6013_GreenwayNorthMeckCDLF_20190315_GWMonReport_FID1286607

SPRING 2018 SEMI-ANNUAL WATER QUALITY MONITORING REPORT
INFILL EXPANSION AREA
GREENWAY WASTE SOLUTIONS Al NORTH MECK, LLC
(FORMERLY NORTH MECKLENBURG C&D LANDFILL)
15300 HOLBROOKS ROAD
HUNTERSVILLE, NORTH CAROLINA
SOLID WASTE FACILITY PERMIT NO, 6043
Prepared For:
GREENWAY WASTE SOLUTIONS AT NORTH MECK, LLC
19109 W. CATAWBA AVENUE
CORNELIUS, NORTH CAROLINA 28031-5611
Prepared By:
CIVIL &ENVIRONMENTAL CONSULTANTS, INC.
1900 CENTER PARK DRIVE, SUITE A
CHARLOTTE NORTH CAROLINA 28217
EC Project No.111-370.001
July 16, 2018
Donald M. Cobb, P.G.
Project Manager
Scott L. Brown, P.E.
Vice President
Civil &Environmental Consultants, Inc.
1900 Center Park Drrve, Suite A I Charlotte, NC 28217 I p 980-224-8104 f: 980-224-8 U2 1 www.cecinc.com

TABLE OF CONTENTS
1.0 PURPOSE...........................................................................................................................1
2.0 SITE DESCRIPTION AND BACKGROUND................................................................2
3.0 RECENT MODIFICATIONS TO THE MONITORING SYSTEM ............................4
4.0 DESCRIPTION OF FIELD SAMPLING ACTIVITIES...............................................5
4.1 Well Water Level Gauging..................................................................................... 5
4.2 Well Purging........................................................................................................... 5
4.3 Groundwater Sample Collection............................................................................. 6
5.0 GROUNDWATER FLOW EVALUATION...................................................................7
6.0 WATER SAMPLE ANALYTICAL PARAMETERS....................................................8
7.0 SAMPLE ANALYTICAL DATA EVALUATION.........................................................9
7.1 Organic Analytes Detected at Concentrations Exceeding the 2L Standards .......... 9
7.2 Metal Analytes Detected at Concentrations Exceeding the 2L Standards .............. 9
7.3 Inorganic Leachate Indicator Parameters.............................................................. 10
7.4 Demonstration Letters on Vinyl Chloride and Metals .......................................... 10
8.0 CONCLUSIONS AND RECOMMENDATIONS.........................................................12
8.1 Conclusions...........................................................................................................12
8.2 Recommendations.................................................................................................13
FIGURES
Figure 1 — Site Location Map
Figure 2 — Site Map
Figure 3 — Groundwater Potentiometric Map
TABLES
Table 1 — Summary of Monitoring Well Gauging Data
Table 2 — Summary of Recent Site Groundwater Sample Analytical Detections
Table 3 — History of Site Groundwater Analytical Detections
Table 4 — Summary of Vertical Hydraulic Gradients
APPENDICES
Appendix A — Groundwater Sampling Field Logs
Appendix B — Laboratory Data Reports
Civil & Environmental Consultants, Inc.
-i- Fall 2017 Water Quality Monitoring Report
January 2018

1.0 PURPOSE
On behalf of Greenway Waste Solutions at North Meck, LLC, Civil & Environmental Consultants,
Inc. (CEC) has prepared this Spring 2018 Semi -Annual Water Quality Monitoring Report for the
Infill Expansion Area (Infill Area) at the subject landfill facility. This report describes the well
gauging and field sampling activities, and provides a summary of the site groundwater conditions
and acquired groundwater sample analytical data.
Civil & Environmental Consultants, Inc.
-1- Spring 2018 Water Quality Monitoring Report

2.0 SITE DESCRIPTION AND BACKGROUND
Greenway Waste Solutions at North Meek, LLC (GWS) operates the subject landfill under Solid
Waste Facility Permit Number 60-13. The facility address is 15300 Holbrooks Road, Huntersville,
North Carolina. As shown in Figure 2, the Infill Area consists of three landfill expansion areas
including: 1) Expansion Area 1 that is a closed C&D landfill cell on the west side; 2) Expansion
Area 2 that contains Phase 1, 2 and 3 C&D landfill cells on the east side; and 3) an infill saddle or
bridge expansion active C&D landfill cell that spans portions of Expansion Areas 1 and 2. The
Infill Area is situated in the northern portion of the landfill property. It is generally bounded by
an unnamed tributary of Cane Creek to the south, beyond which lies a closed C&D landfill area
(i.e. Closed Phase I Area). On the west and northwest, the Infill Area is bounded by private
property, a Colonial Pipeline easement, and land owned by the Town of Huntersville. To the north,
it is bounded by additional GWS landfill property. Land owned by Mecklenburg County,
including the David B. Waymer Flying Regional Park (a former unlined municipal solid waste
landfill - Holbrooks Road Landfill), bounds the site to the north and east. A Site Location Map is
attached as Figure 1.
Waste placement in the closed landfill cell (i.e. Expansion Area 1) generally occurred during the
years 2003 to 2007. The area of the closed Expansion Area 1 disposal cell is approximately 13.6
acres. Waste placement in Expansion Area 2 began in 2006, and portions of this area are presently
being used for C&D disposal. The area of Expansion Area 2 is approximately 15.1 acres. The
bridge landfill expansion cell was permitted in 2012, and it is currently being used for C&D
disposal. The area of the bridge landfill expansion cell is approximately 16.2 acres.
Semi-annual groundwater monitoring has been conducted along the periphery of the Infill Area
since 2009. The approximate locations of landfill monitoring wells are shown on Figure 2. During
the July 2013 and subsequent monitoring events, volatile organic compounds (VOCs) were
reported at concentrations exceeding groundwater quality requirements as defined by Title 15A
North Carolina Administrative Subchapter 02L Groundwater Classifications and Standards (2L
Standards) in several wells. VOCs reported in concentrations greater than the 2L Standards have
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included benzene, methylene chloride, bis(2-ethylhexyl)phthalate, and vinyl chloride
chloride (VC) is the predominant VOC in site groundwater.
Vinyl
Civil & Environmental Consultants, Inc.
-3- Spring 2018 Water Quality Monitoring Report

3.0 RECENT MODIFICATIONS TO THE MONITORING SYSTEM
The North Carolina Department of Environmental Quality (NCDEQ) - Solid Waste Section (SWS)
requested a characterization of the nature and extent of the groundwater contamination in the Infill
Area. The SWS's request was made in response to the detection of VOCs at concentrations above
the 2L Standards in detection/assessment monitoring wells in the subject landfill expansion area
as reported in April 2013.
The facility owner has been conducting on -going contaminant delineation since September 2013.
Recent activities include:
1) Installation of upgradient POC wells monitoring wells MW-15(i) and MW-16(i)
(completed on June 7, 2017) at the northern and eastern margins of the landfill facility
to assess the potential for migration of groundwater contaminants documented at the
adjoining upgradient Mecklenburg Holbrooks Road Landfill onto the subject landfill
property; and
2) Installation of off -site assessment monitoring wells MW-13(i) and MW-14(i)
(completed on June 9 and 12, 2017) at the western perimeter of the landfill facility to
assess the potential for off -site contaminant migration to the west.
3) As part of the preparation of an Assessment of Correction Measures relating to the
vinyl chloride detections, and in the preparation of an updated Water Quality
Monitoring Plan covering the entire facility (including the Closed Phase I Area),
groundwater monitoring wells that are part of the monitoring network for the
Expansion areas (i.e., those covered by this report) had the suffix "(i)" added to their
labels (MW-1(i), MW-2(i), etc.). This was done to avoid confusion when combining
the two separate monitoring well networks under one Water Quality Monitoring Plan.
Developing a new labeling system was not a viable option due to the volume of data
that has been collected. While this report has been prepared under the guidance of the
existing Water Quality Monitoring Plan, the new well labels have been used throughout
to avoid confusion when referencing this report to the Assessment of Corrective
Measures and/or the updated Water Quality Monitoring Plan.
Civil & Environmental Consultants, Inc.
-4- Spring 2018 Water Quality Monitoring Report

4.0 DESCRIPTION OF FIELD SAMPLING ACTIVITIES
Field activities associated with the Spring 2018 semi-annual water quality monitoring were
conducted by CEC personnel from April 9-12, 2018. Project oversight was provided by an NC -
licensed geologist. In April, well water levels were gauged, static well water was purged, and
groundwater samples were collected from 23 monitoring wells including shallow wells MW-1(i)
through MW-16(i); and deeper wells MW-41)(i), MW-51)(i), MW-7D(i), MW-8D(i), MW-91)(i),
MW-11D(i), and MW-121)(i). Split samples were also collected from wells MW-9(i), MW-91)(i),
MW-12(i), and MW-12D(i) as a part of the April 2018 field activities. Wells MW-1(i) and MW-
15(i) were sampled for metals at a later date due to high turbidity. MW-10(i) was not sampled for
metals, because of an unsuccessful well redevelopment. The split samples were analyzed for VOCs
by TestAmerica and Pace Analytical Services, Inc. (Pace). Also, five surface water samples (SW-
1, SW-2, SW-3, SW-4, and SW(eff)) were collected from the adjacent tributary creek located along
the southern perimeter of the Infill Area, and one surface water sample (SW(inf)) was collected at
the influent end of drain pipe that lies beneath the Infill Area. The approximate locations of these
monitoring points are shown on Figure 2.
4.1 WELL WATER LEVEL GAUGING
Prior to well purging/sampling, the water level in each monitoring well was gauged using an
electronic water level meter. The depth -to -groundwater was measured from a reference point on
the top -of -casing and was recorded to the nearest 0.01-inch on the well sampling field log (see
Appendix A). The water level probe was decontaminated between well measurements.
4.2 WELL PURGING
To minimize sampling artifacts and validate certain metals and inorganic parameter data, CEC
carefully monitored turbidity in the site monitoring wells during the well purge process. CEC
made an effort to minimize turbidity prior to collecting well samples.
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Where the water table was shallow, a peristaltic pump was utilized to purge the well at a low -flow
rate until targeted analytical parameters were found to stabilize. During the well purge, specific
conductance, pH, dissolved oxygen, turbidity and oxidation-reduction potential were frequently
measured with either a YSI 556 Water Quality Meter or a YSI Pro Plus Water Quality Meter in a
flow -through cell to observe and document the chemical stability of the formation water entering
the monitoring well. When parameter values indicated stable water chemistry as defined by
USEPA Groundwater Sampling Guidelines for Superfund and RCRA Project Managers (EPA
542-S-02-001, May 2002), the well purge was considered complete and groundwater samples were
then collected. Well purge data was recorded on the well sampling field logs provided in Appendix
A.
Where the water table was too deep to effectively use a low -flow peristaltic pump, a clean
submersible pump was employed to evacuate the monitoring well of three stagnant well volumes
before collecting groundwater samples.
4.3 GROUNDWATER SAMPLE COLLECTION
Following the above -described well purging procedures, groundwater samples were collected
employing the same low -flow pumping protocols using either the peristaltic or submersible pump.
Groundwater samples were collected in laboratory -supplied sample containers, which were labeled
and packed on ice in insulated coolers that were either hand -delivered or shipped overnight by
FedEx to the selected analytical laboratory under chain -of -custody protocol.
Due to high turbidity, monitoring wells MW-1(i), MW-10(i), and MW-15 (i) were not sampled for
metals during the initial round of water quality monitoring. These wells are part of a Metals
Alternative Source Demonstration currently ongoing at the site. As such, turbidity must be below
10 NTUs prior to sampling for metals. The wells were redeveloped on June 7, 2018, and metals
samples were collected for MW-1(i) and MW-15 (i) on June 18, 2018. Elite Drilling attempted to
redevelop MW-10(i) on June 7, 2018 but due to very high turbidity and slow recharge, the well
was not successfully redeveloped. MW-10(i) will be replaced prior to the next sampling event in
October 2018.
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5.0 GROUNDWATER FLOW EVALUATION
A depth -to -water level measurement was performed relative to the top -of -well casing in each
groundwater monitoring well prior to well purging. A water level elevation was calculated by
subtracting the depth -to -water from the respective surveyed top -of -well casing elevation datum.
Monitoring well gauging data are summarized in Table 1.
The calculated groundwater levels were used to prepare the April 2018 groundwater
potentiometric map presented in Figure 3. Groundwater movement across the Infill Area is to the
southeast toward the unnamed stream tributary along the southern boundary of this area. The "V"-
shaped potentiometric contours in the vicinity of the stream tributary are indicative of shallow
groundwater discharge from the Infill Area to this adjacent stream. Vertical hydraulic gradients
were calculated for well clusters MW5(i)/5D(i), MW-7(i)/7D(i), MW-8(i)/8D(i), MW-9(i)/9D(i),
MW-11(i)/11D(i), and MW-12(i)/12D(i) (the respective well pairs are closely spaced to each
other). Downward vertical gradients were determined for MW-7(i)/7D(i), MW-9(i)/9D(i) MW-
11(i)/11D(i) indicating groundwater recharge in these areas. Upward vertical hydraulic gradients
were determined for well clusters MW-4(i)/4D(i), MW-5(i)/5D(i), MW-8(i)/8D(i), and MW-
12(i)/12D(i) indicating groundwater discharge to the adjacent tributary stream. A summary of the
vertical hydraulic gradient data is provided in Table 4.
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6.0 WATER SAMPLE ANALYTICAL PARAMETERS
For the routine Spring 2018 semi-annual monitoring event, groundwater samples that were
collected from 23 monitoring wells and the three off -site water supply wells were submitted to
TestAmerica laboratory for analytical testing for the following Appendix II parameters:
Volatile Organic Compounds (VOCs) plus Tetrahydrofuran (THF) [EPA 8260B]
Semi-VOCs [EPA 8270]
Herbicides [EPA 8151A]
Organochlorine Pesticides [EPA 8081B]
Polychlorinated Biphenyls (PCBs) [EPA 8082A]
Metals [EPA 200.8]
Monitoring well and water supply well samples were also tested for leachate indicator parameters
including the following list:
Alkalinity [SM2320B]
Anions [EPA 9056A]
Mercury [EPA 245.1 ]
Cyanide [EPA 9014]
Total Dissolved Solids [SM2540C)
Six surface water samples were analyzed for Appendix I VOCs plus tetrahydrofuran [EPA 826013]
and Appendix I Metals [EPA 200.8].
A quality control trip blank was analyzed for Appendix II VOCs plus tetrahydrofuran [EPA
8260B].
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-8- Spring 2018 Water Quality Monitoring Report

7.0 SAMPLE ANALYTICAL DATA EVALUATION
Laboratory analytical data reports for the April 2018 semi-annual monitoring event are provided
in Appendix B. A summary of Appendix II organic and inorganic analytes detected in the collected
water samples at concentrations above their respective laboratory reporting limits is provided in
Table 2, and historical detections of target analytes are listed in Table 3.
7.1 ORGANIC ANALYTES DETECTED AT CONCENTRATIONS EXCEEDING
THE 2L STANDARDS
Vinyl Chloride was detected in interior monitoring wells MW-4(i) and MW-7(i) at concentrations
of 1.6 µg/L and 0.88 µg/L respectively. VC was detected in perimeter monitoring wells MW-
12(i), and MW-121)(i) at concentrations ranging from 1.5 to 3.1 µg/L. The 2L Standard for VC is
0.03 µg/L.
Benzene was detected at 1.4 µg/L in interior well MW-7(i) and at 1.5 µg/L in perimeter well MW-
9(i). The 2L Standard for benzene is 1.0 µg/L.
Methylene chloride was detected at 5 µg/L in MW-121)(i). Methylene chloride is a common
laboratory contaminant and its detection is likely an artifact of the analytical testing.
7.2 METAL ANALYTES DETECTED AT CONCENTRATIONS EXCEEDING THE
2L STANDARDS
Laboratory test results for the Spring 2018 sampling event show that cobalt, iron, manganese, and
vanadium were detected at concentrations above the 2L Standards or Interim Maximum Allowable
Concentrations. Negative oxidation-reduction potential (ORP) measured in purged groundwater
from background monitoring wells is indicative of ambient reducing groundwater conditions that
likely result in the occurrence of elevated levels of naturally occurring metals.
Cobalt was detected in background monitoring wells MW-12(i) and MW-12D(i) in a concentration
range between 6.4 and 1.1 µg/L, which exceeds its 2L Standard of 1 µg/L. Cobalt was detected in
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downgradient wells at levels ranging from 2.3 to 39 µg/L. The sample data indicates that cobalt
occurs naturally at concentrations above its 2L Standard.
Iron was detected in background monitoring wells in a concentration range between 400 and
53,000 µg/L, levels that exceed its 2L Standard of 300 µg/L. Iron was detected in downgradient
wells at levels ranging from 66 to 53,000 µg/L with a geometric mean of 1,800 µg/L. The sample
data indicate that iron occurs naturally at concentrations above its 2L Standard.
Manganese was detected in background monitoring wells in a concentration range between 254
µg/L and 2,300 µg/L, levels that exceed its 2L Standard of 50 µg/L. Manganese was detected in
downgradient wells at levels ranging from 0.96 µg/L and 12,000 µg/L with a geometric mean of
897 µg/L. The sample data indicate that manganese occurs naturally at concentrations above its
2L Standard.
Vanadium was detected in background monitoring wells at 4.5 and 3.1 µg/L. Vanadium
concentrations detected in downgradient wells ranged from 2.2 µg/L to 11 µg/L with a geometric
mean of 8.8 µg/L. The Interim Maximum Allowable Concentration (IMAC) for vanadium is
0.0003 mg/L. The sample data indicate that vanadium is naturally occurring at concentrations
above the IMAC.
7.3 INORGANIC LEACHATE INDICATOR PARAMETERS
Total dissolved solids (TDS) levels measured in background wells ranged from 750 to 320,000
µg/L. Downgradient wells exhibited a higher range of TDS values between 120,000 and 1,100,000
µg/L with a geometric mean of 473,005 µg/L.
7.4 DEMONSTRATION LETTERS ON VINYL CHLORIDE AND METALS
In Spring 2017, per 15A NCAC 13B .0544 (b) (1) (I), CEC on behalf of Greenway Waste Solutions
at North Meck, LLC prepared and submitted letters under separate cover to the NCDEQ SWS —
Compliance Unit presenting historical data and recent technical findings regarding the laboratory
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detections of VC and the presence of background metals in the groundwater underlying the landfill.
These letters present and discuss data on the laboratory error in falsely reporting VC due to the Freon
conversion and on the presence of naturally occurring metals in the geology and hydrogeology at the
landfill.
Regarding the SWS Compliance Unit's review of the Demonstration Letter on Laboratory Analyses
for Vinyl Chloride, they issued a letter (DIN 28701) dated December 19, 2017, noting that prior to
Fall 2016 laboratory error may have resulted in the false inflation or detection of VC in several landfill
monitoring wells; however, maintained that the laboratory data still indicate exceedances of vinyl
chloride above the 2L Standard in violation of NC groundwater rules. The SWS Compliance Unit
did not acknowledge that more recent and more accurate laboratory data for VC indicate that
significantly fewer facility monitoring wells are non -compliant with regard to VC levels and that
several non -compliant wells occur in the interior areas of the landfill facility. Further, the SWS
Compliance Unit stated that the proposed updated Water Quality Monitoring Plan (DIN 28684),
which proposes to unify the groundwater monitoring approach for the entire landfill facility utilizing
designated point of compliance groundwater monitoring wells, is currently under Section review.
Regarding the SWS Compliance Unit's review of the Demonstration Letter on Background Metals
in Groundwater, they issued a letter (DIN 28645) dated December 19, 2017, requesting that additional
information be submitted in an Alternate Source Demonstration Addendum. CEC submitted the
requested addendum study on behalf of GWS on April 6, 2018. In this Addendum, CEC proposed a
two-year sampling protocol on the background wells at the site to be followed by a statistical analysis
to establish alternate concentrations of select metals at the site. This Addendum was approved on
April 30, 2018.
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8.0 CONCLUSIONS AND RECOMMENDATIONS
8.1 CONCLUSIONS
Routine field activities associated with the Spring 2018 semi-annual water quality monitoring were
conducted by CEC personnel from April 9-12, 2017. In April, well water levels were gauged,
static well water was purged, and groundwater samples were collected from 23 monitoring wells
including shallow wells MW-1(i) through MW-16(i) (excluding MW-10(i)) and deeper wells MW-
41)(i), MW-51)(i), MW-713(i), MW-813(i), MW-913(i), MW-111)(i), and MW-121)(i). Also, five
surface water samples (SW-1 through SW-4 and SW(eff)) were collected from the adjacent
tributary creek located along the southern perimeter of the Infill Area, and one surface water
sample (SW(inf)) was collected at the influent end of drain pipe that lies beneath the Infill Area.
Vinyl Chloride was detected in interior monitoring wells MW-4(i) and MW-7(i) at concentrations
of 1.6 µg/L and 0.88 µg/L respectively. VC was detected in perimeter monitoring wells MW-12(i)
and MW-121)(i) at concentrations ranging from 1.5 to 3.1 µg/L. The 2L Standard for VC is 0.03
µg/L.
Benzene was detected at 1.4 µg/L in interior well MW-7(i) and at 1.5 µg/L in perimeter well MW-
9(i). The 2L Standard for benzene is 1.0 µg/L.
Methylene chloride was detected at 5 µg/L in MW-121)(i). Methylene chloride is a common
laboratory contaminant and its detection is likely an artifact of the analytical testing.
Metals including chromium, cobalt, iron, manganese, and vanadium were detected in groundwater
monitoring wells at values consistent with naturally occurring values as published by the USGS
(Chapman and others, Naturally Occurring Contaminants in the Piedmont and Blue Ridge
Crystalline -Rock Aquifers and Piedmont Early Mesozoic Basin Siliciclastic-Rock Aquifers,
Eastern United States, 1994-2008, U.S. Geological Survey, Scientific Investigations Report 2013-
5072). Negative oxidation-reduction potential (ORP) measured in purged groundwater from
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background monitoring wells is indicative of ambient reducing groundwater conditions that likely
result in the occurrence of elevated levels of naturally occurring metals.
Total dissolved solids (TDS) levels measured in background wells ranged from 750 to 320,000
µg/L. Downgradient wells exhibited a higher range of TDS values between 120,000 and 1,100,000
µg/L with a geometric mean of 473,005 µg/L.
8.2 RECOMMENDATIONS
An Assessment of Corrective Measures has been submitted to NC DEQ to address the detections
of vinyl chloride and methylene chloride in groundwater wells at the site. In addition, a Metals
Alternative Source Demonstration Addendum has been submitted to and approved by NC DEQ
with the stated goal of establishing alternate concentrations for Appendix II metals as well as iron
and manganese; sampling for the Addendum is ongoing and is scheduled to be completed in 2020,
at which point statistical analyses will be run on the collected data and recommendations made
regarding alternate concentrations.
Please note that this will be the final report under the existing Water Quality Monitoring Plan. An
updated Water Quality Monitoring Plan, prepared by CEC and dated April 19, 2018, was submitted
to NC DEQ and approved in a letter dated April 20, 2018. This updated Water Quality Monitoring
Plan will be followed beginning with the Fall 2018 semi-annual water quality monitoring event.
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Civil & Environmental Consultants, Inc.

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Civil & Environmental Consultants, Inc.

Table 1
Summary of Water Level Gauging Data
Spring 2018 Semi -Annual Groundwater Monitoring
North Meek Infill Area Landfill
CEC Project No. 111-370.001
Well ID
1
Depth
Screen
1
Interval
TOC Elev.
(ft)
Fall 2017
a
W.L. (TOC)
Fall 2017
W.L. Elev.
(ft)
Spring 2018
z
W.L. (TOC)
Spring 2018
W.L. Elev.
(ft)
MW-1 (i)
60
45-60
740.71
52.25
688.46
52.53
688.18
MW-2 (i)
25
10-25
678.34
10.69
667.65
10.00
668.34
MW-3 (i)
16
6-16
667.98
6.34
661.64
6.95
661.03
MW-4 (i)
17.5
7.5-17.5
678.10
10.88
667.22
10.79
667.31
MW-41) (i)
52
42-52
676.10
13.86
662.24
13.89
662.21
MW-5 (i)
18
8-18
672.92
8.49
664.43
8.05
664.87
MW-51) (i)
58
43-58
678.27
11.51
666.76
11.32
666.95
MW-6 (i)
17
7-17
NM
12.11
NM
12.49
NM
MW-7 (i)
23
8-23
691.64
14.01
677.63
13.45
678.19
MW-7D (i)
64
49-64
703.72
27.80
675.92
27.41
676.31
MW-8 (i)
28
13-28
706.71
22.31
684.40
22.42
684.29
MW-8D (i)
100
85-100
719.02
33.40
685.62
32.95
686.07
MW-9 (i)
25
10-25
713.34
23.61
689.73
23.05
690.29
MW-9D (i)
80
65-80
713.24
23.78
689.46
23.41
689.83
MW-10 (i)
60
40-60
761.22
53.01
708.21
53.74
707.48
MW-11 (i)
22
7-22
678.97
17.76
661.21
17.05
661.92
MW-11D (i)
50
45-50
679.22
18.00
661.22
17.31
661.91
MW-12 (i)
32
17-32
708.74
21.65
687.09
21.45
687.29
MW-12D (i)
54
50-54
709.26
22.10
687.16
21.89
687.37
MW-13 (i)
81
71-81
735.17
46.05
689.12
45.50
689.67
MW-14 (i)
24.5
14.5-24.5
704.76
15.00
689.76
14.76
690.00
MW-15 (i)
63.5
48.5-63.5
752.96
41.85
711.11
41.82
711.14
MW-16 i
29
17-27
698.21
24.72
673.49
22.35
675.86
Notes:
TOC= Top of Casing Elevation
WL= Groundwater Level
NM= Not Measured
(1) Measured in feet below ground surface
(2) Depth in feet relative to TOC elevation

Table 2
Site Gr000dwater and Privatc Wells Aoalytieal Detections
Spring 2018 Semi-A000al Gr000dwater Mooitoriog
North Meek 101111 Area LaodDll
CEC Projeet N. 111-370.001
aaamommmmmmmmmmmm��mm®®
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Has—
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FMI
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�o®m�m0m0m0m0mmm0m0m0m0
mo®m�mmm00mmm0000mmmmm0
�oam�m0�®00m�0®0®m0m0m0
Notes:
All wits arein VY/L wless otherwised indicated
NCDEQ S-dard-15A NCAC 02L.0203 GrouMwacer Scds (ER. 3013)
*`Interim Maximum Allowable Concwrcadon (ER 2013)
*LabomtorI., Pace (P), S-ly (S), -Test America (TA)
I=Euimated core. above [he adjusteJ metbod detectloo Iimit
aM below the adjuaed reposing limit
BxorapouM was found In iba blank and swple.
rF Refer to Care Narrative for funFcr devil
Bold /yellow values exceetl [M1e NCDEQ Standard
Blue values eueed dw Solitl Waae 9ectlov Liral[ (SWSL) (Eff.2011)
R� values eueed dw Matlrmw Corcevu'atlon IArNt (MCL) (ER. 2009)
NS—Not Specified
<"Repon Limit" = Value is less tlut tM Repon Lir�tl[

Table 2
Site Gr000dwater and Privatc WeRe Aoalytieal Detections
Spring 2018 Semi-A000al Gr000dwater Mooitoriog
North W& IoDll Area LaodDO
CEC Project No. 111-370.001
®®®
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Notex:
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'*miexlm Maximum Allowable Cowwua�iov (ER. 2015)
'Laboamner P.-(P), Shealy (S), aM Text Amexiea (TA)
l- ErimatM ww. above the adj� ud medwd detection liralt
aM below d adjured xapottlog IIMt
B=Coapowd wax fowl m dre blank aM xer 1,
Bold/yellow values eeceM tyre NCDEQ SlaMmd
Blue values exceM the Solid Ware S-i-L (S—) ME 2011)
Retl valves exceeai the Maxmeun COMeuuatioa Limlt (—) (ER 2009)
NS- Not Specified
<"Repott U mit Value ix leis hat Abe RWp LUJt

Table 3 (Cont.)
History of Groundwater and Surface Water Analytical Data
North Meek Infiil Area Landfill
CEC Project No. 111-370.0001
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Notes:
All units are in µglL unless oat—ss,d i alte. d
NCDEQ Sten ind=15A NCAC 02L .0202 Groundwater St& (Eff. 2013)
•'Interim Maximum Allowable Concentration (Eff. 2013)
•Labomtones-Pace (P), SN aly (S), and Test America (TA)
] - Estimated coot. above as, adjusted method detcefion lint
an below ate ediusted reporting limit
Bxompound was f,u mthe bleat: an sample.
crr= Refer m Case Narrafive for further d-il
Bold/yellow values exceed the NCDEQ Standard
Blue valets exceed Me Solid Waste Section Limit (SWSL) (Eff. 2011)
Red values exceed the Maximum Conc—fion Lint (MCL) (Eff. 2009)
NS=Not Specified
<"Report Lint" = Value is less that ate Report Lnit

Table 3 (Cont.)
History of Groundwater and Surface Water Analytical Data
North Meek Infiil Area Landfill
CEC Project No. 111-370.0001
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Notes:
All units are in µglL unless oat—ss,d i alte. d
NCDEQ Sten ind=15A NCAC 02L .0202 Groundwater St& (Eff. 2013)
•'Interim Maximum Allowable Concentration (Eff. 2013)
•Labomtones-Pace (P), SN aly (S), and Test America (TA)
] - Estimated coot. above as, adjusted method detcefion lint
an below ate ediusted reporting limit
Bxompound was f,u mthe bleat: an sample.
crr= Refer m Case Narrafive for further d-il
Bold/yellow values exceed the NCDEQ Standard
Blue valets exceed Me Solid Waste Section Limit (SWSL) (Eff. 2011)
Red values exceed the Maximum Conc—fion Lint (MCL) (Eff. 2009)
NS=Not Specified
<"Report Lint" = Value is less that ate Report Lnit

Table 3 (Cont.)
History of Groundwater and Surface Water Analytical Data
North Meek Infiil Area Landfill
CEC Project No. 111-370.0001
aaaommmoo©©©©©©©ommm
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Notes:
MI_
are N µglL Mess oN— scd indicated
NCDEQ Sten ind=15A NCAC 02L .0202 Groundwater St& (Eff. 2013)
•'Interim Maximum Allowable Concentration (Eff. 2013)
•Labomtodes— Pace (P), Shealy (S), and Test America (TA)
] = Estimated coot. above the adjusted me Nod detection limit
and below Ne ediusted reporting limit
Bxompound was found m Ne bleak and sample.
— Ref to Case Narrafive for further d-il
Bold /yellow valves exceed Ne NCDEQ Stmdard
Blue valves exceed Ne Solid Waste Section Limit (SWSL) (Eff. 2011)
Red valves exceed Ne Maximum Concentmfion Limit (MCL) (Eff. 2009)
NS=Not Specified
, "Report Limit" = Value is less Nat de Report Limit

Table 4
Summary of Vertical Hydraulic Gradients
Spring 2018 Semi -Annual Groundwater Monitoring
North Meck Infill Area Landfill
CEC Project No. 111-370.001
GRD
TOC
TOS
BOS
ScreenFall
2017
Fall 2017
Spring 2018
Well ID
1
Depth
Elev.
Elev.
TOS'
BOS1
Elev.
Elev.
Midpoint
W.L.pring
W.L. Elev.
2018L•
1
W.L. Elev.
VG
(ft)
(ft)
(ft)
(ft)
Ele(fe)v.
(TOC)1
(ft)
W.L. (TOC)
(ft)
MW-4 (i)
17.5
NM
678.10
7.50
17.50
670.60
660.60
665.6
10.88
667.22
10.79
667.31
MW-4D (i)
52
673.16
676.10
42
42
634.10
631.16
632.63
13.86
662.24
13.89
662.21
-0.15
MW-5 (i)
18
NM
672.92
8
18
664.92
654.92
659.92
8.49
664.43
8.05
664.87
0.06
MW-5D (i)
58
675.07
678.27
43
58
635.27
620.27
627.77
11.51
666.76
11.32
666.95
MW-7 (i)
23
NM
691.64
8
23
683.64
668.64
676.14
14.01
677.63
13.45
678.19
MW-7D (i)
64
700.59
703.72
49
64
654.72
639.72
647.22
27.80
675.92
27.41
676.31
-0.065
MW-8 (i)
28
NM
706.71
13
28
693.71
678.71
686.21
22.31
684.40
22.42
684.29
0.030
MW-8D (i)
100
716.25
719.02
85
100
634.02
619.02
626.52
33.40
685.62
32.95
686.07
MW-9 (i)
25
710.38
713.34
10
25
703.34
688.34
695.84
23.61
689.73
23.05
690.29
MW-9D (i)
80
710.72
713.24
65
80
648.24
633.24
640.74
23.78
689.46
23.41
689.83
-0.008
MW-11 (i)
22
NM
678.97
7
22
671.97
656.97
664.47
17.76
661.21
17.05
661.92
MW-11D (i)
50
NM
679.22
45
50
634.22
629.22
631.72
18.00
661.22
17.31
661.91
-0.0003
MW-12 (i)
32
NM
708.74
17
32
691.74
676.74
684.24
21.65
687.09
21.45
687.29
MW-12D i
54
NM
709.26
50
54
1 659.26
655.26
657.26
22.10
687.16
21.89
687.37
0.003
Notes:
(1) Measured in feet below ground surface
GRD = Ground
TOC
= Top -of -PVC Casing
NM =
Not Measured
TOS
= Top -of -Screen
BOS
= Bottom -of -Screen
W.L.
= Water Level
VG =
Vertical Gradient
Vertical Gradient =
Shallow Well Water Level Elev. -Deep Well Water Level Elev.
-
Shallow Well Screen Midpoint - Deep Well Screen Midpoint

APPENDIX A
Civil & Environmental Consultants, Inc.

Civil & Environmental
Consultants, Inc.
PROJECT -� �! 4 j JOB NUMBER ' r ,'� DATE LI 1
SAMPLE LOCATION 1D / "` w_ fLOCATION ACTIVITY START: END:
LATER LEVEL / WELL DATA
CASINGI ]MEASURED 3 Top or WELL
WELL DEPTH FT I ]HISTORICAL 1 3 TAP OF PROT. CASING (FROM GROUND)P FT OASINGlWELL DIFF, AP
FT
I)
WELL MATERIAL: WELL LOCKED?. WELL DIA. 1 3 2 INCH WATER LEVEL EQUIP.USED:
WATER DEPTH , 3FT [ ) PVC [ 7 C ) YES 13 4 INCH C 3 ELECT.COND PROSE
!) SS 1 3 NO 1 3 6 INCH C 3 FLOAT ACTIVATED
1 ] C ) PRESS. TRANSDUCER
L 3 .16 GAL/FT (21N.) GAL/VOI - C j
HEIGHT OF fT X 1 I .65 GAL/FT (4 IN.) _ WELL INTEGRITY; YES NO
WATER COLUMN 1 3 1.5 GAL/FT (6 IN.) PROT. CASING SECURE C ) I I
17 _GAL/FT (_IN,) TOTAL GAL PURGED CONCRETE COLLAR INTACT I 3 I I
OTHER
EQUIPMENT DOCUMENTATION
J
FIELD
TP
USED FOR.
DECON7kMINATION FLUIDS USED:
PURGING/5AMPLING EQUIP. U5ED: PURGING
SAMPLING
EQUIPMENT ID
(;J ALL THAT APPLY AT LOCATION
11
C)
PERISTALTIC PUMP
I I ETNYL ALCOHOL
C
I
[ 7
SUBMERSIBLE PUMP
I I DEIONCZE6 WATER
C
I
C )
BAILER—
I ) TSP SOLUTION
C
I
C)
PVC/SILICON TUBING
L I NE%ANE
1
I
I)
TEFLONISILICON TUBING
C I HNO3/D:I.WATER SOLUTION
- I
I
1 3
AIR LIFT -
1 I POTABLE WATER
C
3
1 3
HAND PUMP
1 3 NONE
L I
IN -LINE FILTER
1 )
1 3
PRESS/VAC FILTER
1 ]
II
13
ANALYSIS DATA
AMBIENT AIR VOA
PPM
WELL MOUTH PPM
FIELD
DATA
COLLECTED I
71N'L
IF}E
m in: 00
I L,: /Y
IIp.I
/y
C
)1N
CDNTkINER
PURGE DATA
E GAL{D
1�% [ .GALGAL,
i� GAL
9 GAL -
TEMPERATURE, pEI C
pH, units
SPECIFIC CONDUCTIVITY
OXIDATION-REDUCTION y/- qm
DIS OLVED 9 25 dePPM
DISSOLVED OXYGEN, -ppn
l9.2 ..
'7-.l,p
ma's
`r�
p.
_
���ip''NN
SAMPLE OBSERVATIONS:
TURBID
COLORED
[u1", CLOUDY
j CLEAR
I ] ODOR
SAMPLE COLLECTION REQUIREMENTS o.O4FT.w �JW`�)
(J IF REOtl[REO AT THIS LOCATION} I� 7�p / PR .[ Tf
J f FI LD ESERVATION VOLUME SAMPLE SAMPLE BOTTLE ID'S
ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED
i i pf yeast Gc EM k w cI 3 ! /
I I 1 3
13 A 13
1 I
NOT5
ES;
two

Civil & Environmental
Consultants, Inc.
PROTECT 1� \U - _% :.. )LL 146 NUMBER l -3 PATE !� t
SAMPLE LOCATION ID W LOCATION ACTIVITY START: END:
WATER LEVEL / WELL DATA
I )MEASURED I I TOP OF WELL CASING STICK-UP FT CASING/HELL RIFF. FT
WELL DEPTH FT I )HISTOR,ICAL C 170P OF PROT- CASING ('FROM GKWND)
i7
WELL MATERIAL: WELL LOCKED?: WELL CIA. E 3 2 INCH WATER LEVEL EQUIP. . USED:
WATER DEPTH 1� FT [ 3 PVC 17 C 7 YES [ 3. 4 INCH 17 ELECT.CONO+PROSE
I ] SS 17 NO 1 7 6 INCH [ 3 FLOAT ACTIVATED
1 ] C I PRESS* TRANSDUCER
E 7 .16 GAL/FT (2IN:) GAL/VOL [ 3
HEIGHT OF fT X 1 1 .65 GAL/FT (4 IN.) _ WELL INTEGRITY-: YES NO
WATER COLUMN [ 1 145 GAL/FT (6 ;Na) PROT. CASING SECURE E 3 17
C 7 _GAL/FT (, INM) TOTAL CAL PURGED CONCRETE COLLAR INTACT [ 3 F )
OTHER
EQUIPMENT DOCUHENTATIDN
J
IF
USED If OR:
AECONTAM INATSON FLUIDS USED:
PURGING/SAMPLING EQUIP. USED: PURGING
SAMPLING
EQUIPMENT ID
(J ALL THAT APPLY A7 LOCAT30N
C
1
I.I
PERISTALTIC PUMP i
t 7 ETHYL ALCOHOL
C
J
E I
SUBMERSIBLE PUMP �_
[ I DEICRIZEp WATER
(
}
T I
BAILER
I I TSP SOLUTION
[
7
I 3
PVC/SILICON TUBING
17 HEXANE
[
3
17
TEFLON/SILICON TUBING
17 HNO3/D.I*`WATER SOLUTION
L
3
L 3
AIR LIFT
I I POTABLE WATER
C
)
17
HAND PUMP
L 3 NONE
[ 7
IN -LINE FILTER
C 3
_
]
PRESS/VAC FILTER
17
I7
[7
FIELD ANALYSIS DATA
AMBIENT AIR VOA PPM WELL MOUTH - PPM FIELD DATA COLLECTED 13IN-LINE
IrV n•n�� 13IN CONTAINER
PURGE DATA
@ �:5 GAL
a _GAL
c� J�S GAL
as GAL
a GAL
TEMPERATURE, DEC C
pH, unixs
SPECIFIC CONDUCTIVITY'S
(audios /dm. � 25 deg. c)
O%I D,kTI QN-REDUCTI ON,•�/- my
DISSOLVED OXYGEN, ppm
12
�•�*f ..
G o
[
-064i—
63.2
O. fo(.!
b•9J_
SAMPLE COLLECTION REQUIREMENTS
(J IF REQUIRED AT THIS LOCATION) 1 J If
J IF FIELD PRESERVATION _ VOLUME SAMPLE
ANALYTICAL PARAMETER FILTERED METHCC REQUIRED COLLECTED
i7 I]
(I C]
E I �OUd� p Q/ • 1 ', ' y 17
C3 []
t
13
NOTES:
SAMPLE BOTTLE ID 5
/
SAMPLE OBSERVATIONS:
I ] TURBID
I ) COLORED
L 3 CLCUDY
L ] CLEAR
[ 7 ODOR

�� , � Consultants, Inc.
PROJECT I111 iA � � I JDB NUMBER I ,� DATE 'L �� I
SAMPLE LOCATION iD c��yU3 �/ ;\ . LOCATIDN ACTIVITY STARj: END
NA7£R LEVEL( /�NELL DATA
WELL DEPTH U i ]HISTORICAL [ 7] TDP 1)F PRDF�. EASING CSFROM BROJNP7P f7 � EASING/HELL DIFF. � fT
HELL MATERIAL: �i7ELL LOCKED?. l7ELL DIA. C 12 INCH HATER LEVEL EDUIP.. USED:
DATER DEPTH ��� F'f 17 PYC d 7 [ ]YES I J� 4 INCH C ] ELECT. CONpaPROBE
e 17 SS C ] NO t ] b INCH C ] FLOAT ACTIVATED
' [ 7 C 3 PRE55. TRANSDUCER
17 .T6 t,ALjFT (21N.) GAL/VOL' � [ 7
HEIGHT OF FT X i 7 .65 GALlFT (4 1N.) _ �.' 51ELL INTEGRITY-: YES NO
VA7ER COLi7MN C 7 9.5 GALJFT Z6 IN.7 PROT. CASING 5£LURE [ 7 17
17 _GAL/FT {�1N,) TOTAL GAL PURGE6 CONCRETE COLLAR INTACT [ 7 I I
OTHER
EDU3 PMENT DDCUMENTAT IDN
J IF USED 'FOR: DECOHTAM3NATiDN FLU3D5 USED:
PURGING/SAMPLING EDUJP. USES: PURGING SAMPLING EQUIPMENT ID (;/ ALL THAT APPLY AT LOCATION
I I f ] PERT $TACTIC ?UMP � i ] ETHYL ALCOHOL
{ 7 I I 5UBMERSIBLEPUHP �,T_ C 7 DE]ON12ED kATER
L ] [ 7 BAT LER [ 3 TSP S,OLUT4'ON
17 T J PVC/SILICON TUBdNG [ 7 HEXANE
[ 7 I J 7EFLOHfSICICOH�TI78IHG [ 1 HNO3/p.d.17ATER 501UTIDN
i ] 17 Aili L7 F7 � 13 POTABLE 1dAl'ER
17 I I NAND PUMP I I NONE
f I _ tN-L1NE FILTER I I
i 7 PRESS/VAC F7CIER 17
I7 II
FIELD ANALYSIS bATA
AMBIENT AIR VOA DPM MIELL HCXITH PPH FTELD DATA COLLECTED I IIN-1137E '
10•�In:{L; �� I ]TN CDNTAI NER
PURGEDATA
D ) GAL
a GAL.
.� GAL
is GAL'
TEMPERAYURE, DEC C
pH, vrif xs
SPECI FiC CONDUCTIVITY
dun3ipsJcm, a 25 de9.c)
D%I DATigN-REflUCT ION ,+/- mv
D155DLYED q%YGEN, �ppm
--II��GAL
I
L))��4 CC{{
y�1.3' 11
---���'I•
iL
/'
�(1.�
—f-�
�1w
!��"��II.�O��•7.��''�
--el=-Lr"—
SAMPLE OBSERYATIgNS:
17 TURBID
C l COLORED
17 CLOUDY
L 7 CLEAR
17 WDR
SAMPLE C4I LE CTJON REQUIREMENTS
IJ IF REOUlRED AT TH15 LOCATION} J dF
J IT FIELD PRESERVATION _ XQLUFIE SAMPLE SAMPLE BOTTLE ID'S
ANALYTICAL PARAFSETER FdLTE�AED HETNgD REgIy RED COLLECTED
[ I 13 / > !
13 ,�1 I _ [ 7 ! ! 1
I 9 (�T \ v � n � I � X� �/ 17 , t ,
IJ t"`"",,��''TT lM,y�l I Y II , , ,
[ I (p 1T / [ I ! / I
II C7 / f I
NOTES:

Civil & Environmental
Consultants, Inc.
PROJECT Nt JOB NUMBER III PATE '1 g
SAMPLE LOCATION ID W _ LOCATION ACTIVITY START: ERD; !�
WATER LEVEL / WELL DATA
L )MEASURED C I TOP OF WELL CASING STICK-UP FT CASING/WELL PIFF, FT
WELL DEPTH I )HISTORICAL C I TOP OF PROT. CASING (FROM GRDUNG)
rI
WELL
WATER DEPTH 60 FT
HEIGHT OF fT
WATER COLUMN
EQUIPMENT DpCUHENTAT ION
MATERIAL-
WELL
LOCKED?WELL
.1 iF USED 'FOR: DECDNTAM3NA7 TON FLU1D5 UHED:
PURGING/5AMP11 NG EQUIP. USED; PURGING SAMPLING I EQUIPMENT ID (;) ALL THAT APPLY AT LOCATION
I J I PERISTALTIC PUMP [ 3 ETHYL ALCOHOL
13 E J SUBMERSIBLE PUMP I I DE16NIZED WATER
C 7 11 BAI LER I I TSP SOLUTION
[ I I 7 PVCJSILICON TUBING [ J HEXANE
I 7 I J TEFLONJSItICON TUBING E 7 HNO3/1)=LWATER SOLUTION
E I I I AIR LIFT 17 POTABLE WATER
C 7 I J .HAND PUMP E J NONE
- 17 _ IN -LINE FILTER I I
{ ] PRESS/VAC FILTER [ J
t7 []
FIELD ANALYSIS DATA
AMBIENT AIR-VDA Pk WELL MOUTH PPM FIELD DATA COLLECTED 13[N-LINE
I q ��:C�< L41 n I N; Ibl IIn31N CONTAINER
PURGE DATA
a O•rj GAL
2 _,GAL.GAL.
P � GAL
a _GAL
TEMPERATURE, DEC C
PH units
SPECIFIC CONDUCTIVITY
OXIOATIOh O 25 deg Q)
OxIDAT3 DN R DUCTION ,+1'. mV
DISSOLVED OXYGEN PPq
—"
q
—`
SAMPLE OBSERVATIONS:
I ]
TURHID
C J
COLORED
17
CLOUDY
I7
CLEAR
17
ODOR
SAMPLE OOL LE CTION REQUIREMENTS
IJ IF REQUIRED AT THIS LOCATION) l If
✓ IF FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE ID'S
ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED
cI 1y/ zl i a J
I I n I ovrq
I�j {7 ! J J
[1
[ 7 COD
I7 l O I] I I I
I I '� ► E I
NOTES;

PROJECT NEI LL
SAMPLE LOCATION ID
HATFR LEVEL / WE It DATA
I )MEASURED
WELL DEPTH [ )HISTORICAL
WELL
WATER DEPTH FT
HEIGHT OF 3 CJ FT
WATER COLUMN U
M
LOCATION ACTIVITY
7tlP OF WELL CASING ST.ICK-UP. FT CASING/WELL DIFF. FT
TAP OF PROT. CASING {FROM GROUND) .,
LOCATION ACTIVITY
7tlP OF WELL CASING ST.ICK-UP. FT CASING/WELL DIFF. FT
TAP OF PROT. CASING {FROM GROUND) .,
MATERIAL:
EQUIPMENT DOCUMENTATION
,J IF USED FOR: DECONTAMINATION FLUIDS USED:
PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING EQUIPMENT TO (J ALL THAT APPLY AT LOCATION
I J I) PERISTALTIC PUMP - I ] ETHYL ALCOHOL
I J I ) sumeksIlm PUMP I ] DEIONIZEp 'WATER
I } L ) BAILER^'— [ ] TSP SOLUTION
• I } I } PVCJSILICON TUBING I ) HEXANE
L ] I ] TEFLON/SILICON TUBING I I HNO3/D-I.HA7ER SOLUTION
[ ) 17 AIR LIFT I I POTABLE HATER
17 [ 7 .NAND PDBP I ] NONE
I I IN -LINE FILTER L I
I I PRESS/VAC FILTER [ 7
II II
FIELD ANALYSIS DATA
AMBIENT AIR VOA PPM WELL M IN PPM FIELD DATA COLLECTED I I1N-LINE
[q . L{< I )IN CONTAINER
L— PURGE DATA
E D•'� GAL
O GALA
I. 7 GAL
a Z. GAL
a GAL
SAMPLE 'COLLECTION REQUIREMENTS
(./ IF REQUIRED AT THIS LOCATION) W IF
d IF FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE ID'S
ANALYTICAL PARAMETER FILTERED METHOD - REQUIRED COLLECTED
II [7
I I v U [ } J.
NOTES: •
SAMPLE OBSERVATIONS:
L ] TURBID
I J COLORED
17 CLOUDY
b ) CLEAR
[ ) ODOR
_�q J ( DATE
START• -� END;

� ��� ����r � � ,
��,�� �r � ��� ��
Civil & Environmental
Consultants, Inc.
DROJECT � /"' (� I- � („L , r � JOB NUMBER � � /��'� DATF y �� � �f
SANPif LOCATION !D 1 � w _ ,� '� LOCATION ACTIVITY START: �� END: �� � j
( i
WATER LEVEL / WELL DATA '
WELL DEPTX Fi ( )HISTORICAL [ ; TOP Of PROT. CASING C(FRON GRNNO )P FT USING/YELL DIFF. FT
WELL MATERIAL: WELL LOCKED?: HELL 6IA. [ 7 2 INCH � WATER LEVEL EQUIP. USED:
WATER DEPTx b ,^,-j FT ( 7 PVC [ 7 C 7 YES C J 4 SNLN 17-ELECT.COND.PROBE
C J SS [ 7 NO C 7 6 INCH C 7 FLOAT ACTIVATED
[ 7 C ] PRESS. TRANSDUCER
[ ] .16 GAL/FT (2 IN.) GALNOL [ )
xE1GxT OF FT % [ 7 .65 GALlFT (4 IN.) = HELL SNTEGRIT7: YES NO
uA7ER COLUMN C 7 1.5 GAL/FT (6 IN.) PROT. CASING SENRE C J C 7
C 7 _GAL/F7 (_IN.) TOTAL GAL PURGED CONCRETE COLLAR INTACT I I [ ]
O7MER
EDUIPNENT DOCUMENTATION
J
iF
USED FOR:
PURGIH6/SAMPLING EDUID. USED: PURGING
SAMPLING
C
J
I J
PERISTALTIC PUMP
[
7
[ J
5UBMER518LE PUMP
I
I
C 7
BAi L£R
I
J
[ 7
PVC151U CON Tt181NG
C
J
[ 7
TEFLON/S1LiCON TUBING
[
7
[ J
AIR LIFT
[
I
[ 3
NAND PIMP
C 7
[N-LINE FILTER
[ ] �
PRESS/VAC FILTER
CI
IJ
DECONTAMINATION FLUIDS USED:
EQUIPMENT ID (J ALL THAT APPLY AT LOCATION
f 7 ETHYL ALCOHOL
17 DEI OHI2ED LATER
( 7 TSP SOLUTION
[ 7 NE%ANE
[ ] NN03/D.3.WATER SOLUTION
[ 7 POTABLE VATER
( ] NONE
[]
r]
F IECO ANALYSIS DATA
AMBIENT AIR VOA PPN WELL MOUTx PPN FIELD DATA COLLECTED [ 71N-LINE
( 71N CONTAINER
PURGE DATA
a /I/�L O*T,�H
��/.��- g/�y,
a � t— GAC
a 3��� 4A4
a 3 %N /�ffAk
7ENDERATURE, DEG C
px, units �
SPEC1 FlC CONDUCTJVITT
(uMos/cm. a 25 tleg.c)
OXlDATI ON-REDUCTI ON,�/- my
DISSOLVED OXYGEN, ppm
i�-t'I �--
1�-g�
1 �-F�
1e2 .�-I�Ci
! a- �'�
'"I ..1�
I JF g
�
( I b (,
7'-`�
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1. I�l
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to '
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- �1 5-
ii
-�
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r;-�_
D�( 7
f>. h4
! r'�t� ! ,y r /� ) 1 rr e 1 � !, J ! 7S 7 `1 1 � 7 n � `7 i (O �""/
SAMPLE COLLECTION REQUIREMENTS
(J 1F REQUIRED AT THIS LOCATION) � IF
J IF FIELD PRESERVATION _ VOLUME SAMPLE SAMPLE BOTTLE ID'S
ANALYTI[AL PARAMETER FILTERED METHOD REQUIRED COLLECTED
[J 1'
[ 7 1 11V (� {� i'C17
C] .(� �V C�' ��07
[ I � IJv
[ ) li,
[ I (AAA '(�'
( ] ���Il
[7 �� Q
NOTES:
`r}h. J i �.'S
J�. z�
'" /`n.�
[J
I7
[7
[7
Cl
CI
L]
L7
�� ��5�' � � �����
SAMPLE OBSERVATIONS:
[.]
TURBID
C I
COLORED
C J
CLOUDY
[ 7
CLEAR
( 7
ODOR
/ / /
/
!
/
/
/
/
/
/
/
/
1
/
{
/
/
1

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t
_4 a"�1, IINAN'
Civil & Environmental
Consultants, Inc.
PROJECT �; /VfL �._ �h I , JOB NUMBER -OQI DATE
SAMPLE LOCATION ID fJ� IJ — " LOCATION ACTIVITY END:
uATER IEVEI / vE LI DATA
CASINGI ]MEASURED 1 3 TOP OF WELL
WELL DEPTH' FT I ]HISTORICAL I I TOP Of ROT. CASING (CRC-
WELLP FT CASING/YELL Dif F.
FROM ) FT
MATERIAL: WELL LOCKED?: WELL DIA. 112 INCH WATER LEVEL EQUIP- USED:
WATER DEPTH FT I ] PVC I ) I I YES C 14 INCH [ I ELECT-COND.PROSE
17 SS C l NO C 7 6 INCH 17 FLOAT ACTIVATED
C 7 t ) PRESS. TRANSDUCER
I I -16 GAL/FT (2 IN,) GAL/VOL 1 I
HEIGHT OF FT X C 7 -65 GAL/FT (4 1NJ = WELL INTEGRITY: YES NO
WATER COLUMN t ) 1.5 GAL/FT (6 IN-) PROT. CASING SECURE C 7 I I
I I GAL/FT (_IN,) TOTAL GAL PURGED CONCRETE COLLAR INTACT 17 I )
OTHER
EOUI PMENT DOCUMENTATION
PURGING/SAMPL]NG EQUIP. USED:
J
IF USED FOR:
PURGING
SAMPLING
C7
I]
I7
C]
[I
f7
I7
II
[7
I)
Cl
C)
[7
C]
C]
II
t7
I]
PERISTALTIC P1RIP
SUBMER519LE PUMP
BAILER
PVC/SILICON TUBING
TEFLON/SILICON TUBING
AIR LIFT
HAND PUMP
IN -LINE FILTER
PRESS/VAC FILTER
DECONTAMINATION FLUSDS USFD:
EQUIPMENT ID (J ALL TNAT APPLY AT LOCATION
17 ETHYL ALCOHOL
1 7 DEIONIZED WATER
I I TSP SOLUTION
17 HEXANE
1 ) HNO3/D-1.WATER SOLUTION
17 POTABLE WATER
I I NONE
C7
f IELD ANALYSIS DATA
AMBIENT AIR VOA PPM WELL MOUTH PPM FIELD DATA COLLECTED C ]IN -LINE
I )IN CONTAINER aL
PURGE DATA
D C_ �
a I/y' LggL
a GAL
SAMPLE 095ERVA710N5:
TEMPERATURE, DEG C __(_-_}j_. L jj -'�C� �,� - ( j
PN, un175 - �/
SPECIFIC CONDUCTIVITY
(wthos/cm. 0 25 de9.c) t 3�- i 31 qi i 4w 12
OXIDATION-REDUCTION,•/-mv—1y_ 7,`i —1.57 4O
DISSOLVED OXYGEN, ppm D-'d -) D - .3�>
I ) TURB10
17 COLORED
I l CLOUDY
CJ CLEAR
[ 7 ODOR
: ry K j [v`-y Wit? V'�
SAMPLE COLLECTION REQUIREMENTS
(J 2F REQUIRED AT THIS LOCATION) f IF
4 IF FIELD PRESERVATION _ VOLUME SAMPLE SAMPLE BOTTLE ID'S
ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED
t ) COD
I 17
NOTES:
-5�w 14 C (<(Q)
: ry K j [v`-y Wit? V'�
SAMPLE COLLECTION REQUIREMENTS
(J 2F REQUIRED AT THIS LOCATION) f IF
4 IF FIELD PRESERVATION _ VOLUME SAMPLE SAMPLE BOTTLE ID'S
ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED
t ) COD
I 17
NOTES:
-5�w 14 C (<(Q)

Civil & Environmental
Consultants, Inc.
PROJECT �,� t_ �.- I _044 I' JOB NUMBER ' —�` I DATE
SAMPLE LOCATION ID I j /_[ LOCATION ACTIVITY START: END:
L
WATER LEVEL / WELL DATA
I ]MEASURED C i TOP OF WELL CASING STICK-UP FT CASING/WELL DIFF. FT
WELL DEPTH fT C ]HISTORICAL 17 TOP OF PROT. CASING (FROM GROUND)
CI
WELL MATERIAL: WELL LOCKED?: WELL DIA. t 7 2 INCH - WATER LEVEL EQUIP. USED:
WATER DEPTH fT 17 PVC C 7 C I YES t 7 4 INCH 17 ELECT.COND-PROBE
C 7 SS L I NO t J 6 INCH [ J FLOAT ACTIVATED
L J I I PRESS. TRANSDUCER
C 7 .16 GAL/FT (2 IN.) GALNOL C I
HEIGHT OF FT X I 1 .65 GALIFT (4 IN-) = WELL INTEGRITY: YES NO
WATER COLUMN C 7 1.5 GAL/FT (6 IN.) PROT. CASING SECURE C 7 C 1
L 7 _GAL/PT (_IN.) TOTAL GAL PURGED CONCRETE COLLAR INTACT C I C 7
OTHER
EQUIPMENT DOCUMENTATION
PURGING/SAMPLING EQUIP- USED:
J CF
USED FOR:
PURGING SAMPLING
it
I
[]
PERISTALTIC
PUMP
SUBMERSIBLE PUMP
BAILER
PYC/SILICON TUBING
TEFLON/SILICON TUBING
AIR LIFT
HAND PIMP
IN -LINE FILTER
PRESS/VAC FILTER
DECONTAMINATION FLUIDS USED:
EQUIPMENT ID LJ ALL THAT APDL7 AT LOCATION
C ) ETHYL ALCOHOL
I I DEIONIZED WATER
17 TSP SOLUTION
C I HEXANE
t 7 HNO3/D-I.WATER SOLUTION
17 POTABLE WATER
C I NONE
I7
[7
FIELD ANALYSIS DATA
AMBIENT AIR VOA PPN WELL MOUTH PAM fIELO DATA COLLECTED t 71N-LINE
C ]IN CONTAINER
PURGE DATA
a
i /—
Dp7y
a GAL
SAMPLE OBSERVAT10N5:
TEMPERATURE, DEG C
PH, units
SPECIFIC CONDUCTIVITY
(umho5/cm, a 25 deg.c>
OXIDATION-REDUCTION,+/- my
DISSOLVED OXYGEN, ppm
l r�-�'( i0
'�.. % )
1:�'"V 7
i �, �
) 3 P a-
C TURBID �.)
COLORED
7 CLOUDY '
u
I ) ODOR
'-7. d l '
i . c) A
t z
�. t f
�
% �I
—j j-O
_,; �4.5
—C.�S.S
f _ S-�
D-S(p
��, > t
!')- 4 4
SAMPLE COLLECTION REQUIREMENTS
IF REQUIRED AT THIS LOCATION) (J
✓ IF FIELD
ANALYTICAL PARAMETER FILTERED
II
1I
I 1 �
C I
I7 PO
I]
NOTES:
J IF
PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE 1D'S
METHOD REOUiRED COLLECTED
Cl
13

Civil & Environmental
Consultants, Inc.
PROJECT I JUNAL F _ t �q / i
SAMPLE LOCATION 1D �t/� �J._ -7
JOB NUMBER .i%.�I DATE
LOCATION ACTIVITY START: 10L)O END:
DATER LEVEL /WELL DATA
CASINGI ]MEASURED I TOP OF WELL WELL DEPTH FT I )HISTORICAL [ I TOP OF PROT. USING (P FT USING/WELL Dlff.
FROM GRCUND)FT
WELL MATERIAL: WELL LOCKED?: WELL DIA. 17 2 INCH WATER LEVEL EQUIP. USED:
WATER DEPTH FT [ ] PVC 17 [ 7 YES 17 4 INCH C 7 ELECT.COND.PROBE
I l SS 17 NO 17 6 INCH 17 FLOAT ACTIVATED
17 C 7 PRESS. TRANSDUCER
[ 7 .16 GAL/FT (2 1N,) GAL/YOL t 7
HEIGHT OF FT X I ) .65 GAL/FT (4 1N.) _ --- WELL INTEGRITY: YES NO
WATER COLUMN L 7 1.5 GAL/Fi (6 IN.) PROT. CASING SECURE L 7 C J
L I _GAL/FT (.IN.) TOTAL GA l PURGED CONCRETE COLLAR INTACT C 3 17
OTHER
EQUIPMENT DOCUMENTATION
J IF USED FOR: DECONTAMINATION FLUIDS USED:
PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING EQUIPMENT ID (J ALL THAT APPLY AT LOCATION
17 [ 7 PERISTALTIC PUMP I )ETHYL ALCOHOL
I 1 17 SUBMERSIBLE PUMP t 7 DEION12ED WATER
C 1 C 7 BAILER i 7 TSP SOLUTION
C I 17 PVC/SILICON TUBING C l HEXANE
C 7 t 7 TEFLON/SILICON TUBING C 7 MN03/D.I.WATER SOLUTION
C 7 C l AIR LIFT t 7 POTABLE WATER
[ 7 17 HAND PUMP C 7 NONE
C 7 _ TN -LINE FILTER I )
[ 7 PRESS/VAC FILTER 17
[] [7
FIELD ANALYSIS
DATA
AMBIENT AIR VOA PPM WELL MOUTH PPM FIELD DATA COLLECTED [ 71N-LINE
177N CONTAINER
PURGE DATA
Loki
t L 'OAiL
of 11 iy �- 4ii q.
a�(r>
L
jj�f8fl1
i
TEMPERATURE, DEC C
�I
1`'� :�-�
(�Y �i
t`f-�%
�-72-
PH, uni TS
/+y(2
(� �/
i ! cis
'
SPECIFIC CONDUCTIVITY
�, i 3
/ 3J-(p
(umhoslcm. a 25 deB.c)
OXIDATION-REDUCTION,•/- my
t(1;7jN-0
DISSOLVED OXYGEN, PPM
n. (7�i
O- ;
h. S's
lJ.ti
SAMPLE 065ERVATIONS:-3(�1 i..
[ 7 TURBID �y'7�
C 7 COLORED
CLOUDY
CLEAR
ODOR G.IS
17 (3L-L
C 7 3
SAMPLE COLLECTION REQUIREMENTS `
(J 1F REQUIRED AT THIS LOCATION) ,T IF
,7 IF FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE ID$S
ANALYTICAL PARAMETER FILTERED METHOD REWIRED COLLECTED
[ 1 pQp L I / IfI7 I7 ,
I7 I7 ,
NOTES:
9
5�mr1.a�)°Gib

MEET` A1115,43"F/
RAW I,
Civil & Environmental
Consultants, Inc.
PROJECT M.t y, , , JOB NUMBER DATE �'�',I 17 T
SAMPLE LOCATION ID 1 — /l I) - LOCATION ACTIVITY START: ='j! SJ END:
1 iI
WATER LEVEL / WELL DATA
( ]MEASURED ( 7 TOP OF WELL CASING STICK-UP FT CASINGIWELL DIFF_ Ft
WELL DEPTH FT [ ]HISTORICAL [ 7 TOP OF PROT. CASING (FROM GROUND)
WELL MATERIAL: WELL LOCKED?: WELL DIA. I ] 2 INCH . WATER LEVEL EQUIP. USED:
WATER DEPTH 41 L4 FT ( 7 PVC ( 7 1) YES I ] 4 INCH C ] ELECT.COND.PROBE
C l SS C 7 NO 17 6 INCH C] FLOAT ACTIVATED
C 7 C 7 PRESS, TRANSDUCER
C J .16 GAL/FT (2 IN
GAL/YOL C 7
HEIGHT OF FT X C ] .65 GAL/FT (4 IN.) c WELL INTEGRITY: YES NO
WATER COLUMN C ] 1.5 GAL/FT (6 1N.) PROT. CASING SECURE C 7 17
C ] _GAL/FT (_IN.) TOTAL GAL PURGED CONCRETE COLLAR INTACT C 7 C J
OTHER
EQUIPMENT DOCUMENTATION
.1 IF USED FOR: DECONTAMINATION FLUIDS USED:
PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING EQUIPMENT 10 (J ALL THAT APPLY AT LOCATION
1X] 1�1 PERISTALTIC PUMP ( J ETHYL ALCOHOL
[ 7 [ 7 SUBMERSIBLE PUMP 17 DEIONI2ED WATER
C ] VJ BAILER 17 TSP SOLUTION
I J C ] PVC/SILICON TUBING ( 7 HEXANE
I ] 17 TEFLON/SILICDN TUBING I J HNO3/D.I.WATER SOLUTION
C ) I ] AIR LIFT I ] POTABLE WATER
I I C 7 HAND PUMP C 7 NONE
C 7 _ IN -LINE FILTER C )
C ] PRESS/VAC FILTER C I
I C)
FIELD ANALYSIS DATA
AMBIENT AIR VOA PPM WELL MOUTH PAM FIELD DATA COLLECTED [ 71N-LINE
[ ]IN CONTAINER
PURGE DATA
� BA'l
el �i' L 81W
a { L BA4
a 11jil /--Gfb
a (7j3L gA.p
-rxrb L,_i�i G--7s 0S
SAMPLE COLLECTION REQUIREMENTS
(J IP REQUIRED AT THIS LOCATION) .( IF
4 IF FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE ID'S
ANALYTICAL PARAMETER. FILTERED METHOD - REQUIRED COLLECTED
SAMPLE OBSERVATIONS:
C ] TURBID
C I COLORED
[ 7 CLOUDY
[X7 CLEAR
[ 7 ODOR
boos ;
C7
NOTES:

Alf
n
rno_g,7
Civil & Environmental
Consultants, Inc.
PROJECT L� �`v'� _ ,1 ( JOB NUMBER i 7Q�� DATE
SAMPLE LOCATION ID �,j LOCATION ACTIVITY START: ��,�K' END:
WATER LEVEL / WELL DATA
I ]MEASURED 17 TOP OF WELL CASING ST1CK•UP FT CASING/YELL DIFF. FT
WELL DEPTH Fi I ]HISTORICAL 1 I TOP OF PROT. CASING (FROM GROUND)
I]
�f WELL MATERIAL: WELL LOCKED?: WELL DIA. 112 INCH WATER LEVEL EQUIP. USED:
WATER DEPTH �� �I FT I ] PVC I I I ] YES 114 INCH I I ELECT.COND.PROBE
I] SS I I NO L 7 6 INCH I] FLOAT ACTIVATED
PRESS TRANSDUCER
NEIGHT OF FT
WATER COLUMN
EQUIPMENT DOCUMENTATION
I ) .76 GALIFT (2 IN)
% 17 .65 GALIFT (4 INJ
C ) 1.5 GAL/FT (6 IN.)
I I _GAL/FT C_IN.)
Cl C.
7
GTOTAL AL/VDL PURGED
C
I
WELL INTEGRITY: YES NO
PRO
T. CASING SECURE C 7 C I C 7 C ICONCRETE COLLAR INTACT 1 3 L I
OTHER
J IF USED FOR; DECONTAMINATION FLUIDS USED:
PURGING/SAMPLING EOUIP. USED: PURGING SAMPLING EWIPMENT 1D CJ ALL THAT APPLY AT LOCATION
I J ( I PERISTALTIC PUMP I I ETHYL ALCOHOL
I ) [ ] SUBMERSIBLE PUMP I I DEIONI2ED WATER
[ ] 17 BAILER C I TSP SOLUTION
I ] I ] PVC/SILICON TUBING I I HEXANE
I ] C ) TEFLON/SILICON TUBING L ) HNO3/D.1.WATER SOLUTION
[ ] L I AIR LIFT I ] POTABLE WATER
C I I I HAND PUMP C I NONE
17 _ IN -LINE FILTER C I
C I PRESS/VAC FILTER [ I
FIELD ANALYSIS DATA
AMBIENT AIR VOA PPM WELL MOUTH PPM FIELD DATA COLLECTED C IIN-LINE
I )IN CONTAINER
PURGE DATA Ia /1�A(- D I L GAQ a I /�(" a 1 AIAt-ja GAL (SAMPLE OBSERVATIONS:
p _ L ) TURBID
TEMPERATURE, DEG C 1T_- 7 G 1 1. j 7 _5 i C 7 COLORED
pH, mits I ) CLOUDY
SPECIFIC CONDUCTIVITY — 1v7 LLtAN
<urthoslcm, a zs aeB. c7 S [ I DOOR
OXIDATION-REDUCTION,+/-
DISSOLVED OXYGEN, PPm 1 1- / > ).--7
SAMPLE COLLECTION REOU7RfHEN TS
(J Ii REOUCRED AT THIS LOCATION) ./ If
J IF FIELD PRESERVATION _ YDL(M£ SAMPLE SAMPLE BOTTLE 1D'S
ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED
CI CI
[I bow CI
C1 1J I7
NOTES:
Cl C.
7
GTOTAL AL/VDL PURGED
C
I
WELL INTEGRITY: YES NO
PRO
T. CASING SECURE C 7 C I C 7 C ICONCRETE COLLAR INTACT 1 3 L I
OTHER
J IF USED FOR; DECONTAMINATION FLUIDS USED:
PURGING/SAMPLING EOUIP. USED: PURGING SAMPLING EWIPMENT 1D CJ ALL THAT APPLY AT LOCATION
I J ( I PERISTALTIC PUMP I I ETHYL ALCOHOL
I ) [ ] SUBMERSIBLE PUMP I I DEIONI2ED WATER
[ ] 17 BAILER C I TSP SOLUTION
I ] I ] PVC/SILICON TUBING I I HEXANE
I ] C ) TEFLON/SILICON TUBING L ) HNO3/D.1.WATER SOLUTION
[ ] L I AIR LIFT I ] POTABLE WATER
C I I I HAND PUMP C I NONE
17 _ IN -LINE FILTER C I
C I PRESS/VAC FILTER [ I
FIELD ANALYSIS DATA
AMBIENT AIR VOA PPM WELL MOUTH PPM FIELD DATA COLLECTED C IIN-LINE
I )IN CONTAINER
PURGE DATA Ia /1�A(- D I L GAQ a I /�(" a 1 AIAt-ja GAL (SAMPLE OBSERVATIONS:
p _ L ) TURBID
TEMPERATURE, DEG C 1T_- 7 G 1 1. j 7 _5 i C 7 COLORED
pH, mits I ) CLOUDY
SPECIFIC CONDUCTIVITY — 1v7 LLtAN
<urthoslcm, a zs aeB. c7 S [ I DOOR
OXIDATION-REDUCTION,+/-
DISSOLVED OXYGEN, PPm 1 1- / > ).--7
SAMPLE COLLECTION REOU7RfHEN TS
(J Ii REOUCRED AT THIS LOCATION) ./ If
J IF FIELD PRESERVATION _ YDL(M£ SAMPLE SAMPLE BOTTLE 1D'S
ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED
CI CI
[I bow CI
C1 1J I7
NOTES:

Civil & Environmental
Consultants, Inc.
PROJECT NMI
N ILL
SAMPLE LOCATION !D
JOB NUMBER
LOCATION ACTIVITY
` DATE
START: END;
WATER LEVEL / WELT DATA
I ]MEASURED C ] TOP OF WELL CASING STICK-UP FT CASINGIWELL DIFF. fT
WELL DEPTH I ]HISTORICAL C I TOP OF PROT. CASING (FROti GNIw".D)
C]
WELL MATERIAL; WELL LOCKED?: WELL DIA. I T 2 INCH - WATER LEVEL EQUIP.. USED:
WATER DEPTH 'y2 FT C 7 PVC C J C] YES I T 4 INCH C 7 ELECT.COND.PROBF
I I SS 17 NO 17 6 INCH C ] TLOAT ACTIVATED
C ] C I PRESS. TRANSDUCER
1 ] .16 GAL/FT (2 1N:) GAL/VOL C 7
HEIGHT OF FT % I I .65 GAL/FT (4 IN.) _ WELL INTEGRITY; YES NO
WATER COLUMN 1 ] 1.5 GAL/FT (6 IN.) - PHOTO CASING SECURE [ I I 7
17 ,GAL/FT (_IH.) TOTAL GAL PURGED CONCRETE COLLAR INTACT I ] 1 I
OTHER
EQUIPMENT DOCUMENTATION
,1 IF USED FOR: DECONTAMINA71ON FLUIDS USED:
PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING EQUIPMENT ID U ALL THAT APPLY AT LOCATION
C 7 I7 PERISTALTIC PUMP I ] ETHYL ALCOHOL
I I 1] SUBMERSIBLE PUMP I I OEIONIZED WATER -
C ]- I I BAILER C 7 TSP SOLUTION
I I I I PVC/SILICON TUBING I I HEXANE
I) I I TEFLON/SILICON TUBING C I HNO3/D:I.WATER SOLUTION
C I I I AIR LIFT - I I. POTABLE WATER
C I 17 HAND PUMP 17 NONE
I I IN -LINE FILTER C ]
I ] PRESS/VAC FILTER I I
I7 I7
FIELD ANALYSIS DATA
AMBIENT AIR VOA PPM WELL MOUTH - PPM FIELD DATA COLLECTED 17IN-LINE '
&. ry-4%&� 1 W4Z5 1 IIN CONTAINER
PURGE DATA
E _GAL
D I GAL
QGAL.
a GAL
D GAL
SAMPLE OBSERVATIONS:
I i
[ 7 TURBID
C l COLORED
CLOUDY
L ] CLEAR
[ ] ODOR
SAMPLE COLLECTION REQUIREMENTS .
(J IF REQUIRED AT THIS LOCATION) d IF
J IF FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE ID'S
ANALYTICAL PARAMETER FILTERED METHOD ' REQUIRED COLLECTED
I3 IT J J I
I]
IT
I1 �/o L1� IT
NOTES;

x1 A
Civil & Environmental
J r Consultants, Inc.
PROJECT JJ �1 �� — yt-F-S��7�'� �1 JOB NUMBER •Da DATE
SAMPLE LOCATION ID i� ���j - �-1 / )� LOCATION ACTIVITY START: 3 5"U END: jgg6)
WATER LEVEL / WELL DATA
CASINGr )MEASURED I I TOP OF WELL WELL DEPTH FT I )HIST RICAL [ I TOP Of ROT- CASING (P FT CASING/WELL Diff.
FROM GROUND ) FT
ALL MATERIAL:
WELL LOCKED?:
WELL DIA. 2 ]
2
HEIGHT OF F7
WATER COLUMN
EQUIPMENT DDCUMENTATSON
INCH WATER LEVEL EQUIP. USED:
✓ CF
FIELD
USED FOR:
DECONTAMtNAT10N FWIDS USED:
PURGING/SAMPLING EQUIP. USED: PURGING
SAMPLING
EQUIPMENT ID
U ALL THAT APPLY AT LOCATION
I J
I J
PERISTALTIC PUMP
17 ETHYL ALCOHOL
I J
C )
SUBMERSIBLE PUMP
17 DEIONIZED WATER
1 7
C]
BAILER
C 7 TSP SOLUTION
C I
C)
PVC/SILICON TUBING
C J HEXANE
C J
E]
TEFLON/SILICON TUBING
C 7 HNO3/D.I.VATER SOLUTION
L J
C J
AIR LIFT
1 J POTABLE WATER
C I
C J
HAND PUMP
C J NONE
17
IN -LINE FILTER
C ]
_
C J
PRESS/VAC FILTER
17
I
I
ANALYSIS DATA
AMBIENT
AIR VOA
PPM YELL MOUTH
PPM F3ELD
DATA COLLECTED
[ 71N-LINE
[ 71N CONTAi HER
� PURGE DATA
a �LAi:r
a /4)-LJIAC
a 13/yL
a WL
a GAL
SAMPLE 085ERVATI
TEMPERATURE, DEG C I L L! "
y
pH, i t5
SPECIFIC CONDUCTIVITY
(umho5/cm, a 25 deg,c) %� 3 3
OXIDATION•REDUCTION,+/- j
DISSOLVED OXYGEN, ppm
DNS:
C ] iUR81D
C ] COLORED
[ ] CLOUDY
C ] CLEAR
[ 7 ODOR
tNrrb 6Ni�: D.R
SAMPLE COLLECTION REQUIREMENTS
(✓ IF REQUIRED AT THIS LOCATION) ✓ IF
✓ IF FIELD PRESERVATION _ VOLUME SAMPLE SAMPLE BOTTLE ID$S
ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED
[7 I7
NOTES:
CON
(`10
tNrrb 6Ni�: D.R
SAMPLE COLLECTION REQUIREMENTS
(✓ IF REQUIRED AT THIS LOCATION) ✓ IF
✓ IF FIELD PRESERVATION _ VOLUME SAMPLE SAMPLE BOTTLE ID$S
ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED
[7 I7
NOTES:
CON
(`10

A4 INE
4r tAMww '4ANNYJOW
Civil & Environmental
(' Consultants,
In�c�. j
PROJECT !J IA L' F _ ( v� y-, Z JOB NUMBER fit_` DATE
SAMPLE LOCATION ID i M w G�� �71 LOCATION ACTIVITY START: C) END:
PATER LEVEL / WELL DATA
( ]MEASURED ( I TOP Of WELL CASING STICK-UP FT CASING/WELL DIFF- FT
WELL DEPTH FT C ]HISTORICAL C 7 TOP OF PROT. CASING (FROM GROUND)
I]
WELL MATERIAL:
WATER DEPTH 7 PVC ( 7_
[ 7 SS
C 7 .ib GAL/FT
HEIGHT OF fT X C 7 .65 GAL/FT
WATER COLUMN ( 7 1-5 GAL/FT
L ) GAL/FT
EQUIPMENT DOCUHENTATl ON
PURGING/SAMPLING EOU1 P- USED:
WELL
LOCKED?: WELL DIA. L 7
2
✓
IF
USED FOR:
PURGING
SAMPLING
C7
[3
[7
C)
I7
[7
I]
C7
C7
CJ
C]
tl
PERISTALTIC
PUMP
SUBMERSIBLE
PVC
TE
PUMP
BAILER
/SILICON TUBING
FLON/SILICON TUBING
AIR LIFT
HAND PUMP
IN -LINE FILTER
PRESS/VAC FILTER
INCH - WATER LEVEL EQUIP. USED:
INCH ( 3 ELECT.COND-PROBE
INCH ( J FLOAT ACTIVATED
C 7 PRESS- TRANSDUCER
YELL INTEGRITY: YES NO
PROT. CASING SECURE C ] C 7
CONCRETE COLLAR INTACT C 3 17
OTHER
DECON7ANINA710N FLUIDS USED:
EQUIPMENT ID (J ALL THAT APPLY AT LOCATION
17 ETHYL ALCOHOL
C 7 DEIONIZED WATER
17 TSP SOLUTION
[ 7 HEXANE
[ J HNO3/D.I.WATER SOLUTION
17 POTABLE WATER
L 3 NONE
CI
Il
F IELO ANALYSIS DATA
AMBIENT AIR VOA PPX WELL MONTH PPM FIELD DATA COLLECTED C 7IN-LINE
C ]IN CONTAINER
- PURGE DATA
Ag "� L B
ID
a
GAL
-��rb EN�"�1
SAMPLE. COLLECTION REQUIREMENTS
W IF REQUIRED AT THIS LOCATION) ✓ IF
,1 1F FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE ID'S
ANALYTICAL PARAMETER FILTERED METHOD REWIRED COLLECTED
I
SAMPLE OBSERVATIONS:
C 7 TURBID
( 7 COLORED
( ) CLOUDY
(tl CLEAR
( 7 ODOR
[7
I7 v tl ! ! I
NOTES:
[7
I7 v tl ! ! I
NOTES:

Civil & Environmental
Consultants, Inc.
PROJECT pV I V(b 10 1 Lam ... JOB NUMBER ( PATE
SAMPLE LOCATION ID 'Y\w _ ��( j .0 LOCATION ACTIVITY START.: END:
WATER LEVEL / WELL DATA 1 t
I ]MEASURED 1 i TOP OF WELL CASINO STICK-UP FT CASING/WELL DiFF. FT
WELL DEPTH PT I ]HISTORICAL [ 7 TOP OF PROT_ CASING (FROM GROUND)
I]
2 WELL MATERIAL: WELL LOCKED?: WELL DIA. C 1 2 INCH WATER LEVEL EQUIP.. USED:
WATER DEPTH 59 _ FT 1 ] PVC I I 17 YES I 1 4 INCB E 7 ELECT.COND.PROBE
11 SS 11 NO L] 6 INCH 1 1 FLOAT ACTIVATED
HEIGHT DF FT
WATER COLUMN
I ]
.Tb GALJfT
(2
1N:y
17
.65 GAL/FT
(4
IN.) _
1 1
115 GAL/FT
(6
IN.)
1 7
_GALIFT
C ] 17 PRESS, TRANSDUCER
GALJVOL
TOTAL GA
L PURGED
I]
WELL INTEGRITY: YES ND
PROT.
CASING SECURE I I I ]
CONCRETE COLLAR INTACT [ ] 17
OTHER
EQUIPMENT DDCUMENTRTION
,( IF USED POR: _ DECONTAMINA47TON FLUIDS USED:
PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING EQUIPMENT 10 (✓ ALL THAT APPLY AT LOCATION
1 7 I I PERISTALTIC PUMP 17 ETHYL ALCOHOL
C 7 17 SUBMERSIBLE PUMP - C 1 DEIONIZED WATER
C 7 17 BAILER— I ] TSP SOLUTION
I I 1 7 PVC/SILICON TUBING [ ] HEXANE
13 1 7 TEFLON/SILICON TUBING 11 HNO3/D:I.WATER SOLUTION
11 i] AIR LIFT, I I POTABLE WATER
E 7 I I .NAND PUMP E I NONE
L 1 _ IN -LINE FILTER [ 7
E 7 PRESS/VAC FILTER [ 1
FIELD ANALYSIS DATA
AMBIENT AIR VOA PPMWELL MOUTH PPH FIELD DATA COLLECTED I IIN-LINE '
., L ]IN CONTAINER
j.
PURGE DATA E GAL O _GAL D GAL GAL H GAL SAMPLE OBSERVATIONS:
TEHPERATUR£, DEC C .p - fp• Q L 7 COLORED
PH, tmixs (0 I I TURBID
$ C 9 CLOUDY
SPECIFIC CONDUCTIVITY g%o2 f' L 1 CLEAR
(uhoslcm. 2 25 deB•c) —0� 02H E I ODOR
DISSOLVED -REDUCTION,+/- my Ira
DISSOLVED OXYGEN, ppm (,fn^�— 45
V
SAMPLE COLLECTION REQUIREMENTS
LJ IF REQUIRED AT THIS LOCATION) � ./ �Tq IF FIELD PRESERVATION VOLUME 1-SW1l1PLE� SAMPLE BOTTLE ID'S
ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED
C1
C7
[T
I3
t7
CI
CO
J
/
I
/
I
J
7
J
J
/
t
f
J
/
,
f
/
/
/
J
/
J
I
/

PROJECT NM(�IF-i JOB NUMBER tit_ Zp,pp DATE
SAMPLE LOCATION ID LI, LOCATION ACTIVITY START: �� END: t3a�
WATER LEVEL / WELL DATA III
STICK-UP FT CASING/WELL DtFF.
WELL DEPTH F' I )HISTORICAL C ] TOP OF PROT. CASING (FROM GR(AINO ) FT
C3
n WELL MATERIAL: WELL LOCKED?: WELL DIA. C 12 INCH WATER LEVEL EQUIP.. USED:
WATER DEPTH I { I Q FT C I PVC [ I [ 7 YES I 3 4 INCH [ J ELECT.COND�PROBE
I I SS C) NO I I 6 INCH [ 3 FLOAT ACTIVATED
t ) C I PRESS. TRANSDUCER
C 7
.Tb GAL/'FT
t2
1Na
'SAC/VOL. ( 3
HEIGHT OF fT X I ]
m65 GAL/FT
(4
IN.) _
WELL INTEGRITY-:
YES
NO
WATER COLUMN C )
13 GAL/FT
(6
IN.)
- PROT. CASING SECURE
C ]
I }
I )
_GAL/FT
{�IN
J
L TOTAL GAPURGED CONCRETE COLLAR INTACT
I I
I J
OTHER
EOU]PMENT DOCUHENTAT ION
PURGI kG/SAMPLING EDUIP. USED:
,/
CF
USED FOR:
PURGING
SAMPLING
CI
CJ
STALTJC PUMP
SUBMERSIBLE PUMP
6AI LER
VVC/SILICON TUBING
TEFI.ON/SILICON TUBING
AIR LIFT
NAND PUMP
IN -LINE FILTER
PRESS/VAC FILTER
PERT
DECONTAMINATION FLUIDS USED:
EOUIIPMENT ID (J ALL THAT APPLY AT LbGAtI ON
t 7 ETHYL ALCOHOL
I ) DEIONIZED WATER
I ) TSP SOLUTION
I I HEXANE
I I HNOUD.I.WATER SOLUTION
C 7 POTABLE WATER
C I NONE
II
CI
FT ELD ANALYSIS DATA
AMBIENT AIR VDA PPM WELL MOUTH I PPM FIELD DATA COLLECTED I )iN-LINE '
1 3b f 2ri� �Z50 t ]IN CONTAINER
PURGE -DATA
S .GAL
0 .&�SAL
D �-�� GAL.
B Q,7 5.GAL
@ GAL
SAMPLE COLLECTION REOUIREMENFS
.
(•1 If REOUtRED AT TH[S LOCAT30H) J IF
•/ JF FIELD PRESERVATION VOLUME SAMPLE SAMPLE B0T71E ID �S
SAMPLE OBSERVATIONS: [ ] TURGID
I )
I ]
COLORED
CLOUDY
CLEAR
ODOR
C 7
C 7
ME
ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECITE D
13 1 �l6 I]
[ ] Toil
[7 [I J /
MOTES: (5

Civil & Environmental
Consultants, Inc.
PROJECT A A L r 1v��`11 JOB NUMBER „ . DATE
SAMPLE LOCATION ID /1'1W I .� LOCATION ACTIVITY ST END: 123�
WATER LEVEL ! WELL DATA I ]MEASURED r 3 TOP OF WELL
WELL DEPTH I E ]HISTORICAL 13 TOP OF PRO% CASING C(FROM GRCUND)STICK�UP F7 CASINGlWELL DIFF. FT
�.1 WELL MATERIAL: WELL LOCKED?: WELL DIA- I 1 Z INCH WATER LEVEL EQUIP.. USED:
WATER DEPTH 1 F7 I ] PVC I 1 17 YES 13 4 INCH E 7 ELECT.COROiPROBE
17 SS I I NO I 3 6 INCH I] FLOAT ACTIVATED
I I I I PRESS. TRANSDUCER
{ 3 ,76 GAL/FT (2IN.) GAL/VOL' [ 3
HEIGHT OF FT X 13 .65 GAL/FT (4 IN.) _ WELL INTEGRITY: YES NO
WATER COLUMN 13 1<5 GAL/FT (6 IN.) PROT. CASING SECURE E I I 3
I ] iCAL/FT {_IH.) TOTAL GAL PURGED CONCRETE COLLAR INTACT _I 1 13
OTHER
EQUIPMENT DOCUMENTATION
./ IF USED FOR: DECONTAMINATION FLUIDS USED.
PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING EQUIPMENT ID (J ALL THAT APPLY AT LOCATION
13 I3 PERISTALTIC PUMP - I ] ETHYL ALCOHOL
E 7 11 SUBMERSIBLE PUMP I] DEIONIZED WATER
13 I I BAILER [ 7 TV SOLUTION
I ] 13 PVCISILICON TUBING I I HEXANE
_ 13 17 TEFLON/SILICON TUBING I 1 HNO3/D:I.1WATER SOLUTION
11 [ 3 AIR LIFT I I POTABLE WATER
17 I 1 HAND PUMP L 3 NONE
I ) IN -LINE FILTER L 3
I I PRESS/VAC FILTER [ 7
II II
FIELD ANALYSIS DATA
AMBIENT AIR VOA PPM WELL MOUTH PPM FIELD DATA COLLECTED I 3IR-LINE
1/ 1114*1 1 It44 I IIH CONTAINER
PURGE DATA
c� 0,0 GAL
iJ • 2� WL
Q 0.56 GAL
a Q_-7,5 GAL
IQ GAL
SAMPLE OBSERVATIONS.
l
{ 3
I 3 TURBID
L I COLORED
13 CLOMY
L CLEAR
ODOR
SAMPLE CDLLFCTIDN REQUIREMENTS (O�.?
(J IF REQUIRED AT THIS LOCATION) 4 IF
J IF FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE ID'S
ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED
I7 [] I ! I
I3ODD
II I3 ! !

�Y
r
/��" � ,.. mom;,
Civil &Environmental
Consultants, Inc. 7
PROJECT � /� � � -�� JL�1I JOB NUMBER � ,OQ DATE �/Ir/�
SAMPLE LOCAT 10N 1D /�lnJ-I",}-'1 � LOCATION ACTIVITY START: +S�vi. END: f�Ds
WATER LEVEL /WELL DATA � �7
WELL DEPTH FT I )HISTORICAL (; TOD OF PR07. GSING C(FROM GROUHD)P FT GS1NG/YELL Dlff. FT
WELL MATERIAL_• WELL LOCKED?: YELL DIA. [ 7 2 INCH WATER LEVEL EQUIP. USED:
WATER DEPTH �',; +-+'� FT [ 7 PYC [ 7 17 YES C) 4 INCH C 7 ELECT.LOND.PR08E
[) SS [) NO 17 6 JNCH O FLOAT ACTIVATED
[ 7 C ] PRESS. TRANSDUCER
17 .T6 WL/FT (2 1N.) WL/VOL [ )
HEIGHT OF FT X 2 7 .65 GAt/FT (4 IN.) = kELL INTEGRITY: YES NO
WATER COLUMN (7 1.5 WL/FT (b IH.) OROT. CASING SECURE C 7 C 7
C) _WUFT (_1NJ TOTAL Wl PURGED CONCRETE COLLAR IHTACi I) C )
OTHER
EOUI PMENT DOCUMENTATION
J If USED FOR: DECONTAMINATION FLUIDS USED:
PURGING/SAMPL LNG EDUIP. USED: PURGING SAMPLING EDUIPMENT 1D .{J All THAT APPLY AT LOWTION
I 7 [) PERISTALTIC PUMP f 7 ETHYL ALCOHOL
[ 7 C) SUBMERSIBLE P(RIP - !) DEIONI2ED PATER
O C 7 BAILER i 7 TSP SOLUTION
[ 7 [ I PVC/SILICON TUBING I) HEKANE
[ 7 C 7 TEFLON/SILICON TUBING L 7 NN03/D.1.YATER SOLUTION
C ] I S AIR LIFT 17 POTABLE WATER
L I C) HAND PUMP C ] NONE
C7 IN-IiNE FILTER I )
C) � PRESS/VAC FILTER ( 7
I7 C)
FIELD ANALYSIS DATA
ANB7 ENT AIR VOA PPM YELL MWTH PPM FIELD DATA COLLECTED L )IN -LINE
171N CONTAINER
PURGE DATA a I !/�! �-GA9 a � � nAi a a 1/;zL 6AL a �,, UA4 a WL SAMPLE OBSERVATIONS:
[) TURBID
i
i EMPERATURE, DEG C 1 �- � ��% � �-U�. i .� � /�' i _ L � �`I C 7 COLORED
pN, uni Ts �,_ S I ��47 t�.Y �! (O�� I) CLOUDY
SPECIFIC CONDUCTIVITY P'J CLEAR
(urhos/cm. a 25 tleg.q � G�j� I LrU (OLI ) DO G> [ ] WOR
OXIDAT 30N-REDUCTION,+/- my - ,3 S - �- '- I �� � ��— _ �1.a'—
DISSOlVEO OXYGEN, ppn /;. T.�i %. y-.a- h�t� ��..!-�
SAMPLE COLLECTION REOUIREHExTS
(J IF REDUI0.ED AT THIS LOCATION) J IF
J 1F FIELD PRESERVATION YOLLME SAMPLE SAMPLE BOTTLE ID'S
ANALYTIGL DARAMETER fIITERED METH00 REDUIRID COLLECTED
NDTES:
�j ,.,.apt "`-� �
�� ��t C 7
C7
[3
o,, 3-�" cA 0-o i ;
I b •�- p
/
/
/
/
/
/
/
/
/
/
/
/
/
/
/
/
/

r
r
1115 MZIM/ I
Civil & Environmental
Consultants, Inc.
PROJECT jai �n L 1" — j (� JOB NUMBER ( DATE
SAMPLE LOCATION ID �i W - j a '� LOCATION ACTIVITY START: Z S 5 END:
WATER LEVEL /YELL DATA
I )MEASURED C ) TOP OF WELL CASING STICKUP FT CASING/YELL DIFF. FT
WELL DEPIN FT ( ]HISTORICAL [ ) TOP OF PRO% CASING (FROM GROUND)
[J
WELL MATERIAL: WELL LOCKED]: WELL DIA. [ J 2 INCH WATER LEVEL EQUIP. USED:
PATER DEPTH ( 1 FT [ J PVC [ 7 [ I YES 1 3 4 INCH I ] ELECT.COND.PROSE
f 7 SS [ I NO 2 7 6 INCH [ 7 FLOAT ACTIVATED
I J C 3 PRESS. TRANSDUCER
C 3 .16 GAL/FT (2 IN J GAL/VOL [ 3
HEIGHT OF FT X L 7 .65 GAL/FT (4 IX.) = WELL INTEGRITY: YES NO
WATER COLUMN 1 3 1.5 GAL/FT (6 IN.) PROT. CASING SECURE C 3 C 3
C 3 GAL/FT (_INJ TOTAL GAL PURGED CONCRETE COLLAR INTACT C I 17
OTHER
EQUIPMENT DOCUMENTATION
,1 IF USED FOR: DECONTAMINATION FLUIDS USED:
PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING EQUIPMENT ID U ALL THAT APPLY AT LOCATION
I I [ 7 PERISTALTIC PUMP 1 3 ETHYL ALCOHOL
1 3 C 1 SUBMERSIBLE PUMP ( 1 DEIONIZED WATER
I] C 3 BAILER 11 TSP SOLUTION
C 3 1 3 PVC/SILICON TUBING 11 HEXANE
I 1 ( 3 TEFLON/SILICON TUBING ( 3 HNO3/D.I.WATER SOLUTION
C J ( 3 AIR LIFT [ I POTABLE WATER
1 3 I 1 HAND PUMP 13 NONE
C 3 IN -LINE FILTER 1 3
[ J PRESS/VAC FILTER I I
[7 I]
FIELD ANALYSIS DATA
AMBIENT AIR VOA PPM WELL MOUTH PPN FIELD DATA COLLECTED C 11N-LINE '
I )IN CONTAINER
PURGE DATA
o�'%`-! l GFt
SAMPLE OBSERVATIONS:
TEMPERATURE, DEC C
C 3 COLORED
PH, units
—I.3 a
..1-7_�.
'7.255
S
C 7 CLOUDY
SPECIFIC CONDUCTIVITY
�S'7
Q-�3
Y
�[�7
S-3
CLEAR
(untios/cm. a 25 de6•c)
C O
C 1 DOOR
OXIDATIONDISSOLVED REDUCTION,+/- my
DISSOLVED OXYGEN, ppm
'7 io
S'_ '7 `i
5- �—
5 _7 Cu
SAMPLE COLLECTION REQUIREMENTS
(J IF REQUIRED AT THIS LOCATION)
J IF FIELD
ANALYTICAL PARAMETER FILTERED
I IF
PRESERVATION VOLlR1E SAMPLE SAMPLE BOTTLE ID'S
METHCQ REWIRID COLLECTED
I]of
vau
[ 7 DUD CO2 10 b ;
(]
C7 I3
NOTES: . 'Yj�.7 0/0
li U-15 w 5
("�7 ;o3 iit3 iil

PROJECT JKA L IV I L JOB NUMBER f —•3�- I DATE
SAMPLE LOCATION ID LOCATION ACTIVITY ✓START: END:
WATER LEVEL
[�/ WELLDATA
CASINO
''F-7� WELL DEPTH{ —J I ]HISTORICAL I ) TOP OF P OT. MING (FROIJ GROUNU]P FT CASING/6JEL1 DIFF..
L WELL MATERIAL: WELL LOCKED?: WELL DIA. I 1 2 INCH WATER LEVEL EQUIP.. USED:
WATER DEPTH /1 ,(�'O F7 17 PVC T J C 7 Y£5 I ] 4 INCH [ 3 ELECT.CONDPROBE
_I 17 SS 17 NO 1) 6 INCH [ 7 FLOAT ACTIVATED
t 7 I l PRESS. TRANSDUCER
17 .16 GAL/FT (2 IN:) GAL/VOL I I _
HEIGHT OF FTI X I 1 .65 GAL/FT (4 IN.) _ WELL INTEGRITY: YES NO
WATER, COLUMN 17 1.5 GAL/FT (6 IN.) PROT. CASING SECURE I 1 17
17 _GAL/FT tv.]N.> TOTAL GAL PURGED CONCRETE COLLAR INTACT 17 [ )
OTHER
EQUIPMENT DOCUMENTATION
,/ IF USED FOR: DECONTAMINATION FLUIDS USED."
PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING EOUIIPMENT ID (J ALL THAT APPLY AT LOCATION
17 I7 PERISTALTIC PUMP 17 ETHYL ALCOHOL
I I 17 SUBMERSIBLE PUMP 17 DEIONIZED 'WATER
1 3 I 3 DAI LER 17 TSP SOLUTION
I] 1 3 PVC/SILICON TUBING I l HEXANE
I) C l TEFLON/SILICON TUBING 1 3 HNO3/P.I.WATER SOLUTION
E 3 13 AIR LIFT 1 3 POTABLE WATER
[ 1 I 7 .NAND PUMP 1 3 NONE
1 3 IN -LINE FILTER 1 7
1 7 PRESS/VAC FILTER [ 3
t) I7
FIELD ANALYSIS DATA
AMBIENT AIR VOA PPM VEL�.MOU H - PPM FIELD DATA COLLECTED 131R-LINE '
7'V,00 .3 oN NTAINER
D 65 GAL D GALJQ .4 S GAL 2 GAL 0 Z -2 GAL SAMPLE OBSERVATIiNS:
PURGEDATA
TEMPERATURE, DEG C
Whits
SPECIFIC
SPECS FiC CONDUCTIVITY
OXIDATIONREDUCTION,*!'
DISSOLVED OXYGEN, ppm
. Z
. (do
a., S'fl
b
I
{
2
O•
9d
fJ, 2Z
SAMPLE COLLECTION REQUIREMENTS '
CJ IF REQUIREq AT TH15 LOCATION) � If
.1 If FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE IDtS
ANALYTICAL PARAMETER FILTERED METHOD ' REQUIRED COLLECTED
I I {-tYI
I I
II u V O "
13
1 1 b v0� E I
ROTES: =
eve qq

Civil & Environmental
Consultants, Inc.
PROJECT I N,tjc.7_ j,,,,. ,;tj -
SAMPLE LOCATION ID xA toQ . I q C_
JOB NUMBER ��l-3Z �•O� PATE^1 a�,1 6•—.,
LOCATION ACTIVITY START: t'$ Ijr) END:
WATER LEVEL / WELL DATA
t IMEASURED 13 TOP OF WELL CASING STICK-UP FT CASINGIWELL DIFF. FT
WELL DEPTH I IHISTORfCAL 13 TOP OF PROT_ CASING [FROM GROUND]
C3
WELL
MATERIAL:
WELL
LOCKED?: WELL DIA. I 1
2
INCH
WATER LEVEL EQUIP_. USED:
WATER DEPTH
(. t-' .'I�F7
17
PVC
I I
17
YES 13
4
INCH
17 ELECT.COND:PROBE
[ 7
SS
I I
NO [ 1
6
INCH
17 FLOAT ACTIVATED
[ 7
[ 3 PRESS. TRANSDUCER
C 7
.16
GAL/FT
(2
IN,)
HEIGHT OF
fT
X [ I
.65
GALIFT
(4
IN.) _
WELL
INTEGRITY: YES NO
WATER COLUMN
13
7.5
GALIFT
(6
IN.)
EEGAL/VOL
PROT.
CASING SECURE [ 3 I 3
13
(�IN.)
TOTAL GAL PURGED
CONCRETE
COLLAR INTACT C 7 I I
_GAL/FT
OTHER
EOUI PMEH7 DOCUMENTATION
PURGINGI5AMPLING EQUIP. USED:
DECONTAMINATION FWIDS USED:
EOUIIPMEMT ID tJ ALL THAT APPLY R7 LOW IDN
1 J ETHYL ALCOHOL
C 7 DEIONIZE0 'WATER
C 7 TSP SOLUTION
I I HEXANE
[ I HNO3/0:I.WATER SOLUTION
[ ] POTABLE WATER
[ ] NONE
I]
FIELD ANALYSIS DATA
AMBIENT AIR VDA PPM WELL MOUTH PPM FIELD DATA COLLECTED I nN.-LINE
13cse 1344 � /"^]C .4ii.11N CONTAINER
PURGE DATA
,�
IF
USED 'FOR:
PURGING
SAMPLING
[)
27
[7
tl
C7
L7
[3
I7
I7
[3
I]
13
[7
[7
fI
(I�
PERkSTALTIC PUMP
SU8MER5IBLf PUMP
BAILER
PVC/SILICON TUBING
TEFLONJSILICON TUBING
AiR LIFT
NAND PUHP
IN -LINE FILTER
PRESS/VAC FILTER
a /%.(% GAt
f,RL
Q rs.S oGAL.
a cry{ .GAL
is �. Q�QGRL
SAMPLE COLLECTION REQUIREMENTS
IJ IK REQUIRED AT THIS LOCATION) 4 IF
J 1; FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE ID'S
ANALYTICAL PARAMETER FILTERED METHOD - REQUIRED COLLECTED
II II
[T [J
MW 17
t] [I
^pn []
NOTES:
SAMPLE OBSERVATIONS:
[ ]

Consultants, Inc.
PROJECT .i N�i� J013 NUMBER III- DATE /I
I lie
SAMPLE LOCATION ID m w _ Irj ; LOCATION ACTIVITY START: END:
WATER LEVEL /WELL DATA
I )MEASURED I ) TOP OF DELL CASING STICK-UP FT CASINGIWELL DIFF. FT
WELL DEPTH I )HISTORICAL I ) TAP OF PROT. CASING {FROM GRO(]ND)
IJ
WELL MATERIAL: WELL LOCKED?: WELL DIA. C 1 2 INCH WATER LEVEL EQUIP.. USED:
WATER DEPTH ��FT 11 PVC C J 11 YES 11 4 INCH C 7 ELECT.COND.PROHE
11 SS I) NO E 7 6 INCH 11 FLOAT ACTIVATED
C 1 I ) PRESS,. TRANSDUCER
1 ) ,16 GAL/FT (2 114.) SAL/VOL' I 1
HEIGHT OF FT X 1 ) .65 GAL/FT (4 IN.) _ WELL INTEGRITY. YES NO
WATER COLUMN I) 1.5 GAL/FT (6 IN.) PROT. CASING SECURE I I I )
I 1 ,_GAL/FT (,IN*) TOTAL GAL PURGED CONCRETE COLLAR INTACT I I 17
OTHER
EQUIPMENT DOCUHENiAT ION
J iP
PURGE DATA
USED FOR:
DECONTAHi NATION FLUIDS USEb:
PURGING/SAMPLING £QUIP. USEb: PURGING
SAHPLIHG
EQUIPMENT
ID (J ALL THAT APPLY AT LOCATION
I 1
I)
PERISTALTIC PUMP
I 1 ETHYL ALCOHOL
' C I
C)
SUBMERSIBLE PUMP
C 7 DEIOk12Ep WATER
C)
11
BAILER
I I TSP SOLUTION
I 1
1 1
PVC/SILICON TUBING
17 HEXANE
C )
17
TEFI.ON/SILICON-TUBING
17 HNO3/P:l*WATER SOLUTION
_
11
11
AIR LIFT.
11 PDTIABLE WATER
I I
11
.NAND PUMP
E 1 NONE
I 1
IN -LINE FILTER
I 1
17
PRESS/VAC FILTER
I 1
I7
[]
FIELD ANALYSIS DATA
AMBIENT AIR VDAl
PPMJ
WELL MOUTH PPM FIELD
DATA COLLECTED IICN-LINE '
O Oa•111J
09%!;TITINCONTAINER 0�1;sS1
i'1 Q•S At.
a _L�{.AL
a _GAL.
a }Z GAL
a � GAL
TEMPERATURE, DEC D
PH, units
SPECIFIC CONDUCTIVITY
(uiu)os/cm..2 25 des.e)
DISSOLVED OXYGENION,+(-
DISSOLVED OXYGEN, PPm
,�:�
5.. 12
I•T'.Z
h 9 h
4a-•S
I10•S
.Ij�,
L
_—
(' 11 _
.�C
46(0
���
�_
�"�
-'�'�"�
A�rr�I
m
-SAMPLE COLLECTION REQUIREMENTS
{J IF REQUIRED AT THIS LOCATION) �/ If
4 IF FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE ID'S
ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED
11 h�gh�e5} 6aShenoi�v,�
tI
C1Cfl
I
I3
I 1 OL
NOTES:
3
SAMPLE OSS
[ 1 TURBID
17 LOLORE
[ 7 CLOUDY
L 7 CLEAR
[ J ODOR
,tiin1 01 ' S'5

Civil &Environmental
Consultants, Inc.
PROJECT I A)/✓ LF� S vx l9
SAMPLE LOCATION ID l 1. ® , r r0 L.I >_I
LATER LEVEL / WELL DATA
WELL DEPTH
LATER DEPTH 0�0�.'3J F
LATER COLUMN
H£IGN7 OF FT
EQUIPMENT DOCUMENTATION
JOB NUMBER I DATE Ll l IX.
LOCATION ACTIVITY START: ®On� END: I Ci tt
7 MEASURED 13
TOP OF
WELL
CASING ST.I CK-UP
FT
LASING/CELL DIFF.
fT
I HISTORICAL [
3
TOP OF
PROT. CASING (FROM GROUND)
C3
WELL MATERIAL:
WELL
LOCKED?. WELL DIA. [ 3
2
INCH LATER LEVEL EQUIP... USED:
I I PVC I J
[ 3
YES 1 3
4
INCH [ 3 ELECT.COND.PROBE
I I SS
13
NO 13
6
INCH [ ] FLOAT ACTIVATED
[ 3
[ I PRESS. TRANSDUCER
13 ,16 GAL/FT
(2
1N.)
GAL/VOL
- 13
X I I .65 GAL/FT
(4
IN.) _
-
CELL INTEGRITY: YES NO
13 1.5 GAL/FT
(6
IN.)
PROT. CASING SECURE C 3 1 3
-
[ 3 ,GAL/FT
(_IN.
AL PURGED
CONCRETE COLLAR INTACT C ] [ 3
OTHER
J
IF
USED FOR:
DECONTAMINATION FLUIDS USED:
PURGING/SAMPI7 NG EQUIP. USED: PURGING
SAMPLING
EQUIPMENT ID
(v ALLIX APPLY AT LOCATION
I
I
IA
PERISTALTIC PUMP
13 ETHYL ALCOHOL
13
I 3
SUBMERSIBLE PUMP
I I DEIDRIZED STATER
I
I
I ➢
BAILER
I ] TSP SOLUTION
I
I
13
PVC/SILTCON TUBING
I ] HEXANE
1
3
1 3
TEFLON/SILICON TUBING
I] HNO3/D:I.LATER SOLUTION
13
I 3
AIR LIFT
13 POTABLE LATER
C
3
1 3
HAND PUMP
[ 3 NONE
I r
IN -LINE FILTER
t 7
1 3
PRESS/VAC FILTER
C r
I7 I]
FIELD ANALYSIS DATA
AMBIENT AIR VOA PPM WELL MOUTH PPM FIELD DATA COLLECTED 131N-LINE
t9Qmggh reQV S 0705v MQ CONTAINER
GAL SAMPLE
PURGE DATA
a D,f7 GAL
GAL
Q P< Q GAL.
aD I •Z6CGAL
D
/ir7/A: Iq,rj$� 9(0.l03 2$.3a 3'S.YZ 1`i5.2.
AMPLE COLLECTION REQUIREMENTS
(I IF REQUIRED AT THIS LOCATION) 1 4 IF
J If FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE IDtS
ANALYTICAL PARAMETER_ _ 6TLTERED METHOD REQUIRED COLLECTED
SAMPLE OBSERVATIONS:
L }
TURBSD
I3
COLORED
T�7
CLOUDY
L 7
CLEAR
I }
ODOR
t 3 � G,lfo (n•li r / / /
t]_tr St t3
NOTES. (. 6 � �•l/ j'V�\ VI ���1 III/niI
Yam(/

APPENDIX B
Civil & Environmental Consultants, Inc.

TestAmerica °
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Chicago
2417 Bond Street
University Park, IL 60484
Tel: [phone]
TestAmerica Job ID: 500-143859-1
TestAmerica SDG: NCDEQ Solid Waste Facility = # 60-13
Client Project/Site: NC North Mecklenburg Landfill -Infill SW
ror:
Civil & Environmental Consultants Inc
1900 Center Park Drive
Suite A
Charlotte, North Carolina 28217
Attn: Matt Ginther
A6%�/V 6W
Authorized for release by:
71512018 9:01:24 AM
Robin Kintz, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143859-1 F
Project/Site: NC North Mecklenburg Landfill -Infill SW SDG: NCDEQ Solid Waste Facility = # 60-13
Table of Contents
CoverPage ..............................................
1
Table of Contents .........................................
2
Case Narrative ...........................................
3 L
Detection Summary ........................................
4
Method Summary .........................................
5
Sample Summary .........................................
6
Client Sample Results ......................................
7
E:
Definitions ...............................................
21
QC Association ...........................................
22 F
Surrogate Summary .......................................
23
QC Sample Results ........................................
24
Chronicle................................................
29
Certification Summary ......................................
31
Chain of Custody ..........................................
32
E:
Receipt Checklists .........................................
34
TestAmerica Chicago
Page 2 of 34 7/5/2018

Case Narrative
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143859-1
Project/Site: NC North Mecklenburg Landfill -Infill SW SDG: NCDEQ Solid Waste Facility = # 60-13
Job ID: 500-143859-1
Laboratory: TestAmerica Chicago
Narrative
Job Narrative
500-143859-1
Comments
No additional comments.
Receipt
The samples were received on 4/14/2018 12:55 PM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was 3.31 C.
Receipt Exceptions
A trip blank was submitted for analysis with these samples; however, it was not listed on the Chain of Custody (COC). Added to COC and
logged in.
GC/MS VOA
Method(s) 503OB: The laboratory control sample (LCS) for 428305 recovered outside control limits for the following analyte: Acetone. This
analyte was biased high in the LCS and was not detected in the associated samples; therefore, the data has been reported.
Method(s) 8260B: The following samples detected Acetone: SW-1 (500-143859-3) and SW-4 (500-143859-6). The method blank
associated with the sample did not detect Acetone. Since Acetone is a known lab contaminant and the results are below 3X the repoting
limit; the results have been flagged with a "cn" flag to denote the possible lab contamination.
Method(s) 8260B: The method blank for batch 428305 and the following associated samples contained Chloroform above the method
detection limit: SW-Inf (500-143859-1), SW-Eff (500-143859-2), SW-2 (500-143859-4), SW-3 (500-143859-5) and TB (500-143859-7).
This target analyte concentration was less than the reporting limit (RL); therefore, re -analysis of samples was not performed.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TestAmerica Chica o
Page 3 of 34 7/5/20T8

Detection Summary
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143859-1
Project/Site: NC North Mecklenburg Landfill -Infill
SW
SDG:
NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: SW-Inf
Lab Sample ID: 500-143859-1
Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D Method Prep Type
[Analyte
Chloroform 1.1
J B
2.0
1.0
0.37
ug/L
1 8260B Total/NA
Client Sample ID: SW-Eff
Lab Sample ID: 500-143859-2
Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D Method Prep Type
CAnalyte
Chloroform 1.0
J B
2.0
1.0
0.37
ug/L
1 8260B Total/NA
Client Sample ID: SW-1
Lab Sample ID: 500-143859-3
Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D Method Prep Type
CAnalyte
Acetone 6.1
cn
5.0
2.5
1.7
ug/L
1 8260B Total/NA
Client Sample ID: SW-2
Lab Sample ID: 500-143859-4
nalyte Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D Method Prep Type
CA
Chloroform 0.98
J B
2.0
1.0
0.37
ug/L
1 8260B Total/NA
Client Sample ID: SW-3
Lab Sample ID: 500-143859-5
CAnalyte Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D Method Prep Type
Chloroform 0.93
J B
2.0
1.0
0.37
ug/L
1 8260B Total/NA
Client Sample ID: SW-4
Lab Sample ID: 500-143859-6
Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D Method Prep Type
Cmalyte
Acetone 4.1
J cn
5.0
2.5
1.7
ug/L
1 8260B Total/NA
Client Sample ID: TB
Lab Sample ID: 500-143859-7
Analyte Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D Method Prep Type
Carbon disulfide 1.3
J
2.0
1.0
0.45
ug/L
1 8260B Total/NA
Chloroform 1.1
J B
2.0
1.0
0.37
ug/L
1 8260B Total/NA
This Detection Summary does not include radiochemical test results.
TestAmerica Chicago
Page 4 of 34 7/5/2018

Method Summary C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143859-1
Project/Site: NC North Mecklenburg Landfill -Infill SW SDG: NCDEQ Solid Waste Facility = # 60-13
Method Method Description Protocol Laboratory
8260B Volatile Organic Compounds (GC/MS) SW846 TAL CHI
5030B Purge and Trap SW846 TAL CHI
Protocol References:
SW846 ='Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
TestAmerica Chicago
Page 5 of 34 7/5/2018

Sample Summary
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143859-1
Project/Site: NC North
Mecklenburg Landfill -Infill SW
SDG:
NCDEQ Solid Waste Facility
= # 60-13
Lab Sample ID
Client Sample ID
Matrix
Collected
Received
500-143859-1
SW-Inf
Water
04/10/1811:00
04/14/1812:55
500-143859-2
SW-Eff
Water
04/10/1810:50
04/14/1812:55
500-143859-3
SW-1
Water
04/11/1814:50
04/14/1812:55
500-143859-4
SW-2
Water
04/10/1810:30
04/14/1812:55
500-143859-5
SW-3
Water
04/10/1810:40
04/14/18 1 2:55
500-143859-6
SW-4
Water
04/09/1811:30
04/14/1812:55
500-143859-7
TB
Water
04/09/18 00:00
04/14/18 12:55
TestAmerica Chicago
Page 6 of 34 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill -Infill SW
TestAmerica Job ID: 500-143859-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: SW-lnf Lab Sample ID: 500-143859-1
Date Collected: 04/10/18 11:00 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/18/18 15:21
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/18/18 15:21
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/18/18 15:21
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/18/18 15:21
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/18/18 15:21
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/18/18 15:21
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/18/18 15:21
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/18/18 15:21
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/18/18 15:21
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/18/18 15:21
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/18/18 15:21
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/18/18 15:21
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/18/18 15:21
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/18/18 15:21
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/18/18 15:21
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/18/18 15:21
1
Acetone
<1.7
5.0
2.5
1.7
ug/L
04/18/18 15:21
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/18/18 15:21
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/18/18 15:21
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/18/18 15:21
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/18/18 15:21
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/18/18 15:21
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/18/18 15:21
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/18/18 15:21
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/18/18 15:21
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/18/18 15:21
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/18/18 15:21
1
Chloroform
1.1 J B
2.0
1.0
0.37
ug/L
04/18/18 15:21
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/18/18 15:21
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/18/18 15:21
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/18/18 15:21
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/18/18 15:21
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/18/18 15:21
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/18/18 15:21
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/18/18 15:21
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/18/18 15:21
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/18/18 15:21
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/18/18 15:21
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/18/18 15:21
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/18/18 15:21
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/18/18 15:21
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/18/18 15:21
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/18/18 15:21
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/18/18 15:21
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/18/18 15:21
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/18/18 15:21
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/18/18 15:21
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/18/18 15:21
1
TestAmerica Chicago
Page 7 of 34 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143859-1
Project/Site: NC North Mecklenburg Landfill -Infill SW SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: SW-lnf Lab Sample ID: 500-143859-1
Date Collected: 04/10/18 11:00 Matrix: Water
Date Received: 04/14/18 12:55
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr) 109 75- 126 04118118 15:21 1
4-Bromofluorobenzene (Surr) 99 72 - 124 04118118 15:21 1
Dibromofluoromethane 100 75 - 120 04118118 15:21 1
Toluene-d8 (Surr) 102 75 - 120 04118118 15:21 1
TestAmerica Chicago
Page 8 of 34 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill -Infill SW
TestAmerica Job ID: 500-143859-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: SW-Eff Lab Sample ID: 500-143859-2
Date Collected: 04/10/18 10:50 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/18/18 15:48
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/18/18 15:48
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/18/18 15:48
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/18/18 15:48
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/18/18 15:48
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/18/18 15:48
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/18/18 15:48
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/18/18 15:48
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/18/18 15:48
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/18/18 15:48
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/18/18 15:48
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/18/18 15:48
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/18/18 15:48
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/18/18 15:48
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/18/18 15:48
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/18/18 15:48
1
Acetone
<1.7
5.0
2.5
1.7
ug/L
04/18/18 15:48
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/18/18 15:48
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/18/18 15:48
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/18/18 15:48
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/18/18 15:48
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/18/18 15:48
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/18/18 15:48
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/18/18 15:48
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/18/18 15:48
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/18/18 15:48
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/18/18 15:48
1
Chloroform
1.0 J B
2.0
1.0
0.37
ug/L
04/18/18 15:48
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/18/18 15:48
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/18/18 15:48
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/18/18 15:48
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/18/18 15:48
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/18/18 15:48
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/18/18 15:48
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/18/18 15:48
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/18/18 15:48
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/18/18 15:48
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/18/18 15:48
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/18/18 15:48
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/18/18 15:48
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/18/18 15:48
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/18/18 15:48
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/18/18 15:48
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/18/18 15:48
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/18/18 15:48
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/18/18 15:48
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/18/18 15:48
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/18/18 15:48
1
TestAmerica Chicago
Page 9 of 34 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143859-1
Project/Site: NC North Mecklenburg Landfill -Infill SW SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: SW-Eff Lab Sample ID: 500-143859-2
Date Collected: 04/10/18 10:50 Matrix: Water
Date Received: 04/14/18 12:55
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr) 106 75- 126 04118118 15:48 1
4-Bromofluorobenzene (Surr) 97 72- 124 04118118 15:48 1
Dibromofluoromethane 100 75 - 120 04118118 15:48 1
Toluene-d8 (Surr) 102 75 - 120 04118118 15:48 1
TestAmerica Chicago
Page 10 of 34 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill -Infill SW
TestAmerica Job ID: 500-143859-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: SW-1 Lab Sample ID: 500-143859-3
Date Collected: 04/11/18 14:50 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/20/18 00:25
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/20/18 00:25
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/20/18 00:25
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/20/18 00:25
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/20/18 00:25
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 00:25
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/20/18 00:25
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/20/18 00:25
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/20/18 00:25
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/20/18 00:25
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/20/18 00:25
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 00:25
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/20/18 00:25
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/20/18 00:25
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/20/18 00:25
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/20/18 00:25
1
Acetone
6.1 cn
5.0
2.5
1.7
ug/L
04/20/18 00:25
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/20/18 00:25
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/20/18 00:25
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 00:25
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/20/18 00:25
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/20/18 00:25
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/20/18 00:25
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/20/18 00:25
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/20/18 00:25
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 00:25
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/20/18 00:25
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/20/18 00:25
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/20/18 00:25
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/20/18 00:25
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/20/18 00:25
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/20/18 00:25
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/20/18 00:25
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/20/18 00:25
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/20/18 00:25
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/20/18 00:25
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 00:25
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/20/18 00:25
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/20/18 00:25
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/20/18 00:25
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/20/18 00:25
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/20/18 00:25
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/20/18 00:25
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/20/18 00:25
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 00:25
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/20/18 00:25
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/20/18 00:25
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/20/18 00:25
1
TestAmerica Chicago
Page 11 of 34 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143859-1
Project/Site: NC North Mecklenburg Landfill -Infill SW SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: SW-1 Lab Sample ID: 500-143859-3
Date Collected: 04/11/18 14:50 Matrix: Water
Date Received: 04/14/18 12:55
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr) 108 75- 126 04120118 00:25 1
4-Bromofluorobenzene (Surr) 93 72 - 124 04120118 00:25 1
Dibromofluoromethane 96 75 - 120 04120118 00:25 1
Toluene-d8 (Surr) 94 75 - 120 04120118 00:25 1
TestAmerica Chicago
Page 12 of 34 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill -Infill SW
TestAmerica Job ID: 500-143859-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: SW-2 Lab Sample ID: 500-143859-4
Date Collected: 04/10/18 10:30 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/18/18 16:40
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/18/18 16:40
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/18/18 16:40
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/18/18 16:40
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/18/18 16:40
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/18/18 16:40
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/18/18 16:40
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/18/18 16:40
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/18/18 16:40
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/18/18 16:40
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/18/18 16:40
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/18/18 16:40
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/18/18 16:40
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/18/18 16:40
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/18/18 16:40
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/18/18 16:40
1
Acetone
<1.7
5.0
2.5
1.7
ug/L
04/18/18 16:40
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/18/18 16:40
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/18/18 16:40
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/18/18 16:40
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/18/18 16:40
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/18/18 16:40
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/18/18 16:40
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/18/18 16:40
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/18/18 16:40
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/18/18 16:40
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/18/18 16:40
1
Chloroform
0.98 J B
2.0
1.0
0.37
ug/L
04/18/18 16:40
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/18/18 16:40
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/18/18 16:40
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/18/18 16:40
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/18/18 16:40
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/18/18 16:40
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/18/18 16:40
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/18/18 16:40
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/18/18 16:40
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/18/18 16:40
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/18/18 16:40
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/18/18 16:40
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/18/18 16:40
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/18/18 16:40
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/18/18 16:40
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/18/18 16:40
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/18/18 16:40
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/18/18 16:40
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/18/18 16:40
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/18/18 16:40
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/18/18 16:40
1
TestAmerica Chicago
Page 13 of 34 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143859-1
Project/Site: NC North Mecklenburg Landfill -Infill SW SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: SW-2 Lab Sample ID: 500-143859-4
Date Collected: 04/10/18 10:30 Matrix: Water
Date Received: 04/14/18 12:55
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr) 110 75- 126 04118118 16:40 1
4-Bromofluorobenzene (Surr) 99 72 - 124 04118118 16:40 1
Dibromofluoromethane 101 75 - 120 04118118 16:40 1
Toluene-d8 (Surr) 101 75 - 120 04118118 16:40 1
TestAmerica Chicago
Page 14 of 34 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill -Infill SW
TestAmerica Job ID: 500-143859-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: SW-3 Lab Sample ID: 500-143859-5
Date Collected: 04/10/18 10:40 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/18/18 17:07
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/18/18 17:07
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/18/18 17:07
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/18/18 17:07
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/18/18 17:07
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/18/18 17:07
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/18/18 17:07
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/18/18 17:07
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/18/18 17:07
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/18/18 17:07
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/18/18 17:07
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/18/18 17:07
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/18/18 17:07
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/18/18 17:07
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/18/18 17:07
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/18/18 17:07
1
Acetone
<1.7
5.0
2.5
1.7
ug/L
04/18/18 17:07
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/18/18 17:07
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/18/18 17:07
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/18/18 17:07
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/18/18 17:07
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/18/18 17:07
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/18/18 17:07
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/18/18 17:07
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/18/18 17:07
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/18/18 17:07
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/18/18 17:07
1
Chloroform
0.93 J B
2.0
1.0
0.37
ug/L
04/18/18 17:07
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/18/18 17:07
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/18/18 17:07
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/18/18 17:07
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/18/18 17:07
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/18/18 17:07
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/18/18 17:07
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/18/18 17:07
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/18/18 17:07
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/18/18 17:07
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/18/18 17:07
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/18/18 17:07
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/18/18 17:07
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/18/18 17:07
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/18/18 17:07
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/18/18 17:07
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/18/18 17:07
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/18/18 17:07
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/18/18 17:07
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/18/18 17:07
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/18/18 17:07
1
TestAmerica Chicago
Page 15 of 34 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143859-1
Project/Site: NC North Mecklenburg Landfill -Infill SW SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: SW-3 Lab Sample ID: 500-143859-5
Date Collected: 04/10/18 10:40 Matrix: Water
Date Received: 04/14/18 12:55
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr) 108 75- 126 04118118 17:07 1
4-Bromofluorobenzene (Surr) 97 72- 124 04118118 17:07 1
Dibromofluoromethane 102 75 - 120 04118118 17:07 1
Toluene-d8 (Surr) 103 75 - 120 04118118 17:07 1
TestAmerica Chicago
Page 16 of 34 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill -Infill SW
TestAmerica Job ID: 500-143859-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: SW-4 Lab Sample ID: 500-143859-6
Date Collected: 04/09/18 11:30 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/20/18 00:53
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/20/18 00:53
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/20/18 00:53
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/20/18 00:53
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/20/18 00:53
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 00:53
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/20/18 00:53
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/20/18 00:53
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/20/18 00:53
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/20/18 00:53
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/20/18 00:53
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 00:53
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/20/18 00:53
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/20/18 00:53
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/20/18 00:53
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/20/18 00:53
1
Acetone
4.1 J cn
5.0
2.5
1.7
ug/L
04/20/18 00:53
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/20/18 00:53
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/20/18 00:53
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 00:53
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/20/18 00:53
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/20/18 00:53
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/20/18 00:53
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/20/18 00:53
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/20/18 00:53
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 00:53
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/20/18 00:53
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/20/18 00:53
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/20/18 00:53
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/20/18 00:53
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/20/18 00:53
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/20/18 00:53
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/20/18 00:53
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/20/18 00:53
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/20/18 00:53
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/20/18 00:53
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 00:53
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/20/18 00:53
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/20/18 00:53
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/20/18 00:53
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/20/18 00:53
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/20/18 00:53
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/20/18 00:53
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/20/18 00:53
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 00:53
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/20/18 00:53
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/20/18 00:53
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/20/18 00:53
1
TestAmerica Chicago
Page 17 of 34 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143859-1
Project/Site: NC North Mecklenburg Landfill -Infill SW SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: SW-4 Lab Sample ID: 500-143859-6
Date Collected: 04/09/18 11:30 Matrix: Water
Date Received: 04/14/18 12:55
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr) 107 75- 126 04120118 00:53 1
4-Bromofluorobenzene (Surr) 93 72 - 124 04120118 00:53 1
Dibromofluoromethane 98 75 - 120 04120118 00:53 1
Toluene-d8 (Surr) 94 75 - 120 04120118 00:53 1
TestAmerica Chicago
Page 18 of 34 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill -Infill SW
TestAmerica Job ID: 500-143859-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: TB Lab Sample ID: 500-143859-7
Date Collected: 04/09/18 00:00 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/18/18 17:59
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/18/18 17:59
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/18/18 17:59
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/18/18 17:59
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/18/18 17:59
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/18/18 17:59
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/18/18 17:59
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/18/18 17:59
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/18/18 17:59
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/18/18 17:59
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/18/18 17:59
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/18/18 17:59
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/18/18 17:59
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/18/18 17:59
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/18/18 17:59
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/18/18 17:59
1
Acetone
<1.7
5.0
2.5
1.7
ug/L
04/18/18 17:59
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/18/18 17:59
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/18/18 17:59
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/18/18 17:59
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/18/18 17:59
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/18/18 17:59
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/18/18 17:59
1
Carbon disulfide
1.3 J
2.0
1.0
0.45
ug/L
04/18/18 17:59
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/18/18 17:59
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/18/18 17:59
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/18/18 17:59
1
Chloroform
1.1 J B
2.0
1.0
0.37
ug/L
04/18/18 17:59
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/18/18 17:59
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/18/18 17:59
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/18/18 17:59
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/18/18 17:59
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/18/18 17:59
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/18/18 17:59
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/18/18 17:59
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/18/18 17:59
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/18/18 17:59
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/18/18 17:59
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/18/18 17:59
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/18/18 17:59
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/18/18 17:59
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/18/18 17:59
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/18/18 17:59
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/18/18 17:59
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/18/18 17:59
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/18/18 17:59
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/18/18 17:59
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/18/18 17:59
1
TestAmerica Chicago
Page 19 of 34 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143859-1
Project/Site: NC North Mecklenburg Landfill -Infill SW SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: TB Lab Sample ID: 500-143859-7
Date Collected: 04/09/18 00:00 Matrix: Water
Date Received: 04/14/18 12:55
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr) 106 75- 126 04118118 17:59 1
4-Bromofluorobenzene (Surr) 96 72 - 124 04118118 17:59 1
Dibromofluoromethane 102 75 - 120 04118118 17:59 1
Toluene-d8 (Surr) 101 75 - 120 04118118 17:59 1
TestAmerica Chicago
Page 20 of 34 7/5/2018

Definitions/Glossary
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143859-1
Project/Site: NC North Mecklenburg Landfill -Infill SW SDG: NCDEQ Solid Waste Facility = # 60-13
Qualifiers
GC/MS VOA
Qualifier Qualifier Description
LCS or LCSD is outside acceptance limits.
B Compound was found in the blank and sample.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
cn Refer to Case Narrative for further detail
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
tt Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
0
TestAmerica Chicago
Page 21 of 34 7/5/2018

QC Association Summary C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143859-1
Project/Site: NC North Mecklenburg Landfill -Infill SW SDG: NCDEQ Solid Waste Facility = # 60-13
GC/MS VOA
Analysis Batch: 428305
Lab Sample ID
Client Sample ID
500-143859-1
SW-Inf
500-143859-2
SW-Eff
500-143859-4
SW-2
500-143859-5
SW-3
500-143859-7
TB
MB 500-428305/28
Method Blank
LCS 500-428305/26
Lab Control Sample
Analysis Batch: 428546
Lab Sample ID
Client Sample ID
500-143859-3
SW-1
500-143859-6
SW-4
MB 500-428546/30
Method Blank
LCS 500-428546/6
Lab Control Sample
Prep Type
Matrix
Method Prep Batch
Total/NA
Water
8260B
Total/NA
Water
8260B
Total/NA
Water
8260B
Total/NA
Water
8260B
Total/NA
Water
8260B
Total/NA
Water
8260B
Total/NA
Water
8260B
Prep Type
Matrix
Method Prep Batch
Total/NA
Water
8260B
Total/NA
Water
8260B
Total/NA
Water
8260B
Total/NA
Water
8260B
TestAmerica Chicago
Page 22 of 34 7/5/2018

Surrogate Summary
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143859-1
Project/Site: NC North Mecklenburg Landfill -Infill SW SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS)
Matrix: Water Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
DCA BFB DBFM TOL
Lab Sample ID Client Sample ID (75-126) (72-124) (75-120) (75-120)
500-143859-1 SW-Inf
109
99
100
102
500-143859-2 SW-Eff
106
97
100
102
500-143859-3 SW-1
108
93
96
94
500-143859-4 SW-2
110
99
101
101
500-143859-5 SW-3
108
97
102
103
500-143859-6 SW-4
107
93
98
94
500-143859-7 TB
106
96
102
101
LCS 500-428305/26 Lab Control Sample
99
97
94
105
LCS 500-428546/6 Lab Control Sample
103
90
93
95
MB 500-428305/28 Method Blank
102
98
99
103
m
MB 500-428546/30 Method Blank
100
92
91
96
Surrogate Legend
DCA = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
TestAmerica Chicago
Page 23 of 34 7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill -Infill SW
Method: 8260B - Volatile Organic Compounds (GC/MS)
Lab Sample ID: MB 500-428305/28
Matrix: Water
Analysis Batch: 428305
MB MB
Analyte
Result Qualifier
1,1,1,2-Tetrachloroethane
<0.46
1,1,1-Trichloroethane
<0.38
1,1,2,2-Tetrachloroethane
<0.40
1,1,2-Trichloroethane
<0.35
1,1-Dichloroethane
<0.41
1,1-Dichloroethene
<0.39
1,2,3-Trichloropropane
<0.41
1,2-Dibromo-3-Chloropropane
<2.0
1,2-Dibromoethane
<0.39
1,2-Dichlorobenzene
<0.33
1,2-Dichloroethane
<0.39
1,2-Dichloropropane
<0.43
1,4-Dichlorobenzene
<0.36
2-Butanone (MEK)
<2.1
2-Hexanone
<1.6
4-Methyl-2-pentanone (MIBK)
<2.2
Acetone
<1.7
Acrylonitrile
<4.5
Benzene
<0.15
Bromochloromethane
<0.43
Bromodichloromethane
<0.37
Bromoform
<0.48
Bromomethane
<0.80
Carbon disulfide
<0.45
Carbon tetrachloride
<0.38
Chlorobenzene
<0.39
Chloroethane
<0.51
Chloroform
1.01 J
Chloromethane
<0.32
cis-1,2-Dichloroethene
<0.41
cis-1,3-Dichloropropene
<0.42
Dibromochloromethane
<0.49
Dibromomethane
<0.27
Ethylbenzene
<0.18
lodomethane
<0.66
Methylene Chloride
<1.6
Styrene
<0.39
Tetrachloroethene
<0.37
Tetrahydrofuran
<1.9
Toluene
<0.15
trans- 1,2-Dichloroethene
<0.35
trans- 1,3-Dichloropropene
<0.36
trans- 1,4-Dichloro-2-butene
<1.2
Trichloroethene
<0.16
Trichlorofluoromethane
<0.43
Vinyl acetate
<0.91
Vinyl chloride
<0.20
Xylenes, Total
<0.22
TestAmerica Job ID: 500-143859-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: Method Blank
Prep Type: Total/NA
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1.0
0.50
0.46
ug/L
04/18/1811:49
1
1.0
0.50
0.38
ug/L
04/18/1811:49
1
1.0
0.50
0.40
ug/L
04/18/1811:49
1
1.0
0.50
0.35
ug/L
04/18/1811:49
1
1.0
0.50
0.41
ug/L
04/18/1811:49
1
1.0
0.50
0.39
ug/L
04/18/1811:49
1
1.0
0.50
0.41
ug/L
04/18/1811:49
1
5.0
2.5
2.0
ug/L
04/18/1811:49
1
1.0
0.50
0.39
ug/L
04/18/1811:49
1
1.0
0.50
0.33
ug/L
04/18/1811:49
1
1.0
0.50
0.39
ug/L
04/18/1811:49
1
1.0
0.50
0.43
ug/L
04/18/1811:49
1
1.0
0.50
0.36
ug/L
04/18/1811:49
1
5.0
2.5
2.1
ug/L
04/18/1811:49
1
5.0
2.5
1.6
ug/L
04/18/1811:49
1
5.0
2.5
2.2
ug/L
04/18/1811:49
1
5.0
2.5
1.7
ug/L
04/18/1811:49
1
20
10
4.5
ug/L
04/18/1811:49
1
0.50
0.25
0.15
ug/L
04/18/1811:49
1
1.0
0.50
0.43
ug/L
04/18/1811:49
1
1.0
0.50
0.37
ug/L
04/18/1811:49
1
1.0
0.50
0.48
ug/L
04/18/1811:49
1
2.0
1.0
0.80
ug/L
04/18/1811:49
1
2.0
1.0
0.45
ug/L
04/18/1811:49
1
1.0
0.50
0.38
ug/L
04/18/1811:49
1
1.0
0.50
0.39
ug/L
04/18/1811:49
1
1.0
0.51
0.51
ug/L
04/18/1811:49
1
2.0
1.0
0.37
ug/L
04/18/1811:49
1
1.0
0.50
0.32
ug/L
04/18/1811:49
1
1.0
0.50
0.41
ug/L
04/18/1811:49
1
1.0
0.50
0.42
ug/L
04/18/1811:49
1
1.0
0.50
0.49
ug/L
04/18/1811:49
1
1.0
0.50
0.27
ug/L
04/18/1811:49
1
0.50
0.25
0.18
ug/L
04/18/1811:49
1
2.5
1.2
0.66
ug/L
04/18/1811:49
1
5.0
2.5
1.6
ug/L
04/18/1811:49
1
1.0
0.50
0.39
ug/L
04/18/1811:49
1
1.0
0.50
0.37
ug/L
04/18/1811:49
1
10
5.0
1.9
ug/L
04/18/1811:49
1
0.50
0.25
0.15
ug/L
04/18/1811:49
1
1.0
0.50
0.35
ug/L
04/18/1811:49
1
1.0
0.50
0.36
ug/L
04/18/1811:49
1
5.0
5.0
1.2
ug/L
04/18/1811:49
1
0.50
0.25
0.16
ug/L
04/18/1811:49
1
1.0
0.50
0.43
ug/L
04/18/1811:49
1
2.0
1.0
0.91
ug/L
04/18/1811:49
1
1.0
0.50
0.20
ug/L
04/18/1811:49
1
1.0
0.50
0.22
ug/L
04/18/1811:49
1
Li
Page 24 of 34
TestAmerica Chicago
7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill -Infill SW
MB MB
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 102 75- 126
4-Bromofluorobenzene (Surr) 98 72 - 124
Dibromofluoromethane 99 75 - 120
Toluene-d8 (Surr) 103 75 - 120
Lab Sample ID: LCS 500-428305/26
Matrix: Water
Analysis Batch: 428305
Analyte
1,1,1,2-Tetrachloroethane
1,1,1-Trich loroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trich loroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,2,3-Trichloropropane
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
4-Methyl-2-pentanone (MIBK)
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Ethylbenzene
lodomethane
Methylene Chloride
Styrene
Tetrachloroethene
Tetrahydrofuran
Toluene
trans- 1,2-Dichloroethene
trans- 1,3-Dichloropropene
trans- 1,4-Dichloro-2-butene
Trichloroethene
Spike
LCS LCS
Added
Result Qualifier
50.0
49.0
50.0
49.2
50.0
45.8
50.0
49.7
50.0
48.5
50.0
46.4
50.0
45.0
50.0
46.8
50.0
46.5
50.0
48.4
50.0
49.9
50.0
48.1
50.0
48.3
50.0
67.0
50.0
61.3
50.0
60.3
50.0
72.0
500
562
50.0
46.8
50.0
44.4
50.0
47.4
50.0
50.8
50.0
47.1
50.0
46.7
50.0
50.8
50.0
48.6
50.0
49.0
50.0
47.3
50.0
63.4
50.0
45.6
50.0
50.2
50.0
51.7
50.0
45.5
50.0
49.0
50.0
47.1
50.0
45.2
50.0
48.6
50.0
52.5
100
122
50.0
50.7
50.0
47.7
50.0
50.1
50.0
52.3
50.0
49.7
TestAmerica Job ID: 500-143859-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Prepared Analyzed
Dil Fac
04118118 11:49
1
04118118 11:49
1
04118118 11:49
1
04118118 11:49
1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
%Rec.
Unit
D %Rec
Limits
ug/L
98
70-125
ug/L
98
70-125
ug/L
92
67-127
ug/L
99
70-122
ug/L
97
70-125
ug/L
93
67-122
ug/L
90
50-133
ug/L
94
56-123
ug/L
93
70-125
ug/L
97
70-125
ug/L
100
68-127
ug/L
96
67-130
ug/L
97
70-120
ug/L
134
53-141
ug/L
123
56-135
ug/L
121
56-133
ug/L
144
40-143
ug/L
112
67-140
ug/L
94
70-120
ug/L
89
65-122
ug/L
95
69-120
ug/L
102
56-132
ug/L
94
40-130
ug/L
93
66-120
ug/L
102
65-122
ug/L
97
70-120
ug/L
98
45-127
ug/L
95
70-120
ug/L
127
54 -147
ug/L
91
70-125
ug/L
100
64 -127
ug/L
103
68-125
ug/L
91
70-120
ug/L
98
70-120
ug/L
94
61-136
ug/L
90
69-125
ug/L
97
70-120
ug/L
105
70-128
ug/L
122
59-139
ug/L
101
70-125
ug/L
95
70-125
ug/L
100
62 -128
ug/L
105
60-130
ug/L
99
70-125
TestAmerica Chicago
Page 25 of 34 7/5/2018

QC Sample Results C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143859-1
Project/Site: NC North Mecklenburg Landfill -Infill SW SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 500-428305/26
Matrix: Water
Analysis Batch: 428305
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Analyte
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec.
Limits
Trichlorofluoromethane
50.0
50.1
ug/L
100
70 -126
Vinyl acetate
50.0
52.0
ug/L
104
43 -133
Vinyl chloride
50.0
49.7
ug/L
99
64 -126
Xylenes, Total
100
101
ug/L
101
70 -125
Surrogate
1,2-Dichloroethane-d4 (Surr)
4-Bromofluorobenzene (Surr)
Dibromofluoromethane
Toluene-d8 (Surr)
LCS LCS
%Recovery Qualifier
Limits
99
75-126
97
72-124
94
75 - 120
105
75-120
Lab Sample ID: MB 500-428546/30
Matrix: Water
Analysis Batch: 428546
MB MB
Analyte
Result Qualifier
1,1,1,2-Tetrachloroethane
<0.46
1,1,1-Trichloroethane
<0.38
1,1,2,2-Tetrachloroethane
<0.40
1,1,2-Trichloroethane
<0.35
1,1-Dichloroethane
<0.41
1,1-Dichloroethene
<0.39
1,2,3-Trichloropropane
<0.41
1,2-Dibromo-3-Chloropropane
<2.0
1,2-Dibromoethane
<0.39
1,2-Dichlorobenzene
<0.33
1,2-Dichloroethane
<0.39
1,2-Dichloropropane
<0.43
1,4-Dichlorobenzene
<0.36
2-Butanone (MEK)
<2.1
2-Hexanone
<1.6
4-Methyl-2-pentanone (MIBK)
<2.2
Acetone
<1.7
Acrylonitrile
<4.5
Benzene
<0.15
Bromochloromethane
<0.43
Bromodichloromethane
<0.37
Bromoform
<0.48
Bromomethane
<0.80
Carbon disulfide
<0.45
Carbon tetrachloride
<0.38
Chlorobenzene
<0.39
Chloroethane
<0.51
Chloroform
<0.37
Chloromethane
<0.32
cis-1,2-Dichloroethene
<0.41
cis-1,3-Dichloropropene
<0.42
Dibromochloromethane
<0.49
Client Sample ID: Method Blank m
Prep Type: Total/NA
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1.0
0.50
0.46
ug/L
04/19/1817:30
1
1.0
0.50
0.38
ug/L
04/19/1817:30
1
1.0
0.50
0.40
ug/L
04/19/1817:30
1
1.0
0.50
0.35
ug/L
04/19/1817:30
1
1.0
0.50
0.41
ug/L
04/19/1817:30
1
1.0
0.50
0.39
ug/L
04/19/1817:30
1
1.0
0.50
0.41
ug/L
04/19/1817:30
1
5.0
2.5
2.0
ug/L
04/19/1817:30
1
1.0
0.50
0.39
ug/L
04/19/1817:30
1
1.0
0.50
0.33
ug/L
04/19/1817:30
1
1.0
0.50
0.39
ug/L
04/19/1817:30
1
1.0
0.50
0.43
ug/L
04/19/1817:30
1
1.0
0.50
0.36
ug/L
04/19/1817:30
1
5.0
2.5
2.1
ug/L
04/19/1817:30
1
5.0
2.5
1.6
ug/L
04/19/1817:30
1
5.0
2.5
2.2
ug/L
04/19/1817:30
1
5.0
2.5
1.7
ug/L
04/19/1817:30
1
20
10
4.5
ug/L
04/19/1817:30
1
0.50
0.25
0.15
ug/L
04/19/1817:30
1
1.0
0.50
0.43
ug/L
04/19/1817:30
1
1.0
0.50
0.37
ug/L
04/19/1817:30
1
1.0
0.50
0.48
ug/L
04/19/1817:30
1
2.0
1.0
0.80
ug/L
04/19/1817:30
1
2.0
1.0
0.45
ug/L
04/19/1817:30
1
1.0
0.50
0.38
ug/L
04/19/1817:30
1
1.0
0.50
0.39
ug/L
04/19/1817:30
1
1.0
0.51
0.51
ug/L
04/19/1817:30
1
2.0
1.0
0.37
ug/L
04/19/1817:30
1
1.0
0.50
0.32
ug/L
04/19/1817:30
1
1.0
0.50
0.41
ug/L
04/19/1817:30
1
1.0
0.50
0.42
ug/L
04/19/1817:30
1
1.0
0.50
0.49
ug/L
04/19/1817:30
1
Page 26 of 34
TestAmerica Chicago
7/5/2018

QC Sample Results C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143859-1
Project/Site: NC North Mecklenburg Landfill -Infill SW SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 500-428546/30
Matrix: Water
Analysis Batch: 428546
MB MB
Analyte Result Qualifier RL LOD MDL
Client Sample ID: Method Blank
Prep Type: Total/NA
Unit D Analyzed Dil Fac
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/19/18 17:30
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/19/18 17:30
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/19/18 17:30
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/19/18 17:30
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/19/18 17:30
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/19/18 17:30
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/19/18 17:30
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/19/18 17:30
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/19/18 17:30
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/19/18 17:30
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/19/18 17:30
1 m
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/19/18 17:30
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/19/18 17:30
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/19/18 17:30
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/19/18 17:30
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/19/18 17:30
1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
100
75- 126
04119118 17:30
1
4-Bromofluorobenzene (Surr)
92
72 - 124
04119118 17:30
1
Dibromofluoromethane
91
75 - 120
04119118 17:30
1
Toluene-d8 (Surr)
96
75 - 120
04119118 17:30
1
Lab Sample ID: LCS 500-428546/6
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428546
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D
%Rec
Limits
1,1,1,2-Tetrachloroethane
50.0
49.7
ug/L
99
70-125
1,1,1-Trichloroethane
50.0
46.1
ug/L
92
70-125
1,1,2,2-Tetrachloroethane
50.0
46.5
ug/L
93
67-127
1,1,2-Trichloroethane
50.0
49.3
ug/L
99
70-122
1,1-Dichloroethane
50.0
49.6
ug/L
99
70-125
1,1-Dichloroethene
50.0
42.4
ug/L
85
67-122
1,2,3-Trichloropropane
50.0
46.7
ug/L
93
50-133
1,2-Dibromo-3-Chloropropane
50.0
49.6
ug/L
99
56-123
1,2-Dibromoethane
50.0
48.5
ug/L
97
70-125
1,2-Dichlorobenzene
50.0
47.5
ug/L
95
70 -125
1,2-Dichloroethane
50.0
53.7
ug/L
107
68 -127
1,2-Dichloropropane
50.0
51.5
ug/L
103
67 -130
1,4-Dichlorobenzene
50.0
46.2
ug/L
92
70 -120
2-Butanone (MEK)
50.0
58.6
ug/L
117
53 -141
2-Hexanone
50.0
53.0
ug/L
106
56 -135
4-Methyl-2-pentanone (MIBK)
50.0
54.4
ug/L
109
56-133
Acetone
50.0
51.4
ug/L
103
40 -143
Acrylonitrile
500
626
ug/L
125
67 -140
Benzene
50.0
46.8
ug/L
94
70-120
Bromochloromethane
50.0
48.6
ug/L
97
65 -122
TestAmerica Chicago
Page 27 of 34 7/5/2018

QC Sample Results C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143859-1
Project/Site: NC North Mecklenburg Landfill -Infill SW SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 500-428546/6
Matrix: Water
Analysis Batch: 428546
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Bromodichloromethane
50.0
50.9
ug/L
102
69 -120
Bromoform
50.0
56.7
ug/L
113
56 -132
Bromomethane
50.0
37.0
ug/L
74
40 -130
Carbon disulfide
50.0
44.1
ug/L
88
66 -120
Carbon tetrachloride
50.0
49.1
ug/L
98
65 -122
Chlorobenzene
50.0
48.9
ug/L
98
70 -120
Chloroethane
50.0
45.8
ug/L
92
45 -127
Chloroform
50.0
48.2
ug/L
96
70 -120
Chloromethane
50.0
59.2
ug/L
118
54 -147
cis-1,2-Dichloroethene
50.0
45.7
ug/L
91
70 -125
cis-1,3-Dichloropropene
50.0
48.5
ug/L
97
64 -127
Dibromochloromethane
50.0
53.9
ug/L
108
68 -125
Dibromomethane
50.0
48.5
ug/L
97
70 -120
Ethylbenzene
50.0
48.7
ug/L
97
70 -120
lodomethane
50.0
43.4
ug/L
87
61 -136
Methylene Chloride
50.0
45.4
ug/L
91
69 -125
Styrene
50.0
50.4
ug/L
101
70 -120
Tetrachloroethene
50.0
49.7
ug/L
99
70 -128
Tetrahydrofuran
100
104
ug/L
104
59 -139
Toluene
50.0
48.8
ug/L
98
70 -125
trans- 1,2-Dichloroethene
50.0
44.8
ug/L
90
70-125
trans- 1,3-Dichloropropene
50.0
48.0
ug/L
96
62.128
trans- 1,4-Dichloro-2-butene
50.0
59.4
ug/L
119
60-130
Trichloroethene
50.0
48.2
ug/L
96
70 -125
Trichlorofluoromethane
50.0
48.5
ug/L
97
70 -126
Vinyl acetate
50.0
49.4
ug/L
99
43 -133
Vinyl chloride
50.0
51.5
ug/L
103
64 -126
Xylenes, Total
100
95.2
ug/L
95
70 -125
LCS LCS
Surrogate
%Recovery Qualifier
Limits
1,2-Dichloroethene-d4 (Surr)
103
75- 126
4-Bromofluorobenzene (Surr)
90
72 - 124
Dibromofluoromethane
93
75- 120
Toluene-d8 (Surr)
95
75 - 120
TestAmerica Chicago
Page 28 of 34 7/5/2018

Lab Chronicle
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill -Infill SW
TestAmerica Job ID: 500-143859-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: SW-lnf
Lab Sample ID: 500-143859-1
Date Collected: 04/10/18 11:00
Matrix: Water
Date Received: 04/14/18 12:55
Batch Batch
Dilution Batch Prepared
Prep Type Type Method
Run Factor Number or Analyzed Analyst Lab
Total/NA Analysis 8260B
1 428305 04/18/18 15:21 JDD TAL CHI
Client Sample ID: SW-Eff Lab Sample ID: 500-143859-2
Date Collected: 04/10/18 10:50 Matrix: Water
Date Received: 04/14/18 12:55
Batch Batch Dilution Batch Prepared
Prep Type Type Method Run Factor Number or Analyzed Analyst Lab E:
Total/NA Analysis 8260B 1 428305 04/18/18 15:48 JDD TAL CHI
Client Sample ID: SW-1
Lab Sample ID: 500-143859-3
Date Collected: 04/11/18 14:50
Matrix: Water
Date Received: 04/14/18 12:55
Is
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method
Run
Factor
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
428546
04/20/18 00:25
JJH TAL CHI
Client Sample ID: SW-2
Lab Sample ID: 500-143859-4
Date Collected: 04/10/18 10:30
Matrix: Water
Date Received: 04/14/18 12:55
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method
Run
Factor
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
428305
04/18/18 16:40
JDD TAL CHI
Client Sample ID: SW-3
Lab Sample ID: 500-143859-5
Date Collected: 04/10/18 10:40
Matrix: Water
Date Received: 04/14/18 12:55
F Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method
Run
Factor
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
428305
04/18/18 17:07
JDD TAL CHI
Client Sample ID: SW-4
Lab Sample ID: 500-143859-6
Date Collected: 04/09/18 11:30
Matrix: Water
Date Received: 04/14/18 12:55
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method
Run
Factor
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
428546
04/20/18 00:53
JJH TAL CHI
TestAmerica Chicago
Page 29 of 34 7/5/2018

Lab Chronicle C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143859-1
Project/Site: NC North Mecklenburg Landfill -Infill SW SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: TB
Date Collected: 04/09/18 00:00
Date Received: 04/14/18 12:55
Lab Sample ID: 500-143859-7
Matrix: Water
Batch Batch Dilution Batch Prepared
Prep Type Type Method Run Factor Number or Analyzed Analyst Lab
Total/NA Analysis 8260B 1 428305 04/18/18 17:59 JDD TAL CHI
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
Page 30 of 34
TestAmerica Chicago
7/5/2018

Accreditation/Certification Summary C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143859-1
Project/Site: NC North Mecklenburg Landfill -Infill SW SDG: NCDEQ Solid Waste Facility = # 60-13
Laboratory: TestAmerica Chicago
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW) State Program 4 291 12-31-18
The following analytes are included in this report, but accreditation/certification is not offered by the governing authority:
Analysis Method Prep Method Matrix Analyte
8260E Water trans-1,4-Dichloro-2-butene
TestAmerica Chicago
Page 31 of 34 7/5/2018

TestAmerica
THE LEADER IN ENVIRONMENTA
2417 Bond Street, University Park, IL ( '
Phone: [phone] Fax: 708.5'
500-143859 COC
(optional)
Report To
Contact:_ -,' 4 6,,o fR o A&, n
Company:
Address: f
P,J c)ra dw
Address:
1C'
Phone:
it :5't- (') % 2D
Fax:
BIII To
Contact:
Company:
Address:
Address:
Phone:
Fax:
on u ro..r....,...,.,.0
(optional)
Chain of Custody Record
I
Lab Job #: ,
Chain of Custody Number:
Page of
Temperature °C of Cooler: -5t
Client
LCIlentProject #
G ! + 370, 1
Preservative
'
PreservativeKey
1. HCool to 41
H2SO4,S to Cool to 4°
Project Name
Parameter
2.
3. HNO3, Cool to 4°
Va
� �
(�
�
V
�y (' Q
'e.JSampling���J� �`}Sample
�
4. NaOH, Cool to 41
7. Cool to 4°
8. None
9. Other
Project Location/State / /� }
/ ',i � f A .
Lab Project # � n /
n "7 v� l
Sampler
Lab PM
i-\ V
T111H.
ID
\ Cs
Comments
Date
Time
Z
LIZ!0
,
Turnaround Time Required (Business Days) Sample Disposal
_ 1 Day _ 2 Days _ 5 Days `C 7 Days _ 10 Days _ 15 Days Other Disposal by Lab
Requested Due Date Return to Client ,c ' Archive for
Months ( ee may be assessed if samples are retained longer than 1 mgnth)
Da // ' Time
Lab Courier
Relinq •shed Company Date
Time
Received B
o parry
Relinquished By Company Date
Time
1'
rceive 'y
Com antj
ate` C Time
11
Relinquished By Company Date
Time ✓ 1
IA �d'By"�
Comp ny
Date Time
Nlamx Rey ubent Comments LaD Comments:
WW - Wastewater SE -Sediment
W - Water 80 - Soil
-S - Soil L- Leachate
SL-Sludge WI -Wipe
MS - Miscellaneous DW - Drinking Water
OL-011 O-Other
A -Air
Hand Delivered
Page 32 of 34 TAL-41zn--o0209618

ORIGIN ID:JOTA [phone]
MATT GINTHER (CEC)
IISAPR18
-MAN
GREENWAY WASTE OF NORTH MECK
15300 HOLBROOKS ROAD
HUNTERSVILLE, NC 28078
UNITED STATE. U5
14o
TO SAMPLE LOGIN
,Q
TESTAMERICA LABS
2417 BOND ST
UNIVERSITY PARK IL
60484 W albill
(708) 534- 5200
500143859
RMA: III Jill Ili
`Express
FedEx
SATURDAY 12a001
R; KP 4059 7171 6741
PRIORITY OVERNIGHT.
XO JOTA
6a4�4
i�-us ORD "' ,
077514 OVIS 552J1/91321DCA5
L
Page 33 of 34 7/5/2018

Client: Civil & Environmental Consultants Inc
Login Number: 143859
List Number: 1
Creator: Scott, Sherri L
Question
Login Sample Receipt Checklist
Job Number: 500-143859-1
SDG Number: NCDEQ Solid Waste Facility = # 60-13
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
True
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
False
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
False
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
3.3
List Source: TestAmerica Chicago
TestAmerica Chicago
Page 34 of 34 7/5/2018

TestAmerica °
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Chicago
2417 Bond Street
University Park, IL 60484
Tel: [phone]
TestAmerica Job ID: 500-143858-1
TestAmerica SDG: NCDEQ Solid Waste Facility = # 60-13
Client Project/Site: NC North Mecklenburg Landfill - Infill
ror:
Civil & Environmental Consultants Inc
1900 Center Park Drive
Suite A
Charlotte, North Carolina 28217
Attn: Matt Ginther
A6%�/V 6W
Authorized for release by:
71512018 8:38:50 AM
Robin Kintz, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1 F
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Table of Contents
CoverPage ..............................................
1
Table of Contents .........................................
2
Case Narrative ...........................................
3 L
Detection Summary ........................................
5
Method Summary .........................................
17
Sample Summary .........................................
18
Client Sample Results ......................................
19
E:
Definitions ...............................................
164
QC Association ...........................................
166 F
Surrogate Summary .......................................
180
QC Sample Results ........................................
185
Chronicle................................................
232
Certification Summary ......................................
248
Chain of Custody ..........................................
249
E:
Receipt Checklists .........................................
258
TestAmerica Chicago
Page 2 of 258 7/5/2018

Case Narrative
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Job ID: 500-143858-1
Laboratory: TestAmerica Chicago
Narrative
Job Narrative
500-143858-1
Comments
No additional comments.
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Receipt
The samples were received on 4/14/2018 12:55 PM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperatures of the 11 coolers at receipt time were 0.61 C, 0.90 C, 1.40 C, 1.50 C, 1.80 C, 2.30 C, 2.50 C, 2.80 C, 3.30 C, 3.31 C and
9.60 C.
Receipt Exceptions
Received all 3 VOA vials for sample 21 with headspace. Received 1 VOA vial for samples 26 & 27 with headspace. MW-7(i)
(500-143858-21), TB (500-143858-26), TB (500-143858-27)
The following samples were received at the laboratory outside the required temperature criteria: MW11(i) (500-143858-30) and MW11 D(i)
(500-143858-31). The client was contacted regarding this issue, and the laboratory was instructed to proceed with analysis.
The following samples were submitted for analysis; however, it was not listed on the Chain -of -Custody (COC): Duplicate
(500-143858-22), TB (500-143858-25), TB (500-143858-26), TB (500-143858-27), TB (500-143858-28) and TB (500-143858-29). Added
to COC and logged in for analysis.
GC/MS VOA
Method(s) 8260B: The method blank for batch 429099 was non -detect for all target analytes. Samples associated with this method blank
detected Acetone just above or below the reporting limit. Acetone is a known lab contaminant; therefore all low level detects for this
compound should be considered lab contamination. The results have been flagged with a "CN" to denote the probable contamination.
MW-8(i) (500-143858-13), MW-2(i) (500-143858-14), MW-3(i) (500-143858-15), MW-4D(i) (500-143858-16), MW-6(i) (500-143858-18),
MW-7D(i) (500-143858-19), MW-5D(i) (500-143858-20) and Duplicate 1 (500-143858-23)
Method(s) 8260B: The method blank for batch 429099 was non -detect for all target analytes. Samples associated with this method blank
detected Methylene Chloride just above the reporting limit. Methylene Chloride is a known lab contaminant; therefore all low level detects
for this compound should be considered lab contamination. The results have been flagged with a "CN" to denote the probable
contamination. Duplicate 1 (500-143858-23)
Method(s) 8260B: The method blanks for batches 428915, 429099, 429285 and 428709 were non -detect for all target analytes. Samples
associated with this method blank detected Acetone just above or below the reporting limit. Acetone is a known lab contaminant; therefore
all low level detects for this compound should be considered lab contamination. The results have been flagged with a "CN" to denote the
probable contamination.
MW-12(i) (500-143858-1), MW-14(i) (500-143858-2), MW-1(i) (500-143858-5), MW-13(i) (500-143858-6), MW-12D(i) (500-143858-7),
MW-9(i) (500-143858-10), MW-9D(i) (500-143858-11), MW-10(i) (500-143858-12), MW-8(i) (500-143858-13), MW-2(i) (500-143858-14),
MW-3(i) (500-143858-15), MW-4D(i) (500-143858-16), MW-4(i) (500-143858-17), MW-6(i) (500-143858-18), MW-7D(i) (500-143858-19),
MW-5D(i) (500-143858-20), MW-7(i) (500-143858-21), Duplicate (500-143858-22), Duplicate 1 (500-143858-23), Duplicate 2
(500-143858-24), MW11(i) (500-143858-30) and MW11 D(i) (500-143858-31)
Method(s) 8260B: The method blanks for batches 428915 and 429099 were non -detect for all target analytes. Samples associated with
the method blanks detected Methylene Chloride just above or below the reporting limit. Methylene Chloride is a known lab contaminant;
therefore all low level detects for this compound should be considered lab contamination. The results have been flagged with a "CN" to
denote the probable contamination. MW-12(i) (500-143858-1), MW-12D(i) (500-143858-7), MW-9D(i) (500-143858-11) and Duplicate 1
(500-143858-23)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
TestAmerica Chica o
Page 3 of 258 7/5/20T8

Case Narrative C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Job ID: 500-143858-1 (Continued)
Laboratory: TestAmerica Chicago (Continued)
Method(s) 8270D: The following sample contained one base surrogate outside acceptance limits: MW-10(i) (500-143858-12), MW-5D(i)
(500-143858-20) and MW11D(i) (500-143858-31). The laboratory's SOP allows one acid and one base surrogate to be outside
acceptance limits; therefore, re -extraction was not performed. These results have been reported and qualified.
Method(s) 8270D: The method blank for preparation batch 500-428463 and analytical batch 500-428521 contained Acenaphthylene, Butyl
benzyl phthalate and Fluorene above the method detection limit. This target analyte concentration was less than the reporting limit (RL);
therefore, re -extraction and/or re -analysis of samples was not performed.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC Semi VOA
Method(s) 8081 B: The laboratory control sample duplicate (LCSD) for preparation batch 500-428495 and analytical batch 500-428753
recovered outside control limits for delta-BHC. This analyte was biased high in the LCSD and was not detected in the associated
samples; therefore, the data has been reported.
Method(s) 8081 B: The RPD of the laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for batch preparation
batch 500-428495 and analytical batch 500-428753 recovered outside control limits for Aldrin.
Method(s) 8081 B: The following samples were diluted due to the nature of the sample matrix: MW-13(i) (500-143858-6) and MW-12D(i)
(500-143858-7). Elevated reporting limits (RLs) are provided. F
Method(s) 8081 B: Surrogate recovery for the following samples were outside control limits: MW-13(i) (500-143858-6) and MW-12D(i)
(500-143858-7). Evidence of matrix interference is present; therefore, re -extraction and/or re -analysis was not performed.
Method(s) 8081 B: The following sample was diluted due to the nature of the sample matrix: MW-7(i) (500-143858-21). Elevated reporting
limits (RLs) are provided.
Method(s) 8081 B: Surrogate recovery for the following sample was outside control limits: MW-7(i) (500-143858-21). Evidence of matrix
interference is present; therefore, re -extraction and/or re -analysis was not performed. The secondary column recovered within control
limits for these surrogates
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
Method(s) 300.0, 9056A: Manual integration was performed on the following IC 5 samples due to the software identifying the baseline
incorrectly: (CCB 500-429810/11).
Method(s) 300.0, 9056A: Manual integration was performed on the following IC 5 sample due to the software identifying the baseline
incorrectly: (ICB 500-429826/2).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
TestAmerica Chica o
Page 4 of 258 7/5/20T8

Detection Summary C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-12(i)
Analyte Result
Qualifier
RL
LOD
MDL
Unit
Acetone
6.2
cn
5.0
2.5
1.7
ug/L
Benzene
0.54
0.50
0.25
0.15
ug/L
Methylene Chloride
4.0
J cn
5.0
2.5
1.6
ug/L
Arsenic
0.39
J
1.0
0.50
0.23
ug/L
Barium
240
2.5
1.3
0.73
ug/L
Cobalt
6.4
1.0
0.50
0.40
ug/L
Copper
0.84
J B
2.0
1.0
0.50
ug/L
Iron
240
100
50
47
ug/L
Manganese
310
2.5
1.3
0.79
ug/L
Nickel
9.7
2.0
1.0
0.63
ug/L
Silver
0.19
J
0.50
0.25
0.12
ug/L
Arsenic
0.48
J
1.0
0.50
0.23
ug/L
Barium
220
2.5
1.3
0.73
ug/L
Cobalt
6.1
1.0
0.50
0.40
ug/L
Copper
5.0
2.0
1.0
0.50
ug/L
Iron
200
100
50
47
ug/L
Manganese
300
2.5
1.3
0.79
ug/L
Nickel
9.4
2.0
1.0
0.63
ug/L
Lead
0.35
J
0.50
0.25
0.19
ug/L
Zinc
7.2
J
10
20
6.9
ug/L
Chloride
37000
F1
2000
1700
1700
ug/L
Sulfate
67000
B F1
2000
1000
950
ug/L
Alkalinity
440000
5000
5000
3700
ug/L
Total Dissolved Solids
710000
10000
10000
4300
ug/L
Lab Sample ID: 500-143858-1
Dil Fac D
Method
Prep Type
1
8260B
Total/NA
1
8260B
Total/NA
1
8260B
Total/NA
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
1
60206
Total
Recoverable
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
1
6020B
Dissolved
1
6020B
Dissolved
1
6020B
Dissolved
1
6020B
Dissolved
1
6020B
Dissolved
1
6020B
Dissolved
1
6020B
Dissolved
1
6020B
Dissolved
1
6020B
Dissolved
10
9056A
Total/NA
10
9056A
Total/NA
1
SM 2320B
Total/NA
1
SM 2540C
Total/NA
Client Sample ID: MW-14(i)
Lab Sample ID: 500-143858-2
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D
Method
Prep Type
Acetone
4.2
J cn
5.0
2.5
1.7
ug/L
1
8260B
Total/NA
Arsenic
0.34
J
1.0
0.50
0.23
ug/L
1
6020B
Total
Recoverable
Barium
24
2.5
1.3
0.73
ug/L
1
6020B
Total
Recoverable
Copper
1.5
J B
2.0
1.0
0.50
ug/L
1
6020B
Total
Recoverable
Iron
230
100
50
47
ug/L
1
6020B
Total
Recoverable
Manganese
17
2.5
1.3
0.79
ug/L
1
6020B
Total
Recoverable
Vanadium
3.2
J
5.0
2.5
2.2
ug/L
1
6020B
Total
Recoverable
Arsenic
0.25
J
1.0
0.50
0.23
ug/L
1
6020B
Dissolved
Barium
22
2.5
1.3
0.73
ug/L
1
6020B
Dissolved
Copper
10
2.0
1.0
0.50
ug/L
1
6020B
Dissolved
Manganese
4.5
2.5
1.3
0.79
ug/L
1
6020B
Dissolved
Lead
1.5
0.50
0.25
0.19
ug/L
1
6020B
Dissolved
This Detection Summary does not include radiochemical test results.
Page 5 of 258
TestAmerica Chicago
7/5/2018

Detection Summary
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID:
500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG:
NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-14(i) (Continued)
Lab Sample ID: 500-143858-2
Analyte Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D Method
Prep Type
Vanadium 2.6
J
5.0
2.5
2.2
ug/L
1 6020B
Dissolved
Zinc 16
10
20
6.9
ug/L
1 6020B
Dissolved
Chloride 5700
400
340
340
ug/L
2 9056A
Total/NA
Sulfate 9300
B
400
200
190
ug/L
2 9056A
Total/NA
Alkalinity 61000
5000
5000
3700
ug/L
1 SM 2320B
Total/NA
Total Dissolved Solids 120000
10000
10000
4300
ug/L
1 SM 2540C
Total/NA
Client Sample ID: MW-15(i)
Lab Sample ID: 500-143858-3
Analyte Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D Method
Prep Type
Chloride 57000
4000
3400
3400
ug/L
20 9056A
Total/NA
Sulfate 24000
B
1000
500
480
ug/L
5 9056A
Total/NA
Alkalinity 300000
5000
5000
3700
ug/L
1 SM 2320B
Total/NA
Total Dissolved Solids 490000
10000
10000
4300
ug/L
1 SM 2540C
Total/NA
Client Sample ID: MW-16(i)
Lab Sample ID: 500-143858-4
Analyte Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D Method
Prep Type
Arsenic 0.68
J
1.0
0.50
0.23
ug/L
1 6020B
Total
Recoverable
Barium 120
2.5
1.3
0.73
ug/L
1 6020B
Total
Recoverable
Chromium 5.6
B
5.0
2.5
1.1
ug/L
1 6020E
Total
Recoverable
Cobalt 7.9
1.0
0.50
0.40
ug/L
1 6020B
Total
Recoverable
Copper 5.6
B
2.0
1.0
0.50
ug/L
1 6020B
Total
Recoverable
Iron 6600
100
50
47
ug/L
1 6020B
Total
Recoverable
Lead 1.1
0.50
0.25
0.19
ug/L
1 6020B
Total
Recoverable
Manganese 1600
2.5
1.3
0.79
ug/L
1 6020B
Total
Recoverable
Nickel 3.0
2.0
1.0
0.63
ug/L
1 6020B
Total
Recoverable
Vanadium 11
5.0
2.5
2.2
ug/L
1 6020B
Total
Recoverable
Zinc 17
B
10
20
6.9
ug/L
1 6020E
Total
Recoverable
Chloride 3600
400
340
340
ug/L
2 9056A
Total/NA
Sulfate 34000
B
1000
500
480
ug/L
5 9056A
Total/NA
Alkalinity 43000
5000
5000
3700
ug/L
1 SM 2320B
Total/NA
Total Dissolved Solids 120000
10000
10000
4300
ug/L
1 SM 2540C
Total/NA
Client Sample ID: MW-1(i)
Lab Sample ID: 500-143858-5
Analyte Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D Method
Prep Type
Acetone 5.9
cn
5.0
2.5
1.7
ug/L
1 8260B
Total/NA
Bis(2-ethylhexyl) 1.9
J
8.0
4.0
1.4
ug/L
1 8270D
Total/NA
phthalate
Chloride 20000
1000
850
850
ug/L
5 9056A
Total/NA
Sulfate 13000
B
400
200
190
ug/L
2 9056A
Total/NA
This Detection Summary does not include radiochemical test results.
Page 6 of 258
TestAmerica Chicago
7/5/2018

Detection Summary
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID:
500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG:
NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-1(1) (Continued)
Lab Sample ID: 500-143858-5
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D
Method
Prep Type
Alkalinity
210000
5000
5000
3700
ug/L
1
SM 2320B
Total/NA
Total Dissolved Solids
320000
10000
10000
4300
ug/L
1
SM 2540C
Total/NA
Client Sample ID: MW-13(i)
Lab Sample ID: 500-143858-6
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D
Method
Prep Type
Acetone
9.7
cn
5.0
2.5
1.7
ug/L
1
8260E
Total/NA
Arsenic
1.0
1.0
0.50
0.23
ug/L
1
6020B
Total
Recoverable
Barium
65
2.5
1.3
0.73
ug/L
1
6020B
Total
Recoverable
Chromium
8.2
B
5.0
2.5
1.1
ug/L
1
6020B
Total
Recoverable
Cobalt
2.0
1.0
0.50
0.40
ug/L
1
6020B
Total
Recoverable
Copper
18
B
2.0
1.0
0.50
ug/L
1
6020B
Total
Recoverable
Iron
5300
100
50
47
ug/L
1
6020B
Total
Recoverable
Lead
0.36
J
0.50
0.25
0.19
ug/L
1
6020B
Total
Recoverable
Manganese
2300
2.5
1.3
0.79
ug/L
1
6020B
Total
Recoverable
Nickel
4.8
2.0
1.0
0.63
ug/L
1
6020B
Total
Recoverable
Tin
2.0
J
5.0
2.5
1.3
ug/L
1
6020E
Total
Recoverable
Vanadium
4.5
J
5.0
2.5
2.2
ug/L
1
6020E
Total
Recoverable
Zinc
11
B
10
20
6.9
ug/L
1
6020E
Total
Recoverable
Arsenic
0.94
J
1.0
0.50
0.23
ug/L
1
6020B
Dissolved
Barium
37
2.5
1.3
0.73
ug/L
1
6020B
Dissolved
Cobalt
0.63
J
1.0
0.50
0.40
ug/L
1
6020B
Dissolved
Iron
990
100
50
47
ug/L
1
6020B
Dissolved
Manganese
1500
2.5
1.3
0.79
ug/L
1
6020B
Dissolved
Chloride
17000
1000
850
850
ug/L
5
9056A
Total/NA
Sulfate
2200
B
200
100
95
ug/L
1
9056A
Total/NA
Alkalinity
220000
5000
5000
3700
ug/L
1
SM 2320B
Total/NA
Total Dissolved Solids
270000
10000
10000
4300
ug/L
1
SM 2540C
Total/NA
Client Sample ID: MW-121)(i)
Lab Sample ID: 500-143858-7
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D
Method
Prep Type
Acetone
8.2
cn
5.0
2.5
1.7
ug/L
1
8260B
Total/NA
Benzene
0.62
0.50
0.25
0.15
ug/L
1
8260B
Total/NA
Methylene Chloride
5.3
cn
5.0
2.5
1.6
ug/L
1
8260B
Total/NA
Arsenic
2.9
1.0
0.50
0.23
ug/L
1
6020B
Total
Recoverable
Barium
240
2.5
1.3
0.73
ug/L
1
6020B
Total
Recoverable
Cobalt
1.3
1.0
0.50
0.40
ug/L
1
6020B
Total
Recoverable
This Detection Summary does not include radiochemical test results.
Page 7 of 258
TestAmerica Chicago
7/5/2018

Detection Summary
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID:
500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG:
NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-1213(i) (Continued)
Lab Sample ID: 500-143858-7
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D
Method
Prep Type
Iron
6900
100
50
47
ug/L
1
6020B
Total
Recoverable
Manganese
510
2.5
1.3
0.79
ug/L
1
6020B
Total
Recoverable
Nickel
3.2
2.0
1.0
0.63
ug/L
1
6020B
Total
Recoverable
Tin
1.5
J
5.0
2.5
1.3
ug/L
1
6020E
Total
Recoverable
Arsenic
3.6
1.0
0.50
0.23
ug/L
1
6020B
Dissolved
Barium
240
2.5
1.3
0.73
ug/L
1
6020B
Dissolved
Cobalt
1.1
1.0
0.50
0.40
ug/L
1
6020B
Dissolved
Iron
8800
100
50
47
ug/L
1
6020B
Dissolved
Manganese
640
2.5
1.3
0.79
ug/L
1
6020B
Dissolved
Nickel
2.0
2.0
1.0
0.63
ug/L
1
6020B
Dissolved
Zinc
8.0
J
10
20
6.9
ug/L
1
6020E
Dissolved
Chloride
37000
4000
3400
3400
ug/L
20
9056A
Total/NA
Sulfate
68000
B
4000
2000
1900
ug/L
20
9056A
Total/NA
Alkalinity
540000
5000
5000
3700
ug/L
1
SM 2320B
Total/NA
Total Dissolved Solids
750000
10000
10000
4300
ug/L
1
SM 2540C
Total/NA
Client Sample ID: MW-8D(i)
Lab Sample ID: 500-143858-8
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D
Method
Prep Type
Barium
56
2.5
1.3
0.73
ug/L
1
6020B
Total
Recoverable
Copper
1.2
J B
2.0
1.0
0.50
ug/L
1
6020B
Total
Recoverable
Manganese
2.8
2.5
1.3
0.79
ug/L
1
6020B
Total
Recoverable
Vanadium
4.1
J
5.0
2.5
2.2
ug/L
1
6020B
Total
Recoverable
Chloride
40000
4000
3400
3400
ug/L
20
9056A
Total/NA
Sulfate
27000
B
1000
500
480
ug/L
5
9056A
Total/NA
Alkalinity
190000
5000
5000
3700
ug/L
1
SM 2320B
Total/NA
Total Dissolved Solids
330000
10000
10000
4300
ug/L
1
SM 2540C
Total/NA
Client Sample ID: MW-5(i)
Lab Sample ID: 500-143858-9
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D
Method
Prep Type
Arsenic
0.43
J
1.0
0.50
0.23
ug/L
1
6020B
Total
Recoverable
Barium
280
2.5
1.3
0.73
ug/L
1
6020B
Total
Recoverable
Cobalt
0.48
J
1.0
0.50
0.40
ug/L
1
6020B
Total
Recoverable
Copper
0.76
J B
2.0
1.0
0.50
ug/L
1
6020B
Total
Recoverable
Iron
38000
100
50
47
ug/L
1
6020B
Total
Recoverable
Lead
0.24
J
0.50
0.25
0.19
ug/L
1
6020B
Total
Recoverable
Manganese
3800
2.5
1.3
0.79
ug/L
1
6020B
Total
Recoverable
This Detection Summary does not include radiochemical test results.
Page 8 of 258
TestAmerica Chicago
7/5/2018

Detection Summary
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID:
500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG:
NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-5(i) (Continued)
Lab Sample ID: 500-143858-9
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D
Method
Prep Type
Nickel
1.4
J
2.0
1.0
0.63
ug/L
1
6020B
Total
Recoverable
Vanadium
2.2
J
5.0
2.5
2.2
ug/L
1
6020E
Total
Recoverable
Chloride
28000
2000
1700
1700
ug/L
10
9056A
Total/NA
Sulfate
84000
2000
1000
950
ug/L
10
9056A
Total/NA
Alkalinity
420000
5000
5000
3700
ug/L
1
SM 2320B
Total/NA
Total Dissolved Solids
660000
10000
10000
4300
ug/L
1
SM 2540C
Total/NA
Client Sample ID: MW-9(i)
Lab Sample ID: 500-143858-10
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D
Method
Prep Type
Acetone
7.2
cn
5.6
2.5
1.7
ug/L
1
8260B
Tota NANA
Benzene
1.5
0.50
0.25
0.15
ug/L
1
8260B
Total/NA
Di-n-butyl phthalate
0.90
J
4.2
2.1
0.61
ug/L
1
8270D
Total/NA
Arsenic
0.56
J
1.0
0.50
0.23
ug/L
1
6020B
Total
Recoverable
Barium
480
2.5
1.3
0.73
ug/L
1
6020B
Total
Recoverable
Cobalt
5.1
1.0
0.50
0.40
ug/L
1
6020B
Total
Recoverable
Copper
0.69
J B
2.0
1.0
0.50
ug/L
1
6020B
Total
Recoverable
Iron
1500
100
50
47
ug/L
1
6020B
Total
Recoverable
Manganese
220
2.5
1.3
0.79
ug/L
1
6020B
Total
Recoverable
Nickel
5.1
2.0
1.0
0.63
ug/L
1
6020B
Total
Recoverable
Vanadium
4.7
J
5.0
2.5
2.2
ug/L
1
6020B
Total
Recoverable
Chloride
52000
2000
1700
1700
ug/L
10
9056A
Total/NA
Sulfate
40000
2000
1000
950
ug/L
10
9056A
Total/NA
Alkalinity
670000
5000
5000
3700
ug/L
1
SM 2320B
Total/NA
Total Dissolved Solids
840000
10000
10000
4300
ug/L
1
SM 2540C
Total/NA
Client Sample ID: MW-91)(1)
Lab Sample ID: 500-143858-11
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D
Method
Prep Type
Acetone
9.0
cn
1.7
ug/L
1
82606
Total/NA
Benzene
0.47
J
0.50
0.25
0.15
ug/L
1
8260B
Total/NA
cis-1,2-Dichloroethene
2.4
1.0
0.50
0.41
ug/L
1
8260B
Total/NA
Methylene Chloride
4.3
J cn
5.0
2.5
1.6
ug/L
1
8260B
Total/NA
Tetrahydrofuran
12
10
5.0
1.9
ug/L
1
8260B
Total/NA
Di-n-butyl phthalate
0.73
J
3.9
2.0
0.57
ug/L
1
8270D
Total/NA
Arsenic
0.58
J
1.0
0.50
0.23
ug/L
1
6020B
Total
Recoverable
Barium
290
2.5
1.3
0.73
ug/L
1
6020B
Total
Recoverable
Copper
0.74
J B
2.0
1.0
0.50
ug/L
1
6020B
Total
Recoverable
Iron
400
100
50
47
ug/L
1
6020B
Total
Recoverable
This Detection Summary does not include radiochemical test results.
Page 9 of 258
TestAmerica Chicago
7/5/2018

Detection Summary
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG:
NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-9D(i) (Continued)
Lab Sample ID: 500-143858-11
Analyte Result Qualifier
RL
LOD
MDL
Unit
Dil Fac D Method Prep Type
Manganese 470
2.5
1.3
0.79
ug/L
1 6020B Total
Recoverable
Nickel 2.3
2.0
1.0
0.63
ug/L
1 6020B Total
Recoverable
Chloride 36000 F1
2000
1700
1700
ug/L
10 9056A Total/NA
Sulfate 66000
2000
1000
950
ug/L
10 9056A Total/NA
Alkalinity 800000
5000
5000
3700
ug/L
1 SM 2320B Total/NA
Total Dissolved Solids 1000000
10000
10000
4300
ug/L
1 SM 2540C Total/NA
Client Sample ID: MW-10(i)
Lab Sample ID: 500-143858-12
Analyte Result Qualifier
RL
LOD
MDL
Unit
Dil Fac D Method Prep Type
Acetone 2.3 Jan
5.6
2.5
1.7
ug/L
1 8260B Total/NA
Chloride 20000
2000
1700
1700
ug/L
10 9056A Total/NA
Sulfate 120000
4000
2000
1900
ug/L
20 9056A Total/NA
Alkalinity 290000
5000
5000
3700
ug/L
1 SM 2320B Total/NA
Total Dissolved Solids 570000
10000
10000
4300
ug/L
1 SM 2540C Total/NA
l :illent sampie iu: mw-ts(q
Lan sampie iu: ODU-14JUOU-I3
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D
Method
Prep Type
Acetone
5.5
cn
5.0
2.5
1.7
ug/L
1
8260B
Total/NA
Di-n-butyl phthalate
0.56
J
3.8
1.9
0.56
ug/L
1
8270D
Total/NA
Arsenic
0.46
J
1.0
0.50
0.23
ug/L
1
6020B
Total
Recoverable
Barium
44
2.5
1.3
0.73
ug/L
1
6020B
Total
Recoverable
Cobalt
2.5
1.0
0.50
0.40
ug/L
1
6020B
Total
Recoverable
Copper
1.1
J B
2.0
1.0
0.50
ug/L
1
6020B
Total
Recoverable
Iron
1500
100
50
47
ug/L
1
6020B
Total
Recoverable
Manganese
390
2.5
1.3
0.79
ug/L
1
6020B
Total
Recoverable
Nickel
1.6
J
2.0
1.0
0.63
ug/L
1
6020B
Total
Recoverable
Vanadium
6.2
5.0
2.5
2.2
ug/L
1
6020B
Total
Recoverable
Chloride
83000
4000
3400
3400
ug/L
20
9056A
Total/NA
Sulfate
7300
200
100
95
ug/L
1
9056A
Total/NA
Alkalinity
230000
5000
5000
3700
ug/L
1
SM 2320B
Total/NA
Total Dissolved Solids
410000
10000
10000
4300
ug/L
1
SM 2540C
Total/NA
Client Sample ID: MW-2(i)
Lab Sample ID: 500-143858-14
Analyte Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac
D Method
Prep Type
Acetone 7.6
cn
5.0
2.5
1.7
ug/L
1
8260E
Total/NA
Arsenic 0.37
J
1.0
0.50
0.23
ug/L
1
6020B
Total
Recoverable
Barium 44
2.5
1.3
0.73
ug/L
1
6020B
Total
Recoverable
Copper 2.3
B
2.0
1.0
0.50
ug/L
1
6020B
Total
Recoverable
This Detection Summary does not include radiochemical test results.
TestAmerica Chicago
Page 10 of 258 7/5/2018

Detection Summary
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID:
500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG:
NCDEQ Solid
Waste Facility = # 60-13
Client Sample ID: MW-2(i) (Continued)
Lab Sample ID: 500-143858-14
Analyte Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac
D Method
Prep Type
Manganese 140
2.5
1.3
0.79
ug/L
1
6020B
Total
Recoverable
Nickel 0.72
J
2.0
1.0
0.63
ug/L
1
6020B
Total
Recoverable
Chloride 6100
1000
850
850
ug/L
5
9056A
Total/NA
Sulfate 240000
5000
2500
2400
ug/L
25
9056A
Total/NA
Alkalinity 81000
5000
5000
3700
ug/L
1
SM 2320B
Total/NA
Total Dissolved Solids 470000
10000
10000
4300
ug/L
1
SM 2540C
Total/NA
Client Sample ID: MW-3(i)
Lab Sample ID: 500-143858-15
Analyte Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac
D Method
Prep Type
Acetone 6.0
cn
5.0
2.5
1.7
ug/L
1
8260B
Tota NANA
Di-n-butyl phthalate 1.1
J
3.9
2.0
0.58
ug/L
1
8270D
Total/NA
Arsenic 0.26
J
1.0
0.50
0.23
ug/L
1
6020B
Total
Recoverable
Barium 70
2.5
1.3
0.73
ug/L
1
6020B
Total
Recoverable
Cobalt 4.5
1.0
0.50
0.40
ug/L
1
6020B
Total
Recoverable
Copper 0.74
J B
2.0
1.0
0.50
ug/L
1
6020B
Total
Recoverable
Iron 140
100
50
47
ug/L
1
6020B
Total
Recoverable
Manganese 2000
2.5
1.3
0.79
ug/L
1
6020B
Total
Recoverable
Chloride 6500
1000
850
850
ug/L
5
9056A
Total/NA
Sulfate 210000
5000
2500
2400
ug/L
25
9056A
Total/NA
Alkalinity 52000
5000
5000
3700
ug/L
1
SM 2320B
Total/NA
Total Dissolved Solids 390000
10000
10000
4300
ug/L
1
SM 2540C
Total/NA
Client Sample ID: MW-4D(i)
Lab Sample ID: 500-143858-16
Analyte Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac
D Method
Prep Type
Acetone 4.1
J cn
5.0
2.5
1.7
ug/L
1
8260B
Total/NA
Arsenic 0.37
J
1.0
0.50
0.23
ug/L
1
6020B
Total
Recoverable
Barium 40
2.5
1.3
0.73
ug/L
1
6020B
Total
Recoverable
Copper 0.55
J B
2.0
1.0
0.50
ug/L
1
6020B
Total
Recoverable
Manganese 0.96
J
2.5
1.3
0.79
ug/L
1
6020B
Total
Recoverable
Vanadium 3.7
J
5.0
2.5
2.2
ug/L
1
6020B
Total
Recoverable
Chloride 20000
1000
850
850
ug/L
5
9056A
Total/NA
Sulfate 18000
1000
500
480
ug/L
5
9056A
Total/NA
Alkalinity 190000
5000
5000
3700
ug/L
1
SM 2320B
Total/NA
Total Dissolved Solids 290000
10000
10000
4300
ug/L
1
SM 2540C
Total/NA
Client Sample ID: MW-4(i)
Lab Sample ID: 500-143858-17
Analyte Result
Qualifier
RL
LOD
MDL
Unit
DII Fac
D Method
Prep Type
cis- 1,2-Dichloroethene 0.82
J
1.0
0.50
0.41
ug/L
1
8260B
Total/NA
This Detection Summary does not include radiochemical test results.
TestAmerica Chicago
Page 11 of 258
7/5/2018

Detection Summary C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-4(i) (Continued)
Analyte Result Qualifier
RL
LOD
MDL
Unit
Vinyl chloride
1.6
1.0
0.50
0.20
ug/L
Arsenic
0.56
J
1.0
0.50
0.23
ug/L
Barium
210
2.5
1.3
0.73
ug/L
Cadmium
0.35
J
0.50
0.25
0.17
ug/L
Cobalt
39
1.0
0.50
0.40
ug/L
Copper
5.3
B
2.0
1.0
0.50
ug/L
Iron
53000
100
50
47
ug/L
Lead
0.21
J
0.50
0.25
0.19
ug/L
Manganese
12000
2.5
1.3
0.79
ug/L
Nickel
8.0
2.0
1.0
0.63
ug/L
Zinc
19
B
10
20
6.9
ug/L
Chloride
11000
1000
850
850
ug/L
Sulfate
26000
1000
500
480
ug/L
Alkalinity
340000
5000
5000
3700
ug/L
Total Dissolved Solids
460000
10000
10000
4300
ug/L
Lab Sample ID: 500-143858-17
Dil Fac D
Method
Prep Type
1
8260B
Total/NA
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
1
60206
Total
Recoverable
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
5
9056A
Total/NA
5
9056A
Total/NA
1
SM 2320B
Total/NA
1
SM 2540C
Total/NA
Client Sample ID: MW-6(i)
Lab Sample ID: 500-143858-18
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
Dil Fac D
Method
Prep Type
Acetone
8.3
cn
5.0
2.5
1.7
ug/L
1
8260E
Total/NA
Benzene
0.27
J
0.50
0.25
0.15
ug/L
1
8260B
Total/NA
Tetrahydrofuran
8.7
J
10
5.0
1.9
ug/L
1
8260E
Total/NA
Di-n-butyl phthalate
0.68
J
3.7
1.9
0.54
ug/L
1
8270D
Total/NA
Naphthalene
0.59
J
0.75
0.37
0.23
ug/L
1
8270D
Total/NA
Arsenic
1.0
1.0
0.50
0.23
ug/L
1
6020B
Total
Recoverable
Barium
210
2.5
1.3
0.73
ug/L
1
6020B
Total
Recoverable
Cobalt
9.3
1.0
0.50
0.40
ug/L
1
6020B
Total
Recoverable
Copper
0.96
J B
2.0
1.0
0.50
ug/L
1
6020B
Total
Recoverable
Iron
33000
100
50
47
ug/L
1
6020B
Total
Recoverable
Manganese
4700
2.5
1.3
0.79
ug/L
1
6020B
Total
Recoverable
Nickel
1.6
J
2.0
1.0
0.63
ug/L
1
6020B
Total
Recoverable
Chloride
48000
2000
1700
1700
ug/L
10
9056A
Total/NA
Sulfate
9100
200
100
95
ug/L
1
9056A
Total/NA
Alkalinity
530000
5000
5000
3700
ug/L
1
SM 2320B
Total/NA
Total Dissolved Solids
700000
10000
10000
4300
ug/L
1
SM 2540C
Total/NA
Client Sample ID: MW-71)(i)
Lab Sample ID: 500-143858-19
This Detection Summary does not include radiochemical test results
TestAmerica Chicago
Page 12 of 258 7/5/2018

Detection Summary C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-71)(1) (Continued)
Analyte Result Qualifier
RL
LOD
MDL
Unit
Acetone
11
cn
5.0
2.5
1.7
ug/L
Benzene
0.22
J
0.50
0.25
0.15
ug/L
Tetrahydrofuran
15
10
5.0
1.9
ug/L
Di-n-butyl phthalate
2.2
J
3.9
1.9
0.56
ug/L
Arsenic
0.76
J
1.0
0.50
0.23
ug/L
Barium
260
2.5
1.3
0.73
ug/L
Cobalt
2.3
1.0
0.50
0.40
ug/L
Copper
1.7
J B
2.0
1.0
0.50
ug/L
Iron
640
100
50
47
ug/L
Lead
0.49
J
0.50
0.25
0.19
ug/L
Manganese
1200
2.5
1.3
0.79
ug/L
Nickel
13
2.0
1.0
0.63
ug/L
Zinc
12
B
10
20
6.9
ug/L
Chloride
97000
5000
4300
4300
ug/L
Sulfate
130000
5000
2500
2400
ug/L
Alkalinity
670000
5000
5000
3700
ug/L
Total Dissolved Solids
1100000
10000
10000
4300
ug/L
Client Sample ID: MW-51)(1)
Analyte
Result
Qualifier
Acetone
20
cn
Butyl benzyl phthalate
1.1
J
Phenol
4.6
Arsenic
0.50
J
Barium
6.7
Chromium
2.5
J B
Cobalt
0.53
J
Copper
4.9
B
Iron
66
J
Manganese
6.2
Nickel
1.5
J
Chloride
15000
Sulfate
15000
Alkalinity
330000
Total Dissolved Solids
520000
Lab Sample ID: 500-143858-19
Dil Fac D
Method
Prep Type
1
8260B
Total/NA
1
8260B
Total/NA
1
8260B
Total/NA
1
8270D
Total/NA
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
1
60206
Total
Recoverable
1
60206
Total
Recoverable
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
25
9056A
Total/NA
25
9056A
Total/NA
1
SM 2320B
Total/NA
1
SM 2540C
Total/NA
Lab Sample ID: 500-143858-20
RL
LOD
MDL
Unit
Dil Fac D
Method
Prep Type
5.0
2.5
1.7
ug/L
1
8260B
Total/NA
1.5
0.75
0.36
ug/L
1
8270D
Total/NA
3.8
1.9
0.51
ug/L
1
8270D
Total/NA
1.0
0.50
0.23
ug/L
1
6020B
Total
Recoverable
2.5
1.3
0.73
ug/L
1
6020B
Total
Recoverable
5.0
2.5
1.1
ug/L
1
6020E
Total
Recoverable
1.0
0.50
0.40
ug/L
1
6020B
Total
Recoverable
2.0
1.0
0.50
ug/L
1
6020B
Total
Recoverable
100
50
47
ug/L
1
6020B
Total
Recoverable
2.5
1.3
0.79
ug/L
1
6020B
Total
Recoverable
2.0
1.0
0.63
ug/L
1
6020B
Total
Recoverable
1000
850
850
ug/L
5
9056A
Total/NA
1000
500
480
ug/L
5
9056A
Total/NA
5000
5000
3700
ug/L
1
SM 2320B
Total/NA
10000
10000
4300
ug/L
1
SM 2540C
Total/NA
This Detection Summary does not include radiochemical test results.
Page 13 of 258
TestAmerica Chicago
7/5/2018

Detection Summary C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-7(i)
Analyte Result
Qualifier
RL
LOD
MDL
Unit
Acetone
5.0
cn
5.0
2.5
1.7
ug/L
Benzene
1.4
0.50
0.25
0.15
ug/L
cis- 1,2-Dichloroethene
0.64
J
1.0
0.50
0.41
ug/L
Tetrahydrofuran
21
10
5.0
1.9
ug/L
Vinyl chloride
0.88
J
1.0
0.50
0.20
ug/L
Anthracene
0.46
J
0.75
0.38
0.25
ug/L
Di-n-butyl phthalate
1.4
J
3.8
1.9
0.55
ug/L
Arsenic
0.56
J
1.0
0.50
0.23
ug/L
Barium
190
2.5
1.3
0.73
ug/L
Cobalt
3.7
1.0
0.50
0.40
ug/L
Iron
410
100
50
47
ug/L
Manganese
350
2.5
1.3
0.79
ug/L
Nickel
3.6
2.0
1.0
0.63
ug/L
Chloride
81000
4000
3400
3400
ug/L
Sulfate
160000
4000
2000
1900
ug/L
Alkalinity
530000
5000
5000
3700
ug/L
Total Dissolved Solids
1000000
10000
10000
4300
ug/L
Lab Sample ID: 500-143858-21
Dil Fac D
Method
Prep Type
1
8260B
Total/NA
1
8260B
Total/NA
1
8260B
Total/NA
1
8260B
Total/NA
1
8260B
Total/NA
1
8270D
Total/NA
1
8270D
Total/NA
1
60206
Total
Recoverable
1
60206
Total
Recoverable
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
1
6020B
Total
Recoverable
20
9056A
Total/NA
20
9056A
Total/NA
1
SM 2320B
Total/NA
1
SM 2540C
Total/NA
Client Sample ID: Duplicate
Lab Sample ID: 500-143858-22
Analyte Result Qualifier
RL
LOD
MDL
Unit
Dil Fac D Method Prep Type
Acetone 10 cn
5.0
2.5
1.7
ug/L
1 8260B Total/NA
Benzene 1.2
0.50
0.25
0.15
ug/L
1 8260B Total/NA
cis-1,2-Dichloroethene 0.98 J
1.0
0.50
0.41
ug/L
1 8260B Total/NA
Client Sample ID: Duplicate 1
Analyte
Result
Qualifier
Acetone
16
cn
Benzene
0.67
cis-1,2-Dichloroethene
1.8
Methylene Chloride
5.0
cn
Tetrahydrofuran
6.1
J
Trichloroethene
0.19
J
Vinyl chloride
3.1
Client Sample ID: Duplicate 2
Analyte
Result Qualifier
Acetone
10 cn
Benzene
0.56
cis- 1,2-Dichloroethene
1.6
Methylene Chloride
4.7 J
Tetrahydrofuran
4.8 J
Vinyl chloride
1.5
Lab Sample ID: 500-143858-23
RL
LOD
MDL
Unit
Dil Fac
D Method
Prep Type
5.0
2.5
1.7
ug/L
1
8260B
Total/NA
0.50
0.25
0.15
ug/L
1
8260B
Total/NA
1.0
0.50
0.41
ug/L
1
8260B
Total/NA
5.0
2.5
1.6
ug/L
1
8260B
Total/NA
10
5.0
1.9
ug/L
1
8260B
Total/NA
0.50
0.25
0.16
ug/L
1
8260B
Total/NA
1.0
0.50
0.20
ug/L
1
8260B
Total/NA
Lab Sample ID: 500-143858-24
RL
LOD
MDL
Unit
Dil Fac D Method Prep Type
5.0
2.5
1.7
ug/L
1 8260B Total/NA
0.50
0.25
0.15
ug/L
1 8260B Total/NA
1.0
0.50
0.41
ug/L
1 8260B Total/NA
5.0
2.5
1.6
ug/L
1 8260B Total/NA
10
5.0
1.9
ug/L
1 8260B Total/NA
1.0
0.50
0.20
ug/L
1 8260B Total/NA
This Detection Summary does not include radiochemical test results.
Page 14 of 258
TestAmerica Chicago
7/5/2018

Detection Summary
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg
Landfill - Infill
SDG:
NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: TB
Lab Sample ID: 500-143858-25
1 No Detections.
a
Client Sample ID: TB
Lab Sample ID: 500-143858-26 L
INo Detections.
Client Sample ID: TB
Lab Sample ID: 500-143858-27
1 No Detections.
E:
Client Sample ID: TB
Lab Sample ID: 500-143858-28
INo Detections.
F
Client Sample ID: TB
Lab Sample ID: 500-143858-29
FNo Detections.
Client Sample ID: MW11(i)
Lab Sample ID: 500-143858-30
Analyte
Result Qualifier
RL
LOD
MDL
Unit
Dil Fac D Method Prep Type
Acetone
7.2 cn
5.0
2.5
1.7
ug/L
1 8260B Total/NA
Arsenic
1.0
1.0
0.50
0.23
ug/L
1 6020B Total
Recoverable
Barium
85
2.5
1.3
0.73
ug/L
1 6020B Total
Recoverable
Chromium
1.2 J
5.0
2.5
1.1
ug/L
1 6020E Total
Recoverable
Cobalt
2.3
1.0
0.50
0.40
ug/L
1 6020B Total
Recoverable
Copper
1.5 J
2.0
1.0
0.50
ug/L
1 6020B Total
Recoverable
Iron
11000
100
50
47
ug/L
1 6020B Total
Recoverable
Manganese
1000
2.5
1.3
0.79
ug/L
1 6020B Total
Recoverable
Nickel
2.6
2.0
1.0
0.63
ug/L
1 6020B Total
Recoverable
Chloride
14000
1000
850
850
ug/L
5 9056A Total/NA
Sulfate
140000
4000
2000
1900
ug/L
20 9056A Total/NA
Alkalinity
220000
5000
5000
3700
ug/L
1 SM 2320B Total/NA
Total Dissolved Solids
530000
10000
10000
4300
ug/L
1 SM 2540C Total/NA
Client Sample ID: MW11D(i)
Lab Sample ID: 500-143858-31
Analyte Result Qualifier
RL
LOD
MDL
Unit
Dil Fac
D Method
Prep Type
Acetone 4.6 J cn
5.0
2.5
1.7
ug/L
1
8260B
Total/NA
PCB-1260 1.1
0.40
0.20
0.069
ug/L
1
8082A
Total/NA
Arsenic 2.7
1.0
0.50
0.23
ug/L
1
6020B
Total
Recoverable
Barium 51
2.5
1.3
0.73
ug/L
1
6020B
Total
Recoverable
Chromium 11
5.0
2.5
1.1
ug/L
1
6020B
Total
Recoverable
Copper 2.4
2.0
1.0
0.50
ug/L
1
6020B
Total
Recoverable
This Detection Summary does not include radiochemical test results.
Page 15 of 258
TestAmerica Chicago
7/5/2018

Detection Summary
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
SDG:
TestAmerica Job ID: 500-143858-1
NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW11 D(i) (Continued)
Lab Sample ID: 500-143858-31
Analyte Result Qualifier
RL
LOD
MDL
Unit
Dil Fac D Method Prep Type
Manganese 24
2.5
1.3
0.79
ug/L
1 6020B Total
Recoverable
Nickel 2.6
2.0
1.0
0.63
ug/L
1 6020B Total
Recoverable
Selenium 1.5 J
2.5
1.3
0.98
ug/L
1 6020B Total
Recoverable
Vanadium 10
5.0
2.5
2.2
ug/L
1 6020B Total
Recoverable
Zinc 8.1 J
10
20
6.9
ug/L
1 6020E Total
Recoverable
Chloride 7100
400
340
340
ug/L
2 9056A Total/NA
Sulfate 180000
4000
2000
1900
ug/L
20 9056A Total/NA
Alkalinity 63000
5000
5000
3700
ug/L
1 SM 2320B Total/NA
Total Dissolved Solids 390000
10000
10000
4300
ug/L
1 SM 2540C Total/NA
F
This Detection Summary does not include radiochemical test results.
TestAmerica Chicago
Page 16 of 258
7/5/2018

Method Summary
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID:
500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ Solid Waste Facility
= # 60-13
Laboratory
Method Method Description
Protocol
8260B Volatile Organic Compounds (GC/MS)
SW846
TAL CHI
8270D Semivolatile Organic Compounds (GC/MS)
SW846
TAL CHI
8081B Organochlorine Pesticides (GC)
SW846
TAL CHI
8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography
SW846
TAL CHI
8151A Herbicides (GC)
SW846
TAL CHI
6020B Metals (ICP/MS)
SW846
TAL CHI
7470A Mercury (CVAA)
SW846
TAL CHI
9014 Cyanide
SW846
TAL CHI
9056A Anions, Ion Chromatography
SW846
TAL CHI
SM 2320B Alkalinity
SM
TAL CHI
SM 2540C Solids, Total Dissolved (TDS)
SM
TAL CHI
3005A Preparation, Total Recoverable or Dissolved Metals
SW846
TAL CHI
3510C Liquid -Liquid Extraction (Separatory Funnel)
SW846
TAL CHI
5030B Purge and Trap
SW846
TAL CHI
7470A Preparation, Mercury
SW846
TAL CHI
8151A Extraction (Herbicides)
SW846
TAL CHI
9010B Cyanide, Distillation
SW846
TAL CHI
Protocol References:
SM = "Standard Methods For The Examination Of Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods",
Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
TestAmerica Chicago
Page 17 of 258 7/5/2018

Sample Summary
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North
Mecklenburg Landfill - Infill
SDG:
NCDEQ Solid Waste Facility
= # 60-13
Lab Sample ID
Client Sample ID
Matrix
Collected
Received
500-143858-1
MW-12(i)
Water
04/11/1815:40
04/14/18 12:55
500-143858-2
MW-14(i)
Water
04/12/1814:10
04/14/18 12:55
500-143858-3
MW-15(i)
Water
04/11/18 09:55
04/14/18 12:55
500-143858-4
MW-16(i)
Water
04/12/1810:05
04/14/18 12:55
500-143858-5
MW-1(i)
Water
04/11/1816:15
04/14/18 1 2:55
500-143858-6
MW-13(i)
Water
04/11/1812:20
04/14/18 12:55
500-143858-7
MW-12D(i)
Water
04/11/1814:40
04/14/18 12:55
500-143858-8
MW-8D(i)
Water
04/11/1814:35
04/14/18 12:55
500-143858-9
MW-5(i)
Water
04/11/1811:40
04/14/18 1 2:55
500-143858-10
MW-9(i)
Water
04/10/1814:10
04/14/18 12:55
500-143858-11
MW-9D(i)
Water
04/10/1813:30
04/14/18 1 2:55
500-143858-12
MW-10(i)
Water
04/11/1810:50
04/14/18 12:55
500-143858-13
MW-8(i)
Water
04/10/1815:15
04/14/18 12:55
500-143858-14
MW-2(i)
Water
04/12/1810:10
04/14/18 12:55
500-143858-15
MW-3(i)
Water
04/12/1811:00
04/14/18 12:55
500-143858-16
MW-4D(i)
Water
04/12/1812:45
04/14/18 12:55
500-143858-17
MW-4(i)
Water
04/12/1814:10
04/14/18 12:55
500-143858-18
MW-6(i)
Water
04/11/1812:20
04/14/18 12:55
500-143858-19
MW-7D(i)
Water
04/11/18 09:30
04/14/18 12:55
500-143858-20
MW-5D(i)
Water
04/11/1811:10
04/14/18 1 2:55
500-143858-21
MW-7(i)
Water
04/11/1810:10
04/14/18 12:55
500-143858-22
Duplicate
Water
04/10/18 00:00
04/14/18 12:55
500-143858-23
Duplicate 1
Water
04/11/18 00:00
04/14/18 12:55
500-143858-24
Duplicate 2
Water
04/12/18 00:00
04/14/18 12:55
500-143858-25
TB
Water
04/10/18 00:00
04/14/18 12:55
500-143858-26
TB
Water
04/10/18 00:00
04/14/18 12:55
500-143858-27
TB
Water
04/10/18 00:00
04/14/18 12:55
500-143858-28
TB
Water
04/10/18 00:00
04/14/18 12:55
500-143858-29
TB
Water
04/10/18 00:00
04/14/18 12:55
500-143858-30
MW11(i)
Water
04/12/1812:50
04/18/1809:10
500-143858-31
MW11 D(i)
Water
04/12/18 12:00
04/18/18 09:10
TestAmerica Chicago
Page 18 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-12(i) Lab Sample ID: 500-143858-1
Date Collected: 04/11/18 15:40 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/23/18 14:47
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/23/18 14:47
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/23/18 14:47
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/23/18 14:47
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 14:47
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 14:47
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/23/18 14:47
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 14:47
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/23/18 14:47
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/23/18 14:47
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 14:47
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/23/18 14:47
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 14:47
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 14:47
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/23/18 14:47
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/23/18 14:47
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 14:47
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/23/18 14:47
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/23/18 14:47
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/23/18 14:47
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/23/18 14:47
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/23/18 14:47
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/23/18 14:47
1
Acetone
6.2 cn
5.0
2.5
1.7
ug/L
04/23/18 14:47
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/23/18 14:47
1
Acrolein
<23
100
50
23
ug/L
04/23/18 14:47
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/23/18 14:47
1
Benzene
0.54
0.50
0.25
0.15
ug/L
04/23/18 14:47
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 14:47
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/23/18 14:47
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/23/18 14:47
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/23/18 14:47
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/23/18 14:47
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/23/18 14:47
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 14:47
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/23/18 14:47
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/23/18 14:47
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/23/18 14:47
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/23/18 14:47
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/23/18 14:47
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/23/18 14:47
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/23/18 14:47
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/23/18 14:47
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/23/18 14:47
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/23/18 14:47
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/23/18 14:47
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/23/18 14:47
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/23/18 14:47
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/23/18 14:47
1
TestAmerica Chicago
Page 19 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-12(i)
Lab Sample ID: 500-143858-1
Date Collected: 04/11/18 15:40
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/23/18 14:47
1
Methylene Chloride
4.0 J cn
5.0
2.5
1.6
ug/L
04/23/18 14:47
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/23/18 14:47
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 14:47
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/23/18 14:47
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/23/18 14:47
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 14:47
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/23/18 14:47
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 14:47
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/23/18 14:47
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/23/18 14:47
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 14:47
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/23/18 14:47
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/23/18 14:47
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/23/18 14:47
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 109 75- 126
4-Bromofluorobenzene (Surr) 90 72 - 124
Dibromofluoromethane 93 75 - 120
Toluene-d8 (Surr) 94 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04123118 14:47
04123118 14:47
04123118 14:47
04/23/18 14:47
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.23
0.75
0.37
0.23
ug/L
04/17/18 22:46
1
Acenaphthylene
<0.20
0.75
0.37
0.20
ug/L
04/17/18 22:46
1
Acetophenone
<0.50
3.7
1.9
0.50
ug/L
04/17/18 22:46
1
2-Acetylaminofluorene
<1.6
7.5
3.7
1.6
ug/L
04/17/18 22:46
1
4-Aminobiphenyl
<2.8
7.5
3.7
2.8
ug/L
04/17/18 22:46
1
Anthracene
<0.25
0.75
0.37
0.25
ug/L
04/17/18 22:46
1
Benzo[a]anthracene
<0.042
0.15
0.075
0.042
ug/L
04/17/18 22:46
1
Benzo[a]pyrene
<0.074
0.15
0.075
0.074
ug/L
04/17/18 22:46
1
Benzo[b]fluoranthene
<0.060
0.15
0.075
0.060
ug/L
04/17/18 22:46
1
Benzo[g,h,i]perylene
<0.28
0.75
0.37
0.28
ug/L
04/17/18 22:46
1
Benzo[k]fluoranthene
<0.048
0.15
0.075
0.048
ug/L
04/17/18 22:46
1
Benzyl alcohol
<4.5
15
7.5
4.5
ug/L
04/17/18 22:46
1
Bis(2-chloroethoxy)methane
<0.21
1.5
0.75
0.21
ug/L
04/17/18 22:46
1
Bis(2-chloroethyl)ether
<0.22
1.5
0.75
0.22
ug/L
04/17/18 22:46
1
Bis(2-ethylhexyl) phthalate
<1.3
7.5
3.7
1.3
ug/L
04/17/18 22:46
1
4-Bromophenyl phenyl ether
<0.40
3.7
1.9
0.40
ug/L
04/17/18 22:46
1
Butyl benzyl phthalate
<0.36
1.5
0.75
0.36
ug/L
04/17/18 22:46
1
4-Chloroaniline
<1.5
7.5
3.7
1.5
ug/L
04/17/18 22:46
1
Chlorobenzilate
<2.5
7.5
3.7
2.5
ug/L
04/17/18 22:46
1
4-Chloro-3-methylphenol
<1.7
7.5
3.7
1.7
ug/L
04/17/18 22:46
1
2-Chloronaphthalene
<0.18
1.5
0.75
0.18
ug/L
04/17/18 22:46
1
2-Chlorophenol
<0.42
3.7
1.9
0.42
ug/L
04/17/18 22:46
1
4-Chlorophenyl phenyl ether
<0.48
3.7
1.9
0.48
ug/L
04/17/18 22:46
1
Chrysene
<0.051
0.15
0.075
0.051
ug/L
04/17/18 22:46
1
Diallate
<4.1
7.5
4.7
4.1
ug/L
04/17/18 22:46
1
Dibenz(a,h)anthracene
<0.038
0.22
0.11
0.038
ug/L
04/17/18 22:46
1
TestAmerica Chicago
Page 20 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-12(i) Lab Sample ID: 500-143858-1
Date Collected: 04/11/18 15:40 Matrix: Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.20
1.5
0.75
0.20
ug/L
04/17/18 22:46
1
3,3'-Dichlorobenzidine
<1.3
3.7
1.9
1.3
ug/L
04/17/18 22:46
1
2,4-Dichlorophenol
<1.9
7.5
3.7
1.9
ug/L
04/17/18 22:46
1
2,6-Dichlorophenol
<2.6
7.5
3.7
2.6
ug/L
04/17/18 22:46
1
Diethyl phthalate
<0.27
3.7
1.5
0.27
ug/L
04/17/18 22:46
1
Dimethoate
<1.4
7.5
3.7
1.4
ug/L
04/17/18 22:46
1
7,12-Dimethylbenz(a)anthracene
<2.3
30
15
2.3
ug/L
04/17/18 22:46
1
3,3'-Dimethylbenzidine
<13
30
15
13
ug/L
04/17/18 22:46
1
2,4-Dimethylphenol
<1.3
7.5
3.7
1.3
ug/L
04/17/18 22:46
1
Dimethyl phthalate
<0.24
3.7
1.5
0.24
ug/L
04/17/18 22:46
1
Di-n-butyl phthalate
<0.55
3.7
1.9
0.55
ug/L
04/17/18 22:46
1
4,6-Dinitro-2-methylphenol
<4.4
15
7.5
4.4
ug/L
04/17/18 22:46
1
2,4-Dinitrophenol
<6.4
15
7.5
6.4
ug/L
04/17/18 22:46
1
2,4-Dinitrotoluene
<0.18
0.75
0.37
0.18
ug/L
04/17/18 22:46
1
2,6-Dinitrotoluene
<0.055
0.75
0.37
0.055
ug/L
04/17/18 22:46
1
Di-n-octyl phthalate
<0.79
7.5
3.7
0.79
ug/L
04/17/18 22:46
1
Diphenylamine
<1.9
7.5
3.7
1.9
ug/L
04/17/18 22:46
1
Disulfoton
<1.4
7.5
3.7
1.4
ug/L
04/17/18 22:46
1
Ethyl methanesulfonate
<2.8
15
7.5
2.8
ug/L
04/17/18 22:46
1
Ethyl Parathion
<1.6
7.5
3.7
1.6
ug/L
04/17/18 22:46
1
Famphur
<23
30
23
23
ug/L
04/17/18 22:46
1
Fluoranthene
<0.34
0.75
0.37
0.34
ug/L
04/17/18 22:46
1
Fluorene
<0.18
0.75
0.37
0.18
ug/L
04/17/18 22:46
1
Hexachlorobenzene
<0.060
0.37
0.19
0.060
ug/L
04/17/18 22:46
1
Hexachlorocyclopentadiene
<4.8
15
7.5
4.8
ug/L
04/17/18 22:46
1
Hexachloroethane
<0.45
3.7
1.9
0.45
ug/L
04/17/18 22:46
1
Hexachloropropene
<3.5
15
7.5
3.5
ug/L
04/17/18 22:46
1
Indeno[1,2,3-cd]pyrene
<0.056
0.15
0.075
0.056
ug/L
04/17/18 22:46
1
Isodrin
<5.2
15
7.5
5.2
ug/L
04/17/18 22:46
1
Isophorone
<0.28
1.5
0.75
0.28
ug/L
04/17/18 22:46
1
Isosafrole
<2.9
7.5
3.7
2.9
ug/L
04/17/18 22:46
1
Kepone
<1.2
7.5
3.7
1.2
ug/L
04/17/18 22:46
1
m-Dinitrobenzene
<0.99
3.7
1.9
0.99
ug/L
04/17/18 22:46
1
Methapyrilene
<7.6
30
15
7.6
ug/L
04/17/18 22:46
1
3-Methylcholanthrene
<1.7
7.5
3.7
1.7
ug/L
04/17/18 22:46
1
Methyl methanesulfonate
<4.5
30
15
4.5
ug/L
04/17/18 22:46
1
2-Methylnaphthalene
<0.049
1.5
0.75
0.049
ug/L
04/17/18 22:46
1
Methyl parathion
<1.7
7.5
3.7
1.7
ug/L
04/17/18 22:46
1
2-Methylphenol
<0.23
1.5
0.75
0.23
ug/L
04/17/18 22:46
1
3 & 4 Methylphenol
<0.34
1.5
0.75
0.34
ug/L
04/17/18 22:46
1
Naphthalene
<0.23
0.75
0.37
0.23
ug/L
04/17/18 22:46
1
1,4-Naphthoquinone
<29
30
30
29
ug/L
04/17/18 22:46
1
1-Naphthylamine
<4.4
15
7.5
4.4
ug/L
04/17/18 22:46
1
2-Naphthylamine
<6.8
15
7.5
6.8
ug/L
04/17/18 22:46
1
2-Nitroaniline
<0.97
3.7
1.9
0.97
ug/L
04/17/18 22:46
1
3-Nitroaniline
<1.3
7.5
3.7
1.3
ug/L
04/17/18 22:46
1
4-Nitroaniline
<1.2
7.5
3.7
1.2
ug/L
04/17/18 22:46
1
Nitrobenzene
<0.34
0.75
0.37
0.34
ug/L
04/17/18 22:46
1
5-Nitro-o-toluidine
<2.3
7.5
3.7
2.3
ug/L
04/17/18 22:46
1
TestAmerica Chicago
Page 21 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-12(i)
Lab Sample
ID: 500-143858-1
Date Collected: 04/11/18 15:40
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<1.9
7.5
3.7
1.9
ug/L
04/17/18 22:46
1
4-Nitrophenol
<5.6
15
7.5
5.6
ug/L
04/17/18 22:46
1
N-Nitrosodiethylamine
<6.4
15
7.5
6.4
ug/L
04/17/18 22:46
1
N-Nitrosodimethylamine
<3.6
7.5
3.7
3.6
ug/L
04/17/18 22:46
1
N-Nitrosodi-n-butylamine
<3.1
7.5
3.7
3.1
ug/L
04/17/18 22:46
1
N-Nitrosodi-n-propylamine
<0.12
0.37
0.19
0.12
ug/L
04/17/18 22:46
1
N-Nitrosodiphenylamine
<0.28
1.5
0.75
0.28
ug/L
04/17/18 22:46
1
N-Nitrosomethylethylamine
<5.6
15
7.5
5.6
ug/L
04/17/18 22:46
1
N-Nitrosopiperidine
<2.6
7.5
3.7
2.6
ug/L
04/17/18 22:46
1
N-Nitrosopyrrolidine
<2.5
7.5
3.7
2.5
ug/L
04/17/18 22:46
1
o,o',o"-Triethylphosphorothioate
<4.1
15
7.5
4.1
ug/L
04/17/18 22:46
1
o-Toluidine
<5.9
30
15
5.9
ug/L
04/17/18 22:46
1
2,2'-oxybis[l-chloropropane]
<0.28
1.5
0.75
0.28
ug/L
04/17/18 22:46
1
p-Dimethylamino azobenzene
<2.2
7.5
3.7
2.2
ug/L
04/17/18 22:46
1
Pentachlorobenzene
<2.1
7.5
3.7
2.1
ug/L
04/17/18 22:46
1
Pentachloronitrobenzene
<2.7
7.5
3.7
2.7
ug/L
04/17/18 22:46
1
Phenacetin
<1.7
7.5
3.7
1.7
ug/L
04/17/18 22:46
1
Phenanthrene
<0.23
0.75
0.37
0.23
ug/L
04/17/18 22:46
1
Phenol
<0.50
3.7
1.9
0.50
ug/L
04/17/18 22:46
1
Phorate
<1.6
7.5
3.7
1.6
ug/L
04/17/18 22:46
1
p-Phenylene diamine
<12
60
30
12
ug/L
04/17/18 22:46
1
Pronamide
<1.6
7.5
7.5
1.6
ug/L
04/17/18 22:46
1
Pyrene
<0.32
0.75
0.37
0.32
ug/L
04/17/18 22:46
1
Safrole
<3.0
7.5
3.7
3.0
ug/L
04/17/18 22:46
1
sym-Trinitrobenzene
<1.4
7.5
3.7
1.4
ug/L
04/17/18 22:46
1
2,3,7,8-TCDD (Screen)
<7.5
7.5
7.5
7.5
ug/L
04/17/18 22:46
1
1,2,4,5-Tetrachlorobenzene
<0.43
3.7
1.9
0.43
ug/L
04/17/18 22:46
1
2,3,4,6-Tetrachlorophenol
<0.56
3.7
1.9
0.56
ug/L
04/17/18 22:46
1
Thionazin
<1.9
7.5
3.7
1.9
ug/L
04/17/18 22:46
1
2,4,5-Trichlorophenol
<1.9
7.5
3.7
1.9
ug/L
04/17/18 22:46
1
2,4,6-Trichlorophenol
<0.54
3.7
1.9
0.54
ug/L
04/17/18 22:46
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
86
34 - 110
04116118 16:56
04117118 22:46
1
2-Fluorophenol
65
27- 110
04116118 16:56
04117118 22:46
1
Nitrobenzene-d5
92
36 - 120
04116118 16:56
04117118 22:46
1
Phenol-d5
60
20 - 100
04116118 16:56
04117118 22:46
1
Terphenyl-d14
94
40- 145
04116118 16:56
04117118 22:46
1
2,4,6-Tribromophenol
103
40- 145
04116118 16:56
04117118 22:46
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
alpha-BHC
<0.0024
0.037
0.019
0.0024
ug/L
04/19/18 16:54
1
beta-BHC
<0.0094
0.037
0.019
0.0094
ug/L
04/19/18 16:54
1
delta-BHC
<0.0095
0.037
0.019
0.0095
ug/L
04/19/18 16:54
1
gamma-BHC (Lindane)
<0.0052
0.037
0.019
0.0052
ug/L
04/19/18 16:54
1
Heptachlor
<0.013
0.037
0.019
0.013
ug/L
04/19/18 16:54
1
Aldrin
<0.0049
0.037
0.019
0.0049
ug/L
04/19/18 16:54
1
Heptachlor epoxide
<0.013
0.037
0.019
0.013
ug/L
04/19/18 16:54
1
Endosulfan 1
<0.0038
0.037
0.019
0.0038
ug/L
04/19/18 16:54
1
TestAmerica Chicago
Page 22 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-12(i)
Lab Sample
ID: 500-143858-1
Date Collected: 04/11/18 15:40
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.012
0.037
0.019
0.012
ug/L
04/19/18 16:54
1
4,4'-DDE
<0.0035
0.037
0.019
0.0035
ug/L
04/19/18 16:54
1
Endrin
<0.013
0.037
0.019
0.013
ug/L
04/19/18 16:54
1
Endosulfan II
<0.0026
0.037
0.019
0.0026
ug/L
04/19/18 16:54
1
4,4'-DDD
<0.012
0.037
0.019
0.012
ug/L
04/19/18 16:54
1
Endosulfan sulfate
<0.011
0.037
0.019
0.011
ug/L
04/19/18 16:54
1
4,4'-DDT
<0.0030
0.037
0.019
0.0030
ug/L
04/19/18 16:54
1
Methoxychlor
<0.021
0.074
0.037
0.021
ug/L
04/19/18 16:54
1
Toxaphene
<0.19
0.37
0.19
0.19
ug/L
04/19/18 16:54
1
Endrin aldehyde
<0.0076
0.037
0.019
0.0076
ug/L
04/19/18 16:54
1
Chlordane (technical)
<0.037
0.074
0.037
0.037
ug/L
04/19/18 16:54
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
94
30 - 130
04117118 07:38
04119118 16:54
1
Tetrachloro-m-xylene
82
30 - 120
04117118 07:38
04119118 16:54
1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.062
0.37
0.19
0.062
ug/L
04/17/18 18:12
1
PCB-1221
<0.19
0.37
0.19
0.19
ug/L
04/17/18 18:12
1
PCB-1232
<0.19
0.37
0.19
0.19
ug/L
04/17/18 18:12
1
PCB-1242
<0.19
0.37
0.19
0.19
ug/L
04/17/18 18:12
1
PCB-1248
<0.19
0.37
0.19
0.19
ug/L
04/17/18 18:12
1
PCB-1254
<0.19
0.37
0.19
0.19
ug/L
04/17/18 18:12
1
PCB-1260
<0.065
0.37
0.19
0.065
ug/L
04/17/18 18:12
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
63
30 - 120
04117118 07:38
04117118 18:12
1
DCB Decachlorobiphenyl
89
30 - 140
04117118 07:38
04117118 18:12
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.44
0.95
0.48
0.44
ug/L
04/17/18 22:56
1
Dinoseb
<0.16
1.9
0.95
0.16
ug/L
04/17/18 22:56
1
Pentachlorophenol
<0.086
0.48
0.095
0.086
ug/L
04/17/18 22:56
1
Silvex (2,4,5-TP)
<0.28
0.95
0.48
0.28
ug/L
04/17/18 22:56
1
2,4,5-T
<0.41
0.95
0.48
0.41
ug/L
04/17/18 22:56
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
89
25 - 130
04117118 09:02
04117118 22:56
1
Method: 6020B - Metals (ICP/MS) - Total Recoverable
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 02:42
1
Arsenic
0.39 J
1.0
0.50
0.23
ug/L
04/21/18 02:42
1
Barium
240
2.5
1.3
0.73
ug/L
04/21/18 02:42
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 02:42
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 02:42
1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 02:42
1
Cobalt
6.4
1.0
0.50
0.40
ug/L
04/21/18 02:42
1
Copper
0.84 J B
2.0
1.0
0.50
ug/L
04/21/18 02:42
1
TestAmerica Chicago
Page 23 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-12(i) Lab Sample ID: 500-143858-1
Date Collected: 04/11/18 15:40 Matrix: Water
Date Received: 04/14/18 12:55
Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Iron
240
100
50
47
ug/L
04/21/18 02:42
1
Lead
<0.19
0.50
0.25
0.19
ug/L
04/21/18 02:42
1
Manganese
310
2.5
1.3
0.79
ug/L
04/21/18 02:42
1
Nickel
9.7
2.0
1.0
0.63
ug/L
04/21/18 02:42
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 02:42
1
Silver
0.19 J
0.50
0.25
0.12
ug/L
04/21/18 02:42
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 02:42
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 02:42
1
Vanadium
<2.2
5.0
2.5
2.2
ug/L
04/21/18 02:42
1
Zinc
<6.9
10
20
6.9
ug/L
04/21/18 02:42
1
Method: 6020B - Metals (ICP/MS) - Dissolved
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
D
Analyzed
Dil Fac
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 04:35
1
Arsenic
0.48
J
1.0
0.50
0.23
ug/L
04/21/18 04:35
1
Barium
220
2.5
1.3
0.73
ug/L
04/21/18 04:35
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 04:35
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 04:35
1
Cobalt
6.1
1.0
0.50
0.40
ug/L
04/21/18 04:35
1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 04:35
1
Copper
5.0
2.0
1.0
0.50
ug/L
04/21/18 04:35
1
Iron
200
100
50
47
ug/L
04/21/18 04:35
1
Manganese
300
2.5
1.3
0.79
ug/L
04/21/18 04:35
1
Nickel
9.4
2.0
1.0
0.63
ug/L
04/21/18 04:35
1
Lead
0.35
J
0.50
0.25
0.19
ug/L
04/21/18 04:35
1
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 04:35
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 04:35
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 04:35
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 04:35
1
Vanadium
<2.2
5.0
2.5
2.2
ug/L
04/21/18 04:35
1
Zinc
7.2
J
10
20
6.9
ug/L
04/21/18 04:35
1
Method: 7470A - Mercury (CVAA)
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
D
Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/18/1810:44
1
Method: 7470A - Mercury (CVAA) -
Dissolved
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
D
Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/20/18 09:55
1
General Chemistry
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
D
Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/24/18 15:55
1
Chloride
37000
F1
2000
1700
1700
ug/L
04/27/1812:52
10
Sulfate
67000
B F1
2000
1000
950
ug/L
04/26/18 20:48
10
Alkalinity
440000
5000
5000
3700
ug/L
04/23/1815:26
1
Total Dissolved Solids
710000
10000
10000
4300
ug/L
04/17/18 07:45
1
TestAmerica Chicago
Page 24 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-14(i) Lab Sample ID: 500-143858-2
Date Collected: 04/12/18 14:10 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/23/18 15:15
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/23/18 15:15
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/23/18 15:15
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/23/18 15:15
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 15:15
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 15:15
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/23/18 15:15
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 15:15
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/23/18 15:15
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/23/18 15:15
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 15:15
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/23/18 15:15
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 15:15
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 15:15
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/23/18 15:15
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/23/18 15:15
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 15:15
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/23/18 15:15
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/23/18 15:15
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/23/18 15:15
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/23/18 15:15
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/23/18 15:15
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/23/18 15:15
1
Acetone
4.2 J cn
5.0
2.5
1.7
ug/L
04/23/18 15:15
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/23/18 15:15
1
Acrolein
<23
100
50
23
ug/L
04/23/18 15:15
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/23/18 15:15
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 15:15
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 15:15
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/23/18 15:15
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/23/18 15:15
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/23/18 15:15
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/23/18 15:15
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/23/18 15:15
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 15:15
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/23/18 15:15
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/23/18 15:15
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/23/18 15:15
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/23/18 15:15
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/23/18 15:15
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/23/18 15:15
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/23/18 15:15
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/23/18 15:15
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/23/18 15:15
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/23/18 15:15
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/23/18 15:15
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/23/18 15:15
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/23/18 15:15
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/23/18 15:15
1
TestAmerica Chicago
Page 25 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-14(i)
Lab Sample ID: 500-143858-2
Date Collected: 04/12/18 14:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/23/18 15:15
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/23/18 15:15
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/23/18 15:15
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 15:15
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/23/18 15:15
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/23/18 15:15
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 15:15
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/23/18 15:15
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 15:15
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/23/18 15:15
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/23/18 15:15
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 15:15
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/23/18 15:15
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/23/18 15:15
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/23/18 15:15
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 110 75- 126
4-Bromofluorobenzene (Surr) 96 72 - 124
Dibromofluoromethane 93 75 - 120
Toluene-d8 (Surr) 96 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04123118 15:15
04123118 15:15
04123118 15:15
04/23/18 15:15
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.24
0.78
0.39
0.24
ug/L
04/17/18 23:15
1
Acenaphthylene
<0.21
0.78
0.39
0.21
ug/L
04/17/18 23:15
1
Acetophenone
<0.51
3.9
1.9
0.51
ug/L
04/17/18 23:15
1
2-Acetylaminofluorene
<1.6
7.8
3.9
1.6
ug/L
04/17/18 23:15
1
4-Aminobiphenyl
<2.9
7.8
3.9
2.9
ug/L
04/17/18 23:15
1
Anthracene
<0.26
0.78
0.39
0.26
ug/L
04/17/18 23:15
1
Benzo[a]anthracene
<0.044
0.16
0.078
0.044
ug/L
04/17/18 23:15
1
Benzo[a]pyrene
<0.077
0.16
0.078
0.077
ug/L
04/17/18 23:15
1
Benzo[b]fluoranthene
<0.063
0.16
0.078
0.063
ug/L
04/17/18 23:15
1
Benzo[g,h,i]perylene
<0.29
0.78
0.39
0.29
ug/L
04/17/18 23:15
1
Benzo[k]fluoranthene
<0.050
0.16
0.078
0.050
ug/L
04/17/18 23:15
1
Benzyl alcohol
<4.7
16
7.8
4.7
ug/L
04/17/18 23:15
1
Bis(2-chloroethoxy)methane
<0.22
1.6
0.78
0.22
ug/L
04/17/18 23:15
1
Bis(2-chloroethyl)ether
<0.23
1.6
0.78
0.23
ug/L
04/17/18 23:15
1
Bis(2-ethylhexyl) phthalate
<1.3
7.8
3.9
1.3
ug/L
04/17/18 23:15
1
4-Bromophenyl phenyl ether
<0.42
3.9
1.9
0.42
ug/L
04/17/18 23:15
1
Butyl benzyl phthalate
<0.37
1.6
0.78
0.37
ug/L
04/17/18 23:15
1
4-Chloroaniline
<1.6
7.8
3.9
1.6
ug/L
04/17/18 23:15
1
Chlorobenzilate
<2.6
7.8
3.9
2.6
ug/L
04/17/18 23:15
1
4-Chloro-3-methylphenol
<1.8
7.8
3.9
1.8
ug/L
04/17/18 23:15
1
2-Chloronaphthalene
<0.18
1.6
0.78
0.18
ug/L
04/17/18 23:15
1
2-Chlorophenol
<0.43
3.9
1.9
0.43
ug/L
04/17/18 23:15
1
4-Chlorophenyl phenyl ether
<0.49
3.9
1.9
0.49
ug/L
04/17/18 23:15
1
Chrysene
<0.053
0.16
0.078
0.053
ug/L
04/17/18 23:15
1
Diallate
<4.3
7.8
4.8
4.3
ug/L
04/17/18 23:15
1
Dibenz(a,h)anthracene
<0.039
0.23
0.12
0.039
ug/L
04/17/18 23:15
1
TestAmerica Chicago
Page 26 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-14(i) Lab Sample ID: 500-143858-2
Date Collected: 04/12/18 14:10 Matrix: Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.20
1.6
0.78
0.20
ug/L
04/17/18 23:15
1
3,3'-Dichlorobenzidine
<1.3
3.9
1.9
1.3
ug/L
04/17/18 23:15
1
2,4-Dichlorophenol
<2.0
7.8
3.9
2.0
ug/L
04/17/18 23:15
1
2,6-Dichlorophenol
<2.7
7.8
3.9
2.7
ug/L
04/17/18 23:15
1
Diethyl phthalate
<0.28
3.9
1.6
0.28
ug/L
04/17/18 23:15
1
Dimethoate
<1.4
7.8
3.9
1.4
ug/L
04/17/18 23:15
1
7,12-Dimethylbenz(a)anthracene
<2.3
31
16
2.3
ug/L
04/17/18 23:15
1
3,3'-Dimethylbenzidine
<14
31
16
14
ug/L
04/17/18 23:15
1
2,4-Dimethylphenol
<1.4
7.8
3.9
1.4
ug/L
04/17/18 23:15
1
Dimethyl phthalate
<0.24
3.9
1.6
0.24
ug/L
04/17/18 23:15
1
Di-n-butyl phthalate
<0.57
3.9
1.9
0.57
ug/L
04/17/18 23:15
1
4,6-Dinitro-2-methylphenol
<4.6
16
7.8
4.6
ug/L
04/17/18 23:15
1
2,4-Dinitrophenol
<6.7
16
7.8
6.7
ug/L
04/17/18 23:15
1
2,4-Dinitrotoluene
<0.19
0.78
0.39
0.19
ug/L
04/17/18 23:15
1
2,6-Dinitrotoluene
<0.057
0.78
0.39
0.057
ug/L
04/17/18 23:15
1
Di-n-octyl phthalate
<0.81
7.8
3.9
0.81
ug/L
04/17/18 23:15
1
Diphenylamine
<2.0
7.8
3.9
2.0
ug/L
04/17/18 23:15
1
Disulfoton
<1.5
7.8
3.9
1.5
ug/L
04/17/18 23:15
1
Ethyl methanesulfonate
<2.9
16
7.8
2.9
ug/L
04/17/18 23:15
1
Ethyl Parathion
<1.6
7.8
3.9
1.6
ug/L
04/17/18 23:15
1
Famphur
<23
31
24
23
ug/L
04/17/18 23:15
1
Fluoranthene
<0.35
0.78
0.39
0.35
ug/L
04/17/18 23:15
1
Fluorene
<0.19
0.78
0.39
0.19
ug/L
04/17/18 23:15
1
Hexachlorobenzene
<0.062
0.39
0.19
0.062
ug/L
04/17/18 23:15
1
Hexachlorocyclopentadiene
<4.9
16
7.8
4.9
ug/L
04/17/18 23:15
1
Hexachloroethane
<0.46
3.9
1.9
0.46
ug/L
04/17/18 23:15
1
Hexachloropropene
<3.6
16
7.8
3.6
ug/L
04/17/18 23:15
1
Indeno[1,2,3-cd]pyrene
<0.058
0.16
0.078
0.058
ug/L
04/17/18 23:15
1
Isodrin
<5.3
16
7.8
5.3
ug/L
04/17/18 23:15
1
Isophorone
<0.29
1.6
0.78
0.29
ug/L
04/17/18 23:15
1
Isosafrole
<3.0
7.8
3.9
3.0
ug/L
04/17/18 23:15
1
Kepone
<1.3
7.8
3.9
1.3
ug/L
04/17/18 23:15
1
m-Dinitrobenzene
<1.0
3.9
1.9
1.0
ug/L
04/17/18 23:15
1
Methapyrilene
<7.9
31
16
7.9
ug/L
04/17/18 23:15
1
3-Methylcholanthrene
<1.8
7.8
3.9
1.8
ug/L
04/17/18 23:15
1
Methyl methanesulfonate
<4.6
31
16
4.6
ug/L
04/17/18 23:15
1
2-Methylnaphthalene
<0.050
1.6
0.78
0.050
ug/L
04/17/18 23:15
1
Methyl parathion
<1.8
7.8
3.9
1.8
ug/L
04/17/18 23:15
1
2-Methylphenol
<0.24
1.6
0.78
0.24
ug/L
04/17/18 23:15
1
3 & 4 Methylphenol
<0.35
1.6
0.78
0.35
ug/L
04/17/18 23:15
1
Naphthalene
<0.24
0.78
0.39
0.24
ug/L
04/17/18 23:15
1
1,4-Naphthoquinone
<30
31
31
30
ug/L
04/17/18 23:15
1
1-Naphthylamine
<4.6
16
7.8
4.6
ug/L
04/17/18 23:15
1
2-Naphthylamine
<7.1
16
7.8
7.1
ug/L
04/17/18 23:15
1
2-Nitroaniline
<1.0
3.9
1.9
1.0
ug/L
04/17/18 23:15
1
3-Nitroaniline
<1.4
7.8
3.9
1.4
ug/L
04/17/18 23:15
1
4-Nitroaniline
<1.3
7.8
3.9
1.3
ug/L
04/17/18 23:15
1
Nitrobenzene
<0.35
0.78
0.39
0.35
ug/L
04/17/18 23:15
1
5-Nitro-o-toluidine
<2.4
7.8
3.9
2.4
ug/L
04/17/18 23:15
1
TestAmerica Chicago
Page 27 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-14(i)
Lab Sample
ID: 500-143858-2
Date Collected: 04/12/18 14:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<1.9
7.8
3.9
1.9
ug/L
04/17/18 23:15
1
4-Nitrophenol
<5.8
16
7.8
5.8
ug/L
04/17/18 23:15
1
N-Nitrosodiethylamine
<6.7
16
7.8
6.7
ug/L
04/17/18 23:15
1
N-Nitrosodimethylamine
<3.7
7.8
3.9
3.7
ug/L
04/17/18 23:15
1
N-Nitrosodi-n-butylamine
<3.2
7.8
3.9
3.2
ug/L
04/17/18 23:15
1
N-Nitrosodi-n-propylamine
<0.12
0.39
0.19
0.12
ug/L
04/17/18 23:15
1
N-Nitrosodiphenylamine
<0.29
1.6
0.78
0.29
ug/L
04/17/18 23:15
1
N-Nitrosomethylethylamine
<5.8
16
7.8
5.8
ug/L
04/17/18 23:15
1
N-Nitrosopiperidine
<2.7
7.8
3.9
2.7
ug/L
04/17/18 23:15
1
N-Nitrosopyrrolidine
<2.6
7.8
3.9
2.6
ug/L
04/17/18 23:15
1
o,o',o"-Triethylphosphorothioate
<4.3
16
7.8
4.3
ug/L
04/17/18 23:15
1
o-Toluidine
<6.1
31
16
6.1
ug/L
04/17/18 23:15
1
2,2'-oxybis[l-chloropropane]
<0.29
1.6
0.78
0.29
ug/L
04/17/18 23:15
1
p-Dimethylamino azobenzene
<2.3
7.8
3.9
2.3
ug/L
04/17/18 23:15
1
Pentachlorobenzene
<2.2
7.8
3.9
2.2
ug/L
04/17/18 23:15
1
Pentachloronitrobenzene
<2.8
7.8
3.9
2.8
ug/L
04/17/18 23:15
1
Phenacetin
<1.8
7.8
3.9
1.8
ug/L
04/17/18 23:15
1
Phenanthrene
<0.23
0.78
0.39
0.23
ug/L
04/17/18 23:15
1
Phenol
<0.52
3.9
1.9
0.52
ug/L
04/17/18 23:15
1
Phorate
<1.7
7.8
3.9
1.7
ug/L
04/17/18 23:15
1
p-Phenylene diamine
<13
62
31
13
ug/L
04/17/18 23:15
1
Pronamide
<1.7
7.8
7.8
1.7
ug/L
04/17/18 23:15
1
Pyrene
<0.33
0.78
0.39
0.33
ug/L
04/17/18 23:15
1
Safrole
<3.1
7.8
3.9
3.1
ug/L
04/17/18 23:15
1
sym-Trinitrobenzene
<1.4
7.8
3.9
1.4
ug/L
04/17/18 23:15
1
2,3,7,8-TCDD (Screen)
<7.8
7.8
7.8
7.8
ug/L
04/17/18 23:15
1
1,2,4,5-Tetrachlorobenzene
<0.44
3.9
1.9
0.44
ug/L
04/17/18 23:15
1
2,3,4,6-Tetrachlorophenol
<0.58
3.9
1.9
0.58
ug/L
04/17/18 23:15
1
Thionazin
<2.0
7.8
3.9
2.0
ug/L
04/17/18 23:15
1
2,4,5-Trichlorophenol
<2.0
7.8
3.9
2.0
ug/L
04/17/18 23:15
1
2,4,6-Trichlorophenol
<0.56
3.9
1.9
0.56
ug/L
04/17/18 23:15
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
89
34 - 110
04116118 16:56
04117118 23:15
1
2-Fluorophenol
78
27- 110
04116118 16:56
04117118 23:15
1
Nitrobenzene-d5
97
36 - 120
04116118 16:56
04117118 23:15
1
Phenol-d5
57
20 - 100
04116118 16:56
04117118 23:15
1
Terphenyl-d14
96
40- 145
04116118 16:56
04117118 23:15
1
2,4,6-Tribromophenol
95
40- 145
04116118 16:56
04117118 23:15
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
alpha-BHC
<0.0024
0.038
0.019
0.0024
ug/L
04/19/18 17:13
1
beta-BHC
<0.0096
0.038
0.019
0.0096
ug/L
04/19/18 17:13
1
delta-BHC
<0.0097
0.038
0.019
0.0097
ug/L
04/19/18 17:13
1
gamma-BHC (Lindane)
<0.0053
0.038
0.019
0.0053
ug/L
04/19/18 17:13
1
Heptachlor
<0.013
0.038
0.019
0.013
ug/L
04/19/18 17:13
1
Aldrin
<0.0050
0.038
0.019
0.0050
ug/L
04/19/18 17:13
1
Heptachlor epoxide
<0.013
0.038
0.019
0.013
ug/L
04/19/18 17:13
1
Endosulfan 1
<0.0039
0.038
0.019
0.0039
ug/L
04/19/18 17:13
1
TestAmerica Chicago
Page 28 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-14(i)
Lab Sample
ID: 500-143858-2
Date Collected: 04/12/18 14:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.012
0.038
0.019
0.012
ug/L
04/19/18 17:13
1
4,4'-DDE
<0.0036
0.038
0.019
0.0036
ug/L
04/19/18 17:13
1
Endrin
<0.013
0.038
0.019
0.013
ug/L
04/19/18 17:13
1
Endosulfan II
<0.0026
0.038
0.019
0.0026
ug/L
04/19/18 17:13
1
4,4'-DDD
<0.013
0.038
0.019
0.013
ug/L
04/19/18 17:13
1
Endosulfan sulfate
<0.011
0.038
0.019
0.011
ug/L
04/19/18 17:13
1
4,4'-DDT
<0.0030
0.038
0.019
0.0030
ug/L
04/19/18 17:13
1
Methoxychlor
<0.022
0.075
0.038
0.022
ug/L
04/19/18 17:13
1
Toxaphene
<0.19
0.38
0.19
0.19
ug/L
04/19/18 17:13
1
Endrin aldehyde
<0.0077
0.038
0.019
0.0077
ug/L
04/19/18 17:13
1
Chlordane (technical)
<0.038
0.075
0.038
0.038
ug/L
04/19/18 17:13
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
79
30 - 130
04117118 07:38
04119118 17:13
1
Tetrachloro-m-xylene
65
30 - 120
04117118 07:38
04119118 17:13
1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.063
0.38
0.19
0.063
ug/L
04/17/18 18:28
1
PCB-1221
<0.19
0.38
0.19
0.19
ug/L
04/17/18 18:28
1
PCB-1232
<0.19
0.38
0.19
0.19
ug/L
04/17/18 18:28
1
PCB-1242
<0.19
0.38
0.19
0.19
ug/L
04/17/18 18:28
1
PCB-1248
<0.19
0.38
0.19
0.19
ug/L
04/17/18 18:28
1
PCB-1254
<0.19
0.38
0.19
0.19
ug/L
04/17/18 18:28
1
PCB-1260
<0.066
0.38
0.19
0.066
ug/L
04/17/18 18:28
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
65
30 - 120
04117118 07:38
04117118 18:28
1
DCB Decachlorobiphenyl
86
30 - 140
04117118 07:38
04117118 18:28
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.45
0.96
0.48
0.45
ug/L
04/17/18 23:20
1
Dinoseb
<0.16
1.9
0.96
0.16
ug/L
04/17/18 23:20
1
Pentachlorophenol
<0.086
0.48
0.096
0.086
ug/L
04/17/18 23:20
1
Silvex (2,4,5-TP)
<0.28
0.96
0.48
0.28
ug/L
04/17/18 23:20
1
2,4,5-T
<0.42
0.96
0.48
0.42
ug/L
04/17/18 23:20
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
73
25 - 130
04117118 09:02
04117118 23:20
1
Method: 6020B - Metals (ICP/MS) - Total Recoverable
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 02:46
1
Arsenic
0.34 J
1.0
0.50
0.23
ug/L
04/21/18 02:46
1
Barium
24
2.5
1.3
0.73
ug/L
04/21/18 02:46
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 02:46
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 02:46
1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 02:46
1
Cobalt
<0.40
1.0
0.50
0.40
ug/L
04/21/18 02:46
1
Copper
1.5 J B
2.0
1.0
0.50
ug/L
04/21/18 02:46
1
TestAmerica Chicago
Page 29 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-14(i) Lab Sample ID: 500-143858-2
Date Collected: 04/12/18 14:10 Matrix: Water
Date Received: 04/14/18 12:55
Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Iron
230
100
50
47
ug/L
04/21/18 02:46
1
Lead
<0.19
0.50
0.25
0.19
ug/L
04/21/18 02:46
1
Manganese
17
2.5
1.3
0.79
ug/L
04/21/18 02:46
1
Nickel
<0.63
2.0
1.0
0.63
ug/L
04/21/18 02:46
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 02:46
1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 02:46
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 02:46
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 02:46
1
Vanadium
3.2 J
5.0
2.5
2.2
ug/L
04/21/18 02:46
1
Zinc
<6.9
10
20
6.9
ug/L
04/21/18 02:46
1
Method: 6020B - Metals (ICP/MS) - Dissolved
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
D
Analyzed
Dil Fac
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 04:54
1
Arsenic
0.25
J
1.0
0.50
0.23
ug/L
04/21/18 04:54
1
Barium
22
2.5
1.3
0.73
ug/L
04/21/18 04:54
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 04:54
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 04:54
1
Cobalt
<0.40
1.0
0.50
0.40
ug/L
04/21/18 04:54
1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 04:54
1
Copper
10
2.0
1.0
0.50
ug/L
04/21/18 04:54
1
Iron
<47
100
50
47
ug/L
04/21/18 04:54
1
Manganese
4.5
2.5
1.3
0.79
ug/L
04/21/18 04:54
1
Nickel
<0.63
2.0
1.0
0.63
ug/L
04/21/18 04:54
1
Lead
1.5
0.50
0.25
0.19
ug/L
04/21/18 04:54
1
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 04:54
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 04:54
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 04:54
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 04:54
1
Vanadium
2.6
J
5.0
2.5
2.2
ug/L
04/21/18 04:54
1
Zinc
16
10
20
6.9
ug/L
04/21/18 04:54
1
Method: 7470A - Mercury (CVAA)
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
D
Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/18/1810:51
1
Method: 7470A - Mercury (CVAA) - Dissolved
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
D
Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/20/18 09:57
1
General Chemistry
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
D
Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/25/18 09:55
1
Chloride
5700
400
340
340
ug/L
04/27/1813:29
2
Sulfate
9300
B
400
200
190
ug/L
04/26/18 21:50
2
Alkalinity
61000
5000
5000
3700
ug/L
04/24/1814:17
1
Total Dissolved Solids
120000
10000
10000
4300
ug/L
04/17/18 07:50
1
TestAmerica Chicago
Page 30 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-15(i) Lab Sample ID: 500-143858-3
Date Collected: 04/11/18 09:55 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/23/18 15:44
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/23/18 15:44
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/23/18 15:44
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/23/18 15:44
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 15:44
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 15:44
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/23/18 15:44
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 15:44
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/23/18 15:44
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/23/18 15:44
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 15:44
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/23/18 15:44
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 15:44
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 15:44
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/23/18 15:44
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/23/18 15:44
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 15:44
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/23/18 15:44
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/23/18 15:44
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/23/18 15:44
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/23/18 15:44
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/23/18 15:44
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/23/18 15:44
1
Acetone
<1.7
5.0
2.5
1.7
ug/L
04/23/18 15:44
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/23/18 15:44
1
Acrolein
<23
100
50
23
ug/L
04/23/18 15:44
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/23/18 15:44
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 15:44
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 15:44
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/23/18 15:44
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/23/18 15:44
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/23/18 15:44
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/23/18 15:44
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/23/18 15:44
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 15:44
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/23/18 15:44
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/23/18 15:44
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/23/18 15:44
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/23/18 15:44
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/23/18 15:44
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/23/18 15:44
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/23/18 15:44
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/23/18 15:44
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/23/18 15:44
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/23/18 15:44
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/23/18 15:44
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/23/18 15:44
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/23/18 15:44
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/23/18 15:44
1
TestAmerica Chicago
Page 31 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-15(i)
Lab Sample
ID: 500-143858-3
Date Collected: 04/11/18 09:55
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic
Compounds (GC/MS)
(Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/23/18 15:44
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/23/18 15:44
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/23/18 15:44
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 15:44
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/23/18 15:44
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/23/18 15:44
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 15:44
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/23/18 15:44
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 15:44
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/23/18 15:44
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/23/18 15:44
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 15:44
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/23/18 15:44
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/23/18 15:44
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/23/18 15:44
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
109
75- 126
04123118 15:44
1
4-Bromofluorobenzene (Surr)
91
72 - 124
04123118 15:44
1
Dibromofluoromethane
94
75 - 120
04123118 15:44
1
Toluene-d8 (Surr)
94
75 - 120
04/23/18 15:44
1
General Chemistry
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Chloride
57000
4000
3400
3400
ug/L
04/27/1814:06
20
Sulfate
24000 B
1000
500
480
ug/L
04/26/18 22:02
5
Alkalinity
300000
5000
5000
3700
ug/L
04/23/1815:42
1
Total Dissolved Solids
490000
10000
10000
4300
ug/L
04/17/18 07:53
1
TestAmerica Chicago
Page 32 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-16(i) Lab Sample ID: 500-143858-4
Date Collected: 04/12/18 10:05 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/23/18 16:13
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/23/18 16:13
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/23/18 16:13
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/23/18 16:13
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 16:13
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 16:13
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/23/18 16:13
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 16:13
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/23/18 16:13
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/23/18 16:13
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 16:13
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/23/18 16:13
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 16:13
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 16:13
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/23/18 16:13
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/23/18 16:13
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 16:13
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/23/18 16:13
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/23/18 16:13
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/23/18 16:13
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/23/18 16:13
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/23/18 16:13
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/23/18 16:13
1
Acetone
<1.7
5.0
2.5
1.7
ug/L
04/23/18 16:13
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/23/18 16:13
1
Acrolein
<23
100
50
23
ug/L
04/23/18 16:13
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/23/18 16:13
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 16:13
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 16:13
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/23/18 16:13
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/23/18 16:13
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/23/18 16:13
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/23/18 16:13
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/23/18 16:13
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 16:13
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/23/18 16:13
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/23/18 16:13
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/23/18 16:13
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/23/18 16:13
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/23/18 16:13
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/23/18 16:13
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/23/18 16:13
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/23/18 16:13
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/23/18 16:13
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/23/18 16:13
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/23/18 16:13
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/23/18 16:13
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/23/18 16:13
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/23/18 16:13
1
TestAmerica Chicago
Page 33 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-16(i)
Lab Sample ID: 500-143858-4
Date Collected: 04/12/18 10:05
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/23/18 16:13
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/23/18 16:13
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/23/18 16:13
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 16:13
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/23/18 16:13
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/23/18 16:13
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 16:13
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/23/18 16:13
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 16:13
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/23/18 16:13
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/23/18 16:13
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 16:13
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/23/18 16:13
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/23/18 16:13
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/23/18 16:13
1
Surrogate %Recovery Qualifier
1,2-Dichloroethane-d4 (Surr) 109
4-Bromofluorobenzene (Surr) 91
Dibromofluoromethane 95
Toluene-d8 (Surr) 94
Method: 6020B - Metals (ICP/MS) - Total Recoverable
Analyte Result Qualifier
Limits
75- 126
72 - 124
75 - 120
75 - 120
RL
LOD
MDL
Prepared
Unit D
Analyzed
04123118 16:13
04123118 16:13
04123118 16:13
04/23/18 16:13
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 02:50
1
Arsenic
0.68 J
1.0
0.50
0.23
ug/L
04/21/18 02:50
1
Barium
120
2.5
1.3
0.73
ug/L
04/21/18 02:50
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 02:50
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 02:50
1
Chromium
5.6 B
5.0
2.5
1.1
ug/L
04/21/18 02:50
1
Cobalt
7.9
1.0
0.50
0.40
ug/L
04/21/18 02:50
1
Copper
5.6 B
2.0
1.0
0.50
ug/L
04/21/18 02:50
1
Iron
6600
100
50
47
ug/L
04/21/18 02:50
1
Lead
1.1
0.50
0.25
0.19
ug/L
04/21/18 02:50
1
Manganese
1600
2.5
1.3
0.79
ug/L
04/21/18 02:50
1
Nickel
3.0
2.0
1.0
0.63
ug/L
04/21/18 02:50
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 02:50
1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 02:50
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 02:50
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 02:50
1
Vanadium
11
5.0
2.5
2.2
ug/L
04/21/18 02:50
1
Zinc
17 B
10
20
6.9
ug/L
04/21/18 02:50
1
Method: 7470A - Mercury (CVAA)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/18/1810:53
1
General Chemistry
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Chloride
3600
400
340
340
ug/L
04/27/1814:18
2
TestAmerica Chicago
Page 34 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-16(i) Lab Sample ID: 500-143858-4
Date Collected: 04/12/18 10:05 Matrix: Water
Date Received: 04/14/18 12:55
General Chemistry (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Sulfate
34000 B
1000
500
480
ug/L
04/26/18 22:39
5
Alkalinity
43000
5000
5000
3700
ug/L
04/24/1814:23
1
Total Dissolved Solids
120000
10000
10000
4300
ug/L
04/17/18 07:55
1
TestAmerica Chicago
Page 35 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-1(i) Lab Sample ID: 500-143858-5
Date Collected: 04/11/18 16:15 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/23/18 16:40
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/23/18 16:40
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/23/18 16:40
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/23/18 16:40
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 16:40
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 16:40
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/23/18 16:40
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 16:40
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/23/18 16:40
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/23/18 16:40
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 16:40
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/23/18 16:40
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 16:40
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 16:40
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/23/18 16:40
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/23/18 16:40
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 16:40
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/23/18 16:40
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/23/18 16:40
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/23/18 16:40
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/23/18 16:40
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/23/18 16:40
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/23/18 16:40
1
Acetone
5.9 cn
5.0
2.5
1.7
ug/L
04/23/18 16:40
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/23/18 16:40
1
Acrolein
<23
100
50
23
ug/L
04/23/18 16:40
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/23/18 16:40
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 16:40
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 16:40
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/23/18 16:40
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/23/18 16:40
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/23/18 16:40
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/23/18 16:40
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/23/18 16:40
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 16:40
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/23/18 16:40
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/23/18 16:40
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/23/18 16:40
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/23/18 16:40
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/23/18 16:40
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/23/18 16:40
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/23/18 16:40
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/23/18 16:40
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/23/18 16:40
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/23/18 16:40
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/23/18 16:40
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/23/18 16:40
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/23/18 16:40
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/23/18 16:40
1
TestAmerica Chicago
Page 36 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-1(i)
Lab Sample ID: 500-143858-5
Date Collected: 04/11/18 16:15
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/23/18 16:40
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/23/18 16:40
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/23/18 16:40
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 16:40
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/23/18 16:40
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/23/18 16:40
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 16:40
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/23/18 16:40
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 16:40
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/23/18 16:40
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/23/18 16:40
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 16:40
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/23/18 16:40
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/23/18 16:40
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/23/18 16:40
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 110 75- 126
4-Bromofluorobenzene (Surr) 92 72 - 124
Dibromofluoromethane 94 75 - 120
Toluene-d8 (Surr) 95 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04123118 16:40
04123118 16:40
04123118 16:40
04/23/18 16:40
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.25
0.80
0.40
0.25
ug/L
04/17/18 23:44
1
Acenaphthylene
<0.21
0.80
0.40
0.21
ug/L
04/17/18 23:44
1
Acetophenone
<0.53
4.0
2.0
0.53
ug/L
04/17/18 23:44
1
2-Acetylaminofluorene
<1.7
8.0
4.0
1.7
ug/L
04/17/18 23:44
1
4-Aminobiphenyl
<3.0
8.0
4.0
3.0
ug/L
04/17/18 23:44
1
Anthracene
<0.27
0.80
0.40
0.27
ug/L
04/17/18 23:44
1
Benzo[a]anthracene
<0.045
0.16
0.080
0.045
ug/L
04/17/18 23:44
1
Benzo[a]pyrene
<0.079
0.16
0.080
0.079
ug/L
04/17/18 23:44
1
Benzo[b]fluoranthene
<0.065
0.16
0.080
0.065
ug/L
04/17/18 23:44
1
Benzo[g,h,i]perylene
<0.30
0.80
0.40
0.30
ug/L
04/17/18 23:44
1
Benzo[k]fluoranthene
<0.051
0.16
0.080
0.051
ug/L
04/17/18 23:44
1
Benzyl alcohol
<4.8
16
8.0
4.8
ug/L
04/17/18 23:44
1
Bis(2-chloroethoxy)methane
<0.23
1.6
0.80
0.23
ug/L
04/17/18 23:44
1
Bis(2-chloroethyl)ether
<0.23
1.6
0.80
0.23
ug/L
04/17/18 23:44
1
Bis(2-ethylhexyl) phthalate
1.9 J
8.0
4.0
1.4
ug/L
04/17/18 23:44
1
4-Bromophenyl phenyl ether
<0.43
4.0
2.0
0.43
ug/L
04/17/18 23:44
1
Butyl benzyl phthalate
<0.39
1.6
0.80
0.39
ug/L
04/17/18 23:44
1
4-Chloroaniline
<1.6
8.0
4.0
1.6
ug/L
04/17/18 23:44
1
Chlorobenzilate
<2.7
8.0
4.0
2.7
ug/L
04/17/18 23:44
1
4-Chloro-3-methylphenol
<1.8
8.0
4.0
1.8
ug/L
04/17/18 23:44
1
2-Chloronaphthalene
<0.19
1.6
0.80
0.19
ug/L
04/17/18 23:44
1
2-Chlorophenol
<0.45
4.0
2.0
0.45
ug/L
04/17/18 23:44
1
4-Chlorophenyl phenyl ether
<0.51
4.0
2.0
0.51
ug/L
04/17/18 23:44
1
Chrysene
<0.055
0.16
0.080
0.055
ug/L
04/17/18 23:44
1
Diallate
<4.4
8.0
5.0
4.4
ug/L
04/17/18 23:44
1
Dibenz(a,h)anthracene
<0.041
0.24
0.12
0.041
ug/L
04/17/18 23:44
1
TestAmerica Chicago
Page 37 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-1(i) Lab Sample ID: 500-143858-5
Date Collected: 04/11/18 16:15 Matrix: Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.21
1.6
0.80
0.21
ug/L
04/17/18 23:44
1
3,3'-Dichlorobenzidine
<1.4
4.0
2.0
1.4
ug/L
04/17/18 23:44
1
2,4-Dichlorophenol
<2.1
8.0
4.0
2.1
ug/L
04/17/18 23:44
1
2,6-Dichlorophenol
<2.8
8.0
4.0
2.8
ug/L
04/17/18 23:44
1
Diethyl phthalate
<0.29
4.0
1.6
0.29
ug/L
04/17/18 23:44
1
Dimethoate
<1.5
8.0
4.0
1.5
ug/L
04/17/18 23:44
1
7,12-Dimethylbenz(a)anthracene
<2.4
32
16
2.4
ug/L
04/17/18 23:44
1
3,3'-Dimethylbenzidine
<14
32
16
14
ug/L
04/17/18 23:44
1
2,4-Dimethylphenol
<1.4
8.0
4.0
1.4
ug/L
04/17/18 23:44
1
Dimethyl phthalate
<0.25
4.0
1.6
0.25
ug/L
04/17/18 23:44
1
Di-n-butyl phthalate
<0.59
4.0
2.0
0.59
ug/L
04/17/18 23:44
1
4,6-Dinitro-2-methylphenol
<4.7
16
8.0
4.7
ug/L
04/17/18 23:44
1
2,4-Dinitrophenol
<6.9
16
8.0
6.9
ug/L
04/17/18 23:44
1
2,4-Dinitrotoluene
<0.20
0.80
0.40
0.20
ug/L
04/17/18 23:44
1
2,6-Dinitrotoluene
<0.059
0.80
0.40
0.059
ug/L
04/17/18 23:44
1
Di-n-octyl phthalate
<0.84
8.0
4.0
0.84
ug/L
04/17/18 23:44
1
Diphenylamine
<2.0
8.0
4.0
2.0
ug/L
04/17/18 23:44
1
Disulfoton
<1.5
8.0
4.0
1.5
ug/L
04/17/18 23:44
1
Ethyl methanesulfonate
<3.0
16
8.0
3.0
ug/L
04/17/18 23:44
1
Ethyl Parathion
<1.7
8.0
4.0
1.7
ug/L
04/17/18 23:44
1
Famphur
<24
32
25
24
ug/L
04/17/18 23:44
1
Fluoranthene
<0.36
0.80
0.40
0.36
ug/L
04/17/18 23:44
1
Fluorene
<0.20
0.80
0.40
0.20
ug/L
04/17/18 23:44
1
Hexachlorobenzene
<0.064
0.40
0.20
0.064
ug/L
04/17/18 23:44
1
Hexachlorocyclopentadiene
<5.1
16
8.0
5.1
ug/L
04/17/18 23:44
1
Hexachloroethane
<0.48
4.0
2.0
0.48
ug/L
04/17/18 23:44
1
Hexachloropropene
<3.8
16
8.0
3.8
ug/L
04/17/18 23:44
1
Indeno[1,2,3-cd]pyrene
<0.060
0.16
0.080
0.060
ug/L
04/17/18 23:44
1
Isodrin
<5.5
16
8.0
5.5
ug/L
04/17/18 23:44
1
Isophorone
<0.30
1.6
0.80
0.30
ug/L
04/17/18 23:44
1
Isosafrole
<3.1
8.0
4.0
3.1
ug/L
04/17/18 23:44
1
Kepone
<1.3
8.0
4.0
1.3
ug/L
04/17/18 23:44
1
m-Dinitrobenzene
<1.1
4.0
2.0
1.1
ug/L
04/17/18 23:44
1
Methapyrilene
<8.1
32
16
8.1
ug/L
04/17/18 23:44
1
3-Methylcholanthrene
<1.8
8.0
4.0
1.8
ug/L
04/17/18 23:44
1
Methyl methanesulfonate
<4.8
32
16
4.8
ug/L
04/17/18 23:44
1
2-Methylnaphthalene
<0.052
1.6
0.80
0.052
ug/L
04/17/18 23:44
1
Methyl parathion
<1.9
8.0
4.0
1.9
ug/L
04/17/18 23:44
1
2-Methylphenol
<0.24
1.6
0.80
0.24
ug/L
04/17/18 23:44
1
3 & 4 Methylphenol
<0.36
1.6
0.80
0.36
ug/L
04/17/18 23:44
1
Naphthalene
<0.25
0.80
0.40
0.25
ug/L
04/17/18 23:44
1
1,4-Naphthoquinone
<31
32
32
31
ug/L
04/17/18 23:44
1
1-Naphthylamine
<4.7
16
8.0
4.7
ug/L
04/17/18 23:44
1
2-Naphthylamine
<7.3
16
8.0
7.3
ug/L
04/17/18 23:44
1
2-Nitroaniline
<1.0
4.0
2.0
1.0
ug/L
04/17/18 23:44
1
3-Nitroaniline
<1.4
8.0
4.0
1.4
ug/L
04/17/18 23:44
1
4-Nitroaniline
<1.3
8.0
4.0
1.3
ug/L
04/17/18 23:44
1
Nitrobenzene
<0.36
0.80
0.40
0.36
ug/L
04/17/18 23:44
1
5-Nitro-o-toluidine
<2.5
8.0
4.0
2.5
ug/L
04/17/18 23:44
1
TestAmerica Chicago
Page 38 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-1(i)
Lab Sample
ID: 500-143858-5
Date Collected: 04/11/18 16:15
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<2.0
8.0
4.0
2.0
ug/L
04/17/18 23:44
1
4-Nitrophenol
<6.0
16
8.0
6.0
ug/L
04/17/18 23:44
1
N-Nitrosodiethylamine
<6.9
16
8.0
6.9
ug/L
04/17/18 23:44
1
N-Nitrosodimethylamine
<3.8
8.0
4.0
3.8
ug/L
04/17/18 23:44
1
N-Nitrosodi-n-butylamine
<3.4
8.0
4.0
3.4
ug/L
04/17/18 23:44
1
N-Nitrosodi-n-propylamine
<0.12
0.40
0.20
0.12
ug/L
04/17/18 23:44
1
N-Nitrosodiphenylamine
<0.30
1.6
0.80
0.30
ug/L
04/17/18 23:44
1
N-Nitrosomethylethylamine
<6.0
16
8.0
6.0
ug/L
04/17/18 23:44
1
N-Nitrosopiperidine
<2.8
8.0
4.0
2.8
ug/L
04/17/18 23:44
1
N-Nitrosopyrrolidine
<2.7
8.0
4.0
2.7
ug/L
04/17/18 23:44
1
o,o',o"-Triethylphosphorothioate
<4.4
16
8.0
4.4
ug/L
04/17/18 23:44
1
o-Toluidine
<6.4
32
16
6.4
ug/L
04/17/18 23:44
1
2,2'-oxybis[l-chloropropane]
<0.30
1.6
0.80
0.30
ug/L
04/17/18 23:44
1
p-Dimethylamino azobenzene
<2.4
8.0
4.0
2.4
ug/L
04/17/18 23:44
1
Pentachlorobenzene
<2.2
8.0
4.0
2.2
ug/L
04/17/18 23:44
1
Pentachloronitrobenzene
<2.9
8.0
4.0
2.9
ug/L
04/17/18 23:44
1
Phenacetin
<1.8
8.0
4.0
1.8
ug/L
04/17/18 23:44
1
Phenanthrene
<0.24
0.80
0.40
0.24
ug/L
04/17/18 23:44
1
Phenol
<0.54
4.0
2.0
0.54
ug/L
04/17/18 23:44
1
Phorate
<1.7
8.0
4.0
1.7
ug/L
04/17/18 23:44
1
p-Phenylene diamine
<13
64
32
13
ug/L
04/17/18 23:44
1
Pronamide
<1.7
8.0
8.0
1.7
ug/L
04/17/18 23:44
1
Pyrene
<0.34
0.80
0.40
0.34
ug/L
04/17/18 23:44
1
Safrole
<3.2
8.0
4.0
3.2
ug/L
04/17/18 23:44
1
sym-Trinitrobenzene
<1.5
8.0
4.0
1.5
ug/L
04/17/18 23:44
1
2,3,7,8-TCDD (Screen)
<8.0
8.0
8.0
8.0
ug/L
04/17/18 23:44
1
1,2,4,5-Tetrachlorobenzene
<0.46
4.0
2.0
0.46
ug/L
04/17/18 23:44
1
2,3,4,6-Tetrachlorophenol
<0.60
4.0
2.0
0.60
ug/L
04/17/18 23:44
1
Thionazin
<2.1
8.0
4.0
2.1
ug/L
04/17/18 23:44
1
2,4,5-Trichlorophenol
<2.1
8.0
4.0
2.1
ug/L
04/17/18 23:44
1
2,4,6-Trichlorophenol
<0.57
4.0
2.0
0.57
ug/L
04/17/18 23:44
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
84
34 - 110
04116118 16:56
04117118 23:44
1
2-Fluorophenol
69
27- 110
04116118 16:56
04117118 23:44
1
Nitrobenzene-d5
90
36 - 120
04116118 16:56
04117118 23:44
1
Phenol-d5
58
20 - 100
04116118 16:56
04117118 23:44
1
Terphenyl-d14
85
40- 145
04116118 16:56
04117118 23:44
1
2,4,6-Tribromophenol
92
40- 145
04116118 16:56
04117118 23:44
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
alpha-BHC
<0.0026
0.040
0.020
0.0026
ug/L
04/19/18 17:33
1
beta-BHC
<0.010
0.040
0.020
0.010
ug/L
04/19/18 17:33
1
delta-BHC
<0.010
0.040
0.020
0.010
ug/L
04/19/18 17:33
1
gamma-BHC (Lindane)
<0.0055
0.040
0.020
0.0055
ug/L
04/19/18 17:33
1
Heptachlor
<0.013
0.040
0.020
0.013
ug/L
04/19/18 17:33
1
Aldrin
<0.0052
0.040
0.020
0.0052
ug/L
04/19/18 17:33
1
Heptachlor epoxide
<0.014
0.040
0.020
0.014
ug/L
04/19/18 17:33
1
Endosulfan 1
<0.0041
0.040
0.020
0.0041
ug/L
04/19/18 17:33
1
TestAmerica Chicago
Page 39 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-1(i)
Lab Sample
ID: 500-143858-5
Date Collected: 04/11/18 16:15
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.013
0.040
0.020
0.013
ug/L
04/19/18 17:33
1
4,4'-DDE
<0.0038
0.040
0.020
0.0038
ug/L
04/19/18 17:33
1
Endrin
<0.014
0.040
0.020
0.014
ug/L
04/19/18 17:33
1
Endosulfan II
<0.0028
0.040
0.020
0.0028
ug/L
04/19/18 17:33
1
4,4'-DDD
<0.013
0.040
0.020
0.013
ug/L
04/19/18 17:33
1
Endosulfan sulfate
<0.012
0.040
0.020
0.012
ug/L
04/19/18 17:33
1
4,4'-DDT
<0.0032
0.040
0.020
0.0032
ug/L
04/19/18 17:33
1
Methoxychlor
<0.023
0.079
0.040
0.023
ug/L
04/19/18 17:33
1
Toxaphene
<0.20
0.40
0.20
0.20
ug/L
04/19/18 17:33
1
Endrin aldehyde
<0.0081
0.040
0.020
0.0081
ug/L
04/19/18 17:33
1
Chlordane (technical)
<0.040
0.079
0.040
0.040
ug/L
04/19/18 17:33
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
35
30 - 130
04117118 07:38
04119118 17:33
1
Tetrachloro-m-xylene
66
30 - 120
04117118 07:38
04119118 17:33
1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.066
0.40
0.20
0.066
ug/L
04/17/18 18:44
1
PCB-1221
<0.20
0.40
0.20
0.20
ug/L
04/17/18 18:44
1
PCB-1232
<0.20
0.40
0.20
0.20
ug/L
04/17/18 18:44
1
PCB-1242
<0.20
0.40
0.20
0.20
ug/L
04/17/18 18:44
1
PCB-1248
<0.20
0.40
0.20
0.20
ug/L
04/17/18 18:44
1
PCB-1254
<0.20
0.40
0.20
0.20
ug/L
04/17/18 18:44
1
PCB-1260
<0.069
0.40
0.20
0.069
ug/L
04/17/18 18:44
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
60
30 - 120
04117118 07:38
04117118 18:44
1
DCB Decachlorobiphenyl
37
30 - 140
04117118 07:38
04117118 18:44
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.45
0.96
0.48
0.45
ug/L
04/17/18 23:45
1
Dinoseb
<0.16
1.9
0.96
0.16
ug/L
04/17/18 23:45
1
Pentachlorophenol
<0.086
0.48
0.096
0.086
ug/L
04/17/18 23:45
1
Silvex (2,4,5-TP)
<0.28
0.96
0.48
0.28
ug/L
04/17/18 23:45
1
2,4,5-T
<0.42
0.96
0.48
0.42
ug/L
04/17/18 23:45
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
92
25 - 130
04117118 09:02
04117118 23:45
1
General Chemistry
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/24/18 15:56
1
Chloride
20000
1000
850
850
ug/L
04/27/1814:31
5
Sulfate
13000 B
400
200
190
ug/L
04/26/18 22:51
2
Alkalinity
210000
5000
5000
3700
ug/L
04/23/1815:49
1
Total Dissolved Solids
320000
10000
10000
4300
ug/L
04/17/18 07:58
1
TestAmerica Chicago
Page 40 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-13(i) Lab Sample ID: 500-143858-6
Date Collected: 04/11/18 12:20 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/23/18 17:12
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/23/18 17:12
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/23/18 17:12
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/23/18 17:12
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 17:12
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 17:12
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/23/18 17:12
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 17:12
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/23/18 17:12
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/23/18 17:12
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 17:12
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/23/18 17:12
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 17:12
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 17:12
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/23/18 17:12
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/23/18 17:12
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 17:12
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/23/18 17:12
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/23/18 17:12
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/23/18 17:12
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/23/18 17:12
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/23/18 17:12
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/23/18 17:12
1
Acetone
9.7 cn
5.0
2.5
1.7
ug/L
04/23/18 17:12
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/23/18 17:12
1
Acrolein
<23
100
50
23
ug/L
04/23/18 17:12
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/23/18 17:12
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 17:12
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 17:12
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/23/18 17:12
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/23/18 17:12
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/23/18 17:12
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/23/18 17:12
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/23/18 17:12
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 17:12
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/23/18 17:12
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/23/18 17:12
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/23/18 17:12
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/23/18 17:12
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/23/18 17:12
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/23/18 17:12
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/23/18 17:12
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/23/18 17:12
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/23/18 17:12
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/23/18 17:12
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/23/18 17:12
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/23/18 17:12
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/23/18 17:12
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/23/18 17:12
1
TestAmerica Chicago
Page 41 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-13(i)
Lab Sample ID: 500-143858-6
Date Collected: 04/11/18 12:20
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/23/18 17:12
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/23/18 17:12
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/23/18 17:12
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 17:12
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/23/18 17:12
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/23/18 17:12
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 17:12
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/23/18 17:12
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 17:12
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/23/18 17:12
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/23/18 17:12
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 17:12
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/23/18 17:12
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/23/18 17:12
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/23/18 17:12
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 110 75- 126
4-Bromofluorobenzene (Surr) 92 72 - 124
Dibromofluoromethane 94 75 - 120
Toluene-d8 (Surr) 93 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04123118 17:12
04123118 17:12
04123118 17:12
04/23/18 17:12
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.24
0.79
0.39
0.24
ug/L
04/18/18 00:13
1
Acenaphthylene
<0.21
0.79
0.39
0.21
ug/L
04/18/18 00:13
1
Acetophenone
<0.52
3.9
2.0
0.52
ug/L
04/18/18 00:13
1
2-Acetylaminofluorene
<1.7
7.9
3.9
1.7
ug/L
04/18/18 00:13
1
4-Aminobiphenyl
<2.9
7.9
3.9
2.9
ug/L
04/18/18 00:13
1
Anthracene
<0.26
0.79
0.39
0.26
ug/L
04/18/18 00:13
1
Benzo[a]anthracene
<0.044
0.16
0.079
0.044
ug/L
04/18/18 00:13
1
Benzo[a]pyrene
<0.078
0.16
0.079
0.078
ug/L
04/18/18 00:13
1
Benzo[b]fluoranthene
<0.063
0.16
0.079
0.063
ug/L
04/18/18 00:13
1
Benzo[g,h,i]perylene
<0.29
0.79
0.39
0.29
ug/L
04/18/18 00:13
1
Benzo[k]fluoranthene
<0.050
0.16
0.079
0.050
ug/L
04/18/18 00:13
1
Benzyl alcohol
<4.7
16
7.9
4.7
ug/L
04/18/18 00:13
1
Bis(2-chloroethoxy)methane
<0.22
1.6
0.79
0.22
ug/L
04/18/18 00:13
1
Bis(2-chloroethyl)ether
<0.23
1.6
0.79
0.23
ug/L
04/18/18 00:13
1
Bis(2-ethylhexyl) phthalate
<1.3
7.9
3.9
1.3
ug/L
04/18/18 00:13
1
4-Bromophenyl phenyl ether
<0.42
3.9
2.0
0.42
ug/L
04/18/18 00:13
1
Butyl benzyl phthalate
<0.38
1.6
0.79
0.38
ug/L
04/18/18 00:13
1
4-Chloroaniline
<1.6
7.9
3.9
1.6
ug/L
04/18/18 00:13
1
Chlorobenzilate
<2.7
7.9
3.9
2.7
ug/L
04/18/18 00:13
1
4-Chloro-3-methylphenol
<1.8
7.9
3.9
1.8
ug/L
04/18/18 00:13
1
2-Chloronaphthalene
<0.18
1.6
0.79
0.18
ug/L
04/18/18 00:13
1
2-Chlorophenol
<0.44
3.9
2.0
0.44
ug/L
04/18/18 00:13
1
4-Chlorophenyl phenyl ether
<0.50
3.9
2.0
0.50
ug/L
04/18/18 00:13
1
Chrysene
<0.053
0.16
0.079
0.053
ug/L
04/18/18 00:13
1
Diallate
<4.3
7.9
4.9
4.3
ug/L
04/18/18 00:13
1
Dibenz(a,h)anthracene
<0.040
0.24
0.12
0.040
ug/L
04/18/18 00:13
1
TestAmerica Chicago
Page 42 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-13(i) Lab Sample ID: 500-143858-6
Date Collected: 04/11/18 12:20 Matrix: Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.21
1.6
0.79
0.21
ug/L
04/18/18 00:13
1
3,3'-Dichlorobenzidine
<1.3
3.9
2.0
1.3
ug/L
04/18/18 00:13
1
2,4-Dichlorophenol
<2.0
7.9
3.9
2.0
ug/L
04/18/18 00:13
1
2,6-Dichlorophenol
<2.7
7.9
3.9
2.7
ug/L
04/18/18 00:13
1
Diethyl phthalate
<0.28
3.9
1.6
0.28
ug/L
04/18/18 00:13
1
Dimethoate
<1.5
7.9
3.9
1.5
ug/L
04/18/18 00:13
1
7,12-Dimethylbenz(a)anthracene
<2.4
31
16
2.4
ug/L
04/18/18 00:13
1
3,3'-Dimethylbenzidine
<14
31
16
14
ug/L
04/18/18 00:13
1
2,4-Dimethylphenol
<1.4
7.9
3.9
1.4
ug/L
04/18/18 00:13
1
Dimethyl phthalate
<0.25
3.9
1.6
0.25
ug/L
04/18/18 00:13
1
Di-n-butyl phthalate
<0.57
3.9
2.0
0.57
ug/L
04/18/18 00:13
1
4,6-Dinitro-2-methylphenol
<4.6
16
7.9
4.6
ug/L
04/18/18 00:13
1
2,4-Dinitrophenol
<6.7
16
7.9
6.7
ug/L
04/18/18 00:13
1
2,4-Dinitrotoluene
<0.19
0.79
0.39
0.19
ug/L
04/18/18 00:13
1
2,6-Dinitrotoluene
<0.058
0.79
0.39
0.058
ug/L
04/18/18 00:13
1
Di-n-octyl phthalate
<0.82
7.9
3.9
0.82
ug/L
04/18/18 00:13
1
Diphenylamine
<2.0
7.9
3.9
2.0
ug/L
04/18/18 00:13
1
Disulfoton
<1.5
7.9
3.9
1.5
ug/L
04/18/18 00:13
1
Ethyl methanesulfonate
<3.0
16
7.9
3.0
ug/L
04/18/18 00:13
1
Ethyl Parathion
<1.6
7.9
3.9
1.6
ug/L
04/18/18 00:13
1
Famphur
<24
31
25
24
ug/L
04/18/18 00:13
1
Fluoranthene
<0.36
0.79
0.39
0.36
ug/L
04/18/18 00:13
1
Fluorene
<0.19
0.79
0.39
0.19
ug/L
04/18/18 00:13
1
Hexachlorobenzene
<0.062
0.39
0.20
0.062
ug/L
04/18/18 00:13
1
Hexachlorocyclopentadiene
<5.0
16
7.9
5.0
ug/L
04/18/18 00:13
1
Hexachloroethane
<0.47
3.9
2.0
0.47
ug/L
04/18/18 00:13
1
Hexachloropropene
<3.7
16
7.9
3.7
ug/L
04/18/18 00:13
1
Indeno[1,2,3-cd]pyrene
<0.059
0.16
0.079
0.059
ug/L
04/18/18 00:13
1
Isodrin
<5.4
16
7.9
5.4
ug/L
04/18/18 00:13
1
Isophorone
<0.29
1.6
0.79
0.29
ug/L
04/18/18 00:13
1
Isosafrole
<3.0
7.9
3.9
3.0
ug/L
04/18/18 00:13
1
Kepone
<1.3
7.9
3.9
1.3
ug/L
04/18/18 00:13
1
m-Dinitrobenzene
<1.0
3.9
2.0
1.0
ug/L
04/18/18 00:13
1
Methapyrilene
<8.0
31
16
8.0
ug/L
04/18/18 00:13
1
3-Methylcholanthrene
<1.8
7.9
3.9
1.8
ug/L
04/18/18 00:13
1
Methyl methanesulfonate
<4.7
31
16
4.7
ug/L
04/18/18 00:13
1
2-Methylnaphthalene
<0.051
1.6
0.79
0.051
ug/L
04/18/18 00:13
1
Methyl parathion
<1.8
7.9
3.9
1.8
ug/L
04/18/18 00:13
1
2-Methylphenol
<0.24
1.6
0.79
0.24
ug/L
04/18/18 00:13
1
3 & 4 Methylphenol
<0.35
1.6
0.79
0.35
ug/L
04/18/18 00:13
1
Naphthalene
<0.24
0.79
0.39
0.24
ug/L
04/18/18 00:13
1
1,4-Naphthoquinone
<31
31
31
31
ug/L
04/18/18 00:13
1
1-Naphthylamine
<4.6
16
7.9
4.6
ug/L
04/18/18 00:13
1
2-Naphthylamine
<7.2
16
7.9
7.2
ug/L
04/18/18 00:13
1
2-Nitroaniline
<1.0
3.9
2.0
1.0
ug/L
04/18/18 00:13
1
3-Nitroaniline
<1.4
7.9
3.9
1.4
ug/L
04/18/18 00:13
1
4-Nitroaniline
<1.3
7.9
3.9
1.3
ug/L
04/18/18 00:13
1
Nitrobenzene
<0.35
0.79
0.39
0.35
ug/L
04/18/18 00:13
1
5-Nitro-o-toluidine
<2.4
7.9
3.9
2.4
ug/L
04/18/18 00:13
1
TestAmerica Chicago
Page 43 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-13(i)
Lab Sample ID: 500-143858-6
Date Collected: 04/11/18 12:20
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
2-Nitrophenol
<2.0
7.9
3.9
2.0
ug/L
04/18/18 00:13
1
4-Nitrophenol
<5.8
16
7.9
5.8
ug/L
04/18/18 00:13
1
N-Nitrosodiethylamine
<6.7
16
7.9
6.7
ug/L
04/18/18 00:13
1
N-Nitrosodimethylamine
<3.7
7.9
3.9
3.7
ug/L
04/18/18 00:13
1
N-Nitrosodi-n-butylamine
<3.3
7.9
3.9
3.3
ug/L
04/18/18 00:13
1
N-Nitrosodi-n-propylamine
<0.12
0.39
0.20
0.12
ug/L
04/18/18 00:13
1
N-Nitrosodiphenylamine
<0.29
1.6
0.79
0.29
ug/L
04/18/18 00:13
1
N-Nitrosomethylethylamine
<5.9
16
7.9
5.9
ug/L
04/18/18 00:13
1
N-Nitrosopiperidine
<2.8
7.9
3.9
2.8
ug/L
04/18/18 00:13
1
N-Nitrosopyrrolidine
<2.6
7.9
3.9
2.6
ug/L
04/18/18 00:13
1
o,o',o"-Triethylphosphorothioate
<4.3
16
7.9
4.3
ug/L
04/18/18 00:13
1
o-Toluidine
<6.2
31
16
6.2
ug/L
04/18/18 00:13
1
2,2'-oxybis[l-chloropropane]
<0.30
1.6
0.79
0.30
ug/L
04/18/18 00:13
1
p-Dimethylamino azobenzene
<2.4
7.9
3.9
2.4
ug/L
04/18/18 00:13
1
Pentachlorobenzene
<2.2
7.9
3.9
2.2
ug/L
04/18/18 00:13
1
Pentachloronitrobenzene
<2.8
7.9
3.9
2.8
ug/L
04/18/18 00:13
1
Phenacetin
<1.8
7.9
3.9
1.8
ug/L
04/18/18 00:13
1
Phenanthrene
<0.24
0.79
0.39
0.24
ug/L
04/18/18 00:13
1
Phenol
<0.53
3.9
2.0
0.53
ug/L
04/18/18 00:13
1
Phorate
<1.7
7.9
3.9
1.7
ug/L
04/18/18 00:13
1
p-Phenylene diamine
<13
63
31
13
ug/L
04/18/18 00:13
1
Pronamide
<1.7
7.9
7.9
1.7
ug/L
04/18/18 00:13
1
Pyrene
<0.33
0.79
0.39
0.33
ug/L
04/18/18 00:13
1
Safrole
<3.1
7.9
3.9
3.1
ug/L
04/18/18 00:13
1
sym-Trinitrobenzene
<1.5
7.9
3.9
1.5
ug/L
04/18/18 00:13
1
2,3,7,8-TCDD (Screen)
<7.9
7.9
7.9
7.9
ug/L
04/18/18 00:13
1
1,2,4,5-Tetrachlorobenzene
<0.45
3.9
2.0
0.45
ug/L
04/18/18 00:13
1
2,3,4,6-Tetrachlorophenol
<0.59
3.9
2.0
0.59
ug/L
04/18/18 00:13
1
Thionazin
<2.0
7.9
3.9
2.0
ug/L
04/18/18 00:13
1
2,4,5-Trichlorophenol
<2.0
7.9
3.9
2.0
ug/L
04/18/18 00:13
1
2,4,6-Trichlorophenol
<0.56
3.9
2.0
0.56
ug/L
04/18/18 00:13
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
81
34 - 110
04116118 16:56
04118118 00:13
1
2-Fluorophenol
65
27- 110
04116118 16:56
04118118 00:13
1
Nitrobenzene-d5
84
36 - 120
04116118 16:56
04118118 00:13
1
Phenol-d5
56
20- 100
04116118 16:56
04118118 00:13
1
Terphenyl-d14
93
40- 145
04116118 16:56
04118118 00:13
1
2,4,6-Tribromophenol
94
40- 145
04116118 16:56
04118118 00:13
1
Method: 8081B - Organochlorine
Pesticides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
alpha-BHC
<0.013
0.20
0.10
0.013
ug/L
04/19/18 17:52
5
beta-BHC
<0.051
0.20
0.10
0.051
ug/L
04/19/18 17:52
5
delta-BHC
<0.052
0.20
0.10
0.052
ug/L
04/19/18 17:52
5
gamma-BHC (Lindane)
<0.028
0.20
0.10
0.028
ug/L
04/19/18 17:52
5
Heptachlor
<0.068
0.20
0.10
0.068
ug/L
04/19/18 17:52
5
Aldrin
<0.027
0.20
0.10
0.027
ug/L
04/19/18 17:52
5
Heptachlor epoxide
<0.069
0.20
0.10
0.069
ug/L
04/19/18 17:52
5
Endosulfan 1
<0.021
0.20
0.10
0.021
ug/L
04/19/18 17:52
5
TestAmerica Chicago
Page 44 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-13(i)
Lab Sample
ID: 500-143858-6
Date Collected: 04/11/18 12:20
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.065
0.20
0.10
0.065
ug/L
04/19/18 17:52
5
4,4'-DDE
<0.019
0.20
0.10
0.019
ug/L
04/19/18 17:52
5
Endrin
<0.071
0.20
0.10
0.071
ug/L
04/19/18 17:52
5
Endosulfan II
<0.014
0.20
0.10
0.014
ug/L
04/19/18 17:52
5
4,4'-DDD
<0.067
0.20
0.10
0.067
ug/L
04/19/18 17:52
5
Endosulfan sulfate
<0.059
0.20
0.10
0.059
ug/L
04/19/18 17:52
5
4,4'-DDT
<0.016
0.20
0.10
0.016
ug/L
04/19/18 17:52
5
Methoxychlor
<0.12
0.40
0.20
0.12
ug/L
04/19/18 17:52
5
Toxaphene
<1.0
2.0
1.0
1.0
ug/L
04/19/18 17:52
5
Endrin aldehyde
<0.041
0.20
0.10
0.041
ug/L
04/19/18 17:52
5
Chlordane (technical)
<0.20
0.40
0.20
0.20
ug/L
04/19/18 17:52
5
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
58
30 - 130
04117118 07:38
04119118 17:52
5
Tetrachloro-m-xylene
289 X
30 - 120
04117118 07:38
04119118 17:52
5
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.067
0.40
0.20
0.067
ug/L
04/17/1819:01
1
PCB-1221
<0.20
0.40
0.20
0.20
ug/L
04/17/1819:01
1
PCB-1232
<0.20
0.40
0.20
0.20
ug/L
04/17/1819:01
1
PCB-1242
<0.20
0.40
0.20
0.20
ug/L
04/17/1819:01
1
PCB-1248
<0.20
0.40
0.20
0.20
ug/L
04/17/1819:01
1
PCB-1254
<0.20
0.40
0.20
0.20
ug/L
04/17/1819:01
1
PCB-1260
<0.070
0.40
0.20
0.070
ug/L
04/17/1819:01
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
103
30 - 120
04117118 07:38
04117118 19:01
1
DCB Decachlorobiphenyl
54
30 - 140
04117118 07:38
04117118 19:01
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.46
1.0
0.50
0.46
ug/L
04/18/18 00:09
1
Dinoseb
<0.16
2.0
1.0
0.16
ug/L
04/18/18 00:09
1
Pentachlorophenol
<0.089
0.50
0.10
0.089
ug/L
04/18/18 00:09
1
Silvex (2,4,5-TP)
<0.29
1.0
0.50
0.29
ug/L
04/18/18 00:09
1
2,4,5-T
<0.43
1.0
0.50
0.43
ug/L
04/18/18 00:09
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
105
25 - 130
04117118 09:02
04118118 00:09
1
Method: 6020B - Metals (ICP/MS) - Total Recoverable
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 02:54
1
Arsenic
1.0
1.0
0.50
0.23
ug/L
04/21/18 02:54
1
Barium
65
2.5
1.3
0.73
ug/L
04/21/18 02:54
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 02:54
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 02:54
1
Chromium
8.2 B
5.0
2.5
1.1
ug/L
04/21/18 02:54
1
Cobalt
2.0
1.0
0.50
0.40
ug/L
04/21/18 02:54
1
Copper
18 B
2.0
1.0
0.50
ug/L
04/21/18 02:54
1
TestAmerica Chicago
Page 45 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-13(i)
Lab Sample ID: 500-143858-6
Date Collected: 04/11/18 12:20
Matrix: Water
Date Received: 04/14/18 12:55
Method: 6020B - Metals (ICP/MS) -
Total Recoverable (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed Dil Fac
Iron
5300
100
50
47
ug/L
04/21/18 02:54 1
Lead
0.36 J
0.50
0.25
0.19
ug/L
04/21/18 02:54 1
Manganese
2300
2.5
1.3
0.79
ug/L
04/21/18 02:54 1
Nickel
4.8
2.0
1.0
0.63
ug/L
04/21/18 02:54 1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 02:54 1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 02:54 1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 02:54 1
Tin
2.0 J
5.0
2.5
1.3
ug/L
04/21/18 02:54 1
Vanadium
4.5 J
5.0
2.5
2.2
ug/L
04/21/18 02:54 1
Zinc
11 B
10
20
6.9
ug/L
04/21/18 02:54 1
Method: 6020B - Metals (ICP/MS) - Dissolved
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 04:58
1
Arsenic
0.94
J
1.0
0.50
0.23
ug/L
04/21/18 04:58
1
Barium
37
2.5
1.3
0.73
ug/L
04/21/18 04:58
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 04:58
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 04:58
1
Cobalt
0.63
J
1.0
0.50
0.40
ug/L
04/21/18 04:58
1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 04:58
1
Copper
<0.50
2.0
1.0
0.50
ug/L
04/21/18 04:58
1
Iron
990
100
50
47
ug/L
04/21/18 04:58
1
Manganese
1500
2.5
1.3
0.79
ug/L
04/21/18 04:58
1
Nickel
<0.63
2.0
1.0
0.63
ug/L
04/21/18 04:58
1
Lead
<0.19
0.50
0.25
0.19
ug/L
04/21/18 04:58
1
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 04:58
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 04:58
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 04:58
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 04:58
1
Vanadium
<2.2
5.0
2.5
2.2
ug/L
04/21/18 04:58
1
Zinc
<6.9
10
20
6.9
ug/L
04/21/18 04:58
1
Method: 7470A - Mercury (CVAA)
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/18/1810:54
1
Method: 7470A - Mercury (CVAA) - Dissolved
Analyte Result Qualifier
Mercury <0.098
(General Chemistry
Analyte
Cyanide, Total
Chloride
Sulfate
Alkalinity
Total Dissolved Solids
RL LOD MDL Unit D Analyzed Dil Fac
0.20 0.10 0.098 ug/L 04/20/18 09:58 1
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
<3.5
10
5.0
3.5
ug/L
04/24/1815:56
1
17000
1000
850
850
ug/L
04/27/1814:43
5
2200 B
200
100
95
ug/L
04/26/18 23:16
1
220000
5000
5000
3700
ug/L
04/23/1815:56
1
270000
10000
10000
4300
ug/L
04/17/18 08:01
1
Page 46 of 258
TestAmerica Chicago
7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-12D(i) Lab Sample ID: 500-143858-7
Date Collected: 04/11/18 14:40 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/23/18 17:44
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/23/18 17:44
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/23/18 17:44
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/23/18 17:44
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 17:44
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 17:44
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/23/18 17:44
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 17:44
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/23/18 17:44
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/23/18 17:44
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 17:44
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/23/18 17:44
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 17:44
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 17:44
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/23/18 17:44
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/23/18 17:44
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 17:44
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/23/18 17:44
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/23/18 17:44
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/23/18 17:44
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/23/18 17:44
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/23/18 17:44
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/23/18 17:44
1
Acetone
8.2 cn
5.0
2.5
1.7
ug/L
04/23/18 17:44
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/23/18 17:44
1
Acrolein
<23
100
50
23
ug/L
04/23/18 17:44
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/23/18 17:44
1
Benzene
0.62
0.50
0.25
0.15
ug/L
04/23/18 17:44
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 17:44
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/23/18 17:44
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/23/18 17:44
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/23/18 17:44
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/23/18 17:44
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/23/18 17:44
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 17:44
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/23/18 17:44
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/23/18 17:44
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/23/18 17:44
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/23/18 17:44
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/23/18 17:44
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/23/18 17:44
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/23/18 17:44
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/23/18 17:44
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/23/18 17:44
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/23/18 17:44
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/23/18 17:44
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/23/18 17:44
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/23/18 17:44
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/23/18 17:44
1
TestAmerica Chicago
Page 47 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-121)(i)
Lab Sample ID: 500-143858-7
Date Collected: 04/11/18 14:40
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/23/18 17:44
1
Methylene Chloride
5.3 cn
5.0
2.5
1.6
ug/L
04/23/18 17:44
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/23/18 17:44
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 17:44
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/23/18 17:44
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/23/18 17:44
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 17:44
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/23/18 17:44
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 17:44
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/23/18 17:44
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/23/18 17:44
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 17:44
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/23/18 17:44
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/23/18 17:44
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/23/18 17:44
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 111 75- 126
4-Bromofluorobenzene (Surr) 90 72 - 124
Dibromofluoromethane 96 75 - 120
Toluene-d8 (Surr) 94 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04123118 17:44
04123118 17:44
04123118 17:44
04/23/18 17:44
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.23
0.74
0.37
0.23
ug/L
04/18/18 00:42
1
Acenaphthylene
<0.20
0.74
0.37
0.20
ug/L
04/18/18 00:42
1
Acetophenone
<0.49
3.7
1.9
0.49
ug/L
04/18/18 00:42
1
2-Acetylaminofluorene
<1.6
7.4
3.7
1.6
ug/L
04/18/18 00:42
1
4-Aminobiphenyl
<2.8
7.4
3.7
2.8
ug/L
04/18/18 00:42
1
Anthracene
<0.25
0.74
0.37
0.25
ug/L
04/18/18 00:42
1
Benzo[a]anthracene
<0.042
0.15
0.074
0.042
ug/L
04/18/18 00:42
1
Benzo[a]pyrene
<0.073
0.15
0.074
0.073
ug/L
04/18/18 00:42
1
Benzo[b]fluoranthene
<0.060
0.15
0.074
0.060
ug/L
04/18/18 00:42
1
Benzo[g,h,i]perylene
<0.28
0.74
0.37
0.28
ug/L
04/18/18 00:42
1
Benzo[k]fluoranthene
<0.047
0.15
0.074
0.047
ug/L
04/18/18 00:42
1
Benzyl alcohol
<4.5
15
7.4
4.5
ug/L
04/18/18 00:42
1
Bis(2-chloroethoxy)methane
<0.21
1.5
0.74
0.21
ug/L
04/18/18 00:42
1
Bis(2-chloroethyl)ether
<0.22
1.5
0.74
0.22
ug/L
04/18/18 00:42
1
Bis(2-ethylhexyl) phthalate
<1.3
7.4
3.7
1.3
ug/L
04/18/18 00:42
1
4-Bromophenyl phenyl ether
<0.40
3.7
1.9
0.40
ug/L
04/18/18 00:42
1
Butyl benzyl phthalate
<0.36
1.5
0.74
0.36
ug/L
04/18/18 00:42
1
4-Chloroaniline
<1.5
7.4
3.7
1.5
ug/L
04/18/18 00:42
1
Chlorobenzilate
<2.5
7.4
3.7
2.5
ug/L
04/18/18 00:42
1
4-Chloro-3-methylphenol
<1.7
7.4
3.7
1.7
ug/L
04/18/18 00:42
1
2-Chloronaphthalene
<0.17
1.5
0.74
0.17
ug/L
04/18/18 00:42
1
2-Chlorophenol
<0.41
3.7
1.9
0.41
ug/L
04/18/18 00:42
1
4-Chlorophenyl phenyl ether
<0.47
3.7
1.9
0.47
ug/L
04/18/18 00:42
1
Chrysene
<0.050
0.15
0.074
0.050
ug/L
04/18/18 00:42
1
Diallate
<4.1
7.4
4.6
4.1
ug/L
04/18/18 00:42
1
Dibenz(a,h)anthracene
<0.038
0.22
0.11
0.038
ug/L
04/18/18 00:42
1
TestAmerica Chicago
Page 48 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-121)(i) Lab Sample ID: 500-143858-7
Date Collected: 04/11/18 14:40 Matrix: Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.19
1.5
0.74
0.19
ug/L
04/18/18 00:42
1
3,3'-Dichlorobenzidine
<1.3
3.7
1.9
1.3
ug/L
04/18/18 00:42
1
2,4-Dichlorophenol
<1.9
7.4
3.7
1.9
ug/L
04/18/18 00:42
1
2,6-Dichlorophenol
<2.6
7.4
3.7
2.6
ug/L
04/18/18 00:42
1
Diethyl phthalate
<0.27
3.7
1.5
0.27
ug/L
04/18/18 00:42
1
Dimethoate
<1.4
7.4
3.7
1.4
ug/L
04/18/18 00:42
1
7,12-Dimethylbenz(a)anthracene
<2.2
30
15
2.2
ug/L
04/18/18 00:42
1
3,3'-Dimethylbenzidine
<13
30
15
13
ug/L
04/18/18 00:42
1
2,4-Dimethylphenol
<1.3
7.4
3.7
1.3
ug/L
04/18/18 00:42
1
Dimethyl phthalate
<0.23
3.7
1.5
0.23
ug/L
04/18/18 00:42
1
Di-n-butyl phthalate
<0.54
3.7
1.9
0.54
ug/L
04/18/18 00:42
1
4,6-Dinitro-2-methylphenol
<4.4
15
7.4
4.4
ug/L
04/18/18 00:42
1
2,4-Dinitrophenol
<6.4
15
7.4
6.4
ug/L
04/18/18 00:42
1
2,4-Dinitrotoluene
<0.18
0.74
0.37
0.18
ug/L
04/18/18 00:42
1
2,6-Dinitrotoluene
<0.055
0.74
0.37
0.055
ug/L
04/18/18 00:42
1
Di-n-octyl phthalate
<0.78
7.4
3.7
0.78
ug/L
04/18/18 00:42
1
Diphenylamine
<1.9
7.4
3.7
1.9
ug/L
04/18/18 00:42
1
Disulfoton
<1.4
7.4
3.7
1.4
ug/L
04/18/18 00:42
1
Ethyl methanesulfonate
<2.8
15
7.4
2.8
ug/L
04/18/18 00:42
1
Ethyl Parathion
<1.5
7.4
3.7
1.5
ug/L
04/18/18 00:42
1
Famphur
<22
30
23
22
ug/L
04/18/18 00:42
1
Fluoranthene
<0.34
0.74
0.37
0.34
ug/L
04/18/18 00:42
1
Fluorene
<0.18
0.74
0.37
0.18
ug/L
04/18/18 00:42
1
Hexachlorobenzene
<0.059
0.37
0.19
0.059
ug/L
04/18/18 00:42
1
Hexachlorocyclopentadiene
<4.7
15
7.4
4.7
ug/L
04/18/18 00:42
1
Hexachloroethane
<0.44
3.7
1.9
0.44
ug/L
04/18/18 00:42
1
Hexachloropropene
<3.5
15
7.4
3.5
ug/L
04/18/18 00:42
1
Indeno[1,2,3-cd]pyrene
<0.055
0.15
0.074
0.055
ug/L
04/18/18 00:42
1
Isodrin
<5.1
15
7.4
5.1
ug/L
04/18/18 00:42
1
Isophorone
<0.28
1.5
0.74
0.28
ug/L
04/18/18 00:42
1
Isosafrole
<2.9
7.4
3.7
2.9
ug/L
04/18/18 00:42
1
Kepone
<1.2
7.4
3.7
1.2
ug/L
04/18/18 00:42
1
m-Dinitrobenzene
<0.98
3.7
1.9
0.98
ug/L
04/18/18 00:42
1
Methapyrilene
<7.5
30
15
7.5
ug/L
04/18/18 00:42
1
3-Methylcholanthrene
<1.7
7.4
3.7
1.7
ug/L
04/18/18 00:42
1
Methyl methanesulfonate
<4.4
30
15
4.4
ug/L
04/18/18 00:42
1
2-Methylnaphthalene
<0.048
1.5
0.74
0.048
ug/L
04/18/18 00:42
1
Methyl parathion
<1.7
7.4
3.7
1.7
ug/L
04/18/18 00:42
1
2-Methylphenol
<0.23
1.5
0.74
0.23
ug/L
04/18/18 00:42
1
3 & 4 Methylphenol
<0.33
1.5
0.74
0.33
ug/L
04/18/18 00:42
1
Naphthalene
<0.23
0.74
0.37
0.23
ug/L
04/18/18 00:42
1
1,4-Naphthoquinone
<29
30
30
29
ug/L
04/18/18 00:42
1
1-Naphthylamine
<4.4
15
7.4
4.4
ug/L
04/18/18 00:42
1
2-Naphthylamine
<6.8
15
7.4
6.8
ug/L
04/18/18 00:42
1
2-Nitroaniline
<0.95
3.7
1.9
0.95
ug/L
04/18/18 00:42
1
3-Nitroaniline
<1.3
7.4
3.7
1.3
ug/L
04/18/18 00:42
1
4-Nitroaniline
<1.2
7.4
3.7
1.2
ug/L
04/18/18 00:42
1
Nitrobenzene
<0.33
0.74
0.37
0.33
ug/L
04/18/18 00:42
1
5-Nitro-o-toluidine
<2.3
7.4
3.7
2.3
ug/L
04/18/18 00:42
1
TestAmerica Chicago
Page 49 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-121)(i)
Lab Sample
ID: 500-143858-7
Date Collected: 04/11/18 14:40
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<1.9
7.4
3.7
1.9
ug/L
04/18/18 00:42
1
4-Nitrophenol
<5.5
15
7.4
5.5
ug/L
04/18/18 00:42
1
N-Nitrosodiethylamine
<6.4
15
7.4
6.4
ug/L
04/18/18 00:42
1
N-Nitrosodimethylamine
<3.5
7.4
3.7
3.5
ug/L
04/18/18 00:42
1
N-Nitrosodi-n-butylamine
<3.1
7.4
3.7
3.1
ug/L
04/18/18 00:42
1
N-Nitrosodi-n-propylamine
<0.11
0.37
0.19
0.11
ug/L
04/18/18 00:42
1
N-Nitrosodiphenylamine
<0.27
1.5
0.74
0.27
ug/L
04/18/18 00:42
1
N-Nitrosomethylethylamine
<5.5
15
7.4
5.5
ug/L
04/18/18 00:42
1
N-Nitrosopiperidine
<2.6
7.4
3.7
2.6
ug/L
04/18/18 00:42
1
N-Nitrosopyrrolidine
<2.5
7.4
3.7
2.5
ug/L
04/18/18 00:42
1
o,o',o"-Triethylphosphorothioate
<4.1
15
7.4
4.1
ug/L
04/18/18 00:42
1
o-Toluidine
<5.9
30
15
5.9
ug/L
04/18/18 00:42
1
2,2'-oxybis[l-chloropropane]
<0.28
1.5
0.74
0.28
ug/L
04/18/18 00:42
1
p-Dimethylamino azobenzene
<2.2
7.4
3.7
2.2
ug/L
04/18/18 00:42
1
Pentachlorobenzene
<2.1
7.4
3.7
2.1
ug/L
04/18/18 00:42
1
Pentachloronitrobenzene
<2.6
7.4
3.7
2.6
ug/L
04/18/18 00:42
1
Phenacetin
<1.7
7.4
3.7
1.7
ug/L
04/18/18 00:42
1
Phenanthrene
<0.22
0.74
0.37
0.22
ug/L
04/18/18 00:42
1
Phenol
<0.50
3.7
1.9
0.50
ug/L
04/18/18 00:42
1
Phorate
<1.6
7.4
3.7
1.6
ug/L
04/18/18 00:42
1
p-Phenylene diamine
<12
59
30
12
ug/L
04/18/18 00:42
1
Pronamide
<1.6
7.4
7.4
1.6
ug/L
04/18/18 00:42
1
Pyrene
<0.32
0.74
0.37
0.32
ug/L
04/18/18 00:42
1
Safrole
<3.0
7.4
3.7
3.0
ug/L
04/18/18 00:42
1
sym-Trinitrobenzene
<1.4
7.4
3.7
1.4
ug/L
04/18/18 00:42
1
2,3,7,8-TCDD (Screen)
<7.4
7.4
7.4
7.4
ug/L
04/18/18 00:42
1
1,2,4,5-Tetrachlorobenzene
<0.42
3.7
1.9
0.42
ug/L
04/18/18 00:42
1
2,3,4,6-Tetrachlorophenol
<0.55
3.7
1.9
0.55
ug/L
04/18/18 00:42
1
Thionazin
<1.9
7.4
3.7
1.9
ug/L
04/18/18 00:42
1
2,4,5-Trichlorophenol
<1.9
7.4
3.7
1.9
ug/L
04/18/18 00:42
1
2,4,6-Trichlorophenol
<0.53
3.7
1.9
0.53
ug/L
04/18/18 00:42
1
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
79
34 - 110
04116118 16:56
04118118 00:42
1
2-Fluorophenol
60
27- 110
04116118 16:56
04118118 00:42
1
Nitrobenzene-d5
82
36 - 120
04116118 16:56
04118118 00:42
1
Phenol-d5
56
20- 100
04116118 16:56
04118118 00:42
1
Terphenyl-d14
93
40- 145
04116118 16:56
04118118 00:42
1
2,4,6-Tribromophenol
99
40- 145
04116118 16:56
04118118 00:42
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
alpha-BHC
<0.012
beta-BHC
<0.049
delta-BHC
<0.049
gamma-BHC (Lindane)
<0.027
Heptachlor
<0.065
Aldrin
<0.025
Heptachlor epoxide
<0.066
Endosulfan 1
<0.020
RL
LOD
MDL
Unit
D Analyzed
0.19
0.096
0.012
ug/L
04/19/1818:11
0.19
0.096
0.049
ug/L
04/19/1818:11
0.19
0.096
0.049
ug/L
04/19/1818:11
0.19
0.096
0.027
ug/L
04/19/1818:11
0.19
0.096
0.065
ug/L
04/19/1818:11
0.19
0.096
0.025
ug/L
04/19/1818:11
0.19
0.096
0.066
ug/L
04/19/1818:11
0.19
0.096
0.020
ug/L
04/19/1818:11
Dil Fac
Page 50 of 258
TestAmerica Chicago
7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg
Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-121)(i)
Lab Sample
ID: 500-143858-7
Date Collected: 04/11/18 14:40
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8081B - Organochlorine
Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.062
0.19
0.096
0.062
ug/L
04/19/18 18:11
5
4,4'-DDE
<0.018
0.19
0.096
0.018
ug/L
04/19/18 18:11
5
Endrin
<0.068
0.19
0.096
0.068
ug/L
04/19/18 18:11
5
Endosulfan II
<0.013
0.19
0.096
0.013
ug/L
04/19/18 18:11
5
4,4'-DDD
<0.064
0.19
0.096
0.064
ug/L
04/19/18 18:11
5
Endosulfan sulfate
<0.056
0.19
0.096
0.056
ug/L
04/19/18 18:11
5
4,4'-DDT
<0.015
0.19
0.096
0.015
ug/L
04/19/18 18:11
5
Methoxychlor
<0.11
0.38
0.19
0.11
ug/L
04/19/18 18:11
5
Toxaphene
<0.96
1.9
0.96
0.96
ug/L
04/19/18 18:11
5
Endrin aldehyde
<0.039
0.19
0.096
0.039
ug/L
04/19/18 18:11
5
Chlordane (technical)
<0.19
0.38
0.19
0.19
ug/L
04/19/18 18:11
5
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
75
30 - 130
04117118 07:38
04119118 18:11
5
Tetrachloro-m-xylene
190 X
30 - 120
04117118 07:38
04119118 18:11
5
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.064
0.38
0.19
0.064
ug/L
04/17/1819:17
1
PCB-1221
<0.19
0.38
0.19
0.19
ug/L
04/17/1819:17
1
PCB-1232
<0.19
0.38
0.19
0.19
ug/L
04/17/1819:17
1
PCB-1242
<0.19
0.38
0.19
0.19
ug/L
04/17/1819:17
1
PCB-1248
<0.19
0.38
0.19
0.19
ug/L
04/17/1819:17
1
PCB-1254
<0.19
0.38
0.19
0.19
ug/L
04/17/1819:17
1
PCB-1260
<0.067
0.38
0.19
0.067
ug/L
04/17/1819:17
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
65
30 - 120
04117118 07:38
04117118 19:17
1
DCB Decachlorobiphenyl
81
30 - 140
04117118 07:38
04117118 19:17
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.45
0.97
0.48
0.45
ug/L
04/18/18 00:33
1
Dinoseb
<0.16
1.9
0.97
0.16
ug/L
04/18/18 00:33
1
Pentachlorophenol
<0.087
0.48
0.097
0.087
ug/L
04/18/18 00:33
1
Silvex (2,4,5-TP)
<0.28
0.97
0.48
0.28
ug/L
04/18/18 00:33
1
2,4,5-T
<0.42
0.97
0.48
0.42
ug/L
04/18/18 00:33
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
92
25 - 130
04117118 09:02
04118118 00:33
1
Method: 6020B - Metals (ICP/MS) - Total Recoverable
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 02:57
1
Arsenic
2.9
1.0
0.50
0.23
ug/L
04/21/18 02:57
1
Barium
240
2.5
1.3
0.73
ug/L
04/21/18 02:57
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 02:57
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 02:57
1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 02:57
1
Cobalt
1.3
1.0
0.50
0.40
ug/L
04/21/18 02:57
1
Copper
<0.50
2.0
1.0
0.50
ug/L
04/21/18 02:57
1
TestAmerica Chicago
Page 51 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-121)(i) Lab Sample ID: 500-143858-7
Date Collected: 04/11/18 14:40 Matrix: Water
Date Received: 04/14/18 12:55
Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Iron
6900
100
50
47
ug/L
04/21/18 02:57
1
Lead
<0.19
0.50
0.25
0.19
ug/L
04/21/18 02:57
1
Manganese
510
2.5
1.3
0.79
ug/L
04/21/18 02:57
1
Nickel
3.2
2.0
1.0
0.63
ug/L
04/21/18 02:57
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 02:57
1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 02:57
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 02:57
1
Tin
1.5 J
5.0
2.5
1.3
ug/L
04/21/18 02:57
1
Vanadium
<2.2
5.0
2.5
2.2
ug/L
04/21/18 02:57
1
Zinc
<6.9
10
20
6.9
ug/L
04/21/18 02:57
1
Method: 6020B - Metals (ICP/MS) - Dissolved
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
D
Analyzed
Dil Fac
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 05:02
1
Arsenic
3.6
1.0
0.50
0.23
ug/L
04/21/18 05:02
1
Barium
240
2.5
1.3
0.73
ug/L
04/21/18 05:02
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 05:02
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 05:02
1
Cobalt
1.1
1.0
0.50
0.40
ug/L
04/21/18 05:02
1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 05:02
1
Copper
<0.50
2.0
1.0
0.50
ug/L
04/21/18 05:02
1
Iron
8800
100
50
47
ug/L
04/21/18 05:02
1
Manganese
640
2.5
1.3
0.79
ug/L
04/21/18 05:02
1
Nickel
2.0
2.0
1.0
0.63
ug/L
04/21/18 05:02
1
Lead
<0.19
0.50
0.25
0.19
ug/L
04/21/18 05:02
1
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 05:02
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 05:02
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 05:02
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 05:02
1
Vanadium
<2.2
5.0
2.5
2.2
ug/L
04/21/18 05:02
1
Zinc
8.0
J
10
20
6.9
ug/L
04/21/18 05:02
1
Method: 7470A - Mercury (CVAA)
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
D
Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/18/1810:56
1
Method: 7470A - Mercury (CVAA) -
Dissolved
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
D
Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/20/1810:03
1
General Chemistry
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
D
Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/24/18 15:56
1
Chloride
37000
4000
3400
3400
ug/L
04/27/1814:55
20
Sulfate
68000
B
4000
2000
1900
ug/L
04/27/18 00:06
20
Alkalinity
540000
5000
5000
3700
ug/L
04/23/1815:14
1
Total Dissolved Solids
750000
10000
10000
4300
ug/L
04/17/18 08:03
1
TestAmerica Chicago
Page 52 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-8D(i) Lab Sample ID: 500-143858-8
Date Collected: 04/11/18 14:35 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/23/18 18:12
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/23/18 18:12
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/23/18 18:12
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/23/18 18:12
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 18:12
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 18:12
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/23/18 18:12
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 18:12
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/23/18 18:12
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/23/18 18:12
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 18:12
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/23/18 18:12
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 18:12
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 18:12
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/23/18 18:12
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/23/18 18:12
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 18:12
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/23/18 18:12
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/23/18 18:12
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/23/18 18:12
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/23/18 18:12
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/23/18 18:12
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/23/18 18:12
1
Acetone
<1.7
5.0
2.5
1.7
ug/L
04/23/18 18:12
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/23/18 18:12
1
Acrolein
<23
100
50
23
ug/L
04/23/18 18:12
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/23/18 18:12
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 18:12
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 18:12
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/23/18 18:12
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/23/18 18:12
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/23/18 18:12
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/23/18 18:12
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/23/18 18:12
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 18:12
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/23/18 18:12
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/23/18 18:12
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/23/18 18:12
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/23/18 18:12
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/23/18 18:12
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/23/18 18:12
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/23/18 18:12
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/23/18 18:12
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/23/18 18:12
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/23/18 18:12
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/23/18 18:12
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/23/18 18:12
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/23/18 18:12
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/23/18 18:12
1
TestAmerica Chicago
Page 53 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-81)(i)
Lab Sample ID: 500-143858-8
Date Collected: 04/11/18 14:35
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/23/18 18:12
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/23/18 18:12
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/23/18 18:12
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 18:12
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/23/18 18:12
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/23/18 18:12
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 18:12
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/23/18 18:12
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 18:12
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/23/18 18:12
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/23/18 18:12
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 18:12
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/23/18 18:12
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/23/18 18:12
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/23/18 18:12
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 110 75- 226
4-Bromofluorobenzene (Surr) 93 72 - 124
Dibromofluoromethane 95 75 - 120
Toluene-d8 (Surr) 95 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04123118 18:12
04123118 18:12
04123118 18:12
04/23/18 18:12
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.24
0.78
0.39
0.24
ug/L
04/18/18 01:11
1
Acenaphthylene
<0.21
0.78
0.39
0.21
ug/L
04/18/18 01:11
1
Acetophenone
<0.52
3.9
1.9
0.52
ug/L
04/18/18 01:11
1
2-Acetylaminofluorene
<1.7
7.8
3.9
1.7
ug/L
04/18/18 01:11
1
4-Aminobiphenyl
<2.9
7.8
3.9
2.9
ug/L
04/18/18 01:11
1
Anthracene
<0.26
0.78
0.39
0.26
ug/L
04/18/18 01:11
1
Benzo[a]anthracene
<0.044
0.16
0.078
0.044
ug/L
04/18/18 01:11
1
Benzo[a]pyrene
<0.077
0.16
0.078
0.077
ug/L
04/18/18 01:11
1
Benzo[b]fluoranthene
<0.063
0.16
0.078
0.063
ug/L
04/18/18 01:11
1
Benzo[g,h,i]perylene
<0.29
0.78
0.39
0.29
ug/L
04/18/18 01:11
1
Benzo[k]fluoranthene
<0.050
0.16
0.078
0.050
ug/L
04/18/18 01:11
1
Benzyl alcohol
<4.7
16
7.8
4.7
ug/L
04/18/18 01:11
1
Bis(2-chloroethoxy)methane
<0.22
1.6
0.78
0.22
ug/L
04/18/18 01:11
1
Bis(2-chloroethyl)ether
<0.23
1.6
0.78
0.23
ug/L
04/18/18 01:11
1
Bis(2-ethylhexyl) phthalate
<1.3
7.8
3.9
1.3
ug/L
04/18/18 01:11
1
4-Bromophenyl phenyl ether
<0.42
3.9
1.9
0.42
ug/L
04/18/18 01:11
1
Butyl benzyl phthalate
<0.37
1.6
0.78
0.37
ug/L
04/18/18 01:11
1
4-Chloroaniline
<1.6
7.8
3.9
1.6
ug/L
04/18/18 01:11
1
Chlorobenzilate
<2.7
7.8
3.9
2.7
ug/L
04/18/18 01:11
1
4-Chloro-3-methylphenol
<1.8
7.8
3.9
1.8
ug/L
04/18/18 01:11
1
2-Chloronaphthalene
<0.18
1.6
0.78
0.18
ug/L
04/18/18 01:11
1
2-Chlorophenol
<0.44
3.9
1.9
0.44
ug/L
04/18/18 01:11
1
4-Chlorophenyl phenyl ether
<0.49
3.9
1.9
0.49
ug/L
04/18/18 01:11
1
Chrysene
<0.053
0.16
0.078
0.053
ug/L
04/18/18 01:11
1
Diallate
<4.3
7.8
4.9
4.3
ug/L
04/18/18 01:11
1
Dibenz(a,h)anthracene
<0.040
0.23
0.12
0.040
ug/L
04/18/18 01:11
1
TestAmerica Chicago
Page 54 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-81)(i) Lab Sample ID: 500-143858-8
Date Collected: 04/11/18 14:35 Matrix: Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.20
1.6
0.78
0.20
ug/L
04/18/18 01:11
1
3,3'-Dichlorobenzidine
<1.3
3.9
1.9
1.3
ug/L
04/18/18 01:11
1
2,4-Dichlorophenol
<2.0
7.8
3.9
2.0
ug/L
04/18/18 01:11
1
2,6-Dichlorophenol
<2.7
7.8
3.9
2.7
ug/L
04/18/18 01:11
1
Diethyl phthalate
<0.28
3.9
1.6
0.28
ug/L
04/18/18 01:11
1
Dimethoate
<1.5
7.8
3.9
1.5
ug/L
04/18/18 01:11
1
7,12-Dimethylbenz(a)anthracene
<2.3
31
16
2.3
ug/L
04/18/18 01:11
1
3,3'-Dimethylbenzidine
<14
31
16
14
ug/L
04/18/18 01:11
1
2,4-Dimethylphenol
<1.4
7.8
3.9
1.4
ug/L
04/18/18 01:11
1
Dimethyl phthalate
<0.24
3.9
1.6
0.24
ug/L
04/18/18 01:11
1
Di-n-butyl phthalate
<0.57
3.9
1.9
0.57
ug/L
04/18/18 01:11
1
4,6-Dinitro-2-methylphenol
<4.6
16
7.8
4.6
ug/L
04/18/18 01:11
1
2,4-Dinitrophenol
<6.7
16
7.8
6.7
ug/L
04/18/18 01:11
1
2,4-Dinitrotoluene
<0.19
0.78
0.39
0.19
ug/L
04/18/18 01:11
1
2,6-Dinitrotoluene
<0.057
0.78
0.39
0.057
ug/L
04/18/18 01:11
1
Di-n-octyl phthalate
<0.82
7.8
3.9
0.82
ug/L
04/18/18 01:11
1
Diphenylamine
<2.0
7.8
3.9
2.0
ug/L
04/18/18 01:11
1
Disulfoton
<1.5
7.8
3.9
1.5
ug/L
04/18/18 01:11
1
Ethyl methanesulfonate
<3.0
16
7.8
3.0
ug/L
04/18/18 01:11
1
Ethyl Parathion
<1.6
7.8
3.9
1.6
ug/L
04/18/18 01:11
1
Famphur
<23
31
24
23
ug/L
04/18/18 01:11
1
Fluoranthene
<0.35
0.78
0.39
0.35
ug/L
04/18/18 01:11
1
Fluorene
<0.19
0.78
0.39
0.19
ug/L
04/18/18 01:11
1
Hexachlorobenzene
<0.062
0.39
0.19
0.062
ug/L
04/18/18 01:11
1
Hexachlorocyclopentadiene
<5.0
16
7.8
5.0
ug/L
04/18/18 01:11
1
Hexachloroethane
<0.47
3.9
1.9
0.47
ug/L
04/18/18 01:11
1
Hexachloropropene
<3.7
16
7.8
3.7
ug/L
04/18/18 01:11
1
Indeno[1,2,3-cd]pyrene
<0.058
0.16
0.078
0.058
ug/L
04/18/18 01:11
1
Isodrin
<5.4
16
7.8
5.4
ug/L
04/18/18 01:11
1
Isophorone
<0.29
1.6
0.78
0.29
ug/L
04/18/18 01:11
1
Isosafrole
<3.0
7.8
3.9
3.0
ug/L
04/18/18 01:11
1
Kepone
<1.3
7.8
3.9
1.3
ug/L
04/18/18 01:11
1
m-Dinitrobenzene
<1.0
3.9
1.9
1.0
ug/L
04/18/18 01:11
1
Methapyrilene
<7.9
31
16
7.9
ug/L
04/18/18 01:11
1
3-Methylcholanthrene
<1.8
7.8
3.9
1.8
ug/L
04/18/18 01:11
1
Methyl methanesulfonate
<4.6
31
16
4.6
ug/L
04/18/18 01:11
1
2-Methylnaphthalene
<0.051
1.6
0.78
0.051
ug/L
04/18/18 01:11
1
Methyl parathion
<1.8
7.8
3.9
1.8
ug/L
04/18/18 01:11
1
2-Methylphenol
<0.24
1.6
0.78
0.24
ug/L
04/18/18 01:11
1
3 & 4 Methylphenol
<0.35
1.6
0.78
0.35
ug/L
04/18/18 01:11
1
Naphthalene
<0.24
0.78
0.39
0.24
ug/L
04/18/18 01:11
1
1,4-Naphthoquinone
<30
31
31
30
ug/L
04/18/18 01:11
1
1-Naphthylamine
<4.6
16
7.8
4.6
ug/L
04/18/18 01:11
1
2-Naphthylamine
<7.1
16
7.8
7.1
ug/L
04/18/18 01:11
1
2-Nitroaniline
<1.0
3.9
1.9
1.0
ug/L
04/18/18 01:11
1
3-Nitroaniline
<1.4
7.8
3.9
1.4
ug/L
04/18/18 01:11
1
4-Nitroaniline
<1.3
7.8
3.9
1.3
ug/L
04/18/18 01:11
1
Nitrobenzene
<0.35
0.78
0.39
0.35
ug/L
04/18/18 01:11
1
5-Nitro-o-toluidine
<2.4
7.8
3.9
2.4
ug/L
04/18/18 01:11
1
TestAmerica Chicago
Page 55 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-81)(i)
Lab Sample
ID: 500-143858-8
Date Collected: 04/11/18 14:35
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<1.9
7.8
3.9
1.9
ug/L
04/18/18 01:11
1
4-Nitrophenol
<5.8
16
7.8
5.8
ug/L
04/18/18 01:11
1
N-Nitrosodiethylamine
<6.7
16
7.8
6.7
ug/L
04/18/18 01:11
1
N-Nitrosodimethylamine
<3.7
7.8
3.9
3.7
ug/L
04/18/18 01:11
1
N-Nitrosodi-n-butylamine
<3.3
7.8
3.9
3.3
ug/L
04/18/18 01:11
1
N-Nitrosodi-n-propylamine
<0.12
0.39
0.19
0.12
ug/L
04/18/18 01:11
1
N-Nitrosodiphenylamine
<0.29
1.6
0.78
0.29
ug/L
04/18/18 01:11
1
N-Nitrosomethylethylamine
<5.8
16
7.8
5.8
ug/L
04/18/18 01:11
1
N-Nitrosopiperidine
<2.7
7.8
3.9
2.7
ug/L
04/18/18 01:11
1
N-Nitrosopyrrolidine
<2.6
7.8
3.9
2.6
ug/L
04/18/18 01:11
1
o,o',o"-Triethylphosphorothioate
<4.3
16
7.8
4.3
ug/L
04/18/18 01:11
1
o-Toluidine
<6.2
31
16
6.2
ug/L
04/18/18 01:11
1
2,2'-oxybis[l-chloropropane]
<0.30
1.6
0.78
0.30
ug/L
04/18/18 01:11
1
p-Dimethylamino azobenzene
<2.3
7.8
3.9
2.3
ug/L
04/18/18 01:11
1
Pentachlorobenzene
<2.2
7.8
3.9
2.2
ug/L
04/18/18 01:11
1
Pentachloronitrobenzene
<2.8
7.8
3.9
2.8
ug/L
04/18/18 01:11
1
Phenacetin
<1.8
7.8
3.9
1.8
ug/L
04/18/18 01:11
1
Phenanthrene
<0.23
0.78
0.39
0.23
ug/L
04/18/18 01:11
1
Phenol
<0.52
3.9
1.9
0.52
ug/L
04/18/18 01:11
1
Phorate
<1.7
7.8
3.9
1.7
ug/L
04/18/18 01:11
1
p-Phenylene diamine
<13
62
31
13
ug/L
04/18/18 01:11
1
Pronamide
<1.7
7.8
7.8
1.7
ug/L
04/18/18 01:11
1
Pyrene
<0.33
0.78
0.39
0.33
ug/L
04/18/18 01:11
1
Safrole
<3.1
7.8
3.9
3.1
ug/L
04/18/18 01:11
1
sym-Trinitrobenzene
<1.5
7.8
3.9
1.5
ug/L
04/18/18 01:11
1
2,3,7,8-TCDD (Screen)
<7.8
7.8
7.8
7.8
ug/L
04/18/18 01:11
1
1,2,4,5-Tetrachlorobenzene
<0.45
3.9
1.9
0.45
ug/L
04/18/18 01:11
1
2,3,4,6-Tetrachlorophenol
<0.58
3.9
1.9
0.58
ug/L
04/18/18 01:11
1
Thionazin
<2.0
7.8
3.9
2.0
ug/L
04/18/18 01:11
1
2,4,5-Trichlorophenol
<2.0
7.8
3.9
2.0
ug/L
04/18/18 01:11
1
2,4,6-Trichlorophenol
<0.56
3.9
1.9
0.56
ug/L
04/18/18 01:11
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
88
34 - 110
04116118 16:56
04118118 01:11
1
2-Fluorophenol
64
27- 110
04116118 16:56
04118118 01:11
1
Nitrobenzene-d5
93
36 - 120
04116118 16:56
04118118 01:11
1
Phenol-d5
52
20- 100
04116118 16:56
04118118 01:11
1
Terphenyl-d14
99
40- 145
04116118 16:56
04118118 01:11
1
2,4,6-Tribromophenol
90
40- 145
04116118 16:56
04118118 01:11
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
alpha-BHC
<0.0027
0.042
0.021
0.0027
ug/L
04/20/18 14:44
1
beta-BHC
<0.011
0.042
0.021
0.011
ug/L
04/20/18 14:44
1
delta-BHC
<0.011
0.042
0.021
0.011
ug/L
04/20/18 14:44
1
gamma-BHC (Lindane)
<0.0058
0.042
0.021
0.0058
ug/L
04/20/18 14:44
1
Heptachlor
<0.014
0.042
0.021
0.014
ug/L
04/20/18 14:44
1
Aldrin
<0.0055
0.042
0.021
0.0055
ug/L
04/20/18 14:44
1
Heptachlor epoxide
<0.014
0.042
0.021
0.014
ug/L
04/20/18 14:44
1
Endosulfan 1
<0.0043
0.042
0.021
0.0043
ug/L
04/20/18 14:44
1
TestAmerica Chicago
Page 56 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-81)(i)
Lab Sample
ID: 500-143858-8
Date Collected: 04/11/18 14:35
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.013
0.042
0.021
0.013
ug/L
04/20/18 14:44
1
4,4'-DDE
<0.0040
0.042
0.021
0.0040
ug/L
04/20/18 14:44
1
Endrin
<0.015
0.042
0.021
0.015
ug/L
04/20/18 14:44
1
Endosulfan II
<0.0029
0.042
0.021
0.0029
ug/L
04/20/18 14:44
1
4,4'-DDD
<0.014
0.042
0.021
0.014
ug/L
04/20/18 14:44
1
Endosulfan sulfate
<0.012
0.042
0.021
0.012
ug/L
04/20/18 14:44
1
4,4'-DDT
<0.0033
0.042
0.021
0.0033
ug/L
04/20/18 14:44
1
Methoxychlor
<0.024
0.083
0.042
0.024
ug/L
04/20/18 14:44
1
Toxaphene
<0.21
0.42
0.21
0.21
ug/L
04/20/18 14:44
1
Endrin aldehyde
<0.0085
0.042
0.021
0.0085
ug/L
04/20/18 14:44
1
Chlordane (technical)
<0.042
0.083
0.042
0.042
ug/L
04/20/18 14:44
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
77
30 - 130
04117118 07:38
04120118 14:44
1
Tetrachloro-m-xylene
59
30 - 120
04117118 07:38
04120118 14:44
1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.070
0.42
0.21
0.070
ug/L
04/17/1819:33
1
PCB-1221
<0.21
0.42
0.21
0.21
ug/L
04/17/1819:33
1
PCB-1232
<0.21
0.42
0.21
0.21
ug/L
04/17/1819:33
1
PCB-1242
<0.21
0.42
0.21
0.21
ug/L
04/17/1819:33
1
PCB-1248
<0.21
0.42
0.21
0.21
ug/L
04/17/1819:33
1
PCB-1254
<0.21
0.42
0.21
0.21
ug/L
04/17/1819:33
1
PCB-1260
<0.073
0.42
0.21
0.073
ug/L
04/17/1819:33
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
66
30 - 120
04117118 07:38
04117118 19:33
1
DCB Decachlorobiphenyl
90
30 - 140
04117118 07:38
04117118 19:33
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.44
0.95
0.48
0.44
ug/L
04/18/18 00:58
1
Dinoseb
<0.16
1.9
0.95
0.16
ug/L
04/18/18 00:58
1
Pentachlorophenol
<0.085
0.48
0.095
0.085
ug/L
04/18/18 00:58
1
Silvex (2,4,5-TP)
<0.27
0.95
0.48
0.27
ug/L
04/18/18 00:58
1
2,4,5-T
<0.41
0.95
0.48
0.41
ug/L
04/18/18 00:58
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
80
25 - 130
04117118 09:02
04118118 00:58
1
Method: 6020B - Metals (ICP/MS) - Total Recoverable
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 03:01
1
Arsenic
<0.23
1.0
0.50
0.23
ug/L
04/21/18 03:01
1
Barium
56
2.5
1.3
0.73
ug/L
04/21/18 03:01
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 03:01
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 03:01
1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 03:01
1
Cobalt
<0.40
1.0
0.50
0.40
ug/L
04/21/18 03:01
1
Copper
1.2 J B
2.0
1.0
0.50
ug/L
04/21/18 03:01
1
TestAmerica Chicago
Page 57 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill
- Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-81)(i)
Lab Sample ID: 500-143858-8
Date Collected: 04/11/18 14:35
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Iron
<47
100
50
47
ug/L
04/21/18 03:01
1
Lead
<0.19
0.50
0.25
0.19
ug/L
04/21/18 03:01
1
Manganese
2.8
2.5
1.3
0.79
ug/L
04/21/18 03:01
1
Nickel
<0.63
2.0
1.0
0.63
ug/L
04/21/18 03:01
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 03:01
1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 03:01
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 03:01
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 03:01
1
Vanadium
4.1 J
5.0
2.5
2.2
ug/L
04/21/18 03:01
1
Zinc
<6.9
10
20
6.9
ug/L
04/21/18 03:01
1
Method: 7470A - Mercury (CVAA)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/18/1811:01
1
General Chemistry
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/25/18 09:56
1
Chloride
40000
4000
3400
3400
ug/L
04/27/1815:08
20
Sulfate
27000 B
1000
500
480
ug/L
04/27/18 00:18
5
Alkalinity
190000
5000
5000
3700
ug/L
04/23/1816:03
1
Total Dissolved Solids
330000
10000
10000
4300
ug/L
04/17/18 08:06
1
TestAmerica Chicago
Page 58 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-5(i) Lab Sample ID: 500-143858-9
Date Collected: 04/11/18 11:40 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/23/18 18:41
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/23/18 18:41
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/23/18 18:41
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/23/18 18:41
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 18:41
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 18:41
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/23/18 18:41
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 18:41
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/23/18 18:41
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/23/18 18:41
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 18:41
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/23/18 18:41
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 18:41
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 18:41
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/23/18 18:41
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/23/18 18:41
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 18:41
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/23/18 18:41
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/23/18 18:41
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/23/18 18:41
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/23/18 18:41
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/23/18 18:41
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/23/18 18:41
1
Acetone
<1.7
5.0
2.5
1.7
ug/L
04/23/18 18:41
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/23/18 18:41
1
Acrolein
<23
100
50
23
ug/L
04/23/18 18:41
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/23/18 18:41
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 18:41
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 18:41
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/23/18 18:41
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/23/18 18:41
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/23/18 18:41
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/23/18 18:41
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/23/18 18:41
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 18:41
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/23/18 18:41
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/23/18 18:41
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/23/18 18:41
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/23/18 18:41
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/23/18 18:41
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/23/18 18:41
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/23/18 18:41
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/23/18 18:41
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/23/18 18:41
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/23/18 18:41
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/23/18 18:41
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/23/18 18:41
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/23/18 18:41
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/23/18 18:41
1
TestAmerica Chicago
Page 59 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-5(i)
Lab Sample ID: 500-143858-9
Date Collected: 04/11/18 11:40
Matrix: Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/23/18 18:41
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/23/18 18:41
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/23/18 18:41
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 18:41
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/23/18 18:41
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/23/18 18:41
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 18:41
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/23/18 18:41
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 18:41
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/23/18 18:41
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/23/18 18:41
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 18:41
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/23/18 18:41
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/23/18 18:41
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/23/18 18:41
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 111 75- 126
4-Bromofluorobenzene (Surr) 92 72 - 124
Dibromofluoromethane 93 75 - 120
Toluene-d8 (Surr) 94 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04123118 18:41
04123118 18:41
04123118 18:41
04/23/18 18:41
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.23
0.75
0.38
0.23
ug/L
04/18/18 01:40
1
Acenaphthylene
<0.20
0.75
0.38
0.20
ug/L
04/18/18 01:40
1
Acetophenone
<0.50
3.8
1.9
0.50
ug/L
04/18/18 01:40
1
2-Acetylaminofluorene
<1.6
7.5
3.8
1.6
ug/L
04/18/18 01:40
1
4-Aminobiphenyl
<2.8
7.5
3.8
2.8
ug/L
04/18/18 01:40
1
Anthracene
<0.25
0.75
0.38
0.25
ug/L
04/18/18 01:40
1
Benzo[a]anthracene
<0.043
0.15
0.075
0.043
ug/L
04/18/18 01:40
1
Benzo[a]pyrene
<0.074
0.15
0.075
0.074
ug/L
04/18/18 01:40
1
Benzo[b]fluoranthene
<0.061
0.15
0.075
0.061
ug/L
04/18/18 01:40
1
Benzo[g,h,i]perylene
<0.28
0.75
0.38
0.28
ug/L
04/18/18 01:40
1
Benzo[k]fluoranthene
<0.048
0.15
0.075
0.048
ug/L
04/18/18 01:40
1
Benzyl alcohol
<4.5
15
7.5
4.5
ug/L
04/18/18 01:40
1
Bis(2-chloroethoxy)methane
<0.21
1.5
0.75
0.21
ug/L
04/18/18 01:40
1
Bis(2-chloroethyl)ether
<0.22
1.5
0.75
0.22
ug/L
04/18/18 01:40
1
Bis(2-ethylhexyl) phthalate
<1.3
7.5
3.8
1.3
ug/L
04/18/18 01:40
1
4-Bromophenyl phenyl ether
<0.41
3.8
1.9
0.41
ug/L
04/18/18 01:40
1
Butyl benzyl phthalate
<0.36
1.5
0.75
0.36
ug/L
04/18/18 01:40
1
4-Chloroaniline
<1.5
7.5
3.8
1.5
ug/L
04/18/18 01:40
1
Chlorobenzilate
<2.6
7.5
3.8
2.6
ug/L
04/18/18 01:40
1
4-Chloro-3-methylphenol
<1.7
7.5
3.8
1.7
ug/L
04/18/18 01:40
1
2-Chloronaphthalene
<0.18
1.5
0.75
0.18
ug/L
04/18/18 01:40
1
2-Chlorophenol
<0.42
3.8
1.9
0.42
ug/L
04/18/18 01:40
1
4-Chlorophenyl phenyl ether
<0.48
3.8
1.9
0.48
ug/L
04/18/18 01:40
1
Chrysene
<0.051
0.15
0.075
0.051
ug/L
04/18/18 01:40
1
Diallate
<4.2
7.5
4.7
4.2
ug/L
04/18/18 01:40
1
Dibenz(a,h)anthracene
<0.038
0.23
0.11
0.038
ug/L
04/18/18 01:40
1
TestAmerica Chicago
Page 60 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-5(i) Lab Sample ID: 500-143858-9
Date Collected: 04/11/18 11:40 Matrix: Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.20
1.5
0.75
0.20
ug/L
04/18/18 01:40
1
3,3'-Dichlorobenzidine
<1.3
3.8
1.9
1.3
ug/L
04/18/18 01:40
1
2,4-Dichlorophenol
<2.0
7.5
3.8
2.0
ug/L
04/18/18 01:40
1
2,6-Dichlorophenol
<2.6
7.5
3.8
2.6
ug/L
04/18/18 01:40
1
Diethyl phthalate
<0.27
3.8
1.5
0.27
ug/L
04/18/18 01:40
1
Dimethoate
<1.4
7.5
3.8
1.4
ug/L
04/18/18 01:40
1
7,12-Dimethylbenz(a)anthracene
<2.3
30
15
2.3
ug/L
04/18/18 01:40
1
3,3'-Dimethylbenzidine
<13
30
15
13
ug/L
04/18/18 01:40
1
2,4-Dimethylphenol
<1.4
7.5
3.8
1.4
ug/L
04/18/18 01:40
1
Dimethyl phthalate
<0.24
3.8
1.5
0.24
ug/L
04/18/18 01:40
1
Di-n-butyl phthalate
<0.55
3.8
1.9
0.55
ug/L
04/18/18 01:40
1
4,6-Dinitro-2-methylphenol
<4.4
15
7.5
4.4
ug/L
04/18/18 01:40
1
2,4-Dinitrophenol
<6.5
15
7.5
6.5
ug/L
04/18/18 01:40
1
2,4-Dinitrotoluene
<0.18
0.75
0.38
0.18
ug/L
04/18/18 01:40
1
2,6-Dinitrotoluene
<0.056
0.75
0.38
0.056
ug/L
04/18/18 01:40
1
Di-n-octyl phthalate
<0.79
7.5
3.8
0.79
ug/L
04/18/18 01:40
1
Diphenylamine
<1.9
7.5
3.8
1.9
ug/L
04/18/18 01:40
1
Disulfoton
<1.4
7.5
3.8
1.4
ug/L
04/18/18 01:40
1
Ethyl methanesulfonate
<2.9
15
7.5
2.9
ug/L
04/18/18 01:40
1
Ethyl Parathion
<1.6
7.5
3.8
1.6
ug/L
04/18/18 01:40
1
Famphur
<23
30
24
23
ug/L
04/18/18 01:40
1
Fluoranthene
<0.34
0.75
0.38
0.34
ug/L
04/18/18 01:40
1
Fluorene
<0.18
0.75
0.38
0.18
ug/L
04/18/18 01:40
1
Hexachlorobenzene
<0.060
0.38
0.19
0.060
ug/L
04/18/18 01:40
1
Hexachlorocyclopentadiene
<4.8
15
7.5
4.8
ug/L
04/18/18 01:40
1
Hexachloroethane
<0.45
3.8
1.9
0.45
ug/L
04/18/18 01:40
1
Hexachloropropene
<3.5
15
7.5
3.5
ug/L
04/18/18 01:40
1
Indeno[1,2,3-cd]pyrene
<0.056
0.15
0.075
0.056
ug/L
04/18/18 01:40
1
Isodrin
<5.2
15
7.5
5.2
ug/L
04/18/18 01:40
1
Isophorone
<0.28
1.5
0.75
0.28
ug/L
04/18/18 01:40
1
Isosafrole
<2.9
7.5
3.8
2.9
ug/L
04/18/18 01:40
1
Kepone
<1.2
7.5
3.8
1.2
ug/L
04/18/18 01:40
1
m-Dinitrobenzene
<1.0
3.8
1.9
1.0
ug/L
04/18/18 01:40
1
Methapyrilene
<7.6
30
15
7.6
ug/L
04/18/18 01:40
1
3-Methylcholanthrene
<1.7
7.5
3.8
1.7
ug/L
04/18/18 01:40
1
Methyl methanesulfonate
<4.5
30
15
4.5
ug/L
04/18/18 01:40
1
2-Methylnaphthalene
<0.049
1.5
0.75
0.049
ug/L
04/18/18 01:40
1
Methyl parathion
<1.8
7.5
3.8
1.8
ug/L
04/18/18 01:40
1
2-Methylphenol
<0.23
1.5
0.75
0.23
ug/L
04/18/18 01:40
1
3 & 4 Methylphenol
<0.34
1.5
0.75
0.34
ug/L
04/18/18 01:40
1
Naphthalene
<0.23
0.75
0.38
0.23
ug/L
04/18/18 01:40
1
1,4-Naphthoquinone
<29
30
30
29
ug/L
04/18/18 01:40
1
1-Naphthylamine
<4.5
15
7.5
4.5
ug/L
04/18/18 01:40
1
2-Naphthylamine
<6.9
15
7.5
6.9
ug/L
04/18/18 01:40
1
2-Nitroaniline
<0.97
3.8
1.9
0.97
ug/L
04/18/18 01:40
1
3-Nitroaniline
<1.3
7.5
3.8
1.3
ug/L
04/18/18 01:40
1
4-Nitroaniline
<1.3
7.5
3.8
1.3
ug/L
04/18/18 01:40
1
Nitrobenzene
<0.34
0.75
0.38
0.34
ug/L
04/18/18 01:40
1
5-Nitro-o-toluidine
<2.3
7.5
3.8
2.3
ug/L
04/18/18 01:40
1
TestAmerica Chicago
Page 61 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-5(i)
Lab Sample
ID: 500-143858-9
Date Collected: 04/11/18 11:40
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<1.9
7.5
3.8
1.9
ug/L
04/18/18 01:40
1
4-Nitrophenol
<5.6
15
7.5
5.6
ug/L
04/18/18 01:40
1
N-Nitrosodiethylamine
<6.5
15
7.5
6.5
ug/L
04/18/18 01:40
1
N-Nitrosodimethylamine
<3.6
7.5
3.8
3.6
ug/L
04/18/18 01:40
1
N-Nitrosodi-n-butylamine
<3.2
7.5
3.8
3.2
ug/L
04/18/18 01:40
1
N-Nitrosodi-n-propylamine
<0.12
0.38
0.19
0.12
ug/L
04/18/18 01:40
1
N-Nitrosodiphenylamine
<0.28
1.5
0.75
0.28
ug/L
04/18/18 01:40
1
N-Nitrosomethylethylamine
<5.6
15
7.5
5.6
ug/L
04/18/18 01:40
1
N-Nitrosopiperidine
<2.6
7.5
3.8
2.6
ug/L
04/18/18 01:40
1
N-Nitrosopyrrolidine
<2.5
7.5
3.8
2.5
ug/L
04/18/18 01:40
1
o,o',o"-Triethylphosphorothioate
<4.2
15
7.5
4.2
ug/L
04/18/18 01:40
1
o-Toluidine
<6.0
30
15
6.0
ug/L
04/18/18 01:40
1
2,2'-oxybis[l-chloropropane]
<0.29
1.5
0.75
0.29
ug/L
04/18/18 01:40
1
p-Dimethylamino azobenzene
<2.3
7.5
3.8
2.3
ug/L
04/18/18 01:40
1
Pentachlorobenzene
<2.1
7.5
3.8
2.1
ug/L
04/18/18 01:40
1
Pentachloronitrobenzene
<2.7
7.5
3.8
2.7
ug/L
04/18/18 01:40
1
Phenacetin
<1.7
7.5
3.8
1.7
ug/L
04/18/18 01:40
1
Phenanthrene
<0.23
0.75
0.38
0.23
ug/L
04/18/18 01:40
1
Phenol
<0.51
3.8
1.9
0.51
ug/L
04/18/18 01:40
1
Phorate
<1.6
7.5
3.8
1.6
ug/L
04/18/18 01:40
1
p-Phenylene diamine
<12
60
30
12
ug/L
04/18/18 01:40
1
Pronamide
<1.6
7.5
7.5
1.6
ug/L
04/18/18 01:40
1
Pyrene
<0.32
0.75
0.38
0.32
ug/L
04/18/18 01:40
1
Safrole
<3.0
7.5
3.8
3.0
ug/L
04/18/18 01:40
1
sym-Trinitrobenzene
<1.4
7.5
3.8
1.4
ug/L
04/18/18 01:40
1
2,3,7,8-TCDD (Screen)
<7.5
7.5
7.5
7.5
ug/L
04/18/18 01:40
1
1,2,4,5-Tetrachlorobenzene
<0.43
3.8
1.9
0.43
ug/L
04/18/18 01:40
1
2,3,4,6-Tetrachlorophenol
<0.56
3.8
1.9
0.56
ug/L
04/18/18 01:40
1
Thionazin
<1.9
7.5
3.8
1.9
ug/L
04/18/18 01:40
1
2,4,5-Trichlorophenol
<1.9
7.5
3.8
1.9
ug/L
04/18/18 01:40
1
2,4,6-Trichlorophenol
<0.54
3.8
1.9
0.54
ug/L
04/18/18 01:40
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
90
34 - 110
04116118 16:56
04118118 01:40
1
2-Fluorophenol
72
27- 110
04116118 16:56
04118118 01:40
1
Nitrobenzene-d5
95
36 - 120
04116118 16:56
04118118 01:40
1
Phenol-d5
64
20- 100
04116118 16:56
04118118 01:40
1
Terphenyl-d14
100
40- 145
04116118 16:56
04118118 01:40
1
2,4,6-Tribromophenol
107
40- 145
04116118 16:56
04118118 01:40
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
alpha-BHC
<0.0025
0.039
0.019
0.0025
ug/L
04/20/18 15:03
1
beta-BHC
<0.0099
0.039
0.019
0.0099
ug/L
04/20/18 15:03
1
delta-BHC
<0.010
0.039
0.019
0.010
ug/L
04/20/18 15:03
1
gamma-BHC (Lindane)
<0.0054
0.039
0.019
0.0054
ug/L
04/20/18 15:03
1
Heptachlor
<0.013
0.039
0.019
0.013
ug/L
04/20/18 15:03
1
Aldrin
<0.0051
0.039
0.019
0.0051
ug/L
04/20/18 15:03
1
Heptachlor epoxide
<0.013
0.039
0.019
0.013
ug/L
04/20/18 15:03
1
Endosulfan 1
<0.0040
0.039
0.019
0.0040
ug/L
04/20/18 15:03
1
TestAmerica Chicago
Page 62 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-5(i)
Lab Sample
ID: 500-143858-9
Date Collected: 04/11/18 11:40
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.013
0.039
0.019
0.013
ug/L
04/20/18 15:03
1
4,4'-DDE
<0.0037
0.039
0.019
0.0037
ug/L
04/20/18 15:03
1
Endrin
<0.014
0.039
0.019
0.014
ug/L
04/20/18 15:03
1
Endosulfan II
<0.0027
0.039
0.019
0.0027
ug/L
04/20/18 15:03
1
4,4'-DDD
<0.013
0.039
0.019
0.013
ug/L
04/20/18 15:03
1
Endosulfan sulfate
<0.011
0.039
0.019
0.011
ug/L
04/20/18 15:03
1
4,4'-DDT
<0.0031
0.039
0.019
0.0031
ug/L
04/20/18 15:03
1
Methoxychlor
<0.022
0.078
0.039
0.022
ug/L
04/20/18 15:03
1
Toxaphene
<0.19
0.39
0.19
0.19
ug/L
04/20/18 15:03
1
Endrin aldehyde
<0.0080
0.039
0.019
0.0080
ug/L
04/20/18 15:03
1
Chlordane (technical)
<0.039
0.078
0.039
0.039
ug/L
04/20/18 15:03
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
95
30 - 130
04117118 07:38
04120118 15:03
1
Tetrachloro-m-xylene
76
30 - 120
04117118 07:38
04120118 15:03
1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.065
0.39
0.19
0.065
ug/L
04/17/1819:49
1
PCB-1221
<0.19
0.39
0.19
0.19
ug/L
04/17/1819:49
1
PCB-1232
<0.19
0.39
0.19
0.19
ug/L
04/17/1819:49
1
PCB-1242
<0.19
0.39
0.19
0.19
ug/L
04/17/1819:49
1
PCB-1248
<0.19
0.39
0.19
0.19
ug/L
04/17/1819:49
1
PCB-1254
<0.19
0.39
0.19
0.19
ug/L
04/17/1819:49
1
PCB-1260
<0.068
0.39
0.19
0.068
ug/L
04/17/1819:49
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
64
30 - 120
04117118 07:38
04117118 19:49
1
DCB Decachlorobiphenyl
77
30 - 140
04117118 07:38
04117118 19:49
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.45
0.97
0.48
0.45
ug/L
04/18/18 01:22
1
Dinoseb
<0.16
1.9
0.97
0.16
ug/L
04/18/18 01:22
1
Pentachlorophenol
<0.087
0.48
0.097
0.087
ug/L
04/18/18 01:22
1
Silvex (2,4,5-TP)
<0.28
0.97
0.48
0.28
ug/L
04/18/18 01:22
1
2,4,5-T
<0.42
0.97
0.48
0.42
ug/L
04/18/18 01:22
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
68
25 - 130
04117118 09:02
04118118 01:22
1
Method: 6020B - Metals (ICP/MS)
- Total Recoverable
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 03:05
1
Arsenic
0.43 J
1.0
0.50
0.23
ug/L
04/21/18 03:05
1
Barium
280
2.5
1.3
0.73
ug/L
04/21/18 03:05
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 03:05
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 03:05
1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 03:05
1
Cobalt
0.48 J
1.0
0.50
0.40
ug/L
04/21/18 03:05
1
Copper
0.76 J B
2.0
1.0
0.50
ug/L
04/21/18 03:05
1
TestAmerica Chicago
Page 63 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill
- Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-5(i)
Lab Sample ID: 500-143858-9
Date Collected: 04/11/18 11:40
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Iron
38000
100
50
47
ug/L
04/21/18 03:05
1
Lead
0.24 J
0.50
0.25
0.19
ug/L
04/21/18 03:05
1
Manganese
3800
2.5
1.3
0.79
ug/L
04/21/18 03:05
1
Nickel
1.4 J
2.0
1.0
0.63
ug/L
04/21/18 03:05
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 03:05
1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 03:05
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 03:05
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 03:05
1
Vanadium
2.2 J
5.0
2.5
2.2
ug/L
04/21/18 03:05
1
Zinc
<6.9
10
20
6.9
ug/L
04/21/18 03:05
1
Method: 7470A - Mercury (CVAA)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/18/1811:02
1
General Chemistry
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/25/18 09:58
1
Chloride
28000
2000
1700
1700
ug/L
04/27/1818:51
10
Sulfate
84000
2000
1000
950
ug/L
04/26/1819:12
10
Alkalinity
420000
5000
5000
3700
ug/L
04/23/1814:20
1
Total Dissolved Solids
660000
10000
10000
4300
ug/L
04/17/18 08:08
1
TestAmerica Chicago
Page 64 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-9(i) Lab Sample ID: 500-143858-10
Date Collected: 04/10/18 14:10 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/23/18 19:09
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/23/18 19:09
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/23/18 19:09
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/23/18 19:09
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 19:09
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 19:09
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/23/18 19:09
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 19:09
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/23/18 19:09
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/23/18 19:09
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 19:09
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/23/18 19:09
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 19:09
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 19:09
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/23/18 19:09
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/23/18 19:09
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 19:09
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/23/18 19:09
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/23/18 19:09
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/23/18 19:09
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/23/18 19:09
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/23/18 19:09
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/23/18 19:09
1
Acetone
7.2 cn
5.0
2.5
1.7
ug/L
04/23/18 19:09
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/23/18 19:09
1
Acrolein
<23
100
50
23
ug/L
04/23/18 19:09
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/23/18 19:09
1
Benzene
1.5
0.50
0.25
0.15
ug/L
04/23/18 19:09
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 19:09
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/23/18 19:09
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/23/18 19:09
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/23/18 19:09
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/23/18 19:09
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/23/18 19:09
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 19:09
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/23/18 19:09
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/23/18 19:09
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/23/18 19:09
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/23/18 19:09
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/23/18 19:09
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/23/18 19:09
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/23/18 19:09
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/23/18 19:09
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/23/18 19:09
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/23/18 19:09
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/23/18 19:09
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/23/18 19:09
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/23/18 19:09
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/23/18 19:09
1
TestAmerica Chicago
Page 65 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-9(i)
Lab Sample
ID: 500-143858-10
Date Collected: 04/10/18 14:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/23/18 19:09
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/23/18 19:09
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/23/18 19:09
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 19:09
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/23/18 19:09
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/23/18 19:09
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 19:09
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/23/18 19:09
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 19:09
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/23/18 19:09
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/23/18 19:09
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 19:09
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/23/18 19:09
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/23/18 19:09
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/23/18 19:09
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 109 75- 126
4-Bromofluorobenzene (Surr) 94 72 - 124
Dibromofluoromethane 95 75 - 120
Toluene-d8 (Surr) 94 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04123118 19:09
04123118 19:09
04123118 19:09
04/23/18 19:09
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.26
0.84
0.42
0.26
ug/L
04/20/18 14:50
1
Acenaphthylene
<0.22
0.84
0.42
0.22
ug/L
04/20/18 14:50
1
Acetophenone
<0.56
4.2
2.1
0.56
ug/L
04/20/18 14:50
1
2-Acetylaminofluorene
<1.8
8.4
4.2
1.8
ug/L
04/20/18 14:50
1
4-Aminobiphenyl
<3.1
8.4
4.2
3.1
ug/L
04/20/18 14:50
1
Anthracene
<0.28
0.84
0.42
0.28
ug/L
04/20/18 14:50
1
Benzo[a]anthracene
<0.047
0.17
0.084
0.047
ug/L
04/20/18 14:50
1
Benzo[a]pyrene
<0.083
0.17
0.084
0.083
ug/L
04/20/18 14:50
1
Benzo[b]fluoranthene
<0.067
0.17
0.084
0.067
ug/L
04/20/18 14:50
1
Benzo[g,h,i]perylene
<0.31
0.84
0.42
0.31
ug/L
04/20/18 14:50
1
Benzo[k]fluoranthene
<0.054
0.17
0.084
0.054
ug/L
04/20/18 14:50
1
Benzyl alcohol
<5.1
17
8.4
5.1
ug/L
04/20/18 14:50
1
Bis(2-chloroethoxy)methane
<0.24
1.7
0.84
0.24
ug/L
04/20/18 14:50
1
Bis(2-chloroethyl)ether
<0.24
1.7
0.84
0.24
ug/L
04/20/18 14:50
1
Bis(2-ethylhexyl) phthalate
<1.4
8.4
4.2
1.4
ug/L
04/20/18 14:50
1
4-Bromophenyl phenyl ether
<0.45
4.2
2.1
0.45
ug/L
04/20/18 14:50
1
Butyl benzyl phthalate
<0.40
1.7
0.84
0.40
ug/L
04/20/18 14:50
1
4-Chloroaniline
<1.7
8.4
4.2
1.7
ug/L
04/20/18 14:50
1
Chlorobenzilate
<2.8
8.4
4.2
2.8
ug/L
04/20/18 14:50
1
4-Chloro-3-methylphenol
<1.9
8.4
4.2
1.9
ug/L
04/20/18 14:50
1
2-Chloronaphthalene
<0.20
1.7
0.84
0.20
ug/L
04/20/18 14:50
1
2-Chlorophenol
<0.47
4.2
2.1
0.47
ug/L
04/20/18 14:50
1
4-Chlorophenyl phenyl ether
<0.53
4.2
2.1
0.53
ug/L
04/20/18 14:50
1
Chrysene
<0.057
0.17
0.084
0.057
ug/L
04/20/18 14:50
1
Diallate
<4.6
8.4
5.2
4.6
ug/L
04/20/18 14:50
1
Dibenz(a,h)anthracene
<0.042
0.25
0.13
0.042
ug/L
04/20/18 14:50
1
TestAmerica Chicago
Page 66 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-9(i) Lab Sample ID: 500-143858-10
Date Collected: 04/10/18 14:10 Matrix: Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.22
1.7
0.84
0.22
ug/L
04/20/18 14:50
1
3,3'-Dichlorobenzidine
<1.4
4.2
2.1
1.4
ug/L
04/20/18 14:50
1
2,4-Dichlorophenol
<2.2
8.4
4.2
2.2
ug/L
04/20/18 14:50
1
2,6-Dichlorophenol
<2.9
8.4
4.2
2.9
ug/L
04/20/18 14:50
1
Diethyl phthalate
<0.30
4.2
1.7
0.30
ug/L
04/20/18 14:50
1
Dimethoate
<1.6
8.4
4.2
1.6
ug/L
04/20/18 14:50
1
7,12-Dimethylbenz(a)anthracene
<2.5
33
17
2.5
ug/L
04/20/18 14:50
1
3,3'-Dimethylbenzidine
<15
33
17
15
ug/L
04/20/18 14:50
1
2,4-Dimethylphenol
<1.5
8.4
4.2
1.5
ug/L
04/20/18 14:50
1
Dimethyl phthalate
<0.26
4.2
1.7
0.26
ug/L
04/20/18 14:50
1
Di-n-butyl phthalate
0.90 J
4.2
2.1
0.61
ug/L
04/20/18 14:50
1
4,6-Dinitro-2-methylphenol
<4.9
17
8.4
4.9
ug/L
04/20/18 14:50
1
2,4-Dinitrophenol
<7.2
17
8.4
7.2
ug/L
04/20/18 14:50
1
2,4-Dinitrotoluene
<0.21
0.84
0.42
0.21
ug/L
04/20/18 14:50
1
2,6-Dinitrotoluene
<0.062
0.84
0.42
0.062
ug/L
04/20/18 14:50
1
Di-n-octyl phthalate
<0.88
8.4
4.2
0.88
ug/L
04/20/18 14:50
1
Diphenylamine
<2.1
8.4
4.2
2.1
ug/L
04/20/18 14:50
1
Disulfoton
<1.6
8.4
4.2
1.6
ug/L
04/20/18 14:50
1
Ethyl methanesulfonate
<3.2
17
8.4
3.2
ug/L
04/20/18 14:50
1
Ethyl Parathion
<1.7
8.4
4.2
1.7
ug/L
04/20/18 14:50
1
Famphur
<25
33
26
25
ug/L
04/20/18 14:50
1
Fluoranthene
<0.38
0.84
0.42
0.38
ug/L
04/20/18 14:50
1
Fluorene
<0.20
0.84
0.42
0.20
ug/L
04/20/18 14:50
1
Hexachlorobenzene
<0.066
0.42
0.21
0.066
ug/L
04/20/18 14:50
1
Hexachlorocyclopentadiene
<5.3
17
8.4
5.3
ug/L
04/20/18 14:50
1
Hexachloroethane
<0.50
4.2
2.1
0.50
ug/L
04/20/18 14:50
1
Hexachloropropene
<3.9
17
8.4
3.9
ug/L
04/20/18 14:50
1
Indeno[1,2,3-cd]pyrene
<0.063
0.17
0.084
0.063
ug/L
04/20/18 14:50
1
Isodrin
<5.8
17
8.4
5.8
ug/L
04/20/18 14:50
1
Isophorone
<0.31
1.7
0.84
0.31
ug/L
04/20/18 14:50
1
Isosafrole
<3.2
8.4
4.2
3.2
ug/L
04/20/18 14:50
1
Kepone
<1.4
8.4
4.2
1.4
ug/L
04/20/18 14:50
1
m-Dinitrobenzene
<1.1
4.2
2.1
1.1
ug/L
04/20/18 14:50
1
Methapyrilene
<8.5
33
17
8.5
ug/L
04/20/18 14:50
1
3-Methylcholanthrene
<1.9
8.4
4.2
1.9
ug/L
04/20/18 14:50
1
Methyl methanesulfonate
<5.0
33
17
5.0
ug/L
04/20/18 14:50
1
2-Methylnaphthalene
<0.055
1.7
0.84
0.055
ug/L
04/20/18 14:50
1
Methyl parathion
<1.9
8.4
4.2
1.9
ug/L
04/20/18 14:50
1
2-Methylphenol
<0.26
1.7
0.84
0.26
ug/L
04/20/18 14:50
1
3 & 4 Methylphenol
<0.38
1.7
0.84
0.38
ug/L
04/20/18 14:50
1
Naphthalene
<0.26
0.84
0.42
0.26
ug/L
04/20/18 14:50
1
1,4-Naphthoquinone
<33
33
33
33
ug/L
04/20/18 14:50
1
1-Naphthylamine
<4.9
17
8.4
4.9
ug/L
04/20/18 14:50
1
2-Naphthylamine
<7.6
17
8.4
7.6
ug/L
04/20/18 14:50
1
2-Nitroaniline
<1.1
4.2
2.1
1.1
ug/L
04/20/18 14:50
1
3-Nitroaniline
<1.5
8.4
4.2
1.5
ug/L
04/20/18 14:50
1
4-Nitroaniline
<1.4
8.4
4.2
1.4
ug/L
04/20/18 14:50
1
Nitrobenzene
<0.38
0.84
0.42
0.38
ug/L
04/20/18 14:50
1
5-Nitro-o-toluidine
<2.6
8.4
4.2
2.6
ug/L
04/20/18 14:50
1
TestAmerica Chicago
Page 67 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-9(i)
Lab Sample ID: 500-143858-10
Date Collected: 04/10/18 14:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<2.1
8.4
4.2
2.1
ug/L
04/20/18 14:50
1
4-Nitrophenol
<6.2
17
8.4
6.2
ug/L
04/20/18 14:50
1
N-Nitrosodiethylamine
<7.2
17
8.4
7.2
ug/L
04/20/18 14:50
1
N-Nitrosodimethylamine
<4.0
8.4
4.2
4.0
ug/L
04/20/18 14:50
1
N-Nitrosodi-n-butylamine
<3.5
8.4
4.2
3.5
ug/L
04/20/18 14:50
1
N-Nitrosodi-n-propylamine
<0.13
0.42
0.21
0.13
ug/L
04/20/18 14:50
1
N-Nitrosodiphenylamine
<0.31
1.7
0.84
0.31
ug/L
04/20/18 14:50
1
N-Nitrosomethylethylamine
<6.3
17
8.4
6.3
ug/L
04/20/18 14:50
1
N-Nitrosopiperidine
<2.9
8.4
4.2
2.9
ug/L
04/20/18 14:50
1
N-Nitrosopyrrolidine
<2.8
8.4
4.2
2.8
ug/L
04/20/18 14:50
1
o,o',o"-Triethylphosphorothioate
<4.6
17
8.4
4.6
ug/L
04/20/18 14:50
1
o-Toluidine
<6.6
33
17
6.6
ug/L
04/20/18 14:50
1
2,2'-oxybis[l-chloropropane]
<0.32
1.7
0.84
0.32
ug/L
04/20/18 14:50
1
p-Dimethylamino azobenzene
<2.5
8.4
4.2
2.5
ug/L
04/20/18 14:50
1
Pentachlorobenzene
<2.3
8.4
4.2
2.3
ug/L
04/20/18 14:50
1
Pentachloronitrobenzene
<3.0
8.4
4.2
3.0
ug/L
04/20/18 14:50
1
Phenacetin
<1.9
8.4
4.2
1.9
ug/L
04/20/18 14:50
1
Phenanthrene
<0.25
0.84
0.42
0.25
ug/L
04/20/18 14:50
1
Phenol
<0.56
4.2
2.1
0.56
ug/L
04/20/18 14:50
1
Phorate
<1.8
8.4
4.2
1.8
ug/L
04/20/18 14:50
1
p-Phenylene diamine
<14
67
33
14
ug/L
04/20/18 14:50
1
Pronamide
<1.8
8.4
8.4
1.8
ug/L
04/20/18 14:50
1
Pyrene
<0.36
0.84
0.42
0.36
ug/L
04/20/18 14:50
1
Safrole
<3.3
8.4
4.2
3.3
ug/L
04/20/18 14:50
1
sym-Trinitrobenzene
<1.6
8.4
4.2
1.6
ug/L
04/20/18 14:50
1
2,3,7,8-TCDD (Screen)
<8.4
8.4
8.4
8.4
ug/L
04/20/18 14:50
1
1,2,4,5-Tetrachlorobenzene
<0.48
4.2
2.1
0.48
ug/L
04/20/18 14:50
1
2,3,4,6-Tetrachlorophenol
<0.62
4.2
2.1
0.62
ug/L
04/20/18 14:50
1
Thionazin
<2.2
8.4
4.2
2.2
ug/L
04/20/18 14:50
1
2,4,5-Trichlorophenol
<2.1
8.4
4.2
2.1
ug/L
04/20/18 14:50
1
2,4,6-Trichlorophenol
<0.60
4.2
2.1
0.60
ug/L
04/20/18 14:50
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
78
34 - 110
04116118 16:56
04120118 14:50
1
2-Fluorophenol
46
27- 110
04116118 16:56
04120118 14:50
1
Nitrobenzene-d5
71
36 - 120
04116118 16:56
04120118 14:50
1
Phenol-d5
35
20- 100
04116118 16:56
04120118 14:50
1
Terphenyl-d14
129
40- 145
04116118 16:56
04120118 14:50
1
2,4,6-Tribromophenol
93
40- 145
04116118 16:56
04120118 14:50
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
alpha-BHC
<0.0026
0.040
0.020
0.0026
ug/L
04/20/18 15:23
1
beta-BHC
<0.010
0.040
0.020
0.010
ug/L
04/20/18 15:23
1
delta-BHC
<0.010
0.040
0.020
0.010
ug/L
04/20/18 15:23
1
gamma-BHC (Lindane)
<0.0056
0.040
0.020
0.0056
ug/L
04/20/18 15:23
1
Heptachlor
<0.013
0.040
0.020
0.013
ug/L
04/20/18 15:23
1
Aldrin
<0.0053
0.040
0.020
0.0053
ug/L
04/20/18 15:23
1
Heptachlor epoxide
<0.014
0.040
0.020
0.014
ug/L
04/20/18 15:23
1
Endosulfan 1
<0.0041
0.040
0.020
0.0041
ug/L
04/20/18 15:23
1
TestAmerica Chicago
Page 68 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-9(i)
Lab Sample ID: 500-143858-10
Date Collected: 04/10/18 14:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.013
0.040
0.020
0.013
ug/L
04/20/18 15:23
1
4,4'-DDE
<0.0038
0.040
0.020
0.0038
ug/L
04/20/18 15:23
1
Endrin
<0.014
0.040
0.020
0.014
ug/L
04/20/18 15:23
1
Endosulfan II
<0.0028
0.040
0.020
0.0028
ug/L
04/20/18 15:23
1
4,4'-DDD
<0.013
0.040
0.020
0.013
ug/L
04/20/18 15:23
1
Endosulfan sulfate
<0.012
0.040
0.020
0.012
ug/L
04/20/18 15:23
1
4,4'-DDT
<0.0032
0.040
0.020
0.0032
ug/L
04/20/18 15:23
1
Methoxychlor
<0.023
0.080
0.040
0.023
ug/L
04/20/18 15:23
1
Toxaphene
<0.20
0.40
0.20
0.20
ug/L
04/20/18 15:23
1
Endrin aldehyde
<0.0082
0.040
0.020
0.0082
ug/L
04/20/18 15:23
1
Chlordane (technical)
<0.040
0.080
0.040
0.040
ug/L
04/20/18 15:23
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
57
30 - 130
04117118 07:38
04120118 15:23
1
Tetrachloro-m-xylene
102
30 - 120
04117118 07:38
04120118 15:23
1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.067
0.40
0.20
0.067
ug/L
04/17/18 20:06
1
PCB-1221
<0.20
0.40
0.20
0.20
ug/L
04/17/18 20:06
1
PCB-1232
<0.20
0.40
0.20
0.20
ug/L
04/17/18 20:06
1
PCB-1242
<0.20
0.40
0.20
0.20
ug/L
04/17/18 20:06
1
PCB-1248
<0.20
0.40
0.20
0.20
ug/L
04/17/18 20:06
1
PCB-1254
<0.20
0.40
0.20
0.20
ug/L
04/17/18 20:06
1
PCB-1260
<0.070
0.40
0.20
0.070
ug/L
04/17/18 20:06
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
65
30 - 120
04117118 07:38
04117118 20:06
1
DCB Decachlorobiphenyl
84
30 - 140
04117118 07:38
04117118 20:06
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.45
0.96
0.48
0.45
ug/L
04/18/18 02:35
1
Dinoseb
<0.16
1.9
0.96
0.16
ug/L
04/18/18 02:35
1
Pentachlorophenol
<0.086
0.48
0.096
0.086
ug/L
04/18/18 02:35
1
Silvex (2,4,5-TP)
<0.28
0.96
0.48
0.28
ug/L
04/18/18 02:35
1
2,4,5-T
<0.42
0.96
0.48
0.42
ug/L
04/18/18 02:35
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
96
25 - 130
04117118 09:02
04118118 02:35
1
Method: 6020B - Metals (ICP/MS)
- Total Recoverable
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 03:09
1
Arsenic
0.56 J
1.0
0.50
0.23
ug/L
04/21/18 03:09
1
Barium
480
2.5
1.3
0.73
ug/L
04/21/18 03:09
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 03:09
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 03:09
1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 03:09
1
Cobalt
5.1
1.0
0.50
0.40
ug/L
04/21/18 03:09
1
Copper
0.69 J B
2.0
1.0
0.50
ug/L
04/21/18 03:09
1
TestAmerica Chicago
Page 69 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill
- Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-9(i)
Lab Sample
ID: 500-143858-10
Date Collected: 04/10/18 14:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Iron
1500
100
50
47
ug/L
04/21/18 03:09
1
Lead
<0.19
0.50
0.25
0.19
ug/L
04/21/18 03:09
1
Manganese
220
2.5
1.3
0.79
ug/L
04/21/18 03:09
1
Nickel
5.1
2.0
1.0
0.63
ug/L
04/21/18 03:09
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 03:09
1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 03:09
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 03:09
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 03:09
1
Vanadium
4.7 J
5.0
2.5
2.2
ug/L
04/21/18 03:09
1
Zinc
<6.9
10
20
6.9
ug/L
04/21/18 03:09
1
Method: 7470A - Mercury (CVAA)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/18/1811:04
1
General Chemistry
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/24/18 15:56
1
Chloride
52000
2000
1700
1700
ug/L
04/27/1819:03
10
Sulfate
40000
2000
1000
950
ug/L
04/26/1819:25
10
Alkalinity
670000
5000
5000
3700
ug/L
04/23/1816:13
1
Total Dissolved Solids
840000
10000
10000
4300
ug/L
04/17/18 08:11
1
TestAmerica Chicago
Page 70 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-9D(i) Lab Sample ID: 500-143858-11
Date Collected: 04/10/18 13:30 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/23/18 19:38
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/23/18 19:38
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/23/18 19:38
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/23/18 19:38
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 19:38
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 19:38
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/23/18 19:38
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 19:38
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/23/18 19:38
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/23/18 19:38
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 19:38
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/23/18 19:38
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 19:38
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 19:38
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/23/18 19:38
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/23/18 19:38
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 19:38
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/23/18 19:38
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/23/18 19:38
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/23/18 19:38
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/23/18 19:38
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/23/18 19:38
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/23/18 19:38
1
Acetone
9.0 cn
5.0
2.5
1.7
ug/L
04/23/18 19:38
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/23/18 19:38
1
Acrolein
<23
100
50
23
ug/L
04/23/18 19:38
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/23/18 19:38
1
Benzene
0.47 J
0.50
0.25
0.15
ug/L
04/23/18 19:38
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 19:38
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/23/18 19:38
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/23/18 19:38
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/23/18 19:38
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/23/18 19:38
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/23/18 19:38
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 19:38
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/23/18 19:38
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/23/18 19:38
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/23/18 19:38
1
cis-1,2-Dichloroethene
2.4
1.0
0.50
0.41
ug/L
04/23/18 19:38
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/23/18 19:38
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/23/18 19:38
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/23/18 19:38
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/23/18 19:38
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/23/18 19:38
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/23/18 19:38
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/23/18 19:38
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/23/18 19:38
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/23/18 19:38
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/23/18 19:38
1
TestAmerica Chicago
Page 71 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-91)(i)
Lab Sample
ID: 500-143858-11
Date Collected: 04/10/18 13:30
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/23/18 19:38
1
Methylene Chloride
4.3 J cn
5.0
2.5
1.6
ug/L
04/23/18 19:38
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/23/18 19:38
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 19:38
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/23/18 19:38
1
Tetrahydrofuran
12
10
5.0
1.9
ug/L
04/23/18 19:38
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 19:38
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/23/18 19:38
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 19:38
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/23/18 19:38
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/23/18 19:38
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 19:38
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/23/18 19:38
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/23/18 19:38
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/23/18 19:38
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 110 75- 226
4-Bromofluorobenzene (Surr) 93 72 - 124
Dibromofluoromethane 96 75 - 120
Toluene-d8 (Surr) 93 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04123118 19:38
04123118 19:38
04123118 19:38
04/23/18 19:38
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.24
0.78
0.39
0.24
ug/L
04/19/18 16:58
1
Acenaphthylene
<0.21
0.78
0.39
0.21
ug/L
04/19/18 16:58
1
Acetophenone
<0.52
3.9
2.0
0.52
ug/L
04/19/18 16:58
1
2-Acetylaminofluorene
<1.7
7.8
3.9
1.7
ug/L
04/19/18 16:58
1
4-Aminobiphenyl
<2.9
7.8
3.9
2.9
ug/L
04/19/18 16:58
1
Anthracene
<0.26
0.78
0.39
0.26
ug/L
04/19/18 16:58
1
Benzo[a]anthracene
<0.044
0.16
0.078
0.044
ug/L
04/19/18 16:58
1
Benzo[a]pyrene
<0.077
0.16
0.078
0.077
ug/L
04/19/18 16:58
1
Benzo[b]fluoranthene
<0.063
0.16
0.078
0.063
ug/L
04/19/18 16:58
1
Benzo[g,h,i]perylene
<0.29
0.78
0.39
0.29
ug/L
04/19/18 16:58
1
Benzo[k]fluoranthene
<0.050
0.16
0.078
0.050
ug/L
04/19/18 16:58
1
Benzyl alcohol
<4.7
16
7.8
4.7
ug/L
04/19/18 16:58
1
Bis(2-chloroethoxy)methane
<0.22
1.6
0.78
0.22
ug/L
04/19/18 16:58
1
Bis(2-chloroethyl)ether
<0.23
1.6
0.78
0.23
ug/L
04/19/18 16:58
1
Bis(2-ethylhexyl) phthalate
<1.3
7.8
3.9
1.3
ug/L
04/19/18 16:58
1
4-Bromophenyl phenyl ether
<0.42
3.9
2.0
0.42
ug/L
04/19/18 16:58
1
Butyl benzyl phthalate
<0.38
1.6
0.78
0.38
ug/L
04/19/18 16:58
1
4-Chloroaniline
<1.6
7.8
3.9
1.6
ug/L
04/19/18 16:58
1
Chlorobenzilate
<2.7
7.8
3.9
2.7
ug/L
04/19/18 16:58
1
4-Chloro-3-methylphenol
<1.8
7.8
3.9
1.8
ug/L
04/19/18 16:58
1
2-Chloronaphthalene
<0.18
1.6
0.78
0.18
ug/L
04/19/18 16:58
1
2-Chlorophenol
<0.44
3.9
2.0
0.44
ug/L
04/19/18 16:58
1
4-Chlorophenyl phenyl ether
<0.50
3.9
2.0
0.50
ug/L
04/19/18 16:58
1
Chrysene
<0.053
0.16
0.078
0.053
ug/L
04/19/18 16:58
1
Diallate
<4.3
7.8
4.9
4.3
ug/L
04/19/18 16:58
1
Dibenz(a,h)anthracene
<0.040
0.23
0.12
0.040
ug/L
04/19/18 16:58
1
TestAmerica Chicago
Page 72 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-91)(i) Lab Sample ID: 500-143858-11
Date Collected: 04/10/18 13:30 Matrix: Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.21
1.6
0.78
0.21
ug/L
04/19/18 16:58
1
3,3'-Dichlorobenzidine
<1.3
3.9
2.0
1.3
ug/L
04/19/18 16:58
1
2,4-Dichlorophenol
<2.0
7.8
3.9
2.0
ug/L
04/19/18 16:58
1
2,6-Dichlorophenol
<2.7
7.8
3.9
2.7
ug/L
04/19/18 16:58
1
Diethyl phthalate
<0.28
3.9
1.6
0.28
ug/L
04/19/18 16:58
1
Dimethoate
<1.5
7.8
3.9
1.5
ug/L
04/19/18 16:58
1
7,12-Dimethylbenz(a)anthracene
<2.4
31
16
2.4
ug/L
04/19/18 16:58
1
3,3'-Dimethylbenzidine
<14
31
16
14
ug/L
04/19/18 16:58
1
2,4-Dimethylphenol
<1.4
7.8
3.9
1.4
ug/L
04/19/18 16:58
1
Dimethyl phthalate
<0.25
3.9
1.6
0.25
ug/L
04/19/18 16:58
1
Di-n-butyl phthalate
0.73 J
3.9
2.0
0.57
ug/L
04/19/18 16:58
1
4,6-Dinitro-2-methylphenol
<4.6
16
7.8
4.6
ug/L
04/19/18 16:58
1
2,4-Dinitrophenol
<6.7
16
7.8
6.7
ug/L
04/19/18 16:58
1
2,4-Dinitrotoluene
<0.19
0.78
0.39
0.19
ug/L
04/19/18 16:58
1
2,6-Dinitrotoluene
<0.058
0.78
0.39
0.058
ug/L
04/19/18 16:58
1
Di-n-octyl phthalate
<0.82
7.8
3.9
0.82
ug/L
04/19/18 16:58
1
Diphenylamine
<2.0
7.8
3.9
2.0
ug/L
04/19/18 16:58
1
Disulfoton
<1.5
7.8
3.9
1.5
ug/L
04/19/18 16:58
1
Ethyl methanesulfonate
<3.0
16
7.8
3.0
ug/L
04/19/18 16:58
1
Ethyl Parathion
<1.6
7.8
3.9
1.6
ug/L
04/19/18 16:58
1
Famphur
<24
31
24
24
ug/L
04/19/18 16:58
1
Fluoranthene
<0.35
0.78
0.39
0.35
ug/L
04/19/18 16:58
1
Fluorene
<0.19
0.78
0.39
0.19
ug/L
04/19/18 16:58
1
Hexachlorobenzene
<0.062
0.39
0.20
0.062
ug/L
04/19/18 16:58
1
Hexachlorocyclopentadiene
<5.0
16
7.8
5.0
ug/L
04/19/18 16:58
1
Hexachloroethane
<0.47
3.9
2.0
0.47
ug/L
04/19/18 16:58
1
Hexachloropropene
<3.7
16
7.8
3.7
ug/L
04/19/18 16:58
1
Indeno[1,2,3-cd]pyrene
<0.058
0.16
0.078
0.058
ug/L
04/19/18 16:58
1
Isodrin
<5.4
16
7.8
5.4
ug/L
04/19/18 16:58
1
Isophorone
<0.29
1.6
0.78
0.29
ug/L
04/19/18 16:58
1
Isosafrole
<3.0
7.8
3.9
3.0
ug/L
04/19/18 16:58
1
Kepone
<1.3
7.8
3.9
1.3
ug/L
04/19/18 16:58
1
m-Dinitrobenzene
<1.0
3.9
2.0
1.0
ug/L
04/19/18 16:58
1
Methapyrilene
<7.9
31
16
7.9
ug/L
04/19/18 16:58
1
3-Methylcholanthrene
<1.8
7.8
3.9
1.8
ug/L
04/19/18 16:58
1
Methyl methanesulfonate
<4.6
31
16
4.6
ug/L
04/19/18 16:58
1
2-Methylnaphthalene
<0.051
1.6
0.78
0.051
ug/L
04/19/18 16:58
1
Methyl parathion
<1.8
7.8
3.9
1.8
ug/L
04/19/18 16:58
1
2-Methylphenol
<0.24
1.6
0.78
0.24
ug/L
04/19/18 16:58
1
3 & 4 Methylphenol
<0.35
1.6
0.78
0.35
ug/L
04/19/18 16:58
1
Naphthalene
<0.24
0.78
0.39
0.24
ug/L
04/19/18 16:58
1
1,4-Naphthoquinone
<31
31
31
31
ug/L
04/19/18 16:58
1
1-Naphthylamine
<4.6
16
7.8
4.6
ug/L
04/19/18 16:58
1
2-Naphthylamine
<7.1
16
7.8
7.1
ug/L
04/19/18 16:58
1
2-Nitroaniline
<1.0
3.9
2.0
1.0
ug/L
04/19/18 16:58
1
3-Nitroaniline
<1.4
7.8
3.9
1.4
ug/L
04/19/18 16:58
1
4-Nitroaniline
<1.3
7.8
3.9
1.3
ug/L
04/19/18 16:58
1
Nitrobenzene
<0.35
0.78
0.39
0.35
ug/L
04/19/18 16:58
1
5-Nitro-o-toluidine
<2.4
7.8
3.9
2.4
ug/L
04/19/18 16:58
1
TestAmerica Chicago
Page 73 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-91)(i)
Lab Sample ID: 500-143858-11
Date Collected: 04/10/18 13:30
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<2.0
7.8
3.9
2.0
ug/L
04/19/18 16:58
1
4-Nitrophenol
<5.8
16
7.8
5.8
ug/L
04/19/18 16:58
1
N-Nitrosodiethylamine
<6.7
16
7.8
6.7
ug/L
04/19/18 16:58
1
N-Nitrosodimethylamine
<3.7
7.8
3.9
3.7
ug/L
04/19/18 16:58
1
N-Nitrosodi-n-butylamine
<3.3
7.8
3.9
3.3
ug/L
04/19/18 16:58
1
N-Nitrosodi-n-propylamine
<0.12
0.39
0.20
0.12
ug/L
04/19/18 16:58
1
N-Nitrosodiphenylamine
<0.29
1.6
0.78
0.29
ug/L
04/19/18 16:58
1
N-Nitrosomethylethylamine
<5.9
16
7.8
5.9
ug/L
04/19/18 16:58
1
N-Nitrosopiperidine
<2.7
7.8
3.9
2.7
ug/L
04/19/18 16:58
1
N-Nitrosopyrrolidine
<2.6
7.8
3.9
2.6
ug/L
04/19/18 16:58
1
o,o',o"-Triethylphosphorothioate
<4.3
16
7.8
4.3
ug/L
04/19/18 16:58
1
o-Toluidine
<6.2
31
16
6.2
ug/L
04/19/18 16:58
1
2,2'-oxybis[l-chloropropane]
<0.30
1.6
0.78
0.30
ug/L
04/19/18 16:58
1
p-Dimethylamino azobenzene
<2.3
7.8
3.9
2.3
ug/L
04/19/18 16:58
1
Pentachlorobenzene
<2.2
7.8
3.9
2.2
ug/L
04/19/18 16:58
1
Pentachloronitrobenzene
<2.8
7.8
3.9
2.8
ug/L
04/19/18 16:58
1
Phenacetin
<1.8
7.8
3.9
1.8
ug/L
04/19/18 16:58
1
Phenanthrene
<0.24
0.78
0.39
0.24
ug/L
04/19/18 16:58
1
Phenol
<0.53
3.9
2.0
0.53
ug/L
04/19/18 16:58
1
Phorate
<1.7
7.8
3.9
1.7
ug/L
04/19/18 16:58
1
p-Phenylene diamine
<13
63
31
13
ug/L
04/19/18 16:58
1
Pronamide
<1.7
7.8
7.8
1.7
ug/L
04/19/18 16:58
1
Pyrene
<0.33
0.78
0.39
0.33
ug/L
04/19/18 16:58
1
Safrole
<3.1
7.8
3.9
3.1
ug/L
04/19/18 16:58
1
sym-Trinitrobenzene
<1.5
7.8
3.9
1.5
ug/L
04/19/18 16:58
1
2,3,7,8-TCDD (Screen)
<7.8
7.8
7.8
7.8
ug/L
04/19/18 16:58
1
1,2,4,5-Tetrachlorobenzene
<0.45
3.9
2.0
0.45
ug/L
04/19/18 16:58
1
2,3,4,6-Tetrachlorophenol
<0.58
3.9
2.0
0.58
ug/L
04/19/18 16:58
1
Thionazin
<2.0
7.8
3.9
2.0
ug/L
04/19/18 16:58
1
2,4,5-Trichlorophenol
<2.0
7.8
3.9
2.0
ug/L
04/19/18 16:58
1
2,4,6-Trichlorophenol
<0.56
3.9
2.0
0.56
ug/L
04/19/18 16:58
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
75
34 - 110
04116118 16:56
04119118 16:58
1
2-Fluorophenol
50
27- 110
04116118 16:56
04119118 16:58
1
Nitrobenzene-d5
68
36 - 120
04116118 16:56
04119118 16:58
1
Phenol-d5
34
20- 100
04116118 16:56
04119118 16:58
1
Terphenyl-d14
110
40- 145
04116118 16:56
04119118 16:58
1
2,4,6-Tribromophenol
88
40- 145
04116118 16:56
04119118 16:58
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
alpha-BHC
<0.0025
beta-BHC
<0.0097
delta-BHC
<0.0098
gamma-BHC (Lindane)
<0.0053
Heptachlor
<0.013
Aldrin
<0.0050
Heptachlor epoxide
<0.013
Endosulfan 1
<0.0039
RL
LOD
MDL
Unit
D Analyzed
0.038
0.019
0.0025
ug/L
04/20/1815:42
0.038
0.019
0.0097
ug/L
04/20/1815:42
0.038
0.019
0.0098
ug/L
04/20/1815:42
0.038
0.019
0.0053
ug/L
04/20/1815:42
0.038
0.019
0.013
ug/L
04/20/1815:42
0.038
0.019
0.0050
ug/L
04/20/1815:42
0.038
0.019
0.013
ug/L
04/20/1815:42
0.038
0.019
0.0039
ug/L
04/20/1815:42
Dil Fac
1
1
1
1
1
1
1
1
Page 74 of 258
TestAmerica Chicago
7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-91)(i)
Lab Sample ID: 500-143858-11
Date Collected: 04/10/18 13:30
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.012
0.038
0.019
0.012
ug/L
04/20/18 15:42
1
4,4'-DDE
<0.0036
0.038
0.019
0.0036
ug/L
04/20/18 15:42
1
Endrin
<0.013
0.038
0.019
0.013
ug/L
04/20/18 15:42
1
Endosulfan II
<0.0027
0.038
0.019
0.0027
ug/L
04/20/18 15:42
1
4,4'-DDD
<0.013
0.038
0.019
0.013
ug/L
04/20/18 15:42
1
Endosulfan sulfate
<0.011
0.038
0.019
0.011
ug/L
04/20/18 15:42
1
4,4'-DDT
<0.0030
0.038
0.019
0.0030
ug/L
04/20/18 15:42
1
Methoxychlor
<0.022
0.076
0.038
0.022
ug/L
04/20/18 15:42
1
Toxaphene
<0.19
0.38
0.19
0.19
ug/L
04/20/18 15:42
1
Endrin aldehyde
<0.0078
0.038
0.019
0.0078
ug/L
04/20/18 15:42
1
Chlordane (technical)
<0.038
0.076
0.038
0.038
ug/L
04/20/18 15:42
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
44
30 - 130
04117118 07:38
04120118 15:42
1
Tetrachloro-m-xylene
64
30 - 120
04117118 07:38
04120118 15:42
1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.064
0.38
0.19
0.064
ug/L
04/17/18 20:22
1
PCB-1221
<0.19
0.38
0.19
0.19
ug/L
04/17/18 20:22
1
PCB-1232
<0.19
0.38
0.19
0.19
ug/L
04/17/18 20:22
1
PCB-1242
<0.19
0.38
0.19
0.19
ug/L
04/17/18 20:22
1
PCB-1248
<0.19
0.38
0.19
0.19
ug/L
04/17/18 20:22
1
PCB-1254
<0.19
0.38
0.19
0.19
ug/L
04/17/18 20:22
1
PCB-1260
<0.067
0.38
0.19
0.067
ug/L
04/17/18 20:22
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
64
30 - 120
04117118 07:38
04117118 20:22
1
DCB Decachlorobiphenyl
84
30 - 140
04117118 07:38
04117118 20:22
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.45
0.96
0.48
0.45
ug/L
04/18/18 03:00
1
Dinoseb
<0.16
1.9
0.96
0.16
ug/L
04/18/18 03:00
1
Pentachlorophenol
<0.086
0.48
0.096
0.086
ug/L
04/18/18 03:00
1
Silvex (2,4,5-TP)
<0.28
0.96
0.48
0.28
ug/L
04/18/18 03:00
1
2,4,5-T
<0.42
0.96
0.48
0.42
ug/L
04/18/18 03:00
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
87
25 - 130
04117118 09:02
04118118 03:00
1
Method: 6020B - Metals (ICP/MS) - Total Recoverable
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 03:20
1
Arsenic
0.58 J
1.0
0.50
0.23
ug/L
04/21/18 03:20
1
Barium
290
2.5
1.3
0.73
ug/L
04/21/18 03:20
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 03:20
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 03:20
1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 03:20
1
Cobalt
<0.40
1.0
0.50
0.40
ug/L
04/21/18 03:20
1
Copper
0.74 J B
2.0
1.0
0.50
ug/L
04/21/18 03:20
1
TestAmerica Chicago
Page 75 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-91)(i)
Lab Sample
ID: 500-143858-11
Date Collected: 04/10/18 13:30
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 6020B - Metals (ICP/MS) -
Total Recoverable (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Iron
400
100
50
47
ug/L
04/21/18 03:20
1
Lead
<0.19
0.50
0.25
0.19
ug/L
04/21/18 03:20
1
Manganese
470
2.5
1.3
0.79
ug/L
04/21/18 03:20
1
Nickel
2.3
2.0
1.0
0.63
ug/L
04/21/18 03:20
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 03:20
1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 03:20
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 03:20
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 03:20
1
Vanadium
<2.2
5.0
2.5
2.2
ug/L
04/21/18 03:20
1
Zinc
<6.9
10
20
6.9
ug/L
04/21/18 03:20
1
Method: 7470A - Mercury (CVAA)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/18/1811:06
1
General Chemistry
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/24/18 15:57
1
Chloride
36000 F1
2000
1700
1700
ug/L
04/27/1819:16
10
Sulfate
66000
2000
1000
950
ug/L
04/26/1819:38
10
Alkalinity
800000
5000
5000
3700
ug/L
04/23/1816:24
1
Total Dissolved Solids
1000000
10000
10000
4300
ug/L
04/17/18 08:13
1
TestAmerica Chicago
Page 76 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-10(i) Lab Sample ID: 500-143858-12
Date Collected: 04/11/18 10:50 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result
Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/23/18 20:07
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/23/18 20:07
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/23/18 20:07
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/23/18 20:07
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 20:07
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 20:07
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/23/18 20:07
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 20:07
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/23/18 20:07
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/23/18 20:07
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 20:07
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/23/18 20:07
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 20:07
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 20:07
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/23/18 20:07
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/23/18 20:07
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 20:07
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/23/18 20:07
1
2-Butanone (MEK)
<2.1
F2
5.0
2.5
2.1
ug/L
04/23/18 20:07
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/23/18 20:07
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/23/18 20:07
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/23/18 20:07
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/23/18 20:07
1
Acetone
2.3
J cn
5.0
2.5
1.7
ug/L
04/23/18 20:07
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/23/18 20:07
1
Acrolein
<23
100
50
23
ug/L
04/23/18 20:07
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/23/18 20:07
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 20:07
1
Bromochloromethane
<0.43
F2
1.0
0.50
0.43
ug/L
04/23/18 20:07
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/23/18 20:07
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/23/18 20:07
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/23/18 20:07
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/23/18 20:07
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/23/18 20:07
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 20:07
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/23/18 20:07
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/23/18 20:07
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/23/18 20:07
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/23/18 20:07
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/23/18 20:07
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/23/18 20:07
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/23/18 20:07
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/23/18 20:07
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/23/18 20:07
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/23/18 20:07
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/23/18 20:07
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/23/18 20:07
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/23/18 20:07
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/23/18 20:07
1
TestAmerica Chicago
Page 77 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-10(i)
Lab Sample
ID: 500-143858-12
Date Collected: 04/11/18 10:50
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/23/18 20:07
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/23/18 20:07
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/23/18 20:07
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 20:07
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/23/18 20:07
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/23/18 20:07
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 20:07
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/23/18 20:07
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 20:07
1
trans- 1,4-Dichloro-2-butene
<1.2 F2
5.0
5.0
1.2
ug/L
04/23/18 20:07
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/23/18 20:07
1
Trichlorofluoromethane
<0.43 F1
1.0
0.50
0.43
ug/L
04/23/18 20:07
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/23/18 20:07
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/23/18 20:07
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/23/18 20:07
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 113 75- 126
4-Bromofluorobenzene (Surr) 95 72 - 124
Dibromofluoromethane 95 75 - 120
Toluene-d8 (Surr) 95 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04123118 20:07
04123118 20:07
04123118 20:07
04/23/18 20:07
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.26
0.83
0.42
0.26
ug/L
04/20/18 15:15
1
Acenaphthylene
<0.22
0.83
0.42
0.22
ug/L
04/20/18 15:15
1
Acetophenone
<0.55
4.2
2.1
0.55
ug/L
04/20/18 15:15
1
2-Acetylaminofluorene
<1.8
8.3
4.2
1.8
ug/L
04/20/18 15:15
1
4-Aminobiphenyl
<3.1
8.3
4.2
3.1
ug/L
04/20/18 15:15
1
Anthracene
<0.28
0.83
0.42
0.28
ug/L
04/20/18 15:15
1
Benzo[a]anthracene
<0.047
0.17
0.083
0.047
ug/L
04/20/18 15:15
1
Benzo[a]pyrene
<0.082
0.17
0.083
0.082
ug/L
04/20/18 15:15
1
Benzo[b]fluoranthene
<0.067
0.17
0.083
0.067
ug/L
04/20/18 15:15
1
Benzo[g,h,i]perylene
<0.31
0.83
0.42
0.31
ug/L
04/20/18 15:15
1
Benzo[k]fluoranthene
<0.053
0.17
0.083
0.053
ug/L
04/20/18 15:15
1
Benzyl alcohol
<5.0
17
8.3
5.0
ug/L
04/20/18 15:15
1
Bis(2-chloroethoxy)methane
<0.24
1.7
0.83
0.24
ug/L
04/20/18 15:15
1
Bis(2-chloroethyl)ether
<0.24
1.7
0.83
0.24
ug/L
04/20/18 15:15
1
Bis(2-ethylhexyl) phthalate
<1.4
8.3
4.2
1.4
ug/L
04/20/18 15:15
1
4-Bromophenyl phenyl ether
<0.45
4.2
2.1
0.45
ug/L
04/20/18 15:15
1
Butyl benzyl phthalate
<0.40
1.7
0.83
0.40
ug/L
04/20/18 15:15
1
4-Chloroaniline
<1.7
8.3
4.2
1.7
ug/L
04/20/18 15:15
1
Chlorobenzilate
<2.8
8.3
4.2
2.8
ug/L
04/20/18 15:15
1
4-Chloro-3-methylphenol
<1.9
8.3
4.2
1.9
ug/L
04/20/18 15:15
1
2-Chloronaphthalene
<0.20
1.7
0.83
0.20
ug/L
04/20/18 15:15
1
2-Chlorophenol
<0.47
4.2
2.1
0.47
ug/L
04/20/18 15:15
1
4-Chlorophenyl phenyl ether
<0.53
4.2
2.1
0.53
ug/L
04/20/18 15:15
1
Chrysene
<0.057
0.17
0.083
0.057
ug/L
04/20/18 15:15
1
Diallate
<4.6
8.3
5.2
4.6
ug/L
04/20/18 15:15
1
Dibenz(a,h)anthracene
<0.042
0.25
0.13
0.042
ug/L
04/20/18 15:15
1
TestAmerica Chicago
Page 78 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-10(i) Lab Sample ID: 500-143858-12
Date Collected: 04/11/18 10:50 Matrix: Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.22
1.7
0.83
0.22
ug/L
04/20/18 15:15
1
3,3'-Dichlorobenzidine
<1.4
4.2
2.1
1.4
ug/L
04/20/18 15:15
1
2,4-Dichlorophenol
<2.2
8.3
4.2
2.2
ug/L
04/20/18 15:15
1
2,6-Dichlorophenol
<2.9
8.3
4.2
2.9
ug/L
04/20/18 15:15
1
Diethyl phthalate
<0.30
4.2
1.7
0.30
ug/L
04/20/18 15:15
1
Dimethoate
<1.6
8.3
4.2
1.6
ug/L
04/20/18 15:15
1
7,12-Dimethylbenz(a)anthracene
<2.5
33
17
2.5
ug/L
04/20/18 15:15
1
3,3'-Dimethylbenzidine
<15
33
17
15
ug/L
04/20/18 15:15
1
2,4-Dimethylphenol
<1.5
8.3
4.2
1.5
ug/L
04/20/18 15:15
1
Dimethyl phthalate
<0.26
4.2
1.7
0.26
ug/L
04/20/18 15:15
1
Di-n-butyl phthalate
<0.61
4.2
2.1
0.61
ug/L
04/20/18 15:15
1
4,6-Dinitro-2-methylphenol
<4.9
17
8.3
4.9
ug/L
04/20/18 15:15
1
2,4-Dinitrophenol
<7.2
17
8.3
7.2
ug/L
04/20/18 15:15
1
2,4-Dinitrotoluene
<0.20
0.83
0.42
0.20
ug/L
04/20/18 15:15
1
2,6-Dinitrotoluene
<0.061
0.83
0.42
0.061
ug/L
04/20/18 15:15
1
Di-n-octyl phthalate
<0.88
8.3
4.2
0.88
ug/L
04/20/18 15:15
1
Diphenylamine
<2.1
8.3
4.2
2.1
ug/L
04/20/18 15:15
1
Disulfoton
<1.6
8.3
4.2
1.6
ug/L
04/20/18 15:15
1
Ethyl methanesulfonate
<3.2
17
8.3
3.2
ug/L
04/20/18 15:15
1
Ethyl Parathion
<1.7
8.3
4.2
1.7
ug/L
04/20/18 15:15
1
Famphur
<25
33
26
25
ug/L
04/20/18 15:15
1
Fluoranthene
<0.38
0.83
0.42
0.38
ug/L
04/20/18 15:15
1
Fluorene
<0.20
0.83
0.42
0.20
ug/L
04/20/18 15:15
1
Hexachlorobenzene
<0.066
0.42
0.21
0.066
ug/L
04/20/18 15:15
1
Hexachlorocyclopentadiene
<5.3
17
8.3
5.3
ug/L
04/20/18 15:15
1
Hexachloroethane
<0.50
4.2
2.1
0.50
ug/L
04/20/18 15:15
1
Hexachloropropene
<3.9
17
8.3
3.9
ug/L
04/20/18 15:15
1
Indeno[1,2,3-cd]pyrene
<0.062
0.17
0.083
0.062
ug/L
04/20/18 15:15
1
Isodrin
<5.8
17
8.3
5.8
ug/L
04/20/18 15:15
1
Isophorone
<0.31
1.7
0.83
0.31
ug/L
04/20/18 15:15
1
Isosafrole
<3.2
8.3
4.2
3.2
ug/L
04/20/18 15:15
1
Kepone
<1.4
8.3
4.2
1.4
ug/L
04/20/18 15:15
1
m-Dinitrobenzene
<1.1
4.2
2.1
1.1
ug/L
04/20/18 15:15
1
Methapyrilene
<8.4
33
17
8.4
ug/L
04/20/18 15:15
1
3-Methylcholanthrene
<1.9
8.3
4.2
1.9
ug/L
04/20/18 15:15
1
Methyl methanesulfonate
<4.9
33
17
4.9
ug/L
04/20/18 15:15
1
2-Methylnaphthalene
<0.054
1.7
0.83
0.054
ug/L
04/20/18 15:15
1
Methyl parathion
<1.9
8.3
4.2
1.9
ug/L
04/20/18 15:15
1
2-Methylphenol
<0.25
1.7
0.83
0.25
ug/L
04/20/18 15:15
1
3 & 4 Methylphenol
<0.37
1.7
0.83
0.37
ug/L
04/20/18 15:15
1
Naphthalene
<0.26
0.83
0.42
0.26
ug/L
04/20/18 15:15
1
1,4-Naphthoquinone
<33
33
33
33
ug/L
04/20/18 15:15
1
1-Naphthylamine
<4.9
17
8.3
4.9
ug/L
04/20/18 15:15
1
2-Naphthylamine
<7.6
17
8.3
7.6
ug/L
04/20/18 15:15
1
2-Nitroaniline
<1.1
4.2
2.1
1.1
ug/L
04/20/18 15:15
1
3-Nitroaniline
<1.5
8.3
4.2
1.5
ug/L
04/20/18 15:15
1
4-Nitroaniline
<1.4
8.3
4.2
1.4
ug/L
04/20/18 15:15
1
Nitrobenzene
<0.37
0.83
0.42
0.37
ug/L
04/20/18 15:15
1
5-Nitro-o-toluidine
<2.6
8.3
4.2
2.6
ug/L
04/20/18 15:15
1
TestAmerica Chicago
Page 79 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-10(i)
Lab Sample ID: 500-143858-12
Date Collected: 04/11/18 10:50
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<2.1
8.3
4.2
2.1
ug/L
04/20/18 15:15
1
4-Nitrophenol
<6.2
17
8.3
6.2
ug/L
04/20/18 15:15
1
N-Nitrosodiethylamine
<7.2
17
8.3
7.2
ug/L
04/20/18 15:15
1
N-Nitrosodimethylamine
<4.0
8.3
4.2
4.0
ug/L
04/20/18 15:15
1
N-Nitrosodi-n-butylamine
<3.5
8.3
4.2
3.5
ug/L
04/20/18 15:15
1
N-Nitrosodi-n-propylamine
<0.13
0.42
0.21
0.13
ug/L
04/20/18 15:15
1
N-Nitrosodiphenylamine
<0.31
1.7
0.83
0.31
ug/L
04/20/18 15:15
1
N-Nitrosomethylethylamine
<6.2
17
8.3
6.2
ug/L
04/20/18 15:15
1
N-Nitrosopiperidine
<2.9
8.3
4.2
2.9
ug/L
04/20/18 15:15
1
N-Nitrosopyrrolidine
<2.8
8.3
4.2
2.8
ug/L
04/20/18 15:15
1
o,o',o"-Triethylphosphorothioate
<4.6
17
8.3
4.6
ug/L
04/20/18 15:15
1
o-Toluidine
<6.6
33
17
6.6
ug/L
04/20/18 15:15
1
2,2'-oxybis[l-chloropropane]
<0.32
1.7
0.83
0.32
ug/L
04/20/18 15:15
1
p-Dimethylamino azobenzene
<2.5
8.3
4.2
2.5
ug/L
04/20/18 15:15
1
Pentachlorobenzene
<2.3
8.3
4.2
2.3
ug/L
04/20/18 15:15
1
Pentachloronitrobenzene
<3.0
8.3
4.2
3.0
ug/L
04/20/18 15:15
1
Phenacetin
<1.9
8.3
4.2
1.9
ug/L
04/20/18 15:15
1
Phenanthrene
<0.25
0.83
0.42
0.25
ug/L
04/20/18 15:15
1
Phenol
<0.56
4.2
2.1
0.56
ug/L
04/20/18 15:15
1
Phorate
<1.8
8.3
4.2
1.8
ug/L
04/20/18 15:15
1
p-Phenylene diamine
<14
67
33
14
ug/L
04/20/18 15:15
1
Pronamide
<1.8
8.3
8.3
1.8
ug/L
04/20/18 15:15
1
Pyrene
<0.36
0.83
0.42
0.36
ug/L
04/20/18 15:15
1
Safrole
<3.3
8.3
4.2
3.3
ug/L
04/20/18 15:15
1
sym-Trinitrobenzene
<1.6
8.3
4.2
1.6
ug/L
04/20/18 15:15
1
2,3,7,8-TCDD (Screen)
<8.3
8.3
8.3
8.3
ug/L
04/20/18 15:15
1
1,2,4,5-Tetrachlorobenzene
<0.48
4.2
2.1
0.48
ug/L
04/20/18 15:15
1
2,3,4,6-Tetrachlorophenol
<0.62
4.2
2.1
0.62
ug/L
04/20/18 15:15
1
Thionazin
<2.2
8.3
4.2
2.2
ug/L
04/20/18 15:15
1
2,4,5-Trichlorophenol
<2.1
8.3
4.2
2.1
ug/L
04/20/18 15:15
1
2,4,6-Trichlorophenol
<0.60
4.2
2.1
0.60
ug/L
04/20/18 15:15
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
104
34 - 110
04116118 16:56
04120118 15:15
1
2-Fluorophenol
73
27- 110
04116118 16:56
04120118 15:15
1
Nitrobenzene-d5
101
36 - 120
04116118 16:56
04120118 15:15
1
Phenol-d5
51
20- 100
04116118 16:56
04120118 15:15
1
Terphenyl-d14
146 X
40- 145
04116118 16:56
04120118 15:15
1
2,4,6-Tribromophenol
101
40- 145
04116118 16:56
04120118 15:15
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
alpha-BHC
<0.0027
0.041
0.021
0.0027
ug/L
04/20/18 16:01
1
beta-BHC
<0.011
0.041
0.021
0.011
ug/L
04/20/18 16:01
1
delta-BHC
<0.011
0.041
0.021
0.011
ug/L
04/20/18 16:01
1
gamma-BHC (Lindane)
<0.0058
0.041
0.021
0.0058
ug/L
04/20/18 16:01
1
Heptachlor
<0.014
0.041
0.021
0.014
ug/L
04/20/18 16:01
1
Aldrin
<0.0055
0.041
0.021
0.0055
ug/L
04/20/18 16:01
1
Heptachlor epoxide
<0.014
0.041
0.021
0.014
ug/L
04/20/18 16:01
1
Endosulfan 1
<0.0042
0.041
0.021
0.0042
ug/L
04/20/18 16:01
1
TestAmerica Chicago
Page 80 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-10(i)
Lab Sample ID: 500-143858-12
Date Collected: 04/11/18 10:50
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.013
0.041
0.021
0.013
ug/L
04/20/18 16:01
1
4,4'-DDE
<0.0039
0.041
0.021
0.0039
ug/L
04/20/18 16:01
1
Endrin
<0.015
0.041
0.021
0.015
ug/L
04/20/18 16:01
1
Endosulfan II
<0.0029
0.041
0.021
0.0029
ug/L
04/20/18 16:01
1
4,4'-DDD
<0.014
0.041
0.021
0.014
ug/L
04/20/18 16:01
1
Endosulfan sulfate
<0.012
0.041
0.021
0.012
ug/L
04/20/18 16:01
1
4,4'-DDT
<0.0033
0.041
0.021
0.0033
ug/L
04/20/18 16:01
1
Methoxychlor
<0.024
0.083
0.041
0.024
ug/L
04/20/18 16:01
1
Toxaphene
<0.21
0.41
0.21
0.21
ug/L
04/20/18 16:01
1
Endrin aldehyde
<0.0085
0.041
0.021
0.0085
ug/L
04/20/18 16:01
1
Chlordane (technical)
<0.041
0.083
0.041
0.041
ug/L
04/20/18 16:01
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
65
30 - 130
04117118 07:38
04120118 16:01
1
Tetrachloro-m-xylene
67
30 - 120
04117118 07:38
04120118 16:01
1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.069
0.41
0.21
0.069
ug/L
04/17/18 20:38
1
PCB-1221
<0.21
0.41
0.21
0.21
ug/L
04/17/18 20:38
1
PCB-1232
<0.21
0.41
0.21
0.21
ug/L
04/17/18 20:38
1
PCB-1242
<0.21
0.41
0.21
0.21
ug/L
04/17/18 20:38
1
PCB-1248
<0.21
0.41
0.21
0.21
ug/L
04/17/18 20:38
1
PCB-1254
<0.21
0.41
0.21
0.21
ug/L
04/17/18 20:38
1
PCB-1260
<0.072
0.41
0.21
0.072
ug/L
04/17/18 20:38
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
67
30 - 120
04117118 07:38
04117118 20:38
1
DCB Decachlorobiphenyl
73
30 - 140
04117118 07:38
04117118 20:38
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.45
0.97
0.49
0.45
ug/L
04/18/18 03:24
1
Dinoseb
<0.16
1.9
0.97
0.16
ug/L
04/18/18 03:24
1
Pentachlorophenol
<0.087
0.49
0.097
0.087
ug/L
04/18/18 03:24
1
Silvex (2,4,5-TP)
<0.28
0.97
0.49
0.28
ug/L
04/18/18 03:24
1
2,4,5-T
<0.42
0.97
0.49
0.42
ug/L
04/18/18 03:24
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
77
25 - 130
04117118 09:02
04118118 03:24
1
General Chemistry
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/25/18 09:57
1
Chloride
20000
2000
1700
1700
ug/L
04/27/1819:53
10
Sulfate
120000
4000
2000
1900
ug/L
04/27/18 20:30
20
Alkalinity
290000
5000
5000
3700
ug/L
04/23/1816:31
1
Total Dissolved Solids
570000
10000
10000
4300
ug/L
04/17/18 08:16
1
TestAmerica Chicago
Page 81 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-8(i) Lab Sample ID: 500-143858-13
Date Collected: 04/10/18 15:15 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/24/18 14:00
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/24/18 14:00
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/24/18 14:00
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/24/18 14:00
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 14:00
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 14:00
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/24/18 14:00
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 14:00
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/24/18 14:00
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/24/18 14:00
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 14:00
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/24/18 14:00
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 14:00
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 14:00
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/24/18 14:00
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/24/18 14:00
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 14:00
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/24/18 14:00
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/24/18 14:00
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/24/18 14:00
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/24/18 14:00
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/24/18 14:00
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/24/18 14:00
1
Acetone
5.5 cn
5.0
2.5
1.7
ug/L
04/24/18 14:00
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/24/18 14:00
1
Acrolein
<23
100
50
23
ug/L
04/24/18 14:00
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/24/18 14:00
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/24/18 14:00
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 14:00
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/24/18 14:00
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/24/18 14:00
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/24/18 14:00
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/24/18 14:00
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/24/18 14:00
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 14:00
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/24/18 14:00
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/24/18 14:00
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/24/18 14:00
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/24/18 14:00
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/24/18 14:00
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/24/18 14:00
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/24/18 14:00
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/24/18 14:00
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/24/18 14:00
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/24/18 14:00
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/24/18 14:00
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/24/18 14:00
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/24/18 14:00
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/24/18 14:00
1
TestAmerica Chicago
Page 82 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-8(i)
Lab Sample
ID: 500-143858-13
Date Collected: 04/10/18 15:15
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/24/18 14:00
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/24/18 14:00
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/24/18 14:00
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 14:00
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/24/18 14:00
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/24/18 14:00
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/24/18 14:00
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/24/18 14:00
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 14:00
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/24/18 14:00
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/24/18 14:00
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 14:00
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/24/18 14:00
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/24/18 14:00
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/24/18 14:00
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 100 75- 126
4-Bromofluorobenzene (Surr) 106 72 - 124
Dibromofluoromethane 88 75 - 120
Toluene-d8 (Surr) 96 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04124118 14:00
04124118 14:00
04124118 14:00
04124118 14:00
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.23
0.76
0.38
0.23
ug/L
04/20/18 15:41
1
Acenaphthylene
<0.20
0.76
0.38
0.20
ug/L
04/20/18 15:41
1
Acetophenone
<0.51
3.8
1.9
0.51
ug/L
04/20/18 15:41
1
2-Acetylaminofluorene
<1.6
7.6
3.8
1.6
ug/L
04/20/18 15:41
1
4-Aminobiphenyl
<2.9
7.6
3.8
2.9
ug/L
04/20/18 15:41
1
Anthracene
<0.25
0.76
0.38
0.25
ug/L
04/20/18 15:41
1
Benzo[a]anthracene
<0.043
0.15
0.076
0.043
ug/L
04/20/18 15:41
1
Benzo[a]pyrene
<0.075
0.15
0.076
0.075
ug/L
04/20/18 15:41
1
Benzo[b]fluoranthene
<0.061
0.15
0.076
0.061
ug/L
04/20/18 15:41
1
Benzo[g,h,i]perylene
<0.29
0.76
0.38
0.29
ug/L
04/20/18 15:41
1
Benzo[k]fluoranthene
<0.049
0.15
0.076
0.049
ug/L
04/20/18 15:41
1
Benzyl alcohol
<4.6
15
7.6
4.6
ug/L
04/20/18 15:41
1
Bis(2-chloroethoxy)methane
<0.22
1.5
0.76
0.22
ug/L
04/20/18 15:41
1
Bis(2-chloroethyl)ether
<0.22
1.5
0.76
0.22
ug/L
04/20/18 15:41
1
Bis(2-ethylhexyl) phthalate
<1.3
7.6
3.8
1.3
ug/L
04/20/18 15:41
1
4-Bromophenyl phenyl ether
<0.41
3.8
1.9
0.41
ug/L
04/20/18 15:41
1
Butyl benzyl phthalate
<0.37
1.5
0.76
0.37
ug/L
04/20/18 15:41
1
4-Chloroaniline
<1.5
7.6
3.8
1.5
ug/L
04/20/18 15:41
1
Chlorobenzilate
<2.6
7.6
3.8
2.6
ug/L
04/20/18 15:41
1
4-Chloro-3-methylphenol
<1.8
7.6
3.8
1.8
ug/L
04/20/18 15:41
1
2-Chloronaphthalene
<0.18
1.5
0.76
0.18
ug/L
04/20/18 15:41
1
2-Chlorophenol
<0.43
3.8
1.9
0.43
ug/L
04/20/18 15:41
1
4-Chlorophenyl phenyl ether
<0.48
3.8
1.9
0.48
ug/L
04/20/18 15:41
1
Chrysene
<0.052
0.15
0.076
0.052
ug/L
04/20/18 15:41
1
Diallate
<4.2
7.6
4.8
4.2
ug/L
04/20/18 15:41
1
Dibenz(a,h)anthracene
<0.039
0.23
0.11
0.039
ug/L
04/20/18 15:41
1
TestAmerica Chicago
Page 83 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-8(i) Lab Sample ID: 500-143858-13
Date Collected: 04/10/18 15:15 Matrix: Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.20
1.5
0.76
0.20
ug/L
04/20/18 15:41
1
3,3'-Dichlorobenzidine
<1.3
3.8
1.9
1.3
ug/L
04/20/18 15:41
1
2,4-Dichlorophenol
<2.0
7.6
3.8
2.0
ug/L
04/20/18 15:41
1
2,6-Dichlorophenol
<2.7
7.6
3.8
2.7
ug/L
04/20/18 15:41
1
Diethyl phthalate
<0.27
3.8
1.5
0.27
ug/L
04/20/18 15:41
1
Dimethoate
<1.4
7.6
3.8
1.4
ug/L
04/20/18 15:41
1
7,12-Dimethylbenz(a)anthracene
<2.3
30
15
2.3
ug/L
04/20/18 15:41
1
3,3'-Dimethylbenzidine
<14
30
15
14
ug/L
04/20/18 15:41
1
2,4-Dimethylphenol
<1.4
7.6
3.8
1.4
ug/L
04/20/18 15:41
1
Dimethyl phthalate
<0.24
3.8
1.5
0.24
ug/L
04/20/18 15:41
1
Di-n-butyl phthalate
0.56 J
3.8
1.9
0.56
ug/L
04/20/18 15:41
1
4,6-Dinitro-2-methylphenol
<4.5
15
7.6
4.5
ug/L
04/20/18 15:41
1
2,4-Dinitrophenol
<6.5
15
7.6
6.5
ug/L
04/20/18 15:41
1
2,4-Dinitrotoluene
<0.19
0.76
0.38
0.19
ug/L
04/20/18 15:41
1
2,6-Dinitrotoluene
<0.056
0.76
0.38
0.056
ug/L
04/20/18 15:41
1
Di-n-octyl phthalate
<0.80
7.6
3.8
0.80
ug/L
04/20/18 15:41
1
Diphenylamine
<1.9
7.6
3.8
1.9
ug/L
04/20/18 15:41
1
Disulfoton
<1.5
7.6
3.8
1.5
ug/L
04/20/18 15:41
1
Ethyl methanesulfonate
<2.9
15
7.6
2.9
ug/L
04/20/18 15:41
1
Ethyl Parathion
<1.6
7.6
3.8
1.6
ug/L
04/20/18 15:41
1
Famphur
<23
30
24
23
ug/L
04/20/18 15:41
1
Fluoranthene
<0.35
0.76
0.38
0.35
ug/L
04/20/18 15:41
1
Fluorene
<0.19
0.76
0.38
0.19
ug/L
04/20/18 15:41
1
Hexachlorobenzene
<0.060
0.38
0.19
0.060
ug/L
04/20/18 15:41
1
Hexachlorocyclopentadiene
<4.9
15
7.6
4.9
ug/L
04/20/18 15:41
1
Hexachloroethane
<0.46
3.8
1.9
0.46
ug/L
04/20/18 15:41
1
Hexachloropropene
<3.6
15
7.6
3.6
ug/L
04/20/18 15:41
1
Indeno[1,2,3-cd]pyrene
<0.057
0.15
0.076
0.057
ug/L
04/20/18 15:41
1
Isodrin
<5.3
15
7.6
5.3
ug/L
04/20/18 15:41
1
Isophorone
<0.29
1.5
0.76
0.29
ug/L
04/20/18 15:41
1
Isosafrole
<2.9
7.6
3.8
2.9
ug/L
04/20/18 15:41
1
Kepone
<1.3
7.6
3.8
1.3
ug/L
04/20/18 15:41
1
m-Dinitrobenzene
<1.0
3.8
1.9
1.0
ug/L
04/20/18 15:41
1
Methapyrilene
<7.7
30
15
7.7
ug/L
04/20/18 15:41
1
3-Methylcholanthrene
<1.7
7.6
3.8
1.7
ug/L
04/20/18 15:41
1
Methyl methanesulfonate
<4.5
30
15
4.5
ug/L
04/20/18 15:41
1
2-Methylnaphthalene
<0.050
1.5
0.76
0.050
ug/L
04/20/18 15:41
1
Methyl parathion
<1.8
7.6
3.8
1.8
ug/L
04/20/18 15:41
1
2-Methylphenol
<0.23
1.5
0.76
0.23
ug/L
04/20/18 15:41
1
3 & 4 Methylphenol
<0.34
1.5
0.76
0.34
ug/L
04/20/18 15:41
1
Naphthalene
<0.23
0.76
0.38
0.23
ug/L
04/20/18 15:41
1
1,4-Naphthoquinone
<30
30
30
30
ug/L
04/20/18 15:41
1
1-Naphthylamine
<4.5
15
7.6
4.5
ug/L
04/20/18 15:41
1
2-Naphthylamine
<6.9
15
7.6
6.9
ug/L
04/20/18 15:41
1
2-Nitroaniline
<0.98
3.8
1.9
0.98
ug/L
04/20/18 15:41
1
3-Nitroaniline
<1.4
7.6
3.8
1.4
ug/L
04/20/18 15:41
1
4-Nitroaniline
<1.3
7.6
3.8
1.3
ug/L
04/20/18 15:41
1
Nitrobenzene
<0.34
0.76
0.38
0.34
ug/L
04/20/18 15:41
1
5-Nitro-o-toluidine
<2.4
7.6
3.8
2.4
ug/L
04/20/18 15:41
1
TestAmerica Chicago
Page 84 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-8(i)
Lab Sample ID: 500-143858-13
Date Collected: 04/10/18 15:15
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<1.9
7.6
3.8
1.9
ug/L
04/20/18 15:41
1
4-Nitrophenol
<5.7
15
7.6
5.7
ug/L
04/20/18 15:41
1
N-Nitrosodiethylamine
<6.5
15
7.6
6.5
ug/L
04/20/18 15:41
1
N-Nitrosodimethylamine
<3.6
7.6
3.8
3.6
ug/L
04/20/18 15:41
1
N-Nitrosodi-n-butylamine
<3.2
7.6
3.8
3.2
ug/L
04/20/18 15:41
1
N-Nitrosodi-n-propylamine
<0.12
0.38
0.19
0.12
ug/L
04/20/18 15:41
1
N-Nitrosodiphenylamine
<0.28
1.5
0.76
0.28
ug/L
04/20/18 15:41
1
N-Nitrosomethylethylamine
<5.7
15
7.6
5.7
ug/L
04/20/18 15:41
1
N-Nitrosopiperidine
<2.7
7.6
3.8
2.7
ug/L
04/20/18 15:41
1
N-Nitrosopyrrolidine
<2.6
7.6
3.8
2.6
ug/L
04/20/18 15:41
1
o,o',o"-Triethylphosphorothioate
<4.2
15
7.6
4.2
ug/L
04/20/18 15:41
1
o-Toluidine
<6.0
30
15
6.0
ug/L
04/20/18 15:41
1
2,2'-oxybis[l-chloropropane]
<0.29
1.5
0.76
0.29
ug/L
04/20/18 15:41
1
p-Dimethylamino azobenzene
<2.3
7.6
3.8
2.3
ug/L
04/20/18 15:41
1
Pentachlorobenzene
<2.1
7.6
3.8
2.1
ug/L
04/20/18 15:41
1
Pentachloronitrobenzene
<2.7
7.6
3.8
2.7
ug/L
04/20/18 15:41
1
Phenacetin
<1.7
7.6
3.8
1.7
ug/L
04/20/18 15:41
1
Phenanthrene
<0.23
0.76
0.38
0.23
ug/L
04/20/18 15:41
1
Phenol
<0.51
3.8
1.9
0.51
ug/L
04/20/18 15:41
1
Phorate
<1.6
7.6
3.8
1.6
ug/L
04/20/18 15:41
1
p-Phenylene diamine
<12
61
30
12
ug/L
04/20/18 15:41
1
Pronamide
<1.6
7.6
7.6
1.6
ug/L
04/20/18 15:41
1
Pyrene
<0.32
0.76
0.38
0.32
ug/L
04/20/18 15:41
1
Safrole
<3.0
7.6
3.8
3.0
ug/L
04/20/18 15:41
1
sym-Trinitrobenzene
<1.4
7.6
3.8
1.4
ug/L
04/20/18 15:41
1
2,3,7,8-TCDD (Screen)
<7.6
7.6
7.6
7.6
ug/L
04/20/18 15:41
1
1,2,4,5-Tetrachlorobenzene
<0.43
3.8
1.9
0.43
ug/L
04/20/18 15:41
1
2,3,4,6-Tetrachlorophenol
<0.57
3.8
1.9
0.57
ug/L
04/20/18 15:41
1
Thionazin
<2.0
7.6
3.8
2.0
ug/L
04/20/18 15:41
1
2,4,5-Trichlorophenol
<2.0
7.6
3.8
2.0
ug/L
04/20/18 15:41
1
2,4,6-Trichlorophenol
<0.55
3.8
1.9
0.55
ug/L
04/20/18 15:41
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
75
34 - 110
04116118 16:56
04120118 15:41
1
2-Fluorophenol
52
27- 110
04116118 16:56
04120118 15:41
1
Nitrobenzene-d5
71
36 - 120
04116118 16:56
04120118 15:41
1
Phenol-d5
35
20- 100
04116118 16:56
04120118 15:41
1
Terphenyl-d14
140
40- 145
04116118 16:56
04120118 15:41
1
2,4,6-Tribromophenol
95
40- 145
04116118 16:56
04120118 15:41
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
alpha-BHC
<0.0025
0.038
0.019
0.0025
ug/L
04/20/18 16:21
1
beta-BHC
<0.0097
0.038
0.019
0.0097
ug/L
04/20/18 16:21
1
delta-BHC
<0.0098
0.038
0.019
0.0098
ug/L
04/20/18 16:21
1
gamma-BHC (Lindane)
<0.0053
0.038
0.019
0.0053
ug/L
04/20/18 16:21
1
Heptachlor
<0.013
0.038
0.019
0.013
ug/L
04/20/18 16:21
1
Aldrin
<0.0050
0.038
0.019
0.0050
ug/L
04/20/18 16:21
1
Heptachlor epoxide
<0.013
0.038
0.019
0.013
ug/L
04/20/18 16:21
1
Endosulfan 1
<0.0039
0.038
0.019
0.0039
ug/L
04/20/18 16:21
1
TestAmerica Chicago
Page 85 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-8(i)
Lab Sample ID: 500-143858-13
Date Collected: 04/10/18 15:15
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.012
0.038
0.019
0.012
ug/L
04/20/18 16:21
1
4,4'-DDE
<0.0036
0.038
0.019
0.0036
ug/L
04/20/18 16:21
1
Endrin
<0.013
0.038
0.019
0.013
ug/L
04/20/18 16:21
1
Endosulfan II
<0.0027
0.038
0.019
0.0027
ug/L
04/20/18 16:21
1
4,4'-DDD
<0.013
0.038
0.019
0.013
ug/L
04/20/18 16:21
1
Endosulfan sulfate
<0.011
0.038
0.019
0.011
ug/L
04/20/18 16:21
1
4,4'-DDT
<0.0030
0.038
0.019
0.0030
ug/L
04/20/18 16:21
1
Methoxychlor
<0.022
0.076
0.038
0.022
ug/L
04/20/18 16:21
1
Toxaphene
<0.19
0.38
0.19
0.19
ug/L
04/20/18 16:21
1
Endrin aldehyde
<0.0078
0.038
0.019
0.0078
ug/L
04/20/18 16:21
1
Chlordane (technical)
<0.038
0.076
0.038
0.038
ug/L
04/20/18 16:21
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
48
30 - 130
04117118 07:38
04120118 16:21
1
Tetrachloro-m-xylene
61
30 - 120
04117118 07:38
04120118 16:21
1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.064
0.38
0.19
0.064
ug/L
04/17/18 20:54
1
PCB-1221
<0.19
0.38
0.19
0.19
ug/L
04/17/18 20:54
1
PCB-1232
<0.19
0.38
0.19
0.19
ug/L
04/17/18 20:54
1
PCB-1242
<0.19
0.38
0.19
0.19
ug/L
04/17/18 20:54
1
PCB-1248
<0.19
0.38
0.19
0.19
ug/L
04/17/18 20:54
1
PCB-1254
<0.19
0.38
0.19
0.19
ug/L
04/17/18 20:54
1
PCB-1260
<0.066
0.38
0.19
0.066
ug/L
04/17/18 20:54
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
61
30 - 120
04117118 07:38
04117118 20:54
1
DCB Decachlorobiphenyl
84
30 - 140
04117118 07:38
04117118 20:54
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.44
0.95
0.48
0.44
ug/L
04/18/18 03:48
1
Dinoseb
<0.16
1.9
0.95
0.16
ug/L
04/18/18 03:48
1
Pentachlorophenol
<0.085
0.48
0.095
0.085
ug/L
04/18/18 03:48
1
Silvex (2,4,5-TP)
<0.27
0.95
0.48
0.27
ug/L
04/18/18 03:48
1
2,4,5-T
<0.41
0.95
0.48
0.41
ug/L
04/18/18 03:48
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
89
25 - 130
04117118 09:02
04118118 03:48
1
Method: 6020B - Metals (ICP/MS)
- Total Recoverable
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 03:24
1
Arsenic
0.46 J
1.0
0.50
0.23
ug/L
04/21/18 03:24
1
Barium
44
2.5
1.3
0.73
ug/L
04/21/18 03:24
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 03:24
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 03:24
1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 03:24
1
Cobalt
2.5
1.0
0.50
0.40
ug/L
04/21/18 03:24
1
Copper
1.1 J B
2.0
1.0
0.50
ug/L
04/21/18 03:24
1
TestAmerica Chicago
Page 86 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill
- Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-8(i)
Lab Sample
ID: 500-143858-13
Date Collected: 04/10/18 15:15
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Iron
1500
100
50
47
ug/L
04/21/18 03:24
1
Lead
<0.19
0.50
0.25
0.19
ug/L
04/21/18 03:24
1
Manganese
390
2.5
1.3
0.79
ug/L
04/21/18 03:24
1
Nickel
1.6 J
2.0
1.0
0.63
ug/L
04/21/18 03:24
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 03:24
1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 03:24
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 03:24
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 03:24
1
Vanadium
6.2
5.0
2.5
2.2
ug/L
04/21/18 03:24
1
Zinc
<6.9
10
20
6.9
ug/L
04/21/18 03:24
1
Method: 7470A - Mercury (CVAA)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/18/1811:07
1
General Chemistry
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/24/18 15:58
1
Chloride
83000
4000
3400
3400
ug/L
04/27/18 20:43
20
Sulfate
7300
200
100
95
ug/L
04/26/18 20:28
1
Alkalinity
230000
5000
5000
3700
ug/L
04/23/1816:38
1
Total Dissolved Solids
410000
10000
10000
4300
ug/L
04/17/18 08:19
1
TestAmerica Chicago
Page 87 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-2(i) Lab Sample ID: 500-143858-14
Date Collected: 04/12/18 10:10 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/24/18 14:25
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/24/18 14:25
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/24/18 14:25
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/24/18 14:25
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 14:25
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 14:25
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/24/18 14:25
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 14:25
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/24/18 14:25
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/24/18 14:25
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 14:25
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/24/18 14:25
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 14:25
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 14:25
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/24/18 14:25
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/24/18 14:25
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 14:25
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/24/18 14:25
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/24/18 14:25
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/24/18 14:25
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/24/18 14:25
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/24/18 14:25
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/24/18 14:25
1
Acetone
7.6 cn
5.0
2.5
1.7
ug/L
04/24/18 14:25
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/24/18 14:25
1
Acrolein
<23
100
50
23
ug/L
04/24/18 14:25
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/24/18 14:25
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/24/18 14:25
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 14:25
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/24/18 14:25
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/24/18 14:25
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/24/18 14:25
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/24/18 14:25
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/24/18 14:25
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 14:25
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/24/18 14:25
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/24/18 14:25
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/24/18 14:25
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/24/18 14:25
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/24/18 14:25
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/24/18 14:25
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/24/18 14:25
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/24/18 14:25
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/24/18 14:25
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/24/18 14:25
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/24/18 14:25
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/24/18 14:25
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/24/18 14:25
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/24/18 14:25
1
TestAmerica Chicago
Page 88 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-2(i)
Lab Sample
ID: 500-143858-14
Date Collected: 04/12/18 10:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/24/18 14:25
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/24/18 14:25
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/24/18 14:25
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 14:25
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/24/18 14:25
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/24/18 14:25
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/24/18 14:25
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/24/18 14:25
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 14:25
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/24/18 14:25
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/24/18 14:25
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 14:25
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/24/18 14:25
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/24/18 14:25
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/24/18 14:25
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 101 75- 126
4-Bromofluorobenzene (Surr) 104 72 - 124
Dibromofluoromethane 90 75 - 120
Toluene-d8 (Surr) 92 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04124118 14:25
04124118 14:25
04124118 14:25
04124118 14:25
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.24
0.78
0.39
0.24
ug/L
04/20/18 16:06
1
Acenaphthylene
<0.21
0.78
0.39
0.21
ug/L
04/20/18 16:06
1
Acetophenone
<0.52
3.9
2.0
0.52
ug/L
04/20/18 16:06
1
2-Acetylaminofluorene
<1.7
7.8
3.9
1.7
ug/L
04/20/18 16:06
1
4-Aminobiphenyl
<2.9
7.8
3.9
2.9
ug/L
04/20/18 16:06
1
Anthracene
<0.26
0.78
0.39
0.26
ug/L
04/20/18 16:06
1
Benzo[a]anthracene
<0.044
0.16
0.078
0.044
ug/L
04/20/18 16:06
1
Benzo[a]pyrene
<0.077
0.16
0.078
0.077
ug/L
04/20/18 16:06
1
Benzo[b]fluoranthene
<0.063
0.16
0.078
0.063
ug/L
04/20/18 16:06
1
Benzo[g,h,i]perylene
<0.29
0.78
0.39
0.29
ug/L
04/20/18 16:06
1
Benzo[k]fluoranthene
<0.050
0.16
0.078
0.050
ug/L
04/20/18 16:06
1
Benzyl alcohol
<4.7
16
7.8
4.7
ug/L
04/20/18 16:06
1
Bis(2-chloroethoxy)methane
<0.22
1.6
0.78
0.22
ug/L
04/20/18 16:06
1
Bis(2-chloroethyl)ether
<0.23
1.6
0.78
0.23
ug/L
04/20/18 16:06
1
Bis(2-ethylhexyl) phthalate
<1.3
7.8
3.9
1.3
ug/L
04/20/18 16:06
1
4-Bromophenyl phenyl ether
<0.42
3.9
2.0
0.42
ug/L
04/20/18 16:06
1
Butyl benzyl phthalate
<0.37
1.6
0.78
0.37
ug/L
04/20/18 16:06
1
4-Chloroaniline
<1.6
7.8
3.9
1.6
ug/L
04/20/18 16:06
1
Chlorobenzilate
<2.7
7.8
3.9
2.7
ug/L
04/20/18 16:06
1
4-Chloro-3-methylphenol
<1.8
7.8
3.9
1.8
ug/L
04/20/18 16:06
1
2-Chloronaphthalene
<0.18
1.6
0.78
0.18
ug/L
04/20/18 16:06
1
2-Chlorophenol
<0.44
3.9
2.0
0.44
ug/L
04/20/18 16:06
1
4-Chlorophenyl phenyl ether
<0.50
3.9
2.0
0.50
ug/L
04/20/18 16:06
1
Chrysene
<0.053
0.16
0.078
0.053
ug/L
04/20/18 16:06
1
Diallate
<4.3
7.8
4.9
4.3
ug/L
04/20/18 16:06
1
Dibenz(a,h)anthracene
<0.040
0.23
0.12
0.040
ug/L
04/20/18 16:06
1
TestAmerica Chicago
Page 89 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-2(i) Lab Sample ID: 500-143858-14
Date Collected: 04/12/18 10:10 Matrix: Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.20
1.6
0.78
0.20
ug/L
04/20/18 16:06
1
3,3'-Dichlorobenzidine
<1.3
3.9
2.0
1.3
ug/L
04/20/18 16:06
1
2,4-Dichlorophenol
<2.0
7.8
3.9
2.0
ug/L
04/20/18 16:06
1
2,6-Dichlorophenol
<2.7
7.8
3.9
2.7
ug/L
04/20/18 16:06
1
Diethyl phthalate
<0.28
3.9
1.6
0.28
ug/L
04/20/18 16:06
1
Dimethoate
<1.5
7.8
3.9
1.5
ug/L
04/20/18 16:06
1
7,12-Dimethylbenz(a)anthracene
<2.4
31
16
2.4
ug/L
04/20/18 16:06
1
3,3'-Dimethylbenzidine
<14
31
16
14
ug/L
04/20/18 16:06
1
2,4-Dimethylphenol
<1.4
7.8
3.9
1.4
ug/L
04/20/18 16:06
1
Dimethyl phthalate
<0.24
3.9
1.6
0.24
ug/L
04/20/18 16:06
1
Di-n-butyl phthalate
<0.57
3.9
2.0
0.57
ug/L
04/20/18 16:06
1
4,6-Dinitro-2-methylphenol
<4.6
16
7.8
4.6
ug/L
04/20/18 16:06
1
2,4-Dinitrophenol
<6.7
16
7.8
6.7
ug/L
04/20/18 16:06
1
2,4-Dinitrotoluene
<0.19
0.78
0.39
0.19
ug/L
04/20/18 16:06
1
2,6-Dinitrotoluene
<0.058
0.78
0.39
0.058
ug/L
04/20/18 16:06
1
Di-n-octyl phthalate
<0.82
7.8
3.9
0.82
ug/L
04/20/18 16:06
1
Diphenylamine
<2.0
7.8
3.9
2.0
ug/L
04/20/18 16:06
1
Disulfoton
<1.5
7.8
3.9
1.5
ug/L
04/20/18 16:06
1
Ethyl methanesulfonate
<3.0
16
7.8
3.0
ug/L
04/20/18 16:06
1
Ethyl Parathion
<1.6
7.8
3.9
1.6
ug/L
04/20/18 16:06
1
Famphur
<24
31
24
24
ug/L
04/20/18 16:06
1
Fluoranthene
<0.35
0.78
0.39
0.35
ug/L
04/20/18 16:06
1
Fluorene
<0.19
0.78
0.39
0.19
ug/L
04/20/18 16:06
1
Hexachlorobenzene
<0.062
0.39
0.20
0.062
ug/L
04/20/18 16:06
1
Hexachlorocyclopentadiene
<5.0
16
7.8
5.0
ug/L
04/20/18 16:06
1
Hexachloroethane
<0.47
3.9
2.0
0.47
ug/L
04/20/18 16:06
1
Hexachloropropene
<3.7
16
7.8
3.7
ug/L
04/20/18 16:06
1
Indeno[1,2,3-cd]pyrene
<0.058
0.16
0.078
0.058
ug/L
04/20/18 16:06
1
Isodrin
<5.4
16
7.8
5.4
ug/L
04/20/18 16:06
1
Isophorone
<0.29
1.6
0.78
0.29
ug/L
04/20/18 16:06
1
Isosafrole
<3.0
7.8
3.9
3.0
ug/L
04/20/18 16:06
1
Kepone
<1.3
7.8
3.9
1.3
ug/L
04/20/18 16:06
1
m-Dinitrobenzene
<1.0
3.9
2.0
1.0
ug/L
04/20/18 16:06
1
Methapyrilene
<7.9
31
16
7.9
ug/L
04/20/18 16:06
1
3-Methylcholanthrene
<1.8
7.8
3.9
1.8
ug/L
04/20/18 16:06
1
Methyl methanesulfonate
<4.6
31
16
4.6
ug/L
04/20/18 16:06
1
2-Methylnaphthalene
<0.051
1.6
0.78
0.051
ug/L
04/20/18 16:06
1
Methyl parathion
<1.8
7.8
3.9
1.8
ug/L
04/20/18 16:06
1
2-Methylphenol
<0.24
1.6
0.78
0.24
ug/L
04/20/18 16:06
1
3 & 4 Methylphenol
<0.35
1.6
0.78
0.35
ug/L
04/20/18 16:06
1
Naphthalene
<0.24
0.78
0.39
0.24
ug/L
04/20/18 16:06
1
1,4-Naphthoquinone
<30
31
31
30
ug/L
04/20/18 16:06
1
1-Naphthylamine
<4.6
16
7.8
4.6
ug/L
04/20/18 16:06
1
2-Naphthylamine
<7.1
16
7.8
7.1
ug/L
04/20/18 16:06
1
2-Nitroaniline
<1.0
3.9
2.0
1.0
ug/L
04/20/18 16:06
1
3-Nitroaniline
<1.4
7.8
3.9
1.4
ug/L
04/20/18 16:06
1
4-Nitroaniline
<1.3
7.8
3.9
1.3
ug/L
04/20/18 16:06
1
Nitrobenzene
<0.35
0.78
0.39
0.35
ug/L
04/20/18 16:06
1
5-Nitro-o-toluidine
<2.4
7.8
3.9
2.4
ug/L
04/20/18 16:06
1
TestAmerica Chicago
Page 90 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-2(i)
Lab Sample ID: 500-143858-14
Date Collected: 04/12/18 10:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<2.0
7.8
3.9
2.0
ug/L
04/20/18 16:06
1
4-Nitrophenol
<5.8
16
7.8
5.8
ug/L
04/20/18 16:06
1
N-Nitrosodiethylamine
<6.7
16
7.8
6.7
ug/L
04/20/18 16:06
1
N-Nitrosodimethylamine
<3.7
7.8
3.9
3.7
ug/L
04/20/18 16:06
1
N-Nitrosodi-n-butylamine
<3.3
7.8
3.9
3.3
ug/L
04/20/18 16:06
1
N-Nitrosodi-n-propylamine
<0.12
0.39
0.20
0.12
ug/L
04/20/18 16:06
1
N-Nitrosodiphenylamine
<0.29
1.6
0.78
0.29
ug/L
04/20/18 16:06
1
N-Nitrosomethylethylamine
<5.8
16
7.8
5.8
ug/L
04/20/18 16:06
1
N-Nitrosopiperidine
<2.7
7.8
3.9
2.7
ug/L
04/20/18 16:06
1
N-Nitrosopyrrolidine
<2.6
7.8
3.9
2.6
ug/L
04/20/18 16:06
1
o,o',o"-Triethylphosphorothioate
<4.3
16
7.8
4.3
ug/L
04/20/18 16:06
1
o-Toluidine
<6.2
31
16
6.2
ug/L
04/20/18 16:06
1
2,2'-oxybis[l-chloropropane]
<0.30
1.6
0.78
0.30
ug/L
04/20/18 16:06
1
p-Dimethylamino azobenzene
<2.3
7.8
3.9
2.3
ug/L
04/20/18 16:06
1
Pentachlorobenzene
<2.2
7.8
3.9
2.2
ug/L
04/20/18 16:06
1
Pentachloronitrobenzene
<2.8
7.8
3.9
2.8
ug/L
04/20/18 16:06
1
Phenacetin
<1.8
7.8
3.9
1.8
ug/L
04/20/18 16:06
1
Phenanthrene
<0.24
0.78
0.39
0.24
ug/L
04/20/18 16:06
1
Phenol
<0.52
3.9
2.0
0.52
ug/L
04/20/18 16:06
1
Phorate
<1.7
7.8
3.9
1.7
ug/L
04/20/18 16:06
1
p-Phenylene diamine
<13
62
31
13
ug/L
04/20/18 16:06
1
Pronamide
<1.7
7.8
7.8
1.7
ug/L
04/20/18 16:06
1
Pyrene
<0.33
0.78
0.39
0.33
ug/L
04/20/18 16:06
1
Safrole
<3.1
7.8
3.9
3.1
ug/L
04/20/18 16:06
1
sym-Trinitrobenzene
<1.5
7.8
3.9
1.5
ug/L
04/20/18 16:06
1
2,3,7,8-TCDD (Screen)
<7.8
7.8
7.8
7.8
ug/L
04/20/18 16:06
1
1,2,4,5-Tetrachlorobenzene
<0.45
3.9
2.0
0.45
ug/L
04/20/18 16:06
1
2,3,4,6-Tetrachlorophenol
<0.58
3.9
2.0
0.58
ug/L
04/20/18 16:06
1
Thionazin
<2.0
7.8
3.9
2.0
ug/L
04/20/18 16:06
1
2,4,5-Trichlorophenol
<2.0
7.8
3.9
2.0
ug/L
04/20/18 16:06
1
2,4,6-Trichlorophenol
<0.56
3.9
2.0
0.56
ug/L
04/20/18 16:06
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
96
34 - 110
04116118 16:56
04120118 16:06
1
2-Fluorophenol
57
27- 110
04116118 16:56
04120118 16:06
1
Nitrobenzene-d5
91
36 - 120
04116118 16:56
04120118 16:06
1
Phenol-d5
43
20- 100
04116118 16:56
04120118 16:06
1
Terphenyl-d14
142
40- 145
04116118 16:56
04120118 16:06
1
2,4,6-Tribromophenol
103
40- 145
04116118 16:56
04120118 16:06
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
alpha-BHC
<0.0025
beta-BHC
<0.010
delta-BHC
<0.010
gamma-BHC (Lindane)
<0.0055
Heptachlor
<0.013
Aldrin
<0.0052
Heptachlor epoxide
<0.014
Endosulfan 1
<0.0040
RL
LOD
MDL
Unit
D Analyzed
0.039
0.020
0.0025
ug/L
04/20/1816:40
0.039
0.020
0.010
ug/L
04/20/1816:40
0.039
0.020
0.010
ug/L
04/20/1816:40
0.039
0.020
0.0055
ug/L
04/20/1816:40
0.039
0.020
0.013
ug/L
04/20/1816:40
0.039
0.020
0.0052
ug/L
04/20/1816:40
0.039
0.020
0.014
ug/L
04/20/1816:40
0.039
0.020
0.0040
ug/L
04/20/1816:40
Dil Fac
1
1
1
1
1
1
1
1
Page 91 of 258
TestAmerica Chicago
7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-2(i)
Lab Sample ID: 500-143858-14
Date Collected: 04/12/18 10:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.013
0.039
0.020
0.013
ug/L
04/20/18 16:40
1
4,4'-DDE
<0.0037
0.039
0.020
0.0037
ug/L
04/20/18 16:40
1
Endrin
<0.014
0.039
0.020
0.014
ug/L
04/20/18 16:40
1
Endosulfan II
<0.0027
0.039
0.020
0.0027
ug/L
04/20/18 16:40
1
4,4'-DDD
<0.013
0.039
0.020
0.013
ug/L
04/20/18 16:40
1
Endosulfan sulfate
<0.011
0.039
0.020
0.011
ug/L
04/20/18 16:40
1
4,4'-DDT
<0.0031
0.039
0.020
0.0031
ug/L
04/20/18 16:40
1
Methoxychlor
<0.023
0.078
0.039
0.023
ug/L
04/20/18 16:40
1
Toxaphene
<0.20
0.39
0.20
0.20
ug/L
04/20/18 16:40
1
Endrin aldehyde
<0.0080
0.039
0.020
0.0080
ug/L
04/20/18 16:40
1
Chlordane (technical)
<0.039
0.078
0.039
0.039
ug/L
04/20/18 16:40
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
70
30 - 130
04117118 07:38
04120118 16:40
1
Tetrachloro-m-xylene
65
30 - 120
04117118 07:38
04120118 16:40
1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.066
0.39
0.20
0.066
ug/L
04/17/18 21:11
1
PCB-1221
<0.20
0.39
0.20
0.20
ug/L
04/17/18 21:11
1
PCB-1232
<0.20
0.39
0.20
0.20
ug/L
04/17/18 21:11
1
PCB-1242
<0.20
0.39
0.20
0.20
ug/L
04/17/18 21:11
1
PCB-1248
<0.20
0.39
0.20
0.20
ug/L
04/17/18 21:11
1
PCB-1254
<0.20
0.39
0.20
0.20
ug/L
04/17/18 21:11
1
PCB-1260
<0.069
0.39
0.20
0.069
ug/L
04/17/18 21:11
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
71
30 - 120
04117118 07:38
04117118 21:11
1
DCB Decachlorobiphenyl
86
30 - 140
04117118 07:38
04117118 21:11
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.46
0.98
0.49
0.46
ug/L
04/18/18 04:13
1
Dinoseb
<0.16
2.0
0.98
0.16
ug/L
04/18/18 04:13
1
Pentachlorophenol
<0.088
0.49
0.098
0.088
ug/L
04/18/18 04:13
1
Silvex (2,4,5-TP)
<0.28
0.98
0.49
0.28
ug/L
04/18/18 04:13
1
2,4,5-T
<0.43
0.98
0.49
0.43
ug/L
04/18/18 04:13
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
82
25 - 130
04117118 09:02
04118118 04:13
1
Method: 6020B - Metals (ICP/MS)
- Total Recoverable
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 03:43
1
Arsenic
0.37 J
1.0
0.50
0.23
ug/L
04/21/18 03:43
1
Barium
44
2.5
1.3
0.73
ug/L
04/21/18 03:43
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 03:43
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 03:43
1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 03:43
1
Cobalt
<0.40
1.0
0.50
0.40
ug/L
04/21/18 03:43
1
Copper
2.3 B
2.0
1.0
0.50
ug/L
04/21/18 03:43
1
TestAmerica Chicago
Page 92 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill
- Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-2(i)
Lab Sample
ID: 500-143858-14
Date Collected: 04/12/18 10:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Iron
<47
100
50
47
ug/L
04/21/18 03:43
1
Lead
<0.19
0.50
0.25
0.19
ug/L
04/21/18 03:43
1
Manganese
140
2.5
1.3
0.79
ug/L
04/21/18 03:43
1
Nickel
0.72 J
2.0
1.0
0.63
ug/L
04/21/18 03:43
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 03:43
1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 03:43
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 03:43
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 03:43
1
Vanadium
<2.2
5.0
2.5
2.2
ug/L
04/21/18 03:43
1
Zinc
<6.9
10
20
6.9
ug/L
04/21/18 03:43
1
Method: 7470A - Mercury (CVAA)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/18/1811:09
1
General Chemistry
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/25/18 09:55
1
Chloride
6100
1000
850
850
ug/L
04/27/18 20:55
5
Sulfate
240000
5000
2500
2400
ug/L
04/26/18 20:41
25
Alkalinity
81000
5000
5000
3700
ug/L
04/24/1814:29
1
Total Dissolved Solids
470000
10000
10000
4300
ug/L
04/17/18 08:21
1
TestAmerica Chicago
Page 93 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-3(i) Lab Sample ID: 500-143858-15
Date Collected: 04/12/18 11:00 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/24/18 14:52
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/24/18 14:52
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/24/18 14:52
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/24/18 14:52
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 14:52
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 14:52
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/24/18 14:52
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 14:52
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/24/18 14:52
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/24/18 14:52
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 14:52
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/24/18 14:52
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 14:52
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 14:52
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/24/18 14:52
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/24/18 14:52
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 14:52
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/24/18 14:52
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/24/18 14:52
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/24/18 14:52
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/24/18 14:52
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/24/18 14:52
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/24/18 14:52
1
Acetone
6.0 cn
5.0
2.5
1.7
ug/L
04/24/18 14:52
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/24/18 14:52
1
Acrolein
<23
100
50
23
ug/L
04/24/18 14:52
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/24/18 14:52
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/24/18 14:52
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 14:52
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/24/18 14:52
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/24/18 14:52
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/24/18 14:52
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/24/18 14:52
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/24/18 14:52
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 14:52
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/24/18 14:52
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/24/18 14:52
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/24/18 14:52
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/24/18 14:52
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/24/18 14:52
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/24/18 14:52
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/24/18 14:52
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/24/18 14:52
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/24/18 14:52
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/24/18 14:52
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/24/18 14:52
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/24/18 14:52
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/24/18 14:52
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/24/18 14:52
1
TestAmerica Chicago
Page 94 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-3(i)
Lab Sample
ID: 500-143858-15
Date Collected: 04/12/18 11:00
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/24/18 14:52
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/24/18 14:52
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/24/18 14:52
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 14:52
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/24/18 14:52
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/24/18 14:52
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/24/18 14:52
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/24/18 14:52
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 14:52
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/24/18 14:52
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/24/18 14:52
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 14:52
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/24/18 14:52
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/24/18 14:52
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/24/18 14:52
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 101 75- 126
4-Bromofluorobenzene (Surr) 106 72 - 124
Dibromofluoromethane 91 75 - 120
Toluene-d8 (Surr) 91 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04124118 14:52
04124118 14:52
04124118 14:52
04124118 14:52
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.24
0.79
0.39
0.24
ug/L
04/20/18 16:32
1
Acenaphthylene
<0.21
0.79
0.39
0.21
ug/L
04/20/18 16:32
1
Acetophenone
<0.52
3.9
2.0
0.52
ug/L
04/20/18 16:32
1
2-Acetylaminofluorene
<1.7
7.9
3.9
1.7
ug/L
04/20/18 16:32
1
4-Aminobiphenyl
<3.0
7.9
3.9
3.0
ug/L
04/20/18 16:32
1
Anthracene
<0.26
0.79
0.39
0.26
ug/L
04/20/18 16:32
1
Benzo[a]anthracene
<0.045
0.16
0.079
0.045
ug/L
04/20/18 16:32
1
Benzo[a]pyrene
<0.078
0.16
0.079
0.078
ug/L
04/20/18 16:32
1
Benzo[b]fluoranthene
<0.064
0.16
0.079
0.064
ug/L
04/20/18 16:32
1
Benzo[g,h,i]perylene
<0.30
0.79
0.39
0.30
ug/L
04/20/18 16:32
1
Benzo[k]fluoranthene
<0.050
0.16
0.079
0.050
ug/L
04/20/18 16:32
1
Benzyl alcohol
<4.8
16
7.9
4.8
ug/L
04/20/18 16:32
1
Bis(2-chloroethoxy)methane
<0.22
1.6
0.79
0.22
ug/L
04/20/18 16:32
1
Bis(2-chloroethyl)ether
<0.23
1.6
0.79
0.23
ug/L
04/20/18 16:32
1
Bis(2-ethylhexyl) phthalate
<1.4
7.9
3.9
1.4
ug/L
04/20/18 16:32
1
4-Bromophenyl phenyl ether
<0.43
3.9
2.0
0.43
ug/L
04/20/18 16:32
1
Butyl benzyl phthalate
<0.38
1.6
0.79
0.38
ug/L
04/20/18 16:32
1
4-Chloroaniline
<1.6
7.9
3.9
1.6
ug/L
04/20/18 16:32
1
Chlorobenzilate
<2.7
7.9
3.9
2.7
ug/L
04/20/18 16:32
1
4-Chloro-3-methylphenol
<1.8
7.9
3.9
1.8
ug/L
04/20/18 16:32
1
2-Chloronaphthalene
<0.19
1.6
0.79
0.19
ug/L
04/20/18 16:32
1
2-Chlorophenol
<0.44
3.9
2.0
0.44
ug/L
04/20/18 16:32
1
4-Chlorophenyl phenyl ether
<0.50
3.9
2.0
0.50
ug/L
04/20/18 16:32
1
Chrysene
<0.054
0.16
0.079
0.054
ug/L
04/20/18 16:32
1
Diallate
<4.3
7.9
4.9
4.3
ug/L
04/20/18 16:32
1
Dibenz(a,h)anthracene
<0.040
0.24
0.12
0.040
ug/L
04/20/18 16:32
1
TestAmerica Chicago
Page 95 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-3(i) Lab Sample ID: 500-143858-15
Date Collected: 04/12/18 11:00 Matrix: Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.21
1.6
0.79
0.21
ug/L
04/20/18 16:32
1
3,3'-Dichlorobenzidine
<1.4
3.9
2.0
1.4
ug/L
04/20/18 16:32
1
2,4-Dichlorophenol
<2.1
7.9
3.9
2.1
ug/L
04/20/18 16:32
1
2,6-Dichlorophenol
<2.8
7.9
3.9
2.8
ug/L
04/20/18 16:32
1
Diethyl phthalate
<0.28
3.9
1.6
0.28
ug/L
04/20/18 16:32
1
Dimethoate
<1.5
7.9
3.9
1.5
ug/L
04/20/18 16:32
1
7,12-Dimethylbenz(a)anthracene
<2.4
32
16
2.4
ug/L
04/20/18 16:32
1
3,3'-Dimethylbenzidine
<14
32
16
14
ug/L
04/20/18 16:32
1
2,4-Dimethylphenol
<1.4
7.9
3.9
1.4
ug/L
04/20/18 16:32
1
Dimethyl phthalate
<0.25
3.9
1.6
0.25
ug/L
04/20/18 16:32
1
Di-n-butyl phthalate
1.1 J
3.9
2.0
0.58
ug/L
04/20/18 16:32
1
4,6-Dinitro-2-methylphenol
<4.7
16
7.9
4.7
ug/L
04/20/18 16:32
1
2,4-Dinitrophenol
<6.8
16
7.9
6.8
ug/L
04/20/18 16:32
1
2,4-Dinitrotoluene
<0.19
0.79
0.39
0.19
ug/L
04/20/18 16:32
1
2,6-Dinitrotoluene
<0.058
0.79
0.39
0.058
ug/L
04/20/18 16:32
1
Di-n-octyl phthalate
<0.83
7.9
3.9
0.83
ug/L
04/20/18 16:32
1
Diphenylamine
<2.0
7.9
3.9
2.0
ug/L
04/20/18 16:32
1
Disulfoton
<1.5
7.9
3.9
1.5
ug/L
04/20/18 16:32
1
Ethyl methanesulfonate
<3.0
16
7.9
3.0
ug/L
04/20/18 16:32
1
Ethyl Parathion
<1.6
7.9
3.9
1.6
ug/L
04/20/18 16:32
1
Famphur
<24
32
25
24
ug/L
04/20/18 16:32
1
Fluoranthene
<0.36
0.79
0.39
0.36
ug/L
04/20/18 16:32
1
Fluorene
<0.19
0.79
0.39
0.19
ug/L
04/20/18 16:32
1
Hexachlorobenzene
<0.063
0.39
0.20
0.063
ug/L
04/20/18 16:32
1
Hexachlorocyclopentadiene
<5.0
16
7.9
5.0
ug/L
04/20/18 16:32
1
Hexachloroethane
<0.47
3.9
2.0
0.47
ug/L
04/20/18 16:32
1
Hexachloropropene
<3.7
16
7.9
3.7
ug/L
04/20/18 16:32
1
Indeno[1,2,3-cd]pyrene
<0.059
0.16
0.079
0.059
ug/L
04/20/18 16:32
1
Isodrin
<5.4
16
7.9
5.4
ug/L
04/20/18 16:32
1
Isophorone
<0.30
1.6
0.79
0.30
ug/L
04/20/18 16:32
1
Isosafrole
<3.1
7.9
3.9
3.1
ug/L
04/20/18 16:32
1
Kepone
<1.3
7.9
3.9
1.3
ug/L
04/20/18 16:32
1
m-Dinitrobenzene
<1.0
3.9
2.0
1.0
ug/L
04/20/18 16:32
1
Methapyrilene
<8.0
32
16
8.0
ug/L
04/20/18 16:32
1
3-Methylcholanthrene
<1.8
7.9
3.9
1.8
ug/L
04/20/18 16:32
1
Methyl methanesulfonate
<4.7
32
16
4.7
ug/L
04/20/18 16:32
1
2-Methylnaphthalene
<0.051
1.6
0.79
0.051
ug/L
04/20/18 16:32
1
Methyl parathion
<1.8
7.9
3.9
1.8
ug/L
04/20/18 16:32
1
2-Methylphenol
<0.24
1.6
0.79
0.24
ug/L
04/20/18 16:32
1
3 & 4 Methylphenol
<0.35
1.6
0.79
0.35
ug/L
04/20/18 16:32
1
Naphthalene
<0.24
0.79
0.39
0.24
ug/L
04/20/18 16:32
1
1,4-Naphthoquinone
<31
32
32
31
ug/L
04/20/18 16:32
1
1-Naphthylamine
<4.7
16
7.9
4.7
ug/L
04/20/18 16:32
1
2-Naphthylamine
<7.2
16
7.9
7.2
ug/L
04/20/18 16:32
1
2-Nitroaniline
<1.0
3.9
2.0
1.0
ug/L
04/20/18 16:32
1
3-Nitroaniline
<1.4
7.9
3.9
1.4
ug/L
04/20/18 16:32
1
4-Nitroaniline
<1.3
7.9
3.9
1.3
ug/L
04/20/18 16:32
1
Nitrobenzene
<0.35
0.79
0.39
0.35
ug/L
04/20/18 16:32
1
5-Nitro-o-toluidine
<2.4
7.9
3.9
2.4
ug/L
04/20/18 16:32
1
TestAmerica Chicago
Page 96 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-3(i)
Lab Sample ID: 500-143858-15
Date Collected: 04/12/18 11:00
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<2.0
7.9
3.9
2.0
ug/L
04/20/18 16:32
1
4-Nitrophenol
<5.9
16
7.9
5.9
ug/L
04/20/18 16:32
1
N-Nitrosodiethylamine
<6.8
16
7.9
6.8
ug/L
04/20/18 16:32
1
N-Nitrosodimethylamine
<3.7
7.9
3.9
3.7
ug/L
04/20/18 16:32
1
N-Nitrosodi-n-butylamine
<3.3
7.9
3.9
3.3
ug/L
04/20/18 16:32
1
N-Nitrosodi-n-propylamine
<0.12
0.39
0.20
0.12
ug/L
04/20/18 16:32
1
N-Nitrosodiphenylamine
<0.29
1.6
0.79
0.29
ug/L
04/20/18 16:32
1
N-Nitrosomethylethylamine
<5.9
16
7.9
5.9
ug/L
04/20/18 16:32
1
N-Nitrosopiperidine
<2.8
7.9
3.9
2.8
ug/L
04/20/18 16:32
1
N-Nitrosopyrrolidine
<2.7
7.9
3.9
2.7
ug/L
04/20/18 16:32
1
o,o',o"-Triethylphosphorothioate
<4.3
16
7.9
4.3
ug/L
04/20/18 16:32
1
o-Toluidine
<6.3
32
16
6.3
ug/L
04/20/18 16:32
1
2,2'-oxybis[l-chloropropane]
<0.30
1.6
0.79
0.30
ug/L
04/20/18 16:32
1
p-Dimethylamino azobenzene
<2.4
7.9
3.9
2.4
ug/L
04/20/18 16:32
1
Pentachlorobenzene
<2.2
7.9
3.9
2.2
ug/L
04/20/18 16:32
1
Pentachloronitrobenzene
<2.8
7.9
3.9
2.8
ug/L
04/20/18 16:32
1
Phenacetin
<1.8
7.9
3.9
1.8
ug/L
04/20/18 16:32
1
Phenanthrene
<0.24
0.79
0.39
0.24
ug/L
04/20/18 16:32
1
Phenol
<0.53
3.9
2.0
0.53
ug/L
04/20/18 16:32
1
Phorate
<1.7
7.9
3.9
1.7
ug/L
04/20/18 16:32
1
p-Phenylene diamine
<13
63
32
13
ug/L
04/20/18 16:32
1
Pronamide
<1.7
7.9
7.9
1.7
ug/L
04/20/18 16:32
1
Pyrene
<0.34
0.79
0.39
0.34
ug/L
04/20/18 16:32
1
Safrole
<3.2
7.9
3.9
3.2
ug/L
04/20/18 16:32
1
sym-Trinitrobenzene
<1.5
7.9
3.9
1.5
ug/L
04/20/18 16:32
1
2,3,7,8-TCDD (Screen)
<7.9
7.9
7.9
7.9
ug/L
04/20/18 16:32
1
1,2,4,5-Tetrachlorobenzene
<0.45
3.9
2.0
0.45
ug/L
04/20/18 16:32
1
2,3,4,6-Tetrachlorophenol
<0.59
3.9
2.0
0.59
ug/L
04/20/18 16:32
1
Thionazin
<2.0
7.9
3.9
2.0
ug/L
04/20/18 16:32
1
2,4,5-Trichlorophenol
<2.0
7.9
3.9
2.0
ug/L
04/20/18 16:32
1
2,4,6-Trichlorophenol
<0.56
3.9
2.0
0.56
ug/L
04/20/18 16:32
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
75
34 - 110
04116118 16:56
04120118 16:32
1
2-Fluorophenol
53
27- 110
04116118 16:56
04120118 16:32
1
Nitrobenzene-d5
72
36 - 120
04116118 16:56
04120118 16:32
1
Phenol-d5
36
20- 100
04116118 16:56
04120118 16:32
1
Terphenyl-d14
136
40- 145
04116118 16:56
04120118 16:32
1
2,4,6-Tribromophenol
95
40- 145
04116118 16:56
04120118 16:32
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
alpha-BHC
<0.0025
0.039
0.020
0.0025
ug/L
04/20/18 16:59
1
beta-BHC
<0.010
0.039
0.020
0.010
ug/L
04/20/18 16:59
1
delta-BHC
<0.010
0.039
0.020
0.010
ug/L
04/20/18 16:59
1
gamma-BHC (Lindane)
<0.0055
0.039
0.020
0.0055
ug/L
04/20/18 16:59
1
Heptachlor
<0.013
0.039
0.020
0.013
ug/L
04/20/18 16:59
1
Aldrin
<0.0052
0.039
0.020
0.0052
ug/L
04/20/18 16:59
1
Heptachlor epoxide
<0.014
0.039
0.020
0.014
ug/L
04/20/18 16:59
1
Endosulfan 1
<0.0040
0.039
0.020
0.0040
ug/L
04/20/18 16:59
1
TestAmerica Chicago
Page 97 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-3(i)
Lab Sample ID: 500-143858-15
Date Collected: 04/12/18 11:00
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.013
0.039
0.020
0.013
ug/L
04/20/18 16:59
1
4,4'-DDE
<0.0037
0.039
0.020
0.0037
ug/L
04/20/18 16:59
1
Endrin
<0.014
0.039
0.020
0.014
ug/L
04/20/18 16:59
1
Endosulfan II
<0.0027
0.039
0.020
0.0027
ug/L
04/20/18 16:59
1
4,4'-DDD
<0.013
0.039
0.020
0.013
ug/L
04/20/18 16:59
1
Endosulfan sulfate
<0.011
0.039
0.020
0.011
ug/L
04/20/18 16:59
1
4,4'-DDT
<0.0031
0.039
0.020
0.0031
ug/L
04/20/18 16:59
1
Methoxychlor
<0.023
0.078
0.039
0.023
ug/L
04/20/18 16:59
1
Toxaphene
<0.20
0.39
0.20
0.20
ug/L
04/20/18 16:59
1
Endrin aldehyde
<0.0080
0.039
0.020
0.0080
ug/L
04/20/18 16:59
1
Chlordane (technical)
<0.039
0.078
0.039
0.039
ug/L
04/20/18 16:59
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
74
30 - 130
04117118 07:38
04120118 16:59
1
Tetrachloro-m-xylene
68
30 - 120
04117118 07:38
04120118 16:59
1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.066
0.39
0.20
0.066
ug/L
04/17/18 21:27
1
PCB-1221
<0.20
0.39
0.20
0.20
ug/L
04/17/18 21:27
1
PCB-1232
<0.20
0.39
0.20
0.20
ug/L
04/17/18 21:27
1
PCB-1242
<0.20
0.39
0.20
0.20
ug/L
04/17/18 21:27
1
PCB-1248
<0.20
0.39
0.20
0.20
ug/L
04/17/18 21:27
1
PCB-1254
<0.20
0.39
0.20
0.20
ug/L
04/17/18 21:27
1
PCB-1260
<0.069
0.39
0.20
0.069
ug/L
04/17/18 21:27
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
67
30 - 120
04117118 07:38
04117118 21:27
1
DCB Decachlorobiphenyl
85
30 - 140
04117118 07:38
04117118 21:27
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.44
0.95
0.48
0.44
ug/L
04/18/18 04:37
1
Dinoseb
<0.16
1.9
0.95
0.16
ug/L
04/18/18 04:37
1
Pentachlorophenol
<0.085
0.48
0.095
0.085
ug/L
04/18/18 04:37
1
Silvex (2,4,5-TP)
<0.27
0.95
0.48
0.27
ug/L
04/18/18 04:37
1
2,4,5-T
<0.41
0.95
0.48
0.41
ug/L
04/18/18 04:37
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
82
25 - 130
04117118 09:02
04118118 04:37
1
Method: 6020B - Metals (ICP/MS)
- Total Recoverable
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 03:46
1
Arsenic
0.26 J
1.0
0.50
0.23
ug/L
04/21/18 03:46
1
Barium
70
2.5
1.3
0.73
ug/L
04/21/18 03:46
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 03:46
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 03:46
1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 03:46
1
Cobalt
4.5
1.0
0.50
0.40
ug/L
04/21/18 03:46
1
Copper
0.74 J B
2.0
1.0
0.50
ug/L
04/21/18 03:46
1
TestAmerica Chicago
Page 98 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill
- Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-3(i)
Lab Sample
ID: 500-143858-15
Date Collected: 04/12/18 11:00
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Iron
140
100
50
47
ug/L
04/21/18 03:46
1
Lead
<0.19
0.50
0.25
0.19
ug/L
04/21/18 03:46
1
Manganese
2000
2.5
1.3
0.79
ug/L
04/21/18 03:46
1
Nickel
<0.63
2.0
1.0
0.63
ug/L
04/21/18 03:46
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 03:46
1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 03:46
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 03:46
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 03:46
1
Vanadium
<2.2
5.0
2.5
2.2
ug/L
04/21/18 03:46
1
Zinc
<6.9
10
20
6.9
ug/L
04/21/18 03:46
1
Method: 7470A - Mercury (CVAA)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/18/1811:10
1
General Chemistry
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/25/18 09:55
1
Chloride
6500
1000
850
850
ug/L
04/27/18 21:07
5
Sulfate
210000
5000
2500
2400
ug/L
04/26/18 21:19
25
Alkalinity
52000
5000
5000
3700
ug/L
04/24/1814:35
1
Total Dissolved Solids
390000
10000
10000
4300
ug/L
04/17/18 08:24
1
TestAmerica Chicago
Page 99 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-4D(i) Lab Sample ID: 500-143858-16
Date Collected: 04/12/18 12:45 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/24/18 15:18
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/24/18 15:18
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/24/18 15:18
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/24/18 15:18
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 15:18
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 15:18
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/24/18 15:18
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 15:18
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/24/18 15:18
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/24/18 15:18
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 15:18
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/24/18 15:18
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 15:18
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 15:18
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/24/18 15:18
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/24/18 15:18
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 15:18
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/24/18 15:18
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/24/18 15:18
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/24/18 15:18
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/24/18 15:18
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/24/18 15:18
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/24/18 15:18
1
Acetone
4.1 J cn
5.0
2.5
1.7
ug/L
04/24/18 15:18
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/24/18 15:18
1
Acrolein
<23
100
50
23
ug/L
04/24/18 15:18
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/24/18 15:18
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/24/18 15:18
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 15:18
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/24/18 15:18
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/24/18 15:18
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/24/18 15:18
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/24/18 15:18
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/24/18 15:18
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 15:18
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/24/18 15:18
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/24/18 15:18
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/24/18 15:18
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/24/18 15:18
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/24/18 15:18
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/24/18 15:18
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/24/18 15:18
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/24/18 15:18
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/24/18 15:18
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/24/18 15:18
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/24/18 15:18
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/24/18 15:18
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/24/18 15:18
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/24/18 15:18
1
TestAmerica Chicago
Page 100 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-41)(i)
Lab Sample
ID: 500-143858-16
Date Collected: 04/12/18 12:45
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/24/18 15:18
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/24/18 15:18
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/24/18 15:18
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 15:18
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/24/18 15:18
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/24/18 15:18
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/24/18 15:18
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/24/18 15:18
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 15:18
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/24/18 15:18
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/24/18 15:18
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 15:18
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/24/18 15:18
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/24/18 15:18
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/24/18 15:18
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 101 75- 126
4-Bromofluorobenzene (Surr) 106 72 - 124
Dibromofluoromethane 90 75 - 120
Toluene-d8 (Surr) 93 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04124118 15:18
04124118 15:18
04124118 15:18
04124118 15:18
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.24
0.77
0.39
0.24
ug/L
04/20/18 16:57
1
Acenaphthylene
<0.21
0.77
0.39
0.21
ug/L
04/20/18 16:57
1
Acetophenone
<0.51
3.9
1.9
0.51
ug/L
04/20/18 16:57
1
2-Acetylaminofluorene
<1.6
7.7
3.9
1.6
ug/L
04/20/18 16:57
1
4-Aminobiphenyl
<2.9
7.7
3.9
2.9
ug/L
04/20/18 16:57
1
Anthracene
<0.26
0.77
0.39
0.26
ug/L
04/20/18 16:57
1
Benzo[a]anthracene
<0.044
0.15
0.077
0.044
ug/L
04/20/18 16:57
1
Benzo[a]pyrene
<0.076
0.15
0.077
0.076
ug/L
04/20/18 16:57
1
Benzo[b]fluoranthene
<0.062
0.15
0.077
0.062
ug/L
04/20/18 16:57
1
Benzo[g,h,i]perylene
<0.29
0.77
0.39
0.29
ug/L
04/20/18 16:57
1
Benzo[k]fluoranthene
<0.049
0.15
0.077
0.049
ug/L
04/20/18 16:57
1
Benzyl alcohol
<4.7
15
7.7
4.7
ug/L
04/20/18 16:57
1
Bis(2-chloroethoxy)methane
<0.22
1.5
0.77
0.22
ug/L
04/20/18 16:57
1
Bis(2-chloroethyl)ether
<0.23
1.5
0.77
0.23
ug/L
04/20/18 16:57
1
Bis(2-ethylhexyl) phthalate
<1.3
7.7
3.9
1.3
ug/L
04/20/18 16:57
1
4-Bromophenyl phenyl ether
<0.42
3.9
1.9
0.42
ug/L
04/20/18 16:57
1
Butyl benzyl phthalate
<0.37
1.5
0.77
0.37
ug/L
04/20/18 16:57
1
4-Chloroaniline
<1.6
7.7
3.9
1.6
ug/L
04/20/18 16:57
1
Chlorobenzilate
<2.6
7.7
3.9
2.6
ug/L
04/20/18 16:57
1
4-Chloro-3-methylphenol
<1.8
7.7
3.9
1.8
ug/L
04/20/18 16:57
1
2-Chloronaphthalene
<0.18
1.5
0.77
0.18
ug/L
04/20/18 16:57
1
2-Chlorophenol
<0.43
3.9
1.9
0.43
ug/L
04/20/18 16:57
1
4-Chlorophenyl phenyl ether
<0.49
3.9
1.9
0.49
ug/L
04/20/18 16:57
1
Chrysene
<0.053
0.15
0.077
0.053
ug/L
04/20/18 16:57
1
Diallate
<4.3
7.7
4.8
4.3
ug/L
04/20/18 16:57
1
Dibenz(a,h)anthracene
<0.039
0.23
0.12
0.039
ug/L
04/20/18 16:57
1
TestAmerica Chicago
Page 101 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-41)(i) Lab Sample ID: 500-143858-16
Date Collected: 04/12/18 12:45 Matrix: Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.20
1.5
0.77
0.20
ug/L
04/20/18 16:57
1
3,3'-Dichlorobenzidine
<1.3
3.9
1.9
1.3
ug/L
04/20/18 16:57
1
2,4-Dichlorophenol
<2.0
7.7
3.9
2.0
ug/L
04/20/18 16:57
1
2,6-Dichlorophenol
<2.7
7.7
3.9
2.7
ug/L
04/20/18 16:57
1
Diethyl phthalate
<0.28
3.9
1.5
0.28
ug/L
04/20/18 16:57
1
Dimethoate
<1.4
7.7
3.9
1.4
ug/L
04/20/18 16:57
1
7,12-Dimethylbenz(a)anthracene
<2.3
31
15
2.3
ug/L
04/20/18 16:57
1
3,3'-Dimethylbenzidine
<14
31
15
14
ug/L
04/20/18 16:57
1
2,4-Dimethylphenol
<1.4
7.7
3.9
1.4
ug/L
04/20/18 16:57
1
Dimethyl phthalate
<0.24
3.9
1.5
0.24
ug/L
04/20/18 16:57
1
Di-n-butyl phthalate
<0.56
3.9
1.9
0.56
ug/L
04/20/18 16:57
1
4,6-Dinitro-2-methylphenol
<4.6
15
7.7
4.6
ug/L
04/20/18 16:57
1
2,4-Dinitrophenol
<6.6
15
7.7
6.6
ug/L
04/20/18 16:57
1
2,4-Dinitrotoluene
<0.19
0.77
0.39
0.19
ug/L
04/20/18 16:57
1
2,6-Dinitrotoluene
<0.057
0.77
0.39
0.057
ug/L
04/20/18 16:57
1
Di-n-octyl phthalate
<0.81
7.7
3.9
0.81
ug/L
04/20/18 16:57
1
Diphenylamine
<2.0
7.7
3.9
2.0
ug/L
04/20/18 16:57
1
Disulfoton
<1.5
7.7
3.9
1.5
ug/L
04/20/18 16:57
1
Ethyl methanesulfonate
<2.9
15
7.7
2.9
ug/L
04/20/18 16:57
1
Ethyl Parathion
<1.6
7.7
3.9
1.6
ug/L
04/20/18 16:57
1
Famphur
<23
31
24
23
ug/L
04/20/18 16:57
1
Fluoranthene
<0.35
0.77
0.39
0.35
ug/L
04/20/18 16:57
1
Fluorene
<0.19
0.77
0.39
0.19
ug/L
04/20/18 16:57
1
Hexachlorobenzene
<0.061
0.39
0.19
0.061
ug/L
04/20/18 16:57
1
Hexachlorocyclopentadiene
<4.9
15
7.7
4.9
ug/L
04/20/18 16:57
1
Hexachloroethane
<0.46
3.9
1.9
0.46
ug/L
04/20/18 16:57
1
Hexachloropropene
<3.6
15
7.7
3.6
ug/L
04/20/18 16:57
1
Indeno[1,2,3-cd]pyrene
<0.058
0.15
0.077
0.058
ug/L
04/20/18 16:57
1
Isodrin
<5.3
15
7.7
5.3
ug/L
04/20/18 16:57
1
Isophorone
<0.29
1.5
0.77
0.29
ug/L
04/20/18 16:57
1
Isosafrole
<3.0
7.7
3.9
3.0
ug/L
04/20/18 16:57
1
Kepone
<1.3
7.7
3.9
1.3
ug/L
04/20/18 16:57
1
m-Dinitrobenzene
<1.0
3.9
1.9
1.0
ug/L
04/20/18 16:57
1
Methapyrilene
<7.8
31
15
7.8
ug/L
04/20/18 16:57
1
3-Methylcholanthrene
<1.8
7.7
3.9
1.8
ug/L
04/20/18 16:57
1
Methyl methanesulfonate
<4.6
31
15
4.6
ug/L
04/20/18 16:57
1
2-Methylnaphthalene
<0.050
1.5
0.77
0.050
ug/L
04/20/18 16:57
1
Methyl parathion
<1.8
7.7
3.9
1.8
ug/L
04/20/18 16:57
1
2-Methylphenol
<0.24
1.5
0.77
0.24
ug/L
04/20/18 16:57
1
3 & 4 Methylphenol
<0.35
1.5
0.77
0.35
ug/L
04/20/18 16:57
1
Naphthalene
<0.24
0.77
0.39
0.24
ug/L
04/20/18 16:57
1
1,4-Naphthoquinone
<30
31
31
30
ug/L
04/20/18 16:57
1
1-Naphthylamine
<4.6
15
7.7
4.6
ug/L
04/20/18 16:57
1
2-Naphthylamine
<7.0
15
7.7
7.0
ug/L
04/20/18 16:57
1
2-Nitroaniline
<0.99
3.9
1.9
0.99
ug/L
04/20/18 16:57
1
3-Nitroaniline
<1.4
7.7
3.9
1.4
ug/L
04/20/18 16:57
1
4-Nitroaniline
<1.3
7.7
3.9
1.3
ug/L
04/20/18 16:57
1
Nitrobenzene
<0.35
0.77
0.39
0.35
ug/L
04/20/18 16:57
1
5-Nitro-o-toluidine
<2.4
7.7
3.9
2.4
ug/L
04/20/18 16:57
1
TestAmerica Chicago
Page 102 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-41)(i)
Lab Sample ID: 500-143858-16
Date Collected: 04/12/18 12:45
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<1.9
7.7
3.9
1.9
ug/L
04/20/18 16:57
1
4-Nitrophenol
<5.7
15
7.7
5.7
ug/L
04/20/18 16:57
1
N-Nitrosodiethylamine
<6.6
15
7.7
6.6
ug/L
04/20/18 16:57
1
N-Nitrosodimethylamine
<3.7
7.7
3.9
3.7
ug/L
04/20/18 16:57
1
N-Nitrosodi-n-butylamine
<3.2
7.7
3.9
3.2
ug/L
04/20/18 16:57
1
N-Nitrosodi-n-propylamine
<0.12
0.39
0.19
0.12
ug/L
04/20/18 16:57
1
N-Nitrosodiphenylamine
<0.29
1.5
0.77
0.29
ug/L
04/20/18 16:57
1
N-Nitrosomethylethylamine
<5.8
15
7.7
5.8
ug/L
04/20/18 16:57
1
N-Nitrosopiperidine
<2.7
7.7
3.9
2.7
ug/L
04/20/18 16:57
1
N-Nitrosopyrrolidine
<2.6
7.7
3.9
2.6
ug/L
04/20/18 16:57
1
o,o',o"-Triethylphosphorothioate
<4.3
15
7.7
4.3
ug/L
04/20/18 16:57
1
o-Toluidine
<6.1
31
15
6.1
ug/L
04/20/18 16:57
1
2,2'-oxybis[l-chloropropane]
<0.29
1.5
0.77
0.29
ug/L
04/20/18 16:57
1
p-Dimethylamino azobenzene
<2.3
7.7
3.9
2.3
ug/L
04/20/18 16:57
1
Pentachlorobenzene
<2.2
7.7
3.9
2.2
ug/L
04/20/18 16:57
1
Pentachloronitrobenzene
<2.7
7.7
3.9
2.7
ug/L
04/20/18 16:57
1
Phenacetin
<1.7
7.7
3.9
1.7
ug/L
04/20/18 16:57
1
Phenanthrene
<0.23
0.77
0.39
0.23
ug/L
04/20/18 16:57
1
Phenol
<0.52
3.9
1.9
0.52
ug/L
04/20/18 16:57
1
Phorate
<1.7
7.7
3.9
1.7
ug/L
04/20/18 16:57
1
p-Phenylene diamine
<13
62
31
13
ug/L
04/20/18 16:57
1
Pronamide
<1.7
7.7
7.7
1.7
ug/L
04/20/18 16:57
1
Pyrene
<0.33
0.77
0.39
0.33
ug/L
04/20/18 16:57
1
Safrole
<3.1
7.7
3.9
3.1
ug/L
04/20/18 16:57
1
sym-Trinitrobenzene
<1.4
7.7
3.9
1.4
ug/L
04/20/18 16:57
1
2,3,7,8-TCDD (Screen)
<7.7
7.7
7.7
7.7
ug/L
04/20/18 16:57
1
1,2,4,5-Tetrachlorobenzene
<0.44
3.9
1.9
0.44
ug/L
04/20/18 16:57
1
2,3,4,6-Tetrachlorophenol
<0.58
3.9
1.9
0.58
ug/L
04/20/18 16:57
1
Thionazin
<2.0
7.7
3.9
2.0
ug/L
04/20/18 16:57
1
2,4,5-Trichlorophenol
<2.0
7.7
3.9
2.0
ug/L
04/20/18 16:57
1
2,4,6-Trichlorophenol
<0.55
3.9
1.9
0.55
ug/L
04/20/18 16:57
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
82
34 - 110
04116118 16:56
04120118 16:57
1
2-Fluorophenol
53
27- 110
04116118 16:56
04120118 16:57
1
Nitrobenzene-d5
77
36 - 120
04116118 16:56
04120118 16:57
1
Phenol-d5
38
20- 100
04116118 16:56
04120118 16:57
1
Terphenyl-d14
139
40- 145
04116118 16:56
04120118 16:57
1
2,4,6-Tribromophenol
96
40- 145
04116118 16:56
04120118 16:57
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
alpha-BHC
<0.0025
0.039
0.019
0.0025
ug/L
04/20/18 17:19
1
beta-BHC
<0.0099
0.039
0.019
0.0099
ug/L
04/20/18 17:19
1
delta-BHC
<0.010
0.039
0.019
0.010
ug/L
04/20/18 17:19
1
gamma-BHC (Lindane)
<0.0054
0.039
0.019
0.0054
ug/L
04/20/18 17:19
1
Heptachlor
<0.013
0.039
0.019
0.013
ug/L
04/20/18 17:19
1
Aldrin
<0.0051
0.039
0.019
0.0051
ug/L
04/20/18 17:19
1
Heptachlor epoxide
<0.013
0.039
0.019
0.013
ug/L
04/20/18 17:19
1
Endosulfan 1
<0.0040
0.039
0.019
0.0040
ug/L
04/20/18 17:19
1
TestAmerica Chicago
Page 103 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-41)(i)
Lab Sample ID: 500-143858-16
Date Collected: 04/12/18 12:45
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.013
0.039
0.019
0.013
ug/L
04/20/18 17:19
1
4,4'-DDE
<0.0037
0.039
0.019
0.0037
ug/L
04/20/18 17:19
1
Endrin
<0.014
0.039
0.019
0.014
ug/L
04/20/18 17:19
1
Endosulfan II
<0.0027
0.039
0.019
0.0027
ug/L
04/20/18 17:19
1
4,4'-DDD
<0.013
0.039
0.019
0.013
ug/L
04/20/18 17:19
1
Endosulfan sulfate
<0.011
0.039
0.019
0.011
ug/L
04/20/18 17:19
1
4,4'-DDT
<0.0031
0.039
0.019
0.0031
ug/L
04/20/18 17:19
1
Methoxychlor
<0.022
0.078
0.039
0.022
ug/L
04/20/18 17:19
1
Toxaphene
<0.19
0.39
0.19
0.19
ug/L
04/20/18 17:19
1
Endrin aldehyde
<0.0079
0.039
0.019
0.0079
ug/L
04/20/18 17:19
1
Chlordane (technical)
<0.039
0.078
0.039
0.039
ug/L
04/20/18 17:19
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
78
30 - 130
04117118 07:38
04120118 17:19
1
Tetrachloro-m-xylene
64
30 - 120
04117118 07:38
04120118 17:19
1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.065
0.39
0.19
0.065
ug/L
04/17/18 21:43
1
PCB-1221
<0.19
0.39
0.19
0.19
ug/L
04/17/18 21:43
1
PCB-1232
<0.19
0.39
0.19
0.19
ug/L
04/17/18 21:43
1
PCB-1242
<0.19
0.39
0.19
0.19
ug/L
04/17/18 21:43
1
PCB-1248
<0.19
0.39
0.19
0.19
ug/L
04/17/18 21:43
1
PCB-1254
<0.19
0.39
0.19
0.19
ug/L
04/17/18 21:43
1
PCB-1260
<0.068
0.39
0.19
0.068
ug/L
04/17/18 21:43
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
66
30 - 120
04117118 07:38
04117118 21:43
1
DCB Decachlorobiphenyl
89
30 - 140
04117118 07:38
04117118 21:43
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.47
1.0
0.51
0.47
ug/L
04/18/18 05:02
1
Dinoseb
<0.17
2.0
1.0
0.17
ug/L
04/18/18 05:02
1
Pentachlorophenol
<0.091
0.51
0.10
0.091
ug/L
04/18/18 05:02
1
Silvex (2,4,5-TP)
<0.29
1.0
0.51
0.29
ug/L
04/18/18 05:02
1
2,4,5-T
<0.44
1.0
0.51
0.44
ug/L
04/18/18 05:02
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
81
25 - 130
04117118 09:02
04118118 05:02
1
Method: 6020B - Metals (ICP/MS) - Total Recoverable
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 03:50
1
Arsenic
0.37 J
1.0
0.50
0.23
ug/L
04/21/18 03:50
1
Barium
40
2.5
1.3
0.73
ug/L
04/21/18 03:50
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 03:50
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 03:50
1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 03:50
1
Cobalt
<0.40
1.0
0.50
0.40
ug/L
04/21/18 03:50
1
Copper
0.55 J B
2.0
1.0
0.50
ug/L
04/21/18 03:50
1
TestAmerica Chicago
Page 104 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill
- Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-41)(i)
Lab Sample
ID: 500-143858-16
Date Collected: 04/12/18 12:45
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Iron
<47
100
50
47
ug/L
04/21/18 03:50
1
Lead
<0.19
0.50
0.25
0.19
ug/L
04/21/18 03:50
1
Manganese
0.96 J
2.5
1.3
0.79
ug/L
04/21/18 03:50
1
Nickel
<0.63
2.0
1.0
0.63
ug/L
04/21/18 03:50
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 03:50
1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 03:50
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 03:50
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 03:50
1
Vanadium
3.7 J
5.0
2.5
2.2
ug/L
04/21/18 03:50
1
Zinc
<6.9
10
20
6.9
ug/L
04/21/18 03:50
1
Method: 7470A - Mercury (CVAA)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/18/1811:12
1
General Chemistry
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/25/18 09:56
1
Chloride
20000
1000
850
850
ug/L
04/27/18 21:20
5
Sulfate
18000
1000
500
480
ug/L
04/26/18 21:32
5
Alkalinity
190000
5000
5000
3700
ug/L
04/24/1814:42
1
Total Dissolved Solids
290000
10000
10000
4300
ug/L
04/17/18 08:26
1
TestAmerica Chicago
Page 105 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-4(i) Lab Sample ID: 500-143858-17
Date Collected: 04/12/18 14:10 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/25/18 11:24
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/25/18 11:24
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/25/18 11:24
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/25/18 11:24
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/25/18 11:24
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/25/18 11:24
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/25/18 11:24
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/25/18 11:24
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/25/18 11:24
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/25/18 11:24
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/25/18 11:24
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/25/18 11:24
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/25/18 11:24
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/25/18 11:24
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/25/18 11:24
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/25/18 11:24
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/25/18 11:24
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/25/18 11:24
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/25/18 11:24
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/25/18 11:24
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/25/18 11:24
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/25/18 11:24
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/25/18 11:24
1
Acetone
<1.7
5.0
2.5
1.7
ug/L
04/25/18 11:24
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/25/18 11:24
1
Acrolein
<23
100
50
23
ug/L
04/25/18 11:24
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/25/18 11:24
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/25/18 11:24
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/25/18 11:24
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/25/18 11:24
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/25/18 11:24
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/25/18 11:24
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/25/18 11:24
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/25/18 11:24
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/25/18 11:24
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/25/18 11:24
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/25/18 11:24
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/25/18 11:24
1
cis-1,2-Dichloroethene
0.82 J
1.0
0.50
0.41
ug/L
04/25/18 11:24
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/25/18 11:24
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/25/18 11:24
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/25/18 11:24
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/25/18 11:24
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/25/18 11:24
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/25/18 11:24
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/25/18 11:24
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/25/18 11:24
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/25/18 11:24
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/25/18 11:24
1
TestAmerica Chicago
Page 106 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-4(i)
Lab Sample
ID: 500-143858-17
Date Collected: 04/12/18 14:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/25/18 11:24
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/25/18 11:24
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/25/18 11:24
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/25/18 11:24
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/25/18 11:24
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/25/18 11:24
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/25/18 11:24
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/25/18 11:24
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/25/18 11:24
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/25/18 11:24
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/25/18 11:24
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/25/18 11:24
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/25/18 11:24
1
Vinyl chloride
1.6
1.0
0.50
0.20
ug/L
04/25/18 11:24
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/25/18 11:24
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 105 75- 126
4-Bromofluorobenzene (Surr) 102 72 - 124
Dibromofluoromethane 99 75 - 120
Toluene-d8 (Surr) 92 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04125118 11:24
04125118 11:24
04125118 11:24
04/25/18 11:24
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.25
0.80
0.40
0.25
ug/L
04/20/18 17:23
1
Acenaphthylene
<0.21
0.80
0.40
0.21
ug/L
04/20/18 17:23
1
Acetophenone
<0.53
4.0
2.0
0.53
ug/L
04/20/18 17:23
1
2-Acetylaminofluorene
<1.7
8.0
4.0
1.7
ug/L
04/20/18 17:23
1
4-Aminobiphenyl
<3.0
8.0
4.0
3.0
ug/L
04/20/18 17:23
1
Anthracene
<0.27
0.80
0.40
0.27
ug/L
04/20/18 17:23
1
Benzo[a]anthracene
<0.045
0.16
0.080
0.045
ug/L
04/20/18 17:23
1
Benzo[a]pyrene
<0.079
0.16
0.080
0.079
ug/L
04/20/18 17:23
1
Benzo[b]fluoranthene
<0.065
0.16
0.080
0.065
ug/L
04/20/18 17:23
1
Benzo[g,h,i]perylene
<0.30
0.80
0.40
0.30
ug/L
04/20/18 17:23
1
Benzo[k]fluoranthene
<0.051
0.16
0.080
0.051
ug/L
04/20/18 17:23
1
Benzyl alcohol
<4.8
16
8.0
4.8
ug/L
04/20/18 17:23
1
Bis(2-chloroethoxy)methane
<0.23
1.6
0.80
0.23
ug/L
04/20/18 17:23
1
Bis(2-chloroethyl)ether
<0.23
1.6
0.80
0.23
ug/L
04/20/18 17:23
1
Bis(2-ethylhexyl) phthalate
<1.4
8.0
4.0
1.4
ug/L
04/20/18 17:23
1
4-Bromophenyl phenyl ether
<0.43
4.0
2.0
0.43
ug/L
04/20/18 17:23
1
Butyl benzyl phthalate
<0.39
1.6
0.80
0.39
ug/L
04/20/18 17:23
1
4-Chloroaniline
<1.6
8.0
4.0
1.6
ug/L
04/20/18 17:23
1
Chlorobenzilate
<2.7
8.0
4.0
2.7
ug/L
04/20/18 17:23
1
4-Chloro-3-methylphenol
<1.8
8.0
4.0
1.8
ug/L
04/20/18 17:23
1
2-Chloronaphthalene
<0.19
1.6
0.80
0.19
ug/L
04/20/18 17:23
1
2-Chlorophenol
<0.45
4.0
2.0
0.45
ug/L
04/20/18 17:23
1
4-Chlorophenyl phenyl ether
<0.51
4.0
2.0
0.51
ug/L
04/20/18 17:23
1
Chrysene
<0.055
0.16
0.080
0.055
ug/L
04/20/18 17:23
1
Diallate
<4.4
8.0
5.0
4.4
ug/L
04/20/18 17:23
1
Dibenz(a,h)anthracene
<0.041
0.24
0.12
0.041
ug/L
04/20/18 17:23
1
TestAmerica Chicago
Page 107 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-4(i) Lab Sample ID: 500-143858-17
Date Collected: 04/12/18 14:10 Matrix: Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.21
1.6
0.80
0.21
ug/L
04/20/18 17:23
1
3,3'-Dichlorobenzidine
<1.4
4.0
2.0
1.4
ug/L
04/20/18 17:23
1
2,4-Dichlorophenol
<2.1
8.0
4.0
2.1
ug/L
04/20/18 17:23
1
2,6-Dichlorophenol
<2.8
8.0
4.0
2.8
ug/L
04/20/18 17:23
1
Diethyl phthalate
<0.29
4.0
1.6
0.29
ug/L
04/20/18 17:23
1
Dimethoate
<1.5
8.0
4.0
1.5
ug/L
04/20/18 17:23
1
7,12-Dimethylbenz(a)anthracene
<2.4
32
16
2.4
ug/L
04/20/18 17:23
1
3,3'-Dimethylbenzidine
<14
32
16
14
ug/L
04/20/18 17:23
1
2,4-Dimethylphenol
<1.4
8.0
4.0
1.4
ug/L
04/20/18 17:23
1
Dimethyl phthalate
<0.25
4.0
1.6
0.25
ug/L
04/20/18 17:23
1
Di-n-butyl phthalate
<0.59
4.0
2.0
0.59
ug/L
04/20/18 17:23
1
4,6-Dinitro-2-methylphenol
<4.7
16
8.0
4.7
ug/L
04/20/18 17:23
1
2,4-Dinitrophenol
<6.9
16
8.0
6.9
ug/L
04/20/18 17:23
1
2,4-Dinitrotoluene
<0.20
0.80
0.40
0.20
ug/L
04/20/18 17:23
1
2,6-Dinitrotoluene
<0.059
0.80
0.40
0.059
ug/L
04/20/18 17:23
1
Di-n-octyl phthalate
<0.84
8.0
4.0
0.84
ug/L
04/20/18 17:23
1
Diphenylamine
<2.0
8.0
4.0
2.0
ug/L
04/20/18 17:23
1
Disulfoton
<1.5
8.0
4.0
1.5
ug/L
04/20/18 17:23
1
Ethyl methanesulfonate
<3.0
16
8.0
3.0
ug/L
04/20/18 17:23
1
Ethyl Parathion
<1.7
8.0
4.0
1.7
ug/L
04/20/18 17:23
1
Famphur
<24
32
25
24
ug/L
04/20/18 17:23
1
Fluoranthene
<0.36
0.80
0.40
0.36
ug/L
04/20/18 17:23
1
Fluorene
<0.20
0.80
0.40
0.20
ug/L
04/20/18 17:23
1
Hexachlorobenzene
<0.064
0.40
0.20
0.064
ug/L
04/20/18 17:23
1
Hexachlorocyclopentadiene
<5.1
16
8.0
5.1
ug/L
04/20/18 17:23
1
Hexachloroethane
<0.48
4.0
2.0
0.48
ug/L
04/20/18 17:23
1
Hexachloropropene
<3.8
16
8.0
3.8
ug/L
04/20/18 17:23
1
Indeno[1,2,3-cd]pyrene
<0.060
0.16
0.080
0.060
ug/L
04/20/18 17:23
1
Isodrin
<5.5
16
8.0
5.5
ug/L
04/20/18 17:23
1
Isophorone
<0.30
1.6
0.80
0.30
ug/L
04/20/18 17:23
1
Isosafrole
<3.1
8.0
4.0
3.1
ug/L
04/20/18 17:23
1
Kepone
<1.3
8.0
4.0
1.3
ug/L
04/20/18 17:23
1
m-Dinitrobenzene
<1.1
4.0
2.0
1.1
ug/L
04/20/18 17:23
1
Methapyrilene
<8.1
32
16
8.1
ug/L
04/20/18 17:23
1
3-Methylcholanthrene
<1.8
8.0
4.0
1.8
ug/L
04/20/18 17:23
1
Methyl methanesulfonate
<4.8
32
16
4.8
ug/L
04/20/18 17:23
1
2-Methylnaphthalene
<0.052
1.6
0.80
0.052
ug/L
04/20/18 17:23
1
Methyl parathion
<1.9
8.0
4.0
1.9
ug/L
04/20/18 17:23
1
2-Methylphenol
<0.24
1.6
0.80
0.24
ug/L
04/20/18 17:23
1
3 & 4 Methylphenol
<0.36
1.6
0.80
0.36
ug/L
04/20/18 17:23
1
Naphthalene
<0.25
0.80
0.40
0.25
ug/L
04/20/18 17:23
1
1,4-Naphthoquinone
<31
32
32
31
ug/L
04/20/18 17:23
1
1-Naphthylamine
<4.7
16
8.0
4.7
ug/L
04/20/18 17:23
1
2-Naphthylamine
<7.3
16
8.0
7.3
ug/L
04/20/18 17:23
1
2-Nitroaniline
<1.0
4.0
2.0
1.0
ug/L
04/20/18 17:23
1
3-Nitroaniline
<1.4
8.0
4.0
1.4
ug/L
04/20/18 17:23
1
4-Nitroaniline
<1.3
8.0
4.0
1.3
ug/L
04/20/18 17:23
1
Nitrobenzene
<0.36
0.80
0.40
0.36
ug/L
04/20/18 17:23
1
5-Nitro-o-toluidine
<2.5
8.0
4.0
2.5
ug/L
04/20/18 17:23
1
TestAmerica Chicago
Page 108 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-4(i)
Lab Sample ID: 500-143858-17
Date Collected: 04/12/18 14:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<2.0
8.0
4.0
2.0
ug/L
04/20/18 17:23
1
4-Nitrophenol
<6.0
16
8.0
6.0
ug/L
04/20/18 17:23
1
N-Nitrosodiethylamine
<6.9
16
8.0
6.9
ug/L
04/20/18 17:23
1
N-Nitrosodimethylamine
<3.8
8.0
4.0
3.8
ug/L
04/20/18 17:23
1
N-Nitrosodi-n-butylamine
<3.4
8.0
4.0
3.4
ug/L
04/20/18 17:23
1
N-Nitrosodi-n-propylamine
<0.12
0.40
0.20
0.12
ug/L
04/20/18 17:23
1
N-Nitrosodiphenylamine
<0.30
1.6
0.80
0.30
ug/L
04/20/18 17:23
1
N-Nitrosomethylethylamine
<6.0
16
8.0
6.0
ug/L
04/20/18 17:23
1
N-Nitrosopiperidine
<2.8
8.0
4.0
2.8
ug/L
04/20/18 17:23
1
N-Nitrosopyrrolidine
<2.7
8.0
4.0
2.7
ug/L
04/20/18 17:23
1
o,o',o"-Triethylphosphorothioate
<4.4
16
8.0
4.4
ug/L
04/20/18 17:23
1
o-Toluidine
<6.4
32
16
6.4
ug/L
04/20/18 17:23
1
2,2'-oxybis[l-chloropropane]
<0.30
1.6
0.80
0.30
ug/L
04/20/18 17:23
1
p-Dimethylamino azobenzene
<2.4
8.0
4.0
2.4
ug/L
04/20/18 17:23
1
Pentachlorobenzene
<2.2
8.0
4.0
2.2
ug/L
04/20/18 17:23
1
Pentachloronitrobenzene
<2.9
8.0
4.0
2.9
ug/L
04/20/18 17:23
1
Phenacetin
<1.8
8.0
4.0
1.8
ug/L
04/20/18 17:23
1
Phenanthrene
<0.24
0.80
0.40
0.24
ug/L
04/20/18 17:23
1
Phenol
<0.54
4.0
2.0
0.54
ug/L
04/20/18 17:23
1
Phorate
<1.7
8.0
4.0
1.7
ug/L
04/20/18 17:23
1
p-Phenylene diamine
<13
64
32
13
ug/L
04/20/18 17:23
1
Pronamide
<1.7
8.0
8.0
1.7
ug/L
04/20/18 17:23
1
Pyrene
<0.34
0.80
0.40
0.34
ug/L
04/20/18 17:23
1
Safrole
<3.2
8.0
4.0
3.2
ug/L
04/20/18 17:23
1
sym-Trinitrobenzene
<1.5
8.0
4.0
1.5
ug/L
04/20/18 17:23
1
2,3,7,8-TCDD (Screen)
<8.0
8.0
8.0
8.0
ug/L
04/20/18 17:23
1
1,2,4,5-Tetrachlorobenzene
<0.46
4.0
2.0
0.46
ug/L
04/20/18 17:23
1
2,3,4,6-Tetrachlorophenol
<0.60
4.0
2.0
0.60
ug/L
04/20/18 17:23
1
Thionazin
<2.1
8.0
4.0
2.1
ug/L
04/20/18 17:23
1
2,4,5-Trichlorophenol
<2.1
8.0
4.0
2.1
ug/L
04/20/18 17:23
1
2,4,6-Trichlorophenol
<0.57
4.0
2.0
0.57
ug/L
04/20/18 17:23
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
81
34 - 110
04116118 16:56
04120118 17:23
1
2-Fluorophenol
51
27- 110
04116118 16:56
04120118 17:23
1
Nitrobenzene-d5
77
36 - 120
04116118 16:56
04120118 17:23
1
Phenol-d5
37
20- 100
04116118 16:56
04120118 17:23
1
Terphenyl-d14
114
40- 145
04116118 16:56
04120118 17:23
1
2,4,6-Tribromophenol
83
40- 145
04116118 16:56
04120118 17:23
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
alpha-BHC
<0.0025
0.039
0.019
0.0025
ug/L
04/20/18 17:38
1
beta-BHC
<0.0098
0.039
0.019
0.0098
ug/L
04/20/18 17:38
1
delta-BHC
<0.0099
0.039
0.019
0.0099
ug/L
04/20/18 17:38
1
gamma-BHC (Lindane)
<0.0054
0.039
0.019
0.0054
ug/L
04/20/18 17:38
1
Heptachlor
<0.013
0.039
0.019
0.013
ug/L
04/20/18 17:38
1
Aldrin
<0.0051
0.039
0.019
0.0051
ug/L
04/20/18 17:38
1
Heptachlor epoxide
<0.013
0.039
0.019
0.013
ug/L
04/20/18 17:38
1
Endosulfan 1
<0.0040
0.039
0.019
0.0040
ug/L
04/20/18 17:38
1
TestAmerica Chicago
Page 109 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-4(i)
Lab Sample ID: 500-143858-17
Date Collected: 04/12/18 14:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.012
0.039
0.019
0.012
ug/L
04/20/18 17:38
1
4,4'-DDE
<0.0037
0.039
0.019
0.0037
ug/L
04/20/18 17:38
1
Endrin
<0.014
0.039
0.019
0.014
ug/L
04/20/18 17:38
1
Endosulfan II
<0.0027
0.039
0.019
0.0027
ug/L
04/20/18 17:38
1
4,4'-DDD
<0.013
0.039
0.019
0.013
ug/L
04/20/18 17:38
1
Endosulfan sulfate
<0.011
0.039
0.019
0.011
ug/L
04/20/18 17:38
1
4,4'-DDT
<0.0031
0.039
0.019
0.0031
ug/L
04/20/18 17:38
1
Methoxychlor
<0.022
0.077
0.039
0.022
ug/L
04/20/18 17:38
1
Toxaphene
<0.19
0.39
0.19
0.19
ug/L
04/20/18 17:38
1
Endrin aldehyde
<0.0079
0.039
0.019
0.0079
ug/L
04/20/18 17:38
1
Chlordane (technical)
<0.039
0.077
0.039
0.039
ug/L
04/20/18 17:38
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
70
30 - 130
04117118 07:38
04120118 17:38
1
Tetrachloro-m-xylene
59
30 - 120
04117118 07:38
04120118 17:38
1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.065
0.39
0.19
0.065
ug/L
04/17/18 22:32
1
PCB-1221
<0.19
0.39
0.19
0.19
ug/L
04/17/18 22:32
1
PCB-1232
<0.19
0.39
0.19
0.19
ug/L
04/17/18 22:32
1
PCB-1242
<0.19
0.39
0.19
0.19
ug/L
04/17/18 22:32
1
PCB-1248
<0.19
0.39
0.19
0.19
ug/L
04/17/18 22:32
1
PCB-1254
<0.19
0.39
0.19
0.19
ug/L
04/17/18 22:32
1
PCB-1260
<0.067
0.39
0.19
0.067
ug/L
04/17/18 22:32
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
72
30 - 120
04117118 07:38
04117118 22:32
1
DCB Decachlorobiphenyl
84
30 - 140
04117118 07:38
04117118 22:32
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.46
0.98
0.49
0.46
ug/L
04/18/18 05:26
1
Dinoseb
<0.16
2.0
0.98
0.16
ug/L
04/18/18 05:26
1
Pentachlorophenol
<0.088
0.49
0.098
0.088
ug/L
04/18/18 05:26
1
Silvex (2,4,5-TP)
<0.28
0.98
0.49
0.28
ug/L
04/18/18 05:26
1
2,4,5-T
<0.43
0.98
0.49
0.43
ug/L
04/18/18 05:26
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
113
25 - 130
04117118 09:02
04118118 05:26
1
Method: 6020B - Metals (ICP/MS)
- Total Recoverable
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 03:54
1
Arsenic
0.56 J
1.0
0.50
0.23
ug/L
04/21/18 03:54
1
Barium
210
2.5
1.3
0.73
ug/L
04/21/18 03:54
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 03:54
1
Cadmium
0.35 J
0.50
0.25
0.17
ug/L
04/21/18 03:54
1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 03:54
1
Cobalt
39
1.0
0.50
0.40
ug/L
04/21/18 03:54
1
Copper
5.3 B
2.0
1.0
0.50
ug/L
04/21/18 03:54
1
TestAmerica Chicago
Page 110 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill
- Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-4(i)
Lab Sample
ID: 500-143858-17
Date Collected: 04/12/18 14:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Iron
53000
100
50
47
ug/L
04/21/18 03:54
1
Lead
0.21 J
0.50
0.25
0.19
ug/L
04/21/18 03:54
1
Manganese
12000
2.5
1.3
0.79
ug/L
04/21/18 03:54
1
Nickel
8.0
2.0
1.0
0.63
ug/L
04/21/18 03:54
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 03:54
1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 03:54
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 03:54
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 03:54
1
Vanadium
<2.2
5.0
2.5
2.2
ug/L
04/21/18 03:54
1
Zinc
19 B
10
20
6.9
ug/L
04/21/18 03:54
1
Method: 7470A - Mercury (CVAA)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/18/1811:14
1
General Chemistry
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/25/18 09:59
1
Chloride
11000
1000
850
850
ug/L
04/27/18 21:32
5
Sulfate
26000
1000
500
480
ug/L
04/26/18 21:44
5
Alkalinity
340000
5000
5000
3700
ug/L
04/24/1814:11
1
Total Dissolved Solids
460000
10000
10000
4300
ug/L
04/17/18 08:29
1
TestAmerica Chicago
Page 111 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-6(i) Lab Sample ID: 500-143858-18
Date Collected: 04/11/18 12:20 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/24/18 16:10
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/24/18 16:10
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/24/18 16:10
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/24/18 16:10
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 16:10
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 16:10
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/24/18 16:10
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 16:10
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/24/18 16:10
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/24/18 16:10
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 16:10
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/24/18 16:10
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 16:10
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 16:10
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/24/18 16:10
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/24/18 16:10
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 16:10
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/24/18 16:10
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/24/18 16:10
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/24/18 16:10
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/24/18 16:10
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/24/18 16:10
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/24/18 16:10
1
Acetone
8.3 cn
5.0
2.5
1.7
ug/L
04/24/18 16:10
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/24/18 16:10
1
Acrolein
<23
100
50
23
ug/L
04/24/18 16:10
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/24/18 16:10
1
Benzene
0.27 J
0.50
0.25
0.15
ug/L
04/24/18 16:10
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 16:10
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/24/18 16:10
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/24/18 16:10
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/24/18 16:10
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/24/18 16:10
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/24/18 16:10
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 16:10
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/24/18 16:10
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/24/18 16:10
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/24/18 16:10
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/24/18 16:10
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/24/18 16:10
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/24/18 16:10
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/24/18 16:10
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/24/18 16:10
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/24/18 16:10
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/24/18 16:10
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/24/18 16:10
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/24/18 16:10
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/24/18 16:10
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/24/18 16:10
1
TestAmerica Chicago
Page 112 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-6(i)
Lab Sample
ID: 500-143858-18
Date Collected: 04/11/18 12:20
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/24/18 16:10
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/24/18 16:10
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/24/18 16:10
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 16:10
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/24/18 16:10
1
Tetrahydrofuran
8.7 J
10
5.0
1.9
ug/L
04/24/18 16:10
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/24/18 16:10
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/24/18 16:10
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 16:10
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/24/18 16:10
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/24/18 16:10
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 16:10
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/24/18 16:10
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/24/18 16:10
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/24/18 16:10
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 101 75- 126
4-Bromofluorobenzene (Surr) 107 72 - 124
Dibromofluoromethane 90 75 - 120
Toluene-d8 (Surr) 92 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04124118 16:10
04124118 16:10
04124118 16:10
04124118 16:10
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.23
0.75
0.37
0.23
ug/L
04/20/18 17:48
1
Acenaphthylene
<0.20
0.75
0.37
0.20
ug/L
04/20/18 17:48
1
Acetophenone
<0.50
3.7
1.9
0.50
ug/L
04/20/18 17:48
1
2-Acetylaminofluorene
<1.6
7.5
3.7
1.6
ug/L
04/20/18 17:48
1
4-Aminobiphenyl
<2.8
7.5
3.7
2.8
ug/L
04/20/18 17:48
1
Anthracene
<0.25
0.75
0.37
0.25
ug/L
04/20/18 17:48
1
Benzo[a]anthracene
<0.042
0.15
0.075
0.042
ug/L
04/20/18 17:48
1
Benzo[a]pyrene
<0.074
0.15
0.075
0.074
ug/L
04/20/18 17:48
1
Benzo[b]fluoranthene
<0.060
0.15
0.075
0.060
ug/L
04/20/18 17:48
1
Benzo[g,h,i]perylene
<0.28
0.75
0.37
0.28
ug/L
04/20/18 17:48
1
Benzo[k]fluoranthene
<0.048
0.15
0.075
0.048
ug/L
04/20/18 17:48
1
Benzyl alcohol
<4.5
15
7.5
4.5
ug/L
04/20/18 17:48
1
Bis(2-chloroethoxy)methane
<0.21
1.5
0.75
0.21
ug/L
04/20/18 17:48
1
Bis(2-chloroethyl)ether
<0.22
1.5
0.75
0.22
ug/L
04/20/18 17:48
1
Bis(2-ethylhexyl) phthalate
<1.3
7.5
3.7
1.3
ug/L
04/20/18 17:48
1
4-Bromophenyl phenyl ether
<0.40
3.7
1.9
0.40
ug/L
04/20/18 17:48
1
Butyl benzyl phthalate
<0.36
1.5
0.75
0.36
ug/L
04/20/18 17:48
1
4-Chloroaniline
<1.5
7.5
3.7
1.5
ug/L
04/20/18 17:48
1
Chlorobenzilate
<2.5
7.5
3.7
2.5
ug/L
04/20/18 17:48
1
4-Chloro-3-methylphenol
<1.7
7.5
3.7
1.7
ug/L
04/20/18 17:48
1
2-Chloronaphthalene
<0.18
1.5
0.75
0.18
ug/L
04/20/18 17:48
1
2-Chlorophenol
<0.42
3.7
1.9
0.42
ug/L
04/20/18 17:48
1
4-Chlorophenyl phenyl ether
<0.47
3.7
1.9
0.47
ug/L
04/20/18 17:48
1
Chrysene
<0.051
0.15
0.075
0.051
ug/L
04/20/18 17:48
1
Diallate
<4.1
7.5
4.7
4.1
ug/L
04/20/18 17:48
1
Dibenz(a,h)anthracene
<0.038
0.22
0.11
0.038
ug/L
04/20/18 17:48
1
TestAmerica Chicago
Page 113 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-6(i) Lab Sample ID: 500-143858-18
Date Collected: 04/11/18 12:20 Matrix: Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.20
1.5
0.75
0.20
ug/L
04/20/18 17:48
1
3,3'-Dichlorobenzidine
<1.3
3.7
1.9
1.3
ug/L
04/20/18 17:48
1
2,4-Dichlorophenol
<1.9
7.5
3.7
1.9
ug/L
04/20/18 17:48
1
2,6-Dichlorophenol
<2.6
7.5
3.7
2.6
ug/L
04/20/18 17:48
1
Diethyl phthalate
<0.27
3.7
1.5
0.27
ug/L
04/20/18 17:48
1
Dimethoate
<1.4
7.5
3.7
1.4
ug/L
04/20/18 17:48
1
7,12-Dimethylbenz(a)anthracene
<2.2
30
15
2.2
ug/L
04/20/18 17:48
1
3,3'-Dimethylbenzidine
<13
30
15
13
ug/L
04/20/18 17:48
1
2,4-Dimethylphenol
<1.3
7.5
3.7
1.3
ug/L
04/20/18 17:48
1
Dimethyl phthalate
<0.23
3.7
1.5
0.23
ug/L
04/20/18 17:48
1
Di-n-butyl phthalate
0.68 J
3.7
1.9
0.54
ug/L
04/20/18 17:48
1
4,6-Dinitro-2-methylphenol
<4.4
15
7.5
4.4
ug/L
04/20/18 17:48
1
2,4-Dinitrophenol
<6.4
15
7.5
6.4
ug/L
04/20/18 17:48
1
2,4-Dinitrotoluene
<0.18
0.75
0.37
0.18
ug/L
04/20/18 17:48
1
2,6-Dinitrotoluene
<0.055
0.75
0.37
0.055
ug/L
04/20/18 17:48
1
Di-n-octyl phthalate
<0.78
7.5
3.7
0.78
ug/L
04/20/18 17:48
1
Diphenylamine
<1.9
7.5
3.7
1.9
ug/L
04/20/18 17:48
1
Disulfoton
<1.4
7.5
3.7
1.4
ug/L
04/20/18 17:48
1
Ethyl methanesulfonate
<2.8
15
7.5
2.8
ug/L
04/20/18 17:48
1
Ethyl Parathion
<1.6
7.5
3.7
1.6
ug/L
04/20/18 17:48
1
Famphur
<22
30
23
22
ug/L
04/20/18 17:48
1
Fluoranthene
<0.34
0.75
0.37
0.34
ug/L
04/20/18 17:48
1
Fluorene
<0.18
0.75
0.37
0.18
ug/L
04/20/18 17:48
1
Hexachlorobenzene
<0.059
0.37
0.19
0.059
ug/L
04/20/18 17:48
1
Hexachlorocyclopentadiene
<4.8
15
7.5
4.8
ug/L
04/20/18 17:48
1
Hexachloroethane
<0.45
3.7
1.9
0.45
ug/L
04/20/18 17:48
1
Hexachloropropene
<3.5
15
7.5
3.5
ug/L
04/20/18 17:48
1
Indeno[1,2,3-cd]pyrene
<0.056
0.15
0.075
0.056
ug/L
04/20/18 17:48
1
Isodrin
<5.1
15
7.5
5.1
ug/L
04/20/18 17:48
1
Isophorone
<0.28
1.5
0.75
0.28
ug/L
04/20/18 17:48
1
Isosafrole
<2.9
7.5
3.7
2.9
ug/L
04/20/18 17:48
1
Kepone
<1.2
7.5
3.7
1.2
ug/L
04/20/18 17:48
1
m-Dinitrobenzene
<0.99
3.7
1.9
0.99
ug/L
04/20/18 17:48
1
Methapyrilene
<7.6
30
15
7.6
ug/L
04/20/18 17:48
1
3-Methylcholanthrene
<1.7
7.5
3.7
1.7
ug/L
04/20/18 17:48
1
Methyl methanesulfonate
<4.4
30
15
4.4
ug/L
04/20/18 17:48
1
2-Methylnaphthalene
<0.049
1.5
0.75
0.049
ug/L
04/20/18 17:48
1
Methyl parathion
<1.7
7.5
3.7
1.7
ug/L
04/20/18 17:48
1
2-Methylphenol
<0.23
1.5
0.75
0.23
ug/L
04/20/18 17:48
1
3 & 4 Methylphenol
<0.33
1.5
0.75
0.33
ug/L
04/20/18 17:48
1
Naphthalene
0.59 J
0.75
0.37
0.23
ug/L
04/20/18 17:48
1
1,4-Naphthoquinone
<29
30
30
29
ug/L
04/20/18 17:48
1
1-Naphthylamine
<4.4
15
7.5
4.4
ug/L
04/20/18 17:48
1
2-Naphthylamine
<6.8
15
7.5
6.8
ug/L
04/20/18 17:48
1
2-Nitroaniline
<0.96
3.7
1.9
0.96
ug/L
04/20/18 17:48
1
3-Nitroaniline
<1.3
7.5
3.7
1.3
ug/L
04/20/18 17:48
1
4-Nitroaniline
<1.2
7.5
3.7
1.2
ug/L
04/20/18 17:48
1
Nitrobenzene
<0.33
0.75
0.37
0.33
ug/L
04/20/18 17:48
1
5-Nitro-o-toluidine
<2.3
7.5
3.7
2.3
ug/L
04/20/18 17:48
1
TestAmerica Chicago
Page 114 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-6(i)
Lab Sample ID: 500-143858-18
Date Collected: 04/11/18 12:20
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<1.9
7.5
3.7
1.9
ug/L
04/20/18 17:48
1
4-Nitrophenol
<5.5
15
7.5
5.5
ug/L
04/20/18 17:48
1
N-Nitrosodiethylamine
<6.4
15
7.5
6.4
ug/L
04/20/18 17:48
1
N-Nitrosodimethylamine
<3.5
7.5
3.7
3.5
ug/L
04/20/18 17:48
1
N-Nitrosodi-n-butylamine
<3.1
7.5
3.7
3.1
ug/L
04/20/18 17:48
1
N-Nitrosodi-n-propylamine
<0.11
0.37
0.19
0.11
ug/L
04/20/18 17:48
1
N-Nitrosodiphenylamine
<0.28
1.5
0.75
0.28
ug/L
04/20/18 17:48
1
N-Nitrosomethylethylamine
<5.6
15
7.5
5.6
ug/L
04/20/18 17:48
1
N-Nitrosopiperidine
<2.6
7.5
3.7
2.6
ug/L
04/20/18 17:48
1
N-Nitrosopyrrolidine
<2.5
7.5
3.7
2.5
ug/L
04/20/18 17:48
1
o,o',o"-Triethylphosphorothioate
<4.1
15
7.5
4.1
ug/L
04/20/18 17:48
1
o-Toluidine
<5.9
30
15
5.9
ug/L
04/20/18 17:48
1
2,2'-oxybis[l-chloropropane]
<0.28
1.5
0.75
0.28
ug/L
04/20/18 17:48
1
p-Dimethylamino azobenzene
<2.2
7.5
3.7
2.2
ug/L
04/20/18 17:48
1
Pentachlorobenzene
<2.1
7.5
3.7
2.1
ug/L
04/20/18 17:48
1
Pentachloronitrobenzene
<2.7
7.5
3.7
2.7
ug/L
04/20/18 17:48
1
Phenacetin
<1.7
7.5
3.7
1.7
ug/L
04/20/18 17:48
1
Phenanthrene
<0.22
0.75
0.37
0.22
ug/L
04/20/18 17:48
1
Phenol
<0.50
3.7
1.9
0.50
ug/L
04/20/18 17:48
1
Phorate
<1.6
7.5
3.7
1.6
ug/L
04/20/18 17:48
1
p-Phenylene diamine
<12
60
30
12
ug/L
04/20/18 17:48
1
Pronamide
<1.6
7.5
7.5
1.6
ug/L
04/20/18 17:48
1
Pyrene
<0.32
0.75
0.37
0.32
ug/L
04/20/18 17:48
1
Safrole
<3.0
7.5
3.7
3.0
ug/L
04/20/18 17:48
1
sym-Trinitrobenzene
<1.4
7.5
3.7
1.4
ug/L
04/20/18 17:48
1
2,3,7,8-TCDD (Screen)
<7.5
7.5
7.5
7.5
ug/L
04/20/18 17:48
1
1,2,4,5-Tetrachlorobenzene
<0.43
3.7
1.9
0.43
ug/L
04/20/18 17:48
1
2,3,4,6-Tetrachlorophenol
<0.56
3.7
1.9
0.56
ug/L
04/20/18 17:48
1
Thionazin
<1.9
7.5
3.7
1.9
ug/L
04/20/18 17:48
1
2,4,5-Trichlorophenol
<1.9
7.5
3.7
1.9
ug/L
04/20/18 17:48
1
2,4,6-Trichlorophenol
<0.53
3.7
1.9
0.53
ug/L
04/20/18 17:48
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
100
34 - 110
04116118 16:56
04120118 17:48
1
2-Fluorophenol
63
27- 110
04116118 16:56
04120118 17:48
1
Nitrobenzene-d5
93
36 - 120
04116118 16:56
04120118 17:48
1
Phenol-d5
43
20- 100
04116118 16:56
04120118 17:48
1
Terphenyl-d14
137
40- 145
04116118 16:56
04120118 17:48
1
2,4,6-Tribromophenol
104
40- 145
04116118 16:56
04120118 17:48
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
alpha-BHC
<0.0024
0.037
0.018
0.0024
ug/L
04/20/18 17:57
1
beta-BHC
<0.0094
0.037
0.018
0.0094
ug/L
04/20/18 17:57
1
delta-BHC
<0.0095
0.037
0.018
0.0095
ug/L
04/20/18 17:57
1
gamma-BHC (Lindane)
<0.0051
0.037
0.018
0.0051
ug/L
04/20/18 17:57
1
Heptachlor
<0.012
0.037
0.018
0.012
ug/L
04/20/18 17:57
1
Aldrin
<0.0049
0.037
0.018
0.0049
ug/L
04/20/18 17:57
1
Heptachlor epoxide
<0.013
0.037
0.018
0.013
ug/L
04/20/18 17:57
1
Endosulfan 1
<0.0038
0.037
0.018
0.0038
ug/L
04/20/18 17:57
1
TestAmerica Chicago
Page 115 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-6(i)
Lab Sample ID: 500-143858-18
Date Collected: 04/11/18 12:20
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.012
0.037
0.018
0.012
ug/L
04/20/18 17:57
1
4,4'-DDE
<0.0035
0.037
0.018
0.0035
ug/L
04/20/18 17:57
1
Endrin
<0.013
0.037
0.018
0.013
ug/L
04/20/18 17:57
1
Endosulfan II
<0.0026
0.037
0.018
0.0026
ug/L
04/20/18 17:57
1
4,4'-DDD
<0.012
0.037
0.018
0.012
ug/L
04/20/18 17:57
1
Endosulfan sulfate
<0.011
0.037
0.018
0.011
ug/L
04/20/18 17:57
1
4,4'-DDT
<0.0029
0.037
0.018
0.0029
ug/L
04/20/18 17:57
1
Methoxychlor
<0.021
0.074
0.037
0.021
ug/L
04/20/18 17:57
1
Toxaphene
<0.18
0.37
0.18
0.18
ug/L
04/20/18 17:57
1
Endrin aldehyde
<0.0075
0.037
0.018
0.0075
ug/L
04/20/18 17:57
1
Chlordane (technical)
<0.037
0.074
0.037
0.037
ug/L
04/20/18 17:57
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
66
30 - 130
04117118 07:38
04120118 17:57
1
Tetrachloro-m-xylene
57
30 - 120
04117118 07:38
04120118 17:57
1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.062
0.37
0.18
0.062
ug/L
04/17/18 22:48
1
PCB-1221
<0.18
0.37
0.18
0.18
ug/L
04/17/18 22:48
1
PCB-1232
<0.18
0.37
0.18
0.18
ug/L
04/17/18 22:48
1
PCB-1242
<0.18
0.37
0.18
0.18
ug/L
04/17/18 22:48
1
PCB-1248
<0.18
0.37
0.18
0.18
ug/L
04/17/18 22:48
1
PCB-1254
<0.18
0.37
0.18
0.18
ug/L
04/17/18 22:48
1
PCB-1260
<0.064
0.37
0.18
0.064
ug/L
04/17/18 22:48
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
71
30 - 120
04117118 07:38
04117118 22:48
1
DCB Decachlorobiphenyl
77
30 - 140
04117118 07:38
04117118 22:48
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.45
0.96
0.48
0.45
ug/L
04/18/18 05:50
1
Dinoseb
<0.16
1.9
0.96
0.16
ug/L
04/18/18 05:50
1
Pentachlorophenol
<0.086
0.48
0.096
0.086
ug/L
04/18/18 05:50
1
Silvex (2,4,5-TP)
<0.28
0.96
0.48
0.28
ug/L
04/18/18 05:50
1
2,4,5-T
<0.41
0.96
0.48
0.41
ug/L
04/18/18 05:50
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
97
25 - 130
04117118 09:02
04118118 05:50
1
Method: 6020B - Metals (ICP/MS)
- Total Recoverable
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 04:05
1
Arsenic
1.0
1.0
0.50
0.23
ug/L
04/21/18 04:05
1
Barium
210
2.5
1.3
0.73
ug/L
04/21/18 04:05
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 04:05
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 04:05
1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 04:05
1
Cobalt
9.3
1.0
0.50
0.40
ug/L
04/21/18 04:05
1
Copper
0.96 J B
2.0
1.0
0.50
ug/L
04/21/18 04:05
1
TestAmerica Chicago
Page 116 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill
- Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-6(i)
Lab Sample
ID: 500-143858-18
Date Collected: 04/11/18 12:20
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Iron
33000
100
50
47
ug/L
04/21/18 04:05
1
Lead
<0.19
0.50
0.25
0.19
ug/L
04/21/18 04:05
1
Manganese
4700
2.5
1.3
0.79
ug/L
04/21/18 04:05
1
Nickel
1.6 J
2.0
1.0
0.63
ug/L
04/21/18 04:05
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 04:05
1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 04:05
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 04:05
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 04:05
1
Vanadium
<2.2
5.0
2.5
2.2
ug/L
04/21/18 04:05
1
Zinc
<6.9
10
20
6.9
ug/L
04/21/18 04:05
1
Method: 7470A - Mercury (CVAA)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/18/1811:15
1
General Chemistry
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/25/18 09:59
1
Chloride
48000
2000
1700
1700
ug/L
04/27/18 21:44
10
Sulfate
9100
200
100
95
ug/L
04/26/18 21:57
1
Alkalinity
530000
5000
5000
3700
ug/L
04/23/1815:05
1
Total Dissolved Solids
700000
10000
10000
4300
ug/L
04/17/18 23:04
1
TestAmerica Chicago
Page 117 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-7D(i) Lab Sample ID: 500-143858-19
Date Collected: 04/11/18 09:30 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/24/18 16:35
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/24/18 16:35
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/24/18 16:35
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/24/18 16:35
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 16:35
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 16:35
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/24/18 16:35
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 16:35
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/24/18 16:35
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/24/18 16:35
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 16:35
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/24/18 16:35
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 16:35
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 16:35
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/24/18 16:35
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/24/18 16:35
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 16:35
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/24/18 16:35
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/24/18 16:35
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/24/18 16:35
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/24/18 16:35
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/24/18 16:35
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/24/18 16:35
1
Acetone
11 cn
5.0
2.5
1.7
ug/L
04/24/18 16:35
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/24/18 16:35
1
Acrolein
<23
100
50
23
ug/L
04/24/18 16:35
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/24/18 16:35
1
Benzene
0.22 J
0.50
0.25
0.15
ug/L
04/24/18 16:35
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 16:35
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/24/18 16:35
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/24/18 16:35
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/24/18 16:35
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/24/18 16:35
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/24/18 16:35
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 16:35
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/24/18 16:35
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/24/18 16:35
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/24/18 16:35
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/24/18 16:35
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/24/18 16:35
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/24/18 16:35
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/24/18 16:35
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/24/18 16:35
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/24/18 16:35
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/24/18 16:35
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/24/18 16:35
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/24/18 16:35
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/24/18 16:35
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/24/18 16:35
1
TestAmerica Chicago
Page 118 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-71)(i)
Lab Sample
ID: 500-143858-19
Date Collected: 04/11/18 09:30
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/24/18 16:35
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/24/18 16:35
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/24/18 16:35
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 16:35
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/24/18 16:35
1
Tetrahydrofuran
15
10
5.0
1.9
ug/L
04/24/18 16:35
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/24/18 16:35
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/24/18 16:35
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 16:35
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/24/18 16:35
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/24/18 16:35
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 16:35
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/24/18 16:35
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/24/18 16:35
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/24/18 16:35
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 102 75- 126
4-Bromofluorobenzene (Surr) 105 72 - 124
Dibromofluoromethane 95 75 - 120
Toluene-d8 (Surr) 88 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04124118 16:35
04124118 16:35
04124118 16:35
04124118 16:35
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.24
0.77
0.39
0.24
ug/L
04/19/18 20:23
1
Acenaphthylene
<0.21
0.77
0.39
0.21
ug/L
04/19/18 20:23
1
Acetophenone
<0.51
3.9
1.9
0.51
ug/L
04/19/18 20:23
1
2-Acetylaminofluorene
<1.6
7.7
3.9
1.6
ug/L
04/19/18 20:23
1
4-Aminobiphenyl
<2.9
7.7
3.9
2.9
ug/L
04/19/18 20:23
1
Anthracene
<0.26
0.77
0.39
0.26
ug/L
04/19/18 20:23
1
Benzo[a]anthracene
<0.044
0.15
0.077
0.044
ug/L
04/19/18 20:23
1
Benzo[a]pyrene
<0.076
0.15
0.077
0.076
ug/L
04/19/18 20:23
1
Benzo[b]fluoranthene
<0.062
0.15
0.077
0.062
ug/L
04/19/18 20:23
1
Benzo[g,h,i]perylene
<0.29
0.77
0.39
0.29
ug/L
04/19/18 20:23
1
Benzo[k]fluoranthene
<0.049
0.15
0.077
0.049
ug/L
04/19/18 20:23
1
Benzyl alcohol
<4.7
15
7.7
4.7
ug/L
04/19/18 20:23
1
Bis(2-chloroethoxy)methane
<0.22
1.5
0.77
0.22
ug/L
04/19/18 20:23
1
Bis(2-chloroethyl)ether
<0.23
1.5
0.77
0.23
ug/L
04/19/18 20:23
1
Bis(2-ethylhexyl) phthalate
<1.3
7.7
3.9
1.3
ug/L
04/19/18 20:23
1
4-Bromophenyl phenyl ether
<0.42
3.9
1.9
0.42
ug/L
04/19/18 20:23
1
Butyl benzyl phthalate
<0.37
1.5
0.77
0.37
ug/L
04/19/18 20:23
1
4-Chloroaniline
<1.6
7.7
3.9
1.6
ug/L
04/19/18 20:23
1
Chlorobenzilate
<2.6
7.7
3.9
2.6
ug/L
04/19/18 20:23
1
4-Chloro-3-methylphenol
<1.8
7.7
3.9
1.8
ug/L
04/19/18 20:23
1
2-Chloronaphthalene
<0.18
1.5
0.77
0.18
ug/L
04/19/18 20:23
1
2-Chlorophenol
<0.43
3.9
1.9
0.43
ug/L
04/19/18 20:23
1
4-Chlorophenyl phenyl ether
<0.49
3.9
1.9
0.49
ug/L
04/19/18 20:23
1
Chrysene
<0.053
0.15
0.077
0.053
ug/L
04/19/18 20:23
1
Diallate
<4.3
7.7
4.8
4.3
ug/L
04/19/18 20:23
1
Dibenz(a,h)anthracene
<0.039
0.23
0.12
0.039
ug/L
04/19/18 20:23
1
TestAmerica Chicago
Page 119 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-71)(i) Lab Sample ID: 500-143858-19
Date Collected: 04/11/18 09:30 Matrix: Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.20
1.5
0.77
0.20
ug/L
04/19/18 20:23
1
3,3'-Dichlorobenzidine
<1.3
3.9
1.9
1.3
ug/L
04/19/18 20:23
1
2,4-Dichlorophenol
<2.0
7.7
3.9
2.0
ug/L
04/19/18 20:23
1
2,6-Dichlorophenol
<2.7
7.7
3.9
2.7
ug/L
04/19/18 20:23
1
Diethyl phthalate
<0.28
3.9
1.5
0.28
ug/L
04/19/18 20:23
1
Dimethoate
<1.4
7.7
3.9
1.4
ug/L
04/19/18 20:23
1
7,12-Dimethylbenz(a)anthracene
<2.3
31
15
2.3
ug/L
04/19/18 20:23
1
3,3'-Dimethylbenzidine
<14
31
15
14
ug/L
04/19/18 20:23
1
2,4-Dimethylphenol
<1.4
7.7
3.9
1.4
ug/L
04/19/18 20:23
1
Dimethyl phthalate
<0.24
3.9
1.5
0.24
ug/L
04/19/18 20:23
1
Di-n-butyl phthalate
2.2 J
3.9
1.9
0.56
ug/L
04/19/18 20:23
1
4,6-Dinitro-2-methylphenol
<4.5
15
7.7
4.5
ug/L
04/19/18 20:23
1
2,4-Dinitrophenol
<6.6
15
7.7
6.6
ug/L
04/19/18 20:23
1
2,4-Dinitrotoluene
<0.19
0.77
0.39
0.19
ug/L
04/19/18 20:23
1
2,6-Dinitrotoluene
<0.057
0.77
0.39
0.057
ug/L
04/19/18 20:23
1
Di-n-octyl phthalate
<0.81
7.7
3.9
0.81
ug/L
04/19/18 20:23
1
Diphenylamine
<2.0
7.7
3.9
2.0
ug/L
04/19/18 20:23
1
Disulfoton
<1.5
7.7
3.9
1.5
ug/L
04/19/18 20:23
1
Ethyl methanesulfonate
<2.9
15
7.7
2.9
ug/L
04/19/18 20:23
1
Ethyl Parathion
<1.6
7.7
3.9
1.6
ug/L
04/19/18 20:23
1
Famphur
<23
31
24
23
ug/L
04/19/18 20:23
1
Fluoranthene
<0.35
0.77
0.39
0.35
ug/L
04/19/18 20:23
1
Fluorene
<0.19
0.77
0.39
0.19
ug/L
04/19/18 20:23
1
Hexachlorobenzene
<0.061
0.39
0.19
0.061
ug/L
04/19/18 20:23
1
Hexachlorocyclopentadiene
<4.9
15
7.7
4.9
ug/L
04/19/18 20:23
1
Hexachloroethane
<0.46
3.9
1.9
0.46
ug/L
04/19/18 20:23
1
Hexachloropropene
<3.6
15
7.7
3.6
ug/L
04/19/18 20:23
1
Indeno[1,2,3-cd]pyrene
<0.058
0.15
0.077
0.058
ug/L
04/19/18 20:23
1
Isodrin
<5.3
15
7.7
5.3
ug/L
04/19/18 20:23
1
Isophorone
<0.29
1.5
0.77
0.29
ug/L
04/19/18 20:23
1
Isosafrole
<3.0
7.7
3.9
3.0
ug/L
04/19/18 20:23
1
Kepone
<1.3
7.7
3.9
1.3
ug/L
04/19/18 20:23
1
m-Dinitrobenzene
<1.0
3.9
1.9
1.0
ug/L
04/19/18 20:23
1
Methapyrilene
<7.8
31
15
7.8
ug/L
04/19/18 20:23
1
3-Methylcholanthrene
<1.8
7.7
3.9
1.8
ug/L
04/19/18 20:23
1
Methyl methanesulfonate
<4.6
31
15
4.6
ug/L
04/19/18 20:23
1
2-Methylnaphthalene
<0.050
1.5
0.77
0.050
ug/L
04/19/18 20:23
1
Methyl parathion
<1.8
7.7
3.9
1.8
ug/L
04/19/18 20:23
1
2-Methylphenol
<0.24
1.5
0.77
0.24
ug/L
04/19/18 20:23
1
3 & 4 Methylphenol
<0.35
1.5
0.77
0.35
ug/L
04/19/18 20:23
1
Naphthalene
<0.24
0.77
0.39
0.24
ug/L
04/19/18 20:23
1
1,4-Naphthoquinone
<30
31
31
30
ug/L
04/19/18 20:23
1
1-Naphthylamine
<4.6
15
7.7
4.6
ug/L
04/19/18 20:23
1
2-Naphthylamine
<7.0
15
7.7
7.0
ug/L
04/19/18 20:23
1
2-Nitroaniline
<0.99
3.9
1.9
0.99
ug/L
04/19/18 20:23
1
3-Nitroaniline
<1.4
7.7
3.9
1.4
ug/L
04/19/18 20:23
1
4-Nitroaniline
<1.3
7.7
3.9
1.3
ug/L
04/19/18 20:23
1
Nitrobenzene
<0.35
0.77
0.39
0.35
ug/L
04/19/18 20:23
1
5-Nitro-o-toluidine
<2.4
7.7
3.9
2.4
ug/L
04/19/18 20:23
1
TestAmerica Chicago
Page 120 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-71)(i)
Lab Sample ID: 500-143858-19
Date Collected: 04/11/18 09:30
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<1.9
7.7
3.9
1.9
ug/L
04/19/18 20:23
1
4-Nitrophenol
<5.7
15
7.7
5.7
ug/L
04/19/18 20:23
1
N-Nitrosodiethylamine
<6.6
15
7.7
6.6
ug/L
04/19/18 20:23
1
N-Nitrosodimethylamine
<3.7
7.7
3.9
3.7
ug/L
04/19/18 20:23
1
N-Nitrosodi-n-butylamine
<3.2
7.7
3.9
3.2
ug/L
04/19/18 20:23
1
N-Nitrosodi-n-propylamine
<0.12
0.39
0.19
0.12
ug/L
04/19/18 20:23
1
N-Nitrosodiphenylamine
<0.29
1.5
0.77
0.29
ug/L
04/19/18 20:23
1
N-Nitrosomethylethylamine
<5.8
15
7.7
5.8
ug/L
04/19/18 20:23
1
N-Nitrosopiperidine
<2.7
7.7
3.9
2.7
ug/L
04/19/18 20:23
1
N-Nitrosopyrrolidine
<2.6
7.7
3.9
2.6
ug/L
04/19/18 20:23
1
o,o',o"-Triethylphosphorothioate
<4.3
15
7.7
4.3
ug/L
04/19/18 20:23
1
o-Toluidine
<6.1
31
15
6.1
ug/L
04/19/18 20:23
1
2,2'-oxybis[l-chloropropane]
<0.29
1.5
0.77
0.29
ug/L
04/19/18 20:23
1
p-Dimethylamino azobenzene
<2.3
7.7
3.9
2.3
ug/L
04/19/18 20:23
1
Pentachlorobenzene
<2.2
7.7
3.9
2.2
ug/L
04/19/18 20:23
1
Pentachloronitrobenzene
<2.7
7.7
3.9
2.7
ug/L
04/19/18 20:23
1
Phenacetin
<1.7
7.7
3.9
1.7
ug/L
04/19/18 20:23
1
Phenanthrene
<0.23
0.77
0.39
0.23
ug/L
04/19/18 20:23
1
Phenol
<0.52
3.9
1.9
0.52
ug/L
04/19/18 20:23
1
Phorate
<1.7
7.7
3.9
1.7
ug/L
04/19/18 20:23
1
p-Phenylene diamine
<13
62
31
13
ug/L
04/19/18 20:23
1
Pronamide
<1.7
7.7
7.7
1.7
ug/L
04/19/18 20:23
1
Pyrene
<0.33
0.77
0.39
0.33
ug/L
04/19/18 20:23
1
Safrole
<3.1
7.7
3.9
3.1
ug/L
04/19/18 20:23
1
sym-Trinitrobenzene
<1.4
7.7
3.9
1.4
ug/L
04/19/18 20:23
1
2,3,7,8-TCDD (Screen)
<7.7
7.7
7.7
7.7
ug/L
04/19/18 20:23
1
1,2,4,5-Tetrachlorobenzene
<0.44
3.9
1.9
0.44
ug/L
04/19/18 20:23
1
2,3,4,6-Tetrachlorophenol
<0.58
3.9
1.9
0.58
ug/L
04/19/18 20:23
1
Thionazin
<2.0
7.7
3.9
2.0
ug/L
04/19/18 20:23
1
2,4,5-Trichlorophenol
<2.0
7.7
3.9
2.0
ug/L
04/19/18 20:23
1
2,4,6-Trichlorophenol
<0.55
3.9
1.9
0.55
ug/L
04/19/18 20:23
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
79
34 - 110
04116118 16:56
04119118 20:23
1
2-Fluorophenol
54
27- 110
04116118 16:56
04119118 20:23
1
Nitrobenzene-d5
70
36 - 120
04116118 16:56
04119118 20:23
1
Phenol-d5
37
20 - 100
04116118 16:56
04119118 20:23
1
Terphenyl-d14
104
40- 145
04116118 16:56
04119118 20:23
1
2,4,6-Tribromophenol
90
40- 145
04116118 16:56
04119118 20:23
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
alpha-BHC
<0.012
beta-BHC
<0.048
delta-BHC
<0.048
gamma-BHC (Lindane)
<0.026
Heptachlor
<0.063
Aldrin
<0.025
Heptachlor epoxide
<0.065
Endosulfan 1
<0.019
RL
LOD
MDL
Unit
D Analyzed
0.19
0.094
0.012
ug/L
04/20/1818:17
0.19
0.094
0.048
ug/L
04/20/1818:17
0.19
0.094
0.048
ug/L
04/20/1818:17
0.19
0.094
0.026
ug/L
04/20/1818:17
0.19
0.094
0.063
ug/L
04/20/1818:17
0.19
0.094
0.025
ug/L
04/20/1818:17
0.19
0.094
0.065
ug/L
04/20/1818:17
0.19
0.094
0.019
ug/L
04/20/1818:17
Dil Fac
Page 121 of 258
TestAmerica Chicago
7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-71)(i)
Lab Sample ID: 500-143858-19
Date Collected: 04/11/18 09:30
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.060
0.19
0.094
0.060
ug/L
04/20/18 18:17
5
4,4'-DDE
<0.018
0.19
0.094
0.018
ug/L
04/20/18 18:17
5
Endrin
<0.067
0.19
0.094
0.067
ug/L
04/20/18 18:17
5
Endosulfan II
<0.013
0.19
0.094
0.013
ug/L
04/20/18 18:17
5
4,4'-DDD
<0.062
0.19
0.094
0.062
ug/L
04/20/18 18:17
5
Endosulfan sulfate
<0.055
0.19
0.094
0.055
ug/L
04/20/18 18:17
5
4,4'-DDT
<0.015
0.19
0.094
0.015
ug/L
04/20/18 18:17
5
Methoxychlor
<0.11
0.38
0.19
0.11
ug/L
04/20/18 18:17
5
Toxaphene
<0.94
1.9
0.94
0.94
ug/L
04/20/18 18:17
5
Endrin aldehyde
<0.038
0.19
0.094
0.038
ug/L
04/20/18 18:17
5
Chlordane (technical)
<0.19
0.38
0.19
0.19
ug/L
04/20/18 18:17
5
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
54
30 - 130
04117118 07:38
04120118 18:17
5
Tetrachloro-m-xylene
91
30 - 120
04117118 07:38
04120118 18:17
5
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.063
0.38
0.19
0.063
ug/L
04/17/18 23:04
1
PCB-1221
<0.19
0.38
0.19
0.19
ug/L
04/17/18 23:04
1
PCB-1232
<0.19
0.38
0.19
0.19
ug/L
04/17/18 23:04
1
PCB-1242
<0.19
0.38
0.19
0.19
ug/L
04/17/18 23:04
1
PCB-1248
<0.19
0.38
0.19
0.19
ug/L
04/17/18 23:04
1
PCB-1254
<0.19
0.38
0.19
0.19
ug/L
04/17/18 23:04
1
PCB-1260
<0.066
0.38
0.19
0.066
ug/L
04/17/18 23:04
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
70
30 - 120
04117118 07:38
04117118 23:04
1
DCB Decachlorobiphenyl
80
30 - 140
04117118 07:38
04117118 23:04
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.45
0.96
0.48
0.45
ug/L
04/18/18 06:15
1
Dinoseb
<0.16
1.9
0.96
0.16
ug/L
04/18/18 06:15
1
Pentachlorophenol
<0.086
0.48
0.096
0.086
ug/L
04/18/18 06:15
1
Silvex (2,4,5-TP)
<0.28
0.96
0.48
0.28
ug/L
04/18/18 06:15
1
2,4,5-T
<0.42
0.96
0.48
0.42
ug/L
04/18/18 06:15
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
88
25 - 130
04117118 09:02
04118118 06:15
1
Method: 6020B - Metals (ICP/MS) - Total Recoverable
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 04:09
1
Arsenic
0.76 J
1.0
0.50
0.23
ug/L
04/21/18 04:09
1
Barium
260
2.5
1.3
0.73
ug/L
04/21/18 04:09
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 04:09
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 04:09
1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 04:09
1
Cobalt
2.3
1.0
0.50
0.40
ug/L
04/21/18 04:09
1
Copper
1.7 J B
2.0
1.0
0.50
ug/L
04/21/18 04:09
1
TestAmerica Chicago
Page 122 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-71)(i)
Lab Sample
ID: 500-143858-19
Date Collected: 04/11/18 09:30
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 6020B - Metals (ICP/MS) -
Total Recoverable (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Iron
640
100
50
47
ug/L
04/21/18 04:09
1
Lead
0.49 J
0.50
0.25
0.19
ug/L
04/21/18 04:09
1
Manganese
1200
2.5
1.3
0.79
ug/L
04/21/18 04:09
1
Nickel
13
2.0
1.0
0.63
ug/L
04/21/18 04:09
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 04:09
1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 04:09
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 04:09
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 04:09
1
Vanadium
<2.2
5.0
2.5
2.2
ug/L
04/21/18 04:09
1
Zinc
12 B
10
20
6.9
ug/L
04/21/18 04:09
1
Method: 7470A - Mercury (CVAA)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/18/1811:20
1
General Chemistry
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/25/18 09:58
1
Chloride
97000
5000
4300
4300
ug/L
04/27/18 21:57
25
Sulfate
130000
5000
2500
2400
ug/L
04/26/18 22:10
25
Alkalinity
670000
5000
5000
3700
ug/L
04/23/1816:51
1
Total Dissolved Solids
1100000
10000
10000
4300
ug/L
04/17/18 23:07
1
TestAmerica Chicago
Page 123 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-5D(i) Lab Sample ID: 500-143858-20
Date Collected: 04/11/18 11:10 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/24/18 17:26
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/24/18 17:26
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/24/18 17:26
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/24/18 17:26
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 17:26
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 17:26
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/24/18 17:26
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 17:26
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/24/18 17:26
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/24/18 17:26
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 17:26
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/24/18 17:26
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 17:26
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 17:26
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/24/18 17:26
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/24/18 17:26
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 17:26
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/24/18 17:26
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/24/18 17:26
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/24/18 17:26
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/24/18 17:26
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/24/18 17:26
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/24/18 17:26
1
Acetone
20 cn
5.0
2.5
1.7
ug/L
04/24/18 17:26
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/24/18 17:26
1
Acrolein
<23
100
50
23
ug/L
04/24/18 17:26
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/24/18 17:26
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/24/18 17:26
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 17:26
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/24/18 17:26
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/24/18 17:26
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/24/18 17:26
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/24/18 17:26
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/24/18 17:26
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 17:26
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/24/18 17:26
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/24/18 17:26
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/24/18 17:26
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/24/18 17:26
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/24/18 17:26
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/24/18 17:26
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/24/18 17:26
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/24/18 17:26
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/24/18 17:26
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/24/18 17:26
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/24/18 17:26
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/24/18 17:26
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/24/18 17:26
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/24/18 17:26
1
TestAmerica Chicago
Page 124 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-51)(i)
Lab Sample ID: 500-143858-20
Date Collected: 04/11/18 11:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic
Compounds (GC/MS)
(Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/24/18 17:26
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/24/18 17:26
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/24/18 17:26
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 17:26
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/24/18 17:26
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/24/18 17:26
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/24/18 17:26
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/24/18 17:26
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 17:26
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/24/18 17:26
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/24/18 17:26
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 17:26
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/24/18 17:26
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/24/18 17:26
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/24/18 17:26
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
98
75- 126
04124118 17:26
1
4-Bromofluorobenzene (Surr)
108
72 - 124
04124118 17:26
1
Dibromofluoromethane
89
75 - 120
04124118 17:26
1
Toluene-d8 (Surr)
93
75 - 120
04124118 17:26
1
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Acenaphthene
<0.23
0.75
0.38
0.23
ug/L
04/20/18 18:14
1
Acenaphthylene
<0.20
0.75
0.38
0.20
ug/L
04/20/18 18:14
1
Acetophenone
<0.50
3.8
1.9
0.50
ug/L
04/20/18 18:14
1
2-Acetylaminofluorene
<1.6
7.5
3.8
1.6
ug/L
04/20/18 18:14
1
4-Aminobiphenyl
<2.8
7.5
3.8
2.8
ug/L
04/20/18 18:14
1
Anthracene
<0.25
0.75
0.38
0.25
ug/L
04/20/18 18:14
1
Benzo[a]anthracene
<0.043
0.15
0.075
0.043
ug/L
04/20/18 18:14
1
Benzo[a]pyrene
<0.075
0.15
0.075
0.075
ug/L
04/20/18 18:14
1
Benzo[b]fluoranthene
<0.061
0.15
0.075
0.061
ug/L
04/20/18 18:14
1
Benzo[g,h,i]perylene
<0.28
0.75
0.38
0.28
ug/L
04/20/18 18:14
1
Benzo[k]fluoranthene
<0.048
0.15
0.075
0.048
ug/L
04/20/18 18:14
1
Benzyl alcohol
<4.5
15
7.5
4.5
ug/L
04/20/18 18:14
1
Bis(2-chloroethoxy)methane
<0.21
1.5
0.75
0.21
ug/L
04/20/18 18:14
1
Bis(2-chloroethyl)ether
<0.22
1.5
0.75
0.22
ug/L
04/20/18 18:14
1
Bis(2-ethylhexyl) phthalate
<1.3
7.5
3.8
1.3
ug/L
04/20/18 18:14
1
4-Bromophenyl phenyl ether
<0.41
3.8
1.9
0.41
ug/L
04/20/18 18:14
1
Butyl benzyl phthalate
1.1 J
1.5
0.75
0.36
ug/L
04/20/18 18:14
1
4-Chloroaniline
<1.5
7.5
3.8
1.5
ug/L
04/20/18 18:14
1
Chlorobenzilate
<2.6
7.5
3.8
2.6
ug/L
04/20/18 18:14
1
4-Chloro-3-methylphenol
<1.7
7.5
3.8
1.7
ug/L
04/20/18 18:14
1
2-Chloronaphthalene
<0.18
1.5
0.75
0.18
ug/L
04/20/18 18:14
1
2-Chlorophenol
<0.42
3.8
1.9
0.42
ug/L
04/20/18 18:14
1
4-Chlorophenyl phenyl ether
<0.48
3.8
1.9
0.48
ug/L
04/20/18 18:14
1
Chrysene
<0.051
0.15
0.075
0.051
ug/L
04/20/18 18:14
1
Diallate
<4.2
7.5
4.7
4.2
ug/L
04/20/18 18:14
1
Dibenz(a,h)anthracene
<0.038
0.23
0.11
0.038
ug/L
04/20/18 18:14
1
TestAmerica Chicago
Page 125 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-51)(i) Lab Sample ID: 500-143858-20
Date Collected: 04/11/18 11:10 Matrix: Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.20
1.5
0.75
0.20
ug/L
04/20/18 18:14
1
3,3'-Dichlorobenzidine
<1.3
3.8
1.9
1.3
ug/L
04/20/18 18:14
1
2,4-Dichlorophenol
<2.0
7.5
3.8
2.0
ug/L
04/20/18 18:14
1
2,6-Dichlorophenol
<2.6
7.5
3.8
2.6
ug/L
04/20/18 18:14
1
Diethyl phthalate
<0.27
3.8
1.5
0.27
ug/L
04/20/18 18:14
1
Dimethoate
<1.4
7.5
3.8
1.4
ug/L
04/20/18 18:14
1
7,12-Dimethylbenz(a)anthracene
<2.3
30
15
2.3
ug/L
04/20/18 18:14
1
3,3'-Dimethylbenzidine
<13
30
15
13
ug/L
04/20/18 18:14
1
2,4-Dimethylphenol
<1.4
7.5
3.8
1.4
ug/L
04/20/18 18:14
1
Dimethyl phthalate
<0.24
3.8
1.5
0.24
ug/L
04/20/18 18:14
1
Di-n-butyl phthalate
<0.55
3.8
1.9
0.55
ug/L
04/20/18 18:14
1
4,6-Dinitro-2-methylphenol
<4.4
15
7.5
4.4
ug/L
04/20/18 18:14
1
2,4-Dinitrophenol
<6.5
15
7.5
6.5
ug/L
04/20/18 18:14
1
2,4-Dinitrotoluene
<0.18
0.75
0.38
0.18
ug/L
04/20/18 18:14
1
2,6-Dinitrotoluene
<0.056
0.75
0.38
0.056
ug/L
04/20/18 18:14
1
Di-n-octyl phthalate
<0.79
7.5
3.8
0.79
ug/L
04/20/18 18:14
1
Diphenylamine
<1.9
7.5
3.8
1.9
ug/L
04/20/18 18:14
1
Disulfoton
<1.4
7.5
3.8
1.4
ug/L
04/20/18 18:14
1
Ethyl methanesulfonate
<2.9
15
7.5
2.9
ug/L
04/20/18 18:14
1
Ethyl Parathion
<1.6
7.5
3.8
1.6
ug/L
04/20/18 18:14
1
Famphur
<23
30
24
23
ug/L
04/20/18 18:14
1
Fluoranthene
<0.34
0.75
0.38
0.34
ug/L
04/20/18 18:14
1
Fluorene
<0.18
0.75
0.38
0.18
ug/L
04/20/18 18:14
1
Hexachlorobenzene
<0.060
0.38
0.19
0.060
ug/L
04/20/18 18:14
1
Hexachlorocyclopentadiene
<4.8
15
7.5
4.8
ug/L
04/20/18 18:14
1
Hexachloroethane
<0.45
3.8
1.9
0.45
ug/L
04/20/18 18:14
1
Hexachloropropene
<3.5
15
7.5
3.5
ug/L
04/20/18 18:14
1
Indeno[1,2,3-cd]pyrene
<0.056
0.15
0.075
0.056
ug/L
04/20/18 18:14
1
Isodrin
<5.2
15
7.5
5.2
ug/L
04/20/18 18:14
1
Isophorone
<0.28
1.5
0.75
0.28
ug/L
04/20/18 18:14
1
Isosafrole
<2.9
7.5
3.8
2.9
ug/L
04/20/18 18:14
1
Kepone
<1.2
7.5
3.8
1.2
ug/L
04/20/18 18:14
1
m-Dinitrobenzene
<1.0
3.8
1.9
1.0
ug/L
04/20/18 18:14
1
Methapyrilene
<7.6
30
15
7.6
ug/L
04/20/18 18:14
1
3-Methylcholanthrene
<1.7
7.5
3.8
1.7
ug/L
04/20/18 18:14
1
Methyl methanesulfonate
<4.5
30
15
4.5
ug/L
04/20/18 18:14
1
2-Methylnaphthalene
<0.049
1.5
0.75
0.049
ug/L
04/20/18 18:14
1
Methyl parathion
<1.8
7.5
3.8
1.8
ug/L
04/20/18 18:14
1
2-Methylphenol
<0.23
1.5
0.75
0.23
ug/L
04/20/18 18:14
1
3 & 4 Methylphenol
<0.34
1.5
0.75
0.34
ug/L
04/20/18 18:14
1
Naphthalene
<0.23
0.75
0.38
0.23
ug/L
04/20/18 18:14
1
1,4-Naphthoquinone
<29
30
30
29
ug/L
04/20/18 18:14
1
1-Naphthylamine
<4.5
15
7.5
4.5
ug/L
04/20/18 18:14
1
2-Naphthylamine
<6.9
15
7.5
6.9
ug/L
04/20/18 18:14
1
2-Nitroaniline
<0.97
3.8
1.9
0.97
ug/L
04/20/18 18:14
1
3-Nitroaniline
<1.3
7.5
3.8
1.3
ug/L
04/20/18 18:14
1
4-Nitroaniline
<1.3
7.5
3.8
1.3
ug/L
04/20/18 18:14
1
Nitrobenzene
<0.34
0.75
0.38
0.34
ug/L
04/20/18 18:14
1
5-Nitro-o-toluidine
<2.3
7.5
3.8
2.3
ug/L
04/20/18 18:14
1
TestAmerica Chicago
Page 126 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-51)(i)
Lab Sample ID: 500-143858-20
Date Collected: 04/11/18 11:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<1.9
7.5
3.8
1.9
ug/L
04/20/18 18:14
1
4-Nitrophenol
<5.6
15
7.5
5.6
ug/L
04/20/18 18:14
1
N-Nitrosodiethylamine
<6.5
15
7.5
6.5
ug/L
04/20/18 18:14
1
N-Nitrosodimethylamine
<3.6
7.5
3.8
3.6
ug/L
04/20/18 18:14
1
N-Nitrosodi-n-butylamine
<3.2
7.5
3.8
3.2
ug/L
04/20/18 18:14
1
N-Nitrosodi-n-propylamine
<0.12
0.38
0.19
0.12
ug/L
04/20/18 18:14
1
N-Nitrosodiphenylamine
<0.28
1.5
0.75
0.28
ug/L
04/20/18 18:14
1
N-Nitrosomethylethylamine
<5.6
15
7.5
5.6
ug/L
04/20/18 18:14
1
N-Nitrosopiperidine
<2.6
7.5
3.8
2.6
ug/L
04/20/18 18:14
1
N-Nitrosopyrrolidine
<2.5
7.5
3.8
2.5
ug/L
04/20/18 18:14
1
o,o',o"-Triethylphosphorothioate
<4.2
15
7.5
4.2
ug/L
04/20/18 18:14
1
o-Toluidine
<6.0
30
15
6.0
ug/L
04/20/18 18:14
1
2,2'-oxybis[l-chloropropane]
<0.29
1.5
0.75
0.29
ug/L
04/20/18 18:14
1
p-Dimethylamino azobenzene
<2.3
7.5
3.8
2.3
ug/L
04/20/18 18:14
1
Pentachlorobenzene
<2.1
7.5
3.8
2.1
ug/L
04/20/18 18:14
1
Pentachloronitrobenzene
<2.7
7.5
3.8
2.7
ug/L
04/20/18 18:14
1
Phenacetin
<1.7
7.5
3.8
1.7
ug/L
04/20/18 18:14
1
Phenanthrene
<0.23
0.75
0.38
0.23
ug/L
04/20/18 18:14
1
Phenol
4.6
3.8
1.9
0.51
ug/L
04/20/18 18:14
1
Phorate
<1.6
7.5
3.8
1.6
ug/L
04/20/18 18:14
1
p-Phenylene diamine
<12
60
30
12
ug/L
04/20/18 18:14
1
Pronamide
<1.6
7.5
7.5
1.6
ug/L
04/20/18 18:14
1
Pyrene
<0.32
0.75
0.38
0.32
ug/L
04/20/18 18:14
1
Safrole
<3.0
7.5
3.8
3.0
ug/L
04/20/18 18:14
1
sym-Trinitrobenzene
<1.4
7.5
3.8
1.4
ug/L
04/20/18 18:14
1
2,3,7,8-TCDD (Screen)
<7.5
7.5
7.5
7.5
ug/L
04/20/18 18:14
1
1,2,4,5-Tetrachlorobenzene
<0.43
3.8
1.9
0.43
ug/L
04/20/18 18:14
1
2,3,4,6-Tetrachlorophenol
<0.56
3.8
1.9
0.56
ug/L
04/20/18 18:14
1
Thionazin
<1.9
7.5
3.8
1.9
ug/L
04/20/18 18:14
1
2,4,5-Trichlorophenol
<1.9
7.5
3.8
1.9
ug/L
04/20/18 18:14
1
2,4,6-Trichlorophenol
<0.54
3.8
1.9
0.54
ug/L
04/20/18 18:14
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
100
34 - 110
04116118 16:56
04120118 18:14
1
2-Fluorophenol
63
27- 110
04116118 16:56
04120118 18:14
1
Nitrobenzene-d5
94
36 - 120
04116118 16:56
04120118 18:14
1
Phenol-d5
49
20- 100
04116118 16:56
04120118 18:14
1
Terphenyl-d14
146 X
40- 145
04116118 16:56
04120118 18:14
1
2,4,6-Tribromophenol
99
40- 145
04116118 16:56
04120118 18:14
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
alpha-BHC
<0.0024
0.037
0.019
0.0024
ug/L
04/20/18 18:55
1
beta-BHC
<0.0094
0.037
0.019
0.0094
ug/L
04/20/18 18:55
1
delta-BHC
<0.0095
0.037
0.019
0.0095
ug/L
04/20/18 18:55
1
gamma-BHC (Lindane)
<0.0052
0.037
0.019
0.0052
ug/L
04/20/18 18:55
1
Heptachlor
<0.012
0.037
0.019
0.012
ug/L
04/20/18 18:55
1
Aldrin
<0.0049
0.037
0.019
0.0049
ug/L
04/20/18 18:55
1
Heptachlor epoxide
<0.013
0.037
0.019
0.013
ug/L
04/20/18 18:55
1
Endosulfan 1
<0.0038
0.037
0.019
0.0038
ug/L
04/20/18 18:55
1
TestAmerica Chicago
Page 127 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-51)(i)
Lab Sample ID: 500-143858-20
Date Collected: 04/11/18 11:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.012
0.037
0.019
0.012
ug/L
04/20/18 18:55
1
4,4'-DDE
<0.0035
0.037
0.019
0.0035
ug/L
04/20/18 18:55
1
Endrin
<0.013
0.037
0.019
0.013
ug/L
04/20/18 18:55
1
Endosulfan II
<0.0026
0.037
0.019
0.0026
ug/L
04/20/18 18:55
1
4,4'-DDD
<0.012
0.037
0.019
0.012
ug/L
04/20/18 18:55
1
Endosulfan sulfate
<0.011
0.037
0.019
0.011
ug/L
04/20/18 18:55
1
4,4'-DDT
<0.0030
0.037
0.019
0.0030
ug/L
04/20/18 18:55
1
Methoxychlor
<0.021
0.074
0.037
0.021
ug/L
04/20/18 18:55
1
Toxaphene
<0.19
0.37
0.19
0.19
ug/L
04/20/18 18:55
1
Endrin aldehyde
<0.0076
0.037
0.019
0.0076
ug/L
04/20/18 18:55
1
Chlordane (technical)
<0.037
0.074
0.037
0.037
ug/L
04/20/18 18:55
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
65
30 - 130
04117118 07:38
04120118 18:55
1
Tetrachloro-m-xylene
61
30 - 120
04117118 07:38
04120118 18:55
1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.062
0.37
0.19
0.062
ug/L
04/17/18 23:21
1
PCB-1221
<0.19
0.37
0.19
0.19
ug/L
04/17/18 23:21
1
PCB-1232
<0.19
0.37
0.19
0.19
ug/L
04/17/18 23:21
1
PCB-1242
<0.19
0.37
0.19
0.19
ug/L
04/17/18 23:21
1
PCB-1248
<0.19
0.37
0.19
0.19
ug/L
04/17/18 23:21
1
PCB-1254
<0.19
0.37
0.19
0.19
ug/L
04/17/18 23:21
1
PCB-1260
<0.065
0.37
0.19
0.065
ug/L
04/17/18 23:21
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
70
30 - 120
04117118 07:38
04117118 23:21
1
DCB Decachlorobiphenyl
82
30 - 140
04117118 07:38
04117118 23:21
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.45
0.96
0.48
0.45
ug/L
04/19/18 03:17
1
Dinoseb
<0.16
1.9
0.96
0.16
ug/L
04/19/18 03:17
1
Pentachlorophenol
<0.086
0.48
0.096
0.086
ug/L
04/19/18 03:17
1
Silvex (2,4,5-TP)
<0.28
0.96
0.48
0.28
ug/L
04/19/18 03:17
1
2,4,5-T
<0.42
0.96
0.48
0.42
ug/L
04/19/18 03:17
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
40
25 - 130
04118118 10:05
04119118 03:17
1
Method: 6020B - Metals (ICP/MS) - Total Recoverable
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 04:13
1
Arsenic
0.50 J
1.0
0.50
0.23
ug/L
04/21/18 04:13
1
Barium
6.7
2.5
1.3
0.73
ug/L
04/21/18 04:13
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 04:13
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 04:13
1
Chromium
2.5 J B
5.0
2.5
1.1
ug/L
04/21/18 04:13
1
Cobalt
0.53 J
1.0
0.50
0.40
ug/L
04/21/18 04:13
1
Copper
4.9 B
2.0
1.0
0.50
ug/L
04/21/18 04:13
1
TestAmerica Chicago
Page 128 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill
- Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-51)(i)
Lab Sample
ID: 500-143858-20
Date Collected: 04/11/18 11:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Iron
66 J
100
50
47
ug/L
04/21/18 04:13
1
Lead
<0.19
0.50
0.25
0.19
ug/L
04/21/18 04:13
1
Manganese
6.2
2.5
1.3
0.79
ug/L
04/21/18 04:13
1
Nickel
1.5 J
2.0
1.0
0.63
ug/L
04/21/18 04:13
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 04:13
1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 04:13
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 04:13
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 04:13
1
Vanadium
<2.2
5.0
2.5
2.2
ug/L
04/21/18 04:13
1
Zinc
<6.9
10
20
6.9
ug/L
04/21/18 04:13
1
Method: 7470A - Mercury (CVAA)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/18/1811:22
1
General Chemistry
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/25/18 09:57
1
Chloride
15000
1000
850
850
ug/L
04/27/18 22:09
5
Sulfate
15000
1000
500
480
ug/L
04/27/18 22:09
5
Alkalinity
330000
5000
5000
3700
ug/L
04/23/1817:00
1
Total Dissolved Solids
520000
10000
10000
4300
ug/L
04/17/18 23:09
1
TestAmerica Chicago
Page 129 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-7(i) Lab Sample ID: 500-143858-21
Date Collected: 04/11/18 10:10 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/25/18 11:54
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/25/18 11:54
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/25/18 11:54
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/25/18 11:54
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/25/18 11:54
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/25/18 11:54
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/25/18 11:54
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/25/18 11:54
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/25/18 11:54
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/25/18 11:54
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/25/18 11:54
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/25/18 11:54
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/25/18 11:54
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/25/18 11:54
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/25/18 11:54
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/25/18 11:54
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/25/18 11:54
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/25/18 11:54
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/25/18 11:54
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/25/18 11:54
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/25/18 11:54
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/25/18 11:54
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/25/18 11:54
1
Acetone
5.0 cn
5.0
2.5
1.7
ug/L
04/25/18 11:54
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/25/18 11:54
1
Acrolein
<23
100
50
23
ug/L
04/25/18 11:54
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/25/18 11:54
1
Benzene
1.4
0.50
0.25
0.15
ug/L
04/25/18 11:54
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/25/18 11:54
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/25/18 11:54
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/25/18 11:54
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/25/18 11:54
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/25/18 11:54
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/25/18 11:54
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/25/18 11:54
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/25/18 11:54
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/25/18 11:54
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/25/18 11:54
1
cis-1,2-Dichloroethene
0.64 J
1.0
0.50
0.41
ug/L
04/25/18 11:54
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/25/18 11:54
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/25/18 11:54
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/25/18 11:54
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/25/18 11:54
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/25/18 11:54
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/25/18 11:54
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/25/18 11:54
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/25/18 11:54
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/25/18 11:54
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/25/18 11:54
1
TestAmerica Chicago
Page 130 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-7(i)
Lab Sample
ID: 500-143858-21
Date Collected: 04/11/18 10:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/25/18 11:54
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/25/18 11:54
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/25/18 11:54
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/25/18 11:54
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/25/18 11:54
1
Tetrahydrofuran
21
10
5.0
1.9
ug/L
04/25/18 11:54
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/25/18 11:54
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/25/18 11:54
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/25/18 11:54
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/25/18 11:54
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/25/18 11:54
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/25/18 11:54
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/25/18 11:54
1
Vinyl chloride
0.88 J
1.0
0.50
0.20
ug/L
04/25/18 11:54
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/25/18 11:54
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 104 75- 126
4-Bromofluorobenzene (Surr) 101 72 - 124
Dibromofluoromethane 99 75 - 120
Toluene-d8 (Surr) 92 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04125118 11:54
04125118 11:54
04125118 11:54
04/25/18 11:54
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.23
0.75
0.38
0.23
ug/L
04/20/18 18:39
1
Acenaphthylene
<0.20
0.75
0.38
0.20
ug/L
04/20/18 18:39
1
Acetophenone
<0.50
3.8
1.9
0.50
ug/L
04/20/18 18:39
1
2-Acetylaminofluorene
<1.6
7.5
3.8
1.6
ug/L
04/20/18 18:39
1
4-Aminobiphenyl
<2.8
7.5
3.8
2.8
ug/L
04/20/18 18:39
1
Anthracene
0.46 J
0.75
0.38
0.25
ug/L
04/20/18 18:39
1
Benzo[a]anthracene
<0.043
0.15
0.075
0.043
ug/L
04/20/18 18:39
1
Benzo[a]pyrene
<0.074
0.15
0.075
0.074
ug/L
04/20/18 18:39
1
Benzo[b]fluoranthene
<0.061
0.15
0.075
0.061
ug/L
04/20/18 18:39
1
Benzo[g,h,i]perylene
<0.28
0.75
0.38
0.28
ug/L
04/20/18 18:39
1
Benzo[k]fluoranthene
<0.048
0.15
0.075
0.048
ug/L
04/20/18 18:39
1
Benzyl alcohol
<4.5
15
7.5
4.5
ug/L
04/20/18 18:39
1
Bis(2-chloroethoxy)methane
<0.21
1.5
0.75
0.21
ug/L
04/20/18 18:39
1
Bis(2-chloroethyl)ether
<0.22
1.5
0.75
0.22
ug/L
04/20/18 18:39
1
Bis(2-ethylhexyl) phthalate
<1.3
7.5
3.8
1.3
ug/L
04/20/18 18:39
1
4-Bromophenyl phenyl ether
<0.41
3.8
1.9
0.41
ug/L
04/20/18 18:39
1
Butyl benzyl phthalate
<0.36
1.5
0.75
0.36
ug/L
04/20/18 18:39
1
4-Chloroaniline
<1.5
7.5
3.8
1.5
ug/L
04/20/18 18:39
1
Chlorobenzilate
<2.6
7.5
3.8
2.6
ug/L
04/20/18 18:39
1
4-Chloro-3-methylphenol
<1.7
7.5
3.8
1.7
ug/L
04/20/18 18:39
1
2-Chloronaphthalene
<0.18
1.5
0.75
0.18
ug/L
04/20/18 18:39
1
2-Chlorophenol
<0.42
3.8
1.9
0.42
ug/L
04/20/18 18:39
1
4-Chlorophenyl phenyl ether
<0.48
3.8
1.9
0.48
ug/L
04/20/18 18:39
1
Chrysene
<0.051
0.15
0.075
0.051
ug/L
04/20/18 18:39
1
Diallate
<4.2
7.5
4.7
4.2
ug/L
04/20/18 18:39
1
Dibenz(a,h)anthracene
<0.038
0.23
0.11
0.038
ug/L
04/20/18 18:39
1
TestAmerica Chicago
Page 131 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-7(i) Lab Sample ID: 500-143858-21
Date Collected: 04/11/18 10:10 Matrix: Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.20
1.5
0.75
0.20
ug/L
04/20/18 18:39
1
3,3'-Dichlorobenzidine
<1.3
3.8
1.9
1.3
ug/L
04/20/18 18:39
1
2,4-Dichlorophenol
<2.0
7.5
3.8
2.0
ug/L
04/20/18 18:39
1
2,6-Dichlorophenol
<2.6
7.5
3.8
2.6
ug/L
04/20/18 18:39
1
Diethyl phthalate
<0.27
3.8
1.5
0.27
ug/L
04/20/18 18:39
1
Dimethoate
<1.4
7.5
3.8
1.4
ug/L
04/20/18 18:39
1
7,12-Dimethylbenz(a)anthracene
<2.3
30
15
2.3
ug/L
04/20/18 18:39
1
3,3'-Dimethylbenzidine
<13
30
15
13
ug/L
04/20/18 18:39
1
2,4-Dimethylphenol
<1.4
7.5
3.8
1.4
ug/L
04/20/18 18:39
1
Dimethyl phthalate
<0.24
3.8
1.5
0.24
ug/L
04/20/18 18:39
1
Di-n-butyl phthalate
1.4 J
3.8
1.9
0.55
ug/L
04/20/18 18:39
1
4,6-Dinitro-2-methylphenol
<4.4
15
7.5
4.4
ug/L
04/20/18 18:39
1
2,4-Dinitrophenol
<6.5
15
7.5
6.5
ug/L
04/20/18 18:39
1
2,4-Dinitrotoluene
<0.18
0.75
0.38
0.18
ug/L
04/20/18 18:39
1
2,6-Dinitrotoluene
<0.056
0.75
0.38
0.056
ug/L
04/20/18 18:39
1
Di-n-octyl phthalate
<0.79
7.5
3.8
0.79
ug/L
04/20/18 18:39
1
Diphenylamine
<1.9
7.5
3.8
1.9
ug/L
04/20/18 18:39
1
Disulfoton
<1.4
7.5
3.8
1.4
ug/L
04/20/18 18:39
1
Ethyl methanesulfonate
<2.9
15
7.5
2.9
ug/L
04/20/18 18:39
1
Ethyl Parathion
<1.6
7.5
3.8
1.6
ug/L
04/20/18 18:39
1
Famphur
<23
30
24
23
ug/L
04/20/18 18:39
1
Fluoranthene
<0.34
0.75
0.38
0.34
ug/L
04/20/18 18:39
1
Fluorene
<0.18
0.75
0.38
0.18
ug/L
04/20/18 18:39
1
Hexachlorobenzene
<0.060
0.38
0.19
0.060
ug/L
04/20/18 18:39
1
Hexachlorocyclopentadiene
<4.8
15
7.5
4.8
ug/L
04/20/18 18:39
1
Hexachloroethane
<0.45
3.8
1.9
0.45
ug/L
04/20/18 18:39
1
Hexachloropropene
<3.5
15
7.5
3.5
ug/L
04/20/18 18:39
1
Indeno[1,2,3-cd]pyrene
<0.056
0.15
0.075
0.056
ug/L
04/20/18 18:39
1
Isodrin
<5.2
15
7.5
5.2
ug/L
04/20/18 18:39
1
Isophorone
<0.28
1.5
0.75
0.28
ug/L
04/20/18 18:39
1
Isosafrole
<2.9
7.5
3.8
2.9
ug/L
04/20/18 18:39
1
Kepone
<1.2
7.5
3.8
1.2
ug/L
04/20/18 18:39
1
m-Dinitrobenzene
<1.0
3.8
1.9
1.0
ug/L
04/20/18 18:39
1
Methapyrilene
<7.6
30
15
7.6
ug/L
04/20/18 18:39
1
3-Methylcholanthrene
<1.7
7.5
3.8
1.7
ug/L
04/20/18 18:39
1
Methyl methanesulfonate
<4.5
30
15
4.5
ug/L
04/20/18 18:39
1
2-Methylnaphthalene
<0.049
1.5
0.75
0.049
ug/L
04/20/18 18:39
1
Methyl parathion
<1.8
7.5
3.8
1.8
ug/L
04/20/18 18:39
1
2-Methylphenol
<0.23
1.5
0.75
0.23
ug/L
04/20/18 18:39
1
3 & 4 Methylphenol
<0.34
1.5
0.75
0.34
ug/L
04/20/18 18:39
1
Naphthalene
<0.23
0.75
0.38
0.23
ug/L
04/20/18 18:39
1
1,4-Naphthoquinone
<29
30
30
29
ug/L
04/20/18 18:39
1
1-Naphthylamine
<4.5
15
7.5
4.5
ug/L
04/20/18 18:39
1
2-Naphthylamine
<6.9
15
7.5
6.9
ug/L
04/20/18 18:39
1
2-Nitroaniline
<0.97
3.8
1.9
0.97
ug/L
04/20/18 18:39
1
3-Nitroaniline
<1.3
7.5
3.8
1.3
ug/L
04/20/18 18:39
1
4-Nitroaniline
<1.3
7.5
3.8
1.3
ug/L
04/20/18 18:39
1
Nitrobenzene
<0.34
0.75
0.38
0.34
ug/L
04/20/18 18:39
1
5-Nitro-o-toluidine
<2.3
7.5
3.8
2.3
ug/L
04/20/18 18:39
1
TestAmerica Chicago
Page 132 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-7(i)
Lab Sample ID: 500-143858-21
Date Collected: 04/11/18 10:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<1.9
7.5
3.8
1.9
ug/L
04/20/18 18:39
1
4-Nitrophenol
<5.6
15
7.5
5.6
ug/L
04/20/18 18:39
1
N-Nitrosodiethylamine
<6.5
15
7.5
6.5
ug/L
04/20/18 18:39
1
N-Nitrosodimethylamine
<3.6
7.5
3.8
3.6
ug/L
04/20/18 18:39
1
N-Nitrosodi-n-butylamine
<3.2
7.5
3.8
3.2
ug/L
04/20/18 18:39
1
N-Nitrosodi-n-propylamine
<0.12
0.38
0.19
0.12
ug/L
04/20/18 18:39
1
N-Nitrosodiphenylamine
<0.28
1.5
0.75
0.28
ug/L
04/20/18 18:39
1
N-Nitrosomethylethylamine
<5.6
15
7.5
5.6
ug/L
04/20/18 18:39
1
N-Nitrosopiperidine
<2.6
7.5
3.8
2.6
ug/L
04/20/18 18:39
1
N-Nitrosopyrrolidine
<2.5
7.5
3.8
2.5
ug/L
04/20/18 18:39
1
o,o',o"-Triethylphosphorothioate
<4.2
15
7.5
4.2
ug/L
04/20/18 18:39
1
o-Toluidine
<6.0
30
15
6.0
ug/L
04/20/18 18:39
1
2,2'-oxybis[l-chloropropane]
<0.29
1.5
0.75
0.29
ug/L
04/20/18 18:39
1
p-Dimethylamino azobenzene
<2.3
7.5
3.8
2.3
ug/L
04/20/18 18:39
1
Pentachlorobenzene
<2.1
7.5
3.8
2.1
ug/L
04/20/18 18:39
1
Pentachloronitrobenzene
<2.7
7.5
3.8
2.7
ug/L
04/20/18 18:39
1
Phenacetin
<1.7
7.5
3.8
1.7
ug/L
04/20/18 18:39
1
Phenanthrene
<0.23
0.75
0.38
0.23
ug/L
04/20/18 18:39
1
Phenol
<0.51
3.8
1.9
0.51
ug/L
04/20/18 18:39
1
Phorate
<1.6
7.5
3.8
1.6
ug/L
04/20/18 18:39
1
p-Phenylene diamine
<12
60
30
12
ug/L
04/20/18 18:39
1
Pronamide
<1.6
7.5
7.5
1.6
ug/L
04/20/18 18:39
1
Pyrene
<0.32
0.75
0.38
0.32
ug/L
04/20/18 18:39
1
Safrole
<3.0
7.5
3.8
3.0
ug/L
04/20/18 18:39
1
sym-Trinitrobenzene
<1.4
7.5
3.8
1.4
ug/L
04/20/18 18:39
1
2,3,7,8-TCDD (Screen)
<7.5
7.5
7.5
7.5
ug/L
04/20/18 18:39
1
1,2,4,5-Tetrachlorobenzene
<0.43
3.8
1.9
0.43
ug/L
04/20/18 18:39
1
2,3,4,6-Tetrachlorophenol
<0.56
3.8
1.9
0.56
ug/L
04/20/18 18:39
1
Thionazin
<1.9
7.5
3.8
1.9
ug/L
04/20/18 18:39
1
2,4,5-Trichlorophenol
<1.9
7.5
3.8
1.9
ug/L
04/20/18 18:39
1
2,4,6-Trichlorophenol
<0.54
3.8
1.9
0.54
ug/L
04/20/18 18:39
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
107
34 - 110
04116118 16:56
04120118 18:39
1
2-Fluorophenol
70
27- 110
04116118 16:56
04120118 18:39
1
Nitrobenzene-d5
99
36 - 120
04116118 16:56
04120118 18:39
1
Phenol-d5
48
20- 100
04116118 16:56
04120118 18:39
1
Terphenyl-d14
118
40- 145
04116118 16:56
04120118 18:39
1
2,4,6-Tribromophenol
103
40- 145
04116118 16:56
04120118 18:39
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
alpha-BHC
<0.013
beta-BHC
<0.050
delta-BHC
<0.050
gamma-BHC (Lindane)
<0.027
Heptachlor
<0.066
Aldrin
<0.026
Heptachlor epoxide
<0.067
Endosulfan 1
<0.020
RL
LOD
MDL
Unit
D Analyzed
0.19
0.097
0.013
ug/L
04/26/1813:09
0.19
0.097
0.050
ug/L
04/26/1813:09
0.19
0.097
0.050
ug/L
04/26/1813:09
0.19
0.097
0.027
ug/L
04/26/1813:09
0.19
0.097
0.066
ug/L
04/26/1813:09
0.19
0.097
0.026
ug/L
04/26/1813:09
0.19
0.097
0.067
ug/L
04/26/1813:09
0.19
0.097
0.020
ug/L
04/26/1813:09
Dil Fac
Page 133 of 258
TestAmerica Chicago
7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW-7(i)
Lab Sample ID: 500-143858-21
Date Collected: 04/11/18 10:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.063
0.19
0.097
0.063
ug/L
04/26/18 13:09
5
4,4'-DDE
<0.019
0.19
0.097
0.019
ug/L
04/26/18 13:09
5
Endrin
<0.069
0.19
0.097
0.069
ug/L
04/26/18 13:09
5
Endosulfan II
<0.014
0.19
0.097
0.014
ug/L
04/26/18 13:09
5
4,4'-DDD
<0.065
0.19
0.097
0.065
ug/L
04/26/18 13:09
5
Endosulfan sulfate
<0.057
0.19
0.097
0.057
ug/L
04/26/18 13:09
5
4,4'-DDT
<0.016
0.19
0.097
0.016
ug/L
04/26/18 13:09
5
Methoxychlor
<0.11
0.39
0.19
0.11
ug/L
04/26/18 13:09
5
Toxaphene
<0.97
1.9
0.97
0.97
ug/L
04/26/18 13:09
5
Endrin aldehyde
<0.040
0.19
0.097
0.040
ug/L
04/26/18 13:09
5
Chlordane (technical)
<0.19
0.39
0.19
0.19
ug/L
04/26/18 13:09
5
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
151 X
30 - 130
04117118 07:38
04126118 13:09
5
Tetrachloro-m-xylene
27 X
30 - 120
04117118 07:38
04126118 13:09
5
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.065
0.39
0.19
0.065
ug/L
04/17/18 23:37
1
PCB-1221
<0.19
0.39
0.19
0.19
ug/L
04/17/18 23:37
1
PCB-1232
<0.19
0.39
0.19
0.19
ug/L
04/17/18 23:37
1
PCB-1242
<0.19
0.39
0.19
0.19
ug/L
04/17/18 23:37
1
PCB-1248
<0.19
0.39
0.19
0.19
ug/L
04/17/18 23:37
1
PCB-1254
<0.19
0.39
0.19
0.19
ug/L
04/17/18 23:37
1
PCB-1260
<0.068
0.39
0.19
0.068
ug/L
04/17/18 23:37
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
71
30 - 120
04117118 07:38
04117118 23:37
1
DCB Decachlorobiphenyl
87
30 - 140
04117118 07:38
04117118 23:37
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.44
0.95
0.47
0.44
ug/L
04/19/18 03:42
1
Dinoseb
<0.16
1.9
0.95
0.16
ug/L
04/19/18 03:42
1
Pentachlorophenol
<0.085
0.47
0.095
0.085
ug/L
04/19/18 03:42
1
Silvex (2,4,5-TP)
<0.27
0.95
0.47
0.27
ug/L
04/19/18 03:42
1
2,4,5-T
<0.41
0.95
0.47
0.41
ug/L
04/19/18 03:42
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
82
25 - 130
04118118 10:05
04119118 03:42
1
Method: 6020B - Metals (ICP/MS)
- Total Recoverable
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 04:16
1
Arsenic
0.56 J
1.0
0.50
0.23
ug/L
04/21/18 04:16
1
Barium
190
2.5
1.3
0.73
ug/L
04/21/18 04:16
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 04:16
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 04:16
1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 04:16
1
Cobalt
3.7
1.0
0.50
0.40
ug/L
04/21/18 04:16
1
Copper
<0.50
2.0
1.0
0.50
ug/L
04/21/18 04:16
1
TestAmerica Chicago
Page 134 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW-7(i)
Lab Sample
ID: 500-143858-21
Date Collected: 04/11/18 10:10
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 6020B - Metals (ICP/MS) -
Total Recoverable (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Iron
410
100
50
47
ug/L
04/21/18 04:16
1
Lead
<0.19
0.50
0.25
0.19
ug/L
04/21/18 04:16
1
Manganese
350
2.5
1.3
0.79
ug/L
04/21/18 04:16
1
Nickel
3.6
2.0
1.0
0.63
ug/L
04/21/18 04:16
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 04:16
1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 04:16
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 04:16
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 04:16
1
Vanadium
<2.2
5.0
2.5
2.2
ug/L
04/21/18 04:16
1
Zinc
<6.9
10
20
6.9
ug/L
04/21/18 04:16
1
Method: 7470A - Mercury (CVAA)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/18/1811:23
1
General Chemistry
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/25/18 09:58
1
Chloride
81000
4000
3400
3400
ug/L
04/27/18 22:21
20
Sulfate
160000
4000
2000
1900
ug/L
04/26/18 22:35
20
Alkalinity
530000
5000
5000
3700
ug/L
04/23/1817:09
1
Total Dissolved Solids
1000000
10000
10000
4300
ug/L
04/17/18 23:12
1
TestAmerica Chicago
Page 135 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: Duplicate Lab Sample ID: 500-143858-22
Date Collected: 04/10/18 00:00 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/20/18 17:36
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/20/18 17:36
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/20/18 17:36
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/20/18 17:36
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/20/18 17:36
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 17:36
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/20/18 17:36
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/20/18 17:36
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/20/18 17:36
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/20/18 17:36
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/20/18 17:36
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/20/18 17:36
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/20/18 17:36
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 17:36
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/20/18 17:36
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/20/18 17:36
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/20/18 17:36
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/20/18 17:36
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/20/18 17:36
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/20/18 17:36
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/20/18 17:36
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/20/18 17:36
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/20/18 17:36
1
Acetone
10 cn
5.0
2.5
1.7
ug/L
04/20/18 17:36
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/20/18 17:36
1
Acrolein
<23
100
50
23
ug/L
04/20/18 17:36
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/20/18 17:36
1
Benzene
1.2
0.50
0.25
0.15
ug/L
04/20/18 17:36
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 17:36
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/20/18 17:36
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/20/18 17:36
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/20/18 17:36
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/20/18 17:36
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/20/18 17:36
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 17:36
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/20/18 17:36
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/20/18 17:36
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/20/18 17:36
1
cis-1,2-Dichloroethene
0.98 J
1.0
0.50
0.41
ug/L
04/20/18 17:36
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/20/18 17:36
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/20/18 17:36
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/20/18 17:36
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/20/18 17:36
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/20/18 17:36
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/20/18 17:36
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/20/18 17:36
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/20/18 17:36
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/20/18 17:36
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/20/18 17:36
1
TestAmerica Chicago
Page 136 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: Duplicate
Lab Sample ID: 500-143858-22
Date Collected: 04/10/18 00:00
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS)
(Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/20/18 17:36
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/20/18 17:36
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/20/18 17:36
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 17:36
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/20/18 17:36
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/20/18 17:36
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/20/18 17:36
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/20/18 17:36
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/20/18 17:36
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/20/18 17:36
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/20/18 17:36
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 17:36
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/20/18 17:36
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/20/18 17:36
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/20/18 17:36
1
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
108
75- 226
04120118 17:36
1
4-Bromofluorobenzene (Surr)
93
72 - 124
04120118 17:36
1
Dibromofluoromethane
96
75 - 120
04120118 17:36
1
Toluene-d8 (Surr)
95
75 - 120
04120118 17:36
1
TestAmerica Chicago
Page 137 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: Duplicate 1 Lab Sample ID: 500-143858-23
Date Collected: 04/11/18 00:00 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/24/18 17:01
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/24/18 17:01
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/24/18 17:01
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/24/18 17:01
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 17:01
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 17:01
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/24/18 17:01
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 17:01
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/24/18 17:01
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/24/18 17:01
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 17:01
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/24/18 17:01
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 17:01
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 17:01
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/24/18 17:01
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/24/18 17:01
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 17:01
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/24/18 17:01
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/24/18 17:01
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/24/18 17:01
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/24/18 17:01
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/24/18 17:01
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/24/18 17:01
1
Acetone
16 cn
5.0
2.5
1.7
ug/L
04/24/18 17:01
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/24/18 17:01
1
Acrolein
<23
100
50
23
ug/L
04/24/18 17:01
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/24/18 17:01
1
Benzene
0.67
0.50
0.25
0.15
ug/L
04/24/18 17:01
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 17:01
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/24/18 17:01
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/24/18 17:01
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/24/18 17:01
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/24/18 17:01
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/24/18 17:01
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 17:01
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/24/18 17:01
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/24/18 17:01
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/24/18 17:01
1
cis-1,2-Dichloroethene
1.8
1.0
0.50
0.41
ug/L
04/24/18 17:01
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/24/18 17:01
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/24/18 17:01
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/24/18 17:01
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/24/18 17:01
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/24/18 17:01
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/24/18 17:01
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/24/18 17:01
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/24/18 17:01
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/24/18 17:01
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/24/18 17:01
1
TestAmerica Chicago
Page 138 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: Duplicate 1
Lab Sample ID: 500-143858-23
Date Collected: 04/11/18 00:00
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS)
(Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/24/18 17:01
1
Methylene Chloride
5.0 cn
5.0
2.5
1.6
ug/L
04/24/18 17:01
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/24/18 17:01
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 17:01
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/24/18 17:01
1
Tetrahydrofuran
6.1 J
10
5.0
1.9
ug/L
04/24/18 17:01
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/24/18 17:01
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/24/18 17:01
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 17:01
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/24/18 17:01
1
Trichloroethene
0.19 J
0.50
0.25
0.16
ug/L
04/24/18 17:01
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 17:01
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/24/18 17:01
1
Vinyl chloride
3.1
1.0
0.50
0.20
ug/L
04/24/18 17:01
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/24/18 17:01
1
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
105
75- 126
04125118 12:24
1
4-Bromofluorobenzene (Surr)
101
72 - 124
04125118 12:24
1
Dibromofluoromethane
99
75 - 120
04125118 12:24
1
Toluene-d8 (Surr)
93
75 - 120
04/25/18 12:24
1
TestAmerica Chicago
Page 139 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: Duplicate 2 Lab Sample ID: 500-143858-24
Date Collected: 04/12/18 00:00 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/25/18 12:54
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/25/18 12:54
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/25/18 12:54
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/25/18 12:54
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/25/18 12:54
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/25/18 12:54
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/25/18 12:54
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/25/18 12:54
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/25/18 12:54
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/25/18 12:54
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/25/18 12:54
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/25/18 12:54
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/25/18 12:54
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/25/18 12:54
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/25/18 12:54
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/25/18 12:54
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/25/18 12:54
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/25/18 12:54
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/25/18 12:54
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/25/18 12:54
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/25/18 12:54
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/25/18 12:54
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/25/18 12:54
1
Acetone
10 cn
5.0
2.5
1.7
ug/L
04/25/18 12:54
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/25/18 12:54
1
Acrolein
<23
100
50
23
ug/L
04/25/18 12:54
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/25/18 12:54
1
Benzene
0.56
0.50
0.25
0.15
ug/L
04/25/18 12:54
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/25/18 12:54
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/25/18 12:54
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/25/18 12:54
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/25/18 12:54
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/25/18 12:54
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/25/18 12:54
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/25/18 12:54
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/25/18 12:54
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/25/18 12:54
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/25/18 12:54
1
cis-1,2-Dichloroethene
1.6
1.0
0.50
0.41
ug/L
04/25/18 12:54
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/25/18 12:54
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/25/18 12:54
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/25/18 12:54
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/25/18 12:54
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/25/18 12:54
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/25/18 12:54
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/25/18 12:54
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/25/18 12:54
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/25/18 12:54
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/25/18 12:54
1
TestAmerica Chicago
Page 140 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: Duplicate 2
Lab Sample ID: 500-143858-24
Date Collected: 04/12/18 00:00
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS)
(Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/25/18 12:54
1
Methylene Chloride
4.7 J
5.0
2.5
1.6
ug/L
04/25/18 12:54
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/25/18 12:54
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/25/18 12:54
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/25/18 12:54
1
Tetrahydrofuran
4.8 J
10
5.0
1.9
ug/L
04/25/18 12:54
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/25/18 12:54
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/25/18 12:54
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/25/18 12:54
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/25/18 12:54
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/25/18 12:54
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/25/18 12:54
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/25/18 12:54
1
Vinyl chloride
1.5
1.0
0.50
0.20
ug/L
04/25/18 12:54
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/25/18 12:54
1
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
102
75- 126
04125118 12:54
1
4-Bromofluorobenzene (Surr)
102
72 - 124
04125118 12:54
1
Dibromofluoromethane
99
75 - 120
04125118 12:54
1
Toluene-d8 (Surr)
92
75 - 120
04/25/18 12:54
1
TestAmerica Chicago
Page 141 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: TB Lab Sample ID: 500-143858-25
Date Collected: 04/10/18 00:00 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/20/18 18:05
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/20/18 18:05
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/20/18 18:05
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/20/18 18:05
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/20/18 18:05
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 18:05
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/20/18 18:05
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/20/18 18:05
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/20/18 18:05
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/20/18 18:05
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/20/18 18:05
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/20/18 18:05
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/20/18 18:05
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 18:05
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/20/18 18:05
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/20/18 18:05
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/20/18 18:05
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/20/18 18:05
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/20/18 18:05
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/20/18 18:05
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/20/18 18:05
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/20/18 18:05
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/20/18 18:05
1
Acetone
<1.7
5.0
2.5
1.7
ug/L
04/20/18 18:05
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/20/18 18:05
1
Acrolein
<23
100
50
23
ug/L
04/20/18 18:05
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/20/18 18:05
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/20/18 18:05
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 18:05
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/20/18 18:05
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/20/18 18:05
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/20/18 18:05
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/20/18 18:05
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/20/18 18:05
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 18:05
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/20/18 18:05
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/20/18 18:05
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/20/18 18:05
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/20/18 18:05
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/20/18 18:05
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/20/18 18:05
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/20/18 18:05
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/20/18 18:05
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/20/18 18:05
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/20/18 18:05
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/20/18 18:05
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/20/18 18:05
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/20/18 18:05
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/20/18 18:05
1
TestAmerica Chicago
Page 142 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg
Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: TB
Lab Sample ID: 500-143858-25
Date Collected: 04/10/18 00:00
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS)
(Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/20/18 18:05
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/20/18 18:05
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/20/18 18:05
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 18:05
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/20/18 18:05
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/20/18 18:05
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/20/18 18:05
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/20/18 18:05
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/20/18 18:05
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/20/18 18:05
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/20/18 18:05
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 18:05
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/20/18 18:05
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/20/18 18:05
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/20/18 18:05
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
109
75- 126
04120118 18:05
1
4-Bromofluorobenzene (Surr)
91
72 - 124
04120118 18:05
1
Dibromofluoromethane
97
75 - 120
04120118 18:05
1
Toluene-d8 (Surr)
93
75 - 120
04120118 18:05
1
TestAmerica Chicago
Page 143 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: TB Lab Sample ID: 500-143858-26
Date Collected: 04/10/18 00:00 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/20/18 18:33
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/20/18 18:33
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/20/18 18:33
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/20/18 18:33
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/20/18 18:33
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 18:33
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/20/18 18:33
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/20/18 18:33
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/20/18 18:33
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/20/18 18:33
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/20/18 18:33
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/20/18 18:33
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/20/18 18:33
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 18:33
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/20/18 18:33
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/20/18 18:33
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/20/18 18:33
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/20/18 18:33
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/20/18 18:33
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/20/18 18:33
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/20/18 18:33
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/20/18 18:33
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/20/18 18:33
1
Acetone
<1.7
5.0
2.5
1.7
ug/L
04/20/18 18:33
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/20/18 18:33
1
Acrolein
<23
100
50
23
ug/L
04/20/18 18:33
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/20/18 18:33
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/20/18 18:33
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 18:33
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/20/18 18:33
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/20/18 18:33
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/20/18 18:33
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/20/18 18:33
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/20/18 18:33
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 18:33
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/20/18 18:33
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/20/18 18:33
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/20/18 18:33
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/20/18 18:33
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/20/18 18:33
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/20/18 18:33
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/20/18 18:33
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/20/18 18:33
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/20/18 18:33
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/20/18 18:33
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/20/18 18:33
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/20/18 18:33
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/20/18 18:33
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/20/18 18:33
1
TestAmerica Chicago
Page 144 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg
Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: TB
Lab Sample ID: 500-143858-26
Date Collected: 04/10/18 00:00
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS)
(Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/20/18 18:33
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/20/18 18:33
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/20/18 18:33
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 18:33
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/20/18 18:33
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/20/18 18:33
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/20/18 18:33
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/20/18 18:33
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/20/18 18:33
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/20/18 18:33
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/20/18 18:33
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 18:33
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/20/18 18:33
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/20/18 18:33
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/20/18 18:33
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
109
75- 126
04120118 18:33
1
4-Bromofluorobenzene (Surr)
91
72 - 124
04120118 18:33
1
Dibromofluoromethane
94
75 - 120
04120118 18:33
1
Toluene-d8 (Surr)
93
75 - 120
04120118 18:33
1
TestAmerica Chicago
Page 145 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: TB Lab Sample ID: 500-143858-27
Date Collected: 04/10/18 00:00 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/20/18 19:02
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/20/18 19:02
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/20/18 19:02
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/20/18 19:02
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/20/18 19:02
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 19:02
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/20/18 19:02
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/20/18 19:02
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/20/18 19:02
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/20/18 19:02
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/20/18 19:02
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/20/18 19:02
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/20/18 19:02
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 19:02
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/20/18 19:02
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/20/18 19:02
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/20/18 19:02
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/20/18 19:02
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/20/18 19:02
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/20/18 19:02
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/20/18 19:02
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/20/18 19:02
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/20/18 19:02
1
Acetone
<1.7
5.0
2.5
1.7
ug/L
04/20/18 19:02
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/20/18 19:02
1
Acrolein
<23
100
50
23
ug/L
04/20/18 19:02
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/20/18 19:02
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/20/18 19:02
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 19:02
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/20/18 19:02
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/20/18 19:02
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/20/18 19:02
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/20/18 19:02
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/20/18 19:02
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 19:02
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/20/18 19:02
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/20/18 19:02
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/20/18 19:02
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/20/18 19:02
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/20/18 19:02
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/20/18 19:02
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/20/18 19:02
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/20/18 19:02
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/20/18 19:02
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/20/18 19:02
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/20/18 19:02
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/20/18 19:02
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/20/18 19:02
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/20/18 19:02
1
TestAmerica Chicago
Page 146 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg
Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: TB
Lab Sample ID: 500-143858-27
Date Collected: 04/10/18 00:00
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS)
(Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/20/18 19:02
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/20/18 19:02
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/20/18 19:02
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 19:02
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/20/18 19:02
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/20/18 19:02
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/20/18 19:02
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/20/18 19:02
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/20/18 19:02
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/20/18 19:02
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/20/18 19:02
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 19:02
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/20/18 19:02
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/20/18 19:02
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/20/18 19:02
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
108
75- 126
04120118 19:02
1
4-Bromofluorobenzene (Surr)
93
72 - 124
04120118 19:02
1
Dibromofluoromethane
93
75 - 120
04120118 19:02
1
Toluene-d8 (Surr)
94
75 - 120
04120118 19:02
1
TestAmerica Chicago
Page 147 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: TB Lab Sample ID: 500-143858-28
Date Collected: 04/10/18 00:00 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/20/18 19:30
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/20/18 19:30
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/20/18 19:30
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/20/18 19:30
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/20/18 19:30
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 19:30
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/20/18 19:30
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/20/18 19:30
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/20/18 19:30
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/20/18 19:30
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/20/18 19:30
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/20/18 19:30
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/20/18 19:30
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 19:30
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/20/18 19:30
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/20/18 19:30
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/20/18 19:30
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/20/18 19:30
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/20/18 19:30
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/20/18 19:30
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/20/18 19:30
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/20/18 19:30
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/20/18 19:30
1
Acetone
<1.7
5.0
2.5
1.7
ug/L
04/20/18 19:30
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/20/18 19:30
1
Acrolein
<23
100
50
23
ug/L
04/20/18 19:30
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/20/18 19:30
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/20/18 19:30
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 19:30
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/20/18 19:30
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/20/18 19:30
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/20/18 19:30
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/20/18 19:30
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/20/18 19:30
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 19:30
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/20/18 19:30
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/20/18 19:30
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/20/18 19:30
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/20/18 19:30
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/20/18 19:30
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/20/18 19:30
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/20/18 19:30
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/20/18 19:30
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/20/18 19:30
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/20/18 19:30
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/20/18 19:30
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/20/18 19:30
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/20/18 19:30
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/20/18 19:30
1
TestAmerica Chicago
Page 148 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg
Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: TB
Lab Sample ID: 500-143858-28
Date Collected: 04/10/18 00:00
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS)
(Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/20/18 19:30
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/20/18 19:30
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/20/18 19:30
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 19:30
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/20/18 19:30
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/20/18 19:30
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/20/18 19:30
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/20/18 19:30
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/20/18 19:30
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/20/18 19:30
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/20/18 19:30
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 19:30
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/20/18 19:30
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/20/18 19:30
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/20/18 19:30
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
109
75- 126
04120118 19:30
1
4-Bromofluorobenzene (Surr)
90
72 - 124
04120118 19:30
1
Dibromofluoromethane
96
75 - 120
04120118 19:30
1
Toluene-d8 (Surr)
93
75 - 120
04120118 19:30
1
TestAmerica Chicago
Page 149 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: TB Lab Sample ID: 500-143858-29
Date Collected: 04/10/18 00:00 Matrix: Water
Date Received: 04/14/18 12:55
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/20/18 19:59
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/20/18 19:59
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/20/18 19:59
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/20/18 19:59
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/20/18 19:59
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 19:59
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/20/18 19:59
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/20/18 19:59
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/20/18 19:59
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/20/18 19:59
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/20/18 19:59
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/20/18 19:59
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/20/18 19:59
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 19:59
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/20/18 19:59
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/20/18 19:59
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/20/18 19:59
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/20/18 19:59
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/20/18 19:59
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/20/18 19:59
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/20/18 19:59
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/20/18 19:59
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/20/18 19:59
1
Acetone
<1.7
5.0
2.5
1.7
ug/L
04/20/18 19:59
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/20/18 19:59
1
Acrolein
<23
100
50
23
ug/L
04/20/18 19:59
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/20/18 19:59
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/20/18 19:59
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 19:59
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/20/18 19:59
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/20/18 19:59
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/20/18 19:59
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/20/18 19:59
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/20/18 19:59
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 19:59
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/20/18 19:59
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/20/18 19:59
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/20/18 19:59
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/20/18 19:59
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/20/18 19:59
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/20/18 19:59
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/20/18 19:59
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/20/18 19:59
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/20/18 19:59
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/20/18 19:59
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/20/18 19:59
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/20/18 19:59
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/20/18 19:59
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/20/18 19:59
1
TestAmerica Chicago
Page 150 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg
Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: TB
Lab Sample ID: 500-143858-29
Date Collected: 04/10/18 00:00
Matrix:
Water
Date Received: 04/14/18 12:55
Method: 8260B - Volatile Organic Compounds (GC/MS)
(Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/20/18 19:59
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/20/18 19:59
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/20/18 19:59
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 19:59
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/20/18 19:59
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/20/18 19:59
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/20/18 19:59
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/20/18 19:59
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/20/18 19:59
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/20/18 19:59
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/20/18 19:59
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 19:59
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/20/18 19:59
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/20/18 19:59
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/20/18 19:59
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
111
75- 126
04120118 19:59
1
4-Bromofluorobenzene (Surr)
92
72 - 124
04120118 19:59
1
Dibromofluoromethane
97
75 - 120
04120118 19:59
1
Toluene-d8 (Surr)
93
75 - 120
04120118 19:59
1
TestAmerica Chicago
Page 151 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW11(i) Lab Sample ID: 500-143858-30
Date Collected: 04/12/18 12:50 Matrix: Water
Date Received: 04/18/18 09:10
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/24/18 18:43
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/24/18 18:43
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/24/18 18:43
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/24/18 18:43
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 18:43
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 18:43
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/24/18 18:43
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 18:43
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/24/18 18:43
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/24/18 18:43
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 18:43
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/24/18 18:43
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 18:43
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 18:43
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/24/18 18:43
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/24/18 18:43
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 18:43
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/24/18 18:43
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/24/18 18:43
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/24/18 18:43
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/24/18 18:43
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/24/18 18:43
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/24/18 18:43
1
Acetone
7.2 cn
5.0
2.5
1.7
ug/L
04/24/18 18:43
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/24/18 18:43
1
Acrolein
<23
100
50
23
ug/L
04/24/18 18:43
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/24/18 18:43
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/24/18 18:43
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 18:43
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/24/18 18:43
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/24/18 18:43
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/24/18 18:43
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/24/18 18:43
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/24/18 18:43
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 18:43
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/24/18 18:43
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/24/18 18:43
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/24/18 18:43
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/24/18 18:43
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/24/18 18:43
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/24/18 18:43
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/24/18 18:43
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/24/18 18:43
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/24/18 18:43
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/24/18 18:43
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/24/18 18:43
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/24/18 18:43
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/24/18 18:43
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/24/18 18:43
1
TestAmerica Chicago
Page 152 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill
- Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW11(i)
Lab Sample
ID: 500-143858-30
Date Collected: 04/12/18 12:50
Matrix:
Water
Date Received: 04/18/18 09:10
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/24/18 18:43
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/24/18 18:43
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/24/18 18:43
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 18:43
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/24/18 18:43
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/24/18 18:43
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/24/18 18:43
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/24/18 18:43
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 18:43
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/24/18 18:43
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/24/18 18:43
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 18:43
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/24/18 18:43
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/24/18 18:43
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/24/18 18:43
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 99 75- 126
4-Bromofluorobenzene (Surr) 105 72 - 124
Dibromofluoromethane 91 75 - 120
Toluene-d8 (Surr) 92 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04124118 18:43
04124118 18:43
04124118 18:43
04124118 18:43
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.24
0.77
0.39
0.24
ug/L
04/20/18 19:05
1
Acenaphthylene
<0.21
0.77
0.39
0.21
ug/L
04/20/18 19:05
1
Acetophenone
<0.51
3.9
1.9
0.51
ug/L
04/20/18 19:05
1
2-Acetylaminofluorene
<1.6
7.7
3.9
1.6
ug/L
04/20/18 19:05
1
4-Aminobiphenyl
<2.9
7.7
3.9
2.9
ug/L
04/20/18 19:05
1
Anthracene
<0.26
0.77
0.39
0.26
ug/L
04/20/18 19:05
1
Benzo[a]anthracene
<0.044
0.15
0.077
0.044
ug/L
04/20/18 19:05
1
Benzo[a]pyrene
<0.077
0.15
0.077
0.077
ug/L
04/20/18 19:05
1
Benzo[b]fluoranthene
<0.062
0.15
0.077
0.062
ug/L
04/20/18 19:05
1
Benzo[g,h,i]perylene
<0.29
0.77
0.39
0.29
ug/L
04/20/18 19:05
1
Benzo[k]fluoranthene
<0.050
0.15
0.077
0.050
ug/L
04/20/18 19:05
1
Benzyl alcohol
<4.7
15
7.7
4.7
ug/L
04/20/18 19:05
1
Bis(2-chloroethoxy)methane
<0.22
1.5
0.77
0.22
ug/L
04/20/18 19:05
1
Bis(2-chloroethyl)ether
<0.23
1.5
0.77
0.23
ug/L
04/20/18 19:05
1
Bis(2-ethylhexyl) phthalate
<1.3
7.7
3.9
1.3
ug/L
04/20/18 19:05
1
4-Bromophenyl phenyl ether
<0.42
3.9
1.9
0.42
ug/L
04/20/18 19:05
1
Butyl benzyl phthalate
<0.37
1.5
0.77
0.37
ug/L
04/20/18 19:05
1
4-Chloroaniline
<1.6
7.7
3.9
1.6
ug/L
04/20/18 19:05
1
Chlorobenzilate
<2.6
7.7
3.9
2.6
ug/L
04/20/18 19:05
1
4-Chloro-3-methylphenol
<1.8
7.7
3.9
1.8
ug/L
04/20/18 19:05
1
2-Chloronaphthalene
<0.18
1.5
0.77
0.18
ug/L
04/20/18 19:05
1
2-Chlorophenol
<0.43
3.9
1.9
0.43
ug/L
04/20/18 19:05
1
4-Chlorophenyl phenyl ether
<0.49
3.9
1.9
0.49
ug/L
04/20/18 19:05
1
Chrysene
<0.053
0.15
0.077
0.053
ug/L
04/20/18 19:05
1
Diallate
<4.3
7.7
4.8
4.3
ug/L
04/20/18 19:05
1
Dibenz(a,h)anthracene
<0.039
0.23
0.12
0.039
ug/L
04/20/18 19:05
1
TestAmerica Chicago
Page 153 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW11(i) Lab Sample ID: 500-143858-30
Date Collected: 04/12/18 12:50 Matrix: Water
Date Received: 04/18/18 09:10
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.20
1.5
0.77
0.20
ug/L
04/20/18 19:05
1
3,3'-Dichlorobenzidine
<1.3
3.9
1.9
1.3
ug/L
04/20/18 19:05
1
2,4-Dichlorophenol
<2.0
7.7
3.9
2.0
ug/L
04/20/18 19:05
1
2,6-Dichlorophenol
<2.7
7.7
3.9
2.7
ug/L
04/20/18 19:05
1
Diethyl phthalate
<0.28
3.9
1.5
0.28
ug/L
04/20/18 19:05
1
Dimethoate
<1.4
7.7
3.9
1.4
ug/L
04/20/18 19:05
1
7,12-Dimethylbenz(a)anthracene
<2.3
31
15
2.3
ug/L
04/20/18 19:05
1
3,3'-Dimethylbenzidine
<14
31
15
14
ug/L
04/20/18 19:05
1
2,4-Dimethylphenol
<1.4
7.7
3.9
1.4
ug/L
04/20/18 19:05
1
Dimethyl phthalate
<0.24
3.9
1.5
0.24
ug/L
04/20/18 19:05
1
Di-n-butyl phthalate
<0.57
3.9
1.9
0.57
ug/L
04/20/18 19:05
1
4,6-Dinitro-2-methylphenol
<4.6
15
7.7
4.6
ug/L
04/20/18 19:05
1
2,4-Dinitrophenol
<6.7
15
7.7
6.7
ug/L
04/20/18 19:05
1
2,4-Dinitrotoluene
<0.19
0.77
0.39
0.19
ug/L
04/20/18 19:05
1
2,6-Dinitrotoluene
<0.057
0.77
0.39
0.057
ug/L
04/20/18 19:05
1
Di-n-octyl phthalate
<0.81
7.7
3.9
0.81
ug/L
04/20/18 19:05
1
Diphenylamine
<2.0
7.7
3.9
2.0
ug/L
04/20/18 19:05
1
Disulfoton
<1.5
7.7
3.9
1.5
ug/L
04/20/18 19:05
1
Ethyl methanesulfonate
<2.9
15
7.7
2.9
ug/L
04/20/18 19:05
1
Ethyl Parathion
<1.6
7.7
3.9
1.6
ug/L
04/20/18 19:05
1
Famphur
<23
31
24
23
ug/L
04/20/18 19:05
1
Fluoranthene
<0.35
0.77
0.39
0.35
ug/L
04/20/18 19:05
1
Fluorene
<0.19
0.77
0.39
0.19
ug/L
04/20/18 19:05
1
Hexachlorobenzene
<0.061
0.39
0.19
0.061
ug/L
04/20/18 19:05
1
Hexachlorocyclopentadiene
<4.9
15
7.7
4.9
ug/L
04/20/18 19:05
1
Hexachloroethane
<0.46
3.9
1.9
0.46
ug/L
04/20/18 19:05
1
Hexachloropropene
<3.6
15
7.7
3.6
ug/L
04/20/18 19:05
1
Indeno[1,2,3-cd]pyrene
<0.058
0.15
0.077
0.058
ug/L
04/20/18 19:05
1
Isodrin
<5.3
15
7.7
5.3
ug/L
04/20/18 19:05
1
Isophorone
<0.29
1.5
0.77
0.29
ug/L
04/20/18 19:05
1
Isosafrole
<3.0
7.7
3.9
3.0
ug/L
04/20/18 19:05
1
Kepone
<1.3
7.7
3.9
1.3
ug/L
04/20/18 19:05
1
m-Dinitrobenzene
<1.0
3.9
1.9
1.0
ug/L
04/20/18 19:05
1
Methapyrilene
<7.9
31
15
7.9
ug/L
04/20/18 19:05
1
3-Methylcholanthrene
<1.8
7.7
3.9
1.8
ug/L
04/20/18 19:05
1
Methyl methanesulfonate
<4.6
31
15
4.6
ug/L
04/20/18 19:05
1
2-Methylnaphthalene
<0.050
1.5
0.77
0.050
ug/L
04/20/18 19:05
1
Methyl parathion
<1.8
7.7
3.9
1.8
ug/L
04/20/18 19:05
1
2-Methylphenol
<0.24
1.5
0.77
0.24
ug/L
04/20/18 19:05
1
3 & 4 Methylphenol
<0.35
1.5
0.77
0.35
ug/L
04/20/18 19:05
1
Naphthalene
<0.24
0.77
0.39
0.24
ug/L
04/20/18 19:05
1
1,4-Naphthoquinone
<30
31
31
30
ug/L
04/20/18 19:05
1
1-Naphthylamine
<4.6
15
7.7
4.6
ug/L
04/20/18 19:05
1
2-Naphthylamine
<7.1
15
7.7
7.1
ug/L
04/20/18 19:05
1
2-Nitroaniline
<1.0
3.9
1.9
1.0
ug/L
04/20/18 19:05
1
3-Nitroaniline
<1.4
7.7
3.9
1.4
ug/L
04/20/18 19:05
1
4-Nitroaniline
<1.3
7.7
3.9
1.3
ug/L
04/20/18 19:05
1
Nitrobenzene
<0.35
0.77
0.39
0.35
ug/L
04/20/18 19:05
1
5-Nitro-o-toluidine
<2.4
7.7
3.9
2.4
ug/L
04/20/18 19:05
1
TestAmerica Chicago
Page 154 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW11(i)
Lab Sample ID: 500-143858-30
Date Collected: 04/12/18 12:50
Matrix:
Water
Date Received: 04/18/18 09:10
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<1.9
7.7
3.9
1.9
ug/L
04/20/18 19:05
1
4-Nitrophenol
<5.8
15
7.7
5.8
ug/L
04/20/18 19:05
1
N-Nitrosodiethylamine
<6.7
15
7.7
6.7
ug/L
04/20/18 19:05
1
N-Nitrosodimethylamine
<3.7
7.7
3.9
3.7
ug/L
04/20/18 19:05
1
N-Nitrosodi-n-butylamine
<3.2
7.7
3.9
3.2
ug/L
04/20/18 19:05
1
N-Nitrosodi-n-propylamine
<0.12
0.39
0.19
0.12
ug/L
04/20/18 19:05
1
N-Nitrosodiphenylamine
<0.29
1.5
0.77
0.29
ug/L
04/20/18 19:05
1
N-Nitrosomethylethylamine
<5.8
15
7.7
5.8
ug/L
04/20/18 19:05
1
N-Nitrosopiperidine
<2.7
7.7
3.9
2.7
ug/L
04/20/18 19:05
1
N-Nitrosopyrrolidine
<2.6
7.7
3.9
2.6
ug/L
04/20/18 19:05
1
o,o',o"-Triethylphosphorothioate
<4.3
15
7.7
4.3
ug/L
04/20/18 19:05
1
o-Toluidine
<6.1
31
15
6.1
ug/L
04/20/18 19:05
1
2,2'-oxybis[l-chloropropane]
<0.29
1.5
0.77
0.29
ug/L
04/20/18 19:05
1
p-Dimethylamino azobenzene
<2.3
7.7
3.9
2.3
ug/L
04/20/18 19:05
1
Pentachlorobenzene
<2.2
7.7
3.9
2.2
ug/L
04/20/18 19:05
1
Pentachloronitrobenzene
<2.8
7.7
3.9
2.8
ug/L
04/20/18 19:05
1
Phenacetin
<1.8
7.7
3.9
1.8
ug/L
04/20/18 19:05
1
Phenanthrene
<0.23
0.77
0.39
0.23
ug/L
04/20/18 19:05
1
Phenol
<0.52
3.9
1.9
0.52
ug/L
04/20/18 19:05
1
Phorate
<1.7
7.7
3.9
1.7
ug/L
04/20/18 19:05
1
p-Phenylene diamine
<13
62
31
13
ug/L
04/20/18 19:05
1
Pronamide
<1.7
7.7
7.7
1.7
ug/L
04/20/18 19:05
1
Pyrene
<0.33
0.77
0.39
0.33
ug/L
04/20/18 19:05
1
Safrole
<3.1
7.7
3.9
3.1
ug/L
04/20/18 19:05
1
sym-Trinitrobenzene
<1.4
7.7
3.9
1.4
ug/L
04/20/18 19:05
1
2,3,7,8-TCDD (Screen)
<7.7
7.7
7.7
7.7
ug/L
04/20/18 19:05
1
1,2,4,5-Tetrachlorobenzene
<0.44
3.9
1.9
0.44
ug/L
04/20/18 19:05
1
2,3,4,6-Tetrachlorophenol
<0.58
3.9
1.9
0.58
ug/L
04/20/18 19:05
1
Thionazin
<2.0
7.7
3.9
2.0
ug/L
04/20/18 19:05
1
2,4,5-Trichlorophenol
<2.0
7.7
3.9
2.0
ug/L
04/20/18 19:05
1
2,4,6-Trichlorophenol
<0.55
3.9
1.9
0.55
ug/L
04/20/18 19:05
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
94
34 - 110
04118118 17:41
04120118 19:05
1
2-Fluorophenol
52
27- 110
04118118 17:41
04120118 19:05
1
Nitrobenzene-d5
90
36 - 120
04118118 17:41
04120118 19:05
1
Phenol-d5
40
20- 100
04118118 17:41
04120118 19:05
1
Terphenyl-d14
138
40- 145
04118118 17:41
04120118 19:05
1
2,4,6-Tribromophenol
97
40- 145
04118118 17:41
04120118 19:05
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
alpha-BHC
<0.0027
0.041
0.020
0.0027
ug/L
04/20/18 14:06
1
beta-BHC
<0.010
0.041
0.020
0.010
ug/L
04/20/18 14:06
1
delta-BHC
<0.011 *
0.041
0.020
0.011
ug/L
04/20/18 14:06
1
gamma-BHC (Lindane)
<0.0057
0.041
0.020
0.0057
ug/L
04/20/18 14:06
1
Heptachlor
<0.014
0.041
0.020
0.014
ug/L
04/20/18 14:06
1
Aldrin
<0.0054 *
0.041
0.020
0.0054
ug/L
04/20/18 14:06
1
Heptachlor epoxide
<0.014
0.041
0.020
0.014
ug/L
04/20/18 14:06
1
Endosulfan 1
<0.0042
0.041
0.020
0.0042
ug/L
04/20/18 14:06
1
TestAmerica Chicago
Page 155 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW11(i)
Lab Sample ID: 500-143858-30
Date Collected: 04/12/18 12:50
Matrix:
Water
Date Received: 04/18/18 09:10
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.013
0.041
0.020
0.013
ug/L
04/20/18 14:06
1
4,4'-DDE
<0.0039
0.041
0.020
0.0039
ug/L
04/20/18 14:06
1
Endrin
<0.014
0.041
0.020
0.014
ug/L
04/20/18 14:06
1
Endosulfan II
<0.0029
0.041
0.020
0.0029
ug/L
04/20/18 14:06
1
4,4'-DDD
<0.014
0.041
0.020
0.014
ug/L
04/20/18 14:06
1
Endosulfan sulfate
<0.012
0.041
0.020
0.012
ug/L
04/20/18 14:06
1
4,4'-DDT
<0.0033
0.041
0.020
0.0033
ug/L
04/20/18 14:06
1
Methoxychlor
<0.023
0.082
0.041
0.023
ug/L
04/20/18 14:06
1
Toxaphene
<0.20
0.41
0.20
0.20
ug/L
04/20/18 14:06
1
Endrin aldehyde
<0.0084
0.041
0.020
0.0084
ug/L
04/20/18 14:06
1
Chlordane (technical)
<0.041
0.082
0.041
0.041
ug/L
04/20/18 14:06
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
99
30 - 130
04119118 07:40
04120118 14:06
1
Tetrachloro-m-xylene
86
30 - 120
04119118 07:40
04120118 14:06
1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.068
0.41
0.20
0.068
ug/L
04/19/18 16:45
1
PCB-1221
<0.20
0.41
0.20
0.20
ug/L
04/19/18 16:45
1
PCB-1232
<0.20
0.41
0.20
0.20
ug/L
04/19/18 16:45
1
PCB-1242
<0.20
0.41
0.20
0.20
ug/L
04/19/18 16:45
1
PCB-1248
<0.20
0.41
0.20
0.20
ug/L
04/19/18 16:45
1
PCB-1254
<0.20
0.41
0.20
0.20
ug/L
04/19/18 16:45
1
PCB-1260
<0.071
0.41
0.20
0.071
ug/L
04/19/18 16:45
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
65
30 - 120
04119118 07:40
04119118 16:45
1
DCB Decachlorobiphenyl
69
30 - 140
04119118 07:40
04119118 16:45
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.50
1.1
0.53
0.50
ug/L
04/19/18 06:08
1
Dinoseb
<0.18
2.1
1.1
0.18
ug/L
04/19/18 06:08
1
Pentachlorophenol
<0.096
0.53
0.11
0.096
ug/L
04/19/18 06:08
1
Silvex (2,4,5-TP)
<0.31
1.1
0.53
0.31
ug/L
04/19/18 06:08
1
2,4,5-T
<0.46
1.1
0.53
0.46
ug/L
04/19/18 06:08
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
60
25 - 130
04118118 11:15
04119118 06:08
1
Method: 6020B - Metals (ICP/MS)
- Total Recoverable
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 05:13
1
Arsenic
1.0
1.0
0.50
0.23
ug/L
04/21/18 05:13
1
Barium
85
2.5
1.3
0.73
ug/L
04/21/18 05:13
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 05:13
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 05:13
1
Chromium
1.2 J
5.0
2.5
1.1
ug/L
04/21/18 05:13
1
Cobalt
2.3
1.0
0.50
0.40
ug/L
04/21/18 05:13
1
Copper
1.5 J
2.0
1.0
0.50
ug/L
04/21/18 05:13
1
TestAmerica Chicago
Page 156 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill
- Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW11(i)
Lab Sample
ID: 500-143858-30
Date Collected: 04/12/18 12:50
Matrix:
Water
Date Received: 04/18/18 09:10
Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Iron
11000
100
50
47
ug/L
04/21/18 05:13
1
Lead
<0.19
0.50
0.25
0.19
ug/L
04/21/18 05:13
1
Manganese
1000
2.5
1.3
0.79
ug/L
04/21/18 05:13
1
Nickel
2.6
2.0
1.0
0.63
ug/L
04/21/18 05:13
1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 05:13
1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 05:13
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 05:13
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 05:13
1
Vanadium
<2.2
5.0
2.5
2.2
ug/L
04/21/18 05:13
1
Zinc
<6.9
10
20
6.9
ug/L
04/21/18 05:13
1
Method: 7470A - Mercury (CVAA)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/20/1810:05
1
General Chemistry
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/25/18 09:58
1
Chloride
14000
1000
850
850
ug/L
04/27/18 22:58
5
Sulfate
140000
4000
2000
1900
ug/L
04/26/18 22:48
20
Alkalinity
220000
5000
5000
3700
ug/L
04/24/1814:58
1
Total Dissolved Solids
530000
10000
10000
4300
ug/L
04/19/18 04:19
1
TestAmerica Chicago
Page 157 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW11 D(i) Lab Sample ID: 500-143858-31
Date Collected: 04/12/18 12:00 Matrix: Water
Date Received: 04/18/18 09:10
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/24/18 19:08
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/24/18 19:08
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/24/18 19:08
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/24/18 19:08
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 19:08
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 19:08
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/24/18 19:08
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/24/18 19:08
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/24/18 19:08
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/24/18 19:08
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 19:08
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/24/18 19:08
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 19:08
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 19:08
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/24/18 19:08
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/24/18 19:08
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 19:08
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/24/18 19:08
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/24/18 19:08
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/24/18 19:08
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/24/18 19:08
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/24/18 19:08
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/24/18 19:08
1
Acetone
4.6 J cn
5.0
2.5
1.7
ug/L
04/24/18 19:08
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/24/18 19:08
1
Acrolein
<23
100
50
23
ug/L
04/24/18 19:08
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/24/18 19:08
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/24/18 19:08
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 19:08
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/24/18 19:08
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/24/18 19:08
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/24/18 19:08
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/24/18 19:08
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/24/18 19:08
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 19:08
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/24/18 19:08
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/24/18 19:08
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/24/18 19:08
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/24/18 19:08
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/24/18 19:08
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/24/18 19:08
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/24/18 19:08
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/24/18 19:08
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/24/18 19:08
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/24/18 19:08
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/24/18 19:08
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/24/18 19:08
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/24/18 19:08
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/24/18 19:08
1
TestAmerica Chicago
Page 158 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW11 D(i)
Lab Sample
ID: 500-143858-31
Date Collected: 04/12/18 12:00
Matrix:
Water
Date Received: 04/18/18 09:10
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/24/18 19:08
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/24/18 19:08
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/24/18 19:08
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 19:08
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/24/18 19:08
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/24/18 19:08
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/24/18 19:08
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/24/18 19:08
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 19:08
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/24/18 19:08
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/24/18 19:08
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 19:08
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/24/18 19:08
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/24/18 19:08
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/24/18 19:08
1
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 100 75- 126
4-Bromofluorobenzene (Surr) 105 72 - 124
Dibromofluoromethane 91 75 - 120
Toluene-d8 (Surr) 89 75 - 120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
LOD
MDL
Prepared
Unit D
Analyzed
04124118 19:08
04124118 19:08
04124118 19:08
04124118 19:08
Analyzed
Dil Fac
1
1
1
1
Dil Fac
Acenaphthene
<0.23
0.76
0.38
0.23
ug/L
04/20/18 19:30
1
Acenaphthylene
<0.20
0.76
0.38
0.20
ug/L
04/20/18 19:30
1
Acetophenone
<0.50
3.8
1.9
0.50
ug/L
04/20/18 19:30
1
2-Acetylaminofluorene
<1.6
7.6
3.8
1.6
ug/L
04/20/18 19:30
1
4-Aminobiphenyl
<2.8
7.6
3.8
2.8
ug/L
04/20/18 19:30
1
Anthracene
<0.25
0.76
0.38
0.25
ug/L
04/20/18 19:30
1
Benzo[a]anthracene
<0.043
0.15
0.076
0.043
ug/L
04/20/18 19:30
1
Benzo[a]pyrene
<0.075
0.15
0.076
0.075
ug/L
04/20/18 19:30
1
Benzo[b]fluoranthene
<0.061
0.15
0.076
0.061
ug/L
04/20/18 19:30
1
Benzo[g,h,i]perylene
<0.28
0.76
0.38
0.28
ug/L
04/20/18 19:30
1
Benzo[k]fluoranthene
<0.048
0.15
0.076
0.048
ug/L
04/20/18 19:30
1
Benzyl alcohol
<4.6
15
7.6
4.6
ug/L
04/20/18 19:30
1
Bis(2-chloroethoxy)methane
<0.21
1.5
0.76
0.21
ug/L
04/20/18 19:30
1
Bis(2-chloroethyl)ether
<0.22
1.5
0.76
0.22
ug/L
04/20/18 19:30
1
Bis(2-ethylhexyl) phthalate
<1.3
7.6
3.8
1.3
ug/L
04/20/18 19:30
1
4-Bromophenyl phenyl ether
<0.41
3.8
1.9
0.41
ug/L
04/20/18 19:30
1
Butyl benzyl phthalate
<0.36
1.5
0.76
0.36
ug/L
04/20/18 19:30
1
4-Chloroaniline
<1.5
7.6
3.8
1.5
ug/L
04/20/18 19:30
1
Chlorobenzilate
<2.6
7.6
3.8
2.6
ug/L
04/20/18 19:30
1
4-Chloro-3-methylphenol
<1.7
7.6
3.8
1.7
ug/L
04/20/18 19:30
1
2-Chloronaphthalene
<0.18
1.5
0.76
0.18
ug/L
04/20/18 19:30
1
2-Chlorophenol
<0.42
3.8
1.9
0.42
ug/L
04/20/18 19:30
1
4-Chlorophenyl phenyl ether
<0.48
3.8
1.9
0.48
ug/L
04/20/18 19:30
1
Chrysene
<0.052
0.15
0.076
0.052
ug/L
04/20/18 19:30
1
Diallate
<4.2
7.6
4.7
4.2
ug/L
04/20/18 19:30
1
Dibenz(a,h)anthracene
<0.038
0.23
0.11
0.038
ug/L
04/20/18 19:30
1
TestAmerica Chicago
Page 159 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW11 D(i) Lab Sample ID: 500-143858-31
Date Collected: 04/12/18 12:00 Matrix: Water
Date Received: 04/18/18 09:10
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Dibenzofuran
<0.20
1.5
0.76
0.20
ug/L
04/20/18 19:30
1
3,3'-Dichlorobenzidine
<1.3
3.8
1.9
1.3
ug/L
04/20/18 19:30
1
2,4-Dichlorophenol
<2.0
7.6
3.8
2.0
ug/L
04/20/18 19:30
1
2,6-Dichlorophenol
<2.6
7.6
3.8
2.6
ug/L
04/20/18 19:30
1
Diethyl phthalate
<0.27
3.8
1.5
0.27
ug/L
04/20/18 19:30
1
Dimethoate
<1.4
7.6
3.8
1.4
ug/L
04/20/18 19:30
1
7,12-Dimethylbenz(a)anthracene
<2.3
30
15
2.3
ug/L
04/20/18 19:30
1
3,3'-Dimethylbenzidine
<13
30
15
13
ug/L
04/20/18 19:30
1
2,4-Dimethylphenol
<1.4
7.6
3.8
1.4
ug/L
04/20/18 19:30
1
Dimethyl phthalate
<0.24
3.8
1.5
0.24
ug/L
04/20/18 19:30
1
Di-n-butyl phthalate
<0.55
3.8
1.9
0.55
ug/L
04/20/18 19:30
1
4,6-Dinitro-2-methylphenol
<4.5
15
7.6
4.5
ug/L
04/20/18 19:30
1
2,4-Dinitrophenol
<6.5
15
7.6
6.5
ug/L
04/20/18 19:30
1
2,4-Dinitrotoluene
<0.19
0.76
0.38
0.19
ug/L
04/20/18 19:30
1
2,6-Dinitrotoluene
<0.056
0.76
0.38
0.056
ug/L
04/20/18 19:30
1
Di-n-octyl phthalate
<0.80
7.6
3.8
0.80
ug/L
04/20/18 19:30
1
Diphenylamine
<1.9
7.6
3.8
1.9
ug/L
04/20/18 19:30
1
Disulfoton
<1.4
7.6
3.8
1.4
ug/L
04/20/18 19:30
1
Ethyl methanesulfonate
<2.9
15
7.6
2.9
ug/L
04/20/18 19:30
1
Ethyl Parathion
<1.6
7.6
3.8
1.6
ug/L
04/20/18 19:30
1
Famphur
<23
30
24
23
ug/L
04/20/18 19:30
1
Fluoranthene
<0.34
0.76
0.38
0.34
ug/L
04/20/18 19:30
1
Fluorene
<0.18
0.76
0.38
0.18
ug/L
04/20/18 19:30
1
Hexachlorobenzene
<0.060
0.38
0.19
0.060
ug/L
04/20/18 19:30
1
Hexachlorocyclopentadiene
<4.8
15
7.6
4.8
ug/L
04/20/18 19:30
1
Hexachloroethane
<0.45
3.8
1.9
0.45
ug/L
04/20/18 19:30
1
Hexachloropropene
<3.6
15
7.6
3.6
ug/L
04/20/18 19:30
1
Indeno[1,2,3-cd]pyrene
<0.057
0.15
0.076
0.057
ug/L
04/20/18 19:30
1
Isodrin
<5.2
15
7.6
5.2
ug/L
04/20/18 19:30
1
Isophorone
<0.28
1.5
0.76
0.28
ug/L
04/20/18 19:30
1
Isosafrole
<2.9
7.6
3.8
2.9
ug/L
04/20/18 19:30
1
Kepone
<1.3
7.6
3.8
1.3
ug/L
04/20/18 19:30
1
m-Dinitrobenzene
<1.0
3.8
1.9
1.0
ug/L
04/20/18 19:30
1
Methapyrilene
<7.7
30
15
7.7
ug/L
04/20/18 19:30
1
3-Methylcholanthrene
<1.7
7.6
3.8
1.7
ug/L
04/20/18 19:30
1
Methyl methanesulfonate
<4.5
30
15
4.5
ug/L
04/20/18 19:30
1
2-Methylnaphthalene
<0.049
1.5
0.76
0.049
ug/L
04/20/18 19:30
1
Methyl parathion
<1.8
7.6
3.8
1.8
ug/L
04/20/18 19:30
1
2-Methylphenol
<0.23
1.5
0.76
0.23
ug/L
04/20/18 19:30
1
3 & 4 Methylphenol
<0.34
1.5
0.76
0.34
ug/L
04/20/18 19:30
1
Naphthalene
<0.23
0.76
0.38
0.23
ug/L
04/20/18 19:30
1
1,4-Naphthoquinone
<30
30
30
30
ug/L
04/20/18 19:30
1
1-Naphthylamine
<4.5
15
7.6
4.5
ug/L
04/20/18 19:30
1
2-Naphthylamine
<6.9
15
7.6
6.9
ug/L
04/20/18 19:30
1
2-Nitroaniline
<0.98
3.8
1.9
0.98
ug/L
04/20/18 19:30
1
3-Nitroaniline
<1.4
7.6
3.8
1.4
ug/L
04/20/18 19:30
1
4-Nitroaniline
<1.3
7.6
3.8
1.3
ug/L
04/20/18 19:30
1
Nitrobenzene
<0.34
0.76
0.38
0.34
ug/L
04/20/18 19:30
1
5-Nitro-o-toluidine
<2.3
7.6
3.8
2.3
ug/L
04/20/18 19:30
1
TestAmerica Chicago
Page 160 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW11 D(i)
Lab Sample ID: 500-143858-31
Date Collected: 04/12/18 12:00
Matrix:
Water
Date Received: 04/18/18 09:10
Method: 8270D - Semivolatile Organic
Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2-Nitrophenol
<1.9
7.6
3.8
1.9
ug/L
04/20/18 19:30
1
4-Nitrophenol
<5.6
15
7.6
5.6
ug/L
04/20/18 19:30
1
N-Nitrosodiethylamine
<6.5
15
7.6
6.5
ug/L
04/20/18 19:30
1
N-Nitrosodimethylamine
<3.6
7.6
3.8
3.6
ug/L
04/20/18 19:30
1
N-Nitrosodi-n-butylamine
<3.2
7.6
3.8
3.2
ug/L
04/20/18 19:30
1
N-Nitrosodi-n-propylamine
<0.12
0.38
0.19
0.12
ug/L
04/20/18 19:30
1
N-Nitrosodiphenylamine
<0.28
1.5
0.76
0.28
ug/L
04/20/18 19:30
1
N-Nitrosomethylethylamine
<5.7
15
7.6
5.7
ug/L
04/20/18 19:30
1
N-Nitrosopiperidine
<2.7
7.6
3.8
2.7
ug/L
04/20/18 19:30
1
N-Nitrosopyrrolidine
<2.5
7.6
3.8
2.5
ug/L
04/20/18 19:30
1
o,o',o"-Triethylphosphorothioate
<4.2
15
7.6
4.2
ug/L
04/20/18 19:30
1
o-Toluidine
<6.0
30
15
6.0
ug/L
04/20/18 19:30
1
2,2'-oxybis[l-chloropropane]
<0.29
1.5
0.76
0.29
ug/L
04/20/18 19:30
1
p-Dimethylamino azobenzene
<2.3
7.6
3.8
2.3
ug/L
04/20/18 19:30
1
Pentachlorobenzene
<2.1
7.6
3.8
2.1
ug/L
04/20/18 19:30
1
Pentachloronitrobenzene
<2.7
7.6
3.8
2.7
ug/L
04/20/18 19:30
1
Phenacetin
<1.7
7.6
3.8
1.7
ug/L
04/20/18 19:30
1
Phenanthrene
<0.23
0.76
0.38
0.23
ug/L
04/20/18 19:30
1
Phenol
<0.51
3.8
1.9
0.51
ug/L
04/20/18 19:30
1
Phorate
<1.6
7.6
3.8
1.6
ug/L
04/20/18 19:30
1
p-Phenylene diamine
<12
61
30
12
ug/L
04/20/18 19:30
1
Pronamide
<1.6
7.6
7.6
1.6
ug/L
04/20/18 19:30
1
Pyrene
<0.32
0.76
0.38
0.32
ug/L
04/20/18 19:30
1
Safrole
<3.0
7.6
3.8
3.0
ug/L
04/20/18 19:30
1
sym-Trinitrobenzene
<1.4
7.6
3.8
1.4
ug/L
04/20/18 19:30
1
2,3,7,8-TCDD (Screen)
<7.6
7.6
7.6
7.6
ug/L
04/20/18 19:30
1
1,2,4,5-Tetrachlorobenzene
<0.43
3.8
1.9
0.43
ug/L
04/20/18 19:30
1
2,3,4,6-Tetrachlorophenol
<0.57
3.8
1.9
0.57
ug/L
04/20/18 19:30
1
Thionazin
<2.0
7.6
3.8
2.0
ug/L
04/20/18 19:30
1
2,4,5-Trichlorophenol
<1.9
7.6
3.8
1.9
ug/L
04/20/18 19:30
1
2,4,6-Trichlorophenol
<0.54
3.8
1.9
0.54
ug/L
04/20/18 19:30
1
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorobiphenyl
86
34 - 110
04118118 17:41
04120118 19:30
1
2-Fluorophenol
53
27- 110
04118118 17:41
04120118 19:30
1
Nitrobenzene-d5
84
36 - 120
04118118 17:41
04120118 19:30
1
Phenol-d5
39
20- 100
04118118 17:41
04120118 19:30
1
Terphenyl-d14
147 X
40- 145
04118118 17:41
04120118 19:30
1
2,4,6-Tribromophenol
102
40- 145
04118118 17:41
04120118 19:30
1
Method: 8081B - Organochlorine Pesticides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
alpha-BHC
<0.0026
0.040
0.020
0.0026
ug/L
04/20/18 14:25
1
beta-BHC
<0.010
0.040
0.020
0.010
ug/L
04/20/18 14:25
1
delta-BHC
<0.010 *
0.040
0.020
0.010
ug/L
04/20/18 14:25
1
gamma-BHC (Lindane)
<0.0056
0.040
0.020
0.0056
ug/L
04/20/18 14:25
1
Heptachlor
<0.013
0.040
0.020
0.013
ug/L
04/20/18 14:25
1
Aldrin
<0.0053 "
0.040
0.020
0.0053
ug/L
04/20/18 14:25
1
Heptachlor epoxide
<0.014
0.040
0.020
0.014
ug/L
04/20/18 14:25
1
Endosulfan 1
<0.0041
0.040
0.020
0.0041
ug/L
04/20/18 14:25
1
TestAmerica Chicago
Page 161 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg
Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Client Sample ID: MW11 D(i)
Lab Sample ID: 500-143858-31
Date Collected: 04/12/18 12:00
Matrix:
Water
Date Received: 04/18/18 09:10
Method: 8081B - Organochlorine
Pesticides (GC) (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Dieldrin
<0.013
0.040
0.020
0.013
ug/L
04/20/18 14:25
1
4,4'-DDE
<0.0038
0.040
0.020
0.0038
ug/L
04/20/18 14:25
1
Endrin
<0.014
0.040
0.020
0.014
ug/L
04/20/18 14:25
1
Endosulfan II
<0.0028
0.040
0.020
0.0028
ug/L
04/20/18 14:25
1
4,4'-DDD
<0.013
0.040
0.020
0.013
ug/L
04/20/18 14:25
1
Endosulfan sulfate
<0.012
0.040
0.020
0.012
ug/L
04/20/18 14:25
1
4,4'-DDT
<0.0032
0.040
0.020
0.0032
ug/L
04/20/18 14:25
1
Methoxychlor
<0.023
0.079
0.040
0.023
ug/L
04/20/18 14:25
1
Toxaphene
<0.20
0.40
0.20
0.20
ug/L
04/20/18 14:25
1
Endrin aldehyde
<0.0081
0.040
0.020
0.0081
ug/L
04/20/18 14:25
1
Chlordane (technical)
<0.040
0.079
0.040
0.040
ug/L
04/20/18 14:25
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
87
30 - 130
04119118 07:40
04120118 14:25
1
Tetrachloro-m-xylene
102
30 - 120
04119118 07:40
04120118 14:25
1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
E:
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
PCB-1016
<0.066
0.40
0.20
0.066
ug/L
04/19/18 17:01
1
PCB-1221
<0.20
0.40
0.20
0.20
ug/L
04/19/18 17:01
1
PCB-1232
<0.20
0.40
0.20
0.20
ug/L
04/19/18 17:01
1
PCB-1242
<0.20
0.40
0.20
0.20
ug/L
04/19/18 17:01
1
PCB-1248
<0.20
0.40
0.20
0.20
ug/L
04/19/18 17:01
1
PCB-1254
<0.20
0.40
0.20
0.20
ug/L
04/19/18 17:01
1
PCB-1260
1.1
0.40
0.20
0.069
ug/L
04/19/18 17:01
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene
71
30 - 120
04119118 07:40
04119118 17:01
1
DCB Decachlorobiphenyl
84
30 - 140
04119118 07:40
04119118 17:01
1
Method: 8151A - Herbicides (GC)
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
2,4-D
<0.47
1.0
0.51
0.47
ug/L
04/19/18 06:32
1
Dinoseb
<0.17
2.0
1.0
0.17
ug/L
04/19/18 06:32
1
Pentachlorophenol
<0.091
0.51
0.10
0.091
ug/L
04/19/18 06:32
1
Silvex (2,4,5-TP)
<0.29
1.0
0.51
0.29
ug/L
04/19/18 06:32
1
2,4,5-T
<0.44
1.0
0.51
0.44
ug/L
04/19/18 06:32
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCAA
62
25 - 130
04118118 11:15
04119118 06:32
1
Method: 6020B - Metals (ICP/MS) - Total Recoverable
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed
Dil Fac
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 05:17
1
Arsenic
2.7
1.0
0.50
0.23
ug/L
04/21/18 05:17
1
Barium
51
2.5
1.3
0.73
ug/L
04/21/18 05:17
1
Beryllium
<0.53
1.0
0.53
0.53
ug/L
04/21/18 05:17
1
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 05:17
1
Chromium
11
5.0
2.5
1.1
ug/L
04/21/18 05:17
1
Cobalt
<0.40
1.0
0.50
0.40
ug/L
04/21/18 05:17
1
Copper
2.4
2.0
1.0
0.50
ug/L
04/21/18 05:17
1
TestAmerica Chicago
Page 162 of 258 7/5/2018

Client Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill
- Infill
SDG: NCDEQ
Solid
Waste Facility = # 60-13
Client Sample ID: MW11 D(i)
Lab Sample
ID: 500-143858-31
Date Collected: 04/12/18 12:00
Matrix:
Water
Date Received: 04/18/18 09:10
Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Iron
<47
100
50
47
ug/L
04/21/18 05:17
1
Lead
<0.19
0.50
0.25
0.19
ug/L
04/21/18 05:17
1
Manganese
24
2.5
1.3
0.79
ug/L
04/21/18 05:17
1
Nickel
2.6
2.0
1.0
0.63
ug/L
04/21/18 05:17
1
Selenium
1.5 J
2.5
1.3
0.98
ug/L
04/21/18 05:17
1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 05:17
1
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 05:17
1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 05:17
1
Vanadium
10
5.0
2.5
2.2
ug/L
04/21/18 05:17
1
Zinc
8.1 J
10
20
6.9
ug/L
04/21/18 05:17
1
Method: 7470A - Mercury (CVAA)
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Mercury
<0.098
0.20
0.10
0.098
ug/L
04/20/1810:07
1
General Chemistry
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Cyanide, Total
<3.5
10
5.0
3.5
ug/L
04/25/18 09:54
1
Chloride
7100
400
340
340
ug/L
04/27/18 23:11
2
Sulfate
180000
4000
2000
1900
ug/L
04/26/18 23:00
20
Alkalinity
63000
5000
5000
3700
ug/L
04/24/1814:48
1
Total Dissolved Solids
390000
10000
10000
4300
ug/L
04/19/18 04:22
1
TestAmerica Chicago
Page 163 of 258 7/5/2018

Definitions/Glossary
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Qualifiers
GC/MS VOA
Qualifier Qualifier Description
cn Refer to Case Narrative for further detail
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
F2 MS/MSD RPD exceeds control limits
F1 MS and/or MSD Recovery is outside acceptance limits.
GUMS Semi VOA
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
X Surrogate is outside control limits
GC Semi VOA
Qualifier Qualifier Description
X Surrogate is outside control limits
RPD of the LCS and LCSD exceeds the control limits
LCS or LCSD is outside acceptance limits.
Metals
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
B Compound was found in the blank and sample.
F3 Duplicate RPD exceeds the control limit
General Chemistry
Qualifier Qualifier Description
B Compound was found in the blank and sample.
F1 MS and/or MSD Recovery is outside acceptance limits.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
tt Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
TestAmerica Chicago
Page 164 of 258 7/5/2018

Definitions/Glossary
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Glossary (Continued)
Abbreviation These commonly used abbreviations may or may not be present in this report.
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
0
TestAmerica Chicago
Page 165 of 258 7/5/2018

QC Association Summary
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
GC/MS VOA
Analysis Batch: 428709
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
500-143858-22
Duplicate
Total/NA
Water
8260B
500-143858-25
TB
Total/NA
Water
8260B
500-143858-26
TB
Total/NA
Water
8260B
500-143858-27
TB
Total/NA
Water
8260B
500-143858-28
TB
Total/NA
Water
8260B
500-143858-29
TB
Total/NA
Water
8260B
MB 500-428709/6
Method Blank
Total/NA
Water
8260B
LCS 500-428709/4
Lab Control Sample
Total/NA
Water
8260B
Analysis Batch: 428915
Prep Batch
0
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
500-143858-1
MW-12(i)
Total/NA
Water
8260B
500-143858-2
MW-14(i)
Total/NA
Water
8260B
500-143858-3
MW-15(i)
Total/NA
Water
8260B
500-143858-4
MW-16(i)
Total/NA
Water
8260B
500-143858-5
MW-1(i)
Total/NA
Water
8260B
500-143858-6
MW-13(i)
Total/NA
Water
8260B
500-143858-7
MW-12D(i)
Total/NA
Water
8260B
500-143858-8
MW-8D(i)
Total/NA
Water
8260B
500-143858-9
MW-5(i)
Total/NA
Water
8260B
500-143858-10
MW-9(i)
Total/NA
Water
8260B
500-143858-11
MW-9D(i)
Total/NA
Water
8260B
500-143858-12
MW-10(i)
Total/NA
Water
8260B
MB 500-428915/6
Method Blank
Total/NA
Water
8260B
LCS 500-428915/4
Lab Control Sample
Total/NA
Water
8260B
500-143858-12 MS
MW-10(i)
Total/NA
Water
8260B
500-143858-12 MSD
MW-10(i)
Total/NA
Water
8260B
Analysis Batch: 429099
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
500-143858-13
MW-8(i)
Total/NA
Water
8260B
500-143858-14
MW-2(i)
Total/NA
Water
8260B
500-143858-15
MW-3(i)
Total/NA
Water
8260B
500-143858-16
MW-4D(i)
Total/NA
Water
8260B
500-143858-18
MW-6(i)
Total/NA
Water
8260B
500-143858-19
MW-7D(i)
Total/NA
Water
8260B
500-143858-20
MW-5D(i)
Total/NA
Water
8260B
500-143858-23
Duplicate 1
Total/NA
Water
8260B
500-143858-30
MW11(i)
Total/NA
Water
8260B
500-143858-31
MW11D(i)
Total/NA
Water
8260B
MB 500-429099/6
Method Blank
Total/NA
Water
8260B
LCS 500-429099/4
Lab Control Sample
Total/NA
Water
8260B
500-143858-31 MS
MW11D(i)
Total/NA
Water
8260B
500-143858-31 MSD
MW11D(i)
Total/NA
Water
8260B
Analysis Batch: 429285
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
500-143858-17
MW-4(i)
Total/NA
Water
8260B
500-143858-21
MW-7(i)
Total/NA
Water
8260B
500-143858-23
Duplicate 1
Total/NA
Water
8260B
500-143858-24
Duplicate 2
Total/NA
Water
8260B
TestAmerica Chicago
Page 166 of 258 7/5/2018

QC Association Summary
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
GC/MS VOA (Continued)
Analysis Batch: 429285 (Continued)
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
MB 500-429285/20 Method Blank Total/NA Water 8260B
LCS 500-429285/4 Lab Control Sample Total/NA Water 8260B
GC/MS Semi VOA
Prep Batch: 428028
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
500-143858-1
MW-12(i)
Total/NA
Water
3510C
500-143858-2
MW-14(i)
Total/NA
Water
3510C
500-143858-5
MW-1(i)
Total/NA
Water
3510C
500-143858-6
MW-13(i)
Total/NA
Water
3510C
500-143858-7
MW-12D(i)
Total/NA
Water
3510C
500-143858-8
MW-8D(i)
Total/NA
Water
3510C
500-143858-9
MW-5(i)
Total/NA
Water
3510C
500-143858-10
MW-9(i)
Total/NA
Water
3510C
500-143858-11
MW-9D(i)
Total/NA
Water
3510C
500-143858-12
MW-10(i)
Total/NA
Water
3510C
500-143858-13
MW-8(i)
Total/NA
Water
3510C
500-143858-14
MW-2(i)
Total/NA
Water
3510C
500-143858-15
MW-3(i)
Total/NA
Water
3510C
500-143858-16
MW-4D(i)
Total/NA
Water
3510C
500-143858-17
MW-4(i)
Total/NA
Water
3510C
500-143858-18
MW-6(i)
Total/NA
Water
3510C
500-143858-19
MW-7D(i)
Total/NA
Water
3510C
500-143858-20
MW-5D(i)
Total/NA
Water
3510C
500-143858-21
MW-7(i)
Total/NA
Water
3510C
MB 500-428028/1-A
Method Blank
Total/NA
Water
3510C
LCS 500-428028/2-A
Lab Control Sample
Total/NA
Water
3510C
LCSD 500-428028/3-A
Lab Control Sample Dup
Total/NA
Water
3510C
Analysis Batch: 428171
Prep Batch
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-1
MW-12(i)
Total/NA
Water
8270D
428028
500-143858-2
MW-14(i)
Total/NA
Water
8270D
428028
500-143858-5
MW-1(i)
Total/NA
Water
8270D
428028
500-143858-6
MW-13(i)
Total/NA
Water
8270D
428028
500-143858-7
MW-12D(i)
Total/NA
Water
8270D
428028
500-143858-8
MW-8D(i)
Total/NA
Water
8270D
428028
500-143858-9
MW-5(i)
Total/NA
Water
8270D
428028
MB 500-428028/1-A
Method Blank
Total/NA
Water
8270D
428028
LCS 500-428028/2-A
Lab Control Sample
Total/NA
Water
8270D
428028
LCSD 500-428028/3-A
Lab Control Sample Dup
Total/NA
Water
8270D
428028
Prep Batch: 428463
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-30
MW11(i)
Total/NA
Water
3510C
500-143858-31
MW11D(i)
Total/NA
Water
3510C
MB 500-428463/1-A
Method Blank
Total/NA
Water
3510C
LCS 500-428463/2-A
Lab Control Sample
Total/NA
Water
3510C
LCSD 500-428463/3-A
Lab Control Sample Dup
Total/NA
Water
3510C
0
TestAmerica Chicago
Page 167 of 258 7/5/2018

QC Association Summary
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
GC/MS Semi VOA (Continued)
Analysis Batch: 428521
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-11
MW-9D(i)
Total/NA
Water
8270D
428028
500-143858-19
MW-7D(i)
Total/NA
Water
8270D
428028
MB 500-428463/1-A
Method Blank
Total/NA
Water
8270D
428463
LCS 500-428463/2-A
Lab Control Sample
Total/NA
Water
8270D
428463
LCSD 500-428463/3-A
Lab Control Sample Dup
Total/NA
Water
8270D
428463
Analysis Batch: 428757
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-10
MW-9(i)
Total/NA
Water
8270D
428028
500-143858-12
MW-10(i)
Total/NA
Water
8270D
•
428028
500-143858-13
MW-8(i)
Total/NA
Water
8270D
428028
500-143858-14
MW-2(i)
Total/NA
Water
8270D
428028
500-143858-15
MW-3(i)
Total/NA
Water
8270D
428028
500-143858-16
MW-4D(i)
Total/NA
Water
8270D
428028
500-143858-17
MW-4(i)
Total/NA
Water
8270D
428028
500-143858-18
MW-6(i)
Total/NA
Water
8270D
428028
500-143858-20
MW-5D(i)
Total/NA
Water
8270D
428028
500-143858-21
MW-7(i)
Total/NA
Water
8270D
428028
500-143858-30
MW11(i)
Total/NA
Water
8270D
428463
500-143858-31
MW11D(i)
Total/NA
Water
8270D
428463
GC Semi VOA
Analysis Batch: 427712
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-1
MW-12(i)
Total/NA
Water
8151A
428120
500-143858-2
MW-14(i)
Total/NA
Water
8151A
428120
500-143858-5
MW-1(i)
Total/NA
Water
8151A
428120
500-143858-6
MW-13(i)
Total/NA
Water
8151A
428120
500-143858-7
MW-12D(i)
Total/NA
Water
8151A
428120
500-143858-8
MW-8D(i)
Total/NA
Water
8151A
428120
500-143858-9
MW-5(i)
Total/NA
Water
8151A
428120
500-143858-10
MW-9(i)
Total/NA
Water
8151A
428120
500-143858-11
MW-9D(i)
Total/NA
Water
8151A
428120
500-143858-12
MW-10(i)
Total/NA
Water
8151A
428120
500-143858-13
MW-8(i)
Total/NA
Water
8151A
428120
500-143858-14
MW-2(i)
Total/NA
Water
8151A
428120
500-143858-15
MW-3(i)
Total/NA
Water
8151A
428120
500-143858-16
MW-4D(i)
Total/NA
Water
8151A
428120
500-143858-17
MW-4(i)
Total/NA
Water
8151A
428120
500-143858-18
MW-6(i)
Total/NA
Water
8151A
428120
500-143858-19
MW-7D(i)
Total/NA
Water
8151A
428120
MB 500-428120/1-A
Method Blank
Total/NA
Water
8151A
428120
LCS 500-428120/2-A
Lab Control Sample
Total/NA
Water
8151A
428120
LCSD 500-428120/3-A
Lab Control Sample Dup
Total/NA
Water
8151A
428120
Prep Batch: 428097
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-1
MW-12(i)
Total/NA
Water
3510C
500-143858-2
MW-14(i)
Total/NA
Water
3510C
TestAmerica Chicago
Page 168 of 258 7/5/2018

QC Association Summary
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID:
500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ Solid Waste Facility = # 60-13
GC Semi VOA (Continued)
Prep Batch: 428097 (Continued)
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-5
MW-1(i)
Total/NA
Water
3510C
500-143858-6
MW-13(i)
Total/NA
Water
3510C
500-143858-7
MW-12D(i)
Total/NA
Water
3510C
500-143858-8
MW-8D(i)
Total/NA
Water
3510C
500-143858-9
MW-5(i)
Total/NA
Water
3510C
500-143858-10
MW-9(i)
Total/NA
Water
3510C
500-143858-11
MW-9D(i)
Total/NA
Water
3510C
500-143858-12
MW-10(i)
Total/NA
Water
3510C
500-143858-13
MW-8(i)
Total/NA
Water
3510C
500-143858-14
MW-2(i)
Total/NA
Water
3510C
•
500-143858-15
MW-3(i)
Total/NA
Water
3510C
500-143858-16
MW-4D(i)
Total/NA
Water
3510C
500-143858-17
MW-4(i)
Total/NA
Water
3510C
500-143858-18
MW-6(i)
Total/NA
Water
3510C
500-143858-19
MW-7D(i)
Total/NA
Water
3510C
500-143858-20
MW-5D(i)
Total/NA
Water
3510C
500-143858-21
MW-7(i)
Total/NA
Water
3510C
MB 500-428097/1-A
Method Blank
Total/NA
Water
3510C
LCS 500-428097/2-A
Lab Control Sample
Total/NA
Water
3510C
LCS 500-428097/4-A
Lab Control Sample
Total/NA
Water
3510C
LCSD 500-428097/3-A
Lab Control Sample Dup
Total/NA
Water
3510C
LCSD 500-428097/5-A
Lab Control Sample Dup
Total/NA
Water
3510C
Prep Batch: 428120
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-1
MW-12(i)
Total/NA
Water
8151A
500-143858-2
MW-14(i)
Total/NA
Water
8151A
500-143858-5
MW-1(i)
Total/NA
Water
8151A
500-143858-6
MW-13(i)
Total/NA
Water
8151A
500-143858-7
MW-12D(i)
Total/NA
Water
8151A
500-143858-8
MW-8D(i)
Total/NA
Water
8151A
500-143858-9
MW-5(i)
Total/NA
Water
8151A
500-143858-10
MW-9(i)
Total/NA
Water
8151A
500-143858-11
MW-9D(i)
Total/NA
Water
8151A
500-143858-12
MW-10(i)
Total/NA
Water
8151A
500-143858-13
MW-8(i)
Total/NA
Water
8151A
500-143858-14
MW-2(i)
Total/NA
Water
8151A
500-143858-15
MW-3(i)
Total/NA
Water
8151A
500-143858-16
MW-4D(i)
Total/NA
Water
8151A
500-143858-17
MW-4(i)
Total/NA
Water
8151A
500-143858-18
MW-6(i)
Total/NA
Water
8151A
500-143858-19
MW-7D(i)
Total/NA
Water
8151A
MB 500-428120/1-A
Method Blank
Total/NA
Water
8151A
LCS 500-428120/2-A
Lab Control Sample
Total/NA
Water
8151A
LCSD 500-428120/3-A
Lab Control Sample Dup
Total/NA
Water
8151A
Analysis Batch: 428222
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-1
MW-12(i)
Total/NA
Water
8082A
428097
500-143858-2
MW-14(i)
Total/NA
Water
8082A
428097
500-143858-5
MW-1(i)
Total/NA
Water
8082A
428097
TestAmerica Chicago
Page 169 of 258 7/5/2018

QC Association Summary
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
GC Semi VOA (Continued)
Analysis Batch: 428222 (Continued)
Lab Sample ID
Client Sample ID
500-143858-6
MW-13(i)
500-143858-7
MW-12D(i)
500-143858-8
MW-8D(i)
500-143858-9
MW-5(i)
500-143858-10
MW-9(i)
500-143858-11
MW-9D(i)
500-143858-12
MW-10(i)
500-143858-13
MW-8(i)
500-143858-14
MW-2(i)
500-143858-15
MW-3(i)
500-143858-16
MW-4D(i)
500-143858-17
MW-4(i)
500-143858-18
MW-6(i)
500-143858-19
MW-7D(i)
500-143858-20
MW-5D(i)
500-143858-21
MW-7(i)
MB 500-428097/1-A
Method Blank
LCS 500-428097/4-A
Lab Control Sample
LCSD 500-428097/5-A
Lab Control Sample Dup
Prep Batch: 428351
Lab Sample ID
500-143858-20
500-143858-21
500-143858-30
500-143858-31
MB 500-428351/1-A
LCS 500-428351/2-A
LCSD 500-428351/3-A
Analysis Batch: 428477
Lab Sample ID
500-143858-20
500-143858-21
500-143858-30
500-143858-31
MB 500-428351/1-A
LCS 500-428351/2-A
LCSD 500-428351/3-A
Prep Batch: 428495
Lab Sample ID
500-143858-30
500-143858-31
MB 500-428495/1-A
LCS 500-428495/2-A
LCS 500-428495/4-A
LCSD 500-428495/3-A
LCSD 500-428495/5-A
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Prep Type
Matrix
Method
Prep Batch
Total/NA
Water
8082A
428097
Total/NA
Water
8082A
428097
Total/NA
Water
8082A
428097
Total/NA
Water
8082A
428097
Total/NA
Water
8082A
428097
Total/NA
Water
8082A
428097
Total/NA
Water
8082A
428097
Total/NA
Water
8082A
428097
Total/NA
Water
8082A
428097
Total/NA
Water
8082A
428097
Total/NA
Water
8082A
428097
Total/NA
Water
8082A
428097
Total/NA
Water
8082A
428097
Total/NA
Water
8082A
428097
Total/NA
Water
8082A
428097
Total/NA
Water
8082A
428097
Total/NA
Water
8082A
428097
Total/NA
Water
8082A
428097
Total/NA
Water
8082A
428097
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
MW-5D(i)
Total/NA
Water
8151A
MW-7(i)
Total/NA
Water
8151A
MW11(i)
Total/NA
Water
8151A
MW11D(i)
Total/NA
Water
8151A
Method Blank
Total/NA
Water
8151A
Lab Control Sample
Total/NA
Water
8151A
Lab Control Sample Dup
Total/NA
Water
8151A
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
MW-5D(i)
Total/NA
Water
8151A
428351
MW-7(i)
Total/NA
Water
8151A
428351
MW11(i)
Total/NA
Water
8151A
428351
MW11D(i)
Total/NA
Water
8151A
428351
Method Blank
Total/NA
Water
8151A
428351
Lab Control Sample
Total/NA
Water
8151A
428351
Lab Control Sample Dup
Total/NA
Water
8151A
428351
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
MW11(i)
Total/NA
Water
3510C
MW11D(i)
Total/NA
Water
3510C
Method Blank
Total/NA
Water
3510C
Lab Control Sample
Total/NA
Water
3510C
Lab Control Sample
Total/NA
Water
3510C
Lab Control Sample Dup
Total/NA
Water
3510C
Lab Control Sample Dup
Total/NA
Water
3510C
0
Page 170 of 258
TestAmerica Chicago
7/5/2018

QC Association Summary
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
GC Semi VOA (Continued)
Analysis Batch: 428535
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-1
MW-12(i)
Total/NA
Water
8081B
428097
500-143858-2
MW-14(i)
Total/NA
Water
8081B
428097
500-143858-5
MW-1(i)
Total/NA
Water
8081 B
428097
500-143858-6
MW-13(i)
Total/NA
Water
8081B
428097
500-143858-7
MW-12D(i)
Total/NA
Water
8081B
428097
MB 500-428097/1-A
Method Blank
Total/NA
Water
8081B
428097
LCS 500-428097/2-A
Lab Control Sample
Total/NA
Water
8081 B
428097
LCSD 500-428097/3-A
Lab Control Sample Dup
Total/NA
Water
8081B
428097
Analysis Batch: 428582
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-30
MW11(i)
Total/NA
Water
8082A
428495
500-143858-31
MW11D(i)
Total/NA
Water
8082A
428495
MB 500-428495/1-A
Method Blank
Total/NA
Water
8082A
428495
LCS 500-428495/4-A
Lab Control Sample
Total/NA
Water
8082A
428495
LCSD 500-428495/5-A
Lab Control Sample Dup
Total/NA
Water
8082A
428495
Analysis Batch: 428753
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-8
MW-8D(i)
Total/NA
Water
8081B
428097
500-143858-9
MW-5(i)
Total/NA
Water
8081B
428097
500-143858-10
MW-9(i)
Total/NA
Water
8081B
428097
500-143858-11
MW-9D(i)
Total/NA
Water
8081B
428097
500-143858-12
MW-10(i)
Total/NA
Water
8081B
428097
500-143858-13
MW-8(i)
Total/NA
Water
8081B
428097
500-143858-14
MW-2(i)
Total/NA
Water
8081E
428097
500-143858-15
MW-3(i)
Total/NA
Water
8081E
428097
500-143858-16
MW-4D(i)
Total/NA
Water
8081E
428097
500-143858-17
MW-4(i)
Total/NA
Water
8081E
428097
500-143858-18
MW-6(i)
Total/NA
Water
8081E
428097
500-143858-19
MW-7D(i)
Total/NA
Water
8081E
428097
500-143858-20
MW-5D(i)
Total/NA
Water
8081E
428097
500-143858-30
MW11(i)
Total/NA
Water
8081E
428495
500-143858-31
MW11D(i)
Total/NA
Water
8081E
428495
MB 500-428495/1-A
Method Blank
Total/NA
Water
8081B
428495
LCS 500-428495/2-A
Lab Control Sample
Total/NA
Water
8081B
428495
LCSD 500-428495/3-A
Lab Control Sample Dup
Total/NA
Water
8081B
428495
Analysis Batch: 429503
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
500-143858-21
MW-7(i)
Total/NA
Water
8081E 428097
Metals
Prep Batch: 428144
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
500-143858-1
MW-12(i)
Total/NA
Water
7470A
500-143858-2
MW-14(i)
Total/NA
Water
7470A
500-143858-4
MW-16(i)
Total/NA
Water
7470A
500-143858-6
MW-13(i)
Total/NA
Water
7470A
TestAmerica Chicago
Page 171 of 258 7/5/2018

QC Association Summary
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID:
500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ Solid Waste Facility = # 60-13
Metals (Continued)
Prep Batch: 428144 (Continued)
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-7
MW-12D(i)
Total/NA
Water
7470A
500-143858-8
MW-8D(i)
Total/NA
Water
7470A
500-143858-9
MW-5(i)
Total/NA
Water
7470A
500-143858-10
MW-9(i)
Total/NA
Water
7470A
500-143858-11
MW-9D(i)
Total/NA
Water
7470A
500-143858-13
MW-8(i)
Total/NA
Water
7470A
500-143858-14
MW-2(i)
Total/NA
Water
7470A
500-143858-15
MW-3(i)
Total/NA
Water
7470A
500-143858-16
MW-4D(i)
Total/NA
Water
7470A
500-143858-17
MW-4(i)
Total/NA
Water
7470A
•
500-143858-18
MW-6(i)
Total/NA
Water
7470A
500-143858-19
MW-7D(i)
Total/NA
Water
7470A
500-143858-20
MW-5D(i)
Total/NA
Water
7470A
500-143858-21
MW-7(i)
Total/NA
Water
7470A
MB 500-428144/12-A
Method Blank
Total/NA
Water
7470A
LCS 500-428144/13-A
Lab Control Sample
Total/NA
Water
7470A
500-143858-1 MS
MW-12(i)
Total/NA
Water
7470A
500-143858-1 MSD
MW-12(i)
Total/NA
Water
7470A
500-143858-1 DU
MW-12(i)
Total/NA
Water
7470A
Prep Batch: 428299
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-1
MW-12(i)
Total Recoverable
Water
3005A
500-143858-2
MW-14(i)
Total Recoverable
Water
3005A
500-143858-4
MW-16(i)
Total Recoverable
Water
3005A
500-143858-6
MW-13(i)
Total Recoverable
Water
3005A
500-143858-7
MW-12D(i)
Total Recoverable
Water
3005A
500-143858-8
MW-8D(i)
Total Recoverable
Water
3005A
500-143858-9
MW-5(i)
Total Recoverable
Water
3005A
500-143858-10
MW-9(i)
Total Recoverable
Water
3005A
500-143858-11
MW-9D(i)
Total Recoverable
Water
3005A
500-143858-13
MW-8(i)
Total Recoverable
Water
3005A
500-143858-14
MW-2(i)
Total Recoverable
Water
3005A
500-143858-15
MW-3(i)
Total Recoverable
Water
3005A
500-143858-16
MW-4D(i)
Total Recoverable
Water
3005A
500-143858-17
MW-4(i)
Total Recoverable
Water
3005A
500-143858-18
MW-6(i)
Total Recoverable
Water
3005A
500-143858-19
MW-7D(i)
Total Recoverable
Water
3005A
500-143858-20
MW-5D(i)
Total Recoverable
Water
3005A
500-143858-21
MW-7(i)
Total Recoverable
Water
3005A
MB 500-428299/1-A
Method Blank
Total Recoverable
Water
3005A
LCS 500-428299/2-A
Lab Control Sample
Total Recoverable
Water
3005A
500-143858-13 MS
MW-8(i)
Total Recoverable
Water
3005A
500-143858-13 MSD
MW-8(i)
Total Recoverable
Water
3005A
500-143858-13 DU
MW-8(i)
Total Recoverable
Water
3005A
Analysis Batch: 428374
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-1
MW-12(i)
Total/NA
Water
7470A
428144
500-143858-2
MW-14(i)
Total/NA
Water
7470A
428144
500-143858-4
MW-16(i)
Total/NA
Water
7470A
428144
TestAmerica Chicago
Page 172 of 258 7/5/2018

QC Association Summary
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID:
500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ Solid Waste Facility = # 60-13
Metals (Continued)
Analysis Batch: 428374
(Continued)
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-6
MW-13(i)
Total/NA
Water
7470A
428144
500-143858-7
MW-12D(i)
Total/NA
Water
7470A
428144
500-143858-8
MW-8D(i)
Total/NA
Water
7470A
428144
500-143858-9
MW-5(i)
Total/NA
Water
7470A
428144
500-143858-10
MW-9(i)
Total/NA
Water
7470A
428144
500-143858-11
MW-9D(i)
Total/NA
Water
7470A
428144
500-143858-13
MW-8(i)
Total/NA
Water
7470A
428144
500-143858-14
MW-2(i)
Total/NA
Water
7470A
428144
500-143858-15
MW-3(i)
Total/NA
Water
7470A
428144
500-143858-16
MW-4D(i)
Total/NA
Water
7470A
•
428144
500-143858-17
MW-4(i)
Total/NA
Water
7470A
428144
500-143858-18
MW-6(i)
Total/NA
Water
7470A
428144
500-143858-19
MW-7D(i)
Total/NA
Water
7470A
428144
500-143858-20
MW-5D(i)
Total/NA
Water
7470A
428144
500-143858-21
MW-7(i)
Total/NA
Water
7470A
428144
MB 500-428144/12-A
Method Blank
Total/NA
Water
7470A
428144
LCS 500-428144/13-A
Lab Control Sample
Total/NA
Water
7470A
428144
500-143858-1 MS
MW-12(i)
Total/NA
Water
7470A
428144
500-143858-1 MSD
MW-12(i)
Total/NA
Water
7470A
428144
500-143858-1 DU
MW-12(i)
Total/NA
Water
7470A
428144
Prep Batch: 428456
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-1
MW-12(i)
Dissolved
Water
3005A
500-143858-2
MW-14(i)
Dissolved
Water
3005A
500-143858-6
MW-13(i)
Dissolved
Water
3005A
500-143858-7
MW-12D(i)
Dissolved
Water
3005A
500-143858-30
MW11(i)
Total Recoverable
Water
3005A
500-143858-31
MW11D(i)
Total Recoverable
Water
3005A
MB 500-428456/1-A
Method Blank
Total Recoverable
Water
3005A
LCS 500-428456/2-A
Lab Control Sample
Total Recoverable
Water
3005A
500-143858-1 MS
MW-12(i)
Dissolved
Water
3005A
500-143858-1 MSD
MW-12(i)
Dissolved
Water
3005A
500-143858-1 DU
MW-12(i)
Dissolved
Water
3005A
Prep Batch: 428588
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-1
MW-12(i)
Dissolved
Water
7470A
500-143858-2
MW-14(i)
Dissolved
Water
7470A
500-143858-6
MW-13(i)
Dissolved
Water
7470A
500-143858-7
MW-12D(i)
Dissolved
Water
7470A
500-143858-30
MW11(i)
Total/NA
Water
7470A
500-143858-31
MW11D(i)
Total/NA
Water
7470A
MB 500-428588/12-A
Method Blank
Total/NA
Water
7470A
LCS 500-428588/13-A
Lab Control Sample
Total/NA
Water
7470A
Analysis Batch: 428749
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-1
MW-12(i)
Dissolved
Water
7470A
428588
500-143858-2
MW-14(i)
Dissolved
Water
7470A
428588
500-143858-6
MW-13(i)
Dissolved
Water
7470A
428588
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Page 173 of 258 7/5/2018

QC Association Summary
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Metals (Continued)
Analysis Batch: 428749 (Continued)
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-7
MW-12D(i)
Dissolved
Water
7470A
428588
500-143858-30
MW11(i)
Total/NA
Water
7470A
428588
500-143858-31
MW11D(i)
Total/NA
Water
7470A
428588
MB 500-428588/12-A
Method Blank
Total/NA
Water
7470A
428588
LCS 500-428588/13-A
Lab Control Sample
Total/NA
Water
7470A
428588
Analysis Batch: 428958
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-1
MW-12(i)
Dissolved
Water
6020B
428456
500-143858-1
MW-12(i)
Total Recoverable
Water
6020B
•
428299
500-143858-2
MW-14(i)
Dissolved
Water
6020B
428456
500-143858-2
MW-14(i)
Total Recoverable
Water
6020B
428299
500-143858-4
MW-16(i)
Total Recoverable
Water
6020B
428299
500-143858-6
MW-13(i)
Dissolved
Water
6020B
428456
500-143858-6
MW-13(i)
Total Recoverable
Water
6020E
428299
500-143858-7
MW-12D(i)
Dissolved
Water
6020E
428456
500-143858-7
MW-12D(i)
Total Recoverable
Water
6020E
428299
500-143858-8
MW-8D(i)
Total Recoverable
Water
6020B
428299
500-143858-9
MW-5(i)
Total Recoverable
Water
6020B
428299
500-143858-10
MW-9(i)
Total Recoverable
Water
6020B
428299
500-143858-11
MW-9D(i)
Total Recoverable
Water
6020E
428299
500-143858-13
MW-8(i)
Total Recoverable
Water
6020E
428299
500-143858-14
MW-2(i)
Total Recoverable
Water
6020E
428299
500-143858-15
MW-3(i)
Total Recoverable
Water
6020B
428299
500-143858-16
MW-4D(i)
Total Recoverable
Water
6020B
428299
500-143858-17
MW-4(i)
Total Recoverable
Water
6020B
428299
500-143858-18
MW-6(i)
Total Recoverable
Water
6020B
428299
500-143858-19
MW-7D(i)
Total Recoverable
Water
6020B
428299
500-143858-20
MW-5D(i)
Total Recoverable
Water
6020B
428299
500-143858-21
MW-7(i)
Total Recoverable
Water
6020E
428299
500-143858-30
MW11(i)
Total Recoverable
Water
6020E
428456
500-143858-31
MW11D(i)
Total Recoverable
Water
6020E
428456
MB 500-428299/1-A
Method Blank
Total Recoverable
Water
6020E
428299
MB 500-428456/1-A
Method Blank
Total Recoverable
Water
6020E
428456
LCS 500-428299/2-A
Lab Control Sample
Total Recoverable
Water
6020E
428299
LCS 500-428456/2-A
Lab Control Sample
Total Recoverable
Water
6020E
428456
500-143858-1 MS
MW-12(i)
Dissolved
Water
6020E
428456
500-143858-1 MSD
MW-12(i)
Dissolved
Water
6020E
428456
500-143858-13 MS
MW-8(i)
Total Recoverable
Water
6020B
428299
500-143858-13 MSD
MW-8(i)
Total Recoverable
Water
6020B
428299
500-143858-1 DU
MW-12(i)
Dissolved
Water
6020B
428456
500-143858-13 DU
MW-8(i)
Total Recoverable
Water
6020E
428299
General Chemistry
Analysis Batch: 428116
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-1
MW-12(i)
Total/NA
Water
SM 2540C
500-143858-2
MW-14(i)
Total/NA
Water
SM 2540C
500-143858-3
MW-15(i)
Total/NA
Water
SM 2540C
TestAmerica Chicago
Page 174 of 258 7/5/2018

QC Association Summary
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
General Chemistry (Continued)
Analysis Batch: 428116 (Continued)
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-4
MW-16(i)
Total/NA
Water
SM 2540C
500-143858-5
MW-1(i)
Total/NA
Water
SM 2540C
500-143858-6
MW-13(i)
Total/NA
Water
SM 2540C
500-143858-7
MW-12D(i)
Total/NA
Water
SM 2540C
500-143858-8
MW-8D(i)
Total/NA
Water
SM 2540C
500-143858-9
MW-5(i)
Total/NA
Water
SM 2540C
500-143858-10
MW-9(i)
Total/NA
Water
SM 2540C
500-143858-11
MW-9D(i)
Total/NA
Water
SM 2540C
500-143858-12
MW-10(i)
Total/NA
Water
SM 2540C
500-143858-13
MW-8(i)
Total/NA
Water
SM 2540C
•
500-143858-14
MW-2(i)
Total/NA
Water
SM 2540C
500-143858-15
MW-3(i)
Total/NA
Water
SM 2540C
500-143858-16
MW-4D(i)
Total/NA
Water
SM 2540C
500-143858-17
MW-4(i)
Total/NA
Water
SM 2540C
MB 500-428116/1
Method Blank
Total/NA
Water
SM 2540C
LCS 500-428116/2
Lab Control Sample
Total/NA
Water
SM 2540C
500-143858-1 DU
MW-12(i)
Total/NA
Water
SM 2540C
Analysis Batch: 428281
C
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-18
MW-6(i)
Total/NA
Water
SM 2540C
500-143858-19
MW-7D(i)
Total/NA
Water
SM 2540C
500-143858-20
MW-5D(i)
Total/NA
Water
SM 2540C
500-143858-21
MW-7(i)
Total/NA
Water
SM 2540C
MB 500-428281/1
Method Blank
Total/NA
Water
SM 2540C
LCS 500-428281/2
Lab Control Sample
Total/NA
Water
SM 2540C
Analysis Batch: 428478
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-30
MW11(i)
Total/NA
Water
SM 2540C
500-143858-31
MW11D(i)
Total/NA
Water
SM 2540C
MB 500-428478/1
Method Blank
Total/NA
Water
SM 2540C
LCS 500-428478/2
Lab Control Sample
Total/NA
Water
SM 2540C
Analysis Batch: 429134
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-1
MW-12(i)
Total/NA
Water
SM 2320B
500-143858-3
MW-15(i)
Total/NA
Water
SM 2320B
500-143858-5
MW-1(i)
Total/NA
Water
SM 2320B
500-143858-6
MW-13(i)
Total/NA
Water
SM 2320B
500-143858-7
MW-12D(i)
Total/NA
Water
SM 2320B
500-143858-8
MW-8D(i)
Total/NA
Water
SM 2320B
500-143858-9
MW-5(i)
Total/NA
Water
SM 2320B
500-143858-10
MW-9(i)
Total/NA
Water
SM 2320B
500-143858-11
MW-9D(i)
Total/NA
Water
SM 2320B
500-143858-12
MW-10(i)
Total/NA
Water
SM 2320B
500-143858-13
MW-8(i)
Total/NA
Water
SM 2320B
500-143858-18
MW-6(i)
Total/NA
Water
SM 2320B
500-143858-19
MW-7D(i)
Total/NA
Water
SM 2320B
500-143858-20
MW-5D(i)
Total/NA
Water
SM 2320B
500-143858-21
MW-7(i)
Total/NA
Water
SM 2320B
TestAmerica Chicago
Page 175 of 258 7/5/2018

QC Association Summary
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID:
500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ Solid Waste Facility = # 60-13
General Chemistry (Continued)
Analysis Batch: 429134
(Continued)
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
MB 500-429134/3
Method Blank
Total/NA
Water
SM 2320B
LCS 500-429134/4
Lab Control Sample
Total/NA
Water
SM 2320B
500-143858-1 DU
MW-12(i)
Total/NA
Water
SM 2320B
Prep Batch: 429136
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-1
MW-12(i)
Total/NA
Water
9010B
500-143858-5
MW-1(i)
Total/NA
Water
9010B
500-143858-6
MW-13(i)
Total/NA
Water
9010B
500-143858-7
MW-12D(i)
Total/NA
Water
9010B
•
500-143858-10
MW-9(i)
Total/NA
Water
9010B
500-143858-11
MW-9D(i)
Total/NA
Water
9010B
500-143858-13
MW-8(i)
Total/NA
Water
9010B
MB 500-429136/1-A
Method Blank
Total/NA
Water
9010B
LCS 500-429136/2-A
Lab Control Sample
Total/NA
Water
9010B
500-143858-1 MS
MW-12(i)
Total/NA
Water
9010B
500-143858-1 MSD
MW-12(i)
Total/NA
Water
9010B
Prep Batch: 429175
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-2
MW-14(i)
Total/NA
Water
9010B
500-143858-8
MW-8D(i)
Total/NA
Water
9010B
500-143858-9
MW-5(i)
Total/NA
Water
9010B
500-143858-12
MW-10(i)
Total/NA
Water
9010B
500-143858-14
MW-2(i)
Total/NA
Water
9010B
500-143858-15
MW-3(i)
Total/NA
Water
9010B
500-143858-16
MW-4D(i)
Total/NA
Water
9010B
500-143858-17
MW-4(i)
Total/NA
Water
9010B
500-143858-18
MW-6(i)
Total/NA
Water
9010B
500-143858-19
MW-7D(i)
Total/NA
Water
9010B
500-143858-20
MW-5D(i)
Total/NA
Water
9010B
500-143858-21
MW-7(i)
Total/NA
Water
9010B
500-143858-30
MW11(i)
Total/NA
Water
9010B
500-143858-31
MW11D(i)
Total/NA
Water
9010B
MB 500-429175/1-A
Method Blank
Total/NA
Water
9010B
LCS 500-429175/2-A
Lab Control Sample
Total/NA
Water
9010B
500-143858-31 MS
MW11D(i)
Total/NA
Water
9010B
500-143858-31 MSD
MW11D(i)
Total/NA
Water
9010B
Analysis Batch: 429232
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-1
MW-12(i)
Total/NA
Water
9014
429136
500-143858-5
MW-1(i)
Total/NA
Water
9014
429136
500-143858-6
MW-13(i)
Total/NA
Water
9014
429136
500-143858-7
MW-12D(i)
Total/NA
Water
9014
429136
500-143858-10
MW-9(i)
Total/NA
Water
9014
429136
500-143858-11
MW-9D(i)
Total/NA
Water
9014
429136
500-143858-13
MW-8(i)
Total/NA
Water
9014
429136
MB 500-429136/1-A
Method Blank
Total/NA
Water
9014
429136
LCS 500-429136/2-A
Lab Control Sample
Total/NA
Water
9014
429136
500-143858-1 MS
MW-12(i)
Total/NA
Water
9014
429136
TestAmerica Chicago
Page 176 of 258 7/5/2018

QC Association Summary
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID:
500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ Solid Waste Facility = # 60-13
General Chemistry (Continued)
Analysis Batch: 429232
(Continued)
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-1 MSD
MW-12(i)
Total/NA
Water
9014
429136
Analysis Batch: 429325
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-2
MW-14(i)
Total/NA
Water
SM 2320B
500-143858-4
MW-16(i)
Total/NA
Water
SM 2320B
500-143858-14
MW-2(i)
Total/NA
Water
SM 2320B
500-143858-15
MW-3(i)
Total/NA
Water
SM 2320B
500-143858-16
MW-4D(i)
Total/NA
Water
SM 2320B
500-143858-17
MW-4(i)
Total/NA
Water
SM 2320B
•
500-143858-30
MW11(i)
Total/NA
Water
SM 2320B
500-143858-31
MW11D(i)
Total/NA
Water
SM 2320B
MB 500-429325/3
Method Blank
Total/NA
Water
SM 2320B
LCS 500-429325/4
Lab Control Sample
Total/NA
Water
SM 2320B
Analysis Batch: 429363
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-2
MW-14(i)
Total/NA
Water
9014
429175
500-143858-8
MW-8D(i)
Total/NA
Water
9014
429175
500-143858-9
MW-5(i)
Total/NA
Water
9014
429175
500-143858-12
MW-10(i)
Total/NA
Water
9014
429175
500-143858-14
MW-2(i)
Total/NA
Water
9014
429175
500-143858-15
MW-3(i)
Total/NA
Water
9014
429175
500-143858-16
MW-4D(i)
Total/NA
Water
9014
429175
500-143858-17
MW-4(i)
Total/NA
Water
9014
429175
500-143858-18
MW-6(i)
Total/NA
Water
9014
429175
500-143858-19
MW-7D(i)
Total/NA
Water
9014
429175
500-143858-20
MW-5D(i)
Total/NA
Water
9014
429175
500-143858-21
MW-7(i)
Total/NA
Water
9014
429175
500-143858-30
MW11(i)
Total/NA
Water
9014
429175
500-143858-31
MW11D(i)
Total/NA
Water
9014
429175
MB 500-429175/1-A
Method Blank
Total/NA
Water
9014
429175
LCS 500-429175/2-A
Lab Control Sample
Total/NA
Water
9014
429175
500-143858-31 MS
MW11D(i)
Total/NA
Water
9014
429175
500-143858-31 MSD
MW11D(i)
Total/NA
Water
9014
429175
Analysis Batch: 429672
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-143858-1
MW-12(i)
Total/NA
Water
9056A
500-143858-2
MW-14(i)
Total/NA
Water
9056A
500-143858-3
MW-15(i)
Total/NA
Water
9056A
500-143858-4
MW-16(i)
Total/NA
Water
9056A
500-143858-5
MW-1(i)
Total/NA
Water
9056A
500-143858-6
MW-13(i)
Total/NA
Water
9056A
500-143858-7
MW-12D(i)
Total/NA
Water
9056A
500-143858-8
MW-8D(i)
Total/NA
Water
9056A
MB 500-429672/4
Method Blank
Total/NA
Water
9056A
LCS 500-429672/5
Lab Control Sample
Total/NA
Water
9056A
500-143858-1 MS
MW-12(i)
Total/NA
Water
9056A
500-143858-1 MSD
MW-12(i)
Total/NA
Water
9056A
TestAmerica Chicago
Page 177 of 258 7/5/2018

QC Association Summary
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
General Chemistry (Continued)
Analysis Batch: 429675
Lab Sample ID
Client Sample ID
500-143858-9
MW-5(i)
500-143858-10
MW-9(i)
500-143858-11
MW-9D(i)
500-143858-13
MW-8(i)
500-143858-14
MW-2(i)
500-143858-15
MW-3(i)
500-143858-16
MW-4D(i)
500-143858-17
MW-4(i)
500-143858-18
MW-6(i)
500-143858-19
MW-7D(i)
500-143858-21
MW-7(i)
500-143858-30
MW11(i)
500-143858-31
MW11D(i)
MB 500-429675/12
Method Blank
LCS 500-429675/18
Lab Control Sample
500-143858-11 MS
MW-9D(i)
500-143858-11 MSD
MW-9D(i)
500-143858-31 MS
MW11D(i)
500-143858-31 MSD
MW11D(i)
Analysis Batch: 429810
Lab Sample ID
Client Sample ID
500-143858-1
MW-12(i)
500-143858-2
MW-14(i)
500-143858-3
MW-15(i)
500-143858-4
MW-16(i)
500-143858-5
MW-1(i)
500-143858-6
MW-13(i)
500-143858-7
MW-12D(i)
500-143858-8
MW-8D(i)
MB 500-429810/30
Method Blank
LCS 500-429810/4
Lab Control Sample
500-143858-1 MS
MW-12(i)
500-143858-1 MSD
MW-12(i)
Analysis Batch: 429826
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Prep Type
Matrix
Method Prep Batch
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
•
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Prep Type
Matrix
Method Prep Batch
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Lab Sample ID
Client Sample ID
500-143858-9
MW-5(i)
500-143858-10
MW-9(i)
500-143858-11
MW-9D(i)
500-143858-12
MW-10(i)
500-143858-12
MW-10(i)
500-143858-13
MW-8(i)
500-143858-14
MW-2(i)
500-143858-15
MW-3(i)
500-143858-16
MW-4D(i)
500-143858-17
MW-4(i)
500-143858-18
MW-6(i)
500-143858-19
MW-7D(i)
500-143858-20
MW-5D(i)
500-143858-21
MW-7(i)
Prep Type
Matrix
Method Prep Batch
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Total/NA
Water
9056A
Page 178 of 258
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7/5/2018

QC Association Summary
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
General Chemistry (Continued)
Analysis Batch: 429826 (Continued)
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
500-143858-30
MW11(i)
Total/NA
Water
9056A
500-143858-31
MW11D(i)
Total/NA
Water
9056A
MB 500-429826/3
Method Blank
Total/NA
Water
9056A
LCS 500-429826/4
Lab Control Sample
Total/NA
Water
9056A
500-143858-11 MS
MW-9D(i)
Total/NA
Water
9056A
500-143858-11 MSD
MW-9D(i)
Total/NA
Water
9056A
Prep Batch
0
TestAmerica Chicago
Page 179 of 258 7/5/2018

Surrogate Summary
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Matrix: Water
Lab Sample ID
500-143858-1
500-143858-2
500-143858-3
500-143858-4
500-143858-5
500-143858-6
500-143858-7
500-143858-8
500-143858-9
500-143858-10
500-143858-11
500-143858-12
500-143858-12 MS
500-143858-12 MSD
500-143858-13
500-143858-14
500-143858-15
500-143858-16
500-143858-17
500-143858-18
500-143858-19
500-143858-20
500-143858-21
500-143858-22
500-143858-23
500-143858-24
500-143858-25
500-143858-26
500-143858-27
500-143858-28
500-143858-29
500-143858-30
500-143858-31
500-143858-31 MS
500-143858-31 MSD
LCS 500-428709/4
LCS 500-428915/4
LCS 500-429099/4
LCS 500-429285/4
MB 500-428709/6
MB 500-428915/6
MB 500-429099/6
MB 500-429285/20
Surrogate Legend
Client Sample ID
MW-12(i)
MW-14(i)
MW-15(i)
MW-16(i)
MW-1(i)
MW-13(i)
MW-12D(i)
MW-8D(i)
MW-5(i)
MW-9(i)
MW-9D(i)
MW-10(i)
MW-10(i)
MW-10(i)
MW-8(i)
MW-2(i)
MW-3(i)
MW-4D(i)
MW-4(i)
MW-6(i)
MW-7D(i)
MW-5D(i)
MW-7(i)
Duplicate
Duplicate 1
Duplicate 2
TB
TB
TB
TB
TB
MW11(i)
MW11D(i)
MW11D(i)
MW11D(i)
Lab Control Sample
Lab Control Sample
Lab Control Sample
Lab Control Sample
Method Blank
Method Blank
Method Blank
Method Blank
DCA = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Prep Type: Total/NA
DCA
(75-126)
Percent Surrogate Recovery (Acceptance Limits)
BFB DBFM TOL
(72-124) (75-120) (75-120)
109
90
93
94
110
96
93
96
109
91
94
94
109
91
95
94
110
92
94
95
110
92
94
93
111
90
96
94
110
93
95
95
111
92
93
94
109
94
95
94
110
93
96
93
113
95
95
95
106
89
95
93
109
90
94
94
100
106
88
96
101
104
90
92
101
106
91
91
101
106
90
93
105
102
99
92
101
107
90
92
102
105
95
88
98
108
89
93
104
101
99
92
108
93
96
95
105
101
99
93
102
102
99
92
109
91
97
93
109
91
94
93
108
93
93
94
109
90
96
93
111
92
97
93
99
105
91
92
100
105
91
89
98
98
93
95
98
98
94
95
104
88
94
95
106
88
93
95
94
103
93
89
93
103
89
96
102
93
90
93
108
91
93
94
97
105
90
93
99
100
96
93
Page 180 of 258
TestAmerica Chicago
7/5/2018

Surrogate Summary
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Matrix: Water
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Prep Type: Total/NA
Lab Sample ID
Client Sample ID
FBP
(34-110)
Percent Surrogate Recovery (Acceptance Limits)
2FP NBZ PHL TPHL TBP
(27-110) (36-120) (20-100) (40-145) (40-145)
500-143858-1
MW-12(i)
86
65
92
60
94
103
500-143858-2
MW-14(i)
89
78
97
57
96
95
500-143858-5
MW-1(i)
84
69
90
58
85
92
500-143858-6
MW-13(i)
81
65
84
56
93
94
500-143858-7
MW-12D(i)
79
60
82
56
93
99
500-143858-8
MW-8D(i)
88
64
93
52
99
90
500-143858-9
MW-5(i)
90
72
95
64
100
107
500-143858-10
MW-9(i)
78
46
71
35
129
93
500-143858-11
MW-9D(i)
75
50
68
34
110
88
500-143858-12
MW-10(i)
104
73
101
51
146 X
101
500-143858-13
MW-8(i)
75
52
71
35
140
95
500-143858-14
MW-2(i)
96
57
91
43
142
103
500-143858-15
MW-3(i)
75
53
72
36
136
95
500-143858-16
MW-4D(i)
82
53
77
38
139
96
500-143858-17
MW-4(i)
81
51
77
37
114
83
500-143858-18
MW-6(i)
100
63
93
43
137
104
500-143858-19
MW-7D(i)
79
54
70
37
104
90
500-143858-20
MW-5D(i)
100
63
94
49
146 X
99
500-143858-21
MW-7(i)
107
70
99
48
118
103
500-143858-30
MW11(i)
94
52
90
40
138
97
500-143858-31
MW11D(i)
86
53
84
39
147 X
102
LCS 500-428028/2-A
Lab Control Sample
94
86
98
68
107
105
LCS 500-428463/2-A
Lab Control Sample
86
67
88
48
110
91
LCSD 500-428028/3-A
Lab Control Sample Dup
93
82
95
65
107
103
LCSD 500-428463/3-A
Lab Control Sample Dup
83
65
83
46
108
93
MB 500-428028/1-A
Method Blank
84
65
88
55
98
86
MB 500-428463/1-A
Method Blank
90
70
91
45
132
90
Surrogate Legend
FBP = 2-Fluorobiphenyl
2FP = 2-Fluorophenol
NBZ = Nitrobenzene-d5
PHL = Phenol-d5
TPHL = Terphenyl-d14
TBP = 2,4,6-Tribromophenol
Method: 8081 B - Organochlorine Pesticides (GC)
Matrix: Water Prep TVDe: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
DCBP1
TCX1
Lab Sample ID
Client Sample ID
(30-130)
(30-120)
500-143858-1
MW-12(i)
94
82
500-143858-2
MW-14(i)
79
65
500-143858-5
MW-1(i)
35
66
500-143858-6
MW-13(i)
58
289 X
500-143858-7
MW-12D(i)
75
190 X
500-143858-8
MW-8D(i)
77
59
500-143858-9
MW-5(i)
95
76
TestAmerica Chicago
Page 181 of 258 7/5/2018

Surrogate Summary
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8081 B - Organochlorine Pesticides (GC) (Continued)
Matrix: Water Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
DCBP1 TCX1
Lab Sample ID Client Sample ID (30-130) (30-120)
500-143858-10 MW-9(i)
57
102
500-143858-11 MW-9D(i)
44
64
500-143858-12 MW-10(i)
65
67
500-143858-13 MW-8(i)
48
61
500-143858-14 MW-2(i)
70
65
500-143858-15 MW-3(i)
74
68
500-143858-16 MW-4D(i)
78
64
500-143858-17 MW-4(i)
70
59
500-143858-18 MW-6(i)
66
57
500-143858-19 MW-7D(i)
54
91
m
500-143858-20 MW-5D(i)
65
61
500-143858-21 MW-7(i)
151 X
27 X
500-143858-30 MW11(i)
99
86
500-143858-31 MW11D(i)
87
102
LCS 500-428097/2-A Lab Control Sample
82
56
LCS 500-428495/2-A Lab Control Sample
83
58
E:
LCSD 500-428097/3-A Lab Control Sample Dup
73
51
LCSD 500-428495/3-A Lab Control Sample Dup
89
63
MB 500-428097/1-A Method Blank
82
48
MB 500-428495/1-A Method Blank
85
55
Surrogate Legend
DCBP = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Matrix: Water
PreD TVDe: Total/NA
Lab Sample ID
Client Sample ID
TCX2
(30-120)
Percent Surrogate Recovery (Acceptance Limits)
DCBP2
(30-140)
500-143858-1
MW-12(i)
63
89
500-143858-2
MW-14(i)
65
86
500-143858-5
MW-1(i)
60
37
500-143858-6
MW-13(i)
103
54
500-143858-7
MW-12D(i)
65
81
500-143858-8
MW-8D(i)
66
90
500-143858-9
MW-5(i)
64
77
500-143858-10
MW-9(i)
65
84
500-143858-11
MW-9D(i)
64
84
500-143858-12
MW-10(i)
67
73
500-143858-13
MW-8(i)
61
84
500-143858-14
MW-2(i)
71
86
500-143858-15
MW-3(i)
67
85
500-143858-16
MW-4D(i)
66
89
500-143858-17
MW-4(i)
72
84
500-143858-18
MW-6(i)
71
77
500-143858-19
MW-7D(i)
70
80
500-143858-20
MW-5D(i)
70
82
TestAmerica Chicago
Page 182 of 258 7/5/2018

Surrogate Summary
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)
Matrix: Water Prep Tvoe: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
TCX2
DCBP2
Lab Sample ID Client Sample ID
(30-120)
(30-140)
500-143858-21 MW-7(i)
71
87
500-143858-30 MW11(i)
65
69
500-143858-31 MW11D(i)
71
84
LCS 500-428097/4-A Lab Control Sample
79
103
LCS 500-428495/4-A Lab Control Sample
56
66
LCSD 500-428097/5-A Lab Control Sample Dup
84
100
LCSD 500-428495/5-A Lab Control Sample Dup
59
90
MB 500-428097/1-A Method Blank
55
90
MB 500-428495/1-A Method Blank
60
96
Surrogate Legend
m
TCX = Tetrachloro-m-xylene
DCBP = DCB Decachlorobiphenyl
Method: 8151A - Herbicides (GC)
Matrix: Water
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
DCPAA2
Lab Sample ID Client Sample ID
(25-130)
500-143858-1 MW-12(i)
89
500-143858-2 MW-14(i)
73
500-143858-5 MW-1(i)
92
500-143858-6 MW-13(i)
105
500-143858-7 MW-12D(i)
92
500-143858-8 MW-8D(i)
80
500-143858-9 MW-5(i)
68
500-143858-10 MW-9(i)
96
500-143858-11 MW-9D(i)
87
500-143858-12 MW-10(i)
77
500-143858-13 MW-8(i)
89
500-143858-14 MW-2(i)
82
500-143858-15 MW-3(i)
82
500-143858-16 MW-4D(i)
81
500-143858-17 MW-4(i)
113
500-143858-18 MW-6(i)
97
500-143858-19 MW-7D(i)
88
LCS 500-428120/2-A Lab Control Sample
81
LCSD 500-428120/3-A Lab Control Sample Dup
81
MB 500-428120/1-A Method Blank
74
Surrogate Legend
DCPAA = DCAA
TestAmerica Chicago
Page 183 of 258 7/5/2018

Surrogate Summary
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8151A - Herbicides (GC)
Matrix: Water
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
DCPAA1
Lab Sample ID Client Sample ID
(25-130)
500-143858-20 MW-5D(i)
40
500-143858-21 MW-7(i)
82
500-143858-30 MW11(i)
60
500-143858-31 MW11D(i)
62
LCS 500-428351/2-A Lab Control Sample
59
LCSD 500-428351/3-A Lab Control Sample Dup
63
MB 500-428351/1-A Method Blank
57
Surrogate Legend
DCPAA = DCAA
m
TestAmerica Chicago
Page 184 of 258 7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Method: 8260B - Volatile Organic Compounds (GC/MS)
Lab Sample ID: MB 500-428709/6
Matrix: Water
Analysis Batch: 428709
MB MB
Analyte
Result Qualifier
1,1,1,2-Tetrachloroethane
<0.46
1,1,1-Trichloroethane
<0.38
1,1,2,2-Tetrachloroethane
<0.40
1,1,2-Trichloroethane
<0.35
1,1-Dichloroethane
<0.41
1,1-Dichloroethene
<0.39
1,1-Dichloropropene
<0.30
1,2,3-Trichloropropane
<0.41
1,2,4-Trichlorobenzene
<0.34
1,2-Dibromo-3-Chloropropane
<2.0
1,2-Dibromoethane
<0.39
1,2-Dichlorobenzene
<0.33
1,2-Dichloroethane
<0.39
1,2-Dichloropropane
<0.43
1,3-Dichlorobenzene
<0.40
1,3-Dichloropropane
<0.36
1,4-Dichlorobenzene
<0.36
2,2-Dichloropropane
<0.44
2-Butanone (MEK)
<2.1
2-Chloro-1,3-butadiene
<0.23
2-Hexanone
<1.6
3-Chloropropene
<0.86
4-Methyl-2-pentanone (MIBK)
<2.2
Acetone
<1.7
Acetonitrile
<4.2
Acrolein
<23
Acrylonitrile
<4.5
Benzene
<0.15
Bromochloromethane
<0.43
Bromodichloromethane
<0.37
Bromoform
<0.48
Bromomethane
<0.80
Carbon disulfide
<0.45
Carbon tetrachloride
<0.38
Chlorobenzene
<0.39
Chloroethane
<0.51
Chloroform
<0.37
Chloromethane
<0.32
cis-1,2-Dichloroethene
<0.41
cis-1,3-Dichloropropene
<0.42
Dibromochloromethane
<0.49
Dibromomethane
<0.27
Dichlorodifluoromethane
<0.67
Ethyl methacrylate
<0.53
Ethylbenzene
<0.18
Hexachlorobutadiene
<0.45
lodomethane
<0.66
Isobutyl alcohol
<36
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: Method Blank
Prep Type: Total/NA
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1.0
0.50
0.46
ug/L
04/20/1812:24
1
1.0
0.50
0.38
ug/L
04/20/1812:24
1
1.0
0.50
0.40
ug/L
04/20/1812:24
1
1.0
0.50
0.35
ug/L
04/20/1812:24
1
1.0
0.50
0.41
ug/L
04/20/1812:24
1
1.0
0.50
0.39
ug/L
04/20/1812:24
1
1.0
0.50
0.30
ug/L
04/20/1812:24
1
1.0
0.50
0.41
ug/L
04/20/1812:24
1
1.0
0.50
0.34
ug/L
04/20/1812:24
1
5.0
2.5
2.0
ug/L
04/20/1812:24
1
1.0
0.50
0.39
ug/L
04/20/1812:24
1
1.0
0.50
0.33
ug/L
04/20/1812:24
1
1.0
0.50
0.39
ug/L
04/20/1812:24
1
1.0
0.50
0.43
ug/L
04/20/1812:24
1
1.0
0.50
0.40
ug/L
04/20/1812:24
1
1.0
0.50
0.36
ug/L
04/20/1812:24
1
1.0
0.50
0.36
ug/L
04/20/1812:24
1
1.0
0.50
0.44
ug/L
04/20/1812:24
1
5.0
2.5
2.1
ug/L
04/20/1812:24
1
1.0
0.50
0.23
ug/L
04/20/1812:24
1
5.0
2.5
1.6
ug/L
04/20/1812:24
1
2.5
1.2
0.86
ug/L
04/20/1812:24
1
5.0
2.5
2.2
ug/L
04/20/1812:24
1
5.0
2.5
1.7
ug/L
04/20/1812:24
1
10
8.0
4.2
ug/L
04/20/1812:24
1
100
50
23
ug/L
04/20/1812:24
1
20
10
4.5
ug/L
04/20/1812:24
1
0.50
0.25
0.15
ug/L
04/20/1812:24
1
1.0
0.50
0.43
ug/L
04/20/1812:24
1
1.0
0.50
0.37
ug/L
04/20/1812:24
1
1.0
0.50
0.48
ug/L
04/20/1812:24
1
2.0
1.0
0.80
ug/L
04/20/1812:24
1
2.0
1.0
0.45
ug/L
04/20/1812:24
1
1.0
0.50
0.38
ug/L
04/20/1812:24
1
1.0
0.50
0.39
ug/L
04/20/1812:24
1
1.0
0.51
0.51
ug/L
04/20/1812:24
1
2.0
1.0
0.37
ug/L
04/20/1812:24
1
1.0
0.50
0.32
ug/L
04/20/1812:24
1
1.0
0.50
0.41
ug/L
04/20/1812:24
1
1.0
0.50
0.42
ug/L
04/20/1812:24
1
1.0
0.50
0.49
ug/L
04/20/1812:24
1
1.0
0.50
0.27
ug/L
04/20/1812:24
1
2.0
1.0
0.67
ug/L
04/20/1812:24
1
2.5
1.2
0.53
ug/L
04/20/1812:24
1
0.50
0.25
0.18
ug/L
04/20/1812:24
1
1.0
0.50
0.45
ug/L
04/20/1812:24
1
2.5
1.2
0.66
ug/L
04/20/1812:24
1
100
50
36
ug/L
04/20/1812:24
1
Li
Page 185 of 258
TestAmerica Chicago
7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 500-42870916
Matrix: Water
Analysis Batch: 428709
MB MB
Analyte Result Qualifier RL LOD
MDL
Client Sample ID: Method Blank
Prep Type: Total/NA
Unit D Analyzed Dil Fac
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/20/18 12:24
1
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/20/18 12:24
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/20/18 12:24
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/20/18 12:24
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/20/18 12:24
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/20/18 12:24
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/20/18 12:24
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/20/18 12:24
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/20/18 12:24
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/20/18 12:24
1
trans- l,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/20/18 12:24
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/20/18 12:24
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/20/18 12:24
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/20/18 12:24
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/20/18 12:24
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/20/18 12:24
1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr)
102
75- 126
04120118 12:24 1
4-Bromofluorobenzene (Surr)
93
72 - 124
04120118 12:24 1
Dibromofluoromethane
90
75 - 120
04120118 12:24 1
Toluene-d8 (Surr)
93
75 - 120
04120118 12:24 1
Lab Sample ID: LCS 500-428709/4
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428709
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
1,1,1,2-Tetrachloroethane
50.0
52.1
ug/L
104
70-125
1,1,1-Trichloroethane
50.0
50.9
ug/L
102
70-125
1,1,2,2-Tetrachloroethane
50.0
44.4
ug/L
89
67-127
1,1,2-Trichloroethane
50.0
50.9
ug/L
102
70-122
1,1-Dichloroethane
50.0
52.8
ug/L
106
70-125
1,1-Dichloroethene
50.0
44.6
ug/L
89
67-122
1,1-Dichloropropene
50.0
52.0
ug/L
104
70-121
1,2,3-Trichloropropane
50.0
45.6
ug/L
91
50-133
1,2,4-Trichlorobenzene
50.0
55.9
ug/L
112
66-127
1,2-Dibromo-3-Chloropropane
50.0
52.5
ug/L
105
56-123
1,2-Dibromoethane
50.0
51.0
ug/L
102
70-125
1,2-Dichlorobenzene
50.0
48.8
ug/L
98
70 -125
1,2-Dichloroethane
50.0
57.2
ug/L
114
68 -127
1,2-Dichloropropane
50.0
53.2
ug/L
106
67 -130
1,3-Dichlorobenzene
50.0
48.7
ug/L
97
70 -125
1,3-Dichloropropane
50.0
52.0
ug/L
104
62 -136
1,4-Dichlorobenzene
50.0
48.7
ug/L
97
70 -120
2,2-Dichloropropane
50.0
46.3
ug/L
93
58 -129
2-Butanone (MEK)
50.0
55.2
ug/L
110
53 -141
2-Hexanone
50.0
54.6
ug/L
109
56-135
TestAmerica Chicago
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QC Sample Results C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 500-428709/4
Matrix: Water
Analysis Batch: 428709
Analyte
Spike
Added
LCS
Result
LCS
Qualifier
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
%Rec.
Unit D %Rec Limits
4-Methyl-2-pentanone (MIBK)
50.0
53.3
ug/L
107
56-133
Acetone
50.0
57.0
ug/L
114
40-143
Benzene
50.0
48.9
ug/L
98
70-120
Bromochloromethane
50.0
50.4
ug/L
101
65 -122
Bromodichloromethane
50.0
52.6
ug/L
105
69 -120
Bromoform
50.0
59.6
ug/L
119
56 -132
Bromomethane
50.0
39.5
ug/L
79
40 -130
Carbon disulfide
50.0
45.2
ug/L
90
66 -120
Carbon tetrachloride
50.0
52.7
ug/L
105
65 -122
Chlorobenzene
50.0
51.0
ug/L
102
70 -120
Chloroethane
50.0
47.8
ug/L
96
45 -127
Chloroform
50.0
49.7
ug/L
99
70 -120
Chloromethane
50.0
60.8
ug/L
122
54 -147
cis-1,2-Dichloroethene
50.0
47.6
ug/L
95
70 -125
cis-1,3-Dichloropropene
50.0
51.4
ug/L
103
64 -127
Dibromochloromethane
50.0
56.3
ug/L
113
68 -125
Dibromomethane
50.0
49.4
ug/L
99
70 -120
Dichlorodifluoromethane
50.0
56.8
ug/L
114
40 -150
Ethylbenzene
50.0
51.8
ug/L
104
70 -120
Hexachlorobutadiene
50.0
56.2
ug/L
112
51 -150
lodomethane
50.0
46.0
ug/L
92
61 -136
m&p-Xylene
50.0
50.1
ug/L
100
70 -125
Methylene Chloride
50.0
46.4
ug/L
93
69 -125
o-Xylene
50.0
50.5
ug/L
101
70 -120
Styrene
50.0
52.6
ug/L
105
70 -120
Tetrachloroethene
50.0
54.4
ug/L
109
70 -128
Tetrahydrofuran
100
108
ug/L
108
59 -139
Toluene
50.0
51.8
ug/L
104
70 -125
trans- 1,2-Dichloroethene
50.0
45.8
ug/L
92
70-125
trans- 1,3-Dichloropropene
50.0
51.0
ug/L
102
62 -128
Trichloroethene
50.0
51.5
ug/L
103
70 -125
Trichlorofluoromethane
50.0
52.3
ug/L
105
70 -126
Vinyl acetate
50.0
56.5
ug/L
113
43 -133
Vinyl chloride
50.0
53.1
ug/L
106
64 -126
Xylenes, Total
100
101
ug/L
101
70 -125
LCS
LCS
Surrogate %Recovery
Qualifier
Limits
1,2-Dichloroethane-d4 (Surr) 104
75- 126
4-Bromofluorobenzene (Surr) 88
72 - 124
Dibromofluoromethane 94
75 - 120
Toluene-d8 (Surr) 95
75 - 120
Lab Sample ID: MB 500-428915/6
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428915
MB MB
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/23/1811:25 1
TestAmerica Chicago
Page 187 of 258 7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 500-42891516
Matrix: Water
Analysis Batch: 428915
MB MB
Analyte Result Qualifier RL LOD
MDL
Client Sample ID: Method Blank
Prep Type: Total/NA
Unit D Analyzed Dil Fac
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/23/18 11:25
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/23/18 11:25
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/23/18 11:25
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 11:25
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 11:25
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/23/18 11:25
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/23/18 11:25
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/23/18 11:25
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/23/18 11:25
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 11:25
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/23/18 11:25
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/23/18 11:25
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 11:25
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/23/18 11:25
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/23/18 11:25
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 11:25
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/23/18 11:25
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/23/18 11:25
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/23/18 11:25
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/23/18 11:25
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/23/18 11:25
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/23/18 11:25
1
Acetone
<1.7
5.0
2.5
1.7
ug/L
04/23/18 11:25
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/23/18 11:25
1
Acrolein
<23
100
50
23
ug/L
04/23/18 11:25
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/23/18 11:25
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 11:25
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 11:25
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/23/18 11:25
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/23/18 11:25
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/23/18 11:25
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/23/18 11:25
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/23/18 11:25
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 11:25
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/23/18 11:25
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/23/18 11:25
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/23/18 11:25
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/23/18 11:25
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/23/18 11:25
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/23/18 11:25
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/23/18 11:25
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/23/18 11:25
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/23/18 11:25
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/23/18 11:25
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/23/18 11:25
1
Iodomethane
<0.66
2.5
1.2
0.66
ug/L
04/23/18 11:25
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/23/18 11:25
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/23/18 11:25
1
TestAmerica Chicago
Page 188 of 258 7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 500-42891516
Matrix: Water
Analysis Batch: 428915
MB MB
Analyte Result Qualifier RL LOD
MDL
Client Sample ID: Method Blank
Prep Type: Total/NA
Unit D Analyzed Dil Fac
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/23/18 11:25
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/23/18 11:25
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/23/18 11:25
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/23/18 11:25
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/23/18 11:25
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/23/18 11:25
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/23/18 11:25
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/23/18 11:25
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/23/18 11:25
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/23/18 11:25
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/23/18 11:25
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/23/18 11:25
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/23/18 11:25
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/23/18 11:25
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/23/18 11:25
1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr)
108
75- 126
04123118 11:25 1
4-Bromofluorobenzene (Surr)
91
72 - 124
04123118 11:25 1
Dibromofluoromethane
93
75 - 120
04123118 11:25 1
Toluene-d8 (Surr)
94
75 - 120
04/23/18 11:25 1
Lab Sample ID: LCS 500-428915/4
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428915
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
1,1,1,2-Tetrachloroethane
50.0
49.4
ug/L
99
70-125
1,1,1-Trichloroethane
50.0
49.0
ug/L
98
70-125
1,1,2,2-Tetrachloroethane
50.0
43.0
ug/L
86
67-127
1,1,2-Trichloroethane
50.0
47.4
ug/L
95
70-122
1,1-Dichloroethane
50.0
49.7
ug/L
99
70-125
1,1-Dichloroethene
50.0
41.5
ug/L
83
67-122
1,1-Dichloropropene
50.0
48.8
ug/L
98
70-121
1,2,3-Trichooropropane
50.0
42.7
ug/L
85
50-133
1,2,4-Trichoorobenzene
50.0
53.9
ug/L
108
66-127
1,2-Dibromo-3-Chloropropane
50.0
50.7
ug/L
101
56-123
1,2-Dibromoethane
50.0
47.8
ug/L
96
70-125
1,2-Dichlorobenzene
50.0
45.8
ug/L
92
70 -125
1,2-Dichloroethane
50.0
55.0
ug/L
110
68 -127
1,2-Dichloropropane
50.0
50.9
ug/L
102
67 -130
1,3-Dichlorobenzene
50.0
45.5
ug/L
91
70 -125
1,3-Dichloropropane
50.0
47.9
ug/L
96
62 -136
1,4-Dichlorobenzene
50.0
46.2
ug/L
92
70 -120
2,2-Dichloropropane
50.0
44.6
ug/L
89
58 -129
2-Butanone (MEK)
50.0
55.6
ug/L
111
53 -141
2-Hexanone
50.0
54.1
ug/L
108
56 -135
4-Methyl-2-pentanone (MIBK)
50.0
52.4
ug/L
105
56-133
TestAmerica Chicago
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QC Sample Results C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 500-428915/4
Matrix: Water
Analysis Batch: 428915
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Analyte
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec.
Limits
Acetone
50.0
58.5
ug/L
117
40 -143
Benzene
50.0
45.5
ug/L
91
70 -120
Bromochloromethane
50.0
47.1
ug/L
94
65 -122
Bromodichloromethane
50.0
50.8
ug/L
102
69 -120
Bromoform
50.0
56.0
ug/L
112
56 -132
Bromomethane
50.0
36.8
ug/L
74
40 -130
Carbon disulfide
50.0
41.7
ug/L
83
66 -120
Carbon tetrachloride
50.0
49.9
ug/L
100
65 -122
Chlorobenzene
50.0
47.4
ug/L
95
70 -120
Chloroethane
50.0
42.1
ug/L
84
45 -127
Chloroform
50.0
47.0
ug/L
94
70 -120
Chloromethane
50.0
54.2
ug/L
108
54 -147
cis-1,2-Dichloroethene
50.0
44.3
ug/L
89
70 -125
cis-1,3-Dichloropropene
50.0
48.6
ug/L
97
64 -127
Dibromochloromethane
50.0
53.3
ug/L
107
68 -125
Dibromomethane
50.0
47.6
ug/L
95
70 -120
Dichlorodifluoromethane
50.0
48.5
ug/L
97
40 -150
Ethylbenzene
50.0
48.0
ug/L
96
70 -120
Hexachlorobutadiene
50.0
53.2
ug/L
106
51 -150
lodomethane
50.0
42.2
ug/L
84
61 -136
m&p-Xylene
50.0
48.1
ug/L
96
70 -125
Methylene Chloride
50.0
43.7
ug/L
87
69 -125
o-Xylene
50.0
47.8
ug/L
96
70 -120
Styrene
50.0
49.6
ug/L
99
70 -120
Tetrachloroethene
50.0
51.5
ug/L
103
70 -128
Tetrahydrofuran
100
97.8
ug/L
98
59 -139
Toluene
50.0
48.1
ug/L
96
70 -125
trans- 1,2-Dichloroethene
50.0
43.2
ug/L
86
70-125
trans- 1,3-Dichloropropene
50.0
49.0
ug/L
98
62 -128
Trichloroethene
50.0
48.7
ug/L
97
70 -125
Trichlorofluoromethane
50.0
48.6
ug/L
97
70 -126
Vinyl acetate
50.0
53.6
ug/L
107
43 -133
Vinyl chloride
50.0
47.6
ug/L
95
64 -126
Xylenes, Total
100
95.9
ug/L
96
70 -125
LCS LCS
Surrogate
%Recovery Qualifier
Limits
1,2-Dichloroethane-d4 (Surr)
106
75- 126
4-Bromofluorobenzene (Surr)
88
72 - 124
Dibromofluoromethane
93
75 - 120
Toluene-d8 (Surr)
95
75 - 120
Lab Sample ID: 500-143858-12 MS
Matrix: Water
Analysis Batch: 428915
Client Sample ID: MW-10(i)
Prep Type: Total/NA
Sample Sample
Spike
MS MS
%Rec.
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec Limits
1,1,1,2-Tetrachloroethane
<0.46
50.0
49.8
ug/L
100 70-125
1,1,1-Trichloroethane
<0.38
50.0
47.9
ug/L
96 70-125
TestAmerica Chicago
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QC Sample Results C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 500-143858-12 MS
Matrix: Water
Analysis Batch: 428915
Client Sample ID: MW-10(i)
Prep Type: Total/NA
Analyte
Sample
Result
Sample
Qualifier
Spike
Added
MS MS
Result Qualifier
Unit
D %Rec
%Rec.
Limits
1,1,2,2-Tetrachloroethane
<0.40
50.0
47.2
ug/L
94
67-127
1,1,2-Trichloroethane
<0.35
50.0
50.4
ug/L
101
70-122
1,1-Dichloroethane
<0.41
50.0
50.1
ug/L
100
70-125
1,1-Dichloroethene
<0.39
50.0
41.2
ug/L
82
67-122
1,1-Dichloropropene
<0.30
50.0
47.7
ug/L
95
70-121
1,2,3-Trichloropropane
<0.41
50.0
47.0
ug/L
94
50-133
1,2,4-Trichlorobenzene
<0.34
50.0
53.0
ug/L
106
66-127
1,2-Dibromo-3-Chloropropane
<2.0
50.0
51.2
ug/L
102
56-123
1,2-Dibromoethane
<0.39
50.0
49.8
ug/L
100
70-125
1,2-Dichlorobenzene
<0.33
50.0
48.5
ug/L
97
70 -125
1,2-Dichloroethane
<0.39
50.0
57.5
ug/L
115
68 -127
1,2-Dichloropropane
<0.43
50.0
50.5
ug/L
101
67 -130
1,3-Dichlorobenzene
<0.40
50.0
47.3
ug/L
95
70 -125
1,3-Dichloropropane
<0.36
50.0
50.2
ug/L
100
62 -136
1,4-Dichlorobenzene
<0.36
50.0
47.1
ug/L
94
70 -120
2,2-Dichloropropane
<0.44
50.0
42.4
ug/L
85
58 -129
2-Butanone (MEK)
<2.1
F2
50.0
38.8
ug/L
78
53 -141
2-Hexanone
<1.6
50.0
42.6
ug/L
85
56 -135
4-Methyl-2-pentanone (MIBK)
<2.2
50.0
42.8
ug/L
86
56-133
Acetone
2.3
J cn
50.0
48.1
ug/L
92
40 -143
Benzene
<0.15
50.0
46.4
ug/L
93
70 -120
Bromochloromethane
<0.43
F2
50.0
50.2
ug/L
100
65 -122
Bromodichloromethane
<0.37
50.0
51.2
ug/L
102
69 -120
Bromoform
<0.48
50.0
58.6
ug/L
117
56 -132
Bromomethane
<0.80
50.0
34.8
ug/L
70
40 -130
Carbon disulfide
<0.45
50.0
41.1
ug/L
82
66 -120
Carbon tetrachloride
<0.38
50.0
49.1
ug/L
98
65 -122
Chlorobenzene
<0.39
50.0
48.0
ug/L
96
70 -120
Chloroethane
<0.51
50.0
38.6
ug/L
77
45 -127
Chloroform
<0.37
50.0
48.5
ug/L
97
70 -120
Chloromethane
<0.32
50.0
49.7
ug/L
99
54 -147
cis-1,2-Dichloroethene
<0.41
50.0
45.2
ug/L
90
70 -125
cis-1,3-Dichloropropene
<0.42
50.0
47.1
ug/L
94
64 -127
Dibromochloromethane
<0.49
50.0
54.6
ug/L
109
68 -125
Dibromomethane
<0.27
50.0
49.2
ug/L
98
70 -120
Dichlorodifluoromethane
<0.67
50.0
43.3
ug/L
87
40 -150
Ethylbenzene
<0.18
50.0
48.8
ug/L
98
70 -120
Hexachlorobutadiene
<0.45
50.0
54.7
ug/L
109
51 -150
lodomethane
<0.66
50.0
42.7
ug/L
85
61 -136
m&p-Xylene
<0.18
50.0
47.3
ug/L
95
70 -125
Methylene Chloride
<1.6
50.0
43.4
ug/L
87
69 -125
o-Xylene
<0.22
50.0
47.6
ug/L
95
70 -120
Styrene
<0.39
50.0
49.9
ug/L
100
70 -120
Tetrachloroethene
<0.37
50.0
50.2
ug/L
100
70 -128
Tetrahydrofuran
<1.9
100
103
ug/L
103
59 -139
Toluene
<0.15
50.0
48.3
ug/L
97
70 -125
trans- 1,2-Dichloroethene
<0.35
50.0
42.3
ug/L
85
70-125
trans- 1,3-Dichloropropene
<0.36
50.0
48.0
ug/L
96
62 -128
TestAmerica Chicago
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QC Sample Results C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 500-143858-12 MS
Matrix: Water
Analysis Batch: 428915
Sample
Analyte Result
Sample
Qualifier
Spike
Added
MS
Result
MS
Qualifier
Unit
Client Sample ID: MW-10(i)
Prep Type: Total/NA
%Rec.
D %Rec Limits
Trichloroethene
<0.16
50.0
48.3
ug/L
97
70 -125
Trichlorofluoromethane
<0.43
F1
50.0
16.5
F1
ug/L
33
70-126
Vinyl acetate
<0.91
50.0
52.9
ug/L
106
43 -133
Vinyl chloride
<0.20
50.0
44.3
ug/L
89
64 -126
Xylenes, Total
<0.22
100
94.9
ug/L
95
70 -125
MS
MS
Surrogate
%Recovery
Qualifier
Limits
1,2-Dichloroethane-d4 (Surr)
106
75- 126
4-Bromofluorobenzene (Surr)
89
72 - 124
Dibromofluoromethane
95
75 - 120
Toluene-d8 (Surr)
93
75 - 120
Lab Sample ID: 500-143858-12 MSD
Client Sample ID: MW-10(i)
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428915
Sample
Sample
Spike
MSD
MSD
%Rec.
RPD
Analyte
Result
Qualifier
Added
Result
Qualifier
Unit
D %Rec
Limits
RPD
Limit
1,1,1,2-Tetrachloroethane
<0.46
50.0
42.2
ug/L
84
70 -125
17
20
1,1,1-Trichloroethane
<0.38
50.0
39.9
ug/L
80
70-125
18
20
1,1,2,2-Tetrachloroethane
<0.40
50.0
39.3
ug/L
79
67-127
18
20
1,1,2-Trichloroethane
<0.35
50.0
42.3
ug/L
85
70-122
17
20
1,1-Dichloroethane
<0.41
50.0
41.4
ug/L
83
70-125
19
20
1,1-Dichloroethene
<0.39
50.0
34.0
ug/L
68
67-122
19
20
1,1-Dichloropropene
<0.30
50.0
39.9
ug/L
80
70-121
18
20
1,2,3-Trichooropropane
<0.41
50.0
39.5
ug/L
79
50-133
17
20
1,2,4-Trichoorobenzene
<0.34
50.0
45.3
ug/L
91
66-127
16
20
1,2-Dibromo-3-Chloropropane
<2.0
50.0
43.8
ug/L
88
56-123
16
20
1,2-Dibromoethane
<0.39
50.0
42.3
ug/L
85
70 -125
16
20
1,2-Dichlorobenzene
<0.33
50.0
41.6
ug/L
83
70 -125
15
20
1,2-Dichloroethane
<0.39
50.0
48.2
ug/L
96
68 -127
17
20
1,2-Dichloropropane
<0.43
50.0
43.1
ug/L
86
67 -130
16
20
1,3-Dichlorobenzene
<0.40
50.0
40.4
ug/L
81
70 -125
16
20
1,3-Dichloropropane
<0.36
50.0
42.5
ug/L
85
62 -136
17
20
1,4-Dichlorobenzene
<0.36
50.0
39.4
ug/L
79
70 -120
18
20
2,2-Dichloropropane
<0.44
50.0
35.4
ug/L
71
58 -129
18
20
2-Butanone (MEK)
<2.1
F2
50.0
49.8
F2
ug/L
100
53 -141
25
20
2-Hexanone
<1.6
50.0
42.9
ug/L
86
56-135
1
20
4-Methyl-2-pentanone (MIBK)
<2.2
50.0
45.2
ug/L
90
56-133
5
20
Acetone
2.3
J cn
50.0
50.3
ug/L
96
40 -143
4
20
Benzene
<0.15
50.0
38.7
ug/L
77
70 -120
18
20
Bromochloromethane
<0.43
F2
50.0
40.3
F2
ug/L
81
65 -122
22
20
Bromodichloromethane
<0.37
50.0
43.8
ug/L
88
69 -120
16
20
Bromoform
<0.48
50.0
50.0
ug/L
100
56 -132
16
20
Bromomethane
<0.80
50.0
30.4
ug/L
61
40 -130
13
20
Carbon disulfide
<0.45
50.0
34.1
ug/L
68
66 -120
19
20
Carbon tetrachloride
<0.38
50.0
41.2
ug/L
82
65 -122
17
20
Chlorobenzene
<0.39
50.0
40.7
ug/L
81
70-120
17
20
Chloroethane
<0.51
50.0
32.2
ug/L
64
45 -127
18
20
TestAmerica Chicago
Page 192 of 258 7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 500-143858-12 MSD
Matrix: Water
Analysis Batch: 428915
Sample Sample Spike MSD MSD
Analyte Result Qualifier Added Result Qualifier Unit
Client Sample ID: MW-10(i)
Prep Type: Total/NA
%Rec. RPD
D %Rec Limits RPD Limit
Chloroform
<0.37
50.0
39.9
ug/L
80
70 -120
20
20
Chloromethane
<0.32
50.0
43.3
ug/L
87
54 -147
14
20
cis-1,2-Dichloroethene
<0.41
50.0
38.2
ug/L
76
70 -125
17
20
cis-1,3-Dichloropropene
<0.42
50.0
40.3
ug/L
81
64 -127
16
20
Dibromochloromethane
<0.49
50.0
45.9
ug/L
92
68 -125
17
20
Dibromomethane
<0.27
50.0
40.5
ug/L
81
70 -120
20
20
Dichlorodifluoromethane
<0.67
50.0
39.5
ug/L
79
40 -150
9
20
Ethylbenzene
<0.18
50.0
40.5
ug/L
81
70 -120
19
20
Hexachlorobutadiene
<0.45
50.0
45.7
ug/L
91
51 -150
18
20
lodomethane
<0.66
50.0
36.3
ug/L
73
61 -136
16
20
m&p-Xylene
<0.18
50.0
40.2
ug/L
80
70 -125
16
20
Methylene Chloride
<1.6
50.0
37.3
ug/L
75
69 -125
15
20
o-Xylene
<0.22
50.0
40.6
ug/L
81
70 -120
16
20
Styrene
<0.39
50.0
42.0
ug/L
84
70 -120
17
20
Tetrachloroethene
<0.37
50.0
42.0
ug/L
84
70 -128
18
20
Tetrahydrofuran
<1.9
100
88.7
ug/L
89
59 -139
15
20
Toluene
<0.15
50.0
40.7
ug/L
81
70 -125
17
20
trans- 1,2-Dichloroethene
<0.35
50.0
36.2
ug/L
72
70 -125
16
20
trans- 1,3-Dichloropropene
<0.36
50.0
41.7
ug/L
83
62 -128
14
20
Trichloroethene
<0.16
50.0
39.7
ug/L
79
70 -125
19
20
Trichlorofluoromethane
<0.43 F1
50.0
15.8 F1
ug/L
32
70-126
4
20
Vinyl acetate
<0.91
50.0
46.3
ug/L
93
43 -133
13
20
Vinyl chloride
<0.20
50.0
36.4
ug/L
73
64 -126
19
20
Xylenes, Total
<0.22
100
80.8
ug/L
81
70 -125
16
20
MSD
MSD
Surrogate
%Recovery
Qualifier
Limits
1,2-Dichloroethane-d4 (Surr)
109
75- 126
4-Bromofluorobenzene (Surr)
90
72 - 124
Dibromofluoromethane
94
75 - 120
Toluene-d8 (Surr)
94
75 - 120
Lab Sample ID: MB 500-429099/6
Client
Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 429099
MB MB
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/24/18 0036
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/24/1810:36
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/24/1810:36
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/24/1810:36
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/24/1810:36
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/24/1810:36
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/24/1810:36
1
1,2,3-Trichloropropane
<0.41
1.0
0.50
0.41
ug/L
04/24/1810:36
1
1,2,4-Trichlorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/24/1810:36
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/24/1810:36
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/24/1810:36
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/24/1810:36
1
Ill
TestAmerica Chicago
Page 193 of 258 7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 500-42909916
Matrix: Water
Analysis Batch: 429099
MB MB
Analyte Result Qualifier RL LOD
MDL
Client Sample ID: Method Blank
Prep Type: Total/NA
Unit D Analyzed Dil Fac
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/24/18 10:36
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 10:36
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/24/18 10:36
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/24/18 10:36
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 10:36
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/24/18 10:36
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/24/18 10:36
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/24/18 10:36
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/24/18 10:36
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/24/18 10:36
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/24/18 10:36
1
Acetone
<1.7
5.0
2.5
1.7
ug/L
04/24/18 10:36
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/24/18 10:36
1
Acrolein
<23
100
50
23
ug/L
04/24/18 10:36
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/24/18 10:36
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/24/18 10:36
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 10:36
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/24/18 10:36
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/24/18 10:36
1
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/24/18 10:36
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/24/18 10:36
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/24/18 10:36
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 10:36
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/24/18 10:36
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/24/18 10:36
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/24/18 10:36
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/24/18 10:36
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/24/18 10:36
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/24/18 10:36
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/24/18 10:36
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/24/18 10:36
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/24/18 10:36
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/24/18 10:36
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/24/18 10:36
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/24/18 10:36
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/24/18 10:36
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/24/18 10:36
1
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/24/18 10:36
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/24/18 10:36
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/24/18 10:36
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/24/18 10:36
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/24/18 10:36
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/24/18 10:36
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/24/18 10:36
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/24/18 10:36
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/24/18 10:36
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/24/18 10:36
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/24/18 10:36
1
TestAmerica Chicago
Page 194 of 258 7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 500-42909916
Matrix: Water
Analysis Batch: 429099
MB MB
Analyte Result Qualifier RL LOD MDL
Client Sample ID: Method Blank
Prep Type: Total/NA
Unit D Analyzed Dil Fac
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/24/18 10:36 1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/24/18 10:36 1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/24/18 10:36 1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/24/18 10:36 1
MB MB
Surrogate %Recovery
Qualifier
Limits
Prepared
Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr)
97
75- 126
04/24/18 10:36 1
4-Bromofluorobenzene (Surr)
105
72 - 124
04124118 10:36 1
Dibromofluoromethane
90
75 - 120
04124118 10:36 1
Toluene-d8 (Surr)
93
75 - 120
04124118 10:36 1
Lab Sample ID: LCS 500-429099/4
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 429099
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits
1,1,1,2-Tetrachloroethane
50.0
47.6
ug/L
95
70 -125
1,1,1-Trichloroethane
50.0
48.1
ug/L
96
70-125
1,1,2,2-Tetrachloroethane
50.0
56.2
ug/L
112
67-127
1,1,2-Trichloroethane
50.0
53.9
ug/L
108
70-122
1,1-Dichloroethane
50.0
53.2
ug/L
106
70-125
1,1-Dichloroethene
50.0
49.6
ug/L
99
67-122
1,1-Dichloropropene
50.0
51.4
ug/L
103
70-121
1,2,3-Trichooropropane
50.0
55.1
ug/L
110
50-133
1,2,4-Trichoorobenzene
50.0
59.0
ug/L
118
66-127
1,2-Dibromo-3-Chloropropane
50.0
50.1
ug/L
100
56-123
1,2-Dibromoethane
50.0
52.5
ug/L
105
70-125
1,2-Dichlorobenzene
50.0
53.9
ug/L
108
70 -125
1,2-Dichloroethane
50.0
53.6
ug/L
107
68 -127
1,2-Dichloropropane
50.0
57.6
ug/L
115
67 -130
1,3-Dichlorobenzene
50.0
52.6
ug/L
105
70 -125
1,3-Dichloropropane
50.0
53.5
ug/L
107
62 -136
1,4-Dichlorobenzene
50.0
52.8
ug/L
106
70 -120
2,2-Dichloropropane
50.0
42.2
ug/L
84
58 -129
2-Butanone (MEK)
50.0
43.4
ug/L
87
53 -141
2-Hexanone
50.0
45.4
ug/L
91
56 -135
4-Methyl-2-pentanone (MIBK)
50.0
41.4
ug/L
83
56-133
Acetone
50.0
59.7
ug/L
119
40-143
Benzene
50.0
49.8
ug/L
100
70-120
Bromochloromethane
50.0
54.6
ug/L
109
65 -122
Bromodichloromethane
50.0
52.4
ug/L
105
69 -120
Bromoform
50.0
56.6
ug/L
113
56 -132
Bromomethane
50.0
46.2
ug/L
92
40 -130
Carbon disulfide
50.0
48.0
ug/L
96
66 -120
Carbon tetrachloride
50.0
51.2
ug/L
102
65 -122
Chlorobenzene
50.0
52.1
ug/L
104
70 -120
Chloroethane
50.0
53.1
ug/L
106
45 -127
Chloroform
50.0
47.8
ug/L
96
70 -120
TestAmerica Chicago
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QC Sample Results C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 500-429099/4
Matrix: Water
Analysis Batch: 429099
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Analyte
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec.
Limits
Chloromethane
50.0
59.5
ug/L
119
54 -147
cis-1,2-Dichloroethene
50.0
50.3
ug/L
101
70 -125
cis-1,3-Dichloropropene
50.0
51.6
ug/L
103
64 -127
Dibromochloromethane
50.0
56.8
ug/L
114
68 -125
Dibromomethane
50.0
53.9
ug/L
108
70 -120
Dichlorodifluoromethane
50.0
57.8
ug/L
116
40 -150
Ethylbenzene
50.0
48.3
ug/L
97
70 -120
Hexachlorobutadiene
50.0
53.2
ug/L
106
51 -150
lodomethane
50.0
50.6
ug/L
101
61 -136
m&p-Xylene
50.0
47.0
ug/L
94
70 -125
Methylene Chloride
50.0
45.8
ug/L
92
69 -125
o-Xylene
50.0
46.6
ug/L
93
70 -120
Styrene
50.0
50.6
ug/L
101
70 -120
Tetrachloroethene
50.0
53.6
ug/L
107
70 -128
Tetrahydrofuran
100
104
ug/L
104
59 -139
Toluene
50.0
49.6
ug/L
99
70 -125
trans- 1,2-Dichloroethene
50.0
48.7
ug/L
97
70-125
trans- 1,3-Dichloropropene
50.0
52.2
ug/L
104
62 -128
Trichloroethene
50.0
57.3
ug/L
115
70 -125
Trichlorofluoromethane
50.0
47.0
ug/L
94
70 -126
Vinyl acetate
50.0
43.6
ug/L
87
43 -133
Vinyl chloride
50.0
57.0
ug/L
114
64 -126
Xylenes, Total
100
93.6
ug/L
94
70 -125
LCS LCS
Surrogate
%Recovery Qualifier
Limits
1,2-Dichloroethane-d4 (Surr)
94
75- 126
4-Bromofluorobenzene (Surr)
103
72 - 124
Dibromofluoromethane
93
75 - 120
Toluene-d8 (Surr)
89
75 - 120
Lab Sample ID: 500-143858-31 MS
Matrix: Water
Analysis Batch: 429099
Analyte
1,1,1,2-Tetrachloroethane
1,1,1-Trich loroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trich loroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
Client Sample ID: MW11D(i)
Prep Type: Total/NA
Sample Sample
Spike
MS MS
%Rec.
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
<0.46
50.0
52.8
ug/L
106
70 -125
<0.38
50.0
43.8
ug/L
88
70 -125
<0.40
50.0
57.7
ug/L
115
67 -127
<0.35
50.0
59.4
ug/L
119
70 -122
<0.41
50.0
50.6
ug/L
101
70 -125
<0.39
50.0
44.8
ug/L
90
67-122
<0.30
50.0
51.4
ug/L
103
70 -121
<0.41
50.0
55.7
ug/L
111
50 -133
<0.34
50.0
58.4
ug/L
117
66 -127
<2.0
50.0
54.9
ug/L
110
56-123
<0.39
50.0
57.2
ug/L
114
70 -125
<0.33
50.0
54.1
ug/L
108
70 -125
<0.39
50.0
55.9
ug/L
112
68 -127
TestAmerica Chicago
Page 196 of 258 7/5/2018

QC Sample Results C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 500-143858-31 MS
Matrix: Water
Analysis Batch: 429099
Client Sample ID: MW11D(i)
Prep Type: Total/NA
Sample
Sample
Spike
MS MS
%Rec.
Analyte
Result
Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
1,2-Dichloropropane
<0.43
50.0
57.5
ug/L
115
67 -130
1,3-Dichlorobenzene
<0.40
50.0
52.2
ug/L
104
70 -125
1,3-Dichloropropane
<0.36
50.0
56.3
ug/L
113
62 -136
1,4-Dichlorobenzene
<0.36
50.0
53.2
ug/L
106
70 -120
2,2-Dichloropropane
<0.44
50.0
35.2
ug/L
70
58 -129
2-Butanone (MEK)
<2.1
50.0
46.5
ug/L
93
53 -141
2-Hexanone
<1.6
50.0
48.3
ug/L
97
56 -135
4-Methyl-2-pentanone (MIBK)
<2.2
50.0
45.8
ug/L
92
56-133
Acetone
4.6
J cn
50.0
58.7
ug/L
108
40 -143
Benzene
<0.15
50.0
49.8
ug/L
100
70 -120
Bromochloromethane
<0.43
50.0
54.1
ug/L
108
65 -122
Bromodichloromethane
<0.37
50.0
52.1
ug/L
104
69 -120
Bromoform
<0.48
50.0
58.6
ug/L
117
56 -132
Bromomethane
<0.80
50.0
40.9
ug/L
82
40 -130
Carbon disulfide
<0.45
50.0
43.5
ug/L
87
66 -120
Carbon tetrachloride
<0.38
50.0
46.1
ug/L
92
65 -122
Chlorobenzene
<0.39
50.0
51.8
ug/L
104
70 -120
Chloroethane
<0.51
50.0
47.6
ug/L
95
45 -127
Chloroform
<0.37
50.0
46.6
ug/L
93
70 -120
Chloromethane
<0.32
50.0
53.7
ug/L
107
54 -147
cis-1,2-Dichloroethene
<0.41
50.0
48.4
ug/L
97
70 -125
cis-1,3-Dichloropropene
<0.42
50.0
55.7
ug/L
ill
64 -127
Dibromochloromethane
<0.49
50.0
59.2
ug/L
118
68 -125
Dibromomethane
<0.27
50.0
54.9
ug/L
110
70 -120
Dichlorodifluoromethane
<0.67
50.0
51.2
ug/L
102
40 -150
Ethylbenzene
<0.18
50.0
47.2
ug/L
94
70 -120
Hexachlorobutadiene
<0.45
50.0
52.5
ug/L
105
51 -150
lodomethane
<0.66
50.0
46.4
ug/L
93
61 -136
m&p-Xylene
<0.18
50.0
46.3
ug/L
93
70 -125
Methylene Chloride
<1.6
50.0
43.5
ug/L
87
69 -125
o-Xylene
<0.22
50.0
48.1
ug/L
96
70 -120
Styrene
<0.39
50.0
50.8
ug/L
102
70 -120
Tetrachloroethene
<0.37
50.0
55.9
ug/L
112
70 -128
Tetrahydrofuran
<1.9
100
109
ug/L
109
59 -139
Toluene
<0.15
50.0
53.0
ug/L
106
70 -125
trans- 1,2-Dichloroethene
<0.35
50.0
45.3
ug/L
91
70-125
trans- 1,3-Dichloropropene
<0.36
50.0
54.1
ug/L
108
62 -128
Trichloroethene
<0.16
50.0
56.8
ug/L
114
70 -125
Trichlorofluoromethane
<0.43
50.0
41.9
ug/L
84
70 -126
Vinyl acetate
<0.91
50.0
40.2
ug/L
80
43 -133
Vinyl chloride
<0.20
50.0
50.2
ug/L
100
64 -126
Xylenes, Total
<0.22
100
94.4
ug/L
94
70 -125
MS
MS
Surrogate
%Recovery
Qualifier
Limits
1,2-Dichloroethene-d4 (Surr)
98
75- 126
4-Bromofluorobenzene (Surr)
98
72 - 124
Dibromofluoromethane
93
75 - 120
Toluene-d8 (Surr)
95
75 - 120
TestAmerica Chicago
Page 197 of 258 7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Lab Sample ID: 500-143858-31 MSD
Matrix: Water
Analysis Batch: 429099
Sample Sample
Analyte Result Qualifier
Spike
Added
MSD
Result
SDG:
MSD
Qualifier Unit
TestAmerica Job ID: 500-143858-1
NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW11D(i)
Prep Type: Total/NA
%Rec. RPD
D %Rec Limits RPD Limit
1,1,1,2-Tetrachloroethane
<0.46
50.0
45.3
ug/L
91
70 -125
15
20
1,1,1-Trichloroethane
<0.38
50.0
37.8
ug/L
76
70-125
15
20
1,1,2,2-Tetrachloroethane
<0.40
50.0
50.2
ug/L
100
67-127
14
20
1,1,2-Trichloroethane
<0.35
50.0
50.3
ug/L
101
70-122
17
20
1,1-Dichloroethane
<0.41
50.0
43.1
ug/L
86
70-125
16
20
1,1-Dichloroethene
<0.39
50.0
38.3
ug/L
77
67-122
16
20
1,1-Dichloropropene
<0.30
50.0
43.4
ug/L
87
70-121
17
20
1,2,3-Trichloropropane
<0.41
50.0
48.1
ug/L
96
50-133
15
20
1,2,4-Trichlorobenzene
<0.34
50.0
49.8
ug/L
100
66-127
16
20
1,2-Dibromo-3-Chloropropane
<2.0
50.0
46.7
ug/L
93
56-123
16
20
1,2-Dibromoethane
<0.39
50.0
49.1
ug/L
98
70-125
15
20
1,2-Dichlorobenzene
<0.33
50.0
47.2
ug/L
94
70 -125
14
20
1,2-Dichloroethane
<0.39
50.0
47.1
ug/L
94
68 -127
17
20
1,2-Dichloropropane
<0.43
50.0
49.6
ug/L
99
67 -130
15
20
1,3-Dichlorobenzene
<0.40
50.0
45.1
ug/L
90
70 -125
15
20
1,3-Dichloropropane
<0.36
50.0
48.4
ug/L
97
62 -136
15
20
1,4-Dichlorobenzene
<0.36
50.0
46.3
ug/L
93
70 -120
14
20
2,2-Dichloropropane
<0.44
50.0
30.5
ug/L
61
58 -129
14
20
2-Butanone (MEK)
<2.1
50.0
38.5
ug/L
77
53 -141
19
20
2-Hexanone
<1.6
50.0
43.4
ug/L
87
56 -135
11
20
4-Methyl-2-pentanone (MIBK)
<2.2
50.0
41.7
ug/L
83
56-133
9
20
Acetone
4.6 J cn
50.0
53.4
ug/L
98
40 -143
10
20
Benzene
<0.15
50.0
42.7
ug/L
85
70 -120
15
20
Bromochloromethane
<0.43
50.0
45.7
ug/L
91
65 -122
17
20
Bromodichloromethane
<0.37
50.0
45.7
ug/L
91
69 -120
13
20
Bromoform
<0.48
50.0
50.7
ug/L
101
56 -132
14
20
Bromomethane
<0.80
50.0
41.1
ug/L
82
40 -130
0
20
Carbon disulfide
<0.45
50.0
37.0
ug/L
74
66 -120
16
20
Carbon tetrachloride
<0.38
50.0
39.4
ug/L
79
65 -122
16
20
Chlorobenzene
<0.39
50.0
44.0
ug/L
88
70 -120
16
20
Chloroethane
<0.51
50.0
46.7
ug/L
93
45 -127
2
20
Chloroform
<0.37
50.0
39.9
ug/L
80
70 -120
16
20
Chloromethane
<0.32
50.0
54.1
ug/L
108
54 -147
1
20
cis-1,2-Dichloroethene
<0.41
50.0
41.3
ug/L
83
70 -125
16
20
cis-1,3-Dichloropropene
<0.42
50.0
48.5
ug/L
97
64 -127
14
20
Dibromochloromethane
<0.49
50.0
50.7
ug/L
101
68 -125
16
20
Dibromomethane
<0.27
50.0
46.8
ug/L
94
70 -120
16
20
Dichlorodifluoromethane
<0.67
50.0
51.5
ug/L
103
40 -150
0
20
Ethylbenzene
<0.18
50.0
40.1
ug/L
80
70 -120
16
20
Hexachlorobutadiene
<0.45
50.0
45.7
ug/L
91
51 -150
14
20
lodomethane
<0.66
50.0
39.7
ug/L
79
61 -136
16
20
m&p-Xylene
<0.18
50.0
39.3
ug/L
79
70 -125
16
20
Methylene Chloride
<1.6
50.0
37.0
ug/L
74
69 -125
16
20
o-Xylene
<0.22
50.0
41.2
ug/L
82
70 -120
16
20
Styrene
<0.39
50.0
42.8
ug/L
86
70 -120
17
20
Tetrachloroethene
<0.37
50.0
47.9
ug/L
96
70 -128
15
20
Tetrahydrofuran
<1.9
100
93.9
ug/L
94
59 -139
14
20
Toluene
<0.15
50.0
45.2
ug/L
90
70 -125
16
20
trans- 1,2-Dichloroethene
<0.35
50.0
38.2
ug/L
76
70-125
17
20
trans- 1,3-Dichloropropene
<0.36
50.0
47.2
ug/L
94
62 -128
14
20
Ill
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QC Sample Results C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 500-143858-31 MSD
Matrix: Water
Analysis Batch: 429099
Sample Sample Spike MSD MSD
Analyte Result Qualifier Added Result Qualifier Unit
D
Client Sample ID: MW11D(i)
Prep Type: Total/NA
%Rec. RPD
%Rec Limits RPD Limit
Trichloroethene
<0.16
50.0
48.7
ug/L
97 70 -125 15
20
Trichlorofluoromethane
<0.43
50.0
42.1
ug/L
84 70 -126 0
20
Vinyl acetate
<0.91
50.0
44.0
ug/L
88 43 -133 9
20
Vinyl chloride
<0.20
50.0
50.5
ug/L
101 64 -126 0
20
Xylenes, Total
<0.22
100
80.5
ug/L
81 70 -125 16
20
MSD
MSD
Surrogate
%Recovery
Qualifier
Limits
1,2-Dichloroethane-d4 (Surr)
98
75- 126
4-Bromofluorobenzene (Surr)
98
72 - 124
Dibromofluoromethane
94
75 - 120
Toluene-d8 (Surr)
95
75 - 120
m
Lab Sample ID: MB 500-429285/20
Client Sample ID: Method
Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 429285
MB MB
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
1,1,1,2-Tetrachloroethane
<0.46
1.0
0.50
0.46
ug/L
04/25/18 09:55
1
1,1,1-Trichloroethane
<0.38
1.0
0.50
0.38
ug/L
04/25/18 09:55
1
1,1,2,2-Tetrachloroethane
<0.40
1.0
0.50
0.40
ug/L
04/25/18 09:55
1
1,1,2-Trichloroethane
<0.35
1.0
0.50
0.35
ug/L
04/25/18 09:55
1
1,1-Dichloroethane
<0.41
1.0
0.50
0.41
ug/L
04/25/18 09:55
1
1,1-Dichloroethene
<0.39
1.0
0.50
0.39
ug/L
04/25/18 09:55
1
1,1-Dichloropropene
<0.30
1.0
0.50
0.30
ug/L
04/25/18 09:55
1
1,2,3-Trichooropropane
<0.41
1.0
0.50
0.41
ug/L
04/25/18 09:55
1
1,2,4-Trichoorobenzene
<0.34
1.0
0.50
0.34
ug/L
04/25/18 09:55
1
1,2-Dibromo-3-Chloropropane
<2.0
5.0
2.5
2.0
ug/L
04/25/18 09:55
1
1,2-Dibromoethane
<0.39
1.0
0.50
0.39
ug/L
04/25/18 09:55
1
1,2-Dichlorobenzene
<0.33
1.0
0.50
0.33
ug/L
04/25/18 09:55
1
1,2-Dichloroethane
<0.39
1.0
0.50
0.39
ug/L
04/25/18 09:55
1
1,2-Dichloropropane
<0.43
1.0
0.50
0.43
ug/L
04/25/18 09:55
1
1,3-Dichlorobenzene
<0.40
1.0
0.50
0.40
ug/L
04/25/18 09:55
1
1,3-Dichloropropane
<0.36
1.0
0.50
0.36
ug/L
04/25/18 09:55
1
1,4-Dichlorobenzene
<0.36
1.0
0.50
0.36
ug/L
04/25/18 09:55
1
2,2-Dichloropropane
<0.44
1.0
0.50
0.44
ug/L
04/25/18 09:55
1
2-Butanone (MEK)
<2.1
5.0
2.5
2.1
ug/L
04/25/18 09:55
1
2-Chloro-1,3-butadiene
<0.23
1.0
0.50
0.23
ug/L
04/25/18 09:55
1
2-Hexanone
<1.6
5.0
2.5
1.6
ug/L
04/25/18 09:55
1
3-Chloropropene
<0.86
2.5
1.2
0.86
ug/L
04/25/18 09:55
1
4-Methyl-2-pentanone (MIBK)
<2.2
5.0
2.5
2.2
ug/L
04/25/18 09:55
1
Acetone
<1.7
5.0
2.5
1.7
ug/L
04/25/18 09:55
1
Acetonitrile
<4.2
10
8.0
4.2
ug/L
04/25/18 09:55
1
Acrolein
<23
100
50
23
ug/L
04/25/18 09:55
1
Acrylonitrile
<4.5
20
10
4.5
ug/L
04/25/18 09:55
1
Benzene
<0.15
0.50
0.25
0.15
ug/L
04/25/18 09:55
1
Bromochloromethane
<0.43
1.0
0.50
0.43
ug/L
04/25/18 09:55
1
Bromodichloromethane
<0.37
1.0
0.50
0.37
ug/L
04/25/18 09:55
1
Bromoform
<0.48
1.0
0.50
0.48
ug/L
04/25/18 09:55
1
TestAmerica Chicago
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QC Sample Results
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 500-429285/20
Matrix: Water
Analysis Batch: 429285
MB MB
Analyte Result Qualifier RL LOD MDL
Client Sample ID: Method Blank
Prep Type: Total/NA
Unit D Analyzed Dil Fac
Bromomethane
<0.80
2.0
1.0
0.80
ug/L
04/25/18 09:55
1
Carbon disulfide
<0.45
2.0
1.0
0.45
ug/L
04/25/18 09:55
1
Carbon tetrachloride
<0.38
1.0
0.50
0.38
ug/L
04/25/18 09:55
1
Chlorobenzene
<0.39
1.0
0.50
0.39
ug/L
04/25/18 09:55
1
Chloroethane
<0.51
1.0
0.51
0.51
ug/L
04/25/18 09:55
1
Chloroform
<0.37
2.0
1.0
0.37
ug/L
04/25/18 09:55
1
Chloromethane
<0.32
1.0
0.50
0.32
ug/L
04/25/18 09:55
1
cis-1,2-Dichloroethene
<0.41
1.0
0.50
0.41
ug/L
04/25/18 09:55
1
cis-1,3-Dichloropropene
<0.42
1.0
0.50
0.42
ug/L
04/25/18 09:55
1
Dibromochloromethane
<0.49
1.0
0.50
0.49
ug/L
04/25/18 09:55
1
Dibromomethane
<0.27
1.0
0.50
0.27
ug/L
04/25/18 09:55
1
Dichlorodifluoromethane
<0.67
2.0
1.0
0.67
ug/L
04/25/18 09:55
1
Ethyl methacrylate
<0.53
2.5
1.2
0.53
ug/L
04/25/18 09:55
1
Ethylbenzene
<0.18
0.50
0.25
0.18
ug/L
04/25/18 09:55
1
Hexachlorobutadiene
<0.45
1.0
0.50
0.45
ug/L
04/25/18 09:55
1
lodomethane
<0.66
2.5
1.2
0.66
ug/L
04/25/18 09:55
1
Isobutyl alcohol
<36
100
50
36
ug/L
04/25/18 09:55
1
Methacrylonitrile
<2.5
10
5.0
2.5
ug/L
04/25/18 09:55
1
Methyl methacrylate
<0.55
2.5
1.2
0.55
ug/L
04/25/18 09:55
1
Methylene Chloride
<1.6
5.0
2.5
1.6
ug/L
04/25/18 09:55
1
Propionitrile
<4.8
10
5.0
4.8
ug/L
04/25/18 09:55
1
Styrene
<0.39
1.0
0.50
0.39
ug/L
04/25/18 09:55
1
Tetrachloroethene
<0.37
1.0
0.50
0.37
ug/L
04/25/18 09:55
1
Tetrahydrofuran
<1.9
10
5.0
1.9
ug/L
04/25/18 09:55
1
Toluene
<0.15
0.50
0.25
0.15
ug/L
04/25/18 09:55
1
trans- 1,2-Dichloroethene
<0.35
1.0
0.50
0.35
ug/L
04/25/18 09:55
1
trans- 1,3-Dichloropropene
<0.36
1.0
0.50
0.36
ug/L
04/25/18 09:55
1
trans- 1,4-Dichloro-2-butene
<1.2
5.0
5.0
1.2
ug/L
04/25/18 09:55
1
Trichloroethene
<0.16
0.50
0.25
0.16
ug/L
04/25/18 09:55
1
Trichlorofluoromethane
<0.43
1.0
0.50
0.43
ug/L
04/25/18 09:55
1
Vinyl acetate
<0.91
2.0
1.0
0.91
ug/L
04/25/18 09:55
1
Vinyl chloride
<0.20
1.0
0.50
0.20
ug/L
04/25/18 09:55
1
Xylenes, Total
<0.22
1.0
0.50
0.22
ug/L
04/25/18 09:55
1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
99
75- 126
04/25/18 09:55
1
4-Bromofluorobenzene (Surr)
100
72 - 124
04/25/18 09:55
1
Dibromofluoromethane
96
75 - 120
04/25/18 09:55
1
Toluene-d8 (Surr)
93
75 - 120
04125118 09:55
1
Lab Sample ID: LCS 500-429285/4
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 429285
Spike LCS
LCS
%Rec.
Analyte
Added Result
Qualifier
Unit
D %Rec
Limits
1,1,1,2-Tetrachloroethane
50.0 47.7
ug/L
95
70 -125
1,1,1-Trichloroethane
50.0 42.5
ug/L
85
70-125
1,1,2,2-Tetrachloroethane
50.0 53.7
ug/L
107
67-127
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QC Sample Results C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 500-429285/4
Matrix: Water
Analysis Batch: 429285
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Analyte
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec.
Limits
1,1,2-Trichloroethane
50.0
51.1
ug/L
102
70-122
1,1-Dichloroethane
50.0
52.4
ug/L
105
70-125
1,1-Dichloroethene
50.0
47.4
ug/L
95
67-122
1,1-Dichloropropene
50.0
47.4
ug/L
95
70-121
1,2,3-Trichloropropane
50.0
50.4
ug/L
101
50-133
1,2,4-Trichlorobenzene
50.0
48.7
ug/L
97
66-127
1,2-Dibromo-3-Chloropropane
50.0
48.7
ug/L
97
56-123
1,2-Dibromoethane
50.0
49.7
ug/L
99
70-125
1,2-Dichlorobenzene
50.0
51.2
ug/L
102
70 -125
1,2-Dichloroethane
50.0
48.3
ug/L
97
68 -127
1,2-Dichloropropane
50.0
56.6
ug/L
113
67 -130
1,3-Dichlorobenzene
50.0
51.8
ug/L
104
70 -125
1,3-Dichloropropane
50.0
50.9
ug/L
102
62 -136
1,4-Dichlorobenzene
50.0
50.6
ug/L
101
70 -120
2,2-Dichloropropane
50.0
40.1
ug/L
80
58 -129
2-Butanone (MEK)
50.0
54.8
ug/L
110
53 -141
2-Hexanone
50.0
54.5
ug/L
109
56 -135
4-Methyl-2-pentanone (MIBK)
50.0
53.9
ug/L
108
56-133
Acetone
50.0
54.6
ug/L
109
40 -143
Benzene
50.0
48.1
ug/L
96
70 -120
Bromochloromethane
50.0
46.0
ug/L
92
65 -122
Bromodichloromethane
50.0
44.8
ug/L
90
69 -120
Bromoform
50.0
44.1
ug/L
88
56 -132
Bromomethane
50.0
42.3
ug/L
85
40 -130
Carbon disulfide
50.0
47.2
ug/L
94
66 -120
Carbon tetrachloride
50.0
43.7
ug/L
87
65 -122
Chlorobenzene
50.0
49.7
ug/L
99
70 -120
Chloroethane
50.0
38.1
ug/L
76
45 -127
Chloroform
50.0
43.1
ug/L
86
70 -120
Chloromethane
50.0
52.6
ug/L
105
54 -147
cis-1,2-Dichloroethene
50.0
46.8
ug/L
94
70 -125
cis-1,3-Dichloropropene
50.0
48.9
ug/L
98
64 -127
Dibromochloromethane
50.0
48.8
ug/L
98
68 -125
Dibromomethane
50.0
44.4
ug/L
89
70 -120
Dichlorodifluoromethane
50.0
43.2
ug/L
86
40 -150
Ethylbenzene
50.0
52.1
ug/L
104
70 -120
Hexachlorobutadiene
50.0
46.3
ug/L
93
51 -150
lodomethane
50.0
61.5
ug/L
123
61 -136
m&p-Xylene
50.0
52.6
ug/L
105
70 -125
Methylene Chloride
50.0
45.7
ug/L
91
69 -125
o-Xylene
50.0
52.8
ug/L
106
70 -120
Styrene
50.0
52.4
ug/L
105
70 -120
Tetrachloroethene
50.0
47.5
ug/L
95
70 -128
Tetrahydrofuran
100
121
ug/L
121
59 -139
Toluene
50.0
51.7
ug/L
103
70 -125
trans- 1,2-Dichloroethene
50.0
46.8
ug/L
94
70-125
trans- 1,3-Dichloropropene
50.0
47.8
ug/L
96
62 -128
Trichloroethene
50.0
48.0
ug/L
96
70 -125
TestAmerica Chicago
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QC Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill
- Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 500-429285/4
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 429285
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D
%Rec Limits
Trichlorofluoromethane
50.0
37.8
ug/L
76 70 -126
Vinyl acetate
50.0
46.8
ug/L
94 43 -133
Vinyl chloride
50.0
45.2
ug/L
90 64 -126
Xylenes, Total
100
105
ug/L
105 70 -125
LCS
LCS
F
Surrogate %Recovery
Qualifier
Limits
1,2-Dichloroethane-d4 (Surr) 93
75- 126
4-Bromofluorobenzene (Surr) 103
72 - 124
Dibromofluoromethane 89
75 - 120
Toluene-d8 (Surr) 96
75 - 120
m
Method: 8270D - Semivolatile Organic Compounds
(GC/MS)
Lab Sample ID: MB 500-42802811-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428171
Prep Batch: 428028
MB MB
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
Acenaphthene
<0.25
0.80
0.40
0.25
ug/L
04/17/18 18:26
1
Acenaphthylene
<0.21
0.80
0.40
0.21
ug/L
04/17/18 18:26
1
Acetophenone
<0.53
4.0
2.0
0.53
ug/L
04/17/18 18:26
1
2-Acetylaminofluorene
<1.7
8.0
4.0
1.7
ug/L
04/17/18 18:26
1
4-Aminobiphenyl
<3.0
8.0
4.0
3.0
ug/L
04/17/18 18:26
1
Anthracene
<0.27
0.80
0.40
0.27
ug/L
04/17/18 18:26
1
Benzo[a]anthracene
<0.045
0.16
0.080
0.045
ug/L
04/17/18 18:26
1
Benzo[a]pyrene
<0.079
0.16
0.080
0.079
ug/L
04/17/18 18:26
1
Benzo[k]fluoranthene
<0.065
0.16
0.080
0.065
ug/L
04/17/18 18:26
1
Benzo[g,h,i]perylene
<0.30
0.80
0.40
0.30
ug/L
04/17/18 18:26
1
Benzo[k]fluoranthene
<0.051
0.16
0.080
0.051
ug/L
04/17/18 18:26
1
Benzyl alcohol
<4.8
16
8.0
4.8
ug/L
04/17/18 18:26
1
Bis(2-chloroethoxy)methane
<0.23
1.6
0.80
0.23
ug/L
04/17/18 18:26
1
Bis(2-chloroethyl)ether
<0.23
1.6
0.80
0.23
ug/L
04/17/18 18:26
1
Bis(2-ethylhexyl) phthalate
<1.4
8.0
4.0
1.4
ug/L
04/17/18 18:26
1
4-Bromophenyl phenyl ether
<0.43
4.0
2.0
0.43
ug/L
04/17/18 18:26
1
Butyl benzyl phthalate
<0.38
1.6
0.80
0.38
ug/L
04/17/18 18:26
1
4-Chloroaniline
<1.6
8.0
4.0
1.6
ug/L
04/17/18 18:26
1
Chlorobenzilate
<2.7
8.0
4.0
2.7
ug/L
04/17/18 18:26
1
4-Chloro-3-methylphenol
<1.8
8.0
4.0
1.8
ug/L
04/17/18 18:26
1
2-Chloronaphthalene
<0.19
1.6
0.80
0.19
ug/L
04/17/18 18:26
1
2-Chlorophenol
<0.45
4.0
2.0
0.45
ug/L
04/17/18 18:26
1
4-Chlorophenyl phenyl ether
<0.51
4.0
2.0
0.51
ug/L
04/17/18 18:26
1
Chrysene
<0.055
0.16
0.080
0.055
ug/L
04/17/18 18:26
1
Diallate
<4.4
8.0
5.0
4.4
ug/L
04/17/18 18:26
1
Dibenz(a,h)anthracene
<0.041
0.24
0.12
0.041
ug/L
04/17/18 18:26
1
Dibenzofuran
<0.21
1.6
0.80
0.21
ug/L
04/17/18 18:26
1
3,3'-Dichlorobenzidine
<1.4
4.0
2.0
1.4
ug/L
04/17/18 18:26
1
2,4-Dichlorophenol
<2.1
8.0
4.0
2.1
ug/L
04/17/18 18:26
1
2,6-Dichlorophenol
<2.8
8.0
4.0
2.8
ug/L
04/17/18 18:26
1
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QC Sample Results
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 500-428028/1-A Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 428171 Prep Batch: 428028
MB MB
Analyte Result Qualifier RL LOD MDL Unit D Analyzed Dil Fac
Diethyl phthalate
<0.29
4.0
1.6
0.29
ug/L
04/17/18 18:26
1
Dimethoate
<1.5
8.0
4.0
1.5
ug/L
04/17/18 18:26
1
7,12-Dimethylbenz(a)anthracene
<2.4
32
16
2.4
ug/L
04/17/18 18:26
1
3,3'-Dimethylbenzidine
<14
32
16
14
ug/L
04/17/18 18:26
1
2,4-Dimethylphenol
<1.4
8.0
4.0
1.4
ug/L
04/17/18 18:26
1
Dimethyl phthalate
<0.25
4.0
1.6
0.25
ug/L
04/17/18 18:26
1
Di-n-butyl phthalate
<0.58
4.0
2.0
0.58
ug/L
04/17/18 18:26
1
4,6-Dinitro-2-methylphenol
<4.7
16
8.0
4.7
ug/L
04/17/18 18:26
1
2,4-Dinitrophenol
<6.9
16
8.0
6.9
ug/L
04/17/18 18:26
1
2,4-Dinitrotoluene
<0.20
0.80
0.40
0.20
ug/L
04/17/18 18:26
1
2,6-Dinitrotoluene
<0.059
0.80
0.40
0.059
ug/L
04/17/18 18:26
1
Di-n-octyl phthalate
<0.84
8.0
4.0
0.84
ug/L
04/17/18 18:26
1
Diphenylamine
<2.0
8.0
4.0
2.0
ug/L
04/17/18 18:26
1
Disulfoton
<1.5
8.0
4.0
1.5
ug/L
04/17/18 18:26
1
Ethyl methanesulfonate
<3.0
16
8.0
3.0
ug/L
04/17/18 18:26
1
Ethyl Parathion
<1.7
8.0
4.0
1.7
ug/L
04/17/18 18:26
1
Famphur
<24
32
25
24
ug/L
04/17/18 18:26
1
Fluoranthene
<0.36
0.80
0.40
0.36
ug/L
04/17/18 18:26
1
Fluorene
<0.20
0.80
0.40
0.20
ug/L
04/17/18 18:26
1
Hexachlorobenzene
<0.064
0.40
0.20
0.064
ug/L
04/17/18 18:26
1
Hexachlorocyclopentadiene
<5.1
16
8.0
5.1
ug/L
04/17/18 18:26
1
Hexachloroethane
<0.48
4.0
2.0
0.48
ug/L
04/17/18 18:26
1
Hexachloropropene
<3.8
16
8.0
3.8
ug/L
04/17/18 18:26
1
Indeno[1,2,3-cd]pyrene
<0.060
0.16
0.080
0.060
ug/L
04/17/18 18:26
1
Isodrin
<5.5
16
8.0
5.5
ug/L
04/17/18 18:26
1
Isophorone
<0.30
1.6
0.80
0.30
ug/L
04/17/18 18:26
1
Isosafrole
<3.1
8.0
4.0
3.1
ug/L
04/17/18 18:26
1
Kepone
<1.3
8.0
4.0
1.3
ug/L
04/17/18 18:26
1
m-Dinitrobenzene
<1.1
4.0
2.0
1.1
ug/L
04/17/18 18:26
1
Methapyrilene
<8.1
32
16
8.1
ug/L
04/17/18 18:26
1
3-Methylcholanthrene
<1.8
8.0
4.0
1.8
ug/L
04/17/18 18:26
1
Methyl methanesulfonate
<4.8
32
16
4.8
ug/L
04/17/18 18:26
1
2-Methyl naphtha lene
<0.052
1.6
0.80
0.052
ug/L
04/17/18 18:26
1
Methyl parathion
<1.9
8.0
4.0
1.9
ug/L
04/17/18 18:26
1
2-Methylphenol
<0.24
1.6
0.80
0.24
ug/L
04/17/18 18:26
1
3 & 4 Methylphenol
<0.36
1.6
0.80
0.36
ug/L
04/17/18 18:26
1
Naphthalene
<0.25
0.80
0.40
0.25
ug/L
04/17/18 18:26
1
1,4-Naphthoquinone
<31
32
32
31
ug/L
04/17/18 18:26
1
1-Naphthylamine
<4.7
16
8.0
4.7
ug/L
04/17/18 18:26
1
2-Naphthylamine
<7.3
16
8.0
7.3
ug/L
04/17/18 18:26
1
2-Nitroaniline
<1.0
4.0
2.0
1.0
ug/L
04/17/18 18:26
1
3-Nitroaniline
<1.4
8.0
4.0
1.4
ug/L
04/17/18 18:26
1
4-Nitroaniline
<1.3
8.0
4.0
1.3
ug/L
04/17/18 18:26
1
Nitrobenzene
<0.36
0.80
0.40
0.36
ug/L
04/17/18 18:26
1
5-Nitro-o-toluidine
<2.5
8.0
4.0
2.5
ug/L
04/17/18 18:26
1
2-Nitrophenol
<2.0
8.0
4.0
2.0
ug/L
04/17/18 18:26
1
4-Nitrophenol
<5.9
16
8.0
5.9
ug/L
04/17/18 18:26
1
N-Nitrosodiethylamine
<6.9
16
8.0
6.9
ug/L
04/17/18 18:26
1
TestAmerica Chicago
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QC Sample Results
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 500-428028/1-A Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 428171 Prep Batch: 428028
MB MB
Analyte Result Qualifier RL LOD MDL Unit D Analyzed Dil Fac
N-Nitrosodimethylamine
<3.8
8.0
4.0
3.8
ug/L
04/17/18 18:26
1
N-Nitrosodi-n-butylamine
<3.4
8.0
4.0
3.4
ug/L
04/17/18 18:26
1
N-Nitrosodi-n-propylamine
<0.12
0.40
0.20
0.12
ug/L
04/17/18 18:26
1
N-Nitrosodiphenylamine
<0.30
1.6
0.80
0.30
ug/L
04/17/18 18:26
1
N-Nitrosomethylethylamine
<6.0
16
8.0
6.0
ug/L
04/17/18 18:26
1
N-Nitrosopiperidine
<2.8
8.0
4.0
2.8
ug/L
04/17/18 18:26
1
N-Nitrosopyrrolidine
<2.7
8.0
4.0
2.7
ug/L
04/17/18 18:26
1
o,o',o"-Triethylphosphorothioate
<4.4
16
8.0
4.4
ug/L
04/17/18 18:26
1
o-Toluidine
<6.3
32
16
6.3
ug/L
04/17/18 18:26
1
2,2'-oxybis[l-chloropropane]
<0.30
1.6
0.80
0.30
ug/L
04/17/18 18:26
1
p-Dimethylamino azobenzene
<2.4
8.0
4.0
2.4
ug/L
04/17/18 18:26
1
Pentachlorobenzene
<2.2
8.0
4.0
2.2
ug/L
04/17/18 18:26
1
Pentachloronitrobenzene
<2.9
8.0
4.0
2.9
ug/L
04/17/18 18:26
1
Phenacetin
<1.8
8.0
4.0
1.8
ug/L
04/17/18 18:26
1
Phenanthrene
<0.24
0.80
0.40
0.24
ug/L
04/17/18 18:26
1
Phenol
<0.54
4.0
2.0
0.54
ug/L
04/17/18 18:26
1
Phorate
<1.7
8.0
4.0
1.7
ug/L
04/17/18 18:26
1
p-Phenylene diamine
<13
64
32
13
ug/L
04/17/18 18:26
1
Pronamide
<1.7
8.0
8.0
1.7
ug/L
04/17/18 18:26
1
Pyrene
<0.34
0.80
0.40
0.34
ug/L
04/17/18 18:26
1
Safrole
<3.2
8.0
4.0
3.2
ug/L
04/17/18 18:26
1
sym-Trinitrobenzene
<1.5
8.0
4.0
1.5
ug/L
04/17/18 18:26
1
2,3,7,8-TCDD (Screen)
<8.0
8.0
8.0
8.0
ug/L
04/17/18 18:26
1
1,2,4,5-Tetrachlorobenzene
<0.46
4.0
2.0
0.46
ug/L
04/17/18 18:26
1
2,3,4,6-Tetrachlorophenol
<0.60
4.0
2.0
0.60
ug/L
04/17/18 18:26
1
Thionazin
<2.1
8.0
4.0
2.1
ug/L
04/17/18 18:26
1
2,4,5-Trichlorophenol
<2.1
8.0
4.0
2.1
ug/L
04/17/18 18:26
1
2,4,6-Trichlorophenol
<0.57
4.0
2.0
0.57
ug/L
04/17/18 18:26
1
MB MB
Surrogate %Recovery
Qualifier
Limits
Prepared
Analyzed Dil Fac
2-Fluorobiphenyl
84
34 - 110
04116118 16:56
04117118 18:26 1
2-Fluorophenol
65
27- 110
04116118 16:56
04117118 18:26 1
Nitrobenzene-d5
88
36 - 120
04116118 16:56
04117118 18:26 1
Phenol-d5
55
20- 100
04116118 16:56
04117118 18:26 1
Terphenyl-d14
98
40- 145
04116118 16:56
04117118 18:26 1
2,4, 6-Tribromophenol
86
40 - 145
04116118 16:56
04117118 18:26 1
Lab Sample ID: LCS 500-428028/2-A
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428171
Prep Batch: 428028
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Acenaphthene
32.0
26.3
ug/L
82
46-110
Acenaphthylene
32.0
26.4
ug/L
83
47 -110
Acetophenone
32.0
26.0
ug/L
81
60-110
Anthracene
32.0
27.3
ug/L
85
67-110
Benzo[a]anthracene
32.0
28.0
ug/L
88
70 -120
Benzo[a]pyrene
32.0
30.0
ug/L
94
70 -120
TestAmerica Chicago
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QC Sample Results
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 500-428028/2-A Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 428171 Prep Batch: 428028
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Benzo[k]fluoranthene
32.0
28.9
ug/L
90
69 -123
Benzo[g,h,i]perylene
32.0
29.7
ug/L
93
70-120
Benzo[k]fluoranthene
32.0
29.1
ug/L
91
70 -120
Benzyl alcohol
32.0
26.6
ug/L
83
33 -127
Bis(2-chloroethoxy)methane
32.0
27.3
ug/L
85
60 -110
Bis(2-chloroethyl)ether
32.0
26.3
ug/L
82
49 -110
Bis(2-ethylhexyl) phthalate
32.0
31.0
ug/L
97
69 -120
4-Bromophenyl phenyl ether
32.0
28.2
ug/L
88
58 -120
Butyl benzyl phthalate
32.0
30.4
ug/L
95
68 -120
4-Chloroaniline
32.0
23.9
ug/L
75
35 -128
4-Chloro-3-methylphenol
32.0
28.1
ug/L
88
64 -120
2-Chloronaphthalene
32.0
25.6
ug/L
80
39 -110
2-Chlorophenol
32.0
25.5
ug/L
80
59 -110
4-Chlorophenyl phenyl ether
32.0
27.4
ug/L
86
47 -112
Chrysene
32.0
28.4
ug/L
89
68 -120
Dibenz(a,h)anthracene
32.0
29.4
ug/L
92
70-127
Dibenzofuran
32.0
27.0
ug/L
84
51 -110
3,3'-Dichlorobenzidine
32.0
27.4
ug/L
86
60 -132
2,4-Dichlorophenol
32.0
27.0
ug/L
84
62.110
2,6-Dichlorophenol
32.0
26.2
ug/L
82
60 -110
Diethyl phthalate
32.0
27.5
ug/L
86
62.120
2,4-Dimethylphenol
32.0
26.3
ug/L
82
51 -110
Dimethyl phthalate
32.0
27.8
ug/L
87
63 -120
Di-n-butyl phthalate
32.0
28.5
ug/L
89
70 -120
4,6-Dinitro-2-methylphenol
64.0
56.5
ug/L
88
50 -117
2,4-Dinitrophenol
64.0
55.8
ug/L
87
37 -130
2,4-Dinitrotoluene
32.0
28.7
ug/L
90
63-122
2,6-Dinitrotoluene
32.0
29.3
ug/L
92
63-119
Di-n-octyl phthalate
32.0
27.8
ug/L
87
70 -122
Fluoranthene
32.0
27.8
ug/L
87
68 -120
Fluorene
32.0
27.0
ug/L
84
53 -120
Hexachlorobenzene
32.0
27.9
ug/L
87
61 -120
Hexachlorocyclopentadiene
32.0
22.9
ug/L
72
10 -100
Hexachloroethane
32.0
21.5
ug/L
67
20 -100
Indeno[1,2,3-cd]pyrene
32.0
30.5
ug/L
95
65-133
Isophorone
32.0
26.3
ug/L
82
57.110
2-Methylnaphthalene
32.0
24.1
ug/L
75
34 -110
2-Methylphenol
32.0
25.9
ug/L
81
53 -110
3 & 4 Methylphenol
32.0
25.5
ug/L
80
53 -110
Naphthalene
32.0
23.4
ug/L
73
36 -110
2-Nitroaniline
32.0
28.7
ug/L
90
59 -122
3-Nitroaniline
32.0
20.1
ug/L
63
47 -123
4-Nitroaniline
32.0
18.9
ug/L
59
52 -147
Nitrobenzene
32.0
25.8
ug/L
81
53 -110
2-Nitrophenol
32.0
26.1
ug/L
81
58 -110
4-Nitrophenol
64.0
37.7
ug/L
59
20 -110
N-Nitrosodimethylamine
32.0
24.4
ug/L
76
41 -110
N-Nitrosodi-n-propylamine
32.0
27.5
ug/L
86
58-110
TestAmerica Chicago
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QC Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
SDG:
TestAmerica Job ID: 500-143858-1
NCDEQ Solid Waste Facility = # 60-13
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 500-428028/2-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428171
Prep Batch: 428028
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
N-Nitrosodiphenylamine
32.0
27.6
ug/L
86
66-110
2,2'-oxybis[1-chloropropane]
32.0
25.5
ug/L
80
38 -110
Phenanthrene
32.0
27.5
ug/L
86
65 -120
Phenol
32.0
18.4
ug/L
57
33 -100
Pyrene
32.0
29.5
ug/L
92
70 -110
1,2,4,5-Tetrachlorobenzene
32.0
24.8
ug/L
77
30-110
2,3,4,6-Tetrachlorophenol
32.0
28.2
ug/L
88
44 -118
2,4,5-Trichlorophenol
32.0
28.7
ug/L
90
63-120
2,4,6-Trichlorophenol
32.0
28.2
ug/L
88
62 -110
LCS LCS
Surrogate %Recovery Qualifier
Limits
m
2-Fluorobiphenyl 94
34 - 110
2-Fluorophenol 86
27- 110
Nitrobenzene-d5 98
36 - 120
Phenol-d5 68
20-100
Terphenyl-d14 107
40- 145
2,4,6-Tribromophenol 105
40- 145
Lab Sample ID: LCSD 500-42802813-A
Client Sample ID: Lab Control
Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428171
Prep Batch: 428028
Spike
LCSD
LCSD
%Rec.
RPD
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
RPD Limit
Acenaphthene
32.0
27.1
ug/L
85
46-110
3 20
Acenaphthylene
32.0
27.3
ug/L
85
47-110
3 20
Acetophenone
32.0
25.8
ug/L
81
60-110
1 20
Anthracene
32.0
28.5
ug/L
89
67-110
4 20
Benzo[a]anthracene
32.0
29.6
ug/L
93
70 -120
5 20
Benzo[a]pyrene
32.0
31.2
ug/L
98
70 -120
4 20
Benzo[b]fluoranthene
32.0
31.1
ug/L
97
69 -123
7 20
Benzo[g,h,i]perylene
32.0
30.4
ug/L
95
70 -120
2 20
Benzo[k]fluoranthene
32.0
30.2
ug/L
94
70 -120
4 20
Benzyl alcohol
32.0
26.9
ug/L
84
33 -127
1 20
Bis(2-chloroethoxy)methane
32.0
27.9
ug/L
87
60 -110
2 20
Bis(2-chloroethyl)ether
32.0
25.6
ug/L
80
49 -110
3 20
Bis(2-ethylhexyl) phthalate
32.0
31.7
ug/L
99
69 -120
2 20
4-Bromophenyl phenyl ether
32.0
29.1
ug/L
91
58 -120
3 20
Butyl benzyl phthalate
32.0
31.6
ug/L
99
68 -120
4 20
4-Chloroaniline
32.0
25.4
ug/L
79
35 -128
6 20
4-Chloro-3-methylphenol
32.0
28.3
ug/L
89
64 -120
1 20
2-Chloronaphthalene
32.0
26.5
ug/L
83
39 -110
3 20
2-Chlorophenol
32.0
25.3
ug/L
79
59 -110
1 20
4-Chlorophenyl phenyl ether
32.0
28.1
ug/L
88
47 -112
3 20
Chrysene
32.0
29.7
ug/L
93
68 -120
5 20
Dibenz(a,h)anthracene
32.0
30.7
ug/L
96
70-127
4 20
Dibenzofuran
32.0
27.6
ug/L
86
51 -110
2 20
3,3'-Dichlorobenzidine
32.0
28.6
ug/L
89
60 -132
4 20
2,4-Dichlorophenol
32.0
27.3
ug/L
85
62 -110
1 20
TestAmerica Chicago
Page 206 of 258 7/5/2018

QC Sample Results C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 500-428028/3-A
Matrix: Water
Analysis Batch: 428171
Analyte
2,6-Dichlorophenol
Diethyl phthalate
2,4-Dimethylphenol
Dimethyl phthalate
Di-n-butyl phthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno[1,2,3-cd]pyrene
Isophorone
2-Methyl naphtha lene
2-Methylphenol
3 & 4 Methylphenol
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-N itrosod i-n-propylamine
N-Nitrosodiphenylamine
2,2'-oxybis[l -chloropropane]
Phenanthrene
Phenol
Pyrene
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-d 14
2, 4, 6-Tribromophenol
LCSD LCSD
%Recovery Qualifier
93
82
95
65
107
103
Spike
Added
32.0
32.0
32.0
32.0
32.0
64.0
64.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
64.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
Limits
34 - 110
27- 110
36 - 120
20 - 100
40 - 145
40 - 145
LCSD LCSD
Result Qualifier
27.0
28.2
26.8
29.0
29.5
59.8
58.3
30.1
30.3
28.9
29.0
27.9
28.8
23.7
21.5
31.5
27.5
24.4
26.4
25.9
23.9
29.4
21.7
20.0
26.5
26.3
39.7
25.1
27.9
29.3
25.6
28.8
20.8
30.8
25.4
29.3
29.9
28.9
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 428028
%Rec.
RPD
Unit
D %Rec
Limits
RPD
Limit
ug/L
85
60-110
3
20
ug/L
88
62 -120
2
20
ug/L
84
51-110
2
20
ug/L
91
63 -120
4
20
ug/L
92
70-120
3
20
ug/L
93
50-117
6
20
ug/L
91
37-130
4
20
ug/L
94
63-122
5
20
ug/L
95
63-119
3
20
ug/L
90
70-122
4
20
ug/L
91
68-120
4
20
ug/L
87
53-120
3
20
ug/L
90
61 -120
3
20
ug/L
74
10 -100
4
20
ug/L
67
20-100
0
20
ug/L
99
65-133
3
20
ug/L
86
57-110
5
20
ug/L
76
34 -110
1
20
ug/L
83
53-110
2
20
ug/L
81
53-110
2
20
ug/L
75
36-110
2
20
ug/L
92
59-122
2
20
ug/L
68
47-123
8
20
ug/L
63
52 -147
6
20
ug/L
83
53-110
3
20
ug/L
82
58-110
1
20
ug/L
62
20-110
5
20
ug/L
79
41 -110
3
20
ug/L
87
58-110
2
20
ug/L
92
66-110
6
20
ug/L
80
38-110
0
20
ug/L
90
65-120
5
20
ug/L
65
33 -100
12
20
ug/L
96
70-110
4
20
ug/L
79
30-110
2
20
ug/L
91
44-118
4
20
ug/L
93
63-120
4
20
ug/L
90
62 -110
3
20
Li
Page 207 of 258
TestAmerica Chicago
7/5/2018

QC Sample Results C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 500-428463/1-A
Matrix: Water
Analysis Batch: 428521
Analyte
MB
Result
MB
Qualifier
Acenaphthene
<0.25
Acenaphthylene
0.640
J
Acetophenone
<0.53
2-Acetylaminofluorene
<1.7
4-Aminobiphenyl
<3.0
Anthracene
<0.27
Benzo[a]anthracene
<0.045
Benzo[a]pyrene
<0.079
Benzo[b]fluoranthene
<0.065
Benzo[g,h,i]perylene
<0.30
Benzo[k]fluoranthene
<0.051
Benzyl alcohol
<4.8
Bis(2-chloroethoxy)methane
<0.23
Bis(2-chloroethyl)ether
<0.23
Bis(2-ethylhexyl) phthalate
<1.4
4-Bromophenyl phenyl ether
<0.43
Butyl benzyl phthalate
1.14
J
4-Chloroaniline
<1.6
Chlorobenzilate
<2.7
4-Chloro-3-methylphenol
<1.8
2-Chloronaphthalene
<0.19
2-Chlorophenol
<0.45
4-Chlorophenyl phenyl ether
<0.51
Chrysene
<0.055
Diallate
<4.4
Dibenz(a,h)anthracene
<0.041
Dibenzofuran
<0.21
3,3'-Dichlorobenzidine
<1.4
2,4-Dichlorophenol
<2.1
2,6-Dichlorophenol
<2.8
Diethyl phthalate
<0.29
Dimethoate
<1.5
7,12-Dimethylbenz(a)anthracene
<2.4
3,3'-Dimethylbenzidine
<14
2,4-Dimethylphenol
<1.4
Dimethyl phthalate
<0.25
Di-n-butyl phthalate
<0.58
4,6-Dinitro-2-methylphenol
<4.7
2,4-Dinitrophenol
<6.9
2,4-Dinitrotoluene
<0.20
2,6-Dinitrotoluene
<0.059
Di-n-octyl phthalate
<0.84
Diphenylamine
<2.0
Disulfoton
<1.5
Ethyl methanesulfonate
<3.0
Ethyl Parathion
<1.7
Famphur
<24
Fluoranthene
<0.36
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 428463
RL
LOD
MDL
Unit
D Analyzed
Dil Fac
0.80
0.40
0.25
ug/L
04/19/1813:07
1
0.80
0.40
0.21
ug/L
04/19/1813:07
1
4.0
2.0
0.53
ug/L
04/19/1813:07
1
8.0
4.0
1.7
ug/L
04/19/1813:07
1
8.0
4.0
3.0
ug/L
04/19/1813:07
1
0.80
0.40
0.27
ug/L
04/19/1813:07
1
0.16
0.080
0.045
ug/L
04/19/1813:07
1
0.16
0.080
0.079
ug/L
04/19/1813:07
1
0.16
0.080
0.065
ug/L
04/19/1813:07
1
0.80
0.40
0.30
ug/L
04/19/1813:07
1
0.16
0.080
0.051
ug/L
04/19/1813:07
1
16
8.0
4.8
ug/L
04/19/1813:07
1
1.6
0.80
0.23
ug/L
04/19/1813:07
1
1.6
0.80
0.23
ug/L
04/19/1813:07
1
8.0
4.0
1.4
ug/L
04/19/1813:07
1
4.0
2.0
0.43
ug/L
04/19/1813:07
1
1.6
0.80
0.38
ug/L
04/19/1813:07
1
8.0
4.0
1.6
ug/L
04/19/1813:07
1
8.0
4.0
2.7
ug/L
04/19/1813:07
1
8.0
4.0
1.8
ug/L
04/19/1813:07
1
1.6
0.80
0.19
ug/L
04/19/1813:07
1
4.0
2.0
0.45
ug/L
04/19/1813:07
1
4.0
2.0
0.51
ug/L
04/19/1813:07
1
0.16
0.080
0.055
ug/L
04/19/1813:07
1
8.0
5.0
4.4
ug/L
04/19/1813:07
1
0.24
0.12
0.041
ug/L
04/19/1813:07
1
1.6
0.80
0.21
ug/L
04/19/1813:07
1
4.0
2.0
1.4
ug/L
04/19/1813:07
1
8.0
4.0
2.1
ug/L
04/19/1813:07
1
8.0
4.0
2.8
ug/L
04/19/1813:07
1
4.0
1.6
0.29
ug/L
04/19/1813:07
1
8.0
4.0
1.5
ug/L
04/19/1813:07
1
32
16
2.4
ug/L
04/19/1813:07
1
32
16
14
ug/L
04/19/1813:07
1
8.0
4.0
1.4
ug/L
04/19/1813:07
1
4.0
1.6
0.25
ug/L
04/19/1813:07
1
4.0
2.0
0.58
ug/L
04/19/1813:07
1
16
8.0
4.7
ug/L
04/19/1813:07
1
16
8.0
6.9
ug/L
04/19/1813:07
1
0.80
0.40
0.20
ug/L
04/19/1813:07
1
0.80
0.40
0.059
ug/L
04/19/1813:07
1
8.0
4.0
0.84
ug/L
04/19/1813:07
1
8.0
4.0
2.0
ug/L
04/19/1813:07
1
8.0
4.0
1.5
ug/L
04/19/1813:07
1
16
8.0
3.0
ug/L
04/19/1813:07
1
8.0
4.0
1.7
ug/L
04/19/1813:07
1
32
25
24
ug/L
04/19/1813:07
1
0.80
0.40
0.36
ug/L
04/19/1813:07
1
Page 208 of 258
TestAmerica Chicago
7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 500-428463/1-A Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 428521 Prep Batch: 428463
MB MB
Analyte Result Qualifier RL LOD MDL Unit D Analyzed Dil Fac
Fluorene
0.615 J
0.80
0.40
0.20
ug/L
04/19/18 13:07
1
Hexachlorobenzene
<0.064
0.40
0.20
0.064
ug/L
04/19/18 13:07
1
Hexachlorocyclopentadiene
<5.1
16
8.0
5.1
ug/L
04/19/18 13:07
1
Hexachloroethane
<0.48
4.0
2.0
0.48
ug/L
04/19/18 13:07
1
Hexachloropropene
<3.8
16
8.0
3.8
ug/L
04/19/18 13:07
1
Indeno[1,2,3-cd]pyrene
<0.060
0.16
0.080
0.060
ug/L
04/19/18 13:07
1
Isodrin
<5.5
16
8.0
5.5
ug/L
04/19/18 13:07
1
Isophorone
<0.30
1.6
0.80
0.30
ug/L
04/19/18 13:07
1
Isosafrole
<3.1
8.0
4.0
3.1
ug/L
04/19/18 13:07
1
Kepone
<1.3
8.0
4.0
1.3
ug/L
04/19/18 13:07
1
m-Dinitrobenzene
<1.1
4.0
2.0
1.1
ug/L
04/19/18 13:07
1
Methapyrilene
<8.1
32
16
8.1
ug/L
04/19/18 13:07
1
3-Methylcholanthrene
<1.8
8.0
4.0
1.8
ug/L
04/19/18 13:07
1
Methyl methanesulfonate
<4.8
32
16
4.8
ug/L
04/19/18 13:07
1
2-Methylnaphthalene
<0.052
1.6
0.80
0.052
ug/L
04/19/18 13:07
1
Methyl parathion
<1.9
8.0
4.0
1.9
ug/L
04/19/18 13:07
1
2-Methylphenol
<0.24
1.6
0.80
0.24
ug/L
04/19/18 13:07
1
3 & 4 Methylphenol
<0.36
1.6
0.80
0.36
ug/L
04/19/18 13:07
1
Naphthalene
<0.25
0.80
0.40
0.25
ug/L
04/19/18 13:07
1
1,4-Naphthoquinone
<31
32
32
31
ug/L
04/19/18 13:07
1
1-Naphthylamine
<4.7
16
8.0
4.7
ug/L
04/19/18 13:07
1
2-Naphthylamine
<7.3
16
8.0
7.3
ug/L
04/19/18 13:07
1
2-Nitroaniline
<1.0
4.0
2.0
1.0
ug/L
04/19/18 13:07
1
3-Nitroaniline
<1.4
8.0
4.0
1.4
ug/L
04/19/18 13:07
1
4-Nitroaniline
<1.3
8.0
4.0
1.3
ug/L
04/19/18 13:07
1
Nitrobenzene
<0.36
0.80
0.40
0.36
ug/L
04/19/18 13:07
1
5-Nitro-o-toluidine
<2.5
8.0
4.0
2.5
ug/L
04/19/18 13:07
1
2-Nitrophenol
<2.0
8.0
4.0
2.0
ug/L
04/19/18 13:07
1
4-Nitrophenol
<5.9
16
8.0
5.9
ug/L
04/19/18 13:07
1
N-Nitrosodiethylamine
<6.9
16
8.0
6.9
ug/L
04/19/18 13:07
1
N-Nitrosodimethylamine
<3.8
8.0
4.0
3.8
ug/L
04/19/18 13:07
1
N-Nitrosodi-n-butylamine
<3.4
8.0
4.0
3.4
ug/L
04/19/18 13:07
1
N-Nitrosodi-n-propylamine
<0.12
0.40
0.20
0.12
ug/L
04/19/18 13:07
1
N-Nitrosodiphenylamine
<0.30
1.6
0.80
0.30
ug/L
04/19/18 13:07
1
N-Nitrosomethylethylamine
<6.0
16
8.0
6.0
ug/L
04/19/18 13:07
1
N-Nitrosopiperidine
<2.8
8.0
4.0
2.8
ug/L
04/19/18 13:07
1
N-Nitrosopyrrolidine
<2.7
8.0
4.0
2.7
ug/L
04/19/18 13:07
1
o,o',o"-Triethylphosphorothioate
<4.4
16
8.0
4.4
ug/L
04/19/18 13:07
1
o-Toluidine
<6.3
32
16
6.3
ug/L
04/19/18 13:07
1
2,2'-oxybis[1-chloropropane]
<0.30
1.6
0.80
0.30
ug/L
04/19/18 13:07
1
p-Dimethylamino azobenzene
<2.4
8.0
4.0
2.4
ug/L
04/19/18 13:07
1
Pentachlorobenzene
<2.2
8.0
4.0
2.2
ug/L
04/19/18 13:07
1
Pentachloronitrobenzene
<2.9
8.0
4.0
2.9
ug/L
04/19/18 13:07
1
Phenacetin
<1.8
8.0
4.0
1.8
ug/L
04/19/18 13:07
1
Phenanthrene
<0.24
0.80
0.40
0.24
ug/L
04/19/18 13:07
1
Phenol
<0.54
4.0
2.0
0.54
ug/L
04/19/18 13:07
1
Phorate
<1.7
8.0
4.0
1.7
ug/L
04/19/18 13:07
1
p-Phenylene diamine
<13
64
32
13
ug/L
04/19/18 13:07
1
TestAmerica Chicago
Page 209 of 258 7/5/2018

QC Sample Results C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 500-428463/1-A Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 428521 Prep Batch: 428463
MB MB
Analyte Result Qualifier RL LOD MDL Unit D Analyzed Dil Fac
Pronamide
<1.7
8.0
8.0
1.7
ug/L
04/19/1813:07 1
Pyrene
<0.34
0.80
0.40
0.34
ug/L
04/19/1813:07 1
Safrole
<3.2
8.0
4.0
3.2
ug/L
04/19/1813:07 1
sym-Trinitrobenzene
<1.5
8.0
4.0
1.5
ug/L
04/19/1813:07 1
2,3,7,8-TCDD (Screen)
<8.0
8.0
8.0
8.0
ug/L
04/19/18 13:07 1
1,2,4,5-Tetrachlorobenzene
<0.46
4.0
2.0
0.46
ug/L
04/19/1813:07 1
2,3,4,6-Tetrachlorophenol
<0.60
4.0
2.0
0.60
ug/L
04/19/1813:07 1
Thionazin
<2.1
8.0
4.0
2.1
ug/L
04/19/1813:07 1
2,4,5-Trichlorophenol
<2.1
8.0
4.0
2.1
ug/L
04/19/1813:07 1
2,4,6-Trichlorophenol
<0.57
4.0
2.0
0.57
ug/L
04/19/1813:07 1
MB MB
m
Surrogate %Recovery
Qualifier
Limits
Prepared
Analyzed Dil Fac
2-Fluorobiphenyl
90
34 - 110
04118118 17:41
04119118 13:07 1
2-Fluorophenol
70
27- 110
04118118 17:41
04119118 13:07 1
Nitrobenzene-d5
91
36 - 120
04118118 17:41
04119118 13:07 1
Phenol-d5
45
20 - 100
04118118 17:41
04119118 13:07 1
Terphenyl-d14
132
40- 145
04118118 17:41
04119118 13:07 1
2,4,6-Tribromophenol
90
40- 145
04118118 17:41
04119118 13:07 1
Lab Sample ID: LCS 500-428463/2-A
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428521
Prep Batch: 428463
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits
Acenaphthene
32.0
22.6
ug/L
71
46-110
Acenaphthylene
32.0
20.1
ug/L
63
47 -110
Acetophenone
32.0
23.4
ug/L
73
60-110
Anthracene
32.0
29.1
ug/L
91
67 -110
Benzo[a]anthracene
32.0
31.1
ug/L
97
70 -120
Benzo[a]pyrene
32.0
28.4
ug/L
89
70 -120
Benzo[b]fluoranthene
32.0
28.2
ug/L
88
69 -123
Benzo[g,h,i]perylene
32.0
31.2
ug/L
97
70-120
Benzo[k]fluoranthene
32.0
30.9
ug/L
96
70 -120
Benzyl alcohol
32.0
22.3
ug/L
70
33 -127
Bis(2-chloroethoxy)methane
32.0
25.6
ug/L
80
60 -110
Bis(2-chloroethyl)ether
32.0
24.1
ug/L
75
49 -110
Bis(2-ethylhexyl) phthalate
32.0
28.5
ug/L
89
69 -120
4-Bromophenyl phenyl ether
32.0
24.1
ug/L
75
58 -120
Butyl benzyl phthalate
32.0
26.4
ug/L
83
68 -120
4-Chloroaniline
32.0
19.4
ug/L
61
35 -128
4-Chloro-3-methylphenol
32.0
24.0
ug/L
75
64 -120
2-Chloronaphthalene
32.0
17.9
ug/L
56
39 -110
2-Chlorophenol
32.0
23.5
ug/L
73
59 -110
4-Chlorophenyl phenyl ether
32.0
21.4
ug/L
67
47 -112
Chrysene
32.0
29.9
ug/L
93
68 -120
Dibenz(a,h)anthracene
32.0
28.8
ug/L
90
70-127
Dibenzofuran
32.0
22.6
ug/L
71
51 -110
3,3'-Dichlorobenzidine
32.0
33.6
ug/L
105
60 -132
TestAmerica Chicago
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QC Sample Results C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 500-428463/2-A
Matrix: Water
Analysis Batch: 428521
Analyte
2,4-Dichlorophenol
2,6-Dichlorophenol
Diethyl phthalate
2,4-Dimethylphenol
Dimethyl phthalate
Di-n-butyl phthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno[1,2,3-cd]pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol
3 & 4 Methylphenol
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-N itrosod i-n-propylamine
N-Nitrosodiphenylamine
2,2'-oxybis[1-chloropropane]
Phenanthrene
Phenol
Pyrene
1,2,4,5-Tetrachlorobenzene
2,3,4,6-Tetrachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogate
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-d 14
2, 4, 6-Tribromophenol
LCS LCS
%Recovery Qualifier
86
67
88
48
110
91
Spike
Added
32.0
32.0
32.0
32.0
32.0
32.0
64.0
64.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
64.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
32.0
Limits
34 - 110
27- 110
36 - 120
20-100
40-145
40-145
LCS LCS
Result Qualifier
21.8
22.1
29.1
21.8
28.6
29.6
58.5
58.6
25.8
27.7
26.7
26.4
21.6
28.4
13.9 J
13.1
29.6
25.6
18.3
24.0
22.5
18.3
25.1
29.0
25.4
25.0
22.4
27.4
19.0
25.3
33.1
20.5
29.6
15.1
29.4
17.6
27.3
22.9
23.1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 428463
%Rec.
Unit
D %Rec
Limits
ug/L
68
62-110
ug/L
69
60-110
ug/L
91
62-120
ug/L
68
51-110
ug/L
90
63-120
ug/L
92
70-120
ug/L
91
50-117
ug/L
92
37-130
ug/L
81
63-122
ug/L
87
63-119
ug/L
83
70-122
ug/L
82
68-120
ug/L
67
53-120
ug/L
89
61 -120
ug/L
43
10-100
ug/L
41
20-100
ug/L
92
65-133
ug/L
80
57-110
ug/L
57
34-110
ug/L
75
53-110
ug/L
70
53-110
ug/L
57
36-110
ug/L
78
59-122
ug/L
91
47-123
ug/L
79
52 -147
ug/L
78
53-110
ug/L
70
58-110
ug/L
43
20-110
ug/L
59
41-110
ug/L
79
58-110
ug/L
103
66-110
ug/L
64
38-110
ug/L
93
65-120
ug/L
47
33-100
ug/L
92
70-110
ug/L
55
30-110
ug/L
85
44-118
ug/L
72
63-120
ug/L
72
62-110
Page 211 of 258
TestAmerica Chicago
7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 500-42846313-A
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428521
Prep Batch: 428463
Spike
LCSD
LCSD
%Rec.
RPD
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
RPD
Limit
Acenaphthene
32.0
22.5
ug/L
70
46 - 110
1
20
Acenaphthylene
32.0
19.9
ug/L
62
47.110
1
20
Acetophenone
32.0
22.2
ug/L
69
60-110
6
20
Anthracene
32.0
27.9
ug/L
87
67-110
4
20
Benzo[a]anthracene
32.0
30.6
ug/L
96
70 -120
2
20
Benzo[a]pyrene
32.0
28.1
ug/L
88
70 -120
1
20
Benzo[b]fluoranthene
32.0
27.5
ug/L
86
69 -123
2
20
Benzo[g,h,i]perylene
32.0
30.4
ug/L
95
70-120
2
20
Benzo[k]fluoranthene
32.0
30.0
ug/L
94
70 -120
3
20
Benzyl alcohol
32.0
21.1
ug/L
66
33 -127
6
20
Bis(2-chloroethoxy)methane
32.0
24.4
ug/L
76
60 -110
5
20
Bis(2-chloroethyl)ether
32.0
22.7
ug/L
71
49 -110
6
20
Bis(2-ethylhexyl) phthalate
32.0
27.6
ug/L
86
69 -120
3
20
4-Bromophenyl phenyl ether
32.0
23.1
ug/L
72
58 -120
4
20
Butyl benzyl phthalate
32.0
25.7
ug/L
80
68 -120
3
20
4-Chloroaniline
32.0
20.0
ug/L
62
35 -128
3
20
4-Chloro-3-methylphenol
32.0
23.3
ug/L
73
64.120
3
20
2-Chloronaphthalene
32.0
18.7
ug/L
59
39 -110
5
20
2-Chlorophenol
32.0
22.2
ug/L
69
59 -110
6
20
4-Chlorophenyl phenyl ether
32.0
20.5
ug/L
64
47 -112
4
20
Chrysene
32.0
29.2
ug/L
91
68 -120
2
20
Dibenz(a,h)anthracene
32.0
28.2
ug/L
88
70-127
2
20
Dibenzofuran
32.0
21.9
ug/L
68
51 -110
3
20
3,3'-Dichlorobenzidine
32.0
35.3
ug/L
110
60 -132
5
20
2,4-Dichlorophenol
32.0
20.8
ug/L
65
62 -110
5
20
2,6-Dichlorophenol
32.0
20.8
ug/L
65
60 -110
6
20
Diethyl phthalate
32.0
28.1
ug/L
88
62 -120
4
20
2,4-Dimethylphenol
32.0
21.3
ug/L
67
51 -110
2
20
Dimethyl phthalate
32.0
27.7
ug/L
87
63 -120
3
20
Di-n-butyl phthalate
32.0
28.1
ug/L
88
70 -120
5
20
4,6-Dinitro-2-methylphenol
64.0
56.1
ug/L
88
50 -117
4
20
2,4-Dinitrophenol
64.0
56.3
ug/L
88
37.130
4
20
2,4-Dinitrotoluene
32.0
25.1
ug/L
79
63-122
3
20
2,6-Dinitrotoluene
32.0
26.9
ug/L
84
63-119
3
20
Di-n-octyl phthalate
32.0
26.2
ug/L
82
70 -122
2
20
Fluoranthene
32.0
25.2
ug/L
79
68 -120
4
20
Fluorene
32.0
20.8
ug/L
65
53 -120
4
20
Hexachlorobenzene
32.0
27.4
ug/L
86
61 -120
3
20
Hexachlorocyclopentadiene
32.0
15.9
J ug/L
50
10 -100
14
20
Hexachloroethane
32.0
14.3
ug/L
45
20 -100
9
20
Indeno[1,2,3-cd]pyrene
32.0
28.9
ug/L
90
65-133
2
20
Isophorone
32.0
25.0
ug/L
78
57 -110
2
20
2-Methyl naphtha lene
32.0
19.3
ug/L
60
34 -110
6
20
2-Methylphenol
32.0
22.5
ug/L
70
53 -110
7
20
3 & 4 Methylphenol
32.0
21.4
ug/L
67
53 -110
5
20
Naphthalene
32.0
18.8
ug/L
59
36 -110
3
20
2-Nitroaniline
32.0
24.3
ug/L
76
59 -122
3
20
3-Nitroaniline
32.0
29.6
ug/L
93
47.123
2
20
Ill
TestAmerica Chicago
Page 212 of 258 7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 500-428463/3-A
Client Sample
ID: Lab
Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428521
Prep Batch: 428463
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier Unit
D
%Rec
Limits RPD Limit
4-Nitroaniline
32.0
25.6
ug/L
80
52 -147 1 20
Nitrobenzene
32.0
23.4
ug/L
73
53 -110 6 20
2-Nitrophenol
32.0
21.1
ug/L
66
58 -110 6 20
4-Nitrophenol
64.0
31.1
ug/L
49
20 -110 13 20
N-Nitrosodimethylamine
32.0
18.1
ug/L
56
41 -110 5 20
N-Nitrosodi-n-propylamine
32.0
23.9
ug/L
75
58-110 5 20
N-Nitrosodiphenylamine
32.0
34.3
ug/L
107
66-110 4 20 F
2,2'-oxybis[l-chloropropane]
32.0
20.1
ug/L
63
38 -110 2 20
Phenanthrene
32.0
28.2
ug/L
88
65 -120 5 20
Phenol
32.0
14.1
ug/L
44
33 -100 7 20
Pyrene
32.0
28.7
ug/L
90
70 -110 2 20
1,2,4,5-Tetrachlorobenzene
32.0
19.0
ug/L
59
30-110 7 20 IM
2,3,4,6-Tetrachlorophenol
32.0
27.1
ug/L
85
44 -118 1 20
2,4,5-Trichlorophenol
32.0
22.3
ug/L
70
63-120 3 20
2,4,6-Trichlorophenol
32.0
22.2
ug/L
69
62 -110 4 20 F-
LCSD LCSD
Surrogate %Recovery Qualifier
Limits
2-Fluorobiphenyl 83
34 - 110
2-Fluorophenol 65
27 - 110
Nitrobenzene-d5 83
36 - 120
Phenol-d5 46
20 - 100
Terphenyl-d 14 108
40 - 145
2, 4, 6-Tribromophenol 93
40 - 145
Method: 8081 B - Organochlorine Pesticides
(GC)
Lab Sample ID: MB 500-428097/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428535
Prep Batch: 428097
MB MB
Analyte Result Qualifier
RL
LOD
MDL
Unit
D Analyzed Dil Fac
alpha-BHC <0.0026
0.040
0.020
0.0026
ug/L
04/19/18 12:43 1
beta-BHC <0.010
0.040
0.020
0.010
ug/L
04/19/18 12:43 1
delta-BHC <0.010
0.040
0.020
0.010
ug/L
04/19/18 12:43 1
gamma-BHC (Lindane) <0.0056
0.040
0.020
0.0056
ug/L
04/19/18 12:43 1
Heptachlor <0.014
0.040
0.020
0.014
ug/L
04/19/18 12:43 1
Aldrin <0.0053
0.040
0.020
0.0053
ug/L
04/19/18 12:43 1
Heptachlor epoxide <0.014
0.040
0.020
0.014
ug/L
04/19/18 12:43 1
Endosulfan 1 <0.0041
0.040
0.020
0.0041
ug/L
04/19/18 12:43 1
Dieldrin <0.013
0.040
0.020
0.013
ug/L
04/19/18 12:43 1
4,4'-DDE <0.0038
0.040
0.020
0.0038
ug/L
04/19/18 12:43 1
Endrin <0.014
0.040
0.020
0.014
ug/L
04/19/18 12:43 1
Endosulfan 11 <0.0028
0.040
0.020
0.0028
ug/L
04/19/18 12:43 1
4,4'-DDD <0.013
0.040
0.020
0.013
ug/L
04/19/18 12:43 1
Endosulfan sulfate <0.012
0.040
0.020
0.012
ug/L
04/19/18 12:43 1
4,4'-DDT <0.0032
0.040
0.020
0.0032
ug/L
04/19/18 12:43 1
Methoxychlor <0.023
0.080
0.040
0.023
ug/L
04/19/18 12:43 1
Toxaphene <0.20
0.40
0.20
0.20
ug/L
04/19/18 12:43 1
TestAmerica Chicago
Page 213 of 258 7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Method: 8081 B - Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: MB 500-428097/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428535
Prep Batch: 428097
MB MB
Analyte Result Qualifier
RL
LOD
MDL
Unit D
Analyzed Dil Fac
Endrin aldehyde <0.0082
0.040
0.020
0.0082
ug/L
04/19/18 12:43 1
Chlordane (technical) <0.040
0.080
0.040
0.040
ug/L
04/19/18 12:43 1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
DCB Decachlorobiphenyl 82
30 - 130
04117118 07:38
04/19/18 12:43 1
Tetrachloro-m-xylene 48
30 - 120
04117118 07:38
04119118 12:43 1
Lab Sample ID: LCS 500-428097/2-A
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428535
Prep Batch: 428097
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits
alpha-BHC
0.320
0.228
ug/L
71
65 -120
beta-BHC
0.320
0.253
ug/L
79
65 -120
delta-BHC
0.320
0.298
ug/L
93
70 -122
gamma-BHC (Lindane)
0.320
0.243
ug/L
76
68 -120
Heptachlor
0.320
0.189
ug/L
59
40 -120
Aldrin
0.320
0.179
ug/L
56
34 -120
Heptachlor epoxide
0.320
0.245
ug/L
77
64 -120
Endosulfan 1
0.320
0.159
ug/L
50
35 -110
Dieldrin
0.320
0.254
ug/L
79
68 -120
4,4'-DDE
0.320
0.254
ug/L
79
58 -122
Endrin
0.320
0.242
ug/L
76
60 -132
Endosulfan 11
0.320
0.199
ug/L
62
53 -110
4,4'-DDD
0.320
0.272
ug/L
85
69 -124
Endosulfan sulfate
0.320
0.259
ug/L
81
70 -133
4,4'-DDT
0.320
0.280
ug/L
88
62 -127
Methoxychlor
0.320
0.281
ug/L
88
63 -135
Endrin aldehyde
0.320
0.270
ug/L
84
66 -120
LCS LCS
Surrogate %Recovery Qualifier
Limits
DCB Decachlorobiphenyl 82
30 - 130
Tetrachloro-m-xylene 56
30 - 120
Lab Sample ID: LCSD 500-42809713-A
Client Sample
ID: Lab
Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428535
Prep Batch: 428097
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits RPD Limit
alpha-BHC
0.320
0.241
ug/L
75
65 -120 5 20
beta-BHC
0.320
0.255
ug/L
80
65 -120 1 20
delta-BHC
0.320
0.301
ug/L
94
70 -122 1 20
gamma-BHC (Lindane)
0.320
0.252
ug/L
79
68 -120 4 20
Heptachlor
0.320
0.210
ug/L
65
40 -120 10 20
Aldrin
0.320
0.198
ug/L
62
34 -120 10 20
Heptachlor epoxide
0.320
0.251
ug/L
78
64 -120 2 20
Endosulfan 1
0.320
0.168
ug/L
52
35 -110 5 20
Dieldrin
0.320
0.260
ug/L
81
68 -120 2 20
TestAmerica Chicago
Page 214 of 258 7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg
Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Method: 8081 B - Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: LCSD 500-428097/3-A
Client Sample
ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428535
Prep Batch: 428097
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier Unit
D
%Rec Limits RPD Limit
4,4'-DDE
0.320
0.254
ug/L
80 58 -122 0 20
Endrin
0.320
0.247
ug/L
77 60 -132 2 20
Endosulfan II
0.320
0.202
ug/L
63 53 -110 2 20
4,4'-DDD
0.320
0.274
ug/L
86 69 -124 1 20
Endosulfan sulfate
0.320
0.259
ug/L
81 70 -133 0 20
4,4'-DDT
0.320
0.284
ug/L
89 62 -127 1 20
Methoxychlor
0.320
0.291
ug/L
91 63 -135 4 20
Endrin aldehyde
0.320
0.273
ug/L
85 66 -120 1 20
LCSD LCSD
Surrogate
%Recovery Qualifier
Limits
DCB Decachlorobiphenyl
73
30- 130
m
Tetrachloro-m-xylene
51
30 - 120
Lab Sample ID: MB 500-428495/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428753
Prep Batch: 428495
MB MB
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed Dil Fac
alpha-BHC
<0.0026
0.040
0.020
0.0026
ug/L
04/20/18 13:08 1
beta-BHC
<0.010
0.040
0.020
0.010
ug/L
04/20/18 13:08 1
delta-BHC
<0.010
0.040
0.020
0.010
ug/L
04/20/18 13:08 1
gamma-BHC (Lindane)
<0.0056
0.040
0.020
0.0056
ug/L
04/20/18 13:08 1
Heptachlor
<0.014
0.040
0.020
0.014
ug/L
04/20/18 13:08 1
Aldrin
<0.0053
0.040
0.020
0.0053
ug/L
04/20/18 13:08 1
Heptachlor epoxide
<0.014
0.040
0.020
0.014
ug/L
04/20/18 13:08 1
Endosulfan 1
<0.0041
0.040
0.020
0.0041
ug/L
04/20/18 13:08 1
Dieldrin
<0.013
0.040
0.020
0.013
ug/L
04/20/18 13:08 1
4,4'-DDE
<0.0038
0.040
0.020
0.0038
ug/L
04/20/18 13:08 1
Endrin
<0.014
0.040
0.020
0.014
ug/L
04/20/18 13:08 1
Endosulfan II
<0.0028
0.040
0.020
0.0028
ug/L
04/20/18 13:08 1
4,4'-DDD
<0.013
0.040
0.020
0.013
ug/L
04/20/18 13:08 1
Endosulfan sulfate
<0.012
0.040
0.020
0.012
ug/L
04/20/18 13:08 1
4,4'-DDT
<0.0032
0.040
0.020
0.0032
ug/L
04/20/18 13:08 1
Methoxychlor
<0.023
0.080
0.040
0.023
ug/L
04/20/18 13:08 1
Toxaphene
<0.20
0.40
0.20
0.20
ug/L
04/20/18 13:08 1
Endrin aldehyde
<0.0082
0.040
0.020
0.0082
ug/L
04/20/18 13:08 1
Chlordane (technical)
<0.040
0.080
0.040
0.040
ug/L
04/20/18 13:08 1
MB MB
Surrogate %Recovery Qualifier
DCB Decachlorobiphenyl 85
Tetrachloro-m-xylene 55
Lab Sample ID: LCS 500-428495/2-A
Matrix: Water
Analysis Batch: 428753
Analyte
alpha-BHC
Limits
30-130
30-120
Prepared Analyzed Dil Fac
04119118 07:40 04120118 13:08 1
04119118 07:40 04120118 13:08 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 428495
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
0.320 0.263 ug/L 82 65 -120
Page 215 of 258
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7/5/2018

QC Sample Results C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8081 B - Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: LCS 500-428495/2-A
Matrix: Water
Analysis Batch: 428753
Analyte
beta-BHC
delta-BHC
gamma-BHC (Lindane)
Heptachlor
Aldrin
Heptachlor epoxide
Endosulfan I
Dieldrin
4,4'-DDE
Endrin
Endosulfan II
4,4'-DDD
Endosulfan sulfate
4,4'-DDT
Methoxychlor
Endrin aldehyde
Surrogate
DCB Decachlorobiphenyl
Tetrachloro-m-xylene
LCS LCS
%Recovery Qualifier
83
58
Lab Sample ID: LCSD 500-428495/3-A
Matrix: Water
Analysis Batch: 428753
Spike
Added
0.320
0.320
0.320
0.320
0.320
0.320
0.320
0.320
0.320
0.320
0.320
0.320
0.320
0.320
0.320
0.320
Limits
30-130
30-120
LCS LCS
Result Qualifier
0.275
0.370
0.267
0.226
0.200
0.277
0.224
0.285
0.249
0.273
0.215
0.298
0.285
0.307
0.318
0.278
Spike
LCSD LCSD
Analyte
Added
Result Qualifier
alpha-BHC
0.320
0.294
beta-BHC
0.320
0.314
delta-BHC
0.320
0.422
gamma-BHC (Lindane)
0.320
0.321
Heptachlor
0.320
0.258
Aldrin
0.320
0.251
Heptachlor epoxide
0.320
0.315
Endosulfan 1
0.320
0.249
Dieldrin
0.320
0.326
4,4'-DDE
0.320
0.289
Endrin
0.320
0.309
Endosulfan 11
0.320
0.246
4,4'-DDD
0.320
0.341
Endosulfan sulfate
0.320
0.320
4,4'-DDT
0.320
0.354
Methoxychlor
0.320
0.350
Endrin aldehyde
0.320
0.315
LCSD LCSD
Surrogate
%Recovery Qualifier
Limits
DCB Decachlorobiphenyl
89
30- 130
Tetrachloro-m-xylene
63
30 - 120
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 428495
Unit
D %Rec
%Rec.
Limits
ug/L
86
65-120
ug/L
116
70-122
ug/L
83
68-120
ug/L
71
40-120
ug/L
63
34-120
ug/L
87
64 -120
ug/L
70
35-110
ug/L
89
68-120
ug/L
78
58-122
ug/L
85
60-132
ug/L
67
53-110
ug/L
93
69-124
ug/L
89
70-133
ug/L
96
62 -127
ug/L
99
63-135
ug/L
87
66-120
Client
Unit
Sample ID: Lab
D %Rec
Control Sample Dup
Prep Type: Total/NA
Prep Batch: 428495
%Rec. RPD
Limits RPD Limit
ug/L
92
65-120
11
20
ug/L
98
65-120
13
20
ug/L
132
70-122
13
20
ug/L
100
68-120
18
20
ug/L
81
40-120
13
20
ug/L
78
34 -120
23
20
ug/L
98
64 -120
13
20
ug/L
78
35-110
10
20
ug/L
102
68-120
13
20
ug/L
90
58-122
15
20
ug/L
97
60-132
12
20
ug/L
77
53-110
14
20
ug/L
107
69-124
13
20
ug/L
100
70-133
11
20
ug/L
110
62 -127
14
20
ug/L
109
63-135
10
20
ug/L
98
66-120
12
20
Page 216 of 258
TestAmerica Chicago
7/5/2018

QC Sample Results C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Lab Sample ID: MB 500-428097/1-A
Matrix: Water
Analysis Batch: 428222
Analyte
MB MB
Result Qualifier
PCB-1016
<0.067
PCB-1221
<0.20
PCB-1232
<0.20
PCB-1242
<0.20
PCB-1248
<0.20
PCB-1254
<0.20
PCB-1260
<0.070
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 428097
RL
LOD
MDL
Unit
D Analyzed Dil Fac
0.40
0.20
0.067
ug/L
04/17/1817:07 1
0.40
0.20
0.20
ug/L
04/17/1817:07 1
0.40
0.20
0.20
ug/L
04/17/1817:07 1
0.40
0.20
0.20
ug/L
04/17/1817:07 1
0.40
0.20
0.20
ug/L
04/17/1817:07 1
0.40
0.20
0.20
ug/L
04/17/1817:07 1
0.40
0.20
0.070
ug/L
04/17/1817:07 1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
Tetrachloro-m-xylene
55
30 - 120
04117118 07:38 04117118 17:07 1
DCB Decachlorobiphenyl
90
30 - 140
04117118 07:38 04117118 17:07 1 m
Lab Sample ID: LCS 500-428097/4-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428222
Prep Batch: 428097
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec Limits
PCB-1016
4.00
3.72
ug/L
93 56 -120
PCB-1260
4.00
4.17
ug/L
104 53 -137
LCS
LCS
Surrogate %Recovery
Qualifier
Limits
Tetrachloro-m-xylene 79
30 - 120
DCB Decachlorobiphenyl 103
30- 140
Lab Sample ID: LCSD 500-42809715-A
Client Sample
ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428222
Prep Batch: 428097
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier
Unit
D %Rec Limits RPD Limit
PCB-1016
4.00
3.72
ug/L
93 56 -120 0 20
PCB-1260
4.00
3.97
ug/L
99 53 -137 5 20
LCSD
LCSD
Surrogate %Recovery
Qualifier
Limits
Tetrachloro-m-xylene 84
30 - 120
DCB Decachlorobiphenyl 100
30 - 140
Lab Sample ID: MB 500-428495/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428582
Prep Batch: 428495
MB MB
Analyte
Result Qualifier
RL LOD
MDL
Unit D Analyzed Dil Fac
PCB-1016
<0.067
0.40 0.20
0.067
ug/L 04/19/1815:57 1
PCB-1221
<0.20
0.40 0.20
0.20
ug/L 04/19/1815:57 1
PCB-1232
<0.20
0.40 0.20
0.20
ug/L 04/19/1815:57 1
PCB-1242
<0.20
0.40 0.20
0.20
ug/L 04/19/1815:57 1
PCB-1248
<0.20
0.40 0.20
0.20
ug/L 04/19/1815:57 1
PCB-1254
<0.20
0.40 0.20
0.20
ug/L 04/19/1815:57 1
Page 217 of 258
TestAmerica Chicago
7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)
Lab Sample ID: MB 500-428495/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428582
Prep Batch: 428495
MB MB
Analyte Result Qualifier
RL LOD MDL Unit D Analyzed Dil Fac
PCB-1260 <0.070
0.40 0.20 0.070 ug/L 04/19/1815:57 1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
Tetrachloro-m-xylene 60
30 - 120
04119118 07:46 04/19/18 15 1
DCB Decachlorobiphenyl 96
30 - 140
04119118 07:40 04119118 15:57 1
Lab Sample ID: LCS 500-428495/4-A
Client Sample ID: Lab Control Sample
C
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428582
Prep Batch: 428495
Spike
LCS LCS %Rec.
Analyte
Added
Result Qualifier Unit D %Rec Limits
PCB-1016
4.00
3.45 ug/L 86 56 -120
PCB-1260
4.00
3.37 ug/L 84 53 -137
LCS LCS
Surrogate %Recovery Qualifier
Limits
Tetrachloro-m-xylene 56
30 - 120
DCB Decachlorobiphenyl 66
30 - 140
Lab Sample ID: LCSD 500-42849515-A
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428582
Prep Batch: 428495
Spike
LCSD LCSD %Rec. RPD
Analyte
Added
Result Qualifier Unit D %Rec Limits RPD Limit
PCB-1016
4.00
3.70 ug/L 92 56 -120 7 20
PCB-1260
4.00
3.84 ug/L 96 53 -137 13 20
LCSD LCSD
Surrogate %Recovery Qualifier
Limits
Tetrachloro-m-xylene 59
30 - 120
DCB Decachlorobiphenyl 90
30- 140
Method: 8151A - Herbicides (GC)
Lab Sample ID: MB 500-428120/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 427712
Prep Batch: 428120
MB MB
Analyte Result Qualifier
RL LOD MDL Unit D Analyzed Dil Fac
2,4-D <0.47
1.0 0.50 0.47 ug/L 04/17/18 21:43 1
Dinoseb <0.16
2.0 1.0 0.16 ug/L 04/17/18 21:43 1
Pentachlorophenol <0.090
0.50 0.10 0.090 ug/L 04/17/18 21:43 1
Silvex (2,4,5-TP) <0.29
1.0 0.50 0.29 ug/L 04/17/18 21:43 1
2,4,5-T <0.43
1.0 0.50 0.43 ug/L 04/17/18 21:43 1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
DCAA 74
25 - 130
04117118 09:02 04117118 21:43 1
TestAmerica Chicago
Page 218 of 258 7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Method: 8151A - Herbicides (GC) (Continued)
Lab Sample ID: LCS 500-428120/2-A
Matrix: Water
Analysis Batch: 427712
Spike
Analyte
Added
2,4-D
10.1
Dinoseb
10.1
Pentachlorophenol
2.53
Silvex (2,4,5-TP)
2.51
2,4,5-T
2.53
LCS LCS
Surrogate %Recovery Qualifier
DCAA 81
Lab Sample ID: LCSD 500-42812013-A
Matrix: Water
Analysis Batch: 427712
Analyte
2,4-D
Dinoseb
Pentachlorophenol
Silvex (2,4,5-TP)
2,4,5-T
LCSD LCSD
Surrogate %Recovery Qualifier
DCAA 81
Lab Sample ID: MB 500-428351/1-A
Matrix: Water
Analysis Batch: 428477
Limits
25 - 130
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 428120
LCS LCS
%Rec.
Result Qualifier
Unit
D %Rec
Limits
8.19
ug/L
81
30 -115
6.15
ug/L
61
30 -110
1.61
ug/L
64
40 -122
2.04
ug/L
81
32 -115
2.00
ug/L
79
30 -115
Spike
Added
LCSD LCSD
Result Qualifier
10.1
8.41
10.1
5.91
2.53
1.59
2.51
2.03
2.53
2.02
Limits
25 - 130
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 428120
%Rec. RPD
Unit
D %Rec
Limits RPD Limit
ug/L
84
30-115 3 20
ug/L
59
30-110 4 20
ug/L
63
40-122 2 20
ug/L
81
32-115 1 20
ug/L
80
30-115 1 20
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 428351
MB MB
Analyte
Result Qualifier
RL
LOD
MDL
Unit D
Analyzed Dil Fac
2,4-D
<0.47
1.0
0.50
0.47
ug/L
04/18/18 23:38 1
Dinoseb
<0.16
2.0
1.0
0.16
ug/L
04/18/18 23:38 1
Pentachlorophenol
<0.090
0.50
0.10
0.090
ug/L
04/18/18 23:38 1
Silvex (2,4,5-TP)
<0.29
1.0
0.50
0.29
ug/L
04/18/18 23:38 1
2,4,5-T
<0.43
1.0
0.50
0.43
ug/L
04/18/18 23:38 1
MB MB
Surrogate %Recovery
Qualifier
Limits
Prepared
Analyzed Dil Fac
DCAA
57
25 - 130
04118118 10:05
04118118 23:38 1
Lab Sample ID: LCS 500-428351/2-A
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428477
Prep Batch: 428351
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits
2,4-D
10.1
6.29
ug/L
63
30 -115
Dinoseb
10.1
4.74
ug/L
47
30 -110
Pentachlorophenol
2.53
1.44
ug/L
57
40 -122
Silvex (2,4,5-TP)
2.51
1.72
ug/L
68
32 -115
2,4,5-T
2.53
1.50
ug/L
59
30 -115
Li
Page 219 of 258
TestAmerica Chicago
7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Method: 8151A - Herbicides (GC) (Continued)
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Lab Sample ID: LCS 500-428351/2-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428477
Prep Batch: 428351
LCS
LCS
Surrogate %Recovery
Qualifier
Limits
DCAA 59
25-130
Lab Sample ID: LCSD 500-428351/3-A
Client Sample
ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428477
Prep Batch: 428351
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier
Unit
D %Rec Limits RPD Limit
2,4-D
-
10.1
6.19
ug/L
-
62 30 -115 2 20
Dinoseb
10.1
4.67
ug/L
46 30 -110 2 20
Pentachlorophenol
2.53
1.47
ug/L
58 40 -122 2 20
Silvex (2,4,5-TP)
2.51
1.68
ug/L
67 32 -115 2 20
2,4,5-T
2.53
1.47
ug/L
58 30 -115 2 20
LCSD
LCSD
Surrogate %Recovery
Qualifier
Limits
LDCAA 63
25 - 130
Method: 6020B - Metals (ICP/MS)
Lab Sample ID: MB 500-428299/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total Recoverable
Analysis Batch: 428958
Prep Batch: 428299
MB MB
Analyte
Result Qualifier
RL
LOD
MDL
Unit D Analyzed Dil Fac
Arsenic
<0.23
1.0
0.50
0.23
ug/L 04/21/18 02:35 1
Barium
<0.73
2.5
1.3
0.73
ug/L 04/21/18 02:35 1
Beryllium
<0.53
1.0
0.53
0.53
ug/L 04/21/18 02:35 1
Cadmium
<0.17
0.50
0.25
0.17
ug/L 04/21/18 02:35 1
Chromium
1.65 J
5.0
2.5
1.1
ug/L 04/21/18 02:35 1
Cobalt
<0.40
1.0
0.50
0.40
ug/L 04/21/18 02:35 1
Copper
0.641 J
2.0
1.0
0.50
ug/L 04/21/18 02:35 1
Iron
<47
100
50
47
ug/L 04/21/18 02:35 1
Manganese
<0.79
2.5
1.3
0.79
ug/L 04/21/18 02:35 1
Lead
<0.19
0.50
0.25
0.19
ug/L 04/21/18 02:35 1
Nickel
<0.63
2.0
1.0
0.63
ug/L 04/21/18 02:35 1
Antimony
<1.3
3.0
1.5
1.3
ug/L 04/21/18 02:35 1
Selenium
<0.98
2.5
1.3
0.98
ug/L 04/21/18 02:35 1
Silver
<0.12
0.50
0.25
0.12
ug/L 04/21/18 02:35 1
Thallium
<0.57
2.0
1.0
0.57
ug/L 04/21/18 02:35 1
Tin
<1.3
5.0
2.5
1.3
ug/L 04/21/18 02:35 1
Vanadium
<2.2
5.0
2.5
2.2
ug/L 04/21/18 02:35 1
Zinc
9.39 J
10
20
6.9
ug/L 04/21/18 02:35 1
Lab Sample ID: LCS 500-428299/2-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total Recoverable
Analysis Batch: 428958
Prep Batch: 428299
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec Limits
Arsenic
100
101
ug/L
101 80 -120
TestAmerica Chicago
Page 220 of 258 7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG:
NCDEQ Solid Waste Facility = # 60-13
Method: 6020B - Metals
(ICP/MS) (Continued)
Lab Sample ID: LCS 500-428299/2-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total Recoverable
Analysis Batch: 428958
Prep Batch: 428299
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec Limits
Barium
500
516
ug/L
103 80-120
Beryllium
50.0
47.7
ug/L
95 80 -120
Cadmium
50.0
51.1
ug/L
102 80 -120
Chromium
200
209
ug/L
104 80 -120
Cobalt
500
511
ug/L
102 80 -120
Copper
250
263
ug/L
105 80-120
Iron
1000
1050
ug/L
105 80 -120
Manganese
500
514
ug/L
103 80-120
Lead
100
107
ug/L
107 80-120
Nickel
500
520
ug/L
104 80 -120
Antimony
500
508
ug/L
102 80 -120
Selenium
100
102
ug/L
102 80 -120
Silver
50.0
52.8
ug/L
106 80 -120
Thallium
100
105
ug/L
105 80-120
Tin
1000
985
ug/L
99 80 -120
Vanadium
500
506
ug/L
101 80 -120
Zinc
500
527
ug/L
105 80 -120
Lab Sample ID: 500-143858-13
MS
Client Sample ID: MW-8(i)
Matrix: Water
Prep Type: Total Recoverable
Analysis Batch: 428958
Prep Batch: 428299
Sample Sample
Spike
MS
MS
%Rec.
Analyte
Result Qualifier
Added
Result
Qualifier
Unit
D %Rec Limits
Arsenic
0.46 J
100
101
ug/L
100 75 -125
Barium
44
500
557
ug/L
103 75-125
Beryllium
<0.53
50.0
46.0
ug/L
92 75 -125
Cadmium
<0.17
50.0
51.0
ug/L
102 75 -125
Chromium
<1.1
200
191
ug/L
95 75 -125
Cobalt
2.5
500
468
ug/L
93 75 -125
Copper
1.1 J B
250
255
ug/L
102 75 -125
Iron
1500
1000
2460
ug/L
98 75 -125
Manganese
390
500
850
ug/L
93 75-125
Lead
<0.19
100
107
ug/L
107 75 -125
Nickel
1.6 J
500
469
ug/L
94 75 -125
Antimony
<1.3
500
517
ug/L
103 75 -125
Selenium
<0.98
100
102
ug/L
102 75 -125
Silver
<0.12
50.0
51.8
ug/L
104 75 -125
Thallium
<0.57
100
105
ug/L
105 75-125
Tin
<1.3
1000
996
ug/L
100 75 -125
Vanadium
6.2
500
473
ug/L
93 75 -125
Zinc
<6.9
500
508
ug/L
102 75 -125
Lab Sample ID: 500-143858-13
MSD
Client Sample ID: MW-8(i)
Matrix: Water
Prep Type: Total Recoverable
Analysis Batch: 428958
Prep Batch: 428299
Sample Sample
Spike
MSD
MSD
%Rec. RPD
Analyte
Result Qualifier
Added
Result
Qualifier
Unit
D %Rec Limits RPD Limit
Arsenic
0.46 J
100
98.0
ug/L
98 75 -125 3 20
Barium
44
500
547
ug/L
101 75-125 2 20
TestAmerica Chicago
Page 221 of 258 7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill
- Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Method: 6020B - Metals
(ICP/MS) (Continued)
Lab Sample ID: 500-143858-13
MSD
Client Sample ID: MW-8(i)
Matrix: Water
Prep Type: Total Recoverable
Analysis Batch: 428958
Prep Batch: 428299
Sample
Sample
Spike
MSD
MSD
%Rec. RPD
Analyte
Result
Qualifier
Added
Result
Qualifier
Unit
D %Rec Limits RPD Limit
Beryllium
<0.53
50.0
45.0
ug/L
90 75 -125 2 20
Cadmium
<0.17
50.0
50.0
ug/L
100 75 -125 2 20
Chromium
<1.1
200
190
ug/L
95 75 -125 1 20
Cobalt
2.5
500
456
ug/L
91 75 -125 3 20
Copper
1.1
J B
250
249
ug/L
99 75 -125 2 20
Iron
1500
1000
2490
ug/L
102 75-125 1 20
Manganese
390
500
839
ug/L
91 75-125 1 20
Lead
<0.19
100
105
ug/L
105 75-125 2 20
Nickel
1.6
J
500
457
ug/L
91 75 -125 3 20
Antimony
<1.3
500
505
ug/L
101 75-125 2 20
Selenium
<0.98
100
99.2
ug/L
99 75 -125 2 20
Silver
<0.12
50.0
50.4
ug/L
101 75 -125 3 20
Thallium
<0.57
100
103
ug/L
103 75-125 2 20
Tin
<1.3
1000
989
ug/L
99 75 -125 1 20
Vanadium
6.2
500
457
ug/L
90 75 -125 3 20
Zinc
<6.9
500
498
ug/L
100 75 -125 2 20
Lab Sample ID: 500-143858-13
DU
Client Sample ID: MW-8(i)
Matrix: Water
Prep Type: Total Recoverable
Analysis Batch: 428958
Prep Batch: 428299
Sample
Sample
DU
DU
RPD
Analyte
Result
Qualifier
Result
Qualifier
Unit
D RPD Limit
Arsenic
0.46
J
0.432
J
ug/L
6 20
Barium
44
45.1
ug/L
3 20
Beryllium
<0.53
<0.53
ug/L
NC 20
Cadmium
<0.17
<0.17
ug/L
NC 20
Chromium
<1.1
<1.1
ug/L
NC 20
Cobalt
2.5
2.35
ug/L
8 20
Copper
1.1
J B
1.22
J
ug/L
11 20
Iron
1500
1540
ug/L
4 20
Manganese
390
398
ug/L
3 20
Lead
<0.19
<0.19
ug/L
NC 20
Nickel
1.6
J
1.50
J
ug/L
9 20
Antimony
<1.3
<1.3
ug/L
NC 20
Selenium
<0.98
<0.98
ug/L
NC 20
Silver
<0.12
<0.12
ug/L
NC 20
Thallium
<0.57
<0.57
ug/L
NC 20
Tin
<1.3
<1.3
ug/L
NC 20
Vanadium
6.2
6.38
ug/L
3 20
Zinc
<6.9
<6.9
ug/L
NC 20
Lab Sample ID: MB 500-428456/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total Recoverable
Analysis Batch: 428958
Prep Batch: 428456
MB MB
Analyte
Result Qualifier
RL
LOD
MDL
Unit D Analyzed Dil Fac
Arsenic
<0.23
1.0
0.50
0.23
ug/L 04/21/18 04:28 1
Barium
<0.73
2.5
1.3
0.73
ug/L 04/21/18 04:28 1
Beryllium
<0.53
1.0
0.53
0.53
ug/L 04/21/18 04:28 1
Li
TestAmerica Chicago
Page 222 of 258 7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill
- Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Method: 6020B - Metals (ICP/MS) (Continued)
Lab Sample ID: MB 500-428456/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep
Type: Total Recoverable
Analysis Batch: 428958
Prep Batch: 428456
MB MB
Analyte
Result Qualifier
RL
LOD
MDL
Unit
D Analyzed Dil Fac
Cadmium
<0.17
0.50
0.25
0.17
ug/L
04/21/18 04:28 1
Chromium
<1.1
5.0
2.5
1.1
ug/L
04/21/18 04:28 1
Cobalt
<0.40
1.0
0.50
0.40
ug/L
04/21/18 04:28 1
Copper
<0.50
2.0
1.0
0.50
ug/L
04/21/18 04:28 1
Iron
<47
100
50
47
ug/L
04/21/18 04:28 1
Manganese
<0.79
2.5
1.3
0.79
ug/L
04/21/18 04:28 1
Lead
<0.19
0.50
0.25
0.19
ug/L
04/21/18 04:28 1
Nickel
<0.63
2.0
1.0
0.63
ug/L
04/21/18 04:28 1
Antimony
<1.3
3.0
1.5
1.3
ug/L
04/21/18 04:28 1
Selenium
<0.98
2.5
1.3
0.98
ug/L
04/21/18 04:28 1
Silver
<0.12
0.50
0.25
0.12
ug/L
04/21/18 04:28 1 m
Thallium
<0.57
2.0
1.0
0.57
ug/L
04/21/18 04:28 1
Tin
<1.3
5.0
2.5
1.3
ug/L
04/21/18 04:28 1
Vanadium
<2.2
5.0
2.5
2.2
ug/L
04/21/18 04:28 1
<6.9
10
20
6.9
ug/L
04/21/18 04:28 1
-Zinc
Lab Sample ID: LCS 500-428456/2-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep
Type: Total Recoverable
Analysis Batch: 428958
Prep Batch: 428456
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D
%Rec Limits
Arsenic
100
99.5
ug/L
100 80 -120
Barium
500
519
ug/L
104 80-120
Beryllium
50.0
48.2
ug/L
96 80 -120
Cadmium
50.0
52.1
ug/L
104 80 -120
Chromium
200
211
ug/L
106 80 -120
Cobalt
500
522
ug/L
104 80 -120
Copper
250
259
ug/L
104 80-120
Iron
1000
1070
ug/L
107 80 -120
Manganese
500
523
ug/L
105 80-120
Lead
100
109
ug/L
109 80-120
Nickel
500
529
ug/L
106 80 -120
Antimony
500
518
ug/L
104 80 -120
Selenium
100
102
ug/L
102 80 -120
Silver
50.0
52.6
ug/L
105 80 -120
Thallium
100
106
ug/L
106 80-120
Tin
1000
1000
ug/L
100 80 -120
Vanadium
500
514
ug/L
103 80 -120
Zinc
500
517
ug/L
103 80 -120
Lab Sample ID: 500-143858-1 MS
Client Sample ID: MW-12(i)
Matrix: Water
Prep Type: Dissolved
Analysis Batch: 428958
Prep Batch: 428456
Sample
Sample
Spike
MS
MS
%Rec.
Analyte Result
Qualifier
Added
Result
Qualifier
Unit
D
%Rec Limits
Arsenic 0.48
J
100
103
ug/L
102 75 -125
Barium 220
500
739
ug/L
104 75-125
Beryllium <0.53
50.0
47.0
ug/L
94 75 -125
Cadmium <0.17
50.0
51.6
ug/L
103 75 -125
TestAmerica Chicago
Page 223 of 258 7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 6020B - Metals (ICP/MS) (Continued)
Lab Sample ID: 500-143858-1 MS
Matrix: Water
Analysis Batch: 428958
Sample Sample Spike
Analyte Result Qualifier Added
MS MS
Result Qualifier
Unit
Chromium
<1.1
200
198
ug/L
Cobalt
6.1
500
478
ug/L
Copper
5.0
250
254
ug/L
Iron
200
1000
1190
ug/L
Manganese
300
500
788
ug/L
Lead
0.35
J
100
107
ug/L
Nickel
9.4
500
488
ug/L
Antimony
<1.3
500
531
ug/L
Selenium
<0.98
100
104
ug/L
Silver
<0.12
50.0
52.3
ug/L
Thallium
<0.57
100
103
ug/L
Tin
<1.3
1000
1020
ug/L
Vanadium
<2.2
500
487
ug/L
Zinc
7.2
J
500
506
ug/L
Lab Sample ID: 500-143858-1 MSD
Matrix: Water
Analysis Batch: 428958
Analyte
Sample
Result
Sample
Qualifier
Spike
Added
MSD MSD
Result Qualifier
Arsenic
0.48
J
100
102
Barium
220
500
741
Beryllium
<0.53
50.0
46.8
Cadmium
<0.17
50.0
51.4
Chromium
<1.1
200
199
Cobalt
6.1
500
487
Copper
5.0
250
252
Iron
200
1000
1200
Manganese
300
500
795
Lead
0.35
J
100
109
Nickel
9.4
500
491
Antimony
<1.3
500
530
Selenium
<0.98
100
104
Silver
<0.12
50.0
51.8
Thallium
<0.57
100
103
Tin
<1.3
1000
1020
Vanadium
<2.2
500
490
Zinc
7.2
J
500
506
Lab Sample ID: 500-143858-1 DU
Matrix: Water
Analysis Batch: 428958
Client Sample ID: MW-12(i)
Prep Type: Dissolved
Prep Batch: 428456
%Rec.
D %Rec Limits
99 75-125
94 75-125
100 75-125
99 75-125
97 75-125
107 75-125
96 75-125
106 75-125
104 75-125
105 75-125
103 75-125 m
102 75-125
97 75-125
100 75-125
Client Sample
ID: MW-12(i)
C
Prep Type: Dissolved
Prep Batch:
428456
%Rec.
RPD
Unit
D %Rec
Limits
RPD
Limit
ug/L
101
75-125
1
20
ug/L
104
75-125
0
20
ug/L
94
75-125
1
20
ug/L
103
75-125
0
20
ug/L
100
75-125
1
20
ug/L
96
75-125
2
20
ug/L
99
75-125
1
20
ug/L
100
75-125
1
20
ug/L
99
75-125
1
20
ug/L
109
75-125
2
20
ug/L
96
75-125
1
20
ug/L
106
75-125
0
20
ug/L
104
75-125
0
20
ug/L
104
75-125
1
20
ug/L
103
75-125
0
20
ug/L
102
75-125
1
20
ug/L
98
75-125
1
20
ug/L
100
75-125
0
20
Analyte
Sample Sample
Result Qualifier
DU DU
Result Qualifier
Unit
Arsenic
0.48 J
0.438 J
ug/L
Barium
220
223
ug/L
Beryllium
<0.53
<0.53
ug/L
Cadmium
<0.17
<0.17
ug/L
Chromium
<1.1
<1.1
ug/L
Client Sample ID: MW-12(i)
Prep Type: Dissolved
Prep Batch: 428456
RPD
D RPD Limit
8 20
1 20
NC 20
NC 20
NC 20
TestAmerica Chicago
Page 224 of 258 7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ
Solid Waste Facility = # 60-13
Method: 6020B - Metals (ICP/MS) (Continued)
Lab Sample ID: 500-143858-1 DU
Client Sample ID: MW-12(i)
Matrix: Water
Prep Type: Dissolved
Analysis Batch: 428958
Prep Batch: 428456
Sample Sample
DU
DU
RPD
Analyte Result Qualifier
Result
Qualifier
Unit
D RPD Limit
Cobalt 6.1
6.15
ug/L
0.6 20
Copper 5.0
2.14
F3
ug/L
81 20
Iron 200
211
ug/L
7 20
Manganese 300
306
ug/L
1 20
Lead 0.35 J
0.357
J
ug/L
3 20
Nickel 9.4
9.09
ug/L
3 20
Antimony <1.3
<1.3
ug/L
NC 20
Selenium <0.98
<0.98
ug/L
NC 20
Silver <0.12
<0.12
ug/L
NC 20
Thallium <0.57
<0.57
ug/L
NC 20
Tin <1.3
<1.3
ug/L
NC 20
Vanadium <2.2
<2.2
ug/L
NC 20
Zinc 7.2 J
<6.9
ug/L
NC 20
Method: 7470A - Mercury (CVAA)
Lab Sample ID: MB 500-428144/12-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428374
Prep Batch: 428144
MB MB
Analyte Result Qualifier
RL
LOD
MDL
Unit D Analyzed Dil Fac
Mercury <0.098
0.20
0.10
0.098
ug/L 04/18/1810:40 1
Lab Sample ID: LCS 500-428144/13-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428374
Prep Batch: 428144
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec Limits
Mercury
2.00
2.15
ug/L
108 80 -120
Lab Sample ID: 500-143858-1 MS
Client Sample ID: MW-12(i)
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428374
Prep Batch: 428144
Sample Sample
Spike
MS
MS
%Rec.
Analyte Result Qualifier
Added
Result
Qualifier
Unit
D %Rec Limits
Mercury <0.098
1.00
0.856
ug/L
86 75 -125
Lab Sample ID: 500-143858-1 MSD
Client Sample ID: MW-12(i)
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428374
Prep Batch: 428144
Sample Sample
Spike
MSD
MSD
%Rec. RPD
Analyte Result Qualifier
Added
Result
Qualifier
Unit
D %Rec Limits RPD Limit
Mercury <0.098
1.00
0.836
ug/L
84 75 -125 2 20
TestAmerica Chicago
Page 225 of 258 7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill
- Infill
SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 7470A - Mercury (CVAA) (Continued)
Lab Sample ID: 500-143858-1 DU
Client Sample ID: MW-12(i)
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428374
Prep Batch: 428144
Sample
Sample
DU DU RPD
Analyte Result
Qualifier
Result Qualifier Unit D RPD Limit
Mercury <0.098
<0.098 ug/L NC 20
Lab Sample ID: MB 500-428588/12-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428749
Prep Batch: 428588
MB MB
Result Qualifier
RL LOD MDL Unit D Analyzed Dil Fac
[Analyte
Mercury
<0.098
0.20 0.10 0.098 ug/L 04/20/18 09:52 1
Lab Sample ID: LCS 500-428588/13-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 428749
Prep Batch: 428588
Spike
LCS LCS %Rec.
Analyte
Added
Result Qualifier Unit D %Rec Limits
Mercury
2.00
2.02 ug/L 101 80 -120
Method: 9014 - Cyanide
Lab Sample ID: MB 500-429136/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 429232
Prep Batch: 429136
MB MB
Analyte
Result Qualifier
RL LOD MDL Unit D Analyzed Dil Fac
Cyanide, Total
<3.5
10 5.0 3.5 ug/L 04/24/18 15:54 1
Lab Sample ID: LCS 500-429136/2-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 429232
Prep Batch: 429136
Spike
LCS LCS %Rec.
Analyte
Added
Result Qualifier Unit D %Rec Limits
Cyanide, Total
100
111 ug/L 111 80 - 120
Lab Sample ID: 500-143858-1 MS
Client Sample ID: MW-12(i)
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 429232
Prep Batch: 429136
Sample
Sample Spike
MS Ms %Rec.
Analyte Result
cyanide, Total <3.5
Qualifier Added
40.0
Result Qualifier Unit D %Rec Limits
36.5 ug/L 91 75
-125
Lab Sample ID: 500-143858-1 MSD
Client Sample ID: MW-12(i)
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 429232
Prep Batch: 429136
Sample
Sample Spike
MSD MSD %Rec. RPD
Analyte Result
Qualifier Added
Result Qualifier Unit D %Rec Limits RPD Limit
cyanide, Total <3.5
40.0
41.2 ug/L 103 75 - 125 12 20
TestAmerica Chicago
Page 226 of 258 7/5/2018

QC Sample Results C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Method: 9014 - Cyanide (Continued)
Lab Sample ID: MB 500-429175/1-A
Matrix: Water
Analysis Batch: 429363
MB MB
Analyte Result Qualifier
Cyanide, Total <3.5
Lab Sample ID: LCS 500-429175/2-A
Matrix: Water
Analysis Batch: 429363
Analyte
LCyanide, Total
LLab Sample ID: 500-143858-31 MS
Matrix: Water
Analysis Batch: 429363
Sample
Sample
Analyte Result
Qualifier
Cyanide, Total <3.5
Lab Sample ID: 500-143858-31 MSD
Matrix: Water
Analysis Batch: 429363
Sample
Sample
Analyte Result
Qualifier
Cyanide, Total <3.5
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 429175
RL LOD MDL Unit D Analyzed Dil Fac
10 5.0 3.5 ug/L 04/25/18 09:53 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 429175
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
100 104 ug/L 104 80-120
Client Sample ID: MW11 D(i)
Prep Type: Total/NA
Prep Batch: 429175
Spike MS MS %Rec.
Added Result Qualifier Unit D %Rec Limits
40.0 40.8 ug/L 102 75 -125
Client Sample ID: MW11 D(i)
Prep Type: Total/NA
Prep Batch: 429175
Spike MSD MSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
40.0 42.1 ug/L 105 75 -125 3 20
Method: 9056A - Anions, Ion Chromatography
LLab Sample ID: MB 500-429672/4 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 429672
MB MB
Analyte Result Qualifier RL LOD MDL Unit D Analyzed Dil Fac
Sulfate 114 J 200 100 95 ug/L 04/26/1816:28 1
Lab Sample ID: LCS 500-429672/5 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 429672
Spike
LCS
LCS
%Rec.
Added
Result
Qualifier
Unit
D %Rec Limits
LAnalyte
Sulfate
5000
5040
ug/L
101 80 -120
Lab Sample ID: 500-143858-1 MS
Client Sample ID: MW-12(i)
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 429672
Sample Sample
Spike
MS
MS
%Rec.
Analyte Result Qualifier
Added
Result
Qualifier
Unit
D %Rec Limits
Sulfate 67000 BF1
25000
98200
F1
ug/L
125 80-120
11
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TestAmerica Chicago
7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Method: 9056A - Anions, Ion Chromatography (Continued)
Lab Sample ID: 500-143858-1 MSD
Matrix: Water
Analysis Batch: 429672
Sample Sample
Analyte Result Qualifier
Sulfate 67000 B F1
Lab Sample ID: MB 500-429675/12
Matrix: Water
Analysis Batch: 429675
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Spike MSD MSD
Added Result Qualifier Unit
25000 98900 F1 ug/L
MB MB
Analyte Result Qualifier
Sulfate <95
Lab Sample ID: LCS 500-429675/18
Matrix: Water
Analysis Batch: 429675
Analyte
Sulfate
Lab Sample ID: 500-143858-11
MS
Matrix: Water
Analysis Batch: 429675
Sample
Sample
Analyte
Result
Qualifier
Sulfate
66000
Lab Sample ID: 500-143858-11
MSD
Matrix: Water
Analysis Batch: 429675
Sample
Sample
Analyte
Result
Qualifier
Sulfate
66000
Lab Sample ID: 500-143858-31
MS
Matrix: Water
Analysis Batch: 429675
Sample
Sample
Analyte
Result
Qualifier
Sulfate
180000
Lab Sample ID: 500-143858-31
MSD
Matrix: Water
Analysis Batch: 429675
Sample
Sample
Analyte
Result
Qualifier
Sulfate
180000
Lab Sample ID: MB 500-429810/30
Matrix: Water
Analysis Batch: 429810
Analyte
Chloride
Client Sample ID: MW-12(i)
Prep Type: Total/NA
%Rec. RPD
D %Rec Limits RPD Limit
128 80-120 1 15
Client Sample ID: Method Blank
Prep Type: Total/NA F
RL LOD MDL Unit D Analyzed Dil Fac
200 100 95 ug/L 04/26/1818:47 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
5000 4800 ug/L 96 80-120
Client Sample ID: MW-9D(i)
Prep Type: Total/NA
Spike MS MS %Rec.
Added Result Qualifier Unit D %Rec Limits
25000 93300 ug/L 110 80-120
Client Sample ID: MW-9D(i)
Prep Type: Total/NA
Spike MSD MSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
25000 93500 ug/L 111 80-120 0 15
Client Sample ID: MW11D(i)
Prep Type: Total/NA
Spike MS MS %Rec.
Added Result Qualifier Unit D %Rec Limits
50000 224000 ug/L 96 80-120
Client Sample ID: MW11D(i)
Prep Type: Total/NA
Spike MSD MSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
50000 224000 ug/L 97 80-120 0 15
MB MB
Result Qualifier RL
<170 200
Client Sample ID: Method Blank
Prep Type: Total/NA
LOD MDL Unit D Analyzed Dil Fac
170 170 ug/L 04/27/1815:20 1
Page 228 of 258
TestAmerica Chicago
7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Lab Sample ID: LCS 500-429810/4
Matrix: Water
Analysis Batch: 429810
Analyte
Chloride
Lab Sample ID: 500-143858-1 MS
Matrix: Water
Analysis Batch: 429810
Sample Sample
Analyte Result Qualifier
Chloride 37000 F1
Lab Sample ID: 500-143858-1 MSD
Matrix: Water
Analysis Batch: 429810
Sample Sample
Analyte Result Qualifier
Chloride 37000 F1
Lab Sample ID: MB 500-429826/3
Matrix: Water
Analysis Batch: 429826
Analyte
Chloride
Sulfate
Lab Sample ID: LCS 500-429826/4
Matrix: Water
Analysis Batch: 429826
Analyte
Chloride
Sulfate
Lab Sample ID: 500-143858-11 MS
Matrix: Water
Analysis Batch: 429826
F
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS
LCS
%Rec.
Added
Result
Qualifier
Unit
D %Rec Limits
3000
2900
ug/L
97 80-120
Client Sample ID: MW-12(i)
Prep Type: Total/NA
Spike
MS
MS
%Rec.
Added
Result
Qualifier
Unit
D %Rec Limits
10000
53800
F1
ug/L
164 80-120
Client Sample ID: MW-12(i)
Prep Type: Total/NA
Spike
MSD
MSD
%Rec. RPD
Added
Result
Qualifier
Unit
D %Rec Limits RPD Limit
10000
52900
F1
ug/L
156 80-120 2 15
MB MB
Result Qualifier
<170
<95
Spike
Added
3000
5000
Client Sample ID: Method Blank
Prep Type: Total/NA
RL LOD MDL Unit D Analyzed Dil Fac
200 170 170 ug/L 04/27/1818:01 1
200 100 95 ug/L 04/27/1818:01 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
LCS LCS
Result Qualifier
Unit
2930
ug/L
4860
ug/L
%Rec.
D %Rec Limits
98 80-120
97 80-120
Client Sample ID: MW-9D(i)
Prep Type: Total/NA
Sample
Sample
Spike
MS
MS
%Rec.
Analyte
Result
Qualifier
Added
Result
Qualifier
Unit
D %Rec
Limits
Chloride
36000
F1
10000
50700
F1
ug/L
145
80-120
Lab Sample ID: 500-143858-11
MSD
Client Sample ID: MW-9D(i)
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 429826
Sample
Sample
Spike
MSD
MSD
%Rec. RPD
Analyte
Result
Qualifier
Added
Result
Qualifier
Unit
D %Rec
Limits RPD Limit
Chloride
36000
F1
10000
43600
F1
ug/L
74
80-120 15 15
Page 229 of 258
TestAmerica Chicago
7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Method: SM 2320B - Alkalinity
Lab Sample ID: MB 500-429134/3
Matrix: Water
Analysis Batch: 429134
MB MB
Analyte Result Qualifier
Alkalinity <3700
Lab Sample ID: LCS 500-429134/4
Matrix: Water
Analysis Batch: 429134
Analyte
LAlkalinity
LLab Sample ID: 500-143858-1 DU
Matrix: Water
Analysis Batch: 429134
Sample Sample
Analyte Result Qualifier
Alkalinity 440000
r Lab Sample ID: MB 500-429325/3
Matrix: Water
Analysis Batch: 429325
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: Method Blank
Prep Type: Total/NA
RL LOD MDL Unit D Analyzed Dil Fac
5000 5000 3700 ug/L 04/23/1813:55 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
100000 104000 ug/L 104 85-115
MB MB
Analyte Result Qualifier
Alkalinity <3700
Lab Sample ID: LCS 500-429325/4
Matrix: Water
Analysis Batch: 429325
Client Sample ID: MW-12(i)
Prep Type: Total/NA m
DU DU RPD
Result Qualifier Unit D RPD Limit
444000 ug/L 0.7 20
Client Sample ID: Method Blank
Prep Type: Total/NA
RL LOD MDL Unit D Analyzed Dil Fac
5000 5000 3700 ug/L 04/24/1813:50 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Alkalinity 100000 103000 ug/L 103 85-115
Method: SM 2540C - Solids, Total Dissolved (TDS)
Lab Sample ID: MB 500-428116/1
Matrix: Water
Analysis Batch: 428116
Analyte
Total Dissolved Solids
Lab Sample ID: LCS 500-428116/2
Matrix: Water
Analysis Batch: 428116
Analyte
Total Dissolved Solids
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Result Qualifier RL LOD MDL Unit D Analyzed Dil Fac
<4300 10000 10000 4300 ug/L 04/17/18 07:30 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
250000 284000 ug/L 114 80-120
Page 230 of 258
TestAmerica Chicago
7/5/2018

QC Sample Results
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Method: SM 2540C - Solids, Total Dissolved (TDS) (Continued)
Lab Sample ID: 500-143858-1 DU
Matrix: Water
Analysis Batch: 428116
Sample Sample DU DU
Analyte Result Qualifier Result Qualifier Unit D
Total Dissolved Solids 710000 694000 ug/L
Client Sample ID: MW-12(1)
Prep Type: Total/NA
RPD
RPD Limit
2 5
Lab Sample ID: MB 500-428281/1 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 428281
MB MB
Analyte Result Qualifier RL LOD MDL Unit D Analyzed Dil Fac
Total Dissolved Solids <4300 10000 10000 4300 ug/L 04/17/18 22:44 1
Lab Sample ID: LCS 500-428281/2 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 428281 im
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Total Dissolved Solids 250000 296000 ug/L 118 80 -120 F
Lab Sample ID: MB 500-428478/1 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 428478
MB MB
Analyte Result Qualifier
Total Dissolved Solids <4300
Lab Sample ID: LCS 500-428478/2
Matrix: Water
Analysis Batch: 428478
RL LOD MDL Unit D Analyzed Dil Fac
10000 10000 4300 ug/L 04/19/18 03:54 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Total Dissolved Solids 250000 294000 ug/L 118 80-120
Page 231 of 258
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Lab Chronicle
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Client Sample ID: MW-12(i)
Date Collected: 04/11/18 15:40
Date Received: 04/14/18 12:55
Batch
Batch
Prep Type
Type
Method Run
Total/NA
Analysis
8260B
Total/NA
Prep
3510C
Total/NA
Analysis
8270D
Total/NA
Prep
3510C
Total/NA
Analysis
8081 B
Total/NA
Prep
3510C
Total/NA
Analysis
8082A
Total/NA
Prep
8151A
Total/NA
Analysis
8151A
Dissolved
Prep
3005A
Dissolved
Analysis
6020B
Total Recoverable
Prep
3005A
Total Recoverable
Analysis
6020B
Dissolved
Prep
7470A
Dissolved
Analysis
7470A
Total/NA
Prep
7470A
Total/NA
Analysis
7470A
Total/NA
Prep
9010B
Total/NA
Analysis
9014
Total/NA
Analysis
9056A
Total/NA
Analysis
9056A
Total/NA
Analysis
SM 2320B
Total/NA
Analysis
SM 2540C
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Lab Sample ID: 500-143858-1
Matrix: Water
Dilution
Batch
Prepared
Factor
Number
or Analyzed
Analyst
Lab
1
428915
04/23/18 14:47
JJH
TAL CHI
428028
04/16/18 16:56
JP1
TAL CHI
1
428171
04/17/18 22:46
GES
TAL CHI
428097
04/17/18 07:38
NKG
TAL CHI
1
428535
04/19/18 16:54
WDS
TAL CHI
428097
04/17/18 07:38
NKG
TAL CHI
1
428222
04/17/18 18:12
BJH
TAL CHI
428120
04/17/18 09:02
NKG
TAL CHI
1
427712
04/17/18 22:56
JBJ
TAL CHI
428456
04/18/18 16:50
BIDE
TAL CHI
1
428958
04/21/18 04:35
FXG
TAL CHI
428299
04/18/18 07:07
JEF
TAL CHI
1
428958
04/21/18 02:42
FXG
TAL CHI
428588
04/19/18 12:30
EEN
TAL CHI
1
428749
04/20/18 09:55
EEN
TAL CHI
428144
04/17/18 11:45
EEN
TAL CHI
1
428374
04/18/18 10:44
EEN
TAL CHI
429136
04/24/18 10:10
MAN
TAL CHI
1
429232
MAN
TAL CHI
(Start) 04/24/1815:55
(End) 04/24/1815:55
10
429672
04/26/18 20:48
EAT
TAL CHI
10
429810
04/27/18 12:52
EAT
TAL CHI
1
429134
04/23/18 15:26
SMO
TAL CHI
1
428116
04/17/18 07:45
CLB
TAL CHI
Client Sample ID: MW-14(i)
Date Collected: 04/12/18 14:10
Date Received: 04/14/18 12:55
Batch Batch
Prep Type Type Method
Dilution
Run Factor
Batch
Number
Prepared
or Analyzed
Lab Sample ID: 500-143858-2
Matrix: Water
Analyst Lab
Total/NA Analysis 8260B
1
428915
04/23/18 15:15
JJH
TAL CHI
Total/NA Prep 3510C
428028
04/16/18 16:56
JP1
TAL CHI
Total/NA Analysis 8270D
1
428171
04/17/18 23:15
GES
TAL CHI
Total/NA Prep 3510C
428097
04/17/18 07:38
NKG
TAL CHI
Total/NA Analysis 8081E
1
428535
04/19/18 17:13
WDS
TAL CHI
Total/NA Prep 3510C
428097
04/17/18 07:38
NKG
TAL CHI
Total/NA Analysis 8082A
1
428222
04/17/18 18:28
BJH
TAL CHI
Total/NA Prep 8151A
428120
04/17/18 09:02
NKG
TAL CHI
Total/NA Analysis 8151A
1
427712
04/17/18 23:20
JBJ
TAL CHI
Dissolved Prep 3005A
428456
04/18/18 16:50
BIDE
TAL CHI
Dissolved Analysis 6020E
1
428958
04/21/18 04:54
FXG
TAL CHI
Total Recoverable Prep 3005A
428299
04/18/18 07:07
JEF
TAL CHI
TestAmerica Chicago
Page 232 of 258 7/5/2018

Lab Chronicle
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Client Sample ID: MW-14(i)
Date Collected: 04/12/18 14:10
Date Received: 04/14/18 12:55
Batch Batch
Prep Type Type Method
Dilution
Run Factor
Total Recoverable
Analysis
6020B
1
Dissolved
Prep
7470A
Dissolved
Analysis
7470A
1
Total/NA
Prep
7470A
Total/NA
Analysis
7470A
1
Total/NA
Prep
9010B
Total/NA
Analysis
9014
1
Total/NA
Analysis
9056A
2
Total/NA
Analysis
9056A
2
Total/NA
Analysis
SM 2320B
1
Total/NA
Analysis
SM 2540C
1
Client Sample ID: MW-15(i)
Date Collected: 04/11/18 09:55
Date Received: 04/14/18 12:55
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Lab Sample ID: 500-143858-2
Matrix: Water
Batch Prepared
Number or Analyzed Analyst Lab
428958
04/21/18 02:46
FXG
TAL CHI
428588
04/19/18 12:30
EEN
TAL CHI
428749
04/20/18 09:57
EEN
TAL CHI
428144
04/17/18 11:45
EEN
TAL CHI
428374
04/18/18 10:51
EEN
TAL CHI
429175
04/24/18 14:10
MAN
TAL CHI
429363
MAN
TAL CHI
(Start) 04/25/18 09:55
(End) 04/25/18 09:55
429672
04/26/18 21:50
EAT
TAL CHI
429810
04/27/18 13:29
EAT
TAL CHI
429325
04/24/18 14:17
SMO
TAL CHI
428116
04/17/18 07:50
CLB
TAL CHI
Lab Sample
ID: 500-143858-3
Matrix: Water
Prep Type
Batch
Type
Batch
Method
Dilution
Run Factor
Batch
Number
Prepared
or Analyzed
Analyst
Lab
Total/NA
Analysis
8260B
1
428915
04/23/18 15:44
JJH
TAL CHI
Total/NA
Analysis
9056A
5
429672
04/26/18 22:02
EAT
TAL CHI
Total/NA
Analysis
9056A
20
429810
04/27/18 14:06
EAT
TAL CHI
Total/NA
Analysis
SM 2320B
1
429134
04/23/18 15:42
SMO
TAL CHI
Total/NA
Analysis
SM 2540C
1
428116
04/17/18 07:53
CLB
TAL CHI
Client Sample ID: MW-16(i) Lab Sample ID: 500-143858-4
Date Collected: 04/12/18 10:05 Matrix: Water
Date Received: 04/14/18 12:55
Prep Type
Batch
Type
Batch
Method
Dilution
Run Factor
Batch
Number
Prepared
or Analyzed
Analyst
Lab
Total/NA
Analysis
8260B
1
428915
04/23/18 16:13
JJH
TAL CHI
Total Recoverable
Prep
3005A
428299
04/18/18 07:07
JEF
TAL CHI
Total Recoverable
Analysis
6020B
1
428958
04/21/18 02:50
FXG
TAL CHI
Total/NA
Prep
7470A
428144
04/17/18 11:45
EEN
TAL CHI
Total/NA
Analysis
7470A
1
428374
04/18/18 10:53
EEN
TAL CHI
Total/NA
Analysis
9056A
5
429672
04/26/18 22:39
EAT
TAL CHI
Total/NA
Analysis
9056A
2
429810
04/27/18 14:18
EAT
TAL CHI
Total/NA
Analysis
SM 2320B
1
429325
04/24/18 14:23
SMO
TAL CHI
Total/NA
Analysis
SM 2540C
1
428116
04/17/18 07:55
CLB
TAL CHI
TestAmerica Chicago
Page 233 of 258 7/5/2018

Lab Chronicle
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-1(i)
Lab Sample ID: 500-143858-5
Date Collected: 04/11/18 16:15
Matrix: Water
Date Received: 04/14/18 12:55
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
or Analyzed
Analyst
Lab
Total/NA Analysis 8260B
1
428915
04/23/18 16:40
JJH
TAL CHI
Total/NA Prep 3510C
428028
04/16/18 16:56
JP1
TAL CHI
Total/NA Analysis 8270D
1
428171
04/17/18 23:44
GES
TAL CHI
Total/NA Prep 3510C
428097
04/17/18 07:38
NKG
TAL CHI
Total/NA Analysis 8081B
1
428535
04/19/18 17:33
WDS
TAL CHI
Total/NA Prep 3510C
428097
04/17/18 07:38
NKG
TAL CHI
Total/NA Analysis 8082A
1
428222
04/17/18 18:44
BJH
TAL CHI
Total/NA Prep 8151A
428120
04/17/18 09:02
NKG
TAL CHI
Total/NA Analysis 8151A
1
427712
04/17/18 23:45
JBJ
TAL CHI
Total/NA Prep 9010B
429136
04/24/18 10:10
MAN
TAL CHI
Total/NA Analysis 9014
1
429232
MAN
TAL CHI
(Start) 04/24/1815:56
(End) 04/24/1815:56
Total/NA Analysis 9056A
2
429672
04/26/18 22:51
EAT
TAL CHI
Total/NA Analysis 9056A
5
429810
04/27/18 14:31
EAT
TAL CHI
Total/NA Analysis SM 2320B
1
429134
04/23/18 15:49
SMO
TAL CHI
Total/NA Analysis SM 2540C
1
428116
04/17/18 07:58
CLB
TAL CHI
Client Sample ID: MW-13(i) Lab Sample ID: 500-143858-6
Date Collected: 04/11/18 12:20 Matrix: Water
Date Received: 04/14/18 12:55
Prep Type
Batch
Type
Batch
Method
Dilution
Run Factor
Batch
Number
Prepared
or Analyzed
Analyst
Total/NA
Analysis
8260B
1
428915
04/23/1817:12
JJH
Total/NA
Prep
3510C
428028
04/16/1816:56
JP1
Total/NA
Analysis
8270D
1
428171
04/18/18 00:13
GES
Total/NA
Prep
3510C
428097
04/17/18 07:38
NKG
Total/NA
Analysis
8081B
5
428535
04/19/1817:52
WDS
Total/NA
Prep
3510C
428097
04/17/18 07:38
NKG
Total/NA
Analysis
8082A
1
428222
04/17/1819:01
BJH
Total/NA
Prep
8151A
428120
04/17/18 09:02
NKG
Total/NA
Analysis
8151A
1
427712
04/18/18 00:09
JBJ
Dissolved
Prep
3005A
428456
04/18/1816:50
BIDE
Dissolved
Analysis
6020E
1
428958
04/21/18 04:58
FXG
Total Recoverable
Prep
3005A
428299
04/18/18 07:07
JEF
Total Recoverable
Analysis
6020B
1
428958
04/21/18 02:54
FXG
Dissolved
Prep
7470A
428588
04/19/1812:30
EEN
Dissolved
Analysis
7470A
1
428749
04/20/18 09:58
EEN
Total/NA
Prep
7470A
428144
04/17/1811:45
EEN
Total/NA
Analysis
7470A
1
428374
04/18/1810:54
EEN
Total/NA
Prep
9010E
429136
04/24/1810:10
MAN
Lab
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TestAmerica Chicago
Page 234 of 258 7/5/2018

Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Lab Chronicle C
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-13(i)
Date Collected: 04/11/18 12:20
Date Received: 04/14/18 12:55
Batch Batch
Dilution
Prep Type Type Method
Run Factor
Total/NA Analysis 9014
1
Total/NA Analysis 9056A
1
Total/NA Analysis 9056A
5
Total/NA Analysis SM 2320B
1
Total/NA Analysis SM 2540C
1
Client Sample ID: MW-1213(i)
Date Collected: 04/11/18 14:40
Date Received: 04/14/18 12:55
Batch
Batch
Prep Type
Type
Method
Total/NA
Analysis
8260B
Total/NA
Prep
3510C
Total/NA
Analysis
8270D
Total/NA
Prep
3510C
Total/NA
Analysis
8081 B
Total/NA
Prep
3510C
Total/NA
Analysis
8082A
Total/NA
Prep
8151A
Total/NA
Analysis
8151A
Dissolved
Prep
3005A
Dissolved
Analysis
6020B
Total Recoverable
Prep
3005A
Total Recoverable
Analysis
6020B
Dissolved
Prep
7470A
Dissolved
Analysis
7470A
Total/NA
Prep
7470A
Total/NA
Analysis
7470A
Total/NA
Prep
9010B
Total/NA
Analysis
9014
Dilution
Run Factor
1
1
5
1
1
1
1
1
1
1
Total/NA
Analysis
9056A 20
Total/NA
Analysis
9056A 20
Total/NA
Analysis
SM 2320B 1
Total/NA
Analysis
SM 2540C 1
Lab Sample ID: 500-143858-6
Matrix: Water
Batch Prepared
Number or Analyzed Analyst Lab
429232
MAN
TAL CHI
(Start) 04/24/1815:56
(End) 04/24/1815:56
429672 04/26/18 23:16
EAT
TAL CHI
429810 04/27/18 14:43
EAT
TAL CHI
429134 04/23/18 15:56
SMO
TAL CHI
428116 04/17/18 08:01
CLB
TAL CHI
Lab Sample
ID: 500-143858-7
Matrix: Water
Batch Prepared
Number or Analyzed Analyst Lab
428915
04/23/18 17:44
JJH
TAL CHI
428028
04/16/18 16:56
JP1
TAL CHI
428171
04/18/18 00:42
GES
TAL CHI
428097
04/17/18 07:38
NKG
TAL CHI
428535
04/19/18 18:11
WDS
TAL CHI
428097
04/17/18 07:38
NKG
TAL CHI
428222
04/17/18 19:17
BJH
TAL CHI
428120
04/17/18 09:02
NKG
TAL CHI
427712
04/18/18 00:33
JBJ
TAL CHI
428456
04/18/18 16:50
BIDE
TAL CHI
428958
04/21/18 05:02
FXG
TAL CHI
428299
04/18/18 07:07
JEF
TAL CHI
428958
04/21/18 02:57
FXG
TAL CHI
428588
04/19/18 12:30
EEN
TAL CHI
428749
04/20/18 10:03
EEN
TAL CHI
428144
04/17/18 11:45
EEN
TAL CHI
428374
04/18/18 10:56
EEN
TAL CHI
429136
04/24/18 10:10
MAN
TAL CHI
429232
MAN
TAL CHI
(Start) 04/24/1815:56
(End) 04/24/1815:56
429672
04/27/18 00:06
EAT
TAL CHI
429810
04/27/18 14:55
EAT
TAL CHI
429134
04/23/18 15:14
SMO
TAL CHI
428116
04/17/18 08:03
CLB
TAL CHI
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Lab Chronicle
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Client Sample ID: MW-8D(i)
Date Collected: 04/11/18 14:35
Date Received: 04/14/18 12:55
Batch Batch
Prep Type Type Method
Dilution
Run Factor
Total/NA
Analysis
8260B
1
Total/NA
Prep
3510C
Total/NA
Analysis
8270D
1
Total/NA
Prep
3510C
Total/NA
Analysis
8081 B
1
Total/NA
Prep
3510C
Total/NA
Analysis
8082A
1
Total/NA
Prep
8151A
Total/NA
Analysis
8151A
1
Total Recoverable
Prep
3005A
Total Recoverable
Analysis
6020B
1
Total/NA
Prep
7470A
Total/NA
Analysis
7470A
1
Total/NA
Prep
9010B
Total/NA
Analysis
9014
1
Total/NA
Analysis
9056A
5
Total/NA
Analysis
9056A
20
Total/NA
Analysis
SM 2320B
1
Total/NA
Analysis
SM 2540C
1
Client Sample ID: MW-5(i)
Date Collected: 04/11/18 11:40
Date Received: 04/14/18 12:55
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Lab Sample ID: 500-143858-8
Matrix: Water
Batch Prepared
Number or Analyzed Analyst
428915
04/23/1818:12
JJH
428028
04/16/1816:56
JP1
428171
04/18/18 01:11
GES
428097
04/17/18 07:38
NKG
428753
04/20/1814:44
WDS
428097
04/17/18 07:38
NKG
428222
04/17/1819:33
BJH
428120
04/17/18 09:02
NKG
427712
04/18/18 00:58
JBJ
428299
04/18/18 07:07
JEF
428958
04/21/18 03:01
FXG
428144
04/17/1811:45
EEN
428374
04/18/1811:01
EEN
429175
04/24/1814:10
MAN
429363
MAN
(Start) 04/25/18 09:56
(End) 04/25/18 09:56
429672
04/27/18 00:18
EAT
429810
04/27/1815:08
EAT
429134
04/23/1816:03
SMO
428116
04/17/18 08:06
CLB
Lab
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
Lab Sample ID: 500-143858-9
Matrix: Water
Prep Type
Batch
Type
Batch
Method
Dilution
Run Factor
Batch
Number
Prepared
or Analyzed
Analyst
Lab
Total/NA
Analysis
8260B
1
428915
04/23/18 18:41
JJH
TAL CHI
Total/NA
Prep
3510C
428028
04/16/18 16:56
JP1
TAL CHI
Total/NA
Analysis
8270D
1
428171
04/18/18 01:40
GES
TAL CHI
Total/NA
Prep
3510C
428097
04/17/18 07:38
NKG
TAL CHI
Total/NA
Analysis
8081B
1
428753
04/20/18 15:03
WDS
TAL CHI
Total/NA
Prep
3510C
428097
04/17/18 07:38
NKG
TAL CHI
Total/NA
Analysis
8082A
1
428222
04/17/18 19:49
BJH
TAL CHI
Total/NA
Prep
8151A
428120
04/17/18 09:02
NKG
TAL CHI
Total/NA
Analysis
8151A
1
427712
04/18/18 01:22
JBJ
TAL CHI
Total Recoverable
Prep
3005A
428299
04/18/18 07:07
JEF
TAL CHI
Total Recoverable
Analysis
6020E
1
428958
04/21/18 03:05
FXG
TAL CHI
Total/NA
Prep
7470A
428144
04/17/18 11:45
EEN
TAL CHI
Total/NA
Analysis
7470A
1
428374
04/18/18 11:02
EEN
TAL CHI
Total/NA
Prep
9010E
429175
04/24/18 14:10
MAN
TAL CHI
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7/5/2018

Lab Chronicle
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Client Sample ID: MW-5(i)
Date Collected: 04/11/18 11:40
Date Received: 04/14/18 12:55
Batch Batch
Dilution
Prep Type Type Method
Run Factor
Total/NA Analysis 9014
1
Total/NA Analysis 9056A
10
Total/NA Analysis 9056A
10
Total/NA Analysis SM 2320B
1
Total/NA Analysis SM 2540C
1
Client Sample ID: MW-9(i)
Date Collected: 04/10/18 14:10
Date Received: 04/14/18 12:55
Prep Type
Batch
Type
Batch
Method
Dilution
Run Factor
Total/NA
Analysis
8260B
1
Total/NA
Prep
3510C
Total/NA
Analysis
8270D
1
Total/NA
Prep
3510C
Total/NA
Analysis
8081 B
1
Total/NA
Prep
3510C
Total/NA
Analysis
8082A
1
Total/NA
Prep
8151A
Total/NA
Analysis
8151A
1
Total Recoverable
Prep
3005A
Total Recoverable
Analysis
6020B
1
Total/NA
Prep
7470A
Total/NA
Analysis
7470A
1
Total/NA
Prep
9010B
Total/NA
Analysis
9014
1
Total/NA
Analysis
9056A 10
Total/NA
Analysis
9056A 10
Total/NA
Analysis
SM 2320B 1
Total/NA
Analysis
SM 2540C 1
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Lab Sample ID: 500-143858-9
Matrix: Water
Batch Prepared
Number or Analyzed Analyst Lab
429363 MAN TAL CHI
(Start) 04/25/18 09:58
(End) 04/25/18 09:59
429826 04/27/18 18:51 EAT TAL CHI
429675 04/26/18 19:12 EAT TAL CHI
429134 04/23/18 14:20 SMO TAL CHI
428116 04/17/18 08:08 CLB TAL CHI
Lab Sample ID: 500-143858-10
Matrix: Water
Batch
Prepared
Number
or Analyzed
Analyst
Lab
428915
04/23/18 19:09
JJH
TAL CHI
428028
04/16/18 16:56
JP1
TAL CHI
428757
04/20/18 14:50
WDS
TAL CHI
428097
04/17/18 07:38
NKG
TAL CHI
428753
04/20/18 15:23
WDS
TAL CHI
428097
04/17/18 07:38
NKG
TAL CHI
428222
04/17/18 20:06
BJH
TAL CHI
428120
04/17/18 09:02
NKG
TAL CHI
427712
04/18/18 02:35
JBJ
TAL CHI
428299
04/18/18 07:07
JEF
TAL CHI
428958
04/21/18 03:09
FXG
TAL CHI
428144
04/17/18 11:45
EEN
TAL CHI
428374
04/18/18 11:04
EEN
TAL CHI
429136
04/24/18 10:10
MAN
TAL CHI
429232
MAN
TAL CHI
(Start) 04/24/1815:56
(End) 04/24/1815:57
429826
04/27/18 19:03
EAT
TAL CHI
429675
04/26/18 19:25
EAT
TAL CHI
429134
04/23/18 16:13
SMO
TAL CHI
428116
04/17/18 08:11
CLB
TAL CHI
Client Sample ID: MW-9D(i) Lab Sample ID: 500-143858-11
Date Collected: 04/10/18 13:30 Matrix: Water
Date Received: 04/14/18 12:55
Batch
Batch
Prep Type
Type
Method Run
Total/NA
Analysis
8260B
Total/NA
Prep
3510C
Total/NA
Analysis
8270D
Dilution
Batch
Prepared
Factor
Number
or Analyzed
Analyst
Lab
1
428915
04/23/18 19:38
JJH
TAL CHI
428028
04/16/18 16:56
JP1
TAL CHI
1
428521
04/19/18 16:58
AJD
TAL CHI
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7/5/2018

Lab Chronicle
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Batch
Batch
Dilution
Prep Type
Type
Method
Run Factor
Total/NA
Prep
3510C
Total/NA
Analysis
8081 B
1
Total/NA
Prep
3510C
Total/NA
Analysis
8082A
1
Total/NA
Prep
8151A
Total/NA
Analysis
8151A
1
Total Recoverable
Prep
3005A
Total Recoverable
Analysis
6020B
1
Total/NA
Prep
7470A
Total/NA
Analysis
7470A
1
Total/NA
Prep
9010B
Total/NA
Analysis
9014
1
Total/NA
Analysis
9056A
10
Total/NA
Analysis
9056A
10
Total/NA
Analysis
SM 2320B
1
Total/NA
Analysis
SM 2540C
1
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Batch
Prepared
Number
or Analyzed
Analyst
Lab
428097
04/17/18 07:38
NKG
TAL CHI
428753
04/20/18 15:42
WDS
TAL CHI
428097
04/17/18 07:38
NKG
TAL CHI
428222
04/17/18 20:22
BJH
TAL CHI
428120
04/17/18 09:02
NKG
TAL CHI
427712
04/18/18 03:00
JBJ
TAL CHI
428299
04/18/18 07:07
JEF
TAL CHI
428958
04/21/18 03:20
FXG
TAL CHI
428144
04/17/18 11:45
EEN
TAL CHI
428374
04/18/18 11:06
EEN
TAL CHI
429136
04/24/18 10:10
MAN
TAL CHI
429232
MAN
TAL CHI
(Start) 04/24/1815:57
(End) 04/24/1815:57
429826
04/27/18 19:16
EAT
TAL CHI
429675
04/26/18 19:38
EAT
TAL CHI
429134
04/23/18 16:24
SMO
TAL CHI
428116
04/17/18 08:13
CLB
TAL CHI
Client Sample ID: MW-10(i) Lab Sample ID: 500-143858-12
Date Collected: 04/11/18 10:50 Matrix: Water
Date Received: 04/14/18 12:55
Prep Type
Batch
Type
Batch
Method
Dilution
Run Factor
Total/NA
Analysis
8260B
1
Total/NA
Prep
3510C
Total/NA
Analysis
8270D
1
Total/NA
Prep
3510C
Total/NA
Analysis
8081 B
1
Total/NA
Prep
3510C
Total/NA
Analysis
8082A
1
Total/NA
Prep
8151A
Total/NA
Analysis
8151A
1
Total/NA
Prep
9010B
Total/NA
Analysis
9014
1
Total/NA
Analysis
9056A
10
Total/NA
Analysis
9056A
20
Total/NA
Analysis
SM 2320B
1
Total/NA
Analysis
SM 2540C
1
Batch Prepared
Number or Analyzed Analyst
428915 04/23/18 20:07 JJH
428028 04/16/1816:56 JP1
428757 04/20/1815:15 WDS
428097 04/17/18 07:38 NKG
428753 04/20/1816:01 WDS
428097 04/17/18 07:38 NKG
428222 04/17/18 20:38 BJH
428120 04/17/18 09:02 NKG
427712 04/18/18 03:24 JBJ
429175 04/24/1814:10 MAN
429363 MAN
(Start) 04/25/18 09:57
(End) 04/25/18 09:57
429826 04/27/1819:53 EAT
429826 04/27/18 20:30 EAT
429134 04/23/1816:31 SMO
428116 04/17/18 08:16 CLB
Lab
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TestAmerica Chicago
Page 238 of 258 7/5/2018

Lab Chronicle
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Client Sample ID: MW-8(i)
Date Collected: 04/10/18 15:15
Date Received: 04/14/18 12:55
Batch Batch
Prep Type Type Method
Dilution
Run Factor
Total/NA
Analysis
8260B
1
Total/NA
Prep
3510C
Total/NA
Analysis
8270D
1
Total/NA
Prep
3510C
Total/NA
Analysis
8081 B
1
Total/NA
Prep
3510C
Total/NA
Analysis
8082A
1
Total/NA
Prep
8151A
Total/NA
Analysis
8151A
1
Total Recoverable
Prep
3005A
Total Recoverable
Analysis
6020B
1
Total/NA
Prep
7470A
Total/NA
Analysis
7470A
1
Total/NA
Prep
9010B
Total/NA
Analysis
9014
1
Total/NA
Analysis
9056A
20
Total/NA
Analysis
9056A
1
Total/NA
Analysis
SM 2320B
1
Total/NA
Analysis
SM 2540C
1
Client Sample ID: MW-2(i)
Date Collected: 04/12/18 10:10
Date Received: 04/14/18 12:55
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Lab Sample ID: 500-143858-13
Matrix: Water
Batch Prepared
Number or Analyzed Analyst
429099 04/24/1814:00 JJH
428028 04/16/1816:56 JP1
428757 04/20/1815:41 WDS
428097 04/17/18 07:38 NKG
428753 04/20/1816:21 WDS
428097 04/17/18 07:38 NKG
428222 04/17/18 20:54 BJH
428120 04/17/18 09:02 NKG
427712 04/18/18 03:48 JBJ
428299 04/18/18 07:07 JEF
428958 04/21/18 03:24 FXG
428144 04/17/1811:45 EEN
428374 04/18/1811:07 EEN
429136 04/24/1810:10 MAN
429232 MAN
(Start) 04/24/1815:58
(End) 04/24/1815:58
429826 04/27/18 20:43 EAT
429675 04/26/18 20:28 EAT
429134 04/23/1816:38 SMO
428116 04/17/18 08:19 CLB
Lab
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
Lab Sample ID: 500-143858-14
Matrix: Water
Prep Type
Batch
Type
Batch
Method
Dilution
Run Factor
Batch
Number
Prepared
or Analyzed
Analyst
Lab
Total/NA
Analysis
8260B
1
429099
04/24/18 14:25
JJH
TAL CHI
Total/NA
Prep
3510C
428028
04/16/18 16:56
JP1
TAL CHI
Total/NA
Analysis
8270D
1
428757
04/20/18 16:06
WDS
TAL CHI
Total/NA
Prep
3510C
428097
04/17/18 07:38
NKG
TAL CHI
Total/NA
Analysis
8081B
1
428753
04/20/18 16:40
WDS
TAL CHI
Total/NA
Prep
3510C
428097
04/17/18 07:38
NKG
TAL CHI
Total/NA
Analysis
8082A
1
428222
04/17/18 21:11
BJH
TAL CHI
Total/NA
Prep
8151A
428120
04/17/18 09:02
NKG
TAL CHI
Total/NA
Analysis
8151A
1
427712
04/18/18 04:13
JBJ
TAL CHI
Total Recoverable
Prep
3005A
428299
04/18/18 07:07
JEF
TAL CHI
Total Recoverable
Analysis
6020B
1
428958
04/21/18 03:43
FXG
TAL CHI
Total/NA
Prep
7470A
428144
04/17/18 11:45
EEN
TAL CHI
Total/NA
Analysis
7470A
1
428374
04/18/18 11:09
EEN
TAL CHI
Total/NA
Prep
9010B
429175
04/24/18 14:10
MAN
TAL CHI
TestAmerica Chicago
Page 239 of 258 7/5/2018

Lab Chronicle
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Client Sample ID: MW-2(i)
Date Collected: 04/12/18 10:10
Date Received: 04/14/18 12:55
Batch Batch
Dilution
Prep Type Type Method
Run Factor
Total/NA Analysis 9014
1
Total/NA Analysis 9056A
5
Total/NA Analysis 9056A
25
Total/NA Analysis SM 2320B
1
Total/NA Analysis SM 2540C
1
Client Sample ID: MW-3(i)
Date Collected: 04/12/18 11:00
Date Received: 04/14/18 12:55
Prep Type
Batch
Type
Batch
Method
Dilution
Run Factor
Total/NA
Analysis
8260B
1
Total/NA
Prep
3510C
Total/NA
Analysis
8270D
1
Total/NA
Prep
3510C
Total/NA
Analysis
8081 B
1
Total/NA
Prep
3510C
Total/NA
Analysis
8082A
1
Total/NA
Prep
8151A
Total/NA
Analysis
8151A
1
Total Recoverable
Prep
3005A
Total Recoverable
Analysis
6020B
1
Total/NA
Prep
7470A
Total/NA
Analysis
7470A
1
Total/NA
Prep
9010B
Total/NA
Analysis
9014
1
Total/NA
Analysis
9056A 5
Total/NA
Analysis
9056A 25
Total/NA
Analysis
SM 2320B 1
Total/NA
Analysis
SM 2540C 1
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Lab Sample ID: 500-143858-14
Matrix: Water
Batch Prepared
Number or Analyzed Analyst Lab
429363 MAN TAL CHI
(Start) 04/25/18 09:55
(End) 04/25/18 09:55
429826 04/27/18 20:55 EAT TAL CHI
429675 04/26/18 20:41 EAT TAL CHI
429325 04/24/18 14:29 SMO TAL CHI
428116 04/17/18 08:21 CLB TAL CHI
Lab Sample ID: 500-143858-15
Matrix: Water
Batch
Prepared
Number
or Analyzed
Analyst
Lab
429099
04/24/18 14:52
JJH
TAL CHI
428028
04/16/18 16:56
JP1
TAL CHI
428757
04/20/18 16:32
WDS
TAL CHI
428097
04/17/18 07:38
NKG
TAL CHI
428753
04/20/18 16:59
WDS
TAL CHI
428097
04/17/18 07:38
NKG
TAL CHI
428222
04/17/18 21:27
BJH
TAL CHI
428120
04/17/18 09:02
NKG
TAL CHI
427712
04/18/18 04:37
JBJ
TAL CHI
428299
04/18/18 07:07
JEF
TAL CHI
428958
04/21/18 03:46
FXG
TAL CHI
428144
04/17/18 11:45
EEN
TAL CHI
428374
04/18/18 11:10
EEN
TAL CHI
429175
04/24/18 14:10
MAN
TAL CHI
429363
MAN
TAL CHI
(Start) 04/25/18 09:55
(End) 04/25/18 09:56
429826
04/27/18 21:07
EAT
TAL CHI
429675
04/26/18 21:19
EAT
TAL CHI
429325
04/24/18 14:35
SMO
TAL CHI
428116
04/17/18 08:24
CLB
TAL CHI
Client Sample ID: MW-4D(i) Lab Sample ID: 500-143858-16
Date Collected: 04/12/18 12:45 Matrix: Water
Date Received: 04/14/18 12:55
Batch
Batch
Prep Type
Type
Method Run
Total/NA
Analysis
8260B
Total/NA
Prep
3510C
Total/NA
Analysis
8270D
Dilution
Batch
Prepared
Factor
Number
or Analyzed
Analyst
Lab
1
429099
04/24/18 15:18
JJH
TAL CHI
428028
04/16/18 16:56
JP1
TAL CHI
1
428757
04/20/18 16:57
WDS
TAL CHI
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Lab Chronicle
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Batch
Batch
Dilution
Prep Type
Type
Method
Run Factor
Total/NA
Prep
3510C
Total/NA
Analysis
8081 B
1
Total/NA
Prep
3510C
Total/NA
Analysis
8082A
1
Total/NA
Prep
8151A
Total/NA
Analysis
8151A
1
Total Recoverable
Prep
3005A
Total Recoverable
Analysis
6020B
1
Total/NA
Prep
7470A
Total/NA
Analysis
7470A
1
Total/NA
Prep
9010B
Total/NA
Analysis
9014
1
Total/NA
Analysis
9056A
5
Total/NA
Analysis
9056A
5
Total/NA
Analysis
SM 2320B
1
Total/NA
Analysis
SM 2540C
1
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Batch
Prepared
Number
or Analyzed
Analyst
Lab
428097
04/17/18 07:38
NKG
TAL CHI
428753
04/20/18 17:19
WDS
TAL CHI
428097
04/17/18 07:38
NKG
TAL CHI
428222
04/17/18 21:43
BJH
TAL CHI
428120
04/17/18 09:02
NKG
TAL CHI
427712
04/18/18 05:02
JBJ
TAL CHI
428299
04/18/18 07:07
JEF
TAL CHI
428958
04/21/18 03:50
FXG
TAL CHI
428144
04/17/18 11:45
EEN
TAL CHI
428374
04/18/18 11:12
EEN
TAL CHI
429175
04/24/18 14:10
MAN
TAL CHI
429363
MAN
TAL CHI
(Start) 04/25/18 09:56
(End) 04/25/18 09:56
429826
04/27/18 21:20
EAT
TAL CHI
429675
04/26/18 21:32
EAT
TAL CHI
429325
04/24/18 14:42
SMO
TAL CHI
428116
04/17/18 08:26
CLB
TAL CHI
Client Sample ID: MW-4(i) Lab Sample ID: 500-143858-17
Date Collected: 04/12/18 14:10 Matrix: Water
Date Received: 04/14/18 12:55
Prep Type
Batch
Type
Batch
Method
Dilution
Run Factor
Batch
Number
Prepared
or Analyzed
Analyst
Lab
Total/NA
Analysis
8260B
1
429285
04/25/18 11:24
PMF
TAL CHI
Total/NA
Prep
3510C
428028
04/16/18 16:56
JP1
TAL CHI
Total/NA
Analysis
8270D
1
428757
04/20/18 17:23
WDS
TAL CHI
Total/NA
Prep
3510C
428097
04/17/18 07:38
NKG
TAL CHI
Total/NA
Analysis
8081B
1
428753
04/20/18 17:38
WDS
TAL CHI
Total/NA
Prep
3510C
428097
04/17/18 07:38
NKG
TAL CHI
Total/NA
Analysis
8082A
1
428222
04/17/18 22:32
BJH
TAL CHI
Total/NA
Prep
8151A
428120
04/17/18 09:02
NKG
TAL CHI
Total/NA
Analysis
8151A
1
427712
04/18/18 05:26
JBJ
TAL CHI
Total Recoverable
Prep
3005A
428299
04/18/18 07:07
JEF
TAL CHI
Total Recoverable
Analysis
6020B
1
428958
04/21/18 03:54
FXG
TAL CHI
Total/NA
Prep
7470A
428144
04/17/18 11:45
EEN
TAL CHI
Total/NA
Analysis
7470A
1
428374
04/18/18 11:14
EEN
TAL CHI
Total/NA
Prep
9010B
429175
04/24/18 14:10
MAN
TAL CHI
Total/NA
Analysis
9014
1
429363
MAN
TAL CHI
(Start) 04/25/18 09:59
(End) 04/25/18 09:59
Total/NA
Analysis
9056A
5
429826
04/27/18 21:32
EAT
TAL CHI
Total/NA
Analysis
9056A
5
429675
04/26/18 21:44
EAT
TAL CHI
Total/NA
Analysis
SM 2320B
1
429325
04/24/18 14:11
SMO
TAL CHI
Total/NA
Analysis
SM 2540C
1
428116
04/17/18 08:29
CLB
TAL CHI
TestAmerica Chicago
Page 241 of 258 7/5/2018

Lab Chronicle
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Client Sample ID: MW-6(i)
Date Collected: 04/11/18 12:20
Date Received: 04/14/18 12:55
Batch Batch
Prep Type Type Method
Dilution
Run Factor
Total/NA
Analysis
8260B
1
Total/NA
Prep
3510C
Total/NA
Analysis
8270D
1
Total/NA
Prep
3510C
Total/NA
Analysis
8081 B
1
Total/NA
Prep
3510C
Total/NA
Analysis
8082A
1
Total/NA
Prep
8151A
Total/NA
Analysis
8151A
1
Total Recoverable
Prep
3005A
Total Recoverable
Analysis
6020B
1
Total/NA
Prep
7470A
Total/NA
Analysis
7470A
1
Total/NA
Prep
9010B
Total/NA
Analysis
9014
1
Total/NA
Analysis
9056A
10
Total/NA
Analysis
9056A
1
Total/NA
Analysis
SM 2320B
1
Total/NA
Analysis
SM 2540C
1
Client Sample ID: MW-7D(i)
Date Collected: 04/11/18 09:30
Date Received: 04/14/18 12:55
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Lab Sample ID: 500-143858-18
Matrix: Water
Batch Prepared
Number or Analyzed Analyst
429099 04/24/1816:10 JJH
428028 04/16/1816:56 JP1
428757 04/20/1817:48 WDS
428097 04/17/18 07:38 NKG
428753 04/20/1817:57 WDS
428097 04/17/18 07:38 NKG
428222 04/17/18 22:48 BJH
428120 04/17/18 09:02 NKG
427712 04/18/18 05:50 JBJ
428299 04/18/18 07:07 JEF
428958 04/21/18 04:05 FXG
428144 04/17/1811:45 EEN
428374 04/18/1811:15 EEN
429175 04/24/1814:10 MAN
429363 MAN
(Start) 04/25/18 09:59
(End) 04/25/18 09:59
429826 04/27/18 21:44 EAT
429675 04/26/18 21:57 EAT
429134 04/23/1815:05 SMO
428281 04/17/18 23:04 CLB
Lab
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
Lab Sample ID: 500-143858-19
Matrix: Water
Prep Type
Batch
Type
Batch
Method
Dilution
Run Factor
Batch
Number
Prepared
or Analyzed
Analyst
Lab
Total/NA
Analysis
8260B
1
429099
04/24/18 16:35
JJH
TAL CHI
Total/NA
Prep
3510C
428028
04/16/18 16:56
JP1
TAL CHI
Total/NA
Analysis
8270D
1
428521
04/19/18 20:23
AJD
TAL CHI
Total/NA
Prep
3510C
428097
04/17/18 07:38
NKG
TAL CHI
Total/NA
Analysis
8081B
5
428753
04/20/18 18:17
WDS
TAL CHI
Total/NA
Prep
3510C
428097
04/17/18 07:38
NKG
TAL CHI
Total/NA
Analysis
8082A
1
428222
04/17/18 23:04
BJH
TAL CHI
Total/NA
Prep
8151A
428120
04/17/18 09:02
NKG
TAL CHI
Total/NA
Analysis
8151A
1
427712
04/18/18 06:15
JBJ
TAL CHI
Total Recoverable
Prep
3005A
428299
04/18/18 07:07
JEF
TAL CHI
Total Recoverable
Analysis
6020B
1
428958
04/21/18 04:09
FXG
TAL CHI
Total/NA
Prep
7470A
428144
04/17/18 11:45
EEN
TAL CHI
Total/NA
Analysis
7470A
1
428374
04/18/18 11:20
EEN
TAL CHI
Total/NA
Prep
9010B
429175
04/24/18 14:10
MAN
TAL CHI
TestAmerica Chicago
Page 242 of 258 7/5/2018

Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Lab Chronicle C
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW-7D(i)
Date Collected: 04/11/18 09:30
Date Received: 04/14/18 12:55
Batch Batch
Dilution
Prep Type Type Method
Run Factor
Total/NA Analysis 9014
1
Total/NA Analysis 9056A
25
Total/NA Analysis 9056A
25
Total/NA Analysis SM 2320B
1
Total/NA Analysis SM 2540C
1
Client Sample ID: MW-513(i)
Date Collected: 04/11/18 11:10
Date Received: 04/14/18 12:55
Batch
Batch
Prep Type
Type
Method
Total/NA
Analysis
8260B
Total/NA
Prep
3510C
Total/NA
Analysis
8270D
Total/NA
Prep
3510C
Total/NA
Analysis
8081 B
Total/NA
Prep
3510C
Total/NA
Analysis
8082A
Total/NA
Prep
8151A
Total/NA
Analysis
8151A
Total Recoverable
Prep
3005A
Total Recoverable
Analysis
6020B
Total/NA
Prep
7470A
Total/NA
Analysis
7470A
Total/NA
Prep
9010B
Total/NA
Analysis
9014
Total/NA
Analysis
9056A
Total/NA
Analysis
SM 2320B
Total/NA
Analysis
SM 2540C
Client Sample ID: MW-7(i)
Date Collected: 04/11/18 10:10
Date Received: 04/14/18 12:55
Batch Batch
Prep Type Type Method
Total/NA Analysis 8260B
Total/NA Prep 3510C
Total/NA Analysis 8270D
Total/NA Prep 3510C
Lab Sample ID: 500-143858-19
Matrix: Water
Batch Prepared
Number or Analyzed Analyst Lab
429363
MAN
TAL CHI
(Start) 04/25/18 09:58
(End) 04/25/18 09:58
429826 04/27/18 21:57
EAT
TAL CHI
429675 04/26/18 22:10
EAT
TAL CHI
429134 04/23/18 16:51
SMO
TAL CHI
428281 04/17/18 23:07
CLB
TAL CHI
Lab Sample
ID: 500-143858-20
Matrix: Water
Dilution
Run Factor
Batch
Number
Prepared
or Analyzed
Analyst
Lab
1
429099
04/24/18 17:26
JJH
TAL CHI
428028
04/16/18 16:56
JP1
TAL CHI
1
428757
04/20/18 18:14
WDS
TAL CHI
428097
04/17/18 07:38
NKG
TAL CHI
1
428753
04/20/18 18:55
WDS
TAL CHI
428097
04/17/18 07:38
NKG
TAL CHI
1
428222
04/17/18 23:21
BJH
TAL CHI
428351
04/18/18 10:05
NKG
TAL CHI
1
428477
04/19/18 03:17
JBJ
TAL CHI
428299
04/18/18 07:07
JEF
TAL CHI
1
428958
04/21/18 04:13
FXG
TAL CHI
428144
04/17/18 11:45
EEN
TAL CHI
1
428374
04/18/18 11:22
EEN
TAL CHI
429175
04/24/18 14:10
MAN
TAL CHI
1
429363
MAN
TAL CHI
(Start) 04/25/18 09:57
(End) 04/25/18 09:58
5
429826
04/27/18 22:09
EAT
TAL CHI
1
429134
04/23/18 17:00
SMO
TAL CHI
1
428281
04/17/18 23:09
CLB
TAL CHI
Lab Sample ID: 500-143858-21
Matrix: Water
Dilution
Batch
Prepared
Run Factor
Number
or Analyzed
Analyst
Lab
1
429285
04/25/18 11:54
PMF
TAL CHI
428028
04/16/18 16:56
JP1
TAL CHI
1
428757
04/20/18 18:39
WDS
TAL CHI
428097
04/17/18 07:38
NKG
TAL CHI
Page 243 of 258
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7/5/2018

Lab Chronicle
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Client Sample ID: MW-7(i)
Date Collected: 04/11/18 10:10
Date Received: 04/14/18 12:55
Batch Batch
Prep Type Type Method
Dilution
Run Factor
Total/NA
Analysis
8081 B
5
Total/NA
Prep
3510C
Total/NA
Analysis
8082A
1
Total/NA
Prep
8151A
Total/NA
Analysis
8151A
1
Total Recoverable
Prep
3005A
Total Recoverable
Analysis
6020B
1
Total/NA
Prep
7470A
Total/NA
Analysis
7470A
1
Total/NA
Prep
9010B
Total/NA
Analysis
9014
1
Total/NA
Analysis
9056A
20
Total/NA
Analysis
9056A
20
Total/NA
Analysis
SM 2320B
1
Total/NA
Analysis
SM 2540C
1
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Lab Sample ID: 500-143858-21
Matrix: Water
Batch Prepared
Number or Analyzed Analyst Lab
429503
04/26/18 13:09
WDS
TAL CHI
428097
04/17/18 07:38
NKG
TAL CHI
428222
04/17/18 23:37
BJH
TAL CHI
428351
04/18/18 10:05
NKG
TAL CHI
428477
04/19/18 03:42
JBJ
TAL CHI
428299
04/18/18 07:07
JEF
TAL CHI
428958
04/21/18 04:16
FXG
TAL CHI
428144
04/17/18 11:45
EEN
TAL CHI
428374
04/18/18 11:23
EEN
TAL CHI
429175
04/24/18 14:10
MAN
TAL CHI
429363
MAN
TAL CHI
(Start) 04/25/18 09:58
(End) 04/25/18 09:58
429826
04/27/18 22:21
EAT
TAL CHI
429675
04/26/18 22:35
EAT
TAL CHI
429134
04/23/18 17:09
SMO
TAL CHI
428281
04/17/18 23:12
CLB
TAL CHI
Client Sample ID: Duplicate Lab Sample ID: 500-143858-22
Date Collected: 04/10/18 00:00 Matrix: Water
Date Received: 04/14/18 12:55
F Batch Batch
Prep Type Type Method
Total/NA Analysis 8260B
Client Sample ID: Duplicate 1
Date Collected: 04/11/18 00:00
Date Received: 04/14/18 12:55
Dilution Batch Prepared
Run Factor Number or Analyzed Analyst Lab
1 428709 04/20/18 17:36 JJH TAL CHI
Batch
Batch
Prep Type Type
Method Run
Total/NA Analysis
8260B
Total/NA Analysis
8260B
Client Sample ID: Duplicate 2
Date Collected: 04/12/18 00:00
Date Received: 04/14/18 12:55
Lab Sample ID: 500-143858-23
Matrix: Water
Dilution
Batch
Prepared
Factor
Number
or Analyzed Analyst Lab
1
429099
04/24/18 17:01 JJH TAL CHI
1
429285
04/25/18 12:24 PMF TAL CHI
Lab Sample ID: 500-143858-24
Matrix: Water
Batch
Prep Type Type
Batch
Method
Dilution
Run Factor
Batch
Number
Prepared
or Analyzed Analyst Lab
Total/NA Analysis
8260B
1
429285
04/25/18 12:54 PMF TAL CHI
Page 244 of 258
TestAmerica Chicago
7/5/2018

Lab Chronicle
Client: Civil & Environmental Consultants Inc
Project/Site: NC North Mecklenburg Landfill - Infill
Client Sample ID: TB
Date Collected: 04/10/18 00:00
Date Received: 04/14/18 12:55
Batch Batch
Prep Type Type Method
Total/NA Analysis 8260B
TestAmerica Job ID: 500-143858-1
SDG: NCDEQ Solid Waste Facility = # 60-13
Lab Sample ID: 500-143858-25
Matrix: Water
Dilution Batch Prepared
Run Factor Number or Analyzed Analyst Lab
1 428709 04/20/18 18:05 JJH TAL CHI
Client Sample ID: TB Lab Sample ID: 500-143858-26
Date Collected: 04/10/18 00:00 Matrix: Water
Date Received: 04/14/18 12:55
F Batch Batch
Prep Type Type Method Run
Total/NA Analysis 8260B
Dilution Batch Prepared
Factor Number or Analyzed Analyst Lab
1 428709 04/20/18 18:33 JJH TAL CHI
Client Sample ID: TB
Date Collected: 04/10/18 00:00
Date Received: 04/14/18 12:55
Lab Sample ID: 500-143858-27
Matrix: Water
Batch Batch
Prep Type Type Method
Dilution
Run Factor
Batch
Number
Prepared
or Analyzed
Analyst Lab
Is
Total/NA Analysis 8260B
1
428709
04/20/18 19:02 JJH TAL CHI
Client Sample ID: TB
Date Collected: 04/10/18 00:00
Date Received: 04/14/18 12:55
Lab Sample ID: 500-143858-28
Matrix: Water
Batch Batch
Prep Type Type Method
Dilution
Run Factor
Batch
Number
Prepared
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
428709
04/20/18 19:30 JJH TAL CHI
Client Sample ID: TB
Date Collected: 04/10/18 00:00
Date Received: 04/14/18 12:55
Lab Sample ID: 500-143858-29
Matrix: Water
Batch Batch
Prep Type Type Method
Dilution
Run Factor
Batch
Number
Prepared
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
428709
04/20/18 19:59 JJH TAL CHI
Client Sample ID: MW11(1)
Date Collected: 04/12/18 12:50
Date Received: 04/18/18 09:10
Batch
Batch
Prep Type Type
Method
Total/NA Analysis
8260B
Total/NA Prep
3510C
Total/NA Analysis
8270D
Total/NA Prep
3510C
Total/NA Analysis
8081 B
Total/NA Prep
3510C
Total/NA Analysis
8082A
Lab Sample ID: 500-143858-30
Matrix: Water
Dilution
Run Factor
Batch
Number
Prepared
or Analyzed
Analyst
1
429099
04/24/1818:43
JJH
428463
04/18/1817:41
JP1
1
428757
04/20/1819:05
WDS
428495
04/19/18 07:40
NKG
1
428753
04/20/1814:06
WDS
428495
04/19/18 07:40
NKG
1
428582
04/19/1816:45
BJH
Lab
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
TAL CHI
Page 245 of 258
TestAmerica Chicago
7/5/2018

Lab Chronicle
Client: Civil & Environmental Consultants Inc
TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill
SDG: NCDEQ Solid Waste Facility = # 60-13
Client Sample ID: MW11(1)
Lab Sample ID: 500-143858-30
Date Collected: 04/12/18 12:50
Matrix: Water
Date Received: 04/18/18 09:10
Batch
Batch
Dilution
Batch
Prepared
Prep Type
Type
Method Run
Factor
Number
or Analyzed
Analyst
Lab
Total/NA
Prep
8151A
428351
04/18/18 11:15
NKG
TAL CHI
Total/NA
Analysis
8151A
1
428477
04/19/18 06:08
JBJ
TAL CHI
Total Recoverable
Prep
3005A
428456
04/18/18 16:50
BDE
TAL CHI
Total Recoverable
Analysis
6020B
1
428958
04/21/18 05:13
FXG
TAL CHI
Total/NA
Prep
7470A
428588
04/19/18 12:30
EEN
TAL CHI
Total/NA
Analysis
7470A
1
428749
04/20/18 10:05
EEN
TAL CHI
Total/NA
Prep
9010B
429175
04/24/18 14:10
MAN
TAL CHI
Total/NA
Analysis
9014
1
429363
MAN
TAL CHI
(Start) 04/25/18 09:58
(End) 04/25/18 09:59
Total/NA
Analysis
9056A
5
429826
04/27/18 22:58
EAT
TAL CHI
Total/NA
Analysis
9056A
20
429675
04/26/18 22:48
EAT
TAL CHI
Total/NA
Analysis
SM 2320B
1
429325
04/24/18 14:58
SMO
TAL CHI
Total/NA
Analysis
SM 2540C
1
428478
04/19/18 04:19
CLB
TAL CHI
Client Sample ID: MW11 D(i)
Lab Sample ID: 500-143858-31
Date Collected: 04/12/18 12:00
Matrix: Water
Date Received: 04/18/18 09:10
Batch
Batch
Dilution
Batch
Prepared
Prep Type
Type
Method Run
Factor
Number
or Analyzed
Analyst
Lab
Total/NA
Analysis
8260B
1
429099
04/24/18 19:08
JJH
TAL CHI
Total/NA
Prep
3510C
428463
04/18/18 17:41
JP1
TAL CHI
Total/NA
Analysis
8270D
1
428757
04/20/18 19:30
WDS
TAL CHI
Total/NA
Prep
3510C
428495
04/19/18 07:40
NKG
TAL CHI
Total/NA
Analysis
8081B
1
428753
04/20/18 14:25
WDS
TAL CHI
Total/NA
Prep
3510C
428495
04/19/18 07:40
NKG
TAL CHI
Total/NA
Analysis
8082A
1
428582
04/19/18 17:01
BJH
TAL CHI
Total/NA
Prep
8151A
428351
04/18/18 11:15
NKG
TAL CHI
Total/NA
Analysis
8151A
1
428477
04/19/18 06:32
JBJ
TAL CHI
Total Recoverable
Prep
3005A
428456
04/18/18 16:50
BDE
TAL CHI
Total Recoverable
Analysis
6020B
1
428958
04/21/18 05:17
FXG
TAL CHI
Total/NA
Prep
7470A
428588
04/19/18 12:30
EEN
TAL CHI
Total/NA
Analysis
7470A
1
428749
04/20/18 10:07
EEN
TAL CHI
Total/NA
Prep
9010B
429175
04/24/18 14:10
MAN
TAL CHI
Total/NA
Analysis
9014
1
429363
MAN
TAL CHI
(Start) 04/25/18 09:54
(End) 04/25/18 09:54
Total/NA
Analysis
9056A
2
429826
04/27/18 23:11
EAT
TAL CHI
Total/NA
Analysis
9056A
20
429675
04/26/18 23:00
EAT
TAL CHI
Total/NA
Analysis
SM 2320B
1
429325
04/24/18 14:48
SMO
TAL CHI
Total/NA
Analysis
SM 2540C
1
428478
04/19/18 04:22
CLB
TAL CHI
TestAmerica Chicago
Page 246 of 258 7/5/2018

Lab Chronicle
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
TestAmerica Chicago
Page 247 of 258 7/5/2018

Accreditation/Certification Summary C
Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143858-1
Project/Site: NC North Mecklenburg Landfill - Infill SDG: NCDEQ Solid Waste Facility = # 60-13
Laboratory: TestAmerica Chicago
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority
Program
EPA Region Identification Number Expiration Date
North Carolina (WW/SW)
State Program
4 291 12-31-18
The following analytes are included in this report, but
are not accredited/certified under this accreditation/certification:
Analysis Method
Prep Method
Matrix
Analyte
8270D
3510C
Water
Methyl parathion
8270D
3510C
Water
Phorate
The following analytes are included in this report, but
accreditation/certification is not offered by the governing authority:
Analysis Method
Prep Method
Matrix
Analyte
8260E
Water
trans- 1,4-Dichloro-2-butene
8270D
3510C
Water
2,3,7,8-TCDD (Screen)
TestAmerica Chicago
Page 248 of 258 7/5/2018

TestAmerica Chicago
2417 Bond Street
University Park, IL 60484
Phone [phone] Fax [phone]
Chain of Custody Record
TestAmedca
itfE r EADER IN F--VvSd.`ovr4ENrA!- T€ST NO
Sampler: .tL `
Lab PM:
Carder Tracking No(s):
COC No:
Client Information
l� l�jttylQf
Kintz, Robin M
[e-mail]
500-61781-29578.1
Client Contact:
Mr. Ed Stephens
Phone: 2
3
E-Mail:
Page:
Page 1 of & 3
Company:
Job c�
Civil &Environmental Consultants Inc
Analysis Requested
�J S
Address:
Due Date Requested:
Preservation odes:
1900 Center Park Drive Suite A
City:
-�
`•
_=-
--
A -HCL M- Hexane
S-NaOH N - None
TAT Requested (days):
Charlotte
'-_-
6,
ZnAc
C - Zn Acetate O - AsNa02
State, Zip:
D -Nitric Acid P - Na204S
NC, 28217lpt'�
_-_
�--f=
__ _
E - NaHSO4 Q - Na2SO3
F McOH
Phone:
PQ#:
-
-R-Na2S203
_ _
855-859-9932(Tel) 500-143858 COC
Purchase Order not required
--}-G--Amchlor
_
-_
c
----
S—H2Se4
H- Ascorbic Acid T- TSPDodecahydrate
WO #:
Email:
?
,o
- . _
I - Ice U - Acetone
[e-mail]
o Z
w
o'
>
o
E
;
O E
H
21
,,U
n _
y-,
.,°-
J - DI Water V - MCAA
K-EDTA W-pH4-5
L - EDA Z - other (specify)
Project Name:
Project #:
NC North Mecklenburg Landfill
50013286
;;
}✓
o
d
d
o
ago=
Other:
Site: � 1 _
SSOW#: 'a
`Els
P_
Sample
Matrix
N atA'
. _-
U
O
V
°
O
14
a`
Type
W-Water,
(—
E.
N
o
ao
>
d
d
'�
'�Y
?
Sample
(C=comp,
s=a°ra,
o=waetemn,
a -!ti
c
c
v
°�,-
m
o
-:
Sample Identification
Sample Date
Time
G=grab)
BT=Tlssue,A=A1r 5.
10Z
N
n
H
o
f'
Special Instructions/Note:
=- =
Preservation Code .= _
N'
A ,
N _
N
MW-1 \
-1 [ 1'
Water
r
Y
V
n
X
,(
MW-2 i
/ a
t ®10
Water
MW-3
►1
Water
MW-4 C�
yt'1
®
Water
==
MW-4DC%
I�L. <
Water
__
MW-5Li
11'-t(5
Water
MW-5D
tf 1l1
1 li 0
Water
MW-6�
i)
loW�
Water
MW-7 G1 J
yll 1
i D i 0
Water
_-
MW-7DCl
4111
930
Water
MW-8 C
L{ /18
1,'�'f 5-
Water
u
U
y
Possible Hazard Identification
Sample Disposal (A fee may be assessed if samples are retained longer than f month)
Non -Hazard 0 Flammable Q251Skin Irritant Poison 8 = Unknown Radiological
Return To Client Disposal By Lab Archive For Months
Deliverable Requested: I, II, III, IV, Other (specify)
Special Instructions/QC Requirements:
Empty Kit Relinquished by:
Date: Time:
Method of Shipm
Relin ui ed b
Cc
Daterri a
Compan
Receive
D to
Co pa
Relinquished by:
Daterrime: V
Company
Received by:
Date/Time: 1
C mpany
Relinquished by:
Daterrime:
Company
Received by:
Daterrime:
Company
Custody Seals Intact:
Custody Seal No.:
CooerTemp•�eerat refs °C and Other Re arks: y „
d,
A Yes 4 No
U r / ®rl! 7It
- I
Page 249 of 258
Itd+ 43 445 Ver: 004/2016
7/5/2018

TestAmerica Chicago
2417 Bond Street
University Park, IL 60484
Phone [phone] Fax [phone]
Chain of Custody Record
s A n
THE LFAt7£R M ENV!RON-10. -ITAt T£ STING
Sampler: _ r� C
Lab PM:
Carrier Tracking No(s):
COC No:
Client Information
Ii/-, ,/p t
Kintz, Robin M
500-61781-29578.2
Client
Phone: r� ey
E-Mail:
Page:
Mr. Ed Ste hens
d Stephens
y
0 0 ^ �� i G
1,.bian.:[e-mail]
@
2
Page 2 of ® tJ
Company:
Job #j,_
Civil &Environmental Consultants Inc
Analysis Requested
Address:
Due Date Requested:
_
Preservation Codes:
1900 Center Park Drive Suite A;
A - HCL M -Hexane
B - NaOH N -None
City:
TAT Requested (days):
Charlotte
t-_
_ _
-4-
- L_
C- ZnAcetate 0-AsNaO2
D -Nitric Acid P - Na204S
State, Zip:
NC,28217
_-
--�
E-NaHSO4 Q-Na2SO3
F - McOH R - Na2S203
c-ATnchlor s- Hzsoa
. Phone: — __ -
P_O_#:_.___. _. —_ _
•"-
855-859-9932 Tel
( )
Purchase Order not required
q
o-
?'_._;_�
H - Ascorbic Acid T - TSP Dodecahydrate
I - Ice U-Acetone
Email:
WO#:
[e-mail]
o
J- DIWater V -MCAA
'�+_
•-->
o
E
o
E
w
a
-y,
=.e
K- EDTA W- pH 4-5
L - EDA Z - other (specify)
Project Name:
Project #:
!-
9_
NC North Mecklenburg Landfill
50013286
d
mt
u
w
3
w
o
w
a
(
bo>
other:
Site:
SSOW#:
N°
=MS
Sample
Matrix'
Type
wa er,
�:
''4i
w
m
>
u
av
nJ
3-.
Z::
Sample
(C=comp,
a=solid,
o=—eteron,
-.0`
Sample Identification
Sample Date
Time
G=grab)
eT=Tlssae,A=Air
i
Via;:
H
.
.
.
.
H
s
Special Instructions/Note:
F -
reservation Code- -•
-
N-=A
NA-
-
-
MW-8DC�
7,13PJ
Water
MW-9�
,L4�®
Water
MW-9D
��t)frlo
11b
1530
Water
-_-
MW-10 Li
O
Water
MW-11 CL�
la o
Water
MW-11D6)
'�
�a
Water
�=
MW-12
1{d
Water
X
MW-12D Gt
i qo
Water
♦
Aw-i31.1
1L�1�
�/��
�t1
OboZ
Water
�1!
Oi/o�
Water
Y-
(r�
O Q CJ8
Water
=-
Possible Hazard Identification
Sample Disposal (A fee may be assessed if samples are retained longer than 1 month)
=1 Non -Hazard = Flammable Skin Irritant Poison B = Unknown Ell Radiological
1= Return To Client = Disposal By Lab Archive For Months
Deliverable Requested: I, II, 111, IV, Other (specify)
Special Instructions/QC Requirements:
Empty Kit Relinquished by:
Date:
Time:
Method of shipment:
Relinquis y:
Datei/(.f/y�ne•
I
Company
�.r
Received C
D t
.Co
r
Relinquished by:
Daferfime:
Company
Receive
N
(D/
#14-
Co p y
Relinquished by:
Daterl-ime:
Company
Receive by:
Company
Custody Seals Intact:
Custody Seal No.:
Cooler Temperature(s) aC and Other Remarks:
A Yes A No
Page 250 of 258
Ver:08/04/2016 7/5/2018

TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
2417 Bond Street, University Park, IL 60484
Phone: [phone] Fax: [phone]
(optional)
Report To
Contact: t� ti
Company: t!
Bill To
Contact:
Company:
Address:_
Addrass:
Phone:
Fax:
Dn}FL�da.onref!
Address: 0100 C� PDX t:- Pam(
v
Address: l�ll�dr if F7�#� . � Cif, M;.l ~i
%l
Phone: _U o-
Fax:
rr LL / �+
F-Mail• P-544M" A (iY F� iiA� . ♦�
(optional)
Chain of Custody Record
C
Lab Job #: 6 " 1e �K
Chain of Custody Number:
Page of
Temperature °C of Cooler:
Client 1 ^ Client Project # T
C 0 dinA 6ftd,-T0 CO r l �- 3 QQ r
Preservative
�
�
Preservative Key
1. HCL, Cool to 4°
Project Name
A' - — Aug-
��V e
- b w -
Parameter
, l
�/� V
l
yQ
IN
rLv
-
�0
®�
V _
��
_
2. HNO3, Cool to 4°
3. HNO3, Cool to 4°
4. NaOH, Cool to4°
- 5.-NaOH2n-00-ol to 4°
6. NaHSO4
7 Cool to 4°
8. None
9. Other
Project Location/State
Lab Project #
(73a/) &
` tis
Sampler
1
Lab M h�
td t1/L t �/:�
o
a
�
�
Sample ID
Sampling
E2
"
o o
�
i
�
�
Comments
Date
Time
ra
(ao
w
w-
11
tit
3
w-
f
o3a
5 w- 3
Lob
tdtt
r
cca
hup'lt
�iTTirn`bGrld Time Req ire usiness Days) Sample Disposal
_ 1 Day _ 2 Days _ 5 Days 7 Days _ 10 Days _ 15 Days Other t l Return to Client I l l Disposal by Lab n Archive for Mc�nH. fl Fyfel mR, be assessed if samples are retained longer than 1 month)
Requested Due Date ff f I !!! ___ I ` (i y p g
RelinqLphed @x Company Date Time
ReceiveZB 0,_ pa ay � a Time
AA, r3r, �i
Relinquished By Company Date Time
kil
LLi
eived Com any Dat Time
Relinquished By Company Date Time
ed By Company Date Time
Matrix Key
Client Comments
WW - Wastewater
SE - Sediment
W - Water
SO - Soil
S - Soil
L - Leachate
SL - Sludge
WI - Wipe
MS - Miscellaneous
DW - Drinking Water
OL - Oil
0 - Other
A - Air
Lab Comments:
4- -
Lab Courier
Hand Delivered

3RIGIN ID:JOTA [phone]
`IA'TT GINTHER CCEC)
3REENWAY WASTE OF NORTH MECK
nJAPfg1MAN
`\A74
15300 HOLBROOKS ROAD
HUNTERSVILLE, NC 28078
UNITED STATES US
57 of m
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TESTAMERICA LABS
2417BOND ST
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ORIGIN ID:JOTA [phone] SHIP J�ATE: OSAPRIB
MATT GINTHER CCEC) AC'rwW ,' 2500 LB MAN
GREENWAY WASTE OF NORTH MECK CAD 332SPCAF'E3J11
15300 HOLBROOKS ROAD
HUNTEf3VILLErNEC28078
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Page 252 of 258 1 7/5/2018

OR16IN ID:JOTA [phone]
MATT OINTHER (CEC)
ASTE OF NORTH MECK
I0 Q I.- I
a
SHIP C
ACTW(
CAD: -
15300 15300 AY W
HOLBROOKS ROAD
I
HUNTERSYILLE, NC 280751
STATES US ��._----_-------
I __. _
-UNITED
To SAMPLE LOGIN
TESTAMERICA LABS
s
2417 BOND ST
UNIVERSITY PARK IL 60484
(708) 534-- 5200
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SILLES U8 2007E J-_- -- ---
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24,17 BOND, ST
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Page 253 of 258 7/5/2018

ORIGIN ID:JOTA [phone]
MATT GINTHER (CEC)
GREENWAY WASTE OF NORTH MECK
15300 HOLBROOKS ROAD
HUNTERSVILLE, NC 28078
UNITED STATES US
TO SAMPLE LOGIN
TESTAMERICA LABS
2417 BOND ST
SHIP DATE: OSAPR1B
ACTWGT: 25.00 LB MAN
CAD: 33284/CAFE3111
UNIVERSITY PARK IL 60464
[phone]
REF; $500 — 61088
ORIGIIN� ID:JOTA (700) 534-•5200 SH
MATT GIFITNER (CEC) -
.GREENWAY WApSTE OF NORTH MECK ACTIr
1,5300 HOLMOOKS CA
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HUNTERSVILLE, NC 26078
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Page 254 of 258 7/5/2018

41
ORIGIN ID:JOTA [phone] ACTWGT: 25.00 LBiMAN
MATT GINTHER (CEC) CAD 332841CAFE3111
GREENWAY WASTE OF NORTH MECK
15300 HOLBROOKS ROAD
HUNTERSVIGLE, NC 28078 ORIGIN ID:JOTA (708) 534•-5200 SHIP DATE: 09APRIB
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TO SAMPLE LOGIN GREENWAY WASTE OF NORTH MECK CAD 33264ICAFE9111
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[phone]
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Page 255 of 258 7/5/2018

MATTIGIN7HERTACEC>OS)
534-5200
GREENWAY WASTE OF NORTH MECK
15300 HOLBROOKS ROAD �S
HUNTERSVILLE, NC 2$07B o
UNITED STATES US A
TU SAMPLE
TE5TAMERICA LABS
2417 BOND Si
t�
F1
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UNIVERSITY PARK IL 60484
[phone]
REF: 5688-B1888'
RMA:
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MATT GIN'I'HER (CEC) ACTWGT: 25.00 LB MAN
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15300 HOLBROOKS ROAD
rHUN'1'ERSVTLLE, NC 28070
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Page 256 of 258
7/5/2018

405971716650
Greenway Waste of North Meck
Matt Ginther (CEC)
15300.Holbrooks Road
°
H U NTERSVI LLE
NC, 28078 7085345200
T E STA M E R I CA LA
Sample Login
2417 BOND ST500-143858 Waybill
UNIVERSITY PARK, IL 60454
10:30a
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9717I6650 PRIORITY OVERNIGHT i
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M
Page 257 of 258 7/5/2018

Client: Civil & Environmental Consultants Inc
Login Number: 143858
List Number: 1
Creator: Scott, Sherri L
Question
Login Sample Receipt Checklist
Job Number: 500-143858-1
SDG Number: NCDEQ Solid Waste Facility = # 60-13
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
True
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
False
Cooler Temperature is recorded.
True
COC is present.
False
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
False
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
False
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
List Source: TestAmerica Chicago
3.3,2.3,3.3,2.5,0.9,0.6,1.5,1.4,1.8,2.8,9.E
TestAmerica Chicago
Page 258 of 258 7/5/2018

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
June 27, 2018
Donald Cobb
Civil & Environmental Consultants
1900 Center Park Drive
Charlotte, NC 28217
RE: Project: NORTH MECK- INFILL
Pace Project No.: 92389331
Dear Donald Cobb:
Enclosed are the analytical results for sample(s) received by the laboratory on June 21, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely, p
Taylor Ezell
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 16

acmnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: NORTH MECK- INFILL
Pace Project No.: 92389331
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Nevada Certification: FL NELAC Reciprocity
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FLO1264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 2 of 16

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
NORTH MECK- INFILL
92389331
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92389331001
MW-12 D(i)
EPA6010
SC1
1
PASI-O
EPA 6020
KPP
17
PASI-O
EPA7470
JMW1
1
PASI-A
92389331002
MW-13 (i)
EPA6010
SC1
1
PASI-O
EPA 6020
KPP
17
PASI-O
EPA7470
JMW1
1
PASI-A
92389331003
MW-14(i)
EPA6010
SC1
1
PASI-O
EPA 6020
KPP
17
PASI-O
EPA7470
JMW1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project:
Pace Project No.:
NORTH MECK- INFILL
92389331
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92389331001
MW-12 D(i)
EPA 6020
Barium
216
ug/L
1.0
06/27/18 12:44
EPA 6020
Chromium
1.7
ug/L
1.0
06/27/18 12:44
EPA 6020
Iron
631
ug/L
10.0
06/27/18 12:44
EPA 6020
Manganese
360
ug/L
1.0
06/27/18 12:44
EPA 6020
Nickel
7.2
ug/L
1.0
06/27/18 12:44
92389331002
MW-13 (i)
EPA 6020
Barium
43.8
ug/L
1.0
06/27/18 12:53
EPA 6020
Copper
1.8
ug/L
1.0
06/27/18 12:53
EPA 6020
Iron
612
ug/L
10.0
06/27/18 12:53
EPA 6020
Manganese
827
ug/L
2.0
06/27/18 15:30
EPA 6020
Nickel
4.4
ug/L
1.0
06/27/18 12:53
EPA 6020
Vanadium
1.2
ug/L
1.0
06/27/18 12:53
92389331003
MW-14 (1)
EPA 6020
Barium
24.3
ug/L
1.0
06/27/18 12:55
EPA 6020
Iron
309
ug/L
10.0
06/27/18 12:55
EPA 6020
Manganese
19.7
ug/L
1.0
06/27/18 12:55
EPA 6020
Vanadium
2.4
ug/L
1.0
06/27/18 12:55
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: NORTH MECK- INFILL
Pace Project No.: 92389331
Sample: MW-12 D(i) Lab ID: 92389331001 Collected: 06/19/18 12:15 Received: 06/21/18 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Tin
ND
ug/L
50.0
1
06/24/1815:23
06/27/1812:36
7440-31-5
6020 MET ICPMS
Analytical Method:
EPA 6020 Preparation Method:
EPA 3010
Antimony
ND
ug/L
1.0
1
06/24/1815:23
06/27/1812:44
7440-36-0
Arsenic
ND
ug/L
1.0
1
06/24/1815:23
06/27/1812:44
7440-38-2
Barium
216
ug/L
1.0
1
06/24/1815:23
06/27/1812:44
7440-39-3
Beryllium
ND
ug/L
0.10
1
06/24/1815:23
06/27/1812:44
7440-41-7
Cadmium
ND
ug/L
0.10
1
06/24/1815:23
06/27/1812:44
7440-43-9
Chromium
1.7
ug/L
1.0
1
06/24/1815:23
06/27/1812:44
7440-47-3
Cobalt
ND
ug/L
4.0
1
06/24/1815:23
06/27/1812:44
7440-48-4
Copper
ND
ug/L
1.0
1
06/24/1815:23
06/27/1812:44
7440-50-8
Iron
631
ug/L
10.0
1
06/24/1815:23
06/27/1812:44
7439-89-6
Lead
ND
ug/L
1.0
1
06/24/1815:23
06/27/1812:44
7439-92-1
Manganese
360
ug/L
1.0
1
06/24/1815:23
06/27/1812:44
7439-96-5
Nickel
7.2
ug/L
1.0
1
06/24/1815:23
06/27/1812:44
7440-02-0
Selenium
ND
ug/L
1.0
1
06/24/1815:23
06/27/1812:44
7782-49-2
Silver
ND
ug/L
0.10
1
06/24/1815:23
06/27/1812:44
7440-22-4
Thallium
ND
ug/L
2.0
1
06/24/1815:23
06/27/1812:44
7440-28-0
Vanadium
ND
ug/L
1.0
1
06/24/1815:23
06/27/1812:44
7440-62-2
Zinc
ND
ug/L
5.0
1
06/24/1815:23
06/27/1812:44
7440-66-6
7470 Mercury
Analytical Method:
EPA 7470 Preparation Method:
EPA 7470
Mercury
ND
ug/L
0.20
1
06/22/1814:30
06/25/1817:24
7439-97-6 M1
REPORT OF LABORATORY ANALYSIS
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Date: 06/27/2018 04:52 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 16

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: NORTH MECK- INFILL
Pace Project No.: 92389331
Sample: MW-13 (i) Lab ID: 92389331002 Collected: 06/21/18 11:25 Received: 06/21/18 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Tin
ND
ug/L
50.0
1
06/24/1815:23
06/27/1812:47
7440-31-5
6020 MET ICPMS
Analytical Method:
EPA 6020 Preparation Method:
EPA 3010
Antimony
ND
ug/L
1.0
1
06/24/1815:23
06/27/1812:53
7440-36-0
Arsenic
ND
ug/L
1.0
1
06/24/1815:23
06/27/1812:53
7440-38-2
Barium
43.8
ug/L
1.0
1
06/24/1815:23
06/27/1812:53
7440-39-3
Beryllium
ND
ug/L
0.10
1
06/24/1815:23
06/27/1812:53
7440-41-7
Cadmium
ND
ug/L
0.10
1
06/24/1815:23
06/27/1812:53
7440-43-9
Chromium
ND
ug/L
1.0
1
06/24/1815:23
06/27/1812:53
7440-47-3
Cobalt
ND
ug/L
4.0
1
06/24/1815:23
06/27/1812:53
7440-48-4
Copper
1.8
ug/L
1.0
1
06/24/1815:23
06/27/1812:53
7440-50-8
Iron
612
ug/L
10.0
1
06/24/1815:23
06/27/1812:53
7439-89-6
Lead
ND
ug/L
1.0
1
06/24/1815:23
06/27/1812:53
7439-92-1
Manganese
827
ug/L
2.0
2
06/24/1815:23
06/27/1815:30
7439-96-5
Nickel
4.4
ug/L
1.0
1
06/24/1815:23
06/27/1812:53
7440-02-0
Selenium
ND
ug/L
1.0
1
06/24/1815:23
06/27/1812:53
7782-49-2
Silver
ND
ug/L
0.10
1
06/24/1815:23
06/27/1812:53
7440-22-4
Thallium
ND
ug/L
2.0
1
06/24/1815:23
06/27/1812:53
7440-28-0
Vanadium
1.2
ug/L
1.0
1
06/24/1815:23
06/27/1812:53
7440-62-2
Zinc
ND
ug/L
5.0
1
06/24/1815:23
06/27/1812:53
7440-66-6
7470 Mercury
Analytical Method:
EPA 7470 Preparation Method:
EPA 7470
Mercury
ND
ug/L
0.20
1
06/22/1814:30
06/25/1817:32
7439-97-6
REPORT OF LABORATORY ANALYSIS
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Date: 06/27/2018 04:52 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 16

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: NORTH MECK- INFILL
Pace Project No.: 92389331
Sample: MW-14 (i) Lab ID: 92389331003 Collected: 06/19/18 11:38 Received: 06/21/18 12:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Tin
ND
ug/L
50.0
1
06/24/1815:23
06/27/1812:50
7440-31-5
6020 MET ICPMS
Analytical Method:
EPA 6020 Preparation Method:
EPA 3010
Antimony
ND
ug/L
1.0
1
06/24/1815:23
06/27/1812:55
7440-36-0
Arsenic
ND
ug/L
1.0
1
06/24/1815:23
06/27/1812:55
7440-38-2
Barium
24.3
ug/L
1.0
1
06/24/1815:23
06/27/1812:55
7440-39-3
Beryllium
ND
ug/L
0.10
1
06/24/1815:23
06/27/1812:55
7440-41-7
Cadmium
ND
ug/L
0.10
1
06/24/1815:23
06/27/1812:55
7440-43-9
Chromium
ND
ug/L
1.0
1
06/24/1815:23
06/27/1812:55
7440-47-3
Cobalt
ND
ug/L
4.0
1
06/24/1815:23
06/27/1812:55
7440-48-4
Copper
ND
ug/L
1.0
1
06/24/1815:23
06/27/1812:55
7440-50-8
Iron
309
ug/L
10.0
1
06/24/1815:23
06/27/1812:55
7439-89-6
Lead
ND
ug/L
1.0
1
06/24/1815:23
06/27/1812:55
7439-92-1
Manganese
19.7
ug/L
1.0
1
06/24/1815:23
06/27/1812:55
7439-96-5
Nickel
ND
ug/L
1.0
1
06/24/1815:23
06/27/1812:55
7440-02-0
Selenium
ND
ug/L
1.0
1
06/24/1815:23
06/27/1812:55
7782-49-2
Silver
ND
ug/L
0.10
1
06/24/1815:23
06/27/1812:55
7440-22-4
Thallium
ND
ug/L
2.0
1
06/24/1815:23
06/27/1812:55
7440-28-0
Vanadium
2.4
ug/L
1.0
1
06/24/1815:23
06/27/1812:55
7440-62-2
Zinc
ND
ug/L
5.0
1
06/24/1815:23
06/27/1812:55
7440-66-6
7470 Mercury
Analytical Method:
EPA 7470 Preparation Method:
EPA 7470
Mercury
ND
ug/L
0.20
1
06/22/1814:30
06/25/1817:34
7439-97-6
REPORT OF LABORATORY ANALYSIS
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Date: 06/27/2018 04:52 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 16

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: NORTH MECK- INFILL
Pace Project No.: 92389331
QC Batch: 416320
Analysis Method: EPA 7470
QC Batch Method: EPA 7470
Analysis Description: 7470 Mercury
Associated Lab Samples: 92389331001, 92389331002,
92389331003
METHOD BLANK: 2308557
Matrix: Water
Associated Lab Samples: 92389331001, 92389331002,
92389331003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Mercury ug/L
ND 0.20
06/25/1817:20
LABORATORY CONTROL SAMPLE: 2308558
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Mercury ug/L
2.5 2.2
90 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2308559 2308560
MS MSD
92389331001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Mercury ug/L ND
2.5 2.5 1.8
1.7 70 69 75-125 2 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/27/2018 04:52 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 16

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: NORTH MECK- INFILL
Pace Project No.: 92389331
QC Batch: 456864
Analysis Method: EPA 6010
QC Batch Method: EPA 3010
Analysis Description: 6010 MET
Associated Lab Samples: 92389331001, 92389331002,
92389331003
METHOD BLANK: 2473547
Matrix: Water
Associated Lab Samples: 92389331001, 92389331002,
92389331003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Tin ug/L
ND 50.0
06/26/1813:40
LABORATORY CONTROL SAMPLE: 2473548
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Tin ug/L
1250 1280
102 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2473549 2473550
MS MSD
35399097001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Tin ug/L <25.0
1250 1250 1280
1230 102 98 75-125 4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/27/2018 04:52 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 16

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: NORTH MECK- INFILL
Pace Project No.: 92389331
QC Batch: 456865 Analysis Method: EPA 6020
QC Batch Method: EPA 3010 Analysis Description: 6020 MET
Associated Lab Samples: 92389331001, 92389331002, 92389331003
METHOD BLANK: 2473551 Matrix:
Associated Lab Samples: 92389331001, 92389331002, 92389331003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed Qualifiers
Antimony
ug/L
ND
1.0
06/27/1812:19
Arsenic
ug/L
ND
1.0
06/27/1812:19
Barium
ug/L
ND
1.0
06/27/1812:19
Beryllium
ug/L
ND
0.10
06/27/1812:19
Cadmium
ug/L
ND
0.10
06/27/1812:19
Chromium
ug/L
ND
1.0
06/27/1812:19
Cobalt
ug/L
ND
4.0
06/27/1812:19
Copper
ug/L
ND
1.0
06/27/1812:19
Iron
ug/L
ND
10.0
06/27/1812:19
Lead
ug/L
ND
1.0
06/27/1812:19
Manganese
ug/L
ND
1.0
06/27/1812:19
Nickel
ug/L
ND
1.0
06/27/1812:19
Selenium
ug/L
ND
1.0
06/27/1812:19
Silver
ug/L
ND
0.10
06/27/1812:19
Thallium
ug/L
ND
2.0
06/27/1812:19
Vanadium
ug/L
ND
1.0
06/27/1812:19
Zinc
ug/L
ND
5.0
06/27/1812:19
LABORATORY CONTROL SAMPLE:
Parameter
2473552
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
50
47.6
95
80-120
Arsenic
ug/L
50
46.8
94
80-120
Barium
ug/L
50
46.6
93
80-120
Beryllium
ug/L
5
4.9
97
80-120
Cadmium
ug/L
5
4.9
97
80-120
Chromium
ug/L
50
48.1
96
80-120
Cobalt
ug/L
50
48.7
97
80-120
Copper
ug/L
50
48.6
97
80-120
Iron
ug/L
500
492
98
80-120
Lead
ug/L
50
50.2
100
80-120
Manganese
ug/L
50
47.0
94
80-120
Nickel
ug/L
50
48.4
97
80-120
Selenium
ug/L
50
48.3
97
80-120
Silver
ug/L
5
4.9
98
80-120
Thallium
ug/L
50
49.4
99
80-120
Vanadium
ug/L
50
47.3
95
80-120
Zinc
ug/L
250
245
98
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/27/2018 04:52 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 16

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
NORTH MECK- INFILL
92389331
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
2473553
2473554
MS
MSD
35399097002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
<0.50
50
50
48.0
48.7
96
97
75-125
1
Arsenic
ug/L
<0.50
50
50
48.2
49.2
96
98
75-125
2
Barium
ug/L
11.5
50
50
58.1
58.9
93
95
75-125
1
Beryllium
ug/L
<0.050
5
5
6.4
6.3
127
125
75-125
1 M1
Cadmium
ug/L
<0.050
5
5
4.9
5.0
97
100
75-125
3
Chromium
ug/L
1.2
50
50
50.5
51.1
98
100
75-125
1
Cobalt
ug/L
<0.50
50
50
49.6
50.1
99
100
75-125
1
Copper
ug/L
<0.93
50
50
49.5
49.8
97
98
75-125
1
Iron
ug/L
<6.9
500
500
507
510
101
101
75-125
0
Lead
ug/L
<0.50
50
50
49.5
50.5
99
101
75-125
2
Manganese
ug/L
7.3
50
50
55.1
55.9
96
97
75-125
1
Nickel
ug/L
<0.62
50
50
49.4
49.0
99
98
75-125
1
Selenium
ug/L
<0.50
50
50
24.3
22.3
48
44
75-125
8 M1
Silver
ug/L
<0.050
5
5
4.9
5.0
98
99
75-125
2
Thallium
ug/L
<0.50
50
50
49.4
50.5
99
101
75-125
2
Vanadium
ug/L
0.63J
50
50
49.9
50.6
99
100
75-125
1
Zinc
ug/L
<2.5
250
250
241
245
96
98
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/27/2018 04:52 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 16

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: NORTH MECK- INFILL
Pace Project No.: 92389331
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-O Pace Analytical Services - Ormond Beach
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/27/2018 04:52 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 16

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
NORTH MECK- INFILL
92389331
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92389331001
MW-12 D(i)
EPA 3010
456864
EPA 6010
456877
92389331002
MW-13 (i)
EPA 3010
456864
EPA 6010
456877
92389331003
MW-14 (i)
EPA 3010
456864
EPA 6010
456877
92389331001
MW-12 D(i)
EPA 3010
456865
EPA 6020
456878
92389331002
MW-13 (i)
EPA 3010
456865
EPA 6020
456878
92389331003
MW-14 (1)
EPA 3010
456865
EPA 6020
456878
92389331001
MW-12 D(i)
EPA 7470
416320
EPA 7470
416348
92389331002
MW-13 (i)
EPA 7470
416320
EPA 7470
416348
92389331003
MW-14 (i)
EPA 7470
416320
EPA 7470
416348
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/27/2018 04:52 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 16

Document Name:
Sample Condition Upon Rec
Document No.:
F-CAR-CS-033•Rev,(
Document Revised, February 7, 2018
Page 1 of 2
Issuing Authority'
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville Raleigh[] Mechanicsville[]
Sample Condition Client Name:Upon Receipt n Project $1 WO# : 92389331
Illl� r
Courier; []Fed Ex ❑UPS CUSPS ❑Client
❑ Commercial (;>ce []Other: 92389331
Custody Seal Present? ❑lyes Alb Seals Intact? ❑Yes 00
Oate/Initials Person Examinln]3.(gptenrs:"—t--T1
-
Packing Material: ❑Bubble Wrap ❑Bubble Bags 9f4one ❑ Other Blo oglcaI Tissue Frozen?
1 ❑Yes�A1D N/A
Thermomet r: Type of Ice: �V4fet ❑Blue ❑None
IR Gun ID: 92TO40 Yp
Cooler Temp (°C): - Correction Factor: Add/Subtract (°C) +0.4 Temp should he above freezing to VC
Cooler Temp Corrected (°tj:— ❑Samples out of temp criteria. Samples on Ice, cooling process
has begun
USDA Regulated Soll �D N/A, water sample}
Did samples originate in a quarantine zone within the United States: CA, NY, or 5C (check maps)? D1d samples originate from a Foreign source (Internationally,
pale including Hawaii and Puerto Rlcol? QYes E3NO
Chain of Custody Present?
Samples Arrived within Hold Time?
Short Hold Time Analysis (c72 hr.)?
Rush Turn Around Time Requested?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis: Samples Field Filtered?
Sample Labels Match CC1C?
-Includes Dater ime/ID/Analysis M
Headsp ace in VOA Vials (>S-6mm]?
Trip Blank Present?
Trip Blank Custody Seals Present?
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
]Na ❑N/A
2.
i
p
[]N/A
I
r41p
❑ N/A
4.
[:]No
❑N/A
5.
❑No
❑N/A
G.
s [:]No ❑N/A
7,
[]yes
[]No
/A
B.
\ ❑Yes
[:]No
❑N/A
9.
Yes
Date/Time:
Project Manager SCURF Review: i" r
Project Manager SRF Review:
Field Data Required? ❑Yes ❑N❑
Lot 10 of split containers:
Date: (o 72)1 Y
Date: (D 1 ZZ i
Page 14 of 16

Document Name:
Document Revised: February 7, 2018
aceAnalytical1
Sample Condition Upon Recelpt(5CUR)
Page 1 of 2
Document No.;
Issuing Authority;
F•CAR-CS•033-Rev.05
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechiorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Colifarm, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project W0# ; 92389331
PM: PTE Due Date: 06/28/18
CLIENT: 92—CEC
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot N
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form wtil be sent to the North Carolina DEHNR Certification Office 0.e.
out of hold, Incorrect preservative, out cf temp, Incorrect containers.
Page 15 of 16

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16 of 16