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HomeMy WebLinkAbout6301_MooreCounty_MSWLF_CDLF_Oct 2020GW_FID1523824_20210115ENR USE ONLY_j ❑Paper Report ❑Electronic Data - Email CD data loaded: Yes / No Doc/Event #: C DENR I IEnvironmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: • Prepare one form for each individually monitored unit. • Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). • Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. • Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): S&ME, Inc. (Consultant for Moore County) Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Edmund Q.B. Henriques Phone: 336-288-7180 E-mail: ehenriques@smeinc.com NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address: Facility Permit # (.0500 or. 1600) October 20-24, 2006) Moore County Landfill 456 Turning Leaf Way, 63-01 .0500 October 13-15, 2020 Aberdeen, North Carolina 28315 Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring ❑x Detection Monitoring ❑x Assessment Monitoring x❑ Corrective Action of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells ❑ Groundwater monitoring data from private water supply wells ❑x Leachate monitoring data Surface water monitoring data ❑ Methane gas monitoring data Corrective action data (specify) Monitored Natural Attenuation Data Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. RX Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. ❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Edmund Q.B. Henriques, PG Senior Geologist / S&ME, Inc. 336-312-3330 Facility Representative Name (Print) , Title (Area Code) Telephone Number 01-14-2021 Affix NC License, m� ®0 ® i M Signature v t1 Date 8646 W. Market Street, Suite 105, Greensboro NC 27409 Facility Representative Address F-0176 NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 Seal L3 PREPARED FOR: Moore County Solid Waste P.O. Box 1927 Carthage, North Carolina 28327 S&ME, Inc. 8646 West Market Street, Suite 105 Greensboro, North Carolina 27409 January 14, 2020 =0 January 14, 2021 Moore County Solid Waste Department P.O. Box 1927 Carthage, North Carolina 28327-1927 Attention: Mr. David Lambert via email: dlambert1 @moorecountync.gov Solid Waste Director Reference: Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 Dear Mr. Lambert: S&ME, Inc. (S&ME) is pleased to submit this report documenting water quality monitoring conducted between October 13, 2020 through October 15, 2020 at the Moore County Solid Waste Facility located in Aberdeen, North Carolina. These services have been performed in general accordance with S&ME Proposal No. 43-2000335Rev1, dated August 3, 2020. One copy of this report is attached for your file and one copy has been delivered electronically on your behalf directly to the North Carolina Department of Environmental Quality - Division of Waste Management, Solid Waste Section. S&ME appreciates the opportunity to provide environmental services to Moore County. Please call us if you have any questions or comments. Sincerely, S&ME, Inc. 4 Edmund Q.B. Henriques, P.G. Senior Geologist/Project Manager ehenriques@smeinc.com Samuel P. Watts, P.G. Senior Project Manager swatts@smeinc.com Jaclynne Drummond, Hydrogeologist, Solid Waste Section, Division of Waste Management, NC DEQ, 2090 US Highway 70, Swannanoa, NC 28778, jaclynne.drunnnnond@ncdenr.gov (electronic copy) Jimmy Brown, Landfill Manager, NC, 5227 Hwy 15-501, P.O. Box 1927, Carthage, North Carolina, 28327 (hard copy & electronic copy) S&ME, Inc. 18646 W. Market St, Ste 105 1 Greensboro, NC 27409 1 p 336.288.7180 1 www.smeinc.com Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 Table of Contents 1.0 Executive Summary..........................................................................................................1 2.0 Background and Compliance History...........................................................................3 2.1 Background..................................................................................................................................... 3 2.2 Compliance History....................................................................................................................... 3 3.0 Methods Employed...........................................................................................................6 3.1 Groundwater Sampling.................................................................................................................6 3.2 Surface Water Sampling................................................................................................................ 7 4.0 Site Hydrogeology............................................................................................................8 4.1 Groundwater Elevations and Flow Direction............................................................................ 8 4.2 Groundwater Flow Velocity......................................................................................................... 8 5.0 Results.................................................................................................................................9 5.1 Groundwater Analytical Data - MSW Landfill........................................................................10 5.2 Groundwater Analytical Data - C&D Landfill........................................................................11 5.3 Groundwater Analytical for Monitored Natural Attenuation Parameters ..........................11 5.4 Groundwater Analytical - Private Water Well........................................................................11 5.5 Surface Water Analytical Data...................................................................................................11 5.6 Quality Control.............................................................................................................................12 6.0 Discussion of Results.....................................................................................................13 7.0 References.........................................................................................................................13 List of Figures Figure 1 Groundwater Elevations and Contours - October 2020 Monitoring Event List of Tables Table 1 Active Monitoring Well Construciton Information Table 2 Groundwater Elevation Data Table 3 Groundwater Field Parameter Data Table 4 Groundwater Conductivities, Gradients, and Flow Velocities Table 5 Groundwater Monitoring Analytical Results (Detected Constituents) Table 6 Surface Water Monitoring Analytical Results (Detected Constituents) January 14, 2020 Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina I I s S&ME Project No. 4358-20-043A, Task 01 - Appendices Appendix I —Sampling Forms Appendix II — Laboratory Analytical Reports Appendix III — Historical Analytical Results Appendix IV — Time vs Concentration Charts January 14, 2020 Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina I S&ME Project No. 4358-20-043A, Task 01 ! 1.0 Executive Summary Between October 13 and October 15, 2020, nineteen monitoring wells and four surface water locations which monitor the Moore County Solid Waste Facility were sampled as part of the second semi-annual monitoring event for 2020. Monitoring wells MW-1, MW-2, MW-3, MW-4, MW-5, MW-6, MW-7, MW-8, MW-9, MW-11SR, MW- 11 DR, MW-13SR, MW-13DR, MW-14, MW-15R, MW-17S, MW-17D, MW-18 and MW-19 comprise the groundwater monitoring system for the closed municipal solid waste (MSW) landfill and active Construction & Demolition (C&D) landfill. One private off -site water well (Blake residence) was also sampled. Samples were collected from surface water locations SW-1, SW-2, SW-3, and SW-4. Groundwater and surface water sampling was conducted according to North Carolina Department of Environmental Quality, Division of Waste Management, Solid Waste Section (NCDEQ-SWS) guidelines. Samples were analyzed by a North Carolina certified laboratory. Samples collected were submitted for analysis in accordance with the facility's current NCDEQ-SWS approved Water Quality Monitoring Plan. Analyses of the surface water samples collected detected no target constituent at a concentration exceeding the corresponding 15A NCAC 2B Standards (213 Standards). It is noteworthy that 1,4-Dioxane was detected at surface water sample locations SW-1, SW-3 and SW-4 at concentrations greater than the corresponding North Carolina In -Stream Target Value for Surface Waters set at 0.35 micrograms per liter (pg/L) for Class WS (I-V) surface waters; however, no surface water standard promulgated by 15A NCAC 2B (213 Standard) currently exists for 1,4-Dioxane. The table below summarizes the MSW landfill monitor well locations where target constituents were detected at concentrations greater than the corresponding 15A NCAC 2L Groundwater Standards (21- Standards) or NCDEQ- SWS Groundwater Protection Standards (GWPS) during the October 2020 monitoring even.: October 2020 Groundwater Sampling Event - MSW Landfill Monitoring Wells Constituent Concentration Detected Greater Than 2L Standard or GWPS Parameter 2L Standard or GWPS MSW Landfill Monitoring MW-2 MW-4 iLiL Wells MW-6 MW-7 iLiL MW-8 iL MW-9 iL MW-15SR iL 1,4-Dioxane 3 9.7 6.9 29 25 Benzene 1 2.5 2.8 4.0 1.2 Vinyl Chloride 0.03 1.1 5.4 1.1 Arsenic 10 64.8 Cadmium 2 2.16 Iron 300 1 397 Note: Blank cells indicate constituent concentrations less than the corresponding 2L Standard or GWPS. The 2L Standard exceedances for volatile organic compounds (VOCs) summarized above are generally consistent with historic monitoring results, which previously triggered regulatory requirements for implementation of Corrective Measures for the MSW landfill. In 2018, the NCDEQ-SWS requested all MSW and C&D landfills begin to analyze samples for 1,4-Dioxane. Thus, historic data for detections of this parameter at the landfill are limited. January 14, 2020 Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 Site -specific soil data presented in Golder's Second Semi -Annual 2016 Water Quality Monitoring Report indicated that concentrations detected in naturally occurring soils on site can account for arsenic concentrations that were measured in groundwater samples. Based on Golder's prior reported site specific assessment findings, arsenic appears to be naturally occurring. Cadmium has not been detected at monitoring well MW-6 since November 2016. Based on historic data, the reported concentration appears to be an outlier value. The first semi-annual monitoring event for 2021 will be utilized to verify this anomalous concentration. The table below provides a summary of the C&D landfill monitor well locations where target constituents were detected at concentrations greater than the 2L Standard or GWPS during the October 2020 monitoring event: October 2020 Groundwater Sampling Event - C&D Landfill Monitoring Wells Constituent Concentration Detected Greater Than 2L Standard or GWPS Parameter 2L Standard or GWPS MW-11SR (Ng/L) :. Landfill MW-11DR (Ng/L) Monitoring MW-13SR (Ng/L) Wells MW-13DR (Ng/L) MW-14 (gg/L) MW-17S (gg/L) MW-17D (Ng/L) MW-18 (ug/L) 1,4-Dioxane 3 5.4 4.4 3.4 14 6.8 10 Benzene 1 3.2 1.9 2.2 Vinyl Chloride 0.03 2.4 1.8 2.3 1.9 Iron 300 119,000 83,800 66,200 7,600 139,000 14,400 2,500 103,000 Manganese 50 294 180 569 123 183 164 227 Note: Blank cells indicate constituent concentrations less than the corresponding 2L Standard or GWPS. The Alternate Source Demonstration (ASD) prepared by Golder dated, February 28, 2017, indicated that VOCs detected in certain C&D landfill monitoring wells were attributed to the MSW landfill. NCDEQ-SWS responded indicating that they would not approve the ASD for VOCs at the C&D Landfill, at that time. NCDEQ-SWS requested that Moore County implement landfill gas and groundwater corrective action at the closed MSW landfill; and commence assessment monitoring at the C&D landfill pursuant to 15A NCAC 13B .0545. In response to the NCDEQ-SWS request, Moore County commenced with assessment monitoring at the C&D Landfill. At the MSW landfill, a methane cut-off trench was installed in 2018. Solar flares were added to the cut-off trench vents during early 2020. Monitored Natural Attenuation (MNA) is the selected groundwater remedy for the closed MSW landfill monitoring. MNA "Performance Monitoring" continues at MSW wells and select C&D wells. Impacted groundwater at the facility does not appear to be adversely affecting surface water at the site. Benzene and vinyl chloride in the vicinity of the MSW landfill generally exhibit trends of stable or declining concentrations over time, with a few exceptions. Concentrations of these constituents are not rising immediately down -gradient of the source area. The recent 2L Standard exceedance for benzene at monitoring well MW-18 will be closely monitored. The size of the data set for 1,4-Dioxane is currently insufficient for accurate trend analysis. In view of the concentration trends, Moore County plans to continue Assessment Monitoring for the C&D landfill and MNA monitoring of the closed MSW landfill; unless evidence of increasing VOCs concentrations are confirmed or unless Moore County is directed by NCDEQ to proceed to the alternate groundwater remedy. Moore County is proactively evaluating options for alternate groundwater corrective actions that may be appropriate for the CAP contingency plan, including options that would aid in the management of landfill gases; which can contribute to groundwater exceedances. January 14, 2020 Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 - 2.0 Background and Compliance History 2.1 Background Moore County currently operates a solid waste facility at 156 Turning Leaf Road, in Aberdeen , North Carolina. The facility is owned and operated by Moore County under Solid Waste Permit No. 63-01 issued by the NCDEQ- SWS. The facility includes a municipal solid waste (MSW) transfer facility, a closed unlined MSW landfill and an active C&D landfill unit. The C&D landfill unit and closed MSW landfill are regulated in general accordance with NCDEQ-SWS Permit No. 63-10. Moore County performs groundwater and surface water monitoring on a semiannual basis to comply with the requirements of North Carolina Solid Waste Management Rules (Solid Waste Rules), 15A NCAC 13B. S&ME has prepared this report on behalf of Moore County to present the results of the second monitoring event for 2020 as required by § .0600 and .1632 of the Solid Waste Rules. The Golder Associates NC, Inc. (Golder), Water Quality Monitoring Plan — Moore County Landfill, Permit No. 63-70, Volume 2 — Moore County Design Hydrogeological Report and Monitoring Plans (WQMP) dated December 10, 2019, is the current NCDEQ approved WQMP. Based on the WQMP there are two groundwater compliance well networks, with one background monitoring well providing background data for both networks. The active C&D landfill groundwater monitoring network consists of nine downgradient monitoring wells (MW-4, MW-11 SR, MW-11 DR, MW-13SR, MW-13DR, MW-14, MW-17D, MW-18 and MW-19). One monitoring well (MW-5) is shared by both the C&D landfill and MSW landfill for monitoring background groundwater quality. The closed MSW landfill groundwater monitoring network consists of eight downgradient monitoring wells (MW-1, MW-2, MW-3, MW-6, MW-7, MW-8, MW-9 and MW-15R). In addition, two C&D monitoring wells (MW-4, MW-11SR) are also used as MNA performance monitoring wells to assess groundwater impacts from the MSW landfill. The groundwater monitoring wells represent conditions in the uppermost aquifer underlying the facility, positioned for detection of potential releases from the landfill units; with some wells employed to assess the efficacy of natural attenuation as a corrective measure. Monitoring wells with "D" suffixes to the well identifier, represent wells screened within deeper portions of the surficial aquifer. The WQMP also involves four stream sample locations, two upstream and two downstream. One private water supply well on a parcel located east of the facility, the Blake residence well, was monitored in accordance with the approved WQMP. The C&D landfill is currently in Assessment Monitoring. The MSW landfill is currently in Corrective Action Monitoring, which includes MNA performance monitoring parameters for most monitoring wells. 2.2 Compliance History Groundwater quality has been monitored at the landfill facility since 1987. Monitoring wells MW-1 through MW-4 monitored down -gradient regions of the MSW landfill, with MW-5 providing background water quality data for the facility. In March 1995, monitoring wells MW-6 through MW-9 were added to monitor the area between the MSW and the C&D landfill. January 14, 2020 Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 - An NCDEQ-SWS letter dated January 23, 1996, presented initial concerns regarding a potential for off -site migration of VOCs from the facility. Moore County voluntarily initiated corrective measure due to concerns of off - site migration of VOCs in groundwater and measured methane gas concentrations. In 1996, the off -site water supply well at the Blake residence (PW-1) was added to the groundwater monitoring program and monitoring of surface water points SW-2 and SW-1, commenced. Additional groundwater monitoring wells (MW-11 S, MW-11 D, MW-125, MW-12D, MW-135, MW-13D, and MW-14) were installed to assess the extent of groundwater impacts, establish monitoring points for the C&D facility, and to collected data to attempt differentiation of MSW groundwater impacts from C&D landfill impacts. Subsequently, monitoring wells MW12S and MW-12D were abandoned due to planned expansion of the C&D landfill, and replaced by monitoring wells MW-16S and MW16D, located further west and downgradient. In November 1999, HDR Engineering Inc. of the Carolinas (HDR) submitted a Work Plan to further investigate groundwater and methane migration concerns, with assessment activities commencing in March 2000. HDR reported the existence of a clay confining unit at depth beneath the landfill, which was reported to limit vertical groundwater contamination. In January 2005, NCDEQ-SWS requested that Moore County complete an assessment of corrective measures and select a remedy in accordance with 15A NCAC 2L .0106. In July 2005, HDR submitted the Assessment of Corrective Measures Report (ACM) to NCDEQ recommending monitored natural attenuation (MNA) as the primary remedy, with a contingency plan for active landfill gas (LFG) remediation if trends of increasing VOC concentrations over time were observed in groundwater. On November 21, 2005, NCDEQ-SWS approved HDR's ACM. In 2005, a shallow trench vent network consisting of a trench and 12 passive LFG vents were installed to address LFG migration concerns. In 2007, the LFG vent network was expanded with the addition of 12 passive LFG vents. In February 2014, three in -waste passive gas vent wells (GV-30, GV-31, and GV-32) were installed as part of the Joyce Engineering, Inc. Contingency Plan Update and Implementation Plan -Revised approved by NCDEQ-SWS on June 5, 2013. HDR prepared a revised Water Quality Monitoring Plan dated July 20, 2006, which was approved by NCDEQ-SWS on October 13, 2006. The 2006 plan involved monitoring all groundwater and surface water monitoring points for North Carolina Appendix I VOCs and the eight Resource Conservation and Recovery Act (RCRA) metals. MNA parameters were added for "performance monitoring" at select wells. In a letter from the NCDEQ-SWS dated April 18, 2008, NCDEQ-SWS agreed to the elimination of hydrogen, carbon dioxide, and volatile fatty acids from the semi-annual monitoring list, and to the completion of groundwater MNA modeling annually. This letter also specified that Moore County collect the full suite of "performance monitoring parameters" in April and October 2011, and present an MNA Corrective Action Evaluation Report (CAER) after completion of the October 2011 sampling event. Golder submitted a CAER report dated May 15, 2012. Subsequently, NCDEQ-SWS granted Moore County permission to continue MNA for another five-year period at the end of which another CAER report was required. Two additional surface water points (SW-3 and SW-4) were added to the compliance monitoring program upon approval of the May 2012 CAER. On March 10, 2016, Moore County met with NCDEQ-SWS to discuss groundwater impacts at the site and the effectiveness of previously implemented corrective actions. In this meeting and in a March 14, 2016, correspondence from NCDEQ-SWS, Moore County was asked to commence assessment monitoring at the C&D landfill or submit an alternate source demonstration (ASD) to demonstrate the impacts observed in the C&D January 14, 2020 4 Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 landfill monitoring network were from a source other than the C&D landfill. On behalf of Moore County, Golder submitted the ASD for the Active C&D Landfill, dated February 28, 2017, identifying the upgradient closed MSW landfill as the source of VOCs at downgradient C&D wells. In two letters dated September 28, 2017, the NCDEQ-SWS indicated that they would not approve the ASD for VOCs at the C&D Landfill, at that time. They also requested that Moore County implement landfill gas and groundwater corrective action at the closed MSW landfill; and commence assessment monitoring at the C&D landfill pursuant to 15A NCAC 13B .0545. On December 6, 2017, after additional communications and a meeting with NCDEQ-SWS, Moore County submitted a letter confirming their intention to comply with the NCDEQ-SWS requests and requested an extension to comply; which was approved by NCDEQ-SWS on December 11, 2017. On behalf of Moore County, Golder submitted: A CAER dated October 16, 2017, An Assessment Monitoring Work Plan, dated January 5, 2018. A Landfill Gas Remediation Plan dated January 31, 2018, A Groundwater Corrective Action Milestone Schedule, dated January 31, 2018 (which included the submission of the NC Solid Waste .0500 Groundwater Corrective Action Application), and In accordance with Golder's Assessment Monitoring Work Plan, dated January 5, 2018, monitoring wells MW-11 SR, MW-11 DR, and MW-15R were subsequently installed to replace monitoring wells MW-11 S, MW-11 D, and MW-15. The replacement wells were sampled in June 2018, as part of the first assessment monitoring event for the C&D landfill. Groundwater samples collected from assessment monitoring wells were analyzed for constituents listed in North Carolina Appendix II and the C&D landfill indicator parameters required by NCDEQ-SWS (e.g., chloride, manganese, sulfate, iron, alkalinity, total dissolved solids (TDS), and tetrahydrofuran). Samples from monitoring wells MW-6 and MW-7 were also analyzed for Appendix II constituents, to further assess whether the groundwater impacts detected at the C&D landfill were attributable to the upgradient MSW landfill. In a letter dated February 22, 2018, NCDEQ approved a request made by Moore County to decommission monitoring wells MW-16S and MW-16D and replace them in the groundwater monitoring network with MW-175, MW-17D, and MW-18 which were to be installed in conjunction with the permitting of new Cell VI of the C&D landfill. Between May 31 and June 4, 2018, monitoring wells MW-175, MW-17D, and MW-18 were installed, and monitoring wells MW-16S and MW-16D were properly abandoned. Monitoring wells MW-17S and MW-17D were first sampled during the routine semi-annual monitoring event conducted during November 2019. Monitoring well MW-18 was first sampled during the routine semi-annual monitoring event conducted in April 2020. During the April 2020 water quality monitoring event, groundwater monitoring was conducted at the closed MSW landfill in accordance with the approved Water Quality Monitoring Plan and Phase I of the Groundwater Corrective Action Milestone Schedule which was approved by NCDEQ-SWS on February 13, 2018. Phase I of the Groundwater Corrective Action Milestone Schedule included the following activities: Installation of the methane cut-off trench to the south of MW-15 (completed November 2, 2078) Replacement of MW-15 with MW-15R (completed June 1, 2018) Conversion of MW-15 to a compliance methane monitoring well (completed December 7, 2018) Continuation of MNA (as detailed in the approved Water Quality Monitoring Plan) January 14, 2020 Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 - In accordance with the approved Water Quality Monitoring Plan, dated December 10, 2019, hereafter referred to as the WQMP, monitoring wells in the MSW compliance network are corrective action MNA monitoring wells and are currently analyzed for VOCs listed in North Carolina Appendix I, RCRA metals, and an approved suite of MNA parameters (which includes chloride, ethane, ethene, methane, nitrate, sulfate, sulfide, total alkalinity, and total organic carbon). In addition, active C&D monitoring wells MW-4, MW-5, and MW-11SR are also sampled as corrective action MNA monitoring wells and analyzed for the same suite of MNA parameters. Analytical results for the April 2020 water quality monitoring event detected benzene at a concentration of 1.6 pg/L in monitoring well MW-18. Based on this apparent exceedance of the corresponding 2L Standard, a verification sampling event was conducted on June 5, 2020, with laboratory analyses reporting 1.2 pg/L Benzene. Based on the verified exceedance of the 2L Standard for benzene, an update of the Assessment Monitoring Program was required. On June 26, 2020, Golder installed new monitoring well MW-19 down -gradient (in the direction of contaminant migration) of monitoring well MW-18, near the facility boundary. Monitoring well MW- 19 was first sampled during the October 2020 water quality monitoring event. The October 2020 monitoring event represents the second semi-annual water quality monitoring event for the facility in 2020. The event was conducted in general conformance with the WQMP, with the addition of sampling monitoring well MW-19, and analyzing the samples for North Carolina Appendix II constituents. 3.0 Methods Employed 3.1 Groundwater Sampling Groundwater sampling took place between October 13 and October 15, 2020. The groundwater monitoring well locations are shown on Figure 1. S&ME personnel performed sampling in general accordance with the facility's updated WQMP. Groundwater samples were collected from monitor wells MW-1, MW-2, MW-3, MW-6, MW-7, MW-8, MW-9, and MW-15R representing the closed MSW landfill. Monitoring wells MW-4 and MW-11SR represent C&D monitoring wells also monitored as MNA performance wells for the MSW landfill. Monitoring wells MW-11 DR, MW-13SR, MW-13DR, MW-14, MW-17S, MW-17D, MW-18, and MW-19 represent the active C&D landfill. Monitoring well MW-5 was sampled as the background well for both landfills. A groundwater sample was also obtained the off -site water supply well located on the Blake property. Details regarding monitoring well construction and monitored aquifer units are shown in Table 1. Prior to collecting groundwater samples, the monitor wells were opened and allowed to equilibrate with atmospheric conditions before gauging the liquid level. Groundwater depths were measured to an accuracy of ±0.01 feet using an electronic water level indicator, which was decontaminated before its initial use and between measurements. The measurements were collected to calculate relative groundwater elevations, to develop a groundwater potentiometric map, and to estimate the hydraulic gradient and groundwater flow direction at the time of the sampling event. Water level measurements are presented in Table 2 and Figure 1. After collection of groundwater levels, low -flow sampling methods were followed to purge and sample groundwater from the monitoring wells. As purging proceeded, an YSI ProPlus0 multi -meter with a flow -through cell was used to measure field parameters that included pH, temperature, specific conductance, oxidation - January 14, 2020 Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 - reduction potential (ORP), and dissolved oxygen (DO). Turbidity was measured separately. The field data collected during sampling was recorded on the Low -Flow Groundwater Sampling Forms, included in Appendix I. A groundwater sample, for laboratory analysis, was collected after field parameters stabilized and the turbidity measurement was approximately 10 Nephelometric Turbidity Units (NTUs) or less. In accordance with the WQMP, water quality field parameters are considered stable once achieved for three consecutive measurements: Ph (+/- 0.2 S.U.), conductivity (+/- 5% of reading), temperature Ph (+/- 0.2 CO), and dissolved oxygen (+/- 10% of reading or 0.2 mg/L whichever is greater). ORP was measured and should fall within +/- 10 mV or reading; however, it was not a required stabilization parameter. Even with use of low -flow sampling methods, turbidity values obtained at some wells remained higher than target criteria. Accordingly, some samples were collected without meeting the turbidity goal. The field parameter measurements obtained are presented in Table 3. Groundwater samples from monitoring wells were collected using a peristaltic pump or bladder pump, and transferred directly into sample containers provided by the laboratory. Once filled, the sample containers were sealed, labeled, and placed in a cooler with ice. The samples were managed under chain -of -custody protocols and shipped to Environmental Conservation Laboratories, Inc. (ENCO), a North Carolina -certified laboratory. The groundwater sample obtained from the Blake residence water supply well (sample PW-1) was not obtained using low -flow sampling methods. The sample was collected directly from the spigot outside of the well house. Water was run for approximately 15 minutes prior to recording field parameters and sample collection. The sample was transferred directly into laboratory provided sample containers. Once filled, the sample containers were sealed, labeled, and placed in a cooler with ice. The samples were managed under chain -of -custody protocols and shipped to ENCO, a North Carolina -certified laboratory. One blind duplicate sample and one equipment blank sample were collected for quality assurance and quality control (QA/QC). One trip blank accompanied each laboratory package under standard chain -of -custody procedures delivered from the laboratory and returned to the laboratory. Samples were stored in laboratory provided coolers with ice immediately after collection. The samples were delivered to ENCO, a NCDEQ certified laboratory for analysis. The samples were maintained under chain -of -custody procedures through delivery to the laboratory. 3.2 Surface Water Sampling Surface water sampling took place on October 15, 2020. Four surface water samples (SW-1, SW-2, SW-3, and SW- 4) were collected from the locations shown in Figure 1. Sample SW-1 was collected from an unnamed tributary of Horse Creek, south of the MSW landfill. Sample SW-2 was collected from Horse Creek northwest of the C&D landfill. Sample SW-3 was collected downstream of SW-1, prior to the tributary discharging into Horse Creek. Sample SW-4 was collected from an unnamed tributary that drains areas north of both the C&D and MSW landfills. After collection, the surface water samples were placed in a cooler with ice and placed under chain -of -custody. Surface water samples SW-1, SW-2, SW-3, and SW-4 were analyzed for North Carolina Appendix I constituents and 1,4-Dioxane. January 14, 2020 Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 4.0 Site Hydrogeology 4.1 Groundwater Elevations and Flow Direction The facility is situated within the Inner Coastal Plain Province of North Carolina. The uppermost aquifer beneath the facility is unconfined, approximately 55 feet thick, and consist of sands with thin clay seams, and seams of fine sand; reportedly underlain by a basal restrictive clay layer. The surficial aquifer is recharged by inflow from up - gradient areas and by precipitation infiltration. The uppermost aquifer underlying the landfill is expected to discharge to the local surface water features including Horse Creek and it's unnamed tributaries in the vicinity of the landfill. Shallow monitoring wells were installed in the surficial aquifer. Static water level measurements collected during the October monitoring event (Table 1) were used to calculate the corresponding groundwater elevations based on surveyed top of casing (TOC) elevations. Groundwater elevations for the shallow water table monitoring wells and our interpretation of the groundwater surface expressed as a potentiometric map along with estimated groundwater flow directions shown on Figure 1. Based upon the groundwater potentiometric surface elevations, the overall shallow groundwater flow direction was estimated to be to the west. The hydraulic gradient (i) in the vicinity of a monitoring well was estimated by calculating the vertical difference between the groundwater elevation at a monitoring well and one or more nearby contour lines from Figure 1. This value was then divided by the horizontal distance measured from the well to the selected groundwater elevation contour line, utilizing a line formed perpendicular to the referenced groundwater elevation line. The calculated horizontal hydraulic gradient values determined for select wells are summarized in Table 4. 4.2 Groundwater Flow Velocity An approximate average linear groundwater flow velocity (V) was calculated using the following equation (Freeze and Cherry, 1979): V=Ki n where: V = Average linear groundwater flow velocity [feet per year (ft/yr.)] K = Hydraulic conductivity (ft/yr.) i = Flow gradient as a ratio (ft/ft) n = Effective soil porosity (percent) Aquifer rising and falling head tests were previously performed at the site by HDR. The aquifer test data were used to estimate the hydraulic conductivity of the sediments in the surficial aquifer intersected by the screened intervals of the monitoring wells tested. The hydraulic conductivity, K, values previously measured at the site ranged from 0.84 feet per day (feet/day) to 16 feet/day. An average hydraulic conductivity value of 12.2 feet/day was used for calculating the site -wide flow velocity. The average hydraulic gradient of 0.015 ft/ft was calculated from data presented in Table 4. An effective soil porosity, n, of 25% was used as the site -wide average. The average groundwater flow velocity, V, for the site, using the equation and input values above, was estimated to be 254 feet/year. The average groundwater flow velocity information is summarized in Table 4. January 14, 2020 Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 - 5.0 Results In general accordance with the WQMP, background and compliance groundwater monitor wells were sampled during the October 2020 sampling event. The samples were analyzed by ENCO as follows: MSW landfill groundwater samples from monitoring wells MW-1, MW-2, MW-3, MW-4, MW-6, MW-7, MW-8, MW-9 and MW15R were analyzed for constituents listed in the 40 CFR 258, Appendix I VOC analyte list using the analytical methods that included EPA Method 826013, 1,4-Dioxane by Method 8260D SIM, the Eight RCRA Metals using EPA Method 6010/6020 and EPA Method 7470A. Analyses for MNA parameters included chloride by EPA Method 300.0, nitrate by EPA Method 353.2, nitrite by EPA Method 353.2, sulfate by EPA Method 300.0, sulfide by EPA Method 300.0, Total Alkalinity by EPA Method 310.2, and Total Organic Carbon by EPA Method 9060A. Carbon Dioxide, Ethane, Ethene, and Methane by RSK 175. The active C&D landfill groundwater samples from monitoring wells MW-11 SR, MW-11 DR, MW-13SR, MW-13DR, MW-14, MW-17D, MW-18, MW-19, and MW-5 were analyzed for constituents listed in the 40 CFR 258, Appendix I analyte list using the analytical methods that included EPA Method 8260B (VOCs), total metals by EPA Method 6010, 6020 and EPA Method 7470A. Classic chemistry indicator parameters chloride by EPA Method 300.0, sulfate by EPA Method 300.0, sulfide by SM 4500S2-D-2011, Total Alkalinity by EPA Method 310.2 and Total Dissolved Solids by Method SM 2540-C2011. Plus 1,4-Dioxane by Method 8260D SIM. In addition, two C&D monitoring wells (MW-4, MW-11SR) are also used as MNA performance monitoring wells to assess groundwater impacts from the MSW landfill. The field measurements obtained are summarized on Table 3. A summary of constituents detected in groundwater is presented in Table 5. For comparison purposes, these results are shown with their respective 2L Standard, which were revised and became effective April 1, 2013. Where target groundwater constituents have no established 2L Standard, the Method Detection Limit (MDL) is the default 2L Standard. However, the NCDEQ-SWS has listed constituent concentrations protective of groundwater, referred to as the Ground Water Protection Standards (GWPS) established in accordance with the Solid Waste Management Rules, Section .1634(h), which are used as the action level for detections where no 2L Standard is established. The chain -of -custody forms and the laboratory reports from ENCO are provided in Appendix II. Copies of the laboratory reports are provided in Appendix II. Effective December 1, 2006, NCDEQ-SWS changed the standard limits for comparing constituent detections in laboratory analysis from the Practical Quantitation Limits (PQLs) established in 1994 to the Solid Waste Reporting Limits (SWRLs). On February 23, 2007, the Section further revised the reporting limits from the SWRL to the Solid Waste Section Limit (SWSL). The SWSL was defined as the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accuracy. In a memo dated May 29, 2018, the NCDEQ-SWS made a statement that technologies have advanced such over the past 12 years that the majority of the SWSLs are outdated. Given the rapid pace of technology, the NCDEQ- SWS decided that their attempt to continuously update and/or maintain the SWSLs is not warranted. As such, the use of SWSLs will be discontinued. According to the laboratory quality control performed by ENCO, detections above the MDL but below the PQL qualified as estimated values designated by the letter "J". January 14, 2020 Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 5.1 Groundwater Analytical Data - MSW Landfill The analytical data was reviewed by comparing constituent detections in the background and MSW compliance monitor wells to the laboratory's MDL. Multiple targeted constituents were detected above the MDL in one or more groundwater samples collected during the October 2020 monitoring event. Constituents with concentrations detected above the laboratory MDLs are summarized on Table 5. Appendix III contains a table providing historic groundwater analytical results for constituents with concentration detected above the MDL. The following table provides a summary of the monitoring well locations where target constituents were detected at concentrations greater than the 2L Standard or GWPS during the October 2020 monitoring event: October 2020 Groundwater Sampling Event Constituent Concentrations Detected Greater Than 2L Standard or GWPS Parameter 2L Standard or GWPS MSW Landfill Monitoring MW-2 MW-4 iLiL Wells MW-6 MW-7 iLiL MW-8 iL MW-9 iL MW-15SR iL 1,4-Dioxane 3 9.7 6.9 29 25 Benzene 1 2.5 2.8 4.0 1.2 Vinyl Chloride 0.03 1.1 5.4 1.1 Arsenic 10 64.8 Cadmium 2 2.16 Iron 300 1 397 Note: Blank cells indicate constituent concentrations less than the corresponding 2L Standard or GWPS. In accordance with NCDEQ-SWS guidance, where the 2L Standard or GWPS for a substance is less than the PQL, the detection of that substance at or above the PQL constitutes a violation of the 2L Standard or GWPS. The table above was prepared using this framework, which eliminates constituents reported with estimated concentrations ("J" values). Site -specific soil data presented in Golder's Second Semi -Annual 2076 Water Quality Monitoring Report indicated that concentrations detected in naturally occurring soils on site can account for arsenic concentrations that were measured in groundwater samples. Based on Golder's prior reported site specific assessment findings, arsenic appears to be naturally occurring. Cadmium has not been detected at monitoring well MW-6 since November 2016. Based on historic data, the reported concentration appears to be an outlier value. The first semi-annual monitoring event for 2021 will be utilized to verify this anomalous concentration. The 2L Standard exceedances for the VOCs summarized above are generally consistent with prior detections, several of which historically triggered regulatory requirements for implementation of Corrective Measures for the MSW landfill. In 2018, the NCDEQ-SWS requested that all MSW and C&D landfills begin to analyze samples for 1,4-Dioxane. Thus, historic data for detections of this parameter at the landfill are limited. Appendix IV contains time vs concentration charts for benzene, vinyl chloride, and 1,4-Dioxane. These charts were prepared to examine trends in concentration changes overtime. January 14, 2020 10 Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 5.2 Groundwater Analytical Data - C&D Landfill The analytical data was reviewed by comparing constituent detections in the background and C&D landfill compliance monitor wells to the laboratory's MDL. Multiple targeted constituents were detected above the MDL in one or more groundwater samples collected during the October 2020 monitoring event. Constituent concentrations detected above the laboratory MDLs are summarized on Table 5. Appendix III contains a table providing historic groundwater analytical results for constituents with concentration detected above the MDL. The table below provides a summary of the monitor well locations where target constituents were detected at concentrations greater than the 2L Standard or GWPS during the October 2020 monitoring event: October 2020 Groundwater Sampling Event Constituent Concentration Detected Greater Than 2L Standard or GWPS Parameter 2L Standard or GWPS MW-11SR (Ng/L) :. Landfill MW-11DR (Ng/L) Monitoring MW-13SR (Ng/L) Wells MW-13DR (Ng/L) MW-14 (Ng/L) MW-17S (Ng/L) MW-17D (Ng/L) MW-18 (Ng/L) 1,4-Dioxane 3 5.4 4.4 3.4 14 6.8 10 Benzene 1 3.2 1.9 2.2 Vinyl Chloride 0.03 2.4 1.8 2.3 1.9 I ron 300 119,000 83,800 66,200 7,600 139,000 14,400 2,500 103,000 Manganese 50 294 180 569 123 183 164 227 Note: Blank cells indicate constituent concentrations less than the corresponding 2L Standard or GWPS. In accordance with NCDEQ-SWS guidance, where the 2L Standard or GWPS for a substance is less than the PQL, the detection of that substance at or above the PQL constitutes a violation of the 2L Standard or GWPS. The table above was prepared using this framework, which eliminates constituents reported with estimated concentrations ("Y values). Appendix IV contains time vs concentration charts for benzene, vinyl chloride, and 1,4-Dioxane. These charts were prepared to examine trends in concentration changes overtime 5.3 Groundwater Analytical for Monitored Natural Attenuation Parameters Groundwater analytical results for monitoring wells involved in Performance Monitoring for MNA parameters are summarized in Table S. 5.4 Groundwater Analytical - Private Water Well Analytical results for the off -site private water well located on the Blake property to the north of the MSW landfill (sample ID = PW-1), detected no targeted volatile organic compounds, including 1,4-Dioxane. Inorganic constituents, barium and lead were detected at 19.0 pg/I and 11.4 pg/L, respectively. The detected concentrations were less than their corresponding 2L Standards. 5.5 Surface Water Analytical Data Surface water samples were collected from the four designated sample locations illustrated on Figure 1. Horse Creek located west of the landfill is a stream classified by NCDEQ as a WSII, Water Supply. Laboratory analysis of January 14, 2020 11 Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina I S&ME Project No. 4358-20-043A, Task 01 ! the samples collected were compared to their respective 15A NCAC 2B (revised 6-10-2019) water quality standards for class WS surface waters (213 Standards). Table 6 provides a summary of constituents detected during the October 2020 monitoring event. The following constituents were detected at concentrations greater than their respective 2B Standards during the October 2020 event: October 2020 Surface Water Sampling Event Constituent Concentration Detected Greater Than 2B Standards It is noted that 1,4-Dioxane was detected at surface water sample location SW-2, at an estimated concentration of 0.378 pg/L. This concentration is greater than the corresponding North Carolina In -Stream Target Value for Surface Waters set at 0.35 pg/L for Class WS (I-V) surface waters; however, no 2B Standards currently exists. 5.6 Quality Control Quality assurance and quality control of field sampling methods and analytical test methods were assessed by collecting and analyzing one duplicate sample, one equipment blank sample, and one trip blank sample. The duplicate and equipment blank samples were analyzed for Appendix I constituents by the same methods and for the same target constituents as the record samples. Duplicate sample analysis documents the consistency of field sampling methods and the consistency of laboratory testing between samples. Equipment blank sample analysis documents the quality of sampling equipment and decontamination procedures used to reduce the potential of cross -contamination or carry-over effects from sampling equipment used on -site. The trip blank is analyzed for VOCs to document the effect of external conditions on samples/sample containers during lab pack preparation and transportation to and from the site. The concentrations of Appendix I VOCs and inorganic compounds detected in the record and in the duplicate samples collected from monitor well MW-14 were within an acceptable tolerance level and indicate a suitable replication of results from the test procedures. No targeted constituents were detected at concentrations above their respective laboratory method detection limits in the equipment blank sample. In the trip blank sample, no targeted constituents were detected above their respective laboratory MDLs. Some technical limitations exist in the laboratory's reporting of MDLs. MDLs for some VOCs and some inorganic constituents are above the applicable standards. The MDL for vinyl chloride (0.32 pg/L), cobalt (1.4 pg/L), and vanadium (1.4 pg/L) in groundwater are greater than the 2L Standard of 0.03 pg/L for vinyl chloride and the GWPSTs of 1.0 pg/L for cobalt and 0.3 pg/L for vanadium. Therefore, vinyl chloride, cobalt, and vanadium may have been present at concentrations above their respective 2L Standard/GWPS, but were reported as being below their respective MDLs. January 14, 2020 12 Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 - 6.0 Discussion of Results Moore County continues with assessment monitoring at the C&D Landfill. Monitored Natural Attenuation (MNA) is the selected groundwater remedy for the closed MSW landfill monitoring. MNA "Performance Monitoring" continues at MSW wells and select C&D wells. The results of the October 2020 sampling event continue to show that groundwater near the Moore County Landfill has been impacted by a release of constituents from the facility. Impacted groundwater at the facility does not appear to be adversely affecting surface water at the site. Benzene and vinyl chloride in the vicinity of the MSW landfill generally exhibit trends of stable or declining concentrations over time, with a few exceptions. Concentrations of these constituents are not rising immediately down -gradient of the source area. The 2L Standard exceedance for benzene at monitoring well MW-18 will be closely monitored, along with groundwater quality at monitoring well MW-19 installed further down -gradient. The size of the data set for 1,4-Dioxane is currently insufficient for accurate trend analysis. In view of the VOC concentration trends over time, Moore County plans to continue Assessment Monitoring for the C&D landfill and MNA monitoring of the closed MSW landfill; unless evidence of increasing VOCs concentrations are confirmed or unless Moore County is directed by NCDEQ to proceed to the alternate groundwater remedy. Moore County is proactively evaluating options for alternate groundwater corrective actions that may be appropriate for the CAP contingency plan, including options that would aid in the management of landfill gases; which can contribute to groundwater exceedances. 7.0 References Department of Environment and Natural Resources, Division of Water Quality, 75A NC Administrative Code Subchapter 2B .0200 Classifications and Water Quality Standards Applicable to Surface Waters and Wetlands of NC, November 2019. Surface Water Standards Tables updated 06-10-2019. Department of Environment and Natural Resources, Division of Water Quality, 75A NC Administrative Code Subchapter 2L .0200 Groundwater Quality Standards, April 2013. Department of Environment and Natural Resources, Division of Waste Management, 75A NC Administrative Code Subchapter 73B .7634(h) Solid Waste Groundwater Protection Standard, Solid Waste Management Rules, November 2004. Golder Associates NC, Inc. (Golder), Alternate Source Demonstration for Active C&D Landfill, Moore County Construction and Demolition Landfill, NC SWP# 63-01, Submitted to NC DEQ: February 28, 2017. Golder Associates NC, Inc. (Golder), Assessment Monitoring Work Plan, Moore County Construction and Demolition Landfill, NC SWP# 63-01, Submitted to NC DEQ: January 5, 2018. Golder Associates NC, Inc. (Golder), Corrective Action Evaluation Report, Moore County Landfill, NC SWP# 63-01, Submitted to NC DENR: May 15, 2012. January 14, 2020 13 Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina I S&ME Project No. 4358-20-043A, Task 01 - Golder Associates NC, Inc. (Golder), Groundwater Corrective Action Evaluation Report, Moore County Landfill, NC SWP# 63-01, Submitted to NC DEQ: October 16, 2017. Golder Associates NC, Inc. (Golder), Groundwater Corrective Action Milestone Schedule, Moore County Closed MSW Landfill, NC SWP# 63-01, Submitted to NC DEQ: January 31, 2018. Golder Associates NC, Inc. (Golder), Landfill Gas Remediation Plan, Moore County Closed MSW Landfill, NC SWP# 63-01, Submitted to NC DEQ: January 31, 2018. Golder Associates NC, Inc. (Golder), Request for Extension, Moore County Landfill, NC SWP# 63-01, Submitted to NC DEQ: December 6, 2017. Golder Associates NC, Inc. (Golder), Request for Monitored Natural Attenuation Parameter Modification, Moore County Landfill, NC SWP# 63-01, Submitted to NC DENR: January 22, 2008. Golder Associates NC, Inc. (Golder), Response to Letters Received from NC DEQ Dated September 28, 2077, Moore County Landfill, NC SWP# 63-01, Submitted to NC DEQ: October 26, 2017. Golder Associates NC, Inc. (Golder), Second Semi -Annual Water Quality Monitoring Report, Moore County Landfill, NC SWP# 63-01, Submitted to NC DEQ: March 29, 2017. Golder Associates NC, Inc. (Golder), Water Quality Monitoring Plan, Moore County Landfill, NC SWP# 63-01, Submitted to NC DEQ: Submitted to NC DEQ: December 10, 2019. HDR Engineering, Inc. of the Carolinas (HDR), Addendum to Plan to Address Potential Contamination, Moore County Landfill, NC SWP# 63-01, Submitted to NC DENR: March 20, 2000. HDR Engineering, Inc. of the Carolinas (HDR), Assessment of Corrective Measures Report, Moore County Landfill, NC SWP# 63-01, Submitted to NC DENR: July 29, 2005. HDR Engineering, Inc. of the Carolinas (HDR), Phase I Environmental Assessment, Moore County Landfill, NC SWP# 63-01, Submitted to NC DENR: November 30, 1999 HDR Engineering, Inc. of the Carolinas (HDR), Water Quality Monitoring Plan, Moore County Landfill, NC SWP# 63- 01, Submitted to NC DENR: July 20, 2006. Joyce Engineering, Inc., Contingency Plan Update and Implementation Plan - Revised, Moore County Landfill, NC SWP# 63-01, Submitted to NC DENR: May 16, 2013. North Carolina Department of Environment, Health, and Natural Resources (NC DEHNR), Division of Solid Waste Management, Water Quality Monitoring at Moore County Sanitary Landfill, Moore County Landfill, NC SWP# 63- 01, NC DEHNR to Moore County: January 23, 1996. January 14, 2020 14 Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Closed MSW and Active C&D Landfills Aberdeen, North Carolina S&ME Project No. 4358-20-043A, Task 01 - North Carolina Department of Environment and Natural Resources (NC DENR), Division of Waste Management, Request for Monitored Natural Attenuation Parameter Modification, Moore County Landfill, NC SWP# 63-01, NC DENR to Moore County: April 18, 2008. North Carolina Department of Environmental Quality (NC DEQ), Solid Waste Section, Division of Waste Management, Alternate Source Demonstration, Moore County Construction and Demolition Landfill, NC SWP# 63- 01, NC DEQ to Moore County: September 28, 2017. North Carolina Department of Environmental Quality (NC DEQ), Solid Waste Section, Division of Waste Management, Groundwater Corrective Action and Landfill Gas Corrective Action, Moore County Closed MSW Landfill, NC SWP# 63-01, NC DEQ to Moore County: September 28, 2017. North Carolina Department of Environmental Quality (NC DEQ), Solid Waste Section, Division of Waste Management, Groundwater Corrective Action Milestone Schedule, Moore County Closed MSW Landfill, NC SWP# 63-01, NC DEQ to Moore County: February 13, 2018. January 14, 2020 15 TABLE 1 Active Monitoring Well Construction Information Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A = 0 III MW-1 06/05/87 Ad 508605.64 inates 1854636.41 Ground Surface Elevation 390.70 Measuring Point Elevation 392.87 Total Well r- 20 Well Depth 370.70 ell Di:ete, 2 Screened Interval g 6.97 - 17.07 Screened Interval 383.73 - 373.63 Geology of Screened Interval Sand Monitored Landfill Unit MMJ MSW Landfill MW-2 06/06/87 508508.07 1853819.73 373.39 375.50 20 353.39 2 7.52-17.77 365.87 - 355.62 Sand MSW Landfill MW-3 06/06/87 508781.79 1852845.34 362.00 363.82 16.5 345.50 2 5.75 - 15.88 356.25 - 346.12 Sand and Silty Clay MSW Landfill MW-4 06/06/87 509793.80 1853641.22 363.40 366.19 15 348.40 2 4.28 -14.09 359.12 - 349.31 Sand and Silty Clay C&D Landfill MW-5 06/06/87 510970.55 1853091.84 384.06 386.61 20 364.06 2 6.96-17.21 377.10 - 366.85 Sand and Clayey Sand Background MW-6 03/06/95 510385.96 1853881.79 403.50 405.86 20 383.50 2 5.00 - 20.00 398.50 - 383.50 Sand to Silty Sand MSW Landfill MW-7 03/06/95 509783.24 1853820.43 399.20 402.01 20 379.20 2 4.00 - 19.00 395.20 - 380.20 Sand, Silt, Silty Sand, Clay MSW Landfill MW-8 03/06/95 509384.99 1853844.10 395.20 397.85 20 375.20 2 5.00 - 20.00 390.20 - 375.20 Sand, Silt, Silty Sand, Clay MSW Landfill MW-9 03/06/95 508964.80 1854268.28 403.70 406.06 30 373.70 2 15.00 - 30.00 388.70 - 373.70 Silty Sand MSW Landfill MW-11SR O6/01/18 510452.38 1852905.36 383.41 386.13 28 355.41 2 18.00 - 28.00 358.13 - 368.13 Clayey Sand C&D Landfill MW-11DR 05/31/18 510453.00 1852911.56 383.41 386.36 44 339.41 2 34.00-44.00 342.36 - 332.36 Sand C&D Landfill MW-13SR 06/24/20 509541.34 1853156.68 383.87 386.57 20 363.87 2 10.00-20.00 373.87 - 363.87 Sand C&D Landfill MW-13SD O6/24/20 509549.23 1853164.04 383.31 385.99 40 343.31 2 30.00-40.00 353.31-343.31 Sand/Clay C&D Landfill MW-14 09/16/96 510056.32 1853641.99 397.88 400.58 20 377.88 2 5.00 - 20.00 392.88 - 377.88 Sand to Silty Sand Upgradient of C&D Landfill MW-15 09/19/96 510597.22 1854401.13 429.31 431.10 35 394.31 2 20.00 - 35.00 409.31 - 394.31 Sand to Silty Sand MSW Landfill MW-15R 05/29/18 510589.03 1854391.51 428.81 431.48 47 381.81 2 37.00 - 47.00 384.48 - 374.48 Sand MSW Landfill MW-17S 05/31/18 509704.03 1852096.70 371.45 374.16 18 353.45 2 8.00 - 18.00 363.45 - 353.45 Sand C&D Landfill MW-17D 06/01/18 509693.71 1852101.52 372.05 374.56 34 338.05 2 29.00 - 34.00 343.05 - 338.05 Clay/Sandy-Clay C&D Landfill MW-18 06/04/18 509369.85 1852249.28 365.35 368.50 13 352.35 2 5.00 - 13.00 360.35 - 352.35 Gravelly Sand, Sand, Sandy Clay C&D Landfill MW-19 06/25/20 509324.26 1852158.78 363.95 366.67 13 350.95 2 5.00-13.00 358.95 - 350.95 Sand C&D Landfill GP-10R O6/25/20 508889.16 1855952.87 431.90 434.21 15 416.90 2 5.00-15.00 426.90 - 416.90 Sand MSW Landfill GP-13R 05/31/18 509405.06 1852208.08 367.1 370.29 10 357.10 2 3.00 -10.00 364.10 - 357.10 Sand C&D Landfill GP-14R 05/30/18 509680.01 1852109.63 372.05 374.78 10 362.05 2 3.00-10.00 369.05 - 362.05 Clayey Sand to Sand C&D Landfill GP-15R 06/04/18 510038.89 1852041.09 364.85 367.73 10 354.85 2 3.00 -10.00 361.85 - 354.85 Sandy Clay, Gravelly Sand C&D Landfill GP-19 06/25/20 510494.25 1853794.49 397.08 399.33 10 387.08 2 5.00-10.00 1 393.08 - 387.07 Sand MSW Landfill Notes: 1.) ft AMSL = feet above mean sea level 2.) ft BGS = feet below ground surface 3.) Well construction information for monitoring wells MW-1 through MW-16S/D collected from boring logs and well construction records from HDR Engineering, Inc. of the Carolinas July 2006 Water Quality Monitoring Plan. TOC and Ground Elevations are taken from the July 2005 Assessment of Corrective Measures Report and/or well records where available. 4) Well construction information for monitoring well MW-19 obtained from boring logs and well construction records from Golder, Inc. TABLE 2 Groundwater Elevation Data Water Quality Monitoring Report, October 2020 Monitoring Event Moore Count Landfill, NC Solid Waste Permit No. 63-01 Y � Aberdeen, Moore County, North Carolina S&ME Project Number 4358-20-043A Well ID background Wel MW-5 ' roundwater Monitoring Network � IW-6 TOC Elevatio (ft AMSL) g6.61 , ' �05.86 IP Measurement -FGWE r ' r DTW'UMWE (ft AMSL) (ft) Mm I (ft AMSL) GWE -�FGWE-'I�WIGWE (ft AMSL) (ft) mmmm® (ft AMSL) (ft) DTW. WE DTW G1������GWE (ft AMSL) (ft) AMSL) (ft) (ft AMSL) (ft) ®MM� (ft AMSL) (ft) DTW (ft AMSL) (ft) � Notes: 1.) ft AMSL = feet above mean sea level 2.) TOC = top of casing 3.) GWE = Groundwater Elevation (calculated) 4.) DTW = Depth to Water TABLE 3 Groundwater Field Parameter Data Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A pH S.U. 10/14/20 6.4 6.1 5.3 6.4 5.9 7.6 6.3 6.1 6.0 6.5 Specific Conductance us/cm 10/14/20 754 318 88 944 582 328 1031 353 238 1487 Temperature Celsius 10/14/20 19.2 21.3 21.0 19.5 22.1 21.4 22.6 21.1 20.4 19.9 Turbidity NTU 10/14/20 3.94 8.25 73.0 2.45 9.66 57 7.67 8.39 9.89 0.58 Oxidation Reduction Potential my 10/14/20 -81 -45 99 -88 67 -143 18 35 112 -103 Dissolved Oxygen I mg/L 1 10/14/20 1 0.1 1 0.3 1 0.2 0.5 1 1.3 1 1.2 0.10 0.3 4.6 1.6 Notes: 1.) mg/L = milligrams per liter 2.) ND = not detected at or above the laboratory reporting limit 3.) NM = not measured 4.) uS/cm = microseimens per centimeter 5.) NTU = Nephelometric Turbidity Units 6.) S.U. = Standard Units 7.) Samples collected using low -flow purge and sample techniques (when possible). TABLE 4 Groundwater Conductivities, Gradients and Calculated Flow Velocities Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project Number 4358-20-043A = q- Well Hydraulic Cond. Eff. Porosity ID .. MW-1 1.6E+01 25% October Gradient 0.011 Flow Velocity 266 MW-2 1.6E+01 25% 0.024 565 MW-3 3.4E+00 25% 0.023 112 MW-4 7.7E+00 25% 0.013 150 MW-5 7.1 E+00 25% 0.020 209 MW-6 9.8E+00 25% 0.019 275 MW-7 8.4E-01 25% 0.012 15 MW-8 1.8E+01 25% 0.008 199 MW-9 4.2E+01 25% 0.012 727 MW-14 8.8E+00 25% 0.021 270 MW-15 4.8E+00 25% 0.001 10 Mean Values = 1.22E+01 25% 0.015 254 Notes: (1) Hydraulic Conductivity was calculated from slug tests performed by HDR (2) Effective porosity is an estimated value, actual values will vary (3) Hydraulic gradient calculated by measuring linear feet along a line between selected monitor well and contour line. (4) Seepage velocity v = (K*i)/ne Z:\Share \SME\Opa\ENV Projeota\2020W353-20-043A Moore County Roatina LFG & WO Monitoring\Task 01 - Semi -Annual Water Ooality FV 2020-2021\W orking_D—m-, Fall Event\2020-10 W OMR Tables_20210114.,11,, TABLE 5 Groundwater Analytical Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Detected Monitoring Constituent/Parameter Arsenic Units u /L Sam •. 10/13/20 Illfw9p, 7.6 10 10 Background Monitoring Well MW-5 ND •• ND ND Active •• ND C&D Monitoring ND Wells ND r ND MW-18 ND MW-19 ND • Wells• Performance for the Closeuill MW-4 ND Wells ND MW-1 ND Closed MW-2 ND MSW Monitoring MW-3 ND Wells & MNA MW-6 Performance MW-7 Monitoring Wells MW-8 MW-9 ND 64.8 MW-15R ND Private Well im ND ND ND Barium u /L 10/13/20 1.1 10 700 15.4 52.7 19.1 44.0 44.6 87.9 33.4 83.8 59.5 25.9 72.8 26.7 34.7 33.9 41.0 34.4 75.6 95.5 27.5 19.0 Cadmium u /L 10/13/20 0.36 1 2 ND 1.09 1.03 ND 1.93 ND ND 1.26 ND ND 1.11 ND ND ND 2.16 1.57 1.67 0.662 J 1.92 ND Chromium u /L 10/13/20 1.4 10 10 ND ND ND ND ND ND 1.59 J ND ND ND ND NO ND ND ND ND ND ND NO ND Cobalt u /L 10/13/20 1.4 10 1 ND 1.49 J ND 1.51 J ND 1.48 J ND ND ND ND -- -- -- -- -- -- -- -- -- Copper u /L 10/13/20 1.6 10 1000 ND ND ND ND 3.26 J ND 2.97 J 1.99 2.03 J 3.81 J ND -- -- -- -- -- -- Lead u /L 10/13/20 3.1 10 15 ND 6.92 4.49 J ND 11.2 ND ND 7.49 ND ND ND ND ND ND 9.32 J 10.9 9.86 6.58 J 9.94 J 11.4 Vanadium u /L 10/13/20 1.4 10 0.3 ND 1.70 J 2.15 ND 4.83 J ND ND 2.34 J ND ND 2.32 J Zinc u /L 10/13/20 4.4 10 1000 ND ND 455 ND 4.83 J ND ND ND ND ND ND -- -- -- -- -- -- -- -- -- Iron u /L 10/13/20 22 50 300 ND 83,800 66,200 7,600 139,000 14,400 2,500 103,000 NO 397 119,000 Manganese u /L 10/13/20 1.5 10 50 2.85 J 180 569 123 183 164 47.8 227 ND 11.0 294 Benzene u /L 10/13/20 0.15 1 1 ND 1.9 ND ND 2.2 ND ND 0.99 J ND ND 3.2 ND 0.54 J ND 2.5 ND 2.8 4.0 1.2 ND Chlorobenzene u /L 10/13/20 0.17 1 50 ND ND ND ND 5.8 ND ND 0.88 J ND ND 1.9 NO 1.2 ND 1.6 ND 4.3 8.9 ND ND 1,2-Dichlorobenzene u /L 10/13/20 0.19 1 20 ND ND ND ND 1.6 ND ND 0.52 J ND ND ND ND ND ND ND ND 0.54 J ND ND 1,4-Dichlorobenzene u /L 10/13/20 0.19 1 6 ND 2.6 ND ND 5.1 ND ND 1.8 ND ND 3.1 ND 0.59 J ND 1.7 ND 5.3 3.1 0.73 J ND 1,1,-Dichloroethane u /L 10/13/20 0.13 1 6 ND 0.43 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.56 J ND ND ND cis-1,2-Dichloroethene u /L 10/13/20 0.15 1 70 ND 3.0 ND 0.96 J 1.7 ND ND 3.8 ND ND 1.7 ND ND ND 3.1 7.8 0.43 J 0.74 J 1.6 ND Eth (benzene u /L 10/13/20 0.13 1 600 ND ND ND ND 0.67 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Naphthalene u /L 10/13/20 0.11 1 6 ND ND ND ND 0.49 J ND ND ND ND -- -- -- ND Toluene u /L 10/13/20 0.14 1 600 ND ND ND ND 0.48 J ND ND ND ND ND ND ND ND ND 0.40 J ND 0.51 J 0.43 J ND ND Vinyl chloride u /L 10/13/20 0.32 1 0.03 ND 1.8 ND ND 2.3 0.79 J ND 1.9 ND ND 2.4 ND ND ND 1.1 5.4 ND ND 1.1 ND X lenes (Total) u /L 10/13/20 0.45 3 500 ND ND ND 0.49 J ND ND ND ND ND ND ND ND ND ND 2.2 0.46 J ND ND 1,4-Dioxane u /L 04/07/20 0.8 2.0 3 ND 4.4 3.4 2.5 14 2.3 6.8 10 2.8 1.3 5.4 ND 9.7 1.0 J 2.0 6.9 29 25 ND ND Tetrah drofuran u /L 10/13/20 0.53 1.0 NS ND 2.4 ND ND 3.3 ND ND ND ND ND 5.8 -- -- -- -- -- -- -- -- ND Sulfide u /L 10/13/20 100 10 NA ND 22,000 J ND ND 120,000 Monitored ND Natural Attenuation ND Parameters 42 J ND ND 17 J ND ND ND 160.00 ND 78 J 140 27 J Chloride u /L 10/13/20 2200 5000 NA 2,500 J 21,000 7,700 5,800 52,000 22,000 3,000 41,000 14,000 8,900 27,000 2,300 J 38,000 5,500 13,000 20,000 69,000 100,000 D 2900 J Nitrate as N u /L 10/13/20 41 100 NA 380 J -- -- 2,300 J 90 J 850 130 ND 110 200 120 100 510 Nitrite as N u /L 10/13/20 17 100 NA ND -- -- -- -- -- -- -- -- ND ND ND ND ND ND ND ND ND ND Total Dissolved Solids u /L 10/13/20 50000 50000 NA ND 250,000 96,000 50,000 240,000 350,000 200,000 430,000 160,000 150,000 550,000 Sulfate as SO4 u /L 10/13/20 2900 1 5000 NA ND 1 13,000 16,000 9,100 1 7,100 99,000 35,000 1 72,000 12,000 32,000 1 ND 8,000 5,500 1 8,400 7,200 ND ND ND 7,200 Total Alkalinity as CaCO3 u /L 10/13/20 14000 15000 NA ND 220,000 49,000 ND 190,000 140,000 120,000 290,000 95,000 39,000 620,000 ND 180,000 ND 190,000 120,000 240,000 D 830,000 96,000 Total Organic Carbon u /L 10/13/20 540 1000 NA ND -- -- -- -- -- -- -- 11,000 22,000 990 J -- 930 J 30,000 21,000 21,000 37,000 2,600 Nitrate/Nitrite as N u /L 10/13/20 41 100.0 NA 380 J 2,300 J 90 J 850 130 -- 110 200 120 100 510 Ethane u /L 10/13/20 5.1 6 NA ND -- -- -- -- -- -- -- -- ND ND ND -- ND ND ND ND ND -- Ethene u /L 10/13/20 5.1 6 NA ND ND ND ND ND ND ND ND ND ND Methane u /L 10/13/20 5.1 6 NA ND -- -- -- -- -- -- -- -- ND 4,460 ND -- ND 3,680 6,150 5,680 DI 3,200 -- Carbon dioxide ug/L 10/13/20 2070 2500 NA 21,600 573,000 55,700 5,240 47,500 429,000 DI 406,000 DI 462,000 J 729,000 DI 425,000 Notes: 1.) ug/L = Micrograms per liter 2.) ND = Not detected at the stated reporting limit 3.) NA = Not Applicable 4.) J = Estimated concentration reported below Solid Waste Section Limit 5.) -- = Analysis Not Requested 6.) Bold = Concentration above the current NC 2L Groundwater Standard or NC 2L IMAC Groundwater Standard 7.) Shaded and Bold = Concentration above the current NCAC 2L Groundwater Standard (21- Std.) or NC 2L IMAC Groundwater Standard or NC Groundwater Protection Standards (G WPS) 8.) GWPS = Solid Waste Section Groundwater Protection Standard 9.) PQL = Practical quantitation limit - lab specific limit 10.) MDL = Method Detection Limit Z:VSbare ME\Ops1ENVProjecis12020W3M-20-043A Moore CountyR-ineLFG&WO MoniWring\Tesk 01-Semi-Mnual Water Quality FY 2020-2021\Working Documents Fall Event12020-10 WOMR Tables 20210114AW Page 5Of6 TABLE 6 Surface Water Monitoring Analytical Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project Number 4358-20-043A =0 Method 15A NCAC 213 Surface Water Standards Upstream Downstream Detected Constituent Reporting Sample Detection NC Units Date Standard Acute* Chronic* SW-1 SW-2 SW-3 SW-4 Limit Protective* Notes: 1.) MDL = Method Detection Limit 2.) ug/L = micrograms per liter 3.) ND = Not detected at or above MDL 4.) J = Estimated value 5.) -- = Not applicable 6.) Shaded = Constituent exceeds applicable Surface Water Standard 7.) Blanks = Field, trip and method blanks 8.) Surface Water Standards based on WS-II, High Quality Water Classification for Horse Creek and its tributary per 15A NCAC 02B. 9.) SW Standard for lead is a Narrative Standard per 15A NCAC 02B .0211 10.) Upstream and downstream designations based on inspection of site conditions and flow regimes. Reports prior to October 2009 had the designations inadvertently switched. 11.) For standards with both acute and chronic listed, they are shown 12.) NC Protective values are listed within 15A NCAC 02B, but they are not 2B Standards Z\5na,ed\SM a NV� �2020�4358-2o-043AM... -R-1-LFG&WQM-t-g-ko1----wae,oaryF12ozo-20211W.-9o--t.F.11E-zozo-10woMRT.11-2515114 w=. I e � •ems 8 I 34a= I � ❑ vv KE RESIDE AWL TORE i 1 � BLA RESIDENCE (CRAWL SPACE MONITORED) ✓�. 36,.a Cl% / / Y —, Co I Up 440 P-13 398.93 J� aso —_� // o l�l CD \s GROUND OBSCURED MW-11SR - ------ ♦ // sj0 371. 1 SEE ACCURACY NOTE / ° u ♦♦♦ 370.81 ♦ —8Ei71 10 7 / y ^MW-115/' o°MW 6 �'161 4 b 2 1 0°0 0 // .x` V 8 0 0 loo o ° o W.9 �\ ACCT &DE ��z� LANDFILL t 00 I ' \ 32 CLOSED Y 6 -- I I o MW-71� \ _LANDFILL � o _ 3804� �� 31 MW_ 7 ',MW-17D ,: CELL6 \ II'� I , w° 363.30 �. . 141 � � � I � � � ° to � � 'A NDONED) \\ ` ' ob..°..- ` 30 14�W74116r Nx A �G � .ate L� � . I -- _ W 1 P-13 � .- 60.2 62.04 ABANDONED)" II _ ♦ �_� v g GPa� O� �` MAINTEEN NCE SHOP \ ` \ 1 Ir o _ q. `\ 0 o° 383.1.11 0 S. 1 �� b ' - o 0 0 SCALEHOUSE 5 .84 TRANSFER ST OFFICE 0 -p o 10 ]UND OBSCURED ACCURACY NOTE -:.ss \e,,,,� O' 0 - ■ 0 ____�__'/ O W-6810 2o Sw-1 ❑ �' m m PARCEL BOUNDARY .4 GROUNDWATER FLOW DIRECTION ■ m m m m ■ APPROXIMATE LIMITS OF WASTE 357.84 MEASURED GROUNDWATER ELEVATION IN MONITORING WELL EXISTING 2 FT GROUND SURFACE CONTOUR O MONITORING WELL EXISTING 10 FT GROUND SURFACE CONTOUR OO ABANDONED MONITORING WELL STREAM, POND AND WETLAND LIMITS PASSIVE LANDFILL GAS VENTS 0 400 800 = EXISTING ROAD JL( LANDFILL GAS TRENCH VENT MSW LANDFILL COMPLIANCE BOUNDARY A METHANE PROBE (INSTALLED JUNE 2020) C&D LANDFILL COMPLIANCE BOUNDARY A ABANDONED METHANE PROBE L GRAPHIC SCALE (IN FEET) 365 — — — POTENTIOMETRIC GROUNDWATER CONTOUR (5ft INTERVAL) A METHANE PROBE I J Z LL 00 z Q Q J U 2 H � 0 0LU LLj z cf� Lu SCALE: AS SHOWN DATE: NOV. 2020 PROJECT NUMBER 4358-20-043 FIGURE NO. vi Appendices Appendix I -Sampling Forms • • •I I Z IC11 101 Moore County Landfill 4358-20-043A phase 11 Purge Date: October 14, 2020 Project Name: Project Location: Project Number: Source Well: MW-1 Purge Time: 30 Minutes Locked?: Yes Sample Date: October 14, 2020 Sampled By: Gary Simcox Sample Time: 15:45 Weather: Sunny Air Temp: 75° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals a 5 minutes an purge volumes >_ 1 ow -through cell volume) Final: 15:40 0.8 100 10.64 20.5 4.8 48 3.3 204 6.0 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 15:45 Sample End Time: 16:05 Analytical Data Name (1) Gary Simcox Signature Date 10/16/2020 Notes: I tested for Ferrous Iron using a HACH Model IR-18 (0.0 mg/L) Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 10.45 ft-TOC Total Well Depth: 19.30 ft-TOC Height of Water Column: 8.85 feet Screen Length: 10 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.4 Gal 3 *Well Volume 4.33 Gal 5 *Well Volume 7.22 Gal Purge Method: Peristaltic Pump Start Time: 15:10 End Time: 15:40 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 15.0 ft-TOC Water Column Above Pump Intake: 4.55 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 11.59 ft-TOC Comments: Final Volume Purged: 0.8 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp ('C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 15:10 0.0 --- --- --- --- --- --- --- --- Start Purging 15:20 0.3 100 10.61 20.6 4.8 52 2.2 181 10.5 15:25 0.4 100 10.62 20.6 4.8 50 2.1 187 8.76 15:30 0.5 100 10.64 20.6 4.7 49 3.2 195 7.47 15:35 0.7 100 10.63 20.5 4.7 48 3.2 200 6.91 15:40 0.8 100 10.64 20.5 4.8 48 3.3 204 5.99 Method Qty Container Preservative Method Qty Container Preservative 82606 SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 • • •I I Z IC11 101 Moore County Landfill 4358-20-043A phase 11 Purge Date: October 14, 2020 Project Name: Project Location: Project Number: Source Well: MW-2 Purge Time: 30 Minutes Locked?: Yes Sample Date: October 14, 2020 Sampled By: Gary Simcox Sample Time: 17:15 Weather: Sunny Air Temp: 75° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals a 5 minutes an purge volumes _> 1 low -through cell volume) Final: 17:10 0.8 100 7.42 19.6 6.1 469 0.3 65 4.9 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 17:15 Sample End Time: 17:35 Analytical Data Name (1) Gary Simcox Signature Date 10/16/2020 Notes: I tested for Ferrous Iron using a HACH Model IR-18 (1.0 mg/L) Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 7.40 ft-TOC Total Well Depth: 18.80 ft-TOC Height of Water Column: 11.40 feet Screen Length: 10 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.9 Gal 3 *Well Volume 5.58 Gal 5 *Well Volume 9.30 Gal Purge Method: Peristaltic Pump Start Time: 16:40 End Time: 17:10 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 14.0 ft-TOC Water Column Above Pump Intake: 6.60 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 9.05 ft-TOC Comments: Final Volume Purged: 0.8 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp ('C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 16:40 0.0 --- --- --- --- --- --- --- --- Start Purging 16:45 0.1 100 7.43 19.8 6.1 455 1.2 133 29.8 16:50 0.3 100 7.43 19.7 6.1 460 0.6 121 15.1 16:55 0.4 100 7.42 19.3 6.1 461 0.4 100 6.84 17:00 0.5 100 7.42 19.6 6.1 462 0.4 88 5.43 17:05 0.7 100 7.43 19.5 6.1 465 0.3 72 4.47 17:10 0.8 100 7.42 19.6 6.1 469 0.3 65 4.89 Method Qty Container Preservative Method Qty Container Preservative 82606 SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 • • •I I Z IC11 101 Moore County Landfill 4358-20-043A phase 11 Purge Date: October 14, 2020 Project Name: Project Location: Project Number: Source Well: MW-3 Purge Time: 30 Minutes Locked?: Yes Sample Date: October 14, 2020 Sampled By: Gary Simcox Sample Time: 8:35 Weather: Sunny Air Temp: 65° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals a 5 minutes an purge volumes >_ 1 ow -through cell volume) Final: 08:35 0.8 100 6.03 18.2 4.6 53 2.5 352 1.7 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 08:35 Sample End Time: 08:55 Analytical Data Name (1) Gary Simcox Signature Date 10/16/2020 Notes: I tested for Ferrous Iron using a HACH Model IR-18 (0.0 mg/L) Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 5.98 ft-TOC Total Well Depth: 18.10 ft-TOC Height of Water Column: 12.12 feet Screen Length: 10 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 2.0 Gal 3 *Well Volume 5.93 Gal 5 *Well Volume 9.89 Gal Purge Method: Peristaltic Pump Start Time: 8:05 End Time: 8:35 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 13.0 ft-TOC Water Column Above Pump Intake: 7.02 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 7.74 ft-TOC Comments: Final Volume Purged: 0.8 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp ('C) pH (s.u.) Spec. Cond. (p5/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 08:05 0.0 --- --- --- --- --- --- --- --- Start Purging 08:10 0.1 100 6.02 17.5 5.0 64 3.1 200 22.8 08:15 0.3 100 6.03 18.0 4.6 51 2.9 279 6.83 08:20 0.4 100 6.03 18.0 4.6 50 2.8 301 3.29 08:25 0.5 100 6.02 18.1 4.5 51 2.6 323 2.05 08:30 0.7 100 6.02 18.2 4.6 52 2.5 342 1.58 08:35 0.8 100 6.03 18.2 4.6 53 2.5 352 1.69 Method Qty Container Preservative Method Qty Container Preservative 82606 SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 •IVA Project Name: Project Location: Project Number: 9 011 Ill Moore County Landfill 456 Turning Leaf Way Aberdeen, NC 4358-20-043A phase 11 Purge Date: s I E October 13, 2020 Source Well: MW-4 Purge Time: 65 Minutes Locked?: Yes Sample Date: October 13, 2020 Sampled By: James Waters Sample Time: 16:05 Weather: Sunny Air Temp: 75° F Water Level & Well Data Well Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 16:00 2.1 125 5.47 20.4 6.0 238 4.6 112 9.9 End of Purging Sample Method] Peristaltic Pump 1605 Sample Start Time:Analytical Sample End Time: 16:20 Data Name (1) James Waters Signature 'mil ' "r� Date 10/13/2020 Notes: To convert ORP to Eh, add 205 mV to ORP. Measuring Point: Top of Casing Depth to Water: 5.21 ft-TOC Total Well Depth: 16.55 ft-TOC Height of Water Column: 11.34 feet Screen Length: 10 feet Stickup: 2.7 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.9 Gal 3 *Well Volume 5.55 Gal 5 *Well Volume 9.25 Gal Purge Method: Peristaltic Pump Start Time: 14:55 End Time: 16:00 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 11.5 ft-TOC Water Column Above Pump Intake: 6.29 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 6.78 ft-TOC Comments: Final Volume Purged: 2.1 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 125 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (NS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 14:55 0.0 --- --- --- --- --- --- --- --- Start Purging 15:05 0.3 125 5.44 20.8 6.0 205 1.6 76 124 15:15 0.7 125 5.47 20.6 6.0 214 3.7 90 54.8 15:25 1.0 125 5.47 20.6 6.0 219 3.8 94 31.2 15:30 1.2 125 5.47 20.6 6.0 231 3.7 99 21.7 15:35 1.3 125 5.47 20.5 6.0 241 3.8 101 15.5 15:40 1.5 125 5.48 20.6 6.0 242 3.8 99 14.3 15:45 1.7 125 5.47 20.6 6.0 242 3.9 100 20.9 15:50 1.8 125 5.47 20.5 6.0 243 3.9 102 15.5 15:55 2.0 125 5.47 20.4 6.0 243 4.0 106 13.1 16:00 2.1 125 5.47 20.4 6.0 238 4.6 112 9.89 Method Qty Container Preservative Method Qty Container Preservative 8260B 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 Form Revision Date: 2/12/18 16:00 •IVA Project Name: Project Location: Project Number: 9 011 Ill Moore County Landfill 456 Turning Leaf Way Aberdeen, NC 4358-20-043A phase 11 Purge Date: s I E October 13, 2020 Source Well: MW-5 Purge Time: 30 Minutes Locked?: Yes Sample Date: October 13, 2020 Sampled By: James Waters Sample Time: 17:45 Weather: Sunny Air Temp: 75° F Water Level & Well Data Well Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 17:40 0.8 100 9.57 20.0 4.4 19 4.9 338 2.0 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 1745 Sample End Time: 18:00 Analytical Data Name (1) James Waters Signature Poi �r • VY II-W 1� Date 10/13/2020 Notes: To convert ORP to Eh, add 205 mV to ORP. Ferrous Iron is non -detect. Measuring Point: Top of Casing Depth to Water: 9.56 ft-TOC Total Well Depth: 19.85 ft-TOC Height of Water Column: 10.29 feet Screen Length: 10 feet Stickup: 2.6 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.7 Gal 3 *Well Volume 5.04 Gal 5 *Well Volume 8.40 Gal Purge Method: Peristaltic Pump Start Time: 17:10 End Time: 17:40 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 15.0 ft-TOC Water Column Above Pump Intake: 5.44 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 10.92 ft-TOC Comments: Final Volume Purged: 0.8 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (NS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 17:10 0.0 --- --- --- --- --- --- --- --- Start Purging 17:15 0.1 100 9.57 20.4 4.7 19 33.2 309 9.97 17:20 0.3 100 9.58 20.2 4.5 19 5.3 321 5.76 17:25 0.4 100 9.57 20.2 4.4 19 5.2 328 3.08 17:30 0.5 100 9.57 20.1 4.4 19 5.1 332 1.33 17:35 0.7 100 9.57 20.1 4.4 19 5.0 335 1.52 17:40 0.8 100 9.57 20.0 4.4 19 4.9 338 2.01 Method Qty Container Preservative Method Qty Container Preservative 8260B 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 Form Revision Date: 2/12/18 16:00 • • •I I Z IC11 101 Moore County Landfill 4358-20-043A phase 11 Purge Date: October 14, 2020 Project Name: Project Location: Project Number: Source Well: MW-6 Purge Time: 55 Minutes Locked?: Yes Sample Date: October 14, 2020 Sampled By: Gary Simcox Sample Time: 13:55 Weather: Sunny Air Temp: 75° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals a 5 minutes an purge volumes >_ 1 ow -through cell volume) Final: 13:50 1.5 100 18.30 22.0 6.2 806 0.4 -87 8.9 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 13:55 Sample End Time: 14:15 Analytical Data Name (1) Gary Simcox Signature Date 10/16/2020 Notes: I tested for Ferrous Iron using a HACH Model IR-18 (7.0 mg/L) Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 17.15 ft-TOC Total Well Depth: 22.50 ft-TOC Height of Water Column: 5.35 feet Screen Length: 15 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 0.9 Gal 3 *Well Volume 2.62 Gal 5 *Well Volume 4.37 Gal Purge Method: Peristaltic Pump Start Time: 12:55 End Time: 13:50 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 20.0 ft-TOC Water Column Above Pump Intake: 2.85 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 17.86 ft-TOC Comments: Final Volume Purged: 1.5 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp ('C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 12:55 0.0 --- --- --- --- --- --- --- --- Start Purging 13:05 0.3 100 18.12 22.1 6.1 553 1.1 -51 42.3 13:15 0.5 100 18.32 22.2 5.9 584 0.5 -58 33.5 13:25 0.8 100 18.31 21.7 6.1 717 0.4 -82 15.5 13:35 1.1 100 18.30 21.8 6.1 783 0.4 -87 11.1 13:40 1.2 100 18.30 21.8 6.2 797 0.4 -87 9.66 13:45 1.3 100 18.31 22.0 6.2 799 0.4 -87 8.44 13:50 1.5 100 18.30 22.0 6.2 806 0.4 -87 8.89 Method Qty Container Preservative Method Qty Container Preservative 82606 SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 •01119 FA Project Name: Project Location: ILGITITECI'• 1110•' Moore County Landfill 456 Turning Leaf Way Aberdeen, NC s I I s Project Number: 4358-20-043A phase 11 Purge Date: October 14, 2020 Source Well: MW-7 Purge Time: 15 Minutes Locked?: Yes Sample Date: October 14, 2020 Sampled By: James Waters Sample Time: 13:20 Weather: Sunny Air Temp: 75* F Measuring Point: Top of Casing Depth to Water: 15.77 ft-TOC Total Well Depth: 22.00 ft-TOC Height of Water Column: 6.23 feet Screen Length: 15 1 feet I Stickup: 2.7 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.0 Gal 3 * Well Volume 3.05 Gal 5 * Well Volume 5.08 Gal Purge Method: Peristaltic Pump Start Time: 1240 1 End Time: 1 12:55 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): I Pressure: psi Pump Intake Depth from Top of Casing: 19.0 ft-TOC Water Column Above Pump Intake: 3.23 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 16.58 ft-TOC Comments: Final Volume Purged: 1 0.4 Gallons I Used YSI Pro Plus, Final Volume Purge Rate: 125 mL/min Well Purged Dry?: Yes (Yes/No) meters (Taken at time intervals >_ 5 minutes and purge volumes >_ Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (IC) pH (s.u.) Spec. Cond. (Ns/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 12:40 0.0 --- --- --- --- --- --- --- --- Start Purging 12:45 0.2 125 17.01 21.6 6.1 442 1.0 -15 29.1 12:50 0.3 125 18.15 21.9 6.0 444 0.3 -21 30.1 12:55 0.4 125 19.24 21.9 6.0 445 0.3 -23 32.6 Final: 12:55 1 0.4 1 125 1 19.24 1 21.9 1 6.0 1 445 1 0.3 1 -23 1 32.6 1 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 13:20 Sample End Time: 13:35 Method Qty Container Preservative Method Qty Container Preservative 8260E SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 James Waters OW uliu_ 10/14/2020 To convert ORP to Eh, add 205 mV to ORP. The water level is dropping to rapidly and the well is being purged dry. The MW-7 sample is taken before the well is Form Revision Date: 2/12/18 16:00 •IVA Project Name: Project Location: Project Number: 9 011 Ill Moore County Landfill 456 Turning Leaf Way Aberdeen, NC 4358-20-043A phase 11 Purge Date: s I E October 14, 2020 Source Well: MW-8 Purge Time: 45 Minutes Locked?: Yes Sample Date: October 14, 2020 Sampled By: James Waters Sample Time: 16:00 Weather: Sunny Air Temp: 75° F Water Level & Well Data Well Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 15:55 1.8 150 11.96 20.7 6.1 1,006 0.1 -54 2.0 End of Purging Sample Method] Peristaltic Pump 1600 Sample Start Time:Analytical Sample End Time: 16:15 Data Name (1) James Waters Signature 54/� • OWWN14' Date 10/14/2020 Notes: To convert ORP to Eh, add 205 mV to ORP. Ferrous iron is 7 mg/L. Measuring Point: Top of Casing Depth to Water: 11.94 ft-TOC Total Well Depth: 22.00 ft-TOC Height of Water Column: 10.06 feet Screen Length: 15 feet Stickup: 2.6 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.6 Gal 3 *Well Volume 4.93 Gal 5 *Well Volume 8.21 Gal Purge Method: Peristaltic Pump Start Time: 15:10 End Time: 15:55 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 17.0 ft-TOC Water Column Above Pump Intake: 5.06 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 13.21 ft-TOC Comments: Final Volume Purged: 1.8 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 150 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (NS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 15:10 0.0 --- --- --- --- --- --- --- --- Start Purging 15:20 0.4 150 11.96 20.9 6.0 429 2.8 -72 64.3 15:25 0.6 150 11.96 20.9 5.9 741 1.7 -49 43.2 15:30 0.8 150 11.96 20.8 5.9 752 1.1 -54 22.2 15:35 1.0 150 11.96 20.7 6.0 966 0.4 -56 11.8 15:40 1.2 150 11.97 20.7 6.0 988 0.2 -56 4.89 15:45 1.4 150 11.96 20.7 6.0 992 0.2 -54 3.92 15:50 1.6 150 11.96 20.7 6.1 1,006 0.2 -54 2.39 15:55 1.8 150 11.96 20.7 6.1 1,006 0.1 -54 2.00 Method Qty Container Preservative Method Qty Container Preservative 8260B SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 Form Revision Date: 2/12/18 16:00 •IVA Project Name: Project Location: Project Number: 9 011 Ill Moore County Landfill 456 Turning Leaf Way Aberdeen, NC 4358-20-043A phase 11 Purge Date: s I E October 14, 2020 Source Well: MW-9 Purge Time: 45 Minutes Locked?: Yes Sample Date: October 14, 2020 Sampled By: James Waters Sample Time: 17:30 Weather: Sunny Air Temp: 75° F Water Level & Well Data Well Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 17:25 1.8 150 23.09 20.7 6.4 2,005 0.1 -105 5.1 End of Purging Sample Method] Bladder Pump 17 30 Sample Start Time:Analytical Sample End Time: 17:45 Data Name (1) James Waters Signature J� VY( Date 10/14/2020 Notes: To convert ORP to Eh, add 205 mV to ORP. At the beginning of purging, black liquid came from the well. Ferrous iron is 7 mg/L. Measuring Point: Top of Casing Depth to Water: 22.95 ft-TOC Total Well Depth: 32.00 ft-TOC Height of Water Column: 9.05 feet Screen Length: 15 feet Stickup: 2.3 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.5 Gal 3 *Well Volume 4.43 Gal 5 *Well Volume 7.38 Gal Purge Method: Peristaltic Pump Start Time: 16:40 End Time: 17:25 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 28.0 ft-TOC Water Column Above Pump Intake: 5.05 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 24.21 ft-TOC Comments: Final Volume Purged: 1.8 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 150 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (NS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 16:40 0.0 --- --- --- --- --- --- --- --- Start Purging 16:55 0.6 150 23.10 20.5 6.5 2,119 0.4 -87 8.20 17:00 0.8 150 23.09 20.7 6.5 2,089 0.2 -95 8.69 17:05 1.0 150 23.09 20.8 6.5 2,006 0.1 -94 7.88 17:10 1.2 150 23.09 20.8 6.5 2,006 0.1 -95 8.23 17:15 1.4 150 23.09 20.8 6.4 2,003 0.1 -98 6.25 17:20 1.6 150 23.09 20.8 6.4 1,998 0.1 -102 6.33 17:25 1.8 150 23.09 20.7 6.4 2,005 0.1 -105 5.12 Method Qty Container Preservative Method Qty Container Preservative 8260B SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 Form Revision Date: 2/12/18 16:00 •IVA Project Name: Project Location: Project Number: 9 011 Ill Moore County Landfill 456 Turning Leaf Way Aberdeen, NC 4358-20-043A phase 11 Purge Date: s I E October 14, 2020 Source Well: MW-11SR Purge Time: 30 Minutes Locked?: Yes Sample Date: October 14, 2020 Sampled By: James Waters Sample Time: 10:35 Weather: Sunny Air Temp: 75° F Water Level & Well Data Well Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 10:30 1.0 125 14.93 19.9 6.5 1,497 1.6 -103 0.6 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 1035 Sample End Time: 10:50 Analytical Data Name (1) James Waters Signature I/IJ WN°� Date 10/14/2020 Notes: To convert ORP to Eh, add 205 mV to ORP. Lock was cut to open. MW-11 SR needs a new lock. Measuring Point: Top of Casing Depth to Water: 14.92 ft-TOC Total Well Depth: 31.20 ft-TOC Height of Water Column: 16.28 feet Screen Length: 10 feet Stickup: 2.3 ft-GRD Well Volume Well Diameter 2 inch Water Volume 2.7 Gal 3 *Well Volume 7.97 Gal 5 *Well Volume 13.28 Gal Purge Method: Peristaltic Pump Start Time: 10:00 End Time: 10:30 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 26.0 ft-TOC Water Column Above Pump Intake: 11.08 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 17.69 ft-TOC Comments: Final Volume Purged: 1.0 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 125 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (NS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 10:00 0.0 --- --- --- --- --- --- --- --- Start Purging 10:05 0.2 125 14.93 19.9 6.5 1,495 0.4 -94 2.37 10:10 0.3 125 14.93 19.9 6.5 1,498 0.3 -98 0.98 10:15 0.5 125 14.93 19.9 6.5 1,498 0.2 -100 1.60 10:20 0.7 125 14.93 19.9 6.5 1,497 1.9 -101 0.68 10:25 0.8 125 14.93 19.9 6.5 1,499 1.7 -102 0.67 10:30 1.0 125 14.93 19.9 6.5 1,497 1.6 -103 0.58 Method Qty Container Preservative Method Qty Container Preservative 8260B 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 Form Revision Date: 2/12/18 16:00 •01119 FA Project Name: Project Location: ILGITITECI'• 1110•' Moore County Landfill 456 Turning Leaf Way Aberdeen, NC s I s Project Number: 4358-20-043A phase 11 Purge Date: October 14, 2020 Source Well: MW-11 DR Purge Time: 30 Minutes Locked?: Yes Sample Date: October 14, 2020 Sampled By: James Waters Sample Time: 11:45 Weather: Sunny Air Temp: 75* F Measuring Point: Top of Casing Depth to Water: 15.55 ft-TOC Total Well Depth: 42.20 ft-TOC Height of Water Column: 26.65 feet Screen Length: 10 1 feet I Stickup: 2.45 ft-GRD Well Volume Well Diameter 2 inch Water Volume 4.3 Gal 3 * Well Volume 13.05 1 Gal 5 * Well Volume 21.74 Gal Purge Method: Peristaltic Pump Start Time: 11:10 1 End Time: 1 11:40 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): I Pressure:1 I psi Pump Intake Depth from Top of Casing: 39.0 ft-TOC Water Column Above Pump Intake: 23.45 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 21.41 ft-TOC Comments: Final Volume Purged: 1 1.0 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 125 mL/min Well Purged Dry?: No (Yes/No) meters (Taken at time intervals >_ 5 minutes and purge volumes >_ Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (IC) pH (s.u.) Spec. Cond. (NS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 11:10 0.0 --- --- --- --- --- --- --- --- Start Purging 11:15 0.2 125 15.62 19.4 6.4 879 0.2 -80 3.87 11:20 0.3 125 15.63 19.3 6.4 873 0.2 -80 5.86 11:25 0.5 125 15.63 19.3 6.4 754 0.2 -81 5.34 11:30 0.7 125 15.63 19.3 6.4 754 0.1 -80 4.53 11:35 0.8 125 15.63 19.3 6.4 754 0.1 -81 4.01 11:40 1.0 125 15.63 19.2 6.4 754 0.1 -81 3.94 Final: 11:40 1 1.0 1 125 1 15.63 1 19.2 1 6.4 1 754 1 0.1 1 -81 1 3.9 1 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 11:45 Sample End Time: 11:55 Method Qty Container Preservative Method Qty Container Preservative 8260E 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 ame (1) James Waters To convert ORP to Eh, add 205 mV to ORP. MW-11 DR is damaged. i LA . W PAW 10/14/2020 is a whole in the casing and the pad is not stable. This could allow the surface water Form Revision Date: 2/12/18 16:00 • • •I I Z IC11 Moore County Landfill 4358-20-043A phase 11 101 Purge Date: October 13, 2020 Project Name: Project Location: Project Number: Source Well: MW-13SR Purge Time: 45 Minutes Locked?: Yes Sample Date: October 13, 2020 Sampled By: Gary Simcox Sample Time: 14:55 Weather: Sunny Air Temp: 75° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals a 5 minutes an purge volumes >_ 1 ow -through cell volume) Final: 14:50 1.2 100 11.10 21.3 6.1 318 0.3 -45 8.3 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 14:55 Sample End Time: 15:05 Analytical Data Name (1) Gary Simcox Signature Date 10/16/2020 Notes: Raised the intake line from 20' to 17' below TOC at 1430 hours Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 11.09 ft-TOC Total Well Depth: 22.50 ft-TOC Height of Water Column: 11.41 feet Screen Length: 10 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.9 Gal 3 *Well Volume 5.59 Gal 5 *Well Volume 9.31 Gal Purge Method: Peristaltic Pump Start Time: 14:05 End Time: 14:50 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 20.0 ft-TOC Water Column Above Pump Intake: 8.91 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 13.32 ft-TOC Comments: Final Volume Purged: 1.2 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp ('C) pH (s.u.) Spec. Cond. (p5/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 14:05 0.0 --- --- --- --- --- --- --- --- Start Purging 14:10 0.1 100 11.12 20.6 6.1 318 1.2 -44 67.9 14:15 0.3 100 11.09 20.7 6.1 317 0.8 -47 73.7 14:20 0.4 100 11.10 20.6 6.1 316 0.7 -48 85.3 14:25 0.5 100 11.11 20.8 6.1 314 0.6 -47 99.8 14:30 0.7 100 11.09 20.9 6.1 314 0.5 -49 101 14:35 0.8 100 11.10 20.9 6.1 312 0.4 -44 95.7 14:40 0.9 100 11.10 21.5 6.1 315 0.4 -47 33.1 14:45 1.1 100 11.00 21.4 6.1 316 0.3 -45 10.2 14:50 1.2 100 11.10 21.3 6.1 318 0.3 -45 8.25 Method Qty Container Preservative Method Qty Container Preservative 82606 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 • • •I I Z IC11 Moore County Landfill 4358-20-043A phase 11 101 Purge Date: October 13, 2020 Project Name: Project Location: Project Number: Source Well: MW-13DR Purge Time: 75 Minutes Locked?: Yes Sample Date: October 13, 2020 Sampled By: Gary Simcox Sample Time: 16:55 Weather: Sunny Air Temp: 85° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals a 5 minutes an purge volumes >_ 1 ow -through cell volume) Final: 16:50 2.0 100 11.60 21.0 5.3 88 0.2 99 73.0 End of Purging Sample Method: Bladder Pump Sample Start Time: 16:55 Sample End Time: 17:05 Analytical Data Name (1) Gary Simcox Signature Date 10/16/2020 Notes: To convert ORP to Eh, add 205 mV to ORP. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 11.53 ft-TOC Total Well Depth: 43.50 ft-TOC Height of Water Column: 31.97 feet Screen Length: 10 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 5.2 Gal 3 *Well Volume 15.65 Gal 5 *Well Volume 26.09 Gal Purge Method: Peristaltic Pump Start Time: 15:35 End Time: 16:50 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 38.0 ft-TOC Water Column Above Pump Intake: 26.47 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 18.15 ft-TOC Comments: Final Volume Purged: 2.0 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp ('C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 15:35 0.0 --- --- --- --- --- --- --- --- Start Purging 15:40 0.1 100 11.59 21.6 5.4 96 1.0 74 716 15:50 0.4 100 11.62 21.2 5.4 90 0.6 87 220 16:00 0.7 100 11.59 20.7 5.3 90 0.4 92 112 16:10 0.9 100 11.60 20.2 5.3 90 0.3 94 91.1 16:20 1.2 100 11.60 20.6 5.3 90 0.3 95 81.0 16:30 1.5 100 11.59 20.8 5.3 90 0.2 96 78.6 16:40 1.7 100 11.61 21.1 5.3 89 0.2 98 69.7 16:50 2.0 100 11.60 21.0 5.3 88 0.2 99 73.0 Method Qty Container Preservative Method Qty Container Preservative 82606 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 •IVA Project Name: Project Location: Project Number: 9 ILGITITEC1.11-6111Ill Moore County Landfill 456 Turning Leaf Way Aberdeen, NC 4358-20-043A phase 11 Purge Date: s I E October 14, 2020 Source Well: MW-14 Purge Time: 30 Minutes Locked?: Yes Sample Date: October 14, 2020 Sampled By: James Waters Sample Time: 8:55 Weather: Sunny Air Temp: 75° F Water Level & Well Data Well Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 08:50 1.0 125 17.63 19.5 6.4 944 0.5 -88 2.5 End of Purging Sample Method] Peristaltic Pump 08 55 Sample Start Time:Analytical Sample End Time: 09:05 Data Name (1) James Waters Signature 0 w4OA- 10/14/2020 Notes: To convert ORP to Eh, add 205 mV to ORP. Measuring Point: Top of Casing Depth to Water: 17.26 ft-TOC Total Well Depth: 23.00 ft-TOC Height of Water Column: 5.74 feet Screen Length: 15 feet Stickup: 1.9 ft-GRD Well Volume Well Diameter 2 inch Water Volume 0.9 Gal 3 *Well Volume 2.81 Gal 5 *Well Volume 4.68 Gal Purge Method: Peristaltic Pump Start Time: 8:20 End Time: 8:50 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 19.5 ft-TOC Water Column Above Pump Intake: 2.24 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 17.82 ft-TOC Comments: Final Volume Purged: 1.0 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 125 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (NS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 08:20 0.0 --- --- --- --- --- --- --- --- Start Purging 08:25 0.2 125 17.60 24.1 6.4 942 291.E -78 8.08 08:30 0.3 125 17.62 19.5 6.4 958 1.2 -82 4.91 08:35 0.5 125 17.63 19.5 6.4 964 0.9 -85 3.85 08:40 0.7 125 17.63 19.4 6.4 968 0.8 -86 2.31 08:45 0.8 125 17.63 19.5 6.4 951 0.5 -88 2.22 08:50 1.0 125 17.63 19.5 6.4 944 0.5 -88 2.45 Method Qty Container Preservative Method Qty Container Preservative 8260B 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 Form Revision Date: 2/12/18 16:00 • • •I I Z IC11 101 Moore County Landfill 4358-20-043A phase 11 Purge Date: October 14, 2020 Project Name: Project Location: Project Number: Source Well: MW-15R Purge Time: 85 Minutes Locked?: Yes Sample Date: October 14, 2020 Sampled By: Gary Simcox Sample Time: 11:45 Weather: Sunny Air Temp: 75° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals a 5 minutes an purge volumes >_ 1 ow -through cell volume) Final: 11:40 2.2 100 32.52 18.5 6.1 461 2.0 -70 15.7 End of Purging Sample Method: Bladder Pump Sample Start Time: 11:45 Sample End Time: 12:30 Analytical Data Name (1) Gary Simcox Signature Date 10/16/2020 Notes: Duplicate collected at this location. (Sample time recorded as 0700 hrs) I tested for Ferrous Iron using a HACH Model IR-18 (7.0 mg/L) Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 32.45 ft-TOC Total Well Depth: 50.20 ft-TOC Height of Water Column: 17.75 feet Screen Length: 10 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 2.9 Gal 3 *Well Volume 8.69 Gal 5 *Well Volume 14.48 Gal Purge Method: Peristaltic Pump Start Time: 10:15 End Time: 11:40 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 45.0 ft-TOC Water Column Above Pump Intake: 12.55 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 35.59 ft-TOC Comments: Final Volume Purged: 2.2 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp ('C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 10:15 0.0 --- --- --- --- --- --- --- --- Start Purging 10:20 0.1 100 32.50 18.5 6.1 563 4.8 -56 1100 10:30 0.4 100 32.51 18.3 6.1 547 4.3 -63 512 10:40 0.7 100 32.54 18.4 6.1 552 3.7 -67 158 10:50 0.9 100 32.53 18.3 6.1 539 3.2 -67 103 11:00 1.2 100 32.52 18.4 6.1 516 2.8 -68 54.8 11:10 1.5 100 32.52 18.4 6.1 503 2.7 -67 44.8 11:20 1.7 100 32.53 18.4 6.1 483 2.4 -69 33.9 11:30 2.0 100 32.51 18.5 6.1 470 2.1 -70 24.2 11:40 2.2 100 32.52 18.5 6.1 461 2.0 -70 15.7 Method Qty Container Preservative Method Qty Container Preservative 82606 SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 LOW Project Name: Project Location: Project Number: FLOW• I► Moore County Landfill 456 Turning Leaf Way Aberdeen, NC 4358-20-043A phase 11 Purge Date: October 13, 2020 Source Well: MW-17S Purge Time: 120 Minutes Locked?: Yes Sample Date: October 13, 2020 Sampled By: James Waters Sample Time: 11:35 Weather: Overcast Air Temp: 75° F Water Level & Well Data Measuring Point: Top of Casing Well Volume Well Diameter 2 inch Water Volume 1.7 Gal 3 Well Volume 5.16 Gal 5 Well Volume 8.60 Gal Time: 9:30 End Time: 11:30 if Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 19.0 ft-TOC Water Column Above Pump Intake: 8.14 feet Flow Through Cell Vol: 200 DTW-TOC at 25% Drawdown of WC Above Pump: 12.90 ft-TOC Comments: Final Volume Purged: 3.2 Gallons Used Y51 Pro Plus, Final Volume Purge Rate: 100 mUmin Well Purged Dry?: No (Yes/No) mL Volume Depth to Dissolved Time Purged Flow Rate Water Temp pH Spec. Cond. Oxygen ORP* Turbidity Comment (gal) (mL/min) (ft) VC) (s.u.) (PS/cm) (mg/L) (mV) (NTU) 09:30 0.0 --- --- --- --- --- --- --- --- Start Purging 09:35 0.1 100 10.92 21.9 5.3 262 3.6 178 122 09:40 0.3 100 10.93 21.9 5.5 287 3.3 150 142 09:45 0.4 100 10.92 21.9 5.6 328 3.0 124 121 09:50 0.5 100 10.92 21.9 5.7 350 2.8 112 89.9 09:55 0.7 100 10.92 21.9 5.7 361 2.7 106 84.5 10:00 0.8 100 10.92 21.9 5.7 375 2.6 104 88.7 10:05 0.9 100 10.92 22.0 5.8 390 2.4 95 62.4 10:10 1.1 100 10.92 22.0 5.8 404 2.2 92 54.4 10:15 1.2 100 10.92 22.0 5.8 415 2.1 88 45.9 10:20 1.3 100 10.92 22.0 5.9 422 2.1 87 44.0 10:25 1.5 100 10.92 22.0 5.9 423 2.0 87 37.6 10:30 1.6 100 10.92 22.0 5.9 435 1.9 84 24.4 10:35 1.7 100 10.92 22.0 5.9 448 1.8 82 22.1 10:40 1.8 100 10.92 22.0 5.9 465 1.7 79 20.7 10:45 2.0 100 10.92 22.0 5.9 480 1.7 77 17.3 10:50 2.1 100 10.92 22.0 5.9 499 1.6 74 15.8 10:55 2.2 100 10.92 22.0 6.0 515 1.7 71 13.8 11:00 2.4 100 10.92 22.0 6.0 563 1.6 68 15.6 11:10 2.6 100 10.92 22.1 6.0 571 1.4 62 24.0 11:20 2.9 100 10.92 22.1 5.9 572 1.3 65 17.0 11:30 3.2 100 10.92 22.1 5.9 582 1.3 67 9.66 Form Revision Date: 2/12/18 16:00 Time: 9:30 End Time: 11:30 if Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 19.0 ft-TOC Water Column Above Pump Intake: 8.14 feet Flow Through Cell Vol: 200 DTW-TOC at 25% Drawdown of WC Above Pump: 12.90 ft-TOC Comments: Final Volume Purged: 3.2 Gallons Used Y51 Pro Plus, Final Volume Purge Rate: 100 mUmin Well Purged Dry?: No (Yes/No) mL Volume Depth to Dissolved Time Purged Flow Rate Water Temp pH Spec. Cond. Oxygen ORP* Turbidity Comment (gal) (mL/min) (ft) VC) (s.u.) (PS/cm) (mg/L) (mV) (NTU) 09:30 0.0 --- --- --- --- --- --- --- --- Start Purging 09:35 0.1 100 10.92 21.9 5.3 262 3.6 178 122 09:40 0.3 100 10.93 21.9 5.5 287 3.3 150 142 09:45 0.4 100 10.92 21.9 5.6 328 3.0 124 121 09:50 0.5 100 10.92 21.9 5.7 350 2.8 112 89.9 09:55 0.7 100 10.92 21.9 5.7 361 2.7 106 84.5 10:00 0.8 100 10.92 21.9 5.7 375 2.6 104 88.7 10:05 0.9 100 10.92 22.0 5.8 390 2.4 95 62.4 10:10 1.1 100 10.92 22.0 5.8 404 2.2 92 54.4 10:15 1.2 100 10.92 22.0 5.8 415 2.1 88 45.9 10:20 1.3 100 10.92 22.0 5.9 422 2.1 87 44.0 10:25 1.5 100 10.92 22.0 5.9 423 2.0 87 37.6 10:30 1.6 100 10.92 22.0 5.9 435 1.9 84 24.4 10:35 1.7 100 10.92 22.0 5.9 448 1.8 82 22.1 10:40 1.8 100 10.92 22.0 5.9 465 1.7 79 20.7 10:45 2.0 100 10.92 22.0 5.9 480 1.7 77 17.3 10:50 2.1 100 10.92 22.0 5.9 499 1.6 74 15.8 10:55 2.2 100 10.92 22.0 6.0 515 1.7 71 13.8 11:00 2.4 100 10.92 22.0 6.0 563 1.6 68 15.6 11:10 2.6 100 10.92 22.1 6.0 571 1.4 62 24.0 11:20 2.9 100 10.92 22.1 5.9 572 1.3 65 17.0 11:30 3.2 100 10.92 22.1 5.9 582 1.3 67 9.66 Form Revision Date: 2/12/18 16:00 Volume Depth to Dissolved Time Purged Flow Rate Water Temp pH Spec. Cond. Oxygen ORP* Turbidity Comment (gal) (mL/min) (ft) VC) (s.u.) (PS/cm) (mg/L) (mV) (NTU) 09:30 0.0 --- --- --- --- --- --- --- --- Start Purging 09:35 0.1 100 10.92 21.9 5.3 262 3.6 178 122 09:40 0.3 100 10.93 21.9 5.5 287 3.3 150 142 09:45 0.4 100 10.92 21.9 5.6 328 3.0 124 121 09:50 0.5 100 10.92 21.9 5.7 350 2.8 112 89.9 09:55 0.7 100 10.92 21.9 5.7 361 2.7 106 84.5 10:00 0.8 100 10.92 21.9 5.7 375 2.6 104 88.7 10:05 0.9 100 10.92 22.0 5.8 390 2.4 95 62.4 10:10 1.1 100 10.92 22.0 5.8 404 2.2 92 54.4 10:15 1.2 100 10.92 22.0 5.8 415 2.1 88 45.9 10:20 1.3 100 10.92 22.0 5.9 422 2.1 87 44.0 10:25 1.5 100 10.92 22.0 5.9 423 2.0 87 37.6 10:30 1.6 100 10.92 22.0 5.9 435 1.9 84 24.4 10:35 1.7 100 10.92 22.0 5.9 448 1.8 82 22.1 10:40 1.8 100 10.92 22.0 5.9 465 1.7 79 20.7 10:45 2.0 100 10.92 22.0 5.9 480 1.7 77 17.3 10:50 2.1 100 10.92 22.0 5.9 499 1.6 74 15.8 10:55 2.2 100 10.92 22.0 6.0 515 1.7 71 13.8 11:00 2.4 100 10.92 22.0 6.0 563 1.6 68 15.6 11:10 2.6 100 10.92 22.1 6.0 571 1.4 62 24.0 11:20 2.9 100 10.92 22.1 5.9 572 1.3 65 17.0 11:30 3.2 100 10.92 22.1 5.9 582 1.3 67 9.66 Form Revision Date: 2/12/18 16:00 Form Revision Date: 2/12/18 16:00 • • •I I Z IC11 Moore County Landfill 4358-20-043A phase 11 101 Purge Date: October 13, 2020 Project Name: Project Location: Project Number: Source Well: MW-17D Purge Time: 90 Minutes Locked?: Yes Sample Date: October 13, 2020 Sampled By: Gary Simcox Sample Time: 11:05 Weather: Overcast Air Temp: 75° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals a 5 minutes an purge volumes >_ 1 ow -through cell volume) Final: 11:00 2.9 120 21.4 7.6 328 1.2 -143 57.0 End of Purging Sample Method: Bladder Pump Sample Start Time: 11:05 Sample End Time: 11:15 Analytical Data Name (1) Gary Simcox Signature Date 10/16/2020 Notes: To convert ORP to Eh, add 205 mV to ORP. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 10.30 ft-TOC Total Well Depth: 37.30 ft-TOC Height of Water Column: 27.00 feet Screen Length: 5 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 4.4 Gal 3 *Well Volume 13.22 Gal 5 *Well Volume 22.03 Gal Purge Method: Peristaltic Pump Start Time: 9:30 End Time: 11:00 (If Used) Bladder Pump Control Settings: On (sec): 5 Off (sec): 30 Pressure: 25 psi Pump Intake Depth from Top of Casing: 35.0 ft-TOC Water Column Above Pump Intake: 24.70 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 16.48 ft-TOC Comments: Final Volume Purged: 2.9 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 120 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp ('C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 09:30 0.0 --- --- --- --- --- --- --- --- Start Purging 09:35 0.2 150 21.3 7.8 326 5.8 -115 551 09:40 0.4 150 21.5 7.8 324 4.1 -149 291 09:45 0.6 120 21.4 7.7 323 3.3 -154 192 09:50 0.7 120 21.6 7.7 323 3.0 -155 142 09:55 0.9 120 14.39 21.5 7.6 324 2.8 -154 112 10:00 1.0 120 15.12 21.5 7.6 324 2.6 -154 89.4 10:05 1.2 120 16.06 21.6 7.6 325 2.1 -153 77.3 10:10 1.3 120 16.64 21.5 7.6 325 2.1 -152 72.4 10:15 1.5 120 17.35 21.5 7.6 326 1.9 -151 67.2 10:20 1.7 120 18.02 21.6 7.6 326 1.7 -149 63.9 10:30 2.0 120 19.25 21.6 7.6 327 1.5 -149 60.9 10:40 2.3 120 20.49 21.4 7.6 327 1.3 -148 60.2 10:50 2.6 120 21.75 21.4 7.6 328 1.2 -146 57.3 11:00 2.9 120 22.97 21.4 7.6 328 1.2 -143 57.0 Method Qty Container Preservative Method Qty Container Preservative 82606 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 •IVA Project Name: Project Location: Project Number: 9 011 Ill Moore County Landfill 456 Turning Leaf Way Aberdeen, NC 4358-20-043A phase 11 Purge Date: s I E October 13, 2020 Source Well: MW-18 Purge Time: 105 Minutes Locked?: Yes Sample Date: October 13, 2020 Sampled By: James Waters Sample Time: 14:05 Weather: Sunny Air Temp: 75° F Water Level & Well Data Well Purging Information Field Parameters (Taken at time intervals >_ 5 minutes and purge volumes >_ 1 flow -through cell volume) Final: 14:00 3.5 125 6.51 22.6 6.3 1,031 0.1 18 7.7 End of Purging Sample Method] Peristaltic Pump 1405 Sample Start Time:Analytical Sample End Time: 14:15 Data Name (1) James Waters Signature vYll�i%N� Date 10/13/2020 Notes: To convert ORP to Eh, add 205 mV to ORP. Measuring Point: Top of Casing Depth to Water: 6.46 ft-TOC Total Well Depth: 16.20 ft-TOC Height of Water Column: 9.74 feet Screen Length: 8 feet Stickup: 2.6 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.6 Gal 3 *Well Volume 4.77 Gal 5 *Well Volume 7.95 Gal Purge Method: Peristaltic Pump Start Time: 12:15 End Time: 14:00 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 14.0 ft-TOC Water Column Above Pump Intake: 7.54 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 8.35 ft-TOC Comments: Final Volume Purged: 3.5 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 125 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (NS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 12:15 0.0 --- --- --- --- --- --- --- --- Start Purging 12:30 0.5 125 6.51 22.7 6.1 664 0.9 37 149 12:40 0.8 125 6.51 22.7 6.2 720 0.6 33 107 12:50 1.2 125 6.51 22.7 6.2 792 0.4 28 80.9 13:00 1.5 125 6.51 22.7 6.2 839 0.3 27 50.4 13:10 1.8 125 6.51 22.6 6.2 885 0.4 23 48.6 13:20 2.1 125 6.51 22.6 6.2 904 0.5 24 32.4 13:30 2.5 125 6.51 22.6 6.3 958 0.2 23 23.7 13:40 2.8 125 6.51 22.6 6.3 995 0.2 21 13.9 13:50 3.1 125 6.51 22.6 6.3 1,023 0.1 18 10.2 14:00 3.5 125 6.51 22.6 6.3 1,031 0.1 18 7.67 Method Qty Container Preservative Method Qty Container Preservative 8260B 300 8260 D-SIM SIM 450052 D-2011 6010/6020 310.2 7470 SIM 2540C-2011 Form Revision Date: 2/12/18 16:00 • • •I I Z IC11 Moore County Landfill 4358-20-043A phase 11 101 Purge Date: October 13, 2020 Project Name: Project Location: Project Number: Source Well: MW-19 Purge Time: 45 Minutes Locked?: Yes Sample Date: October 13, 2020 Sampled By: Gary Simcox Sample Time: 12:25 Weather: Overcast Air Temp: 75° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals a 5 minutes an purge volumes >_ 1 ow -through cell volume) Final: 12:20 1.2 100 6.40 21.1 6.1 353 0.3 35 8.4 End of Purging Sample Method: Peristaltic Pump Sample Start Time: 12:25 Sample End Time: 13:10 Analytical Data Name (1) Gary Simcox Signature Date 10/16/2020 Notes: To convert ORP to Eh, add 205 mV to ORP. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: 6.38 ft-TOC Total Well Depth: 15.70 ft-TOC Height of Water Column: 9.32 feet Screen Length: 8 feet Stickup: 2.5 ft-GRD Well Volume Well Diameter 2 inch Water Volume 1.5 Gal 3 *Well Volume 4.56 Gal 5 *Well Volume 7.60 Gal Purge Method: Peristaltic Pump Start Time: 11:35 End Time: 12:20 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: 13.5 ft-TOC Water Column Above Pump Intake: 7.12 feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: 8.16 ft-TOC Comments: Final Volume Purged: 1.2 Gallons Used YSI Pro Plus, Final Volume Purge Rate: 100 mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp ('C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 11:35 0.0 --- --- --- --- --- --- --- --- Start Purging 11:40 0.1 100 6.41 20.9 6.1 363 1.7 27 93.0 11:45 0.3 100 6.40 20.9 6.1 359 0.9 31 82.4 11:50 0.4 100 6.40 20.9 6.1 356 0.6 29 78.4 11:55 0.5 100 6.42 20.9 6.2 357 0.5 30 63.9 12:00 0.7 100 6.40 20.9 6.2 357 0.4 31 62.6 12:05 0.8 100 6.41 20.9 6.1 357 0.4 31 53.1 12:10 0.9 100 6.41 21.1 6.1 357 0.3 31 32.0 12:15 1.1 100 6.40 21.1 6.1 356 0.3 32 13.7 12:20 1.2 100 6.40 21.1 6.1 353 0.3 35 8.39 Method Qty Container Preservative Method Qty Container Preservative Full App II SIM 450052 D-2011 8260 D-SIM 310.2 7470 SIM 2540C-2011 300 Moore County Landfill 356 Turning Leaf Way, Aberdeen, NC 4358-20-043A phase 01 Sample Date: i i E Thursday, October 15, 2020 Project Name: Project Location: Project Number: Client Name/Contact: Water Supply Well ID: PW-1 Weather: Sunny Well Address: Air Temp (°F): 50 ° F Owner Name: Blake POE Present (Y/N): No IOwner Phone No.: Equipment Calibration Information: Equipment Date Time Calibration Solution Calibration Check PH 10/13/20 07:30 4.00, 7.00, 10.00 4.00 7.00 10.00 Conductivity 10/13/20 07:30 1413 Units 1 1,413 Units I Purging Information Purge Rate (GPM): 5.0 Purge Start Time: 10:45 Volume Purged (Gal): 75.0 Purge End Time: 11:00 Parameters and Sampling Total Volume (Gal) Time pH (s.u.) Temperature °C Conductivity PS/cm 75.00 11:00 4.84 17.6 22 Turbidity (NTU) Dissolved Oxygen (mg/L) ORP (mV) 0.83 12.36 192.8 Sample ID Sample Location Sample Date Sample Time PW-1 Spigot on well house 10/15/2020 11:00 Method Qty Container Pres. Method Qty Container Pres. VOCs 6200 3 40mL VOAs HCl Additional Comments (description of location of sample port, water well, filters, etc.) Site Sketch Signature Simcox Well / System Photographs Date 10/16/2020 Revision: 9/1/17 13:30 Moore County Landfill 4358-20-043A phase 11 Purge Date: !A October 15, 2020 Project Name: Project Location: Project Number: Source Well: SW-1 Purge Time: 0 Minutes Locked?: No Sample Date: October 15, 2020 Sampled By: Gary Simcox Sample Time: 10:30 Weather: Sunny Air Temp: 50 ° F Water Level & Well Data Measuring Point: Top of Casing Well Volume Depth to Water: ft-TOC Well Diameter 2 inch Total Well Depth: ft-TOC Water Volume Gal Height of Water Column: feet 3 * Well Volume Gal Screen Length:1 Ifeet I Stickup: ft-GRD 5 * Well Volume Gal Well Purging Information Purge Method: Peristaltic Pump Start Time: 10:30 End Time: 10:30 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: ft-TOC Water Column Above Pump Intake: feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: ft-TOC Comments: Final Volume Purged: I Gallons Used YSI Pro Plus, Final Volume Purge Rate: I I mL/min Well Purged Dry?: I No I (Yes/No) Field Parameters (Taken at time intervals z 5 minutes and purge volumes >_ 1 flow -through cell volume) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (IC) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTLI) Comment 10:30 0.0 --- --- --- --- --- --- --- --- Start Purging 10:30 16.6 6.5 186 7.0 -55 6.34 Final: 10:30 1 1 1 1 16.6 1 6.5 1 186 1 7.0 1 -55 1 6.3 1 End of Purging Sample Method: Sample Start Time: 10:30 Sample End Time: Analytical Data Method Qty Container Preservative Method Qty Container Preservative 8260B SM 450OSD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1 /9056 RSK-175 Name Signature Date (1) Gary Simcox 10/16/2020 Notes: Drive on the dirt road towel MW-2. Park at MW-2 and walk south down a path to the creek. I collected sample SW-1 at a location marked with 1" vc and red ribbon. The creek has a red tint but good flow. Form Revision Date: 2/12/18 16:00 • • •I I Z IC11 101 Moore County Landfill 4358-20-043A phase 11 Purge Date: October 15, 2020 Project Name: Project Location: Project Number: Source Well: SW-2 Purge Time: 0 Minutes Locked?: No Sample Date: October 15, 2020 Sampled By: Gary Simcox Sample Time: 8:05 Weather: Sunny Air Temp: 50 ° F Water Level & Well Data We Purging Information Field Parameters (Taken at time intervals a 5 minutes an purge volumes _> 1 low -through cell volume) Final: 08:05 17.4 5.7 41 5.4 87 1.0 End of Purging Sample Method: Sample Start Time: 08:05 Sample End Time: Analytical Data Name Signature Date (1) Gary Simcox 10/16/2020 Notes: I collected sample SW-2 at the end of the trail past the mulch piles. There is a 1" pvc stake with red ribbon marking the location. Form Revision Date: 2/12/18 16:00 Measuring Point: Top of Casing Depth to Water: ft-TOC Total Well Depth: ft-TOC Height of Water Column: feet Screen Length: feet Stickup: ft-GRD Well Volume Well Diameter 2 inch Water Volume Gal 3 *Well Volume Gal 5 *Well Volume Gal Purge Method: Peristaltic Pump Start Time: 8:05 End Time: 8:05 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: ft-TOC Water Column Above Pump Intake: feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: ft-TOC Comments: Final Volume Purged: Gallons Used YSI Pro Plus, Final Volume Purge Rate: mL/min Well Purged Dry?: No (Yes/No) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (°C) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTU) Comment 08:05 0.0 --- --- --- --- --- Start Purging 08:05 17.4 5.7 41 5.4 87 0.98 Method Qty Container Preservative Method Qty Container Preservative 82606 SM 4500SD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1/9056 RSK-175 Moore County Landfill 4358-20-043A phase 11 Purge Date: !A October 15, 2020 Project Name: Project Location: Project Number: Source Well: SW-3 Purge Time: 0 Minutes Locked?: No Sample Date: October 15, 2020 Sampled By: Gary Simcox Sample Time: 9:45 Weather: Sunny Air Temp: 50 ° F Water Level & Well Data Measuring Point: Top of Casing Well Volume Depth to Water: ft-TOC Well Diameter 2 inch Total Well Depth: ft-TOC Water Volume Gal Height of Water Column: feet 3 * Well Volume Gal Screen Length:1 Ifeet I Stickup: ft-GRD 5 * Well Volume Gal Well Purging Information Purge Method: Peristaltic Pump Start Time: 9:45 End Time: 9A5 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: ft-TOC Water Column Above Pump Intake: feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: ft-TOC Comments: Final Volume Purged: I Gallons Used YSI Pro Plus, Final Volume Purge Rate: I I mL/min Well Purged Dry?: INo I (Yes/No) Field Parameters (Taken at time intervals z 5 minutes and purge volumes >_ 1 flow -through cell volume) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (IC) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTLI) Comment 09:45 0.0 --- --- --- --- --- --- --- --- Start Purging 09:45 16.0 6.7 172 1 8.7 -55 22.0 Final: 09:45 1 1 1 1 16.0 1 6.7 1 172 1 8.7 1 -55 1 22.0 1 End of Purging Sample Method: Sample Start Time: 09:45 Sample End Time: Analytical Data Method Qty Container Preservative Method Qty Container Preservative 8260B SM 450OSD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1 /9056 RSK-175 Name Signature Date (1) Gary Simcox 10/16/2020 Notes: I collected sample SW-3 at a location marked with pink flagging. Drive on the dirt road SE past MW-3 toward MW-2. About 200 yards past MW-3 there is a path marked with pink flagging. Park and walk in another 200 yards to the creek. The creek has a red tint but good flow. Form Revision Date: 2/12/18 16:00 Moore County Landfill 4358-20-043A phase 11 Purge Date: October 15, 2020 Project Name: Project Location: Project Number: Source Well: SW-4 Purge Time: 0 Minutes Locked?: No Sample Date: October 15, 2020 Sampled By: Gary Simcox Sample Time: 9:00 Weather: Sunny Air Temp: 50 ° F Water Level & Well Data Measuring Point: Top of Casing Well Volume Depth to Water: ft-TOC Well Diameter 2 inch Total Well Depth: ft-TOC Water Volume Gal Height of Water Column: feet 3 * Well Volume Gal Screen Length:1 Ifeet I Stickup: ft-GRD 5 * Well Volume Gal Well Purging Information Purge Method: Peristaltic Pump Start Time: 9:00 End Time: 9:00 (If Used) Bladder Pump Control Settings: On (sec): Off (sec): Pressure: psi Pump Intake Depth from Top of Casing: ft-TOC Water Column Above Pump Intake: feet Flow Through Cell Vol: 200 mL DTW-TOC at 25% Drawdown of WC Above Pump: ft-TOC Comments: Final Volume Purged: I Gallons Used YSI Pro Plus, Final Volume Purge Rate: I I mL/min Well Purged Dry?: I No I (Yes/No) Field Parameters (Taken at time intervals z 5 minutes and purge volumes >_ 1 flow -through cell volume) Time Volume Purged (gal) Flow Rate (mL/min) Depth to Water (ft) Temp (IC) pH (s.u.) Spec. Cond. (PS/cm) Dissolved Oxygen (mg/L) ORP* (mV) Turbidity (NTLI) Comment 09:00 0.0 --- --- --- --- --- --- --- --- Start Purging 09:00 15.9 6.7 188 1 8.0 -41 9.62 Final: 09:00 1 1 1 1 15.9 1 6.7 1 188 1 8.0 1 -41 1 9.6 1 End of Purging Sample Method: Sample Start Time: 09:00 Sample End Time: Analytical Data Method Qty Container Preservative Method Qty Container Preservative 8260B SM 450OSD 8260 D-SIM 310.2 6010/6020/7470 415.1/9060 300.0/300.1 /9056 RSK-175 Name Signature Date (1) Gary Simcox 10/16/2020 Notes: Walked down the slope at Outfall #1. 1 located the surface water (creek) flowing from NE to SW. I collected sample SW-4 approximatley 100' SW of the intersection of Outfall #1 and the creek. Form Revision Date: 2/12/18 16:00 Appendix II - Laboratory Analytical Reports 2�SQ pCCgF ENCO Laboratories 9e0 Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, November 6, 2020 S&ME, Inc. (SM004) Attn: Edmund Henriques 8646 West Market Street, Suite 105 Greensboro, NC 27409 RE: Laboratory Results for Project Number: 4358-20-043A Phase 01, Project Name/Desc: Moore County Private Well ENCO Workorder(s): CD16587 Dear Edmund Henriques, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, October 16, 2020. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, 0"6LC'=-:;tA Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 21 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: PW-1 Lab ID: CD36587-01 Sampled: 10/15/20 11:00 Received: 10/16/20 12:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A 04/13/21 10/22/20 13:01 10/26/20 11:20 EPA 7470A EPA 7470A 11/12/20 10/26/20 09:24 10/28/20 11:17 EPA 8260D EPA 503013_MS 10/29/20 10/23/20 00:00 10/23/20 13:53 EPA 8260D EPA 503013_MS 10/29/20 10/25/20 10:52 10/27/20 02:23 Client ID: 6301-SW-1 Lab ID: CD36587-02 Sampled: 10/15/20 10:30 Received: 10/16/20 12:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A 04/13/21 10/22/20 13:01 10/26/20 11:23 EPA 6020E EPA 3005A 04/13/21 11/02/20 13:41 11/05/20 02:50 EPA 7470A EPA 7470A 11/12/20 10/26/20 09:24 10/28/20 11:19 EPA 8260D EPA 503013_MS 10/29/20 10/23/20 00:00 10/23/20 14:38 EPA 8260D EPA 503013_MS 10/29/20 10/25/20 10:52 10/27/20 02:53 Client ID: 6301-SW-2 Lab ID: CD36587-03 Sampled: 10/15/20 08:05 Received: 10/16/20 12:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A 04/13/21 10/22/20 13:01 10/26/20 11:25 EPA 6020E EPA 3005A 04/13/21 11/02/20 13:41 11/05/20 02:54 EPA 7470A EPA 7470A 11/12/20 10/26/20 09:24 10/28/20 11:21 EPA 8260D EPA 503013_MS 10/29/20 10/23/20 00:00 10/23/20 15:03 EPA 8260D EPA 503013_MS 10/29/20 10/25/20 10:52 10/27/20 03:23 Client ID: 6301-SW-3 Lab ID: CD16587-04 Sampled: 10/15/20 09:45 Received: 10/16/20 12:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A 04/13/21 10/22/20 13:01 10/26/20 11:28 EPA 6020E EPA 3005A 04/13/21 11/02/20 13:41 11/05/20 02:58 EPA 7470A EPA 7470A 11/12/20 10/26/20 09:24 10/28/20 11:24 EPA 8260D EPA 5030B_MS 10/29/20 10/23/20 00:00 10/23/20 15:28 EPA 8260D EPA 503013_MS 10/29/20 10/25/20 10:52 10/27/20 03:53 Client ID: 6301-SW-4 Lab ID: CD16587-05 Sampled: 10/15/20 09:00 Received: 10/16/20 12:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A 04/13/21 10/22/20 13:01 10/26/20 11:30 EPA 6020E EPA 3005A 04/13/21 11/02/20 13:41 11/05/20 03:03 EPA 7470A EPA 7470A 11/12/20 10/26/20 09:24 10/28/20 11:26 EPA 8260D EPA 503013_MS 10/29/20 10/23/20 00:00 10/23/20 15:54 EPA 8260D EPA 5030B_MS 10/29/20 10/25/20 10:52 10/27/20 04:23 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 21 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: PW-1 Lab ID: CD16587-01 Analvte Results Flag MDL PQL Units Method Notes Barium - Total 19.0 1.10 10.0 ug/L EPA 6010D Lead - Total 11.4 3.10 10.0 ug/L EPA 6010D Client ID: 6301-SW-1 Lab ID: CD16587-02 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 2.5 0.80 2.0 ug/L EPA 8260D Barium - Total 22.6 1.10 10.0 ug/L EPA 6010D Chlorobenzene 0.98 3 0.17 1.0 ug/L EPA 8260D Copper - Total 1.78 3 1.60 10.0 ug/L EPA 6010D Iron - Total 25200 22.0 50.0 ug/L EPA 6010D Manganese - Total 51.7 1.50 10.0 uq/L EPA 6010D Client ID: 6301-SW-2 Lab ID: CD16587-03 Analvte Results Flag MDL PQL Units Method Notes Barium - Total 11.1 1.10 10.0 ug/L EPA 6010D Iron - Total 618 22.0 50.0 ug/L EPA 6010D Manganese - Total 13.7 1.50 10.0 ug/L EPA 6010D Client ID: 6301-SW-3 Lab ID: CD16587-04 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 2.7 0.80 2.0 ug/L EPA 8260D Barium - Total 23.0 1.10 10.0 ug/L EPA 6010D Cadmium - Total 0.378 3 0.360 1.00 ug/L EPA 6010D Copper - Total 2.13 3 1.60 10.0 ug/L EPA 6010D Iron - Total 20800 22.0 50.0 ug/L EPA 6010D Manganese - Total 50.6 1.50 10.0 ug/L EPA 6010D Client ID: 6301-SW-4 Lab ID: CD16587-05 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 0.91 3 0.80 2.0 ug/L EPA 8260D Barium - Total 27.6 1.10 10.0 ug/L EPA 6010D Iron - Total 8690 22.0 50.0 ug/L EPA 6010D Manganese - Total 88.0 1.50 10.0 ug/L EPA 6010D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 21 00� www.encolabs.com ANALYTICAL RESULTS Description: PW-1 Lab Sample ID:CD16587-01 Received: 10/16/20 12:30 Matrix: Ground Water Sampled:10/15/20 11:00 Work Order: CD16587 Project: Moore County Private Well Sampled By: Gary Simcox Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte FCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 O126029 EPA 8260D 10/27/20 02:23 REF 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 O126029 EPA 8260D 10/27/20 02:23 REF 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 O126029 EPA 8260D 10/27/20 02:23 REF 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 O126029 EPA 8260D 10/27/20 02:23 REF 1,1-Dichloroethane [75-34-3]A 0.13 u ug/L 1 0.13 1.0 O126029 EPA 8260D 10/27/20 02:23 REF 1,1-Dichloroethene [75-35-4]A 0.21 u ug/L 1 0.21 1.0 O126029 EPA 8260D 10/27/20 02:23 REF QL-02, QV-01 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF 1,2-Dichloroethane [107-06-2]A 0.21 U ug/L 1 0.21 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF 1,2-Dichloropropene [78-87-5]A 0.10 U ug/L 1 0.10 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 OJ26029 EPA 8260D 10/27/20 02:23 REF 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 OJ26029 EPA 8260D 10/27/20 02:23 REF 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Acetone [67-64-1]A 10 U ug/L 1 10 20 OJ26029 EPA 8260D 10/27/20 02:23 REF Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 OJ26029 EPA 8260D 10/27/20 02:23 REF Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Bromodichloromethane [75-27-4]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Carbon disulfide [75-15-O]A 1.5 u ug/L 1 1.5 5.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF QV-01 Chloroform [67-66-3]A 0.18 u ug/L 1 0.18 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF cis-1,2-Dichloroethene [156-59-2]A 0.15 u ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Tetrahydrofuran [109-99-9]A 0.53 u ug/L 1 0.53 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Toluene [108-88-3]A 0.14 u ug/L 1 0.14 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 OJ26029 EPA 8260D 10/27/20 02:23 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 21 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: PW-1 Lab Sample ID:CD16587-01 Received: 10/16/20 12:30 Matrix: Ground Water Sampled:10/15/20 11:00 Work Order: CD16587 Project: Moore County Private Well Sampled By: Gary Simcox Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 OJ26029 EPA 8260D 10/27/20 02:23 REF QV-01 Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 OJ26029 EPA 8260D 10/27/20 02:23 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 51 1 50.0 103 % 53-136 OJ26029 EPA 626OD 10127120 02:23 REF Dibromofluoromethane 61 1 50.0 122 % 67-129 OJ26029 EPA 626OD 10127120 02:23 REF Toluene-d8 54 1 50.0 108 % 59-134 OJ26029 EPA 626OD 10127120 02:23 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 OJ26011 EPA 7470A 10/28/20 11:17 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 OJ22023 EPA 6010D 10/26/20 11:20 JDH Barium [7440-39-3]^ 19.0 ug/L 1 1.10 10.0 O122023 EPA 6010D 10/26/20 11:20 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 OJ22023 EPA 6010D 10/26/20 11:20 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 OJ22023 EPA 6010D 10/26/20 11:20 JDH Lead [7439-92-1]^ 11.4 ug/L 1 3.10 10.0 O122023 EPA 6010D 10/26/20 11:20 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 OJ22023 EPA 6010D 10/26/20 11:20 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 OJ22023 EPA 6010D 10/26/20 11:20 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte MAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 OJ23037 EPA 8260D 10/23/20 13:53 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.1 1 5.00 102 % 75-125 OJ23037 EPA 826OD 1012312013:53 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 21 00� www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW-1 Lab Sample ID:CD16587-02 Received: 10/16/20 12:30 Matrix: Ground Water Sampled:10/15/20 10:30 Work Order: CD16587 Project: Moore County Private Well Sampled By: Gary Simcox Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte FCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 u ug/L 1 0.17 1.0 O126029 EPA 8260D 10/27/20 02:53 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 u ug/L 1 0.12 1.0 O126029 EPA 8260D 10/27/20 02:53 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 u ug/L 1 0.28 1.0 O126029 EPA 8260D 10/27/20 02:53 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 u ug/L 1 0.14 1.0 O126029 EPA 8260D 10/27/20 02:53 REF 1,1-Dichloroethane [75-34-3]A 0.13 u ug/L 1 0.13 1.0 O126029 EPA 8260D 10/27/20 02:53 REF 1,1-Dichloroethene [75-35-4]A 0.21 u ug/L 1 0.21 1.0 O126029 EPA 8260D 10/27/20 02:53 REF QL-02, QV-01 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF 1,2-Dichloropropene [78-87-5]A 0.10 U ug/L 1 0.10 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 OJ26029 EPA 8260D 10/27/20 02:53 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 OJ26029 EPA 8260D 10/27/20 02:53 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 OJ26029 EPA 8260D 10/27/20 02:53 REF Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 OJ26029 EPA 8260D 10/27/20 02:53 REF Benzene[71-43-2]^ 0.15 u ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Bromochloromethane [74-97-5]^ 0.48 u ug/L 1 0.48 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Carbon disulfide [75-15-O]^ 1.5 U ug/L 1 1.5 5.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Chlorobenzene [108-90-7]^ 0.98 J ug/L 1 0.17 1.0 O326029 EPA 8260D 10/27/20 02:53 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF QV-01 Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Chloromethane [74-87-3]^ 0.13 u ug/L 1 0.13 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF cis-1,2-Dichloroethene [156-59-2]A 0.15 u ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 u ug/L 1 0.20 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Dibromochloromethane [124-48-1]^ 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Dibromomethane [74-95-3]^ 0.27 u ug/L 1 0.27 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Ethylbenzene [100-41-4]^ 0.13 u ug/L 1 0.13 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Naphthalene [91-20-3]A 0.11 u ug/L 1 0.11 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Styrene [100-42-5]^ 0.11 u ug/L 1 0.11 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Tetrachloroethene [127-18-4]^ 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Tetrahydrofuran [109-99-9]^ 0.53 u ug/L 1 0.53 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 21 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW-1 Lab Sample ID:CD16587-02 Received: 10/16/20 12:30 Matrix: Ground Water Sampled:10/15/20 10:30 Work Order: CD16587 Project: Moore County Private Well Sampled By: Gary Simcox Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl acetate [108-05-4]^ 0.95 u ug/L 1 0.95 5.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Vinyl chloride [75-01-4]^ 0.32 u ug/L 1 0.32 1.0 OJ26029 EPA 8260D 10/27/20 02:53 REF QV-01 Xylenes (Total) [1330-20-7]^ 0.45 u ug/L 1 0.45 3.0 OJ26029 EPA 8260D 10/27/20 02:53 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 52 1 50.0 103 % 53-136 OJ26029 EPA 6260D 10127120 02:53 REF Dlbromofluoromethane 60 1 50.0 120 % 67-129 OJ26029 EPA 6260D 10127120 02:53 REF Toluene-d8 55 1 50.0 109 % 59-134 OJ26029 EPA 6260D 10127120 02:53 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 u ug/L 1 0.150 0.200 OJ26011 EPA 7470A 10/28/20 11:19 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Antimony [7440-36-O]^ 0.740 u ug/L 2 0.740 2.00 OK02037 EPA 6020B 11/05/20 02:50 RLF Arsenic[7440-38-2]^ 7.60 u ug/L 1 7.60 10.0 OJ22023 EPA 6010D 10/26/20 11:23 JDH Barium [7440-39-3]^ 22.6 ug/L 1 1.10 10.0 0122023 EPA 6010D 10/26/20 11:23 JDH Beryllium [7440-41-7]^ 0.160 u ug/L 1 0.160 1.00 OJ22023 EPA 6010D 10/26/20 11:23 JDH Cadmium [7440-43-9]^ 0.360 u ug/L 1 0.360 1.00 OJ22023 EPA 6010D 10/26/20 11:23 JDH Chromium [7440-47-3]^ 1.40 u ug/L 1 1.40 10.0 OJ22023 EPA 6010D 10/26/20 11:23 JDH Cobalt[7440-48-4]^ 1.40 u ug/L 1 1.40 10.0 OJ22023 EPA 6010D 10/26/20 11:23 JDH Copper[7440-50-8]^ 1.78 J ug/L 1 1.60 10.0 0122023 EPA 6010D 10/26/20 11:23 JDH Iron [7439-89-6]^ 25200 ug/L 1 22.0 50.0 0122023 EPA 6010D 10/26/20 11:23 JDH Lead [7439-92-1]^ 3.10 u ug/L 1 3.10 10.0 OJ22023 EPA 6010D 10/26/20 11:23 JDH Manganese [7439-96-5]^ 51.7 ug/L 1 1.50 10.0 0122023 EPA 6010D 10/26/20 11:23 JDH Nickel[7440-02-O]^ 2.20 u ug/L 1 2.20 10.0 OJ22023 EPA 6010D 10/26/20 11:23 JDH Selenium [7782-49-2]^ 1.82 u ug/L 2 1.82 2.00 OK02037 EPA 6020B 11/05/20 02:50 RLF Silver[7440-22-4]^ 1.90 u ug/L 1 1.90 10.0 OJ22023 EPA 6010D 10/26/20 11:23 JDH Thallium [7440-28-O]^ 0.220 u ug/L 2 0.220 2.00 OK02037 EPA 6020B 11/05/20 02:50 RLF Vanadium [7440-62-2]^ 1.40 u ug/L 1 1.40 10.0 OJ22023 EPA 6010D 10/26/20 11:23 JDH Zinc[7440-66-6]^ 4.40 u ug/L 1 4.40 10.0 OJ22023 EPA 6010D 10/26/20 11:23 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl 1,4-Dioxane [123-91-1]^ Surrogates Toluene-d8 Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 2.5 ug/L 1 0.80 2.0 0123037 EPA 8260D 10/23/20 14:38 KKW Results DF Soike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes 5.4 1 5.00 108 % 75-125 OJ23037 EPA 8260D 10123120 14:38 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 21 00� www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW-2 Lab Sample ID:CD16587-03 Received: 10/16/20 12:30 Matrix: Ground Water Sampled:10/15/20 08:05 Work Order: CD16587 Project: Moore County Private Well Sampled By: Gary Simcox Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte FCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 O126029 EPA 8260D 10/27/20 03:23 REF 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 O126029 EPA 8260D 10/27/20 03:23 REF 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 O126029 EPA 8260D 10/27/20 03:23 REF 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 O126029 EPA 8260D 10/27/20 03:23 REF 1,1-Dichloroethane [75-34-3]A 0.13 u ug/L 1 0.13 1.0 O126029 EPA 8260D 10/27/20 03:23 REF 1,1-Dichloroethene [75-35-4]A 0.21 u ug/L 1 0.21 1.0 O126029 EPA 8260D 10/27/20 03:23 REF QL-02, QV-01 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF 1,2-Dichloroethane [107-06-2]A 0.21 U ug/L 1 0.21 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF 1,2-Dichloropropene [78-87-5]A 0.10 U ug/L 1 0.10 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 OJ26029 EPA 8260D 10/27/20 03:23 REF 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 OJ26029 EPA 8260D 10/27/20 03:23 REF 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Acetone [67-64-1]A 10 U ug/L 1 10 20 OJ26029 EPA 8260D 10/27/20 03:23 REF Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 OJ26029 EPA 8260D 10/27/20 03:23 REF Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Bromodichloromethane [75-27-4]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF QV-01 Chloroform [67-66-3]A 0.18 u ug/L 1 0.18 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF cis-1,2-Dichloroethene [156-59-2]A 0.15 u ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Naphthalene [91-20-3]A 0.11 u ug/L 1 0.11 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Tetrahydrofuran [109-99-9]A 0.53 u ug/L 1 0.53 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 21 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW-2 Lab Sample ID:CD16587-03 Received: 10/16/20 12:30 Matrix: Ground Water Sampled:10/15/20 08:05 Work Order: CD16587 Project: Moore County Private Well Sampled By: Gary Simcox Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 OJ26029 EPA 8260D 10/27/20 03:23 REF QV-01 Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 OJ26029 EPA 8260D 10/27/20 03:23 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 53 1 50.0 105 % 53-136 OJ26029 EPA 6260D 10127120 03:23 REF Dlbromofluoromethane 59 1 50.0 117 % 67-129 OJ26029 EPA 6260D 10127120 03:23 REF Toluene-d8 53 1 50.0 105 % 59-134 OJ26029 EPA 6260D 10127120 03:23 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 OJ26011 EPA 7470A 10/28/20 11:21 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 OK02037 EPA 6020B 11/05/20 02:54 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 OJ22023 EPA 6010D 10/26/20 11:25 JDH Barium [7440-39-3]^ 11.1 ug/L 1 1.10 10.0 0122023 EPA 6010D 10/26/20 11:25 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 OJ22023 EPA 6010D 10/26/20 11:25 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 OJ22023 EPA 6010D 10/26/20 11:25 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 OJ22023 EPA 6010D 10/26/20 11:25 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 OJ22023 EPA 6010D 10/26/20 11:25 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 OJ22023 EPA 6010D 10/26/20 11:25 JDH Iron [7439-89-6]^ 618 ug/L 1 22.0 50.0 0122023 EPA 6010D 10/26/20 11:25 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 OJ22023 EPA 6010D 10/26/20 11:25 JDH Manganese [7439-96-S]^ 13.7 ug/L 1 1.50 10.0 0122023 EPA 6010D 10/26/20 11:25 JDH Nickel[7440-02-O]^ 2.20 U ug/L 1 2.20 10.0 OJ22023 EPA 6010D 10/26/20 11:25 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 OK02037 EPA 6020B 11/05/20 02:54 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 OJ22023 EPA 6010D 10/26/20 11:25 JDH Thallium [7440-28-O]^ 0.220 U ug/L 2 0.220 2.00 OK02037 EPA 6020B 11/05/20 02:54 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 OJ22023 EPA 6010D 10/26/20 11:25 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 OJ22023 EPA 6010D 10/26/20 11:25 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl 1,4-Dioxane [123-91-1]^ Surrogates Toluene-d8 Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 0.80 U ug/L 1 0.80 2.0 OJ23037 EPA 8260D 10/23/20 15:03 KKW Results DF Soike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes 5.1 1 5.00 102 % 75-125 OJ23037 EPA 8260D 1012312015:03 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 21 00� www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW-3 Lab Sample ID:CD16587-04 Received: 10/16/20 12:30 Matrix: Ground Water Sampled:10/15/20 09:45 Work Order: CD16587 Project: Moore County Private Well Sampled By: Gary Simcox Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte FCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 0126029 EPA 8260D 10/27/20 03:53 REF 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 0126029 EPA 8260D 10/27/20 03:53 REF 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 0126029 EPA 8260D 10/27/20 03:53 REF 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 0126029 EPA 8260D 10/27/20 03:53 REF 1,1-Dichloroethane [75-34-3]A 0.13 u ug/L 1 0.13 1.0 0126029 EPA 8260D 10/27/20 03:53 REF 1,1-Dichloroethene [75-35-4]A 0.21 u ug/L 1 0.21 1.0 0126029 EPA 8260D 10/27/20 03:53 REF QL-02, QV-01 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF 1,2-Dichloroethane [107-06-2]A 0.21 U ug/L 1 0.21 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF 1,2-Dichloropropene [78-87-5]A 0.10 U ug/L 1 0.10 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 OJ26029 EPA 8260D 10/27/20 03:53 REF 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 OJ26029 EPA 8260D 10/27/20 03:53 REF 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Acetone [67-64-1]A 10 U ug/L 1 10 20 OJ26029 EPA 8260D 10/27/20 03:53 REF Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 OJ26029 EPA 8260D 10/27/20 03:53 REF Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Bromodichloromethane [75-27-4]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Carbon disulfide [75-15-O]A 1.5 u ug/L 1 1.5 5.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF QV-01 Chloroform [67-66-3]A 0.18 u ug/L 1 0.18 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF cis-1,2-Dichloroethene [156-59-2]A 0.15 u ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Naphthalene [91-20-3]A 0.11 u ug/L 1 0.11 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Tetrahydrofuran [109-99-9]A 0.53 u ug/L 1 0.53 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 21 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW-3 Lab Sample ID:CD16587-04 Received: 10/16/20 12:30 Matrix: Ground Water Sampled:10/15/20 09:45 Work Order: CD16587 Project: Moore County Private Well Sampled By: Gary Simcox Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl acetate [108-05-4]^ 0.95 u ug/L 1 0.95 5.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Vinyl chloride [75-01-4]^ 0.32 u ug/L 1 0.32 1.0 OJ26029 EPA 8260D 10/27/20 03:53 REF QV-01 Xylenes (Total) [1330-20-7]^ 0.45 u ug/L 1 0.45 3.0 OJ26029 EPA 8260D 10/27/20 03:53 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 52 1 50.0 103 % 53-136 OJ26029 EPA 6260D 10127120 03:53 REF Dlbromofluoromethane 60 1 50.0 120 % 67-129 OJ26029 EPA 6260D 10127120 03:53 REF Toluene-d8 54 1 50.0 108 % 59-134 OJ26029 EPA 6260D 10127120 03:53 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 u ug/L 1 0.150 0.200 OJ26011 EPA 7470A 10/28/20 11:24 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 u ug/L 2 0.740 2.00 OK02037 EPA 6020B 11/05/20 02:58 RLF Arsenic[7440-38-2]^ 7.60 u ug/L 1 7.60 10.0 OJ22023 EPA 6010D 10/26/20 11:28 JDH Barium [7440-39-3]^ 23.0 ug/L 1 1.10 10.0 0122023 EPA 6010D 10/26/20 11:28 JDH Beryllium [7440-41-7]^ 0.160 u ug/L 1 0.160 1.00 OJ22023 EPA 6010D 10/26/20 11:28 JDH Cadmium [7440-43-9]^ 0.378 J ug/L 1 0.360 1.00 0122023 EPA 6010D 10/26/20 11:28 JDH Chromium [7440-47-3]^ 1.40 u ug/L 1 1.40 10.0 OJ22023 EPA 6010D 10/26/20 11:28 JDH Cobalt[7440-48-4]^ 1.40 u ug/L 1 1.40 10.0 OJ22023 EPA 6010D 10/26/20 11:28 JDH Copper[7440-50-8]^ 2.13 J ug/L 1 1.60 10.0 0122023 EPA 6010D 10/26/20 11:28 JDH Iron [7439-89-6]^ 20800 ug/L 1 22.0 50.0 0122023 EPA 6010D 10/26/20 11:28 JDH Lead [7439-92-1]^ 3.10 u ug/L 1 3.10 10.0 OJ22023 EPA 6010D 10/26/20 11:28 JDH Manganese [7439-96-5]^ 50.6 ug/L 1 1.50 10.0 0122023 EPA 6010D 10/26/20 11:28 JDH Nickel[7440-02-O]^ 2.20 u ug/L 1 2.20 10.0 OJ22023 EPA 6010D 10/26/20 11:28 JDH Selenium [7782-49-2]^ 1.82 u ug/L 2 1.82 2.00 OK02037 EPA 6020B 11/05/20 02:58 RLF Silver[7440-22-4]^ 1.90 u ug/L 1 1.90 10.0 OJ22023 EPA 6010D 10/26/20 11:28 JDH Thallium [7440-28-O]^ 0.220 u ug/L 2 0.220 2.00 OK02037 EPA 6020B 11/05/20 02:58 RLF Vanadium [7440-62-2]^ 1.40 u ug/L 1 1.40 10.0 OJ22023 EPA 6010D 10/26/20 11:28 JDH Zinc[7440-66-6]^ 4.40 u ug/L 1 4.40 10.0 OJ22023 EPA 6010D 10/26/20 11:28 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl 1,4-Dioxane [123-91-1]^ Surrogates Toluene-d8 Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 2.7 ug/L 1 0.80 2.0 0123037 EPA 8260D 10/23/20 15:28 KKW Results DF Soike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes 5.1 1 5.00 101 % 75-125 OJ23037 EPA 8260D 1012312015:28 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 21 00� www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW-4 Lab Sample ID:CD16587-05 Received: 10/16/20 12:30 Matrix: Ground Water Sampled:10/15/20 09:00 Work Order: CD16587 Project: Moore County Private Well Sampled By: Gary Simcox Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte FCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 u ug/L 1 0.17 1.0 O126029 EPA 8260D 10/27/20 04:23 REF 1,1,1-Trichloroethane [71-55-6]A 0.12 u ug/L 1 0.12 1.0 O126029 EPA 8260D 10/27/20 04:23 REF 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 u ug/L 1 0.28 1.0 O126029 EPA 8260D 10/27/20 04:23 REF 1,1,2-Trichloroethane [79-00-5]A 0.14 u ug/L 1 0.14 1.0 O126029 EPA 8260D 10/27/20 04:23 REF 1,1-Dichloroethane [75-34-3]A 0.13 u ug/L 1 0.13 1.0 O126029 EPA 8260D 10/27/20 04:23 REF 1,1-Dichloroethene [75-35-4]A 0.21 u ug/L 1 0.21 1.0 O126029 EPA 8260D 10/27/20 04:23 REF QL-02, QV-01 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF 1,2-Dichloroethane [107-06-2]A 0.21 U ug/L 1 0.21 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF 1,2-Dichloropropene [78-87-5]A 0.10 U ug/L 1 0.10 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 OJ26029 EPA 8260D 10/27/20 04:23 REF 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 OJ26029 EPA 8260D 10/27/20 04:23 REF 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Acetone [67-64-1]A 10 U ug/L 1 10 20 OJ26029 EPA 8260D 10/27/20 04:23 REF Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 OJ26029 EPA 8260D 10/27/20 04:23 REF Benzene[71-43-2]A 0.15 u ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Bromochloromethane [74-97-5]A 0.48 u ug/L 1 0.48 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Bromodichloromethane [75-27-4]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Carbon disulfide [75-15-0]A 1.5 u ug/L 1 1.5 5.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Carbon tetrachloride [56-23-5]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Chlorobenzene [108-90-7]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Chloroethane [75-00-3]A 0.23 u ug/L 1 0.23 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF QV-01 Chloroform [67-66-3]A 0.18 u ug/L 1 0.18 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Chloromethane [74-87-3]A 0.13 u ug/L 1 0.13 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF cis-1,2-Dichloroethene [156-59-2]A 0.15 u ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF cis-1,3-Dichloropropene [10061-01-5]A 0.20 u ug/L 1 0.20 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Dibromochloromethane [124-48-1]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Dibromomethane [74-95-3]A 0.27 u ug/L 1 0.27 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Ethylbenzene [100-41-4]A 0.13 u ug/L 1 0.13 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Naphthalene [91-20-3]A 0.11 u ug/L 1 0.11 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Styrene [100-42-5]A 0.11 u ug/L 1 0.11 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Tetrachloroethene [127-18-4]A 0.17 u ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Tetrahydrofuran [109-99-9]A 0.53 u ug/L 1 0.53 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 21 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-SW-4 Lab Sample ID:CD16587-05 Received: 10/16/20 12:30 Matrix: Ground Water Sampled:10/15/20 09:00 Work Order: CD16587 Project: Moore County Private Well Sampled By: Gary Simcox Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl acetate [108-05-4]^ 0.95 u ug/L 1 0.95 5.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Vinyl chloride [75-01-4]^ 0.32 u ug/L 1 0.32 1.0 OJ26029 EPA 8260D 10/27/20 04:23 REF QV-01 Xylenes (Total) [1330-20-7]^ 0.45 u ug/L 1 0.45 3.0 OJ26029 EPA 8260D 10/27/20 04:23 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 51 1 50.0 102 % 53-136 OJ26029 EPA 6260D 10127120 04:23 REF Dlbromofluoromethane 60 1 50.0 119 % 67-129 OJ26029 EPA 6260D 10127120 04:23 REF Toluene-d8 55 1 50.0 110 % 59-134 OJ26029 EPA 6260D 10127120 04:23 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 u ug/L 1 0.150 0.200 OJ26011 EPA 7470A 10/28/20 11:26 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Antimony [7440-36-O]^ 0.740 u ug/L 2 0.740 2.00 OK02037 EPA 6020B 11/05/20 03:03 RLF Arsenic[7440-38-2]^ 7.60 u ug/L 1 7.60 10.0 OJ22023 EPA 6010D 10/26/20 11:30 JDH Barium [7440-39-3]^ 27.6 ug/L 1 1.10 10.0 0122023 EPA 6010D 10/26/20 11:30 JDH Beryllium [7440-41-7]^ 0.160 u ug/L 1 0.160 1.00 OJ22023 EPA 6010D 10/26/20 11:30 JDH Cadmium [7440-43-9]^ 0.360 u ug/L 1 0.360 1.00 OJ22023 EPA 6010D 10/26/20 11:30 JDH Chromium [7440-47-3]^ 1.40 u ug/L 1 1.40 10.0 OJ22023 EPA 6010D 10/26/20 11:30 JDH Cobalt[7440-48-4]^ 1.40 u ug/L 1 1.40 10.0 OJ22023 EPA 6010D 10/26/20 11:30 JDH Copper[7440-50-8]^ 1.60 u ug/L 1 1.60 10.0 OJ22023 EPA 6010D 10/26/20 11:30 JDH Iron [7439-89-6]^ 8690 ug/L 1 22.0 50.0 0122023 EPA 6010D 10/26/20 11:30 JDH Lead [7439-92-1]^ 3.10 u ug/L 1 3.10 10.0 OJ22023 EPA 6010D 10/26/20 11:30 JDH Manganese [7439-96-S]^ 88.0 ug/L 1 1.50 10.0 0122023 EPA 6010D 10/26/20 11:30 JDH Nickel[7440-02-O]^ 2.20 u ug/L 1 2.20 10.0 OJ22023 EPA 6010D 10/26/20 11:30 JDH Selenium [7782-49-2]^ 1.82 u ug/L 2 1.82 2.00 OK02037 EPA 6020B 11/05/20 03:03 RLF Silver[7440-22-4]^ 1.90 u ug/L 1 1.90 10.0 OJ22023 EPA 6010D 10/26/20 11:30 JDH Thallium [7440-28-O]^ 0.220 u ug/L 2 0.220 2.00 OK02037 EPA 6020B 11/05/20 03:03 RLF Vanadium [7440-62-2]^ 1.40 u ug/L 1 1.40 10.0 OJ22023 EPA 6010D 10/26/20 11:30 JDH Zinc[7440-66-6]^ 4.40 u ug/L 1 4.40 10.0 OJ22023 EPA 6010D 10/26/20 11:30 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution A - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl 1,4-Dioxane [123-91-1]^ Surrogates Toluene-d8 Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 0.91 J ug/L 1 0.80 2.0 0123037 EPA 8260D 10/23/20 15:54 KKW Results DF Soike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes 5.5 1 5.00 109 % 75-125 OJ23037 EPA 8260D 1012312015:54 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 21 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch OJ26029 - EPA 5030B MS Blank (0326029-BLK1) Prepared: 10/26/2020 16:09 Analyzed: 10/26/2020 19:53 Analvte Result Flaq POL Units 1, 1, 1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Naphthalene 0.11 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Tetrahydrofuran 0.53 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 21 QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch OJ26029 - EPA 5O3OB MS - Continued (� �Eo www.encolabs.com Blank (0326029-BLK1) Continued Prepared: 10/26/2020 16:09 Analyzed: 10/26/2020 19:53 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 52 u91L 50.0 104 53-136 Dibromofluoromethane 58 u91L 50.0 117 67-129 Toluene-d8 53 u91L 50.0 106 59-134 LCS (0326029-BS1) Prepared: 10/26/2020 16:09 Analyzed: 10/26/2020 17:52 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 30 1.0 ug/L 20.0 149 75-133 QL-02 Benzene 17 1.0 ug/L 20.0 84 80-134 Chlorobenzene 18 1.0 ug/L 20.0 89 80-120 Toluene 18 1.0 ug/L 20.0 89 71-120 Trichloroethene 19 1.0 ug/L 20.0 93 74-120 Matrix Spike (OJ26029-MS1) Prepared: 10/26/2020 16:09 Analyzed: 10/26/2020 18:23 Source: CD17278-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 32 1.0 ug/L 20.0 0.21 U 162 75-133 QM-07 Benzene 19 1.0 ug/L 20.0 0.15 U 96 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 97 80-120 Toluene 20 1.0 ug/L 20.0 0.14 U 101 71-120 Trichloroethene 21 1.0 ug/L 20.0 0.15 U 107 74-120 Matrix Spike Dup (0326029-MSD1) Prepared: 10/26/2020 16:09 Analyzed: 10/26/2020 18:53 Source: CD17278-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 28 1.0 ug/L 20.0 0.21 U 139 75-133 16 20 QM-07 Benzene 16 1.0 ug/L 20.0 0.15 U 79 80-134 19 17 QM-07, QM-11 Chlorobenzene 17 1.0 ug/L 20.0 0.17 U 84 80-120 14 16 Toluene 17 1.0 ug/L 20.0 0.14 U 84 71-120 19 17 QM-11 Trichloroethene 17 1.0 ug/L 20.0 0.15 U 85 74-120 23 22 QM-11 Metals by EPA 6000/7000 Series Methods - Quality Control Batch 0116011 - EPA 747OA Blank (0326011-BLK3) Prepared: 10/26/2020 09:24 Analyzed: 10/27/2020 13:58 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Mercury 0.150 U 0.200 ug/L LCS (0326011-BS3) Prepared: 10/26/2020 09:24 Analyzed: 10/27/2020 14:01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.02 0.200 ug/L 5.00 100 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 21 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals by EPA 6000/7000 Series Methods - Quality Control Batch OJ26011 - EPA 7470A - Continued Matrix Spike (0326011-MS3) Prepared: 10/26/2020 09:24 Analyzed: 10/27/2020 14:09 Source: CD16047-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.54 0.200 ug/L 5.00 0.569 100 75-125 Matrix Spike Dup (0726011-MSD1) Prepared: 10/26/2020 09:24 Analyzed: 10/27/2020 14:11 Source: CD16047-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.63 0.200 ug/L 5.00 0.569 101 75-125 2 25 Post Spike (0326011-PS1) Prepared: 10/26/2020 09:24 Analyzed: 10/27/2020 14:13 Source: CD16047-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.75 0.200 ug/L 5.00 0.569 104 75-125 Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 0.722023 - EPA 3005A Blank (0322023-BLK3) Prepared: 10/22/2020 13:01 Analyzed: 10/26/2020 10:13 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 7.60 U 10.0 ug/L Barium 1.10 U 10.0 ug/L Beryllium 0.160 U 1.00 ug/L Cadmium 0.360 U 1.00 ug/L Chromium 1.40 U 10.0 ug/L Cobalt 1.40 U 10.0 ug/L Copper 1.60 U 10.0 ug/L Iron 22.0 U 50.0 ug/L Lead 3.10 U 10.0 ug/L Manganese 1.50 U 10.0 ug/L Nickel 2.20 U 10.0 ug/L Selenium 6.20 U 10.0 ug/L Silver 1.90 U 10.0 ug/L Vanadium 1.40 U 10.0 ug/L Zinc 4.40 U 10.0 ug/L LCS (0322023-BSI) Prepared: 10/22/2020 13:01 Analyzed: 10/26/2020 10:19 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 206 10.0 ug/L 200 103 80-120 Barium 222 10.0 ug/L 200 111 80-120 Beryllium 21.1 1.00 ug/L 20.0 105 80-120 Cadmium 21.3 1.00 ug/L 20.0 107 80-120 Chromium 214 10.0 ug/L 200 107 80-120 Cobalt 213 10.0 ug/L 200 106 80-120 Copper 213 10.0 ug/L 200 107 80-120 Iron 1090 50.0 ug/L 1000 109 80-120 Lead 215 10.0 ug/L 200 108 80-120 Manganese 215 10.0 ug/L 200 107 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 21 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch OJ22023 - EPA 3005A - Continued LCS (0322023-BS1) Continued Prepared: 10/22/2020 13:01 Analyzed: 10/26/2020 10:19 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nickel 220 10.0 ug/L 200 110 80-120 Selenium 216 10.0 ug/L 200 108 80-120 Silver 221 10.0 ug/L 200 110 80-120 Vanadium 212 10.0 ug/L 200 106 80-120 Zinc 220 10.0 ug/L 200 110 80-120 Matrix Spike (0322023-MS3) Prepared: 10/22/2020 13:01 Analyzed: 10/26/2020 10:22 Source: CD16047-05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 214 10.0 ug/L 200 7.60 U 107 75-125 Barium 243 10.0 ug/L 200 17.0 113 75-125 Beryllium 21.3 1.00 ug/L 20.0 0.160 U 106 75-125 Cadmium 21.8 1.00 ug/L 20.0 0.360 U 109 75-125 Chromium 217 10.0 ug/L 200 1.40 U 109 75-125 Cobalt 219 10.0 ug/L 200 1.40 U 109 75-125 Copper 215 10.0 ug/L 200 2.74 106 75-125 Iron 1150 50.0 ug/L 1000 150 100 75-125 Lead 217 10.0 ug/L 200 3.10 U 109 75-125 Manganese 274 10.0 ug/L 200 58.9 108 75-125 Nickel 226 10.0 ug/L 200 2.20 U 113 75-125 Selenium 224 10.0 ug/L 200 6.20 U 112 75-125 Silver 220 10.0 ug/L 200 1.90 U 110 75-125 Vanadium 214 10.0 ug/L 200 1.40 U 107 75-125 Zinc 228 10.0 ug/L 200 4.40 U 114 75-125 Matrix Spike Dup (0322023-MSD1) Prepared: 10/22/2020 13:01 Analyzed: 10/26/2020 10:25 Source: CD16047-05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 204 10.0 ug/L 200 7.60 U 102 75-125 5 20 Barium 241 10.0 ug/L 200 17.0 112 75-125 1 20 Beryllium 21.2 1.00 ug/L 20.0 0.160 U 106 75-125 0.09 20 Cadmium 21.5 1.00 ug/L 20.0 0.360 U 108 75-125 1 20 Chromium 217 10.0 ug/L 200 1.40 U 109 75-125 0.01 20 Cobalt 216 10.0 ug/L 200 1.40 U 108 75-125 1 20 Copper 215 10.0 ug/L 200 2.74 106 75-125 0.2 20 Iron 1190 50.0 ug/L 1000 150 104 75-125 3 20 Lead 213 10.0 ug/L 200 3.10 U 106 75-125 2 20 Manganese 276 10.0 ug/L 200 58.9 109 75-125 0.6 20 Nickel 223 10.0 ug/L 200 2.20 U 112 75-125 1 20 Selenium 216 10.0 ug/L 200 6.20 U 108 75-125 4 20 Silver 221 10.0 ug/L 200 1.90 U 110 75-125 0.1 20 Vanadium 213 10.0 ug/L 200 1.40 U 106 75-125 0.4 20 Zinc 224 10.0 ug/L 200 4.40 U 112 75-125 2 20 Post Spike (0322023-PSI) Prepared: 10/22/2020 13:01 Analyzed: 10/26/2020 10:27 Source: CD16047-05 Analvte Arsenic Spike Source %REC Result Flaq POL Units Level Result %REC Limits RPD 0.211 0.0100 mg/L 0.200-0.00432 106 80-120 RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 21 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch OJ22023 - EPA 3OO5A - Continued Post Spike (0322023-PSI) Continued Prepared: 10/22/2020 13:01 Analyzed: 10/26/2020 10:27 Source: CD16047-OS Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Barium 0.244 0.0100 mg/L 0.200 0.0170 113 80-120 Beryllium 0.0213 0.00100 mg/L 0.0200 3.56E-6 107 80-120 Cadmium 0.0219 0.00100 mg/L 0.0200 0.000180 109 80-120 Chromium 0.219 0.0100 mg/L 0.200 0.00114 109 80-120 Cobalt 0.219 0.0100 mg/L 0.200 0.000496 109 80-120 Copper 0.217 0.0100 mg/L 0.200 0.00274 107 80-120 Iron 1.27 0.0500 mg/L 1.00 0.150 112 80-120 Lead 0.220 0.0100 mg/L 0.200 -0.00288 110 80-120 Manganese 0.275 0.0100 mg/L 0.200 0.0589 108 80-120 Nickel 0.227 0.0100 mg/L 0.200 0.000874 113 80-120 Selenium 0.220 0.0100 mg/L 0.200 0.000285 110 80-120 Silver 0.227 0.0100 mg/L 0.200 -0.00162 114 80-120 Vanadium 0.215 0.0100 mg/L 0.200 2.30E-5 107 80-120 Zinc 0.232 0.0100 mg/L 0.200 0.00379 114 80-120 Batch OKO2O37 - EPA 3OO5A Blank (OK02037-BLK1) Prepared: 11/02/2020 13:41 Analyzed: 11/05/2020 01:28 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 0.370 U 1.00 ug/L Selenium 0.910 U 1.00 ug/L Thallium 0.110 U 1.00 ug/L LCS (OK02037-BS3) Prepared: 11/02/2020 13:41 Analyzed: 11/05/2020 01:33 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 21.2 1.00 ug/L 20.0 106 80-120 Selenium 20.8 1.00 ug/L 20.0 104 80-120 Thallium 21.3 1.00 ug/L 20.0 106 80-120 Matrix Spike (OK02037-MS3) Prepared: 11/02/2020 13:41 Analyzed: 11/05/2020 01:37 Source: CD15961-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 42.9 2.00 ug/L 40.0 0.740 U 107 75-125 Selenium 43.2 2.00 ug/L 40.0 1.82 U 108 75-125 Thallium 42.5 2.00 ug/L 40.0 0.220 U 106 75-125 Matrix Spike Dup (OK02037-MSD3) Prepared: 11/02/2020 13:41 Analyzed: 11/05/2020 01:41 Source: CD15961-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 41.8 2.00 ug/L 40.0 0.740 U 104 75-125 3 20 Selenium 41.5 2.00 ug/L 40.0 1.82 U 104 75-125 4 20 Thallium 42.2 2.00 ug/L 40.0 0.220 U 105 75-125 0.7 20 Post Spike (OK02037-PSI) Prepared: 11/02/2020 13:41 Analyzed: 11/05/2020 01:45 Source: CD15961-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 21 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch OK02037 - EPA 3005A - Continued Post Spike (OK02037-PS3) Continued Prepared: 11/02/2020 13:41 Analyzed: 11/05/2020 01:45 Source: CD15961-02 Analvte Result Flaq Antimony 23.7 Selenium 24.2 Thallium 23.8 Spike Source %REC RPD POL Units Level Result %REC Limits RPD Limit Notes 1.00 ug/L 20.0 0.0878 118 75-125 1.00 ug/L 20.0 0.185 120 75-125 1.00 ug/L 20.0 0.0750 119 75-125 Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch OJ23037 - EPA 5030B MS Blank (0123037-BLK3) Prepared: 10/23/2020 00:00 Analyzed: 10/23/2020 10:24 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 0.80 U 2.0 ug/L Toluene-& 5.4 ug/L 5.00 108 75-125 LCS (0323037-BS1) Prepared: 10/23/2020 00:00 Analyzed: 10/23/2020 09:59 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 27 2.0 ug/L 25.0 107 80-133 Toluene-& 5.0 ug/L 5.00 101 75-125 Matrix Spike (0723037-MS1) Prepared: 10/23/2020 00:00 Analyzed: 10/23/2020 12:35 Source: AD07026-01 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 26 2.0 ug/L 25.0 1.0 100 80-133 Toluene-& 5.4 ug/L 5.00 108 75-125 Matrix Spike Dup (0323037-MSD1) Prepared: 10/23/2020 00:00 Analyzed: 10/23/2020 13:00 Source: AD07026-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 27 2.0 ug/L 25.0 1.0 102 80-133 2 19 Toluene-& 5.4 ug/L 5.00 108 75-125 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 21 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits. QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there is no impact. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 21 Lam: 0 of m m m m n a n m m ocr _ LA '� a _ 3 m rr m G m R v o�om _ m �Nt l?� 41 ��vi ii� � � N0 on � w 1 Q (} m w r = 0 w m M ro v A' o o °N° o t!1 � O � - O N m m ilS N CL g m AZ O L jj u� 3 @ a n m i a _ 3 m IIJ m M1 o J Q c c c N J to cn a _ CT 'd rn ►� l� sf' ISM �m C � � � �� xr n 3 � 0 N 82800 Apponi* 1,9zBOD j O oEjdmndadA20W SIM to m a, : Ag,As,Ba,Cd,Cr,Pb,Se N ?c x Hg w � � z _ X $Z1,f3A, S740g.4A0f:g,%jk J BZW6 a `—' m fixT4A1nD�.! 67f+Q, Sly Zia A > C Z 0 a 70 Oat 8 R CD C. W e w u �A7 a �p X a /� /1 p q 0 � � m� i1RA, loll J i 7� 7 J'"�J ��i 1 LL CL ❑ z V ffi V 0 ° r N O 6 ` n N M _ v O rcr n o � c n m Q m A mIr m -can m X CA c m O a N �' y o m =Y � � w C' � a � o to ❑. w� 9� o CL O 2` Sample Preservation Verification ENCO Cary Work Order: CD16587 Client: S&ME, Inc. (5M004) �-D Logged In: 16-Oct-20 15:19 1 Logged By: Rachel Ann o ish Preservation Check Performed By: Date/Time: n��- CD19587-01 Project: Moore County Private Well Project #: 4358-20-043A Phase 01 Cant" Type Pres (pH) Requirement- pH Checked 1 In Control DatelTime Adjusted pH Adjusted Reagent Used/Comments A 250mLP+HNO3 <2 Y N I NA Y FNNA CD16587-02 Cont Type Pre$ (pH) pH Checked I Requirement In Control H Adjusted Date/Time p i Adjusted Reagent Used/Comments 9 A 250mLP+HNO3 <2 Y N I NA Y/ N NA CD16587-03 Cont Type Pres (pH) I pH Checked I Requirement In Control pH Adjusted DateMme Adjusted Reagent Used/Comments A 250mLP+HNO3 <2 Y N I NA Y N NA CD16687-04 Cont. Type. Pres (pH) pH Checked 1 pH Adjusted Date/TimeReagent UsedlComments Requirement , in Control Adjusted A 250mLP+HNO3 <2 Y 1 N/ NA I Y 1�b NA CD16587-05 A t Type Pres (pH) Requirement pH Checked,) In.Control Date/Time PHA djusted Adjusted Reagent UsedlComments A 250mLP+HNO3 <2 Y N / NA Y NJ NA Rea ent Name ID 1 H Strip ID: PH Strips COF0555 C:lelmntlPrir<<tiwKu_r-I U5erVallonunecK. rpt Reagent Name ID 3 4 Reagent Name ID 5 6 r ar;e 1 2�SQ pCCgF ENCO Laboratories 9e0 Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, November 6, 2020 S&ME, Inc. (SM004) Attn: Edmund Henriques 8646 West Market Street, Suite 105 Greensboro, NC 27409 RE: Laboratory Results for Project Number: 4358-20-043A Phase 01, Project Name/Desc: Moore County Active C & D LF ENCO Workorder(s): CD16585 Dear Edmund Henriques, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Thursday, October 15, 2020. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, 0"6LC'=-:;tA Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 83 PROJECT NARRATIVE Client: S&ME, Inc. (SM004) Project: Moore County Active C & D LF Lab ID: CD16585 (� �Eo www.encolabs.com Overview Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in the QC Remarks section below. Quality Control Samples The TOC continuing calibration blank had a positive result for the analyte ; howwever, the concentration in the CCB is less than 10% of the sample result. There is minimal impact to the data (QB-06). The associated LCS exhibited high bias; since the result is ND, there is no impact (QL-02). The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on an aceptable LCS recovery (QM-07). Post -digestion spike did not meet method requirements due to confirmed matrix effects (QM-08). Precision between duplicate matrix spikes of the same sample was outside acceptance limits (QM-11). Duplicate presision outside acceptance limits due to low analyte concentration (QR-04). Quality Control Remarks The associated CCV standard exhibited high bias; since the result is ND, there is no impact (QV-01). Other Comments The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of the report. Released By: Environmental Conservation Laboratories, Inc. Chuck Smith Project Manager FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 83 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW4 Lab ID: CD36585-01 Sampled: 10/13/20 16:05 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/10/20 10/21/20 11:28 10/22/20 00:07 EPA 310.2 NO PREP 10/27/20 10/23/20 11:23 10/23/20 12:49 EPA 353.2 NO PREP 10/15/20 16:05 10/14/20 14:46 10/15/20 11:05 EPA 353.2 [CALC] 10/15/20 16:05 10/26/20 09:34 10/26/20 14:48 EPA 6010D EPA 3005A 04/11/21 10/21/20 12:00 10/23/20 10:51 EPA 6020B EPA 3005A 04/11/21 10/27/20 14:33 11/04/20 23:33 EPA 7470A EPA 7470A 11/10/20 10/21/20 16:27 10/23/20 14:45 EPA 8260D EPA 503013_MS 10/27/20 10/20/20 00:00 10/20/20 12:27 EPA 8260D EPA 503013_MS 10/27/20 10/23/20 10:16 10/23/20 19:19 EPA 9060A NA 11/10/20 10/23/20 12:30 10/23/20 12:59 RSK 175 Same 10/27/20 10/19/20 08:01 10/19/20 13:40 SM 254OC-2011 NO PREP 10/20/20 10/20/20 17:13 10/20/20 17:13 SM 4500S2 D-2011 NO PREP 10/20/20 10/20/20 14:41 10/20/20 15:00 Client ID: 6301-MW4 Lab ID: CD36585-01RE1 Sampled: 10/13/20 16:05 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 353.2 NO PREP 11/10/20 10/26/20 09:34 10/26/20 14:48 Client ID: 6301-MWS Lab ID: CD36585-02 Sampled: 10/13/20 17:45 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/10/20 10/21/20 11:28 10/22/20 00:25 EPA 310.2 NO PREP 10/27/20 10/23/20 11:23 10/23/20 12:50 EPA 353.2 NO PREP 10/15/20 17:45 10/15/20 15:34 10/15/20 17:14 EPA 353.2 [CALC] 10/15/20 17:45 10/26/20 09:34 10/26/20 14:07 EPA 353.2 NO PREP 11/10/20 10/26/20 09:34 10/26/20 14:07 EPA 6010D EPA 3005A 04/11/21 10/21/20 12:00 10/23/20 10:54 EPA 6020E EPA 3005A 04/11/21 10/27/20 14:33 11/04/20 23:51 EPA 7470A EPA 7470A 11/10/20 10/21/20 16:27 10/23/20 15:40 EPA 8260D EPA 503013_MS 10/27/20 10/20/20 00:00 10/20/20 12:52 EPA 8260D EPA 5030B_MS 10/27/20 10/23/20 10:16 10/23/20 19:50 RSK 175 Same 10/27/20 10/19/20 08:01 10/19/20 13:56 SM 254OC-2011 NO PREP 10/20/20 10/20/20 17:13 10/20/20 17:13 SM 4500S2 D-2011 NO PREP 10/20/20 10/20/20 14:41 10/20/20 15:00 Client ID: 6301-MW5 Lab ID: CD16585-02RE1 Sampled: 10/13/20 17:45 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 9060A NA 11/10/20 10/23/20 12:30 10/27/20 11:08 Client ID: 6301-MW11SR Lab ID: CD16585-03 Sampled: 10/14/20 10:35 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/11/20 10/21/20 11:28 10/22/20 00:43 EPA 353.2 NO PREP 10/16/20 10:35 10/15/20 15:34 10/15/20 17:18 EPA 353.2 [CALC] 10/16/20 10:35 10/26/20 09:33 10/26/20 12:45 EPA 353.2 NO PREP 11/11/20 10/26/20 09:33 10/26/20 12:45 EPA 6010D EPA 3005A 04/12/21 10/21/20 12:00 10/23/20 10:56 EPA 6020B EPA 3005A 04/12/21 10/27/20 14:33 11/04/20 23:55 EPA 7470A EPA 7470A 11/11/20 10/21/20 16:27 10/23/20 15:43 EPA 8260D EPA 5030B_MS 10/28/20 10/20/20 00:00 10/20/20 13:18 EPA 8260D EPA 503013_MS 10/28/20 10/23/20 13:57 10/26/20 05:17 EPA 9060A NA 11/11/20 10/23/20 12:30 10/23/20 12:59 RSK 175 Same 10/28/20 10/19/20 08:01 10/19/20 14:12 SM 2540C-2011 NO PREP 10/21/20 10/20/20 17:13 10/20/20 17:13 SM 4500S2 D-2011 NO PREP 10/21/20 10/20/20 13:21 10/20/20 16:38 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 83 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW11SR Lab ID: CD36585-03RE3 Sampled: 10/14/20 10:35 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 310.2 NO PREP 10/28/20 10/23/20 11:23 10/23/20 13:30 RSK 175 Same 10/28/20 10/19/20 08:01 10/19/20 15:31 Client ID: 6301-MW11DR Lab ID: CD16585-04 Sampled: 10/14/20 11:45 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(sl Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/11/20 10/21/20 11:28 10/22/20 01:00 EPA 6010D EPA 3005A 04/12/21 10/21/20 12:00 10/23/20 10:58 EPA 6020E EPA 3005A 04/12/21 10/27/20 14:33 11/05/20 00:00 EPA 7470A EPA 7470A 11/11/20 10/21/20 16:27 10/23/20 15:45 EPA 8260D EPA 503013_MS 10/28/20 10/20/20 00:00 10/20/20 13:43 EPA 8260D EPA 503013_MS 10/28/20 10/23/20 13:57 10/26/20 05:44 SM 254OC-2011 NO PREP 10/21/20 10/20/20 17:13 10/20/20 17:13 SM 4500S2 D-2011 NO PREP 10/21/20 10/20/20 13:21 10/20/20 16:38 Client ID: 6301-MW11DR Lab ID: CD36585-04RE1 Sampled: 10/14/20 11:45 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(sl Prep Date/Time(s) Analysis Date/Time(s) EPA 310.2 NO PREP 10/28/20 10/23/20 11:23 10/23/20 13:31 Client ID: 6301-MW13SR Lab ID: CD36585-05 Sampled: 10/13/20 14:55 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/10/20 10/21/20 11:28 10/22/20 01:18 EPA 310.2 NO PREP 10/27/20 10/23/20 11:23 10/23/20 12:52 EPA 6010D EPA 3005A 04/11/21 10/21/20 12:00 10/23/20 11:01 EPA 6020E EPA 3005A 04/11/21 10/27/20 14:33 11/05/20 00:04 EPA 7470A EPA 7470A 11/10/20 10/21/20 16:27 10/23/20 15:47 EPA 8260D EPA 503013_MS 10/27/20 10/20/20 00:00 10/20/20 14:08 EPA 8260D EPA 5030B_MS 10/27/20 10/23/20 10:16 10/23/20 20:20 SM 2540C-2011 NO PREP 10/20/20 10/20/20 17:13 10/20/20 17:13 SM 4500S2 D-2011 NO PREP 10/20/20 10/20/20 14:41 10/20/20 15:00 Client ID: 6301-MW13DR Lab ID: CD36585-06 Sampled: 10/13/20 16:55 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/10/20 10/21/20 11:28 10/22/20 02:11 EPA 310.2 NO PREP 10/27/20 10/23/20 11:23 10/23/20 12:54 EPA 6010D EPA 3005A 04/11/21 10/21/20 12:00 10/23/20 11:03 EPA 6020E EPA 3005A 04/11/21 10/27/20 14:33 11/05/20 00:08 EPA 7470A EPA 7470A 11/10/20 10/21/20 16:27 10/23/20 15:50 EPA 8260D EPA 503013_MS 10/27/20 10/20/20 00:00 10/20/20 14:34 EPA 8260D EPA 503013_MS 10/27/20 10/23/20 10:23 10/24/20 05:49 SM 2540C-2011 NO PREP 10/20/20 10/20/20 17:13 10/20/20 17:13 SM 4500S2 D-2011 NO PREP 10/20/20 10/20/20 14:41 10/20/20 15:00 Client ID: 6301-MW14 Lab ID: CD16585-07 Sampled: 10/14/20 08:55 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/11/20 10/21/20 11:28 10/22/20 02:29 EPA 310.2 NO PREP 10/28/20 10/23/20 11:23 10/23/20 12:55 EPA 6010D EPA 3005A 04/12/21 10/21/20 12:00 10/23/20 11:06 EPA 6020E EPA 3005A 04/12/21 10/27/20 14:33 11/05/20 00:13 EPA 7470A EPA 7470A 11/11/20 10/21/20 16:27 10/23/20 16:00 EPA 8260D EPA 503013_MS 10/28/20 10/20/20 00:00 10/20/20 14:59 EPA 8260D EPA 503013_MS 10/28/20 10/23/20 13:57 10/26/20 06:12 SM 254OC-2011 NO PREP 10/21/20 10/20/20 17:13 10/20/20 17:13 SM 4500S2 D-2011 NO PREP 10/21/20 10/20/20 18:02 10/20/20 18:26 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 83 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW17S Lab ID: CD36585-08 Sampled: 10/13/20 10:35 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/10/20 10/21/20 11:28 10/21/20 14:24 EPA 310.2 NO PREP 10/27/20 10/23/20 11:23 10/23/20 12:55 EPA 6010D EPA 3005A 04/11/21 10/21/20 12:00 10/23/20 11:08 EPA 6020B EPA 3005A 04/11/21 10/27/20 14:33 11/05/20 00:17 EPA 7470A EPA 7470A 11/10/20 10/21/20 16:27 10/23/20 16:03 EPA 8260D EPA 503013_MS 10/27/20 10/20/20 00:00 10/20/20 15:24 EPA 8260D EPA 5030B_MIS 10/27/20 10/23/20 10:23 10/24/20 06:18 SM 254OC-2011 NO PREP 10/20/20 10/20/20 17:13 10/20/20 17:13 SM 4500S2 D-2011 NO PREP 10/20/20 10/20/20 14:41 10/20/20 15:00 Client ID: 6301-MW17D Lab ID: CD36585-09 Sampled: 10/13/20 11:05 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/10/20 10/21/20 11:28 10/21/20 14:42 EPA 310.2 NO PREP 10/27/20 10/20/20 13:40 10/20/20 15:44 EPA 6010D EPA 3005A 04/11/21 10/21/20 12:00 10/23/20 11:11 EPA 6020E EPA 3005A 04/11/21 10/27/20 14:33 11/05/20 00:21 EPA 7470A EPA 7470A 11/10/20 10/21/20 16:27 10/23/20 16:05 EPA 8260D EPA 503013_MS 10/27/20 10/20/20 00:00 10/20/20 15:49 EPA 8260D EPA 503013_MS 10/27/20 10/23/20 10:23 10/24/20 06:48 SM 2540C-2011 NO PREP 10/20/20 10/20/20 17:13 10/20/20 17:13 SM 4500S2 D-2011 NO PREP 10/20/20 10/20/20 14:41 10/20/20 15:00 Client ID: 6301-MW18 Lab ID: CD16585-10 Sampled: 10/13/20 14:05 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(sl EPA 300.0 NO PREP 11/10/20 10/21/20 11:28 10/21/20 15:35 EPA 6010D EPA 3005A 04/11/21 10/21/20 12:00 10/23/20 11:18 EPA 6020E EPA 3005A 04/11/21 10/27/20 14:33 11/05/20 00:25 EPA 7470A EPA 7470A 11/10/20 10/21/20 16:34 10/23/20 16:34 EPA 8260D EPA 503013_MS 10/27/20 10/20/20 00:00 10/20/20 16:15 EPA 8260D EPA 5030B_MS 10/27/20 10/23/20 10:23 10/24/20 07:18 SM 2540C-2011 NO PREP 10/20/20 10/20/20 17:13 10/20/20 17:13 SM 4500S2 D-2011 NO PREP 10/20/20 10/20/20 14:41 10/20/20 15:00 Client ID: 6301-MW18 Lab ID: CD16585-10RE1 Sampled: 10/13/20 14:05 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 310.2 NO PREP 10/27/20 10/20/20 13:40 10/20/20 16:13 Client ID: 6301-MW19 Lab ID: CD16585-11 Sampled: 10/13/20 12:25 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/10/20 10/21/20 11:28 10/21/20 15:53 EPA 310.2 NO PREP 10/27/20 10/20/20 13:40 10/20/20 15:53 EPA 6010D EPA 3005A 04/11/21 10/21/20 12:00 10/23/20 11:21 EPA 6020E EPA 3005A 04/11/21 10/27/20 14:33 11/05/20 00:30 EPA 7470A EPA 7470A 11/10/20 10/21/20 16:34 10/23/20 16:36 EPA 8081E EPA 3510C 10/20/20 11/29/20 10/20/20 04:06 10/21/20 13:20 EPA 8082A EPA 3510C 10/13/21 11/29/20 10/20/20 04:14 10/21/20 13:20 EPA 8151A Same 2 10/20/20 11/29/20 10/20/20 14:30 10/22/20 21:38 EPA 8260D EPA 5030B_MS 10/27/20 10/20/20 00:00 10/20/20 16:40 EPA 8260D EPA 503013_MS 10/27/20 10/23/20 10:23 10/24/20 07:48 EPA 8270E EPA 3510C—MS 10/20/20 11/28/20 10/19/20 07:16 10/23/20 19:30 EPA 9014 EPA 9010C 10/27/20 10/22/20 08:39 10/23/20 10:11 SM 2540C-2011 NO PREP 10/20/20 10/20/20 17:13 10/20/20 17:13 SM 4500S2 D-2011 NO PREP 10/20/20 10/20/20 14:41 10/20/20 15:00 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 83 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-FIELDBLANK Lab ID: CD36585-12 Sampled: 10/14/20 07:45 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/11/20 10/21/20 11:28 10/21/20 16:10 EPA 310.2 NO PREP 10/28/20 10/20/20 13:40 10/20/20 15:54 EPA 6010D EPA 3005A 04/12/21 10/21/20 12:00 10/23/20 11:23 EPA 6020B EPA 3005A 04/12/21 10/27/20 14:33 11/05/20 00:47 EPA 7470A EPA 7470A 11/11/20 10/21/20 16:34 10/23/20 16:39 EPA 8260D EPA 5030B_MS 10/28/20 10/20/20 00:00 10/20/20 17:05 EPA 8260D EPA 5030B_MIS 10/28/20 10/23/20 13:57 10/26/20 06:39 SM 254OC-2011 NO PREP 10/21/20 10/20/20 17:13 10/20/20 17:13 SM 4500S2 D-2011 NO PREP 10/21/20 10/20/20 18:02 10/20/20 18:26 Client ID: 6301-DUPLICATE Lab ID: CD36585-13 Sampled: 10/14/20 07:00 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/11/20 10/21/20 11:28 10/21/20 16:28 EPA 310.2 NO PREP 10/28/20 10/20/20 13:40 10/20/20 15:55 EPA 6010D EPA 3005A 04/12/21 10/21/20 12:00 10/23/20 11:25 EPA 6020E EPA 3005A 04/12/21 10/27/20 14:33 11/05/20 00:51 EPA 7470A EPA 7470A 11/11/20 10/21/20 16:34 10/23/20 16:13 EPA 8260D EPA 503013_MS 10/28/20 10/20/20 00:00 10/20/20 17:30 EPA 8260D EPA 503013_MS 10/28/20 10/23/20 13:57 10/26/20 07:07 SM 2540C-2011 NO PREP 10/21/20 10/20/20 17:13 10/20/20 17:13 SM 4500S2 D-2011 NO PREP 10/21/20 10/20/20 18:02 10/20/20 18:26 Client ID: 6301-TRIPBLANK Lab ID: CD16585-14 Sampled: 10/13/20 10:35 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MIS 10/27/20 10/20/20 00:00 10/20/20 17:56 EPA 8260D EPA 503013_MS 10/27/20 10/23/20 10:23 10/24/20 08:18 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 83 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MW4 Lab ID: CD16585-01 Analvte Results Flag MDL Q Units Method Notes 1,4-Dioxane 1.3 3 0.80 2.0 ug/L EPA 8260D Barium - Total 25.9 1.10 10.0 ug/L EPA 6010D Carbon dioxide 51.0 2.07 2.50 mg/L RSK 175 Chloride 8.9 2.2 5.0 mg/L EPA 300.0 Copper - Total 3.81 3 1.60 10.0 ug/L EPA 6010D Iron - Total 397 22.0 50.0 ug/L EPA 6010D Manganese - Total 11.0 1.50 10.0 ug/L EPA 6010D Nitrate as N 2.3 D 0.41 1.0 mg/L EPA 353.2 Sulfate as SO4 32 2.9 5.0 mg/L EPA 300.0 Total Alkalinity as CaCO3 39 14 15 mg/L EPA 310.2 Total Dissolved Solids 150 50 50 mg/L SM 2540C-2011 Total Organic Carbon 11 0.54 1.0 mg/L EPA 9060A QB-06 Client ID: 6301-MW4 Lab ID: CD36585-01RE3 Analvte Results Flag MDL PQL Units Method Notes Nitrate/Nitrite as N 2.3 D 0.41 1.0 mg/L EPA 353.2 Client ID: 6301-MWS Lab ID: CD16585-02 Analvte Results Flag MDL PQL Units Method Notes Barium - Total 15.4 1.10 10.0 ug/L EPA 6010D Carbon dioxide 21.6 2.07 2.50 mg/L RSK 175 Chloride 2.5 1 2.2 5.0 mg/L EPA 300.0 Manganese - Total 2.85 3 1.50 10.0 ug/L EPA 6010D Nitrate as N 0.38 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.38 0.041 0.10 mq/L EPA 353.2 Client ID: 6301-MW11SR Lab ID: CD16585-03 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dichlorobenzene 3.1 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 5.4 0.80 2.0 ug/L EPA 8260D Barium - Total 72.8 1.10 10.0 ug/L EPA 6010D Benzene 3.2 0.15 1.0 ug/L EPA 8260D Cadmium - Total 1.11 0.360 1.00 ug/L EPA 6010D Chloride 27 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 1.9 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 1.7 0.15 1.0 ug/L EPA 8260D Iron - Total 119000 22.0 50.0 ug/L EPA 6010D Lead - Total 7.17 3 3.10 10.0 ug/L EPA 6010D Manganese - Total 294 1.50 10.0 ug/L EPA 6010D Nitrate as N 0.090 3 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.090 3 0.041 0.10 mg/L EPA 353.2 Sulfide 0.017 3 0.010 0.10 mg/L SM 4500S2 D-2011 Tetrahydrofuran 5.8 0.53 1.0 ug/L EPA 8260D Total Dissolved Solids 550 50 50 mg/L SM 2540C-2011 Total Organic Carbon 22 0.54 1.0 mg/L EPA 9060A QB-06 Vanadium - Total 2.32 3 1.40 10.0 ug/L EPA 6010D Vinyl chloride 2.4 0.32 1.0 ug/L EPA 8260D Client ID: 6301-MW11SR Lab ID: CD16585-03RE3 Analvte Results Flag MDL PQL Units Method Notes Carbon dioxide 573 D 43.5 52.5 mg/L RSK 175 Methane 4.46 D 0.0840 0.105 mg/L RSK 175 Total Alkalinity as CaCO3 620 D 70 75 mg/L EPA 310.2 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 83 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MW11DR Lab ID: CD16585-04 Analvte Results Flag MDL Q Units Method Notes 1,1-Dichloroethane 0.43 3 0.13 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 2.6 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 4.4 0.80 2.0 ug/L EPA 8260D Barium - Total 52.7 1.10 10.0 ug/L EPA 6010D Benzene 1.9 0.15 1.0 ug/L EPA 8260D Cadmium - Total 1.09 0.360 1.00 ug/L EPA 6010D Chloride 21 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 1.3 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 3.0 0.15 1.0 ug/L EPA 8260D Cobalt - Total 1.49 3 1.40 10.0 ug/L EPA 6010D Iron - Total 83800 22.0 50.0 ug/L EPA 6010D Lead - Total 6.92 3 3.10 10.0 ug/L EPA 6010D Manganese - Total 180 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 13 2.9 5.0 mg/L EPA 300.0 Sulfide 0.022 3 0.010 0.10 mg/L SM 4500S2 D-2011 Tetrahydrofuran 2.4 0.53 1.0 ug/L EPA 8260D Total Dissolved Solids 250 50 50 mg/L SM 2540C-2011 Vanadium - Total 1.70 3 1.40 10.0 ug/L EPA 6010D Vinyl chloride 1.8 0.32 1.0 ug/L EPA 8260D Client ID: 6301-MW11DR Lab ID: CD36585-04RE3 Analvte Results Flag MDL PQL Units Method Notes Total Alkalinity as CaCO3 220 D 70 75 mq/L EPA 310.2 I Client ID: 6301-MW13SR Lab ID: CD16585-05 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 3.4 0.80 2.0 ug/L EPA 8260D Barium - Total 19.1 1.10 10.0 ug/L EPA 6010D Cadmium - Total 1.03 0.360 1.00 ug/L EPA 6010D Chloride 7.7 2.2 5.0 mg/L EPA 300.0 Iron - Total 66200 22.0 50.0 ug/L EPA 6010D Lead - Total 4.49 3 3.10 10.0 ug/L EPA 6010D Manganese - Total 569 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 16 2.9 5.0 mg/L EPA 300.0 Total Alkalinity as CaCO3 49 14 15 mg/L EPA 310.2 Total Dissolved Solids 96 50 50 mg/L SM 2540C-2011 Vanadium - Total 2.15 3 1.40 10.0 ug/L EPA 6010D Zinc - Total 455 4.40 10.0 ug/L EPA 6010D Client ID: 6301-MW13DR Lab ID: CD16585-06 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 2.5 0.80 2.0 ug/L EPA 8260D Barium - Total 44.0 1.10 10.0 ug/L EPA 6010D Chloride 5.8 2.2 5.0 mg/L EPA 300.0 cis-1,2-Dichloroethene 0.96 3 0.15 1.0 ug/L EPA 8260D Cobalt - Total 1.51 3 1.40 10.0 ug/L EPA 6010D Iron - Total 7600 22.0 50.0 ug/L EPA 6010D Manganese - Total 123 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 9.1 2.9 5.0 mg/L EPA 300.0 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 83 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MW34 Lab ID: CD16585-07 Analvte Results Flag MDL Q Units Method Notes 1,2-Dichlorobenzene 1.6 0.19 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 5.1 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 14 0.80 2.0 ug/L EPA 8260D Barium - Total 44.6 1.10 10.0 ug/L EPA 6010D Benzene 2.2 0.15 1.0 ug/L EPA 8260D Cadmium - Total 1.93 0.360 1.00 ug/L EPA 6010D Chloride 52 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 5.8 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 1.7 0.15 1.0 ug/L EPA 8260D Copper - Total 3.26 3 1.60 10.0 ug/L EPA 6010D Ethylbenzene 0.67 3 0.13 1.0 ug/L EPA 8260D Iron - Total 139000 22.0 50.0 ug/L EPA 6010D Lead - Total 11.2 3.10 10.0 ug/L EPA 6010D Manganese - Total 183 1.50 10.0 ug/L EPA 6010D Naphthalene 0.49 3 0.11 1.0 ug/L EPA 8260D Sulfate as SO4 7.1 2.9 5.0 mg/L EPA 300.0 Sulfide 0.12 0.010 0.10 mg/L SM 4500S2 D-2011 Tetrahydrofuran 3.3 0.53 1.0 ug/L EPA 8260D Toluene 0.48 3 0.14 1.0 ug/L EPA 8260D Total Alkalinity as CaCO3 190 14 15 mg/L EPA 310.2 Total Dissolved Solids 240 50 50 mg/L SM 2540C-2011 Vanadium - Total 4.83 3 1.40 10.0 ug/L EPA 6010D Vinyl chloride 2.3 0.32 1.0 ug/L EPA 8260D Xylenes (Total) 0.49 3 0.45 3.0 ug/L EPA 8260D Client ID: 6301-MW17S Lab ID: CD16585-08 Analvte Results Flag MDL Q Units Method Notes 1,4-Dioxane 2.3 0.80 2.0 ug/L EPA 8260D Barium - Total 87.9 1.10 10.0 ug/L EPA 6010D Chloride 22 2.2 5.0 mg/L EPA 300.0 cis-1,2-Dichloroethene 1.9 0.15 1.0 ug/L EPA 8260D Iron - Total 14400 22.0 50.0 ug/L EPA 6010D Manganese - Total 164 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 99 2.9 5.0 mg/L EPA 300.0 Total Alkalinity as CaCO3 140 14 15 mg/L EPA 310.2 Total Dissolved Solids 350 50 50 mg/L SM 2540C-2011 Vinyl chloride 0.79 3 0.32 1.0 ug/L EPA 8260D Client ID: 6301-MW17D Lab ID: CD16585-09 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 6.8 0.80 2.0 ug/L EPA 8260D Barium - Total 33.4 1.10 10.0 ug/L EPA 6010D Chloride 3.0 3 2.2 5.0 mg/L EPA 300.0 Chromium - Total 1.59 3 1.40 10.0 ug/L EPA 6010D Cobalt - Total 1.48 3 1.40 10.0 ug/L EPA 6010D Copper - Total 2.97 3 1.60 10.0 ug/L EPA 6010D Iron - Total 2500 22.0 50.0 ug/L EPA 6010D Manganese - Total 47.8 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 35 2.9 5.0 mg/L EPA 300.0 Total Alkalinity as CaCO3 120 14 15 mg/L EPA 310.2 Total Dissolved Solids 200 50 50 mg/L SM 2540C-2011 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 83 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MW38 Lab ID: CD16585-10 Analvte Results Flag MDL Q Units Method Notes 1,2-Dichlorobenzene 0.52 3 0.19 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 1.8 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 10 0.80 2.0 ug/L EPA 8260D Barium - Total 83.8 1.10 10.0 ug/L EPA 6010D Benzene 0.99 3 0.15 1.0 ug/L EPA 8260D Cadmium - Total 1.26 0.360 1.00 ug/L EPA 6010D Chloride 41 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 0.88 3 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 3.8 0.15 1.0 ug/L EPA 8260D Copper - Total 1.99 3 1.60 10.0 ug/L EPA 6010D Iron - Total 103000 22.0 50.0 ug/L EPA 6010D Lead - Total 7.49 3 3.10 10.0 ug/L EPA 6010D Manganese - Total 227 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 72 2.9 5.0 mg/L EPA 300.0 Sulfide 0.042 3 0.010 0.10 mg/L SM 4500S2 D-2011 Total Dissolved Solids 430 50 50 mg/L SM 2540C-2011 Vanadium - Total 2.34 1 1.40 10.0 ug/L EPA 6010D Vinyl chloride 1.9 0.32 1.0 ug/L EPA 8260D Client ID: 6301-MW38 Lab ID: CD16585-10RE3 Analvte Results Flag MDL Q Units Method Notes Total Alkalinity as CaCO3 290 D 28 30 mg/L EPA 310.2 Client ID: 6301-MW39 Lab ID: CD16585-11 Analvte Results Flag MDL Q Units Method Notes 1,4-Dioxane 2.8 0.80 2.0 ug/L EPA 8260D Barium - Total 59.5 1.10 10.0 ug/L EPA 6010D Chloride 14 2.2 5.0 mg/L EPA 300.0 Copper - Total 2.03 3 1.60 10.0 ug/L EPA 6010D Sulfate as SO4 12 2.9 5.0 mg/L EPA 300.0 Total Alkalinity as CaCO3 95 14 15 mg/L EPA 310.2 Total Dissolved Solids 160 50 50 mg/L SM 2540C-2011 Client ID: 6301-DUPLICATE Lab ID: CD16585-13 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dichlorobenzene 0.67 3 0.19 1.0 ug/L EPA 8260D Barium - Total 26.9 1.10 10.0 ug/L EPA 6010D Benzene 1.2 0.15 1.0 ug/L EPA 8260D Cadmium - Total 2.16 0.360 1.00 ug/L EPA 6010D Chloride 2.9 3 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 0.55 3 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 1.6 0.15 1.0 ug/L EPA 8260D Copper - Total 3.60 3 1.60 10.0 ug/L EPA 6010D Iron - Total 123000 22.0 50.0 ug/L EPA 6010D Lead - Total 10.1 3.10 10.0 ug/L EPA 6010D Manganese - Total 104 1.50 10.0 ug/L EPA 6010D Sulfate as SO4 7.3 2.9 5.0 mg/L EPA 300.0 Sulfide 0.016 3 0.010 0.10 mg/L SM 4500S2 D-2011 Total Alkalinity as CaCO3 110 14 15 mg/L EPA 310.2 Total Dissolved Solids 98 50 50 mg/L SM 2540C-2011 Vanadium - Total 4.97 3 1.40 10.0 ug/L EPA 6010D Vinyl chloride 0.97 3 0.32 1.0 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 83 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW4 Lab Sample ID:CD16585-01 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 16:05 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 0123010 EPA 8260D 10/23/20 19:19 REF 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 0123010 EPA 8260D 10/23/20 19:19 REF 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 0123010 EPA 8260D 10/23/20 19:19 REF 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 0123010 EPA 8260D 10/23/20 19:19 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 0123010 EPA 8260D 10/23/20 19:19 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 0123010 EPA 8260D 10/23/20 19:19 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 0123010 EPA 8260D 10/23/20 19:19 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 0123010 EPA 8260D 10/23/20 19:19 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 0123010 EPA 8260D 10/23/20 19:19 REF QV-01 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 0123010 EPA 8260D 10/23/20 19:19 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 0123010 EPA 8260D 10/23/20 19:19 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 0123010 EPA 8260D 10/23/20 19:19 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 0123010 EPA 8260D 10/23/20 19:19 REF 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 0123010 EPA 8260D 10/23/20 19:19 REF 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 0123010 EPA 8260D 10/23/20 19:19 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 0123010 EPA 8260D 10/23/20 19:19 REF Acetone [67-64- 1]A 10 U ug/L 1 10 20 0123010 EPA 8260D 10/23/20 19:19 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 0123010 EPA 8260D 10/23/20 19:19 REF Benzene [71-43-2]A 0.15 U ug/L 1 0.15 1.0 0123010 EPA 8260D 10/23/20 19:19 REF Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 0123010 EPA 8260D 10/23/20 19:19 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 0123010 EPA 8260D 10/23/20 19:19 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 0123010 EPA 8260D 10/23/20 19:19 REF Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 0123010 EPA 8260D 10/23/20 19:19 REF Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 0123010 EPA 8260D 10/23/20 19:19 REF Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 0123010 EPA 8260D 10/23/20 19:19 REF Chlorobenzene [108-90-7]A 0.17 U ug/L 1 0.17 1.0 0123010 EPA 8260D 10/23/20 19:19 REF Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 0123010 EPA 8260D 10/23/20 19:19 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 0123010 EPA 8260D 10/23/20 19:19 REF Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 0123010 EPA 8260D 10/23/20 19:19 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 0123010 EPA 8260D 10/23/20 19:19 REF cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 0123010 EPA 8260D 10/23/20 19:19 REF Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 0123010 EPA 8260D 10/23/20 19:19 REF Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 0123010 EPA 8260D 10/23/20 19:19 REF QL-02 Ethylbenzene [100-41-4]A 0.13 U ug/L 1 0.13 1.0 0123010 EPA 8260D 10/23/20 19:19 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 0123010 EPA 8260D 10/23/20 19:19 REF Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 0123010 EPA 8260D 10/23/20 19:19 REF Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 0123010 EPA 8260D 10/23/20 19:19 REF Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 0123010 EPA 8260D 10/23/20 19:19 REF Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 0123010 EPA 8260D 10/23/20 19:19 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 0123010 EPA 8260D 10/23/20 19:19 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 0123010 EPA 8260D 10/23/20 19:19 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 0123010 EPA 8260D 10/23/20 19:19 REF trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 0123010 EPA 8260D 10/23/20 19:19 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 0123010 EPA 8260D 10/23/20 19:19 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 0123010 EPA 8260D 10/23/20 19:19 REF Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 0123010 EPA 8260D 10/23/20 19:19 REF Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 0123010 EPA 8260D 10/23/20 19:19 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW4 Lab Sample ID:CD16585-01 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 16:05 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 0J23010 EPA 8260D 10/23/20 19:19 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 53 1 50.0 107 % 53-136 OJ23010 EPA 6260D 10123120 19:19 REF Dibromofluoromethane 40 1 50.0 79 % 67-129 OJ23010 EPA 6260D 10123120 19:19 REF Toluene-c48 55 1 50.0 110 % 59-134 OJ23010 EPA 6260D 10123120 19:19 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 0J21044 EPA 7470A 10/23/20 14:45 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 0J27036 EPA 6020B 11/04/20 23:33 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 0J21028 EPA 6010D 10/23/20 10:51 JDH Barium [7440-39-3]^ 25.9 ug/L 1 1.10 10.0 0121028 EPA 6010D 10/23/20 10:51 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 0J21028 EPA 6010D 10/23/20 10:51 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 0J21028 EPA 6010D 10/23/20 10:51 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 10:51 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 10:51 JDH Copper[7440-50-8]^ 3.81 J ug/L 1 1.60 10.0 0121028 EPA 6010D 10/23/20 10:51 JDH Iron [7439-89-6]^ 397 ug/L 1 22.0 50.0 0121028 EPA 6010D 10/23/20 10:51 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 0J21028 EPA 6010D 10/23/20 10:51 JDH Manganese [7439-96-5]^ 11.0 ug/L 1 1.50 10.0 0121028 EPA 6010D 10/23/20 10:51 JDH Nickel[7440-02-O]^ 2.20 U ug/L 1 2.20 10.0 0J21028 EPA 6010D 10/23/20 10:51 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 0J27036 EPA 6020B 11/04/20 23:33 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 0J21028 EPA 6010D 10/23/20 10:51 JDH Thallium [7440-28-O]^ 0.220 U ug/L 2 0.220 2.00 0J27036 EPA 6020B 11/04/20 23:33 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 10:51 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 0J21028 EPA 6010D 10/23/20 10:51 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 8.9 mg/L 1 2.2 5.0 0121015 EPA 300.0 10/22/20 00:07 UI Nitrate as N [14797-55-8] 2.3 D mg/L 10 0.41 1.0 [CALC] EPA 353.2 10/26/20 14:48 JAH Nitrate/Nitrite as N^ 2.3 D mg/L 10 0.41 1.0 0126014 EPA 353.2 10/26/20 14:48 JAH Nitrite as N [14797-65-O]^ 0.017 U mg/L 1 0.017 0.10 0J14040 EPA 353.2 10/15/20 11:05 JAH Sulfate as SO4 [14808-79-B]^ 32 mg/L 1 2.9 5.0 0121015 EPA 300.0 10/22/20 00:07 LJI Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 0J20015 iM 450052 D-2011 10/20/20 15:00 JOC Total Alkalinity as CaCO3 [471-34-1]^ 39 mg/L 1 14 15 0123015 EPA 310.2 10/23/20 12:49 JAH Total Dissolved Solids^ 150 mg/L 1 50 50 0120011 SM 254OC-2011 10/20/20 17:13 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW4 Lab Sample ID:CD16585-01 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 16:05 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MOIL P L Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 1.3 J ug/L 1 0.80 2.0 0320037 EPA 8260D 10/20/20 12:27 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.5 1 5.00 109 % 75-125 OJ20037 EPA 6260D 1012012012:27 KKW Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MOIL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 51.0 mg/L 1 2.07 2.50 O119006 RSK 175 10/19/20 13:40 KG Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 OJ19006 RSK 175 10/19/20 13:40 KG Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 OJ19006 RSK 175 10/19/20 13:40 KG Methane [74-82-8] 0.00400 U mg/L 1 0.00400 0.00500 OJ19006 RSK 175 10/19/20 13:40 KG Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MOIL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 11 mg/L 1 0.54 1.0 O122067 EPA 9060A 10/23/20 12:59 RSA QB-06 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 83 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW5 Lab Sample ID:CD16585-02 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 17:45 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 0123010 EPA 8260D 10/23/20 19:50 REF 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 0123010 EPA 8260D 10/23/20 19:50 REF 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 0123010 EPA 8260D 10/23/20 19:50 REF 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 0123010 EPA 8260D 10/23/20 19:50 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 0123010 EPA 8260D 10/23/20 19:50 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 0123010 EPA 8260D 10/23/20 19:50 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 0123010 EPA 8260D 10/23/20 19:50 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 0123010 EPA 8260D 10/23/20 19:50 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 0123010 EPA 8260D 10/23/20 19:50 REF QV-01 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 0123010 EPA 8260D 10/23/20 19:50 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 0123010 EPA 8260D 10/23/20 19:50 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 0123010 EPA 8260D 10/23/20 19:50 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 0123010 EPA 8260D 10/23/20 19:50 REF 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 0123010 EPA 8260D 10/23/20 19:50 REF 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 0123010 EPA 8260D 10/23/20 19:50 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 0123010 EPA 8260D 10/23/20 19:50 REF Acetone [67-64- 1]A 10 U ug/L 1 10 20 0123010 EPA 8260D 10/23/20 19:50 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 0123010 EPA 8260D 10/23/20 19:50 REF Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 0123010 EPA 8260D 10/23/20 19:50 REF Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Chlorobenzene [108-90-7]A 0.17 U ug/L 1 0.17 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 0123010 EPA 8260D 10/23/20 19:50 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 0123010 EPA 8260D 10/23/20 19:50 REF cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 0123010 EPA 8260D 10/23/20 19:50 REF QL-02 Ethylbenzene [100-41-4]A 0.13 U ug/L 1 0.13 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 0123010 EPA 8260D 10/23/20 19:50 REF Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 0123010 EPA 8260D 10/23/20 19:50 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 0123010 EPA 8260D 10/23/20 19:50 REF trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 0123010 EPA 8260D 10/23/20 19:50 REF trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 0123010 EPA 8260D 10/23/20 19:50 REF Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 0123010 EPA 8260D 10/23/20 19:50 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW5 Lab Sample ID:CD16585-02 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 17:45 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 0J23010 EPA 8260D 10/23/20 19:50 REF Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 0J23010 EPA 8260D 10/23/20 19:50 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 52 1 50.0 104 % 53-136 OJ23010 EPA 6260D 10123120 19:50 REF Dibromofluoromethane 54 1 50.0 107 % 67-129 OJ23010 EPA 6260D 10123120 19:50 REF Toluene-d8 54 1 50.0 109 % 59-134 OJ23010 EPA 6260D 10123120 19:50 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 0J21044 EPA 7470A 10/23/20 15:40 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes Antimony [7440-36-O]^ 0.740 U ug/L 2 0.740 2.00 0J27036 EPA 6020B 11/04/20 23:51 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 0J21028 EPA 6010D 10/23/20 10:54 JDH Barium [7440-39-3]^ 15.4 ug/L 1 1.10 10.0 0121028 EPA 6010D 10/23/20 10:54 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 0J21028 EPA 6010D 10/23/20 10:54 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 0J21028 EPA 6010D 10/23/20 10:54 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 10:54 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 10:54 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 0J21028 EPA 6010D 10/23/20 10:54 JDH Iron [7439-89-6]^ 22.0 U ug/L 1 22.0 50.0 0J21028 EPA 6010D 10/23/20 10:54 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 0J21028 EPA 6010D 10/23/20 10:54 JDH Manganese [7439-96-5]^ 2.85 J ug/L 1 1.50 10.0 0121028 EPA 6010D 10/23/20 10:54 JDH Nickel[7440-02-O]^ 2.20 U ug/L 1 2.20 10.0 0J21028 EPA 6010D 10/23/20 10:54 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 0J27036 EPA 6020B 11/04/20 23:51 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 0J21028 EPA 6010D 10/23/20 10:54 JDH Thallium [7440-28-O]^ 0.220 U ug/L 2 0.220 2.00 0J27036 EPA 6020B 11/04/20 23:51 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 10:54 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 0J21028 EPA 6010D 10/23/20 10:54 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 2.5 J mg/L 1 2.2 5.0 0121015 EPA 300.0 10/22/20 00:25 UI Nitrate as N [14797-55-8] 0.38 mg/L 1 0.041 0.10 [CALC] EPA 353.2 10/26/20 14:07 JAH Nitrate/Nitrite as N^ 0.38 mg/L 1 0.041 0.10 0126014 EPA 353.2 10/26/20 14:07 JAH Nitrite as N [14797-65-O]^ 0.017 U mg/L 1 0.017 0.10 0J15042 EPA 353.2 10/15/20 17:14 JAH Sulfate as SO4 [14808-79-8]^ 2.9 U mg/L 1 2.9 5.0 0J21015 EPA 300.0 10/22/20 00:25 LJI Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 0J20015 iM 450052 D-2011 10/20/20 15:00 JOC Total Alkalinity as CaCO3 [471-34-1]^ 14 U mg/L 1 14 15 0J23015 EPA 310.2 10/23/20 12:50 JAH Total Dissolved Solids^ 50 U mg/L 1 50 50 0J20011 SM 254OC-2011 10/20/20 17:13 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW5 Lab Sample ID:CD16585-02 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 17:45 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 0J20037 EPA 8260D 10/20/20 12:52 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.2 1 5.00 104 % 75-125 OJ20037 EPA 6260D 1012012012:52 KKW Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 21.6 mg/L 1 2.07 2.50 0119006 RSK 175 10/19/20 13:56 KG Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 0J19006 RSK 175 10/19/20 13:56 KG Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 0J19006 RSK 175 10/19/20 13:56 KG Methane [74-82-8] 0.00400 U mg/L 1 0.00400 0.00500 0J19006 RSK 175 10/19/20 13:56 KG Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Total Organic Carbon^ 0.54 U mg/L 1 0.54 1.0 0J26043 EPA 9060A 10/27/20 11:08 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 83 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW11SR Lab Sample ID:CD16585-03 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 10:35 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 05:17 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 0123024 EPA 8260D 10/26/20 05:17 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 0123024 EPA 8260D 10/26/20 05:17 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 05:17 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 05:17 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 05:17 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 05:17 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 0123024 EPA 8260D 10/26/20 05:17 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 0123024 EPA 8260D 10/26/20 05:17 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 0123024 EPA 8260D 10/26/20 05:17 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 05:17 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 0123024 EPA 8260D 10/26/20 05:17 REF 1,4-Dichlorobenzene [306-46-7]^ 3.1 ug/L 1 0.19 1.0 0123024 EPA 8260D 10/26/20 05:17 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 0123024 EPA 8260D 10/26/20 05:17 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 0123024 EPA 8260D 10/26/20 05:17 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 0123024 EPA 8260D 10/26/20 05:17 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 0123024 EPA 8260D 10/26/20 05:17 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 0123024 EPA 8260D 10/26/20 05:17 REF Benzene [71-43-2]A 3.2 ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 0123024 EPA 8260D 10/26/20 05:17 REF QV-01 Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 0123024 EPA 8260D 10/26/20 05:17 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Chlorobenzene [308-90-7]A 1.9 ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 05:17 REF cis-1,2-Dichloroethene [156-59-2]A 1.7 ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 05:17 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 0123024 EPA 8260D 10/26/20 05:17 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Tetrahydrofuran [109-99-9]A 5.8 ug/L 1 0.53 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 05:17 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 05:17 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 05:17 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 0123024 EPA 8260D 10/26/20 05:17 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW11SR Lab Sample ID:CD16585-03 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 10:35 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 2.4 ug/L 1 0.32 1.0 0123024 EPA 8260D 10/26/20 05:17 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 0J23024 EPA 8260D 10/26/20 05:17 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 46 1 50.0 92 % 53-136 OJ23024 EPA 6260D 10126120 05:17 REF Dibromofluoromethane 50 1 50.0 100 % 67-129 OJ23024 EPA 6260D 10126120 05:17 REF Toluene-d8 51 1 50.0 102 % 59-134 OJ23024 EPA 6260D 10126120 05:17 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 0J21044 EPA 7470A 10/23/20 15:43 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-O]^ 0.740 U ug/L 2 0.740 2.00 0J27036 EPA 6020B 11/04/20 23:55 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 0J21028 EPA 6010D 10/23/20 10:56 JDH Barium [7440-39-3]^ 72.8 ug/L 1 1.10 10.0 0121028 EPA 6010D 10/23/20 10:56 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 0J21028 EPA 6010D 10/23/20 10:56 JDH Cadmium [7440-43-9]^ 1.11 ug/L 1 0.360 1.00 0121028 EPA 6010D 10/23/20 10:56 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 10:56 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 10:56 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 0J21028 EPA 6010D 10/23/20 10:56 JDH Iron [7439-89-6]^ 119000 ug/L 1 22.0 50.0 0121028 EPA 6010D 10/23/20 10:56 JDH Lead [7439-92-1]^ 7.17 J ug/L 1 3.10 10.0 0121028 EPA 6010D 10/23/20 10:56 JDH Manganese [7439-96-5]^ 294 ug/L 1 1.50 10.0 0121028 EPA 6010D 10/23/20 10:56 JDH Nickel[7440-02-O]^ 2.20 U ug/L 1 2.20 10.0 0J21028 EPA 6010D 10/23/20 10:56 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 0J27036 EPA 6020B 11/04/20 23:55 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 0J21028 EPA 6010D 10/23/20 10:56 JDH Thallium [7440-28-O]^ 0.220 U ug/L 2 0.220 2.00 0J27036 EPA 6020B 11/04/20 23:55 RLF Vanadium [7440-62-2]^ 2.32 J ug/L 1 1.40 10.0 0121028 EPA 6010D 10/23/20 10:56 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 0J21028 EPA 6010D 10/23/20 10:56 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 27 mg/L 1 2.2 5.0 0121015 EPA 300.0 10/22/20 00:43 UI Nitrate as N [14797-55-8] 0.090 J mg/L 1 0.041 0.10 [CALC] EPA 353.2 10/26/20 12:45 JAH Nitrate/Nitrite as N^ 0.090 J mg/L 1 0.041 0.10 0126013 EPA 353.2 10/26/20 12:45 JAH Nitrite as N [14797-65-O]^ 0.017 U mg/L 1 0.017 0.10 0J15042 EPA 353.2 10/15/20 17:18 JAH Sulfate as SO4 [14808-79-8]^ 2.9 U mg/L 1 2.9 5.0 0J21015 EPA 300.0 10/22/20 00:43 LJI Sulfide [18496-25-8]^ 0.017 J mg/L 1 0.010 0.10 0120016 iM 450052 D-2011 10/20/20 16:38 JOC Total Alkalinity as CaCO3 [471-34-1]^ 620 D mg/L 5 70 75 0123015 EPA 310.2 10/23/20 13:30 JAH Total Dissolved Solids^ 550 mg/L 1 50 50 0120011 SM 254OC-2011 10/20/20 17:13 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW11SR Lab Sample ID:CD16585-03 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 10:35 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 5.4 ug/L 1 0.80 2.0 0320037 EPA 8260D 10/20/20 13:18 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.2 1 5.00 103 % 75-125 OJ20037 EPA 6260D 1012012013:18 KKW Dissolved Gases by GC Analyte fCAS Numberl Results Flaa Units DF MOIL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 573 D mg/L 21 43.5 52.5 O119006 RSK 175 10/19/20 15:31 KG Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 OJ19006 RSK 175 10/19/20 14:12 KG Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 OJ19006 RSK 175 10/19/20 14:12 KG Methane [74-82-8] 4.46 D mg/L 21 0.0840 0.105 O119006 RSK 175 10/19/20 15:31 KG Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flag Units DF MOIL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 22 mg/L 1 0.54 1.0 O122067 EPA 9060A 10/23/20 12:59 RSA QB-06 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 83 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW11DR Lab Sample ID:CD16585-04 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 11:45 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analvte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 05:44 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 0123024 EPA 8260D 10/26/20 05:44 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 0123024 EPA 8260D 10/26/20 05:44 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 05:44 REF 1,1-Dichloroethane [75-34-3]A 0.43 J ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 05:44 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 05:44 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 05:44 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 0123024 EPA 8260D 10/26/20 05:44 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 0123024 EPA 8260D 10/26/20 05:44 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 0123024 EPA 8260D 10/26/20 05:44 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 05:44 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 0123024 EPA 8260D 10/26/20 05:44 REF 1,4-Dichlorobenzene [306-46-7]^ 2.6 ug/L 1 0.19 1.0 0123024 EPA 8260D 10/26/20 05:44 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 0123024 EPA 8260D 10/26/20 05:44 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 0123024 EPA 8260D 10/26/20 05:44 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 0123024 EPA 8260D 10/26/20 05:44 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 0123024 EPA 8260D 10/26/20 05:44 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 0123024 EPA 8260D 10/26/20 05:44 REF Benzene [71-43-2]A 1.9 ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 05:44 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 0123024 EPA 8260D 10/26/20 05:44 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 05:44 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 0123024 EPA 8260D 10/26/20 05:44 REF QV-01 Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 05:44 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 0123024 EPA 8260D 10/26/20 05:44 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 05:44 REF Chlorobenzene [108-90-7]A 1.3 ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 05:44 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 05:44 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 0123024 EPA 8260D 10/26/20 05:44 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 05:44 REF cis-1,2-Dichloroethene [156-59-2]A 3.0 ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 05:44 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 0123024 EPA 8260D 10/26/20 05:44 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 05:44 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 0123024 EPA 8260D 10/26/20 05:44 REF Ethylbenzene[100-41-4]^ 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 05:44 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 0123024 EPA 8260D 10/26/20 05:44 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 05:44 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 0123024 EPA 8260D 10/26/20 05:44 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 05:44 REF Tetrahydrofuran [109-99-9]^ 2.4 ug/L 1 0.53 1.0 0123024 EPA 8260D 10/26/20 05:44 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 05:44 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 05:44 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 05:44 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 0123024 EPA 8260D 10/26/20 05:44 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 05:44 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 0123024 EPA 8260D 10/26/20 05:44 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 0123024 EPA 8260D 10/26/20 05:44 REF Vinyl chloride [75-01-4]A 1.8 ug/L 1 0.32 1.0 0123024 EPA 8260D 10/26/20 05:44 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW11DR Lab Sample ID:CD16585-04 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 11:45 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 0J23024 EPA 8260D 10/26/20 05:44 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 43 1 50.0 87 % 53-136 OJ23024 EPA 6260D 10126120 05:44 REF Dibromofluoromethane 49 1 50.0 99 % 67-129 OJ23024 EPA 6260D 10126120 05:44 REF Toluene-& 50 1 50.0 100 % 59-134 OJ23024 EPA 6260D 10126120 05:44 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed gy Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 0J21044 EPA 7470A 10/23/20 15:45 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 0J27036 EPA 6020B 11/05/20 00:00 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 0J21028 EPA 6010D 10/23/20 10:58 JDH Barium [7440-39-3]^ 52.7 ug/L 1 1.10 10.0 0121028 EPA 6010D 10/23/20 10:58 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 0J21028 EPA 6010D 10/23/20 10:58 JDH Cadmium [7440-43-9]^ 1.09 ug/L 1 0.360 1.00 0121028 EPA 6010D 10/23/20 10:58 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 10:58 JDH Cobalt[7440-48-4]^ 1.49 J ug/L 1 1.40 10.0 0121028 EPA 6010D 10/23/20 10:58 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 0J21028 EPA 6010D 10/23/20 10:58 JDH Iron [7439-89-6]^ 83800 ug/L 1 22.0 50.0 0121028 EPA 6010D 10/23/20 10:58 JDH Lead [7439-92-1]^ 6.92 J ug/L 1 3.10 10.0 0121028 EPA 6010D 10/23/20 10:58 JDH Manganese [7439-96-5]^ 180 ug/L 1 1.50 10.0 0121028 EPA 6010D 10/23/20 10:58 JDH Nickel[7440-02-O]^ 2.20 U ug/L 1 2.20 10.0 0J21028 EPA 6010D 10/23/20 10:58 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 0J27036 EPA 6020B 11/05/20 00:00 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 0J21028 EPA 6010D 10/23/20 10:58 JDH Thallium [7440-28-O]^ 0.220 U ug/L 2 0.220 2.00 0J27036 EPA 6020B 11/05/20 00:00 RLF Vanadium [7440-62-2]^ 1.70 J ug/L 1 1.40 10.0 0121028 EPA 6010D 10/23/20 10:58 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 0J21028 EPA 6010D 10/23/20 10:58 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed gy Notes Chloride [16887-00-6]^ 21 mg/L 1 2.2 5.0 0121015 EPA 300.0 10/22/20 01:00 UI Sulfate as SO4 [14808-79-B]^ 13 mg/L 1 2.9 5.0 0121015 EPA 300.0 10/22/20 01:00 UI Sulfide [18496-25-8]^ 0.022 J mg/L 1 0.010 0.10 0120016 iM 450052 D-2011 10/20/20 16:38 JOC Total Alkalinity as CaCO3 [471-34-1]^ 220 D mg/L 5 70 75 0123015 EPA 310.2 10/23/20 13:31 JAH Total Dissolved Solids^ 250 mg/L 1 50 50 0120011 SM 254OC-2011 10/20/20 17:13 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW11DR Lab Sample ID:CD16585-04 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 11:45 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 4.4 ug/L 1 0.80 2.0 0320037 EPA 8260D 10/20/20 13:43 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.2 1 5.00 104 % 75-125 OJ20037 EPA 6260D 1012012013:43 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 83 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW13SR Lab Sample ID:CD16585-05 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 14:55 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 0123010 EPA 8260D 10/23/20 20:20 REF 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 0123010 EPA 8260D 10/23/20 20:20 REF 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 0123010 EPA 8260D 10/23/20 20:20 REF 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 0123010 EPA 8260D 10/23/20 20:20 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 0123010 EPA 8260D 10/23/20 20:20 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 0123010 EPA 8260D 10/23/20 20:20 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 0123010 EPA 8260D 10/23/20 20:20 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 0123010 EPA 8260D 10/23/20 20:20 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 0123010 EPA 8260D 10/23/20 20:20 REF QV-01 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 0123010 EPA 8260D 10/23/20 20:20 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 0123010 EPA 8260D 10/23/20 20:20 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 0123010 EPA 8260D 10/23/20 20:20 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 0123010 EPA 8260D 10/23/20 20:20 REF 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 0123010 EPA 8260D 10/23/20 20:20 REF 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 0123010 EPA 8260D 10/23/20 20:20 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 0123010 EPA 8260D 10/23/20 20:20 REF Acetone [67-64- 1]A 10 U ug/L 1 10 20 0123010 EPA 8260D 10/23/20 20:20 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 0123010 EPA 8260D 10/23/20 20:20 REF Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 0123010 EPA 8260D 10/23/20 20:20 REF Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 0123010 EPA 8260D 10/23/20 20:20 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 0123010 EPA 8260D 10/23/20 20:20 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 0123010 EPA 8260D 10/23/20 20:20 REF Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 0123010 EPA 8260D 10/23/20 20:20 REF Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 0123010 EPA 8260D 10/23/20 20:20 REF Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 0123010 EPA 8260D 10/23/20 20:20 REF Chlorobenzene[108-90-7]A 0.17 U ug/L 1 0.17 1.0 0123010 EPA 8260D 10/23/20 20:20 REF Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 0123010 EPA 8260D 10/23/20 20:20 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 0123010 EPA 8260D 10/23/20 20:20 REF Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 0123010 EPA 8260D 10/23/20 20:20 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 0123010 EPA 8260D 10/23/20 20:20 REF cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 0123010 EPA 8260D 10/23/20 20:20 REF Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 0123010 EPA 8260D 10/23/20 20:20 REF Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 0123010 EPA 8260D 10/23/20 20:20 REF QL-02 Ethylbenzene[100-41-4]A 0.13 U ug/L 1 0.13 1.0 0123010 EPA 8260D 10/23/20 20:20 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 0123010 EPA 8260D 10/23/20 20:20 REF Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 0123010 EPA 8260D 10/23/20 20:20 REF Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 0123010 EPA 8260D 10/23/20 20:20 REF Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 0123010 EPA 8260D 10/23/20 20:20 REF Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 0123010 EPA 8260D 10/23/20 20:20 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 0123010 EPA 8260D 10/23/20 20:20 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 0123010 EPA 8260D 10/23/20 20:20 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 0123010 EPA 8260D 10/23/20 20:20 REF trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 0123010 EPA 8260D 10/23/20 20:20 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 0123010 EPA 8260D 10/23/20 20:20 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 0123010 EPA 8260D 10/23/20 20:20 REF Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 0123010 EPA 8260D 10/23/20 20:20 REF Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 0123010 EPA 8260D 10/23/20 20:20 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 23 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW13SR Lab Sample ID:CD16585-05 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 14:55 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 0J23010 EPA 8260D 10/23/20 20:20 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 54 1 50.0 107 % 53-136 OJ23010 EPA 6260D 10123120 20:20 REF Dibromofluoromethane 54 1 50.0 107 % 67-129 OJ23010 EPA 6260D 10123120 20:20 REF Toluene-c48 54 1 50.0 107 % 59-134 OJ23010 EPA 6260D 10123120 20:20 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 0J21044 EPA 7470A 10/23/20 15:47 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 0J27036 EPA 6020B 11/05/20 00:04 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 0J21028 EPA 6010D 10/23/20 11:01 JDH Barium [7440-39-3]^ 19.1 ug/L 1 1.10 10.0 0121028 EPA 6010D 10/23/20 11:01 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 0J21028 EPA 6010D 10/23/20 11:01 JDH Cadmium [7440-43-9]^ 1.03 ug/L 1 0.360 1.00 0121028 EPA 6010D 10/23/20 11:01 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 11:01 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 11:01 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 0J21028 EPA 6010D 10/23/20 11:01 JDH Iron [7439-89-6]^ 66200 ug/L 1 22.0 50.0 0121028 EPA 6010D 10/23/20 11:01 JDH Lead [7439-92-1]^ 4.49 J ug/L 1 3.10 10.0 0121028 EPA 6010D 10/23/20 11:01 JDH Manganese [7439-96-5]^ 569 ug/L 1 1.50 10.0 0121028 EPA 6010D 10/23/20 11:01 JDH Nickel[7440-02-O]^ 2.20 U ug/L 1 2.20 10.0 0J21028 EPA 6010D 10/23/20 11:01 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 0J27036 EPA 6020B 11/05/20 00:04 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 0J21028 EPA 6010D 10/23/20 11:01 JDH Thallium [7440-28-O]^ 0.220 U ug/L 2 0.220 2.00 0J27036 EPA 6020B 11/05/20 00:04 RLF Vanadium [7440-62-2]^ 2.15 J ug/L 1 1.40 10.0 0121028 EPA 6010D 10/23/20 11:01 JDH Zinc[7440-66-6]^ 455 ug/L 1 4.40 10.0 0121028 EPA 6010D 10/23/20 11:01 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed gy Notes Chloride [16887-00-6]^ 7.7 mg/L 1 2.2 5.0 0121015 EPA 300.0 10/22/20 01:18 UI Sulfate as SO4 [14808-79-B]^ 16 mg/L 1 2.9 5.0 0121015 EPA 300.0 10/22/20 01:18 UI Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 0J20015 iM 450052 D-2011 10/20/20 15:00 JOC Total Alkalinity as CaCO3 [471-34-1]^ 49 mg/L 1 14 15 0123015 EPA 310.2 10/23/20 12:52 JAH Total Dissolved Solids^ 96 mg/L 1 50 50 0120011 SM 254OC-2011 10/20/20 17:13 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 24 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW13SR Lab Sample ID:CD16585-05 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 14:55 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 3.4 ug/L 1 0.80 2.0 0320037 EPA 8260D 10/20/20 14:08 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.3 1 5.00 105 % 75-125 OJ20037 EPA 6260D 10120120 14:08 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 25 of 83 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW13DR Lab Sample ID:CD16585-06 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 16:55 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 05:49 REF 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 0123011 EPA 8260D 10/24/20 05:49 REF 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 0123011 EPA 8260D 10/24/20 05:49 REF 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 0123011 EPA 8260D 10/24/20 05:49 REF 1,1-Dichloroethane [75-34-3]A 0.13 U ug/L 1 0.13 1.0 0123011 EPA 8260D 10/24/20 05:49 REF 1,1-Dichloroethene [75-35-4]A 0.21 U ug/L 1 0.21 1.0 0123011 EPA 8260D 10/24/20 05:49 REF QV-01 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 0123011 EPA 8260D 10/24/20 05:49 REF 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 0123011 EPA 8260D 10/24/20 05:49 REF 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 0123011 EPA 8260D 10/24/20 05:49 REF 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 0123011 EPA 8260D 10/24/20 05:49 REF 1,2-Dichloroethane [107-06-2]A 0.21 U ug/L 1 0.21 1.0 0123011 EPA 8260D 10/24/20 05:49 REF 1,2-Dichloropropane [78-87-5]A 0.10 U ug/L 1 0.10 1.0 0123011 EPA 8260D 10/24/20 05:49 REF 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 0123011 EPA 8260D 10/24/20 05:49 REF 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 0123011 EPA 8260D 10/24/20 05:49 REF 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 0123011 EPA 8260D 10/24/20 05:49 REF 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 0123011 EPA 8260D 10/24/20 05:49 REF Acetone [67-64- 1]A 10 U ug/L 1 10 20 0123011 EPA 8260D 10/24/20 05:49 REF Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 0123011 EPA 8260D 10/24/20 05:49 REF Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Bromodichloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 0123011 EPA 8260D 10/24/20 05:49 REF Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Chlorobenzene[108-90-7]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Chloroform [67-66-3]A 0.18 U ug/L 1 0.18 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 0123011 EPA 8260D 10/24/20 05:49 REF cis-1,2-Dichloroethene [156-59-2]A 0.96 J ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 05:49 REF cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Ethylbenzene[100-41-4]A 0.13 U ug/L 1 0.13 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 0123011 EPA 8260D 10/24/20 05:49 REF Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Tetrahydrofuran [109-99-9]A 0.53 U ug/L 1 0.53 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 0123011 EPA 8260D 10/24/20 05:49 REF trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 0123011 EPA 8260D 10/24/20 05:49 REF trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 05:49 REF trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 0123011 EPA 8260D 10/24/20 05:49 REF Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 0123011 EPA 8260D 10/24/20 05:49 REF Vinyl chloride [75-01-4]A 0.32 U ug/L 1 0.32 1.0 0123011 EPA 8260D 10/24/20 05:49 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 26 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW13DR Lab Sample ID:CD16585-06 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 16:55 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 0J23011 EPA 8260D 10/24/20 05:49 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 53 1 50.0 107 % 53-136 OJ23011 EPA 6260D 10124120 05:49 REF Dibromofluoromethane 57 1 50.0 114 % 67-129 OJ23011 EPA 6260D 10124120 05:49 REF Toluene-c48 53 1 50.0 106 % 59-134 OJ23011 EPA 6260D 10124120 05:49 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 0J21044 EPA 7470A 10/23/20 15:50 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 0J27036 EPA 6020B 11/05/20 00:08 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 0J21028 EPA 6010D 10/23/20 11:03 JDH Barium [7440-39-3]^ 44.0 ug/L 1 1.10 10.0 0121028 EPA 6010D 10/23/20 11:03 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 0J21028 EPA 6010D 10/23/20 11:03 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 0J21028 EPA 6010D 10/23/20 11:03 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 11:03 JDH Cobalt[7440-48-4]^ 1.51 J ug/L 1 1.40 10.0 0121028 EPA 6010D 10/23/20 11:03 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 0J21028 EPA 6010D 10/23/20 11:03 JDH Iron [7439-89-6]^ 7600 ug/L 1 22.0 50.0 0121028 EPA 6010D 10/23/20 11:03 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 0J21028 EPA 6010D 10/23/20 11:03 JDH Manganese [7439-96-5]^ 123 ug/L 1 1.50 10.0 0121028 EPA 6010D 10/23/20 11:03 JDH Nickel[7440-02-O]^ 2.20 U ug/L 1 2.20 10.0 0J21028 EPA 6010D 10/23/20 11:03 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 0J27036 EPA 6020B 11/05/20 00:08 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 0J21028 EPA 6010D 10/23/20 11:03 JDH Thallium [7440-28-O]^ 0.220 U ug/L 2 0.220 2.00 0J27036 EPA 6020B 11/05/20 00:08 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 11:03 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 0J21028 EPA 6010D 10/23/20 11:03 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 5.8 mg/L 1 2.2 5.0 0121015 EPA 300.0 10/22/20 02:11 LJI Sulfate as SO4 [14808-79-8]^ 9.1 mg/L 1 2.9 5.0 0121015 EPA 300.0 10/22/20 02:11 LJI Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 0J20015 iM 450052 D-2011 10/20/20 15:00 JOC Total Alkalinity as CaCO3 [471-34-1]^ 14 U mg/L 1 14 15 0J23015 EPA 310.2 10/23/20 12:54 JAH Total Dissolved Solids^ 50 U mg/L 1 50 50 0J20011 SM 254OC-2011 10/20/20 17:13 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 27 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW13DR Lab Sample ID:CD16585-06 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 16:55 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 2.5 ug/L 1 0.80 2.0 0320037 EPA 8260D 10/20/20 14:34 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.5 1 5.00 111 % 75-125 OJ20037 EPA 6260D 10120120 14:34 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 28 of 83 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW14 Lab Sample ID:CD16585-07 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 08:55 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 06:12 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 0123024 EPA 8260D 10/26/20 06:12 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 0123024 EPA 8260D 10/26/20 06:12 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 06:12 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 06:12 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 06:12 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 06:12 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 0123024 EPA 8260D 10/26/20 06:12 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 0123024 EPA 8260D 10/26/20 06:12 REF 1,2-Dichlorobenzene [95-50-1]A 1.6 ug/L 1 0.19 1.0 0123024 EPA 8260D 10/26/20 06:12 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 06:12 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 0123024 EPA 8260D 10/26/20 06:12 REF 1,4-Dichlorobenzene [306-46-7]^ 5.1 ug/L 1 0.19 1.0 0123024 EPA 8260D 10/26/20 06:12 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 0123024 EPA 8260D 10/26/20 06:12 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 0123024 EPA 8260D 10/26/20 06:12 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 0123024 EPA 8260D 10/26/20 06:12 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 0123024 EPA 8260D 10/26/20 06:12 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 0123024 EPA 8260D 10/26/20 06:12 REF Benzene [71-43-2]A 2.2 ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 0123024 EPA 8260D 10/26/20 06:12 REF QV-01 Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 0123024 EPA 8260D 10/26/20 06:12 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Chlorobenzene [308-90-7]A 5.8 ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 06:12 REF cis-1,2-Dichloroethene [156-59-2]A 1.7 ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 06:12 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Ethylbenzene [300-41-4]A 0.67 J ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 0123024 EPA 8260D 10/26/20 06:12 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Naphthalene [91-20-3]A 0.49 J ug/L 1 0.11 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Tetrahydrofuran [109-99-9]A 3.3 ug/L 1 0.53 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Toluene [108-88-3]A 0.48 J ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 06:12 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 06:12 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 06:12 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 0123024 EPA 8260D 10/26/20 06:12 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 0123024 EPA 8260D 10/26/20 06:12 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 29 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW14 Lab Sample ID:CD16585-07 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 08:55 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 2.3 ug/L 1 0.32 1.0 0323024 EPA 8260D 10/26/20 06:12 REF Xylenes(Total)[1330-20-7]^ 0.49 J ug/L 1 0.45 3.0 0323024 EPA 8260D 10/26/20 06:12 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 44 1 50.0 88 % 53-136 OJ23024 EPA 6260D 10126120 06:12 REF Dibromofluoromethane 48 1 50.0 97 % 67-129 OJ23024 EPA 6260D 10126120 06:12 REF Toluene-d8 50 1 50.0 99 % 59-134 OJ23024 EPA 8260D 10126120 06:12 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 OJ21044 EPA 7470A 10/23/20 16:00 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-O]^ 0.740 U ug/L 2 0.740 2.00 OJ27036 EPA 6020B 11/05/20 00:13 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 OJ21028 EPA 6010D 10/23/20 11:06 JDH Barium [7440-39-3]^ 44.6 ug/L 1 1.10 10.0 0121028 EPA 6010D 10/23/20 11:06 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 OJ21028 EPA 6010D 10/23/20 11:06 JDH Cadmium [7440-43-9]^ 1.93 ug/L 1 0.360 1.00 0121028 EPA 6010D 10/23/20 11:06 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 OJ21028 EPA 6010D 10/23/20 11:06 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 OJ21028 EPA 6010D 10/23/20 11:06 JDH Copper[7440-50-8]^ 3.26 J ug/L 1 1.60 10.0 0121028 EPA 6010D 10/23/20 11:06 JDH Iron [7439-89-6]^ 139000 ug/L 1 22.0 50.0 0121028 EPA 6010D 10/23/20 11:06 JDH Lead [7439-92-1]^ 11.2 ug/L 1 3.10 10.0 0121028 EPA 6010D 10/23/20 11:06 JDH Manganese [7439-96-5]^ 183 ug/L 1 1.50 10.0 0121028 EPA 6010D 10/23/20 11:06 JDH Nickel[7440-02-O]^ 2.20 U ug/L 1 2.20 10.0 OJ21028 EPA 6010D 10/23/20 11:06 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 OJ27036 EPA 6020B 11/05/20 00:13 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 OJ21028 EPA 6010D 10/23/20 11:06 JDH Thallium [7440-28-O]^ 0.220 U ug/L 2 0.220 2.00 OJ27036 EPA 6020B 11/05/20 00:13 RLF Vanadium [7440-62-2]^ 4.83 J ug/L 1 1.40 10.0 0121028 EPA 6010D 10/23/20 11:06 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 OJ21028 EPA 6010D 10/23/20 11:06 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 52 mg/L 1 2.2 5.0 0121015 EPA 300.0 10/22/20 02:29 LJI Sulfate as SO4 [14808-79-B]^ 7.1 mg/L 1 2.9 5.0 0121015 EPA 300.0 10/22/20 02:29 LJI Sulfide [18496-25-8]^ 0.12 mg/L 1 0.010 0.10 0120017 iM 450OS2 D-2011 10/20/20 18:26 JOC Total Alkalinity as CaCO3 [471-34-1]^ 190 mg/L 1 14 15 0123015 EPA 310.2 10/23/20 12:55 JAH Total Dissolved Solids^ 240 mg/L 1 50 50 0120011 SM 254OC-2011 10/20/20 17:13 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 30 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW14 Lab Sample ID:CD16585-07 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 08:55 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 14 ug/L 1 0.80 2.0 0320037 EPA 8260D 10/20/20 14:59 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.2 1 5.00 104 % 75-125 OJ20037 EPA 6260D 10120120 14:59 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 31 of 83 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW17S Lab Sample ID:CD16585-08 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 10:35 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 06:18 REF 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 0123011 EPA 8260D 10/24/20 06:18 REF 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 0123011 EPA 8260D 10/24/20 06:18 REF 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 0123011 EPA 8260D 10/24/20 06:18 REF 1,1-Dichloroethane [75-34-3]A 0.13 U ug/L 1 0.13 1.0 0123011 EPA 8260D 10/24/20 06:18 REF 1,1-Dichloroethene [75-35-4]A 0.21 U ug/L 1 0.21 1.0 0123011 EPA 8260D 10/24/20 06:18 REF QV-01 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 0123011 EPA 8260D 10/24/20 06:18 REF 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 0123011 EPA 8260D 10/24/20 06:18 REF 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 0123011 EPA 8260D 10/24/20 06:18 REF 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 0123011 EPA 8260D 10/24/20 06:18 REF 1,2-Dichloroethane [107-06-2]A 0.21 U ug/L 1 0.21 1.0 0123011 EPA 8260D 10/24/20 06:18 REF 1,2-Dichloropropane [78-87-5]A 0.10 U ug/L 1 0.10 1.0 0123011 EPA 8260D 10/24/20 06:18 REF 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 0123011 EPA 8260D 10/24/20 06:18 REF 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 0123011 EPA 8260D 10/24/20 06:18 REF 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 0123011 EPA 8260D 10/24/20 06:18 REF 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 0123011 EPA 8260D 10/24/20 06:18 REF Acetone [67-64- 1]A 10 U ug/L 1 10 20 0123011 EPA 8260D 10/24/20 06:18 REF Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 0123011 EPA 8260D 10/24/20 06:18 REF Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Bromodichloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 0123011 EPA 8260D 10/24/20 06:18 REF Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Chlorobenzene [108-90-7]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Chloroform [67-66-3]A 0.18 U ug/L 1 0.18 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 0123011 EPA 8260D 10/24/20 06:18 REF cis-1,2-Dichloroethene [156-59-2]A 1.9 ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 06:18 REF cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Ethylbenzene [100-41-4]A 0.13 U ug/L 1 0.13 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Iodomethane [74-88-4]A 1.7 U ug/L 1 1.7 5.0 0123011 EPA 8260D 10/24/20 06:18 REF Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Tetrahydrofuran [109-99-9]A 0.53 U ug/L 1 0.53 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Toluene [108-88-3]A 0.14 U ug/L 1 0.14 1.0 0123011 EPA 8260D 10/24/20 06:18 REF trans-1,2-Dichloroethene [156-60-5]A 0.21 U ug/L 1 0.21 1.0 0123011 EPA 8260D 10/24/20 06:18 REF trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 06:18 REF trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Trichloroethene [79-01-6]A 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Trichlorofluoromethane [75-69-4]A 0.24 U ug/L 1 0.24 1.0 0123011 EPA 8260D 10/24/20 06:18 REF Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 0123011 EPA 8260D 10/24/20 06:18 REF Vinyl chloride [75-01-4]A 0.79 J ug/L 1 0.32 1.0 0123011 EPA 8260D 10/24/20 06:18 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 32 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW17S Lab Sample ID:CD16585-08 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 10:35 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 0J23011 EPA 8260D 10/24/20 06:18 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 52 1 50.0 104 % 53-136 OJ23011 EPA 6260D 10124120 06:16 REF Dibromofluoromethane 55 1 50.0 110 % 67-129 OJ23011 EPA 6260D 10124120 06:16 REF Toluene-c48 55 1 50.0 110 % 59-134 OJ23011 EPA 6260D 10124120 06:18 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 0J21044 EPA 7470A 10/23/20 16:03 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 0J27036 EPA 6020B 11/05/20 00:17 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 0J21028 EPA 6010D 10/23/20 11:08 JDH Barium [7440-39-3]^ 87.9 ug/L 1 1.10 10.0 0121028 EPA 6010D 10/23/20 11:08 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 0J21028 EPA 6010D 10/23/20 11:08 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 0J21028 EPA 6010D 10/23/20 11:08 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 11:08 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 11:08 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 0J21028 EPA 6010D 10/23/20 11:08 JDH Iron [7439-89-6]^ 14400 ug/L 1 22.0 50.0 0121028 EPA 6010D 10/23/20 11:08 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 0J21028 EPA 6010D 10/23/20 11:08 JDH Manganese [7439-96-5]^ 164 ug/L 1 1.50 10.0 0121028 EPA 6010D 10/23/20 11:08 JDH Nickel[7440-02-O]^ 2.20 U ug/L 1 2.20 10.0 0J21028 EPA 6010D 10/23/20 11:08 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 0J27036 EPA 6020B 11/05/20 00:17 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 0J21028 EPA 6010D 10/23/20 11:08 JDH Thallium [7440-28-O]^ 0.220 U ug/L 2 0.220 2.00 0J27036 EPA 6020B 11/05/20 00:17 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 11:08 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 0J21028 EPA 6010D 10/23/20 11:08 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed gy Notes Chloride [16887-00-6]^ 22 mg/L 1 2.2 5.0 0121014 EPA 300.0 10/21/20 14:24 LJI Sulfate as SO4 [14808-79-B]^ 99 mg/L 1 2.9 5.0 0121014 EPA 300.0 10/21/20 14:24 LJI Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 0J20015 iM 450052 D-2011 10/20/20 15:00 JOC Total Alkalinity as CaCO3 [471-34-1]^ 140 mg/L 1 14 15 0123015 EPA 310.2 10/23/20 12:55 JAH Total Dissolved Solids^ 350 mg/L 1 50 50 0120011 SM 254OC-2011 10/20/20 17:13 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 33 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW17S Lab Sample ID:CD16585-08 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 10:35 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 2.3 ug/L 1 0.80 2.0 0320037 EPA 8260D 10/20/20 15:24 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.2 1 5.00 104 % 75-125 OJ20037 EPA 6260D 1012012015:24 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 34 of 83 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW17D Lab Sample ID:CD16585-09 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 11:05 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analvte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 06:48 REF 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 0123011 EPA 8260D 10/24/20 06:48 REF 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 0123011 EPA 8260D 10/24/20 06:48 REF 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 0123011 EPA 8260D 10/24/20 06:48 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 0123011 EPA 8260D 10/24/20 06:48 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 0123011 EPA 8260D 10/24/20 06:48 REF QV-01 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 0123011 EPA 8260D 10/24/20 06:48 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 0123011 EPA 8260D 10/24/20 06:48 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 0123011 EPA 8260D 10/24/20 06:48 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 0123011 EPA 8260D 10/24/20 06:48 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 0123011 EPA 8260D 10/24/20 06:48 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 0123011 EPA 8260D 10/24/20 06:48 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 0123011 EPA 8260D 10/24/20 06:48 REF 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 0123011 EPA 8260D 10/24/20 06:48 REF 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 0123011 EPA 8260D 10/24/20 06:48 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 0123011 EPA 8260D 10/24/20 06:48 REF Acetone [67-64- 1]A 10 U ug/L 1 10 20 0123011 EPA 8260D 10/24/20 06:48 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 0123011 EPA 8260D 10/24/20 06:48 REF Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 0123011 EPA 8260D 10/24/20 06:48 REF Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Chlorobenzene[108-90-7]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 0123011 EPA 8260D 10/24/20 06:48 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 06:48 REF cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Ethylbenzene [500-41-4]A 0.13 U ug/L 1 0.13 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 0123011 EPA 8260D 10/24/20 06:48 REF Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 0123011 EPA 8260D 10/24/20 06:48 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 0123011 EPA 8260D 10/24/20 06:48 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 06:48 REF trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 0123011 EPA 8260D 10/24/20 06:48 REF Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 0123011 EPA 8260D 10/24/20 06:48 REF Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 0123011 EPA 8260D 10/24/20 06:48 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 35 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW17D Lab Sample ID:CD16585-09 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 11:05 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 0J23011 EPA 8260D 10/24/20 06:48 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 52 1 50.0 104 % 53-136 OJ23011 EPA 6260D 10124120 06:48 REF Dibromofluoromethane 59 1 50.0 118 % 67-129 OJ23011 EPA 6260D 10124120 06:48 REF Toluene-c48 53 1 50.0 107 % 59-134 OJ23011 EPA 6260D 10124120 06:48 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 0J21044 EPA 7470A 10/23/20 16:05 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 0J27036 EPA 6020B 11/05/20 00:21 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 0J21028 EPA 6010D 10/23/20 11:11 JDH Barium [7440-39-3]^ 33.4 ug/L 1 1.10 10.0 0121028 EPA 6010D 10/23/20 11:11 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 0J21028 EPA 6010D 10/23/20 11:11 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 0J21028 EPA 6010D 10/23/20 11:11 JDH Chromium [7440-47-3]^ 1.59 J ug/L 1 1.40 10.0 0121028 EPA 6010D 10/23/20 11:11 JDH Cobalt[7440-48-4]^ 1.48 J ug/L 1 1.40 10.0 0121028 EPA 6010D 10/23/20 11:11 JDH Copper[7440-50-8]^ 2.97 J ug/L 1 1.60 10.0 0121028 EPA 6010D 10/23/20 11:11 JDH Iron [7439-89-6]^ 2500 ug/L 1 22.0 50.0 0121028 EPA 6010D 10/23/20 11:11 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 0J21028 EPA 6010D 10/23/20 11:11 JDH Manganese [7439-96-5]^ 47.8 ug/L 1 1.50 10.0 0121028 EPA 6010D 10/23/20 11:11 JDH Nickel[7440-02-O]^ 2.20 U ug/L 1 2.20 10.0 0J21028 EPA 6010D 10/23/20 11:11 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 0J27036 EPA 6020B 11/05/20 00:21 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 0J21028 EPA 6010D 10/23/20 11:11 JDH Thallium [7440-28-O]^ 0.220 U ug/L 2 0.220 2.00 0J27036 EPA 6020B 11/05/20 00:21 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 11:11 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 0J21028 EPA 6010D 10/23/20 11:11 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 3.0 J mg/L 1 2.2 5.0 0121014 EPA 300.0 10/21/20 14:42 LJI Sulfate as SO4 [14808-79-B]^ 35 mg/L 1 2.9 5.0 0121014 EPA 300.0 10/21/20 14:42 LJI Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 0J20015 iM 450052 D-2011 10/20/20 15:00 JOC Total Alkalinity as CaCO3 [471-34-1]^ 120 mg/L 1 14 15 0120019 EPA 310.2 10/20/20 15:44 JAH Total Dissolved Solids^ 200 mg/L 1 50 50 0120011 SM 254OC-2011 10/20/20 17:13 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 36 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW17D Lab Sample ID:CD16585-09 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 11:05 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte KAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 6.8 ug/L 1 0.80 2.0 0320037 EPA 8260D 10/20/20 15:49 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.2 1 5.00 103 % 75-125 OJ20037 EPA 6260D 1012012015:49 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 37 of 83 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CD16585-10 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 14:05 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 07:18 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 0123011 EPA 8260D 10/24/20 07:18 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 0123011 EPA 8260D 10/24/20 07:18 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 0123011 EPA 8260D 10/24/20 07:18 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 0123011 EPA 8260D 10/24/20 07:18 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 0123011 EPA 8260D 10/24/20 07:18 REF QV-01 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 0123011 EPA 8260D 10/24/20 07:18 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 0123011 EPA 8260D 10/24/20 07:18 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 0123011 EPA 8260D 10/24/20 07:18 REF 1,2-Dichlorobenzene [95-50-1]^ 0.52 J ug/L 1 0.19 1.0 0123011 EPA 8260D 10/24/20 07:18 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 0123011 EPA 8260D 10/24/20 07:18 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 0123011 EPA 8260D 10/24/20 07:18 REF 1,4-Dichlorobenzene [306-46-7]^ 1.8 ug/L 1 0.19 1.0 0123011 EPA 8260D 10/24/20 07:18 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 0123011 EPA 8260D 10/24/20 07:18 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 0123011 EPA 8260D 10/24/20 07:18 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 0123011 EPA 8260D 10/24/20 07:18 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 0123011 EPA 8260D 10/24/20 07:18 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 0123011 EPA 8260D 10/24/20 07:18 REF Benzene [71-43-2]A 0.99 J ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 0123011 EPA 8260D 10/24/20 07:18 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Chlorobenzene [308-90-7]^ 0.88 J ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 0123011 EPA 8260D 10/24/20 07:18 REF cis-1,2-Dichloroethene [156-59-2]^ 3.8 ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 07:18 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 0123011 EPA 8260D 10/24/20 07:18 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 0123011 EPA 8260D 10/24/20 07:18 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 0123011 EPA 8260D 10/24/20 07:18 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 07:18 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 0123011 EPA 8260D 10/24/20 07:18 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 0123011 EPA 8260D 10/24/20 07:18 REF Vinyl chloride [75-01-4]^ 1.9 ug/L 1 0.32 1.0 0123011 EPA 8260D 10/24/20 07:18 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 38 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CD16585-10 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 14:05 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 0J23011 EPA 8260D 10/24/20 07:18 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 52 1 50.0 105 % 53-136 OJ23011 EPA 6260D 10124120 07:18 REF Dibromofluoromethane 55 1 50.0 110 % 67-129 OJ23011 EPA 6260D 10124120 07:18 REF Toluene-c48 54 1 50.0 107 % 59-134 OJ23011 EPA 6260D 10124120 07:18 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 0J21046 EPA 7470A 10/23/20 16:34 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-0]^ 0.740 U ug/L 2 0.740 2.00 0J27036 EPA 6020B 11/05/20 00:25 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 0J21028 EPA 6010D 10/23/20 11:18 JDH Barium [7440-39-3]^ 83.8 ug/L 1 1.10 10.0 0121028 EPA 6010D 10/23/20 11:18 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 0J21028 EPA 6010D 10/23/20 11:18 JDH Cadmium [7440-43-9]^ 1.26 ug/L 1 0.360 1.00 0121028 EPA 6010D 10/23/20 11:18 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 11:18 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 11:18 JDH Copper[7440-50-8]^ 1.99 J ug/L 1 1.60 10.0 0121028 EPA 6010D 10/23/20 11:18 JDH Iron [7439-89-6]^ 103000 ug/L 1 22.0 50.0 0121028 EPA 6010D 10/23/20 11:18 JDH Lead [7439-92-1]^ 7.49 J ug/L 1 3.10 10.0 0121028 EPA 6010D 10/23/20 11:18 JDH Manganese [7439-96-5]^ 227 ug/L 1 1.50 10.0 0121028 EPA 6010D 10/23/20 11:18 JDH Nickel[7440-02-O]^ 2.20 U ug/L 1 2.20 10.0 0J21028 EPA 6010D 10/23/20 11:18 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 0J27036 EPA 6020B 11/05/20 00:25 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 0J21028 EPA 6010D 10/23/20 11:18 JDH Thallium [7440-28-O]^ 0.220 U ug/L 2 0.220 2.00 0J27036 EPA 6020B 11/05/20 00:25 RLF Vanadium [7440-62-2]^ 2.34 J ug/L 1 1.40 10.0 0121028 EPA 6010D 10/23/20 11:18 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 0J21028 EPA 6010D 10/23/20 11:18 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed gy Notes Chloride [16887-00-6]^ 41 mg/L 1 2.2 5.0 0121014 EPA 300.0 10/21/20 15:35 UI Sulfate as SO4 [14808-79-B]^ 72 mg/L 1 2.9 5.0 0121014 EPA 300.0 10/21/20 15:35 UI Sulfide [18496-25-8]^ 0.042 J mg/L 1 0.010 0.10 0120015 iM 450052 D-2011 10/20/20 15:00 JOC Total Alkalinity as CaCO3 [471-34-1]^ 290 D mg/L 2 28 30 0120019 EPA 310.2 10/20/20 16:13 JAH Total Dissolved Solids^ 430 mg/L 1 50 50 0120011 SM 254OC-2011 10/20/20 17:13 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 39 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW18 Lab Sample ID:CD16585-10 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 14:05 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte KAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 10 ug/L 1 0.80 2.0 0320037 EPA 8260D 10/20/20 16:15 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.1 1 5.00 103 % 75-125 OJ20037 EPA 6260D 10120120 16:15 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 40 of 83 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CD16585-11 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 12:25 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 07:48 REF 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 0123011 EPA 8260D 10/24/20 07:48 REF 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 0123011 EPA 8260D 10/24/20 07:48 REF 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 0123011 EPA 8260D 10/24/20 07:48 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 0123011 EPA 8260D 10/24/20 07:48 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 0123011 EPA 8260D 10/24/20 07:48 REF QV-01 1,1-Dichloropropene [563-58-6]^ 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 07:48 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 0123011 EPA 8260D 10/24/20 07:48 REF 1,2,4-Trichlorobenzene [120-82-1]^ 0.14 U ug/L 1 0.14 1.0 0123011 EPA 8260D 10/24/20 07:48 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 0123011 EPA 8260D 10/24/20 07:48 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 0123011 EPA 8260D 10/24/20 07:48 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 0123011 EPA 8260D 10/24/20 07:48 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 0123011 EPA 8260D 10/24/20 07:48 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 0123011 EPA 8260D 10/24/20 07:48 REF 1,3-Dichlorobenzene [541-73-1]^ 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 07:48 REF 1,3-Dichloropropane [142-28-9]^ 0.16 U ug/L 1 0.16 1.0 0123011 EPA 8260D 10/24/20 07:48 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 0123011 EPA 8260D 10/24/20 07:48 REF 2,2-Dichloropropane [594-20-7]^ 0.28 U ug/L 1 0.28 1.0 0123011 EPA 8260D 10/24/20 07:48 REF 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 0123011 EPA 8260D 10/24/20 07:48 REF 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 0123011 EPA 8260D 10/24/20 07:48 REF 3-Chloropropene [107-05- 1]A 0.11 U ug/L 1 0.11 1.0 0123011 EPA 8260D 10/24/20 07:48 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 0123011 EPA 8260D 10/24/20 07:48 REF Acetone [67-64- 1]A 10 U ug/L 1 10 20 0123011 EPA 8260D 10/24/20 07:48 REF Acetonitrile [75-05-8]A 5.0 U ug/L 1 5.0 10 0123011 EPA 8260D 10/24/20 07:48 REF Acrolein [107-02-8]A 4.0 U ug/L 1 4.0 10 0123011 EPA 8260D 10/24/20 07:48 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 0123011 EPA 8260D 10/24/20 07:48 REF Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 07:48 REF Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 0123011 EPA 8260D 10/24/20 07:48 REF Bromodichloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 07:48 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 0123011 EPA 8260D 10/24/20 07:48 REF Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 0123011 EPA 8260D 10/24/20 07:48 REF Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 0123011 EPA 8260D 10/24/20 07:48 REF Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 07:48 REF Chlorobenzene[108-90-7]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 07:48 REF Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 0123011 EPA 8260D 10/24/20 07:48 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 0123011 EPA 8260D 10/24/20 07:48 REF Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 0123011 EPA 8260D 10/24/20 07:48 REF Chloroprene [126-99-8]A 0.64 U ug/L 1 0.64 1.0 0123011 EPA 8260D 10/24/20 07:48 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 07:48 REF cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 0123011 EPA 8260D 10/24/20 07:48 REF Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 07:48 REF Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 0123011 EPA 8260D 10/24/20 07:48 REF Dichlorodifluoromethane [75-71-8]A 0.20 U ug/L 1 0.20 1.0 0123011 EPA 8260D 10/24/20 07:48 REF Ethyl Methacrylate [97-63-2]^ 0.38 U ug/L 1 0.38 1.0 0123011 EPA 8260D 10/24/20 07:48 REF Ethylbenzene[100-41-4]A 0.13 U ug/L 1 0.13 1.0 0123011 EPA 8260D 10/24/20 07:48 REF Hexachlorobutadiene [87-68-3]A 0.22 U ug/L 1 0.22 1.0 0123011 EPA 8260D 10/24/20 07:48 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 0123011 EPA 8260D 10/24/20 07:48 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 41 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CD16585-11 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 12:25 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed AX Notes Isobutyl alcohol [78-83-1]^ 11 U ug/L 1 11 50 OJ23011 EPA 8260D 10/24/20 07:48 REF QL-02 Methacrylonitrile [126-98-7]^ 4.9 U ug/L 1 4.9 10 OJ23011 EPA 8260D 10/24/20 07:48 REF Methyl Methacrylate [80-62-6]^ 0.51 U ug/L 1 0.51 1.0 OJ23011 EPA 8260D 10/24/20 07:48 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 OJ23011 EPA 8260D 10/24/20 07:48 REF Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 OJ23011 EPA 8260D 10/24/20 07:48 REF Propionitrile [107-12-O]^ 5.0 U ug/L 1 5.0 10 OJ23011 EPA 8260D 10/24/20 07:48 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 OJ23011 EPA 8260D 10/24/20 07:48 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 OJ23011 EPA 8260D 10/24/20 07:48 REF Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 OJ23011 EPA 8260D 10/24/20 07:48 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 OJ23011 EPA 8260D 10/24/20 07:48 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 OJ23011 EPA 8260D 10/24/20 07:48 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 OJ23011 EPA 8260D 10/24/20 07:48 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 OJ23011 EPA 8260D 10/24/20 07:48 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 OJ23011 EPA 8260D 10/24/20 07:48 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 OJ23011 EPA 8260D 10/24/20 07:48 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 OJ23011 EPA 8260D 10/24/20 07:48 REF Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 OJ23011 EPA 8260D 10/24/20 07:48 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 OJ23011 EPA 8260D 10/24/20 07:48 REF Surrogates Results DF Spike LN % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 52 1 50.0 103 % 53-136 OJ23011 EPA 626OD 10124120 07:48 REF Dibromofluoromethane 57 1 50.0 114 % 67-129 OJ23011 EPA 626OD 10124120 07:48 REF Toluene-d8 55 1 50.0 110 % 59-134 OJ23011 EPA 626OD 10124120 07:48 REF Semivolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes 1,2,4,5-Tetrachlorobenzene [95-94-3]^ 3.4 U ug/L 1 3.4 10 OJ19001 EPA 8270E 1O/23/20 19:30 DFM 1,3,5-Trinitrobenzene [99-35-4]^ 3.0 U ug/L 1 3.0 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM 1,3-Dinitrobenzene [99-65-O]^ 2.5 U ug/L 1 2.5 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM 1,4-Naphthoquinone [130-15-4]^ 2.5 U ug/L 1 2.5 10 OJ19001 EPA 8270E 1O/23/20 19:30 DFM 1,4-Phenylenediamine [106-50-3]^ 4.0 U ug/L 1 4.0 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM 1-Naphthylamine [134-32-7]^ 2.2 U ug/L 1 2.2 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM 2,3,4,6-Tetrachlorophenol[58-90-2]^ 2.4 U ug/L 1 2.4 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM 2,4,5-Trichlorophenol[95-95-4]^ 2.5 U ug/L 1 2.5 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM 2,4,6-Trichlorophenol[88-06-2]^ 2.6 U ug/L 1 2.6 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM 2,4-Dichlorophenol[120-83-2]^ 2.6 U ug/L 1 2.6 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM 2,4-Di methyl phenol[105-67-9]^ 2.3 U ug/L 1 2.3 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM 2,4-Dinitrophenol[51-28-5]^ 2.6 U ug/L 1 2.6 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM 2,4-Dinitrotoluene [121-14-2]^ 2.6 U ug/L 1 2.6 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM 2,6-Dichlorophenol[87-65-O]^ 2.0 U ug/L 1 2.0 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM 2,6-Dinitrotoluene [606-20-2]^ 2.5 U ug/L 1 2.5 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM 2-Acetylaminofluorene [53-96-3]^ 3.1 U ug/L 1 3.1 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM 2-Chloronaphthalene [91-58-7]^ 2.8 U ug/L 1 2.8 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM 2-Chlorophenol[95-57-8]^ 2.2 U ug/L 1 2.2 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM 2-Methyl-4,6-dinitrophenol[534-52-1]^ 3.3 U ug/L 1 3.3 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM 2- Methyl naphthalene [91-57-6]^ 2.8 U ug/L 1 2.8 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 42 of 83 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CD16585-11 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 12:25 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Semivolatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte FCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed By Notes 2-Methylphenol[95-48-7]A 2.0 U ug/L 1 2.0 10 O119001 EPA 8270E 10/23/20 19:30 DFM 2-Naphthylamine [91-59-8]A 3.0 U ug/L 1 3.0 10 O119001 EPA 8270E 10/23/20 19:30 DFM 2-Nitroaniline [88-74-4]A 2.5 U ug/L 1 2.5 10 O119001 EPA 8270E 10/23/20 19:30 DFM 2-Nitrophenol[88-75-5]A 1.1 U ug/L 1 1.1 10 O119001 EPA 8270E 10/23/20 19:30 DFM 3 & 4-Methylphenol[108-39-4/106-44-5]A 2.1 U ug/L 1 2.1 10 O119001 EPA 8270E 10/23/20 19:30 DFM 3,3'-Dichlorobenzidine [91-94-1]A 3.5 U ug/L 1 3.5 10 O119001 EPA 8270E 10/23/20 19:30 DFM 3,3'-Dimethylbenzidine [119-93-71A 2.2 U ug/L 1 2.2 10 O119001 EPA 8270E 10/23/20 19:30 DFM 3-Methylcholanthrene [56-49-5]A 1.3 U ug/L 1 1.3 10 O119001 EPA 8270E 10/23/20 19:30 DFM 3-Nitroaniline [99-09-2]A 2.6 U ug/L 1 2.6 10 O119001 EPA 8270E 10/23/20 19:30 DFM 4-Aminobiphenyl [92-67- 1]A 3.5 U ug/L 1 3.5 10 O119001 EPA 8270E 10/23/20 19:30 DFM 4-Bromophenyl-phenylether[101-55-3]A 2.4 U ug/L 1 2.4 10 O119001 EPA 8270E 10/23/20 19:30 DFM 4-Chloro-3-methylphenol[59-50-7]A 2.4 U ug/L 1 2.4 10 O119001 EPA 8270E 10/23/20 19:30 DFM 4-Chloroaniline [106-47-8]A 2.0 U ug/L 1 2.0 10 O119001 EPA 8270E 10/23/20 19:30 DFM 4-Chlorophenyl-phenylether[7005-72-3]A 2.6 U ug/L 1 2.6 10 O119001 EPA 8270E 10/23/20 19:30 DFM 4-Nitroaniline [100-01-6]A 3.2 U ug/L 1 3.2 10 O119001 EPA 8270E 10/23/20 19:30 DFM 4-Nitrophenol[100-02-7]A 2.8 U ug/L 1 2.8 10 O119001 EPA 8270E 10/23/20 19:30 DFM 5-Nitro-o-toluidine [99-55-8]A 3.2 U ug/L 1 3.2 10 O119001 EPA 8270E 10/23/20 19:30 DFM 7,12-Dimethylbenz(a)anthracene 1.4 U ug/L 1 1.4 10 O119001 EPA 8270E 10/23/20 19:30 DFM [57-97-6]A a,a-Dimethylphenethylamine [122-09-8]A 3.5 U ug/L 1 3.5 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Acenaphthene [83-32-9]A 2.7 U ug/L 1 2.7 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Acenaphthylene [208-96-8]A 2.6 U ug/L 1 2.6 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Acetophenone [98-86-2]A 2.0 U ug/L 1 2.0 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Anthracene [120-12-7]A 2.4 U ug/L 1 2.4 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Benzo(a)anthracene [56-55-3]A 2.4 U ug/L 1 2.4 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Benzo(a)pyrene [50-32-8]A 2.2 U ug/L 1 2.2 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Benzo(b)fluoranthene [205-99-2]A 2.8 U ug/L 1 2.8 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Benzo(g,hJ)perylene [191-24-2]A 2.4 U ug/L 1 2.4 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Benzo(k)fluoranthene [207-08-9]A 2.4 U ug/L 1 2.4 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Benzyl alcohol [100-51-6]A 2.4 U ug/L 1 2.4 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Bis(2-chloroethoxy)methane [111-91-1]A 2.4 U ug/L 1 2.4 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Bis(2-chloroethyl)ether [111-44-4]A 2.6 U ug/L 1 2.6 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Bis(2-chloroisopropyl)ether [108-60-1]A 2.5 U ug/L 1 2.5 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Bis(2-ethylhexyl)phthalate [117-81-7]A 1.9 U ug/L 1 1.9 5.0 OJ19001 EPA 8270E 10/23/20 19:30 DFM Butylbenzylphthalate [85-68-7]A 3.8 U ug/L 1 3.8 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Chlorobenzilate [510-15-6]A 2.4 U ug/L 1 2.4 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Chrysene [218-01-9]A 2.2 U ug/L 1 2.2 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Diallate [2303-16-4]A 1.9 U ug/L 1 1.9 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Dibenzo(a,h)anthracene [53-70-3]A 2.3 U ug/L 1 2.3 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Dibenzofuran [132-64-9]A 2.6 U ug/L 1 2.6 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Diethylphthalate [84-66-2]A 2.4 U ug/L 1 2.4 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Dimethoate [60-51-5]A 2.3 U ug/L 1 2.3 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Dimethylphthalate [131-11-3]A 2.5 U ug/L 1 2.5 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Di-n-butylphthalate [84-74-2]A 2.8 U ug/L 1 2.8 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Di-n-octylphthalate [117-84-0]A 3.1 U ug/L 1 3.1 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Disulfoton [298-04-4]A 2.0 U ug/L 1 2.0 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Ethyl methanesulfonate [62-50-O]A 2.2 U ug/L 1 2.2 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 43 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CD16585-11 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 12:25 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Semivolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Famphur[52-85-7]^ 2.7 U ug/L 1 2.7 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Fluoranthene [206-44-0]^ 3.1 U ug/L 1 3.1 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Fluorene [86-73-7]^ 2.5 U ug/L 1 2.5 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Hexachlorobenzene [118-74-1]1 2.3 U ug/L 1 2.3 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Hexachlorobutadiene [87-68-3]^ 2.8 U ug/L 1 2.8 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Hexachlorocyclopentadiene [77-47-4]^ 2.7 U ug/L 1 2.7 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Hexachloroethane [67-72-1]^ 2.6 U ug/L 1 2.6 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Hexachloropropene [1888-71-7]^ 6.8 U ug/L 1 6.8 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Indeno(1,2,3-cd)pyrene [193-39-5]^ 2.2 U ug/L 1 2.2 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Isodrin [465-73-6]^ 1.5 U ug/L 1 1.5 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Isophorone [78-59-1]^ 2.5 U ug/L 1 2.5 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Isosafrole [120-58-1]^ 2.2 U ug/L 1 2.2 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Kepone [143-50-O]^ 7.2 U ug/L 1 7.2 20 OJ19001 EPA 8270E 10/23/20 19:30 DFM Methapyrilene [91-80-5]^ 4.8 U ug/L 1 4.8 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Methyl Methanesulfonate [66-27-3]^ 2.2 U ug/L 1 2.2 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Methyl parathion [298-00-0]^ 2.5 U ug/L 1 2.5 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Nitrobenzene [98-95-3]^ 2.5 U ug/L 1 2.5 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM N-Nitrosodiethylamine [55-18-5]^ 2.1 U ug/L 1 2.1 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM N-Nitrosodimethylamine [62-75-9]^ 1.9 U ug/L 1 1.9 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM N-Nitrosodi-n-butylamine [924-16-3]^ 2.0 U ug/L 1 2.0 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM N-Nitroso-di-n-propylamine [621-64-7]^ 2.3 U ug/L 1 2.3 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM N-nitrosodiphenylamine/Diphenylamine 2.5 U ug/L 1 2.5 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM [86-30-6/122-39-4]^ N-Nitrosomethylethylamine [10595-95-6]^ 1.9 U ug/L 1 1.9 10 0J19001 EPA 8270E 10/23/20 19:30 DFM N-Nitrosopiperidine [100-75-4]^ 2.1 U ug/L 1 2.1 10 0J19001 EPA 8270E 10/23/20 19:30 DFM N-Nitrosopyrrolidine [930-55-2]^ 1.9 U ug/L 1 1.9 10 0J19001 EPA 8270E 10/23/20 19:30 DFM 0,0,0-Triethylphosphorothioate 2.2 U ug/L 1 2.2 10 0J19001 EPA 8270E 10/23/20 19:30 DFM [126-68-1]^ o-Toluidine [95-53-4]^ 1.6 U ug/L 1 1.6 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Parathion [56-38-2]^ 1.7 U ug/L 1 1.7 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM p-Dimethylaminoazobenzene [60-11-7]^ 2.6 U ug/L 1 2.6 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Pentachlorobenzene [608-93-5]^ 2.7 U ug/L 1 2.7 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Pentachloronitrobenzene [82-68-8]^ 1.9 U ug/L 1 1.9 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Phenacetin [62-44-2]^ 2.7 U ug/L 1 2.7 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Phenanthrene [85-01-8]^ 2.6 U ug/L 1 2.6 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Phenol[108-95-2]^ 1.7 U ug/L 1 1.7 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Phorate [298-02-2]^ 2.1 U ug/L 1 2.1 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Pronamide [23950-58-5]^ 1.7 U ug/L 1 1.7 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Pyrene [129-00-O]^ 3.5 U ug/L 1 3.5 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Safrole [94-59-7]^ 2.2 U ug/L 1 2.2 10 OJ19001 EPA 8270E 10/23/20 19:30 DFM Thionazin [297-97-2]^ 2.3 U ug/L 1 2.3 10 0J19001 EPA 8270E 10/23/20 19:30 DFM Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes 2,4,6-Tribromophenol 80 1 100 80 % 10-179 0J19001 EPA 8270E 10123120 1920 DFM 2-Fluorobiphenyl 47 1 50.0 93 % 10-149 0J19001 EPA 8270E 10123120 1920 DFM 2-Fluorophenol 53 1 100 53 % 10-110 0J19001 EPA 8270E 10123120 19:30 DFM Nitrobenzene-d5 37 1 50.0 74 % 10-149 0J19001 EPA 8270E 10123120 19:30 DFM Phenol-d5 42 1 100 42 % 10-88 0J19001 EPA 8270E 10123120 19:30 DFM FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 44 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CD16585-11 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 12:25 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Semivolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Terphenyl-d14 48 1 50.0 96 % 10-166 OJi9001 EPA 8270E 10123120 1930 DFM Organochlorine Pesticides by GC ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed gy Notes 4,4'-DDD [72-54-8]^ 0.044 U ug/L 1 0.044 0.050 OJ20002 EPA 8081B 10/21/20 13:20 LSK 4,4'-DDE [72-55-9]^ 0.048 U ug/L 1 0.048 0.050 OJ20002 EPA 8081B 10/21/20 13:20 LSK 4,4'-DDT [50-29-3]^ 0.049 U ug/L 1 0.049 0.050 OJ20002 EPA 8081B 10/21/20 13:20 LSK Aldrin [309-00-2]^ 0.041 U ug/L 1 0.041 0.050 OJ20002 EPA 8081B 10/21/20 13:20 LSK alpha-BHC [319-84-6]^ 0.036 U ug/L 1 0.036 0.050 OJ20002 EPA 8081B 10/21/20 13:20 LSK beta-BHC [319-85-7]^ 0.041 U ug/L 1 0.041 0.050 OJ20002 EPA 8081B 10/21/20 13:20 LSK Chlordane (tech)[12789-03-6]^ 0.37 U ug/L 1 0.37 0.50 OJ20002 EPA 8081B 10/21/20 13:20 LSK Chlordane -alpha [5103-71-9]^ 0.048 U ug/L 1 0.048 0.050 OJ20002 EPA 8081B 10/21/20 13:20 LSK Chlordane -gamma [5103-74-2]^ 0.042 U ug/L 1 0.042 0.050 OJ20002 EPA 8081B 10/21/20 13:20 LSK delta-BHC [319-86-8]^ 0.048 U ug/L 1 0.048 0.050 OJ20002 EPA 8081B 10/21/20 13:20 LSK Dieldrin [60-57-1]^ 0.045 U ug/L 1 0.045 0.050 OJ20002 EPA 8081B 10/21/20 13:20 LSK Endosulfan I[959-98-8]^ 0.045 U ug/L 1 0.045 0.050 OJ20002 EPA 8081B 10/21/20 13:20 LSK Endosulfan II[33213-65-9]^ 0.038 U ug/L 1 0.038 0.050 OJ20002 EPA 8081B 10/21/20 13:20 LSK Endosulfan sulfate [1031-07-8]^ 0.032 U ug/L 1 0.032 0.050 OJ20002 EPA 8081B 10/21/20 13:20 LSK Endrin [72-20-8]^ 0.041 U ug/L 1 0.041 0.050 OJ20002 EPA 8081B 10/21/20 13:20 LSK Endrin aldehyde [7421-93-4]^ 0.049 U ug/L 1 0.049 0.050 OJ20002 EPA 8081B 10/21/20 13:20 LSK gamma-BHC [58-89-9]^ 0.034 U ug/L 1 0.034 0.050 OJ20002 EPA 8081B 10/21/20 13:20 LSK Heptachlor[76-44-8]^ 0.047 U ug/L 1 0.047 0.050 OJ20002 EPA 8081B 10/21/20 13:20 LSK Heptachlor epoxide [1024-57-3]^ 0.037 U ug/L 1 0.037 0.050 OJ20002 EPA 8081B 10/21/20 13:20 LSK Methoxychlor[72-43-5]^ 0.048 U ug/L 1 0.048 0.050 OJ20002 EPA 8081B 10/21/20 13:20 LSK Toxaphene[8001-35-2]^ 0.28 U ug/L 1 0.28 1.0 OJ20002 EPA 8081B 10/21/20 13:20 LSK Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes 2,4,5,6-TCMX 0.66 1 1.00 66 % 10-139 OJ20002 EPA 8081E 1012112013:20 LSK Decachlorobiphenyl 1.1 1 1.00 112 % 10-122 OJ20002 EPA 8081E 1012112013:20 LSK Polychlorinated Biphenyls by GC ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes PCB-1016/1242 [12674-11-2/53469-21-9]^ 0.48 U ug/L 1 0.48 0.50 OJ20003 EPA 8082A 10/21/20 13:20 LSK PCB-1221[11104-28-2]^ 0.43 U ug/L 1 0.43 0.50 OJ20003 EPA 8082A 10/21/20 13:20 LSK PCB-1232 [11141-16-5]^ 0.50 U ug/L 1 0.50 0.50 OJ20003 EPA 8082A 10/21/20 13:20 LSK PCB-1248[12672-29-6]^ 0.45 U ug/L 1 0.45 0.50 OJ20003 EPA 8082A 10/21/20 13:20 LSK PCB-1254[11097-69-1]^ 0.43 U ug/L 1 0.43 0.50 OJ20003 EPA 8082A 10/21/20 13:20 LSK PCB-1260[11096-82-5]^ 0.47 U ug/L 1 0.47 0.50 OJ20003 EPA 8082A 10/21/20 13:20 LSK Surrogates 2,4,5,E-TCMX Decachlorobiphenyl Results DF Spike L v/ % Rec % Rec Limits Batch Method 0.93 1 1.00 93 % 10-126 OJ20003 EPA 6062A 1.2 1 1.00 118 % 10-129 OJ20003 EPA 6062A Ana/vzed By Notes 1012112013:20 L5K 1012112013:20 L5K FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 45 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CD16585-11 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 12:25 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 OJ21046 EPA 7470A 10/23/20 16:36 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Antimony [7440-36-O]^ 0.740 U ug/L 2 0.740 2.00 OJ27036 EPA 6020B 11/05/20 00:30 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 OJ21028 EPA 6010D 10/23/20 11:21 JDH Barium [7440-39-3]^ 59.5 ug/L 1 1.10 10.0 0321028 EPA 6010D 10/23/20 11:21 JDH Beryllium [7440-41-7]1 0.160 U ug/L 1 0.160 1.00 OJ21028 EPA 6010D 10/23/20 11:21 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 OJ21028 EPA 6010D 10/23/20 11:21 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 OJ21028 EPA 6010D 10/23/20 11:21 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 OJ21028 EPA 6010D 10/23/20 11:21 JDH Copper[7440-50-8]^ 2.03 J ug/L 1 1.60 10.0 0321028 EPA 6010D 10/23/20 11:21 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 OJ21028 EPA 6010D 10/23/20 11:21 JDH Nickel[7440-02-O]^ 2.20 U ug/L 1 2.20 10.0 OJ21028 EPA 6010D 10/23/20 11:21 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 OJ27036 EPA 6020B 11/05/20 00:30 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 OJ21028 EPA 6010D 10/23/20 11:21 JDH Thallium [7440-28-0]^ 0.220 U ug/L 2 0.220 2.00 OJ27036 EPA 6020B 11/05/20 00:30 RLF Tin [7440-31-5]^ 2.90 U ug/L 1 2.90 10.0 OJ21028 EPA 6010D 10/23/20 11:21 JDH Vanadium [7440-62-2]1 1.40 U ug/L 1 1.40 10.0 OJ21028 EPA 6010D 10/23/20 11:21 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 OJ21028 EPA 6010D 10/23/20 11:21 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 14 mg/L 1 2.2 5.0 0321014 EPA 300.0 10/21/20 15:53 LII Cyanide (total)[57-12-5]^ 0.0049 U mg/L 1 0.0049 0.010 OJ21029 EPA 9014 10/23/20 10:11 JAH Sulfate as SO4 [14808-79-8]^ 12 mg/L 1 2.9 5.0 0321014 EPA 300.0 10/21/20 15:53 LII Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 OJ20015 iM 450OS2 D-2011 10/20/20 15:00 JOC Total Alkalinity as CaCO3 [471-34-1]^ 95 mg/L 1 14 15 0320019 EPA 310.2 10/20/20 15:53 JAH Total Dissolved Solids^ 160 mg/L 1 50 50 0320011 SM 2540C-2011 10/20/20 17:13 DMJ Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 2.8 ug/L 1 0.80 2.0 0320037 EPA 8260D 10/20/20 16:40 KKW Surrogates Results DF Spike LN % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-c48 5.2 1 5.00 104 % 75-125 OJ20037 EPA 6260D 10120120 16:40 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 46 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW19 Lab Sample ID:CD16585-11 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/13/20 12:25 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Chlorinated Herbicides by GC A - ENCO Orlando certified analyte [NC 424] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 2,4,5-T [93-76-5]^ 0.28 U ug/L 1 0.28 0.50 OJ20036 EPA 8151A 10/22/20 21:38 FCV 2,4,5-TP (Silvex) [93-72-1]^ 0.44 U ug/L 1 0.44 0.50 OJ20036 EPA 8151A 10/22/20 21:38 FCV 2,4-D [94-75-7]^ 0.27 U ug/L 1 0.27 0.50 OJ20036 EPA 8151A 10/22/20 21:38 FCV Dinoseb [88-85-7]^ 0.32 U ug/L 1 0.32 0.50 OJ20036 EPA 8151A 10/22/20 21:38 FCV Pentachlorophenol[87-86-5]^ 0.19 U ug/L 1 0.19 0.50 OJ20036 EPA 8151A 10/22/20 21:38 FCV Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 2, 4-DCAA 2,4 1 2.00 119 % 37-134 OJ20036 EPA 6151A 10122120 21:38 FCV FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 47 of 83 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-FIELDBLANK Lab Sample ID:CD16585-12 Received: 10/15/20 08:19 Matrix: Water Sampled:10/14/20 07:45 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 06:39 REF 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 0123024 EPA 8260D 10/26/20 06:39 REF 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 0123024 EPA 8260D 10/26/20 06:39 REF 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 06:39 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 06:39 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 06:39 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 06:39 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 0123024 EPA 8260D 10/26/20 06:39 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 0123024 EPA 8260D 10/26/20 06:39 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 0123024 EPA 8260D 10/26/20 06:39 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 06:39 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 0123024 EPA 8260D 10/26/20 06:39 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 0123024 EPA 8260D 10/26/20 06:39 REF 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 0123024 EPA 8260D 10/26/20 06:39 REF 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 0123024 EPA 8260D 10/26/20 06:39 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 0123024 EPA 8260D 10/26/20 06:39 REF Acetone [67-64- 1]A 10 U ug/L 1 10 20 0123024 EPA 8260D 10/26/20 06:39 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 0123024 EPA 8260D 10/26/20 06:39 REF Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 0123024 EPA 8260D 10/26/20 06:39 REF QV-01 Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 0123024 EPA 8260D 10/26/20 06:39 REF Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Chlorobenzene[108-90-7]A 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 06:39 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 06:39 REF cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Ethylbenzene[100-41-4]A 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 0123024 EPA 8260D 10/26/20 06:39 REF Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 06:39 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 06:39 REF trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 06:39 REF trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 0123024 EPA 8260D 10/26/20 06:39 REF Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 0123024 EPA 8260D 10/26/20 06:39 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 48 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-FIELDBLANK Lab Sample ID:CD16585-12 Received: 10/15/20 08:19 Matrix: Water Sampled:10/14/20 07:45 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 0J23024 EPA 8260D 10/26/20 06:39 REF Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 0J23024 EPA 8260D 10/26/20 06:39 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 43 1 50.0 86 % 53-136 OJ23024 EPA 6260D 10126120 06:39 REF Dibromofluoromethane 49 1 50.0 97 % 67-129 OJ23024 EPA 6260D 10126120 06:39 REF Toluene-d8 49 1 50.0 98 % 59-134 OJ23024 EPA 8260D 10126120 0639 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 0J21046 EPA 7470A 10/23/20 16:39 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Antimony [7440-36-O]^ 0.740 U ug/L 2 0.740 2.00 0J27036 EPA 6020B 11/05/20 00:47 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 0J21028 EPA 6010D 10/23/20 11:23 JDH Barium [7440-39-3]^ 1.10 U ug/L 1 1.10 10.0 0J21028 EPA 6010D 10/23/20 11:23 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 0J21028 EPA 6010D 10/23/20 11:23 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 0J21028 EPA 6010D 10/23/20 11:23 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 11:23 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 11:23 JDH Copper[7440-50-8]^ 1.60 U ug/L 1 1.60 10.0 0J21028 EPA 6010D 10/23/20 11:23 JDH Iron [7439-89-6]^ 22.0 U ug/L 1 22.0 50.0 0J21028 EPA 6010D 10/23/20 11:23 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 0J21028 EPA 6010D 10/23/20 11:23 JDH Manganese [7439-96-5]^ 1.50 U ug/L 1 1.50 10.0 0J21028 EPA 6010D 10/23/20 11:23 JDH Nickel[7440-02-O]^ 2.20 U ug/L 1 2.20 10.0 0J21028 EPA 6010D 10/23/20 11:23 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 0J27036 EPA 6020B 11/05/20 00:47 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 0J21028 EPA 6010D 10/23/20 11:23 JDH Thallium [7440-28-O]^ 0.220 U ug/L 2 0.220 2.00 0J27036 EPA 6020B 11/05/20 00:47 RLF Vanadium [7440-62-2]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 11:23 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 0J21028 EPA 6010D 10/23/20 11:23 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 2.2 U mg/L 1 2.2 5.0 0J21014 EPA 300.0 10/21/20 16:10 LJI Sulfate as SO4 [14808-79-8]^ 2.9 U mg/L 1 2.9 5.0 0J21014 EPA 300.0 10/21/20 16:10 LJI Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 0J20017 iM 450052 D-2011 10/20/20 18:26 JOC Total Alkalinity as CaCO3 [471-34-1]^ 14 U mg/L 1 14 15 0J20019 EPA 310.2 10/20/20 15:54 JAH Total Dissolved Solids^ 50 U mg/L 1 50 50 0J20011 SM 254OC-2011 10/20/20 17:13 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 49 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-FIELDBLANK Lab Sample ID:CD16585-12 Received: 10/15/20 08:19 Matrix: Water Sampled:10/14/20 07:45 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte KAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 OJ20037 EPA 8260D 10/20/20 17:05 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.1 1 5.00 103 % 75-125 OJ20037 EPA 6260D 10120120 17:05 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 50 of 83 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-DUPLICATE Lab Sample ID:CD16585-13 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 07:00 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 07:07 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 0123024 EPA 8260D 10/26/20 07:07 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 0123024 EPA 8260D 10/26/20 07:07 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 07:07 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 07:07 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 07:07 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 07:07 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 0123024 EPA 8260D 10/26/20 07:07 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 0123024 EPA 8260D 10/26/20 07:07 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 0123024 EPA 8260D 10/26/20 07:07 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 07:07 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 0123024 EPA 8260D 10/26/20 07:07 REF 1,4-Dichlorobenzene [306-46-7]^ 0.67 J ug/L 1 0.19 1.0 0123024 EPA 8260D 10/26/20 07:07 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 0123024 EPA 8260D 10/26/20 07:07 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 0123024 EPA 8260D 10/26/20 07:07 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 0123024 EPA 8260D 10/26/20 07:07 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 0123024 EPA 8260D 10/26/20 07:07 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 0123024 EPA 8260D 10/26/20 07:07 REF Benzene [71-43-2]A 1.2 ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 0123024 EPA 8260D 10/26/20 07:07 REF QV-01 Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 0123024 EPA 8260D 10/26/20 07:07 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Chlorobenzene [308-90-7]A 0.55 J ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 07:07 REF cis-1,2-Dichloroethene [156-59-2]A 1.6 ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 07:07 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Ethylbenzene [500-41-4]^ 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 0123024 EPA 8260D 10/26/20 07:07 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 07:07 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 07:07 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 07:07 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 0123024 EPA 8260D 10/26/20 07:07 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 51 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-DUPLICATE Lab Sample ID:CD16585-13 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 07:00 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.97 J ug/L 1 0.32 1.0 0123024 EPA 8260D 10/26/20 07:07 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 0J23024 EPA 8260D 10/26/20 07:07 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 43 1 50.0 87 % 53-136 OJ23024 EPA 6260D 10126120 07:07 REF Dibromofluoromethane 49 1 50.0 99 % 67-129 OJ23024 EPA 6260D 10126120 07:07 REF Toluene-d8 51 1 50.0 102 % 59-134 OJ23024 EPA 6260D 10126120 07:07 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 0J21046 EPA 7470A 10/23/20 16:13 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Antimony [7440-36-O]^ 0.740 U ug/L 2 0.740 2.00 0J27036 EPA 6020B 11/05/20 00:51 RLF Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 0J21028 EPA 6010D 10/23/20 11:25 JDH Barium [7440-39-3]^ 26.9 ug/L 1 1.10 10.0 0121028 EPA 6010D 10/23/20 11:25 JDH Beryllium [7440-41-7]^ 0.160 U ug/L 1 0.160 1.00 0J21028 EPA 6010D 10/23/20 11:25 JDH Cadmium [7440-43-9]^ 2.16 ug/L 1 0.360 1.00 0121028 EPA 6010D 10/23/20 11:25 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 11:25 JDH Cobalt[7440-48-4]^ 1.40 U ug/L 1 1.40 10.0 0J21028 EPA 6010D 10/23/20 11:25 JDH Copper[7440-50-8]^ 3.60 J ug/L 1 1.60 10.0 0121028 EPA 6010D 10/23/20 11:25 JDH Iron [7439-89-6]^ 123000 ug/L 1 22.0 50.0 0121028 EPA 6010D 10/23/20 11:25 JDH Lead [7439-92-1]^ 10.1 ug/L 1 3.10 10.0 0121028 EPA 6010D 10/23/20 11:25 JDH Manganese [7439-96-5]^ 104 ug/L 1 1.50 10.0 0121028 EPA 6010D 10/23/20 11:25 JDH Nickel[7440-02-O]^ 2.20 U ug/L 1 2.20 10.0 0J21028 EPA 6010D 10/23/20 11:25 JDH Selenium [7782-49-2]^ 1.82 U ug/L 2 1.82 2.00 0J27036 EPA 6020B 11/05/20 00:51 RLF Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 0J21028 EPA 6010D 10/23/20 11:25 JDH Thallium [7440-28-O]^ 0.220 U ug/L 2 0.220 2.00 0J27036 EPA 6020B 11/05/20 00:51 RLF Vanadium [7440-62-2]^ 4.97 J ug/L 1 1.40 10.0 0121028 EPA 6010D 10/23/20 11:25 JDH Zinc[7440-66-6]^ 4.40 U ug/L 1 4.40 10.0 0J21028 EPA 6010D 10/23/20 11:25 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 2.9 J mg/L 1 2.2 5.0 0121014 EPA 300.0 10/21/20 16:28 LJI Sulfate as SO4 [14808-79-B]^ 7.3 mg/L 1 2.9 5.0 0121014 EPA 300.0 10/21/20 16:28 LJI Sulfide [18496-25-8]^ 0.016 J mg/L 1 0.010 0.10 0120017 iM 450052 D-2011 10/20/20 18:26 JOC Total Alkalinity as CaCO3 [471-34-1]^ 110 mg/L 1 14 15 0120019 EPA 310.2 10/20/20 15:55 JAH Total Dissolved Solids^ 98 mg/L 1 50 50 0120011 SM 254OC-2011 10/20/20 17:13 DMJ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 52 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-DUPLICATE Lab Sample ID:CD16585-13 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 07:00 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed py Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 OJ20037 EPA 8260D 10/20/20 17:30 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.4 1 5.00 109 % 75-125 OJ20037 EPA 626OD 10120120 17:30 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 53 of 83 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-TRIPBLANK Lab Sample ID:CD16585-14 Received: 10/15/20 08:19 Matrix: Water Sampled:10/13/20 10:35 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 08:18 REF 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 0123011 EPA 8260D 10/24/20 08:18 REF 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 0123011 EPA 8260D 10/24/20 08:18 REF 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 0123011 EPA 8260D 10/24/20 08:18 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 0123011 EPA 8260D 10/24/20 08:18 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 0123011 EPA 8260D 10/24/20 08:18 REF QV-01 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 0123011 EPA 8260D 10/24/20 08:18 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 0123011 EPA 8260D 10/24/20 08:18 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 0123011 EPA 8260D 10/24/20 08:18 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 0123011 EPA 8260D 10/24/20 08:18 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 0123011 EPA 8260D 10/24/20 08:18 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 0123011 EPA 8260D 10/24/20 08:18 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 0123011 EPA 8260D 10/24/20 08:18 REF 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 0123011 EPA 8260D 10/24/20 08:18 REF 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 0123011 EPA 8260D 10/24/20 08:18 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 0123011 EPA 8260D 10/24/20 08:18 REF Acetone [67-64-1]A 10 U ug/L 1 10 20 0123011 EPA 8260D 10/24/20 08:18 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 0123011 EPA 8260D 10/24/20 08:18 REF Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 0123011 EPA 8260D 10/24/20 08:18 REF Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Chlorobenzene [108-90-7]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 0123011 EPA 8260D 10/24/20 08:18 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 08:18 REF cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Ethylbenzene [500-41-4]A 0.13 U ug/L 1 0.13 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 0123011 EPA 8260D 10/24/20 08:18 REF Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 0123011 EPA 8260D 10/24/20 08:18 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 0123011 EPA 8260D 10/24/20 08:18 REF trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 08:18 REF trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 0123011 EPA 8260D 10/24/20 08:18 REF Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 0123011 EPA 8260D 10/24/20 08:18 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 54 of 83 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-TRIPBLANK Lab Sample ID:CD16585-14 Received: 10/15/20 08:19 Matrix: Water Sampled:10/13/20 10:35 Work Order: CD16585 Project: Moore County Active C & D LF Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 OJ23011 EPA 8260D 10/24/20 08:18 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 OJ23011 EPA 8260D 10/24/20 08:18 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 52 1 50.0 105 % 53-136 OJ23011 EPA 626OD 10124120 06:16 REF Dibromofluoromethane 57 1 50.0 114 % 67-129 OJ23011 EPA 626OD 10124120 06:16 REF Toluene-d8 55 1 50.0 110 % 59-134 OJ23011 EPA 626OD 10124120 06:16 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 OJ20037 EPA 8260D 1O/20/20 17:56 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.4 1 5.00 108 % 75-125 OJ20037 EPA 826OD 10120120 17:56 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 55 of 83 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch OJ23010 -EPA 5030B MS Blank (0323010-BLK1) Prepared: 10/23/2020 10:16 Analyzed: 10/23/2020 13:18 Analvte Result Flaq POL Units 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Naphthalene 0.11 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Tetrahydrofuran 0.53 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 56 of 83 QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch OJ23010 - EPA 5O3OB MS - Continued (� �Eo www.encolabs.com Blank (0323010-BLK1) Continued Prepared: 10/23/2020 10:16 Analyzed: 10/23/2020 13:18 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 54 ug/L 50.0 109 53-136 Dibromofluoromethane 50 ug/L 50.0 99 67-129 Toluene-d8 56 ug/L 50.0 111 59-134 LCS (0323010-BS1) Prepared: 10/23/2020 10:16 Analyzed: 10/23/2020 11:18 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 23 1.0 ug/L 20.0 116 75-133 Benzene 19 1.0 ug/L 20.0 95 80-134 Chlorobenzene 20 1.0 ug/L 20.0 101 80-120 Toluene 20 1.0 ug/L 20.0 102 71-120 Trichloroethene 21 1.0 ug/L 20.0 104 74-120 Matrix Spike (OJ23030-MS1) Prepared: 10/23/2020 10:16 Analyzed: 10/23/2020 11:48 Source: CD17278-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 23 1.0 ug/L 20.0 0.21 U 114 75-133 Benzene 19 1.0 ug/L 20.0 0.15 U 95 80-134 Chlorobenzene 21 1.0 ug/L 20.0 0.17 U 104 80-120 Toluene 21 1.0 ug/L 20.0 0.14 U 104 71-120 Trichloroethene 20 1.0 ug/L 20.0 0.15 U 101 74-120 Matrix Spike Dup (OJ23030-MSD1) Prepared: 10/23/2020 10:16 Analyzed: 10/23/2020 12:18 Source: CD17278-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 22 1.0 ug/L 20.0 0.21 U 110 75-133 4 20 Benzene 17 1.0 ug/L 20.0 0.15 U 83 80-134 14 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 93 80-120 11 16 Toluene 19 1.0 ug/L 20.0 0.14 U 96 71-120 8 17 Trichloroethene 19 1.0 ug/L 20.0 0.15 U 94 74-120 7 22 Batch OJ23011 - EPA 5O3OB MS Blank (0323011-BLK1) Prepared: 10/23/2020 10:23 Analyzed: 10/24/2020 02:19 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,1-Dichloropropene 0.15 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2,4-Trichlorobenzene 0.14 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 57 of 83 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch OJ23011 - EPA 5030B MS - Continued Blank (0323011-BLK1) Continued Prepared: 10/23/2020 10:23 Analyzed: 10/24/2020 02:19 Analvte Result Flaq POL Units 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,3-Dichlorobenzene 0.15 U 1.0 ug/L 1,3-Dichloropropane 0.16 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2,2-Dichloropropane 0.28 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 3-Chloropropene 0.11 U 1.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acetonitrile 5.0 U 10 ug/L Acrolein 4.0 U 10 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L Chloroprene 0.64 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Dichlorodifluoromethane 0.20 U 1.0 ug/L Ethyl Methacrylate 0.38 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Hexachlorobutadiene 0.22 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Isobutyl alcohol 11 U 50 ug/L Methacrylonitrile 4.9 U 10 ug/L Methyl Methacrylate 0.51 U 1.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Naphthalene 0.11 U 1.0 ug/L Propionitrile 5.0 U 10 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Tetrahydrofuran 0.53 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 58 of 83 0Nk"q09 www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch OJ23011 - EPA 5030E MS - Continued Blank (0323011-BLK1) Continued Prepared: 10/23/2020 10:23 Analyzed: 10/24/2020 02:19 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromofluorobenzene 54 ug/L 50.0 107 53-136 Dibromofluoromethane 53 ug/L 50.0 107 67-129 Toluene-d8 54 ug/L 50.0 107 59-134 LCS (0123011-BS1) Prepared: 10/23/2020 10:23 Analyzed: 10/24/2020 00:19 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limi RPD Mina Notes 1,1-Dichloroethene 26 1.0 ug/L 20.0 130 75-133 Benzene 18 1.0 ug/L 20.0 90 80-134 Chlorobenzene 20 1.0 ug/L 20.0 98 80-120 Toluene 19 1.0 ug/L 20.0 97 71-120 Trichloroethene 20 1.0 ug/L 20.0 100 74-120 4-8romofluorobenzene 55 ug/L 50.0 110 53-136 Dibromofluoromethane 52 ug/L 50.0 104 67-129 Toluene-& 55 ug/L 50.0 110 59-134 Matrix Spike (0723011-MS1) Prepared: 10/23/2020 10:23 Analyzed: 10/24/2020 00:49 Source: CD17245-08 Spike Source %REC RPD Analvte Result Flaa Q Units Level Res 1 %REC Limits RPD Limit Notes 1,1-Dichloroethene 26 1.0 ug/L 20.0 0.21 U 131 75-133 Benzene 19 1.0 ug/L 20.0 0.15 U 94 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 96 80-120 Toluene 20 1.0 ug/L 20.0 0.14 U 100 71-120 Trichloroethene 23 1.0 ug/L 20.0 0.15 U 113 74-120 4-Bromofluorobenzene 57 ug/L 50.0 114 53-136 Dibromofluoromethane 51 ug/L 50.0 102 67-129 Toluene-d8 55 U91L 50.0 110 59-134 Matrix Spike Dup (0323011-MSD1) Prepared: 10/23/2020 10:23 Analyzed: 10/24/2020 01:19 Source: CD17245-08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Lima RPD Limit Notes 1,1-Dichloroethene 26 1.0 ug/L 20.0 0.21 U 129 75-133 1 20 Benzene 19 1.0 ug/L 20.0 0.15 U 93 80-134 0.6 17 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 100 80-120 4 16 Toluene 20 1.0 ug/L 20.0 0.14 U 99 71-120 1 17 Trichloroethene 20 1.0 ug/L 20.0 0.15 U 102 74-120 10 22 4-Bromofluorobenzene 55 ug/L 50.0 111 53-136 Dibromofluoromethane 51 ug/L 50.0 102 67-129 Toluene-& 55 ug/L 50.0 110 59-134 Batch OJ23024 - EPA 5030B MS FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 59 of 83 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch OJ23024 - EPA 5030B MS - Continued Blank (0323024-BLK1) Prepared: 10/23/2020 13:57 Analyzed: 10/26/2020 03:54 Analvte Result Flaq POL Units 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Naphthalene 0.11 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Tetrahydrofuran 0.53 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 60 of 83 QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch OJ23024 - EPA 5030B MS - Continued (� �Eo www.encolabs.com Blank (0323024-BLK1) Continued Prepared: 10/23/2020 13:57 Analyzed: 10/26/2020 03:54 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 44 u91L 50.0 67 53-136 Dibromofluoromethane 47 u91L 50.0 95 67-129 Toluene-d8 49 u91L 50.0 98 59-134 LCS (0323024-BS1) Prepared: 10/23/2020 13:57 Analyzed: 10/26/2020 02:03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 96 75-133 Benzene 19 1.0 ug/L 20.0 97 80-134 Chlorobenzene 19 1.0 ug/L 20.0 93 80-120 Toluene 18 1.0 ug/L 20.0 88 71-120 Trichloroethene 21 1.0 ug/L 20.0 106 74-120 Matrix Spike (0323024-MS1) Prepared: 10/23/2020 13:57 Analyzed: 10/26/2020 02:31 Source: CD17102-10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 22 1.0 ug/L 20.0 2.3 99 75-133 Benzene 19 1.0 ug/L 20.0 0.15 U 96 80-134 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 92 80-120 Toluene 17 1.0 ug/L 20.0 0.14 U 87 71-120 Trichloroethene 60 1.0 ug/L 20.0 41 95 74-120 Matrix Spike Dup (0323024-MSD1) Prepared: 10/23/2020 13:57 Analyzed: 10/26/2020 02:58 Source: CD17102-10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 23 1.0 ug/L 20.0 2.3 102 75-133 3 20 Benzene 20 1.0 ug/L 20.0 0.15 U 98 80-134 3 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 95 80-120 3 16 Toluene 18 1.0 ug/L 20.0 0.14 U 92 71-120 5 17 Trichloroethene 61 1.0 ug/L 20.0 41 103 74-120 3 22 Semivolatile Organic Compounds by GCMS - Quality Control Batch 0119001 - EPA 3510C MS Blank (0319001-BLK3) Prepared: 10/19/2020 07:16 Analyzed: 10/22/2020 13:52 Analvte Result Flaq POL Units 1,2,4,5-Tetrachlorobenzene 3.4 U 10 ug/L 1,3,5-Trinitrobenzene 3.0 U 10 ug/L 1,3-Dinitrobenzene 2.5 U 10 ug/L 1,4-Naphthoquinone 2.5 U 10 ug/L 1,4-Phenylenediamine 4.0 U 10 ug/L 1-Naphthylamine 2.2 U 10 ug/L 2,3,4,6-TetrachIorophen o1 2.4 U 10 ug/L 2,4,5-Trichlorophenol 2.5 U 10 ug/L 2,4,6-Trichlorophenol 2.6 U 10 ug/L 2,4-Dichlorophenol 2.6 U 10 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 61 of 83 0Nk"q09 www.encolabs.com QUALITY CONTROL DATA Semivolatile Organic Compounds by GCMS - Quality Control Batch 0119001 - EPA 3510C MS - Continued Blank (0319001-BLK1) Continued Prepared: 10/19/2020 07:16 Analyzed: 10/22/2020 13:52 Analvte Result Flaq POL Units 2,4-Dimethylphenol 2.3 U 10 ug/L 2,4-Dinitrophenol 2.6 U 10 ug/L 2,4-Dinitrotoluene 2.6 U 10 ug/L 2,6-Dichlorophenol 2.0 U 10 ug/L 2,6-Dinitrotoluene 2.5 U 10 ug/L 2-Acetylaminofluorene 3.1 U 10 ug/L 2-Chloronaphthalene 2.8 U 10 ug/L 2-Chlorophenol 2.2 U 10 ug/L 2-Methyl-4,6-dinitrophenol 3.3 U 10 ug/L 2-Methylnaphthalene 2.8 U 10 ug/L 2-Methylphenol 2.0 U 10 ug/L 2-Naphthylamine 3.0 U 10 ug/L 2-Nitroaniline 2.5 U 10 ug/L 2-Nitrophenol 1.1 U 10 ug/L 3 & 4-Methylphenol 2.1 U 10 ug/L 3,3'-Dichlorobenzidine 3.5 U 10 ug/L 3,3'-Dimethylbenzidine 2.2 U 10 ug/L 3-Methylcholanthrene 1.3 U 10 ug/L 3-Nitroaniline 2.6 U 10 ug/L 4-Aminobiphenyl 3.5 U 10 ug/L 4-Bromophenyl-phenylether 2.4 U 10 ug/L 4-Chloro-3-methylphenol 2.4 U 10 ug/L 4-Chloroaniline 2.0 U 10 ug/L 4-Chlorophenyl-phenylether 2.6 U 10 ug/L 4-Nitroaniline 3.2 U 10 ug/L 4-Nitrophenol 2.8 U 10 ug/L 5-Nitro-o-toluidine 3.2 U 10 ug/L 7,12-Dimethylbenz(a)anthracene 1.4 U 10 ug/L a,a-Dimethylphenethylamine 3.5 U 10 ug/L Acenaphthene 2.7 U 10 ug/L Acenaphthylene 2.6 U 10 ug/L Acetophenone 2.0 U 10 ug/L Anthracene 2.4 U 10 ug/L Benzo(a)anthracene 2.4 U 10 ug/L Benzo(a)pyrene 2.2 U 10 ug/L Benzo(b)fluoranthene 2.8 U 10 ug/L Benzo(g,h,i)perylene 2.4 U 10 ug/L Benzo(k)fluoranthene 2.4 U 10 ug/L Benzyl alcohol 2.4 U 10 ug/L Bis(2-chloroethoxy)methane 2.4 U 10 ug/L Bis(2-chloroethyl)ether 2.6 U 10 ug/L Bis(2-chloroisopropyl)ether 2.5 U 10 ug/L Bis(2-ethylhexyl)phthalate 1.9 U 5.0 ug/L Butylbenzylphthalate 3.8 U 10 ug/L Chlorobenzilate 2.4 U 10 ug/L Chrysene 2.2 U 10 ug/L Diallate 1.9 U 10 ug/L Dibenzo(a,h)anthracene 2.3 U 10 ug/L Dibenzofuran 2.6 U 10 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 62 of 83 (� �Eo www.encolabs.com QUALITY CONTROL DATA Semivolatile Organic Compounds by GCMS - Quality Control Batch 0119001 - EPA 3510C MS - Continued Blank (0319001-BLK1) Continued Prepared: 10/19/2020 07:16 Analyzed: 10/22/2020 13:52 Analvte Result Flaq POL Units Diethylphtha late 2.4 U 10 ug/L Dimethoate 2.3 U 10 ug/L Dimethylphthalate 2.5 U 10 ug/L Di-n-butylphthalate 2.8 U 10 ug/L Di-n-octylphthalate 3.1 U 10 ug/L Disulfoton 2.0 U 10 ug/L Ethyl methanesulfonate 2.2 U 10 ug/L Famphur 2.7 U 10 ug/L Fluoranthene 3.1 U 10 ug/L Fluorene 2.5 U 10 ug/L Hexachlorobenzene 2.3 U 10 ug/L Hexachlorobutadiene 2.8 U 10 ug/L Hexachlorocyclopentadiene 2.7 U 10 ug/L Hexachloroethane 2.6 U 10 ug/L Hexachloropropene 6.8 U 10 ug/L Indeno(1,2,3-cd)pyrene 2.2 U 10 ug/L Isodrin 1.5 U 10 ug/L Isophorone 2.5 U 10 ug/L Isosafrole 2.2 U 10 ug/L Kepone 7.2 U 20 ug/L Methapyrilene 4.8 U 10 ug/L Methyl Methanesulfonate 2.2 U 10 ug/L Methyl parathion 2.5 U 10 ug/L Nitrobenzene 2.5 U 10 ug/L N-Nitrosodiethylamine 2.1 U 10 ug/L N-Nitrosodimethylamine 1.9 U 10 ug/L N-Nitrosodi-n-butylamine 2.0 U 10 ug/L N-Nitroso-di-n-propylamine 2.3 U 10 ug/L N-nitrosodiphenylamine/Diphenylamine 2.5 U 10 ug/L N-Nitrosomethylethylamine 1.9 U 10 ug/L N-Nitrosopiperidine 2.1 U 10 ug/L N-Nitrosopyrrolidine 1.9 U 10 ug/L O,O,O-Triethylphosphorothioate 2.2 U 10 ug/L o-Toluidine 1.6 U 10 ug/L Parathion 1.7 U 10 ug/L p-Dimethylaminoazobenzene 2.6 U 10 ug/L Pentachlorobenzene 2.7 U 10 ug/L Pentachloronitrobenzene 1.9 U 10 ug/L Phenacetin 2.7 U 10 ug/L Phenanthrene 2.6 U 10 ug/L Phenol 1.7 U 10 ug/L Phorate 2.1 U 10 ug/L Pronamide 1.7 U 10 ug/L Pyrene 3.5 U 10 ug/L Safrole 2.2 U 10 ug/L Thionazin 2.3 U 10 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 2,4,6-Tribromophenol 76 ug/L 100 76 10-179 2-Fluoroblphenyl 45 u91L 50.0 90 10-149 2-Fluorophenol 56 u91L 100 56 10-110 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 63 of 83 (� �Eo www.encolabs.com QUALITY CONTROL DATA Semivolatile Organic Compounds by GCMS - Quality Control Batch 0119001 - EPA 3510C MS - Continued Blank (0319001-BLK1) Continued Prepared: 10/19/2020 07:16 Analyzed: 10/22/2020 13:52 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrobenzene-d5 37 u91L 50.0 75 10-149 Phenol-d5 47 u91L 100 47 10-66 Terphenyl-d14 44 u91L 50.0 89 10-188 LCS (0319001-BS1) Prepared: 10/19/2020 07:16 Analyzed: 10/22/2020 14:24 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2-Chlorophenol 41 10 ug/L 50.0 82 40-109 4-Chloro-3-methylphenol 43 10 ug/L 50.0 85 58-121 4-Nitrophenol 28 10 ug/L 50.0 56 33-105 Acenaphthene 47 10 ug/L 50.0 94 39-125 N-Nitroso-di-n-propylamine 39 10 ug/L 50.0 77 48-126 Phenol 28 10 ug/L 50.0 56 19-78 Pyrene 51 10 ug/L 50.0 103 44-137 2,4,6-Tribromophenol 98 u91L 100 98 10-179 2-Fluorobiphenyl 48 u91L 50.0 96 10-149 2-Fluorophenol 63 u91L 100 63 10-110 Nitrobenzene-d5 40 u91L 50.0 81 10-149 Phenol-d5 51 u91L 100 51 10-88 Terphenyhd14 52 u91L 50.0 103 10-188 Matrix Spike (0319001-MS1) Prepared: 10/19/2020 07:16 Analyzed: 10/22/2020 14:55 Source: CD17019-06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2-Chlorophenol 40 10 ug/L 50.0 2.2 U 80 40-109 4-Chloro-3-methylphenol 44 10 ug/L 50.0 2.4 U 87 58-121 4-Nitrophenol 30 10 ug/L 50.0 2.8 U 59 33-105 Acenaphthene 47 10 ug/L 50.0 2.7 U 95 39-125 N-Nitroso-di-n-propylamine 40 10 ug/L 50.0 2.3 U 80 48-126 Phenol 27 10 ug/L 50.0 1.7 U 54 19-78 Pyrene 52 10 ug/L 50.0 3.5 U 104 44-137 2,4,6-Tribromophenol 100 u91L 100 101 10-179 2-Fluorobiphenyl 48 u91L 50.0 96 10-149 2-Fluorophenol 65 u91L 100 65 10-110 Nitrobenzene-d5 41 u91L 50.0 81 10-149 Phenol-d5 51 u91L 100 51 10-88 Terphenyl-d14 52 u91L 50.0 104 10-188 Matrix Spike Dup (0719001-MSD1) Prepared: 10/19/2020 07:16 Analyzed: 10/22/2020 15:27 Source: CD17019-06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2-Chlorophenol 40 10 ug/L 50.0 2.2 U 79 40-109 0.9 22 4-Chloro-3-methylphenol 43 10 ug/L 50.0 2.4 U 85 58-121 3 22 4-Nitrophenol 28 10 ug/L 50.0 2.8 U 56 33-105 5 27 Acenaphthene 46 10 ug/L 50.0 2.7 U 92 39-125 3 25 N-Nitroso-di-n-propylamine 38 10 ug/L 50.0 2.3 U 77 48-126 4 23 Phenol 28 10 ug/L 50.0 1.7 U 55 19-78 2 18 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 64 of 83 (� �Eo www.encolabs.com QUALITY CONTROL DATA Semivolatile Organic Compounds by GCMS - Quality Control Batch 0119001 - EPA 3510C MS - Continued Matrix Spike Dup (0319001-MSDI) Continued Prepared: 10/19/2020 07:16 Analyzed: 10/22/2020 15:27 Source: CD17019-06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Pyrene 46 10 ug/L 50.0 3.5 U 93 44-137 11 24 2,4,6-Tribromophenol 98 u91L 100 96 10-179 2-Fluoroblphenyl 47 u91L 50.0 94 10-149 2-Fluorophenol 64 u91L 100 64 10-110 Nitrobenzene-d5 40 u91L 50.0 81 10-149 Phenol-d5 51 u91L 100 51 10-88 Terphenyhd14 47 u91L 50.0 95 10-188 Organochlorine Pesticides by GC - Quality Control Batch OJ20002 - EPA 3510C Blank (0120002-BLK3) Prepared: 10/20/2020 04:06 Analyzed: 10/21/2020 07:24 Spike Analvte Result Flaq POL Units Level 4,4'-DDD 0.044 U 0.050 ug/L 4,4'-DDE 0.048 U 0.050 ug/L 4,4'-DDT 0.049 U 0.050 ug/L Aldrin 0.041 U 0.050 ug/L alpha-BHC 0.036 U 0.050 ug/L beta-BHC 0.041 U 0.050 ug/L Chlordane (tech) 0.37 U 0.50 ug/L Chlordane -alpha 0.048 U 0.050 ug/L Chlordane -gamma 0.042 U 0.050 ug/L delta-BHC 0.048 U 0.050 ug/L Dieldrin 0.045 U 0.050 ug/L Endosulfan I 0.045 U 0.050 ug/L Endosulfan II 0.038 U 0.050 ug/L Endosulfan sulfate 0.032 U 0.050 ug/L Endrin 0.041 U 0.050 ug/L Endrin aldehyde 0.049 U 0.050 ug/L gamma-BHC 0.034 U 0.050 ug/L Heptachlor 0.047 U 0.050 ug/L Heptachlor epoxide 0.037 U 0.050 ug/L Methoxychlor 0.048 U 0.050 ug/L Toxaphene 0.28 U 1.0 ug/L Source %REC RPD Result %REC Limits RPD Limit Notes 2,4,5,6-TCMX 0.78 u91L 1.00 78 10-139 Decachlorobiphenyl 1.2 u91L 1.00 120 10-122 LCS (0720002-BS3) Prepared: 10/20/2020 04:06 Analyzed: 10/21/2020 07:51 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4,4'-DDT 1.2 0.050 ug/L 1.00 119 37-139 Dieldrin 0.93 0.050 ug/L 1.00 93 46-132 Endrin 1.0 0.050 ug/L 1.00 101 43-133 2,4,5,E-TCMX 0.68 u91L 1.00 66 10-139 Decachlorobiphenyl 1.2 u91L 1.00 117 10-122 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 65 of 83 (� �Eo www.encolabs.com QUALITY CONTROL DATA Organochlorine Pesticides by GC - Quality Control Batch OJ20002 - EPA 3510C - Continued Matrix Spike (0320002-MS3) Prepared: 10/20/2020 04:06 Analyzed: 10/21/2020 08:05 Source: CD17019-08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4,4'-DDT 1.3 0.050 ug/L 1.00 0.049 U 129 37-139 Dieldrin 1.0 0.050 ug/L 1.00 0.045 U 101 46-132 Endrin 1.1 0.050 ug/L 1.00 0.041 U 110 43-133 2,4,5,E-TCMX 0.70 u91L 1.00 70 10-139 Decachloroblphenyl 0.94 u91L 1.00 94 10-122 Matrix Spike Dup (0720002-MSD1) Prepared: 10/20/2020 04:06 Analyzed: 10/21/2020 08:19 Source: CD17019-08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4,4'-DDT 1.2 0.050 ug/L 1.00 0.049 U 122 37-139 6 26 Dieldrin 0.87 0.050 ug/L 1.00 0.045 U 87 46-132 15 27 Endrin 0.94 0.050 ug/L 1.00 0.041 U 94 43-133 16 26 2,4,5,E-TCMX 0.63 u91L 1.00 63 10-139 Decachlorobiphenyl 0.88 u91L 1.00 88 10-122 Polychlorinated Biphenyls by GC - Quality Control Batch 0110003 - EPA 3510C Blank (0320003-BLK3) Prepared: 10/20/2020 04:14 Analyzed: 10/21/2020 08:33 Analvte Result Flag Q Units PCB-1016/1242 0.48 U 0.50 ug/L PCB-1221 0.43 U 0.50 ug/L PCB-1232 0.50 U 0.50 ug/L PCB-1248 0.45 U 0.50 ug/L PCB-1254 0.43 U 0.50 ug/L PCB-1260 0.47 U 0.50 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 2,4,5,6-TCMX 0.83 u91L 1.00 83 10-128 Decachlorobiphenyl 1.1 u91L 1.00 106 10-129 LCS (0320003-BS1) Prepared: 10/20/2020 04:14 Analyzed: 10/21/2020 08:46 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes PCB-1016/1242 6.8 0.50 ug/L 10.0 68 43-123 PCB-1260 9.0 0.50 ug/L 10.0 90 41-125 2,4,5,6-TCMX 0.80 u91L 1.00 80 10-128 Decachlorobiphenyl 0.48 u91L 1.00 48 10-129 Matrix Spike (0320003-MS1) Prepared: 10/20/2020 04:14 Analyzed: 10/21/2020 09:00 Source: CD17019-08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes PCB-1016/1242 8.6 0.50 ug/L 10.0 0.48 U 86 43-123 PCB-1260 14 0.50 ug/L 10.0 0.47 U 139 41-125 QM-07 2,4,5,E-TCMX 1.0 u91L 1.00 101 10-128 Decachlorobiphenyl 1.1 u91L 1.00 114 10-129 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 66 of 83 (� �Eo www.encolabs.com QUALITY CONTROL DATA Polychlorinated Biphenyls by GC - Quality Control Batch OJ20003 - EPA 3510C - Continued Matrix Spike Dup (0320003-MSDI) Prepared: 10/20/2020 04:14 Analyzed: 10/21/2020 09:13 Source: CD17019-08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes PCB-1016/1242 7.1 0.50 ug/L 10.0 0.48 U 71 43-123 18 23 PCB-1260 11 0.50 ug/L 10.0 0.47 U 108 41-125 25 31 2,4,5,6-TCMX 0.95 u91L 1.00 95 10-128 Decachloroblphenyl 0.84 u91L 1.00 84 10-129 Metals by EPA 6000/7000 Series Methods - Quality Control Batch OJ21044 - EPA 7470A Blank (0121044-BLK3) Prepared: 10/21/2020 16:27 Analyzed: 10/23/2020 14:39 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.150 U 0.200 ug/L LCS (0321044-BS1) Prepared: 10/21/2020 16:27 Analyzed: 10/23/2020 14:42 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.20 0.200 ug/L 5.00 104 80-120 Matrix Spike (0723044-MS1) Prepared: 10/21/2020 16:27 Analyzed: 10/23/2020 14:52 Source: CD16585-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.28 0.200 ug/L 5.00 0.150 U 106 75-125 Matrix Spike Dup (0323044-MSD1) Prepared: 10/21/2020 16:27 Analyzed: 10/23/2020 14:55 Source: CD16585-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.31 0.200 ug/L 5.00 0.150 U 106 75-125 0.6 25 Post Spike (0321044-PS1) Prepared: 10/21/2020 16:27 Analyzed: 10/23/2020 14:58 Source: CD16585-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.58 0.200 ug/L 5.00 0.00500 112 75-125 Batch OJ21046 - EPA 7470A Blank (0321046-BLK3) Prepared: 10/21/2020 16:34 Analyzed: 10/23/2020 16:08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.150 U 0.200 ug/L LCS (0321046-BSI) Prepared: 10/21/2020 16:34 Analyzed: 10/23/2020 16:10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.13 0.200 ug/L 5.00 103 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 67 of 83 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals by EPA 6000/7000 Series Methods - Quality Control Batch OJ21046 - EPA 7470A - Continued Matrix Spike (0323046-MS3) Prepared: 10/21/2020 16:34 Analyzed: 10/23/2020 16:15 Source: CD16SSS-13 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.09 0.200 ug/L 5.00 0.150 U 102 75-125 Matrix Spike Dup (0723046-MSD1) Prepared: 10/21/2020 16:34 Analyzed: 10/23/2020 16:17 Source: CD16585-13 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.07 0.200 ug/L 5.00 0.150 U 101 75-125 0.4 25 Post Spike (0323046-PS1) Prepared: 10/21/2020 16:34 Analyzed: 10/23/2020 16:20 Source: CD16585-13 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.42 0.200 ug/L 5.00-0.0520 108 75-125 Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 012102E - EPA 3005A Blank (0321028-BLKI) Prepared: 10/21/2020 12:00 Analyzed: 10/23/2020 10:19 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 7.60 U 10.0 ug/L Barium 1.10 U 10.0 ug/L Beryllium 0.160 U 1.00 ug/L Cadmium 0.360 U 1.00 ug/L Chromium 1.40 U 10.0 ug/L Cobalt 1.40 U 10.0 ug/L Copper 1.60 U 10.0 ug/L Iron 22.0 U 50.0 ug/L Lead 3.10 U 10.0 ug/L Manganese 1.50 U 10.0 ug/L Nickel 2.20 U 10.0 ug/L Silver 1.90 U 10.0 ug/L Tin 2.90 U 10.0 ug/L Vanadium 1.40 U 10.0 ug/L Zinc 4.40 U 10.0 ug/L LCS (0321028-BSI) Prepared: 10/21/2020 12:00 Analyzed: 10/23/2020 10:27 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 208 10.0 ug/L 200 104 80-120 Barium 216 10.0 ug/L 200 108 80-120 Beryllium 20.3 1.00 ug/L 20.0 101 80-120 Cadmium 20.8 1.00 ug/L 20.0 104 80-120 Chromium 207 10.0 ug/L 200 104 80-120 Cobalt 209 10.0 ug/L 200 104 80-120 Copper 206 10.0 ug/L 200 103 80-120 Iron 1060 50.0 ug/L 1000 106 80-120 Lead 210 10.0 ug/L 200 105 80-120 Manganese 207 10.0 ug/L 200 104 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 68 of 83 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 012102E - EPA 3OO5A - Continued LCS (OJ21028-BS1) Continued Prepared: 10/21/2020 12:00 Analyzed: 10/23/2020 10:27 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nickel 215 10.0 ug/L 200 107 80-120 Silver 211 10.0 ug/L 200 105 80-120 Tin 206 10.0 ug/L 200 103 80-120 Vanadium 204 10.0 ug/L 200 102 80-120 Zinc 213 10.0 ug/L 200 107 80-120 Matrix Spike (OJ23028-MS3) Prepared: 10/21/2020 12:00 Analyzed: 10/23/2020 10:30 Source: CD16320-08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 201 10.0 ug/L 200 7.60 U 100 75-125 Barium 369 10.0 ug/L 200 192 89 75-125 Beryllium 20.1 1.00 ug/L 20.0 0.160 U 101 75-125 Cadmium 20.3 1.00 ug/L 20.0 0.360 U 101 75-125 Chromium 201 10.0 ug/L 200 1.40 U 101 75-125 Cobalt 204 10.0 ug/L 200 1.40 U 102 75-125 Copper 200 10.0 ug/L 200 3.06 98 75-125 Iron 1150 50.0 ug/L 1000 784 36 75-125 QM-07 Lead 205 10.0 ug/L 200 3.10 U 103 75-125 Manganese 231 10.0 ug/L 200 32.0 99 75-125 Nickel 208 10.0 ug/L 200 2.20 U 104 75-125 Silver 203 10.0 ug/L 200 1.90 U 101 75-125 Tin 204 10.0 ug/L 200 2.90 U 102 75-125 Vanadium 200 10.0 ug/L 200 1.40 U 100 75-125 Zinc 214 10.0 ug/L 200 5.92 104 75-125 Matrix Spike Dup (OJ23028-MSDI) Prepared: 10/21/2020 12:00 Analyzed: 10/23/2020 10:32 Source: CD16320-08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 194 10.0 ug/L 200 7.60 U 97 75-125 3 20 Barium 386 10.0 ug/L 200 192 97 75-125 4 20 Beryllium 20.4 1.00 ug/L 20.0 0.160 U 102 75-125 1 20 Cadmium 20.3 1.00 ug/L 20.0 0.360 U 101 75-125 0.2 20 Chromium 205 10.0 ug/L 200 1.40 U 102 75-125 2 20 Cobalt 205 10.0 ug/L 200 1.40 U 103 75-125 0.7 20 Copper 201 10.0 ug/L 200 3.06 99 75-125 0.7 20 Iron 1750 50.0 ug/L 1000 784 97 75-125 42 20 QM-11 Lead 207 10.0 ug/L 200 3.10 U 103 75-125 0.8 20 Manganese 238 10.0 ug/L 200 32.0 103 75-125 3 20 Nickel 209 10.0 ug/L 200 2.20 U 104 75-125 0.08 20 Silver 203 10.0 ug/L 200 1.90 U 101 75-125 0.03 20 Tin 204 10.0 ug/L 200 2.90 U 102 75-125 0.3 20 Vanadium 202 10.0 ug/L 200 1.40 U 101 75-125 1 20 Zinc 213 10.0 ug/L 200 5.92 103 75-125 0.4 20 Post Spike (0323028-PSI) Prepared: 10/21/2020 12:00 Analyzed: 10/23/2020 10:34 Source: CD16320-08 Analvte Arsenic Spike Source %REC Result Flaq POL Units Level Result %REC Limits RPD 0.203 0.0100 mg/L 0.200 0.00301 100 80-120 RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 69 of 83 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch OJ21028 - EPA 3005A - Continued Post Spike (0321028-PSI) Continued Prepared: 10/21/2020 12:00 Analyzed: 10/23/2020 10:34 Source: CD16320-08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Barium 0.393 0.0100 mg/L 0.200 0.192 101 80-120 Beryllium 0.0206 0.00100 mg/L 0.0200 6.29E-5 103 80-120 Cadmium 0.0207 0.00100 mg/L 0.0200 -3.76E-5 103 80-120 Chromium 0.209 0.0100 mg/L 0.200 0.00123 104 80-120 Cobalt 0.210 0.0100 mg/L 0.200 0.00118 104 80-120 Copper 0.205 0.0100 mg/L 0.200 0.00306 101 80-120 Iron 1.89 0.0500 mg/L 1.00 0.784 111 80-120 Lead 0.210 0.0100 mg/L 0.200 0.00263 104 80-120 Manganese 0.241 0.0100 mg/L 0.200 0.0320 105 80-120 Nickel 0.214 0.0100 mg/L 0.200 0.000773 107 80-120 Silver 0.215 0.0100 mg/L 0.200 0.000109 108 80-120 Tin 0.209 0.0100 mg/L 0.200 0.00146 104 80-120 Vanadium 0.206 0.0100 mg/L 0.200 0.00118 103 80-120 Zinc 0.220 0.0100 mg/L 0.200 0.00592 107 80-120 Batch OJ27036 - EPA 3005A Blank (0127036-BLK3) Prepared: 10/27/2020 14:33 Analyzed: 11/04/2020 22:55 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 0.370 U 1.00 ug/L Selenium 0.910 U 1.00 ug/L Thallium 0.110 U 1.00 ug/L LCS (0327036-BSI) Prepared: 10/27/2020 14:33 Analyzed: 11/04/2020 22:59 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 20.7 1.00 ug/L 20.0 104 80-120 Selenium 21.8 1.00 ug/L 20.0 109 80-120 Thallium 21.2 1.00 ug/L 20.0 106 80-120 Matrix Spike (OJ27036-MS3) Prepared: 10/27/2020 14:33 Analyzed: 11/04/2020 23:03 Source: CD16047-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 43.0 2.00 ug/L 40.0 0.740 U 108 75-125 Selenium 44.4 2.00 ug/L 40.0 1.82 U 111 75-125 Thallium 43.1 2.00 ug/L 40.0 0.220 U 108 75-125 Matrix Spike Dup (OJ27036-MSDI) Prepared: 10/27/2020 14:33 Analyzed: 11/04/2020 23:07 Source: CD16047-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 42.3 2.00 ug/L 40.0 0.740 U 106 75-125 2 20 Selenium 40.0 2.00 ug/L 40.0 1.82 U 100 75-125 10 20 Thallium 42.7 2.00 ug/L 40.0 0.220 U 107 75-125 1 20 Post Spike (0327036-PSI) Prepared: 10/27/2020 14:33 Analyzed: 11/04/2020 23:12 Source: CD16047-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 70 of 83 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch OJ27036 - EPA 3OO5A - Continued Post Spike (0327036-PS1) Continued Prepared: 10/27/2020 14:33 Analyzed: 11/04/2020 23:12 Source: CD16047-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Antimony 25.3 1.00 ug/L 20.0 0.0791 126 75-125 QM-08 Selenium 25.3 1.00 ug/L 20.0 -0.0433 127 75-125 QM-08 Thallium 25.0 1.00 ug/L 20.0 0.0471 125 75-125 Classical Chemistry Parameters - Quality Control Batch 0114040 - NO PREP Blank (0114040-BLK3) Prepared: 10/14/2020 14:46 Analyzed: 10/14/2020 16:38 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.017 U 0.10 mg/L LCS (O]14040-BS1) Prepared: 10/14/2020 14:46 Analyzed: 10/14/2020 16:59 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.1 0.10 mg/L 1.00 105 90-110 LCS (0714040-BS2) Prepared: 10/14/2020 14:46 Analyzed: 10/15/2020 11:04 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 101 90-110 LCS (0314040-BS3) Prepared: 10/14/2020 14:46 Analyzed: 10/15/2020 11:07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 101 90-110 Matrix Spike (0314040-MS3) Prepared: 10/14/2020 14:46 Analyzed: 10/14/2020 16:40 Source: CD14179-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 0.017 U 104 90-110 Matrix Spike Dup (0714040-MSD1) Prepared: 10/14/2020 14:46 Analyzed: 10/14/2020 16:41 111 Source: CD14179-01 Analvte Nitrite as N Batch 0115042 - NO PREP Result Flaq POL 1.1 0.10 Spike Source %REC RPD Units Level Result %REC Limits RPD Limit Notes mg/L 1.00 0.017 U 105 90-110 2 10 Blank (0315042-BLK3) Prepared: 10/15/2020 15:34 Analyzed: 10/15/2020 17:09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.017 U 0.10 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 71 of 83 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 0JI5042 - NO PREP - Continued LCS (OJ15042-BS1) Prepared: 10/15/2020 15:34 Analyzed: 10/15/2020 17:32 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Nitrite as N 0.96 0.10 mg/L 1.00 96 90-110 Matrix Spike (0315042-MS3) Prepared: 10/15/2020 15:34 Analyzed: 10/15/2020 17:11 Source: CD15705-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 0.017 U 100 90-110 Matrix Spike (OJ15042-MS2) Prepared: 10/15/2020 15:34 Analyzed: 10/15/2020 17:15 Source: CD16585-02 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 0.017 U 101 90-110 Matrix Spike Dup (0315042-MSDI) Prepared: 10/15/2020 15:34 Analyzed: 10/15/2020 17:12 Source: CD15705-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 0.017 U 100 90-110 0.3 10 Batch OJ20011 - NO PREP Blank (0320011-BLK3) Prepared & Analyzed: 10/20/2020 17:13 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Dissolved Solids 50 U 50 mg/L LCS (0320011-BSI) Prepared & Analyzed: 10/20/2020 17:13 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Dissolved Solids 960 50 mg/L 1000 96 80-120 Duplicate (0320011-DUP3) Prepared & Analyzed: 10/20/2020 17:13 Source: CD15656-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Dissolved Solids 2300 100 mg/L 2400 2 20 Duplicate (0320011-DUP2) Prepared & Analyzed: 10/20/2020 17:13 Source: CD15656-02 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Dissolved Solids 2000 100 mg/L 1900 0.8 20 Batch 0.720015 - NO PREP Blank (0120015-BLK3) Prepared: 10/20/2020 14:41 Analyzed: 10/20/2020 15:00 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Sulfide 0.010 U 0.10 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 72 of 83 QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch OJ20015 - NO PREP - Continued (� �Eo www.encolabs.com LCS (0320015-BS1) Prepared: 10/20/2020 14:41 Analyzed: 10/20/2020 15:00 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.34 0.10 mg/L 0.401 85 80-120 Duplicate (0320015-DUPl) Prepared: 10/20/2020 14:41 Analyzed: 10/20/2020 15:00 Source: CD16585-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.010 U 0.10 mg/L 0.010 U 25 Matrix Spike (OJ20015-MS3) Prepared: 10/20/2020 14:41 Analyzed: 10/20/2020 15:00 Source: CD16585-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.24 0.10 mg/L 0.401 0.010 U 60 80-120 QM-07 Matrix Spike Dup (0320015-MSDI) Prepared: 10/20/2020 14:41 Analyzed: 10/20/2020 15:00 Source: CD16585-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.28 0.10 mg/L 0.401 0.010 U 71 80-120 16 25 QM-07 Batch OJ2OO16 - NO PREP Blank (0320016-BLK3) Prepared: 10/20/2020 13:21 Analyzed: 10/20/2020 16:38 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.010 U 0.10 mg/L LCS (0320016-BSI) Prepared: 10/20/2020 13:21 Analyzed: 10/20/2020 16:38 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.36 0.10 mg/L 0.401 89 80-120 Duplicate (0320016-DUPl) Prepared: 10/20/2020 13:21 Analyzed: 10/20/2020 16:38 Source: CD16585-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.023 3 0.10 mg/L 0.017 30 25 QR-04 Matrix Spike (0320016-MS3) Prepared: 10/20/2020 13:21 Analyzed: 10/20/2020 16:38 Source: CD16585-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.16 0.10 mg/L 0.401 0.017 35 80-120 QM-07 Matrix Spike Dup (0320016-MSDI) Prepared: 10/20/2020 13:21 Analyzed: 10/20/2020 16:38 Source: CD16585-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.15 0.10 mg/L 0.401 0.017 32 80-120 8 25 QM-07 Batch OJ2OO17 - NO PREP FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 73 of 83 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch OJ20017 - NO PREP - Continued Blank (0320017-BLK1) Prepared: 10/20/2020 18:02 Analyzed: 10/20/2020 18:26 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.010 U 0.10 mg/L LCS (0720017-BS3) Prepared: 10/20/2020 18:02 Analyzed: 10/20/2020 18:26 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.34 0.10 mg/L 0.401 85 80-120 Duplicate (0120017-DUP3) Prepared: 10/20/2020 18:02 Analyzed: 10/20/2020 18:26 Source: CD15705-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.010 U 0.10 mg/L 0.010 U 25 Matrix Spike (0320017-MS3) Prepared: 10/20/2020 18:02 Analyzed: 10/20/2020 18:26 Source: CD15705-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.30 0.10 mg/L 0.401 0.010 U 74 80-120 QM-07 Matrix Spike Dup (0720017-MSD1) Prepared: 10/20/2020 18:02 Analyzed: 10/20/2020 18:26 Source: CD15705-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.30 0.10 mg/L 0.401 0.010 U 74 80-120 1 25 QM-07 Batch OJ20019 - NO PREP Blank (0120019-BLK3) Prepared: 10/20/2020 13:40 Analyzed: 10/20/2020 15:42 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 14 U 15 mg/L LCS (O]20019-BS1) Prepared: 10/20/2020 13:40 Analyzed: 10/20/2020 15:43 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 100 15 mg/L 100 102 80-120 Matrix Spike (0720019-MS3) Prepared: 10/20/2020 13:40 Analyzed: 10/20/2020 15:44 Source: CD16585-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 170 15 mg/L 37.8 120 135 80-120 QM-07 Matrix Spike Dup (0320019-MSDi) Prepared: 10/20/2020 13:40 Analyzed: 10/20/2020 15:45 Source: CD16585-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 170 15 mg/L 37.8 120 135 80-120 0.1 25 QM-07 Batch OJ21014 - NO PREP FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 74 of 83 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch OJ21014 - NO PREP - Continued Blank (0321014-BLK1) Prepared: 10/21/2020 11:28 Analyzed: 10/21/2020 12:03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 2.2 U 5.0 mg/L Sulfate as SO4 2.9 U 5.0 mg/L LCS (0323014-BSI) Prepared: 10/21/2020 11:28 Analyzed: 10/21/2020 12:21 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 49 5.0 mg/L 50.0 97 90-110 Sulfate as SO4 48 5.0 mg/L 50.0 95 90-110 Matrix Spike (0323014-MS3) Prepared: 10/21/2020 11:28 Analyzed: 10/21/2020 12:56 Source: CD14179-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 41 10 mg/L 40.0 5.4 89 90-110 QM-07 Sulfate as SO4 43 10 mg/L 40.0 8.3 86 90-110 QM-07 Matrix Spike (0323014-MS2) Prepared: 10/21/2020 11:28 Analyzed: 10/21/2020 13:49 Source: CD15832-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 580 E 5.0 mg/L 20.0 570 89 90-110 QM-07 Sulfate as SO4 30 5.0 mg/L 20.0 10 97 90-110 Matrix Spike Dup (0323014-MSDI) Prepared: 10/21/2020 11:28 Analyzed: 10/21/2020 13:14 Source: CD14179-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 41 10 mg/L 40.0 5.4 89 90-110 0.1 10 QM-07 Sulfate as SO4 43 10 mg/L 40.0 8.3 87 90-110 0.3 10 QM-07 Batch 0121015 - NO PREP Blank (0321015-BLK3) Prepared: 10/21/2020 11:28 Analyzed: 10/21/2020 20:35 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 2.2 U 5.0 mg/L Sulfate as SO4 2.9 U 5.0 mg/L LCS (0321015-BS1) Prepared: 10/21/2020 11:28 Analyzed: 10/21/2020 20:53 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 49 5.0 mg/L 50.0 97 90-110 Sulfate as SO4 48 5.0 mg/L 50.0 95 90-110 Matrix Spike (0321015-MS3) Prepared: 10/21/2020 11:28 Analyzed: 10/21/2020 21:28 Source: CD14306-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 25 5.0 mg/L 20.0 6.6 92 90-110 Sulfate as SO4 32 5.0 mg/L 20.0 14 93 90-110 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 75 of 83 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch OJ21015 - NO PREP - Continued Matrix Spike (0321015-MS2) Prepared: 10/21/2020 11:28 Analyzed: 10/21/2020 22:57 Source: CD15655-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 690 50 mg/L 200 500 96 90-110 Sulfate as SO4 290 50 mg/L 200 110 91 90-110 Matrix Spike Dup (0]23015-MSDi) Prepared: 10/21/2020 11:28 Analyzed: 10/21/2020 21:46 Source: CD14306-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 25 5.0 mg/L 20.0 6.6 94 90-110 1 10 Sulfate as SO4 33 5.0 mg/L 20.0 14 95 90-110 2 10 Batch OJ21029 - Same Blank (0321029-BLK3) Prepared: 10/22/2020 08:39 Analyzed: 10/23/2020 09:56 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes Cyanide (total) 0.0049 U 0.010 mg/L LCS (0321029-BSI) Prepared: 10/22/2020 08:39 Analyzed: 10/23/2020 09:58 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Cyanide (total) 0.15 0.010 mg/L 0.150 102 85-115 Matrix Spike (0323029-MS1) Prepared: 10/22/2020 08:39 Analyzed: 10/23/2020 10:05 Source: CD10575-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Cyanide (total) 0.12 0.010 mg/L 0.150 0.0049 77 85-115 QM-07 Matrix Spike (0323029-MS2) Prepared: 10/22/2020 08:39 Analyzed: 10/23/2020 10:10 Source: CD16230-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Cyanide (total) 0.16 0.010 mg/L 0.150 0.0049 U 105 85-115 Matrix Spike Dup (0]23029-MSDi) Prepared: 10/22/2020 08:39 Analyzed: 10/23/2020 10:06 Source: CD10575-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Cyanide (total) 0.11 0.010 mg/L 0.150 0.0049 67 85-115 13 20 QM-07 Batch OJ23015 - NO PREP Blank (0323015-BLK1) Prepared: 10/23/2020 11:23 Analyzed: 10/23/2020 12:38 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 14 U 15 mg/L LCS (0323015-BS3) Prepared: 10/23/2020 11:23 Analyzed: 10/23/2020 12:39 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 100 15 mg/L 100 104 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 76 of 83 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch OJ23015 - NO PREP - Continued Matrix Spike (0323015-MS3) Prepared: 10/23/2020 11:23 Analyzed: 10/23/2020 12:40 Source: CD16049-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 56 15 mg/L 37.8 14 U 149 80-120 QM-07 Matrix Spike Dup (0723015-MSD1) Prepared: 10/23/2020 11:23 Analyzed: 10/23/2020 12:41 Source: CD16049-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 52 15 mg/L 37.8 14 U 138 80-120 8 25 QM-07 Batch OJ26O13 - NO PREP Blank (0326013-BLK3) Prepared: 10/26/2020 09:33 Analyzed: 10/26/2020 12:41 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/L LCS (OJ26013-BS1) Prepared: 10/26/2020 09:33 Analyzed: 10/26/2020 12:43 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.3 0.10 mg/L 1.25 101 90-110 Matrix Spike (0326013-MS3) Prepared: 10/26/2020 09:33 Analyzed: 10/26/2020 12:47 Source: CD16585-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.52 0.10 mg/L 0.521 0.090 83 90-110 QM-07 Matrix Spike (OJ26013-MS2) Prepared: 10/26/2020 09:33 Analyzed: 10/26/2020 12:52 Source: CD16586-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.3 0.10 mg/L 0.521 0.85 90 90-110 Matrix Spike Dup (0326013-MSDI) Prepared: 10/26/2020 09:33 Analyzed: 10/26/2020 12:48 Source: CD16585-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.49 0.10 mg/L 0.521 0.090 76 90-110 8 10 QM-07 Batch OJ26O14 - NO PREP Blank (0326014-BLK3) Prepared: 10/26/2020 09:34 Analyzed: 10/26/2020 13:33 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/L LCS (0326014-BSI) Prepared: 10/26/2020 09:34 Analyzed: 10/26/2020 13:35 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.3 0.10 mg/L 1.25 102 90-110 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 77 of 83 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch OJ26014 - NO PREP - Continued Matrix Spike (0326014-MS3) Prepared: 10/26/2020 09:34 Analyzed: 10/26/2020 13:38 Source: CD12415-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.59 0.10 mg/L 0.521 0.041 U 113 90-110 QM-07 Matrix Spike (0326014-MS2) Prepared: 10/26/2020 09:34 Analyzed: 10/26/2020 13:47 Source: CD14180-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.58 0.10 mg/L 0.521 0.078 97 90-110 Matrix Spike Dup (0326014-MSDi) Prepared: 10/26/2020 09:34 Analyzed: 10/26/2020 13:40 Source: CD12415-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.59 0.10 mg/L 0.521 0.041 U 113 90-110 0.7 10 QM-07 Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 0.720037 - EPA 5030B MS Blank (0320037-BLK3) Prepared: 10/20/2020 00:00 Analyzed: 10/20/2020 12:02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 0.80 U 2.0 ug/L Toluene-& 5.2 ug/L 5.00 104 75-125 LCS (0320037-BS1) Prepared: 10/20/2020 00:00 Analyzed: 10/20/2020 11:37 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 24 2.0 ug/L 20.0 121 80-133 Toluene-& 5.2 ug/L 5.00 104 75-125 Matrix Spike (0320037-MS1) Prepared: 10/20/2020 00:00 Analyzed: 10/20/2020 20:02 Source: CD16585-01 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 26 2.0 ug/L 20.0 1.3 123 80-133 Toluene-& 5.1 ug/L 5.00 103 75-125 Matrix Spike Dup (0320037-MSDi) Prepared: 10/20/2020 00:00 Analyzed: 10/20/2020 20:27 Source: CD16585-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 26 2.0 ug/L 20.0 1.3 124 80-133 0.9 19 Toluene-d8 5.6 ug/L 5.00 i11 75-125 Chlorinated Herbicides by GC - Quality Control Batch OJ20036 - EPA 3510C Blank (0320036-BLK1) Prepared: 10/20/2020 14:30 Analyzed: 10/22/2020 15:43 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 78 of 83 (� �Eo www.encolabs.com QUALITY CONTROL DATA Chlorinated Herbicides by GC - Quality Control Batch OJ20036 - EPA 3510C - Continued Blank (0320036-BLK1) Continued Prepared: 10/20/2020 14:30 Analyzed: 10/22/2020 15:43 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2,4,5-T 0.28 U 0.50 ug/L 2,4,5-TP (Silvex) 0.44 U 0.50 ug/L 2,4-D 0.27 U 0.50 ug/L Dinoseb 0.32 U 0.50 ug/L Pentachlorophenol 0.19 U 0.50 ug/L 2,4-DC,4A 2.6 ug/L 2.00 132 37-134 LCS (0320036-BSI) Prepared: 10/20/2020 14:30 Analyzed: 10/22/2020 16:59 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 1.8 0.50 ug/L 2.00 90 24-135 2,4-D 2.0 0.50 ug/L 2.00 98 20-134 2,4-OCAA 2.3 ug/L 2.00 114 37-134 Matrix Spike (0320036-MS3) Prepared: 10/20/2020 14:30 Analyzed: 10/22/2020 17:24 Source: AD06819-01 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 7.0 2.5 ug/L 10.0 2.2 U 70 24-135 2,4-D 7.4 2.5 ug/L 10.0 1.4 U 74 20-134 2,4-DCAA 12 ug/L 10.0 118 37-134 Matrix Spike Dup (0320036-MSD1) Prepared: 10/20/2020 14:30 Analyzed: 10/22/2020 17:50 Source: AD06819-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 6.6 2.5 ug/L 10.0 2.2 U 66 24-135 7 19 2,4-D 6.2 2.5 ug/L 10.0 1.4 U 62 20-134 17 19 2,4-DC4A 12 u9/L 10.0 116 37-134 Dissolved Gases by GC - Quality Control Batch 0119006 - Same Blank (0319006-BLK3) Prepared: 10/19/2020 08:01 Analyzed: 10/19/2020 10:09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 2.07 U 2.50 mg/L Ethane 0.00510 U 0.00600 mg/L Ethene 0.00510 U 0.00600 mg/L Methane 0.00400 U 0.00500 mg/L LCS (0319006-BSI) Prepared: 10/19/2020 08:01 Analyzed: 10/19/2020 09:31 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 55.3 2.50 mg/L 45.8 121 70-130 Ethane 0.414 0.00600 mg/L 0.323 128 70-130 Ethene 0.353 0.00600 mg/L 0.302 117 70-130 Methane 0.199 0.00500 mg/L 0.172 116 70-130 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 79 of 83 QUALITY CONTROL DATA Dissolved Gases by GC - Quality Control Batch 0JI9006 - Same - Continued (� �Eo www.encolabs.com LCS Dup (0319006-BSD1) Prepared: 10/19/2020 08:01 Analyzed: 10/19/2020 09:47 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 51.6 2.50 mg/L 45.8 113 70-130 7 30 Ethane 0.359 0.00600 mg/L 0.323 111 70-130 14 30 Ethene 0.316 0.00600 mg/L 0.302 104 70-130 11 30 Methane 0.171 0.00500 mg/L 0.172 99 70-130 15 30 Duplicate (0719006-DUPl) Prepared: 10/19/2020 08:01 Analyzed: 10/19/2020 13:24 Source: AD06825-21 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 177 2.50 mg/L 157 12 30 Ethane 0.00510 U 0.00600 mg/L 0.00510 U 30 Ethene 0.00510 U 0.00600 mg/L 0.00510 U 30 Methane 0.0602 0.00500 mg/L 0.0457 27 30 Classical Chemistry Parameters - Quality Control Batch OJ22067 - NO PREP Blank (0322067-BLK3) Prepared: 10/23/2020 12:30 Analyzed: 10/23/2020 12:59 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 0.54 U 1.0 mg/L LCS (0322067-BSI) Prepared: 10/23/2020 12:30 Analyzed: 10/23/2020 12:59 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 48 1.0 mg/L 50.0 96 85-115 Duplicate (0322067-DUPl) Prepared: 10/23/2020 12:30 Analyzed: 10/27/2020 16:42 Source: AD06963-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 36 1.0 mg/L 37 1 20 Matrix Spike (0722067-MS3) Prepared: 10/23/2020 12:30 Analyzed: 10/23/2020 12:59 Source: AD07020-06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 48 1.0 mg/L 50.0 2.0 92 85-115 Matrix Spike Dup (0322067-MSDI) Prepared: 10/23/2020 12:30 Analyzed: 10/23/2020 12:59 Source: AD07020-06 Analvte Total Organic Carbon Batch OJ26043 - NO PREP Result Flaq POL 48 1.0 Spike Source %REC RPD Units Level Result %REC Limits RPD Limit Notes mg/L 50.0 2.0 92 85-115 0.8 21 Blank (0326043-BLK1) Prepared: 10/26/2020 15:22 Analyzed: 10/27/2020 11:08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon FINAL 0.54 U 1.0 mg/L This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 80 of 83 QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch OJ26043 - NO PREP - Continued (� �Eo www.encolabs.com LCS (O]26043-BS1) Prepared: 10/26/2020 15:22 Analyzed: 10/27/2020 11:08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 46 1.0 mg/L 50.0 92 85-115 Matrix Spike (0726043-MS3) Prepared: 10/26/2020 15:22 Analyzed: 10/27/2020 11:08 Source: AD07020-06RE3 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 44 1.0 mg/L 50.0 2.3 84 85-115 QM-07 Matrix Spike Dup (0]26043-MSDi) Prepared: 10/26/2020 15:22 Analyzed: 10/27/2020 11:08 Source: AD07020-06RE3 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 43 1.0 mg/L 50.0 2.3 83 85-115 2 21 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 81 of 83 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. QB-06 The continuing calibration blank had a positive result for the analyte; however, the concentration in the continuing calibration blank is less than 10% of the sample result. There is minimal impact to the data. QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test). QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits. QR-04 Duplicate precision outside acceptance limits due to low analyte concentration. QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there is no impact. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 82 of 83 o 3 mm m ,�3 n x a FF m a m m 0 o� �m _ S a a } w m c m G m y K �C / AN m 1 r N 1 m 31 m m � � fnp 0 � N t q W n 7 n c n m � � n 6 c m 0 w 0— w o w 3 m' 3 m m 3 3 m C v h SD "6 m 6 [D W m m m -Ni n ti R;' 2 ppQ� map] w O) m J i i i i c cr fig, }J ii Jim }i f��► J �► i i i i J i J J (n A, ao 00 v W v m T T T a t� co Nca C SQ o w CA �NV N N p w tn t V1 O o ° n o m Z z 4Q U1 3 mw 3 m a = n d m a i o �pON ��� L� p L]QP G7 6) o Q G) 0 G} 6CC3 Q 0 � � m � -4 W m 0 RQ co tO LO cn w w L I m o X —L 8081 B Appendix 2 X S082A Appondtx 28151 A Appendix 2 o800 X X X X X )C 82Appendix 1 �82OW R. 9 Exiended,92600 $IM 10 CD y m 82600 Appendix 2,826W X E48nded,62600 Sim IL) m X X X X 82800,82WD Appendix 1,42000 o S EAended,82KO SO M a o 8270E Appendix 2 ryry a m X a 'm N n Sb,S%TI,V,Zn m X X X X X X X X X X X X Sr%TI,V Zn 3W-2,T[)S SM2640C X X SM2540C X X X X X X X X w T N 0 a CD R F 3 -.i ID m 0 m m CD -� Q XCD 3 coC ID _N - Q `0 3 (D /�� V ! w m Cl 2� a g 0 U CL 7 n C s d- A 98 m o j - z rn 'n m �r- N w O A A Z �M z a r tl m N f1 O Oi cr N n O 3 3 n _ � c 1 � � 3 o �_ o m. c 0 3 Z fl m 7, rn Z S m m v y m Vr- D m o' 0 O m N V] c 3 m m m m m z chi 8 Q m C3 m 3a s a A s m v D a E m w x 0 T� n — n y m z n n � O " ro � a o o � o ID 0 � m 3 m Q. 5 gV O 0 e j C m m n_ h c 3 = o x x x x x w K i N : � O i 3 iz xxxx Xd Z E � N � 2 .m m 3 n N ]7 SD m Q v rD m m m (D C o 3 CD 'O ,{M�/ �3 N co y � C D Q N h^,� a m m m9° a +VI 0 � Qo co 0 CT fA ro m Sl ° 9 b o 0 C � co". n ' C a 3 m m a O m ci o v 8081 B Appendix 2 SOWA AppendbcZ8161A Appendix 2 MOD Ajpimft 1,BMW EA&nded,62$0D s`a +o 8280D AppWMW 2,8280D EA@nded,82M 8NI ID 82600,826QDAppend+x 1,8280D ExterKWAMM Sim +a 8270E Appendix 2 36 2,-ros S+2640C SM2640C O 2 3 � a c CD m cn 7 ID _a w n a E.d - Sample Preservation Verification ENCO Cary. NCLI Work Order: CD16585 Project: Moore County Active C & D LF Client: S&ME, Inc. (SM004) Project #: 4358-20-043A Phase 01 Logged In: 15-Oct-20 09:37 Logged By: John C King Preservation Check Performed By: Date/Time: /Oy -2b „// Y_'O C D16585-01 Cont Type B 250mLP+HNO3 C 250mLP+ZnAc+NaOH D 250mLP+H2SO4 CD16585-02 Pres (pH) pH Checked / PH Adjusted Requirement In Control <2 NINA YI INA >9 IN/NA YI INA <2 ININA Y//N INA .)aiei i ime I Reagent Used/Comments Adjusted Cont Type Pres (pH) Requirement PH Checked / In Control PH Adjusted DatelTime Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 I N I NA Y /(I I NA C 250mLP+ZnAc+NaOH >9 / N / NA Y I(A I NA D 250mLP+H2SO4 <2 1 N / NA Y /(f / NA CD16585-03 Cant Type yP Pres (PH) Requirement PH Checked/ In Control DatelTime PI t Adjusted Adiusted Reagent Used/Comments B 250mLP+HNO3 <2 f N / NA Y I � / NA C 250mLP+ZnAc+NaOH >9(/ N/ NA Y /&I 1 NA D 250mLP+H2SO4 <2 Y 1 N/ NA Y /(jV 1 NA I'`CD16585-04 Cont Type 8 250mLP+HNO3 C 250mLP+ZnAc+NaOH CD16585-05 s (PH) PH Checked f PH Adjusted iirement In Control <2 &/N/NA Y15 NA >9 /NINA Y/ INA CD16585-06 Cant Type Pres (PH) Requirement 13 250mLP+HNO3 <2 ;. C 250mLP+ZnAc+NaOH .g 1ELMNT1Printlwko_Preservation Check . rpt ra: In Control PH Adjusted /N/NA YI INA N I NA Y / (j I NA Adjusted I Reagent Used/Comments pater i tme Adjusted I Reagent Used/Comments Page 1 of 3 ample Preservation Verification NCO Carly Work Order: CD16585 Project: Moore County Active C & D LF Client: S&ME, Inc. (SM004) Project #: 4358-20-043A Phase 01 Logged In: 15-Oct-20 09:37 Logged By: John C King Preservation Check Performed By: RIQ Date/Time: 20 CD16585-07 Cont T pe y Pres (pH) Requirement pH Checked / In Control Date/Time PH Adjusted Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 1 N/ NA Y 1 / NA C 250mLP+ZnAc+NaOH >9 I N I NA Y I '1 NA CD16585-08 Cont Type yP Pres (pH) Requirement pH Checked / In Control Date/Time pH Adjusted Adjusted Reagent UsedlCorments LP+HNO3 <2 I N I NA Y IN I NA LP+ZnAc+NaOH >9 Y/ N I NA Y I / NA B 250m C 250m CD16585-09 Cont Type Yp Pres (pH) Requirement PH Checked/ In Control Date/Time PH Adjusted Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 I N l NA Y I 1 NA C 250mLP+ZnAc+NaOH >9 I N/ NA Y I I NA CD16585-10 Cont Type yp Pres (pH) Requirement pH Checked / In Control Date/Time PH Adjusted Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 Y 1 N/ NA Y I 1 NA C 250mLP+ZnAc+NaOH >9 I N/ NA Y I 1 NA CD16586-11 Cant yP Type Pres (pH) Requirement pH Checked/ In Control CatelTime PH Adjusted Adjusted Reagent Used/Cornments C 250mLA (PEST) Pest PH 5-9 / N / NA Y 1 / NA G 250mLP+HNO3 <2 / N / NA Y I / NA H 250mLP+ZnAc+NaOH >9 [� 1 N / NA Y / tl�t / NA I 250mLP+NaOH >12 IFJ/ N / NA Y / &// NA 10, CD16585-12 Cant Type Pres (pH) Requirement pH Checked / In Control pH Adjusted DateMme Adjusted Reagent Used/Comments 9 B 250mLP+HNO3 ,2 1 N/ NA Y 1 Io 1 NA C 250mLP+ZnAc+NaOH >5 Y), N/ NA Y/ I NA C:IELMNT1Printlwko_Preservation Check. rpt Page 2 of 3 Sample Preservation Verification ENCO Caiy Work Order: CD16585 Project: Client: S&.ME, Inc. (SM004) Project #: Logged In: 15-Oct-20 09:37 Logged By: Preservation Check Performed By: L Rea ent Name ID 1 2 pH Strip ID: M`(PH) quiretnent:-� pH Ghecked 1 .'. in.Contr<il : pN adjusted — <2 /N/NA _. Y INA >9 / N / NA Y / /NI / NA Rea ent Name ID 3 4 Moore County Active C & D LF 4358-20-043A Phase 01 John C King Date/Time: , ' Reagent Used/Comments Reagent Name ID 5 6 C:IELMNT1Printlwko_PreservationCheck. rpt Page 3 of 3 2�SQ pCCgF ENCO Laboratories 9e0 Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, November 6, 2020 S&ME, Inc. (SM004) Attn: Edmund Henriques 8646 West Market Street, Suite 105 Greensboro, NC 27409 RE: Laboratory Results for Project Number: 4358-20-043A Phase 01, Project Name/Desc: Moore County MSW LF CA ENCO Workorder(s): CD16586 Dear Edmund Henriques, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Thursday, October 15, 2020. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, 0"6LC'=-:;tA Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 53 PROJECT NARRATIVE Client: S&ME, Inc. (SM004) Project: Moore County MSW LF CA Lab ID: CD16586 (� �Eo www.encolabs.com Overview Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in the QC Remarks section below. Quality Control Samples The associated LCS exhibited high bias; since the result is ND, there is no impact (QL-02). The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on an aceptable LCS recovery (QM-07). Post -digestion spike did not meet method requirements due to confirmed matrix effects (QM-08). Precision between duplicate matrix spikes of the same sample was outside acceptance limits (QM-11). Precision between duplicate samples was outside acceptance limits (QM-12). Duplicate presision outside acceptance limits due to low analyte concentration (QR-04). Quality Control Remarks The associated CCV standard exhibited high bias; since the result is ND, there is no impact (QV-01). Other Comments The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of the report. Released By: Environmental Conservation Laboratories, Inc. Chuck Smith Project Manager FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 53 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW3 Lab ID: CD36586-01 Sampled: 10/14/20 15:45 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/11/20 10/21/20 11:28 10/21/20 16:46 EPA 310.2 NO PREP 10/28/20 10/20/20 13:40 10/20/20 15:55 EPA 353.2 NO PREP 10/16/20 15:45 10/15/20 15:34 10/15/20 17:19 EPA 353.2 [CALC] 10/16/20 15:45 10/26/20 09:33 10/26/20 12:50 EPA 353.2 NO PREP 11/11/20 10/26/20 09:33 10/26/20 12:50 EPA 6010D EPA 3005A 04/12/21 10/21/20 12:00 10/23/20 11:28 EPA 7470A EPA 7470A 11/11/20 10/21/20 16:34 10/23/20 16:42 EPA 8260D EPA 503013_MS 10/28/20 10/19/20 00:00 10/20/20 03:43 EPA 8260D EPA 503013_MS 10/28/20 10/23/20 13:57 10/26/20 07:34 EPA 9060A NA 11/11/20 10/23/20 12:30 10/23/20 12:59 RSK 175 Same 10/28/20 10/21/20 08:38 10/21/20 13:33 SM 4500S2 D-2011 NO PREP 10/21/20 10/20/20 13:21 10/20/20 16:38 Client ID: 6301-MW2 Lab ID: CD16586-02 Sampled: 10/14/20 17:15 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/11/20 10/21/20 11:28 10/21/20 17:03 EPA 310.2 NO PREP 10/28/20 10/20/20 13:40 10/20/20 15:56 EPA 353.2 NO PREP 10/16/20 17:15 10/15/20 15:34 10/15/20 17:20 EPA 353.2 [CALC] 10/16/20 17:15 10/26/20 09:33 10/26/20 12:55 EPA 353.2 NO PREP 11/11/20 10/26/20 09:33 10/26/20 12:55 EPA 6010D EPA 3005A 04/12/21 10/21/20 12:00 10/23/20 11:30 EPA 7470A EPA 7470A 11/11/20 10/21/20 16:34 10/23/20 16:44 EPA 8260D EPA 503013_MS 10/28/20 10/19/20 00:00 10/20/20 04:08 EPA 8260D EPA 503013_MS 10/28/20 10/23/20 13:57 10/26/20 08:02 EPA 9060A NA 11/11/20 10/23/20 12:30 10/23/20 12:59 RSK 175 Same 10/28/20 10/21/20 08:38 10/21/20 13:49 SM 4500S2 D-2011 NO PREP 10/21/20 10/20/20 13:21 10/20/20 16:38 Client ID: 6301-MW3 Lab ID: CD36586-03 Sampled: 10/14/20 08:35 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/11/20 10/21/20 11:28 10/21/20 17:21 EPA 310.2 NO PREP 10/28/20 10/20/20 13:40 10/20/20 15:57 EPA 353.2 NO PREP 10/16/20 08:35 10/15/20 15:34 10/15/20 17:21 EPA 353.2 [CALC] 10/16/20 08:35 10/26/20 09:33 10/26/20 12:57 EPA 353.2 NO PREP 11/11/20 10/26/20 09:33 10/26/20 12:57 EPA 6010D EPA 3005A 04/12/21 10/21/20 12:00 10/23/20 11:33 EPA 7470A EPA 7470A 11/11/20 10/21/20 16:34 10/23/20 16:47 EPA 8260D EPA 503013_MS 10/28/20 10/19/20 00:00 10/20/20 04:34 EPA 8260D EPA 503013_MS 10/28/20 10/23/20 13:57 10/26/20 08:30 EPA 9060A NA 11/11/20 10/23/20 12:30 10/23/20 12:59 RSK 175 Same 10/28/20 10/21/20 08:38 10/21/20 14:05 SM 4500S2 D-2011 NO PREP 10/21/20 10/20/20 13:21 10/20/20 16:38 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 53 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW6 Lab ID: CD36586-04 Sampled: 10/14/20 13:55 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/11/20 10/21/20 11:28 10/21/20 17:39 EPA 310.2 NO PREP 10/28/20 10/20/20 13:40 10/20/20 15:57 EPA 353.2 NO PREP 10/16/20 13:55 10/15/20 15:34 10/15/20 17:22 EPA 353.2 [CALC] 10/16/20 13:55 10/26/20 09:33 10/26/20 13:03 EPA 353.2 NO PREP 11/11/20 10/26/20 09:33 10/26/20 13:03 EPA 6010D EPA 3005A 04/12/21 10/21/20 12:23 10/23/20 11:37 EPA 7470A EPA 7470A 11/11/20 10/21/20 16:34 10/23/20 16:49 EPA 8260D EPA 503013_MS 10/28/20 10/19/20 00:00 10/20/20 04:59 EPA 8260D EPA 503013_MS 10/28/20 10/23/20 13:57 10/26/20 08:57 EPA 9060A NA 11/11/20 10/23/20 12:30 10/23/20 12:59 RSK 175 Same 10/28/20 10/21/20 08:38 10/21/20 14:20 SM 450052 D-2011 NO PREP 10/21/20 10/20/20 13:21 10/20/20 16:38 Client ID: 6301-MW7 Lab ID: CD16586-05 Sampled: 10/14/20 13:20 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/11/20 10/21/20 11:28 10/21/20 17:56 EPA 310.2 NO PREP 10/28/20 10/20/20 13:40 10/20/20 15:58 EPA 353.2 NO PREP 10/16/20 13:20 10/15/20 15:34 10/15/20 17:23 EPA 353.2 [CALC] 10/16/20 13:20 10/26/20 09:33 10/26/20 13:04 EPA 353.2 NO PREP 11/11/20 10/26/20 09:33 10/26/20 13:04 EPA 6010D EPA 3005A 04/12/21 10/21/20 12:23 10/23/20 13:05 EPA 7470A EPA 7470A 11/11/20 10/21/20 16:34 10/23/20 16:52 EPA 8260D EPA 503013_MS 10/28/20 10/19/20 00:00 10/20/20 05:24 EPA 8260D EPA 503013_MS 10/28/20 10/23/20 13:57 10/26/20 09:25 EPA 9060A NA 11/11/20 10/23/20 12:30 10/23/20 12:59 RSK 175 Same 10/28/20 10/21/20 08:38 10/21/20 15:08 SM 450052 D-2011 NO PREP 10/21/20 10/20/20 13:21 10/20/20 16:38 Client ID: 6301-MW7 Lab ID: CD36586-OSRE1 Sampled: 10/14/20 13:20 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 10/28/20 10/26/20 09:28 10/27/20 15:22 Client ID: 6301-MW8 Lab ID: CD36586-06 Sampled: 10/14/20 16:00 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/11/20 10/21/20 11:28 10/21/20 18:14 EPA 353.2 NO PREP 10/16/20 16:00 10/15/20 15:34 10/15/20 17:24 EPA 353.2 [CALC] 10/16/20 16:00 10/26/20 09:33 10/26/20 13:06 EPA 353.2 NO PREP 11/11/20 10/26/20 09:33 10/26/20 13:06 EPA 6010D EPA 3005A 04/12/21 10/21/20 12:23 10/23/20 13:07 EPA 7470A EPA 7470A 11/11/20 10/21/20 16:34 10/23/20 17:00 EPA 8260D EPA 503013_MS 10/28/20 10/19/20 00:00 10/20/20 05:49 EPA 8260D EPA 503013_MS 10/28/20 10/23/20 13:23 10/24/20 20:41 EPA 9060A NA 11/11/20 10/23/20 12:30 10/23/20 12:59 RSK 175 Same 10/28/20 10/21/20 08:38 10/21/20 15:24 SM 450052 D-2011 NO PREP 10/21/20 10/20/20 13:21 10/20/20 16:38 Client ID: 6301-MW8 Lab ID: CD36586-06RE1 Sampled: 10/14/20 16:00 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 310.2 NO PREP 10/28/20 10/20/20 13:40 10/20/20 16:14 EPA 8260D EPA 503013_MS 10/28/20 10/26/20 14:06 10/26/20 20:53 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 53 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 6301-MW9 Lab ID: CD36586-07 Sampled: 10/14/20 17:30 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/11/20 10/21/20 11:28 10/21/20 19:07 EPA 353.2 NO PREP 10/16/20 17:30 10/15/20 15:34 10/15/20 17:26 EPA 353.2 [CALC] 10/16/20 17:30 10/26/20 09:33 10/26/20 13:08 EPA 353.2 NO PREP 11/11/20 10/26/20 09:33 10/26/20 13:08 EPA 6010D EPA 3005A 04/12/21 10/21/20 12:23 10/23/20 13:09 EPA 7470A EPA 7470A 11/11/20 10/21/20 16:34 10/23/20 17:02 EPA 8260D EPA 5030B_MIS 10/28/20 10/19/20 00:00 10/20/20 06:15 EPA 8260D EPA 503013_MS 10/28/20 10/23/20 13:23 10/24/20 21:09 EPA 9060A NA 11/11/20 10/23/20 12:30 10/23/20 12:59 RSK 175 Same 10/28/20 10/21/20 08:38 10/21/20 15:40 SM 4500S2 D-2011 NO PREP 10/21/20 10/20/20 13:21 10/20/20 16:38 Client ID: 6301-MW9 Lab ID: CD16586-07RE1 Sampled: 10/14/20 17:30 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/11/20 10/23/20 11:01 10/23/20 13:05 Client ID: 6301-MW9 Lab ID: CD36586-07RE2 Sampled: 10/14/20 17:30 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 310.2 NO PREP 10/28/20 10/23/20 11:23 10/23/20 12:56 Client ID: 6301-MW15R Lab ID: CD36586-08 Sampled: 10/14/20 11:45 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 11/11/20 10/21/20 11:28 10/21/20 19:25 EPA 310.2 NO PREP 10/28/20 10/20/20 13:40 10/20/20 16:01 EPA 353.2 NO PREP 10/16/20 11:45 10/15/20 15:34 10/15/20 17:27 EPA 353.2 [CALC] 10/16/20 11:45 10/26/20 09:33 10/26/20 13:10 EPA 353.2 NO PREP 11/11/20 10/26/20 09:33 10/26/20 13:10 EPA 6010D EPA 3005A 04/12/21 10/21/20 12:23 10/23/20 13:12 EPA 7470A EPA 7470A 11/11/20 10/21/20 16:34 10/23/20 17:05 EPA 8260D EPA 503013_MS 10/28/20 10/19/20 00:00 10/20/20 06:40 EPA 8260D EPA 503013_MS 10/28/20 10/23/20 13:23 10/24/20 21:37 RSK 175 Same 10/28/20 10/22/20 07:52 10/22/20 10:00 SM 4500S2 D-2011 NO PREP 10/21/20 10/20/20 13:21 10/20/20 16:38 Client ID: 6301-MW15R Lab ID: CD36586-08RE1 Sampled: 10/14/20 11:45 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 9060A NA 11/11/20 10/23/20 12:30 10/27/20 11:08 Client ID: 6301-TRIPBLANK Lab ID: CD36586-09 Sampled: 10/14/20 08:35 Received: 10/15/20 08:19 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 10/28/20 10/19/20 00:00 10/20/20 07:05 EPA 8260D EPA 503013_MS 10/28/20 10/23/20 13:23 10/24/20 14:09 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 53 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MW3 Lab ID: CD16586-01 Analvte Results Flag MDL PQL Units Method Notes Barium - Total 26.7 1.10 10.0 ug/L EPA 6010D Carbon dioxide 55.7 2.07 2.50 mg/L RSK 175 Chloride 2.3 3 2.2 5.0 mg/L EPA 300.0 Nitrate as N 0.85 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.85 0.041 0.10 mg/L EPA 353.2 Sulfate as SO4 8.0 2.9 5.0 mg/L EPA 300.0 Total Organic Carbon 0.99 1 0.54 1.0 mg/L EPA 9060A Client ID: 6301-MW2 Lab ID: CD16586-02 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dichlorobenzene 0.59 3 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 9.7 0.80 2.0 ug/L EPA 8260D Barium - Total 34.7 1.10 10.0 ug/L EPA 6010D Benzene 0.54 3 0.15 1.0 ug/L EPA 8260D Carbon dioxide 5.24 2.07 2.50 mg/L RSK 175 Chloride 38 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 1.2 0.17 1.0 ug/L EPA 8260D Nitrate as N 0.13 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.13 0.041 0.10 mg/L EPA 353.2 Sulfate as SO4 5.5 2.9 5.0 mg/L EPA 300.0 Total Alkalinity as CaCO3 180 14 15 mg/L EPA 310.2 Total Organic Carbon 5.3 0.54 1.0 mg/L EPA 9060A Client ID: 6301-MW3 Lab ID: CD16586-03 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 1.0 1 0.80 2.0 ug/L EPA 8260D Barium - Total 33.9 1.10 10.0 ug/L EPA 6010D Carbon dioxide 47.5 2.07 2.50 mg/L RSK 175 Chloride 5.5 2.2 5.0 mg/L EPA 300.0 Sulfate as SO4 8.4 2.9 5.0 mg/L EPA 300.0 Total Organic Carbon 0.93 3 0.54 1.0 mg/L EPA 9060A Client ID: 6301-MW6 Lab ID: CD16586-04 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dichlorobenzene 1.7 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 2.0 0.80 2.0 ug/L EPA 8260D Barium - Total 41.0 1.10 10.0 ug/L EPA 6010D Benzene 2.5 0.15 1.0 ug/L EPA 8260D Cadmium - Total 2.16 0.360 1.00 ug/L EPA 6010D Carbon dioxide 429 D 43.5 52.5 mg/L RSK 175 Chloride 13 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 1.6 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 3.1 0.15 1.0 ug/L EPA 8260D Lead - Total 9.32 3 3.10 10.0 ug/L EPA 6010D Methane 4.28 D 0.0840 0.105 mg/L RSK 175 Nitrate as N 0.11 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.11 0.041 0.10 mg/L EPA 353.2 Sulfate as SO4 7.2 2.9 5.0 mg/L EPA 300.0 Sulfide 0.16 0.010 0.10 mg/L SM 4500S2 D-2011 Toluene 0.40 3 0.14 1.0 ug/L EPA 8260D Total Alkalinity as CaCO3 190 14 15 mg/L EPA 310.2 Total Organic Carbon 30 0.54 1.0 mg/L EPA 9060A Vinyl chloride 1.1 0.32 1.0 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 53 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MW7 Lab ID: CD16586-05 Analvte Results Flag MDL Q Units Method Notes 1,4-Dioxane 6.9 0.80 2.0 ug/L EPA 8260D Barium - Total 34.4 1.10 10.0 ug/L EPA 6010D Cadmium - Total 1.57 0.360 1.00 ug/L EPA 6010D Carbon dioxide 406 D 43.5 52.5 mg/L RSK 175 Chloride 20 2.2 5.0 mg/L EPA 300.0 Lead - Total 10.9 3.10 10.0 ug/L EPA 6010D Methane 3.68 D 0.0840 0.105 mg/L RSK 175 Nitrate as N 0.20 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.20 0.041 0.10 mg/L EPA 353.2 Sulfide 0.19 0.010 0.10 mg/L SM 4500S2 D-2011 Total Alkalinity as CaCO3 120 14 15 mg/L EPA 310.2 Total Organic Carbon 21 0.54 1.0 mg/L EPA 9060A Client ID: 6301-MW7 Lab ID: CD36586-05RE3 Analvte Results Flag MDL PQL Units Method Notes Acetone 490 D 50 100 ug/L EPA 8260D cis-1,2-Dichloroethene 7.8 D 0.75 5.0 ug/L EPA 8260D Vinyl chloride 5.4 D 1.6 5.0 ug/L EPA 8260D Client ID: 6301-MW8 Lab ID: CD16586-06 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dioxane 29 0.80 2.0 ug/L EPA 8260D Barium - Total 75.6 1.10 10.0 ug/L EPA 6010D Cadmium - Total 1.67 0.360 1.00 ug/L EPA 6010D Carbon dioxide 462 D 43.5 52.5 mg/L RSK 175 Chloride 69 2.2 5.0 mg/L EPA 300.0 Lead - Total 9.86 3 3.10 10.0 ug/L EPA 6010D Methane 6.15 D 0.0840 0.105 mg/L RSK 175 Nitrate as N 0.12 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.12 0.041 0.10 mg/L EPA 353.2 Sulfide 0.078 3 0.010 0.10 mg/L SM 4500S2 D-2011 Total Organic Carbon 21 0.54 1.0 mg/L EPA 9060A Client ID: 6301-MW8 Lab ID: CD36586-06RE3 Analvte Results Flag MDL PQL Units Method Notes 1,1-Dichloroethane 0.56 1 0.13 1.0 ug/L EPA 8260D 1,2-Dichlorobenzene 0.54 3 0.19 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 5.3 0.19 1.0 ug/L EPA 8260D Benzene 2.8 0.15 1.0 ug/L EPA 8260D Chlorobenzene 4.3 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 0.43 3 0.15 1.0 ug/L EPA 8260D Toluene 0.51 3 0.14 1.0 ug/L EPA 8260D Total Alkalinity as CaCO3 240 D 28 30 mg/L EPA 310.2 Xylenes (Total) 2.2 3 0.45 3.0 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 53 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 6301-MW9 Lab ID: CD16586-07 Analvte Results Flag MDL Q Units Method Notes 1,4-Dichlorobenzene 3.1 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 25 0.80 2.0 ug/L EPA 8260D Arsenic - Total 64.8 7.60 10.0 ug/L EPA 6010D Barium - Total 95.5 1.10 10.0 ug/L EPA 6010D Benzene 4.0 0.15 1.0 ug/L EPA 8260D Cadmium - Total 0.662 3 0.360 1.00 ug/L EPA 6010D Carbon dioxide 729 D 43.5 52.5 mg/L RSK 175 Chlorobenzene 8.9 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 0.74 3 0.15 1.0 ug/L EPA 8260D Lead - Total 6.58 3 3.10 10.0 ug/L EPA 6010D Methane 5.68 D 0.0840 0.105 mg/L RSK 175 Nitrate as N 0.10 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.10 0.041 0.10 mg/L EPA 353.2 Sulfide 0.14 0.010 0.10 mg/L SM 4500S2 D-2011 Toluene 0.43 3 0.14 1.0 ug/L EPA 8260D Total Organic Carbon 37 0.54 1.0 mg/L EPA 9060A Xylenes (Total) 0.46 1 0.45 3.0 ug/L EPA 8260D Client ID: 6301-MW9 Lab ID: CD36586-07RE3 Analvte Results Flag MDL PQL Units Method Notes Chloride 100 D 4.4 10 mg/L EPA 300.0 Client ID: 6301-MW9 Lab ID: CD36586-07RE2 Analvte Results Flag MDL PQL Units Method Notes Total Alkalinity as CaCO3 830 D 70 75 mg/L EPA 310.2 Client ID: 6301-MW15R Lab ID: CD16586-08 Analvte Results Flag MDL PQL Units Method Notes 1,4-Dichlorobenzene 0.73 3 0.19 1.0 ug/L EPA 8260D Barium - Total 27.5 1.10 10.0 ug/L EPA 6010D Benzene 1.2 0.15 1.0 ug/L EPA 8260D Cadmium - Total 1.92 0.360 1.00 ug/L EPA 6010D Carbon dioxide 425 D 43.5 52.5 mg/L RSK 175 Chloride 2.9 3 2.2 5.0 mg/L EPA 300.0 Chlorobenzene 0.56 3 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 1.6 0.15 1.0 ug/L EPA 8260D Lead - Total 9.94 3 3.10 10.0 ug/L EPA 6010D Methane 3.20 D 0.0840 0.105 mg/L RSK 175 Nitrate as N 0.51 0.041 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.51 0.041 0.10 mg/L EPA 353.2 Sulfate as SO4 7.2 2.9 5.0 mg/L EPA 300.0 Sulfide 0.027 3 0.010 0.10 mg/L SM 4500S2 D-2011 Total Alkalinity as CaCO3 96 14 15 mg/L EPA 310.2 Vinyl chloride 1.1 0.32 1.0 ug/L EPA 8260D Client ID: 6301-MW15R Lab ID: CD16586-08RE3 Analvte Results Flag MDL PQL Units Method Notes Total Organic Carbon 2.6 0.54 1.0 mg/L EPA 9060A FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 53 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW1 Lab Sample ID:CD16586-01 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 15:45 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 07:34 REF 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 0123024 EPA 8260D 10/26/20 07:34 REF 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 0123024 EPA 8260D 10/26/20 07:34 REF 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 07:34 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 07:34 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 07:34 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 07:34 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 0123024 EPA 8260D 10/26/20 07:34 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 0123024 EPA 8260D 10/26/20 07:34 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 0123024 EPA 8260D 10/26/20 07:34 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 07:34 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 0123024 EPA 8260D 10/26/20 07:34 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 0123024 EPA 8260D 10/26/20 07:34 REF 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 0123024 EPA 8260D 10/26/20 07:34 REF 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 0123024 EPA 8260D 10/26/20 07:34 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 0123024 EPA 8260D 10/26/20 07:34 REF Acetone [67-64- 1]A 10 U ug/L 1 10 20 0123024 EPA 8260D 10/26/20 07:34 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 0123024 EPA 8260D 10/26/20 07:34 REF Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 07:34 REF Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 0123024 EPA 8260D 10/26/20 07:34 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 07:34 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 0123024 EPA 8260D 10/26/20 07:34 REF QV-01 Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 07:34 REF Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 0123024 EPA 8260D 10/26/20 07:34 REF Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 07:34 REF Chlorobenzene[108-90-7]A 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 07:34 REF Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 07:34 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 0123024 EPA 8260D 10/26/20 07:34 REF Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 07:34 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 07:34 REF cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 0123024 EPA 8260D 10/26/20 07:34 REF Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 07:34 REF Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 0123024 EPA 8260D 10/26/20 07:34 REF Ethylbenzene [500-41-4]A 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 07:34 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 0123024 EPA 8260D 10/26/20 07:34 REF Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 07:34 REF Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 0123024 EPA 8260D 10/26/20 07:34 REF Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 07:34 REF Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 0123024 EPA 8260D 10/26/20 07:34 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 07:34 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 07:34 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 07:34 REF trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 0123024 EPA 8260D 10/26/20 07:34 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 07:34 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 0123024 EPA 8260D 10/26/20 07:34 REF Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 0123024 EPA 8260D 10/26/20 07:34 REF Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 0123024 EPA 8260D 10/26/20 07:34 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 53 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW1 Lab Sample ID:CD16586-01 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 15:45 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 OJ23024 EPA 8260D 10/26/20 07:34 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 44 1 50.0 89 % 53-136 OJ23024 EPA 6260D 10126120 0734 REF Dibromofluoromethane 50 1 50.0 99 % 67-129 OJ23024 EPA 6260D 10126120 0734 REF Toluene-& 51 1 50.0 102 % 59-134 OJ23024 EPA 6260D 10126120 0734 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 OJ21046 EPA 7470A 10/23/20 16:42 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 OJ21028 EPA 6010D 10/23/20 11:28 JDH Barium [7440-39-3]^ 26.7 ug/L 1 1.10 10.0 0121028 EPA 6010D 10/23/20 11:28 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 OJ21028 EPA 6010D 10/23/20 11:28 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 OJ21028 EPA 6010D 10/23/20 11:28 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 OJ21028 EPA 6010D 10/23/20 11:28 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 OJ21028 EPA 6010D 10/23/20 11:28 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 OJ21028 EPA 6010D 10/23/20 11:28 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 2.3 J mg/L 1 2.2 5.0 0121014 EPA 300.0 10/21/20 16:46 LJI Nitrate as N [14797-55-8] 0.85 mg/L 1 0.041 0.10 [CALC] EPA 353.2 10/26/20 12:50 JAH Nitrate/Nitrite as N^ 0.85 mg/L 1 0.041 0.10 0126013 EPA 353.2 10/26/20 12:50 JAH Nitrite as N [14797-65-O]^ 0.017 U mg/L 1 0.017 0.10 OJ15042 EPA 353.2 10/15/20 17:19 JAH Sulfate as SO4 [14808-79-B]^ 8.0 mg/L 1 2.9 5.0 0121014 EPA 300.0 10/21/20 16:46 LJI Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 OJ20016 iM 450OS2 D-2011 10/20/20 16:38 JOC Total Alkalinity as CaCO3 [471-34-1]^ 14 U mg/L 1 14 15 OJ20019 EPA 310.2 10/20/20 15:55 JAH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 0J19034 EPA 8260D 10/20/20 03:43 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.5 1 5.00 110 % 75-125 0J19034 EPA 8260D 10120120 03:43 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 53 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW1 Lab Sample ID:CD16586-01 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 15:45 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 55.7 mg/L 1 2.07 2.50 0321005 RSK 175 10/21/20 13:33 KG Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 OJ21005 RSK 175 10/21/20 13:33 KG Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 OJ21005 RSK 175 10/21/20 13:33 KG Methane [74-82-8] 0.00400 U mg/L 1 0.00400 0.00500 OJ21005 RSK 175 10/21/20 13:33 KG Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 0.99 J mg/L 1 0.54 1.0 0322067 EPA 9060A 10/23/20 12:59 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 53 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW2 Lab Sample ID:CD16586-02 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 17:15 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 08:02 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 0123024 EPA 8260D 10/26/20 08:02 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 0123024 EPA 8260D 10/26/20 08:02 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 08:02 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 08:02 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 08:02 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 08:02 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 0123024 EPA 8260D 10/26/20 08:02 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 0123024 EPA 8260D 10/26/20 08:02 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 0123024 EPA 8260D 10/26/20 08:02 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 08:02 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 0123024 EPA 8260D 10/26/20 08:02 REF 1,4-Dichlorobenzene [306-46-7]^ 0.59 J ug/L 1 0.19 1.0 0123024 EPA 8260D 10/26/20 08:02 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 0123024 EPA 8260D 10/26/20 08:02 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 0123024 EPA 8260D 10/26/20 08:02 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 0123024 EPA 8260D 10/26/20 08:02 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 0123024 EPA 8260D 10/26/20 08:02 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 0123024 EPA 8260D 10/26/20 08:02 REF Benzene [71-43-2]A 0.54 J ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 08:02 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 0123024 EPA 8260D 10/26/20 08:02 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 08:02 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 0123024 EPA 8260D 10/26/20 08:02 REF QV-01 Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 08:02 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 0123024 EPA 8260D 10/26/20 08:02 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 08:02 REF Chlorobenzene [308-90-7]A 1.2 ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 08:02 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 08:02 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 0123024 EPA 8260D 10/26/20 08:02 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 08:02 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 08:02 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 0123024 EPA 8260D 10/26/20 08:02 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 08:02 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 0123024 EPA 8260D 10/26/20 08:02 REF Ethylbenzene [500-41-4]^ 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 08:02 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 0123024 EPA 8260D 10/26/20 08:02 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 08:02 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 0123024 EPA 8260D 10/26/20 08:02 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 08:02 REF Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 0123024 EPA 8260D 10/26/20 08:02 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 08:02 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 08:02 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 08:02 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 0123024 EPA 8260D 10/26/20 08:02 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 08:02 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 0123024 EPA 8260D 10/26/20 08:02 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 0123024 EPA 8260D 10/26/20 08:02 REF Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 0123024 EPA 8260D 10/26/20 08:02 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 53 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW2 Lab Sample ID:CD16586-02 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 17:15 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 OJ23024 EPA 8260D 10/26/20 08:02 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 44 1 50.0 87 % 53-136 OJ23024 EPA 626OD 10126120 08:02 REF Dibromofluoromethane 49 1 50.0 98 % 67-129 OJ23024 EPA 626OD 10126120 08:02 REF Toluene-& 51 1 50.0 102 % 59-134 OJ23024 EPA 626OD 10126120 08:02 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 OJ21046 EPA 7470A 10/23/20 16:44 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 OJ21028 EPA 6010D 10/23/20 11:30 JDH Barium [7440-39-3]^ 34.7 ug/L 1 1.10 10.0 O121028 EPA 6010D 10/23/20 11:30 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 OJ21028 EPA 6010D 10/23/20 11:30 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 OJ21028 EPA 6010D 10/23/20 11:30 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 OJ21028 EPA 6010D 10/23/20 11:30 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 OJ21028 EPA 6010D 10/23/20 11:30 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 OJ21028 EPA 6010D 10/23/20 11:30 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 38 mg/L 1 2.2 5.0 O121014 EPA 300.0 10/21/20 17:03 LJI Nitrate as N [14797-55-8] 0.13 mg/L 1 0.041 0.10 [CALC] EPA 353.2 10/26/20 12:55 JAH Nitrate/Nitrite as N^ 0.13 mg/L 1 0.041 0.10 O126013 EPA 353.2 10/26/20 12:55 JAH Nitrite as N [14797-65-O]^ 0.017 U mg/L 1 0.017 0.10 OJ15042 EPA 353.2 10/15/20 17:20 JAH Sulfate as SO4 [14808-79-8]^ 5.5 mg/L 1 2.9 5.0 O121014 EPA 300.0 10/21/20 17:03 LJI Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 OJ20016 iM 450052 D-2011 10/20/20 16:38 JOC Total Alkalinity as CaCO3 [471-34-1]^ 180 mg/L 1 14 15 O120019 EPA 310.2 10/20/20 15:56 JAH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 9.7 ug/L 1 0.80 2.0 O119034 EPA 8260D 10/20/20 04:08 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.5 1 5.00 110 % 75-125 0J19034 EPA 826OD 10120120 04:08 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 53 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW2 Lab Sample ID:CD16586-02 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 17:15 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 5.24 mg/L 1 2.07 2.50 0321005 RSK 175 10/21/20 13:49 KG Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 OJ21005 RSK 175 10/21/20 13:49 KG Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 OJ21005 RSK 175 10/21/20 13:49 KG Methane [74-82-8] 0.00400 U mg/L 1 0.00400 0.00500 OJ21005 RSK 175 10/21/20 13:49 KG Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 5.3 mg/L 1 0.54 1.0 0322067 EPA 9060A 10/23/20 12:59 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 53 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW3 Lab Sample ID:CD16586-03 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 08:35 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 08:30 REF 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 0123024 EPA 8260D 10/26/20 08:30 REF 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 0123024 EPA 8260D 10/26/20 08:30 REF 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 08:30 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 08:30 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 08:30 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 08:30 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 0123024 EPA 8260D 10/26/20 08:30 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 0123024 EPA 8260D 10/26/20 08:30 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 0123024 EPA 8260D 10/26/20 08:30 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 08:30 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 0123024 EPA 8260D 10/26/20 08:30 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 0123024 EPA 8260D 10/26/20 08:30 REF 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 0123024 EPA 8260D 10/26/20 08:30 REF 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 0123024 EPA 8260D 10/26/20 08:30 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 0123024 EPA 8260D 10/26/20 08:30 REF Acetone [67-64- 1]A 10 U ug/L 1 10 20 0123024 EPA 8260D 10/26/20 08:30 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 0123024 EPA 8260D 10/26/20 08:30 REF Benzene[71-43-2]A 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 08:30 REF Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 0123024 EPA 8260D 10/26/20 08:30 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 08:30 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 0123024 EPA 8260D 10/26/20 08:30 REF QV-01 Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 08:30 REF Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 0123024 EPA 8260D 10/26/20 08:30 REF Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 08:30 REF Chlorobenzene[108-90-7]A 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 08:30 REF Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 08:30 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 0123024 EPA 8260D 10/26/20 08:30 REF Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 08:30 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 08:30 REF cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 0123024 EPA 8260D 10/26/20 08:30 REF Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 08:30 REF Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 0123024 EPA 8260D 10/26/20 08:30 REF Ethylbenzene [500-41-4]A 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 08:30 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 0123024 EPA 8260D 10/26/20 08:30 REF Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 08:30 REF Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 0123024 EPA 8260D 10/26/20 08:30 REF Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 08:30 REF Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 0123024 EPA 8260D 10/26/20 08:30 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 08:30 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 08:30 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 08:30 REF trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 0123024 EPA 8260D 10/26/20 08:30 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 08:30 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 0123024 EPA 8260D 10/26/20 08:30 REF Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 0123024 EPA 8260D 10/26/20 08:30 REF Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 0123024 EPA 8260D 10/26/20 08:30 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 53 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW3 Lab Sample ID:CD16586-03 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 08:35 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 OJ23024 EPA 8260D 10/26/20 08:30 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 44 1 50.0 88 % 53-136 OJ23024 EPA 626OD 10126120 08:30 REF Dibromofluoromethane 50 1 50.0 100 % 67-129 OJ23024 EPA 626OD 10126120 08:30 REF Toluene-c48 50 1 50.0 100 % 59-134 OJ23024 EPA 626OD 10126120 08:30 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 OJ21046 EPA 7470A 10/23/20 16:47 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 OJ21028 EPA 6010D 10/23/20 11:33 JDH Barium [7440-39-3]^ 33.9 ug/L 1 1.10 10.0 O121028 EPA 6010D 10/23/20 11:33 JDH Cadmium [7440-43-9]^ 0.360 U ug/L 1 0.360 1.00 OJ21028 EPA 6010D 10/23/20 11:33 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 OJ21028 EPA 6010D 10/23/20 11:33 JDH Lead [7439-92-1]^ 3.10 U ug/L 1 3.10 10.0 OJ21028 EPA 6010D 10/23/20 11:33 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 OJ21028 EPA 6010D 10/23/20 11:33 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 OJ21028 EPA 6010D 10/23/20 11:33 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 5.5 mg/L 1 2.2 5.0 O121014 EPA 300.0 10/21/20 17:21 LJI Nitrate as N [14797-55-8] 0.041 U mg/L 1 0.041 0.10 [CALC] EPA 353.2 1O/26/20 12:57 JAH Nitrate/Nitrite as N^ 0.041 U mg/L 1 0.041 0.10 OJ26013 EPA 353.2 10/26/20 12:57 JAH Nitrite as N [14797-65-O]^ 0.017 U mg/L 1 0.017 0.10 OJ15042 EPA 353.2 10/15/20 17:21 JAH Sulfate as SO4 [14808-79-8]^ 8.4 mg/L 1 2.9 5.0 O121014 EPA 300.0 10/21/20 17:21 LJI Sulfide [18496-25-8]^ 0.010 U mg/L 1 0.010 0.10 OJ20016 iM 450052 D-2011 10/20/20 16:38 JOC Total Alkalinity as CaCO3 [471-34-1]^ 14 U mg/L 1 14 15 OJ20019 EPA 310.2 1O/20/20 15:57 JAH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.0 J ug/L 1 0.80 2.0 O119034 EPA 8260D 10/20/20 04:34 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.2 1 5.00 104 % 75-125 0J19034 EPA 826OD 10120120 0424 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 53 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW3 Lab Sample ID:CD16586-03 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 08:35 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 47.5 mg/L 1 2.07 2.50 0321005 RSK 175 10/21/20 14:05 KG Ethane [74-84-0] 0.00510 U mg/L 1 0.00510 0.00600 OJ21005 RSK 175 10/21/20 14:05 KG Ethene [74-85-1] 0.00510 U mg/L 1 0.00510 0.00600 OJ21005 RSK 175 10/21/20 14:05 KG Methane [74-82-8] 0.00400 U mg/L 1 0.00400 0.00500 OJ21005 RSK 175 10/21/20 14:05 KG Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 0.93 J mg/L 1 0.54 1.0 0322067 EPA 9060A 10/23/20 12:59 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 53 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW6 Lab Sample ID:CD16586-04 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 13:55 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 08:57 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 0123024 EPA 8260D 10/26/20 08:57 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 0123024 EPA 8260D 10/26/20 08:57 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 08:57 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 08:57 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 08:57 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 08:57 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 0123024 EPA 8260D 10/26/20 08:57 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 0123024 EPA 8260D 10/26/20 08:57 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 0123024 EPA 8260D 10/26/20 08:57 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 08:57 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 0123024 EPA 8260D 10/26/20 08:57 REF 1,4-Dichlorobenzene [306-46-7]^ 1.7 ug/L 1 0.19 1.0 0123024 EPA 8260D 10/26/20 08:57 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 0123024 EPA 8260D 10/26/20 08:57 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 0123024 EPA 8260D 10/26/20 08:57 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 0123024 EPA 8260D 10/26/20 08:57 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 0123024 EPA 8260D 10/26/20 08:57 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 0123024 EPA 8260D 10/26/20 08:57 REF Benzene [71-43-2]A 2.5 ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 08:57 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 0123024 EPA 8260D 10/26/20 08:57 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 08:57 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 0123024 EPA 8260D 10/26/20 08:57 REF QV-01 Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 08:57 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 0123024 EPA 8260D 10/26/20 08:57 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 08:57 REF Chlorobenzene [308-90-7]^ 1.6 ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 08:57 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 08:57 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 0123024 EPA 8260D 10/26/20 08:57 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 08:57 REF cis-1,2-Dichloroethene [156-59-2]^ 3.1 ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 08:57 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 0123024 EPA 8260D 10/26/20 08:57 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 08:57 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 0123024 EPA 8260D 10/26/20 08:57 REF Ethylbenzene [500-41-4]^ 0.13 U ug/L 1 0.13 1.0 0123024 EPA 8260D 10/26/20 08:57 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 0123024 EPA 8260D 10/26/20 08:57 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 0123024 EPA 8260D 10/26/20 08:57 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 0123024 EPA 8260D 10/26/20 08:57 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 0123024 EPA 8260D 10/26/20 08:57 REF Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 0123024 EPA 8260D 10/26/20 08:57 REF Toluene [108-88-3]^ 0.40 J ug/L 1 0.14 1.0 0123024 EPA 8260D 10/26/20 08:57 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 0123024 EPA 8260D 10/26/20 08:57 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 08:57 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 0123024 EPA 8260D 10/26/20 08:57 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 0123024 EPA 8260D 10/26/20 08:57 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 0123024 EPA 8260D 10/26/20 08:57 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 0123024 EPA 8260D 10/26/20 08:57 REF Vinyl chloride [75-01-4]^ 1.1 ug/L 1 0.32 1.0 0123024 EPA 8260D 10/26/20 08:57 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 53 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW6 Lab Sample ID:CD16586-04 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 13:55 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 OJ23024 EPA 8260D 10/26/20 08:57 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 43 1 50.0 86 % 53-136 OJ23024 EPA 626OD 10126120 08:57 REF Dibromofluoromethane 48 1 50.0 96 % 67-129 OJ23024 EPA 626OD 10126120 08:57 REF Toluene-& 50 1 50.0 100 % 59-134 0723024 EPA 626OD 10126120 08:57 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 OJ21046 EPA 7470A 10/23/20 16:49 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 OJ21030 EPA 6010D 10/23/20 11:37 JDH Barium [7440-39-3]^ 41.0 ug/L 1 1.10 10.0 O121030 EPA 6010D 10/23/20 11:37 JDH Cadmium [7440-43-9]^ 2.16 ug/L 1 0.360 1.00 O121030 EPA 6010D 10/23/20 11:37 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 OJ21030 EPA 6010D 10/23/20 11:37 JDH Lead [7439-92-1]^ 9.32 J ug/L 1 3.10 10.0 O121030 EPA 6010D 10/23/20 11:37 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 OJ21030 EPA 6010D 10/23/20 11:37 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 OJ21030 EPA 6010D 10/23/20 11:37 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 13 mg/L 1 2.2 5.0 O121014 EPA 300.0 10/21/20 17:39 LJI Nitrate as N [14797-55-8] 0.11 mg/L 1 0.041 0.10 [CALC] EPA 353.2 10/26/20 13:03 JAH Nitrate/Nitrite as N^ 0.11 mg/L 1 0.041 0.10 O126013 EPA 353.2 10/26/20 13:03 JAH Nitrite as N [14797-65-O]^ 0.017 U mg/L 1 0.017 0.10 OJ15042 EPA 353.2 10/15/20 17:22 JAH Sulfate as SO4 [14808-79-8]^ 7.2 mg/L 1 2.9 5.0 O121014 EPA 300.0 10/21/20 17:39 LJI Sulfide [18496-25-8]^ 0.16 mg/L 1 0.010 0.10 O120016 iM 450052 D-2011 10/20/20 16:38 JOC Total Alkalinity as CaCO3 [471-34-1]^ 190 mg/L 1 14 15 O120019 EPA 310.2 1O/20/20 15:57 JAH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 2.0 ug/L 1 0.80 2.0 O119034 EPA 8260D 10/20/20 04:59 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.2 1 5.00 103 % 75-125 0J19034 EPA 826OD 10120120 04:59 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 53 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW6 Lab Sample ID:CD16586-04 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 13:55 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 429 D mg/L 21 43.5 52.5 0321005 RSK 175 10/21/20 14:20 KG Ethane [74-84-0] 0.107 UD mg/L 21 0.107 0.126 OJ21005 RSK 175 10/21/20 14:20 KG Ethene [74-85-1] 0.107 UD mg/L 21 0.107 0.126 OJ21005 RSK 175 10/21/20 14:20 KG Methane [74-82-8] 4.28 D mg/L 21 0.0840 0.105 0321005 RSK 175 10/21/20 14:20 KG Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MOIL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 30 mg/L 1 0.54 1.0 0322067 EPA 9060A 10/23/20 12:59 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 53 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW7 Lab Sample ID:CD16586-05 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 13:20 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.85 UD ug/L 5 0.85 5.0 O126036 EPA 8260D 10/27/20 15:22 REF 1,1,1-Trichloroethane [71-55-6]^ 0.60 UD ug/L 5 0.60 5.0 O126036 EPA 8260D 10/27/20 15:22 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 1.4 UD ug/L 5 1.4 5.0 O126036 EPA 8260D 10/27/20 15:22 REF 1,1,2-Trichloroethane [79-00-5]^ 0.70 UD ug/L 5 0.70 5.0 O126036 EPA 8260D 10/27/20 15:22 REF 1,1-Dichloroethane [75-34-3]^ 0.65 UD ug/L 5 0.65 5.0 O126036 EPA 8260D 10/27/20 15:22 REF 1,1-Dichloroethene [75-35-4]^ 1.0 UD ug/L 5 1.0 5.0 O126036 EPA 8260D 10/27/20 15:22 REF 1,2,3-Trichloropropane [96-18-4]^ 1.2 UD ug/L 5 1.2 5.0 O126036 EPA 8260D 10/27/20 15:22 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 2.4 UD ug/L 5 2.4 5.0 O126036 EPA 8260D 10/27/20 15:22 REF 1,2-Dibromoethane [106-93-4]^ 3.3 UD ug/L 5 3.3 5.0 O126036 EPA 8260D 10/27/20 15:22 REF 1,2-Dichlorobenzene [95-50-1]^ 0.95 UD ug/L 5 0.95 5.0 O126036 EPA 8260D 10/27/20 15:22 REF 1,2-Dichloroethane [107-06-2]^ 1.0 UD ug/L 5 1.0 5.0 O126036 EPA 8260D 10/27/20 15:22 REF 1,2-Dichloropropane [78-87-5]^ 0.50 UD ug/L 5 0.50 5.0 O126036 EPA 8260D 10/27/20 15:22 REF 1,4-Dichlorobenzene [106-46-7]^ 0.95 UD ug/L 5 0.95 5.0 O126036 EPA 8260D 10/27/20 15:22 REF 2-Butanone [78-93-3]^ 6.5 UD ug/L 5 6.5 25 O126036 EPA 8260D 10/27/20 15:22 REF 2-Hexanone [591-78-6]^ 4.4 UD ug/L 5 4.4 25 O126036 EPA 8260D 10/27/20 15:22 REF 4-Methyl-2-pentanone [108-10-1]^ 5.5 UD ug/L 5 5.5 25 O126036 EPA 8260D 10/27/20 15:22 REF Acetone [67-64-1]^ 490 D ug/L 5 50 100 O126036 EPA 8260D 10/27/20 15:22 REF Acrylonitrile [107-13-1]^ 18 UD ug/L 5 18 50 O126036 EPA 8260D 10/27/20 15:22 REF Benzene[71-43-2]^ 0.75 UD ug/L 5 0.75 5.0 O126036 EPA 8260D 10/27/20 15:22 REF Bromochloromethane [74-97-5]^ 2.4 UD ug/L 5 2.4 5.0 O126036 EPA 8260D 10/27/20 15:22 REF Bromodichloromethane [75-27-4]^ 0.85 UD ug/L 5 0.85 5.0 O126036 EPA 8260D 10/27/20 15:22 REF Bromoform [75-25-2]^ 1.1 UD ug/L 5 1.1 5.0 O126036 EPA 8260D 10/27/20 15:22 REF QL-02, QV-01 Bromomethane [74-83-9]^ 0.70 UD ug/L 5 0.70 5.0 OJ26036 EPA 8260D 10/27/20 15:22 REF Carbon disulfide [75-15-O]^ 7.5 UD ug/L 5 7.5 25 OJ26036 EPA 8260D 10/27/20 15:22 REF Carbon tetrachloride [56-23-5]^ 0.85 UD ug/L 5 0.85 5.0 OJ26036 EPA 8260D 10/27/20 15:22 REF QV-01 Chlorobenzene [108-90-7]^ 0.85 UD ug/L 5 0.85 5.0 OJ26036 EPA 8260D 10/27/20 15:22 REF Chloroethane [75-00-3]^ 1.2 UD ug/L 5 1.2 5.0 OJ26036 EPA 8260D 10/27/20 15:22 REF Chloroform [67-66-3]^ 0.90 UD ug/L 5 0.90 5.0 OJ26036 EPA 8260D 10/27/20 15:22 REF Chloromethane [74-87-3]^ 0.65 UD ug/L 5 0.65 5.0 OJ26036 EPA 8260D 10/27/20 15:22 REF cis-1,2-Dichloroethene [156-59-2]^ 7.8 D ug/L 5 0.75 5.0 O326036 EPA 8260D 10/27/20 15:22 REF cis-1,3-Dichloropropene [10061-01-5]^ 1.0 UD ug/L 5 1.0 5.0 OJ26036 EPA 8260D 10/27/20 15:22 REF Dibromochloromethane [124-48-1]^ 0.85 UD ug/L 5 0.85 5.0 OJ26036 EPA 8260D 10/27/20 15:22 REF Dibromomethane [74-95-3]^ 1.4 UD ug/L 5 1.4 5.0 OJ26036 EPA 8260D 10/27/20 15:22 REF Ethylbenzene [500-41-4]^ 0.65 UD ug/L 5 0.65 5.0 OJ26036 EPA 8260D 10/27/20 15:22 REF Iodomethane [74-88-4]^ 8.5 UD ug/L 5 8.5 25 OJ26036 EPA 8260D 10/27/20 15:22 REF Methylene chloride [75-09-2]^ 1.2 UD ug/L 5 1.2 5.0 OJ26036 EPA 8260D 10/27/20 15:22 REF Styrene [100-42-5]^ 0.55 UD ug/L 5 0.55 5.0 OJ26036 EPA 8260D 10/27/20 15:22 REF Tetrachloroethene [127-18-4]^ 0.85 UD ug/L 5 0.85 5.0 OJ26036 EPA 8260D 10/27/20 15:22 REF Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 OJ23024 EPA 8260D 10/26/20 09:25 REF Toluene [108-88-3]^ 0.70 UD ug/L 5 0.70 5.0 OJ26036 EPA 8260D 10/27/20 15:22 REF trans-1,2-Dichloroethene [156-60-5]^ 1.0 UD ug/L 5 1.0 5.0 OJ26036 EPA 8260D 10/27/20 15:22 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.75 UD ug/L 5 0.75 5.0 OJ26036 EPA 8260D 10/27/20 15:22 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 3.5 UD ug/L 5 3.5 5.0 OJ26036 EPA 8260D 10/27/20 15:22 REF Trichloroethene [79-01-6]^ 0.75 UD ug/L 5 0.75 5.0 OJ26036 EPA 8260D 10/27/20 15:22 REF Trichlorofluoromethane [75-69-4]^ 1.2 UD ug/L 5 1.2 5.0 OJ26036 EPA 8260D 10/27/20 15:22 REF Vinyl acetate [108-05-4]^ 4.8 UD ug/L 5 4.8 25 OJ26036 EPA 8260D 10/27/20 15:22 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 53 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW7 Lab Sample ID:CD16586-05 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 13:20 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 5.4 D ug/L 5 1.6 5.0 0326036 EPA 8260D 10/27/20 15:22 REF Xylenes (Total) [1330-20-7]^ 2.2 UD ug/L 5 2.2 15 OJ26036 EPA 8260D 10/27/20 15:22 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 42 1 50.0 85 % 53-136 OJ26036 EPA 626OD 10127120 15:22 REF Dibromofluoromethane 48 1 50.0 96 % 67-129 OJ26036 EPA 626OD 1012712015:22 REF Toluene-d8 49 1 50.0 98 % 59-134 OJ26036 EPA 826OD 1012712015:22 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 OJ21046 EPA 7470A 10/23/20 16:52 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 OJ21030 EPA 6010D 10/23/20 13:05 JDH Barium [7440-39-3]^ 34.4 ug/L 1 1.10 10.0 O121030 EPA 6010D 10/23/20 13:05 JDH Cadmium [7440-43-9]^ 1.57 ug/L 1 0.360 1.00 O121030 EPA 6010D 10/23/20 13:05 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 OJ21030 EPA 6010D 10/23/20 13:05 JDH Lead [7439-92-1]^ 10.9 ug/L 1 3.10 10.0 O121030 EPA 6010D 10/23/20 13:05 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 OJ21030 EPA 6010D 10/23/20 13:05 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 OJ21030 EPA 6010D 10/23/20 13:05 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 20 mg/L 1 2.2 5.0 O121014 EPA 300.0 10/21/20 17:56 UI Nitrate as N [14797-55-8] 0.20 mg/L 1 0.041 0.10 [CALC] EPA 353.2 10/26/20 13:04 JAH Nitrate/Nitrite as N^ 0.20 mg/L 1 0.041 0.10 O126013 EPA 353.2 10/26/20 13:04 JAH Nitrite as N [14797-65-O]^ 0.017 U mg/L 1 0.017 0.10 OJ15042 EPA 353.2 10/15/20 17:23 JAH Sulfate as SO4 [14808-79-8]^ 2.9 U mg/L 1 2.9 5.0 OJ21014 EPA 300.0 10/21/20 17:56 UI Sulfide [18496-25-8]^ 0.19 mg/L 1 0.010 0.10 O120016 iM 450052 D-2011 10/20/20 16:38 JOC Total Alkalinity as CaCO3 [471-34-1]^ 120 mg/L 1 14 15 O120019 EPA 310.2 1O/20/20 15:58 JAH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed gy Notes 1,4-Dioxane [123-91-1]^ 6.9 ug/L 1 0.80 2.0 O119034 EPA 8260D 10/20/20 05:24 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed By Notes Toluene-d8 5.2 1 5.00 104 % 75-125 0J19034 EPA 8260D 10120120 05:24 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 53 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW7 Lab Sample ID:CD16586-05 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 13:20 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 406 D mg/L 21 43.5 52.5 0321005 RSK 175 10/21/20 15:08 KG Ethane [74-84-0] 0.107 UD mg/L 21 0.107 0.126 OJ21005 RSK 175 10/21/20 15:08 KG Ethene [74-85-1] 0.107 UD mg/L 21 0.107 0.126 OJ21005 RSK 175 10/21/20 15:08 KG Methane [74-82-8] 3.68 D mg/L 21 0.0840 0.105 0321005 RSK 175 10/21/20 15:08 KG Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MOIL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 21 mg/L 1 0.54 1.0 0322067 EPA 9060A 10/23/20 12:59 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 23 of 53 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW8 Lab Sample ID:CD16586-06 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 16:00 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary rertified analyte [NC 591] Analyte FCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 O126029 EPA 8260D 10/26/20 20:53 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 O126029 EPA 8260D 10/26/20 20:53 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 O126029 EPA 8260D 10/26/20 20:53 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 O126029 EPA 8260D 10/26/20 20:53 REF 1,1-Dichloroethane [75-34-3]^ 0.56 J ug/L 1 0.13 1.0 O126029 EPA 8260D 10/26/20 20:53 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 O126029 EPA 8260D 10/26/20 20:53 REF QL-02, QV-01 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF 1,2-Dichlorobenzene [95-50-1]^ 0.54 J ug/L 1 0.19 1.0 O326029 EPA 8260D 10/26/20 20:53 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF 1,2-Dichloropropene [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF 1,4-Dichlorobenzene [106-46-7]^ 5.3 ug/L 1 0.19 1.0 O326029 EPA 8260D 10/26/20 20:53 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 OJ26029 EPA 8260D 10/26/20 20:53 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 OJ26029 EPA 8260D 10/26/20 20:53 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 OJ26029 EPA 8260D 10/26/20 20:53 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 OJ26029 EPA 8260D 10/26/20 20:53 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 OJ26029 EPA 8260D 10/26/20 20:53 REF Benzene [71-43-2]^ 2.8 ug/L 1 0.15 1.0 O326029 EPA 8260D 10/26/20 20:53 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF Carbon disulfide [75-15-O]^ 1.5 U ug/L 1 1.5 5.0 OJ26029 EPA 8260D 10/26/20 20:53 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF Chlorobenzene [108-90-7]^ 4.3 ug/L 1 0.17 1.0 O326029 EPA 8260D 10/26/20 20:53 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF QV-01 Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF cis-1,2-Dichloroethene [156-59-2]^ 0.43 J ug/L 1 0.15 1.0 O326029 EPA 8260D 10/26/20 20:53 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF Ethylbenzene [500-41-4]^ 0.13 U ug/L 1 0.13 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 OJ26029 EPA 8260D 10/26/20 20:53 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 OJ23023 EPA 8260D 10/24/20 20:41 REF Toluene [108-88-3]^ 0.51 J ug/L 1 0.14 1.0 O326029 EPA 8260D 10/26/20 20:53 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 OJ26029 EPA 8260D 10/26/20 20:53 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 24 of 53 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW8 Lab Sample ID:CD16586-06 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 16:00 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 OJ26029 EPA 8260D 10/26/20 20:53 REF QV-01 Xylenes(Total)[133O-20-7]^ 2.2 J ug/L 1 0.45 3.0 0326029 EPA 8260D 10/26/20 20:53 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 53 1 50.0 105 % 53-136 OJ26029 EPA 626OD 10126120 20:53 REF Dibromofluoromethane 49 1 50.0 98 % 67-129 OJ26029 EPA 626OD 10126120 20:53 REF Toluene-d8 54 1 50.0 109 % 59-134 OJ26029 EPA 626OD 10126120 20:53 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 OJ21046 EPA 7470A 10/23/20 17:00 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 OJ21030 EPA 6010D 10/23/20 13:07 JDH Barium [7440-39-3]^ 75.6 ug/L 1 1.10 10.0 O121030 EPA 6010D 10/23/20 13:07 JDH Cadmium [7440-43-9]^ 1.67 ug/L 1 0.360 1.00 O121030 EPA 6010D 10/23/20 13:07 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 OJ21030 EPA 6010D 10/23/20 13:07 JDH Lead [7439-92-1]^ 9.86 J ug/L 1 3.10 10.0 O121030 EPA 6010D 10/23/20 13:07 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 OJ21030 EPA 6010D 10/23/20 13:07 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 OJ21030 EPA 6010D 10/23/20 13:07 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 69 mg/L 1 2.2 5.0 O121014 EPA 300.0 10/21/20 18:14 UI Nitrate as N [14797-55-8] 0.12 mg/L 1 0.041 0.10 [CALC] EPA 353.2 10/26/20 13:06 JAH Nitrate/Nitrite as N^ 0.12 mg/L 1 0.041 0.10 O126013 EPA 353.2 10/26/20 13:06 JAH Nitrite as N [14797-65-O]^ 0.017 U mg/L 1 0.017 0.10 OJ15042 EPA 353.2 10/15/20 17:24 JAH Sulfate as SO4 [14808-79-8]^ 2.9 U mg/L 1 2.9 5.0 OJ21014 EPA 300.0 10/21/20 18:14 UI Sulfide [18496-25-8]^ 0.078 J mg/L 1 0.010 0.10 O120016 iM 450052 D-2011 10/20/20 16:38 JOC Total Alkalinity as CaCO3 [471-34-1]^ 240 D mg/L 2 28 30 O120019 EPA 310.2 1O/20/20 16:14 JAH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed gy Notes 1,4-Dioxane [123-91-1]^ 29 ug/L 1 0.80 2.0 O119034 EPA 8260D 10/20/20 05:49 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed By Notes Toluene-d8 5.2 1 5.00 103 % 75-125 0J19034 EPA 8260D 10120120 05:49 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 25 of 53 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW8 Lab Sample ID:CD16586-06 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 16:00 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 462 D mg/L 21 43.5 52.5 0321005 RSK 175 10/21/20 15:24 KG Ethane [74-84-0] 0.107 UD mg/L 21 0.107 0.126 OJ21005 RSK 175 10/21/20 15:24 KG Ethene [74-85-1] 0.107 UD mg/L 21 0.107 0.126 OJ21005 RSK 175 10/21/20 15:24 KG Methane [74-82-8] 6.15 D mg/L 21 0.0840 0.105 0321005 RSK 175 10/21/20 15:24 KG Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MOIL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 21 mg/L 1 0.54 1.0 0322067 EPA 9060A 10/23/20 12:59 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 26 of 53 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW9 Lab Sample ID:CD16586-07 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 17:30 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 0123023 EPA 8260D 10/24/20 21:09 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 0123023 EPA 8260D 10/24/20 21:09 REF QV-01 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 0123023 EPA 8260D 10/24/20 21:09 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 0123023 EPA 8260D 10/24/20 21:09 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 0123023 EPA 8260D 10/24/20 21:09 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 0123023 EPA 8260D 10/24/20 21:09 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 0123023 EPA 8260D 10/24/20 21:09 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 0123023 EPA 8260D 10/24/20 21:09 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 0123023 EPA 8260D 10/24/20 21:09 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 0123023 EPA 8260D 10/24/20 21:09 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 0123023 EPA 8260D 10/24/20 21:09 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 0123023 EPA 8260D 10/24/20 21:09 REF 1,4-Dichlorobenzene [306-46-7]^ 3.1 ug/L 1 0.19 1.0 0123023 EPA 8260D 10/24/20 21:09 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 0123023 EPA 8260D 10/24/20 21:09 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 0123023 EPA 8260D 10/24/20 21:09 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 0123023 EPA 8260D 10/24/20 21:09 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 0123023 EPA 8260D 10/24/20 21:09 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 0123023 EPA 8260D 10/24/20 21:09 REF Benzene [71-43-2]A 4.0 ug/L 1 0.15 1.0 0123023 EPA 8260D 10/24/20 21:09 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 0123023 EPA 8260D 10/24/20 21:09 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 0123023 EPA 8260D 10/24/20 21:09 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 0123023 EPA 8260D 10/24/20 21:09 REF QV-01 Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 0123023 EPA 8260D 10/24/20 21:09 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 0123023 EPA 8260D 10/24/20 21:09 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 0123023 EPA 8260D 10/24/20 21:09 REF QV-01 Chlorobenzene [308-90-7]A 8.9 ug/L 1 0.17 1.0 0123023 EPA 8260D 10/24/20 21:09 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 0123023 EPA 8260D 10/24/20 21:09 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 0123023 EPA 8260D 10/24/20 21:09 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 0123023 EPA 8260D 10/24/20 21:09 REF cis-1,2-Dichloroethene [156-59-2]A 0.74 J ug/L 1 0.15 1.0 0123023 EPA 8260D 10/24/20 21:09 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 0123023 EPA 8260D 10/24/20 21:09 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 0123023 EPA 8260D 10/24/20 21:09 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 0123023 EPA 8260D 10/24/20 21:09 REF Ethylbenzene [500-41-4]^ 0.13 U ug/L 1 0.13 1.0 0123023 EPA 8260D 10/24/20 21:09 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 0123023 EPA 8260D 10/24/20 21:09 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 0123023 EPA 8260D 10/24/20 21:09 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 0123023 EPA 8260D 10/24/20 21:09 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 0123023 EPA 8260D 10/24/20 21:09 REF Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 0123023 EPA 8260D 10/24/20 21:09 REF Toluene [108-88-3]A 0.43 J ug/L 1 0.14 1.0 0123023 EPA 8260D 10/24/20 21:09 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 0123023 EPA 8260D 10/24/20 21:09 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 0123023 EPA 8260D 10/24/20 21:09 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 0123023 EPA 8260D 10/24/20 21:09 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 0123023 EPA 8260D 10/24/20 21:09 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 0123023 EPA 8260D 10/24/20 21:09 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 0123023 EPA 8260D 10/24/20 21:09 REF Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 0123023 EPA 8260D 10/24/20 21:09 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 27 of 53 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW9 Lab Sample ID:CD16586-07 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 17:30 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes(Total)[1330-20-7]^ 0.46 J ug/L 1 0.45 3.0 0323023 EPA 8260D 10/24/20 21:09 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 45 1 50.0 90 % 53-136 OJ23023 EPA 6260D 10124120 21:09 REF Dibromofluoromethane 51 1 50.0 102 % 67-129 OJ23023 EPA 6260D 10124120 21:09 REF Toluene-c48 50 1 50.0 100 % 59-134 OJ23023 EPA 6260D 10124120 21:09 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 OJ21046 EPA 7470A 10/23/20 17:02 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Arsenic [7440-38-2]^ 64.8 ug/L 1 7.60 10.0 0121030 EPA 6010D 10/23/20 13:09 JDH Barium [7440-39-3]^ 95.5 ug/L 1 1.10 10.0 0121030 EPA 6010D 10/23/20 13:09 JDH Cadmium [7440-43-9]^ 0.662 J ug/L 1 0.360 1.00 0121030 EPA 6010D 10/23/20 13:09 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 OJ21030 EPA 6010D 10/23/20 13:09 JDH Lead [7439-92-1]^ 6.58 J ug/L 1 3.10 10.0 0121030 EPA 6010D 10/23/20 13:09 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 OJ21030 EPA 6010D 10/23/20 13:09 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 OJ21030 EPA 6010D 10/23/20 13:09 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 100 D mg/L 2 4.4 10 0123009 EPA 300.0 10/23/20 13:05 LJI Nitrate as N [14797-55-8] 0.10 mg/L 1 0.041 0.10 [CALC] EPA 353.2 10/26/20 13:08 JAH Nitrate/Nitrite as N^ 0.10 mg/L 1 0.041 0.10 0126013 EPA 353.2 10/26/20 13:08 JAH Nitrite as N [14797-65-O]^ 0.017 U mg/L 1 0.017 0.10 OJ15042 EPA 353.2 10/15/20 17:26 JAH Sulfate as SO4 [14808-79-8]^ 2.9 U mg/L 1 2.9 5.0 OJ21014 EPA 300.0 10/21/20 19:07 LJI Sulfide [18496-25-8]^ 0.14 mg/L 1 0.010 0.10 0120016 iM 450OS2 D-2011 10/20/20 16:38 JOC Total Alkalinity as CaCO3 [471-34-1]^ 830 D mg/L 5 70 75 0123015 EPA 310.2 10/23/20 12:56 JAH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 25 ug/L 1 0.80 2.0 0119034 EPA 8260D 10/20/20 06:15 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 5.1 1 5.00 102 % 75-125 0J19034 EPA 8260D 10120120 06:15 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 28 of 53 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW9 Lab Sample ID:CD16586-07 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 17:30 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 729 D mg/L 21 43.5 52.5 0321005 RSK 175 10/21/20 15:40 KG Ethane [74-84-0] 0.107 UD mg/L 21 0.107 0.126 OJ21005 RSK 175 10/21/20 15:40 KG Ethene [74-85-1] 0.107 UD mg/L 21 0.107 0.126 OJ21005 RSK 175 10/21/20 15:40 KG Methane [74-82-8] 5.68 D mg/L 21 0.0840 0.105 0321005 RSK 175 10/21/20 15:40 KG Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MOIL POLL Batch Method Analyzed Ay Notes Total Organic Carbon^ 37 mg/L 1 0.54 1.0 0322067 EPA 9060A 10/23/20 12:59 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 29 of 53 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW15R Lab Sample ID:CD16586-08 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 11:45 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 0123023 EPA 8260D 10/24/20 21:37 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 0123023 EPA 8260D 10/24/20 21:37 REF QV-01 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 0123023 EPA 8260D 10/24/20 21:37 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 0123023 EPA 8260D 10/24/20 21:37 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 0123023 EPA 8260D 10/24/20 21:37 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 0123023 EPA 8260D 10/24/20 21:37 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 0123023 EPA 8260D 10/24/20 21:37 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 0123023 EPA 8260D 10/24/20 21:37 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 0123023 EPA 8260D 10/24/20 21:37 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 0123023 EPA 8260D 10/24/20 21:37 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 0123023 EPA 8260D 10/24/20 21:37 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 0123023 EPA 8260D 10/24/20 21:37 REF 1,4-Dichlorobenzene [306-46-7]^ 0.73 J ug/L 1 0.19 1.0 0123023 EPA 8260D 10/24/20 21:37 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 0123023 EPA 8260D 10/24/20 21:37 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 0123023 EPA 8260D 10/24/20 21:37 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 0123023 EPA 8260D 10/24/20 21:37 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 0123023 EPA 8260D 10/24/20 21:37 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 0123023 EPA 8260D 10/24/20 21:37 REF Benzene [71-43-2]A 1.2 ug/L 1 0.15 1.0 0123023 EPA 8260D 10/24/20 21:37 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 0123023 EPA 8260D 10/24/20 21:37 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 0123023 EPA 8260D 10/24/20 21:37 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 0123023 EPA 8260D 10/24/20 21:37 REF QV-01 Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 0123023 EPA 8260D 10/24/20 21:37 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 0123023 EPA 8260D 10/24/20 21:37 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 0123023 EPA 8260D 10/24/20 21:37 REF QV-01 Chlorobenzene [108-90-7]^ 0.56 J ug/L 1 0.17 1.0 0123023 EPA 8260D 10/24/20 21:37 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 0123023 EPA 8260D 10/24/20 21:37 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 0123023 EPA 8260D 10/24/20 21:37 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 0123023 EPA 8260D 10/24/20 21:37 REF cis-1,2-Dichloroethene [156-59-2]^ 1.6 ug/L 1 0.15 1.0 0123023 EPA 8260D 10/24/20 21:37 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 0123023 EPA 8260D 10/24/20 21:37 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 0123023 EPA 8260D 10/24/20 21:37 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 0123023 EPA 8260D 10/24/20 21:37 REF Ethylbenzene [500-41-4]^ 0.13 U ug/L 1 0.13 1.0 0123023 EPA 8260D 10/24/20 21:37 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 0123023 EPA 8260D 10/24/20 21:37 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 0123023 EPA 8260D 10/24/20 21:37 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 0123023 EPA 8260D 10/24/20 21:37 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 0123023 EPA 8260D 10/24/20 21:37 REF Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 0123023 EPA 8260D 10/24/20 21:37 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 0123023 EPA 8260D 10/24/20 21:37 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 0123023 EPA 8260D 10/24/20 21:37 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 0123023 EPA 8260D 10/24/20 21:37 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 0123023 EPA 8260D 10/24/20 21:37 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 0123023 EPA 8260D 10/24/20 21:37 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 0123023 EPA 8260D 10/24/20 21:37 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 0123023 EPA 8260D 10/24/20 21:37 REF Vinyl chloride [75-01-4]^ 1.1 ug/L 1 0.32 1.0 0123023 EPA 8260D 10/24/20 21:37 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 30 of 53 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW15R Lab Sample ID:CD16586-08 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 11:45 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Xylenes (Total) [1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 OJ23023 EPA 8260D 10/24/20 21:37 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 45 1 50.0 89 % 53-136 OJ23023 EPA 626OD 10124120 21:37 REF Dibromofluoromethane 51 1 50.0 103 % 67-129 OJ23023 EPA 626OD 10124120 21:37 REF Toluene-c48 49 1 50.0 98 % 59-134 OJ23023 EPA 626OD 10124120 21:37 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 U ug/L 1 0.150 0.200 OJ21046 EPA 7470A 10/23/20 17:05 KAH Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 U ug/L 1 7.60 10.0 OJ21030 EPA 6010D 10/23/20 13:12 JDH Barium [7440-39-3]^ 27.5 ug/L 1 1.10 10.0 O121030 EPA 6010D 10/23/20 13:12 JDH Cadmium [7440-43-9]^ 1.92 ug/L 1 0.360 1.00 O121030 EPA 6010D 10/23/20 13:12 JDH Chromium [7440-47-3]^ 1.40 U ug/L 1 1.40 10.0 OJ21030 EPA 6010D 10/23/20 13:12 JDH Lead [7439-92-1]^ 9.94 J ug/L 1 3.10 10.0 O121030 EPA 6010D 10/23/20 13:12 JDH Selenium [7782-49-2]^ 6.20 U ug/L 1 6.20 10.0 OJ21030 EPA 6010D 10/23/20 13:12 JDH Silver[7440-22-4]^ 1.90 U ug/L 1 1.90 10.0 OJ21030 EPA 6010D 10/23/20 13:12 JDH Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes Chloride [16887-00-6]^ 2.9 J mg/L 1 2.2 5.0 O121014 EPA 300.0 10/21/20 19:25 LJI Nitrate as N [14797-55-8] 0.51 mg/L 1 0.041 0.10 [CALC] EPA 353.2 10/26/20 13:10 JAH Nitrate/Nitrite as N^ 0.51 mg/L 1 0.041 0.10 O126013 EPA 353.2 10/26/20 13:10 JAH Nitrite as N [14797-65-O]^ 0.017 U mg/L 1 0.017 0.10 OJ15042 EPA 353.2 10/15/20 17:27 JAH Sulfate as SO4 [14808-79-8]^ 7.2 mg/L 1 2.9 5.0 O121014 EPA 300.0 10/21/20 19:25 LJI Sulfide [18496-25-8]^ 0.027 J mg/L 1 0.010 0.10 O120016 iM 450052 D-2011 10/20/20 16:38 JOC Total Alkalinity as CaCO3 [471-34-1]^ 96 mg/L 1 14 15 O120019 EPA 310.2 1O/20/20 16:01 JAH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 OJ19034 EPA 8260D 10/20/20 06:40 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.2 1 5.00 103 % 75-125 0J19034 EPA 826OD 10120120 06:40 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 31 of 53 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-MW15R Lab Sample ID:CD16586-08 Received: 10/15/20 08:19 Matrix: Ground Water Sampled:10/14/20 11:45 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: Gary Simcox/ James Water Dissolved Gases by GC Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes Carbon dioxide [124-38-9] 425 D mg/L 21 43.5 52.5 0322022 RSK 175 10/22/20 10:00 KG Ethane [74-84-0] 0.107 UD mg/L 21 0.107 0.126 OJ22022 RSK 175 10/22/20 10:00 KG Ethene [74-85-1] 0.107 UD mg/L 21 0.107 0.126 OJ22022 RSK 175 10/22/20 10:00 KG Methane [74-82-8] 3.20 D mg/L 21 0.0840 0.105 0322022 RSK 175 10/22/20 10:00 KG Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MOIL P L Batch Method Analyzed Ay Notes Total Organic Carbon^ 2.6 mg/L 1 0.54 1.0 0326043 EPA 9060A 10/27/20 11:08 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 32 of 53 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 6301-TRIPBLANK Lab Sample ID:CD16586-09 Received: 10/15/20 08:19 Matrix: Water Sampled:10/14/20 08:35 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certfied anaiyte [NC 591] Analyte ICAS Numberl Results Flaa Units DF MDL P L Batch Method Analyzed Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 0123023 EPA 8260D 10/24/20 14:09 REF 1,1,1-Trichloroethane [71-55-6]A 0.12 U ug/L 1 0.12 1.0 0123023 EPA 8260D 10/24/20 14:09 REF QV-01 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 0123023 EPA 8260D 10/24/20 14:09 REF 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 0123023 EPA 8260D 10/24/20 14:09 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 0123023 EPA 8260D 10/24/20 14:09 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 0123023 EPA 8260D 10/24/20 14:09 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 0123023 EPA 8260D 10/24/20 14:09 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 0123023 EPA 8260D 10/24/20 14:09 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 0123023 EPA 8260D 10/24/20 14:09 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 0123023 EPA 8260D 10/24/20 14:09 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 0123023 EPA 8260D 10/24/20 14:09 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 0123023 EPA 8260D 10/24/20 14:09 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 0123023 EPA 8260D 10/24/20 14:09 REF 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 0123023 EPA 8260D 10/24/20 14:09 REF 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 0123023 EPA 8260D 10/24/20 14:09 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 0123023 EPA 8260D 10/24/20 14:09 REF Acetone [67-64-1]A 10 U ug/L 1 10 20 0123023 EPA 8260D 10/24/20 14:09 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 0123023 EPA 8260D 10/24/20 14:09 REF Benzene [71-43-2]A 0.15 U ug/L 1 0.15 1.0 0123023 EPA 8260D 10/24/20 14:09 REF Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 0123023 EPA 8260D 10/24/20 14:09 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 0123023 EPA 8260D 10/24/20 14:09 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 0123023 EPA 8260D 10/24/20 14:09 REF QV-01 Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 0123023 EPA 8260D 10/24/20 14:09 REF Carbon disulfide [75-15-0]A 1.5 U ug/L 1 1.5 5.0 0123023 EPA 8260D 10/24/20 14:09 REF Carbon tetrachloride [56-23-5]A 0.17 U ug/L 1 0.17 1.0 0123023 EPA 8260D 10/24/20 14:09 REF QV-01 Chlorobenzene [108-90-7]A 0.17 U ug/L 1 0.17 1.0 0123023 EPA 8260D 10/24/20 14:09 REF Chloroethane [75-00-3]A 0.23 U ug/L 1 0.23 1.0 0123023 EPA 8260D 10/24/20 14:09 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 0123023 EPA 8260D 10/24/20 14:09 REF Chloromethane [74-87-3]A 0.13 U ug/L 1 0.13 1.0 0123023 EPA 8260D 10/24/20 14:09 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 0123023 EPA 8260D 10/24/20 14:09 REF cis-1,3-Dichloropropene [10061-01-5]A 0.20 U ug/L 1 0.20 1.0 0123023 EPA 8260D 10/24/20 14:09 REF Dibromochloromethane [124-48-1]A 0.17 U ug/L 1 0.17 1.0 0123023 EPA 8260D 10/24/20 14:09 REF Dibromomethane [74-95-3]A 0.27 U ug/L 1 0.27 1.0 0123023 EPA 8260D 10/24/20 14:09 REF Ethylbenzene [500-41-4]A 0.13 U ug/L 1 0.13 1.0 0123023 EPA 8260D 10/24/20 14:09 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 0123023 EPA 8260D 10/24/20 14:09 REF Methylene chloride [75-09-2]A 0.23 U ug/L 1 0.23 1.0 0123023 EPA 8260D 10/24/20 14:09 REF Naphthalene [91-20-3]^ 0.11 U ug/L 1 0.11 1.0 0123023 EPA 8260D 10/24/20 14:09 REF Styrene [100-42-5]A 0.11 U ug/L 1 0.11 1.0 0123023 EPA 8260D 10/24/20 14:09 REF Tetrachloroethene [127-18-4]A 0.17 U ug/L 1 0.17 1.0 0123023 EPA 8260D 10/24/20 14:09 REF Tetrahydrofuran [109-99-9]^ 0.53 U ug/L 1 0.53 1.0 0123023 EPA 8260D 10/24/20 14:09 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 0123023 EPA 8260D 10/24/20 14:09 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 0123023 EPA 8260D 10/24/20 14:09 REF trans-1,3-Dichloropropene [10061-02-6]A 0.15 U ug/L 1 0.15 1.0 0123023 EPA 8260D 10/24/20 14:09 REF trans-1,4-Dichloro-2-butene [110-57-6]A 0.70 U ug/L 1 0.70 1.0 0123023 EPA 8260D 10/24/20 14:09 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 0123023 EPA 8260D 10/24/20 14:09 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 0123023 EPA 8260D 10/24/20 14:09 REF Vinyl acetate [108-05-4]A 0.95 U ug/L 1 0.95 5.0 0123023 EPA 8260D 10/24/20 14:09 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 33 of 53 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 6301-TRIPBLANK Lab Sample ID:CD16586-09 Received: 10/15/20 08:19 Matrix: Water Sampled:10/14/20 08:35 Work Order: CD16586 Project: Moore County MSW LF CA Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed AX Notes Vinyl chloride [75-01-4]^ 0.32 U ug/L 1 0.32 1.0 OJ23023 EPA 8260D 10/24/20 14:09 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 OJ23023 EPA 8260D 10/24/20 14:09 REF Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 44 1 50.0 87 % 53-136 OJ23023 EPA 626OD 10124120 14:09 REF Dibromofluoromethane 48 1 50.0 96 % 67-129 OJ23023 EPA 626OD 10124120 14:09 REF Toluene-d8 48 1 50.0 96 % 59-134 OJ23023 EPA 826OD 10124120 14:09 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 0.80 U ug/L 1 0.80 2.0 OJ19034 EPA 8260D 1O/20/20 07:05 KKW Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffly Notes Toluene-d8 5.3 1 5.00 105 % 75-125 0J19034 EPA 826OD 10120120 07:05 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 34 of 53 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch OJ23023 - EPA 5030B MS Blank (0323023-BLK1) Prepared: 10/23/2020 13:23 Analyzed: 10/24/2020 13:40 Analvte Result Flaq POL Units 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Naphthalene 0.11 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Tetrahydrofuran 0.53 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes QV-01 QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 35 of 53 QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch OJ23023 - EPA 5O3OB MS - Continued (� �Eo www.encolabs.com Blank (0323023-BLK1) Continued Prepared: 10/23/2020 13:23 Analyzed: 10/24/2020 13:40 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 44 ug/L 50.0 88 53-136 Dibromofluoromethane 49 u9/L 50.0 98 67-129 Toluene-d8 50 u9/L 50.0 100 59-134 LCS (0323023-BS1) Prepared: 10/23/2020 13:23 Analyzed: 10/24/2020 11:48 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 22 1.0 ug/L 20.0 109 75-133 Benzene 20 1.0 ug/L 20.0 102 80-134 Chlorobenzene 20 1.0 ug/L 20.0 101 80-120 Toluene 19 1.0 ug/L 20.0 97 71-120 Trichloroethene 23 1.0 ug/L 20.0 117 74-120 Matrix Spike (OJ23023-MS1) Prepared: 10/23/2020 13:23 Analyzed: 10/24/2020 12:16 Source: CD17278-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 0.21 U 107 75-133 Benzene 21 1.0 ug/L 20.0 0.15 U 106 80-134 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 102 80-120 Toluene 20 1.0 ug/L 20.0 0.14 U 98 71-120 Trichloroethene 24 1.0 ug/L 20.0 0.15 U 120 74-120 Matrix Spike Dup (OJ23023-MSD1) Prepared: 10/23/2020 13:23 Analyzed: 10/24/2020 12:44 Source: CD17278-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 0.21 U 105 75-133 2 20 Benzene 20 1.0 ug/L 20.0 0.15 U 101 80-134 5 17 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 101 80-120 2 16 Toluene 19 1.0 ug/L 20.0 0.14 U 93 71-120 5 17 Trichloroethene 22 1.0 ug/L 20.0 0.15 U 111 74-120 8 22 Batch OJ23024 - EPA 5O3OB MS Blank (0323024-BLK1) Prepared: 10/23/2020 13:57 Analyzed: 10/26/2020 03:54 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 36 of 53 0Nk"q09 www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch OJ23024 - EPA 5030E MS - Continued Blank (0323024-BLK1) Continued Prepared: 10/23/2020 13:57 Analyzed: 10/26/2020 03:54 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis-1,2-Dichloroethene 0.15 U 1.0 ug/L cis-1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Tetrahydrofuran 0.53 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromofluorobenzene 44 u9/L 50.0 87 53-136 Dibromofluoromethane 47 u9/L 50.0 95 67-129 Toluene-& 49 u9/L 50.0 98 59-134 LCS (0323024-BSI) Prepared: 10/23/2020 13:57 Analyzed: 10/26/2020 02:03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 96 75-133 Benzene 19 1.0 ug/L 20.0 97 80-134 Chlorobenzene 19 1.0 ug/L 20.0 93 80-120 Toluene 18 1.0 ug/L 20.0 88 71-120 Trichloroethene 21 1.0 ug/L 20.0 106 74-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 37 of 53 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch OJ23024 - EPA 5030B MS - Continued Matrix Spike (0323024-MS3) Prepared: 10/23/2020 13:57 Analyzed: 10/26/2020 02:31 Source: CD17102-10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 22 1.0 ug/L 20.0 2.3 99 75-133 Benzene 19 1.0 ug/L 20.0 0.15 U 96 80-134 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 92 80-120 Toluene 17 1.0 ug/L 20.0 0.14 U 87 71-120 Trichloroethene 60 1.0 ug/L 20.0 41 95 74-120 Matrix Spike Dup (0]23024-MSD1) Prepared: 10/23/2020 13:57 Analyzed: 10/26/2020 02:58 Source: CD17102-10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 23 1.0 ug/L 20.0 2.3 102 75-133 3 20 Benzene 20 1.0 ug/L 20.0 0.15 U 98 80-134 3 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 95 80-120 3 16 Toluene 18 1.0 ug/L 20.0 0.14 U 92 71-120 5 17 Trichloroethene 61 1.0 ug/L 20.0 41 103 74-120 3 22 Batch OJ26029 - EPA 5030E MS Blank (0326029-BLK3) Prepared: 10/26/2020 16:09 Analyzed: 10/26/2020 19:53 Analvte Result Flaq POL Units 1, 1, 1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 38 of 53 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch OJ26029 - EPA 5030B MS - Continued Blank (0326029-BLK1) Continued Prepared: 10/26/2020 16:09 Analyzed: 10/26/2020 19:53 Analvte Result Flaq POL Units cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 52 u9/L 50.0 104 53-136 Dibromofluoromethane 56 u9/L 50.0 117 67-129 Toluene-d8 53 u9/L 50.0 106 59-134 LCS (0326029-BSI) Prepared: 10/26/2020 16:09 Analyzed: 10/26/2020 17:52 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 30 1.0 ug/L 20.0 149 75-133 QL-02 Benzene 17 1.0 ug/L 20.0 84 80-134 Chlorobenzene 18 1.0 ug/L 20.0 89 80-120 Toluene 18 1.0 ug/L 20.0 89 71-120 Trichloroethene 19 1.0 ug/L 20.0 93 74-120 Matrix Spike (0726029-MS1) Prepared: 10/26/2020 16:09 Analyzed: 10/26/2020 18:23 Source: CD17278-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 32 1.0 ug/L 20.0 0.21 U 162 75-133 QM-07 Benzene 19 1.0 ug/L 20.0 0.15 U 96 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 97 80-120 Toluene 20 1.0 ug/L 20.0 0.14 U 101 71-120 Trichloroethene 21 1.0 ug/L 20.0 0.15 U 107 74-120 Matrix Spike Dup (0326029-MSD1) Prepared: 10/26/2020 16:09 Analyzed: 10/26/2020 18:53 Source: CD17278-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 28 1.0 ug/L 20.0 0.21 U 139 75-133 16 20 QM-07 Benzene 16 1.0 ug/L 20.0 0.15 U 79 80-134 19 17 QM-07, QM-11 Chlorobenzene 17 1.0 ug/L 20.0 0.17 U 84 80-120 14 16 Toluene 17 1.0 ug/L 20.0 0.14 U 84 71-120 19 17 QM-11 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 39 of 53 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch OJ26029 - EPA 5030B MS - Continued Matrix Spike Dup (0326029-MSDI) Continued Prepared: 10/26/2020 16:09 Analyzed: 10/26/2020 18:53 Source: CD17278-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Trichloroethene 17 1.0 ug/L 20.0 0.15 U 85 74-120 23 22 QM-11 Batch OJ26036 - EPA 5030E MS Blank (0326036-BLK3) Prepared: 10/26/2020 16:56 Analyzed: 10/27/2020 13:29 Analvte Result Flaa POL Units 1, 1, 1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L Methylene chloride 0.23 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 40 of 53 QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch OJ26036 - EPA 5030B MS - Continued (� �Eo www.encolabs.com Blank (0326036-BLK1) Continued Prepared: 10/26/2020 16:56 Analyzed: 10/27/2020 13:29 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromofluorobenzene 43 u91L 50.0 87 53-136 D/bromofluoromethane 47 u91L 50.0 94 67-129 Toluene-d8 50 u91L 50.0 99 59-134 LCS (0726036-BS1) Prepared: 10/26/2020 16:56 Analyzed: 10/27/2020 11:37 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 102 75-133 Benzene 21 1.0 ug/L 20.0 106 80-134 Chlorobenzene 20 1.0 ug/L 20.0 101 80-120 Toluene 19 1.0 ug/L 20.0 96 71-120 Trichloroethene 24 1.0 ug/L 20.0 119 74-120 Matrix Spike (0326036-MS1) Prepared: 10/26/2020 16:56 Analyzed: 10/27/2020 12:05 Source: CD17165-08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 0.21 U 97 75-133 Benzene 20 1.0 ug/L 20.0 0.15 U 99 80-134 Chlorobenzene 20 1.0 ug/L 20.0 0.17 U 98 80-120 Toluene 18 1.0 ug/L 20.0 0.14 U 92 71-120 Trichloroethene 22 1.0 ug/L 20.0 0.15 U 110 74-120 Matrix Spike Dup (0126036-MSD1) Prepared: 10/26/2020 16:56 Analyzed: 10/27/2020 12:33 Source: CD17165-08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 0.21 U 98 75-133 0.7 20 Benzene 19 1.0 ug/L 20.0 0.15 U 96 80-134 4 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 97 80-120 0.8 16 Toluene 18 1.0 ug/L 20.0 0.14 U 92 71-120 0 17 Trichloroethene 22 1.0 ug/L 20.0 0.15 U 112 74-120 2 22 Metals by EPA 6000/7000 Series Methods - Quality Control Batch OJ21046 - EPA 7470A Blank (0321046-BLK1) Prepared: 10/21/2020 16:34 Analyzed: 10/23/2020 16:08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.150 U 0.200 ug/L LCS (0721046-BS3) Prepared: 10/21/2020 16:34 Analyzed: 10/23/2020 16:10 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 41 of 53 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals by EPA 6000/7000 Series Methods - Quality Control Batch OJ21046 - EPA 747OA - Continued LCS (O]21046-BS1) Continued Prepared: 10/21/2020 16:34 Analyzed: 10/23/2020 16:10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.13 0.200 ug/L 5.00 103 80-120 Matrix Spike (0323046-MS1) Prepared: 10/21/2020 16:34 Analyzed: 10/23/2020 16:15 Source: CD16585-13 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.09 0.200 ug/L 5.00 0.150 U 102 75-125 Matrix Spike Dup (0323046-MSD1) Prepared: 10/21/2020 16:34 Analyzed: 10/23/2020 16:17 Source: CD16585-13 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.07 0.200 ug/L 5.00 0.150 U 101 75-125 0.4 25 Post Spike (0321046-PS1) Prepared: 10/21/2020 16:34 Analyzed: 10/23/2020 16:20 Source: CD16585-13 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.42 0.200 ug/L 5.00 -0.0520 108 75-125 Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch OJ21028 - EPA 3OO5A Blank (0321028-BLK1) Prepared: 10/21/2020 12:00 Analyzed: 10/23/2020 10:19 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 7.60 U 10.0 ug/L Barium 1.10 U 10.0 ug/L Cadmium 0.360 U 1.00 ug/L Chromium 1.40 U 10.0 ug/L Lead 3.10 U 10.0 ug/L Selenium 6.20 U 10.0 ug/L Silver 1.90 U 10.0 ug/L LCS (0321028-BS1) Prepared: 10/21/2020 12:00 Analyzed: 10/23/2020 10:27 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 208 10.0 ug/L 200 104 80-120 Barium 216 10.0 ug/L 200 108 80-120 Cadmium 20.8 1.00 ug/L 20.0 104 80-120 Chromium 207 10.0 ug/L 200 104 80-120 Lead 210 10.0 ug/L 200 105 80-120 Selenium 210 10.0 ug/L 200 105 80-120 Silver 211 10.0 ug/L 200 105 80-120 Matrix Spike (0323028-MS1) Prepared: 10/21/2020 12:00 Analyzed: 10/23/2020 10:30 Source: CD16320-08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 201 10.0 ug/L 200 7.60 U 100 75-125 Barium 369 10.0 ug/L 200 192 89 75-125 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 42 of 53 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 012102E - EPA 3005A - Continued Matrix Spike (0321028-MS3) Continued Prepared: 10/21/2020 12:00 Analyzed: 10/23/2020 10:30 Source: CD16320-08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Cadmium 20.3 1.00 ug/L 20.0 0.360 U 101 75-125 Chromium 201 10.0 ug/L 200 1.40 U 101 75-125 Lead 205 10.0 ug/L 200 3.10 U 103 75-125 Selenium 205 10.0 ug/L 200 6.20 U 102 75-125 Silver 203 10.0 ug/L 200 1.90 U 101 75-125 Matrix Spike Dup (0323028-MSDi) Prepared: 10/21/2020 12:00 Analyzed: 10/23/2020 10:32 Source: CD16320-08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 194 10.0 ug/L 200 7.60 U 97 75-125 3 20 Barium 386 10.0 ug/L 200 192 97 75-125 4 20 Cadmium 20.3 1.00 ug/L 20.0 0.360 U 101 75-125 0.2 20 Chromium 205 10.0 ug/L 200 1.40 U 102 75-125 2 20 Lead 207 10.0 ug/L 200 3.10 U 103 75-125 0.8 20 Selenium 204 10.0 ug/L 200 6.20 U 102 75-125 0.5 20 Silver 203 10.0 ug/L 200 1.90 U 101 75-125 0.03 20 Post Spike (0321028-PS1) Prepared: 10/21/2020 12:00 Analyzed: 10/23/2020 10:34 Source: CD16320-08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 0.203 0.0100 mg/L 0.200 0.00301 100 80-120 Barium 0.393 0.0100 mg/L 0.200 0.192 101 80-120 Cadmium 0.0207 0.00100 mg/L 0.0200 -3.76E-5 103 80-120 Chromium 0.209 0.0100 mg/L 0.200 0.00123 104 80-120 Lead 0.210 0.0100 mg/L 0.200 0.00263 104 80-120 Selenium 0.207 0.0100 mg/L 0.200 -0.00222 103 80-120 Silver 0.215 0.0100 mg/L 0.200 0.000109 108 80-120 Batch OJ21030 - EPA 3005A Blank (0321030-BLK3) Prepared: 10/21/2020 12:23 Analyzed: 10/23/2020 10:16 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 7.60 U 10.0 ug/L Barium 1.10 U 10.0 ug/L Cadmium 0.360 U 1.00 ug/L Chromium 1.40 U 10.0 ug/L Lead 3.10 U 10.0 ug/L Selenium 6.20 U 10.0 ug/L Silver 1.90 U 10.0 ug/L Blank (0321030-BLK2) Prepared: 10/21/2020 12:23 Analyzed: 10/23/2020 11:35 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 7.60 U 10.0 ug/L Barium 1.10 U 10.0 ug/L Cadmium 0.360 U 1.00 ug/L Chromium 1.40 U 10.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 43 of 53 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch OJ21030 - EPA 3005A - Continued Blank (0321030-BLK2) Continued Prepared: 10/21/2020 12:23 Analyzed: 10/23/2020 11:35 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Lead 3.10 U 10.0 ug/L Selenium 6.20 U 10.0 ug/L Silver 1.90 U 10.0 ug/L LCS (0321030-BS1) Prepared: 10/21/2020 12:23 Analyzed: 10/23/2020 11:40 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 199 10.0 ug/L 200 99 80-120 Barium 212 10.0 ug/L 200 106 80-120 Cadmium 20.4 1.00 ug/L 20.0 102 80-120 Chromium 204 10.0 ug/L 200 102 80-120 Lead 205 10.0 ug/L 200 103 80-120 Selenium 205 10.0 ug/L 200 102 80-120 Silver 212 10.0 ug/L 200 106 80-120 Matrix Spike (0323030-MS1) Prepared: 10/21/2020 12:23 Analyzed: 10/23/2020 11:48 Source: CD16586-04 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 208 10.0 ug/L 200 7.60 U 104 75-125 Barium 254 10.0 ug/L 200 41.0 106 75-125 Cadmium 22.0 1.00 ug/L 20.0 2.16 99 75-125 Chromium 200 10.0 ug/L 200 1.40 U 100 75-125 Lead 216 10.0 ug/L 200 9.32 103 75-125 Selenium 156 10.0 ug/L 200 6.20 U 78 75-125 Silver 212 10.0 ug/L 200 1.90 U 106 75-125 Matrix Spike Dup (0323030-MSDi) Prepared: 10/21/2020 12:23 Analyzed: 10/23/2020 11:50 Source: CD16586-04 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 212 10.0 ug/L 200 7.60 U 106 75-125 2 20 Barium 252 10.0 ug/L 200 41.0 106 75-125 0.5 20 Cadmium 22.0 1.00 ug/L 20.0 2.16 99 75-125 0.2 20 Chromium 200 10.0 ug/L 200 1.40 U 100 75-125 0.2 20 Lead 215 10.0 ug/L 200 9.32 103 75-125 0.4 20 Selenium 160 10.0 ug/L 200 6.20 U 80 75-125 3 20 Silver 212 10.0 ug/L 200 1.90 U 106 75-125 0.2 20 Post Spike (0321030-PS1) Prepared: 10/21/2020 12:23 Analyzed: 10/23/2020 11:52 Source: CD16586-04 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 0.208 0.0100 mg/L 0.200 0.00216 103 80-120 Barium 0.250 0.0100 mg/L 0.200 0.0410 105 80-120 Cadmium 0.0217 0.00100 mg/L 0.0200 0.00216 98 80-120 Chromium 0.197 0.0100 mg/L 0.200 -0.00564 99 80-120 Lead 0.212 0.0100 mg/L 0.200 0.00932 101 80-120 Selenium 0.159 0.0100 mg/L 0.200 -0.0555 80 80-120 Silver 0.215 0.0100 mg/L 0.200 -0.00141 108 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 44 of 53 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch OJ15042 - NO PREP Blank (0315042-BLK3) Prepared: 10/15/2020 15:34 Analyzed: 10/15/2020 17:09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.017 U 0.10 mg/L LCS (0315042-BSI) Prepared: 10/15/2020 15:34 Analyzed: 10/15/2020 17:32 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.96 0.10 mg/L 1.00 96 90-110 Matrix Spike (0315042-MS1) Prepared: 10/15/2020 15:34 Analyzed: 10/15/2020 17:11 Source: CD15705-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 0.017 U 100 90-110 Matrix Spike (0715042-MS2) Prepared: 10/15/2020 15:34 Analyzed: 10/15/2020 17:15 Source: CD16585-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 0.017 U 101 90-110 Matrix Spike Dup (0]35042-MSDI) Prepared: 10/15/2020 15:34 Analyzed: 10/15/2020 17:12 Source: CD15705-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 0.017 U 100 90-110 0.3 10 Batch OJ20016 - NO PREP Blank (0320016-BLK1) Prepared: 10/20/2020 13:21 Analyzed: 10/20/2020 16:38 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.010 U 0.10 mg/L LCS (0720016-BS3) Prepared: 10/20/2020 13:21 Analyzed: 10/20/2020 16:38 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.36 0.10 mg/L 0.401 89 80-120 Duplicate (0120016-DUPI) Prepared: 10/20/2020 13:21 Analyzed: 10/20/2020 16:38 Source: CD16585-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.023 J 0.10 mg/L 0.017 30 25 QR-04 Matrix Spike (0320016-MS1) Prepared: 10/20/2020 13:21 Analyzed: 10/20/2020 16:38 Source: CD16585-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.16 0.10 mg/L 0.401 0.017 35 80-120 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 45 of 53 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch OJ20016 - NO PREP - Continued Matrix Spike Dup (0320016-MSDI) Prepared: 10/20/2020 13:21 Analyzed: 10/20/2020 16:38 Source: CD16585-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Sulfide 0.15 0.10 mg/L 0.401 0.017 32 80-120 8 25 QM-07 Batch OJ2OO19 - NO PREP Blank (0320019-BLK3) Prepared: 10/20/2020 13:40 Analyzed: 10/20/2020 15:42 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 14 U 15 mg/L LCS (0320019-BSI) Prepared: 10/20/2020 13:40 Analyzed: 10/20/2020 15:43 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 100 15 mg/L 100 102 80-120 Matrix Spike (0320019-MS1) Prepared: 10/20/2020 13:40 Analyzed: 10/20/2020 15:44 Source: CD16585-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 170 15 mg/L 37.8 120 135 80-120 QM-07 Matrix Spike Dup (0320019-MSD1) Prepared: 10/20/2020 13:40 Analyzed: 10/20/2020 15:45 Source: CD16585-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 170 15 mg/L 37.8 120 135 80-120 0.1 25 QM-07 Batch 0.721014 - NO PREP Blank (0121014-BLK3) Prepared: 10/21/2020 11:28 Analyzed: 10/21/2020 12:03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 2.2 U 5.0 mg/L Sulfate as SO4 2.9 U 5.0 mg/L LCS (0723014-BS3) Prepared: 10/21/2020 11:28 Analyzed: 10/21/2020 12:21 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 49 5.0 mg/L 50.0 97 90-110 Sulfate as SO4 48 5.0 mg/L 50.0 95 90-110 Matrix Spike (0323014-MS3) Prepared: 10/21/2020 11:28 Analyzed: 10/21/2020 12:56 Source: CD14179-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 41 10 mg/L 40.0 5.4 89 90-110 QM-07 Sulfate as SO4 43 10 mg/L 40.0 8.3 86 90-110 QM-07 Matrix Spike (OJ23014-MS2) Prepared: 10/21/2020 11:28 Analyzed: 10/21/2020 13:49 Source: CD15832-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 46 of 53 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch OJ21014 - NO PREP - Continued Matrix Spike (0321014-MS2) Continued Prepared: 10/21/2020 11:28 Analyzed: 10/21/2020 13:49 Source: CD15832-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 580 E 5.0 mg/L 20.0 570 89 90-110 QM-07 Sulfate as SO4 30 5.0 mg/L 20.0 10 97 90-110 Matrix Spike Dup (0323014-MSDI) Prepared: 10/21/2020 11:28 Analyzed: 10/21/2020 13:14 Source: CD14179-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 41 10 mg/L 40.0 5.4 89 90-110 0.1 10 QM-07 Sulfate as SO4 43 10 mg/L 40.0 8.3 87 90-110 0.3 10 QM-07 Batch OJ23009 - NO PREP Blank (0323009-BLK3) Prepared: 10/23/2020 11:01 Analyzed: 10/23/2020 11:36 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes Chloride 2.2 U 5.0 mg/L LCS (0323009-BSI) Prepared: 10/23/2020 11:01 Analyzed: 10/23/2020 11:54 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 49 5.0 mg/L 50.0 98 90-110 Matrix Spike (0323009-MS1) Prepared: 10/23/2020 11:01 Analyzed: 10/23/2020 12:29 Source: CD34179-01RE1 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 22 5.0 mg/L 20.0 3.8 92 90-110 Matrix Spike Dup (0323009-MSD3) Prepared: 10/23/2020 11:01 Analyzed: 10/23/2020 12:47 Source: CD34179-01RE1 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Chloride 22 5.0 mg/L 20.0 3.8 91 90-110 0.2 10 Batch OJ23015 - NO PREP Blank (0323015-BLK3) Prepared: 10/23/2020 11:23 Analyzed: 10/23/2020 12:38 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 14 U 15 mg/L LCS (0323015-BS1) Prepared: 10/23/2020 11:23 Analyzed: 10/23/2020 12:39 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 100 15 mg/L 100 104 80-120 Matrix Spike (0323015-MS3) Prepared: 10/23/2020 11:23 Analyzed: 10/23/2020 12:40 Source: CD16049-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 56 15 mg/L 37.8 14 U 149 80-120 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 47 of 53 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch OJ23015 - NO PREP - Continued Matrix Spike Dup (0323015-MSDI) Prepared: 10/23/2020 11:23 Analyzed: 10/23/2020 12:41 Source: CD16049-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Alkalinity as CaCO3 52 15 mg/L 37.8 14 U 138 80-120 8 25 QM-07 Batch OJ26013 - NO PREP Blank (0326013-BLK3) Prepared: 10/26/2020 09:33 Analyzed: 10/26/2020 12:41 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/L LCS (0326013-BSI) Prepared: 10/26/2020 09:33 Analyzed: 10/26/2020 12:43 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.3 0.10 mg/L 1.25 101 90-110 Matrix Spike (0326013-MS1) Prepared: 10/26/2020 09:33 Analyzed: 10/26/2020 12:47 Source: CD16585-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.52 0.10 mg/L 0.521 0.090 83 90-110 QM-07 Matrix Spike (0326013-MS2) Prepared: 10/26/2020 09:33 Analyzed: 10/26/2020 12:52 Source: CD16586-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.3 0.10 mg/L 0.521 0.85 90 90-110 Matrix Spike Dup (0326013-MSDI) Prepared: 10/26/2020 09:33 Analyzed: 10/26/2020 12:48 Source: CD16585-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.49 0.10 mg/L 0.521 0.090 76 90-110 8 10 QM-07 Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 0.719034 - EPA 5030B MS Blank (0319034-BLK3) Prepared: 10/19/2020 00:00 Analyzed: 10/19/2020 23:31 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 0.80 U 2.0 ug/L Toluene-& 5.2 ug/L 5.00 105 75-125 LCS (0319034-BS1) Prepared: 10/19/2020 00:00 Analyzed: 10/19/2020 21:50 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 25 2.0 ug/L 25.0 101 80-133 Toluene-d8 5.2 ug/L 5.00 104 75-125 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 48 of 53 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 0119034 - EPA 5030B MS - Continued Matrix Spike (0319034-MS3) Prepared: 10/19/2020 00:00 Analyzed: 10/19/2020 22:15 Source: AD06923-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes 1,4-Dioxane 27 2.0 ug/L 25.0 0.80 U 108 80-133 Toluene-& 5.2 ug/L 5.00 105 75-125 Matrix Spike Dup (0319034-MSD1) Prepared: 10/19/2020 00:00 Analyzed: 10/19/2020 22:40 Source: AD06923-01 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes 1,4-Dioxane 27 2.0 ug/L 25.0 0.80 U 108 80-133 0.04 19 Toluene-d8 5.2 ug/L 5.00 104 75-125 Dissolved Gases by GC - Quality Control Batch 0111005 - Same Blank (0321005-BLK3) Prepared: 10/21/2020 08:20 Analyzed: 10/21/2020 10:00 Spike Source O/oREC RPD Analvte Result Flaa Q Units Level Result O/oREC Limits RPD Limit Notes Carbon dioxide 2.07 U 2.50 mg/L Ethane 0.00510 U 0.00600 mg/L Ethene 0.00510 U 0.00600 mg/L Methane 0.00400 U 0.00500 mg/L LCS (OJ21005-BSI) Prepared: 10/21/2020 08:20 Analyzed: 10/21/2020 09:22 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Carbon dioxide 51.4 2.50 mg/L 45.8 112 70-130 Ethane 0.333 0.00600 mg/L 0.323 103 70-130 Ethene 0.300 0.00600 mg/L 0.302 99 70-130 Methane 0.158 0.00500 mg/L 0.172 92 70-130 LCS Dup (0321005-BSD1) Prepared: 10/21/2020 08:20 Analyzed: 10/21/2020 09:38 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Carbon dioxide 51.0 2.50 mg/L 45.8 111 70-130 0.6 30 Ethane 0.349 0.00600 mg/L 0.323 108 70-130 5 30 Ethene 0.307 0.00600 mg/L 0.302 102 70-130 2 30 Methane 0.168 0.00500 mg/L 0.172 98 70-130 6 30 Duplicate (0323005-DUPl) Prepared: 10/21/2020 08:20 Analyzed: 10/21/2020 13:17 Source: AD06910-04 Spike Source O/oREC RPD Analvte Result Flaa Q Units Level Result O/oREC Limits RPD Limit Notes Carbon dioxide 24.7 2.50 mg/L 28.7 15 30 Ethane 0.00510 U 0.00600 mg/L 0.00510 U 30 Ethene 0.00510 U 0.00600 mg/L 0.00510 U 30 Methane 0.00588 0.00500 mg/L 0.00809 32 30 QM-12 Batch OJ22022 - Same FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 49 of 53 QUALITY CONTROL DATA Dissolved Gases by GC - Quality Control Batch OJ22022 - Same - Continued (� �Eo www.encolabs.com Blank (0322022-BLK1) Prepared: 10/22/2020 07:52 Analyzed: 10/22/2020 09:39 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 2.07 U 2.50 mg/L Ethane 0.00510 U 0.00600 mg/L Ethene 0.00510 U 0.00600 mg/L Methane 0.00400 U 0.00500 mg/L LCS (0722022-BS1) Prepared: 10/22/2020 07:52 Analyzed: 10/22/2020 09:00 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 49.8 2.50 mg/L 45.8 109 70-130 Ethane 0.343 0.00600 mg/L 0.323 106 70-130 Ethene 0.299 0.00600 mg/L 0.302 99 70-130 Methane 0.162 0.00500 mg/L 0.172 94 70-130 LCS Dup (O]22022-BSD1) Prepared: 10/22/2020 07:52 Analyzed: 10/22/2020 09:16 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 49.7 2.50 mg/L 45.8 109 70-130 0.3 30 Ethane 0.339 0.00600 mg/L 0.323 105 70-130 1 30 Ethene 0.297 0.00600 mg/L 0.302 98 70-130 0.7 30 Methane 0.160 0.00500 mg/L 0.172 93 70-130 2 30 Duplicate (0322022-DUP1) Prepared: 10/22/2020 07:52 Analyzed: 10/22/2020 13:42 Source: AD06965-03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Carbon dioxide 168 2.50 mg/L 130 26 30 Ethane 0.00510 U 0.00600 mg/L 0.00510 U 30 Ethene 0.00510 U 0.00600 mg/L 0.00510 U 30 Methane 0.0465 0.00500 mg/L 0.0172 92 30 QM-12 Classical Chemistry Parameters - Quality Control Batch OJ22067 - NO PREP Blank (0322067-BLK1) Prepared: 10/23/2020 12:30 Analyzed: 10/23/2020 12:59 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 0.54 U 1.0 mg/L LCS (0722067-BS3) Prepared: 10/23/2020 12:30 Analyzed: 10/23/2020 12:59 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 48 1.0 mg/L 50.0 96 85-115 Duplicate (0122067-DUP3) Prepared: 10/23/2020 12:30 Analyzed: 10/27/2020 16:42 Source: CD16586-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 36 1.0 mg/L 37 1 20 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 50 of 53 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch OJ22067 - NO PREP - Continued Matrix Spike (0322067-MS3) Prepared: 10/23/2020 12:30 Analyzed: 10/23/2020 12:59 Source: AD07020-06 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Organic Carbon 48 1.0 mg/L 50.0 2.0 92 85-115 Matrix Spike Dup (0322067-MSD1) Prepared: 10/23/2020 12:30 Analyzed: 10/23/2020 12:59 Source: AD07020-06 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Organic Carbon 48 1.0 mg/L 50.0 2.0 92 85-115 0.8 21 Batch OJ26043 - NO PREP Blank (0126043-BLK3) Prepared: 10/26/2020 15:22 Analyzed: 10/27/2020 11:08 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Organic Carbon 0.54 U 1.0 mg/L LCS (0326043-BS1) Prepared: 10/26/2020 15:22 Analyzed: 10/27/2020 11:08 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Organic Carbon 46 1.0 mg/L 50.0 92 85-115 Matrix Spike (0326043-MS3) Prepared: 10/26/2020 15:22 Analyzed: 10/27/2020 11:08 Source: AD07020-06RE3 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Organic Carbon 44 1.0 mg/L 50.0 2.3 84 85-115 QM-07 Matrix Spike Dup (0]26043-MSDi) Prepared: 10/26/2020 15:22 Analyzed: 10/27/2020 11:08 Source: AD07020-06RE3 Spike Source O/oREC RPD Analvte Result Flaq POL Units Level Result O/oREC Limits RPD Limit Notes Total Organic Carbon 43 1.0 mg/L 50.0 2.3 83 85-115 2 21 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 51 of 53 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits. QM-12 Precision between duplicate samples was outside acceptance limits. QR-04 Duplicate precision outside acceptance limits due to low analyte concentration. QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there is no impact. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 52 of 53 m 3 m obi g (7 v n m QK N D m 0 � 3 7c CA) �. �• � v Z m m o o tim o `9 � N y ,M ro W — + m O o m m ro �( ol`� W 1►� b' C-A a W o m rQ o� MNA n A o m c`n V` o V{ m � r CL g o a QO 3 a m a¢ m C7 v g •� o67 0G) G) G7 -n �► T — o Nx �o �o X x x x x x x x EAWO gIWj0 o m a v x x x x x x x Ag,As,Ba,Cd,Cr,Pb,Se D, m g10 47 is x x )t x x xM. 310 2Ahlorlds sao,NNrlce ae N m CD � ro 2 x x x x x x x oHg 3 � ♦ � z a x x x x x x x NOX 353.2 m � O m o= x x xxx x x RSK 175 + CO2 m T v m p x x x x X x x m Sulfate 300 o x x x x x x x Su de 4 x� o x x x x x x x � n w v o CD I m c •O m 7C Q m x — 'f7 a $ � 2 SO CR a o co CD � g N N 3 Q n ID E o3i N c w cr d 0 o Z a � na'i o C) r Ni O A T A a m n r 0 0 Z 0 m > Q 9 Z V �0v ..� 0 �U n -0 �m m w CD CD IN A 0 a Q O 3 Sample Preservation Verification ENCO Cary Work Order: CD16586 Project: Moore County MSW LF CA Client: S&ME, Inc. (SM004) Project #: 4358-20-043A Phase 01 Logged In: 15-Oct-20 10:09 Logged By: John C King '^,' Preservation Check Performed By: : t Date/Time: 10-IS-2-0 C ❑ 16586-01 Cont Type Pres (pH) Requirement pH Checked / In Control pH Adjusted DatelTime Adjusted Reagent Used/Comments 8 250mLP+HNO3 <2 Y)I N I NA Y I�PI 1 NA C 250mLP+ZnAc+NaOH >9 I N I NA Y I I NA D 250mLP+H2SO4 <2 Y 1 N 1 NA Y/ I NA CD16586-02 t'� t'4. Cont Type Pres (pH) Requirement pH Checked / In Control pH Adjusted Date/Time Adjusted Reagent UsedlComments B 250mLP+HNO3 <2 Y I N / NA Y //,NI / NA C 250mLP+ZnAc+NaOH >9 I N/ NA Y VIM I NA D 250mLP+H2SO4 <2 Y I N/ NA Y 16 1 NA CD16586-03 Cant Type Pres (pH) Requirement pH Checked /!; In Control pH Adjusted DatelTime Adjusted Reagent Used/Comments B 250snLP+HNO3 <2 CY I N I NA Y 1 N 1 NA C 250mLP+ZnAc+NaOH >9 1 N 1 NA Y I IY 1 NA D 254mLP+H2SO4 <2 / N I NA Y I / NA C D 16586-04 Cont Type Pres (pH) Requirement pH Checked/ In Control pH Adjusted DateMrne Adjusted Reagent UsedlComments B 250mLP+HNO3 <2 Y I N I NA Y/ N I NA C 250mLP+ZnAc+NaOH >9 I N I NA Y/ 1 NA D 250mLP+H2SO4 <2 I N/ NA Y/ N 1 NA C D 16586-05 I, grit Type Pres (pH) Requirement pH Checked 1 in Control Date/Time pH Adjusted Adlusked Reagent Used/Comments B 250mLP+HNO3 <2 Y. 1 N / NA Y 1 ! NA C 250mLP+ZnAc+NaOH >9 1 4NA I I NA D 250mLP+H2SO4 <2 Y t / / NA C:IELMNTIPrintlwko_Preservation Check. rpt Page 1 of 2 Sample Preservation Verification •• ENC• Car y Work Order: CD16586 Project: Moore County MSW LF CA Client: S&ME, Inc. (SM004) Project #: 4358-20-043A Phase 01 Logged In: 15-Oct-20 10:09 _ Lagged By: John C King � ��� `y �� t� Preservation Check Performed By: \ Date/Time: -Y) CD16586-06 Cont Type Pres (pH) Requirement pH Checked / In Control pH Adjusted DatelTime Adjusted Reagent Used/Comments B 250mLP+HNO3 <2 Y,1 N 1 NA Y I N.1 NA C 250mLP+ZnAc+NaOH >9 / N 1 NA Y / / NA D 250mLP+H2SO4 <2 / N/ NA Y I 611 NA CD16586-07 Cont Type yp Pres (pH) Requirement pH C"hecked ! In Control Adjusted Date�me PH AdAdiustecf Reagent Used/Comments B 250mLP+HNO3 <2 Y`/ N I NA Y I N/ NA C 250mLP+ZnAc+NaOH >9 1 N/ NA Y I / NA D 250mLP+H2SO4 1 <2 1 N / NA I Y J / NA 4, CD16586-08 Cont Type YP Pres (pH) Requirement pH Checked i In Control DatelTime Adjusted PH AdAdjusted Reagent Lased/Comments B 250rnLP+HNO3 <2 / N / NA Y ILiV / NA C 250mLP+ZnAc+NaOH >9 1 N/ NA Y //14 / NA D 250mLP+H2SO4 <2 N / NA Y I NA Reacient Name ID 1 pH Strip ID: Rea ent Name ID 3 4 Reacient Name ID 5 6 C:IELMNTIPrintlwko_Preservation Check. rpt Page 2 of 2 Appendix III — Historical Analytical Results TABLE 5 Summary of Historical Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SBME Project No. 4358-20-043A �IMAC=1 ug/L ug/L 'ILNO -- NO - -- -- - - - - ND NO NO -- NO - - -- -- -- -- ND NO NO NO -- NO - - -- -- -- i,n/I 1n/1'1Mn n7d I _ Nrl __ __ Nrl __ __ -. _ Nrl Nrl Nll __ __ Nll MnNrl Nrl Mn__ Nrl Arsenic u9/L 03/05/90 -- -- -- ND -- -- -- -- -- - - -- -- -- - -- - - NO - - ND ND ND -- -- -- - - - NO NC 2L = 10 ug/L ug/L 03/21/91 - - - NO -- -- -- -- -- -- -- - -- -- - -- - - NO - - NO NO NO -- -- -- - -- - NO EPA MCL = 10 ug/L ug/L 03/10/92 - - - NO -- -- -- -- -- -- -- - - - - -- - - NO - - NO NO NO -- -- -- - -- - NO ug/L 04/20/95 - - - NO NO -- -- -- -- -- -- -- - -- -- -- - - - -- - - - - NO NO NO NO -- - NO ug/L O6/27/95 _ _ _ _ __ __ __ __ __ __ __ __ _ __ -- -- _ _ _ __ _ _ _ __ __ _ __ _ __ _ NO ug/L 09/22/95 - - - NO -- -- -- -- -- -- -- -- - -- -- -- - - - -- - ND - -- NO NO NO NO -- - NO ug/L 03/28/96 - - - NO -- -- -- -- -- -- -- -- -- -- -- -- - - - -- - NO NO -- NO NO NO NO -- - NO ug/L 10/29/96 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - -- NO - - -- -- NO NO NO NO NO - NO ug/L 04/08/97 - - - NO -- ND -- NO NO NO NO NO -- - -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/29/97 - - - NO -- ND -- NO NO NO NO NO -- - -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/30/98 - - - NO -- ND -- NO NO NO NO ND - - -- -- - - -- ND - - - -- NO NO NO NO NO - NO ug/L 10/14/98 - - - NO -- ND -- NO ND NO ND ND - - -- -- - - - ND - - - -- NO ND NO NO NO - NO ug/L 04/27/99 - - - NO -- ND -- NO ND NO ND ND - - -- -- - - - ND - - - -- NO ND NO NO NO - NO ug/L 10/21/99 - - - NO -- ND -- NO ND NO ND ND - - -- -- - - - ND - - - -- NO 18 NO NO NO - NO ug/L 03/14/00 _ _ _ __ __ __ __ __ __ __ __ __ _ _ -- -- _ _ _ __ _ _ _ __ __ __ __ __ __ _ NO ug/L .1.00 - - - NO -- ND -- NO NO NO NO NO - - -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/17/00 - - - NO -- ND -- NO NO NO NO NO -- - -- -- - - - NO - - - -- NO NO NO NO NO - NO ug/L 04/10/01 - - - NO -- ND -- NO NO NO NO NO -- - -- -- - - - NO - - - -- NO NO NO NO NO - NO ug/L 10/11/01 - - - NO -- ND -- NO ND NO ND ND -- - -- -- - - - ND - - - -- NO ND NO NO NO - NO ug/L 04/11/02 - - - NO -- ND -- NO ND NO ND ND -- - -- -- - - - ND - - - -- NO ND NO NO NO - NO ug/L 10/O8/02 - - - NO -- ND -- NO ND NO ND 11 -- - -- -- - - - ND - - - -- 19 NO NO 10 NO - NO ug/L 04/09/03 - - - ND -- ND -- NO ND NO NO ND -- - -- -- - - -- ND - - - -- 11 NO NO NO 10 - NO ug/L 1.13/03 - - - NO -- ND -- -- -- NO NO NO NO NO -- -- - - -- NO - - - -- 14 17 14 14 11 - NO ug/L 04/26/04 - - - NO -- ND -- -- -- NO NO NO NO NO -- -- - - -- NO - - - -- NO NO NO NO 12 - NO ug/L 10/25/04 - - - NO -- ND -- -- -- NO NO NO NO - -- -- - - -- NO - - - -- 15 NO NO NO 14 - NO u9/L 04/04/OS - - - 10 -- 10 -- -- -- 15 10 10 10 13 -- -- - - - 10 - - - -- 10 15 10 29 10 - NO ug/L 10/04/OS - - - NO ND ND -- NO NO 13 NO ND NO NO -- -- - - - 15 - - - -- 13 15 12 21 NO - NO ug/L 04/28/06 - - - NO -- ND -- -- -- NO NO 11 NO NO -- -- - - ND NO - ND NO ND 12 NO NO 11 16 - NO ug/L 10/09/06 - - - NO -- ND -- -- -- NO NO 13 NO NO -- -- - - NO NO - ND NO ND 14 NO NO NO 11 - NO ug/L 04/24/07 - - - NO -- ND -- -- -- NO NO NO NO NO -- -- - - NO NO - ND ND ND NO NO NO 38 27 - NO ug/L 10/30/07 - - 10 NO -- ND -- -- -- NO NO NO NO NO -- -- - - NO NO - NO ND ND 3.2 J NO NO 6.9 J 7.8 J - NO ug/L 04/23/08 - - 10 NO -- ND -- -- -- NO NO NO NO NO -- -- - - NO NO - 3.2 J NO NO NO NO NO NO 2.3 J - NO ug/L 10/06/08 - - 10 NO -- ND -- -- -- NO NO NO NO NO -- -- - - NO NO - NO NO NO NO NO NO NO 7.7 J - NO ug/L 04/13/09 - - 10 NO -- ND -- -- -- NO NO 5.1 J 5.7 J NO -- -- - - NO NO - NO NO NO 8.2 J 17.1 6.6 J 11.4 10.1 J - NO ug/L 10/15/09 - - 10 5.30 J -- ND -- -- -- 5.83 J NO 6.47 J 10.3 6.56 J -- -- - - 5.54 J 4.42 J - 6.53 J 2.86 J NO 8.63 J 18.3 11.6 15.9 12.6 - NO ug/L 04/26/10 - - 10 NO -- ND -- -- -- NO NO 10.6 5.23 J ND -- -- - - ND 10.3 - 3.14 J ND 3.50 J 14.2 31.0 8.54 J 13.4 28.5 - NO ug/L 10/19/10 - - 10 5.16 J -- ND -- -- -- 10.3 ND 24.9 10.2 NO -- -- - - ND 21.2 - NO ND NO 29.5 33.0 22.6 28.0 26.6 - NO ug/L 04/18/11 - - 10 NO -- ND -- -- -- NO ND 20.0 12.5 B NO -- -- - - ND 5.05 B - 3.29 B ND 5.35 B 18.7 14.6 B 16.1 B 19.2 14.6 B - 5.39 B ug/L 10/10/11 - - 10 NO -- ND -- -- -- NO ND NO ND NO -- -- - - NO NO - NO ND 2.96 J 5.48 J 4.73 J 5.67 J 19.0 Dry - 126 J u9/L 04/17/12 - - 10 4.42 B -- NO -- -- -- NO NO NO 4.95 B NO -- -- - - NO NO - NO 4.31 B 3.32 B NO 29.4 NO 17.9 B Dry - NO ug/L 10/09/12 - - 10 NO -- NO -- -- -- 4.17 J NO 6.36 J 5.72 J 4.58 J -- -- - - NO 4.17 J - 2.90 J NO 2.91 J 9.82 J 21.6 9.74 J 10.7 Dry - NO ug/L 04/15/13 - - 10 3.97 B -- NO -- - -- NO NO NO 4.87 B NO -- -- - - 5.21 B ND - 2.87 B NO 4.492 B 17.8 NO NO 14.7 B Dry - NO ug/L 09/30/13 - - 10 NO -- NO -- - -- NO NO 9.62 J NO NO -- -- - - NO 11.5 - NO NO NO 24.5 32.0 20.3 18.0 Dry - NO ug/L 04/16/14 - - 10 NO -- NO -- - -- NO NO 8.25 J NO NO -- -- - - ND NO - NO ND NO 23.3 19.7 15.2 19.5 Dry - NO ug/L 10/15/14 5.4 - 10 Dry -- NO -- - -- NO 5.96 J NO 13.7 6.18 J -- -- - - NO NO - NO ND NO 6.99 J 1 0. 8 14.1 38.6 Dry - NO ug/L 04/15/15 5.4 - 10 NO -- NO -- - -- NO NO NO NO NO -- -- - - NO NO - NO NO NO 20.3 21.8 ND 8.41 J Dry - NO ug/L 10/07/15 5.4 - 10 NO -- NO -- - -- NO NO NO 7.45 J NO -- -- - - NO NO - NO NO NO NO 20.0 NO 32.4 8.73 J - NO ug/L 04/11/16 5.4 - 10 NO -- NO -- - -- NO NO NO 12.9 NO -- -- - - NO NO - NO NO NO 12.6 27.0 11.3 38.7 29.6 - NO ug/L 11/30/16 6.8 - 10 NO -- NO -- - -- 22.6 (ND) ND 48.1 (ND) 16.9 (ND) 12.9 (ND) -- -- - - NO 43.4 (ND) - NO NO NO 65.8 (ND) 20.4 (ND) 14.9 (ND) 85.6 (41.9) 39.6 (42.4) - NO (Dissolved) ug/L 11/30/i6 6.8 - 10 - -- -- - -- -- -- - - - -- -- - - - - - - -- - - - - - 14.4 (Verification Event) ug/L 02/09/17 6.8 - 10 NO -- -- -- - -- -- -- - - - -- -- - - -- - - - -- - - - - 40.5 (Dissolved) ug/L 02/09/17 6.8 - 10 - -- -- -- -- -- -- - - -- -- -- - - -- - - - -- - - - - 39.0 - ug/L 04/11/17 68 - 10 NO -- ND -- -- -- NO ND 7.78 J NO ND -- -- - - NO NO - NO NO ND 10.5 8.67 J NO 53.7 31.8 - NO ug/L 12/1217 6.8 - 10 NO -- NO -- -- -- NO ND 19.3 NO ND -- -- - - NO 17.8 - NO NO ND 25.9 21.5 8.49 J 53.2 25.4 - NO ug/L O6/20/18 7.6 - 10 NO -- -- ND - -- NO ND 22.7 NO ND -- -- -- - NO - NO NO NO ND 22.8 NO NO 38.6 - NO - ug/L 11/27/18 7.6 10 - NO -- -- ND - -- NO ND NO NO ND -- -- -- - NO - NO NO NO ND NO 14.9 NO 36.4 - NO NO ug/L 04/02/19 7.6 10 - NO -- -- ND - -- NO ND NO NO ND -- -- -- - NO -- NO NO NO ND NO 11.7 NO NO - NO NO ug/L 11/19/19 7.6 10 - NO -- -- ND - -- NO ND NO - -- NO NO -- - NO -- NO NO NO ND NO NO NO 36.5 - NO NO ug/L 04/07/20 7.6 10 - NO -- -- ND - -- NO ND NO - -- NO NO NO - NO -- NO - -- -- NO NO NO 23.8 - NO - u /L 10/13/20 7.6 10 - NO -- -- ND - -- -- -- NO ND NO - -- NO NO NO NO NO -- NO NO NO ND NO NO NO 64.8 - NO - i,spa..ms,.�w,ENvw,aMs�zozwasazo.w.0 Mwnoa�v aow�. iF�awo Mm.m.��amnb,,. o,. ---12ozo-2oznWw­--Ewmzo l WeMa,ea.. a,.1 a17 TABLE 5 Summary of Historical Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SBME Project No. 4358-20-043A Detected Monitoring 'M.q Active C&D Monitoring Wells Active Perfo&rnnanc C D Monitoring M Wells & NINA Wells Closed MSW Monitoring Wells & NINA Performance Monitoring Wells Offsite Constituent/Parameter Barium Unit. u9/L a, 03/05/90 St. INNIBac.k�ro"rid,. -- - - onit ring We] 35 - - - -- -- -- -- - - -- -- -- - -- for 15 the C ritoring or 0: ad MSW Landfill Pr ivate Well NC 2L = 700 ug/L ug/L 03/21/91 - - - 35 -- -- -- -- -- -- -- - - - - - - - 23 -- - 73 66 23 - - - - - - NO EPA MCL=2000 ug/L ug/L 03/10/92 - - - 30 -- -- -- -- -- -- -- - - - - - - - 23 -- - 43 69 12 - - - - - - NO ug/L 04/20/95 - - - ND ND -- -- -- -- -- -- - - - - -- - - - -- - - - -- NO NO NO NO - - NO u9/L O6/27/95 _ _ _ _ __ __ __ __ __ __ __ __ _ _ _ -- _ _ _ __ _ _ _ _ NO ug/L 09/22/95 - - - NO -- -- -- -- -- -- -- -- -- -- - -- - - - -- - NO - - ND ND ND ND - - NO ug/L 03/28/96 - - - NO -- -- -- -- -- -- -- -- -- -- - -- - - - -- - NO NO - NO NO NO NO -- - NO ug/L 10/29/96 - - - NO -- ND -- NO NO NO NO NO -- -- - -- - - -- NO - - -- -- NO NO NO NO NO - NO ug/L 04/08/97 - - - NO -- ND -- NO NO NO NO NO -- -- - -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/29/97 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/30/98 - - - NO -- ND -- NO ND NO ND ND -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/14/98 - - - ND -- ND -- NO ND NO ND ND -- -- -- -- - - -- NO - - - -- NO ND NO ND NO - NO ug/L 04/27/99 - - - ND -- ND -- NO ND NO ND ND -- -- -- -- - - -- NO - - - -- NO ND NO ND NO - NO ug/L 10/21/99 - - - ND -- ND -- NO ND NO ND ND -- - -- -- - - -- NO - - - -- NO ND NO ND NO - NO ug/L 03/14/00 _ _ _ __ __ __ __ __ __ __ __ __ __ _ -- -- _ _ __ __ _ _ _ _ __ __ __ __ __ _ NO ug/L .1.00 - - - NO -- ND -- NO NO NO NO NO -- - -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L 10/17/00 - - - NO -- ND -- NO NO NO NO NO - - -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L .10/01 - - - NO -- ND -- NO NO NO NO NO - - -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L 10/11/01 - - - NO -- ND -- NO ND NO ND ND - - -- -- - - -- NO - - - - NO ND NO ND NO - NO ug/L .1.02 - - - NO -- ND -- NO ND NO ND ND -- - -- -- - - -- NO - - - - NO ND NO ND NO - NO ug/L 10/O1/02 - - - NO -- ND -- NO ND NO ND ND -- - -- -- - - -- NO - - - - NO ND NO ND NO - NO ug/L 04/09/03 - - - NO -- ND -- NO ND NO ND ND -- - -- -- - - -- NO - - - - NO ND NO ND NO - NO ug/L 10/13/03 - - - NO -- ND -- -- -- NO NO NO NO NO -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L 04/26/04 - - - NO -- ND -- -- -- NO NO NO NO NO -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L 10/25/04 - - - NO -- ND -- -- -- NO NO NO NO -- -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L .04/05 - - - NO -- NO -- -- -- NO NO NO NO NO -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L 10/04/05 - - - NO NO NO -- NO ND NO NO NO ND NO -- -- - - - NO - - - - NO NO NO NO NO - NO ug/L 04/28/06 - - - NO -- NO -- - -- NO NO NO ND NO -- -- - - ND NO - NO NO NO ND NO ND NO ND - NO ug/L 10/09/06 - - - NO -- NO -- - - ND NO NO ND NO -- -- - - NO NO - NO NO NO ND NO ND NO ND - NO ug/L .24/07 - - - NO -- NO -- - - NO NO NO ND NO -- -- - - NO NO - NO NO NO NO NO NO NO ND - NO ug/L 10/30/07 - - 100 13.5 J -- 24.6 J -- - - 21........1 J 12..0 JJ 44...4 J J 90..8 41-.....6 J 52.. J J 46. J 65-......8 J 13-..8 J J 40.....1 17..0 J 60.....3 J 8....2 J 15...5 J 14- J ...........6 ug/L 43/08 100 . . 268 J 185 124 426 J 16 55. 31.7 J 7.2 J 57.1 J554 J 121 J595 J268 J521 J811 J 123 J -... 148 JJJ 10/06/08 00 128 J 16 14.8 J 45.7 J 20 03 584 J 41.8 J . 7598 J 409J 588 J 138 J 420 J 312 J 514 J 83.1 J 12.4 J 156ug/L J ug/L 04/13/09 100 13.5 J 41.1 J 6.1 J 17 51.3 J 13 492 5 J 674 J 4.5J 658 J 172 J 426 J 37 J 16 J 98 J 149 145 J9 u 10/15/09 .53 J 44.7 J 84J 12 72.6 69.0 J 28 3.9 67.5 J 78.6 J 2.8 J 1 4.5 J ug/L 9/L 04/2 100 9J .47 4 J . . 9 98.0J 6 480 J 5.7 J 77.4 J 43.3 J 660 J 19.8 J 39.8J 33.4 672 803 117 114.8 J 10/19/10 100 1.6 J 243 J 177 J 1 42.4 J 44 1 J 295 73 31.4 J 5.6 J 14.9 J 2J 25.2 J 39 697 1 J 1u9/L J 9 100 1J 31 286 223 J 14.1 69 J 4 J 86.1 J 50 41.9 J 73 48.8 J648 0.2 28.2 70.3uJ 1.9 J 136 75 J 11.8 54 J u9/L 10/10/11 100 14.3 J 28.6 J 26.9 J 11.3 J . 75 94 56.9 7 0.7 J 46.1 J 6.7 747 Dry 15.5 1 ug/L 04/17/12 100 J . 295 J -- -- 243 J 160 521 J 652 J 442 J 40.5 J 66.2 J 627 J750 J 21.7 J 3.9 J 30.1 J 67.5 J 84J D 155 J14 10/0912 00 5 45 J 471 101 606 520 J 6ug/L 81 J 18.8 J 39.8 J 39.7 J 64.2 J 73.0 Dry 14.7 J u/L 04/15/13 100 14.6 J 217 J 21.8 J 21.1 J 49.4 J 79.4 J 478 26.8 J 73.0 J 40.5 J 6 J 20.4 J 492.7 J 36.7 J 78.4 J 86.4 J D 146 J ug/L 09/30/13 00 124 J 342 J 2351 24.4 J 55 J 1 569 245J868 J -. 35.8 J 308.83 J 21.1 J 505 J 47.1 J 6.3 J 901 JDry 14.9 J ug/L 04/16/14 100 13.6 J 338 J 176 J255 J 467.3 J 7911.18 J 627 J 15.9 J 5.7 J 35.3 J 41.8 J 15.2 J 426 J 28.9 J 60.6 J 102 Dry 16.2 J ug/L 10/15/14 1 00 D 25. J 20.5 J 14.8 J 50.4 J 112 1 25.9 J783 33.6 J 463 J 25.5 J 493 J 31.1 J 103 98.4 J D 231 J u 04/15/5 1 1 100 56 40 219 36 49.2 J 105 14 956 J 1.7 J 46.6 J 53.3 J32.9 J 45J 28.4 J 74.7 J 9g/L 37 D 18.2 J u9/L 10/07/15 1 100 14 424 172 7.7 J 45 J 74.8 14 21.2 J 69.3 J 304 521 J 25.2 J 36J 28.6 J 88.8 J 928 J 12.6 J 1 58 ug 137 J 4 99 J 140 J3 41.5 145 1018 69.3 J 7 31.9 J 388 J 34.0 J 444 J 28.6 J 65.5 J 840 J 88 .7 J 18.5 J u 11/30/16 1 100 144 B 45 . .1 . 11 132 38.3 B 80.4 .0 . . 1 78 B ug/L g/L 04/11/7 1 100 145 43.5 J 23.2 J 230J 453 J 3 131 2 J 8.0 J 26.6 J 54.5 J 32.6 J 4 266 J 957 J 9 106 9 J 186 JJ 12/1/17 1 100 29 . 1 J 11 435 J5 J 13 35.6 J 98.2 J 1445 1ug/L 87 g/ O6/20/18 1.1 - 00 11.J 19 J 3 J 44.J 7 105 403 J - 59.9 J 26.7 J 5uL 7.0 J 31.8 J 427 J 333 J 763 J 89.3 J - 38.6 J ug/L 11/27/18 10 - 13.9 53.1 180 3% 49.4 590 110 604 68.4 305 387 3 38.9 39.2 505 78.8 323 202 uL04/02/ 9 1. 10 15.4 490 162 5 97.6 549 980 30.4 383 33.5 37.8 408 542 78.4 389 2089/ ug/L 11/1919 1.1 10 14.5 59.3 367 187 569 - 683 165 - 53.9 71.2 37.8 54.9 38.5 527 383 102 117 198 207 u/L g 7 04/0/20 1.1 . 10 1 2A 54.7 21.7 31.7 422 91.8 10.6 86.7 430 69.3 - 49 257 69 83 40.0 - u 33.4 83.8 59.5 25.9 72.8 26. 41.0 34.4 75.6 95.5 27.5 19.0 z�snaremsMeq+,Ervvw,a•ns�zoswasasuw.0 Mwrecwm.- Lrcawo ram-- --uaw-12-2osnw-­-ray Ewmzos 1-o.a.w.. PJe2m17 TABLE 5 Summary of Historical Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SBME Project No. 4358-20-043A Detected M Active C&D Monitoring Wells Active C&D Perfor Monitoring Wells & NINA Wells Closed MSW Monitoring Wells & NINA Performance Monitoring Wells Offsite -it-ing Constituent/Parameter Cadmium Unit. ug/L a, 03/05/90 St. JENkc1grourid -- - - '.ran __ _ ND -- -- - -- -- -- -- -- -- -- -- -- - -- arc for t a ND or o:M nitoring ad MSW -- Landfill - ND ND ND - -- -- -- - -- Private Well ND NC 2L=2 ug/L ug/L 03/21/91 - - - ND -- - - -- -- -- -- - - - - - - - NO -- - NO ND ND - - - - - - NO EPA MCL = 5 ug/L ug/L 03/10/92 - - - ND -- - - -- -- -- -- - - - - - - - NO -- - ND ND NO - - - - - - NO ug/L 04/20/95 - - - ND ND - - -- -- -- -- - - - - -- - - - -- - - - -- NO NO NO NO - - NO ug/L O6/27/95 _ _ _ _ __ __ __ __ __ __ __ __ _ _ _ -- _ _ _ __ _ _ _ __ _ _ _ _ _ _ NO ug/L 09/22/95 - - - NO -- -- -- -- -- -- -- -- -- -- - -- - - - -- -- NO -- -- NO NO NO NO - - NO ug/L 03/28/96 - - - NO -- -- -- -- -- -- -- -- -- -- -- -- - - - -- - NO ND -- NO NO NO NO -- - NO ug/L 10/29/96 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - -- NO - - -- -- NO NO NO NO NO - NO ug/L 04/08/97 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/29/97 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/30/98 - - - NO -- ND -- NO ND NO ND ND -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/14/98 - - - ND -- ND -- NO ND NO ND ND -- -- -- -- - - -- NO - - - -- NO ND NO ND NO - NO ug/L 04/27/99 - - - ND -- ND -- NO ND NO ND ND -- -- -- -- - - -- NO - - - -- NO ND NO ND NO - NO ug/L 10/21/99 - - - ND -- ND -- NO ND NO ND ND -- - -- -- - - -- NO - - - -- NO ND NO ND NO - NO ug/L 03/14/'0 _ _ _ __ __ __ __ __ __ __ __ __ __ _ -- -- _ _ __ __ _ _ _ __ __ __ __ __ __ _ NO ug/L .1.00 - - - NO -- ND -- NO NO NO NO NO -- - -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/17/00 - - - NO -- ND -- NO NO NO NO NO - - -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/10/01 - - - NO -- ND -- NO NO NO NO NO - - -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/11/01 - - - NO -- ND -- NO ND NO ND ND - - -- -- - - -- NO - - - -- NO ND NO ND NO - NO ug/L 04/18/02 - - - NO -- ND -- NO ND NO ND ND -- - -- -- - - -- NO - - - -- NO ND NO ND NO - NO ug/L 10/08/02 - - - NO -- ND -- NO ND NO ND ND -- - -- -- - - -- NO - - - -- NO ND NO ND NO - NO ug/L 04/09/03 - - - NO -- ND -- NO ND NO ND ND -- - -- -- - - -- NO - - -- -- NO ND NO ND NO - NO ug/L 1.13/03 - - - 2 -- ND -- -- -- NO NO NO NO NO -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/26/04 - - - 1 -- ND -- -- -- NO NO NO NO NO -- -- - - -- NO - - - -- 1 NO NO NO NO - NO ug/L 10/25/04 - - - 1 -- ND -- -- -- NO NO NO NO -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/04/05 - - - NO -- ND -- -- -- NO NO NO NO NO -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 1.04/05 - - - NO ND ND -- NO ND NO NO ND NO NO -- -- - - - NO - - - -- NO NO NO NO NO - NO ug/L 04/28/06 - - - NO -- ND -- -- -- NO NO ND NO 2 -- -- - - ND NO - ND ND ND NO 1 NO 1 2 - NO ug/L 10/09/06 - - - NO -- NO -- -- -- NO NO ND NO NO -- -- - - ND NO - ND ND ND NO NO NO NO NO - NO ug/L 04/24/07 - - - NO -- NO -- -- -- NO NO ND NO NO -- -- - - ND NO - ND ND ND NO NO NO NO NO - NO ug/L 10/30/07 - - 1 NO -- NO -- -- -- NO NO NO NO NO -- -- - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 04/23/08 - - 1 NO -- NO -- -- -- NO NO NO NO NO -- -- - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/06/08 - - 1 NO -- NO -- -- -- NO NO NO NO NO -- -- - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/15/09 - - 1 NO -- NO -- -- -- NO NO NO NO NO -- -- - - NO NO - ND NO 0.487 J NO NO NO NO NO - NO ug/L 04/26/10 - - 1 NO -- NO -- -- -- NO NO NO NO NO -- -- - - NO NO - ND NO NO NO NO NO NO NO - NO ug/L 10/19/10 - - 1 NO -- NO -- -- -- NO NO ND NO NO -- -- - - NO NO - ND ND ND NO NO NO NO NO - NO ug/L 04/18/11 - - 1 NO -- NO -- -- -- NO NO ND NO NO -- -- - - NO NO - ND ND ND NO NO NO NO NO - NO ug/L 10/10/11 - - 1 NO -- NO -- -- -- NO NO ND NO 0.407 J -- -- - - NO NO - ND ND ND NO 0.685 J NO NO Dry - NO ug/L 04/17/12 - - 1 NO -- NO -- -- -- NO NO ND NO NO -- -- - - NO NO - ND ND ND NO NO NO NO Dry - NO ug/L 10/09/12 - - 1 NO -- NO -- -- -- NO NO NO NO NO -- -- - - NO NO - ND NO NO NO NO NO NO Dry - NO ug/L 04/15/13 - - 1 NO -- NO -- -- -- NO NO NO NO NO -- -- - - NO NO - ND NO NO NO NO NO NO Dry - NO ug/L 09/30/13 - - 1 NO -- NO -- -- -- NO NO NO NO NO -- -- - - NO 0.882 J - ND NO NO 1.15 0.722 J NO NO Dry - NO ug/L 04/16/14 - - 1 NO -- NO -- -- -- NO NO NO NO NO -- -- - - NO NO - ND NO NO NO NO NO NO Dry - NO ug/L 10/15/14 0.36 - 1 Dry -- NO -- -- -- NO NO ND NO NO -- -- - - NO NO - ND ND ND NO NO NO NO Dry - NO ug/L 04/15/15 0.36 - 1 NO -- NO -- -- -- NO NO ND NO NO -- -- - - NO NO - ND ND ND NO ND NO NO Dry - NO ug/L 10/07/15 0.36 - 1 NO -- NO -- -- -- NO NO ND NO NO -- -- - - NO NO - ND ND ND NO NO NO NO NO - NO ug/L 04/11/i6 0.36 - 1 NO -- NO -- -- -- NO NO ND NO NO -- -- - - NO NO - ND ND ND NO NO NO NO NO - NO u9/L 11/30/16 0.36 - 1 NO -- NO -- - -- NO NO NO NO NO -- -- - - NO NO - ND ND ND ND ND ND ND ND - NO ug/L 04/11/17 0.36 - 1 NO -- NO -- - -- NO NO NO NO NO -- -- - - NO NO -- ND NO NO 0.585 J NO NO 0.696 J NO - NO ug/L 12/12/17 0.36 - 1 NO -- 0.425 J -- - -- NO NO NO NO NO -- -- - - NO NO -- ND NO NO NO NO 0.734 J NO NO - 0.371 J ug/L O6/20/18 0.36 - 1 NO -- -- 0.500 B - -- 0.367 B NO NO NO NO -- -- - - NO -- NO NO NO NO NO NO NO NO -- NO - ug/L 11/27/18 0.36 1 - NO -- -- NO - -- NO NO NO NO NO -- -- - - NO -- NO NO ND ND NO NO NO NO -- NO NO ug/L 04/02/19 0.36 1 - NO -- -- NO - -- NO NO NO NO NO -- -- - - NO -- NO NO ND ND NO NO ND NO -- NO NO ug/L 11/19/19 0.36 1 - NO -- -- NO - -- NO NO 0.409 J - - NO NO - - NO - NO NO NO NO NO NO ND NO - NO NO ug/L 04/07/20 0.36 1 - NO -- -- NO - -- NO NO NO - - ND NO NO - NO - NO - - - NO NO ND NO - NO - ug/L 10/13/20 0.36 1 NO 1.09 1.03 NO 1.93 NO NO 1.26 NO NO 1.11 NO NO NO 2.16 1.57 1.67 0.662 J 1.92 Chromium u9/L 03/05/90 -- -- - ND - - -- - -- -- -- -- - - -- -- - - ND - - ND NO NO -- -- -- -- - - ND NC 2L = 10 ug/L ug/L 03/21/91 - - - NO -- -- -- -- -- -- -- - - -- -- -- - - NO - - NO 12 10 - -- -- -- -- - NO EPA MCL = 100 ug/L ug/L 03/10/92 - - - NO -- -- -- -- -- -- -- - - - -- -- - - NO - - NO NO NO - -- -- -- -- - NO ug/L 04/20/95 - - - NO 15 -- -- -- -- -- -- - - - -- -- - - - -- - - -- - NO NO 12 7 -- - NO ug/L O6/27/95 _ _ _ __ __ __ __ __ __ __ __ _ __ _ __ __ _ _ _ __ _ __ __ _ __ __ __ __ __ _ NO ug/L 09/22/95 - - - ND -- -- -- -- -- -- -- -- -- - -- -- - - - -- - NO - - NO ND NO NO -- - NO ug/L 03/28/96 - - - ND -- -- -- -- -- -- -- -- -- - -- -- - - - -- - NO NO - NO ND NO NO -- - NO ug/L 10/29/96 - - - NO -- NO -- NO NO 36 NO ND -- - -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L 04/08/97 - - - NO -- ND -- NO NO NO NO NO -- - -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L 10/29/97 - - - NO -- ND -- NO NO NO NO NO -- - -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L 04/30/98 - - - NO -- ND -- NO NO NO NO NO -- - -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L 10/14/98 - - - NO -- ND -- NO NO 24 NO NO -- - -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L 04/27/99 - - - NO -- ND -- NO NO NO NO ND -- - -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/21/99 - - - NO -- ND -- NO NO NO NO ND -- - -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 03/14/00 _ _ _ __ __ __ __ __ __ __ __ __ __ _ -- -- _ _ __ __ _ _ _ __ __ __ __ __ __ _ NO ug/L 04/19/00 - - - NO -- ND -- NO NO NO NO ND - - -- -- - - -- 10 - - - -- NO NO NO NO NO - NO ug/L 10/17/00 - - - NO -- ND -- NO NO NO NO NO - - -- -- - - - NO - - - -- NO NO NO NO NO - NO ug/L 04/10/01 - - - NO -- ND -- NO NO NO NO NO - - -- -- - - - NO - - - -- NO NO NO NO NO - NO ug/L 10/11/0, - - - NO -- ND -- NO NO NO NO NO - - -- -- - - - NO - - - -- NO NO NO NO NO - NO ug/L 04/18/02 - - - NO -- ND -- NO NO NO NO NO -- - -- -- - - - NO - - - -- NO NO NO NO NO - NO ug/L 10/08/02 - - - NO -- ND -- NO ND NO NO ND -- - -- -- - - - NO - - - -- NO NO NO NO NO - NO ug/L 04/09/03 - - - 20 -- ND -- NO 28 44 14 ND -- - -- -- - - - 73 - - - -- NO NO NO 11 NO - NO ug/L 10/13/03 - - - NO -- ND -- -- -- NO ND ND NO NO -- -- - - - NO - - - - NO ND NO NO NO - NO ug/L 04/26/04 - - - NO -- ND -- -- -- 88 ND ND NO NO -- -- - - - 27 - - - - NO ND NO 19 NO - NO ug/L 10/25/04 - - - NO -- ND -- -- -- NO NO NO NO - -- -- - - - NO - - - - NO NO NO NO NO - NO u9/L 04/04/05 - - - NO -- ND -- -- -- NO NO NO NO NO -- -- - - - NO - - - -- NO NO NO NO NO - NO ug/L 10/04/05 - - - NO NO ND -- NO NO 16 NO NO NO NO -- -- - - - NO - - - -- NO NO NO NO NO - NO ug/L 04/28/06 - - - NO -- ND -- -- -- NO NO NO NO NO -- -- - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/09/06 - - - NO -- ND -- -- -- NO NO NO NO NO -- -- - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 04/24/07 - - - ND -- ND -- -- -- NO ND ND NO NO -- -- - - ND ND - NO ND ND NO ND NO NO NO - NO ug/L 10/30/07 - - 10 ND -- ND -- -- -- NO ND ND NO ND -- -- - - 2.4 J ND - NO ND ND NO ND NO ND NO - 2.8 J ug/L 04/23/08 - - 10 NO -- ND -- -- -- NO ND ND NO ND -- -- - - ND ND - NO ND ND NO ND NO ND NO - NO ug/L 10/06/08 - - 10 NO -- ND -- -- -- NO NO ND NO NO -- -- - - ND ND - NO ND NO NO NO NO NO NO - NO ug/L 04/13/09 - - 10 NO -- ND -- -- -- NO NO NO NO NO -- -- - - NO NO - NO NO NO NO 1.1 J NO NO NO - NO ug/L 10/15/09 - - 10 NO -- ND -- -- -- NO NO NO NO NO -- -- - - NO NO - NO NO 1.02 J NO NO NO NO NO - NO u9/L 04/26/10 - - 10 NO -- ND -- -- -- ND NO NO NO NO -- -- - - NO NO - NO NO NO NO NO NO ND NO - NO ug/L 10/19/10 - - 10 5.84 J -- ND -- -- -- NO NO NO NO NO -- -- - - 3.07 J NO - NO NO NO NO NO NO NO NO - NO ug/L 04/18/11 - - 10 NO -- 2.00 J -- -- -- NO NO ND NO NO -- -- - - 1.02 J ND - 1.90 J ND ND NO NO NO NO ND - NO ug/L 10/10/11 - - 10 NO -- ND -- -- -- NO NO ND NO NO -- -- - - NO ND - NO ND ND NO NO NO NO Dry - NO ug/L 04/17/12 - - 10 3.10 J -- ND -- -- -- NO NO ND NO ND -- -- - - NO ND - NO ND ND NO NO NO 2.25 J Dry - NO ug/L 10/09/12 - - 10 1.65 J -- ND -- -- -- NO NO ND NO NO -- -- - - 3.37 J ND - NO ND ND NO NO NO NO Dry - NO ug/L 04/15/13 - - 10 NO -- ND -- -- -- NO NO NO NO NO -- -- - - NO NO - NO NO NO 2.64 B NO NO NO Dry - NO ug/L 09/30/13 - - 10 NO -- ND -- -- -- NO NO NO NO NO -- -- - - 2.25 J NO - NO NO NO NO NO NO NO Dry - NO ug/L 04/16/14 - - 10 NO -- ND -- -- -- NO NO NO NO NO -- -- - - 1.88 J NO - NO NO NO NO NO NO NO Dry - NO ug/L 10/15/14 1.4 - 10 Dry -- ND -- -- -- NO NO NO 2.35 J NO -- -- - - 5.71 J NO - 1.83 J NO NO NO NO NO NO Dry - NO ug/L 04/15/15 1.4 - 10 NO -- ND -- -- -- NO NO ND 2.49 J ND -- -- - - NO 10.9 - ND ND 1.64 J ND ND ND ND Dry - NO ug/L 10/07/15 1.4 - 10 NO -- ND -- -- -- NO NO ND 2.00 J NO -- -- - - 2.97 J NO - NO ND ND NO NO NO NO NO - NO ug/L 04/11/16 1.4 - 10 NO -- ND -- -- -- NO ND ND 4.32 J ND -- -- - - NO ND - NO ND ND NO ND NO ND 4.36 J - NO ug/L 11/30/16 1.4 - 10 ND -- NO -- -- -- NO ND ND NO ND -- -- - - NO ND - NO ND ND NO ND NO ND 1.42 J - NO u9/L 04/11/17 1.4 - 10 NO -- NO -- -- -- NO NO NO 2.31 J NO -- - - - 2.22 J NO -- NO NO NO NO NO NO NO NO - NO ug/L 12/12/17 1.4 - 10 NO -- NO -- -- -- NO NO NO NO NO -- -- - - 1.88 J NO -- NO NO NO NO NO NO NO NO - NO ug/L O6/20/18 1.4 - 10 NO -- -- NO -- -- NO NO NO NO NO -- -- - - 1.55 J -- NO NO NO NO NO NO NO NO - NO - ug/L 11/27/18 1.4 10 - NO -- -- NO -- -- NO NO NO NO NO -- -- - - NO -- NO NO NO NO NO NO NO NO - NO NO ug/L 04/02/19 1.4 10 - NO -- -- NO -- -- NO NO NO NO 2.02 J -- -- - - NO - NO NO NO NO NO NO NO NO - NO NO ug/L 11/19/19 1.4 10 - NO -- -- NO -- -- NO ND ND - - ND ND - - NO - NO NO ND ND NO ND NO ND - NO ND ug/L 04/07/20 1.4 10 - NO -- -- NO -- -- NO NO NO - - NO NO NO - 3.46 J - 3.68 J - - -- NO NO NO NO - NO - ug/L 10/13/20 1.4 10 - NO -- -- NO -- -- -- -- NO ND NO - - NO 1.59 J NO NO NO -- NO NO NO NO NO NO NO NO - NO - zssnareesMeoia�Euvw,o•car�zozwass-zuw.0 Mwncwm .-ircawa ram-­--uaw-rrzozo-z-wu­-- Ewmzo 1-oms.eu.. Page 3 d17 TABLE 5 Summary of Historical Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SBME Project No. 4358-20-043A Detected Monitor! P. .. Constituent/ rameter Cohalt NC 2L IMAC = 1 ug/L nitl%§L ug/L ug/L ug/L ug/L ug/L ug/L 06/20/18 11/27/18 04/02/19 11/1 9/1 9 04/07/20 10/13/20 JEEkc1.rno..nd 1.4 1.4 1.4 1.4 1.4 1.4 -- 10 10 10 10 10 10 - - - - - i,.ri we] ND ND ND NO NO NO -- -- -- -- -- -- + -- - - - - -- •- 2.13 2.03 2.55 ND ND 1.49 J -- J -- J -- -- -- J -- r -- -- -- -- -- -- NO NO NO NO NO Active C&D r - ND ND ND ND ND ND Monitoring Wells r- ND ND ND ND 1.50 J 1.51 J ND ND ND - - -- .r 67 J-- 6.53 J 6.27 J -- -- -- - - NO NO NO • - - NO NO 1.48 J - - - NO NO - - - - NO Active Performanc: forthe NO NO NO NO NO C&D Monitoring CIO Wells Monitoring ad MSW Landfill -- -- - - - & NINA Wells - NO 1.63 J ND ND NO - - - - - -- - - - - Closed -- -- -- - - MSW Monitoring Wells -- -- -- -- -- & MNA Performance -- -- -- -- -- Monitoring -- -- -- -- -- Wells -- -- -- -- - - - - - - - - - - - Offsite Private Well - - - - - Copper ug/L 03/05/90 -- -- -- ND -- - -- -- -- -- -- -- - - -- -- - - ND -- - 10 NO ND -- -- -- -- -- - NO NC 2L=1000 ug/L ug/L 03/21/91 - - - NO -- -- -- -- -- -- -- -- -- -- -- -- - - NO - - 14 12 NO -- -- -- - -- - NO EPA MCL = 1300 ug/L ug/L 03/10/92 - - - NO -- -- -- -- -- -- -- -- -- -- -- -- - - NO - - NO 110 NO -- -- -- - -- - NO ug/L 04/20/95 - - - NO 9 -- -- -- -- -- -- -- -- -- -- -- - - - -- - - - - NO NO 14 11 -- - NO ug/L O6/27/95 _ _ _ _ __ __ __ __ __ __ __ __ _ __ __ __ _ _ _ __ _ _ _ __ __ __ __ _ __ _ NO ug/L 09/22/95 - - - NO -- -- -- -- -- -- -- -- - -- -- -- - - - -- - ND - -- NO NO NO NO -- - NO ug/L 03/28/96 - - - NO -- -- -- -- -- -- -- -- -- -- -- -- - - - -- - ND NO -- NO NO NO NO -- - NO ug/L 10/29/96 - - - NO -- NO -- NO ND NO ND ND -- -- -- -- - - -- NO - - -- -- NO NO NO NO NO - NO ug/L 04/08/97 - - - NO -- NO -- NO NO NO NO NO -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/29/97 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/30/98 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/14/98 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/27/99 - - - ND -- ND -- NO ND NO ND ND -- - -- -- - - -- NO - - - -- NO ND NO ND NO - NO ug/L 10/21/99 - - - ND -- ND -- NO ND NO ND ND -- - -- -- - - -- NO - - - -- NO ND NO ND NO - NO ug/L 03/14/00 _ _ _ __ __ __ __ __ __ __ __ __ __ _ -_ -- _ _ __ __ _ _ _ __ __ __ __ __ __ _ NO ug/L .19/00 - - - ND -- ND -- NO ND NO ND ND - - -- -- - - -- NO - - - -- NO ND NO ND NO - NO ug/L 10/17/00 - - - NO -- ND -- NO NO NO NO NO - - -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L .10/01 - - - NO -- ND -- NO NO NO NO NO - - -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/11/01 - - - NO -- ND -- NO NO NO NO NO - - -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/18/02 - - - NO -- ND -- NO NO NO NO NO - - -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L 10/O1/02 - - - NO -- ND -- NO NO NO NO ND - - -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L .09/03 - - - NO -- ND -- NO NO NO NO ND - - -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L 10/13/03 - - - NO -- ND -- -- -- NO NO ND NO NO -- -- - - - NO - - - - NO NO NO NO NO - NO ug/L 04/26/04 - - - NO -- ND -- -- -- NO NO ND NO NO -- -- - - - NO - - - -- NO NO NO NO NO - NO ug/L 10/25/04 - - - NO -- ND -- -- -- NO NO NO NO - -- -- - - - NO - - - -- NO NO NO NO NO - NO ug/L .04/05 - - - NO -- ND -- -- - NO NO NO NO NO -- -- - - - NO - - - -- NO NO NO NO NO - NO ug/L 10/04/05 - - - NO ND ND -- NO NO NO NO NO NO NO -- -- - - - NO - - - -- NO NO NO NO NO - NO ug/L 04/28/06 ug/L 10/09/06 ug/L .24/07 ug/L 10/30/07 ug/L 04/23/08 ug/L O6/20/18 1.6 - 10 2.28 B -- -- NO -- -- NO NO ND 1.90 B NO - - - - 5.70 B -- NO - - -- NO NO - - - ug/L 11/27/18 1.6 10 - NO -- -- NO -- -- NO NO NO NO NO - - - - ,.17 B - NO - - - -- - - - - - - ug/L 04/02/19 1.6 10 - NO -- -- NO -- -- NO NO NO NO NO - - - - 3.37 J - NO - - - - - - - - - - u9/L 11/19/19 1.6 10 - NO -- -- NO -- -- NO 2.75 J NO - - NO 2.96 J - - 1.76 J - NO - - - - - - - - - - ug/L 04/07/20 1.6 10 - NO -- -- NO -- -- NO NO NO - - NO NO NO - 1.75 J - NO - - - - - - -- - - - ug/L 10/13/20 1.6 10 - NO -- -- NO -- -- -- - ND ND 3.26 J - - ND 2.97 J 1.99 2.03 J 3.81 J -- NO - - - - - -- -- - - - Lead u9/L 03/05/90 __ __ __ 16 14 __ _ 7 29 6 __ __ __ __ __ _ NO NC 2L = 15 ug/L ug/L 03/21/901 - - - NO -- -- -- -- -- -- - -- - - -- -- - - ND -- - NO ND NO -- - -- -- - - ND EPA MCL = 15 ug/L' ug/L 03/10/92 - - - 14 -- -- -- -- -- -- - -- - - -- -- - - 25 -- - 10 39 12 -- - -- -- -- - NO ug/L 04/20/95 - - - NO 14 -- -- -- -- -- - -- - - -- -- - - - -- - - - -- 7 NO 18 16 -- - NO ug/L O6/27/95 _ _ _ _ __ __ __ __ __ __ _ __ __ _ -- -- _ _ _ __ _ _ _ __ __ _ __ __ __ _ NO ug/L 09/22/95 - - - NO -- -- -- -- -- - - -- -- - -- -- - - - -- - NO - -- NO NO NO NO -- - NO ug/L 03/28/96 - - - NO -- -- -- -- -- - -- -- -- - -- -- - - - -- - NO NO -- NO NO NO NO -- - NO ug/L 10/29/96 - - - NO -- NO -- NO NO 12 NO ND -- - -- -- - - -- 13 - - - -- NO NO NO NO NO - 39 ug/L 0 08/97 - - - NO -- NO -- NO NO ND NO ND -- - -- -- - - -- NO - - - -- NO NO NO NO NO - 34 ug/L 10/29/97 - - - NO -- ND -- NO NO ND NO ND -- - -- -- - - - NO - - - -- NO NO NO NO NO - 70 ug/L 04/30/98 - - - NO -- ND -- NO NO ND NO ND -- -- -- -- - - - NO - - - -- NO NO NO NO NO - 42 ug/L 10/14/98 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - - NO - - - -- NO NO NO NO NO - 26 ug/L 04/27/99 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - - NO - - - -- NO NO NO NO 13 - 166 ug/L 10/21/99 - - - NO -- ND -- NO NO NO NO NO -- - -- -- - - -- NO - - - -- NO NO NO NO NO - 135 ug/L 03/14/00 _ _ _ _ __ __ __ __ _ __ _ __ __ _ __ __ _ _ __ __ _ _ _ __ __ _ __ _ _ _ NO ug/L .19/00 - - - NO -- ND -- NO NO NO NO NO -- - -- -- - - - NO - - - -- NO NO NO NO NO - NO ug/L 10/17/00 - - - ND -- ND -- NO ND NO ND ND - - -- -- - - - ND - - - -- NO ND NO ND NO - NO ug/L .10/01 - - - ND -- ND -- NO ND NO ND ND - - -- -- - - - ND - - - -- NO ND NO ND 10 - 14 ug/L 10/11/01 - - - NO -- ND -- NO ND NO ND ND - - -- -- - - -- ND - - - -- NO NO NO ND NO - NO ug/L .18/02 - - - NO -- ND -- NO ND NO NO ND - - -- -- - - -- ND - - - -- NO NO NO NO NO - NO ug/L 10/08/02 - - - NO -- ND -- NO NO NO NO NO -- - -- -- - - -- ND - - - -- NO NO NO NO NO - NO ug/L 04/09/03 - - - 10 -- ND -- NO 15 11 NO NO -- - -- -- - - -- 48 - - - -- NO 13 NO NO 19 - NO ug/L 10/13/03 - - - NO -- ND -- -- -- NO NO NO NO NO -- -- - - -- NO - - - -- NO NO NO NO ND - 11 ug/L 04/26/04 - - - NO -- ND -- -- -- 20 NO NO NO NO -- -- - - -- 12 - - - -- NO NO NO NO NO - NO ug/L 10/25/04 - - - NO -- NO -- -- -- NO NO ND NO - -- -- - - -- NO - - -- -- NO NO NO NO NO - NO ug/L .04/05 - - - NO -- NO -- -- -- 19 NO ND NO 70 -- -- - - -- 15 - - -- -- NO 12 NO 14 NO - i6 ug/L 10/04/05 - - - NO NO NO -- NO ND 24 NO ND NO NO -- -- - - -- 19 - - -- -- NO 11 NO NO NO - 17 ug/L 04/28/06 - - - NO -- NO -- -- -- ND NO ND NO NO -- -- - - NO NO - NO NO ND NO NO NO NO 13 - 18 ug/L 10/09/06 - - - NO -- NO -- -- -- NO NO NO NO NO -- -- - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L .24/07 - - - NO -- NO -- - -- NO NO NO NO NO -- -- - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/30/07 - - 10 NO -- NO -- - - 3.1 J NO 3.9 J 2.6 J NO -- -- - - NO 15.9 - NO NO NO 4.6 J 5.2 J 6.5 J 2.6 J 2.5 J - 8 6.J ug/L 04/23/08 - - 10 NO -- NO -- - - NO NO NO NO NO -- -- - - NO 4.3 J - NO NO NO NO NO NO NO NO - 15.8 ug/L 10/06/08 - - 10 NO -- ND -- - - NO NO NO 2.2 J NO -- -- - - 9.4 J 5.0 J - NO ND ND 29 J 4.9 J ND NO 2.2 J - 13.4 ug/L 04/13/09 - - 10 NO -- ND -- - - 3.1 J NO 6.3 J 4.6 J ND -- -- - - ND 2.4 J - NO 2.1 J 2.3 J 14 J 5.2 J 6.5 J 6.4 J 5.5 J - 10.4 ug/L 10/15/09 - - 10 NO -- ND -- - - NO ND NO NO NO -- -- - - NO 2.86 J - NO ND ND ND 3.90 J NO NO 2.27 J - 3.37 J ug/L 04/26/10 - - 10 NO -- ND -- - - 3.90 J ND 3.82 J 2.85 J 2.27 J -- -- - - ND 5.86 J - ND 2.47 J ND 3.17 J 4.54 J 3.95 J 3.09 J 3.89 J - 2.18 J ug/L 10/19/10 - - 10 4.34 J -- ND -- -- -- NO NO 2.07 J 2.21 J NO -- -- - - 3.45 J NO - NO NO NO NO NO 1.92 J NO ND - 8.93 J ug/L 04/18/11 - - 10 NO -- 2.78 J -- - - 2.78 J NO 5.09 J 2.79 J NO -- -- - - 2.00 J 4.75 J - NO NO NO 5.57 J 5.07 J 6.87 J NO 5.19 J - 19.0 ug/L 10/10/11 - - 10 NO -- ND -- - - NO NO NO NO NO -- -- - - NO NO - NO NO NO NO NO NO NO Dry - ND u9/L 04/17/12 - - 10 NO -- ND -- - - NO NO NO NO NO -- -- - - 2.26 J NO - NO NO NO NO 4.08 J NO NO Dry - 16.6 ug/L 10/09/12 - - 10 NO -- ND -- - - NO NO 3.49 J NO NO -- -- - - 2.51 J 3.21 J - NO NO NO 3.89 J 2.89 J NO NO Dry - 20.6 ug/L 04/15/13 - - 10 NO -- NO -- - - NO ND NO ND ND -- -- - - 2.11 J NO - NO ND ND NO ND ND ND Dry - 20.4 ug/L 09/30/13 - - 10 NO -- ND -- - - 2.41 J ND 4.05 J NO NO -- -- - - 2.75 J 7.30 J - NO ND ND 6.67 J 5.81 J 5.32 J 3.31 J Dry - 37.3 ug/L 04/16/14 - - 10 NO -- ND -- - - 3.25 J ND 4.17 J NO 8.96 J -- -- - - 3.06 J 2.54 J - NO ND ND 5.24 J 7.02 J 4.95 J 2.83 J Dry - 60.5 ug/L 10/15/14 2.1 - 10 Dry -- ND -- - - ND NO NO NO NO -- -- - - NO NO - NO ND ND ND NO ND NO Dry - 18.3 ug/L 04/15/15 2.1 - 10 NO -- ND -- - - NO NO NO ND NO -- -- - - NO 9.49 J - NO NO ND NO NO NO NO Dry - 26.2 ug/L 10/07/15 2.1 - 10 NO -- ND -- - - NO NO NO NO NO - - - - 4.58 J 123 J - 3.55 J NO NO 3.21 J 4.36 J NO 5.90 J 6.76 J - 22.2 ug/L 04/11/16 2.1 - 10 NO -- ND -- - - NO NO NO NO NO - - - - NO NO - NO NO NO NO NO NO NO 4.87 J - 21.0 ug/L 11/30/16 3.1 - 10 NO -- ND -- - - NO NO NO NO NO - - - - NO NO - NO NO NO NO NO NO NO NO - 11.5 ug/L 04/11/17 3.1 - 10 NO -- ND -- - - NO NO NO NO NO -- -- - - 4.48 J NO -- NO ND ND NO NO NO NO NO - 38.0 ug/L 12/12/17 3.1 - 10 NO -- NO -- - - 3.37 J NO 7.48 J NO NO -- -- - - NO NO -- NO ND ND 7.80 J NO 3.33 J NO 5.91 J ug/L O6/20/18 3.1 - 10 NO -- -- NO -- -- NO NO NO NO NO -- -- - - ND - NO NO ND ND ND NO NO NO - NO - ug/L 11/27/18 3.1 10 - NO -- -- 3.42 J -- -- NO NO ND NO NO -- -- - - ND -- NO NO ND ND ND NO NO NO - NO 23.7 ug/L 04/02/19 3.1 10 - NO -- -- NO -- -- NO NO NO NO NO -- - - - NO -- NO NO NO NO NO NO NO NO - 23.8 22.4 ug/L 11/19/19 3.1 10 - NO -- -- NO -- -- NO NO NO -- -- NO NO - - NO -- NO NO NO NO NO NO NO NO - NO 28.3 ug/L 04/07/20 3.1 10 - NO -- -- NO -- -- NO NO NO -- -- NO NO NO - NO -- NO - - -- NO NO NO NO -- NO - ug/L 10/13/20 3.1 10 - NO -- -- 6.92 - -- -- -- 4.49 J ND 11.2 -- -- NO NO 7.49 NO NO -- NO NO NO NO 9.32 J 10.9 9.86 6.58 J -- 9.94 J 11.4 zssnareesMeoia�Euvw,o•carwozwass-zo-wu Mwncwmy aamre ircawa ram�m.��a+T�so+ se�uawa�e.auaM rrzozo-zoz+�wwu�w.u.wm ra.Ewmzozo-+owams.err. cwnw.a�.ss. Page 4 of 17 TABLE 5 Summary of Historical Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SBME Project No. 4358-20-043A Detected Monitoring 'M.q Active C&D Monitoring Wells Active C&D Performanc Monitoring Wells & NINA Wells Closed MSW Monitoring Wells & NINA Performance Monitoring Wells Offsite Constituent/Parameter Mercury Unit. ug/L a, 03/05/90 INNIBackgro.nd -- - - onitoring We] I 0.5 - - - -- -- -- -- - - -- -- -- - -- for t h a ND o:M ritoring Cl ed`MSW Landfill -- - ND 0.5 ND -- -- -- -- -- -- Private Well ND NC 2L = 1 ug/L ug/L 03/21/91 - - - 0.6 -- -- -- -- -- -- -- - - - - - - - 0.6 -- - 0.8 2.4 0.6 - - -- - - - NO EPA MCL=2 ug/L ug/L 03/10/92 - - - 0.7 -- -- -- -- -- -- -- - - - - - - - 1.1 -- - ND 6 1.3 - - -- - - - NO ug/L 04/20/95 - - - ND 0.4 -- -- -- -- -- -- - - - - -- - - - -- - - - -- NO NO 1.2 0.3 - - NO ug/L O6/27/95 NO ug/L 09/22/95 - - - NO -- -- -- -- -- -- -- -- -- -- - -- - - - -- -- NO -- -- NO NO NO NO - - NO ug/L 03/28/96 - - - NO -- -- -- -- -- -- -- -- -- -- -- -- - - - -- - NO ND -- NO NO NO NO - - NO ug/L 10/29/96 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - -- NO - - -- -- NO NO NO NO NO - NO ug/L 04/08/97 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/29/97 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/30/98 - - - NO -- ND -- NO ND NO ND ND -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/14/98 - - - ND -- ND -- NO ND NO ND ND -- -- -- -- - - -- NO - - - -- NO ND NO ND NO - NO ug/L 04/27/99 - - - ND -- ND -- NO ND NO ND ND -- -- -- -- - - -- NO - - - -- NO ND NO ND NO - NO ug/L 10/21/99 - - - ND -- ND -- NO ND NO ND ND -- - -- -- - - -- NO - - - -- NO ND NO ND NO - NO ug/L 03/14/00 _ _ _ __ __ __ __ __ __ __ __ __ __ _ -- -- _ _ __ __ _ _ _ __ __ __ __ __ __ _ NO ug/L .1.00 - - - NO -- ND -- NO NO NO NO NO -- - -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/17/00 - - - NO -- ND -- NO NO NO NO NO -- - -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L .10/01 - - - NO -- ND -- NO NO NO NO NO - - -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L 10/11/01 - - - NO -- ND -- NO ND NO ND ND - - -- -- - - - NO - - - - NO ND NO ND NO - NO ug/L .1.02 - - - NO -- ND -- NO ND NO ND ND - - -- -- - - - NO - - - - NO ND NO ND NO - NO ug/L 10/O1/02 - - - NO -- ND -- NO ND NO ND ND - - -- -- - - -- NO - - - - NO ND NO ND NO - NO ug/L 04/09/03 - - - NO -- ND -- NO ND NO ND ND - - -- -- - - -- 3.67 - - - - 1.01 ND NO ND NO - NO ug/L 10/13/03 - - - NO -- ND -- -- -- NO NO NO NO NO -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L 04/26/04 - - - NO -- ND -- -- -- NO NO NO 0.5 NO -- -- - - -- 2.5 - - - - NO NO NO NO NO - NO ug/L 10/25/04 - - - NO -- ND -- -- -- NO NO NO NO - -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L .04/05 - - - NO -- ND -- -- -- NO NO NO NO NO -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L 10/04/05 - - - NO ND ND -- NO NO 1.6 NO NO NO NO -- -- - - - NO - - - - NO NO NO NO NO - NO ug/L 04/28/06 - - - NO -- ND -- -- -- ND NO NO ND NO -- -- - - ND NO - ND NO NO NO NO NO NO NO - NO ug/L 10/09/06 - - - NO -- ND -- -- -- ND NO NO ND NO -- -- - - ND NO - NO NO NO NO NO NO NO NO - NO ug/L .24/07 - - - NO -- NO -- -- - ND NO NO NO NO -- -- - - ND NO - NO NO NO NO NO NO NO NO - NO ug/L 10/30/07 - - 0.2 0.17 J -- NO -- -- - NO NO 0.12 J 0.43 NO -- -- - - 0.24 0.25 - 0.21 0.16 J NO NO NO 0.17 J NO NO - NO ug/L 04/23/08 - - 0.2 NO -- NO -- -- - NO NO NO NO NO -- -- - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/06/08 - - 0.2 NO -- NO -- -- -- NO NO NO NO NO -- -- - - NO NO - NO NO 0.21 NO NO NO NO NO - NO ug/L 04/13/09 - - 0.2 NO -- NO -- -- -- NO NO NO NO NO -- -- - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/15/09 - - 0.2 NO -- NO -- -- -- NO NO NO NO 0.0582 J -- -- - - NO NO - 0.0952 J NO NO NO NO NO NO NO - NO ug/L 04/26/10 - - 0.2 NO -- NO -- -- -- NO NO ND NO NO -- -- - - NO NO - NO ND NO NO NO NO NO NO - NO ug/L 10/19/10 - - 0.2 NO -- NO -- -- -- NO NO ND NO NO -- -- - - NO NO - NO ND ND NO NO NO NO NO - NO ug/L 04/18/11 - - 0.2 NO -- NO -- -- -- NO NO ND NO NO -- -- - - NO NO - NO ND NO NO NO NO NO ND - NO ug/L 10/10/11 - - 0.2 NO -- NO -- -- -- NO NO ND NO NO -- -- - - NO NO - 0.478 ND NO NO NO NO NO Dry - NO ug/L 04/17/12 - - 0.2 NO -- NO -- -- -- NO NO NO NO NO -- -- - - NO NO - 0.175 J NO NO NO NO NO NO Dry - NO ug/L 10/09/12 - - 0.2 NO -- NO -- -- -- NO NO NO NO NO -- -- - - NO NO - NO NO NO NO NO NO NO Dry - NO ug/L 04/15/13 - - 0.2 NO -- NO -- -- -- NO NO NO NO NO -- -- - - NO NO - NO NO NO NO NO NO NO Dry - NO ug/L 09/30/13 - - 0.2 NO -- NO -- -- -- NO NO NO NO NO -- -- - - NO NO - NO NO NO NO NO NO NO Dry - NO ug/L 04/16/14 - - 0.2 NO -- NO -- -- -- NO NO ND NO NO -- -- - - NO NO - NO ND NO NO NO NO NO Dry - NO ug/L 10/15/14 0.17 - 0.2 Dry -- NO -- -- -- NO NO ND NO NO -- -- - - NO NO - NO ND NO NO NO NO NO Dry - NO ug/L 04/15/15 0.17 - 0.2 NO -- NO -- -- -- NO NO ND NO NO -- -- - - 0.0261 J 0.0688 J - NO ND NO 0.0796 J NO NO NO Dry - NO ug/L 10/07/15 0.17 - 0.2 NO -- NO -- -- -- NO NO ND NO NO -- -- - - NO ND - NO ND NO 0.197 J NO NO NO 0.201 - NO ug/L 04/11/i6 0.17 - 0.2 NO -- NO -- -- -- NO NO NO NO NO -- -- - - NO NO - NO NO NO NO 0.274 NO NO 0.219 - NO ug/L 11/30/16 0.17 - 0.2 ND -- ND -- -- -- ND ND ND ND ND -- -- - - ND ND - NO NO NO NO NO NO NO NO - NO ug/L 04/11/17 0.17 - 0.2 NO -- NO -- -- -- NO NO NO NO NO -- -- - - NO NO -- NO NO NO NO NO NO NO NO - NO ug/L 12/12/17 0.10 - 0.2 NO -- NO -- - -- NO NO 0.0990 J NO NO -- -- - - NO NO -- 0.103 J NO NO NO NO NO 0.118 J 0.111 J - NO ug/L O6/20/18 0.15 - 0.2 NO -- -- NO - -- NO NO ND NO NO -- -- - - NO -- NO NO ND NO NO NO NO NO -- NO - ug/L 11/27/18 0 0.2 - 0.281 -- -- NO - -- NO NO ND NO NO -- -- - - NO -- NO NO ND NO NO 0.338 NO 0,187 J -- NO NO ug/L 04/02/19 0..15 15 0.2 - NO -- -- NO - -- NO NO ND NO NO -- -- - - NO -- NO NO ND NO NO ND NO NO -- NO NO ug/L 11/19/19 0.15 0.2 - NO -- -- NO - -- NO NO ND - - NO ND - - NO -- NO NO ND NO NO NO NO NO -- NO NO ug/L 04/07/20 0.15 0.2 - NO -- -- NO - -- NO NO NO - - NO NO NO - NO -- NO - - - NO NO NO NO - NO - ug/L 10/13/20 0.15 0.2 NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO Nickel Total ug/L O6120/18 2.2 - 50 4.03 B -- -- 3.14 B - - 2.30 B 2.61 B NO 3.18 B 8.76 B - - - - 2.30 B -- NO - - - NO NO -- - - - - NC 2L = 100 ug/L ug/L 1 1/27/1 8 2.2 10 - NO -- -- NO - - NO NO NO NO 6.48 J - - - - NO -- NO - - - -- - -- - - - - ug/L 04/02/19 2.2 10 - NO -- -- NO - - NO NO NO NO 5.47 J - - - - NO -- NO - - - -- - -- - - - - ug/L 11/19/19 2.2 10 - NO -- -- NO - - NO NO NO - - ND ND - - NO - ND - - - -- - -- - - - - ug/L 04/07/20 2.2 10 - NO -- -- NO - - NO NO NO - - ND ND ND - NO -- ND - - -- -- - -- - - - - ug/L 10/13/20 2.2 10 - NO -- -- NO - - - - ND NO NO - - ND ND ND NO NO -- ND - - -- -- - -- - - - - Selenium ug/L 04/28/06 - - -- NO -- NO -- - - NO NO NO ND NO - - - - NO NO - NO ND ND NO NO NO NO ND - NO NC 2L = 20 ug/L ug/L 10/09/06 - - -- NO -- NO -- - - NO NO NO NO NO - - - - NO NO - NO NO NO NO NO NO NO NO - NO EPA MCL = 50 ug/L ug/L 04/24/07 - - -- NO -- NO -- - -- NO NO NO NO NO - - - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/30/07 - - 10 NO -- NO -- - -- NO NO NO NO NO - - - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 04/23/08 - - 10 NO -- NO -- - -- NO NO NO NO NO -- - - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/06/08 - - 10 NO -- NO -- - -- NO NO NO NO NO -- - - - NO NO - NO ND ND ND NO NO NO ND - NO ug/L 04/13/09 - - 10 NO -- NO -- -- -- 17.0 B 5.2 B 6.4 B ND NO -- - - - NO NO - ND ND ND 4.7 B 13.9 B NO 14.6 B 15.2 B - NO ug/L 10/15/09 - - 10 NO -- NO -- -- -- NO NO NO ND NO -- - - - NO NO - ND ND ND ND NO 1.02 B 2.47 B NO - NO ug/L 04/26/10 - - 10 NO -- NO -- -- -- NO NO 1.35 J ND NO -- - - - NO 2.46 J - ND ND ND 1.17 J 1.18 J NO NO 3.22 J - NO ug/L 10/19/10 - - 10 NO -- NO -- -- -- NO NO NO 1.84 J NO -- - - - NO 1.72 J - ND 2.48 J 1.09 J 0.919 J 2.88 J 1.30 J 4.50 J 1.49 J - NO ug/L 04/18/11 - - 10 NO -- NO -- -- -- NO NO NO NO NO -- - - - 4.90 J NO - ND NO NO NO NO NO NO NO - NO ug/L 10/10/11 - - 10 NO -- NO -- -- -- NO NO NO NO NO -- -- - - NO NO - ND NO 2.71 J NO NO NO NO Dry - NO -- NO -- NO 4.47 (ND) J 5.54 (ND) J NO NO -- -- - - 2.86 (ND) J NO - ND NO NO 4.55 (ND) J NO NO NO Dry - NO ug/L 10/09/12 - - 10 NO -- ND -- -- -- NO ND NO NO NO -- -- - - NO NO - ND ND ND NO NO NO 12.4 Dry - NO ug/L 04/15/13 - - 10 NO -- ND -- -- -- NO ND ND NO NO -- -- - - NO NO - ND ND ND NO NO NO NO Dry - NO ug/L 09/30/13 - - 10 NO -- ND -- -- -- NO ND ND NO ND -- -- - - NO NO - ND ND ND NO ND NO NO Dry - NO ug/L 04/16/14 - - 10 NO -- ND -- -- -- NO ND ND NO ND -- -- - - NO NO - ND ND ND NO ND NO NO Dry - NO ug/L 10/15/14 5.0 - 10 Dry -- ND -- -- -- NO NO NO NO NO -- -- - - NO NO - ND NO NO NO NO NO NO Dry - NO ug/L 04/15/15 5.0 - 10 NO -- ND -- -- -- NO NO NO NO NO -- - - - NO NO - ND NO NO NO NO NO NO Dry - NO ug/L 10/07/15 5.0 - 10 NO -- ND -- -- -- NO NO NO NO NO -- - - - NO NO - ND NO NO NO NO NO NO NO - NO ug/L 04/11/i6 5.0 - 10 NO -- ND -- - -- NO NO NO NO NO -- - - - NO NO - ND NO NO NO NO NO NO NO - NO ug/L 11/30/16 6.2 - 10 NO -- ND -- - -- NO NO NO NO NO -- - - - NO NO - ND NO NO NO NO NO NO NO - NO ug/L 04/11/17 6.2 - 10 NO -- ND -- - -- NO ND ND NO ND -- -- - - NO NO -- ND ND ND NO ND NO ND ND - NO ug/L 12/12/17 6.2 - 10 ND -- ND -- - -- NO ND ND NO ND -- -- - - NO NO -- ND ND ND NO ND NO ND NO - NO ug/L O6/20/18 6.2 - 10 ND -- -- NO - -- NO ND ND NO ND -- -- - - NO -- NO NO ND ND NO ND NO ND -- NO - ug/L 11/27/18 6.2 10 - NO -- -- NO - -- NO NO ND NO ND -- -- - - NO -- NO ND ND ND NO NO NO NO -- NO NO ug/L 04/02/19 6.2 10 - NO -- -- NO - -- NO NO NO NO NO -- - - - NO -- NO NO NO NO NO NO NO NO -- NO NO u9/L 11/19/19 6.2 10 - NO -- -- NO - -- NO NO NO -- -- NO NO - - NO -- NO NO NO NO NO NO NO NO -- NO NO ug/L 04/07/20 6.2 10 - NO -- -- NO - -- NO NO NO -- -- NO NO NO - NO -- NO - - -- NO NO NO NO -- NO - ug/L 1W13/20 6.2 10 - ND -- -- NO - -- -- -- NO ND NO -- -- NO NO ND NO NO -- NO NO NO NO NO NO NO NO -- NO - spa..ms,.eo�,E��,a �ozw�r-zo.w.0 MPon­.-LI.-M.-­ ----12ozo-2oznw-moo -F..- 1-o.a,.a.. aay5a17 TABLE 5 Summary of Historical Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SBME Project No. 4358-20-043A Detected Monitoring Constituent/ rameter Silver Unit. ug/L Date 04/28/O6 JWNk;cl,.rno..d -- -- -- ND -- • ND •- - -- r -- NO • Active C&D Monitoring - Wells r- .• I • Active Perfo&rnnarc for C D Monitoring Cl ad MSW Wells & MNA Landfill - Closed MSW Monitoring Wells & MNA Performance Monitoring Wells Offsite NC 21 =20 ug/L ug/L 10/09/06 - - -- ND -- ND -- -- -- NO NO ND ND NO -- - - - NO ND - NO NO ND NO ND NO ND NO - NO EPA MCL = 100 ug/L" ug/L 04/24/07 - - -- ND -- NO -- -- -- NO NO ND NO NO -- - - - NO ND - NO ND ND NO NO NO NO NO - NO ug/L 10/30/07 - - 10 ND -- ND -- -- -- NO NO NO NO NO -- - - - NO ND - NO ND ND NO NO NO NO NO - NO ug/L 04/23/08 - - 10 2.8 B -- ND -- - - NO NO NO NO NO -- - - - NO NO - NO ND ND NO NO NO NO NO - NO ug/L 10/06/08 - - 10 NO -- ND -- - - NO NO NO NO NO -- -- - - NO NO - ND NO NO NO NO NO 4.6 B NO - NO ug/L 04/13/09 - - 10 NO -- ND -- - - NO NO NO NO NO -- -- - - NO NO - ND NO NO NO NO NO NO NO - NO ug/L 10/15/09 - - 10 NO -- ND -- - - NO NO NO NO NO -- -- - - NO NO - ND NO NO NO NO NO 3.03 J NO - NO ug/L 04/26/10 - - 10 NO -- ND -- - - 3.57 J NO 5.35 J NO NO -- -- - - NO 6.48 J - ND NO NO 3.86 J 5.70 J 5.29 J 5.55 J 2.17 J - NO ug/L 10/19/10 - - 10 NO -- ND -- -- -- NO NO NO NO NO -- -- - - NO NO - ND NO NO NO NO NO NO NO - NO ug/L 04/18/11 - - 10 NO -- ND -- - - ND NO 5.35 J NO NO -- -- - - NO 4.46 J - ND ND ND 5.13 J NO NO 5.64 J 1.95 J - NO ug/L 10/10/11 - - 10 ND -- ND -- -- -- NO ND NO NO ND -- -- - - NO 8.74 J - ND ND ND NO 9.37 J NO NO Dry - NO ug/L 04/17/12 - - 10 ND -- ND -- -- -- NO ND NO NO ND -- -- - - NO NO - ND ND ND NO NO NO NO Dry - NO ug/L 10/09/12 - - 10 ND -- ND -- -- -- NO ND NO NO ND -- -- - - NO NO - ND ND ND NO 2.66 J ND 2.43 J Dry - NO ug/L 04/15/13 - - 10 NO -- ND -- -- -- NO NO 2.19 J NO NO -- - - - NO NO - ND NO NO NO NO NO NO Dry - NO ug/L 09/30/13 - - 10 NO -- ND -- -- -- 2.99 J NO 4.10 J NO NO -- - - - NO 4.63 J - ND NO NO 4.63 J 5.55 J 4.09 J 2.61 J Dry - NO ug/L 04/16/14 - - 10 NO -- ND -- -- -- NO NO NO NO NO -- - - - NO NO - ND NO NO NO NO NO NO Dry - NO ug/L 10/15/14 1.9 - 10 Dry -- ND -- -- -- NO NO NO NO NO -- - - - NO NO - ND NO NO NO NO NO NO Dry - NO ug/L 04/15/15 1.9 - 10 NO -- ND -- -- -- NO ND NO NO ND -- - - - NO NO - ND ND ND NO NO ND NO Dry - NO ug/L 10/07/15 1.9 - 10 NO -- ND -- -- -- NO ND NO NO ND -- - - - NO NO - ND ND ND NO ND ND NO ND - NO ug/L 04/11/16 1.9 - 10 ND -- ND -- -- -- NO ND NO NO ND -- - - - NO NO - ND ND ND NO NO ND NO ND - NO ug/L 11/30/16 1.9 - 10 NO -- ND -- - - NO ND ND NO ND -- - - - NO NO -- ND ND ND NO NO ND NO ND - NO u9/L 04/11/17 1.9 - 10 NO -- ND -- - -- NO NO NO NO NO -- - - - NO NO -- ND NO NO NO 1.92 J NO NO NO - NO u9/L 12/12/17 1.9 - 10 NO -- NO -- - -- 2.75 B NO NO NO NO -- - - - NO 1.90 B -- ND NO NO NO NO 2.43 B NO NO - NO ug/L O6/20/18 1.9 - 10 NO -- -- NO - -- NO NO NO NO NO -- - - - NO -- NO ND NO NO NO NO NO NO - NO - ug/L 11/27/18 1.9 10 - NO -- -- NO - - NO NO NO NO NO - - - - NO -- NO NO NO NO NO NO NO NO -- NO NO ug/L 04/02/19 1.9 10 - NO -- -- NO - - ND NO ND NO NO - - - - NO -- NO NO ND ND NO NO NO NO -- NO NO ug/L 11/19/19 1.9 10 - NO -- -- NO - - ND NO ND - - ND NO - - NO -- NO NO ND ND NO NO ND NO -- NO NO ug/L 04/07/20 1.9 10 - NO -- -- NO - - NO NO NO - - ND NO NO - NO - NO - - -- NO NO ND NO - NO - ug/L 10/13/20 1.9 10 NO NO ND NO NO ND NO NO NO NO NO NO NO ND NO NO ND NO NO Vanadium Total ug/L O10/18 1.4 - 25 NO -- -- 2.86 J - - 1.81 J NO 3.60 J NO NO - - - - NO - 3.39 J - -- -- 4.40 J 3.09 J - -- - - - NC 2L IMAC = 0.3 ug/L ug/L 11/27/18 1.4 10 - NO -- -- 1.65 J - - 2.86 J NO 1.95 J NO 1.42 J - - - - NO - 2.90 J - -- -- -- -- - -- - - - ug/L 04/02/19 1.4 10 - NO -- -- 1.65 J - - NO NO 1.65 J NO NO - - - - NO - 2.46 J - - -- -- -- - -- - - - ug/L 11/19/19 1.4 10 - NO -- -- NO - - NO NO NO - - NO NO - - 1.92 J - NO - - -- -- - - -- - - - ug/L 04/07/20 1.4 10 - NO -- -- NO - - NO NO 1.55 J - - NO 2.02 J NO - NO - NO - - -- -- - - - - - - ug/L 10/13/20 1.4 10 _ NO __ __ 1.70 J _ _ _ _ 2.15 NO 4.83 J _ _ ND NO 2.34 J NO ND _ 2.32 J _ Zinc ug/L 03/05/90 -- -- -- 34 - - -- -- -- -- -- -- -- -- -- -- - -- 26 -- - 43 79 11 -- -- -- -- -- - NO NC 21- = 1000 ug/L ug/L 03/21/91 - - - NO -- -- -- - - - - - - - -- -- - - ND - - 24 24 NO -- - - - - - NO EPA MCL = 5000 ug/L ug/L 03/10/92 - - - 30 -- -- -- -- -- - -- - - - -- -- - - 31 - - 40 31 21 -- - - - - - NO ug/L 04/20/95 - - - 35 68 -- -- -- -- - -- - - - -- -- - - - -- - - - - 47 60 49 51 - - NO ug/L O6/27/95 _ _ _ _ __ __ __ __ __ __ __ __ _ _ -- -- _ _ _ __ _ _ _ __ __ _ _ _ _ _ NO ug/L 09/22/95 - - - NO -- -- -- -- -- -- -- -- - - -- -- - - - -- - NO -- -- NO NO NO NO - - NO ug/L 03/28/96 - - - NO -- -- -- -- -- -- -- -- - - -- -- - - - -- - NO NO -- NO NO NO NO - - NO ug/L 10/29/96 - - - NO -- NO -- NO ND NO ND ND -- - -- -- - - -- ND - - -- -- NO NO NO NO NO - NO ug/L 04/08/97 - - - NO -- ND -- NO ND NO ND ND -- - -- -- - - -- ND - - -- -- NO NO NO NO NO - NO ug/L 10/29/97 - - - NO -- ND -- NO ND NO ND ND -- - -- -- - - -- ND - - - -- NO NO NO NO NO - NO ug/L .30/98 - - - NO -- ND -- NO ND NO ND ND -- -- -- -- - - -- ND - - - -- NO NO NO NO NO - NO ug/L 10/14/98 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/27/99 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/21/99 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 03/14/00 _ _ _ _ __ __ __ __ __ __ __ __ __ __ __ __ _ _ __ __ _ _ _ __ __ __ __ __ __ _ NO ug/L 04/19/00 - - - ND -- ND -- NO NO NO NO ND -- -- -- -- - - -- ND - - -- -- NO NO NO NO NO - NO ug/L 10/17/00 - - - NO -- ND -- NO NO NO NO ND -- -- -- -- - - -- NO - - -- -- NO NO NO NO NO - NO ug/L 04/10/01 - - - NO -- ND -- NO NO NO NO ND -- -- -- -- - - -- NO - - -- -- NO NO NO NO NO - NO ug/L 10/11/01 - - - NO -- ND -- NO NO NO NO ND -- -- -- -- - - -- NO - - -- -- NO NO NO NO ND - NO ug/L 04/18/02 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - -- NO - - -- -- NO NO NO NO NO - NO ug/L 10/08/02 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/09/03 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/13/03 - - - NO -- ND -- -- - NO NO NO NO NO -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/26/04 - - - NO -- ND -- - -- NO NO NO NO NO -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/25/04 - - - NO -- ND -- - -- NO NO NO NO -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/04/OS - - - NO -- ND -- - -- NO NO NO NO NO -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/04/05 - - - NO NO ND -- NO NO NO NO NO NO ND -- -- - - -- NO - - - - ND NO NO NO ND - NO ug/L 04/28/O6 u9/L 10/09/0 ug/L 04/24/07 - - - - -- -- -- - -- - - - ug/L 10/30/07 ug/L 04/23/08 - - - - -- -- -- - -- - - - ug/L O6/20/18 4.4 - 10 NO -- -- NO -- -- NO ND NO NO NO -- -- - - ND -- NO - - - ND NO -- -- - - - ug/L 11/27/18 4.4 10 - ND -- -- NO -- -- NO ND NO NO NO -- -- - - ND -- NO - - - - -- -- -- - - - ug/L 04/02/19 4.4 10 - NO -- -- NO - -- NO ND NO NO 6.14 J -- -- - - ND -- NO - - - - -- -- -- - - - ug/L 11/19/19 4.4 10 - NO -- -- NO - -- NO ND 5.24 J -- - ND ND - - 22.6 -- NO - - - - -- -- -- - - - ug/L 04/07/20 4.4 10 - NO -- -- 27.7 - -- NO NO NO -- - NO NO NO - NO - NO - - - - -- -- -- - - - ug/L 10/13/20 4.4 10 - NO -- -- NO - - -- - 455 NO 4.83 J -- - NO NO NO NO NO - NO - - - - -- -- -- - - - Iron ug/L 03/05/90 -- -- - 1469 -- -- -- - - -- - -- -- -- - - - - 419 - -- 239 1110 394 - -- -- -- - - NO NC 21 300 ug/L ug/L 03/21 /91 - - - 7800 -- -- -- - - -- - -- -- -- - - - - 700 - - 2510 17000 6500 - -- -- -- - - NO EPA MCL = 300 ug/L ug/L 03/10/92 - - - 213 -- -- -- - - -- - -- -- -- - - - - 463 - - 90 3"0 323 - -- -- -- - - NO ug/L 04/20/95 - - - 186 6000 -- -- - - -- - - -- -- - - - - - - - - - - 1340 9600 51200 71500 -- - NO ug/L O6/27/95 _ _ _ _ __ __ __ _ _ __ _ __ __ __ _ _ _ _ _ _ _ _ _ _ __ __ __ __ __ __ _ NO ug/L 09/22/95 - - - NO -- -- -- -- - -- - -- -- -- - - - - - - - NO - - NO NO NO NO -- - NO ug/L 03/28/96 - - - NO -- -- -- -- - -- - -- -- -- - - - - - - - NO NO - NO NO NO NO -- - NO ug/L 10/29/96 - - - NO -- ND -- NO NO NO NO NO -- -- - - - - - NO - - - - NO NO NO NO NO - NO ug/L 04/OS/97 - - - NO -- ND -- NO NO NO NO NO -- -- - - - - - NO - - - - NO NO NO NO NO - NO ug/L 10/29/97 - - - NO -- ND -- NO NO NO NO NO -- -- - - - - -- NO - - - - NO NO NO NO NO - NO ug/L 04/30/98 - - - NO -- ND -- NO ND NO ND NO -- -- - - - - -- NO - - - - NO NO NO NO NO - NO ug/L 10/14/98 - - - NO -- ND -- NO NO NO NO ND -- -- - - - - -- NO - - - - NO ND NO ND NO - NO ug/L 04/27/99 - - - ND -- ND -- NO ND NO ND ND -- -- - - - - -- NO - - - - NO ND NO ND NO - NO ug/L 10/21/99 - - - ND -- ND -- NO ND NO ND ND -- -- - - - - -- NO - - - -- NO ND NO ND NO - NO ug/L 03/14/00 _ _ _ __ __ __ __ __ __ __ __ __ __ __ __ _ _ _ __ __ _ _ _ __ __ __ __ __ __ _ NO u9/L 04/19/00 - - - NO -- ND -- NO NO NO NO NO -- -- -- - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/17/00 - - - NO -- ND -- NO NO NO NO NO -- -- -- - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/10/01 - - - NO -- ND -- NO NO NO NO NO -- -- -- - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/11/01 - - - NO -- ND -- NO NO NO NO NO -- -- -- - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/18/02 - - - NO -- ND -- NO NO NO NO ND -- -- -- - - - -- ND - - - -- NO NO NO NO NO - NO ug/L 10/08/02 - - - NO -- ND -- NO NO NO NO ND -- -- -- - - - -- ND - - - -- NO NO NO NO NO - NO ug/L 04/09/03 - - - NO -- ND -- NO NO NO NO ND -- -- -- - - - -- ND - - - -- NO NO NO NO NO - NO ug/L 10/13/03 - - - NO -- ND -- - - -- NO NO ND NO NO -- -- - - -- ND - - - -- NO NO NO NO NO - NO u9/L 04/26/04 - - - NO -- ND -- - - -- NO NO NO NO NO -- - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/25/04 - - - NO -- ND -- - - -- NO NO NO NO -- -- - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/04/05 - - - NO -- ND -- - - -- NO NO NO NO NO -- - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/04/05 - - - NO NO ND -- NO NO NO NO NO NO NO -- - - - - NO - - - -- NO NO NO NO NO - NO ug/L 04/28/06 ug/L 10/09/06 ug/L 04/24/07 ug/L 10/30/07 _ _ _ _ ug/L 04/23/08 ug/L O6/20/18 22 - 300 72.9 J -- -- 83,700 - - 61,400 10,300 135,000 5,220 20,200 - - - - 1,790 - 144,000 - - ug/L 11/27/18 22 50 - NO -- -- 88,300 - - 62,600 21,400 142,000 10,300 23,100 - - - - 417 - 141,000 - - -- -- -- -- -- - - - ug/L 04/02/19 22 50 - NO -- -- 82,700 - - 65,600 28,800 134,000 3,890 23,200 - - - - "0 - 129,000 - - -- -- -- -- -- - - - ug/L 11/19/19 22 50 - NO -- -- 75,"0 - - 99,700 6,040 152,001 -- -- 38,400 181 - - 15,500 - 101,000 - - -- -- -- -- -- - - - ug/L 04/07/20 22 50 - NO -- -- 52,300 - - 63,200 18,100 141,000 -- -- 2,670 448 111,000 - 2,510 - 101,000 - - -- -- -- -- -- - - - ug/L 10/13/20 22 50 - nD -- -- 83,800 -- - -- -- 66,200 7,600 139,000 -- -- 14,400 2,500 103:000 ND 397 - 119,000 - - -- -- -- -- -- - - - z�snaremsMeq+,Ervvw,a•ns�zoswasaso-wu Mwrecwmv xomreircawo ram�m.��e,.asxo,. se�uaws�.,euare Frsoso-sosnwwx��aoa�u�wm rarEwmzoso-,owema.w.. co.nw+•b.�s. P Je6m17 TABLE 5 Summary of Historical Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SBME Project No. 4358-20-043A Detected Monitoring Constituent/Parameter Manganese "' Unit. ug/L a, q. 03/05/90 St. INEkic1grourid -- - -- '.rin we] , __ NO -- -- - -- -- -- Active C&D Monitoring -- Wells -- -- -- -- I - - -- Active C&D Performanc: for the CIO ND Monitoring Wells Monitoring ad MSW Landfill -- & NINA Wells - 31 NO Closed MSW ND Monitoring -- Wells & NINA -- Performance -- Monitoring Wells -- - -- Offsite Pr ivate Well ND NC 2L = 50 ug/L ug/L 03/21/91 - - - 20 -- - - -- -- -- -- - - - - - - - 14 -- - 50 50 13 -- - - - - - NO EPA MCL = 50 ug/L ug/L 03/10/92 - - - ND -- - - -- -- -- -- - - - - - - - NO -- - 47 32 ND -- - - - - - NO ug/L 04/20/95 - - - ND 127 - - -- -- -- -- - - - - - - - - -- - - - -- 23 23 1020 173 - - NO ug/L O6/27/95 _ _ _ _ __ __ __ __ __ __ __ __ _ _ _ _ _ _ _ __ _ _ __ __ NO ug/L 09/22/95 - - - NO -- -- -- -- -- -- -- -- -- -- -- - - - - -- - NO -- -- NO NO NO NO - - NO ug/L 03/28/96 - - - NO -- -- -- -- -- -- -- -- -- -- -- - - - - -- - NO NO -- NO NO NO NO - - NO ug/L 10/29/96 - - - NO -- ND -- NO NO NO NO NO -- -- - - - - -- NO - - -- -- NO NO NO NO NO - NO ug/L 04/08/97 - - - NO -- ND -- NO NO NO NO NO -- -- - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/29/97 - - - NO -- ND -- NO NO NO NO NO -- -- - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/30/98 - - - NO -- ND -- NO ND NO ND ND -- -- - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/14/98 - - - ND -- ND -- NO ND NO ND ND -- -- - - - - -- NO - - - -- NO ND NO ND NO - NO ug/L 04/27/99 - - - ND -- ND -- NO ND NO ND ND -- -- - - - - -- NO - - - -- NO ND NO ND NO - NO ug/L 10/21/99 - - - ND -- ND -- NO ND NO ND ND -- - - - - - -- NO - - - -- NO ND NO ND NO - NO ug/L 03/14/00 _ _ _ __ __ __ __ __ __ __ __ __ __ _ _ _ _ _ __ __ _ _ _ __ __ __ __ __ __ _ NO ug/L .1.00 - - - NO -- ND -- NO NO NO NO NO -- - - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/17/00 - - - NO -- ND -- NO NO NO NO NO - - - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L .10/01 - - - NO -- ND -- NO NO NO NO NO - - - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/11/01 - - - NO -- ND -- NO ND NO ND ND - - - - - - -- NO - - - -- NO ND NO ND NO - NO ug/L .1.02 - - - NO -- ND -- NO ND NO ND ND -- - - - - - -- NO - - - -- NO ND NO ND NO - NO ug/L 10/O1/02 - - - NO -- ND -- NO ND NO ND ND -- - - - - - -- NO - - - -- NO ND NO ND NO - NO ug/L 04/09/03 - - - NO -- ND -- NO ND NO ND ND -- - - - - - -- NO - - - -- NO ND NO ND NO - NO ug/L 10/13/03 - - - NO -- ND -- -- -- NO NO NO NO NO - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/26/04 - - - NO -- ND -- -- -- NO NO NO NO NO - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/25/04 - - - NO -- ND -- -- -- NO NO NO NO - - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/04/05 - - - NO -- NO -- -- -- NO NO NO NO NO - - - - -- NO - - - - NO NO NO NO NO - NO ug/L 10/04/05 - - - NO NO NO -- NO ND NO NO ND NO NO - - - - -- NO - - - - NO NO NO NO NO - NO ug/L 04/28/06 ug/L 10/09/06 ug/L 04/24/07 ug/L 10/30/07 ug/L 04/23/08 ug/L O6/20/18 1.5 - 50 NO -- -- 200 - - 117 18.9 J 186 58.6 131 - - - - 40.2 J -- 346 - - - -- - -- - - - - ug/L 11/27/18 1.5 10 - 1.73 J -- -- 203 -- - 147 56.2 185 43.8 125 - - - - 103 -- 384 - - - -- - - - - - - ug/L 04/02/19 1.5 10 - 3.52 J -- -- 190 -- - 186 42.8 174 68.3 146 - - - - 185 -- 443 - - - - - - - - - - ug/L 11/19/19 1.5 10 - 2.68 J -- -- 191 -- - 189 15.2 212 - - 114 2.71 J - - 131 -- 248 - - - - - - - - - - ug/L 04/07/20 1.5 10 - 1.59 J -- -- 166 -- - 128 39.4 229 - - 99.6 8.4 J 228 - 53 - 258 - - - - - - - - - - ug/L 10/13/20 1.5 10 _ 2.85 J __ __ 180 589 123 183 _ _ 164 47.8 227 NO 11.0 _ 294 Acetone ug/L 03/05/90 -- -- _ _ __ __ __ __ __ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ NO NC 2L = 6000 ug/L ug/L 03/21/91 - - - - -- -- -- -- -- - - - - - - - - - - - - - - - - - - - - - NO ug/L 03/10/92 _ _ _ _ __ __ __ __ __ __ __ _ _ _ _ _ _ _ _ __ _ _ _ _ _ _ _ _ __ _ NO ug/L 04/20/95 NO ug/L O6/27/95 - - - - NO -- -- -- -- -- -- -- -- -- - - - - - - - - - - -- NO NO NO -- - NO ug/L 09/22/95 - - - ND -- -- -- -- -- -- -- -- -- -- - - - - ND - - NO NO NO NO NO NO NO -- - NO ug/L 03/28/96 - - - ND -- -- -- -- -- -- -- -- -- -- - - - - NO - - ND ND NO NO NO NO NO -- - NO ug/L 10/29/96 - - - ND -- NO -- NO NO NO NO ND -- -- - - - - - NO - - - -- NO NO NO NO NO - NO ug/L 04/08/97 - - - ND -- NO -- NO NO NO NO ND -- -- -- - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/29/97 - - - NO -- NO -- NO NO NO NO NO -- -- -- - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/30/98 - - - NO -- NO -- NO NO NO NO NO -- -- -- - - - -- NO - - - -- NO NO ND NO NO - NO ug/L 10/14/98 - - - NO -- NO -- NO NO NO NO NO -- -- -- - - - -- NO - - - -- NO NO 3085 NO NO - NO ug/L 04/27/99 - - - NO -- NO -- NO NO NO NO NO -- -- -- - - - -- NO - - - - NO 541 NO NO NO - NO ug/L 10/21/99 - - - NO -- ND -- NO NO NO NO ND -- -- -- - - - -- ND - - - - 335 390 108 NO NO - NO ug/L 03/14/00 - - - NO -- ND -- NO NO NO NO ND -- -- -- - - - NO NO - ND ND NO ND NO NO NO NO - NO ug/L 04/19/00 - - - NO -- ND -- NO NO NO NO ND -- -- -- - - - -- ND - - - - NO NO 728 NO 139 - NO ug/L 10/17/00 - - - NO -- ND -- NO NO NO NO ND -- -- -- - - - -- ND - - - - NO NO NO NO NO - NO ug/L 04/10/01 - - - NO -- ND -- NO NO NO NO NO -- -- -- - - - -- NO - - - - 185 NO 2628 NO NO - NO ug/L 10/11/01 - - - NO -- ND -- NO NO NO NO NO -- -- -- - - - - NO - - - - NO NO NO NO NO - NO ug/L 04/18/02 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - - 167 - - -- -- 129 NO NO NO NO - NO ug/L 10/08/02 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - - NO - - -- -- 422 110 NO NO NO - NO ug/L 04/09/03 - - - NO -- ND -- NO NO NO NO NO -- -- -- -- - - -- NO - - -- -- NO 192 119 NO NO - NO ug/L 10/13/03 - - - ND -- ND -- NO ND NO ND ND NO ND -- -- - - -- ND - - -- -- 125 113 361 ND NO - NO ug/L 04/26/04 - - - ND -- ND -- NO ND NO ND ND NO ND -- -- - - -- ND - - - -- ND NO NO ND NO - NO ug/L 10/25/04 - - - ND -- ND -- NO ND NO ND ND NO ND -- -- - - -- ND - - - -- ND NO NO ND NO - NO ug/L 04/04/OS - - - NO -- ND -- NO ND NO NO ND NO NO -- -- - - -- ND - - - -- NO 1400 123 NO NO - NO u9/L 10/04/05 - - - NO NO ND -- NO NO NO NO NO NO NO -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/28/06 - - - NO -- ND -- -- -- NO NO NO NO NO -- -- - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/09/06 - - - NO -- ND -- -- -- NO NO NO NO NO -- -- - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 04/24/07 - - - NO -- ND -- -- -- NO NO NO NO NO - - - - NO NO - NO NO NO NO 138 NO NO NO - NO ug/L 10/30/07 - - 100 NO -- ND -- -- -- NO NO 4.8 J 4.3 J NO - - - - ND 17 - NO ND ND 380 60 16 7.7 5.6 - NO ug/L 04/23/08 - - 100 NO -- NO -- -- -- NO 37 J NO 5.5 J NO - - - - 5.7 J 15 J - ND ND ND 420 120 220 10 J NO - NO ug/L 10/06/08 - - 100 NO -- 4.9 B -- -- -- 5.3 B NO 7.6 B ND 5.1 B - - - - ND 280 - ND ND ND 1100 160 56 J 20 B 210 - NO ug/L 04/13/09 - - 100 NO -- NO -- -- -- NO NO NO NO NO - - - - ND 88 J - ND ND ND 48 J 240 160 NO 45 J - NO ug/L 10/15/09 - - 100 NO -- NO -- -- -- NO NO NO NO NO - - - - NO NO - ND NO NO ND 78 J ND NO NO - NO ug/L 04/26/10 - - 100 NO -- NO -- -- -- NO NO NO 2.3 J NO - - - - NO 6.2 J - ND NO NO 80 J 25 J 77 J 8.9 J 140 - NO ug/L 10/19/10 - - 100 NO -- NO -- -- -- NO NO NO NO NO - - - - NO 7.0 J - ND NO NO 180 170 NO NO 170 - NO ug/L 04/18/11 - - 100 NO -- ND -- - - ND NO NO 10 J NO -- -- - - NO NO - ND NO NO 29 J 36 J NO 36 J NO - NO ug/L 10/10/11 - - 100 NO -- ND -- - - 82 J NO ND 4.4 J NO -- -- - - NO NO - ND ND ND 15 J - NO 5.0 J Dry - NO ug/L 04/17/12 - - 100 NO -- ND -- - - ND NO ND 6.0 J NO -- -- - - NO 10 J - ND ND ND 10 J 56 J 12 J 18 J Dry - NO ug/L 10/09/12 - - 100 NO -- ND -- - - ND ND ND 5.1 J ND - - - - NO 16 J - ND ND ND NO 290 NO 13 J Dry - NO ug/L 04/15/13 - - 100 NO -- ND -- - - 26 J ND ND 10 J ND - - - - NO 6.3 J - ND ND ND 150 88 J 73 J 12 J Dry - NO ug/L 09/30/13 - - 100 NO -- ND -- - - 11 J NO NO 5.6 J NO - - - - NO 18 J - ND NO NO 94 J 24 J 9.8 J 5.5 J Dry - NO ug/L 04/16/14 - - 100 NO -- ND -- - - 8.4 J NO NO 27 J 5.2 J - - - - NO 37 J - ND NO NO 280 36 J 6.3 J 15 J Dry - NO ug/L 10/15/14 1.2 - 100 Dry -- ND -- - - NO NO NO 25 J 7.4 J - - - - NO 14 J - ND NO NO 16 J 110 6.6 J 12 J Dry - NO u9/L 04/15/15 1.2 - 100 NO -- ND -- - -- NO NO NO 10 J 13 J - - - - NO 32 J - ND NO NO 210 110 16 J 7.0 J Dry - NO ug/L 10/07/15 1.2 - 100 NO -- ND -- -- -- 13 J NO NO NO 9.4 J - - - - NO NO - ND NO NO 130 200 6.4 J 2.6 J 98 J - NO ug/L 04/11/16 1.2 - 100 NO -- ND -- -- -- NO ND ND 21 J NO - - - - NO 52 J - ND ND ND 290 110 ND 55 J 300 - NO ug/L 11/30/i6 10 - 100 ND -- ND -- -- -- ND ND ND 12 J 13 J - - - - ND ND - ND ND ND 46 J 10 J ND 19 J 980 - NO ug/L 04/11/17 10 - 100 ND -- NO -- -- -- NO ND ND ND NO - - - - NO NO - ND ND ND NO 20 J ND NO 880 - NO ug/L 12/12/17 10 - 100 NO -- NO -- -- -- NO NO ND NO NO - - - - NO NO -- ND ND ND NO NO ND 11 J 20 J - NO ug/L O6/20/18 10 - 100 NO -- -- NO -- -- NO NO NO NO 26 B - - - - NO -- NO NO NO NO 20 B 19 B 11 B 20 B - NO - ug/L 11/27/18 10 20 - NO -- -- NO -- -- NO NO NO NO NO - - - - NO -- NO NO NO NO 28 190 56 57 - NO NO ug/L 04/02/19 10 20 - NO -- -- NO -- -- NO NO NO NO NO - - - - NO -- NO NO NO NO 12 J 490 21 NO - NO NO ug/L 11/19/19 10 20 - NO -- -- NO -- -- NO NO NO -- - NO NO - - NO - NO NO NO NO NO 12 J NO NO - 190 NO ug/L 04/07/20 10 20 - NO -- -- NO -- -- NO NO ND -- - NO NO NO - NO - ND - - - 26 59 NO 17 J - NO - ug/L 10/13/20 10 20 - NO -- -- NO -- -- -- -- NO ND ND -- - NO NO NO NO NO - ND NO ND NO NO 490 D ND NO - NO - zssnareesMeoia�Euvw,o•carwozwase-zo-oau Mwncwmy aamreircawa ram�m.��a+T�so+ se �uawa�e.auaM rrzozo-zoz+�wwu�w.u.wm ra.Ewmzozo-+owams.eu.. cwnw.a�.ss. Page7d17 TABLE 5 Summary of Historical Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Detected Monitoring Active C&D Monito Wells Active Perfo&rnnarc C D Monitoring Wells & NINA Wells Closed MSW Monitoring Wells & NINA Performance Monitoring Wells Offsite Constituent/Parameter "In. Unit. u9 L a, Wlub/9u St. JEEIBac.kgroi-d, onit ring We] MIV MW-IID MW-11DR MW-12S MW-12D MW-1 3S MW-13D MW-13SR ring MW-13DR MW-IGS MW-16D MW-17S MW-17D Mw-18 MW-19 for MW-4 or a o:M nitoring th Cl ad MSW MW-11S Landfill MW-11SR Mw-1 MW-2 MW-3 MW-6 MW-7 MW-8 MW-9 MW-15 MW-15R Pr ivate Well PW-1 C 2L - I ug/L ug L 03/2 1 /91 D EPA MCL = 5 ug/L ug/L 03/10/92 NO ug/L 04/20/95 NO ug'L 06/27/95 NO NO 3.2 8.8 9.8 - NO ugIL 09/22/95 NO NO NO NO NO NO NO 6 6 NO ug/L 03 �28 96 NO NO NO 5 NO 5 6 - NO u g/L 9�9 102 6 NO ND NO NO NO NO NO NO NO NO NO 6 NO ug/L 0 /08/97 NO ND NO NO NO NO NO NO NO NO NO 6 .1 NO ug/L 10/29/97 NO ND NO NO NO NO NO NO 5 NO NO 6'5 11 NO ug/L 04/30/98 NO ND NO ND NO ND ND NO NO 6.6 NO 6.4 11 NO ug/L 10/14/98 ND ND NO ND NO ND ND NO NO NO NO NO 8.5 NO ug/L 04/27/99 ND ND NO ND NO ND 5.3 NO NO NO NO 6.2 10 NO ug/L 10/2 1/99 ND ND NO ND NO ND ND NO NO NO NO NO I NO ug'L 03/1 4/00 NO 4 NO 3 NO NO NO NO NO NO 3 NO 3 NO NO 4 1 NO ugIL .1.00 NO ND NO NO NO NO NO NO NO NO NO NO 7.6 NO ug'L 10/1 7/00 NO ND NO NO NO NO NO NO NO NO 5 52 92 NO ugIL .10/01 NO ND NO NO NO NO NO NO NO NO NO 5.1 9.6 NO ug'L 10/1 1/01 NO ND NO ND NO ND ND NO NO ND NO NO 8 NO ugIL .1.02 NO ND NO ND NO ND ND NO NO ND 5 NO ND NO ug'L 10/01/02 NO ND NO ND NO ND ND NO NO ND ND NO N NO ugIL 04/09/03 NO ND NO ND NO ND ND NO NO ND NO NO 6.8 NO ug/L 10/13/03 NO ND NO NO NO NO NO - - - - NO NO NO NO NO 89 NO ug/L 04/26/04 NO ND NO NO NO NO NO NO NO NO NO NO 8.4 NO ug'L 10/25/04 NO ND NO NO NO NO NO - - - - NO NO NO NO NO 6.8 NO ugIL .04/05 NO ND NO NO NO NO NO NO NO NO NO NO 79 NO ug'L 10/04/05 NO NO NO NO ND NO NO NO NO NO NO NO NO NO NO 6 5 NO ugIL .28/06 NO NO ND NO NO NO NO ND NO ND NO NO NO NO NO NO 6.6 NO ug'L 10/09/06 NO NO ND NO NO ND NO ND NO NO ND NO NO NO NO NO NO ugIL .24/07 NO NO NO NO NO ND NO ND NO NO NO NO NO NO 41 35 3.3 NO ug L 10/3 0 03//08 1 NO 0.80 J 0.33 J NO 22 069 J NO NO 2.0 NO 1.2 NO 3.0 1.5 2'7 3:2 4.2 NO u ' gIL 1 NO 1.1 NO 5.1 2:5 O�42 J NO NO 2:4 NO 0 J NO NO 2 0.84 J 4.0 ND NO ug/L 10/06/08 1 NO NO NO NO NO NO NO NO NO NO 0�9'7 NO NO 2:1 2.2 2.5 64 NO ug/L 04/13/09 1 NO 1:2 0.53 J 0.53 J 23 056 J NO NO 0.88 J NO NO NO 26 NO 31 3.:4 59 NO uglL 10/15/09 1 NO 2 1.2 NO 2:2 0�98 J NO 0.40 J 24 1.1 1:4 NO 3:4 1. 3 2:9 5 3.6 40 NO ug/L 04/26/10 1 NO ':'2 06 J NO 2.5 NO NO NO 2:6 NO 1.1 NO 2.2 2.4 31 3 52 NO ug/L 10/19/io I NO 1 5 0:89 J NO 2.3 057 J NO NO 2.6 NO 1. NO 3.1 NO 3' 3.6 46 NO u g/L 04/18/ 1 1 NO 1.1 0.89 J NO NO O�72 J NO NO 2.4 NO NO NO NO 0.80 J 3 NO 4'. 1 NO ug/L 10/1 0/11 1 NO 1:2 NO NO 2.2 NO NO NO 2.4 NO 1.0 NO 3.4 - 3:4 3.5 D NO ug,L 04/17/1 2 1 NO 3 07 J NO 23 066 J NO NO 2.4 081 J 1.0 NO 3.6 1.2 4.3 3.9 Dry NO ug/L 10/0 12 1 NO 0:799 J NO 2:0 O�4 J NO NO 2.0 0:69 J 1.2 NO 22 22 36 4.0 Dry NO ug/L 04/195//1 3 1 NO 3 0.63 J NO 2.1 0.59 J NO NO 2.5 NO 0 NO 2:4 1:1 3:6 4.2 Dry NO u 9 /L 09/30/�3 1 NO 1 041 J NO 2.1 9 0.59 J NO NO N D NO 05 NO 2.2 2.7 2.4 34 Dry NO g L U / 04/16/ 4 1 NO ':3 3 NO 0.41 J 2.0 N D 056 J NO 1. 7 NO 0 . 60 7 J NO 2 . 1 . 2. 33 Dry NO ug L / 10/ 5/14 1 0115 1 Dry 1:12 0 J NO 1.9 1.2 O�63 J NO 2.4 NO 0.8 J NO 2 J.: 3.: 3.4 Dry NO u g/L 04/15/ 5 0: 5 1 NO 1 0: 5, J 0 NO 12 1.0 NO NO 2 0 - NO 0.�� , NO 1.5 0.69 J 1 .9 2. Dry NO u /L 10/0 7/ 15 0115 1 NO 0 . 7 J NO 24 0. J 0. NO 2.3 NO 0.80 J NO 3.: 1.6 3 . 1 3.8 6 NO ug L 9 04/11/ 6 0: 5 1 NO 1 3 ND NO 2'2 147 .0 047 61 NO I a NO 0.54 J NO 2 0.64 J 3.5 3 :3 2 NO U g L 11/3 16 015 1 NO 0 J NO 2:0 0 J 0 NO 2:6 NO 0.45 J NO 2.:6 1.4 .9 2.9 2 .9 3.6 NO u g/L 04/11/ 7 0: 5 1 1 NO 1 056 91 J NO 2.2 043 72 J 064 82 NO 35 NO 1.2 NO 2 9 NO 3 41 3.4 NO u /L g 12/12/17 0.15 1 NO 1.2 0 84 J NO 1.4 0.55 J 0.67 NO 1:8 -- 0.87 J 0.60 J NO 2.4 1.1 2.7 33: '4 4.4 - NO / ug L 0 6/20/18 0.15 1 NO 1.2 NO NO 1 .6 ND 0.5 NO 2.4 NO 1.0 NO 2 .5 1 1 3.3 1.1 ug L 11/27/18 0 1, - NO 2.0 NO 0.43 J - 2.0 ND 0.410 NO 28 NO ND NO 3.3 0.'75 J 2.3 36 1.5 NO g/L u / 04/02/ 9 0 5 :11 NO 2.1 NO NO 1:6 ND 0.54 NO 2:7 NO 050 J NO 3.4 1.1 J 2.7 3:4 1.8 NO ug/L 11/19/1 9 0.15 1 - NO 1.6 1.1 NO - 2.3 NO NO ND 2.8 0.48 J O�97 J NO 3.7 1.6 2.9 3.8 5.7 NO (Ve "ication Event) ugL 01 /08/20 0.57 1 - - - - - - - - 1.5 ug/L 04/0 0 0.15 1 - NO 1.6 0.54 J NO - 1.7 NO NO NO 3.1 1.4 NO 2.5 3.6 15 (Ve "ication Event) u g/L 06/075//220 0:1 5 1 - - 1 2 - - ug/L 10/13/20 0.15 1 NO 1.9 NO NO 2.2 NO NO 0. 99 J NO NO 3.2 NO 0.54 J NO 2.5 NO 2.8 4.0 1.2 NO Chloroberoene u IL 03/05/90 -- NO NC 2L = 50 ug/L gL 03/21/91 NO EPA MCL = 100 ug/L ug/L 03/10/92 NO ug/L 04/20/95 NO ug/L 06/27/95 NO NO NO NO 6.5 NO ug/L Og �22 95 NO NO NO NO NO NO NO NO 6 NO ug/L 03 28�96 NO NO NO NO NO NO NO NO uglL 1 /29/96 NO NO NO NO NO NO - NO NO NO NO NO NO NO NO ug,L 04/08/97 NO NO NO NO NO NO NO NO NO NO NO NO NO NO ug'L 10/29/97 NO NO NO NO NO NO - ND NO NO NO NO 75 NO NO ug/L .30/98 NO ND NO NO NO NO ND ND NO NO NO 5�4 NO NO uglL 10/14/98 NO NO NO NO NO NO - NO NO NO NO NO 51 NO NO ug/L 04/27/99 NO ND NO NO NO NO ND ND NO NO NO 61 NO NO ug'L 1 0'2 1/99 NO NO NO NO NO NO NO NO NO NO NO 7.1 NO NO ugIL 03/14/00 NO NO NO NO NO NO NO NO NO NO 3 NO NO NO NO 6 NO NO u /L 04/19/00 NO 3 NO NO NO NO NO NO NO NO NO 55 NO NO ug/L 10/17/00 NO NO NO NO NO NO ND NO -- NO NO NO 12 NO NO ug/L 04/1 0/01 NO NO NO NO NO NO ND NO NO NO NO 7.3 NO NO ug/L 10/11/01 NO NO NO NO NO NO ND NO NO NO NO 13 NO NO ug/L 04/18/02 NO ND NO NO NO NO ND NO NO NO NO 10.5 NO NO ug,L 10/08/02 NO ND NO NO NO NO NO NO NO NO NO 86 NO NO ug/L 04/09/03 NO ND NO NO NO NO NO NO NO NO NO 8:6 NO NO ug/L 10/13/03 NO ND NO NO NO NO NO NO NO NO NO 10: NO NO ug/L 04/26/04 NO ND NO NO NO NO NO NO NO NO NO 1 0 NO NO ug,L 10/25/04 NO ND NO NO NO NO NO NO NO NO NO 11.9 NO NO ug'L D4/45 0 NO NO NO NO ND NO NO NO NO NO NO 9 NO NO ugIL 1.004//05 NO NO NO NO NO NO NO ND ND NO NO NO NO ND 91 ND NO ug/L 04/28/06 NO NO NO NO ND ND NO NO NO NO NO NO NO NO ND 7:8 ND NO ug/L 10/09/06 NO NO NO NO ND ND NO NO NO NO NO NO NO ND NO NO NO NO ug/L 04/24/07 NO NO NO NO NO NO NO NO NO NO 32 NO NO NO NO 91 NO NO ug/L 10/30/07 3 NO 0:6 8 J .51 J 0NO NO 30 0.58 J NO NO NO NO 4�O NO 0.93 J 09 J 2.4 J 92 0.48 J NO ug/L 04/23/08 3 NO 052 J NO 2:7 J NO NO NO 1.1 J NO 25 J NO NO 0Z J NO 9:9 NO NO ug,L 10/06/08 3 NO 0.47 J NO NO 21 J NO NO NO 0.85 J NO 26 J NO NO 0.93 J NO 90 NO NO ug/L 04/1 3/ 9 3 NO 0.54 J NO ND 2:9 J NO ND NO NO NO 3.4 NO 0.71 J NO 1.1 J ii ND NO ug/L 10/15/009 3 NO 056 J 0.95 J ND 32 0.75 J ND NO 1:0 J 8.4 38 NO 1.2 J 1.0 1 2:9 1 11 0.57 J NO u /L 04/2 6/10 3 ND 05 J 051 J ND 3:2 NO ND NO 12 NO 27 J NO 081 J 0. 61 10 1 ND NO ugg L 10/1 9/ 0 3 NO 0.637 J 0:59 J NO 30 0.51 J ND NO 0. 91 J NO 31 NO 0�99 J NO 1 10 ND NO ug/L 04/ 8/11 3 NO NO 1.0 J NO 3:2 NO NO NO 1 J NO 2:6 J NO NO 0.81 J 2:57 7.8 NO NO u g/L 101110/ 11 3 NO NO 096 J NO 39 NO NO NO 1:2 J 67 30 NO 1:6 J - 3.6 9.6 Dry NO u /L 04/17/112 3 NO 061 J 0:95 J NO 3:6 0.78 J NO NO 10 J 6:3 2:8 J NO 1.4 , .86 1 2:3 1 12 Dry NO ug g L 101091 2 3 NO 08 0.91 J NO 35 05 J NO NO 10 2 5.6 31 NO 1 3 J 1.4 , 25 , 11 Dry NO / u g L 04/1 13 3 NO 060 J 061 J NO 3:1 0:597 J ND NO 1. 2 NO 1 NO J 1:21 0.41 J . 1 1 J 1 0 Dry NO u g/L 09/350// 3 1 3 NO 0.702 J 0:47 J NO 2.5 J 0.5 0 J ND NO 0. 45 J NO 1:2, " NO I J 1.0 1 64 1 0: 92 D NO u /L 04/1 6/14 - 3 NO 0.72 J NO 0.52 J 3.3 NO NO NO 0.74 J NO 1. J NO 1.2 J 0. 75 , 074 9:1 Dry NO ug /L 10/15/ 4 0.17 3 Dry 5 0 9 J 051 J NO 2.6 J 0. 62 J ND NO 0. 86 J 1.6 J 1 2.8 J NO 0 1 .4 J 31 10 Dry Dry NO ug g L / 04/1 5/ 15 0:117 3 NO 0 .72 J 053 J 0.44 J 2.7 J 0 76 J NO NO 0 86 J NO 2.1 NO :' " 069 NO 1 1 1 0 Dry NO u g/L 10/07/ 5 0 7 3 NO 0 .76 J 048 J NO 26 J 0.51 J NO NO 1.2 J NO 2.3 J NO 1.2 J 1.8 J 36 9.9 0 64 J NO uglL 04/11/16 0.17 3 NO 0.71 J NO NO 2�6 J 0.65 J NO NO 0.88 J NO 1.2 J NO 0.74 J NO 21 J 10 NO NO ug,L 11/30/16 0.17 3 NO .72 0.73 J 0.64 J NO 23 1 044 J 041 J NO 1:2 1 NO 1.4 J NO 1:0 1.4 J 31 84 NO NO ug/L 04/11/�7 0:117 3 NO J 1�2 J NO 2�6 1 0:68 J om NO 1.4 NO 3.3 NO 14 NO 46 12 NO NO u g/L 12/12/ 7 0 7 3 NO 0.77 J 1 2 NO 12 J 0.71 J 0.5 2 NO 0. 93 J 7.1 2.1 J NO NO 1.4 1 4:0 10 0.62 J NO u /L 06/20/18 0:117 3 NO 0 2 J 0.54 J NO 2.� 9 J ND NO NO - 1:3 J NO 2.8 J NO 1 J 093 , 28 , 1 - 0.40 J - / ugg L 1 1/27/ 8 0 7 1 - NO 9 0Z J NO 0.43 J 35 ND NO NO 1 0 NO 0.90 J NO I �'6 0:46 J 0.91 J 70 NO NO U 04/02/19 0.117 1 NO 1. 2 NO NO 3.4 ND 0. 54 J NO 1.0 NO 1.3 NO 1�4 NO 12 S:4 3 044 J NO ug'L g/L 11/19/ 9 0 7 1 NO 0 90 J 2.1 NO 51 NO NO NO 1.3 3.7 2.6 NO 1.9 4.1 6:1 11 0�91 J NO u:,ILL 14 7200 " / 0.17 1 NO NO NO NO 5.3 NO NO 1.2 NO 1 - - 1.2 NO 19 96 NO u 10113/2 0:1 1 NO NO NO NO 5.8 NO NO 0.88 J NO NO 1 : NO 1.2 NO 1.6 NO 43 8:9 NO -­.- LI.- ..-­ - ---­ 12-2--­- - -1-o.- Page 8 of 17 TABLE 5 Summary of Historical Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SBME Project No. 4358-20-043A Detected Monitoring Active C&D Monito Wells Active C Perfo&rnnarc D Monitoring Wells & NINA Wells Closed MSW Monitoring Wells & NINA Performance Monitoring Wells Offsite Constituent/Parameter Chloroethare Unit. u9/L a, 03/05/90 St. JEEIBac.kgroi-d, -- - -- onit ring We] MIV -- r -- -- r- - -- r -- -- r - -- -- ring r- - -- -- .• -- -- - - -- for th -- or a o:M nitoring Cl ad MSW Landfill -- - - -- -- -- -- -- -- - -- Pr ivate Well ND NC 2L = 3000 u9/L u9/L 03/21/91 - - - - -- - - -- -- -- -- -- -- - - - - - - - - -- - - -- -- - - -- - - - ND u9/L 03/10/92 _ _ _ _ __ _ _ __ __ __ __ __ __ _ _ _ _ _ _ _ _ __ _ _ _ __ _ _ __ _ _ _ NO u9/L 04/20/95 _ _ _ __ __ _ _ __ __ __ __ __ __ _ _ _ _ _ _ _ _ __ _ _ _ _ _ _ __ _ _ _ NO u9/L O6/27/95 - - - -- NO - -- -- -- -- -- -- -- -- - - - - - - - -- - - - - 13.3 4.2 6.6 8.5 -- - NO ug/L 09/22/95 - - - NO -- -- -- -- -- -- -- -- -- -- -- -- -- - - - NO -- - NO NO NO 12 14 NO NO -- - NO ug/L 03/28/96 - - - NO -- -- -- -- -- -- -- -- -- -- -- -- -- - - - - -- - NO NO - 23 14 NO NO -- - NO ug/L 10/29/96 - - - NO -- -- -- NO NO NO NO -- -- NO -- -- - - - - - -- - - - - NO NO NO NO NO - NO ug/L 04/08/97 - - - NO -- -- -- NO NO NO NO -- -- NO -- -- - - - - - -- - - - - 23 NO NO NO NO - NO ug/L 10/29/97 - - - NO -- NO -- NO NO NO NO -- -- NO -- -- - - - - - NO - - - - 17 NO NO NO NO - NO ug/L 04/30/98 - - - NO -- NO -- NO ND NO ND -- -- ND -- -- - - - - -- ND - - - - 19 ND NO NO NO - NO ug/L 10/14/98 - - - ND -- NO -- NO ND NO ND -- -- ND -- -- - - - - -- ND - - - - 16 ND NO ND NO - NO ug/L 04/27/99 - - - ND -- ND -- NO ND NO ND -- -- ND -- -- - - - - -- ND - - - - 15 ND NO ND NO - NO ug/L 10/21/99 - - - ND -- ND -- NO ND NO ND -- -- ND -- - - - - - -- NO - - - - 11 ND NO ND NO - NO ug/L 03/14/00 - - - NO -- ND -- NO NO NO NO -- -- NO -- - - - - - NO 2 - NO NO NO 6 NO NO NO 2 - NO ug/L .1.00 - - - NO -- ND -- NO NO NO NO -- -- NO -- - - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/17/00 - - - NO -- ND -- NO NO NO NO -- -- NO - - - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L .10/01 - - - NO -- ND -- NO NO NO NO -- -- NO - - - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/11/01 - - - NO -- ND -- NO ND NO ND -- -- ND - - - - - - -- NO - - -- -- NO ND NO ND NO - NO ug/L .1.02 - - - NO -- ND -- NO ND NO ND -- -- ND -- - - - - - -- NO - - -- -- NO ND NO ND NO - NO ug/L 10/O1/02 - - - NO -- ND -- NO ND NO ND -- -- ND -- - - - - - -- NO - - -- -- NO ND NO ND NO - NO ug/L 04/09/03 - - - NO -- ND -- NO ND NO ND -- -- ND -- - - - - - -- NO - - -- -- NO ND NO ND NO - NO ug/L 10/13/03 - - - NO -- ND -- -- -- NO NO -- -- NO NO NO - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/26/04 - - - NO -- ND -- -- -- NO NO -- -- NO NO NO - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/25/04 - - - NO -- ND -- -- -- NO NO -- -- NO NO NO - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L .04/05 - - - NO -- ND -- -- -- NO NO -- -- NO NO NO -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/04/05 - - - NO ND ND -- NO ND NO NO -- -- ND NO NO -- -- - - - NO - - - -- NO NO NO NO NO - NO ug/L 04/28/06 - - - NO -- ND -- -- -- NO NO -- -- ND NO NO -- - - - ND NO - ND ND ND NO NO NO NO NO - NO ug/L 10/09/06 - - - NO -- ND -- -- -- NO NO -- -- NO NO NO -- - - - ND NO - ND ND ND NO NO NO NO ND - NO ug/L .24/07 - - - NO -- NO -- -- -- NO NO -- -- NO NO NO -- - - - ND NO - ND ND ND NO NO ND NO NO - NO ug/L 10/30/07 - - 10 NO -- NO -- -- -- NO NO -- -- NO NO NO -- - - - NO NO - NO NO NO 1.3 J NO NO NO NO - NO ug/L 04/23/08 - - 10 NO -- NO -- -- -- NO NO -- -- NO NO NO -- - - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/06/08 - - 10 NO -- NO -- -- -- NO NO -- -- 1.2 J NO NO -- -- - - NO 2.0 J - NO NO NO 4.8 J 0.55 J 0.78 J 1.3 J 2.5 J - NO ug/L 04/13/09 - - 10 NO -- NO -- -- -- NO NO -- -- NO NO NO -- -- - - NO NO - ND NO NO NO NO 1.1 J NO NO - NO ug/L 10/15/09 - - 10 NO -- NO -- -- -- NO NO -- -- NO NO NO -- -- - - NO NO - ND NO NO NO NO NO NO NO - NO ug/L 04/26/10 - - 10 NO -- NO -- -- -- NO NO -- -- NO NO NO -- -- - - NO NO - ND ND ND NO NO ND ND ND - NO ug/L 10/19/10 - - 10 NO -- NO -- -- -- NO NO -- -- NO NO NO -- -- - - NO NO - ND ND ND NO NO ND ND ND - NO ug/L 04/18/11 - - 10 NO -- NO -- -- -- NO NO -- -- NO NO NO -- -- - - NO 0.80 J - ND ND ND NO NO ND ND ND - NO ug/L 10/10/11 - - 10 NO -- NO -- -- -- NO NO -- -- NO NO NO -- -- - - NO NO - ND ND ND NO -- ND NO Dry - NO ug/L 04/17/12 - - 10 NO -- NO -- -- -- NO NO -- -- NO NO NO -- -- - - NO NO - ND NO NO NO NO 0.54 J NO Dry - NO ug/L 10/09/12 - - 10 NO -- NO -- -- -- NO NO -- -- NO NO NO -- -- - - NO NO - ND NO NO NO NO NO NO Dry - NO ug/L 04/15/13 - - 10 NO -- NO -- -- -- NO NO -- -- 0.65 J NO NO -- - - - NO NO - ND NO NO NO NO 0.79 J NO Dry - NO ug/L 09/30/13 - - 10 NO -- NO -- -- -- NO NO -- -- NO NO NO -- - - - NO NO - ND NO NO NO NO NO NO Dry - NO ug/L 04/16/14 - - 10 NO -- NO -- -- -- NO NO -- -- NO NO NO -- - - - NO NO - ND ND ND NO NO ND NO Dry - NO ug/L 10/15/14 0.23 - 10 Dry -- NO -- -- -- NO NO -- -- NO NO NO -- - - - NO NO - ND ND ND NO NO NO NO Dry - NO ug/L 04/15/15 0.23 - 10 NO -- NO -- -- -- NO NO -- -- NO NO NO -- - - - NO NO - ND ND ND NO NO NO NO Dry - NO ug/L 10/07/15 0.23 - 10 NO -- NO -- -- -- NO NO -- -- ND NO NO -- - - - NO NO - ND ND ND NO NO NO NO NO - NO ug/L 04/11/16 0.23 - 10 NO -- NO -- -- -- NO NO -- -- NO NO NO -- - - - NO NO - ND NO NO NO NO NO NO NO - NO ug/L 11/30/16 0.23 - 10 NO -- NO -- -- -- NO NO -- -- NO NO NO -- - - - NO NO - ND NO NO NO NO NO NO NO - NO ug/L 04/11/17 0.23 - 10 NO -- NO -- -- -- NO NO -- -- NO NO NO -- - - - NO NO -- ND NO NO NO NO NO NO NO - NO ug/L 12/12/17 0.23 - 10 NO -- NO -- - -- NO NO -- -- NO NO NO -- - - - NO NO -- NO NO NO NO NO NO NO 0.65 J - NO ug/L O6/20/18 0.23 - 10 NO -- -- NO - -- NO NO -- -- ND NO NO -- - - - NO -- NO NO ND ND NO NO NO NO -- NO - ug/L 11/27/18 0.23 1 - NO -- -- NO - -- NO NO -- -- ND NO NO -- - - - NO -- NO ND ND ND NO NO NO NO -- NO NO ug/L 04/02/19 0.23 1 - NO -- -- NO - -- NO ND -- -- ND NO NO - - - - NO -- NO NO ND NO NO NO NO NO -- NO NO ug/L 11/19/19 0.23 1 - NO -- -- NO - -- NO ND -- -- ND -- -- NO ND - - NO - NO NO NO NO NO NO NO NO -- NO NO ug/L 04/07/20 0.23 1 - NO -- -- NO - -- NO NO -- -- NO -- -- NO NO NO - NO - NO - - - NO NO NO NO -- NO - ug/L 10/13/20 0.23 1 - NO -- -- NO - -- -- -- NO ND NO - -- NO NO NO ND NO - NO NO NO NO NO NO NO NO -- NO - 1,2-Dichloroben- ug/L 04/24/07 - - - NO -- NO -- - -- NO NO -- -- NO NO NO -- - - - NO NO -- NO NO NO NO NO NO NO NO - NO NC 2L=20 ug/L ug/L 04/28/07 - - - NO -- NO -- - -- NO NO -- -- NO NO NO -- - - - NO NO - NO NO NO NO NO NO NO NO - NO EPA MCL=600 ug/L ug/L 10/09/07 - - - NO -- NO -- - -- NO NO -- -- NO NO NO -- - - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/30/07 - - 5 ND -- 0.33 J -- -- -- NO ND -- -- 2.7 J 0.77 J ND -- - - - NO 0.39 J - NO 0.75 J NO NO ND 0.81 J 0.61 J NO - NO ug/L 04/23/08 - - 5 ND -- NO -- -- -- ND ND -- -- 2.1 J NO ND -- - - - NO NO - NO 0.43 J NO NO ND NO 0.69 J NO - NO ug/L 10/O6/08 - - 5 ND -- ND -- -- -- NO ND -- -- 1.5 J NO ND -- - - - NO NO - NO 0.42 J NO NO ND NO 0.64 J NO - NO ug/L 04/13/09 - - 5 NO -- ND -- -- -- ND NO -- -- 2.3 J 0.49 J NO -- - - - NO NO - NO 0.64 J NO NO NO NO 0.73 J NO - NO ug/L 10/15/09 - - 5 NO -- ND -- - -- NO NO -- -- 2.2 J 0.75 J NO -- - - - NO NO - 0.62 J 0.67 J NO NO NO 0.81 J 0.69 J NO - NO ug/L 04/26/10 - - 5 NO -- ND -- - -- NO NO -- -- 2.0 J NO NO -- - - - NO 0.50 J - NO 0.50 J NO NO NO NO 0.82 J NO - NO ug/L 10/19/10 - - 5 NO -- ND -- -- -- NO NO -- -- 2.1 J 0.57 J NO -- - - - NO NO - NO 0.53 J NO NO NO NO 0.88 J NO - NO ug/L 04/18/11 - - 5 NO -- ND -- - -- NO NO -- -- 2.0 J 0.64 J NO -- - - - NO NO - NO 0.43 J NO NO NO 0.51 J 0.67 J NO - NO ug/L 10/10/11 - - 5 NO -- NO -- -- -- NO NO -- -- 1.9 J 0.62 J ND -- - - - NO NO - 0.47 J 0.49 J NO NO - 0.86 J 0.49 J Dry - NO ug/L 04/17/12 - - 5 NO -- 0.36 J -- -- -- NO NO -- -- 2.0 J 0.75 J ND -- - - - NO 0.33 J - 0.49 J 0.64 J NO NO NO NO 0.66 J Dry - NO ug/L 10/09/12 - - 5 NO -- NO -- -- -- NO NO -- -- 2.0 J 0.54 J ND -- - - - NO NO - NO 0.49 J NO NO NO 0.48 J 0.76 J Dry - NO ug/L 04/15/13 - - 5 NO -- NO -- -- -- NO NO -- -- 1.7 J 0.56 J ND -- - - - NO NO - NO ND NO NO NO NO 0.65 J Dry - NO ug/L 09/30/13 - - 5 NO -- NO -- -- -- NO NO -- -- 1.2 J 0.45 J NO -- - - - NO NO - NO NO NO NO NO NO 0.72 J Dry - NO ug/L 04/16/14 - - 5 NO -- NO -- -- -- NO NO -- -- 1.7 J NO NO -- - - - NO NO - NO NO NO NO NO NO 0.68 J Dry - NO ug/L 10/15/14 0.19 - 5 Dry -- NO -- -- -- NO NO -- -- 1.3 J 0.54 J NO -- -- - - NO NO - NO NO NO NO NO 0.59 J 0.58 J Dry - NO ug/L 04/15/15 0.19 - 5 NO -- NO -- - -- NO NO -- -- 1.4 J 0.72 J NO -- -- - - NO NO - NO NO NO NO NO NO 0.51 J Dry - NO ug/L 10/07/15 0.19 - 5 NO -- ND -- - -- NO NO -- -- 1.1 J 0.50 J NO -- -- - - NO ND - NO 0.42 J NO NO NO 0.65 J NO NO - NO ug/L 04/11/i6 0.19 - 5 ND -- ND -- - -- NO NO -- -- 1.0 J 0.59 J NO -- -- - - NO NO - NO ND NO NO NO NO ND NO - NO ug/L 11/30/16 0.19 - 5 NO -- ND -- - -- NO ND -- -- 0.92 J NO ND -- -- - - NO ND - NO ND NO NO ND NO ND NO - NO ug/L 04/11/17 0.19 - 5 NO -- NO -- -- -- NO ND -- -- 0.94 J NO ND -- -- - - NO ND - NO ND NO NO ND 0.57 J ND NO - NO ug/L 12/12/17 0.19 - 5 NO -- NO -- -- -- NO NO -- -- 0.82 J 0.41 J NO -- -- - - NO NO - 0.44 J NO NO NO NO 0.59 J NO NO - NO ug/L O6/20/18 0.19 - 5 NO -- -- NO -- -- NO NO -- -- NO NO NO -- - - - NO -- NO NO NO NO NO NO NO NO - NO - ug/L 11/27/18 0.19 1 - NO -- -- NO -- -- NO NO -- -- 1.1 NO NO -- - - - NO -- NO NO NO NO NO NO NO NO - NO NO ug/L 04/02/19 0.19 1 - NO -- -- NO - -- NO NO -- -- 1.1 NO NO -- - - - NO -- NO NO NO NO NO NO NO NO - NO NO ug/L 11/19/19 0.19 1 - NO -- -- NO - -- NO NO -- -- 1.8 - -- NO NO - - NO -- NO NO NO NO NO 0.49 J 0.84 J 0.41 J - NO NO ug/L 04/07/20 0.19 1 - NO -- -- NO - -- NO ND -- -- 1.3 - -- NO NO 0.55 J - NO -- NO - - - NO NO ND NO - NO - ug/L 10/13/20 0.19 1 - ND -- -- NO - -- -- -- NO NO 1.6 - -- NO ND 0.52 J NO NO -- NO NO ND NO NO NO 0.54 J NO - - spa..ms,.eo�,E��,a �ozw�r-zo.w.0 MPon­.-LI.-M.-­ ----12ozo-2oznw-moo -F..- 1-o.a,.a.. P,.9a17 TABLE 5 Summary of Historical Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SBME Project No. 4358-20-043A Detected Monitoring eq.9 Active C&D Monito Wells Active C&D Performarc Monitoring Wells & NINA Wells Closed MSW Monitoring Wells & NINA Performance Monitoring Wells Offsite Constituent/Parameter 1,4-Dichlorohenzene Units ug/L at. 03/05/90 INNIBac.k�r-nd,. -- - -- onit ring We] MIV -- -- r -- r- - -- r -- -- r -- - -- ring r- - -- -- .• -- -- - - -- for th Cl a -- or o:M nitoring ad MSW -- Landfill - - -- -- -- -- -- -- - -- Private Well ND NC 2L = 6 ug/L ug/L 03/21/91 ND EPA MCL = 75 ug/L ug/L 03/10/92 - - - - -- - - -- -- -- -- -- -- - - - - - - - - -- - - - -- -- - -- - - - NO ug/L 04/20/95 _ _ _ __ __ _ _ __ __ __ __ __ __ __ _ _ _ _ _ _ _ __ _ _ __ __ __ _ _ _ _ _ NO ug/L O6/27/95 _ _ _ __ NO __ __ __ __ __ __ __ __ __ _ _ _ _ _ _ _ __ _ _ __ __ NO 3.3 2 7.4 - - NO ug/L 09/22/95 - - - NO -- -- -- -- -- -- -- -- -- -- -- -- -- - - - NO -- - NO NO NO NO NO NO NO - - NO ug/L 03/28/96 - - - NO -- -- -- -- -- -- -- -- -- -- -- -- -- - - - - -- - NO NO - NO NO NO NO - - NO ug/L 10/29/96 - - - NO -- ND -- NO NO NO NO -- -- NO -- -- - - - - -- NO - - - - NO NO NO NO NO - NO ug/L 04/08/97 - - - NO -- ND -- NO NO NO NO -- -- 6 -- -- - - - - -- NO - - - - NO NO NO 7 6 - NO ug/L 10/29/97 - - - NO -- ND -- NO NO NO NO -- -- 7.8 - -- - - - - -- NO - - - -- NO NO NO 7 6.1 - NO ug/L 04/30/98 - - - NO -- ND -- NO ND NO ND - -- NO - - - - - - -- NO - - - -- NO NO NO 7.1 NO - NO ug/L 10/14/98 - - - ND -- ND -- NO ND NO ND - -- 9.7 - - - - - - - NO - - - -- NO ND NO 5.2 NO - NO ug/L 04/27/99 - - - ND -- ND -- NO ND NO ND -- -- 8.7 -- - - - - - - NO - - -- -- NO ND NO 5.9 5.6 - NO ug/L 10/21/99 - - - ND -- ND -- NO ND NO ND -- -- NO -- - - - - - - NO - - -- -- NO ND NO NO 21 - NO ug/L 03/14/00 - - - NO -- 3 -- NO 3 NO NO -- -- 2 - - - - - - NO NO - NO 3 NO NO NO NO 4 NO - NO ug/L .1.00 - - - NO -- ND -- NO NO NO NO -- -- 7.5 - - - - - - -- NO - - - -- NO NO NO NO 6.4 - NO ug/L 10/17/00 - - - NO -- ND -- NO NO NO NO -- -- 9.5 - - - - - - -- NO - - - -- NO NO NO 10 6.3 - NO ug/L .10/01 - - - NO -- ND -- NO NO NO NO -- -- 6.7 -- - - - - - -- NO - - - -- NO NO NO 5.1 5.9 - NO ug/L 10/11/01 - - - NO -- ND -- NO ND NO ND -- -- NO -- - - - - - -- NO - - -- -- NO ND NO 5.6 8.3 - NO ug/L .1.02 - - - NO -- ND -- NO ND NO ND -- -- NO -- - - - - - -- NO - - -- -- NO ND NO 5.9 ND - NO ug/L 10/01/02 - - - NO -- ND -- NO ND NO ND -- -- ND -- - - - - - -- 5.1 - - -- -- NO ND NO 5.7 ND - NO ug/L 04/09/03 - - - NO -- ND -- NO ND NO ND -- -- ND -- - - - - - -- NO - - -- -- NO ND NO 53 7.5 - NO ug/L 10/13/03 - - - NO -- ND -- -- -- NO NO -- -- NO NO NO - - - - -- NO - - -- -- NO NO NO 18 7.8 - NO ug/L 04/26/04 - - - NO -- ND -- -- -- NO NO -- -- 5.1 NO NO - - - - -- NO - - -- -- NO NO NO 5.9 6.9 - NO ug/L 10/25/04 - - - NO -- ND -- -- -- NO NO -- -- NO NO NO - - - - -- NO - - -- -- NO NO NO NO NO - NO ug/L .04/05 - - - NO -- ND -- -- -- NO NO -- -- NO NO NO -- -- - - -- NO - - -- -- NO NO NO NO 6.1 - NO ug/L 10/04/05 - - - NO NO ND -- NO ND NO NO -- -- NO NO NO -- -- - - - NO - - - -- NO NO NO NO 6.6 - NO ug/L 04/28/06 - - - NO -- NO -- -- -- ND NO - -- NO NO NO -- - - - ND NO - ND NO ND NO NO NO NO 6.8 - NO ug/L 10/09/06 - - - NO -- NO -- - -- ND NO - -- NO ND NO -- - - - ND NO - NO NO ND NO NO ND NO 6 - NO ug/L .24/07 - - - NO -- NO -- - - ND NO - -- 53 NO NO -- - - - ND NO - NO NO ND NO NO ND 3.5 5.7 - NO u9/L 10/30/07 - - 1 NO -- 2.1 -- - - 0.97 J 0.54 J - -- 17 1.1 NO -- - - - NO 3.4 - NO 1.9 NO 2.0 0.49 J 4.0 3.0 3.3 - NO ug/L 04/23/08 - - 1 NO -- NO -- - - NO 3.5 - -- 5.5 NO NO -- - - - NO 3.6 - NO 1.8 NO NO NO NO 4.2 NO - NO ug/L 10/06/08 - - 1 NO -- ND -- - - 0.44 J 0.60 J - -- 4.9 NO NO -- -- - - NO 3.3 - NO NO NO NO 1.5 NO 3.6 5.8 - NO u9/L 04/13/09 - - 1 NO -- 2.1 -- - - 0.70 J 0.85 J - -- 6.9 1.1 NO -- -- - - NO 1.2 - NO 2.3 NO 1.6 NO 0.97 J 4.2 5.9 - NO ug/L 10/15/09 - - 1 NO -- 2.2 -- - - NO ND - -- 5.5 1.8 NO -- -- - - NO 3.2 - NO 2.6 NO 3.4 1.6 4.1 3.7 5.3 - NO ug/L 04/26/10 - - 1 NO -- NO -- - - 1.1 0.66 J - -- 6.0 ND NO -- -- - - NO 3.6 - NO 2.0 ND 1.8 1.2 0.67 J 3.9 4.9 - NO ug/L 10/19/10 - - 1 NO -- NO -- -- -- NO 0.59 J - -- 4.2 ND NO -- -- - - NO 2.8 - NO NO ND NO NO 1.8 3.9 5.3 - NO ug/L 04/18/11 - - 1 NO -- 1.6 -- - - 1.7 NO - -- 5.0 NO NO -- -- - - NO 3.2 - NO 1.5 ND 1.7 0.92 J 3.0 3.0 14 - NO ug/L 10/10/11 - - 1 NO -- NO -- - - 1.5 NO - -- 5.1 1.7 NO -- -- - - NO 2.9 - 0.82 J NO ND 4.0 - 4.1 3.1 Dry - NO u9/L 04/17/12 - - 1 NO -- NO -- - - ND 0.50 J - -- 12 1.5 NO -- -- - - NO 3.0 - NO 2.2 NO 4.3 1.1 2.6 4.0 Dry - NO ug/L 10/09/12 - - 1 NO -- NO -- - - NO 0.61 J - -- 5.1 NO NO -- -- - - NO 3.3 - NO NO NO 3.7 1.8 3.3 4.9 Dry - NO ug/L 04/15/13 - - 1 NO -- 2.0 -- - - 0.89 J 0.52 J - -- 4.7 1.3 NO -- -- - - NO 3.1 - NO 1.9 NO 3.2 0.74 J 1.1 3.9 Dry - NO ug/L 09/30/13 - - 1 NO -- 2.2 -- - - 0.63 J 0.66 J - -- 4.4 NO NO - - - - NO 0.99 J - NO NO NO 3.0 1.4 0.41 J 3.9 Dry - NO ug/L 04/16/14 - - 1 NO -- 1.9 -- - - NO NO - -- 4.7 NO NO - - - - NO 2.0 - NO ND ND 3.1 0.83 J 0.60 J 3.7 Dry - NO ug/L 10/15/14 0.19 - 1 Dry -- NO -- - - NO NO - -- 4.0 NO NO - - - - ND 2.4 - NO ND ND 2.4 1.6 4.1 3.3 Dry - NO ug/L 04/15/15 0.19 - 1 NO -- 2.1 -- - - 0.41 J NO -- -- 4.0 1.3 NO - - - - 0.45 J NO - NO ND ND 1.2 0.58 J 0.72 J 3.4 Dry - NO ug/L 10/07/15 0.19 - 1 NO -- NO -- - - 0.71 J 0.52 J -- -- 3.9 0.84 J ND - - - - ND 3.0 - ND ND ND 2.3 1.4 5.4 3.3 7.8 - NO ug/L 04/11/i6 0.19 - 1 NO -- 2.1 -- - - NO 0.64 J -- -- 4.8 1.2 0.47 J - - - - NO 2.1 - NO NO NO 1.4 NO 2.3 3.1 5.4 - NO ug/L 11/30/16 0.19 - 1 NO -- NO -- - - 0.65 J 0.44 J -- -- 3.5 NO NO - - - - NO 2.7 - NO NO NO 1.9 1.3 IS 2.5 4.8 - NO ug/L 04/11/17 0.19 - 1 NO -- NO -- - - 1.3 0.50 J -- -- 4.4 NO NO - - - - NO 3.5 - NO 1.7 NO 2.8 0.63 J 6.1 3.6 5.0 - NO ug/L 12/12/17 0.19 - 1 NO -- NO -- - - 1.3 NO -- -- 2.7 NO NO - - - - NO 1.9 - 0.97 J 1.2 NO 2.4 1.3 4.6 2.7 5.1 - NO ug/L O6/20/18 0.19 - 1 NO -- -- 1.7 - - 0.64 J NO -- -- 4.3 NO NO - - - - NO - 2.8 NO 1.9 ND 2.9 0.72 J 3.4 2.6 - 0.89 J - ug/L 11/27/18 0.19 1 - NO -- -- 2.1 - - NO 0.62 J -- -- 4.2 NO 0.43 J - - - - NO - 2.3 NO 0.53 J ND 2.6 NO 1.2 2.7 - 0.89 J NO ug/L 04/02/19 0.19 1 - NO -- -- 2.9 - - NO 0.76 J -- -- 4.2 ND 0.93 J - - - - NO - 2.6 NO 0.74 J ND 2.0 NO 1.2 2.6 - 1.3 NO ug/L 11/19/19 0.19 1 - NO -- -- 2.0 - - ND ND -- -- 5.6 - - ND ND - - 0.46 J - 2.9 0.45 J 1.2 ND 2.3 3.0 6.2 2.9 - 5.8 NO ug/L 04/07/20 0.19 1 - NO -- -- 2.1 - - 0.89 J 0.55 J -- -- 5.1 - - NO NO 2.1 - NO - 2.9 - - -- 1.3 NO 2.5 2.6 - 0.92 J - ug/L 10/13/20 0.19 1 NO 2.6 NO NO 5.1 NO NO 1.8 NO NO 3.1 NO 0.59 J NO 1.7 NO 5.3 3.1 0.73 J 1,1,-Dichloroethane ug/L 03/05/90 -- -- - - -- -- -- - - - -- -- -- - - - - - - - - - - - - - - - - - - - NO NC 2L = 6 ug/L ug/L 03/21/91 _ _ _ _ __ __ __ _ _ _ __ __ __ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ NO ug/L 03/10/92 _ _ _ _ __ __ __ _ _ _ _ __ __ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ NO ug/L 04/20/95 _ _ _ _ __ __ __ _ _ _ _ __ __ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ NO ug/L O6/27/95 - - - - NO -- -- - -- - - -- -- - - - - - - - - - - - - - 7.9 9.3 13.4 9.6 -- - NO ug/L 09/22/95 - - - NO -- -- -- - -- - - - -- - - - - - - - NO - - NO 9 NO 18 10 19 12 -- - NO ug/L 03/28/96 - - - NO -- - -- - -- - - - -- -- -- - - - - - - - - ND 11 - ND 14 ND 10 -- - NO ug/L 10/29/96 - - - NO -- 19 -- NO ND NO 6 - -- NO -- - - - - - - NO - - - - 70 7 NO 7 80 - NO ug/L 04/08/97 - - - NO -- 22 -- NO 21 6 8 - -- 14 -- - - - - - - 16 - - - - 74 5 NO 6 72 - NO ug/L 10/29/97 - - - NO -- 20 -- NO 18 NO 6.8 - -- 12 -- -- - - - - - 22 - - - - 64 6.2 8.3 7.5 72 - NO ug/L 04/30/98 - - - NO -- 21 -- NO 18 NO 6.7 - -- NO -- -- - - - - - NO - - - - 45 8.1 NO 5.3 60 - NO ug/L 10/14/98 - - - NO -- ND -- 6.1 15 NO 5.2 - -- 8.4 -- -- - - - - - 9.8 - - - - 50 NO ND NO 46 - NO ug/L 04/27/99 - - - NO -- 21 -- NO 18 NO NO - -- 9.7 -- -- - - - - - 7.8 - - - - 37 NO NO 5.6 39 - NO ug/L 10/21/99 - - - NO -- ifi -- ND 13 ND ND - -- ND -- -- - - - - - 5.1 - - - - 12 NO NO NO 24 - NO ug/L 03/14/00 - - - NO -- 14 -- NO 10 NO 2 - -- NO -- -- -- - - - ND 4 - ND 4 NO 12 NO NO NO 20 - NO ug/L .19/00 - - - NO -- 17 -- NO 14 NO NO - -- 5.9 -- -- -- - - - - 6.4 - - - -- 19 NO NO NO 23 - NO u9/L 10/17/00 - - - NO -- 17 -- NO 12 NO NO - -- NO -- -- -- - - - - 9.6 - - - -- 909 NO NO NO 24 - NO ug/L .1.1 - - - NO -- 18 -- NO 13 NO NO -- -- 5.5 -- -- -- - - - - 8.4 - - - - 9.2 NO NO NO 23 - NO ug/L 10/11/01 - - - NO -- 16 -- NO 11 NO NO -- -- NO -- -- -- - - - - 11 - - - - 16 NO 6 NO 22 - NO ug/L .18/02 - - - NO -- 13.8 -- NO 9.3 NO NO -- -- ND -- -- -- - - - - 9.9 - - - - 5.5 NO NO NO NO - NO ug/L 10/08/02 - - - NO -- 10.9 -- NO 7.6 NO NO -- -- ND -- -- - - - - - 9 - - - - 5.7 NO NO NO ND - NO ug/L 04/09/03 - - - ND -- .7-- NO 7.3 NO ND -- -- ND -- -- - - - - - 6.8 - - - -- NO ND NO ND 9.5 - NO ug/L 10/13/03 - - - NO -- -- -- NO -- NO ND -- -- ND NO 6.9 - - - - - 5.1 - - - -- NO ND NO ND 11.7 - NO ug/L 04/26/04 - - - NO -- 10.6 -- NO -- NO NO -- -- NO NO 6.9 - - - - - 14 - - - -- NO NO NO NO 10.7 - NO u9/L 10/25/04 - - - NO -- -- -- NO -- NO NO -- -- NO NO NO - - - - - NO - - - -- NO NO NO NO 8.5 - NO ug/L 04/04/05 - - - NO -- 8.4 -- NO -- NO NO -- -- NO NO NO - - - - -- NO - - - -- NO NO NO NO 11.5 - NO ug/L 10/04/05 - - - NO NO NO -- NO NO NO NO -- -- NO NO NO - - - - - NO - - - -- NO NO NO NO 10.7 - NO ug/L 04/28/06 - - - NO -- 7.6 -- -- -- -- NO -- -- NO NO NO - - - - NO NO - NO NO NO NO NO NO NO 10.1 - NO ug/L 10/09/06 - - - ND -- 7.9 -- -- - NO ND -- -- ND NO NO - - - - NO NO - ND ND ND NO NO NO NO 17.7 - NO ug/L 04/24/07 - - - ND -- 7.5 -- - ND ND -- -- NO ND NO - - - - NO NO - NO NO ND NO NO ND NO 5.9 - NO ug/L 10/30/07 - - 5 ND -- 7.8 -- -- - 3.4 J 3.5 J - -- 1.0 J 1.5 J 1.4 J - - - - 0.69 J 5.2 - NO 1.1 J NO 1.4 J 0.38 J 4.3 J 0.51 J 3.6 J - NO ug/L .23/08 - - 5 NO -- 5.8 -- -- - ND 5.1 - -- 1.2 J 1.0 J NO - - - - NO 2.8 J - ND 0.84 J NO NO 0.76 J NO 0.87 J 1.0 J - NO ug/L 10/06/08 - - 5 NO -- 7.0 -- -- - NO 0.42 J - -- 1.2 J 0.76 J 1.3 J - - - - NO 2.8 J - ND 0.61 J NO NO NO NO 0.83 J 7.4 - NO ug/L 04/13/09 - - 5 NO -- 4.9 J -- - - NO NO - -- 0.79 J 0.74 J 0.74 J - - - - NO 0.50 J - ND 0.77 J NO 0.67 J NO 0.65 J 0.74 J 4.7 J - NO ug/L 10/15/09 - - 5 NO -- 4.4 J -- - -- NO NO - -- 0.71 J 1.0 J 0.67 J - - - - 0.78 J 1.8 J - ND 0.76 J NO 1.1 J NO 1.2 J 0.45 J 2.4 J - NO ug/L 04/26/10 - - 5 NO -- 4.7 J -- -- -- NO NO - -- 0.64 J NO 0.85 J - - - - NO 1.6 J - ND 0.56 J NO 0.51 J NO 0.86 J 0.49 J 2.8 J - NO ug/L 10/19/10 - - 5 NO -- 5.0 -- -- -- NO NO -- -- 0.68 J 0.53 J 0.79 J - - - - NO 1.2 J - ND 0.59 J NO 0.75 J NO 0.74 J 0.59 J 2.7 J - NO ug/L 04/18/11 - - 5 NO -- 4.2 J -- - -- NO NO -- -- 0.68 J 0.83 J 0.697 J - - - - ND 1.4 J - ND 0.47 J NO 0.51 J NO 1.0 J 0.50 J 2.0 J - NO ug/L 10/10/11 - - 5 NO -- 3.8 J -- - -- NO NO -- -- 0.78 J 0.85 J 0.65 J - - - - 0.42 J 1.4 J - ND 0.53 J NO 0.91 J -- 1.0 J 0.45 J Dry - NO ug/L 04/17/12 - - 5 NO -- 4.1 J -- - -- NO NO -- -- 0.66 J 0.71 J 0.46 J - - - - ND 1.2 J - ND 0.51 J NO 0.87 J NO 1.0 J 0.40 J Dry - NO ug/L 10/09/12 - - 5 NO -- 4.2 J -- - -- NO NO -- -- 0.58 J 0.59 J 0.46 J - - - - NO 1.0 J - ND 0.64 J NO 0.46 J NO 0.75 J 0.55 J Dry - NO ug/L 04/15/13 - - 5 NO -- 5.6 -- - -- NO NO -- -- 0.49 J 0.64 J 0.60 NO 1.1 J - ND NO NO 0.53 J NO 0.85 J 0.45 J Dry - NO ug/L 09/30/13 - - 5 NO -- 2.9 J -- -- -- NO NO -- -- NO NO 0.73 J - - - - NO NO - ND NO NO 0.49 J 0.42 J NO NO Dry - NO ug/L 04/16/14 - - 5 NO -- 3.8 J -- -- -- NO NO -- -- NO NO 1.6 J - - - - NO 0.47 J - ND NO NO 0.53 J NO 0.45 J 0.42 J Dry - NO ug/L 10/15/14 0.13 - 5 Dry -- 4.2 J -- -- -- NO NO -- -- ND NO 0.80 J - - - - NO 0.59 J - ND ND NO 0.50 J NO 0.87 J NO Dry - NO ug/L 04/15/15 0.13 - 5 NO -- 3.0 J -- -- -- NO NO -- -- ND 0.44 J NO - - - - NO 0.49 J - ND ND NO ND NO NO NO Dry - NO ug/L 10/07/15 0.13 - 5 NO -- 3.9 J -- -- -- ND ND -- -- 0.73 J ND 0.45 J - - - - NO 0.53 J - ND ND ND 0.58 J NO 0.62 J ND 1.1 J - NO ug/L 04/11/i6 0.13 - 5 NO -- 1.7 J -- -- -- NO ND -- -- 0.66 J ND 0.62 J - - - - ND 0.42 J - ND ND NO NO ND 0.61 J ND 0.90 J - NO ug/L 11/30/16 0.13 - 5 NO -- 1.9 J -- -- -- NO NO -- -- 0.59 J NO 0.48 J - - - - NO 0.44 J - ND NO NO NO NO 0.70 J NO 0.77 J - NO ug/L 04/11/17 0.13 - 5 NO -- 2.8 J -- -- -- NO NO - -- 0.61 J NO 0.68 J - - - - NO 0.58 J - ND 0.44 J NO NO NO 1.1 J NO NO - NO ug/L 12'12/17 0.13 - 5 NO -- 1.7 J -- -- -- NO NO - -- NO NO NO - - - - NO NO -- ND NO NO NO NO 0.46 J NO 0.66 J - NO ug/L O6120/18 0.13 - 5 NO -- -- NO - -- NO NO - -- NO NO NO - - - - NO - NO NO NO NO NO NO 0.49 J NO - NO - ug/L 11/27/18 0.13 1 - NO -- -- 0.64 J - -- NO NO - -- 0.50 J NO NO - - - - NO - NO NO NO NO NO NO NO NO - NO NO ug/L 04/02/19 0.13 1 - NO -- -- NO - -- NO ND - -- ND NO 0.76 J - - - - NO - NO NO ND NO NO ND ND ND - NO ND ug/L 11/19/19 0.13 1 - NO -- -- NO - -- NO NO - -- ND -- - NO NO - - NO - ND NO ND NO NO ND ND ND - 0.93 J ND ug/L 04/07/20 0.13 1 - NO -- -- NO - -- NO NO - -- NO -- - NO NO NO - NO - NO - -- -- NO NO NO NO - NO - ug/L 10/13/20 0.13 1 NO 0.43 J ND NO NO NO NO ND NO NO ND NO NO ND ND ND 0.56 J ND NO z�snaremsMeq+,Ervvw,awns�zoswasasuw.0 Mwrecwm .- Lrcawo ram-- --uaw-12-2osnw-­- ray Ewmzos 1-o.a.w.. Psge 10 m17 TABLE 5 Summary of Historical Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SBME Project No. 4358-20-043A Detected .,"It,rl P. "g Constituent/ rameter 1,2-Dichloroethane NC 2L = 0.4 ug/L EPA MCL=5 ug/L Linits u9/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L u9/L ug/L ug/L ug/L ug/L ug/L u9/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L Is 10130i07 04/23/08 10/06/08 04/13/09 10/15/09 04/26/10 10/19/10 04/18/11 10/10/11 04/17/12 10/09/12 04/15/13 09/30/13 04/16/14 10/15/14 04/15/15 10/07/15 04/11/16 11/30/16 04/11/17 12/12/17 O6/20/18 11/27/18 04/02/19 11/19/19 04/07/20 St. JENkc1grourid - - - - - - - - - - - - - 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21 0.21 - - - - - - - - - - - - - - - - - - - - - 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 - - - .'.ran we] ND ND ND ND NO NO NO NO ND NO ND NO NO Dry NO NO NO NO ND ND ND NO NO NO NO r -- ND -- ND -- ND -- ND -- 0.45 J -- ND -- 0.48 J -- ND -- 0.40 J -- ND -- ND -- ND -- ND -- ND -- ND -- ND -- ND -- ND -- NO -- NO -- -- -- -- -- -- -- -- r- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- NO NO NO NO NO -- -- -- -- -- -- -- -- -- -- -- - - - - - - - - - -- -- -- -- r -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- NO NO NO NO NO NO NO NO ND NO ND NO NO NO NO NO NO NO NO NO NO NO NO NO NO r NO NO NO NO NO NO NO NO ND NO ND ND ND NO NO NO NO ND ND ND ND NO NO NO NO Active C&D Monitoring - -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- NO Wells r- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- NO ND ND ND ND NO NO NO NO NO ND ND ND ND NO NO NO NO ND ND ND ND NO NO NO NO ND NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO - .D NO NO NO NO NO NO NO NO NO NO ND ND ND NO NO NO NO ND ND ND ND NO NO -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- - NO NO r -- - - - - - -- -- -- -- -- -- -- -- -- -- -- -- - - - - - NO NO - - - - - - - - - - - - - - - - - - - - - - - - NO - - - - - - - - - - - - - - - - - - - - - - - - NO Active C D Perfo&rnnarc for Cl the NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO Monitoring or o:M nitoring ad MSW ND ND ND NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO - - -- -- Wells Landfill & NINA Wells - - - - - - - - - - - - - - - - - - -- -- -- NO NO NO NO NO NO NO NO NO ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NO NO NO NO NO ND ND ND NO NO NO NO NO ND ND ND 1.4 NO NO NO NO ND ND ND ND NO NO NO NO Closed MSW ND ND ND ND NO NO NO NO NO ND ND ND ND NO NO NO NO ND ND ND ND NO NO NO NO Monitoring NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO Wells & NINA Performance ND NO NO NO NO NO NO - NO ND ND ND ND NO NO NO NO ND ND ND ND NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO Monitoring Wells ND NO NO NO NO NO NO NO NO NO ND ND ND NO NO NO NO ND ND ND ND NO NO NO NO NO NO NO NO NO NO NO Dry Dry Dry Dry Dry Dry Dry Dry NO NO ND ND ND - -- -- -- - - - - - - - - - - - - - - - - - - - - NO NO NO NO NO Offsite Private Well NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO - NO NO NO cis-1,2-Dichloroethene ug/L 04/28/06 - - - NO -- 31 -- - - -- NO - -- 16.3 13.1 8.4 - - - - ND 13.9 -- NO 6.4 NO 19.6 NO ND NO 18.4 - NO NC 2L = 70 ug/L ug/L 10/09/06 - - - NO -- 26.3 -- - - ND NO - -- 17.3 11.3 8.6 - - - - ND 12 - NO 5.1 NO 14.3 9.5 ND 9.3 19.4 - NO EPA MCL = 70 ug/L ug/L 04/24/07 - - - NO -- 27.4 -- - - ND 5 - -- 19.3 8.7 12.1 - - - - NO 8.3 - NO NO NO 15.3 NO NO NO 7.3 - ND ug/L 10/30/07 - - 5 NO -- 25 -- - - 3.8 J 3.0 J - -- 20 12 5.3 - - - - 4.4 J 9.8 - NO 5.1 0.35 J 14 6.4 3.0 J 1.6 J 17 - NO ug/L 04/23/08 - - 5 NO -- 19 -- - - 3.6 J 11 - -- 20 7.0 NO - - - - NO 9.8 - NO 3.0 J NO 3.8 J 3.1 J NO 2.2 J 3.2 J - NO ug/L 10/06/08 - - 5 NO -- 22 -- - - 1.6 J 3.2 J - -- 14 5.2 4.3 J - - - - NO 8.7 - NO 2.8 J NO 5.1 18 NO 2.5 J 12 - NO u9/L 04/13/09 - - 5 NO -- 19 -- - - 2.8 J 3.6 J - -- 14 6.4 2.4 J - - - - NO 2.3 J - NO 3.7 J NO 6.1 NO NO 2.9 J 12 - NO ug/L 10/15/09 - - 5 NO -- 22 -- - - 4.3 J 2.0 J - -- 17 12 3.0 J - - - - 6.2 8.1 - 1.9 J 4.6 J 0.41 J 15 5.1 5.0 1.8 J 16 - NO ug/L 04/26/10 - - 5 NO -- 18 -- - - 3.0 J 2.6 J - -- 13 5.2 2.9 J - - - - 0.60 J 8.0 - NO 2.8 J 0.43 J 7.5 3.2 J NO 2.3 J 7.2 - NO ug/L 10/19/10 - - 5 NO -- 23 -- -- -- 3.4 J 2.6 J - -- 13 6.8 4.4 J - - - - NO 17 - NO 3.0 J NO 8.4 NO ND 2.8 J 10 - NO ug/L 04/18/11 - - 5 NO -- 18 -- - - 2.8 J 2.1 J - -- 12 8.2 2.0 J - - - - NO 6.3 - NO 2.8 J NO 6.8 3.4 J ND 1.9 J 11 - NO ug/L 10/10/11 - - 5 NO -- 19 -- - - 3.4 J 2.0 J - -- 12 9.1 3.4 J - - - - 3.0 J 6.7 - 1.5 J 2.6 J NO 13 - 2.8 J 1.6 J Dry - NO ug/L 04/17/12 - - 5 NO -- 19 -- - - 3.3 J 1.9 J - -- 11 8.0 0.88 J - - - - 1.8 J 6.4 - 1.4 J 2.2 J 0.39 J 16 2.8 J ND 1.6 J Dry - NO ug/L 10/09/12 - - 5 NO -- 18 -- - - 2.2 J 1.6 J - -- 7.0 5.5 2.5 J - - - - NO 6.6 - 1.5 J 2.5 J NO 9.1 3.2 J NO 2.0 J Dry - NO ug/L 04/15/13 - - 5 NO -- 23 -- - - 1.8 J 1.9 J - -- 7.3 6.6 2.0 J - - - - NO 6.9 - NO 1.7 J NO 11 1.2 J NO 1.7 J Dry - NO ug/L 09/30/13 - - 5 NO -- 14 -- - - 1.2 J 1.9 J - -- 4.0 J 4.3 J 3.20 J - - - - NO 1.8 J - NO 1.2 J NO 5.6 2.7 J ND 1.7 J Dry - NO ug/L 04/16/14 - - 5 NO -- 16 -- - - 0.66 J 1.9 J - -- 6.7 2.1 J 6.8 - - - - NO 2.4 J - NO 1.6 J NO 6.8 1.6 J NO 2.1 J Dry - NO ug/L 10/15/14 0.15 - 5 Dry -- 17 -- - - 1.3 J 1.4 J - -- 5.3 5.5 4.9 J - - - - 0.43 J 2.9 J - 0.70 J 1.9 J NO 4.3 J 2.5 J ND 1.2 J Dry - NO ug/L 04/15/15 0.15 - 5 NO -- 14 -- - - 0.76 J 0.72 J - -- 3.4 J 6.4 3.7 J - - - - 3.1 J 2.2 J - NO 2.0 J NO 1.6 J 0.47 J ND 0.89 J Dry - NO ug/L 10/07/15 0.15 - 5 NO -- 15 -- - - 1.3 J 1.5 J - -- 4.3 J 2.5 J 2.9 J - - - - NO 2.5 J - NO 1.7 J NO 2.6 J 2.7 J NO 0.69 J 1.5 J - NO ug/L 04/11/16 0.15 - 5 NO -- 8.6 -- - - 0.82 J 1.4 J - -- 3.1 J 3.9 J 3.9 J - - - - 1.0 J 1.1 J - NO 0.88 J NO 2.0 J 0.49 J 0.50 J 0.85 J 0.42 J - NO ug/L 11/30/16 0.15 - 5 NO -- 8.8 -- - - 0.79 J 0.94 J - -- 3.6 J 1.7 J 3.9 J - - - - 0.58 J 1.5 J - NO 0.68 J NO 2.0 J 2.1 J 0.52 J 0.63 J 0.53 J - NO ug/L 04/11/17 0.15 - 5 NO -- 10.0 -- - - 1.4 B 1.3 11 - -- 3.0 J 3.0 J 3.8 J - - - - NO 1.2 B - NO 1.9 B NO 2.5 B NO 0.66 B 0.60 B NO - NO ug/L 12/12/17 0.15 - 5 NO -- 9.9 -- - - 1.6 J 0.84 J - -- 2.2 J 3.4 J 4.3 J - - - - NO 1.6 J - 1.1 J 0.81 J NO 0.68 J 1.8 J 2.0 J 0.84 J 1.0 J - NO ug/L O6/20/18 0.15 - 5 NO -- -- 2.6 J - - ND NO - -- 3.0 J NO 2.8 J - - - - NO - 1.6 J NO 1.2 J NO 4.4 J 1.0 J NO 0.54 J - 1.9 J - ug/L 11/27/18 0.15 1 - NO -- -- 3.6 - - 0.40 J 1.5 - -- 3.0 ND 3.1 - - - - 0.80 J - 1.8 NO NO NO 3.3 0.64 J ND 1.0 - 1.6 NO ug/L 04/02/19 0.15 1 - NO -- -- 3.3 - - 0.62 J 0.98 J - -- 2.3 ND 4.8 - - - - NO - 1.1 NO 0.44 J NO 1.3 NO NO 1.3 - 2.5 NO ug/L 11/19/19 0.15 1 - NO -- -- 2.4 - - 1.1 0.71 J - -- 3.9 - - 1.8 NO - - 1.5 - 1.1 0.72 J 0.84 J NO 1.5 2.0 NO 0.43 J - 0.76 J NO ug/L 04/07/20 0.15 1 - NO -- -- NO - - NO NO - -- NO - - ND NO 3.9 - NO - ND - - - 1.9 NO NO NO - 2.1 - ug/L 10/13/20 0.15 1 NO 3.0 NO 0.96 J 1.7 NO NO 3.8 NO NO 1.7 NO NO NO 3.1 7.8 0.43 J 0.74 J 1.6 Ethylbenzene ug/L 03/05/90 -- -- - - -- -- -- - - - - - -- - - - - - - - - - - - - - - - - - - - NO NC 2L = 600 ug/L ug/L 03/21/91 - - - - -- -- -- -- - -- -- - -- - - - - - - - - - - - - - - -- - - - - NO EPA MCL = 700 ug/L ug/L 03/10/92 - - - - -- -- -- -- - -- -- - -- -- - - - - - - - - - - - - - -- - - - - NO ug/L 04/20/95 _ _ _ _ __ __ __ __ __ __ __ _ __ __ _ _ _ _ _ _ _ __ _ _ _ _ __ __ _ _ _ _ NO ug/L O6/27/95 - - - -- NO -- -- -- -- -- -- - -- -- - - - - - - - -- - - - - NO ND NO ND -- - NO ug/L 09/22/95 - - - NO -- -- -- -- -- -- -- - -- -- - - - - - - NO -- - ND ND NO NO ND NO ND -- - NO ug/L 03/28/96 - - - NO -- -- -- -- -- -- -- - -- -- -- - - - - - - -- - ND ND - NO ND NO ND - - NO ug/L 10/29/96 - - - NO -- NO -- NO NO NO NO - -- ND -- - - - - - -- NO - - - - NO NO NO NO ND - NO ug/L 04/08/97 - - - NO -- ND -- NO NO NO NO - -- NO -- - - - - - -- NO - - - - NO NO NO NO NO - NO ug/L 10/29/97 - - - NO -- ND -- NO NO NO NO - -- NO -- - - - - - -- NO - - - - NO NO NO NO 9.4 - NO ug/L 04/30/98 - - - NO -- ND -- NO NO NO NO -- -- NO -- - - - - - -- NO - - - - NO NO NO NO NO - NO ug/L 10/14/98 - - - NO -- ND -- NO NO NO NO -- -- NO -- - - - - - - NO - - - -- NO NO NO NO NO - NO ug/L 04/27/99 - - - NO -- NO -- NO NO NO NO -- -- ND -- - - - - - - NO - - -- -- NO NO NO NO ND - NO ug/L 10/21/99 - - - NO -- NO -- NO NO NO NO -- -- ND -- - - - - - - NO - - -- -- NO NO NO NO NO - NO ug/L 03/14/00 - - - NO -- NO -- NO NO NO NO -- -- ND -- - - - - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 04/19/00 - - - NO -- NO -- NO NO NO NO -- -- ND - - - - - - - NO - - - -- NO NO NO NO NO - NO ug/L 10/17/00 - - - NO -- NO -- NO NO NO NO -- -- NO - - - - - - - NO - - - -- NO NO NO NO NO - NO ug/L 04/10/01 - - - NO -- NO -- NO NO NO NO -- -- NO - - - - - - - NO - - - -- NO NO NO NO NO - NO ug/L 10/11/0, - - - NO -- NO -- NO NO NO NO -- -- NO - - - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/18/02 - - - NO -- NO -- NO NO NO NO -- -- NO -- - - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/08/02 - - - NO -- ND -- NO NO NO NO -- -- ND -- - - - - - -- ND - - - -- NO NO NO NO NO - NO ug/L 04/09/03 - - - NO -- ND -- NO NO NO NO -- -- ND -- - - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/13/03 - - - NO -- ND -- -- -- NO ND -- -- ND NO NO - - - - - NO - - - -- NO ND NO ND NO - NO ug/L 04/26/04 - - - NO -- ND -- -- -- NO ND -- -- ND NO NO - - - - - NO - - - -- NO ND NO ND NO - NO ug/L 10/25/04 - - - NO -- ND -- -- -- NO NO -- -- NO NO - - - - - - NO - - - -- NO NO NO NO NO - NO u9/L 04/04/05 - - - NO -- ND -- -- -- NO NO -- -- NO NO NO - - - - - NO - - - -- NO NO NO NO NO - NO ug/L 10/04/05 - - - NO NO ND -- NO NO NO NO -- -- NO NO NO - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/28/06 - - - NO -- ND -- -- -- NO NO -- -- NO NO NO - - - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/09/06 - - - NO -- ND -- -- -- NO NO -- -- NO NO NO -- -- - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 04/24/07 - - - ND -- ND -- -- -- NO ND -- -- ND NO NO -- -- - - NO ND - ND ND ND NO ND NO ND NO - NO ug/L 10/30/07 - - 1 ND -- ND -- -- -- NO ND -- -- ND NO ND -- -- - - NO ND - NO ND ND NO ND NO ND NO - NO ug/L 04/23/08 - - 1 ND -- ND -- -- -- NO ND -- -- ND NO ND -- -- - - NO ND - NO ND ND NO ND NO ND NO - NO ug/L 10/06/08 - - 1 NO -- ND -- -- -- NO NO -- -- ND NO NO -- -- - - NO ND - ND ND ND NO NO NO NO NO - NO ug/L 04/13/09 - - 1 NO -- ND -- -- -- NO NO -- -- NO NO NO -- - - - NO NO - ND NO NO NO NO NO NO NO - NO ug/L 10/15/09 - - 1 NO -- ND -- -- -- NO NO -- -- NO NO NO -- - - - NO NO - ND NO NO NO NO NO NO NO - NO u9/L 04/26/10 - - 1 NO -- ND -- -- -- NO NO -- -- NO NO NO -- - - - NO NO - ND NO NO NO NO NO NO NO - NO ug/L 10/19/10 - - 1 NO -- ND -- -- -- NO NO -- -- NO NO NO -- - - - NO NO - ND NO NO NO NO NO NO NO - NO ug/L 04/18/11 - - 1 NO -- ND -- -- -- NO NO -- -- ND NO NO -- - - - NO ND - ND ND ND NO NO NO NO ND - NO ug/L 10/10/11 - - 1 NO -- ND -- -- -- NO NO -- -- ND NO NO -- -- - - NO ND - ND ND ND NO -- NO NO Dry - NO ug/L 04/17/12 - - 1 NO -- ND -- -- -- NO NO -- -- ND NO NO -- -- - - NO ND - ND ND ND NO NO NO NO Dry - NO ug/L 10/09/12 - - 1 NO -- ND -- -- -- NO NO -- -- ND NO NO -- -- - - NO ND - ND ND ND NO NO NO NO Dry - NO ug/L 04/15/13 - - 1 NO -- ND -- -- -- NO NO -- -- NO NO NO -- -- - - NO NO - ND NO NO NO NO NO NO Dry - NO ug/L 09/30/13 - - 1 NO -- ND -- -- -- NO NO -- -- NO NO NO -- -- - - NO NO - ND NO NO NO NO NO NO Dry - NO ug/L 04/16/14 - - 1 NO -- ND -- -- -- NO NO -- -- NO NO NO -- -- - - NO NO - ND NO NO NO NO NO NO Dry - NO ug/L 10/15/14 0.13 - 1 Dry -- ND -- -- -- NO NO -- -- NO NO NO -- -- - - NO NO - ND NO NO NO NO NO NO Dry - NO ug/L 04/15/15 0.13 - 1 NO -- ND -- -- -- NO NO -- -- NO NO NO -- -- - - NO ND - ND ND ND ND ND ND ND Dry - NO ug/L 10/07/15 0.13 - 1 NO -- ND -- -- -- NO NO -- -- 0.62 J NO NO -- -- - - NO NO - ND ND ND 0.66 J NO NO NO NO - NO ug/L 04/11/16 0.13 - 1 NO -- ND -- -- -- NO ND -- -- NO NO ND -- -- - - NO ND - ND ND ND NO ND NO ND NO - NO ug/L 11/30/16 0.13 - 1 NO -- NO -- -- -- NO ND -- -- 0.48 J NO ND -- -- - - NO ND -- ND ND ND NO ND NO ND NO - NO ug/L 04/11/17 0.13 - 1 NO -- NO -- -- -- NO NO -- -- NO NO NO -- -- - - NO NO -- ND NO NO NO NO NO NO - - NO ug/L 12/12/17 0.13 - 1 NO -- NO -- -- -- NO NO - -- 0.48 J NO NO - - - - NO NO -- NO NO NO NO NO NO NO NO - NO ug/L O6/20/18 0.13 - 1 NO -- -- NO -- -- NO NO - -- 0.41 J NO NO - - - - NO -- NO NO NO NO NO NO NO NO - NO - ug/L 11/27/18 0.13 1 - NO -- -- NO -- -- NO NO - -- 0.46 J NO NO - - - - NO -- NO NO NO NO NO NO NO NO - NO NO u9/L 04/02/19 0.13 1 - NO -- -- NO - -- NO NO - -- NO NO NO - - - - NO -- NO NO NO NO NO NO NO NO - NO NO ug/L 11/19/19 0.13 1 - NO -- -- NO - -- NO ND - -- 0.58 J -- - NO NO - - NO -- NO NO ND ND NO ND NO ND - NO ND ug/L 04/07/20 0.13 1 - NO -- -- NO - -- NO NO - -- NO -- - NO NO NO - NO -- NO - - -- NO ND NO ND - NO - ug/L 10/13/20 0.13 1 - ND -- -- NO - -- -- - ND NO 0.67 J -- - NO NO NO NO NO -- NO NO NO ND NO ND NO ND - NO - z�sna.eesMeow�E�vw,awns�zoswasasuw.0 Mwrecwmv xomreLrcawo ram�m.��e,.esxo,. -uaw-12-2osnw-­- -Ewmzos l-o.a.en.. Psge 11 a17 TABLE 5 Summary of Historical Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SBME Project No. 4358-20-043A Detected Monitoring Active C&D Monitoring Wells Active C Perfo&rnnarc D Monitoring Wells & NINA Wells Closed MSW Monitoring Wells & NINA Performance Monitoring Wells Offsite Constituent/Parameter Chloromethare Unit. u9/L a, 03/05/90 St. JEEIBac.kgroi-d, -- - -- onit ring We] MIV -- -- r -- r- - -- r -- -- r - -- -- r- - -- -- .r -- -- -- -- -- for th -- or a o:M nitoring Cl ad MSW -- Landfill - - -- -- -- -- -- -- - -- Pr ivate Well ND NC 2L = 3 u9/L u9/L 03/21/91 _ _ _ _ __ _ _ __ __ __ __ __ __ _ _ _ _ _ _ _ _ __ _ _ __ __ __ __ __ __ _ _ ND u9/L 03/10/92 _ _ _ _ __ _ _ __ __ __ __ __ __ _ _ _ _ _ _ _ _ __ _ _ _ __ __ __ __ __ _ _ ND u9/L 04/20/95 _ _ _ __ __ _ _ __ __ __ __ __ __ _ _ _ __ _ _ _ _ __ _ _ __ __ __ __ __ __ _ _ NO ug/L O6/27/95 - - - -- NO - - -- -- -- -- -- -- - - - - - - - - -- - - -- -- NO NO NO NO - - NO ug/L 09/22/95 - - - NO -- -- -- -- -- -- -- -- -- -- -- -- - - - - NO -- - NO NO NO NO NO NO NO - - NO ug/L 03/28/96 - - - NO -- -- -- -- -- -- -- -- -- -- -- -- - - - - - -- - NO NO -- NO NO NO NO - - NO ug/L 10/29/96 - - - NO -- -- -- -- -- -- -- -- -- -- -- -- - - - - -- -- - - -- -- NO NO NO NO -- - NO ug/L 04/08/97 _ _ _ NO __ __ __ _ _ _ _ __ __ _ _ _ _ _ _ _ _ _ _ _ _ _ NO ND NO ND -- - NO ug/L 10/29/97 - - - ND -- ND -- NO ND NO ND -- -- ND - -- - - - - -- ND - - - -- NO ND 26 ND NO - NO ug/L 04/30/98 - - - ND -- ND -- NO ND NO ND -- -- 40 - -- - - - - -- ND - - - -- NO ND NO ND NO - NO ug/L 10/14/98 - - - NO -- NO -- NO ND NO ND -- -- 32 -- -- - - - - - ND - - - -- NO ND NO ND NO - NO ug/L 04/27/99 - - - NO -- NO -- NO ND NO ND -- -- ND -- -- - - - - - ND - - - -- NO ND NO ND NO - NO ug/L 10/21/99 - - - NO -- NO -- NO ND NO ND -- -- ND -- - - - - - - ND - - -- -- NO ND NO ND NO - NO ug/L 03/14/00 - - - NO -- NO -- NO ND NO ND -- -- ND -- - - - - - NO ND - NO NO ND NO ND NO ND NO - NO ug/L 04/19/00 - - - NO -- NO -- NO ND NO ND -- -- ND -- - - - - - - ND - - - -- NO ND NO ND NO - NO ug/L 10/17/00 - - - ND -- NO -- NO ND NO ND -- -- ND -- - - - - - -- ND - - - -- NO ND NO ND NO - NO ug/L 04/10/01 - - - NO -- NO -- NO ND NO ND -- -- ND -- - - - - - -- ND - - - -- NO ND NO ND NO - NO ug/L 10/11/01 - - - NO -- NO -- NO ND NO ND -- -- ND -- - - - - - -- ND - - -- -- NO ND NO ND NO - NO ug/L 04/18/02 - - - NO -- NO -- NO ND NO ND -- -- ND -- - - - - - -- ND - - -- -- NO ND NO ND NO - NO ug/L 10/08/02 - - - NO -- NO -- NO ND NO ND -- -- ND -- - - - - - -- ND - - -- -- NO ND NO ND NO - NO ug/L 04/09/03 - - - ND -- NO -- NO ND NO ND -- -- ND - - - - - - -- ND - - -- -- NO ND NO ND NO - NO ug/L 10/13/03 - - - NO -- NO -- NO ND NO ND -- -- ND NO NO - - - - -- ND - - -- -- NO ND NO ND NO - NO ug/L 04/26/04 - - - NO -- NO -- NO ND NO ND -- -- ND NO NO - - - - -- ND - - -- -- NO ND NO ND NO - NO ug/L 10/25/04 - - - NO -- NO -- NO ND NO ND -- -- ND NO -- - - - - -- ND - - -- -- NO ND NO ND NO - NO ug/L 04/04/05 - - - NO -- NO -- NO ND NO ND -- -- ND NO ND -- -- - - -- ND - - -- -- NO ND NO ND NO - NO ug/L 10/'4/05 - - - ND NO ND -- NO ND NO ND -- -- ND NO ND -- -- - - -- ND - - -- -- NO ND NO ND NO - NO ug/L 04/28/06 - - - ND -- ND -- - -- NO ND -- -- ND NO ND -- -- - - NO ND - NO NO ND NO ND NO ND NO - NO ug/L 10/09/06 - - - NO -- ND -- - -- NO ND -- -- ND NO ND -- -- - - NO ND - NO NO ND NO ND NO ND NO - NO ug/L 04/24/07 - - - NO -- ND -- - -- NO ND -- -- ND NO ND -- -- - - NO ND - NO NO ND NO ND NO ND NO - NO ug/L 10/30/07 - - 1 NO -- ND -- - -- NO ND -- -- ND NO ND -- -- - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L .23/08 - - 1 NO -- ND -- - -- NO ND -- -- ND NO ND -- -- - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L 10/06/08 - - 1 ND -- ND -- - -- NO ND -- -- ND NO ND -- -- - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L 04/13/09 - - 1 NO -- ND -- - -- NO ND - -- ND NO ND -- -- - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L 10/15/09 - - 1 NO -- ND -- - -- NO ND - -- ND NO ND -- -- - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L 04/26/10 - - 1 NO -- ND -- - -- NO ND - -- ND NO ND -- -- - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L 10/19/10 - - 1 NO -- ND -- -- -- NO ND - -- ND NO ND -- -- - - NO NO - ND NO 0.67 J NO ND NO ND NO - NO ug/L 04/1 8/1 1 - - 1 NO -- ND -- - -- NO ND - -- ND NO ND -- -- - - NO NO - ND NO ND NO ND NO ND NO - NO ug/L 10/10/11 - - 1 ND -- ND -- - -- NO ND - -- ND NO ND -- -- - - NO NO - ND NO ND NO -- NO ND Dry - NO ug/L 04/17/12 - - 1 ND -- ND -- - -- NO NO - -- ND NO ND -- - - - NO NO - ND NO ND NO ND NO ND Dry - NO ug/L 10/09/12 - - 1 NO -- NO -- - -- NO NO - -- ND NO ND -- - - - NO NO - ND NO ND NO ND NO ND Dry - NO ug/L 04/15/13 - - 1 NO -- NO -- - -- NO NO - -- ND NO ND -- - - - NO ND - ND NO ND NO ND NO ND Dry - NO ug/L 09/30/13 - - 1 NO -- NO -- - -- NO ND - -- ND NO ND -- - - - NO ND - ND NO ND NO ND NO ND Dry - NO ug/L 04/16/14 - - 1 NO -- NO -- - -- NO ND - -- ND NO ND -- - - - NO ND - ND NO ND NO ND NO ND Dry - NO ug/L 10/15/14 0.13 - 1 Dry -- NO -- - -- NO ND - -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND Dry - NO ug/L 04/15/15 0.13 - 1 NO -- NO -- - -- NO NO - -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND Dry - NO ug/L 10/07/15 0.13 - 1 NO -- NO -- - -- NO NO - -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L 04/11/i6 0.13 - 1 NO -- NO -- - -- NO NO - -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L 11/30/16 0.13 - 1 ND -- NO -- - -- NO NO - -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L 04/11/17 0.13 - 1 ND -- NO -- - -- NO ND - -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L 12/12/17 0.13 - 1 NO -- NO -- - -- NO ND - -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L O6/20/18 0.13 - 1 NO -- -- ND - -- NO ND - -- ND NO ND - - - - NO -- NO ND NO ND NO ND NO ND -- NO - ug/L 11/27/18 0.13 1 - NO -- -- ND -- -- NO ND - -- ND NO ND - - - - NO -- NO NO NO ND NO ND NO ND -- NO NO ug/L 04/02/19 0.13 1 - NO -- -- NO - -- NO NO - -- ND NO ND - - - - NO -- NO NO NO ND NO ND NO ND -- NO NO ug/L 11/19/19 0.13 1 - NO -- -- NO - -- NO NO - -- ND -- -- NO NO - - NO -- NO NO NO ND NO ND NO ND -- NO NO ug/L 04/07/20 0.13 1 - NO -- -- NO - -- NO NO - -- ND -- -- NO NO NO - NO -- NO - -- -- NO ND NO ND - NO - u /L 10/13/20 0.13 1 - NO -- -- NO - -- -- -- NO ND ND -- -- NO NO NO NO NO -- NO NO NO ND ND NO ND - NO - Methylene chloride ug/L 03/05/90 -- -- - - -- -- -- - -- -- -- - -- -- -- -- - - - - -- -- -- - -- -- -- -- -- -- - - NO NC 2L = 5 ug/L ug/L 03/21/91 _ _ _ _ __ __ __ _ _ _ _ _ __ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ NO EPA MCL = 5 ug/L ug/L 03/10/92 - - - - -- -- -- - -- -- -- - -- -- -- -- - - - - - -- - - -- -- -- - - - - - NO ug/L 04/20/95 _ _ _ _ __ __ __ _ _ _ _ _ __ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ NO ug/L O6/27/95 - - - - NO -- -- - -- -- -- - -- -- -- -- - - - - - - - - - - NO NO NO NO - - NO ug/L 09/22/95 - - - NO -- -- -- - -- -- - - -- -- -- -- - - - - NO - - NO NO NO 40 NO NO NO - - NO ug/L 03/28/96 - - - ND -- -- -- - -- - - - -- - - - - - - - - - - NO NO - 15 NO NO NO - - NO ug/L 10/29/96 - - - NO -- 12 -- NO 12 NO NO - -- ND -- -- -- - - - - NO - - - - NO ND NO ND NO - NO ug/L 04/08/97 - - - NO -- 13 -- NO ND NO NO - -- ND -- -- -- - - - - NO - - - -- NO ND NO ND NO - NO ug/L 10/29/97 - - - NO -- 15 -- NO ND NO NO -- -- ND -- -- -- - - - -- NO - - - -- NO ND NO ND NO - NO ug/L 04/30/98 - - - NO -- NO -- NO ND NO ND -- -- ND -- -- -- - - - -- ND - - - -- NO ND NO ND NO - NO ug/L 10/14/98 - - - ND -- NO -- NO ND NO ND -- -- ND -- -- -- - - - -- ND - - - -- NO ND NO ND NO - NO ug/L 04/27/99 - - - ND -- NO -- NO ND NO ND -- -- ND -- -- -- - - - - ND - - - -- NO ND NO ND NO - NO ug/L 10/21/99 - - - NO -- NO -- NO ND NO ND -- -- ND -- -- -- - - - - ND - - - -- NO ND NO ND NO - NO ug/L 03/14/00 - - - NO -- 3 -- NO ND NO ND -- -- ND -- -- -- -- - - NO ND - NO NO ND NO ND NO ND NO - NO ug/L 04/19/00 - - - NO -- NO -- NO ND NO ND -- -- ND -- -- -- - - - - ND - - -- -- NO ND NO ND NO - NO ug/L 10/17/00 - - - NO -- NO -- NO ND NO ND -- -- ND -- -- -- - - - - ND - - -- -- NO ND NO ND NO - NO ug/L 04/10/01 - - - ND -- NO -- NO ND NO ND -- -- ND -- -- -- - - - -- ND - - -- -- NO ND NO ND NO - NO ug/L 10/11/01 - - - NO -- NO -- NO ND NO ND -- -- ND -- -- -- - - - -- ND - - -- -- NO ND NO ND NO - NO ug/L 04/18/02 - - - NO -- NO -- NO ND NO ND -- -- ND -- -- -- - - - -- ND - - -- -- NO ND NO ND NO - NO ug/L 10/08/02 - - - NO -- NO -- NO ND NO ND -- -- ND -- -- -- - - - -- ND - - -- -- NO ND NO ND NO - NO ug/L .09/03 - - - NO -- NO -- NO ND NO ND -- -- ND -- -- -- - - - -- ND - - -- -- NO ND NO ND NO - NO ug/L 10/13/03 - - - NO -- NO -- -- -- NO ND -- -- ND NO ND -- - - - -- ND - - -- -- NO ND NO ND NO - NO ug/L 04/26/04 - - - ND -- NO -- -- -- NO ND -- -- ND NO ND -- - - - -- ND - - -- -- NO ND NO ND NO - NO ug/L 10/25/04 - - - NO -- NO -- -- -- NO ND -- -- ND NO -- - - - - -- ND - - -- -- NO ND NO ND NO - NO ug/L .04/05 - - - NO -- NO -- -- -- NO ND -- -- ND NO ND - - - - -- ND - - -- -- NO ND NO ND NO - NO ug/L 10/04/05 - - - NO NO NO -- NO ND NO ND -- -- ND NO ND - - - - -- ND - - -- -- NO ND NO ND NO - NO ug/L 04/28/06 - - - NO -- NO -- -- -- NO ND -- -- ND NO ND - - - - NO ND - NO NO ND NO ND NO ND NO - NO ug/L 10/09/06 - - - ND -- NO -- -- -- NO ND -- -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L .24/07 - - - ND -- NO -- - -- NO ND -- -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L 10/30/07 - - 1 NO -- NO -- - -- NO ND -- -- ND NO ND - - - - NO NO - ND NO ND NO ND NO ND NO - NO ug/L 04/23/08 - - 1 NO -- 0.60 B -- - -- NO ND -- -- ND NO ND - - - - NO NO - ND NO ND NO ND NO ND NO - NO ug/L 10/06/08 - - 1 NO -- NO -- - -- NO ND -- -- ND NO ND - - - - NO NO - ND NO ND NO ND NO ND NO - NO ug/L 04/13/09 - - 1 NO -- NO -- - -- NO ND -- -- ND NO ND - - - - NO NO - ND ND ND NO ND NO ND NO - NO ug/L 10/15/09 - - 1 ND -- NO -- - -- NO ND -- -- ND NO ND - - - - NO ND - ND ND ND NO ND NO ND NO - NO ug/L 04/26/10 - - 1 NO -- NO -- - -- NO ND -- -- ND NO ND - - - - NO ND - ND ND ND NO ND NO ND NO - NO ug/L 10/19/10 - - 1 NO -- NO -- -- -- NO ND -- -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L 04/18/11 - - 1 NO -- 0.42 J -- - -- NO ND -- -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L 10/1 0/1 1 - - 1 NO -- 0.40 J -- - -- NO ND -- -- ND NO ND - - - - NO ND - ND NO ND NO -- NO ND Dry - NO ug/L 04/17/12 - - 1 ND -- 0.52 J -- - -- NO ND -- -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND Dry - NO ug/L 10/09/12 - - 1 NO -- 0.50 J -- - -- NO ND -- -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND Dry - NO ug/L 04/15/13 - - 1 NO -- 0.92 J -- - -- NO ND -- -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND Dry - NO ug/L 09/30/13 - - 1 NO -- NO -- - -- NO ND -- -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND Dry - NO ug/L 04/16/14 - - 1 NO -- NO -- - -- NO ND -- -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND Dry - NO ug/L 10/15/14 0.23 - 1 Dry -- NO -- - -- NO ND -- -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND Dry - NO ug/L 04/15/15 0.23 - 1 ND -- NO -- - -- NO ND -- -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND Dry - NO ug/L 10/07/15 0.23 - 1 NO -- NO -- - -- NO ND -- -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L 04/11/i6 0.23 - 1 NO -- NO -- - -- NO ND -- -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L 11/30/16 0.23 - 1 NO -- NO -- - -- NO ND -- -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L 04/11/7 0.23 - 1 NO -- NO -- - -- NO ND - -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L 12/12/17 0.23 - 1 ND -- NO -- - -- NO ND - -- ND NO ND - - - - NO ND - ND NO ND NO ND NO ND NO - NO ug/L O6/20/18 0.23 - 1 ND -- -- ND - -- NO ND - -- ND NO ND - - - - NO -- NO ND NO ND NO NO NO ND - NO - ug/L 11/27/18 0.23 1 - ND -- -- ND - -- NO ND - -- ND NO ND - - - - NO -- NO ND NO ND NO NO NO ND - NO NO ug/L .02/19 0.23 1 - NO -- -- ND - -- NO NO - -- ND NO ND - - - - NO -- NO ND NO NO NO NO NO NO - NO NO ug/L 11/19/19 0.23 1 - NO -- -- ND - -- NO NO - -- ND - -- NO NO - - NO -- NO NO NO NO NO 0.64 J NO NO - NO NO ug/L 04/07/20 0.23 1 - NO -- -- ND - -- NO NO - -- NO - -- NO NO NO - NO -- NO - - - NO NO NO NO - NO - u /L 04/07/20 0.23 1 - NO -- -- ND - -- -- - NO ND NO - -- NO NO NO NO NO -- NO NO NO NO NO NO NO NO - NO - zssnareesMeoia�Euvw,owcar�zozwase-zuw.0 Mwncwm .-Lrcawa ram-­--uaw-rrzozo-z-wu­-- Ewmzo 1-oms.eu.. Page 12 of 17 TABLE 5 Summary of Historical Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SBME Project No. 4358-20-043A Detected Monitor! Constituent/ rameter 2-Bulanone nitl%§L ug/L 10/30i07 JEEkcI.rno..nd -- -- 100 i,.ri we] r ND r- - -- r -- ND Active C&D Monitoring r - ND -- Wells r- - ND ND .D ND r -- -- -- -- Active C&D Performanc for t he ND Monitoring or o:M nitoringWells Cl edMSWLandfill ND Wells & NINA - ND ND Closed MSW ND Monitoring Wells ND & NINA Performance ND ND Monitoring Wells ND ND -- Offsite Private Well ND NC 2L=4000 ug/L ug/L 04/23/08 - - 100 ND -- ND -- -- -- NO NO -- -- ND ND NO -- -- - - NO NO - NO NO ND NO 4.8 J 2.8 J ND NO - NO ug/L 10/06/08 - - 100 ND -- NO -- -- -- NO NO -- -- ND NO NO -- - - - NO 33 J - NO ND ND 17 J 14 J ND NO NO - NO ug/L 04/13/09 - - 100 ND -- ND -- -- -- NO NO -- -- ND NO NO -- - - - NO NO - NO ND ND NO NO ND NO NO - NO ug/L 10/15/09 - - 100 ND -- ND -- -- -- NO NO -- -- ND NO NO -- - - - NO NO - NO ND ND NO NO ND NO NO - NO ug/L 04/26/10 - - 100 NO -- ND -- -- -- NO NO -- -- NO NO NO -- - - - NO NO - ND NO NO NO NO NO 6.8 J NO - NO ug/L 10/19/10 - - 100 NO -- ND -- -- -- NO NO -- -- NO NO NO -- - - - NO NO - ND NO NO 3.8 J NO NO NO NO - NO ug/L 04/18/11 - - 100 NO -- ND -- -- -- NO NO -- -- NO NO NO -- -- - - NO NO - ND NO NO NO NO NO NO NO - NO ug/L 10/10/11 - - 100 NO -- ND -- -- -- NO NO -- -- NO NO NO -- -- - - NO NO - ND NO NO NO - NO NO Dry - NO ug/L 04/17/12 - - 100 NO -- ND -- -- -- NO NO -- -- NO NO NO -- -- - - NO NO - ND NO NO NO NO NO NO Dry - NO ug/L 10/09/12 - - 100 NO -- ND -- -- -- NO ND -- -- ND NO NO -- -- - - NO NO - ND ND ND NO NO NO NO Dry - NO ug/L 04/15/13 - - 100 NO -- ND -- -- -- NO ND -- -- ND NO ND -- -- - - NO NO - ND ND ND NO NO NO NO Dry - NO ug/L 09/30/13 - - 100 NO -- ND -- -- -- NO ND -- -- ND NO ND -- -- - - NO NO - ND ND ND 2.6 J NO NO NO Dry - NO ug/L 04/16/14 - - 100 NO -- ND -- -- -- NO ND -- -- ND NO ND -- -- - - NO NO - ND ND ND 2.4 J 1.3 J NO 13 J Dry - NO ug/L 10/15/14 1.3 - 100 Dry -- ND -- - -- NO NO -- -- NO NO NO -- - - - NO NO - ND NO NO NO NO NO NO Dry - NO ug/L 04/15/15 1.3 - 100 NO -- ND -- - -- NO NO -- -- NO NO NO -- - - - NO NO - ND NO NO NO NO NO NO Dry - NO ug/L 10/07/15 1.3 - 100 NO -- ND -- - -- NO NO -- -- NO NO NO -- - - - NO NO - ND NO NO NO NO NO NO NO - NO ug/L 04/1 1/1 6 1.3 - 100 NO -- ND -- - -- NO NO -- -- NO NO NO -- - - - NO NO - ND NO NO 28 J 7.0 J NO 4.2 J NO - NO ug/L 11/30/16 1.3 - 100 NO -- ND -- - -- NO ND -- -- ND NO ND -- - - - NO NO -- ND ND ND 1.4 J NO NO NO 6.4 J - NO ug/L 04/11/17 1.3 - 100 ND -- NO -- - -- NO ND -- -- ND NO ND - - - - NO NO -- ND ND ND NO NO NO ND 24 J - NO ug/L 12/12/17 1.3 - 100 ND -- NO -- - -- NO ND -- -- ND NO ND - - - - NO NO -- ND ND ND NO ND NO ND NO - NO ug/L O6/20/18 1.3 - 100 ND -- -- NO - -- NO ND -- -- ND NO ND - - - - NO - NO ND ND ND NO NO NO ND - NO - ug/L 11/27/18 1.3 5 - NO -- -- NO - -- NO NO -- -- NO NO NO - - - - NO - NO NO NO NO NO NO NO NO - NO NO ug/L 04/02/19 1.3 5 - NO -- -- NO - -- NO NO - -- NO NO NO - - - - NO -- NO NO NO NO NO 21 NO NO - NO NO ug/L 11/19/19 1.3 5 - NO -- -- NO -- -- NO NO - -- NO -- -- NO NO - - NO -- NO NO NO NO NO NO NO NO -- 5.7 NO ug/L 04/07/20 1.3 5 - NO -- -- NO -- -- NO NO - -- NO - -- NO NO NO - NO -- NO - - - NO NO NO NO - NO - ug/L 10/13/20 1.3 5 - NO -- -- NO -- -- -- -- NO NO NO - -- ND ND ND NO NO - NO ND NO NO NO NO NO NO - NO - Naphthalene u9/L 03/05/90 __ __ _ _ __ __ __ __ __ __ __ _ __ _ _ __ _ _ _ _ __ _ _ _ __ _ _ _ _ _ _ _ NO NC 2L=6 ug/L ug/L 03/21/91 ND ug/L 03/10/92 _ _ _ _ __ __ __ __ __ __ __ _ __ _ _ __ _ _ _ _ _ _ _ _ __ __ _ _ _ _ __ _ NO ug/L 04/20/95 NO ug/L O6/27/95 - - - - NO NO -- NO NO NO NO - -- NO -- -- - - - - - NO - - - -- NO NO NO 2.5 NO - NO ug/L 09/22/95 - - - NO -- NO -- NO NO NO NO - -- NO -- -- - - - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 03/28/96 - - - NO -- NO -- NO NO NO NO - -- NO -- -- - - - - -- NO - NO NO -- NO NO NO NO NO - NO ug/L 10/29/96 - - - NO -- NO -- NO NO NO NO - -- NO -- -- - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/08/97 - - - ND -- NO -- NO NO NO NO -- -- ND -- -- -- - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 1.29/97 - - - ND -- NO -- NO NO NO NO -- -- ND -- -- -- - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/30/98 - - - ND -- NO -- NO NO NO NO -- -- ND -- -- -- - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/14/98 - - - NO -- NO -- NO NO NO NO -- -- ND -- -- -- - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/27/99 - - - NO -- NO -- NO NO NO NO -- -- NO -- -- -- - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/21/99 - - - NO -- NO -- NO NO NO NO -- -- NO -- -- -- - - - -- NO - - -- -- NO NO NO NO NO - NO ug/L 03/14/00 - - - NO -- NO -- NO NO NO NO -- -- NO -- -- -- - - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L .1.0 - - - NO -- ND -- NO NO NO NO -- -- NO -- -- -- - - - -- NO - - -- -- NO NO NO NO NO - NO ug/L 10/17/00 - - - NO -- ND -- NO NO NO NO -- -- ND -- -- -- -- - - -- NO - - -- -- NO NO NO NO NO - NO ug/L .1.1 - - - NO -- ND -- NO NO NO NO -- -- ND -- -- -- -- - - -- NO - - -- -- NO NO NO NO NO - NO ug/L 10/11/01 - - - NO -- ND -- NO NO NO NO -- -- ND -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/18/02 - - - NO -- ND -- NO NO NO NO -- -- ND -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/08/02 - - - NO -- ND -- NO NO NO NO -- -- NO -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/09/03 - - - NO -- ND -- NO NO NO NO -- -- NO -- -- -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/13/03 - - - NO -- ND -- - - NO NO -- -- NO NO NO -- -- - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/26/04 - - - NO -- ND -- - - NO NO -- -- NO NO NO -- - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/25/04 - - - NO -- ND -- - - NO NO -- -- ND NO -- -- - - - -- NO - - - -- NO NO NO NO NO - NO ug/L .04/05 - - - NO -- ND -- - - NO NO -- -- ND NO NO -- - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/04/05 - - - NO NO ND -- NO NO NO NO -- -- NO NO NO -- - - - -- NO -- - - -- NO NO NO NO NO - NO ug/L 04/28/06 ug/L 10/09/06 ug/L .24/07 ug/L O6/20/18 0.11 - 10 NO -- -- NO - -- NO NO - -- 0.65 J NO NO -- - - - NO -- 0 58 J - - - NO NO - - - ug/L 11/27/18 0.11 1 - NO __ __ __ _ __ __ __ _ __ NO __ __ __ _ _ _ _ __ ND ug/L 04/02/19 0.11 1 - NO __ __ __ _ __ __ __ _ __ 0.40 J __ __ __ _ _ _ _ __ ND _ _ _ ug/L 11/19/19 0.11 1 - NO __ __ __ _ __ __ __ _ __ NO __ __ __ _ _ _ _ __ ND ug/L 04/07/20 0.11 1 - NO __ __ __ _ __ _ _ _ __ 0.42 J __ __ __ _ _ _ _ __ ND _ _ _ ug/L 10/13/20 0.11 1 - NO -- -- NO - -- - - ND NO 0.49 J - -- -- - - NO - -- NO NO - NO -- -- -- -- - - - zssnareesMeoia�Euvw,owcarwozwase-zuw.0 Mwncwmy aamreLrcawa ram�m.��a+T�so+--uaw-rrzozo-z-wu­- ra.Ewmzoz l-Ms.eu.. Page 13 of 17 TABLE 5 Summary of Historical Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina S&ME Project No. 4358-20-043A Detected Monitor! Active C&D Monitoring Wells Active Performanc: C&D Monitoring Wells M nitoring & NINA Wells Closed MSW Monitoring Wells & NINA Performance Monitoring Wells Offsite Constituent/ rameter Tetrachloroethe Is nitl%§L ug L 030 JEEIBackgro.nd,. onitoring We] Mw J111111111111'�� MW-12D MW-1 3S MW-13D MW-13SR MW-13DR MW-I6S MW-16D Mw-1 MW-17D Mw-18 MW-19 for MW-4 the Clo ed`MSW Landfill MW-11S MW-11SR MW-1 MW-2 MW-3 MW-6 MW-7 MW-8 MW-9 MW-15 MW-15R Private Well PW-1 NC 2L = 0.7 ug/L ug L 01251//990 NO EPA MCL = 5 ug/L ug/L 03/10/92 NO ug/L 04/20/95 NO ug/L 06/27/95 NO 8.4 3.2 NO NO - NO ug/L 09/22/95 NO NO ND NO NO NO NO NO ND NO ug/L 03/28/96 NO NO NO 12 NO NO NO - NO ug/L 10/29/96 NO 8 NO 7 NO NO ND NO NO NO NO NO 6 NO ug/L 04/08/97 NO ND NO NO NO NO NO NO NO NO NO NO 8 NO ug/L 10/299 NO NO 15 NO NO ND NO 9.2 NO NO NO 9.1 NO ug/L 3 8 . .�97 NO i5 7 NO 13 NO NO NO NO NO NO NO NO 8.2 NO ug/L 10/14/98 NO 1 2.7 NO 8.7 NO NO NO NO NO NO NO NO 5 NO ug/L 04/27/99 NO 10 NO 7.9 NO NO ND NO NO NO NO NO NO NO ug/L 10/2 1/99 NO 8.6 NO 6.5 NO NO NO NO NO NO NO NO 7.6 NO ug/L 03/14/00 NO 8 NO 6 NO NO ND NO NO ND ND NO NO NO NO NO 3 NO ug/L 04/1 9/00 NO 10 NO NO NO NO NO NO NO NO NO NO NO NO ug/L 10117/00 ND NO 6.5 NO NO ND NO NO NO NO NO NO NO ug/L 04/1 0/01 NO 65 NO NO NO NO NO NO 8.1 NO NO NO NO NO ug/L 10/11/01 NO 8.4 NO 6.3 NO NO ND NO NO NO NO NO NO NO ug/L 04/18/0 NO 73 NO 5.9 NO NO NO NO NO NO NO NO NO NO ug,L 10/08/02 NO 6 NO NO NO NO NO NO NO NO NO NO NO NO ug'L 04/09/03 NO 5.3 NO NO NO NO ND NO NO NO NO NO NO NO ugIL 1.13/03 NO NO NO NO NO 6.3 - - - - NO NO NO NO NO NO NO ug/L 04/26/04 NO 5.2 NO NO ND NO NO NO NO NO NO NO NO NO ug/L 10/25/04 NO NO NO NO NO - - - - NO NO NO NO NO NO NO ug'L 04/4/05 NO ND NO NO ND NO NO NO NO NO NO NO NO NO ugIL 1.04/05 NO NO ND NO NO NO NO - NO NO NO - - - - NO NO NO NO NO NO NO ug/L 04/28/06 ND ND NO NO NO NO NO NO NO ND NO ND NO NO NO NO NO NO ug/L 10/09/06 NO ND NO NO - NO NO NO - - - NO NO ND ND ND NO NO NO NO NO NO ug/L 04/24/07 NO 4 J NO NO NO NO 3 NO NO NO NO NO NO NO NO NO NO NO ug/L 10/30/07 1 NO 3.1 J NO 0.43 J - 052 J 0.71 J 0 .49 J - - - 0.35 J NO NO ND ND NO NO NO NO 0.38 J NO ug/L 04/23/08 1 NO 28 NO NO O�40 J 0 J NO NO NO ND NO NO NO NO NO NO NO NO u g/L 10/06/08 1 ND 20 NO NO - NO ��I , 49 NO - - - NO NO ND ND ND NO NO NO NO 0.49 J NO ug/L 04/1 3/09 1 NO 29 NO 048 J 0.44 J 0.47 J 0.84 J NO NO ND NO NO NO NO NO NO 0.49 J NO ug/L 10/15/09 1 NO 2.7 NO OA4 J - NO 0.53 J NO NO NO ND ND ND NO NO NO NO 0.50 J NO ug/L 04126/10 1 NO 2.9 NO 0.52 J NO NO 046 J NO NO ND NO NO NO NO NO NO 0.47 J NO ug/L 10119/1 0 1 NO 2.7 NO NO - NO NO OA1 J NO NO ND NO NO NO NO NO NO 0.52 J NO u /L 04/18/11 1 NO NO NO - NO NO NO NO NO ND ND ND NO NO NO NO NO NO ug, L 10110/I1 1 NO 8 NO NO NO NO NO NO NO ND NO NO NO NO NO Dry NO ug/L 04/17/12 1 NO 2.0 NO NO - ND NO NO NO NO ND ND ND NO NO NO NO Dry NO ug/L 10109/1 2 1 NO 25 NO NO NO NO NO NO NO ND NO NO NO NO NO NO Dry NO ug/L 04/15/13 1 NO 22 NO NO ND NO NO NO NO ND ND ND NO NO NO NO D NO ug,L 09130/1 3 1 NO 1.5 NO NO NO NO NO NO NO ND NO NO NO NO NO NO Dry Dry NO ug/L 04/16/14 1 NO 22 NO NO ND NO 0.57 J NO NO ND ND ND NO NO NO NO Dry NO ug/L 10115/14 0 .17 1 Dry 8 NO NO NO NO NO NO NO ND NO NO NO NO NO NO Dry NO uglL 04/15/15 017 1 NO 7 NO NO NO NO NO NO NO ND NO NO NO NO NO NO Dry NO ug/L 10107/1 5 0.17 1 NO 1.4 NO NO ND NO NO NO NO ND ND ND NO NO NO NO NO NO ug/L 04/11/16 017 1 NO 0,6 J NO NO NO NO NO NO NO ND NO NO NO NO NO NO NO NO ug/L 11130/1 6 0.17 1 NO 0 J NO NO ND NO NO NO ND ND ND ND NO NO NO NO NO NO ug/L 04/1 1/17 17 0:1 1 NO :4 0 7 J NO NO NO NO NO NO NO ND NO NO NO NO NO NO NO NO ug/L 12/12/17 0.17 1 NO 0.84 J NO NO ND NO NO NO ND ND ND ND NO NO NO NO NO NO ug/L 06/20/4 0:117 1 NO NO NO NO NO NO NO NO NO ND NO NO NO NO NO NO NO ug/L 11/27/ 8 0.17 1 - NO NO NO NO ND NO NO NO NO ND ND ND NO NO NO NO NO NO u /L ' 04/ 0.117 I NO NO NO NO ND N NO NO NO ND ND ND NO NO NO NO NO NO , ug L 11/02/19 19/ 9 0.17 NO NO NO NO NO _D NO NO NO NO NO NO NO NO NO NO NO NO NO U g/L 04/07/20 0.17 1 I - ND NO NO ND ND NO NO ND NO NO NO ND NO ND NO ug/L 1 10/13/20 1 0.17 1 1 NO I NO NO ND NO NO NO NO NO NO NO NO ND NO NO NO NO NO NO - Toluene ug/L 03/05/90 -- -- NO NC 2L = 600 ug/L UgIL 03/21/91 NO EPA MCL = 1000 ug/L ug/L 03/10/92 ND ug/L 04/20 55 NO ug/L 06/27�99 NO NO NO NO NO NO u'/L 09/22�95 NO NO ND NO ND NO NO NO NO NO ug,L 03/2896 NO NO NO NO NO NO NO NO ug/L 10/29/96 NO ND NO NO NO NO - NO - NO NO NO NO NO NO NO ug/L 04/08/97 NO ND NO NO NO NO NO NO NO NO NO NO NO NO u'/L 10/29/97 NO ND NO NO NO NO - NO - NO NO NO NO NO NO NO ug,L 04/30/98 NO ND NO NO NO NO NO NO NO NO NO NO 15 NO ug/L 10/14/98 NO ND NO NO NO NO ND - NO NO NO NO NO NO NO ug/L 04/27/99 NO ND NO NO NO NO NO NO NO NO NO NO NO NO ug/L 10/21/99 NO ND NO NO NO NO NO - NO NO NO NO NO NO NO ug/L 03/14/00 NO ND NO NO NO NO ND 2 NO NO NO NO NO NO NO NO NO NO ug/L 04/19/00 NO ND NO NO NO NO NO NO NO NO NO NO NO NO ug/L 10/17/00 NO ND NO NO NO NO ND -- NO NO NO NO NO NO NO ug/L 04/10/01 NO ND NO NO NO NO NO NO NO NO NO NO NO NO ug/L 10/11/0, NO ND NO NO NO NO ND - NO NO NO NO NO NO NO ug/L 04/1 8/0 NO ND NO NO NO NO NO NO NO NO NO NO NO NO ug/L 10/08/02 NO ND NO NO NO NO ND - NO NO NO NO NO NO NO u'/L 04/09/03 NO ND NO NO NO NO ND NO NO NO NO NO NO NO ug,L 10/1 3/03 NO ND NO NO NO NO NO NO NO NO NO NO NO NO ug/L 04/26/04 NO NO NO NO ND NO NO NO NO NO NO NO NO NO ug/L 10/25/04 NO NO NO NO NO NO NO NO NO NO NO NO NO u'IL 04/04/05 NO NO NO NO ND NO NO NO NO NO NO NO NO NO ug,L 10/04/05 NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO ug/L 04/28/06 NO NO NO NO ND NO NO NO NO NO ND ND NO NO NO NO NO NO .g/L 10/09/06 NO ND NO ND ND NO NO NO ND NO NO ND NO NO NO NO NO NO ug/L 04/24/07 NO NO NO NO ND NO NO NO NO NO ND ND NO NO NO NO NO NO .g/L 10/30/07 1 ND ND NO ND 0.31 J NO ND NO 0.52 J NO NO ND NO ND NO ND NO NO ug/L 04/23/08 1 NO NO NO 0.44 J NO NO NO NO NO NO NO ND NO NO NO NO NO NO .g/L 10/06/08 1 NO ND NO ND ND NO ND NO ND NO NO ND NO ND NO ND NO NO ug/L 04/1 3/09 1 NO NO NO NO 0.53 J NO NO NO 0.56 J NO NO ND NO NO NO NO NO NO .g/L 10/15/09 1 NO ND NO ND ND NO ND NO ND NO NO ND NO NO NO ND NO NO ug L 04/2 1 NO NO NO NO 0.47 J NO NO NO NO NO NO ND NO NO NO NO NO NO gI/L �O 10/169// 0 1 ND NO NO ND ND NO ND NO ND NO NO ND NO NO NO ND NO NO ug I L 04/1 8/1 1 NO NO NO NO NO NO NO NO NO NO ND ND NO NO NO NO ND NO g/L 10/10/ 1 1 NO ND NO NO ND NO NO NO ND NO NO ND NO NO NO D Dry NO u IL 04/17/12 1 NO NO NO NO 0.47 J NO NO NO NO ND ND ND NO NO NO NO Dry NO ug/ g L 10/09/ 2 1 NO ND NO NO 043 J NO NO NO ND NO NO ND NO 0.44 J NO NO Dry NO ug/L 04/1 5/13 1 NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO Dry NO ug/L 09/30/1 3 1 NO NO NO NO ND 0.46 J NO NO ND NO NO ND NO NO NO NO Dry NO ug/L 04/1 6/14 1 NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO Dry NO ug/L 10/15/14 0.14 1 Dry NO NO NO ND 0.40 J NO - NO ND NO NO ND NO NO 0.59 J NO Dry NO ug L I 04/1 15 5 014 1 NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO Dry NO ug/L 10/07//l 5 0.14 1 NO NO NO NO ND NO NO - NO ND NO NO ND NO NO 0.56 J NO NO NO ug/L 04/11/16 0.14 1 NO NO NO NO ND NO NO NO NO NO ND ND NO NO NO NO ND NO ug/L 11/30/16 0.14 1 NO NO NO ND ND NO ND NO ND NO NO ND 0.48 J ND 0.60 J ND NO NO ug/L 04/11/17 014 1 NO NO NO NO ND NO NO NO NO NO ND ND NO NO 1.0 B NO ND NO ug/L 12/1211 7 0.14 1 ND NO NO ND ND NO ND NO ND NO NO ND NO ND 0.64 J ND 0.4 J NO u IL 06/20/�8 0:114 1 NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO - NO ug/L 1 1/27/ 8 0.14 ND ND NO ND ND NO ND NO NO NO NO ND NO ND 0.48 J NO NO NO U 04/02/�9 0:1 1 NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO ug/L g/L 11/19/ 9 14 0.14 NO ND NO ND ND NO NO NO NO NO NO ND NO ND 0.48 J NO 0.43 J NO ugIL 041 720 4 1 NO NO NO NO NO NO NO NO NO NO NO NO 0.40 J NO NO U/L 13/2 J./ 0 / 0 0:1 014 1 NO ND NO ND 0.48 J NO NO NO NO NO NO NO NO ND 0.40 J ND 0.51 J 0.43 J rD -­.- LI.- ..-­ - ---­ 12-2--­- - -1-o.- Page 14 of 17 TABLE 5 Summary of Historical Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SBME Project No. 4358-20-043A Detected Monitor! Active C&D Monitoring Wells Active C D Perfo&rnnanc Monitoring M Wells & NINA Wells Closed MSW Monitoring Wells & NINA Performance Monitoring Wells Offsite "g Constituent/ rameter Trichloroethene Units ug/L 03I05/90 JEEIBackgro.nd,. -- - - onitoring We] - _JJJJJJJJJJJJP�� - r -- r- - -- r - -- r - -- -- r- - - - .• -- -- - - -- for the CIO: -- nitoring ' ed`MSW -- Landfill - - -- -- -- -- -- -- - -- Private Well ND NC 2L = 3 ug/L ug/L 03/2,191 ND EPA MCL = 5 ug/L ug/L 03/10/92 - - - - -- -- -- -- - -- -- -- -- - - - - - - - - -- - - - -- -- -- -- -- - - NO u9/L 04/20/95 _ _ _ __ __ __ __ __ _ __ __ __ __ _ _ _ _ _ _ _ _ __ _ _ _ __ __ __ __ __ _ _ NO ug/L O6/27/95 - - - -- ND -- -- -- - -- -- -- -- -- - - - - - - - -- - - - - 3.6 ND NO ND - - NO ug/L 09/22/95 - - - NO -- -- -- -- - -- -- -- -- -- - - - - - - NO -- - ND ND NO NO NO NO NO - - NO ug/L 03/28/96 - - - NO -- -- -- -- - -- -- -- -- -- -- -- -- - - - - -- - NO NO - 6.4 ND NO ND - - NO ug/L 10/29/96 - - - NO -- 7 -- NO NO NO NO -- -- NO -- -- -- - - - -- NO - - - -- NO NO NO NO 5 - NO ug/L .08/97 - - - NO -- 9 -- NO 6 NO ND -- -- ND -- -- -- - - - -- ND - - - -- NO ND NO ND NO - NO ug/L 10/29/97 - - - NO -- 6.8 -- NO 6.3 NO NO -- -- NO -- -- -- - - - -- NO - - - -- NO NO NO NO 5.9 - NO ug/L .30/98 - - - ND -- 9.8 -- NO 6.4 NO ND -- -- ND -- -- -- - - - -- ND - - - -- NO ND NO ND 5.4 - NO ug/L 10/14/98 - - - NO -- 6.4 -- NO NO NO NO -- -- NO -- -- -- - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/27/99 - - - NO -- 7.2 -- NO NO NO ND -- -- ND -- - - - - - -- ND - - - -- NO ND NO ND NO - NO ug/L 10/21/99 - - - NO -- 6.2 -- NO NO NO NO -- -- ND -- - - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 03/14/00 - - - NO -- 8 -- NO NO NO ND -- -- ND -- - - - - - NO ND - NO NO ND NO ND NO ND 3 - NO ug/L 04/19/00 - - - NO -- 7.6 -- NO NO NO NO -- -- ND -- - - - - - - NO - - - -- NO NO NO NO NO - NO ug/L 10/17/00 - - - ND -- 5.1 -- NO ND NO ND -- -- ND -- - - - - - - ND - - - -- NO ND NO ND NO - NO ug/L 04/10/01 - - - NO -- NO -- NO NO NO NO -- -- NO -- - - - - - - NO - - - -- 5.2 NO NO NO NO - NO ug/L 10/11/01 - - - NO -- 5.6 -- NO NO NO ND -- -- ND -- - - - - - - ND - - - -- NO ND NO ND NO - NO ug/L 04/18/02 - - - NO -- NO -- NO NO NO NO - -- NO -- - - - - - -- NO - - -- -- NO NO NO NO NO - NO ug/L 10/08/02 - - - NO -- ND -- NO NO NO ND - -- ND -- - - - - - - ND - - -- -- NO ND NO ND NO - NO ug/L 04/09/03 - - - NO -- NO -- NO NO NO NO - -- NO -- - - - - - - NO - - -- -- NO NO NO NO NO - NO ug/L 10/13/03 - - - ND -- NO -- -- - NO ND - -- ND NO NO - - - - - ND - - - -- NO ND NO ND NO - NO ug/L 04/26/04 - - - NO -- -- -- -- - NO NO - -- ND NO NO - - - - - NO - - - -- NO NO NO NO NO - NO ug/L 10/25/04 - - - NO -- NO -- -- - NO ND - -- ND NO - - - - - - ND - - - -- NO ND NO ND NO - NO ug/L 04/04/05 - - - NO -- NO -- -- - NO NO - -- ND NO NO - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/04/05 - - - NO ND NO -- NO NO NO ND - -- ND NO NO - - - - - ND - - - -- NO ND NO ND NO - NO ug/L 04/28/06 - - - NO -- NO -- -- - NO NO - -- NO NO NO - - - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/09/06 - - - NO -- NO -- - - NO NO - -- ND NO NO - - - - NO NO - NO NO ND NO ND NO ND NO - NO ug/L 04/24/07 - - - NO -- ND -- - - NO NO - -- NO NO NO - - - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/30/07 - - 1 NO -- 1.9 J -- - - 0.31 J NO - -- 1.5 J 0.85 J 0.48 J - - - - 0.40 J 0.36 J - NO 0.30 J ND NO ND 0.31 J ND 0.46 J - NO ug/L 04/23/08 - - 1 NO -- 2.2 -- - - NO 0.50 J - -- 1.0 0.53 J NO - - - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/06/08 - - 1 NO -- 1.5 -- - - NO NO - -- 0.76 J 0.41 J NO - - - - NO NO - NO NO ND ND ND ND ND 0.46 J - NO ug/L 04/13/09 - - 1 NO -- 1.7 -- -- -- NO NO - -- 1.0 0.51 J NO - - - - ND NO - NO ND ND NO NO NO NO 0.74 J - NO ug/L 10/15/09 - - 1 NO -- 1.6 -- -- -- NO NO -- -- 0.97 J 0.79 J NO - - - - 0.51 J NO - 0.64 J NO ND NO ND 0.44 J ND 0.50 J - NO ug/L 04/26/10 - - 1 NO -- 1.7 -- -- -- NO NO -- -- 0.85 J 0.42 J ND -- -- - - NO NO - NO ND ND NO NO ND NO 0.50 J - NO ug/L 10/19/10 - - 1 NO -- 1.6 -- -- -- NO ND -- -- 0.59 J NO ND -- -- - - NO ND - NO NO ND NO ND NO ND 0.42 J - NO ug/L 04/18/11 - - 1 NO -- 1.3 -- -- -- NO NO -- -- NO NO NO -- -- - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/10/11 - - 1 NO -- 1.2 -- -- -- NO ND -- -- 0.77 J NO ND -- -- - - NO ND - NO NO ND NO -- NO ND Dry - NO ug/L 04/17/12 - - 1 NO -- 1.6 -- -- -- ND ND - -- 0.50 J 0.61 J NO -- -- - - NO NO - NO NO NO NO NO NO NO Dry - NO ug/L 10/09/12 - - 1 NO -- 1.9 -- -- -- NO ND - -- 0.54 J 0.56 J NO - - - - NO ND - NO NO ND NO ND NO ND Dry - NO ug/L 04/15/13 - - 1 NO -- 1.9 -- -- -- NO NO - -- NO 0.58 J NO - - - - NO NO - NO NO NO NO NO NO NO Dry - NO ug/L 09/30/13 - - 1 NO -- 1.1 -- -- -- NO ND - -- NO NO NO - - - - NO ND - NO NO ND NO ND NO ND Dry - NO ug/L 04/16/14 - - 1 NO -- NO -- -- -- NO NO - -- 0.41 J NO 0.55 J - - - - NO NO - NO ND ND NO NO NO NO Dry - NO ug/L 10/15/14 0.15 - 1 Dry -- 1.3 -- -- -- NO ND - -- ND 0.40 J NO - - - - NO ND - NO NO ND NO ND NO ND Dry - NO ug/L 04/15/15 0.15 - 1 NO -- 1.5 -- -- -- NO NO - -- 0.50 J NO NO - - - - NO NO - NO ND ND NO NO NO NO Dry - NO ug/L 10/07/15 0.15 - 1 NO -- 1.1 -- -- -- NO ND - -- ND NO 0.51 J - - - - NO ND - NO NO ND NO ND NO ND 0.53 J - NO u9/L 04/11/16 0.15 - 1 NO -- 0.70 J -- -- -- NO NO - -- NO NO NO - - - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 11/30/ifi 0.15 - 1 NO -- 0.68 J -- - -- NO ND - -- ND NO NO - - - - NO ND - NO NO ND NO ND NO ND NO - NO ug/L 04/11/17 0.15 - 1 NO -- 0.85 J -- - -- NO NO - -- NO NO NO - - - - NO NO - NO 0.95 J NO NO NO NO NO NO - NO ug/L 12/12/17 0.15 - 1 ND -- 0.70 J -- - -- NO ND - -- ND NO NO - - - - NO ND - NO NO ND NO ND NO ND NO - NO u9/L O6/20/18 0.15 - 1 NO -- -- NO - -- NO NO - -- NO NO NO - - - - NO -- NO NO NO NO NO NO NO NO -- NO - ug/L 11/27/18 0.15 1 - ND -- -- NO - -- NO ND - -- ND NO NO - - - - NO -- NO NO NO ND NO ND NO ND - NO NO ug/L 04/02/19 0.15 1 - NO -- -- NO - -- NO NO - -- NO NO NO - - - - NO -- NO NO ND ND NO NO NO NO - NO NO ug/L 11/19/19 0.15 1 - NO -- -- ND - -- NO NO - -- ND -- -- NO NO - - NO - NO NO NO ND NO NO NO NO - NO NO ug/L 04/07/20 0.15 1 - NO -- -- NO - -- NO NO - -- NO -- -- ND NO NO - NO - NO - - -- NO NO NO NO - NO - u /L 10/13/20 0.15 1 - NO -- -- ND - -- -- - NO ND NO -- -- NO NO NO NO NO - NO NO NO ND NO NO NO NO - NO - Vinyl chloride ug/L 03/05/90 -- -- - - -- -- -- - -- -- - - -- -- -- -- - - - - - - - - - -- -- - -- - -- - NO NC 2L = 0.03 ug/L ug/L 03/21/91 - - - - -- -- -- -- -- -- -- - -- -- -- -- - - - - - - - - - -- -- -- -- - -- - NO EPA MCL=2 ug/L ug/L 03/10/92 _ _ _ _ __ __ __ __ __ __ __ _ __ __ __ __ _ _ _ _ _ _ _ _ _ _ __ __ __ _ __ _ NO ug/L 04/20/95 _ _ _ _ __ __ __ _ _ _ _ _ __ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ NO ug/L O6/27/95 - - - - NO -- -- -- -- -- -- - -- -- -- -- - - - - - - - - - -- 5.3 9.4 40.3 15.9 -- - NO ug/L 09/22/95 - - - ND -- -- -- -- -- -- -- - -- -- -- -- - - - - NO -- - NO NO ND NO ND 45 20 -- - NO ug/L 03/28/96 - - - NO -- -- -- -- -- -- -- - -- -- -- -- -- - - - - -- - ND 13 -- NO NO 12 NO -- - NO ug/L 10/29/96 - - - ND -- ND -- NO ND NO ND - -- ND -- -- -- - - - -- ND - - - -- NO ND NO NO NO - NO ug/L 04/08/97 - - - NO -- ND -- NO NO NO NO - -- ND -- -- -- - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/29/97 - - - NO -- ND -- NO ND NO ND - -- ND -- -- - - - - -- ND - - - -- NO ND NO ND NO - NO ug/L 04/30/98 - - - NO -- ND -- NO NO NO NO - -- NO -- -- - - - - -- NO - - - -- NO 10 NO NO NO - NO ug/L 10/14/98 - - - NO -- ND -- 13 ND NO ND - -- 35 -- -- - - - - -- ND - - - -- NO ND NO ND NO - NO ug/L 04/27/99 - - - NO -- ND -- NO NO NO NO -- -- 58 -- - - - - - -- NO - - - -- 18 NO NO NO NO - NO ug/L 10/21/99 - - - ND -- ND -- NO ND NO ND -- -- 28 -- - - - - - -- ND - - - -- 21 NO NO NO 17 - NO ug/L 03/14/00 - - - NO -- 8 -- NO 8 3 NO -- -- i6 -- - - - - - NO 7 - NO 8 NO 15 5 4 NO 9 - NO ug/L .19/00 - - - NO -- 16 -- NO ND NO ND -- -- ND -- - - - - - -- 19 - - - - 25 21 NO NO 11 - NO ug/L 10/17/00 - - - NO -- NO -- 14 NO NO NO -- -- 40 -- - - - - - -- 18 - - - - 14 NO 28 13 NO - NO ug/L .10/01 - - - NO -- 13 -- 13 14 NO ND -- -- 35 -- - - - - - - 21 - - - - 25 16 NO 11 16 - NO ug/L 10/11/01 - - - NO -- NO -- 14 NO NO NO -- -- 12 -- - - - - - - 26 - - - - 15 12 28 ND NO - NO ug/L 04/18/02 - - - ND -- ND -- NO NO NO ND -- -- ND -- - - - - - - 25.9 - - - - 13 10.8 17.7 NO NO - NO ug/L 10/08/02 - - - NO -- NO -- NO NO NO NO -- -- NO -- - - - - - - 22 - - - - NO NO NO NO NO - NO ug/L 04/09/03 - - - NO -- ND -- NO NO NO ND -- -- 18.5 -- - - - - - - 26.1 - - - -- NO NO NO ND NO - NO u9/L 10/13/03 - - - NO -- NO -- -- - NO NO - -- 12.5 NO NO - - - - - 15.8 - - -- -- NO NO NO 11.4 NO - NO ug/L 04/26/04 - - - NO -- ND -- -- - NO ND - -- 15.9 ND ND - - - - - 19.4 - - -- -- NO ND 19.4 NO NO - NO ug/L 10/25/04 - - - NO -- -- -- -- - NO NO - -- NO NO - - - - - - 13.3 - - -- -- NO NO 13.3 NO NO - NO ug/L .04/05 - - - NO -- ND -- -- - NO ND - -- ND NO NO - - - - - ND - - -- -- ND ND NO NO NO - NO ug/L 10/04/05 - - - NO NO NO -- NO NO NO NO - -- ND NO NO - - - - - 11.9 - - -- -- 11.7 NO 12.8 NO NO - NO ug/L 04/28/06 - - - NO -- ND -- -- - NO ND - -- 12.8 NO NO - - - - NO 25 - NO NO ND 14.2 ND NO ND NO - NO ug/L 10/09/06 - - - NO -- NO -- -- - NO NO - -- ND NO NO - - - - NO 16.9 - NO NO ND NO NO 12.4 NO NO - NO ug/L .204/07 - - - NO -- ND -- - -- NO ND - -- 7.6 NO NO - - - - NO 10.2 - NO NO ND NO ND NO - NO - NO u9/L 10/30/07 - - 1 NO -- 2.6 -- - -- NO NO - -- 2.8 NO 0.43 J - - - - 0.30 J 6.3 - NO 2.7 NO 3.6 NO 4.2 1.2 NO - NO ug/L 04/23/08 - - 1 NO -- 1.6 -- - -- NO NO - -- 5.1 0.90 J ND - - - - NO S. - NO 1.4 ND NO 3.0 NO 1.8 NO - NO ug/L 10/06/08 NO -- 3.3 -- - -- NO 0.59 J - -- 5.8 0.78 J NO -- -- - - NO 11 - NO 1.2 NO 3.4 J 2.1 NO 1.9 3.9 - NO ug/L .13/09 - - 1 NO -- 2.2 -- -- -- 0.59 J NO - -- 5.4 0.95 J ND -- -- - - NO 3.1 - NO 1.6 ND 1.3 ND 0.67 J 1.7 3.0 - NO u9/L 10/15/09 - - 1 NO -- 2.7 -- -- -- NO NO - -- 3.5 1.4 NO -- -- - - 0.62 J 7.5 - 0.92 J 2.1 NO 4.0 NO 5.3 1.1 NO - NO ug/L 04/26/10 - - 1 NO -- ND -- -- -- 0.84 J NO - -- 5.4 0.61 J ND -- -- - - NO 7.2 - NO 1.9 ND 2.0 2.4 0.81 J 1.6 2.4 - NO ug/L 10/19/10 - - 1 NO -- 3.3 -- -- -- NO NO - -- NO ND ND -- -- - - NO NO - NO 1.3 ND ND NO 0.53 J NO 2.1 - NO ug/L 04/18/11 - - 1 NO -- 2.8 -- -- -- NO NO - -- 2.8 0.81 J NO - - - - NO 5.7 - NO 0.91 J ND 0.78 J 0.90 J 1.0 0.71 J 2.2 - NO ug/L 10/10/11 - - 1 NO -- 2.2 - -- - NO NO - -- 3.1 0.73 J NO - - - - NO 5.0 - NO 0.86 J ND 2.8 - 3.7 1.2 Dry - NO ug/L 04/17/12 - - 1 NO -- 2.3 - -- - 0.85 J NO - -- 3.7 0.79 J NO - - - - NO 5.0 - 0.39 J 0.79 J ND 2.0 1.5 NO 1.1 Dry - NO ug/L 10/09/12 - - 1 ND -- 2.0 -- -- - 0.66 J NO - -- 2.6 0.70 J NO - - - - NO 4.0 - NO 1.3 NO 2.0 2.0 NO 1.4 Dry - NO ug/L 04/15/13 - - 1 NO -- 2.4 - -- - 0.67 J NO - -- 3.5 0.75 J NO - - - - NO 6.2 - NO 0.61 J ND 2.6 1.5 NO 1.1 Dry - NO u9/L 09/30/13 - - 1 NO -- 2.2 -- -- - 0.41 J NO - -- 2.3 NO NO - - - - NO 1.6 - ND ND ND 3.1 1.4 NO 0.85 J Dry - NO ug/L 04/16/14 - - 1 NO -- 2.5 -- - - NO 0.43 J -- -- 3.1 NO 0.59 J - - - - NO 3.1 - NO NO ND 1.7 1.8 NO 1.3 Dry - NO ug/L 10/15/14 0.32 - 1 Dry -- 2.6 -- - - 0.77 J NO -- -- 2.3 0.94 J 0.42 J - - - - NO 4.8 - NO 0.62 J NO 2.2 1.5 0.57 J 0.55 J Dry - NO ug/L 04/15/15 0.32 - 1 ND -- 2.3 -- - - NO ND -- -- 1.8 1.2 ND - - - - NO NO - NO 0.72 J ND 0.78 J NO NO NO Dry - NO ug/L 10/07/15 0.32 - 1 NO -- 3.7 -- - - ND NO -- -- 3.4 NO NO - - - - NO 3.4 - NO 0.61 J ND 2.7 1.5 NO 0.51 J 1.2 - NO ug/L 04/11/i6 0.32 - 1 NO - 2.5 -- - - NO ND -- -- 3.3 1.2 0.61 J - - - - NO 2.8 - NO NO ND 0.72 J 0.71 J 0.48 J 0.42 J NO - NO ug/L 11/30/i6 0.32 - 1 ND -- 1.8 -- - - 0.40 J NO -- -- 2.5 0.77 J 0.62 J - - - - ND 2.6 - ND ND ND 1.3 1.1 0.64 J ND 0.48 J - NO ug/L 04/11/17 0.32 - 1 NO -- 2.4 -- - - 0.73 J ND -- -- 1.9 1.3 1.1 - - - - NO 3.9 - NO NO ND 1.4 0.45 J 0.65 J ND NO - NO u9/L 12/12/17 0.32 - 1 NO -- 1.1 -- - - 0.48 J NO -- -- 2.0 0.63 J 0.67 J - - - - NO 1.2 - NO NO NO 1.5 1.1 0.99 J NO 0.47 J - NO ug/L O6/20/18 0.32 - 1 NO -- -- 2.2 - - NO ND -- -- 2.7 NO NO - - - - NO - 1.9 NO NO ND 2.1 2.1 NO ND - NO - u9/L 11/27/18 0.32 1 - NO -- -- 1.8 - -- NO NO -- -- 2.3 NO 0.55 J - - - - NO - 2.3 NO NO NO 1.9 1.1 NO NO -- 0.50 J NO ug/L 04/02/19 0.32 1 - NO -- -- 2.1 - -- NO ND -- -- 1.4 NO 0.97 J - - - - NO -- 2.1 NO NO ND NO 2.4 NO ND -- NO NO ug/L 11/1 9/1 9 0.32 1 - NO -- -- 1.3 - -- 0.70 J NO -- -- 2.5 - - NO NO - - NO -- 2.0 NO NO NO 1.3 1.3 NO NO -- 0.74 J NO ug/L 04/07/20 0.32 1 - NO -- -- 1.3 - -- NO ND -- -- 1.3 - - NO NO 1.8 - NO -- 2.0 - - -- NO 0.89 J NO ND - NO - (Verification Event) ug/L O6/OS/20 0.32 1 - NO -- - - -- -- u /L 10/13/20 0.32 1 - ND -- 1.8 - -- -- NO ND 2.3 - - 0.79 J NO 1.9 NO NO -- 2.4 NO NO ND 1.1 5.4 NO ND - 1.1 zssnareesMeoia�Euvw,owcar�zozwase-zuw.0 Mwncwm .-ircawa ram-­--uaw-rrzozo-z-wu­-- Ewmzoz 1-o.s.eu.. Page 15 d 17 TABLE 5 Summary of Historical Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, NC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SBME Project No. 4358-20-043A Detected Is Active C&D Monitoring Wells Active C Perfo&rnnanc D Monitoring Wells M & NINA Wells Closed MSW Monitoring Wells & NINA Performance Monitoring Wells Off"Ite o"Itorl P. "g Constituent/ r.meter Xylenes (Total) Unit ug/L VI I'll JEEJBac.Igro.nd,. -- - - onit ring We] M - _JJJJJJJJJJJJP�� r - -- r- - -- r -- -- r - -- -- r- - - - .r - - -- -- -- for the -- or nitoring CIO: ad MSW Landfill -- - - -- -- -- -- -- -- - -- Pr ND NC 2L = 500 ug/L ug/L 03/2,191ND EPA MCL = 10000 ug/L ug/L 03/10/92 - - - - -- -- -- -- -- -- -- -- -- - - - - - - - - -- - - - -- -- -- - - - - ND ug/L 04/20/95 _ _ _ __ __ __ __ __ __ __ __ __ __ _ _ _ __ _ _ _ _ __ _ _ _ __ __ __ _ _ _ _ ND ug/L O6/27/95 - - - -- ND -- -- -- -- -- -- -- -- -- - - - - - - - -- - - - - NO ND 4.7 4.3 - - NO ug/L 09/22/95 - - - NO -- -- -- -- -- -- -- -- -- -- - - - - - - NO -- - ND ND NO NO NO NO NO - - NO ug/L 03/28/96 - - - NO -- -- -- -- -- -- -- -- -- -- -- -- - - - - - -- - NO NO - NO ND NO NO - - NO ug/L 10/29/96 - - - NO -- NO -- NO NO NO NO -- -- NO -- -- - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 04/08/97 - - - NO NO ND -- NO ND NO ND -- -- ND -- -- - - - - -- ND - - - -- NO ND NO NO NO - NO ug/L 10/29/97 - - - NO -- NO -- NO NO NO NO -- -- NO -- -- - - - - -- NO - - - - 10.2 NO NO NO NO - NO ug/L 04/30/98 - - - ND -- NO -- NO ND NO ND -- -- ND -- -- -- -- - - -- ND - - - - NO ND NO ND 18 - NO ug/L 10/14/98 - - - NO -- NO -- NO NO NO NO -- -- NO -- -- -- -- - - -- NO - - - - NO NO NO NO NO - NO ug/L 04/27/99 - - - NO -- NO -- NO ND NO ND -- -- ND -- - - - - - -- ND - - - -- NO ND NO ND NO - NO ug/L 10/21/99 - - - NO -- NO -- NO NO NO NO -- -- ND -- - - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 03/14/00 - - - NO -- NO -- NO ND NO ND -- -- ND -- - - - - - NO ND - NO NO ND NO ND NO ND NO - NO ug/L 04/19/00 - - - NO -- NO -- NO NO NO NO -- -- ND -- - - - - - - NO - - - -- NO NO NO NO NO - NO ug/L 10/17/00 - - - ND -- NO -- NO ND NO ND -- -- ND -- - - - - - - ND - - - -- NO ND NO ND NO - NO ug/L 04/10/01 - - - NO -- NO -- NO NO NO NO -- -- NO -- - - - - - - NO - - - -- NO NO NO NO NO - NO ug/L 10/11/01 - - - NO -- ND -- NO NO NO ND -- -- ND -- - - - - - - ND - - - -- NO ND NO ND NO - NO ug/L 04/18/02 - - - NO -- NO -- NO NO NO NO -- -- NO -- - - - - - -- NO - - -- -- NO NO NO NO NO - NO ug/L 10/O'/02 - - - NO -- ND -- NO NO NO ND -- -- ND -- - - - - - - ND - - -- -- NO ND NO ND NO - NO ug/L 04/09/03 - - - NO -- ND -- NO NO NO NO -- -- NO -- - - - - - - NO - - -- -- NO NO NO NO NO - NO ug/L 10/13/03 - - - ND -- ND -- -- - NO ND -- -- ND NO NO - - - - - ND - - - -- NO ND NO ND NO - NO ug/L 04/26/04 - - - NO -- ND -- -- - NO NO -- -- ND NO NO - - - - - NO - - - -- NO NO NO NO NO - NO ug/L 10/25/04 - - - NO -- ND -- -- - NO ND -- -- ND NO - - - - - - ND - - - -- NO ND NO ND NO - NO ug/L .04/05 - - - NO -- ND -- -- - NO NO -- -- ND NO NO - - - - -- NO - - - -- NO NO NO NO NO - NO ug/L 10/04/05 - - - NO ND ND -- NO NO NO ND -- -- ND NO NO - - - - -- NO - - - -- NO ND NO NO NO - NO ug/L 04/28/06 - - - NO -- ND -- -- - NO NO -- -- NO NO NO - - - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/09/06 - - - NO -- ND -- - - NO ND -- -- ND NO NO - - - - NO NO - NO NO ND NO ND NO NO NO - NO ug/L .24/07 - - - NO -- ND -- - - NO NO - -- NO NO ND - - - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/30/07 - - 5 NO -- 3.8 J -- - - 3.7 J ND - -- 0.52 J NO ND -- -- - - NO 4.3 J - NO NO ND 0.34 J ND 4.4 J 0.44 J NO - NO ug/L 04/23/08 - - 5 NO -- ND -- - - NO NO - -- NO NO NO -- - - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/06/08 - - 5 NO -- ND -- - - NO ND - -- NO NO ND -- - - - NO NO - NO NO ND NO ND NO NO 5.4 - NO ug/L 04/13/09 - - 5 NO -- ND -- -- -- NO NO - -- 0.47 J NO NO -- - - - NO NO - NO ND ND NO NO ND 0.41 J 0.98 J - NO ug/L 10/15/09 - - 5 NO -- ND -- -- -- NO ND - -- 0.51 J NO ND -- - - - NO 0.54 J - NO NO ND NO ND 0.46 J 0.45 J NO - NO ug/L 04/26/10 - - 5 NO -- ND -- -- -- NO NO - -- 0.52 J NO NO -- - - - NO NO - NO ND ND NO NO ND NO 1.3 J - NO ug/L 10/19/10 - - 5 NO -- ND -- -- -- NO NO - -- 0.48 J NO ND -- -- - - NO 0.47 J - NO NO ND NO ND 0.47 J 0.41 J NO - NO ug/L 04/18/11 - - 5 NO -- ND -- -- -- NO NO - -- NO NO NO -- - - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 10/1 0/1 1 - - 5 NO -- ND -- -- -- NO ND - -- NO NO ND -- - - - NO NO - NO NO ND NO -- NO NO Dry - NO ug/L 04/17/12 - - 5 NO -- ND -- -- -- NO NO - -- 0.56 J NO NO - - - - NO NO - NO NO NO NO NO NO NO Dry - NO ug/L 10/09/12 - - 5 NO -- ND -- -- -- NO ND - -- 0.45 J NO ND - - - - NO ND - NO NO ND NO ND NO ND Dry - NO ug/L 04/15/13 - - 5 NO -- ND -- -- -- NO NO - -- NO NO NO - - - - NO NO - NO NO NO NO NO NO NO Dry - NO ug/L 09/30/13 - - 5 NO -- ND -- -- -- NO ND -- -- ND NO ND - - - - NO ND - NO NO ND NO ND NO ND Dry - NO ug/L 04/16/14 - - 5 NO -- ND -- -- -- NO NO -- -- NO NO NO - - - - NO NO - NO ND ND NO NO ND NO Dry - NO ug/L 10/15/14 0.45 - 5 Dry -- ND -- -- -- NO ND -- -- ND NO ND - - - - NO ND - NO NO ND NO ND 0.60 J ND Dry - NO ug/L 04/15/15 0.45 - 5 NO -- ND -- -- -- NO NO -- -- ND NO NO - - - - NO NO - NO ND ND NO NO NO NO Dry - NO ug/L 10/07/15 0.45 - 5 NO -- ND -- -- -- NO NO - -- ND NO ND - - - - NO ND - NO NO ND NO ND 0.93 J ND NO - NO ug/L 04/1 1/1 6 0.45 - 5 NO -- ND -- -- -- NO NO - -- NO NO NO - - - - NO NO - NO NO NO NO NO NO NO NO - NO ug/L 11/30/16 0.45 - 5 NO -- ND -- - -- NO NO - -- ND NO ND - - - - NO ND - NO NO ND NO ND 0.61 J NO NO - NO ug/L 04/11/17 0.45 - 5 NO -- ND -- - -- NO NO - -- ND NO NO - - - - NO NO - NO ND ND NO NO 1.3 B NO NO - NO ug/L 12/12/17 0.45 - 5 ND -- ND -- - -- NO ND - -- ND NO ND -- - - - NO ND -- NO NO ND NO ND 1.2 J NO NO - NO ug/L O6120/18 0.45 - 5 NO -- -- NO - -- NO NO - -- NO NO NO - - - - NO -- NO NO NO NO NO NO 0.99 J NO -- NO - ug/L 11/27/18 0.45 3 - ND -- -- ND - -- NO ND - -- ND NO ND - - - - NO -- NO NO NO ND NO ND NO NO - NO NO ug/L 04/02/19 0.45 3 - NO -- -- NO - -- NO NO - -- NO NO NO - - - - NO -- NO NO NO NO NO NO NO 0.45 J - NO NO ug/L 11/19/19 0.45 3 - NO -- -- ND - - NO NO - -- NO -- - NO NO - - NO - NO NO NO ND NO NO 2.2 J NO - NO NO ug/L 04/07/20 0.45 3 - NO -- -- NO - - NO NO - -- 0.48 J -- - NO NO NO - NO - NO - - -- NO NO 0.7 J NO - NO - u /L 10/13/20 0.45 3 ND NO ND 0.49 J NO NO NO NO ND NO NO NO NO NO 2.2 0.46 J NO 1,4-Di-ne ug/L 11/27/18 1.2 2.0 - ND -- -- 5.6 - - 1.8 J 2.6 - -- 15 ND 4.8 - - - - 2.8 - 7.3 NO 7.8 NO 2.9 4.6 6.3 39 -- NO NO NC 2L= 3.0 ug/L ug/L 04/02/19 1.2 2.0 - NO -- -- 4.8 - - 1.5 J 4.6 - -- 11 NO 3.9 - - - - 2.0 - 8.4 NO 7.5 NO 1.6 J 4.0 7.2 23 - NO NO ug/L 11/19/19 0.8 2.0 - NO -- -- 3.9 - - 6.0 2.8 - -- 15 - - 1.6 J 5.2 -- - 2.0 - 4.8 2.3 14 1.1 J 1.4 J 10 39 22 - NO NO ug/L 04/07/20 0.8 2.0 - NO -- -- 5.9 - - 4.1 3.8 - -- 15 - - 3.0 8.5 11 - 2.2 - 4.3 - -- - 2.5 1 J 16 29 - NO - u /L 04/07/20 0.8 2.0 NO 4.4 3.4 2.5 14 2.3 6.8 10 2.8 1.3 5.4 NO 9.7 1.0 J 2.0 6.9 29 25 NO Tetrahydrofuran ug/L O6/20/18 0.53 - - NO -- -- 2.6 - - NO NO - -- 1.8 NO NO - - - - NO - 5.5 - - - - - - - - - - ug/L 11/27/18 0.53 1.0 - NO -- -- NO - - NO NO - -- NO NO NO - - - - NO - NO - - - - - - - - - - ug/L 04/02/19 0.53 1.0 - NO -- -- ND - - NO NO - -- NO NO 8.5 - - - - NO - 15 - - - - - - - - - - ug/L 11/19/19 0.53 1.0 - NO -- -- NO - - NO NO - -- NO - - NO NO - - ND - NO - - - - - - - - - - u /L 1.1.0 0.53 1.0 NO 2.4 NO ND 3.3 NO NO 5.8 zssnareesMeoia�Euvw,owcar�zozwass-zuw.0 Mwncwm .-ircawa ram-­--uaw-rrzozo-z-wu­-- Ewmzoz 1-o.s.eu.. Page 16 d17 TABLE 5 Summary of Historical Groundwater Monitoring Results (Detected Constituents) Water Quality Monitoring Report, October 2020 Monitoring Event Moore County Landfill, INC Solid Waste Permit No. 63-01 Aberdeen, Moore County, North Carolina SBME Project No. 4358-20-043A Detected Monitoring Sulfide ug/L S-Ple 04/11/17-- M.L EEk�c ground .JVMM r •• r Active C&D Monitoring r Wells .• Active Perfo&rnnaoc C D Monitoring Wells ritoring o:Mor & MINA Wells - Closed MSW Monitoring Wells & MINA Performance Monitoring Wells OffsIte Private Well ug/L 12/12/17 1000 ND -- -- -- - -- NO - - - -- 91, 000 J - - - 54 J - 16 J -- - ND ND ND 110 J 130 J 270 J 660 J - ug/L 06/20/18 0.01 1 ND -- NO 38,000 J NO ND NO - - - -- - ND - - 50 J - NO -- - ND ND ND 130.00 J NO 270 J - NO - ug/L 11/27/18 - ND -- -- 17,000 J - -- NO - - -- - -- 43.000 J - - 62 J - NO -- - ND ND NO 97 J 320 140 - NO - ug/L 04/02/19 0.01 0.1 - NO -- -- 150,000 - -- NO - - -- - - 110 - - 46 J - NO - - NO NO ND 65.000 J 57.000 J 170 - 21 J - ug/L 04/07/20 - NO -- 42,000 J 83,000 J NO - NO -- -- -- 42,000 J - 110 - - 16 J - - NO 28 J - - - 160.00 270.00 100 - 58 J - u /L 10/13/20 NO 22,000 J NO ND 120,000 NO NO 42 J NO NO NO 17 J NO NO NO 160.00 NO 78 J 140 27 J Chloride ug/L 04/11/17 - NO -- -- -- - - 12,000 - - -- - 41,000 - - - 42,000 - 43,000 - - NO 40,000 3,700 J 16,000 2,900 J 95,000 NO - - ug/L 12/121 7 - 2,200 J -- -- -- - - 17,000 - - -- - 38,000 - - - 47,000 - 31,000 - - 9,900 54,000 4,100 J 20,000 14,000 92,000 NO - ug/L O6/20/18 2.2 - NO -- 22,000 6,900 4,800 J 17,000 14,000 - - -- - - 28,000 - - 44,000 - 34,000 - - NO 63,000 2,800 J 15,000 7,100 110,000 - 3100 J - ug/L 11/27/18 2.2 5.0 - NO -- 23,000 3,900 J 5,200 16,000 15,000 - - -- - - 32,000 - - 42,000 - 20,000 - - NO 30,000 2,700 J 16,000 6,300 120:000 - NO - ug/L 04/02/19 2.2 5 - NO -- 23,000 3,500 J 7,800 20,000 15,000 - - -- - - 40,000 - - 39,000 - 20,000 - - NO 29,000 3,800 J 13,000 5,000 94,000 - NO - ug/L 04/07/20 - NO -- 21,000 8,400 7,300 - 14,000 - - -- 33,000 - 23,000 - - 56,000 - - 20,000 3,200 J - - - 14,000 4,000 J 1,000,000 - 3100 J - ug/L 10/13/20 2,500 J 21,000 7,700 5,600 52,000 22,000 3,000 41,000 14,000 8,900 27,000 2,300 J 38,000 5,500 13,000 20,000 69,000 100,000 D 2900 J Nitrate as ug/L 04/11/17 10000 240 J -- -- -- - - 6,200 J - - -- - 86,000 J - - - 100 J - 14,000 - - 950 J 180 J NO 77 J 160 J 140 J 180 J - - ug/L 12/12/17 10000 550 J -- -- -- - - 2,600 J - - -- - 140,000 J - - - 130 J - 280 J - - 600 J 1,100 J NO 140 J 140 J 120 J 160 J - ug/L O6/20/18 0.025 10 450 J -- -- -- - - 810 J - - -- - - 90,000 J - - 120 J - 6,000 J - - 840 J 1,700 J ND 140 J 110 J 170 J - 140 J - ug/L 11/27/18 - 410 -- -- -- - - 3,300 - - -- - - 180,000 - - 170 - 4,400 - - 1,200 50 J NO 130 200 200 - 240 - ug/L 04/07/20 - 320 -- -- -- - - 4,600 - - -- - - 110 - - - - - - - - - - 89 J 95 J 90 J - 76 J - ug/L 10/13/20 380 J 2,300 J 90 J 850 130 NO 110 200 120 100 510 Nitrite as ug/L 04/11/17 1000 NO -- -- -- - - NO - - -- - NO - - - 19 J - 30 J - - NO NO NO 33 J NO NO NO - - ug/L 12/12/17 1000 NO -- -- -- - - 34 J - - -- - NO - - - ND - NO - - NO NO NO NO NO NO NO - ug/L O6/20/18 0.017 1 NO -- -- -- - - NO - - -- - - NO - - NO - NO - - NO NO NO NO NO NO - NO - ug/L 11/27/18 - NO -- -- -- - - NO - - -- - - NO - - NO - NO - - NO NO NO 17 J NO NO - NO - ug/L 04/0219 0.017 0.1 - ND -- -- -- - - 82 J - - -- - - NO - - 27 J - NO - - NO NO NO 98 J NO ND - NO - u9/L 04/07/20 - NO -- -- -- - - NO - - -- - - NO - - - - - - - - - - NO NO NO - 38 J - u /L 10/13/20 ND ND NO NO NO NO NO NO NO ND NO Total Dissolved Solids ug/L O6/20/18 50 - NO -- 160,000 NO NO 250,000 190,000 - - -- - - 490,000 - - 180,000 - 200,000 - - - - - - - -- - - - ug/L 11/27/18 50 50 - ND -- 250,000 ND 52,000 250,000 190,000 - - -- - - 540:000 - - 160,000 - 110:000 - - - - - - - -- - - - ug/L 04/02/19 50 50 - NO -- 260,000 NO 74,000 350,000 298:000 - - -- - - 970,000 - - 270,000 - 220,000 - - - - - - - -- - - - ug/L 04/07/20 - NO -- 290,000 66,000 80,000 - 240,000 - - -- 420,000 - 550,000 - - 280:000 - - 410,000 290,000 - - - - - -- - - - ug/L 10/13/20 NO 290,000 250,000 80,000 240,000 96,000 50,000 240,000 550,000 350,000 200,000 430,000 160,000 150,000 410,000 550,000 Sulfate as SO4 ug/L 04/11/17 250000 NO -- -- -- - - 24,000 J - - -- - 61,000 J - - - 14,000 J - 98,000 J - - 9,300 J 10,000 J 8,700 J 14,000 J NO 3500 J NO - - ug/L 12/12/17 250000 NO -- -- -- - - 31,000 J - - -- - 33,000 J - - - 11,000 J - 38,000 J - - 10,000 J 16,000 J 10,000 J 8,900 J NO NO 18,000 J - ug/L O6/20/18 2.9 250 ND -- 19,000 J ND NO 44,000 J 23,000 J - - -- - - 3,500 J - - 9,800 J - 22,000 J - - 8,600 J 13,000 J 9,100 J 7,300 J NO ND - 31,000 J - ug/L 11/27/18 2.9 5.0 - NO -- 20,000 NO 6,300 43,000 26,000 - - -- - - 4,300 J - - 8,100 - 29,000 - - 7,600 5,200 7,600 9,200 NO NO - 1, 100 - ug/L 04/02/19 2.9 5 - ND -- 18,000 NO 3,600 J 94,000 24,000 - - -- - - 67,000 - - 9,200 - 61,000 - - 8,200 4,500 J 7,900 1,600 ND ND - 8,700 - ug/L 04/07/20 - NO -- 14,000 NO 4,900 J - 37,000 - - -- 35,000 - NO - - ND - - 82,000 38,000 - - - 10,000 NO NO - 9,700 - u /L 10/13/20 ND 13,000 16,000 9,100 7,100 99,000 35,000 72,000 12,000 32,000 NO 8,000 5,500 8,400 7,200 NO NO NO 7,200 Total Alkalinity as CaCO3 ug/L 04/11/17 - NO -- -- -- - - 34,000 - - -- - 810,000 - - - 150,000 - 470,000 - - NO 230,000 NO 200,000 110,000 920,000 110,000 - - ug/L 12/121 7 - ND -- -- -- - - 82,000 - - -- - 630,000 - - - 170:000 - 350:000 - - 49,000 290:000 D ND 260,000 110,000 1,000,000 130,000 - ug/L O6/20/18 14 - NO -- 200,000 87,000 24,000 190,000 120,000 - - -- - - 550,000 - - 170,000 - 94,000 - - NO 310,000 NO 250:000 150,000 1,100,000 - 85,000 - ug/L 11/27/18 14 15 - NO -- 1fi0,000 81,000 33,000 170,000 140,000 - - -- - - 610,000 - - 1,300,000 - 41,000 - - NO 180,000 ND 240,000 160,000 890,000 - 90,000 - ug/L 04/02/19 14 15 - NO -- 200,000 NO 59,000 140,000 110,000 - - -- - - 750,000 - - 120,000 - 20,000 - - NO 170,000 NO NO NO 710,000 - 40,000 - ug/L 04/07/20 - NO -- 190,000 51,000 31,000 - 100,000 - - -- 190,000 - 490,000 - - 140,000 - - 140,000 170,000 - - - 210,000 110,000 740,000 - 83,000 - u /L 10/13/20 NO 220,000 49,000 NO 190:000 140,000 120,000 290,000 95,000 39,000 620,000 NO 180,000 NO 190,000 120,000 240,000 D 830,000 96,000 Total Organic Carbon ug/L 04/11/17 - NO -- -- -- - - 14,000 - - -- - 33,000 - - - 9,200 - 43,000 - - 1200 9,100 780 J 26,000 13,000 59,000 37,000 - - ug/L 12/12/17 - ND -- -- -- - - 22,000 - - -- - 32,000 - - - 13,000 - 27,000 - - 5200 8,700 9,200 15,000 7,100 40,000 14,000 - ug/L O6/20/18 0.00034 - NO -- -- -- - - 27 - - -- - - 24 - -- 12.000 I - 11.000 - - 0.0017 12,000 1,100 19,000 6,500 66,000 - 4.8 - ug/L 11/27/18 340 1000 - 470 J -- -- -- - - 21,000 - - -- - - 28,000 - -- 15,000 - 9,300 - - 1900 7,800 1,000 25,000 60,000 68,000 - 3,300 - ug/L 04/02/19 0.00034 0.001 - NO -- -- -- - - 21 - - -- - - 66 - -- 12.000 - 11.000 - - 0.0011 0.0062 0.00095 J 0.056 0.694 42,000 - 43 - ug/L 04/07/20 - NO -- -- -- - - - - - -- - - 15,000 - -- -- - -- - - - -- -- 26,000 17,000 32,000 - 1,700 - u /L 10/13/20 NO 11,000 22,000 930 J 30,000 21,000 21,000 37,000 2,600 Nitrate/Nitrite as IN ug/L 04/11/17 - 240 -- -- -- - - 6,200 - - -- - 86,000 J - - - 120 - 14,000 - - 950 180 NO 110 160 140 180 - - ug/L 12/121 7 - 550 -- -- -- - - 2,600 - - -- - 140,000 - - - 130 - 280 - - 600 1100 NO 140 140 120 160 - ug/L O6/20/18 0.041 - 450 -- -- -- - - 810 - - -- - - 90 J - - 120 - 6,000 - - 0.84 1700 NO 140 110 170 - 140 - ug/L 11/27/18 0.04 0.1 - 410 -- -- -- - - 3,300 - - -- - - 180 - - 170 - 4,400 - - 1.2 50 J NO 150 200 200 - 240 - ug/L 04/02/19 0.041 0.1 - 320 -- -- -- - - 7,600 - - -- - - 110 - - 110 - 3,600 - - 1 48 J NO 150 80 J 100 - 120 - ug/L 04/07/20 - 320 -- -- -- - - 4,600 - - -- - - 110 - - - - - - - - - - 0.089 J 0.095 J 99 J - 0.11 - u /L 10/13/20 - 380 J -- -- -- - - - - - -- - - - -- -- - 2,300 J - 90 J 850 130 - 110 200 120 100 - 510 - Ethane ug/L 04/11/17 - NO -- -- -- - - NO - - -- - NO - - -- NO - NO - - NO NO NO NO NO NO NO - - ug/L 12/12/17 - NO -- -- -- - - NO - - -- - NO - - -- NO - NO - - NO NO NO NO NO NO NO - ug/L O6/20/18 0.0013 - ND -- -- -- -- -- NO -- -- -- - - NO - -- NO - NO - - NO ND ND NO ND ND -- NO - u9/L 11/27/18 1.30 2.00 - NO -- -- -- -- -- NO -- -- -- - - NO - -- NO - NO - - NO NO NO NO NO NO -- NO - ug/L 04/02/19 0.0013 0.002 - ND -- -- -- - -- NO -- -- -- - - NO - -- NO - NO -- - NO NO ND NO ND ND -- NO - ug/L 04/07/20 - NO -- -- -- - -- -- -- -- -- - - NO - -- -- - -- -- - - - - NO NO NO -- NO - u /L 10/13/20 - NO -- -- -- - -- -- -- -- -- - - -- -- -- - NO -- NO NO - ND ND NO ND -- NO - Ethene ug/L 04/11/17 - NO -- -- -- - -- NO -- -- -- - NO - -- -- NO - NO -- - NO NO NO NO NO NO NO - - ug/L 12/1 21 7 - NO -- -- -- - -- NO -- -- -- - NO - - - NO - NO -- - NO NO ND NO ND ND NO - u9/L O6/20/18 0.0015 - NO -- -- -- - -- NO -- -- -- - - NO - - NO - NO -- - NO NO NO NO NO NO - NO - ug/L 11/27/18 1.50 3.00 - NO -- -- -- - -- NO -- -- -- - - NO - - NO - NO -- - NO NO ND NO NO NO - NO - ug/L 04/02/19 0.0015 0.003 - NO -- -- -- - -- NO -- -- -- - - NO - - ND - NO - - NO NO NO ND NO NO - NO - ug/L 04/07/20 - NO -- -- -- - -- -- -- -- -- - - NO - - - - -- - - - - - NO NO NO - NO - u9/L 10/13/20 NO NO NO NO NO NO NO NO NO NO Methane ug/L 04/11/17 - 496 J -- -- -- - - 564 J - - -- - 226 5060 - 72 636 J 993 ND 6050 1,560 590 5100 -- - ug 2,12M7 567 J 187 1,670 1,670 879 264 11.6 NO 1,,790 1,620 2,340 3,580 u O6/20/18 0.0004 NO 134 - 2,850 3,100 154 NO 40.9 NO 45 2970 2,350 - 397 - ug 11/27/18 0.45 1.00 NO 19 3,730 10 9 NO 185 NO 3,840 4,020 5,640 958 - ug/L 04/02/1 0.00045 0.001 ND 6 1,96 3,6600 39 566 J 54.9 NO 4060 5930 , 5,04 2080 - 04/07/20 NO -- -- -- - - - - - -- - - - - - - - - - - - - 2,g/L 160 1940 5 1360u - u /L 10/13/20 NO NO 4,460 NO NO 3,680 6,150 5,680 D 3,200 Carbon dioxide u9/L 04/07/20 17,200 547,000 51,000 55,700 499,000 288,000 451,000 365,000 u /L 10/13/2. 21,600 573,000 55,700 5,240 47,500 429,000 D 406,000 D 462,000 J 729,000 D 425,000 2,4-D [2C] u /L O6/20/18 0.27 ND NO NO ND NO ND ND ND ND ND ND NO Dlnoseb [2C1 u /L O6120/18 0.32 ND ND ND NO NO NO NO NO ND NO NO NO 2,4,STP Silvex u /L O6120/18 0.44 ND I NO 0.49 J ND NO ND ND NO ND NO I NO ND Notes: 1.) ug/L = Micrograms par liter 2.) NO = Not detected at the stated reporting limit 3.) NM = Not measured 4.) J = Estimated concentration reported below Solid Waste Section Limit S.) - = No data available 6.) Blanks = Field, trip, and method blanks 7.) Reanalysis = Reanalysis result in parenthesis next to the original result (e.g., reanalysis was performed for arsenic in January 2017) 8.) Dissolved = Dissolved sample in brackets [e.g. a dissolved sample was analyzed for Ml for the Febuary 2017 verification event] 9.) Bold = Concentration above the current INC 2L Groundwater Standard or INC 2L IMAC Groundwater Standard 10.) Shaded and Bold = Concentration above the current NC 2L Groundwater Standard or NC 2L IMAC Groundwater Standard and EPA MCL 11.) EPA MCL = US Environmental Protection Agency Maximum Contaminant Level 12.) SWS GSP = Solid Waste Section Groundwater Protection Standard 13.) SWS Reporting Limit = NCPQL or lab-specifc reporting limit prior to October 2007 and NCSWSL starting in October 2007 and ending June 1, 2018 14.) - = EPA MCL is an action level 15.) ° = EPA MCL is a secondary standard 16.) Historical data prior to 10/30/07 provided by HDR Engineering of the Carolinas, Inc. Data 10/30/07 to 6/30/2020 Provided by Golder 17.) Samples collected using low -flow purge and sample techniques. 18.) The following dilutions were noted for the April 2020 event: Chloride & Sulfate 2x @ MW-17S, 4x @ MW-1Q Sx @ Ml 10x @ MW-14, 50x @ Ml Nitrate as IN, Nitrate/Nitrite as N 10x @ Ml Total Alkalinity as CaCO3 2x @ Ml Ml Ml MW-14, 5x @ MW-11SR, MW-11DR, Ml 10x @ Ml Antimony, Selenium, Thallium 2x @ Ml Ml MW-11SR, MW-11 DR, MW-135, MW-13D, MW-14, MW-175, MW-17D, MW-18, SW-1, SW-2, SW-3, SW-4, Field Blank;CO2 & Methane 2.1x @ MW-iSR, Sx: MW-11SR, 10x @ Ml Ml Ml Ml 19.) PQL -Practical quantitation limit -lab specific limit 20.) MOIL= Method Detection Limit 21.) SWSL = Solid Waste Section Reporting Limits (historic) 22.) The Blake Well not sampled in June 2018 and April 2020 as the power was out at the residence and no sample could be obtained. zssnareesMeoia�Euvw,owcarwozwass-zo-oau Mwncwmy aamre ircawa ram�m.��a+T•o+ se�uawa�e.auaM rrzozo-zoz+�wwu„�w.u.wm ra.awmzozo-+owams.eu.. cwnw.a�.ss. Page 17 of 17 Appendix IV - Time vs Concentration Charts 12.0 11.5 11.0 10.5 10.0 9.5 9.0 8.5 8.0 7.5 J ao 7.0 7 •E- 6.5 c 0 4� 6.0 nz L U 5.5 U 0 5.0 U 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 0.0 Benzene Concentrations Over Time - MSW Landfill Wells lD n n 00 00 M M O O ci ci N N M M V V M M lD lD n n 00 00 M M O O -1 ci N N m m V V M M LD LD n n 00 00 O M O O Ql Ql Ql Ql Ql Ql M O O O O O O O O O O O O O O O O O O O O c-i c-i c-i c-i i--I -4 -4 -4 -4 -4 -4 -4 c-i c-i c-i c-i c-i c-i c-i c-i N N \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O KT O KT O KT O O O O O KT O KT O KT O KT O K* O K* O O O KT O KT O �T O KT O O O K* O O O c-i O c-i O c-i O c-i O c-i O N O N O c-i O c-i O c-i O c-i O c-i O c-i O N O N O N O N O N O c-i O c-i O c-i O c-i O c-i O c-i O N Sampling Dates MW-6 MW-7 MW-8 MW-9 MW-15R Z:\Shared\SME\Ops\ENV\Projects\2020\4358-20-043A Moore County Routine LFG & WQ Monitoring\Task 01 - Semi -Annual Water Quality FY 2020-2021\Working_Documents Fall Event\Table for 2L Exceedance Charts —Fall 2020.xlsx 5.0 4.5 4.0 3.5 3.0 c v 2.0 1.5 1.0 0.5 0.0 Benzene Concentrations Over Time - C&D Landfill Wells lD r\ r\ 00 00 M M O O cI cI N N M m V V M M lD lD r\ r\ 00 00 M M O O cI cI N N m M V V M M LD LD r\ r\ 00 00 M M O O M M M M M M M O O O O O O O O O O O O O O O O O O O O c-i c-i N N i--I N i--I N i--I N i--I N N N N N N N N N N N \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O KT O KT O KT O O K* O K* O O �T O �T O KT O KT O K* O K* O O O KT O KT O KT O KT O O O K* O O KT O N O c-i O c-i O c-i O c-i O c-i O N O N O N O N O N O c-i O c-i O c-i O c-i O c-i O c-i O c-i O N O N O N O N O N O c-i O c-i Sampling Dates MW-11DR MW-11SR MW-13SR —MW-14 Z:\Shared\SME\Ops\ENV\Projects\2020\4358-20-043A Moore County Routine LFG & WQ Monitoring\Task 01 - Semi -Annual Water Quality FY 2020-2021\Working_Documents Fall Event\Table for 2L Exceedance Charts —Fall 2020.xlsx C 30.0 25.0 20.0 10.0 5.0 0.0 Vinyl Chloride Concentrations Over Time - MSW Landfill Wells l0 n n 00 00 M M O O ci ci N N M M V V M M lD lD n n 00 00 O M O O ci ci N N m m V V M Ln lD l0 n n 00 00 O M O O Ql Ql Ql Ql Ql Ql M O O O O O O O O O O O O O O O O O O O O c-i c-i c-i c-i i--I -4 -4 -4 -4 -4 -4 _q c-I C-I C-I C-I C-I C-I C-I C-I N N \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O KT O KT O KT O O O O O KT O KT O KT O KT O K* O K* O O O KT O KT O �T O KT O O O K* O O O c-i O c-i O c-i O c-i O c-i O N O N O c-i O c-i O c-i O c-i O c-i O c-i O N O N O N O N O N O c-i O c-i O c-i O c-i O c-i O c-i O c-i Sampling Dates MW-6 MW-7 MW-8 MW-9 MW-15R Z:\Shared\SME\Ops\ENV\Projects\2020\4358-20-043A Moore County Routine LFG & WQ Monitoring\Task 01 - Semi -Annual Water Quality FY 2020-2021\Working_Documents Fall Event\Table for 2L Exceedance Charts —Fall 2020.xlsx 60.0 50.0 40.0 C C 0 +� 30.0 L Y U C 0 U 20.0 10.0 0.0 Vinyl Chloride Concentrations Over Time - C&D Landfill Wells tD n n W 00 M M O O -1 -1 N N M M V V M M tD tD n n 00 00 M M O O -1 rH N N M M V V M M l0 l0 n n 00 00 M M O O Ol 01 Ol 01 Ol M M O O O O O O O O O O O O O O O O O O O O \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ \ ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci ci O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O KT O KT O KT O O K* O K* O O KT O KT O KT O KT O K* O K* O O O �T O �T O KT O KT O O O K* O O O N O N O N O N O c-i O c-i O c-i O c-i O c-i O c-i O c-i O N O N O N O N O N O N O c-i O c-i O c-i O c-i O c-i O c-i O c-i O N Sampling Dates MW-11DR MW-11SR MW-13SR —MW-14 Z:\Shared\SME\Ops\ENV\Projects\2020\4358-20-043A Moore County Routine LFG & WQ Monitoring\Task 01 - Semi -Annual Water Quality FY 2020-2021\Working_Documents Fall Event\Table for 2L Exceedance Charts —Fall 2020.xlsx 1,4-Dioxane Concentrations Over Time - MSW Landfill Wells 39.0 MIXII, 29.0 24.0 c c 0 a 19.0 14.0 9.0 Leta: -1.0 y(b 00 yam' y�i ti� ti0 tiC tiC5 ti� yam' y°, tiC tiC tiC5 y0 10 10 10 to l0 10 10 10 10 titi\o�\ titi\Q, oti\o�\ oti\oy\ o�\oy\ o°\o�\ o`'\o�\ oo�\oy\ oo y yy\oti� y�\oti� Sampling Dates MW-6 MW-7 MW-8 MW-9 MW-15R MW-2 Z:\Shared\SME\Ops\ENV\Projects\2020\4358-20-043A Moore County Routine LFG & WQ Monitoring\Task 01 - Semi -Annual Water Quality FY 2020-2021\Working_Documents Fall Event\Table for 2L Exceedance Charts —Fall 2020.xlsx 1,4-Dioxane Concentrations Over Time - C&D Landfill Wells 16.0 15.0 14.0 13.0 12.0 11.0 10.0 J 9.0 c 0 +� 8.0 L u 7.0 c 0 v 6.0 5.0 4.0 3.0 2.0 1.0 0.0 y° o o ° \y° titi\°�\y00 titi\°y\y00 oti\°y\y° oti\°'\y° o�,\°y\y° o�\y° o�\y° o�,\°y\y° oo,\°�\y° ti°�o�\y° titi�oy\y° titi�o�\y° oti° otio o�o o°�oy\�o o`'�oy\�o o�o o��oy\�o Sampling Dates MW-11DR—MW-11SR MW-13SR -MW-14 Z:\Shared\SME\Ops\ENV\Projects\2020\4358-20-043A Moore County Routine LFG & WQ Monitoring\Task 01 - Semi -Annual Water Quality FY 2020-2021\Working_Documents Fall Event\Table for 2L Exceedance Charts —Fall 2020.xlsx