60H_ThomasRd_ClosureReport Addendum_20200107

CLOSURE REPORT ADDENDUM
S. S. GILES/BLYTHE IND. DEMOLITION LANDFILL THOMAS ROAD CHARLOTTE MECKLENBURG COUNTY NORTH CAROLINA
PERMIT NO. 60H-LCID SUMMIT PROJECT NO. 4319.514 Prepared For:
North Carolina Department of Environmental Quality Division of Waste Management 1646 Mail Service Center Raleigh, NC 27699
Prepared By: SUMMIT ENGINEERING, LABORATORY & TESTING, P.C. 3575 Centre Circle
Fort Mill, South Carolina 29715 704-504-1717 January 7, 2020

SUMMIT Engineering, Laboratory & Testing, P.C. 3575 Centre Circle Fort Mill, South Carolina 29715 www.SUMMIT-companies.com Phone: [phone] Fax: [phone] January 7, 2020
Ms. Deborah Aja North Carolina Department of Environmental Quality Division of Waste Management
1646 Mail Service Center Raleigh, NC 27699
Subject: Closure Report Addendum Thomas Road/S.S. Giles Demolition Landfill 14816 Thomas Road Charlotte, Mecklenburg County, North Carolina SUMMIT Project No. 4319.514
Dear Ms. Aja:
SUMMIT ENGINEERING, LABORATORY & TESTING, P.C . (SUMMIT) is pleased to submit the
following Addendum to the March 26, 2019 Closure Report. This report is provided to outline
assessment methodology, sampling collection, analysis and comparison to regulatory values. If you have any questions regarding our addendum, please do not hesitate to call us at [phone].
Sincerely, SUMMIT

Patrick W. Lowery, PG Michael D. Zavislak, NRCC-EAC, CIH, PE Senior Environmental Manager Environmental Department Manager
NC LG No: 2421
SUMMIT’s NC Engineering Firm License No. C-2530
Thomas Road/S.S. Giles Demolition Landfill - Closure Report SUMMIT Project No. 4319.514
Charlotte, North Carolina January 7, 2020

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TABLE OF CONTENTS
1.0 INTRODUCTION .................................................................................................................... 1
1.1. PURPOSE .......................................................................................................................................... 1
1.2. SITE DESCRIPTION ........................................................................................................................ 1
1.3. ASSESSMENT HISTORY ................................................................................................................ 2
2.0 SAMPLING .............................................................................................................................. 3
2.1. SOIL SAMPLING OVERVIEW ....................................................................................................... 3
2.2. SAMPLING EVENT ......................................................................................................................... 3
2.3. SAMPLE LOCATION ....................................................................................................................... 3
2.4. SAMPLE RESULTS .......................................................................................................................... 4
2.5. LABORATORY DATA EVALUATION ........................................................................................... 5
3.0 FINDINGS AND CONCLUSIONS ......................................................................................... 6

TABLES
Table 1: Soil Sample Detection Summary Table FIGURES
Figure 1: Topographic Map Figure 2: Approximate Buried Landscape Debris Map
Figure 3: September Sampling Location Map LABORATORY REPORT
October 16, 2019 Shealy Environmental Services FIELD REPORTS September 27, 2019 Field Report
Thomas Road/S.S. Giles Demolition Landfill - Closure Report SUMMIT Project No. 4319.514
Charlotte, North Carolina January 7, 2020

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1.0 INTRODUCTION
1.1. PURPOSE

SUMMIT prepared this Addendum to the March 26, 2019 Closure Report at the request of North
Carolina Department of Environmental Quality (NCDEQ) Solid Waste section. This work was
conducted to characterize soils excavated and spread on-site as part of the closure of the former
Thomas Road Demolition Landfill (aka S. S. Giles Landfill &Blythe Industries Landfill). Previous
assessments identified Arsenic and Total Chromium detections of soils spread on-site at
concentrations exceeding unrestricted use. Therefore, additional characterization of this material was
required by NCDEQ.

1.2. SITE DESCRIPTION

The subject site is approximately 38.3 acers in area and is consists of Mecklenburg County Tax
Parcels 21703155 and 21703102. According to records, the property contained an inactive former
demolition landfill. File review information obtained from the Mecklenburg County Environmental
Health Department Groundwater and Wastewater Services revealed that the S.S. Giles Landfill is
located at 14816 Thomas Road, the address of the former on-site residence. This landfill was operated
as a demolition landfill by Blythe Industries from January 8, 1985 to December 23, 1987. According
to additional documentation from the file review, the property is on the Mecklenburg County Priority
List (MPL), and as a requirement at MPL sites, the County sampled four (4) water supply wells in the
vicinity of the landfill in February 2003. No contaminants were detected in the nearby water supply
wells. Subsequent Environmental and Geotechnical Assessments of the sites potential dump areas
only encountered surface debris consisting of inert material (concrete, brick, metal).

Century Communities retained SUMMIT to monitor the development of the property and provide
guidance on disposal options for potential wastes if encountered.

Thomas Road/S.S. Giles Demolition Landfill - Closure Report SUMMIT Project No. 4319.514
Charlotte, North Carolina January 7, 2020

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1.3. ASSESSMENT HISTORY

The following assessment reports have been completed for the subject site:

Report: Completed By: Date:
Phase I ESA ATC December 2016 Geotechnical Engineering Evaluation ATC December 2016
Limited Phase II ESA SUMMIT July 2018
Subsurface Geotechnical Investigation SUMMIT July 2018 Refraction Microtremor Testing SUMMIT July 2018
Phase I ESA SUMMIT July 2018
Hand Auger Borings SUMMIT August 2018
Closure Report SUMMIT March 2019

The subject site has been investigated by completion of test pits, mechanical soil borings, hand
auger soil borings, remote sensing technology (ReMi) and temporary monitoring wells. The
December 2016 geotechnical report completed by ATC documented the presence of fill materials
consisting of landscaping debris and organic laden fill soils. This material was encountered in the
western portion of the property within a natural topographic draw. This material was excavated
and spread along the western side slope of the stormwater detention pond detailed in Figure 3 of
this report.

No other buried debris or buried waste materials were encountered during the completion of the
geotechnical investigations. Groundwater sampling conducted in July 2018 did not document
groundwater impacts at the site. Water supply well sampling conducted by Mecklenburg County
of surrounding water wells did not identify groundwater impacts.

Composite sampling conducted in the landscape debris area following the removal of the material
did not document VOC or SVOC impacts. Arsenic and Chromium were reported at concentrations
above unrestricted use (Residential PSRGs). Based on a review of these detections, our review of
previous assessments and SUMMITs experience, those concentrations were believed to be consistent
with naturally occurring background concentrations.

Thomas Road/S.S. Giles Demolition Landfill - Closure Report SUMMIT Project No. 4319.514
Charlotte, North Carolina January 7, 2020

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2.0 SAMPLING
2.1. SOIL SAMPLING OVERVIEW

Soil samples were collected utilizing IHSB and US EPA Field Branches Quality System and Technical
Procedures for composite sampling methodology whereby sub-samples are collected from the
composite sampling zones and combined for analysis. At each composite sample zone, soils were
collected utilizing a decontaminated stainless-steel hand auger. Equal amounts of soil from the
surficial soil intervals from each sub-sample location were collected and mixed with the remaining
sub-sample locations prior to collection in the laboratory vials and jars for SVOC, RCRA Metals and
Hexavalent Chromium. An additional location in the composite sampling zone was collected as a
grab sample and placed in the laboratory vials and jars for VOC analysis. Two (2) composite soil
samples (TR-1 & TR-2) were collected from the side slope of the stormwater pond intending to
analyze the waste material/soils deposited on the slope during development of the property. One (1)
background composite soil sample was collected from the adjacent land area for comparison.

2.2. SAMPLING EVENT

This sampling event was conducted on September 27, 2019 in connection to the material excavated
and placed on the side slope of the stormwater pond. This material consisted of buried landscape
debris and organic laden soils found buried in the western portion of the site. Sampling was conducted
by Patrick Lowery of SUMMIT. A copy of the field reports can be viewed in Appendix III of this
report.

2.3. SAMPLE LOCATION

The landscape debris/waste material was spread along the western side slope of the stormwater pond,
noted as BMP Basin R1. For this sampling event, the area of waste material placement was divided
into 2 zones for composite sampling. Four (4) sub-samples were collected from the 0-1 ft interval of
each zone and mixed for composite sampling in accordance with IHSB guidance. A grab sample was
additionally collected for VOC analysis from each zone. The two (2) samples collected from these
Thomas Road/S.S. Giles Demolition Landfill - Closure Report SUMMIT Project No. 4319.514
Charlotte, North Carolina January 7, 2020

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zones are identified as TR-1 and TR-2 on the attached September Sampling Location Map (Figure 3).
Additionally, one (1) background composite soil sample and grab VOC sample were collected as BG-
1 as detailed on the attached sampling location map.

2.4. SAMPLE RESULTS

Three (3) soil samples were collected and submitted to Shealy Environmental Services, Inc for
analysis of VOCs by EPA Method 8260, SVOCs by EPA Method 8260, RCRA Metals by EPA Method
6010/6020 and Hexavalent Chromium by EPA Method 7199 on October 2, 2019. A summary of
laboratory detections and comparisons to IHSB PSRGs for Unrestricted Use (Residential) can be
found on Table 1.0 in Appendix II of this report. The following summarizes the soil sample
detections:
• No VOC detections were reported for samples TR-1 and TR-2. Low concentrations of
Acetone, 2-Butanone, Methyl Acetate and Toluene were reported in the background samples
BG-1. No detection exceeded the IHSB PSRGs or Protection of Groundwater values.
• Estimated concentrations (J-Values) of Pyrene and Fluoranthene were reported in TR-2 and
BG-1 respectively. No detection exceeded the IHSB PSRGs or Protection of Groundwater
values.
• Arsenic was detected above the IHSB PSRGs for unrestricted use soils in all submitted
samples. Concentrations ranged from 1.0 – 2.3 mg/kg in the three samples. The background
sample collected from the site indicates that the concentrations reported in TR-1 and TR-2 are
consistent with naturally occurring background concentrations.
• Hexavalent Chromium was not reported in submitted samples. Therefore, SUMMIT
concludes that the reported Total Chromium concentrations represent Trivalent Chromium
and do not exceed the IHSB PSRGs or Protection of Groundwater values.

Thomas Road/S.S. Giles Demolition Landfill - Closure Report SUMMIT Project No. 4319.514
Charlotte, North Carolina January 7, 2020

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2.5. LABORATORY DATA EVALUATION

All samples collected were relinquished to a NC certified laboratory for analysis. Composite soil
samples were analyzed for Semi-Volatile Organic Compounds by EPA method 8270, RCRA Metals
by EPA method 6010 and Hexavalent Chromium by EPA method 7199. Grab samples were analyzed
for Volatile Organic Compounds by EPA method 8260.

The laboratory completed validation and verification of laboratory processes and data, and delivered
a laboratory report to SUMMIT. The laboratory report and the QC information provide
documentation of compliance with the industry standards.

In reviewing the laboratory results, several analytes are reported as detections with “J” data qualifiers,
indicating the reported value is an estimate reported within the 95% confidence interval. These
compounds were detected above the MDL, but below the RDL. The MDL is the lowest concentration
at which an analyte can be detected in a sample by the particular laboratory method used. “Detected”
indicates that the analyte can be distinguished from the blank with reasonable certainty. The RDL
(also called practical quantitation limit, or PQL) is approximately five times the MDL or the lower
calibration standard, whichever is higher. Results above the report limit can be distinguished from the
blank and fall within applicable standard curves. For the purposes of this assessment, all “J” qualified
data are considered acceptable for making site management decisions.

Thomas Road/S.S. Giles Demolition Landfill - Closure Report SUMMIT Project No. 4319.514
Charlotte, North Carolina January 7, 2020

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3.0 FINDINGS AND CONCLUSIONS
Buried landscape debris and organic laden soils were encountered during grading of the western
portions of the site. The buried landscape debris consisted of stumps, limbs and organic fill soils.
This material was localized to a topographic draw that was filled with the landscape debris ranging
from 3 to 7 feet in placement depths. This material was excavated and spread on the western side
slope of the constructed BMP Basin R1 (see Figure 3). Confirmation soil sampling was conducted
following the removal of the landscape debris. Arsenic and Chromium (total) were reported at
concentrations above the IHSB-PSRGs for residential soils. At the request of NCDEQ Solid Waste
Division, SUMMIT collected two (2) composite samples of the material spread on the western side
slope of the stormwater basin (BMP Basin R1). An additional background sample was collected
from native undisturbed areas adjacent to the composite sampling zones.

Low concentrations of Arsenic were reported in the soil analysis at concentrations exceeding IHSB
PSRG for unrestricted/residential use. The background sample collected from the site indicates that
the concentrations reported in TR-1 and TR-2 are consistent with naturally occurring background
concentrations and therefore do not represent environmental impacts.

No other detections were reported at concentrations exceeding their respective IHSB PSRGs or
Protection of Groundwater values.

No other debris or waste materials were encountered in site grading. Furthermore, no other buried
debris or buried waste materials were identified in previous geotechnical and environmental
assessments.

SUMMIT concludes that the landscaping debris and organic laden fill soils that were excavated and
spread on the western side slope of onsite BMP Basin R1 do not exceed unrestricted/residential use.
Background arsenic concentrations indicate that reported arsenic detections are within naturally
occurring background concentrations for piedmont soils.

Thomas Road/S.S. Giles Demolition Landfill - Closure Report SUMMIT Project No. 4319.514
Charlotte, North Carolina January 7, 2020

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TABLES
Page 1 of 1
CAS VOC Analyte PSRG-Res
Protection
of GW Result RL Result RL Result RL
67-64-1 Acetone 1.20E+04 2.50E+01 BRL 0.0095 BRL 0.0089 0.39 0.0088
78-93-3 2-Butanone (MEK)5.50E+03 1.70E+01 BRL 0.0047 BRL 0.0044 0.0085 J 0.0044
79-20-9 Methyl Acetate 1.60E+04 1.40E-01 BRL 0.0024 BRL 0.0022 0.0023 J 0.0022
108-88-3 Toluene 9.90E+02 8.30E+00 BRL 0.0024 BRL 0.0022 0.0032 J 0.0022
CAS SVOC Analyte PSRG-Res
Protection
of GW Result RL Result RL Result RL
206-44-0 Fluoranthene 4.80E+02 6.70E+02 BRL 0.00048 BRL 0.0024 0.01 J 0.0044
129-00-0 Pyrene 3.60E+02 4.40E+02 BRL 0.00058 0.005 J 0.0029 BRL 0.0052
CAS Metals PSRG-Res
Protection
of GW Result RL Result RL Result RL
7440-38-2 Arsenic 6.80E-01 5.80E+00 2 0.28 2.3 0.51 1.1 0.25
7440-39-3 Barium 3.10E+03 5.80E+02 96 0.36 120 0.33 47 0.32
7440-47-3 Chromium (III)2.30E+04 3.60E+05 11 0.14 16 0.13 4 0.12
18540-29-9 Chromium (VI)3.10E-01 3.80E+01 BRL 0.24 BRL 0.23 BRL 0.21
7439-92-1 Lead NA 2.70E+02 25 0.74 16 0.46 13 0.22
BRL = Below Reporting Limit J = Estimated Concentration RL = Lab BOLD = Concentration Above Reference Values NT = Not Tested
PSRG - December 2019 Preliminary Soil Remediaiton Goals - Residential Unrestricted Use
Table 1: Soil Sample Detection Summary Table
DEQ Reference Values
TR-1 TR-2 BG-1
All Values in mg/kg 0-1' Composite 0-1' Composite 0-1' Composite
9/27/2019 9/27/2019 9/27/2019
Thomas RoadCharlotte, NC January 7, 2020SUMMIT Project No: 4319.515
Thomas Road/S.S. Giles Demolition Landfill - Closure Report SUMMIT Project No. 4319.514 Charlotte, North Carolina January 7, 2020

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FIGURES
Image Provided By EDR USGS Topographic Maps
Boundaries are approximate
TOPOGRAPHIC MAP
7/16/2018
Charlotte, North Carolina 28278
Thomas Road
Thomas Road Site
Source: Drawn by SUMMITPrepared By\Date: PL/03/19Checked By\Date: MZ/03/19ScaleFigure 2As ShownApproximate Burried Landscape Debris MapThomas Road/S.S. Giles Demolition LandfillCentury Communities14816 Thomas Road7400 Carmel Executive ParkCharlotte, NC Suite 205Charlotte, NC 28226NEst. Location of Buried Landscape DebrisDec. 2016 Geotech
Source: Drawn by SUMMITPrepared By\Date: PL/01/20Checked By\Date: MZ/01/20ScaleFigure 31 inch = 130 feetCharlotte, NC 28226September Sampling Location MapThomas Road/S.S. Giles Demolition LandfillCentury Communities14816 Thomas Road7400 Carmel Executive ParkCharlotte, NCSuite 205KeyLimits of observed buried material Composite Soil Aliquot LocationExcavated Material Placement LocationNotes:Landscape Debris (stumps, limbs, organic soils) excavated to  native soils and placed along the surface of the BMP Basin R1. Composite soil samples collected from the placed material on the western side of Basin R1.TR‐2TR‐1BG‐1N
Thomas Road/S.S. Giles Demolition Landfill - Closure Report SUMMIT Project No. 4319.514 Charlotte, North Carolina January 7, 2020

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LABORATORY REPORT
SHEALY ENVIRONMENTAL SERVICES,INC.
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced,except in its entirety,without the written approval of Shealy Environmental Services,Inc.
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.shealylab.com
Report of Analysis
SUMMIT Engineering,Laboratory &Testing,P.C.
3575 Centre Circle
Fort Mill,SC 28715
Attention:Patrick Lowery
Project Name:Thomas Rd.
Project Number:4319.514
Lot Number:UJ02058
Date Completed:10/15/2019
10/16/2019 9:12 AM
Approved and released by:
Lab Director -Greenville:Lucas Odom
Page 1 of 39
SHEALY ENVIRONMENTAL SERVICES,INC.
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.shealylab.com
Case Narrative
SUMMIT Engineering,Laboratory &Testing,P.C.
Lot Number:UJ02058
This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary
following this Case Narrative.The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt,sample analysis,and data review have been performed in accordance with the most
current approved NELAC standards,the Shealy Environmental Services,Inc.("Shealy")Quality
Assurance Management Plan (QAMP),standard operating procedures (SOPs),and Shealy policies.Any
exceptions to the NELAC standards,the QAMP,SOPs or policies are qualified on the results page or
discussed below.
Where applicable,all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
SVOCs by GC/MS
The following samples were diluted due to appearance or color:UJ02058-002,UJ02058-003.The LOQ
has been elevated to reflect the dilution.In addition,the LCS associated with batch 30821 recovered
Pyridine below method criteria.
RCRA Metals
The following sample was diluted due to the nature of the sample matrix:UJ02058-002.The LOQ has
been elevated to reflect the dilution.
Hexavalent Chromium
Due to suspected matrix interferences the hexavalent chromium insoluble spike was prepared twice and
failed to meet acceptance criteria for sample -001,-002,and -003.All other spiked samples meet
acceptance criteria further indicating matrix interferences.
Page 2 of 39
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: UJ02058

Sample Number Sample ID Matrix Date Sampled Date Received
001 09/27/2019 1000TR-1 Solid 10/02/2019
002 09/27/2019 1030TR-2 Solid 10/02/2019
003 09/27/2019 1100BG-1 Solid 10/02/2019
(3 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 3 of 39
SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: UJ02058

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 TR-1 Solid Arsenic 6010D 2.0 mg/kg 8
001 TR-1 Solid Barium 6010D 96 mg/kg 8
001 TR-1 Solid Chromium 6010D 11 mg/kg 8
001 TR-1 Solid Lead 6010D 25 mg/kg 8
002 TR-2 Solid Pyrene 8270E 5.0 J ug/kg 12
002 TR-2 Solid Arsenic 6010D 2.3 mg/kg 12
002 TR-2 Solid Barium 6010D 120 mg/kg 12
002 TR-2 Solid Chromium 6010D 16 mg/kg 12
002 TR-2 Solid Lead 6010D 16 mg/kg 12
003 BG-1 Solid Acetone 8260D 390 ug/kg 13
003 BG-1 Solid 2-Butanone (MEK)8260D 8.5 J ug/kg 13
003 BG-1 Solid Methyl acetate 8260D 2.3 J ug/kg 13
003 BG-1 Solid Toluene 8260D 3.2 J ug/kg 14
003 BG-1 Solid Fluoranthene 8270E 10 J ug/kg 15
003 BG-1 Solid Arsenic 6010D 1.1 mg/kg 16
003 BG-1 Solid Barium 6010D 47 mg/kg 16
003 BG-1 Solid Chromium 6010D 4.0 mg/kg 16
003 BG-1 Solid Lead 6010D 13 mg/kg 16
(18 detections)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 4 of 39
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
TR-1
UJ02058-001
09/27/2019 1000
10/02/2019
Solid
% Solids:83.0 10/03/2019 0002
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 3060A (Hexavalent C) 7199 1 10/14/2019 1933 SLU 10/14/2019 1202 31594
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 2mg/kg0.241.2
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 10/03/2019 2201 ALR1 30951 5.09
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/kg9.524
Benzene 71-43-2 8260D ND 1ug/kg2.45.9
Bromodichloromethane 75-27-4 8260D ND 1ug/kg2.45.9
Bromoform 75-25-2 8260D ND 1ug/kg2.45.9
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg3.65.9
2-Butanone (MEK)78-93-3 8260D ND 1ug/kg4.724
Carbon disulfide 75-15-0 8260D ND 1ug/kg2.45.9
Carbon tetrachloride 56-23-5 8260D ND 1ug/kg2.45.9
Chlorobenzene 108-90-7 8260D ND 1ug/kg2.45.9
Chloroethane 75-00-3 8260D ND 1ug/kg2.45.9
Chloroform 67-66-3 8260D ND 1ug/kg2.45.9
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg3.65.9
Cyclohexane 110-82-7 8260D ND 1ug/kg2.45.9
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg2.45.9
Dibromochloromethane 124-48-1 8260D ND 1ug/kg2.45.9
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg2.45.9
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg2.45.9
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg2.45.9
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg2.45.9
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg3.65.9
1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg2.45.9
1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg2.45.9
1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg2.45.9
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg2.45.9
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg2.45.9
1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg2.45.9
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg2.45.9
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg2.45.9
Ethylbenzene 100-41-4 8260D ND 1ug/kg2.45.9
2-Hexanone 591-78-6 8260D ND 1ug/kg4.712
Isopropylbenzene 98-82-8 8260D ND 1ug/kg2.45.9
Methyl acetate 79-20-9 8260D ND 1ug/kg2.45.9
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 5 of 39
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
TR-1
UJ02058-001
09/27/2019 1000
10/02/2019
Solid
% Solids:83.0 10/03/2019 0002
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 10/03/2019 2201 ALR1 30951 5.09
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg2.45.9
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg4.712
Methylcyclohexane 108-87-2 8260D ND 1ug/kg2.45.9
Methylene chloride 75-09-2 8260D ND 1ug/kg2.45.9
Styrene 100-42-5 8260D ND 1ug/kg2.45.9
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg2.45.9
Tetrachloroethene 127-18-4 8260D ND 1ug/kg2.45.9
Toluene 108-88-3 8260D ND 1ug/kg2.45.9
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg2.45.9
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg2.45.9
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg2.45.9
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg2.45.9
Trichloroethene 79-01-6 8260D ND 1ug/kg2.45.9
Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg2.45.9
Vinyl chloride 75-01-4 8260D ND 1ug/kg3.65.9
Xylenes (total)1330-20-7 8260D ND 1ug/kg4.712
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 116 47-138
1,2-Dichloroethane-d4 103 53-142
Toluene-d8 119 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 1 10/05/2019 2107 SCD 10/03/2019 1200 30821
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270E ND 1ug/kg0.963.1
Acenaphthylene 208-96-8 8270E ND 1ug/kg1.13.1
Acetophenone 98-86-2 8270E ND 1ug/kg5.815
Anthracene 120-12-7 8270E ND 1ug/kg0.593.1
Atrazine 1912-24-9 8270E ND 1ug/kg5.815
Benzaldehyde 100-52-7 8270E ND 1ug/kg5.815
Benzo(a)anthracene 56-55-3 8270E ND 1ug/kg0.683.1
Benzo(a)pyrene 50-32-8 8270E ND 1ug/kg0.763.1
Benzo(b)fluoranthene 205-99-2 8270E ND 1ug/kg0.583.1
Benzo(g,h,i)perylene 191-24-2 8270E ND 1ug/kg0.753.1
Benzo(k)fluoranthene 207-08-9 8270E ND 1ug/kg0.553.1
1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg5.815
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 6 of 39
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
TR-1
UJ02058-001
09/27/2019 1000
10/02/2019
Solid
% Solids:83.0 10/03/2019 0002
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 1 10/05/2019 2107 SCD 10/03/2019 1200 30821
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg5.815
Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg5.815
Caprolactam 105-60-2 8270E ND 1ug/kg5.815
Carbazole 86-74-8 8270E ND 1ug/kg5.815
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg5.815
4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg5.815
4-Chloroaniline 106-47-8 8270E ND 1ug/kg5.815
bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg5.815
bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg5.815
2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg5.815
2-Chlorophenol 95-57-8 8270E ND 1ug/kg5.815
4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg5.815
Chrysene 218-01-9 8270E ND 1ug/kg0.523.1
Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg0.593.1
Dibenzofuran 132-64-9 8270E ND 1ug/kg5.815
3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg5.815
2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg5.815
Diethylphthalate 84-66-2 8270E ND 1ug/kg5.815
Dimethyl phthalate 131-11-3 8270E ND 1ug/kg8.515
2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg5.815
Di-n-butyl phthalate 84-74-2 8270E ND 1ug/kg5.815
4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg2977
2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg2977
2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg1231
2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg1231
Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg5.815
bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg2977
Fluoranthene 206-44-0 8270E ND 1ug/kg0.483.1
Fluorene 86-73-7 8270E ND 1ug/kg0.663.1
Hexachlorobenzene 118-74-1 8270E ND 1ug/kg5.815
Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg5.815
Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg2977
Hexachloroethane 67-72-1 8270E ND 1ug/kg5.815
Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 1ug/kg1.23.1
Isophorone 78-59-1 8270E ND 1ug/kg5.815
2-Methylnaphthalene 91-57-6 8270E ND 1ug/kg1.13.1
2-Methylphenol 95-48-7 8270E ND 1ug/kg5.815
3+4-Methylphenol 106-44-5 8270E ND 1ug/kg1231
Naphthalene 91-20-3 8270E ND 1ug/kg1.13.1
2-Nitroaniline 88-74-4 8270E ND 1ug/kg1231
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 7 of 39
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
TR-1
UJ02058-001
09/27/2019 1000
10/02/2019
Solid
% Solids:83.0 10/03/2019 0002
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 1 10/05/2019 2107 SCD 10/03/2019 1200 30821
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
3-Nitroaniline 99-09-2 8270E ND 1ug/kg1231
4-Nitroaniline 100-01-6 8270E ND 1ug/kg1231
Nitrobenzene 98-95-3 8270E ND 1ug/kg5.815
2-Nitrophenol 88-75-5 8270E ND 1ug/kg1231
4-Nitrophenol 100-02-7 8270E ND 1ug/kg2977
N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg5.815
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg5.815
Pentachlorophenol 87-86-5 8270E ND 1ug/kg2977
Phenanthrene 85-01-8 8270E ND 1ug/kg0.833.1
Phenol 108-95-2 8270E ND 1ug/kg5.815
Pyrene 129-00-0 8270E ND 1ug/kg0.583.1
Pyridine 110-86-1 8270E ND 1ug/kg5.815
2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg5.815
2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg5.815
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 75 33-102
2-Fluorophenol 80 35-115
Nitrobenzene-d5 77 22-109
Phenol-d5 83 33-122
Terphenyl-d14 90 41-120
2,4,6-Tribromophenol 110 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 10/08/2019 0129 LLL 10/07/2019 0921 30967
1 7471B 7471B 1 10/08/2019 1226 KSH2 10/07/2019 1458 30969
2 3050B 6010D 3 10/08/2019 0902 LLL 10/07/2019 0921 30967
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Arsenic 7440-38-2 6010D 2.0 1mg/kg0.280.83
Barium 7440-39-3 6010D 96 1mg/kg0.361.4
Cadmium 7440-43-9 6010D ND 1mg/kg0.0690.28
Chromium 7440-47-3 6010D 11 1mg/kg0.140.55
Lead 7439-92-1 6010D 25 2mg/kg0.741.7
Mercury 7439-97-6 7471B ND 1mg/kg0.0230.096
Selenium 7782-49-2 6010D ND 1mg/kg0.451.1
Silver 7440-22-4 6010D ND 1mg/kg0.140.55
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 8 of 39
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
TR-2
UJ02058-002
09/27/2019 1030
10/02/2019
Solid
% Solids:85.8 10/03/2019 0002
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 3060A (Hexavalent C) 7199 1 10/14/2019 2012 SLU 10/14/2019 1202 31594
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 2mg/kg0.231.2
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 10/03/2019 2224 ALR1 30951 5.24
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D ND 1ug/kg8.922
Benzene 71-43-2 8260D ND 1ug/kg2.25.6
Bromodichloromethane 75-27-4 8260D ND 1ug/kg2.25.6
Bromoform 75-25-2 8260D ND 1ug/kg2.25.6
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg3.35.6
2-Butanone (MEK)78-93-3 8260D ND 1ug/kg4.422
Carbon disulfide 75-15-0 8260D ND 1ug/kg2.25.6
Carbon tetrachloride 56-23-5 8260D ND 1ug/kg2.25.6
Chlorobenzene 108-90-7 8260D ND 1ug/kg2.25.6
Chloroethane 75-00-3 8260D ND 1ug/kg2.25.6
Chloroform 67-66-3 8260D ND 1ug/kg2.25.6
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg3.35.6
Cyclohexane 110-82-7 8260D ND 1ug/kg2.25.6
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg2.25.6
Dibromochloromethane 124-48-1 8260D ND 1ug/kg2.25.6
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg2.25.6
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg2.25.6
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg2.25.6
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg2.25.6
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg3.35.6
1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg2.25.6
1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg2.25.6
1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg2.25.6
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg2.25.6
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg2.25.6
1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg2.25.6
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg2.25.6
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg2.25.6
Ethylbenzene 100-41-4 8260D ND 1ug/kg2.25.6
2-Hexanone 591-78-6 8260D ND 1ug/kg4.411
Isopropylbenzene 98-82-8 8260D ND 1ug/kg2.25.6
Methyl acetate 79-20-9 8260D ND 1ug/kg2.25.6
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 9 of 39
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
TR-2
UJ02058-002
09/27/2019 1030
10/02/2019
Solid
% Solids:85.8 10/03/2019 0002
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 10/03/2019 2224 ALR1 30951 5.24
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg2.25.6
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg4.411
Methylcyclohexane 108-87-2 8260D ND 1ug/kg2.25.6
Methylene chloride 75-09-2 8260D ND 1ug/kg2.25.6
Styrene 100-42-5 8260D ND 1ug/kg2.25.6
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg2.25.6
Tetrachloroethene 127-18-4 8260D ND 1ug/kg2.25.6
Toluene 108-88-3 8260D ND 1ug/kg2.25.6
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg2.25.6
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg2.25.6
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg2.25.6
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg2.25.6
Trichloroethene 79-01-6 8260D ND 1ug/kg2.25.6
Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg2.25.6
Vinyl chloride 75-01-4 8260D ND 1ug/kg3.35.6
Xylenes (total)1330-20-7 8260D ND 1ug/kg4.411
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 113 47-138
1,2-Dichloroethane-d4 107 53-142
Toluene-d8 115 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 5 10/05/2019 2131 SCD 10/03/2019 1200 30821
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270E ND 1ug/kg4.816
Acenaphthylene 208-96-8 8270E ND 1ug/kg5.516
Acetophenone 98-86-2 8270E ND 1ug/kg2976
Anthracene 120-12-7 8270E ND 1ug/kg3.016
Atrazine 1912-24-9 8270E ND 1ug/kg2976
Benzaldehyde 100-52-7 8270E ND 1ug/kg2976
Benzo(a)anthracene 56-55-3 8270E ND 1ug/kg3.416
Benzo(a)pyrene 50-32-8 8270E ND 1ug/kg3.816
Benzo(b)fluoranthene 205-99-2 8270E ND 1ug/kg2.916
Benzo(g,h,i)perylene 191-24-2 8270E ND 1ug/kg3.816
Benzo(k)fluoranthene 207-08-9 8270E ND 1ug/kg2.816
1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg2976
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 10 of 39
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
TR-2
UJ02058-002
09/27/2019 1030
10/02/2019
Solid
% Solids:85.8 10/03/2019 0002
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 5 10/05/2019 2131 SCD 10/03/2019 1200 30821
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg2976
Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg2976
Caprolactam 105-60-2 8270E ND 1ug/kg2976
Carbazole 86-74-8 8270E ND 1ug/kg2976
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg2976
4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg2976
4-Chloroaniline 106-47-8 8270E ND 1ug/kg2976
bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg2976
bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg2976
2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg2976
2-Chlorophenol 95-57-8 8270E ND 1ug/kg2976
4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg2976
Chrysene 218-01-9 8270E ND 1ug/kg2.616
Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg3.016
Dibenzofuran 132-64-9 8270E ND 1ug/kg2976
3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg2976
2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg2976
Diethylphthalate 84-66-2 8270E ND 1ug/kg2976
Dimethyl phthalate 131-11-3 8270E ND 1ug/kg4376
2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg2976
Di-n-butyl phthalate 84-74-2 8270E ND 1ug/kg2976
4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg150390
2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg150390
2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg58160
2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg58160
Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg2976
bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg150390
Fluoranthene 206-44-0 8270E ND 1ug/kg2.416
Fluorene 86-73-7 8270E ND 1ug/kg3.316
Hexachlorobenzene 118-74-1 8270E ND 1ug/kg2976
Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg2976
Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg150390
Hexachloroethane 67-72-1 8270E ND 1ug/kg2976
Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 1ug/kg5.816
Isophorone 78-59-1 8270E ND 1ug/kg2976
2-Methylnaphthalene 91-57-6 8270E ND 1ug/kg5.816
2-Methylphenol 95-48-7 8270E ND 1ug/kg2976
3+4-Methylphenol 106-44-5 8270E ND 1ug/kg58160
Naphthalene 91-20-3 8270E ND 1ug/kg5.616
2-Nitroaniline 88-74-4 8270E ND 1ug/kg58160
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 11 of 39
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
TR-2
UJ02058-002
09/27/2019 1030
10/02/2019
Solid
% Solids:85.8 10/03/2019 0002
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 5 10/05/2019 2131 SCD 10/03/2019 1200 30821
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
3-Nitroaniline 99-09-2 8270E ND 1ug/kg58160
4-Nitroaniline 100-01-6 8270E ND 1ug/kg58160
Nitrobenzene 98-95-3 8270E ND 1ug/kg2976
2-Nitrophenol 88-75-5 8270E ND 1ug/kg58160
4-Nitrophenol 100-02-7 8270E ND 1ug/kg150390
N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg2976
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg2976
Pentachlorophenol 87-86-5 8270E ND 1ug/kg150390
Phenanthrene 85-01-8 8270E ND 1ug/kg4.216
Phenol 108-95-2 8270E ND 1ug/kg2976
Pyrene 129-00-0 8270E 5.0 J 1ug/kg2.916
Pyridine 110-86-1 8270E ND 1ug/kg2976
2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg2976
2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg2976
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 80 33-102
2-Fluorophenol 70 35-115
Nitrobenzene-d5 80 22-109
Phenol-d5 77 33-122
Terphenyl-d14 91 41-120
2,4,6-Tribromophenol 85 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 10/08/2019 0134 LLL 10/07/2019 0921 30967
1 7471B 7471B 1 10/08/2019 1228 KSH2 10/07/2019 1458 30969
2 3050B 6010D 2 10/08/2019 0907 LLL 10/07/2019 0921 30967
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Arsenic 7440-38-2 6010D 2.3 2mg/kg0.511.5
Barium 7440-39-3 6010D 120 1mg/kg0.331.3
Cadmium 7440-43-9 6010D ND 2mg/kg0.130.51
Chromium 7440-47-3 6010D 16 1mg/kg0.130.51
Lead 7439-92-1 6010D 16 2mg/kg0.461.0
Mercury 7439-97-6 7471B ND 1mg/kg0.0210.085
Selenium 7782-49-2 6010D ND 2mg/kg0.832.0
Silver 7440-22-4 6010D ND 1mg/kg0.130.51
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 12 of 39
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
BG-1
UJ02058-003
09/27/2019 1100
10/02/2019
Solid
% Solids:95.3 10/03/2019 2322
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
3 3060A (Hexavalent C) 7199 1 10/14/2019 2038 SLU 10/14/2019 1202 31594
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 3mg/kg0.211.0
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 10/03/2019 2247 ALR1 30951 4.78
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260D 390 1ug/kg8.822
Benzene 71-43-2 8260D ND 1ug/kg2.25.5
Bromodichloromethane 75-27-4 8260D ND 1ug/kg2.25.5
Bromoform 75-25-2 8260D ND 1ug/kg2.25.5
Bromomethane (Methyl bromide)74-83-9 8260D ND 1ug/kg3.35.5
2-Butanone (MEK)78-93-3 8260D 8.5 J 1ug/kg4.422
Carbon disulfide 75-15-0 8260D ND 1ug/kg2.25.5
Carbon tetrachloride 56-23-5 8260D ND 1ug/kg2.25.5
Chlorobenzene 108-90-7 8260D ND 1ug/kg2.25.5
Chloroethane 75-00-3 8260D ND 1ug/kg2.25.5
Chloroform 67-66-3 8260D ND 1ug/kg2.25.5
Chloromethane (Methyl chloride)74-87-3 8260D ND 1ug/kg3.35.5
Cyclohexane 110-82-7 8260D ND 1ug/kg2.25.5
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260D ND 1ug/kg2.25.5
Dibromochloromethane 124-48-1 8260D ND 1ug/kg2.25.5
1,2-Dibromoethane (EDB)106-93-4 8260D ND 1ug/kg2.25.5
1,2-Dichlorobenzene 95-50-1 8260D ND 1ug/kg2.25.5
1,3-Dichlorobenzene 541-73-1 8260D ND 1ug/kg2.25.5
1,4-Dichlorobenzene 106-46-7 8260D ND 1ug/kg2.25.5
Dichlorodifluoromethane 75-71-8 8260D ND 1ug/kg3.35.5
1,1-Dichloroethane 75-34-3 8260D ND 1ug/kg2.25.5
1,2-Dichloroethane 107-06-2 8260D ND 1ug/kg2.25.5
1,1-Dichloroethene 75-35-4 8260D ND 1ug/kg2.25.5
cis-1,2-Dichloroethene 156-59-2 8260D ND 1ug/kg2.25.5
trans-1,2-Dichloroethene 156-60-5 8260D ND 1ug/kg2.25.5
1,2-Dichloropropane 78-87-5 8260D ND 1ug/kg2.25.5
cis-1,3-Dichloropropene 10061-01-5 8260D ND 1ug/kg2.25.5
trans-1,3-Dichloropropene 10061-02-6 8260D ND 1ug/kg2.25.5
Ethylbenzene 100-41-4 8260D ND 1ug/kg2.25.5
2-Hexanone 591-78-6 8260D ND 1ug/kg4.411
Isopropylbenzene 98-82-8 8260D ND 1ug/kg2.25.5
Methyl acetate 79-20-9 8260D 2.3 J 1ug/kg2.25.5
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
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Shealy Environmental Services, Inc.

Page 13 of 39
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
BG-1
UJ02058-003
09/27/2019 1100
10/02/2019
Solid
% Solids:95.3 10/03/2019 2322
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 10/03/2019 2247 ALR1 30951 4.78
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Methyl tertiary butyl ether (MTBE)1634-04-4 8260D ND 1ug/kg2.25.5
4-Methyl-2-pentanone 108-10-1 8260D ND 1ug/kg4.411
Methylcyclohexane 108-87-2 8260D ND 1ug/kg2.25.5
Methylene chloride 75-09-2 8260D ND 1ug/kg2.25.5
Styrene 100-42-5 8260D ND 1ug/kg2.25.5
1,1,2,2-Tetrachloroethane 79-34-5 8260D ND 1ug/kg2.25.5
Tetrachloroethene 127-18-4 8260D ND 1ug/kg2.25.5
Toluene 108-88-3 8260D 3.2 J 1ug/kg2.25.5
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260D ND 1ug/kg2.25.5
1,2,4-Trichlorobenzene 120-82-1 8260D ND 1ug/kg2.25.5
1,1,1-Trichloroethane 71-55-6 8260D ND 1ug/kg2.25.5
1,1,2-Trichloroethane 79-00-5 8260D ND 1ug/kg2.25.5
Trichloroethene 79-01-6 8260D ND 1ug/kg2.25.5
Trichlorofluoromethane 75-69-4 8260D ND 1ug/kg2.25.5
Vinyl chloride 75-01-4 8260D ND 1ug/kg3.35.5
Xylenes (total)1330-20-7 8260D ND 1ug/kg4.411
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 118 47-138
1,2-Dichloroethane-d4 101 53-142
Toluene-d8 117 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 10 10/05/2019 1611 SCD 10/03/2019 1200 30821
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270E ND 1ug/kg8.728
Acenaphthylene 208-96-8 8270E ND 1ug/kg1028
Acetophenone 98-86-2 8270E ND 1ug/kg52140
Anthracene 120-12-7 8270E ND 1ug/kg5.428
Atrazine 1912-24-9 8270E ND 1ug/kg52140
Benzaldehyde 100-52-7 8270E ND 1ug/kg52140
Benzo(a)anthracene 56-55-3 8270E ND 1ug/kg6.228
Benzo(a)pyrene 50-32-8 8270E ND 1ug/kg6.928
Benzo(b)fluoranthene 205-99-2 8270E ND 1ug/kg5.228
Benzo(g,h,i)perylene 191-24-2 8270E ND 1ug/kg6.828
Benzo(k)fluoranthene 207-08-9 8270E ND 1ug/kg5.028
1,1'-Biphenyl 92-52-4 8270E ND 1ug/kg52140
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 14 of 39
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
BG-1
UJ02058-003
09/27/2019 1100
10/02/2019
Solid
% Solids:95.3 10/03/2019 2322
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 10 10/05/2019 1611 SCD 10/03/2019 1200 30821
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
4-Bromophenyl phenyl ether 101-55-3 8270E ND 1ug/kg52140
Butyl benzyl phthalate 85-68-7 8270E ND 1ug/kg52140
Caprolactam 105-60-2 8270E ND 1ug/kg52140
Carbazole 86-74-8 8270E ND 1ug/kg52140
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270E ND 1ug/kg52140
4-Chloro-3-methyl phenol 59-50-7 8270E ND 1ug/kg52140
4-Chloroaniline 106-47-8 8270E ND 1ug/kg52140
bis(2-Chloroethoxy)methane 111-91-1 8270E ND 1ug/kg52140
bis(2-Chloroethyl)ether 111-44-4 8270E ND 1ug/kg52140
2-Chloronaphthalene 91-58-7 8270E ND 1ug/kg52140
2-Chlorophenol 95-57-8 8270E ND 1ug/kg52140
4-Chlorophenyl phenyl ether 7005-72-3 8270E ND 1ug/kg52140
Chrysene 218-01-9 8270E ND 1ug/kg4.728
Dibenzo(a,h)anthracene 53-70-3 8270E ND 1ug/kg5.428
Dibenzofuran 132-64-9 8270E ND 1ug/kg52140
3,3'-Dichlorobenzidine 91-94-1 8270E ND 1ug/kg52140
2,4-Dichlorophenol 120-83-2 8270E ND 1ug/kg52140
Diethylphthalate 84-66-2 8270E ND 1ug/kg52140
Dimethyl phthalate 131-11-3 8270E ND 1ug/kg78140
2,4-Dimethylphenol 105-67-9 8270E ND 1ug/kg52140
Di-n-butyl phthalate 84-74-2 8270E ND 1ug/kg52140
4,6-Dinitro-2-methylphenol 534-52-1 8270E ND 1ug/kg260700
2,4-Dinitrophenol 51-28-5 8270E ND 1ug/kg260700
2,4-Dinitrotoluene 121-14-2 8270E ND 1ug/kg100280
2,6-Dinitrotoluene 606-20-2 8270E ND 1ug/kg100280
Di-n-octylphthalate 117-84-0 8270E ND 1ug/kg52140
bis(2-Ethylhexyl)phthalate 117-81-7 8270E ND 1ug/kg260700
Fluoranthene 206-44-0 8270E 10 J 1ug/kg4.428
Fluorene 86-73-7 8270E ND 1ug/kg6.028
Hexachlorobenzene 118-74-1 8270E ND 1ug/kg52140
Hexachlorobutadiene 87-68-3 8270E ND 1ug/kg52140
Hexachlorocyclopentadiene 77-47-4 8270E ND 1ug/kg260700
Hexachloroethane 67-72-1 8270E ND 1ug/kg52140
Indeno(1,2,3-c,d)pyrene 193-39-5 8270E ND 1ug/kg1028
Isophorone 78-59-1 8270E ND 1ug/kg52140
2-Methylnaphthalene 91-57-6 8270E ND 1ug/kg1028
2-Methylphenol 95-48-7 8270E ND 1ug/kg52140
3+4-Methylphenol 106-44-5 8270E ND 1ug/kg100280
Naphthalene 91-20-3 8270E ND 1ug/kg1028
2-Nitroaniline 88-74-4 8270E ND 1ug/kg100280
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 15 of 39
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
BG-1
UJ02058-003
09/27/2019 1100
10/02/2019
Solid
% Solids:95.3 10/03/2019 2322
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 10 10/05/2019 1611 SCD 10/03/2019 1200 30821
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
3-Nitroaniline 99-09-2 8270E ND 1ug/kg100280
4-Nitroaniline 100-01-6 8270E ND 1ug/kg100280
Nitrobenzene 98-95-3 8270E ND 1ug/kg52140
2-Nitrophenol 88-75-5 8270E ND 1ug/kg100280
4-Nitrophenol 100-02-7 8270E ND 1ug/kg260700
N-Nitrosodi-n-propylamine 621-64-7 8270E ND 1ug/kg52140
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270E ND 1ug/kg52140
Pentachlorophenol 87-86-5 8270E ND 1ug/kg260700
Phenanthrene 85-01-8 8270E ND 1ug/kg7.628
Phenol 108-95-2 8270E ND 1ug/kg52140
Pyrene 129-00-0 8270E ND 1ug/kg5.228
Pyridine 110-86-1 8270E ND 1ug/kg52140
2,4,5-Trichlorophenol 95-95-4 8270E ND 1ug/kg52140
2,4,6-Trichlorophenol 88-06-2 8270E ND 1ug/kg52140
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 57 33-102
2-Fluorophenol 53 35-115
Nitrobenzene-d5 59 22-109
Phenol-d5 51 33-122
Terphenyl-d14 67 41-120
2,4,6-Tribromophenol 65 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 10/08/2019 0151 LLL 10/07/2019 0921 30967
1 7471B 7471B 1 10/08/2019 1230 KSH2 10/07/2019 1458 30969
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Arsenic 7440-38-2 6010D 1.1 1mg/kg0.250.75
Barium 7440-39-3 6010D 47 1mg/kg0.321.3
Cadmium 7440-43-9 6010D ND 1mg/kg0.0630.25
Chromium 7440-47-3 6010D 4.0 1mg/kg0.120.50
Lead 7439-92-1 6010D 13 1mg/kg0.220.50
Mercury 7439-97-6 7471B ND 1mg/kg0.0210.085
Selenium 7782-49-2 6010D ND 1mg/kg0.411.0
Silver 7440-22-4 6010D ND 1mg/kg0.120.50
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 16 of 39
QC Summary
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Shealy Environmental Services, Inc.

Page 17 of 39
Inorganic non-metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:UQ31594-001
31594 3060A
10/14/2019 1202Analytical Method:7199
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Hexavalent Chromium ND 10/14/2019 19081.0 0.20 mg/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 18 of 39
Inorganic non-metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:UQ31594-002
31594 3060A
10/14/2019 1202Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
Hexavalent Chromium 10 10/14/2019 19201021080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 19 of 39
Inorganic non-metals - MS
Batch:Prep Method:
Prep Date:
Sample ID:UJ02058-001MS
31594 3060A
10/14/2019 1202Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/kg)(mg/kg)(mg/kg)
Hexavalent Chromium 11 10/14/2019 1946901270-130ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 20 of 39
Inorganic non-metals - MSD
Batch:Prep Method:
Prep Date:
Sample ID:UJ02058-001MD
31594 3060A
10/14/2019 1202Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/kg)(mg/kg)(mg/kg)
Hexavalent Chromium 12 10/14/2019 19591011270-13012 20ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 21 of 39
Inorganic non-metals - MS
Batch:Prep Method:
Prep Date:
Sample ID:UJ02058-003MS
31594 3060A
10/14/2019 1202Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/kg)(mg/kg)(mg/kg)
Hexavalent Chromium 1300 10/14/2019 2051N15584070-130ND50
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 22 of 39
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:UQ30951-001
30951 5035
Analytical Method:8260D
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Acetone ND 10/03/2019 2121208.0 ug/kg1
Benzene ND 10/03/2019 21215.0 2.0 ug/kg1
Bromodichloromethane ND 10/03/2019 21215.0 2.0 ug/kg1
Bromoform ND 10/03/2019 21215.0 2.0 ug/kg1
Bromomethane (Methyl bromide)ND 10/03/2019 21215.0 3.0 ug/kg1
2-Butanone (MEK)ND 10/03/2019 2121204.0 ug/kg1
Carbon disulfide ND 10/03/2019 21215.0 2.0 ug/kg1
Carbon tetrachloride ND 10/03/2019 21215.0 2.0 ug/kg1
Chlorobenzene ND 10/03/2019 21215.0 2.0 ug/kg1
Chloroethane ND 10/03/2019 21215.0 2.0 ug/kg1
Chloroform ND 10/03/2019 21215.0 2.0 ug/kg1
Chloromethane (Methyl chloride)ND 10/03/2019 21215.0 3.0 ug/kg1
Cyclohexane ND 10/03/2019 21215.0 2.0 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 10/03/2019 21215.0 2.0 ug/kg1
Dibromochloromethane ND 10/03/2019 21215.0 2.0 ug/kg1
1,2-Dibromoethane (EDB)ND 10/03/2019 21215.0 2.0 ug/kg1
1,2-Dichlorobenzene ND 10/03/2019 21215.0 2.0 ug/kg1
1,3-Dichlorobenzene ND 10/03/2019 21215.0 2.0 ug/kg1
1,4-Dichlorobenzene ND 10/03/2019 21215.0 2.0 ug/kg1
Dichlorodifluoromethane ND 10/03/2019 21215.0 3.0 ug/kg1
1,1-Dichloroethane ND 10/03/2019 21215.0 2.0 ug/kg1
1,2-Dichloroethane ND 10/03/2019 21215.0 2.0 ug/kg1
1,1-Dichloroethene ND 10/03/2019 21215.0 2.0 ug/kg1
cis-1,2-Dichloroethene ND 10/03/2019 21215.0 2.0 ug/kg1
trans-1,2-Dichloroethene ND 10/03/2019 21215.0 2.0 ug/kg1
1,2-Dichloropropane ND 10/03/2019 21215.0 2.0 ug/kg1
cis-1,3-Dichloropropene ND 10/03/2019 21215.0 2.0 ug/kg1
trans-1,3-Dichloropropene ND 10/03/2019 21215.0 2.0 ug/kg1
Ethylbenzene ND 10/03/2019 21215.0 2.0 ug/kg1
2-Hexanone ND 10/03/2019 2121104.0 ug/kg1
Isopropylbenzene ND 10/03/2019 21215.0 2.0 ug/kg1
Methyl acetate ND 10/03/2019 21215.0 2.0 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 10/03/2019 21215.0 2.0 ug/kg1
4-Methyl-2-pentanone ND 10/03/2019 2121104.0 ug/kg1
Methylcyclohexane ND 10/03/2019 21215.0 2.0 ug/kg1
Methylene chloride ND 10/03/2019 21215.0 2.0 ug/kg1
Styrene ND 10/03/2019 21215.0 2.0 ug/kg1
1,1,2,2-Tetrachloroethane ND 10/03/2019 21215.0 2.0 ug/kg1
Tetrachloroethene ND 10/03/2019 21215.0 2.0 ug/kg1
Toluene ND 10/03/2019 21215.0 2.0 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 10/03/2019 21215.0 2.0 ug/kg1
1,2,4-Trichlorobenzene ND 10/03/2019 21215.0 2.0 ug/kg1
1,1,1-Trichloroethane ND 10/03/2019 21215.0 2.0 ug/kg1
1,1,2-Trichloroethane ND 10/03/2019 21215.0 2.0 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Shealy Environmental Services, Inc.

Page 23 of 39
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:UQ30951-001
30951 5035
Analytical Method:8260D
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Trichloroethene ND 10/03/2019 21215.0 2.0 ug/kg1
Trichlorofluoromethane ND 10/03/2019 21215.0 2.0 ug/kg1
Vinyl chloride ND 10/03/2019 21215.0 3.0 ug/kg1
Xylenes (total)ND 10/03/2019 2121104.0 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 118 47-138
1,2-Dichloroethane-d4 103 53-142
Toluene-d8 118 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 24 of 39
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:UQ30951-002
30951 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 92 10/03/2019 20189210060-1401
Benzene 54 10/03/2019 20181075070-1301
Bromodichloromethane 51 10/03/2019 20181025070-1301
Bromoform 49 10/03/2019 2018975070-1301
Bromomethane (Methyl bromide)51 10/03/2019 20181035070-1301
2-Butanone (MEK)90 10/03/2019 20189010060-1401
Carbon disulfide 56 10/03/2019 20181135070-1301
Carbon tetrachloride 56 10/03/2019 20181125070-1301
Chlorobenzene 52 10/03/2019 20181045070-1301
Chloroethane 54 10/03/2019 20181085070-1301
Chloroform 52 10/03/2019 20181045070-1301
Chloromethane (Methyl chloride)54 10/03/2019 20181085060-1401
Cyclohexane 57 10/03/2019 20181155070-1301
1,2-Dibromo-3-chloropropane (DBCP)48 10/03/2019 2018975070-1301
Dibromochloromethane 50 10/03/2019 20181005070-1301
1,2-Dibromoethane (EDB)49 10/03/2019 2018985070-1301
1,2-Dichlorobenzene 52 10/03/2019 20181045070-1301
1,3-Dichlorobenzene 53 10/03/2019 20181055070-1301
1,4-Dichlorobenzene 52 10/03/2019 20181045070-1301
Dichlorodifluoromethane 54 10/03/2019 20181085060-1401
1,1-Dichloroethane 52 10/03/2019 20181055070-1301
1,2-Dichloroethane 49 10/03/2019 2018975070-1301
1,1-Dichloroethene 56 10/03/2019 20181135070-1301
cis-1,2-Dichloroethene 52 10/03/2019 20181055070-1301
trans-1,2-Dichloroethene 55 10/03/2019 20181095070-1301
1,2-Dichloropropane 51 10/03/2019 20181025070-1301
cis-1,3-Dichloropropene 51 10/03/2019 20181025070-1301
trans-1,3-Dichloropropene 50 10/03/2019 20181015070-1301
Ethylbenzene 54 10/03/2019 20181095070-1301
2-Hexanone 94 10/03/2019 20189410070-1301
Isopropylbenzene 55 10/03/2019 20181095070-1301
Methyl acetate 47 10/03/2019 2018935070-1301
Methyl tertiary butyl ether (MTBE)48 10/03/2019 2018975070-1301
4-Methyl-2-pentanone 95 10/03/2019 20189510070-1301
Methylcyclohexane 59 10/03/2019 20181185070-1301
Methylene chloride 51 10/03/2019 20181025070-1301
Styrene 52 10/03/2019 20181055070-1301
1,1,2,2-Tetrachloroethane 48 10/03/2019 2018965070-1301
Tetrachloroethene 56 10/03/2019 20181125070-1301
Toluene 54 10/03/2019 20181085070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 57 10/03/2019 20181145070-1301
1,2,4-Trichlorobenzene 56 10/03/2019 20181125070-1301
1,1,1-Trichloroethane 55 10/03/2019 20181105070-1301
1,1,2-Trichloroethane 49 10/03/2019 2018985070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 25 of 39
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:UQ30951-002
30951 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 54 10/03/2019 20181085070-1301
Trichlorofluoromethane 58 10/03/2019 20181155070-1301
Vinyl chloride 58 10/03/2019 20181155070-1301
Xylenes (total)110 10/03/2019 201810910070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 109 47-138
1,2-Dichloroethane-d4 102 53-142
Toluene-d8 113 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 26 of 39
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:UQ30951-003
30951 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Acetone 130 10/03/2019 2041+127100 60-14033 201
Benzene 52 10/03/2019 20411045070-1303.1 201
Bromodichloromethane 51 10/03/2019 20411025070-1300.26 201
Bromoform 48 10/03/2019 2041975070-1300.15 201
Bromomethane (Methyl bromide)57 10/03/2019 20411145070-13010 201
2-Butanone (MEK)120 10/03/2019 2041+122100 60-14030 201
Carbon disulfide 49 10/03/2019 2041985070-13014 201
Carbon tetrachloride 56 10/03/2019 20411115070-1300.78 201
Chlorobenzene 50 10/03/2019 20411005070-1303.7 201
Chloroethane 62 10/03/2019 20411255070-13014 201
Chloroform 53 10/03/2019 20411065070-1302.0 201
Chloromethane (Methyl chloride)54 10/03/2019 20411085060-1400.013 201
Cyclohexane 58 10/03/2019 20411165070-1300.91 201
1,2-Dibromo-3-chloropropane (DBCP)46 10/03/2019 2041925070-1305.3 201
Dibromochloromethane 50 10/03/2019 2041995070-1301.1 201
1,2-Dibromoethane (EDB)49 10/03/2019 2041975070-1301.1 201
1,2-Dichlorobenzene 50 10/03/2019 20411015070-1303.3 201
1,3-Dichlorobenzene 51 10/03/2019 20411025070-1302.6 201
1,4-Dichlorobenzene 50 10/03/2019 20411015070-1303.7 201
Dichlorodifluoromethane 62 10/03/2019 20411235060-14013 201
1,1-Dichloroethane 52 10/03/2019 20411045070-1300.34 201
1,2-Dichloroethane 47 10/03/2019 2041945070-1303.0 201
1,1-Dichloroethene 63 10/03/2019 20411275070-13012 201
cis-1,2-Dichloroethene 53 10/03/2019 20411055070-1300.32 201
trans-1,2-Dichloroethene 58 10/03/2019 20411165070-1305.6 201
1,2-Dichloropropane 51 10/03/2019 20411015070-1300.64 201
cis-1,3-Dichloropropene 53 10/03/2019 20411065070-1303.2 201
trans-1,3-Dichloropropene 52 10/03/2019 20411035070-1302.2 201
Ethylbenzene 54 10/03/2019 20411075070-1301.1 201
2-Hexanone 110 10/03/2019 204111310070-13018 201
Isopropylbenzene 54 10/03/2019 20411075070-1302.2 201
Methyl acetate 53 10/03/2019 20411065070-13013 201
Methyl tertiary butyl ether (MTBE)47 10/03/2019 2041955070-1301.7 201
4-Methyl-2-pentanone 94 10/03/2019 20419410070-1301.4 201
Methylcyclohexane 57 10/03/2019 20411145070-1303.2 201
Methylene chloride 50 10/03/2019 20411005070-1301.7 201
Styrene 50 10/03/2019 20411015070-1303.8 201
1,1,2,2-Tetrachloroethane 48 10/03/2019 2041955070-1300.54 201
Tetrachloroethene 56 10/03/2019 20411125070-1300.50 201
Toluene 52 10/03/2019 20411055070-1303.1 201
1,1,2-Trichloro-1,2,2-Trifluoroethane 53 10/03/2019 20411075070-1306.3 201
1,2,4-Trichlorobenzene 52 10/03/2019 20411035070-1308.6 201
1,1,1-Trichloroethane 54 10/03/2019 20411085070-1302.0 201
1,1,2-Trichloroethane 48 10/03/2019 2041965070-1301.4 201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 27 of 39
Volatile Organic Compounds by GC/MS - LCSD
Batch:Prep Method:
Sample ID:UQ30951-003
30951 5035
Analytical Method:8260D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/kg)(ug/kg)
Trichloroethene 52 10/03/2019 20411055070-1303.2 201
Trichlorofluoromethane 63 10/03/2019 20411255070-1308.4 201
Vinyl chloride 55 10/03/2019 20411105070-1305.1 201
Xylenes (total)110 10/03/2019 204110610070-1303.2 201
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 116 47-138
1,2-Dichloroethane-d4 98 53-142
Toluene-d8 117 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 28 of 39
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:UQ30821-001
30821 3546
10/03/2019 1200Analytical Method:8270E
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Acenaphthene ND 10/05/2019 14562.7 0.83 ug/kg1
Acenaphthylene ND 10/05/2019 14562.7 0.95 ug/kg1
Acetophenone ND 10/05/2019 1456135.0 ug/kg1
Anthracene ND 10/05/2019 14562.7 0.51 ug/kg1
Atrazine ND 10/05/2019 1456135.0 ug/kg1
Benzaldehyde ND 10/05/2019 1456135.0 ug/kg1
Benzo(a)anthracene ND 10/05/2019 14562.7 0.59 ug/kg1
Benzo(a)pyrene ND 10/05/2019 14562.7 0.66 ug/kg1
Benzo(b)fluoranthene ND 10/05/2019 14562.7 0.50 ug/kg1
Benzo(g,h,i)perylene ND 10/05/2019 14562.7 0.65 ug/kg1
Benzo(k)fluoranthene ND 10/05/2019 14562.7 0.48 ug/kg1
1,1'-Biphenyl ND 10/05/2019 1456135.0 ug/kg1
4-Bromophenyl phenyl ether ND 10/05/2019 1456135.0 ug/kg1
Butyl benzyl phthalate ND 10/05/2019 1456135.0 ug/kg1
Caprolactam ND 10/05/2019 1456135.0 ug/kg1
Carbazole ND 10/05/2019 1456135.0 ug/kg1
bis (2-Chloro-1-methylethyl) ether ND 10/05/2019 1456135.0 ug/kg1
4-Chloro-3-methyl phenol ND 10/05/2019 1456135.0 ug/kg1
4-Chloroaniline ND 10/05/2019 1456135.0 ug/kg1
bis(2-Chloroethoxy)methane ND 10/05/2019 1456135.0 ug/kg1
bis(2-Chloroethyl)ether ND 10/05/2019 1456135.0 ug/kg1
2-Chloronaphthalene ND 10/05/2019 1456135.0 ug/kg1
2-Chlorophenol ND 10/05/2019 1456135.0 ug/kg1
4-Chlorophenyl phenyl ether ND 10/05/2019 1456135.0 ug/kg1
Chrysene ND 10/05/2019 14562.7 0.45 ug/kg1
Dibenzo(a,h)anthracene ND 10/05/2019 14562.7 0.51 ug/kg1
Dibenzofuran ND 10/05/2019 1456135.0 ug/kg1
3,3'-Dichlorobenzidine ND 10/05/2019 1456135.0 ug/kg1
2,4-Dichlorophenol ND 10/05/2019 1456135.0 ug/kg1
Diethylphthalate ND 10/05/2019 1456135.0 ug/kg1
Dimethyl phthalate ND 10/05/2019 1456137.4 ug/kg1
2,4-Dimethylphenol ND 10/05/2019 1456135.0 ug/kg1
Di-n-butyl phthalate ND 10/05/2019 1456135.0 ug/kg1
4,6-Dinitro-2-methylphenol ND 10/05/2019 14566725ug/kg1
2,4-Dinitrophenol ND 10/05/2019 14566725ug/kg1
2,4-Dinitrotoluene ND 10/05/2019 14562710ug/kg1
2,6-Dinitrotoluene ND 10/05/2019 14562710ug/kg1
Di-n-octylphthalate ND 10/05/2019 1456135.0 ug/kg1
bis(2-Ethylhexyl)phthalate ND 10/05/2019 14566725ug/kg1
Fluoranthene ND 10/05/2019 14562.7 0.42 ug/kg1
Fluorene ND 10/05/2019 14562.7 0.57 ug/kg1
Hexachlorobenzene ND 10/05/2019 1456135.0 ug/kg1
Hexachlorobutadiene ND 10/05/2019 1456135.0 ug/kg1
Hexachlorocyclopentadiene ND 10/05/2019 14566725ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 29 of 39
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:UQ30821-001
30821 3546
10/03/2019 1200Analytical Method:8270E
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Hexachloroethane ND 10/05/2019 1456135.0 ug/kg1
Indeno(1,2,3-c,d)pyrene ND 10/05/2019 14562.7 1.0 ug/kg1
Isophorone ND 10/05/2019 1456135.0 ug/kg1
2-Methylnaphthalene ND 10/05/2019 14562.7 0.99 ug/kg1
2-Methylphenol ND 10/05/2019 1456135.0 ug/kg1
3+4-Methylphenol ND 10/05/2019 14562710ug/kg1
Naphthalene ND 10/05/2019 14562.7 0.97 ug/kg1
2-Nitroaniline ND 10/05/2019 14562710ug/kg1
3-Nitroaniline ND 10/05/2019 14562710ug/kg1
4-Nitroaniline ND 10/05/2019 14562710ug/kg1
Nitrobenzene ND 10/05/2019 1456135.0 ug/kg1
2-Nitrophenol ND 10/05/2019 14562710ug/kg1
4-Nitrophenol ND 10/05/2019 14566725ug/kg1
N-Nitrosodi-n-propylamine ND 10/05/2019 1456135.0 ug/kg1
N-Nitrosodiphenylamine (Diphenylamine)ND 10/05/2019 1456135.0 ug/kg1
Pentachlorophenol ND 10/05/2019 14566725ug/kg1
Phenanthrene ND 10/05/2019 14562.7 0.72 ug/kg1
Phenol ND 10/05/2019 1456135.0 ug/kg1
Pyrene ND 10/05/2019 14562.7 0.50 ug/kg1
Pyridine ND 10/05/2019 1456135.0 ug/kg1
2,4,5-Trichlorophenol ND 10/05/2019 1456135.0 ug/kg1
2,4,6-Trichlorophenol ND 10/05/2019 1456135.0 ug/kg1
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 40 33-102
2-Fluorophenol 46 35-115
Nitrobenzene-d5 45 22-109
Phenol-d5 49 33-122
Terphenyl-d14 49 41-120
2,4,6-Tribromophenol 45 30-117
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 30 of 39
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:UQ30821-002
30821 3546
10/03/2019 1200Analytical Method:8270E
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acenaphthene 66 10/05/2019 15215013012-1111
Acenaphthylene 67 10/05/2019 15215113044-1221
Acetophenone 70 10/05/2019 15215313048-1111
Anthracene 72 10/05/2019 15215413016-1221
Atrazine 75 10/05/2019 15215713048-1161
Benzaldehyde 87 10/05/2019 15216513010-1101
Benzo(a)anthracene 69 10/05/2019 15215213040-1211
Benzo(a)pyrene 73 10/05/2019 15215513036-1141
Benzo(b)fluoranthene 75 10/05/2019 15215713038-1231
Benzo(g,h,i)perylene 84 10/05/2019 15216313043-1201
Benzo(k)fluoranthene 72 10/05/2019 15215413040-1261
1,1'-Biphenyl 66 10/05/2019 15215013049-1101
4-Bromophenyl phenyl ether 74 10/05/2019 15215613046-1181
Butyl benzyl phthalate 67 10/05/2019 15215113046-1281
Caprolactam 85 10/05/2019 15216413043-1211
Carbazole 74 10/05/2019 15215513047-1281
bis (2-Chloro-1-methylethyl) ether 88 10/05/2019 15216613031-1021
4-Chloro-3-methyl phenol 79 10/05/2019 15215913049-1181
4-Chloroaniline 38 10/05/2019 15212813017-1061
bis(2-Chloroethoxy)methane 73 10/05/2019 15215513039-1081
bis(2-Chloroethyl)ether 77 10/05/2019 15215813032-1051
2-Chloronaphthalene 68 10/05/2019 15215113031-1271
2-Chlorophenol 74 10/05/2019 15215613037-1061
4-Chlorophenyl phenyl ether 71 10/05/2019 15215413047-1161
Chrysene 72 10/05/2019 15215413041-1241
Dibenzo(a,h)anthracene 80 10/05/2019 15216013038-1251
Dibenzofuran 69 10/05/2019 15215213045-1121
3,3'-Dichlorobenzidine 65 10/05/2019 15214913010-1191
2,4-Dichlorophenol 72 10/05/2019 15215513041-1131
Diethylphthalate 72 10/05/2019 15215413049-1231
Dimethyl phthalate 74 10/05/2019 15215613048-1201
2,4-Dimethylphenol 110 10/05/2019 15218613033-1231
Di-n-butyl phthalate 73 10/05/2019 15215513051-1291
4,6-Dinitro-2-methylphenol 94 10/05/2019 15217113040-1301
2,4-Dinitrophenol 170 10/05/2019 15216227045-1271
2,4-Dinitrotoluene 76 10/05/2019 15215713048-1241
2,6-Dinitrotoluene 77 10/05/2019 15215813047-1251
Di-n-octylphthalate 74 10/05/2019 15215613049-1421
bis(2-Ethylhexyl)phthalate 66 10/05/2019 15215013045-1281
Fluoranthene 72 10/05/2019 15215413026-1331
Fluorene 69 10/05/2019 15215213019-1081
Hexachlorobenzene 76 10/05/2019 15215713044-1221
Hexachlorobutadiene 58 10/05/2019 15214313033-1031
Hexachlorocyclopentadiene 290 10/05/2019 15214467018-1211
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 31 of 39
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:UQ30821-002
30821 3546
10/03/2019 1200Analytical Method:8270E
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Hexachloroethane 50 10/05/2019 15213713030-961
Indeno(1,2,3-c,d)pyrene 79 10/05/2019 15216013042-1231
Isophorone 81 10/05/2019 15216113041-1131
2-Methylnaphthalene 68 10/05/2019 15215113010-1071
2-Methylphenol 81 10/05/2019 15216113032-1071
3+4-Methylphenol 86 10/05/2019 15216513039-1081
Naphthalene 66 10/05/2019 15215013010-1121
2-Nitroaniline 71 10/05/2019 15215313045-1231
3-Nitroaniline 45 10/05/2019 15213413024-1271
4-Nitroaniline 73 10/05/2019 15215513048-1271
Nitrobenzene 74 10/05/2019 15215513033-1141
2-Nitrophenol 70 10/05/2019 15215313035-1081
4-Nitrophenol 120 10/05/2019 15214627018-1541
N-Nitrosodi-n-propylamine 84 10/05/2019 15216413032-1151
N-Nitrosodiphenylamine (Diphenylamine)74 10/05/2019 15215513053-1501
Pentachlorophenol 160 10/05/2019 15216127027-1381
Phenanthrene 69 10/05/2019 15215213016-1231
Phenol 86 10/05/2019 15216513036-1081
Pyrene 70 10/05/2019 15215313034-1211
Pyridine 3.3 10/05/2019 1521N2.5130 30-1301
2,4,5-Trichlorophenol 79 10/05/2019 15215913046-1221
2,4,6-Trichlorophenol 75 10/05/2019 15215613038-1151
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 41 33-102
2-Fluorophenol 51 35-115
Nitrobenzene-d5 55 22-109
Phenol-d5 57 33-122
Terphenyl-d14 62 41-120
2,4,6-Tribromophenol 65 30-117
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 32 of 39
RCRA Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:UQ30967-001
30967 3050B
10/07/2019 0921Analytical Method:6010D
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Arsenic ND 10/08/2019 01070.75 0.25 mg/kg1
Barium ND 10/08/2019 01071.3 0.33 mg/kg1
Cadmium ND 10/08/2019 01070.25 0.063 mg/kg1
Chromium ND 10/08/2019 01070.50 0.13 mg/kg1
Lead ND 10/08/2019 01070.50 0.23 mg/kg1
Selenium ND 10/08/2019 01071.0 0.41 mg/kg1
Silver ND 10/08/2019 01070.50 0.13 mg/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 33 of 39
RCRA Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:UQ30967-002
30967 3050B
10/07/2019 0921Analytical Method:6010D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
Arsenic 270 10/08/2019 011210925080-1201
Barium 550 10/08/2019 011211050080-1201
Cadmium 51 10/08/2019 01121015080-1201
Chromium 270 10/08/2019 011210925080-1201
Lead 270 10/08/2019 011210825080-1201
Selenium 53 10/08/2019 01121055080-1201
Silver 51 10/08/2019 01121035080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 34 of 39
RCRA Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:UQ30969-001
30969 7471B
10/07/2019 1458Analytical Method:7471B
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Mercury ND 10/08/2019 12120.083 0.020 mg/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 35 of 39
RCRA Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:UQ30969-002
30969 7471B
10/07/2019 1458Analytical Method:7471B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
Mercury 0.80 10/08/2019 1219960.83 80-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

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Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

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SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

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SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

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Thomas Road/S.S. Giles Demolition Landfill - Closure Report SUMMIT Project No. 4319.514 Charlotte, North Carolina January 7, 2020

C:\plowery\Documents\2-Projects\4319.514 Thomas Road Site - Phase I ESA\Landfill\DEQ Sampling\Appendix Field Report.rtf

FIELD REPORTS