6001_Mecklenburg_Harrisburg_MSWLF_Dec20GW_FID1523804_20210114

�fDENR USE ONLY ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No } Doc/Event #:
' 'NC DENR ' Environmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Mecklenburg County Solid Waste Services
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Amber R. Grzymski, P.G. Phone: [phone]
E-mail: [e-mail]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Harrisburg Road Landfill 7817 Harrisburg Road, Charlotte 60-01 .0500 December 8 & 11, 2020
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring QX Detection Monitoring ❑ Assessment Monitoring Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells �R Methane gas monitoring data
Groundwater monitoring data from private water supply wells F1 Corrective action data (specify)
Leachate monitoring data ❑ Other(specify)
Surface water monitoring data
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Amber R. Grzymski, P.G. 1 Project Manager
Facility Rep dentat ve am int) Title
/I A x ^ 1-14-2021
Signatu Date
2145 Suttle Ave, Charlotte, NC 28208
Facility Representative Address
980-314-3855
(Area Code) Telephone Number
Affix NC Licensed,(•, gtgssional Geologist Seal
SEAL
1877
4
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009
n._ 1VE

MECKLENBURG COUNTY
Land Use and Environmental Services Agency
Solid Waste Services
January 14, 2021
Jaclynne Drummond
North Carolina Department of Environment
and Natural Resources
Division of Waste Management - Solid Waste Section
2090 US Highway 70
Swannanoa, NC 28778
Subject: Water Quality Monitoring Report December 2020
Harrisburg Road Landfill, Permit 60-01
Dear Ms. Drummond:
Mecklenburg County conducted semi-annual water quality monitoring at the closed
Harrisburg Road Landfill December 8, 2020, in accordance with the approved revised
sample and analysis plan dated May 11, 2004. Samples were collected from seven
monitoring wells (HB W-12B, HB W-14, HB W-17B, HB W-20, HB W-21, HB W-22 and
background well HBW-28) and three surface -water sampling locations (H132006,
HB2008 and, HB2010). The water supply well MAINTE has been disconnected from
service and will be abandoned by the end of January. A well abandonment record will be
submitted once the abandonment is complete. Public water is now connected to the
Maintenance Shop. Laboratory analytical data, field -measured data, and a table of results
exceeding water quality standards along with a preliminary explanation of the cause and
significance are included on the electronic data deliverable (EDD) submittal.
The EDD containing the monitoring data are labeled to reflect the units that are used for
reporting. Detection levels and applicable standards have been included for all sampling
locations. Surface water standards listed are the water quality standards established for
freshwater classification for aquatic life as outlined in 15A NCAC 213 "Classification and
Water Quality Standards Applicable to Surface Waters of North Carolina". Groundwater
standards listed are the standards outlined in 15A NCAC 2L "Classification of Water
Quality Standards applicable to the Groundwaters of North Carolina". If the sample is
reported in parts per billion, then the standard is also reported in parts per billion.
PEOPLE • PRIDE • PROGRESS • PARTNERSHIP
2145 Suttle Ave • Charlotte, NC 28208-5237 • [phone] • FAX [phone]
www.wipeoutwastexom

Page 2
Surface -water samples:
Barium was detected in FIB 2006, FIB 2008 and FIB 2010 at 24.2 ppb, 19.9 ppb and 47.8
ppb, respectively. Antimony was detected in HB2008 at 5.5 ppb. No other analytes were
detected in the surface water samples. Field -measured parameters for surface -water
samples were within the range of established standards and are summarized in the table
below.
Location
Temperature
PH
Specific
Conductivity
Dissolved
Oxygen
HB2006
8.5° C
6.4
0.156 ms/cm
16.64 mg/l
HB2008
8.70 C
6.5
0.152 ms/cm
12.22 mg/1
HB2010
6.5° C
6.5
0.263 ms/cm
19.12 mg/l
Groundwater samples:
Multiple metals were detected above 21, standards. The table below summarizes metals
detections in groundwater samples.
Well ID
Ba
ug/l
Be
ug/l
Cd
ug/l
Cr
ug/l
Co
ug/l
Cu
ug/l
Ni
ug/l
Pb
ug/1
Th
ug/l
Vn
ug/1
Zn
ug/l
HBW 12B
28.1
-----
-----
-----
------
-----
-----
-----
------
-----
-----
HB W 14
123
-----
-----
-----
6.2
66.8
-----
-----
------
31.2
18.2
HBW17B
71.8
-----
------
-----
20.9
50.1
-----
-----
0.11
-----
16.3
HBW-20
12.5
-----
-----
-----
-----
5.7
-----
-----
------
13.4
-----
HB W-21
5.6
-----
-----
-----
-----
-----
-----
-----
------
-----
-----
HB W-22
41.2
-----
-----
20.5
-----
-----
5.3
-----
-----
-----
-----
HBW-28*
104
-----
-----
6.6
125
42.5
14.7
-----
------
13.0
10.8
2L Std. ug/l
700
4
2.0
10
1
1,000
100
15
F-012-7
0.3
1,000
Note: Bolded results exceed 2L Standard, *Background Well
The following volatile organic compounds ("VOCs") were detected in the sample
collected from well HBW-17B:
VOC
Sample Result u /l
2L Standard u /1
Benzene
9.0
1
Tetra chloroeth lene
31.6
0.7
Trichloroeth lene
24.4
2.8
1,1-Dichloroethane
6.6
6
1,2-Dichloro ro ane
9.8
0.6
cis-1,2 Dichloroethene
124
70
trans-1,2 Dichloroethene
1.4
100
1,4-Dichlorobenzene
1.1
6
X lenes total
12.3
500
Vinyl Chloride
1.7
0.03
Note: Bolded results exceed 2L Standard

Page 3
The pH was measured to be more acidic than the standard in the samples collected from
HBW-12B, HBW14, HBW17B, HBW-20, HBW-21, HBW-22 and background
monitoring well HBW-28. Field -measured parameters for groundwater samples are
summarized in the following table:
Location
Temperature
pH
Conductivity
HBW12B
15.7 °C
5.3
0.377 ms/cm
HBW14
15.7 °C
6.2
0.208 ms/cm
HBW17B
16.0 °C
4.5
0.067 ms/cm
HBW-20
16.0 °C
5.9
0.150 ms/cm
HBW-21
15.5 °C
5.7
0.193 ms/cm
HBW-22
16.4 °C
5.4
0.074 ms/cm
*HBW-28
16.3 °C
5.1
0.080 ms/cm
Note: Bolded results are outside of the 6.5 to 8.5 S.U. range 2L Standard
*Background Well
Please call me at [phone], if you have any questions concerning this report.
p0pp0°9°0 Sincerely,
SEAL
� Amber R. Grzymski, P.
.� ��®� Project Manager
D�Q�/In_..n00af" LUESA Solid Waste Services

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® POTABLE MONITORING
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SURFACE -WATER SAMPLING LOCATIONS
® WATER SUPPLY WELLS FOR IRRIGATION PURPOSES
1998 1982
!/ 11146 GROUNDWATER SURFACE ELEVATION ITT) 11MA1)
APPROXIMATE WASTE BOUNDARY AN'DDATES OF PLACEMENT
! s\ 00�.\\ U\- o ❑ I O GROUNDWATER SURFACE(ESTIMATED WHEREDASHED)
01 �OGENERALIZED GROUNDWATER FLOW DIRECTION PLANIMETRICFERCELINECAPTUREDATPHUTOSCALEI'-IOW
SURFACE WATER CAPTURED AT PHOTOSCALE V-1000'
CI D®MW S /-/ TAX PARCELBOUNDARY
- o NOTE$-
\ - I 1. ALL ON SIE WELL LOCATIONS WERE SURVEYED BY FDL ASSOC
• /X/ ° q s Q 2 GROUNDWATER DATA REFLECTS PUMPING CONDITIONS FROM WATER
SUP LY WELLS IN THE AREA L 26
3, SURFACE WATER SAMPLING SS IT `OCATED USING CPS- SEPTEMBER3,2002
4. GROUNDWAERSURFACECONTOURE BASED ON MME MAP DATED IUNE4,2001
PRE-1998 °w 5. HBW-]%RENAMED FROM MW26
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Op0OOO Q0 0 SOURCE'. MECKLENBURG COUNTY GIS AND CPS SURVEY FOR WELL LOCATIONS
o0 0.y: AND SBME MAP DATED JUNE 4 2001
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- CHARLOTTE, NORTH
300' •µS.GREGORY
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N0'MAPIGIS ` 10)15102 `"FGURE1

Landfill Gas Monitoring Data Form
Facility Name: Harrisburg Road Landfill Pennit Number: 60-01
Date of Sampling: =12/11/2020 NC Landfill Rule (.0500 or .1600): .0500
Name and Position of Sample Collector: David E. Coleman, Environmental Specialist
Type and Serial Number of Gas Meter: Gem 2000 #GM 13774
Calibration Date of Gas Meter: 8/5//2020 Date and Time of Field Calibration: 12/ 11/2020 14:00
Type of Field Calibration Gas (15/15 or 35/50): �35/50
Expiration Date of Field Calibration Gas Canister: uADril 2025
Pump Rate of Gas Meter: �120 Seconds_ Ambient Air Temperature: 62 Degrees
Barometric Pressure: 29.29 General Weather Conditions: Partly Sunny, SSW3
Sample ID
Time
% LEL
% CH4
% CO2
% 02
Comments
MP-1
13:27
>100
60.5
39.4
0
Methane Extraction System
MP-2
13:35
>100
59.0
30.8
2.4
Methane Extraction System
MP-3
13:41
2
0.1
0.3
20.9
Methane Extraction System
MP-4
13:44
>100
29.2
20.8
10.6
Methane Extraction System
MP-5
14:53
0
0
3.4
17.0
MP-6
14:59
0
0
5.0
12.9
MP-7
15:05
0
0
7.3
13.5
MP-8
15:17
0
0
8.0
13.4
MP-9A
15:23
0
0
1.3
19.8
MP-9B
15:28
0
0
5.9
13.8
MP-11
14:17
>100
30.5
21.7
6.3
MP-12
14:25
0
0
10.6
10.1
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and
attachments are true and correct. I am aware that there are significant penalties for making any false
statement, representation, or certification including the possibility of a fine and imprisonment.
r -_'� ���-�" �ny'e9►l2c��NJ'r� �.l'rf�L 2G,fac,osJ1'
SIGNATURE TITLE

60-01 Harrisburg Rd Landfill Methane Wells
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leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
January 11, 2021
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510382
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on December 08, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
This revision was issued on 01/11/21 to correct the title of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510382
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510382
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92510382001 HBW-28
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
52
PASI-C
92510382002 HBW-20
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
52
PASI-C
92510382003 HBW-14
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
52
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510382
Sample: HBW-28 Lab ID: 92510382001 Collected: 12/08/20 10:05 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:07
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:07
7440-38-2
Barium
104
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:07
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/16/20 01:12
12/17/20 11:07
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/16/20 01:12
12/17/20 11:07
7440-43-9
Chromium
6.6
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:07
7440-47-3
Cobalt
125
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:07
7440-48-4
Copper
42.5
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:07
7440-50-8
Lead
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:07
7439-92-1
Nickel
14.7
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:07
7440-02-0
Selenium
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:07
7782-49-2
Silver
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:07
7440-22-4
Thallium
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:07
7440-28-0
Vanadium
13.0
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:07
7440-62-2
Zinc
10.8
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:07
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
12/24/20 00:56
12/29/20 22:45
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/12/20 08:11
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/12/20 08:11
107-13-1
Benzene
ND
ug/L
1.0
1
12/12/20 08:11
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/12/20 08:11
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/12/20 08:11
75-27-4
Bromoform
ND
ug/L
1.0
1
12/12/20 08:11
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/12/20 08:11
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/12/20 08:11
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/12/20 08:11
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/12/20 08:11
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/12/20 08:11
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/12/20 08:11
75-00-3
Chloroform
ND
ug/L
5.0
1
12/12/20 08:11
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/12/20 08:11
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
12/12/20 08:11
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/12/20 08:11
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/12/20 08:11
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/12/20 08:11
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 08:11
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 08:11
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/12/20 08:11
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/12/20 08:11
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/12/20 08:11
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
v2
v1
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510382
Sample: HBW-28 Lab ID: 92510382001 Collected: 12/08/20 10:05 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/12/20 08:11
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 08:11
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 08:11
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/12/20 08:11
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 08:11
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 08:11
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/12/20 08:11
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/12/20 08:11
591-78-6
lodomethane
ND
ug/L
20.0
1
12/12/20 08:11
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/12/20 08:11
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/12/20 08:11
108-10-1
Styrene
ND
ug/L
1.0
1
12/12/20 08:11
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 08:11
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 08:11
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/12/20 08:11
127-18-4
Toluene
ND
ug/L
1.0
1
12/12/20 08:11
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/12/20 08:11
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/12/20 08:11
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/12/20 08:11
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/12/20 08:11
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/12/20 08:11
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/12/20 08:11
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/12/20 08:11
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/12/20 08:11
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/12/20 08:11
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/12/20 08:11
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
12/12/20 08:11
460-00-4
1,2-Dichloroethane-d4 (S)
100
%
70-130
1
12/12/20 08:11
17060-07-0
Toluene-d8 (S)
105
%
70-130
1
12/12/20 08:11
2037-26-5
Date:01/11/2021 04:51 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510382
Sample: HBW-20 Lab ID: 92510382002 Collected: 12/08/20 10:40 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:10
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:10
7440-38-2
Barium
12.5
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:10
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/16/20 01:12
12/17/20 11:10
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/16/20 01:12
12/17/20 11:10
7440-43-9
Chromium
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:10
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:10
7440-48-4
Copper
5.7
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:10
7440-50-8
Lead
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:10
7439-92-1
Nickel
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:10
7440-02-0
Selenium
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:10
7782-49-2
Silver
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:10
7440-22-4
Thallium
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:10
7440-28-0
Vanadium
13.4
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:10
7440-62-2
Zinc
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:10
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
12/24/20 00:56
12/29/20 22:49
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/12/20 08:29
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/12/20 08:29
107-13-1
Benzene
ND
ug/L
1.0
1
12/12/20 08:29
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/12/20 08:29
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/12/20 08:29
75-27-4
Bromoform
ND
ug/L
1.0
1
12/12/20 08:29
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/12/20 08:29
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/12/20 08:29
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/12/20 08:29
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/12/20 08:29
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/12/20 08:29
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/12/20 08:29
75-00-3
Chloroform
ND
ug/L
5.0
1
12/12/20 08:29
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/12/20 08:29
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
12/12/20 08:29
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/12/20 08:29
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/12/20 08:29
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/12/20 08:29
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 08:29
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 08:29
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/12/20 08:29
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/12/20 08:29
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/12/20 08:29
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
v2
v1
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510382
Sample: HBW-20 Lab ID: 92510382002 Collected: 12/08/20 10:40 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/12/20 08:29
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 08:29
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 08:29
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/12/20 08:29
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 08:29
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 08:29
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/12/20 08:29
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/12/20 08:29
591-78-6
lodomethane
ND
ug/L
20.0
1
12/12/20 08:29
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/12/20 08:29
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/12/20 08:29
108-10-1
Styrene
ND
ug/L
1.0
1
12/12/20 08:29
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 08:29
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 08:29
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/12/20 08:29
127-18-4
Toluene
ND
ug/L
1.0
1
12/12/20 08:29
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/12/20 08:29
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/12/20 08:29
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/12/20 08:29
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/12/20 08:29
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/12/20 08:29
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/12/20 08:29
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/12/20 08:29
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/12/20 08:29
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/12/20 08:29
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/12/20 08:29
95-47-6
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
12/12/20 08:29
460-00-4
1,2-Dichloroethane-d4 (S)
103
%
70-130
1
12/12/20 08:29
17060-07-0
Toluene-d8 (S)
102
%
70-130
1
12/12/20 08:29
2037-26-5
Date:01/11/2021 04:51 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510382
Sample: HBW-14 Lab ID: 92510382003 Collected: 12/08/20 11:05 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:14
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:14
7440-38-2
Barium
123
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:14
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/16/20 01:12
12/17/20 11:14
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/16/20 01:12
12/17/20 11:14
7440-43-9
Chromium
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:14
7440-47-3
Cobalt
6.2
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:14
7440-48-4
Copper
66.8
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:14
7440-50-8
Lead
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:14
7439-92-1
Nickel
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:14
7440-02-0
Selenium
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:14
7782-49-2
Silver
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:14
7440-22-4
Thallium
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:14
7440-28-0
Vanadium
31.2
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:14
7440-62-2
Zinc
18.2
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:14
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
12/24/20 00:56
12/29/20 22:53
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/12/20 08:48
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/12/20 08:48
107-13-1
Benzene
ND
ug/L
1.0
1
12/12/20 08:48
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/12/20 08:48
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/12/20 08:48
75-27-4
Bromoform
ND
ug/L
1.0
1
12/12/20 08:48
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/12/20 08:48
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/12/20 08:48
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/12/20 08:48
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/12/20 08:48
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/12/20 08:48
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/12/20 08:48
75-00-3
Chloroform
ND
ug/L
5.0
1
12/12/20 08:48
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/12/20 08:48
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
12/12/20 08:48
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/12/20 08:48
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/12/20 08:48
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/12/20 08:48
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 08:48
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 08:48
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/12/20 08:48
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/12/20 08:48
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/12/20 08:48
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
v2
v1
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510382
Sample: HBW-14 Lab ID: 92510382003 Collected: 12/08/20 11:05 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/12/20 08:48
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 08:48
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 08:48
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/12/20 08:48
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 08:48
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 08:48
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/12/20 08:48
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/12/20 08:48
591-78-6
lodomethane
ND
ug/L
20.0
1
12/12/20 08:48
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/12/20 08:48
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/12/20 08:48
108-10-1
Styrene
ND
ug/L
1.0
1
12/12/20 08:48
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 08:48
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 08:48
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/12/20 08:48
127-18-4
Toluene
ND
ug/L
1.0
1
12/12/20 08:48
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/12/20 08:48
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/12/20 08:48
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/12/20 08:48
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/12/20 08:48
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/12/20 08:48
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/12/20 08:48
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/12/20 08:48
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/12/20 08:48
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/12/20 08:48
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/12/20 08:48
95-47-6
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
12/12/20 08:48
460-00-4
1,2-Dichloroethane-d4 (S)
101
%
70-130
1
12/12/20 08:48
17060-07-0
Toluene-d8 (S)
102
%
70-130
1
12/12/20 08:48
2037-26-5
Date:01/11/2021 04:51 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510382
QC Batch: 587141 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92510382001, 92510382002, 92510382003
METHOD BLANK: 3103223 Matrix: Water
Associated Lab Samples: 92510382001, 92510382002, 92510382003
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
5.0
12/17/20 10:41
10.0
12/17/20 10:41
5.0
12/17/20 10:41
1.0
12/17/20 10:41
1.0
12/17/20 10:41
5.0
12/17/20 10:41
5.0
12/17/20 10:41
5.0
12/17/20 10:41
5.0
12/17/20 10:41
5.0
12/17/20 10:41
10.0
12/17/20 10:41
5.0
12/17/20 10:41
10.0
12/17/20 10:41
5.0
12/17/20 10:41
10.0
12/17/20 10:41
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3103224
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
514
103
80-120
Arsenic
ug/L
500
513
103
80-120
Barium
ug/L
500
522
104
80-120
Beryllium
ug/L
500
522
104
80-120
Cadmium
ug/L
500
513
103
80-120
Chromium
ug/L
500
514
103
80-120
Cobalt
ug/L
500
522
104
80-120
Copper
ug/L
500
527
105
80-120
Lead
ug/L
500
517
103
80-120
Nickel
ug/L
500
514
103
80-120
Selenium
ug/L
500
510
102
80-120
Silver
ug/L
250
251
100
80-120
Thallium
ug/L
500
504
101
80-120
Vanadium
ug/L
500
526
105
80-120
Zinc
ug/L
500
504
101
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:51 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 21

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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QUALITY CONTROL DATA
Project:
Pace Project No.:
Harrisburg Rd LF-Revised Report
92510382
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3103225
3103226
MS
MSD
92509420001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
531
525
106
105
75-125
1
Arsenic
ug/L
ND
500
500
517
516
103
103
75-125
0
Barium
ug/L
75.8
500
500
600
594
105
104
75-125
1
Beryllium
ug/L
ND
500
500
533
526
107
105
75-125
2
Cadmium
ug/L
ND
500
500
515
510
103
102
75-125
1
Chromium
ug/L
ND
500
500
516
511
103
102
75-125
1
Cobalt
ug/L
13.0
500
500
535
528
104
103
75-125
1
Copper
ug/L
15.7
500
500
540
534
105
104
75-125
1
Lead
ug/L
ND
500
500
517
507
103
101
75-125
2
Nickel
ug/L
ND
500
500
520
514
103
102
75-125
1
Selenium
ug/L
ND
500
500
537
542
107
108
75-125
1
Silver
ug/L
ND
250
250
260
257
104
103
75-125
1
Thallium
ug/L
ND
500
500
499
504
100
101
75-125
1
Vanadium
ug/L
ND
500
500
528
522
106
104
75-125
1
Zinc
ug/L
39.2
500
500
549
545
102
101
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 21

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510382
QC Batch: 589260 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92510382001, 92510382002, 92510382003
METHOD BLANK: 3112841
Matrix:
Water
Associated Lab Samples: 92510382001, 92510382002, 92510382003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
0.10
12/29/20 22:37
LABORATORY CONTROL SAMPLE:
3112842
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
10
10.5
105 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3112843 3112844
MS MSD
92511882002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 10 10 10.1 10 101 100 75-125 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:51 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 21

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510382
QC Batch: 586490 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92510382001, 92510382002, 92510382003
METHOD BLANK: 3099796 Matrix:
Associated Lab Samples: 92510382001, 92510382002, 92510382003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
12/12/20 04:49
1,1,1-Trichloroethane
ug/L
ND
1.0
12/12/20 04:49
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/12/20 04:49
1,1,2-Trichloroethane
ug/L
ND
1.0
12/12/20 04:49
1,1-Dichloroethane
ug/L
ND
1.0
12/12/20 04:49
1,1-Dichloroethene
ug/L
ND
1.0
12/12/20 04:49
1,2,3-Trichloropropane
ug/L
ND
1.0
12/12/20 04:49
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
12/12/20 04:49
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/12/20 04:49
1,2-Dichlorobenzene
ug/L
ND
1.0
12/12/20 04:49
1,2-Dichloroethane
ug/L
ND
1.0
12/12/20 04:49
1,2-Dichloropropane
ug/L
ND
1.0
12/12/20 04:49
1,4-Dichlorobenzene
ug/L
ND
1.0
12/12/20 04:49
2-Butanone (MEK)
ug/L
ND
5.0
12/12/20 04:49
2-Hexanone
ug/L
ND
5.0
12/12/20 04:49
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/12/20 04:49
Acetone
ug/L
ND
25.0
12/12/20 04:49
Acrylonitrile
ug/L
ND
10.0
12/12/20 04:49
Benzene
ug/L
ND
1.0
12/12/20 04:49
Bromochloromethane
ug/L
ND
1.0
12/12/20 04:49
Bromodichloromethane
ug/L
ND
1.0
12/12/20 04:49
Bromoform
ug/L
ND
1.0
12/12/20 04:49
Bromomethane
ug/L
ND
2.0
12/12/20 04:49
Carbon disulfide
ug/L
ND
2.0
12/12/20 04:49
Carbon tetrachloride
ug/L
ND
1.0
12/12/20 04:49
Chlorobenzene
ug/L
ND
1.0
12/12/20 04:49
Chloroethane
ug/L
ND
1.0
12/12/20 04:49
Chloroform
ug/L
ND
5.0
12/12/20 04:49
Chloromethane
ug/L
ND
1.0
12/12/20 04:49
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/12/20 04:49
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/12/20 04:49
Dibromochloromethane
ug/L
ND
1.0
12/12/20 04:49
Dibromomethane
ug/L
ND
1.0
12/12/20 04:49
Ethylbenzene
ug/L
ND
1.0
12/12/20 04:49
lodomethane
ug/L
ND
20.0
12/12/20 04:49
m&p-Xylene
ug/L
ND
2.0
12/12/20 04:49
Methylene Chloride
ug/L
ND
5.0
12/12/20 04:49
o-Xylene
ug/L
ND
1.0
12/12/20 04:49
Styrene
ug/L
ND
1.0
12/12/20 04:49
Tetrachloroethene
ug/L
ND
1.0
12/12/20 04:49
v1
v2
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510382
METHOD BLANK: 3099796 Matrix:
Associated Lab Samples: 92510382001, 92510382002, 92510382003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed Qualifiers
Toluene
ug/L
ND
1.0
12/12/20 04:49
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/12/20 04:49
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/12/20 04:49
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
12/12/20 04:49
Trichloroethene
ug/L
ND
1.0
12/12/20 04:49
Trichlorofluoromethane
ug/L
ND
1.0
12/12/20 04:49
Vinyl acetate
ug/L
ND
2.0
12/12/20 04:49
Vinyl chloride
ug/L
ND
1.0
12/12/20 04:49
Xylene (Total)
ug/L
ND
1.0
12/12/20 04:49
1,2-Dichloroethane-d4 (S)
%
99
70-130
12/12/20 04:49
4-Bromofluorobenzene (S)
%
98
70-130
12/12/20 04:49
Toluene-d8 (S)
%
100
70-130
12/12/20 04:49
LABORATORY CONTROL SAMPLE:
Parameter
3099797
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
49.6
99
70-130
1,1,1-Trichloroethane
ug/L
50
44.1
88
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.8
102
70-130
1,1,2-Trichloroethane
ug/L
50
48.5
97
70-130
1,1-Dichloroethane
ug/L
50
42.3
85
70-130
1,1-Dichloroethene
ug/L
50
44.0
88
70-132
1,2,3-Trichloropropane
ug/L
50
48.2
96
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
53.3
107
70-132
1,2-Dibromoethane (EDB)
ug/L
50
51.8
104
70-130
1,2-Dichlorobenzene
ug/L
50
48.9
98
70-130
1,2-Dichloroethane
ug/L
50
44.5
89
70-130
1,2-Dichloropropane
ug/L
50
45.0
90
70-130
1,4-Dichlorobenzene
ug/L
50
47.7
95
70-130 v1
2-Butanone (MEK)
ug/L
100
98.6
99
70-133
2-Hexanone
ug/L
100
110
110
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
93.7
94
70-130
Acetone
ug/L
100
107
107
70-144
Acrylonitrile
ug/L
250
229
92
70-130
Benzene
ug/L
50
42.9
86
70-130
Bromochloromethane
ug/L
50
42.5
85
70-130
Bromodichloromethane
ug/L
50
45.2
90
70-130
Bromoform
ug/L
50
52.1
104
70-131
Bromomethane
ug/L
50
41.5
83
30-177 v2
Carbon disulfide
ug/L
50
42.5
85
70-133
Carbon tetrachloride
ug/L
50
47.5
95
70-130
Chlorobenzene
ug/L
50
47.4
95
70-130
Chloroethane
ug/L
50
43.2
86
46-131
Chloroform
ug/L
50
39.6
79
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 21

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510382
LABORATORY CONTROL SAMPLE:
Parameter
3099797
Units
Spike
Conc.
LCS LCS
Result % Rec
Chloromethane
ug/L
50
36.7
cis-1,2-Dichloroethene
ug/L
50
41.3
cis-1,3-Dichloropropene
ug/L
50
46.1
Dibromochloromethane
ug/L
50
50.9
Dibromomethane
ug/L
50
48.5
Ethylbenzene
ug/L
50
46.9
lodomethane
ug/L
100
82.9
m&p-Xylene
ug/L
100
94.9
Methylene Chloride
ug/L
50
42.5
o-Xylene
ug/L
50
47.8
Styrene
ug/L
50
49.8
Tetrachloroethene
ug/L
50
48.3
Toluene
ug/L
50
43.5
trans-1,2-Dichloroethene
ug/L
50
42.6
trans- 1,3-Dichloropropene
ug/L
50
48.0
trans-1,4-Dichloro-2-butene
ug/L
50
56.9
Trichloroethene
ug/L
50
46.0
Trichlorofluoromethane
ug/L
50
41.7
Vinyl acetate
ug/L
100
99.2
Vinyl chloride
ug/L
50
38.2
Xylene (Total)
ug/L
150
143
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
% Rec
Limits Qualifiers
73
49-130 v2
83
70-130
92
70-130
102
70-130
97
70-130
94
70-130
83
47-140
95
70-130
85
68-130
96
70-130
100
70-130
97
70-130
87
70-130
85
70-130
96
70-130
114
25-200
92
70-130
83
61-130
99
70-140
76
59-142
95
70-130
92
70-130
102
70-130
96
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3099798
MS
92510341001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3099799
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.9
19.2
110
96
70-135
14
1,1,1-Trichloroethane
ug/L
ND
20
20
22.0
20.6
110
103
70-148
7
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
20.3
18.7
102
93
70-131
8
1,1,2-Trichloroethane
ug/L
ND
20
20
20.8
19.2
104
96
70-136
8
1,1-Dichloroethane
ug/L
ND
20
20
22.0
19.9
110
99
70-147
10
1,1-Dichloroethene
ug/L
ND
20
20
22.7
20.9
114
104
70-158
9
1,2,3-Trichloropropane
ug/L
ND
20
20
21.6
19.0
108
95
67-137
13
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
21.6
18.7
108
93
69-136
15
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.3
19.4
112
97
70-137
14
1,2-Dichlorobenzene
ug/L
ND
20
20
21.2
18.8
106
94
70-133
12
1,2-Dichloroethane
ug/L
ND
20
20
20.9
19.6
105
98
67-138
7
1,2-Dichloropropane
ug/L
ND
20
20
22.2
20.3
111
101
70-138
9
1,4-Dichlorobenzene
ug/L
ND
20
20
20.5
18.9
103
95
70-133
8
2-Butanone (MEK)
ug/L
ND
40
40
42.9
40.3
107
101
61-147
6
2-Hexanone
ug/L
ND
40
40
43.5
39.4
109
98
67-139
10
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
42.6
38.7
107
97
67-136
10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:51 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 21

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510382
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3099798
MS
92510341001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3099799
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
46.8
42.7
117
107
55-159
9
Acrylonitrile
ug/L
ND
100
100
106
100
106
100
68-140
6
Benzene
ug/L
ND
20
20
21.7
19.7
109
99
67-150
10
Bromochloromethane
ug/L
ND
20
20
22.9
21.4
114
107
70-146
7
Bromodichloromethane
ug/L
ND
20
20
20.5
18.2
103
91
70-138
12
Bromoform
ug/L
ND
20
20
18.8
16.6
94
83
57-138
13
Bromomethane
ug/L
ND
20
20
23.9
23.1
120
116
10-200
31K
Carbon disulfide
ug/L
ND
20
20
21.4
19.6
107
98
70-152
9
Carbon tetrachloride
ug/L
ND
20
20
23.0
20.7
115
104
70-147
10
Chlorobenzene
ug/L
ND
20
20
21.5
18.9
108
95
70-137
13
Chloroethane
ug/L
ND
20
20
21.0
18.2
105
91
51-166
14
Chloroform
ug/L
ND
20
20
21.5
20.3
107
101
70-144
6
Chloromethane
ug/L
ND
20
20
20.4
19.0
102
95
24-161
7
cis-1,2-Dichloroethene
ug/L
ND
20
20
21.2
19.6
106
98
67-148
8
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.2
19.4
106
97
70-142
9
Dibromochloromethane
ug/L
ND
20
20
20.4
18.4
102
92
68-138
10
Dibromomethane
ug/L
ND
20
20
21.5
19.8
108
99
70-134
8
Ethylbenzene
ug/L
ND
20
20
20.8
18.3
104
91
68-143
13
lodomethane
ug/L
ND
40
40
43.6
41.6
109
104
20-161
5
m&p-Xylene
ug/L
ND
40
40
42.6
38.1
107
95
53-157
11
Methylene Chloride
ug/L
ND
20
20
21.5
19.5
107
98
64-148
9
o-Xylene
ug/L
ND
20
20
21.5
18.8
107
94
68-143
13
Styrene
ug/L
ND
20
20
20.1
17.5
100
88
70-136
14
Tetrachloroethene
ug/L
ND
20
20
20.1
18.1
100
90
70-139
11
Toluene
ug/L
ND
20
20
21.8
19.7
109
98
47-157
10
trans-1,2-Dichloroethene
ug/L
ND
20
20
21.4
19.4
107
97
70-149
10
trans- 1,3-Dichloropropene
ug/L
ND
20
20
21.2
19.0
106
95
70-138
11
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
18.5
17.4
93
87
31-145
6
Trichloroethene
ug/L
ND
20
20
21.7
18.9
109
95
70-149
14
Trichlorofluoromethane
ug/L
ND
20
20
20.1
19.0
101
95
61-154
6
Vinyl acetate
ug/L
ND
40
40
34.7
30.8
87
77
48-156
12
Vinyl chloride
ug/L
ND
20
20
19.1
18.0
95
90
55-172
6
Xylene (Total)
ug/L
ND
60
60
64.1
56.9
107
95
66-145
12
1,2-Dichloroethane-d4 (S)
%
100
102
70-130
4-Bromofluorobenzene (S)
%
101
99
70-130
Toluene-d8(S)
%
99
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:51 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 21

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510382
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510382
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92510382001
HBW-28
EPA 3010A
587141
EPA 6010D
587292
92510382002
HBW-20
EPA 3010A
587141
EPA 6010D
587292
92510382003
HBW-14
EPA 3010A
587141
EPA 6010D
587292
92510382001
HBW-28
EPA 3010A
589260
EPA6020B
589269
92510382002
HBW-20
EPA 3010A
589260
EPA6020B
589269
92510382003
HBW-14
EPA 3010A
589260
EPA6020B
589269
92510382001
HBW-28
EPA 8260D
586490
92510382002
HBW-20
EPA 8260D
586490
92510382003
HBW-14
EPA 8260D
586490
Date:01/11/2021 04:51 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 21

Document Name: Document Revised: October 28, ZU20
Sample Condition Upon Receipt(SCUR) Page 1 of 2
�2eAnalytieal, Document No.: Issuing Authority:
F-CAR-CS-033-Rev.07 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville a- Raleigh❑ Mechanicsville❑ Atlanta[] Kernersville❑
Sample Condition Client Name: WO� � 9 (��� � O �J]��
.. �i . 1 � b
L Project #:
Holrobdb
Gautier: Fed Ex UPS ❑ P5
❑ Commercial []Pace ❑Other; 92510382 III III111
0
Packing Material; ❑Bubble Wrap ❑Bubble Bags ONone ❑ Other
L.
Date/initials Person Examining Contents:_ t( {A�,[�
Biological Tissue Frozen?
❑Yes ❑No ❑N/A
T ermometer. "Wet ❑Blue ❑None
Gun 10: 92TO64 Type of Ice: `
(j �} Correction Factor:
Cooler Temp: ^7 Add/Subtract (°C) -0.1 Temp should be above freezing to 6'C
r j ❑Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected (°C): has begun
USDA Regulated Sail N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source {internationally,
Myer. MNn includine Hawaii and Puerto Rico)? FlYes FlNo
Comments/Dlscrepan cy:
Chain of Custody Present?
1KYes
❑No
❑N/A
1.
Samples Arrived within Hold Time?
'dyes
❑No
N/A
2.
Short Hold Time Analysis (<72 hr.)?
Yes
No
❑NIA
3.
Rush Turn Around Time Requested?
❑Yes
T2Ca
❑,N/A
4.
Sufficient Volume?
Yes
No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
(9Yes
2LYes
❑No
❑No
❑N/A
N/A
6,
Containers Intact?
es
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑Na
LKNIA
8.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
` __�"``Yes
, �
�
❑No
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
No
N/A
10,
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
Yes
179vo
❑No
El N/A
EIN/A
11.
COMMENTS/SAMPLE DISCREPANCY Field Data Required? Des [:]No
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Date/Time:
Lot ID of split containers:
Date:
Project Manager SRF Review:
Date:
Page 19 of 21

Document Name:
Sample Condition Upon Recei
AnaVical R Document No.:
F-CAR-CS-033-Rev.07
Document Revised: October 18, 1U1U
Page 2 of 2
Issuing Authority:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptlons: VOA, Coliform, TOC, oil and Grease, DRO/8015 {water) DOC, LLHg
"Bottom half of box is to list number of bottles
Project # Wog : 92510382
PM: MWB Due Date: 12/22/20
CLIENT: 92-MECK CO
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot d
Note: Whenever there is a discrepancy artecting Nortn taranna compnance 5ampiK>, a Lupy vi w1,. — 5e11L w VIC Imul «i 1-v o • • •�;
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 20 of 21

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Page 21 of 21

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
January 11, 2021
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510386
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on December 08, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
This revision was issued on 01/11/21 to correct the title of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510386
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510386
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92510386001 HBW-21
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
52
PASI-C
92510386002 HBW-22
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
52
PASI-C
92510386003 HBW-12B
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
52
PASI-C
92510386004 HBW-17B
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
52
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510386
Sample: HBW-21 Lab ID: 92510386001 Collected: 12/08/20 12:05 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:20
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:20
7440-38-2
Barium
5.6
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:20
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/16/20 01:12
12/17/20 11:20
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/16/20 01:12
12/17/20 11:20
7440-43-9
Chromium
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:20
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:20
7440-48-4
Copper
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:20
7440-50-8
Lead
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:20
7439-92-1
Nickel
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:20
7440-02-0
Selenium
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:20
7782-49-2
Silver
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:20
7440-22-4
Thallium
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:20
7440-28-0
Vanadium
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:20
7440-62-2
Zinc
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:20
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
12/24/20 00:56
12/29/20 22:57
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/12/20 09:06
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/12/20 09:06
107-13-1
Benzene
ND
ug/L
1.0
1
12/12/20 09:06
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/12/20 09:06
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/12/20 09:06
75-27-4
Bromoform
ND
ug/L
1.0
1
12/12/20 09:06
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/12/20 09:06
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/12/20 09:06
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/12/20 09:06
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/12/20 09:06
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/12/20 09:06
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/12/20 09:06
75-00-3
Chloroform
ND
ug/L
5.0
1
12/12/20 09:06
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/12/20 09:06
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
12/12/20 09:06
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/12/20 09:06
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/12/20 09:06
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/12/20 09:06
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 09:06
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 09:06
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/12/20 09:06
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/12/20 09:06
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/12/20 09:06
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
v2
v1
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510386
Sample: HBW-21 Lab ID: 92510386001 Collected: 12/08/20 12:05 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/12/20 09:06
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 09:06
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 09:06
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/12/20 09:06
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 09:06
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 09:06
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/12/20 09:06
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/12/20 09:06
591-78-6
lodomethane
ND
ug/L
20.0
1
12/12/20 09:06
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/12/20 09:06
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/12/20 09:06
108-10-1
Styrene
ND
ug/L
1.0
1
12/12/20 09:06
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 09:06
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 09:06
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/12/20 09:06
127-18-4
Toluene
ND
ug/L
1.0
1
12/12/20 09:06
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/12/20 09:06
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/12/20 09:06
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/12/20 09:06
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/12/20 09:06
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/12/20 09:06
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/12/20 09:06
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/12/20 09:06
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/12/20 09:06
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/12/20 09:06
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/12/20 09:06
95-47-6
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
12/12/20 09:06
460-00-4
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
12/12/20 09:06
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
12/12/20 09:06
2037-26-5
Date: 01/11/2021 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510386
Sample: HBW-22 Lab ID: 92510386002 Collected: 12/08/20 11:50 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:23
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:23
7440-38-2
Barium
41.2
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:23
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/16/20 01:12
12/17/20 11:23
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/16/20 01:12
12/17/20 11:23
7440-43-9
Chromium
20.5
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:23
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:23
7440-48-4
Copper
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:23
7440-50-8
Lead
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:23
7439-92-1
Nickel
5.3
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:23
7440-02-0
Selenium
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:23
7782-49-2
Silver
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:23
7440-22-4
Thallium
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:23
7440-28-0
Vanadium
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:23
7440-62-2
Zinc
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:23
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
12/24/20 00:56
12/29/20 23:01
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/12/20 09:25
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/12/20 09:25
107-13-1
Benzene
ND
ug/L
1.0
1
12/12/20 09:25
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/12/20 09:25
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/12/20 09:25
75-27-4
Bromoform
ND
ug/L
1.0
1
12/12/20 09:25
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/12/20 09:25
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/12/20 09:25
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/12/20 09:25
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/12/20 09:25
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/12/20 09:25
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/12/20 09:25
75-00-3
Chloroform
ND
ug/L
5.0
1
12/12/20 09:25
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/12/20 09:25
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
12/12/20 09:25
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/12/20 09:25
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/12/20 09:25
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/12/20 09:25
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 09:25
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 09:25
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/12/20 09:25
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/12/20 09:25
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/12/20 09:25
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
v2
v1
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510386
Sample: HBW-22 Lab ID: 92510386002 Collected: 12/08/20 11:50 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/12/20 09:25
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 09:25
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 09:25
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/12/20 09:25
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 09:25
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 09:25
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/12/20 09:25
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/12/20 09:25
591-78-6
lodomethane
ND
ug/L
20.0
1
12/12/20 09:25
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/12/20 09:25
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/12/20 09:25
108-10-1
Styrene
ND
ug/L
1.0
1
12/12/20 09:25
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 09:25
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 09:25
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/12/20 09:25
127-18-4
Toluene
ND
ug/L
1.0
1
12/12/20 09:25
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/12/20 09:25
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/12/20 09:25
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/12/20 09:25
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/12/20 09:25
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/12/20 09:25
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/12/20 09:25
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/12/20 09:25
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/12/20 09:25
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/12/20 09:25
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/12/20 09:25
95-47-6
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
12/12/20 09:25
460-00-4
1,2-Dichloroethane-d4 (S)
102
%
70-130
1
12/12/20 09:25
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
12/12/20 09:25
2037-26-5
Date: 01/11/2021 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510386
Sample: HBW-12B Lab ID: 92510386003 Collected: 12/08/20 12:15 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:26
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:26
7440-38-2
Barium
28.1
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:26
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/16/20 01:12
12/17/20 11:26
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/16/20 01:12
12/17/20 11:26
7440-43-9
Chromium
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:26
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:26
7440-48-4
Copper
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:26
7440-50-8
Lead
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:26
7439-92-1
Nickel
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:26
7440-02-0
Selenium
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:26
7782-49-2
Silver
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:26
7440-22-4
Thallium
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:26
7440-28-0
Vanadium
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:26
7440-62-2
Zinc
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:26
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
12/24/20 00:56
12/29/20 23:05
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/12/20 09:43
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/12/20 09:43
107-13-1
Benzene
ND
ug/L
1.0
1
12/12/20 09:43
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/12/20 09:43
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/12/20 09:43
75-27-4
Bromoform
ND
ug/L
1.0
1
12/12/20 09:43
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/12/20 09:43
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/12/20 09:43
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/12/20 09:43
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/12/20 09:43
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/12/20 09:43
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/12/20 09:43
75-00-3
Chloroform
ND
ug/L
5.0
1
12/12/20 09:43
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/12/20 09:43
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
12/12/20 09:43
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/12/20 09:43
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/12/20 09:43
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/12/20 09:43
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 09:43
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 09:43
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/12/20 09:43
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/12/20 09:43
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/12/20 09:43
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
v2
v1
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510386
Sample: HBW-12B Lab ID: 92510386003 Collected: 12/08/20 12:15 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/12/20 09:43
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 09:43
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 09:43
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/12/20 09:43
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 09:43
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 09:43
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/12/20 09:43
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/12/20 09:43
591-78-6
lodomethane
ND
ug/L
20.0
1
12/12/20 09:43
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/12/20 09:43
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/12/20 09:43
108-10-1
Styrene
ND
ug/L
1.0
1
12/12/20 09:43
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 09:43
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 09:43
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/12/20 09:43
127-18-4
Toluene
ND
ug/L
1.0
1
12/12/20 09:43
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/12/20 09:43
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/12/20 09:43
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/12/20 09:43
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/12/20 09:43
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/12/20 09:43
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/12/20 09:43
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/12/20 09:43
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/12/20 09:43
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/12/20 09:43
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/12/20 09:43
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
12/12/20 09:43
460-00-4
1,2-Dichloroethane-d4 (S)
106
%
70-130
1
12/12/20 09:43
17060-07-0
Toluene-d8 (S)
102
%
70-130
1
12/12/20 09:43
2037-26-5
Date: 01/11/2021 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510386
Sample: HBW-17B Lab ID: 92510386004 Collected: 12/08/20 13:00 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:30
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:30
7440-38-2
Barium
71.8
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:30
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/16/20 01:12
12/17/20 11:30
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/16/20 01:12
12/17/20 11:30
7440-43-9
Chromium
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:30
7440-47-3
Cobalt
20.9
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:30
7440-48-4
Copper
50.1
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:30
7440-50-8
Lead
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:30
7439-92-1
Nickel
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:30
7440-02-0
Selenium
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:30
7782-49-2
Silver
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:30
7440-22-4
Thallium
ND
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:30
7440-28-0
Vanadium
ND
ug/L
5.0
1
12/16/20 01:12
12/17/20 11:30
7440-62-2
Zinc
16.3
ug/L
10.0
1
12/16/20 01:12
12/17/20 11:30
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
0.11
ug/L
0.10
1
12/24/20 00:56
12/29/20 23:09
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/12/20 10:01
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/12/20 10:01
107-13-1
Benzene
9.0
ug/L
1.0
1
12/12/20 10:01
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/12/20 10:01
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/12/20 10:01
75-27-4
Bromoform
ND
ug/L
1.0
1
12/12/20 10:01
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/12/20 10:01
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/12/20 10:01
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/12/20 10:01
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/12/20 10:01
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/12/20 10:01
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/12/20 10:01
75-00-3
Chloroform
ND
ug/L
5.0
1
12/12/20 10:01
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/12/20 10:01
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
12/12/20 10:01
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/12/20 10:01
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/12/20 10:01
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/12/20 10:01
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 10:01
95-50-1
1,4-Dichlorobenzene
1.1
ug/L
1.0
1
12/12/20 10:01
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/12/20 10:01
110-57-6
1,1-Dichloroethane
6.6
ug/L
1.0
1
12/12/20 10:01
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/12/20 10:01
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
v2
v1
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510386
Sample: HBW-17B Lab ID: 92510386004 Collected: 12/08/20 13:00 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 01/11/2021 04:50 PM
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
ND
ug/L
124
ug/L
1.4
ug/L
9.8
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
31.6
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
24.4
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
1.7
ug/L
12.3
ug/L
ND
ug/L
12.3
ug/L
105
%
103
%
98
%
1.0
1
12/12/20 10:01
75-35-4
1.0
1
12/12/20 10:01
156-59-2
1.0
1
12/12/20 10:01
156-60-5
1.0
1
12/12/20 10:01
78-87-5
1.0
1
12/12/20 10:01
10061-01-5
1.0
1
12/12/20 10:01
10061-02-6
1.0
1
12/12/20 10:01
100-41-4
5.0
1
12/12/20 10:01
591-78-6
20.0
1
12/12/20 10:01
74-88-4
5.0
1
12/12/20 10:01
75-09-2
5.0
1
12/12/20 10:01
108-10-1
1.0
1
12/12/20 10:01
100-42-5
1.0
1
12/12/20 10:01
630-20-6
1.0
1
12/12/20 10:01
79-34-5
1.0
1
12/12/20 10:01
127-18-4
1.0
1
12/12/20 10:01
108-88-3
1.0
1
12/12/20 10:01
71-55-6
1.0
1
12/12/20 10:01
79-00-5
1.0
1
12/12/20 10:01
79-01-6
1.0
1
12/12/20 10:01
75-69-4
1.0
1
12/12/20 10:01
96-18-4
2.0
1
12/12/20 10:01
108-05-4
1.0
1
12/12/20 10:01
75-01-4
1.0
1
12/12/20 10:01
1330-20-7
2.0
1
12/12/20 10:01
179601-23-1
1.0
1
12/12/20 10:01
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
12/12/20 10:01 460-00-4
12/12/20 10:01 17060-07-0
12/12/20 10:01 2037-26-5
Page 11 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510386
QC Batch: 587141 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92510386001, 92510386002, 92510386003, 92510386004
METHOD BLANK: 3103223 Matrix: Water
Associated Lab Samples: 92510386001, 92510386002, 92510386003, 92510386004
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
5.0
12/17/20 10:41
10.0
12/17/20 10:41
5.0
12/17/20 10:41
1.0
12/17/20 10:41
1.0
12/17/20 10:41
5.0
12/17/20 10:41
5.0
12/17/20 10:41
5.0
12/17/20 10:41
5.0
12/17/20 10:41
5.0
12/17/20 10:41
10.0
12/17/20 10:41
5.0
12/17/20 10:41
10.0
12/17/20 10:41
5.0
12/17/20 10:41
10.0
12/17/20 10:41
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3103224
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
514
103
80-120
Arsenic
ug/L
500
513
103
80-120
Barium
ug/L
500
522
104
80-120
Beryllium
ug/L
500
522
104
80-120
Cadmium
ug/L
500
513
103
80-120
Chromium
ug/L
500
514
103
80-120
Cobalt
ug/L
500
522
104
80-120
Copper
ug/L
500
527
105
80-120
Lead
ug/L
500
517
103
80-120
Nickel
ug/L
500
514
103
80-120
Selenium
ug/L
500
510
102
80-120
Silver
ug/L
250
251
100
80-120
Thallium
ug/L
500
504
101
80-120
Vanadium
ug/L
500
526
105
80-120
Zinc
ug/L
500
504
101
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Harrisburg Rd LF-Revised Report
92510386
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3103225
3103226
MS
MSD
92509420001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
531
525
106
105
75-125
1
Arsenic
ug/L
ND
500
500
517
516
103
103
75-125
0
Barium
ug/L
75.8
500
500
600
594
105
104
75-125
1
Beryllium
ug/L
ND
500
500
533
526
107
105
75-125
2
Cadmium
ug/L
ND
500
500
515
510
103
102
75-125
1
Chromium
ug/L
ND
500
500
516
511
103
102
75-125
1
Cobalt
ug/L
13.0
500
500
535
528
104
103
75-125
1
Copper
ug/L
15.7
500
500
540
534
105
104
75-125
1
Lead
ug/L
ND
500
500
517
507
103
101
75-125
2
Nickel
ug/L
ND
500
500
520
514
103
102
75-125
1
Selenium
ug/L
ND
500
500
537
542
107
108
75-125
1
Silver
ug/L
ND
250
250
260
257
104
103
75-125
1
Thallium
ug/L
ND
500
500
499
504
100
101
75-125
1
Vanadium
ug/L
ND
500
500
528
522
106
104
75-125
1
Zinc
ug/L
39.2
500
500
549
545
102
101
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510386
QC Batch: 589260 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92510386001, 92510386002, 92510386003, 92510386004
METHOD BLANK: 3112841
Matrix:
Water
Associated Lab Samples: 92510386001, 92510386002, 92510386003, 92510386004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
0.10
12/29/20 22:37
LABORATORY CONTROL SAMPLE:
3112842
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
10
10.5
105 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3112843 3112844
MS MSD
92511882002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 10 10 10.1 10 101 100 75-125 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510386
QC Batch: 586490 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92510386001, 92510386002, 92510386003, 92510386004
METHOD BLANK: 3099796 Matrix: Water
Associated Lab Samples: 92510386001, 92510386002, 92510386003, 92510386004
Blank Reporting
Parameter Units Result Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
12/12/20 04:49
1,1,1-Trichloroethane
ug/L
ND
1.0
12/12/20 04:49
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/12/20 04:49
1,1,2-Trichloroethane
ug/L
ND
1.0
12/12/20 04:49
1,1-Dichloroethane
ug/L
ND
1.0
12/12/20 04:49
1,1-Dichloroethene
ug/L
ND
1.0
12/12/20 04:49
1,2,3-Trichloropropane
ug/L
ND
1.0
12/12/20 04:49
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
12/12/20 04:49
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/12/20 04:49
1,2-Dichlorobenzene
ug/L
ND
1.0
12/12/20 04:49
1,2-Dichloroethane
ug/L
ND
1.0
12/12/20 04:49
1,2-Dichloropropane
ug/L
ND
1.0
12/12/20 04:49
1,4-Dichlorobenzene
ug/L
ND
1.0
12/12/20 04:49
2-Butanone (MEK)
ug/L
ND
5.0
12/12/20 04:49
2-Hexanone
ug/L
ND
5.0
12/12/20 04:49
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/12/20 04:49
Acetone
ug/L
ND
25.0
12/12/20 04:49
Acrylonitrile
ug/L
ND
10.0
12/12/20 04:49
Benzene
ug/L
ND
1.0
12/12/20 04:49
Bromochloromethane
ug/L
ND
1.0
12/12/20 04:49
Bromodichloromethane
ug/L
ND
1.0
12/12/20 04:49
Bromoform
ug/L
ND
1.0
12/12/20 04:49
Bromomethane
ug/L
ND
2.0
12/12/20 04:49
Carbon disulfide
ug/L
ND
2.0
12/12/20 04:49
Carbon tetrachloride
ug/L
ND
1.0
12/12/20 04:49
Chlorobenzene
ug/L
ND
1.0
12/12/20 04:49
Chloroethane
ug/L
ND
1.0
12/12/20 04:49
Chloroform
ug/L
ND
5.0
12/12/20 04:49
Chloromethane
ug/L
ND
1.0
12/12/20 04:49
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/12/20 04:49
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/12/20 04:49
Dibromochloromethane
ug/L
ND
1.0
12/12/20 04:49
Dibromomethane
ug/L
ND
1.0
12/12/20 04:49
Ethylbenzene
ug/L
ND
1.0
12/12/20 04:49
lodomethane
ug/L
ND
20.0
12/12/20 04:49
m&p-Xylene
ug/L
ND
2.0
12/12/20 04:49
Methylene Chloride
ug/L
ND
5.0
12/12/20 04:49
o-Xylene
ug/L
ND
1.0
12/12/20 04:49
Styrene
ug/L
ND
1.0
12/12/20 04:49
Tetrachloroethene
ug/L
ND
1.0
12/12/20 04:49
v1
v2
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510386
METHOD BLANK: 3099796 Matrix: Water
Associated Lab Samples: 92510386001, 92510386002, 92510386003, 92510386004
Blank Reporting
Parameter Units Result Limit
Analyzed Qualifiers
Toluene
ug/L
ND
1.0
12/12/20 04:49
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/12/20 04:49
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/12/20 04:49
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
12/12/20 04:49
Trichloroethene
ug/L
ND
1.0
12/12/20 04:49
Trichlorofluoromethane
ug/L
ND
1.0
12/12/20 04:49
Vinyl acetate
ug/L
ND
2.0
12/12/20 04:49
Vinyl chloride
ug/L
ND
1.0
12/12/20 04:49
Xylene (Total)
ug/L
ND
1.0
12/12/20 04:49
1,2-Dichloroethane-d4 (S)
%
99
70-130
12/12/20 04:49
4-Bromofluorobenzene (S)
%
98
70-130
12/12/20 04:49
Toluene-d8 (S)
%
100
70-130
12/12/20 04:49
LABORATORY CONTROL SAMPLE:
Parameter
3099797
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
49.6
99
70-130
1,1,1-Trichloroethane
ug/L
50
44.1
88
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.8
102
70-130
1,1,2-Trichloroethane
ug/L
50
48.5
97
70-130
1,1-Dichloroethane
ug/L
50
42.3
85
70-130
1,1-Dichloroethene
ug/L
50
44.0
88
70-132
1,2,3-Trichloropropane
ug/L
50
48.2
96
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
53.3
107
70-132
1,2-Dibromoethane (EDB)
ug/L
50
51.8
104
70-130
1,2-Dichlorobenzene
ug/L
50
48.9
98
70-130
1,2-Dichloroethane
ug/L
50
44.5
89
70-130
1,2-Dichloropropane
ug/L
50
45.0
90
70-130
1,4-Dichlorobenzene
ug/L
50
47.7
95
70-130 v1
2-Butanone (MEK)
ug/L
100
98.6
99
70-133
2-Hexanone
ug/L
100
110
110
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
93.7
94
70-130
Acetone
ug/L
100
107
107
70-144
Acrylonitrile
ug/L
250
229
92
70-130
Benzene
ug/L
50
42.9
86
70-130
Bromochloromethane
ug/L
50
42.5
85
70-130
Bromodichloromethane
ug/L
50
45.2
90
70-130
Bromoform
ug/L
50
52.1
104
70-131
Bromomethane
ug/L
50
41.5
83
30-177 v2
Carbon disulfide
ug/L
50
42.5
85
70-133
Carbon tetrachloride
ug/L
50
47.5
95
70-130
Chlorobenzene
ug/L
50
47.4
95
70-130
Chloroethane
ug/L
50
43.2
86
46-131
Chloroform
ug/L
50
39.6
79
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510386
LABORATORY CONTROL SAMPLE:
Parameter
3099797
Units
Spike
Conc.
LCS LCS
Result % Rec
Chloromethane
ug/L
50
36.7
cis-1,2-Dichloroethene
ug/L
50
41.3
cis-1,3-Dichloropropene
ug/L
50
46.1
Dibromochloromethane
ug/L
50
50.9
Dibromomethane
ug/L
50
48.5
Ethylbenzene
ug/L
50
46.9
lodomethane
ug/L
100
82.9
m&p-Xylene
ug/L
100
94.9
Methylene Chloride
ug/L
50
42.5
o-Xylene
ug/L
50
47.8
Styrene
ug/L
50
49.8
Tetrachloroethene
ug/L
50
48.3
Toluene
ug/L
50
43.5
trans-1,2-Dichloroethene
ug/L
50
42.6
trans- 1,3-Dichloropropene
ug/L
50
48.0
trans-1,4-Dichloro-2-butene
ug/L
50
56.9
Trichloroethene
ug/L
50
46.0
Trichlorofluoromethane
ug/L
50
41.7
Vinyl acetate
ug/L
100
99.2
Vinyl chloride
ug/L
50
38.2
Xylene (Total)
ug/L
150
143
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
% Rec
Limits Qualifiers
73
49-130 v2
83
70-130
92
70-130
102
70-130
97
70-130
94
70-130
83
47-140
95
70-130
85
68-130
96
70-130
100
70-130
97
70-130
87
70-130
85
70-130
96
70-130
114
25-200
92
70-130
83
61-130
99
70-140
76
59-142
95
70-130
92
70-130
102
70-130
96
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3099798
MS
92510341001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3099799
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.9
19.2
110
96
70-135
14
1,1,1-Trichloroethane
ug/L
ND
20
20
22.0
20.6
110
103
70-148
7
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
20.3
18.7
102
93
70-131
8
1,1,2-Trichloroethane
ug/L
ND
20
20
20.8
19.2
104
96
70-136
8
1,1-Dichloroethane
ug/L
ND
20
20
22.0
19.9
110
99
70-147
10
1,1-Dichloroethene
ug/L
ND
20
20
22.7
20.9
114
104
70-158
9
1,2,3-Trichloropropane
ug/L
ND
20
20
21.6
19.0
108
95
67-137
13
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
21.6
18.7
108
93
69-136
15
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.3
19.4
112
97
70-137
14
1,2-Dichlorobenzene
ug/L
ND
20
20
21.2
18.8
106
94
70-133
12
1,2-Dichloroethane
ug/L
ND
20
20
20.9
19.6
105
98
67-138
7
1,2-Dichloropropane
ug/L
ND
20
20
22.2
20.3
111
101
70-138
9
1,4-Dichlorobenzene
ug/L
ND
20
20
20.5
18.9
103
95
70-133
8
2-Butanone (MEK)
ug/L
ND
40
40
42.9
40.3
107
101
61-147
6
2-Hexanone
ug/L
ND
40
40
43.5
39.4
109
98
67-139
10
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
42.6
38.7
107
97
67-136
10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510386
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3099798
MS
92510341001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3099799
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
46.8
42.7
117
107
55-159
9
Acrylonitrile
ug/L
ND
100
100
106
100
106
100
68-140
6
Benzene
ug/L
ND
20
20
21.7
19.7
109
99
67-150
10
Bromochloromethane
ug/L
ND
20
20
22.9
21.4
114
107
70-146
7
Bromodichloromethane
ug/L
ND
20
20
20.5
18.2
103
91
70-138
12
Bromoform
ug/L
ND
20
20
18.8
16.6
94
83
57-138
13
Bromomethane
ug/L
ND
20
20
23.9
23.1
120
116
10-200
31K
Carbon disulfide
ug/L
ND
20
20
21.4
19.6
107
98
70-152
9
Carbon tetrachloride
ug/L
ND
20
20
23.0
20.7
115
104
70-147
10
Chlorobenzene
ug/L
ND
20
20
21.5
18.9
108
95
70-137
13
Chloroethane
ug/L
ND
20
20
21.0
18.2
105
91
51-166
14
Chloroform
ug/L
ND
20
20
21.5
20.3
107
101
70-144
6
Chloromethane
ug/L
ND
20
20
20.4
19.0
102
95
24-161
7
cis-1,2-Dichloroethene
ug/L
ND
20
20
21.2
19.6
106
98
67-148
8
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.2
19.4
106
97
70-142
9
Dibromochloromethane
ug/L
ND
20
20
20.4
18.4
102
92
68-138
10
Dibromomethane
ug/L
ND
20
20
21.5
19.8
108
99
70-134
8
Ethylbenzene
ug/L
ND
20
20
20.8
18.3
104
91
68-143
13
lodomethane
ug/L
ND
40
40
43.6
41.6
109
104
20-161
5
m&p-Xylene
ug/L
ND
40
40
42.6
38.1
107
95
53-157
11
Methylene Chloride
ug/L
ND
20
20
21.5
19.5
107
98
64-148
9
o-Xylene
ug/L
ND
20
20
21.5
18.8
107
94
68-143
13
Styrene
ug/L
ND
20
20
20.1
17.5
100
88
70-136
14
Tetrachloroethene
ug/L
ND
20
20
20.1
18.1
100
90
70-139
11
Toluene
ug/L
ND
20
20
21.8
19.7
109
98
47-157
10
trans-1,2-Dichloroethene
ug/L
ND
20
20
21.4
19.4
107
97
70-149
10
trans- 1,3-Dichloropropene
ug/L
ND
20
20
21.2
19.0
106
95
70-138
11
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
18.5
17.4
93
87
31-145
6
Trichloroethene
ug/L
ND
20
20
21.7
18.9
109
95
70-149
14
Trichlorofluoromethane
ug/L
ND
20
20
20.1
19.0
101
95
61-154
6
Vinyl acetate
ug/L
ND
40
40
34.7
30.8
87
77
48-156
12
Vinyl chloride
ug/L
ND
20
20
19.1
18.0
95
90
55-172
6
Xylene (Total)
ug/L
ND
60
60
64.1
56.9
107
95
66-145
12
1,2-Dichloroethane-d4 (S)
%
100
102
70-130
4-Bromofluorobenzene (S)
%
101
99
70-130
Toluene-d8(S)
%
99
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 23

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510386
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 23

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Harrisburg Rd LF-Revised Report
92510386
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92510386001
HBW-21
EPA 3010A
587141
EPA 6010D
587292
92510386002
HBW-22
EPA 3010A
587141
EPA 6010D
587292
92510386003
HBW-12B
EPA 3010A
587141
EPA 6010D
587292
92510386004
HBW-17B
EPA 3010A
587141
EPA 6010D
587292
92510386001
HBW-21
EPA 3010A
589260
EPA6020B
589269
92510386002
HBW-22
EPA 3010A
589260
EPA6020B
589269
92510386003
HBW-12B
EPA 3010A
589260
EPA6020B
589269
92510386004
HBW-17B
EPA 3010A
589260
EPA6020B
589269
92510386001
HBW-21
EPA 8260D
586490
92510386002
HBW-22
EPA 8260D
586490
92510386003
HBW-12B
EPA 8260D
586490
92510386004
HBW-17B
EPA 8260D
586490
Date: 01/11/2021 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 20 of 23

Document Name: Document Revised: Dctober 28, 2020
Sample Condition Upon Receipt(SCUR) Page 1 of 2
i aceAnalytkafr Document No.: Issuing Authority:
1 F-CAR-CS-033-Rev.07 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Q Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville❑
ConditionClient Name: WO# 92510386
.. 1 �I/ic"I )1V d ( J J' Project q: •
Courier: []Fed Ex BPS ❑U5P r CI,eni
❑ Commercial ❑Pace []Other: 92530386
- Custody Seat Present? Yes o Seals Intact? []—Yes W0
Date/Initials Person Examining Contents:
Packing Material: ❑Bubble Wrap ❑Bubble Bags [?'None ❑ Other Biological Tissue Frozen?
Thermometer: ,(vet ❑81ue ❑None ❑Yes []No Ulal/A
PR Gun IM 92TO64 Type of Ice:
\\ Correction Factor:
Cooler Temp: �. Add/Subtract ("C) -0.1 Temp should be above freezing to 6'C
C:I []Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected ('C): i has begun
USDA Regulated Soil (([g N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
IlYes rlNo including Hawaii and Puerto Ricol? FlYes MNo
Comm a nts/al s crepa n cy:
Chain of Custody Present?
cKyes
ONO
[-]N/A
1.
Samples Arrived within Hold Time?
oyes
❑ND
[]N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑yes
c No
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
( No
❑N/A
4.
Sufficient Volume?
t3Yes
❑No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
es
Res
❑No
❑ND
❑N/A
❑N/A
6.
Containers Intact?
Zies
No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑yes
[]No
/A
8,
Sample Labels Match COC?
-Includes Date/Time/ID Matrix:
q5yes
3__�
n/Analysis
[-]NO
❑NIA
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
No
❑N/A
10.
Trip Blank Present?
Trip Blank Custody_Seals Present?
[]Yes
Yes
J2No
❑No
[-I N/A
'21PIA
11.
COMMENTS/SAMPLE DISCREPANCY
Field Data Required? ❑Yes ❑No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review; Date:
Project Manager SRF Review: Date:
Page 21 of 23

Document Name:
Sample Condition Upon Recei
aceAnaWical Document No.:
F-CAR-CS-033-R ev.07
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLlig
"Bottom half of box is to list number of bottles
Document Revised: October 18, lU1U
t(SCUR) Page 2 of 2
Issuing Authority:
Pace Carolinas Quality Office
Project #
Wo#:92510386
PM: MWB Due Date: 12/22/20
CLIENT: 92-MECK CO
lu
z
NCL
N
z
Z
N
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Page 22 of 23

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Page 23 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
January 11, 2021
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510381
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on December 08, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
This revision was issued on 01/11/21 to correct the title of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510381
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510381
Analytes
Lab ID Sample ID
Method
Analysts
Reported
Laboratory
92510381001 HB2006
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
52
PASI-C
92510381002 HB2008
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
52
PASI-C
92510381003 HB2010
EPA 601OD
SH1
15
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
52
PASI-C
92510381004 TRIP BLANK
EPA 8260D
CL
52
PASI-C
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510381
Sample: HB2006 Lab ID: 92510381001 Collected: 12/08/20 14:25 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
12/16/20 09:55
12/29/20 15:22
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/16/20 09:55
12/24/20 17:35
7440-38-2
Barium
24.2
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:35
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/16/20 09:55
12/24/20 17:35
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/16/20 09:55
12/24/20 17:35
7440-43-9
Chromium
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:35
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:35
7440-48-4
Copper
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:35
7440-50-8
Lead
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:35
7439-92-1
Nickel
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:35
7440-02-0
Selenium
ND
ug/L
10.0
1
12/16/20 09:55
12/24/20 17:35
7782-49-2
Silver
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:35
7440-22-4
Thallium
ND
ug/L
10.0
1
12/16/20 09:55
12/24/20 17:35
7440-28-0
Vanadium
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:35
7440-62-2
Zinc
ND
ug/L
10.0
1
12/16/20 09:55
12/24/20 17:35
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
12/24/20 00:56
12/29/20 23:13
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/12/20 07:16
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/12/20 07:16
107-13-1
Benzene
ND
ug/L
1.0
1
12/12/20 07:16
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/12/20 07:16
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/12/20 07:16
75-27-4
Bromoform
ND
ug/L
1.0
1
12/12/20 07:16
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/12/20 07:16
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/12/20 07:16
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/12/20 07:16
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/12/20 07:16
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/12/20 07:16
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/12/20 07:16
75-00-3
Chloroform
ND
ug/L
5.0
1
12/12/20 07:16
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/12/20 07:16
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
12/12/20 07:16
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/12/20 07:16
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/12/20 07:16
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/12/20 07:16
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 07:16
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 07:16
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/12/20 07:16
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/12/20 07:16
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/12/20 07:16
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
v2
v1
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510381
Sample: HB2006 Lab ID: 92510381001 Collected: 12/08/20 14:25 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/12/20 07:16
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 07:16
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 07:16
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/12/20 07:16
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 07:16
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 07:16
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/12/20 07:16
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/12/20 07:16
591-78-6
lodomethane
ND
ug/L
20.0
1
12/12/20 07:16
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/12/20 07:16
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/12/20 07:16
108-10-1
Styrene
ND
ug/L
1.0
1
12/12/20 07:16
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 07:16
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 07:16
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/12/20 07:16
127-18-4
Toluene
ND
ug/L
1.0
1
12/12/20 07:16
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/12/20 07:16
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/12/20 07:16
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/12/20 07:16
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/12/20 07:16
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/12/20 07:16
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/12/20 07:16
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/12/20 07:16
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/12/20 07:16
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/12/20 07:16
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/12/20 07:16
95-47-6
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
12/12/20 07:16
460-00-4
1,2-Dichloroethane-d4 (S)
103
%
70-130
1
12/12/20 07:16
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
12/12/20 07:16
2037-26-5
Date: 01/11/2021 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510381
Sample: HB2008 Lab ID: 92510381002 Collected: 12/08/20 14:45 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
5.5
ug/L
5.0
1
12/16/20 09:55
12/29/20 15:25
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/16/20 09:55
12/24/20 17:39
7440-38-2
Barium
19.9
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:39
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/16/20 09:55
12/24/20 17:39
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/16/20 09:55
12/24/20 17:39
7440-43-9
Chromium
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:39
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:39
7440-48-4
Copper
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:39
7440-50-8
Lead
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:39
7439-92-1
Nickel
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:39
7440-02-0
Selenium
ND
ug/L
10.0
1
12/16/20 09:55
12/24/20 17:39
7782-49-2
Silver
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:39
7440-22-4
Thallium
ND
ug/L
10.0
1
12/16/20 09:55
12/24/20 17:39
7440-28-0
Vanadium
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:39
7440-62-2
Zinc
ND
ug/L
10.0
1
12/16/20 09:55
12/24/20 17:39
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
12/24/20 00:56
12/29/20 23:25
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/12/20 07:34
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/12/20 07:34
107-13-1
Benzene
ND
ug/L
1.0
1
12/12/20 07:34
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/12/20 07:34
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/12/20 07:34
75-27-4
Bromoform
ND
ug/L
1.0
1
12/12/20 07:34
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/12/20 07:34
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/12/20 07:34
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/12/20 07:34
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/12/20 07:34
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/12/20 07:34
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/12/20 07:34
75-00-3
Chloroform
ND
ug/L
5.0
1
12/12/20 07:34
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/12/20 07:34
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
12/12/20 07:34
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/12/20 07:34
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/12/20 07:34
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/12/20 07:34
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 07:34
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 07:34
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/12/20 07:34
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/12/20 07:34
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/12/20 07:34
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
v2
v1
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510381
Sample: HB2008 Lab ID: 92510381002 Collected: 12/08/20 14:45 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/12/20 07:34
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 07:34
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 07:34
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/12/20 07:34
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 07:34
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 07:34
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/12/20 07:34
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/12/20 07:34
591-78-6
lodomethane
ND
ug/L
20.0
1
12/12/20 07:34
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/12/20 07:34
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/12/20 07:34
108-10-1
Styrene
ND
ug/L
1.0
1
12/12/20 07:34
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 07:34
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 07:34
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/12/20 07:34
127-18-4
Toluene
ND
ug/L
1.0
1
12/12/20 07:34
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/12/20 07:34
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/12/20 07:34
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/12/20 07:34
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/12/20 07:34
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/12/20 07:34
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/12/20 07:34
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/12/20 07:34
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/12/20 07:34
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/12/20 07:34
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/12/20 07:34
95-47-6
Surrogates
4-Bromofluorobenzene (S)
104
%
70-130
1
12/12/20 07:34
460-00-4
1,2-Dichloroethane-d4 (S)
104
%
70-130
1
12/12/20 07:34
17060-07-0
Toluene-d8 (S)
102
%
70-130
1
12/12/20 07:34
2037-26-5
Date: 01/11/2021 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510381
Sample: HB2010 Lab ID: 92510381003 Collected: 12/08/20 11:15 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Antimony
ND
ug/L
5.0
1
12/16/20 09:55
12/29/20 15:29
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/16/20 09:55
12/24/20 17:42
7440-38-2
Barium
47.8
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:42
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/16/20 09:55
12/24/20 17:42
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/16/20 09:55
12/24/20 17:42
7440-43-9
Chromium
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:42
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:42
7440-48-4
Copper
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:42
7440-50-8
Lead
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:42
7439-92-1
Nickel
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:42
7440-02-0
Selenium
ND
ug/L
10.0
1
12/16/20 09:55
12/24/20 17:42
7782-49-2
Silver
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:42
7440-22-4
Thallium
ND
ug/L
10.0
1
12/16/20 09:55
12/24/20 17:42
7440-28-0
Vanadium
ND
ug/L
5.0
1
12/16/20 09:55
12/24/20 17:42
7440-62-2
Zinc
ND
ug/L
10.0
1
12/16/20 09:55
12/24/20 17:42
7440-66-6
6020 MET ICPMS
Analytical Method:
EPA 6020E Preparation Method: EPA 3010A
Pace Analytical
Services -Asheville
Thallium
ND
ug/L
0.10
1
12/24/20 00:56
12/29/20 23:29
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Pace Analytical
Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/12/20 07:53
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/12/20 07:53
107-13-1
Benzene
ND
ug/L
1.0
1
12/12/20 07:53
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/12/20 07:53
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/12/20 07:53
75-27-4
Bromoform
ND
ug/L
1.0
1
12/12/20 07:53
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/12/20 07:53
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/12/20 07:53
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/12/20 07:53
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/12/20 07:53
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/12/20 07:53
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/12/20 07:53
75-00-3
Chloroform
ND
ug/L
5.0
1
12/12/20 07:53
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/12/20 07:53
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
12/12/20 07:53
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/12/20 07:53
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/12/20 07:53
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/12/20 07:53
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 07:53
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 07:53
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/12/20 07:53
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/12/20 07:53
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/12/20 07:53
107-06-2
REPORT OF LABORATORY ANALYSIS
v2
v2
v1
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510381
Sample: HB2010 Lab ID: 92510381003 Collected: 12/08/20 11:15 Received: 12/08/20 15:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical
Services - Charlotte
1,1-Dichloroethene
ND
ug/L
1.0
1
12/12/20 07:53
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 07:53
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 07:53
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/12/20 07:53
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 07:53
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 07:53
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/12/20 07:53
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/12/20 07:53
591-78-6
lodomethane
ND
ug/L
20.0
1
12/12/20 07:53
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/12/20 07:53
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/12/20 07:53
108-10-1
Styrene
ND
ug/L
1.0
1
12/12/20 07:53
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 07:53
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 07:53
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/12/20 07:53
127-18-4
Toluene
ND
ug/L
1.0
1
12/12/20 07:53
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/12/20 07:53
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/12/20 07:53
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/12/20 07:53
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/12/20 07:53
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/12/20 07:53
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/12/20 07:53
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/12/20 07:53
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/12/20 07:53
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/12/20 07:53
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/12/20 07:53
95-47-6
Surrogates
4-Bromofluorobenzene (S)
101
%
70-130
1
12/12/20 07:53
460-00-4
1,2-Dichloroethane-d4 (S)
98
%
70-130
1
12/12/20 07:53
17060-07-0
Toluene-d8(S)
99
%
70-130
1
12/12/20 07:53
2037-26-5
Date: 01/11/2021 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510381
Sample: TRIP BLANK
Lab ID: 92510381004 Collected:
12/08/20
09:39
Received: 12/08/20 15:53 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Acetone
ND
ug/L
25.0
1
12/12/20 05:44
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/12/20 05:44
107-13-1
Benzene
ND
ug/L
1.0
1
12/12/20 05:44
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/12/20 05:44
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/12/20 05:44
75-27-4
Bromoform
ND
ug/L
1.0
1
12/12/20 05:44
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/12/20 05:44
74-83-9 v2
2-Butanone (MEK)
ND
ug/L
5.0
1
12/12/20 05:44
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/12/20 05:44
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/12/20 05:44
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/12/20 05:44
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/12/20 05:44
75-00-3
Chloroform
ND
ug/L
5.0
1
12/12/20 05:44
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/12/20 05:44
74-87-3 v2
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
12/12/20 05:44
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/12/20 05:44
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/12/20 05:44
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/12/20 05:44
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 05:44
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/12/20 05:44
106-46-7 v1
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/12/20 05:44
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/12/20 05:44
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/12/20 05:44
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/12/20 05:44
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 05:44
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/20 05:44
156-60-5
1,2-Dichloropropene
ND
ug/L
1.0
1
12/12/20 05:44
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 05:44
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/20 05:44
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/12/20 05:44
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/12/20 05:44
591-78-6
lodomethane
ND
ug/L
20.0
1
12/12/20 05:44
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
12/12/20 05:44
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/12/20 05:44
108-10-1
Styrene
ND
ug/L
1.0
1
12/12/20 05:44
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 05:44
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/20 05:44
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/12/20 05:44
127-18-4
Toluene
ND
ug/L
1.0
1
12/12/20 05:44
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/12/20 05:44
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/12/20 05:44
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/12/20 05:44
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/12/20 05:44
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/12/20 05:44
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/12/20 05:44
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/12/20 05:44
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510381
Sample: TRIP BLANK
Parameters
Lab ID: 92510381004 Collected: 12/08/20 09:39
Results Units Report Limit DF
Received: 12/08/20 15:53 Matrix: Water
Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Xylene (Total)
ND ug/L
1.0
1
12/12/20 05:44
1330-20-7
m&p-Xylene
ND ug/L
2.0
1
12/12/20 05:44
179601-23-1
o-Xylene
ND ug/L
1.0
1
12/12/20 05:44
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99 %
70-130
1
12/12/20 05:44
460-00-4
1,2-Dichloroethane-d4 (S)
102 %
70-130
1
12/12/20 05:44
17060-07-0
Toluene-d8 (S)
96 %
70-130
1
12/12/20 05:44
2037-26-5
Date: 01/11/2021 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510381
QC Batch: 587333 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92510381001, 92510381002, 92510381003
METHOD BLANK: 3104052 Matrix: Water
Associated Lab Samples: 92510381001, 92510381002, 92510381003
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
5.0
12/30/20 15:10
10.0
12/30/20 15:10
5.0
12/30/20 15:10
1.0
12/30/20 15:10
1.0
12/30/20 15:10
5.0
12/30/20 15:10
5.0
12/30/20 15:10
5.0
12/30/20 15:10
5.0
12/30/20 15:10
5.0
12/30/20 15:10
10.0
12/30/20 15:10
5.0
12/30/20 15:10
10.0
12/30/20 15:10
5.0
12/30/20 15:10
10.0
12/30/20 15:10
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
3104053
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
514
103
80-120
Arsenic
ug/L
500
507
101
80-120
Barium
ug/L
500
520
104
80-120
Beryllium
ug/L
500
523
105
80-120
Cadmium
ug/L
500
516
103
80-120
Chromium
ug/L
500
516
103
80-120
Cobalt
ug/L
500
526
105
80-120
Copper
ug/L
500
533
107
80-120
Lead
ug/L
500
517
103
80-120
Nickel
ug/L
500
521
104
80-120
Selenium
ug/L
500
510
102
80-120
Silver
ug/L
250
274
110
80-120
Thallium
ug/L
500
531
106
80-120
Vanadium
ug/L
500
518
104
80-120
Zinc
ug/L
500
508
102
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Harrisburg Rd LF-Revised Report
92510381
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
3104054
3104055
MS
MSD
92510341001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
3AJ
500
500
533
522
106
104
75-125
2
Arsenic
ug/L
ND
500
500
516
502
103
100
75-125
3
Barium
ug/L
36.5
500
500
550
543
103
101
75-125
1
Beryllium
ug/L
ND
500
500
528
521
106
104
75-125
1
Cadmium
ug/L
ND
500
500
515
509
103
102
75-125
1
Chromium
ug/L
9.4
500
500
519
511
102
100
75-125
2
Cobalt
ug/L
ND
500
500
517
512
103
102
75-125
1
Copper
ug/L
ND
500
500
530
523
106
104
75-125
1
Lead
ug/L
ND
500
500
508
501
102
100
75-125
1
Nickel
ug/L
5.2
500
500
514
511
102
101
75-125
1
Selenium
ug/L
ND
500
500
530
524
106
105
75-125
1
Silver
ug/L
ND
250
250
283
281
113
112
75-125
1
Thallium
ug/L
ND
500
500
522
515
104
103
75-125
1
Vanadium
ug/L
20.8
500
500
536
530
103
102
75-125
1
Zinc
ug/L
ND
500
500
512
504
102
100
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510381
QC Batch: 589260 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92510381001, 92510381002, 92510381003
METHOD BLANK: 3112841
Matrix:
Water
Associated Lab Samples: 92510381001, 92510381002, 92510381003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Thallium
ug/L
ND
0.10
12/29/20 22:37
LABORATORY CONTROL SAMPLE:
3112842
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Thallium
ug/L
10
10.5
105 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3112843 3112844
MS MSD
92511882002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 10 10 10.1 10 101 100 75-125 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510381
QC Batch: 586490 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92510381001, 92510381002, 92510381003, 92510381004
METHOD BLANK: 3099796 Matrix: Water
Associated Lab Samples: 92510381001, 92510381002, 92510381003, 92510381004
Blank Reporting
Parameter Units Result Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
12/12/20 04:49
1,1,1-Trichloroethane
ug/L
ND
1.0
12/12/20 04:49
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/12/20 04:49
1,1,2-Trichloroethane
ug/L
ND
1.0
12/12/20 04:49
1,1-Dichloroethane
ug/L
ND
1.0
12/12/20 04:49
1,1-Dichloroethene
ug/L
ND
1.0
12/12/20 04:49
1,2,3-Trichloropropane
ug/L
ND
1.0
12/12/20 04:49
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
12/12/20 04:49
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/12/20 04:49
1,2-Dichlorobenzene
ug/L
ND
1.0
12/12/20 04:49
1,2-Dichloroethane
ug/L
ND
1.0
12/12/20 04:49
1,2-Dichloropropane
ug/L
ND
1.0
12/12/20 04:49
1,4-Dichlorobenzene
ug/L
ND
1.0
12/12/20 04:49
2-Butanone (MEK)
ug/L
ND
5.0
12/12/20 04:49
2-Hexanone
ug/L
ND
5.0
12/12/20 04:49
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/12/20 04:49
Acetone
ug/L
ND
25.0
12/12/20 04:49
Acrylonitrile
ug/L
ND
10.0
12/12/20 04:49
Benzene
ug/L
ND
1.0
12/12/20 04:49
Bromochloromethane
ug/L
ND
1.0
12/12/20 04:49
Bromodichloromethane
ug/L
ND
1.0
12/12/20 04:49
Bromoform
ug/L
ND
1.0
12/12/20 04:49
Bromomethane
ug/L
ND
2.0
12/12/20 04:49
Carbon disulfide
ug/L
ND
2.0
12/12/20 04:49
Carbon tetrachloride
ug/L
ND
1.0
12/12/20 04:49
Chlorobenzene
ug/L
ND
1.0
12/12/20 04:49
Chloroethane
ug/L
ND
1.0
12/12/20 04:49
Chloroform
ug/L
ND
5.0
12/12/20 04:49
Chloromethane
ug/L
ND
1.0
12/12/20 04:49
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/12/20 04:49
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/12/20 04:49
Dibromochloromethane
ug/L
ND
1.0
12/12/20 04:49
Dibromomethane
ug/L
ND
1.0
12/12/20 04:49
Ethylbenzene
ug/L
ND
1.0
12/12/20 04:49
lodomethane
ug/L
ND
20.0
12/12/20 04:49
m&p-Xylene
ug/L
ND
2.0
12/12/20 04:49
Methylene Chloride
ug/L
ND
5.0
12/12/20 04:49
o-Xylene
ug/L
ND
1.0
12/12/20 04:49
Styrene
ug/L
ND
1.0
12/12/20 04:49
Tetrachloroethene
ug/L
ND
1.0
12/12/20 04:49
v1
v2
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510381
METHOD BLANK: 3099796 Matrix: Water
Associated Lab Samples: 92510381001, 92510381002, 92510381003, 92510381004
Blank Reporting
Parameter Units Result Limit
Analyzed Qualifiers
Toluene
ug/L
ND
1.0
12/12/20 04:49
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/12/20 04:49
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/12/20 04:49
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
12/12/20 04:49
Trichloroethene
ug/L
ND
1.0
12/12/20 04:49
Trichlorofluoromethane
ug/L
ND
1.0
12/12/20 04:49
Vinyl acetate
ug/L
ND
2.0
12/12/20 04:49
Vinyl chloride
ug/L
ND
1.0
12/12/20 04:49
Xylene (Total)
ug/L
ND
1.0
12/12/20 04:49
1,2-Dichloroethane-d4 (S)
%
99
70-130
12/12/20 04:49
4-Bromofluorobenzene (S)
%
98
70-130
12/12/20 04:49
Toluene-d8 (S)
%
100
70-130
12/12/20 04:49
LABORATORY CONTROL SAMPLE:
Parameter
3099797
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
49.6
99
70-130
1,1,1-Trichloroethane
ug/L
50
44.1
88
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.8
102
70-130
1,1,2-Trichloroethane
ug/L
50
48.5
97
70-130
1,1-Dichloroethane
ug/L
50
42.3
85
70-130
1,1-Dichloroethene
ug/L
50
44.0
88
70-132
1,2,3-Trichloropropane
ug/L
50
48.2
96
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
53.3
107
70-132
1,2-Dibromoethane (EDB)
ug/L
50
51.8
104
70-130
1,2-Dichlorobenzene
ug/L
50
48.9
98
70-130
1,2-Dichloroethane
ug/L
50
44.5
89
70-130
1,2-Dichloropropane
ug/L
50
45.0
90
70-130
1,4-Dichlorobenzene
ug/L
50
47.7
95
70-130 v1
2-Butanone (MEK)
ug/L
100
98.6
99
70-133
2-Hexanone
ug/L
100
110
110
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
93.7
94
70-130
Acetone
ug/L
100
107
107
70-144
Acrylonitrile
ug/L
250
229
92
70-130
Benzene
ug/L
50
42.9
86
70-130
Bromochloromethane
ug/L
50
42.5
85
70-130
Bromodichloromethane
ug/L
50
45.2
90
70-130
Bromoform
ug/L
50
52.1
104
70-131
Bromomethane
ug/L
50
41.5
83
30-177 v2
Carbon disulfide
ug/L
50
42.5
85
70-133
Carbon tetrachloride
ug/L
50
47.5
95
70-130
Chlorobenzene
ug/L
50
47.4
95
70-130
Chloroethane
ug/L
50
43.2
86
46-131
Chloroform
ug/L
50
39.6
79
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510381
LABORATORY CONTROL SAMPLE:
Parameter
3099797
Units
Spike
Conc.
LCS LCS
Result % Rec
Chloromethane
ug/L
50
36.7
cis-1,2-Dichloroethene
ug/L
50
41.3
cis-1,3-Dichloropropene
ug/L
50
46.1
Dibromochloromethane
ug/L
50
50.9
Dibromomethane
ug/L
50
48.5
Ethylbenzene
ug/L
50
46.9
lodomethane
ug/L
100
82.9
m&p-Xylene
ug/L
100
94.9
Methylene Chloride
ug/L
50
42.5
o-Xylene
ug/L
50
47.8
Styrene
ug/L
50
49.8
Tetrachloroethene
ug/L
50
48.3
Toluene
ug/L
50
43.5
trans-1,2-Dichloroethene
ug/L
50
42.6
trans- 1,3-Dichloropropene
ug/L
50
48.0
trans-1,4-Dichloro-2-butene
ug/L
50
56.9
Trichloroethene
ug/L
50
46.0
Trichlorofluoromethane
ug/L
50
41.7
Vinyl acetate
ug/L
100
99.2
Vinyl chloride
ug/L
50
38.2
Xylene (Total)
ug/L
150
143
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
% Rec
Limits Qualifiers
73
49-130 v2
83
70-130
92
70-130
102
70-130
97
70-130
94
70-130
83
47-140
95
70-130
85
68-130
96
70-130
100
70-130
97
70-130
87
70-130
85
70-130
96
70-130
114
25-200
92
70-130
83
61-130
99
70-140
76
59-142
95
70-130
92
70-130
102
70-130
96
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3099798
MS
92510341001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3099799
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.9
19.2
110
96
70-135
14
1,1,1-Trichloroethane
ug/L
ND
20
20
22.0
20.6
110
103
70-148
7
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
20.3
18.7
102
93
70-131
8
1,1,2-Trichloroethane
ug/L
ND
20
20
20.8
19.2
104
96
70-136
8
1,1-Dichloroethane
ug/L
ND
20
20
22.0
19.9
110
99
70-147
10
1,1-Dichloroethene
ug/L
ND
20
20
22.7
20.9
114
104
70-158
9
1,2,3-Trichloropropane
ug/L
ND
20
20
21.6
19.0
108
95
67-137
13
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
21.6
18.7
108
93
69-136
15
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.3
19.4
112
97
70-137
14
1,2-Dichlorobenzene
ug/L
ND
20
20
21.2
18.8
106
94
70-133
12
1,2-Dichloroethane
ug/L
ND
20
20
20.9
19.6
105
98
67-138
7
1,2-Dichloropropane
ug/L
ND
20
20
22.2
20.3
111
101
70-138
9
1,4-Dichlorobenzene
ug/L
ND
20
20
20.5
18.9
103
95
70-133
8
2-Butanone (MEK)
ug/L
ND
40
40
42.9
40.3
107
101
61-147
6
2-Hexanone
ug/L
ND
40
40
43.5
39.4
109
98
67-139
10
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
42.6
38.7
107
97
67-136
10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510381
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3099798
MS
92510341001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
3099799
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Acetone
ug/L
ND
40
40
46.8
42.7
117
107
55-159
9
Acrylonitrile
ug/L
ND
100
100
106
100
106
100
68-140
6
Benzene
ug/L
ND
20
20
21.7
19.7
109
99
67-150
10
Bromochloromethane
ug/L
ND
20
20
22.9
21.4
114
107
70-146
7
Bromodichloromethane
ug/L
ND
20
20
20.5
18.2
103
91
70-138
12
Bromoform
ug/L
ND
20
20
18.8
16.6
94
83
57-138
13
Bromomethane
ug/L
ND
20
20
23.9
23.1
120
116
10-200
31K
Carbon disulfide
ug/L
ND
20
20
21.4
19.6
107
98
70-152
9
Carbon tetrachloride
ug/L
ND
20
20
23.0
20.7
115
104
70-147
10
Chlorobenzene
ug/L
ND
20
20
21.5
18.9
108
95
70-137
13
Chloroethane
ug/L
ND
20
20
21.0
18.2
105
91
51-166
14
Chloroform
ug/L
ND
20
20
21.5
20.3
107
101
70-144
6
Chloromethane
ug/L
ND
20
20
20.4
19.0
102
95
24-161
7
cis-1,2-Dichloroethene
ug/L
ND
20
20
21.2
19.6
106
98
67-148
8
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.2
19.4
106
97
70-142
9
Dibromochloromethane
ug/L
ND
20
20
20.4
18.4
102
92
68-138
10
Dibromomethane
ug/L
ND
20
20
21.5
19.8
108
99
70-134
8
Ethylbenzene
ug/L
ND
20
20
20.8
18.3
104
91
68-143
13
lodomethane
ug/L
ND
40
40
43.6
41.6
109
104
20-161
5
m&p-Xylene
ug/L
ND
40
40
42.6
38.1
107
95
53-157
11
Methylene Chloride
ug/L
ND
20
20
21.5
19.5
107
98
64-148
9
o-Xylene
ug/L
ND
20
20
21.5
18.8
107
94
68-143
13
Styrene
ug/L
ND
20
20
20.1
17.5
100
88
70-136
14
Tetrachloroethene
ug/L
ND
20
20
20.1
18.1
100
90
70-139
11
Toluene
ug/L
ND
20
20
21.8
19.7
109
98
47-157
10
trans-1,2-Dichloroethene
ug/L
ND
20
20
21.4
19.4
107
97
70-149
10
trans- 1,3-Dichloropropene
ug/L
ND
20
20
21.2
19.0
106
95
70-138
11
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
18.5
17.4
93
87
31-145
6
Trichloroethene
ug/L
ND
20
20
21.7
18.9
109
95
70-149
14
Trichlorofluoromethane
ug/L
ND
20
20
20.1
19.0
101
95
61-154
6
Vinyl acetate
ug/L
ND
40
40
34.7
30.8
87
77
48-156
12
Vinyl chloride
ug/L
ND
20
20
19.1
18.0
95
90
55-172
6
Xylene (Total)
ug/L
ND
60
60
64.1
56.9
107
95
66-145
12
1,2-Dichloroethane-d4 (S)
%
100
102
70-130
4-Bromofluorobenzene (S)
%
101
99
70-130
Toluene-d8(S)
%
99
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 23

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: Harrisburg Rd LF-Revised Report
Pace Project No.: 92510381
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 23

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Harrisburg Rd LF-Revised Report
92510381
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92510381001
HB2006
EPA 3010A
587333
EPA 6010D
587369
92510381002
HB2008
EPA 3010A
587333
EPA 6010D
587369
92510381003
HB2010
EPA 3010A
587333
EPA 6010D
587369
92510381001
HB2006
EPA 3010A
589260
EPA 6020B
589269
92510381002
HB2008
EPA 3010A
589260
EPA 6020B
589269
92510381003
HB2010
EPA 3010A
589260
EPA 6020B
589269
92510381001
HB2006
EPA 8260D
586490
92510381002
HB2008
EPA 8260D
586490
92510381003
HB2010
EPA 8260D
586490
92510381004
TRIP BLANK
EPA 8260D
586490
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/11/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 23

uocument Name: uocument neviseo: uctooer [is, zuzu
Sample Condition Upon Receipt(SCUR) Page 1 of 2
Z aceAnaVical6 Document No.: Issuing Authority:
It F-CAR-CS-033-Rev.07 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville fE. Raleigh❑ Mechanicsville[] Atlanta❑ Kernersville❑
IlentN me: WO# : 92510381
. , 0 Can � �� � � Project #t:
Courier: fed Ex JZUPS 06SPS &Iient
❑ Commercial ❑Pace QOther: I l 1 l
92510381
Custody Sea I risen s o Seals Intacti i ii — —
Date/initials Person Examining Conte nts:1
Packing Material: ❑Bubble Wrap []Bubble Bags bone ❑ Other Biological Tissue Frozen?
Thermome S: []Yes ❑No Q6/A
ITR sun ID: 92TO64 � t ❑Blue ❑None
Type of ice:
Correction Factor:
Cooler Temp: �' Add/Subtract (°C) -0.1 Temp should be above freezing to 6*C
-2 9❑Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected (°C): has begun
USDA Regulated Soil �N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
11Yes nNo including Hawaii and Puprta RiroI7 oyes nNo
Comments/Discrepancy:
Chain of Custody Present?
E: Yes
❑No
❑N/A
1.
Samples Arrived within Hold Time?
E�ies
❑No
❑N/A
2.
Short Hold Time Analysis (<72 ht.)?
[]Yes
JkNo
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
Maio
❑N/A
4.
Sufficient Volume?
0yes
❑No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
Yes
1 Yes
❑No
No
❑N/A
N/A
6.
Containers Intact?
ayes
[]NO
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
[-]Yes
❑No
©-14/A
8.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
es
1
❑No
❑N/A
9.
Headspace in VOA Vials (>5-6mrn)?
Yes
bkn
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
Kees
❑Yes
❑No
(Ra
❑N/A
❑NIA
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/FtESOLUTION
Person contacted:
Project Manager SCURF Review:
Date/Time:
Lot ID of split containers:
Date:
Field Data Required? ❑Yes [:)No
Project Manager SRF Review:
Date:
Page 21 of 23

Document Revised: OCtoper 28, 2U20
Page 2 of 2
aceAnalj&cal R
Document Name:
Sample Condition Upon Recei
Document No.:
F-CAR-CS-033-Rev.07
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottles
Issuing Authority:
Pace Carolinas fluafiry flffira
Project# Wp# : 92510381
PM: MWB Due Date: 12/22/20
CLIENT: 92-MECK CO
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Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will he sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 22 of 23

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Page 23 of 23