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HomeMy WebLinkAbout8602_Surry_MtAiry_MSWLF_CDLF_June20GW_FID1522105_20210106Electronic Data - Email CD (data loaded: Yes / No NC DENR Division of Waste Management - Solid Waste Doc/Event #: Environmental Monitoring ReDortina Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6), Instructions: Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed_ explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i): Send the original signed- and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646, Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): Municipal Engineering Services Co., PA Con -tact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Jonathan Pfohl Phone: (919)772-5393 E-mail: jpfohl@mesco.com NC Landfill Rule: Actual sampling dates (e.g,, Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006) Surry County Closed C&D and 237 Landfill Road Closed MSW Landfill -Mt. Airy Mt. Airy, NC 27030 86-02 .1600 June 25, 2020 Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring Q Detection Monitoring Q Assessment Monitoring 0 Corrective Action of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells ❑ Groundwater monitoring data from private water supply wells Leachate monitoring -data Fx Surface water monitoring data ❑ Methane gas monitoring data Corrective action data (specify) MNA parameters on 7 wells Other(specity) Notification attached? No. No groundwater -or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater orsurface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary -analysis of the cause and significance of any concentration. ❑ Yes, a notification of values exceeding an explosive .methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments -are true and correct. Furthermore, 1 have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levelsand a preliminary analysis of he cause and signif ,icance of concentrations exceeding groundwater standards. I am aware that there are -significant penalties for making -any false statement, -representation, or certification including the possibility of a fine and imprisonment. Benjamin Clawson, P.E. Senior Project Manager (919) 772--5393 Facili Represen Name (Print) Title (Area Code) Telephone Number �,✓`_ I S a Affix NC Licensed/ Professional Geologist Seal Signature P.O. BOX 97, Garner, NC 27529 Facility Representative Address C-0281 NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 CARS �,�o ��Ssia ••.YYy ; O ti•. 'IL SEAL 9roe • 03 10 r(1►i)eti Semi -Annual Water Quality Monitoring Report with Corrective Action Update June 2020 Prepared for Surry County Closed C�iD and Closed Landfill Mt. Airy, North Carolina Permit No. 86-02 Prepared by Municipal Engineering Services Company, P.A. P.O. BOX 97 ~\ o6 ESS%0`/2y% SEAL r; _ 033710 A& Benjamin Clawson, P.E. Senior Project Manager bclawson(,,,mesco.com Garner, North Carolina MESCO Project 1�I��x►ber: G20031.0 MUNICIPAL ENGINEERING SERVICES CDMPANY� P.A. Jonathan Pfohl Environmental Specialist ipfohl(j mesco.com 6S 5HIPWABH ORrvE, GARNER, NC 27529 -PHONE: 91 9-772-5393 P.O. SOX 349, SOONE, NC 2B607 -PHONE: 528-262-1767 LICFN.RF NiiN aFa: C-0221 TABLE OF CONTENTS SECTION Introduction....................................................................................................................................................................................................................................................................................................................................Page 1 Background...................................................................................................................................................................................................................................................................................................................................... Page 1 SamplingProcedures........................................................................................................................................................................................................................................................................................................Page 2 FieldParameter Data......................................................................................................................................................................................................................................................................................................._Page 2 LaboratoryResults.............................................................................................................................................................................................................................................................................................................._Page 2 QualityControl Samples..........................................................................................................................................................................................................................................................................................Page 3 Groundwater Samples Detected Above Standards..........................................................................................................................................................................................................Page 3 Surface Water Samples Detected Above Standards......................................................................................................................................................................................................Page 4 CorrectiveAction Update.........................................................................................................................................................................................................................................................................................Page 4 MNA Analysis (AOCs Northern, Southern and MW-11)...................................................................................................................................................................................Page 4 Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern)....................................................................................................Page 4 MW-I I AOC Investigations................................................................................................................................................................................................................................................................................Page 5 Groundwaterand Surface Water Characterization..........................................................................................................................................................................................................Page 5 Findings..................................................................................................................................................................................................................................................................................................................................................Page 5 Closing....................................................................................................................................................................................................................................................................................................................................................Page 6 Topographic Map with Site Location................................................................. Single Event Potentiometric Map of Uppermost Aquifer FIGURES 1 2 Total Cumulative VOC Concentrations Pre/Post Injection Comparison..........................................................................................................................Figure 1 Total Cumulative VOC Concentrations Time Series Graphs/Table.........................................................................................................................................Figure 2 TABLES GroundwaterMonitoring Well Construction Table....................................................................................................................................................................................................Table 1 FieldObservations of Monitoring Locations.........................................................................................................................................................................................................................Table 2 FieldParameter Data Summary ................................................................................................................................................................................................................................................................_Table 3 Samplingand Analysis Summary ............................................................................................................................................................................................................................................................Table 4 Groundwaterand QC Sample Detections..................................................................................................................................................................................................................................Table 5 SurfaceWater Sample Detections............................................................................................................................................................................................................................................................Table 6 Hydrologic Properties at Monitoring Well Locations.............................................................................................................................................................................................Table 7 APPENDICIES Laboratory Analysis Report and Chains of Custody................................................................................................................................................................................_Appendix A FieldSampling Parameter Data Sheet(s).......................................................................................................................................................................................................................Appendix B Introduction On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this Semi - Annual Water Quality Report with Corrective Action Update for the Spring 2020 event performed at the Surry County closed construction and demolition (C&D) and closed municipal solid waste landfill (MSWLF)-Mount Airy. NCDEQ Solid Waste Rules 15A NCAC 13B.1632 requires that Surry County provide this report to the NC Solid Waste Section (SWS) on a semi-annual basis. This report documents the quality of the ground and surface waters during an event performed on June 25, 2020. During this event laboratory analytical results indicate Appendix I constituents continue to persist in concentrations above groundwater compliance Standards in samples collected from nine monitoring wells. Total zinc was detected in a surface water sample above established NC 2B Standards. Corrective action to remediate VOCs in groundwater is ongoing within all three areas of concern (AOC) as described in the most recent Corrective Action Evaluation Report (CAER) and improvement has been observed with updated information presented herein. Background The Surry County closed C&D and MSWLF, permit #86-02, is located at 237 Landfill Road in Mt. Airy North Carolina. The site location topographic map is depicted in the attached Sheet 1. Prior to becoming a C&D landfill the site operated as an unlined sanitary landfill that consisted of two units. The northern unit was closed prior to October 1991. The southern unit is comprised of two contiguous portions. The first part stopped receiving waste prior to October 1991 and the second part stopped receiving waste prior to January 1, 1999. Both portions of the southern unit were properly closed with a low permeability cohesive cap per the Transition Plan. The top portion of the southern unit served as an exclusive C&D landfill until prior to June 1, 2008 at which time it was properly closed with another cohesive cap in accordance with the Closure Plan. For continuity, both the northern and the southern units are monitored and reported together. An Alternative Source Demonstration (ASD) which established Site Maximum Allowable Contaminate (SMAC) regulatory compliance levels for three metals (cadmium, cobalt, vanadium) was approved by the NCDEQ on April 20, 2020 (FID 11395468). Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available since 1994. This event was performed in accordance with the NC SWS rules/regulations as promulgated in 15A NCAC 13B and as a condition of the post -closure portion of the permit to operate and memorandums this report contains sampling procedures, field and laboratory results, groundwater and surface water characterization, and findings. This report also contains a table of detections compared to Standards, field data results table, groundwater flow directions/rates table, field observations of the monitoring network table, a potentiometric map of the uppermost aquifer, histograms of historical detections, statistical trend analysis, laboratory analytical reports with chains -of - custody (C-O-C) and quality assurance/quality control data. Sampling Procedures The water quality monitoring program, current as of this event date, includes sampling locations and parameters as outlined in the Water Quality Sampling and Analysis Plan (SAP) (DIN:1320110 dated April 2019 and approved by the SWS (DIN: 1320181) on May 1, 2019. Monitoring locations are shown on the enclosed potentiometric map (Sheet 2). MESCO personnel collected water samples from 18 downgradient groundwater monitoring wells (MW-3R, MW-4, MW-6 through MW-11, MW-125, MW-13 through MW-17 and MW-19 through MW-23), one background well (MW-1), one newly installed water supply well (WSW-2) and four surface water locations (SW-1, SW-2, SW-3 and SW-4). Data from three surface water points (SWN-1, SWN-2 and SW-C) designated in the Water Quality Monitoring Plan for the adjacent lined MSWLF are presented because both permitted landfills share discharge areas. Quality control measures implemented during this event included the quantification of potential artifact contaminants via equipment (EB) and field (FB) blanks. Samples were not analyzed from the six injection wells (IW-1), (IW- 2/MW-2), (IW-3/MW-3RS), (IW-4/MW-4), (IW-5/MW-5) and (IW-6/MW-8) since they are exempt due to the presence of injectant residue which would yield unrepresentative water quality results. Additionally a sample was not analyzed from MW-12S since recharge was limited hence would not be representative. A summary of the construction of the water monitoring wells is presented on Table 1. The function and integrity of all monitoring locations were visually evaluated as documented on Table 2. The depth to water in each well was electronically gaged prior to purging to quantify the static water level elevation. Low -flow pumping methodology or bailing was utilized to adequately purge the wells to a minimum of three times the volume of standing water in the well or until dry. Surface water samples were collected from Stoney Creek discharge feature at previously designated locations. During well purging and surface water sample collection the required field parameters were recorded. The samples were then placed into laboratory -prepared, pre -preserved containers via a new disposable polyethylene bailer. Samples were collected, kept on ice, and transported to a NC -certified laboratory under proper C-O-C protocols within the specified hold times for each analysis. Field Parameter Data Stabilized field parameters were recorded during purging which included depth to water, pH, temperature, specific conductance and turbidity. The field parameter data indicates the monitored groundwater is slightly acidic with relatively low specific conductance which is generally consistent relative to each other and congruent with data historically reported. Field parameter data recorded at the surface water locations had low specific conductance and neutral pH which is consistent with uncontaminated water. A summary of the field parameter data is presented in Table 3 and the field sampling data sheet is enclosed in Appendix B. Laboratory Results Pace Analytical Laboratory (PACE) performed the laboratory analysis of water samples for the total recoverable constituents listed in 40 CFR Appendix I and 1,4-dioxane. As part of assessment monitoring MW-20 was tested for an expanded list of parameters found in 40 CFR Appendix II and 1,4-dioxane since contaminants have been recently detected above Standards. A sampling and analysis table summarizing the locations, constituents, and methods is presented on Table 4. Laboratory results and C-O-Cs are contained in Appendix A. 2 Water samples were analyzed to the laboratory -established Method Detection Limits (MDL) and any value between the MDL and laboratory -established Reporting Limit (RL) is qualified by the laboratory as an estimated concentration hence qualified with a "J". Estimated concentrations are considered non -quantifiable and discretion should be made prior to making decisions based solely on an approximate value. Table 5 summarizes constituents detected in groundwater and QC samples compared to groundwater compliance standards which include Interim Maximum Allowable Concentrations (IMAC), North Carolina Groundwater Standards (2L) and Site Maximum Allowable Concentrations (SMAC). Although not applicable for regulatory compliance purposes detections are also compared to the Maximum Contaminant Level (MCL) commonly referenced as the Federal "Drinking Water Standard". Table 6 lists the constituents detected in surface water samples compared to the current version of the Division of Water Quality Surface Water Quality Tables. Quality Control Samples Total cadmium was detected in the EB sample. Arsenic was detected in the laboratory quality control blanks associated with samples MW-3R, MW-6, MW-9 and MW-20, therefore they were flagged by the laboratory. Groundwater Samples Detected Above Standards One to three metals were detected in quantifiable concentrations (> RL) above the NC 2L/IMAC/SMAC Value in samples collected from 8 wells as shown on Table 5 and summarized below. Metals Detected Above RL and 2L/SMAC Values in Groundwater Ar Co Tl arsenic cobalt thallium 2L/SMAC 10 11 0.28 MW-3R 13.8 MW-6 36 0.53 MW-7 56 MW-9 10.6 286 0.35 MW-11 15.8 MW-16 289 0.31 MW-20 122 0.72 MW-22 53.6 Concentrations in ug/L. VOC(s) were detected in quantifiable concentrations (> RL) above the NC 2L Standard in samples collected from four wells as shown on Table 5 and summarized below. VOC(s) Detected Above 2L Standards in Groundwater 1,2-DCA Benzene VC 2L STD. 0.4 1 0.03 MW-9 1.3 10.3 MW-15 1.6 MW-16 1.2 1.2 MW-20 1.1 3.1 Concentrations in ug/L, 3 The majority of the monitoring locations that were found to contain VOCs included a mixture of dissolved phase aromatic hydrocarbons and chlorinated aliphatic hydrocarbons. The only constituent which originated from an anthropogenic source in levels above the EPA established maximum contaminant levels (MCLs) primary "Drinking Water Standards" was vinyl chloride in samples MW-9 and MW-20. A site map depicting the concentrations and estimated horizontal extent of VOCs that exceeded the 2L Standard during this event is presented on Sheet 2. Surface Water Samples Zinc was detected in sample SW-3 at 44.9 ug/L which is above it's calculated 2B Standard (29.97 ug/L). Corrective Action Update Groundwater remediation continues to be implemented per the approved Corrective Action Plan (CAP) at the three designated areas of concern (AOC) (Northern, Southern and MW-11). A second Corrective Action Evaluation Report (CAER) (DIN: 1320112) was submitted on April 30, 2019 which demonstrated that groundwater conditions continue to improve, except for area near MW-9, which was approved by the SWS on May 1, 2019 (DIN:1320182). A historical summary of corrective actions performed to date are briefly described in the following sections. MNAAnalysis (AOCs Northern, Southern and MW-11) Semi-annual MNA monitoring of a subset of 12 wells for the full suite of SWS recommended parameters was initiated on May 18, 2010 and performed for four consecutive semi-annual events to establish a baseline. A revised SAP prescribing 7 wells with various targeted MNA constituents was approved by the SWS and initiated during an event performed in May 2013. MNA monitoring was limited to field parameters (turbidity) during this event as presented on Table 3. Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern) Per the SWS approved Corrective Action Plan enhanced bioremediation via substrate and tracer injection was initiated in the Southern and Northern AOCs in accordance with requirements outlined in the Injection Well Permit Application and Well Permit No. WI0400176 (5/6/11) in an effort to reduce low level aliphatic and aromatic chlorinated hydrocarbons in groundwater to below the 2L Standards. An edible oil substate (EOS)-water emulsion with sodium bromide tracer was injected into four wells (IW-1, IW-2, IW-3 and IW-5) on November 2-3, 2011. Similar substrates were injected into monitoring wells MW-4/IW-4 and MW-8/IW-6 on October 24-25, 2012. Details of the injection events are provided in the Injection Event Record dated November 4, 2011 and January 10, 2013. As directed in the UIC Injection Well Permit renewed on April 15, 2013 semi-annual post -injection water quality monitoring of wells located downgradient of viable injection points (MW-3R, MW-7, MW-9, MW-12S, MW-13, MW-14, MW-15, MW-16, MW-17, MW-18, MW-19, MW-20, MW-21, MW-22, MW-23) and upgradient background well MW-1 was also performed in conjunction with this semi-annual event. Total aggregate VOC concentrations reported during this event were lower at all locations and an increasing trend is not evident when compared to the respective moving averages of the five events preceding injection in the selected wells downgradient of the injection points (Figure 1). 4 MW-11 AOC Investigations The CAP designated MW-11 as an area of concern due to detections of VOCs detected in exceedance of 2L Standards. MW-11 is located within the compliance boundary near the northern property line which is hydraulically upgradient of the closed northern landfill. The northern landfill closed before October 1991 which was before adoption of NC Section .1600 rules that address assessment and corrective action. VOCs have historically been detected in excess of the 2L Standard at MW-11 which include a mixture of aromatics (fuel hydrocarbons) and chlorinated hydrocarbons (solvents). VOCs were not detected above allowable Standards in samples collected from MW-11 for the third consecutive event which is an improvement compared to previous events. MNA will continue at MW-11 and substrate injection is no longer planned nor required as described in the most recent CAER. Groundwater and Surface Water Characterization A potentiometric map constructed from water elevations taken from the uppermost aquifer which consists of both saprolite and the hydraulically connected upper portion of the fractured bedrock system is enclosed as Sheet 2. Groundwater flow directions and velocity rates were calculated through modified Darcy's equation as shown on Table 7. Consistent with previous events the groundwater apparently flows in a general southeasterly direction towards the tributaries of the Ararat River. The calculated average linear velocity of groundwater indicates an approximate average of 1,311 ft/yr in the wells screened in regolith and 373 ft/yr in the wells screened in the bedrock. The consistent disparity in flow rates between wells is indicative of heterogeneous geologic conditions and/or a product of the limitations of the linear velocity equation when applied to anisotropic conditions which are characteristic of the geology of the Piedmont. Streams located within the facility boundaries were observed to be of moderate volume and flow with low turbidity. Findings One or more Appendix I constituent(s) were detected above allowable compliance levels in samples collected from the uppermost aquifer at nine locations (MW-3R, MW-6, MW-7, MW-9, MW-11, MW-15, MW-16, MW-20 and MW- 22) and Stoney Creek at SW-3. Since the October 2018 event the plume appears to have advanced from the northern AOC to beyond MW-20. All VOC concentrations remain within their own respective historically identified range. The concentrations of arsenic reported during this event were unprecedented in samples MW-3R, MW-6, MW-9, MW-20 and WSW-2. These detections are suspected to be false positive or high bias since it was also detected in the associated lab blank. Results of future analysis should determine the validity of the arsenic detections. Qualitative evaluation of VOC concentrations indicates a general decreasing trend over time and distance from the landfill. During this event total cumulative VOC concentrations decreased compared to their respective five event averages preceding corrective action at most locations (Figure 2). Results of statistical temporal trend analysis, using Sen's Slope Estimator at a 95% confidence level indicate that none of the individual well's cumulative VOC concentrations have increased compared to when corrective action began 8 years ago except for MW-9. The Southern AOC and site -wide cumulative VOC levels continue to exhibit a decreasing trend. The area of the uppermost aquifer beyond the compliance boundary containing quantifiable concentrations of VOCs in exceedance of the 2L Standard during this event is estimated at 0.0 acres in the Northern AOC, 0.0 acres in the MW-11 AOC and 4 acres in the Southern AOC for a total facility wide area of approximately 4 acres (Sheet 2). The total area impacted beyond the compliance boundary has retracted an estimated 50% (from 8 acres to 4 acres) 5 compared to when corrective action was initiated 10 years ago and remains the same as the previous event. Evaluation of the most current water quality data continues to support assertions drawn in previous reports. A few VOCs persist in the upper portion of the aquifer but concentrations are decreasing over time and distance away from the landfill. Samples collected from the local discharge features, which are all located within the property boundaries, continue to lack contaminates above allowable levels. Data continues to indicate that the plumes within each AOC have stabilized and/or decreasing and there is adequate evidence that groundwater is naturally attenuating. Corrective action will continue per the approved CAP with amendments described in the latest CAER. Closing Water quality monitoring and corrective action which consisted of targeting MNA and assessment parameters was performed in December 2020. Sheets Topographic Map with Site Location Surry County Landfill, Mt. Airy fl 237 Landfill Road Mount Airy, NC 28621 Lat: 36-26-30.065 Long:-80-34-15.314 Northing:983356.18 Easting:1537885.48 0 Surry Co Property Line O Closed Unlined C&D Landfill O Closed Unlined Sanitary Landfill O Active Lined MSW Landfill SHEET 1 NOW OR FORMERLY OWNED BY JOHNNY COX SWN-1 (--350 FT UPSTREAM) 1050 1100 10 INACTIVE LINED � PHASE 1 PTO 12/1 /98 MONITORED SEPERATELY 100000 \ ACTIVE LFG EXTRACTION MW-9 Benzene - 1.3 ry ll Chloride - 10.3 Bnezene - 1. inyl Chlori 237 LANDFILL ROAD D IW-6 -n� --O'--GWE=1049.00 —< GWE=1062.05 —MW--20 Im --d—WE=1063.63 ��yo SW-2 sw MW-6 / , GWE=1045. i r I IW-3 GWE=989.7 %GWE7974.87� W 16 /GWE=977.75 NOMMOMW-16 ,2-Dichloroethane - 1.2 �1 SW-3 sw MW-17 GWE=955.45 o' MW-11 `- GWE1129.51 � SCALEHOUSE < W� r7jo 1 1MW--7 ' GWE=1062.40 I � 10 GWE \j070 ,1 I o CLOSED UNLINED MSW (8602-MSWLF-1983) STOPPED RECEIVING WASTE BEFORE OC I OBER 9, 1991 ACTIVE LCID (NO PERMIT) <2 ACRES 1 1 / 1 1 WSW-2 w/ vv-1 GWE=1111.24 ` TIRES BURIED UNDER SOIL AND GRASS I CLOSED UNLINED C&D(8602-CDLF-2001) STOPPED RECEIVING C&D BEFORE JUNE 30, 2008 CLOSURE REQUIREMENTS COMPLETED BEFORE MAY 3C I / / / CLOSED C&D OVER CLOSED UNLINED MSW (8602-CDLF ON TOP OF MSW) STOPPED RECEIVING C&D BEFORE MARCH 3, 2006 STOPPED RECEIVING MSW BY JAN. 1, 1999 LFG EXTRACTION SYSTEM MW-12D* IW--2 ^ GWE=>1027.05 / GWE= "': MW--12S ,GWE=1012.78 ARO��� MW-18 / T y</NF � GWE=974.19 M- / � W-13 GWE=984.00 GWE= / / sw SW-1.- / ' PROPERTY LINE MW--14 AO O GWE=985.68 MW-21 6WE=960.41 r / df 0 o° ,moo MW-15 mil (-hlnri MW-23 Mw MW-15 v / GWE948.03 GWE=1026.40 -- - - o GWE=937.03 l SW-4 1 LAGOON / SWN-2 (-1,420') & SW-C (-450') i / DOWNSTREAM) NOW OR FORMERLY OWNED BY SHAWNA SUMMERS LEGEND EXISTING TOPOGRAPHIC CONTOURS EXISITING ROAD/PATH EXISTING CHAINLINK FENCE EXISTING STRUCTURE PERENNIAL CREEK, STREAM, ETC. INTERMITTANT CREEK, STREAM, ETC. PROPERTY LINE LINED MSWLF PHASE LIMITS — — — — — — — — — — UNLINED WASTE LIMITS (APPROXIMATE) — COMPLIANCE BOUNDARY 1060 POTENTIOMETRIC GROUNDWATER CONTOUR (JUNE 2020) GWE = 2626.85 GROUNDWATER POTENTIOMETRIC ELEVATION *MW- ELEVATION NOT USED FOR CONTOURING ESTIMATED EXTENT OF VOC VIOLATIONS (JUNE. 2020) BEYOND COMPLIANCE BOUNDARY (-4 ACRES) sw SURFACE WATER SAMPLING LOCATION na: MONITORING WELL EXISTING iw INJECTION WELL EXISTING WATER SUPPLY WELL EXISTING (APPROXIMATE LOCATION) GRAPHIC SCALE 0 100 200 400 ( IN FEET ) 1 inch = ft. SHEET 2 800 L9Q N r, Z0. ■ � N l0 0� N l0 W �N W ;a; N °° Z ZZ °W� a o 00 _ fn a m = N 1_I Z � N `n . 0 Ll w w 0 N V002 0m L3L3 Z N 71 Z J w W Z ZW En Z Q U] <WW Q L7 Z ° U a W wm ° J - °m Z> a/ m 3 X m W = O En ul to a mftft J J J J� O � L OC QQZ= J J � I► 0a cn V O 0 cc T W 0 cc cc Lu Z O J � � O LL- Q � z ° a � Q N Q C � z O CL O Q m Q U � z OLu K W U Lu m W z o U O O o C SCALE: SEE SCALE BAR DATE: 811120 DRWN. BY: J. PFOHL CHKD. BY: B. CLAWSON PROJECT NUMBER DRAWING NO. SHEET NO. SHEET 2 1 OF 1 Figures Figure 1 Total Cumulative VOC Concentrations Pre/Post Injection Comparison October 22, 2009 - June 25, 2020 DOWNGRADIENT OF IW-2 (TOTAL CUMULATIVE VOC CONCENTRATIONS) s.mkox: ��nv.,s ovxns DOWNGRADIENT OF IWA (TOTAL CUMULATIVE VOC CONCENTRATIONS) s.meou. �uws o�+a nrrvza DOWNGRADIENT OF IW-7 (TOTAL CUMULATIVE VOC CONCENTRATIONS) s.meoa. �M,v.m or�vax DOWNGRADIENT OF IW-5 (TOTAL CUMULATIVE VOC CONCENTRATIONS) s�oemx Baseline Period (Oct. 2009-Oct. 2011) Difference Difference Average of Between Between first Five Corrective Most Most Statistical Oct May Oct May Oct Action June Recent & Recent & Trend* Between 2009 2010 2010 2011 2011 Events 2020 Baseline Baseline Oct. 2009-June Well ID (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (uq/L) (uq/L) (D/D) 2020 INJECTION WELL (IW-1) UNSUCCESSFUL INJECTION SO DOWNGRADIENT WELLS NOT SHOWN INJECTION WELL (IW-2) MONITORED DOWNGRADIENT BY MW-12S & MW-13 MW-12S 0.00 0.00 0.00 0.00 5.40 1.08 0.00 0.00 0 HNo TrendH MW-13 61.00 50.60 74.20 87.30 72.50 69.12 12.21 -56.91 -82 �Downward� INJECTION WELL (IW-3) MONITORED DOWNGRADIENT BY MW-3R & MW-16 MW-3R 0.00 0.00 1 0.00 1 0.00 0.00 0.00 2.15 2.15 100 HNo TrendH MW-16 1137.90 113.60 135.70 1121.20 116.30 124.94 14.66 -110.28 -88 . Downward. INJECTION WELL (IW-4) MONITORED DOWNGRADIENT BY MW-14, MW-21 & MW-23 MW-14 15.20 15.60 15.60 8.20 17.00 14.32 4.40 -9.92 -69 HNo TrendH MW-21 52.10 50.70 51.38 39.10 32.41 45.14 13.93 -31.21 -69 �Downward� MW-23 4.30 0.00 0.00 0.00 0.00 0.86 0.51 -0.35 -41 HNo TrendH INJECTION WELL (IW-5) MONITORED DOWNGRADIENT BY MW-15 & MW-19 MW-15 96.13 63.89 55.00 78.10 64.06 71.44 30.70 -40.74 -57 �Downward� MW-19 0.00 0.00 0.00 0.00 0.00 0.00 2.09 2.09 100 HNo TrendH INJECTION WELL (IW-6) NOT SHOWN AS NO WELLS DOWNGRADIENT WITHIN ZONE OF INFLUENCE * = Statistical Trend analysis via Sen's Slope Estimator at a 95% confidence level Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Figure 2 Total Cumulative VOC Concentrations Time Series Graphs/Table October 22, 2009 - June 25, 2020 Total Cumulative VOCs (SOUTHERN AOC) s.�meom eva.,. n 1.a.,.:, ova.,. o 1. Total Cumulative VOCs -0- Total Cumulative VOCs (NORTHERN AOC) AOC Well ID Oct 2009 May 2010 Oct 2010 May 2011 Oct 2011 Average of first Five Corrective Action Events June 2020 Difference Difference Statistical Trend (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) N Oct 2009 -Dec. 2019 Background MW-1 0.00 0.00 0.00 0.00 0.00 0.00 0 0.00 0 No Trend IW-2 (MW-2) 105.25 207.00 207.93 159.90 79.10 151.84 79.10 NS NS NS No Trend IW-3 (MW-3RS) 202.90 127.50 127.50 144.00 127.60 145.90 127.60 NS NS NS No Trend MW-3R 0.00 0.00 0.00 0.00 0.00 0.00 0 0.00 0 No Trend IW-4 (MW-4) 27.00 24.20 24.20 27.60 23.50 25.30 18.10 NS NS NS No Trend IW-5 (MW-5) 35.00 46.50 46.50 47.40 34.80 42.04 34.80 NS NS NS No Trend MW-12S 0.06 0.00 0.00 0.00 5.40 1.08 0.00 -1.08 -100 No Trend MW-12D 0.00 0.00 0.00 0.00 0.00 0.00 0 NS NS NS No Trend MW-13 61.00 50.60 74.20 87.30 72.50 69.12 12.21 -56.91 -82 Downward Southern MW-14 15.20 15.60 15.60 8.20 17.00 14.32 4.4 -9.92 -69 Downward MW-15 96.13 55.00 55.00 78.10 64.06 69.66 30.7 -38.96 -56 Downward MW-16 137.90 113.60 135.70 121.20 116.30 124.94 14.66 -110.28 -88 Downward MW-17 20.34 8.40 8.85 0.00 5.77 8.67 0 -8.67 -100 No Trend MW-18 0.00 0.00 0.00 0.00 0.00 0.00 0 NS NS NS No Trend MW-19 0.00 0.00 0.00 0.00 0.00 0.00 2.09 2.09 100 No Trend MW-21 52.10 50.70 51.38 39.10 32.41 45.14 13.93 -31.21 -69 Downward MW-22 28.90 23.80 23.80 11.66 5.20 18.67 2.93 -15.74 -84 Downward MW-23 4.30 0.00 0.00 0.00 0.00 0.86 0.51 -0.35 -41 No Trend Combined Total 786.02 722.90 770.66 724.46 583.64 717.54 341.03 -376.51 -53 Downward MW-6 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 -100 No Trend MW-7 7.40 9.40 11.20 9.70 8.80 9.30 1.18 -8.12 -87 Downward Northern IW-6 (MW-8) 22.00 23.90 16.00 12.30 12.60 17.36 10.20 NS NS NS No Trend MW-9 23.50 20.40 23.20 25.80 22.90 23.16 44.04 20.88 90 Upward MW-20 0.00 0.00 0.00 0.00 0.00 0.00 14.05 14.05 100 No Trend Combined Total 52.90 53.70 50.40 47.80 44.30 49.82 69.47 19.65 39 No Trend MW-11 MW-11 10.10 6.00 6.00 5.44 23.20 10.15 0.34 -9.81 -51 No Trend SITEWIDE Combined Total 849.02 782.60 827.06 777.70 651.14 777.50 410.84 -366.66 -47 Downward "5 = Not sampled this event so most recent concentration shown and used in calculations * = Statistical trend analysis via Sen's Slope Estimator on original and transformed log -normal at a 95% Confidence Level Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Tables Table 1 Groundwater Monitoring Well Construction Table June 24-25, 2020 Monitoring Well Date Installed Well Diameter Total Well Depth Top of Screen Depth Screen Length Geology of Screened Interval Top of Casing Elevation Ground Elevation Groundwater Elevation Depth to Water Latitude Longitude (inches) (ft bgs) (ft bgs) (ft) (ft amsl) (ft amsl) (ft amsl) (ft btoc) MW-1 11/28/89 2 40 30 10 Clay 1134.35 1133.15 1111.24 23.11 36.439211 -80.568133 0-2 (was MW-2) 11/28/89 2 70 60 10 Clay 1068.86 1068.36 1029.95 38.91 36.435833 -80.568894 MW-3R 9/27/94 2 101 86 15 Rock 1017.50 1015.00 977.75 39.75 36.434725 -80.571989 IW-3 (was MW-3RS) 5/17/01 2 52 37 15 Rock 1020.57 1018.24 989.78 30.79 36.434656 -80.571858 IW-4 (was MW-4) 8/30/94 2 55.4 40.4 15 Rock 1026.26 1025.06 NR NR 36.434686 -80.569200 0-5 (was MW-5) 8/27/94 2 63 48 15 Rock 1080.18 1077.78 NR NR 36.434614 -80.570436 MW-6 9/7/94 2 29.7 14.7 15 Rock 1067.67 1065.61 1045.38 22.29 36.437431 -80.571067 MW-7 8/23/94 2 23 8 15 Rock 1073.50 1071.50 1062.40 11.10 36.438439 -80.570722 IW-6 (was MW-8) 8/16/94 2 54 39 15 Rock 1088.45 1086.45 1049.00 39.45 36.439278 -80.570381 MW-9 8/22/94 2 43.8 28.8 15 Rock 1094.07 1092.07 1062.05 32.02 36.439289 -80.571508 MW-11 8/15/94 2 40 25 15 Rock 1151.80 1150.40 1130.93 20.87 36.441589 -80.569558 MW-12S 5/31/01 2 51 11 40 Rock 1025.80 1023.25 1012.78 13.02 36.435942 -80.567972 MW-12D 5/30/01 2 100 90 10 Rock 1027.05 1023.75 1027.05 0.00 36.435964 -80.567994 MW-13 5/30/06 2 35.78 20.78 15 Saprolite 1008.48 1005.75 984.00 24.48 36.435036 -80.568183 MW-14 5/30/06 2 48.03 33.03 15 Rock 1018.80 1016.11 985.68 33.12 36.434267 -80.569239 MW-15 6/22/06 2 57 42 15 Rock 1075.96 1073.23 1026.40 49.56 36.433797 -80.570467 MW-16 6/21/06 2 36.3 21.3 15 Rock 999.54 996.67 974.87 24.67 36.434536 -80.572117 MW-17 6/1/07 2 15.32 5.32 10 Rock 965.43 962.26 955.45 9.98 36.433558 -80.572517 MW-18 6/1/07 2 18.15 8.15 10 Saprolite 983.00 980.00 NR NR 36.435453 -80.567050 MW-19 6/1/07 2 17.1 7.1 10 PWR 946.27 942.97 937.03 9.24 36.432231 -80.570556 MW-20 6/1/07 2 25.64 10.64 15 Rock 1082.19 1079.12 1063.63 18.56 36.439025 -80.571650 MW-21 6/1/07 2 15.41 5.41 10 Saprolite/PWR 965.36 962.22 960.41 4.95 36.434214 -80.568717 MW-22 6/1/07 2 16.04 6.04 10 Saprolite 953.40 950.23 948.95 4.45 36.432928 -80.571678 MW-23 6/1/07 2 17.1 7.1 10 Sandy Silt 955.31 952.09 948.03 7.28 36.432828 -80.569156 NOTE: bgs = below ground surface amsl= above mean sea level btoc = below top of casing (PVC well casing) Slurry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1 Table 2 Field Observations of Monitoring Locations June 24-25, 2020 Location Viable Monitoring Location Lack of Any Evidence of Tampering Locked on Arrival & Departure Hinge/Hasp Operational Tagged or Labeled Concrete Surface Pad Appears Effective Comments MW-1 Yes Yes Yes Yes Yes Yes IW-1 No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. IW-2 (was MW-2) No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. No pad visible MW-3R Yes Yes Yes Yes Yes Yes IW-3 (was MW-3RS) No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. IW-4 (was MW-4) No Yes Yes Yes Yes Yes Fouled since injection 10/24/12. IW-5 (was MW-5) No Yes Yes Yes Yes Yes Fouled since injection 11/2/11. Bailer would not descend MW-6 Yes Yes Yes Yes Yes Yes MW-7 Yes Yes Yes Yes Yes Yes IW-6 (was MW-8) No Yes Yes Yes Yes Yes Fouled since injection 10/24/12. MW-9 Yes Yes Yes Yes Yes Yes MW-11 Yes Yes Yes Yes Yes Yes MW-12S No Yes Yes Yes Yes Yes MW-12D Yes Yes Yes Yes Yes Yes Flowing artesian which is typical MW-13 Yes Yes Yes Yes Yes Yes MW-14 Yes Yes Yes Yes Yes Yes MW-15 Yes Yes Yes Yes Yes Yes MW-16 Yes Yes Yes Yes Yes Yes Red purge water MW-17 Yes Yes Yes Yes Yes Yes MW-18 Yes Yes Yes Yes Yes Yes MW-19 Yes Yes Yes Yes Yes Yes MW-20 Yes Yes Yes Yes Yes Yes MW-21 Yes Yes Yes Yes Yes Yes MW-22 Yes Yes Yes Yes Yes Yes Red purge water MW-23 Yes Yes Yes Yes Yes Yes SW-1 Yes SW-2 Yes Moderate gage height & flow SW-3 Yes Moderate gage height & flow SW-4 Yes Moderate gage height & flow SW-c Yes Moderate gage height & flow SW N-1 Yes Moderate gage height & flow SWN-2 Yes Moderate gage height & flow SCALEHOUSE No Sample taken from new WSW instead Any unusual field conditions, observations, or events: Injection wells (IW-1, IW-2, IW-3, IW4, IW-5 and IW-6) exempt from laboratory analysis as approved by NC SWS on May 10, 2013 (DIN:18938) Visual markers (10 ft PVC pipes) remain secured to each monitoring well case Slurry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1 Table 3 Field Parameter Data Summary June 24-25, 2020 Parameter Depth to Water Water Elevation TOC Elevation Temp. pH Hardness Specific Conductance Turbidity Units ft (btoc) ft (amsl) ft (amsl) C SU mg/L umhos/cm NTU MW-1 23.11 1111.24 1134.35 15.0 5.97 NR 33 3.34 IW-2 38.91 1029.95 1068.86 NR NR NR NR >1000 MW-3R 39.75 977.75 1017.50 15.4 6.99 NR 235 8.92 IW-3 30.79 989.78 1020.57 NR NR NR NR >1000 IW-4 NR NR 1026.26 NR NR NR NR >1000 IW-5 NR <1040.18 1080.18 NR NR NR NR NR MW-6 22.29 1045.38 1067.67 14.1 6.21 NR 158 8.11 MW-7 11.10 1062.40 1073.50 14.4 5.68 NR 255 0.87 IW-6 39.45 1049.00 1088.45 NR NR NR NR NR MW-9 32.02 1062.05 1094.07 15.8 6.18 NR 435 6.61 MW-11 22.29 1129.51 1151.80 16.4 6.36 NR 108 8.01 MW-12S 13.02 1012.78 1025.80 15.9 6.64 NR 280 18.3 MW-12D 0.00 >1027.05 1027.05 NR NR NR NR NR MW-13 24.48 984.00 1008.48 14.6 6.03 NR 137 6.53 MW-14 33.12 985.68 1018.80 13.9 5.32 NR 68 1.62 MW-15 49.56 1026.40 1075.96 14.9 5.41 NR 95 20.4 MW-16 24.67 974.87 999.54 14.4 5.83 NR 431 8.38 MW-17 9.98 955.45 965.43 14.1 6.37 NR 240 3.96 MW-18 8.81 974.19 983.00 NR NR NR NR NR MW-19 9.24 937.03 946.27 14.9 5.58 NR 47 6.30 MW-20 18.56 1063.63 1082.19 13.9 5.52 NR 111 65.9 MW-21 4.95 960.41 965.36 13.6 5.17 NR 151 14.9 MW-22 4.45 948.95 953.40 16.9 5.92 NR 297 12.0 MW-23 7.28 948.03 955.31 13.9 5.49 NR 45 7.99 Scalehouse na na na 17.5 7.01 NR 143 NR Minimum 0.00 937.03 946.27 13.6 5.17 NR 33 0.86 Average 21.27 1010.88 1034.58 15.0 5.98 NR 182 153 Maximum 49.56 1129.51 1151.80 17.5 7.01 NR 435 >1000 SW-1 - - - 17.1 6.51 20 58 9.66 SW-2 - - - 19.1 6.52 20 83 9.20 SW-3 - - - 18.1 6.81 20 332 37.9 SW-4 - - - 18.3 6.82 30 63 9.55 SW-C 17.8 7.01 20 119 10.0 SWN-1 - - - 17.2 7.73 20 121 6.52 SWN-2 - - - 17.9 7.81 20 132 8.25 Minimum - - - 17.1 6.51 20 58 6.52 Average - - - 17.9 7.03 21 130 13.01 Maximum - - - 19.1 7.81 30 332 37.9 btoc = Below top of casing amsl = Above mean sea level na = Not available NR = No reading attempted Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1 Table 4 Sampling and Analysis Summary June 24-25, 2020 App. I Other App. II Field Parameters a a Q = w U n O aj a m (0 f6 U O Q a7 O a a) _ ❑ w Cc = n y U a) Q o Q m x 0. Q k° a) >. .0 N w N U as uJ U as 2 E rn M D '- p_ E c C '� O o v_ O o a`) a) a> o� a) o Co 2� > H > H S U a H In H U S n H 0 0 O O 0 0 0 0 N 0 Q 0 0 v 0 Y N 00CD N W W N W W O O I W N m L N N w w w w W w W w to a -0 m C9 .0 m m z m z m z a z aJcc J J J J J M MJJ LL IW-1 Not sampled since exempt per NC SWS approved WQMP MW-1 X X I X I I I X X X X IW-2 Not sampled since exempt per NC SWS approved WQMP MW-3R X X I X I I I X X X X IW-3 Not sampled since exempt per NC SWS approved WQMP IW-4 Not sampled since exempt per NC SWS approved WQMP IW-5 Not sampled since exempt per NC SWS approved WQMP MW-6 X X X X X X X MW-7 X X X X X X X IW-6 Not sampled since exempt per NC SWS approved WQMP MW-9 X X X X X X X MW-11 X X X X X X X MW-12S X X X X X X X MW-12D Not sampled since exempt per NC SWS approved WQMP MW-13 X X X X X X X MW-14 X X X X X X X MW-15 X X X X X X X MW-16 X X X X X X X MW-17 X X X X X X X MW-18 Not sampled since exempt per NC SWS approved WQMP MW-19 X X X X X X X MW-20 X X X X X X X X X X X X X X MW-21 X X X X X X X MW-22 X X X X X X X MW-23 X X X X X X X Scalehouse X X X X X X SW-1 X X X X X X X X SW-2 X X X X X X X X SW-3 X X X X X X X X SW-4 X X X X X X X X SW-C X X X X X X X X SWN-1 X X X X X X X X SWN-2 X X X X X X X X EB X X X FB X X X App I & II Lists = hrom current 40 GFH 258 Eight wells exempt from lab testing per NC SWS approved WQMP [FIDA3201811 Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1 Table 5 Groundwater and Quality Control Sample Detections June 23-25, 2020 Parameter Name MDL RLBG MW-1 111l MW-6 MW-7 MW-9 MW-11 MW-12S MW-13 MW-14 MW-15 MW-16 fil fil MW-20 MW-21 MW-22 MW-23 WSW-2 EB FB =St-dard S S S S S S S S S S S S S S S S WSW Metals (Targeted 40CFR 258 Appendix I Arsenic, total 4.7 10 10 10 13.8 BC (A) 9.7 J BC 10.6 BC (A) 5.8 J BC 7.3 J B Barium, total 3.5 5 700 2000 30.6 42.8 71.3 53.8 43.9 35.8 10.5 66.4 21.1 45.5 68.2 18.9 25.4 50.8 55.7 68.3 22.7 Cadmium, total 0.4 1 8" 5 2.6 2.3 0.721 0.79 J 2 0.79 J 0.42 J 1.8 0.43 J 0.6 J 0.42 J 1 0.89 J 0.47 J Cobalt, total 3.6 5 1 V. NE 36 (L) 56 (L) 286 (L) 15.8 (L) 10.4 289 (L) 122 (L) 3.8 J 53.6 (L) Nickel, total 3.5 5 100 NE 8 12.4 6.9 4.5 J Thallium, total 0.05 0.1 0.28 2 0.53 (N) 0.13 0.35 (N) 0.099 J 0.079 J 0.09 J 0.31 (N) 0.72 (N) 0.13 Selenium, total 4.7 10 20 50 6.2 J Zinc, total 9.5 10 1000 NE 9.7 J 16 21.8 VOCs (Targeted 40CFR 258 pendix I and 1,4-Dionne) 1,1-Dichloroe[hane 0.27 1 6 NE 0.85 0.87 1.1 1.1 4.6 0.44J 0.69JX6.90.51J 1J 1,2-Dichlombenzene 0.29 1 20 NE 1.1 0.34 J 31 J 1,2-Dichloroethane 0.34 1 0.4 5 0.37 0.51 J 0.56 J 1.2 (L) 4 J 1,2-Dichloropropane 0.19 1 0.6 5 0.34 J 0.49 J 1,4-Dichlorobenzene 0.26 1 6 75 0.53 Benzene 0.15 1 1 5 1.3 (L) 0.34 J 0.76 J Bromomethane 0.62 2 10 NE 7 J B Chlomethane 0.49 1 3000 NE 1.1 Chlorobenzene 0.23 1 50 100 0.65 J cis-1,2-Dichloroethene 0.29 1 70 70 1.3 29 10.6 3.3 21.4 10.2 1.4.1 0.51 J Trichloroethene 0.22 1 3 5 2.2 Vinyl chloride 0.24 1 0.03 2 10.3 (L) 1 1.6(L) 1.2 (L) I Turbidity (Field Measured) (NTU) TurbidityNTU 0.01 NE NE 3.34 8.92 8.11 0.87 6.61 8.01 18.3 6.53 1.62 1 20.4 1 8.38 1 3.96 6.3 1 65.9 1 14.9 1 12 7.99 Notes: Units ug/L unless shown otherwise, Blank cells means not detected above MDL, - means parameter not analyzed, NE means not established. Bold Above RL and Established 2L/IMAC/SMAC (Regulatory compliance Standard) Above Established Federal MCL Drinking Water Std. (NOT a regulatory compliance Standard) BG= Background Well Sample, QC = Quality Control Sample, S = Sentinel Well Sample MDL = Adjusted Method Detection Limit established by the laboratory via a statistical calculation. Since the MDL is below the point of calibration, results reported down to the MDL are not reliable and must be qualBed as estimated values and as such, carry a "J" qualifier designation. RL = Reporting Limit dented by Pace laboratory as "The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a spec analyte in a specific mark" 21JIMAC/SMAC = NC 2L, IMAC and SMAC values recognized by the NC SW S as regulatory goundaler Standards. 21- = NC 2L Groundater Standard 15A NCAC 02L.0202 IMAC = Interim Maximum Allowable Concentration SMAC = Site Maximum Allwable Concentration. Approved by NC SW S via ASO April 1, 2020. MCL = Primary Maximum Contaminant Level for drinking water established by the USEPA. J = "J-qualified". Defined by the lab as "estimated concentration above the adjusted method detection limit and below the adjusted reporting limit". BC = The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the laboratory reporting limit. May indicate a false positive. (N) Preliminary source is believed to be Natural originating from erosion of natural deposits. Source not anthropogenic. (L) Prelilminary source is believed to be anthropogenic with Landfill Gas Wor leachale as suspected transport mechanism. (A) Preliminary source is believed to be artifact contamination. High bias or false postive as evidenced by quality control data. A definitive source of the detections was not determined as part of this report. Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1 Table 6 Surface Water Sample Detections June 25, 2020 Parameter Name MDL RL NC 2B STD EPA z NRWQC NC ISTV3 MCL° SWN-1 SW-1 SW-2 SW-3 SW-4 SW-C SWN-2 Up I Down Down Down Down Down Down Targeted 40CFR 258 Appendix I and 1,4-Dioxane Arsenic, total 4.7 10 340 NE NE 10 6.1 J Barium, total 3.5 5 NE NE 21,000 2000 17.7 22.9 26.6 37.4 18 17.8 17.5 Cobalt, total 3.6 5 NE NE 4 NE 29 13.8 Thallium, total 0.05 0.1 NE 0.47 NE 2 0.068 J Zinc, total 9.5 10 29. 77 NE NE NE 44.9 VOCs (Targeted 40CFR 258 Appendix I and 1,4-Dioxane) cis-1,2-Dichloroethene 0.22 1 NE NE 720 70 2.6 Vinyl chloride 0.24 1 2.4 NE NE 2 0.56 J Hardness as CaCo3 (Field Measured) Hardness (mg/L) 20 20 NE NE NE NE 20 20 20 20 30 40 20 Turbidity (NTU) 0.01 50 NE NE 6.52 82.3 9.20 37.9 6.52 10.0 8.25 Notes: Units ug/L unless indicated otherwise, Blank cells means Not Detected, NE means Standard Not Established J = "J-qualified". Defined by the lab as "Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit". BC = The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the laboratory reporting limit. Red Bold Above RL and Applicable Established 26 Std. Above Established Federal MCL Primary Drinking Water Std. MDL = Adjusted Method Detection Limit established by the laboratory via a statistical calculation. Since the MDL is below the point of calibration, results reported down to the MDL are not reliable and must be qualified as estimated values and, as such, carry a "J" qualifier designation. precision and bias for a specific analyte in a specific matrix" Receivina surface waters are Stonev Creek (12-72-12) and Ararat River (12-7244.5) Both Class C. 03040101 (8-Diait HUC). ' NC 2B STD = North Carolina 15A NCAC 02B Water Quality Standards for Surface Waters. Presumed NC SWS adopted the numerical Standard for regulatory compliance purposes 2B Standards from All Waters (C & SC) or Class C. 2B Standard for zinc is determined via a calculation (below) for acute that is dependent upon hardness. Zinc 2B Standard calculation:WER*[0.986*e^{0.8473[In hardness]+0.884)] EPA NRWQC = EPA Nationally Recommended Water Quality Criteria for Aquatic Life & Human Health. Nationally Recommended Water Quality Criteria for which NC does not have a Water Quality Standard for one or more uses NC ISTV= North Carolina In -Stream Target Value. Established per language in 15A NCAC 02B .0202 & .0208. Contact DW R staff for further information. NC ISTV for barium and cobalt fresh water All waters (Class C) MCL= Maximum Contaminant Level. Federal Primary "Drinking Water Standard". Shown for comparison purposes only. Not applicable for regulatory compliance purposes. Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1 Table 7 Hydrogeolofic Properties at Monitoring Well Locations June 24-25, 2020 Well Hydraulic Conductivity Effective Porosity Hydraulic Gradient Groundwater Average Linear Velocity Rate Flow Direction inimum Distance From Upgradient EOW Ground Water Depth Groundwater Potentiometric Elevation Screened Interval Lithology (cm/second) (ft/day) N (feet/feet) (feet/year) (ft) (feet btoc) (feet amsl) MW-1 4.30E-05 0.12 15 0.083 25 N65W 0 23.11 1111.24 Clay IW-2 4.30E-05 0.12 15 - - - 38.91 NR Clay MW-7 8.10E-04 2.30 1 15 0.095 1 532 N64W 1 704 11.10 1062.40 PWR / Fractured Rock IW-6 4.40E-04 1.25 15 0.126 383 S01E - 39.45 1049.00 PWR/ Fractured Rock MW-9 1.90E-04 0.54 15 0.091 119 S38E 614 32.02 1062.05 Sandy Silt MW-13 2.06E-04 0.58 23 0.167 154 S44E 1,850 24.48 984.00 Saprolite MW-18 2.04E-03 5.78 15 0.136 1,907 0 8.81 974.19 Saprolite MW-19 1.10E-03 3.12 3 0.098 3,733 S17W 2,663 9.24 937.03 PWR MW-21 1.28E-03 3.63 3 0.130 5,744 S73E 2,041 4.95 960.41 Saprolite/PWR MW-22 9.88E-04 2.80 15 0.050 341 S30W 2,506 4.45 948.95 Saprolite MW-23 3.04E-04 0.86 1 15 0.081 170 S29E 2,610 7.28 948.03 Sandy Silt Minimum 4.30E-05 0.12 3 0.050 25 0 4.45 937.03 Average 6.77E-04 1.92 14 0.106 1,311 1,443 18.53 1003.73 Maximum 2.04E-03 5.78 23 0.167 5,744 2,663 39.45 1111.24 MW-3R 2.40E-04 0.68 5 na na NR 1,994 39.75 977.75 Fractured Rock IW-3 2.40E-05 0.07 5 0.208 103 S40W - 30.79 989.78 Fractured Rock IW-4 1.10E-04 0.31 5 - NR NR Fractured Rock IW-5 1.50E-05 0.04 5 - - - >40.68 <1039.50 Fractured Rock MW-6 1.90E-05 0.05 5 0.130 51 S77W 963 22.29 1045.38 Fractured Rock MW-11 3.10E-04 0.88 5 0.069 442 S24W 0 22.29 1129.51 Fractured Rock MW-12S na na 3 0.140 na S21E 0 13.02 1012.78 Fractured Rock MW-12D 1.30E-06 0.00 5 -- -- 0 0.00 >1027.05 Fractured Rock MW-14 7.45E-03 21.12 3 0.143 36,705 S75E 2,098 33.12 985.68 Fractured Rock MW-15 7.21E-05 0.20 3 0.092 228 S09E 2,020 49.56 1026.40 Fractured Rock MW-16 2.82E-05 0.08 3 0.164 159 S41W 2,089 24.67 974.87 Fractured Rock MW-17 2.94E-04 0.83 3 0.123 1,252 S68W 2,547 9.98 955.45 Rock MW-20 1.92E-04 0.54 3 0.056 374 S23E 692 18.56 1063.63 Rock Minimum 1.30E-06 0.00 3 0.056 51 0 0.00 955.45 Average 7.30E-04 2.07 4 0.125 373 1,240 24.00 1016.12 Maximum 7.45E-03 21.12 5 0.208 1,252 2 547 49.56 1129.51 NOTES: Values for hydraulic conductivity determined via slug test by GAI, MESCO, or Joyce. Hydrologic gradient from water levels recorded on June 24-25, 2020. Wells screened entirely in rock were not utilized for flow directions/gradients. Screens that traverse both rock and regolith assumed flow in regolith dominates. Hydraulic Conducitivity value and flow rate for MW-14 was considered an outlier; therefore not included in the average or maximum. na = Not available/applicable Average Linear Velocity (Q) is defined by modified Darcy's equation: K A K= hydraulic conductivity where Q ri dl ne = effective porosity e dh=head difference dl= horizontal distance Slurry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1 Appendix A Laboratory Analysis Reports Chains of Custody lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 July 02, 2020 Mr. Jonathan Pfohl Municipal Engineering Services 68 Shipwash Dr. Garner, NC 27529 RE: Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on June 26, 2020. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Steven R. Gandy, Municipal Engineering Services Co. REPORT OF LABORATORY ANALYSIS r e This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Lab ID Sample ID Matrix Date Collected Date Received 92483829001 MW-1 Water 06/25/2014:37 06/26/2014:41 92483829002 MW-11 Water 06/25/2015:03 06/26/2014:41 92483829003 MW-12S Water 06/25/2014:16 06/26/2014:41 92483829004 MW-13 Water 06/25/2014:02 06/26/2014:41 92483829005 MW-14 Water 06/25/2014:00 06/26/2014:41 92483829006 MW-15 Water 06/25/2012:00 06/26/2014:41 92483829007 MW-16 Water 06/25/2011:43 06/26/2014:41 92483829008 MW-17 Water 06/25/2011:03 06/26/2014:41 92483829009 MW-19 Water 06/25/2011:14 06/26/2014:41 92483829010 MW-21 Water 06/25/2014:08 06/26/2014:41 92483829011 MW-22 Water 06/25/2010:59 06/26/2014:41 92483829012 MW-23 Water 06/25/2014:05 06/26/2014:41 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: Surry Closed- Mt. Airy 92483829 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92483829001 MW-1 EPA 6010D SH1 14 PASI-A EPA 6020E BG2 1 PASI-A EPA 8260D CL 51 PASI-C 92483829002 MW-11 EPA 6010D SH1 14 PASI-A EPA 6020E BG2 1 PASI-A EPA 8260D SAS 51 PASI-C 92483829003 MW-12S EPA 6010D SH1 14 PASI-A EPA 6020E BG2 1 PASI-A EPA 8260D CL 51 PASI-C 92483829004 MW-13 EPA 6010D SH1 14 PASI-A EPA 6020E BG2 1 PASI-A EPA 8260D SAS 51 PASI-C 92483829005 MW-14 EPA 6010D SH1 14 PASI-A EPA 6020E BG2 1 PASI-A EPA 8260D SAS 51 PASI-C 92483829006 MW-15 EPA 6010D SH1 14 PASI-A EPA 6020E BG2 1 PASI-A EPA 8260D SAS 51 PASI-C 92483829007 MW-16 EPA 6010D SH1 14 PASI-A EPA 6020E BG2 1 PASI-A EPA 8260D SAS 51 PASI-C 92483829008 MW-17 EPA 6010D SH1 14 PASI-A EPA 6020E BG2 1 PASI-A EPA 8260D SAS 51 PASI-C 92483829009 MW-19 EPA 6010D SH1 14 PASI-A EPA 6020E BG2 1 PASI-A EPA 8260D CL 51 PASI-C 92483829010 MW-21 EPA 6010D SH1 14 PASI-A EPA 6020E BG2 1 PASI-A EPA 8260D SAS 51 PASI-C 92483829011 MW-22 EPA 6010D SH1 14 PASI-A EPA 6020E BG2 1 PASI-A EPA 8260D SAS 51 PASI-C 92483829012 MW-23 EPA 6010D SH1 14 PASI-A EPA 6020E BG2 1 PASI-A EPA 8260D CL 51 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Analytes Lab ID Sample ID Method Analysts Reported Laboratory PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MWA Lab ID: 92483829001 Collected: 06/25/20 14:37 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 06/30/20 00:35 07/01/20 01:08 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 01:08 7440-38-2 Barium 30.6 ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 01:08 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 06/30/20 00:35 07/01/20 01:08 7440-41-7 Cadmium 2.6 ug/L 1.0 0.40 1 06/30/20 00:35 07/01/20 01:08 7440-43-9 Chromium ND ug/L 5.0 3.7 1 06/30/20 00:35 07/01/20 01:08 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 06/30/20 00:35 07/01/20 01:08 7440-48-4 Copper ND ug/L 5.0 4.3 1 06/30/20 00:35 07/01/20 01:08 7440-50-8 Lead ND ug/L 5.0 4.5 1 06/30/20 00:35 07/01/20 01:08 7439-92-1 Nickel ND ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 01:08 7440-02-0 Selenium ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 01:08 7782-49-2 Silver ND ug/L 5.0 2.5 1 06/30/20 00:35 07/01/20 01:08 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 06/30/20 00:35 07/01/20 01:08 7440-62-2 Zinc ND ug/L 10.0 9.5 1 06/30/20 00:35 07/01/20 01:08 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium ND ug/L 0.10 0.050 1 06/30/20 00:13 06/30/20 14:46 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 07/02/20 05:23 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 07/02/20 05:23 107-13-1 Benzene ND ug/L 1.0 0.15 1 07/02/20 05:23 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 07/02/20 05:23 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 07/02/20 05:23 75-27-4 Bromoform ND ug/L 1.0 0.62 1 07/02/20 05:23 75-25-2 Bromomethane ND ug/L 2.0 0.62 1 07/02/20 05:23 74-83-9 IK 2-Butanone (MEK) ND ug/L 5.0 3.3 1 07/02/20 05:23 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 07/02/20 05:23 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 07/02/20 05:23 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 07/02/20 05:23 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 07/02/20 05:23 75-00-3 Chloroform ND ug/L 5.0 2.3 1 07/02/20 05:23 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 07/02/20 05:23 74-87-3 v2 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 07/02/20 05:23 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 07/02/20 05:23 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 07/02/20 05:23 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 07/02/20 05:23 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.29 1 07/02/20 05:23 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 07/02/20 05:23 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 07/02/20 05:23 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.27 1 07/02/20 05:23 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.34 1 07/02/20 05:23 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 07/02/20 05:23 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-1 Lab ID: 92483829001 Collected: 06/25/20 14:37 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene 1,4-Dioxane (p-Dioxane) Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 07/02/2020 04:47 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.29 1 07/02/20 05:23 156-59-2 ND ug/L 1.0 0.25 1 07/02/20 05:23 156-60-5 ND ug/L 1.0 0.19 1 07/02/20 05:23 78-87-5 ND ug/L 1.0 0.30 1 07/02/20 05:23 10061-01-5 ND ug/L 1.0 0.31 1 07/02/20 05:23 10061-02-6 ND ug/L 150 56.2 1 07/02/20 05:23 123-91-1 ND ug/L 1.0 0.26 1 07/02/20 05:23 100-41-4 ND ug/L 5.0 0.57 1 07/02/20 05:23 591-78-6 ND ug/L 20.0 12.5 1 07/02/20 05:23 74-88-4 ND ug/L 5.0 3.7 1 07/02/20 05:23 75-09-2 ND ug/L 5.0 4.5 1 07/02/20 05:23 108-10-1 ND ug/L 1.0 0.27 1 07/02/20 05:23 100-42-5 ND ug/L 1.0 0.34 1 07/02/20 05:23 630-20-6 ND ug/L 1.0 0.22 1 07/02/20 05:23 79-34-5 ND ug/L 1.0 0.16 1 07/02/20 05:23 127-18-4 ND ug/L 1.0 0.24 1 07/02/20 05:23 108-88-3 ND ug/L 1.0 0.18 1 07/02/20 05:23 71-55-6 ND ug/L 1.0 0.24 1 07/02/20 05:23 79-00-5 ND ug/L 1.0 0.22 1 07/02/20 05:23 79-01-6 ND ug/L 1.0 0.31 1 07/02/20 05:23 75-69-4 ND ug/L 1.0 0.35 1 07/02/20 05:23 96-18-4 ND ug/L 2.0 1.4 1 07/02/20 05:23 108-05-4 ND ug/L 1.0 0.24 1 07/02/20 05:23 75-01-4 ND ug/L 1.0 0.63 1 07/02/20 05:23 1330-20-7 95 % 70-130 1 07/02/20 05:23 460-00-4 90 % 70-130 1 07/02/20 05:23 17060-07-0 99 % 70-130 1 07/02/20 05:23 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-11 Lab ID: 92483829002 Collected: 06/25/20 15:03 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 06/30/20 00:35 07/01/20 01:12 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 01:12 7440-38-2 Barium 35.8 ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 01:12 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 06/30/20 00:35 07/01/20 01:12 7440-41-7 Cadmium 2.0 ug/L 1.0 0.40 1 06/30/20 00:35 07/01/20 01:12 7440-43-9 Chromium ND ug/L 5.0 3.7 1 06/30/20 00:35 07/01/20 01:12 7440-47-3 Cobalt 15.8 ug/L 5.0 3.6 1 06/30/20 00:35 07/01/20 01:12 7440-48-4 Copper ND ug/L 5.0 4.3 1 06/30/20 00:35 07/01/20 01:12 7440-50-8 Lead ND ug/L 5.0 4.5 1 06/30/20 00:35 07/01/20 01:12 7439-92-1 Nickel ND ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 01:12 7440-02-0 Selenium ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 01:12 7782-49-2 Silver ND ug/L 5.0 2.5 1 06/30/20 00:35 07/01/20 01:12 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 06/30/20 00:35 07/01/20 01:12 7440-62-2 Zinc 9.7.1 ug/L 10.0 9.5 1 06/30/20 00:35 07/01/20 01:12 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium 0.0991 ug/L 0.10 0.050 1 06/30/20 00:13 06/30/20 14:50 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 07/02/20 04:01 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 07/02/20 04:01 107-13-1 Benzene ND ug/L 1.0 0.15 1 07/02/20 04:01 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 07/02/20 04:01 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 07/02/20 04:01 75-27-4 Bromoform ND ug/L 1.0 0.62 1 07/02/20 04:01 75-25-2 v1 Bromomethane ND ug/L 2.0 0.62 1 07/02/20 04:01 74-83-9 v2 2-Butanone (MEK) ND ug/L 5.0 3.3 1 07/02/20 04:01 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 07/02/20 04:01 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 07/02/20 04:01 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 07/02/20 04:01 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 07/02/20 04:01 75-00-3 Chloroform ND ug/L 5.0 2.3 1 07/02/20 04:01 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 07/02/20 04:01 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 07/02/20 04:01 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 07/02/20 04:01 124-48-1 v2 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 07/02/20 04:01 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 07/02/20 04:01 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.29 1 07/02/20 04:01 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 07/02/20 04:01 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 07/02/20 04:01 110-57-6 v2 1,1-Dichloroethane ND ug/L 1.0 0.27 1 07/02/20 04:01 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.34 1 07/02/20 04:01 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 07/02/20 04:01 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-11 Lab ID: 92483829002 Collected: 06/25/20 15:03 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene 1,4-Dioxane (p-Dioxane) Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 07/02/2020 04:47 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.29 1 07/02/20 04:01 156-59-2 ND ug/L 1.0 0.25 1 07/02/20 04:01 156-60-5 0.34J ug/L 1.0 0.19 1 07/02/20 04:01 78-87-5 N D ug/L 1.0 0.30 1 07/02/20 04:01 10061-01-5 ND ug/L 1.0 0.31 1 07/02/20 04:01 10061-02-6 ND ug/L 150 56.2 1 07/02/20 04:01 123-91-1 ND ug/L 1.0 0.26 1 07/02/20 04:01 100-41-4 ND ug/L 5.0 0.57 1 07/02/20 04:01 591-78-6 ND ug/L 20.0 12.5 1 07/02/20 04:01 74-88-4 ND ug/L 5.0 3.7 1 07/02/20 04:01 75-09-2 ND ug/L 5.0 4.5 1 07/02/20 04:01 108-10-1 ND ug/L 1.0 0.27 1 07/02/20 04:01 100-42-5 ND ug/L 1.0 0.34 1 07/02/20 04:01 630-20-6 ND ug/L 1.0 0.22 1 07/02/20 04:01 79-34-5 ND ug/L 1.0 0.16 1 07/02/20 04:01 127-18-4 ND ug/L 1.0 0.24 1 07/02/20 04:01 108-88-3 ND ug/L 1.0 0.18 1 07/02/20 04:01 71-55-6 ND ug/L 1.0 0.24 1 07/02/20 04:01 79-00-5 ND ug/L 1.0 0.22 1 07/02/20 04:01 79-01-6 ND ug/L 1.0 0.31 1 07/02/20 04:01 75-69-4 ND ug/L 1.0 0.35 1 07/02/20 04:01 96-18-4 ND ug/L 2.0 1.4 1 07/02/20 04:01 108-05-4 ND ug/L 1.0 0.24 1 07/02/20 04:01 75-01-4 ND ug/L 1.0 0.63 1 07/02/20 04:01 1330-20-7 99 % 70-130 1 07/02/20 04:01 460-00-4 91 % 70-130 1 07/02/20 04:01 17060-07-0 100 % 70-130 1 07/02/20 04:01 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v1 IK Page 9 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-12S Lab ID: 92483829003 Collected: 06/25/20 14:16 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 06/30/20 00:35 07/01/20 01:15 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 01:15 7440-38-2 Barium 10.5 ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 01:15 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 06/30/20 00:35 07/01/20 01:15 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 06/30/20 00:35 07/01/20 01:15 7440-43-9 Chromium ND ug/L 5.0 3.7 1 06/30/20 00:35 07/01/20 01:15 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 06/30/20 00:35 07/01/20 01:15 7440-48-4 Copper ND ug/L 5.0 4.3 1 06/30/20 00:35 07/01/20 01:15 7440-50-8 Lead ND ug/L 5.0 4.5 1 06/30/20 00:35 07/01/20 01:15 7439-92-1 Nickel ND ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 01:15 7440-02-0 Selenium ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 01:15 7782-49-2 Silver ND ug/L 5.0 2.5 1 06/30/20 00:35 07/01/20 01:15 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 06/30/20 00:35 07/01/20 01:15 7440-62-2 Zinc ND ug/L 10.0 9.5 1 06/30/20 00:35 07/01/20 01:15 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium ND ug/L 0.10 0.050 1 06/30/20 00:13 06/30/20 14:53 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 07/02/20 07:13 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 07/02/20 07:13 107-13-1 Benzene ND ug/L 1.0 0.15 1 07/02/20 07:13 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 07/02/20 07:13 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 07/02/20 07:13 75-27-4 Bromoform ND ug/L 1.0 0.62 1 07/02/20 07:13 75-25-2 Bromomethane ND ug/L 2.0 0.62 1 07/02/20 07:13 74-83-9 2-Butanone (MEK) ND ug/L 5.0 3.3 1 07/02/20 07:13 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 07/02/20 07:13 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 07/02/20 07:13 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 07/02/20 07:13 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 07/02/20 07:13 75-00-3 Chloroform ND ug/L 5.0 2.3 1 07/02/20 07:13 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 07/02/20 07:13 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 07/02/20 07:13 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 07/02/20 07:13 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 07/02/20 07:13 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 07/02/20 07:13 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.29 1 07/02/20 07:13 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 07/02/20 07:13 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 07/02/20 07:13 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.27 1 07/02/20 07:13 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.34 1 07/02/20 07:13 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 07/02/20 07:13 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. IK v2 Page 10 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-12S Lab ID: 92483829003 Collected: 06/25/20 14:16 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene 1,4-Dioxane (p-Dioxane) Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 07/02/2020 04:47 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.29 1 07/02/20 07:13 156-59-2 ND ug/L 1.0 0.25 1 07/02/20 07:13 156-60-5 ND ug/L 1.0 0.19 1 07/02/20 07:13 78-87-5 ND ug/L 1.0 0.30 1 07/02/20 07:13 10061-01-5 ND ug/L 1.0 0.31 1 07/02/20 07:13 10061-02-6 ND ug/L 150 56.2 1 07/02/20 07:13 123-91-1 ND ug/L 1.0 0.26 1 07/02/20 07:13 100-41-4 ND ug/L 5.0 0.57 1 07/02/20 07:13 591-78-6 ND ug/L 20.0 12.5 1 07/02/20 07:13 74-88-4 ND ug/L 5.0 3.7 1 07/02/20 07:13 75-09-2 ND ug/L 5.0 4.5 1 07/02/20 07:13 108-10-1 ND ug/L 1.0 0.27 1 07/02/20 07:13 100-42-5 ND ug/L 1.0 0.34 1 07/02/20 07:13 630-20-6 ND ug/L 1.0 0.22 1 07/02/20 07:13 79-34-5 ND ug/L 1.0 0.16 1 07/02/20 07:13 127-18-4 ND ug/L 1.0 0.24 1 07/02/20 07:13 108-88-3 ND ug/L 1.0 0.18 1 07/02/20 07:13 71-55-6 ND ug/L 1.0 0.24 1 07/02/20 07:13 79-00-5 ND ug/L 1.0 0.22 1 07/02/20 07:13 79-01-6 ND ug/L 1.0 0.31 1 07/02/20 07:13 75-69-4 ND ug/L 1.0 0.35 1 07/02/20 07:13 96-18-4 ND ug/L 2.0 1.4 1 07/02/20 07:13 108-05-4 ND ug/L 1.0 0.24 1 07/02/20 07:13 75-01-4 ND ug/L 1.0 0.63 1 07/02/20 07:13 1330-20-7 94 % 70-130 1 07/02/20 07:13 460-00-4 92 % 70-130 1 07/02/20 07:13 17060-07-0 99 % 70-130 1 07/02/20 07:13 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-13 Lab ID: 92483829004 Collected: 06/25/20 14:02 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 06/30/20 00:35 07/01/20 01:18 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 01:18 7440-38-2 Barium 66.4 ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 01:18 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 06/30/20 00:35 07/01/20 01:18 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 06/30/20 00:35 07/01/20 01:18 7440-43-9 Chromium ND ug/L 5.0 3.7 1 06/30/20 00:35 07/01/20 01:18 7440-47-3 Cobalt 10.4 ug/L 5.0 3.6 1 06/30/20 00:35 07/01/20 01:18 7440-48-4 Copper ND ug/L 5.0 4.3 1 06/30/20 00:35 07/01/20 01:18 7440-50-8 Lead ND ug/L 5.0 4.5 1 06/30/20 00:35 07/01/20 01:18 7439-92-1 Nickel ND ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 01:18 7440-02-0 Selenium ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 01:18 7782-49-2 Silver ND ug/L 5.0 2.5 1 06/30/20 00:35 07/01/20 01:18 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 06/30/20 00:35 07/01/20 01:18 7440-62-2 Zinc ND ug/L 10.0 9.5 1 06/30/20 00:35 07/01/20 01:18 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium 0.079J ug/L 0.10 0.050 1 06/30/20 00:13 06/30/20 14:57 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 07/02/20 03:06 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 07/02/20 03:06 107-13-1 Benzene ND ug/L 1.0 0.15 1 07/02/20 03:06 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 07/02/20 03:06 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 07/02/20 03:06 75-27-4 Bromoform ND ug/L 1.0 0.62 1 07/02/20 03:06 75-25-2 Bromomethane ND ug/L 2.0 0.62 1 07/02/20 03:06 74-83-9 2-Butanone (MEK) ND ug/L 5.0 3.3 1 07/02/20 03:06 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 07/02/20 03:06 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 07/02/20 03:06 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 07/02/20 03:06 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 07/02/20 03:06 75-00-3 Chloroform ND ug/L 5.0 2.3 1 07/02/20 03:06 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 07/02/20 03:06 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 07/02/20 03:06 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 07/02/20 03:06 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 07/02/20 03:06 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 07/02/20 03:06 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.29 1 07/02/20 03:06 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 07/02/20 03:06 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 07/02/20 03:06 110-57-6 1,1-Dichloroethane 1.1 ug/L 1.0 0.27 1 07/02/20 03:06 75-34-3 1,2-Dichloroethane 0.51J ug/L 1.0 0.34 1 07/02/20 03:06 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 07/02/20 03:06 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. IH,v2 v2 v2 IK Page 12 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-13 Lab ID: 92483829004 Collected: 06/25/20 14:02 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene 1,4-Dioxane (p-Dioxane) Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 07/02/2020 04:47 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 10.6 ug/L 1.0 0.29 1 07/02/20 03:06 156-59-2 ND ug/L 1.0 0.25 1 07/02/20 03:06 156-60-5 ND ug/L 1.0 0.19 1 07/02/20 03:06 78-87-5 ND ug/L 1.0 0.30 1 07/02/20 03:06 10061-01-5 ND ug/L 1.0 0.31 1 07/02/20 03:06 10061-02-6 ND ug/L 150 56.2 1 07/02/20 03:06 123-91-1 ND ug/L 1.0 0.26 1 07/02/20 03:06 100-41-4 ND ug/L 5.0 0.57 1 07/02/20 03:06 591-78-6 ND ug/L 20.0 12.5 1 07/02/20 03:06 74-88-4 ND ug/L 5.0 3.7 1 07/02/20 03:06 75-09-2 ND ug/L 5.0 4.5 1 07/02/20 03:06 108-10-1 ND ug/L 1.0 0.27 1 07/02/20 03:06 100-42-5 ND ug/L 1.0 0.34 1 07/02/20 03:06 630-20-6 ND ug/L 1.0 0.22 1 07/02/20 03:06 79-34-5 ND ug/L 1.0 0.16 1 07/02/20 03:06 127-18-4 ND ug/L 1.0 0.24 1 07/02/20 03:06 108-88-3 ND ug/L 1.0 0.18 1 07/02/20 03:06 71-55-6 ND ug/L 1.0 0.24 1 07/02/20 03:06 79-00-5 ND ug/L 1.0 0.22 1 07/02/20 03:06 79-01-6 ND ug/L 1.0 0.31 1 07/02/20 03:06 75-69-4 ND ug/L 1.0 0.35 1 07/02/20 03:06 96-18-4 ND ug/L 2.0 1.4 1 07/02/20 03:06 108-05-4 ND ug/L 1.0 0.24 1 07/02/20 03:06 75-01-4 ND ug/L 1.0 0.63 1 07/02/20 03:06 1330-20-7 96 % 70-130 1 07/02/20 03:06 460-00-4 106 % 70-130 1 07/02/20 03:06 17060-07-0 98 % 70-130 1 07/02/20 03:06 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v1 v2 Page 13 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-14 Lab ID: 92483829005 Collected: 06/25/20 14:00 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 06/30/20 00:35 07/01/20 01:21 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 01:21 7440-38-2 Barium 21.1 ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 01:21 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 06/30/20 00:35 07/01/20 01:21 7440-41-7 Cadmium 0.79J ug/L 1.0 0.40 1 06/30/20 00:35 07/01/20 01:21 7440-43-9 Chromium ND ug/L 5.0 3.7 1 06/30/20 00:35 07/01/20 01:21 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 06/30/20 00:35 07/01/20 01:21 7440-48-4 Copper ND ug/L 5.0 4.3 1 06/30/20 00:35 07/01/20 01:21 7440-50-8 Lead ND ug/L 5.0 4.5 1 06/30/20 00:35 07/01/20 01:21 7439-92-1 Nickel ND ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 01:21 7440-02-0 Selenium ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 01:21 7782-49-2 Silver ND ug/L 5.0 2.5 1 06/30/20 00:35 07/01/20 01:21 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 06/30/20 00:35 07/01/20 01:21 7440-62-2 Zinc ND ug/L 10.0 9.5 1 06/30/20 00:35 07/01/20 01:21 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium ND ug/L 0.10 0.050 1 06/30/20 00:13 06/30/20 15:01 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 07/02/20 04:19 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 07/02/20 04:19 107-13-1 Benzene ND ug/L 1.0 0.15 1 07/02/20 04:19 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 07/02/20 04:19 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 07/02/20 04:19 75-27-4 Bromoform ND ug/L 1.0 0.62 1 07/02/20 04:19 75-25-2 Bromomethane ND ug/L 2.0 0.62 1 07/02/20 04:19 74-83-9 2-Butanone (MEK) ND ug/L 5.0 3.3 1 07/02/20 04:19 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 07/02/20 04:19 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 07/02/20 04:19 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 07/02/20 04:19 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 07/02/20 04:19 75-00-3 Chloroform ND ug/L 5.0 2.3 1 07/02/20 04:19 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 07/02/20 04:19 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 07/02/20 04:19 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 07/02/20 04:19 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 07/02/20 04:19 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 07/02/20 04:19 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.29 1 07/02/20 04:19 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 07/02/20 04:19 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 07/02/20 04:19 110-57-6 1,1-Dichloroethane 1.1 ug/L 1.0 0.27 1 07/02/20 04:19 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.34 1 07/02/20 04:19 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 07/02/20 04:19 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. v1 v2 v2 v2 Page 14 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-14 Lab ID: 92483829005 Collected: 06/25/20 14:00 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene 1,4-Dioxane (p-Dioxane) Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 07/02/2020 04:47 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 3.3 ug/L 1.0 0.29 1 07/02/20 04:19 156-59-2 ND ug/L 1.0 0.25 1 07/02/20 04:19 156-60-5 ND ug/L 1.0 0.19 1 07/02/20 04:19 78-87-5 ND ug/L 1.0 0.30 1 07/02/20 04:19 10061-01-5 ND ug/L 1.0 0.31 1 07/02/20 04:19 10061-02-6 ND ug/L 150 56.2 1 07/02/20 04:19 123-91-1 ND ug/L 1.0 0.26 1 07/02/20 04:19 100-41-4 ND ug/L 5.0 0.57 1 07/02/20 04:19 591-78-6 ND ug/L 20.0 12.5 1 07/02/20 04:19 74-88-4 ND ug/L 5.0 3.7 1 07/02/20 04:19 75-09-2 ND ug/L 5.0 4.5 1 07/02/20 04:19 108-10-1 ND ug/L 1.0 0.27 1 07/02/20 04:19 100-42-5 ND ug/L 1.0 0.34 1 07/02/20 04:19 630-20-6 ND ug/L 1.0 0.22 1 07/02/20 04:19 79-34-5 ND ug/L 1.0 0.16 1 07/02/20 04:19 127-18-4 ND ug/L 1.0 0.24 1 07/02/20 04:19 108-88-3 ND ug/L 1.0 0.18 1 07/02/20 04:19 71-55-6 ND ug/L 1.0 0.24 1 07/02/20 04:19 79-00-5 ND ug/L 1.0 0.22 1 07/02/20 04:19 79-01-6 ND ug/L 1.0 0.31 1 07/02/20 04:19 75-69-4 ND ug/L 1.0 0.35 1 07/02/20 04:19 96-18-4 ND ug/L 2.0 1.4 1 07/02/20 04:19 108-05-4 ND ug/L 1.0 0.24 1 07/02/20 04:19 75-01-4 ND ug/L 1.0 0.63 1 07/02/20 04:19 1330-20-7 99 % 70-130 1 07/02/20 04:19 460-00-4 91 % 70-130 1 07/02/20 04:19 17060-07-0 100 % 70-130 1 07/02/20 04:19 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v1 IK Page 15 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-15 Lab ID: 92483829006 Collected: 06/25/20 12:00 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 06/30/20 00:35 07/01/20 01:24 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 01:24 7440-38-2 Barium 45.5 ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 01:24 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 06/30/20 00:35 07/01/20 01:24 7440-41-7 Cadmium 0.42J ug/L 1.0 0.40 1 06/30/20 00:35 07/01/20 01:24 7440-43-9 Chromium ND ug/L 5.0 3.7 1 06/30/20 00:35 07/01/20 01:24 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 06/30/20 00:35 07/01/20 01:24 7440-48-4 Copper ND ug/L 5.0 4.3 1 06/30/20 00:35 07/01/20 01:24 7440-50-8 Lead ND ug/L 5.0 4.5 1 06/30/20 00:35 07/01/20 01:24 7439-92-1 Nickel ND ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 01:24 7440-02-0 Selenium ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 01:24 7782-49-2 Silver ND ug/L 5.0 2.5 1 06/30/20 00:35 07/01/20 01:24 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 06/30/20 00:35 07/01/20 01:24 7440-62-2 Zinc ND ug/L 10.0 9.5 1 06/30/20 00:35 07/01/20 01:24 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium 0.0901 ug/L 0.10 0.050 1 06/30/20 00:13 06/30/20 15:31 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 07/02/20 04:00 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 07/02/20 04:00 107-13-1 Benzene 0.34J ug/L 1.0 0.15 1 07/02/20 04:00 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 07/02/20 04:00 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 07/02/20 04:00 75-27-4 Bromoform ND ug/L 1.0 0.62 1 07/02/20 04:00 75-25-2 Bromomethane ND ug/L 2.0 0.62 1 07/02/20 04:00 74-83-9 2-Butanone (MEK) ND ug/L 5.0 3.3 1 07/02/20 04:00 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 07/02/20 04:00 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 07/02/20 04:00 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 07/02/20 04:00 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 07/02/20 04:00 75-00-3 Chloroform ND ug/L 5.0 2.3 1 07/02/20 04:00 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 07/02/20 04:00 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 07/02/20 04:00 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 07/02/20 04:00 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 07/02/20 04:00 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 07/02/20 04:00 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.29 1 07/02/20 04:00 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 07/02/20 04:00 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 07/02/20 04:00 110-57-6 1,1-Dichloroethane 4.6 ug/L 1.0 0.27 1 07/02/20 04:00 75-34-3 1,2-Dichloroethane 0.56J ug/L 1.0 0.34 1 07/02/20 04:00 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 07/02/20 04:00 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. IH,v2 v2 v2 IK Page 16 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-15 Lab ID: 92483829006 Collected: 06/25/20 12:00 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene 1,4-Dioxane (p-Dioxane) Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 07/02/2020 04:47 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 21.4 ug/L 1.0 0.29 1 07/02/20 04:00 156-59-2 ND ug/L 1.0 0.25 1 07/02/20 04:00 156-60-5 ND ug/L 1.0 0.19 1 07/02/20 04:00 78-87-5 ND ug/L 1.0 0.30 1 07/02/20 04:00 10061-01-5 ND ug/L 1.0 0.31 1 07/02/20 04:00 10061-02-6 ND ug/L 150 56.2 1 07/02/20 04:00 123-91-1 ND ug/L 1.0 0.26 1 07/02/20 04:00 100-41-4 ND ug/L 5.0 0.57 1 07/02/20 04:00 591-78-6 ND ug/L 20.0 12.5 1 07/02/20 04:00 74-88-4 ND ug/L 5.0 3.7 1 07/02/20 04:00 75-09-2 ND ug/L 5.0 4.5 1 07/02/20 04:00 108-10-1 ND ug/L 1.0 0.27 1 07/02/20 04:00 100-42-5 ND ug/L 1.0 0.34 1 07/02/20 04:00 630-20-6 ND ug/L 1.0 0.22 1 07/02/20 04:00 79-34-5 ND ug/L 1.0 0.16 1 07/02/20 04:00 127-18-4 ND ug/L 1.0 0.24 1 07/02/20 04:00 108-88-3 ND ug/L 1.0 0.18 1 07/02/20 04:00 71-55-6 ND ug/L 1.0 0.24 1 07/02/20 04:00 79-00-5 2.2 ug/L 1.0 0.22 1 07/02/20 04:00 79-01-6 ND ug/L 1.0 0.31 1 07/02/20 04:00 75-69-4 ND ug/L 1.0 0.35 1 07/02/20 04:00 96-18-4 ND ug/L 2.0 1.4 1 07/02/20 04:00 108-05-4 1.6 ug/L 1.0 0.24 1 07/02/20 04:00 75-01-4 ND ug/L 1.0 0.63 1 07/02/20 04:00 1330-20-7 99 % 70-130 1 07/02/20 04:00 460-00-4 108 % 70-130 1 07/02/20 04:00 17060-07-0 99 % 70-130 1 07/02/20 04:00 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v1 v2 Page 17 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-16 Lab ID: 92483829007 Collected: 06/25/20 11:43 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 06/30/20 00:35 07/01/20 01:40 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 01:40 7440-38-2 Barium 68.2 ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 01:40 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 06/30/20 00:35 07/01/20 01:40 7440-41-7 Cadmium 1.8 ug/L 1.0 0.40 1 06/30/20 00:35 07/01/20 01:40 7440-43-9 Chromium ND ug/L 5.0 3.7 1 06/30/20 00:35 07/01/20 01:40 7440-47-3 Cobalt 289 ug/L 5.0 3.6 1 06/30/20 00:35 07/01/20 01:40 7440-48-4 Copper ND ug/L 5.0 4.3 1 06/30/20 00:35 07/01/20 01:40 7440-50-8 Lead ND ug/L 5.0 4.5 1 06/30/20 00:35 07/01/20 01:40 7439-92-1 Nickel 12.4 ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 01:40 7440-02-0 Selenium ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 01:40 7782-49-2 Silver ND ug/L 5.0 2.5 1 06/30/20 00:35 07/01/20 01:40 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 06/30/20 00:35 07/01/20 01:40 7440-62-2 Zinc ND ug/L 10.0 9.5 1 06/30/20 00:35 07/01/20 01:40 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium 0.31 ug/L 0.10 0.050 1 06/30/20 00:13 06/30/20 15:58 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 07/02/20 03:42 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 07/02/20 03:42 107-13-1 Benzene 0.76J ug/L 1.0 0.15 1 07/02/20 03:42 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 07/02/20 03:42 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 07/02/20 03:42 75-27-4 Bromoform ND ug/L 1.0 0.62 1 07/02/20 03:42 75-25-2 Bromomethane ND ug/L 2.0 0.62 1 07/02/20 03:42 74-83-9 2-Butanone (MEK) ND ug/L 5.0 3.3 1 07/02/20 03:42 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 07/02/20 03:42 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 07/02/20 03:42 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 07/02/20 03:42 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 07/02/20 03:42 75-00-3 Chloroform ND ug/L 5.0 2.3 1 07/02/20 03:42 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 07/02/20 03:42 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 07/02/20 03:42 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 07/02/20 03:42 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 07/02/20 03:42 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 07/02/20 03:42 74-95-3 1,2-Dichlorobenzene 0.34J ug/L 1.0 0.29 1 07/02/20 03:42 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 07/02/20 03:42 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 07/02/20 03:42 110-57-6 1,1-Dichloroethane 0.44J ug/L 1.0 0.27 1 07/02/20 03:42 75-34-3 1,2-Dichloroethane 1.2 ug/L 1.0 0.34 1 07/02/20 03:42 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 07/02/20 03:42 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. IH,v2 v2 v2 IK Page 18 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-16 Lab ID: 92483829007 Collected: 06/25/20 11:43 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene 1,4-Dioxane (p-Dioxane) Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 07/02/2020 04:47 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 10.2 ug/L 1.0 0.29 1 07/02/20 03:42 156-59-2 ND ug/L 1.0 0.25 1 07/02/20 03:42 156-60-5 0.49J ug/L 1.0 0.19 1 07/02/20 03:42 78-87-5 ND ug/L 1.0 0.30 1 07/02/20 03:42 10061-01-5 ND ug/L 1.0 0.31 1 07/02/20 03:42 10061-02-6 ND ug/L 150 56.2 1 07/02/20 03:42 123-91-1 ND ug/L 1.0 0.26 1 07/02/20 03:42 100-41-4 ND ug/L 5.0 0.57 1 07/02/20 03:42 591-78-6 ND ug/L 20.0 12.5 1 07/02/20 03:42 74-88-4 ND ug/L 5.0 3.7 1 07/02/20 03:42 75-09-2 ND ug/L 5.0 4.5 1 07/02/20 03:42 108-10-1 ND ug/L 1.0 0.27 1 07/02/20 03:42 100-42-5 ND ug/L 1.0 0.34 1 07/02/20 03:42 630-20-6 ND ug/L 1.0 0.22 1 07/02/20 03:42 79-34-5 ND ug/L 1.0 0.16 1 07/02/20 03:42 127-18-4 ND ug/L 1.0 0.24 1 07/02/20 03:42 108-88-3 ND ug/L 1.0 0.18 1 07/02/20 03:42 71-55-6 ND ug/L 1.0 0.24 1 07/02/20 03:42 79-00-5 ND ug/L 1.0 0.22 1 07/02/20 03:42 79-01-6 ND ug/L 1.0 0.31 1 07/02/20 03:42 75-69-4 ND ug/L 1.0 0.35 1 07/02/20 03:42 96-18-4 ND ug/L 2.0 1.4 1 07/02/20 03:42 108-05-4 1.2 ug/L 1.0 0.24 1 07/02/20 03:42 75-01-4 ND ug/L 1.0 0.63 1 07/02/20 03:42 1330-20-7 98 % 70-130 1 07/02/20 03:42 460-00-4 108 % 70-130 1 07/02/20 03:42 17060-07-0 96 % 70-130 1 07/02/20 03:42 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v1 v2 Page 19 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-17 Lab ID: 92483829008 Collected: 06/25/20 11:03 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 06/30/20 00:35 07/01/20 03:27 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 03:27 7440-38-2 Barium 18.9 ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 03:27 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 06/30/20 00:35 07/01/20 03:27 7440-41-7 Cadmium 0.43J ug/L 1.0 0.40 1 06/30/20 00:35 07/01/20 03:27 7440-43-9 Chromium ND ug/L 5.0 3.7 1 06/30/20 00:35 07/01/20 03:27 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 06/30/20 00:35 07/01/20 03:27 7440-48-4 Copper ND ug/L 5.0 4.3 1 06/30/20 00:35 07/01/20 03:27 7440-50-8 Lead ND ug/L 5.0 4.5 1 06/30/20 00:35 07/01/20 03:27 7439-92-1 Nickel ND ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 03:27 7440-02-0 Selenium ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 03:27 7782-49-2 Silver ND ug/L 5.0 2.5 1 06/30/20 00:35 07/01/20 03:27 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 06/30/20 00:35 07/01/20 03:27 7440-62-2 Zinc ND ug/L 10.0 9.5 1 06/30/20 00:35 07/01/20 03:27 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium ND ug/L 0.10 0.050 1 06/30/20 00:13 06/30/20 16:02 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 07/02/20 04:36 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 07/02/20 04:36 107-13-1 Benzene ND ug/L 1.0 0.15 1 07/02/20 04:36 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 07/02/20 04:36 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 07/02/20 04:36 75-27-4 Bromoform ND ug/L 1.0 0.62 1 07/02/20 04:36 75-25-2 Bromomethane ND ug/L 2.0 0.62 1 07/02/20 04:36 74-83-9 2-Butanone (MEK) ND ug/L 5.0 3.3 1 07/02/20 04:36 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 07/02/20 04:36 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 07/02/20 04:36 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 07/02/20 04:36 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 07/02/20 04:36 75-00-3 Chloroform ND ug/L 5.0 2.3 1 07/02/20 04:36 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 07/02/20 04:36 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 07/02/20 04:36 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 07/02/20 04:36 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 07/02/20 04:36 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 07/02/20 04:36 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.29 1 07/02/20 04:36 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 07/02/20 04:36 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 07/02/20 04:36 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.27 1 07/02/20 04:36 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.34 1 07/02/20 04:36 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 07/02/20 04:36 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. v1 v2 v2 v2 Page 20 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-17 Lab ID: 92483829008 Collected: 06/25/20 11:03 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene 1,4-Dioxane (p-Dioxane) Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 07/02/2020 04:47 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.29 1 07/02/20 04:36 156-59-2 ND ug/L 1.0 0.25 1 07/02/20 04:36 156-60-5 ND ug/L 1.0 0.19 1 07/02/20 04:36 78-87-5 ND ug/L 1.0 0.30 1 07/02/20 04:36 10061-01-5 ND ug/L 1.0 0.31 1 07/02/20 04:36 10061-02-6 ND ug/L 150 56.2 1 07/02/20 04:36 123-91-1 ND ug/L 1.0 0.26 1 07/02/20 04:36 100-41-4 ND ug/L 5.0 0.57 1 07/02/20 04:36 591-78-6 ND ug/L 20.0 12.5 1 07/02/20 04:36 74-88-4 ND ug/L 5.0 3.7 1 07/02/20 04:36 75-09-2 ND ug/L 5.0 4.5 1 07/02/20 04:36 108-10-1 ND ug/L 1.0 0.27 1 07/02/20 04:36 100-42-5 ND ug/L 1.0 0.34 1 07/02/20 04:36 630-20-6 ND ug/L 1.0 0.22 1 07/02/20 04:36 79-34-5 ND ug/L 1.0 0.16 1 07/02/20 04:36 127-18-4 ND ug/L 1.0 0.24 1 07/02/20 04:36 108-88-3 ND ug/L 1.0 0.18 1 07/02/20 04:36 71-55-6 ND ug/L 1.0 0.24 1 07/02/20 04:36 79-00-5 ND ug/L 1.0 0.22 1 07/02/20 04:36 79-01-6 ND ug/L 1.0 0.31 1 07/02/20 04:36 75-69-4 ND ug/L 1.0 0.35 1 07/02/20 04:36 96-18-4 ND ug/L 2.0 1.4 1 07/02/20 04:36 108-05-4 ND ug/L 1.0 0.24 1 07/02/20 04:36 75-01-4 ND ug/L 1.0 0.63 1 07/02/20 04:36 1330-20-7 99 % 70-130 1 07/02/20 04:36 460-00-4 91 % 70-130 1 07/02/20 04:36 17060-07-0 101 % 70-130 1 07/02/20 04:36 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v1 IK Page 21 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-19 Lab ID: 92483829009 Collected: 06/25/20 11:14 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 06/30/20 00:35 07/01/20 03:53 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 03:53 7440-38-2 Barium 25.4 ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 03:53 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 06/30/20 00:35 07/01/20 03:53 7440-41-7 Cadmium 0.60J ug/L 1.0 0.40 1 06/30/20 00:35 07/01/20 03:53 7440-43-9 Chromium ND ug/L 5.0 3.7 1 06/30/20 00:35 07/01/20 03:53 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 06/30/20 00:35 07/01/20 03:53 7440-48-4 Copper ND ug/L 5.0 4.3 1 06/30/20 00:35 07/01/20 03:53 7440-50-8 Lead ND ug/L 5.0 4.5 1 06/30/20 00:35 07/01/20 03:53 7439-92-1 Nickel ND ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 03:53 7440-02-0 Selenium ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 03:53 7782-49-2 Silver ND ug/L 5.0 2.5 1 06/30/20 00:35 07/01/20 03:53 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 06/30/20 00:35 07/01/20 03:53 7440-62-2 Zinc ND ug/L 10.0 9.5 1 06/30/20 00:35 07/01/20 03:53 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium ND ug/L 0.10 0.050 1 06/30/20 00:13 06/30/20 16:05 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 07/02/20 08:07 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 07/02/20 08:07 107-13-1 Benzene ND ug/L 1.0 0.15 1 07/02/20 08:07 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 07/02/20 08:07 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 07/02/20 08:07 75-27-4 Bromoform ND ug/L 1.0 0.62 1 07/02/20 08:07 75-25-2 Bromomethane ND ug/L 2.0 0.62 1 07/02/20 08:07 74-83-9 2-Butanone (MEK) ND ug/L 5.0 3.3 1 07/02/20 08:07 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 07/02/20 08:07 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 07/02/20 08:07 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 07/02/20 08:07 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 07/02/20 08:07 75-00-3 Chloroform ND ug/L 5.0 2.3 1 07/02/20 08:07 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 07/02/20 08:07 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 07/02/20 08:07 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 07/02/20 08:07 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 07/02/20 08:07 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 07/02/20 08:07 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.29 1 07/02/20 08:07 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 07/02/20 08:07 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 07/02/20 08:07 110-57-6 1,1-Dichloroethane 0.69J ug/L 1.0 0.27 1 07/02/20 08:07 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.34 1 07/02/20 08:07 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 07/02/20 08:07 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. IK v2 Page 22 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-19 Lab ID: 92483829009 Collected: 06/25/20 11:14 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene 1,4-Dioxane (p-Dioxane) Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 07/02/2020 04:47 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1.4 ug/L 1.0 0.29 1 07/02/20 08:07 156-59-2 ND ug/L 1.0 0.25 1 07/02/20 08:07 156-60-5 ND ug/L 1.0 0.19 1 07/02/20 08:07 78-87-5 ND ug/L 1.0 0.30 1 07/02/20 08:07 10061-01-5 ND ug/L 1.0 0.31 1 07/02/20 08:07 10061-02-6 ND ug/L 150 56.2 1 07/02/20 08:07 123-91-1 ND ug/L 1.0 0.26 1 07/02/20 08:07 100-41-4 ND ug/L 5.0 0.57 1 07/02/20 08:07 591-78-6 ND ug/L 20.0 12.5 1 07/02/20 08:07 74-88-4 ND ug/L 5.0 3.7 1 07/02/20 08:07 75-09-2 ND ug/L 5.0 4.5 1 07/02/20 08:07 108-10-1 ND ug/L 1.0 0.27 1 07/02/20 08:07 100-42-5 ND ug/L 1.0 0.34 1 07/02/20 08:07 630-20-6 ND ug/L 1.0 0.22 1 07/02/20 08:07 79-34-5 ND ug/L 1.0 0.16 1 07/02/20 08:07 127-18-4 ND ug/L 1.0 0.24 1 07/02/20 08:07 108-88-3 ND ug/L 1.0 0.18 1 07/02/20 08:07 71-55-6 ND ug/L 1.0 0.24 1 07/02/20 08:07 79-00-5 ND ug/L 1.0 0.22 1 07/02/20 08:07 79-01-6 ND ug/L 1.0 0.31 1 07/02/20 08:07 75-69-4 ND ug/L 1.0 0.35 1 07/02/20 08:07 96-18-4 ND ug/L 2.0 1.4 1 07/02/20 08:07 108-05-4 ND ug/L 1.0 0.24 1 07/02/20 08:07 75-01-4 ND ug/L 1.0 0.63 1 07/02/20 08:07 1330-20-7 94 % 70-130 1 07/02/20 08:07 460-00-4 91 % 70-130 1 07/02/20 08:07 17060-07-0 99 % 70-130 1 07/02/20 08:07 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 23 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-21 Lab ID: 92483829010 Collected: 06/25/20 14:08 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 06/30/20 00:35 07/01/20 03:56 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 03:56 7440-38-2 Barium 55.7 ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 03:56 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 06/30/20 00:35 07/01/20 03:56 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 06/30/20 00:35 07/01/20 03:56 7440-43-9 Chromium ND ug/L 5.0 3.7 1 06/30/20 00:35 07/01/20 03:56 7440-47-3 Cobalt 3.8.1 ug/L 5.0 3.6 1 06/30/20 00:35 07/01/20 03:56 7440-48-4 Copper ND ug/L 5.0 4.3 1 06/30/20 00:35 07/01/20 03:56 7440-50-8 Lead ND ug/L 5.0 4.5 1 06/30/20 00:35 07/01/20 03:56 7439-92-1 Nickel ND ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 03:56 7440-02-0 Selenium ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 03:56 7782-49-2 Silver ND ug/L 5.0 2.5 1 06/30/20 00:35 07/01/20 03:56 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 06/30/20 00:35 07/01/20 03:56 7440-62-2 Zinc ND ug/L 10.0 9.5 1 06/30/20 00:35 07/01/20 03:56 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium ND ug/L 0.10 0.050 1 06/30/20 00:13 06/30/20 16:09 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 07/02/20 02:48 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 07/02/20 02:48 107-13-1 Benzene ND ug/L 1.0 0.15 1 07/02/20 02:48 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 07/02/20 02:48 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 07/02/20 02:48 75-27-4 Bromoform ND ug/L 1.0 0.62 1 07/02/20 02:48 75-25-2 Bromomethane 0.64J ug/L 2.0 0.62 1 07/02/20 02:48 74-83-9 2-Butanone (MEK) ND ug/L 5.0 3.3 1 07/02/20 02:48 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 07/02/20 02:48 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 07/02/20 02:48 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 07/02/20 02:48 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 07/02/20 02:48 75-00-3 Chloroform ND ug/L 5.0 2.3 1 07/02/20 02:48 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 07/02/20 02:48 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 07/02/20 02:48 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 07/02/20 02:48 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 07/02/20 02:48 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 07/02/20 02:48 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.29 1 07/02/20 02:48 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 07/02/20 02:48 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 07/02/20 02:48 110-57-6 1,1-Dichloroethane 1.6 ug/L 1.0 0.27 1 07/02/20 02:48 75-34-3 1,2-Dichloroethane 0.591 ug/L 1.0 0.34 1 07/02/20 02:48 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 07/02/20 02:48 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. B,IH,v2 v2 v2 IK Page 24 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-21 Lab ID: 92483829010 Collected: 06/25/20 14:08 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene 1,4-Dioxane (p-Dioxane) Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 07/02/2020 04:47 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 11.1 ug/L 1.0 0.29 1 07/02/20 02:48 156-59-2 ND ug/L 1.0 0.25 1 07/02/20 02:48 156-60-5 ND ug/L 1.0 0.19 1 07/02/20 02:48 78-87-5 ND ug/L 1.0 0.30 1 07/02/20 02:48 10061-01-5 ND ug/L 1.0 0.31 1 07/02/20 02:48 10061-02-6 ND ug/L 150 56.2 1 07/02/20 02:48 123-91-1 ND ug/L 1.0 0.26 1 07/02/20 02:48 100-41-4 ND ug/L 5.0 0.57 1 07/02/20 02:48 591-78-6 ND ug/L 20.0 12.5 1 07/02/20 02:48 74-88-4 ND ug/L 5.0 3.7 1 07/02/20 02:48 75-09-2 ND ug/L 5.0 4.5 1 07/02/20 02:48 108-10-1 ND ug/L 1.0 0.27 1 07/02/20 02:48 100-42-5 ND ug/L 1.0 0.34 1 07/02/20 02:48 630-20-6 ND ug/L 1.0 0.22 1 07/02/20 02:48 79-34-5 ND ug/L 1.0 0.16 1 07/02/20 02:48 127-18-4 ND ug/L 1.0 0.24 1 07/02/20 02:48 108-88-3 ND ug/L 1.0 0.18 1 07/02/20 02:48 71-55-6 ND ug/L 1.0 0.24 1 07/02/20 02:48 79-00-5 ND ug/L 1.0 0.22 1 07/02/20 02:48 79-01-6 ND ug/L 1.0 0.31 1 07/02/20 02:48 75-69-4 ND ug/L 1.0 0.35 1 07/02/20 02:48 96-18-4 ND ug/L 2.0 1.4 1 07/02/20 02:48 108-05-4 ND ug/L 1.0 0.24 1 07/02/20 02:48 75-01-4 ND ug/L 1.0 0.63 1 07/02/20 02:48 1330-20-7 98 % 70-130 1 07/02/20 02:48 460-00-4 107 % 70-130 1 07/02/20 02:48 17060-07-0 99 % 70-130 1 07/02/20 02:48 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v1 v2 Page 25 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-22 Lab ID: 92483829011 Collected: 06/25/20 10:59 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 06/30/20 00:35 07/01/20 03:59 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 03:59 7440-38-2 Barium 68.3 ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 03:59 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 06/30/20 00:35 07/01/20 03:59 7440-41-7 Cadmium 1.0 ug/L 1.0 0.40 1 06/30/20 00:35 07/01/20 03:59 7440-43-9 Chromium ND ug/L 5.0 3.7 1 06/30/20 00:35 07/01/20 03:59 7440-47-3 Cobalt 53.6 ug/L 5.0 3.6 1 06/30/20 00:35 07/01/20 03:59 7440-48-4 Copper ND ug/L 5.0 4.3 1 06/30/20 00:35 07/01/20 03:59 7440-50-8 Lead ND ug/L 5.0 4.5 1 06/30/20 00:35 07/01/20 03:59 7439-92-1 Nickel 4.5.1 ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 03:59 7440-02-0 Selenium ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 03:59 7782-49-2 Silver ND ug/L 5.0 2.5 1 06/30/20 00:35 07/01/20 03:59 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 06/30/20 00:35 07/01/20 03:59 7440-62-2 Zinc ND ug/L 10.0 9.5 1 06/30/20 00:35 07/01/20 03:59 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium 0.13 ug/L 0.10 0.050 1 06/30/20 00:13 06/30/20 16:13 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 07/02/20 04:53 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 07/02/20 04:53 107-13-1 Benzene ND ug/L 1.0 0.15 1 07/02/20 04:53 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 07/02/20 04:53 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 07/02/20 04:53 75-27-4 Bromoform ND ug/L 1.0 0.62 1 07/02/20 04:53 75-25-2 Bromomethane 0.67J ug/L 2.0 0.62 1 07/02/20 04:53 74-83-9 2-Butanone (MEK) ND ug/L 5.0 3.3 1 07/02/20 04:53 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 07/02/20 04:53 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 07/02/20 04:53 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 07/02/20 04:53 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 07/02/20 04:53 75-00-3 Chloroform ND ug/L 5.0 2.3 1 07/02/20 04:53 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 07/02/20 04:53 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 07/02/20 04:53 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 07/02/20 04:53 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 07/02/20 04:53 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 07/02/20 04:53 74-95-3 1,2-Dichlorobenzene 0.31J ug/L 1.0 0.29 1 07/02/20 04:53 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 07/02/20 04:53 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 07/02/20 04:53 110-57-6 1,1-Dichloroethane 0.41J ug/L 1.0 0.27 1 07/02/20 04:53 75-34-3 1,2-Dichloroethane 0.44J ug/L 1.0 0.34 1 07/02/20 04:53 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 07/02/20 04:53 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. B,IH,v2 v2 v2 IK Page 26 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-22 Lab ID: 92483829011 Collected: 06/25/20 10:59 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene 1,4-Dioxane (p-Dioxane) Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 07/02/2020 04:47 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1.1 ug/L 1.0 0.29 1 07/02/20 04:53 156-59-2 ND ug/L 1.0 0.25 1 07/02/20 04:53 156-60-5 ND ug/L 1.0 0.19 1 07/02/20 04:53 78-87-5 ND ug/L 1.0 0.30 1 07/02/20 04:53 10061-01-5 ND ug/L 1.0 0.31 1 07/02/20 04:53 10061-02-6 ND ug/L 150 56.2 1 07/02/20 04:53 123-91-1 ND ug/L 1.0 0.26 1 07/02/20 04:53 100-41-4 ND ug/L 5.0 0.57 1 07/02/20 04:53 591-78-6 ND ug/L 20.0 12.5 1 07/02/20 04:53 74-88-4 ND ug/L 5.0 3.7 1 07/02/20 04:53 75-09-2 ND ug/L 5.0 4.5 1 07/02/20 04:53 108-10-1 ND ug/L 1.0 0.27 1 07/02/20 04:53 100-42-5 ND ug/L 1.0 0.34 1 07/02/20 04:53 630-20-6 ND ug/L 1.0 0.22 1 07/02/20 04:53 79-34-5 ND ug/L 1.0 0.16 1 07/02/20 04:53 127-18-4 ND ug/L 1.0 0.24 1 07/02/20 04:53 108-88-3 ND ug/L 1.0 0.18 1 07/02/20 04:53 71-55-6 ND ug/L 1.0 0.24 1 07/02/20 04:53 79-00-5 ND ug/L 1.0 0.22 1 07/02/20 04:53 79-01-6 ND ug/L 1.0 0.31 1 07/02/20 04:53 75-69-4 ND ug/L 1.0 0.35 1 07/02/20 04:53 96-18-4 ND ug/L 2.0 1.4 1 07/02/20 04:53 108-05-4 ND ug/L 1.0 0.24 1 07/02/20 04:53 75-01-4 ND ug/L 1.0 0.63 1 07/02/20 04:53 1330-20-7 99 % 70-130 1 07/02/20 04:53 460-00-4 109 % 70-130 1 07/02/20 04:53 17060-07-0 103 % 70-130 1 07/02/20 04:53 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v1 v2 Page 27 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-23 Lab ID: 92483829012 Collected: 06/25/20 14:05 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 06/30/20 00:35 07/01/20 04:03 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 04:03 7440-38-2 Barium 22.7 ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 04:03 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 06/30/20 00:35 07/01/20 04:03 7440-41-7 Cadmium 0.89J ug/L 1.0 0.40 1 06/30/20 00:35 07/01/20 04:03 7440-43-9 Chromium ND ug/L 5.0 3.7 1 06/30/20 00:35 07/01/20 04:03 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 06/30/20 00:35 07/01/20 04:03 7440-48-4 Copper ND ug/L 5.0 4.3 1 06/30/20 00:35 07/01/20 04:03 7440-50-8 Lead ND ug/L 5.0 4.5 1 06/30/20 00:35 07/01/20 04:03 7439-92-1 Nickel ND ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 04:03 7440-02-0 Selenium ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 04:03 7782-49-2 Silver ND ug/L 5.0 2.5 1 06/30/20 00:35 07/01/20 04:03 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 06/30/20 00:35 07/01/20 04:03 7440-62-2 Zinc ND ug/L 10.0 9.5 1 06/30/20 00:35 07/01/20 04:03 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium ND ug/L 0.10 0.050 1 06/30/20 00:13 06/30/20 16:17 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 07/02/20 05:41 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 07/02/20 05:41 107-13-1 Benzene ND ug/L 1.0 0.15 1 07/02/20 05:41 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 07/02/20 05:41 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 07/02/20 05:41 75-27-4 Bromoform ND ug/L 1.0 0.62 1 07/02/20 05:41 75-25-2 Bromomethane ND ug/L 2.0 0.62 1 07/02/20 05:41 74-83-9 2-Butanone (MEK) ND ug/L 5.0 3.3 1 07/02/20 05:41 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 07/02/20 05:41 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 07/02/20 05:41 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 07/02/20 05:41 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 07/02/20 05:41 75-00-3 Chloroform ND ug/L 5.0 2.3 1 07/02/20 05:41 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 07/02/20 05:41 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 07/02/20 05:41 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 07/02/20 05:41 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 07/02/20 05:41 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 07/02/20 05:41 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.29 1 07/02/20 05:41 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 07/02/20 05:41 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 07/02/20 05:41 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.27 1 07/02/20 05:41 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.34 1 07/02/20 05:41 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 07/02/20 05:41 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. IK v2 Page 28 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 Sample: MW-23 Lab ID: 92483829012 Collected: 06/25/20 14:05 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene 1,4-Dioxane (p-Dioxane) Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 07/02/2020 04:47 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 0.511 ug/L 1.0 0.29 1 07/02/20 05:41 156-59-2 ND ug/L 1.0 0.25 1 07/02/20 05:41 156-60-5 ND ug/L 1.0 0.19 1 07/02/20 05:41 78-87-5 ND ug/L 1.0 0.30 1 07/02/20 05:41 10061-01-5 ND ug/L 1.0 0.31 1 07/02/20 05:41 10061-02-6 ND ug/L 150 56.2 1 07/02/20 05:41 123-91-1 ND ug/L 1.0 0.26 1 07/02/20 05:41 100-41-4 ND ug/L 5.0 0.57 1 07/02/20 05:41 591-78-6 ND ug/L 20.0 12.5 1 07/02/20 05:41 74-88-4 ND ug/L 5.0 3.7 1 07/02/20 05:41 75-09-2 ND ug/L 5.0 4.5 1 07/02/20 05:41 108-10-1 ND ug/L 1.0 0.27 1 07/02/20 05:41 100-42-5 ND ug/L 1.0 0.34 1 07/02/20 05:41 630-20-6 ND ug/L 1.0 0.22 1 07/02/20 05:41 79-34-5 ND ug/L 1.0 0.16 1 07/02/20 05:41 127-18-4 ND ug/L 1.0 0.24 1 07/02/20 05:41 108-88-3 ND ug/L 1.0 0.18 1 07/02/20 05:41 71-55-6 ND ug/L 1.0 0.24 1 07/02/20 05:41 79-00-5 ND ug/L 1.0 0.22 1 07/02/20 05:41 79-01-6 ND ug/L 1.0 0.31 1 07/02/20 05:41 75-69-4 ND ug/L 1.0 0.35 1 07/02/20 05:41 96-18-4 ND ug/L 2.0 1.4 1 07/02/20 05:41 108-05-4 ND ug/L 1.0 0.24 1 07/02/20 05:41 75-01-4 ND ug/L 1.0 0.63 1 07/02/20 05:41 1330-20-7 95 % 70-130 1 07/02/20 05:41 460-00-4 90 % 70-130 1 07/02/20 05:41 17060-07-0 99 % 70-130 1 07/02/20 05:41 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 29 of 52 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 QC Batch: 550337 Analysis Method: EPA 6010D QC Batch Method: EPA 3010A Analysis Description: 6010 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92483829001, 92483829002, 92483829003, 92483829004, 92483829005, 92483829006, 92483829007 METHOD BLANK: 2926131 Matrix: Water Associated Lab Samples: 92483829001, 92483829002, 92483829003, 92483829004, 92483829005, 92483829006, 92483829007 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Antimony ug/L ND 5.0 3.0 06/30/20 23:57 Arsenic ug/L ND 10.0 4.7 06/30/20 23:57 Barium ug/L ND 5.0 3.5 06/30/20 23:57 Beryllium ug/L ND 1.0 0.70 06/30/20 23:57 Cadmium ug/L ND 1.0 0.40 06/30/20 23:57 Chromium ug/L ND 5.0 3.7 07/01/2018:57 Cobalt ug/L ND 5.0 3.6 06/30/20 23:57 Copper ug/L ND 5.0 4.3 06/30/20 23:57 Lead ug/L ND 5.0 4.5 06/30/20 23:57 Nickel ug/L ND 5.0 3.5 06/30/20 23:57 Selenium ug/L ND 10.0 4.7 06/30/20 23:57 Silver ug/L ND 5.0 2.5 06/30/20 23:57 Vanadium ug/L ND 5.0 3.9 07/01/2018:57 Zinc ug/L ND 10.0 9.5 06/30/20 23:57 LABORATORY CONTROL SAMPLE: Parameter 2926132 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Antimony ug/L 500 489 98 80-120 Arsenic ug/L 500 492 98 80-120 Barium ug/L 500 484 97 80-120 Beryllium ug/L 500 470 94 80-120 Cadmium ug/L 500 472 94 80-120 Chromium ug/L 500 495 99 80-120 Cobalt ug/L 500 473 95 80-120 Copper ug/L 500 491 98 80-120 Lead ug/L 500 478 96 80-120 Nickel ug/L 500 472 94 80-120 Selenium ug/L 500 481 96 80-120 Silver ug/L 250 225 90 80-120 Vanadium ug/L 500 499 100 80-120 Zinc ug/L 500 442 88 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 52 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: Surry Closed- Mt. Airy 92483829 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2926133 2926134 MS MSD 92483926003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 512 507 102 101 75-125 1 20 Arsenic ug/L ND 500 500 524 517 105 103 75-125 1 20 Barium ug/L 60.9 500 500 560 550 100 98 75-125 2 20 Beryllium ug/L ND 500 500 493 476 99 95 75-125 4 20 Cadmium ug/L ND 500 500 504 495 101 99 75-125 2 20 Chromium ug/L ND 500 500 515 ND 103 0 75-125 20 M1 Cobalt ug/L ND 500 500 495 483 99 97 75-125 2 20 Copper ug/L ND 500 500 500 496 100 99 75-125 1 20 Lead ug/L ND 500 500 494 488 99 98 75-125 1 20 Nickel ug/L ND 500 500 494 482 98 96 75-125 2 20 Selenium ug/L ND 500 500 533 530 107 106 75-125 1 20 Silver ug/L ND 250 250 237 232 95 93 75-125 2 20 Vanadium ug/L ND 500 500 513 ND 103 0 75-125 20 M1 Zinc ug/L ND 500 500 490 469 97 93 75-125 4 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 52 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 QC Batch: 550338 Analysis Method: EPA 6010D QC Batch Method: EPA 3010A Analysis Description: 6010 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92483829008, 92483829009, 92483829010, 92483829011, 92483829012 METHOD BLANK: 2926135 Matrix: Water Associated Lab Samples: 92483829008, 92483829009, 92483829010, 92483829011, 92483829012 Blank Reporting Parameter Units Result Limit MDL Antimony ug/L ND 5.0 Arsenic ug/L ND 10.0 Barium ug/L ND 5.0 Beryllium ug/L ND 1.0 Cadmium ug/L ND 1.0 Chromium ug/L ND 5.0 Cobalt ug/L ND 5.0 Copper ug/L ND 5.0 Lead ug/L ND 5.0 Nickel ug/L ND 5.0 Selenium ug/L ND 10.0 Silver ug/L ND 5.0 Vanadium ug/L ND 5.0 Zinc ug/L ND 10.0 Analyzed 3.0 07/01 /20 03:21 4.7 07/01 /20 03:21 3.5 07/01 /20 03:21 0.70 07/01 /20 03:21 0.40 07/01 /20 03:21 3.7 07/01 /20 03:21 3.6 07/01 /20 03:21 4.3 07/01 /20 03:21 4.5 07/01 /20 03:21 3.5 07/01 /20 03:21 4.7 07/01 /20 03:21 2.5 07/01 /20 03:21 3.9 07/01 /20 03:21 9.5 07/01 /20 03:21 LABORATORY CONTROL SAMPLE: Parameter 2926136 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 498 100 80-120 Arsenic ug/L 500 504 101 80-120 Barium ug/L 500 502 100 80-120 Beryllium ug/L 500 493 99 80-120 Cadmium ug/L 500 490 98 80-120 Chromium ug/L 500 479 96 80-120 Cobalt ug/L 500 491 98 80-120 Copper ug/L 500 504 101 80-120 Lead ug/L 500 496 99 80-120 Nickel ug/L 500 493 99 80-120 Selenium ug/L 500 488 98 80-120 Silver ug/L 250 239 96 80-120 Vanadium ug/L 500 478 96 80-120 Zinc ug/L 500 468 94 80-120 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 52 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: Surry Closed- Mt. Airy 92483829 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2926137 2926138 MS MSD 92483829008 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 507 502 101 100 75-125 1 20 Arsenic ug/L ND 500 500 514 511 103 102 75-125 1 20 Barium ug/L 18.9 500 500 520 516 100 99 75-125 1 20 Beryllium ug/L ND 500 500 495 491 99 98 75-125 1 20 Cadmium ug/L 0.43J 500 500 507 501 101 100 75-125 1 20 Chromium ug/L ND 500 500 479 479 96 96 75-125 0 20 Cobalt ug/L ND 500 500 489 485 98 97 75-125 1 20 Copper ug/L ND 500 500 508 503 101 100 75-125 1 20 Lead ug/L ND 500 500 492 488 98 98 75-125 1 20 Nickel ug/L ND 500 500 493 488 98 97 75-125 1 20 Selenium ug/L ND 500 500 523 522 105 104 75-125 0 20 Silver ug/L ND 250 250 243 242 97 97 75-125 1 20 Vanadium ug/L ND 500 500 483 480 97 96 75-125 0 20 Zinc ug/L ND 500 500 478 474 96 95 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 52 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 QC Batch: 550340 Analysis Method: EPA 6020B QC Batch Method: EPA 3010A Analysis Description: 6020 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92483829001, 92483829002, 92483829003, 92483829004, 92483829005 METHOD BLANK: 2926143 Matrix: Water Associated Lab Samples: 92483829001, 92483829002, 92483829003, 92483829004, 92483829005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L ND 0.10 0.050 06/30/2013:04 LABORATORY CONTROL SAMPLE: 2926144 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 10 10.1 101 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2926145 2926146 MS MSD 92483822002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L ND 10 10 10.1 10.3 100 102 75-125 2 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 52 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 QC Batch: 550341 Analysis Method: EPA 6020B QC Batch Method: EPA 3010A Analysis Description: 6020 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92483829006,92483829007,92483829008,92483829009,92483829010,92483829011,92483829012 METHOD BLANK: 2926147 Matrix: Water Associated Lab Samples: 92483829006,92483829007,92483829008,92483829009,92483829010,92483829011,92483829012 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L ND 0.10 0.050 06/30/2015:24 LABORATORY CONTROL SAMPLE: 2926148 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 10 10.2 102 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2926149 2926150 MS MSD 92483829006 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L 0.0901 10 10 10.1 10.3 100 102 75-125 2 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 52 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 QC Batch: 550875 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92483829001, 92483829003, 92483829009, 92483829012 METHOD BLANK: 2928332 Matrix: Water Associated Lab Samples: 92483829001, 92483829003, 92483829009, 92483829012 Blank Reporting Parameter Units Result Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.34 07/02/20 00:15 1,1,1-Trichloroethane ug/L ND 1.0 0.18 07/02/20 00:15 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 07/02/20 00:15 1,1,2-Trichloroethane ug/L ND 1.0 0.24 07/02/20 00:15 1,1-Dichloroethane ug/L ND 1.0 0.27 07/02/20 00:15 1,1-Dichloroethene ug/L ND 1.0 0.24 07/02/20 00:15 1,2,3-Trichloropropane ug/L ND 1.0 0.35 07/02/20 00:15 1,2-Dibromo-3-chloropropane ug/L ND 5.0 0.26 07/02/20 00:15 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.26 07/02/20 00:15 1,2-Dichlorobenzene ug/L ND 1.0 0.29 07/02/20 00:15 1,2-Dichloroethane ug/L ND 1.0 0.34 07/02/20 00:15 1,2-Dichloropropane ug/L ND 1.0 0.19 07/02/20 00:15 1,4-Dichlorobenzene ug/L ND 1.0 0.26 07/02/20 00:15 1,4-Dioxane (p-Dioxane) ug/L ND 150 56.2 07/02/20 00:15 2-Butanone (MEK) ug/L ND 5.0 3.3 07/02/20 00:15 2-Hexanone ug/L ND 5.0 0.57 07/02/20 00:15 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 4.5 07/02/20 00:15 Acetone ug/L ND 25.0 6.2 07/02/20 00:15 Acrylonitrile ug/L ND 10.0 0.90 07/02/20 00:15 Benzene ug/L ND 1.0 0.15 07/02/20 00:15 Bromochloromethane ug/L ND 1.0 0.34 07/02/20 00:15 Bromodichloromethane ug/L ND 1.0 0.26 07/02/20 00:15 Bromoform ug/L ND 1.0 0.62 07/02/20 00:15 Bromomethane ug/L ND 2.0 0.62 07/02/20 00:15 Carbon disulfide ug/L ND 2.0 0.40 07/02/20 00:15 Carbon tetrachloride ug/L ND 1.0 0.22 07/02/20 00:15 Chlorobenzene ug/L ND 1.0 0.23 07/02/20 00:15 Chloroethane ug/L ND 1.0 0.49 07/02/20 00:15 Chloroform ug/L ND 5.0 2.3 07/02/20 00:15 Chloromethane ug/L ND 1.0 0.39 07/02/20 00:15 cis-1,2-Dichloroethene ug/L ND 1.0 0.29 07/02/20 00:15 cis-1,3-Dichloropropene ug/L ND 1.0 0.30 07/02/20 00:15 Dibromochloromethane ug/L ND 1.0 0.41 07/02/20 00:15 Dibromomethane ug/L ND 1.0 0.46 07/02/20 00:15 Ethylbenzene ug/L ND 1.0 0.26 07/02/20 00:15 lodomethane ug/L ND 20.0 12.5 07/02/20 00:15 Methylene Chloride ug/L ND 5.0 3.7 07/02/20 00:15 Styrene ug/L ND 1.0 0.27 07/02/20 00:15 Tetrachloroethene ug/L ND 1.0 0.16 07/02/20 00:15 Toluene ug/L ND 1.0 0.24 07/02/20 00:15 13 v2 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 52 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 METHOD BLANK: 2928332 Matrix: Water Associated Lab Samples: 92483829001, 92483829003, 92483829009, 92483829012 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers trans-1,2-Dichloroethene ug/L ND 1.0 0.25 07/02/20 00:15 trans- 1,3-Dichloropropene ug/L ND 1.0 0.31 07/02/20 00:15 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.54 07/02/20 00:15 Trichloroethene ug/L ND 1.0 0.22 07/02/20 00:15 Trichlorofluoromethane ug/L ND 1.0 0.31 07/02/20 00:15 Vinyl acetate ug/L ND 2.0 1.4 07/02/20 00:15 Vinyl chloride ug/L ND 1.0 0.24 07/02/20 00:15 Xylene (Total) ug/L ND 1.0 0.63 07/02/20 00:15 1,2-Dichloroethane-d4 (S) % 90 70-130 07/02/20 00:15 4-Bromofluorobenzene (S) % 95 70-130 07/02/20 00:15 Toluene-d8 (S) % 99 70-130 07/02/20 00:15 LABORATORY CONTROL SAMPLE: Parameter 2928333 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 53.7 107 70-130 1,1,1-Trichloroethane ug/L 50 47.5 95 70-130 1,1,2,2-Tetrachloroethane ug/L 50 53.5 107 70-130 1,1,2-Trichloroethane ug/L 50 50.2 100 70-130 1,1-Dichloroethane ug/L 50 46.3 93 70-130 1,1-Dichloroethene ug/L 50 49.5 99 70-130 1,2,3-Trichloropropane ug/L 50 52.9 106 70-130 1,2-Dibromo-3-chloropropane ug/L 50 51.0 102 70-130 1,2-Dibromoethane (EDB) ug/L 50 52.3 105 70-130 1,2-Dichlorobenzene ug/L 50 52.2 104 70-130 1,2-Dichloroethane ug/L 50 48.2 96 70-130 1,2-Dichloropropane ug/L 50 50.0 100 70-130 1,4-Dichlorobenzene ug/L 50 51.9 104 70-130 1,4-Dioxane(p-Dioxane) ug/L 1000 1060 106 59-169 2-Butanone (MEK) ug/L 100 88.8 89 64-135 2-Hexanone ug/L 100 103 103 66-135 4-Methyl-2-pentanone (MIBK) ug/L 100 96.9 97 70-130 Acetone ug/L 100 86.1 86 61-157 Acrylonitrile ug/L 250 223 89 61-143 Benzene ug/L 50 49.4 99 70-130 Bromochloromethane ug/L 50 47.3 95 70-130 Bromodichloromethane ug/L 50 46.4 93 70-130 Bromoform ug/L 50 54.0 108 70-130 Bromomethane ug/L 50 43.4 87 38-130lK Carbon disulfide ug/L 50 43.2 86 68-130 Carbon tetrachloride ug/L 50 50.4 101 70-130 Chlorobenzene ug/L 50 51.3 103 70-130 Chloroethane ug/L 50 51.5 103 37-142 Chloroform ug/L 50 47.1 94 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 52 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 LABORATORY CONTROL SAMPLE: Parameter 2928333 Units Spike Conc. LCS LCS Result % Rec Chloromethane ug/L 50 33.5 cis-1,2-Dichloroethene ug/L 50 47.0 cis-1,3-Dichloropropene ug/L 50 51.7 Dibromochloromethane ug/L 50 53.5 Dibromomethane ug/L 50 51.2 Ethylbenzene ug/L 50 51.3 lodomethane ug/L 100 77.6 Methylene Chloride ug/L 50 46.5 Styrene ug/L 50 54.7 Tetrachloroethene ug/L 50 50.4 Toluene ug/L 50 48.4 trans-1,2-Dichloroethene ug/L 50 47.7 trans- 1,3-Dichloropropene ug/L 50 50.8 trans-1,4-Dichloro-2-butene ug/L 50 50.2 Trichloroethene ug/L 50 51.9 Trichlorofluoromethane ug/L 50 45.5 Vinyl acetate ug/L 100 94.3 Vinyl chloride ug/L 50 40.7 Xylene (Total) ug/L 150 156 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % % Rec Limits Qualifiers 67 48-130 v3 94 70-130 103 70-130 107 70-130 102 70-130 103 70-130 78 40-130 93 67-132 109 70-130 101 69-130 97 70-130 95 70-130 102 70-130 100 35-189 104 70-130 91 63-130 94 55-143 81 70-131 104 70-130 92 70-130 104 70-130 96 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2928334 MS 92483822003 Spike Parameter Units Result Conc. MSD Spike Conc. 2928335 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 21.2 20.9 106 105 73-134 1 30 1,1,1-Trichloroethane ug/L ND 20 20 24.0 23.9 120 119 82-143 1 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 23.4 23.3 117 116 70-136 1 30 1,1,2-Trichloroethane ug/L ND 20 20 21.9 21.7 109 108 70-135 1 30 1,1-Dichloroethane ug/L ND 20 20 25.8 25.6 129 128 70-139 1 30 1,1-Dichloroethene ug/L ND 20 20 26.5 26.4 132 132 70-154 0 30 1,2,3-Trichloropropane ug/L ND 20 20 22.5 22.9 112 115 71-137 2 30 1,2-Dibromo-3- ug/L ND 20 20 20.6 20.4 103 102 65-134 1 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 22.6 22.6 113 113 70-137 0 30 1,2-Dichlorobenzene ug/L ND 20 20 23.0 23.0 115 115 70-133 0 30 1,2-Dichloroethane ug/L ND 20 20 24.4 24.4 122 122 70-137 0 30 1,2-Dichloropropane ug/L ND 20 20 24.1 24.1 121 121 70-140 0 30 1,4-Dichlorobenzene ug/L ND 20 20 22.5 22.4 112 112 70-133 0 30 1,4-Dioxane (p-Dioxane) ug/L ND 400 400 479 485 120 121 53-168 1 30 2-Butanone (MEK) ug/L ND 40 40 53.2 51.9 133 130 60-139 2 30 2-Hexanone ug/L ND 40 40 48.1 47.5 120 119 65-138 1 30 4-Methyl-2-pentanone ug/L ND 40 40 46.4 45.8 116 114 65-135 1 30 (MIBK) Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 52 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2928334 2928335 MS MSD 92483822003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Acetone ug/L ND 40 40 56.4 54.7 141 137 60-148 3 30 v1 Acrylonitrile ug/L ND 100 100 123 126 123 126 64-147 2 30 Benzene ug/L ND 20 20 23.3 23.4 117 117 70-151 0 30 Bromochloromethane ug/L ND 20 20 23.7 23.8 118 119 70-141 0 30 Bromodichloromethane ug/L ND 20 20 19.3 19.6 97 98 70-138 2 30 Bromoform ug/L ND 20 20 18.2 18.2 91 91 63-130 0 30 Bromomethane ug/L ND 20 20 28.5 28.8 142 144 15-152 1 30 Carbon disulfide ug/L ND 20 20 25.9 25.8 129 129 69-149 1 30 Carbon tetrachloride ug/L ND 20 20 20.9 21.3 104 106 70-143 2 30 Chlorobenzene ug/L ND 20 20 22.5 22.7 112 113 70-138 1 30 Chloroethane ug/L ND 20 20 38.1 37.4 190 187 52-163 2 30 IK,IL, M1,v1 Chloroform ug/L ND 20 20 23.8 23.6 119 118 70-139 1 30 Chloromethane ug/L ND 20 20 24.4 24.6 122 123 41-139 1 30 cis-1,2-Dichloroethene ug/L ND 20 20 25.0 25.0 125 125 70-141 0 30 cis-1,3-Dichloropropene ug/L ND 20 20 22.6 22.6 113 113 70-137 0 30 Dibromochloromethane ug/L ND 20 20 20.4 20.3 102 101 70-134 1 30 Dibromomethane ug/L ND 20 20 20.5 20.4 103 102 70-138 1 30 Ethylbenzene ug/L ND 20 20 22.8 22.9 114 115 66-153 0 30 lodomethane ug/L ND 40 40 28.6 28.0 71 70 20-138 2 30 v3 Methylene Chloride ug/L ND 20 20 25.3 25.5 126 127 42-159 1 30 Styrene ug/L ND 20 20 22.8 22.5 114 113 70-135 1 30 Tetrachloroethene ug/L ND 20 20 20.7 21.2 103 106 59-143 3 30 Toluene ug/L ND 20 20 22.4 22.5 112 112 59-148 0 30 trans-1,2-Dichloroethene ug/L ND 20 20 26.2 26.4 131 132 70-146 1 30 trans-1,3-Dichloropropene ug/L ND 20 20 21.7 21.8 108 109 70-135 0 30 trans-1,4-Dichloro-2-butene ug/L ND 20 20 17.7 17.8 88 89 47-135 1 30 Trichloroethene ug/L ND 20 20 22.1 22.3 110 111 70-147 1 30 Trichlorofluoromethane ug/L ND 20 20 25.0 25.1 125 125 70-148 0 30 Vinyl acetate ug/L ND 40 40 50.8 49.8 127 125 49-151 2 30 Vinyl chloride ug/L ND 20 20 23.4 23.0 117 115 70-156 2 30 Xylene (Total) ug/L ND 60 60 68.8 69.3 115 115 63-158 1 30 1,2-Dichloroethane-d4 (S) % 115 116 70-130 4-Bromofluorobenzene (S) % 101 101 70-130 Toluene-d8 (S) % 102 103 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 52 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 QC Batch: 550877 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92483829002, 92483829005, 92483829008 METHOD BLANK: 2928353 Matrix: Associated Lab Samples: 92483829002, 92483829005, 92483829008 Blank Parameter Units Result Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.34 07/01/20 22:24 1,1,1-Trichloroethane ug/L ND 1.0 0.18 07/01/20 22:24 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 07/01/20 22:24 1,1,2-Trichloroethane ug/L ND 1.0 0.24 07/01/20 22:24 1,1-Dichloroethane ug/L ND 1.0 0.27 07/01/20 22:24 1,1-Dichloroethene ug/L ND 1.0 0.24 07/01/20 22:24 1,2,3-Trichloropropane ug/L ND 1.0 0.35 07/01/20 22:24 1,2-Dibromo-3-chloropropane ug/L ND 5.0 0.26 07/01/20 22:24 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.26 07/01/20 22:24 1,2-Dichlorobenzene ug/L ND 1.0 0.29 07/01/20 22:24 1,2-Dichloroethane ug/L ND 1.0 0.34 07/01/20 22:24 1,2-Dichloropropane ug/L ND 1.0 0.19 07/01/20 22:24 1,4-Dichlorobenzene ug/L ND 1.0 0.26 07/01/20 22:24 1,4-Dioxane (p-Dioxane) ug/L ND 150 56.2 07/01/20 22:24 2-Butanone (MEK) ug/L ND 5.0 3.3 07/01/20 22:24 2-Hexanone ug/L ND 5.0 0.57 07/01/20 22:24 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 4.5 07/01/20 22:24 Acetone ug/L ND 25.0 6.2 07/01/20 22:24 Acrylonitrile ug/L ND 10.0 0.90 07/01/20 22:24 Benzene ug/L ND 1.0 0.15 07/01/20 22:24 Bromochloromethane ug/L ND 1.0 0.34 07/01/20 22:24 Bromodichloromethane ug/L ND 1.0 0.26 07/01/20 22:24 Bromoform ug/L ND 1.0 0.62 07/01/20 22:24 Bromomethane ug/L ND 2.0 0.62 07/01/20 22:24 Carbon disulfide ug/L ND 2.0 0.40 07/01/20 22:24 Carbon tetrachloride ug/L ND 1.0 0.22 07/01/20 22:24 Chlorobenzene ug/L ND 1.0 0.23 07/01/20 22:24 Chloroethane ug/L ND 1.0 0.49 07/01/20 22:24 Chloroform ug/L ND 5.0 2.3 07/01/20 22:24 Chloromethane ug/L ND 1.0 0.39 07/01/20 22:24 cis-1,2-Dichloroethene ug/L ND 1.0 0.29 07/01/20 22:24 cis-1,3-Dichloropropene ug/L ND 1.0 0.30 07/01/20 22:24 Dibromochloromethane ug/L ND 1.0 0.41 07/01/20 22:24 Dibromomethane ug/L ND 1.0 0.46 07/01/20 22:24 Ethylbenzene ug/L ND 1.0 0.26 07/01/20 22:24 lodomethane ug/L ND 20.0 12.5 07/01/20 22:24 Methylene Chloride ug/L ND 5.0 3.7 07/01/20 22:24 Styrene ug/L ND 1.0 0.27 07/01/20 22:24 Tetrachloroethene ug/L ND 1.0 0.16 07/01/20 22:24 Toluene ug/L ND 1.0 0.24 07/01/20 22:24 v1 v1 v2 v1 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 52 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 METHOD BLANK: 2928353 Matrix: Associated Lab Samples: 92483829002, 92483829005, 92483829008 Blank Parameter Units Result Water Reporting Limit MDL Analyzed Qualifiers trans-1,2-Dichloroethene ug/L ND 1.0 0.25 07/01/20 22:24 trans- 1,3-Dichloropropene ug/L ND 1.0 0.31 07/01/20 22:24 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.54 07/01/20 22:24 v2 Trichloroethene ug/L ND 1.0 0.22 07/01/20 22:24 Trichlorofluoromethane ug/L ND 1.0 0.31 07/01/20 22:24 Vinyl acetate ug/L ND 2.0 1.4 07/01/20 22:24 IK Vinyl chloride ug/L ND 1.0 0.24 07/01/20 22:24 Xylene (Total) ug/L ND 1.0 0.63 07/01/20 22:24 1,2-Dichloroethane-d4 (S) % 90 70-130 07/01/20 22:24 4-Bromofluorobenzene (S) % 100 70-130 07/01/20 22:24 Toluene-d8 (S) % 100 70-130 07/01/20 22:24 LABORATORY CONTROL SAMPLE: Parameter 2928354 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 58.6 117 70-130 1,1,1-Trichloroethane ug/L 50 50.3 101 70-130 1,1,2,2-Tetrachloroethane ug/L 50 53.6 107 70-130 1,1,2-Trichloroethane ug/L 50 54.0 108 70-130 1,1-Dichloroethane ug/L 50 46.7 93 70-130 1,1-Dichloroethene ug/L 50 48.2 96 70-130 1,2,3-Trichloropropane ug/L 50 53.7 107 70-130 1,2-Dibromo-3-chloropropane ug/L 50 58.8 118 70-130 1,2-Dibromoethane (EDB) ug/L 50 58.1 116 70-130 1,2-Dichlorobenzene ug/L 50 56.6 113 70-130 1,2-Dichloroethane ug/L 50 47.1 94 70-130 1,2-Dichloropropane ug/L 50 49.7 99 70-130 1,4-Dichlorobenzene ug/L 50 56.9 114 70-130 1,4-Dioxane(p-Dioxane) ug/L 1000 1340 134 59-169 v1 2-Butanone (MEK) ug/L 100 101 101 64-135 2-Hexanone ug/L 100 103 103 66-135 4-Methyl-2-pentanone (MIBK) ug/L 100 95.8 96 70-130 Acetone ug/L 100 101 101 61-157 Acrylonitrile ug/L 250 227 91 61-143 Benzene ug/L 50 50.9 102 70-130 Bromochloromethane ug/L 50 54.3 109 70-130 Bromodichloromethane ug/L 50 46.7 93 70-130 Bromoform ug/L 50 61.5 123 70-130 v1 Bromomethane ug/L 50 30.1 60 38-130 v3 Carbon disulfide ug/L 50 49.5 99 68-130 Carbon tetrachloride ug/L 50 52.9 106 70-130 Chlorobenzene ug/L 50 56.1 112 70-130 Chloroethane ug/L 50 44.4 89 37-142 Chloroform ug/L 50 49.4 99 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 52 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 LABORATORY CONTROL SAMPLE: Parameter 2928354 Units Spike Conc. LCS LCS Result % Rec Chloromethane ug/L 50 33.8 cis-1,2-Dichloroethene ug/L 50 47.2 cis-1,3-Dichloropropene ug/L 50 54.7 Dibromochloromethane ug/L 50 60.6 Dibromomethane ug/L 50 57.2 Ethylbenzene ug/L 50 53.2 lodomethane ug/L 100 92.7 Methylene Chloride ug/L 50 42.2 Styrene ug/L 50 56.0 Tetrachloroethene ug/L 50 57.7 Toluene ug/L 50 51.7 trans-1,2-Dichloroethene ug/L 50 47.3 trans- 1,3-Dichloropropene ug/L 50 53.2 trans-1,4-Dichloro-2-butene ug/L 50 29.5 Trichloroethene ug/L 50 57.3 Trichlorofluoromethane ug/L 50 46.2 Vinyl acetate ug/L 100 95.9 Vinyl chloride ug/L 50 40.9 Xylene (Total) ug/L 150 162 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % % Rec Limits Qualifiers 68 48-130 94 70-130 109 70-130 121 70-130 v3 114 70-130 106 70-130 93 40-130 84 67-132 112 70-130 115 69-130 103 70-130 95 70-130 106 70-130 59 35-189 v3 115 70-130 92 63-130 96 55-1431K 82 70-131 108 70-130 88 70-130 97 70-130 96 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2928355 MS 7332839008 Spike Parameter Units Result Conc. MSD Spike Conc. 2928356 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 17.2 18.7 86 94 73-134 9 30 1,1,1-Trichloroethane ug/L ND 20 20 16.4 16.8 82 84 82-143 3 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 18.3 19.4 92 97 70-136 5 30 1,1,2-Trichloroethane ug/L ND 20 20 15.3 16.2 77 81 70-135 5 30 1,1-Dichloroethane ug/L ND 20 20 17.6 18.5 86 90 70-139 5 30 1,1-Dichloroethene ug/L ND 20 20 18.9 17.8 95 89 70-154 6 30 1,2,3-Trichloropropane ug/L ND 20 20 19.5 19.4 97 97 71-137 0 30 1,2-Dibromo-3- ug/L ND 20 20 19.4 22.1 97 111 65-134 13 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 18.1 19.7 90 99 70-137 9 30 1,2-Dichlorobenzene ug/L ND 20 20 19.2 20.2 96 101 70-133 5 30 1,2-Dichloroethane ug/L ND 20 20 15.1 15.7 76 78 70-137 4 30 1,2-Dichloropropane ug/L ND 20 20 16.9 16.9 85 84 70-140 0 30 1,4-Dichlorobenzene ug/L ND 20 20 16.7 19.1 84 96 70-133 14 30 1,4-Dioxane (p-Dioxane) ug/L ND 400 400 442 393 111 98 53-168 12 30 2-Butanone (MEK) ug/L ND 40 40 35.1 35.7 88 89 60-139 2 30 2-Hexanone ug/L ND 40 40 40.1 39.3 100 98 65-138 2 30 4-Methyl-2-pentanone ug/L ND 40 40 33.1 33.7 83 84 65-135 2 30 (MIBK) Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 52 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2928355 2928356 MS MSD 7332839008 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Acetone ug/L ND 40 40 38.6 41.3 97 103 60-148 7 30 Acrylonitrile ug/L ND 100 100 87.1 90.0 87 90 64-147 3 30 Benzene ug/L ND 20 20 17.5 18.0 87 90 70-151 3 30 Bromochloromethane ug/L ND 20 20 17.4 18.4 87 92 70-141 6 30 Bromodichloromethane ug/L ND 20 20 13.9 15.1 70 76 70-138 8 30 Bromoform ug/L ND 20 20 16.1 17.7 81 88 63-130 9 30 Bromomethane ug/L ND 20 20 19.4 19.3 97 97 15-152 1 30 IH,v3 Carbon disulfide ug/L ND 20 20 17.6 17.2 88 86 69-149 2 30 Carbon tetrachloride ug/L ND 20 20 16.4 17.2 82 86 70-143 5 30 Chlorobenzene ug/L ND 20 20 18.5 18.2 93 91 70-138 2 30 Chloroethane ug/L ND 20 20 16.4 16.5 82 82 52-163 1 30 Chloroform ug/L ND 20 20 16.7 17.6 84 88 70-139 5 30 Chloromethane ug/L ND 20 20 12.4 12.9 62 65 41-139 4 30 v3 cis-1,2-Dichloroethene ug/L ND 20 20 17.0 17.7 84 88 70-141 4 30 cis-1,3-Dichloropropene ug/L ND 20 20 17.0 18.4 85 92 70-137 8 30 Dibromochloromethane ug/L ND 20 20 17.2 17.6 86 88 70-134 2 30 Dibromomethane ug/L ND 20 20 18.5 19.0 92 95 70-138 3 30 Ethylbenzene ug/L ND 20 20 18.2 18.5 91 93 66-153 2 30 lodomethane ug/L ND 40 40 34.8 34.2 87 85 20-138 2 30 v3 Methylene Chloride ug/L ND 20 20 16.2 17.0 81 85 42-159 4 30 Styrene ug/L ND 20 20 18.5 19.3 92 96 70-135 4 30 Tetrachloroethene ug/L ND 20 20 18.4 18.3 92 92 59-143 1 30 Toluene ug/L ND 20 20 16.1 16.9 80 84 59-148 5 30 trans-1,2-Dichloroethene ug/L ND 20 20 16.6 17.9 83 90 70-146 8 30 trans-1,3-Dichloropropene ug/L ND 20 20 15.7 17.3 78 87 70-135 10 30 trans-1,4-Dichloro-2-butene ug/L ND 20 20 13.3 13.7 66 68 47-135 3 30 IK,v3 Trichloroethene ug/L ND 20 20 17.4 17.3 87 86 70-147 1 30 Trichlorofluoromethane ug/L ND 20 20 13.9 14.5 69 72 70-148 4 30 M1 Vinyl acetate ug/L ND 40 40 33.0 33.8 83 84 49-151 2 30 Vinyl chloride ug/L ND 20 20 14.4 15.2 72 76 70-156 6 30 Xylene (Total) ug/L ND 60 60 56.9 57.4 95 96 63-158 1 30 1,2-Dichloroethane-d4 (S) % 94 94 70-130 4-Bromofluorobenzene (S) % 103 99 70-130 Toluene-d8 (S) % 96 100 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 52 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 QC Batch: 550889 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92483829004, 92483829006, 92483829007, 92483829010, 92483829011 METHOD BLANK: 2928454 Matrix: Water Associated Lab Samples: 92483829004, 92483829006, 92483829007, 92483829010, 92483829011 Blank Reporting Parameter Units Result Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.34 07/02/20 01:01 1,1,1-Trichloroethane ug/L ND 1.0 0.18 07/02/20 01:01 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 07/02/20 01:01 1,1,2-Trichloroethane ug/L ND 1.0 0.24 07/02/20 01:01 1,1-Dichloroethane ug/L ND 1.0 0.27 07/02/20 01:01 1,1-Dichloroethene ug/L ND 1.0 0.24 07/02/20 01:01 1,2,3-Trichloropropane ug/L ND 1.0 0.35 07/02/20 01:01 1,2-Dibromo-3-chloropropane ug/L ND 5.0 0.26 07/02/20 01:01 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.26 07/02/20 01:01 1,2-Dichlorobenzene ug/L ND 1.0 0.29 07/02/20 01:01 1,2-Dichloroethane ug/L ND 1.0 0.34 07/02/20 01:01 1,2-Dichloropropane ug/L ND 1.0 0.19 07/02/20 01:01 1,4-Dichlorobenzene ug/L ND 1.0 0.26 07/02/20 01:01 1,4-Dioxane (p-Dioxane) ug/L ND 150 56.2 07/02/20 01:01 2-Butanone (MEK) ug/L ND 5.0 3.3 07/02/20 01:01 2-Hexanone ug/L ND 5.0 0.57 07/02/20 01:01 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 4.5 07/02/20 01:01 Acetone ug/L ND 25.0 6.2 07/02/20 01:01 Acrylonitrile ug/L ND 10.0 0.90 07/02/20 01:01 Benzene ug/L ND 1.0 0.15 07/02/20 01:01 Bromochloromethane ug/L ND 1.0 0.34 07/02/20 01:01 Bromodichloromethane ug/L ND 1.0 0.26 07/02/20 01:01 Bromoform ug/L ND 1.0 0.62 07/02/20 01:01 Bromomethane ug/L 0.89J 2.0 0.62 07/02/20 01:01 Carbon disulfide ug/L ND 2.0 0.40 07/02/20 01:01 Carbon tetrachloride ug/L ND 1.0 0.22 07/02/20 01:01 Chlorobenzene ug/L ND 1.0 0.23 07/02/20 01:01 Chloroethane ug/L ND 1.0 0.49 07/02/20 01:01 Chloroform ug/L ND 5.0 2.3 07/02/20 01:01 Chloromethane ug/L ND 1.0 0.39 07/02/20 01:01 cis-1,2-Dichloroethene ug/L ND 1.0 0.29 07/02/20 01:01 cis-1,3-Dichloropropene ug/L ND 1.0 0.30 07/02/20 01:01 Dibromochloromethane ug/L ND 1.0 0.41 07/02/20 01:01 Dibromomethane ug/L ND 1.0 0.46 07/02/20 01:01 Ethylbenzene ug/L ND 1.0 0.26 07/02/20 01:01 lodomethane ug/L ND 20.0 12.5 07/02/20 01:01 Methylene Chloride ug/L ND 5.0 3.7 07/02/20 01:01 Styrene ug/L ND 1.0 0.27 07/02/20 01:01 Tetrachloroethene ug/L ND 1.0 0.16 07/02/20 01:01 Toluene ug/L ND 1.0 0.24 07/02/20 01:01 Qualifiers v1 IH,v2 v2 v2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 52 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 METHOD BLANK: 2928454 Matrix: Water Associated Lab Samples: 92483829004, 92483829006, 92483829007, 92483829010, 92483829011 Blank Reporting Parameter Units Result Limit MDL Analyzed trans-1,2-Dichloroethene ug/L ND 1.0 0.25 07/02/20 01:01 trans- 1,3-Dichloropropene ug/L ND 1.0 0.31 07/02/20 01:01 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.54 07/02/20 01:01 Trichloroethene ug/L ND 1.0 0.22 07/02/20 01:01 Trichlorofluoromethane ug/L ND 1.0 0.31 07/02/20 01:01 Vinyl acetate ug/L ND 2.0 1.4 07/02/20 01:01 Vinyl chloride ug/L ND 1.0 0.24 07/02/20 01:01 Xylene (Total) ug/L ND 1.0 0.63 07/02/20 01:01 1,2-Dichloroethane-d4 (S) % 106 70-130 07/02/20 01:01 4-Bromofluorobenzene (S) % 102 70-130 07/02/20 01:01 Toluene-d8 (S) % 100 70-130 07/02/20 01:01 Parameter Qualifiers IK v2 Spike LCS LCS % Rec Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 53.4 107 70-130 1,1,1-Trichloroethane ug/L 50 46.6 93 70-130 1,1,2,2-Tetrachloroethane ug/L 50 53.7 107 70-130 1,1,2-Trichloroethane ug/L 50 47.2 94 70-130 1,1-Dichloroethane ug/L 50 48.2 96 70-130 1,1-Dichloroethene ug/L 50 47.6 95 70-130 1,2,3-Trichloropropane ug/L 50 54.5 109 70-130 1,2-Dibromo-3-chloropropane ug/L 50 58.8 118 70-130 1,2-Dibromoethane (EDB) ug/L 50 53.3 107 70-130 1,2-Dichlorobenzene ug/L 50 52.7 105 70-130 1,2-Dichloroethane ug/L 50 44.0 88 70-130 1,2-Dichloropropane ug/L 50 49.1 98 70-130 1,4-Dichlorobenzene ug/L 50 52.0 104 70-130 1,4-Dioxane(p-Dioxane) ug/L 1000 1180 118 59-169 2-Butanone (MEK) ug/L 100 99.1 99 64-135 2-Hexanone ug/L 100 121 121 66-135 v1 4-Methyl-2-pentanone (MIBK) ug/L 100 99.4 99 70-130 Acetone ug/L 100 103 103 61-157 Acrylonitrile ug/L 250 241 96 61-143 Benzene ug/L 50 49.4 99 70-130 Bromochloromethane ug/L 50 49.9 100 70-130 Bromodichloromethane ug/L 50 44.2 88 70-130 Bromoform ug/L 50 54.2 108 70-130 Bromomethane ug/L 50 38.4 77 38-130lH,v3 Carbon disulfide ug/L 50 44.3 89 68-130 Carbon tetrachloride ug/L 50 51.0 102 70-130 Chlorobenzene ug/L 50 52.5 105 70-130 Chloroethane ug/L 50 39.0 78 37-142 v3 Chloroform ug/L 50 46.7 93 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 52 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 LABORATORY CONTROL SAMPLE: Parameter 2928455 Units Spike Conc. LCS LCS Result % Rec Chloromethane ug/L 50 33.0 cis-1,2-Dichloroethene ug/L 50 47.1 cis-1,3-Dichloropropene ug/L 50 52.5 Dibromochloromethane ug/L 50 56.4 Dibromomethane ug/L 50 52.2 Ethylbenzene ug/L 50 53.0 lodomethane ug/L 100 92.7 Methylene Chloride ug/L 50 46.7 Styrene ug/L 50 53.7 Tetrachloroethene ug/L 50 56.4 Toluene ug/L 50 49.1 trans-1,2-Dichloroethene ug/L 50 48.8 trans- 1,3-Dichloropropene ug/L 50 50.9 trans-1,4-Dichloro-2-butene ug/L 50 43.5 Trichloroethene ug/L 50 51.0 Trichlorofluoromethane ug/L 50 33.9 Vinyl acetate ug/L 100 98.9 Vinyl chloride ug/L 50 40.9 Xylene (Total) ug/L 150 161 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % % Rec Limits Qualifiers 66 48-130 v3 94 70-130 105 70-130 113 70-130 104 70-130 106 70-130 93 40-130 93 67-132 107 70-130 113 69-130 98 70-130 98 70-130 102 70-130 87 35-1891K 102 70-130 68 63-130 v3 99 55-143 82 70-131 107 70-130 102 70-130 102 70-130 100 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2928456 MS 92483759023 Spike Parameter Units Result Conc. MSD Spike Conc. 2928457 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 23.2 21.7 116 109 73-134 7 30 1,1,1-Trichloroethane ug/L ND 20 20 21.1 19.9 106 100 82-143 6 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 22.8 21.1 114 106 70-136 8 30 1,1,2-Trichloroethane ug/L ND 20 20 20.6 19.0 103 95 70-135 8 30 1,1-Dichloroethane ug/L ND 20 20 21.3 20.0 106 100 70-139 6 30 1,1-Dichloroethene ug/L ND 20 20 23.0 20.5 115 103 70-154 11 30 1,2,3-Trichloropropane ug/L ND 20 20 22.4 21.9 112 109 71-137 2 30 1,2-Dibromo-3- ug/L ND 20 20 22.9 24.3 115 122 65-134 6 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 22.4 20.1 112 100 70-137 11 30 1,2-Dichlorobenzene ug/L ND 20 20 23.6 21.7 118 109 70-133 8 30 1,2-Dichloroethane ug/L ND 20 20 18.5 17.7 93 88 70-137 5 30 1,2-Dichloropropane ug/L ND 20 20 20.8 20.0 104 100 70-140 4 30 1,4-Dichlorobenzene ug/L ND 20 20 21.2 22.5 106 112 70-133 6 30 1,4-Dioxane (p-Dioxane) ug/L ND 400 400 431 378 108 94 53-168 13 30 2-Butanone (MEK) ug/L ND 40 40 41.3 37.9 103 95 60-139 9 30 2-Hexanone ug/L ND 40 40 44.6 44.8 111 112 65-138 0 30 4-Methyl-2-pentanone ug/L ND 40 40 40.1 36.2 100 90 65-135 10 30 (MIBK) Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 52 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2928456 2928457 MS MSD 92483759023 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Acetone ug/L ND 40 40 42.4 39.6 106 99 60-148 7 30 Acrylonitrile ug/L ND 100 100 100 94.0 100 94 64-147 6 30 Benzene ug/L ND 20 20 21.7 20.7 109 103 70-151 5 30 Bromochloromethane ug/L ND 20 20 21.9 20.3 109 101 70-141 8 30 Bromodichloromethane ug/L ND 20 20 17.5 17.0 87 85 70-138 3 30 Bromoform ug/L ND 20 20 20.9 19.2 105 96 63-130 8 30 Bromomethane ug/L ND 20 20 26.8 24.6 131 119 15-152 9 30 IH,v3 Carbon disulfide ug/L ND 20 20 20.3 19.1 102 96 69-149 6 30 Carbon tetrachloride ug/L ND 20 20 21.2 19.7 106 99 70-143 7 30 Chlorobenzene ug/L ND 20 20 21.8 21.0 109 105 70-138 4 30 Chloroethane ug/L ND 20 20 19.9 18.1 99 91 52-163 9 30 Chloroform ug/L ND 20 20 21.1 18.9 105 95 70-139 11 30 Chloromethane ug/L ND 20 20 14.4 13.5 72 68 41-139 6 30 v3 cis-1,2-Dichloroethene ug/L ND 20 20 20.5 19.8 103 99 70-141 4 30 cis-1,3-Dichloropropene ug/L ND 20 20 21.7 19.4 109 97 70-137 11 30 Dibromochloromethane ug/L ND 20 20 21.1 20.2 105 101 70-134 4 30 Dibromomethane ug/L ND 20 20 21.8 20.6 109 103 70-138 6 30 Ethylbenzene ug/L ND 20 20 22.3 21.4 111 107 66-153 4 30 lodomethane ug/L ND 40 40 36.7 35.0 92 88 20-138 5 30 v3 Methylene Chloride ug/L ND 20 20 19.8 18.7 99 93 42-159 6 30 Styrene ug/L ND 20 20 22.4 22.7 112 113 70-135 1 30 Tetrachloroethene ug/L ND 20 20 24.0 21.8 120 109 59-143 9 30 Toluene ug/L ND 20 20 20.4 18.2 102 91 59-148 11 30 trans-1,2-Dichloroethene ug/L ND 20 20 21.9 18.7 109 94 70-146 16 30 trans-1,3-Dichloropropene ug/L ND 20 20 20.1 18.1 100 90 70-135 10 30 trans-1,4-Dichloro-2-butene ug/L ND 20 20 11.7 13.1 58 65 47-135 11 30 IK,v3 Trichloroethene ug/L ND 20 20 21.5 19.6 107 98 70-147 9 30 Trichlorofluoromethane ug/L ND 20 20 18.6 16.8 93 84 70-148 10 30 Vinyl acetate ug/L ND 40 40 40.1 37.4 100 93 49-151 7 30 Vinyl chloride ug/L ND 20 20 17.6 16.9 88 85 70-156 4 30 Xylene (Total) ug/L ND 60 60 69.6 64.8 116 108 63-158 7 30 1,2-Dichloroethane-d4 (S) % 103 104 70-130 4-Bromofluorobenzene (S) % 98 99 70-130 Toluene-d8 (S) % 99 98 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: Surry Closed- Mt. Airy Pace Project No.: 92483829 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. ANALYTE QUALIFIERS B Analyte was detected in the associated method blank. IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be considered an estimated value. IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be considered an estimated value. IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be considered an estimated value. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias. v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: Surry Closed- Mt. Airy 92483829 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92483829001 MW-1 EPA 3010A 550337 EPA 6010D 550349 92483829002 MW-11 EPA 3010A 550337 EPA 6010D 550349 92483829003 MW-12S EPA 3010A 550337 EPA 6010D 550349 92483829004 MW-13 EPA 3010A 550337 EPA 6010D 550349 92483829005 MW-14 EPA 3010A 550337 EPA 6010D 550349 92483829006 MW-15 EPA 3010A 550337 EPA 6010D 550349 92483829007 MW-16 EPA 3010A 550337 EPA 6010D 550349 92483829008 MW-17 EPA 3010A 550338 EPA 6010D 550348 92483829009 MW-19 EPA 3010A 550338 EPA 6010D 550348 92483829010 MW-21 EPA 3010A 550338 EPA 6010D 550348 92483829011 MW-22 EPA 3010A 550338 EPA 6010D 550348 92483829012 MW-23 EPA 3010A 550338 EPA 6010D 550348 92483829001 MW-1 EPA 3010A 550340 EPA 6020B 550353 92483829002 MW-11 EPA 3010A 550340 EPA 6020B 550353 92483829003 MW-12S EPA 3010A 550340 EPA 6020B 550353 92483829004 MW-13 EPA 3010A 550340 EPA 6020B 550353 92483829005 MW-14 EPA 3010A 550340 EPA 6020B 550353 92483829006 MW-15 EPA 3010A 550341 EPA 6020B 550352 92483829007 MW-16 EPA 3010A 550341 EPA 6020B 550352 92483829008 MW-17 EPA 3010A 550341 EPA 6020B 550352 92483829009 MW-19 EPA 3010A 550341 EPA 6020B 550352 92483829010 MW-21 EPA 3010A 550341 EPA 6020B 550352 92483829011 MW-22 EPA 3010A 550341 EPA 6020B 550352 92483829012 MW-23 EPA 3010A 550341 EPA 6020B 550352 92483829001 MW-1 EPA 8260D 550875 92483829002 MW-11 EPA 8260D 550877 92483829003 MW-12S EPA 8260D 550875 92483829004 MW-13 EPA 8260D 550889 92483829005 MW-14 EPA 8260D 550877 92483829006 MW-15 EPA 8260D 550889 92483829007 MW-16 EPA 8260D 550889 92483829008 MW-17 EPA 8260D 550877 92483829009 MW-19 EPA 8260D 550875 92483829010 MW-21 EPA 8260D 550889 92483829011 MW-22 EPA 8260D 550889 92483829012 MW-23 EPA 8260D 550875 Date: 07/02/2020 04:47 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 49 of 52 Cocument Name: Document Revised: February 7, 2018 Sample Condition Upon Receipt(SCUR) Page 1 of 2 c1C8AMIACdl Document No.: Issuing Authority: F-CAR-CS-033-Rev-06 Pace Carolinas Quality Office 1 Laboratory receiving SarepieS: Asheville ❑ Eden[] Greenwood ❑ Htantersville RaEeigh❑ Methanitsviite❑ Sarnple Conditiorl Client Natne: Wo## : 92483829 Courier: ❑Face CUPS OUSPS ❑Client IN INI1III �II ❑ Commercial ❑ 92463529 Custody SealPresent7 Des 'I Seals Intact? []Yes 50 Datellnitiais Person Examining Cantents2-q T..� �.I L Packing Material: ❑Bubble Wrap ubble Bags ❑Non ❑ Other BlolagicaI Tissue Fr sen? ❑Yes []No I/A Thermometer: }ZT061 Type of Ice: ��-'t ❑REue ❑None ❑SR Gun ID: _ Cooler Temp ('Cl: 3'17 Correction Factor: Add/Subtract ('C) +0.1 Temp should be abovefreezingto VC Cooler Temp Corrected ("C): []Samples out of temp criteria. SampleS an Ice, cooling process has begun USDA Regulated Soil l /A, water sample Did samples originate in a quarantine ?one within the United States: CA, NY, or SC (check maps)? old samples originate from a foreign source {internationally, 1­7.. ram., lncludingslawali and Puerto Rico)? Oyes ONO Chain of Custody Present? Samples Arrived within Hold Time? Short Hold Time Analysis j<72 hr.)? Rush Turn Ara und Time Requested? Sufficient Volume? Correct Containers Used? -Pace Containers Used? Containers Intact? Dissolved analysis: Samples Field Filtered? Heads ace in VOA Vials (:&6mm) Trip Blank Present? Trio Blank Custody Seals Present? COMMENTS/5AMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Yes ❑No ❑N/A []Yes ❑No I. 2, 3, 4. 5. 7, 8. Datefrime: Lot ID of soft contalners: Date: late: Field Data Required7 []Yes []No Page 50 of 52 Document Name: Document Revised: February 7, 2018 aceAndlyflcal Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR•CS•033-Rev.06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Conform, TOC, Oil and Grease, ORO/8015 (water) OOC, LLHg **Bottom half of box is to list number of bottle Project It WQ# a 92483829 PM: PMB Due Date: 07/13/20 CLIENT: 92-Municipal z ? a A U � z _ z ¢ ro Z c3 Cl Cl v 91 2 Z N ¢ N a io a f° Z v v Z ai N v a v v z ? Y m z z c0 n a a a O M p V ¢ S O A c7 a a C _ 4. c V O Q N a E Z '^ 0 Q Z Z c M 0 = a « '��' ry = `Q c } c n A c. a a 5 E ¢ a E C 4 E E ¢ o N a Oy z a O > 7 a > 2 a D JR a`, Q. Y M m Y L m n E c a E E n N ry E o o N E 0 0 ul v t — E a E E ry 5 a c`, — E u) v - E o M 0 E 0 et a E u of E ct f9 w - '' E E E o E n E C E a Q a M a N a .r a V a M a P4 a a ri l7 i ,i to M to N m 0 cFi M r7 Q M 0 2 m r7 H QI v7 7 dl t7 4 T %2 ¢ C3 . � � aa N M O 0 L7 Vi M 0 m m m m m m m cc 3¢ a a a a a❑>' 0 7 v m a 7 a i 3 4 5 6 � -7 � l I 8 y 10 1 , NN' 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot it Note: Whenever there Is a discrepancy affecting North Carolina corn pAance samples, a copy of this form WilI be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, Incorrect preservative, out of temp, Incorrect containers. Page 51 of 52 X v rn a g n M y N j C f0 fb V 4Y Cn A W N ITEM# m � o 3 j m_ 3 m v. 7 a �3 o n a � N n n f5 > w r.Ni N in m in a w to p m 3� m » O 3 n n n N F n n n N F � n w 7 � o c Q s 'n n aEn _m ° ❑ ° N m a x z N c _2 -tO b�D a+�gFq� m V- O m s L ry L h�g90r4 go `m—° e3i D O c' o # w m o o a m 3 O v MATRIX CODE (sea valid modes to loft) m D � SAMPLETYPE (G=GRAB C=COMP} -- N w o x Z v d ) co rn � a rn D �{ A z n c Z Z D m m m 3 nn m m O o a D Z n a o nn N T v v z m m m > SAMPLE TEMP AT COLLECTION rnN OF CONTAINERS y - -Dn C) p c n y n el n d n a N 3 m ] o n F Unpreserved _ m v v s� y>> H2SO4 �_ m m n (1 o 71 3 HNO3 EnN o HCI o � NaOH nr Na2S2D3 N m � Methanol m m Q Co Other ?' � m x x x x x x x x x x x x VQCsAPP I 3 v x x x x x x x x X x X x Metals App I n S Me z x x x x x x X x x x X x Turbidity � Me r, 3 n 4 VOCs App II Metals APP 11 � C N \ o m w _3 r � m p N TEMP in C (_. n Residual Chlorine (YIN) 0 o Received on Ice ro N n ' {YIN) F-n o Q C)o c)D C� a �,y c , y Sealed Cooler Dew C)Q1 OA o' Cd V (Q_' Samples Intact (YJN) Page 52 of 52 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 July 10, 2020 Mr. Jonathan Pfohl Municipal Engineering Services 68 Shipwash Dr. Garner, NC 27529 RE: Project: Surry Closed Mt. Airy Pace Project No.: 92483783 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on June 26, 2020. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace National - Mt. Juliet • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Steven R. Gandy, Municipal Engineering Services Co. REPORT OF LABORATORY ANALYSIS r e This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 54 laneAnalytical www,pacelabs.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Surry Closed Mt. Airy Pace Project No.: 92483783 Pace Analytical Services National 12065 Lebanon Road, Mt. Juliet, TN 37122 Alabama Certification #: 40660 Alaska Certification 17-026 Arizona Certification #: AZ0612 Arkansas Certification #: 88-0469 California Certification #: 2932 Canada Certification #: 1461.01 Colorado Certification #: TN00003 Connecticut Certification #: PH-0197 DOD Certification: #1461.01 EPA# TN00003 Florida Certification #: E87487 Georgia DW Certification #: 923 Georgia Certification: NELAP Idaho Certification #: TN00003 Illinois Certification #: 200008 Indiana Certification #: C-TN-01 Iowa Certification #: 364 Kansas Certification #: E-10277 Kentucky UST Certification #: 16 Kentucky Certification #: 90010 Louisiana Certification #: A130792 Louisiana DW Certification #: LA180010 Maine Certification #: TN0002 Maryland Certification #: 324 Massachusetts Certification #: M-TNO03 Michigan Certification #: 9958 Minnesota Certification #: 047-999-395 Mississippi Certification #: TN00003 Missouri Certification #: 340 Montana Certification M CERT0086 Nebraska Certification #: NE-OS-15-05 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Nevada Certification #: TN-03-2002-34 New Hampshire Certification #: 2975 New Jersey Certification #: TNO02 New Mexico DW Certification New York Certification #: 11742 North Carolina Aquatic Toxicity Certification #: 41 North Carolina Drinking Water Certification #: 21704 North Carolina Environmental Certificate #: 375 North Dakota Certification #: R-140 Ohio VAP Certification #: CL0069 Oklahoma Certification #: 9915 Oregon Certification #: TN200002 Pennsylvania Certification #: 68-02979 Rhode Island Certification #: LA000356 South Carolina Certification #: 84004 South Dakota Certification Tennessee DW/Chem/Micro Certification #: 2006 Texas Certification #: T 104704245-17-14 Texas Mold Certification #: LAB0152 USDA Soil Permit #: P330-15-00234 Utah Certification #: TN00003 Vermont Dept. of Health: ID# VT-2006 Virginia Certification #: VT2006 Virginia Certification #: 460132 Washington Certification #: C847 West Virginia Certification #: 233 Wisconsin Certification #: 9980939910 Wyoming UST Certification #: via A21-A 2926.01 A21-A-ISO 17025 Certification #: 1461.01 A21-A-ISO 17025 Certification #: 1461.02 AIHA-LAP/LLC EMLAP Certification #:100789 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: Surry Closed Mt. Airy Pace Project No.: 92483783 Lab ID Sample ID Matrix Date Collected Date Received 92483783001 MW-20 Water 06/25/20 13:15 06/26/20 08:30 92483783002 MW-3R Water 06/25/20 11:45 06/26/20 08:30 92483783003 MW-6 Water 06/25/20 13:40 06/26/20 08:30 92483783004 MW-7 Water 06/25/20 13:42 06/26/20 08:30 92483783005 MW-9 Water 06/25/20 13:18 06/26/20 08:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Surry Closed Mt. Airy Pace Project No.: 92483783 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92483783001 MW-20 EPA 8151 MTJ 11 PAN EPA 8081 B SEM 21 PASI-C EPA 8082A SEM 8 PASI-C EPA 601 OD KQ 15 PASI-A EPA 6020E JOR 1 PASI-A EPA 7470A SOO 1 PASI-A EPA 8270E PKS 111 PASI-C EPA 8260D SAS 65 PASI-C SM 4500-S2D-2011 LMS1 1 PASI-A SM 4500-CN-E-2011 CJL 1 PASI-A 92483783002 MW-3R EPA 601 OD KQ 14 PASI-A EPA 6020E JOR 1 PASI-A EPA 8260D CL 51 PASI-C 92483783003 MW-6 EPA 601 OD KQ 14 PASI-A EPA 6020E JOR 1 PASI-A EPA 8260D CL 51 PASI-C 92483783004 MW-7 EPA 601 OD KQ 14 PASI-A EPA 6020E JOR 1 PASI-A EPA 8260D CL 51 PASI-C 92483783005 MW-9 EPA 601 OD KQ 14 PASI-A EPA 6020E JOR 1 PASI-A EPA 8260D SAS 51 PASI-C PAN = Pace National - Mt. Juliet PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed Mt. Airy Pace Project No.: 92483783 Sample: MW-20 Lab ID: 92483783001 Collected: 06/25/20 13:15 Received: 06/26/20 08:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Chlorinated Herb. (GC) 8151 2,4-D Dalapon 2,4-DB Dicamba Dichloroprop Dinoseb MCPA MCPP 2,4,5-T 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 8081 OC Pesticides RVE Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) 4,4'-DDD 4,4'-DDE 4,4'-DDT Dieldrin Endosulfan I Endosulfan 11 Endosulfan sulfate Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 8082 GCS PCB RVE PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) Date: 07/10/2020 04:54 PM Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet ND ug/L 2.00 0.547 1 06/29/20 18:12 07/03/20 03:31 94-75-7 ND ug/L 2.00 0.344 1 06/29/20 18:12 07/03/20 03:31 127-20-8 ND ug/L 2.00 0.302 1 06/29/20 18:12 07/03/20 03:31 94-82-6 ND ug/L 2.00 0.245 1 06/29/20 18:12 07/03/20 03:31 1918-00-9 ND ug/L 2.00 1.04 1 06/29/20 18:12 07/03/20 03:31 15165-67-0 ND ug/L 2.00 0.250 1 06/29/20 18:12 07/03/20 03:31 88-85-7 ND ug/L 100 13.1 1 06/29/20 18:12 07/03/20 03:31 94-74-6 ND ug/L 100 66.0 1 06/29/20 18:12 07/03/20 03:31 7085-19-0 ND ug/L 2.00 0.258 1 06/29/20 18:12 07/03/20 03:31 93-76-5 ND ug/L 2.00 0.335 1 06/29/20 18:12 07/03/20 03:31 93-72-1 60.1 % 14.0-158 1 06/29/20 18:12 07/03/20 03:31 19719-28-9 Analytical Method: EPA 8081 B Preparation Method: EPA 351 OC Pace Analytical Services - Charlotte ND ug/L 0.050 0.022 1 07/01/20 11:13 07/06/20 14:29 309-00-2 ND ug/L 0.050 0.019 1 07/01/20 11:13 07/06/20 14:29 319-84-6 ND ug/L 0.050 0.014 1 07/01/20 11:13 07/06/20 14:29 319-85-7 ND ug/L 0.050 0.020 1 07/01/20 11:13 07/06/20 14:29 319-86-8 ND ug/L 0.050 0.012 1 07/01/20 11:13 07/06/20 14:29 58-89-9 ND ug/L 0.20 0.14 1 07/01/20 11:13 07/06/20 14:29 57-74-9 ND ug/L 0.050 0.0069 1 07/01/20 11:13 07/06/20 14:29 72-54-8 ND ug/L 0.050 0.0064 1 07/01/20 11:13 07/06/20 14:29 72-55-9 ND ug/L 0.050 0.018 1 07/01/20 11:13 07/06/20 14:29 50-29-3 ND ug/L 0.050 0.0073 1 07/01/20 11:13 07/06/20 14:29 60-57-1 ND ug/L 0.050 0.0094 1 07/01/20 11:13 07/06/20 14:29 959-98-8 ND ug/L 0.050 0.0065 1 07/01/20 11:13 07/06/20 14:29 33213-65-9 ND ug/L 0.050 0.0091 1 07/01/20 11:13 07/06/20 14:29 1031-07-8 ND ug/L 0.050 0.0089 1 07/01/20 11:13 07/06/20 14:29 72-20-8 ND ug/L 0.050 0.013 1 07/01/20 11:13 07/06/20 14:29 7421-93-4 ND ug/L 0.050 0.016 1 07/01/20 11:13 07/06/20 14:29 76-44-8 ND ug/L 0.050 0.0097 1 07/01/20 11:13 07/06/20 14:29 1024-57-3 ND ug/L 0.15 0.033 1 07/01/20 11:13 07/06/20 14:29 72-43-5 ND ug/L 0.20 0.19 1 07/01/20 11:13 07/06/20 14:29 8001-35-2 84 % 10-130 1 07/01/20 11:13 07/06/20 14:29 877-09-8 70 % 10-130 1 07/01/20 11:13 07/06/20 14:29 2051-24-3 Analytical Method: EPA 8082A Preparation Method: EPA 351 OC Pace Analytical Services - Charlotte ND ug/L 0.50 0.22 1 07/01/20 11:13 07/02/20 22:35 12674-11-2 ND ug/L 0.50 0.32 1 07/01/20 11:13 07/02/20 22:35 11104-28-2 ND ug/L 0.50 0.21 1 07/01/20 11:13 07/02/20 22:35 11141-16-5 ND ug/L 0.50 0.44 1 07/01/20 11:13 07/02/20 22:35 53469-21-9 ND ug/L 0.50 0.34 1 07/01/20 11:13 07/02/20 22:35 12672-29-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. R1 LO Page 5 of 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed Mt. Airy Pace Project No.: 92483783 Sample: MW-20 Lab ID: 92483783001 Collected: 06/25/20 13:15 Received: 06/26/20 08:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Pace Analytical Services - Charlotte PCB-1254 (Aroclor 1254) ND ug/L 0.50 0.24 1 07/01/20 11:13 07/02/20 22:35 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.50 0.30 1 07/01/20 11:13 07/02/20 22:35 11096-82-5 Surrogates Decachlorobiphenyl (S) 77 % 10-130 1 07/01/20 11:13 07/02/20 22:35 2051-24-3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 06/27/20 00:47 06/30/20 03:54 7440-36-0 Arsenic 5.8J ug/L 10.0 4.7 1 06/27/20 00:47 06/30/20 03:54 7440-38-2 BC Barium 50.8 ug/L 5.0 3.5 1 06/27/20 00:47 06/30/20 03:54 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 06/27/20 00:47 06/30/20 03:54 7440-41-7 Cadmium 0.42J ug/L 1.0 0.40 1 06/27/20 00:47 06/30/20 03:54 7440-43-9 Chromium ND ug/L 5.0 3.7 1 06/27/20 00:47 06/30/20 03:54 7440-47-3 Cobalt 122 ug/L 5.0 3.6 1 06/27/20 00:47 06/30/20 03:54 7440-48-4 Copper ND ug/L 5.0 4.3 1 06/27/20 00:47 06/30/20 03:54 7440-50-8 Lead ND ug/L 5.0 4.5 1 06/27/20 00:47 06/30/20 03:54 7439-92-1 Nickel 6.9 ug/L 5.0 3.5 1 06/27/20 00:47 06/30/20 03:54 7440-02-0 Selenium ND ug/L 10.0 4.7 1 06/27/20 00:47 06/30/20 03:54 7782-49-2 Silver ND ug/L 5.0 2.5 1 06/27/20 00:47 06/30/20 03:54 7440-22-4 Tin ND ug/L 5.0 4.7 1 06/27/20 00:47 06/30/20 03:54 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 06/27/20 00:47 06/30/20 03:54 7440-62-2 Zinc 16.0 ug/L 10.0 9.5 1 06/27/20 00:47 06/30/20 03:54 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium 0.72 ug/L 0.10 0.050 1 06/27/20 00:13 06/29/20 04:10 7440-28-0 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 06/28/20 23:35 06/29/20 16:09 7439-97-6 8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Acenaphthene ND ug/L 10.0 1.4 1 07/01/20 11:28 07/10/20 03:21 83-32-9 Acenaphthylene ND ug/L 10.0 1.5 1 07/01/20 11:28 07/10/20 03:21 208-96-8 Acetophenone ND ug/L 10.0 1.3 1 07/01/20 11:28 07/10/20 03:21 98-86-2 2-Acetylaminofluorene ND ug/L 10.0 1.9 1 07/01/20 11:28 07/10/20 03:21 53-96-3 4-Aminobiphenyl ND ug/L 10.0 4.2 1 07/01/20 11:28 07/10/20 03:21 92-67-1 Anthracene ND ug/L 10.0 1.6 1 07/01/20 11:28 07/10/20 03:21 120-12-7 Benzo(a)anthracene ND ug/L 10.0 1.5 1 07/01/20 11:28 07/10/20 03:21 56-55-3 Benzo(a)pyrene ND ug/L 10.0 1.8 1 07/01/20 11:28 07/10/20 03:21 50-32-8 Benzo(b)fluoranthene ND ug/L 10.0 1.7 1 07/01/20 11:28 07/10/20 03:21 205-99-2 Benzo(g,h,i)perylene ND ug/L 10.0 1.6 1 07/01/20 11:28 07/10/20 03:21 191-24-2 Benzo(k)fluoranthene ND ug/L 10.0 1.5 1 07/01/20 11:28 07/10/20 03:21 207-08-9 Benzyl alcohol ND ug/L 20.0 2.6 1 07/01/20 11:28 07/10/20 03:21 100-51-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed Mt. Airy Pace Project No.: 92483783 Sample: MW-20 Lab ID: 92483783001 Collected: 06/25/20 13:15 Received: 06/26/20 08:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 4-Bromophenylphenyl ether ND ug/L 10.0 1.2 1 07/01/20 11:28 07/10/20 03:21 101-55-3 Butylbenzylphthalate ND ug/L 10.0 1.9 1 07/01/20 11:28 07/10/20 03:21 85-68-7 4-ChIoro-3-methyl phenol ND ug/L 10.0 2.8 1 07/01/20 11:28 07/10/20 03:21 59-50-7 4-Chloroaniline ND ug/L 20.0 2.8 1 07/01/20 11:28 07/10/20 03:21 106-47-8 Chlorobenzilate ND ug/L 10.0 3.6 1 07/01/20 11:28 07/10/20 03:21 510-15-6 L1,M0 bis(2-Chloroethoxy)methane ND ug/L 10.0 1.3 1 07/01/20 11:28 07/10/20 03:21 111-91-1 bis(2-Chloroethyl) ether ND ug/L 10.0 1.7 1 07/01/20 11:28 07/10/20 03:21 111-44-4 2-Chloronaphthalene ND ug/L 10.0 1.4 1 07/01/20 11:28 07/10/20 03:21 91-58-7 2-Chlorophenol ND ug/L 10.0 1.4 1 07/01/20 11:28 07/10/20 03:21 95-57-8 4-Chlorophenylphenyl ether ND ug/L 10.0 1.5 1 07/01/20 11:28 07/10/20 03:21 7005-72-3 Chrysene ND ug/L 10.0 1.4 1 07/01/20 11:28 07/10/20 03:21 218-01-9 Diallate ND ug/L 10.0 2.7 1 07/01/20 11:28 07/10/20 03:21 2303-16-4 Dibenz(a,h)anthracene ND ug/L 10.0 1.6 1 07/01/20 11:28 07/10/20 03:21 53-70-3 Dibenzofuran ND ug/L 10.0 1.3 1 07/01/20 11:28 07/10/20 03:21 132-64-9 3,3'-Dichlorobenzidine ND ug/L 20.0 2.7 1 07/01/20 11:28 07/10/20 03:21 91-94-1 2,4-Dichlorophenol ND ug/L 10.0 1.5 1 07/01/20 11:28 07/10/20 03:21 120-83-2 2,6-Dichlorophenol ND ug/L 10.0 2.7 1 07/01/20 11:28 07/10/20 03:21 87-65-0 Diethylphthalate ND ug/L 10.0 1.6 1 07/01/20 11:28 07/10/20 03:21 84-66-2 Dimethoate ND ug/L 10.0 2.0 1 07/01/20 11:28 07/10/20 03:21 60-51-5 P-Dimethylaminoazobenzene ND ug/L 5.0 3.3 1 07/01/20 11:28 07/10/20 03:21 60-11-7 7,12-Dimethylbenz(a)anthracene ND ug/L 10.0 2.8 1 07/01/20 11:28 07/10/20 03:21 57-97-6 3,3'-Dimethylbenzidine ND ug/L 25.0 23.5 1 07/01/20 11:28 07/10/20 03:21 119-93-7 IH 2,4-Dimethylphenol ND ug/L 10.0 1.5 1 07/01/20 11:28 07/10/20 03:21 105-67-9 Dimethylphthalate ND ug/L 10.0 1.4 1 07/01/20 11:28 07/10/20 03:21 131-11-3 Di-n-butylphthalate ND ug/L 10.0 1.6 1 07/01/20 11:28 07/10/20 03:21 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 20.0 4.5 1 07/01/20 11:28 07/10/20 03:21 534-52-1 1,3-Dinitrobenzene ND ug/L 10.0 3.7 1 07/01/20 11:28 07/10/20 03:21 99-65-0 2,4-Dinitrophenol ND ug/L 50.0 7.3 1 07/01/20 11:28 07/10/20 03:21 51-28-5 2,4-Dinitrotoluene ND ug/L 10.0 1.7 1 07/01/20 11:28 07/10/20 03:21 121-14-2 2,6-Dinitrotoluene ND ug/L 10.0 1.7 1 07/01/20 11:28 07/10/20 03:21 606-20-2 Di-n-octylphthalate ND ug/L 10.0 2.2 1 07/01/20 11:28 07/10/20 03:21 117-84-0 Diphenylamine ND ug/L 10.0 1.4 1 07/01/20 11:28 07/10/20 03:21 122-39-4 Disulfoton ND ug/L 10.0 6.0 1 07/01/20 11:28 07/10/20 03:21 298-04-4 bis(2- Ethyl hexyl)phthalate ND ug/L 6.0 2.0 1 07/01/20 11:28 07/10/20 03:21 117-81-7 Ethyl methanesulfonate ND ug/L 20.0 2.8 1 07/01/20 11:28 07/10/20 03:21 62-50-0 Famphur ND ug/L 10.0 5.7 1 07/01/20 11:28 07/10/20 03:21 52-85-7 Fluoranthene ND ug/L 10.0 1.6 1 07/01/20 11:28 07/10/20 03:21 206-44-0 Fluorene ND ug/L 10.0 1.4 1 07/01/20 11:28 07/10/20 03:21 86-73-7 Hexachlorobenzene ND ug/L 10.0 1.3 1 07/01/20 11:28 07/10/20 03:21 118-74-1 Hexachlorocyclopentadiene ND ug/L 10.0 2.4 1 07/01/20 11:28 07/10/20 03:21 77-47-4 Hexachloroethane ND ug/L 10.0 1.3 1 07/01/20 11:28 07/10/20 03:21 67-72-1 Hexachloropropene ND ug/L 10.0 5.5 1 07/01/20 11:28 07/10/20 03:21 1888-71-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 1.7 1 07/01/20 11:28 07/10/20 03:21 193-39-5 Isodrin ND ug/L 10.0 3.0 1 07/01/20 11:28 07/10/20 03:21 465-73-6 Isophorone ND ug/L 10.0 1.3 1 07/01/20 11:28 07/10/20 03:21 78-59-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed Mt. Airy Pace Project No.: 92483783 Sample: MW-20 Lab ID: 92483783001 Collected: 06/25/20 13:15 Received: 06/26/20 08:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Isosafrole ND ug/L 10.0 3.6 1 07/01/20 11:28 07/10/20 03:21 120-58-1 Kepone ND ug/L 10.0 8.2 1 07/01/20 11:28 07/10/20 03:21 143-50-0 Methapyrilene ND ug/L 50.0 27.2 1 07/01/20 11:28 07/10/20 03:21 91-80-5 3-Methylcholanthrene ND ug/L 10.0 5.3 1 07/01/20 11:28 07/10/20 03:21 56-49-5 Methyl methanesulfonate ND ug/L 5.0 3.0 1 07/01/20 11:28 07/10/20 03:21 66-27-3 2-Methylnaphthalene ND ug/L 10.0 1.4 1 07/01/20 11:28 07/10/20 03:21 91-57-6 Methyl parathion ND ug/L 10.0 2.0 1 07/01/20 11:28 07/10/20 03:21 298-00-0 2-Methylphenol(o-Cresol) ND ug/L 10.0 1.2 1 07/01/20 11:28 07/10/20 03:21 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/L 10.0 1.2 1 07/01/20 11:28 07/10/20 03:21 15831-10-4 1-Naphthalenamine ND ug/L 5.0 4.6 1 07/01/20 11:28 07/10/20 03:21 134-32-7 2-Naphthalenamine ND ug/L 10.0 6.1 1 07/01/20 11:28 07/10/20 03:21 91-59-8 1,4-Naphthoquinone ND ug/L 5.0 2.4 1 07/01/20 11:28 07/10/20 03:21 130-15-4 2-Nitroaniline ND ug/L 20.0 3.0 1 07/01/20 11:28 07/10/20 03:21 88-74-4 3-Nitroaniline ND ug/L 20.0 2.8 1 07/01/20 11:28 07/10/20 03:21 99-09-2 4-Nitroaniline ND ug/L 20.0 3.1 1 07/01/20 11:28 07/10/20 03:21 100-01-6 Nitrobenzene ND ug/L 10.0 1.5 1 07/01/20 11:28 07/10/20 03:21 98-95-3 2-Nitrophenol ND ug/L 10.0 1.7 1 07/01/20 11:28 07/10/20 03:21 88-75-5 4-Nitrophenol ND ug/L 50.0 9.4 1 07/01/20 11:28 07/10/20 03:21 100-02-7 5-Nitro-o-toluidine ND ug/L 10.0 2.4 1 07/01/20 11:28 07/10/20 03:21 99-55-8 N-Nitrosodiethylamine ND ug/L 10.0 2.0 1 07/01/20 11:28 07/10/20 03:21 55-18-5 N-Nitrosodimethylamine ND ug/L 10.0 1.8 1 07/01/20 11:28 07/10/20 03:21 62-75-9 N-Nitroso-di-n-butylamine ND ug/L 10.0 6.2 1 07/01/20 11:28 07/10/20 03:21 924-16-3 N-Nitroso-di-n-propylamine ND ug/L 10.0 1.3 1 07/01/20 11:28 07/10/20 03:21 621-64-7 N-Nitrosodiphenylamine ND ug/L 10.0 1.4 1 07/01/20 11:28 07/10/20 03:21 86-30-6 N-Nitrosomethylethylamine ND ug/L 10.0 3.3 1 07/01/20 11:28 07/10/20 03:21 10595-95-6 N-Nitrosopiperidine ND ug/L 10.0 2.6 1 07/01/20 11:28 07/10/20 03:21 100-75-4 N-Nitrosopyrrolidine ND ug/L 10.0 2.1 1 07/01/20 11:28 07/10/20 03:21 930-55-2 O,O,O-Triethylphosphorothioate ND ug/L 10.0 3.5 1 07/01/20 11:28 07/10/20 03:21 126-68-1 2,2'-Oxybis(1-chloropropane) ND ug/L 10.0 1.3 1 07/01/20 11:28 07/10/20 03:21 108-60-1 Parathion (Ethyl parathion) ND ug/L 10.0 2.0 1 07/01/20 11:28 07/10/20 03:21 56-38-2 Pentachlorobenzene ND ug/L 10.0 4.4 1 07/01/20 11:28 07/10/20 03:21 608-93-5 Pentachloronitrobenzene ND ug/L 10.0 2.4 1 07/01/20 11:28 07/10/20 03:21 82-68-8 Pentachlorophenol ND ug/L 20.0 2.8 1 07/01/20 11:28 07/10/20 03:21 87-86-5 Phenacetin ND ug/L 10.0 1.9 1 07/01/20 11:28 07/10/20 03:21 62-44-2 Phenanthrene ND ug/L 10.0 1.4 1 07/01/20 11:28 07/10/20 03:21 85-01-8 Phenol ND ug/L 10.0 1.5 1 07/01/20 11:28 07/10/20 03:21 108-95-2 p-Phenylenediamine ND ug/L 10.0 4.2 1 07/01/20 11:28 07/10/20 03:21 106-50-3 Phorate ND ug/L 10.0 3.8 1 07/01/20 11:28 07/10/20 03:21 298-02-2 Pronamide ND ug/L 10.0 2.4 1 07/01/20 11:28 07/10/20 03:21 23950-58-5 Pyrene ND ug/L 10.0 1.5 1 07/01/20 11:28 07/10/20 03:21 129-00-0 Safrole ND ug/L 10.0 3.2 1 07/01/20 11:28 07/10/20 03:21 94-59-7 1,2,4,5-Tetrachlorobenzene ND ug/L 10.0 4.6 1 07/01/20 11:28 07/10/20 03:21 95-94-3 2,3,4,6-Tetrachlorophenol ND ug/L 10.0 1.6 1 07/01/20 11:28 07/10/20 03:21 58-90-2 Thionazin ND ug/L 10.0 1.8 1 07/01/20 11:28 07/10/20 03:21 297-97-2 O-Toluidine ND ug/L 10.0 2.8 1 07/01/20 11:28 07/10/20 03:21 95-53-4 REPORT OF LABORATORY ANALYSIS IH IL L2,M0 This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed Mt. Airy Pace Project No.: 92483783 Sample: MW-20 Lab ID: 92483783001 Collected: 06/25/20 13:15 Received: 06/26/20 08:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E APP9 RV Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte 2,4,5-Trichlorophenol ND ug/L 10.0 1.5 1 07/01/20 11:28 07/10/20 03:21 95-95-4 2,4,6-Trichlorophenol ND ug/L 10.0 1.4 1 07/01/20 11:28 07/10/20 03:21 88-06-2 1,3,5-Trinitrobenzene ND ug/L 10.0 5.3 1 07/01/20 11:28 07/10/20 03:21 99-35-4 Surrogates Nitrobenzene-d5 (S) 73 % 13-130 1 07/01/20 11:28 07/10/20 03:21 4165-60-0 2-Fluorobiphenyl (S) 70 % 13-130 1 07/01/20 11:28 07/10/20 03:21 321-60-8 Terphenyl-d14 (S) 109 % 25-130 1 07/01/20 11:28 07/10/20 03:21 1718-51-0 Phenol-d6 (S) 39 % 10-130 1 07/01/20 11:28 07/10/20 03:21 13127-88-3 2-Fluorophenol (S) 50 % 10-130 1 07/01/20 11:28 07/10/20 03:21 367-12-4 2,4,6-Tribromophenol (S) 89 % 10-137 1 07/01/20 11:28 07/10/20 03:21 118-79-6 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 07/02/20 05:11 67-64-1 Acetonitrile ND ug/L 50.0 30.4 1 07/02/20 05:11 75-05-8 Acrolein ND ug/L 10.0 2.7 1 07/02/20 05:11 107-02-8 v2 Acrylonitrile ND ug/L 10.0 0.90 1 07/02/20 05:11 107-13-1 Allyl chloride ND ug/L 2.0 0.28 1 07/02/20 05:11 107-05-1 Benzene 1.1 ug/L 1.0 0.15 1 07/02/20 05:11 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 07/02/20 05:11 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 07/02/20 05:11 75-27-4 Bromoform ND ug/L 1.0 0.62 1 07/02/20 05:11 75-25-2 Bromomethane ND ug/L 2.0 0.62 1 07/02/20 05:11 74-83-9 IH,v2 2-Butanone (MEK) ND ug/L 5.0 3.3 1 07/02/20 05:11 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 07/02/20 05:11 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 07/02/20 05:11 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 07/02/20 05:11 108-90-7 Chloroethane 0.901 ug/L 1.0 0.49 1 07/02/20 05:11 75-00-3 v2 Chloroform ND ug/L 5.0 2.3 1 07/02/20 05:11 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 07/02/20 05:11 74-87-3 v2 Chloroprene ND ug/L 5.0 1.7 1 07/02/20 05:11 126-99-8 Dibromochloromethane ND ug/L 1.0 0.41 1 07/02/20 05:11 124-48-1 Dibromomethane ND ug/L 1.0 0.46 1 07/02/20 05:11 74-95-3 1,2-Dichlorobenzene 1.2 ug/L 1.0 0.29 1 07/02/20 05:11 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 07/02/20 05:11 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 07/02/20 05:11 110-57-6 IK Dichlorodifluoromethane ND ug/L 1.0 0.23 1 07/02/20 05:11 75-71-8 1,1-Dichloroethane 0.85J ug/L 1.0 0.27 1 07/02/20 05:11 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.34 1 07/02/20 05:11 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 07/02/20 05:11 75-35-4 cis-1,2-Dichloroethene 6.9 ug/L 1.0 0.29 1 07/02/20 05:11 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.25 1 07/02/20 05:11 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.19 1 07/02/20 05:11 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.16 1 07/02/20 05:11 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.27 1 07/02/20 05:11 594-20-7 Date: 07/10/2020 04:54 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed Mt. Airy Pace Project No.: 92483783 Sample: MW-20 Lab ID: 92483783001 Collected: 06/25/20 13:15 Received: 06/26/20 08:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene Ethyl methacrylate Hexachloro-1,3-butadiene 2-Hexanone lodomethane Isobutanol Methacrylonitrile Methylene Chloride Methyl methacrylate 4-Methyl-2-pentanone (MIBK) Naphthalene Propionitrile Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 4500S2D Sulfide Water Sulfide 4500CNE Cyanide, Total Cyanide Date: 07/10/2020 04:54 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.21 1 07/02/20 05:11 563-58-6 ND ug/L 1.0 0.30 1 07/02/20 05:11 10061-01-5 ND ug/L 1.0 0.31 1 07/02/20 05:11 10061-02-6 ND ug/L 1.0 0.26 1 07/02/20 05:11 100-41-4 ND ug/L 1.0 0.51 1 07/02/20 05:11 97-63-2 ND ug/L 1.0 0.44 1 07/02/20 05:11 87-68-3 ND ug/L 5.0 0.57 1 07/02/20 05:11 591-78-6 ND ug/L 20.0 12.5 1 07/02/20 05:11 74-88-4 ND ug/L 100 66.4 1 07/02/20 05:11 78-83-1 ND ug/L 10.0 1.9 1 07/02/20 05:11 126-98-7 ND ug/L 5.0 3.7 1 07/02/20 05:11 75-09-2 ND ug/L 2.0 0.46 1 07/02/20 05:11 80-62-6 ND ug/L 5.0 4.5 1 07/02/20 05:11 108-10-1 ND ug/L 1.0 0.35 1 07/02/20 05:11 91-20-3 ND ug/L 20.0 1.8 1 07/02/20 05:11 107-12-0 ND ug/L 1.0 0.27 1 07/02/20 05:11 100-42-5 ND ug/L 1.0 0.34 1 07/02/20 05:11 630-20-6 ND ug/L 1.0 0.22 1 07/02/20 05:11 79-34-5 ND ug/L 1.0 0.16 1 07/02/20 05:11 127-18-4 ND ug/L 1.0 0.24 1 07/02/20 05:11 108-88-3 ND ug/L 1.0 0.34 1 07/02/20 05:11 87-61-6 ND ug/L 1.0 0.22 1 07/02/20 05:11 120-82-1 ND ug/L 1.0 0.18 1 07/02/20 05:11 71-55-6 ND ug/L 1.0 0.24 1 07/02/20 05:11 79-00-5 ND ug/L 1.0 0.22 1 07/02/20 05:11 79-01-6 ND ug/L 1.0 0.31 1 07/02/20 05:11 75-69-4 ND ug/L 1.0 0.35 1 07/02/20 05:11 96-18-4 ND ug/L 2.0 1.4 1 07/02/20 05:11 108-05-4 3.1 ug/L 1.0 0.24 1 07/02/20 05:11 75-01-4 ND ug/L 1.0 0.63 1 07/02/20 05:11 1330-20-7 95 % 70-130 1 07/02/20 05:11 460-00-4 106 % 70-130 1 07/02/20 05:11 17060-07-0 99 % 70-130 1 07/02/20 05:11 2037-26-5 Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville ND ug/L 100 50.0 1 06/30/2018:35 18496-25-8 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville ND ug/L 8.0 6.0 1 06/29/20 22:28 06/30/20 01:33 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v1 v2 Page 10 of 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed Mt. Airy Pace Project No.: 92483783 Sample: MW-3R Lab ID: 92483783002 Collected: 06/25/20 11:45 Received: 06/26/20 08:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 06/27/20 00:47 06/30/20 03:58 7440-36-0 Arsenic 13.8 ug/L 10.0 4.7 1 06/27/20 00:47 06/30/20 03:58 7440-38-2 BC Barium 42.8 ug/L 5.0 3.5 1 06/27/20 00:47 06/30/20 03:58 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 06/27/20 00:47 06/30/20 03:58 7440-41-7 Cadmium 2.3 ug/L 1.0 0.40 1 06/27/20 00:47 06/30/20 03:58 7440-43-9 Chromium ND ug/L 5.0 3.7 1 06/27/20 00:47 06/30/20 03:58 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 06/27/20 00:47 06/30/20 03:58 7440-48-4 Copper ND ug/L 5.0 4.3 1 06/27/20 00:47 06/30/20 03:58 7440-50-8 Lead ND ug/L 5.0 4.5 1 06/27/20 00:47 06/30/20 03:58 7439-92-1 Nickel ND ug/L 5.0 3.5 1 06/27/20 00:47 06/30/20 03:58 7440-02-0 Selenium 6.2J ug/L 10.0 4.7 1 06/27/20 00:47 06/30/20 03:58 7782-49-2 Silver ND ug/L 5.0 2.5 1 06/27/20 00:47 06/30/20 03:58 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 06/27/20 00:47 06/30/20 03:58 7440-62-2 Zinc ND ug/L 10.0 9.5 1 06/27/20 00:47 06/30/20 03:58 7440-66-6 6020 MET ICPMS Thallium 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene Date: 07/10/2020 04:54 PM Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville ND ug/L 0.10 0.050 1 06/27/20 00:13 06/29/20 04:25 7440-28-0 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 6.2 1 07/02/20 04:47 67-64-1 ND ug/L 10.0 0.90 1 07/02/20 04:47 107-13-1 ND ug/L 1.0 0.15 1 07/02/20 04:47 71-43-2 ND ug/L 1.0 0.34 1 07/02/20 04:47 74-97-5 ND ug/L 1.0 0.26 1 07/02/20 04:47 75-27-4 ND ug/L 1.0 0.62 1 07/02/20 04:47 75-25-2 ND ug/L 2.0 0.62 1 07/02/20 04:47 74-83-9 ND ug/L 5.0 3.3 1 07/02/20 04:47 78-93-3 ND ug/L 2.0 0.40 1 07/02/20 04:47 75-15-0 ND ug/L 1.0 0.22 1 07/02/20 04:47 56-23-5 ND ug/L 1.0 0.23 1 07/02/20 04:47 108-90-7 ND ug/L 1.0 0.49 1 07/02/20 04:47 75-00-3 ND ug/L 5.0 2.3 1 07/02/20 04:47 67-66-3 ND ug/L 1.0 0.39 1 07/02/20 04:47 74-87-3 ND ug/L 5.0 0.26 1 07/02/20 04:47 96-12-8 ND ug/L 1.0 0.41 1 07/02/20 04:47 124-48-1 ND ug/L 1.0 0.26 1 07/02/20 04:47 106-93-4 ND ug/L 1.0 0.46 1 07/02/20 04:47 74-95-3 ND ug/L 1.0 0.29 1 07/02/20 04:47 95-50-1 ND ug/L 1.0 0.26 1 07/02/20 04:47 106-46-7 ND ug/L 1.0 0.54 1 07/02/20 04:47 110-57-6 0.85J ug/L 1.0 0.27 1 07/02/20 04:47 75-34-3 ND ug/L 1.0 0.34 1 07/02/20 04:47 107-06-2 ND ug/L 1.0 0.24 1 07/02/20 04:47 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. IK v2 Page 11 of 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed Mt. Airy Pace Project No.: 92483783 Sample: MW-3R Lab ID: 92483783002 Collected: 06/25/20 11:45 Received: 06/26/20 08:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene 1,4-Dioxane (p-Dioxane) Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 07/10/2020 04:54 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1.3 ug/L 1.0 0.29 1 07/02/20 04:47 156-59-2 ND ug/L 1.0 0.25 1 07/02/20 04:47 156-60-5 ND ug/L 1.0 0.19 1 07/02/20 04:47 78-87-5 ND ug/L 1.0 0.30 1 07/02/20 04:47 10061-01-5 ND ug/L 1.0 0.31 1 07/02/20 04:47 10061-02-6 ND ug/L 150 56.2 1 07/02/20 04:47 123-91-1 ND ug/L 1.0 0.26 1 07/02/20 04:47 100-41-4 ND ug/L 5.0 0.57 1 07/02/20 04:47 591-78-6 ND ug/L 20.0 12.5 1 07/02/20 04:47 74-88-4 ND ug/L 5.0 3.7 1 07/02/20 04:47 75-09-2 ND ug/L 5.0 4.5 1 07/02/20 04:47 108-10-1 ND ug/L 1.0 0.27 1 07/02/20 04:47 100-42-5 ND ug/L 1.0 0.34 1 07/02/20 04:47 630-20-6 ND ug/L 1.0 0.22 1 07/02/20 04:47 79-34-5 ND ug/L 1.0 0.16 1 07/02/20 04:47 127-18-4 ND ug/L 1.0 0.24 1 07/02/20 04:47 108-88-3 ND ug/L 1.0 0.18 1 07/02/20 04:47 71-55-6 ND ug/L 1.0 0.24 1 07/02/20 04:47 79-00-5 ND ug/L 1.0 0.22 1 07/02/20 04:47 79-01-6 ND ug/L 1.0 0.31 1 07/02/20 04:47 75-69-4 ND ug/L 1.0 0.35 1 07/02/20 04:47 96-18-4 ND ug/L 2.0 1.4 1 07/02/20 04:47 108-05-4 ND ug/L 1.0 0.24 1 07/02/20 04:47 75-01-4 ND ug/L 1.0 0.63 1 07/02/20 04:47 1330-20-7 95 % 70-130 1 07/02/20 04:47 460-00-4 91 % 70-130 1 07/02/20 04:47 17060-07-0 99 % 70-130 1 07/02/20 04:47 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 12 of 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed Mt. Airy Pace Project No.: 92483783 Sample: MW-6 Lab ID: 92483783003 Collected: 06/25/20 13:40 Received: 06/26/20 08:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 06/27/20 00:47 06/30/20 04:01 7440-36-0 Arsenic 9.7J ug/L 10.0 4.7 1 06/27/20 00:47 06/30/20 04:01 7440-38-2 BC Barium 71.3 ug/L 5.0 3.5 1 06/27/20 00:47 06/30/20 04:01 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 06/27/20 00:47 06/30/20 04:01 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 06/27/20 00:47 06/30/20 04:01 7440-43-9 Chromium ND ug/L 5.0 3.7 1 06/27/20 00:47 06/30/20 04:01 7440-47-3 Cobalt 36.0 ug/L 5.0 3.6 1 06/27/20 00:47 06/30/20 04:01 7440-48-4 Copper ND ug/L 5.0 4.3 1 06/27/20 00:47 06/30/20 04:01 7440-50-8 Lead ND ug/L 5.0 4.5 1 06/27/20 00:47 06/30/20 04:01 7439-92-1 Nickel ND ug/L 5.0 3.5 1 06/27/20 00:47 06/30/20 04:01 7440-02-0 Selenium ND ug/L 10.0 4.7 1 06/27/20 00:47 06/30/20 04:01 7782-49-2 Silver ND ug/L 5.0 2.5 1 06/27/20 00:47 06/30/20 04:01 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 06/27/20 00:47 06/30/20 04:01 7440-62-2 Zinc ND ug/L 10.0 9.5 1 06/27/20 00:47 06/30/20 04:01 7440-66-6 6020 MET ICPMS Thallium 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene Date: 07/10/2020 04:54 PM Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville 0.53 ug/L 0.10 0.050 1 06/27/20 00:13 06/29/20 04:32 7440-28-0 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 6.2 1 07/02/20 05:05 67-64-1 ND ug/L 10.0 0.90 1 07/02/20 05:05 107-13-1 ND ug/L 1.0 0.15 1 07/02/20 05:05 71-43-2 ND ug/L 1.0 0.34 1 07/02/20 05:05 74-97-5 ND ug/L 1.0 0.26 1 07/02/20 05:05 75-27-4 ND ug/L 1.0 0.62 1 07/02/20 05:05 75-25-2 ND ug/L 2.0 0.62 1 07/02/20 05:05 74-83-9 ND ug/L 5.0 3.3 1 07/02/20 05:05 78-93-3 ND ug/L 2.0 0.40 1 07/02/20 05:05 75-15-0 ND ug/L 1.0 0.22 1 07/02/20 05:05 56-23-5 ND ug/L 1.0 0.23 1 07/02/20 05:05 108-90-7 ND ug/L 1.0 0.49 1 07/02/20 05:05 75-00-3 ND ug/L 5.0 2.3 1 07/02/20 05:05 67-66-3 ND ug/L 1.0 0.39 1 07/02/20 05:05 74-87-3 ND ug/L 5.0 0.26 1 07/02/20 05:05 96-12-8 ND ug/L 1.0 0.41 1 07/02/20 05:05 124-48-1 ND ug/L 1.0 0.26 1 07/02/20 05:05 106-93-4 ND ug/L 1.0 0.46 1 07/02/20 05:05 74-95-3 ND ug/L 1.0 0.29 1 07/02/20 05:05 95-50-1 ND ug/L 1.0 0.26 1 07/02/20 05:05 106-46-7 ND ug/L 1.0 0.54 1 07/02/20 05:05 110-57-6 ND ug/L 1.0 0.27 1 07/02/20 05:05 75-34-3 ND ug/L 1.0 0.34 1 07/02/20 05:05 107-06-2 ND ug/L 1.0 0.24 1 07/02/20 05:05 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. IK v2 Page 13 of 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed Mt. Airy Pace Project No.: 92483783 Sample: MW-6 Lab ID: 92483783003 Collected: 06/25/20 13:40 Received: 06/26/20 08:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene 1,4-Dioxane (p-Dioxane) Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 07/10/2020 04:54 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.29 1 07/02/20 05:05 156-59-2 ND ug/L 1.0 0.25 1 07/02/20 05:05 156-60-5 ND ug/L 1.0 0.19 1 07/02/20 05:05 78-87-5 ND ug/L 1.0 0.30 1 07/02/20 05:05 10061-01-5 ND ug/L 1.0 0.31 1 07/02/20 05:05 10061-02-6 ND ug/L 150 56.2 1 07/02/20 05:05 123-91-1 ND ug/L 1.0 0.26 1 07/02/20 05:05 100-41-4 ND ug/L 5.0 0.57 1 07/02/20 05:05 591-78-6 ND ug/L 20.0 12.5 1 07/02/20 05:05 74-88-4 ND ug/L 5.0 3.7 1 07/02/20 05:05 75-09-2 ND ug/L 5.0 4.5 1 07/02/20 05:05 108-10-1 ND ug/L 1.0 0.27 1 07/02/20 05:05 100-42-5 ND ug/L 1.0 0.34 1 07/02/20 05:05 630-20-6 ND ug/L 1.0 0.22 1 07/02/20 05:05 79-34-5 ND ug/L 1.0 0.16 1 07/02/20 05:05 127-18-4 ND ug/L 1.0 0.24 1 07/02/20 05:05 108-88-3 ND ug/L 1.0 0.18 1 07/02/20 05:05 71-55-6 ND ug/L 1.0 0.24 1 07/02/20 05:05 79-00-5 ND ug/L 1.0 0.22 1 07/02/20 05:05 79-01-6 ND ug/L 1.0 0.31 1 07/02/20 05:05 75-69-4 ND ug/L 1.0 0.35 1 07/02/20 05:05 96-18-4 ND ug/L 2.0 1.4 1 07/02/20 05:05 108-05-4 ND ug/L 1.0 0.24 1 07/02/20 05:05 75-01-4 ND ug/L 1.0 0.63 1 07/02/20 05:05 1330-20-7 93 % 70-130 1 07/02/20 05:05 460-00-4 89 % 70-130 1 07/02/20 05:05 17060-07-0 100 % 70-130 1 07/02/20 05:05 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed Mt. Airy Pace Project No.: 92483783 Sample: MW-7 Lab ID: 92483783004 Collected: 06/25/20 13:42 Received: 06/26/20 08:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 06/27/20 00:47 06/30/20 04:04 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 06/27/20 00:47 06/30/20 04:04 7440-38-2 BC Barium 53.8 ug/L 5.0 3.5 1 06/27/20 00:47 06/30/20 04:04 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 06/27/20 00:47 06/30/20 04:04 7440-41-7 Cadmium 0.72J ug/L 1.0 0.40 1 06/27/20 00:47 06/30/20 04:04 7440-43-9 Chromium ND ug/L 5.0 3.7 1 06/27/20 00:47 06/30/20 04:04 7440-47-3 Cobalt 56.0 ug/L 5.0 3.6 1 06/27/20 00:47 06/30/20 04:04 7440-48-4 Copper ND ug/L 5.0 4.3 1 06/27/20 00:47 06/30/20 04:04 7440-50-8 Lead ND ug/L 5.0 4.5 1 06/27/20 00:47 06/30/20 04:04 7439-92-1 Nickel ND ug/L 5.0 3.5 1 06/27/20 00:47 06/30/20 04:04 7440-02-0 Selenium ND ug/L 10.0 4.7 1 06/27/20 00:47 06/30/20 04:04 7782-49-2 Silver ND ug/L 5.0 2.5 1 06/27/20 00:47 06/30/20 04:04 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 06/27/20 00:47 06/30/20 04:04 7440-62-2 Zinc ND ug/L 10.0 9.5 1 06/27/20 00:47 06/30/20 04:04 7440-66-6 6020 MET ICPMS Thallium 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene Date: 07/10/2020 04:54 PM Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville 0.13 ug/L 0.10 0.050 1 06/27/20 00:13 06/29/20 04:39 7440-28-0 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 6.2 1 07/02/20 08:44 67-64-1 ND ug/L 10.0 0.90 1 07/02/20 08:44 107-13-1 ND ug/L 1.0 0.15 1 07/02/20 08:44 71-43-2 ND ug/L 1.0 0.34 1 07/02/20 08:44 74-97-5 ND ug/L 1.0 0.26 1 07/02/20 08:44 75-27-4 ND ug/L 1.0 0.62 1 07/02/20 08:44 75-25-2 ND ug/L 2.0 0.62 1 07/02/20 08:44 74-83-9 ND ug/L 5.0 3.3 1 07/02/20 08:44 78-93-3 ND ug/L 2.0 0.40 1 07/02/20 08:44 75-15-0 ND ug/L 1.0 0.22 1 07/02/20 08:44 56-23-5 0.65J ug/L 1.0 0.23 1 07/02/20 08:44 108-90-7 ND ug/L 1.0 0.49 1 07/02/20 08:44 75-00-3 ND ug/L 5.0 2.3 1 07/02/20 08:44 67-66-3 ND ug/L 1.0 0.39 1 07/02/20 08:44 74-87-3 ND ug/L 5.0 0.26 1 07/02/20 08:44 96-12-8 ND ug/L 1.0 0.41 1 07/02/20 08:44 124-48-1 ND ug/L 1.0 0.26 1 07/02/20 08:44 106-93-4 ND ug/L 1.0 0.46 1 07/02/20 08:44 74-95-3 ND ug/L 1.0 0.29 1 07/02/20 08:44 95-50-1 0.53J ug/L 1.0 0.26 1 07/02/20 08:44 106-46-7 ND ug/L 1.0 0.54 1 07/02/20 08:44 110-57-6 ND ug/L 1.0 0.27 1 07/02/20 08:44 75-34-3 ND ug/L 1.0 0.34 1 07/02/20 08:44 107-06-2 ND ug/L 1.0 0.24 1 07/02/20 08:44 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. IK v2 Page 15 of 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed Mt. Airy Pace Project No.: 92483783 Sample: MW-7 Lab ID: 92483783004 Collected: 06/25/20 13:42 Received: 06/26/20 08:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene 1,4-Dioxane (p-Dioxane) Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 07/10/2020 04:54 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.29 1 07/02/20 08:44 156-59-2 ND ug/L 1.0 0.25 1 07/02/20 08:44 156-60-5 ND ug/L 1.0 0.19 1 07/02/20 08:44 78-87-5 ND ug/L 1.0 0.30 1 07/02/20 08:44 10061-01-5 ND ug/L 1.0 0.31 1 07/02/20 08:44 10061-02-6 ND ug/L 150 56.2 1 07/02/20 08:44 123-91-1 ND ug/L 1.0 0.26 1 07/02/20 08:44 100-41-4 ND ug/L 5.0 0.57 1 07/02/20 08:44 591-78-6 ND ug/L 20.0 12.5 1 07/02/20 08:44 74-88-4 ND ug/L 5.0 3.7 1 07/02/20 08:44 75-09-2 ND ug/L 5.0 4.5 1 07/02/20 08:44 108-10-1 ND ug/L 1.0 0.27 1 07/02/20 08:44 100-42-5 ND ug/L 1.0 0.34 1 07/02/20 08:44 630-20-6 ND ug/L 1.0 0.22 1 07/02/20 08:44 79-34-5 ND ug/L 1.0 0.16 1 07/02/20 08:44 127-18-4 ND ug/L 1.0 0.24 1 07/02/20 08:44 108-88-3 ND ug/L 1.0 0.18 1 07/02/20 08:44 71-55-6 ND ug/L 1.0 0.24 1 07/02/20 08:44 79-00-5 ND ug/L 1.0 0.22 1 07/02/20 08:44 79-01-6 ND ug/L 1.0 0.31 1 07/02/20 08:44 75-69-4 ND ug/L 1.0 0.35 1 07/02/20 08:44 96-18-4 ND ug/L 2.0 1.4 1 07/02/20 08:44 108-05-4 ND ug/L 1.0 0.24 1 07/02/20 08:44 75-01-4 ND ug/L 1.0 0.63 1 07/02/20 08:44 1330-20-7 94 % 70-130 1 07/02/20 08:44 460-00-4 89 % 70-130 1 07/02/20 08:44 17060-07-0 100 % 70-130 1 07/02/20 08:44 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 16 of 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed Mt. Airy Pace Project No.: 92483783 Sample: MW-9 Lab ID: 92483783005 Collected: 06/25/20 13:18 Received: 06/26/20 08:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 06/27/20 00:47 06/30/20 04:07 7440-36-0 Arsenic 10.6 ug/L 10.0 4.7 1 06/27/20 00:47 06/30/20 04:07 7440-38-2 BC Barium 43.9 ug/L 5.0 3.5 1 06/27/20 00:47 06/30/20 04:07 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 06/27/20 00:47 06/30/20 04:07 7440-41-7 Cadmium 0.79J ug/L 1.0 0.40 1 06/27/20 00:47 06/30/20 04:07 7440-43-9 Chromium ND ug/L 5.0 3.7 1 06/27/20 00:47 06/30/20 04:07 7440-47-3 Cobalt 286 ug/L 5.0 3.6 1 06/27/20 00:47 06/30/20 04:07 7440-48-4 Copper ND ug/L 5.0 4.3 1 06/27/20 00:47 06/30/20 04:07 7440-50-8 Lead ND ug/L 5.0 4.5 1 06/27/20 00:47 06/30/20 04:07 7439-92-1 Nickel 8.0 ug/L 5.0 3.5 1 06/27/20 00:47 06/30/20 04:07 7440-02-0 Selenium ND ug/L 10.0 4.7 1 06/27/20 00:47 06/30/20 04:07 7782-49-2 Silver ND ug/L 5.0 2.5 1 06/27/20 00:47 06/30/20 04:07 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 06/27/20 00:47 06/30/20 04:07 7440-62-2 Zinc ND ug/L 10.0 9.5 1 06/27/20 00:47 06/30/20 04:07 7440-66-6 6020 MET ICPMS Thallium 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene Date: 07/10/2020 04:54 PM Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville 0.35 ug/L 0.10 0.050 1 06/27/20 00:13 06/29/20 04:46 7440-28-0 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 6.2 1 07/02/20 02:31 67-64-1 ND ug/L 10.0 0.90 1 07/02/20 02:31 107-13-1 1.3 ug/L 1.0 0.15 1 07/02/20 02:31 71-43-2 ND ug/L 1.0 0.34 1 07/02/20 02:31 74-97-5 ND ug/L 1.0 0.26 1 07/02/20 02:31 75-27-4 ND ug/L 1.0 0.62 1 07/02/20 02:31 75-25-2 ND ug/L 2.0 0.62 1 07/02/20 02:31 74-83-9 ND ug/L 5.0 3.3 1 07/02/20 02:31 78-93-3 ND ug/L 2.0 0.40 1 07/02/20 02:31 75-15-0 ND ug/L 1.0 0.22 1 07/02/20 02:31 56-23-5 ND ug/L 1.0 0.23 1 07/02/20 02:31 108-90-7 1.1 ug/L 1.0 0.49 1 07/02/20 02:31 75-00-3 ND ug/L 5.0 2.3 1 07/02/20 02:31 67-66-3 ND ug/L 1.0 0.39 1 07/02/20 02:31 74-87-3 ND ug/L 5.0 0.26 1 07/02/20 02:31 96-12-8 ND ug/L 1.0 0.41 1 07/02/20 02:31 124-48-1 ND ug/L 1.0 0.26 1 07/02/20 02:31 106-93-4 ND ug/L 1.0 0.46 1 07/02/20 02:31 74-95-3 1.1 ug/L 1.0 0.29 1 07/02/20 02:31 95-50-1 ND ug/L 1.0 0.26 1 07/02/20 02:31 106-46-7 ND ug/L 1.0 0.54 1 07/02/20 02:31 110-57-6 0.87J ug/L 1.0 0.27 1 07/02/20 02:31 75-34-3 0.37J ug/L 1.0 0.34 1 07/02/20 02:31 107-06-2 ND ug/L 1.0 0.24 1 07/02/20 02:31 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. IH,v2 v2 v2 IK Page 17 of 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Closed Mt. Airy Pace Project No.: 92483783 Sample: MW-9 Lab ID: 92483783005 Collected: 06/25/20 13:18 Received: 06/26/20 08:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene 1,4-Dioxane (p-Dioxane) Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 07/10/2020 04:54 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 29.0 ug/L 1.0 0.29 1 07/02/20 02:31 156-59-2 ND ug/L 1.0 0.25 1 07/02/20 02:31 156-60-5 ND ug/L 1.0 0.19 1 07/02/20 02:31 78-87-5 ND ug/L 1.0 0.30 1 07/02/20 02:31 10061-01-5 ND ug/L 1.0 0.31 1 07/02/20 02:31 10061-02-6 ND ug/L 150 56.2 1 07/02/20 02:31 123-91-1 ND ug/L 1.0 0.26 1 07/02/20 02:31 100-41-4 ND ug/L 5.0 0.57 1 07/02/20 02:31 591-78-6 ND ug/L 20.0 12.5 1 07/02/20 02:31 74-88-4 ND ug/L 5.0 3.7 1 07/02/20 02:31 75-09-2 ND ug/L 5.0 4.5 1 07/02/20 02:31 108-10-1 ND ug/L 1.0 0.27 1 07/02/20 02:31 100-42-5 ND ug/L 1.0 0.34 1 07/02/20 02:31 630-20-6 ND ug/L 1.0 0.22 1 07/02/20 02:31 79-34-5 ND ug/L 1.0 0.16 1 07/02/20 02:31 127-18-4 ND ug/L 1.0 0.24 1 07/02/20 02:31 108-88-3 ND ug/L 1.0 0.18 1 07/02/20 02:31 71-55-6 ND ug/L 1.0 0.24 1 07/02/20 02:31 79-00-5 ND ug/L 1.0 0.22 1 07/02/20 02:31 79-01-6 ND ug/L 1.0 0.31 1 07/02/20 02:31 75-69-4 ND ug/L 1.0 0.35 1 07/02/20 02:31 96-18-4 ND ug/L 2.0 1.4 1 07/02/20 02:31 108-05-4 10.3 ug/L 1.0 0.24 1 07/02/20 02:31 75-01-4 ND ug/L 1.0 0.63 1 07/02/20 02:31 1330-20-7 99 % 70-130 1 07/02/20 02:31 460-00-4 105 % 70-130 1 07/02/20 02:31 17060-07-0 98 % 70-130 1 07/02/20 02:31 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v1 v2 Page 18 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 QC Batch: 1501187 Analysis Method: EPA 8151 QC Batch Method: 8151A Analysis Description: Chlorinated Herb. (GC) 8151 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92483783001 METHOD BLANK: R3545459-1 Associated Lab Samples: 92483783001 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed 2,4-D ug/L ND 2.00 0.547 07/01/2015:22 Dalapon ug/L ND 2.00 0.344 07/01/2015:22 2,4-DB ug/L ND 2.00 0.302 07/01/2015:22 Dicamba ug/L ND 2.00 0.245 07/01/2015:22 Dichloroprop ug/L ND 2.00 1.04 07/01/2015:22 Dinoseb ug/L ND 2.00 0.250 07/01/2015:22 MCPA ug/L ND 100 13.1 07/01/2015:22 MCPP ug/L ND 100 66.0 07/01/2015:22 2,4,5-T ug/L ND 2.00 0.258 07/01/2015:22 2,4,5-TP (Silvex) ug/L ND 2.00 0.335 07/01/20 15:22 2,4-DCAA (S) % 76.4 14.0-158 07/01 /20 15:22 Qualifiers LABORATORY CONTROL SAMPLE & LCSD: R3545459-2 R3545459-3 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers 2,4-D ug/L 5.00 4.05 3.88 81.0 77.6 50.0-120 4.29 20 Dalapon ug/L 5.00 4.10 3.32 82.0 66.4 32.0-120 21.0 20 P9,R1 2,4-DB ug/L 5.00 4.26 4.11 85.2 82.2 53.0-140 3.58 20 Dicamba ug/L 5.00 4.01 3.89 80.2 77.8 51.0-120 3.04 20 Dichloroprop ug/L 5.00 4.33 4.22 86.6 84.4 55.0-127 2.57 20 Dinoseb ug/L 5.00 4.19 4.05 83.8 81.0 36.0-134 3.40 20 MCPA ug/L 50.0 113 99.5 226 199 10.0-160 12.7 40 E,L0,P9 MCPP ug/L 50.0 26.6 26.2 53.2 52.4 10.0-160 1.52 23 2,4,5-T ug/L 5.00 4.69 4.51 93.8 90.2 54.0-120 3.91 20 2,4,5-TP (Silvex) ug/L 5.00 3.67 4.22 73.4 84.4 50.0-125 13.9 20 2,4-DCAA (S) % 81.6 77.4 14.0-158 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 QC Batch: 550099 Analysis Method: EPA 7470A QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92483783001 METHOD BLANK: 2925125 Matrix: Water Associated Lab Samples: 92483783001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury ug/L ND 0.20 0.12 06/29/2015:50 LABORATORY CONTROL SAMPLE: 2925126 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.6 102 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2925127 2925128 MS MSD 92483741015 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L ND 2.5 2.5 2.0 2.0 78 80 75-125 3 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 QC Batch: 550033 Analysis Method: EPA 6010D QC Batch Method: EPA 3010A Analysis Description: 6010 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92483783001, 92483783002, 92483783003, 92483783004, 92483783005 METHOD BLANK: 2924973 Matrix: Water Associated Lab Samples: 92483783001, 92483783002, 92483783003, 92483783004, 9248378300f Blank Reporting Parameter Units Result Limit MDL Antimony ug/L ND 5.0 Arsenic ug/L 6.8J 10.0 Barium ug/L ND 5.0 Beryllium ug/L ND 1.0 Cadmium ug/L ND 1.0 Chromium ug/L ND 5.0 Cobalt ug/L ND 5.0 Copper ug/L ND 5.0 Lead ug/L ND 5.0 Nickel ug/L ND 5.0 Selenium ug/L ND 10.0 Silver ug/L ND 5.0 Tin ug/L ND 5.0 Vanadium ug/L ND 5.0 Zinc ug/L ND 10.0 Analyzed Qualifiers 3.0 06/30/20 02:42 4.7 06/30/20 02:42 BC 3.5 06/30/20 02:42 0.70 06/30/20 02:42 0.40 06/30/20 02:42 3.7 06/30/20 02:42 3.6 06/30/20 02:42 4.3 06/30/20 02:42 4.5 06/30/20 02:42 3.5 06/30/20 02:42 4.7 06/30/20 02:42 2.5 06/30/20 02:42 4.7 06/30/20 02:42 3.9 06/30/20 02:42 9.5 06/30/20 02:42 LABORATORY CONTROL SAMPLE: Parameter 2924974 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 523 105 80-120 Arsenic ug/L 500 516 103 80-120 Barium ug/L 500 516 103 80-120 Beryllium ug/L 500 510 102 80-120 Cadmium ug/L 500 511 102 80-120 Chromium ug/L 500 495 99 80-120 Cobalt ug/L 500 514 103 80-120 Copper ug/L 500 527 105 80-120 Lead ug/L 500 511 102 80-120 Nickel ug/L 500 518 104 80-120 Selenium ug/L 500 511 102 80-120 Silver ug/L 250 244 98 80-120 Tin ug/L 500 507 101 80-120 Vanadium ug/L 500 498 100 80-120 Zinc ug/L 500 479 96 80-120 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: Surry Closed Mt. Airy 92483783 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2924975 2924976 MS MSD 92483741007 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 537 537 107 107 75-125 0 20 Arsenic ug/L ND 500 500 527 546 104 108 75-125 4 20 Barium ug/L 191 500 500 722 725 106 107 75-125 0 20 Beryllium ug/L ND 500 500 526 527 105 105 75-125 0 20 Cadmium ug/L 1.4 500 500 539 538 108 107 75-125 0 20 Chromium ug/L ND 500 500 524 522 105 104 75-125 0 20 Cobalt ug/L 18.2 500 500 540 538 104 104 75-125 0 20 Copper ug/L ND 500 500 539 538 108 107 75-125 0 20 Lead ug/L ND 500 500 522 516 104 103 75-125 1 20 Nickel ug/L ND 500 500 528 526 105 105 75-125 0 20 Selenium ug/L ND 500 500 550 564 109 112 75-125 2 20 Silver ug/L ND 250 250 258 256 103 102 75-125 1 20 Tin ug/L ND 500 500 524 521 104 104 75-125 0 20 Vanadium ug/L ND 500 500 524 521 104 104 75-125 1 20 Zinc ug/L ND 500 500 517 516 102 102 75-125 0 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 QC Batch: 550035 Analysis Method: EPA 6020B QC Batch Method: EPA 3010A Analysis Description: 6020 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92483783001, 92483783002, 92483783003, 92483783004, 92483783005 METHOD BLANK: 2924981 Matrix: Water Associated Lab Samples: 92483783001, 92483783002, 92483783003, 92483783004, 92483783005 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L ND 0.10 0.050 06/28/20 23:02 LABORATORY CONTROL SAMPLE: 2924982 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 10 10.4 104 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2924983 2924984 MS MSD 92483741002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L ND 10 10 10.4 10.3 104 103 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 QC Batch: 550875 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92483783002, 92483783003, 92483783004 METHOD BLANK: 2928332 Matrix: Associated Lab Samples: 92483783002, 92483783003, 92483783004 Blank Parameter Units Result Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.34 07/02/20 00:15 1,1,1-Trichloroethane ug/L ND 1.0 0.18 07/02/20 00:15 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 07/02/20 00:15 1,1,2-Trichloroethane ug/L ND 1.0 0.24 07/02/20 00:15 1,1-Dichloroethane ug/L ND 1.0 0.27 07/02/20 00:15 1,1-Dichloroethene ug/L ND 1.0 0.24 07/02/20 00:15 1,2,3-Trichloropropane ug/L ND 1.0 0.35 07/02/20 00:15 1,2-Dibromo-3-chloropropane ug/L ND 5.0 0.26 07/02/20 00:15 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.26 07/02/20 00:15 1,2-Dichlorobenzene ug/L ND 1.0 0.29 07/02/20 00:15 1,2-Dichloroethane ug/L ND 1.0 0.34 07/02/20 00:15 1,2-Dichloropropane ug/L ND 1.0 0.19 07/02/20 00:15 1,4-Dichlorobenzene ug/L ND 1.0 0.26 07/02/20 00:15 1,4-Dioxane (p-Dioxane) ug/L ND 150 56.2 07/02/20 00:15 2-Butanone (MEK) ug/L ND 5.0 3.3 07/02/20 00:15 2-Hexanone ug/L ND 5.0 0.57 07/02/20 00:15 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 4.5 07/02/20 00:15 Acetone ug/L ND 25.0 6.2 07/02/20 00:15 Acrylonitrile ug/L ND 10.0 0.90 07/02/20 00:15 Benzene ug/L ND 1.0 0.15 07/02/20 00:15 Bromochloromethane ug/L ND 1.0 0.34 07/02/20 00:15 Bromodichloromethane ug/L ND 1.0 0.26 07/02/20 00:15 Bromoform ug/L ND 1.0 0.62 07/02/20 00:15 Bromomethane ug/L ND 2.0 0.62 07/02/20 00:15 Carbon disulfide ug/L ND 2.0 0.40 07/02/20 00:15 Carbon tetrachloride ug/L ND 1.0 0.22 07/02/20 00:15 Chlorobenzene ug/L ND 1.0 0.23 07/02/20 00:15 Chloroethane ug/L ND 1.0 0.49 07/02/20 00:15 Chloroform ug/L ND 5.0 2.3 07/02/20 00:15 Chloromethane ug/L ND 1.0 0.39 07/02/20 00:15 cis-1,2-Dichloroethene ug/L ND 1.0 0.29 07/02/20 00:15 cis-1,3-Dichloropropene ug/L ND 1.0 0.30 07/02/20 00:15 Dibromochloromethane ug/L ND 1.0 0.41 07/02/20 00:15 Dibromomethane ug/L ND 1.0 0.46 07/02/20 00:15 Ethylbenzene ug/L ND 1.0 0.26 07/02/20 00:15 lodomethane ug/L ND 20.0 12.5 07/02/20 00:15 Methylene Chloride ug/L ND 5.0 3.7 07/02/20 00:15 Styrene ug/L ND 1.0 0.27 07/02/20 00:15 Tetrachloroethene ug/L ND 1.0 0.16 07/02/20 00:15 Toluene ug/L ND 1.0 0.24 07/02/20 00:15 13 v2 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 METHOD BLANK: 2928332 Matrix: Associated Lab Samples: 92483783002, 92483783003, 92483783004 Blank Parameter Units Result Water Reporting Limit MDL Analyzed Qualifiers trans-1,2-Dichloroethene ug/L ND 1.0 0.25 07/02/20 00:15 trans- 1,3-Dichloropropene ug/L ND 1.0 0.31 07/02/20 00:15 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.54 07/02/20 00:15 Trichloroethene ug/L ND 1.0 0.22 07/02/20 00:15 Trichlorofluoromethane ug/L ND 1.0 0.31 07/02/20 00:15 Vinyl acetate ug/L ND 2.0 1.4 07/02/20 00:15 Vinyl chloride ug/L ND 1.0 0.24 07/02/20 00:15 Xylene (Total) ug/L ND 1.0 0.63 07/02/20 00:15 1,2-Dichloroethane-d4 (S) % 90 70-130 07/02/20 00:15 4-Bromofluorobenzene (S) % 95 70-130 07/02/20 00:15 Toluene-d8 (S) % 99 70-130 07/02/20 00:15 LABORATORY CONTROL SAMPLE: Parameter 2928333 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 53.7 107 70-130 1,1,1-Trichloroethane ug/L 50 47.5 95 70-130 1,1,2,2-Tetrachloroethane ug/L 50 53.5 107 70-130 1,1,2-Trichloroethane ug/L 50 50.2 100 70-130 1,1-Dichloroethane ug/L 50 46.3 93 70-130 1,1-Dichloroethene ug/L 50 49.5 99 70-130 1,2,3-Trichloropropane ug/L 50 52.9 106 70-130 1,2-Dibromo-3-chloropropane ug/L 50 51.0 102 70-130 1,2-Dibromoethane (EDB) ug/L 50 52.3 105 70-130 1,2-Dichlorobenzene ug/L 50 52.2 104 70-130 1,2-Dichloroethane ug/L 50 48.2 96 70-130 1,2-Dichloropropane ug/L 50 50.0 100 70-130 1,4-Dichlorobenzene ug/L 50 51.9 104 70-130 1,4-Dioxane(p-Dioxane) ug/L 1000 1060 106 59-169 2-Butanone (MEK) ug/L 100 88.8 89 64-135 2-Hexanone ug/L 100 103 103 66-135 4-Methyl-2-pentanone (MIBK) ug/L 100 96.9 97 70-130 Acetone ug/L 100 86.1 86 61-157 Acrylonitrile ug/L 250 223 89 61-143 Benzene ug/L 50 49.4 99 70-130 Bromochloromethane ug/L 50 47.3 95 70-130 Bromodichloromethane ug/L 50 46.4 93 70-130 Bromoform ug/L 50 54.0 108 70-130 Bromomethane ug/L 50 43.4 87 38-130lK Carbon disulfide ug/L 50 43.2 86 68-130 Carbon tetrachloride ug/L 50 50.4 101 70-130 Chlorobenzene ug/L 50 51.3 103 70-130 Chloroethane ug/L 50 51.5 103 37-142 Chloroform ug/L 50 47.1 94 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 LABORATORY CONTROL SAMPLE: Parameter 2928333 Units Spike Conc. LCS LCS Result % Rec Chloromethane ug/L 50 33.5 cis-1,2-Dichloroethene ug/L 50 47.0 cis-1,3-Dichloropropene ug/L 50 51.7 Dibromochloromethane ug/L 50 53.5 Dibromomethane ug/L 50 51.2 Ethylbenzene ug/L 50 51.3 lodomethane ug/L 100 77.6 Methylene Chloride ug/L 50 46.5 Styrene ug/L 50 54.7 Tetrachloroethene ug/L 50 50.4 Toluene ug/L 50 48.4 trans-1,2-Dichloroethene ug/L 50 47.7 trans- 1,3-Dichloropropene ug/L 50 50.8 trans-1,4-Dichloro-2-butene ug/L 50 50.2 Trichloroethene ug/L 50 51.9 Trichlorofluoromethane ug/L 50 45.5 Vinyl acetate ug/L 100 94.3 Vinyl chloride ug/L 50 40.7 Xylene (Total) ug/L 150 156 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % % Rec Limits Qualifiers 67 48-130 v3 94 70-130 103 70-130 107 70-130 102 70-130 103 70-130 78 40-130 93 67-132 109 70-130 101 69-130 97 70-130 95 70-130 102 70-130 100 35-189 104 70-130 91 63-130 94 55-143 81 70-131 104 70-130 92 70-130 104 70-130 96 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2928334 MS 92483822003 Spike Parameter Units Result Conc. MSD Spike Conc. 2928335 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 21.2 20.9 106 105 73-134 1 30 1,1,1-Trichloroethane ug/L ND 20 20 24.0 23.9 120 119 82-143 1 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 23.4 23.3 117 116 70-136 1 30 1,1,2-Trichloroethane ug/L ND 20 20 21.9 21.7 109 108 70-135 1 30 1,1-Dichloroethane ug/L ND 20 20 25.8 25.6 129 128 70-139 1 30 1,1-Dichloroethene ug/L ND 20 20 26.5 26.4 132 132 70-154 0 30 1,2,3-Trichloropropane ug/L ND 20 20 22.5 22.9 112 115 71-137 2 30 1,2-Dibromo-3- ug/L ND 20 20 20.6 20.4 103 102 65-134 1 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 22.6 22.6 113 113 70-137 0 30 1,2-Dichlorobenzene ug/L ND 20 20 23.0 23.0 115 115 70-133 0 30 1,2-Dichloroethane ug/L ND 20 20 24.4 24.4 122 122 70-137 0 30 1,2-Dichloropropane ug/L ND 20 20 24.1 24.1 121 121 70-140 0 30 1,4-Dichlorobenzene ug/L ND 20 20 22.5 22.4 112 112 70-133 0 30 1,4-Dioxane (p-Dioxane) ug/L ND 400 400 479 485 120 121 53-168 1 30 2-Butanone (MEK) ug/L ND 40 40 53.2 51.9 133 130 60-139 2 30 2-Hexanone ug/L ND 40 40 48.1 47.5 120 119 65-138 1 30 4-Methyl-2-pentanone ug/L ND 40 40 46.4 45.8 116 114 65-135 1 30 (MIBK) Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2928334 2928335 MS MSD 92483822003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Acetone ug/L ND 40 40 56.4 54.7 141 137 60-148 3 30 v1 Acrylonitrile ug/L ND 100 100 123 126 123 126 64-147 2 30 Benzene ug/L ND 20 20 23.3 23.4 117 117 70-151 0 30 Bromochloromethane ug/L ND 20 20 23.7 23.8 118 119 70-141 0 30 Bromodichloromethane ug/L ND 20 20 19.3 19.6 97 98 70-138 2 30 Bromoform ug/L ND 20 20 18.2 18.2 91 91 63-130 0 30 Bromomethane ug/L ND 20 20 28.5 28.8 142 144 15-152 1 30 Carbon disulfide ug/L ND 20 20 25.9 25.8 129 129 69-149 1 30 Carbon tetrachloride ug/L ND 20 20 20.9 21.3 104 106 70-143 2 30 Chlorobenzene ug/L ND 20 20 22.5 22.7 112 113 70-138 1 30 Chloroethane ug/L ND 20 20 38.1 37.4 190 187 52-163 2 30 IK,IL, M1,v1 Chloroform ug/L ND 20 20 23.8 23.6 119 118 70-139 1 30 Chloromethane ug/L ND 20 20 24.4 24.6 122 123 41-139 1 30 cis-1,2-Dichloroethene ug/L ND 20 20 25.0 25.0 125 125 70-141 0 30 cis-1,3-Dichloropropene ug/L ND 20 20 22.6 22.6 113 113 70-137 0 30 Dibromochloromethane ug/L ND 20 20 20.4 20.3 102 101 70-134 1 30 Dibromomethane ug/L ND 20 20 20.5 20.4 103 102 70-138 1 30 Ethylbenzene ug/L ND 20 20 22.8 22.9 114 115 66-153 0 30 lodomethane ug/L ND 40 40 28.6 28.0 71 70 20-138 2 30 v3 Methylene Chloride ug/L ND 20 20 25.3 25.5 126 127 42-159 1 30 Styrene ug/L ND 20 20 22.8 22.5 114 113 70-135 1 30 Tetrachloroethene ug/L ND 20 20 20.7 21.2 103 106 59-143 3 30 Toluene ug/L ND 20 20 22.4 22.5 112 112 59-148 0 30 trans-1,2-Dichloroethene ug/L ND 20 20 26.2 26.4 131 132 70-146 1 30 trans-1,3-Dichloropropene ug/L ND 20 20 21.7 21.8 108 109 70-135 0 30 trans-1,4-Dichloro-2-butene ug/L ND 20 20 17.7 17.8 88 89 47-135 1 30 Trichloroethene ug/L ND 20 20 22.1 22.3 110 111 70-147 1 30 Trichlorofluoromethane ug/L ND 20 20 25.0 25.1 125 125 70-148 0 30 Vinyl acetate ug/L ND 40 40 50.8 49.8 127 125 49-151 2 30 Vinyl chloride ug/L ND 20 20 23.4 23.0 117 115 70-156 2 30 Xylene (Total) ug/L ND 60 60 68.8 69.3 115 115 63-158 1 30 1,2-Dichloroethane-d4 (S) % 115 116 70-130 4-Bromofluorobenzene (S) % 101 101 70-130 Toluene-d8 (S) % 102 103 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 QC Batch: 550889 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92483783001, 92483783005 METHOD BLANK: 2928454 Associated Lab Samples: 92483783001, 92483783005 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.34 07/02/20 01:01 1,1,1-Trichloroethane ug/L ND 1.0 0.18 07/02/20 01:01 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 07/02/20 01:01 1,1,2-Trichloroethane ug/L ND 1.0 0.24 07/02/20 01:01 1,1-Dichloroethane ug/L ND 1.0 0.27 07/02/20 01:01 1,1-Dichloroethene ug/L ND 1.0 0.24 07/02/20 01:01 1,1-Dichloropropene ug/L ND 1.0 0.21 07/02/20 01:01 1,2,3-Trichlorobenzene ug/L ND 1.0 0.34 07/02/20 01:01 1,2,3-Trichloropropane ug/L ND 1.0 0.35 07/02/20 01:01 1,2,4-Trichlorobenzene ug/L ND 1.0 0.22 07/02/20 01:01 1,2-Dibromo-3-chloropropane ug/L ND 5.0 0.26 07/02/20 01:01 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.26 07/02/20 01:01 1,2-Dichlorobenzene ug/L ND 1.0 0.29 07/02/20 01:01 1,2-Dichloroethane ug/L ND 1.0 0.34 07/02/20 01:01 1,2-Dichloropropane ug/L ND 1.0 0.19 07/02/20 01:01 1,3-Dichloropropane ug/L ND 1.0 0.16 07/02/20 01:01 1,4-Dichlorobenzene ug/L ND 1.0 0.26 07/02/20 01:01 1,4-Dioxane (p-Dioxane) ug/L ND 150 56.2 07/02/20 01:01 2,2-Dichloropropane ug/L ND 1.0 0.27 07/02/20 01:01 2-Butanone (MEK) ug/L ND 5.0 3.3 07/02/20 01:01 2-Hexanone ug/L ND 5.0 0.57 07/02/20 01:01 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 4.5 07/02/20 01:01 Acetone ug/L ND 25.0 6.2 07/02/20 01:01 Acetonitrile ug/L ND 50.0 30.4 07/02/20 01:01 Acrolein ug/L ND 10.0 2.7 07/02/20 01:01 Acrylonitrile ug/L ND 10.0 0.90 07/02/20 01:01 Allyl chloride ug/L ND 2.0 0.28 07/02/20 01:01 Benzene ug/L ND 1.0 0.15 07/02/20 01:01 Bromochloromethane ug/L ND 1.0 0.34 07/02/20 01:01 Bromodichloromethane ug/L ND 1.0 0.26 07/02/20 01:01 Bromoform ug/L ND 1.0 0.62 07/02/20 01:01 Bromomethane ug/L 0.89J 2.0 0.62 07/02/20 01:01 Carbon disulfide ug/L ND 2.0 0.40 07/02/20 01:01 Carbon tetrachloride ug/L ND 1.0 0.22 07/02/20 01:01 Chlorobenzene ug/L ND 1.0 0.23 07/02/20 01:01 Chloroethane ug/L ND 1.0 0.49 07/02/20 01:01 Chloroform ug/L ND 5.0 2.3 07/02/20 01:01 Chloromethane ug/L ND 1.0 0.39 07/02/20 01:01 Chloroprene ug/L ND 5.0 1.7 07/02/20 01:01 cis-1,2-Dichloroethene ug/L ND 1.0 0.29 07/02/20 01:01 Qualifiers v1 v1 IH,v2 v2 v2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 METHOD BLANK: 2928454 Associated Lab Samples: 92483783001, 92483783005 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed cis-1,3-Dichloropropene ug/L ND 1.0 0.30 07/02/20 01:01 Dibromochloromethane ug/L ND 1.0 0.41 07/02/20 01:01 Dibromomethane ug/L ND 1.0 0.46 07/02/20 01:01 Dichlorodifluoromethane ug/L ND 1.0 0.23 07/02/20 01:01 Ethyl methacrylate ug/L ND 1.0 0.51 07/02/20 01:01 Ethylbenzene ug/L ND 1.0 0.26 07/02/20 01:01 Hexachloro-1,3-butadiene ug/L 1.1 1.0 0.44 07/02/20 01:01 lodomethane ug/L ND 20.0 12.5 07/02/20 01:01 Isobutanol ug/L ND 100 66.4 07/02/20 01:01 Methacrylonitrile ug/L ND 10.0 1.9 07/02/20 01:01 Methyl methacrylate ug/L ND 2.0 0.46 07/02/20 01:01 Methylene Chloride ug/L ND 5.0 3.7 07/02/20 01:01 Naphthalene ug/L ND 1.0 0.35 07/02/20 01:01 Propionitrile ug/L ND 20.0 1.8 07/02/20 01:01 Styrene ug/L ND 1.0 0.27 07/02/20 01:01 Tetrachloroethene ug/L ND 1.0 0.16 07/02/20 01:01 Toluene ug/L ND 1.0 0.24 07/02/20 01:01 trans-1,2-Dichloroethene ug/L ND 1.0 0.25 07/02/20 01:01 trans- 1,3-Dichloropropene ug/L ND 1.0 0.31 07/02/20 01:01 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.54 07/02/20 01:01 Trichloroethene ug/L ND 1.0 0.22 07/02/20 01:01 Trichlorofluoromethane ug/L ND 1.0 0.31 07/02/20 01:01 Vinyl acetate ug/L ND 2.0 1.4 07/02/20 01:01 Vinyl chloride ug/L ND 1.0 0.24 07/02/20 01:01 Xylene (Total) ug/L ND 1.0 0.63 07/02/20 01:01 1,2-Dichloroethane-d4 (S) % 106 70-130 07/02/20 01:01 4-Bromofluorobenzene (S) % 102 70-130 07/02/20 01:01 Toluene-d8 (S) % 100 70-130 07/02/20 01:01 LABORATORY CONTROL SAMPLE: Parameter 2928455 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 53.4 107 70-130 1,1,1-Trichloroethane ug/L 50 46.6 93 70-130 1,1,2,2-Tetrachloroethane ug/L 50 53.7 107 70-130 1,1,2-Trichloroethane ug/L 50 47.2 94 70-130 1,1-Dichloroethane ug/L 50 48.2 96 70-130 1,1-Dichloroethene ug/L 50 47.6 95 70-130 1,1-Dichloropropene ug/L 50 45.7 91 70-130 1,2,3-Trichlorobenzene ug/L 50 52.3 105 70-130 1,2,3-Trichloropropane ug/L 50 54.5 109 70-130 1,2,4-Trichlorobenzene ug/L 50 50.2 100 70-130 1,2-Dibromo-3-chloropropane ug/L 50 58.8 118 70-130 1,2-Dibromoethane (EDB) ug/L 50 53.3 107 70-130 Qualifiers IK v2 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Surry Closed Mt. Airy Pace Project No.: 92483783 LABORATORY CONTROL SAMPLE: 2928455 Parameter QUALITY CONTROL DATA Spike LCS LCS % Rec Units Conc. Result % Rec Limits Qualifiers 1,2-Dichlorobenzene ug/L 50 52.7 105 70-130 1,2-Dichloroethane ug/L 50 44.0 88 70-130 1,2-Dichloropropane ug/L 50 49.1 98 70-130 1,3-Dichloropropane ug/L 50 56.4 113 70-131 1,4-Dichlorobenzene ug/L 50 52.0 104 70-130 1,4-Dioxane(p-Dioxane) ug/L 1000 1180 118 59-169 2,2-Dichloropropane ug/L 50 46.7 93 69-130 2-Butanone (MEK) ug/L 100 99.1 99 64-135 2-Hexanone ug/L 100 121 121 66-135 v1 4-Methyl-2-pentanone (MIBK) ug/L 100 99.4 99 70-130 Acetone ug/L 100 103 103 61-157 Acetonitrile ug/L 500 585 117 62-130 Acrolein ug/L 250 308 123 10-200 v3 Acrylonitrile ug/L 250 241 96 61-143 Allyl chloride ug/L 50 51.6 103 70-130 Benzene ug/L 50 49.4 99 70-130 Bromochloromethane ug/L 50 49.9 100 70-130 Bromodichloromethane ug/L 50 44.2 88 70-130 Bromoform ug/L 50 54.2 108 70-130 Bromomethane ug/L 50 38.4 77 38-130lH,v3 Carbon disulfide ug/L 50 44.3 89 68-130 Carbon tetrachloride ug/L 50 51.0 102 70-130 Chlorobenzene ug/L 50 52.5 105 70-130 Chloroethane ug/L 50 39.0 78 37-142 v3 Chloroform ug/L 50 46.7 93 70-130 Chloromethane ug/L 50 33.0 66 48-130 v3 Chloroprene ug/L 50 47.9 96 70-130 cis-1,2-Dichloroethene ug/L 50 47.1 94 70-130 cis-1,3-Dichloropropene ug/L 50 52.5 105 70-130 Dibromochloromethane ug/L 50 56.4 113 70-130 Dibromomethane ug/L 50 52.2 104 70-130 Dichlorodifluoromethane ug/L 50 40.4 81 53-134 Ethyl methacrylate ug/L 50 56.7 113 70-130 Ethylbenzene ug/L 50 53.0 106 70-130 Hexachloro-1,3-butadiene ug/L 50 47.0 94 68-132 lodomethane ug/L 100 92.7 93 40-130 Isobutanol ug/L 1000 1020 102 44-144 Methacrylonitrile ug/L 500 487 97 66-130 Methyl methacrylate ug/L 50 50.3 101 69-130 Methylene Chloride ug/L 50 46.7 93 67-132 Naphthalene ug/L 50 56.4 113 70-130 Propionitrile ug/L 500 506 101 70-130 Styrene ug/L 50 53.7 107 70-130 Tetrachloroethene ug/L 50 56.4 113 69-130 Toluene ug/L 50 49.1 98 70-130 trans-1,2-Dichloroethene ug/L 50 48.8 98 70-130 trans- 1,3-Dichloropropene ug/L 50 50.9 102 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 LABORATORY CONTROL SAMPLE: Parameter 2928455 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers trans-1,4-Dichloro-2-butene ug/L 50 43.5 87 35-1891K Trichloroethene ug/L 50 51.0 102 70-130 Trichlorofluoromethane ug/L 50 33.9 68 63-130 v3 Vinyl acetate ug/L 100 98.9 99 55-143 Vinyl chloride ug/L 50 40.9 82 70-131 Xylene (Total) ug/L 150 161 107 70-130 1,2-Dichloroethane-d4 (S) % 102 70-130 4-Bromofluorobenzene (S) % 102 70-130 Toluene-d8 (S) % 100 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2928456 MS 92483759023 Spike Parameter Units Result Conc. MSD Spike Conc. 2928457 MS Result MSD MS Result % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 23.2 21.7 116 109 73-134 7 30 1,1,1-Trichloroethane ug/L ND 20 20 21.1 19.9 106 100 82-143 6 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 22.8 21.1 114 106 70-136 8 30 1,1,2-Trichloroethane ug/L ND 20 20 20.6 19.0 103 95 70-135 8 30 1,1-Dichloroethane ug/L ND 20 20 21.3 20.0 106 100 70-139 6 30 1,1-Dichloroethene ug/L ND 20 20 23.0 20.5 115 103 70-154 11 30 1,1-Dichloropropene ug/L ND 20 20 21.0 19.7 105 99 70-149 6 30 1,2,3-Trichlorobenzene ug/L ND 20 20 23.8 22.9 119 114 70-135 4 30 1,2,3-Trichloropropane ug/L ND 20 20 22.4 21.9 112 109 71-137 2 30 1,2,4-Trichlorobenzene ug/L ND 20 20 23.5 23.6 118 118 73-140 0 30 1,2-Dibromo-3- ug/L ND 20 20 22.9 24.3 115 122 65-134 6 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 22.4 20.1 112 100 70-137 11 30 1,2-Dichlorobenzene ug/L ND 20 20 23.6 21.7 118 109 70-133 8 30 1,2-Dichloroethane ug/L ND 20 20 18.5 17.7 93 88 70-137 5 30 1,2-Dichloropropane ug/L ND 20 20 20.8 20.0 104 100 70-140 4 30 1,3-Dichloropropane ug/L ND 20 20 23.0 22.7 115 114 70-143 1 30 1,4-Dichlorobenzene ug/L ND 20 20 21.2 22.5 106 112 70-133 6 30 1,4-Dioxane (p-Dioxane) ug/L ND 400 400 431 378 108 94 53-168 13 30 2,2-Dichloropropane ug/L ND 20 20 21.2 19.9 106 100 61-148 6 30 2-Butanone (MEK) ug/L ND 40 40 41.3 37.9 103 95 60-139 9 30 2-Hexanone ug/L ND 40 40 44.6 44.8 111 112 65-138 0 30 4-Methyl-2-pentanone ug/L ND 40 40 40.1 36.2 100 90 65-135 10 30 (MIBK) Acetone ug/L ND 40 40 42.4 39.6 106 99 60-148 7 30 Acetonitrile ug/L ND 200 200 305 190 152 95 65-141 47 30 M1,R1 Acrolein ug/L ND 100 100 121 112 121 112 28-162 8 30 Acrylonitrile ug/L ND 100 100 100 94.0 100 94 64-147 6 30 Allyl chloride ug/L ND 20 20 22.8 19.2 114 96 70-133 17 30 Benzene ug/L ND 20 20 21.7 20.7 109 103 70-151 5 30 Bromochloromethane ug/L ND 20 20 21.9 20.3 109 101 70-141 8 30 Bromodichloromethane ug/L ND 20 20 17.5 17.0 87 85 70-138 3 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2928456 2928457 MS MSD 92483759023 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Bromoform ug/L ND 20 20 20.9 19.2 105 96 63-130 8 30 Bromomethane ug/L ND 20 20 26.8 24.6 131 119 15-152 9 30 IH,v3 Carbon disulfide ug/L ND 20 20 20.3 19.1 102 96 69-149 6 30 Carbon tetrachloride ug/L ND 20 20 21.2 19.7 106 99 70-143 7 30 Chlorobenzene ug/L ND 20 20 21.8 21.0 109 105 70-138 4 30 Chloroethane ug/L ND 20 20 19.9 18.1 99 91 52-163 9 30 Chloroform ug/L ND 20 20 21.1 18.9 105 95 70-139 11 30 Chloromethane ug/L ND 20 20 14.4 13.5 72 68 41-139 6 30 v3 Chloroprene ug/L ND 20 20 21.1 20.1 106 101 70-135 5 30 cis-1,2-Dichloroethene ug/L ND 20 20 20.5 19.8 103 99 70-141 4 30 cis-1,3-Dichloropropene ug/L ND 20 20 21.7 19.4 109 97 70-137 11 30 Dibromochloromethane ug/L ND 20 20 21.1 20.2 105 101 70-134 4 30 Dibromomethane ug/L ND 20 20 21.8 20.6 109 103 70-138 6 30 Dichlorodifluoromethane ug/L ND 20 20 17.2 16.0 86 80 47-155 7 30 Ethyl methacrylate ug/L ND 20 20 22.2 21.1 111 106 70-132 5 30 Ethylbenzene ug/L ND 20 20 22.3 21.4 111 107 66-153 4 30 Hexachloro-1,3-butadiene ug/L ND 20 20 24.3 22.4 121 112 65-149 8 30 lodomethane ug/L ND 40 40 36.7 35.0 92 88 20-138 5 30 v3 Isobutanol ug/L ND 400 400 446 409 112 102 41-152 9 30 Methacrylonitrile ug/L ND 200 200 202 190 101 95 67-134 6 30 Methyl methacrylate ug/L ND 20 20 20.8 17.3 104 86 70-130 19 30 Methylene Chloride ug/L ND 20 20 19.8 18.7 99 93 42-159 6 30 Naphthalene ug/L ND 20 20 24.6 24.4 123 122 61-148 1 30 Propionitrile ug/L ND 200 200 205 192 102 96 70-131 7 30 Styrene ug/L ND 20 20 22.4 22.7 112 113 70-135 1 30 Tetrachloroethene ug/L ND 20 20 24.0 21.8 120 109 59-143 9 30 Toluene ug/L ND 20 20 20.4 18.2 102 91 59-148 11 30 trans-1,2-Dichloroethene ug/L ND 20 20 21.9 18.7 109 94 70-146 16 30 trans-1,3-Dichloropropene ug/L ND 20 20 20.1 18.1 100 90 70-135 10 30 trans-1,4-Dichloro-2-butene ug/L ND 20 20 11.7 13.1 58 65 47-135 11 30 IK,v3 Trichloroethene ug/L ND 20 20 21.5 19.6 107 98 70-147 9 30 Trichlorofluoromethane ug/L ND 20 20 18.6 16.8 93 84 70-148 10 30 Vinyl acetate ug/L ND 40 40 40.1 37.4 100 93 49-151 7 30 Vinyl chloride ug/L ND 20 20 17.6 16.9 88 85 70-156 4 30 Xylene (Total) ug/L ND 60 60 69.6 64.8 116 108 63-158 7 30 1,2-Dichloroethane-d4 (S) % 103 104 70-130 4-Bromofluorobenzene (S) % 98 99 70-130 Toluene-d8 (S) % 99 98 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 QC Batch: 550642 Analysis Method: EPA 8081 B QC Batch Method: EPA 3510C Analysis Description: 8081 OC Pesticides Red Vol Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92483783001 METHOD BLANK: 2927269 Associated Lab Samples: 92483783001 Parameter 4,4'-DDD 4,4'-DDE 4,4'-DDT Aldrin alpha-BHC beta-BHC Chlordane (Technical) delta-BHC Dieldrin Endosulfan I Endosulfan 11 Endosulfan sulfate Endrin Endrin aldehyde gamma-BHC (Lindane) Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Matrix: Water Units Blank Result Reporting Limit MDL Analyzed ug/L ND 0.050 0.0069 07/06/20 15:43 ug/L ND 0.050 0.0064 07/06/20 15:43 ug/L ND 0.050 0.018 07/06/20 15:43 ug/L ND 0.050 0.022 07/06/20 15:43 ug/L ND 0.050 0.019 07/06/20 15:43 ug/L ND 0.050 0.014 07/06/20 15:43 ug/L ND 0.20 0.14 07/06/20 15:43 ug/L ND 0.050 0.020 07/06/20 15:43 ug/L ND 0.050 0.0073 07/06/20 15:43 ug/L ND 0.050 0.0094 07/06/20 15:43 ug/L ND 0.050 0.0065 07/06/20 15:43 ug/L ND 0.050 0.0091 07/06/20 15:43 ug/L ND 0.050 0.0089 07/06/20 15:43 ug/L ND 0.050 0.013 07/06/20 15:43 ug/L ND 0.050 0.012 07/06/20 15:43 ug/L ND 0.050 0.016 07/06/20 15:43 ug/L ND 0.050 0.0097 07/06/20 15:43 ug/L ND 0.15 0.033 07/06/20 15:43 ug/L ND 0.20 0.19 07/06/20 15:43 % 89 10-130 07/06/20 15:43 % 75 10-130 07/06/20 15:43 LABORATORY CONTROL SAMPLE: 2927270 Qualifiers Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 4,4'-DDD ug/L 0.25 0.30 119 49-130 4,4'-DDE ug/L 0.25 0.26 105 56-130 4,4'-DDT ug/L 0.25 0.28 112 45-130 Aldrin ug/L 0.25 0.21 86 25-130 alpha-BHC ug/L 0.25 0.24 96 53-130 beta-BHC ug/L 0.25 0.30 120 46-130 delta-BHC ug/L 0.25 0.26 102 54-130 Dieldrin ug/L 0.25 0.28 110 54-130 Endosulfan I ug/L 0.25 0.26 104 43-130 Endosulfan II ug/L 0.25 0.29 115 64-130 Endosulfan sulfate ug/L 0.25 0.29 115 66-130 Endrin ug/L 0.25 0.27 109 56-130 Endrin aldehyde ug/L 0.25 0.26 106 59-130 gamma-BHC (Lindane) ug/L 0.25 0.25 99 57-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 LABORATORY CONTROL SAMPLE: 2927270 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Heptachlor ug/L 0.25 0.22 89 37-130 Heptachlor epoxide ug/L 0.25 0.24 96 56-130 Methoxychlor ug/L 0.75 0.79 106 46-130 Decachlorobiphenyl (S) % 92 10-130 Tetrachloro-m-xylene (S) % 89 10-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2927271 2927272 MS MSD 92471456023 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 4,4'-DDD ug/L ND 0.25 0.25 0.23 0.12 92 48 28-130 63 30 R1 4,4'-DDE ug/L ND 0.25 0.25 0.18 0.099 73 40 26-130 59 30 R1 4,4'-DDT ug/L ND 0.25 0.25 0.21 0.11 84 44 11-130 62 30 R1 Aldrin ug/L ND 0.25 0.25 0.20 0.10 78 40 10-130 65 30 R1 alpha-BHC ug/L ND 0.25 0.25 0.20 0.10 79 40 27-130 65 30 R1 beta-BHC ug/L ND 0.25 0.25 0.26 0.13 102 53 15-130 64 30 R1 delta-BHC ug/L ND 0.25 0.25 0.24 0.14 97 54 44-130 56 30 R1 Dieldrin ug/L ND 0.25 0.25 0.21 0.11 84 45 20-130 61 30 R1 Endosulfan I ug/L ND 0.25 0.25 0.25 0.13 99 50 10-139 65 30 R1 Endosulfan II ug/L ND 0.25 0.25 0.23 0.14 94 56 36-130 50 30 R1 Endosulfan sulfate ug/L ND 0.25 0.25 0.30 0.14 118 57 45-130 69 30 R1 Endrin ug/L ND 0.25 0.25 0.23 0.11 90 46 26-130 66 30 R1 Endrin aldehyde ug/L ND 0.25 0.25 0.23 0.12 93 50 19-160 61 30 R1 gamma-BHC (Lindane) ug/L ND 0.25 0.25 0.21 0.10 83 42 33-130 66 30 R1 Heptachlor ug/L ND 0.25 0.25 0.19 0.10 77 42 25-130 59 30 R1 Heptachlor epoxide ug/L ND 0.25 0.25 0.22 0.11 87 44 18-130 66 30 R1 Methoxychlor ug/L ND 0.75 0.75 0.59 0.34 79 45 10-130 55 30 R1 Decachlorobiphenyl (S) % 31 24 10-130 Tetrachloro-m-xylene (S) % 76 40 10-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 QC Batch: 550643 Analysis Method: EPA 8082A QC Batch Method: EPA 3510C Analysis Description: 8082 GCS PCB Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92483783001 METHOD BLANK: 2927273 Matrix: Water Associated Lab Samples: 92483783001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers PCB-1016 (Aroclor 1016) ug/L ND 0.50 0.22 07/03/20 00:04 PCB-1221 (Aroclor 1221) ug/L ND 0.50 0.32 07/03/20 00:04 PCB-1232 (Aroclor 1232) ug/L ND 0.50 0.21 07/03/20 00:04 PCB-1242 (Aroclor 1242) ug/L ND 0.50 0.44 07/03/20 00:04 PCB-1248 (Aroclor 1248) ug/L ND 0.50 0.34 07/03/20 00:04 PCB-1254 (Aroclor 1254) ug/L ND 0.50 0.24 07/03/20 00:04 PCB-1260 (Aroclor 1260) ug/L ND 0.50 0.30 07/03/20 00:04 Decachlorobiphenyl (S) % 56 10-130 07/03/20 00:04 LABORATORY CONTROL SAMPLE: 2927274 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers PCB-1016 (Aroclor 1016) ug/L 5 5.3 105 41-130 PCB-1260 (Aroclor 1260) ug/L 5 5.0 100 42-130 Decachlorobiphenyl (S) % 76 10-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2927275 2927276 MS MSD 92476314022 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual PCB-1016 (Aroclor 1016) ug/L ND 5 5 4.4 4.9 88 98 15-130 11 30 PCB-1260 (Aroclor 1260) ug/L ND 5 5 3.2 3.5 63 69 10-130 9 30 Decachlorobiphenyl (S) % 38 39 10-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 QC Batch: 550645 Analysis Method: EPA 8270E QC Batch Method: EPA 3510C Analysis Description: 8270E Water APP9 RV MSSV Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92483783001 METHOD BLANK: 2927281 Associated Lab Samples: 92483783001 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed 1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 4.6 07/09/20 21:45 1,3,5-Trinitrobenzene ug/L ND 10.0 5.3 07/09/20 21:45 1,3-Dinitrobenzene ug/L ND 10.0 3.7 07/09/20 21:45 1,4-Naphthoquinone ug/L ND 5.0 2.4 07/09/20 21:45 1-Naphthalenamine ug/L ND 5.0 4.6 07/09/20 21:45 2,2'-Oxybis(1-chloropropane) ug/L ND 10.0 1.3 07/09/20 21:45 2,3,4,6-Tetrachlorophenol ug/L ND 10.0 1.6 07/09/20 21:45 2,4,5-Trichlorophenol ug/L ND 10.0 1.5 07/09/20 21:45 2,4,6-Trichlorophenol ug/L ND 10.0 1.4 07/09/20 21:45 2,4-Dichlorophenol ug/L ND 10.0 1.5 07/09/20 21:45 2,4-Dimethylphenol ug/L ND 10.0 1.5 07/09/20 21:45 2,4-Dinitrophenol ug/L ND 50.0 7.3 07/09/20 21:45 2,4-Dinitrotoluene ug/L ND 10.0 1.7 07/09/20 21:45 2,6-Dichlorophenol ug/L ND 10.0 2.7 07/09/20 21:45 2,6-Dinitrotoluene ug/L ND 10.0 1.7 07/09/20 21:45 2-Acetylaminofluorene ug/L ND 10.0 1.9 07/09/20 21:45 2-Chloronaphthalene ug/L ND 10.0 1.4 07/09/20 21:45 2-Chlorophenol ug/L ND 10.0 1.4 07/09/20 21:45 2-Methylnaphthalene ug/L ND 10.0 1.4 07/09/20 21:45 2-Methylphenol(o-Cresol) ug/L ND 10.0 1.2 07/09/20 21:45 2-Naphthalenamine ug/L ND 10.0 6.1 07/09/20 21:45 2-Nitroaniline ug/L ND 20.0 3.0 07/09/20 21:45 2-Nitrophenol ug/L ND 10.0 1.7 07/09/20 21:45 3&4-Methyl phenol (m&p Cresol) ug/L ND 10.0 1.2 07/09/20 21:45 3,3'-Dichlorobenzidine ug/L ND 20.0 2.7 07/09/20 21:45 3,3'-Dimethylbenzidine ug/L ND 25.0 23.5 07/09/20 21:45 3-Methylcholanthrene ug/L ND 10.0 5.3 07/09/20 21:45 3-Nitroaniline ug/L ND 20.0 2.8 07/09/20 21:45 4,6-Dinitro-2-methyl phenol ug/L ND 20.0 4.5 07/09/20 21:45 4-Aminobiphenyl ug/L ND 10.0 4.2 07/09/20 21:45 4-Bromophenylphenyl ether ug/L ND 10.0 1.2 07/09/20 21:45 4-ChIoro-3-methyl phenol ug/L ND 10.0 2.8 07/09/20 21:45 4-Chloroaniline ug/L ND 20.0 2.8 07/09/20 21:45 4-Chlorophenylphenyl ether ug/L ND 10.0 1.5 07/09/20 21:45 4-Nitroaniline ug/L ND 20.0 3.1 07/09/20 21:45 4-Nitrophenol ug/L ND 50.0 9.4 07/09/20 21:45 5-Nitro-o-toluidine ug/L ND 10.0 2.4 07/09/20 21:45 7,12-Dimethylbenz(a)anthracene ug/L ND 10.0 2.8 07/09/20 21:45 Acenaphthene ug/L ND 10.0 1.4 07/09/20 21:45 Acenaphthylene ug/L ND 10.0 1.5 07/09/20 21:45 IH IL Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 METHOD BLANK: 2927281 Matrix: Water Associated Lab Samples: 92483783001 Blank Reporting Parameter Units Result Limit MDL Analyzed Acetophenone ug/L ND 10.0 1.3 07/09/20 21:45 Anthracene ug/L ND 10.0 1.6 07/09/20 21:45 Benzo(a)anthracene ug/L ND 10.0 1.5 07/09/20 21:45 Benzo(a)pyrene ug/L ND 10.0 1.8 07/09/20 21:45 Benzo(b)fluoranthene ug/L ND 10.0 1.7 07/09/20 21:45 Benzo(g,h,i)perylene ug/L ND 10.0 1.6 07/09/20 21:45 Benzo(k)fluoranthene ug/L ND 10.0 1.5 07/09/20 21:45 Benzyl alcohol ug/L ND 20.0 2.6 07/09/20 21:45 bis(2-Chloroethoxy)methane ug/L ND 10.0 1.3 07/09/20 21:45 bis(2-Chloroethyl) ether ug/L ND 10.0 1.7 07/09/20 21:45 bis(2-Ethylhexyl)phthalate ug/L ND 6.0 2.0 07/09/20 21:45 Butylbenzylphthalate ug/L ND 10.0 1.9 07/09/20 21:45 Chlorobenzilate ug/L ND 10.0 3.6 07/09/20 21:45 Chrysene ug/L ND 10.0 1.4 07/09/20 21:45 Di-n-butylphthalate ug/L ND 10.0 1.6 07/09/20 21:45 Di-n-octylphthalate ug/L ND 10.0 2.2 07/09/20 21:45 Diallate ug/L ND 10.0 2.7 07/09/20 21:45 Dibenz(a,h)anthracene ug/L ND 10.0 1.6 07/09/20 21:45 Dibenzofuran ug/L ND 10.0 1.3 07/09/20 21:45 Diethylphthalate ug/L ND 10.0 1.6 07/09/20 21:45 Dimethoate ug/L ND 10.0 2.0 07/09/20 21:45 Dimethylphthalate ug/L ND 10.0 1.4 07/09/20 21:45 Diphenylamine ug/L ND 10.0 1.4 07/09/20 21:45 Disulfoton ug/L ND 10.0 6.0 07/09/20 21:45 Ethyl methanesulfonate ug/L ND 20.0 2.8 07/09/20 21:45 Famphur ug/L ND 10.0 5.7 07/09/20 21:45 Fluoranthene ug/L ND 10.0 1.6 07/09/20 21:45 Fluorene ug/L ND 10.0 1.4 07/09/20 21:45 Hexachlorobenzene ug/L ND 10.0 1.3 07/09/20 21:45 Hexachlorocyclopentadiene ug/L ND 10.0 2.4 07/09/20 21:45 Hexachloroethane ug/L ND 10.0 1.3 07/09/20 21:45 Hexachloropropene ug/L ND 10.0 5.5 07/09/20 21:45 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 1.7 07/09/20 21:45 Isodrin ug/L ND 10.0 3.0 07/09/20 21:45 Isophorone ug/L ND 10.0 1.3 07/09/20 21:45 Isosafrole ug/L ND 10.0 3.6 07/09/20 21:45 Kepone ug/L ND 10.0 8.2 07/09/20 21:45 Methapyrilene ug/L ND 50.0 27.2 07/09/20 21:45 IH Methyl methanesulfonate ug/L ND 5.0 3.0 07/09/20 21:45 Methyl parathion ug/L ND 10.0 2.0 07/09/20 21:45 N-Nitroso-di-n-butylamine ug/L ND 10.0 6.2 07/09/20 21:45 N-Nitroso-di-n-propylamine ug/L ND 10.0 1.3 07/09/20 21:45 N-Nitrosodiethylamine ug/L ND 10.0 2.0 07/09/20 21:45 N-Nitrosodimethylamine ug/L ND 10.0 1.8 07/09/20 21:45 N-Nitrosodiphenylamine ug/L ND 10.0 1.4 07/09/20 21:45 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 METHOD BLANK: 2927281 Associated Lab Samples: 92483783001 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed N-Nitrosomethylethylamine ug/L ND 10.0 3.3 07/09/20 21:45 N-Nitrosopiperidine ug/L ND 10.0 2.6 07/09/20 21:45 N-Nitrosopyrrolidine ug/L ND 10.0 2.1 07/09/20 21:45 Nitrobenzene ug/L ND 10.0 1.5 07/09/20 21:45 O,O,O-Triethylphosphorothioate ug/L ND 10.0 3.5 07/09/20 21:45 O-Toluidine ug/L ND 10.0 2.8 07/09/20 21:45 P-Dimethylaminoazobenzene ug/L ND 5.0 3.3 07/09/20 21:45 p-Phenylenediamine ug/L ND 10.0 4.2 07/09/20 21:45 Parathion (Ethyl parathion) ug/L ND 10.0 2.0 07/09/20 21:45 Pentachlorobenzene ug/L ND 10.0 4.4 07/09/20 21:45 Pentachloronitrobenzene ug/L ND 10.0 2.4 07/09/20 21:45 Pentachlorophenol ug/L ND 20.0 2.8 07/09/20 21:45 Phenacetin ug/L ND 10.0 1.9 07/09/20 21:45 Phenanthrene ug/L ND 10.0 1.4 07/09/20 21:45 Phenol ug/L ND 10.0 1.5 07/09/20 21:45 Phorate ug/L ND 10.0 3.8 07/09/20 21:45 Pronamide ug/L ND 10.0 2.4 07/09/20 21:45 Pyrene ug/L ND 10.0 1.5 07/09/20 21:45 Safrole ug/L ND 10.0 3.2 07/09/20 21:45 Thionazin ug/L ND 10.0 1.8 07/09/20 21:45 2,4,6-Tribromophenol (S) % 95 10-137 07/09/20 21:45 2-Fluorobiphenyl (S) % 91 13-130 07/09/20 21:45 2-Fluorophenol (S) % 68 10-130 07/09/20 21:45 Nitrobenzene-d5 (S) % 96 13-130 07/09/20 21:45 Phenol-d6 (S) % 54 10-130 07/09/20 21:45 Terphenyl-d14 (S) % 121 25-130 07/09/20 21:45 LABORATORY CONTROL SAMPLE: Parameter 2927282 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,2,4,5-Tetrachlorobenzene ug/L 50 42.8 86 10-130 1,3,5-Trinitrobenzene ug/L 50 65.0 130 50-130 1,3-Dinitrobenzene ug/L 50 59.3 119 30-130 1,4-Naphthoquinone ug/L 50 31.4 63 30-130 1-Naphthalenamine ug/L 50 44.9 90 30-130 2,2'-Oxybis(1-chloropropane) ug/L 50 47.8 96 20-130 2,3,4,6-Tetrachlorophenol ug/L 50 56.9 114 40-200 2,4,5-Trichlorophenol ug/L 50 55.1 110 40-130 2,4,6-Trichlorophenol ug/L 50 54.0 108 40-130 2,4-Dichlorophenol ug/L 50 50.6 101 31-130 2,4-Dimethylphenol ug/L 50 50.6 101 30-130 2,4-Dinitrophenol ug/L 250 295 118 30-130 2,4-Dinitrotoluene ug/L 50 54.2 108 49-130 2,6-Dichlorophenol ug/L 50 52.5 105 50-130 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 LABORATORY CONTROL SAMPLE: Parameter 2927282 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2,6-Dinitrotoluene ug/L 50 55.6 111 50-130 2-Acetylaminofluorene ug/L 50 62.3 125 70-150 2-Chloronaphthalene ug/L 50 49.3 99 30-130 2-Chlorophenol ug/L 50 46.4 93 30-130 2-Methylnaphthalene ug/L 50 47.7 95 30-130 2-Methylphenol(o-Cresol) ug/L 50 45.8 92 30-130 2-Naphthalenamine ug/L 50 47.9 96 30-130 2-Nitroaniline ug/L 100 109 109 40-130 2-Nitrophenol ug/L 50 51.0 102 20-130 3&4-Methyl phenol (m&p Cresol) ug/L 50 42.1 84 20-130 3,3'-Dichlorobenzidine ug/L 100 104 104 10-150 3,3'-Dimethylbenzidine ug/L 100 122 122 10-150lH 3-Methylcholanthrene ug/L 50 55.9 112 40-130IL 3-Nitroaniline ug/L 100 108 108 40-130 4,6-Dinitro-2-methyl phenol ug/L 100 111 111 40-130 4-Aminobiphenyl ug/L 50 37.8 76 20-130 4-Bromophenylphenyl ether ug/L 50 51.4 103 30-130 4-Chloro-3-methylphenol ug/L 100 99.9 100 30-130 4-Chloroaniline ug/L 100 98.1 98 20-130 4-Chlorophenylphenyl ether ug/L 50 49.8 100 20-130 4-Nitroaniline ug/L 100 110 110 40-130 4-Nitrophenol ug/L 250 180 72 10-130 5-Nitro-o-toluidine ug/L 50 62.4 125 50-150 7,12-Dimethylbenz(a)anthracene ug/L 50 51.8 104 50-130 Acenaphthene ug/L 50 51.2 102 30-130 Acenaphthylene ug/L 50 51.9 104 30-130 Acetophenone ug/L 50 46.9 94 20-130 Anthracene ug/L 50 52.1 104 50-130 Benzo(a)anthracene ug/L 50 54.7 109 50-130 Benzo(a)pyrene ug/L 50 56.0 112 50-130 Benzo(b)fluoranthene ug/L 50 59.6 119 50-130 Benzo(g,h,i)perylene ug/L 50 55.5 111 50-130 Benzo(k)fluoranthene ug/L 50 57.2 114 50-130 Benzyl alcohol ug/L 100 92.0 92 20-130 bis(2-Chloroethoxy)methane ug/L 50 50.0 100 30-130 bis(2-Chloroethyl) ether ug/L 50 48.6 97 30-130 bis(2-Ethylhexyl)phthalate ug/L 50 55.8 112 50-130 Butylbenzylphthalate ug/L 50 57.5 115 50-150 Chlorobenzilate ug/L 50 71.4 143 50-130 L1 Chrysene ug/L 50 54.7 109 50-130 Di-n-butylphthalate ug/L 50 52.7 105 50-130 Di-n-octylphthalate ug/L 50 56.0 112 50-130 Diallate ug/L 50 51.8 104 50-130 Dibenz(a,h)anthracene ug/L 50 56.0 112 40-130 Dibenzofuran ug/L 50 50.2 100 40-130 Diethylphthalate ug/L 50 51.3 103 40-130 Dimethoate ug/L 50 57.3 115 50-150 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 LABORATORY CONTROL SAMPLE: Parameter 2927282 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Dimethylphthalate ug/L 50 50.8 102 40-130 Diphenylamine ug/L 50 50.9 102 30-130 Disulfoton ug/L 50 53.9 108 40-150 Ethyl methanesulfonate ug/L 50 47.7 95 40-130 Famphur ug/L 100 69.0 69 30-150 Fluoranthene ug/L 50 52.6 105 30-130 Fluorene ug/L 50 51.5 103 20-130 Hexachlorobenzene ug/L 50 50.5 101 30-130 Hexachlorocyclopentadiene ug/L 50 44.0 88 10-150 Hexachloroethane ug/L 50 40.1 80 10-130 Hexachloropropene ug/L 50 29.6 59 10-150 Indeno(1,2,3-cd)pyrene ug/L 50 55.3 111 40-130 Isodrin ug/L 50 52.8 106 40-130 Isophorone ug/L 50 50.2 100 30-130 Isosafrole ug/L 50 47.6 95 40-130 Kepone ug/L 100 70.8 71 10-130 Methapyrilene ug/L 50 ND 48 10-150IH Methyl methanesulfonate ug/L 50 43.6 87 20-130 Methyl parathion ug/L 50 64.0 128 50-130 N-Nitroso-di-n-butylamine ug/L 50 44.0 88 30-130 N-Nitroso-di-n-propylamine ug/L 50 48.1 96 30-130 N-Nitrosodiethylamine ug/L 50 49.1 98 40-130 N-Nitrosodimethylamine ug/L 50 42.2 84 10-130 N-Nitrosodiphenylamine ug/L 50 50.9 102 30-130 N-Nitrosomethylethylamine ug/L 50 47.0 94 30-130 N-Nitrosopiperidine ug/L 50 53.2 106 30-130 N-Nitrosopyrrolidine ug/L 50 50.3 101 30-130 Nitrobenzene ug/L 50 50.1 100 20-130 O,O,O-Triethylphosphorothioate ug/L 50 49.2 98 40-130 O-Toluidine ug/L 50 47.2 94 20-130 P-Dimethylaminoazobenzene ug/L 50 26.5 53 10-130 p-Phenylenediamine ug/L 50 ND 0 70-140 L2 Parathion (Ethyl parathion) ug/L 50 65.0 130 50-150 Pentachlorobenzene ug/L 50 47.6 95 30-150 Pentachloronitrobenzene ug/L 50 63.9 128 60-130 Pentachlorophenol ug/L 100 120 120 10-140 Phenacetin ug/L 50 60.5 121 60-130 Phenanthrene ug/L 50 51.9 104 50-130 Phenol ug/L 50 30.0 60 10-130 Phorate ug/L 50 53.0 106 50-130 Pronamide ug/L 50 56.4 113 70-130 Pyrene ug/L 50 54.9 110 50-130 Safrole ug/L 50 47.9 96 30-130 Thionazin ug/L 50 56.1 112 60-130 2,4,6-Tribromophenol (S) % 125 10-137 2-Fluorobiphenyl (S) % 108 13-130 2-Fluorophenol (S) % 79 10-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 LABORATORY CONTROL SAMPLE: 2927282 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrobenzene-d5 (S) % 110 13-130 Phenol-d6 (S) % 65 10-130 Terphenyl-d14 (S) % 136 25-130 SO MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2927283 2927284 MS MSD 92483783001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,2,4,5-Tetrachlorobenzene ug/L ND 100 100 45.8 55.5 46 55 10-130 19 30 1,3,5-Trinitrobenzene ug/L ND 100 100 95.0 104 95 104 50-130 9 30 1,3-Dinitrobenzene ug/L ND 100 100 82.5 96.3 82 96 30-130 16 30 1,4-Naphthoquinone ug/L ND 100 100 41.4 51.0 41 51 30-130 21 30 1-Naphthalenamine ug/L ND 100 100 38.4 49.1 38 49 30-130 24 30 2,2'-Oxybis(1- ug/L ND 100 100 46.7 55.2 47 55 20-130 17 30 chloropropane) 2,3,4,6-Tetrachlorophenol ug/L ND 100 100 81.5 94.2 82 94 40-200 14 30 2,4,5-Trichlorophenol ug/L ND 100 100 70.6 85.1 71 85 40-130 19 30 2,4,6-Trichlorophenol ug/L ND 100 100 60.8 76.9 61 77 40-130 23 30 2,4-Dichlorophenol ug/L ND 100 100 55.1 66.6 55 67 31-130 19 30 2,4-Dimethylphenol ug/L ND 100 100 57.6 65.6 58 66 30-130 13 30 2,4-Dinitrophenol ug/L ND 500 500 402 472 80 94 30-130 16 30 2,4-Dinitrotoluene ug/L ND 100 100 80.7 89.0 81 89 49-130 10 30 2,6-Dichlorophenol ug/L ND 100 100 57.5 70.0 58 70 50-130 20 30 2,6-Dinitrotoluene ug/L ND 100 100 73.9 85.7 74 86 50-130 15 30 2-Acetylam inofl uorene ug/L ND 100 100 97.1 111 97 111 70-150 14 30 2-Chloronaphthalene ug/L ND 100 100 52.3 62.6 52 63 30-130 18 30 2-Chlorophenol ug/L ND 100 100 51.1 59.6 51 60 30-130 15 30 2-Methyl naphthalene ug/L ND 100 100 51.7 61.2 52 61 30-130 17 30 2-Methyl phenol(o-Cresol) ug/L ND 100 100 53.1 64.4 53 64 30-130 19 30 2-Naphthalenamine ug/L ND 100 100 41.3 52.3 41 52 30-130 23 30 2-Nitroaniline ug/L ND 200 200 131 158 66 79 40-130 19 30 2-Nitrophenol ug/L ND 100 100 54.9 67.1 55 67 20-130 20 30 3&4-Methylphenol(m&p ug/L ND 100 100 49.8 60.5 50 61 20-130 19 30 Cresol) 3,3'-Dichlorobenzidine ug/L ND 200 200 158 168 79 84 10-150 6 30 3,3'-Dimethylbenzidine ug/L ND 200 200 218 215 109 108 10-150 1 30 IH 3-Methylcholanthrene ug/L ND 100 100 89.7 95.7 90 96 40-130 7 30 IL 3-Nitroaniline ug/L ND 200 200 153 176 76 88 40-130 14 30 4,6-Dinitro-2-methylphenol ug/L ND 200 200 161 178 81 89 40-130 10 30 4-Aminobiphenyl ug/L ND 100 100 51.5 56.6 51 57 20-130 10 30 4-Bromophenylphenyl ether ug/L ND 100 100 68.2 80.8 68 81 30-130 17 30 4-Chloro-3-methylphenol ug/L ND 200 200 123 151 61 75 30-130 21 30 4-Chloroaniline ug/L ND 200 200 91.4 119 46 60 20-130 26 30 4-Chlorophenylphenyl ether ug/L ND 100 100 60.4 72.5 60 73 20-130 18 30 4-Nitroaniline ug/L ND 200 200 166 182 83 91 40-130 9 30 4-Nitrophenol ug/L ND 500 500 339 378 68 76 10-130 11 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2927283 MS 92483783001 Spike Parameter Units Result Conc. MSD Spike Conc. 2927284 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 5-Nitro-o-toluidine ug/L ND 100 100 96.0 105 96 105 50-150 9 30 7,12- ug/L ND 100 100 79.7 84.0 80 84 50-130 5 30 Dimethylbenz(a)anthracene Acenaphthene ug/L ND 100 100 56.6 68.8 57 69 30-130 19 30 Acenaphthylene ug/L ND 100 100 57.4 69.8 57 70 30-130 20 30 Acetophenone ug/L ND 100 100 50.1 59.7 50 60 20-130 17 30 Anthracene ug/L ND 100 100 76.9 84.6 77 85 50-130 10 30 Benzo(a)anth race ne ug/L ND 100 100 86.2 91.1 86 91 50-130 5 30 Benzo(a)pyrene ug/L ND 100 100 84.7 89.8 85 90 50-130 6 30 Benzo(b)fluoranthene ug/L ND 100 100 89.1 94.9 89 95 50-130 6 30 Benzo(g,h,i)perylene ug/L ND 100 100 84.1 89.9 84 90 50-130 7 30 Benzo(k)fluoranthene ug/L ND 100 100 86.0 89.3 86 89 50-130 4 30 Benzyl alcohol ug/L ND 200 200 105 126 52 63 20-130 18 30 bis(2- ug/L ND 100 100 51.9 62.2 52 62 30-130 18 30 Chloroethoxy)methane bis(2-Chloroethyl) ether ug/L ND 100 100 52.1 61.7 52 62 30-130 17 30 bis(2- Ethyl hexyl)phthalate ug/L ND 100 100 90.0 95.0 88 93 50-130 5 30 Butylbenzylphthalate ug/L ND 100 100 89.2 94.2 89 94 50-150 5 30 Chlorobenzilate ug/L ND 100 100 134 133 134 133 50-130 0 30 MO Chrysene ug/L ND 100 100 85.5 89.9 86 90 50-130 5 30 Di-n-butylphthalate ug/L ND 100 100 84.9 89.0 85 89 50-130 5 30 Di-n-octylphthalate ug/L ND 100 100 90.0 103 90 103 50-130 14 30 Diallate ug/L ND 100 100 69.5 81.0 70 81 50-130 15 30 Dibenz(a,h)anthracene ug/L ND 100 100 84.6 90.6 85 91 40-130 7 30 Dibenzofuran ug/L ND 100 100 58.5 71.1 59 71 40-130 19 30 Diethylphthalate ug/L ND 100 100 77.0 84.6 77 85 40-130 9 30 Dimethoate ug/L ND 100 100 91.0 97.0 91 97 50-150 6 30 Dimethylphthalate ug/L ND 100 100 68.5 78.8 68 79 40-130 14 30 Diphenylamine ug/L ND 100 100 71.3 79.7 71 80 30-130 11 30 Disulfoton ug/L ND 100 100 82.4 91.3 82 91 40-150 10 30 Ethyl methanesulfonate ug/L ND 100 100 51.2 62.3 51 62 40-130 20 30 Famphur ug/L ND 200 200 119 128 60 64 30-150 7 30 Fluoranthene ug/L ND 100 100 83.2 87.5 83 88 30-130 5 30 Fluorene ug/L ND 100 100 63.8 76.4 64 76 20-130 18 30 Hexachlorobenzene ug/L ND 100 100 71.3 79.7 71 80 30-130 11 30 Hexachlorocyclopentadiene ug/L ND 100 100 43.0 51.3 43 51 10-150 18 30 Hexachloroethane ug/L ND 100 100 40.9 44.1 41 44 10-130 8 30 Hexachloropropene ug/L ND 100 100 34.3 36.5 34 37 10-150 6 30 Indeno(1,2,3-cd)pyrene ug/L ND 100 100 83.9 89.3 84 89 40-130 6 30 Isodrin ug/L ND 100 100 77.9 85.1 78 85 40-130 9 30 Isophorone ug/L ND 100 100 53.3 64.4 53 64 30-130 19 30 Isosafrole ug/L ND 100 100 51.2 62.9 51 63 40-130 20 30 Kepone ug/L ND 200 200 127 148 63 74 10-130 15 30 Methapyrilene ug/L ND 100 100 58.5J 69.9J 58 70 10-150 30 IH Methyl methanesulfonate ug/L ND 100 100 46.8 58.8 47 59 20-130 23 30 Methyl parathion ug/L ND 100 100 101 107 101 107 50-130 6 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2927283 2927284 MS MSD 92483783001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual N-Nitroso-di-n-butylamine ug/L ND 100 100 58.5 68.8 58 69 30-130 16 30 N-Nitroso-di-n-propylamine ug/L ND 100 100 51.4 62.1 51 62 30-130 19 30 N-Nitrosodiethylamine ug/L ND 100 100 51.8 63.1 52 63 40-130 20 30 N-Nitrosodimethylamine ug/L ND 100 100 49.3 58.8 49 59 10-130 18 30 N-Nitrosodiphenylamine ug/L ND 100 100 71.3 79.7 71 80 30-130 11 30 N-Nitrosomethylethylamine ug/L ND 100 100 57.2 65.2 57 65 30-130 13 30 N-Nitrosopiperidine ug/L ND 100 100 57.7 69.8 58 70 30-130 19 30 N-Nitrosopyrrolidine ug/L ND 100 100 57.2 70.6 57 71 30-130 21 30 Nitrobenzene ug/L ND 100 100 51.6 61.9 52 62 20-130 18 30 0,0,0- ug/L ND 100 100 51.9 64.0 52 64 40-130 21 30 Triethylphosphorothioate O-Toluidine ug/L ND 100 100 40.9 54.3 41 54 20-130 28 30 P- ug/L ND 100 100 41.8 43.7 42 44 10-130 4 30 Dimethylaminoazobenzene p-Phenylenediamine ug/L ND 100 100 ND ND 0 0 70-140 30 MO Parathion (Ethyl parathion) ug/L ND 100 100 101 108 101 108 50-150 7 30 Pentachlorobenzene ug/L ND 100 100 55.0 67.9 55 68 30-150 21 30 Pentachloronitrobenzene ug/L ND 100 100 96.0 104 96 104 60-130 8 30 Pentachlorophenol ug/L ND 200 200 166 187 83 94 10-140 12 30 Phenacetin ug/L ND 100 100 95.6 102 96 102 60-130 6 30 Phenanthrene ug/L ND 100 100 76.4 83.8 76 84 50-130 9 30 Phenol ug/L ND 100 100 38.8 48.5 39 48 10-130 22 30 Phorate ug/L ND 100 100 73.0 83.5 73 83 50-130 13 30 Pronamide ug/L ND 100 100 89.9 95.5 90 95 70-130 6 30 Pyrene ug/L ND 100 100 86.4 91.4 86 91 50-130 6 30 Safrole ug/L ND 100 100 51.7 61.5 52 61 30-130 17 30 Thionazin ug/L ND 100 100 84.1 91.3 84 91 60-130 8 30 2,4,6-Tribromophenol (S) % 92 103 10-137 2-Fluorobiphenyl (S) % 55 67 13-130 2-Fluorophenol (S) % 45 55 10-130 Nitrobenzene-d5 (S) % 55 67 13-130 Phenol-d6 (S) % 41 52 10-130 Terphenyl-d14 (S) % 106 113 25-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 QC Batch: 550256 Analysis Method: SM 4500-S2D-2011 QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92483783001 METHOD BLANK: 2925884 Matrix: Water Associated Lab Samples: 92483783001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfide ug/L ND 100 50.0 06/30/2018:31 LABORATORY CONTROL SAMPLE: 2925885 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 517 103 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2925886 2925887 MS MSD 92483478002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 567 570 107 107 80-120 1 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2925888 2925890 MS MSD 92483619013 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 479 478 96 96 80-120 0 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 54 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Closed Mt. Airy Pace Project No.: 92483783 QC Batch: 550319 Analysis Method: SM 4500-CN-E-2011 QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 450OCNE Cyanide, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92483783001 METHOD BLANK: 2926095 Matrix: Water Associated Lab Samples: 92483783001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 8.0 6.0 06/30/20 01:19 LABORATORY CONTROL SAMPLE: 2926096 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 103 103 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2926097 2926098 MS MSD 92483594002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L 0.019 100 100 109 107 90 88 80-120 2 10 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: Surry Closed Mt. Airy Pace Project No.: 92483783 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. ANALYTE QUALIFIERS BC The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the laboratory reporting limit. E Analyte concentration exceeded the calibration range. The reported result is estimated. IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be considered an estimated value. IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be considered an estimated value. IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be considered an estimated value. LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits. L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samples may be biased low. MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. P9 RPD between the primary and confirmatory analysis exceeded 40%. R1 RPD value was outside control limits. SO Surrogate recovery outside laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: Surry Closed Mt. Airy Pace Project No.: 92483783 ANALYTE QUALIFIERS v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias. v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: Surry Closed Mt. Airy 92483783 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92483783001 MW-20 8151A 1501187 EPA 8151 1501187 92483783001 MW-20 EPA 3510C 550642 EPA 8081B 550969 92483783001 MW-20 EPA 3510C 550643 EPA 8082A 550971 92483783001 MW-20 EPA 3010A 550033 EPA 6010D 550040 92483783002 MW-3R EPA 3010A 550033 EPA 6010D 550040 92483783003 MW-6 EPA 3010A 550033 EPA 6010D 550040 92483783004 MW-7 EPA 3010A 550033 EPA 6010D 550040 92483783005 MW-9 EPA 3010A 550033 EPA 6010D 550040 92483783001 MW-20 EPA 3010A 550035 EPA 6020B 550045 92483783002 MW-3R EPA 3010A 550035 EPA 6020B 550045 92483783003 MW-6 EPA 3010A 550035 EPA 6020B 550045 92483783004 MW-7 EPA 3010A 550035 EPA 6020B 550045 92483783005 MW-9 EPA 3010A 550035 EPA 6020B 550045 92483783001 MW-20 EPA 7470A 550099 EPA 7470A 550105 92483783001 MW-20 EPA 3510C 550645 EPA 8270E 550849 92483783001 MW-20 EPA 8260D 550889 92483783002 MW-3R EPA 8260D 550875 92483783003 MW-6 EPA 8260D 550875 92483783004 MW-7 EPA 8260D 550875 92483783005 MW-9 EPA 8260D 550889 92483783001 MW-20 SM 4500-S2D-2011 550256 92483783001 MW-20 SM 4500-CN-E-2011 550319 SM 4500-CN-E-2011 550344 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/10/2020 04:54 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 54 a aC8Analytteal Document Name: Sample Condition Upon Recelpt(SCUR) Document Revised: February 7, 2018 Page 1 of 2 Document No.: lssuingAuthority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville [� Raleigh❑ Mechanicsville❑ Simple Condition Client Name: Receipt Wo# : 92483783 upon �: iProject # � Courier,, ❑Fed Ex ❑UPS CUSPS ❑Client []Other:111111 IN 111111111 Ili Commercial Pace Other: ��/ U^� 11f2463783 Custody Seal Present? [:]yes [2KO Seals Intact? ❑Yes fO late/Initlala Person Examining Contents: A76 Packing Material: ❑Bubble wrap Bubble Bags []None ❑ Other Thermometer Type of Ice* ❑t et []Blue IR Gun ID: 92 061 Cooler Temp J'Q Z c7ection Factor: Add/Subtract (T) +0.1 Cooler Temp Corrected USDA Regulated Soil (do, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? ram. - Biological Tissue Frozen ❑None Dyes ❑No ❑IV< Temp should be above freezing to VC ❑Samples out of temp criteria. Samples on Ice, coaling process has begun Old samples originate from a foreign source (internatia ally, tnrlur ine Hawaii and Puerto Ricol? ❑Yes ❑7 [omments/Plscre ancy: Chain of Custody Present? ❑4� es []No❑NIA i. Samples Arrived within Hold Time? ice's No ❑N/A 2. Short Hold Time Analysis (02 hr.)? Dyes I }No ❑N!A 3. Rush Turn Around Time Requested? ❑Yes Na [:]N/A 4, Sufficient Volume? D Yes []No ❑N/A 5. Correct Containers Used? ❑'res - []No ❑N/A Pace Containers Used? ❑des []No ❑N/A 6, Containers Intact? Yes r]No -[—]N/A 7. Dissolved analysis: Samples Field Filtered? ❑Y ❑No FJWIA es No g. Mal Heads ace in VOA Vials (>5-6mm)? ❑Yes DlQ— NIA 10. Trip Blank Present? (—]Yes No []N/A / Trip Blank Custody Seals Present? Yes ❑No ❑N/FC 11. COMMENTS/SAMPLE DISCREPANCY Field Clata Required? ❑Yes []NO a O &fir CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Datenme: Lot ID of spfit containers: Date: Date: Page 49 of 54 Document Name: Sample Cendltlan viacin Recel AnaryticalJ Document No.: F•GAR•C5.033-Rev.06 Document Revised: February 7, 2018 Page Iof2 Issuing Authority: Pace Carolinas Quality Office *Check rraarlc tap half of box if pig and/or dechlorination is verified and wlthin the acceptance range for preservation Samples. Exceptions: VOA, Coliform, TOC, 0J and Grease, DRO/2015 (water) DOC, LLNg ,,*Bottom half of box is to Ust nun, bar of battle U m �- J a 'a y W ? 2 v Y e = V V Z y ? v y L e V D N v x Q ry v x ry7 U x 0 r+ n a x 6i z C V L v � � 2 v O. e m v ri m 'a a E E a 2 E v i1 E Q- a a E E E 4 a m m m m m m 3 a 1 2 3 4 5 6 h I I I N N"1\"�-I\"k I 9 10 11 17 Project 9 rWO : 92483733 PM: AMB Due Date: 07/13/20 CLIENT: 92-11unicipal z — z = V 2 a z T v a E V) 6 ? y .Ya. v C O N 2 A m a E E v ttD LLO a a I y 0. Q Q = m a E O Q Q_ z _ Z d a -+ E N a LD a 4 Z a 4 O 7 O in z Q m 4 Z Z Q N a a Q Q o Q O 5 > E E E cat c> UI Q LD 7 7 O _ ? 2 Y ut O a a L ro y ka O � 7 > �° I Z a E ^n 6 a VI m r E o N n. n n q ry r9 a E ry m 4 y C E c ¢ ; of E a o a 7 > n a E c C] pH Adjustment Loge for Preserved Samples Sample ID Type of FfeSeFVat0Je pH upon rece;pt Date preservation adlusted Time preservation Amount of Preservative Lot 9 adjusted added Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a Copy of this farm will be s:ne tothe North Carollna DEHNR Certification Office (i.e. out of hold, incorrect preservative, out of temp, Incorrect containers. Page 50 of 54 N m 4 0 M r m D � F C a D m 3 m n m m 3 z 3 3 0 N o v Z r r Z m • c m TEMP in C Received on Ice (YIN) usl-oTy— Sealed Cooler (YIN) Samples Intact (YIN) 9 0 L 0 3 m y N 1 0 m m m L m ro 1V 00 O rO 1:1 1 8 18 s f7i A .• W ITEM # NO V u b 0 V 0 T a w 3 c ^ °; r 0 m J3 K ❑ C m ya z� Otero ��� o �{ 5 7dATRl%CODE (sea valkd codes to left) SAMPLE TYPE (G=GRAB C=COMP) O m N n O m m m z O 7:! IT SAMPLETEMP AT COLLECTION S OF CONTAINERS Unpreserved H2SO4 HNO3 c HCI { NaOH a Na2S203 d a Methanol Other Analyses Test ` VCCs APP I Metals App I Turbidity VOCs App II Metals APP II Residual Chlorine (YIN) 4� v v mG a ti F N a a n z a y n n m - ❑ � � m � „ f s ]Shy a Ua m w 3 m x ,p n n' In T _> a O C O N 1 -o a C'I a F N m ia' m °' 3 1° o^ o �c C v v O H m ,^ o 5 0 3 � rn 41 - o s n 1° f° w ° m ? � 1 °D � C g Cl n M `C or L z �rt P. ' n n m m (D � 6 s CD 3 N (p r-h 3 v t �O CT 0 o 3 - rU .� N r-q- 4 N n c v � K o O � c m m >v Z r O n R a o n N D v Page 51 of 54 Document Name: Document Revised: February 7, 2018 Sample Condition Upon Retelpt(SCUR) Page 1 of 2 5a'ce*alytical'Document No.: tssuingAuthority: F-CAR-CS•033-Rev.05 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑� Raleigh[] Mechanicsville❑ Sample Condition Client Name: WO# : 92483783 . , PrsJect #: n -I P) / Courier: ❑Fed Ex ❑UPS ❑U5PS ❑Client 11111111 IN����1I�����❑ Commercial /ZPace ❑ Other: - 92483783 Custody Seal Present? Dyes Dqo' Seals Intact? ❑Yes DiVo' -1 G. G 6_18 Date/lnitlaisPerson ExaminingContents! -- ---- Packing Materfal: ❑Hubble Wrap U/ bubble Bags ❑None ❑ Other BiologicaI Tissue Frozen Thermometer Elves ❑No ❑N¢ 92TO61 Type of Ice: ❑Vtlet❑Blue ❑None IR Gun ID: �— Cooler Temp (°C): L Correction Factor: Add/Subtract ("C) +4. j Temp should be above freezing to VC Cooler Temp Corrected {°Gj: L ❑Samples out of temp criteria. Samples on ace, cooling process has begun USDA Regulated Soil (d/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC )check maps)? Did samples originate from a foreign source linternatio fl ...._ I—y, nli,1., inciudingHawall and Puerto Rico)? []Yes❑N6 Chain of Custody Present? Samples Arrived within Hold Time? Short Hold Ttme Analysis (<72 hr.)? Rush Turn Around Time Requested? Sufficient Volume? Correct Containers Used? -Pace Containers Used? Containers Intact? Dissolved analysis: Samples Field Filtered? Includes Date/Time/ID/Analysis Mat Heads ace in VOA Vials (>S-6mm)? Trip Blank Present? Trio Blank Custodv Seals Present? ]No ❑N/A I. No ❑N/A 2, U1V0 ❑NIA 3. No ❑NJA 4. ONO ❑NJA 5. ONO ❑NJA fi. [-]NO ❑NJA ❑Na ❑N/A 1 7. 11Nn r-1/A 1 g. ❑Yes ❑No— []N/A 1 10. ❑Yes ONO ❑N/A i11. i Flyes ❑No ❑NIA"I COMMENTS/SAMPLE DISCREPANCY field Data Required? ❑Yes ❑No ,5 () r ""I I L � - , �r_ CLIENT NOTOCATION/RESOLUTION Person contacted: Project Manager SCURF Review: Av � --, Project Manager SRF Review: Date/Time: Lot ID of split centalners: Date: . ��. o Z' c' Date; 76i-1-0.2 C) Page 52 of 54 Document Name: 5arnple Conclltlan Upon Recell Analytical Document No.: F-CAR-CS.033-Rev.06 Check mark top hEilf of b0u if PH and/or deehlorination Is verified and tjvlthin the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRQ/8015 (water) DOC, LLHg *uBottoirri half of box is to list number of bottle E�oament Revised: February 7, 2018 Page Iof2 Issuing Authority: Pace Caroilnas Quality Office Project 'WO# : 92483783 PM: AMB Due Date_ 07/13/20 CLIENT: 92-Municipal = - Z y n C D a E �n 7 IT a.m z nl a c 7 a E o 3 M Q. Z m q c U A a E o rd 2 a v ¢ r: � a y a •+ m N V O N = o E vt ry �+SI A m N v O Z x Y '9 a G A N 6 m A Z ILx 4 Z J E ,n d m N ^ p N 2 9 a E ch A ep a c r 0 dE a - Z y n C D `m E ¢ 0 _ l'J ¢ '� a u x m E ¢ = U 6 W a c `m Q E o n ry ,i 0 Q N V x ON N x `+ a E q P - N 0 q '-'� V S a Q N x `v n 4 v T ) Q y. U S Z y E q E N 4 m t7 a m 4 2 r u O E 0 Oyi `V o q Z ry o SO J E 0 4 T U' 7 Q Z n c 0 E o T a=1 t7 7 4 Z p a m 0 E a , 4 v4i O 2 N u�i u a n "s �d x Q ? H m \ a m 5 � > Z l/ n In Ni N s 2 l.� °- ^ E cl M N H _ O N Z m a E rV ran m ? C 9 E ¢ of o 3 G q .5 o c n E o ry a 'A ] z �? Z Cl c 7 ¢ E a v 7 m II / 1 2 3 ) 1 4 5 — pH Adjustment Log for Preserved Samples Sample I I Type of Preservative pH upon receipt Date preservation adiusted Tlme preservation— Amount of Preservative — Lot 0 adiustmad edded Note: whenever there Is a discrepancy affecting Nerth Carolina compliance samples, a copy of this farm uili be;int to?he NorthCarollna OEHNR Certification Office il.e• out cf hold, Incorrect preservative, out of temp, Incorrect contalners. Page 53 of 54 WA) r }ael�l ry Sald We$ F._ 2 N!A f 0 Jeloao ^r palees p h olun V v ¢ - m N u° paniaaad O J z (NIA) eulJolyO lenpgsaa —y v 0 u!cr dW31 dJ a: V m tB F d lu 1i a rl N N R II ddVSleleW x a m 43 � II ddv SOOA X hyp!gJnl x .. x - -x - --x d w 1 ddV splayy X x x x x H R z a I o I ddH sOO/t x x x x x `—y° U 7 LL Nl.l ;sal sasl({euy a a _° eyyO r d cue a I 44 W u COZSZeN c y ¢ m yZL HOLN b `v N IOH ° m N EONH d m 0- E 60SZH z ui .v 'O panJasoiduH U S O O a` a w - 0 u a d y v F 1 u N ¢ G01 4 a M a Sa3 NIV1N00 A p - NOU0311001VdVi3131dVOVS `� W uLJ FW- !`y- (� 4 m w � a G �' FA N • O (¢1J 2 z a `° w w g ° w cc W 6 Z F U O z a i 0 ¢ a h U C� ~ - LL N a a w C O w m y Y ED m r 3 U A w {dW00=0 9tli1`J=0) 3dA131dWb5 L N O On t $ tt 5 w {yal of sapoa p�len 6es) 3000 XITJIV6Y _ ` r ° ° In a a U d� a so;�amo3ao" ° V) w 2 7 Q y C w R 3 W 6 A O l J d�� 4 0 c a z o E F F- aa, U q LU 0 A M Q u U a a ¢ a z # w31� r� r v r >r, m �-• ti r oo m r o N N N N eo N v N N .�o ; Page 54, Lo C U 4 U' )f 54 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 July 02, 2020 Mr. Jonathan Pfohl Municipal Engineering Services 68 Shipwash Dr. Garner, NC 27529 RE: Project: Surry Blanks Pace Project No.: 92483826 Dear Mr. Pfohl: Enclosed are the analytical results for sample(s) received by the laboratory on June 26, 2020. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Steven R. Gandy, Municipal Engineering Services Co. REPORT OF LABORATORY ANALYSIS r e This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 20 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Surry Blanks Pace Project No.: 92483826 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 20 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: Surry Blanks Pace Project No.: 92483826 Lab ID Sample ID Matrix Date Collected Date Received 92483826001 92483826002 EB FIB Water Water 06/25/2015:50 06/25/2015:52 06/26/20 14:41 06/26/20 14:41 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 20 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Surry Blanks Pace Project No.: 92483826 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92483826001 EB EPA 6010D SH1 14 PASI-A EPA 6020E BG2 1 PASI-A EPA 8260D CL 51 PASI-C 92483826002 FIB EPA 6010D SH1 14 PASI-A EPA 6020E BG2 1 PASI-A EPA 8260D CL 51 PASI-C PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 20 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Blanks Pace Project No.: 92483826 Sample: EB Lab ID: 92483826001 Collected: 06/25/20 15:50 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 06/30/20 00:35 07/01/20 01:02 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 01:02 7440-38-2 Barium ND ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 01:02 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 06/30/20 00:35 07/01/20 01:02 7440-41-7 Cadmium 0.47J ug/L 1.0 0.40 1 06/30/20 00:35 07/01/20 01:02 7440-43-9 Chromium ND ug/L 5.0 3.7 1 06/30/20 00:35 07/01/20 01:02 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 06/30/20 00:35 07/01/20 01:02 7440-48-4 Copper ND ug/L 5.0 4.3 1 06/30/20 00:35 07/01/20 01:02 7440-50-8 Lead ND ug/L 5.0 4.5 1 06/30/20 00:35 07/01/20 01:02 7439-92-1 Nickel ND ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 01:02 7440-02-0 Selenium ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 01:02 7782-49-2 Silver ND ug/L 5.0 2.5 1 06/30/20 00:35 07/01/20 01:02 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 06/30/20 00:35 07/01/20 01:02 7440-62-2 Zinc ND ug/L 10.0 9.5 1 06/30/20 00:35 07/01/20 01:02 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium ND ug/L 0.10 0.050 1 06/30/20 00:13 06/30/20 14:38 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 07/02/20 04:11 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 07/02/20 04:11 107-13-1 Benzene ND ug/L 1.0 0.15 1 07/02/20 04:11 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 07/02/20 04:11 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 07/02/20 04:11 75-27-4 Bromoform ND ug/L 1.0 0.62 1 07/02/20 04:11 75-25-2 Bromomethane ND ug/L 2.0 0.62 1 07/02/20 04:11 74-83-9 IK 2-Butanone (MEK) ND ug/L 5.0 3.3 1 07/02/20 04:11 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 07/02/20 04:11 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 07/02/20 04:11 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 07/02/20 04:11 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 07/02/20 04:11 75-00-3 Chloroform ND ug/L 5.0 2.3 1 07/02/20 04:11 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 07/02/20 04:11 74-87-3 v2 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 07/02/20 04:11 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 07/02/20 04:11 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 07/02/20 04:11 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 07/02/20 04:11 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.29 1 07/02/20 04:11 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 07/02/20 04:11 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 07/02/20 04:11 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.27 1 07/02/20 04:11 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.34 1 07/02/20 04:11 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 07/02/20 04:11 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 20 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Blanks Pace Project No.: 92483826 Sample: EB Lab ID: 92483826001 Collected: 06/25/20 15:50 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene 1,4-Dioxane (p-Dioxane) Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 07/02/2020 04:47 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.29 1 07/02/20 04:11 156-59-2 ND ug/L 1.0 0.25 1 07/02/20 04:11 156-60-5 ND ug/L 1.0 0.19 1 07/02/20 04:11 78-87-5 ND ug/L 1.0 0.30 1 07/02/20 04:11 10061-01-5 ND ug/L 1.0 0.31 1 07/02/20 04:11 10061-02-6 ND ug/L 150 56.2 1 07/02/20 04:11 123-91-1 ND ug/L 1.0 0.26 1 07/02/20 04:11 100-41-4 ND ug/L 5.0 0.57 1 07/02/20 04:11 591-78-6 ND ug/L 20.0 12.5 1 07/02/20 04:11 74-88-4 ND ug/L 5.0 3.7 1 07/02/20 04:11 75-09-2 ND ug/L 5.0 4.5 1 07/02/20 04:11 108-10-1 ND ug/L 1.0 0.27 1 07/02/20 04:11 100-42-5 ND ug/L 1.0 0.34 1 07/02/20 04:11 630-20-6 ND ug/L 1.0 0.22 1 07/02/20 04:11 79-34-5 ND ug/L 1.0 0.16 1 07/02/20 04:11 127-18-4 ND ug/L 1.0 0.24 1 07/02/20 04:11 108-88-3 ND ug/L 1.0 0.18 1 07/02/20 04:11 71-55-6 ND ug/L 1.0 0.24 1 07/02/20 04:11 79-00-5 ND ug/L 1.0 0.22 1 07/02/20 04:11 79-01-6 ND ug/L 1.0 0.31 1 07/02/20 04:11 75-69-4 ND ug/L 1.0 0.35 1 07/02/20 04:11 96-18-4 ND ug/L 2.0 1.4 1 07/02/20 04:11 108-05-4 ND ug/L 1.0 0.24 1 07/02/20 04:11 75-01-4 ND ug/L 1.0 0.63 1 07/02/20 04:11 1330-20-7 93 % 70-130 1 07/02/20 04:11 460-00-4 90 % 70-130 1 07/02/20 04:11 17060-07-0 99 % 70-130 1 07/02/20 04:11 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 20 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Blanks Pace Project No.: 92483826 Sample: FIB Lab ID: 92483826002 Collected: 06/25/20 15:52 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 06/30/20 00:35 07/01/20 01:05 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 01:05 7440-38-2 Barium ND ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 01:05 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 06/30/20 00:35 07/01/20 01:05 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 06/30/20 00:35 07/01/20 01:05 7440-43-9 Chromium ND ug/L 5.0 3.7 1 06/30/20 00:35 07/01/20 01:05 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 06/30/20 00:35 07/01/20 01:05 7440-48-4 Copper ND ug/L 5.0 4.3 1 06/30/20 00:35 07/01/20 01:05 7440-50-8 Lead ND ug/L 5.0 4.5 1 06/30/20 00:35 07/01/20 01:05 7439-92-1 Nickel ND ug/L 5.0 3.5 1 06/30/20 00:35 07/01/20 01:05 7440-02-0 Selenium ND ug/L 10.0 4.7 1 06/30/20 00:35 07/01/20 01:05 7782-49-2 Silver ND ug/L 5.0 2.5 1 06/30/20 00:35 07/01/20 01:05 7440-22-4 Vanadium ND ug/L 5.0 3.9 1 06/30/20 00:35 07/01/20 01:05 7440-62-2 Zinc ND ug/L 10.0 9.5 1 06/30/20 00:35 07/01/20 01:05 7440-66-6 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services -Asheville Thallium ND ug/L 0.10 0.050 1 06/30/20 00:13 06/30/20 14:42 7440-28-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 07/02/20 04:29 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 07/02/20 04:29 107-13-1 Benzene ND ug/L 1.0 0.15 1 07/02/20 04:29 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 07/02/20 04:29 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 07/02/20 04:29 75-27-4 Bromoform ND ug/L 1.0 0.62 1 07/02/20 04:29 75-25-2 Bromomethane ND ug/L 2.0 0.62 1 07/02/20 04:29 74-83-9 IK 2-Butanone (MEK) ND ug/L 5.0 3.3 1 07/02/20 04:29 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 07/02/20 04:29 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 07/02/20 04:29 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 07/02/20 04:29 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 07/02/20 04:29 75-00-3 Chloroform ND ug/L 5.0 2.3 1 07/02/20 04:29 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 07/02/20 04:29 74-87-3 v2 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 07/02/20 04:29 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 07/02/20 04:29 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 07/02/20 04:29 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 07/02/20 04:29 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.29 1 07/02/20 04:29 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 07/02/20 04:29 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 07/02/20 04:29 110-57-6 1,1-Dichloroethane ND ug/L 1.0 0.27 1 07/02/20 04:29 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.34 1 07/02/20 04:29 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 07/02/20 04:29 75-35-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 20 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Surry Blanks Pace Project No.: 92483826 Sample: FIB Lab ID: 92483826002 Collected: 06/25/20 15:52 Received: 06/26/20 14:41 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene 1,4-Dioxane (p-Dioxane) Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 07/02/2020 04:47 PM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.29 1 07/02/20 04:29 156-59-2 ND ug/L 1.0 0.25 1 07/02/20 04:29 156-60-5 ND ug/L 1.0 0.19 1 07/02/20 04:29 78-87-5 ND ug/L 1.0 0.30 1 07/02/20 04:29 10061-01-5 ND ug/L 1.0 0.31 1 07/02/20 04:29 10061-02-6 ND ug/L 150 56.2 1 07/02/20 04:29 123-91-1 ND ug/L 1.0 0.26 1 07/02/20 04:29 100-41-4 ND ug/L 5.0 0.57 1 07/02/20 04:29 591-78-6 ND ug/L 20.0 12.5 1 07/02/20 04:29 74-88-4 ND ug/L 5.0 3.7 1 07/02/20 04:29 75-09-2 ND ug/L 5.0 4.5 1 07/02/20 04:29 108-10-1 ND ug/L 1.0 0.27 1 07/02/20 04:29 100-42-5 ND ug/L 1.0 0.34 1 07/02/20 04:29 630-20-6 ND ug/L 1.0 0.22 1 07/02/20 04:29 79-34-5 ND ug/L 1.0 0.16 1 07/02/20 04:29 127-18-4 ND ug/L 1.0 0.24 1 07/02/20 04:29 108-88-3 ND ug/L 1.0 0.18 1 07/02/20 04:29 71-55-6 ND ug/L 1.0 0.24 1 07/02/20 04:29 79-00-5 ND ug/L 1.0 0.22 1 07/02/20 04:29 79-01-6 ND ug/L 1.0 0.31 1 07/02/20 04:29 75-69-4 ND ug/L 1.0 0.35 1 07/02/20 04:29 96-18-4 ND ug/L 2.0 1.4 1 07/02/20 04:29 108-05-4 ND ug/L 1.0 0.24 1 07/02/20 04:29 75-01-4 ND ug/L 1.0 0.63 1 07/02/20 04:29 1330-20-7 95 % 70-130 1 07/02/20 04:29 460-00-4 89 % 70-130 1 07/02/20 04:29 17060-07-0 100 % 70-130 1 07/02/20 04:29 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 20 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Blanks Pace Project No.: 92483826 QC Batch: 550337 Analysis Method: EPA 6010D QC Batch Method: EPA 3010A Analysis Description: 6010 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92483826001, 92483826002 METHOD BLANK: 2926131 Associated Lab Samples: 92483826001, 92483826002 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Antimony ug/L ND 5.0 3.0 06/30/20 23:57 Arsenic ug/L ND 10.0 4.7 06/30/20 23:57 Barium ug/L ND 5.0 3.5 06/30/20 23:57 Beryllium ug/L ND 1.0 0.70 06/30/20 23:57 Cadmium ug/L ND 1.0 0.40 06/30/20 23:57 Chromium ug/L ND 5.0 3.7 07/01/2018:57 Cobalt ug/L ND 5.0 3.6 06/30/20 23:57 Copper ug/L ND 5.0 4.3 06/30/20 23:57 Lead ug/L ND 5.0 4.5 06/30/20 23:57 Nickel ug/L ND 5.0 3.5 06/30/20 23:57 Selenium ug/L ND 10.0 4.7 06/30/20 23:57 Silver ug/L ND 5.0 2.5 06/30/20 23:57 Vanadium ug/L ND 5.0 3.9 07/01/2018:57 Zinc ug/L ND 10.0 9.5 06/30/20 23:57 LABORATORY CONTROL SAMPLE: Parameter 2926132 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 489 98 80-120 Arsenic ug/L 500 492 98 80-120 Barium ug/L 500 484 97 80-120 Beryllium ug/L 500 470 94 80-120 Cadmium ug/L 500 472 94 80-120 Chromium ug/L 500 495 99 80-120 Cobalt ug/L 500 473 95 80-120 Copper ug/L 500 491 98 80-120 Lead ug/L 500 478 96 80-120 Nickel ug/L 500 472 94 80-120 Selenium ug/L 500 481 96 80-120 Silver ug/L 250 225 90 80-120 Vanadium ug/L 500 499 100 80-120 Zinc ug/L 500 442 88 80-120 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 20 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Pace Project No.: Surry Blanks 92483826 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2926133 2926134 MS MSD 92483926003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 512 507 102 101 75-125 1 20 Arsenic ug/L ND 500 500 524 517 105 103 75-125 1 20 Barium ug/L 60.9 500 500 560 550 100 98 75-125 2 20 Beryllium ug/L ND 500 500 493 476 99 95 75-125 4 20 Cadmium ug/L ND 500 500 504 495 101 99 75-125 2 20 Chromium ug/L ND 500 500 515 ND 103 0 75-125 20 M1 Cobalt ug/L ND 500 500 495 483 99 97 75-125 2 20 Copper ug/L ND 500 500 500 496 100 99 75-125 1 20 Lead ug/L ND 500 500 494 488 99 98 75-125 1 20 Nickel ug/L ND 500 500 494 482 98 96 75-125 2 20 Selenium ug/L ND 500 500 533 530 107 106 75-125 1 20 Silver ug/L ND 250 250 237 232 95 93 75-125 2 20 Vanadium ug/L ND 500 500 513 ND 103 0 75-125 20 M1 Zinc ug/L ND 500 500 490 469 97 93 75-125 4 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 20 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Blanks Pace Project No.: 92483826 QC Batch: 550340 Analysis Method: EPA 6020B QC Batch Method: EPA 3010A Analysis Description: 6020 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92483826001, 92483826002 METHOD BLANK: 2926143 Matrix: Water Associated Lab Samples: 92483826001, 92483826002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Thallium ug/L ND 0.10 0.050 06/30/2013:04 LABORATORY CONTROL SAMPLE: 2926144 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Thallium ug/L 10 10.1 101 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2926145 2926146 MS MSD 92483822002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Thallium ug/L ND 10 10 10.1 10.3 100 102 75-125 2 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 20 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Blanks Pace Project No.: 92483826 QC Batch: 550875 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92483826001, 92483826002 METHOD BLANK: 2928332 Associated Lab Samples: 92483826001, 92483826002 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.34 07/02/20 00:15 1,1,1-Trichloroethane ug/L ND 1.0 0.18 07/02/20 00:15 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 07/02/20 00:15 1,1,2-Trichloroethane ug/L ND 1.0 0.24 07/02/20 00:15 1,1-Dichloroethane ug/L ND 1.0 0.27 07/02/20 00:15 1,1-Dichloroethene ug/L ND 1.0 0.24 07/02/20 00:15 1,2,3-Trichloropropane ug/L ND 1.0 0.35 07/02/20 00:15 1,2-Dibromo-3-chloropropane ug/L ND 5.0 0.26 07/02/20 00:15 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.26 07/02/20 00:15 1,2-Dichlorobenzene ug/L ND 1.0 0.29 07/02/20 00:15 1,2-Dichloroethane ug/L ND 1.0 0.34 07/02/20 00:15 1,2-Dichloropropane ug/L ND 1.0 0.19 07/02/20 00:15 1,4-Dichlorobenzene ug/L ND 1.0 0.26 07/02/20 00:15 1,4-Dioxane (p-Dioxane) ug/L ND 150 56.2 07/02/20 00:15 2-Butanone (MEK) ug/L ND 5.0 3.3 07/02/20 00:15 2-Hexanone ug/L ND 5.0 0.57 07/02/20 00:15 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 4.5 07/02/20 00:15 Acetone ug/L ND 25.0 6.2 07/02/20 00:15 Acrylonitrile ug/L ND 10.0 0.90 07/02/20 00:15 Benzene ug/L ND 1.0 0.15 07/02/20 00:15 Bromochloromethane ug/L ND 1.0 0.34 07/02/20 00:15 Bromodichloromethane ug/L ND 1.0 0.26 07/02/20 00:15 Bromoform ug/L ND 1.0 0.62 07/02/20 00:15 Bromomethane ug/L ND 2.0 0.62 07/02/20 00:15 IK Carbon disulfide ug/L ND 2.0 0.40 07/02/20 00:15 Carbon tetrachloride ug/L ND 1.0 0.22 07/02/20 00:15 Chlorobenzene ug/L ND 1.0 0.23 07/02/20 00:15 Chloroethane ug/L ND 1.0 0.49 07/02/20 00:15 Chloroform ug/L ND 5.0 2.3 07/02/20 00:15 Chloromethane ug/L ND 1.0 0.39 07/02/20 00:15 v2 cis-1,2-Dichloroethene ug/L ND 1.0 0.29 07/02/20 00:15 cis-1,3-Dichloropropene ug/L ND 1.0 0.30 07/02/20 00:15 Dibromochloromethane ug/L ND 1.0 0.41 07/02/20 00:15 Dibromomethane ug/L ND 1.0 0.46 07/02/20 00:15 Ethylbenzene ug/L ND 1.0 0.26 07/02/20 00:15 lodomethane ug/L ND 20.0 12.5 07/02/20 00:15 Methylene Chloride ug/L ND 5.0 3.7 07/02/20 00:15 Styrene ug/L ND 1.0 0.27 07/02/20 00:15 Tetrachloroethene ug/L ND 1.0 0.16 07/02/20 00:15 Toluene ug/L ND 1.0 0.24 07/02/20 00:15 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 20 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Blanks Pace Project No.: 92483826 METHOD BLANK: 2928332 Associated Lab Samples: 92483826001, 92483826002 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers trans-1,2-Dichloroethene ug/L ND 1.0 0.25 07/02/20 00:15 trans- 1,3-Dichloropropene ug/L ND 1.0 0.31 07/02/20 00:15 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.54 07/02/20 00:15 Trichloroethene ug/L ND 1.0 0.22 07/02/20 00:15 Trichlorofluoromethane ug/L ND 1.0 0.31 07/02/20 00:15 Vinyl acetate ug/L ND 2.0 1.4 07/02/20 00:15 Vinyl chloride ug/L ND 1.0 0.24 07/02/20 00:15 Xylene (Total) ug/L ND 1.0 0.63 07/02/20 00:15 1,2-Dichloroethane-d4 (S) % 90 70-130 07/02/20 00:15 4-Bromofluorobenzene (S) % 95 70-130 07/02/20 00:15 Toluene-d8 (S) % 99 70-130 07/02/20 00:15 LABORATORY CONTROL SAMPLE: Parameter 2928333 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 53.7 107 70-130 1,1,1-Trichloroethane ug/L 50 47.5 95 70-130 1,1,2,2-Tetrachloroethane ug/L 50 53.5 107 70-130 1,1,2-Trichloroethane ug/L 50 50.2 100 70-130 1,1-Dichloroethane ug/L 50 46.3 93 70-130 1,1-Dichloroethene ug/L 50 49.5 99 70-130 1,2,3-Trichloropropane ug/L 50 52.9 106 70-130 1,2-Dibromo-3-chloropropane ug/L 50 51.0 102 70-130 1,2-Dibromoethane (EDB) ug/L 50 52.3 105 70-130 1,2-Dichlorobenzene ug/L 50 52.2 104 70-130 1,2-Dichloroethane ug/L 50 48.2 96 70-130 1,2-Dichloropropane ug/L 50 50.0 100 70-130 1,4-Dichlorobenzene ug/L 50 51.9 104 70-130 1,4-Dioxane(p-Dioxane) ug/L 1000 1060 106 59-169 2-Butanone (MEK) ug/L 100 88.8 89 64-135 2-Hexanone ug/L 100 103 103 66-135 4-Methyl-2-pentanone (MIBK) ug/L 100 96.9 97 70-130 Acetone ug/L 100 86.1 86 61-157 Acrylonitrile ug/L 250 223 89 61-143 Benzene ug/L 50 49.4 99 70-130 Bromochloromethane ug/L 50 47.3 95 70-130 Bromodichloromethane ug/L 50 46.4 93 70-130 Bromoform ug/L 50 54.0 108 70-130 Bromomethane ug/L 50 43.4 87 38-130lK Carbon disulfide ug/L 50 43.2 86 68-130 Carbon tetrachloride ug/L 50 50.4 101 70-130 Chlorobenzene ug/L 50 51.3 103 70-130 Chloroethane ug/L 50 51.5 103 37-142 Chloroform ug/L 50 47.1 94 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 20 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Blanks Pace Project No.: 92483826 LABORATORY CONTROL SAMPLE: Parameter 2928333 Units Spike Conc. LCS LCS Result % Rec Chloromethane ug/L 50 33.5 cis-1,2-Dichloroethene ug/L 50 47.0 cis-1,3-Dichloropropene ug/L 50 51.7 Dibromochloromethane ug/L 50 53.5 Dibromomethane ug/L 50 51.2 Ethylbenzene ug/L 50 51.3 lodomethane ug/L 100 77.6 Methylene Chloride ug/L 50 46.5 Styrene ug/L 50 54.7 Tetrachloroethene ug/L 50 50.4 Toluene ug/L 50 48.4 trans-1,2-Dichloroethene ug/L 50 47.7 trans- 1,3-Dichloropropene ug/L 50 50.8 trans-1,4-Dichloro-2-butene ug/L 50 50.2 Trichloroethene ug/L 50 51.9 Trichlorofluoromethane ug/L 50 45.5 Vinyl acetate ug/L 100 94.3 Vinyl chloride ug/L 50 40.7 Xylene (Total) ug/L 150 156 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % % Rec Limits Qualifiers 67 48-130 v3 94 70-130 103 70-130 107 70-130 102 70-130 103 70-130 78 40-130 93 67-132 109 70-130 101 69-130 97 70-130 95 70-130 102 70-130 100 35-189 104 70-130 91 63-130 94 55-143 81 70-131 104 70-130 92 70-130 104 70-130 96 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2928334 MS 92483822003 Spike Parameter Units Result Conc. MSD Spike Conc. 2928335 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 21.2 20.9 106 105 73-134 1 30 1,1,1-Trichloroethane ug/L ND 20 20 24.0 23.9 120 119 82-143 1 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 23.4 23.3 117 116 70-136 1 30 1,1,2-Trichloroethane ug/L ND 20 20 21.9 21.7 109 108 70-135 1 30 1,1-Dichloroethane ug/L ND 20 20 25.8 25.6 129 128 70-139 1 30 1,1-Dichloroethene ug/L ND 20 20 26.5 26.4 132 132 70-154 0 30 1,2,3-Trichloropropane ug/L ND 20 20 22.5 22.9 112 115 71-137 2 30 1,2-Dibromo-3- ug/L ND 20 20 20.6 20.4 103 102 65-134 1 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 22.6 22.6 113 113 70-137 0 30 1,2-Dichlorobenzene ug/L ND 20 20 23.0 23.0 115 115 70-133 0 30 1,2-Dichloroethane ug/L ND 20 20 24.4 24.4 122 122 70-137 0 30 1,2-Dichloropropane ug/L ND 20 20 24.1 24.1 121 121 70-140 0 30 1,4-Dichlorobenzene ug/L ND 20 20 22.5 22.4 112 112 70-133 0 30 1,4-Dioxane (p-Dioxane) ug/L ND 400 400 479 485 120 121 53-168 1 30 2-Butanone (MEK) ug/L ND 40 40 53.2 51.9 133 130 60-139 2 30 2-Hexanone ug/L ND 40 40 48.1 47.5 120 119 65-138 1 30 4-Methyl-2-pentanone ug/L ND 40 40 46.4 45.8 116 114 65-135 1 30 (MIBK) Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 20 lV11.1 Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Surry Blanks Pace Project No.: 92483826 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2928334 2928335 MS MSD 92483822003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Acetone ug/L ND 40 40 56.4 54.7 141 137 60-148 3 30 v1 Acrylonitrile ug/L ND 100 100 123 126 123 126 64-147 2 30 Benzene ug/L ND 20 20 23.3 23.4 117 117 70-151 0 30 Bromochloromethane ug/L ND 20 20 23.7 23.8 118 119 70-141 0 30 Bromodichloromethane ug/L ND 20 20 19.3 19.6 97 98 70-138 2 30 Bromoform ug/L ND 20 20 18.2 18.2 91 91 63-130 0 30 Bromomethane ug/L ND 20 20 28.5 28.8 142 144 15-152 1 30 Carbon disulfide ug/L ND 20 20 25.9 25.8 129 129 69-149 1 30 Carbon tetrachloride ug/L ND 20 20 20.9 21.3 104 106 70-143 2 30 Chlorobenzene ug/L ND 20 20 22.5 22.7 112 113 70-138 1 30 Chloroethane ug/L ND 20 20 38.1 37.4 190 187 52-163 2 30 IK,IL, M1,v1 Chloroform ug/L ND 20 20 23.8 23.6 119 118 70-139 1 30 Chloromethane ug/L ND 20 20 24.4 24.6 122 123 41-139 1 30 cis-1,2-Dichloroethene ug/L ND 20 20 25.0 25.0 125 125 70-141 0 30 cis-1,3-Dichloropropene ug/L ND 20 20 22.6 22.6 113 113 70-137 0 30 Dibromochloromethane ug/L ND 20 20 20.4 20.3 102 101 70-134 1 30 Dibromomethane ug/L ND 20 20 20.5 20.4 103 102 70-138 1 30 Ethylbenzene ug/L ND 20 20 22.8 22.9 114 115 66-153 0 30 lodomethane ug/L ND 40 40 28.6 28.0 71 70 20-138 2 30 v3 Methylene Chloride ug/L ND 20 20 25.3 25.5 126 127 42-159 1 30 Styrene ug/L ND 20 20 22.8 22.5 114 113 70-135 1 30 Tetrachloroethene ug/L ND 20 20 20.7 21.2 103 106 59-143 3 30 Toluene ug/L ND 20 20 22.4 22.5 112 112 59-148 0 30 trans-1,2-Dichloroethene ug/L ND 20 20 26.2 26.4 131 132 70-146 1 30 trans-1,3-Dichloropropene ug/L ND 20 20 21.7 21.8 108 109 70-135 0 30 trans-1,4-Dichloro-2-butene ug/L ND 20 20 17.7 17.8 88 89 47-135 1 30 Trichloroethene ug/L ND 20 20 22.1 22.3 110 111 70-147 1 30 Trichlorofluoromethane ug/L ND 20 20 25.0 25.1 125 125 70-148 0 30 Vinyl acetate ug/L ND 40 40 50.8 49.8 127 125 49-151 2 30 Vinyl chloride ug/L ND 20 20 23.4 23.0 117 115 70-156 2 30 Xylene (Total) ug/L ND 60 60 68.8 69.3 115 115 63-158 1 30 1,2-Dichloroethane-d4 (S) % 115 116 70-130 4-Bromofluorobenzene (S) % 101 101 70-130 Toluene-d8 (S) % 102 103 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 20 Pace Analytical Services, LLC 9800 lCtaac,Analyfical ® Kiney Ave. Suite 100 Huntersville, NC 28078 0788 www.pacelabs.com (704)875-9092 QUALIFIERS Project: Surry Blanks Pace Project No.: 92483826 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. ANALYTE QUALIFIERS IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be considered an estimated value. IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be considered an estimated value. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias. v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/02/2020 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 20 lceAnalyircal www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Surry Blanks Pace Project No.: 92483826 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92483826001 EB EPA 3010A 550337 EPA 6010D 550349 92483826002 FB EPA 3010A 550337 EPA 6010D 550349 92483826001 EB EPA 3010A 550340 EPA 6020B 550353 92483826002 FB EPA 3010A 550340 EPA 6020B 550353 92483826001 EB EPA 8260D 550875 92483826002 FB EPA 8260D 550875 Date: 07/02/2020 04:47 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 17 of 20 Document Name: Document Revised: February 7, 2018 Sample Condition Upon Recelpt(SCUR) Page 1 of 2 �C@A0001 Document No.: Issuing Authority: r F-CAR-CS•033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ �iuntersville Raleigh[:] iVlechanitsdille❑ ConditionSample Client Name: PrQJeet #: WO# :92483826 Upon Receipt n 16, nS-eyvc-_' l! I Courier, ❑F c � []UPS CI USPS other: ❑Client ❑ Commercial a e ❑ 92463826 I 111I 1 Custody Seal Present? Des C i Seats Intact? Des o Zq I (�J T E Enln Contents _ J Pacidng Material: []Bubble Wrap ubble Sags []None ❑ Other Thermometer: 92TQ61 Type of Ice: W-t ❑ewe ❑IR Gun ID: Cooler Temp (°C): I - q %Correction Factor: Add/Subtract CQ +� Cooler Temp Corrected ("C): `� USDA Regulated Soil ( /A, water sample) Did samples originate in a quarantine sane within the United States: CA, NY, or SC )check maps)? Chain of Custady Present? samples Arrived within Hold Time? Short Hold Time Analysis j<72 hr.)? Rush Turn Around Time Requested? Sufficient Volume? Correct Containers Used? -Pace Containers Used? Containers Intact? Dissolved analysis: Samples Field Filtered? Heads ace in VOA Vials (>5-6mm)? Trip Blank Present? Trip Blank Custody Seals Present? COMMENTSISAMPLE DISCREPANCY ]No ❑N/A I 1• N []N/A 2, 3. go❑N/ON/A g4. A []No ❑NIA 5. [:]No ❑N/A 6. []No ❑N/A I1Nn l`INGd1 7. DateHnitlalsPerson Nam g Biological Tissue F zen? []yes []No /A []None Temp should be above freezing to VC ❑5arnples out of temptnteria. Samples an Ice, tooling process has begun Did samptes ariginate from a foreign source {internationally, includingNavra" and Puerto Rico!? Oyes []No Lot It) of spit containers: CLIENT NOTIFICATION/RESOLUTION Person contacted_ Project Manager SCURF Review: Project Manager SRF Review: Dateffime: Date: date:. Field Oata Required? []Yes ❑No Page 18 of 20 Document Name: Document Revised: February 7, 2018 aceAnalytical Sample Condition Upon Retelpt(5CUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, ORO/8015 (water) DOC, LLH8 **Bottom half of box is to list number of bottle Project It W4# a 92483826 PM: AMB Due Date: 07/13/20 CLIENT: 92-Municipal Qr z 'O 2 a c E N 0.O. m z Y] Z a c E o m z U Z a c E 7 G. ro a` a a n v a co _ f'V x O vi a E a _ ry v m o a E Y M a co Z a u ¢ a E V 0. coca x O a E V Q. n n e E 4 t7 u Z u a a E a rY 4 ry a E Q .i i7 4 ? v 2 n c E ¢ r E M V' d N v c O E v rl {:1 d _ N V x O N E 4 E M 0 4 ? U i a E o r�i m M 0 d � Z a O > E dl l;7 A ¢ rn NO a O 7 E M l7 7 C 2 7) ¢ O 7 E In s7 ] ? v p CL 2 a O E a) u 4 ? ran o `^ Ji a ° d p > - 9 Y a ° on U' � > ¢ A u E Ln a yr - m in E N N a, 0 _ gg = 2 Z a E Ln M a m z 76 Z c 'M b E 4 E C Q` 4 c o - c z E > T c c a E E D G 1 -� 1 ` I 3 4 5 6 -\ EN I N\\1a �z pH Adjustment tog for Preserved Samples Sample In Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot 0 Nate: Whenever there is a discrepancy affec[Irg North Carolina compilance samples, a copy of this form will be Sent to the North Carolina DFHNR Certification Office (i.e. Out of hold, Incorrect preservative, out of temp, Incorrect contalners. Page 19 of 20 En rn 0 z z A f z m C d D m m M a � n z Ell n n vLO z r m 2 A A D ' C m n TEMP in C Received on Ice (WN) ustL -orb Sealed Cooler (YIN) Samples Intact (YIN) 9 0 z n n 0 m z a ? M m O C to J = m ° W 'O z y G IC lb � C1� w la � ITEM # m m `a zrno'o SC � r m MATRIX CODE (see valid codes to loll) SAMPLE TYPE (G=GRAB C=COMP) . o D � En m D n J M Or m n m Z o K m SAMPLE TEMP AT COLLECTION 9 OF CONTAINERS Unpreserved H2SO4 HNO3 T HCI NaOH m Na2S203 m Methanol Other VOCs APP I Metals App I Residual Chtorine (YIN) S Q Q w 777 0 o 3 va° 3 a . (0 fp - f� N � -• O a n z � � 0 J a D n V ❑ � N � 3 ? � h m 3 m m 5 N O f N �s m � 3 � � o x � n' m N n m = 0A v— �' Z 0 0 C' 1l rn 1 a 0 N N O' 3 j O n K �C: 9 0 m n A d o M at 3 L7 0 m ,z N z r} � C7 n � N v CO a Q 0 m C n 0 a CD so rM n n n c or v CD c E v z o n R D J n a Page 20 of 20 Appendix B Field Sampling Parameter Data Sheet(s) - -- I Jl It"Iliv. NI Project: burry Co Closed C&D and Closed MSWLF-Mt. Airy samplers: .,., Sampling Parameters Water Quality Parameters (Stabilized) Depth Goes Total Depth to Total T Specific CH4 Monitoring Purge Purge Collect Collect to Volume Dry Depth Water Sample Depth Comment DO Temp. TDS `� Point Date Time Date Time Water Purged Durin Measured ORP pH Cond. Gas © (mg/L) (BTOP) Type Expecte s (mg/L) (Gal) as (us/cm Vapors (STOP) g Collection d Purge expected Static MW-1 % �/ I 40 . IW-2 - - - - - - - - 68.08 - - - - - - 100 IW-3 - - - - - - - - 52 - - - - - - IW-4 - - - - - - - - 57 - - - - - - IW-5 - - - - - 64 - - - MW-6 t G, 1b6 31 0 �� , 25 IW-6 - - - - . 14 - - - 56 - - - - - MW-9 ! 46 r MW-11,0 �, 40 MW-121D - - s - - - 100 - - - - - - MW-12S �., i � �r �: 13,�� �� 51 , . `i v 35.78 L, d +. � MW-13. MW-14 �, ' i :O ,� 48.03I oS I ' )7 k .E„„� /'fr 56,98 All, MW-15 �✓ 1r MW-16 �,r',.;� 36,28 - — MW-17'�`i C �� � c�e�<„ 15.32 MW-18 - - - - - - - 18.15- - MW-19 (( / q ry. 17.1 25,64 { I 1 E / ,' „t,. MW-20 ; �' �_ MW-21 C 15,41 `) L SUs 16.04. MW-22l a �I« 1; — ^_f MW 23 222 1pd�i - , SS B=Stainless Steel Baler, D B=Disposable Baler, P=Low flow Pump, PD=Purged Dry VT=Very Turbid, MT=Moderately Turbid, ST=Slightly Turbid, C=Clear NR=No Reading Attempted, NS=No Sample Obtained I` J v' Project: MonitoringCollect Point SW-1 SW-27 SW-4SUM Surry Co Closed Collect Date Time n� Iti s^ C% �V C&D over Closed MSWLF & Active Subtitle D Lined- Mt. Airy (Shared Surface e101 _ Sampling Parameters Goes Total Visual Lab Visual D , Depth Parameters Sample ry, p Flow Gua Durin Measured Comments to be 9 Type as Rats, analyzed for e Ht. 9 Purge expected — 1 _ _ I - - plers: Water Quality Parameters (Stabilized) Specific DO Temp. Hardness ORP pH Cond. (m9/L) © (us/cm (m9/L) q ^µ47��- a CH4 Gas Vapors (ppm) I - _ SWN-1 SWW2 SW-C SS B=Stainless Steel Baler, D B=Disposable Baler, P=Low flow Pump, PD=Purged Dry VT=Very Turbid, MT=Moderately 'iurbid, ST=Slightly Turbid, C=Clear NR=No Reading Attempted, NS=No Sample Obtained