3507_PRTI_CA_20191216

Solid Material
Acenaphthene
16 mg/kg
0.13 mg/Kg
0.069 mg/kg
Acenapthylene
0.13 mg/Kg
0.085 mg/kg
Anthracene
1300 mg/kg
0.13 mg/Kg
0.069 mg/kg
Benzo(a)anthracene
0.35 mg/kg
0.13 mg/Kg
0.085 mg/kg
Benzo(a)pyrene
0.11 mg/kg
0.13 mg/Kg
0.085 mg/kg
Benzo(b)fluorathene
1.1 mg/kg
0.13 mg/Kg
0.085 mg/kg
Benzo(g,h,i)perylene
0.13 mg/Kg
0.077 mg/kg
Benzo(k)fluoranthene
11 mg/kg
0.13 mg/Kg
0.085 mg/kg
2-Chloronapththalene
0.26 mg/Kg
0.077 mg/kg
Chrysene
36 mg/kg
0.13 mg/Kg
0.085 mg/kg
Dibenz(a,h)anth racene
0.11 mg/kg
0.13 mg/Kg
0.077 mg/kg
Fluoranthene
480 mg/kg
0.13 mg/Kg
0.077 mg/kg
Fluorene
110 mg/kg
0.13 mg/Kg
0.092 mg/kg
Indeno(1,2,3-cd)pyrene
1.1 mg/kg
0.13 mg/Kg
0.092 mg/kg
2-Methylnaphthalene
3.1 mg/kg
0.13 mg/Kg
0.085 mg/kg
1-Methylnaphthalene
0.11 mg/kg
0.13 mg/Kg
0.069 mg/kg
Naphthalene
0.39 mg/kg
0.13 mg/Kg
0.085 mg/kg
Phenanthrene
0.13 mg/Kg
10.069 mg/kg
Pyrenel
360 mg/kg
1 0.13 mg/Kg
10.085 mg/kg
Chromium
5.6 mg/Kg
0.16 mg/Kg
Trivalent Chromium
23,000 mg/kg
Hexavalent Chromium
0.43 mg/Kg
0.27 mg/Kg
Copper
630 mg/kg
5.6 mg/Kg
0.094 mg/Kg
Lead
250 mg/kg
2.2 mg/Kg
0.029 mg/Kg
Nickell
140 mg/kg
5.6 mg/Kg
0.13 mg/Kg
Zincl
1200 mg/kg
11 mg/Kg
0.60 mg/Kg
Cadmium
14 mg/kR
0.45 mg/KR
10.020 mR/Kg

Capital
-
Control
D-
Reporting
Limit (RL)
Detection
Limit (DL)
PRTI North
West Corner
D-
Reporting
Limit (RL)
Detection
Limit (DL)
North West
WoodsMaterials
D- •
Reporting
<0.069 mg/kg
0.12 mg/Kg
0.065 mg/kg
<0.065 mg/kg
0.12 mg/Kg
0.061 mg/kg
<0.061 mg/kg
0.11 mg/Kg
<0.085 mg/kg
0.12 mg/Kg
0.080 mg/kg
<0.080 mg/kg
0.12 mg/Kg
0.075 mg/kg
<0.075 mg/kg
0.11 mg/Kg
<0.069 mg/kg
0.12 mg/Kg
0.065 mg/kg
<0.065 mg/kg
0.12 mg/Kg
0.061 mg/kg
<0.061 mg/kg
0.11 mg/Kg
<0.085 mg/kg
0.12 mg/Kg
0.080 mg/kg
<0.080 mg/kg
0.12 mg/Kg
0.075 mg/kg
<0.075 mg/kg
0.11 mg/Kg
<0.085 mg/kg
0.12 mg/Kg
0.080 mg/kg
<0.080 mg/kg
0.12 mg/Kg
0.075 mg/kg
<0.075 mg/kg
0.11 mg/Kg
<0.085 mg/kg
0.12 mg/Kg
0.080 mg/kg
<0.080 mg/kg
0.12 mg/Kg
0.075 mg/kg
<0.075 mg/kg
0.11 mg/Kg
<0.077 mg/kg
0.12 mg/Kg
0.073 mg/kg
<0.073 mg/kg
0.12 mg/Kg
0.068 mg/kg
<0.068 mg/kg
0.11 mg/Kg
<0.085 mg/kg
0.12 mg/Kg
0.080 mg/kg
<0.080 mg/kg
0.12 mg/Kg
0.075 mg/kg
<0.075 mg/kg
0.11 mg/Kg
<0.077 mg/kg
0.25 mg/Kg
0.073 mg/kg
<0.073 mg/kg
0.23 mg/Kg
0.068 mg/kg
<0.068 mg/kg
0.23 mg/Kg
<0.085 mg/kg
0.12 mg/Kg
0.080 mg/kg
<0.080 mg/kg
0.12 mg/Kg
0.075 mg/kg
<0.075 mg/kg
0.11 mg/Kg
<0.077 mg/kg
0.12 mg/Kg
0.073 mg/kg
<0.073 mg/kg
0.12 mg/Kg
0.068 mg/kg
<0.068 mg/kg
0.11 mg/Kg
<0.077 mg/kg
0.12 mg/Kg
0.073 mg/kg
<0.073 mg/kg
0.12 mg/Kg
0.068 mg/kg
<0.068 mg/kg
0.11 mg/Kg
<0.092 mg/kg
0.12 mg/Kg
0.087 mg/kg
<0.087 mg/kg
0.12 mg/Kg
0.082 mg/kg
<0.082 mg/kg
0.11 mg/Kg
<0.092 mg/kg
0.12 mg/Kg
0.087 mg/kg
<0.087 mg/kg
0.12 mg/Kg
0.082 mg/kg
<0.082 mg/kg
0.11 mg/Kg
<0.085 mg/kg
0.12 mg/Kg
0.080 mg/kg
<0.080 mg/kg
0.12 mg/Kg
0.075 mg/kg
<0.075 mg/kg
0.11 mg/Kg
<0.069 mg/kg
0.12 mg/Kg
0.065 mg/kg
<0.065 mg/kg
0.12 mg/Kg
0.061 mg/kg
<0.061 mg/kg
0.11 mg/Kg
<0.085 mg/kg
0.12 mg/Kg
0.080 mg/kg
<0.080 mg/kg
0.12 mg/Kg
0.075 mg/kg
<0.075 mg/kg
0.11 mg/Kg
<0.069 mg/kg
0.12 mg/Kg
0.065 mg/kg
<0.065 mg/kg
0.12 mg/Kg
0.061 mg/kg
<0.061 mg/kg
0.11 mg/Kg
<0.085 mg/kg
0.12 mg/Kg
0.080 mg/kg
<0.080 mg/kg
0.12 mg/Kg
0.075 mg/kg
<0.075 mg/kg
0.11 mg/Kg
16 mg/kg
5.5 mg/Kg
0.16 mg/Kg
14 mg/kg
5.3 mg/Kg
0.15 mg/Kg
9.4 mg/kg
5.5 mg/Kg
16 mg/kg
14 mg/kg
9.4 mg/kg
<0.27 mg/kg
0.42 mg/Kg
0.26 mg/Kg
<0.26 mg/kg
0.40 mg/Kg
0.25 mg/Kg
<0.25 mg/kg
0.42 mg/Kg
19 mg/kg
5.5 mg/Kg
0.092 mg/Kg
10 mg/kg
5.3 mg/Kg
0.088 mg/Kg
5.9 mg/kg
5.5 mg/Kg
20 mg/kg
2.2 mg/Kg
0.029 mg/Kg
13 mg/kg
2.1 mg/Kg
0.027 mg/Kg
13 mg/kg
2.2 mg/Kg
4.7 j mg/kg
5.5 mg/Kg
0.13 mg/Kg
4.1 j mg/kg
5.3 mg/Kg
0.12 mg/Kg
2.8 j mg/kg
5.5 mg/Kg
60 mg/kg
11 mg/Kg
0.59 mg/Kg
120 mg/kg
11 mg/Kg
0.56 mg/Kg
14 mg/kg
11 mg/Kg
0.11 j mg/kg
0.44 mg/Kg
0.019 mg/Kg
0.12 j mg/kg
0.42 mg/Kg
0.018 mg/Kg
0.057 j mg/kg
0.44 mg/Kg

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
January 6, 2020
Compton Donahue
PRTI, INC
2105 US 1 HWY
Franklinton, NC 27587
Project Location: 2105 US 1 Highway, Franklinton, NC
Client Job Number:
Project Number: NC FR 1375
Laboratory Work Order Number: 19L0710
Enclosed are results of analyses for samples received by the laboratory on December 16, 2019. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
M
Michelle M. Koch
Project Manager

Table of Contents
Table of Contents
Sample Summary
4
Case Narrative
5
Sample Results
8
19L0710-01
8
19L0710-02
10
19L0710-03
12
19L0710-04
14
19L0710-05
16
19L0710-07
18
19L0710-09
20
19L0710-11
22
19L0710-12
24
19L0710-13
26
19L0710-14
28
19L0710-15
30
19L0710-16
32
19L0710-17
34
Sample Preparation Information
36
QC Data
38
Semivolatile Organic Compounds by GUMS
38
B248570
38
B248698
40
B248798
41
Metals Analyses (Total)
43
B248645
43

Table of Contents
Table of Contents (continued)
B248713
B249387
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
B248582
B249020
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
43
44
45
45
45
46
47
50

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
PRTI, INC
2105 US 1 HWY REPORT DATE: 1/6/2020
Franklinton, NC 27587 PURCHASE ORDER NUMBER: NC FR 1375
ATTN: Compton Donahue
PROJECT NUMBER: NC FR 1375
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 19LO710
The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report.
PROJECT LOCATION: 2105 US 1 Highway, Franklinton, NC
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
A.1 19LO710-01 Soil SM 254OG
SW-846 8270E
B.1 19LO710-02 Soil SM 2540G
SW-846 8270E
CA 19LO710-03 Soil SM 254OG
SW-846 8270E
D.1 19LO710-04 Soil SM 254OG
SW-846 8270E
E.La 19LO710-05 Surface Water SW-846 6010
SW-846 8270E
F. La 19LO710-07 Surface Water SW-846 6010
SW-846 8270E
G.La 19LO710-09 Surface Water SW-846 6010
SW-846 8270E
A.2 19LO710-11 Soil SM 2540G
SW-846 6020B
SW-846 7196A
Tri Chrome Calc.
B.2 19LO710-12 Soil SM 254OG
SW-846 6020B
SW-846 7196A
Tri Chrome Calc.
C.2 19LO710-13 Soil SM 254OG
SW-846 6020B
SW-846 7196A
Tri Chrome Calc.
D.2 19LO710-14 Soil SM 2540G
SW-846 6020B
SW-846 7196A
Tri Chrome Calc.
E.2 19LO710-15 Surface Water SW-846 6020B
SW-846 7196A
Tri Chrome Calc.
F.2 19LO710-16 Surface Water SW-846 6020B
SW-846 7196A
Tri Chrome Calc.
G.2 19LO710-17 Surface Water SW-846 6020B
SW-846 7196A
Tri Chrome Calc.

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
REVISED REPORT - 1/6/2020 - Hardness added to samples 19LO710-05 & -07 & -09 per clients request. 1-Methylnaphthlene added and 8270 data
reported to MDL.
For method 6020, all dilutions were performed as per standard operating procedure.

Table of Contents
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40
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
SW-846 7196A
Qualifications:
MS-07A
Matrix spike and spike duplicate recovery is outside of control limits. Analysis is in control based on laboratory fortified blank recovery.
Possiblity of matrix effects that lead to low bias or non -homogeneous sample aliquot cannot be eliminated.
Analyte & Samples(s) Qualified:
Hexavalent Chromium
B249020-MS1, B249020-MSDI
W-06
Elevated method reporting limit due to intense color of sample
Analyte & Samples(s) Qualified:
Hexavalent Chromium
19LO710-11[A.2],19Lo710-12[B.2],19Lo710-13[C.2],19Lo710-14[D.2]
Z-01
Samples ran passed recommended holding time
Analyte & Samples(s) Qualified:
Hexavalent Chromium
19L0710-15[E.2], 19L0710-16[F.2], 19L0710-17[G.2]
SW-846 8270E
Qualifications:
NIS-22
Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the two MS/MSD results is
within method specified criteria.
Analyte & Samples(s) Qualified:
Benzo(g,h,i)perylene
B248570-MSDI
R-05
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
Pyrene (SIM)
19L0710-05[E. La], 19L0710-07[F. La], 19L0710-09[G. La], B248798-BLKI, B248798-BSI, B248798-BSDI
V-04
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method
specified criteria. Reported result is estimated.
Analyte & Samples(s) Qualified:
Benzidine
S044002-CCV 1
V-05
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
Benzidine
5043945-CCV1, S044002-CCV1
Hexachlorocyclopentadiene
S044002-CCV 1
Pentachlorophenol
S044002-CCV 1
V-34
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
4-Chloroaniline
S044002-CCV 1
Benzoic Acid
S043945-CCV 1

Table of Contents
,con-testo
ANALYTICAL LABORATORY
V-35
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] ` TEL. [phone]
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
Benzidine
5043945-CCVI, S044002-CCVI
The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative

Table of Contents
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ANALYTICAL LABQRATURY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: 2105 US 1 Highway, Franklinton, Sample Description: Work Order: 19LO710
Date Received: 12/16/2019
Field Sample #: A.1 Sampled: 12/16/2019 09:15
Sample ID: 19LO710-01
Samnle Matrix: Soil
Semivolatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Acenaphthene
ND
0.13
0.069
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:28
KLB
Acenaphthylene
ND
0.13
0.085
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:28
KLB
Anthracene
ND
0.13
0.069
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:28
KLB
Benzo(a)anthracene
ND
0.13
0.085
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:28
KLB
Benzo(a)pyrene
ND
0.13
0.085
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:28
KLB
Benzo(b)fluoranthene
ND
0.13
0.085
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:28
KLB
Benzo(g,h,i)perylene
ND
0.13
0.077
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:28
KLB
Benzo(k)fluoranthene
ND
0.13
0.085
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:28
KLB
2-Chloronaphthalene
ND
0.26
0.077
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:28
KLB
Chrysene
ND
0.13
0.085
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:28
KLB
Dibenz(a,h)anthracene
ND
0.13
0.077
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:28
KLB
Fluoranthene
ND
0.13
0.077
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:28
KLB
Fluorene
ND
0.13
0.092
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:28
KLB
Indeno(1,2,3-cd)pyrene
ND
0.13
0.092
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:28
KLB
2-Methylnaphthalene
ND
0.13
0.085
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:28
KLB
1-Methylnaphthalene
ND
0.13
0.069
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:28
KLB
Naphthalene
ND
0.13
0.085
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:28
KLB
Phenanthrene
ND
0.13
0.069
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:28
KLB
Pyrene
ND
0.13
0.085
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:28
KLB
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
52.3
30-130
12/19/19 15:28
Phenol-d6
55.2
30-130
12/19/19 15:28
Nitrobenzene-d5
48.5
30-130
12/19/19 15:28
Nitrobenzene-d5
48.5
30-130
12/19/19 15:28
2-Fluorobiphenyl
69.7
30-130
12/19/19 15:28
2-Fluorobiphenyl
69.7
30-130
12/19/19 15:28
2,4,6-Tribromophenol
68.7
30-130
12/19/19 15:28
p-Terphenyl-dl4
60.7
30-130
12/19/19 15:28
p-Terphenyl-dl4
60.7
30-130
12/19/19 15:28

Table of Contents
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ANALYTICAL LABQRATURY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: 2105 US 1 Highway, Franklinton, Sample Description: Work Order: 19L0710
Date Received: 12/16/2019
Field Sample #: A.1 Sampled: 12/16/2019 09:15
Sample ID: 19L0710-01
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 65.1 % Wt 1 SM 2540G 12/18/19 12/18/19 15:54 ADB

Table of Contents
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ANALYTICAL LABQRATURY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: 2105 US 1 Highway, Franklinton, Sample Description: Work Order: 19LO710
Date Received: 12/16/2019
Field Sample #: B.1 Sampled: 12/16/2019 09:47
Sample ID: 19LO710-02
Samnle Matrix: Soil
Semivolatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Acenaphthene
ND
0.12
0.065
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:54
KLB
Acenaphthylene
ND
0.12
0.080
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:54
KLB
Anthracene
ND
0.12
0.065
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:54
KLB
Benzo(a)anthracene
ND
0.12
0.080
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:54
KLB
Benzo(a)pyrene
ND
0.12
0.080
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:54
KLB
Benzo(b)fluoranthene
ND
0.12
0.080
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:54
KLB
Benzo(g,h,i)perylene
ND
0.12
0.073
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:54
KLB
Benzo(k)fluoranthene
ND
0.12
0.080
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:54
KLB
2-Chloronaphthalene
ND
0.25
0.073
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:54
KLB
Chrysene
ND
0.12
0.080
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:54
KLB
Dibenz(a,h)anthracene
ND
0.12
0.073
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:54
KLB
Fluoranthene
ND
0.12
0.073
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:54
KLB
Fluorene
ND
0.12
0.087
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:54
KLB
Indeno(1,2,3-cd)pyrene
ND
0.12
0.087
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:54
KLB
2-Methylnaphthalene
ND
0.12
0.080
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:54
KLB
1-Methylnaphthalene
ND
0.12
0.065
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:54
KLB
Naphthalene
ND
0.12
0.080
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:54
KLB
Phenanthrene
ND
0.12
0.065
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:54
KLB
Pyrene
ND
0.12
0.080
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 15:54
KLB
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Flumophenol
51.6
30-130
12/19/19 15:54
Phenol-d6
52.5
30-130
12/19/19 15:54
Nitrobenzene-d5
49.3
30-130
12/19/19 15:54
Nitrobenzene-d5
49.3
30-130
12/19/19 15:54
2-Fluorobiphenyl
67.1
30-130
12/19/19 15:54
2-Fluorobiphenyl
67.1
30-130
12/19/19 15:54
2,4,6-Tribromophenol
57.3
30-130
12/19/19 15:54
p-Terphenyl-dl4
55.5
30-130
12/19/19 15:54
p-Terphenyl-dl4
55.5
30-130
12/19/19 15:54

Table of Contents
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ANALYTICAL LABQRATURY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: 2105 US 1 Highway, Franklinton, Sample Description: Work Order: 19L0710
Date Received: 12/16/2019
Field Sample #: B.1 Sampled: 12/16/2019 09:47
Sample ID: 19L0710-02
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 68.7 % Wt 1 SM 2540G 12/18/19 12/18/19 15:54 ADB

Table of Contents
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ANALYTICAL LABQRATURY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: 2105 US 1 Highway, Franklinton, Sample Description: Work Order: 19LO710
Date Received: 12/16/2019
Field Sample #: C.1 Sampled: 12/16/2019 09:30
Sample ID: 19LO710-03
Samnle Matrix: Soil
Semivolatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Acenaphthene
ND
0.12
0.061
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 13:39
KLB
Acenaphthylene
ND
0.12
0.075
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 13:39
KLB
Anthracene
ND
0.12
0.061
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 13:39
KLB
Benzo(a)anthracene
ND
0.12
0.075
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 13:39
KLB
Benzo(a)pyrene
ND
0.12
0.075
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 13:39
KLB
Benzo(b)fluoranthene
ND
0.12
0.075
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 13:39
KLB
Benzo(g,h,i)perylene
ND
0.12
0.068
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 13:39
KLB
Benzo(k)fluoranthene
ND
0.12
0.075
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 13:39
KLB
2-Chloronaphthalene
ND
0.23
0.068
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 13:39
KLB
Chrysene
ND
0.12
0.075
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 13:39
KLB
Dibenz(a,h)anthracene
ND
0.12
0.068
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 13:39
KLB
Fluoranthene
ND
0.12
0.068
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 13:39
KLB
Fluorene
ND
0.12
0.082
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 13:39
KLB
Indeno(1,2,3-cd)pyrene
ND
0.12
0.082
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 13:39
KLB
2-Methylnaphthalene
ND
0.12
0.075
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 13:39
KLB
1-Methylnaphthalene
ND
0.12
0.061
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 13:39
KLB
Naphthalene
ND
0.12
0.075
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 13:39
KLB
Phenanthrene
ND
0.12
0.061
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 13:39
KLB
Pyrene
ND
0.12
0.075
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 13:39
KLB
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
64.0
30-130
12/19/19 13:39
Phenol-d6
67.8
30-130
12/19/19 13:39
Nitrobenzene-d5
58.5
30-130
12/19/19 13:39
Nitrobenzene-d5
58.5
30-130
12/19/19 13:39
2-Fluorobiphenyl
82.8
30-130
12/19/19 13:39
2-Fluorobiphenyl
82.8
30-130
12/19/19 13:39
2,4,6-Tribromophenol
80.8
30-130
12/19/19 13:39
p-Terphenyl-dl4
71.9
30-130
12/19/19 13:39
p-Terphenyl-dl4
71.9
30-130
12/19/19 13:39

Table of Contents
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ANALYTICAL LABQRATURY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: 2105 US 1 Highway, Franklinton, Sample Description: Work Order: 19L0710
Date Received: 12/16/2019
Field Sample #: C.1 Sampled: 12/16/2019 09:30
Sample ID: 19L0710-03
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 73.3 % Wt 1 SM 2540G 12/18/19 12/18/19 15:54 ADB

Table of Contents
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ANALYTICAL LABQRATURY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: 2105 US 1 Highway, Franklinton, Sample Description: Work Order: 19LO710
Date Received: 12/16/2019
Field Sample #: D.1 Sampled: 12/16/2019 09:25
Sample ID: 19LO710-04
Samnle Matrix: Soil
Semivolatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Acenaphthene
ND
0.11
0.061
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 14:04
KLB
Acenaphthylene
ND
0.11
0.074
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 14:04
KLB
Anthracene
ND
0.11
0.061
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 14:04
KLB
Benzo(a)anthracene
ND
0.11
0.074
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 14:04
KLB
Benzo(a)pyrene
ND
0.11
0.074
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 14:04
KLB
Benzo(b)fluoranthene
ND
0.11
0.074
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 14:04
KLB
Benzo(g,h,i)perylene
ND
0.11
0.068
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 14:04
KLB
Benzo(k)fluoranthene
ND
0.11
0.074
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 14:04
KLB
2-Chloronaphthalene
ND
0.23
0.068
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 14:04
KLB
Chrysene
ND
0.11
0.074
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 14:04
KLB
Dibenz(a,h)anthracene
ND
0.11
0.068
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 14:04
KLB
Fluoranthene
ND
0.11
0.068
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 14:04
KLB
Fluorene
ND
0.11
0.081
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 14:04
KLB
Indeno(1,2,3-cd)pyrene
ND
0.11
0.081
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 14:04
KLB
2-Methylnaphthalene
ND
0.11
0.074
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 14:04
KLB
1-Methylnaphthalene
ND
0.11
0.061
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 14:04
KLB
Naphthalene
ND
0.11
0.074
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 14:04
KLB
Phenanthrene
ND
0.11
0.061
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 14:04
KLB
Pyrene
ND
0.11
0.074
mg/Kg dry
1
SW-846 8270E
12/18/19
12/19/19 14:04
KLB
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
81.8
30-130
12/19/19 14:04
Phenol-d6
86.6
30-130
12/19/19 14:04
Nitrobenzene-d5
78.1
30-130
12/19/19 14:04
Nitrobenzene-d5
78.1
30-130
12/19/19 14:04
2-Fluorobiphenyl
93.7
30-130
12/19/19 14:04
2-Fluorobiphenyl
93.7
30-130
12/19/19 14:04
2,4,6-Tribromophenol
102
30-130
12/19/19 14:04
p-Terphenyl-dl4
82.1
30-130
12/19/19 14:04
p-Terphenyl-dl4
82.1
30-130
12/19/19 14:04

Table of Contents
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ANALYTICAL LABQRATURY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: 2105 US 1 Highway, Franklinton, Sample Description: Work Order: 19L0710
Date Received: 12/16/2019
Field Sample #: D.1 Sampled: 12/16/2019 09:25
Sample ID: 19L0710-04
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 73.9 % Wt 1 SM 2540G 12/18/19 12/18/19 15:54 ADB

Table of Contents
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ANALYTICAL LABQRATURY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: 2105 US 1 Highway, Franklinton, Sample Description: Work Order: 19L0710
Date Received: 12/16/2019
Field Sample #: A.2 Sampled: 12/16/2019 09:16
Sample ID: 19L0710-11
Samnle Matrix: Soil
Analyte
Results
RL
DL
Metals Analyses (Total)
Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Chromium
16
5.6
0.16
mg/Kg dry
5
SW-846 6020B
12/18/19
12/19/19 16:43
MJH
Chromium, Trivalent
16
mg/Kg
1
Tri Chrome Cale.
12/18/19
12/19/19 17:45
MJH
Copper
19
5.6
0.094
mg/Kg dry
5
SW-846 6020B
12/18/19
12/19/19 16:43
MJH
Lead
20
2.2
0.029
mg/Kg dry
5
SW-846 6020B
12/18/19
12/19/19 16:43
MJH
Nickel
4.7
5.6
0.13
mg/Kg dry
5 J
SW-846 6020B
12/18/19
12/19/19 16:43
MJH
Zinc
60
11
0.60
mg/Kg dry
5
SW-846 6020B
12/18/19
12/19/19 16:43
MJH
Cadmium
0.11
0.45
0.020
mg/Kg dry
5 J
SW-846 6020B
12/18/19
12/19/19 16:43
MJH

Table of Contents
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ANALYTICAL LABQRATURY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: 2105 US 1 Highway, Franklinton, Sample Description: Work Order: 19L0710
Date Received: 12/16/2019
Field Sample #: A.2 Sampled: 12/16/2019 09:16
Sample ID: 19L0710-11
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 71.9 % Wt 1 SM 2540G 12/18/19 12/18/19 15:54 ADB
Hexavalent Chromium ND 0.43 0.27 mg/Kg dry 2 W-06 SW-846 7196A 12/18/19 12/19/19 8:40 LL

Table of Contents
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ANALYTICAL LABQRATURY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: 2105 US 1 Highway, Franklinton, Sample Description: Work Order: 19L0710
Date Received: 12/16/2019
Field Sample #: B.2 Sampled: 12/16/2019 09:23
Sample ID: 19L0710-12
Samnle Matrix: Soil
Analyte
Results
RL
DL
Metals Analyses (Total)
Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Chromium
14
5.5
0.16
mg/Kg dry
5
SW-846 6020B
12/18/19
12/19/19 16:46
MJH
Chromium, Trivalent
14
mg/Kg
1
Tri Chrome Cale.
12/18/19
12/19/19 17:45
MJH
Copper
10
5.5
0.092
mg/Kg dry
5
SW-846 6020B
12/18/19
12/19/19 16:46
MJH
Lead
13
2.2
0.029
mg/Kg dry
5
SW-846 6020B
12/18/19
12/19/19 16:46
MJH
Nickel
4.1
5.5
0.13
mg/Kg dry
5 J
SW-846 6020B
12/18/19
12/19/19 16:46
MJH
Zinc
120
11
0.59
mg/Kg dry
5
SW-846 6020B
12/18/19
12/19/19 16:46
MJH
Cadmium
0.12
0.44
0.019
mg/Kg dry
5 J
SW-846 6020B
12/18/19
12/19/19 16:46
MJH

Table of Contents
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ANALYTICAL LABQRATURY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: 2105 US 1 Highway, Franklinton, Sample Description: Work Order: 19L0710
Date Received: 12/16/2019
Field Sample #: B.2 Sampled: 12/16/2019 09:23
Sample ID: 19L0710-12
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 73.9 % Wt 1 SM 2540G 12/18/19 12/18/19 15:55 ADB
Hexavalent Chromium ND 0.42 0.26 mg/Kg dry 2 W-06 SW-846 7196A 12/18/19 12/19/19 8:40 LL

Table of Contents
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ANALYTICAL LABQRATURY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: 2105 US 1 Highway, Franklinton, Sample Description: Work Order: 19L0710
Date Received: 12/16/2019
Field Sample #: C.2 Sampled: 12/16/2019 09:45
Sample ID: 19L0710-13
Samnle Matrix: Soil
Analyte
Results
RL
DL
Metals Analyses (Total)
Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Chromium
9.4
5.3
0.15
mg/Kg dry
5
SW-846 6020B
12/18/19
12/19/19 16:49
MJH
Chromium, Trivalent
9.4
mg/Kg
1
Tri Chrome Cale.
12/18/19
12/19/19 17:45
MJH
Copper
5.9
5.3
0.088
mg/Kg dry
5
SW-846 6020B
12/18/19
12/19/19 16:49
MJH
Lead
13
2.1
0.027
mg/Kg dry
5
SW-846 6020B
12/18/19
12/19/19 16:49
MJH
Nickel
2.8
5.3
0.12
mg/Kg dry
5 J
SW-846 6020B
12/18/19
12/19/19 16:49
MJH
Zinc
14
11
0.56
mg/Kg dry
5
SW-846 6020B
12/18/19
12/19/19 16:49
MJH
Cadmium
0.057
0.42
0.018
mg/Kg dry
5 J
SW-846 6020B
12/18/19
12/19/19 16:49
MJH

Table of Contents
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ANALYTICAL LABQRATURY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: 2105 US 1 Highway, Franklinton, Sample Description: Work Order: 19L0710
Date Received: 12/16/2019
Field Sample #: C.2 Sampled: 12/16/2019 09:45
Sample ID: 19L0710-13
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 77.9 % Wt 1 SM 2540G 12/18/19 12/18/19 15:55 ADB
Hexavalent Chromium ND 0.40 0.25 mg/Kg dry 2 W-06 SW-846 7196A 12/18/19 12/19/19 8:40 LL

Table of Contents
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ANALYTICAL LABQRATURY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: 2105 US 1 Highway, Franklinton, Sample Description: Work Order: 19L0710
Date Received: 12/16/2019
Field Sample #: D.2 Sampled: 12/16/2019 09:32
Sample ID: 19L0710-14
Samnle Matrix: Soil
Analyte
Results
RL
DL
Metals Analyses (Total)
Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Chromium
17
5.5
0.16
mg/Kg dry
5
SW-846 6020B
12/18/19
12/19/19 17:09
MJH
Chromium, Trivalent
17
mg/Kg
1
Tri Chrome Cale.
12/18/19
12/19/19 17:45
MJH
Copper
9.3
5.5
0.091
mg/Kg dry
5
SW-846 6020B
12/18/19
12/19/19 17:09
MJH
Lead
17
2.2
0.028
mg/Kg dry
5
SW-846 6020B
12/18/19
12/19/19 17:09
MJH
Nickel
4.2
5.5
0.13
mg/Kg dry
5 J
SW-846 6020B
12/18/19
12/19/19 17:09
MJH
Zinc
27
11
0.58
mg/Kg dry
5
SW-846 6020B
12/18/19
12/19/19 17:09
MJH
Cadmium
0.15
0.44
0.019
mg/Kg dry
5 J
SW-846 6020B
12/18/19
12/19/19 17:09
MJH

Table of Contents
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ANALYTICAL LABQRATURY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: 2105 US 1 Highway, Franklinton, Sample Description: Work Order: 19L0710
Date Received: 12/16/2019
Field Sample #: D.2 Sampled: 12/16/2019 09:32
Sample ID: 19L0710-14
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 75.0 % Wt 1 SM 2540G 12/18/19 12/18/19 15:55 ADB
Hexavalent Chromium ND 0.42 0.25 mg/Kg dry 2 W-06 SW-846 7196A 12/18/19 12/19/19 8:40 LL

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] TEL. [phone]
Sample Extraction Data
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]
Batch
Date
19L0710-01 [A.1]
B248588
12/18/19
19L0710-02 [B.1]
B248588
12/18/19
19L0710-03 [C.1]
B248588
12/18/19
19L0710-04 [D.1]
B248588
12/18/19
19L0710-11 [A.2]
B248588
12/18/19
19L0710-12 [B.2]
B248588
12/18/19
19L0710-13 [C.2]
B248588
12/18/19
19L0710-14 [D.2]
B248588
12/18/19
Prep Method: SW-846 3005A-SW-846 6010
Lab Number [Field ID]
Batch
Initial [mL]
Date
19L0710-05[E.La]
B249387
50.0
01/03/20
19L0710-07 [F.La]
B249387
50.0
01/03/20
19L0710-09[G.l.a]
B249387
50.0
01/03/20
Prep Method: SW-846 3050B-SW-846 6020B
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
19L0710-11 [A.2]
B248645
1.55
50.0
12/18/19
19L0710-12[B.2]
B248645
1.53
50.0
12/18/19
19L0710-13 [C.2]
B248645
1.53
50.0
12/18/19
19L0710-14 [D.2]
B248645
1.52
50.0
12/18/19
Prep Method: SW-846 3005A-SW-846 6020B
Lab Number [Field ID]
Batch
Initial [mL]
Final [mL]
Date
19L0710-15[E.2]
B248713
50.0
50.0
12/19/19
19L0710-16[F.2]
B248713
50.0
50.0
12/19/19
19L0710-17[G.2]
B248713
50.0
50.0
12/19/19
SW-846 7196A
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
19L0710-11[A.2]
B248582
2.56
100
12/18/19
19L0710-12[B.2]
B248582
2.58
100
12/18/19
19L0710-13[C.2]
B248582
2.56
100
12/18/19
19L0710-14 [D.2]
B248582
2.56
100
12/18/19
SW-846 7196A
Lab Number [Field ID]
Batch
Initial [mL]
Final [mL]
Date
19L0710-15[E.2]
B249020
50.0
50.0
12/24/19
19L0710-16 [F.2]
B249020
50.0
50.0
12/24/19
19L0710-17 [G.2]
B249020
50.0
50.0
12/24/19

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3546-SW-846 8270E
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
19L0710-01 [A.1]
B248570
30.0
0.500
12/18/19
19L0710-02 [B.1]
B248570
30.0
0.500
12/18/19
19L0710-03 [C.1]
B248570
30.0
0.500
12/18/19
19L0710-04 [D.1]
B248570
30.0
0.500
12/18/19
Prep Method: SW-846 3510C-SW-846 8270E
Lab Number [Field ID]
Batch
Initial [mL]
Final [mL]
Date
19L0710-05 [E.La]
B248698
1030
1.00
12/19/19
19L0710-07 [F.l.a]
B248698
1030
1.00
12/19/19
19L0710-09 [G.l.a]
B248698
1040
1.00
12/19/19
Prep Method: SW-846 3510C-SW-846 8270E
Lab Number [Field ID]
Batch
Initial [mL]
Final [mL]
Date
19L0710-05 [E.La]
B248798
1030
1.00
12/19/19
19L0710-07 [F.l.a]
B248798
1030
1.00
12/19/19
19L0710-09 [G.l.a]
B248798
1040
1.00
12/19/19
Prep Method: SW-846 3050B-Tri Chrome Calc.
Lab Number [Field ID]
Batch
Initial [g]
Date
19L0710-11 [A.2]
B248645
1.55
12/18/19
19L0710-12 [B.2]
B248645
1.53
12/18/19
19L0710-13 [C.2]
B248645
1.53
12/18/19
19L0710-14[D.2]
B248645
1.52
12/18/19
Prep Method: SW-846 3005A-Tri Chrome Cale.
Lab Number [Field ID]
Batch
Initial [mL]
Date
19L0710-15[E.2]
B248713
50.0
12/19/19
19L0710-16[F.2]
B248713
50.0
12/19/19
19L0710-17[G.2]
B248713
50.0
12/19/19

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
\nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B248570 - SW-846 3546
Blank (B248570-BLK1)
Prepared: 12/18/19 Analyzed: 12/19/19
Acenaphthene
ND
0.085
mg/Kg wet
Acenaphthylene
ND
0.085
mg/Kg wet
Anthracene
ND
0.085
mg/Kg wet
Benzo(a)anthracene
ND
0.085
mg/Kg wet
Benzo(a)pyrene
ND
0.085
mg/Kg wet
Benzo(b)fluoranthene
ND
0.085
mg/Kg wet
Benzo(g,h,i)perylene
ND
0.085
mg/Kg wet
Benzo(k)fluoranthene
ND
0.085
mg/Kg wet
2-Chloronaphthalene
ND
0.17
mg/Kg wet
Chrysene
ND
0.085
mg/Kg wet
Dibenz(a,h)anthracene
ND
0.085
mg/Kg wet
Fluoranthene
ND
0.085
mg/Kg wet
Fluorene
ND
0.085
mg/Kg wet
Indeno(1,2,3-cd)pyrene
ND
0.085
mg/Kg wet
2-Methylnaphthalene
ND
0.085
mg/Kg wet
I-Methylnaphthalene
ND
0.085
mg/Kg wet
Naphthalene
ND
0.085
mg/Kg wet
Phenanthrene
ND
0.085
mg/Kg wet
Pyrene
ND
0.085
mg/Kg wet
Surrogate:2-Fluorophenol
5.61
mg/Kg wet
6.67
84.2
30-130
Surrogate: Phenol-d6
5.65
mg/Kg wet
6.67
84.8
30-130
Surrogate: Nitrobenzene-d5
2.52
mg/Kg wet
3.33
75.6
30-130
Surrogate:2-Fluorobiphenyl
3.41
mg/Kg wet
3.33
102
30-130
Surrogate: 2,4,6-Tribromophenol
7.64
mg/Kg wet
6.67
115
30-130
Surrogate: p-Terphenyl-dl4
3.32
mg/Kg wet
3.33
99.5
30-130
LCS (B248570-BS1)
Prepared: 12/18/19 Analyzed: 12/19/19
Acenaphthene
1.31
0.17
mg/Kg wet
1.67
78.7
40-140
Acenaphthylene
1.34
0.17
mg/Kg wet
1.67
80.4
40-140
Anthracene
1.39
0.17
mg/Kg wet
1.67
83.3
40-140
Benzo(a)anthracene
1.38
0.17
mg/Kg wet
1.67
82.5
40-140
Benzo(a)pyrene
137
0.17
mg/Kg wet
1.67
82.0
40-140
Benzo(b)fluoranthene
1.38
0.17
mg/Kg wet
1.67
82.7
40-140
Benzo(g,h,i)perylene
1.36
0.17
mg/Kg wet
1.67
81.7
40-140
Benzo(k)fluoranthene
1.39
0.17
mg/Kg wet
1.67
83.6
40-140
2-Chloronaphthalene
1.22
0.34
mg/Kg wet
1.67
73.3
40-140
Chrysene
1.36
0.17
mg/Kg wet
1.67
81.8
40-140
Dibenz(a,h)anthracene
1.36
0.17
mg/Kg wet
1.67
81.8
40-140
Fluoranthene
1.39
0.17
mg/Kg wet
1.67
83.6
40-140
Fluorene
1.36
0.17
mg/Kg wet
1.67
81.7
40-140
Indeno(1,2,3-cd)pyrene
1.46
0.17
mg/Kg wet
1.67
87.6
40-140
2-Methylnaphthalene
1.51
0.17
mg/Kg wet
1.67
90.6
40-140
1-Methylnaphthalene
1.30
0.17
mg/Kg wet
1.67
78.2
40-140
Naphthalene
1.27
0.17
mg/Kg wet
1.67
76.5
40-140
Phenanthrene
1.40
0.17
mg/Kg wet
1.67
83.9
40-140
Pyrene
1.36
0.17
mg/Kg wet
1.67
81.8
40-140
Surrogate:2-Fluorophenol
5.51
mg/Kg wet
6.67
82.6
30-130
Surrogate: Phenol-d6
5.55
mg/Kg wet
6.67
83.3
30-130
Surrogate: Nitrobenzene-d5
2.69
mg/Kg wet
3.33
80.6
30-130
Surrogate:2-Fluorobiphenyl
3.60
mg/Kg wet
3.33
108
30-130
Surrogate: 2,4,6-Tribromophenol
7.20
mg/Kg wet
6.67
108
30-130
Surrogate: p-Terphenyl-d 14
3.13
mg/Kg wet
3.33
94.0
30-130

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
.nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B248570 - SW-846 3546
LCS Dup (B248570-BSD1) Prepared: 12/18/19 Analyzed: 12/19/19
Acenaphthene
1.29
0.17
mg/Kg wet
1.67
77.5
40-140
1.54
30
Acenaphthylene
1.30
0.17
mg/Kg wet
1.67
78.1
40-140
3.00
30
Anthracene
1.39
0.17
mg/Kg wet
1.67
83.2
40-140
0.120
30
Benzo(a)anthracene
137
0.17
mg/Kg wet
1.67
82.3
40-140
0.194
30
Benzo(a)pyrene
1.36
0.17
mg/Kg wet
1.67
81.7
40-140
0.367
30
Benzo(b)fluoranthene
138
0.17
mg/Kg wet
1.67
82.6
40-140
0.121
30
Benzo(g,h,i)perylene
1.33
0.17
mg/Kg wet
1.67
80.1
40-140
1.98
30
Benzo(k)fluoranthene
138
0.17
mg/Kg wet
1.67
82.7
40-140
1.01
30
2-Chloronaphthalene
1.17
0.34
mg/Kg wet
1.67
70.3
40-140
4.23
30
Chrysene
1.35
0.17
mg/Kg wet
1.67
81.2
40-140
0.760
30
Dibenz(a,h)anthracene
1.40
0.17
mg/Kg wet
1.67
83.9
40-140
2.58
30
Fluoranthene
1.39
0.17
mg/Kg wet
1.67
83.2
40-140
0.480
30
Fluorene
1.34
0.17
mg/Kg wet
1.67
80.2
40-140
1.78
30
Indeno(1,2,3-cd)pyrene
1.44
0.17
mg/Kg wet
1.67
86.4
40-140
1.33
30
2-Methylnaphthalene
1.46
0.17
mg/Kg wet
1.67
87.6
40-140
3.37
30
1-Methylnaphthalene
1.28
0.17
mg/Kg wet
1.67
76.8
40-140
1.86
30
Naphthalene
1.22
0.17
mg/Kg wet
1.67
73.2
40-140
4.41
30
Phenanthrene
1.38
0.17
mg/Kg wet
1.67
82.9
40-140
1.13
30
Pyrene
137
0.17
mg/Kg wet
1.67
82.5
40-140
0.804
30
Surrogate:2-Fluorophenol
5.25
mg/Kg wet
6.67
78.7
30-130
Surrogate: Phenol-d6
5.44
mg/Kg wet
6.67
81.7
30-130
Surrogate: Nitrobenzene-d5
2.50
mg/Kg wet
3.33
75.0
30-130
Surrogate:2-Fluorobiphenyl
3.50
mg/Kg wet
3.33
105
30-130
Surrogate: 2,4,6-Tribromophenol
6.97
mg/Kg wet
6.67
104
30-130
Surrogate:p-Terphenyl-dl4
3.08
mg/Kg wet
3.33
92.4
30-130
Matrix Spike (B248570-MS1)
Source: 19LO710-01
Prepared: 12/18/19 Analyzed: 12/19/19
Acenaphthene
1.40
0.13
mg/Kg dry
2.56
ND
54.8
40-140
Acenaphthylene
1.35
0.13
mg/Kg dry
2.56
ND
52.7
40-140
Anthracene
1.44
0.13
mg/Kg dry
2.56
ND
56.3
40-140
Benzo(a)anthracene
1.44
0.13
mg/Kg dry
2.56
ND
56.2
40-140
Benzo(a)pyrene
1.43
0.13
mg/Kg dry
2.56
ND
55.7
40-140
Benzo(b)fluoranthene
1.48
0.13
mg/Kg dry
2.56
ND
57.9
40-140
Benzo(g,h,i)perylene
1.15
0.13
mg/Kg dry
2.56
ND
44.8
40-140
Benzo(k)fluoranthene
1.52
0.13
mg/Kg dry
2.56
ND
59.2
40-140
Chrysene
1.45
0.13
mg/Kg dry
2.56
ND
56.6
40-140
Dibenz(a,h)anthracene
1.18
0.13
mg/Kg dry
2.56
ND
46.2
40-140
Fluoranthene
1.51
0.13
mg/Kg dry
2.56
ND
58.9
40-140
Fluorene
138
0.13
mg/Kg dry
2.56
ND
54.0
40-140
Indeno(1,2,3-cd)pyrene
1.28
0.13
mg/Kg dry
2.56
ND
50.0
40-140
2-Methylnaphthalene
1.61
0.13
mg/Kg dry
2.56
ND
62.7
40-140
1-Methylnaphthalene
137
0.13
mg/Kg dry
2.56
ND
53.5
40-140
Naphthalene
1.35
0.13
mg/Kg dry
2.56
ND
52.7
40-140
Phenanthrene
1.47
0.13
mg/Kg dry
2.56
ND
57.5
40-140
Pyrene
137
0.13
mg/Kg dry
2.56
ND
53.3
40-140
Surrogate: Nitrobenzene-d5
2.75
mg/Kg dry
5.12
53.6
30-130
Surrogate: Nitrobenzene-d5
2.75
mg/Kg dry
5.12
53.6
30-130
Surrogate:2-Fluorobiphenyl
3.79
mg/Kg dry
5.12
74.0
30-130
Surrogate:2-Fluorobiphenyl
3.79
mg/Kg dry
5.12
74.0
30-130
Surrogate: p-Terphenyl-dl4
3.09
mg/Kg dry
5.12
60.4
30-130
Surrogate: p-Terphenyl-dl4
3.09
mg/Kg dry
5.12
60.4
30-130

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 * FAX [phone] " TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B248570 - SW-846 3546
Matrix Spike Dup (B248570-MSD1)
Source: 19LO710-01
Prepared: 12/18/19 Analyzed: 12/19/19
Acenaphthene
1.16
0.13
mg/Kg dry
2.56
ND
45.4
40-140
18.8
30
Acenaphthylene
1.13
0.13
mg/Kg dry
2.56
ND
44.1
40-140
17.6
30
Anthracene
1.19
0.13
mg/Kg dry
2.56
ND
46.5
40-140
19.0
30
Benzo(a)anthracene
1.24
0.13
mg/Kg dry
2.56
ND
48.4
40-140
15.0
30
Benzo(a)pyrene
1.20
0.13
mg/Kg dry
2.56
ND
46.8
40-140
17.4
30
Benzo(b)fluoranthene
1.22
0.13
mg/Kg dry
2.56
ND
47.7
40-140
19.2
30
Benzo(g,h,i)perylene
0.983
0.13
mg/Kg dry
2.56
ND
38.4 *
40-140
15.5
30 MS-22
Benzo(k)fluoranthene
1.27
0.13
mg/Kg dry
2.56
ND
49.6
40-140
17.8
30
Chrysene
1.21
0.13
mg/Kg dry
2.56
ND
47.4
40-140
17.7
30
Dibenz(a,h)anthracene
1.05
0.13
mg/Kg dry
2.56
ND
41.0
40-140
11.8
30
Fluoranthene
1.25
0.13
mg/Kg dry
2.56
ND
48.9
40-140
18.5
30
Fluorene
1.17
0.13
mg/Kg dry
2.56
ND
45.5
40-140
17.0
30
Indeno(1,2,3-cd)pyrene
1.08
0.13
mg/Kg dry
2.56
ND
42.1
40-140
17.1
30
2-Methylnaphthalene
1.26
0.13
mg/Kg dry
2.56
ND
49.2
40-140
24.1
30
1-Methylnaphthalene
1.09
0.13
mg/Kg dry
2.56
ND
42.4
40-140
23.0
30
Naphthalene
1.04
0.13
mg/Kg dry
2.56
ND
40.5
40-140
26.1
30
Phenanthrene
1.22
0.13
mg/Kg dry
2.56
ND
47.6
40-140
18.9
30
Pyrene
1.16
0.13
mg/Kg dry
2.56
ND
45.2
40-140
16.6
30
Surrogate: Nitrobenzene-d5
2.11
mg/Kg dry
5.12
41.3
30-130
Surrogate: Nitrobenzene-d5
2.11
mg/Kg dry
5.12
41.3
30-130
Surrogate:2-Fluorobiphenyl
2.98
mg/Kg dry
5.12
58.2
30-130
Surogate:2-Fluorobiphenyl
2.98
mg/Kg dry
5.12
58.2
30-130
Surrogate: p-Terphenyl-d14
2.62
mg/Kg dry
5.12
51.1
30-130
Surrogate:p-Terphenyl-dl4
2.62
mg/Kg dry
5.12
51.1
30-130
Batch B248698 - SW-846 3510C
Blank (B248698-BLK1)
Prepared: 12/19/19 Analyzed: 12/20/19
2-Chloronaphthalene
ND
10
µg/L
Surrogate:2-Fluorophenol
0.00
µg/L
200
*
15-110
Surrogate: Phenol-d6
0.300
µg/L
200
0.150 *
15-110
Surrogate: Nitrobenzene-d5
66.4
µg/L
100
66.4
30-130
Surogate:2-Fluorobiphenyl
80.8
µg/L
100
80.8
30-130
Surrogate: 2,4,6-Tribromophenol
0.00
µg/L
200
*
15-110
Surogate:p-Terphenyl-dl4
73.6
µg/L
100
73.6
30-130
LCS (B248698-BS1)
Prepared: 12/19/19 Analyzed: 12/20/19
2-Chloronaphthalene
37.6
10
µg/L
50.0
75.2
40-140
Surrogate:2-Fluorophenol
0.0100
µg/L
200
0.00500 *
15-110
Surrogate: Phenol-d6
0.540
µg/L
200
0.270 *
15-110
Surrogate: Nitrobenzene-d5
79.5
µg/L
100
79.5
30-130
Surogate:2-Fluorobiphenyl
97.6
µg/L
100
97.6
30-130
Surrogate: 2,4,6-Tribromophenol
0.00
µg/L
200
*
15-110
Surogate:p-Terphenyl-dl4
88.0
µg/L
100
88.0
30-130

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 * FAX [phone] " TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B248698 - SW-846 3510C
LCS Dup (B248698-BSD1) Prepared: 12/19/19 Analyzed: 12/20/19
2-Chloronaphthalene
33.4
10 µg/L
50.0
66.9
40-140 11.7 20
Surrogate:2-Fluorophenol
0.0100
µg/L
200
0.00500 *
15-110
Surrogate: Phenol-d6
0.420
µg/L
200
0.210 *
15-110
Surrogate: Nitrobenzene-d5
73.5
µg/L
100
73.5
30-130
Surrogate:2-Fluorobiphenyl
91.0
µg/L
100
91.0
30-130
Surrogate: 2,4,6-Tribromophenol
0.00
µg/L
200
*
15-110
Surrogate:p-Terphenyl-dl4
81.8
µg/L
100
81.8
30-130
Batch B248798 - SW-846 3510C
Blank (B248798-BLK1) Prepared & Analyzed: 12/20/19
Acenaphthene (SIM)
ND
0.30
µg/L
Acenaphthylene (SIM)
ND
0.20
µg/L
Anthracene (SIM)
ND
0.20
µg/L
Benzo(a)anthracene (SIM)
ND
0.050
µg/L
Benzo(a)pyrene (SIM)
ND
0.10
µg/L
Benzo(b)fluoranthene (SIM)
ND
0.050
µg/L
Benzo(g,h,i)perylene (SIM)
ND
0.50
µg/L
Benzo(k)fluoranthene (SIM)
ND
0.20
µg/L
Chrysene (SIM)
ND
0.20
µg/L
Dibenz(a,h)anthracene (SIM)
ND
0.10
µg/L
Fluoranthene (SIM)
ND
0.50
µg/L
Fluorene (SIM)
ND
1.0
µg/L
Indeno(1,2,3-cd)pyrene (SIM)
ND
0.10
µg/L
2-Methylnaphthalene (SIM)
ND
1.0
µg/L
1-Methylnaphthalene (SIM)
ND
1.0
µg/L
Naphthalene (SIM)
ND
1.0
µg/L
Phenanthrene (SIM)
ND
0.050
µg/L
Pyrene (SIM)
ND
1.0
µg/L R-05
Surrogate: Nitrobenzene-d5
67.6
µg/L
100
67.6
30-130
Surrogate: Nitrobenzene-d5 (SIM)
65.6
µg/L
100
65.6
30-130
Surrogate:2-Fluorobiphenyl
59.9
µg/L
100
59.9
30-130
Surrogate: 2-Fluorobiphenyl (SIM)
54.4
µg/L
100
54.4
30-130
Surrogate:p-Terphenyl-dl4
66.2
µg/L
100
66.2
30-130
Surrogate:p-Terphenyl-dl4 (SIM)
56.0
µg/L
100
56.0
30-130
LCS (B248798-BS1)
Prepared & Analyzed:
12/20/19
Acenaphthene (SIM)
40.2
6.0
µg/L
50.0
80.4
40-140
Acenaphthylene (SIM)
37.7
4.0
µg/L
50.0
75.4
40-140
Anthracene (SIM)
43.4
4.0
µg/L
50.0
86.8
40-140
Benzo(a)anthracene (SIM)
42.0
1.0
µg/L
50.0
84.1
40-140
Benzo(a)pyrene(SIM)
42.2
2.0
µg/L
50.0
84.3
40-140
Benzo(b)fluoranthene (SIM)
45.7
1.0
µg/L
50.0
91.4
40-140
Benzo(g,h,i)perylene (SIM)
41.4
10
µg/L
50.0
82.9
40-140
Benzo(k)fluoranthene (SIM)
45.1
4.0
µg/L
50.0
90.2
40-140
Chrysene (SIM)
41.9
4.0
µg/L
50.0
83.9
40-140
Dibenz(a,h)anthracene (SIM)
42.6
2.0
µg/L
50.0
85.1
40-140
Fluoranthene (SIM)
42.3
10
µg/L
50.0
84.7
40-140
Fluorene (SIM)
42.9
20
µg/L
50.0
85.9
40-140
Indeno(1,2,3-cd)pyrene (SIM)
42.2
2.0
µg/L
50.0
84.4
40-140
2-Methylnaphthalene (SIM)
36.0
20
µg/L
50.0
72.1
40-140
1-Methylnaphthalene (SIM)
37.1
20
µg/L
50.0
74.2
40-140
Naphthalene (SIM)
37.8
20
µg/L
50.0
75.7
40-140

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B248798 - SW-846 3510C
LCS (B248798-BS1)
Prepared & Analyzed: 12/20/19
Phenanthrene (SIM)
41.9
1.0
µg/L
50.0
83.9
40-140
Pyrene(SIM)
46.1
20
µg/L
50.0
92.2
40-140
R-05
Surrogate: Nitrobenzene-d5
78.0
µg/L
100
78.0
30-130
Surrogate: Nitrobenzene-d5 (SIM)
73.4
µg/L
100
73.4
30-130
Surrogate:2-Fluorobiphenyl
71.6
µg/L
100
71.6
30-130
Surrogate: 2-Fluorobiphenyl (SIM)
70.5
µg/L
100
70.5
30-130
Surrogate:p-Terphenyl-dl4
70.0
µg/L
100
70.0
30-130
Surrogate: p-Terphenyl-d14 (SIM)
78.3
µg/L
100
78.3
30-130
LCS Dup (B248798-BSD1)
Prepared & Analyzed: 12/20/19
Acenaphthene (SIM)
35.2
6.0
µg/L
50.0
70.5
40-140
13.1
20
Acenaphthylene (SIM)
34.7
4.0
µg/L
50.0
69.3
40-140
8.40
20
Anthracene (SIM)
38.2
4.0
µg/L
50.0
76.4
40-140
12.8
20
Benzo(a)anthracene (SIM)
37.4
1.0
µg/L
50.0
74.8
40-140
11.7
20
Benzo(a)pyrene (SIM)
37.5
2.0
µg/L
50.0
75.0
40-140
11.8
20
Benzo(b)fluoranthene (SIM)
40.6
1.0
µg/L
50.0
81.1
40-140
11.9
20
Benzo(g,h,i)perylene (SIM)
36.8
10
µg/L
50.0
73.6
40-140
11.9
20
Benzo(k)fluoranthene (SIM)
40.1
4.0
µg/L
50.0
80.2
40-140
11.7
20
Chrysene (SIM)
37.4
4.0
µg/L
50.0
74.7
40-140
11.6
20
Dibenz(a,h)anthracene (SIM)
38.0
2.0
µg/L
50.0
75.9
40-140
11.4
20
Fluoranthene (SIM)
35.3
10
µg/L
50.0
70.5
40-140
18.2
20
Fluorene (SIM)
36.0
20
µg/L
50.0
72.1
40-140
17.5
20
Indeno(1,2,3-cd)pyrene (SIM)
37.3
2.0
µg/L
50.0
74.6
40-140
12.3
20
2-Methylnaphthalene (SIM)
31.3
20
µg/L
50.0
62.6
40-140
14.1
20
1-Methylnaphthalene (SIM)
32.5
20
µg/L
50.0
65.0
40-140
13.3
20
Naphthalene (SIM)
32.4
20
µg/L
50.0
64.8
40-140
15.5
20
Phenanthrene (SIM)
37.1
1.0
µg/L
50.0
74.2
40-140
12.2
20
Pyrene(SIM)
34.4
20
µg/L
50.0
68.7
40-140
29.2 *
20 R-05
Surrogate: Nitrobenzene-d5
64.4
µg/L
100
64.4
30-130
Surrogate: Nitrobenzene-d5 (SIM)
63.9
µg/L
100
63.9
30-130
Surrogate:2-Fluorobiphenyl
63.0
µg/L
100
63.0
30-130
Surrogate: 2-Fluorobiphenyl (SIM)
61.1
µg/L
100
61.1
30-130
Surrogate:p-Terphenyl-dl4
60.8
µg/L
100
60.8
30-130
Surrogate: p-Terphenyl-d14 (SIM)
58.5
µg/L
100
58.5
30-130

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Metals Analyses (Total) - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B248645 - SW-846 3050B
Blank (B248645-BLK1)
Prepared: 12/18/19 Analyzed: 12/19/19
Chromium
0.12
4.2
mg/Kg wet
J
Copper
ND
4.2
mg/Kg wet
Lead
ND
1.7
mg/Kg wet
Nickel
ND
4.2
mg/Kg wet
Zinc
ND
8.3
mg/Kg wet
Cadmium
ND
0.33
mg/Kg wet
LCS (B248645-BS1)
Prepared: 12/18/19 Analyzed: 12/19/19
Chromium
99.6
50
mg/Kg wet
101 98.6 82.4-116.8
Copper
62.4
50
mg/Kg wet
63.1 99.0 84.2-115.8
Lead
121
20
mg/Kg wet
125 96.4 82.4-116.8
Nickel
111
50
mg/Kg wet
108 103 82.9-117.6
Zinc
240
100
mg/Kg wet
240 100 80.8-118.8
Cadmium
57.2
4.0
mg/Kg wet
56.2 102 82.9-117.3
LCS Dup (B248645-BSDI)
Prepared: 12/18/19 Analyzed: 12/19/19
Chromium
96.8
49
mg/Kg wet
101 95.9 82.4-116.8
2.79
30
Copper
61.2
49
mg/Kg wet
63.1 96.9 84.2-115.8
2.07
30
Lead
120
20
mg/Kg wet
125 95.7 82.4-116.8
0.775
30
Nickel
110
49
mg/Kg wet
108 102 82.9-117.6
1.11
30
Zinc
237
98
mg/Kg wet
240 98.5 80.8-118.8
1.62
30
Cadmium
56.4
3.9
mg/Kg wet
56.2 100 82.9-117.3
1.37
20
Duplicate (B248645-DUPI)
Source: 19LO710-11
Prepared: 12/18/19 Analyzed: 12/19/19
Chromium
15.1
5.7
mg/Kg dry
15.5
3.01
35
Copper
18.1
5.7
mg/Kg dry
18.9
4.65
35
Lead
18.5
23
mg/Kg dry
19.5
5.54
35
Nickel
4.47
5.7
mg/Kg dry
4.71
5.31
35 J
Zinc
47.4
11
mg/Kg dry
60.3
5.00
35
Cadmium
0.107
0.46
mg/Kg dry
0.113
5.20
35 J
Matrix Spike (B248645-MSI)
Source: 19LO710-11
Prepared: 12/18/19 Analyzed: 12/19/19
Chromium
38.2
23
mg/Kg dry
22.8 15.5 99.4 75-125
Copper
61.5
23
mg/Kg dry
45.6 18.9 93.5 75-125
Lead
41.4
9.1
mg/Kg dry
22.8 19.5 96.0 75-125
Nickel
25.6
23
mg/Kg dry
22.8 4.71 91.7 75-125
Zinc
105
46
mg/Kg dry
45.6 60.3 97.5 75-125
Cadmium
22.4
1.8
mg/Kg dry
22.8 0.113 97.8 75-125
Batch B248713 - SW-846 3005A
Blank (B248713-BLK1)
Prepared & Analyzed: 12/19/19
Cadmium
ND
0.20
µg/L
Chromium
ND
1.0
µg/L
Copper
ND
1.0
µg/L
Lead
ND
0.50
µg/L
Nickel
ND
5.0
µg/L
Zinc
ND
10
µg/L

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Metals Analyses (Total) - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B248713 - SW-846 3005A
LCS (B248713-BSI)
Prepared & Analyzed: 12/19/19
Cadmium
482
2.0
µg/L
500 96.5
80-120
Chromium
483
10
µg/L
500 96.7
80-120
Copper
957
10
µg/L
1000 95.7
80-120
Lead
483
5.0
µg/L
500 96.5
80-120
Nickel
482
50
µg/L
500 96.4
80-120
Zinc
984
100
µg/L
1000 98.4
80-120
LCS Dup (B248713-BSD1)
Prepared & Analyzed: 12/19/19
Cadmium
489
2.0
µg/L
500 97.7
80-120
1.33
20
Chromium
490
10
µg/L
500 98.0
80-120
1.32
20
Copper
963
10
µg/L
1000 96.3
80-120
0.603
20
Lead
495
5.0
µg/L
500 99.0
80-120
2.50
20
Nickel
485
50
µg/L
500 97.1
80-120
0.695
20
Zinc
998
100
µg/L
1000 99.8
80-120
1.41
20
Batch B249387 - SW-846 3005A
Blank (B249387-BLK1)
Prepared & Analyzed: 01/03/20
Hardness
0.0
mg/L
LCS (B249387-BS1)
Prepared & Analyzed: 01/03/20
Hardness
26
mg/L
26.5 98.1
80-120
LCS Dup (B249387-BSD1)
Prepared & Analyzed: 01/03/20
Hardness
26
mg/L
26.5 98.1
80-120
0.0365
20
Duplicate (B249387-DUPl)
Source: 19LO710-09
Prepared & Analyzed: 01/03/20
Hardness
140
mg/L
140
1.21
Matrix Spike (B249387-MS1)
Source: 19LO710-09
Prepared & Analyzed: 01/03/20
Hardness
170
mg/L
26.5 140 101
75-125

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 * FAX [phone] " TEL. [phone]
QUALITY CONTROL
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B248582 - SW-846 7196A
Blank (B248582-BLK1)
Prepared: 12/18/19 Analyzed: 12/19/19
Hexavalent Chromium
LCS (B248582-BS1)
ND
0.16
mg/Kg wet
Prepared: 12/18/19 Analyzed: 12/19/19
Hexavalent Chromium
LCS Dup (B248582-BSD1)
38
0.79
mg/Kg wet
46.9 82.0
Prepared: 12/18/19 Analyzed: 12/19/19
80-120
Hexavalent Chromium
Batch B249020 - SW-846 7196A
40
0.79
mg/Kg wet
47.0 84.2
80-120 2.80 20
Blank (B249020-BLK1)
Prepared & Analyzed: 12/24/19
Hexavalent Chromium
LCS (B249020-BS1)
ND
0.0040
mg/L
Prepared & Analyzed: 12/24/19
Hexavalent Chromium
LCS Dup (B249020-BSD1)
0.093
0.0040
mg/L
0.100 93.0
Prepared & Analyzed: 12/24/19
80-120
Hexavalent Chromium
Matrix Spike (B249020-MSI)
0.094 0.0040 mg/L
Source: 19LO710-17
0.100 94.4
Prepared & Analyzed: 12/24/19
80-120 1.42 20
Hexavalent Chromium
Matrix Spike Dup (B249020-MSD1)
0.065 0.0040 mg/L
Source: 19LO710-17
0.100 ND 65.1 *
Prepared & Analyzed: 12/24/19
75-125 MS-07A
Hexavalent Chromium
0.064
0.0040
mg/L
0.100 ND 64.4 *
75-125 1.03 20 MS-07A

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 * FAX [phone] " TEL. [phone]
FLAG/QUALIFIER SUMMARY
*
QC result is outside of established limits.
fi
Wide recovery limits established for difficult compound.
$
Wide RPD limits established for difficult compound.
#
Data exceeded client recommended or regulatory level
ND
Not Detected
RL
Reporting Limit is at the level of quantitation (LOQ)
DL
Detection Limit is the lower limit of detection determined by the MDL study
MCL
Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
MS-07A Matrix spike and spike duplicate recovery is outside of control limits. Analysis is in control based on laboratory
fortified blank recovery. Possiblity of matrix effects that lead to low bias or non -homogeneous sample aliquot
cannot be eliminated.
MS-22 Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the
two MS/MSD results is within method specified criteria.
R-05 Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any
reported value for this compound.
V-04 Initial calibration did not meet method specifications. Compound was calibrated using a response factor where
%RSD is outside of method specified criteria. Reported result is estimated.
V-05 Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for
this compound.
V-34 Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
V-35 Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this
compound. Reported result is estimated.
W-06 Elevated method reporting limit due to intense color of sample
Z-01 Samples ran passed recommended holding time

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SW-846 6010 in Water
Hardness CTMA,NH,NY
SW-846 6020B in Soil
Chromium
NY,NC,ME
Copper
NY,NC,ME
Lead
NY,NC,ME
Nickel
NY,NC,ME
Zinc
NY,NC,ME
Cadmium
NY,NC,ME
SW-846 6020B in Water
Cadmium
CTNH,NY,RI,ME,VA,NC
Chromium
CT,NH,NY,ME,VA,NC
Copper
CTNH,NY,ME,VA,NC
Lead
CTNH,NY,ME,VA,NC
Nickel
CTNH,NY,ME,VA,NC
Zinc
CTNH,NY,ME,VA,NC
SW-846 7196A in Soil
Hexavalent Chromium
NY,CTNH,NC,ME,VA
SW-846 7196A in Water
Hexavalent Chromium
CTNH,NY,NC,ME,VA
SW-846 8270E in Soil
Acenaphthene
CTNY,NH,ME,NC,VA
Acenaphthene
CTNY,NH,ME,NC,VA
Acenaphthylene
CTNY,NH,ME,NC,VA
Acenaphthylene
CTNY,NH,ME,NC,VA
Anthracene
CTNY,NH,ME,NC,VA
Anthracene
CTNY,NH,ME,NC, VA
Benzo(a)anthracene
CT,NY,NH,ME,NC,VA
Benzo(a)anthracene
CT,NY,NH,ME,NC,VA
Benzo(a)pyrene
CTNY,NH,ME,NC,VA
Benzo(a)pyrene
CTNY,NH,ME,NC,VA
Benzo(b)fluoranthene
CTNY,NH,ME,NC,VA
Benzo(b)fluoranthene
CTNY,NH,ME,NC,VA
Benzo(g,h,i)perylene
CTNY,NH,ME,NC,VA
Benzo(g,h,i)perylene
CTNY,NH,ME,NC,VA
Benzo(k)fluoranthene
CTNY,NH,ME,NC,VA
Benzo(k)fluoranthene
CTNY,NH,ME,NC,VA
2-Chloronaphthalene
CTNY,NH,NC,VA
Chrysene
CTNY,NH,ME,NC,VA
Chrysene
CTNY,NH,ME,NC,VA
Dibenz(a,h)anthracene
CTNY,NH,ME,NC,VA
Dibenz(a,h)anthracene
CTNY,NH,ME,NC,VA
Fluoranthene
CTNY,NH,ME,NC,VA
Fluoranthene
CTNY,NH,ME,NC,VA
Fluorene
NY,NH,ME,NC,VA
Fluorene
CTNY,NH,ME,NC,VA

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
SW-846 8270E in Soil
Indeno(1,2,3-cd)pyrene
CT,NY,NH,ME,NC,VA
Indeno(1,2,3-cd)pyrene
CT,NY,NH,ME,NC,VA
1-Methylnaphthalene
NC
2-Methylnaphthalene
CT,NY,NH,ME,NC,VA
2-Methylnaphthalene
CT,NY,NH,ME,NC,VA
Naphthalene
CT,NY,NH,ME,NC,VA
Naphthalene
CT,NY,NH,ME,NC,VA
Phenanthrene
CT,NY,NH,ME,NC,VA
Phenanthrene
CT,NY,NH,ME,NC,VA
Pyrene
CT,NY,NH,ME,NC,VA
Pyrene
CT,NY,NH,ME,NC,VA
2-Fluorophenol
NC
SW-846 8270E in Water
Acenaphthene
CT,NY,NC,ME,NH,VA
Acenaphthylene
CT,NY,NC,ME,NH,VA
Anthracene
CT,NY,NC,ME,NH,VA
Benzo(a)anthracene
CT,NY,NC,ME,NH,VA
Benzo(a)pyrene
CT,NY,NC,ME,NH,VA
Benzo(b)fluoranthene
CT,NY,NC,ME,NH,VA
Benzo(g,h,i)perylene
CT,NY,NC,ME,NH,VA
Benzo(k)fluoranthene
CT,NY,NC,ME,NH,VA
2-Chloronaphthalene
CT,NY,NC,ME,NH,VA
Chrysene
CT,NY,NC,ME,NH,VA
Dibenz(a,h)anthracene
CT,NY,NC,ME,NH,VA
Fluoranthene
CT,NY,NC,ME,NH,VA
Fluorene
NY,NC,ME,NH,VA
Indeno(1,2,3-cd)pyrene
CT,NY,NC,ME,NH,VA
1-Methylnaphthalene
NC
2-Methylnaphthalene
CT,NYNC,ME,NH,VA
Naphthalene
CT,NY,NC,ME,NH,VA
Phenanthrene
CT,NY,NC,ME,NH,VA
Pyrene
CT,NY,NC,ME,NH,VA
2-Fluorophenol
NC

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
The CON -TEST Environmental Laboratory operates under the following certifications and accreditations:
Code
Description
Number
Expires
AIHA
AIHA-LAP, LLC - ISO17025:2017
100033
03/1/2022
MA
Massachusetts DEP
M-MA100
06/30/2020
CT
Connecticut Department of Publilc Health
PH-0567
09/30/2021
NY
New York State Department of Health
10899 NELAP
04/1/2020
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2020
RI
Rhode Island Department of Health
LAO00112
12/30/2020
NC
North Carolina Div. of Water Quality
652
12/31/2020
NJ
New Jersey DEP
MA007 NELAP
06/30/2020
FL
Florida Department of Health
E871027 NELAP
06/30/2020
VT
Vermont Department of Health Lead Laboratory
LL015036
07/30/2020
ME
State of Maine
2011028
06/9/2021
VA
Commonwealth of Virginia
460217
12/14/2020
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2020
VT-DW
Vermont Department of Health Drinking Water
VT-255716
06/12/2020
NC-DW
North Carolina Department of Health
25703
07/31/2020
PA
Commonwealth of Pennsylvania DEP
68-05812
06/30/2020

Table of Contents
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t 2/17/2019 Track your package or shipment with FedEx Tracking
Table of Contents
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Tuesday 12/17/2019 at 12.35 pry
FROM
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Shipment Facts
TRACKING NUMBER
815336531264
TOTAL. PIECES
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WINDSOR LOCKS, CT
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Table of Contents
Client
Received By
Date i2
N
How were the samples In Cooler No Cooler
received? Direct from Sampling
Time
On Ice i
Ambient
�Z3�—
No Ice
Melted Ice
Were samples within By Gun #
��
11�> Actual Temp -
Temperature? 2-60C By Blank #
Actual Temp -
Was Custody Seal Intact?_
Were Samples Tampered with? �4
Was COC Relinquished ?
Does Chain Agree With Samples?
Are there broken/leaking/loose caps on any samples?
Is COC in ink/ Legible? 1-Were
_
samples received within holding time? 1
Did COC include all Client
Analysis Sampler Name
pertinent Information? Project
ID's - Collection Dates[Times _ --I-- �
Are Sample labels filled out and legible?
Are there Lab to Filters?
Who was notified?
Are there Rushes?
Who was notified?
_
Are there Short Holds? r
Who was notified?
Is there enough Volume?
Is there Headspace where applicable?
MS/MSD?
Proper Media/Containers Used?
Is splitting samples required?
Were trip blanks received?
On COC? F
Do all samples have the proper pH?
Acid h)- Base
. 4
II.
� _ _
Via•-
`�S'�5*"
16 oz Amb.
Unp-
1 Liter Amb.
1 Liter Plastic
HCL-
500 mL Amb.
500 mL Plastic
8oz Amb/Clear
Meoh-
250 mL Amb.
250 mL Plastic
4 Amb Clear
Bisulfate-
Flashpoint
Col./Bacteria
2oz mb/Clear
DI-
Other Glass
Other Plastic
Encore
Thiosulfate-
SOC Kit
Plastic Bag
Frozen:
Sulfuric-
Perchlorate
Ziplock
OEM
Unp-
1 Liter Amb.
1 Liter Plastic
16 oz Amb.
HCL-
500 mL Amb.
500 mL Plastic
8oz Amb/Clear
Meoh-
250 mL Amb.
250 mL Plastic
4oz AmblClear
Bisulfate-
Cal./Bacteria
Flashpoint
2oz AmblClear
DI-
Other Plastic
Other Glass
Encore
Thiosulfate-
SOC Kit
Plastic Bag
Frozen:
Sulfuric-
Perchlorate
Ziplock
%.ommenzs:
TN— 3
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