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HomeMy WebLinkAbout1304_Cabarrus_CMSV_MSWLF_GW_FID1279938_20181001ENR USE ONLY: ❑Pa er Report ❑Electronic Data - Email CD data loaded. Yes / No Doc/Event #: NC DENR I Environmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: • Prepare one form for each individually monitored unit. • Please type or print legibly. • Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). • Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. • Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). • Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): Jett Environmental Consulting, PLLC Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: STEVE JETT E-mail: STEVE.JETT(QJETTENVIRO.COM Phone: (314) 496-4654 NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address: Facility Permit # (.0500 or. 1600) October 20-24, 2006) .1600 BFI Waste Systems of North 5105 Morehead Road, America, Inc. -Charlotte Motor 13-04 Speedway, Landfill V Concord, NC 28027 ctober 1, 2, 3, 10, 11, 2018 Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring ❑ Detection Monitoring [X] Assessment Monitoring ❑ Corrective Action of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells Groundwater monitoring data from private water supply wells Leachate monitoring data Surface water monitoring data ❑ Methane gas monitoring data Corrective action data (specify) Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Steve Jett _ Owner (314) 496-4654 Facility Represen#tive*me (Prin Signature Title zl S/i9 Date Jett Environmental Consulting, PLLC, 10 Quiet Brook Court, St. Charles, Missouri 63303 Facility Representative Address NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 (Area Code) Telephone Number Affix NC Licensed/ P bonal Geologist Seal o 4 z • Groundwater Statistical Analysis Report Second Semi -Annual 2018 Sampling Event Charlotte Motor Speedway, Landfill V Concord, North Carolina Permit No. 13-04 February 2019 Prepared by: 0 JETT LNVIKUNIVIr-ir it - is C O N S U LT I N G 1002 Morgan Meadow Drive 314-496-4654 Wentzville, MO 63385 www.jettenviro.com TABLE OF CONTENTS 1.0 INTRODUCTION.............................................................................1 2.0 SITE BACKGROUND AND MONITORING NETWORK................1 3.0 SITE HYDROGEOLOGY................................................................1 4.0 DATA EVALUATION......................................................................2 5.0 STATISTICAL PROCEDURES.......................................................2 5.1 Inter -Well Prediction Intervals....................................................2 5.2 Intra-Well Confidence Intervals..................................................3 5.3 Statistical Results Summary.......................................................4 6.0 ASSESSMENT MONITORING STATUS........................................4 7.0 WATER QUALITY ASSESSMENT ACTIVITIES ............................7 Table 1 Wells Analyzed Table 2 Organic Detections Table 3A Comparisons to GWPSs (Inorganics) Table 313 Comparisons to GWPSs (Organics) Table 4 Surface Water Data Compared to NC 213 Standards Table 5 Inter -Well Prediction Limit Exceedances Table 6 Water Quality Assessment Well Data Compared to GWPSs APPENDICES Appendix A Potentiometric Surface Map Appendix B Statistical Evaluations Appendix C Laboratory Analytical Reports & Field Information Forms Groundwater Statistical Analysis Report Charlotte Motor Speedway, Landfill V, North Carolina 1 1.0 INTRODUCTION On behalf of BFI Waste Systems of North America, Inc. -Charlotte Motor Speedway, Landfill V, Jett Environmental Consulting statistically evaluated the Second Semi -Annual 2018 water quality monitoring data. Groundwater, surface water, and leachate sampling was completed by Pace Analytical Services, LLC (Pace) on October 10, 2018 and analytical testing was performed by Pace. The statistical analysis software package utilized, Sanitasll' follows a documented decision logic that incorporates the following guidance document: USEPA "Statistical Analysis of Groundwater Monitoring Data at RCRA Facilities, Unified Guidance" (March 2009). 2.0 SITE BACKGROUND AND MONITORING NETWORK Jett Environmental Consulting statistically evaluated parameters from the Second Semi -Annual 2018 event against background data using inter -well prediction interval analysis. Prediction intervals are considered a powerful tool for groundwater statistical analysis, when feasible, due to their inherent low false negative and false positive rates utilizing confirmatory resampling, if necessary. Statistical comparisons of data to the Groundwater Protection Standards (GWPSs) were performed utilizing intra-well confidence limits. Background for the inter -well prediction limits was defined as all samples taken from each upgradient well. The parameters subject to statistical evaluation during detection monitoring are noted in NCDEQ Section .1633 as constituents listed in Appendix I of 40 CFR Part 258 "Constituents for Detection Monitoring". Due to previous detections, the Appendix II constituent mercury is also sampled semi-annually at each well along with the Appendix I constituents. In addition, in a May 29, 2018 memorandum, NCDEQ requested groundwater and surface water samples collected at landfills after July 1, 2018 be analyzed for 1,4-dioxane. Table 1 lists the groundwater monitoring wells for the site. Each of the wells was sampled during the Second Semi -Annual 2018 event. In correspondence dated October 13, 2015 (DIN 25121), NCDEQ approved a request to sample MW-17, MW-17A, and MW-24 annually. Wells MW-17, MW-17A, and MW-24 were sampled during the first semi- annual 2018 event. The next scheduled annual sampling event for wells MW-17, MW-17A, and MW-24 is during the First Semi -Annual 2019 event. In addition to groundwater monitoring, the site has a surface water monitoring network consisting of one upstream surface water sampling point (SW-1) and one downstream point (SW-2). These points are sampled semi-annually for the 40 CFR Part 258 Appendix I list in conjunction with the groundwater monitoring wells. Both surface water monitoring points were sampled during the Second Semi -Annual 2018 event. A leachate sample is also routinely collected for analysis in accordance with the facility's permit. The leachate sample was analyzed for the 40 CFR Part 258 Appendix I list, biochemical oxygen demand, chemical oxygen demand, nitrate as N, phosphorous, and sulfate. 3.0 SITE HYDROGEOLOGY Previous site investigations indicate that groundwater is present in either the saprolite, Piedmont weathered rock, or bedrock depending on location. Data suggests hydraulic connection between these units, which form the uppermost aquifer. Generally, data indicate that the groundwater flow is principally within the saprolite and Piedmont weathered rock, in the direction of the Rocky River. Locally, the vertical component of the groundwater flow may be slightly downward in topographic high areas and slightly upward in topographic low areas. In general, the configuration of the groundwater surface is similar to the topography of the site. Appendix A provides a potentiometric surface map for the site utilizing groundwater level data from the Second Semi -Annual 2018 event. Groundwater flow direction for the Second Semi -Annual 2018 event was Groundwater Statistical Analysis Report Charlotte Motor Speedway, Landfill V, North Carolina 2 to the southwest, consistent with past events. Groundwater flow rate for the Second Semi -Annual 2018 event was estimated to range from 22 feet/year to 135 feet/year, consistent with past events. Flow rate calculations are available in Appendix A. A well construction summary table is provided in Appendix A. 4.0 DATA EVALUATION The analytical results for the Second Semi -Annual 2018 event for the groundwater samples are summarized on Tables 2, 3A, and 3B. Table 2 provides a summary of volatile organic compounds (VOCs) detected at or above a laboratory practical quantitation limit (PQL) in groundwater samples. Of the thirty quantifiable VOC detections, nineteen were above a NC 2L Groundwater Standard (NC 2L): 1,4- dichlorobenzene at MW-25; benzene at MW-18A, MW-32R, MW-33, MW-34; and vinyl chloride at MW- 18A, MW-32R, MW-33, and MW-34. The detected VOCs are consistent with past events. The Second Semi -Annual 2018 event sampling results also exhibited detections of 1,4-dioxane at MW-1A, MW-1 B, MW-2A, MW-18A, MW-19, MW-19A, MW-20B, MW-22, MW-22A. As noted previously, the Second Semi -Annual 2018 event was the first event for 1,4-dioxane to be sampled at the site. As shown on Table 3A, four Appendix I inorganic constituents (barium at MW-20B; cobalt at MW-213, MW- 21, MW-22, MW-22A, and MW-32R; nickel at MW-21 and MW-22A; and vanadium at MW-21) were detected above a PQL and a Groundwater Protection Standard (GWPS) during the Second Semi -Annual 2018 sampling event. Results are generally consistent with past events. As shown on Table 4, during the Second Semi -Annual 2018 event, no NC 2B Surface Water Standards were exceeded in surface water samples. No VOCs were detected in surface water samples at quantified concentrations above their respective PQLs during the Second Semi -Annual 2018 event. The constituents detected in the leachate sample collected during the Second Semi -Annual 2018 event are typical for leachate at this facility. Appendix C contains a copy of the groundwater, surface water, and leachate laboratory analytical reports and field information forms for the Second Semi -Annual 2018 event. 5.0 STATISTICAL PROCEDURES The SanitaSTM program was utilized to compile and statistically evaluate the data for the Second Semi - Annual 2018 sampling event. Summary tables for the inter -well prediction interval analysis are available in Appendix B. Statistical analyses (i.e. inter -well prediction limits) were performed to establish background concentrations and determine if the NC GWPS/NC 2L value -to -value exceedances for barium at MW-2013; cobalt at MW-213, MW-21, MW-22, MW-22A, and MW-32R; nickel at MW-21 and MW-22A; and vanadium at MW-21 exhibited statistically significant increases above background. 5.1 Inter -Well Prediction Intervals The prediction interval is a statistical method used to compare a single observation to a group of observations. The prediction interval is calculated to include observations from the same population with a specified confidence. In groundwater monitoring, a prediction interval approach may be used to make comparisons between background and compliance data. The interval is developed to contain all future observations, within a certain probability. For the Charlotte Motor Speedway V site, inter -well prediction intervals have been developed based on a 99% confidence that future observations will fall within the range. If any future observation exceeds the prediction interval, this is considered statistically significant evidence that the observation is not representative of the background group. During parametric prediction interval analysis, the mean and the standard deviation are calculated for the raw or transformed background data. The number of comparison observations, K, is defined to be included in the interval. If less than 15% of the background observations are nondetects, the nondetects are replaced Groundwater Statistical Analysis Report Charlotte Motor Speedway, Landfill V, North Carolina 3 with one half of the reporting limit prior to performing the analysis. If more than 15% but less than 50% of the background data are below the reporting limit, the data's sample mean and standard deviation are adjusted according to the Kaplan -Meier method. However, when the background data are not transformed - normal or contain greater than 50% observations below the reporting limit, SanitasT" automatically constructs a nonparametric prediction interval. During nonparametric analysis, the highest value from the background data is used to set the upper limit of the prediction interval. For the Second Semi -Annual 2018 event, barium at MW-20B; cobalt at MW-2B, MW-21, MW-22, MW-22A, and MW-32R; nickel at MW-21 and MW-22A; and vanadium at MW-21 statistically exceeded background and were above NC GWPS/NC 2L standards in a value -to -value comparison. Table 5 provides a summary of the prediction limit exceedances. The prediction limit exceedances are generally consistent with past events. Included in Appendix B are time series plots for each of the inorganic parameters statistically analyzed for this reporting period and plots of the Second Semi -Annual 2018 organic detections at or above PQLs. 5.2 Intra-Well Confidence Intervals Per NCDEQ Regulation .1634(H), Groundwater Protection Standards (GWPSs) are equal to the National Primary Drinking Water Standard -Maximum Contaminant Level (MCL) or North Carolina 15A NCAC 2L Water Quality Standard, whichever is lower. Tables 3A and 3B provide comparisons of the Second Semi -Annual 2018 results to the GWPSs. In order to determine if the groundwater concentrations exhibit a statistical exceedance of the GWPS, a statistical comparison was made to the GWPSs. The following text outlines the procedures that were used to statistically compare concentrations to GWPSs. Per the U.S. Environmental Protection Agency document (dated March 2009), titled Statistical Analysis of Groundwater Monitoring Data at RCRA Facilities, Unified Guidance, a Confidence Interval is constructed from sample data and is designed to contain the mean concentration of a well analyte in groundwater monitoring, with a designated level of confidence. A confidence interval generally is used when samples are being compared to a GWPS, which is typically the MCL or alternate concentration limit (i.e. 2L Standard or NC GWPS). A lower confidence interval analysis was used to statistically compare to GWPSs. The method constructs a normal confidence interval on the mean concentration of a constituent incorporating, at a minimum, the four most recent measurements. The lower confidence interval on the mean was compared to the GWPS to determine whether the mean concentration exceeded its GWPS. If the lower confidence interval on the mean exceeds the GWPS then there is statistically significant evidence that the mean concentration of that constituent exceeds the GWPS. The distribution of the data is evaluated by applying the Shapiro -Wilk or Shapiro-Francia test for normality to the raw data or, when applicable, transformed data. If less than 15 percent of the observations are non - detects, the non -detects will be replaced with one half the reporting limit prior to performing the normality test and constructing the confidence limit. Per .1634(g)(5), if background (statistical limit based on upgradient well data) is higher than the NC 2L Standard, then background may be utilized as the GWPS. Background for organics is considered the non - detect level (equivalent to the PQL). The following is a summary of background data that was utilized as the GWPS: ➢ The PQL (1.0 ug/L) for 1,2-dichloroethane, tetrachloroethene, and vinyl chloride is higher than the 2L Standard (0.4 ug/L, 0.7 ug/L, and 0.03 ug/L, respectively); therefore, the PQL (1.0 ug/L) was utilized as the GWPS for 1,2-dichloroethane, tetrachloroethene, and vinyl chloride. Groundwater Statistical Analysis Report Charlotte Motor Speedway, Landfill V, North Carolina 4 ➢ Background for total antimony (6 ug/L) is higher than the NC 2L Standard (1 ug/L), therefore 6 ug/L was utilized as the GWPS as outlined in .1634(g)(5). ➢ Background for total chromium (98 ug/L) is higher than the NC 2L Standard (10 ug/L), therefore 98 ug/L was utilized as the GWPS as outlined in .1634(g)(5). ➢ Background for total cobalt (12 ug/L) is higher than the NC 2L Standard (1 ug/L), therefore 12 ug/L was utilized as the GWPS as outlined in .1634(g)(5). ➢ Background for total thallium (5.5 ug/L) is higher than the NC 2L Standard (0.28 ug/L), therefore 5.5 ug/L was utilized as the GWPS as outlined in .1634(g)(5). ➢ Background for total vanadium (33 ug/L) is higher than the NC 2L Standard (0.3 ug/L), therefore 33 ug/L was utilized as the GWPS as outlined in .1634(g)(5). Inorganic and organic concentrations detected above PQLs and GWPSs (See Tables 3A and 3113) were statistically compared to their respective GWPSs utilizing intra-well confidence limits. As provided in Appendix B, one inorganic statistically exceeded a GWPS for the Second Semi -Annual 2018 event: cobalt at MW-22 and MW-22A. Three VOCs statistically exceeded a GWPS for the Second Semi -Annual 2018 event: 1,4-dichlorobenzene at MW-25; benzene at MW-32R and MW-34; and vinyl chloride at MW-32R, MW-33, and MW-34. Wells MW-25, MW-32R, MW-33, and MW-34 are already in the Assessment Monitoring Program. 5.3 Statistical Results Summary Assessment Monitoring Inorganic and organic concentrations detected above PQLs and GWPSs were statistically compared to their respective GWPSs utilizing intra-well confidence limits. One inorganic statistically exceeded a GWPS for the Second Semi -Annual 2018 event: cobalt at MW-22 and MW-22A. Three VOCs statistically exceeded a GWPS for the Second Semi -Annual 2018 event: 1,4-dichlorobenzene at MW-25; benzene at MW-32R and MW-34; and vinyl chloride at MW-32R, MW-33, and MW-34. 6.0 ASSESSMENT MONITORING STATUS In accordance with Assessment Monitoring requirements set forth in the NCDEQ Regulations for Municipal Solid Waste Landfills Section .1634: (e) If the concentrations of all Appendix II constituents are shown to be at or below the approved ground- water protection standards, for two consecutive sampling events, the owner or operator shall report this information to the Division, and the Division shall give approval to the owner or operator to return to detection monitoring. (f) If one or more Appendix II constituents are detected above the approved ground -water protection standards in any sampling event, the owner or operator, shall within 14 days of this finding, submit a report to the Division, place a notice in the operating record, and notify local government officials. The owner or operator: (1) shall: (A) Characterize the nature and extent of the release by installing additional monitoring wells, as necessary; (B) Install at least one additional monitoring well at the facility boundary in the direction of contaminant migration and sample this well in accordance with Paragraph (d)(2) of this Rule; (C) Notify all persons who own land or reside on land that directly overlies any part of the plume of contamination if contaminants have migrated off -site; and (D) Within 90 days, initiate an assessment of corrective measures as required under Rule .1635 of this Section; or (2) may demonstrate that a source other than a MSWLF unit caused the exceedance of the ground -water protection standards, or the exceedance resulted from error in sampling, analysis, or natural variation in ground -water quality. A report documenting this demonstration shall be approved by the Division. If required by G. S. 89C or G. S. 89E, a professional engineer or licensed geologist shall prepare these documents. (Note: The North Carolina Board of Examiners for Engineers and Surveyors and the Board of Licensing of Groundwater Statistical Analysis Report Charlotte Motor Speedway, Landfill V, North Carolina 5 Geologist has determined, via letters dated July 16, 2010 and November 30, 2010 respectively, that preparation of documents pursuant to this Paragraph constitutes practicing engineering or geology under G.S. 89C and G.S. 89E.] A copy of the approved report shall also be placed in the operating record. If a successful demonstration is made, the owner or operator may discontinue assessment monitoring, and may return to detection monitoring when approval is given by the Division. Until a successful demonstration is made, the owner or operator shall comply with Paragraph (0(1) of this Rule including initiating an assessment of corrective measures. During the Second Semi -Annual 2018 event, no Appendix II constituents (not also on the Appendix I list) were detected above GWPSs (see Tables 3A and 3113). One inorganic statistically exceeded a GWPS for the Second Semi -Annual 2018 event: cobalt at MW-22 and MW-22A. Three VOCs statistically exceeded a GWPS for the Second Semi -Annual 2018 event: 1,4-dichlorobenzene at MW-25; benzene at MW-32R and MW-34; and vinyl chloride at MW-32R, MW-33, and MW-34. The following groundwater monitoring wells are in assessment monitoring due to past exceedances: MW-17, MW-17A, MW-18A, MW-19, MW-19A, MW-20B, MW-25, MW-26, MW-32R, MW-33, and MW-34. Wells with GWPS statistical exceedances during the Second Semi -Annual 2018 event (MW-22, , MW-22A, MW-25, MW-32R, MW-33, and MW-34) are already in the assessment monitoring program, except wells MW-22 and MW-22A. Therefore, wells MW-22 and MW-22A will be added to the assessment monitoring program. The following items are noted in regards to the Second Semi -Annual 2018 GWPS statistical exceedances • Wells in the proximity of MW-25 (MW-2A, MW-2B, MW-22, and MW-22A) and wells downgradient of MW-25 (MW-10 and MW-10A) did not exhibit quantifiable (i.e. at or above the PQL) detections of 1,4-dichlorobenzene. Therefore, 1,4-dichlorobenzene is limited to the vicinity of MW-25. It is recommended that MW-25 continue in Assessment Monitoring. It has been previously concluded that the VOC migration in the MW-32R, MW-33, and MW-34 portion of the site is due to landfill gas migration. The facility has implemented several phases of improvements to the gas collection system in recent years to address gas migration and improve groundwater conditions. Wells MW-32R and MW-34 have exceeded the GWPS for benzene. Wells MW-32R, MW-33, and MW-34 have exceeded the GWPS for vinyl chloride. Monitoring wells MW- 32R, MW-33, and MW-34 will continue in Assessment Monitoring. The site recently performed a methane/landfill gas investigation in this southeast portion of the site to determine if additional measures are warranted, to be submitted under separate cover. • Cobalt at MW-22 and MW-22A statistically exceeded the respective GWPSs. Cobalt is naturally occurring at the site, evident by the historical cobalt detections in various wells across this site, and as typically found within soils of the Upper Piedmont Region of North Carolina (per a USGS Scientific Investigations Report 2013-5072 titled, "Naturally Occurring Contaminants in the Piedmont and Blue Ridge Crystalline -Rock Aquifers and Piedmont Early Mesozoic Basin Siliciclastic-Rock Aquifers, Eastern United States, 1994-2008"). The site does not recommend additional corrective measures other than the upgrades that have been implemented to the landfill Gas Collection and Control System (GCCS) described below. The GCCS improvements and future upgrades to be implemented as needed should further enhance the removal of landfill gas and improve groundwater quality. As noted above, the site recently performed a methane/landfill gas investigation in the southeast portion of the site to determine if additional measures are warranted, to be submitted under separate cover. In correspondence dated October 23, 2014 (DIN 22116), NCDEQ approved a site request to sample the full suite of Appendix II constituents every three years. The most recent full set of Appendix II sampling event occurred during the First Semi -Annual 2017 event. Therefore, the next Appendix II event will occur during the first semi-annual 2020 event for the assessment wells. Previously, dichlorodifluoromethane, mercury, and tin were the only Appendix 11 (non -Appendix 1) constituents confirmed detected above an Groundwater Statistical Analysis Report Charlotte Motor Speedway, Landfill V, North Carolina 6 PQL. However, dichlorodifluoromethane and tin have not been confirmed detected since October 2011. Therefore, only mercury will continue to be sampled semi-annually at each well along with the Appendix I constituents. As noted above, well MW-33 was sampled for the Appendix 11 list for the first time during the Second Semi -Annual 2018 event. The only non -Appendix I constituent detected at MW-33 was sulfide. Sulfide does not have an MCL, NC 2L Standard, or NC IMAC established. The Second Semi -Annual 2018 event was the first event 1,4-dioxane has been monitored. Recent correspondences from DEQ for various landfills have requested 1,4-dioxane be monitored for two semi- annual confirmatory events. Therefore, 1,4-dioxane will be sampled during the First Semi -Annual 2019 event to serve as a confirmatory event and determine if potential seasonal affects exist. Landfill Gas Collection and Control System (GCCS) The following landfill gas system information was provided by SCS Engineers. The GCCS has been operational at the Landfill since 1996. As areas of the Landfill reached 5 years old or 2 years old and at final grade, the GCCS was expanded in general accordance with the NSPS GCCS Design Plan. The GCCS includes over 200 vertical extraction wells, 1 horizontal collector, and is connected to over 25 leachate cleanouts. The facility includes the following major control system components: • A 3,000 scfm candlestick flare, • A 6,000 scfm enclosed flare, • A 12,000 scfm blower system, and • 3 LFG-fired turbines. The turbines are part of a landfill gas -to -energy (LFGTE) facility at the site. The LFGTE facility is owned and operated by Fortistar. The LFGTE facility began generating electricity in early 2000 with power being sold to the City of Concord. The following GCCS summary through the Second Semi -Annual 2018 event was provided by SCS Engineers. Construction on the 2018 GCCS Expansion began on August 17, 2018 and ended on October 1, 2018. Construction and installation were performed by B&M Excavating Co., LLC, and its drilling subcontractor Recovery Drilling Services. SCS provided construction quality assurance (CQA) services to verify that construction activities were completed in general accordance with the Construction Drawings. The project consisted of construction and installation of the following: • Sixteen (16) replacement vertical LFG extraction wells: EW-43A, EW-52A, EW-69C, EW-71 D, EW- 85B, EW-86B, EW-180B, EXP-10C, EXP-11 B, EXP-12A, EXP-1313, EXP-14B, EXP-15B, EXP- 16B, EXP-17A, and EXP-35A; 1,186 feet in total depth. • 18-inch diameter HDPE SDR-17 LFG header pipe. • One (1) 18-inch LFG isolation valve. • 12-inch diameter HDPE SDR-17 LFG header pipe. • One (1) 12-inch LFG isolation valve. • 6-inch diameter HDPE SDR-17 LFG lateral pipe. • 6-inch diameter HDPE SDR-17 Liquids drain pipe for existing and replacement wells. • Two (2) 6-inch wye liquids drain pipe cleanouts. • 4-inch diameter HDPE SDR-11 forcemain pipe to existing and replacement wells. • 2-inch diameter HDPE SDR-9 airline pipe to existing and replacement wells. • Three (3) 2-inch diameter airline isolation/blowoff valves. According to the site a Report is forthcoming in the near future summarizing results of a recent landfill gas investigation in the southern portion of the site. The Report will likely propose additional gas extraction in the area of interest to act as additional interim corrective measures to address the potential gas migration. Groundwater Statistical Analysis Report Charlotte Motor Soeedway. Landfill V. North Carolina 7 Because of the improvements stated above, the efficiency of the GCCS has improved. 2018 upgrades to the GCCS should further enhance the removal of landfill gas and continued improvement in groundwater quality. 7.0 WATER QUALITY ASSESSMENT ACTIVITIES Past Water Qualitv Assessment Activities In a letter dated January 28, 2010 from NCDEQ to the site, a Water Quality Assessment Plan was requested. The requirements for, or the contents of a Water Quality Assessment Plan (WQAP) are not referenced in NC Solid Waste Regulations or Guidance Documents, therefore the facility met with NCDEQ on March 9, 2010 in order to discuss potential items to include in the requested WQAP. Site representatives discussed with NCDEQ the planned items to be included in the WQAP. Subsequently, the site submitted a WQAP on March 19, 2010 of the proposed activities to address the constituents detected above the North Carolina 15A NCAC 2L Water Quality Standards at the site. In correspondence dated April 8, 2010, NCDEQ approved the Water Quality Assessment Plan. The proposed field activities associated with the WQAP were conducted in May 2010. A Water Quality Assessment Report summarizing the data collected during the Water Quality Assessment activities was submitted under separate cover on August 2, 2010. The August 2, 2010 Water Quality Assessment Report provided a summary of actions completed to date and proposed actions in order to address the source and extent of the VOC detections in groundwater monitoring wells at the site. The first phase of the field work occurred in conjunction with the First Semi - Annual 2010 event (May 2010) and consisted of (1) a sewer line examination, (2) headspace methane monitoring in groundwater monitoring wells of concern, and (3) a geochemical evaluation of groundwater and leachate. The results and summary of the first phase activities were submitted within the August 2, 2010 Water Quality Assessment Report. Results of the first phase indicated that (a) no apparent impacts were identified in the vicinity of the sewer line, (b) no significant concentrations of methane are currently present in the headspace of the groundwater monitoring wells of concern, and (c) the geochemical comparisons of MW-19A to leachate indicate possible mixing of groundwater and leachate. However the lack of heavy metals and the presence of downward trending VOCs in groundwater indicate that landfill gas likely was the source of impact at some stage. The improving groundwater conditions indicate that the source has likely been mitigated by the upgrades to the GCCS over the last few years. The February 28, 2011 Water Quality Assessment Report provided an updated summary of the data collected during the Water Quality Assessment activities in the Second Semi -Annual 2010 event (second phase). Installation and monitoring of wells downgradient of the wells of concern would allow the delineation of the horizontal and vertical extent of VOCs. The second phase of the field work occurred in October and November 2010 (in conjunction with the Second Semi -Annual 2010 event) and consisted of (4) installing new wells MW-18R, MW-18AR, MW-19R, and MW-19AR, and (5) sampling the new wells for the Appendix I list of constituents. Results of the second phase indicated that (d) lack of impact at well MW-18AR, which defines the extent of horizontal and vertical area of impact in the MW-18A area, and (e) impacts below the 2L Standards have not been horizontally or vertically defined in the MW-1 9R/MW-1 9AR portion of the site. Latest Water Quality Assessment Activities In correspondence dated September 12, 2013 (DIN 19706), NCDEQ approved a site request to monitor wells MW-18R and MW-18AR on an annual basis due to lack of confirmed exceedances since installation in 2010. Therefore, wells MW-18R and MW-18AR are sampled during the first semi-annual event of each year. Table 6 summarizes the results of the Second Semi -Annual 2018 event at water quality assessment (extent) wells. The Second Semi -Annual 2018 event sampling results exhibited concentrations above the Groundwater Statistical Analysis Report Charlotte Motor Speedway, Landfill V, North Carolina 8 GWPSs for barium at MW-19R; cobalt at MW-19AR and MW-19R; and 1,4-dichlorobenzene at MW-19AR and MW-19R. These results are generally consistent with historical data (since installation in 2010). Review of data for MW-19AR and MW-19R indicated that barium, cobalt, and 1,4-dichlorobenzene were previously above GWPSs in adjacent/upgradient wells MW-19A and/or MW-19. No organic GWPSs have been statistically exceeded at MW-19 or MW-19A since the Second Semi -Annual 2009 event, likely due to the enhancements to the GCCS in combination with natural attenuations. It is recommended that MW-19R and MW-19AR continue to be monitored on a semi-annual basis. The Second Semi -Annual 2018 event sampling results also exhibited concentrations above the GWPS for 1,4-dioxane at MW-19AR and MW-19R. As noted previously, the Second Semi -Annual 2018 event was the first event for 1,4-dioxane to be sampled at the site. TABLES TABLE 1 WELLS ANALYZED SECOND SEMI-ANNUAL 2018 EVENT CHARLOTTE MOTOR SPEEDWAY, LANDFILL V UPGRADIENT DOWNGRADIENT WELLS WELLS MW-11, MW-14, MW- MW-1A, MW-1B, MW-2A, MW-2B, MW-10, MW-10A, MW-12, 14B, MW-15 MW-16, MW-17, MW-17A, MW-18A, MW-19, MW-19A, MW-20AR, MW-20B, MW-21, MW-22, MW-22A, MW-24, MW-25, MW-26, MW-27, MW-28, MW-29R, MW-30R, MW-31, MW-32R, MW-33, MW-34 Wells MW-17, MW-17A, and MW-24 are sampled annually during the first semi-annual events each year. Wells MW-18R, MW-18AR, MW-19R, and MW-19AR are Water Quality Assessment Wells and addressed separately in Section 7.0 of the Report. Wells MW-18R and MW-18AR are sampled annually during the first semi-annual events each year, while MW-19R and MW-19AR are sampled semi-annually. TABLE 2 ORGANIC DETECTIONS SECOND SEMI-ANNUAL 2018 EVENT CHARLOTTE MOTOR SPEEDWAY, LANDFILL V Monitoring Point Parameter National Primary Drinking Water Standard-MCL (ug/L) 15A NCAC 2L Water Quality Standard (ug/L) Results (ug/L) MDL (ug/L) PQL (ug/L) MW-1A 1,4-Dioxane N/A 3 14.6 1.9 2 MW-1B 1,4-Dioxane N/A 3 22.8 1.9 2 MW-2A 1,4-Dioxane N/A 3 3.5 1.9 2 1,4-Dichlorobenzene 75 6 2.2 0.58 1 MW-18A 1,4-Dioxane N/A 3 37.9 1.9 2 Benzene 5 1 1.2 0.2 1 Vinyl chloride 2 0.03 2.9 0.6 1 MW-19 1,4-Dichlorobenzene 75 6 1.4 0.58 1 1,4-Dioxane N/A 3 8 1.9 2 MW-19A 1,4-Dioxane N/A 3 3.6 1.9 2 MW-20B 1,4-Dichlorobenzene 75 6 2.8 0.58 1 1,4-Dioxane N/A 3 3.7 1.9 2 MW-22 1,4-Dioxane N/A 3 23.7 1.9 2 MW-22A 1,4-Dioxane N/A 3 29 1.9 2 MW-25 1,4-Dichlorobenzene 75 6 12.4 0.58 1 Chlorobenzene 100 50 8.3 0.53 3 MW-32R Benzene 5 1 4.5 0.2 1 Vinyl chloride 2 0.03 4.2 0.6 1 Benzene 5 1 4.3 0.2 1 cis-1,2-Dichloroethene 70 70 5.9 0.66 5 MW-33 Methylene Chloride 5 5 4.1 0.5 1 Trichloroethene 5 3 1.6 0.34 1 Vinyl chloride 2 0.03 3.6 0.6 1 1,4-Dichlorobenzene 75 6 1.3 0.58 1 Benzene 5 1 9.6 0.2 1 cis-1,2-Dichloroethene 70 70 12.7 0.66 5 MW-34 Methylene Chloride 5 5 1.2 0.5 1 Tetrachloroethene 5 0.7 3 0.78 1 Trichloroethene 5 3 1 B 0.34 1 Vinyl chloride 2 0.03 2.1 0.6 1 Detections listed are for concentrations reported at or above the Solid Waste Section Limit (S WSL). 2L Standards updated by NCDEQ on 10110118. Value exceed the applicable 2L Standard. 8: Denotes parameter also detected in the associated equipment blank, field blank, trip blank, or laboratory method blank. TABLE 3A COMPARISONS TO GWPSs (INORGANICS) SECOND SEMI-ANNUAL 2018 EVENT CHARLOTTE MOTOR SPEEDWAY, LANDFILL V Constituent (ug/L) MDL PQL MCL NC 2L Std NC IMAC Final GWPS MW-1A MW-1B MW-2A MW-2B MW-10 MW-10A MW-11 MW-12 MW-14 MW-14B MW-15 MW-16 MW-17 MW-17A MW-18A MW-19 Antimony Total 0.78 6 6 NE 1 6** <6 <6 <6 <6 <6 <6 <6 <6 <6 <6 1.7 J <6 NS NS <6 <6 Arsenic Total 0.57 10 10 10 NE 10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 NS NS <10 <10 Barium Total 0.78 100 2,000 700 NE 700 121 8.8 180 46.9 33.5 J 31.5 J 22 J 18.6 J 8.5 J 5.2 J 46.2 J 48.8 J NS NS 609 275 Beryllium Total 0.05 1 4 NE 4 4 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS NS <1 <1 Cadmium Total 0.093 1 5 2 NE 2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS NS 0.49 J <1 Chromium Total 1.6 10 100 10 NE 98** <10 <10 <10 1.6 J <10 <10 <10 7.3 J <10 <10 8.4 J 2.9 J NS NS 2 J <10 Cobalt Total 0.52 10 NE NE 1 12** 6.4 J 2.3 J <10 13.2 <10 <10 <10 1.5 J <10 <10 1.1 J 3.1 J NS NS 11.1 1.4 J Copper Total 1.3 10 1,300 1,000 NE 1,000 3.9 <10 <10 <10 <10 <10 <10 <10 2.7 J <10 7.9 J 1.6 J NS NS 3.9 J <10 Cyanide Total 10 10 200 70 NE 70 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS Lead Total 0.27 10 15 15 NE 15 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 1.9 J 11 NS NS <10 <10 Mercury Total 0.036 0.2 2 1 NE 1 0.058 JB 0.066 JB 0.074 JB 0.12 JB 0.071 JB 0.08 JB 0.061 JB 0.063 JB 0.057 JB 0.09 JB 0.088 JB 0.077 JB NS NS 0.083 JB 0.061 JB Nickel Total 0.95 50 NE 100 NE 100 5 J 22.7 J 7.9 J 16 J 1.4 J 1.3 J 1.3 J 6.4 J 12.4J 1.2 J 17 J 3.6 J NS NS 7.8 J 59.7 Selenium Total 1.4 10 50 20 NE 20 1.8 J <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 NS NS 1.6 J <10 Silver Total 0.95 10 NE 20 NE 20 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 NS NS <10 <10 Sulfide NE 1000 NE NE NE NE NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS Thallium Total 0.14 5.5 2 NE 0.28 5.5** <5.5 <5.5 <5.5 <5.5 <5.5 <5.5 <5.5 <5.5 <5.5 <5.5 <5.5 <5.5 NS NS <5.5 <5.5 Tin Total 7 20 NE NE 2000 2000 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS Vanadium Total 1.9 25 NE NE 0.3 33** 2.6 J 3.9 J 5.3 J 3.8 J <25 <25 5.2 J 6.4 J 6.5 J 6.7 J 9.5 J 11.4 J NS NS <25 <25 Zinc Total 2.1 10 NE 1,000 NE 1,000 4.4 JB 7.5 JB 3.7 JB 4 JB 5.5 JB 5.3 JB 3 JB 5.9 JB 6.3 JB 4.8 JB 6.6 JB 9.4 JB NS NS 34.1 3.5 JB Field Dissolved Oxygen (ug/L) NE NE NE NE NE NE 1.19 1.72 1.43 1.24 1.11 1.67 2.21 3.97 3.6 1.03 2.2 1.22 NS NS 1.34 1.16 Field pH (SU) NE NE NE NE NE NE 6.62 7.24 6.21 6.42 5.76 6.63 6.58 6.25 6.59 7.03 6.64 6.45 NS NS 6.04 6.37 Field Specific Conductance (umhos/cm) NE NE NE NE NE NE 982 793 1197 886 107 236 479 384 342 610 397 689 NS NS 1631 1015 Field Temperature (°C) NE NE NE NE NE NE 19.3 18.5 20.9 17.8 17.6 19.6 19.9 17.8 19.7 17.8 22.8 20.6 NS NS 21.1 19.4 Field Turbidity (NTU) NE NE NE NE NE NE 3.24 1.32 3.17 3.11 6.00 4.99 2.04 5.83 4.12 2.78 3.82 4.63 NS NS 0.44 1.08 Constituent (ug/L) MDL PQL MCL NC 2L Std NC IMAC Final GWPS MW-19A MW-20AR MW-20B MW-21 MW-22 MW-22A MW-24 MW-25 MW-26 MW-27 MW-28 MW-29R MW-30R MW-31 MW-32R MW-33 MW-34 Antimony Total 0.78 6 6 NE 1 6** 1.8 J <6 <6 0.86 J <6 <6 NS <6 <6 <6 <6 <6 <6 <6 <6 <6 <6 Arsenic Total 0.57 10 10 10 NE 10 <10 <10 <10 1.2 J <10 <10 NS <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 Barium Total 0.78 100 2,000 700 NE 700 93.35 206 784 131 206 65.3 NS 108 155 40.8 60.1 37.2 100 59.5 176 91.2 179 Beryllium Total 0.05 1 4 NE 4 4 <1 <1 <1 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 <1 <1 0.065 J <1 Cadmium Total 0.093 1 5 2 NE 2 <1 0.18 J 1.5 0.29 J 0.18 J 0.79 J NS 0.19 J <1 <1 <1 <1 <1 <1 <1 0.21 J <1 Chromium Total 1.6 10 100 10 NE 98** <10 <10 <10 92.7 2.8 J 1.6 J NS <10 1.7 J 3.6 J 4 J 3 J 7.7 J I <10 9 J 2.3 J 2.3 J Cobalt Total 0.52 10 NE NE 1 12** 7.6 J 1.5 J 8.8 J 1680 52.9 23 NS 5.7 J 5.6 J 0.96 J <10 1.7 J 1.4 J <10 87.6 0.77 J 2.6 J Copper Total 1.3 10 1,300 1,000 NE 1,000 <10 1.9 J 4.9 J 688 35.6 5.5 J NS <10 <10 7.8 J <10 8.7 J 8.8 J 1.4 J 33.5 9.6 J 4.2 J Cyanide Total 10 10 200 70 NE 70 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS <10 NS Lead Total 0.27 10 15 15 NE 15 <10 <10 0.74 J 8 J <10 <10 NS <10 <10 <10 <10 <10 <10 <10 13.1 0.33 J <10 Mercury Total 0.036 0.2 2 1 NE 1 0.079 JB 0.1 JB 0.12 JB 0.13 JB <0.2 0.042 JB NS 0.17 JB 0.22 B 0.083 JB 0.1 JB 0.065 JB 0.085 JB 0.4 B 0.08 JB 0.31 B 0.073 JB Nickel Total 0.95 50 NE 100 NE 100 14 J 26.8 40.6 J 170 56.9 126 NS 24.1 J 16 J 7 J 12.7 J 5.9 J 15.2 J 3 J 41 J 3.4 J 3.9 J Selenium Total 1.4 10 50 20 NE 20 <10 <10 <10 <10 1.9 J <10 NS <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 Silver Total 0.95 10 NE 20 NE 20 <10 <10 <10 <10 <10 <10 NS <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 Sulfide NE 1000 NE NE NE NE NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS 3800 NS Thallium Total 0.14 5.5 2 NE 0.28 5.5** <5.5 <5.5 <5.5 <5.5 <5.5 <5.5 NS <5.5 <5.5 <5.5 <5.5 <5.5 <5.5 <5.5 <5.5 <5.5 <5.5 Tin Total 7 20 NE NE 2,000 2,000 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS <20 NS Vanadium Total 1.9 25 NE NE 0.3 33** <25 <25 <25 55.4 5 J <25 NS 4.1 J 6.5 J 5.9 J 2.1 J 5.4 J 6.5 J 2.9 J 9.6 J <25 <25 Zinc Total 2.1 10 NE 1,000 NE 1,000 454 21.7 B 51 127 6.3 JB 10 JB NS 6.5 JB 3.9 JB 5.3 JB 4.5 JB 5.5 JB 17.2 B 4.9 JB 9.8 JB 12.7 B 14.9 B Field Dissolved Oxygen (ug/L) NE NE NE NE NE NE 2.51 1.52 1.19 2.52 2.35 1.09 NS 2.23 1.22 3.28 3.16 2.00 1.72 2.52 1.45 2.17 1.36 Field pH (SU) NE NE NE NE NE NE 7.21 6.20 6.23 6.62 6.29 6.44 NS 6.33 6.24 6.34 6.60 6.27 6.69 6.98 6.70 5.51 5.95 Field Specific Conductance (umhos/cm) NE NE NE NE NE I NE 762 615 1131 448 1462 1963 1 NS 1238 894 230 436 307 236 220 697 1219 347 Field Temperature (°C) NE NE NE NE NE NE 19.6 18.7 20.1 20.8 24.8 20.9 NS 23.9 19.8 20.8 18.9 19.3 18.7 19.0 23.9 21.1 21.4 Field Turbidity (NTU) NE NE NE NE NE NE 1.88 3.59 3.72 5.86 4.19 1.98 NS 3.75 1.23 7.29 3.19 5.01 9.11 0.08 5.44 12 8.31 B: Denotes parameter also detected in the associated equipment blank, field blank, trip blank, or laboratory method blank. J: Denotes Sample result above the MDL but below the PQL; estimated value; value may not be accurate. Final GWPS is the lowest of the MCL, NC 2L Standard, and NC Interim Maximum Allowable Concentration (IMAC) values. ": Denotes background limit or PQL used if higher than NC 2L Standard and NC IMAC. Denotes a concentration at or above a PQL is also above the Final GWPS: NS: Denotes not required to be sampled this event. Wells MW-17, MW-17A, and MW-24 are sampled annually during the first semi-annual events each year. TABLE3B COMPARISONS TO GWPSs (ORGANICS) SECOND SEMI-ANNUAL 2018 EVENT CHARLOTTE MOTOR SPEEDWAY, LANDFILL V Constituent (ug/L) MDL PQL MCL NC 2L Std NC IMAC Final GWPS MW-1A MW-1 B MW-2A MW-213 MW-10 MW-10A MW-11 MW-12 MW-14 MW-14B MW-15 MW-16 MW-17 MW-17A MW-18A MW-19 MW-19A 1,1-Dichloroethane 0.41 5 NE 6 NE 6 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 NS NS <5 <5 <5 1,2-Dichloroethane 0.67 1 5 0.4 NE 1** <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS NS <1 <1 <1 1,4-Dichlorobenzene 0.58 1 75 6 NE 6 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS NS 2.2 1.4 <1 1,4-Dioxane 1.9 2 NE 3 NE 3 14.6 22.8 3.5 <2 <2 <2 <2 <2 <2 <2 <2 <2 NS NS 37.9 8 3.6 Benzene 0.2 1 5 1 NE 1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS NS 1.2 <1 <1 Carbon Disulfide 0.79 100 NE 700 NE 700 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 NS NS 3 J <100 <100 Chlorobenzene 0.53 3 100 50 NE 50 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 NS NS 1.4 J <3 <3 cis- 1,2-Dichloroethene 0.66 5 70 70 NE 70 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 NS NS 1.6 J <5 <5 Methylene Chloride 0.5 1 5 5 NE 5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS NS <1 <1 <1 Tetrachloroethene 0.78 1 5 0.7 NE 1** <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS NS <1 <1 <1 trans-1,2-Dichloroethene 0.46 5 100 100 NE 100 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 NS NS <5 <5 <5 Trichloroethene 0.34 1 5 3 NE 3 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS NS <1 <1 <1 Vinyl Chloride 0.6 1 2 0.03 NE 1** <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 NS NS 2.9 <1 <1 Constituent (ug/L) MDL PQL MCL NC 2L Std NC IMAC Final GWPS MW-20AR MW-20B MW-21 MW-22 MW-22A MW-24 MW-25 MW-26 MW-27 MW-28 MW-29R MW-30R MW-31 MW-32R MW-33 MW-34 1,1-Dichloroethane 0.41 5 NE 6 NE 6 <5 2.1 J <5 <5 <5 NS <5 <5 <5 <5 <5 <5 <5 <5 2 J 1.7 J 1,2-Dichloroethane 0.67 1 5 0.4 NE 1** <1 <1 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 <1 <1 0.88 J <1 1,4-Dichlorobenzene 0.58 1 75 6 NE 6 <1 2.8 <1 <1 <1 NS 12.4 0.97 J <1 <1 <1 <1 <1 <1 <1 1.3 1,4-Dioxane 1.9 2 NE 3 NE 3 <2 3.7 <2 23.7 29 NS <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 Benzene 0.2 1 5 1 NE 1 <1 0.25 J <1 <1 <1 NS 0.35 J 0.58 J <1 <1 <1 <1 <1 4.5 4.3 9.6 Carbon Disulfide 0.79 100 NE 700 NE 700 <100 <100 <100 <100 <100 NS <100 <100 <100 <100 <100 <100 <100 <100 <100 <100 Chlorobenzene 0.53 3 100 50 NE 50 <3 <3 <3 <3 <3 NS 8.3 <3 <3 <3 <3 <3 <3 <3 <3 0.56 J cis- 1,2-Dichloroethene 0.66 5 70 70 NE 70 <5 <5 <5 <5 <5 NS <5 1 J <5 <5 <5 <5 <5 4.5 J 5.9 12.7 Methylene Chloride 0.5 1 5 5 NE 5 <1 <1 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 <1 0.57 J 4.1 1.2 Tetrachloroethene 0.78 1 5 0.7 NE 1** <1 <1 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 <1 <1 0.92 J 3 trans-1,2-Dichloroethene 0.46 5 100 100 NE 100 <5 <5 <5 <5 <5 NS <5 <5 <5 <5 <5 <5 <5 <5 1 J 1.1 J Trichloroethene 0.34 1 5 3 NE 3 <1 <1 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 <1 0.6 JB 1.6 1 B Vinyl Chloride 0.6 1 2 0.03 NE 1** <1 <1 <1 <1 <1 NS <1 <1 <1 <1 <1 <1 <1 4.2 3.6 2.1 B: Denotes parameter also detected in the associated equipment blank, field blank, trip blank, or laboratory method blank. J: Denotes Sample result above the MDL but below the PQL; estimated value; value may not be accurate. Final GWPS is the lowest of the MCL, NC 2L Standard, and NC Interim Maximum Allowable Concentration (IMAC) values. * : Denotes background limit or PQL used if higher than NC 2L Standard and NC IMAC. Denotes a concentration at or above a PQL is also above the Final GWPS: Only the VOCs reported above an MDL this event are summarized on the table. NS: Denotes not required to be sampled this event. Wells MW-17, MW-17A, and MW-24 are sampled annually during the first semi-annual events each year. TABLE 4 SURFACE WATER DATA COMPARED TO NC 2B STANDARDS SECOND SEMI-ANNUAL 2018 EVENT CHARLOTTE MOTOR SPEEDWAY, LANDFILL V Constituent Units NC 2B Standard MDL PQL SW-1 SW-2 Antimony Total u /L NE 0.78 6 <6 <6 Arsenic Total u /L 10 0.57 10 <10 <10 Barium Total u /L 1,000 0.78 100 42.6 J 51.3 J Beryllium Total u /L 6.5 0.05 1 <1 <1 Cadmium Total u /L 2 0.093 1 <1 <1 Chromium Total u /L 20 0.58 10 <10 <10 Cobalt Total u /L NE 0.52 10 1 0.56 J <10 Copper Total u /L 3 1.3 10 2.4 J <10 Lead Total u /L 25 0.27 10 <10 <10 Nickel Total u /L 8.3 0.95 50 <50 1 J Selenium Total u /L 5 1.4 10 <10 <10 Silver Total u /L 0.06 0.95 10 <10 <10 Thallium Total ug/L NE 0.14 5.5 <5.5 <5.5 Vanadium Total ug/L NE 1.9 25 3.2 J 7.4 J Zinc Total ug/L 50 2.1 10 4.7 JB 4.2 JB Field Dissolved Oxygen ug/L NE n/a n/a 1.19 1.36 Field pH SU I NE I n/a n/a 7.67 7.21 Field Specific Conductance umhos/cm NE n/a n/a 272 463 Field Temperature °C NE n/a n/a 21.6 20.6 Field Turbidity NTU NE n/a n/a 9.31 2.86 B: Denotes parameter also detected in the associated field blank, trip blank, or laboratory method blank. J: Denotes Sample result above the MDL but below the PQL; estimated value; value may not be accurate. No VOCs detected above a PQL this event, therefore not included on this table. For NC 2B Standard, lowest value utilized from the classifications from the 2B Table published May 15, 2013. TABLE 5 INTER -WELL PREDICTION LIMIT EXCEEDANCES SECOND SEMI-ANNUAL 2018 EVENT CHARLOTTE MOTOR SPEEDWAY, LANDFILL V Well Parameter (Total Metals) MDL PQL MCL NC 2L NC IMAC Final GWPS Results Prediction Limit MW-22B Cobalt 0.52 10 NE NE 1 12— 13.2 12 MW-20B Barium 0.78 100 2,000 700 NE 700 784 380 MW-21 Cobalt 0.52 10 NE NE 1 12— 1680 12 Nickel 0.95 50 NE 100 NE 100 170 43 Vanadium 1.9 25 NE NE 0.3 33" 55.4 1 33 MW-22 Cobalt 0.52 10 NE NE 1 12— 52.9 12 MW-22A Cobalt 0.52 10 NE NE 1 12— 23 12 Nickel 0.95 50 NE 100 NE 100 126 43 MW-32R Cobalt 0.52 10 NE NE 1 12" 87.6 12 All units are in ug/L. Final GWPS is the lowest of the MCL, NC 2L Standard, and NC Interim Maximum Allowable Concentration (IMAC) values. '*: Denotes background limit or PQL used if higher than MCL, NC 2L, and NC IMAC. TABLE 6 WATER QUALITY ASSESSMENT WELL DATA COMPARED TO GWPSs SECOND SEMI-ANNUAL 2018 EVENT CHARLOTTE MOTOR SPEEDWAY, LANDFILL V Constituent u /L MDL PQL MCL NC 2L Std NC GWPS Final GWPS MW-18AR MW-18R MW-19AR MW-19R Antimony Total 0.78 6 6 NE 1 6** NS NS 0.87 J <6 Arsenic Total 0.57 10 10 10 NE 10 NS NS 0.74 J 0.687 Barium Total 0.78 100 2,000 700 NE 700 NS NS 280 817 Beryllium Total 0.05 1 4 NE 4 4 NS NS <1 <1 Cadmium Total 0.093 1 5 2 NE 2 NS NS 0.92 J 0.69 J Chromium Total 1.6 10 100 10 NE 98** NS NS 19.7 1.7 J Cobalt Total 0.52 10 NE NE 1 12** NS NS 22.6 35.5 Copper Total 1.3 10 1,300 1,000 NE 1,000 NS NS 14.3 16.4 Cyanide Total NS 10 200 70 NE 70 NS NS NS NS Lead Total 0.27 10 15 15 NE 15 NS NS 0.63 J 0.47 J Mercury Total 0.036 0.2 2 1 NE 1 NS NS 0.13 JB 0.083 JB Nickel Total 0.95 50 NE 100 NE 100 NS NS 58.2 52.8 Selenium Total 1.4 10 50 20 NE 20 NS NS <10 <10 Silver Total 0.95 10 NE 20 NE 20 NS NS 2.1 J <10 Sulfide NS 1000 NE NE NE NE NS NS NS NS Thallium Total 0.14 5.5 2 NE 0.28 5.5** NS NS <5.5 <5.5 Tin Total NS 100 NE NE 2,000 2,000 NS NS NS NS Vanadium Total 1.9 25 NE NE 0.3 19** NS NS 5.7 J 3.1 J Zinc Total 2.1 10 NE 1,000 NE 1,000 NS NS 30.5 17.6 B Field Dissolved Oxygen (ug/L) NE NE NE NE NE NE NS NS 1.26 1.68 Field pH (SU) NE NE NE NE NE NE NS NS 6.4 6.23 Field Specific Conductance umhos/cm) NE NE NE NE NE NE NS NS 2777 2621 Field Temperature °C NE NE NE NE NE NE NS NS 19 18.1 Field Turbidity (NTU) NE NE NE NE NE NE NS NS 7.1 3.23 Constituent (ug/L) MDL PQL MCL NC 2L Std NC GWPS Final GWPS MW-18AR MW-18R MW-19AR MW-19R 1,1-Dichloroethane 0.41 5 NE 6 NE 6 NS NS 1.1 J <5 1,2-Dichloroethane 0.67 1 5 0.4 NE 1** NS NS <1 <1 1,4-Dichlorobenzene 0.58 1 75 6 NE 6 NS NS 6.4 6.1 1,4-Dioxane 1.9 2 N/A 3 NE 3 NS NS 55.8 52.6 Benzene 0.2 1 5 1 NE 1 NS NS 1 0.73 J Carbon Disulfide 0.79 100 NE 700 NE 700 NS NS <100 <100 Chlorobenzene 0.53 3 100 50 NE 50 NS NS 3.2 1.9 J cis-1,2-Dichloroethene 0.66 5 70 70 NE 70 NS NS <5 <5 Methylene Chloride 0.5 1 5 5 NE 5 NS NS <1 <1 Tetrachloroethene 0.78 1 5 0.7 NE 1** NS NS <1 <1 trans-1,2-Dichloroethene 0.46 5 100 100 NE 100 NS NS <5 <5 Trichloroethene 0.34 1 5 3 NE 3 NS NS <1 <1 Vinyl Chloride 0.6 1 1 2 1 0.03 NE 1** NS NS <1 <1 B: Denotes parameter also detected in the associated equipment blank, field blank, trip blank, or laboratory method blank. J: Denotes Sample result above the MDL but below the PQL; estimated value; value may not be accurate. Final GWPS is the lowest of the MCL, NC 2L Standard, and NC Interim Maximum Allowable Concentration (IMAC) values. **: Denotes background limit or PQL used if higher than NC 2L Standard and NC IMAC. Denotes a concentration at or above a PQL is also above the Final GWPS: NS: Denotes not required to be sampled this event. Wells MW-18R and MW-18AR are sampled annually during the first semi-annual events each year. APPENDICES APPENDIX A POTENTIOMETRIC SURFACE MAP SW-1 9 / / 1 I 0 \MW-10 55 .10 \ 557.13 57.13 LEGEND SMW-22 Shallow Monitoring Well Location MW-22A Deep Monitoring Well Location 580.94 Groundwater Elevation (fmsl) — 0 _ 565 — Potentiometric Surface Contour (fmsl) J .12 Hydraulic Gradient Inferred 58718 . Groundwater er low Direction t J &SW-1 Surface Water Sampling Location (Approx) Landfill Cell Boundary Expansion Areas I ^ 1 Denotes Assessment Monitoring \ Program Well I \ 1 Denotes Water Quality Assessment (Extent) Well MW-1A CLOSE 574.MW_ Water levels collected by Pace Analytical services, LLC on 84 .73 CELL 1 —\ O l October 1, zol8. 57373 I 629.69 (\ Basemap provided by Cooper Aerial Surveys Co., date of ti tl Photography is January 27, 2013. L— I I � NORTH I \ CLOSED \� CELL I \\\ EXISTIN rr 0 250 500 1000 \ \ CELL 2 �\ \ ® PHAS 6 p \ MW-2A i �� MW-14 574.60 \ � 620.36� Scale in Feet � Graphic Scale: finch = 500 feet 57417 \\\\ t 0p22 �620.18 EXIST 6,1 CELL 2s PHASE 1 J MW-25* / \ � s MW-22A \ o ;580.52 1\ MW-22 1 580.94 I \ \ s EXI TING �� \ / l CEL 213 / lss PHA 1 ses MW-21 IM 15 568.26 ^i' �� �611.80 E STIN / D \\ 1 LL 2C/ ' \ ASE 1 1 \ 1 J MW-20B 576.84 i(11 MW-20AR 574.96 1 \ 1 1 n \ 1 ELL 2D S 2 ISTING� sy XISTIE G ELL \ MW-16 1 591.73 i EXISTING �558.62 "M\N_19R*' U / I CELL 21- ,\ 5 9.411 / MW-17* MW-17A* vv / 558.08 558.74 � A ;ti� (• MW-18A*, 56.6.53 �. ��� \ „;\ — SW-2 o EXIST j MW-27 MW-18R** 1 1 572.45 MW-18AR** 560.31 MW-34* CELL 2 \ 556.79� 548.76 \ PHASE \ 1 \ 1 MW-33 . 548.30 i EXI NG \ CEL H vv PHAS 2 \ 1 565.68 562 318 \ MW 566.6.64 / / 1 y65 EXISTING l CELL 21 / o Q q - 11A I/ PHASE 3 j o MW-30R' / �• / i' ___ �MW-29R D — — — 559.37 NETT Figure 1 1002 Morgan Meadow Drive Second Semi -Annual 2018 Potentiometric Surface Map Wentzville, MO 63385 314-496-4654 0 N nn T I G www.jettenviro.com C Charlotte Motor Speedway Landfill V, Harrisburg, North Carolina Groundwater Elevation Summary Table Charlotte Motor Speedway, Landfill V Well Top of PVC Casing Elevation (fmsl)' Depth to z Water (ft) Groundwater Elevation (fmsl) Shallow Wells MW-1A 579.45 4.61 574.84 MW-2A 579.92 5.32 574.60 MW-10 578.10 21.00 557.10 MW-11 638.82 9.13 629.69 MW-12 596.69 9.51 587.18 MW-14 629.56 9.20 620.36 MW-15 620.60 8.80 611.80 MW-16 606.53 14.80 591.73 MW-17 569.88 11.80 558.08 MW-18A 581.81 15.28 566.53 MW-18R 580.02 19.71 560.31 MW-19 588.58 27.58 561.00 MW-19R 582.53 23.35 559.18 MW-20AR 585.28 10.32 574.96 MW-21 581.99 13.73 568.26 MW-22 586.21 5.27 580.94 MW-24 576.00 11.37 564.63 MW-25 589.07 6.33 582.74 MW-26 594.86 15.45 579.41 MW-27 581.32 8.87 572.45 MW-28 574.45 12.14 562.31 MW-29R 565.61 6.24 559.37 MW-30R 587.84 27.95 559.89 MW-31 592.26 25.62 566.64 MW-32R 587.80 22.12 565.68 MW-33 575.70 27.40 548.30 MW-34 577.71---j- 28.95 548.76 Deep Wells MW-1 B 580.74 7.01 573.73 MW-2B 579.92 5.75 574.17 MW-10A 578.67 21.54 557.13 MW-14B 629.82 9.64 620.18 MW-17A 570.12 11.38 558.74 MW-18AR 579.93 23.14 556.79 MW-19A 588.07 28.00 560.07 MW-19AR 582.83 24.21 558.62 MW-20B 583.57 6.73 576.84 MW-22A 1 586.13 1 5.61 580.52 Note 1: Top of PVC Casing Elevations from the December 1, 2000 Correspondence from S&ME, Inc. to the site regarding the October 2000 groundwater flow data. Top of PVC Casing Elevations for wells MW-16, MW-26 through MW-34 from survey information provided by Earnhardt Grading in correspondence dated June 19, 2008. Top of PVC Casing Elevations for wells MW-18R, MW-18AR, MW-19R, MW-19AR, MW-29R, MW-30R, and MW-32R from survey information provided by David Garrett & Associates in correspondence dated December 6, 2010. Note 2: Depth to water collected by Pace Analytical Services, LLC on October 1, 2018. Groundwater Flow Velocity Calculations Charlotte Motor Speedway, Landfill V Second Semi -Annual 2018 Event Velocitv Ranae For wells in Saprolite V = [(k)(i)]/(n) V = [(1 x 10-3 cm/sec)(0.021)]/0.16 V = 1.3 x 10-4 cm/sec V = 0.37 ft/day V = 135 ft/year For wells in PWR V = [(k)(i)]/(n) V = [(2 x 10-4 cm/sec)(0.021)]/0.20 V = 2.1 x 10-5 cm/sec V = 0.060 ft/day V = 22 ft/year For wells in Bedrock V = [(k)(i)]/(n) V = [(7 x 10-5 cm/sec)(0.021)]/0.07 V = 2.1 x 10-5 cm/sec V = 0.060 ft/day V = 22 ft/year Hydraulic conductivities (k) are from the geometric mean of the hydraulic conductivity for each unit monitored at the site. Hydraulic conductivities provided in "Groundwater Certification Document, CMS Landfill V" by S&ME, Inc. dated October 4, 1994. Effective porosities (n) are from the geometric mean of the effective porosities for each unit monitored at the site. Effective porosities provided in "Groundwater Certification Document, CMS Landfill V" by S&ME, Inc. dated October 4, 1994. Conversion factor. ft/day = 2,835 x cm/sec. Gradient (i) is from the average gradient at site using the potentiometric surface map across the northern portion of the site and the southern portion of the site. Gradient (i) = Change in Groundwater Elevation along Flow Path inortn: = 50 ft / 2,295 ft = 0.022 isouth: = 50 ft / 2,624 ft = 0. 019 Average gradient across the site is (0.022 + 0.019) / 2 = 0.021 WELL CONSTRUCTION SUMMARY SECOND SEMI-ANNUAL 2018 EVENT CHARLOTTE MOTOR SPEEDWAY, LANDFILL V Phase Well Northing Easting Ground Surface Elevation Top of Casing Elevation Casin Stickup Total Depth Elevation of Bottom of Boring Depth to Partially Weathered Rock Elevation of Partially Weathered Rock Depth to Rock Elevation of Rock Depth to Top of Screen Top of Screen Elevation Depth to Bottom of Screen Bottom of Screen Elevation Screen Thickness Litho. Unit Hydro. Unit Comments ft. msl ft. Mel ft. ft. b s ft. msl ft. b s ft. msl ft. b s ft. msl ft. b s ft. msl ft. b s ft. msl ft. 1 MW-1A 589012.548 1502604.566 576.45 579.45 3 17 559.45 NA NA NA NA 6.5 569.95 16.5 559.95 10 "Gneiss" Soil Likely Diorite 1 MW-1B 589012.548 1502604.566 578.24 580.74 2.5 32 546.24 24 554.24 29 549.24 25.5 552.74 31.5 546.74 5 "Gneiss" Bedrock Likely Diorite 1 MW-2A 587925.997 1502545.587 577.67 579.92 2.25 17 560.67 NA NA NA NA 4.5 573.17 16.5 561.17 2.5 Diorite*** Soil 1 MW-2B 587912.904 1502534.016 576.92 579.92 3 37 539.92 26 550.92 30 546.92 26 550.92 36 540.92 10 Diorite*** Bedrock 5 MW-10 587262.857 1501693.493 575.90 578.10 2.2 25 550.90 NA NA NA NA 9.5 566.40 24.5 551.40 15 Diorite*** Soil 5 MW-10A* 587262.857 1501693.493 576.17 578.67 2.5 43 533.17 NA NA 32.5 543.67 32.5 543.67 42.5 533.67 10 Diorite*** Bedrock 1 MW-11 588977.331 1504541.502 636.62 638.82 2.2 22 614.62 NA NA NA NA 6.5 630.12 21.5 615.12 15 Diorite*** Soil 1 MW-12 589652.175 1502979.749 594.49 596.69 2.2 26 568.49 NA NA NA NA 10 584.49 25 569.49 15 Diorite*** Soil 1 MW-14 587899.549 1504980.859 627.54 629.56 2.02 15 612.54 1 626.54 12.8 614.74 5 622.54 15 612.54 10 Diorite*** PWR 1 MW-14B 587850.011 1505064.753 627.56 629.82 2.26 50 577.56 1 626.56 12.8 614.76 40 587.56 50 577.56 10 Diorite*** Bedrock 1 MW-15* 586871.0366 1505415.301 618.10 620.60 2.5 9.5 608.60 NA NA 9.5 608.60 4 614.10 9 609.10 5 Diorite*** Soil 2 MW-16**** 585653.703 1505654.468 604.03 606.53 2.5 27 577.03 23.5 580.53 NA NA 12 592.03 27 577.03 15 Diorite Soil/PWR 4 MW-17* 584792.54 1504230.802 566.88 569.88 3 25 541.88 NA NA 25 541.88 15 551.88 25 541.88 10 S enite Soil/PWR Assumed rock depth 4 MW-17A* 584792.54 1504230.802 567.12 570.12 3 40 527.12 NA NA 25 527.12 30 537.12 40 527.12 10 S enite Bedrock Assumed rock depth 1 MW-18A* 584658.688 1503258.693 579.31 581.81 2.5 26 553.31 NA NA 26 553.31 11 568.31 26 553.31 15 S enite*** PWR Assumed rock depth 1 MW-19* 585155.848 1503186.087 586.08 588.58 2.5 53 533.08 NA NA 53 533.08 25 561.08 40 546.08 15 Diorite*** PWR Assumed rock depth 1 MW-19A* 585155.848 1503186.087 586.17 588.07 1.9 71 515.17 NA NA 53 533.17 61 525.17 71 515.17 10 Diorite*** Bedrock Assumed rock depth 1 MW-20AR 586092.717 1503211.489 582.78 585.28 2.5 19.7 563.08 NA NA 9 573.78 8.3 574.48 18.3 564.48 10 Diorite*** Soil 1 MW-20B 586092.717 1503211.489 581.43 583.57 2.14 60 521.43 NA NA 11 570.43 45 536.43 60 521.43 15 Diorite*** Soil 1 MW-21 586674.371 1502868.591 579.43 581.99 2.56 20 559.43 7 572.43 20 559.43 10 569.43 20 559.43 10 Diorite*** PWR 1 MW-22 587314.247 1502996.856 583.71 586.21 2.5 13 570.71 NA NA 13 570.71 2.5 581.21 12.5 571.21 10 Diorite Soil 1 MW-22A c 587314.247 1502996.856 583.53 586.13 2.6 26 557.53 NA NA 15.5 568.03 21 562.53 26 557.53 5 Diorite Bedrock 4 MW-24* 585310.927 1504239.235 574.50 576.00 1.5 30 544.50 NA NA 30 544.50 20 554.50 30 544.50 10 S enite Soil/PWR Assumed rock depth 1 MW-25 587428.551 1502970.342 589.00 589.00 0 20.8 568.20 7 582.00 20.8 568.20 10.8 578.20 20.8 568.20 10 Diorite*** PWR 2 MW-26**** 585074.598 1505960.33 592.36 594.86 2.5 20 572.36 NA NA NA NA 5 587.36 20 572.36 15 Diorite Soil/PWR 2 MW-27**** 584646.73 1506060.422 578.82 581.32 2.5 12.5 566.32 NA NA NA NA 2.5 576.32 12.5 566.32 10 Diorite Soil 2 MW-28**** 583886.994 1506289.934 571.95 574.45 2.5 23 548.95 9 562.95 NA NA 8 563.95 20 551.95 12 Diorite Soil/PWR 3 MW-29R 583153.3 1506273.4 563.27 565.61 2.34 22.7 540.57 11 552.27 NA NA 5 558.28 20 543.27 15 Diorite Soil/PWR Assumed Diorite 3 MW-30R 583359.1 1504850.7 585.77 587.84 2.07 33.2 552.57 24.1 561.67 NA NA 18 567.77 33 552.77 15 Diorite Soil/PWR Assumed Diorite 2 MW-31**** 583669.983 1504988.978 589.76 592.26 2.5 30 559.76 12.5 577.26 NA NA 15 574.76 30 559.76 15 Diorite PWR 3 MW-32R 583967 1504900.4 585.36 587.80 2.44 28.5 556.86 13 572.36 NA NA 13.5 571.86 28.5 556.86 15 Diorite PWR Assumed Diorite 2 MW-33**** 584254.832 1504461.194 573.20 575.70 2.5 30.5 542.70 19.5 553.70 NA NA 15.5 557.70 30.5 542.70 15 Diorite Soil/PWR 2 MW-34**** 584444.191 1504280.597 575.21 577.71 2.5 30 545.21 16.5 558.71 NA NA 15 560.21 30 545.21 15 S enite S0il/PWR Nature -Extent MW-18AR 584566.7 1503436.E 577.61 579.93 2.32 42.2 535.41 23 554.61 23.7 553.91 32.3 545.31 42.2 535.41 10 Diorite Bedrock Nature -Extent MW-18R 584568.2 1503441.5 577.60 580.02 2.42 24 553.66 23 552.60 NA NA 9 568.60 24 553.60 15 Diorite Soil/PWR Nature -Extent MW-19AR 585080.3 1503080.9 580.09 582.82 2.73 52.7 527.39 NA NA 36.4 543.69 41 539.09 51 529.09 10 Diorite Bedrock Nature -Extent MW-19R 585077.1 1503087.8 580.17 582.53 2.36 35 545.17 NA NA NA NA 20 560.17 35 545.17 10 Diorite Soil/PWR Notes: msl - mean sea level bgs - below ground surface NA - not applicable *No logs can be located; Depths and screen interval from well tags or tables; lithology based on field observations. **Screen intervals estimated based on conventional practice at the time of the earlier investigation and nearby boring records. *** Litho/ogy assumed from soil description and/or field observation ****Ground elevation determined by subtracting 2.5 feet from surveyed well head data Boring numbers followed by "c" were cored. All information from this table is from Table 1 of the "Design Hydrogeologic Report, CMS Landfill V - Phase 3' prepared by David Garrett and Associates, dated May 2009 and approved by NCDENR on July 15, 2009, with the exception of wells MW-29R, MW-30R, MW-32R, MW-18AR, MW-18R, MW-19AR, and MW-19R from which the information was derived from the "Record of Monitoring Well Installations' dated January 13, 2011 by David Garrett & Associates. APPENDIX B STATISTICAL EVALUATIONS INTER -WELL PREDICTION LIMITS Prediction Limit Charlotte Motor Speedway Client: RSI Data: CMS Printed 11/12/2018, 4,42 PM Constituent Well Upper Lim. Lower Lim. Date Observ. S11c, Ba N Ba Mean Std. Dev. %NDs ND Ad. Barium Total (mg/L) MW-20B 0.38 n/a 10/2/2018 0.784 Yes 201 n/a n/a 18.41 We Cobalt Total (ug/L) MW-21 12 n/a 10/3/2018 1680 Yes 188 n/a n/a 62.23 n/a Cobalt Total (ug/L) MW-22 12 n/a 10/1/2018 52.9 Yes 188 n/a We 62.23 We Cobalt Total (ug/L) MW-22A 12 nla 10/1/2018 23 Yes 188 n/a n/a 62.23 nla Cobalt Total (ug/L) MW-213 12 n/a 10/1/2018 13.2 Yes 188 n/a n/a 62.23 We Cobalt Total (ug/L) MW-32R 12 We 10/2/2018 87.6 Yes 188 n/a We 62.23 We Nickel Total (ug/L) MW-21 43 n/a 10/3/2018 170 Yes 193 n/a n/a 38.34 n/a Nickel Total (ug/L) MW-22A 43 n/a 10/1/2018 126 Yes 193 n/a n/a 38.34 n/a Vanadium Total (ug/L) MW-21 33 n/a 10/3/2018 55.4 Yes 193 n/a We 27.46 n/a Transform Aloha Method n/a 0.00004896 NP Inter (normality) 1 of 2 n/a 0.00005574 NP Inter (NDs) 1 of 2 n/a 0.00005574 NP Inter (NDs) 1 of 2 n/a 0.00005574 NP Inter (NDs) 1 of 2 n/a 0.00005574 NP Inter (NDs) 1 of 2 n/a 0.00005574 NP Inter (NDs) 1 of 2 n/a 0.00005291 NP Inter (normality) 1 of 2 n/a 0.00005291 NP Inter (normality) 1 of 2 n/a 0.00005291 NP Inter (normality) 1 of 2 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. Exceeds Limit: MW-20B 1 W• 0.6 E ) 0.2 0 4- 1 /23/96 Prediction Limit Interwell Non -parametric 8/6/00 2/19/05 9/3/09 3/19/14 10/2/18 MW-20B Limit = 0.38 Non -parametric test used in lieu of parametric prediction limit because the Chi Squared normality test showed the data to be non -normal at the 0.01 alpha level. Limit is highest of 201 background values. 18.41 % NDs. Annual per - constituent alpha = 0.002543. Individual comparison alpha = 0.00004896 (1 of 2). Assumes 25 future values. Outlier test was not run because sample size exceeded table. Constituent: Barium Total Analysis Run 11/12/2018 4:40 PM Charlotte Motor Speedway Client: RSI Data: CMS Sanitas" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. Exceeds Limit: MW-213, MW-21, MW-22, MW-22A, MW-32R 2000 1600 1200 800 400 0 11 /17/93 Prediction Limit Interwell Non -parametric 11 /8/98 10/30/03 10/20/08 10/11 /13 10/3/18 ♦ MW-2B ■ MW-21 MW-22 ♦ MW-22A MW-32R Limit = 12 Non -parametric test used in lieu of parametric prediction limit because censored data exceeded 50%. Limit is highest of 188 background values. 62.23% NDs. Annual per -constituent alpha = 0.002894. Individual comparison alpha = 0.00005574 (1 of 2). Comparing 5 points to limit. Assumes 21 future values. Outlier test was not run because sample size exceeded table. Constituent: Cobalt Total Analysis Run 11/12/2018 4:39 PM Charlotte Motor Speedway Client: RSI Data: CMS Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. Exceeds Limit: MW-21, MW-22A J 7 200 160 120 0 1 /22/96 Prediction Limit Interwell Non -parametric 8/6/00 2/19/05 9/4/09 3/20/14 10/3/18 ■ M W-21 MW-22A Limit = 43 Non -parametric test used in lieu of parametric prediction limit because the Chi Squared normality test showed the data to be non -normal at the 0.01 alpha level. Limit is highest of 193 background values. 38.34% NDs. Annual per - constituent alpha = 0.002748. Individual comparison alpha = 0.00005291 (1 of 2). Comparing 2 points to limit. Assumes 24 future values. Outlier test was not run because sample size exceeded table. Constituent: Nickel Total Analysis Run 11/12/2018 4:41 PM Charlotte Motor Speedway Client: RSI Data: CMS Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. Exceeds Limit: MW-21 Prediction Limit Interwell Non -parametric 60 48 36 24 12 0 1 /22/96 8/6/00 2/19/05 9/4/09 3/20/14 10/3/18 ■ MW-21 Limit = 33 Non -parametric test used in lieu of parametric prediction limit because the Chi Squared normality test showed the data to be non -normal at the 0.01 alpha level. Limit is highest of 193 background values. 27.46% NDs. Annual per - constituent alpha = 0.002748. Individual comparison alpha = 0.00005291 (1 of 2). Assumes 25 future values. Outlier test was not run because sample size exceeded table. Constituent: Vanadium Total Analysis Run 11/12/2018 4:41 PM Charlotte Motor Speedway Client: RSI Data: CMS 1 /22/96 8/6/00 2/19/05 9/4/09 3/20/14 10/3/18 ■ MW-21 Limit = 33 Non -parametric test used in lieu of parametric prediction limit because the Chi Squared normality test showed the data to be non -normal at the 0.01 alpha level. Limit is highest of 193 background values. 27.46% NDs. Annual per - constituent alpha = 0.002748. Individual comparison alpha = 0.00005291 (1 of 2). Assumes 25 future values. Outlier test was not run because sample size exceeded table. Constituent: Vanadium Total Analysis Run 11/12/2018 4:41 PM Charlotte Motor Speedway Client: RSI Data: CMS INTRA-WELL CONFIDENCE LIMITS Confidence Interval Charlotte Motor Speedway Client: RSI Data: CMS Printed 11/13/2018, 10:03 AM Constituent Well Upper Lim. Lower Lim. Compliance Sic. N %NDs Transform Alpha Method Barium Total (mg/L) MW-20B 1.089 0.6341 0.7 No 4 0 In(x) 0.01 Param. Cobalt Total (ug/L) MW-2B 15.19 7.291 12 No 4 25 In(x) 0.01 Param. Cobalt Total (ug/L) MW-21 7127 10.73 12 No 4 0 In(x) 0.01 Param. Cobalt Total (ug/L) MW-22 242.6 22.02 12 Yes 4 0 In(x) 0.01 Param. Cobalt Total (ug/L) MW-22A 28.63 16.22 12 Yes 4 0 No 0.01 Param. Cobalt Total (ug/L) MW-32R 119.4 -24.46 12 No 4 0 No 0.01 Param. Nickel Total (ug/L) MW-21 273 13.81 100 No 4 25 In(x) 0.01 Param. Nickel Total (ug/L) MW-22A 137.4 91.61 100 No 4 0 No 0.01 Param. Vanadium Total (ug/L) MW-21 94.03 1.443 33 No 4 25 In(x) 0.01 Param. Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Parametric Confidence Interval Compliance Limit is not exceeded. Per -well alpha = 0.01. Normality Test: Shapiro Wilk, alpha based on n. 3 2.4 M 1.2 J 0) E 0.6 111 Constituent: Barium Total Analysis Run 11/13/2018 10:00 AM Charlotte Motor Speedway Client: RSI Data: CMS Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Parametric Confidence Interval Compliance limit is exceeded.* Per -well alpha = 0.01. Normality Test: Shapiro Wilk, alpha based on n. 9000 V0111I 5000 3000 J 1000 5IIIII4 =12 Constituent: Cobalt Total Analysis Run 11/13/2018 10:01 AM Charlotte Motor Speedway Client: RSI Data: CMS Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Parametric Confidence Interval Compliance Limit is not exceeded. Per -well alpha = 0.01. Normality Test: Shapiro Wilk, alpha based on n. 400 320 240 160 J 80 Constituent: Nickel Total Analysis Run 11/13/2018 10:02 AM Charlotte Motor Speedway Client: RSI Data: CMS Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Parametric Confidence Interval Compliance Limit is not exceeded. Per -well alpha = 0.01. Normality Test: Shapiro Wilk, alpha based on n. 150 120 M J 30 -----L+r-nit = 33 Constituent: Vanadium Total Analysis Run 11/13/2018 10:02 AM Charlotte Motor Speedway Client: RSI Data: CMS Confidence Interval Charlotte Motor Speedway Client: RSI Data: CMS Printed 11/13/2018, 10:11 AM Constituent Well Upper Lim. Lower Lim. Compliance Sig. N %NDs Transform Alpha Method 14-Dichlorobenzene (ug/L) MW-25 17.7 10.9 6 Yes 4 0 In(x) 0.01 Param. Benzene (ug/L) MW-18A 1.808 0.7923 1 No 4 25 No 0.01 Param. Benzene (ug/L) MW-33 5.154 -2.268 1 No 4 0 x^2 0.01 Param. Benzene (ug/L) MW-34 12.2 5.556 1 Yes 4 0 In(x) 0.01 Param. Benzene (ug/L) MW-32R 5.352 2.198 1 Yes 4 0 No 0.01 Param. Tetrachloroethylene (ug/L) MW-34 3 1 1 No 4 0 No 0.0625 NP (normality) Vinyl chloride (ug/L) MW-18A 2.9 1 1 No 4 75 No 0.0625 NP (normality) Vinyl chloride (ug/L) MW-33 3.964 2.436 1 Yes 4 0 No 0.01 Param. Vinyl chloride (ug/L) MW-34 3.47 1.23 1 Yes 4 0 No 0.01 Param. Vinyl chloride (ug/L) MW-32R 4.379 3.345 1 Yes 4 0 x^6 0.01 Param. Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Parametric Confidence Interval Compliance limit is exceeded. Per -well alpha = 0.01. Normality Test: Shapiro Wilk, alpha based on n. 30 24 Im 12 J 6 111 Constituent: 14-Dichlorobenzene Analysis Run 11/13/2018 10:08 AM Charlotte Motor Speedway Client: RSI Data: CMS Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Parametric Confidence Interval Compliance limit is exceeded.* Per -well alpha = 0.01. Normality Test: Shapiro Wilk, alpha based on n. 30 22 14 91 J -2 ��AGL '�pR GL r Constituent: Benzene Analysis Run 11/13/2018 10:09 AM Charlotte Motor Speedway Client: RSI Data: CMS Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG 4 3.2 2.4 1.6 J 0.8 111 Non -Parametric Confidence Interval Compliance Limit is not exceeded. Linnit= Constituent: Tetra chloroethylene Analysis Run 11/13/2018 10:09 AM Charlotte Motor Speedway Client: RSI Data: CMS Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Parametric and Non -Parametric (NP) Confidence Interval Compliance limit is exceeded.* Per -well alpha = 0.01 except as noted. Normality Test: Shapiro Wilk, alpha based on 6 W-111 3.6 2.4 J 1.2 Id Limil— �o r Q11 • 06, Constituent: Vinyl chloride Analysis Run 11/13/2018 10:10 AM Charlotte Motor Speedway Client: RSI Data: CMS TIME SERIES PLOTS Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 30 24 18 J 7 12 6 0 11 /17/93 Time Series 11 /8/98 10/30/03 10/20/08 10/11 /13 10/3/ 18 Constituent: Antimony Total Analysis Run 11/6/2018 1:24 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-11 MW-14 ♦ MW-14B MW-15 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 50 40 30 J 0) 7 20 10 0 4- 8/26/92 Time Series 11 /14/97 2/3/03 4/24/08 7/14/13 10/3/18 Constituent: Arsenic Total Analysis Run 11/13/2018 11:18 AM Charlotte Motor Speedway Client: RSI Data: CMS MW-11 MW-14 ♦ MW-14B MW-15 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. Time Series 0.5 0.4 0.3 J E 0.2 0.1 0 1 /29/92 5/30/97 9/30/02 1 /31 /08 6/2/13 10/3/18 Constituent: Barium Total Analysis Run 11/6/2018 1:24 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-11 MW-14 ♦ MW-14B MW-15 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 10 8 6 J 4 2 0 ! 11 /17/93 Time Series 11 /8/98 10/30/03 10/20/08 10/11 /13 10/3/18 Constituent: Beryllium Total Analysis Run 11/6/2018 1:24 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-11 MW-14 ♦ MW-14B MW-15 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. Time Series 0.01 0.008 0.006 J � s 0.004 0.002 0 CU�= kAA^AAAAAA&AA= 1 /29/92 5/30/97 9/30/02 1 /31 /08 6/2/13 10/3/18 Constituent: Cadmium Total Analysis Run 11/6/2018 1:24 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-11 MW-14 ♦ MW-14B MW-15 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 0.1 0.08 0.06 J E 0.04 c 0.02 0 1 /29/92 Time Series J , I 5/30/97 9/30/02 1 /31 /08 6/2/13 10/3/18 Constituent: Chromium Total Analysis Run 11/6/2018 1:24 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-11 MW-14 ♦ MW-14B MW-15 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. Time Series 50 40 30 J 7 20 10 0 11 /17/93 11 /8/98 10/30/03 10/20/08 10/11 /13 10/3/18 Constituent: Cobalt Total Analysis Run 11/6/2018 1:24 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-11 MW-14 ♦ MW-14B MW-15 11 /17/93 11 /8/98 10/30/03 10/20/08 10/11 /13 10/3/18 Constituent: Cobalt Total Analysis Run 11/6/2018 1:24 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-11 MW-14 ♦ MW-14B MW-15 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 0.4 0.32 0.24 J E 0.16 0.08 i 0 1 /29/92 Time Series 41 e - —' p 6. Q. . A� .1LAZ 5/30/97 9/30/02 1 /31 /08 6/2/13 10/3/18 Constituent: Copper Total Analysis Run 11/6/2018 1:24 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-11 MW-14 ♦ MW-14B MW-15 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. Time Series 20 16 12 J 4 8 I� 4 0 1 /29/92 5/30/97 9/30/02 1 /31 /08 6/2/13 10/3/18 Constituent: Lead Total Analysis Run 11/6/2018 1:24 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-11 MW-14 ♦ MW-14B MW-15 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 300 240 180 J 0) 7 120 60 0 11 /17/93 Time Series IF A 000/O/oAivp •• •. �, A , 11 /8/98 10/30/03 10/20/08 10/11 /13 10/3/ 18 Constituent: Nickel Total Analysis Run 11/6/2018 1:24 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-11 MW-14 ♦ MW-14B MW-15 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 50 40 30 J 0) 7 20 10 0 8/26/92 Time Series Cl/�AOd. O i 0. A 1 � 11 /14/97 2/3/03 4/24/08 7/14/13 10/3/18 Constituent: Selenium Total Analysis Run 11/6/2018 1:24 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-11 MW-14 ♦ MW-14B MW-15 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 0.03 0.024 0.018 J 0) E 0.012 0.006 0 8/26/92 Time Series 11 /14/97 2/3/03 4/24/08 7/14/13 10/3/18 Constituent: Silver Total Analysis Run 11/6/2018 1:24 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-11 MW-14 ♦ MW-14B MW-15 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 10 8 6 J 0) Z3 4 2 0 11 /17/93 Time Series 11 /8/98 10/30/03 10/20/08 10/11 /13 10/3/ 18 Constituent: Thallium Total Analysis Run 11/6/2018 1:24 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-11 MW-14 ♦ MW-14B MW-15 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 200 160 120 J 0) 7 80 40 i 0 11 /17/93 Time Series CK 11 /8/98 10/30/03 10/20/08 10/11 /13 10/3/ 18 Constituent: Vanadium Total Analysis Run 11/6/2018 1:24 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-11 MW-14 ♦ MW-14B MW-15 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 0.7 0.56 0.42 J t� E 0.28 0.14 i 0 1 /29/92 Time Series . • a vavav� v�vadOd\ve. von F ♦ - dW�- r . �r�. 5/30/97 9/30/02 1 /31 /08 6/2/13 10/3/18 Constituent: Zinc Total Analysis Run 11/6/2018 1:24 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-11 MW-14 ♦ MW-14B MW-15 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 30 24 18 J 7 12 6 0 ! 11 /17/93 Time Series n 11 /8/98 10/30/03 10/20/08 10/11 /13 10/3/18 Constituent: Antimony Total Analysis Run 11/8/2018 9:35 AM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-10 ■ MW-10A ♦ MW-12 ♦ MW-1A ■ MW-1 B • MW-2A ♦ MW-2B ■ MW-21 • MW-22 ♦ MW-22A MW-25 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. Time Series 50 40 30 J 0) 7 20 10 0 8/26/92 11 /14/97 2/3/03 4/24/08 7/14/13 10/3/18 Constituent: Arsenic Total Analysis Run 11/13/2018 11:18 AM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-10 ■ MW-10A ♦ MW-12 ♦ MW-1A ■ MW-1 B • MW-2A ♦ MW-2B ■ MW-21 • MW-22 ♦ MW-22A MW-25 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 2 1.6 1.2 J 0) E 0.8 0.4 1 /29/92 Time Series 5/30/97 9/30/02 1 /31 /08 6/2/13 10/3/18 Constituent: Barium Total Analysis Run 11/8/2018 9:35 AM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-10 ■ MW-10A ♦ MW-12 ♦ MW-1A ■ MW-1 B • MW-2A ♦ MW-2B ■ MW-21 • MW-22 ♦ MW-22A MW-25 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. Time Series 10 8 6 J 7 4 2 114, 0 11 /17/93 11 /8/98 10/30/03 10/20/08 10/11 /13 10/3/18 Constituent: Beryllium Total Analysis Run 11/8/2018 9:35 AM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-10 ■ MW-10A ♦ MW-12 ♦ MW-1A ■ MW-1 B • MW-2A ♦ MW-2B ■ MW-21 • MW-22 ♦ MW-22A MW-25 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 1 /29/92 Time Series 5/30/97 9/30/02 1/31/08 6/2/13 10/3/18 Constituent: Cadmium Total Analysis Run 11/8/2018 9:35 AM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-10 ■ MW-10A ♦ MW-12 ♦ MW-1A ■ MW-1 B • MW-2A ♦ MW-2B ■ MW-21 • MW-22 ♦ MW-22A MW-25 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 0.3 0.24 0.18 J 0) E 0.12 0.06 1 /29/92 Time Series /1s■9AA'A ���'�'�"�n��!�`���!1`�L:..: oJ:.�..�G...:�J.. — ___ r �t it It , 5/30/97 9/30/02 1 /31 /08 6/2/13 10/3/18 Constituent: Chromium Total Analysis Run 11/8/2018 9:35 AM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-10 ■ MW-10A ♦ MW-12 ♦ MW-1A ■ MW-1 B • MW-2A ♦ MW-2B ■ MW-21 • MW-22 ♦ MW-22A ♦ MW-25 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 2000 1600 1200 J 7 800 400 11 /17/93 Time Series 11 /8/98 10/30/03 10/20/08 10/11 /13 10/3/18 Constituent: Cobalt Total Analysis Run 11/8/2018 9:35 AM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-10 ■ MW-10A ♦ MW-12 ♦ MW-1A ■ MW-1 B MW-2A ♦ MW-2B ■ MW-21 • MW-22 ♦ MW-22A MW-25 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 0.7 0.56 0.42 J 0) E 0.28 0.14 1 /29/92 Time Series 5/30/97 9/30/02 1 /31 /08 6/2/13 10/3/18 Constituent: Copper Total Analysis Run 11/8/2018 9:35 AM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-10 ■ MW-10A ♦ MW-12 ♦ MW-1A ■ MW-1 B MW-2A ♦ MW-2B ■ MW-21 • MW-22 ♦ MW-22A MW-25 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 110 88 66 J 7 44 22 0 4- 1 /29/92 Time Series 5/30/97 9/30/02 1 /31 /08 6/2/13 10/3/18 Constituent: Lead Total Analysis Run 11/8/2018 9:35 AM Charlotte Motor Speedway Client: RSI Data: CMS MW-10 MW-10A MW-12 MW-1A MW-1 B MW-2A MW-2B M W-21 MW-22 MW-22A MW-25 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 200 160 120 J 7 80 40 0 11 /17/93 Time Series 11 /8/98 10/30/03 10/20/08 10/11 /13 10/3/ 18 Constituent: Nickel Total Analysis Run 11/8/2018 9:35 AM Charlotte Motor Speedway Client: RSI Data: CMS MW-10 MW-10A MW-12 MW-1A MW-1 B MW-2A MW-2B M W-21 MW-22 MW-22A MW-25 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. Time Series 50 40 30 J 0) 7 20 10 kwyyyyyyyl 8/26/92 11 /14/97 2/3/03 4/24/08 7/14/13 10/3/18 Constituent: Selenium Total Analysis Run 11/8/2018 9:35 AM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-10 ■ MW-10A ♦ MW-12 ♦ MW-1A ■ MW-1 B • MW-2A ♦ MW-2B ■ MW-21 • MW-22 ♦ MW-22A MW-25 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 0.03 0.024 0.018 J 0) E 0.012 0.006 0 8/26/92 Time Series 11 /14/97 2/3/03 4/24/08 7/14/13 10/3/18 Constituent: Silver Total Analysis Run 11/8/2018 9:35 AM Charlotte Motor Speedway Client: RSI Data: CMS MW-10 MW-10A MW-12 MW-1A MW-1 B MW-2A MW-2B M W-21 MW-22 MW-22A MW-25 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 20 16 12 J 0) Z3 8 4 0 ! 11 /17/93 Time Series 11 /8/98 10/30/03 10/20/08 10/11 /13 10/3/18 Constituent: Thallium Total Analysis Run 11/8/2018 9:35 AM Charlotte Motor Speedway Client: RSI Data: CMS MW-10 MW-10A MW-12 MW-1A MW-1 B MW-2A MW-2B M W-21 MW-22 MW-22A MW-25 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 80 64 48 J 7 32 16 0 11 /17/93 Time Series 11 /8/98 10/30/03 10/20/08 10/11 /13 10/3/ 18 Constituent: Vanadium Total Analysis Run 11/8/2018 9:35 AM Charlotte Motor Speedway Client: RSI Data: CMS MW-10 MW-10A MW-12 MW-1A MW-1 B MW-2A MW-2B M W-21 MW-22 MW-22A MW-25 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 0.4 0.32 0.24 J E 0.16 0.08 1 /29/92 Time Series 5/30/97 9/30/02 1 /31 /08 6/2/13 10/3/18 Constituent: Zinc Total Analysis Run 11/8/2018 9:35 AM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-10 ■ MW-10A ♦ MW-12 ♦ MW-1A ■ MW-1 B • MW-2A ♦ MW-2B ■ MW-21 • MW-22 ♦ MW-22A MW-25 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 30 24 18 J a� 12 6 0 4- 1 /23/96 Time Series 8/6/00 2/19/05 9/4/09 3/20/14 10/3/18 Constituent: Antimony Total Analysis Run 11/6/2018 1:38 PM Charlotte Motor Speedway Client: RSI Data: CMS • MW-20B ♦ MW-20AR ♦ MW-19 ♦ MW-19A ■ MW-18AR • MW-19AR ♦ MW-19R Sanitas'"v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. J 0) Z3 10 8 I: 4 2 0 1 /23/96 Time Series 7-1- "r inn (YU lvl� 1► 8/6/00 2/19/05 9/4/09 3/20/14 10/3/18 Constituent: Arsenic Total Analysis Run 11/13/2018 11:19 AM Charlotte Motor Speedway Client: RSI Data: CMS • MW-20B ♦ MW-20AR MW-19 ♦ MW-19A ■ MW-18AR • MW-19AR ♦ MW-19R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 2 1.6 1.2 J 0) E 0.8 0.4 0 1 /23/96 Time Series 8/6/00 2/19/05 9/4/09 3/20/14 10/3/18 Constituent: Barium Total Analysis Run 11/6/2018 1:38 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-20B MW-20AR MW-19 MW-19A MW-18AR MW-19AR MW-19R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. Time Series 5 4 3 41 J 2 1 IM 0 1 /23/96 8/6/00 2/19/05 9/4/09 3/20/14 10/3/18 Constituent: Beryllium Total Analysis Run 11/6/2018 1:38 PM Charlotte Motor Speedway Client: RSI Data: CMS • MW-20B ♦ MW-20AR ♦ MW-19 ♦ MW-19A ■ MW-18AR • MW-19AR ♦ MW-19R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 0.01 0.008 0.006 J a E 0.004 0.002 0 1 /23/96 Time Series 8/6/00 2/19/05 9/4/09 3/20/14 10/3/18 Constituent: Cadmium Total Analysis Run 11/6/2018 1:38 PM Charlotte Motor Speedway Client: RSI Data: CMS • MW-20B ♦ MW-20AR ♦ MW-19 ♦ MW-19A ■ MW-18AR • MW-19AR ♦ MW-19R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 0.2 0.16 0.12 J 0) E 0.08 0.04 0 1 /23/96 Time Series 8/6/00 2/19/05 9/4/09 3/20/14 10/3/18 Constituent: Chromium Total Analysis Run 11/6/2018 1:38 PM Charlotte Motor Speedway Client: RSI Data: CMS • MW-20B ♦ MW-20AR MW-19 ♦ MW-19A ■ MW-18AR • MW-19AR ♦ MW-19R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 80 64 48 J a� 32 16 c 0 1 /23/96 Time Series 8/6/00 2/19/05 9/4/09 3/20/14 • MW-20B ♦ MW-20AR MW-19 ♦ MW-19A ■ MW-18AR • MW-19AR ♦ i MW-19R 10/3/18 Constituent: Cobalt Total Analysis Run 11/6/2018 1:38 PM Charlotte Motor Speedway Client: RSI Data: CMS Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. Time Series 0.3 0.24 0.18 J 0) E 0.12 0.06 0 • MW-20B ♦ MW-20AR ♦ MW-19 ♦ MW-19A ■ MW-18AR • MW-19AR ♦ MW-19R 1 /23/96 8/6/00 2/19/05 9/4/09 3/20/14 10/3/18 Constituent: Copper Total Analysis Run 11/6/2018 1:38 PM Charlotte Motor Speedway Client: RSI Data: CMS Sanitas'"v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 10 8 6 J 4 2 0 1 /23/96 Time Series 8/6/00 2/19/05 9/4/09 3/20/14 10/3/ 18 Constituent: Lead Total Analysis Run 11/6/2018 1:38 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-20B MW-20AR MW-19 MW-19A MW-18AR MW-19AR MW-19R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 200 160 120 J 0) 80 40 0 1 /23/96 Time Series TY v) i r � ivy 8/6/00 2/19/05 9/4/09 3/20/14 10/3/18 Constituent: Nickel Total Analysis Run 11/6/2018 1:38 PM Charlotte Motor Speedway Client: RSI Data: CMS • MW-20B ♦ MW-20AR ♦ MW-19 ♦ MW-19A ■ MW-18AR • MW-19AR ♦ MW-19R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 30 24 18 J a� 12 6 0 1 /23/96 Time Series f � • MW-20B ♦ MW-20AR ♦ MW-19 ♦ MW-19A ■ MW-18AR • MW-19AR I ♦ MW-19R 8/6/00 2/19/05 9/4/09 3/20/14 10/3/18 Constituent: Selenium Total Analysis Run 11/6/2018 1:38 PM Charlotte Motor Speedway Client: RSI Data: CMS Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 0.2 0.16 0.12 J E 0.08 0.04 0 1 /23/96 Time Series ri n � �� �➢0 �� � AFT � r lDQr �DQ � � r 8/6/00 2/19/05 9/4/09 3/20/14 10/3/18 Constituent: Silver Total Analysis Run 11/6/2018 1:38 PM Charlotte Motor Speedway Client: RSI Data: CMS • MW-20B ♦ MW-20AR ♦ MW-19 ♦ MW-19A ■ MW-18AR • MW-19AR ♦ MW-19R Sanitas'"v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 10 8 6 J 4 2 Time Series 0 1 /23/96 • MW-20B ♦ MW-20AR ♦ MW-19 ♦ MW-19A ■ MW-18AR 1 MW-19AR ♦ MW-19R 8/6/00 2/19/05 9/4/09 3/20/14 10/3/18 Constituent: Thallium Total Analysis Run 11/6/2018 1:38 PM Charlotte Motor Speedway Client: RSI Data: CMS Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 80 64 48 J a� 32 16 0 1 /23/96 Time Series 8/6/00 2/19/05 9/4/09 3/20/14 iflUffE:1 Constituent: Vanadium Total Analysis Run 11/6/2018 1:38 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-20B MW-20AR MW-19 MW-19A MW-18AR MW-19AR MW-19R Sanitas'"v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 40 32 24 J E 16 8 1 /23/96 Time Series 8/6/00 2/19/05 9/4/09 3/20/14 10/3/18 Constituent: Zinc Total Analysis Run 11/6/2018 1:38 PM Charlotte Motor Speedway Client: RSI Data: CMS • MW-20B ♦ MW-20AR ♦ MW-19 ♦ MW-19A ■ MW-18AR • MW-19AR MW-19R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 30 24 18 J 7 12 6 0 ! 11 /19/97 Time Series 1 /23/02 3/29/06 6/2/10 8/6/14 10/11 /18 Constituent: Antimony Total Analysis Run 11/6/2018 1:42 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-17 MW-17A MW-24 M W-31 MW-33 M W-34 MW-30R MW-32R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 20 16 12 J 0) Z3 8 4 0 ! 11 /19/97 Time Series 1 /23/02 3/29/06 6/2/10 8/6/14 10/11 /18 Constituent: Arsenic Total Analysis Run 11/13/2018 11:20 AM Charlotte Motor Speedway Client: RSI Data: CMS MW-17 MW-17A MW-24 MW-31 MW-33 M W-34 MW-30R MW-32R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 2 1.6 1.2 J 0) E 0.8 0.4 0 11 /19/97 Time Series 1 /23/02 3/29/06 6/2/10 8/6/14 10/11 /18 Constituent: Barium Total Analysis Run 11/6/2018 1:42 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-17 MW-17A MW-24 MW-31 MW-33 M W-34 MW-30R MW-32R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. Time Series 5 4 3 J 7 2 1 0 11 /19/97 1 /23/02 3/29/06 6/2/10 8/6/14 10/11 /18 Constituent: Beryllium Total Analysis Run 11/6/2018 1:42 PM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-17 ■ MW-17A • MW-24 • MW-31 ♦ MW-33 ♦ MW-34 ♦ MW-30R ■ MW-32R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 0.005 0.004 0.003 J 0) E 0.002 0.001 11 /19/97 Time Series 1 /23/02 3/29/06 6/2/10 8/6/14 10/11 /18 Constituent: Cadmium Total Analysis Run 11/6/2018 1:42 PM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-17 ■ MW-17A • MW-24 • MW-31 ♦ MW-33 ♦ MW-34 ♦ MW-30R ■ MW-32R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 0.7 0.56 0.42 J 0) E 0.28 0.14 11 /19/97 Time Series 1 /23/02 3/29/06 6/2/10 8/6/14 10/11 /18 Constituent: Chromium Total Analysis Run 11/6/2018 1:42 PM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-17 ■ MW-17A • MW-24 • MW-31 ♦ MW-33 ♦ MW-34 ♦ MW-30R ■ MW-32R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 90 72 54 J 0) 7 36 18 11 /19/97 Time Series 1 /23/02 3/29/06 6/2/10 8/6/14 10/11 /18 Constituent: Cobalt Total Analysis Run 11/6/2018 1:42 PM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-17 ■ MW-17A • MW-24 • MW-31 ♦ MW-33 ♦ MW-34 ♦ MW-30R ■ MW-32R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 0.2 0.16 0.12 J 0) E 0.08 0.04 11 /19/97 Time Series 1 /23/02 3/29/06 6/2/10 8/6/14 10/11 /18 Constituent: Copper Total Analysis Run 11/6/2018 1:42 PM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-17 ■ MW-17A • MW-24 • MW-31 ♦ MW-33 ♦ MW-34 ♦ MW-30R ■ MW-32R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 200 160 120 J 0) 7 80 40 11 /19/97 Time Series 1 /23/02 3/29/06 6/2/10 8/6/14 10/11 /18 Constituent: Lead Total Analysis Run 11/6/2018 1:42 PM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-17 ■ MW-17A • MW-24 • MW-31 ♦ MW-33 ♦ MW-34 ♦ MW-30R ■ MW-32R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 300 240 180 J 0) 7 120 60 11/19/97 Time Series 1 /23/02 3/29/06 6/2/10 8/6/14 10/11 /18 Constituent: Nickel Total Analysis Run 11/6/2018 1:42 PM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-17 ■ MW-17A • MW-24 • MW-31 ♦ MW-33 ♦ MW-34 ♦ MW-30R ■ MW-32R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 30 24 18 J 7 12 6 0 ! 11 /19/97 Time Series 1 /23/02 3/29/06 6/2/10 8/6/14 10/11 /18 Constituent: Selenium Total Analysis Run 11/6/2018 1:42 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-17 MW-17A MW-24 MW-31 MW-33 M W-34 MW-30R MW-32R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. Time Series 0.01 0.008 0.006 J E 0.004 0.002 Kelm =1111 11 /19/97 1 /23/02 3/29/06 6/2/10 8/6/14 10/11 /18 Constituent: Silver Total Analysis Run 11/6/2018 1:42 PM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-17 ■ MW-17A • MW-24 • MW-31 ♦ MW-33 ♦ MW-34 ♦ MW-30R ■ MW-32R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 20 16 12 J 7 8 4 0 ! 11 /19/97 Time Series 1 /23/02 3/29/06 6/2/10 8/6/14 10/11 /18 Constituent: Thallium Total Analysis Run 11/6/2018 1:42 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-17 MW-17A MW-24 MW-31 MW-33 M W-34 MW-30R MW-32R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 200 160 120 J 0) Z3 80 40 0 11 /19/97 Time Series 1 /23/02 3/29/06 6/2/10 8/6/14 10/11 /18 Constituent: Vanadium Total Analysis Run 11/6/2018 1:42 PM Charlotte Motor Speedway Client: RSI Data: CMS MW-17 MW-17A MW-24 MW-31 MW-33 M W-34 MW-30R MW-32R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 1 0.8 0.6 J 0) E 0.4 0.2 11 /19/97 Time Series 1 /23/02 3/29/06 6/2/10 8/6/14 10/11 /18 Constituent: Zinc Total Analysis Run 11/6/2018 1:42 PM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-17 ■ MW-17A • MW-24 • MW-31 ♦ MW-33 ♦ MW-34 ♦ MW-30R ■ MW-32R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 20 16 12 J 7 8 4 0 4- 6/11 /07 Time Series 9/14/09 12/19/11 3/25/14 6/28/16 10/3/18 Constituent: Antimony Total Analysis Run 11/6/2018 1:55 PM Charlotte Motor Speedway Client: RSI Data: CMS ■ MW-16 • MW-26 ♦ MW-27 ♦ MW-28 ♦ MW-29R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 50 40 30 J 0) 7 20 10 0 4- 6/11 /07 Time Series 9/14/09 12/19/11 3/25/14 6/28/16 10/3/18 Constituent: Arsenic Total Analysis Run 11/13/2018 11:20 AM Charlotte Motor Speedway Client: RSI Data: CMS ■ MW-16 • MW-26 ♦ MW-27 ♦ MW-28 ♦ MW-29R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. Time Series 0.8 0.64 0.48 J E 0.32 0.16 0 6/11 /07 9/14/09 12/19/11 3/25/14 6/28/16 10/3/18 Constituent: Barium Total Analysis Run 11/6/2018 1:55 PM Charlotte Motor Speedway Client: RSI Data: CMS ■ MW-16 • MW-26 ♦ MW-27 ♦ MW-28 r MW-29R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 3 2.4 1.8 J 0) Z3 1.2 0.6 0 4- 6/11 /07 Time Series 6 1 ! 1 4 r xs zs LA IF 9/14/09 12/19/11 3/25/14 6/28/16 10/3/18 Constituent: Beryllium Total Analysis Run 11/6/2018 1:55 PM Charlotte Motor Speedway Client: RSI Data: CMS ■ MW-16 • MW-26 ♦ MW-27 ♦ MW-28 ♦ MW-29R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 0.0011 0.00088 0.00066 J 0) E 0.00044 0.00022 0 4- 6/11 /07 Time Series 9/14/09 12/19/11 3/25/14 6/28/16 10/3/18 Constituent: Cadmium Total Analysis Run 11/6/2018 1:55 PM Charlotte Motor Speedway Client: RSI Data: CMS ■ MW-16 • MW-26 ♦ MW-27 ♦ MW-28 r MW-29R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 0.4 0.32 0.24 J 0) E 0.16 0.08 0 91ha— 6/11 /07 Time Series 9/14/09 12/19/11 3/25/14 6/28/16 10/3/18 Constituent: Chromium Total Analysis Run 11/6/2018 1:55 PM Charlotte Motor Speedway Client: RSI Data: CMS ■ MW-16 • MW-26 ♦ MW-27 ♦ MW-28 ♦ MW-29R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 200 160 120 J 0) Z3 80 40 0 q-- 6/11 /07 Time Series 9/14/09 12/19/11 3/25/14 6/28/16 10/3/18 Constituent: Cobalt Total Analysis Run 11/6/2018 1:55 PM Charlotte Motor Speedway Client: RSI Data: CMS ■ MW-16 • MW-26 ♦ MW-27 ♦ MW-28 ♦ MW-29R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. Time Series 0.5 0.4 0.3 J E 0.2 0.1 0 6/11 /07 9/14/09 12/19/11 3/25/14 6/28/16 10/3/18 Constituent: Copper Total Analysis Run 11/6/2018 1:56 PM Charlotte Motor Speedway Client: RSI Data: CMS ■ MW-16 • MW-26 ♦ MW-27 ♦ MW-28 r MW-29R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 50 40 30 J 7 20 10 0 4- 6/11 /07 Time Series 9/14/09 12/19/11 3/25/14 6/28/16 10/3/18 Constituent: Lead Total Analysis Run 11/6/2018 1:56 PM Charlotte Motor Speedway Client: RSI Data: CMS ■ MW-16 • MW-26 ♦ MW-27 ♦ MW-28 ♦ MW-29R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 600 480 360 J 7 240 120 0 -PQL-- 6/11 /07 Time Series 9/14/09 12/19/11 3/25/14 6/28/16 10/3/18 Constituent: Nickel Total Analysis Run 11/6/2018 1:56 PM Charlotte Motor Speedway Client: RSI Data: CMS ■ MW-16 • MW-26 ♦ MW-27 ♦ MW-28 ♦ MW-29R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 50 40 30 J 0) Z3 20 10 0 4- 6/11 /07 Time Series 9/14/09 12/19/11 3/25/14 6/28/16 10/3/18 Constituent: Selenium Total Analysis Run 11/6/2018 1:56 PM Charlotte Motor Speedway Client: RSI Data: CMS ■ MW-16 • MW-26 ♦ MW-27 ♦ MW-28 ♦ MW-29R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 0.02 0.016 0.012 J E 0.008 0.004 0 4- 6/11 /07 Time Series 9/14/09 12/19/11 3/25/14 6/28/16 10/3/18 Constituent: Silver Total Analysis Run 11/6/2018 1:56 PM Charlotte Motor Speedway Client: RSI Data: CMS ■ MW-16 • MW-26 ♦ MW-27 ♦ MW-28 ♦ MW-29R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 10 8 6 J 4 2 0 4- 6/11 /07 Time Series 9/14/09 12/19/11 3/25/14 6/28/16 10/3/18 Constituent: Thallium Total Analysis Run 11/6/2018 1:56 PM Charlotte Motor Speedway Client: RSI Data: CMS ■ MW-16 • MW-26 ♦ MW-27 ♦ MW-28 MW-29R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 400 320 240 J 7 160 80 0 *d-- 6/11/07 Time Series 9/14/09 12/19/11 3/25/14 6/28/16 10/3/18 Constituent: Vanadium Total Analysis Run 11/6/2018 1:56 PM Charlotte Motor Speedway Client: RSI Data: CMS ■ MW-16 • MW-26 ♦ MW-27 ♦ MW-28 MW-29R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 0.3 0.24 0.18 J 0) E 0.12 0.06 0 4- 6/11 /07 Time Series 9/14/09 12/19/11 3/25/14 6/28/16 10/3/18 Constituent: Zinc Total Analysis Run 11/6/2018 1:56 PM Charlotte Motor Speedway Client: RSI Data: CMS ■ MW-16 • MW-26 ♦ MW-27 ♦ MW-28 r MW-29R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 20 16 12 J 0) Z3 8 4 0 1 /23/96 Time Series J �Y 8/6/00 2/19/05 9/4/09 3/20/14 10/3/18 Constituent: 14-Dichlorobenzene Analysis Run 11/13/2018 11:11 AM Charlotte Motor Speedway Client: RSI Data: CMS MW-20B MW-19 MW-25 ♦ MW-34 MW-19AR ♦ MW-19R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 10 8 6 J 7 4 2 0 4- 1 /19/99 Time Series 12/29/02 12/9/06 11 /19/10 10/30/14 10/10/18 Constituent: Benzene Analysis Run 11/13/2018 11:12 AM Charlotte Motor Speedway Client: RSI Data: CMS MW-33 ♦ MW-34 ■ MW-32R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 20 16 12 J 0) Z3 8 4 0 4- 6/6/02 Time Series 9/10/05 12/16/08 3/22/12 6/28/15 10/3/18 Constituent: Chlorobenzene Analysis Run 11/13/2018 11:12 AM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-25 MW-19AR * MW-19R Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 20 16 12 J 7 8 4 0 4- 6/11 /07 Time Series 9/15/09 12/22/11 3/29/14 7/4/16 10/10/18 ♦ MW-33 ♦ MW-34 Constituent: cis- 1 2-Dichloroethylene Analysis Run 11/13/2018 11:13 AM Charlotte Motor Speedway Client: RSI Data: CMS Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 5 4 3 J 7 2 1 0 4- 6/11 /07 Time Series 9/15/09 12/22/11 3/29/14 7/4/16 10/10/18 Constituent: Methylene chloride Analysis Run 11/13/2018 11:13 AM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-33 ♦ MW-34 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 3 2.4 1.8 J 0) Z3 1.2 0.6 0 4- 6/11 /07 Time Series 9/15/09 12/22/11 3/29/14 7/4/16 10/10/18 Constituent: Tetra chloroethylene Analysis Run 11/13/2018 11:13 AM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-33 ♦ MW-34 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 2 1.6 1.2 J 0.8 0.4 0 4- 6/11 /07 Time Series 9/15/09 12/22/11 3/29/14 7/4/16 10/10/18 Constituent: Trichloroethylene Analysis Run 11/13/2018 11:14 AM Charlotte Motor Speedway Client: RSI Data: CMS ♦ MW-33 ♦ MW-34 Sanitas'" v.9.6.10 Software licensed to Jett Environmental Consulting. UG Hollow symbols indicate censored values. 10 8 6 J 7 4 2 0 4- 1 /19/99 Time Series 12/29/02 12/9/06 11 /19/10 10/30/14 10/10/18 Constituent: Vinyl chloride Analysis Run 11/13/2018 11:14 AM Charlotte Motor Speedway Client: RSI Data: CMS MW-33 ♦ MW-34 ■ MW-32R APPENDIX C LABORATORY ANALYTICAL REPORTS FIELD INFORMATION FORMS aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 November 07, 2018 Environmental Manager BFI Waste Systems of North America. LLC 5105 Moreland Road Concord, NC 28027 RE: Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Dear Environmental Manager: Enclosed are the analytical results for sample(s) received by the laboratory on October 04, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. This revised report replaces the report issued on October 30, 2018. The report has been revised to remove the Well Integrity Forms per consultant request. No other changes have been made to this report. If you have any questions concerning this report, please feel free to contact me. Sincerely, 8 -,,-Y?0 Betsy McDaniel betsy.mcdaniel@pacelabs.com (770)734-4200 Project Manager Enclosures cc: Database Manager REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Atlanta Certification IDs 110 Technology Parkway Peachtree Corners, GA 30092 Florida DOH Certification #: E87315 Georgia DW Inorganics Certification #: 812 Georgia DW Microbiology Certification #: 812 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 CERTIFICATIONS North Carolina Certification #: 381 South Carolina Certification #: 98011001 Texas Certification #: T104704397-08-TX Virginia Certification #: 460204 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 SAMPLE SUMMARY Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Lab ID Sample ID Matrix Date Collected Date Received 2610107001 1304-MW1A Water 10/01/18 14:44 10/04/18 08:00 2610107002 1304-MW1B Water 10/01/1815:39 10/04/18 08:00 2610107003 1304-MW2A Water 10/01/18 15:31 10/04/18 08:00 2610107004 1304-MW2B Water 10/01/18 16:00 10/04/18 08:00 2610107005 1304-MW10 Water 10/02/18 15:08 10/04/18 08:00 2610107006 1304-MW10A Water 10/02/18 16:28 10/04/18 08:00 2610107007 1304-MW11 Water 10/02/18 08:58 10/04/18 08:00 2610107008 1304-MW12 Water 10/02/18 08:29 10/04/18 08:00 2610107009 1304-MW14 Water 10/02/18 09:19 10/04/18 08:00 2610107010 1304-MW14B Water 10/03/18 08:55 10/04/18 08:00 2610107011 1304-MW15 Water 10/02/18 10:11 10/04/18 08:00 2610107012 1304-MW16 Water 10/02/18 11:00 10/04/18 08:00 2610107013 1304-MW18A Water 10/02/18 14:19 10/04/18 08:00 2610107014 1304-MW19 Water 10/03/18 12:15 10/04/18 08:00 2610107015 1304-MW19A Water 10/03/18 13:18 10/04/18 08:00 2610107016 1304-MW19AR Water 10/03/18 11:15 10/04/18 08:00 2610107017 1304-MW19R Water 10/03/18 10:54 10/04/18 08:00 2610107018 1304-MW20AR Water 10/02/18 14:00 10/04/18 08:00 2610107019 1304-MW20B Water 10/02/18 14:49 10/04/18 08:00 2610107020 1304-MW21 Water 10/03/18 10:14 10/04/18 08:00 2610107021 1304-MW22 Water 10/01/18 12:50 10/04/18 08:00 2610107022 1304-MW22A Water 10/01/18 13:25 10/04/18 08:00 2610107023 1304-MW25 Water 10/01/18 13:58 10/04/18 08:00 2610107024 1304-MW26 Water 10/02/18 11:41 10/04/18 08:00 2610107025 1304-MW27 Water 10/03/18 09:24 10/04/18 08:00 2610107026 1304-MW28 Water 10/02/18 12:16 10/04/18 08:00 2610107027 1304-MW29R Water 10/02/18 15:26 10/04/18 08:00 2610107028 1304-MW30R Water 10/02/18 09:30 10/04/18 08:00 2610107029 1304-MW31 Water 10/02/18 10:04 10/04/18 08:00 2610107030 1304-MW32R Water 10/02/18 11:00 10/04/18 08:00 2610107032 1304-MW34 Water 10/02/18 13:34 10/04/18 08:00 2610107033 1304-Trip Day 1 Water 10/01/18 00:00 10/04/18 08:00 2610107034 1304-Duplicate Water 10/02/18 00:00 10/04/18 08:00 2610107035 1304-Equip Blank Water 10/04/18 06:11 10/04/18 08:00 2610107036 1304-SW2 Water 10/03/18 07:40 10/04/18 08:00 2610107037 1304-SW1 Water 10/03/18 08:05 10/04/18 08:00 2610107038 1304-Field Blank Water 10/03/18 09:27 10/04/18 08:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 SAMPLE ANALYTE COUNT Project: Pace Project No.: Charlotte Motor Speedway V LF 2610107 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 2610107001 1304-MW1A EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E JHG 51 PASI-GA 2610107002 1304-MW1B EPA6020B CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E JHG 51 PASI-GA 2610107003 1304-MW2A EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E JHG 51 PASI-GA 2610107004 1304-MW2B EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E JHG 51 PASI-GA 2610107005 1304-MW10 EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E RAC 51 PASI-GA 2610107006 1304-MW10A EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E RAC 51 PASI-GA 2610107007 1304-MW11 EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E RAC 51 PASI-GA 2610107008 1304-MW12 EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E RAC 51 PASI-GA 2610107009 1304-MW14 EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E RAC 51 PASI-GA 2610107010 1304-MW14B EPA 6020E CSW 15 PASI-GA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 SAMPLE ANALYTE COUNT Project: Pace Project No.: Charlotte Motor Speedway V LF 2610107 Analytes Lab ID Sample ID Method Analysts Reported Laboratory EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E RAC 51 PASI-GA 2610107011 1304-MW15 EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E RAC 51 PASI-GA 2610107012 1304-MW16 EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E RAC 51 PASI-GA 2610107013 1304-MW18A EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E RAC 51 PASI-GA 2610107014 1304-MW19 EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E JHG 51 PASI-GA 2610107015 1304-MW19A EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260B LIH 51 PASI-GA 2610107016 1304-MW19AR EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260B LIH 51 PASI-GA 2610107017 1304-MW19R EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E JHG 51 PASI-GA 2610107018 1304-MW20AR EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E RAC 51 PASI-GA 2610107019 1304-MW20B EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 SAMPLE ANALYTE COUNT Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Lab ID Sample ID Method Analysts Analytes Reported Laboratory EPA 8260B Mod. DLK 3 PASI-C EPA 8260E JHG 51 PASI-GA 2610107020 1304-MW21 EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260B LIH 51 PASI-GA 2610107021 1304-MW22 EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E JHG 51 PASI-GA 2610107022 1304-MW22A EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E JHG 51 PASI-GA 2610107023 1304-MW25 EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E JHG 51 PASI-GA 2610107024 1304-MW26 EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E JHG 51 PASI-GA 2610107025 1304-MW27 EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260B LIH 51 PASI-GA 2610107026 1304-MW28 EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E RAC 51 PASI-GA 2610107027 1304-MW29R EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E RAC 51 PASI-GA 2610107028 1304-MW30R EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 SAMPLE ANALYTE COUNT Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Lab ID Sample ID Method Analysts Analytes Reported Laboratory EPA 8260E RAC 51 PASI-GA 2610107029 1304-MW31 EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E RAC 51 PASI-GA 2610107030 1304-MW32R EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E RAC 51 PASI-GA 2610107032 1304-MW34 EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E RAC 51 PASI-GA 2610107033 1304-Trip Day 1 EPA 8260B Mod. DLK 3 PASI-C EPA 8260E JHG 51 PASI-GA 2610107034 1304-Duplicate EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E RAC 51 PASI-GA 2610107035 1304-Equip Blank EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260B LIH 51 PASI-GA 2610107036 1304-SW2 EPA 6020E CSW 15 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260B LIH 51 PASI-GA 2610107037 1304-SW1 EPA 6020E CSW 15 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260B LIH 51 PASI-GA 2610107038 1304-Field Blank EPA 6020E CSW 15 PASI-GA EPA 7470A DRB 1 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260B LIH 51 PASI-GA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW1A Lab ID: 2610107001 Collected: 10/01/18 14:44 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: KR 1 10/16/18 10:53 6.62 Std. Units 1 10/16/18 10:53 19.3 deg C 1 10/16/18 10:53 982 umhos/c 1 10/16/18 10:53 m 3.24 NTU 1 10/16/18 10:53 1.19 ug/L 1 10/16/18 10:53 7782-44-7 4.67 feet 1 10/16/18 10:53 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1816:58 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1816:58 7440-38-2 121 ug/L 100 0.78 1 10/15/1813:00 10/16/1816:58 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1816:58 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1816:58 7440-43-9 ND ug/L 10.0 1.6 1 10/15/1813:00 10/16/1816:58 7440-47-3 6.4J ug/L 10.0 0.52 1 10/15/1813:00 10/16/1816:58 7440-48-4 3.9J ug/L 10.0 1.3 1 10/15/1813:00 10/16/1816:58 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1816:58 7439-92-1 5.OJ ug/L 50.0 0.95 1 10/15/1813:00 10/16/1816:58 7440-02-0 1.8J ug/L 10.0 1.4 1 10/15/1813:00 10/16/1816:58 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1816:58 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1816:58 7440-28-0 2.6J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1816:58 7440-62-2 4.4J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1816:58 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.058J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1811:30 7439-97-6 Analytical Method: EPA 8260B Mod. 14.6 ug/L 2.0 1.9 1 10/12/1813:17 123-91-1 110 % 50-150 110 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/12/18 13:17 17060-07-0 1 10/12/1813:17 2037-26-5 8.2 1 10/12/18 21:30 67-64-1 2.5 1 10/12/18 21:30 107-13-1 0.20 1 10/12/18 21:30 71-43-2 0.50 1 10/12/18 21:30 74-97-5 0.36 1 10/12/18 21:30 75-27-4 0.55 1 10/12/18 21:30 75-25-2 0.95 1 10/12/18 21:30 74-83-9 3.2 1 10/12/18 21:30 78-93-3 0.79 1 10/12/18 21:30 75-15-0 0.42 1 10/12/18 21:30 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 8 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW1A Lab ID: 2610107001 Collected: 10/01/18 14:44 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/12/18 21:30 108-90-7 ND ug/L 10.0 0.52 1 10/12/18 21:30 75-00-3 ND ug/L 5.0 0.58 1 10/12/18 21:30 67-66-3 ND ug/L 1.0 0.38 1 10/12/18 21:30 74-87-3 ND ug/L 13.0 0.55 1 10/12/18 21:30 96-12-8 ND ug/L 3.0 0.31 1 10/12/18 21:30 124-48-1 ND ug/L 2.0 0.28 1 10/12/18 21:30 106-93-4 ND ug/L 10.0 0.62 1 10/12/18 21:30 74-95-3 ND ug/L 5.0 0.49 1 10/12/18 21:30 95-50-1 ND ug/L 1.0 0.58 1 10/12/18 21:30 106-46-7 ND ug/L 100 1.6 1 10/12/18 21:30 110-57-6 ND ug/L 5.0 0.41 1 10/12/18 21:30 75-34-3 ND ug/L 1.0 0.67 1 10/12/18 21:30 107-06-2 ND ug/L 5.0 0.72 1 10/12/18 21:30 75-35-4 ND ug/L 5.0 0.66 1 10/12/18 21:30 156-59-2 ND ug/L 5.0 0.46 1 10/12/18 21:30 156-60-5 ND ug/L 1.0 0.60 1 10/12/18 21:30 78-87-5 ND ug/L 1.0 0.22 1 10/12/18 21:30 10061-01-5 ND ug/L 1.0 0.30 1 10/12/18 21:30 10061-02-6 ND ug/L 1.0 0.45 1 10/12/18 21:30 100-41-4 ND ug/L 50.0 0.89 1 10/12/18 21:30 591-78-6 ND ug/L 10.0 3.1 1 10/12/18 21:30 74-88-4 ND ug/L 1.0 0.50 1 10/12/18 21:30 75-09-2 ND ug/L 100 0.86 1 10/12/18 21:30 108-10-1 ND ug/L 1.0 0.50 1 10/12/18 21:30 100-42-5 ND ug/L 5.0 0.32 1 10/12/18 21:30 630-20-6 ND ug/L 3.0 0.53 1 10/12/18 21:30 79-34-5 ND ug/L 1.0 0.78 1 10/12/18 21:30 127-18-4 ND ug/L 1.0 0.31 1 10/12/18 21:30 108-88-3 ND ug/L 1.0 0.38 1 10/12/18 21:30 71-55-6 ND ug/L 1.0 0.59 1 10/12/18 21:30 79-00-5 ND ug/L 1.0 0.34 1 10/12/18 21:30 79-01-6 ND ug/L 1.0 0.51 1 10/12/18 21:30 75-69-4 ND ug/L 1.0 0.46 1 10/12/18 21:30 96-18-4 ND ug/L 50.0 0.42 1 10/12/18 21:30 108-05-4 ND ug/L 1.0 0.60 1 10/12/18 21:30 75-01-4 ND ug/L 5.0 1.5 1 10/12/18 21:30 1330-20-7 99 %. 81-119 1 10/12/18 21:30 17060-07-0 98 %. 82-114 1 10/12/18 21:30 1868-53-7 107 %. 82-120 1 10/12/18 21:30 460-00-4 97 %. 82-109 1 10/12/18 21:30 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW1B Lab ID: 2610107002 Collected: 10/01/18 15:39 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: KR 1 10/16/18 10:53 7.24 Std. Units 1 10/16/18 10:53 18.5 deg C 1 10/16/18 10:53 793 umhos/c 1 10/16/18 10:53 m 1.32 NTU 1 10/16/18 10:53 1.72 ug/L 1 10/16/18 10:53 7782-44-7 7.05 feet 1 10/16/18 10:53 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1817:03 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1817:03 7440-38-2 8.8J ug/L 100 0.78 1 10/15/1813:00 10/16/1817:03 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1817:03 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1817:03 7440-43-9 ND ug/L 10.0 1.6 1 10/15/1813:00 10/16/1817:03 7440-47-3 2.3J ug/L 10.0 0.52 1 10/15/1813:00 10/16/1817:03 7440-48-4 ND ug/L 10.0 1.3 1 10/15/1813:00 10/16/1817:03 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1817:03 7439-92-1 22.7J ug/L 50.0 0.95 1 10/15/1813:00 10/16/1817:03 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1817:03 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1817:03 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1817:03 7440-28-0 3.9J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1817:03 7440-62-2 7.5J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1817:03 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.066J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1811:44 7439-97-6 Analytical Method: EPA 8260B Mod. 22.8 ug/L 2.0 1.9 1 10/12/1814:15 123-91-1 105 % 50-150 109 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/12/18 14:15 17060-07-0 1 10/12/1814:15 2037-26-5 8.2 1 10/12/18 21:59 67-64-1 2.5 1 10/12/18 21:59 107-13-1 0.20 1 10/12/18 21:59 71-43-2 0.50 1 10/12/18 21:59 74-97-5 0.36 1 10/12/18 21:59 75-27-4 0.55 1 10/12/18 21:59 75-25-2 0.95 1 10/12/18 21:59 74-83-9 3.2 1 10/12/18 21:59 78-93-3 0.79 1 10/12/18 21:59 75-15-0 0.42 1 10/12/18 21:59 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 10 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW1B Lab ID: 2610107002 Collected: 10/01/18 15:39 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/12/18 21:59 108-90-7 ND ug/L 10.0 0.52 1 10/12/18 21:59 75-00-3 ND ug/L 5.0 0.58 1 10/12/18 21:59 67-66-3 ND ug/L 1.0 0.38 1 10/12/18 21:59 74-87-3 ND ug/L 13.0 0.55 1 10/12/18 21:59 96-12-8 ND ug/L 3.0 0.31 1 10/12/18 21:59 124-48-1 ND ug/L 2.0 0.28 1 10/12/18 21:59 106-93-4 ND ug/L 10.0 0.62 1 10/12/18 21:59 74-95-3 ND ug/L 5.0 0.49 1 10/12/18 21:59 95-50-1 ND ug/L 1.0 0.58 1 10/12/18 21:59 106-46-7 ND ug/L 100 1.6 1 10/12/18 21:59 110-57-6 ND ug/L 5.0 0.41 1 10/12/18 21:59 75-34-3 ND ug/L 1.0 0.67 1 10/12/18 21:59 107-06-2 ND ug/L 5.0 0.72 1 10/12/18 21:59 75-35-4 ND ug/L 5.0 0.66 1 10/12/18 21:59 156-59-2 ND ug/L 5.0 0.46 1 10/12/18 21:59 156-60-5 ND ug/L 1.0 0.60 1 10/12/18 21:59 78-87-5 ND ug/L 1.0 0.22 1 10/12/18 21:59 10061-01-5 ND ug/L 1.0 0.30 1 10/12/18 21:59 10061-02-6 ND ug/L 1.0 0.45 1 10/12/18 21:59 100-41-4 ND ug/L 50.0 0.89 1 10/12/18 21:59 591-78-6 ND ug/L 10.0 3.1 1 10/12/18 21:59 74-88-4 ND ug/L 1.0 0.50 1 10/12/18 21:59 75-09-2 ND ug/L 100 0.86 1 10/12/18 21:59 108-10-1 ND ug/L 1.0 0.50 1 10/12/18 21:59 100-42-5 ND ug/L 5.0 0.32 1 10/12/18 21:59 630-20-6 ND ug/L 3.0 0.53 1 10/12/18 21:59 79-34-5 ND ug/L 1.0 0.78 1 10/12/18 21:59 127-18-4 ND ug/L 1.0 0.31 1 10/12/18 21:59 108-88-3 ND ug/L 1.0 0.38 1 10/12/18 21:59 71-55-6 ND ug/L 1.0 0.59 1 10/12/18 21:59 79-00-5 ND ug/L 1.0 0.34 1 10/12/18 21:59 79-01-6 ND ug/L 1.0 0.51 1 10/12/18 21:59 75-69-4 ND ug/L 1.0 0.46 1 10/12/18 21:59 96-18-4 ND ug/L 50.0 0.42 1 10/12/18 21:59 108-05-4 ND ug/L 1.0 0.60 1 10/12/18 21:59 75-01-4 ND ug/L 5.0 1.5 1 10/12/18 21:59 1330-20-7 99 %. 81-119 1 10/12/18 21:59 17060-07-0 96 %. 82-114 1 10/12/18 21:59 1868-53-7 106 %. 82-120 1 10/12/18 21:59 460-00-4 96 %. 82-109 1 10/12/18 21:59 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW2A Lab ID: 2610107003 Collected: 10/01/18 15:31 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: WF 1 10/16/18 10:54 6.21 Std. Units 1 10/16/18 10:54 20.9 deg C 1 10/16/18 10:54 1197 umhos/c 1 10/16/18 10:54 m 3.17 NTU 1 10/16/18 10:54 1.43 ug/L 1 10/16/18 10:54 7782-44-7 5.32 feet 1 10/16/18 10:54 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1817:09 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1817:09 7440-38-2 180 ug/L 100 0.78 1 10/15/1813:00 10/16/1817:09 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1817:09 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1817:09 7440-43-9 ND ug/L 10.0 1.6 1 10/15/1813:00 10/16/1817:09 7440-47-3 ND ug/L 10.0 0.52 1 10/15/1813:00 10/16/1817:09 7440-48-4 ND ug/L 10.0 1.3 1 10/15/1813:00 10/16/1817:09 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1817:09 7439-92-1 7.9J ug/L 50.0 0.95 1 10/15/1813:00 10/16/1817:09 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1817:09 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1817:09 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1817:09 7440-28-0 5.3J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1817:09 7440-62-2 3.7J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1817:09 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.074J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1811:46 7439-97-6 Analytical Method: EPA 8260B Mod. 3.5 ug/L 2.0 1.9 1 10/12/1814:35 123-91-1 104 % 50-150 107 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/12/18 14:35 17060-07-0 1 10/12/1814:35 2037-26-5 8.2 1 10/12/18 22:29 67-64-1 2.5 1 10/12/18 22:29 107-13-1 0.20 1 10/12/18 22:29 71-43-2 0.50 1 10/12/18 22:29 74-97-5 0.36 1 10/12/18 22:29 75-27-4 0.55 1 10/12/18 22:29 75-25-2 0.95 1 10/12/18 22:29 74-83-9 3.2 1 10/12/18 22:29 78-93-3 0.79 1 10/12/18 22:29 75-15-0 0.42 1 10/12/18 22:29 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 12 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW2A Lab ID: 2610107003 Collected: 10/01/18 15:31 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/12/18 22:29 108-90-7 ND ug/L 10.0 0.52 1 10/12/18 22:29 75-00-3 ND ug/L 5.0 0.58 1 10/12/18 22:29 67-66-3 ND ug/L 1.0 0.38 1 10/12/18 22:29 74-87-3 ND ug/L 13.0 0.55 1 10/12/18 22:29 96-12-8 ND ug/L 3.0 0.31 1 10/12/18 22:29 124-48-1 ND ug/L 2.0 0.28 1 10/12/18 22:29 106-93-4 ND ug/L 10.0 0.62 1 10/12/18 22:29 74-95-3 ND ug/L 5.0 0.49 1 10/12/18 22:29 95-50-1 ND ug/L 1.0 0.58 1 10/12/18 22:29 106-46-7 ND ug/L 100 1.6 1 10/12/18 22:29 110-57-6 ND ug/L 5.0 0.41 1 10/12/18 22:29 75-34-3 ND ug/L 1.0 0.67 1 10/12/18 22:29 107-06-2 ND ug/L 5.0 0.72 1 10/12/18 22:29 75-35-4 ND ug/L 5.0 0.66 1 10/12/18 22:29 156-59-2 ND ug/L 5.0 0.46 1 10/12/18 22:29 156-60-5 ND ug/L 1.0 0.60 1 10/12/18 22:29 78-87-5 ND ug/L 1.0 0.22 1 10/12/18 22:29 10061-01-5 ND ug/L 1.0 0.30 1 10/12/18 22:29 10061-02-6 ND ug/L 1.0 0.45 1 10/12/18 22:29 100-41-4 ND ug/L 50.0 0.89 1 10/12/18 22:29 591-78-6 ND ug/L 10.0 3.1 1 10/12/18 22:29 74-88-4 ND ug/L 1.0 0.50 1 10/12/18 22:29 75-09-2 ND ug/L 100 0.86 1 10/12/18 22:29 108-10-1 ND ug/L 1.0 0.50 1 10/12/18 22:29 100-42-5 ND ug/L 5.0 0.32 1 10/12/18 22:29 630-20-6 ND ug/L 3.0 0.53 1 10/12/18 22:29 79-34-5 ND ug/L 1.0 0.78 1 10/12/18 22:29 127-18-4 ND ug/L 1.0 0.31 1 10/12/18 22:29 108-88-3 ND ug/L 1.0 0.38 1 10/12/18 22:29 71-55-6 ND ug/L 1.0 0.59 1 10/12/18 22:29 79-00-5 ND ug/L 1.0 0.34 1 10/12/18 22:29 79-01-6 ND ug/L 1.0 0.51 1 10/12/18 22:29 75-69-4 ND ug/L 1.0 0.46 1 10/12/18 22:29 96-18-4 ND ug/L 50.0 0.42 1 10/12/18 22:29 108-05-4 ND ug/L 1.0 0.60 1 10/12/18 22:29 75-01-4 ND ug/L 5.0 1.5 1 10/12/18 22:29 1330-20-7 98 %. 81-119 1 10/12/18 22:29 17060-07-0 95 %. 82-114 1 10/12/18 22:29 1868-53-7 105 %. 82-120 1 10/12/18 22:29 460-00-4 96 %. 82-109 1 10/12/18 22:29 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 13 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW2B Lab ID: 2610107004 Collected: 10/01/18 16:00 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: WF 1 10/16/18 10:55 6.42 Std. Units 1 10/16/18 10:55 17.8 deg C 1 10/16/18 10:55 886 umhos/c 1 10/16/18 10:55 m 3.11 NTU 1 10/16/18 10:55 1.24 ug/L 1 10/16/18 10:55 7782-44-7 5.75 feet 1 10/16/18 10:55 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1817:15 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1817:15 7440-38-2 46.9J ug/L 100 0.78 1 10/15/1813:00 10/16/1817:15 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1817:15 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1817:15 7440-43-9 1.6J ug/L 10.0 1.6 1 10/15/1813:00 10/16/1817:15 7440-47-3 13.2 ug/L 10.0 0.52 1 10/15/1813:00 10/16/1817:15 7440-48-4 ND ug/L 10.0 1.3 1 10/15/1813:00 10/16/1817:15 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1817:15 7439-92-1 16.OJ ug/L 50.0 0.95 1 10/15/1813:00 10/16/1817:15 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1817:15 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1817:15 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1817:15 7440-28-0 3.8J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1817:15 7440-62-2 4.OJ ug/L 10.0 2.1 1 10/15/1813:00 10/16/1817:15 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.12J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1811:49 7439-97-6 Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/12/1814:54 123-91-1 102 % 50-150 106 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/12/18 14:54 17060-07-0 1 10/12/1814:54 2037-26-5 8.2 1 10/12/18 22:59 67-64-1 2.5 1 10/12/18 22:59 107-13-1 0.20 1 10/12/18 22:59 71-43-2 0.50 1 10/12/18 22:59 74-97-5 0.36 1 10/12/18 22:59 75-27-4 0.55 1 10/12/18 22:59 75-25-2 0.95 1 10/12/18 22:59 74-83-9 3.2 1 10/12/18 22:59 78-93-3 0.79 1 10/12/18 22:59 75-15-0 0.42 1 10/12/18 22:59 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 14 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW2B Lab ID: 2610107004 Collected: 10/01/18 16:00 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/12/18 22:59 108-90-7 ND ug/L 10.0 0.52 1 10/12/18 22:59 75-00-3 ND ug/L 5.0 0.58 1 10/12/18 22:59 67-66-3 ND ug/L 1.0 0.38 1 10/12/18 22:59 74-87-3 ND ug/L 13.0 0.55 1 10/12/18 22:59 96-12-8 ND ug/L 3.0 0.31 1 10/12/18 22:59 124-48-1 ND ug/L 2.0 0.28 1 10/12/18 22:59 106-93-4 ND ug/L 10.0 0.62 1 10/12/18 22:59 74-95-3 ND ug/L 5.0 0.49 1 10/12/18 22:59 95-50-1 ND ug/L 1.0 0.58 1 10/12/18 22:59 106-46-7 ND ug/L 100 1.6 1 10/12/18 22:59 110-57-6 ND ug/L 5.0 0.41 1 10/12/18 22:59 75-34-3 ND ug/L 1.0 0.67 1 10/12/18 22:59 107-06-2 ND ug/L 5.0 0.72 1 10/12/18 22:59 75-35-4 ND ug/L 5.0 0.66 1 10/12/18 22:59 156-59-2 ND ug/L 5.0 0.46 1 10/12/18 22:59 156-60-5 ND ug/L 1.0 0.60 1 10/12/18 22:59 78-87-5 ND ug/L 1.0 0.22 1 10/12/18 22:59 10061-01-5 ND ug/L 1.0 0.30 1 10/12/18 22:59 10061-02-6 ND ug/L 1.0 0.45 1 10/12/18 22:59 100-41-4 ND ug/L 50.0 0.89 1 10/12/18 22:59 591-78-6 ND ug/L 10.0 3.1 1 10/12/18 22:59 74-88-4 ND ug/L 1.0 0.50 1 10/12/18 22:59 75-09-2 ND ug/L 100 0.86 1 10/12/18 22:59 108-10-1 ND ug/L 1.0 0.50 1 10/12/18 22:59 100-42-5 ND ug/L 5.0 0.32 1 10/12/18 22:59 630-20-6 ND ug/L 3.0 0.53 1 10/12/18 22:59 79-34-5 ND ug/L 1.0 0.78 1 10/12/18 22:59 127-18-4 ND ug/L 1.0 0.31 1 10/12/18 22:59 108-88-3 ND ug/L 1.0 0.38 1 10/12/18 22:59 71-55-6 ND ug/L 1.0 0.59 1 10/12/18 22:59 79-00-5 ND ug/L 1.0 0.34 1 10/12/18 22:59 79-01-6 ND ug/L 1.0 0.51 1 10/12/18 22:59 75-69-4 ND ug/L 1.0 0.46 1 10/12/18 22:59 96-18-4 ND ug/L 50.0 0.42 1 10/12/18 22:59 108-05-4 ND ug/L 1.0 0.60 1 10/12/18 22:59 75-01-4 ND ug/L 5.0 1.5 1 10/12/18 22:59 1330-20-7 103 %. 81-119 1 10/12/18 22:59 17060-07-0 99 %. 82-114 1 10/12/18 22:59 1868-53-7 106 %. 82-120 1 10/12/18 22:59 460-00-4 96 %. 82-109 1 10/12/18 22:59 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 15 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW10 Lab ID: 2610107005 Collected: 10/02/18 15:08 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: WF 1 10/16/18 10:55 5.76 Std. Units 1 10/16/18 10:55 17.6 deg C 1 10/16/18 10:55 107 umhos/c 1 10/16/18 10:55 m 6.00 NTU 1 10/16/18 10:55 1.11 ug/L 1 10/16/18 10:55 7782-44-7 21.00 feet 1 10/16/18 10:55 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1817:20 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1817:20 7440-38-2 33.5J ug/L 100 0.78 1 10/15/1813:00 10/16/1817:20 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1817:20 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1817:20 7440-43-9 ND ug/L 10.0 1.6 1 10/15/1813:00 10/16/1817:20 7440-47-3 ND ug/L 10.0 0.52 1 10/15/1813:00 10/16/1817:20 7440-48-4 ND ug/L 10.0 1.3 1 10/15/1813:00 10/16/1817:20 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1817:20 7439-92-1 1.4J ug/L 50.0 0.95 1 10/15/1813:00 10/16/1817:20 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1817:20 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1817:20 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1817:20 7440-28-0 ND ug/L 25.0 1.9 1 10/15/1813:00 10/16/1817:20 7440-62-2 5.5J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1817:20 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.071J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1811:51 7439-97-6 Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/12/1816:32 123-91-1 103 % 50-150 106 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/12/18 16:32 17060-07-0 1 10/12/1816:32 2037-26-5 8.2 1 10/13/1812:44 67-64-1 2.5 1 10/13/18 12:44 107-13-1 0.20 1 10/13/1812:44 71-43-2 0.50 1 10/13/1812:44 74-97-5 0.36 1 10/13/1812:44 75-27-4 0.55 1 10/13/1812:44 75-25-2 0.95 1 10/13/1812:44 74-83-9 3.2 1 10/13/1812:44 78-93-3 0.79 1 10/13/1812:44 75-15-0 0.42 1 10/13/1812:44 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 16 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW10 Lab ID: 2610107005 Collected: 10/02/18 15:08 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/13/1812:44 108-90-7 ND ug/L 10.0 0.52 1 10/13/1812:44 75-00-3 ND ug/L 5.0 0.58 1 10/13/1812:44 67-66-3 ND ug/L 1.0 0.38 1 10/13/1812:44 74-87-3 ND ug/L 13.0 0.55 1 10/13/1812:44 96-12-8 ND ug/L 3.0 0.31 1 10/13/1812:44 124-48-1 ND ug/L 2.0 0.28 1 10/13/1812:44 106-93-4 ND ug/L 10.0 0.62 1 10/13/1812:44 74-95-3 ND ug/L 5.0 0.49 1 10/13/1812:44 95-50-1 ND ug/L 1.0 0.58 1 10/13/1812:44 106-46-7 ND ug/L 100 1.6 1 10/13/1812:44 110-57-6 ND ug/L 5.0 0.41 1 10/13/1812:44 75-34-3 ND ug/L 1.0 0.67 1 10/13/1812:44 107-06-2 ND ug/L 5.0 0.72 1 10/13/1812:44 75-35-4 ND ug/L 5.0 0.66 1 10/13/1812:44 156-59-2 ND ug/L 5.0 0.46 1 10/13/1812:44 156-60-5 ND ug/L 1.0 0.60 1 10/13/1812:44 78-87-5 ND ug/L 1.0 0.22 1 10/13/1812:44 10061-01-5 ND ug/L 1.0 0.30 1 10/13/1812:44 10061-02-6 ND ug/L 1.0 0.45 1 10/13/1812:44 100-41-4 ND ug/L 50.0 0.89 1 10/13/1812:44 591-78-6 ND ug/L 10.0 3.1 1 10/13/1812:44 74-88-4 ND ug/L 1.0 0.50 1 10/13/1812:44 75-09-2 ND ug/L 100 0.86 1 10/13/1812:44 108-10-1 ND ug/L 1.0 0.50 1 10/13/1812:44 100-42-5 ND ug/L 5.0 0.32 1 10/13/1812:44 630-20-6 ND ug/L 3.0 0.53 1 10/13/1812:44 79-34-5 ND ug/L 1.0 0.78 1 10/13/1812:44 127-18-4 ND ug/L 1.0 0.31 1 10/13/1812:44 108-88-3 ND ug/L 1.0 0.38 1 10/13/1812:44 71-55-6 ND ug/L 1.0 0.59 1 10/13/1812:44 79-00-5 0.97J ug/L 1.0 0.34 1 10/13/1812:44 79-01-6 ND ug/L 1.0 0.51 1 10/13/1812:44 75-69-4 ND ug/L 1.0 0.46 1 10/13/1812:44 96-18-4 ND ug/L 50.0 0.42 1 10/13/1812:44 108-05-4 ND ug/L 1.0 0.60 1 10/13/1812:44 75-01-4 ND ug/L 5.0 1.5 1 10/13/1812:44 1330-20-7 115 %. 81-119 1 10/13/1812:44 17060-07-0 97 %. 82-114 1 10/13/1812:44 1868-53-7 107 %. 82-120 1 10/13/1812:44 460-00-4 107 %. 82-109 1 10/13/1812:44 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. B Page 17 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW10A Lab ID: 2610107006 Collected: 10/02/18 16:28 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: WF 1 10/16/18 10:56 6.63 Std. Units 1 10/16/18 10:56 19.6 deg C 1 10/16/18 10:56 236 umhos/c 1 10/16/18 10:56 m 4.99 NTU 1 10/16/18 10:56 1.67 ug/L 1 10/16/18 10:56 7782-44-7 21.54 feet 1 10/16/18 10:56 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1817:26 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1817:26 7440-38-2 31.5J ug/L 100 0.78 1 10/15/1813:00 10/16/1817:26 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1817:26 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1817:26 7440-43-9 ND ug/L 10.0 1.6 1 10/15/1813:00 10/16/1817:26 7440-47-3 ND ug/L 10.0 0.52 1 10/15/1813:00 10/16/1817:26 7440-48-4 ND ug/L 10.0 1.3 1 10/15/1813:00 10/16/1817:26 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1817:26 7439-92-1 1.3J ug/L 50.0 0.95 1 10/15/1813:00 10/16/1817:26 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1817:26 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1817:26 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1817:26 7440-28-0 ND ug/L 25.0 1.9 1 10/15/1813:00 10/16/1817:26 7440-62-2 5.3J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1817:26 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.080J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1811:54 7439-97-6 Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/12/18 16:51 123-91-1 102 % 50-150 107 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/12/18 16:51 17060-07-0 1 10/12/18 16:51 2037-26-5 8.2 1 10/13/1813:08 67-64-1 2.5 1 10/13/18 13:08 107-13-1 0.20 1 10/13/1813:08 71-43-2 0.50 1 10/13/1813:08 74-97-5 0.36 1 10/13/1813:08 75-27-4 0.55 1 10/13/1813:08 75-25-2 0.95 1 10/13/1813:08 74-83-9 3.2 1 10/13/1813:08 78-93-3 0.79 1 10/13/1813:08 75-15-0 0.42 1 10/13/1813:08 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 18 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW10A Lab ID: 2610107006 Collected: 10/02/18 16:28 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/13/1813:08 108-90-7 ND ug/L 10.0 0.52 1 10/13/1813:08 75-00-3 ND ug/L 5.0 0.58 1 10/13/1813:08 67-66-3 ND ug/L 1.0 0.38 1 10/13/1813:08 74-87-3 ND ug/L 13.0 0.55 1 10/13/1813:08 96-12-8 ND ug/L 3.0 0.31 1 10/13/1813:08 124-48-1 ND ug/L 2.0 0.28 1 10/13/1813:08 106-93-4 ND ug/L 10.0 0.62 1 10/13/1813:08 74-95-3 ND ug/L 5.0 0.49 1 10/13/1813:08 95-50-1 ND ug/L 1.0 0.58 1 10/13/1813:08 106-46-7 ND ug/L 100 1.6 1 10/13/1813:08 110-57-6 ND ug/L 5.0 0.41 1 10/13/1813:08 75-34-3 ND ug/L 1.0 0.67 1 10/13/1813:08 107-06-2 ND ug/L 5.0 0.72 1 10/13/1813:08 75-35-4 ND ug/L 5.0 0.66 1 10/13/1813:08 156-59-2 ND ug/L 5.0 0.46 1 10/13/1813:08 156-60-5 ND ug/L 1.0 0.60 1 10/13/1813:08 78-87-5 ND ug/L 1.0 0.22 1 10/13/1813:08 10061-01-5 ND ug/L 1.0 0.30 1 10/13/1813:08 10061-02-6 ND ug/L 1.0 0.45 1 10/13/1813:08 100-41-4 ND ug/L 50.0 0.89 1 10/13/1813:08 591-78-6 ND ug/L 10.0 3.1 1 10/13/1813:08 74-88-4 ND ug/L 1.0 0.50 1 10/13/1813:08 75-09-2 ND ug/L 100 0.86 1 10/13/1813:08 108-10-1 ND ug/L 1.0 0.50 1 10/13/1813:08 100-42-5 ND ug/L 5.0 0.32 1 10/13/1813:08 630-20-6 ND ug/L 3.0 0.53 1 10/13/1813:08 79-34-5 ND ug/L 1.0 0.78 1 10/13/1813:08 127-18-4 ND ug/L 1.0 0.31 1 10/13/1813:08 108-88-3 ND ug/L 1.0 0.38 1 10/13/1813:08 71-55-6 ND ug/L 1.0 0.59 1 10/13/1813:08 79-00-5 0.49J ug/L 1.0 0.34 1 10/13/1813:08 79-01-6 ND ug/L 1.0 0.51 1 10/13/1813:08 75-69-4 ND ug/L 1.0 0.46 1 10/13/1813:08 96-18-4 ND ug/L 50.0 0.42 1 10/13/1813:08 108-05-4 ND ug/L 1.0 0.60 1 10/13/1813:08 75-01-4 ND ug/L 5.0 1.5 1 10/13/1813:08 1330-20-7 113 %. 81-119 1 10/13/1813:08 17060-07-0 98 %. 82-114 1 10/13/1813:08 1868-53-7 109 %. 82-120 1 10/13/1813:08 460-00-4 107 %. 82-109 1 10/13/1813:08 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. B Page 19 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW11 Lab ID: 2610107007 Collected: 10/02/18 08:58 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: SF 1 10/16/18 10:56 6.58 Std. Units 1 10/16/18 10:56 19.9 deg C 1 10/16/18 10:56 479 umhos/c 1 10/16/18 10:56 m 2.04 NTU 1 10/16/18 10:56 2.21 ug/L 1 10/16/18 10:56 7782-44-7 9.13 feet 1 10/16/18 10:56 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1817:32 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1817:32 7440-38-2 22.OJ ug/L 100 0.78 1 10/15/1813:00 10/16/1817:32 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1817:32 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1817:32 7440-43-9 ND ug/L 10.0 1.6 1 10/15/1813:00 10/16/1817:32 7440-47-3 ND ug/L 10.0 0.52 1 10/15/1813:00 10/16/1817:32 7440-48-4 ND ug/L 10.0 1.3 1 10/15/1813:00 10/16/1817:32 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1817:32 7439-92-1 1.3J ug/L 50.0 0.95 1 10/15/1813:00 10/16/1817:32 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1817:32 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1817:32 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1817:32 7440-28-0 5.2J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1817:32 7440-62-2 3.OJ ug/L 10.0 2.1 1 10/15/1813:00 10/16/1817:32 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.061J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1811:56 7439-97-6 Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/12/18 17:11 123-91-1 101 % 50-150 107 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/12/18 17:11 17060-07-0 1 10/12/18 17:11 2037-26-5 8.2 1 10/13/1813:33 67-64-1 2.5 1 10/13/18 13:33 107-13-1 0.20 1 10/13/1813:33 71-43-2 0.50 1 10/13/1813:33 74-97-5 0.36 1 10/13/1813:33 75-27-4 0.55 1 10/13/1813:33 75-25-2 0.95 1 10/13/1813:33 74-83-9 3.2 1 10/13/1813:33 78-93-3 0.79 1 10/13/1813:33 75-15-0 0.42 1 10/13/1813:33 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B R1 R1 R1 R1 R1 R1 M1,R1 Page 20 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW11 Lab ID: 2610107007 Collected: 10/02/18 08:58 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/13/1813:33 108-90-7 R1 ND ug/L 10.0 0.52 1 10/13/1813:33 75-00-3 R1 ND ug/L 5.0 0.58 1 10/13/1813:33 67-66-3 R1 ND ug/L 1.0 0.38 1 10/13/1813:33 74-87-3 R1 ND ug/L 13.0 0.55 1 10/13/1813:33 96-12-8 R1 ND ug/L 3.0 0.31 1 10/13/1813:33 124-48-1 R1 ND ug/L 2.0 0.28 1 10/13/1813:33 106-93-4 R1 ND ug/L 10.0 0.62 1 10/13/1813:33 74-95-3 R1 ND ug/L 5.0 0.49 1 10/13/1813:33 95-50-1 R1 ND ug/L 1.0 0.58 1 10/13/1813:33 106-46-7 R1 ND ug/L 100 1.6 1 10/13/1813:33 110-57-6 R1 ND ug/L 5.0 0.41 1 10/13/1813:33 75-34-3 R1 ND ug/L 1.0 0.67 1 10/13/1813:33 107-06-2 R1 ND ug/L 5.0 0.72 1 10/13/1813:33 75-35-4 ND ug/L 5.0 0.66 1 10/13/1813:33 156-59-2 R1 ND ug/L 5.0 0.46 1 10/13/1813:33 156-60-5 R1 ND ug/L 1.0 0.60 1 10/13/1813:33 78-87-5 R1 ND ug/L 1.0 0.22 1 10/13/1813:33 10061-01-5 R1 ND ug/L 1.0 0.30 1 10/13/1813:33 10061-02-6 R1 ND ug/L 1.0 0.45 1 10/13/1813:33 100-41-4 R1 ND ug/L 50.0 0.89 1 10/13/1813:33 591-78-6 R1 ND ug/L 10.0 3.1 1 10/13/1813:33 74-88-4 R1 ND ug/L 1.0 0.50 1 10/13/1813:33 75-09-2 R1 ND ug/L 100 0.86 1 10/13/1813:33 108-10-1 R1 ND ug/L 1.0 0.50 1 10/13/1813:33 100-42-5 R1 ND ug/L 5.0 0.32 1 10/13/1813:33 630-20-6 R1 ND ug/L 3.0 0.53 1 10/13/1813:33 79-34-5 R1 ND ug/L 1.0 0.78 1 10/13/1813:33 127-18-4 R1 ND ug/L 1.0 0.31 1 10/13/1813:33 108-88-3 R1 ND ug/L 1.0 0.38 1 10/13/1813:33 71-55-6 R1 ND ug/L 1.0 0.59 1 10/13/1813:33 79-00-5 R1 ND ug/L 1.0 0.34 1 10/13/1813:33 79-01-6 R1 ND ug/L 1.0 0.51 1 10/13/1813:33 75-69-4 R1 ND ug/L 1.0 0.46 1 10/13/1813:33 96-18-4 M1,R1 ND ug/L 50.0 0.42 1 10/13/1813:33 108-05-4 R1 ND ug/L 1.0 0.60 1 10/13/1813:33 75-01-4 ND ug/L 5.0 1.5 1 10/13/1813:33 1330-20-7 115 %. 81-119 1 10/13/1813:33 17060-07-0 97 %. 82-114 1 10/13/1813:33 1868-53-7 108 %. 82-120 1 10/13/1813:33 460-00-4 108 %. 82-109 1 10/13/1813:33 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 21 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW12 Lab ID: 2610107008 Collected: 10/02/18 08:29 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: SF 1 10/16/18 10:57 6.25 Std. Units 1 10/16/18 10:57 17.8 deg C 1 10/16/18 10:57 384 umhos/c 1 10/16/18 10:57 m 5.83 NTU 1 10/16/18 10:57 3.97 ug/L 1 10/16/18 10:57 7782-44-7 9.51 feet 1 10/16/18 10:57 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1817:38 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1817:38 7440-38-2 18.6J ug/L 100 0.78 1 10/15/1813:00 10/16/1817:38 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1817:38 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1817:38 7440-43-9 7.3J ug/L 10.0 1.6 1 10/15/1813:00 10/16/1817:38 7440-47-3 1.5J ug/L 10.0 0.52 1 10/15/1813:00 10/16/1817:38 7440-48-4 ND ug/L 10.0 1.3 1 10/15/1813:00 10/16/1817:38 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1817:38 7439-92-1 6.4J ug/L 50.0 0.95 1 10/15/1813:00 10/16/1817:38 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1817:38 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1817:38 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1817:38 7440-28-0 6.4J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1817:38 7440-62-2 5.9J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1817:38 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.063J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1811:58 7439-97-6 Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/12/1817:30 123-91-1 104 % 50-150 107 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/12/18 17:30 17060-07-0 1 10/12/1817:30 2037-26-5 8.2 1 10/13/1813:58 67-64-1 2.5 1 10/13/18 13:58 107-13-1 0.20 1 10/13/1813:58 71-43-2 0.50 1 10/13/1813:58 74-97-5 0.36 1 10/13/1813:58 75-27-4 0.55 1 10/13/1813:58 75-25-2 0.95 1 10/13/1813:58 74-83-9 3.2 1 10/13/1813:58 78-93-3 0.79 1 10/13/1813:58 75-15-0 0.42 1 10/13/1813:58 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 22 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW12 Lab ID: 2610107008 Collected: 10/02/18 08:29 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/13/1813:58 108-90-7 ND ug/L 10.0 0.52 1 10/13/1813:58 75-00-3 ND ug/L 5.0 0.58 1 10/13/1813:58 67-66-3 ND ug/L 1.0 0.38 1 10/13/1813:58 74-87-3 ND ug/L 13.0 0.55 1 10/13/1813:58 96-12-8 ND ug/L 3.0 0.31 1 10/13/1813:58 124-48-1 ND ug/L 2.0 0.28 1 10/13/1813:58 106-93-4 ND ug/L 10.0 0.62 1 10/13/1813:58 74-95-3 ND ug/L 5.0 0.49 1 10/13/1813:58 95-50-1 ND ug/L 1.0 0.58 1 10/13/1813:58 106-46-7 ND ug/L 100 1.6 1 10/13/1813:58 110-57-6 ND ug/L 5.0 0.41 1 10/13/1813:58 75-34-3 ND ug/L 1.0 0.67 1 10/13/1813:58 107-06-2 ND ug/L 5.0 0.72 1 10/13/1813:58 75-35-4 ND ug/L 5.0 0.66 1 10/13/1813:58 156-59-2 ND ug/L 5.0 0.46 1 10/13/1813:58 156-60-5 ND ug/L 1.0 0.60 1 10/13/1813:58 78-87-5 ND ug/L 1.0 0.22 1 10/13/1813:58 10061-01-5 ND ug/L 1.0 0.30 1 10/13/1813:58 10061-02-6 ND ug/L 1.0 0.45 1 10/13/1813:58 100-41-4 ND ug/L 50.0 0.89 1 10/13/1813:58 591-78-6 ND ug/L 10.0 3.1 1 10/13/1813:58 74-88-4 ND ug/L 1.0 0.50 1 10/13/1813:58 75-09-2 ND ug/L 100 0.86 1 10/13/1813:58 108-10-1 ND ug/L 1.0 0.50 1 10/13/1813:58 100-42-5 ND ug/L 5.0 0.32 1 10/13/1813:58 630-20-6 ND ug/L 3.0 0.53 1 10/13/1813:58 79-34-5 ND ug/L 1.0 0.78 1 10/13/1813:58 127-18-4 ND ug/L 1.0 0.31 1 10/13/1813:58 108-88-3 ND ug/L 1.0 0.38 1 10/13/1813:58 71-55-6 ND ug/L 1.0 0.59 1 10/13/1813:58 79-00-5 ND ug/L 1.0 0.34 1 10/13/1813:58 79-01-6 ND ug/L 1.0 0.51 1 10/13/1813:58 75-69-4 ND ug/L 1.0 0.46 1 10/13/1813:58 96-18-4 ND ug/L 50.0 0.42 1 10/13/1813:58 108-05-4 ND ug/L 1.0 0.60 1 10/13/1813:58 75-01-4 ND ug/L 5.0 1.5 1 10/13/1813:58 1330-20-7 113 %. 81-119 1 10/13/1813:58 17060-07-0 96 %. 82-114 1 10/13/1813:58 1868-53-7 109 %. 82-120 1 10/13/1813:58 460-00-4 108 %. 82-109 1 10/13/1813:58 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 23 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW14 Lab ID: 2610107009 Collected: 10/02/18 09:19 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: KR 1 10/16/18 10:58 6.59 Std. Units 1 10/16/18 10:58 19.7 deg C 1 10/16/18 10:58 342 umhos/c 1 10/16/18 10:58 m 4.12 NTU 1 10/16/18 10:58 3.60 ug/L 1 10/16/18 10:58 7782-44-7 9.20 feet 1 10/16/18 10:58 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1817:55 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1817:55 7440-38-2 8.5J ug/L 100 0.78 1 10/15/1813:00 10/16/1817:55 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1817:55 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1817:55 7440-43-9 ND ug/L 10.0 1.6 1 10/15/1813:00 10/16/1817:55 7440-47-3 ND ug/L 10.0 0.52 1 10/15/1813:00 10/16/1817:55 7440-48-4 2.7J ug/L 10.0 1.3 1 10/15/1813:00 10/16/1817:55 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1817:55 7439-92-1 12.4J ug/L 50.0 0.95 1 10/15/1813:00 10/16/1817:55 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1817:55 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1817:55 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1817:55 7440-28-0 6.5J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1817:55 7440-62-2 6.3J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1817:55 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.057J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1812:01 7439-97-6 Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/12/1817:50 123-91-1 102 % 50-150 108 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/12/18 17:50 17060-07-0 1 10/12/1817:50 2037-26-5 8.2 1 10/13/1814:23 67-64-1 2.5 1 10/13/18 14:23 107-13-1 0.20 1 10/13/1814:23 71-43-2 0.50 1 10/13/1814:23 74-97-5 0.36 1 10/13/1814:23 75-27-4 0.55 1 10/13/1814:23 75-25-2 0.95 1 10/13/1814:23 74-83-9 3.2 1 10/13/1814:23 78-93-3 0.79 1 10/13/1814:23 75-15-0 0.42 1 10/13/1814:23 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 24 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW14 Lab ID: 2610107009 Collected: 10/02/18 09:19 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/13/1814:23 108-90-7 ND ug/L 10.0 0.52 1 10/13/1814:23 75-00-3 ND ug/L 5.0 0.58 1 10/13/1814:23 67-66-3 ND ug/L 1.0 0.38 1 10/13/1814:23 74-87-3 ND ug/L 13.0 0.55 1 10/13/1814:23 96-12-8 ND ug/L 3.0 0.31 1 10/13/1814:23 124-48-1 ND ug/L 2.0 0.28 1 10/13/1814:23 106-93-4 ND ug/L 10.0 0.62 1 10/13/1814:23 74-95-3 ND ug/L 5.0 0.49 1 10/13/1814:23 95-50-1 ND ug/L 1.0 0.58 1 10/13/1814:23 106-46-7 ND ug/L 100 1.6 1 10/13/1814:23 110-57-6 ND ug/L 5.0 0.41 1 10/13/1814:23 75-34-3 ND ug/L 1.0 0.67 1 10/13/1814:23 107-06-2 ND ug/L 5.0 0.72 1 10/13/1814:23 75-35-4 ND ug/L 5.0 0.66 1 10/13/1814:23 156-59-2 ND ug/L 5.0 0.46 1 10/13/1814:23 156-60-5 ND ug/L 1.0 0.60 1 10/13/1814:23 78-87-5 ND ug/L 1.0 0.22 1 10/13/1814:23 10061-01-5 ND ug/L 1.0 0.30 1 10/13/1814:23 10061-02-6 ND ug/L 1.0 0.45 1 10/13/1814:23 100-41-4 ND ug/L 50.0 0.89 1 10/13/1814:23 591-78-6 ND ug/L 10.0 3.1 1 10/13/1814:23 74-88-4 ND ug/L 1.0 0.50 1 10/13/1814:23 75-09-2 ND ug/L 100 0.86 1 10/13/1814:23 108-10-1 ND ug/L 1.0 0.50 1 10/13/1814:23 100-42-5 ND ug/L 5.0 0.32 1 10/13/1814:23 630-20-6 ND ug/L 3.0 0.53 1 10/13/1814:23 79-34-5 ND ug/L 1.0 0.78 1 10/13/1814:23 127-18-4 ND ug/L 1.0 0.31 1 10/13/1814:23 108-88-3 ND ug/L 1.0 0.38 1 10/13/1814:23 71-55-6 ND ug/L 1.0 0.59 1 10/13/1814:23 79-00-5 ND ug/L 1.0 0.34 1 10/13/1814:23 79-01-6 ND ug/L 1.0 0.51 1 10/13/1814:23 75-69-4 ND ug/L 1.0 0.46 1 10/13/1814:23 96-18-4 ND ug/L 50.0 0.42 1 10/13/1814:23 108-05-4 ND ug/L 1.0 0.60 1 10/13/1814:23 75-01-4 ND ug/L 5.0 1.5 1 10/13/1814:23 1330-20-7 116 %. 81-119 1 10/13/1814:23 17060-07-0 97 %. 82-114 1 10/13/1814:23 1868-53-7 111 %. 82-120 1 10/13/1814:23 460-00-4 109 %. 82-109 1 10/13/1814:23 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 25 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW14B Lab ID: 2610107010 Collected: 10/03/18 08:55 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: KR 1 10/16/18 10:58 7.03 Std. Units 1 10/16/18 10:58 17.8 deg C 1 10/16/18 10:58 610 umhos/c 1 10/16/18 10:58 m 2.78 NTU 1 10/16/18 10:58 1.03 ug/L 1 10/16/18 10:58 7782-44-7 9.64 feet 1 10/16/18 10:58 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1818:01 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1818:01 7440-38-2 5.2J ug/L 100 0.78 1 10/15/1813:00 10/16/1818:01 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1818:01 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1818:01 7440-43-9 ND ug/L 10.0 1.6 1 10/15/1813:00 10/16/1818:01 7440-47-3 ND ug/L 10.0 0.52 1 10/15/1813:00 10/16/1818:01 7440-48-4 ND ug/L 10.0 1.3 1 10/15/1813:00 10/16/1818:01 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1818:01 7439-92-1 1.2J ug/L 50.0 0.95 1 10/15/1813:00 10/16/1818:01 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1818:01 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1818:01 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1818:01 7440-28-0 6.7J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1818:01 7440-62-2 4.8J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1818:01 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.090J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1812:03 7439-97-6 Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/17/1815:07 123-91-1 103 % 50-150 114 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/17/18 15:07 17060-07-0 1 10/17/1815:07 2037-26-5 8.2 1 10/13/1814:47 67-64-1 2.5 1 10/13/18 14:47 107-13-1 0.20 1 10/13/1814:47 71-43-2 0.50 1 10/13/1814:47 74-97-5 0.36 1 10/13/1814:47 75-27-4 0.55 1 10/13/1814:47 75-25-2 0.95 1 10/13/1814:47 74-83-9 3.2 1 10/13/1814:47 78-93-3 0.79 1 10/13/1814:47 75-15-0 0.42 1 10/13/1814:47 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 26 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW14B Lab ID: 2610107010 Collected: 10/03/18 08:55 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/13/1814:47 108-90-7 ND ug/L 10.0 0.52 1 10/13/1814:47 75-00-3 ND ug/L 5.0 0.58 1 10/13/1814:47 67-66-3 ND ug/L 1.0 0.38 1 10/13/1814:47 74-87-3 ND ug/L 13.0 0.55 1 10/13/1814:47 96-12-8 ND ug/L 3.0 0.31 1 10/13/1814:47 124-48-1 ND ug/L 2.0 0.28 1 10/13/1814:47 106-93-4 ND ug/L 10.0 0.62 1 10/13/1814:47 74-95-3 ND ug/L 5.0 0.49 1 10/13/1814:47 95-50-1 ND ug/L 1.0 0.58 1 10/13/1814:47 106-46-7 ND ug/L 100 1.6 1 10/13/1814:47 110-57-6 ND ug/L 5.0 0.41 1 10/13/1814:47 75-34-3 ND ug/L 1.0 0.67 1 10/13/1814:47 107-06-2 ND ug/L 5.0 0.72 1 10/13/1814:47 75-35-4 ND ug/L 5.0 0.66 1 10/13/1814:47 156-59-2 ND ug/L 5.0 0.46 1 10/13/1814:47 156-60-5 ND ug/L 1.0 0.60 1 10/13/1814:47 78-87-5 ND ug/L 1.0 0.22 1 10/13/1814:47 10061-01-5 ND ug/L 1.0 0.30 1 10/13/1814:47 10061-02-6 ND ug/L 1.0 0.45 1 10/13/1814:47 100-41-4 ND ug/L 50.0 0.89 1 10/13/1814:47 591-78-6 ND ug/L 10.0 3.1 1 10/13/1814:47 74-88-4 ND ug/L 1.0 0.50 1 10/13/1814:47 75-09-2 ND ug/L 100 0.86 1 10/13/1814:47 108-10-1 ND ug/L 1.0 0.50 1 10/13/1814:47 100-42-5 ND ug/L 5.0 0.32 1 10/13/1814:47 630-20-6 ND ug/L 3.0 0.53 1 10/13/1814:47 79-34-5 ND ug/L 1.0 0.78 1 10/13/1814:47 127-18-4 ND ug/L 1.0 0.31 1 10/13/1814:47 108-88-3 ND ug/L 1.0 0.38 1 10/13/1814:47 71-55-6 ND ug/L 1.0 0.59 1 10/13/1814:47 79-00-5 ND ug/L 1.0 0.34 1 10/13/1814:47 79-01-6 ND ug/L 1.0 0.51 1 10/13/1814:47 75-69-4 ND ug/L 1.0 0.46 1 10/13/1814:47 96-18-4 ND ug/L 50.0 0.42 1 10/13/1814:47 108-05-4 ND ug/L 1.0 0.60 1 10/13/1814:47 75-01-4 ND ug/L 5.0 1.5 1 10/13/1814:47 1330-20-7 117 %. 81-119 1 10/13/1814:47 17060-07-0 95 %. 82-114 1 10/13/1814:47 1868-53-7 109 %. 82-120 1 10/13/1814:47 460-00-4 109 %. 82-109 1 10/13/1814:47 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 27 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW15 Lab ID: 2610107011 Collected: 10/02/18 10:11 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: KR 1 10/16/18 10:59 6.64 Std. Units 1 10/16/18 10:59 22.8 deg C 1 10/16/18 10:59 397 umhos/c 1 10/16/18 10:59 m 3.82 NTU 1 10/16/18 10:59 2.20 ug/L 1 10/16/18 10:59 7782-44-7 8.80 feet 1 10/16/18 10:59 Analytical Method: EPA 6020B Preparation Method: EPA 3005A 1.7J ug/L 6.0 0.78 1 10/15/1813:00 10/16/1818:06 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1818:06 7440-38-2 46.2J ug/L 100 0.78 1 10/15/1813:00 10/16/1818:06 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1818:06 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1818:06 7440-43-9 8.4J ug/L 10.0 1.6 1 10/15/1813:00 10/16/1818:06 7440-47-3 1.1J ug/L 10.0 0.52 1 10/15/1813:00 10/16/1818:06 7440-48-4 7.9J ug/L 10.0 1.3 1 10/15/1813:00 10/16/1818:06 7440-50-8 1.9J ug/L 10.0 0.27 1 10/15/1813:00 10/16/1818:06 7439-92-1 17.OJ ug/L 50.0 0.95 1 10/15/1813:00 10/16/1818:06 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1818:06 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1818:06 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1818:06 7440-28-0 9.5J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1818:06 7440-62-2 6.6J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1818:06 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.088J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1812:10 7439-97-6 Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/12/1818:09 123-91-1 105 % 50-150 107 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/12/18 18:09 17060-07-0 1 10/12/1818:09 2037-26-5 8.2 1 10/13/1815:12 67-64-1 2.5 1 10/13/18 15:12 107-13-1 0.20 1 10/13/1815:12 71-43-2 0.50 1 10/13/1815:12 74-97-5 0.36 1 10/13/1815:12 75-27-4 0.55 1 10/13/1815:12 75-25-2 0.95 1 10/13/1815:12 74-83-9 3.2 1 10/13/1815:12 78-93-3 0.79 1 10/13/1815:12 75-15-0 0.42 1 10/13/1815:12 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 28 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW15 Lab ID: 2610107011 Collected: 10/02/18 10:11 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/13/1815:12 108-90-7 ND ug/L 10.0 0.52 1 10/13/1815:12 75-00-3 ND ug/L 5.0 0.58 1 10/13/1815:12 67-66-3 ND ug/L 1.0 0.38 1 10/13/1815:12 74-87-3 ND ug/L 13.0 0.55 1 10/13/1815:12 96-12-8 ND ug/L 3.0 0.31 1 10/13/1815:12 124-48-1 ND ug/L 2.0 0.28 1 10/13/1815:12 106-93-4 ND ug/L 10.0 0.62 1 10/13/1815:12 74-95-3 ND ug/L 5.0 0.49 1 10/13/1815:12 95-50-1 ND ug/L 1.0 0.58 1 10/13/1815:12 106-46-7 ND ug/L 100 1.6 1 10/13/1815:12 110-57-6 ND ug/L 5.0 0.41 1 10/13/1815:12 75-34-3 ND ug/L 1.0 0.67 1 10/13/1815:12 107-06-2 ND ug/L 5.0 0.72 1 10/13/1815:12 75-35-4 ND ug/L 5.0 0.66 1 10/13/1815:12 156-59-2 ND ug/L 5.0 0.46 1 10/13/1815:12 156-60-5 ND ug/L 1.0 0.60 1 10/13/1815:12 78-87-5 ND ug/L 1.0 0.22 1 10/13/1815:12 10061-01-5 ND ug/L 1.0 0.30 1 10/13/1815:12 10061-02-6 ND ug/L 1.0 0.45 1 10/13/1815:12 100-41-4 ND ug/L 50.0 0.89 1 10/13/1815:12 591-78-6 ND ug/L 10.0 3.1 1 10/13/1815:12 74-88-4 ND ug/L 1.0 0.50 1 10/13/1815:12 75-09-2 ND ug/L 100 0.86 1 10/13/1815:12 108-10-1 ND ug/L 1.0 0.50 1 10/13/1815:12 100-42-5 ND ug/L 5.0 0.32 1 10/13/1815:12 630-20-6 ND ug/L 3.0 0.53 1 10/13/1815:12 79-34-5 ND ug/L 1.0 0.78 1 10/13/1815:12 127-18-4 ND ug/L 1.0 0.31 1 10/13/1815:12 108-88-3 ND ug/L 1.0 0.38 1 10/13/1815:12 71-55-6 ND ug/L 1.0 0.59 1 10/13/1815:12 79-00-5 ND ug/L 1.0 0.34 1 10/13/1815:12 79-01-6 ND ug/L 1.0 0.51 1 10/13/1815:12 75-69-4 ND ug/L 1.0 0.46 1 10/13/1815:12 96-18-4 ND ug/L 50.0 0.42 1 10/13/1815:12 108-05-4 ND ug/L 1.0 0.60 1 10/13/1815:12 75-01-4 ND ug/L 5.0 1.5 1 10/13/1815:12 1330-20-7 115 %. 81-119 1 10/13/1815:12 17060-07-0 96 %. 82-114 1 10/13/1815:12 1868-53-7 108 %. 82-120 1 10/13/1815:12 460-00-4 109 %. 82-109 1 10/13/1815:12 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 29 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW16 Lab ID: 2610107012 Collected: 10/02/18 11:00 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: SF 1 10/16/18 10:59 6.45 Std. Units 1 10/16/18 10:59 20.6 deg C 1 10/16/18 10:59 689 umhos/c 1 10/16/18 10:59 m 4.63 NTU 1 10/16/18 10:59 1.22 ug/L 1 10/16/18 10:59 7782-44-7 14.80 feet 1 10/16/18 10:59 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1818:12 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1818:12 7440-38-2 48.8J ug/L 100 0.78 1 10/15/1813:00 10/16/1818:12 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1818:12 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1818:12 7440-43-9 2.9J ug/L 10.0 1.6 1 10/15/1813:00 10/16/1818:12 7440-47-3 3.1J ug/L 10.0 0.52 1 10/15/1813:00 10/16/1818:12 7440-48-4 1.6J ug/L 10.0 1.3 1 10/15/1813:00 10/16/1818:12 7440-50-8 1.OJ ug/L 10.0 0.27 1 10/15/1813:00 10/16/1818:12 7439-92-1 3.6J ug/L 50.0 0.95 1 10/15/1813:00 10/16/1818:12 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1818:12 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1818:12 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1818:12 7440-28-0 11.4J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1818:12 7440-62-2 9.4J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1818:12 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.077J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1812:13 7439-97-6 Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/12/1818:28 123-91-1 102 % 50-150 105 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/12/18 18:28 17060-07-0 1 10/12/1818:28 2037-26-5 8.2 1 10/15/18 23:40 67-64-1 2.5 1 10/15/18 23:40 107-13-1 0.20 1 10/15/18 23:40 71-43-2 0.50 1 10/15/18 23:40 74-97-5 0.36 1 10/15/18 23:40 75-27-4 0.55 1 10/15/18 23:40 75-25-2 0.95 1 10/15/18 23:40 74-83-9 3.2 1 10/15/18 23:40 78-93-3 0.79 1 10/15/18 23:40 75-15-0 0.42 1 10/15/18 23:40 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 30 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW16 Lab ID: 2610107012 Collected: 10/02/18 11:00 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/15/18 23:40 108-90-7 ND ug/L 10.0 0.52 1 10/15/18 23:40 75-00-3 ND ug/L 5.0 0.58 1 10/15/18 23:40 67-66-3 ND ug/L 1.0 0.38 1 10/15/18 23:40 74-87-3 ND ug/L 13.0 0.55 1 10/15/18 23:40 96-12-8 ND ug/L 3.0 0.31 1 10/15/18 23:40 124-48-1 ND ug/L 2.0 0.28 1 10/15/18 23:40 106-93-4 ND ug/L 10.0 0.62 1 10/15/18 23:40 74-95-3 ND ug/L 5.0 0.49 1 10/15/18 23:40 95-50-1 ND ug/L 1.0 0.58 1 10/15/18 23:40 106-46-7 ND ug/L 100 1.6 1 10/15/18 23:40 110-57-6 ND ug/L 5.0 0.41 1 10/15/18 23:40 75-34-3 ND ug/L 1.0 0.67 1 10/15/18 23:40 107-06-2 ND ug/L 5.0 0.72 1 10/15/18 23:40 75-35-4 ND ug/L 5.0 0.66 1 10/15/18 23:40 156-59-2 ND ug/L 5.0 0.46 1 10/15/18 23:40 156-60-5 ND ug/L 1.0 0.60 1 10/15/18 23:40 78-87-5 ND ug/L 1.0 0.22 1 10/15/18 23:40 10061-01-5 ND ug/L 1.0 0.30 1 10/15/18 23:40 10061-02-6 ND ug/L 1.0 0.45 1 10/15/18 23:40 100-41-4 ND ug/L 50.0 0.89 1 10/15/18 23:40 591-78-6 ND ug/L 10.0 3.1 1 10/15/18 23:40 74-88-4 ND ug/L 1.0 0.50 1 10/15/18 23:40 75-09-2 ND ug/L 100 0.86 1 10/15/18 23:40 108-10-1 ND ug/L 1.0 0.50 1 10/15/18 23:40 100-42-5 ND ug/L 5.0 0.32 1 10/15/18 23:40 630-20-6 ND ug/L 3.0 0.53 1 10/15/18 23:40 79-34-5 ND ug/L 1.0 0.78 1 10/15/18 23:40 127-18-4 ND ug/L 1.0 0.31 1 10/15/18 23:40 108-88-3 ND ug/L 1.0 0.38 1 10/15/18 23:40 71-55-6 ND ug/L 1.0 0.59 1 10/15/18 23:40 79-00-5 ND ug/L 1.0 0.34 1 10/15/18 23:40 79-01-6 ND ug/L 1.0 0.51 1 10/15/18 23:40 75-69-4 ND ug/L 1.0 0.46 1 10/15/18 23:40 96-18-4 ND ug/L 50.0 0.42 1 10/15/18 23:40 108-05-4 ND ug/L 1.0 0.60 1 10/15/18 23:40 75-01-4 ND ug/L 5.0 1.5 1 10/15/18 23:40 1330-20-7 104 %. 81-119 1 10/15/18 23:40 17060-07-0 97 %. 82-114 1 10/15/18 23:40 1868-53-7 110 %. 82-120 1 10/15/18 23:40 460-00-4 104 %. 82-109 1 10/15/18 23:40 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 31 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW18A Lab ID: 2610107013 Collected: 10/02/18 14:19 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: WF 1 10/16/18 11:00 6.04 Std. Units 1 10/16/18 11:00 21.1 deg C 1 10/16/18 11:00 1631 umhos/c 1 10/16/18 11:00 m 0.44 NTU 1 10/16/18 11:00 1.34 ug/L 1 10/16/18 11:00 7782-44-7 15.28 feet 1 10/16/18 11:00 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1818:18 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1818:18 7440-38-2 609 ug/L 100 0.78 1 10/15/1813:00 10/16/1818:18 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1818:18 7440-41-7 0.49J ug/L 1.0 0.093 1 10/15/1813:00 10/16/1818:18 7440-43-9 2.OJ ug/L 10.0 1.6 1 10/15/1813:00 10/16/1818:18 7440-47-3 11.1 ug/L 10.0 0.52 1 10/15/1813:00 10/16/1818:18 7440-48-4 3.9J ug/L 10.0 1.3 1 10/15/1813:00 10/16/1818:18 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1818:18 7439-92-1 7.8J ug/L 50.0 0.95 1 10/15/1813:00 10/16/1818:18 7440-02-0 1.6J ug/L 10.0 1.4 1 10/15/1813:00 10/16/1818:18 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1818:18 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1818:18 7440-28-0 ND ug/L 25.0 1.9 1 10/15/1813:00 10/16/1818:18 7440-62-2 34.1 ug/L 10.0 2.1 1 10/15/1813:00 10/16/1818:18 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.083J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1812:15 7439-97-6 Analytical Method: EPA 8260B Mod. 37.9 ug/L 2.0 1.9 1 10/12/1818:48 123-91-1 103 % 50-150 106 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 1.2 ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 3.OJ ug/L 100 ND ug/L 1.0 1 10/12/18 18:48 17060-07-0 1 10/12/1818:48 2037-26-5 8.2 1 10/16/18 00:04 67-64-1 2.5 1 10/16/18 00:04 107-13-1 0.20 1 10/16/18 00:04 71-43-2 0.50 1 10/16/18 00:04 74-97-5 0.36 1 10/16/18 00:04 75-27-4 0.55 1 10/16/18 00:04 75-25-2 0.95 1 10/16/18 00:04 74-83-9 3.2 1 10/16/18 00:04 78-93-3 0.79 1 10/16/18 00:04 75-15-0 0.42 1 10/16/18 00:04 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B Page 32 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW18A Lab ID: 2610107013 Collected: 10/02/18 14:19 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E 1.4J ug/L 3.0 0.53 1 10/16/18 00:04 108-90-7 ND ug/L 10.0 0.52 1 10/16/18 00:04 75-00-3 ND ug/L 5.0 0.58 1 10/16/18 00:04 67-66-3 ND ug/L 1.0 0.38 1 10/16/18 00:04 74-87-3 ND ug/L 13.0 0.55 1 10/16/18 00:04 96-12-8 ND ug/L 3.0 0.31 1 10/16/18 00:04 124-48-1 ND ug/L 2.0 0.28 1 10/16/18 00:04 106-93-4 ND ug/L 10.0 0.62 1 10/16/18 00:04 74-95-3 ND ug/L 5.0 0.49 1 10/16/18 00:04 95-50-1 2.2 ug/L 1.0 0.58 1 10/16/18 00:04 106-46-7 ND ug/L 100 1.6 1 10/16/18 00:04 110-57-6 ND ug/L 5.0 0.41 1 10/16/18 00:04 75-34-3 ND ug/L 1.0 0.67 1 10/16/18 00:04 107-06-2 ND ug/L 5.0 0.72 1 10/16/18 00:04 75-35-4 1.6J ug/L 5.0 0.66 1 10/16/18 00:04 156-59-2 ND ug/L 5.0 0.46 1 10/16/18 00:04 156-60-5 ND ug/L 1.0 0.60 1 10/16/18 00:04 78-87-5 ND ug/L 1.0 0.22 1 10/16/18 00:04 10061-01-5 ND ug/L 1.0 0.30 1 10/16/18 00:04 10061-02-6 ND ug/L 1.0 0.45 1 10/16/18 00:04 100-41-4 ND ug/L 50.0 0.89 1 10/16/18 00:04 591-78-6 ND ug/L 10.0 3.1 1 10/16/18 00:04 74-88-4 ND ug/L 1.0 0.50 1 10/16/18 00:04 75-09-2 ND ug/L 100 0.86 1 10/16/18 00:04 108-10-1 ND ug/L 1.0 0.50 1 10/16/18 00:04 100-42-5 ND ug/L 5.0 0.32 1 10/16/18 00:04 630-20-6 ND ug/L 3.0 0.53 1 10/16/18 00:04 79-34-5 ND ug/L 1.0 0.78 1 10/16/18 00:04 127-18-4 ND ug/L 1.0 0.31 1 10/16/18 00:04 108-88-3 ND ug/L 1.0 0.38 1 10/16/18 00:04 71-55-6 ND ug/L 1.0 0.59 1 10/16/18 00:04 79-00-5 ND ug/L 1.0 0.34 1 10/16/18 00:04 79-01-6 ND ug/L 1.0 0.51 1 10/16/18 00:04 75-69-4 ND ug/L 1.0 0.46 1 10/16/18 00:04 96-18-4 ND ug/L 50.0 0.42 1 10/16/18 00:04 108-05-4 2.9 ug/L 1.0 0.60 1 10/16/18 00:04 75-01-4 ND ug/L 5.0 1.5 1 10/16/18 00:04 1330-20-7 106 %. 81-119 1 10/16/18 00:04 17060-07-0 99 %. 82-114 1 10/16/18 00:04 1868-53-7 106 %. 82-120 1 10/16/18 00:04 460-00-4 104 %. 82-109 1 10/16/18 00:04 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 33 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW19 Lab ID: 2610107014 Collected: 10/03/18 12:15 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: KR 1 10/16/18 11:01 6.37 Std. Units 1 10/16/18 11:01 19.4 deg C 1 10/16/18 11:01 1015 umhos/c 1 10/16/18 11:01 m 1.08 NTU 1 10/16/18 11:01 1.16 ug/L 1 10/16/18 11:01 7782-44-7 27.58 feet 1 10/16/18 11:01 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1818:23 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1818:23 7440-38-2 275 ug/L 100 0.78 1 10/15/1813:00 10/16/1818:23 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1818:23 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1818:23 7440-43-9 ND ug/L 10.0 1.6 1 10/15/1813:00 10/16/1818:23 7440-47-3 1.4J ug/L 10.0 0.52 1 10/15/1813:00 10/16/1818:23 7440-48-4 ND ug/L 10.0 1.3 1 10/15/1813:00 10/16/1818:23 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1818:23 7439-92-1 59.7 ug/L 50.0 0.95 1 10/15/1813:00 10/16/1818:23 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1818:23 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1818:23 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1818:23 7440-28-0 ND ug/L 25.0 1.9 1 10/15/1813:00 10/16/1818:23 7440-62-2 3.5J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1818:23 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.061J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1812:17 7439-97-6 Analytical Method: EPA 8260B Mod. 8.0 ug/L 2.0 1.9 1 10/17/1815:26 123-91-1 109 % 50-150 118 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/17/18 15:26 17060-07-0 1 10/17/1815:26 2037-26-5 8.2 1 10/16/1817:00 67-64-1 2.5 1 10/16/18 17:00 107-13-1 0.20 1 10/16/1817:00 71-43-2 0.50 1 10/16/1817:00 74-97-5 0.36 1 10/16/1817:00 75-27-4 0.55 1 10/16/1817:00 75-25-2 0.95 1 10/16/1817:00 74-83-9 3.2 1 10/16/1817:00 78-93-3 0.79 1 10/16/1817:00 75-15-0 0.42 1 10/16/1817:00 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 34 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW19 Lab ID: 2610107014 Collected: 10/03/18 12:15 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/16/1817:00 108-90-7 ND ug/L 10.0 0.52 1 10/16/1817:00 75-00-3 ND ug/L 5.0 0.58 1 10/16/1817:00 67-66-3 ND ug/L 1.0 0.38 1 10/16/1817:00 74-87-3 ND ug/L 13.0 0.55 1 10/16/1817:00 96-12-8 ND ug/L 3.0 0.31 1 10/16/1817:00 124-48-1 ND ug/L 2.0 0.28 1 10/16/1817:00 106-93-4 ND ug/L 10.0 0.62 1 10/16/1817:00 74-95-3 ND ug/L 5.0 0.49 1 10/16/1817:00 95-50-1 1.4 ug/L 1.0 0.58 1 10/16/1817:00 106-46-7 ND ug/L 100 1.6 1 10/16/1817:00 110-57-6 ND ug/L 5.0 0.41 1 10/16/1817:00 75-34-3 ND ug/L 1.0 0.67 1 10/16/1817:00 107-06-2 ND ug/L 5.0 0.72 1 10/16/1817:00 75-35-4 ND ug/L 5.0 0.66 1 10/16/1817:00 156-59-2 ND ug/L 5.0 0.46 1 10/16/1817:00 156-60-5 ND ug/L 1.0 0.60 1 10/16/1817:00 78-87-5 ND ug/L 1.0 0.22 1 10/16/1817:00 10061-01-5 ND ug/L 1.0 0.30 1 10/16/1817:00 10061-02-6 ND ug/L 1.0 0.45 1 10/16/1817:00 100-41-4 ND ug/L 50.0 0.89 1 10/16/1817:00 591-78-6 ND ug/L 10.0 3.1 1 10/16/1817:00 74-88-4 ND ug/L 1.0 0.50 1 10/16/1817:00 75-09-2 ND ug/L 100 0.86 1 10/16/1817:00 108-10-1 ND ug/L 1.0 0.50 1 10/16/1817:00 100-42-5 ND ug/L 5.0 0.32 1 10/16/1817:00 630-20-6 ND ug/L 3.0 0.53 1 10/16/1817:00 79-34-5 ND ug/L 1.0 0.78 1 10/16/1817:00 127-18-4 ND ug/L 1.0 0.31 1 10/16/1817:00 108-88-3 ND ug/L 1.0 0.38 1 10/16/1817:00 71-55-6 ND ug/L 1.0 0.59 1 10/16/1817:00 79-00-5 ND ug/L 1.0 0.34 1 10/16/1817:00 79-01-6 ND ug/L 1.0 0.51 1 10/16/1817:00 75-69-4 ND ug/L 1.0 0.46 1 10/16/1817:00 96-18-4 ND ug/L 50.0 0.42 1 10/16/1817:00 108-05-4 ND ug/L 1.0 0.60 1 10/16/1817:00 75-01-4 ND ug/L 5.0 1.5 1 10/16/1817:00 1330-20-7 98 %. 81-119 1 10/16/1817:00 17060-07-0 101 %. 82-114 1 10/16/1817:00 1868-53-7 104 %. 82-120 1 10/16/1817:00 460-00-4 94 %. 82-109 1 10/16/1817:00 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 35 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW19A Lab ID: 2610107015 Collected: 10/03/18 13:18 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: KR 1 10/16/18 11:02 7.21 Std. Units 1 10/16/18 11:02 19.6 deg C 1 10/16/18 11:02 762 umhos/c 1 10/16/18 11:02 m 1.88 NTU 1 10/16/18 11:02 2.51 ug/L 1 10/16/18 11:02 7782-44-7 28.00 feet 1 10/16/18 11:02 Analytical Method: EPA 6020B Preparation Method: EPA 3005A 1.8J ug/L 6.0 0.78 1 10/15/1813:00 10/16/1818:46 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1818:46 7440-38-2 93.3J ug/L 100 0.78 1 10/15/1813:00 10/16/1818:46 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1818:46 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1818:46 7440-43-9 ND ug/L 10.0 1.6 1 10/15/1813:00 10/16/1818:46 7440-47-3 7.6J ug/L 10.0 0.52 1 10/15/1813:00 10/16/1818:46 7440-48-4 ND ug/L 10.0 1.3 1 10/15/1813:00 10/16/1818:46 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1818:46 7439-92-1 14.OJ ug/L 50.0 0.95 1 10/15/1813:00 10/16/1818:46 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1818:46 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1818:46 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1818:46 7440-28-0 ND ug/L 25.0 1.9 1 10/15/1813:00 10/16/1818:46 7440-62-2 454 ug/L 10.0 2.1 1 10/15/1813:00 10/16/1818:46 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.079J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1812:20 7439-97-6 Analytical Method: EPA 8260B Mod. 3.6 ug/L 2.0 1.9 1 10/17/1815:46 123-91-1 104 % 50-150 113 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/17/18 15:46 17060-07-0 1 10/17/1815:46 2037-26-5 8.2 1 10/15/1813:44 67-64-1 2.5 1 10/15/18 13:44 107-13-1 0.20 1 10/15/1813:44 71-43-2 0.50 1 10/15/1813:44 74-97-5 0.36 1 10/15/1813:44 75-27-4 0.55 1 10/15/1813:44 75-25-2 0.95 1 10/15/1813:44 74-83-9 3.2 1 10/15/1813:44 78-93-3 0.79 1 10/15/1813:44 75-15-0 0.42 1 10/15/1813:44 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B Page 36 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW19A Lab ID: 2610107015 Collected: 10/03/18 13:18 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/15/1813:44 108-90-7 ND ug/L 10.0 0.52 1 10/15/1813:44 75-00-3 ND ug/L 5.0 0.58 1 10/15/1813:44 67-66-3 ND ug/L 1.0 0.38 1 10/15/1813:44 74-87-3 ND ug/L 13.0 0.55 1 10/15/1813:44 96-12-8 ND ug/L 3.0 0.31 1 10/15/1813:44 124-48-1 ND ug/L 2.0 0.28 1 10/15/1813:44 106-93-4 ND ug/L 10.0 0.62 1 10/15/1813:44 74-95-3 ND ug/L 5.0 0.49 1 10/15/1813:44 95-50-1 ND ug/L 1.0 0.58 1 10/15/1813:44 106-46-7 ND ug/L 100 1.6 1 10/15/1813:44 110-57-6 ND ug/L 5.0 0.41 1 10/15/1813:44 75-34-3 ND ug/L 1.0 0.67 1 10/15/1813:44 107-06-2 ND ug/L 5.0 0.72 1 10/15/1813:44 75-35-4 ND ug/L 5.0 0.66 1 10/15/1813:44 156-59-2 ND ug/L 5.0 0.46 1 10/15/1813:44 156-60-5 ND ug/L 1.0 0.60 1 10/15/1813:44 78-87-5 ND ug/L 1.0 0.22 1 10/15/1813:44 10061-01-5 ND ug/L 1.0 0.30 1 10/15/1813:44 10061-02-6 ND ug/L 1.0 0.45 1 10/15/1813:44 100-41-4 ND ug/L 50.0 0.89 1 10/15/1813:44 591-78-6 ND ug/L 10.0 3.1 1 10/15/1813:44 74-88-4 ND ug/L 1.0 0.50 1 10/15/1813:44 75-09-2 ND ug/L 100 0.86 1 10/15/1813:44 108-10-1 ND ug/L 1.0 0.50 1 10/15/1813:44 100-42-5 ND ug/L 5.0 0.32 1 10/15/1813:44 630-20-6 ND ug/L 3.0 0.53 1 10/15/1813:44 79-34-5 ND ug/L 1.0 0.78 1 10/15/1813:44 127-18-4 ND ug/L 1.0 0.31 1 10/15/1813:44 108-88-3 ND ug/L 1.0 0.38 1 10/15/1813:44 71-55-6 ND ug/L 1.0 0.59 1 10/15/1813:44 79-00-5 ND ug/L 1.0 0.34 1 10/15/1813:44 79-01-6 ND ug/L 1.0 0.51 1 10/15/1813:44 75-69-4 ND ug/L 1.0 0.46 1 10/15/1813:44 96-18-4 ND ug/L 50.0 0.42 1 10/15/1813:44 108-05-4 ND ug/L 1.0 0.60 1 10/15/1813:44 75-01-4 ND ug/L 5.0 1.5 1 10/15/1813:44 1330-20-7 100 %. 81-119 1 10/15/1813:44 17060-07-0 93 %. 82-114 1 10/15/1813:44 1868-53-7 105 %. 82-120 1 10/15/1813:44 460-00-4 101 %. 82-109 1 10/15/1813:44 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 37 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW19AR Lab ID: 2610107016 Collected: 10/03/18 11:15 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: SF 1 10/16/18 11:02 6.40 Std. Units 1 10/16/18 11:02 19.0 deg C 1 10/16/18 11:02 2777 umhos/c 1 10/16/18 11:02 m 7.10 NTU 1 10/16/18 11:02 1.26 ug/L 1 10/16/18 11:02 7782-44-7 24.21 feet 1 10/16/18 11:02 Analytical Method: EPA 6020B Preparation Method: EPA 3005A 0.87J ug/L 6.0 0.78 1 10/15/1813:00 10/16/1819:03 7440-36-0 0.74J ug/L 10.0 0.57 1 10/15/1813:00 10/16/1819:03 7440-38-2 280 ug/L 100 0.78 1 10/15/1813:00 10/16/1819:03 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1819:03 7440-41-7 0.92J ug/L 1.0 0.093 1 10/15/1813:00 10/16/1819:03 7440-43-9 19.7 ug/L 10.0 1.6 1 10/15/1813:00 10/16/1819:03 7440-47-3 22.6 ug/L 10.0 0.52 1 10/15/1813:00 10/16/1819:03 7440-48-4 14.3 ug/L 10.0 1.3 1 10/15/1813:00 10/16/1819:03 7440-50-8 0.63J ug/L 10.0 0.27 1 10/15/1813:00 10/16/1819:03 7439-92-1 58.2 ug/L 50.0 0.95 1 10/15/1813:00 10/16/1819:03 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1819:03 7782-49-2 2.1J ug/L 10.0 0.95 1 10/15/1813:00 10/16/1819:03 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1819:03 7440-28-0 5.7J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1819:03 7440-62-2 30.5 ug/L 10.0 2.1 1 10/15/1813:00 10/16/1819:03 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.13J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1812:22 7439-97-6 Analytical Method: EPA 8260B Mod. 55.8 ug/L 2.0 1.9 1 10/12/1815:14 123-91-1 110 % 50-150 108 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 1.0 ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/12/18 15:14 17060-07-0 1 10/12/1815:14 2037-26-5 8.2 1 10/15/1814:10 67-64-1 2.5 1 10/15/18 14:10 107-13-1 0.20 1 10/15/1814:10 71-43-2 0.50 1 10/15/1814:10 74-97-5 0.36 1 10/15/1814:10 75-27-4 0.55 1 10/15/1814:10 75-25-2 0.95 1 10/15/1814:10 74-83-9 3.2 1 10/15/1814:10 78-93-3 0.79 1 10/15/1814:10 75-15-0 0.42 1 10/15/1814:10 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B Page 38 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW19AR Lab ID: 2610107016 Collected: 10/03/18 11:15 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E 3.2 ug/L 3.0 0.53 1 10/15/1814:10 108-90-7 ND ug/L 10.0 0.52 1 10/15/1814:10 75-00-3 ND ug/L 5.0 0.58 1 10/15/1814:10 67-66-3 ND ug/L 1.0 0.38 1 10/15/1814:10 74-87-3 ND ug/L 13.0 0.55 1 10/15/1814:10 96-12-8 ND ug/L 3.0 0.31 1 10/15/1814:10 124-48-1 ND ug/L 2.0 0.28 1 10/15/1814:10 106-93-4 ND ug/L 10.0 0.62 1 10/15/1814:10 74-95-3 ND ug/L 5.0 0.49 1 10/15/1814:10 95-50-1 6.4 ug/L 1.0 0.58 1 10/15/1814:10 106-46-7 ND ug/L 100 1.6 1 10/15/1814:10 110-57-6 1.1J ug/L 5.0 0.41 1 10/15/1814:10 75-34-3 ND ug/L 1.0 0.67 1 10/15/1814:10 107-06-2 ND ug/L 5.0 0.72 1 10/15/1814:10 75-35-4 ND ug/L 5.0 0.66 1 10/15/1814:10 156-59-2 ND ug/L 5.0 0.46 1 10/15/1814:10 156-60-5 ND ug/L 1.0 0.60 1 10/15/1814:10 78-87-5 ND ug/L 1.0 0.22 1 10/15/1814:10 10061-01-5 ND ug/L 1.0 0.30 1 10/15/1814:10 10061-02-6 ND ug/L 1.0 0.45 1 10/15/1814:10 100-41-4 ND ug/L 50.0 0.89 1 10/15/1814:10 591-78-6 ND ug/L 10.0 3.1 1 10/15/1814:10 74-88-4 ND ug/L 1.0 0.50 1 10/15/1814:10 75-09-2 ND ug/L 100 0.86 1 10/15/1814:10 108-10-1 ND ug/L 1.0 0.50 1 10/15/1814:10 100-42-5 ND ug/L 5.0 0.32 1 10/15/1814:10 630-20-6 ND ug/L 3.0 0.53 1 10/15/1814:10 79-34-5 ND ug/L 1.0 0.78 1 10/15/1814:10 127-18-4 ND ug/L 1.0 0.31 1 10/15/1814:10 108-88-3 ND ug/L 1.0 0.38 1 10/15/1814:10 71-55-6 ND ug/L 1.0 0.59 1 10/15/1814:10 79-00-5 ND ug/L 1.0 0.34 1 10/15/1814:10 79-01-6 ND ug/L 1.0 0.51 1 10/15/1814:10 75-69-4 ND ug/L 1.0 0.46 1 10/15/1814:10 96-18-4 ND ug/L 50.0 0.42 1 10/15/1814:10 108-05-4 ND ug/L 1.0 0.60 1 10/15/1814:10 75-01-4 ND ug/L 5.0 1.5 1 10/15/1814:10 1330-20-7 101 %. 81-119 1 10/15/1814:10 17060-07-0 100 %. 82-114 1 10/15/1814:10 1868-53-7 104 %. 82-120 1 10/15/1814:10 460-00-4 99 %. 82-109 1 10/15/1814:10 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 39 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW19R Lab ID: 2610107017 Collected: 10/03/18 10:54 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: SF 1 10/16/18 11:03 6.23 Std. Units 1 10/16/18 11:03 18.1 deg C 1 10/16/18 11:03 2621 umhos/c 1 10/16/18 11:03 m 3.23 NTU 1 10/16/18 11:03 1.68 ug/L 1 10/16/18 11:03 7782-44-7 23.35 feet 1 10/16/18 11:03 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1819:09 7440-36-0 0.68J ug/L 10.0 0.57 1 10/15/1813:00 10/16/1819:09 7440-38-2 817 ug/L 100 0.78 1 10/15/1813:00 10/16/1819:09 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1819:09 7440-41-7 0.69J ug/L 1.0 0.093 1 10/15/1813:00 10/16/1819:09 7440-43-9 1.7J ug/L 10.0 1.6 1 10/15/1813:00 10/16/1819:09 7440-47-3 35.5 ug/L 10.0 0.52 1 10/15/1813:00 10/16/1819:09 7440-48-4 16.4 ug/L 10.0 1.3 1 10/15/1813:00 10/16/1819:09 7440-50-8 0.47J ug/L 10.0 0.27 1 10/15/1813:00 10/16/1819:09 7439-92-1 52.8 ug/L 50.0 0.95 1 10/15/1813:00 10/16/1819:09 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1819:09 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1819:09 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1819:09 7440-28-0 3.1J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1819:09 7440-62-2 17.6 ug/L 10.0 2.1 1 10/15/1813:00 10/16/1819:09 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.083J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1812:24 7439-97-6 Analytical Method: EPA 8260B Mod. 52.6 ug/L 2.0 1.9 1 10/17/1818:02 123-91-1 103 % 50-150 123 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 0.73J ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/17/18 18:02 17060-07-0 1 10/17/1818:02 2037-26-5 8.2 1 10/12/18 23:28 67-64-1 2.5 1 10/12/18 23:28 107-13-1 0.20 1 10/12/18 23:28 71-43-2 0.50 1 10/12/18 23:28 74-97-5 0.36 1 10/12/18 23:28 75-27-4 0.55 1 10/12/18 23:28 75-25-2 0.95 1 10/12/18 23:28 74-83-9 3.2 1 10/12/18 23:28 78-93-3 0.79 1 10/12/18 23:28 75-15-0 0.42 1 10/12/18 23:28 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 40 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW19R Lab ID: 2610107017 Collected: 10/03/18 10:54 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E 1.9J ug/L 3.0 0.53 1 10/12/18 23:28 108-90-7 ND ug/L 10.0 0.52 1 10/12/18 23:28 75-00-3 ND ug/L 5.0 0.58 1 10/12/18 23:28 67-66-3 ND ug/L 1.0 0.38 1 10/12/18 23:28 74-87-3 ND ug/L 13.0 0.55 1 10/12/18 23:28 96-12-8 ND ug/L 3.0 0.31 1 10/12/18 23:28 124-48-1 ND ug/L 2.0 0.28 1 10/12/18 23:28 106-93-4 ND ug/L 10.0 0.62 1 10/12/18 23:28 74-95-3 ND ug/L 5.0 0.49 1 10/12/18 23:28 95-50-1 6.1 ug/L 1.0 0.58 1 10/12/18 23:28 106-46-7 ND ug/L 100 1.6 1 10/12/18 23:28 110-57-6 ND ug/L 5.0 0.41 1 10/12/18 23:28 75-34-3 ND ug/L 1.0 0.67 1 10/12/18 23:28 107-06-2 ND ug/L 5.0 0.72 1 10/12/18 23:28 75-35-4 ND ug/L 5.0 0.66 1 10/12/18 23:28 156-59-2 ND ug/L 5.0 0.46 1 10/12/18 23:28 156-60-5 ND ug/L 1.0 0.60 1 10/12/18 23:28 78-87-5 ND ug/L 1.0 0.22 1 10/12/18 23:28 10061-01-5 ND ug/L 1.0 0.30 1 10/12/18 23:28 10061-02-6 ND ug/L 1.0 0.45 1 10/12/18 23:28 100-41-4 ND ug/L 50.0 0.89 1 10/12/18 23:28 591-78-6 ND ug/L 10.0 3.1 1 10/12/18 23:28 74-88-4 ND ug/L 1.0 0.50 1 10/12/18 23:28 75-09-2 ND ug/L 100 0.86 1 10/12/18 23:28 108-10-1 ND ug/L 1.0 0.50 1 10/12/18 23:28 100-42-5 ND ug/L 5.0 0.32 1 10/12/18 23:28 630-20-6 ND ug/L 3.0 0.53 1 10/12/18 23:28 79-34-5 ND ug/L 1.0 0.78 1 10/12/18 23:28 127-18-4 ND ug/L 1.0 0.31 1 10/12/18 23:28 108-88-3 ND ug/L 1.0 0.38 1 10/12/18 23:28 71-55-6 ND ug/L 1.0 0.59 1 10/12/18 23:28 79-00-5 ND ug/L 1.0 0.34 1 10/12/18 23:28 79-01-6 ND ug/L 1.0 0.51 1 10/12/18 23:28 75-69-4 ND ug/L 1.0 0.46 1 10/12/18 23:28 96-18-4 ND ug/L 50.0 0.42 1 10/12/18 23:28 108-05-4 ND ug/L 1.0 0.60 1 10/12/18 23:28 75-01-4 ND ug/L 5.0 1.5 1 10/12/18 23:28 1330-20-7 98 %. 81-119 1 10/12/18 23:28 17060-07-0 94 %. 82-114 1 10/12/18 23:28 1868-53-7 107 %. 82-120 1 10/12/18 23:28 460-00-4 98 %. 82-109 1 10/12/18 23:28 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 41 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW20AR Lab ID: 2610107018 Collected: 10/02/18 14:00 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: KR 1 10/16/18 11:03 6.20 Std. Units 1 10/16/18 11:03 18.7 deg C 1 10/16/18 11:03 615 umhos/c 1 10/16/18 11:03 m 3.59 NTU 1 10/16/18 11:03 1.52 ug/L 1 10/16/18 11:03 7782-44-7 N2 10.32 feet 1 10/16/18 11:03 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1819:15 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1819:15 7440-38-2 206 ug/L 100 0.78 1 10/15/1813:00 10/16/1819:15 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1819:15 7440-41-7 0.18J ug/L 1.0 0.093 1 10/15/1813:00 10/16/1819:15 7440-43-9 ND ug/L 10.0 1.6 1 10/15/1813:00 10/16/1819:15 7440-47-3 1.5J ug/L 10.0 0.52 1 10/15/1813:00 10/16/1819:15 7440-48-4 1.9J ug/L 10.0 1.3 1 10/15/1813:00 10/16/1819:15 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1819:15 7439-92-1 26.8J ug/L 50.0 0.95 1 10/15/1813:00 10/16/1819:15 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1819:15 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1819:15 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1819:15 7440-28-0 ND ug/L 25.0 1.9 1 10/15/1813:00 10/16/1819:15 7440-62-2 21.7 ug/L 10.0 2.1 1 10/15/1813:00 10/16/1819:15 7440-66-6 B Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.10J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1812:27 7439-97-6 B Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/29/1813:36 123-91-1 H3 97 % 50-150 1 10/29/1813:36 17060-07-0 97 % 50-150 1 10/29/1813:36 2037-26-5 Analytical Method: EPA 8260E ND ug/L 100 8.2 1 10/16/18 00:29 67-64-1 ND ug/L 200 2.5 1 10/16/18 00:29 107-13-1 ND ug/L 1.0 0.20 1 10/16/18 00:29 71-43-2 ND ug/L 3.0 0.50 1 10/16/18 00:29 74-97-5 ND ug/L 1.0 0.36 1 10/16/18 00:29 75-27-4 ND ug/L 3.0 0.55 1 10/16/18 00:29 75-25-2 ND ug/L 10.0 0.95 1 10/16/18 00:29 74-83-9 ND ug/L 100 3.2 1 10/16/18 00:29 78-93-3 ND ug/L 100 0.79 1 10/16/18 00:29 75-15-0 ND ug/L 1.0 0.42 1 10/16/18 00:29 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 42 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW20AR Lab ID: 2610107018 Collected: 10/02/18 14:00 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/16/18 00:29 108-90-7 ND ug/L 10.0 0.52 1 10/16/18 00:29 75-00-3 ND ug/L 5.0 0.58 1 10/16/18 00:29 67-66-3 ND ug/L 1.0 0.38 1 10/16/18 00:29 74-87-3 ND ug/L 13.0 0.55 1 10/16/18 00:29 96-12-8 ND ug/L 3.0 0.31 1 10/16/18 00:29 124-48-1 ND ug/L 2.0 0.28 1 10/16/18 00:29 106-93-4 ND ug/L 10.0 0.62 1 10/16/18 00:29 74-95-3 ND ug/L 5.0 0.49 1 10/16/18 00:29 95-50-1 ND ug/L 1.0 0.58 1 10/16/18 00:29 106-46-7 ND ug/L 100 1.6 1 10/16/18 00:29 110-57-6 ND ug/L 5.0 0.41 1 10/16/18 00:29 75-34-3 ND ug/L 1.0 0.67 1 10/16/18 00:29 107-06-2 ND ug/L 5.0 0.72 1 10/16/18 00:29 75-35-4 ND ug/L 5.0 0.66 1 10/16/18 00:29 156-59-2 ND ug/L 5.0 0.46 1 10/16/18 00:29 156-60-5 ND ug/L 1.0 0.60 1 10/16/18 00:29 78-87-5 ND ug/L 1.0 0.22 1 10/16/18 00:29 10061-01-5 ND ug/L 1.0 0.30 1 10/16/18 00:29 10061-02-6 ND ug/L 1.0 0.45 1 10/16/18 00:29 100-41-4 ND ug/L 50.0 0.89 1 10/16/18 00:29 591-78-6 ND ug/L 10.0 3.1 1 10/16/18 00:29 74-88-4 ND ug/L 1.0 0.50 1 10/16/18 00:29 75-09-2 ND ug/L 100 0.86 1 10/16/18 00:29 108-10-1 ND ug/L 1.0 0.50 1 10/16/18 00:29 100-42-5 ND ug/L 5.0 0.32 1 10/16/18 00:29 630-20-6 ND ug/L 3.0 0.53 1 10/16/18 00:29 79-34-5 ND ug/L 1.0 0.78 1 10/16/18 00:29 127-18-4 ND ug/L 1.0 0.31 1 10/16/18 00:29 108-88-3 ND ug/L 1.0 0.38 1 10/16/18 00:29 71-55-6 ND ug/L 1.0 0.59 1 10/16/18 00:29 79-00-5 ND ug/L 1.0 0.34 1 10/16/18 00:29 79-01-6 ND ug/L 1.0 0.51 1 10/16/18 00:29 75-69-4 ND ug/L 1.0 0.46 1 10/16/18 00:29 96-18-4 ND ug/L 50.0 0.42 1 10/16/18 00:29 108-05-4 ND ug/L 1.0 0.60 1 10/16/18 00:29 75-01-4 ND ug/L 5.0 1.5 1 10/16/18 00:29 1330-20-7 105 %. 81-119 1 10/16/18 00:29 17060-07-0 96 %. 82-114 1 10/16/18 00:29 1868-53-7 109 %. 82-120 1 10/16/18 00:29 460-00-4 106 %. 82-109 1 10/16/18 00:29 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 43 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW20B Lab ID: 2610107019 Collected: 10/02/18 14:49 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: KR 1 10/16/18 11:04 6.23 Std. Units 1 10/16/18 11:04 20.1 deg C 1 10/16/18 11:04 1.13 umhos/c 1 10/16/18 11:04 m 3.72 NTU 1 10/16/18 11:04 1.19 ug/L 1 10/16/18 11:04 7782-44-7 6.73 feet 1 10/16/18 11:04 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1819:21 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1819:21 7440-38-2 784 ug/L 100 0.78 1 10/15/1813:00 10/16/1819:21 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1819:21 7440-41-7 1.5 ug/L 1.0 0.093 1 10/15/1813:00 10/16/1819:21 7440-43-9 ND ug/L 10.0 1.6 1 10/15/1813:00 10/16/1819:21 7440-47-3 8.8J ug/L 10.0 0.52 1 10/15/1813:00 10/16/1819:21 7440-48-4 4.9J ug/L 10.0 1.3 1 10/15/1813:00 10/16/1819:21 7440-50-8 0.74J ug/L 10.0 0.27 1 10/15/1813:00 10/16/1819:21 7439-92-1 40.6J ug/L 50.0 0.95 1 10/15/1813:00 10/16/1819:21 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1819:21 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1819:21 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1819:21 7440-28-0 ND ug/L 25.0 1.9 1 10/15/1813:00 10/16/1819:21 7440-62-2 51.0 ug/L 10.0 2.1 1 10/15/1813:00 10/16/1819:21 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.12J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1812:29 7439-97-6 Analytical Method: EPA 8260B Mod. 3.7 ug/L 2.0 1.9 1 10/12/1819:27 123-91-1 107 % 50-150 107 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 0.25J ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/12/18 19:27 17060-07-0 1 10/12/1819:27 2037-26-5 8.2 1 10/16/1817:29 67-64-1 2.5 1 10/16/18 17:29 107-13-1 0.20 1 10/16/1817:29 71-43-2 0.50 1 10/16/1817:29 74-97-5 0.36 1 10/16/1817:29 75-27-4 0.55 1 10/16/1817:29 75-25-2 0.95 1 10/16/1817:29 74-83-9 3.2 1 10/16/1817:29 78-93-3 0.79 1 10/16/1817:29 75-15-0 0.42 1 10/16/1817:29 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B Page 44 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW20B Lab ID: 2610107019 Collected: 10/02/18 14:49 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/16/1817:29 108-90-7 ND ug/L 10.0 0.52 1 10/16/1817:29 75-00-3 ND ug/L 5.0 0.58 1 10/16/1817:29 67-66-3 ND ug/L 1.0 0.38 1 10/16/1817:29 74-87-3 ND ug/L 13.0 0.55 1 10/16/1817:29 96-12-8 ND ug/L 3.0 0.31 1 10/16/1817:29 124-48-1 ND ug/L 2.0 0.28 1 10/16/1817:29 106-93-4 ND ug/L 10.0 0.62 1 10/16/1817:29 74-95-3 ND ug/L 5.0 0.49 1 10/16/1817:29 95-50-1 2.8 ug/L 1.0 0.58 1 10/16/1817:29 106-46-7 ND ug/L 100 1.6 1 10/16/1817:29 110-57-6 2.1J ug/L 5.0 0.41 1 10/16/1817:29 75-34-3 ND ug/L 1.0 0.67 1 10/16/1817:29 107-06-2 ND ug/L 5.0 0.72 1 10/16/1817:29 75-35-4 ND ug/L 5.0 0.66 1 10/16/1817:29 156-59-2 ND ug/L 5.0 0.46 1 10/16/1817:29 156-60-5 ND ug/L 1.0 0.60 1 10/16/1817:29 78-87-5 ND ug/L 1.0 0.22 1 10/16/1817:29 10061-01-5 ND ug/L 1.0 0.30 1 10/16/1817:29 10061-02-6 ND ug/L 1.0 0.45 1 10/16/1817:29 100-41-4 ND ug/L 50.0 0.89 1 10/16/1817:29 591-78-6 ND ug/L 10.0 3.1 1 10/16/1817:29 74-88-4 ND ug/L 1.0 0.50 1 10/16/1817:29 75-09-2 ND ug/L 100 0.86 1 10/16/1817:29 108-10-1 ND ug/L 1.0 0.50 1 10/16/1817:29 100-42-5 ND ug/L 5.0 0.32 1 10/16/1817:29 630-20-6 ND ug/L 3.0 0.53 1 10/16/1817:29 79-34-5 ND ug/L 1.0 0.78 1 10/16/1817:29 127-18-4 ND ug/L 1.0 0.31 1 10/16/1817:29 108-88-3 ND ug/L 1.0 0.38 1 10/16/1817:29 71-55-6 ND ug/L 1.0 0.59 1 10/16/1817:29 79-00-5 ND ug/L 1.0 0.34 1 10/16/1817:29 79-01-6 ND ug/L 1.0 0.51 1 10/16/1817:29 75-69-4 ND ug/L 1.0 0.46 1 10/16/1817:29 96-18-4 ND ug/L 50.0 0.42 1 10/16/1817:29 108-05-4 ND ug/L 1.0 0.60 1 10/16/1817:29 75-01-4 ND ug/L 5.0 1.5 1 10/16/1817:29 1330-20-7 100 %. 81-119 1 10/16/1817:29 17060-07-0 102 %. 82-114 1 10/16/1817:29 1868-53-7 106 %. 82-120 1 10/16/1817:29 460-00-4 94 %. 82-109 1 10/16/1817:29 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. R1 Page 45 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW21 Lab ID: 2610107020 Collected: 10/03/18 10:14 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: SF 1 10/16/18 11:05 6.62 Std. Units 1 10/16/18 11:05 20.8 deg C 1 10/16/18 11:05 448 umhos/c 1 10/16/18 11:05 m 5.86 NTU 1 10/16/18 11:05 2.52 ug/L 1 10/16/18 11:05 7782-44-7 13.73 feet 1 10/16/18 11:05 Analytical Method: EPA 6020B Preparation Method: EPA 3005A 0.86J ug/L 6.0 0.78 1 10/15/1813:00 10/16/1819:26 7440-36-0 1.2J ug/L 10.0 0.57 1 10/15/1813:00 10/16/1819:26 7440-38-2 131 ug/L 100 0.78 1 10/15/1813:00 10/16/1819:26 7440-39-3 ND ug/L 1.0 0.50 10 10/15/1813:00 10/22/1814:35 7440-41-7 0.29J ug/L 1.0 0.093 1 10/15/1813:00 10/16/1819:26 7440-43-9 92.7 ug/L 10.0 1.6 1 10/15/1813:00 10/16/1819:26 7440-47-3 1680 ug/L 50.0 2.6 5 10/15/1813:00 10/22/1814:21 7440-48-4 688 ug/L 10.0 1.3 1 10/15/1813:00 10/16/1819:26 7440-50-8 8.OJ ug/L 10.0 0.27 1 10/15/1813:00 10/16/1819:26 7439-92-1 170 ug/L 50.0 0.95 1 10/15/1813:00 10/16/1819:26 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1819:26 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1819:26 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1819:26 7440-28-0 55.4 ug/L 25.0 1.9 1 10/15/1813:00 10/16/1819:26 7440-62-2 127 ug/L 10.0 2.1 1 10/15/1813:00 10/16/1819:26 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.13J ug/L 0.20 0.036 1 10/15/1815:25 10/16/1812:32 7439-97-6 Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/17/1816:05 123-91-1 101 % 50-150 114 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/17/18 16:05 17060-07-0 1 10/17/1816:05 2037-26-5 8.2 1 10/15/1814:35 67-64-1 2.5 1 10/15/18 14:35 107-13-1 0.20 1 10/15/1814:35 71-43-2 0.50 1 10/15/1814:35 74-97-5 0.36 1 10/15/1814:35 75-27-4 0.55 1 10/15/1814:35 75-25-2 0.95 1 10/15/1814:35 74-83-9 3.2 1 10/15/1814:35 78-93-3 0.79 1 10/15/1814:35 75-15-0 0.42 1 10/15/1814:35 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B Page 46 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW21 Lab ID: 2610107020 Collected: 10/03/18 10:14 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/15/1814:35 108-90-7 ND ug/L 10.0 0.52 1 10/15/1814:35 75-00-3 ND ug/L 5.0 0.58 1 10/15/1814:35 67-66-3 ND ug/L 1.0 0.38 1 10/15/1814:35 74-87-3 ND ug/L 13.0 0.55 1 10/15/1814:35 96-12-8 ND ug/L 3.0 0.31 1 10/15/1814:35 124-48-1 ND ug/L 2.0 0.28 1 10/15/1814:35 106-93-4 ND ug/L 10.0 0.62 1 10/15/1814:35 74-95-3 ND ug/L 5.0 0.49 1 10/15/1814:35 95-50-1 ND ug/L 1.0 0.58 1 10/15/1814:35 106-46-7 ND ug/L 100 1.6 1 10/15/1814:35 110-57-6 ND ug/L 5.0 0.41 1 10/15/1814:35 75-34-3 ND ug/L 1.0 0.67 1 10/15/1814:35 107-06-2 ND ug/L 5.0 0.72 1 10/15/1814:35 75-35-4 ND ug/L 5.0 0.66 1 10/15/1814:35 156-59-2 ND ug/L 5.0 0.46 1 10/15/1814:35 156-60-5 ND ug/L 1.0 0.60 1 10/15/1814:35 78-87-5 ND ug/L 1.0 0.22 1 10/15/1814:35 10061-01-5 ND ug/L 1.0 0.30 1 10/15/1814:35 10061-02-6 ND ug/L 1.0 0.45 1 10/15/1814:35 100-41-4 ND ug/L 50.0 0.89 1 10/15/1814:35 591-78-6 ND ug/L 10.0 3.1 1 10/15/1814:35 74-88-4 ND ug/L 1.0 0.50 1 10/15/1814:35 75-09-2 ND ug/L 100 0.86 1 10/15/1814:35 108-10-1 ND ug/L 1.0 0.50 1 10/15/1814:35 100-42-5 ND ug/L 5.0 0.32 1 10/15/1814:35 630-20-6 ND ug/L 3.0 0.53 1 10/15/1814:35 79-34-5 ND ug/L 1.0 0.78 1 10/15/1814:35 127-18-4 ND ug/L 1.0 0.31 1 10/15/1814:35 108-88-3 ND ug/L 1.0 0.38 1 10/15/1814:35 71-55-6 ND ug/L 1.0 0.59 1 10/15/1814:35 79-00-5 ND ug/L 1.0 0.34 1 10/15/1814:35 79-01-6 ND ug/L 1.0 0.51 1 10/15/1814:35 75-69-4 ND ug/L 1.0 0.46 1 10/15/1814:35 96-18-4 ND ug/L 50.0 0.42 1 10/15/1814:35 108-05-4 ND ug/L 1.0 0.60 1 10/15/1814:35 75-01-4 ND ug/L 5.0 1.5 1 10/15/1814:35 1330-20-7 102 %. 81-119 1 10/15/1814:35 17060-07-0 96 %. 82-114 1 10/15/1814:35 1868-53-7 103 %. 82-120 1 10/15/1814:35 460-00-4 96 %. 82-109 1 10/15/1814:35 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 47 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW22 Lab ID: 2610107021 Collected: 10/01/18 12:50 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: KR 1 10/16/18 11:05 6.29 Std. Units 1 10/16/18 11:05 24.8 deg C 1 10/16/18 11:05 1462 umhos/c 1 10/16/18 11:05 m 4.19 NTU 1 10/16/18 11:05 2.35 ug/L 1 10/16/18 11:05 7782-44-7 5.27 feet 1 10/16/18 11:05 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1812:49 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1812:49 7440-38-2 206 ug/L 100 0.78 1 10/15/1813:00 10/16/1812:49 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1812:49 7440-41-7 0.18J ug/L 1.0 0.093 1 10/15/1813:00 10/16/1812:49 7440-43-9 2.8J ug/L 10.0 1.6 1 10/15/1813:00 10/16/1812:49 7440-47-3 52.9 ug/L 10.0 0.52 1 10/15/1813:00 10/16/1812:49 7440-48-4 35.6 ug/L 10.0 1.3 1 10/15/1813:00 10/16/1812:49 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1812:49 7439-92-1 56.9 ug/L 50.0 0.95 1 10/15/1813:00 10/16/1812:49 7440-02-0 1.9J ug/L 10.0 1.4 1 10/15/1813:00 10/16/1812:49 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1812:49 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1812:49 7440-28-0 5.OJ ug/L 25.0 1.9 1 10/15/1813:00 10/16/1812:49 7440-62-2 6.3J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1812:49 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A ND ug/L 0.20 0.036 1 10/15/1816:08 10/16/1813:22 7439-97-6 Analytical Method: EPA 8260B Mod. 23.7 ug/L 2.0 1.9 1 10/12/1815:33 123-91-1 106 % 50-150 108 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/12/18 15:33 17060-07-0 1 10/12/1815:33 2037-26-5 8.2 1 10/12/18 23:58 67-64-1 2.5 1 10/12/18 23:58 107-13-1 0.20 1 10/12/18 23:58 71-43-2 0.50 1 10/12/18 23:58 74-97-5 0.36 1 10/12/18 23:58 75-27-4 0.55 1 10/12/18 23:58 75-25-2 0.95 1 10/12/18 23:58 74-83-9 3.2 1 10/12/18 23:58 78-93-3 0.79 1 10/12/18 23:58 75-15-0 0.42 1 10/12/18 23:58 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B Page 48 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW22 Lab ID: 2610107021 Collected: 10/01/18 12:50 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/12/18 23:58 108-90-7 ND ug/L 10.0 0.52 1 10/12/18 23:58 75-00-3 ND ug/L 5.0 0.58 1 10/12/18 23:58 67-66-3 ND ug/L 1.0 0.38 1 10/12/18 23:58 74-87-3 ND ug/L 13.0 0.55 1 10/12/18 23:58 96-12-8 ND ug/L 3.0 0.31 1 10/12/18 23:58 124-48-1 ND ug/L 2.0 0.28 1 10/12/18 23:58 106-93-4 ND ug/L 10.0 0.62 1 10/12/18 23:58 74-95-3 ND ug/L 5.0 0.49 1 10/12/18 23:58 95-50-1 ND ug/L 1.0 0.58 1 10/12/18 23:58 106-46-7 ND ug/L 100 1.6 1 10/12/18 23:58 110-57-6 ND ug/L 5.0 0.41 1 10/12/18 23:58 75-34-3 ND ug/L 1.0 0.67 1 10/12/18 23:58 107-06-2 ND ug/L 5.0 0.72 1 10/12/18 23:58 75-35-4 ND ug/L 5.0 0.66 1 10/12/18 23:58 156-59-2 ND ug/L 5.0 0.46 1 10/12/18 23:58 156-60-5 ND ug/L 1.0 0.60 1 10/12/18 23:58 78-87-5 ND ug/L 1.0 0.22 1 10/12/18 23:58 10061-01-5 ND ug/L 1.0 0.30 1 10/12/18 23:58 10061-02-6 ND ug/L 1.0 0.45 1 10/12/18 23:58 100-41-4 ND ug/L 50.0 0.89 1 10/12/18 23:58 591-78-6 ND ug/L 10.0 3.1 1 10/12/18 23:58 74-88-4 ND ug/L 1.0 0.50 1 10/12/18 23:58 75-09-2 ND ug/L 100 0.86 1 10/12/18 23:58 108-10-1 ND ug/L 1.0 0.50 1 10/12/18 23:58 100-42-5 ND ug/L 5.0 0.32 1 10/12/18 23:58 630-20-6 ND ug/L 3.0 0.53 1 10/12/18 23:58 79-34-5 ND ug/L 1.0 0.78 1 10/12/18 23:58 127-18-4 ND ug/L 1.0 0.31 1 10/12/18 23:58 108-88-3 ND ug/L 1.0 0.38 1 10/12/18 23:58 71-55-6 ND ug/L 1.0 0.59 1 10/12/18 23:58 79-00-5 ND ug/L 1.0 0.34 1 10/12/18 23:58 79-01-6 ND ug/L 1.0 0.51 1 10/12/18 23:58 75-69-4 ND ug/L 1.0 0.46 1 10/12/18 23:58 96-18-4 ND ug/L 50.0 0.42 1 10/12/18 23:58 108-05-4 ND ug/L 1.0 0.60 1 10/12/18 23:58 75-01-4 ND ug/L 5.0 1.5 1 10/12/18 23:58 1330-20-7 102 %. 81-119 1 10/12/18 23:58 17060-07-0 101 %. 82-114 1 10/12/18 23:58 1868-53-7 105 %. 82-120 1 10/12/18 23:58 460-00-4 93 %. 82-109 1 10/12/18 23:58 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 49 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW22A Lab ID: 2610107022 Collected: 10/01/18 13:25 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: KR 1 10/16/18 11:06 6.44 Std. Units 1 10/16/18 11:06 20.9 deg C 1 10/16/18 11:06 1963 umhos/c 1 10/16/18 11:06 m 1.98 NTU 1 10/16/18 11:06 1.09 ug/L 1 10/16/18 11:06 7782-44-7 5.61 feet 1 10/16/18 11:06 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1812:55 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1812:55 7440-38-2 65.3J ug/L 100 0.78 1 10/15/1813:00 10/16/1812:55 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1812:55 7440-41-7 0.79J ug/L 1.0 0.093 1 10/15/1813:00 10/16/1812:55 7440-43-9 1.6J ug/L 10.0 1.6 1 10/15/1813:00 10/16/1812:55 7440-47-3 23.0 ug/L 10.0 0.52 1 10/15/1813:00 10/16/1812:55 7440-48-4 5.5J ug/L 10.0 1.3 1 10/15/1813:00 10/16/1812:55 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1812:55 7439-92-1 126 ug/L 50.0 0.95 1 10/15/1813:00 10/16/1812:55 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1812:55 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1812:55 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1812:55 7440-28-0 ND ug/L 25.0 1.9 1 10/15/1813:00 10/16/1812:55 7440-62-2 10J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1812:55 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.042J ug/L 0.20 0.036 1 10/15/1816:08 10/16/1813:31 7439-97-6 Analytical Method: EPA 8260B Mod. 29.0 ug/L 2.0 1.9 1 10/12/1815:53 123-91-1 106 % 50-150 108 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/12/18 15:53 17060-07-0 1 10/12/1815:53 2037-26-5 8.2 1 10/13/18 00:28 67-64-1 2.5 1 10/13/18 00:28 107-13-1 0.20 1 10/13/18 00:28 71-43-2 0.50 1 10/13/18 00:28 74-97-5 0.36 1 10/13/18 00:28 75-27-4 0.55 1 10/13/18 00:28 75-25-2 0.95 1 10/13/18 00:28 74-83-9 3.2 1 10/13/18 00:28 78-93-3 0.79 1 10/13/18 00:28 75-15-0 0.42 1 10/13/18 00:28 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 50 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW22A Lab ID: 2610107022 Collected: 10/01/18 13:25 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/13/18 00:28 108-90-7 ND ug/L 10.0 0.52 1 10/13/18 00:28 75-00-3 ND ug/L 5.0 0.58 1 10/13/18 00:28 67-66-3 ND ug/L 1.0 0.38 1 10/13/18 00:28 74-87-3 ND ug/L 13.0 0.55 1 10/13/18 00:28 96-12-8 ND ug/L 3.0 0.31 1 10/13/18 00:28 124-48-1 ND ug/L 2.0 0.28 1 10/13/18 00:28 106-93-4 ND ug/L 10.0 0.62 1 10/13/18 00:28 74-95-3 ND ug/L 5.0 0.49 1 10/13/18 00:28 95-50-1 ND ug/L 1.0 0.58 1 10/13/18 00:28 106-46-7 ND ug/L 100 1.6 1 10/13/18 00:28 110-57-6 ND ug/L 5.0 0.41 1 10/13/18 00:28 75-34-3 ND ug/L 1.0 0.67 1 10/13/18 00:28 107-06-2 ND ug/L 5.0 0.72 1 10/13/18 00:28 75-35-4 ND ug/L 5.0 0.66 1 10/13/18 00:28 156-59-2 ND ug/L 5.0 0.46 1 10/13/18 00:28 156-60-5 ND ug/L 1.0 0.60 1 10/13/18 00:28 78-87-5 ND ug/L 1.0 0.22 1 10/13/18 00:28 10061-01-5 ND ug/L 1.0 0.30 1 10/13/18 00:28 10061-02-6 ND ug/L 1.0 0.45 1 10/13/18 00:28 100-41-4 ND ug/L 50.0 0.89 1 10/13/18 00:28 591-78-6 ND ug/L 10.0 3.1 1 10/13/18 00:28 74-88-4 ND ug/L 1.0 0.50 1 10/13/18 00:28 75-09-2 ND ug/L 100 0.86 1 10/13/18 00:28 108-10-1 ND ug/L 1.0 0.50 1 10/13/18 00:28 100-42-5 ND ug/L 5.0 0.32 1 10/13/18 00:28 630-20-6 ND ug/L 3.0 0.53 1 10/13/18 00:28 79-34-5 ND ug/L 1.0 0.78 1 10/13/18 00:28 127-18-4 ND ug/L 1.0 0.31 1 10/13/18 00:28 108-88-3 ND ug/L 1.0 0.38 1 10/13/18 00:28 71-55-6 ND ug/L 1.0 0.59 1 10/13/18 00:28 79-00-5 ND ug/L 1.0 0.34 1 10/13/18 00:28 79-01-6 ND ug/L 1.0 0.51 1 10/13/18 00:28 75-69-4 ND ug/L 1.0 0.46 1 10/13/18 00:28 96-18-4 ND ug/L 50.0 0.42 1 10/13/18 00:28 108-05-4 ND ug/L 1.0 0.60 1 10/13/18 00:28 75-01-4 ND ug/L 5.0 1.5 1 10/13/18 00:28 1330-20-7 99 %. 81-119 1 10/13/18 00:28 17060-07-0 98 %. 82-114 1 10/13/18 00:28 1868-53-7 104 %. 82-120 1 10/13/18 00:28 460-00-4 97 %. 82-109 1 10/13/18 00:28 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 51 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW25 Lab ID: 2610107023 Collected: 10/01/18 13:58 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: KR 1 10/16/18 11:07 6.33 Std. Units 1 10/16/18 11:07 23.9 deg C 1 10/16/18 11:07 1238 umhos/c 1 10/16/18 11:07 m 3.75 NTU 1 10/16/18 11:07 2.23 ug/L 1 10/16/18 11:07 7782-44-7 6.40 feet 1 10/16/18 11:07 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1813:01 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1813:01 7440-38-2 108 ug/L 100 0.78 1 10/15/1813:00 10/16/1813:01 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1813:01 7440-41-7 0.19J ug/L 1.0 0.093 1 10/15/1813:00 10/16/1813:01 7440-43-9 ND ug/L 10.0 1.6 1 10/15/1813:00 10/16/1813:01 7440-47-3 5.7J ug/L 10.0 0.52 1 10/15/1813:00 10/16/1813:01 7440-48-4 ND ug/L 10.0 1.3 1 10/15/1813:00 10/16/1813:01 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1813:01 7439-92-1 24.1J ug/L 50.0 0.95 1 10/15/1813:00 10/16/1813:01 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1813:01 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1813:01 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1813:01 7440-28-0 4.1J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1813:01 7440-62-2 6.5J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1813:01 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.17J ug/L 0.20 0.036 1 10/15/1816:08 10/16/1813:34 7439-97-6 Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/12/1816:12 123-91-1 102 % 50-150 105 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 0.35J ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 31.1J ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/12/18 16:12 17060-07-0 1 10/12/1816:12 2037-26-5 8.2 1 10/13/18 00:58 67-64-1 2.5 1 10/13/18 00:58 107-13-1 0.20 1 10/13/18 00:58 71-43-2 0.50 1 10/13/18 00:58 74-97-5 0.36 1 10/13/18 00:58 75-27-4 0.55 1 10/13/18 00:58 75-25-2 0.95 1 10/13/18 00:58 74-83-9 3.2 1 10/13/18 00:58 78-93-3 0.79 1 10/13/18 00:58 75-15-0 0.42 1 10/13/18 00:58 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 52 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW25 Lab ID: 2610107023 Collected: 10/01/18 13:58 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E 8.3 ug/L 3.0 0.53 1 10/13/18 00:58 108-90-7 ND ug/L 10.0 0.52 1 10/13/18 00:58 75-00-3 ND ug/L 5.0 0.58 1 10/13/18 00:58 67-66-3 ND ug/L 1.0 0.38 1 10/13/18 00:58 74-87-3 ND ug/L 13.0 0.55 1 10/13/18 00:58 96-12-8 ND ug/L 3.0 0.31 1 10/13/18 00:58 124-48-1 ND ug/L 2.0 0.28 1 10/13/18 00:58 106-93-4 ND ug/L 10.0 0.62 1 10/13/18 00:58 74-95-3 ND ug/L 5.0 0.49 1 10/13/18 00:58 95-50-1 12.4 ug/L 1.0 0.58 1 10/13/18 00:58 106-46-7 ND ug/L 100 1.6 1 10/13/18 00:58 110-57-6 ND ug/L 5.0 0.41 1 10/13/18 00:58 75-34-3 ND ug/L 1.0 0.67 1 10/13/18 00:58 107-06-2 ND ug/L 5.0 0.72 1 10/13/18 00:58 75-35-4 ND ug/L 5.0 0.66 1 10/13/18 00:58 156-59-2 ND ug/L 5.0 0.46 1 10/13/18 00:58 156-60-5 ND ug/L 1.0 0.60 1 10/13/18 00:58 78-87-5 ND ug/L 1.0 0.22 1 10/13/18 00:58 10061-01-5 ND ug/L 1.0 0.30 1 10/13/18 00:58 10061-02-6 ND ug/L 1.0 0.45 1 10/13/18 00:58 100-41-4 ND ug/L 50.0 0.89 1 10/13/18 00:58 591-78-6 ND ug/L 10.0 3.1 1 10/13/18 00:58 74-88-4 ND ug/L 1.0 0.50 1 10/13/18 00:58 75-09-2 ND ug/L 100 0.86 1 10/13/18 00:58 108-10-1 ND ug/L 1.0 0.50 1 10/13/18 00:58 100-42-5 ND ug/L 5.0 0.32 1 10/13/18 00:58 630-20-6 ND ug/L 3.0 0.53 1 10/13/18 00:58 79-34-5 ND ug/L 1.0 0.78 1 10/13/18 00:58 127-18-4 ND ug/L 1.0 0.31 1 10/13/18 00:58 108-88-3 ND ug/L 1.0 0.38 1 10/13/18 00:58 71-55-6 ND ug/L 1.0 0.59 1 10/13/18 00:58 79-00-5 ND ug/L 1.0 0.34 1 10/13/18 00:58 79-01-6 ND ug/L 1.0 0.51 1 10/13/18 00:58 75-69-4 ND ug/L 1.0 0.46 1 10/13/18 00:58 96-18-4 ND ug/L 50.0 0.42 1 10/13/18 00:58 108-05-4 ND ug/L 1.0 0.60 1 10/13/18 00:58 75-01-4 ND ug/L 5.0 1.5 1 10/13/18 00:58 1330-20-7 100 %. 81-119 1 10/13/18 00:58 17060-07-0 96 %. 82-114 1 10/13/18 00:58 1868-53-7 104 %. 82-120 1 10/13/18 00:58 460-00-4 96 %. 82-109 1 10/13/18 00:58 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 53 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW26 Lab ID: 2610107024 Collected: 10/02/18 11:41 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: SF 1 10/16/18 11:07 6.24 Std. Units 1 10/16/18 11:07 19.8 deg C 1 10/16/18 11:07 894 umhos/c 1 10/16/18 11:07 m 1.23 NTU 1 10/16/18 11:07 1.22 ug/L 1 10/16/18 11:07 7782-44-7 15.45 feet 1 10/16/18 11:07 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1813:06 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1813:06 7440-38-2 155 ug/L 100 0.78 1 10/15/1813:00 10/16/1813:06 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1813:06 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1813:06 7440-43-9 1.7J ug/L 10.0 1.6 1 10/15/1813:00 10/16/1813:06 7440-47-3 5.6J ug/L 10.0 0.52 1 10/15/1813:00 10/16/1813:06 7440-48-4 ND ug/L 10.0 1.3 1 10/15/1813:00 10/16/1813:06 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1813:06 7439-92-1 16.OJ ug/L 50.0 0.95 1 10/15/1813:00 10/16/1813:06 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1813:06 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1813:06 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1813:06 7440-28-0 6.5J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1813:06 7440-62-2 3.9J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1813:06 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.22 ug/L 0.20 0.036 1 10/15/1816:08 10/16/1813:36 7439-97-6 Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/12/18 21:42 123-91-1 102 % 50-150 107 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 0.58J ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/12/18 21:42 17060-07-0 1 10/12/18 21:42 2037-26-5 8.2 1 10/16/1817:59 67-64-1 2.5 1 10/16/18 17:59 107-13-1 0.20 1 10/16/1817:59 71-43-2 0.50 1 10/16/1817:59 74-97-5 0.36 1 10/16/1817:59 75-27-4 0.55 1 10/16/1817:59 75-25-2 0.95 1 10/16/1817:59 74-83-9 3.2 1 10/16/1817:59 78-93-3 0.79 1 10/16/1817:59 75-15-0 0.42 1 10/16/1817:59 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 54 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW26 Lab ID: 2610107024 Collected: 10/02/18 11:41 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/16/1817:59 108-90-7 ND ug/L 10.0 0.52 1 10/16/1817:59 75-00-3 ND ug/L 5.0 0.58 1 10/16/1817:59 67-66-3 ND ug/L 1.0 0.38 1 10/16/1817:59 74-87-3 ND ug/L 13.0 0.55 1 10/16/1817:59 96-12-8 ND ug/L 3.0 0.31 1 10/16/1817:59 124-48-1 ND ug/L 2.0 0.28 1 10/16/1817:59 106-93-4 ND ug/L 10.0 0.62 1 10/16/1817:59 74-95-3 ND ug/L 5.0 0.49 1 10/16/1817:59 95-50-1 0.97J ug/L 1.0 0.58 1 10/16/1817:59 106-46-7 ND ug/L 100 1.6 1 10/16/1817:59 110-57-6 ND ug/L 5.0 0.41 1 10/16/1817:59 75-34-3 ND ug/L 1.0 0.67 1 10/16/1817:59 107-06-2 ND ug/L 5.0 0.72 1 10/16/1817:59 75-35-4 1.OJ ug/L 5.0 0.66 1 10/16/1817:59 156-59-2 ND ug/L 5.0 0.46 1 10/16/1817:59 156-60-5 ND ug/L 1.0 0.60 1 10/16/1817:59 78-87-5 ND ug/L 1.0 0.22 1 10/16/1817:59 10061-01-5 ND ug/L 1.0 0.30 1 10/16/1817:59 10061-02-6 ND ug/L 1.0 0.45 1 10/16/1817:59 100-41-4 ND ug/L 50.0 0.89 1 10/16/1817:59 591-78-6 ND ug/L 10.0 3.1 1 10/16/1817:59 74-88-4 ND ug/L 1.0 0.50 1 10/16/1817:59 75-09-2 ND ug/L 100 0.86 1 10/16/1817:59 108-10-1 ND ug/L 1.0 0.50 1 10/16/1817:59 100-42-5 ND ug/L 5.0 0.32 1 10/16/1817:59 630-20-6 ND ug/L 3.0 0.53 1 10/16/1817:59 79-34-5 ND ug/L 1.0 0.78 1 10/16/1817:59 127-18-4 ND ug/L 1.0 0.31 1 10/16/1817:59 108-88-3 ND ug/L 1.0 0.38 1 10/16/1817:59 71-55-6 ND ug/L 1.0 0.59 1 10/16/1817:59 79-00-5 ND ug/L 1.0 0.34 1 10/16/1817:59 79-01-6 ND ug/L 1.0 0.51 1 10/16/1817:59 75-69-4 ND ug/L 1.0 0.46 1 10/16/1817:59 96-18-4 ND ug/L 50.0 0.42 1 10/16/1817:59 108-05-4 ND ug/L 1.0 0.60 1 10/16/1817:59 75-01-4 ND ug/L 5.0 1.5 1 10/16/1817:59 1330-20-7 99 %. 81-119 1 10/16/1817:59 17060-07-0 98 %. 82-114 1 10/16/1817:59 1868-53-7 106 %. 82-120 1 10/16/1817:59 460-00-4 94 %. 82-109 1 10/16/1817:59 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 55 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW27 Lab ID: 2610107025 Collected: 10/03/18 09:24 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: KR 1 10/16/18 11:08 6.34 Std. Units 1 10/16/18 11:08 20.8 deg C 1 10/16/18 11:08 230 umhos/c 1 10/16/18 11:08 m 7.29 NTU 1 10/16/18 11:08 3.28 ug/L 1 10/16/18 11:08 7782-44-7 8.87 feet 1 10/16/18 11:08 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1813:12 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1813:12 7440-38-2 40.8J ug/L 100 0.78 1 10/15/1813:00 10/16/1813:12 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1813:12 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1813:12 7440-43-9 3.6J ug/L 10.0 1.6 1 10/15/1813:00 10/16/1813:12 7440-47-3 0.96J ug/L 10.0 0.52 1 10/15/1813:00 10/16/1813:12 7440-48-4 7.8J ug/L 10.0 1.3 1 10/15/1813:00 10/16/1813:12 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1813:12 7439-92-1 7.OJ ug/L 50.0 0.95 1 10/15/1813:00 10/16/1813:12 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1813:12 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1813:12 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1813:12 7440-28-0 5.9J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1813:12 7440-62-2 5.3J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1813:12 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.083J ug/L 0.20 0.036 1 10/15/1816:08 10/16/1813:38 7439-97-6 Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/17/1816:25 123-91-1 104 % 50-150 115 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/17/18 16:25 17060-07-0 1 10/17/1816:25 2037-26-5 8.2 1 10/15/1815:00 67-64-1 2.5 1 10/15/18 15:00 107-13-1 0.20 1 10/15/1815:00 71-43-2 0.50 1 10/15/1815:00 74-97-5 0.36 1 10/15/1815:00 75-27-4 0.55 1 10/15/1815:00 75-25-2 0.95 1 10/15/1815:00 74-83-9 3.2 1 10/15/1815:00 78-93-3 0.79 1 10/15/1815:00 75-15-0 0.42 1 10/15/1815:00 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 56 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW27 Lab ID: 2610107025 Collected: 10/03/18 09:24 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/15/1815:00 108-90-7 ND ug/L 10.0 0.52 1 10/15/1815:00 75-00-3 ND ug/L 5.0 0.58 1 10/15/1815:00 67-66-3 ND ug/L 1.0 0.38 1 10/15/1815:00 74-87-3 ND ug/L 13.0 0.55 1 10/15/1815:00 96-12-8 ND ug/L 3.0 0.31 1 10/15/1815:00 124-48-1 ND ug/L 2.0 0.28 1 10/15/1815:00 106-93-4 ND ug/L 10.0 0.62 1 10/15/1815:00 74-95-3 ND ug/L 5.0 0.49 1 10/15/1815:00 95-50-1 ND ug/L 1.0 0.58 1 10/15/1815:00 106-46-7 ND ug/L 100 1.6 1 10/15/1815:00 110-57-6 ND ug/L 5.0 0.41 1 10/15/1815:00 75-34-3 ND ug/L 1.0 0.67 1 10/15/1815:00 107-06-2 ND ug/L 5.0 0.72 1 10/15/1815:00 75-35-4 ND ug/L 5.0 0.66 1 10/15/1815:00 156-59-2 ND ug/L 5.0 0.46 1 10/15/1815:00 156-60-5 ND ug/L 1.0 0.60 1 10/15/1815:00 78-87-5 ND ug/L 1.0 0.22 1 10/15/1815:00 10061-01-5 ND ug/L 1.0 0.30 1 10/15/1815:00 10061-02-6 ND ug/L 1.0 0.45 1 10/15/1815:00 100-41-4 ND ug/L 50.0 0.89 1 10/15/1815:00 591-78-6 ND ug/L 10.0 3.1 1 10/15/1815:00 74-88-4 ND ug/L 1.0 0.50 1 10/15/1815:00 75-09-2 ND ug/L 100 0.86 1 10/15/1815:00 108-10-1 ND ug/L 1.0 0.50 1 10/15/1815:00 100-42-5 ND ug/L 5.0 0.32 1 10/15/1815:00 630-20-6 ND ug/L 3.0 0.53 1 10/15/1815:00 79-34-5 ND ug/L 1.0 0.78 1 10/15/1815:00 127-18-4 ND ug/L 1.0 0.31 1 10/15/1815:00 108-88-3 ND ug/L 1.0 0.38 1 10/15/1815:00 71-55-6 ND ug/L 1.0 0.59 1 10/15/1815:00 79-00-5 ND ug/L 1.0 0.34 1 10/15/1815:00 79-01-6 ND ug/L 1.0 0.51 1 10/15/1815:00 75-69-4 ND ug/L 1.0 0.46 1 10/15/1815:00 96-18-4 ND ug/L 50.0 0.42 1 10/15/1815:00 108-05-4 ND ug/L 1.0 0.60 1 10/15/1815:00 75-01-4 ND ug/L 5.0 1.5 1 10/15/1815:00 1330-20-7 98 %. 81-119 1 10/15/1815:00 17060-07-0 98 %. 82-114 1 10/15/1815:00 1868-53-7 106 %. 82-120 1 10/15/1815:00 460-00-4 99 %. 82-109 1 10/15/1815:00 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 57 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW28 Lab ID: 2610107026 Collected: 10/02/18 12:16 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: KR 1 10/16/18 11:08 6.60 Std. Units 1 10/16/18 11:08 18.9 deg C 1 10/16/18 11:08 436 umhos/c 1 10/16/18 11:08 m 3.19 NTU 1 10/16/18 11:08 3.16 ug/L 1 10/16/18 11:08 7782-44-7 12.14 feet 1 10/16/18 11:08 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1813:18 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1813:18 7440-38-2 60.1J ug/L 100 0.78 1 10/15/1813:00 10/16/1813:18 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1813:18 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1813:18 7440-43-9 4.OJ ug/L 10.0 1.6 1 10/15/1813:00 10/16/1813:18 7440-47-3 ND ug/L 10.0 0.52 1 10/15/1813:00 10/16/1813:18 7440-48-4 ND ug/L 10.0 1.3 1 10/15/1813:00 10/16/1813:18 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1813:18 7439-92-1 12.7J ug/L 50.0 0.95 1 10/15/1813:00 10/16/1813:18 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1813:18 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1813:18 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1813:18 7440-28-0 2.1J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1813:18 7440-62-2 4.5J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1813:18 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.10J ug/L 0.20 0.036 1 10/15/1816:08 10/16/1813:45 7439-97-6 Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/12/18 22:01 123-91-1 100 % 50-150 105 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/12/18 22:01 17060-07-0 1 10/12/18 22:01 2037-26-5 8.2 1 10/16/18 00:54 67-64-1 2.5 1 10/16/18 00:54 107-13-1 0.20 1 10/16/18 00:54 71-43-2 0.50 1 10/16/18 00:54 74-97-5 0.36 1 10/16/18 00:54 75-27-4 0.55 1 10/16/18 00:54 75-25-2 0.95 1 10/16/18 00:54 74-83-9 3.2 1 10/16/18 00:54 78-93-3 0.79 1 10/16/18 00:54 75-15-0 0.42 1 10/16/18 00:54 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 58 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW28 Lab ID: 2610107026 Collected: 10/02/18 12:16 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/16/18 00:54 108-90-7 ND ug/L 10.0 0.52 1 10/16/18 00:54 75-00-3 ND ug/L 5.0 0.58 1 10/16/18 00:54 67-66-3 ND ug/L 1.0 0.38 1 10/16/18 00:54 74-87-3 ND ug/L 13.0 0.55 1 10/16/18 00:54 96-12-8 ND ug/L 3.0 0.31 1 10/16/18 00:54 124-48-1 ND ug/L 2.0 0.28 1 10/16/18 00:54 106-93-4 ND ug/L 10.0 0.62 1 10/16/18 00:54 74-95-3 ND ug/L 5.0 0.49 1 10/16/18 00:54 95-50-1 ND ug/L 1.0 0.58 1 10/16/18 00:54 106-46-7 ND ug/L 100 1.6 1 10/16/18 00:54 110-57-6 ND ug/L 5.0 0.41 1 10/16/18 00:54 75-34-3 ND ug/L 1.0 0.67 1 10/16/18 00:54 107-06-2 ND ug/L 5.0 0.72 1 10/16/18 00:54 75-35-4 ND ug/L 5.0 0.66 1 10/16/18 00:54 156-59-2 ND ug/L 5.0 0.46 1 10/16/18 00:54 156-60-5 ND ug/L 1.0 0.60 1 10/16/18 00:54 78-87-5 ND ug/L 1.0 0.22 1 10/16/18 00:54 10061-01-5 ND ug/L 1.0 0.30 1 10/16/18 00:54 10061-02-6 ND ug/L 1.0 0.45 1 10/16/18 00:54 100-41-4 ND ug/L 50.0 0.89 1 10/16/18 00:54 591-78-6 ND ug/L 10.0 3.1 1 10/16/18 00:54 74-88-4 ND ug/L 1.0 0.50 1 10/16/18 00:54 75-09-2 ND ug/L 100 0.86 1 10/16/18 00:54 108-10-1 ND ug/L 1.0 0.50 1 10/16/18 00:54 100-42-5 ND ug/L 5.0 0.32 1 10/16/18 00:54 630-20-6 ND ug/L 3.0 0.53 1 10/16/18 00:54 79-34-5 ND ug/L 1.0 0.78 1 10/16/18 00:54 127-18-4 ND ug/L 1.0 0.31 1 10/16/18 00:54 108-88-3 ND ug/L 1.0 0.38 1 10/16/18 00:54 71-55-6 ND ug/L 1.0 0.59 1 10/16/18 00:54 79-00-5 ND ug/L 1.0 0.34 1 10/16/18 00:54 79-01-6 ND ug/L 1.0 0.51 1 10/16/18 00:54 75-69-4 ND ug/L 1.0 0.46 1 10/16/18 00:54 96-18-4 ND ug/L 50.0 0.42 1 10/16/18 00:54 108-05-4 ND ug/L 1.0 0.60 1 10/16/18 00:54 75-01-4 ND ug/L 5.0 1.5 1 10/16/18 00:54 1330-20-7 104 %. 81-119 1 10/16/18 00:54 17060-07-0 95 %. 82-114 1 10/16/18 00:54 1868-53-7 108 %. 82-120 1 10/16/18 00:54 460-00-4 105 %. 82-109 1 10/16/18 00:54 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 59 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW29R Lab ID: 2610107027 Collected: 10/02/18 15:26 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: SF 1 10/16/18 11:09 6.27 Std. Units 1 10/16/18 11:09 19.3 deg C 1 10/16/18 11:09 307 umhos/c 1 10/16/18 11:09 m 5.01 NTU 1 10/16/18 11:09 2.00 ug/L 1 10/16/18 11:09 7782-44-7 6.24 feet 1 10/16/18 11:09 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1813:24 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1813:24 7440-38-2 37.2J ug/L 100 0.78 1 10/15/1813:00 10/16/1813:24 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1813:24 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1813:24 7440-43-9 3.OJ ug/L 10.0 1.6 1 10/15/1813:00 10/16/1813:24 7440-47-3 1.7J ug/L 10.0 0.52 1 10/15/1813:00 10/16/1813:24 7440-48-4 8.7J ug/L 10.0 1.3 1 10/15/1813:00 10/16/1813:24 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1813:24 7439-92-1 5.9J ug/L 50.0 0.95 1 10/15/1813:00 10/16/1813:24 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1813:24 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1813:24 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1813:24 7440-28-0 5.4J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1813:24 7440-62-2 5.5J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1813:24 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.065J ug/L 0.20 0.036 1 10/15/1816:08 10/16/1813:48 7439-97-6 Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/15/1818:49 123-91-1 108 % 50-150 113 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/15/18 18:49 17060-07-0 1 10/15/1818:49 2037-26-5 8.2 1 10/16/18 01:18 67-64-1 2.5 1 10/16/18 01:18 107-13-1 0.20 1 10/16/18 01:18 71-43-2 0.50 1 10/16/18 01:18 74-97-5 0.36 1 10/16/18 01:18 75-27-4 0.55 1 10/16/18 01:18 75-25-2 0.95 1 10/16/18 01:18 74-83-9 3.2 1 10/16/18 01:18 78-93-3 0.79 1 10/16/18 01:18 75-15-0 0.42 1 10/16/18 01:18 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 60 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW29R Lab ID: 2610107027 Collected: 10/02/18 15:26 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/16/18 01:18 108-90-7 ND ug/L 10.0 0.52 1 10/16/18 01:18 75-00-3 ND ug/L 5.0 0.58 1 10/16/18 01:18 67-66-3 ND ug/L 1.0 0.38 1 10/16/18 01:18 74-87-3 ND ug/L 13.0 0.55 1 10/16/18 01:18 96-12-8 ND ug/L 3.0 0.31 1 10/16/18 01:18 124-48-1 ND ug/L 2.0 0.28 1 10/16/18 01:18 106-93-4 ND ug/L 10.0 0.62 1 10/16/18 01:18 74-95-3 ND ug/L 5.0 0.49 1 10/16/18 01:18 95-50-1 ND ug/L 1.0 0.58 1 10/16/18 01:18 106-46-7 ND ug/L 100 1.6 1 10/16/18 01:18 110-57-6 ND ug/L 5.0 0.41 1 10/16/18 01:18 75-34-3 ND ug/L 1.0 0.67 1 10/16/18 01:18 107-06-2 ND ug/L 5.0 0.72 1 10/16/18 01:18 75-35-4 ND ug/L 5.0 0.66 1 10/16/18 01:18 156-59-2 ND ug/L 5.0 0.46 1 10/16/18 01:18 156-60-5 ND ug/L 1.0 0.60 1 10/16/18 01:18 78-87-5 ND ug/L 1.0 0.22 1 10/16/18 01:18 10061-01-5 ND ug/L 1.0 0.30 1 10/16/18 01:18 10061-02-6 ND ug/L 1.0 0.45 1 10/16/18 01:18 100-41-4 ND ug/L 50.0 0.89 1 10/16/18 01:18 591-78-6 ND ug/L 10.0 3.1 1 10/16/18 01:18 74-88-4 ND ug/L 1.0 0.50 1 10/16/18 01:18 75-09-2 ND ug/L 100 0.86 1 10/16/18 01:18 108-10-1 ND ug/L 1.0 0.50 1 10/16/18 01:18 100-42-5 ND ug/L 5.0 0.32 1 10/16/18 01:18 630-20-6 ND ug/L 3.0 0.53 1 10/16/18 01:18 79-34-5 ND ug/L 1.0 0.78 1 10/16/18 01:18 127-18-4 ND ug/L 1.0 0.31 1 10/16/18 01:18 108-88-3 ND ug/L 1.0 0.38 1 10/16/18 01:18 71-55-6 ND ug/L 1.0 0.59 1 10/16/18 01:18 79-00-5 ND ug/L 1.0 0.34 1 10/16/18 01:18 79-01-6 ND ug/L 1.0 0.51 1 10/16/18 01:18 75-69-4 ND ug/L 1.0 0.46 1 10/16/18 01:18 96-18-4 ND ug/L 50.0 0.42 1 10/16/18 01:18 108-05-4 ND ug/L 1.0 0.60 1 10/16/18 01:18 75-01-4 ND ug/L 5.0 1.5 1 10/16/18 01:18 1330-20-7 105 %. 81-119 1 10/16/18 01:18 17060-07-0 95 %. 82-114 1 10/16/18 01:18 1868-53-7 110 %. 82-120 1 10/16/18 01:18 460-00-4 106 %. 82-109 1 10/16/18 01:18 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 61 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW30R Lab ID: 2610107028 Collected: 10/02/18 09:30 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: WF 1 10/16/18 11:10 6.69 Std. Units 1 10/16/18 11:10 18.7 deg C 1 10/16/18 11:10 236 umhos/c 1 10/16/18 11:10 m 9.11 NTU 1 10/16/18 11:10 1.72 ug/L 1 10/16/18 11:10 7782-44-7 27.95 feet 1 10/16/18 11:10 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1813:29 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1813:29 7440-38-2 100 ug/L 100 0.78 1 10/15/1813:00 10/16/1813:29 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1813:29 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1813:29 7440-43-9 7.7J ug/L 10.0 1.6 1 10/15/1813:00 10/16/1813:29 7440-47-3 1.4J ug/L 10.0 0.52 1 10/15/1813:00 10/16/1813:29 7440-48-4 8.8J ug/L 10.0 1.3 1 10/15/1813:00 10/16/1813:29 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1813:29 7439-92-1 15.2J ug/L 50.0 0.95 1 10/15/1813:00 10/16/1813:29 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1813:29 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1813:29 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1813:29 7440-28-0 6.5J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1813:29 7440-62-2 17.2 ug/L 10.0 2.1 1 10/15/1813:00 10/16/1813:29 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.085J ug/L 0.20 0.036 1 10/15/1816:08 10/16/1813:50 7439-97-6 Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/15/1819:08 123-91-1 105 % 50-150 119 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/15/18 19:08 17060-07-0 1 10/15/1819:08 2037-26-5 8.2 1 10/16/18 01:43 67-64-1 2.5 1 10/16/18 01:43 107-13-1 0.20 1 10/16/18 01:43 71-43-2 0.50 1 10/16/18 01:43 74-97-5 0.36 1 10/16/18 01:43 75-27-4 0.55 1 10/16/18 01:43 75-25-2 0.95 1 10/16/18 01:43 74-83-9 3.2 1 10/16/18 01:43 78-93-3 0.79 1 10/16/18 01:43 75-15-0 0.42 1 10/16/18 01:43 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 62 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW30R Lab ID: 2610107028 Collected: 10/02/18 09:30 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/16/18 01:43 108-90-7 ND ug/L 10.0 0.52 1 10/16/18 01:43 75-00-3 ND ug/L 5.0 0.58 1 10/16/18 01:43 67-66-3 ND ug/L 1.0 0.38 1 10/16/18 01:43 74-87-3 ND ug/L 13.0 0.55 1 10/16/18 01:43 96-12-8 ND ug/L 3.0 0.31 1 10/16/18 01:43 124-48-1 ND ug/L 2.0 0.28 1 10/16/18 01:43 106-93-4 ND ug/L 10.0 0.62 1 10/16/18 01:43 74-95-3 ND ug/L 5.0 0.49 1 10/16/18 01:43 95-50-1 ND ug/L 1.0 0.58 1 10/16/18 01:43 106-46-7 ND ug/L 100 1.6 1 10/16/18 01:43 110-57-6 ND ug/L 5.0 0.41 1 10/16/18 01:43 75-34-3 ND ug/L 1.0 0.67 1 10/16/18 01:43 107-06-2 ND ug/L 5.0 0.72 1 10/16/18 01:43 75-35-4 ND ug/L 5.0 0.66 1 10/16/18 01:43 156-59-2 ND ug/L 5.0 0.46 1 10/16/18 01:43 156-60-5 ND ug/L 1.0 0.60 1 10/16/18 01:43 78-87-5 ND ug/L 1.0 0.22 1 10/16/18 01:43 10061-01-5 ND ug/L 1.0 0.30 1 10/16/18 01:43 10061-02-6 ND ug/L 1.0 0.45 1 10/16/18 01:43 100-41-4 ND ug/L 50.0 0.89 1 10/16/18 01:43 591-78-6 ND ug/L 10.0 3.1 1 10/16/18 01:43 74-88-4 ND ug/L 1.0 0.50 1 10/16/18 01:43 75-09-2 ND ug/L 100 0.86 1 10/16/18 01:43 108-10-1 ND ug/L 1.0 0.50 1 10/16/18 01:43 100-42-5 ND ug/L 5.0 0.32 1 10/16/18 01:43 630-20-6 ND ug/L 3.0 0.53 1 10/16/18 01:43 79-34-5 ND ug/L 1.0 0.78 1 10/16/18 01:43 127-18-4 ND ug/L 1.0 0.31 1 10/16/18 01:43 108-88-3 ND ug/L 1.0 0.38 1 10/16/18 01:43 71-55-6 ND ug/L 1.0 0.59 1 10/16/18 01:43 79-00-5 ND ug/L 1.0 0.34 1 10/16/18 01:43 79-01-6 ND ug/L 1.0 0.51 1 10/16/18 01:43 75-69-4 ND ug/L 1.0 0.46 1 10/16/18 01:43 96-18-4 ND ug/L 50.0 0.42 1 10/16/18 01:43 108-05-4 ND ug/L 1.0 0.60 1 10/16/18 01:43 75-01-4 ND ug/L 5.0 1.5 1 10/16/18 01:43 1330-20-7 104 %. 81-119 1 10/16/18 01:43 17060-07-0 93 %. 82-114 1 10/16/18 01:43 1868-53-7 110 %. 82-120 1 10/16/18 01:43 460-00-4 104 %. 82-109 1 10/16/18 01:43 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 63 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW31 Lab ID: 2610107029 Collected: 10/02/18 10:04 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: WF 1 10/16/18 11:11 6.98 Std. Units 1 10/16/18 11:11 19.0 deg C 1 10/16/18 11:11 220 umhos/c 1 10/16/18 11:11 m 0.08 NTU 1 10/16/18 11:11 2.52 ug/L 1 10/16/18 11:11 7782-44-7 25.62 feet 1 10/16/18 11:11 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1813:55 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1813:55 7440-38-2 59.5J ug/L 100 0.78 1 10/15/1813:00 10/16/1813:55 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1813:55 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1813:55 7440-43-9 ND ug/L 10.0 1.6 1 10/15/1813:00 10/16/1813:55 7440-47-3 ND ug/L 10.0 0.52 1 10/15/1813:00 10/16/1813:55 7440-48-4 1.4J ug/L 10.0 1.3 1 10/15/1813:00 10/16/1813:55 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1813:55 7439-92-1 3.OJ ug/L 50.0 0.95 1 10/15/1813:00 10/16/1813:55 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1813:55 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1813:55 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1813:55 7440-28-0 2.9J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1813:55 7440-62-2 4.9J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1813:55 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.40 ug/L 0.20 0.036 1 10/15/1816:08 10/16/1813:53 7439-97-6 Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/15/1819:27 123-91-1 108 % 50-150 112 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/15/18 19:27 17060-07-0 1 10/15/1819:27 2037-26-5 8.2 1 10/16/18 02:08 67-64-1 2.5 1 10/16/18 02:08 107-13-1 0.20 1 10/16/18 02:08 71-43-2 0.50 1 10/16/18 02:08 74-97-5 0.36 1 10/16/18 02:08 75-27-4 0.55 1 10/16/18 02:08 75-25-2 0.95 1 10/16/18 02:08 74-83-9 3.2 1 10/16/18 02:08 78-93-3 0.79 1 10/16/18 02:08 75-15-0 0.42 1 10/16/18 02:08 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 64 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW31 Lab ID: 2610107029 Collected: 10/02/18 10:04 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/16/18 02:08 108-90-7 ND ug/L 10.0 0.52 1 10/16/18 02:08 75-00-3 ND ug/L 5.0 0.58 1 10/16/18 02:08 67-66-3 ND ug/L 1.0 0.38 1 10/16/18 02:08 74-87-3 ND ug/L 13.0 0.55 1 10/16/18 02:08 96-12-8 ND ug/L 3.0 0.31 1 10/16/18 02:08 124-48-1 ND ug/L 2.0 0.28 1 10/16/18 02:08 106-93-4 ND ug/L 10.0 0.62 1 10/16/18 02:08 74-95-3 ND ug/L 5.0 0.49 1 10/16/18 02:08 95-50-1 ND ug/L 1.0 0.58 1 10/16/18 02:08 106-46-7 ND ug/L 100 1.6 1 10/16/18 02:08 110-57-6 ND ug/L 5.0 0.41 1 10/16/18 02:08 75-34-3 ND ug/L 1.0 0.67 1 10/16/18 02:08 107-06-2 ND ug/L 5.0 0.72 1 10/16/18 02:08 75-35-4 ND ug/L 5.0 0.66 1 10/16/18 02:08 156-59-2 ND ug/L 5.0 0.46 1 10/16/18 02:08 156-60-5 ND ug/L 1.0 0.60 1 10/16/18 02:08 78-87-5 ND ug/L 1.0 0.22 1 10/16/18 02:08 10061-01-5 ND ug/L 1.0 0.30 1 10/16/18 02:08 10061-02-6 ND ug/L 1.0 0.45 1 10/16/18 02:08 100-41-4 ND ug/L 50.0 0.89 1 10/16/18 02:08 591-78-6 ND ug/L 10.0 3.1 1 10/16/18 02:08 74-88-4 ND ug/L 1.0 0.50 1 10/16/18 02:08 75-09-2 ND ug/L 100 0.86 1 10/16/18 02:08 108-10-1 ND ug/L 1.0 0.50 1 10/16/18 02:08 100-42-5 ND ug/L 5.0 0.32 1 10/16/18 02:08 630-20-6 ND ug/L 3.0 0.53 1 10/16/18 02:08 79-34-5 ND ug/L 1.0 0.78 1 10/16/18 02:08 127-18-4 ND ug/L 1.0 0.31 1 10/16/18 02:08 108-88-3 ND ug/L 1.0 0.38 1 10/16/18 02:08 71-55-6 ND ug/L 1.0 0.59 1 10/16/18 02:08 79-00-5 ND ug/L 1.0 0.34 1 10/16/18 02:08 79-01-6 ND ug/L 1.0 0.51 1 10/16/18 02:08 75-69-4 ND ug/L 1.0 0.46 1 10/16/18 02:08 96-18-4 ND ug/L 50.0 0.42 1 10/16/18 02:08 108-05-4 ND ug/L 1.0 0.60 1 10/16/18 02:08 75-01-4 ND ug/L 5.0 1.5 1 10/16/18 02:08 1330-20-7 105 %. 81-119 1 10/16/18 02:08 17060-07-0 94 %. 82-114 1 10/16/18 02:08 1868-53-7 108 %. 82-120 1 10/16/18 02:08 460-00-4 104 %. 82-109 1 10/16/18 02:08 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 65 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW32R Lab ID: 2610107030 Collected: 10/02/18 11:00 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: WF 1 10/16/18 11:11 6.70 Std. Units 1 10/16/18 11:11 23.9 deg C 1 10/16/18 11:11 697 umhos/c 1 10/16/18 11:11 m 5.44 NTU 1 10/16/18 11:11 1.45 ug/L 1 10/16/18 11:11 7782-44-7 22.12 feet 1 10/16/18 11:11 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1814:00 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1814:00 7440-38-2 176 ug/L 100 0.78 1 10/15/1813:00 10/16/1814:00 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1814:00 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1814:00 7440-43-9 9.OJ ug/L 10.0 1.6 1 10/15/1813:00 10/16/1814:00 7440-47-3 87.6 ug/L 10.0 0.52 1 10/15/1813:00 10/16/1814:00 7440-48-4 33.5 ug/L 10.0 1.3 1 10/15/1813:00 10/16/1814:00 7440-50-8 13.1 ug/L 10.0 0.27 1 10/15/1813:00 10/16/1814:00 7439-92-1 41.OJ ug/L 50.0 0.95 1 10/15/1813:00 10/16/1814:00 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1814:00 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1814:00 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1814:00 7440-28-0 9.6J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1814:00 7440-62-2 9.8J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1814:00 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.080J ug/L 0.20 0.036 1 10/15/1816:08 10/16/1813:55 7439-97-6 Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/15/1819:47 123-91-1 105 % 50-150 112 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 4.5 ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/15/18 19:47 17060-07-0 1 10/15/1819:47 2037-26-5 8.2 1 10/16/18 02:32 67-64-1 2.5 1 10/16/18 02:32 107-13-1 0.20 1 10/16/18 02:32 71-43-2 0.50 1 10/16/18 02:32 74-97-5 0.36 1 10/16/18 02:32 75-27-4 0.55 1 10/16/18 02:32 75-25-2 0.95 1 10/16/18 02:32 74-83-9 3.2 1 10/16/18 02:32 78-93-3 0.79 1 10/16/18 02:32 75-15-0 0.42 1 10/16/18 02:32 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 66 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW32R Lab ID: 2610107030 Collected: 10/02/18 11:00 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/16/18 02:32 108-90-7 ND ug/L 10.0 0.52 1 10/16/18 02:32 75-00-3 ND ug/L 5.0 0.58 1 10/16/18 02:32 67-66-3 ND ug/L 1.0 0.38 1 10/16/18 02:32 74-87-3 ND ug/L 13.0 0.55 1 10/16/18 02:32 96-12-8 ND ug/L 3.0 0.31 1 10/16/18 02:32 124-48-1 ND ug/L 2.0 0.28 1 10/16/18 02:32 106-93-4 ND ug/L 10.0 0.62 1 10/16/18 02:32 74-95-3 ND ug/L 5.0 0.49 1 10/16/18 02:32 95-50-1 ND ug/L 1.0 0.58 1 10/16/18 02:32 106-46-7 ND ug/L 100 1.6 1 10/16/18 02:32 110-57-6 ND ug/L 5.0 0.41 1 10/16/18 02:32 75-34-3 ND ug/L 1.0 0.67 1 10/16/18 02:32 107-06-2 ND ug/L 5.0 0.72 1 10/16/18 02:32 75-35-4 4.5J ug/L 5.0 0.66 1 10/16/18 02:32 156-59-2 ND ug/L 5.0 0.46 1 10/16/18 02:32 156-60-5 ND ug/L 1.0 0.60 1 10/16/18 02:32 78-87-5 ND ug/L 1.0 0.22 1 10/16/18 02:32 10061-01-5 ND ug/L 1.0 0.30 1 10/16/18 02:32 10061-02-6 ND ug/L 1.0 0.45 1 10/16/18 02:32 100-41-4 ND ug/L 50.0 0.89 1 10/16/18 02:32 591-78-6 ND ug/L 10.0 3.1 1 10/16/18 02:32 74-88-4 0.57J ug/L 1.0 0.50 1 10/16/18 02:32 75-09-2 ND ug/L 100 0.86 1 10/16/18 02:32 108-10-1 ND ug/L 1.0 0.50 1 10/16/18 02:32 100-42-5 ND ug/L 5.0 0.32 1 10/16/18 02:32 630-20-6 ND ug/L 3.0 0.53 1 10/16/18 02:32 79-34-5 ND ug/L 1.0 0.78 1 10/16/18 02:32 127-18-4 ND ug/L 1.0 0.31 1 10/16/18 02:32 108-88-3 ND ug/L 1.0 0.38 1 10/16/18 02:32 71-55-6 ND ug/L 1.0 0.59 1 10/16/18 02:32 79-00-5 O.60J ug/L 1.0 0.34 1 10/16/18 02:32 79-01-6 ND ug/L 1.0 0.51 1 10/16/18 02:32 75-69-4 ND ug/L 1.0 0.46 1 10/16/18 02:32 96-18-4 ND ug/L 50.0 0.42 1 10/16/18 02:32 108-05-4 4.2 ug/L 1.0 0.60 1 10/16/18 02:32 75-01-4 ND ug/L 5.0 1.5 1 10/16/18 02:32 1330-20-7 104 %. 81-119 1 10/16/18 02:32 17060-07-0 96 %. 82-114 1 10/16/18 02:32 1868-53-7 109 %. 82-120 1 10/16/18 02:32 460-00-4 105 %. 82-109 1 10/16/18 02:32 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. B Page 67 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW34 Lab ID: 2610107032 Collected: 10/02/18 13:34 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved Depth to Water 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Date: 11/07/2018 04:17 PM Analytical Method: WF 1 10/16/18 11:12 5.95 Std. Units 1 10/16/18 11:12 21.4 deg C 1 10/16/18 11:12 347 umhos/c 1 10/16/18 11:12 m 8.31 NTU 1 10/16/18 11:12 1.36 ug/L 1 10/16/18 11:12 7782-44-7 28.95 feet 1 10/16/18 11:12 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1814:06 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1814:06 7440-38-2 179 ug/L 100 0.78 1 10/15/1813:00 10/16/1814:06 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1814:06 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1814:06 7440-43-9 2.3J ug/L 10.0 1.6 1 10/15/1813:00 10/16/1814:06 7440-47-3 2.6J ug/L 10.0 0.52 1 10/15/1813:00 10/16/1814:06 7440-48-4 4.2J ug/L 10.0 1.3 1 10/15/1813:00 10/16/1814:06 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1814:06 7439-92-1 3.9J ug/L 50.0 0.95 1 10/15/1813:00 10/16/1814:06 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1814:06 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1814:06 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1814:06 7440-28-0 ND ug/L 25.0 1.9 1 10/15/1813:00 10/16/1814:06 7440-62-2 14.9 ug/L 10.0 2.1 1 10/15/1813:00 10/16/1814:06 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.073J ug/L 0.20 0.036 1 10/15/1816:08 10/16/1813:57 7439-97-6 Analytical Method: EPA 8260B Mod. ND ug/L 2.0 1.9 1 10/15/18 20:06 123-91-1 108 % 50-150 111 % 50-150 Analytical Method: EPA 8260E ND ug/L 100 ND ug/L 200 9.6 ug/L 1.0 ND ug/L 3.0 ND ug/L 1.0 ND ug/L 3.0 ND ug/L 10.0 ND ug/L 100 ND ug/L 100 ND ug/L 1.0 1 10/15/18 20:06 17060-07-0 1 10/15/18 20:06 2037-26-5 8.2 1 10/16/18 02:57 67-64-1 2.5 1 10/16/18 02:57 107-13-1 0.20 1 10/16/18 02:57 71-43-2 0.50 1 10/16/18 02:57 74-97-5 0.36 1 10/16/18 02:57 75-27-4 0.55 1 10/16/18 02:57 75-25-2 0.95 1 10/16/18 02:57 74-83-9 3.2 1 10/16/18 02:57 78-93-3 0.79 1 10/16/18 02:57 75-15-0 0.42 1 10/16/18 02:57 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. N2 B B Page 68 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-MW34 Lab ID: 2610107032 Collected: 10/02/18 13:34 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E 0.56J ug/L 3.0 0.53 1 10/16/18 02:57 108-90-7 ND ug/L 10.0 0.52 1 10/16/18 02:57 75-00-3 ND ug/L 5.0 0.58 1 10/16/18 02:57 67-66-3 ND ug/L 1.0 0.38 1 10/16/18 02:57 74-87-3 ND ug/L 13.0 0.55 1 10/16/18 02:57 96-12-8 ND ug/L 3.0 0.31 1 10/16/18 02:57 124-48-1 ND ug/L 2.0 0.28 1 10/16/18 02:57 106-93-4 ND ug/L 10.0 0.62 1 10/16/18 02:57 74-95-3 ND ug/L 5.0 0.49 1 10/16/18 02:57 95-50-1 1.3 ug/L 1.0 0.58 1 10/16/18 02:57 106-46-7 ND ug/L 100 1.6 1 10/16/18 02:57 110-57-6 1.7J ug/L 5.0 0.41 1 10/16/18 02:57 75-34-3 ND ug/L 1.0 0.67 1 10/16/18 02:57 107-06-2 ND ug/L 5.0 0.72 1 10/16/18 02:57 75-35-4 12.7 ug/L 5.0 0.66 1 10/16/18 02:57 156-59-2 1.1J ug/L 5.0 0.46 1 10/16/18 02:57 156-60-5 ND ug/L 1.0 0.60 1 10/16/18 02:57 78-87-5 ND ug/L 1.0 0.22 1 10/16/18 02:57 10061-01-5 ND ug/L 1.0 0.30 1 10/16/18 02:57 10061-02-6 ND ug/L 1.0 0.45 1 10/16/18 02:57 100-41-4 ND ug/L 50.0 0.89 1 10/16/18 02:57 591-78-6 ND ug/L 10.0 3.1 1 10/16/18 02:57 74-88-4 1.2 ug/L 1.0 0.50 1 10/16/18 02:57 75-09-2 ND ug/L 100 0.86 1 10/16/18 02:57 108-10-1 ND ug/L 1.0 0.50 1 10/16/18 02:57 100-42-5 ND ug/L 5.0 0.32 1 10/16/18 02:57 630-20-6 ND ug/L 3.0 0.53 1 10/16/18 02:57 79-34-5 3.0 ug/L 1.0 0.78 1 10/16/18 02:57 127-18-4 ND ug/L 1.0 0.31 1 10/16/18 02:57 108-88-3 ND ug/L 1.0 0.38 1 10/16/18 02:57 71-55-6 ND ug/L 1.0 0.59 1 10/16/18 02:57 79-00-5 1.0 ug/L 1.0 0.34 1 10/16/18 02:57 79-01-6 ND ug/L 1.0 0.51 1 10/16/18 02:57 75-69-4 ND ug/L 1.0 0.46 1 10/16/18 02:57 96-18-4 ND ug/L 50.0 0.42 1 10/16/18 02:57 108-05-4 2.1 ug/L 1.0 0.60 1 10/16/18 02:57 75-01-4 ND ug/L 5.0 1.5 1 10/16/18 02:57 1330-20-7 105 %. 81-119 1 10/16/18 02:57 17060-07-0 95 %. 82-114 1 10/16/18 02:57 1868-53-7 108 %. 82-120 1 10/16/18 02:57 460-00-4 106 %. 82-109 1 10/16/18 02:57 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. B Page 69 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-Trip Day 1 Lab ID: 2610107033 Collected: 10/01/18 00:00 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E Mod. ND ug/L 2.0 1.9 1 10/12/1812:38 123-91-1 98 % 50-150 1 10/12/1812:38 17060-07-0 104 % 50-150 1 10/12/1812:38 2037-26-5 Analytical Method: EPA 8260E ND ug/L 100 8.2 1 10/13/18 01:27 67-64-1 ND ug/L 200 2.5 1 10/13/18 01:27 107-13-1 ND ug/L 1.0 0.20 1 10/13/18 01:27 71-43-2 ND ug/L 3.0 0.50 1 10/13/18 01:27 74-97-5 ND ug/L 1.0 0.36 1 10/13/18 01:27 75-27-4 ND ug/L 3.0 0.55 1 10/13/18 01:27 75-25-2 ND ug/L 10.0 0.95 1 10/13/18 01:27 74-83-9 ND ug/L 100 3.2 1 10/13/18 01:27 78-93-3 ND ug/L 100 0.79 1 10/13/18 01:27 75-15-0 ND ug/L 1.0 0.42 1 10/13/18 01:27 56-23-5 ND ug/L 3.0 0.53 1 10/13/18 01:27 108-90-7 ND ug/L 10.0 0.52 1 10/13/18 01:27 75-00-3 ND ug/L 5.0 0.58 1 10/13/18 01:27 67-66-3 ND ug/L 1.0 0.38 1 10/13/18 01:27 74-87-3 ND ug/L 13.0 0.55 1 10/13/18 01:27 96-12-8 ND ug/L 3.0 0.31 1 10/13/18 01:27 124-48-1 ND ug/L 2.0 0.28 1 10/13/18 01:27 106-93-4 ND ug/L 10.0 0.62 1 10/13/18 01:27 74-95-3 ND ug/L 5.0 0.49 1 10/13/18 01:27 95-50-1 ND ug/L 1.0 0.58 1 10/13/18 01:27 106-46-7 ND ug/L 100 1.6 1 10/13/18 01:27 110-57-6 ND ug/L 5.0 0.41 1 10/13/18 01:27 75-34-3 ND ug/L 1.0 0.67 1 10/13/18 01:27 107-06-2 ND ug/L 5.0 0.72 1 10/13/18 01:27 75-35-4 ND ug/L 5.0 0.66 1 10/13/18 01:27 156-59-2 ND ug/L 5.0 0.46 1 10/13/18 01:27 156-60-5 ND ug/L 1.0 0.60 1 10/13/18 01:27 78-87-5 ND ug/L 1.0 0.22 1 10/13/18 01:27 10061-01-5 ND ug/L 1.0 0.30 1 10/13/18 01:27 10061-02-6 ND ug/L 1.0 0.45 1 10/13/18 01:27 100-41-4 ND ug/L 50.0 0.89 1 10/13/18 01:27 591-78-6 ND ug/L 10.0 3.1 1 10/13/18 01:27 74-88-4 ND ug/L 1.0 0.50 1 10/13/18 01:27 75-09-2 ND ug/L 100 0.86 1 10/13/18 01:27 108-10-1 ND ug/L 1.0 0.50 1 10/13/18 01:27 100-42-5 ND ug/L 5.0 0.32 1 10/13/18 01:27 630-20-6 ND ug/L 3.0 0.53 1 10/13/18 01:27 79-34-5 ND ug/L 1.0 0.78 1 10/13/18 01:27 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 70 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-Trip Day 1 Lab ID: 2610107033 Collected: 10/01/18 00:00 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Analytical Method: EPA 8260E Toluene ND ug/L 1.0 0.31 1 10/13/18 01:27 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 0.38 1 10/13/18 01:27 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.59 1 10/13/18 01:27 79-00-5 Trichloroethene ND ug/L 1.0 0.34 1 10/13/18 01:27 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.51 1 10/13/18 01:27 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.46 1 10/13/18 01:27 96-18-4 Vinyl acetate ND ug/L 50.0 0.42 1 10/13/18 01:27 108-05-4 Vinyl chloride ND ug/L 1.0 0.60 1 10/13/18 01:27 75-01-4 Xylene (Total) ND ug/L 5.0 1.5 1 10/13/18 01:27 1330-20-7 Surrogates 1,2-Dichloroethane-d4 (S) 100 %. 81-119 1 10/13/18 01:27 17060-07-0 Dibromofluoromethane (S) 97 %. 82-114 1 10/13/18 01:27 1868-53-7 4-Bromofluorobenzene (S) 103 %. 82-120 1 10/13/18 01:27 460-00-4 Toluene-d8 (S) 97 %. 82-109 1 10/13/18 01:27 2037-26-5 Date: 11/07/2018 04:17 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 71 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-Duplicate Lab ID: 2610107034 Collected: 10/02/18 00:00 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene Date: 11/07/2018 04:17 PM Analytical Method: EPA 6020E Preparation Method: EPA 3005A 2.1J ug/L 6.0 0.78 1 10/15/1813:00 10/16/1814:29 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1814:29 7440-38-2 171 ug/L 100 0.78 1 10/15/1813:00 10/16/1814:29 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1814:29 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1814:29 7440-43-9 2.9J ug/L 10.0 1.6 1 10/15/1813:00 10/16/1814:29 7440-47-3 3.1J ug/L 10.0 0.52 1 10/15/1813:00 10/16/1814:29 7440-48-4 4.1J ug/L 10.0 1.3 1 10/15/1813:00 10/16/1814:29 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1814:29 7439-92-1 4.2J ug/L 50.0 0.95 1 10/15/1813:00 10/16/1814:29 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1814:29 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1814:29 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1814:29 7440-28-0 ND ug/L 25.0 1.9 1 10/15/1813:00 10/16/1814:29 7440-62-2 15.5 ug/L 10.0 2.1 1 10/15/1813:00 10/16/1814:29 7440-66-6 B Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.071J ug/L 0.20 0.036 1 10/15/1816:08 10/16/1814:00 7439-97-6 B Analytical Method: EPA 8260E Mod. ND ug/L 2.0 1.9 1 10/15/18 22:03 123-91-1 107 % 50-150 1 10/15/18 22:03 17060-07-0 107 % 50-150 1 10/15/18 22:03 2037-26-5 Analytical Method: EPA 8260E ND ug/L 100 8.2 1 10/16/18 03:22 67-64-1 ND ug/L 200 2.5 1 10/16/18 03:22 107-13-1 9.6 ug/L 1.0 0.20 1 10/16/18 03:22 71-43-2 ND ug/L 3.0 0.50 1 10/16/18 03:22 74-97-5 ND ug/L 1.0 0.36 1 10/16/18 03:22 75-27-4 ND ug/L 3.0 0.55 1 10/16/18 03:22 75-25-2 ND ug/L 10.0 0.95 1 10/16/18 03:22 74-83-9 ND ug/L 100 3.2 1 10/16/18 03:22 78-93-3 ND ug/L 100 0.79 1 10/16/18 03:22 75-15-0 ND ug/L 1.0 0.42 1 10/16/18 03:22 56-23-5 0.61J ug/L 3.0 0.53 1 10/16/18 03:22 108-90-7 ND ug/L 10.0 0.52 1 10/16/18 03:22 75-00-3 ND ug/L 5.0 0.58 1 10/16/18 03:22 67-66-3 ND ug/L 1.0 0.38 1 10/16/18 03:22 74-87-3 ND ug/L 13.0 0.55 1 10/16/18 03:22 96-12-8 ND ug/L 3.0 0.31 1 10/16/18 03:22 124-48-1 ND ug/L 2.0 0.28 1 10/16/18 03:22 106-93-4 ND ug/L 10.0 0.62 1 10/16/18 03:22 74-95-3 ND ug/L 5.0 0.49 1 10/16/18 03:22 95-50-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 72 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-Duplicate Lab ID: 2610107034 Collected: 10/02/18 00:00 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E 1.3 ug/L 1.0 0.58 1 10/16/18 03:22 106-46-7 ND ug/L 100 1.6 1 10/16/18 03:22 110-57-6 1.7J ug/L 5.0 0.41 1 10/16/18 03:22 75-34-3 ND ug/L 1.0 0.67 1 10/16/18 03:22 107-06-2 ND ug/L 5.0 0.72 1 10/16/18 03:22 75-35-4 12.8 ug/L 5.0 0.66 1 10/16/18 03:22 156-59-2 1.1J ug/L 5.0 0.46 1 10/16/18 03:22 156-60-5 0.69J ug/L 1.0 0.60 1 10/16/18 03:22 78-87-5 ND ug/L 1.0 0.22 1 10/16/18 03:22 10061-01-5 ND ug/L 1.0 0.30 1 10/16/18 03:22 10061-02-6 ND ug/L 1.0 0.45 1 10/16/18 03:22 100-41-4 ND ug/L 50.0 0.89 1 10/16/18 03:22 591-78-6 ND ug/L 10.0 3.1 1 10/16/18 03:22 74-88-4 1.2 ug/L 1.0 0.50 1 10/16/18 03:22 75-09-2 ND ug/L 100 0.86 1 10/16/18 03:22 108-10-1 ND ug/L 1.0 0.50 1 10/16/18 03:22 100-42-5 ND ug/L 5.0 0.32 1 10/16/18 03:22 630-20-6 ND ug/L 3.0 0.53 1 10/16/18 03:22 79-34-5 3.0 ug/L 1.0 0.78 1 10/16/18 03:22 127-18-4 ND ug/L 1.0 0.31 1 10/16/18 03:22 108-88-3 ND ug/L 1.0 0.38 1 10/16/18 03:22 71-55-6 ND ug/L 1.0 0.59 1 10/16/18 03:22 79-00-5 1.2 ug/L 1.0 0.34 1 10/16/18 03:22 79-01-6 ND ug/L 1.0 0.51 1 10/16/18 03:22 75-69-4 ND ug/L 1.0 0.46 1 10/16/18 03:22 96-18-4 ND ug/L 50.0 0.42 1 10/16/18 03:22 108-05-4 2.1 ug/L 1.0 0.60 1 10/16/18 03:22 75-01-4 ND ug/L 5.0 1.5 1 10/16/18 03:22 1330-20-7 105 %. 81-119 1 10/16/18 03:22 17060-07-0 95 %. 82-114 1 10/16/18 03:22 1868-53-7 107 %. 82-120 1 10/16/18 03:22 460-00-4 105 %. 82-109 1 10/16/18 03:22 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. B Page 73 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-Equip Blank Lab ID: 2610107035 Collected: 10/04/18 06:11 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene Date: 11/07/2018 04:17 PM Analytical Method: EPA 6020E Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1814:35 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1814:35 7440-38-2 ND ug/L 100 0.78 1 10/15/1813:00 10/16/1814:35 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1814:35 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1814:35 7440-43-9 ND ug/L 10.0 1.6 1 10/15/1813:00 10/16/1814:35 7440-47-3 ND ug/L 10.0 0.52 1 10/15/1813:00 10/16/1814:35 7440-48-4 ND ug/L 10.0 1.3 1 10/15/1813:00 10/16/1814:35 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1814:35 7439-92-1 ND ug/L 50.0 0.95 1 10/15/1813:00 10/16/1814:35 7440-02-0 1.5J ug/L 10.0 1.4 1 10/15/1813:00 10/16/1814:35 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1814:35 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1814:35 7440-28-0 ND ug/L 25.0 1.9 1 10/15/1813:00 10/16/1814:35 7440-62-2 3.4J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1814:35 7440-66-6 B Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.060J ug/L 0.20 0.036 1 10/15/1816:08 10/16/1814:02 7439-97-6 B Analytical Method: EPA 8260E Mod. ND ug/L 2.0 1.9 1 10/17/1812:50 123-91-1 106 % 50-150 1 10/17/1812:50 17060-07-0 116 % 50-150 1 10/17/1812:50 2037-26-5 Analytical Method: EPA 8260E ND ug/L 100 8.2 1 10/15/1816:42 67-64-1 ND ug/L 200 2.5 1 10/15/1816:42 107-13-1 ND ug/L 1.0 0.20 1 10/15/1816:42 71-43-2 ND ug/L 3.0 0.50 1 10/15/1816:42 74-97-5 ND ug/L 1.0 0.36 1 10/15/1816:42 75-27-4 ND ug/L 3.0 0.55 1 10/15/1816:42 75-25-2 ND ug/L 10.0 0.95 1 10/15/1816:42 74-83-9 ND ug/L 100 3.2 1 10/15/1816:42 78-93-3 ND ug/L 100 0.79 1 10/15/1816:42 75-15-0 ND ug/L 1.0 0.42 1 10/15/1816:42 56-23-5 ND ug/L 3.0 0.53 1 10/15/1816:42 108-90-7 ND ug/L 10.0 0.52 1 10/15/1816:42 75-00-3 ND ug/L 5.0 0.58 1 10/15/1816:42 67-66-3 ND ug/L 1.0 0.38 1 10/15/1816:42 74-87-3 ND ug/L 13.0 0.55 1 10/15/1816:42 96-12-8 ND ug/L 3.0 0.31 1 10/15/1816:42 124-48-1 ND ug/L 2.0 0.28 1 10/15/1816:42 106-93-4 ND ug/L 10.0 0.62 1 10/15/1816:42 74-95-3 ND ug/L 5.0 0.49 1 10/15/1816:42 95-50-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 74 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-Equip Blank Lab ID: 2610107035 Collected: 10/04/18 06:11 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 1.0 0.58 1 10/15/1816:42 106-46-7 ND ug/L 100 1.6 1 10/15/1816:42 110-57-6 ND ug/L 5.0 0.41 1 10/15/1816:42 75-34-3 ND ug/L 1.0 0.67 1 10/15/1816:42 107-06-2 ND ug/L 5.0 0.72 1 10/15/1816:42 75-35-4 ND ug/L 5.0 0.66 1 10/15/1816:42 156-59-2 ND ug/L 5.0 0.46 1 10/15/1816:42 156-60-5 ND ug/L 1.0 0.60 1 10/15/1816:42 78-87-5 ND ug/L 1.0 0.22 1 10/15/1816:42 10061-01-5 ND ug/L 1.0 0.30 1 10/15/1816:42 10061-02-6 ND ug/L 1.0 0.45 1 10/15/1816:42 100-41-4 ND ug/L 50.0 0.89 1 10/15/1816:42 591-78-6 ND ug/L 10.0 3.1 1 10/15/1816:42 74-88-4 ND ug/L 1.0 0.50 1 10/15/1816:42 75-09-2 ND ug/L 100 0.86 1 10/15/1816:42 108-10-1 ND ug/L 1.0 0.50 1 10/15/1816:42 100-42-5 ND ug/L 5.0 0.32 1 10/15/1816:42 630-20-6 ND ug/L 3.0 0.53 1 10/15/1816:42 79-34-5 ND ug/L 1.0 0.78 1 10/15/1816:42 127-18-4 ND ug/L 1.0 0.31 1 10/15/1816:42 108-88-3 ND ug/L 1.0 0.38 1 10/15/1816:42 71-55-6 ND ug/L 1.0 0.59 1 10/15/1816:42 79-00-5 ND ug/L 1.0 0.34 1 10/15/1816:42 79-01-6 ND ug/L 1.0 0.51 1 10/15/1816:42 75-69-4 ND ug/L 1.0 0.46 1 10/15/1816:42 96-18-4 ND ug/L 50.0 0.42 1 10/15/1816:42 108-05-4 ND ug/L 1.0 0.60 1 10/15/1816:42 75-01-4 ND ug/L 5.0 1.5 1 10/15/1816:42 1330-20-7 97 %. 81-119 1 10/15/1816:42 17060-07-0 92 %. 82-114 1 10/15/1816:42 1868-53-7 104 %. 82-120 1 10/15/1816:42 460-00-4 101 %. 82-109 1 10/15/1816:42 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 75 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-SW2 Lab ID: 2610107036 Collected: 10/03/18 07:40 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Analytical Method: WF 1 10/16/18 10:28 7.21 Std. Units 1 10/16/18 10:28 20.6 deg C 1 10/16/18 10:28 463 umhos/c 1 10/16/18 10:28 m 2.86 NTU 1 10/16/18 10:28 1.36 ug/L 1 10/16/18 10:28 7782-44-7 N2 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1814:40 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1814:40 7440-38-2 51.3J ug/L 100 0.78 1 10/15/1813:00 10/16/1814:40 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1814:40 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1814:40 7440-43-9 ND ug/L 10.0 1.6 1 10/15/1813:00 10/16/1814:40 7440-47-3 ND ug/L 10.0 0.52 1 10/15/1813:00 10/16/1814:40 7440-48-4 ND ug/L 10.0 1.3 1 10/15/1813:00 10/16/1814:40 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1814:40 7439-92-1 1.OJ ug/L 50.0 0.95 1 10/15/1813:00 10/16/1814:40 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1814:40 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1814:40 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1814:40 7440-28-0 7.4J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1814:40 7440-62-2 4.2J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1814:40 7440-66-6 B Analytical Method: EPA 8260E Mod ND ug/L 2.0 1.9 1 10/17/1816:44 123-91-1 102 % 50-150 1 10/17/1816:44 17060-07-0 115 % 50-150 1 10/17/1816:44 2037-26-5 Analytical Method: EPA 8260E Acetone ND ug/L 100 8.2 1 10/15/18 15:26 67-64-1 Acrylonitrile ND ug/L 200 2.5 1 10/15/18 15:26 107-13-1 Benzene ND ug/L 1.0 0.20 1 10/15/18 15:26 71-43-2 Bromochloromethane ND ug/L 3.0 0.50 1 10/15/18 15:26 74-97-5 Bromodichloromethane ND ug/L 1.0 0.36 1 10/15/18 15:26 75-27-4 Bromoform ND ug/L 3.0 0.55 1 10/15/18 15:26 75-25-2 Bromomethane ND ug/L 10.0 0.95 1 10/15/18 15:26 74-83-9 2-Butanone (MEK) ND ug/L 100 3.2 1 10/15/18 15:26 78-93-3 Carbon disulfide ND ug/L 100 0.79 1 10/15/18 15:26 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.42 1 10/15/18 15:26 56-23-5 Chlorobenzene ND ug/L 3.0 0.53 1 10/15/18 15:26 108-90-7 Chloroethane ND ug/L 10.0 0.52 1 10/15/18 15:26 75-00-3 Chloroform ND ug/L 5.0 0.58 1 10/15/18 15:26 67-66-3 Chloromethane ND ug/L 1.0 0.38 1 10/15/18 15:26 74-87-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 76 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-SW2 Lab ID: 2610107036 Collected: 10/03/18 07:40 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 13.0 0.55 1 10/15/1815:26 96-12-8 ND ug/L 3.0 0.31 1 10/15/1815:26 124-48-1 ND ug/L 2.0 0.28 1 10/15/1815:26 106-93-4 ND ug/L 10.0 0.62 1 10/15/1815:26 74-95-3 ND ug/L 5.0 0.49 1 10/15/1815:26 95-50-1 ND ug/L 1.0 0.58 1 10/15/1815:26 106-46-7 ND ug/L 100 1.6 1 10/15/1815:26 110-57-6 ND ug/L 5.0 0.41 1 10/15/1815:26 75-34-3 ND ug/L 1.0 0.67 1 10/15/1815:26 107-06-2 ND ug/L 5.0 0.72 1 10/15/1815:26 75-35-4 ND ug/L 5.0 0.66 1 10/15/1815:26 156-59-2 ND ug/L 5.0 0.46 1 10/15/1815:26 156-60-5 ND ug/L 1.0 0.60 1 10/15/1815:26 78-87-5 ND ug/L 1.0 0.22 1 10/15/1815:26 10061-01-5 ND ug/L 1.0 0.30 1 10/15/1815:26 10061-02-6 ND ug/L 1.0 0.45 1 10/15/1815:26 100-41-4 ND ug/L 50.0 0.89 1 10/15/1815:26 591-78-6 ND ug/L 10.0 3.1 1 10/15/1815:26 74-88-4 ND ug/L 1.0 0.50 1 10/15/1815:26 75-09-2 ND ug/L 100 0.86 1 10/15/1815:26 108-10-1 ND ug/L 1.0 0.50 1 10/15/1815:26 100-42-5 ND ug/L 5.0 0.32 1 10/15/1815:26 630-20-6 ND ug/L 3.0 0.53 1 10/15/1815:26 79-34-5 ND ug/L 1.0 0.78 1 10/15/1815:26 127-18-4 ND ug/L 1.0 0.31 1 10/15/1815:26 108-88-3 ND ug/L 1.0 0.38 1 10/15/1815:26 71-55-6 ND ug/L 1.0 0.59 1 10/15/1815:26 79-00-5 ND ug/L 1.0 0.34 1 10/15/1815:26 79-01-6 ND ug/L 1.0 0.51 1 10/15/1815:26 75-69-4 ND ug/L 1.0 0.46 1 10/15/1815:26 96-18-4 ND ug/L 50.0 0.42 1 10/15/1815:26 108-05-4 ND ug/L 1.0 0.60 1 10/15/1815:26 75-01-4 ND ug/L 5.0 1.5 1 10/15/1815:26 1330-20-7 101 %. 81-119 1 10/15/1815:26 17060-07-0 92 %. 82-114 1 10/15/1815:26 1868-53-7 106 %. 82-120 1 10/15/1815:26 460-00-4 100 %. 82-109 1 10/15/1815:26 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 77 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-SW1 Lab ID: 2610107037 Collected: 10/03/18 08:05 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance Field Turbidity Oxygen, Dissolved 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Analytical Method: WF 1 10/16/18 10:28 7.67 Std. Units 1 10/16/18 10:28 21.6 deg C 1 10/16/18 10:28 272 umhos/c 1 10/16/18 10:28 m 9.31 NTU 1 10/16/18 10:28 1.19 ug/L 1 10/16/18 10:28 7782-44-7 N2 Analytical Method: EPA 6020B Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1814:46 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1814:46 7440-38-2 42.6J ug/L 100 0.78 1 10/15/1813:00 10/16/1814:46 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1814:46 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1814:46 7440-43-9 ND ug/L 10.0 1.6 1 10/15/1813:00 10/16/1814:46 7440-47-3 0.56J ug/L 10.0 0.52 1 10/15/1813:00 10/16/1814:46 7440-48-4 2.4J ug/L 10.0 1.3 1 10/15/1813:00 10/16/1814:46 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1814:46 7439-92-1 ND ug/L 50.0 0.95 1 10/15/1813:00 10/16/1814:46 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1814:46 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1814:46 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1814:46 7440-28-0 3.2J ug/L 25.0 1.9 1 10/15/1813:00 10/16/1814:46 7440-62-2 4.7J ug/L 10.0 2.1 1 10/15/1813:00 10/16/1814:46 7440-66-6 B Analytical Method: EPA 8260E Mod ND ug/L 2.0 1.9 1 10/17/1817:04 123-91-1 104 % 50-150 1 10/17/1817:04 17060-07-0 113 % 50-150 1 10/17/1817:04 2037-26-5 Analytical Method: EPA 8260E Acetone ND ug/L 100 8.2 1 10/15/18 15:51 67-64-1 Acrylonitrile ND ug/L 200 2.5 1 10/15/18 15:51 107-13-1 Benzene ND ug/L 1.0 0.20 1 10/15/18 15:51 71-43-2 Bromochloromethane ND ug/L 3.0 0.50 1 10/15/18 15:51 74-97-5 Bromodichloromethane ND ug/L 1.0 0.36 1 10/15/18 15:51 75-27-4 Bromoform ND ug/L 3.0 0.55 1 10/15/18 15:51 75-25-2 Bromomethane ND ug/L 10.0 0.95 1 10/15/18 15:51 74-83-9 2-Butanone (MEK) ND ug/L 100 3.2 1 10/15/18 15:51 78-93-3 Carbon disulfide ND ug/L 100 0.79 1 10/15/18 15:51 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.42 1 10/15/18 15:51 56-23-5 Chlorobenzene ND ug/L 3.0 0.53 1 10/15/18 15:51 108-90-7 Chloroethane ND ug/L 10.0 0.52 1 10/15/18 15:51 75-00-3 Chloroform ND ug/L 5.0 0.58 1 10/15/18 15:51 67-66-3 Chloromethane ND ug/L 1.0 0.38 1 10/15/18 15:51 74-87-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 78 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-SW1 Lab ID: 2610107037 Collected: 10/03/18 08:05 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 13.0 0.55 1 10/15/1815:51 96-12-8 ND ug/L 3.0 0.31 1 10/15/1815:51 124-48-1 ND ug/L 2.0 0.28 1 10/15/1815:51 106-93-4 ND ug/L 10.0 0.62 1 10/15/1815:51 74-95-3 ND ug/L 5.0 0.49 1 10/15/1815:51 95-50-1 ND ug/L 1.0 0.58 1 10/15/1815:51 106-46-7 ND ug/L 100 1.6 1 10/15/1815:51 110-57-6 ND ug/L 5.0 0.41 1 10/15/1815:51 75-34-3 ND ug/L 1.0 0.67 1 10/15/1815:51 107-06-2 ND ug/L 5.0 0.72 1 10/15/1815:51 75-35-4 ND ug/L 5.0 0.66 1 10/15/1815:51 156-59-2 ND ug/L 5.0 0.46 1 10/15/1815:51 156-60-5 ND ug/L 1.0 0.60 1 10/15/1815:51 78-87-5 ND ug/L 1.0 0.22 1 10/15/1815:51 10061-01-5 ND ug/L 1.0 0.30 1 10/15/1815:51 10061-02-6 ND ug/L 1.0 0.45 1 10/15/1815:51 100-41-4 ND ug/L 50.0 0.89 1 10/15/1815:51 591-78-6 ND ug/L 10.0 3.1 1 10/15/1815:51 74-88-4 ND ug/L 1.0 0.50 1 10/15/1815:51 75-09-2 ND ug/L 100 0.86 1 10/15/1815:51 108-10-1 ND ug/L 1.0 0.50 1 10/15/1815:51 100-42-5 ND ug/L 5.0 0.32 1 10/15/1815:51 630-20-6 ND ug/L 3.0 0.53 1 10/15/1815:51 79-34-5 ND ug/L 1.0 0.78 1 10/15/1815:51 127-18-4 ND ug/L 1.0 0.31 1 10/15/1815:51 108-88-3 ND ug/L 1.0 0.38 1 10/15/1815:51 71-55-6 ND ug/L 1.0 0.59 1 10/15/1815:51 79-00-5 ND ug/L 1.0 0.34 1 10/15/1815:51 79-01-6 ND ug/L 1.0 0.51 1 10/15/1815:51 75-69-4 ND ug/L 1.0 0.46 1 10/15/1815:51 96-18-4 ND ug/L 50.0 0.42 1 10/15/1815:51 108-05-4 ND ug/L 1.0 0.60 1 10/15/1815:51 75-01-4 ND ug/L 5.0 1.5 1 10/15/1815:51 1330-20-7 102 %. 81-119 1 10/15/1815:51 17060-07-0 93 %. 82-114 1 10/15/1815:51 1868-53-7 109 %. 82-120 1 10/15/1815:51 460-00-4 98 %. 82-109 1 10/15/1815:51 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 79 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-Field Blank Lab ID: 2610107038 Collected: 10/03/18 09:27 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 7470 Mercury Mercury 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene Date: 11/07/2018 04:17 PM Analytical Method: EPA 6020E Preparation Method: EPA 3005A ND ug/L 6.0 0.78 1 10/15/1813:00 10/16/1815:06 7440-36-0 ND ug/L 10.0 0.57 1 10/15/1813:00 10/16/1815:06 7440-38-2 ND ug/L 100 0.78 1 10/15/1813:00 10/16/1815:06 7440-39-3 ND ug/L 1.0 0.050 1 10/15/1813:00 10/16/1815:06 7440-41-7 ND ug/L 1.0 0.093 1 10/15/1813:00 10/16/1815:06 7440-43-9 ND ug/L 10.0 1.6 1 10/15/1813:00 10/16/1815:06 7440-47-3 ND ug/L 10.0 0.52 1 10/15/1813:00 10/16/1815:06 7440-48-4 ND ug/L 10.0 1.3 1 10/15/1813:00 10/16/1815:06 7440-50-8 ND ug/L 10.0 0.27 1 10/15/1813:00 10/16/1815:06 7439-92-1 ND ug/L 50.0 0.95 1 10/15/1813:00 10/16/1815:06 7440-02-0 ND ug/L 10.0 1.4 1 10/15/1813:00 10/16/1815:06 7782-49-2 ND ug/L 10.0 0.95 1 10/15/1813:00 10/16/1815:06 7440-22-4 ND ug/L 5.5 0.14 1 10/15/1813:00 10/16/1815:06 7440-28-0 ND ug/L 25.0 1.9 1 10/15/1813:00 10/16/1815:06 7440-62-2 3.OJ ug/L 10.0 2.1 1 10/15/1813:00 10/16/1815:06 7440-66-6 B Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.066J ug/L 0.20 0.036 1 10/15/1816:08 10/16/1814:04 7439-97-6 B Analytical Method: EPA 8260E Mod. ND ug/L 2.0 1.9 1 10/17/1812:31 123-91-1 105 % 50-150 1 10/17/1812:31 17060-07-0 114 % 50-150 1 10/17/1812:31 2037-26-5 Analytical Method: EPA 8260E ND ug/L 100 8.2 1 10/15/1816:17 67-64-1 ND ug/L 200 2.5 1 10/15/1816:17 107-13-1 ND ug/L 1.0 0.20 1 10/15/1816:17 71-43-2 ND ug/L 3.0 0.50 1 10/15/1816:17 74-97-5 ND ug/L 1.0 0.36 1 10/15/1816:17 75-27-4 ND ug/L 3.0 0.55 1 10/15/1816:17 75-25-2 ND ug/L 10.0 0.95 1 10/15/1816:17 74-83-9 ND ug/L 100 3.2 1 10/15/1816:17 78-93-3 ND ug/L 100 0.79 1 10/15/1816:17 75-15-0 ND ug/L 1.0 0.42 1 10/15/1816:17 56-23-5 ND ug/L 3.0 0.53 1 10/15/1816:17 108-90-7 ND ug/L 10.0 0.52 1 10/15/1816:17 75-00-3 ND ug/L 5.0 0.58 1 10/15/1816:17 67-66-3 ND ug/L 1.0 0.38 1 10/15/1816:17 74-87-3 ND ug/L 13.0 0.55 1 10/15/1816:17 96-12-8 ND ug/L 3.0 0.31 1 10/15/1816:17 124-48-1 ND ug/L 2.0 0.28 1 10/15/1816:17 106-93-4 ND ug/L 10.0 0.62 1 10/15/1816:17 74-95-3 ND ug/L 5.0 0.49 1 10/15/1816:17 95-50-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 80 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Sample: 1304-Field Blank Lab ID: 2610107038 Collected: 10/03/18 09:27 Received: 10/04/18 08:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pe n to n o n e (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 11/07/2018 04:17 PM Analytical Method: EPA 8260E ND ug/L 1.0 0.58 1 10/15/1816:17 106-46-7 ND ug/L 100 1.6 1 10/15/1816:17 110-57-6 ND ug/L 5.0 0.41 1 10/15/1816:17 75-34-3 ND ug/L 1.0 0.67 1 10/15/1816:17 107-06-2 ND ug/L 5.0 0.72 1 10/15/1816:17 75-35-4 ND ug/L 5.0 0.66 1 10/15/1816:17 156-59-2 ND ug/L 5.0 0.46 1 10/15/1816:17 156-60-5 ND ug/L 1.0 0.60 1 10/15/1816:17 78-87-5 ND ug/L 1.0 0.22 1 10/15/1816:17 10061-01-5 ND ug/L 1.0 0.30 1 10/15/1816:17 10061-02-6 ND ug/L 1.0 0.45 1 10/15/1816:17 100-41-4 ND ug/L 50.0 0.89 1 10/15/1816:17 591-78-6 ND ug/L 10.0 3.1 1 10/15/1816:17 74-88-4 ND ug/L 1.0 0.50 1 10/15/1816:17 75-09-2 ND ug/L 100 0.86 1 10/15/1816:17 108-10-1 ND ug/L 1.0 0.50 1 10/15/1816:17 100-42-5 ND ug/L 5.0 0.32 1 10/15/1816:17 630-20-6 ND ug/L 3.0 0.53 1 10/15/1816:17 79-34-5 ND ug/L 1.0 0.78 1 10/15/1816:17 127-18-4 ND ug/L 1.0 0.31 1 10/15/1816:17 108-88-3 ND ug/L 1.0 0.38 1 10/15/1816:17 71-55-6 ND ug/L 1.0 0.59 1 10/15/1816:17 79-00-5 ND ug/L 1.0 0.34 1 10/15/1816:17 79-01-6 ND ug/L 1.0 0.51 1 10/15/1816:17 75-69-4 ND ug/L 1.0 0.46 1 10/15/1816:17 96-18-4 ND ug/L 50.0 0.42 1 10/15/1816:17 108-05-4 ND ug/L 1.0 0.60 1 10/15/1816:17 75-01-4 ND ug/L 5.0 1.5 1 10/15/1816:17 1330-20-7 101 %. 81-119 1 10/15/1816:17 17060-07-0 93 %. 82-114 1 10/15/1816:17 1868-53-7 105 %. 82-120 1 10/15/1816:17 460-00-4 101 %. 82-109 1 10/15/1816:17 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 81 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 QC Batch: 15401 Analysis Method: EPA 7470A QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury Associated Lab Samples: 2610107001, 2610107002, 2610107003, 2610107004, 2610107005, 2610107006, 2610107007, 2610107008, 2610107009, 2610107010, 2610107011, 2610107012, 2610107013, 2610107014, 2610107015, 2610107016, 2610107017, 2610107018, 2610107019, 2610107020 METHOD BLANK: 68872 Matrix: Water Associated Lab Samples: 2610107001, 2610107002, 2610107003, 2610107004, 2610107005, 2610107006, 2610107007, 2610107008, 2610107009, 2610107010, 2610107011, 2610107012, 2610107013, 2610107014, 2610107015, 2610107016, 2610107017, 2610107018, 2610107019, 2610107020 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury ug/L 0.065J 0.20 0.036 10/16/1811:25 LABORATORY CONTROL SAMPLE: 68873 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.7 106 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 68874 68875 MS MSD 2610107001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L 0.058J 2.5 2.5 2.7 2.7 104 105 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 82 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 QC Batch: 15402 Analysis Method: EPA 7470A QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury Associated Lab Samples: 2610107021, 2610107022, 2610107023, 2610107024, 2610107025, 2610107026, 2610107027, 2610107028, 2610107029,2610107030,2610107032,2610107034,2610107035,2610107038 METHOD BLANK: 68876 Matrix: Water Associated Lab Samples: 2610107021, 2610107022, 2610107023, 2610107024, 2610107025, 2610107026, 2610107027, 2610107028, 2610107029,2610107030,2610107032,2610107034,2610107035,2610107038 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury ug/L 0.064J 0.20 0.036 10/16/1813:17 LABORATORY CONTROL SAMPLE: 68877 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.7 107 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 68878 68879 MS MSD 2610107021 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L ND 2.5 2.5 2.5 2.1 99 83 75-125 18 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 83 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 QC Batch: 15369 Analysis Method: EPA 6020B QC Batch Method: EPA 3005A Analysis Description: 6020E MET Associated Lab Samples: 2610107001, 2610107002, 2610107003, 2610107004, 2610107005, 2610107006, 2610107007, 2610107008, 2610107009, 2610107010, 2610107011, 2610107012, 2610107013, 2610107014, 2610107015, 2610107016, 2610107017, 2610107018, 2610107019, 2610107020 METHOD BLANK: 68790 Matrix: Water Associated Lab Samples: 2610107001, 2610107002, 2610107003, 2610107004, 2610107005, 2610107006, 2610107007, 2610107008, 2610107009, 2610107010, 2610107011, 2610107012, 2610107013, 2610107014, 2610107015, 2610107016, 2610107017, 2610107018, 2610107019, 2610107020 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Antimony ug/L ND 6.0 0.78 10/16/1816:46 Arsenic ug/L ND 10.0 0.57 10/16/1816:46 Barium ug/L ND 100 0.78 10/16/1816:46 Beryllium ug/L ND 1.0 0.050 10/16/1816:46 Cadmium ug/L ND 1.0 0.093 10/16/1816:46 Chromium ug/L ND 10.0 1.6 10/16/1816:46 Cobalt ug/L ND 10.0 0.52 10/16/1816:46 Copper ug/L ND 10.0 1.3 10/16/1816:46 Lead ug/L ND 10.0 0.27 10/16/1816:46 Nickel ug/L ND 50.0 0.95 10/16/1816:46 Selenium ug/L ND 10.0 1.4 10/16/1816:46 Silver ug/L ND 10.0 0.95 10/16/1816:46 Thallium ug/L ND 5.5 0.14 10/16/1816:46 Vanadium ug/L ND 25.0 1.9 10/16/1816:46 Zinc ug/L 2AJ 10.0 2.1 10/16/1816:46 LABORATORY CONTROL SAMPLE: 68791 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Antimony ug/L 100 106 106 80-120 Arsenic ug/L 100 98.2 98 80-120 Barium ug/L 100 97.7J 98 80-120 Beryllium ug/L 100 99.4 99 80-120 Cadmium ug/L 100 103 103 80-120 Chromium ug/L 100 103 103 80-120 Cobalt ug/L 100 99.6 100 80-120 Copper ug/L 100 101 101 80-120 Lead ug/L 100 101 101 80-120 Nickel ug/L 100 100 100 80-120 Selenium ug/L 100 100 100 80-120 Silver ug/L 100 102 102 80-120 Thallium ug/L 100 100 100 80-120 Vanadium ug/L 100 104 104 80-120 Zinc ug/L 100 106 106 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 84 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Pace Project No.: Charlotte Motor Speedway V LF 2610107 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 68792 68793 MS MSD 2610107014 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 100 100 106 108 106 108 75-125 2 20 Arsenic ug/L ND 100 100 99.4 101 99 101 75-125 1 20 Barium ug/L 275 100 100 366 364 91 89 75-125 1 20 Beryllium ug/L ND 100 100 94.3 95.7 94 96 75-125 2 20 Cadmium ug/L ND 100 100 102 104 102 104 75-125 2 20 Chromium ug/L ND 100 100 104 102 104 102 75-125 2 20 Cobalt ug/L 1.4J 100 100 101 102 100 100 75-125 0 20 Copper ug/L ND 100 100 99.7 100 99 100 75-125 0 20 Lead ug/L ND 100 100 96.5 100 96 100 75-125 4 20 Nickel ug/L 59.7 100 100 159 159 100 99 75-125 0 20 Selenium ug/L ND 100 100 100 99.4 100 99 75-125 1 20 Silver ug/L ND 100 100 97.5 99.1 97 99 75-125 2 20 Thallium ug/L ND 100 100 97.2 98.7 97 99 75-125 2 20 Vanadium ug/L ND 100 100 106 107 106 107 75-125 1 20 Zinc ug/L 3.5J 100 100 104 107 100 103 75-125 3 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 85 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 QC Batch: 15379 Analysis Method: EPA 6020B QC Batch Method: EPA 3005A Analysis Description: 6020E MET Associated Lab Samples: 2610107021, 2610107022, 2610107023, 2610107024, 2610107025, 2610107026, 2610107027, 2610107028, 2610107029, 2610107030, 2610107032, 2610107034, 2610107035, 2610107036, 2610107037, 2610107038 METHOD BLANK: 68820 Matrix: Water Associated Lab Samples: 2610107021, 2610107022, 2610107023, 2610107024, 2610107025, 2610107026, 2610107027, 2610107028, 2610107029, 2610107030, 2610107032, 2610107034, 2610107035, 2610107036, 2610107037, 2610107038 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Antimony ug/L ND 6.0 0.78 10/16/1812:38 Arsenic ug/L ND 10.0 0.57 10/16/1812:38 Barium ug/L ND 100 0.78 10/16/1812:38 Beryllium ug/L ND 1.0 0.050 10/16/1812:38 Cadmium ug/L ND 1.0 0.093 10/16/1812:38 Chromium ug/L ND 10.0 1.6 10/16/1812:38 Cobalt ug/L ND 10.0 0.52 10/16/1812:38 Copper ug/L ND 10.0 1.3 10/16/1812:38 Lead ug/L ND 10.0 0.27 10/16/1812:38 Nickel ug/L ND 50.0 0.95 10/16/1812:38 Selenium ug/L ND 10.0 1.4 10/16/1812:38 Silver ug/L ND 10.0 0.95 10/16/1812:38 Thallium ug/L ND 5.5 0.14 10/16/1812:38 Vanadium ug/L ND 25.0 1.9 10/16/1812:38 Zinc ug/L 2.8J 10.0 2.1 10/16/1812:38 LABORATORY CONTROL SAMPLE: Parameter 68821 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Antimony ug/L 100 110 110 80-120 Arsenic ug/L 100 98.4 98 80-120 Barium ug/L 100 102 102 80-120 Beryllium ug/L 100 99.7 100 80-120 Cadmium ug/L 100 103 103 80-120 Chromium ug/L 100 103 103 80-120 Cobalt ug/L 100 101 101 80-120 Copper ug/L 100 101 101 80-120 Lead ug/L 100 100 100 80-120 Nickel ug/L 100 103 103 80-120 Selenium ug/L 100 98.7 99 80-120 Silver ug/L 100 102 102 80-120 Thallium ug/L 100 99.2 99 80-120 Vanadium ug/L 100 106 106 80-120 Zinc ug/L 100 106 106 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 86 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Pace Project No.: Charlotte Motor Speedway V LF 2610107 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 68822 68823 MS MSD 2610107032 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 100 100 111 109 111 109 75-125 2 20 Arsenic ug/L ND 100 100 102 99.7 102 100 75-125 3 20 Barium ug/L 179 100 100 272 265 93 85 75-125 3 20 Beryllium ug/L ND 100 100 99.8 101 100 101 75-125 1 20 Cadmium ug/L ND 100 100 104 104 104 103 75-125 1 20 Chromium ug/L 2.3J 100 100 106 112 104 110 75-125 5 20 Cobalt ug/L 2.6J 100 100 102 108 99 105 75-125 6 20 Copper ug/L 4.2J 100 100 106 109 102 105 75-125 3 20 Lead ug/L ND 100 100 101 98.6 101 99 75-125 3 20 Nickel ug/L 3.9J 100 100 105 109 101 106 75-125 4 20 Selenium ug/L ND 100 100 101 101 101 100 75-125 0 20 Silver ug/L ND 100 100 105 103 105 103 75-125 2 20 Thallium ug/L ND 100 100 99.9 98.0 100 98 75-125 2 20 Vanadium ug/L ND 100 100 109 113 108 112 75-125 3 20 Zinc ug/L 14.9 100 100 116 120 102 105 75-125 3 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 87 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 QC Batch: 435960 Analysis Method: EPA 8260B Mod. QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM Associated Lab Samples: 2610107001, 2610107002, 2610107003, 2610107004, 2610107005, 2610107006, 2610107007, 2610107008, 2610107009,2610107011,2610107012,2610107013,2610107016,2610107019,2610107021,2610107022, 2610107023,2610107033 METHOD BLANK: 2399108 Matrix: Water Associated Lab Samples: 2610107001, 2610107002, 2610107003, 2610107004, 2610107005, 2610107006, 2610107007, 2610107008, 2610107009,2610107011,2610107012,2610107013,2610107016,2610107019,2610107021,2610107022, 2610107023,2610107033 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 1.9 10/12/18 12:18 1,2-Dichloroethane-d4 (S) % 99 50-150 10/12/18 12:18 Toluene-d8 (S) % 105 50-150 10/12/18 12:18 LABORATORY CONTROL SAMPLE: 2399109 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane(p-Dioxane) ug/L 20 21.3 107 71-125 1,2-Dichloroethane-d4 (S) % 103 50-150 Toluene-d8(S) % 106 50-150 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399110 2399111 MS MSD 92402028009 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane(p-Dioxane) ug/L 5.7 20 20 35.9 37.1 151 157 50-150 3 30 M1 1,2-Dichloroethane-d4 (S) % 110 108 50-150 30 Toluene-d8(S) % 110 107 50-150 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 88 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 QC Batch: 435961 Analysis Method: EPA 8260B Mod. QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM Associated Lab Samples: 2610107024, 2610107026 METHOD BLANK: 2399114 Matrix: Water Associated Lab Samples: 2610107024, 2610107026 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 1.9 10/12/18 11:59 1,2-Dichloroethane-d4 (S) % 99 50-150 10/12/18 11:59 Toluene-d8 (S) % 103 50-150 10/12/18 11:59 LABORATORY CONTROL SAMPLE: 2399115 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 20.8 104 71-125 1,2-Dichloroethane-d4 (S) % 101 50-150 Toluene-d8(S) % 103 50-150 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399116 2399117 MS MSD 92402488001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 20 20 21.2 22.1 106 111 50-150 4 30 1,2-Dichloroethane-d4 (S) % 103 105 50-150 30 Toluene-d8 (S) % 105 107 50-150 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 89 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 QC Batch: 436230 Analysis Method: EPA 8260B Mod. QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM Associated Lab Samples: 2610107027, 2610107028, 2610107029, 2610107030, 2610107032 METHOD BLANK: 2400347 Matrix: Water Associated Lab Samples: 2610107027, 2610107028, 2610107029, 2610107030, 2610107032 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 1.9 10/15/18 13:17 1,2-Dichloroethane-d4 (S) % 105 50-150 10/15/18 13:17 Toluene-d8 (S) % 109 50-150 10/15/18 13:17 LABORATORY CONTROL SAMPLE: 2400348 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 22.0 110 71-125 1,2-Dichloroethane-d4 (S) % 101 50-150 Toluene-d8(S) % 106 50-150 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2400349 2400350 MS MSD 2610107032 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 20 20 19.8 19.6 99 98 50-150 1 30 1,2-Dichloroethane-d4 (S) % 112 102 50-150 30 Toluene-d8 (S) % 115 116 50-150 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 90 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 QC Batch: 436231 Analysis Method: EPA 8260B Mod. QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM Associated Lab Samples: 2610107034 METHOD BLANK: 2400351 Associated Lab Samples: 2610107034 Parameter Units 1,4-Dioxane (p-Dioxane) ug/L 1,2-Dichloroethane-d4 (S) % Toluene-d8 (S) % Matrix: Water Blank Reporting Result Limit ND 2.0 102 50-150 108 50-150 MDL Analyzed 1.9 10/15/18 12:57 10/15/18 12:57 10/15/18 12:57 Qualifiers LABORATORY CONTROL SAMPLE: 2400352 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 21.0 105 71-125 1,2-Dichloroethane-d4 (S) % 107 50-150 Toluene-d8(S) % 108 50-150 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2400353 2400354 MS MSD 92402906002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 20 20 19.5 20.5 98 103 50-150 5 30 1,2-Dichloroethane-d4 (S) % 104 103 50-150 30 Toluene-d8 (S) % 115 114 50-150 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 91 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 QC Batch: 436645 Analysis Method: EPA 8260B Mod. QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM Associated Lab Samples: 2610107010, 2610107014, 2610107015, 2610107017, 2610107020, 2610107025, 2610107035, 2610107036, 2610107037,2610107038 METHOD BLANK: 2402221 Matrix: Water Associated Lab Samples: 2610107010, 2610107014, 2610107015, 2610107017, 2610107020, 2610107025, 2610107035, 2610107036, 2610107037,2610107038 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 1.9 10/17/18 11:52 1,2-Dichloroethane-d4 (S) % 105 50-150 10/17/18 11:52 Toluene-d8 (S) % 115 50-150 10/17/18 11:52 LABORATORY CONTROL SAMPLE: 2402222 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 19.1 95 71-125 1,2-Dichloroethane-d4 (S) % 102 50-150 Toluene-d8 (S) % 109 50-150 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2402223 2402224 MS MSD 2610107037 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 20 20 17.9 19.2 90 96 50-150 7 30 1,2-Dichloroethane-d4 (S) % 105 105 50-150 30 Toluene-d8(S) % 114 122 50-150 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 92 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 QC Batch: 438946 Analysis Method: EPA 8260B Mod. QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM Associated Lab Samples: 2610107018 METHOD BLANK: 2412709 Associated Lab Samples: 2610107018 Parameter Units 1,4-Dioxane (p-Dioxane) ug/L 1,2-Dichloroethane-d4 (S) % Toluene-d8 (S) % Matrix: Water Blank Reporting Result Limit ND 2.0 97 50-150 101 50-150 MDL Analyzed 1.9 10/29/18 11:58 10/29/18 11:58 10/29/18 11:58 Qualifiers LABORATORY CONTROL SAMPLE: 2412710 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 20.2 101 71-125 1,2-Dichloroethane-d4 (S) % 95 50-150 Toluene-d8 (S) % 96 50-150 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2412711 2412712 MS MSD 92403967004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane (p-Dioxane) ug/L 6.4 20 20 25.7 29.0 96 113 50-150 12 30 1,2-Dichloroethane-d4 (S) % 95 97 50-150 30 Toluene-d8 (S) % 86 101 50-150 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 93 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 QC Batch: 15268 Analysis Method: EPA 8260B QC Batch Method: EPA 8260E Analysis Description: 8260E MSV Associated Lab Samples: 2610107001, 2610107002, 2610107003, 2610107004, 2610107017, 2610107021, 2610107022, 2610107023, 2610107033 METHOD BLANK: 68329 Matrix: Water Associated Lab Samples: 2610107001, 2610107002, 2610107003, 2610107004, 2610107017, 2610107021, 2610107022, 2610107023, 2610107033 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 5.0 0.32 10/12/18 11:04 1,1,1-Trichloroethane ug/L ND 1.0 0.38 10/12/18 11:04 1,1,2,2-Tetrachloroethane ug/L ND 3.0 0.53 10/12/18 11:04 1,1,2-Trichloroethane ug/L ND 1.0 0.59 10/12/18 11:04 1,1-Dichloroethane ug/L ND 5.0 0.41 10/12/18 11:04 1,1-Dichloroethene ug/L ND 5.0 0.72 10/12/18 11:04 1,2,3-Trichloropropane ug/L ND 1.0 0.46 10/12/18 11:04 1,2-Dibromo-3-chloropropane ug/L ND 13.0 0.55 10/12/18 11:04 1,2-Dibromoethane (EDB) ug/L ND 2.0 0.28 10/12/18 11:04 1,2-Dichlorobenzene ug/L ND 5.0 0.49 10/12/18 11:04 1,2-Dichloroethane ug/L ND 1.0 0.67 10/12/18 11:04 1,2-Dichloropropane ug/L ND 1.0 0.60 10/12/18 11:04 1,4-Dichlorobenzene ug/L ND 1.0 0.58 10/12/18 11:04 2-Butanone (MEK) ug/L ND 100 3.2 10/12/18 11:04 2-Hexanone ug/L ND 50.0 0.89 10/12/18 11:04 4-Methyl-2-pentanone (MIBK) ug/L ND 100 0.86 10/12/18 11:04 Acetone ug/L ND 100 8.2 10/12/18 11:04 Acrylonitrile ug/L ND 200 2.5 10/12/18 11:04 Benzene ug/L ND 1.0 0.20 10/12/18 11:04 Bromochloromethane ug/L ND 3.0 0.50 10/12/18 11:04 Bromodichloromethane ug/L ND 1.0 0.36 10/12/18 11:04 Bromoform ug/L ND 3.0 0.55 10/12/18 11:04 Bromomethane ug/L ND 10.0 0.95 10/12/18 11:04 Carbon disulfide ug/L ND 100 0.79 10/12/18 11:04 Carbon tetrachloride ug/L ND 1.0 0.42 10/12/18 11:04 Chlorobenzene ug/L ND 3.0 0.53 10/12/18 11:04 Chloroethane ug/L ND 10.0 0.52 10/12/18 11:04 Chloroform ug/L ND 5.0 0.58 10/12/18 11:04 Chloromethane ug/L ND 1.0 0.38 10/12/18 11:04 cis-1,2-Dichloroethene ug/L ND 5.0 0.66 10/12/18 11:04 cis-1,3-Dichloropropene ug/L ND 1.0 0.22 10/12/18 11:04 Dibromochloromethane ug/L ND 3.0 0.31 10/12/18 11:04 Dibromomethane ug/L ND 10.0 0.62 10/12/18 11:04 Ethylbenzene ug/L ND 1.0 0.45 10/12/18 11:04 lodomethane ug/L ND 10.0 3.1 10/12/18 11:04 Methylene Chloride ug/L ND 1.0 0.50 10/12/18 11:04 Styrene ug/L ND 1.0 0.50 10/12/18 11:04 Tetrachloroethene ug/L ND 1.0 0.78 10/12/18 11:04 Toluene ug/L ND 1.0 0.31 10/12/18 11:04 trans-1,2-Dichloroethene ug/L ND 5.0 0.46 10/12/18 11:04 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 94 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 METHOD BLANK: 68329 Matrix: Water Associated Lab Samples: 2610107001,2610107002,2610107003,2610107004,2610107017,2610107021,2610107022,2610107023, 2610107033 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers trans- 1,3-Dichloropropene ug/L ND 1.0 0.30 10/12/18 11:04 trans-1,4-Dichloro-2-butene ug/L ND 100 1.6 10/12/18 11:04 Trichloroethene ug/L ND 1.0 0.34 10/12/18 11:04 Trichlorofluoromethane ug/L ND 1.0 0.51 10/12/18 11:04 Vinyl acetate ug/L ND 50.0 0.42 10/12/18 11:04 Vinyl chloride ug/L ND 1.0 0.60 10/12/18 11:04 Xylene (Total) ug/L ND 5.0 1.5 10/12/18 11:04 1,2-Dichloroethane-d4 (S) %. 95 81-119 10/12/18 11:04 4-Bromofluorobenzene (S) %. 105 82-120 10/12/18 11:04 Dibromofluoromethane (S) %. 94 82-114 10/12/18 11:04 Toluene-d8 (S) %. 94 82-109 10/12/18 11:04 LABORATORY CONTROL SAMPLE: 68330 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 50.8 102 68-137 1,1,1-Trichloroethane ug/L 50 59.1 118 72-134 1,1,2,2-Tetrachloroethane ug/L 50 51.9 104 51-158 1,1,2-Trichloroethane ug/L 50 51.9 104 78-131 1,1-Dichloroethane ug/L 50 55.0 110 69-151 1,1-Dichloroethene ug/L 50 46.8 94 64-158 1,2,3-Trichloropropane ug/L 50 47.1 94 78-133 1,2-Dibromo-3-chloropropane ug/L 50 47.3 95 58-124 1,2-Dibromoethane (EDB) ug/L 50 50.0 100 71-134 1,2-Dichlorobenzene ug/L 50 55.6 111 70-135 1,2-Dichloroethane ug/L 50 49.6 99 72-129 1,2-Dichloropropane ug/L 50 54.5 109 64-135 1,4-Dichlorobenzene ug/L 50 52.8 106 70-131 2-Butanone (MEK) ug/L 100 96.2J 96 52-143 2-Hexanone ug/L 100 86.8 87 61-136 4-Methyl-2-pentanone (MIBK) ug/L 100 93.2J 93 71-129 Acetone ug/L 100 77.3J 77 48-224 Acrylonitrile ug/L 200 168J 84 66-154 Benzene ug/L 50 54.9 110 68-132 Bromochloromethane ug/L 50 61.0 122 73-133 Bromodichloromethane ug/L 50 47.4 95 67-121 Bromoform ug/L 50 47.6 95 57-125 Bromomethane ug/L 50 46.9 94 35-156 Carbon disulfide ug/L 100 96.8J 97 47-141 Carbon tetrachloride ug/L 50 57.5 115 66-122 Chlorobenzene ug/L 50 52.3 105 71-126 Chloroethane ug/L 50 44.3 89 43-143 Chloroform ug/L 50 54.2 108 71-136 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 95 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 LABORATORY CONTROL SAMPLE: 68330 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloromethane ug/L 50 42.9 86 47-123 cis-1,2-Dichloroethene ug/L 50 57.6 115 74-131 cis-1,3-Dichloropropene ug/L 50 48.3 97 78-120 Dibromochloromethane ug/L 50 46.9 94 65-115 Dibromomethane ug/L 50 57.7 115 79-129 Ethylbenzene ug/L 50 52.8 106 68-129 lodomethane ug/L 100 94.1 94 49-154 Methylene Chloride ug/L 50 49.4 99 61-147 Styrene ug/L 50 51.1 102 77-128 Tetrachloroethene ug/L 50 49.3 99 51-139 Toluene ug/L 50 51.7 103 60-133 trans-1,2-Dichloroethene ug/L 50 50.2 100 69-144 trans- 1,3-Dichloropropene ug/L 50 46.9 94 74-128 trans-1,4-Dichloro-2-butene ug/L 100 90.91 91 61-139 Trichloroethene ug/L 50 53.9 108 73-126 Trichlorofluoromethane ug/L 50 45.1 90 55-132 Vinyl acetate ug/L 50 53.7 107 52-141 Vinyl chloride ug/L 50 45.8 92 50-133 Xylene (Total) ug/L 150 159 106 78-132 1,2-Dichloroethane-d4 (S) %. 95 81-119 4-Bromofluorobenzene (S) %. 101 82-120 Dibromofluoromethane (S) %. 104 82-114 Toluene-d8 (S) %. 96 82-109 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 68331 68332 MS MSD 2610339001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 50 50 51.3 52.0 103 104 68-137 1 11 1,1,1-Trichloroethane ug/L ND 50 50 59.8 58.1 120 116 66-142 3 11 1,1,2,2-Tetrachloroethane ug/L ND 50 50 55.0 55.5 110 111 39-171 1 13 1,1,2-Trichloroethane ug/L ND 50 50 55.4 55.8 111 112 73-136 1 12 1,1-Dichloroethane ug/L ND 50 50 58.2 57.6 116 115 66-155 1 15 1,1-Dichloroethene ug/L ND 50 50 48.4 50.6 97 101 33-181 5 34 1,2,3-Trichloropropane ug/L ND 50 50 45.1 47.1 90 94 78-133 4 14 1,2-Dibromo-3- ug/L ND 50 50 46.7 50.0 93 100 58-124 7 15 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 50 50 54.0 52.7 108 105 71-134 2 12 1,2-Dichlorobenzene ug/L ND 50 50 53.3 52.7 107 105 69-135 1 10 1,2-Dichloroethane ug/L ND 50 50 56.3 56.9 113 114 36-159 1 10 1,2-Dichloropropane ug/L ND 50 50 57.6 56.6 115 113 68-132 2 11 1,4-Dichlorobenzene ug/L ND 50 50 48.9 47.6 98 95 49-153 3 9 2-Butanone (MEK) ug/L ND 100 100 84.5J 85.5J 84 86 10-189 1 23 2-Hexanone ug/L ND 100 100 87.8 86.5 88 86 40-135 2 18 4-Methyl-2-pentanone ug/L ND 100 100 90.2J 91.3J 90 91 30-177 1 10 (MIBK) Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 96 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 68331 68332 MS MSD 2610339001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Acetone ug/L ND 100 100 66.7J 68.OJ 65 67 44-223 2 14 Acrylonitrile ug/L ND 200 200 189J 192J 95 96 13-189 1 12 Benzene ug/L 6.6 50 50 63.0 61.9 113 111 66-139 2 10 Bromochloromethane ug/L ND 50 50 59.2 59.5 118 119 73-133 1 13 Bromodichloromethane ug/L ND 50 50 50.6 49.1 101 98 57-120 3 13 Bromoform ug/L ND 50 50 47.4 50.5 95 101 48-128 6 13 Bromomethane ug/L ND 50 50 49.4 50.4 99 101 10-187 2 32 Carbon disulfide ug/L ND 100 100 91.11 91.6J 91 92 47-141 1 322 Carbon tetrachloride ug/L ND 50 50 58.2 57.4 116 115 58-127 1 14 Chlorobenzene ug/L ND 50 50 51.9 51.8 104 104 63-137 0 10 Chloroethane ug/L ND 50 50 44.3 45.7 89 91 52-146 3 16 Chloroform ug/L ND 50 50 56.7 56.0 113 112 74-137 1 9 Chloromethane ug/L ND 50 50 43.5 45.9 87 92 41-127 5 10 cis-1,2-Dichloroethene ug/L ND 50 50 58.6 58.5 117 117 71-138 0 16 cis-1,3-Dichloropropene ug/L ND 50 50 48.1 48.1 96 96 32-145 0 12 Dibromochloromethane ug/L ND 50 50 48.9 48.8 98 98 52-116 0 13 Dibromomethane ug/L ND 50 50 61.1 61.1 122 122 79-129 0 14 Ethylbenzene ug/L ND 50 50 52.6 51.4 105 103 31-174 2 10 lodomethane ug/L ND 100 100 86.1 94.0 86 94 49-154 9 30 Methylene Chloride ug/L ND 50 50 53.5 55.1 107 110 61-146 3 15 Styrene ug/L ND 50 50 51.7 50.3 103 101 77-128 3 14 Tetrachloroethene ug/L 27.5 50 50 75.4 72.0 96 89 36-155 5 14 Toluene ug/L ND 50 50 54.2 52.8 108 105 52-146 3 11 trans-1,2-Dichloroethene ug/L ND 50 50 52.6 52.4 105 105 61-152 0 14 trans-1,3-Dichloropropene ug/L ND 50 50 47.3 46.7 95 93 37-146 1 12 trans-1,4-Dichloro-2-butene ug/L ND 100 100 86.8J 88.OJ 87 88 61-139 1 12 Trichloroethene ug/L 7.3 50 50 57.1 55.8 100 97 61-141 2 12 Trichlorofluoromethane ug/L ND 50 50 49.0 48.7 98 97 51-141 1 13 Vinyl acetate ug/L ND 50 50 51.5 52.7 103 105 52-141 2 14 Vinyl chloride ug/L ND 50 50 43.5 46.2 87 92 22-156 6 26 Xylene (Total) ug/L ND 150 150 159 158 106 105 78-132 1 7 1,2-Dichloroethane-d4 (S) %. 100 98 81-119 4-Bromofluorobenzene (S) %. 99 98 82-120 Dibromofluoromethane (S) %. 106 103 82-114 Toluene-d8 (S) %. 98 96 82-109 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 97 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 QC Batch: 15344 Analysis Method: EPA 8260B QC Batch Method: EPA 8260E Analysis Description: 8260E MSV Associated Lab Samples: 2610107005, 2610107006, 2610107007, 2610107008, 2610107009, 2610107010, 2610107011, 2610107012, 2610107013, 2610107018, 2610107026, 2610107027, 2610107028, 2610107029, 2610107030, 2610107032, 2610107034 METHOD BLANK: 68716 Matrix: Water Associated Lab Samples: 2610107005, 2610107006, 2610107007, 2610107008, 2610107009, 2610107010, 2610107011, 2610107012, 2610107013, 2610107018, 2610107026, 2610107027, 2610107028, 2610107029, 2610107030, 2610107032, 2610107034 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 5.0 0.32 10/13/18 11:41 1,1,1-Trichloroethane ug/L ND 1.0 0.38 10/13/18 11:41 1,1,2,2-Tetrachloroethane ug/L ND 3.0 0.53 10/13/18 11:41 1,1,2-Trichloroethane ug/L ND 1.0 0.59 10/13/18 11:41 1,1-Dichloroethane ug/L ND 5.0 0.41 10/13/18 11:41 1,1-Dichloroethene ug/L ND 5.0 0.72 10/13/18 11:41 1,2,3-Trichloropropane ug/L ND 1.0 0.46 10/13/18 11:41 1,2-Dibromo-3-chloropropane ug/L ND 13.0 0.55 10/13/18 11:41 1,2-Dibromoethane (EDB) ug/L ND 2.0 0.28 10/13/18 11:41 1,2-Dichlorobenzene ug/L ND 5.0 0.49 10/13/18 11:41 1,2-Dichloroethane ug/L ND 1.0 0.67 10/13/18 11:41 1,2-Dichloropropane ug/L ND 1.0 0.60 10/13/18 11:41 1,4-Dichlorobenzene ug/L ND 1.0 0.58 10/13/18 11:41 2-Butanone (MEK) ug/L ND 100 3.2 10/13/18 11:41 2-Hexanone ug/L ND 50.0 0.89 10/13/18 11:41 4-Methyl-2-pentanone (MIBK) ug/L ND 100 0.86 10/13/18 11:41 Acetone ug/L ND 100 8.2 10/13/18 11:41 Acrylonitrile ug/L ND 200 2.5 10/13/18 11:41 Benzene ug/L ND 1.0 0.20 10/13/18 11:41 Bromochloromethane ug/L ND 3.0 0.50 10/13/18 11:41 Bromodichloromethane ug/L ND 1.0 0.36 10/13/18 11:41 Bromoform ug/L ND 3.0 0.55 10/13/18 11:41 Bromomethane ug/L ND 10.0 0.95 10/13/18 11:41 Carbon disulfide ug/L ND 100 0.79 10/13/18 11:41 Carbon tetrachloride ug/L ND 1.0 0.42 10/13/18 11:41 Chlorobenzene ug/L ND 3.0 0.53 10/13/18 11:41 Chloroethane ug/L ND 10.0 0.52 10/13/18 11:41 Chloroform ug/L ND 5.0 0.58 10/13/18 11:41 Chloromethane ug/L ND 1.0 0.38 10/13/18 11:41 cis-1,2-Dichloroethene ug/L ND 5.0 0.66 10/13/18 11:41 cis-1,3-Dichloropropene ug/L ND 1.0 0.22 10/13/18 11:41 Dibromochloromethane ug/L ND 3.0 0.31 10/13/18 11:41 Dibromomethane ug/L ND 10.0 0.62 10/13/18 11:41 Ethylbenzene ug/L ND 1.0 0.45 10/13/18 11:41 lodomethane ug/L ND 10.0 3.1 10/13/18 11:41 Methylene Chloride ug/L ND 1.0 0.50 10/13/18 11:41 Styrene ug/L ND 1.0 0.50 10/13/18 11:41 Tetrachloroethene ug/L ND 1.0 0.78 10/13/18 11:41 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 98 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 METHOD BLANK: 68716 Matrix: Water Associated Lab Samples: 2610107005, 2610107006, 2610107007, 2610107008, 2610107009, 2610107010, 2610107011, 2610107012, 2610107013, 2610107018, 2610107026, 2610107027, 2610107028, 2610107029, 2610107030, 2610107032, 2610107034 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Toluene ug/L ND 1.0 0.31 10/13/18 11:41 trans-1,2-Dichloroethene ug/L ND 5.0 0.46 10/13/18 11:41 trans- 1,3-Dichloropropene ug/L ND 1.0 0.30 10/13/18 11:41 trans-1,4-Dichloro-2-butene ug/L ND 100 1.6 10/13/18 11:41 Trichloroethene ug/L 0.74J 1.0 0.34 10/13/18 11:41 Trichlorofluoromethane ug/L ND 1.0 0.51 10/13/18 11:41 Vinyl acetate ug/L ND 50.0 0.42 10/13/18 11:41 Vinyl chloride ug/L ND 1.0 0.60 10/13/18 11:41 Xylene (Total) ug/L ND 5.0 1.5 10/13/18 11:41 1,2-Dichloroethane-d4 (S) %. 112 81-119 10/13/18 11:41 4-Bromofluorobenzene (S) %. 109 82-120 10/13/18 11:41 Dibromofluoromethane (S) %. 100 82-114 10/13/18 11:41 Toluene-d8 (S) %. 108 82-109 10/13/18 11:41 LABORATORY CONTROL SAMPLE: 68717 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 48.4 97 68-137 1,1,1-Trichloroethane ug/L 50 51.4 103 72-134 1,1,2,2-Tetrachloroethane ug/L 50 55.5 111 51-158 1,1,2-Trichloroethane ug/L 50 59.1 118 78-131 1,1-Dichloroethane ug/L 50 57.0 114 69-151 1,1-Dichloroethene ug/L 50 64.2 128 64-158 1,2,3-Trichloropropane ug/L 50 41.9 84 78-133 1,2-Dibromo-3-chloropropane ug/L 50 39.7 79 58-124 1,2-Dibromoethane (EDB) ug/L 50 53.2 106 71-134 1,2-Dichlorobenzene ug/L 50 54.2 108 70-135 1,2-Dichloroethane ug/L 50 54.5 109 72-129 1,2-Dichloropropane ug/L 50 59.4 119 64-135 1,4-Dichlorobenzene ug/L 50 54.6 109 70-131 2-Butanone (MEK) ug/L 100 120 120 52-143 2-Hexanone ug/L 100 86.4 86 61-136 4-Methyl-2-pentanone (MIBK) ug/L 100 88.6J 89 71-129 Acetone ug/L 100 154 154 48-224 Acrylonitrile ug/L 200 216 108 66-154 Benzene ug/L 50 56.2 112 68-132 Bromochloromethane ug/L 50 57.2 114 73-133 Bromodichloromethane ug/L 50 49.7 99 67-121 Bromoform ug/L 50 37.4 75 57-125 Bromomethane ug/L 50 55.5 111 35-156 Carbon disulfide ug/L 100 112 112 47-141 Carbon tetrachloride ug/L 50 57.0 114 66-122 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 99 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 LABORATORY CONTROL SAMPLE: 68717 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chlorobenzene ug/L 50 54.5 109 71-126 Chloroethane ug/L 50 64.1 128 43-143 Chloroform ug/L 50 58.2 116 71-136 Chloromethane ug/L 50 54.3 109 47-123 cis-1,2-Dichloroethene ug/L 50 59.7 119 74-131 cis-1,3-Dichloropropene ug/L 50 52.2 104 78-120 Dibromochloromethane ug/L 50 44.9 90 65-115 Dibromomethane ug/L 50 52.1 104 79-129 Ethylbenzene ug/L 50 56.2 112 68-129 lodomethane ug/L 100 92.4 92 49-154 Methylene Chloride ug/L 50 60.8 122 61-147 Styrene ug/L 50 53.8 108 77-128 Tetrachloroethene ug/L 50 40.0 80 51-139 Toluene ug/L 50 55.9 112 60-133 trans-1,2-Dichloroethene ug/L 50 65.5 131 69-144 trans- 1,3-Dichloropropene ug/L 50 48.1 96 74-128 trans-1,4-Dichloro-2-butene ug/L 100 85.5J 86 61-139 Trichloroethene ug/L 50 54.1 108 73-126 Trichlorofluoromethane ug/L 50 60.0 120 55-132 Vinyl acetate ug/L 50 66.3 133 52-141 Vinyl chloride ug/L 50 57.2 114 50-133 Xylene (Total) ug/L 150 177 118 78-132 1,2-Dichloroethane-d4 (S) %. 109 81-119 4-Bromofluorobenzene (S) %. 103 82-120 Dibromofluoromethane (S) %. 109 82-114 Toluene-d8 (S) %. 108 82-109 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 68718 68719 MS MSD 2610107007 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 50 50 38.2 49.2 76 98 68-137 25 11 R1 1,1,1-Trichloroethane ug/L ND 50 50 45.8 58.3 92 117 66-142 24 11 R1 1,1,2,2-Tetrachloroethane ug/L ND 50 50 44.6 54.9 89 110 39-171 21 13 R1 1,1,2-Trichloroethane ug/L ND 50 50 42.8 54.3 86 109 73-136 24 12 R1 1,1-Dichloroethane ug/L ND 50 50 45.2 67.3 90 135 66-155 39 15 R1 1,1-Dichloroethene ug/L ND 50 50 60.6 72.7 121 145 33-181 18 34 1,2,3-Trichloropropane ug/L ND 50 50 38.0 49.0 76 98 78-133 25 14 M1,R1 1,2-Dibromo-3- ug/L ND 50 50 38.4 50.8 77 102 58-124 28 15 R1 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 50 50 42.6 52.8 85 106 71-134 21 12 R1 1,2-Dichlorobenzene ug/L ND 50 50 46.4 56.6 93 113 69-135 20 10 R1 1,2-Dichloroethane ug/L ND 50 50 46.2 55.5 92 111 36-159 18 10 R1 1,2-Dichloropropane ug/L ND 50 50 47.7 60.4 95 121 68-132 24 11 R1 1,4-Dichlorobenzene ug/L ND 50 50 45.5 57.0 91 114 49-153 22 9 R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 100 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 68718 68719 MS MSD 2610107007 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 2-Butanone (MEK) ug/L ND 100 100 75.9J 96.1J 76 96 10-189 23 23 2-Hexanone ug/L ND 100 100 68.5 86.3 69 86 40-135 23 18 R1 4-Methyl-2-pentanone ug/L ND 100 100 76.7J 99.3J 77 99 30-177 26 10 R1 (MIBK) Acetone ug/L ND 100 100 69.2J 84.8J 69 85 44-223 20 14 R1 Acrylonitrile ug/L ND 200 200 196J 238 98 119 13-189 20 12 R1 Benzene ug/L ND 50 50 47.4 59.3 95 119 66-139 22 10 R1 Bromochloromethane ug/L ND 50 50 43.0 51.6 86 103 73-133 18 13 R1 Bromodichloromethane ug/L ND 50 50 38.4 49.2 77 98 57-120 25 13 R1 Bromoform ug/L ND 50 50 29.8 40.1 60 80 48-128 30 13 R1 Bromomethane ug/L ND 50 50 42.0 52.8 84 106 10-187 23 32 Carbon disulfide ug/L ND 100 100 94.OJ 119 94 119 47-141 24 322 Carbon tetrachloride ug/L ND 50 50 51.1 64.3 102 129 58-127 23 14 M1,R1 Chlorobenzene ug/L ND 50 50 45.7 58.2 91 116 63-137 24 10 R1 Chloroethane ug/L ND 50 50 52.0 62.0 104 124 52-146 18 16 R1 Chloroform ug/L ND 50 50 47.2 59.5 94 119 74-137 23 9 R1 Chloromethane ug/L ND 50 50 48.0 56.8 96 114 41-127 17 10 R1 cis-1,2-Dichloroethene ug/L ND 50 50 44.0 54.6 88 109 71-138 22 16 R1 cis-1,3-Dichloropropene ug/L ND 50 50 39.1 50.1 78 100 32-145 25 12 R1 Dibromochloromethane ug/L ND 50 50 34.2 44.4 68 89 52-116 26 13 R1 Dibromomethane ug/L ND 50 50 42.9 53.5 86 107 79-129 22 14 R1 Ethylbenzene ug/L ND 50 50 47.9 60.3 96 121 31-174 23 10 R1 lodomethane ug/L ND 100 100 80.0 116 80 116 49-154 37 30 R1 Methylene Chloride ug/L ND 50 50 51.0 61.7 102 123 61-146 19 15 R1 Styrene ug/L ND 50 50 40.7 51.6 81 103 77-128 24 14 R1 Tetrachloroethene ug/L ND 50 50 33.1 41.3 66 83 36-155 22 14 R1 Toluene ug/L ND 50 50 47.7 60.5 95 121 52-146 24 11 R1 trans-1,2-Dichloroethene ug/L ND 50 50 53.8 65.9 108 132 61-152 20 14 R1 trans-1,3-Dichloropropene ug/L ND 50 50 36.1 46.5 72 93 37-146 25 12 R1 trans-1,4-Dichloro-2-butene ug/L ND 100 100 74.3J 95.3J 74 95 61-139 25 12 R1 Trichloroethene ug/L ND 50 50 44.3 55.9 88 111 61-141 23 12 R1 Trichlorofluoromethane ug/L ND 50 50 58.8 70.7 118 141 51-141 18 13 R1 Vinyl acetate ug/L ND 50 50 38.1J 61.6 76 123 52-141 47 14 R1 Vinyl chloride ug/L ND 50 50 53.9 64.9 108 130 22-156 18 26 Xylene (Total) ug/L ND 150 150 149 188 100 126 78-132 23 7 RS 1,2-Dichloroethane-d4 (S) %. 105 104 81-119 4-Bromofluorobenzene (S) %. 100 98 82-120 Dibromofluoromethane (S) %. 106 108 82-114 Toluene-d8 (S) %. 104 105 82-109 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 101 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 QC Batch: 15378 Analysis Method: EPA 8260B QC Batch Method: EPA 8260E Analysis Description: 8260E MSV Associated Lab Samples: 2610107015, 2610107016, 2610107020, 2610107025, 2610107035, 2610107036, 2610107037, 2610107038 METHOD BLANK: 68815 Matrix: Water Associated Lab Samples: 2610107015, 2610107016, 2610107020, 2610107025, 2610107035, 2610107036, 2610107037, 2610107038 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 5.0 0.32 10/15/18 11:12 1,1,1-Trichloroethane ug/L ND 1.0 0.38 10/15/18 11:12 1,1,2,2-Tetrachloroethane ug/L ND 3.0 0.53 10/15/18 11:12 1,1,2-Trichloroethane ug/L ND 1.0 0.59 10/15/18 11:12 1,1-Dichloroethane ug/L ND 5.0 0.41 10/15/18 11:12 1,1-Dichloroethene ug/L ND 5.0 0.72 10/15/18 11:12 1,2,3-Trichloropropane ug/L ND 1.0 0.46 10/15/18 11:12 1,2-Dibromo-3-chloropropane ug/L ND 13.0 0.55 10/15/18 11:12 1,2-Dibromoethane (EDB) ug/L ND 2.0 0.28 10/15/18 11:12 1,2-Dichlorobenzene ug/L ND 5.0 0.49 10/15/18 11:12 1,2-Dichloroethane ug/L ND 1.0 0.67 10/15/18 11:12 1,2-Dichloropropane ug/L ND 1.0 0.60 10/15/18 11:12 1,4-Dichlorobenzene ug/L ND 1.0 0.58 10/15/18 11:12 2-Butanone (MEK) ug/L ND 100 3.2 10/15/18 11:12 2-Hexanone ug/L ND 50.0 0.89 10/15/18 11:12 4-Methyl-2-pentanone (MIBK) ug/L ND 100 0.86 10/15/18 11:12 Acetone ug/L ND 100 8.2 10/15/18 11:12 Acrylonitrile ug/L ND 200 2.5 10/15/18 11:12 Benzene ug/L ND 1.0 0.20 10/15/18 11:12 Bromochloromethane ug/L ND 3.0 0.50 10/15/18 11:12 Bromodichloromethane ug/L ND 1.0 0.36 10/15/18 11:12 Bromoform ug/L ND 3.0 0.55 10/15/18 11:12 Bromomethane ug/L ND 10.0 0.95 10/15/18 11:12 Carbon disulfide ug/L ND 100 0.79 10/15/18 11:12 Carbon tetrachloride ug/L ND 1.0 0.42 10/15/18 11:12 Chlorobenzene ug/L ND 3.0 0.53 10/15/18 11:12 Chloroethane ug/L ND 10.0 0.52 10/15/18 11:12 Chloroform ug/L ND 5.0 0.58 10/15/18 11:12 Chloromethane ug/L ND 1.0 0.38 10/15/18 11:12 cis-1,2-Dichloroethene ug/L ND 5.0 0.66 10/15/18 11:12 cis-1,3-Dichloropropene ug/L ND 1.0 0.22 10/15/18 11:12 Dibromochloromethane ug/L ND 3.0 0.31 10/15/18 11:12 Dibromomethane ug/L ND 10.0 0.62 10/15/18 11:12 Ethylbenzene ug/L ND 1.0 0.45 10/15/18 11:12 lodomethane ug/L ND 10.0 3.1 10/15/18 11:12 Methylene Chloride ug/L ND 1.0 0.50 10/15/18 11:12 Styrene ug/L ND 1.0 0.50 10/15/18 11:12 Tetrachloroethene ug/L 1.1 1.0 0.78 10/15/18 11:12 Toluene ug/L ND 1.0 0.31 10/15/18 11:12 trans-1,2-Dichloroethene ug/L ND 5.0 0.46 10/15/18 11:12 trans- 1,3-Dichloropropene ug/L ND 1.0 0.30 10/15/18 11:12 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 102 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 METHOD BLANK: 68815 Matrix: Water Associated Lab Samples: 2610107015, 2610107016, 2610107020, 2610107025, 2610107035, 2610107036, 2610107037, 2610107038 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers trans-1,4-Dichloro-2-butene ug/L ND 100 1.6 10/15/18 11:12 Trichloroethene ug/L ND 1.0 0.34 10/15/18 11:12 Trichlorofluoromethane ug/L ND 1.0 0.51 10/15/18 11:12 Vinyl acetate ug/L ND 50.0 0.42 10/15/18 11:12 Vinyl chloride ug/L ND 1.0 0.60 10/15/18 11:12 Xylene (Total) ug/L ND 5.0 1.5 10/15/18 11:12 1,2-Dichloroethane-d4 (S) %. 98 81-119 10/15/18 11:12 4-Bromofluorobenzene (S) %. 105 82-120 10/15/18 11:12 Dibromofluoromethane (S) %. 103 82-114 10/15/18 11:12 Toluene-d8 (S) %. 96 82-109 10/15/18 11:12 LABORATORY CONTROL SAMPLE: Parameter 68816 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 44.6 89 68-137 1,1,1-Trichloroethane ug/L 50 47.8 96 72-134 1,1,2,2-Tetrachloroethane ug/L 50 52.7 105 51-158 1,1,2-Trichloroethane ug/L 50 47.1 94 78-131 1,1-Dichloroethane ug/L 50 49.3 99 69-151 1,1-Dichloroethene ug/L 50 47.4 95 64-158 1,2,3-Trichloropropane ug/L 50 47.3 95 78-133 1,2-Dibromo-3-chloropropane ug/L 50 51.2 102 58-124 1,2-Dibromoethane (EDB) ug/L 50 46.9 94 71-134 1,2-Dichlorobenzene ug/L 50 54.3 109 70-135 1,2-Dichloroethane ug/L 50 54.1 108 72-129 1,2-Dichloropropane ug/L 50 49.8 100 64-135 1,4-Dichlorobenzene ug/L 50 49.8 100 70-131 2-Butanone (MEK) ug/L 100 83.OJ 83 52-143 2-Hexanone ug/L 100 80.0 80 61-136 4-Methyl-2-pentanone (MIBK) ug/L 100 81.6J 82 71-129 Acetone ug/L 100 72.2J 72 48-224 Acrylonitrile ug/L 200 177J 88 66-154 Benzene ug/L 50 51.9 104 68-132 Bromochloromethane ug/L 50 48.7 97 73-133 Bromodichloromethane ug/L 50 45.0 90 67-121 Bromoform ug/L 50 45.3 91 57-125 Bromomethane ug/L 50 41.0 82 35-156 Carbon disulfide ug/L 100 79.2J 79 47-141 Carbon tetrachloride ug/L 50 48.2 96 66-122 Chlorobenzene ug/L 50 50.7 101 71-126 Chloroethane ug/L 50 39.6 79 43-143 Chloroform ug/L 50 50.2 100 71-136 Chloromethane ug/L 50 43.9 88 47-123 cis-1,2-Dichloroethene ug/L 50 51.8 104 74-131 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 103 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 LABORATORY CONTROL SAMPLE: 68816 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers cis-1,3-Dichloropropene ug/L 50 45.0 90 78-120 Dibromochloromethane ug/L 50 44.7 89 65-115 Dibromomethane ug/L 50 49.9 100 79-129 Ethylbenzene ug/L 50 50.1 100 68-129 lodomethane ug/L 100 73.0 73 49-154 Methylene Chloride ug/L 50 44.6 89 61-147 Styrene ug/L 50 48.0 96 77-128 Tetrachloroethene ug/L 50 35.7 71 51-139 Toluene ug/L 50 52.2 104 60-133 trans-1,2-Dichloroethene ug/L 50 45.9 92 69-144 trans- 1,3-Dichloropropene ug/L 50 40.3 81 74-128 trans-1,4-Dichloro-2-butene ug/L 100 95.1J 95 61-139 Trichloroethene ug/L 50 51.9 104 73-126 Trichlorofluoromethane ug/L 50 50.0 100 55-132 Vinyl acetate ug/L 50 63.7 127 52-141 Vinyl chloride ug/L 50 46.8 94 50-133 Xylene (Total) ug/L 150 142 95 78-132 1,2-Dichloroethane-d4 (S) %. 105 81-119 4-Bromofluorobenzene (S) %. 99 82-120 Dibromofluoromethane (S) %. 108 82-114 Toluene-d8 (S) %. 96 82-109 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 68817 68818 MS MSD 2610241001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 50 50 45.0 44.6 90 89 68-137 1 11 1,1,1-Trichloroethane ug/L ND 50 50 52.9 57.4 106 115 66-142 8 11 1,1,2,2-Tetrachloroethane ug/L ND 50 50 51.8 52.3 104 105 39-171 1 13 1,1,2-Trichloroethane ug/L ND 50 50 46.1 38.4 92 77 73-136 18 12 R1 1,1-Dichloroethane ug/L ND 50 50 50.6 49.5 101 99 66-155 2 15 1,1-Dichloroethene ug/L ND 50 50 54.2 44.2 108 88 33-181 20 34 1,2,3-Trichloropropane ug/L ND 50 50 46.2 45.7 92 91 78-133 1 14 1,2-Dibromo-3- ug/L ND 50 50 48.3 48.7 97 97 58-124 1 15 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 50 50 46.8 40.0 94 80 71-134 16 12 R1 1,2-Dichlorobenzene ug/L ND 50 50 52.2 53.4 104 107 69-135 2 10 1,2-Dichloroethane ug/L ND 50 50 53.6 52.0 107 104 36-159 3 10 1,2-Dichloropropane ug/L ND 50 50 48.4 44.0 97 88 68-132 9 11 1,4-Dichlorobenzene ug/L ND 50 50 47.0 48.0 94 96 49-153 2 9 2-Butanone (MEK) ug/L 5AJ 100 100 86.1J 68.8J 81 63 10-189 22 23 2-Hexanone ug/L ND 100 100 80.6 67.7 81 68 40-135 17 18 4-Methyl-2-pentanone ug/L ND 100 100 80.7J 68.8J 81 69 30-177 16 10 R1 (MIBK) Acetone ug/L ND 100 100 70.5J 59.5J 66 55 44-223 17 14 R1 Acrylonitrile ug/L ND 200 200 174J 146J 87 73 13-189 18 12 R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 104 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 68817 68818 MS MSD 2610241001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Benzene ug/L ND 50 50 52.6 49.6 105 99 66-139 6 10 Bromochloromethane ug/L ND 50 50 47.5 53.7 95 107 73-133 12 13 Bromodichloromethane ug/L ND 50 50 44.5 36.8 89 74 57-120 19 13 R1 Bromoform ug/L ND 50 50 42.7 43.0 85 86 48-128 1 13 Bromomethane ug/L ND 50 50 40.9 36.1 82 72 10-187 13 32 Carbon disulfide ug/L ND 100 100 82AJ 70.OJ 82 70 47-141 16 322 Carbon tetrachloride ug/L ND 50 50 56.0 58.7 112 117 58-127 5 14 Chlorobenzene ug/L ND 50 50 49.5 50.0 99 100 63-137 1 10 Chloroethane ug/L ND 50 50 42.9 36.2 86 72 52-146 17 16 R1 Chloroform ug/L ND 50 50 51.0 52.8 102 106 74-137 3 9 Chloromethane ug/L ND 50 50 43.3 35.8 87 72 41-127 19 10 R1 cis-1,2-Dichloroethene ug/L ND 50 50 55.2 55.9 110 112 71-138 1 16 cis-1,3-Dichloropropene ug/L ND 50 50 42.7 36.2 85 72 32-145 17 12 R1 Dibromochloromethane ug/L ND 50 50 42.7 36.8 85 74 52-116 15 13 R1 Dibromomethane ug/L ND 50 50 48.4 39.9 97 80 79-129 19 14 R1 Ethylbenzene ug/L ND 50 50 50.4 51.4 101 103 31-174 2 10 lodomethane ug/L ND 100 100 81.0 67.2 81 67 49-154 19 30 Methylene Chloride ug/L ND 50 50 44.1 36.5 88 73 61-146 19 15 R1 Styrene ug/L ND 50 50 46.5 48.2 93 96 77-128 4 14 Tetrachloroethene ug/L ND 50 50 38.5 30.5 75 60 36-155 23 14 R1 Toluene ug/L ND 50 50 53.2 43.3 106 87 52-146 21 11 R1 trans-1,2-Dichloroethene ug/L ND 50 50 47.7 38.6 95 77 61-152 21 14 R1 trans-1,3-Dichloropropene ug/L ND 50 50 38.3 33.5 77 67 37-146 14 12 R1 trans-1,4-Dichloro-2-butene ug/L ND 100 100 94.OJ 92.1J 94 92 61-139 2 12 Trichloroethene ug/L ND 50 50 50.9 51.6 102 103 61-141 1 12 Trichlorofluoromethane ug/L ND 50 50 64.9 52.3 130 105 51-141 21 13 R1 Vinyl acetate ug/L ND 50 50 59.3 55.9 119 112 52-141 6 14 Vinyl chloride ug/L ND 50 50 50.7 40.9 101 82 22-156 22 26 Xylene (Total) ug/L ND 150 150 140 140 93 94 78-132 0 7 1,2-Dichloroethane-d4 (S) %. 105 102 81-119 4-Bromofluorobenzene (S) %. 95 92 82-120 Dibromofluoromethane (S) %. 109 115 82-114 SO Toluene-d8 (S) %. 95 95 82-109 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 105 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 QC Batch: 15440 Analysis Method: EPA 8260B QC Batch Method: EPA 8260E Analysis Description: 8260E MSV Associated Lab Samples: 2610107014, 2610107019, 2610107024 METHOD BLANK: 69052 Matrix: Associated Lab Samples: 2610107014, 2610107019, 2610107024 Blank Parameter Units Result Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 0.32 10/16/18 16:30 1,1,1-Trichloroethane ug/L ND 1.0 0.38 10/16/18 16:30 1,1,2,2-Tetrachloroethane ug/L ND 3.0 0.53 10/16/18 16:30 1,1,2-Trichloroethane ug/L ND 1.0 0.59 10/16/18 16:30 1,1-Dichloroethane ug/L ND 5.0 0.41 10/16/18 16:30 1,1-Dichloroethene ug/L ND 5.0 0.72 10/16/18 16:30 1,2,3-Trichloropropane ug/L ND 1.0 0.46 10/16/18 16:30 1,2-Dibromo-3-chloropropane ug/L ND 13.0 0.55 10/16/18 16:30 1,2-Dibromoethane (EDB) ug/L ND 2.0 0.28 10/16/18 16:30 1,2-Dichlorobenzene ug/L ND 5.0 0.49 10/16/18 16:30 1,2-Dichloroethane ug/L ND 1.0 0.67 10/16/18 16:30 1,2-Dichloropropane ug/L ND 1.0 0.60 10/16/18 16:30 1,4-Dichlorobenzene ug/L ND 1.0 0.58 10/16/18 16:30 2-Butanone (MEK) ug/L ND 100 3.2 10/16/18 16:30 2-Hexanone ug/L ND 50.0 0.89 10/16/18 16:30 4-Methyl-2-pentanone (MIBK) ug/L ND 100 0.86 10/16/18 16:30 Acetone ug/L ND 100 8.2 10/16/18 16:30 Acrylonitrile ug/L ND 200 2.5 10/16/18 16:30 Benzene ug/L ND 1.0 0.20 10/16/18 16:30 Bromochloromethane ug/L ND 3.0 0.50 10/16/18 16:30 Bromodichloromethane ug/L ND 1.0 0.36 10/16/18 16:30 Bromoform ug/L ND 3.0 0.55 10/16/18 16:30 Bromomethane ug/L ND 10.0 0.95 10/16/18 16:30 Carbon disulfide ug/L ND 100 0.79 10/16/18 16:30 Carbon tetrachloride ug/L ND 1.0 0.42 10/16/18 16:30 Chlorobenzene ug/L ND 3.0 0.53 10/16/18 16:30 Chloroethane ug/L ND 10.0 0.52 10/16/18 16:30 Chloroform ug/L ND 5.0 0.58 10/16/18 16:30 Chloromethane ug/L ND 1.0 0.38 10/16/18 16:30 cis-1,2-Dichloroethene ug/L ND 5.0 0.66 10/16/18 16:30 cis-1,3-Dichloropropene ug/L ND 1.0 0.22 10/16/18 16:30 Dibromochloromethane ug/L ND 3.0 0.31 10/16/18 16:30 Dibromomethane ug/L ND 10.0 0.62 10/16/18 16:30 Ethylbenzene ug/L ND 1.0 0.45 10/16/18 16:30 lodomethane ug/L ND 10.0 3.1 10/16/18 16:30 Methylene Chloride ug/L ND 1.0 0.50 10/16/18 16:30 Styrene ug/L ND 1.0 0.50 10/16/18 16:30 Tetrachloroethene ug/L ND 1.0 0.78 10/16/18 16:30 Toluene ug/L ND 1.0 0.31 10/16/18 16:30 trans-1,2-Dichloroethene ug/L ND 5.0 0.46 10/16/18 16:30 trans- 1,3-Dichloropropene ug/L ND 1.0 0.30 10/16/18 16:30 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 106 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 METHOD BLANK: 69052 Associated Lab Samples: Parameter Matrix: 2610107014, 2610107019, 2610107024 Blank Units Result Water Reporting Limit MDL Analyzed trans-1,4-Dichloro-2-butene ug/L ND 100 1.6 10/16/18 16:30 Trichloroethene ug/L ND 1.0 0.34 10/16/18 16:30 Trichlorofluoromethane ug/L ND 1.0 0.51 10/16/18 16:30 Vinyl acetate ug/L ND 50.0 0.42 10/16/18 16:30 Vinyl chloride ug/L ND 1.0 0.60 10/16/18 16:30 Xylene (Total) ug/L ND 5.0 1.5 10/16/18 16:30 1,2-Dichloroethane-d4 (S) %. 98 81-119 10/16/18 16:30 4-Bromofluorobenzene (S) %. 102 82-120 10/16/18 16:30 Dibromofluoromethane (S) %. 99 82-114 10/16/18 16:30 Toluene-d8 (S) %. 94 82-109 10/16/18 16:30 LABORATORY CONTROL SAMPLE: Parameter 69053 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 49.7 99 68-137 1,1,1-Trichloroethane ug/L 50 58.8 118 72-134 1,1,2,2-Tetrachloroethane ug/L 50 51.5 103 51-158 1,1,2-Trichloroethane ug/L 50 49.3 99 78-131 1,1-Dichloroethane ug/L 50 50.1 100 69-151 1,1-Dichloroethene ug/L 50 44.8 90 64-158 1,2,3-Trichloropropane ug/L 50 45.5 91 78-133 1,2-Dibromo-3-chloropropane ug/L 50 45.5 91 58-124 1,2-Dibromoethane (EDB) ug/L 50 49.9 100 71-134 1,2-Dichlorobenzene ug/L 50 51.8 104 70-135 1,2-Dichloroethane ug/L 50 50.6 101 72-129 1,2-Dichloropropane ug/L 50 52.5 105 64-135 1,4-Dichlorobenzene ug/L 50 49.1 98 70-131 2-Butanone (MEK) ug/L 100 90.2J 90 52-143 2-Hexanone ug/L 100 85.0 85 61-136 4-Methyl-2-pentanone (MIBK) ug/L 100 90.2J 90 71-129 Acetone ug/L 100 71.2J 71 48-224 Acrylonitrile ug/L 200 166J 83 66-154 Benzene ug/L 50 53.8 108 68-132 Bromochloromethane ug/L 50 58.9 118 73-133 Bromodichloromethane ug/L 50 46.5 93 67-121 Bromoform ug/L 50 47.2 94 57-125 Bromomethane ug/L 50 44.7 89 35-156 Carbon disulfide ug/L 100 88.5J 89 47-141 Carbon tetrachloride ug/L 50 56.2 112 66-122 Chlorobenzene ug/L 50 49.1 98 71-126 Chloroethane ug/L 50 43.9 88 43-143 Chloroform ug/L 50 53.7 107 71-136 Chloromethane ug/L 50 44.0 88 47-123 cis-1,2-Dichloroethene ug/L 50 56.3 113 74-131 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 107 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 LABORATORY CONTROL SAMPLE: 69053 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers cis-1,3-Dichloropropene ug/L 50 46.8 94 78-120 Dibromochloromethane ug/L 50 47.0 94 65-115 Dibromomethane ug/L 50 57.3 115 79-129 Ethylbenzene ug/L 50 49.4 99 68-129 lodomethane ug/L 100 90.2 90 49-154 Methylene Chloride ug/L 50 47.9 96 61-147 Styrene ug/L 50 47.6 95 77-128 Tetrachloroethene ug/L 50 51.1 102 51-139 Toluene ug/L 50 50.0 100 60-133 trans-1,2-Dichloroethene ug/L 50 49.1 98 69-144 trans- 1,3-Dichloropropene ug/L 50 45.3 91 74-128 trans-1,4-Dichloro-2-butene ug/L 100 88.1J 88 61-139 Trichloroethene ug/L 50 51.6 103 73-126 Trichlorofluoromethane ug/L 50 45.6 91 55-132 Vinyl acetate ug/L 50 50.9 102 52-141 Vinyl chloride ug/L 50 45.8 92 50-133 Xylene (Total) ug/L 150 149 99 78-132 1,2-Dichloroethane-d4 (S) %. 97 81-119 4-Bromofluorobenzene (S) %. 102 82-120 Dibromofluoromethane (S) %. 104 82-114 Toluene-d8 (S) %. 96 82-109 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 69054 69055 MS MSD 2610107019 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 50 50 50.0 49.4 100 99 68-137 1 11 1,1,1-Trichloroethane ug/L ND 50 50 59.3 59.8 119 120 66-142 1 11 1,1,2,2-Tetrachloroethane ug/L ND 50 50 52.9 54.0 106 108 39-171 2 13 1,1,2-Trichloroethane ug/L ND 50 50 54.2 54.5 108 109 73-136 0 12 1,1-Dichloroethane ug/L 2.1J 50 50 54.7 56.7 105 109 66-155 4 15 1,1-Dichloroethene ug/L ND 50 50 45.8 47.0 92 94 33-181 2 34 1,2,3-Trichloropropane ug/L ND 50 50 45.8 46.2 92 92 78-133 1 14 1,2-Dibromo-3- ug/L ND 50 50 47.9 48.6 96 97 58-124 1 15 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 50 50 53.0 53.9 106 108 71-134 2 12 1,2-Dichlorobenzene ug/L ND 50 50 51.6 53.6 103 107 69-135 4 10 1,2-Dichloroethane ug/L ND 50 50 55.3 55.9 111 112 36-159 1 10 1,2-Dichloropropane ug/L ND 50 50 54.3 56.3 108 112 68-132 3 11 1,4-Dichlorobenzene ug/L 2.8 50 50 50.9 51.3 96 97 49-153 1 9 2-Butanone (MEK) ug/L ND 100 100 83.6J 82.1J 84 82 10-189 2 23 2-Hexanone ug/L ND 100 100 79.7 81.5 80 81 40-135 2 18 4-Methyl-2-pentanone ug/L ND 100 100 87.9J 92.1J 88 92 30-177 5 10 (MIBK) Acetone ug/L ND 100 100 53.6J 54.OJ 54 54 44-223 1 14 Acrylonitrile ug/L ND 200 200 168J 167J 84 84 13-189 0 12 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 108 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 69054 69055 MS MSD 2610107019 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Benzene ug/L 0.25J 50 50 54.9 54.5 109 109 66-139 1 10 Bromochloromethane ug/L ND 50 50 58.8 60.0 118 120 73-133 2 13 Bromodichloromethane ug/L ND 50 50 49.8 50.1 100 100 57-120 1 13 Bromoform ug/L ND 50 50 48.8 49.4 98 99 48-128 1 13 Bromomethane ug/L ND 50 50 42.4 42.2 85 84 10-187 0 32 Carbon disulfide ug/L ND 100 100 84.6J 84AJ 85 84 47-141 0 322 Carbon tetrachloride ug/L ND 50 50 56.2 56.4 112 113 58-127 0 14 Chlorobenzene ug/L ND 50 50 51.4 50.9 103 102 63-137 1 10 Chloroethane ug/L ND 50 50 40.0 39.9 80 80 52-146 0 16 Chloroform ug/L ND 50 50 55.0 54.8 110 110 74-137 0 9 Chloromethane ug/L ND 50 50 40.0 39.4 80 79 41-127 1 10 cis-1,2-Dichloroethene ug/L ND 50 50 62.6 62.2 125 124 71-138 1 16 cis-1,3-Dichloropropene ug/L ND 50 50 47.8 48.5 96 97 32-145 1 12 Dibromochloromethane ug/L ND 50 50 48.3 50.3 97 101 52-116 4 13 Dibromomethane ug/L ND 50 50 62.1 62.7 124 125 79-129 1 14 Ethylbenzene ug/L ND 50 50 50.1 49.9 100 100 31-174 0 10 lodomethane ug/L ND 100 100 86.8 90.0 87 90 49-154 4 30 Methylene Chloride ug/L ND 50 50 49.5 50.3 99 101 61-146 2 15 Styrene ug/L ND 50 50 42.6 48.3 85 97 77-128 13 14 Tetrachloroethene ug/L ND 50 50 44.6 45.8 89 92 36-155 3 14 Toluene ug/L ND 50 50 50.8 51.4 101 103 52-146 1 11 trans-1,2-Dichloroethene ug/L ND 50 50 49.2 49.7 98 99 61-152 1 14 trans-1,3-Dichloropropene ug/L ND 50 50 46.6 47.2 93 94 37-146 1 12 trans-1,4-Dichloro-2-butene ug/L ND 100 100 86.1J 85AJ 86 85 61-139 1 12 Trichloroethene ug/L ND 50 50 48.8 50.9 98 102 61-141 4 12 Trichlorofluoromethane ug/L ND 50 50 43.6 43.9 87 88 51-141 1 13 Vinyl acetate ug/L ND 50 50 45AJ 53.4 91 107 52-141 16 14 R1 Vinyl chloride ug/L ND 50 50 40.3 40.7 81 81 22-156 1 26 Xylene (Total) ug/L ND 150 150 153 152 102 101 78-132 1 7 1,2-Dichloroethane-d4 (S) %. 100 97 81-119 4-Bromofluorobenzene (S) %. 101 102 82-120 Dibromofluoromethane (S) %. 107 106 82-114 Toluene-d8 (S) %. 95 94 82-109 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 109 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALIFIERS Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. IW_1.101Ica] NI*i PASI-C Pace Analytical Services - Charlotte PASI-GA Pace Analytical Services - Atlanta, GA ANALYTE QUALIFIERS B Analyte was detected in the associated method blank. H3 Sample was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. N2 The lab does not hold NELAC/TNI accreditation for this parameter. R1 RPD value was outside control limits. RS The RPD value in one of the constituent analytes was outside the control limits. SO Surrogate recovery outside laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 110 of 155 lacmnalytical' www.pacelabs.corn Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 2610107001 1304-MW1A 14870 2610107002 1304-MW1B 14870 2610107003 1304-MW2A 14870 2610107004 1304-MW2B 14870 2610107005 1304-MW10 14870 2610107006 1304-MW10A 14870 2610107007 1304-MW11 14870 2610107008 1304-MW12 14870 2610107009 1304-MW14 14870 2610107010 1304-MW14B 14870 2610107011 1304-MW15 14870 2610107012 1304-MW16 14870 2610107013 1304-MW18A 14870 2610107014 1304-MW19 14870 2610107015 1304-MW19A 14870 2610107016 1304-MW19AR 14870 2610107017 1304-MW19R 14870 2610107018 1304-MW20AR 14870 2610107019 1304-MW20B 14870 2610107020 1304-MW21 14870 2610107021 1304-MW22 14870 2610107022 1304-MW22A 14870 2610107023 1304-MW25 14870 2610107024 1304-MW26 14870 2610107025 1304-MW27 14870 2610107026 1304-MW28 14870 2610107027 1304-MW29R 14870 2610107028 1304-MW30R 14870 2610107029 1304-MW31 14870 2610107030 1304-MW32R 14870 2610107032 1304-MW34 14870 2610107036 1304-SW2 15449 2610107037 1304-SW1 15449 2610107001 1304-MW1A EPA 3005A 15369 EPA 6020B 15409 2610107002 1304-MW1B EPA 3005A 15369 EPA 6020B 15409 2610107003 1304-MW2A EPA 3005A 15369 EPA 6020B 15409 2610107004 1304-MW2B EPA 3005A 15369 EPA 6020B 15409 2610107005 1304-MW10 EPA 3005A 15369 EPA 6020B 15409 2610107006 1304-MW10A EPA 3005A 15369 EPA 6020B 15409 2610107007 1304-MW11 EPA 3005A 15369 EPA 6020B 15409 2610107008 1304-MW12 EPA 3005A 15369 EPA 6020B 15409 2610107009 1304-MW14 EPA 3005A 15369 EPA 6020B 15409 2610107010 1304-MW14B EPA 3005A 15369 EPA 6020B 15409 2610107011 1304-MW15 EPA 3005A 15369 EPA 6020B 15409 2610107012 1304-MW16 EPA 3005A 15369 EPA 6020B 15409 2610107013 1304-MW18A EPA 3005A 15369 EPA 6020B 15409 2610107014 1304-MW19 EPA 3005A 15369 EPA 6020B 15409 2610107015 1304-MW19A EPA 3005A 15369 EPA 6020B 15409 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 111 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 2610107016 1304-MW19AR EPA 3005A 15369 EPA 6020B 15409 2610107017 1304-MW19R EPA 3005A 15369 EPA 6020B 15409 2610107018 1304-MW20AR EPA 3005A 15369 EPA 6020B 15409 2610107019 1304-MW20B EPA 3005A 15369 EPA 6020B 15409 2610107020 1304-MW21 EPA 3005A 15369 EPA 6020B 15409 2610107021 1304-MW22 EPA 3005A 15379 EPA 6020B 15410 2610107022 1304-MW22A EPA 3005A 15379 EPA 6020B 15410 2610107023 1304-MW25 EPA 3005A 15379 EPA 6020B 15410 2610107024 1304-MW26 EPA 3005A 15379 EPA 6020B 15410 2610107025 1304-MW27 EPA 3005A 15379 EPA 6020B 15410 2610107026 1304-MW28 EPA 3005A 15379 EPA 6020B 15410 2610107027 1304-MW29R EPA 3005A 15379 EPA 6020B 15410 2610107028 1304-MW30R EPA 3005A 15379 EPA 6020B 15410 2610107029 1304-MW31 EPA 3005A 15379 EPA 6020B 15410 2610107030 1304-MW32R EPA 3005A 15379 EPA 6020B 15410 2610107032 1304-MW34 EPA 3005A 15379 EPA 6020B 15410 2610107034 1304-Duplicate EPA 3005A 15379 EPA 6020B 15410 2610107035 1304-Equip Blank EPA 3005A 15379 EPA 6020B 15410 2610107036 1304-SW2 EPA 3005A 15379 EPA 6020B 15410 2610107037 1304-SW1 EPA 3005A 15379 EPA 6020B 15410 2610107038 1304-Field Blank EPA 3005A 15379 EPA 6020B 15410 2610107001 1304-MW1A EPA 7470A 15401 EPA 7470A 15434 2610107002 1304-MW1 B EPA 7470A 15401 EPA 7470A 15434 2610107003 1304-MW2A EPA 7470A 15401 EPA 7470A 15434 2610107004 1304-MW2B EPA 7470A 15401 EPA 7470A 15434 2610107005 1304-MW10 EPA 7470A 15401 EPA 7470A 15434 2610107006 1304-MW10A EPA 7470A 15401 EPA 7470A 15434 2610107007 1304-MW11 EPA 7470A 15401 EPA 7470A 15434 2610107008 1304-MW12 EPA 7470A 15401 EPA 7470A 15434 2610107009 1304-MW14 EPA 7470A 15401 EPA 7470A 15434 2610107010 1304-MW14B EPA 7470A 15401 EPA 7470A 15434 2610107011 1304-MW15 EPA 7470A 15401 EPA 7470A 15434 2610107012 1304-MW16 EPA 7470A 15401 EPA 7470A 15434 2610107013 1304-MW18A EPA 7470A 15401 EPA 7470A 15434 2610107014 1304-MW19 EPA 7470A 15401 EPA 7470A 15434 2610107015 1304-MW19A EPA 7470A 15401 EPA 7470A 15434 2610107016 1304-MW19AR EPA 7470A 15401 EPA 7470A 15434 2610107017 1304-MW19R EPA 7470A 15401 EPA 7470A 15434 2610107018 1304-MW20AR EPA 7470A 15401 EPA 7470A 15434 2610107019 1304-MW20B EPA 7470A 15401 EPA 7470A 15434 2610107020 1304-MW21 EPA 7470A 15401 EPA 7470A 15434 2610107021 1304-MW22 EPA 7470A 15402 EPA 7470A 15435 2610107022 1304-MW22A EPA 7470A 15402 EPA 7470A 15435 2610107023 1304-MW25 EPA 7470A 15402 EPA 7470A 15435 2610107024 1304-MW26 EPA 7470A 15402 EPA 7470A 15435 2610107025 1304-MW27 EPA 7470A 15402 EPA 7470A 15435 2610107026 1304-MW28 EPA 7470A 15402 EPA 7470A 15435 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 112 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 2610107027 1304-MW29R EPA 7470A 15402 EPA 7470A 15435 2610107028 1304-MW30R EPA 7470A 15402 EPA 7470A 15435 2610107029 1304-MW31 EPA 7470A 15402 EPA 7470A 15435 2610107030 1304-MW32R EPA 7470A 15402 EPA 7470A 15435 2610107032 1304-MW34 EPA 7470A 15402 EPA 7470A 15435 2610107034 1304-Duplicate EPA 7470A 15402 EPA 7470A 15435 2610107035 1304-Equip Blank EPA 7470A 15402 EPA 7470A 15435 2610107038 1304-Field Blank EPA 7470A 15402 EPA 7470A 15435 2610107001 1304-MW1A EPA 8260B Mod. 435960 2610107002 1304-MW1B EPA 8260B Mod. 435960 2610107003 1304-MW2A EPA 8260B Mod. 435960 2610107004 1304-MW2B EPA 8260B Mod. 435960 2610107005 1304-MW10 EPA 8260B Mod. 435960 2610107006 1304-MW10A EPA 8260B Mod. 435960 2610107007 1304-MW11 EPA 8260B Mod. 435960 2610107008 1304-MW12 EPA 8260B Mod. 435960 2610107009 1304-MW14 EPA 8260B Mod. 435960 2610107010 1304-MW14B EPA 8260B Mod. 436645 2610107011 1304-MW15 EPA 8260B Mod. 435960 2610107012 1304-MW16 EPA 8260B Mod. 435960 2610107013 1304-MW18A EPA 8260B Mod. 435960 2610107014 1304-MW19 EPA 8260B Mod. 436645 2610107015 1304-MW19A EPA 8260B Mod. 436645 2610107016 1304-MW19AR EPA 8260B Mod. 435960 2610107017 1304-MW19R EPA 8260B Mod. 436645 2610107018 1304-MW20AR EPA 8260B Mod. 438946 2610107019 1304-MW20B EPA 8260B Mod. 435960 2610107020 1304-MW21 EPA 8260B Mod. 436645 2610107021 1304-MW22 EPA 8260B Mod. 435960 2610107022 1304-MW22A EPA 8260B Mod. 435960 2610107023 1304-MW25 EPA 8260B Mod. 435960 2610107024 1304-MW26 EPA 8260B Mod. 435961 2610107025 1304-MW27 EPA 8260B Mod. 436645 2610107026 1304-MW28 EPA 8260B Mod. 435961 2610107027 1304-MW29R EPA 8260B Mod. 436230 2610107028 1304-MW30R EPA 8260B Mod. 436230 2610107029 1304-MW31 EPA 8260B Mod. 436230 2610107030 1304-MW32R EPA 8260B Mod. 436230 2610107032 1304-MW34 EPA 8260B Mod. 436230 2610107033 1304-Trip Day 1 EPA 8260B Mod. 435960 2610107034 1304-Duplicate EPA 8260B Mod. 436231 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 113 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 2610107035 1304-Equip Blank EPA 8260B Mod. 436645 2610107036 1304-SW2 EPA 8260B Mod. 436645 2610107037 1304-SW1 EPA 8260B Mod. 436645 2610107038 1304-Field Blank EPA 8260B Mod. 436645 2610107001 1304-MW1A EPA 8260B 15268 2610107002 1304-MW1 B EPA 8260B 15268 2610107003 1304-MW2A EPA 8260B 15268 2610107004 1304-MW2B EPA 8260B 15268 2610107005 1304-MW10 EPA 8260B 15344 2610107006 1304-MW10A EPA 8260B 15344 2610107007 1304-MW11 EPA 8260B 15344 2610107008 1304-MW12 EPA 8260B 15344 2610107009 1304-MW14 EPA 8260B 15344 2610107010 1304-MW14B EPA 8260B 15344 2610107011 1304-MW15 EPA 8260B 15344 2610107012 1304-MW16 EPA 8260B 15344 2610107013 1304-MW18A EPA 8260B 15344 2610107014 1304-MW19 EPA 8260B 15440 2610107015 1304-MW19A EPA 8260B 15378 2610107016 1304-MW19AR EPA 8260B 15378 2610107017 1304-MW19R EPA 8260B 15268 2610107018 1304-MW20AR EPA 8260B 15344 2610107019 1304-MW20B EPA 8260B 15440 2610107020 1304-MW21 EPA 8260B 15378 2610107021 1304-MW22 EPA 8260B 15268 2610107022 1304-MW22A EPA 8260B 15268 2610107023 1304-MW25 EPA 8260B 15268 2610107024 1304-MW26 EPA 8260B 15440 2610107025 1304-MW27 EPA 8260B 15378 2610107026 1304-MW28 EPA 8260B 15344 2610107027 1304-MW29R EPA 8260B 15344 2610107028 1304-MW30R EPA 8260B 15344 2610107029 1304-MW31 EPA 8260B 15344 2610107030 1304-MW32R EPA 8260B 15344 2610107032 1304-MW34 EPA 8260B 15344 2610107033 1304-Trip Day 1 EPA 8260B 15268 2610107034 1304-Duplicate EPA 8260B 15344 2610107035 1304-Equip Blank EPA 8260B 15378 2610107036 1304-SW2 EPA 8260B 15378 2610107037 1304-SW1 EPA 8260B 15378 2610107038 1304-Field Blank EPA 8260B 15378 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 114 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Charlotte Motor Speedway V LF Pace Project No.: 2610107 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /07/2018 04:17 PM without the written consent of Pace Analytical Services, LLC. Page 115 of 155 U) X W z 0 U w w U W a } U� J J N m} U)O 0 O z QW F- a O 0 0 U W } 0 0 V) D U LL 0 W °v N U T o `�go w C.) 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O z w wl + 6H + sle3eW 11 ddy ON m U (elis uo) OO q,nl dwel OS Hd x x w 22 6H + SMIGH I ddV ON M O 5 c) M (1) m m m w W W d DOA I ddy ON r� cn cry co cry ? ? co W .. z z u U O Z I- d— Z W w o co r r r r M m a co # x F z O In U � s y LL Z U m N Z o fib o C o c w �lJ �O r — w ~ w U `v a ui w N J Q >> — rp w f t- a) U d O N ¢ z N t70:¢m x j( X X a U O 2 a W N a � U o Q, X . m Z i p w r Q o ¢ O O U !� 0 c Z g U w Z U 7 (,� F- O ca L W U J a� v tt mo Lu F I to O r- O 00 O 0 1 Z w m t O ¢ m ¢ Z O p N ¢ N ZO W Z F 4k � ao m aD a0 ao Q Q w Z Z ¢i n Z M)' w Q C7 N ci. M J > W W o o -' �W.. a O O Q O O O O O U w U L)) C) w ¢ m a a 1 of 7 5 Sample ... .. Receipt" WO# : 26 10107 FaceAnalytical Client Name: PM: BM Due Date: 10/22/18 CLIENT: Republic -NC Courier: ❑ Fed Ex ❑ UPS ❑ USPS ❑ Client ❑Commercial Pace Other Tracking #: Proj. Due Date: ,,���� Proj. Name: Custody Seal on Cooler/Box Present: yews ❑ no Seals intact:'1 yes ❑ no Packin_q Material: bble uWrap ❑ u� bble Bags ❑ None ❑ Other Thermometer Used Type of Ice: et lue None O Cooler Temperature lE Biological Tissue is Frozen: Ye No Temp should be above freezing to 60C Comments: ❑ Samples on ice, cooli Date and Initial Chain of Custody Present: es ❑No El N/A 1. Chain of Custody Filled Out: es El No El N/A 2. Chain of Custody Relinquished: es ON. El N/A 3. Sampler Name & Signature on COC: e1es ❑No El N/A 4, Samples Arrived within Hold Time: C e� El N/A 5. Short Hold Time Analysis.(<72hr): ❑Yes 2A-.o ❑N/A 6, Rush Turn Around Time Requested: ❑Yes B< ❑N/A 7. Sufficient Volume: Gres ON. El N/A g. Correct Containers Used: -Pace Containers Used: ZY'. S Yes El No ❑No ❑N/A ❑N/A g, Containers Intact: ❑Yes No 11 N/A 10. ©n'L' VO 4-e ,e Filtered volume received for Dissolved tests ❑Yes ❑No EqhNihir 11. Sample Labels match COC: -Includes date/time/ID/Analysis kTatrix: Gres t�'Wz ONo ❑N/A "'Y7 12."i'fIpOal z+-3 Fr -e % A91& nK P.,-,PSeht— We rC no`fi h/1-t—d All containers needing preservation have been checked. _ 4f!'fes ❑No ❑N!A 13 All containers needing preservation are found to be in 1;1�e ONO 11 N/A compliance with EPA recommendation. has begun examining h tce n ,( P S ❑NO Initial when Lot # of added exceptio s: oA oliform, TOC, O&G, WI-DRO (water; completed preservative Samples checked for dechlorination: ❑Yes ❑No I<A 14. Headspace in VOA Vials ( >6mm): ❑Yes o E ❑NSA 15. Trip Blank Present: 2s No ❑WA 16. Trip Blank Custody Seals Present es ❑No ❑N:A , Pace Trip Blank Lot # (if purchased): Client Notification/ Resolution: Field Data Required? Y N Person Contacted: Date/Time. Comments/ Resolution: Project Manager Review: Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( 0 out of hold, incorrect preservative, out of temp. incorrect containers) F-ALLC003rev.3, 11 SepterRi&gfi�ObV of 155 acieAnalytical° October 16, 2018 BFI Waste Systems of North Carolina Mr. Mike Gurley 5105-A Morehead Road, Concord, North Carolina 28027 RE: Charlotte Motor Speedway V Landfill Report 2610107 Mr. Gurley: Pace Analytical Services, Inc. 110 Technology Parkway Peachtree Corners, GA 30092 Pace Analytical completed the semi-annual groundwater and surface water at the referenced site on October 4, 2018. Our representatives performed groundwater monitoring in accordance with the most recently approved U.S. E.P.A. Region 4 Operating Procedures. Presented herein is a description of our work. Phone:770.734.4200 Fax: 770, 734.4201 www.pacelabs.com The following wells were purged and sampled using a dedicated Grundfos pump and Teflon -lined tubing: MW-1A,113, 2A, 213,10,10A,11,12,14,1413,15,16,18A,19,19A, 19AR,19R, 20AR, 2013, 21, 22, 22A, 25, 26, 27, 28, 29R, 30R, 31, 32R, 33, and 34. MW-17,17A, 18R, 18AR, and 24 where water levels only. Surface water points sampled: SW-1 and 2. Water levels and bottom of casing depths were measured to the nearest hundredth of a foot prior to purging the wells. Indicator parameters were measured on site for pH, specific conductance, temperature, dissolved oxygen, and turbidity. All indicator parameter were also measured on surface waters. The meters were calibrated in the field according to the manufacturers' specifications and checked periodically. The water level indicator and instrument probes were decontaminated in the field using a modified version of the EPA Appendix B. All pumps/tubing were decontaminated prior to being brought on site. The samples were collected in A certified -clean bottles as soon as three well volumes had been removed and field parameters stabilized. The bottles were labeled in the field at the time of sampling. The members of the sampling team initialed the labels before placing them on the bottles. New gloves were donned prior to collecting samples. Page 120 of 155 PaceAnalytical� Pace Analytical Services, Inc. 110 Technology Parkway Peachtree Corners, GA 30092 Phone: 770.734.4200 Fax: 770.734.4201 www.pacelabs.com Samples for Appendix I Metals were collected in 250 mL wide -mouth HDPE bottles pre -preserved by the supplier with HNO3. Samples for Appendix I VOC's were collected in three 40 mL vials pre -preserved by the supplier with HCI. Once the bottles were filled they were placed in an ice chest filled with ice to maintain four degrees centigrade. Attached are the results from this sampling event and table listing the water levels recorded. Respectfully submitted, Jonathan Scott Field Services Manager Page 121 of 155 m t a O a Q- W R U cn a a Q a H Q W 0 Z O F- Z 2 LO O N Co N r- O 'd' LO (3) Q N N N N N Q Of CD �>> W C14 O > > N M M ". N CO 00 Q Lf� CU U-) 00 � CO Q N d' LO Cfl I- CO —_ N N N N CN N � CN N d > > •- Il- 00 LO O O N LO CM N M ti M I,- N N N N p �- p - �rnQQOfQmr- 00 > CV N Cep 000 O 00 O 00 00 CO 00 CV r1' r- Q O CA 00 c- c- LO CO N Q V Lfi CD I� Q < Q — 00 O O N M o I- O LO LO Q ti In In N N M M o a c CD o N m c G 5, m .O 3 R Cf- Page 122 of 155 r_. a 4 0 0 ww 4L. z ° a ° L 1 c O '4� �ro U N _ O O U O N W °� F- a cj N co Q p ° Q) 0 C C cco O O U co Q �3cn �F 'b 3 w rrl O M �D M v, U O O k O � II U U Ii ~ tj �' (,� II II E ° c LIUU II o o t"U CLl II A U w w r 3 " E 3 v c E c°04 E o o w E = o = O > p�3U G p > > to 00 cd 3 ! 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En 12 c c 0 7 4 `r U z C7 C7 Qu o a 0 i C - 00 •� �, O cd i•� O _ O U cz U W a�i ?co E ^ E a U 3 En Ll o o� �? p tom`° oo�-� U U 3 Ln w b °' �U, o a� 0 0 O o K k II U U II E p II II fi' II e U U > o a�3 ^5....�w_ Q�3 wo�n�> 3 _ ° •` E E ° VI %, _3U°3 C, O > > O fC 0 ° U M 'C cV U c c^ p p o 3 U U E E =Ik U o 03 a Q `- 3 •� aJ ��w3 Oj m C3 0 0 a-l- c .-r ..V _r 0 b 0 c � � 4 Y ry * U v I O fA -H > Ocz E W C7 U rA U7 • a O N � ° '° O H>3a�3�=o� [CM On Page 154 of 155 ti if 7 o nnO N � C O O O > ca U (U ev Q o o n, O O O G C V � ccz u co U 0 0 � � 3 cn b aq c� V o M U �" 0 0 O O '�' k X it U U II E C w I^ >> UU o �U3 3 to N �5X3�=Gym 0 II o o cd `. II �U 3 o`�noc°n�> c o -4'�wuEE y -=r- E0 c N cH O O ? O > N vi O 3u O > dnen•°3 > C ❑'- M rn G oC O O 0 cd UU cd u > O 8 U -- C7 4-. — — W E �Q moo.... -moo �> +; z a-- s3-c "' 3 y 3 w3 Q3�°oaNItc0 f Z c a l ,a .9 f 1 1V} �q ry ii n O O � C7 U CA p co -- �- 0. > o p N W 0 d G "U 'O � C O u >> A .3�=0� M W m a —M Page 155 of 155 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 October 30, 2018 Environmental Manager BFI Waste Systems of North America. LLC 5105 Moreland Road Concord, NC 28027 RE: Project: CMS V Landfill Pace Project No.: 2610392 Dear Environmental Manager: Enclosed are the analytical results for sample(s) received by the laboratory on October 11, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Betsy McDaniel betsy.mcdaniel@pacelabs.com (770)734-4200 Project Manager Enclosures cc: Database Manager REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 Project: CMS V Landfill Pace Project No.: 2610392 Atlanta Certification IDs 110 Technology Parkway Peachtree Corners, GA 30092 Florida DOH Certification #: E87315 Georgia DW Inorganics Certification #: 812 Georgia DW Microbiology Certification #: 812 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 CERTIFICATIONS North Carolina Certification #: 381 South Carolina Certification #: 98011001 Texas Certification #: T104704397-08-TX Virginia Certification #: 460204 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 SAMPLE SUMMARY Project: CMS V Landfill Pace Project No.: 2610392 Lab ID Sample ID Matrix Date Collected Date Received 2610392001 1304-MW33 Water 10/10/1815:42 10/11/18 13:00 2610392002 1304-MW33 Water 10/11/18 07:28 10/11/18 13:00 2610392003 1304-Trip Blank Water 10/10/18 00:00 10/11/18 13:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 SAMPLE ANALYTE COUNT Project: CMS V Landfill Pace Project No.: 2610392 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 2610392001 1304-MW33 EPA 8081B SFI 22 PASI-GA EPA 8082A SFI 8 PASI-GA EPA 8270D JRS 113 PASI-GA EPA 8260B Mod. DLK 3 PASI-C EPA 8260E LIH, RAC 65 PASI-GA EPA 9014 Cyanide KN 1 PASI-GA EPA 9034 JPT 1 PASI-GA 2610392002 1304-MW33 EPA 6020E CSW 16 PASI-GA EPA 7470A DRB 1 PASI-GA 2610392003 1304-Trip Blank EPA 8260B Mod. DLK 3 PASI-C EPA 8260B LIH 65 PASI-GA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: CMS V Landfill Pace Project No.: 2610392 Sample: 1304-MW33 Lab ID: 2610392001 Collected: 10/10/18 15:42 Received: 10/11/18 13:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Analytical Method Collected By WF 1 10/16/18 10:36 Field pH 5.51 Std. Units 1 10/16/18 10:36 Field Temperature 21.1 deg C 1 10/16/18 10:36 Field Specific 1219 umhos/c 1 10/16/18 10:36 Conductance m Field Turbidity 800+ NTU 1 10/16/18 10:36 Oxygen, Dissolved 2.17 mg/L 1 10/16/18 10:36 7782-44-7 N2 Depth to Water 28.02 feet 1 10/16/18 10:36 8081 GCS Pesticide Waters Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Aldrin ND ug/L 0.10 0.014 1 10/15/18 14:00 10/18/18 17:04 309-00-2 alpha-BHC ND ug/L 0.10 0.015 1 10/15/18 14:00 10/18/18 17:04 319-84-6 beta-BHC ND ug/L 0.10 0.032 1 10/15/18 14:00 10/18/18 17:04 319-85-7 delta-BHC ND ug/L 0.10 0.018 1 10/15/18 14:00 10/18/18 17:04 319-86-8 gamma-BHC (Lindane) ND ug/L 0.10 0.015 1 10/15/18 14:00 10/18/18 17:04 58-89-9 Chlordane (Technical) ND ug/L 0.50 0.14 1 10/15/18 14:00 10/18/18 17:04 57-74-9 4,4'-DDD ND ug/L 0.10 0.022 1 10/15/18 14:00 10/18/18 17:04 72-54-8 4,4'-DDE ND ug/L 0.10 0.021 1 10/15/18 14:00 10/18/18 17:04 72-55-9 4,4'-DDT ND ug/L 0.10 0.019 1 10/15/18 14:00 10/18/18 17:04 50-29-3 Dieldrin ND ug/L 0.10 0.015 1 10/15/18 14:00 10/18/18 17:04 60-57-1 Endosulfan I ND ug/L 0.50 0.013 1 10/15/18 14:00 10/18/18 17:04 959-98-8 Endosulfan 11 ND ug/L 0.50 0.016 1 10/15/18 14:00 10/18/18 17:04 33213-65-9 Endosulfan sulfate ND ug/L 0.50 0.030 1 10/15/18 14:00 10/18/18 17:04 1031-07-8 Endrin ND ug/L 0.20 0.019 1 10/15/18 14:00 10/18/18 17:04 72-20-8 Endrin aldehyde ND ug/L 0.20 0.024 1 10/15/18 14:00 10/18/18 17:04 7421-93-4 Heptachlor ND ug/L 0.10 0.014 1 10/15/18 14:00 10/18/18 17:04 76-44-8 Heptachlor epoxide ND ug/L 0.10 0.017 1 10/15/18 14:00 10/18/18 17:04 1024-57-3 Isodrin ND ug/L 0.50 0.021 1 10/15/18 14:00 10/18/18 17:04 465-73-6 Methoxychlor ND ug/L 0.30 0.025 1 10/15/18 14:00 10/18/18 17:04 72-43-5 Toxaphene ND ug/L 2.0 0.23 1 10/15/18 14:00 10/18/18 17:04 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 76 %. 19-148 1 10/15/18 14:00 10/18/18 17:04 877-09-8 Decachlorobiphenyl (S) 64 %. 10-157 1 10/15/18 14:00 10/18/18 17:04 2051-24-3 8082 PCB Water GCS Analytical Method: EPA 8082A Preparation Method: EPA 3510C PCB-1016 (Aroclor 1016) ND ug/L 0.50 0.34 1 10/15/18 14:00 10/17/18 11:20 12674-11-2 PCB-1221 (Aroclor 1221) ND ug/L 0.50 0.50 1 10/15/18 14:00 10/17/18 11:20 11104-28-2 PCB-1232 (Aroclor 1232) ND ug/L 0.50 0.50 1 10/15/18 14:00 10/17/18 11:20 11141-16-5 PCB-1242 (Aroclor 1242) ND ug/L 0.50 0.50 1 10/15/18 14:00 10/17/18 11:20 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.50 0.50 1 10/15/18 14:00 10/17/18 11:20 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.50 0.50 1 10/15/18 14:00 10/17/18 11:20 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.50 0.24 1 10/15/18 14:00 10/17/18 11:20 11096-82-5 Surrogates Decachlorobiphenyl (S) 64 %. 17-144 1 10/15/18 14:00 10/17/18 11:20 2051-24-3 Date: 10/30/2018 07:56 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: CMS V Landfill Pace Project No.: 2610392 Sample: 1304-MW33 Lab ID: 2610392001 Collected: 10/10/18 15:42 Received: 10/11/18 13:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8270D MSSV Water, Extend Analytical Method: EPA 8270D Preparation Method: EPA 3510C Acenaphthene ND ug/L 10.0 1.9 1 10/16/18 08:55 10/17/18 21:24 83-32-9 Acenaphthylene ND ug/L 10.0 1.9 1 10/16/18 08:55 10/17/18 21:24 208-96-8 Acetophenone ND ug/L 10.0 3.3 1 10/16/18 08:55 10/17/18 21:24 98-86-2 2-Acetylaminofluorene ND ug/L 10.0 2.7 1 10/16/18 08:55 10/17/18 21:24 53-96-3 4-Aminobiphenyl ND ug/L 10.0 1.4 1 10/16/18 08:55 10/17/18 21:24 92-67-1 Anthracene ND ug/L 10.0 2.7 1 10/16/18 08:55 10/17/18 21:24 120-12-7 Benzo(a)anthracene ND ug/L 10.0 4.2 1 10/16/18 08:55 10/17/18 21:24 56-55-3 Benzo(a)pyrene ND ug/L 10.0 3.7 1 10/16/18 08:55 10/17/18 21:24 50-32-8 Benzo(b)fluoranthene ND ug/L 10.0 4.1 1 10/16/18 08:55 10/17/18 21:24 205-99-2 Benzo(g,h,i)perylene ND ug/L 10.0 4.0 1 10/16/18 08:55 10/17/18 21:24 191-24-2 Benzo(k)fluoranthene ND ug/L 10.0 4.5 1 10/16/18 08:55 10/17/18 21:24 207-08-9 Benzyl alcohol ND ug/L 20.0 2.3 1 10/16/18 08:55 10/17/18 21:24 100-51-6 4-Bromophenylphenyl ND ug/L 10.0 2.5 1 10/16/18 08:55 10/17/18 21:24 101-55-3 ether Butylbenzylphthalate ND ug/L 10.0 4.5 1 10/16/18 08:55 10/17/18 21:24 85-68-7 4-ChIoro-3-methyl phenol ND ug/L 10.0 2.8 1 10/16/18 08:55 10/17/18 21:24 59-50-7 4-Chloroaniline ND ug/L 20.0 2.8 1 10/16/18 08:55 10/17/18 21:24 106-47-8 Chlorobenzilate ND ug/L 10.0 1.6 1 10/16/18 08:55 10/17/18 21:24 510-15-6 bis(2- ND ug/L 10.0 1.6 1 10/16/18 08:55 10/17/18 21:24 111-91-1 Chloroethoxy)methane bis(2-Chloroethyl) ether ND ug/L 10.0 1.4 1 10/16/18 08:55 10/17/18 21:24 111-44-4 2-Chloronaphthalene ND ug/L 10.0 1.6 1 10/16/18 08:55 10/17/18 21:24 91-58-7 2-Chlorophenol ND ug/L 10.0 1.2 1 10/16/18 08:55 10/17/18 21:24 95-57-8 4-Chlorophenylphenyl ND ug/L 10.0 2.7 1 10/16/18 08:55 10/17/18 21:24 7005-72-3 ether Chrysene ND ug/L 10.0 4.1 1 10/16/18 08:55 10/17/18 21:24 218-01-9 Diallate ND ug/L 50.0 2.5 1 10/16/18 08:55 10/17/18 21:24 2303-16-4 Dibenz(a,h)anthracene ND ug/L 10.0 4.5 1 10/16/18 08:55 10/17/18 21:24 53-70-3 Dibenzofuran ND ug/L 10.0 2.1 1 10/16/18 08:55 10/17/18 21:24 132-64-9 3,3'-Dichlorobenzidine ND ug/L 20.0 5.5 1 10/16/18 08:55 10/17/18 21:24 91-94-1 2,4-Dichlorophenol ND ug/L 10.0 2.0 1 10/16/18 08:55 10/17/18 21:24 120-83-2 2,6-Dichlorophenol ND ug/L 10.0 5.1 1 10/16/18 08:55 10/17/18 21:24 87-65-0 Diethylphthalate ND ug/L 10.0 2.7 1 10/16/18 08:55 10/17/18 21:24 84-66-2 Dimethoate ND ug/L 50.0 1.4 1 10/16/18 08:55 10/17/18 21:24 60-51-5 7,12- ND ug/L 50.0 1.5 1 10/16/18 08:55 10/17/18 21:24 57-97-6 Dimethylbenz(a)anthracen e 3,3'-Dimethylbenzidine ND ug/L 50.0 2.3 1 10/16/18 08:55 10/17/18 21:24 119-93-7 2,4-Dimethylphenol ND ug/L 10.0 4.4 1 10/16/18 08:55 10/17/18 21:24 105-67-9 Dimethylphthalate ND ug/L 10.0 2.0 1 10/16/18 08:55 10/17/18 21:24 131-11-3 Di-n-butylphthalate ND ug/L 10.0 3.5 1 10/16/18 08:55 10/17/18 21:24 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 50.0 7.4 1 10/16/18 08:55 10/17/18 21:24 534-52-1 1,3-Dinitrobenzene ND ug/L 10.0 2.9 1 10/16/18 08:55 10/17/18 21:24 99-65-0 2,4-Dinitrophenol ND ug/L 50.0 8.1 1 10/16/18 08:55 10/17/18 21:24 51-28-5 2,4-Dinitrotoluene ND ug/L 20.0 4.2 1 10/16/18 08:55 10/17/18 21:24 121-14-2 2,6-Dinitrotoluene ND ug/L 20.0 2.5 1 10/16/18 08:55 10/17/18 21:24 606-20-2 Di-n-octylphthalate ND ug/L 10.0 5.8 1 10/16/18 08:55 10/17/18 21:24 117-84-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: CMS V Landfill Pace Project No.: 2610392 Sample: 1304-MW33 Lab ID: 2610392001 Collected: 10/10/18 15:42 Received: 10/11/18 13:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8270D MSSV Water, Extend Analytical Method: EPA 8270D Preparation Method: EPA 3510C Dinoseb ND ug/L 10.0 3.3 1 10/16/18 08:55 10/17/18 21:24 88-85-7 1,2-Diphenylhydrazine ND ug/L 10.0 2.0 1 10/16/18 08:55 10/17/18 21:24 122-66-7 Disulfoton ND ug/L 10.0 3.0 1 10/16/18 08:55 10/17/18 21:24 298-04-4 bis(2- Ethyl hexyl)phthalate ND ug/L 10.0 5.2 1 10/16/18 08:55 10/17/18 21:24 117-81-7 Ethyl methanesulfonate ND ug/L 50.0 3.4 1 10/16/18 08:55 10/17/18 21:24 62-50-0 Famphur ND ug/L 10.0 2.1 1 10/16/18 08:55 10/17/18 21:24 52-85-7 Fluoranthene ND ug/L 10.0 3.9 1 10/16/18 08:55 10/17/18 21:24 206-44-0 Fluorene ND ug/L 10.0 2.4 1 10/16/18 08:55 10/17/18 21:24 86-73-7 Hexachloro-1,3-butadiene ND ug/L 10.0 3.7 1 10/16/18 08:55 10/17/18 21:24 87-68-3 Hexachlorobenzene ND ug/L 10.0 2.7 1 10/16/18 08:55 10/17/18 21:24 118-74-1 Hexachlorocyclopentadien ND ug/L 10.0 3.6 1 10/16/18 08:55 10/17/18 21:24 77-47-4 e Hexachloroethane ND ug/L 10.0 2.4 1 10/16/18 08:55 10/17/18 21:24 67-72-1 Hexachloropropene ND ug/L 10.0 2.9 1 10/16/18 08:55 10/17/18 21:24 1888-71-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 4.1 1 10/16/18 08:55 10/17/18 21:24 193-39-5 Isophorone ND ug/L 10.0 2.1 1 10/16/18 08:55 10/17/18 21:24 78-59-1 Isosafrole ND ug/L 50.0 4.0 1 10/16/18 08:55 10/17/18 21:24 120-58-1 Kepone ND ug/L 20.0 12.4 1 10/16/18 08:55 10/17/18 21:24 143-50-0 Methapyrilene ND ug/L 50.0 5.0 1 10/16/18 08:55 10/17/18 21:24 91-80-5 3-Methylcholanthrene ND ug/L 50.0 1.6 1 10/16/18 08:55 10/17/18 21:24 56-49-5 Methyl methanesulfonate ND ug/L 50.0 4.2 1 10/16/18 08:55 10/17/18 21:24 66-27-3 2-Methylnaphthalene ND ug/L 10.0 1.6 1 10/16/18 08:55 10/17/18 21:24 91-57-6 Methyl parathion ND ug/L 10.0 2.4 1 10/16/18 08:55 10/17/18 21:24 298-00-0 2-Methylphenol(o-Cresol) ND ug/L 10.0 2.0 1 10/16/18 08:55 10/17/18 21:24 95-48-7 3&4-Methyl phenol (m&p ND ug/L 10.0 2.0 1 10/16/18 08:55 10/17/18 21:24 Cresol) 1-Naphthalenamine ND ug/L 10.0 2.6 1 10/16/18 08:55 10/17/18 21:24 134-32-7 2-Naphthalenamine ND ug/L 10.0 1.7 1 10/16/18 08:55 10/17/18 21:24 91-59-8 Naphthalene ND ug/L 10.0 1.3 1 10/16/18 08:55 10/17/18 21:24 91-20-3 1,4-Naphthoquinone ND ug/L 50.0 3.7 1 10/16/18 08:55 10/17/18 21:24 130-15-4 2-Nitroaniline ND ug/L 50.0 3.1 1 10/16/18 08:55 10/17/18 21:24 88-74-4 3-Nitroaniline ND ug/L 50.0 3.3 1 10/16/18 08:55 10/17/18 21:24 99-09-2 4-Nitroaniline ND ug/L 50.0 4.9 1 10/16/18 08:55 10/17/18 21:24 100-01-6 Nitrobenzene ND ug/L 10.0 1.4 1 10/16/18 08:55 10/17/18 21:24 98-95-3 2-Nitrophenol ND ug/L 50.0 2.5 1 10/16/18 08:55 10/17/18 21:24 88-75-5 4-Nitrophenol ND ug/L 50.0 9.6 1 10/16/18 08:55 10/17/18 21:24 100-02-7 5-Nitro-o-toluidine ND ug/L 10.0 2.0 1 10/16/18 08:55 10/17/18 21:24 99-55-8 N-Nitrosodiethylamine ND ug/L 10.0 3.5 1 10/16/18 08:55 10/17/18 21:24 55-18-5 N-Nitrosodimethylamine ND ug/L 10.0 2.3 1 10/16/18 08:55 10/17/18 21:24 62-75-9 N-Nitroso-di-n-butylamine ND ug/L 10.0 4.5 1 10/16/18 08:55 10/17/18 21:24 924-16-3 N-Nitroso-di-n- ND ug/L 10.0 2.1 1 10/16/18 08:55 10/17/18 21:24 621-64-7 propylamine N-Nitrosodiphenylamine ND ug/L 10.0 2.3 1 10/16/18 08:55 10/17/18 21:24 86-30-6 N- ND ug/L 10.0 3.5 1 10/16/18 08:55 10/17/18 21:24 10595-95-6 Nitrosomethylethylamine N-Nitrosopiperidine ND ug/L 10.0 3.7 1 10/16/18 08:55 10/17/18 21:24 100-75-4 N-Nitrosopyrrolidine ND ug/L 10.0 4.2 1 10/16/18 08:55 10/17/18 21:24 930-55-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: CMS V Landfill Pace Project No.: 2610392 Sample: 1304-MW33 Lab ID: 2610392001 Collected: 10/10/18 15:42 Received: 10/11/18 13:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8270D MSSV Water, Extend O,O,O- Tri ethyl phosphorothioate 2,2'-Oxybis(1- chloropropane) Parathion (Ethyl parathion) Pentachlorobenzene Pentachloronitrobenzene Pentachlorophenol Phenacetin Phenanthrene Phenol p-Phenylenediamine Phorate Pronamide Pyrene Safrole 1,2,4,5- Tetrachlorobenzene 2,3,4,6-Tetrachlorophenol Thionazin O-Toluidine 1,2,4-Trichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 1,3,5-Trinitrobenzene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) p-Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Water, Extend Acetone Acetonitrile Acrolein Acrylonitrile Allyl chloride Benzene Date: 10/30/2018 07:56 AM Analytical Method: EPA 8270D Preparation Method: EPA 3510C ND ug/L 10.0 3.2 1 10/16/18 08:55 10/17/18 21:24 126-68-1 ND ug/L 10.0 2.6 1 10/16/18 08:55 10/17/18 21:24 108-60-1 ND ug/L 10.0 2.2 1 10/16/18 08:55 10/17/18 21:24 56-38-2 ND ug/L 10.0 3.3 1 10/16/18 08:55 10/17/18 21:24 608-93-5 ND ug/L 10.0 2.3 1 10/16/18 08:55 10/17/18 21:24 82-68-8 ND ug/L 20.0 8.3 1 10/16/18 08:55 10/17/18 21:24 87-86-5 ND ug/L 10.0 1.4 1 10/16/18 08:55 10/17/18 21:24 62-44-2 ND ug/L 10.0 2.5 1 10/16/18 08:55 10/17/18 21:24 85-01-8 ND ug/L 10.0 1.4 1 10/16/18 08:55 10/17/18 21:24 108-95-2 ND ug/L 50.0 9.1 1 10/16/18 08:55 10/17/18 21:24 106-50-3 ND ug/L 10.0 2.0 1 10/16/18 08:55 10/17/18 21:24 298-02-2 ND ug/L 50.0 1.3 1 10/16/18 08:55 10/17/18 21:24 23950-58-5 ND ug/L 10.0 3.4 1 10/16/18 08:55 10/17/18 21:24 129-00-0 ND ug/L 50.0 3.0 1 10/16/18 08:55 10/17/18 21:24 94-59-7 ND ug/L 10.0 1.7 1 10/16/18 08:55 10/17/18 21:24 95-94-3 ND ug/L 20.0 3.2 1 10/16/18 08:55 10/17/18 21:24 58-90-2 ND ug/L 10.0 1.2 1 10/16/18 08:55 10/17/18 21:24 297-97-2 ND ug/L 10.0 3.4 1 10/16/18 08:55 10/17/18 21:24 95-53-4 ND ug/L 10.0 2.0 1 10/16/18 08:55 10/17/18 21:24 120-82-1 ND ug/L 10.0 2.7 1 10/16/18 08:55 10/17/18 21:24 95-95-4 ND ug/L 10.0 2.2 1 10/16/18 08:55 10/17/18 21:24 88-06-2 ND ug/L 10.0 1.4 1 10/16/18 08:55 10/17/18 21:24 99-35-4 56 %. 13-107 1 10/16/18 08:55 10/17/18 21:24 4165-60-0 68 %. 12-129 1 10/16/18 08:55 10/17/18 21:24 321-60-8 89 %. 14-147 1 10/16/18 08:55 10/17/18 21:24 1718-51-0 26 %. 10-46 1 10/16/18 08:55 10/17/18 21:24 13127-88-3 35 %. 10-64 1 10/16/18 08:55 10/17/18 21:24 367-12-4 87 %. 10-148 1 10/16/18 08:55 10/17/18 21:24 118-79-6 Analytical Method: EPA 8260E Mod. ND ug/L 2.0 1.9 1 10/23/18 01:32 123-91-1 98 % 50-150 1 10/23/18 01:32 17060-07-0 110 % 50-150 1 10/23/18 01:32 2037-26-5 Analytical Method: EPA 8260E ND ug/L 100 8.2 1 10/22/1812:34 67-64-1 ND ug/L 50.0 10.0 1 10/22/1812:34 75-05-8 ND ug/L 50.0 7.8 1 10/22/1812:34 107-02-8 ND ug/L 200 2.5 1 10/22/1812:34 107-13-1 ND ug/L 10.0 0.96 1 10/22/1812:34 107-05-1 4.3 ug/L 1.0 0.20 1 10/22/1812:34 71-43-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: CMS V Landfill Pace Project No.: 2610392 Sample: 1304-MW33 Lab ID: 2610392001 Collected: 10/10/18 15:42 Received: 10/11/18 13:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Water, Extend Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Chloroprene 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene Ethyl methacrylate 2-Hexanone lodomethane Isobutanol Methacrylonitrile Methylene Chloride Methyl methacrylate 4-Methyl-2-pe n to n o n e (MIBK) Propionitrile Styrene 1,1,1,2-Tetrachloroethane Date: 10/30/2018 07:56 AM Analytical Method: EPA 8260E ND ug/L 3.0 0.50 1 10/22/1812:34 74-97-5 ND ug/L 1.0 0.36 1 10/22/1812:34 75-27-4 ND ug/L 3.0 0.55 1 10/22/1812:34 75-25-2 ND ug/L 10.0 0.95 1 10/22/1812:34 74-83-9 ND ug/L 100 3.2 1 10/22/1812:34 78-93-3 ND ug/L 100 0.79 1 10/22/1812:34 75-15-0 ND ug/L 1.0 0.42 1 10/22/1812:34 56-23-5 ND ug/L 3.0 0.53 1 10/22/1812:34 108-90-7 ND ug/L 10.0 0.52 1 10/22/1812:34 75-00-3 ND ug/L 5.0 0.58 1 10/22/1812:34 67-66-3 ND ug/L 1.0 0.38 1 10/22/1812:34 74-87-3 ND ug/L 10.0 1.4 1 10/22/1812:34 126-99-8 ND ug/L 13.0 0.55 1 10/22/1812:34 96-12-8 ND ug/L 3.0 0.31 1 10/22/1812:34 124-48-1 ND ug/L 2.0 0.28 1 10/22/1812:34 106-93-4 ND ug/L 10.0 0.62 1 10/22/1812:34 74-95-3 ND ug/L 5.0 0.49 1 10/22/1812:34 95-50-1 ND ug/L 1.0 0.59 1 10/22/1812:34 541-73-1 ND ug/L 1.0 0.58 1 10/22/1812:34 106-46-7 ND ug/L 100 1.6 1 10/22/1812:34 110-57-6 ND ug/L 1.0 0.48 1 10/24/1813:43 75-71-8 2.OJ ug/L 5.0 0.41 1 10/22/1812:34 75-34-3 0.88J ug/L 1.0 0.67 1 10/22/1812:34 107-06-2 ND ug/L 5.0 0.72 1 10/22/1812:34 75-35-4 5.9 ug/L 5.0 0.66 1 10/22/1812:34 156-59-2 1.OJ ug/L 5.0 0.46 1 10/22/1812:34 156-60-5 ND ug/L 1.0 0.60 1 10/22/1812:34 78-87-5 ND ug/L 1.0 0.69 1 10/22/1812:34 142-28-9 ND ug/L 1.0 0.23 1 10/22/1812:34 594-20-7 ND ug/L 1.0 0.60 1 10/22/1812:34 563-58-6 ND ug/L 1.0 0.22 1 10/22/18 12:34 10061-01-5 ND ug/L 1.0 0.30 1 10/22/1812:34 10061-02-6 ND ug/L 1.0 0.45 1 10/22/1812:34 100-41-4 ND ug/L 10.0 0.59 1 10/22/1812:34 97-63-2 ND ug/L 50.0 0.89 1 10/22/1812:34 591-78-6 ND ug/L 10.0 3.1 1 10/22/1812:34 74-88-4 ND ug/L 100 19.0 1 10/22/1812:34 78-83-1 ND ug/L 10.0 0.79 1 10/22/1812:34 126-98-7 4.1 ug/L 1.0 0.50 1 10/22/1812:34 75-09-2 ND ug/L 10.0 0.89 1 10/22/1812:34 80-62-6 ND ug/L 100 0.86 1 10/22/1812:34 108-10-1 ND ug/L 20.0 3.1 1 10/22/1812:34 107-12-0 ND ug/L 1.0 0.50 1 10/22/1812:34 100-42-5 ND ug/L 5.0 0.32 1 10/22/1812:34 630-20-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: CMS V Landfill Pace Project No.: 2610392 Sample: 1304-MW33 Lab ID: 2610392001 Collected: 10/10/18 15:42 Received: 10/11/18 13:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Water, Extend 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Toluene-d8 (S) 9014 Cyanide Cyanide 9034 Sulfide, Titration Sulfide Date: 10/30/2018 07:56 AM Analytical Method: EPA 8260E ND ug/L 3.0 0.53 1 10/22/1812:34 79-34-5 0.92J ug/L 1.0 0.78 1 10/22/1812:34 127-18-4 ND ug/L 1.0 0.31 1 10/22/1812:34 108-88-3 ND ug/L 1.0 0.38 1 10/22/1812:34 71-55-6 ND ug/L 1.0 0.59 1 10/22/1812:34 79-00-5 1.6 ug/L 1.0 0.34 1 10/22/1812:34 79-01-6 ND ug/L 1.0 0.51 1 10/22/1812:34 75-69-4 ND ug/L 1.0 0.46 1 10/22/1812:34 96-18-4 ND ug/L 50.0 0.42 1 10/22/1812:34 108-05-4 3.6 ug/L 1.0 0.60 1 10/22/1812:34 75-01-4 ND ug/L 5.0 1.5 1 10/22/1812:34 1330-20-7 106 %. 81-119 1 10/22/1812:34 17060-07-0 102 %. 81-119 1 10/24/1813:43 17060-07-0 96 %. 82-114 1 10/24/1813:43 1868-53-7 103 %. 82-114 1 10/22/1812:34 1868-53-7 106 %. 82-120 1 10/24/1813:43 460-00-4 107 %. 82-120 1 10/22/1812:34 460-00-4 96 %. 82-109 1 10/22/1812:34 2037-26-5 102 %. 82-109 1 10/24/1813:43 2037-26-5 Analytical Method: EPA 9014 Cyanide Preparation Method: EPA 9010C ND mg/L 0.010 0.010 1 10/15/1810:43 10/15/1814:02 57-12-5 Analytical Method: EPA 9034 Preparation Method: EPA 9030A 3.8 mg/L 1.0 1 10/15/1812:19 10/16/1813:58 18496-25-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: CMS V Landfill Pace Project No.: 2610392 Sample: 1304-MW33 Lab ID: 2610392002 Collected: 10/11/18 07:28 Received: 10/11/18 13:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Analytical Method: Collected By WF 1 10/16/18 10:36 Field Turbidity 12 NTU 1 10/16/18 10:36 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3005A Antimony ND ug/L 6.0 0.78 1 10/18/1810:32 10/22/1818:01 7440-36-0 Arsenic ND ug/L 10.0 0.57 1 10/18/1810:32 10/22/1818:01 7440-38-2 Barium 91.2J ug/L 100 0.78 1 10/18/1810:32 10/22/1818:01 7440-39-3 Beryllium 0.065J ug/L 1.0 0.050 1 10/18/1810:32 10/22/1818:01 7440-41-7 Cadmium 0.21J ug/L 1.0 0.093 1 10/18/1810:32 10/22/1818:01 7440-43-9 Chromium 2.3J ug/L 10.0 1.6 1 10/18/1810:32 10/22/1818:01 7440-47-3 Cobalt 0.77J ug/L 10.0 0.52 1 10/18/1810:32 10/22/1818:01 7440-48-4 Copper 9.6J ug/L 10.0 1.3 1 10/18/1810:32 10/22/1818:01 7440-50-8 Lead 0.33J ug/L 10.0 0.27 1 10/18/1810:32 10/22/1818:01 7439-92-1 Nickel 3.4J ug/L 50.0 0.95 1 10/18/1810:32 10/22/1818:01 7440-02-0 Selenium ND ug/L 10.0 1.4 1 10/18/1810:32 10/22/1818:01 7782-49-2 Silver ND ug/L 10.0 0.95 1 10/18/1810:32 10/22/1818:01 7440-22-4 Thallium ND ug/L 5.5 0.14 1 10/18/1810:32 10/22/1818:01 7440-28-0 Tin ND ug/L 20.0 7.0 1 10/18/1810:32 10/22/1818:01 7440-31-5 Vanadium ND ug/L 25.0 1.9 1 10/18/1810:32 10/22/1818:01 7440-62-2 Zinc 12.7 ug/L 10.0 2.1 1 10/18/1810:32 10/22/1818:01 7440-66-6 B 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury 0.31 ug/L 0.20 0.036 1 10/15/1816:08 10/16/1814:23 7439-97-6 B Date: 10/30/2018 07:56 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: CMS V Landfill Pace Project No.: 2610392 Sample: 1304-Trip Blank Lab ID: 2610392003 Collected: 10/10/18 00:00 Received: 10/11/18 13:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260B MSV Water, Extend Acetone Acetonitrile Acrolein Acrylonitrile Allyl chloride Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Chloroprene 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene Date: 10/30/2018 07:56 AM Analytical Method: EPA 8260E Mod. ND ug/L 2.0 1.9 1 10/22/1816:50 123-91-1 96 % 50-150 1 10/22/1816:50 17060-07-0 97 % 50-150 1 10/22/1816:50 2037-26-5 Analytical Method: EPA 8260E ND ug/L 100 8.2 1 10/22/1812:09 67-64-1 ND ug/L 50.0 10.0 1 10/22/1812:09 75-05-8 ND ug/L 50.0 7.8 1 10/22/1812:09 107-02-8 ND ug/L 200 2.5 1 10/22/1812:09 107-13-1 ND ug/L 10.0 0.96 1 10/22/1812:09 107-05-1 ND ug/L 1.0 0.20 1 10/22/1812:09 71-43-2 ND ug/L 3.0 0.50 1 10/22/1812:09 74-97-5 ND ug/L 1.0 0.36 1 10/22/1812:09 75-27-4 ND ug/L 3.0 0.55 1 10/22/1812:09 75-25-2 ND ug/L 10.0 0.95 1 10/22/1812:09 74-83-9 ND ug/L 100 3.2 1 10/22/1812:09 78-93-3 ND ug/L 100 0.79 1 10/22/1812:09 75-15-0 ND ug/L 1.0 0.42 1 10/22/1812:09 56-23-5 ND ug/L 3.0 0.53 1 10/22/1812:09 108-90-7 ND ug/L 10.0 0.52 1 10/22/1812:09 75-00-3 ND ug/L 5.0 0.58 1 10/22/1812:09 67-66-3 ND ug/L 1.0 0.38 1 10/22/1812:09 74-87-3 ND ug/L 10.0 1.4 1 10/22/1812:09 126-99-8 ND ug/L 13.0 0.55 1 10/22/1812:09 96-12-8 ND ug/L 3.0 0.31 1 10/22/1812:09 124-48-1 ND ug/L 2.0 0.28 1 10/22/1812:09 106-93-4 ND ug/L 10.0 0.62 1 10/22/1812:09 74-95-3 ND ug/L 5.0 0.49 1 10/22/1812:09 95-50-1 ND ug/L 1.0 0.59 1 10/22/1812:09 541-73-1 ND ug/L 1.0 0.58 1 10/22/1812:09 106-46-7 ND ug/L 100 1.6 1 10/22/1812:09 110-57-6 ND ug/L 1.0 0.48 1 10/22/1812:09 75-71-8 ND ug/L 5.0 0.41 1 10/22/1812:09 75-34-3 ND ug/L 1.0 0.67 1 10/22/1812:09 107-06-2 ND ug/L 5.0 0.72 1 10/22/1812:09 75-35-4 ND ug/L 5.0 0.66 1 10/22/1812:09 156-59-2 ND ug/L 5.0 0.46 1 10/22/1812:09 156-60-5 ND ug/L 1.0 0.60 1 10/22/1812:09 78-87-5 ND ug/L 1.0 0.69 1 10/22/1812:09 142-28-9 ND ug/L 1.0 0.23 1 10/22/1812:09 594-20-7 ND ug/L 1.0 0.60 1 10/22/1812:09 563-58-6 ND ug/L 1.0 0.22 1 10/22/1812:09 10061-01-5 ND ug/L 1.0 0.30 1 10/22/1812:09 10061-02-6 ND ug/L 1.0 0.45 1 10/22/1812:09 100-41-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. L1 Page 12 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: CMS V Landfill Pace Project No.: 2610392 Sample: 1304-Trip Blank Lab ID: 2610392003 Collected: 10/10/18 00:00 Received: 10/11/18 13:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Water, Extend Ethyl methacrylate 2-Hexanone lodomethane Isobutanol Methacrylonitrile Methylene Chloride Methyl methacrylate 4-M ethyl-2-pe n to n o n e (MIBK) Propionitrile Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) Surrogates 1,2-Dichloroethane-d4 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 10/30/2018 07:56 AM Analytical Method: EPA 8260E ND ug/L 10.0 0.59 ND ug/L 50.0 0.89 ND ug/L 10.0 3.1 ND ug/L 100 19.0 ND ug/L 10.0 0.79 ND ug/L 1.0 0.50 ND ug/L 10.0 0.89 ND ug/L 100 0.86 ND ug/L 20.0 3.1 ND ug/L 1.0 0.50 ND ug/L 5.0 0.32 ND ug/L 3.0 0.53 ND ug/L 1.0 0.78 ND ug/L 1.0 0.31 ND ug/L 1.0 0.38 ND ug/L 1.0 0.59 ND ug/L 1.0 0.34 ND ug/L 1.0 0.51 ND ug/L 1.0 0.46 ND ug/L 50.0 0.42 ND ug/L 1.0 0.60 ND ug/L 5.0 1.5 103 %. 81-119 101 %. 82-114 107 %. 82-120 98 %. 82-109 1 10/22/18 12:09 97-63-2 1 10/22/18 12:09 591-78-6 1 10/22/18 12:09 74-88-4 1 10/22/18 12:09 78-83-1 1 10/22/18 12:09 126-98-7 1 10/22/18 12:09 75-09-2 1 10/22/18 12:09 80-62-6 1 10/22/18 12:09 108-10-1 1 10/22/18 12:09 107-12-0 1 10/22/18 12:09 100-42-5 1 10/22/18 12:09 630-20-6 1 10/22/18 12:09 79-34-5 1 10/22/18 12:09 127-18-4 1 10/22/18 12:09 108-88-3 1 10/22/18 12:09 71-55-6 1 10/22/18 12:09 79-00-5 1 10/22/18 12:09 79-01-6 1 10/22/18 12:09 75-69-4 1 10/22/18 12:09 96-18-4 1 10/22/18 12:09 108-05-4 1 10/22/18 12:09 75-01-4 1 10/22/18 12:09 1330-20-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 10/22/18 12:09 17060-07-0 10/22/18 12:09 1868-53-7 10/22/18 12:09 460-00-4 10/22/18 12:09 2037-26-5 Page 13 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 QC Batch: 15402 Analysis Method: EPA 7470A QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury Associated Lab Samples: 2610392002 METHOD BLANK: 68876 Matrix: Water Associated Lab Samples: 2610392002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury ug/L 0.064J 0.20 0.036 10/16/1813:17 LABORATORY CONTROL SAMPLE: 68877 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.7 107 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 68878 68879 MS MSD 2610107021 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L ND 2.5 2.5 2.5 2.1 99 83 75-125 18 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 QC Batch: 15602 Analysis Method: EPA 6020B QC Batch Method: EPA 3005A Analysis Description: 6020E MET Associated Lab Samples: 2610392002 METHOD BLANK: 69649 Associated Lab Samples: 2610392002 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Antimony ug/L ND 6.0 0.78 10/22/1817:49 Arsenic ug/L ND 10.0 0.57 10/22/1817:49 Barium ug/L ND 100 0.78 10/22/1817:49 Beryllium ug/L ND 1.0 0.050 10/22/1817:49 Cadmium ug/L ND 1.0 0.093 10/22/1817:49 Chromium ug/L ND 10.0 1.6 10/22/1817:49 Cobalt ug/L ND 10.0 0.52 10/22/1817:49 Copper ug/L ND 10.0 1.3 10/22/1817:49 Lead ug/L ND 10.0 0.27 10/22/1817:49 Nickel ug/L ND 50.0 0.95 10/22/1817:49 Selenium ug/L ND 10.0 1.4 10/22/1817:49 Silver ug/L ND 10.0 0.95 10/22/1817:49 Thallium ug/L ND 5.5 0.14 10/22/1817:49 Tin ug/L ND 20.0 7.0 10/22/1817:49 Vanadium ug/L ND 25.0 1.9 10/22/1817:49 Zinc ug/L 2.8J 10.0 2.1 10/22/1817:49 LABORATORY CONTROL SAMPLE: 69650 Parameter Units Antimony ug/L Arsenic ug/L Barium ug/L Beryllium ug/L Cadmium ug/L Chromium ug/L Cobalt ug/L Copper ug/L Lead ug/L Nickel ug/L Selenium ug/L Silver ug/L Thallium ug/L Tin ug/L Vanadium ug/L Zinc ug/L Spike Conc. LCS Result LCS % Rec % Rec Limits 100 102 102 80-120 100 101 101 80-120 100 100 100 80-120 100 104 104 80-120 100 99.0 99 80-120 100 103 103 80-120 100 103 103 80-120 100 104 104 80-120 100 100 100 80-120 100 101 101 80-120 100 103 103 80-120 100 102 102 80-120 100 99.9 100 80-120 100 100 100 80-120 100 106 106 80-120 100 104 104 80-120 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 69651 69652 MS MSD 2610392002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 100 100 103 101 103 101 75-125 2 20 Arsenic ug/L ND 100 100 101 96.7 100 96 75-125 4 20 Barium ug/L 91.2J 100 100 193 193 101 102 75-125 0 20 Beryllium ug/L 0.065J 100 100 101 103 101 103 75-125 2 20 Cadmium ug/L 0.21J 100 100 99.6 99.9 99 100 75-125 0 20 Chromium ug/L 2.3J 100 100 106 102 103 100 75-125 3 20 Cobalt ug/L 0.77J 100 100 102 98.3 101 97 75-125 4 20 Copper ug/L 9.6J 100 100 114 111 104 101 75-125 2 20 Lead ug/L 0.33J 100 100 98.0 95.6 98 95 75-125 2 20 Nickel ug/L 3AJ 100 100 103 102 100 98 75-125 1 20 Selenium ug/L ND 100 100 104 103 103 101 75-125 1 20 Silver ug/L ND 100 100 98.4 99.6 98 100 75-125 1 20 Thallium ug/L ND 100 100 97.4 95.3 97 95 75-125 2 20 Tin ug/L ND 100 100 99.4 99.2 99 99 75-125 0 20 Vanadium ug/L ND 100 100 109 104 107 102 75-125 4 20 Zinc ug/L 12.7 100 100 112 111 99 98 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 QC Batch: 437651 Analysis Method: EPA 8260B Mod. QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM Associated Lab Samples: 2610392001, 2610392003 METHOD BLANK: 2406638 Matrix: Water Associated Lab Samples: 2610392001, 2610392003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 1.9 10/22/18 15:51 1,2-Dichloroethane-d4 (S) % 97 50-150 10/22/18 15:51 Toluene-d8 (S) % 97 50-150 10/22/18 15:51 LABORATORY CONTROL SAMPLE: 2406639 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 19.4 97 71-125 1,2-Dichloroethane-d4 (S) % 94 50-150 Toluene-d8(S) % 103 50-150 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2406640 2406641 MS MSD 2610388002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane(p-Dioxane) ug/L 12.6 20 20 33.8 33.0 106 102 50-150 2 30 1,2-Dichloroethane-d4 (S) % 101 101 50-150 30 Toluene-d8 (S) % 108 112 50-150 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 QC Batch: 15738 Analysis Method: EPA 8260B QC Batch Method: EPA 8260E Analysis Description: 8260E MSV Water, Extend Associated Lab Samples: 2610392001, 2610392003 METHOD BLANK: 70307 Associated Lab Samples: 2610392001, 2610392003 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 0.32 10/22/18 11:43 1,1,1-Trichloroethane ug/L ND 1.0 0.38 10/22/18 11:43 1,1,2,2-Tetrachloroethane ug/L ND 3.0 0.53 10/22/18 11:43 1,1,2-Trichloroethane ug/L ND 1.0 0.59 10/22/18 11:43 1,1-Dichloroethane ug/L ND 5.0 0.41 10/22/18 11:43 1,1-Dichloroethene ug/L ND 5.0 0.72 10/22/18 11:43 1,1-Dichloropropene ug/L ND 1.0 0.60 10/22/18 11:43 1,2,3-Trichloropropane ug/L ND 1.0 0.46 10/22/18 11:43 1,2-Dibromo-3-chloropropane ug/L ND 13.0 0.55 10/22/18 11:43 1,2-Dibromoethane (EDB) ug/L ND 2.0 0.28 10/22/18 11:43 1,2-Dichlorobenzene ug/L ND 5.0 0.49 10/22/18 11:43 1,2-Dichloroethane ug/L ND 1.0 0.67 10/22/18 11:43 1,2-Dichloropropane ug/L ND 1.0 0.60 10/22/18 11:43 1,3-Dichlorobenzene ug/L ND 1.0 0.59 10/22/18 11:43 1,3-Dichloropropane ug/L ND 1.0 0.69 10/22/18 11:43 1,4-Dichlorobenzene ug/L ND 1.0 0.58 10/22/18 11:43 2,2-Dichloropropane ug/L ND 1.0 0.23 10/22/18 11:43 2-Butanone (MEK) ug/L ND 100 3.2 10/22/18 11:43 2-Hexanone ug/L ND 50.0 0.89 10/22/18 11:43 4-Methyl-2-pentanone (MIBK) ug/L ND 100 0.86 10/22/18 11:43 Acetone ug/L ND 100 8.2 10/22/18 11:43 Acetonitrile ug/L ND 50.0 10.0 10/22/18 11:43 Acrolein ug/L ND 50.0 7.8 10/22/18 11:43 Acrylonitrile ug/L ND 200 2.5 10/22/18 11:43 Allyl chloride ug/L ND 10.0 0.96 10/22/18 11:43 Benzene ug/L ND 1.0 0.20 10/22/18 11:43 Bromochloromethane ug/L ND 3.0 0.50 10/22/18 11:43 Bromodichloromethane ug/L ND 1.0 0.36 10/22/18 11:43 Bromoform ug/L ND 3.0 0.55 10/22/18 11:43 Bromomethane ug/L ND 10.0 0.95 10/22/18 11:43 Carbon disulfide ug/L ND 100 0.79 10/22/18 11:43 Carbon tetrachloride ug/L ND 1.0 0.42 10/22/18 11:43 Chlorobenzene ug/L ND 3.0 0.53 10/22/18 11:43 Chloroethane ug/L ND 10.0 0.52 10/22/18 11:43 Chloroform ug/L ND 5.0 0.58 10/22/18 11:43 Chloromethane ug/L ND 1.0 0.38 10/22/18 11:43 Chloroprene ug/L ND 10.0 1.4 10/22/18 11:43 cis-1,2-Dichloroethene ug/L ND 5.0 0.66 10/22/18 11:43 cis-1,3-Dichloropropene ug/L ND 1.0 0.22 10/22/18 11:43 Dibromochloromethane ug/L ND 3.0 0.31 10/22/18 11:43 Dibromomethane ug/L ND 10.0 0.62 10/22/18 11:43 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 METHOD BLANK: 70307 Associated Lab Samples: Parameter 2610392001, 2610392003 Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Dichlorodifluoromethane ug/L ND 1.0 0.48 10/22/18 11:43 Ethyl methacrylate ug/L ND 10.0 0.59 10/22/18 11:43 Ethylbenzene ug/L ND 1.0 0.45 10/22/18 11:43 lodomethane ug/L ND 10.0 3.1 10/22/18 11:43 Isobutanol ug/L ND 100 19.0 10/22/18 11:43 Methacrylonitrile ug/L ND 10.0 0.79 10/22/18 11:43 Methyl methacrylate ug/L ND 10.0 0.89 10/22/18 11:43 Methylene Chloride ug/L ND 1.0 0.50 10/22/18 11:43 Propionitrile ug/L ND 20.0 3.1 10/22/18 11:43 Styrene ug/L ND 1.0 0.50 10/22/18 11:43 Tetrachloroethene ug/L ND 1.0 0.78 10/22/18 11:43 Toluene ug/L ND 1.0 0.31 10/22/18 11:43 trans-1,2-Dichloroethene ug/L ND 5.0 0.46 10/22/18 11:43 trans- 1,3-Dichloropropene ug/L ND 1.0 0.30 10/22/18 11:43 trans-1,4-Dichloro-2-butene ug/L ND 100 1.6 10/22/18 11:43 Trichloroethene ug/L ND 1.0 0.34 10/22/18 11:43 Trichlorofluoromethane ug/L ND 1.0 0.51 10/22/18 11:43 Vinyl acetate ug/L ND 50.0 0.42 10/22/18 11:43 Vinyl chloride ug/L ND 1.0 0.60 10/22/18 11:43 Xylene (Total) ug/L ND 5.0 1.5 10/22/18 11:43 1,2-Dichloroethane-d4 (S) %. 100 81-119 10/22/18 11:43 4-Bromofluorobenzene (S) %. 105 82-120 10/22/18 11:43 Dibromofluoromethane (S) %. 101 82-114 10/22/18 11:43 Toluene-d8 (S) %. 97 82-109 10/22/18 11:43 LABORATORY CONTROL SAMPLE: Parameter 70308 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 49.4 99 68-137 1,1,1-Trichloroethane ug/L 50 56.0 112 72-134 1,1,2,2-Tetrachloroethane ug/L 50 48.1 96 51-158 1,1,2-Trichloroethane ug/L 50 54.7 109 78-131 1,1-Dichloroethane ug/L 50 56.4 113 69-151 1,1-Dichloroethene ug/L 50 55.3 111 64-158 1,1-Dichloropropene ug/L 50 53.1 106 70-133 1,2,3-Trichloropropane ug/L 50 47.1 94 78-133 1,2-Dibromo-3-chloropropane ug/L 50 45.4 91 58-124 1,2-Dibromoethane (EDB) ug/L 50 50.8 102 71-134 1,2-Dichlorobenzene ug/L 50 53.3 107 70-135 1,2-Dichloroethane ug/L 50 55.8 112 72-129 1,2-Dichloropropane ug/L 50 54.4 109 64-135 1,3-Dichlorobenzene ug/L 50 55.2 110 71-134 1,3-Dichloropropane ug/L 50 54.2 108 70-140 1,4-Dichlorobenzene ug/L 50 49.4 99 70-131 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 LABORATORY CONTROL SAMPLE: Parameter 70308 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2,2-Dichloropropane ug/L 50 59.9 120 34-170 2-Butanone (MEK) ug/L 100 103 103 52-143 2-Hexanone ug/L 100 93.4 93 61-136 4-Methyl-2-pentanone (MIBK) ug/L 100 83.2J 83 71-129 Acetone ug/L 100 104 104 48-224 Acrolein ug/L 100 107 107 57-185 Acrylonitrile ug/L 200 181J 90 66-154 Allyl chloride ug/L 100 95.0 95 58-150 Benzene ug/L 50 54.4 109 68-132 Bromochloromethane ug/L 50 53.5 107 73-133 Bromodichloromethane ug/L 50 47.4 95 67-121 Bromoform ug/L 50 45.4 91 57-125 Bromomethane ug/L 50 35.0 70 35-156 Carbon disulfide ug/L 100 99.8J 100 47-141 Carbon tetrachloride ug/L 50 56.2 112 66-122 Chlorobenzene ug/L 50 52.7 105 71-126 Chloroethane ug/L 50 45.2 90 43-143 Chloroform ug/L 50 56.2 112 71-136 Chloromethane ug/L 50 48.3 97 47-123 cis-1,2-Dichloroethene ug/L 50 56.7 113 74-131 cis-1,3-Dichloropropene ug/L 50 47.3 95 78-120 Dibromochloromethane ug/L 50 46.5 93 65-115 Dibromomethane ug/L 50 56.8 114 79-129 Dichlorodifluoromethane ug/L 50 73.7 147 29-124 L1 Ethyl methacrylate ug/L 100 92.6 93 75-130 Ethylbenzene ug/L 50 55.8 112 68-129 lodomethane ug/L 100 109 109 49-154 Methacrylonitrile ug/L 100 87.9 88 74-139 Methyl methacrylate ug/L 100 87.9 88 75-133 Methylene Chloride ug/L 50 47.8 96 61-147 Propionitrile ug/L 100 88.8 89 69-139 Styrene ug/L 50 50.5 101 77-128 Tetrachloroethene ug/L 50 40.7 81 51-139 Toluene ug/L 50 55.4 111 60-133 trans-1,2-Dichloroethene ug/L 50 53.1 106 69-144 trans- 1,3-Dichloropropene ug/L 50 47.0 94 74-128 trans-1,4-Dichloro-2-butene ug/L 100 99.5J 100 61-139 Trichloroethene ug/L 50 51.5 103 73-126 Trichlorofluoromethane ug/L 50 59.1 118 55-132 Vinyl acetate ug/L 50 45.5J 91 52-141 Vinyl chloride ug/L 50 49.1 98 50-133 Xylene (Total) ug/L 150 155 104 78-132 1,2-Dichloroethane-d4 (S) %. 99 81-119 4-Bromofluorobenzene (S) %. 100 82-120 Dibromofluoromethane (S) %. 107 82-114 Toluene-d8 (S) %. 97 82-109 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 70309 70310 MS MSD 2610663006 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 50 50 42.2 45.4 84 91 68-137 7 11 1,1,1-Trichloroethane ug/L ND 50 50 56.2 58.9 112 118 66-142 5 11 1,1,2,2-Tetrachloroethane ug/L ND 50 50 39.7 42.6 79 85 39-171 7 13 1,1,2-Trichloroethane ug/L ND 50 50 46.9 48.4 94 97 73-136 3 12 1,1-Dichloroethane ug/L ND 50 50 52.5 54.2 105 108 66-155 3 15 1,1-Dichloroethene ug/L ND 50 50 54.7 56.4 109 113 33-181 3 34 1,1-Dichloropropene ug/L ND 50 50 51.5 54.0 103 108 70-133 5 12 1,2,3-Trichloropropane ug/L ND 50 50 35.5 38.0 71 76 78-133 7 14 M1 1,2-Dibromo-3- ug/L ND 50 50 40.7 40.1 81 80 58-124 1 15 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 50 50 43.3 46.0 87 92 71-134 6 12 1,2-Dichlorobenzene ug/L ND 50 50 46.3 51.0 93 102 69-135 10 10 1,2-Dichloroethane ug/L ND 50 50 47.0 48.8 94 98 36-159 4 10 1,2-Dichloropropane ug/L ND 50 50 45.6 50.2 91 100 68-132 10 11 1,3-Dichlorobenzene ug/L ND 50 50 48.4 52.8 97 106 68-135 9 10 1,3-Dichloropropane ug/L ND 50 50 47.4 48.6 95 97 70-138 3 10 1,4-Dichlorobenzene ug/L ND 50 50 42.7 47.3 85 95 49-153 10 9 R1 2,2-Dichloropropane ug/L ND 50 50 55.8 57.6 112 115 34-170 3 9 2-Butanone (MEK) ug/L ND 100 100 64.8J 69.3J 65 69 10-189 7 23 2-Hexanone ug/L ND 100 100 61.8 65.4 62 65 40-135 6 18 4-Methyl-2-pentanone ug/L ND 100 100 72.6J 75.5J 73 76 30-177 4 10 (MIBK) Acetone ug/L ND 100 100 48.6J 52.5J 49 53 44-223 8 14 Acrolein ug/L ND 100 100 87.7 87.3 88 87 57-185 0 30 Acrylonitrile ug/L ND 200 200 146J 154J 73 77 13-189 5 12 Allyl chloride ug/L ND 100 100 83.8 89.2 84 89 58-150 6 18 Benzene ug/L 26.1 50 50 60.1 86.5 68 121 66-139 36 10 R1 Bromochloromethane ug/L ND 50 50 51.9 53.0 104 106 73-133 2 13 Bromodichloromethane ug/L ND 50 50 41.2 42.6 82 85 57-120 3 13 Bromoform ug/L ND 50 50 38.7 42.7 77 85 48-128 10 13 Bromomethane ug/L ND 50 50 24.0 27.9 48 56 10-187 15 32 Carbon disulfide ug/L ND 100 100 94.2J 101 94 101 47-141 7 322 Carbon tetrachloride ug/L ND 50 50 55.7 58.2 111 116 58-127 4 14 Chlorobenzene ug/L ND 50 50 46.2 49.0 92 98 63-137 6 10 Chloroethane ug/L ND 50 50 40.3 42.2 81 84 52-146 5 16 Chloroform ug/L ND 50 50 50.4 53.2 101 106 74-137 5 9 Chloromethane ug/L ND 50 50 41.2 42.9 82 86 41-127 4 10 cis-1,2-Dichloroethene ug/L ND 50 50 53.0 56.1 106 112 71-138 6 16 cis-1,3-Dichloropropene ug/L ND 50 50 42.2 44.1 84 88 32-145 4 12 Dibromochloromethane ug/L ND 50 50 40.5 42.9 81 86 52-116 6 13 Dibromomethane ug/L ND 50 50 52.3 56.1 105 112 79-129 7 14 Dichlorodifluoromethane ug/L ND 50 50 87.2 93.3 174 187 36-126 7 15 MO Ethyl methacrylate ug/L ND 100 100 79.4 85.6 79 86 75-130 8 14 Ethylbenzene ug/L ND 50 50 47.9 52.4 95 104 31-174 9 10 lodomethane ug/L ND 100 100 87.4 86.1 87 86 49-154 2 30 Methacrylonitrile ug/L ND 100 100 75.0 78.5 75 79 74-139 5 14 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 70309 70310 MS MSD 2610663006 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Methyl methacrylate ug/L ND 100 100 70.5 76.0 70 76 75-133 8 13 M1 Methylene Chloride ug/L ND 50 50 40.9 42.1 82 84 61-146 3 15 Propionitrile ug/L ND 100 100 82.1 78.7 82 79 69-139 4 16 Styrene ug/L ND 50 50 42.8 46.9 86 94 77-128 9 14 Tetrachloroethene ug/L ND 50 50 39.6 44.3 79 89 36-155 11 14 Toluene ug/L 34.9 50 50 60.4 95.2 51 120 52-146 45 11 M1,R1 trans-1,2-Dichloroethene ug/L ND 50 50 47.5 50.4 95 101 61-152 6 14 trans-1,3-Dichloropropene ug/L ND 50 50 39.9 42.8 80 86 37-146 7 12 trans-1,4-Dichloro-2-butene ug/L ND 100 100 58.3J 62.2J 58 62 61-139 6 12 M1 Trichloroethene ug/L ND 50 50 45.0 47.5 90 95 61-141 5 12 Trichlorofluoromethane ug/L ND 50 50 55.5 59.3 111 119 51-141 7 13 Vinyl acetate ug/L ND 50 50 46.3J 49AJ 93 99 52-141 6 14 Vinyl chloride ug/L ND 50 50 50.3 52.3 101 105 22-156 4 26 Xylene (Total) ug/L 9.1 150 150 134 152 83 95 78-132 13 7 RS 1,2-Dichloroethane-d4 (S) %. 97 95 81-119 4-Bromofluorobenzene (S) %. 103 101 82-120 Dibromofluoromethane (S) %. 111 110 82-114 Toluene-d8 (S) %. 92 94 82-109 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 22 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 QC Batch: 15908 Analysis Method: EPA 8260B QC Batch Method: EPA 8260E Analysis Description: 8260E MSV Water, Extend Associated Lab Samples: 2610392001 METHOD BLANK: 70967 Matrix: Water Associated Lab Samples: 2610392001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Dichlorodifluoromethane ug/L ND 1.0 0.48 10/24/18 13:18 1,2-Dichloroethane-d4 (S) %. 101 81-119 10/24/18 13:18 4-Bromofluorobenzene (S) %. 105 82-120 10/24/18 13:18 Dibromofluoromethane (S) %. 98 82-114 10/24/18 13:18 Toluene-d8 (S) %. 100 82-109 10/24/18 13:18 LABORATORY CONTROL SAMPLE: 70968 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Dichlorodifluoromethane ug/L 50 59.8 120 29-124 1,2-Dichloroethane-d4 (S) %. 99 81-119 4-Bromofluorobenzene (S) %. 100 82-120 Dibromofluoromethane (S) %. 110 82-114 Toluene-d8 (S) %. 100 82-109 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 QC Batch: 15353 Analysis Method: EPA 8081 B QC Batch Method: EPA 3510C Analysis Description: 8081 GCS Pesticides Associated Lab Samples: 2610392001 METHOD BLANK: 68744 Associated Lab Samples: 2610392001 Parameter Units 4,4'-DDD ug/L 4,4'-DDE ug/L 4,4'-DDT ug/L Aldrin ug/L alpha-BHC ug/L beta-BHC ug/L Chlordane (Technical) ug/L delta-BHC ug/L Dieldrin ug/L Endosulfan I ug/L Endosulfan 11 ug/L Endosulfan sulfate ug/L Endrin ug/L Endrin aldehyde ug/L gamma-BHC (Lindane) ug/L Heptachlor ug/L Heptachlor epoxide ug/L Isodrin ug/L Methoxychlor ug/L Toxaphene ug/L Decachlorobiphenyl (S) %. Tetrachloro-m-xylene (S) %. LABORATORY CONTROL SAMPLE: 68745 Matrix: Water Blank Result Reporting Limit MDL Analyzed ND 0.10 0.022 10/18/18 15:59 ND 0.10 0.021 10/18/18 15:59 ND 0.10 0.019 10/18/18 15:59 ND 0.10 0.014 10/18/18 15:59 ND 0.10 0.015 10/18/18 15:59 ND 0.10 0.032 10/18/18 15:59 ND 0.50 0.14 10/18/18 15:59 ND 0.10 0.018 10/18/18 15:59 ND 0.10 0.015 10/18/18 15:59 ND 0.50 0.013 10/18/18 15:59 ND 0.50 0.016 10/18/18 15:59 ND 0.50 0.030 10/18/18 15:59 ND 0.20 0.019 10/18/18 15:59 ND 0.20 0.024 10/18/18 15:59 ND 0.10 0.015 10/18/18 15:59 ND 0.10 0.014 10/18/18 15:59 ND 0.10 0.017 10/18/18 15:59 ND 0.50 0.021 10/18/18 15:59 ND 0.30 0.025 10/18/18 15:59 ND 2.0 0.23 10/18/18 15:59 61 10-157 10/18/18 15:59 40 19-148 10/18/18 15:59 Qualifiers Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 4,4'-DDD ug/L 2.5 2.2 86 56-149 4,4'-DDE ug/L 2.5 2.1 85 54-138 4,4'-DDT ug/L 2.5 2.2 87 29-173 Aldrin ug/L 2.5 1.8 70 49-126 alpha-BHC ug/L 2.5 1.6 64 47-135 beta-BHC ug/L 2.5 2.2 87 57-136 delta-BHC ug/L 2.5 2.1 83 39-121 Dieldrin ug/L 2.5 2.1 84 56-129 Endosulfan I ug/L 2.5 2.3 90 57-135 Endosulfan II ug/L 2.5 2.2 86 60-142 Endosulfan sulfate ug/L 2.5 2.0 81 55-133 Endrin ug/L 2.5 2.2 89 58-148 Endrin aldehyde ug/L 2.5 1.7 68 57-131 gamma-BHC (Lindane) ug/L 2.5 1.8 71 48-135 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 LABORATORY CONTROL SAMPLE: 68745 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Heptachlor ug/L 2.5 1.8 71 45-144 Heptachlor epoxide ug/L 2.5 2.1 82 56-131 Isodrin ug/L 2.5 2.1 83 46-147 Methoxychlor ug/L 2.5 2.1 83 47-166 Decachlorobiphenyl (S) %. 62 10-157 Tetrachloro-m-xylene (S) %. 54 19-148 Qualifiers MATRIX SPIKE SAMPLE: Parameter 68746 Units 2610392001 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 4,4'-DDD ug/L ND 2.5 2.3 94 38-173 4,4'-DDE ug/L ND 2.5 2.2 90 24-172 4,4'-DDT ug/L ND 2.5 2.3 94 28-169 Aldrin ug/L ND 2.5 2.1 86 25-152 alpha-BHC ug/L ND 2.5 2.2 88 45-136 beta-BHC ug/L ND 2.5 2.3 90 34-159 delta-BHC ug/L ND 2.5 2.3 91 32-138 Dieldrin ug/L ND 2.5 2.2 88 32-160 Endosulfan I ug/L ND 2.5 2.3 93 48-151 Endosulfan II ug/L ND 2.5 2.3 93 55-153 Endosulfan sulfate ug/L ND 2.5 2.3 91 52-138 Endrin ug/L ND 2.5 2.3 94 39-180 Endrin aldehyde ug/L ND 2.5 2.3 91 29-164 gamma-BHC (Lindane) ug/L ND 2.5 2.3 91 45-140 Heptachlor ug/L ND 2.5 2.2 89 40-153 Heptachlor epoxide ug/L ND 2.5 2.2 88 46-144 Isodrin ug/L ND 2.5 2.4 97 10-184 Methoxychlor ug/L ND 2.5 2.4 97 10-208 Decachlorobiphenyl (S) %. 72 10-157 Tetrachloro-m-xylene (S) %. 76 19-148 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 QC Batch: 15354 Analysis Method: EPA 8082A QC Batch Method: EPA 3510C Analysis Description: 8082 GCS PCB Associated Lab Samples: 2610392001 METHOD BLANK: 68748 Matrix: Water Associated Lab Samples: 2610392001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers PCB-1016 (Aroclor 1016) ug/L ND 0.50 0.34 10/17/18 09:57 PCB-1221 (Aroclor 1221) ug/L ND 0.50 0.50 10/17/18 09:57 PCB-1232 (Aroclor 1232) ug/L ND 0.50 0.50 10/17/18 09:57 PCB-1242 (Aroclor 1242) ug/L ND 0.50 0.50 10/17/18 09:57 PCB-1248 (Aroclor 1248) ug/L ND 0.50 0.50 10/17/18 09:57 PCB-1254 (Aroclor 1254) ug/L ND 0.50 0.50 10/17/18 09:57 PCB-1260 (Aroclor 1260) ug/L ND 0.50 0.24 10/17/18 09:57 Decachlorobiphenyl (S) %. 62 17-144 10/17/18 09:57 LABORATORY CONTROL SAMPLE: 68749 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers PCB-1016 (Aroclor 1016) ug/L 5 4.1 83 47-120 PCB-1260 (Aroclor 1260) ug/L 5 4.4 89 51-126 Decachlorobiphenyl (S) %. 69 17-144 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 68798 68799 MS MSD 2610392001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual PCB-1016 (Aroclor 1016) ug/L ND 5 5 3.9 4.1 78 82 10-183 5 18 PCB-1260 (Aroclor 1260) ug/L ND 5 5 3.9 4.1 78 82 19-141 5 27 Decachlorobiphenyl (S) %. 65 68 17-144 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 26 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 QC Batch: 15428 Analysis Method: EPA 8270D QC Batch Method: EPA 3510C Analysis Description: 8270D MSSV Extend Associated Lab Samples: 2610392001 METHOD BLANK: 69031 Associated Lab Samples: 2610392001 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed 1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 1.7 10/17/18 18:32 1,2,4-Trichlorobenzene ug/L ND 10.0 2.0 10/17/18 18:32 1,2-Diphenylhydrazine ug/L ND 10.0 2.0 10/17/18 18:32 1,3,5-Trinitrobenzene ug/L ND 10.0 1.4 10/17/18 18:32 1,3-Dinitrobenzene ug/L ND 10.0 2.9 10/17/18 18:32 1,4-Naphthoquinone ug/L ND 50.0 3.7 10/17/18 18:32 1-Naphthalenamine ug/L ND 10.0 2.6 10/17/18 18:32 2,2'-Oxybis(1-chloropropane) ug/L ND 10.0 2.6 10/17/18 18:32 2,3,4,6-Tetrachlorophenol ug/L ND 20.0 3.2 10/17/18 18:32 2,4,5-Trichlorophenol ug/L ND 10.0 2.7 10/17/18 18:32 2,4,6-Trichlorophenol ug/L ND 10.0 2.2 10/17/18 18:32 2,4-Dichlorophenol ug/L ND 10.0 2.0 10/17/18 18:32 2,4-Dimethylphenol ug/L ND 10.0 4.4 10/17/18 18:32 2,4-Dinitrophenol ug/L ND 50.0 8.1 10/17/18 18:32 2,4-Dinitrotoluene ug/L ND 20.0 4.2 10/17/18 18:32 2,6-Dichlorophenol ug/L ND 10.0 5.1 10/17/18 18:32 2,6-Dinitrotoluene ug/L ND 20.0 2.5 10/17/18 18:32 2-Acetylaminofluorene ug/L ND 10.0 2.7 10/17/18 18:32 2-Chloronaphthalene ug/L ND 10.0 1.6 10/17/18 18:32 2-Chlorophenol ug/L ND 10.0 1.2 10/17/18 18:32 2-Methylnaphthalene ug/L ND 10.0 1.6 10/17/18 18:32 2-Methylphenol(o-Cresol) ug/L ND 10.0 2.0 10/17/18 18:32 2-Naphthalenamine ug/L ND 10.0 1.7 10/17/18 18:32 2-Nitroaniline ug/L ND 50.0 3.1 10/17/18 18:32 2-Nitrophenol ug/L ND 50.0 2.5 10/17/18 18:32 3&4-Methyl phenol (m&p Cresol) ug/L ND 10.0 2.0 10/17/18 18:32 3,3'-Dichlorobenzidine ug/L ND 20.0 5.5 10/17/18 18:32 3,3'-Dimethylbenzidine ug/L ND 50.0 2.3 10/17/18 18:32 3-Methylcholanthrene ug/L ND 50.0 1.6 10/17/18 18:32 3-Nitroaniline ug/L ND 50.0 3.3 10/17/18 18:32 4,6-Dinitro-2-methyl phenol ug/L ND 50.0 7.4 10/17/18 18:32 4-Aminobiphenyl ug/L ND 10.0 1.4 10/17/18 18:32 4-Bromophenylphenyl ether ug/L ND 10.0 2.5 10/17/18 18:32 4-ChIoro-3-methyl phenol ug/L ND 10.0 2.8 10/17/18 18:32 4-Chloroaniline ug/L ND 20.0 2.8 10/17/18 18:32 4-Chlorophenylphenyl ether ug/L ND 10.0 2.7 10/17/18 18:32 4-Nitroaniline ug/L ND 50.0 4.9 10/17/18 18:32 4-Nitrophenol ug/L ND 50.0 9.6 10/17/18 18:32 5-Nitro-o-toluidine ug/L ND 10.0 2.0 10/17/18 18:32 7,12-Dimethylbenz(a)anthracene ug/L ND 50.0 1.5 10/17/18 18:32 Acenaphthene ug/L ND 10.0 1.9 10/17/18 18:32 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 27 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 METHOD BLANK: 69031 Associated Lab Samples: 2610392001 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Acenaphthylene ug/L ND 10.0 1.9 10/17/18 18:32 Acetophenone ug/L ND 10.0 3.3 10/17/18 18:32 Anthracene ug/L ND 10.0 2.7 10/17/18 18:32 Benzo(a)anthracene ug/L ND 10.0 4.2 10/17/18 18:32 Benzo(a)pyrene ug/L ND 10.0 3.7 10/17/18 18:32 Benzo(b)fluoranthene ug/L ND 10.0 4.1 10/17/18 18:32 Benzo(g,h,i)perylene ug/L ND 10.0 4.0 10/17/18 18:32 Benzo(k)fluoranthene ug/L ND 10.0 4.5 10/17/18 18:32 Benzyl alcohol ug/L ND 20.0 2.3 10/17/18 18:32 bis(2-Chloroethoxy)methane ug/L ND 10.0 1.6 10/17/18 18:32 bis(2-Chloroethyl) ether ug/L ND 10.0 1.4 10/17/18 18:32 bis(2-Ethylhexyl)phthalate ug/L ND 10.0 5.2 10/17/18 18:32 Butylbenzylphthalate ug/L ND 10.0 4.5 10/17/18 18:32 Chlorobenzilate ug/L ND 10.0 1.6 10/17/18 18:32 Chrysene ug/L ND 10.0 4.1 10/17/18 18:32 Di-n-butylphthalate ug/L ND 10.0 3.5 10/17/18 18:32 Di-n-octylphthalate ug/L ND 10.0 5.8 10/17/18 18:32 Diallate ug/L ND 50.0 2.5 10/17/18 18:32 Dibenz(a,h)anthracene ug/L ND 10.0 4.5 10/17/18 18:32 Dibenzofuran ug/L ND 10.0 2.1 10/17/18 18:32 Diethylphthalate ug/L ND 10.0 2.7 10/17/18 18:32 Dimethoate ug/L ND 50.0 1.4 10/17/18 18:32 Dimethylphthalate ug/L ND 10.0 2.0 10/17/18 18:32 Dinoseb ug/L ND 10.0 3.3 10/17/18 18:32 Disulfoton ug/L ND 10.0 3.0 10/17/18 18:32 Ethyl methanesulfonate ug/L ND 50.0 3.4 10/17/18 18:32 Famphur ug/L ND 10.0 2.1 10/17/18 18:32 Fluoranthene ug/L ND 10.0 3.9 10/17/18 18:32 Fluorene ug/L ND 10.0 2.4 10/17/18 18:32 Hexachloro-1,3-butadiene ug/L ND 10.0 3.7 10/17/18 18:32 Hexachlorobenzene ug/L ND 10.0 2.7 10/17/18 18:32 Hexachlorocyclopentadiene ug/L ND 10.0 3.6 10/17/18 18:32 Hexachloroethane ug/L ND 10.0 2.4 10/17/18 18:32 Hexachloropropene ug/L ND 10.0 2.9 10/17/18 18:32 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 4.1 10/17/18 18:32 Isophorone ug/L ND 10.0 2.1 10/17/18 18:32 Isosafrole ug/L ND 50.0 4.0 10/17/18 18:32 Kepone ug/L ND 20.0 12.4 10/17/18 18:32 Methapyrilene ug/L ND 50.0 5.0 10/17/18 18:32 Methyl methanesulfonate ug/L ND 50.0 4.2 10/17/18 18:32 Methyl parathion ug/L ND 10.0 2.4 10/17/18 18:32 N-Nitroso-di-n-butylamine ug/L ND 10.0 4.5 10/17/18 18:32 N-Nitroso-di-n-propylamine ug/L ND 10.0 2.1 10/17/18 18:32 N-Nitrosodiethylamine ug/L ND 10.0 3.5 10/17/18 18:32 N-Nitrosodimethylamine ug/L ND 10.0 2.3 10/17/18 18:32 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 28 of 49 Pace Analytical Services, LLC aceAnalXica! � 110 Technology Parkway Peachtree Corners, GA 30092 www.pacelabs.com (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 METHOD BLANK: 69031 Associated Lab Samples: 2610392001 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers N-Nitrosodiphenylamine ug/L ND 10.0 2.3 10/17/18 18:32 N-Nitrosomethylethylamine ug/L ND 10.0 3.5 10/17/18 18:32 N-Nitrosopiperidine ug/L ND 10.0 3.7 10/17/18 18:32 N-Nitrosopyrrolidine ug/L ND 10.0 4.2 10/17/18 18:32 Naphthalene ug/L ND 10.0 1.3 10/17/18 18:32 Nitrobenzene ug/L ND 10.0 1.4 10/17/18 18:32 O,O,O-Triethylphosphorothioate ug/L ND 10.0 3.2 10/17/18 18:32 O-Toluidine ug/L ND 10.0 3.4 10/17/18 18:32 p-Phenylenediamine ug/L ND 50.0 9.1 10/17/18 18:32 Parathion (Ethyl parathion) ug/L ND 10.0 2.2 10/17/18 18:32 Pentachlorobenzene ug/L ND 10.0 3.3 10/17/18 18:32 Pentachloronitrobenzene ug/L ND 10.0 2.3 10/17/18 18:32 Pentachlorophenol ug/L ND 20.0 8.3 10/17/18 18:32 Phenacetin ug/L ND 10.0 1.4 10/17/18 18:32 Phenanthrene ug/L ND 10.0 2.5 10/17/18 18:32 Phenol ug/L ND 10.0 1.4 10/17/18 18:32 Phorate ug/L ND 10.0 2.0 10/17/18 18:32 Pronamide ug/L ND 50.0 1.3 10/17/18 18:32 Pyrene ug/L ND 10.0 3.4 10/17/18 18:32 Safrole ug/L ND 50.0 3.0 10/17/18 18:32 Thionazin ug/L ND 10.0 1.2 10/17/18 18:32 2,4,6-Tribromophenol (S) %. 82 10-148 10/17/18 18:32 2-Fluorobiphenyl (S) %. 75 12-129 10/17/18 18:32 2-Fluorophenol (S) %. 35 10-64 10/17/18 18:32 Nitrobenzene-d5 (S) %. 58 13-107 10/17/18 18:32 p-Terphenyl-d14 (S) %. 98 14-147 10/17/18 18:32 Phenol-d6 (S) %. 23 10-46 10/17/18 18:32 LABORATORY CONTROL SAMPLE: 69032 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,2,4,5-Tetrachlorobenzene ug/L 80 65.0 81 52-96 1,2,4-Trichlorobenzene ug/L 80 63.3 79 20-123 1,2-Diphenylhydrazine ug/L 80 61.8 77 29-156 2,2'-Oxybis(1-chloropropane) ug/L 80 54.5 68 22-129 2,4,5-Trichlorophenol ug/L 80 73.8 92 42-149 2,4,6-Trichlorophenol ug/L 80 71.5 89 43-150 2,4-Dichlorophenol ug/L 80 69.3 87 41-117 2,4-Dimethylphenol ug/L 80 59.2 74 25-108 2,4-Dinitrophenol ug/L 80 70.4 88 35-160 2,4-Dinitrotoluene ug/L 80 77.0 96 43-162 2,6-Dinitrotoluene ug/L 80 78.1 98 46-145 2-Chloronaphthalene ug/L 80 66.7 83 37-135 2-Chlorophenol ug/L 80 51.7 65 37-104 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 29 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 LABORATORY CONTROL SAMPLE: Parameter 69032 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 2-Methylnaphthalene ug/L 80 71.6 89 36-114 2-Methylphenol(o-Cresol) ug/L 80 48.2 60 10-114 2-Nitroaniline ug/L 80 60.4 75 22-161 2-Nitrophenol ug/L 80 66.2 83 42-116 3&4-Methyl phenol (m&p Cresol) ug/L 80 47.9 60 10-110 3,3'-Dichlorobenzidine ug/L 80 93.9 117 34-148 3-Nitroaniline ug/L 80 74.0 93 37-156 4,6-Dinitro-2-methyl phenol ug/L 80 85.3 107 56-154 4-Bromophenylphenyl ether ug/L 80 78.6 98 48-153 4-Chloro-3-methylphenol ug/L 80 69.0 86 46-119 4-Chloroaniline ug/L 80 74.2 93 34-121 4-Chlorophenylphenyl ether ug/L 80 76.1 95 44-145 4-Nitroaniline ug/L 80 55.4 69 37-163 4-Nitrophenol ug/L 80 22.8J 28 15-45 Acenaphthene ug/L 80 69.3 87 37-138 Acenaphthylene ug/L 80 70.9 89 43-136 Anthracene ug/L 80 76.9 96 48-151 Benzo(a)anthracene ug/L 80 83.2 104 49-154 Benzo(a)pyrene ug/L 80 80.4 101 45-164 Benzo(b)fluoranthene ug/L 80 76.7 96 46-157 Benzo(g,h,i)perylene ug/L 80 75.6 95 50-161 Benzo(k)fluoranthene ug/L 80 90.8 114 48-158 Benzyl alcohol ug/L 80 52.7 66 21-124 bis(2-Chloroethoxy)methane ug/L 80 64.0 80 29-120 bis(2-Chloroethyl) ether ug/L 80 54.7 68 23-126 bis(2-Ethylhexyl)phthalate ug/L 80 76.7 96 40-156 Butylbenzylphthalate ug/L 80 73.4 92 40-163 Chrysene ug/L 80 85.1 106 49-155 Di-n-butylphthalate ug/L 80 77.3 97 48-160 Di-n-octylphthalate ug/L 80 86.5 108 65-144 Dibenz(a,h)anthracene ug/L 80 74.8 93 44-165 Dibenzofuran ug/L 80 71.7 90 45-135 Diethylphthalate ug/L 80 74.5 93 38-162 Dimethylphthalate ug/L 80 74.5 93 44-150 Fluoranthene ug/L 80 80.3 100 53-156 Fluorene ug/L 80 75.2 94 45-142 Hexachloro-1,3-butadiene ug/L 80 58.8 74 27-92 Hexachlorobenzene ug/L 80 81.9 102 50-149 Hexachlorocyclopentadiene ug/L 80 50.0 63 23-123 Hexachloroethane ug/L 80 45.0 56 19-91 Indeno(1,2,3-cd)pyrene ug/L 80 75.5 94 43-171 Isophorone ug/L 80 66.4 83 18-137 N-Nitroso-di-n-propylamine ug/L 80 59.5 74 12-148 N-Nitrosodimethylamine ug/L 80 37.1 46 12-83 N-Nitrosodiphenylamine ug/L 80 75.6 94 50-130 Naphthalene ug/L 80 61.0 76 35-106 Nitrobenzene ug/L 80 53.3 67 22-115 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 30 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 LABORATORY CONTROL SAMPLE: Parameter 69032 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Pentachlorophenol ug/L 80 68.0 85 42-127 Phenanthrene ug/L 80 76.6 96 49-146 Phenol ug/L 80 22.7 28 18-48 Pyrene ug/L 80 78.1 98 50-146 2,4,6-Tribromophenol (S) %. 116 10-148 2-Fluorobiphenyl (S) %. 93 12-129 2-Fluorophenol (S) %. 38 10-64 Nitrobenzene-d5 (S) %. 73 13-107 p-Terphenyl-d14 (S) %. 122 14-147 Phenol-d6 (S) %. 28 10-46 MATRIX SPIKE SAMPLE: Parameter 69033 Units 2610392001 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,2,4,5-Tetrachlorobenzene ug/L ND 80 45.3 57 52-96 1,2,4-Trichlorobenzene ug/L ND 80 44.8 56 10-127 1,2-Diphenylhydrazine ug/L ND 80 44.0 55 29-156 2,2'-Oxybis(1-chloropropane) ug/L ND 80 41.5 52 22-129 2,4,5-Trichlorophenol ug/L ND 80 53.5 67 42-149 2,4,6-Trichlorophenol ug/L ND 80 53.5 67 43-150 2,4-Dichlorophenol ug/L ND 80 53.1 66 41-117 2,4-Dimethylphenol ug/L ND 80 44.6 56 25-108 2,4-Dinitrophenol ug/L ND 80 45.1J 56 35-160 2,4-Dinitrotoluene ug/L ND 80 62.4 78 43-162 2,6-Dinitrotoluene ug/L ND 80 59.5 74 60-125 2-Chloronaphthalene ug/L ND 80 46.7 58 37-135 2-Chlorophenol ug/L ND 80 41.0 51 33-98 2-Methylnaphthalene ug/L ND 80 51.9 65 36-114 2-Methylphenol(o-Cresol) ug/L ND 80 39.8 50 10-114 2-Nitroaniline ug/L ND 80 47.6J 60 22-161 2-Nitrophenol ug/L ND 80 49.9J 62 42-116 3&4-Methyl phenol (m&p Cresol) ug/L ND 80 39.5 49 10-110 3,3'-Dichlorobenzidine ug/L ND 80 61.3 77 34-148 3-Nitroaniline ug/L ND 80 64.1 80 37-156 4,6-Dinitro-2-methyl phenol ug/L ND 80 60.0 75 56-154 4-Bromophenylphenyl ether ug/L ND 80 56.6 71 48-153 4-Chloro-3-methylphenol ug/L ND 80 56.0 70 44-118 4-Chloroaniline ug/L ND 80 55.5 69 34-121 4-Chlorophenylphenyl ether ug/L ND 80 56.1 70 44-145 4-Nitroaniline ug/L ND 80 48.3J 60 37-163 4-Nitrophenol ug/L ND 80 21.2J 27 10-54 Acenaphthene ug/L ND 80 49.5 62 40-124 Acenaphthylene ug/L ND 80 50.8 64 43-136 Anthracene ug/L ND 80 57.1 71 48-151 Benzo(a)anthracene ug/L ND 80 63.5 79 49-154 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 31 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 MATRIX SPIKE SAMPLE: 69033 2610392001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Benzo(a)pyrene ug/L ND 80 60.0 75 45-164 Benzo(b)fluoranthene ug/L ND 80 54.9 69 46-157 Benzo(g,h,i)perylene ug/L ND 80 57.2 72 50-161 Benzo(k)fluoranthene ug/L ND 80 61.6 77 48-158 Benzyl alcohol ug/L ND 80 44.3 55 21-124 bis(2-Chloroethoxy)methane ug/L ND 80 48.2 60 29-120 bis(2-Chloroethyl) ether ug/L ND 80 39.5 49 23-126 bis(2-Ethylhexyl)phthalate ug/L ND 80 60.5 76 40-156 Butylbenzylphthalate ug/L ND 80 57.7 72 40-163 Chrysene ug/L ND 80 64.1 80 49-155 Di-n-butylphthalate ug/L ND 80 59.1 74 40-163 Di-n-octylphthalate ug/L ND 80 60.9 76 65-144 Dibenz(a,h)anthracene ug/L ND 80 56.5 71 44-165 Dibenzofuran ug/L ND 80 51.7 65 45-135 Diethylphthalate ug/L ND 80 59.1 74 38-162 Dimethylphthalate ug/L ND 80 57.4 72 44-150 Fluoranthene ug/L ND 80 59.5 74 53-156 Fluorene ug/L ND 80 56.1 70 45-142 Hexachloro-1,3-butadiene ug/L ND 80 41.9 52 27-92 Hexachlorobenzene ug/L ND 80 60.6 76 50-149 Hexachlorocyclopentadiene ug/L ND 80 33.2 42 23-123 Hexachloroethane ug/L ND 80 31.9 40 19-91 Indeno(1,2,3-cd)pyrene ug/L ND 80 56.8 71 43-171 Isophorone ug/L ND 80 50.2 63 18-137 N-Nitroso-di-n-propylamine ug/L ND 80 46.2 58 39-106 N-Nitrosodimethylamine ug/L ND 80 27.1 34 12-83 N-Nitrosodiphenylamine ug/L ND 80 51.9 65 50-130 Naphthalene ug/L ND 80 44.4 55 35-106 Nitrobenzene ug/L ND 80 39.4 49 22-115 Pentachlorophenol ug/L ND 80 43.2 54 40-136 Phenanthrene ug/L ND 80 56.1 70 49-146 Phenol ug/L ND 80 18.6 23 20-42 Pyrene ug/L ND 80 60.5 76 52-131 2,4,6-Tribromophenol (S) %. 88 10-148 2-Fluorobiphenyl (S) %. 67 12-129 2-Fluorophenol (S) %. 30 10-64 Nitrobenzene-d5 (S) %. 55 13-107 p-Terphenyl-d14 (S) %. 82 14-147 Phenol-d6 (S) %. 24 10-46 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 32 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 QC Batch: 15361 Analysis Method: EPA 9014 Cyanide QC Batch Method: EPA 9010C Analysis Description: 9014 Cyanide Associated Lab Samples: 2610392001 METHOD BLANK: 68764 Matrix: Water Associated Lab Samples: 2610392001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide mg/L ND 0.010 0.010 10/15/1813:52 LABORATORY CONTROL SAMPLE: 68765 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide mg/L .08 0.082 103 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 68766 68767 MS MSD 2610406049 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide mg/L 0.0102 .08 .08 0.082 0.083 97 99 85-119 2 13 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 33 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: CMS V Landfill Pace Project No.: 2610392 QC Batch: 15362 Analysis Method: EPA 9034 QC Batch Method: EPA 9030A Analysis Description: 9034 Sulfide Waste Water Associated Lab Samples: 2610392001 METHOD BLANK: 68772 Matrix: Water Associated Lab Samples: 2610392001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfide mg/L 0.01 1.0 10/16/18 13:58 LABORATORY CONTROL SAMPLE: 68773 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide mg/L 4 4.0 100 40-104 MATRIX SPIKE SAMPLE: 68774 92403374009 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Sulfide mg/L 7940 ug/L 5.7 12.1 74 10-143 MATRIX SPIKE SAMPLE: 68775 92403374011 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Sulfide mg/L 6080 ug/L 5.7 16.4 180 10-143 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 34 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALIFIERS Project: CMS V Landfill Pace Project No.: 2610392 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. IW_1.101Ica] NI*i PASI-C Pace Analytical Services - Charlotte PASI-GA Pace Analytical Services - Atlanta, GA ANALYTE QUALIFIERS B Analyte was detected in the associated method blank. L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. N2 The lab does not hold NELAC/TNI accreditation for this parameter. R1 RPD value was outside control limits. RS The RPD value in one of the constituent analytes was outside the control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/30/2018 07:56 AM without the written consent of Pace Analytical Services, LLC. Page 35 of 49 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: CMS V Landfill 2610392 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 2610392001 1304-MW33 15449 2610392002 1304-MW33 15449 2610392001 1304-MW33 EPA 3510C 15353 EPA 8081 B 15638 2610392001 1304-MW33 EPA 3510C 15354 EPA 8082A 15421 2610392002 1304-MW33 EPA 3005A 15602 EPA 6020B 15637 2610392002 1304-MW33 EPA 7470A 15402 EPA 7470A 15435 2610392001 1304-MW33 EPA 3510C 15428 EPA 8270D 15569 2610392001 1304-MW33 EPA 8260B Mod. 437651 2610392003 1304-Trip Blank EPA 8260B Mod. 437651 2610392001 1304-MW33 EPA 8260B 15738 2610392001 1304-MW33 EPA 8260B 15908 2610392003 1304-Trip Blank EPA 8260B 15738 2610392001 1304-MW33 EPA 9010C 15361 EPA 9014 Cyanide 15383 2610392001 1304-MW33 EPA 9030A 15362 EPA 9034 15469 Date: 10/30/2018 07:56 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 36 of 49 ]�elul saldwes z OF NA _ Inlo4� D paleag +[ a s n NA) m 3 vwl � ��� y� uo pan�aaaa .. a [NIA} auudiyD ie p�sad c / i� t D uI dY131 [os uo] DO'9af11 dW31 S Hd t .� d CD E m 4aH 1c O U tiC IN C� ❑ m m 8 dRsad G1 � L.1 4cipjjnS ti' Q IW p ❑ Eus . 6H siela4V II 1 dtl 7N :3 'g w N a a uvAo •C �rCV � In YL W iv m "- � a auex ip CL '+C P F 4 m ti pp N ❑ cj OQA IY dy ON x saSAIify NIA ;sal _ m Q m u U r 2 OVuz HDeNLU r £D szeN G i '1 = v HDeN n J 0 a F � a1 SDNH p 2 Z and g 457M g o 4 o ILA pan]a aiduN L,{'Y w F N cG c n ¢ Sti3NIVAN i 7C4 W O N u¢ 0. 0 a Uw dW31 ldWVI; ix HDI1:t37,1QD IV �y7 C 0. L q �. 74 ' p 4 Cl N N Z . E- a ❑ ¢ `v `a @ r E W W.. E a z 4 ~ N r]`j � w t 8 a =z s m d Y N c Z.IdWO�•� BVtI�.�I 3d Al 7dWV5 0 C7 Ly i 0. y � � O ILL�I oI SoDc�P�len a�sl 3[]Q:J Vii1YW � y m � m o o a z rt o ti P 4 J R .0 N ❑ 0 LY} LL 20 ^n O m `` 2 J rJ — ] 7 J 4 a 3E d `4 � ❑ f/) c E Q C M ly p C [V N 2r � f 3 n m N Ill � � Q P,d, 37 of 49 Sampl�, -.-a keAna1yP1caf Client Name: Courier: ❑ Fed Ex ❑ UPS ❑ USPS ❑ Client M Tracking #: Custody Seal on CoolerlBox Present: yes E Packing Material: ❑ Bubble Wrap 215'ub'ble Bags Thermometer Used Ty Cooler Temperature L(' Bi should be above freezing to 6'C j Ct # - - WO# ❑ pN: pN CLIENT; fie ❑ ❑ate and Initia contents: —MyTomp Condition Upon Receipt aL't'bLP- Commercial ❑ Pace Other no Seals intact; I'?— yBs ❑. None ❑ Other a of Ice:ciw'"' I Blue None logical Tis Frozen: ves too Comments: 6 1 039Z pue pate; 101; ubl is -NC s of ers examining r� f 9 Chain of Custody Present: s El No El NIA 1. Chain of Custody Filled Out: s ❑N❑ ❑NIA 2. Chain of Custod Relinquished: -s ❑N❑ ❑NIA 3, Sampler Name & Signature on COC: s El No ❑WA 4, Samples Arrived within Hold Time: s ❑No ❑N/A 5, Short Hold Time Analysis <72hr : LN e s -2<' ❑NIA 6. Rush Turn Around Time Requested: C as Le< ❑NIA 7, Sufficient Volume: s ❑No ❑NIA g. Correct Containers Used: -Pace Containers Used: s ❑No ❑NIA .s ❑NO ❑NIA 9. Containers Intact; .s ❑NU I:]NIA I, Filtered volume received for Dissolved tests ❑ s ONO 1 1 - Sample Labels match COC: -Includes date/time/ID/Analysis Matrix: s No ❑NSA 12. All containers needing preservatier•, nave been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exreptions: A, co+form, TOC, O&G, WI-DRO (water) s ONo El N/A s ❑Na ❑NIP s LINO 13. Initial when completed Lot # of added preservative Samples checked for dechlorination: C es ❑,NNQ ❑ . 14, Heads ace in VOA Vials ( >6mnt); ❑ es 1ar+o ❑:rI+A 15. Trip Blank Present: 21 Trip Blank Custody Seals Present Pace Trip Blank Lot # (ifpurchased): as El No ❑MA es ❑No ❑NIA 16, . Client Notification/ Resolution: Person Contacted: Comments/ Resolution: DatelTime: Field Data Require ? Y N Project Manager Review: Nate: Whenever there is a discrepancy affecting North Carolin Certification Office { i.e out of hold, incorrect preservative, out Date: will be sent to the NoWi F-ALLCO I it compliance samples. a copy of this for I temp, incorrect containers} Carolina DEHr•IR Pagg 38 o tov.3. 11 Septemoer2006 W18 49 I a7 A ceAnaIXical ° National Center for Testing & Innovation ANALYTICAL REPORT October 19, 2018 Pace Analytical - Atlanta, GA Sample Delivery Group: L1034440 Samples Received: 10/12/2018 Project Number: 2610392 Description: CMS VLandfill Report To: Betsy McDaniel 110 Technology Pky Peachtree Corners, GA 30092 Entire Report Reviewed By: nn i�,, � �vUL� Nancy McLain k Project Manager F Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. NIP J0 Awe- 411 1 - .090 11 !%1-1 '— k 39 of 49 TABLE OF CONTENTS ONE LAB. NATIONWIDE. Cp: Cover Page Tc: Table of Contents Ss: Sample Summary Cn: Case Narrative Sr: Sample Results 1304-MW33 L1034440-01 Qc: Quality Control Summary Chlorinated Acid Herbicides (GC) by Method 8151 GI: Glossary of Terms Al: Accreditations & Locations Sc: Sample Chain of Custody 1 Fn 2 3 4 FS5 5 [Cn] 6 6 Fr 7 RC6 9 F, rAl FSC Page 40 of 49 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Atlanta, GA 2610392 L1034440 10/19/18 11:27 2 of 10 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received date/time 1304-MW33 L1034440-01 GW 10/10/1815:42 10/12/1808:45 , C P Method Batch Dilution Preparation Analysis date/time date/time Chlorinated Acid Herbicides (GC) by Method 8151 WG1180951 5 10/15/18 09:57 10/18/18 00:54 Analyst ADF FTC M [Cn] FSr RC F, FAI FSC Page 41 of 49 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Atlanta, GA 2610392 L1034440 10/19/18 11:27 3 of 10 CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. VV VV� � �t La�'_ Nancy McLain Project Manager FP1 FTC FSS FSr FC-1 F, FAI FSC Page 42 of 49 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Atlanta, GA 2610392 L1034440 10/19/18 11:27 4 of 10 ONE LAB. NATIONWIDE. 1304-MW33 SAMPLE RESULTS - 01 Collected date/time: 10/10/18 15:42 L1034440 Chlorinated Acid Herbicides (GC) by Method 8151 Result Analyte ug/I 2,4-D IJ 2,4,5-T J 2,4,5-TP (Silvex) IJ (S)2,4-Dich/oropheny/Acetic 66.6 Acid Qualifier MDL RDL Dilution Analysis ug/I ug/I date / time 3.72 10.0 5 10/18/2018 00:54 4.22 10.0 5 10/18/2018 00:54 4.23 10.0 5 10/18/2018 00:54 14.0-158 1011812018 00:54 Batch WG1180951 WG1180951 WG1180951 WG1180951 Page 43 of 49 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Atlanta, GA 2610392 L1034440 10/19/18 11:27 5 of 10 WG1180951 Chlorinated Acid Herbicides (GC) by Method 8151 Method Blank (MB) (MB) R3351980-3 10/17/18 21:30 MB Result Analyte ug/I 2,4-D U 2,4,5-T U 2,4,5-TP (Silvex) U (S)2,4-Dichloropheny/Acetic 71.6 Acid MB Qualifier MB MDL MB RDL ug/I ug/I 0.744 2.00 0.843 2.00 0.845 2.00 14.0-158 QUALITY CONTROL SUMMARY L1034440-01 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3351980-1 10/17/18 21:03 • (LCSD) R3351980-2 10/17/18 21:17 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits Analyte ug/I ug/I ug/I % % % 2,4-D 5.00 3.84 4.01 76.8 80.2 50.0-120 2,4,5-T 5.00 4.31 4.52 86.2 90.4 54.0-120 2,4,5-TP (Silvex) 5.00 4.03 4.22 80.6 84.4 50.0-125 (S)2,4-Dichloropheny/Acetic 82.0 84.2 14.0-158 Acid LCS Qualifier LCSD Qualifier RPD RPD Limits 4.33 20 4.76 20 4.61 20 ONE LAB. NATIONWIDE. FP1 FTC FSS 4 Cn FSr �GI FAI FSC ACCOUNT: Pace Analytical - Atlanta, GA PROJECT: 2610392 SDG: DATE/TIME: L1034440 10/19/18 11:27 Page 44 of 49 PAGE: 6 of10 GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report ONE LAB. NATIONWIDE. The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Abbreviations and Definitions CP IP FTC MDL Method Detection Limit. RDL Reported Detection Limit. FSS Rec. Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. [Cn] Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. FSr U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes Fc reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or FAI duplicated within these ranges. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and FSC potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG. Page 45 of 49 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Atlanta, GA 2610392 L1034440 10/19/18 11:27 7 of 10 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1 turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z Tc State Accreditations f—� Alabama 40660 Nebraska _ NE-OS-15-05 SS Alaska 17-026 Nevada TN-03-2002-34 Arizona AZO612 New Hampshire 2975 Arkansas 88-0469 New Jersey_NELAP TNO02 C n California 2932 New Mexico n/a Colorado TN00003 New York 11742 s Connecticut PH-0197 North Carolina Env375 Sr Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina' 41 Georgia' 923 North Dakota R-140 RC Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 G Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky76 90010 South Carolina 84004 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee' 4 2006 Louisiana' LA180010 Texas T 104704245-17-14 [SC Maine TN0002 Texas' LABO152 Maryland 324 Utah Massachusetts M-TNO03 Vermont Michigan 9958 Virginia Minnesota 047-999-395 Washington Mississippi TN00003 West Virginia Missouri 340 Wisconsin Montana CERT0086 Wyoming Third Party Federal Accreditations A21LA — ISO 17025 1461.01 AIHA-LAP,LLC EMLAP A21LA — ISO 17025 5 1461.02 DOD Canada 1461.01 USDA EPA—Crypto TN00003 ' Drinking Water 'Underground Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Our Locations TN00003 VT2006 460132 C847 233 9980939910 A2LA 100789 1461.01 P330-15-00234 Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. WA MT NO OR MN T ID t SD WI NY WY MI NV t NE IA OH PA T f IL Ills WV vA UT T CA�� T KS MO KY N NM O� AR `7T Sc T MS AL GA T TX * LA T AK q FL wo HI ACCOUNT: PROJECT: SDG: DATE/TIME: Pace Analytical - Atlanta, GA 2610392 L1034440 10/19/18 11:27 ME Page 46 of 49 PAGE: 8 of 10 Chain Of CLIstodyCeAtry �.r r-W'11 rcrn Workordet; 2510392 VVorkorder Name. CMS V LafldFill Rcpart+G yaVcrto StFhcor<tracaTp Betsy h1Uatsiel P ace Analytical All2nta 110 Te&flolagy Parkway Feachtree Comers, GA 30092 Phone (770)734-4200 email- het5y.rncdanief@p&celahs.com Slate of Sample Origin; No }w(" 1 Simple In 1 13p4MV433 2 3 4 Transfers kR.1 a I oo ler 31'M l)t Results Requested By_ 1012912018 Rna nested A na tyz if. e Prmarved C ntafners Cpfr9GL 4 UQtafitl119e Lab III Matrix y d 14+1012018 15-42 �5 i03920G1- 1^+�te; � By Carolina sample on Recelt ►4' Custody Seal Y or N Received un Ice CY2 a N RAD S CREEN.. 4,S CQMMCn%S S 0 LAS USE ONLY 5 k. o1 or N 1=MT-ALL-C-002rew 00 2+4MaMn2W2 Page 1 or I Thvr!&dBy, October 11. 2G18 4 38.19 PM Page 47 of 49 Pa ce An • or Testi ng & I n n • Cooler Receipt• cliew. PwaKtrw 6.wler R Cce ivcLI10pened On I OOLI$ Temperaturu� Received By: malik tfRial'e Signature: TrbJ0 Receipt Check List NP Yes No COC Seal Present f Intact? COC Signed j Accurate?" Bottles arrive intact? Correct bottles used? { sufficient volume sent? If Applicable VOA Zero head -,pace? Preservation Correct J Checked? Page 48 of 49 L b 1U 4° 4° 0 -o -o , �* 2 G o 0 _ y c a� W F- 7 Q 4. 0 4. 0 0 to c cl 0 0 CL NNE U U i-1 3 CO 6 r � w .d N cn O O U O k kLA — `� o (UCO �33a II U U II 4-1\y II QUv> ? ; w ru= ` 33��i o S C7 II 0 0 on �S�jQU II ^ c`�ntoM U -00 �3 0 r E s0 E �R2 0=c 3u o»=C13 O E l3 0 C "C7 0L1 N 7 03UU cd cd U > E 0 U—C7 r.r w = co a 0 z �" --„ a�'33 c Oj w3 m3: cO - !� �0 i� e cl �� S-F� . V J tv .r CJ G� , v1 r C CQ C 0tA cl 0 cJ j%! cc�6 c c� O b` 0 d z o o 44 � Q o co � w .. .. 0 U o.�p r. p a > z Ea p �; aD rn m a. 7--. .Q �I0 Page 49 of 49 lacieAnalXical" www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 October 29, 2018 Environmental Manager BFI Waste Systems of North America. LLC 5105 Moreland Road Concord, NC 28027 RE: Project: Untreated Leachate WW Pace Project No.: 2610403 Dear Environmental Manager: Enclosed are the analytical results for sample(s) received by the laboratory on October 11, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Betsy McDaniel betsy.mcdaniel@pacelabs.com (770)734-4200 Project Manager Enclosures cc: Database Manager REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 CERTIFICATIONS Project: Untreated Leachate WW Pace Project No.: 2610403 Atlanta Certification IDs 110 Technology Parkway Peachtree Corners, GA 30092 North Carolina Certification #: 381 Florida DOH Certification #: E87315 South Carolina Certification #: 98011001 Georgia DW Inorganics Certification #: 812 Texas Certification #: T104704397-08-TX Georgia DW Microbiology Certification #: 812 Virginia Certification #: 460204 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 SAMPLE SUMMARY Project: Untreated Leachate WW Pace Project No.: 2610403 Lab ID Sample ID Matrix Date Collected Date Received 2610403001 Untreated Leachate Water 10/11/18 07:42 10/11/18 13:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 SAMPLE ANALYTE COUNT Project: Untreated Leachate WW Pace Project No.: 2610403 Lab ID Sample ID Method Analysts Analytes Reported 2610403001 Untreated Leachate EPA6020B CSW 15 EPA 8260E LIH 51 EPA410.4 RNB 1 SM 4500-P MWB 1 SM 4500-P MWB 1 SM 5210B RNB 1 EPA 9056A RLC 1 EPA 9056A MWB 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Untreated Leachate WW Pace Project No.: 2610403 Sample: Untreated Leachate Lab ID: 2610403001 Collected: 10/11/18 07:42 Received: 10/11/18 13:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual Field Data Collected By Field pH Field Temperature Field Specific Conductance 6020B MET ICPMS Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Nickel Selenium Silver Thallium Vanadium Zinc 8260B MSV Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3- chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2- butene Date: 10/29/2018 11:23 AM Analytical Method SF 1 10/16/18 10:50 8.77 Std. Units 1 10/16/18 10:50 25.2 deg C 1 10/16/18 10:50 1387 umhos/c 1 10/16/18 10:50 m Analytical Method: EPA 6020B Preparation Method: EPA 3005A 111 ug/L 30.0 3.9 5 10/18/1810:32 10/22/1819:44 7440-36-0 331 ug/L 50.0 2.8 5 10/18/1810:32 10/22/1819:44 7440-38-2 676 ug/L 500 3.9 5 10/18/1810:32 10/22/1819:44 7440-39-3 ND ug/L 5.0 0.25 5 10/18/1810:32 10/22/1819:44 7440-41-7 D3 ND ug/L 5.0 0.46 5 10/18/1810:32 10/22/1819:44 7440-43-9 D3 70.5 ug/L 50.0 7.8 5 10/18/1810:32 10/22/1819:44 7440-47-3 26.4J ug/L 50.0 2.6 5 10/18/1810:32 10/22/1819:44 7440-48-4 D3 6.8J ug/L 50.0 6.4 5 10/18/1810:32 10/22/1819:44 7440-50-8 D3 6.4J ug/L 50.0 1.4 5 10/18/1810:32 10/22/1819:44 7439-92-1 D3 179J ug/L 250 4.8 5 10/18/1810:32 10/22/1819:44 7440-02-0 ND ug/L 50.0 6.8 5 10/18/1810:32 10/22/1819:44 7782-49-2 D3 ND ug/L 50.0 4.8 5 10/18/1810:32 10/22/1819:44 7440-22-4 D3 ND ug/L 27.5 0.71 5 10/18/1810:32 10/22/1819:44 7440-28-0 D3 16.OJ ug/L 125 9.7 5 10/18/1810:32 10/22/1819:44 7440-62-2 D3 189 ug/L 50.0 10.3 5 10/18/1810:32 10/22/1819:44 7440-66-6 Analytical Method: EPA 8260E 112J ug/L 1000 82.0 10 10/19/18 00:03 67-64-1 ND ug/L 2000 25.0 10 10/19/18 00:03 107-13-1 ND ug/L 10.0 2.0 10 10/19/18 00:03 71-43-2 ND ug/L 30.0 5.0 10 10/19/18 00:03 74-97-5 ND ug/L 10.0 3.6 10 10/19/18 00:03 75-27-4 ND ug/L 30.0 5.5 10 10/19/18 00:03 75-25-2 63.OJ ug/L 100 9.5 10 10/19/18 00:03 74-83-9 ND ug/L 1000 32.0 10 10/19/18 00:03 78-93-3 ND ug/L 1000 7.9 10 10/19/18 00:03 75-15-0 ND ug/L 10.0 4.2 10 10/19/18 00:03 56-23-5 ND ug/L 30.0 5.3 10 10/19/18 00:03 108-90-7 ND ug/L 100 5.2 10 10/19/18 00:03 75-00-3 ND ug/L 50.0 5.8 10 10/19/18 00:03 67-66-3 25.4 ug/L 10.0 3.8 10 10/19/18 00:03 74-87-3 ND ug/L 130 5.5 10 10/19/18 00:03 96-12-8 ND ug/L 10.0 3.1 10 10/19/18 00:03 124-48-1 ND ug/L 20.0 2.8 10 10/19/18 00:03 106-93-4 ND ug/L 100 6.2 10 10/19/18 00:03 74-95-3 ND ug/L 50.0 4.9 10 10/19/18 00:03 95-50-1 ND ug/L 10.0 5.8 10 10/19/18 00:03 106-46-7 ND ug/L 1000 16.0 10 10/19/18 00:03 110-57-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Untreated Leachate WW Pace Project No.: 2610403 Sample: Untreated Leachate Lab ID: 2610403001 Collected: 10/11/18 07:42 Received: 10/11/18 13:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 8260B MSV Analytical Method: EPA 8260E 1,1-Dichloroethane ND ug/L 50.0 4.1 10 10/19/18 00:03 75-34-3 1,2-Dichloroethane ND ug/L 10.0 6.7 10 10/19/18 00:03 107-06-2 1,1-Dichloroethene ND ug/L 50.0 7.2 10 10/19/18 00:03 75-35-4 cis-1,2-Dichloroethene ND ug/L 50.0 6.6 10 10/19/18 00:03 156-59-2 trans-1,2-Dichloroethene ND ug/L 50.0 4.6 10 10/19/18 00:03 156-60-5 1,2-Dichloropropane ND ug/L 10.0 6.0 10 10/19/18 00:03 78-87-5 cis-1,3-Dichloropropene ND ug/L 10.0 2.2 10 10/19/18 00:03 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 10.0 3.0 10 10/19/18 00:03 10061-02-6 Ethylbenzene ND ug/L 10.0 4.5 10 10/19/18 00:03 100-41-4 2-Hexanone ND ug/L 500 8.9 10 10/19/18 00:03 591-78-6 lodomethane 67.6J ug/L 100 31.0 10 10/19/18 00:03 74-88-4 Methylene Chloride ND ug/L 10.0 5.0 10 10/19/18 00:03 75-09-2 4-Methyl-2-pentanone ND ug/L 500 8.6 10 10/19/18 00:03 108-10-1 (MIBK) Styrene ND ug/L 10.0 5.0 10 10/19/18 00:03 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 50.0 3.2 10 10/19/18 00:03 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 10.0 5.3 10 10/19/18 00:03 79-34-5 Tetrachloroethene ND ug/L 10.0 7.8 10 10/19/18 00:03 127-18-4 Toluene ND ug/L 10.0 3.1 10 10/19/18 00:03 108-88-3 1,1,1-Trichloroethane ND ug/L 10.0 3.8 10 10/19/18 00:03 71-55-6 1,1,2-Trichloroethane ND ug/L 10.0 5.9 10 10/19/18 00:03 79-00-5 Trichloroethene ND ug/L 10.0 3.4 10 10/19/18 00:03 79-01-6 Trichlorofluoromethane ND ug/L 10.0 5.1 10 10/19/18 00:03 75-69-4 1,2,3-Trichloropropane ND ug/L 10.0 4.6 10 10/19/18 00:03 96-18-4 Vinyl acetate ND ug/L 500 4.2 10 10/19/18 00:03 108-05-4 Vinyl chloride ND ug/L 10.0 6.0 10 10/19/18 00:03 75-01-4 Xylene (Total) ND ug/L 40.0 14.6 10 10/19/18 00:03 1330-20-7 Surrogates 1,2-Dichloroethane-d4 (S) 101 %. 81-119 10 10/19/18 00:03 17060-07-0 Dibromofluoromethane (S) 104 %. 82-114 10 10/19/18 00:03 1868-53-7 4-Bromofluorobenzene (S) 101 %. 82-120 10 10/19/18 00:03 460-00-4 Toluene-d8 (S) 99 %. 82-109 10 10/19/18 00:03 2037-26-5 410.4 COD Analytical Method: EPA 410.4 Preparation Method: EPA 410.4 Chemical Oxygen 1370000 ug/L 10000 10000 1 10/18/1815:30 10/18/1817:46 Demand 450OPE Total Phosphorus Analytical Method: SM 4500-P Preparation Method: SM 4500-P Phosphorus 1810 ug/L 220 1.1 10/18/1810:40 10/18/1818:36 7723-14-0 M1 450OPE Ortho Phosphorus Analytical Method: SM 4500-P Orthophosphate as P 81.5J ug/L 100 5 10/12/18 17:23 5210B BOD, 5 day Analytical Method: SM 5210B Preparation Method: SM 5210B BOD, 5 day 194000 ug/L 81000 81000 60 10/12/18 14:00 10/17/18 10:47 R6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/29/2018 11:23 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 ANALYTICAL RESULTS Project: Untreated Leachate WW Pace Project No.: 2610403 Sample: Untreated Leachate Lab ID: 2610403001 Collected: 10/11/18 07:42 Received: 10/11/18 13:00 Matrix: Water Report Reg. Parameters Results Units Limit MDL Limit DF Prepared Analyzed CAS No. Qual 9056 IC Anions 48hr Analytical Method: EPA 9056A Nitrate as N 142 ug/L 50.0 5.0 1 10/12/18 14:07 14797-55-8 9056 IC Anions Analytical Method: EPA 9056A Sulfate 66200 ug/L 50000 170 10 10/24/18 08:01 14808-79-8 Date: 10/29/2018 11:23 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Untreated Leachate WW Pace Project No.: 2610403 QC Batch: 15602 Analysis Method: EPA 6020B QC Batch Method: EPA 3005A Analysis Description: 6020E MET Associated Lab Samples: 2610403001 METHOD BLANK: 69649 Associated Lab Samples: 2610403001 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers Antimony ug/L ND 6.0 0.78 10/22/1817:49 Arsenic ug/L ND 10.0 0.57 10/22/1817:49 Barium ug/L ND 100 0.78 10/22/1817:49 Beryllium ug/L ND 1.0 0.050 10/22/1817:49 Cadmium ug/L ND 1.0 0.093 10/22/1817:49 Chromium ug/L ND 10.0 1.6 10/22/1817:49 Cobalt ug/L ND 10.0 0.52 10/22/1817:49 Copper ug/L ND 10.0 1.3 10/22/1817:49 Lead ug/L ND 10.0 0.27 10/22/1817:49 Nickel ug/L ND 50.0 0.95 10/22/1817:49 Selenium ug/L ND 10.0 1.4 10/22/1817:49 Silver ug/L ND 10.0 0.95 10/22/1817:49 Thallium ug/L ND 5.5 0.14 10/22/1817:49 Vanadium ug/L ND 25.0 1.9 10/22/1817:49 Zinc ug/L 2.8J 10.0 2.1 10/22/1817:49 LABORATORY CONTROL SAMPLE: 69650 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Antimony ug/L 100 102 102 80-120 Arsenic ug/L 100 101 101 80-120 Barium ug/L 100 100 100 80-120 Beryllium ug/L 100 104 104 80-120 Cadmium ug/L 100 99.0 99 80-120 Chromium ug/L 100 103 103 80-120 Cobalt ug/L 100 103 103 80-120 Copper ug/L 100 104 104 80-120 Lead ug/L 100 100 100 80-120 Nickel ug/L 100 101 101 80-120 Selenium ug/L 100 103 103 80-120 Silver ug/L 100 102 102 80-120 Thallium ug/L 100 99.9 100 80-120 Vanadium ug/L 100 106 106 80-120 Zinc ug/L 100 104 104 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/29/2018 11:23 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Untreated Leachate WW Pace Project No.: 2610403 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 69651 69652 MS MSD 2610392002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 100 100 103 101 103 101 75-125 2 20 Arsenic ug/L ND 100 100 101 96.7 100 96 75-125 4 20 Barium ug/L 91.2J 100 100 193 193 101 102 75-125 0 20 Beryllium ug/L 0.065J 100 100 101 103 101 103 75-125 2 20 Cadmium ug/L 0.21J 100 100 99.6 99.9 99 100 75-125 0 20 Chromium ug/L 2.3J 100 100 106 102 103 100 75-125 3 20 Cobalt ug/L 0.77J 100 100 102 98.3 101 97 75-125 4 20 Copper ug/L 9.6J 100 100 114 111 104 101 75-125 2 20 Lead ug/L 0.33J 100 100 98.0 95.6 98 95 75-125 2 20 Nickel ug/L 3AJ 100 100 103 102 100 98 75-125 1 20 Selenium ug/L ND 100 100 104 103 103 101 75-125 1 20 Silver ug/L ND 100 100 98.4 99.6 98 100 75-125 1 20 Thallium ug/L ND 100 100 97.4 95.3 97 95 75-125 2 20 Vanadium ug/L ND 100 100 109 104 107 102 75-125 4 20 Zinc ug/L 12.7 100 100 112 111 99 98 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/29/2018 11:23 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Untreated Leachate WW Pace Project No.: 2610403 QC Batch: 15591 Analysis Method: EPA 8260B QC Batch Method: EPA 8260E Analysis Description: 8260E MSV Associated Lab Samples: 2610403001 METHOD BLANK: 69612 Associated Lab Samples: 2610403001 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 5.0 0.32 10/18/18 15:35 1,1,1-Trichloroethane ug/L ND 1.0 0.38 10/18/18 15:35 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.53 10/18/18 15:35 1,1,2-Trichloroethane ug/L ND 1.0 0.59 10/18/18 15:35 1,1-Dichloroethane ug/L ND 5.0 0.41 10/18/18 15:35 1,1-Dichloroethene ug/L ND 5.0 0.72 10/18/18 15:35 1,2,3-Trichloropropane ug/L ND 1.0 0.46 10/18/18 15:35 1,2-Dibromo-3-chloropropane ug/L ND 13.0 0.55 10/18/18 15:35 1,2-Dibromoethane (EDB) ug/L ND 2.0 0.28 10/18/18 15:35 1,2-Dichlorobenzene ug/L ND 5.0 0.49 10/18/18 15:35 1,2-Dichloroethane ug/L ND 1.0 0.67 10/18/18 15:35 1,2-Dichloropropane ug/L ND 1.0 0.60 10/18/18 15:35 1,4-Dichlorobenzene ug/L ND 1.0 0.58 10/18/18 15:35 2-Butanone (MEK) ug/L ND 100 3.2 10/18/18 15:35 2-Hexanone ug/L ND 50.0 0.89 10/18/18 15:35 4-Methyl-2-pentanone (MIBK) ug/L ND 50.0 0.86 10/18/18 15:35 Acetone ug/L ND 100 8.2 10/18/18 15:35 Acrylonitrile ug/L ND 200 2.5 10/18/18 15:35 Benzene ug/L ND 1.0 0.20 10/18/18 15:35 Bromochloromethane ug/L ND 3.0 0.50 10/18/18 15:35 Bromodichloromethane ug/L ND 1.0 0.36 10/18/18 15:35 Bromoform ug/L ND 3.0 0.55 10/18/18 15:35 Bromomethane ug/L ND 10.0 0.95 10/18/18 15:35 Carbon disulfide ug/L ND 100 0.79 10/18/18 15:35 Carbon tetrachloride ug/L ND 1.0 0.42 10/18/18 15:35 Chlorobenzene ug/L ND 3.0 0.53 10/18/18 15:35 Chloroethane ug/L ND 10.0 0.52 10/18/18 15:35 Chloroform ug/L ND 5.0 0.58 10/18/18 15:35 Chloromethane ug/L ND 1.0 0.38 10/18/18 15:35 cis-1,2-Dichloroethene ug/L ND 5.0 0.66 10/18/18 15:35 cis-1,3-Dichloropropene ug/L ND 1.0 0.22 10/18/18 15:35 Dibromochloromethane ug/L ND 1.0 0.31 10/18/18 15:35 Dibromomethane ug/L ND 10.0 0.62 10/18/18 15:35 Ethylbenzene ug/L ND 1.0 0.45 10/18/18 15:35 lodomethane ug/L ND 10.0 3.1 10/18/18 15:35 Methylene Chloride ug/L ND 1.0 0.50 10/18/18 15:35 Styrene ug/L ND 1.0 0.50 10/18/18 15:35 Tetrachloroethene ug/L ND 1.0 0.78 10/18/18 15:35 Toluene ug/L ND 1.0 0.31 10/18/18 15:35 trans-1,2-Dichloroethene ug/L ND 5.0 0.46 10/18/18 15:35 trans- 1,3-Dichloropropene ug/L ND 1.0 0.30 10/18/18 15:35 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/29/2018 11:23 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Untreated Leachate WW Pace Project No.: 2610403 METHOD BLANK: 69612 Associated Lab Samples: 2610403001 Parameter Units Matrix: Blank Result Water Reporting Limit MDL trans-1,4-Dichloro-2-butene ug/L ND 100 Trichloroethene ug/L ND 1.0 Trichlorofluoromethane ug/L ND 1.0 Vinyl acetate ug/L ND 50.0 Vinyl chloride ug/L ND 1.0 Xylene (Total) ug/L ND 4.0 1,2-Dichloroethane-d4 (S) %. 99 81-119 4-Bromofluorobenzene (S) %. 105 82-120 Dibromofluoromethane (S) %. 98 82-114 Toluene-d8 (S) %. 100 82-109 Analyzed 1.6 10/18/18 15:35 0.34 10/18/18 15:35 0.51 10/18/18 15:35 0.42 10/18/18 15:35 0.60 10/18/18 15:35 1.5 10/18/18 15:35 10/18/18 15:35 10/18/18 15:35 10/18/18 15:35 10/18/18 15:35 LABORATORY CONTROL SAMPLE: Parameter 69613 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 47.8 96 68-137 1,1,1-Trichloroethane ug/L 50 51.1 102 72-134 1,1,2,2-Tetrachloroethane ug/L 50 50.4 101 51-158 1,1,2-Trichloroethane ug/L 50 55.7 111 78-131 1,1-Dichloroethane ug/L 50 53.4 107 69-151 1,1-Dichloroethene ug/L 50 51.6 103 64-158 1,2,3-Trichloropropane ug/L 50 46.0 92 78-133 1,2-Dibromo-3-chloropropane ug/L 50 47.5 95 58-124 1,2-Dibromoethane (EDB) ug/L 50 50.8 102 71-134 1,2-Dichlorobenzene ug/L 50 54.5 109 70-135 1,2-Dichloroethane ug/L 50 52.7 105 72-129 1,2-Dichloropropane ug/L 50 55.9 112 64-135 1,4-Dichlorobenzene ug/L 50 50.2 100 70-131 2-Butanone (MEK) ug/L 100 74.1J 74 52-143 2-Hexanone ug/L 100 81.2 81 61-136 4-Methyl-2-pentanone (MIBK) ug/L 100 90.5 91 71-129 Acetone ug/L 100 74.8J 75 48-224 Acrylonitrile ug/L 200 177J 88 66-154 Benzene ug/L 50 53.8 108 68-132 Bromochloromethane ug/L 50 53.0 106 73-133 Bromodichloromethane ug/L 50 46.5 93 67-121 Bromoform ug/L 50 43.8 88 57-125 Bromomethane ug/L 50 37.7 75 35-156 Carbon disulfide ug/L 100 89.OJ 89 47-141 Carbon tetrachloride ug/L 50 50.1 100 66-122 Chlorobenzene ug/L 50 52.3 105 71-126 Chloroethane ug/L 50 41.1 82 43-143 Chloroform ug/L 50 53.6 107 71-136 Chloromethane ug/L 50 45.2 90 47-123 cis-1,2-Dichloroethene ug/L 50 54.9 110 74-131 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/29/2018 11:23 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Untreated Leachate WW Pace Project No.: 2610403 LABORATORY CONTROL SAMPLE: 69613 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers cis-1,3-Dichloropropene ug/L 50 49.3 99 78-120 Dibromochloromethane ug/L 50 46.1 92 65-115 Dibromomethane ug/L 50 56.9 114 79-129 Ethylbenzene ug/L 50 54.0 108 68-129 lodomethane ug/L 100 86.8 87 49-154 Methylene Chloride ug/L 50 48.1 96 61-147 Styrene ug/L 50 50.6 101 77-128 Tetrachloroethene ug/L 50 39.2 78 51-139 Toluene ug/L 50 55.9 112 60-133 trans-1,2-Dichloroethene ug/L 50 50.5 101 69-144 trans- 1,3-Dichloropropene ug/L 50 46.0 92 74-128 trans-1,4-Dichloro-2-butene ug/L 100 91.11 91 61-139 Trichloroethene ug/L 50 50.1 100 73-126 Trichlorofluoromethane ug/L 50 52.0 104 55-132 Vinyl acetate ug/L 50 46.8J 94 52-141 Vinyl chloride ug/L 50 46.4 93 50-133 Xylene (Total) ug/L 150 152 101 78-132 1,2-Dichloroethane-d4 (S) %. 99 81-119 4-Bromofluorobenzene (S) %. 102 82-120 Dibromofluoromethane (S) %. 105 82-114 Toluene-d8 (S) %. 99 82-109 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 69614 69615 MS MSD 2610406011 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 50 50 47.5 44.6 95 89 68-137 6 11 1,1,1-Trichloroethane ug/L ND 50 50 56.6 54.0 113 108 66-142 5 11 1,1,2,2-Tetrachloroethane ug/L ND 50 50 46.7 44.9 93 90 39-171 4 13 1,1,2-Trichloroethane ug/L ND 50 50 53.2 49.4 106 99 73-136 8 12 1,1-Dichloroethane ug/L 0.98J 50 50 57.0 53.5 112 105 66-155 6 15 1,1-Dichloroethene ug/L ND 50 50 59.4 58.3 119 117 33-181 2 34 1,2,3-Trichloropropane ug/L ND 50 50 41.9 39.7 84 79 78-133 5 14 1,2-Dibromo-3- ug/L ND 50 50 39.4 39.9 79 80 58-124 1 15 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 50 50 48.4 44.9 97 90 71-134 8 12 1,2-Dichlorobenzene ug/L ND 50 50 51.1 49.4 102 99 69-135 3 10 1,2-Dichloroethane ug/L ND 50 50 54.4 49.3 109 99 36-159 10 10 1,2-Dichloropropane ug/L ND 50 50 52.5 49.8 105 100 68-132 5 11 1,4-Dichlorobenzene ug/L 2.5J 50 50 50.8 48.3 97 92 49-153 5 9 2-Butanone (MEK) ug/L ND 100 100 71.8J 66.3J 72 66 10-189 8 23 2-Hexanone ug/L ND 100 100 69.6 67.7 70 68 40-135 3 18 4-Methyl-2-pentanone ug/L ND 100 100 76.6 70.6 77 71 30-177 8 10 (MIBK) Acetone ug/L ND 100 100 64.3J 62.5J 64 63 44-223 3 14 Acrylonitrile ug/L ND 200 200 167J 155J 84 77 13-189 8 12 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/29/2018 11:23 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Untreated Leachate WW Pace Project No.: 2610403 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 69614 69615 MS MSD 2610406011 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Benzene ug/L 1.7J 50 50 57.3 53.4 111 104 66-139 7 10 Bromochloromethane ug/L ND 50 50 52.4 ND 105 0 73-133 13 M1 Bromodichloromethane ug/L ND 50 50 46.0 43.2 92 86 57-120 6 13 Bromoform ug/L ND 50 50 41.6 39.0 83 78 48-128 6 13 Bromomethane ug/L ND 50 50 38.6 38.6 77 77 10-187 0 32 Carbon disulfide ug/L ND 100 100 99.1J 95.2J 99 95 47-141 4 322 Carbon tetrachloride ug/L ND 50 50 61.0 57.3 122 115 58-127 6 14 Chlorobenzene ug/L 0.55J 50 50 52.8 49.2 105 97 63-137 7 10 Chloroethane ug/L ND 50 50 45.8 44.3 92 89 52-146 3 16 Chloroform ug/L ND 50 50 55.4 52.1 111 104 74-137 6 9 Chloromethane ug/L ND 50 50 49.5 47.8 99 96 41-127 3 10 cis-1,2-Dichloroethene ug/L 1.8J 50 50 58.3 56.9 113 110 71-138 2 16 cis-1,3-Dichloropropene ug/L ND 50 50 42.2 40.3 84 81 32-145 5 12 Dibromochloromethane ug/L ND 50 50 44.0 41.1 88 82 52-116 7 13 Dibromomethane ug/L ND 50 50 52.0 49.6 104 99 79-129 5 14 Ethylbenzene ug/L ND 50 50 55.8 52.2 112 104 31-174 7 10 lodomethane ug/L ND 100 100 54.7 67.9 55 68 49-154 21 30 Methylene Chloride ug/L 14.5 50 50 61.0 57.2 93 85 61-146 6 15 Styrene ug/L ND 50 50 48.9 46.0 98 92 77-128 6 14 Tetrachloroethene ug/L ND 50 50 41.7 39.3 83 79 36-155 6 14 Toluene ug/L ND 50 50 56.6 52.0 113 104 52-146 9 11 trans-1,2-Dichloroethene ug/L ND 50 50 53.6 50.5 107 101 61-152 6 14 trans-1,3-Dichloropropene ug/L ND 50 50 40.5 38.8 81 78 37-146 4 12 trans-1,4-Dichloro-2-butene ug/L ND 100 100 82.1J 78AJ 82 78 61-139 5 12 Trichloroethene ug/L ND 50 50 52.0 47.7 104 95 61-141 9 12 Trichlorofluoromethane ug/L 1.2J 50 50 70.2 67.4 138 132 51-141 4 13 Vinyl acetate ug/L ND 50 50 51.5 49.8J 103 100 52-141 3 14 Vinyl chloride ug/L ND 50 50 54.6 51.9 109 104 22-156 5 26 Xylene (Total) ug/L 5.4 150 150 156 145 100 93 78-132 7 7 1,2-Dichloroethane-d4 (S) %. 104 101 81-119 4-Bromofluorobenzene (S) %. 101 100 82-120 Dibromofluoromethane (S) %. 109 105 82-114 Toluene-d8 (S) %. 98 97 82-109 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/29/2018 11:23 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Untreated Leachate WW Pace Project No.: 2610403 QC Batch: 15640 Analysis Method: EPA 410.4 QC Batch Method: EPA 410.4 Analysis Description: 410.4 COD Associated Lab Samples: 2610403001 METHOD BLANK: 69776 Matrix: Water Associated Lab Samples: 2610403001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Chemical Oxygen Demand ug/L ND 10000 10000 10/18/18 17:42 LABORATORY CONTROL SAMPLE: 69777 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand ug/L 200000 195000 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 69780 69781 MS MSD 2610441001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chemical Oxygen Demand ug/L 15000 5000000 5000000 2000000 1980000 99 96 90-110 1 10 mg/L 0 0 MATRIX SPIKE SAMPLE: 69783 2610361001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand ug/L 2030 mg/L 2000000 4130000 105 90-110 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/29/2018 11:23 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Untreated Leachate WW Pace Project No.: 2610403 QC Batch: 15598 Analysis Method: SM 4500-P QC Batch Method: SM 4500-P Analysis Description: 450OPE Total Phosphorus Associated Lab Samples: 2610403001 METHOD BLANK: 69637 Matrix: Water Associated Lab Samples: 2610403001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Phosphorus ug/L ND 20.0 10/18/1818:30 LABORATORY CONTROL SAMPLE: 69638 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus ug/L 100 91.2 91 89-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 69639 69640 MS MSD 2610403001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Phosphorus ug/L 1810 1000 1000 2950 3060 114 125 73-117 4 19 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/29/2018 11:23 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Untreated Leachate WW Pace Project No.: 2610403 QC Batch: 15333 Analysis Method: SM 4500-P QC Batch Method: SM 4500-P Analysis Description: 450OPE Ortho Phosphorus Associated Lab Samples: 2610403001 METHOD BLANK: 68611 Matrix: Water Associated Lab Samples: 2610403001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Orthophosphate as P ug/L ND 20.0 10/12/18 17:21 LABORATORY CONTROL SAMPLE: 68612 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Orthophosphate as P ug/L 500 538 108 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 68613 68614 MS MSD 2610421001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Orthophosphate as P ug/L 0.15 mg/L 500 500 658 690 103 109 87-111 5 5 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/29/2018 11:23 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Untreated Leachate WW Pace Project No.: 2610403 QC Batch: 15332 Analysis Method: SM 5210B QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day Associated Lab Samples: 2610403001 METHOD BLANK: 68606 Matrix: Water Associated Lab Samples: 2610403001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers BOD, 5 day ug/L ND 2000 2000 10/17/18 10:44 LABORATORY CONTROL SAMPLE: 68608 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day ug/L 198000 194000 98 85-115 SAMPLE DUPLICATE: 68609 2610403001 Dup Max Parameter Units Result Result RPD RPD Qualifiers BOD, 5 day ug/L 194000 201000 4 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/29/2018 11:23 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Untreated Leachate WW Pace Project No.: 2610403 QC Batch: 15253 Analysis Method: EPA 9056A QC Batch Method: EPA 9056A Analysis Description: 9056 IC Anions Associated Lab Samples: 2610403001 METHOD BLANK: 68282 Matrix: Water Associated Lab Samples: 2610403001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Nitrate as N ug/L ND 50.0 5.0 10/12/18 13:21 LABORATORY CONTROL SAMPLE: 68283 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrate as N ug/L 10000 10400 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 68284 68285 MS MSD 2610403001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Nitrate as N ug/L 142 10000 10000 10600 10700 105 105 90-110 0 15 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/29/2018 11:23 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA Project: Untreated Leachate WW Pace Project No.: 2610403 QC Batch: 15515 Analysis Method: EPA 9056A QC Batch Method: EPA 9056A Analysis Description: 9056 IC Anions Associated Lab Samples: 2610403001 METHOD BLANK: 69294 Matrix: Water Associated Lab Samples: 2610403001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfate ug/L ND 5000 17.0 10/17/18 20:32 LABORATORY CONTROL SAMPLE: 69295 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate ug/L 10000 10900 109 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 69296 69297 MS MSD 2610453015 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 6.2 mg/L 10000 10000 16800 16900 106 106 90-110 0 15 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/29/2018 11:23 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 24 Pace Analytical Services, LLC aceAnalXica! � 110 Technology Parkway Peachtree Corners, GA 30092 www.pacelabs.com (770)734-4200 QUALIFIERS Project: Untreated Leachate WW Pace Project No.: 2610403 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. ANALYTE QUALIFIERS D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R6 The RPD between valid sample dilutions exceeded 30%. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/29/2018 11:23 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 24 aceAnalXical www.pacelabs.com Pace Analytical Services, LLC 110 Technology Parkway Peachtree Corners, GA 30092 (770)734-4200 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Untreated Leachate WW Pace Project No.: 2610403 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 2610403001 Untreated Leachate 15449 2610403001 Untreated Leachate EPA 3005A 15602 EPA 6020B 2610403001 Untreated Leachate EPA8260B 15591 2610403001 Untreated Leachate EPA 410.4 15640 EPA 410.4 2610403001 Untreated Leachate SM 4500-P 15598 SM 4500-P 2610403001 Untreated Leachate SM 4500-P 15333 2610403001 Untreated Leachate SM 5210B 15332 SM 5210B 2610403001 Untreated Leachate EPA 9056A 15253 2610403001 Untreated Leachate EPA9056A 15515 Date: 10/29/2018 11:23 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch 15637 15643 15642 15499 Page 21 of 24 I a Q � O p y N I<: pf ilr f5 7 v u n a � u Ol � u C3 � O �11 ❑ r= � N a C;7 o Q1 y [a Q �• a LLI w Q 4 m � o m 00 a r J 0 b C b rHyg� � ❑ G kri u H o Q � c � c n u i J o C c § P � L 2 y 1 ,; n` F rcir u 3 ❑ CID as"n j LL �a w� Qt Q rn m Q lL • 11 - V' � s � ❑- f a Irjr&} auuOlyQ 1�W-48 InesNsielow Ha e CIQQ�11i0ekN rtv ON ' DOA I ddV and ISJ,1 saigAILMV 3yu2 . -o-14 CoMep f HQler! IOH £QNH vos�H paivasosduf) S43211VINO:� j0 C NOU-Oa 110] 1V dW 31 71dwV`r a 1L a w w v O a o U 14 L Jr .r iyarvifap❑DpR-aril �ao�x,albrf C g S # 3ij? 3 o F LU a 2 a � eye m Q U) a � ❑ n a MESS MENU lrt+A] }7 rkul s altlutec v MiL z a lalo�9 f= c5 pelv❑S x ac❑ tin $ Ira+h1 L un pgn4a7a �{ u dW3S IJ 1 M R� LU t F J •j LU 7 � a 2 Q ❑ z x z g a a a 4 4 f-/ F R m 2249=cn CC p[j 41 � if r „. Fail Analylical Client Name: { m an: ail CLIENT: F Courier: ❑ Fed Ex ❑ UPS UUSPS ❑ Client LJCornmercialr. Pace blhE Tracking H: �iS3 Custody Seat on Cooler/Box Present: es ❑ rto Seals intact: es L no Packing Material: ❑ Bubble Wrap ubble Bags ❑ None [J Other Thermometer Used /*)?�L— Type of Ice: Nvet! Blue None ❑ samplE 610403 Clue Date: 10/29/18 tic —NC Prof, Due Dahl: Prof. Name: on ice, cooling process has teoun Cooler Temperature Blot❑ iCal Tissue is Frozen: 9 ❑at and Initials of person examining co tents: Temp should b above freezing to 6'C Comments: Chain of Cus�ody Present: C41 rs ClNo 04.4 1. Chain of Custody Filled Out: Yes ❑No ❑N:A 2, Chain of Gus ody Relinquished: Y<es ❑Nn ❑NSA 3, Sample Name & Signature on CDC: ?! es ❑No DNA 4, Samples ArnVed within Hold Time: LrYes, ❑No ON A 5. Short Hold Time Analysis <72hr : 2<5 ❑Now❑NSA 6. Rush Turn Around Time Requested: ❑Yes LdEJ❑ ❑N:A 7, Sufficient Volume' 0 9 �:�No EN: A g, Correct Cont�Iners Used: f % ❑Na ❑N A g, -Pace Containers Used: fees ❑too ❑N A Containers Intact: E;hl's” ONo ❑N_A i j Filtered volume received for Dissolved tests Dyes ONO 2N1a 11, er�es! Sample Labels match COC: rT ONO El WA 12, -Includes date/timeilDlAnal sis Vatnx: All containers me cling preservation have been checked - 775es ONO ❑NSA 13, All containers nleding preservation are found to be in C--res ONO C❑N A compliance ,nnlh EPA recommendation. Initial when Lol rl of a ded exceptons: ❑A,+ lifarm, TOC, ❑&G, WI-aRO (water) Yes ONo completed preserva;i e Samples checked for dechiorination: ❑YBs =TN* Fef4 R. 14. Headspace in VOA Vials t >6mmj: Dyes t0 7N:"� 15 Trip Blank Present; pYes � ❑N• A 16. Trip Blank Custody Seals Present Eyes ❑Na N A Pace Trip Blank. Lot # (ifpurchased). Client Notification/ Resolution; Person Contacted. Commentsi Resolution: Project Manager Review: Date)'Time: Field Data Required' Y + N Now Whenew,r there is a discrepancy alfw3ing North Carolina compliance samples. a copy of this form will be sent to �he North Carolina DEHNR ,-ertiIicalion 01fiue i i e out of hold, encorrect preservativ8. out of Temp incorrect :]ontctiF113rsi ,3. 11 septemde d 3 of 24 t z z z z z 0 O U Ecl 3� _ua E o o p 0 o o V t C tG� CC U vG� h U N m N 0.) cn z z .� •� o u � 94 u a : 3 c r- 3 0 c o La 0 d o N n s .. a w o � G r r CC m rn m a im Page 24 of 24