CCB0051_TerrySmith_DWRStreamSampleReport_20200306

PO Number #
Loc. Descr.:TIRE MASTERS (CCB0051) COAL ASH STRUCTURAL FILL
Loc. Type:RIVER/STREAM
Collector:B COSTNER
Collect Date:01/22/2020
Collect Time:12:05
Date Received:01/23/2020
Time Received:08:30
Location ID:TM_SW_1
County:IREDELL
Region:MRO
Labworks LoginID MSWIFTSample Matrix:SURFACEWATER
Report Print Date:
North Carolina Division of Water Resources Water Sciences Section Laboratory Results
`VisitID
Sample Depth
MROReport To
CTBRiver Basin
03/06/2020
YesEmergency
YESCOC Yes/No
Sample ID:AC71842
3/6/20Final Report Date:
Final Report
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
NC CourierDelivery Method
COCPriority
AC71842
Analysis
Date
Method
Reference
Result/
QualifierPQLAnalyte NameCAS #Units Validated by
LAB
Sample temperature at receipt by lab
MSWIFT°CSample temperature at receipt by lab 1/23/200.3
MET
Ag by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUAg by ICPMS7440-22-4 1/30/201.0 1.0
Al by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LAl by ICP7429-90-5 1/30/2050110
Antimony by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUAntimony by ICPMS7440-36-0 1/30/201010
As by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUAs by ICPMS7440-38-2 1/30/202.0 2.0
B by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUB by ICP7429-90-5 1/30/205050
Ba by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LBa by ICP7440-38-3 1/30/201046
Be by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUBe by ICP7440-41-7 1/30/205.0 5.0
Ca by ICP
EPA 200.7 Rev4.4 ESTAFFORD1mg/LCa by ICP7440-70-2 1/30/200.10 6.9
Cd by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUCd by ICPMS7440-43-9 1/29/200.50 0.50
Cobalt by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUCobalt by ICP7440-48-4 1/30/205050
Cr by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUCr by ICPMS7440-47-3 1/29/205.0 5.0
Cu by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUCu by ICPMS7440-50-8 1/29/202.0 2.0
Fe by ICP
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 1 of 3
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
AC71842Sample ID:
NC DWR Laboratory Section Results/Sample Comments/Qualifier Definitions
CAS #Analyte Name PQL Result/
Qualifier Units
Method
Reference
Analysis
Date Validated by
EPA 200.7 Rev4.4 ESTAFFORD1ug/LFe by ICP7439-89-6 1/30/20501300
Hardness by Calculation
SM 2340B-1997 ESTAFFORD1mg/LHardness by Calculation 2/4/201.0 26
Hg 245.1
EPA 245.1 Rev3 ESTAFFORD1ug/LUHg 245.17439-97-6 1/29/200.2 0.20
K by ICP
EPA 200.7 Rev4.4 ESTAFFORD1mg/LK by ICP7440-09-7 1/30/200.10 2.5
Li ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LULi ICP7439-93-2 1/30/202525
Mg by ICP
EPA 200.7 Rev4.4 ESTAFFORD1mg/LMg by ICP7439-95-4 1/30/200.10 2.0
Mn by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LMn by ICP7439-96-5 1/30/2010110
Mo by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUMo by ICPMS7439-98-7 1/30/201010
Na by ICP
EPA 200.7 Rev4.4 ESTAFFORD1mg/LNa by ICP7440-23-5 1/30/200.10 9.1
Ni by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUNi by ICPMS7440-02-0 1/30/202.0 2.0
Pb by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUPb by ICPMS7439-92-1 1/30/202.0 2.0
Se by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUSe by ICPMS7782-49-2 1/30/201.0 1.0
Sn by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUSn by ICPMS7440-31-5 1/30/201010
Sr by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LSr by ICPMS7440-24-6 1/30/2010150
Thallium (Tl) ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUThallium (Tl) ICPMS7440-28-0 1/30/202.0 2.0
Ti (Titanium) by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUTi (Titanium) by ICP7440-32-6 1/30/201010
V by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUV by ICP7440-62-2 1/30/201010
Zn by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUZn by ICPMS7440-66-6 1/30/201010
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 2 of 3
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
AC71842Sample ID:
NC DWR Laboratory Section Results/Sample Comments/Qualifier Definitions
CAS #Analyte Name PQL Result/
Qualifier Units
Method
Reference
Analysis
Date Validated by
WET
Fluoride,Chloride,Bromide,Sulfate by IC
EPA 300.0 rev2.1 AWILLIAMSmg/LUBromide 1/24/200.4 0.4
EPA 300.0 rev2.1 AWILLIAMSmg/LChloride 1/24/201.0 9.2
EPA 300.0 rev2.1 AWILLIAMSmg/LUFluoride 1/24/200.4 0.4
EPA 300.0 rev2.1 AWILLIAMSmg/LSulfate 1/24/202.0 6.3
Total Dissolved Solids in liquid
SM 2540 C-1997 AWILLIAMSmg/LTotal Dissolved Solids in liquid 1/23/201295
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 3 of 3
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
PO Number #
Loc. Descr.:TIRE MASTERS (CCB0051) COAL ASH STRUCTURAL FILL
Loc. Type:RIVER/STREAM
Collector:B COSTNER
Collect Date:01/22/2020
Collect Time:12:05
Date Received:01/23/2020
Time Received:08:30
Location ID:TM_SW_1
County:IREDELL
Region:MRO
Labworks LoginID MSWIFTSample Matrix:SURFACEWATER
Report Print Date:
North Carolina Division of Water Resources Water Sciences Section Laboratory Results
VisitID
Sample Depth
MROReport To
CTBRiver Basin
03/06/2020
YESEmergency
YESCOC Yes/No
Sample ID:AC71843
3/6/20Final Report Date:
Final Report
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
NC CourierDelivery Method
COCPriority
AC71843
Analysis
Date
Method
Reference
Result/
QualifierPQLAnalyte NameCAS #Units Validated by
LAB
Sample temperature at receipt by lab
MSWIFT°CSample temperature at receipt by lab 1/23/200.3
MET
Ag-Dissolved Silver by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUAg-Dissolved Silver by ICPMS7440-22-4 1/30/201.0 1.0
Al - Dissolved Aluminum by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUAl - Dissolved Aluminum by ICP7429-90-5 1/30/205050
As- Dissolved by ICPMS Arsenic
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUAs- Dissolved by ICPMS Arsenic7440-38-2 1/30/202.0 2.0
B Dissolved by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUB Dissolved by ICP7429-90-5 1/30/205050
Ba- Dissolved Barium by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LBa- Dissolved Barium by ICP7440-38-3 1/30/201046
Be-Beryllium Dissolved by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUBe-Beryllium Dissolved by ICP7440-41-7 1/30/205.0 5.0
Ca-Dissolved Calcium by ICP
EPA 200.7 Rev4.4 ESTAFFORD1mg/LCa-Dissolved Calcium by ICP7440-70-2 1/30/200.10 6.8
Cd- Dissolved Cadmium by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUCd- Dissolved Cadmium by ICPMS7440-43-9 1/29/200.50 0.50
Cobalt Dissolved by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUCobalt Dissolved by ICP7440-48-4 1/30/205050
Cr- Dissolved Chromium by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUCr- Dissolved Chromium by ICPMS7440-47-3 1/29/205.0 5.0
Cu- Dissolved Copper by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUCu- Dissolved Copper by ICPMS7440-50-8 1/29/202.0 2.0
Fe- Dissolved Iron by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LFe- Dissolved Iron by ICP7439-89-6 1/30/2050920
Hg 245.1 Dissolved
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 1 of 2
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
AC71843Sample ID:
NC DWR Laboratory Section Results/Sample Comments/Qualifier Definitions
CAS #Analyte Name PQL Result/
Qualifier Units
Method
Reference
Analysis
Date Validated by
EPA 245.1 Rev3 ESTAFFORD1ug/LUHg 245.1 Dissolved7439-97-6 1/29/200.2 0.20
K-Dissolved Potassium by ICP
EPA 200.7 Rev4.4 ESTAFFORD1mg/LK-Dissolved Potassium by ICP7440-09-7 1/30/200.10 2.5
Li DISSOLVED ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LULi DISSOLVED ICP7439-93-2 1/30/202525
Mg- Dissolved Magnesium by ICP
EPA 200.7 Rev4.4 ESTAFFORD1mg/LMg- Dissolved Magnesium by ICP7439-95-4 1/30/200.10 2.0
Mn Dissolved by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LMn Dissolved by ICP7439-96-5 1/30/2010110
Mo Dissolved by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUMo Dissolved by ICPMS7439-98-7 1/30/201010
Na-Dissolved Sodium by ICP
EPA 200.7 Rev4.4 ESTAFFORD1mg/LNa-Dissolved Sodium by ICP7440-23-5 1/30/200.10 9.1
Ni-Dissolved Nickel by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUNi-Dissolved Nickel by ICPMS7440-02-0 1/30/202.0 2.0
Pb-Dissolved Lead by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUPb-Dissolved Lead by ICPMS7439-92-1 1/30/202.0 2.0
Sb Dissolved by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUSb Dissolved by ICPMS7440-36-0 1/30/201010
Se-Dissolved Selenium by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUSe-Dissolved Selenium by ICPMS7782-49-2 1/30/201.0 1.0
Sn Dissolved by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUSn Dissolved by ICPMS7440-31-5 1/30/201010
Sr Dissolved by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LSr Dissolved by ICPMS 1/30/2010140
Thallium (Tl) Dissolved by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUThallium (Tl) Dissolved by ICPMS7440-28-0 1/30/202.0 2.0
Ti (Titanium) Dissolved by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUTi (Titanium) Dissolved by ICP7440-32-6 1/30/201010
V Dissolved by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUV Dissolved by ICP7440-62-2 1/30/201010
Zn-Dissolved Zinc by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUZn-Dissolved Zinc by ICPMS7440-66-6 1/30/201010
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 2 of 2
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
PO Number #
Loc. Descr.:TIRE MASTERS (CCB0051) COAL ASH STRUCTURAL FILL
Loc. Type:RIVER/STREAM
Collector:B COSTNER
Collect Date:01/22/2020
Collect Time:11:20
Date Received:01/23/2020
Time Received:08:30
Location ID:TM_SW_2
County:IREDELL
Region:MRO
Labworks LoginID MSWIFTSample Matrix:SURFACEWATER
Report Print Date:
North Carolina Division of Water Resources Water Sciences Section Laboratory Results
VisitID
Sample Depth
MROReport To
CTBRiver Basin
03/06/2020
YESEmergency
YESCOC Yes/No
Sample ID:AC71844
3/6/20Final Report Date:
Final Report
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
NC CourierDelivery Method
COCPriority
AC71844
Analysis
Date
Method
Reference
Result/
QualifierPQLAnalyte NameCAS #Units Validated by
MET
Ag by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUAg by ICPMS7440-22-4 1/30/201.0 1.0
Al by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LAl by ICP7429-90-5 1/30/205088
Antimony by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUAntimony by ICPMS7440-36-0 1/30/201010
As by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUAs by ICPMS7440-38-2 1/30/202.0 2.0
B by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LB by ICP7429-90-5 1/30/2050120
Ba by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LBa by ICP7440-38-3 1/30/201071
Be by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUBe by ICP7440-41-7 1/30/205.0 5.0
Ca by ICP
EPA 200.7 Rev4.4 ESTAFFORD1mg/LCa by ICP7440-70-2 1/30/200.10 13
Cd by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUCd by ICPMS7440-43-9 1/29/200.50 0.50
Cobalt by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUCobalt by ICP7440-48-4 1/30/205050
Cr by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUCr by ICPMS7440-47-3 1/29/205.0 5.0
Cu by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUCu by ICPMS7440-50-8 1/29/202.0 2.0
Fe by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LFe by ICP7439-89-6 1/30/20501600
Hardness by Calculation
SM 2340B-1997 ESTAFFORD1mg/LHardness by Calculation 1/30/201.0 46
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 1 of 3
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
AC71844Sample ID:
NC DWR Laboratory Section Results/Sample Comments/Qualifier Definitions
CAS #Analyte Name PQL Result/
Qualifier Units
Method
Reference
Analysis
Date Validated by
Hg 245.1
EPA 245.1 Rev3 ESTAFFORD1ug/LUHg 245.17439-97-6 1/29/200.2 0.20
K by ICP
EPA 200.7 Rev4.4 ESTAFFORD1mg/LK by ICP7440-09-7 1/30/200.10 3.0
Li ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LULi ICP7439-93-2 1/30/202525
Mg by ICP
EPA 200.7 Rev4.4 ESTAFFORD1mg/LMg by ICP7439-95-4 1/30/200.10 3.2
Mn by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LMn by ICP7439-96-5 1/30/2010290
Mo by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUMo by ICPMS7439-98-7 1/30/201010
Na by ICP
EPA 200.7 Rev4.4 ESTAFFORD1mg/LNa by ICP7440-23-5 1/30/200.10 9.5
Ni by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUNi by ICPMS7440-02-0 1/30/202.0 2.0
Pb by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUPb by ICPMS7439-92-1 1/30/202.0 2.0
Se by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUSe by ICPMS7782-49-2 1/30/201.0 1.0
Sn by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUSn by ICPMS7440-31-5 1/30/201010
Sr by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LSr by ICPMS7440-24-6 1/30/2010300
Thallium (Tl) ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUThallium (Tl) ICPMS7440-28-0 1/30/202.0 2.0
Ti (Titanium) by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUTi (Titanium) by ICP7440-32-6 1/30/201010
V by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUV by ICP7440-62-2 1/30/201010
Zn by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LZn by ICPMS7440-66-6 1/30/201013
WET
Fluoride,Chloride,Bromide,Sulfate by IC
EPA 300.0 rev2.1 AWILLIAMSmg/LUBromide 1/24/200.4 0.4
EPA 300.0 rev2.1 AWILLIAMSmg/LChloride 1/24/201.0 9.9
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 2 of 3
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
AC71844Sample ID:
NC DWR Laboratory Section Results/Sample Comments/Qualifier Definitions
CAS #Analyte Name PQL Result/
Qualifier Units
Method
Reference
Analysis
Date Validated by
EPA 300.0 rev2.1 AWILLIAMSmg/LUFluoride 1/24/200.4 0.4
EPA 300.0 rev2.1 AWILLIAMSmg/LSulfate 1/24/202.0 12
Total Dissolved Solids in liquid
SM 2540 C-1997 AWILLIAMSmg/LTotal Dissolved Solids in liquid 1/23/201298
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 3 of 3
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
PO Number #
Loc. Descr.:TIRE MASTERS (CCB0051) COAL ASH STRUCTURAL FILL
Loc. Type:RIVER/STREAM
Collector:B COSTNER
Collect Date:01/22/2020
Collect Time:11:20
Date Received:01/23/2020
Time Received:08:30
Location ID:TM_SW_2
County:IREDELL
Region:MRO
Labworks LoginID MSWIFTSample Matrix:SURFACEWATER
Report Print Date:
North Carolina Division of Water Resources Water Sciences Section Laboratory Results
VisitID
Sample Depth
MROReport To
CTBRiver Basin
03/06/2020
YESEmergency
YESCOC Yes/No
Sample ID:AC71845
3/6/20Final Report Date:
Final Report
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
NC CourierDelivery Method
COCPriority
AC71845
Analysis
Date
Method
Reference
Result/
QualifierPQLAnalyte NameCAS #Units Validated by
LAB
Sample temperature at receipt by lab
MSWIFT°CSample temperature at receipt by lab 1/23/200.3
MET
Ag-Dissolved Silver by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUAg-Dissolved Silver by ICPMS7440-22-4 1/30/201.0 1.0
Al - Dissolved Aluminum by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUAl - Dissolved Aluminum by ICP7429-90-5 1/30/205050
As- Dissolved by ICPMS Arsenic
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUAs- Dissolved by ICPMS Arsenic7440-38-2 1/30/202.0 2.0
B Dissolved by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LB Dissolved by ICP7429-90-5 1/30/2050110
Ba- Dissolved Barium by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LBa- Dissolved Barium by ICP7440-38-3 1/30/201070
Be-Beryllium Dissolved by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUBe-Beryllium Dissolved by ICP7440-41-7 1/30/205.0 5.0
Ca-Dissolved Calcium by ICP
EPA 200.7 Rev4.4 ESTAFFORD1mg/LCa-Dissolved Calcium by ICP7440-70-2 1/30/200.10 13
Cd- Dissolved Cadmium by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUCd- Dissolved Cadmium by ICPMS7440-43-9 1/29/200.50 0.50
Cobalt Dissolved by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUCobalt Dissolved by ICP7440-48-4 1/30/205050
Cr- Dissolved Chromium by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUCr- Dissolved Chromium by ICPMS7440-47-3 1/29/205.0 5.0
Cu- Dissolved Copper by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUCu- Dissolved Copper by ICPMS7440-50-8 1/29/202.0 2.0
Fe- Dissolved Iron by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LFe- Dissolved Iron by ICP7439-89-6 1/30/20501200
Hg 245.1 Dissolved
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 1 of 2
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
AC71845Sample ID:
NC DWR Laboratory Section Results/Sample Comments/Qualifier Definitions
CAS #Analyte Name PQL Result/
Qualifier Units
Method
Reference
Analysis
Date Validated by
EPA 245.1 Rev3 ESTAFFORD1ug/LUHg 245.1 Dissolved7439-97-6 1/29/200.2 0.20
K-Dissolved Potassium by ICP
EPA 200.7 Rev4.4 ESTAFFORD1mg/LK-Dissolved Potassium by ICP7440-09-7 1/30/200.10 3.0
Li DISSOLVED ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LULi DISSOLVED ICP7439-93-2 1/30/202525
Mg- Dissolved Magnesium by ICP
EPA 200.7 Rev4.4 ESTAFFORD1mg/LMg- Dissolved Magnesium by ICP7439-95-4 1/30/200.10 3.2
Mn Dissolved by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LMn Dissolved by ICP7439-96-5 1/30/2010290
Mo Dissolved by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUMo Dissolved by ICPMS7439-98-7 1/30/201010
Na-Dissolved Sodium by ICP
EPA 200.7 Rev4.4 ESTAFFORD1mg/LNa-Dissolved Sodium by ICP7440-23-5 1/30/200.10 9.5
Ni-Dissolved Nickel by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUNi-Dissolved Nickel by ICPMS7440-02-0 1/30/202.0 2.0
Pb-Dissolved Lead by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUPb-Dissolved Lead by ICPMS7439-92-1 1/30/202.0 2.0
Sb Dissolved by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUSb Dissolved by ICPMS7440-36-0 1/30/201010
Se-Dissolved Selenium by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUSe-Dissolved Selenium by ICPMS7782-49-2 1/30/201.0 1.0
Sn Dissolved by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUSn Dissolved by ICPMS7440-31-5 1/30/201010
Sr Dissolved by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LSr Dissolved by ICPMS 1/30/2010310
Thallium (Tl) Dissolved by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LUThallium (Tl) Dissolved by ICPMS7440-28-0 1/30/202.0 2.0
Ti (Titanium) Dissolved by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUTi (Titanium) Dissolved by ICP7440-32-6 1/30/201010
V Dissolved by ICP
EPA 200.7 Rev4.4 ESTAFFORD1ug/LUV Dissolved by ICP7440-62-2 1/30/201010
Zn-Dissolved Zinc by ICPMS
EPA 200.8 Rev5.4 ESTAFFORD1ug/LZn-Dissolved Zinc by ICPMS7440-66-6 1/30/201016
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 2 of 2
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.