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HomeMy WebLinkAbout9208_Wake_NCFairgrounds_MSWLF_AnnualGW_FID1343027_20190819ENR USE ONLY: fil L]PaiperR.port ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #: NC DENR Environmental Monitoring Division of Waste Management - Solid Waste Reoortina Form Notice: This form and any information attached to it are "Pubfio Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6), Instructions: Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). Attach a notification table of any groundwater or surface water values that equal or ox000d the reporting limito Attach a notification table of any methane gas values that attain or exceed explosive gas levels This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646 Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): WithersRavenel, Inc (Consultant) Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Matthew James, PG Phone: 919-469-3340 E-mail: mjames@withersravenel.com NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006) rcl sed NC Fairgrounds Landfill Nowell Road, Raleigh, Wake County ) g(Northwest of Intersection with NC 54) �92-08 .1600 GW: July 18, 2019 i Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring ❑X Detection Monitoring Assessment Monitoring U Corrective Action T e of data submitted: (Check all that apply) X Groundwater monitoring data from monitoring wells ❑ Methane gas monitoring data Groundwater monitoring data from private water supply wells ❑ Corrective action data (specify) _ Leachate monitoring data X' Surface water monitoring data ❑ Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration ❑ Yes, a Patifircation of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. 1 am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Matthew James, PG Project Geolgist 919-469-3340 Title 115 MacKenan Drive, Cary, NC 27511 Facility Representative Address C-0832 NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 (Area Code) Telephone Number �gEtHnirf�yr�r Affix NC LlcensSeal sZ _ SEAL = 2310 s ` CO �"+" ' JH i ■■ WithersRavenel ,. Our People. Your Success. August 19, 2019 Jaclynne Drummond, Hydrogeologist Environmental Compliance - Solid Waste Section NC DEQ, Division of Waste Management 1646 Mail Service Center Raleigh, NC 27699-1646 Subject: Summer 2019 Annual Groundwater and Surface Water Monitoring Report Closed NC Fairgrounds Landfill, Permit #92-08, NC Dept of Agriculture and Consumer Services WR Project No. 02000082.20 Ms. Drummond: WithersRavenel (WR) has completed the Summer 2019 Annual Groundwater and Surface Water monitoring event at the above referenced facility. The scope of work performed by WR included groundwater sample collection from existing groundwater monitoring wells and surface water sample collection along Richland Creek in accordance with the North Carolina Department of Environment Quality (NCDEQ) approved Water Quality and Landfill Gas Monitoring Plan dated September 2008, which will be referenced as "The Plan" throughout this report. The closed NC Fairgrounds Landfill is located approximately four miles west of downtown Raleigh and approximately 1,600 feet northeast of the intersection of NC Highway 54 (Chapel Hill Road) and Nowell Road (Figure 1). The facility was permitted as a sanitary landfill on August 9, 1982 (Permit #92-08). According to documentation reviewed by WR, the closed landfill was operated between approximately 1982 and 1988. Samples from five groundwater monitoring wells and two surface water collection points are intended to be collected and tested on annual basis in accordance with The Plan and correspondence received from the Department of Waste Management. The following paragraphs summarize the event which took place on July 18, 2019. Cordially, WithersRavenel Austin Pote G. Matthew James, P.G. Staff Engineer Senior Geologist 115 MacKenan Drive I Cary, NC 275111 tel.: 919.469.3340 1 fax: 919.467-6008 1 www.withersravenel.com I License No. C-0832 1410 Commonwealth Drive Suite 1011 Wilmington, NC 28403 1 tel: 910.256.9277 1 fax: 910.256.2584 416 Gallimore Dairy Road Suite D I Greensboro, NC 27409 1 tel: 336.605.3009 1 fax: 919.467.6008 Closed NC Fairgrounds Landfill Annual Groundwater and Surface Water Monitoring Report WR Project No.: 02000082.20 August 2019 1.0 WATER QUALITY SAMPLING METHODOLOGY 1.1 Groundwater Sampling Five groundwater monitoring wells, MW-1, MW-2, MW-3, MW-4, and MW-5, were installed at the site in November 2000 at locations proximal to two waste areas. Figure 2 illustrates the locations of the waste boundary and monitoring wells. Monitoring well construction details are summarized in Table 1 and copies of the boring logs and well completion reports for the monitoring wells are included as Appendix A. Groundwater sampling activities were performed on July 18, 2019 in accordance with protocols detailed in The Plan. Prior to monitoring well gauging, each monitoring well was opened to allow water levels to equilibrate to atmospheric pressure. Water levels within each monitoring well were then measured using a decontaminated electronic water level meter. Groundwater elevation measurements were referenced to the top of the well casing. The groundwater elevations were calculated to range from 411.90 to 437.54 feet above mean sea level (MSL) for this sampling event. The July 18, 2019 groundwater elevation data is summarized in Table 1 and a Groundwater Potentiometric Map is included as Figure 2. Each monitoring well was purged using the low -flow technique. During the purging process, turbidity was monitored until a clarity less than 10 Nephelometric Turbidity Units (NTU) was achieved. Final turbidity measurements were recorded in the field notes. Copies of the field notes are included as Appendix B. Following purging activities, groundwater samples were collected using the same polyethylene tubing used to purge the wells. Groundwater samples were decanted into laboratory provided bottleware and immediately placed into an ice -chilled cooler. Collected samples were shipped under proper chain -of - custody to ENCO Labs in Cary, NC for analysis of volatile organic compounds (VOCs) by EPA Method 8260B, the eight RCRA metals by EPA Method 6010D and 7470A, and 1,4-Dioxane by EPA Method 8260B SIM. 1.2 Surface Water Sampling Surface water samples were also collected on July 18, 2019 from monitoring points designated as SA-1 and SA-2, located along Richland Creek. SA-1 is considered the upstream sampling location (approximately 35' 47' 28" North and 78' 43' 43" West) and SA-2 is considered the downstream sampling location (approximately 35' 47' 31" North and 78' 43' 37" West). To preserve the integrity of the preservatives within the sample containers, a properly decontaminated Teflon' ladle was used to collect the surface water samples. The contents of the ladle were immediately decanted into laboratory provided bottleware. The samples were then placed into ice -chilled coolers and shipped under proper chain -of - custody to ENCO Labs in Cary, NC for analysis of volatile organic compounds (VOCs) by EPA Method 8260B, the eight RCRA metals by EPA Method 6010D and 7470A, and 1,4-Dioxane by EPA Method 8260B SIM. Page 2 Closed NC Fairgrounds Landfill Annual Groundwater and Surface Water Monitoring Report WR Project No.: 02000082.20 August 2019 2.0 LABORATORY ANALYTICAL RESULTS Julv 2019 - Groundwater and Surface Water SamalinR Event The following analytical results exceeded the North Carolina 2L Standard. • MW-3: Selenium - 76.4 µg/L Laboratory results for the analytes identified in the July 2019 samples are summarized in Table 2. Copies of the laboratory analytical reports are included as Appendix C. Page 3 Closed NC Fairgrounds Landfill Annual Groundwater and Surface Water Monitoring Report WR Project No.: 02000082.20 August 2019 3.0 SUMMARY OF REGULATORY EXCEEDANCES AND CONCLUSIONS Groundwater and Surface Water Monitoring: • No targeted VOC compounds were detected at concentrations that exceeded their NC 2L Standard. • MW-3 had a detection Selenium above NC 2L Standards. If you have any questions or require additional information concerning this Report and the request to pursue incident closure, please do not hesitate to contact us at (919) 469-3340. The next annual groundwater and surface water monitoring event for the Closed NC Fairgrounds Landfill is planned to occur in Summer 2020. Sincerely, WithersRavenel Austin Pote G. Matthew James, P.G. Staff Engineer Senior Geologist cc: Mr. Richard Clark, richard.clark@ncagr.gov, NCDACS Page 4 TABLES Table 1 Monitoring Well and Groundwater Data Closed NC Fairgrounds Landfill Wake County, North Carolina WithersRavenel Project # 2000082.20 GW Monitoring Ground Surface TOC Depth to Water in Elevation in Well Depth Screen Well Northing Easting Elevation Elevation in Feet Below TOC Feet MSL in Feet Bls Interval in in Feet MSL Feet MSL Feet BLS 7/18/2019 7/18/2019 MW-1 743884.26 2079242.17 450.9 453.47 15.93 437.54 19 9 t019 MW-2 744085.55 2079482.30 432.1 435.08 5.56 429.52 15 2 to 14 MW-3 743914.97 2080239.77 429.6 432.89 20.99 411.90 25 10 to 25 MW-4 743570.71 2080213.13 433.3 436.21 20.45 415.76 30 11 to 26 MW-5 j 744186.3297 j 2079598.90 j 431.8 j 433.59 j 15.80 j 417.79 j 25 j 8 to 23 Notes: BLS = Below the Land Surface MSL = Mean See Level TOC = Top of Casing All wells constructed of two (2)-inch PVC Page 1 of 1 TABLE 2 Summary of Detected Parameters in Groundwater and Surface Water Closed NC Fairgrounds Landfill Wake County, North Carolina WithersRavenel Project # 2000082.20 ORGANIC MW-1 MW-2 MW-3 MW-4 MW-5 SA-1 SA-2 NC 2L Limit CONSTITUENTS (µg/L) Sample Date 7/18/2019 7/18/2019 7/18/2019 7/18/2019 7/18/2019 7/18/2019 7/18/2019 VOCS All Non -Detect NA INORGANIC CONSTITUENTS Arsenic <7.60 <7.60 <7.60 <7.60 <7.60 <7.60 <7.60 10 Barium 16.7 152 195 35.8 35.2 39.5 23.7 700 Cadmium <0.360 0.69 <0.360 0.586 <0.360 <0.360 <0.360 2 Chromium <1.40 <1.40 2.35 <1.40 <1.40 <1.40 <1.40 10 Lead <3.10 <3.10 <3.10 <3.10 <3.10 <3.10 <3.10 15 Selenium <6.20 <6.20 76.4 <6.20 <6.20 <6.20 <6.20 20 Silver <1.90 <1.90 <1.90 <1.90 <1.90 <1.90 <1.90 20 Mercury <0.150 <0.150 <0.150 <0.150 <0.150 <0.150 <0.150 1 Notes: Qualifiers: J - The identification of the analyte is acceptable; the reported value is an estimate. B - The same analyte is found in the associated blank. NIL = Not Listed All Concentrations reported in tag/L (Parts per Billion) Concentrations in BOLD Exceed the Labortory Detection Limit Concentrations in BOLD and Shaded Exceed the NC 2L Standard MW = Monitoring Well Designation SA = Surface Water Designation Page 1 of 1 TABLE 3 LANDFILL GAS PROBE DATA Closed NC Fairgrounds Landfill Wake County, North Carolina WithersRavenel Project # 2000082.20 Ground Surface Screen Methane Probe Depth in Northing Easting Elevation in Feet Interval in Probe feet BLS MSL Feet BLS LFG-1 743753.92 2079430.96 460.3 10 3 to 10 LFG-2 743748.48 2079583.23 456.0 10 3 to 10 LFG-3 743746.98 2079796.58 449.7 10 3 to 10 LFG-4 743697.32 2079878.36 441.1 10 2.5 to 9.5 LFG-5 743581.77 2079872.59 436.0 10 3 to 9 LFG-6 743440.17 2079870.99 445.0 10 3 to 10 LFG-7 ND ND ND 10 3 to 10 LFG-8 ND ND ND 12 2 to 12 LFG-9 ND ND ND 10 3 to 10 Notes: BLS = Below the Land Surface MSL = Mean See Level ND = Not Defined All Probes are constructed of 1.25-inch PVC Page 1 of 1 FIGURES I u r f Jr Mount Ve`r\no\n FllttSBO(. rN - w U 4 � � LU TRWI T-Y_--Rp r WESTCf �i .Western � om jti62? u t k-ja GRAPHIC SCALE r— . r 0 500 1000 Q00 1 inch =1000 ft. 1/ CLOSED NC FAIRGROUNDS DRAWN BY: SCALE: FIGURENO.: WithersRavenel LANDFILL AP 1"=1000' 1 I / Engineers I Planners I Surveyors RALEIGH, WAKE COUNTY, NORTH CAROLINA APPROVED BY: DATE: PROJECTNO.: 1.-1-1, ,NC,,,11 1-1,1-1:-GENERAL LOCATION MAP mi 07/24/2017 0200082.20 k\00\00-080\0008222-9a1e !y w4a Mo Qo6"\Praj\2016 9a A Y Eaa1\6d1 YM R wt - i\uSOS -1:14 �w"- JJ7 24, 2017 - PO7E, AUSM PROPERTY TINE --------------- 04 sit 00 ^-I b o N ° O a w G o td - 0 O O Ol O N Z3 h r � 1 N N e�-r oo oo I 6 4 m rLLLZ Q o Y o a $ PROPERTY LINE MW-5 '" 420 0 425 417.79 430^ MW-2 7\ 42952 435 440 \ \0 M W` 437.54 L F G - 8 LFG-7 y� `LFG-9 —LFG-E LFG-1 \ \ �VLD E fEF" YONF11 Po Q H ems' 41O i _ M W - 3 415 411.90 \ ' JLFG-3 r SA-2 u LEGEND GROUNDWATER ELEVATION CONTOUR LANDFILL PROPERTY BOUNDARY PROPERTY LINES FOR ADJACENT PARCELS CENTERLINE OF DRAINAGE FEATURE FEATURE (ROAD 0 (ROADS,, STRUCTURES, ETC.) W 0 W F d Q W � j 9 0 J J LL LFG-4 OBSERVED U OF BURIED WASTE inz O MW-1 EXISTING (A u _ �pLFG-5 101 GROUNDWATER MONITORING WELL in = •,rr--,; $ MW-4 Z o EXISTING LANDFILL GAS (METHANE) z O 415.76 LFG-1 9 MONITORING PROBE 0 z \ Ov SA-1 0 SURFACE WATER MONITORING LOCATION LFG-G ° Q Y LL Q l7 NOTE. N P 1. TOPOGRAPHIC, PLANIMETRIC, AND PROPERTY UNE INFORMATION 0 FURNISHED 13Y CITY OF RALEIGH GIS. V 2. PROPERTY LINE TAKEN FROM CITY OF RALEIGH GIS. 3. GROUNDWATER MONITORING WELLS AND LANDFILL GAS MONITORING PROBE LOCATIONS SURVEYED BY WITHERSRAVENEL. 4. 2013 AERIAL OBTAINED FROM LOCAL GIS SOURCES. ^ , 0 ^C W SA-1 pro S L.L v EXISTING EDWARDS MILL ROAD RIGHT-OF-WAY W � 41 � � u w 6 GRAPHIC SCALE 200 0 100 200 400 ft. , APT 1 inch = 200 APPENDIXA MONITORING WELL INSTALLATION RECORDS rvrraEns& RA L LOG OF BORING MWA urve Engineering & Surveying, Inc ill MacKanan Drive -Cary. N.C. Z7511 w.uxE+S��� (Page 1 of 1) Dept. of Agriculture/State Fair Date Started : 11/6/2000 Drilling Company : GeoTechnologies, Inc. Nowell Road Date Completed : 11110/2000 Northing Coord. : NIA Raleigh, NC Hole Diameter : 8.5 in. Easting Coord. : NIA Project # 200082.0 Dolling Method : H.SA_ Survey By : WRES Sampling Method : Split Spoon Logged By : Ty Colwell U Depth = in o) 9 Feet OUT 0 S 10 M 1 20 DESCRIPTION Stiff to very stiff Micaceous CLAYEY SANDY SILT, Red, Pink, Gray and Gold Layers Boring terminated at 19.0 feet. Installed groundwater monitoring well. = Well: MW-1 H o - Elev.:450.85 U FID CL E o iPPm) Cover cf6n m o t fl 5 1 6 7 .I [�—Casing Bentonite pack Well Construction Information WELL CONSTRUCTION Date Compl. :11/10/2000 Hole Dia. : 8.5 in. Drill. Method : HSA Company Rep. WELL CASING Material : Sch 40 PVC Diameter : 2 in. Joints : threaded WELLSCREEN Material : Sch 40 PVC Diameter : 2 in. Joints : threaded Opening :.010 slot SAND PACK: medium SEAL : bentonite NOTES Groundwater is approx. 11.6 feet below ground surface. Top of casing is 2.62 feet above ground surface. Elevation shown is ground surface elevation. North Carolina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section 1636 Mail Service Center - Raleigh, N.C. 276941636-Phone (919) 733.3221 WELL CONSTRUCTION RECORD WELL CONTRACTOR: GeoTechnologies, Inc. WELL CONSTRUCTION CERTIFICATION #: 2504 MW-1 STATE WELL CONSTRUCTION PERMIT #: 2504 1. WELL USE (Check Applicable Box): Municipal ❑ Industrial ❑ Agricultural ❑ Monitoring Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use: 2. WELL LOCATION: (Show sketch of the location below) Nearest Town: Raleigh County: Nowell Road (Road Name and Numbers, Community, or Subdivision and Lot No.) 3. OWNER: Department of Aadculture/ State Fair Address: 1025 Blue Ridge Road Raleigh NC 27607 (City or Town) (State) (Zip Code) 4. DATE DRILLED 11/6/2000 5. TOTAL DEPTH 19.0 6. CUTTINGS COLLECTED YES❑ NO® 7. DOES WELL REPLACE EXISTING WELL? YES❑ NO® 8. STATIC WATER LEVEL Below Top of Casing) 11.6 R. (Use "+" 9 Above Top of Casing) 9. TOP OF CASING IS +2.62 Ft above Land Surface* Top orcasing lertninated attor below land surface requires a variance In Accordance YAM 15A NCAV ZC.0778 10. YIELD (gpm) N/A METHOD OF TEST N/A 11. WATER ZONES (depth) N/A 12. CLORINATION: Type N/A Amount N/A 13. CASING Depth. Diameter Wall Thickness Material Or Weight/Ft. From 9.0 To +2.62 Ft. 2" Sch.40 PVC From To Ft. From To Ft. 14. GROUT Depth Material Method From 5.0 To 0.0 Ft. Neat Cement Pump & Trim From To Ft. 15. SCREEN Depth Diameter Slot Size Material From 19.0 To 9.0 Ft. 2 In 0.010 In PVC From To Ft. In In From To Ft. In In 16. SAND/GRAVEL PACK: Depth Size Material From 19.0 To 7.0 FL #2 Sand From To Ft. 17. REMARKS: Bentonite Plug from 7.0 feet to 5.0 feet. Wake DRILLING LOG From To DEPTH Formation Description 0.0 3" Topsoil 3" 19.0 Micaceous clayey sandy silt, red, pink, gray; and gold layers If additional space is needed use back of form. LOCATION SKETCH (Show direction and distance from at least two State Roads, or other map reference points) I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY 0 THI` S/RECORDV N PROVIDED TO THE WELL OWNER. FOR OFFICE USE ONLY (S NATUR OF PERSO CONSTRUCTING THE WELL) (DATE) Quad no: Submit original to Division of Water Quality, Groundwater Section within 30 days. Serial No. o- WITHERS & RAVENEL LOG OF BORING M W-2 Engineering & Sarveyiag, Ine 111 MacKenan Drive • Cary, N.C. 27511 wmrExs� (Page 1 of 1) Dept. of AgricultureiState Fair Date Started : 111712000 . Drilling Company : GeoTechnologhes, Inc. Nowell Road Date Completed : 1111012000 Northing Coord. : N/A Raleigh, NC Hole Diameter : 8.5 in. Easting Coord. : N/A Project # 200082.0 Drilling Method : H.S.A. Survey By : WRES Sampling Method : Split Spoon Lagged By : Ty Colwell U Depth z in m Q Feet aj OC a � 0 2 3] SM 5 7 SM 9 10 SM 11 12 13 SM Cr Iw 0 m 3 15 N m O O 16 0 0 rr d 17 CD z w 18 S 19 N N �n DESCRIPTION Soft Micaceous CLAYEY Red, Light Gray and White Stiff Micaceous CLAYEY SANDY SILT, Dark, Medium and Light Brown Layers Stiff Micaceous SANDY SILT, Gold and Light Brown SILT, Gold, Gray, Brown and White Layers Boring terminated at 15.0 feet. Installed groundwater monitoring well. Well: MW-2 y 0 FID Elev.:432.06 E o (PPIM) �— Cover ca m m D 1 Cash Grout 10i=1 4 2 7 6 3 3 7 12 Bentonite Screen Sand pack Well Construction Information WELL CONSTRUCTION Date Compl.: 11/10/2000 Hole Dia. : 8.5 in. Drill. Method : HSA Company Rep. WELL CASING Material : Sch 40 PVC Diameter : 2 in. Joints : threaded WELL SCREEN Material : Sch 40 PVC Diameter : 2 in. Joints . threaded Opening :.010 slot SAND PACK: medium SEAL : bentonite NOTES Groundwater is approx. 1.8 feet below ground surface. Top of casing is 3.02 feet above ground surface. Elevation shown is ground surface elevation. North Carol ina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section 1636 Mail Service Center - Raleigh, N.C. 27699-1636-Phone (919) 733-3221 WELL CONSTRUCTION RECORD WELL CONTRACTOR: GeoTechnologies, Inc. WELL CONSTRUCTION CERTIFICATION #: 2504 '-2 STATE WELL CONSTRUCTION PERMIT #: 2504 1. WELL USE (Check Applicable Box): Municipal ❑ Industrial ❑ Agricultural ❑ Monitoring Recovery 0 Heat Pump Water Injection ❑ Other ❑ If Other, List Use: 2. WELL LOCATION: (Show sketch of the location below) Nearest Town: Raleigh County: Wake Nowell Road (Road Name and Numbers, Community, or Subdivision and Lot No.) M]%V-2 3. OWNER: Department of Aadculture/ State Fair Address: 1025 Blue Ridge Road Raleigh NC 27607 (City or Town) (State) (Zip Code) 4. DATE DRILLED 11M2000 5. TOTAL DEPTH 15.0 6. CUTTINGS COLLECTED YES❑ NON 7. DOES WELL REPLACE EXISTING WELL? YES❑ - NO® 8. STATIC WATER LEVEL Below Top of Casing) 1.8 Ft. (Use "V if Above Top of Casing) 9. TOP OF CASING IS +3.02 Ft above Land Surface* 'Top olcaft lemAnated atlor below land surface requires a variance In Accordance Wilb 15A NCAV 2C.0118 10. YIELD (gpm) N/A METHOD OF TEST 11. WATER ZONES (depth) N/A 12. CLORINATION: 13. CASING Depth From 2.0 To +3.02 From To From To 14. GROUT Depth From 5.0 To 0.0 From To 15. SCREEN Depth From 14.0 To 2.0 From To _ From To ype WA Amount WA N/A DRILLING LOG From To DEPTH Formation Description 0.0 3" Topsoil 3" 7.0 Mic cl. sandy silt, red, It. gry., & white 7.0 9.5 Mic. cl. sandy silt, dark, med. and light brown layers 9.5 11.0 Mic. sd . silt, white, gold & light brown layers 11.0 15.0 Mic. cl. sandy silt, gold, gray, brown and white layers If additional space is needed use back of form. Diameter Wall Thickness Material LOCATION SKETCH Or Weight/Ft (Show direction and distance from at least two State Ft. 2" Sch. 40 PVC Roads, or other map reference points) FL Ft. Material Method Ft. Neat Cement Pump & Trim FL Diameter Slot Size Ft. 2 In 0.010 Ft. In R. In 16. SAND/GRAVEL PACK: Depth From 15.0 To 1.5 FL From To FL Size #2 Sand 17. REMARKS: Bentonite Plug from 1.5 feet to 1.25 feet. Material In PVC In In Material I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY S I CORD S PROVIDED TO THE WELL OWNER. FOR OFFICE USE ONLY (S19NATURE OF PERSO CONSTRUCTING THE WELL) (DATE) Quad no: Submit original to Division of WaterQuality, Groundwater Section within 30 days. Serial No. RURERS & RAVENEL LOG OF BORING MW 3 Engineering&Surveying,Inc 111 MacKenan Orive . Cary, N.C. 27511 irmreRr� (Page 1 of 1) Dept. of Agriculture/State Fair Date Started : 11/8/2000 Drilling Company : GeoTechnologies, Inc. Nowell Road Date Completed : 11/10/2000 Northing Coord. : N/A Raleigh, NC Hole Diameter Drilling Method Sampling Method : 8.5 in. Easting Coord. : H.SA. Survey By : Split Spoon Logged By : N/A : WRES : Ty Colwell Project # 200082.0 U Depth = in U Feet j 0 _ . 1 1 20 SM SM SM SM DESCRIPTION SANDY SILT, Brown Very Stiff to stiff Micaceous SANDY SILT with traces of PARTIALLY WEATHERED ROCK, Red, Gold, Gray and Light Brown Layers SILT, Brown, Gold, Gray and Light Brown Layers traces of PARTIALLY WEATHERED ROCK, Gray and Brown Boring terminated at 25.0 feet. Installed groundwater monitoring well_ Well: MW-3 y o' Elev.:429.63 U FID E o (ppm) Cover rn in 0 1 5 5 6 3 4 5 5 II 5 k Well Construction Information WELL CONSTRUCTION Date Compl.: 11/10/2000 Hole Dia. : 8.5 in. Drill. Method . HSA Company Rep. WELL CASING Material : Sch 40 PVC Diameter : 2 in. Joints : threaded WELL SCREEN Material : Sch 40 PVC Diameter : 2 in. Joints : threaded Opening :.010 slot SAND PACK: medium SEAL : bentonite NOTES Groundwater is approx_ 19.9 feet below ground surface. Top of casing is 3.26 feet above ground surface. Elevation shown is ground surface elevation. North Carolina- Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section 1636 Mail Service Center - Raleigh, N.C_ 27699-1636-Phone (919) 733-3" 1 WELL CONSTRUCTION RECORD WELL CONTRACTOR: GeoTechnologies, Inc. WELL CONSTRUCTION CERTIFICATION #: 2504 MW-3 STATE WELL CONSTRUCTION PERMIT #: 2504 1. WELL USE (Check Applicable Box): Municipal ❑ Industrial ❑ Agricultural ❑ Monitoring Recovery ❑ Heat Pump Water Injectibn ❑ Other ❑ If Other, List Use: 2. WELL LOCATION: (Show sketch of the location below) Nearest Town: Raleigh County: Wake Nowell Road (Road Name and Numbers, Community, or Subdivision and Lot No.) MW-3 3. OWNER: Department of Agriculture/ State Fair Address: 1025 Blue Ridge Road Raleigh NC 27607 (City or Town) (State) (Zip Code) 4. DATE DRILLED 11/8/2000 5. TOTAL DEPTH 25.0 . 6. CUTTINGS COLLECTED YES[:] NO® 7. DOES WELL REPLACE EXISTING WELL? YES[:] NO® 8. STATIC WATER LEVEL Below Top of Casing) 19.9 Ft. (Use "+' if Above Top of Casing) 9. TOP OF CASING 1S +3.26 Ft above Land Surface" 'rop of rasing term nated allar below land surface requires a variance In Accordance Wdh 15A NCAV 2C.0118 10. YIELD (gpm) N/A METHOD OF TEST 11. WATER ZONES (depth) N/A N/A 12. CLORINATION: Type N/A Amount N/A 13. CASING Depth Diameter Wall Thickness Material Or Weighl/Ft. From 10.0 To +3.26 Ft 2" Sch.40 PVC From To Ft From To Ft 14. GROUT Depth Material Method From 6.5 To 0.0 Ft. Neat Cement Pump & Trim From To Ft. 15. SCREEN Depth Diameter Slot Size Material From 25.0 To 10.0 R. 2 In 0.010 In PVC From To Ft. In In From To Ft In In 16. SAND/GRAVEL PACK: Depth Size Material From 25.0 To 8.5 FL #2 Sand From To Ft. 17. REMARKS: Bentonite Plug from 8.5 feet to 6.5 feet. DRILLING LOG From To DEPTH Formation Description 0.0 3" Topsoil 3" 3.0 Mic. sandy silt, br. 3.0 13.5 Mic. sandy silt with traces of P.W.R, red, gold, gray and light brown layers 13.5 23.5 Mic. sandy silt, br., gld., gry. & It. br. 23.5 25.0 Mic. sandy silt with traces of P.W.R, gray and brown If additional space is needed use back of form. LOCATION SKETCH (Show direction and distance from at least two State Roads, or other map reference points) I DO HEREBY CERTIFY THATTHIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY R CORD H B PROVIDED TO THE WELL OWNER. /Z /j 2oao FOR OFFICE USE ONLY (SIdNATURff OF PERSON dONSTRUCTING THE WELL) (DATE) Quad no: Submit original to Division of Water Quality, Groundwater Section within 30 days. c ,.;. t h l P WITHERS & RA MVEL Engineering &Surveying, Inc LOG OF BORING MW-4 WIdiPRSkRAYFYHl 711 MacKenm Drive - Cary, N.C.27511 (Page 1 of 1) Dept of Agriculture/State Fair Date Started : 11/7/2000 Drilling Company : GeoTechnologies, Inc. Nowell Road Date Completed :11/1012000 Northing Coord. : NIA Raleigh, NC Hole Diameter : 8.5 in. Easting Coord. : N/A Project # 200082.0 Drilling Method : H.SA Survey By : WRES Sampling Method : Split Spoon Logged By : Ty Colwell U Depth in m Q Feet � rC 0 5 10 ML 15 z 0 25 m N m oO_ O O z a 30 Q z w N N 35 SM DESCRIPTION and Light Brown Layers ~ V Well: MW-4 0 FID Elev.:433.33 E o (ppm) Cover CU co m o 1 fl F2]1 66 91 ❑ 6 I 7 ❑I 8 Stiff Micaceous SANDY SILT with ❑ 4 traces of PARTIALLY WEATHERED 5 s 8 ROCK, Red, Gray, Gold and Light Brown Layers Boring terminated at 30.0 feet. Installed groundwater monitoring well. Grout Casing Bentonite Screen Sand pack Well Construction Information WELL CONSTRUCTION Date Compl.: 11/1012000 Hole Dia. : 8.5 in. Drill. Method : HSA Company Rep. WELL CASING Material : Sch 40 PVC Diameter :2 in. Joints :threaded WELL SCREEN Material : Sch 40 PVC Diameter : 2 in. Joints : threaded Opening :.010 slot SAND PACK: medium SEAL : bentonite NOTES Groundwater is approx. 18.5 feet below ground surface. Top of casing is 2.88 feet above ground surface. Elevation shown is ground surface elevation. North Carolina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section 1636 Mail Service Center - Raleigh, N.C. 27699-1636-Phone (919) 733-3221 ` WELL CONSTRUCTION RECORD WELL CONTRACTOR: GeoTechnolociees, Inc. WELL CONSTRUCTION CERTIFICATION #: 2504 MW-4 STATE WELL CONSTRUCTION PERMIT #: 2504 1. WELL USE (Check Applicable Box): Municipal ❑ Industrial ❑ Agricultural ❑ Monitoring Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use: 2. WELL LOCATION: (Show sketch of the location below) Nearest Town: Raleigh County: Wake Nowell Road (Road Name and Numbers, Community, or Subdivision and Lot No.) MW-4 3. OWNER: Department of Aariculturel State Fair Address:. 1025 Blue Ridge Road Raleigh NC 27607 (City or town) (State) (Zip Code) 4. DATE DRILLED 11I712000 5. TOTAL DEPTH 30.0 6. CUTTINGS COLLECTED YES[!] NO® 7. DOES WELL REPLACE EXISTING WELL? YES[:] NO® 8. STATIC WATER LEVEL Below Top.of Casing) 18.5 Ft. (Use'+"d Above Top of Casing) 9. TOP OF CASING IS +2.88 Ft above Land Surface* 'Top of rasing tordnated atror bebw land surface requires a variance In Accordance WAh 15A NCAV 2C.0118 10. YIELD (gpm) NIA METHOD OF TEST 11. WATER ZONES (depth) NIA WA 12. CLORINATION: Type NIA Amount NIA 13. CASING Depth Diameter Wall Thickness Material Or WeightiFt From 11.0 To +2.88 Ft. 2" Sch.40 PVC From To Ft. From To FL 14. GROUT Depth Material Method From 7.0 To 0.0 Ft. Neat Cement Pump & Trim From To Ft 15. SCREEN Depth Diameter Slot Size Material From 26.0 To 11.0 FL 2 In 0.010 In PVC From To Ft In In From To Ft In In 16. SAND/GRAVEL PACK: Depth Size Material From 30.0 To 9.0 Ft. #2 Sand From To FL 17. REMARKS: Bentonite Pluq from 9.0 feet to 7.0 feet. DRILLING LOG From To DEPTH Formation Description 0.0 3" Topsoil 3" 23.5 Micaceous silt, purple, gold, red and light brown layers 23.5 30.0 Micaceous sandy silt with traces of partially weathered rock, red, gray, gold and light brown layers If additional space is needed use back of form. LOCATION SKETCH (Show direction and distance from at least two State Roads, or other map reference points) I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS RECORD HAS-BEEN.PROVIDED TO THE WELL OWNER. /2 /3 2000 FOR OFFICE USE ONLY (SIGNATURE OV PERSON C NSTRUCTING THE WELL) (DATE) Quad no: Submit original to Division of Water Quality, Groundwater Section within 30 days. WITHERS & RAYENEL Engineering & Surveying, fne- LOG OF BORING M W-5 111 MacKsnan Drive - Cary, N.C. 27511 wrffreRsrr�� (Page 1 of 1) Dept. of Agricutture/State Fair Date Started : 11f7/2000 Drilling Company : Geo-rechnologies, Inc. Nowell Road Date Completed : 11/1012000 Northing Coord. : N/A Raleigh, NC Hole Diameter : &5 in. Easting Ccord. : N/A Project # 200082.0 Drilling Method : H-SA Survey By : WRES Sampling Method : Sprit Spoon Logged By : Ty Colwell U Depth r in o7 a Feet � � U 0 ALI 5 SM 10 DESCRIPTION Stiff Micaceous SILT, Brown Stiff to very stiff Micaceous SAND SILT, Gray, Gold and Light Brown Layers c Well: MW-5 F!D Elev.:431.77 E U o c(PPm) Cover `o m o 1 F I 3 3 4 15 Medium Stiff Micaceous SANDY SILT 5 with traces of PARTIALLY WEATHERED ROCK, Red, Gray, Gold and Light Brown Layers 20� SM Boring terminated at 25.0 feet. Installed groundwater monitoring well. El 3 Screen Sand Pack Well Construction Information WELL CONSTRUCTION Date Compl. :1111012000 Hole Dia. : 8.5 in. Drill. Method : HSA Company Rep. WELL CASING Material : Sch 40 PVC Diameter : 2 in. Joints : threaded WELL SCREEN Material : Sch 40 PVC Diameter : 2 in. Joints : threaded Opening :.010 slot SAND PACK: medium SEAL : bentonite NOTES Groundwater is approx. 12.9 feet below ground surface. Top of casing is 1.82 feet above ground surface. Elevation shown is ground surface elevation. V Ngrth Carolina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section 1636 Mail Service Center - Raleigh, N.C. 276991636-Phone (919) 733-3221 WELL CONSTRUCTION RECORD WELL CONTRACTOR: GeoTechnologies, Inc. WELL CONSTRUCTION CERTIFICATION #: 2504 MW-S STATE WELL CONSTRUCTION PERMIT #: 2504 1. WELL USE (Check Applicable Box): Municipal ❑ Industrial ❑ Agricultural ❑ Monitoring Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use: 2. WELL LOCH 1-ION: (Show sketch of the location below) Nearest Town: Raleigh County: Wake Nowell Road (Road Name and Numbers, Community, or Subdivision and Lot No.) 3. OWNER: Department of AQ6cultur/ State Fair Address: 1025 Blue Ridge Road Raleigh NC 27607 (City or Town) (State) (zip Code) 4. DATE DRILLED 11[7/2000 5. TOTAL DEPTH 25.0 6. CUTTINGS COLLECTED YES[:] NO® 7. DOES WELL REPLACE EXISTING WELL? YES[:] NON 8. STATIC WATER LEVEL Below Top of Casing) 12.9 Ft. (Use "+" if Above Top of casing) 9. TOP OF CASING IS +1.82 Ft above Land Surface* 'Top of casing terminated atlor below land surface requires a variance In Accordance Wilh 15A NCAV 2CD118 10. YIELD (gpm) N/A METHOD OF TEST N/A 11. WATER ZONES (depth) N/A 12. CLORINATION: Type N/A Amount N/A 13. CASING Depth Diameter Wall Thickness Material Or WeighttFt. From 8.0 To +1.82 Ft. 2" Sch.40 PVC From To Ft. From To Ft. 14. GROUT Depth Material Method From 4.0 To 0.0 Ft. Neat Cement Pump & Trim From To Ft. 15. SCREEN Depth Diameter Slot Size Material From 23.0 To 8.0 Ft. 2 In 0.010 In PVC From To Ft. In In From To Ft. In In 16. SAND/GRAVEL PACK: Depth Size Material From 25.0 To 6.0 Ft. #2 Sand From To Ft. 17. REMARKS: Bentonite Plug from 6.0 feet to 4.0 feet. DRILLING LOG From To DEPTH Formation Description 0.0 3n Topsoil 3" 2.0 Mic. silt, brown 2.0 14.5 Mic. sandy silt, gray, gold and light brown layers 14.5 25.0 Micaceous sandy silt with traces of partially weathered rock, red, gray, gold and light brown layers If additional space is needed use back of form. LOCATION SKETCH (Show direction and distance from at least two State Roads, or other map reference points) I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OFITIJJS RECORD S B PROVIDED TO THE WELL OWNER. /2 /3/C»o FOR OFFICE USE ONLY (SI ATURE OF PERSON(CONSTRUCTING THE WELL) (DATE) Quad no: Submit original to Division of Water Quality, Groundwater Section within 30 days. APPENDIX B FIELD NOTES Page of Job Number Groundwater Sampling Form State ID Well ID I. Site Name t., f r I 4...Jf!Date Well Depth Depth to Water . `r Well Diameter Casing Material Screen Length Well Water Volume Sampling Crew Pump Type Tubing Type Intake set at Weather Conditions Notes (eg odor or color) Time Water Level Volume Purged DO Temp EC pH ORP Turbidity KUM Other Parameters Sampled at l rJ Parameters taken with Samples delivered to by at .Analysis VOCs Preservative HCL Bottle ware 40 ml VOAs glass Number of Bottles Hold Time 14 Days SVOCs None 1 Liter glass 7 Days Metals Nitric Acid 250 ml plastic 180 Days NO3+NO2 Sulfuric Acid 125 ml plastic 28 Days Herbicides None 1 Liter glass 7 days Pesticides None 1 Liter glass 7 Days Other Well Volume Ualculat[on 1" well [well depth -depth to water] x 0.0408 gallons/ft. x 3 = 0.124/ft. _ 2" well [well depth -depth to water] x 0.163 gallons/ft. x 3 = 0.489/ft = 4" well [well depth -depth to water] x 0.653 gallons/ft. x 3 = 1.959/ft = C:\Users\jgarrett\Desktop\Revised GW Sampling Form 2016 Page of i! - Your Succe-- Job Number Groundwater Sampling Form State ID ]] � Well ID W 1 Site Name `fGf� ;,("r �,� Date t Well Depth Depth to Water 5,56 Well Diameter Casing Material Screen Length Well Water Volume Sampling Crew Pump Type Tubing Type Intake set at Weather Conditions _ Notes (eg. odor or color) Time Water Level Volume Purged DO Temp EC pH ORP Turbidity 124 Hr.) (from TOM IGals 1 Imnll 1 toM h iC/rm% kfnnHnrr % !m\/1 WTI 1) Other Parameters Sampled at Parameters taken with Samples delivered to rby at Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 14 Days SVOCs None 1 Liter glass 7 Days Metals Nitric Acid 250 ml plastic 180 Days NO3+NO2 Sulfuric Acid 125 ml plastic 28 Days Herbicides None 1 Liter glass 7 days Pesticides None 1 Liter glass 7 Days Other Well Volume Calculation 1 " well [well depth -depth to water] x 0.0408 gallons/ft. x 3 = 0.124/ft. _ 2" well [well depth -depth to water] x 0.163 gallons/ft. x 3 = 0.489/ft = 4" well [well depth -depth to water] x 0.653 gallons/ft. x 3 = 1.959/ft = C:\Users\jgarrett\Desktop\Revised GW Sampling Form 2016 Page of Job Number Groundwater Sampling Form State ID Well ID f-A�_j _ Site Name Date Well Depth _ Depth to Watery '• Well Diameter Casing Material Screen Length Well Water Volume Sampling Crew Pump Type Tubing Type Intake set at Weather Conditions Notes (eg. odor or color) Time Water Level Volume Purged DO Temp EC pH ORP Turbidity (94 Hr )i lfrnm Tnr.7 ft;alc ) tmnll 1 (Cry (Wqh-m) 1&nnrinrrl) IMM W71 i% rl MdM EN utner rarameters Sampled at Samples delivered to Parameters taken with by at Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs HCL 40 ml VOAs glass 14 Days SVOCs None 1 Liter glass 7 Days Metals Nitric Acid 250 ml plastic 180 Days NO3+NO2 Sulfuric Acid 125 ml plastic 28 Days Herbicides None 1 Liter glass 7 days Pesticides None 1 Liter glass 7 Days Other vven volume ua[cu[anon 1 n well [well depth -depth to water] x 2" well [well depth -depth to water] x 4° well [well depth -depth to water] x 0.0408 gallons/ft. x 3 = 0.124/ft. _ 0.163 gallons/ft. x 3 = 0.489/ft = 0.653 gallons/ft. x 3 = 1.959/ft = C:\Users\jgarrett\Desktop\Revised GW Sampling Form 2016 % 0 V f i1 � -n r s R v -, 1 Page of Our Per3ple, Your Success Job Number Groundwater Sampling Form State ID Qp r Well ID Ul 1 JLd Site Name r,,,-l` Date Well Depth d Depth to Water Well Diameter Casing Material Screen Length Well Water Volume Sampling Crew Pump Type Tubing Type Intake set at Weather Conditions Notes (eg. odor or color) Time Water Level Volume Purged DO Temp EC pH ORP Turbidity (24 Hr 1 (frnm TC)('. (("aIQ ) lmnll 1 !or`l e­ Q/..—I i-4--.,A. ,A) r—%M /KiTi I% outer rararneters Sampled at L(5 Parameters taken with Samples delivered to by at Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs SVOCs Metals NO3+NO2 Herbicides Pesticides Other HCL None Nitric Acid Sulfuric Acid None None 40 ml VOAs glass 1 Liter glass 250 ml plastic 125 ml plastic 1 Liter glass 1 Liter glass 14 Days 7 Days 180 Days 28 Days 7 days 7 Days • vn V v U1 I lu oar UlQ Llul I 1" well [well depth -depth to water] x 0.0408 gallonslft. x 3 = 0.124/ft. _ 2" well [well depth -depth to water] x 0.163 gallons/ft. x 3 = 0.489/ft = 4" well [well depth -depth to water] x 0.653 gallons/ft. x 3 = 1.959/ft = C:\Users\jgarrett\Desktop\Revised GW Sampling Form 2016 Page of NO Our neopl., Job Number Groundwater Sampling Form State ID Well ID Site Namer �ct �}c�'� Date Well Depth .� Depth to Well Diameter Casing Material Screen Length Well Water Volume Sampling Crew Pump Type Tubing Type Intake set at Weather Conditions Notes (eg. odor or color) Time Water Level Volume Purged DO Temp EC pH ORP Turbidity (24 Hr.l rfrnm T(-)r..) (talc 1 fmr/I ) lot,% I'.C/--% vU IGI f-OI QI1 ICLCI J Sampled at Parameters taken with Samples delivered to by at Analysis Preservative Bottle ware Number of Bottles Hold Time VOCs SVOCs Metals NO3+NO2 Herbicides Pesticides Other HCL None Nitric Acid Sulfuric Acid None None 40 ml VOAs glass 1 Liter glass 250 ml plastic 125 ml plastic 1 Liter glass 1 Liter glass 14 Days 7 Days 180 Days 28 Days 7 days 7 Days vv Gu vv U11 IC. Va UUIQIRAI 1"well [well depth -depth to water] x 0.0408 gallons/ft. x 3 = 0.124/ft. _ 2" well [well depth -depth to water] x 0.163 gallons/ft. x 3 = 0.489/ft = 4" well [well depth -depth to water] x 0.653gallons/ft. x 3 = 1.959/ft = C:\Users\jgarrett\Desktop\Revised GW Sampling Form 2016 APPENDIX C ANALYTICAL REPORT 2�SQ ENCO Laboratories 9g Accurate. Timely. Respousive. luuavative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Tuesday, July 30, 2019 Withers & Ravenel Environmental (WI009) Attn: Matt James 115 MacKenan Drive Cary, NC 27511 RE: Laboratory Results for Project Number: 02000082.20, Project Name/Desc: Closed State Fairgrounds Landfill ENCO Workorder(s): CC11273 Dear Matt James, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, July 19, 2019. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, OUCLC'=-:�CA Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 28 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: MW-1 Lab ID: CC11273-01 Sampled: 07/18/19 11:30 Received: 07/19/19 14:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A O1/14/20 07/25/19 06:36 07/26/19 11:27 EPA 6010D EPA 3005A O1/14/20 07/25/19 09:34 07/29/19 13:21 EPA 7470A EPA 7470A 08/15/19 07/29/19 13:02 07/30/19 10:51 EPA 8260D EPA 503013_MS 08/01/19 07/24/19 00:00 07/24/19 16:24 EPA 8260D EPA 503013_MS 08/01/19 07/25/19 15:06 07/25/19 21:17 Client ID: MW-2 Lab ID: CC11273-02 Sampled: 07/18/19 12:55 Received: 07/19/19 14:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A O1/14/20 07/25/19 09:34 07/29/19 14:40 EPA 7470A EPA 7470A 08/15/19 07/29/19 13:02 07/30/19 11:04 EPA 8260D EPA 503013_MS 08/01/19 07/24/19 00:00 07/24/19 17:01 EPA 8260D EPA 503013_MS 08/01/19 07/25/19 15:06 07/25/19 21:49 Client ID: MW-3 Lab ID: CC11273-03 Sampled: 07/18/19 14:15 Received: 07/19/19 14:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A 01/14/20 07/25/19 09:34 07/29/19 13:36 EPA 7470A EPA 7470A 08/15/19 07/29/19 13:02 07/30/19 11:06 EPA 8260D EPA 5030B_MS 08/01/19 07/24/19 00:00 07/24/19 17:37 EPA 8260D EPA 5030B_MIS 08/01/19 07/25/19 15:06 07/25/19 22:20 Client ID: MW-3 Lab ID: CC11273-03RE1 Sampled: 07/18/19 14:15 Received: 07/19/19 14:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A O1/14/20 07/25/19 09:34 07/29/19 15:29 Client ID: MW-4 Lab ID: CC11273-04 Sampled: 07/18/19 14:55 Received: 07/19/19 14:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A 01/14/20 07/25/19 09:34 07/29/19 13:39 EPA 7470A EPA 7470A 08/15/19 07/29/19 13:02 07/30/19 11:08 EPA 8260D EPA 503013_MS 08/01/19 07/24/19 00:00 07/24/19 18:14 EPA 8260D EPA 5030B_MS 08/01/19 07/25/19 15:06 07/25/19 22:51 Client ID: MW-5 Lab ID: CC11273-05 Sampled: 07/18/19 13:35 Received: 07/19/19 14:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A O1/14/20 07/25/19 09:34 07/29/19 13:41 EPA 7470A EPA 7470A 08/15/19 07/29/19 13:02 07/30/19 11:15 EPA 8260D EPA 503013_MS 08/01/19 07/24/19 00:00 07/24/19 18:50 EPA 8260D EPA 503013_MS 08/01/19 07/25/19 15:06 07/25/19 23:23 Client ID: SA-1 Lab ID: CC11273-06 Sampled: 07/18/19 15:30 Received: 07/19/19 14:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A O1/14/20 07/25/19 09:34 07/29/19 13:44 EPA 7470A EPA 7470A 08/15/19 07/29/19 13:02 07/30/19 11:17 EPA 8260D EPA 5030B_MIS 08/01/19 07/24/19 00:00 07/24/19 19:27 EPA 8260D EPA 503013_MS 08/01/19 07/25/19 15:06 07/25/19 23:54 Client ID: SA-2 Lab ID: CC11273-07 Sampled: 07/18/19 16:00 Received: 07/19/19 14:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 6010D EPA 3005A O1/14/20 07/25/19 09:34 07/29/19 13:55 EPA 7470A EPA 7470A 08/15/19 07/29/19 13:02 07/30/19 11:20 EPA 8260D EPA 50306_MS 08/01/19 07/24/19 00:00 07/24/19 20:04 EPA 8260D EPA 503013_MS 08/01/19 07/25/19 15:06 07/26/19 00:25 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 28 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Trip Blank Lab ID: CC11273-08 Sampled: 07/18/19 11:30 Received: 07/19/19 14:20 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 08/01/19 EPA 8260D EPA 5030B_MS 08/01/19 07/24/19 00:00 07/24/19 20:41 07/25/19 15:06 07/26/19 00:57 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 28 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: MW-1 Lab ID: CC11273-01 Anala Results Flag MDL POLL Units Method Notes Barium - Total 16.7 1.10 10.0 EPA 6010D Client ID: MW-2 Lab ID: CC11273-02 Anala Results Flag MDL POLL Units Method Notes Barium - Total 152 1.10 10.0 ug/L EPA 6010D Cadmium - Total 0.690 1 0.360 1.00 ug/L EPA 6010D Client ID: MW-3 Lab ID: CC11273-03 Anala Barium - Total Chromium - Total Results 195 2.35 Flag 1 MDL 1.10 1.40 POLL 10.0 10.0 Units ug/L ug/L Method EPA 6010D EPA 6010D Notes Client ID: MW-3 Lab ID: CC11273-03RE3 Anala Selenium - Total Results 76.4 Flag ID MDL 62.0 POLL 100 Units ug/L Method EPA 6010D Notes R-05 Client ID: MW-4 Lab ID: CC11273-04 Anala Barium - Total Cadmium - Total Results 35.8 0.586 Flag 1 MDL 1.10 0.360 POLL 10.0 1.00 Units ug/L ug/L Method EPA 6010D EPA 6010D Notes Client ID: MW-5 Lab ID: CC11273-05 Anala Barium - Total Results 35.2 Flag MDL 1.10 POLL 10.0 Units ug/L Method EPA 6010D Notes Client ID: SA-1 Lab ID: CC11273-06 Anala Barium - Total Results 39.5 Flag MDL 1.10 POLL 10.0 Units ug/L Method EPA 6010D Notes Client ID: SA-2 Lab ID: CC11273-07 Anala Barium - Total Results 23.7 Flag MDL 1.10 POLL 10.0 Units ug/L Method EPA 6010D Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 28 00� www.encolabs.com ANALYTICAL RESULTS Description: MW-1 Lab Sample ID: CC11273-01 Received: 07/19/19 14:20 Matrix: Ground Water Sampled:07/18/19 11:30 Work Order: CC11273 Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flao Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 u ug/L 1 0.12 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 u ug/L 1 0.28 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF QV-01 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF 2-Butanone [78-93-3]^ 1.3 u ug/L 1 1.3 5.0 9G25033 EPA 8260D 07/25/19 21:17 REF 2-Hexanone [591-78-6]^ 0.88 u ug/L 1 0.88 5.0 9G25033 EPA 8260D 07/25/19 21:17 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 9G25033 EPA 8260D 07/25/19 21:17 REF Acetone [67-64-1]^ 10 u ug/L 1 10 20 9G25033 EPA 8260D 07/25/19 21:17 REF Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 9G25033 EPA 8260D 07/25/19 21:17 REF Benzene[71-43-2]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF Bromochloromethane [74-97-5]^ 0.48 u ug/L 1 0.48 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF QV-01 Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF QL-02, QV-01 Bromomethane [74-83-9]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF Carbon disulfide [75-15-0]^ 1.5 u ug/L 1 1.5 5.0 9G25033 EPA 8260D 07/25/19 21:17 REF Carbon tetrachloride [56-23-5]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF QV-01 Chlorobenzene[108-90-7]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF Chloroethane [75-00-31^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF Chloromethane [74-87-3]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 u ug/L 1 0.20 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF Dibromochloromethane [124-48-1]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF Dibromomethane [74-95-3]^ 0.27 u ug/L 1 0.27 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF Ethylbenzene[100-41-4]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 9G25033 EPA 8260D 07/25/19 21:17 REF m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 9G25033 EPA 8260D 07/25/19 21:17 REF Methylene chloride [75-09-2]^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF o-Xylene [95-47-6]^ 0.065 u ug/L 1 0.065 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF Styrene[100-42-5]^ 0.11 u ug/L 1 0.11 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF Tetrachloroethene [127-18-4]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 u ug/L 1 0.70 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF QV-01 Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF QV-01 Vinyl acetate [108-05-4]^ 0.95 u ug/L 1 0.95 5.0 9G25033 EPA 8260D 07/25/19 21:17 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 28 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: MW-1 Lab Sample ID: CC11273-01 Received: 07/19/19 14:20 Matrix: Ground Water Sampled:07/18/19 11:30 Work Order: CC11273 Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 u ug/L 1 0.32 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF Xylenes(Total)[1330-20-7]^ 0.45 u ug/L 1 0.45 3.0 9G25033 EPA 8260D 07/25/19 21:17 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 55 1 50.0 110 % 53-136 9G25033 EPA 8260D 07125119 21:17 REF Dlbromofluoromethane 51 1 50.0 102 % 67-129 9G25033 EPA 8260D 07125119 21:17 REF Toluene-d8 48 1 50.0 96 % 59-134 9G25033 EPA 8260D 07125119 21:17 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes Mercury [7439-97-6]^ 0.150 u ug/L 1 0.150 0.200 9G29038 EPA 7470A 07/30/19 10:51 RLF Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes Arsenic[7440-38-2]^ 7.60 u ug/L 1 7.60 10.0 9G25003 EPA 6010D 07/26/19 11:27 JDH Barium [7440-39-3]^ 16.7 ug/L 1 1.10 10.0 9G25003 EPA 6010D 07/26/19 11:27 JDH Cadmium [7440-43-9]^ 0.360 u ug/L 1 0.360 1.00 9G25003 EPA 6010D 07/26/19 11:27 JDH Chromium [7440-47-3]^ 1.40 u ug/L 1 1.40 10.0 9G25003 EPA 6010D 07/26/19 11:27 JDH Lead [7439-92-1]^ 3.10 u ug/L 1 3.10 10.0 9G25003 EPA 6010D 07/26/19 11:27 JDH Selenium [7782-49-2]^ 6.20 u ug/L 1 6.20 10.0 9G25013 EPA 6010D 07/29/19 13:21 JDH Silver [7440-22-4]^ 1.90 u ug/L 1 1.90 10.0 9G25003 EPA 6010D 07/26/19 11:27 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.2 u ug/L 1 1.2 2.0 9G24024 EPA 8260D 07/24/19 16:24 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.3 1 5.00 107 % 75-125 9G24024 EPA 8260D 0712411916:24 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 28 00� www.encolabs.com ANALYTICAL RESULTS Description: MW-2 Lab Sample ID: CC11273-02 Received: 07/19/19 14:20 Matrix: Ground Water Sampled:07/18/19 12:55 Work Order: CC11273 Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flao Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 u ug/L 1 0.12 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 u ug/L 1 0.28 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF QV-01 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF 2-Butanone [78-93-3]^ 1.3 u ug/L 1 1.3 5.0 9G25033 EPA 8260D 07/25/19 21:49 REF 2-Hexanone [591-78-6]^ 0.88 u ug/L 1 0.88 5.0 9G25033 EPA 8260D 07/25/19 21:49 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 9G25033 EPA 8260D 07/25/19 21:49 REF Acetone [67-64-1]^ 10 u ug/L 1 10 20 9G25033 EPA 8260D 07/25/19 21:49 REF Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 9G25033 EPA 8260D 07/25/19 21:49 REF Benzene[71-43-2]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF Bromochloromethane [74-97-5]^ 0.48 u ug/L 1 0.48 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF QV-01 Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF QL-02, QV-01 Bromomethane [74-83-9]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF Carbon disulfide [75-15-0]^ 1.5 u ug/L 1 1.5 5.0 9G25033 EPA 8260D 07/25/19 21:49 REF Carbon tetrachloride [56-23-5]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF QV-01 Chlorobenzene[108-90-7]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF Chloroethane [75-00-31^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF Chloromethane [74-87-3]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 u ug/L 1 0.20 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF Dibromochloromethane [124-48-1]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF Dibromomethane [74-95-3]^ 0.27 u ug/L 1 0.27 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF Ethylbenzene[100-41-4]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 9G25033 EPA 8260D 07/25/19 21:49 REF m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 9G25033 EPA 8260D 07/25/19 21:49 REF Methylene chloride [75-09-2]^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF o-Xylene [95-47-6]^ 0.065 u ug/L 1 0.065 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF Styrene[100-42-5]^ 0.11 u ug/L 1 0.11 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF Tetrachloroethene [127-18-4]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 u ug/L 1 0.70 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF QV-01 Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF QV-01 Vinyl acetate [108-05-4]^ 0.95 u ug/L 1 0.95 5.0 9G25033 EPA 8260D 07/25/19 21:49 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 28 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: MW-2 Lab Sample ID: CC1 1273-02 Received: 07/19/19 14:20 Matrix: Ground Water Sampled:07/18/19 12:55 Work Order: CC11273 Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 u ug/L 1 0.32 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF Xylenes (Total) [1330-20-7]1 0.45 u ug/L 1 0.45 3.0 9G25033 EPA 8260D 07/25/19 21:49 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 54 1 50.0 109 % 53-136 9G25033 EPA 8260D 07125119 21:49 REF Dlbromofluoromethane 52 1 50.0 105 % 67-129 9G25033 EPA 8260D 07125119 21:49 REF Toluene-d8 49 1 50.0 97 % 59-134 9G25033 EPA 8260D 07125119 21:49 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes Mercury [7439-97-6]^ 0.150 u ug/L 1 0.150 0.200 9G29038 EPA 7470A 07/30/19 11:04 RLF Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes Arsenic[7440-38-2]^ 7.60 u ug/L 1 7.60 10.0 9G25013 EPA 6010D 07/29/19 14:40 JDH Barium [7440-39-3]^ 152 ug/L 1 1.10 10.0 9G25013 EPA 6010D 07/29/19 14:40 JDH Cadmium [7440-43-9]^ 0.690 J ug/L 1 0.360 1.00 9G25013 EPA 6010D 07/29/19 14:40 JDH Chromium [7440-47-3]^ 1.40 u ug/L 1 1.40 10.0 9G25013 EPA 6010D 07/29/19 14:40 JDH Lead [7439-92-1]^ 3.10 u ug/L 1 3.10 10.0 9G25013 EPA 6010D 07/29/19 14:40 JDH Selenium [7782-49-2]^ 6.20 u ug/L 1 6.20 10.0 9G25013 EPA 6010D 07/29/19 14:40 JDH Silver[7440-22-4]^ 1.90 u ug/L 1 1.90 10.0 9G25013 EPA 6010D 07/29/19 14:40 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes 1,4-Dioxane [123-91-1]^ 1.2 u ug/L 1 1.2 2.0 9G24024 EPA 8260D 07/24/19 17:01 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.4 1 5.00 109 % 75-125 9G24024 EPA 8260D 0712411917:01 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 28 00� www.encolabs.com ANALYTICAL RESULTS Description: MW-3 Lab Sample ID: CC11273-03 Received: 07/19/19 14:20 Matrix: Ground Water Sampled:07/18/19 14:15 Work Order: CC11273 Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flao Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 u ug/L 1 0.12 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 u ug/L 1 0.28 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF QV-01 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF 2-Butanone [78-93-3]^ 1.3 u ug/L 1 1.3 5.0 9G25033 EPA 8260D 07/25/19 22:20 REF 2-Hexanone [591-78-6]^ 0.88 u ug/L 1 0.88 5.0 9G25033 EPA 8260D 07/25/19 22:20 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 9G25033 EPA 8260D 07/25/19 22:20 REF Acetone [67-64-1]^ 10 u ug/L 1 10 20 9G25033 EPA 8260D 07/25/19 22:20 REF Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 9G25033 EPA 8260D 07/25/19 22:20 REF Benzene[71-43-2]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF Bromochloromethane [74-97-5]^ 0.48 u ug/L 1 0.48 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF QV-01 Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF QL-02, QV-01 Bromomethane [74-83-9]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF Carbon disulfide [75-15-0]^ 1.5 u ug/L 1 1.5 5.0 9G25033 EPA 8260D 07/25/19 22:20 REF Carbon tetrachloride [56-23-5]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF QV-01 Chlorobenzene[108-90-7]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF Chloroethane [75-00-31^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF Chloromethane [74-87-3]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 u ug/L 1 0.20 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF Dibromochloromethane [124-48-1]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF Dibromomethane [74-95-3]^ 0.27 u ug/L 1 0.27 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF Ethylbenzene[100-41-4]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 9G25033 EPA 8260D 07/25/19 22:20 REF m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 9G25033 EPA 8260D 07/25/19 22:20 REF Methylene chloride [75-09-2]^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF o-Xylene [95-47-6]^ 0.065 u ug/L 1 0.065 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF Styrene[100-42-5]^ 0.11 u ug/L 1 0.11 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF Tetrachloroethene [127-18-4]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 u ug/L 1 0.70 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF QV-01 Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF QV-01 Vinyl acetate [108-05-4]^ 0.95 u ug/L 1 0.95 5.0 9G25033 EPA 8260D 07/25/19 22:20 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 28 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: MW-3 Lab Sample ID: CC1 1273-03 Received: 07/19/19 14:20 Matrix: Ground Water Sampled:07/18/19 14:15 Work Order: CC11273 Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 u ug/L 1 0.32 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF Xylenes (Total) [1330-20-7]1 0.45 u ug/L 1 0.45 3.0 9G25033 EPA 8260D 07/25/19 22:20 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 56 1 50.0 ill % 53-136 9G25033 EPA 8260D 07125119 22:20 REF Dlbromofluoromethane 50 1 50.0 99 % 67-129 9G25033 EPA 8260D 07125119 22:20 REF Toluene-d8 48 1 50.0 97 % 59-134 9G25033 EPA 6260D 07125119 22:20 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 u ug/L 1 0.150 0.200 9G29038 EPA 7470A 07/30/19 11:06 RLF Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 u ug/L 1 7.60 10.0 9G25013 EPA 6010D 07/29/19 13:36 JDH Barium [7440-39-3]^ 195 ug/L 1 1.10 10.0 9G25013 EPA 6010D 07/29/19 13:36 JDH Cadmium [7440-43-9]^ 0.360 u ug/L 1 0.360 1.00 9G25013 EPA 6010D 07/29/19 13:36 JDH Chromium [7440-47-3]^ 2.35 J ug/L 1 1.40 10.0 9G25013 EPA 6010D 07/29/19 13:36 JDH Lead [7439-92-1]^ 3.10 u ug/L 1 3.10 10.0 9G25013 EPA 6010D 07/29/19 13:36 JDH Selenium [7782-49-2]^ 76.4 JD ug/L 10 62.0 100 9G25013 EPA 6010D 07/29/19 15:29 JDH R-05 Silver[7440-22-4]^ 1.90 u ug/L 1 1.90 10.0 9G25013 EPA 6010D 07/29/19 13:36 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.2 u ug/L 1 1.2 2.0 9G24024 EPA 8260D 07/24/19 17:37 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 5.5 1 5.00 110 % 75-125 9G24024 EPA 8260D 071241191737 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 28 00� www.encolabs.com ANALYTICAL RESULTS Description: MW-4 Lab Sample ID: CC11273-04 Received: 07/19/19 14:20 Matrix: Ground Water Sampled:07/18/19 14:55 Work Order: CC11273 Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flao Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 u ug/L 1 0.12 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 u ug/L 1 0.28 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF QV-01 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF 2-Butanone [78-93-3]^ 1.3 u ug/L 1 1.3 5.0 9G25033 EPA 8260D 07/25/19 22:51 REF 2-Hexanone [591-78-6]^ 0.88 u ug/L 1 0.88 5.0 9G25033 EPA 8260D 07/25/19 22:51 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 9G25033 EPA 8260D 07/25/19 22:51 REF Acetone [67-64-1]^ 10 u ug/L 1 10 20 9G25033 EPA 8260D 07/25/19 22:51 REF Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 9G25033 EPA 8260D 07/25/19 22:51 REF Benzene[71-43-2]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF Bromochloromethane [74-97-5]^ 0.48 u ug/L 1 0.48 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF QV-01 Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF QL-02, QV-01 Bromomethane [74-83-9]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF Carbon disulfide [75-15-0]^ 1.5 u ug/L 1 1.5 5.0 9G25033 EPA 8260D 07/25/19 22:51 REF Carbon tetrachloride [56-23-5]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF QV-01 Chlorobenzene[108-90-7]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF Chloroethane [75-00-31^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF Chloromethane [74-87-3]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 u ug/L 1 0.20 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF Dibromochloromethane [124-48-1]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF Dibromomethane [74-95-3]^ 0.27 u ug/L 1 0.27 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF Ethylbenzene[100-41-4]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 9G25033 EPA 8260D 07/25/19 22:51 REF m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 9G25033 EPA 8260D 07/25/19 22:51 REF Methylene chloride [75-09-2]^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF o-Xylene [95-47-6]^ 0.065 u ug/L 1 0.065 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF Styrene[100-42-5]^ 0.11 u ug/L 1 0.11 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF Tetrachloroethene [127-18-4]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 u ug/L 1 0.70 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF QV-01 Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF QV-01 Vinyl acetate [108-05-4]^ 0.95 u ug/L 1 0.95 5.0 9G25033 EPA 8260D 07/25/19 22:51 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 28 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: MW-4 Lab Sample ID: CC1 1273-04 Received: 07/19/19 14:20 Matrix: Ground Water Sampled:07/18/19 14:55 Work Order: CC11273 Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 u ug/L 1 0.32 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF Xylenes (Total) [1330-20-7]1 0.45 u ug/L 1 0.45 3.0 9G25033 EPA 8260D 07/25/19 22:51 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 57 1 50.0 115 % 53-136 9G25033 EPA 8260D 07125119 22:51 REF Dlbromofluoromethane 51 1 50.0 102 % 67-129 9G25033 EPA 8260D 07125119 22:51 REF Toluene-d8 49 1 50.0 98 % 59-134 9G25033 EPA 8260D 07125119 22:51 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes Mercury [7439-97-6]^ 0.150 u ug/L 1 0.150 0.200 9G29038 EPA 7470A 07/30/19 11:08 RLF Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes Arsenic[7440-38-2]^ 7.60 u ug/L 1 7.60 10.0 9G25013 EPA 6010D 07/29/19 13:39 JDH Barium [7440-39-3]^ 35.8 ug/L 1 1.10 10.0 9G25013 EPA 6010D 07/29/19 13:39 JDH Cadmium [7440-43-9]^ 0.586 J ug/L 1 0.360 1.00 9G25013 EPA 6010D 07/29/19 13:39 JDH Chromium [7440-47-3]^ 1.40 u ug/L 1 1.40 10.0 9G25013 EPA 6010D 07/29/19 13:39 JDH Lead [7439-92-1]^ 3.10 u ug/L 1 3.10 10.0 9G25013 EPA 6010D 07/29/19 13:39 JDH Selenium [7782-49-2]^ 6.20 u ug/L 1 6.20 10.0 9G25013 EPA 6010D 07/29/19 13:39 JDH Silver[7440-22-4]^ 1.90 u ug/L 1 1.90 10.0 9G25013 EPA 6010D 07/29/19 13:39 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.2 u ug/L 1 1.2 2.0 9G24024 EPA 8260D 07/24/19 18:14 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.5 1 5.00 109 % 75-125 9G24024 EPA 8260D 0712411918:14 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 28 00� www.encolabs.com ANALYTICAL RESULTS Description: MW-5 Lab Sample ID: CC11273-05 Received: 07/19/19 14:20 Matrix: Ground Water Sampled:07/18/19 13:35 Work Order: CC11273 Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flao Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 u ug/L 1 0.12 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 u ug/L 1 0.28 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF QV-01 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF 2-Butanone [78-93-3]^ 1.3 u ug/L 1 1.3 5.0 9G25033 EPA 8260D 07/25/19 23:23 REF 2-Hexanone [591-78-6]^ 0.88 u ug/L 1 0.88 5.0 9G25033 EPA 8260D 07/25/19 23:23 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 9G25033 EPA 8260D 07/25/19 23:23 REF Acetone [67-64-1]^ 10 u ug/L 1 10 20 9G25033 EPA 8260D 07/25/19 23:23 REF Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 9G25033 EPA 8260D 07/25/19 23:23 REF Benzene[71-43-2]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF Bromochloromethane [74-97-5]^ 0.48 u ug/L 1 0.48 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF QV-01 Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF QL-02, QV-01 Bromomethane [74-83-9]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF Carbon disulfide [75-15-0]^ 1.5 u ug/L 1 1.5 5.0 9G25033 EPA 8260D 07/25/19 23:23 REF Carbon tetrachloride [56-23-5]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF QV-01 Chlorobenzene[108-90-7]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF Chloroethane [75-00-3]^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF Chloromethane [74-87-3]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 u ug/L 1 0.20 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF Dibromochloromethane [124-48-1]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF Dibromomethane [74-95-3]^ 0.27 u ug/L 1 0.27 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF Ethylbenzene[100-41-4]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 9G25033 EPA 8260D 07/25/19 23:23 REF m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 9G25033 EPA 8260D 07/25/19 23:23 REF Methylene chloride [75-09-2]^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF o-Xylene [95-47-6]^ 0.065 u ug/L 1 0.065 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF Styrene[100-42-5]^ 0.11 u ug/L 1 0.11 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF Tetrachloroethene [127-18-4]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 u ug/L 1 0.70 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF QV-01 Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF QV-01 Vinyl acetate [108-05-4]^ 0.95 u ug/L 1 0.95 5.0 9G25033 EPA 8260D 07/25/19 23:23 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 28 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: MW-5 Lab Sample ID: CC11273-05 Received: 07/19/19 14:20 Matrix: Ground Water Sampled:07/18/19 13:35 Work Order: CC11273 Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 u ug/L 1 0.32 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF Xylenes (Total) [1330-20-7]1 0.45 u ug/L 1 0.45 3.0 9G25033 EPA 8260D 07/25/19 23:23 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 56 1 50.0 113 % 53-136 9G25033 EPA 8260D 07125119 23:23 REF Dlbromofluoromethane 50 1 50.0 100 % 67-129 9G25033 EPA 8260D 07125119 23:23 REF Toluene-d8 50 1 50.0 99 % 59-134 9G25033 EPA 8260D 07125119 23:23 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes Mercury [7439-97-6]^ 0.150 u ug/L 1 0.150 0.200 9G29038 EPA 7470A 07/30/19 11:15 RLF Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes Arsenic[7440-38-2]^ 7.60 u ug/L 1 7.60 10.0 9G25013 EPA 6010D 07/29/19 13:41 JDH Barium [7440-39-3]^ 35.2 ug/L 1 1.10 10.0 9G25013 EPA 6010D 07/29/19 13:41 JDH Cadmium [7440-43-9]^ 0.360 u ug/L 1 0.360 1.00 9G25013 EPA 6010D 07/29/19 13:41 JDH Chromium [7440-47-3]^ 1.40 u ug/L 1 1.40 10.0 9G25013 EPA 6010D 07/29/19 13:41 JDH Lead [7439-92-1]^ 3.10 u ug/L 1 3.10 10.0 9G25013 EPA 6010D 07/29/19 13:41 JDH Selenium [7782-49-2]^ 6.20 u ug/L 1 6.20 10.0 9G25013 EPA 6010D 07/29/19 13:41 JDH Silver[7440-22-4]^ 1.90 u ug/L 1 1.90 10.0 9G25013 EPA 6010D 07/29/19 13:41 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.2 u ug/L 1 1.2 2.0 9G24024 EPA 8260D 07/24/19 18:50 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.0 1 5.00 99 % 75-125 9G24024 EPA 8260D 0712411918:50 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 28 00� www.encolabs.com ANALYTICAL RESULTS Description: SA-1 Lab Sample ID: CC11273-06 Received: 07/19/19 14:20 Matrix: Ground Water Sampled:07/18/19 15:30 Work Order: CC11273 Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 u ug/L 1 0.12 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 u ug/L 1 0.28 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF QV-01 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF 2-Butanone [78-93-3]^ 1.3 u ug/L 1 1.3 5.0 9G25033 EPA 8260D 07/25/19 23:54 REF 2-Hexanone [591-78-6]^ 0.88 u ug/L 1 0.88 5.0 9G25033 EPA 8260D 07/25/19 23:54 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 9G25033 EPA 8260D 07/25/19 23:54 REF Acetone [67-64-1]^ 10 u ug/L 1 10 20 9G25033 EPA 8260D 07/25/19 23:54 REF Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 9G25033 EPA 8260D 07/25/19 23:54 REF Benzene[71-43-2]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF Bromochloromethane [74-97-5]^ 0.48 u ug/L 1 0.48 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF QV-01 Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF QL-02, QV-01 Bromomethane [74-83-9]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF Carbon disulfide [75-15-0]^ 1.5 u ug/L 1 1.5 5.0 9G25033 EPA 8260D 07/25/19 23:54 REF Carbon tetrachloride [56-23-5]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF QV-01 Chlorobenzene[108-90-7]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF Chloroethane [75-00-31^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF Chloromethane [74-87-3]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 u ug/L 1 0.20 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF Dibromochloromethane [124-48-1]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF Dibromomethane [74-95-3]^ 0.27 u ug/L 1 0.27 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF Ethylbenzene[100-41-4]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 9G25033 EPA 8260D 07/25/19 23:54 REF m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 9G25033 EPA 8260D 07/25/19 23:54 REF Methylene chloride [75-09-2]^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF o-Xylene [95-47-6]^ 0.065 u ug/L 1 0.065 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF Styrene[100-42-5]^ 0.11 u ug/L 1 0.11 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF Tetrachloroethene [127-18-4]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 u ug/L 1 0.70 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF QV-01 Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF QV-01 Vinyl acetate [108-05-4]^ 0.95 u ug/L 1 0.95 5.0 9G25033 EPA 8260D 07/25/19 23:54 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 28 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: SA-1 Lab Sample ID: CC1 1273-06 Received: 07/19/19 14:20 Matrix: Ground Water Sampled:07/18/19 15:30 Work Order: CC11273 Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 u ug/L 1 0.32 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF Xylenes (Total) [1330-20-7]1 0.45 u ug/L 1 0.45 3.0 9G25033 EPA 8260D 07/25/19 23:54 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 56 1 50.0 112 % 53-136 9G25033 EPA 8260D 07125119 23:54 REF Dlbromofluoromethane 50 1 50.0 100 % 67-129 9G25033 EPA 8260D 07125119 23:54 REF Toluene-d8 48 1 50.0 96 % 59-134 9G25033 EPA 8260D 07125119 23:54 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes Mercury [7439-97-6]^ 0.150 u ug/L 1 0.150 0.200 9G29038 EPA 7470A 07/30/19 11:17 RLF Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes Arsenic[7440-38-2]^ 7.60 u ug/L 1 7.60 10.0 9G25013 EPA 6010D 07/29/19 13:44 JDH Barium [7440-39-3]^ 39.5 ug/L 1 1.10 10.0 9G25013 EPA 6010D 07/29/19 13:44 JDH Cadmium [7440-43-9]^ 0.360 u ug/L 1 0.360 1.00 9G25013 EPA 6010D 07/29/19 13:44 JDH Chromium [7440-47-3]^ 1.40 u ug/L 1 1.40 10.0 9G25013 EPA 6010D 07/29/19 13:44 JDH Lead [7439-92-1]^ 3.10 u ug/L 1 3.10 10.0 9G25013 EPA 6010D 07/29/19 13:44 JDH Selenium [7782-49-2]^ 6.20 u ug/L 1 6.20 10.0 9G25013 EPA 6010D 07/29/19 13:44 JDH Silver[7440-22-4]^ 1.90 u ug/L 1 1.90 10.0 9G25013 EPA 6010D 07/29/19 13:44 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.2 u ug/L 1 1.2 2.0 9G24024 EPA 8260D 07/24/19 19:27 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-d8 5.4 1 5.00 107 % 75-125 9G24024 EPA 8260D 0712411919:27 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 28 00� www.encolabs.com ANALYTICAL RESULTS Description: SA-2 Lab Sample ID: CC11273-07 Received: 07/19/19 14:20 Matrix: Ground Water Sampled:07/18/19 16:00 Work Order: CC11273 Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 u ug/L 1 0.12 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 u ug/L 1 0.28 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF QV-01 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF 2-Butanone [78-93-3]^ 1.3 u ug/L 1 1.3 5.0 9G25033 EPA 8260D 07/26/19 00:25 REF 2-Hexanone [591-78-6]^ 0.88 u ug/L 1 0.88 5.0 9G25033 EPA 8260D 07/26/19 00:25 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 9G25033 EPA 8260D 07/26/19 00:25 REF Acetone [67-64-1]^ 10 u ug/L 1 10 20 9G25033 EPA 8260D 07/26/19 00:25 REF Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 9G25033 EPA 8260D 07/26/19 00:25 REF Benzene[71-43-2]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF Bromochloromethane [74-97-5]^ 0.48 u ug/L 1 0.48 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF QV-01 Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF QL-02, QV-01 Bromomethane [74-83-9]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF Carbon disulfide [75-15-0]^ 1.5 u ug/L 1 1.5 5.0 9G25033 EPA 8260D 07/26/19 00:25 REF Carbon tetrachloride [56-23-5]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF QV-01 Chlorobenzene[108-90-7]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF Chloroethane [75-00-31^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF Chloromethane [74-87-3]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 u ug/L 1 0.20 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF Dibromochloromethane [124-48-1]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF Dibromomethane [74-95-3]^ 0.27 u ug/L 1 0.27 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF Ethylbenzene[100-41-4]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 9G25033 EPA 8260D 07/26/19 00:25 REF m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 9G25033 EPA 8260D 07/26/19 00:25 REF Methylene chloride [75-09-2]^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF o-Xylene [95-47-6]^ 0.065 u ug/L 1 0.065 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF Styrene[100-42-5]^ 0.11 u ug/L 1 0.11 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF Tetrachloroethene [127-18-4]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 u ug/L 1 0.70 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF QV-01 Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF QV-01 Vinyl acetate [108-05-4]^ 0.95 u ug/L 1 0.95 5.0 9G25033 EPA 8260D 07/26/19 00:25 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 28 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: SA-2 Lab Sample ID: CC1 1273-07 Received: 07/19/19 14:20 Matrix: Ground Water Sampled:07/18/19 16:00 Work Order: CC11273 Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 u ug/L 1 0.32 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF Xylenes (Total) [1330-20-7]1 0.45 u ug/L 1 0.45 3.0 9G25033 EPA 8260D 07/26/19 00:25 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 55 1 50.0 ill % 53-136 9G25033 EPA 8260D 07126119 00:25 REF Dlbromofluoromethane 49 1 50.0 97 % 67-129 9G25033 EPA 8260D 07126119 00:25 REF Toluene-d8 48 1 50.0 97 % 59-134 9G25033 EPA 6260D 07126119 00:25 REF Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes Mercury [7439-97-6]^ 0.150 u ug/L 1 0.150 0.200 9G29038 EPA 7470A 07/30/19 11:20 RLF Metals (total recoverable) by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes Arsenic[7440-38-2]^ 7.60 u ug/L 1 7.60 10.0 9G25013 EPA 6010D 07/29/19 13:55 JDH Barium [7440-39-3]^ 23.7 ug/L 1 1.10 10.0 9G25013 EPA 6010D 07/29/19 13:55 JDH Cadmium [7440-43-9]^ 0.360 u ug/L 1 0.360 1.00 9G25013 EPA 6010D 07/29/19 13:55 JDH Chromium [7440-47-3]^ 1.40 u ug/L 1 1.40 10.0 9G25013 EPA 6010D 07/29/19 13:55 JDH Lead [7439-92-1]^ 3.10 u ug/L 1 3.10 10.0 9G25013 EPA 6010D 07/29/19 13:55 JDH Selenium [7782-49-2]^ 6.20 u ug/L 1 6.20 10.0 9G25013 EPA 6010D 07/29/19 13:55 JDH Silver[7440-22-4]^ 1.90 u ug/L 1 1.90 10.0 9G25013 EPA 6010D 07/29/19 13:55 JDH Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.2 u ug/L 1 1.2 2.0 9G24024 EPA 8260D 07/24/19 20:04 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 5.4 1 5.00 108 % 75-125 9G24024 EPA 8260D 07124119 20:04 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 28 00� www.encolabs.com ANALYTICAL RESULTS Description: Trip Blank Lab Sample ID: CC11273-08 Received: 07/19/19 14:20 Matrix: Water Sampled:07/18/19 11:30 Work Order: CC11273 Project: Closed State Fairgrounds Landfill Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte fCAS Numberl Results Flao Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 u ug/L 1 0.12 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 u ug/L 1 0.28 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF 1,1-Dichloroethane [75-34-3]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF 1,1-Dichloroethene [75-35-4]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 u ug/L 1 0.48 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF 1,2-Dibromoethane [106-93-4]^ 0.66 u ug/L 1 0.66 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 u ug/L 1 0.19 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF 1,2-Dichloroethane [107-06-2]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF QV-01 1,2-Dichloropropane [78-87-5]^ 0.10 u ug/L 1 0.10 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 u ug/L 1 0.19 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF 2-Butanone [78-93-3]^ 1.3 u ug/L 1 1.3 5.0 9G25033 EPA 8260D 07/26/19 00:57 REF 2-Hexanone [591-78-6]^ 0.88 u ug/L 1 0.88 5.0 9G25033 EPA 8260D 07/26/19 00:57 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 u ug/L 1 1.1 5.0 9G25033 EPA 8260D 07/26/19 00:57 REF Acetone [67-64-1]^ 10 u ug/L 1 10 20 9G25033 EPA 8260D 07/26/19 00:57 REF Acrylonitrile [107-13-1]^ 3.5 u ug/L 1 3.5 10 9G25033 EPA 8260D 07/26/19 00:57 REF Benzene[71-43-2]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF Bromochloromethane [74-97-5]^ 0.48 u ug/L 1 0.48 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF Bromodichloromethane [75-27-4]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF QV-01 Bromoform [75-25-2]^ 0.22 u ug/L 1 0.22 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF QL-02, QV-01 Bromomethane [74-83-9]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF Carbon disulfide [75-15-0]^ 1.5 u ug/L 1 1.5 5.0 9G25033 EPA 8260D 07/26/19 00:57 REF Carbon tetrachloride [56-23-5]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF QV-01 Chlorobenzene[108-90-7]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF Chloroethane [75-00-31^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF Chloroform [67-66-3]^ 0.18 u ug/L 1 0.18 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF Chloromethane [74-87-3]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 u ug/L 1 0.20 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF Dibromochloromethane [124-48-1]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF Dibromomethane [74-95-3]^ 0.27 u ug/L 1 0.27 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF Ethylbenzene[100-41-4]^ 0.13 u ug/L 1 0.13 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF Iodomethane [74-88-4]^ 1.7 u ug/L 1 1.7 5.0 9G25033 EPA 8260D 07/26/19 00:57 REF m,p-Xylenes[108-38-3/106-42-3]^ 0.17 u ug/L 1 0.17 2.0 9G25033 EPA 8260D 07/26/19 00:57 REF Methylene chloride [75-09-2]^ 0.23 u ug/L 1 0.23 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF o-Xylene [95-47-6]^ 0.065 u ug/L 1 0.065 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF Styrene[100-42-5]^ 0.11 u ug/L 1 0.11 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF Tetrachloroethene [127-18-4]^ 0.17 u ug/L 1 0.17 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF Toluene [108-88-3]^ 0.14 u ug/L 1 0.14 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 u ug/L 1 0.21 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 u ug/L 1 0.70 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF QV-01 Trichloroethene [79-01-6]^ 0.15 u ug/L 1 0.15 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF Trichlorofluoromethane [75-69-4]^ 0.24 u ug/L 1 0.24 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF QV-01 Vinyl acetate [108-05-4]^ 0.95 u ug/L 1 0.95 5.0 9G25033 EPA 8260D 07/26/19 00:57 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 28 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: Trip Blank Lab Sample ID: CC1 1273-08 Received: 07/19/19 14:20 Matrix: Water Sampled:07/18/19 11:30 Work Order: CC11273 Project: Closed State Fairgrounds Landfill Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF Xylenes (Total) [1330-20-7]1 0.45 U ug/L 1 0.45 3.0 9G25033 EPA 8260D 07/26/19 00:57 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 56 1 50.0 112 % 53-136 9G25033 EPA 8260D 07126119 00:57 REF Dlbromofluoromethane 49 1 50.0 98 % 67-129 9G25033 EPA 8260D 07126119 00:57 REF Toluene-d8 49 1 50.0 99 % 59-134 9G25033 EPA 6260D 07126119 00:57 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.2 U ug/L 1 1.2 2.0 9G24024 EPA 8260D 07/24/19 20:41 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 5.2 1 5.00 104 % 75-125 9G24024 EPA 8260D 07124119 20:41 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 28 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9G25033 - EPA 5030E MS Blank (9G25033-BLK3) Prepared: 07/25/2019 15:06 Analyzed: 07/25/2019 20:46 Analvte Result Flaa POL Units 1, 1, 1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 28 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9G25033 - EPA 5030E MS - Continued Blank (9G25033-BLK3) Continued Prepared: 07/25/2019 15:06 Analyzed: 07/25/2019 20:46 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 55 u9/L 50.0 111 53-136 Dibromofluoromethane 51 u9/L 50.0 102 67-129 Toluene-d8 50 u9/L 50.0 100 59-134 LCS (9G25033-BS1) Prepared: 07/25/2019 15:06 Analyzed: 07/25/2019 18:39 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 105 75-133 Benzene 20 1.0 ug/L 20.0 98 80-134 Chlorobenzene 18 1.0 ug/L 20.0 92 80-120 Toluene 18 1.0 ug/L 20.0 88 71-120 Trichloroethene 22 1.0 ug/L 20.0 111 74-120 4-Bromofluorobenzene 56 u9/L 50.0 115 53-136 Dibromofluoromethane 52 u9/L 50.0 103 67-129 Toluene-d8 56 u9/L 50.0 111 59-134 Matrix Spike (9G25033-M81) Prepared: 07/25/2019 15:06 Analyzed: 07/25/2019 19:11 Source: CC12372-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 0.21 U 103 75-133 Benzene 20 1.0 ug/L 20.0 0.15 U 99 80-134 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 90 80-120 Toluene 17 1.0 ug/L 20.0 0.14 U 85 71-120 Trichloroethene 22 1.0 ug/L 20.0 0.15 U 109 74-120 4-Bromofluorobenzene 58 u9/L 50.0 116 53-136 Dibromofluoromethane 51 u9/L 50.0 101 67-129 Toluene-d8 51 u9/L 50.0 101 59-134 Matrix Spike Dup (9G25033-MSD1) Prepared: 07/25/2019 15:06 Analyzed: 07/25/2019 19:43 Source: CC12372-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 0.21 U 106 75-133 2 20 Benzene 19 1.0 ug/L 20.0 0.15 U 93 80-134 5 17 Chlorobenzene 17 1.0 ug/L 20.0 0.17 U 84 80-120 7 16 Toluene 16 1.0 ug/L 20.0 0.14 U 82 71-120 3 17 Trichloroethene 21 1.0 ug/L 20.0 0.15 U 103 74-120 6 22 4-Bromofluorobenzene 55 u9/L 50.0 111 53-136 Dibromofluoromethane 51 u9/L 50.0 103 67-129 Toluene-d8 50 u9/L 50.0 99 59-134 Metals by EPA 6000/7000 Series Methods - Quality Control Batch 9G29038 - EPA 7470A Blank (9G29038-BLK3) Prepared: 07/29/2019 13:02 Analyzed: 07/30/2019 10:47 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes Mercury 0.150 U 0.200 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 28 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals by EPA 6000/7000 Series Methods - Quality Control Batch 9G29038 - EPA 7470A - Continued LCS (9G29038-BS3) Prepared: 07/29/2019 13:02 Analyzed: 07/30/2019 10:49 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Mercury 5.18 0.200 ug/L 5.00 104 80-120 Matrix Spike (9G29038-MS1) Prepared: 07/29/2019 13:02 Analyzed: 07/30/2019 10:54 Source: CC11273-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 4.96 0.200 ug/L 5.00 0.150 U 99 75-125 Matrix Spike Dup (9G29038-MSD1) Prepared: 07/29/2019 13:02 Analyzed: 07/30/2019 10:56 Source: CC11273-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 4.97 0.200 ug/L 5.00 0.150 U 99 75-125 0.2 25 Post Spike (9G29038-PSI) Prepared: 07/29/2019 13:02 Analyzed: 07/30/2019 10:59 Source: CC11273-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Mercury 5.75 0.200 ug/L 4.76 0.0343 120 75-125 Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 9G25003 - EPA 3005A Blank (9G25003-BLK3) Prepared: 07/25/2019 06:36 Analyzed: 07/26/2019 10:53 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 7.60 U 10.0 ug/L Barium 1.10 U 10.0 ug/L Cadmium 0.360 U 1.00 ug/L Chromium 1.40 U 10.0 ug/L Lead 3.10 U 10.0 ug/L Silver 1.90 U 10.0 ug/L Blank (9G25003-BLK2) Prepared: 07/25/2019 06:36 Analyzed: 07/26/2019 10:57 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 7.60 U 10.0 ug/L Barium 1.10 U 10.0 ug/L Cadmium 0.360 U 1.00 ug/L Chromium 1.40 U 10.0 ug/L Lead 3.10 U 10.0 ug/L Silver 1.90 U 10.0 ug/L LCS (9G25003-BS1) Prepared: 07/25/2019 06:36 Analyzed: 07/26/2019 11:02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 192 10.0 ug/L 200 96 80-120 Barium 200 10.0 ug/L 200 100 80-120 Cadmium 19.3 1.00 ug/L 20.0 97 80-120 Chromium 193 10.0 ug/L 200 96 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 23 of 28 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 9G25003 - EPA 3005A - Continued LCS (9G25003-BS1) Continued Prepared: 07/25/2019 06:36 Analyzed: 07/26/2019 11:02 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Lead 191 10.0 ug/L 200 95 80-120 Silver 201 10.0 ug/L 200 101 80-120 Matrix Spike (9G25003-MSS) Prepared: 07/25/2019 06:36 Analyzed: 07/26/2019 11:04 Source: CC09034-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 191 10.0 ug/L 200 7.60 U 95 75-125 Barium 209 10.0 ug/L 200 11.8 98 75-125 Cadmium 19.5 1.00 ug/L 20.0 0.360 U 97 75-125 Chromium 199 10.0 ug/L 200 1.40 U 99 75-125 Lead 198 10.0 ug/L 200 3.10 U 99 75-125 Silver 206 10.0 ug/L 200 1.90 U 103 75-125 Matrix Spike Dup (9G25003-MSDI) Prepared: 07/25/2019 06:36 Analyzed: 07/26/2019 11:07 Source: CC09034-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 192 10.0 ug/L 200 7.60 U 96 75-125 0.8 20 Barium 215 10.0 ug/L 200 11.8 102 75-125 3 20 Cadmium 19.5 1.00 ug/L 20.0 0.360 U 97 75-125 0.07 20 Chromium 197 10.0 ug/L 200 1.40 U 98 75-125 1 20 Lead 194 10.0 ug/L 200 3.10 U 97 75-125 2 20 Silver 204 10.0 ug/L 200 1.90 U 102 75-125 0.9 20 Post Spike (9G25003-PSI) Prepared: 07/25/2019 06:36 Analyzed: 07/26/2019 11:10 Source: CC09034-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 0.191 0.0100 mg/L 0.200 -0.00811 96 80-120 Barium 0.208 0.0100 mg/L 0.200 0.0118 98 80-120 Cadmium 0.0195 0.00100 mg/L 0.0200 4.46E-5 97 80-120 Chromium 0.198 0.0100 mg/L 0.200 0.000455 99 80-120 Lead 0.196 0.0100 mg/L 0.200 0.00139 97 80-120 Silver 0.209 0.0100 mg/L 0.200 -0.000309 105 80-120 Batch 9G25013 - EPA 3005A Blank (9G25013-BLK1) Prepared: 07/25/2019 09:34 Analyzed: 07/29/2019 12:52 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 7.60 U 10.0 ug/L Barium 1.10 U 10.0 ug/L Cadmium 0.360 U 1.00 ug/L Chromium 1.40 U 10.0 ug/L Lead 3.10 U 10.0 ug/L Selenium 6.20 U 10.0 ug/L Silver 1.90 U 10.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 24 of 28 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 9G25013 - EPA 3005A - Continued Blank (9G25013-BLK2) Prepared: 07/25/2019 09:34 Analyzed: 07/29/2019 12:55 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 7.60 U 10.0 ug/L Barium 1.10 U 10.0 ug/L Cadmium 0.360 U 1.00 ug/L Chromium 1.40 U 10.0 ug/L Lead 3.10 U 10.0 ug/L Selenium 6.20 U 10.0 ug/L Silver 1.90 U 10.0 ug/L LCS (9G25013-BSI) Prepared: 07/25/2019 09:34 Analyzed: 07/29/2019 13:08 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 197 10.0 ug/L 200 98 80-120 Barium 195 10.0 ug/L 200 98 80-120 Cadmium 20.2 1.00 ug/L 20.0 101 80-120 Chromium 196 10.0 ug/L 200 98 80-120 Lead 193 10.0 ug/L 200 96 80-120 Selenium 209 10.0 ug/L 200 105 80-120 Silver 203 10.0 ug/L 200 101 80-120 Matrix Spike (9G25013-MSS) Prepared: 07/25/2019 09:34 Analyzed: 07/29/2019 13:11 Source: CC11273-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 204 10.0 ug/L 200 7.60 U 102 75-125 Barium 351 10.0 ug/L 200 152 99 75-125 Cadmium 21.5 1.00 ug/L 20.0 0.690 104 75-125 Chromium 207 10.0 ug/L 200 1.40 U 103 75-125 Lead 197 10.0 ug/L 200 3.10 U 98 75-125 Selenium 213 10.0 ug/L 200 6.20 U 107 75-125 Silver 214 10.0 ug/L 200 1.90 U 107 75-125 Matrix Spike Dup (9G25013-MSD3) Prepared: 07/25/2019 09:34 Analyzed: 07/29/2019 13:14 Source: CC11273-02 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Arsenic 207 10.0 ug/L 200 7.60 U 103 75-125 2 20 Barium 354 10.0 ug/L 200 152 101 75-125 0.7 20 Cadmium 21.7 1.00 ug/L 20.0 0.690 105 75-125 0.8 20 Chromium 207 10.0 ug/L 200 1.40 U 104 75-125 0.2 20 Lead 202 10.0 ug/L 200 3.10 U 101 75-125 2 20 Selenium 222 10.0 ug/L 200 6.20 U 111 75-125 4 20 Silver 216 10.0 ug/L 200 1.90 U 108 75-125 0.9 20 Post Spike (9G25013-PSI) Prepared: 07/25/2019 09:34 Analyzed: 07/29/2019 13:16 Source: CC11273-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Arsenic 0.202 0.0100 mg/L 0.200 0.00178 100 80-120 Barium 0.352 0.0100 mg/L 0.200 0.152 100 80-120 Cadmium 0.0216 0.00100 mg/L 0.0200 0.000690 105 80-120 Chromium 0.207 0.0100 mg/L 0.200 0.000376 103 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 25 of 28 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control Batch 9G25013 - EPA 3005A - Continued Post Spike (9G25013-PSI) Continued Prepared: 07/25/2019 09:34 Analyzed: 07/29/2019 13:16 Source: CC11273-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Lead 0.194 0.0100 mg/L 0.200 -0.00286 97 80-120 Selenium 0.217 0.0100 mg/L 0.200 -0.00534 108 80-120 Silver 0.220 0.0100 mg/L 0.200 -0.00101 110 80-120 Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 9G24024 - EPA 5030E MS Blank (9G24024-BLK1) Prepared: 07/24/2019 00:00 Analyzed: 07/24/2019 11:47 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 1.2 U 2.0 ug/L Toluene-d8 5.4 u91L 5.00 108 75-125 LCS (9G24024-BSI) Prepared: 07/24/2019 00:00 Analyzed: 07/24/2019 10:40 Spike Source %REC RPD Analvte Result Flao POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 24 2.0 ug/L 25.0 95 80-133 Toluene-d8 5.0 u91L 5.00 99 75-125 LCS Dup (9G24024-BSD1) Prepared: 07/24/2019 00:00 Analyzed: 07/24/2019 11:13 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 26 2.0 ug/L 25.0 103 80-133 8 19 QM-10 Toluene-& 5.1 u9/L 5.00 103 75-125 QM-10 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 26 of 28 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact. QM-10 LCS/LCSD were analyzed in place of MS/MSD. QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there is no impact. R-05 The sample was diluted due to the presence of high levels of non -target analytes resulting in elevated reporting limits. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 27 of 28 o 3 w Cl) a � J a m � � � m a 3J o m n W 7J a m O w a 3 m 0 g m a m N w m 3 a J m m a E. n w 0 w 0 w 9 ti Z n m n m n a n O n o: J D � n o c� O m _0 o Q CD 0 0 0 _ D w CD c6 O m 3 m �_ m 3 m - Cp O 2 n in n �n (� m �+ m CD D p Z N Q7 N Cn W N Cn 3 > (0 C! u v m d w v ro _� o cn �_ < T ry J � CD D n n -• � 0 @ ^_ m (D < T J 3 W CD 3 Z � G ED ,�� •c c/� W 7J v � v C4 09 0 mg o � o3 (n N 3 � N � N • � o � w � Q � C; G) 0 G) C) C) 0 o J�- V -I V -t -I v J � m o y n ool X X Y. X X X X X 8260D Appendix 1,8260D SIM ID w X X X X X X X Ag,As,Ba,Cd,Cr,Pb,Se 0 0 O _ v X,X X X X X X Hg d 0 J 0 o a c m a m H 5 D o 3 � � m w p N N w 1 J w y N w r /'1 -IMD cn CD w 'O O a m N m h � CD o 3 N L �N �3 CD N w (D Q s. Q o cn W o 73 o O Sample Preservation Verification ENCO Cary C1 ,,a .Om= N6, CG$ Iml Work Order: CC11273 Project: Closed State Fairgrounds Landfill Client: Withers & Ravenel Environmental (W1009) Project #: 02000082.20 Logged In: 19-Jul-19 14:23 Logged By: John C King Preservation Check Performed By: Date/Time: �. ��% / CC11273-01 Cont Type Pres (pH) Requirement pH Checked / In Control pH Adjusted Date/Time Adjusted Reagent Used/Comments A 250mLP+HNO3 <2 Y7/ N / NA Y /'N_,/ NA CC11273-02 Cont Type Pres (pH) Requirement pH Checked / Control, pH Adjusted Date/Time Adjusted Reagent Used/Comments A 250mLP+HNO3 <2 ( / N / NA Y / / NA CC11273-03 Cont Type Pres (pH) pH Checked / pH Adjusted Date/Time Reagent Used/Comments Requirement In Control Adjusted A 250mLP+HNO3 <2 Y- / N / NA Y / N ,/ NA CC11273-04 Cont Type Pres (pH) pH Checked / pH Adjusted DateTme Reagent Used/Comments Requirement In Control Adjusted A 250mLP+HNO3 <2 ()/ N / NA Y / / NA CC11273-05 Cant Type Pres (pH) Requirement pH Checked / In Control pH Adjusted DateMme Adjusted Reagent Used/Comments A 250mLP+HNO3 <2 & / N / NA Y / NA CC11273-06 Cont Type Pres (pH) pH Checked / pH Adjusted Date/Time Reagent Used/Comments Requirement In Control Adiusted A 250mLP+HNO3 <2 Y;/ N / NA Y / N / NA CC11273-07 Cont Type Pres (pH) Requirement IpH Checked / I In Control pH Adjusted Date/Time Adjusted Reagent Used/Comments A 250mLP+HNO3 <2 Y / N / NA Y / N '4 NA Reagent Name ID 1 2 /} pH Strip ID: < D. -/ C:\ELM NT\Print\wko_PreservationCheck. rpt Rea ent Name ID Rea ent Name ID 3 5 4 6 Page 1 c