�
6
3
10
pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot p
Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, Incorrect containers.
Page 32 of 33

21
CL
c�
ems
C —
E
E E
U
.7 N
t1 �
fl w
N a
C1
cr
m
a, W
C
Q Q
CD
Ow
w
N S2
a
O
1 7
o
F O
ZG
Q �
= m
U�
(NlAI
}oeyul
i(NIA)
�
p
2
alBas
P%Es
m
°c(NIA)
a
6
u
sal
C
J
Z
N
Ua QahI8OB8
A
�
N
—(NIA) Buuo!yO lenp!sea
0U!dN131
i
Lao]
w
�
r
`a
M;
Q
N
4
p
(jy 9ti) e}eydsoydoyuo
x
X
X
X
X
X
X
X
X
k
`m
d`
Oq 90) 41MI N
x
X
x
x
x
x
x
x
x
r
9jepng Aj!uijBjjV
X
X
X
X
x
X
X
X
x
,
I=AIO euoA( LI;3
X
x
x
x
x
X
_CI
(n
uj
3
F
V w)eylmoa OLz9
x
X
x
K
in
auex0!4-y'I, WIS 09Z9
x
x
x
x
x
x
x
x
x
x
x
x
3
NlA
;88j sesli�euy
n
a
`
,Bulo
!°ueyleW
a
E
W
4
EOZSZeN
HoeN
1c.
W
ICH
Cn
rr%..
M
M
t
c
N
soNrl
€
�,
E
a
eoszH
°
z
v
c u
`m
a ay`
a`
LU
peruesajdun
rA
M
M
52i3 NItl1N00 dO #
r i =
¢
U ¢
a a
a
NOU331100IVdw313ldw4'S
1
1
13
i7
[
o
C
r�
r,CL
CL
o-
ijl
a
s
z
y
uQi
Z
Q
C
O
~
'
w
III
uj
w
1"
O
+•
N
z0
CC
2
Z
Z
1-
z
p
Q
5
w
0.
N
W
U
ir
o
LL
m
K
rn
C
'
I
z
fdw03=0 EvtiE)=E)) 34AI MMV5
N
y
0
t
$
t
$
r
$
r
$
t
$
r
$
r
$
(URI ay sepoa pyen aes) 3000 XIHIVIN
n ai
o [ 2K
a
m
F
o
° p
N z#
li 7
ii
U
T
U m
N
U$ SRNO �iQ Or
Q
dda,
a
0
3 e
o
x 3 �
�o`33a�io 3aor
3
z
0
'°
8 ¢
$ �
W d a
n
O
U
C�
a d
E
a u m
u o E
2 . M 7
-
O
S
o¢
°a3
g
m
Q$S7
o
w
z
{n c E
o
�
¢
S
rn
d
Y
cn
m
N
L1
O
O
C
n
in
m
m
Pl
m
m
m
m
m
7T
cn
y
U
# YY311
ir
a
N C
w
N
c
d
yr
L
¢ m
-Ea
Page 33 of

Appendix B
Completed Inspection Forms
for Landfill Cap and
Phytoremediation System

A=COM
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE:
1/31/2020
CLIENT: CNA
INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry
Wet X Weather: clear
Water Flow From Culvert: Yes X
No
Rain Gauge Readings (unit in inches)
Date
1 /3/2020
1 /10/2020
1 /17/2020
1 /24, 31 /2020
Reading
1.6
0.3
1.7
1.4,.2
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: ❑ Improving/Positive ❑ Declining No Change
Area of Declining Health (if any):
Tree Status: Tree Identification:
R2T3 R6T4 R9T6 R13T8
Trunk Size (inches circ.)
36.5 56.75 17.5 12.75
Approx Tree Height 30'+
30'+ 20'+ 20'+
Foliage Condition N/A
no full canopy N/A N/A
Other Observations: leaves fallen
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
Fertilize the Tree:
Yes
No
X
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No
X
Tree Prune:
Yes
No
X
Fence Condition:
Intact
X�
Damaged
Repaired
F7
Evidence of Grazing:
Yes
No
Photos Taken:
Yes
71
No
Ld
Tree Growth Audit by Others:
Yes
No

A=COM
PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation: good condition
Landfill Cap Maintenance Activities: None
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

A=COM
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
2/28/2020
CLIENT: CNA INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry Wet X I Weather: clear
Water Flow From Culvert: Yes X No
Rain Gauge Readings (unit in inches)
Date
2/7/2020
2/14/2020
2/21 /2020
2/28/2020
Reading
4
1.9
0.6
0.7
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: ❑ Improving/Positive ❑ Declining No Change
Area of Declining Health (if any):
Tree Status: Tree Identification: R2T3 R6T4 R9T6 R13T8
Trunk Size (inches circ.) 36.5 56.75 17.75 12.75
Approx Tree Height 30'+ 30'+ 20'+ 20'+
Foliage Condition N/A no full canopy N/A N/A
Other Observations: leaves fallen
(attach additional
pages if needed) Dead poplars removed. See other activities below.
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
X
Fertilize the Tree: Yes No
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No
X
X
Tree Prune: Yes No
Fence Condition:
Intact
X�
Damaged
Repaired
Evidence of Grazing:
Yes
No
Photos Taken: Yes FX I No
Tree Growth Audit by Others:
Yes
No
X
PI/

A=COM
PAGE 2 of 2
IROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
OCATION: Salisbury, NC DATE:
:LIENT: CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation: good condition
Landfill Cap Maintenance Activities: None
Other Activities
Received Celanese approval to remove standing, dead poplars with mobile crane. These trees pose risk to new trees to be
planted in March. 12 standing, dead poplars were remove by tree crew and mobile crane.
Monitorinq tree R6T4 was dead and removed amonq the 12. New monitor will be selected for next report.
Form Reviewed By:
Date:
Rev. 1111512007

A=COM
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation
JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE: 3/27/2020
CLIENT: CNA
INSPECTED BY: L.Brooks
General Site Conditions
Site Conditions: Dry Wet X I
Weather: rain
Water Flow From Culvert: Yes X No
Rain Gauge Readings (unit in inches)
Date
3/6/2020
3/13/2020
3/20/2020
3/27/2020
Reading
0.2
0.1
0.5
1.7
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: ❑ Improving/Positive ❑ Declining No Change
Area of Declining Health (if any):
Tree Status: Tree Identification: R2T3 R8T3
R9T6 R13T8
Trunk Size (inches circ.) 36.75 N/A
18 13
Approx Tree Height 30'+ N/A
20'+ 20'+
Foliage Condition N/A N/A
N/A N/A
Other Observations: leaves fallen
(attach additional
pages if needed) Black willows planted. See other activities below. R8T3 too small to measure, but will monitor
its health as it grows to measurable size.
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
X
Fertilize the Tree: Yes No
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No
X
Tree Prune:
Yes
No
X
Fence Condition:
Intact
X�
Damaged
Repaired
Evidence of Grazing:
Yes
No
Photos Taken: Yes FX I No
Tree Growth Audit by Others:
Yes
No
X
PI/

A=COM
PAGE 2 of 2
IROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
OCATION: Salisbury, NC DATE:
:LIENT: CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation: good condition
Landfill Cap Maintenance Activities: None
Other Activities
100 black willow 4' whips were planted by augering 6" diameter x 12" deep holes. Trees were planted in these holes and backfil led
with compost. Each tree was fertilized individually. Trees were planted 3' on center with expectation of some not surviving.
Row 8, Tree 3 (R8T3) was selected to replace R6T4 monitorinq tree.
Form Reviewed By:
Date:
Rev. 1111512007

A=COM
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation
JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE:
4/24/2020
CLIENT: CNA
INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry Wet X I
Weather:
Water Flow From Culvert: Yes X No
Rain Gauge Readings (unit in inches)
Date
4/3/2020
4/10/2020
4/17/2020
4/24/2020
Reading
0.1
0.2
2
1.5
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: Improving/Positive ❑ Declining 0 No Change
Area of Declining Health (if any):
Tree Status: Tree Identification: R2T3 R8T3
R9T6 R13T8
Trunk Size (inches circ.) 36.75 N/A
18.25 13.25
Approx Tree Height 30'+ N/A
20'+ 20'+
Foliage Condition N/A N/A
N/A N/A
Other Observations: leaves budding, R8T3 too small to measure circumference
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
17/17/17
Fertilize the Tree: Yes X No
Site Irrigation:
Yes
No
X
F—xl
Apply Herbicide:
Yes
No
Generic Round up
El
Tree Prune: Yes No
Fence Condition:
Intact
X�
Damaged
Repaired
Evidence of Grazing:
Yes
No
Photos Taken: Yes ❑ No
x
Tree Growth Audit by Others:
Yes
El
No
X
PI/

A=COM
PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation: good condition
Landfill Cap Maintenance Activities: None
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

A=COM
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE:
5/29/2020
CLIENT: CNA
INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry Wet
X I Weather:
Water Flow From Culvert: Yes X No
Rain Gauge Readings (unit in inches)
Date
5/1/2020
5/8/2020
5/15/2020
5/22,29/2020
Reading
3.3
0.5
0
3.5,2.1
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed:
❑ Improving/Positive ❑ Declining No Change
Area of Declining Health (if any):
Tree Status: Tree Identification: R2T3
R8T3 R9T6 R13T8
Trunk Size (inches circ.) 37 N/A
18.5 13.5
Approx Tree Height 30'+ N/A
20'+ 20'+
Foliage Condition N/A N/A
N/A N/A
Other Observations: full foilage, R8T3 too small to measure circumference
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
X
No
X
Fertilize the Tree: Yes No
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No
X
Tree Prune:
Yes
No
X
Fence Condition:
Intact
X�
Damaged
Repaired
Evidence of Grazing:
Yes
No
Photos Taken: Yes ❑ No
x
Tree Growth Audit by Others:
Yes
El
No
X
PI/

ACOM PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation: good condition
Landfill Cap Maintenance Activities: Mowing
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

A=COM
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation
JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE:
6/26/2020
CLIENT: CNA
INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry Wet X I
Weather:
Water Flow From Culvert: Yes X No
Rain Gauge Readings (unit in inches)
Date
6/5/2020
6/12/2020
6/19/2020
6/26/2020
Reading
0
0.8
0.7
0.4
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: ❑ Improving/Positive ❑ Declining No Change
Area of Declining Health (if any):
Tree Status: Tree Identification: R2T3 R8T3
R9T6 R13T8
Trunk Size (inches circ.) 37 N/A
18.5 13.5
Approx Tree Height 30'+ N/A
20'+ 20'+
Foliage Condition N/A N/A
N/A N/A
Other Observations: full foilage, R8T3 too small to measure circumference
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
X
Fertilize the Tree: Yes No
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No
X
X
Tree Prune: Yes No
Fence Condition:
Intact
X�
Damaged
El Repaired
Evidence of Grazing:
Yes
No
Photos Taken: Yes ❑ No
x
Tree Growth Audit by Others:
Yes
El
No
X
PI/

A=COM
PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation: good condition
Landfill Cap Maintenance Activities: none
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

A=COM
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE:
7/31/2020
CLIENT: CNA
INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry X
Wet Weather:
Water Flow From Culvert: Yes X
No
Rain Gauge Readings (unit in inches)
Date
7/3/2020
7/10/2020
7/17/2020
7/24,31/2020
Reading
1
0.1
0.2
2.3,0.7
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: ❑ Improving/Positive 0 Declining 0 No Change
Area of Declining Health (if any):
Leaf canopy diminishing on 5 poplars
Willows continue to do well
Tree Status: Tree Identification:
R2T3 R8T3 R9T6 R13T8
Trunk Size (inches circ.)
37 N/A 18.5 13.5
Approx Tree Height 30'+
N/A 20'+ 20'+
Foliage Condition N/A
N/A N/A N/A
Other Observations: full foilage, R8T3 too small to measure circumference
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
Fertilize the Tree: Yes No X
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No X
Tree Prune:
Yes
No
X
Repaired
Fence Condition: Intact X� Damaged
Evidence of Grazing:
Photos Taken:
Yes
Yes
❑
No
No
Tree Growth Audit by Others:
Yes
Ej
No
X
PI/

ACOM PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation: good condition
Landfill Cap Maintenance Activities: mowing
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

A=COM
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE:
8/28/2020
CLIENT: CNA
INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry X
Wet Weather:
Water Flow From Culvert: Yes X
No
Rain Gauge Readings (unit in inches)
Date
8/7/2020
8/14/2020
8/21 /2020
8/28/2020
Reading
0.7
0.5
1.7
0.2
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: ❑ Improving/Positive E Declining ED No Change
Area of Declining Health (if any):
Leaf canopy diminishing/bark delaminating on 5 poplars
Willows continue to do well
Tree Status: Tree Identification:
R2T3 R8T3 R9T6 R13T8
Trunk Size (inches circ.)
37.25 N/A 18.75 13.5
Approx Tree Height 30'+
N/A 20'+ 20'+
Foliage Condition N/A
N/A N/A N/A
Other Observations: full foilage, R8T3 too small to measure circumference
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
Fertilize the Tree: Yes No X
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No X
Tree Prune:
Yes
No
X
Repaired
Fence Condition: Intact X� Damaged
Evidence of Grazing:
Photos Taken:
Yes
Yes
❑
No
No
Tree Growth Audit by Others:
Yes
Ej
No
X
PI/

A=COM
PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation: good condition
Landfill Cap Maintenance Activities: Added well pads and locks to landfill wells
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

A=COM
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation
JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE:
9/25/2020
CLIENT: CNA
INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry Wet X
Weather: rain
Water Flow From Culvert: Yes X No
Rain Gauge Readings (unit in inches)
Date
9/4/2020
9/11 /2020
9/18/2020
9/25/2020
Reading
1.8
0.1
1.9
1.5
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: ❑ Improving/Positive ❑ Declining No Change
Area of Declining Health (if any):
Tree Status: Tree Identification: R2T3 R8T3
R9T6 R13T8
Trunk Size (inches circ.) 37.25 N/A
18.75 13.5
Approx Tree Height 30'+ N/A
20'+ 20'+
Foliage Condition N/A N/A
N/A N/A
Other Observations: full foilage, R8T3 too small to measure circumference
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
Fertilize the Tree: Yes No X
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No X
Tree Prune:
Yes
No
X
Repaired
Fence Condition: Intact X� Damaged
Evidence of Grazing:
Photos Taken:
Yes
Yes
❑
No
No
Tree Growth Audit by Others:
Yes
Ej
No
X
PI/

ACOM PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation: good condition
Landfill Cap Maintenance Activities: mowing
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

A=COM
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation
JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE:
10/23/2020
CLIENT: CNA
INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry X Wet
Weather:
Water Flow From Culvert: Yes X No
Rain Gauge Readings (unit in inches)
Date
10/2/2020
10/9/2020
10/16/2020
10/23/2020
Reading
0.3
0.1
4.3
0
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: ❑ Improving/Positive ❑ Declining No Change
Area of Declining Health (if any):
Tree Status: Tree Identification: R2T3 R8T3
R9T6 R13T8
Trunk Size (inches circ.) 37.25 N/A
19 13.75
Approx Tree Height 30'+ N/A
20'+ 20'+
Foliage Condition N/A N/A
N/A N/A
Other Observations: Leaves falling, R8T3 too small to measure circumference
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
Fertilize the Tree: Yes No X
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No X
Tree Prune:
Yes
No
X
Repaired
Fence Condition: Intact X� Damaged
Evidence of Grazing:
Photos Taken:
Yes
Yes
❑
No
No
Tree Growth Audit by Others:
Yes
Ej
No
X
PI/

A=COM
PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation: good condition
Landfill Cap Maintenance Activities: none
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

A=COM
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation
JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE:
11/27/2020
CLIENT: CNA
INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry X Wet
Weather:
Water Flow From Culvert: Yes X No
Rain Gauge Readings (unit in inches)
Date
11/6/2020
11/13/2020
11/20/2020
11/27/2020
Reading
0.4
5
0
0.1
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: ❑ Improving/Positive ❑ Declining No Change
Area of Declining Health (if any):
Tree Status: Tree Identification: R2T3 R8T3
R9T6 R13T8
Trunk Size (inches circ.) 37.25 N/A
19 13.75
Approx Tree Height 30'+ N/A
20'+ 20'+
Foliage Condition N/A N/A
N/A N/A
Other Observations: Leaves falling, R8T3 too small to measure circumference
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
Fertilize the Tree: Yes No X
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No X
Tree Prune:
Yes
No
X
Repaired
Fence Condition: Intact X� Damaged
Evidence of Grazing:
Photos Taken:
Yes
Yes
❑
No
No
Tree Growth Audit by Others:
Yes
Ej
No
X
PI/

ACOM PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation: good condition
Landfill Cap Maintenance Activities: mowing
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007

A=COM
PAGE 1 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation
JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC
DATE:
12/26/2020
CLIENT: CNA
INSPECTED BY:
L.Brooks
General Site Conditions
Site Conditions: Dry Wet X
Weather: rain
Water Flow From Culvert: Yes X No
Rain Gauge Readings (unit in inches)
Date
12/4/2020
12/ 11 /2020
12/18/2020
12/26/2020
Reading
1.8
0
1.2
1.1
Tree Farm Inspection
Tree Observation: Change in Tree Health Observed: ❑ Improving/Positive ❑ Declining No Change
Area of Declining Health (if any):
Tree Status: Tree Identification: R2T3 R8T3
R9T6 R13T8
Trunk Size (inches circ.) 37.25 N/A
19.25 14
Approx Tree Height 30'+ N/A
20'+ 20'+
Foliage Condition N/A N/A
N/A N/A
Other Observations: Leaves have fallen, R8T3 too small to measure circumference
(attach additional
pagesifneeded)
Tree Farm Maintenance
Notes: (Please provide the chemical brand name
when applicable)
Grass Seeding:
Yes
No
X
Grass Mowing:
Yes
No
X
Fertilize the Tree: Yes No X
Site Irrigation:
Yes
No
X
Apply Herbicide:
Yes
No X
Tree Prune:
Yes
No
X
Repaired
Fence Condition: Intact X� Damaged
Evidence of Grazing:
Photos Taken:
Yes
Yes
❑
No
No
Tree Growth Audit by Others:
Yes
Ej
No
X
PI/

A=COM
PAGE 2 of 2
PROJECT: Celanese Needmore Road Landfill Site Seep Remediation JOB NUMBER: AECOM - 60135443
LOCATION: Salisbury, NC DATE:
CLIENT: CNA INSPECTED BY:
Landfill Cap Inspection
Landfill Cap Observation: good condition
Landfill Cap Maintenance Activities: none
Other Activities
Form Reviewed By:
Date:
Rev. 1111512007