NCD003162542_Badin Business Park_Corrective Action_20190129

Badin Business Park LLC c/o Alcoa Corporation 201 Isabella Street Suite 500 Pittsburgh, PA 15212-5858 USA Tel: [phone]

January 29, 2019
Mr. Robert C. McDaniel Facility Management Branch Hazardous Waste Section
North Carolina Department of Environmental Quality
217 West Jones Street Raleigh, North Carolina 27603 VIA ELECTRONIC MAIL
Re: Targeted Sampling Report Badin Business Park (f/k/a Alcoa - Badin Works) Badin, North Carolina EPA ID: NCD 003 162 542

Dear Mr. McDaniel: Badin Business Park LLC respectfully submits the above-referenced report for your review. The report is being provided as a condition of the May 31, 2018 Targeted Sampling Work Plan.

Should you have any questions or comments, please contact Jason Mibroda of Alcoa at [phone] at your convenience. Sincerely,
Ronald M. Morosky Director, Corporate Remediation

Enc. cc: Jason Mibroda, Alcoa

ENVIRONEERING, INC.

TARGETED SAMPLING REPORT

FOR THE

BADIN BUSINESS PARK FACILITY
BADIN, NORTH CAROLINA

January 28, 2019

Prepared for:

Badin Business Park LLC
201 Isabella Street,
Pittsburgh, PA 15212

Prepared by:

ENVIRONEERING, INC.
16100 Cairnway, Suite 320
Houston, Texas 77084
832-674-8800
ENVIRONEERING, INC.

137-263 Targeted Sampling Report – Badin Business Park Facility - Badin, NC; January 2019 i
TABLE OF CONTENTS

1.0 INTRODUCTION .......................................................................................................................1
1.1 Overview ..........................................................................................................................1
1.2 Basis of Work ..................................................................................................................1
2.0 SAMPLE COLLECTION ..........................................................................................................2
3.0 SAMPLING RESULTS ..............................................................................................................3
3.1 Former Electrical Shop and Warehouse .......................................................................3
3.1.1 Volatile Organic Compounds ................................................................................3
3.1.2 Polychlorinated Biphenyls ....................................................................................3
3.1.3 Fluoride and Cyanide ............................................................................................3
3.1.4 Polycyclic Aromatic Hydrocarbons ......................................................................3
3.2 Former Maintenance Shop Area ...................................................................................4
3.2.1 Volatile Organic Compounds ................................................................................4
3.2.2 Polycyclic Aromatic Hydrocarbons ......................................................................4
3.3 Former Cathode Plant Area ...........................................................................................4
3.3.1 Polychlorinated Biphenyls ....................................................................................5
3.3.2 Polycyclic Aromatic Hydrocarbons ......................................................................5
3.4 Former Anode Plant Area ..............................................................................................5
3.4.1 Polychlorinated Biphenyls ....................................................................................5
3.4.2 Polycyclic Aromatic Hydrocarbons ......................................................................5
3.5 Former Potline and Bath Crushing Area .....................................................................6
3.5.1 Fluoride and Cyanide ............................................................................................6
3.5.2 Polycyclic Aromatic Hydrocarbons ......................................................................6
3.6 Former Anode Butt Reclamation and Rod Shop .........................................................6
3.6.1 Polycyclic Aromatic Hydrocarbons ......................................................................7
3.7 Former Carbon Baking Furnace ...................................................................................7
3.7.1 Polycyclic Aromatic Hydrocarbons ......................................................................7
3.8 Former Rectifier Station ................................................................................................7
3.8.1 Polychlorinated Biphenyls ....................................................................................8
3.8.2 Fluoride and Cyanide ............................................................................................8
3.8.3 Polycyclic Aromatic Hydrocarbons ......................................................................8
3.9 Field Blanks .....................................................................................................................8
4.0 CONCLUSIONS .........................................................................................................................23

LIST OF FIGURES

Figure 2-1 Targeted Sampling Areas of Interest.......................................................................... 9
Figure 2-2 Targeted Sampling Locations .................................................................................. 10

ENVIRONEERING, INC.

137-263 Targeted Sampling Report – Badin Business Park Facility - Badin, NC; January 2019 ii
LIST OF TABLES

Table 2-1 Former Electrical Shop and Warehouse Area Analytical Results ........................... 11
Table 2-2 Former Maintenance Shop Area Analytical Results ................................................ 12
Table 2-3 Former Cathode Plant Area Analytical Results ....................................................... 13
Table 2-4 Former Anode Plant Area Analytical Results .......................................................... 14
Table 2-5 Former Potline and Bath Crushing Area Analytical Results ................................... 15
Table 2-6 Former Anode Butt Reclamation and Rod Shop Analytical Results ....................... 19
Table 2-7 Former Carbon Baking Furnace Analytical Results ................................................ 20
Table 2-8 Former Rectifier Station Analytical Results ............................................................ 21
Table 2-9 Equipment and Trip Blank Sample Analytical Results............................................ 22

LIST OF APPENDICES

Appendix A Laboratory Reports and Chain of Custody Forms

ENVIRONEERING, INC.

137-263 Targeted Sampling Report – Badin Business Park Facility - Badin, NC; January 2019 1
1.0 INTRODUCTION

The May 31, 2018 Targeted Sampling Work Plan (Work Plan) was developed as a guidance document in
support of investigative sampling activities at the Badin Business Park LLC facility (facility), formerly
known as the Alcoa Badin Works facility. The Work Plan followed the January 31, 2018 North Carolina
Department of Environmental Quality (NCDEQ) request for soil sampling at the former facility and
subsequent meetings on May 10 and 24, 2018. The approach for the sampling activities was developed
based on information obtained from reconnaissance, previous investigations, and historical remedial
activities conducted at the facility. NCDEQ granted approval of the Work Plan on June 15, 2018.

1.1 Overview

The former Alcoa-Badin Works facility was a primary aluminum smelting plant. Aluminum production
began at the facility in 1916 after purchasing and completing the holdings of a French combine, which
had begun work on a smelter. The former Alcoa-Badin Works facility consisted of potlines; electrode
plants where anodes and cathodes were manufactured; casting facilities; a machine shop; and various
offices and utility buildings. Aluminum production was curtailed in August 2002. The plant continued to
manufacture anodes and high-purity aluminum until 2007. The plant was permanently closed in 2010.
Demolition related activities (i.e., removal of selected equipment, buildings and foundations) were
completed in 2012. Since closing the plant, the facility has been redeveloped into a business park for
manufacturing companies.

1.2 Basis of Work

Environmental investigations have been performed at the facility in the past; however, these
investigations targeted specific areas of the facility where constituents of interest (COIs) were known or
suspected to have been utilized. Other areas of the facility were not historically evaluated because
environmental impacts were not believed to be present or the areas were otherwise covered by plant
buildings or obstructions. The basis for the work was to supplement previous investigations by obtaining
information to assess for the presence of COIs in soils on the facility. To accomplish this, soil samples
were collected and analyzed to evaluate soil quality. Results from the investigation are detailed below.
ENVIRONEERING, INC.

137-263 Targeted Sampling Report – Badin Business Park Facility - Badin, NC; January 2019 2
2.0 SAMPLE COLLECTION

Implementation of the soil sampling program was conducted September 24 through 26, 2018. Sample
collection, shipment, and decontamination were conducted following procedures outlined in the Work
Plan. Field work included collection of sixty-five (65) soil samples across eight (8) facility locations. Soil
sample locations are presented on Figure 2-1.

At each location, a soil core was collected from soil borings using direct-push technology (e.g.,
Geoprobe). As previously stated in the Work Plan, demolition related activities (removal of selected
equipment, buildings and foundations) were completed in 2012. Selected building foundations remain in
place and a substantial portion of the facility was backfilled with crushed concrete and soil backfill. If
demolition-related materials (e.g. crushed concrete and backfill) or a concrete pad were not present at the
surface, a soil sample was collected between the interval of 0 to 1 foot below ground surface (bgs). If
demolition materials or a concrete pad were encountered, the shallow soil sample interval of 0 to 1 foot
was collected immediately below the demolition materials or concrete pad and the sampling proceeded
according to the deeper soil sample collection procedures.

Deeper soil samples were targeted for collection between the interval of 4 to 5 feet below the collection of
the shallow soil sample. Where remnant building foundations were encountered, an attempt was made to
core through the foundation and collect a sample beneath the foundation. If the foundation could not be
cored through, the boring was relocated to a location outside the understood footprint of the former
building foundation.
ENVIRONEERING, INC.

137-263 Targeted Sampling Report – Badin Business Park Facility - Badin, NC; January 2019 3
3.0 SAMPLING RESULTS

Samples were provided to Pace Analytical Services, LCC of Huntersville, North Carolina for analysis in
accordance with the Work Plan. Laboratory reports and completed chain of custody forms are provided in
Appendix A. Laboratory analytical results were compared to the February 2018 published NCDEQ
Preliminary Soil Remediation Goals, more specifically the Protection of Groundwater and the
Industrial/Commercial Health-based (Industrial) Preliminary Soil Remediation Goals (PSRGs). A
summary of sampling results from targeted areas follows.

3.1 Former Electrical Shop and Warehouse

The former Electrical Shop and Warehouse buildings (Buildings 007 and 007A) were located in the
central portion of the facility inside the eastern fenceline. Prior to demolition, a portion of Building 007A
served as a central accumulation area for waste. A review of historical data indicated that this area had
continually served as an electrical shop and warehouse. Potential COIs resulting from operations include
volatile organic compounds (VOCs), polychlorinated biphenyls (PCBs), and additional constituents
associated with waste management from primary reduction operations (fluoride, cyanide, and polycyclic
aromatic hydrocarbons (PAHs)).

Two soil samples and one duplicate soil sample were collected from one soil boring (ESW-SB001) from
within the former Electrical Shop and Warehouse Area. Soil sample analytical results are summarized in
Table 2-1.

3.1.1 Volatile Organic Compounds

Volatile organic compounds were not detected in the samples at concentrations above NCDEQ Protection
of Groundwater PSRGs or Industrial PSRGs.

3.1.2 Polychlorinated Biphenyls

PCB Aroclors were not detected in the samples at concentrations above laboratory detection limits.

3.1.3 Fluoride and Cyanide

Fluoride and cyanide were not detected in the samples at concentrations above the PSRGs.

3.1.4 Polycyclic Aromatic Hydrocarbons

Benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, dibenz(a,h)anthracene, and
1-methylnaphthalene were detected in the shallow soil sample (ESW-SB001 (0’-1’)) at concentrations
above Protection of Groundwater PSRGs; however, concentrations were below Industrial PSRGs. PAHs
were not detected in the deep soil sample (ESW-SB001 (4’-5’)) at concentrations above the PSRGs.

Dibenz(a,h)anthracene was detected in the duplicate shallow soil sample (ESW-SB001 (0’-1’) DUP) at a
concentration below the Protection of Groundwater PSRG.
ENVIRONEERING, INC.

137-263 Targeted Sampling Report – Badin Business Park Facility - Badin, NC; January 2019 4

3.2 Former Maintenance Shop Area

The former Maintenance Shops (Buildings 010 and 012) were located in the central portion of the facility
and comprised several buildings which are believed to have contained specialized maintenance activities.
Activities in this area potentially utilized various oils, greases, and solvents during routine operations. A
review of historical data indicated that this area had continually served as a maintenance shop and
warehouse. Potential COIs resulting from operations include VOCs and PAHs.

Eight soil samples were collected from four soil borings (MSA-SB001 through MSA-SB004) from within
the former Maintenance Shop Area. Soil sample analytical results are summarized in Table 2-2.

3.2.1 Volatile Organic Compounds

Volatile organic compounds were not detected in the samples at concentrations above the PSRGs.

3.2.2 Polycyclic Aromatic Hydrocarbons

Benzo(a)anthracene, benzo(a)pyrene, and 1-methylnaphthalene were detected in one shallow soil sample
(MSA-SB001 (0’-1’)) at concentrations above Protection of Groundwater PSRGs; however,
concentrations were below Industrial PSRGs. PAHs were not detected in the deep soil sample
(MSA-SB001 (4’-5’)) at concentrations above the PSRGs.

Benzo(a)pyrene was detected in two shallow soil samples (MSA-SB002 (0’-1’) and MSA-SB004 (0’-1’))
at concentrations above the Protection of Groundwater PSRG; however, the concentrations were below
the Industrial PSRG. PAHs were not detected in the deep soil sample (MSA-SB002 (4’-5’) and
MSA-SB004 (4’-5’)) at concentrations above the PSRGs.

Benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, dibenz(a,h)anthracene, 1-methylnaphthalene,
and naphthalene were detected in one shallow soil sample (MSA-SB003 (0’-1’)) at concentrations above
Protection of Groundwater PSRGs. Benzo(a)pyrene was the only constituent detected at a concentration
above the Industrial PSRGs. PAHs were not detected in the deep soil sample (MSA-SB003 (4’-5’)) at
concentrations above the PSRGs.

3.3 Former Cathode Plant Area

The former Cathode Plant Area (Buildings 014 and 139) was located on the eastern edge of the facility.
Carbon cathodes were formed with anthracite coal, graphite, and coal tar pitch, and rodded with collector
bars. A review of historical data indicated that this area had continually served as a cathode plant.
Potential COIs in the former Cathode Plant Area include PCBs and PAHs.

Four soil samples were collected from two soil borings (CAT-SB001 and CAT-SB002) from within the
former Cathode Plant Area. Soil sample analytical results are summarized in Table 2-3.

ENVIRONEERING, INC.

137-263 Targeted Sampling Report – Badin Business Park Facility - Badin, NC; January 2019 5
3.3.1 Polychlorinated Biphenyls

PCB Aroclors were not detected in the samples at concentrations above laboratory detection limits.

3.3.2 Polycyclic Aromatic Hydrocarbons

Benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, and dibenz(a,h)anthracene were detected in
one shallow soil sample (CAT-SB001 (0’-1’)) at concentrations above Protection of Groundwater PSRGs.
Benzo(a)pyrene was the only constituent detected at a concentration above the Industrial PSRGs.
Benzo(a)pyrene was detected in the deep soil sample (CAT-SB001 (0’-1’)) at a concentration above the
Protection of Groundwater PSRG; however, the concentration was below the Industrial PSRG.

PAHs were not detected in the remaining samples at concentrations above the PSRGs.

3.4 Former Anode Plant Area

The former Anode Plant Area (Buildings 050B and 050C) was located in the northern portion of the
facility. In the former Anode Plant, calcined petroleum coke was ground, segregated by size, blended,
oven dried, and combined with carbon pitch to create a paste which was then formed into a green anode
block via a hydraulic press. A review of historical data indicated that this area has continually served as
an anode plant. Potential COIs in the former Anode Plant Area include PCBs and PAHs.

Four soil samples were collected from two soil borings (ANO-SB001 and ANO-SB002) from within the
former Anode Plant Area. Soil sample analytical results are summarized in Table 2-4.

3.4.1 Polychlorinated Biphenyls

Aroclor 1232 was detected in one shallow soil sample (ANO-SB002 (0’-1’)) at a concentration above the
Protection of Groundwater PSRG; however, the concentration was below the Industrial PSRG. PCB
Aroclors were not detected in the deep soil sample (ANO-SB002 (4’-5’)) at concentrations above the
PSRGs.

PCB Aroclors were not detected in the remaining samples at concentrations above the PSRGs.

3.4.2 Polycyclic Aromatic Hydrocarbons

Benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, and dibenz(a,h)anthracene were detected in
one shallow soil sample (ANO-SB001 (0’-1’)) at concentrations above Protection of Groundwater
PSRGs; however, the concentrations were below the Industrial PSRGs. PAHs were not detected in the
deep soil sample (ANO-SB001 (4’-5’)) at concentrations above the PSRGs.

Benzo(a)anthracene, benzo(a)pyrene, and benzo(b)fluoranthene were detected in one shallow soil sample
(ANO-SB002 (0’-1’)) at concentrations above Protection of Groundwater PSRGs. Benzo(a)pyrene was
the only constituent detected at a concentration above the Industrial PSRGs. PAHs were not detected in
the deep soil sample (ANO-SB002 (4’-5’)) at concentrations above the PSRGs.
ENVIRONEERING, INC.

137-263 Targeted Sampling Report – Badin Business Park Facility - Badin, NC; January 2019 6
3.5 Former Potline and Bath Crushing Area

The Potlines (Buildings 201 through 204) were the main aluminum production areas in the central and
southern portions of the facility. The former Bath Crushing Area (Building 204H) was located
immediately west of the potlines. The potlines were each comprised of multiple rectangular “pots” where
aluminum was generated through electrolysis of a molten cryolite and alumina solution. Carbon was used
for the cathodes and anodes, which were consumed in the process. A review of historical data indicated
that this area may also have been historically utilized for potlines. Potential COIs in these areas are
constituents associated with primary reduction operations (fluoride, cyanide, and PAHs).

Thirty-four (34) soil samples were collected from seventeen (17) soil borings (PBC-SB001 through
PBC-SB017) from within the former Potline and Bath Crushing Area. Soil sample analytical results are
summarized in Table 2-5.

3.5.1 Fluoride and Cyanide

Fluoride and cyanide were not detected in the samples at concentrations above the PSRGs.

3.5.2 Polycyclic Aromatic Hydrocarbons

Benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, and 1-methylnaphthalene were detected in
one shallow soil sample (PBC-SB004 (0’-1’)) at concentrations above Protection of Groundwater PSRGs;
however, the concentrations were below Industrial PSRGs. PAHs were not detected in the deep soil
sample (PBC-SB004 (4’-5’)) at concentrations above laboratory detection limits.

Benzo(a)anthracene and benzo(a)pyrene were detected in one shallow soil sample (PBC-SB008 (0’-1’)) at
concentrations above Protection of Groundwater PSRGs; however, concentrations were below Industrial
PSRGs. PAHs were not detected in the deep soil sample (PBC-SB008 (4’-5’)) at concentrations above
laboratory detection limits.

PAHs were not detected in the remaining samples at concentrations above the PSRGs.

3.6 Former Anode Butt Reclamation and Rod Shop

The former Anode Butt Reclamation and Rod Shop (Building 232) was located in the central portion of
the facility. After the anodes were consumed as part of the reduction process, the rod and cast iron were
removed for reuse and recycling from the remnants of the anode, or anode butt. The anode butts were
transported back to the Anode Plant for forming into new anodes. After baking at the former Carbon
Baking Furnace, the anode was coupled to the anode rod with cast iron prior to storage or transport to the
potline. Potential COIs in this area include PAHs.

Four soil samples were collected from two soil borings (ABR-SB001 and ABR-SB002) from within the
former Anode Butt Reclamation and Rod Shop area. Soil sample analytical results are summarized in
Table 2-6.

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137-263 Targeted Sampling Report – Badin Business Park Facility - Badin, NC; January 2019 7
3.6.1 Polycyclic Aromatic Hydrocarbons

Benzo(a)pyrene was detected in one shallow soil sample (ABR-SB001 (0’-1’)) at a concentration above
the Protection of Groundwater PSRG; however, the concentration was below the Industrial PSRG. PAHs
were not detected in the deep soil sample (ABR-SB001 (4’-5’)) at concentrations above the PSRGs.

Benzo(a)anthracene, benzo(a)pyrene, and benzo(b)fluoranthene were detected in one shallow soil sample
(ABR-SB002 (0’-1’)) at concentrations above Protection of Groundwater PSRGs; however,
concentrations were below Industrial PSRGs. Benzo(a)pyrene was detected in the deep soil sample
(ABR-SB002 (4’-5’)) at a concentration above the Protection of Groundwater PSRG; however, the
concentration was below the Industrial PSRG. No additional PAHs were detected in the deep soil sample
at concentrations above the PSRGs.

3.7 Former Carbon Baking Furnace

The former Carbon Baking Furnace (Buildings 261 and 262) was located in the central portion of the
facility. Green anodes manufactured in the former Anode Plant were either stored or transported to the
baking furnace where they were baked to drive off pitch volatiles. A review of historical data indicated
that this area previously contained a baking furnace. Potential COIs in this area include PAHs.

Four soil samples were collected from two soil borings (CBF-SB001 and CBF-SB002) from within the
former Carbon Baking Furnace area. Soil sample analytical results are summarized in Table 2-7.

3.7.1 Polycyclic Aromatic Hydrocarbons

Benzo(a)anthracene and benzo(a)pyrene were detected in one shallow soil sample (CBF-SB001 (0’-1’)) at
concentrations above Protection of Groundwater PSRGs; however, concentrations were below Industrial
PSRGs. PAHs were not detected in the deep soil sample (CBF-SB001 (4’-5’)) at concentrations above the
PSRGs.

Benzo(a)pyrene was detected in one shallow soil sample (CBF-SB002 (0’-1’)) at a concentration above
the Protection of Groundwater PSRG; however, the concentration was below the Industrial PSRG. PAHs
were not detected in the deep soil sample (CBF-SB002 (4’-5’)) at concentrations above the PSRGs.

3.8 Former Rectifier Station

The former Rectifier Station (Buildings 301 and 302) was located on the northern edge of the former
potlines (Buildings 201 through 204) and near the former potlines associated with the early 20th century
plant. A review of historical data indicated that this area may have been historically utilized for potlines.
Potential COIs in this area include PCBs and constituents associated with primary reduction operations
(fluoride, cyanide, and PAHs).

Four soil samples were collected from two soil borings (REC-SB001 and REC-SB002) from within the
former Rectifier Station area. Soil sample analytical results are summarized in Table 2-8.

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137-263 Targeted Sampling Report – Badin Business Park Facility - Badin, NC; January 2019 8
3.8.1 Polychlorinated Biphenyls

PCB Aroclors were not detected in the samples at concentrations above laboratory detection limits.

3.8.2 Fluoride and Cyanide

Fluoride and cyanide were not detected in the samples at concentrations above the PSRGs.

3.8.3 Polycyclic Aromatic Hydrocarbons

Benzo(a)anthracene, benzo(a)pyrene, and benzo(b)fluoranthene were detected in one shallow soil sample
(REC-SB001 (0’-1’)) at concentrations above Protection of Groundwater PSRGs; however,
concentrations were below Industrial PSRGs. PAHs were not detected in the deep soil sample
(REC-SB001 (4’-5’)) at concentrations above the PSRGs.

PAHs were not detected in the remaining samples at concentrations above the PSRGs.

3.9 Field Blanks

One equipment blank was analyzed as part of this project. The equipment blank was prepared by running
analyte free distilled water across sample collection equipment (sampling core barrel) after
decontamination and placing it in the appropriate sample containers for analysis. No constituents were
detected at concentrations above laboratory detection limits. Results are summarized in Table 2-9.

One trip blank was analyzed as part of this project. The trip blank was prepared by the laboratory and
placed in the cooler containing samples selected for VOC analysis. No constituents were detected at
concentrations above laboratory detection limits. Results are summarized in Table 2-9.

ENVIRONEERING, INC.
LEGEND:
PARCEL BOUNDARY
SOIL BORING
NOTE: BACKGROUND AERIAL PHOTOGRAPH DATED 2015
FORMER
CATHODE
PLANT
FORMER
ANODE
PLANT
FORMER
MAINTENANCE
SHOP AREA
FORMER
ELECTRICAL
SHOP AND
WAREHOUSE
FORMER
RECTIFIER
STATION
FORMER
ANODE BUTT
RECLAIMING
AND ROD
SHOP
FORMER POTLINE
AND BATH
CRUSHING AREA
FORMER
CARBON
BAKING
FURNACE
ENVIRONEERING, INC.
CBF-SB002
LEGEND:
PARCEL BOUNDARY
SOIL BORING
NOTE: BACKGROUND AERIAL PHOTOGRAPH DATED 2015
ESW-SB001
MSA-SB001
ANO-SB001
ANO-SB002
MSA-SB002
MSA-SB003
MSA-SB004
CBF-SB001ABR-SB001
ABR-SB002
CAT-SB001
CAT-SB002
REC-SB001
REC-SB002
PBC-SB001
PBC-SB002
PBC-SB003
PBC-SB004
PBC-SB005PBC-SB012
PBC-SB013
PBC-SB014
PBC-SB017
PBC-SB015
PBC-SB016
PBC-SB008
PBC-SB009
PBC-SB007
PBC-SB010
PBC-SB006PBC-SB011
Sample ID Method CAS Units
PSRG
Prot. of GW
PSRG
Ind/Comm
Surface Material
Thickness of Surface Material
Sample Depth Below Surface Material
Date
Time
Percent Moisture ASTM D2974-87 %
PCB-1016 (Aroclor 1016)EPA 8082 12674-11-2 mg/kg ND <0.0188 ND <0.0178 ND <0.0193 0.94 10
PCB-1221 (Aroclor 1221)EPA 8082 11104-28-2 mg/kg ND <0.0188 ND <0.0178 ND <0.0193 0.0059 0.84
PCB-1232 (Aroclor 1232)EPA 8082 11141-16-5 mg/kg ND <0.0188 ND <0.0178 ND <0.0193 0.0059 0.73
PCB-1242 (Aroclor 1242)EPA 8082 53469-21-9 mg/kg ND <0.0188 ND <0.0178 ND <0.0193 0.055 0.95
PCB-1248 (Aroclor 1248)EPA 8082 12672-29-6 mg/kg ND <0.0188 ND <0.0178 ND <0.0193 0.054 0.96
PCB-1254 (Aroclor 1254)EPA 8082 11097-69-1 mg/kg ND <0.0188 ND <0.0178 ND <0.0193 0.091 0.97
PCB-1260 (Aroclor 1260)EPA 8082 11096-82-5 mg/kg ND <0.0188 ND <0.0178 ND <0.0193 0.24 0.99
Total Polychlorinated Biphenyls mg/kg 0.055 0.95
1-Methylnaphthalene EPA 8270 90-12-0 mg/kg ND <0.0015 0.11 73
2-Methylnaphthalene EPA 8270 91-57-6 mg/kg 3.1 600
Acenaphthene EPA 8270 83-32-9 mg/kg ND <0.0019 16 9000
Acenaphthylene EPA 8270 208-96-8 mg/kg ND <0.0016 NE NE
Anthracene EPA 8270 120-12-7 mg/kg ND <0.0018 1300 45000
Benzo(a)anthracene EPA 8270 56-55-3 mg/kg 0.35 21
Benzo(a)pyrene EPA 8270 50-32-8 mg/kg 0.12 2.1
Benzo(b)fluoranthene EPA 8270 205-99-2 mg/kg 1.2 21
Benzo(g,h,i)perylene EPA 8270 191-24-2 mg/kg ND <0.0033 NE NE
Benzo(k)fluoranthene EPA 8270 207-08-9 mg/kg ND <0.0019 12 210
Chrysene EPA 8270 218-01-9 mg/kg 36 2100
Dibenz(a,h)anthracene EPA 8270 53-70-3 mg/kg ND <0.0023 0.38 2.1
Fluoranthene EPA 8270 206-44-0 mg/kg 670 6000
Fluorene EPA 8270 86-73-7 mg/kg ND <0.0020 110 6000
Indeno(1,2,3-cd)pyrene EPA 8270 193-39-5 mg/kg ND <0.0035 3.9 21
Naphthalene EPA 8270 91-20-3 mg/kg ND <0.0029 0.39 18
Phenanthrene EPA 8270 85-01-8 mg/kg ND <0.0019 NE NE
Pyrene EPA 8270 129-00-0 mg/kg 440 4500
1,1,1,2-Tetrachloroethane EPA 8260B 630-20-6 mg/kg ND <0.0021 ND <0.0018 ND <0.0019 0.0076 9.3
1,1,1-Trichloroethane EPA 8260B 71-55-6 mg/kg ND <0.0018 ND <0.0016 ND <0.0017 1.4 7600
1,1,2,2-Tetrachloroethane EPA 8260B 79-34-5 mg/kg ND <0.0019 ND <0.0016 ND <0.0018 0.0016 2.8
1,1,2-Trichloroethane EPA 8260B 79-00-5 mg/kg ND <0.0021 ND <0.0018 ND <0.0019 0.0039 1.3
1,1-Dichloroethane EPA 8260B 75-34-3 mg/kg ND <0.0015 ND <0.0013 ND <0.0014 0.034 17
1,1-Dichloroethene EPA 8260B 75-35-4 mg/kg ND <0.0018 ND <0.0016 ND <0.0017 2.5 210
1,1-Dichloropropene EPA 8260B 563-58-6 mg/kg ND <0.0015 ND <0.0013 ND <0.0014 NE NE
1,2,3-Trichlorobenzene EPA 8260B 87-61-6 mg/kg ND <0.0022 ND <0.0019 ND <0.0020 0.33 190
1,2,3-Trichloropropane EPA 8260B 96-18-4 mg/kg ND <0.0016 ND <0.0014 ND <0.0015 0.000045 0.11
1,2,4-Trichlorobenzene EPA 8260B 120-82-1 mg/kg ND <0.0016 ND <0.0014 ND <0.0015 4.1 55
1,2,4-Trimethylbenzene EPA 8260B 95-63-6 mg/kg ND <0.0020 ND <0.0017 ND <0.0019 1.2 370
1,2-Dibromo-3-chloropropane EPA 8260B 96-12-8 mg/kg ND <0.0036 ND <0.0031 ND <0.0033 0.00035 0.068
1,2-Dibromoethane (EDB)EPA 8260B 106-93-4 mg/kg ND <0.0018 ND <0.0016 ND <0.0017 0.00011 0.17
1,2-Dichlorobenzene EPA 8260B 95-50-1 mg/kg ND <0.0019 ND <0.0016 ND <0.0018 0.39 2000
1,2-Dichloroethane EPA 8260B 107-06-2 mg/kg ND <0.0022 ND <0.0019 ND <0.0020 0.0023 2.2
1,2-Dichloropropane EPA 8260B 78-87-5 mg/kg ND <0.0017 ND <0.0015 ND <0.0016 0.004 12
1,3,5-Trimethylbenzene EPA 8260B 108-67-8 mg/kg ND <0.0018 ND <0.0016 ND <0.0017 11 320
1,3-Dichlorobenzene EPA 8260B 541-73-1 mg/kg ND <0.0020 ND <0.0017 ND <0.0019 3.8 NE
1,3-Dichloropropane EPA 8260B 142-28-9 mg/kg ND <0.0019 ND <0.0016 ND <0.0018 0.97 4700
1,4-Dichlorobenzene EPA 8260B 106-46-7 mg/kg ND <0.0017 ND <0.0015 ND <0.0016 0.12 12
2,2-Dichloropropane EPA 8260B 594-20-7 mg/kg ND <0.0017 ND <0.0015 ND <0.0016 NE NE
2-Butanone (MEK)EPA 8260B 78-93-3 mg/kg ND <0.0029 ND <0.0025 ND <0.0027 17 40000
2-Chlorotoluene EPA 8260B 95-49-8 mg/kg ND <0.0017 ND <0.0015 ND <0.0016 2 4700
2-Hexanone EPA 8260B 591-78-6 mg/kg ND <0.0039 ND <0.0034 ND <0.0036 0.18 280
4-Chlorotoluene EPA 8260B 106-43-4 mg/kg ND <0.0018 ND <0.0016 ND <0.0017 0.46 4700
4-Methyl-2-pentanone (MIBK) EPA 8260B 108-10-1 mg/kg ND <0.0037 ND <0.0032 ND <0.0034 0.45 30000
Acetone EPA 8260B 67-64-1 mg/kg ND <0.0093 25 140000
Benzene EPA 8260B 71-43-2 mg/kg ND <0.0016 ND <0.0014 ND <0.0015 0.01 5.4
Bromobenzene EPA 8260B 108-86-1 mg/kg ND <0.0020 ND <0.0017 ND <0.0019 0.76 370
Bromochloromethane EPA 8260B 74-97-5 mg/kg ND <0.0017 ND <0.0015 ND <0.0016 NE 130
Bromodichloromethane EPA 8260B 75-27-4 mg/kg ND <0.0019 ND <0.0016 ND <0.0018 0.0033 1.4
Bromoform EPA 8260B 75-25-2 mg/kg ND <0.0023 ND <0.0020 ND <0.0021 0.021 90
Bromomethane EPA 8260B 74-83-9 mg/kg ND <0.0025 ND <0.0022 ND <0.0023 0.05 6.4
Carbon tetrachloride EPA 8260B 56-23-5 mg/kg ND <0.0026 ND <0.0022 ND <0.0024 0.0023 3
Chlorobenzene EPA 8260B 108-90-7 mg/kg ND <0.0019 ND <0.0016 ND <0.0018 0.68 280
Chloroethane EPA 8260B 75-00-3 mg/kg ND <0.0024 ND <0.0021 ND <0.0022 17 12000
Chloroform EPA 8260B 67-66-3 mg/kg ND <0.0016 ND <0.0014 ND <0.0015 0.39 1.5
Chloromethane EPA 8260B 74-87-3 mg/kg ND <0.0024 ND <0.0021 ND <0.0022 0.015 99
cis-1,2-Dichloroethene EPA 8260B 156-59-2 mg/kg ND <0.0014 ND <0.0012 ND <0.0013 0.41 470
cis-1,3-Dichloropropene EPA 8260B 10061-01-5 mg/kg ND <0.0018 ND <0.0016 ND <0.0017 NE NE
Dibromochloromethane EPA 8260B 124-48-1 mg/kg ND <0.0018 ND <0.0016 ND <0.0017 0.0021 39
Dibromomethane EPA 8260B 74-95-3 mg/kg ND <0.0025 ND <0.0022 ND <0.0023 0.34 21
Dichlorodifluoromethane EPA 8260B 75-71-8 mg/kg ND <0.0036 ND <0.0031 ND <0.0033 30 78
Diisopropyl ether EPA 8260B 108-20-3 mg/kg ND <0.0017 ND <0.0015 ND <0.0016 0.36 2000
Ethylbenzene EPA 8260B 100-41-4 mg/kg ND <0.0018 ND <0.0016 ND <0.0017 13 27
Hexachloro-1,3-butadiene EPA 8260B 87-68-3 mg/kg ND <0.0020 ND <0.0017 ND <0.0019 0.015 5.6
Isopropylbenzene (Cumene) EPA 8260B 98-82-8 mg/kg ND <0.0019 ND <0.0016 ND <0.0018 2.3 2100
m&p-Xylene EPA 8260B 179601-23-1 mg/kg ND <0.0036 ND <0.0031 ND <0.0033 9.8 500
Methylene Chloride EPA 8260B 75-09-2 mg/kg ND <0.0030 ND <0.0026 0.025 6500
Methyl-tert-butyl ether EPA 8260B 1634-04-4 mg/kg ND <0.0015 ND <0.0013 ND <0.0014 0.09 220
Naphthalene EPA 8260B 91-20-3 mg/kg ND <0.0012 ND <0.0010 ND <0.0011 0.39 18
n-Butylbenzene EPA 8260B 104-51-8 mg/kg ND <0.0018 ND <0.0016 ND <0.0017 4.5 12000
n-Propylbenzene EPA 8260B 103-65-1 mg/kg ND <0.0017 ND <0.0015 ND <0.0016 2.6 5100
o-Xylene EPA 8260B 95-47-6 mg/kg ND <0.0019 ND <0.0016 ND <0.0018 9.8 590
p-Isopropyltoluene EPA 8260B 99-87-6 mg/kg ND <0.0017 ND <0.0015 ND <0.0016 1.24 NE
sec-Butylbenzene EPA 8260B 135-98-8 mg/kg ND <0.0016 ND <0.0014 ND <0.0015 4.1 23000
Styrene EPA 8260B 100-42-5 mg/kg ND <0.0018 ND <0.0016 ND <0.0017 1.5 7300
tert-Butylbenzene EPA 8260B 98-06-6 mg/kg ND <0.0020 ND <0.0017 ND <0.0019 3.1 23000
Tetrachloroethene EPA 8260B 127-18-4 mg/kg ND <0.0017 ND <0.0015 ND <0.0016 0.0063 82
Toluene EPA 8260B 108-88-3 mg/kg ND <0.0018 ND <0.0016 ND <0.0017 8.3 9700
trans-1,2-Dichloroethene EPA 8260B 156-60-5 mg/kg ND <0.0019 ND <0.0016 ND <0.0018 0.62 4700
trans-1,3-Dichloropropene EPA 8260B 10061-02-6 mg/kg ND <0.0015 ND <0.0013 ND <0.0014 NE NE
Trichloroethene EPA 8260B 79-01-6 mg/kg ND <0.0021 ND <0.0018 ND <0.0019 0.021 4
Trichlorofluoromethane EPA 8260B 75-69-4 mg/kg ND <0.0022 ND <0.0019 ND <0.0020 25 70000
Vinyl acetate EPA 8260B 108-05-4 mg/kg ND <0.0087 ND <0.0076 ND <0.0082 0.37 820
Vinyl chloride EPA 8260B 75-01-4 mg/kg ND <0.0018 ND <0.0016 ND <0.0017 0.00024 1.7
Xylene (Total)EPA 8260B 1330-20-7 mg/kg ND <0.0036 ND <0.0031 ND <0.0033 9.9 530
Cyanide EPA 9012 57-12-5 mg/kg ND <0.17 ND <0.17 14 31
Fluoride EPA 9056 16984-48-8 mg/kg ND <3.2 6000 9300
ND - The analyte was not detected above laboratory detection limits. Subscript indicates compound-specific MDL in mg/kg.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NCDEQ Preliminary Soil Remediation Goals (PSRG) - February 2018
NE - Not established.
0.0025 J
33 40.1
0.0037 J
0.29 J
0.0121 J 0.0128 J
0.456 0.499
1.77 0.868
0.0063 J
0.509 0.242
1.53 0.899 0.0022 J
0.0168 J 0.0207
1.15 0.555
0.167 0.155
1.37 0.627
1.76 0.639
4.17 1.79
0.0032 J
1.55 0.773 0.0019 J
5.57 1.83 0.0042 J
0.0346 J 0.0266
0.133 0.107
3.91 0.875
0.0227 J 0.0268
20.1 15.7 21.4
ND ND ND
0.15 0.127
0.213 0.184 0.0019 J
9/24/2018 9/24/2018 9/24/2018
12:10 12:15 12:25
Concrete slab Concrete slab Concrete slab
0'-1'0'-1'4'-5'
8"8"8"
ESW-SB001
(0'-1')
ESW-SB001
(0'-1') DUP
ESW-SB001
(4'-5')
Table 2-1
Soil Sample Analytical Results
Former Electrical Shop and Warehouse Area
Badin Business Park Facility
Badin, North Carolina
Sample ID Method CAS Units
PSRG
Prot. of GW
PSRG
Ind/Comm
Surface Material
Thickness of Surface Material
Sample Depth Below Surface Material
Date
Time
Percent Moisture ASTM D2974-87 %
1-Methylnaphthalene EPA 8270 90-12-0 mg/kg ND <0.0015 ND <0.0015 ND <0.0014 0.11 73
2-Methylnaphthalene EPA 8270 91-57-6 mg/kg ND <0.0013 ND <0.0014 ND <0.0013 3.1 600
Acenaphthene EPA 8270 83-32-9 mg/kg ND <0.0018 ND <0.0019 ND <0.0018 16 9000
Acenaphthylene EPA 8270 208-96-8 mg/kg ND <0.0016 ND <0.0016 ND <0.0016 NE NE
Anthracene EPA 8270 120-12-7 mg/kg ND <0.0017 ND <0.0017 ND <0.0017 1300 45000
Benzo(a)anthracene EPA 8270 56-55-3 mg/kg 0.35 21
Benzo(a)pyrene EPA 8270 50-32-8 mg/kg ND <0.0013 ND <0.0013 0.12 2.1
Benzo(b)fluoranthene EPA 8270 205-99-2 mg/kg 1.2 21
Benzo(g,h,i)perylene EPA 8270 191-24-2 mg/kg ND <0.0032 ND <0.0032 ND <0.0031 NE NE
Benzo(k)fluoranthene EPA 8270 207-08-9 mg/kg ND <0.0018 ND <0.0018 ND <0.0018 ND <0.0018 ND <0.0019 ND <0.0018 12 210
Chrysene EPA 8270 218-01-9 mg/kg ND <0.0022 ND <0.0022 ND <0.0022 ND <0.0022 36 2100
Dibenz(a,h)anthracene EPA 8270 53-70-3 mg/kg ND <0.0022 ND <0.0022 ND <0.0022 ND <0.0022 0.38 2.1
Fluoranthene EPA 8270 206-44-0 mg/kg ND <0.0010 670 6000
Fluorene EPA 8270 86-73-7 mg/kg ND <0.0019 ND <0.0020 ND <0.0020 ND <0.0019 110 6000
Indeno(1,2,3-cd)pyrene EPA 8270 193-39-5 mg/kg ND <0.0034 ND <0.0034 ND <0.0035 ND <0.0034 3.9 21
Naphthalene EPA 8270 91-20-3 mg/kg ND <0.0028 ND <0.0028 ND <0.0029 ND <0.0028 0.39 18
Phenanthrene EPA 8270 85-01-8 mg/kg ND <0.0018 NE NE
Pyrene EPA 8270 129-00-0 mg/kg 440 4500
1,1,1,2-Tetrachloroethane EPA 8260B 630-20-6 mg/kg ND <0.0027 ND <0.0019 ND <0.0021 ND <0.0029 ND <0.0021 ND <0.0022 ND <0.0019 ND <0.0017 0.0076 9.3
1,1,1-Trichloroethane EPA 8260B 71-55-6 mg/kg ND <0.0023 ND <0.0016 ND <0.0018 ND <0.0025 ND <0.0018 ND <0.0019 ND <0.0016 ND <0.0015 1.4 7600
1,1,2,2-Tetrachloroethane EPA 8260B 79-34-5 mg/kg ND <0.0025 ND <0.0017 ND <0.0019 ND <0.0026 ND <0.0019 ND <0.0020 ND <0.0017 ND <0.0016 0.0016 2.8
1,1,2-Trichloroethane EPA 8260B 79-00-5 mg/kg ND <0.0027 ND <0.0019 ND <0.0021 ND <0.0029 ND <0.0021 ND <0.0022 ND <0.0019 ND <0.0017 0.0039 1.3
1,1-Dichloroethane EPA 8260B 75-34-3 mg/kg ND <0.0019 ND <0.0014 ND <0.0015 ND <0.0021 ND <0.0015 ND <0.0016 ND <0.0013 ND <0.0012 0.034 17
1,1-Dichloroethene EPA 8260B 75-35-4 mg/kg ND <0.0023 ND <0.0016 ND <0.0018 ND <0.0025 ND <0.0018 ND <0.0019 ND <0.0016 ND <0.0015 2.5 210
1,1-Dichloropropene EPA 8260B 563-58-6 mg/kg ND <0.0019 ND <0.0014 ND <0.0015 ND <0.0021 ND <0.0015 ND <0.0016 ND <0.0013 ND <0.0012 NE NE
1,2,3-Trichlorobenzene EPA 8260B 87-61-6 mg/kg ND <0.0029 ND <0.0020 ND <0.0022 ND <0.0031 ND <0.0022 ND <0.0024 ND <0.0019 ND <0.0018 0.33 190
1,2,3-Trichloropropane EPA 8260B 96-18-4 mg/kg ND <0.0021 ND <0.0014 ND <0.0016 ND <0.0022 ND <0.0016 ND <0.0017 ND <0.0014 ND <0.0013 0.000045 0.11
1,2,4-Trichlorobenzene EPA 8260B 120-82-1 mg/kg ND <0.0021 ND <0.0014 ND <0.0016 ND <0.0022 ND <0.0016 ND <0.0017 ND <0.0014 ND <0.0013 4.1 55
1,2,4-Trimethylbenzene EPA 8260B 95-63-6 mg/kg ND <0.0026 ND <0.0018 ND <0.0020 ND <0.0028 ND <0.0020 ND <0.0021 ND <0.0018 ND <0.0016 1.2 370
1,2-Dibromo-3-chloropropane EPA 8260B 96-12-8 mg/kg ND <0.0047 ND <0.0033 ND <0.0035 ND <0.0050 ND <0.0036 ND <0.0038 ND <0.0032 ND <0.0030 0.00035 0.068
1,2-Dibromoethane (EDB) EPA 8260B 106-93-4 mg/kg ND <0.0023 ND <0.0016 ND <0.0018 ND <0.0025 ND <0.0018 ND <0.0019 ND <0.0016 ND <0.0015 0.00011 0.17
1,2-Dichlorobenzene EPA 8260B 95-50-1 mg/kg ND <0.0025 ND <0.0017 ND <0.0019 ND <0.0026 ND <0.0019 ND <0.0020 ND <0.0017 ND <0.0016 0.39 2000
1,2-Dichloroethane EPA 8260B 107-06-2 mg/kg ND <0.0029 ND <0.0020 ND <0.0022 ND <0.0031 ND <0.0022 ND <0.0024 ND <0.0019 ND <0.0018 0.0023 2.2
1,2-Dichloropropane EPA 8260B 78-87-5 mg/kg ND <0.0022 ND <0.0015 ND <0.0017 ND <0.0024 ND <0.0017 ND <0.0018 ND <0.0015 ND <0.0014 0.004 12
1,3,5-Trimethylbenzene EPA 8260B 108-67-8 mg/kg ND <0.0023 ND <0.0016 ND <0.0018 ND <0.0025 ND <0.0018 ND <0.0019 ND <0.0016 ND <0.0015 11 320
1,3-Dichlorobenzene EPA 8260B 541-73-1 mg/kg ND <0.0026 ND <0.0018 ND <0.0020 ND <0.0028 ND <0.0020 ND <0.0021 ND <0.0018 ND <0.0016 3.8 NE
1,3-Dichloropropane EPA 8260B 142-28-9 mg/kg ND <0.0025 ND <0.0017 ND <0.0019 ND <0.0026 ND <0.0019 ND <0.0020 ND <0.0017 ND <0.0016 0.97 4700
1,4-Dichlorobenzene EPA 8260B 106-46-7 mg/kg ND <0.0022 ND <0.0015 ND <0.0017 ND <0.0024 ND <0.0017 ND <0.0018 ND <0.0015 ND <0.0014 0.12 12
2,2-Dichloropropane EPA 8260B 594-20-7 mg/kg ND <0.0022 ND <0.0015 ND <0.0017 ND <0.0024 ND <0.0017 ND <0.0018 ND <0.0015 ND <0.0014 NE NE
2-Butanone (MEK)EPA 8260B 78-93-3 mg/kg ND <0.0038 ND <0.0026 ND <0.0028 ND <0.0040 ND <0.0029 ND <0.0031 ND <0.0026 ND <0.0024 17 40000
2-Chlorotoluene EPA 8260B 95-49-8 mg/kg ND <0.0022 ND <0.0015 ND <0.0017 ND <0.0024 ND <0.0017 ND <0.0018 ND <0.0015 ND <0.0014 2 4700
2-Hexanone EPA 8260B 591-78-6 mg/kg ND <0.0051 ND <0.0035 ND <0.0038 ND <0.0054 ND <0.0039 ND <0.0042 ND <0.0034 ND <0.0032 0.18 280
4-Chlorotoluene EPA 8260B 106-43-4 mg/kg ND <0.0023 ND <0.0016 ND <0.0018 ND <0.0025 ND <0.0018 ND <0.0019 ND <0.0016 ND <0.0015 0.46 4700
4-Methyl-2-pentanone (MIBK) EPA 8260B 108-10-1 mg/kg ND <0.0048 ND <0.0033 ND <0.0036 ND <0.0051 ND <0.0037 ND <0.0040 ND <0.0033 ND <0.0030 0.45 30000
Acetone EPA 8260B 67-64-1 mg/kg ND <0.0130 ND <0.0090 ND <0.0098 25 140000
Benzene EPA 8260B 71-43-2 mg/kg ND <0.0021 ND <0.0014 ND <0.0016 ND <0.0022 ND <0.0016 ND <0.0017 ND <0.0014 ND <0.0013 0.01 5.4
Bromobenzene EPA 8260B 108-86-1 mg/kg ND <0.0026 ND <0.0018 ND <0.0020 ND <0.0028 ND <0.0020 ND <0.0021 ND <0.0018 ND <0.0016 0.76 370
Bromochloromethane EPA 8260B 74-97-5 mg/kg ND <0.0022 ND <0.0015 ND <0.0017 ND <0.0024 ND <0.0017 ND <0.0018 ND <0.0015 ND <0.0014 NE 130
Bromodichloromethane EPA 8260B 75-27-4 mg/kg ND <0.0025 ND <0.0017 ND <0.0019 ND <0.0026 ND <0.0019 ND <0.0020 ND <0.0017 ND <0.0016 0.0033 1.4
Bromoform EPA 8260B 75-25-2 mg/kg ND <0.0030 ND <0.0021 ND <0.0023 ND <0.0032 ND <0.0023 ND <0.0025 ND <0.0020 ND <0.0019 0.021 90
Bromomethane EPA 8260B 74-83-9 mg/kg ND <0.0032 ND <0.0023 ND <0.0024 ND <0.0035 ND <0.0025 ND <0.0027 ND <0.0022 ND <0.0021 0.05 6.4
Carbon tetrachloride EPA 8260B 56-23-5 mg/kg ND <0.0034 ND <0.0023 ND <0.0025 ND <0.0036 ND <0.0026 ND <0.0028 ND <0.0023 ND <0.0021 0.0023 3
Chlorobenzene EPA 8260B 108-90-7 mg/kg ND <0.0025 ND <0.0017 ND <0.0019 ND <0.0026 ND <0.0019 ND <0.0020 ND <0.0017 ND <0.0016 0.68 280
Chloroethane EPA 8260B 75-00-3 mg/kg ND <0.0031 ND <0.0022 ND <0.0024 ND <0.0033 ND <0.0024 ND <0.0026 ND <0.0021 ND <0.0020 17 12000
Chloroform EPA 8260B 67-66-3 mg/kg ND <0.0021 ND <0.0014 ND <0.0016 ND <0.0022 ND <0.0016 ND <0.0017 ND <0.0014 ND <0.0013 0.39 1.5
Chloromethane EPA 8260B 74-87-3 mg/kg ND <0.0031 ND <0.0022 ND <0.0024 ND <0.0033 ND <0.0024 ND <0.0026 ND <0.0021 ND <0.0020 0.015 99
cis-1,2-Dichloroethene EPA 8260B 156-59-2 mg/kg ND <0.0018 ND <0.0013 ND <0.0014 ND <0.0019 ND <0.0014 ND <0.0015 ND <0.0012 ND <0.0012 0.41 470
cis-1,3-Dichloropropene EPA 8260B 10061-01-5 mg/kg ND <0.0023 ND <0.0016 ND <0.0018 ND <0.0025 ND <0.0018 ND <0.0019 ND <0.0016 ND <0.0015 NE NE
Dibromochloromethane EPA 8260B 124-48-1 mg/kg ND <0.0023 ND <0.0016 ND <0.0018 ND <0.0025 ND <0.0018 ND <0.0019 ND <0.0016 ND <0.0015 0.0021 39
Dibromomethane EPA 8260B 74-95-3 mg/kg ND <0.0032 ND <0.0023 ND <0.0024 ND <0.0035 ND <0.0025 ND <0.0027 ND <0.0022 ND <0.0021 0.34 21
Dichlorodifluoromethane EPA 8260B 75-71-8 mg/kg ND <0.0047 ND <0.0033 ND <0.0035 ND <0.0050 ND <0.0036 ND <0.0038 ND <0.0032 ND <0.0030 30 78
Diisopropyl ether EPA 8260B 108-20-3 mg/kg ND <0.0022 ND <0.0015 ND <0.0017 ND <0.0024 ND <0.0017 ND <0.0018 ND <0.0015 ND <0.0014 0.36 2000
Ethylbenzene EPA 8260B 100-41-4 mg/kg ND <0.0023 ND <0.0016 ND <0.0018 ND <0.0025 ND <0.0018 ND <0.0019 ND <0.0016 ND <0.0015 13 27
Hexachloro-1,3-butadiene EPA 8260B 87-68-3 mg/kg ND <0.0026 ND <0.0018 ND <0.0020 ND <0.0028 ND <0.0020 ND <0.0021 ND <0.0018 ND <0.0016 0.015 5.6
Isopropylbenzene (Cumene) EPA 8260B 98-82-8 mg/kg ND <0.0025 ND <0.0017 ND <0.0019 ND <0.0026 ND <0.0019 ND <0.0020 ND <0.0017 ND <0.0016 2.3 2100
m&p-Xylene EPA 8260B 179601-23-1 mg/kg ND <0.0047 ND <0.0033 ND <0.0035 ND <0.0050 ND <0.0036 ND <0.0038 ND <0.0032 ND <0.0030 9.8 500
Methylene Chloride EPA 8260B 75-09-2 mg/kg ND <0.0039 ND <0.0027 ND <0.0029 ND <0.0042 ND <0.0030 ND <0.0025 0.025 6500
Methyl-tert-butyl ether EPA 8260B 1634-04-4 mg/kg ND <0.0019 ND <0.0014 ND <0.0015 ND <0.0021 ND <0.0015 ND <0.0016 ND <0.0013 ND <0.0012 0.09 220
Naphthalene EPA 8260B 91-20-3 mg/kg ND <0.0016 ND <0.0011 ND <0.0012 ND <0.0017 ND <0.0013 ND <0.0011 ND <0.00099 0.39 18
n-Butylbenzene EPA 8260B 104-51-8 mg/kg ND <0.0023 ND <0.0016 ND <0.0018 ND <0.0025 ND <0.0018 ND <0.0019 ND <0.0016 ND <0.0015 4.5 12000
n-Propylbenzene EPA 8260B 103-65-1 mg/kg ND <0.0022 ND <0.0015 ND <0.0017 ND <0.0024 ND <0.0017 ND <0.0018 ND <0.0015 ND <0.0014 2.6 5100
o-Xylene EPA 8260B 95-47-6 mg/kg ND <0.0025 ND <0.0017 ND <0.0019 ND <0.0026 ND <0.0019 ND <0.0020 ND <0.0017 ND <0.0016 9.8 590
p-Isopropyltoluene EPA 8260B 99-87-6 mg/kg ND <0.0022 ND <0.0015 ND <0.0017 ND <0.0024 ND <0.0017 ND <0.0018 ND <0.0015 ND <0.0014 1.24 NE
sec-Butylbenzene EPA 8260B 135-98-8 mg/kg ND <0.0021 ND <0.0014 ND <0.0016 ND <0.0022 ND <0.0016 ND <0.0017 ND <0.0014 ND <0.0013 4.1 23000
Styrene EPA 8260B 100-42-5 mg/kg ND <0.0023 ND <0.0016 ND <0.0018 ND <0.0025 ND <0.0018 ND <0.0019 ND <0.0016 ND <0.0015 1.5 7300
tert-Butylbenzene EPA 8260B 98-06-6 mg/kg ND <0.0026 ND <0.0018 ND <0.0020 ND <0.0028 ND <0.0020 ND <0.0021 ND <0.0018 ND <0.0016 3.1 23000
Tetrachloroethene EPA 8260B 127-18-4 mg/kg ND <0.0022 ND <0.0015 ND <0.0017 ND <0.0024 ND <0.0017 ND <0.0018 ND <0.0015 ND <0.0014 0.0063 82
Toluene EPA 8260B 108-88-3 mg/kg ND <0.0023 ND <0.0016 ND <0.0018 ND <0.0025 ND <0.0018 ND <0.0019 ND <0.0016 ND <0.0015 8.3 9700
trans-1,2-Dichloroethene EPA 8260B 156-60-5 mg/kg ND <0.0025 ND <0.0017 ND <0.0019 ND <0.0026 ND <0.0019 ND <0.0020 ND <0.0017 ND <0.0016 0.62 4700
trans-1,3-Dichloropropene EPA 8260B 10061-02-6 mg/kg ND <0.0019 ND <0.0014 ND <0.0015 ND <0.0021 ND <0.0015 ND <0.0016 ND <0.0013 ND <0.0012 NE NE
Trichloroethene EPA 8260B 79-01-6 mg/kg ND <0.0027 ND <0.0019 ND <0.0021 ND <0.0029 ND <0.0021 ND <0.0022 ND <0.0019 ND <0.0017 0.021 4
Trichlorofluoromethane EPA 8260B 75-69-4 mg/kg ND <0.0029 ND <0.0020 ND <0.0022 ND <0.0031 ND <0.0022 ND <0.0024 ND <0.0019 ND <0.0018 25 70000
Vinyl acetate EPA 8260B 108-05-4 mg/kg ND <0.0114 ND <0.0079 ND <0.0086 ND <0.0122 ND <0.0088 ND <0.0094 ND <0.0078 ND <0.0072 0.37 820
Vinyl chloride EPA 8260B 75-01-4 mg/kg ND <0.0023 ND <0.0016 ND <0.0018 ND <0.0025 ND <0.0018 ND <0.0019 ND <0.0016 ND <0.0015 0.00024 1.7
Xylene (Total)EPA 8260B 1330-20-7 mg/kg ND <0.0047 ND <0.0033 ND <0.0035 ND <0.0050 ND <0.0036 ND <0.0038 ND <0.0032 ND <0.0030 9.9 530
ND - The analyte was not detected above laboratory detection limits. Subscript indicates compound-specific MDL in mg/kg.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NCDEQ Preliminary Soil Remediation Goals (PSRG) - February 2018
NE - Not established.
0.0050 J 0.0040 J
0.0073
0.0022 J
0.0332 J 0.0157 J 0.0286 J 0.231 0.0772 J
0.11
1.37 0.0037 J 0.267 0.031 5.12 0.0047 J 0.166
0.0855 0.021 1.24 0.0106 J
1.27 0.0031 J 0.158 0.0053 J 5.17 0.0056 J
0.0025 J
0.118 0.0060 J 0.66 0.0084 J
0.51 0.228 1.61 0.0904
0.163 0.0661 0.56 0.0078 J
1.67 0.0040 J 0.3 5.9 0.0053 J 0.198
0.395 0.0925
0.857 0.349 2.85 0.194
0.298 0.0020 J
0.539 0.266 1.74 0.0033 J 0.0949
1.19 0.0027 J 0.537 0.0123 4.07 0.0025 J
0.153 0.0016 J
0.929 0.0020 J 0.29 2.54 0.0023 J 0.134
0.892 0.0022 J 0.235 0.0635 2.97 0.0023 J
0.0492 0.0084 J 0.0080 J 0.0999 0.0059 J
0.345 0.0366 0.0065 J 1.32 0.0345
0.107 0.0287 0.0061 J 0.42 0.0092 J
0.166 0.0104 J 0.0044 J 0.765 0.0126
17.9 17.6
0.118 0.0174 0.0046 J 0.243 0.0074 J
17.8 17.1 16.8 19.4 14.7 18.4
9/24/2018 9/24/2018
14:25 14:30 14:40 14:45 15:00 15:05 15:30 15:35
9/24/2018 9/24/2018 9/24/2018 9/24/2018 9/24/2018 9/24/2018
Soil Soil Soil Soil Gravel Gravel Gravel Gravel
0'-1'4'-5'0'-1'4'-5'0'-1'4'-5'0'-1'4'-5'
N/A N/A N/A N/A 4"4"6"6"
Table 2-2
Soil Sample Analytical Results
Former Maintenance Shop Area
Badin Business Park Facility
Badin, North Carolina
MSA-SB001
(0'-1')
MSA-SB001
(4'-5')
MSA-SB002
(0'-1')
MSA-SB002
(4'-5')
MSA-SB003
(0'-1')
MSA-SB003
(4'-5')
MSA-SB004
(0'-1')
MSA-SB004
(4'-5')
Sample ID Method CAS Units
PSRG
Prot. of GW
PSRG
Ind/Comm
Surface Material
Thickness of Surface Material
Sample Depth Below Surface Material
Date
Time
Percent Moisture ASTM D2974-87 %
PCB-1016 (Aroclor 1016)EPA 8082 12674-11-2 mg/kg ND <0.0177 ND <0.0175 ND <0.0184 ND <0.0181 0.94 10
PCB-1221 (Aroclor 1221)EPA 8082 11104-28-2 mg/kg ND <0.0177 ND <0.0175 ND <0.0184 ND <0.0181 0.0059 0.84
PCB-1232 (Aroclor 1232)EPA 8082 11141-16-5 mg/kg ND <0.0177 ND <0.0175 ND <0.0184 ND <0.0181 0.0059 0.73
PCB-1242 (Aroclor 1242)EPA 8082 53469-21-9 mg/kg ND <0.0177 ND <0.0175 ND <0.0184 ND <0.0181 0.055 0.95
PCB-1248 (Aroclor 1248)EPA 8082 12672-29-6 mg/kg ND <0.0177 ND <0.0175 ND <0.0184 ND <0.0181 0.054 0.96
PCB-1254 (Aroclor 1254)EPA 8082 11097-69-1 mg/kg ND <0.0177 ND <0.0175 ND <0.0184 ND <0.0181 0.091 0.97
PCB-1260 (Aroclor 1260)EPA 8082 11096-82-5 mg/kg ND <0.0177 ND <0.0175 ND <0.0184 ND <0.0181 0.24 0.99
Total Polychlorinated Biphenyls mg/kg 0.055 0.95
1-Methylnaphthalene EPA 8270 90-12-0 mg/kg ND <0.0015 ND <0.0014 0.11 73
2-Methylnaphthalene EPA 8270 91-57-6 mg/kg ND <0.0014 ND <0.0013 3.1 600
Acenaphthene EPA 8270 83-32-9 mg/kg ND <0.0019 ND <0.0018 16 9000
Acenaphthylene EPA 8270 208-96-8 mg/kg ND <0.0015 ND <0.0016 ND <0.0015 NE NE
Anthracene EPA 8270 120-12-7 mg/kg ND <0.0017 ND <0.0017 1300 45000
Benzo(a)anthracene EPA 8270 56-55-3 mg/kg ND <0.00084 0.35 21
Benzo(a)pyrene EPA 8270 50-32-8 mg/kg ND <0.0013 0.12 2.1
Benzo(b)fluoranthene EPA 8270 205-99-2 mg/kg ND <0.00079 1.2 21
Benzo(g,h,i)perylene EPA 8270 191-24-2 mg/kg ND <0.0031 NE NE
Benzo(k)fluoranthene EPA 8270 207-08-9 mg/kg ND <0.0018 12 210
Chrysene EPA 8270 218-01-9 mg/kg ND <0.0021 36 2100
Dibenz(a,h)anthracene EPA 8270 53-70-3 mg/kg ND <0.0022 ND <0.0021 0.38 2.1
Fluoranthene EPA 8270 206-44-0 mg/kg ND <0.00098 670 6000
Fluorene EPA 8270 86-73-7 mg/kg ND <0.0020 ND <0.0019 110 6000
Indeno(1,2,3-cd)pyrene EPA 8270 193-39-5 mg/kg ND <0.0035 ND <0.0033 3.9 21
Naphthalene EPA 8270 91-20-3 mg/kg ND <0.0029 ND <0.0027 0.39 18
Phenanthrene EPA 8270 85-01-8 mg/kg ND <0.0018 NE NE
Pyrene EPA 8270 129-00-0 mg/kg ND <0.0021 440 4500
ND - The analyte was not detected above laboratory detection limits. Subscript indicates compound-specific MDL in mg/kg.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NCDEQ Preliminary Soil Remediation Goals (PSRG) - February 2018
NE - Not established.
Table 2-3
Soil Sample Analytical Results
Former Cathode Plant Area
Badin Business Park Facility
Badin, North Carolina
CAT-SB001
(4'-5')
2.73 0.337
ND
0.504
0.0474
0.0529
0.235
0.0162
0.906
0.308
Crushed Concrete
0'-1'4'-5'
CAT-SB001
(0'-1')
Crushed Concrete
3.47
1.33
0.429
0.0051 J
0.0036 J
0.0089 J
0.0039 J
4.15
2.23
2.59
0.0109 J
0.338
0.013
0.203
0.0133
0.261
3.85
0.997
2.62
1.18
0.446
0.282
0.0595
0.0037 J
0.0031 J
0.0070 J
0.0106 J
ND
0.53
0.212
0.169
0.0059 J
0.0099 J
0.0173
0.0812
0.0177
NDND
CAT-SB002
(4'-5')
Crushed Concrete
4'-5'
9/25/2018
8:45
19.4
CAT-SB002
(0'-1')
Crushed Concrete
9/25/2018
8:40
0'-1'
6"6"6"6"
16.6
9/25/2018
8:30
15.7 15.6
9/25/2018
8:25
Sample ID Method CAS Units
PSRG
Prot. of GW
PSRG
Ind/Comm
Surface Material
Thickness of Surface Material
Sample Depth Below Surface Material
Date
Time
Percent Moisture ASTM D2974-87 %
PCB-1016 (Aroclor 1016)EPA 8082 12674-11-2 mg/kg ND <0.0179 ND <0.0169 ND <0.0169 ND <0.0183 0.94 10
PCB-1221 (Aroclor 1221)EPA 8082 11104-28-2 mg/kg ND <0.0179 ND <0.0169 ND <0.0169 ND <0.0183 0.0059 0.84
PCB-1232 (Aroclor 1232)EPA 8082 11141-16-5 mg/kg ND <0.0179 ND <0.0169 ND <0.0183 0.0059 0.73
PCB-1242 (Aroclor 1242)EPA 8082 53469-21-9 mg/kg ND <0.0169 ND <0.0169 ND <0.0183 0.055 0.95
PCB-1248 (Aroclor 1248)EPA 8082 12672-29-6 mg/kg ND <0.0179 ND <0.0169 ND <0.0169 ND <0.0183 0.054 0.96
PCB-1254 (Aroclor 1254)EPA 8082 11097-69-1 mg/kg ND <0.0179 ND <0.0169 ND <0.0169 ND <0.0183 0.091 0.97
PCB-1260 (Aroclor 1260)EPA 8082 11096-82-5 mg/kg ND <0.0179 ND <0.0169 ND <0.0169 ND <0.0183 0.24 0.99
Total Polychlorinated Biphenyls mg/kg 0.055 0.95
1-Methylnaphthalene EPA 8270 90-12-0 mg/kg ND <0.0014 0.11 73
2-Methylnaphthalene EPA 8270 91-57-6 mg/kg 3.1 600
Acenaphthene EPA 8270 83-32-9 mg/kg ND <0.0018 16 9000
Acenaphthylene EPA 8270 208-96-8 mg/kg ND <0.0015 ND <0.0016 NE NE
Anthracene EPA 8270 120-12-7 mg/kg 1300 45000
Benzo(a)anthracene EPA 8270 56-55-3 mg/kg 0.35 21
Benzo(a)pyrene EPA 8270 50-32-8 mg/kg 0.12 2.1
Benzo(b)fluoranthene EPA 8270 205-99-2 mg/kg 1.2 21
Benzo(g,h,i)perylene EPA 8270 191-24-2 mg/kg NE NE
Benzo(k)fluoranthene EPA 8270 207-08-9 mg/kg 12 210
Chrysene EPA 8270 218-01-9 mg/kg 36 2100
Dibenz(a,h)anthracene EPA 8270 53-70-3 mg/kg ND <0.0022 0.38 2.1
Fluoranthene EPA 8270 206-44-0 mg/kg 670 6000
Fluorene EPA 8270 86-73-7 mg/kg ND <0.0019 110 6000
Indeno(1,2,3-cd)pyrene EPA 8270 193-39-5 mg/kg 3.9 21
Naphthalene EPA 8270 91-20-3 mg/kg ND <0.0028 0.39 18
Phenanthrene EPA 8270 85-01-8 mg/kg NE NE
Pyrene EPA 8270 129-00-0 mg/kg 440 4500
ND - The analyte was not detected above laboratory detection limits. Subscript indicates compound-specific MDL in mg/kg.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NCDEQ Preliminary Soil Remediation Goals (PSRG) - February 2018
NE - Not established.
1.77 0.0245 0.371 0.0041 J
0.559 0.0059 J 0.0473
4.75 0.0561 1.12 0.0103 J
0.155 0.0115 0.0768
3.67 0.0521 0.488 0.0082 J
0.0113 J
2.69 0.0327 0.851 0.0060 J
0.501 0.0075 J 0.04
5.87 0.0709 1.08
4.39 0.0523 1.29 0.0096 J
2.71 0.0355 0.81 0.0060 J
1.17 0.0183 0.338 0.0028 J
1.83 0.0271 0.372 0.0050 J
0.84 0.0887
3.14 0.0351 0.815 0.0063 J
1.06 0.012 0.157 0.0022 J
0.0782 0.0039 J 0.0525 0.0018 J
0.0613 0.0020 J 0.0379
0.199 0.0084 J 0.0596
13:40 13:45 14:05 14:10
9/24/2018 9/24/2018 9/24/2018 9/24/2018
ND
16.0 12.2 11.5 17.2
0.0445
0.018 J
0.018 J ND 0.0445
0'-1'4'-5'0'-1'4'-5'
Crushed Concrete Crushed Concrete Crushed Concrete Crushed Concrete
6"6"6"6"
ANO-SB001
(0'-'1)
ANO-SB002
(4'-5')
ANO-SB002
(0'-1')
ANO-SB002
(4'-5')
Table 2-4
Soil Sample Analytical Results
Former Anode Plant Area
Badin Business Park Facility
Badin, North Carolina
Sample ID Method CAS Units
PSRG
Prot. of GW
PSRG
Ind/Comm
Surface Material
Thickness of Surface Material
Sample Depth Below Surface Material
Date
Time
Percent Moisture ASTM D2974-87 %
1-Methylnaphthalene EPA 8270 90-12-0 mg/kg ND <0.0015 ND <0.0015 ND <0.0015 ND <0.0016 ND <0.0015 0.11 73
2-Methylnaphthalene EPA 8270 91-57-6 mg/kg ND <0.0013 ND <0.0014 ND <0.0014 ND <0.0015 3.1 600
Acenaphthene EPA 8270 83-32-9 mg/kg ND <0.0018 ND <0.0018 ND <0.0019 ND <0.0019 ND <0.0020 ND <0.0019 16 9000
Acenaphthylene EPA 8270 208-96-8 mg/kg ND <0.0016 ND <0.0016 ND <0.0016 ND <0.0016 ND <0.0015 ND <0.0018 NE NE
Anthracene EPA 8270 120-12-7 mg/kg ND <0.0017 ND <0.0018 ND <0.0018 ND <0.0019 1300 45000
Benzo(a)anthracene EPA 8270 56-55-3 mg/kg ND <0.00087 ND <0.00096 0.35 21
Benzo(a)pyrene EPA 8270 50-32-8 mg/kg ND <0.0013 ND <0.0014 ND <0.0015 0.12 2.1
Benzo(b)fluoranthene EPA 8270 205-99-2 mg/kg ND <0.00082 ND <0.00090 1.2 21
Benzo(g,h,i)perylene EPA 8270 191-24-2 mg/kg ND <0.0032 ND <0.0033 ND <0.0033 ND <0.0035 NE NE
Benzo(k)fluoranthene EPA 8270 207-08-9 mg/kg ND <0.0018 ND <0.0019 ND <0.0019 ND <0.0020 12 210
Chrysene EPA 8270 218-01-9 mg/kg ND <0.0022 ND <0.0023 ND <0.0024 36 2100
Dibenz(a,h)anthracene EPA 8270 53-70-3 mg/kg ND <0.0022 ND <0.0023 ND <0.0023 ND <0.0024 ND <0.0022 0.38 2.1
Fluoranthene EPA 8270 206-44-0 mg/kg ND <0.0010 ND <0.0010 ND <0.0011 670 6000
Fluorene EPA 8270 86-73-7 mg/kg ND <0.0019 ND <0.0020 ND <0.0020 ND <0.0020 ND <0.0022 ND <0.0020 110 6000
Indeno(1,2,3-cd)pyrene EPA 8270 193-39-5 mg/kg ND <0.0034 ND <0.0035 ND <0.0035 ND <0.0038 3.9 21
Naphthalene EPA 8270 91-20-3 mg/kg ND <0.0028 ND <0.0029 ND <0.0029 ND <0.0031 ND <0.0028 0.39 18
Phenanthrene EPA 8270 85-01-8 mg/kg ND <0.0018 ND <0.0019 ND <0.0019 ND <0.0020 NE NE
Pyrene EPA 8270 129-00-0 mg/kg ND <0.0022 ND <0.0023 ND <0.0024 440 4500
Cyanide EPA 9012 57-12-5 mg/kg ND <0.17 ND <0.18 ND <0.18 ND <0.17 ND <0.18 ND <0.17 ND <0.19 ND <0.18 14 31
Fluoride EPA 9056 16984-48-8 mg/kg ND <3.1 ND <31.6 ND <3.1 ND <3.3 6000 9300
ND - The analyte was not detected above laboratory detection limits. Subscript indicates compound-specific MDL in mg/kg.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NCDEQ Preliminary Soil Remediation Goals (PSRG) - February 2018
NE - Not established.
Badin, North Carolina
Badin Business Park Facility
Former Potline and Bath Crushing Areas
Soil Sample Analytical Results
Table 2-5
218 33.1 24 24.6 J 161
0.31 J
0.0355 0.0761 0.0029 J 0.0789 2.35 0.0245
0.0127 0.0524 0.072 3.03 0.0080 J
0.0028 J 0.0090 J 0.0486 0.158
0.0526 0.043 0.0245 0.683 0.0126
0.0030 J 0.0111 J 0.224
0.0382 0.0923 0.0031 J 0.084 3.37 0.0288
0.0047 J 0.0037 J 0.0087 J 0.0853
0.0375 0.0774 0.0034 J 0.0541 1.57 0.0196
0.0319 0.0376 0.0237 0.884 0.0091 J
0.0594 0.0474 0.0275 0.64 0.0136
0.03320.0948 0.121 0.0010 J 0.0029 J 0.0739 2.28
0.01810.0501 0.0549 0.0016 J 0.0502 1.24
0.0328 0.0649 0.0029 J 0.0017 J 0.0492 1.75 0.0175
0.0025 J 0.0103 J 0.0146 0.76 0.0022 J
0.0031 J 0.0096 J 0.247
0.0022 J 0.0082 J 0.0022 J
0.0031 J 0.0105 J 0.0332 0.326 0.0019 J
16.5 18.3 20.8 19.2 19.8
0.0020 J 0.0114 J 0.0197 0.256
9:45 10:40 10:45 11:45
17.8 16.8 25.4 17.8
9:05 9:10 9:20 9:25 9:40
9/25/2018 9/25/2018 9/25/2018 9/25/20189/25/2018 9/25/2018 9/25/2018 9/25/2018 9/25/2018
4'-5'0'-1'4'-5'0'-1'0'-1'4'-5'0'-1'4'-5'0'-1'
1"1"8"8"7"
Concrete/Gravel Concrete/Gravel Concrete/Gravel Concrete/Gravel
PBC-SB003
(4'-5')
PBC-SB004
(0'-1')
PBC-SB004
(4'-5')
PBC-SB005
(0'-1')
PBC-SB001
(0'-1')
PBC-SB001
(4'-5')
PBC-SB002
(0'-1')
PBC-SB002
(4'-5')
PBC-SB003
(0'-1')
Gravel Gravel Concrete/Gravel Concrete/Gravel Concrete/Gravel
7"6"6"4"
Sample ID Method CAS Units
PSRG
Prot. of GW
PSRG
Ind/Comm
Surface Material
Thickness of Surface Material
Sample Depth Below Surface Material
Date
Time
Percent Moisture ASTM D2974-87 %
1-Methylnaphthalene EPA 8270 90-12-0 mg/kg ND <0.0014 ND <0.0013 ND <0.0014 ND <0.0014 0.11 73
2-Methylnaphthalene EPA 8270 91-57-6 mg/kg ND <0.0013 ND <0.0012 ND <0.0013 ND <0.0013 3.1 600
Acenaphthene EPA 8270 83-32-9 mg/kg ND <0.0018 ND <0.0018 ND <0.0019 ND <0.0019 ND <0.0016 ND <0.0017 ND <0.0018 16 9000
Acenaphthylene EPA 8270 208-96-8 mg/kg ND <0.0015 ND <0.0017 ND <0.0016 ND <0.0014 ND <0.0015 ND <0.0015 ND <0.0016 NE NE
Anthracene EPA 8270 120-12-7 mg/kg ND <0.0017 ND <0.0018 ND <0.0015 ND <0.0016 ND <0.0017 1300 45000
Benzo(a)anthracene EPA 8270 56-55-3 mg/kg ND <0.00077 ND <0.00082 0.35 21
Benzo(a)pyrene EPA 8270 50-32-8 mg/kg ND <0.0012 ND <0.0013 0.12 2.1
Benzo(b)fluoranthene EPA 8270 205-99-2 mg/kg ND <0.00072 ND <0.00077 1.2 21
Benzo(g,h,i)perylene EPA 8270 191-24-2 mg/kg ND <0.0034 ND <0.0028 ND <0.0030 NE NE
Benzo(k)fluoranthene EPA 8270 207-08-9 mg/kg ND <0.0019 ND <0.0016 ND <0.0017 12 210
Chrysene EPA 8270 218-01-9 mg/kg ND <0.0019 ND <0.0021 36 2100
Dibenz(a,h)anthracene EPA 8270 53-70-3 mg/kg ND <0.0021 ND <0.0021 ND <0.0023 ND <0.0019 ND <0.0021 0.38 2.1
Fluoranthene EPA 8270 206-44-0 mg/kg ND <0.00090 ND <0.00096 670 6000
Fluorene EPA 8270 86-73-7 mg/kg ND <0.0019 ND <0.0019 ND <0.0021 ND <0.0020 ND <0.0017 ND <0.0018 ND <0.0019 110 6000
Indeno(1,2,3-cd)pyrene EPA 8270 193-39-5 mg/kg ND <0.0033 ND <0.0036 ND <0.0030 ND <0.0032 3.9 21
Naphthalene EPA 8270 91-20-3 mg/kg ND <0.0027 ND <0.0027 ND <0.0025 ND <0.0027 ND <0.0028 0.39 18
Phenanthrene EPA 8270 85-01-8 mg/kg ND <0.0016 ND <0.0017 NE NE
Pyrene EPA 8270 129-00-0 mg/kg ND <0.0019 ND <0.0021 440 4500
Cyanide EPA 9012 57-12-5 mg/kg ND <0.17 ND <0.17 ND <0.18 ND <0.18 ND <0.15 ND <0.17 ND <0.17 14 31
Fluoride EPA 9056 16984-48-8 mg/kg ND <3.0 ND <3.2 ND <2.6 6000 9300
ND - The analyte was not detected above laboratory detection limits. Subscript indicates compound-specific MDL in mg/kg.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NCDEQ Preliminary Soil Remediation Goals (PSRG) - February 2018
NE - Not established.
47.2 21.3 72.9 35.3 41.3
0.0120 J
0.0232 0.023 0.0036 J 0.0194 0.864 0.0542
0.23 J
0.0065 J 0.0145 0.148
0.0064 J 0.0149 0.0050 J 0.0168 0.843
0.11 0.0064 J
0.0296 0.0041 J 0.958 0.0647
0.12
0.0127 0.336 0.0178
0.356 0.0234
0.0048 J 0.264 0.0184
0.0121 0.0027 J 0.59 0.0355
0.0189
0.0049 J 0.0022 J 0.509 0.0217
0.012 0.0037 J 0.916 0.0475
0.173
0.0024 J
0.0020 J 0.0024 J 0.212
0.0025 J 0.0024 J 0.62
6.3 15.7 13.2 16.7
0.0016 J 0.0084 J 0.0120 J 0.0315
0.0115 J 0.0176 0.0504
9/25/2018 9/25/2018 9/25/2018 9/25/2018
11:50 12:05 13:00 14:25 14:30 14:45
Concrete/Gravel Concrete/Gravel Concrete/Gravel Concrete/Gravel
4"4"4"4"
4'-5'0'-1'4'-5'0'-1'
Table 2-5
Soil Sample Analytical Results
Former Potline and Bath Crushing Areas
Badin Business Park Facility
Badin, North Carolina
PBC-SB007
(4'-5')
PBC-SB008
(0'-1')
PBC-SB008
(4'-5')
PBC-SB009
(0'-1')
0.0105 J
0.0276 0.0227
0.0038 J
0.0196 0.015
0.0116 J 0.0093 J
0.0125 J0.01370.0046 J
0.02460.0313
0.01420.0174
0.0151 0.0141
0.0024 J
12:10 12:55
21.5 21.115.7 14.9
9/25/2018 9/25/20189/25/2018 9/25/2018
4'-5'0'-1'4'-5'0'-1'
Concrete/Gravel Concrete/GravelConcrete/Gravel Concrete/Gravel
PBC-SB006
(0'-1')
PBC-SB006
(4'-5')
PBC-SB007
(0'-1')
4"
PBC-SB005
(4'-5')
4"4"4"
Sample ID Method CAS Units
PSRG
Prot. of GW
PSRG
Ind/Comm
Surface Material
Thickness of Surface Material
Sample Depth Below Surface Material
Date
Time
Percent Moisture ASTM D2974-87 %
1-Methylnaphthalene EPA 8270 90-12-0 mg/kg ND <0.0014 ND <0.0015 ND <0.0014 ND <0.0015 ND <0.0014 ND <0.0014 ND <0.0015 ND <0.0015 0.11 73
2-Methylnaphthalene EPA 8270 91-57-6 mg/kg ND <0.0013 ND <0.0014 ND <0.0013 ND <0.0013 ND <0.0013 ND <0.0013 ND <0.0014 ND <0.0014 3.1 600
Acenaphthene EPA 8270 83-32-9 mg/kg ND <0.0018 ND <0.0019 ND <0.0017 ND <0.0018 ND <0.0017 ND <0.0017 ND <0.0017 ND <0.0019 ND <0.0019 16 9000
Acenaphthylene EPA 8270 208-96-8 mg/kg ND <0.0015 ND <0.0015 ND <0.0016 ND <0.0014 ND <0.0015 ND <0.0015 ND <0.0016 ND <0.0017 NE NE
Anthracene EPA 8270 120-12-7 mg/kg ND <0.0017 ND <0.0016 ND <0.0017 ND <0.0016 ND <0.0016 ND <0.0016 ND <0.0017 ND <0.0018 1300 45000
Benzo(a)anthracene EPA 8270 56-55-3 mg/kg ND <0.00084 ND <0.00083 ND <0.00079 ND <0.00083 ND <0.00081 ND <0.00088 0.35 21
Benzo(a)pyrene EPA 8270 50-32-8 mg/kg ND <0.0013 ND <0.0013 ND <0.0012 ND <0.0013 ND <0.0013 ND <0.0014 ND <0.0014 0.12 2.1
Benzo(b)fluoranthene EPA 8270 205-99-2 mg/kg ND <0.00079 ND <0.00078 ND <0.00074 ND <0.00078 ND <0.00076 ND <0.00083 1.2 21
Benzo(g,h,i)perylene EPA 8270 191-24-2 mg/kg ND <0.0031 ND <0.0030 ND <0.0029 ND <0.0030 ND <0.0030 ND <0.0032 ND <0.0033 NE NE
Benzo(k)fluoranthene EPA 8270 207-08-9 mg/kg ND <0.0018 ND <0.0017 ND <0.0017 ND <0.0017 ND <0.0017 ND <0.0019 ND <0.0019 12 210
Chrysene EPA 8270 218-01-9 mg/kg ND <0.0021 ND <0.0021 ND <0.0020 ND <0.0021 ND <0.0020 ND <0.0022 ND <0.0023 36 2100
Dibenz(a,h)anthracene EPA 8270 53-70-3 mg/kg ND <0.0021 ND <0.0021 ND <0.0022 ND <0.0020 ND <0.0021 ND <0.0020 ND <0.0022 ND <0.0023 0.38 2.1
Fluoranthene EPA 8270 206-44-0 mg/kg ND <0.00098 ND <0.00097 ND <0.00092 ND <0.00096 ND <0.00094 ND <0.0010 ND <0.0011 670 6000
Fluorene EPA 8270 86-73-7 mg/kg ND <0.0019 ND <0.0020 ND <0.0019 ND <0.0019 ND <0.0018 ND <0.0019 ND <0.0018 ND <0.0020 ND <0.0020 110 6000
Indeno(1,2,3-cd)pyrene EPA 8270 193-39-5 mg/kg ND <0.0033 ND <0.0033 ND <0.0031 ND <0.0033 ND <0.0032 ND <0.0035 ND <0.0036 3.9 21
Naphthalene EPA 8270 91-20-3 mg/kg ND <0.0027 ND <0.0029 ND <0.0027 ND <0.0028 ND <0.0027 ND <0.0026 ND <0.0029 ND <0.0029 0.39 18
Phenanthrene EPA 8270 85-01-8 mg/kg ND <0.0018 ND <0.0017 ND <0.0017 ND <0.0017 ND <0.0017 ND <0.0019 ND <0.0019 NE NE
Pyrene EPA 8270 129-00-0 mg/kg ND <0.0021 ND <0.0021 ND <0.0020 ND <0.0021 ND <0.0020 ND <0.0022 ND <0.0023 440 4500
Cyanide EPA 9012 57-12-5 mg/kg ND <0.18 ND <0.18 ND <0.18 ND <0.17 ND <0.16 ND <0.18 ND <0.18 14 31
Fluoride EPA 9056 16984-48-8 mg/kg ND <2.9 ND <3.1 6000 9300
ND - The analyte was not detected above laboratory detection limits. Subscript indicates compound-specific MDL in mg/kg.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NCDEQ Preliminary Soil Remediation Goals (PSRG) - February 2018
NE - Not established.
0.21 J
57.2 11.2 92.3 8.2
0.0027 J
0.0045 J 0.0031 J
0.0191 0.0085 J
0.0286
0.0028 J
0.0197 0.0093 J
0.0692
0.0413 0.0061 J
0.0249 0.0050 J
0.0039 J
0.0234
0.0311 0.0063 J
0.0164
0.0058 J 0.00095 J
0.0017 J
0.0046 J
0.0040 J
0.0365 0.0060 J
0.0080 J
0.0017 J
15.9 48.3 3.7 J
0.18 J
13.2 18.4 20.715.5 19.1 13.6 17.4 11.3 14.5
16:15 16:30 16:3514:50 15:00 15:05 15:30 15:35 16:10
9/25/2018 9/25/2018 9/25/2018
4'-5'0'-1'4'-5'0'-1'2'-3'0'-1'
9/25/2018 9/25/2018 9/25/2018 9/25/2018 9/25/2018 9/25/2018
Concrete/Gravel Concrete/Gravel Concrete/Gravel
4'-5'0'-1'4'-5'
Concrete/Gravel Concrete/Gravel Concrete/Gravel Concrete/Gravel Concrete/Gravel Concrete/Gravel
PBC-SB012
(4'-5')
PBC-SB013
(0'-1')
PBC-SB013
(4'-5')
Soil Sample Analytical Results
Former Potline and Bath Crushing Areas
Badin Business Park Facility
Badin, North Carolina
PBC-SB009
(4'-5')
PBC-SB010
(0'-1')
PBC-SB010
(4'-5')
PBC-SB011
(0'-1')
PBC-SB011
(2'-3')
PBC-SB012
(0'-1')
Table 2-5
4"4"4"4"4"4"4"4"4"
Sample ID Method CAS Units
PSRG
Prot. of GW
PSRG
Ind/Comm
Surface Material
Thickness of Surface Material
Sample Depth Below Surface Material
Date
Time
Percent Moisture ASTM D2974-87 %
1-Methylnaphthalene EPA 8270 90-12-0 mg/kg ND <0.0016 ND <0.0014 ND <0.0014 ND <0.0014 ND <0.0014 ND <0.0015 0.11 73
2-Methylnaphthalene EPA 8270 91-57-6 mg/kg ND <0.0015 ND <0.0013 ND <0.0013 ND <0.0013 ND <0.0013 ND <0.0013 3.1 600
Acenaphthene EPA 8270 83-32-9 mg/kg ND <0.0019 ND <0.0020 ND <0.0018 ND <0.0017 ND <0.0017 ND <0.0017 ND <0.0018 ND <0.0018 16 9000
Acenaphthylene EPA 8270 208-96-8 mg/kg ND <0.0018 ND <0.0016 ND <0.0015 ND <0.0015 ND <0.0015 ND <0.0016 ND <0.0016 NE NE
Anthracene EPA 8270 120-12-7 mg/kg ND <0.0019 ND <0.0017 ND <0.0016 ND <0.0016 ND <0.0016 ND <0.0017 ND <0.0017 1300 45000
Benzo(a)anthracene EPA 8270 56-55-3 mg/kg ND <0.00096 ND <0.00083 ND <0.00083 ND <0.00082 ND <0.00087 0.35 21
Benzo(a)pyrene EPA 8270 50-32-8 mg/kg ND <0.0015 ND <0.0013 ND <0.0013 ND <0.0013 ND <0.0013 0.12 2.1
Benzo(b)fluoranthene EPA 8270 205-99-2 mg/kg ND <0.00091 ND <0.00078 ND <0.00078 ND <0.00078 ND <0.00082 1.2 21
Benzo(g,h,i)perylene EPA 8270 191-24-2 mg/kg ND <0.0035 ND <0.0032 ND <0.0030 ND <0.0030 ND <0.0030 ND <0.0032 NE NE
Benzo(k)fluoranthene EPA 8270 207-08-9 mg/kg ND <0.0020 ND <0.0018 ND <0.0017 ND <0.0017 ND <0.0017 ND <0.0018 12 210
Chrysene EPA 8270 218-01-9 mg/kg ND <0.0024 ND <0.0021 ND <0.0021 ND <0.0021 ND <0.0022 36 2100
Dibenz(a,h)anthracene EPA 8270 53-70-3 mg/kg ND <0.0024 ND <0.0022 ND <0.0021 ND <0.0021 ND <0.0021 ND <0.0022 ND <0.0022 0.38 2.1
Fluoranthene EPA 8270 206-44-0 mg/kg ND <0.0011 ND <0.00097 ND <0.00097 ND <0.00096 ND <0.0010 670 6000
Fluorene EPA 8270 86-73-7 mg/kg ND <0.0020 ND <0.0022 ND <0.0020 ND <0.0019 ND <0.0019 ND <0.0019 ND <0.0019 ND <0.0020 110 6000
Indeno(1,2,3-cd)pyrene EPA 8270 193-39-5 mg/kg ND <0.0038 ND <0.0034 ND <0.0033 ND <0.0033 ND <0.0032 ND <0.0034 3.9 21
Naphthalene EPA 8270 91-20-3 mg/kg ND <0.0031 ND <0.0027 ND <0.0027 ND <0.0027 ND <0.0028 ND <0.0028 0.39 18
Phenanthrene EPA 8270 85-01-8 mg/kg ND <0.0020 ND <0.0017 ND <0.0017 ND <0.0017 ND <0.0018 NE NE
Pyrene EPA 8270 129-00-0 mg/kg ND <0.0024 ND <0.0021 ND <0.0021 ND <0.0021 ND <0.0022 440 4500
Cyanide EPA 9012 57-12-5 mg/kg ND <0.18 ND <0.20 ND <0.18 ND <0.17 ND <0.17 ND <0.17 ND <0.18 ND <0.18 14 31
Fluoride EPA 9056 16984-48-8 mg/kg ND <3.0 6000 9300
ND - The analyte was not detected above laboratory detection limits. Subscript indicates compound-specific MDL in mg/kg.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NCDEQ Preliminary Soil Remediation Goals (PSRG) - February 2018
NE - Not established.
66
0.0049 J
0.0592 0.0038 J 0.0214
57.3 33.3 149 39 8.5 42.5 J
0.0063 J
0.0446 0.013
0.0028 J
0.0709 0.0159
0.0287 0.0060 J
0.0088 J 0.0088 J
0.0093 J
0.043 0.0029 J 0.0022 J
0.0723 0.0172
0.0293 0.0067 J
9:40 9:45 10:35 10:40
14.3 14 17.4 18.2
0.0119 J 0.0124
4"4"6"6"
0'-1'4'-5'0'-1'4'-5'
9/26/2018 9/26/2018 9/26/2018 9/26/2018
PBC-SB014
(0'-1')
PBC-SB014
(4'-5')
PBC-SB015
(0'-1')
PBC-SB015
(4'-5')
PBC-SB016
(0'-1')
PBC-SB016
(4'-5')
PBC-SB017
(0'-1')
PBC-SB017
(4'-5')
Concrete/Gravel Concrete/Gravel Concrete/Gravel Concrete/Gravel Concrete/Gravel Concrete/Gravel Crushed Concrete Crushed Concrete
Table 2-5
Soil Sample Analytical Results
Former Potline and Bath Crushing Areas
0.0047 J
25.818.5
0.0047 J
0.0055 J
0.0381 0.0028 J
0.0037 J
0.0207
0.027
0.0043 J
0.0064 J
0.0101 J 0.0087 J
19.5 15.4
0'-1'4'-5'
8:50 8:558:15 8:20
4'-5'0'-1'
4"4"4"4"
Badin Business Park Facility
Badin, North Carolina
9/26/2018 9/26/2018 9/26/2018 9/26/2018
Sample ID Method CAS Units
PSRG
Prot. of GW
PSRG
Ind/Comm
Surface Material
Thickness of Surface Material
Sample Depth Below Surface Material
Date
Time
Percent Moisture ASTM D2974-87 %
1-Methylnaphthalene EPA 8270 90-12-0 mg/kg ND <0.0014 ND <0.0366 ND <0.0075 0.11 73
2-Methylnaphthalene EPA 8270 91-57-6 mg/kg ND <0.0013 ND <0.0336 3.1 600
Acenaphthene EPA 8270 83-32-9 mg/kg ND <0.0018 16 9000
Acenaphthylene EPA 8270 208-96-8 mg/kg ND <0.0016 ND <0.0081 NE NE
Anthracene EPA 8270 120-12-7 mg/kg ND <0.0017 1300 45000
Benzo(a)anthracene EPA 8270 56-55-3 mg/kg 0.35 21
Benzo(a)pyrene EPA 8270 50-32-8 mg/kg 0.12 2.1
Benzo(b)fluoranthene EPA 8270 205-99-2 mg/kg 1.2 21
Benzo(g,h,i)perylene EPA 8270 191-24-2 mg/kg ND <0.0031 NE NE
Benzo(k)fluoranthene EPA 8270 207-08-9 mg/kg ND <0.0018 12 210
Chrysene EPA 8270 218-01-9 mg/kg 36 2100
Dibenz(a,h)anthracene EPA 8270 53-70-3 mg/kg ND <0.0022 0.38 2.1
Fluoranthene EPA 8270 206-44-0 mg/kg 670 6000
Fluorene EPA 8270 86-73-7 mg/kg ND <0.0019 110 6000
Indeno(1,2,3-cd)pyrene EPA 8270 193-39-5 mg/kg ND <0.0034 3.9 21
Naphthalene EPA 8270 91-20-3 mg/kg ND <0.0028 ND <0.0702 ND <0.0144 0.39 18
Phenanthrene EPA 8270 85-01-8 mg/kg ND <0.0018 NE NE
Pyrene EPA 8270 129-00-0 mg/kg ND <0.0022 440 4500
ND - The analyte was not detected above laboratory detection limits. Subscript indicates compound-specific MDL in mg/kg.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NCDEQ Preliminary Soil Remediation Goals (PSRG) - February 2018
NE - Not established.
0.19 1.61 0.372
0.0028 J
0.0642 0.795 0.194
0.0776 0.563 0.199
0.0029 J 0.0388 J 0.0119 J
0.214 0.0014 J 1.84 0.432
0.0251 0.186 0.0628
0.15 0.0026 J 1.14 0.305
0.0903 0.538 0.171
0.0791 0.623 0.22
0.211 0.0021 J 1.51 0.474
0.128 0.0015 J 1.05 0.325
0.129 0.0015 J 1.18 0.287
0.0021 J 0.0152 J
0.0156 0.257 0.0541 J
0.0022 J 0.0076 J
0.0046 J 0.063 0.0166 J
0.0030 J
16.7 16.7 17.3 18.8
0'-1'4'-5'0'-1'4'-5'
17:45 17:50 18:00 18:05
9/24/2018 9/24/2018 9/24/2018 9/24/2018
ABR-SB001
(0'-1')
ABR-SB001
(4'-5')
ABR-SB002
(0'-1')
ABR-SB002
(4'-5')
Table 2-6
Soil Sample Analytical Results
Former Anode Butt Reclamation Area
Badin Business Park Facility
Badin, North Carolina
Crushed Concrete Crushed Concrete Crushed Concrete Crushed Concrete
2"2"4"4"
Sample ID Method CAS Units
PSRG
Prot. of GW
PSRG
Ind/Comm
Surface Material
Thickness of Surface Material
Sample Depth Below Surface Material
Date
Time
Percent Moisture ASTM D2974-87 %
1-Methylnaphthalene EPA 8270 90-12-0 mg/kg ND <0.0014 0.11 73
2-Methylnaphthalene EPA 8270 91-57-6 mg/kg ND <0.0013 3.1 600
Acenaphthene EPA 8270 83-32-9 mg/kg ND <0.0018 ND <0.0018 16 9000
Acenaphthylene EPA 8270 208-96-8 mg/kg ND <0.0015 ND <0.0016 NE NE
Anthracene EPA 8270 120-12-7 mg/kg ND <0.0017 1300 45000
Benzo(a)anthracene EPA 8270 56-55-3 mg/kg 0.35 21
Benzo(a)pyrene EPA 8270 50-32-8 mg/kg 0.12 2.1
Benzo(b)fluoranthene EPA 8270 205-99-2 mg/kg 1.2 21
Benzo(g,h,i)perylene EPA 8270 191-24-2 mg/kg ND <0.0031 NE NE
Benzo(k)fluoranthene EPA 8270 207-08-9 mg/kg ND <0.0018 12 210
Chrysene EPA 8270 218-01-9 mg/kg 36 2100
Dibenz(a,h)anthracene EPA 8270 53-70-3 mg/kg ND <0.0021 ND <0.0022 0.38 2.1
Fluoranthene EPA 8270 206-44-0 mg/kg 670 6000
Fluorene EPA 8270 86-73-7 mg/kg ND <0.0019 ND <0.0019 110 6000
Indeno(1,2,3-cd)pyrene EPA 8270 193-39-5 mg/kg ND <0.0033 3.9 21
Naphthalene EPA 8270 91-20-3 mg/kg ND <0.0027 0.39 18
Phenanthrene EPA 8270 85-01-8 mg/kg ND <0.0018 NE NE
Pyrene EPA 8270 129-00-0 mg/kg 440 4500
ND - The analyte was not detected above laboratory detection limits. Subscript indicates compound-specific MDL in mg/kg.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NCDEQ Preliminary Soil Remediation Goals (PSRG) - February 2018
NE - Not established.
Crushed Concrete
2"2"2"
Table 2-7
Soil Sample Analytical Results
Former Carbon Bake Furnace Area
Badin Business Park Facility
Badin, North Carolina
17.6 15.9
9/24/2018
17:10
24.3
9/24/2018
17:20
0'-1'
Crushed Concrete Crushed Concrete
9/24/2018
17:15
CBF-SB001
(0'-1')
CBF-SB001
(4'-5')
Crushed Concrete
0'-1'4'-5'
0.0194
0.186
0.0732
0.0272
0.278
0.0105 J
0.597
0.397
0.48
0.0272
0.0198
0.0481
0.0055 J
0.662
0.223
0.424
0.497
0.204
CBF-SB002
(4'-5')
4'-5'
9/24/2018
17:25
17.7
0.0136
0.0341
0.0144
0.237
0.39
0.123 0.025
0.0185
CBF-SB002
(0'-1')
0.312
0.0229
0.0385
0.0159
0.0222
0.0266
0.0369
0.0494
0.0286
0.0174
0.0375
0.0422
0.0038 J
0.129
0.124
2"
0.0027 J
0.0076 J
0.0109 J
0.0039 J
0.0106 J
0.0072 J
0.135
0.362
0.0026 J
0.0033 J
0.0038 J
0.0032 J
0.0027 J
0.23
0.235
Sample ID Method CAS Units
PSRG
Prot. of GW
PSRG
Ind/Comm
Surface Material
Thickness of Surface Material
Sample Depth Below Surface Material
Date
Time
Percent Moisture ASTM D2974-87 %
PCB-1016 (Aroclor 1016)EPA 8082 12674-11-2 mg/kg ND <0.0172 ND <0.0172 ND <0.0167 ND <0.0177 0.94 10
PCB-1221 (Aroclor 1221)EPA 8082 11104-28-2 mg/kg ND <0.0172 ND <0.0172 ND <0.0167 ND <0.0177 0.0059 0.84
PCB-1232 (Aroclor 1232)EPA 8082 11141-16-5 mg/kg ND <0.0172 ND <0.0172 ND <0.0167 ND <0.0177 0.0059 0.73
PCB-1242 (Aroclor 1242)EPA 8082 53469-21-9 mg/kg ND <0.0172 ND <0.0172 ND <0.0167 ND <0.0177 0.055 0.95
PCB-1248 (Aroclor 1248)EPA 8082 12672-29-6 mg/kg ND <0.0172 ND <0.0172 ND <0.0167 ND <0.0177 0.054 0.96
PCB-1254 (Aroclor 1254)EPA 8082 11097-69-1 mg/kg ND <0.0172 ND <0.0172 ND <0.0167 ND <0.0177 0.091 0.97
PCB-1260 (Aroclor 1260)EPA 8082 11096-82-5 mg/kg ND <0.0172 ND <0.0172 ND <0.0167 ND <0.0177 0.24 0.99
Total Polychlorinated Biphenyls mg/kg 0.055 0.95
1-Methylnaphthalene EPA 8270 90-12-0 mg/kg ND <0.0014 ND <0.0013 ND <0.0014 0.11 73
2-Methylnaphthalene EPA 8270 91-57-6 mg/kg ND <0.0013 ND <0.0012 3.1 600
Acenaphthene EPA 8270 83-32-9 mg/kg ND <0.0017 ND <0.0017 ND <0.0018 16 9000
Acenaphthylene EPA 8270 208-96-8 mg/kg ND <0.0015 ND <0.0015 ND <0.0015 NE NE
Anthracene EPA 8270 120-12-7 mg/kg ND <0.0016 ND <0.0016 1300 45000
Benzo(a)anthracene EPA 8270 56-55-3 mg/kg ND <0.00083 0.35 21
Benzo(a)pyrene EPA 8270 50-32-8 mg/kg ND <0.0013 0.12 2.1
Benzo(b)fluoranthene EPA 8270 205-99-2 mg/kg 1.2 21
Benzo(g,h,i)perylene EPA 8270 191-24-2 mg/kg ND <0.0030 ND <0.0030 NE NE
Benzo(k)fluoranthene EPA 8270 207-08-9 mg/kg ND <0.0017 ND <0.0018 12 210
Chrysene EPA 8270 218-01-9 mg/kg ND <0.0021 36 2100
Dibenz(a,h)anthracene EPA 8270 53-70-3 mg/kg ND <0.0021 ND <0.0021 0.38 2.1
Fluoranthene EPA 8270 206-44-0 mg/kg ND <0.00097 670 6000
Fluorene EPA 8270 86-73-7 mg/kg ND <0.0019 ND <0.0018 ND <0.0019 110 6000
Indeno(1,2,3-cd)pyrene EPA 8270 193-39-5 mg/kg ND <0.0032 ND <0.0033 3.9 21
Naphthalene EPA 8270 91-20-3 mg/kg ND <0.0027 ND <0.0026 ND <0.0027 0.39 18
Phenanthrene EPA 8270 85-01-8 mg/kg ND <0.0018 NE NE
Pyrene EPA 8270 129-00-0 mg/kg ND <0.0021 440 4500
Cyanide EPA 9012 57-12-5 mg/kg ND <0.17 ND <0.17 ND <0.15 ND <0.17 14 31
Fluoride EPA 9056 16984-48-8 mg/kg ND <2.8 6000 9300
ND - The analyte was not detected above laboratory detection limits. Subscript indicates compound-specific MDL in mg/kg.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
NCDEQ Preliminary Soil Remediation Goals (PSRG) - February 2018
NE - Not established.
15.8 3.6 J 16.4
1.82 0.0033 J 0.0341
0.243
0.407 0.0306
0.0103 J
0.0329
0.0378
1.58
1.46
0.0023 J
0.0032 J
0.605 0.0032 J
0.177 0.0122
1.28 0.0032 J 0.0823
0.462 0.0325
1.06 0.0024 J 0.0753
0.00086 J
0.383 0.0356
1.14 0.0023 J 0.0438
0.827 0.0022 J 0.0513
0.0578
0.0762 0.0014 J
0.31
0.0149
14
ND ND ND ND
12.1 14.1 11.2
9/24/2018 9/24/2018 9/24/2018 9/24/2018
18:15 18:20 18:40 18:45
Crushed Concrete Crushed Concrete Crushed Concrete Crushed Concrete
0'-1'4'-5'0'-1'4'-5'
12"12"6"6"
REC-SB001
(0'-1')
REC-SB001
(4'-5')
REC-SB002
(0'-1')
REC-SB002
(4'-5')
Table 2-8
Soil Sample Analytical Results
Former Rectifier Station Area
Badin Business Park Facility
Badin, North Carolina
Table 2-9
Field Blank Sample Analytical Results
Targeted Sampling Work Plan Implementation
Badin Business Park Facility
Badin, North Carolina
Sample ID Method CAS Units ESW-TB001ESW-EB001Location
Date
Time
PCB-1016 (Aroclor 1016)EPA 8082 12674-11-2 mg/l ND <0.00042
PCB-1221 (Aroclor 1221)EPA 8082 11104-28-2 mg/l ND <0.00042
PCB-1232 (Aroclor 1232)EPA 8082 11141-16-5 mg/l ND <0.00042
PCB-1242 (Aroclor 1242)EPA 8082 53469-21-9 mg/l ND <0.00042
PCB-1248 (Aroclor 1248)EPA 8082 12672-29-6 mg/l ND <0.00042
PCB-1254 (Aroclor 1254)EPA 8082 11097-69-1 mg/l ND <0.00042
PCB-1260 (Aroclor 1260)EPA 8082 11096-82-5 mg/l ND <0.00042
Total Polychlorinated Biphenyls mg/l
1-Methylnaphthalene EPA 8270 90-12-0 mg/l ND <0.00080
2-Methylnaphthalene EPA 8270 91-57-6 mg/l ND <0.00080
Acenaphthene EPA 8270 83-32-9 mg/l ND <0.00050
Acenaphthylene EPA 8270 208-96-8 mg/l ND <0.00050
Anthracene EPA 8270 120-12-7 mg/l ND <0.000050
Benzo(a)anthracene EPA 8270 56-55-3 mg/l ND <0.000050
Benzo(a)pyrene EPA 8270 50-32-8 mg/l ND <0.00010
Benzo(b)fluoranthene EPA 8270 205-99-2 mg/l ND <0.000050
Benzo(g,h,i)perylene EPA 8270 191-24-2 mg/l ND <0.00020
Benzo(k)fluoranthene EPA 8270 207-08-9 mg/l ND <0.00020
Chrysene EPA 8270 218-01-9 mg/l ND <0.00010
Dibenz(a,h)anthracene EPA 8270 53-70-3 mg/l ND <0.00015
Fluoranthene EPA 8270 206-44-0 mg/l ND <0.00030
Fluorene EPA 8270 86-73-7 mg/l ND <0.00031
Indeno(1,2,3-cd)pyrene EPA 8270 193-39-5 mg/l ND <0.000050
Naphthalene EPA 8270 91-20-3 mg/l ND <0.0015
Phenanthrene EPA 8270 85-01-8 mg/l ND <0.00020
Pyrene EPA 8270 129-00-0 mg/l ND <0.00010
1,1,1,2-Tetrachloroethane EPA 8260B 630-20-6 mg/l ND <0.0017 ND <0.0017
1,1,1-Trichloroethane EPA 8260B 71-55-6 mg/l ND <0.0019 ND <0.0019
1,1,2,2-Tetrachloroethane EPA 8260B 79-34-5 mg/l ND <0.0015 ND <0.0015
1,1,2-Trichloroethane EPA 8260B 79-00-5 mg/l ND <0.0017 ND <0.0017
1,1-Dichloroethane EPA 8260B 75-34-3 mg/l ND <0.0018 ND <0.0018
1,1-Dichloroethene EPA 8260B 75-35-4 mg/l ND <0.0019 ND <0.0019
1,1-Dichloropropene EPA 8260B 563-58-6 mg/l ND <0.0017 ND <0.0017
1,2,3-Trichlorobenzene EPA 8260B 87-61-6 mg/l ND <0.0020 ND <0.0020
1,2,3-Trichloropropane EPA 8260B 96-18-4 mg/l ND <0.0015 ND <0.0015
1,2,4-Trichlorobenzene EPA 8260B 120-82-1 mg/l ND <0.0017 ND <0.0017
1,2,4-Trimethylbenzene EPA 8260B 95-63-6 mg/l ND <0.0015 ND <0.0015
1,2-Dibromo-3-chloropropane EPA 8260B 96-12-8 mg/l ND <0.0017 ND <0.0017
1,2-Dibromoethane (EDB)EPA 8260B 106-93-4 mg/l ND <0.0017 ND <0.0017
1,2-Dichlorobenzene EPA 8260B 95-50-1 mg/l ND <0.0015 ND <0.0015
1,2-Dichloroethane EPA 8260B 107-06-2 mg/l ND <0.0018 ND <0.0018
1,2-Dichloroethene (Total)EPA 8260B 540-59-0 mg/l ND <0.0044 ND <0.0044
1,2-Dichloropropane EPA 8260B 78-87-5 mg/l ND <0.0017 ND <0.0017
1,3,5-Trimethylbenzene EPA 8260B 108-67-8 mg/l ND <0.0013 ND <0.0013
1,3-Dichlorobenzene EPA 8260B 541-73-1 mg/l ND <0.0015 ND <0.0015
1,3-Dichloropropane EPA 8260B 142-28-9 mg/l ND <0.0017 ND <0.0017
1,4-Dichlorobenzene EPA 8260B 106-46-7 mg/l ND <0.0015 ND <0.0015
2,2-Dichloropropane EPA 8260B 594-20-7 mg/l ND <0.0016 ND <0.0016
2-Butanone (MEK)EPA 8260B 78-93-3 mg/l ND <0.0049 ND <0.0049
2-Chlorotoluene EPA 8260B 95-49-8 mg/l ND <0.0015 ND <0.0015
2-Hexanone EPA 8260B 591-78-6 mg/l ND <0.0038 ND <0.0038
4-Chlorotoluene EPA 8260B 106-43-4 mg/l ND <0.0016 ND <0.0016
4-Methyl-2-pentanone (MIBK)EPA 8260B 108-10-1 mg/l ND <0.0036 ND <0.0036
Acetone EPA 8260B 67-64-1 mg/l ND <0.0100 ND <0.0100
Benzene EPA 8260B 71-43-2 mg/l ND <0.0017 ND <0.0017
Bromobenzene EPA 8260B 108-86-1 mg/l ND <0.0015 ND <0.0015
Bromochloromethane EPA 8260B 74-97-5 mg/l ND <0.0022 ND <0.0022
Bromodichloromethane EPA 8260B 75-27-4 mg/l ND <0.0017 ND <0.0017
Bromoform EPA 8260B 75-25-2 mg/l ND <0.0015 ND <0.0015
Bromomethane EPA 8260B 74-83-9 mg/l ND <0.0025 ND <0.0025
Carbon tetrachloride EPA 8260B 56-23-5 mg/l ND <0.0019 ND <0.0019
Chlorobenzene EPA 8260B 108-90-7 mg/l ND <0.0017 ND <0.0017
Chloroethane EPA 8260B 75-00-3 mg/l ND <0.0016 ND <0.0016
Chloroform EPA 8260B 67-66-3 mg/l ND <0.0019 ND <0.0019
Chloromethane EPA 8260B 74-87-3 mg/l ND <0.0015 ND <0.0015
cis-1,2-Dichloroethene EPA 8260B 156-59-2 mg/l ND <0.0018 ND <0.0018
cis-1,3-Dichloropropene EPA 8260B 10061-01-5 mg/l ND <0.0016 ND <0.0016
Dibromochloromethane EPA 8260B 124-48-1 mg/l ND <0.0018 ND <0.0018
Dibromomethane EPA 8260B 74-95-3 mg/l ND <0.0020 ND <0.0020
Dichlorodifluoromethane EPA 8260B 75-71-8 mg/l ND <0.0016 ND <0.0016
Diisopropyl ether EPA 8260B 108-20-3 mg/l ND <0.0017 ND <0.0017
Ethylbenzene EPA 8260B 100-41-4 mg/l ND <0.0016 ND <0.0016
Hexachloro-1,3-butadiene EPA 8260B 87-68-3 mg/l ND <0.0018 ND <0.0018
Isopropylbenzene (Cumene)EPA 8260B 98-82-8 mg/l ND <0.0016 ND <0.0016
m&p-Xylene EPA 8260B 179601-23-1 mg/l ND <0.0031 ND <0.0031
Methylene Chloride EPA 8260B 75-09-2 mg/l ND <0.0019 ND <0.0019
Methyl-tert-butyl ether EPA 8260B 1634-04-4 mg/l ND <0.0017 ND <0.0017
Naphthalene EPA 8260B 91-20-3 mg/l ND <0.0020 ND <0.0020
n-Butylbenzene EPA 8260B 104-51-8 mg/l ND <0.0019 ND <0.0019
n-Propylbenzene EPA 8260B 103-65-1 mg/l ND <0.0015 ND <0.0015
o-Xylene EPA 8260B 95-47-6 mg/l ND <0.0016 ND <0.0016
p-Isopropyltoluene EPA 8260B 99-87-6 mg/l ND <0.0016 ND <0.0016
sec-Butylbenzene EPA 8260B 135-98-8 mg/l ND <0.0017 ND <0.0017
Styrene EPA 8260B 100-42-5 mg/l ND <0.0016 ND <0.0016
tert-Butyl Alcohol EPA 8260B 75-65-0 mg/l ND <0.0577 ND <0.0577
tert-Butylbenzene EPA 8260B 98-06-6 mg/l ND <0.0016 ND <0.0016
Tetrachloroethene EPA 8260B 127-18-4 mg/l ND <0.0018 ND <0.0018
Toluene EPA 8260B 108-88-3 mg/l ND <0.0016 ND <0.0016
trans-1,2-Dichloroethene EPA 8260B 156-60-5 mg/l ND <0.0018 ND <0.0018
trans-1,3-Dichloropropene EPA 8260B 10061-02-6 mg/l ND <0.0016 ND <0.0016
Trichloroethene EPA 8260B 79-01-6 mg/l ND <0.0018 ND <0.0018
Trichlorofluoromethane EPA 8260B 75-69-4 mg/l ND <0.0017 ND <0.0017
Vinyl acetate EPA 8260B 108-05-4 mg/l ND <0.0023 ND <0.0023
Vinyl chloride EPA 8260B 75-01-4 mg/l ND <0.0015 ND <0.0015
Cyanide EPA 9012 57-12-5 mg/l ND <0.0040
Fluoride EPA 9056 16984-48-8 mg/l ND <0.005
ND - The analyte was not detected above laboratory detection limits. Subscript indicates compound-specific MDL in mg/l.
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
ND
9/24/2018 9/25/2018
0:00 17:00
NA
NA
NA
NA
NA
Trip Blank Equipment Blank
ENVIRONEERING, INC.

137-263 Targeted Sampling Report – Badin Business Park Facility - Badin, NC; January 2019 23
4.0 CONCLUSIONS

The basis for the investigation was to provide information to assess the presence of COIs in soils on the
facility property not previously investigated. To accomplish this, sixty-five (65) soil samples were
collected across eight (8) facility locations and submitted for analytical analysis in accordance with the
May 31, 2018 Targeted Sampling Work Plan. Results from the investigation are summarized below.

 Fluoride, cyanide, and VOCs were not detected at concentrations above Protection of
Groundwater PSRGs or Industrial PSRGs.

 A single Aroclor, Aroclor 1232, was detected in one shallow soil sample at a concentration above
the Protection of Groundwater PSRG but below the Industrial PSRG. PCB Aroclors were not
detected in the remaining soil samples at concentrations above either PSRG. Aroclor 1232 has not
been historically detected in soil or groundwater samples; therefore, exposure via the soil-to-
groundwater leaching pathway is not believed to be present. Further, Aroclor 1232 is not common
to past operations and as a result the detection of Aroclor 1232 is believed to be anomalous.

 Concentrations of PAHs were detected in shallow soil samples above the Protection of
Groundwater PSRG in fifteen (15) soil samples; however, detection of PAHs in the deep soil
samples at a concentration above the Protection of Groundwater PSRG was limited to a single
constituent in a single instance (i.e., benzo(a)pyrene at ABR-SB002 (4’-5’)). Because PAHs have
not been historically detected in groundwater samples, exposure via the soil-to-groundwater
leaching pathway is not believed to be present.

 Three shallow soil samples in three separate targeted areas each contained a concentration of a
single PAH (i.e., benzo(a)pyrene) slightly exceeding the Industrial PSRG. PAHs were not detected
at concentrations exceeding the Industrial PSRGs in the deeper soil samples. Exposure to the soils
exceeding the Industrial PSRG is limited as all three sample locations are currently covered by
crushed concrete fill or gravel.

ENVIRONEERING, INC.

Appendix A
Laboratory Reports and Chain of Custody Forms

#=CL#
November 12, 2018
LIMS USE: FR - MICHAEL WORDEN
LIMS OBJECT ID: 92400789
92400789
Project:
Pace Project No.:
RE:
Michael W. Worden
Environeering, Inc.
16100 Cairnway
Suite 320
Houston, TX 77084
Anode Butt Rec./Carbon Baking
Dear Michael Worden:
Enclosed are the analytical results for sample(s) received by the laboratory on September 25, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
This revision was issued on 11/12/18 to report J-flagged results to the MDL, per client request.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 22
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92400789
Anode Butt Rec./Carbon Baking
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 22
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92400789
Anode Butt Rec./Carbon Baking
Lab ID Sample ID Matrix Date Collected Date Received
92400789001 ABR-SB001 (0'-1')Solid 09/24/18 17:45 09/25/18 07:30
92400789002 ABR-SB001 (4'-5')Solid 09/24/18 17:50 09/25/18 07:30
92400789003 ABR-SB002 (0'-1')Solid 09/24/18 18:00 09/25/18 07:30
92400789004 ABR-SB002 (4'-5')Solid 09/24/18 18:05 09/25/18 07:30
92400789005 CBF-SB001 (0'-1')Solid 09/24/18 17:10 09/25/18 07:30
92400789006 CBF-SB001 (4'-5')Solid 09/24/18 17:15 09/25/18 07:30
92400789007 CBF-SB002 (0'-1')Solid 09/24/18 17:20 09/25/18 07:30
92400789008 CBF-SB002 (4'-5')Solid 09/24/18 17:25 09/25/18 07:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 22
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92400789
Anode Butt Rec./Carbon Baking
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92400789001 ABR-SB001 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
92400789002 ABR-SB001 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
92400789003 ABR-SB002 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
92400789004 ABR-SB002 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
92400789005 CBF-SB001 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
92400789006 CBF-SB001 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
92400789007 CBF-SB002 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
92400789008 CBF-SB002 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400789
Anode Butt Rec./Carbon Baking
Sample:ABR-SB001 (0'-1')Lab ID:92400789001 Collected:09/24/18 17:45 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 4.6J ug/kg 09/27/18 18:46 83-32-909/26/18 14:1712.0 1.8 1
Acenaphthylene 2.1J ug/kg 09/27/18 18:46 208-96-809/26/18 14:1712.0 1.6 1
Anthracene 15.6 ug/kg 09/27/18 18:46 120-12-709/26/18 14:1712.0 1.7 1
Benzo(a)anthracene 129 ug/kg 09/27/18 18:46 56-55-3 M109/26/18 14:1712.0 0.86 1
Benzo(a)pyrene 128 ug/kg 09/27/18 18:46 50-32-8 M109/26/18 14:1712.0 1.3 1
Benzo(b)fluoranthene 211 ug/kg 09/27/18 18:46 205-99-2 M109/26/18 14:1712.0 0.81 1
Benzo(g,h,i)perylene 79.1 ug/kg 09/27/18 18:46 191-24-209/26/18 14:1712.0 3.1 1
Benzo(k)fluoranthene 90.3 ug/kg 09/27/18 18:46 207-08-9 M109/26/18 14:1712.0 1.8 1
Chrysene 150 ug/kg 09/27/18 18:46 218-01-9 M109/26/18 14:1712.0 2.2 1
Dibenz(a,h)anthracene 25.1 ug/kg 09/27/18 18:46 53-70-309/26/18 14:1712.0 2.2 1
Fluoranthene 214 ug/kg 09/27/18 18:46 206-44-009/26/18 14:1712.0 1.0 1
Fluorene 2.9J ug/kg 09/27/18 18:46 86-73-709/26/18 14:1712.0 1.9 1
Indeno(1,2,3-cd)pyrene 77.6 ug/kg 09/27/18 18:46 193-39-509/26/18 14:1712.0 3.4 1
1-Methylnaphthalene 3.0J ug/kg 09/27/18 18:46 90-12-009/26/18 14:1712.0 1.4 1
2-Methylnaphthalene 2.2J ug/kg 09/27/18 18:46 91-57-609/26/18 14:1712.0 1.3 1
Naphthalene 2.8J ug/kg 09/27/18 18:46 91-20-309/26/18 14:1712.0 2.8 1
Phenanthrene 64.2 ug/kg 09/27/18 18:46 85-01-809/26/18 14:1712.0 1.8 1
Pyrene 190 ug/kg 09/27/18 18:46 129-00-009/26/18 14:1712.0 2.2 1
Surrogates
Nitrobenzene-d5 (S)63 %09/27/18 18:46 4165-60-009/26/18 14:1710-128 1
2-Fluorobiphenyl (S)61 %09/27/18 18:46 321-60-809/26/18 14:1710-110 1
Terphenyl-d14 (S)70 %09/27/18 18:46 1718-51-009/26/18 14:1739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.7 %09/25/18 17:350.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400789
Anode Butt Rec./Carbon Baking
Sample:ABR-SB001 (4'-5')Lab ID:92400789002 Collected:09/24/18 17:50 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 09/27/18 19:28 83-32-909/26/18 14:1712.0 1.8 1
Acenaphthylene ND ug/kg 09/27/18 19:28 208-96-809/26/18 14:1712.0 1.6 1
Anthracene ND ug/kg 09/27/18 19:28 120-12-709/26/18 14:1712.0 1.7 1
Benzo(a)anthracene 1.5J ug/kg 09/27/18 19:28 56-55-309/26/18 14:1712.0 0.85 1
Benzo(a)pyrene 1.5J ug/kg 09/27/18 19:28 50-32-809/26/18 14:1712.0 1.3 1
Benzo(b)fluoranthene 2.1J ug/kg 09/27/18 19:28 205-99-209/26/18 14:1712.0 0.81 1
Benzo(g,h,i)perylene ND ug/kg 09/27/18 19:28 191-24-209/26/18 14:1712.0 3.1 1
Benzo(k)fluoranthene ND ug/kg 09/27/18 19:28 207-08-909/26/18 14:1712.0 1.8 1
Chrysene 2.6J ug/kg 09/27/18 19:28 218-01-909/26/18 14:1712.0 2.2 1
Dibenz(a,h)anthracene ND ug/kg 09/27/18 19:28 53-70-309/26/18 14:1712.0 2.2 1
Fluoranthene 1.4J ug/kg 09/27/18 19:28 206-44-009/26/18 14:1712.0 1.0 1
Fluorene ND ug/kg 09/27/18 19:28 86-73-709/26/18 14:1712.0 1.9 1
Indeno(1,2,3-cd)pyrene ND ug/kg 09/27/18 19:28 193-39-509/26/18 14:1712.0 3.4 1
1-Methylnaphthalene ND ug/kg 09/27/18 19:28 90-12-009/26/18 14:1712.0 1.4 1
2-Methylnaphthalene ND ug/kg 09/27/18 19:28 91-57-609/26/18 14:1712.0 1.3 1
Naphthalene ND ug/kg 09/27/18 19:28 91-20-309/26/18 14:1712.0 2.8 1
Phenanthrene ND ug/kg 09/27/18 19:28 85-01-809/26/18 14:1712.0 1.8 1
Pyrene ND ug/kg 09/27/18 19:28 129-00-009/26/18 14:1712.0 2.2 1
Surrogates
Nitrobenzene-d5 (S)69 %09/27/18 19:28 4165-60-009/26/18 14:1710-128 1
2-Fluorobiphenyl (S)70 %09/27/18 19:28 321-60-809/26/18 14:1710-110 1
Terphenyl-d14 (S)72 %09/27/18 19:28 1718-51-009/26/18 14:1739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.7 %09/25/18 17:350.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400789
Anode Butt Rec./Carbon Baking
Sample:ABR-SB002 (0'-1')Lab ID:92400789003 Collected:09/24/18 18:00 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 63.0 ug/kg 09/28/18 14:04 83-32-909/26/18 14:1761.1 9.2 5
Acenaphthylene 15.2J ug/kg 09/28/18 14:04 208-96-809/26/18 14:1761.1 7.9 5
Anthracene 257 ug/kg 09/28/18 14:04 120-12-709/26/18 14:1761.1 8.6 5
Benzo(a)anthracene 1180 ug/kg 09/28/18 14:04 56-55-309/26/18 14:1761.1 4.3 5
Benzo(a)pyrene 1050 ug/kg 09/28/18 14:04 50-32-809/26/18 14:1761.1 6.7 5
Benzo(b)fluoranthene 1510 ug/kg 09/28/18 14:04 205-99-209/26/18 14:1761.1 4.1 5
Benzo(g,h,i)perylene 623 ug/kg 09/28/18 14:04 191-24-209/26/18 14:1761.1 15.9 5
Benzo(k)fluoranthene 538 ug/kg 09/28/18 14:04 207-08-909/26/18 14:1761.1 9.2 5
Chrysene 1140 ug/kg 09/28/18 14:04 218-01-909/26/18 14:1761.1 11.0 5
Dibenz(a,h)anthracene 186 ug/kg 09/28/18 14:04 53-70-309/26/18 14:1761.1 11.0 5
Fluoranthene 1840 ug/kg 09/28/18 14:04 206-44-009/26/18 14:1761.1 5.1 5
Fluorene 38.8J ug/kg 09/28/18 14:04 86-73-709/26/18 14:1761.1 9.8 5
Indeno(1,2,3-cd)pyrene 563 ug/kg 09/28/18 14:04 193-39-509/26/18 14:1761.1 17.1 5
1-Methylnaphthalene ND ug/kg 09/28/18 16:11 90-12-0 D309/26/18 14:1730536.6 25
2-Methylnaphthalene ND ug/kg 09/28/18 16:11 91-57-6 D309/26/18 14:1730533.6 25
Naphthalene ND ug/kg 09/28/18 16:11 91-20-3 D309/26/18 14:1730570.2 25
Phenanthrene 795 ug/kg 09/28/18 14:04 85-01-809/26/18 14:1761.1 9.2 5
Pyrene 1610 ug/kg 09/28/18 14:04 129-00-009/26/18 14:1761.1 11.0 5
Surrogates
Nitrobenzene-d5 (S)13 %09/28/18 14:04 4165-60-0 D309/26/18 14:1710-128 5
2-Fluorobiphenyl (S)60 %09/28/18 14:04 321-60-809/26/18 14:1710-110 5
Terphenyl-d14 (S)73 %09/28/18 14:04 1718-51-009/26/18 14:1739-119 5
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.3 %09/25/18 17:350.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400789
Anode Butt Rec./Carbon Baking
Sample:ABR-SB002 (4'-5')Lab ID:92400789004 Collected:09/24/18 18:05 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 16.6J ug/kg 09/28/18 14:25 83-32-909/26/18 14:1762.7 9.4 5
Acenaphthylene ND ug/kg 09/28/18 14:25 208-96-809/26/18 14:1762.7 8.1 5
Anthracene 54.1J ug/kg 09/28/18 14:25 120-12-709/26/18 14:1762.7 8.8 5
Benzo(a)anthracene 287 ug/kg 09/28/18 14:25 56-55-309/26/18 14:1762.7 4.4 5
Benzo(a)pyrene 325 ug/kg 09/28/18 14:25 50-32-809/26/18 14:1762.7 6.9 5
Benzo(b)fluoranthene 474 ug/kg 09/28/18 14:25 205-99-209/26/18 14:1762.7 4.2 5
Benzo(g,h,i)perylene 220 ug/kg 09/28/18 14:25 191-24-209/26/18 14:1762.7 16.3 5
Benzo(k)fluoranthene 171 ug/kg 09/28/18 14:25 207-08-909/26/18 14:1762.7 9.4 5
Chrysene 305 ug/kg 09/28/18 14:25 218-01-909/26/18 14:1762.7 11.3 5
Dibenz(a,h)anthracene 62.8 ug/kg 09/28/18 14:25 53-70-309/26/18 14:1762.7 11.3 5
Fluoranthene 432 ug/kg 09/28/18 14:25 206-44-009/26/18 14:1762.7 5.2 5
Fluorene 11.9J ug/kg 09/28/18 14:25 86-73-709/26/18 14:1762.7 10.0 5
Indeno(1,2,3-cd)pyrene 199 ug/kg 09/28/18 14:25 193-39-509/26/18 14:1762.7 17.5 5
1-Methylnaphthalene ND ug/kg 09/28/18 14:25 90-12-009/26/18 14:1762.7 7.5 5
2-Methylnaphthalene 7.6J ug/kg 09/28/18 14:25 91-57-609/26/18 14:1762.7 6.9 5
Naphthalene ND ug/kg 09/28/18 14:25 91-20-309/26/18 14:1762.7 14.4 5
Phenanthrene 194 ug/kg 09/28/18 14:25 85-01-809/26/18 14:1762.7 9.4 5
Pyrene 372 ug/kg 09/28/18 14:25 129-00-009/26/18 14:1762.7 11.3 5
Surrogates
Nitrobenzene-d5 (S)73 %09/28/18 14:25 4165-60-0 D309/26/18 14:1710-128 5
2-Fluorobiphenyl (S)61 %09/28/18 14:25 321-60-809/26/18 14:1710-110 5
Terphenyl-d14 (S)60 %09/28/18 14:25 1718-51-009/26/18 14:1739-119 5
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 18.8 %09/25/18 17:350.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:48 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 8 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400789
Anode Butt Rec./Carbon Baking
Sample:CBF-SB001 (0'-1')Lab ID:92400789005 Collected:09/24/18 17:10 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 19.8 ug/kg 09/27/18 20:53 83-32-909/26/18 14:1712.3 1.9 1
Acenaphthylene 5.5J ug/kg 09/27/18 20:53 208-96-809/26/18 14:1712.3 1.6 1
Anthracene 48.1 ug/kg 09/27/18 20:53 120-12-709/26/18 14:1712.3 1.7 1
Benzo(a)anthracene 424 ug/kg 09/27/18 20:53 56-55-309/26/18 14:1712.3 0.88 1
Benzo(a)pyrene 397 ug/kg 09/27/18 20:53 50-32-809/26/18 14:1712.3 1.4 1
Benzo(b)fluoranthene 662 ug/kg 09/27/18 20:53 205-99-209/26/18 14:1712.3 0.83 1
Benzo(g,h,i)perylene 223 ug/kg 09/27/18 20:53 191-24-209/26/18 14:1712.3 3.2 1
Benzo(k)fluoranthene 186 ug/kg 09/27/18 20:53 207-08-909/26/18 14:1712.3 1.9 1
Chrysene 480 ug/kg 09/27/18 20:53 218-01-909/26/18 14:1712.3 2.2 1
Dibenz(a,h)anthracene 73.2 ug/kg 09/27/18 20:53 53-70-309/26/18 14:1712.3 2.2 1
Fluoranthene 597 ug/kg 09/27/18 20:53 206-44-009/26/18 14:1712.3 1.0 1
Fluorene 10.5J ug/kg 09/27/18 20:53 86-73-709/26/18 14:1712.3 2.0 1
Indeno(1,2,3-cd)pyrene 204 ug/kg 09/27/18 20:53 193-39-509/26/18 14:1712.3 3.5 1
1-Methylnaphthalene 19.4 ug/kg 09/27/18 20:53 90-12-009/26/18 14:1712.3 1.5 1
2-Methylnaphthalene 27.2 ug/kg 09/27/18 20:53 91-57-609/26/18 14:1712.3 1.4 1
Naphthalene 27.2 ug/kg 09/27/18 20:53 91-20-309/26/18 14:1712.3 2.8 1
Phenanthrene 278 ug/kg 09/27/18 20:53 85-01-809/26/18 14:1712.3 1.9 1
Pyrene 497 ug/kg 09/27/18 20:53 129-00-009/26/18 14:1712.3 2.2 1
Surrogates
Nitrobenzene-d5 (S)49 %09/27/18 20:53 4165-60-009/26/18 14:1710-128 1
2-Fluorobiphenyl (S)49 %09/27/18 20:53 321-60-809/26/18 14:1710-110 1
Terphenyl-d14 (S)68 %09/27/18 20:53 1718-51-009/26/18 14:1739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.6 %09/25/18 17:350.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400789
Anode Butt Rec./Carbon Baking
Sample:CBF-SB001 (4'-5')Lab ID:92400789006 Collected:09/24/18 17:15 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 09/27/18 21:14 83-32-909/26/18 14:1711.9 1.8 1
Acenaphthylene ND ug/kg 09/27/18 21:14 208-96-809/26/18 14:1711.9 1.5 1
Anthracene ND ug/kg 09/27/18 21:14 120-12-709/26/18 14:1711.9 1.7 1
Benzo(a)anthracene 2.6J ug/kg 09/27/18 21:14 56-55-309/26/18 14:1711.9 0.84 1
Benzo(a)pyrene 3.3J ug/kg 09/27/18 21:14 50-32-809/26/18 14:1711.9 1.3 1
Benzo(b)fluoranthene 3.8J ug/kg 09/27/18 21:14 205-99-209/26/18 14:1711.9 0.79 1
Benzo(g,h,i)perylene ND ug/kg 09/27/18 21:14 191-24-209/26/18 14:1711.9 3.1 1
Benzo(k)fluoranthene ND ug/kg 09/27/18 21:14 207-08-909/26/18 14:1711.9 1.8 1
Chrysene 3.2J ug/kg 09/27/18 21:14 218-01-909/26/18 14:1711.9 2.1 1
Dibenz(a,h)anthracene ND ug/kg 09/27/18 21:14 53-70-309/26/18 14:1711.9 2.1 1
Fluoranthene 2.7J ug/kg 09/27/18 21:14 206-44-009/26/18 14:1711.9 0.98 1
Fluorene ND ug/kg 09/27/18 21:14 86-73-709/26/18 14:1711.9 1.9 1
Indeno(1,2,3-cd)pyrene ND ug/kg 09/27/18 21:14 193-39-509/26/18 14:1711.9 3.3 1
1-Methylnaphthalene ND ug/kg 09/27/18 21:14 90-12-009/26/18 14:1711.9 1.4 1
2-Methylnaphthalene ND ug/kg 09/27/18 21:14 91-57-609/26/18 14:1711.9 1.3 1
Naphthalene ND ug/kg 09/27/18 21:14 91-20-309/26/18 14:1711.9 2.7 1
Phenanthrene ND ug/kg 09/27/18 21:14 85-01-809/26/18 14:1711.9 1.8 1
Pyrene 2.7J ug/kg 09/27/18 21:14 129-00-009/26/18 14:1711.9 2.1 1
Surrogates
Nitrobenzene-d5 (S)41 %09/27/18 21:14 4165-60-009/26/18 14:1710-128 1
2-Fluorobiphenyl (S)38 %09/27/18 21:14 321-60-809/26/18 14:1710-110 1
Terphenyl-d14 (S)54 %09/27/18 21:14 1718-51-009/26/18 14:1739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.9 %09/25/18 17:350.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:48 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400789
Anode Butt Rec./Carbon Baking
Sample:CBF-SB002 (0'-1')Lab ID:92400789007 Collected:09/24/18 17:20 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 13.6 ug/kg 09/27/18 21:35 83-32-909/26/18 14:1713.2 2.0 1
Acenaphthylene 3.9J ug/kg 09/27/18 21:35 208-96-809/26/18 14:1713.2 1.7 1
Anthracene 34.1 ug/kg 09/27/18 21:35 120-12-709/26/18 14:1713.2 1.9 1
Benzo(a)anthracene 230 ug/kg 09/27/18 21:35 56-55-309/26/18 14:1713.2 0.94 1
Benzo(a)pyrene 235 ug/kg 09/27/18 21:35 50-32-809/26/18 14:1713.2 1.5 1
Benzo(b)fluoranthene 312 ug/kg 09/27/18 21:35 205-99-209/26/18 14:1713.2 0.89 1
Benzo(g,h,i)perylene 129 ug/kg 09/27/18 21:35 191-24-209/26/18 14:1713.2 3.4 1
Benzo(k)fluoranthene 124 ug/kg 09/27/18 21:35 207-08-909/26/18 14:1713.2 2.0 1
Chrysene 237 ug/kg 09/27/18 21:35 218-01-909/26/18 14:1713.2 2.4 1
Dibenz(a,h)anthracene 10.6J ug/kg 09/27/18 21:35 53-70-309/26/18 14:1713.2 2.4 1
Fluoranthene 390 ug/kg 09/27/18 21:35 206-44-009/26/18 14:1713.2 1.1 1
Fluorene 7.2J ug/kg 09/27/18 21:35 86-73-709/26/18 14:1713.2 2.1 1
Indeno(1,2,3-cd)pyrene 123 ug/kg 09/27/18 21:35 193-39-509/26/18 14:1713.2 3.7 1
1-Methylnaphthalene 7.6J ug/kg 09/27/18 21:35 90-12-009/26/18 14:1713.2 1.6 1
2-Methylnaphthalene 10.9J ug/kg 09/27/18 21:35 91-57-609/26/18 14:1713.2 1.5 1
Naphthalene 14.4 ug/kg 09/27/18 21:35 91-20-309/26/18 14:1713.2 3.0 1
Phenanthrene 135 ug/kg 09/27/18 21:35 85-01-809/26/18 14:1713.2 2.0 1
Pyrene 362 ug/kg 09/27/18 21:35 129-00-009/26/18 14:1713.2 2.4 1
Surrogates
Nitrobenzene-d5 (S)60 %09/27/18 21:35 4165-60-009/26/18 14:1710-128 1
2-Fluorobiphenyl (S)58 %09/27/18 21:35 321-60-809/26/18 14:1710-110 1
Terphenyl-d14 (S)67 %09/27/18 21:35 1718-51-009/26/18 14:1739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 24.3 %09/25/18 18:040.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 22
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400789
Anode Butt Rec./Carbon Baking
Sample:CBF-SB002 (4'-5')Lab ID:92400789008 Collected:09/24/18 17:25 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 09/27/18 21:56 83-32-909/26/18 14:1712.0 1.8 1
Acenaphthylene ND ug/kg 09/27/18 21:56 208-96-809/26/18 14:1712.0 1.6 1
Anthracene 3.8J ug/kg 09/27/18 21:56 120-12-709/26/18 14:1712.0 1.7 1
Benzo(a)anthracene 26.6 ug/kg 09/27/18 21:56 56-55-309/26/18 14:1712.0 0.85 1
Benzo(a)pyrene 36.9 ug/kg 09/27/18 21:56 50-32-809/26/18 14:1712.0 1.3 1
Benzo(b)fluoranthene 49.4 ug/kg 09/27/18 21:56 205-99-209/26/18 14:1712.0 0.80 1
Benzo(g,h,i)perylene 28.6 ug/kg 09/27/18 21:56 191-24-209/26/18 14:1712.0 3.1 1
Benzo(k)fluoranthene 17.4 ug/kg 09/27/18 21:56 207-08-909/26/18 14:1712.0 1.8 1
Chrysene 37.5 ug/kg 09/27/18 21:56 218-01-909/26/18 14:1712.0 2.2 1
Dibenz(a,h)anthracene ND ug/kg 09/27/18 21:56 53-70-309/26/18 14:1712.0 2.2 1
Fluoranthene 42.2 ug/kg 09/27/18 21:56 206-44-009/26/18 14:1712.0 0.99 1
Fluorene ND ug/kg 09/27/18 21:56 86-73-709/26/18 14:1712.0 1.9 1
Indeno(1,2,3-cd)pyrene 25.0 ug/kg 09/27/18 21:56 193-39-509/26/18 14:1712.0 3.3 1
1-Methylnaphthalene 15.9 ug/kg 09/27/18 21:56 90-12-009/26/18 14:1712.0 1.4 1
2-Methylnaphthalene 22.2 ug/kg 09/27/18 21:56 91-57-609/26/18 14:1712.0 1.3 1
Naphthalene 18.5 ug/kg 09/27/18 21:56 91-20-309/26/18 14:1712.0 2.7 1
Phenanthrene 22.9 ug/kg 09/27/18 21:56 85-01-809/26/18 14:1712.0 1.8 1
Pyrene 38.5 ug/kg 09/27/18 21:56 129-00-009/26/18 14:1712.0 2.2 1
Surrogates
Nitrobenzene-d5 (S)48 %09/27/18 21:56 4165-60-009/26/18 14:1710-128 1
2-Fluorobiphenyl (S)40 %09/27/18 21:56 321-60-809/26/18 14:1710-110 1
Terphenyl-d14 (S)57 %09/27/18 21:56 1718-51-009/26/18 14:1739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.7 %09/25/18 18:040.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400789
Anode Butt Rec./Carbon Baking
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
432770
EPA 3546
EPA 8270D by SIM
8270 MSSV PAH by SIM
Associated Lab Samples:92400789001, 92400789002, 92400789003, 92400789004, 92400789005, 92400789006, 92400789007,
92400789008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2385110
Associated Lab Samples:92400789001, 92400789002, 92400789003, 92400789004, 92400789005, 92400789006, 92400789007,
92400789008
Matrix:Solid
AnalyzedMDL
1-Methylnaphthalene ug/kg ND 10.1 09/27/18 14:111.2
2-Methylnaphthalene ug/kg ND 10.1 09/27/18 14:111.1
Acenaphthene ug/kg ND 10.1 09/27/18 14:111.5
Acenaphthylene ug/kg ND 10.1 09/27/18 14:111.3
Anthracene ug/kg ND 10.1 09/27/18 14:111.4
Benzo(a)anthracene ug/kg ND 10.1 09/27/18 14:110.71
Benzo(a)pyrene ug/kg ND 10.1 09/27/18 14:111.1
Benzo(b)fluoranthene ug/kg 0.96J 10.1 09/27/18 14:110.67
Benzo(g,h,i)perylene ug/kg ND 10.1 09/27/18 14:112.6
Benzo(k)fluoranthene ug/kg ND 10.1 09/27/18 14:111.5
Chrysene ug/kg ND 10.1 09/27/18 14:111.8
Dibenz(a,h)anthracene ug/kg ND 10.1 09/27/18 14:111.8
Fluoranthene ug/kg ND 10.1 09/27/18 14:110.84
Fluorene ug/kg ND 10.1 09/27/18 14:111.6
Indeno(1,2,3-cd)pyrene ug/kg ND 10.1 09/27/18 14:112.8
Naphthalene ug/kg ND 10.1 09/27/18 14:112.3
Phenanthrene ug/kg ND 10.1 09/27/18 14:111.5
Pyrene ug/kg ND 10.1 09/27/18 14:111.8
2-Fluorobiphenyl (S)%51 10-110 09/27/18 14:11
Nitrobenzene-d5 (S)%54 10-128 09/27/18 14:11
Terphenyl-d14 (S)%60 39-119 09/27/18 14:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2385111LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/kg 26.333.3 79 44-130
2-Methylnaphthalene ug/kg 27.833.3 83 41-134
Acenaphthene ug/kg 29.433.3 88 52-123
Acenaphthylene ug/kg 26.533.3 79 49-116
Anthracene ug/kg 29.333.3 88 41-133
Benzo(a)anthracene ug/kg 29.233.3 88 56-130
Benzo(a)pyrene ug/kg 28.233.3 85 51-136
Benzo(b)fluoranthene ug/kg 28.733.3 86 37-149
Benzo(g,h,i)perylene ug/kg 26.333.3 79 39-127
Benzo(k)fluoranthene ug/kg 29.333.3 88 45-139
Chrysene ug/kg 30.133.3 90 59-127
Dibenz(a,h)anthracene ug/kg 28.833.3 86 37-139
Fluoranthene ug/kg 31.033.3 93 53-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400789
Anode Butt Rec./Carbon Baking
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2385111LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 26.033.3 78 45-127
Indeno(1,2,3-cd)pyrene ug/kg 29.433.3 88 35-145
Naphthalene ug/kg 27.933.3 84 45-123
Phenanthrene ug/kg 30.433.3 91 50-125
Pyrene ug/kg 31.033.3 93 52-132
2-Fluorobiphenyl (S)%87 10-110
Nitrobenzene-d5 (S)%92 10-128
Terphenyl-d14 (S)%81 39-119
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2385112MATRIX SPIKE SAMPLE:
MSSpike
Result
92400789001
1-Methylnaphthalene ug/kg 25.240.4 55 50-1503.0J
2-Methylnaphthalene ug/kg 26.140.4 59 50-1502.2J
Acenaphthene ug/kg 31.140.4 65 50-1504.6J
Acenaphthylene ug/kg 24.840.4 56 50-1502.1J
Anthracene ug/kg 45.840.4 75 50-15015.6
Benzo(a)anthracene ug/kg 192 M140.4 156 50-150129
Benzo(a)pyrene ug/kg 206 M140.4 194 50-150128
Benzo(b)fluoranthene ug/kg 324 M140.4 280 50-150211
Benzo(g,h,i)perylene ug/kg 10640.4 67 50-15079.1
Benzo(k)fluoranthene ug/kg 102 M140.4 28 50-15090.3
Chrysene ug/kg 220 M140.4 173 50-150150
Dibenz(a,h)anthracene ug/kg 47.240.4 55 50-15025.1
Fluoranthene ug/kg 25040.4 88 50-150214
Fluorene ug/kg 26.040.4 57 50-1502.9J
Indeno(1,2,3-cd)pyrene ug/kg 11040.4 81 50-15077.6
Naphthalene ug/kg 25.340.4 56 50-1502.8J
Phenanthrene ug/kg 92.240.4 69 50-15064.2
Pyrene ug/kg 24840.4 144 50-150190
2-Fluorobiphenyl (S)%62 10-110
Nitrobenzene-d5 (S)%62 10-128
Terphenyl-d14 (S)%61 39-119
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400789002
2385113SAMPLE DUPLICATE:
1-Methylnaphthalene ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg 1.3J 301.5J
Benzo(a)pyrene ug/kg ND 301.5J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400789
Anode Butt Rec./Carbon Baking
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400789002
2385113SAMPLE DUPLICATE:
Benzo(b)fluoranthene ug/kg 1.9J 302.1J
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Chrysene ug/kg 2.2J 302.6J
Dibenz(a,h)anthracene ug/kg ND 30ND
Fluoranthene ug/kg 1.2J 301.4J
Fluorene ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2-Fluorobiphenyl (S)%69 370
Nitrobenzene-d5 (S)%70 069
Terphenyl-d14 (S)%70 372
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400789
Anode Butt Rec./Carbon Baking
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
432629
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92400789001, 92400789002, 92400789003, 92400789004, 92400789005, 92400789006
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400378001
2384622SAMPLE DUPLICATE:
Percent Moisture %65.1 1 2565.5
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400789006
2384623SAMPLE DUPLICATE:
Percent Moisture %16.0 0 2515.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 22
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400789
Anode Butt Rec./Carbon Baking
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
432644
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92400789007, 92400789008
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400798001
2384677SAMPLE DUPLICATE:
Percent Moisture %17.0 1 2516.8
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400796007
2384678SAMPLE DUPLICATE:
Percent Moisture %18.2 2 2517.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:48 AM
Pace Analytical Services, LLC
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Page 17 of 22
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92400789
Anode Butt Rec./Carbon Baking
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:48 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 22
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92400789
Anode Butt Rec./Carbon Baking
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92400789001 432770 432998ABR-SB001 (0'-1')EPA 3546 EPA 8270D by SIM
92400789002 432770 432998ABR-SB001 (4'-5')EPA 3546 EPA 8270D by SIM
92400789003 432770 432998ABR-SB002 (0'-1')EPA 3546 EPA 8270D by SIM
92400789004 432770 432998ABR-SB002 (4'-5')EPA 3546 EPA 8270D by SIM
92400789005 432770 432998CBF-SB001 (0'-1')EPA 3546 EPA 8270D by SIM
92400789006 432770 432998CBF-SB001 (4'-5')EPA 3546 EPA 8270D by SIM
92400789007 432770 432998CBF-SB002 (0'-1')EPA 3546 EPA 8270D by SIM
92400789008 432770 432998CBF-SB002 (4'-5')EPA 3546 EPA 8270D by SIM
92400789001 432629ABR-SB001 (0'-1')ASTM D2974-87
92400789002 432629ABR-SB001 (4'-5')ASTM D2974-87
92400789003 432629ABR-SB002 (0'-1')ASTM D2974-87
92400789004 432629ABR-SB002 (4'-5')ASTM D2974-87
92400789005 432629CBF-SB001 (0'-1')ASTM D2974-87
92400789006 432629CBF-SB001 (4'-5')ASTM D2974-87
92400789007 432644CBF-SB002 (0'-1')ASTM D2974-87
92400789008 432644CBF-SB002 (4'-5')ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:48 AM
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9800 Kincey Ave. Suite 100
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[phone]
Page 19 of 22
Page 20 of 22
Page 21 of 22
Page 22 of 22
#=CL#
November 12, 2018
LIMS USE: FR - MICHAEL WORDEN
LIMS OBJECT ID: 92401220
92401220
Project:
Pace Project No.:
RE:
Michael W. Worden
Environeering, Inc.
16100 Cairnway
Suite 320
Houston, TX 77084
Frmr Cathode/Anode Plant Area
Dear Michael Worden:
Enclosed are the analytical results for sample(s) received by the laboratory on September 26, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
This revision was issued on 11/12/18 to report J-flagged results to the MDL, per client request.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 23
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92401220
Frmr Cathode/Anode Plant Area
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 23
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92401220
Frmr Cathode/Anode Plant Area
Lab ID Sample ID Matrix Date Collected Date Received
92401220001 CAT-SB001 (0'-1')Solid 09/25/18 08:25 09/26/18 15:25
92401220002 CAT-SB001 (4'-5')Solid 09/25/18 08:30 09/26/18 15:25
92401220003 CAT-SB002 (0'-1')Solid 09/25/18 08:40 09/26/18 15:25
92401220004 CAT-SB002 (4'-5')Solid 09/25/18 08:45 09/26/18 15:25
92401220005 ANO-SB001 (0'-1')Solid 09/24/18 13:40 09/26/18 15:25
92401220006 ANO-SB001 (4'-5')Solid 09/24/18 13:45 09/26/18 15:25
92401220007 ANO-SB002 (0'-1')Solid 09/24/18 14:05 09/26/18 15:25
92401220008 ANO-SB002 (4'-5')Solid 09/24/18 14:10 09/26/18 15:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 23
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92401220
Frmr Cathode/Anode Plant Area
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92401220001 CAT-SB001 (0'-1')EPA 8082A 8 PASI-CSEM
EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
92401220002 CAT-SB001 (4'-5')EPA 8082A 8 PASI-CSEM
EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
92401220003 CAT-SB002 (0'-1')EPA 8082A 8 PASI-CSEM
EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
92401220004 CAT-SB002 (4'-5')EPA 8082A 8 PASI-CSEM
EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
92401220005 ANO-SB001 (0'-1')EPA 8082A 8 PASI-CSEM
EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
92401220006 ANO-SB001 (4'-5')EPA 8082A 8 PASI-CSEM
EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
92401220007 ANO-SB002 (0'-1')EPA 8082A 8 PASI-CSEM
EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
92401220008 ANO-SB002 (4'-5')EPA 8082A 8 PASI-CSEM
EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401220
Frmr Cathode/Anode Plant Area
Sample:CAT-SB001 (0'-1')Lab ID:92401220001 Collected:09/25/18 08:25 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8082A Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 09/29/18 13:08 12674-11-209/28/18 14:5338.9 17.7 1
PCB-1221 (Aroclor 1221)ND ug/kg 09/29/18 13:08 11104-28-209/28/18 14:5338.9 17.7 1
PCB-1232 (Aroclor 1232)ND ug/kg 09/29/18 13:08 11141-16-509/28/18 14:5338.9 17.7 1
PCB-1242 (Aroclor 1242)ND ug/kg 09/29/18 13:08 53469-21-909/28/18 14:5338.9 17.7 1
PCB-1248 (Aroclor 1248)ND ug/kg 09/29/18 13:08 12672-29-609/28/18 14:5338.9 17.7 1
PCB-1254 (Aroclor 1254)ND ug/kg 09/29/18 13:08 11097-69-109/28/18 14:5338.9 17.7 1
PCB-1260 (Aroclor 1260)ND ug/kg 09/29/18 13:08 11096-82-509/28/18 14:5338.9 17.7 1
Surrogates
Decachlorobiphenyl (S)124 %09/29/18 13:08 2051-24-309/28/18 14:5321-132 1
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 235 ug/kg 10/03/18 00:02 83-32-909/28/18 16:1912.0 1.8 1
Acenaphthylene 16.2 ug/kg 10/03/18 00:02 208-96-809/28/18 16:1912.0 1.6 1
Anthracene 906 ug/kg 10/03/18 00:02 120-12-709/28/18 16:1912.0 1.7 1
Benzo(a)anthracene 2730 ug/kg 10/03/18 09:14 56-55-309/28/18 16:1960.1 4.3 5
Benzo(a)pyrene 2230 ug/kg 10/03/18 09:14 50-32-809/28/18 16:1960.1 6.6 5
Benzo(b)fluoranthene 3850 ug/kg 10/03/18 09:14 205-99-209/28/18 16:1960.1 4.0 5
Benzo(g,h,i)perylene 997 ug/kg 10/03/18 00:02 191-24-209/28/18 16:1912.0 3.1 1
Benzo(k)fluoranthene 1180 ug/kg 10/03/18 09:14 207-08-909/28/18 16:1960.1 9.0 5
Chrysene 2590 ug/kg 10/03/18 09:14 218-01-909/28/18 16:1960.1 10.8 5
Dibenz(a,h)anthracene 446 ug/kg 10/03/18 00:02 53-70-309/28/18 16:1912.0 2.2 1
Fluoranthene 4150 ug/kg 10/03/18 09:14 206-44-009/28/18 16:1960.1 5.0 5
Fluorene 282 ug/kg 10/03/18 00:02 86-73-709/28/18 16:1912.0 1.9 1
Indeno(1,2,3-cd)pyrene 1330 ug/kg 10/03/18 09:14 193-39-509/28/18 16:1960.1 16.8 5
1-Methylnaphthalene 47.4 ug/kg 10/03/18 00:02 90-12-009/28/18 16:1912.0 1.4 1
2-Methylnaphthalene 52.9 ug/kg 10/03/18 00:02 91-57-609/28/18 16:1912.0 1.3 1
Naphthalene 59.5 ug/kg 10/03/18 00:02 91-20-309/28/18 16:1912.0 2.8 1
Phenanthrene 2620 ug/kg 10/03/18 09:14 85-01-809/28/18 16:1960.1 9.0 5
Pyrene 3470 ug/kg 10/03/18 09:14 129-00-009/28/18 16:1960.1 10.8 5
Surrogates
Nitrobenzene-d5 (S)81 %10/03/18 00:02 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)76 %10/03/18 00:02 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)96 %10/03/18 00:02 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.7 %09/27/18 17:230.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:50 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 5 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401220
Frmr Cathode/Anode Plant Area
Sample:CAT-SB001 (4'-5')Lab ID:92401220002 Collected:09/25/18 08:30 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8082A Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 09/29/18 13:28 12674-11-209/28/18 14:5338.6 17.5 1
PCB-1221 (Aroclor 1221)ND ug/kg 09/29/18 13:28 11104-28-209/28/18 14:5338.6 17.5 1
PCB-1232 (Aroclor 1232)ND ug/kg 09/29/18 13:28 11141-16-509/28/18 14:5338.6 17.5 1
PCB-1242 (Aroclor 1242)ND ug/kg 09/29/18 13:28 53469-21-909/28/18 14:5338.6 17.5 1
PCB-1248 (Aroclor 1248)ND ug/kg 09/29/18 13:28 12672-29-609/28/18 14:5338.6 17.5 1
PCB-1254 (Aroclor 1254)ND ug/kg 09/29/18 13:28 11097-69-109/28/18 14:5338.6 17.5 1
PCB-1260 (Aroclor 1260)ND ug/kg 09/29/18 13:28 11096-82-509/28/18 14:5338.6 17.5 1
Surrogates
Decachlorobiphenyl (S)132 %09/29/18 13:28 2051-24-309/28/18 14:5321-132 1
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 17.3 ug/kg 10/02/18 18:03 83-32-909/28/18 16:1911.9 1.8 1
Acenaphthylene ND ug/kg 10/02/18 18:03 208-96-809/28/18 16:1911.9 1.5 1
Anthracene 81.2 ug/kg 10/02/18 18:03 120-12-709/28/18 16:1911.9 1.7 1
Benzo(a)anthracene 337 ug/kg 10/02/18 18:03 56-55-309/28/18 16:1911.9 0.84 1
Benzo(a)pyrene 308 ug/kg 10/02/18 18:03 50-32-809/28/18 16:1911.9 1.3 1
Benzo(b)fluoranthene 504 ug/kg 10/02/18 18:03 205-99-209/28/18 16:1911.9 0.79 1
Benzo(g,h,i)perylene 212 ug/kg 10/02/18 18:03 191-24-209/28/18 16:1911.9 3.1 1
Benzo(k)fluoranthene 169 ug/kg 10/02/18 18:03 207-08-909/28/18 16:1911.9 1.8 1
Chrysene 338 ug/kg 10/02/18 18:03 218-01-909/28/18 16:1911.9 2.1 1
Dibenz(a,h)anthracene 17.7 ug/kg 10/02/18 18:03 53-70-309/28/18 16:1911.9 2.1 1
Fluoranthene 530 ug/kg 10/02/18 18:03 206-44-009/28/18 16:1911.9 0.98 1
Fluorene 13.0 ug/kg 10/02/18 18:03 86-73-709/28/18 16:1911.9 1.9 1
Indeno(1,2,3-cd)pyrene 203 ug/kg 10/02/18 18:03 193-39-509/28/18 16:1911.9 3.3 1
1-Methylnaphthalene 5.9J ug/kg 10/02/18 18:03 90-12-009/28/18 16:1911.9 1.4 1
2-Methylnaphthalene 9.9J ug/kg 10/02/18 18:03 91-57-609/28/18 16:1911.9 1.3 1
Naphthalene 10.9J ug/kg 10/02/18 18:03 91-20-309/28/18 16:1911.9 2.7 1
Phenanthrene 261 ug/kg 10/02/18 18:03 85-01-809/28/18 16:1911.9 1.8 1
Pyrene 429 ug/kg 10/02/18 18:03 129-00-009/28/18 16:1911.9 2.1 1
Surrogates
Nitrobenzene-d5 (S)71 %10/02/18 18:03 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)63 %10/02/18 18:03 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)74 %10/02/18 18:03 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.6 %09/27/18 18:200.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:50 AM
Pace Analytical Services, LLC
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[phone]
Page 6 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401220
Frmr Cathode/Anode Plant Area
Sample:CAT-SB002 (0'-1')Lab ID:92401220003 Collected:09/25/18 08:40 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8082A Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 09/29/18 13:48 12674-11-209/28/18 14:5340.5 18.4 1
PCB-1221 (Aroclor 1221)ND ug/kg 09/29/18 13:48 11104-28-209/28/18 14:5340.5 18.4 1
PCB-1232 (Aroclor 1232)ND ug/kg 09/29/18 13:48 11141-16-509/28/18 14:5340.5 18.4 1
PCB-1242 (Aroclor 1242)ND ug/kg 09/29/18 13:48 53469-21-909/28/18 14:5340.5 18.4 1
PCB-1248 (Aroclor 1248)ND ug/kg 09/29/18 13:48 12672-29-609/28/18 14:5340.5 18.4 1
PCB-1254 (Aroclor 1254)ND ug/kg 09/29/18 13:48 11097-69-109/28/18 14:5340.5 18.4 1
PCB-1260 (Aroclor 1260)ND ug/kg 09/29/18 13:48 11096-82-509/28/18 14:5340.5 18.4 1
Surrogates
Decachlorobiphenyl (S)85 %09/29/18 13:48 2051-24-309/28/18 14:5321-132 1
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/02/18 18:24 83-32-909/28/18 16:1912.4 1.9 1
Acenaphthylene ND ug/kg 10/02/18 18:24 208-96-809/28/18 16:1912.4 1.6 1
Anthracene ND ug/kg 10/02/18 18:24 120-12-709/28/18 16:1912.4 1.7 1
Benzo(a)anthracene 5.1J ug/kg 10/02/18 18:24 56-55-309/28/18 16:1912.4 0.88 1
Benzo(a)pyrene 3.6J ug/kg 10/02/18 18:24 50-32-809/28/18 16:1912.4 1.4 1
Benzo(b)fluoranthene 8.9J ug/kg 10/02/18 18:24 205-99-209/28/18 16:1912.4 0.83 1
Benzo(g,h,i)perylene 3.7J ug/kg 10/02/18 18:24 191-24-209/28/18 16:1912.4 3.2 1
Benzo(k)fluoranthene 3.1J ug/kg 10/02/18 18:24 207-08-909/28/18 16:1912.4 1.9 1
Chrysene 7.0J ug/kg 10/02/18 18:24 218-01-909/28/18 16:1912.4 2.2 1
Dibenz(a,h)anthracene ND ug/kg 10/02/18 18:24 53-70-309/28/18 16:1912.4 2.2 1
Fluoranthene 10.6J ug/kg 10/02/18 18:24 206-44-009/28/18 16:1912.4 1.0 1
Fluorene ND ug/kg 10/02/18 18:24 86-73-709/28/18 16:1912.4 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/02/18 18:24 193-39-509/28/18 16:1912.4 3.5 1
1-Methylnaphthalene ND ug/kg 10/02/18 18:24 90-12-009/28/18 16:1912.4 1.5 1
2-Methylnaphthalene ND ug/kg 10/02/18 18:24 91-57-609/28/18 16:1912.4 1.4 1
Naphthalene ND ug/kg 10/02/18 18:24 91-20-309/28/18 16:1912.4 2.9 1
Phenanthrene 3.9J ug/kg 10/02/18 18:24 85-01-809/28/18 16:1912.4 1.9 1
Pyrene 13.3 ug/kg 10/02/18 18:24 129-00-009/28/18 16:1912.4 2.2 1
Surrogates
Nitrobenzene-d5 (S)72 %10/02/18 18:24 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)68 %10/02/18 18:24 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)78 %10/02/18 18:24 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.4 %09/27/18 18:200.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:50 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401220
Frmr Cathode/Anode Plant Area
Sample:CAT-SB002 (4'-5')Lab ID:92401220004 Collected:09/25/18 08:45 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8082A Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 09/29/18 14:08 12674-11-209/28/18 14:5339.8 18.1 1
PCB-1221 (Aroclor 1221)ND ug/kg 09/29/18 14:08 11104-28-209/28/18 14:5339.8 18.1 1
PCB-1232 (Aroclor 1232)ND ug/kg 09/29/18 14:08 11141-16-509/28/18 14:5339.8 18.1 1
PCB-1242 (Aroclor 1242)ND ug/kg 09/29/18 14:08 53469-21-909/28/18 14:5339.8 18.1 1
PCB-1248 (Aroclor 1248)ND ug/kg 09/29/18 14:08 12672-29-609/28/18 14:5339.8 18.1 1
PCB-1254 (Aroclor 1254)ND ug/kg 09/29/18 14:08 11097-69-109/28/18 14:5339.8 18.1 1
PCB-1260 (Aroclor 1260)ND ug/kg 09/29/18 14:08 11096-82-509/28/18 14:5339.8 18.1 1
Surrogates
Decachlorobiphenyl (S)94 %09/29/18 14:08 2051-24-309/28/18 14:5321-132 1
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/02/18 18:45 83-32-909/28/18 16:1911.8 1.8 1
Acenaphthylene ND ug/kg 10/02/18 18:45 208-96-809/28/18 16:1911.8 1.5 1
Anthracene ND ug/kg 10/02/18 18:45 120-12-709/28/18 16:1911.8 1.7 1
Benzo(a)anthracene ND ug/kg 10/02/18 18:45 56-55-309/28/18 16:1911.8 0.84 1
Benzo(a)pyrene ND ug/kg 10/02/18 18:45 50-32-809/28/18 16:1911.8 1.3 1
Benzo(b)fluoranthene ND ug/kg 10/02/18 18:45 205-99-209/28/18 16:1911.8 0.79 1
Benzo(g,h,i)perylene ND ug/kg 10/02/18 18:45 191-24-209/28/18 16:1911.8 3.1 1
Benzo(k)fluoranthene ND ug/kg 10/02/18 18:45 207-08-909/28/18 16:1911.8 1.8 1
Chrysene ND ug/kg 10/02/18 18:45 218-01-909/28/18 16:1911.8 2.1 1
Dibenz(a,h)anthracene ND ug/kg 10/02/18 18:45 53-70-309/28/18 16:1911.8 2.1 1
Fluoranthene ND ug/kg 10/02/18 18:45 206-44-009/28/18 16:1911.8 0.98 1
Fluorene ND ug/kg 10/02/18 18:45 86-73-709/28/18 16:1911.8 1.9 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/02/18 18:45 193-39-509/28/18 16:1911.8 3.3 1
1-Methylnaphthalene ND ug/kg 10/02/18 18:45 90-12-009/28/18 16:1911.8 1.4 1
2-Methylnaphthalene ND ug/kg 10/02/18 18:45 91-57-609/28/18 16:1911.8 1.3 1
Naphthalene ND ug/kg 10/02/18 18:45 91-20-309/28/18 16:1911.8 2.7 1
Phenanthrene ND ug/kg 10/02/18 18:45 85-01-809/28/18 16:1911.8 1.8 1
Pyrene ND ug/kg 10/02/18 18:45 129-00-009/28/18 16:1911.8 2.1 1
Surrogates
Nitrobenzene-d5 (S)69 %10/02/18 18:45 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)63 %10/02/18 18:45 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)71 %10/02/18 18:45 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.6 %09/27/18 18:200.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:50 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401220
Frmr Cathode/Anode Plant Area
Sample:ANO-SB001 (0'-1')Lab ID:92401220005 Collected:09/24/18 13:40 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8082A Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 09/29/18 14:28 12674-11-209/28/18 14:5339.4 17.9 1
PCB-1221 (Aroclor 1221)ND ug/kg 09/29/18 14:28 11104-28-209/28/18 14:5339.4 17.9 1
PCB-1232 (Aroclor 1232)ND ug/kg 09/29/18 14:28 11141-16-509/28/18 14:5339.4 17.9 1
PCB-1242 (Aroclor 1242)18.0J ug/kg 09/29/18 14:28 53469-21-909/28/18 14:5339.4 17.9 1
PCB-1248 (Aroclor 1248)ND ug/kg 09/29/18 14:28 12672-29-609/28/18 14:5339.4 17.9 1
PCB-1254 (Aroclor 1254)ND ug/kg 09/29/18 14:28 11097-69-109/28/18 14:5339.4 17.9 1
PCB-1260 (Aroclor 1260)ND ug/kg 09/29/18 14:28 11096-82-509/28/18 14:5339.4 17.9 1
Surrogates
Decachlorobiphenyl (S)113 %09/29/18 14:28 2051-24-309/28/18 14:5321-132 1
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 199 ug/kg 10/03/18 00:23 83-32-909/28/18 16:1911.9 1.8 1
Acenaphthylene 840 ug/kg 10/03/18 00:23 208-96-809/28/18 16:1911.9 1.6 1
Anthracene 1060 ug/kg 10/03/18 09:35 120-12-709/28/18 16:1911916.7 10
Benzo(a)anthracene 3140 ug/kg 10/03/18 09:35 56-55-309/28/18 16:191198.5 10
Benzo(a)pyrene 2710 ug/kg 10/03/18 09:35 50-32-809/28/18 16:1911913.1 10
Benzo(b)fluoranthene 4390 ug/kg 10/03/18 09:35 205-99-209/28/18 16:191198.0 10
Benzo(g,h,i)perylene 1830 ug/kg 10/03/18 09:35 191-24-209/28/18 16:1911931.1 10
Benzo(k)fluoranthene 1170 ug/kg 10/03/18 09:35 207-08-909/28/18 16:1911917.9 10
Chrysene 2690 ug/kg 10/03/18 09:35 218-01-909/28/18 16:1911921.5 10
Dibenz(a,h)anthracene 501 ug/kg 10/03/18 00:23 53-70-309/28/18 16:1911.9 2.2 1
Fluoranthene 5870 ug/kg 10/03/18 09:35 206-44-009/28/18 16:191199.9 10
Fluorene 559 ug/kg 10/03/18 00:23 86-73-709/28/18 16:1911.9 1.9 1
Indeno(1,2,3-cd)pyrene 1770 ug/kg 10/03/18 09:35 193-39-509/28/18 16:1911933.5 10
1-Methylnaphthalene 61.3 ug/kg 10/03/18 00:23 90-12-009/28/18 16:1911.9 1.4 1
2-Methylnaphthalene 78.2 ug/kg 10/03/18 00:23 91-57-609/28/18 16:1911.9 1.3 1
Naphthalene 155 ug/kg 10/03/18 00:23 91-20-309/28/18 16:1911.9 2.7 1
Phenanthrene 3670 ug/kg 10/03/18 09:35 85-01-809/28/18 16:1911917.9 10
Pyrene 4750 ug/kg 10/03/18 09:35 129-00-009/28/18 16:1911921.5 10
Surrogates
Nitrobenzene-d5 (S)71 %10/03/18 00:23 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)73 %10/03/18 00:23 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)92 %10/03/18 00:23 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.0 %09/27/18 18:210.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:50 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401220
Frmr Cathode/Anode Plant Area
Sample:ANO-SB001 (4'-5')Lab ID:92401220006 Collected:09/24/18 13:45 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8082A Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 09/29/18 14:48 12674-11-209/28/18 14:5337.2 16.9 1
PCB-1221 (Aroclor 1221)ND ug/kg 09/29/18 14:48 11104-28-209/28/18 14:5337.2 16.9 1
PCB-1232 (Aroclor 1232)ND ug/kg 09/29/18 14:48 11141-16-509/28/18 14:5337.2 16.9 1
PCB-1242 (Aroclor 1242)ND ug/kg 09/29/18 14:48 53469-21-909/28/18 14:5337.2 16.9 1
PCB-1248 (Aroclor 1248)ND ug/kg 09/29/18 14:48 12672-29-609/28/18 14:5337.2 16.9 1
PCB-1254 (Aroclor 1254)ND ug/kg 09/29/18 14:48 11097-69-109/28/18 14:5337.2 16.9 1
PCB-1260 (Aroclor 1260)ND ug/kg 09/29/18 14:48 11096-82-509/28/18 14:5337.2 16.9 1
Surrogates
Decachlorobiphenyl (S)102 %09/29/18 14:48 2051-24-309/28/18 14:5321-132 1
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 8.4J ug/kg 10/02/18 19:07 83-32-909/28/18 16:1911.3 1.7 1
Acenaphthylene ND ug/kg 10/02/18 19:07 208-96-809/28/18 16:1911.3 1.5 1
Anthracene 12.0 ug/kg 10/02/18 19:07 120-12-709/28/18 16:1911.3 1.6 1
Benzo(a)anthracene 35.1 ug/kg 10/02/18 19:07 56-55-309/28/18 16:1911.3 0.80 1
Benzo(a)pyrene 35.5 ug/kg 10/02/18 19:07 50-32-809/28/18 16:1911.3 1.2 1
Benzo(b)fluoranthene 52.3 ug/kg 10/02/18 19:07 205-99-209/28/18 16:1911.3 0.76 1
Benzo(g,h,i)perylene 27.1 ug/kg 10/02/18 19:07 191-24-209/28/18 16:1911.3 2.9 1
Benzo(k)fluoranthene 18.3 ug/kg 10/02/18 19:07 207-08-909/28/18 16:1911.3 1.7 1
Chrysene 32.7 ug/kg 10/02/18 19:07 218-01-909/28/18 16:1911.3 2.0 1
Dibenz(a,h)anthracene 7.5J ug/kg 10/02/18 19:07 53-70-309/28/18 16:1911.3 2.0 1
Fluoranthene 70.9 ug/kg 10/02/18 19:07 206-44-009/28/18 16:1911.3 0.94 1
Fluorene 5.9J ug/kg 10/02/18 19:07 86-73-709/28/18 16:1911.3 1.8 1
Indeno(1,2,3-cd)pyrene 24.5 ug/kg 10/02/18 19:07 193-39-509/28/18 16:1911.3 3.2 1
1-Methylnaphthalene 2.0J ug/kg 10/02/18 19:07 90-12-009/28/18 16:1911.3 1.4 1
2-Methylnaphthalene 3.9J ug/kg 10/02/18 19:07 91-57-609/28/18 16:1911.3 1.2 1
Naphthalene 11.5 ug/kg 10/02/18 19:07 91-20-309/28/18 16:1911.3 2.6 1
Phenanthrene 52.1 ug/kg 10/02/18 19:07 85-01-809/28/18 16:1911.3 1.7 1
Pyrene 56.1 ug/kg 10/02/18 19:07 129-00-009/28/18 16:1911.3 2.0 1
Surrogates
Nitrobenzene-d5 (S)70 %10/02/18 19:07 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)63 %10/02/18 19:07 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)68 %10/02/18 19:07 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 12.2 %09/27/18 18:210.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:50 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401220
Frmr Cathode/Anode Plant Area
Sample:ANO-SB002 (0'-1')Lab ID:92401220007 Collected:09/24/18 14:05 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8082A Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 10/02/18 16:33 12674-11-209/28/18 14:5337.3 16.9 1
PCB-1221 (Aroclor 1221)ND ug/kg 10/02/18 16:33 11104-28-209/28/18 14:5337.3 16.9 1
PCB-1232 (Aroclor 1232)44.5 ug/kg 10/02/18 16:33 11141-16-509/28/18 14:5337.3 16.9 1
PCB-1242 (Aroclor 1242)ND ug/kg 10/02/18 16:33 53469-21-909/28/18 14:5337.3 16.9 1
PCB-1248 (Aroclor 1248)ND ug/kg 10/02/18 16:33 12672-29-609/28/18 14:5337.3 16.9 1
PCB-1254 (Aroclor 1254)ND ug/kg 10/02/18 16:33 11097-69-109/28/18 14:5337.3 16.9 1
PCB-1260 (Aroclor 1260)ND ug/kg 10/02/18 16:33 11096-82-509/28/18 14:5337.3 16.9 1
Surrogates
Decachlorobiphenyl (S)65 %10/02/18 16:33 2051-24-309/28/18 14:5321-132 1
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 59.6 ug/kg 10/03/18 00:44 83-32-909/28/18 16:1911.3 1.7 1
Acenaphthylene 88.7 ug/kg 10/03/18 00:44 208-96-809/28/18 16:1911.3 1.5 1
Anthracene 157 ug/kg 10/03/18 00:44 120-12-709/28/18 16:1911.3 1.6 1
Benzo(a)anthracene 815 ug/kg 10/03/18 00:44 56-55-309/28/18 16:1911.3 0.80 1
Benzo(a)pyrene 810 ug/kg 10/03/18 00:44 50-32-809/28/18 16:1911.3 1.2 1
Benzo(b)fluoranthene 1290 ug/kg 10/03/18 09:56 205-99-209/28/18 16:1922.5 1.5 2
Benzo(g,h,i)perylene 372 ug/kg 10/03/18 00:44 191-24-209/28/18 16:1911.3 2.9 1
Benzo(k)fluoranthene 338 ug/kg 10/03/18 00:44 207-08-909/28/18 16:1911.3 1.7 1
Chrysene 851 ug/kg 10/03/18 00:44 218-01-909/28/18 16:1911.3 2.0 1
Dibenz(a,h)anthracene 40.0 ug/kg 10/03/18 00:44 53-70-309/28/18 16:1911.3 2.0 1
Fluoranthene 1080 ug/kg 10/03/18 09:56 206-44-009/28/18 16:1922.5 1.9 2
Fluorene 47.3 ug/kg 10/03/18 00:44 86-73-709/28/18 16:1911.3 1.8 1
Indeno(1,2,3-cd)pyrene 371 ug/kg 10/03/18 00:44 193-39-509/28/18 16:1911.3 3.2 1
1-Methylnaphthalene 37.9 ug/kg 10/03/18 00:44 90-12-009/28/18 16:1911.3 1.4 1
2-Methylnaphthalene 52.5 ug/kg 10/03/18 00:44 91-57-609/28/18 16:1911.3 1.2 1
Naphthalene 76.8 ug/kg 10/03/18 00:44 91-20-309/28/18 16:1911.3 2.6 1
Phenanthrene 488 ug/kg 10/03/18 00:44 85-01-809/28/18 16:1911.3 1.7 1
Pyrene 1120 ug/kg 10/03/18 09:56 129-00-009/28/18 16:1922.5 4.1 2
Surrogates
Nitrobenzene-d5 (S)71 %10/03/18 00:44 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)71 %10/03/18 00:44 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)84 %10/03/18 00:44 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 11.5 %09/27/18 18:210.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:50 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401220
Frmr Cathode/Anode Plant Area
Sample:ANO-SB002 (4'-5')Lab ID:92401220008 Collected:09/24/18 14:10 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8082A Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 09/29/18 15:28 12674-11-209/28/18 14:5340.2 18.3 1
PCB-1221 (Aroclor 1221)ND ug/kg 09/29/18 15:28 11104-28-209/28/18 14:5340.2 18.3 1
PCB-1232 (Aroclor 1232)ND ug/kg 09/29/18 15:28 11141-16-509/28/18 14:5340.2 18.3 1
PCB-1242 (Aroclor 1242)ND ug/kg 09/29/18 15:28 53469-21-909/28/18 14:5340.2 18.3 1
PCB-1248 (Aroclor 1248)ND ug/kg 09/29/18 15:28 12672-29-609/28/18 14:5340.2 18.3 1
PCB-1254 (Aroclor 1254)ND ug/kg 09/29/18 15:28 11097-69-109/28/18 14:5340.2 18.3 1
PCB-1260 (Aroclor 1260)ND ug/kg 09/29/18 15:28 11096-82-509/28/18 14:5340.2 18.3 1
Surrogates
Decachlorobiphenyl (S)107 %09/29/18 15:28 2051-24-309/28/18 14:5321-132 1
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/02/18 19:28 83-32-909/28/18 16:1912.1 1.8 1
Acenaphthylene ND ug/kg 10/02/18 19:28 208-96-809/28/18 16:1912.1 1.6 1
Anthracene 2.2J ug/kg 10/02/18 19:28 120-12-709/28/18 16:1912.1 1.7 1
Benzo(a)anthracene 6.3J ug/kg 10/02/18 19:28 56-55-309/28/18 16:1912.1 0.86 1
Benzo(a)pyrene 6.0J ug/kg 10/02/18 19:28 50-32-809/28/18 16:1912.1 1.3 1
Benzo(b)fluoranthene 9.6J ug/kg 10/02/18 19:28 205-99-209/28/18 16:1912.1 0.81 1
Benzo(g,h,i)perylene 5.0J ug/kg 10/02/18 19:28 191-24-209/28/18 16:1912.1 3.1 1
Benzo(k)fluoranthene 2.8J ug/kg 10/02/18 19:28 207-08-909/28/18 16:1912.1 1.8 1
Chrysene 6.0J ug/kg 10/02/18 19:28 218-01-909/28/18 16:1912.1 2.2 1
Dibenz(a,h)anthracene ND ug/kg 10/02/18 19:28 53-70-309/28/18 16:1912.1 2.2 1
Fluoranthene 11.3J ug/kg 10/02/18 19:28 206-44-009/28/18 16:1912.1 1.0 1
Fluorene ND ug/kg 10/02/18 19:28 86-73-709/28/18 16:1912.1 1.9 1
Indeno(1,2,3-cd)pyrene 4.1J ug/kg 10/02/18 19:28 193-39-509/28/18 16:1912.1 3.4 1
1-Methylnaphthalene ND ug/kg 10/02/18 19:28 90-12-009/28/18 16:1912.1 1.4 1
2-Methylnaphthalene 1.8J ug/kg 10/02/18 19:28 91-57-609/28/18 16:1912.1 1.3 1
Naphthalene ND ug/kg 10/02/18 19:28 91-20-309/28/18 16:1912.1 2.8 1
Phenanthrene 8.2J ug/kg 10/02/18 19:28 85-01-809/28/18 16:1912.1 1.8 1
Pyrene 10.3J ug/kg 10/02/18 19:28 129-00-009/28/18 16:1912.1 2.2 1
Surrogates
Nitrobenzene-d5 (S)91 %10/02/18 19:28 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)83 %10/02/18 19:28 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)92 %10/02/18 19:28 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.2 %09/27/18 18:210.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:50 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401220
Frmr Cathode/Anode Plant Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
433359
EPA 3546
EPA 8082A
8082 GCS PCB
Associated Lab Samples:92401220001, 92401220002, 92401220003, 92401220004, 92401220005, 92401220006, 92401220007,
92401220008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2387887
Associated Lab Samples:92401220001, 92401220002, 92401220003, 92401220004, 92401220005, 92401220006, 92401220007,
92401220008
Matrix:Solid
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/kg ND 33.1 09/29/18 17:4815.1
PCB-1221 (Aroclor 1221)ug/kg ND 33.1 09/29/18 17:4815.1
PCB-1232 (Aroclor 1232)ug/kg ND 33.1 09/29/18 17:4815.1
PCB-1242 (Aroclor 1242)ug/kg ND 33.1 09/29/18 17:4815.1
PCB-1248 (Aroclor 1248)ug/kg ND 33.1 09/29/18 17:4815.1
PCB-1254 (Aroclor 1254)ug/kg ND 33.1 09/29/18 17:4815.1
PCB-1260 (Aroclor 1260)ug/kg ND 33.1 09/29/18 17:4815.1
Decachlorobiphenyl (S)%116 21-132 09/29/18 17:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2387888LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2387889
PCB-1016 (Aroclor 1016)ug/kg 157169 93 31-12091149 5 30
PCB-1260 (Aroclor 1260)ug/kg 187169 111 32-120104172 8 30
Decachlorobiphenyl (S)%110 21-132102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:50 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401220
Frmr Cathode/Anode Plant Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
433443
EPA 3546
EPA 8270D by SIM
8270 MSSV PAH by SIM
Associated Lab Samples:92401220001, 92401220002, 92401220003, 92401220004, 92401220005, 92401220006, 92401220007,
92401220008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2388169
Associated Lab Samples:92401220001, 92401220002, 92401220003, 92401220004, 92401220005, 92401220006, 92401220007,
92401220008
Matrix:Solid
AnalyzedMDL
1-Methylnaphthalene ug/kg ND 10 10/02/18 10:571.2
2-Methylnaphthalene ug/kg ND 10 10/02/18 10:571.1
Acenaphthene ug/kg ND 10 10/02/18 10:571.5
Acenaphthylene ug/kg ND 10 10/02/18 10:571.3
Anthracene ug/kg ND 10 10/02/18 10:571.4
Benzo(a)anthracene ug/kg ND 10 10/02/18 10:570.71
Benzo(a)pyrene ug/kg ND 10 10/02/18 10:571.1
Benzo(b)fluoranthene ug/kg ND 10 10/02/18 10:570.67
Benzo(g,h,i)perylene ug/kg ND 10 10/02/18 10:572.6
Benzo(k)fluoranthene ug/kg ND 10 10/02/18 10:571.5
Chrysene ug/kg ND 10 10/02/18 10:571.8
Dibenz(a,h)anthracene ug/kg ND 10 10/02/18 10:571.8
Fluoranthene ug/kg ND 10 10/02/18 10:570.83
Fluorene ug/kg ND 10 10/02/18 10:571.6
Indeno(1,2,3-cd)pyrene ug/kg ND 10 10/02/18 10:572.8
Naphthalene ug/kg ND 10 10/02/18 10:572.3
Phenanthrene ug/kg ND 10 10/02/18 10:571.5
Pyrene ug/kg ND 10 10/02/18 10:571.8
2-Fluorobiphenyl (S)%88 10-110 10/02/18 10:57
Nitrobenzene-d5 (S)%98 10-128 10/02/18 10:57
Terphenyl-d14 (S)%101 39-119 10/02/18 10:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2388171LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/kg 30.133.8 89 44-130
2-Methylnaphthalene ug/kg 31.133.8 92 41-134
Acenaphthene ug/kg 31.833.8 94 52-123
Acenaphthylene ug/kg 30.633.8 90 49-116
Anthracene ug/kg 31.833.8 94 41-133
Benzo(a)anthracene ug/kg 31.933.8 94 56-130
Benzo(a)pyrene ug/kg 31.033.8 92 51-136
Benzo(b)fluoranthene ug/kg 34.633.8 102 37-149
Benzo(g,h,i)perylene ug/kg 29.333.8 87 39-127
Benzo(k)fluoranthene ug/kg 31.933.8 94 45-139
Chrysene ug/kg 32.433.8 96 59-127
Dibenz(a,h)anthracene ug/kg 32.933.8 97 37-139
Fluoranthene ug/kg 32.333.8 96 53-132
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:50 AM
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Page 14 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401220
Frmr Cathode/Anode Plant Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2388171LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 32.133.8 95 45-127
Indeno(1,2,3-cd)pyrene ug/kg 33.633.8 99 35-145
Naphthalene ug/kg 29.533.8 87 45-123
Phenanthrene ug/kg 31.633.8 93 50-125
Pyrene ug/kg 32.233.8 95 52-132
2-Fluorobiphenyl (S)%93 10-110
Nitrobenzene-d5 (S)%99 10-128
Terphenyl-d14 (S)%99 39-119
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2388172MATRIX SPIKE SAMPLE:
MSSpike
Result
92401224001
1-Methylnaphthalene ug/kg 33.540.6 78 50-150ND
2-Methylnaphthalene ug/kg 37.240.6 84 50-150ND
Acenaphthene ug/kg 30.840.6 74 50-150ND
Acenaphthylene ug/kg 27.740.6 67 50-150ND
Anthracene ug/kg 33.640.6 77 50-150ND
Benzo(a)anthracene ug/kg 80.440.6 117 50-15032.8
Benzo(a)pyrene ug/kg 83.340.6 82 50-15050.1
Benzo(b)fluoranthene ug/kg 12740.6 79 50-15094.8
Benzo(g,h,i)perylene ug/kg 76.5 M140.6 42 50-15059.4
Benzo(k)fluoranthene ug/kg 59.240.6 67 50-15031.9
Chrysene ug/kg 82.240.6 110 50-15037.5
Dibenz(a,h)anthracene ug/kg 39.340.6 85 50-150ND
Fluoranthene ug/kg 101 M140.6 154 50-15038.2
Fluorene ug/kg 30.540.6 74 50-150ND
Indeno(1,2,3-cd)pyrene ug/kg 74.340.6 53 50-15052.6
Naphthalene ug/kg 36.840.6 84 50-150ND
Phenanthrene ug/kg 55.340.6 105 50-15012.7
Pyrene ug/kg 89.340.6 132 50-15035.5
2-Fluorobiphenyl (S)%72 10-110
Nitrobenzene-d5 (S)%78 10-128
Terphenyl-d14 (S)%74 39-119
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92401224002
2388173SAMPLE DUPLICATE:
1-Methylnaphthalene ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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Page 15 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401220
Frmr Cathode/Anode Plant Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92401224002
2388173SAMPLE DUPLICATE:
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2-Fluorobiphenyl (S)%70 977
Nitrobenzene-d5 (S)%77 984
Terphenyl-d14 (S)%80 584
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:50 AM
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Page 16 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401220
Frmr Cathode/Anode Plant Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
433173
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92401220001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92401023029
2387221SAMPLE DUPLICATE:
Percent Moisture %19.5 D6432512.6
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92401224018
2387222SAMPLE DUPLICATE:
Percent Moisture %15.1 3 2515.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:50 AM
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Page 17 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401220
Frmr Cathode/Anode Plant Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
433178
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92401220002, 92401220003, 92401220004, 92401220005, 92401220006, 92401220007, 92401220008
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92401183013
2387274SAMPLE DUPLICATE:
Percent Moisture %17.2 8 2518.7
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400899002
2387275SAMPLE DUPLICATE:
Percent Moisture %13.8 5 2514.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:50 AM
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Page 18 of 23
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92401220
Frmr Cathode/Anode Plant Area
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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Page 19 of 23
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92401220
Frmr Cathode/Anode Plant Area
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92401220001 433359 433541CAT-SB001 (0'-1')EPA 3546 EPA 8082A
92401220002 433359 433541CAT-SB001 (4'-5')EPA 3546 EPA 8082A
92401220003 433359 433541CAT-SB002 (0'-1')EPA 3546 EPA 8082A
92401220004 433359 433541CAT-SB002 (4'-5')EPA 3546 EPA 8082A
92401220005 433359 433541ANO-SB001 (0'-1')EPA 3546 EPA 8082A
92401220006 433359 433541ANO-SB001 (4'-5')EPA 3546 EPA 8082A
92401220007 433359 433541ANO-SB002 (0'-1')EPA 3546 EPA 8082A
92401220008 433359 433541ANO-SB002 (4'-5')EPA 3546 EPA 8082A
92401220001 433443 433807CAT-SB001 (0'-1')EPA 3546 EPA 8270D by SIM
92401220002 433443 433807CAT-SB001 (4'-5')EPA 3546 EPA 8270D by SIM
92401220003 433443 433807CAT-SB002 (0'-1')EPA 3546 EPA 8270D by SIM
92401220004 433443 433807CAT-SB002 (4'-5')EPA 3546 EPA 8270D by SIM
92401220005 433443 433807ANO-SB001 (0'-1')EPA 3546 EPA 8270D by SIM
92401220006 433443 433807ANO-SB001 (4'-5')EPA 3546 EPA 8270D by SIM
92401220007 433443 433807ANO-SB002 (0'-1')EPA 3546 EPA 8270D by SIM
92401220008 433443 433807ANO-SB002 (4'-5')EPA 3546 EPA 8270D by SIM
92401220001 433173CAT-SB001 (0'-1')ASTM D2974-87
92401220002 433178CAT-SB001 (4'-5')ASTM D2974-87
92401220003 433178CAT-SB002 (0'-1')ASTM D2974-87
92401220004 433178CAT-SB002 (4'-5')ASTM D2974-87
92401220005 433178ANO-SB001 (0'-1')ASTM D2974-87
92401220006 433178ANO-SB001 (4'-5')ASTM D2974-87
92401220007 433178ANO-SB002 (0'-1')ASTM D2974-87
92401220008 433178ANO-SB002 (4'-5')ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 08:50 AM
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Page 20 of 23
Page 21 of 23
Page 22 of 23
Page 23 of 23
#=CL#
November 12, 2018
LIMS USE: FR - MICHAEL WORDEN
LIMS OBJECT ID: 92400643
92400643
Project:
Pace Project No.:
RE:
Michael W. Worden
Environeering, Inc.
16100 Cairnway
Suite 320
Houston, TX 77084
Frmr Electrical Shop/Warehouse
Dear Michael Worden:
Enclosed are the analytical results for sample(s) received by the laboratory on September 25, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
This revision was issued on 11/12/18 to report J-flagged results to the MDL, per client request.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 1 of 40
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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Page 2 of 40
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Lab ID Sample ID Matrix Date Collected Date Received
92400643001 ESW-SB001 (0'-1')Solid 09/24/18 12:10 09/25/18 07:30
92400643002 ESW-SB001 (0'-1') DUP Solid 09/24/18 12:15 09/25/18 07:30
92400643003 ESW-SB001 (4'-5')Solid 09/24/18 12:25 09/25/18 07:30
92400643004 ESW-TB001 Water 09/24/18 00:00 09/25/18 07:30
REPORT OF LABORATORY ANALYSIS
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Page 3 of 40
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92400643001 ESW-SB001 (0'-1')EPA 8082A 8 PASI-CSEM
EPA 8270D by SIM 21 PASI-CPKS
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92400643002 ESW-SB001 (0'-1') DUP EPA 8082A 8 PASI-CSEM
EPA 8270D by SIM 21 PASI-CPKS
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92400643003 ESW-SB001 (4'-5')EPA 8082A 8 PASI-CSEM
EPA 8270D by SIM 21 PASI-CPKS
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92400643004 ESW-TB001 EPA 8260B 71 PASI-CSAS
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 4 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Sample:ESW-SB001 (0'-1')Lab ID:92400643001 Collected:09/24/18 12:10 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8082A Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 09/26/18 15:56 12674-11-209/25/18 15:3541.3 18.8 1
PCB-1221 (Aroclor 1221)ND ug/kg 09/26/18 15:56 11104-28-209/25/18 15:3541.3 18.8 1
PCB-1232 (Aroclor 1232)ND ug/kg 09/26/18 15:56 11141-16-509/25/18 15:3541.3 18.8 1
PCB-1242 (Aroclor 1242)ND ug/kg 09/26/18 15:56 53469-21-909/25/18 15:3541.3 18.8 1
PCB-1248 (Aroclor 1248)ND ug/kg 09/26/18 15:56 12672-29-609/25/18 15:3541.3 18.8 1
PCB-1254 (Aroclor 1254)ND ug/kg 09/26/18 15:56 11097-69-109/25/18 15:3541.3 18.8 1
PCB-1260 (Aroclor 1260)ND ug/kg 09/26/18 15:56 11096-82-509/25/18 15:3541.3 18.8 1
Surrogates
Decachlorobiphenyl (S)33 %09/26/18 15:56 2051-24-309/25/18 15:3521-132 1
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 22.7J ug/kg 09/28/18 13:22 83-32-909/25/18 15:5262.4 9.4 5
Acenaphthylene 34.6J ug/kg 09/28/18 13:22 208-96-809/25/18 15:5262.4 8.1 5
Anthracene 133 ug/kg 09/28/18 13:22 120-12-709/25/18 15:5262.4 8.7 5
Benzo(a)anthracene 3910 ug/kg 09/28/18 13:22 56-55-309/25/18 15:5262.4 4.4 5
Benzo(a)pyrene 1550 ug/kg 09/28/18 13:22 50-32-809/25/18 15:5262.4 6.9 5
Benzo(b)fluoranthene 5570 ug/kg 09/28/18 15:49 205-99-209/25/18 15:521258.4 10
Benzo(g,h,i)perylene 1370 ug/kg 09/28/18 13:22 191-24-209/25/18 15:5262.4 16.2 5
Benzo(k)fluoranthene 1760 ug/kg 09/28/18 13:22 207-08-909/25/18 15:5262.4 9.4 5
Chrysene 4170 ug/kg 09/28/18 13:22 218-01-909/25/18 15:5262.4 11.2 5
Dibenz(a,h)anthracene 509 ug/kg 09/28/18 13:22 53-70-309/25/18 15:5262.4 11.2 5
Fluoranthene 1530 ug/kg 09/28/18 13:22 206-44-009/25/18 15:5262.4 5.2 5
Fluorene 16.8J ug/kg 09/28/18 13:22 86-73-709/25/18 15:5262.4 10 5
Indeno(1,2,3-cd)pyrene 1150 ug/kg 09/28/18 13:22 193-39-509/25/18 15:5262.4 17.5 5
1-Methylnaphthalene 150 ug/kg 09/28/18 13:22 90-12-009/25/18 15:5262.4 7.5 5
2-Methylnaphthalene 213 ug/kg 09/28/18 13:22 91-57-609/25/18 15:5262.4 6.9 5
Naphthalene 167 ug/kg 09/28/18 13:22 91-20-309/25/18 15:5262.4 14.3 5
Phenanthrene 456 ug/kg 09/28/18 13:22 85-01-809/25/18 15:5262.4 9.4 5
Pyrene 1770 ug/kg 09/28/18 13:22 129-00-009/25/18 15:5262.4 11.2 5
Surrogates
Nitrobenzene-d5 (S)60 %09/28/18 13:22 4165-60-0 D309/25/18 15:5210-128 5
2-Fluorobiphenyl (S)60 %09/28/18 13:22 321-60-809/25/18 15:5210-110 5
Terphenyl-d14 (S)75 %09/28/18 13:22 1718-51-009/25/18 15:5239-119 5
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone 12.1J ug/kg 09/25/18 19:02 67-64-109/25/18 14:4299.4 9.9 1
Benzene ND ug/kg 09/25/18 19:02 71-43-209/25/18 14:425.0 1.6 1
Bromobenzene ND ug/kg 09/25/18 19:02 108-86-109/25/18 14:425.0 2.0 1
Bromochloromethane ND ug/kg 09/25/18 19:02 74-97-509/25/18 14:425.0 1.7 1
Bromodichloromethane ND ug/kg 09/25/18 19:02 75-27-409/25/18 14:425.0 1.9 1
Bromoform ND ug/kg 09/25/18 19:02 75-25-209/25/18 14:425.0 2.3 1
Bromomethane ND ug/kg 09/25/18 19:02 74-83-909/25/18 14:429.9 2.5 1
2-Butanone (MEK)ND ug/kg 09/25/18 19:02 78-93-309/25/18 14:4299.4 2.9 1
n-Butylbenzene ND ug/kg 09/25/18 19:02 104-51-809/25/18 14:425.0 1.8 1
sec-Butylbenzene ND ug/kg 09/25/18 19:02 135-98-809/25/18 14:425.0 1.6 1
REPORT OF LABORATORY ANALYSIS
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Page 5 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Sample:ESW-SB001 (0'-1')Lab ID:92400643001 Collected:09/24/18 12:10 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
tert-Butylbenzene ND ug/kg 09/25/18 19:02 98-06-609/25/18 14:425.0 2.0 1
Carbon tetrachloride ND ug/kg 09/25/18 19:02 56-23-509/25/18 14:425.0 2.6 1
Chlorobenzene ND ug/kg 09/25/18 19:02 108-90-709/25/18 14:425.0 1.9 1
Chloroethane ND ug/kg 09/25/18 19:02 75-00-309/25/18 14:429.9 2.4 1
Chloroform ND ug/kg 09/25/18 19:02 67-66-309/25/18 14:425.0 1.6 1
Chloromethane ND ug/kg 09/25/18 19:02 74-87-309/25/18 14:429.9 2.4 1
2-Chlorotoluene ND ug/kg 09/25/18 19:02 95-49-809/25/18 14:425.0 1.7 1
4-Chlorotoluene ND ug/kg 09/25/18 19:02 106-43-409/25/18 14:425.0 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/25/18 19:02 96-12-809/25/18 14:425.0 3.6 1
Dibromochloromethane ND ug/kg 09/25/18 19:02 124-48-109/25/18 14:425.0 1.8 1
1,2-Dibromoethane (EDB)ND ug/kg 09/25/18 19:02 106-93-409/25/18 14:425.0 1.8 1
Dibromomethane ND ug/kg 09/25/18 19:02 74-95-309/25/18 14:425.0 2.5 1
1,2-Dichlorobenzene ND ug/kg 09/25/18 19:02 95-50-109/25/18 14:425.0 1.9 1
1,3-Dichlorobenzene ND ug/kg 09/25/18 19:02 541-73-109/25/18 14:425.0 2.0 1
1,4-Dichlorobenzene ND ug/kg 09/25/18 19:02 106-46-709/25/18 14:425.0 1.7 1
Dichlorodifluoromethane ND ug/kg 09/25/18 19:02 75-71-809/25/18 14:429.9 3.6 1
1,1-Dichloroethane ND ug/kg 09/25/18 19:02 75-34-309/25/18 14:425.0 1.5 1
1,2-Dichloroethane ND ug/kg 09/25/18 19:02 107-06-209/25/18 14:425.0 2.2 1
1,1-Dichloroethene ND ug/kg 09/25/18 19:02 75-35-409/25/18 14:425.0 1.8 1
cis-1,2-Dichloroethene ND ug/kg 09/25/18 19:02 156-59-209/25/18 14:425.0 1.4 1
trans-1,2-Dichloroethene ND ug/kg 09/25/18 19:02 156-60-509/25/18 14:425.0 1.9 1
1,2-Dichloropropane ND ug/kg 09/25/18 19:02 78-87-509/25/18 14:425.0 1.7 1
1,3-Dichloropropane ND ug/kg 09/25/18 19:02 142-28-909/25/18 14:425.0 1.9 1
2,2-Dichloropropane ND ug/kg 09/25/18 19:02 594-20-709/25/18 14:425.0 1.7 1
1,1-Dichloropropene ND ug/kg 09/25/18 19:02 563-58-609/25/18 14:425.0 1.5 1
cis-1,3-Dichloropropene ND ug/kg 09/25/18 19:02 10061-01-509/25/18 14:425.0 1.8 1
trans-1,3-Dichloropropene ND ug/kg 09/25/18 19:02 10061-02-609/25/18 14:425.0 1.5 1
Diisopropyl ether ND ug/kg 09/25/18 19:02 108-20-309/25/18 14:425.0 1.7 1
Ethylbenzene ND ug/kg 09/25/18 19:02 100-41-409/25/18 14:425.0 1.8 1
Hexachloro-1,3-butadiene ND ug/kg 09/25/18 19:02 87-68-309/25/18 14:425.0 2.0 1
2-Hexanone ND ug/kg 09/25/18 19:02 591-78-609/25/18 14:4249.7 3.9 1
Isopropylbenzene (Cumene)ND ug/kg 09/25/18 19:02 98-82-809/25/18 14:425.0 1.9 1
p-Isopropyltoluene ND ug/kg 09/25/18 19:02 99-87-609/25/18 14:425.0 1.7 1
Methylene Chloride ND ug/kg 09/25/18 19:02 75-09-209/25/18 14:4219.9 3.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/25/18 19:02 108-10-109/25/18 14:4249.7 3.7 1
Methyl-tert-butyl ether ND ug/kg 09/25/18 19:02 1634-04-409/25/18 14:425.0 1.5 1
Naphthalene ND ug/kg 09/25/18 19:02 91-20-309/25/18 14:425.0 1.2 1
n-Propylbenzene ND ug/kg 09/25/18 19:02 103-65-109/25/18 14:425.0 1.7 1
Styrene ND ug/kg 09/25/18 19:02 100-42-509/25/18 14:425.0 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/25/18 19:02 630-20-609/25/18 14:425.0 2.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/25/18 19:02 79-34-509/25/18 14:425.0 1.9 1
Tetrachloroethene ND ug/kg 09/25/18 19:02 127-18-409/25/18 14:425.0 1.7 1
Toluene ND ug/kg 09/25/18 19:02 108-88-309/25/18 14:425.0 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 09/25/18 19:02 87-61-609/25/18 14:425.0 2.2 1
1,2,4-Trichlorobenzene ND ug/kg 09/25/18 19:02 120-82-109/25/18 14:425.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Sample:ESW-SB001 (0'-1')Lab ID:92400643001 Collected:09/24/18 12:10 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
1,1,1-Trichloroethane ND ug/kg 09/25/18 19:02 71-55-609/25/18 14:425.0 1.8 1
1,1,2-Trichloroethane ND ug/kg 09/25/18 19:02 79-00-509/25/18 14:425.0 2.1 1
Trichloroethene ND ug/kg 09/25/18 19:02 79-01-609/25/18 14:425.0 2.1 1
Trichlorofluoromethane ND ug/kg 09/25/18 19:02 75-69-409/25/18 14:425.0 2.2 1
1,2,3-Trichloropropane ND ug/kg 09/25/18 19:02 96-18-409/25/18 14:425.0 1.6 1
1,2,4-Trimethylbenzene ND ug/kg 09/25/18 19:02 95-63-609/25/18 14:425.0 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 09/25/18 19:02 108-67-809/25/18 14:425.0 1.8 1
Vinyl acetate ND ug/kg 09/25/18 19:02 108-05-409/25/18 14:4249.7 8.7 1
Vinyl chloride ND ug/kg 09/25/18 19:02 75-01-409/25/18 14:429.9 1.8 1
Xylene (Total)ND ug/kg 09/25/18 19:02 1330-20-709/25/18 14:429.9 3.6 1
m&p-Xylene ND ug/kg 09/25/18 19:02 179601-23-109/25/18 14:429.9 3.6 1
o-Xylene ND ug/kg 09/25/18 19:02 95-47-609/25/18 14:425.0 1.9 1
Surrogates
Toluene-d8 (S)98 %09/25/18 19:02 2037-26-509/25/18 14:4270-130 1
4-Bromofluorobenzene (S)89 %09/25/18 19:02 460-00-409/25/18 14:4270-130 1
1,2-Dichloroethane-d4 (S)93 %09/25/18 19:02 17060-07-009/25/18 14:4270-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.1 %09/25/18 15:100.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/02/18 16:12 57-12-5 M109/29/18 18:450.31 0.17 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 33.0 mg/kg 10/01/18 12:49 16984-48-810/01/18 09:306.2 3.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Sample:ESW-SB001 (0'-1') DUP Lab ID:92400643002 Collected:09/24/18 12:15 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8082A Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 09/26/18 16:16 12674-11-209/25/18 15:3539.2 17.8 1
PCB-1221 (Aroclor 1221)ND ug/kg 09/26/18 16:16 11104-28-209/25/18 15:3539.2 17.8 1
PCB-1232 (Aroclor 1232)ND ug/kg 09/26/18 16:16 11141-16-509/25/18 15:3539.2 17.8 1
PCB-1242 (Aroclor 1242)ND ug/kg 09/26/18 16:16 53469-21-909/25/18 15:3539.2 17.8 1
PCB-1248 (Aroclor 1248)ND ug/kg 09/26/18 16:16 12672-29-609/25/18 15:3539.2 17.8 1
PCB-1254 (Aroclor 1254)ND ug/kg 09/26/18 16:16 11097-69-109/25/18 15:3539.2 17.8 1
PCB-1260 (Aroclor 1260)ND ug/kg 09/26/18 16:16 11096-82-509/25/18 15:3539.2 17.8 1
Surrogates
Decachlorobiphenyl (S)178 %09/26/18 16:16 2051-24-3 S309/25/18 15:3521-132 1
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 26.8 ug/kg 09/27/18 18:03 83-32-909/25/18 15:5211.7 1.8 1
Acenaphthylene 26.6 ug/kg 09/27/18 18:03 208-96-809/25/18 15:5211.7 1.5 1
Anthracene 107 ug/kg 09/27/18 18:03 120-12-709/25/18 15:5211.7 1.6 1
Benzo(a)anthracene 875 ug/kg 09/28/18 13:43 56-55-309/25/18 15:5246.7 3.3 4
Benzo(a)pyrene 773 ug/kg 09/27/18 18:03 50-32-809/25/18 15:5211.7 1.3 1
Benzo(b)fluoranthene 1830 ug/kg 09/28/18 13:43 205-99-209/25/18 15:5246.7 3.1 4
Benzo(g,h,i)perylene 627 ug/kg 09/27/18 18:03 191-24-209/25/18 15:5211.7 3.0 1
Benzo(k)fluoranthene 639 ug/kg 09/27/18 18:03 207-08-909/25/18 15:5211.7 1.8 1
Chrysene 1790 ug/kg 09/28/18 13:43 218-01-909/25/18 15:5246.7 8.4 4
Dibenz(a,h)anthracene 242 ug/kg 09/27/18 18:03 53-70-309/25/18 15:5211.7 2.1 1
Fluoranthene 899 ug/kg 09/27/18 18:03 206-44-009/25/18 15:5211.7 0.97 1
Fluorene 20.7 ug/kg 09/27/18 18:03 86-73-709/25/18 15:5211.7 1.9 1
Indeno(1,2,3-cd)pyrene 555 ug/kg 09/27/18 18:03 193-39-509/25/18 15:5211.7 3.3 1
1-Methylnaphthalene 127 ug/kg 09/27/18 18:03 90-12-009/25/18 15:5211.7 1.4 1
2-Methylnaphthalene 184 ug/kg 09/27/18 18:03 91-57-609/25/18 15:5211.7 1.3 1
Naphthalene 155 ug/kg 09/27/18 18:03 91-20-309/25/18 15:5211.7 2.7 1
Phenanthrene 499 ug/kg 09/27/18 18:03 85-01-809/25/18 15:5211.7 1.8 1
Pyrene 868 ug/kg 09/27/18 18:03 129-00-009/25/18 15:5211.7 2.1 1
Surrogates
Nitrobenzene-d5 (S)68 %09/27/18 18:03 4165-60-009/25/18 15:5210-128 1
2-Fluorobiphenyl (S)66 %09/27/18 18:03 321-60-809/25/18 15:5210-110 1
Terphenyl-d14 (S)90 %09/27/18 18:03 1718-51-009/25/18 15:5239-119 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone 12.8J ug/kg 09/25/18 19:42 67-64-109/25/18 14:4286.4 8.6 1
Benzene ND ug/kg 09/25/18 19:42 71-43-209/25/18 14:424.3 1.4 1
Bromobenzene ND ug/kg 09/25/18 19:42 108-86-109/25/18 14:424.3 1.7 1
Bromochloromethane ND ug/kg 09/25/18 19:42 74-97-509/25/18 14:424.3 1.5 1
Bromodichloromethane ND ug/kg 09/25/18 19:42 75-27-409/25/18 14:424.3 1.6 1
Bromoform ND ug/kg 09/25/18 19:42 75-25-209/25/18 14:424.3 2.0 1
Bromomethane ND ug/kg 09/25/18 19:42 74-83-909/25/18 14:428.6 2.2 1
2-Butanone (MEK)ND ug/kg 09/25/18 19:42 78-93-309/25/18 14:4286.4 2.5 1
n-Butylbenzene ND ug/kg 09/25/18 19:42 104-51-809/25/18 14:424.3 1.6 1
sec-Butylbenzene ND ug/kg 09/25/18 19:42 135-98-809/25/18 14:424.3 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Sample:ESW-SB001 (0'-1') DUP Lab ID:92400643002 Collected:09/24/18 12:15 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
tert-Butylbenzene ND ug/kg 09/25/18 19:42 98-06-609/25/18 14:424.3 1.7 1
Carbon tetrachloride ND ug/kg 09/25/18 19:42 56-23-509/25/18 14:424.3 2.2 1
Chlorobenzene ND ug/kg 09/25/18 19:42 108-90-709/25/18 14:424.3 1.6 1
Chloroethane ND ug/kg 09/25/18 19:42 75-00-309/25/18 14:428.6 2.1 1
Chloroform ND ug/kg 09/25/18 19:42 67-66-309/25/18 14:424.3 1.4 1
Chloromethane ND ug/kg 09/25/18 19:42 74-87-309/25/18 14:428.6 2.1 1
2-Chlorotoluene ND ug/kg 09/25/18 19:42 95-49-809/25/18 14:424.3 1.5 1
4-Chlorotoluene ND ug/kg 09/25/18 19:42 106-43-409/25/18 14:424.3 1.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/25/18 19:42 96-12-809/25/18 14:424.3 3.1 1
Dibromochloromethane ND ug/kg 09/25/18 19:42 124-48-109/25/18 14:424.3 1.6 1
1,2-Dibromoethane (EDB)ND ug/kg 09/25/18 19:42 106-93-409/25/18 14:424.3 1.6 1
Dibromomethane ND ug/kg 09/25/18 19:42 74-95-309/25/18 14:424.3 2.2 1
1,2-Dichlorobenzene ND ug/kg 09/25/18 19:42 95-50-109/25/18 14:424.3 1.6 1
1,3-Dichlorobenzene ND ug/kg 09/25/18 19:42 541-73-109/25/18 14:424.3 1.7 1
1,4-Dichlorobenzene ND ug/kg 09/25/18 19:42 106-46-709/25/18 14:424.3 1.5 1
Dichlorodifluoromethane ND ug/kg 09/25/18 19:42 75-71-809/25/18 14:428.6 3.1 1
1,1-Dichloroethane ND ug/kg 09/25/18 19:42 75-34-309/25/18 14:424.3 1.3 1
1,2-Dichloroethane ND ug/kg 09/25/18 19:42 107-06-209/25/18 14:424.3 1.9 1
1,1-Dichloroethene ND ug/kg 09/25/18 19:42 75-35-409/25/18 14:424.3 1.6 1
cis-1,2-Dichloroethene ND ug/kg 09/25/18 19:42 156-59-209/25/18 14:424.3 1.2 1
trans-1,2-Dichloroethene ND ug/kg 09/25/18 19:42 156-60-509/25/18 14:424.3 1.6 1
1,2-Dichloropropane ND ug/kg 09/25/18 19:42 78-87-509/25/18 14:424.3 1.5 1
1,3-Dichloropropane ND ug/kg 09/25/18 19:42 142-28-909/25/18 14:424.3 1.6 1
2,2-Dichloropropane ND ug/kg 09/25/18 19:42 594-20-709/25/18 14:424.3 1.5 1
1,1-Dichloropropene ND ug/kg 09/25/18 19:42 563-58-609/25/18 14:424.3 1.3 1
cis-1,3-Dichloropropene ND ug/kg 09/25/18 19:42 10061-01-509/25/18 14:424.3 1.6 1
trans-1,3-Dichloropropene ND ug/kg 09/25/18 19:42 10061-02-609/25/18 14:424.3 1.3 1
Diisopropyl ether ND ug/kg 09/25/18 19:42 108-20-309/25/18 14:424.3 1.5 1
Ethylbenzene ND ug/kg 09/25/18 19:42 100-41-409/25/18 14:424.3 1.6 1
Hexachloro-1,3-butadiene ND ug/kg 09/25/18 19:42 87-68-3 M109/25/18 14:424.3 1.7 1
2-Hexanone ND ug/kg 09/25/18 19:42 591-78-609/25/18 14:4243.2 3.4 1
Isopropylbenzene (Cumene)ND ug/kg 09/25/18 19:42 98-82-809/25/18 14:424.3 1.6 1
p-Isopropyltoluene ND ug/kg 09/25/18 19:42 99-87-609/25/18 14:424.3 1.5 1
Methylene Chloride ND ug/kg 09/25/18 19:42 75-09-209/25/18 14:4217.3 2.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/25/18 19:42 108-10-109/25/18 14:4243.2 3.2 1
Methyl-tert-butyl ether ND ug/kg 09/25/18 19:42 1634-04-409/25/18 14:424.3 1.3 1
Naphthalene ND ug/kg 09/25/18 19:42 91-20-309/25/18 14:424.3 1.0 1
n-Propylbenzene ND ug/kg 09/25/18 19:42 103-65-109/25/18 14:424.3 1.5 1
Styrene ND ug/kg 09/25/18 19:42 100-42-509/25/18 14:424.3 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/25/18 19:42 630-20-609/25/18 14:424.3 1.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/25/18 19:42 79-34-5 M109/25/18 14:424.3 1.6 1
Tetrachloroethene ND ug/kg 09/25/18 19:42 127-18-409/25/18 14:424.3 1.5 1
Toluene ND ug/kg 09/25/18 19:42 108-88-309/25/18 14:424.3 1.6 1
1,2,3-Trichlorobenzene ND ug/kg 09/25/18 19:42 87-61-6 M109/25/18 14:424.3 1.9 1
1,2,4-Trichlorobenzene ND ug/kg 09/25/18 19:42 120-82-1 M109/25/18 14:424.3 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Sample:ESW-SB001 (0'-1') DUP Lab ID:92400643002 Collected:09/24/18 12:15 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
1,1,1-Trichloroethane ND ug/kg 09/25/18 19:42 71-55-609/25/18 14:424.3 1.6 1
1,1,2-Trichloroethane ND ug/kg 09/25/18 19:42 79-00-509/25/18 14:424.3 1.8 1
Trichloroethene ND ug/kg 09/25/18 19:42 79-01-609/25/18 14:424.3 1.8 1
Trichlorofluoromethane ND ug/kg 09/25/18 19:42 75-69-409/25/18 14:424.3 1.9 1
1,2,3-Trichloropropane ND ug/kg 09/25/18 19:42 96-18-409/25/18 14:424.3 1.4 1
1,2,4-Trimethylbenzene ND ug/kg 09/25/18 19:42 95-63-609/25/18 14:424.3 1.7 1
1,3,5-Trimethylbenzene ND ug/kg 09/25/18 19:42 108-67-809/25/18 14:424.3 1.6 1
Vinyl acetate ND ug/kg 09/25/18 19:42 108-05-4 M109/25/18 14:4243.2 7.6 1
Vinyl chloride ND ug/kg 09/25/18 19:42 75-01-409/25/18 14:428.6 1.6 1
Xylene (Total)ND ug/kg 09/25/18 19:42 1330-20-709/25/18 14:428.6 3.1 1
m&p-Xylene ND ug/kg 09/25/18 19:42 179601-23-109/25/18 14:428.6 3.1 1
o-Xylene ND ug/kg 09/25/18 19:42 95-47-609/25/18 14:424.3 1.6 1
Surrogates
Toluene-d8 (S)99 %09/25/18 19:42 2037-26-509/25/18 14:4270-130 1
4-Bromofluorobenzene (S)95 %09/25/18 19:42 460-00-409/25/18 14:4270-130 1
1,2-Dichloroethane-d4 (S)94 %09/25/18 19:42 17060-07-009/25/18 14:4270-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.7 %09/25/18 15:100.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide 0.29J mg/kg 10/02/18 16:15 57-12-509/29/18 18:450.30 0.17 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 40.1 mg/kg 10/01/18 13:13 16984-48-810/01/18 09:305.9 3.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Sample:ESW-SB001 (4'-5')Lab ID:92400643003 Collected:09/24/18 12:25 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8082A Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 09/26/18 16:36 12674-11-209/25/18 15:3542.4 19.3 1
PCB-1221 (Aroclor 1221)ND ug/kg 09/26/18 16:36 11104-28-209/25/18 15:3542.4 19.3 1
PCB-1232 (Aroclor 1232)ND ug/kg 09/26/18 16:36 11141-16-509/25/18 15:3542.4 19.3 1
PCB-1242 (Aroclor 1242)ND ug/kg 09/26/18 16:36 53469-21-909/25/18 15:3542.4 19.3 1
PCB-1248 (Aroclor 1248)ND ug/kg 09/26/18 16:36 12672-29-609/25/18 15:3542.4 19.3 1
PCB-1254 (Aroclor 1254)ND ug/kg 09/26/18 16:36 11097-69-109/25/18 15:3542.4 19.3 1
PCB-1260 (Aroclor 1260)ND ug/kg 09/26/18 16:36 11096-82-509/25/18 15:3542.4 19.3 1
Surrogates
Decachlorobiphenyl (S)94 %09/26/18 16:36 2051-24-309/25/18 15:3521-132 1
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 09/27/18 18:25 83-32-909/25/18 15:5212.6 1.9 1
Acenaphthylene ND ug/kg 09/27/18 18:25 208-96-809/25/18 15:5212.6 1.6 1
Anthracene ND ug/kg 09/27/18 18:25 120-12-709/25/18 15:5212.6 1.8 1
Benzo(a)anthracene 3.2J ug/kg 09/27/18 18:25 56-55-309/25/18 15:5212.6 0.89 1
Benzo(a)pyrene 1.9J ug/kg 09/27/18 18:25 50-32-809/25/18 15:5212.6 1.4 1
Benzo(b)fluoranthene 4.2J ug/kg 09/27/18 18:25 205-99-209/25/18 15:5212.6 0.84 1
Benzo(g,h,i)perylene ND ug/kg 09/27/18 18:25 191-24-209/25/18 15:5212.6 3.3 1
Benzo(k)fluoranthene ND ug/kg 09/27/18 18:25 207-08-909/25/18 15:5212.6 1.9 1
Chrysene 6.3J ug/kg 09/27/18 18:25 218-01-909/25/18 15:5212.6 2.3 1
Dibenz(a,h)anthracene ND ug/kg 09/27/18 18:25 53-70-309/25/18 15:5212.6 2.3 1
Fluoranthene 2.2J ug/kg 09/27/18 18:25 206-44-009/25/18 15:5212.6 1.0 1
Fluorene ND ug/kg 09/27/18 18:25 86-73-709/25/18 15:5212.6 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/kg 09/27/18 18:25 193-39-509/25/18 15:5212.6 3.5 1
1-Methylnaphthalene ND ug/kg 09/27/18 18:25 90-12-009/25/18 15:5212.6 1.5 1
2-Methylnaphthalene 1.9J ug/kg 09/27/18 18:25 91-57-609/25/18 15:5212.6 1.4 1
Naphthalene ND ug/kg 09/27/18 18:25 91-20-309/25/18 15:5212.6 2.9 1
Phenanthrene ND ug/kg 09/27/18 18:25 85-01-809/25/18 15:5212.6 1.9 1
Pyrene 2.5J ug/kg 09/27/18 18:25 129-00-009/25/18 15:5212.6 2.3 1
Surrogates
Nitrobenzene-d5 (S)81 %09/27/18 18:25 4165-60-009/25/18 15:5210-128 1
2-Fluorobiphenyl (S)76 %09/27/18 18:25 321-60-809/25/18 15:5210-110 1
Terphenyl-d14 (S)72 %09/27/18 18:25 1718-51-009/25/18 15:5239-119 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone ND ug/kg 09/25/18 20:22 67-64-109/25/18 14:4292.8 9.3 1
Benzene ND ug/kg 09/25/18 20:22 71-43-209/25/18 14:424.6 1.5 1
Bromobenzene ND ug/kg 09/25/18 20:22 108-86-109/25/18 14:424.6 1.9 1
Bromochloromethane ND ug/kg 09/25/18 20:22 74-97-509/25/18 14:424.6 1.6 1
Bromodichloromethane ND ug/kg 09/25/18 20:22 75-27-409/25/18 14:424.6 1.8 1
Bromoform ND ug/kg 09/25/18 20:22 75-25-209/25/18 14:424.6 2.1 1
Bromomethane ND ug/kg 09/25/18 20:22 74-83-909/25/18 14:429.3 2.3 1
2-Butanone (MEK)ND ug/kg 09/25/18 20:22 78-93-309/25/18 14:4292.8 2.7 1
n-Butylbenzene ND ug/kg 09/25/18 20:22 104-51-809/25/18 14:424.6 1.7 1
sec-Butylbenzene ND ug/kg 09/25/18 20:22 135-98-809/25/18 14:424.6 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Sample:ESW-SB001 (4'-5')Lab ID:92400643003 Collected:09/24/18 12:25 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
tert-Butylbenzene ND ug/kg 09/25/18 20:22 98-06-609/25/18 14:424.6 1.9 1
Carbon tetrachloride ND ug/kg 09/25/18 20:22 56-23-509/25/18 14:424.6 2.4 1
Chlorobenzene ND ug/kg 09/25/18 20:22 108-90-709/25/18 14:424.6 1.8 1
Chloroethane ND ug/kg 09/25/18 20:22 75-00-309/25/18 14:429.3 2.2 1
Chloroform ND ug/kg 09/25/18 20:22 67-66-309/25/18 14:424.6 1.5 1
Chloromethane ND ug/kg 09/25/18 20:22 74-87-309/25/18 14:429.3 2.2 1
2-Chlorotoluene ND ug/kg 09/25/18 20:22 95-49-809/25/18 14:424.6 1.6 1
4-Chlorotoluene ND ug/kg 09/25/18 20:22 106-43-409/25/18 14:424.6 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/25/18 20:22 96-12-809/25/18 14:424.6 3.3 1
Dibromochloromethane ND ug/kg 09/25/18 20:22 124-48-109/25/18 14:424.6 1.7 1
1,2-Dibromoethane (EDB)ND ug/kg 09/25/18 20:22 106-93-409/25/18 14:424.6 1.7 1
Dibromomethane ND ug/kg 09/25/18 20:22 74-95-309/25/18 14:424.6 2.3 1
1,2-Dichlorobenzene ND ug/kg 09/25/18 20:22 95-50-109/25/18 14:424.6 1.8 1
1,3-Dichlorobenzene ND ug/kg 09/25/18 20:22 541-73-109/25/18 14:424.6 1.9 1
1,4-Dichlorobenzene ND ug/kg 09/25/18 20:22 106-46-709/25/18 14:424.6 1.6 1
Dichlorodifluoromethane ND ug/kg 09/25/18 20:22 75-71-809/25/18 14:429.3 3.3 1
1,1-Dichloroethane ND ug/kg 09/25/18 20:22 75-34-309/25/18 14:424.6 1.4 1
1,2-Dichloroethane ND ug/kg 09/25/18 20:22 107-06-209/25/18 14:424.6 2.0 1
1,1-Dichloroethene ND ug/kg 09/25/18 20:22 75-35-409/25/18 14:424.6 1.7 1
cis-1,2-Dichloroethene ND ug/kg 09/25/18 20:22 156-59-209/25/18 14:424.6 1.3 1
trans-1,2-Dichloroethene ND ug/kg 09/25/18 20:22 156-60-509/25/18 14:424.6 1.8 1
1,2-Dichloropropane ND ug/kg 09/25/18 20:22 78-87-509/25/18 14:424.6 1.6 1
1,3-Dichloropropane ND ug/kg 09/25/18 20:22 142-28-909/25/18 14:424.6 1.8 1
2,2-Dichloropropane ND ug/kg 09/25/18 20:22 594-20-709/25/18 14:424.6 1.6 1
1,1-Dichloropropene ND ug/kg 09/25/18 20:22 563-58-609/25/18 14:424.6 1.4 1
cis-1,3-Dichloropropene ND ug/kg 09/25/18 20:22 10061-01-509/25/18 14:424.6 1.7 1
trans-1,3-Dichloropropene ND ug/kg 09/25/18 20:22 10061-02-609/25/18 14:424.6 1.4 1
Diisopropyl ether ND ug/kg 09/25/18 20:22 108-20-309/25/18 14:424.6 1.6 1
Ethylbenzene ND ug/kg 09/25/18 20:22 100-41-409/25/18 14:424.6 1.7 1
Hexachloro-1,3-butadiene ND ug/kg 09/25/18 20:22 87-68-309/25/18 14:424.6 1.9 1
2-Hexanone ND ug/kg 09/25/18 20:22 591-78-609/25/18 14:4246.4 3.6 1
Isopropylbenzene (Cumene)ND ug/kg 09/25/18 20:22 98-82-809/25/18 14:424.6 1.8 1
p-Isopropyltoluene ND ug/kg 09/25/18 20:22 99-87-609/25/18 14:424.6 1.6 1
Methylene Chloride 3.7J ug/kg 09/25/18 20:22 75-09-209/25/18 14:4218.6 2.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/25/18 20:22 108-10-109/25/18 14:4246.4 3.4 1
Methyl-tert-butyl ether ND ug/kg 09/25/18 20:22 1634-04-409/25/18 14:424.6 1.4 1
Naphthalene ND ug/kg 09/25/18 20:22 91-20-309/25/18 14:424.6 1.1 1
n-Propylbenzene ND ug/kg 09/25/18 20:22 103-65-109/25/18 14:424.6 1.6 1
Styrene ND ug/kg 09/25/18 20:22 100-42-509/25/18 14:424.6 1.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/25/18 20:22 630-20-609/25/18 14:424.6 1.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/25/18 20:22 79-34-509/25/18 14:424.6 1.8 1
Tetrachloroethene ND ug/kg 09/25/18 20:22 127-18-409/25/18 14:424.6 1.6 1
Toluene ND ug/kg 09/25/18 20:22 108-88-309/25/18 14:424.6 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 09/25/18 20:22 87-61-609/25/18 14:424.6 2.0 1
1,2,4-Trichlorobenzene ND ug/kg 09/25/18 20:22 120-82-109/25/18 14:424.6 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Sample:ESW-SB001 (4'-5')Lab ID:92400643003 Collected:09/24/18 12:25 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
1,1,1-Trichloroethane ND ug/kg 09/25/18 20:22 71-55-609/25/18 14:424.6 1.7 1
1,1,2-Trichloroethane ND ug/kg 09/25/18 20:22 79-00-509/25/18 14:424.6 1.9 1
Trichloroethene ND ug/kg 09/25/18 20:22 79-01-609/25/18 14:424.6 1.9 1
Trichlorofluoromethane ND ug/kg 09/25/18 20:22 75-69-409/25/18 14:424.6 2.0 1
1,2,3-Trichloropropane ND ug/kg 09/25/18 20:22 96-18-409/25/18 14:424.6 1.5 1
1,2,4-Trimethylbenzene ND ug/kg 09/25/18 20:22 95-63-609/25/18 14:424.6 1.9 1
1,3,5-Trimethylbenzene ND ug/kg 09/25/18 20:22 108-67-809/25/18 14:424.6 1.7 1
Vinyl acetate ND ug/kg 09/25/18 20:22 108-05-409/25/18 14:4246.4 8.2 1
Vinyl chloride ND ug/kg 09/25/18 20:22 75-01-409/25/18 14:429.3 1.7 1
Xylene (Total)ND ug/kg 09/25/18 20:22 1330-20-709/25/18 14:429.3 3.3 1
m&p-Xylene ND ug/kg 09/25/18 20:22 179601-23-109/25/18 14:429.3 3.3 1
o-Xylene ND ug/kg 09/25/18 20:22 95-47-609/25/18 14:424.6 1.8 1
Surrogates
Toluene-d8 (S)98 %09/25/18 20:22 2037-26-509/25/18 14:4270-130 1
4-Bromofluorobenzene (S)96 %09/25/18 20:22 460-00-409/25/18 14:4270-130 1
1,2-Dichloroethane-d4 (S)89 %09/25/18 20:22 17060-07-009/25/18 14:4270-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 21.4 %09/25/18 15:100.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/02/18 16:19 57-12-509/29/18 18:450.31 0.17 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride ND mg/kg 10/01/18 13:36 16984-48-810/01/18 09:306.4 3.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Sample:ESW-TB001 Lab ID:92400643004 Collected:09/24/18 00:00 Received:09/25/18 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B8260 MSV
Acetone ND ug/L 10/02/18 14:40 67-64-125.0 10.0 1
Benzene ND ug/L 10/02/18 14:40 71-43-25.0 1.7 1
Bromobenzene ND ug/L 10/02/18 14:40 108-86-15.0 1.5 1
Bromochloromethane ND ug/L 10/02/18 14:40 74-97-55.0 2.2 1
Bromodichloromethane ND ug/L 10/02/18 14:40 75-27-45.0 1.7 1
Bromoform ND ug/L 10/02/18 14:40 75-25-25.0 1.5 1
Bromomethane ND ug/L 10/02/18 14:40 74-83-910.0 2.5 1
2-Butanone (MEK)ND ug/L 10/02/18 14:40 78-93-310.0 4.9 1
tert-Butyl Alcohol ND ug/L 10/02/18 14:40 75-65-010057.7 1
n-Butylbenzene ND ug/L 10/02/18 14:40 104-51-85.0 1.9 1
sec-Butylbenzene ND ug/L 10/02/18 14:40 135-98-85.0 1.7 1
tert-Butylbenzene ND ug/L 10/02/18 14:40 98-06-65.0 1.6 1
Carbon tetrachloride ND ug/L 10/02/18 14:40 56-23-55.0 1.9 1
Chlorobenzene ND ug/L 10/02/18 14:40 108-90-75.0 1.7 1
Chloroethane ND ug/L 10/02/18 14:40 75-00-310.0 1.6 1
Chloroform ND ug/L 10/02/18 14:40 67-66-35.0 1.9 1
Chloromethane ND ug/L 10/02/18 14:40 74-87-35.0 1.5 1
2-Chlorotoluene ND ug/L 10/02/18 14:40 95-49-85.0 1.5 1
4-Chlorotoluene ND ug/L 10/02/18 14:40 106-43-45.0 1.6 1
1,2-Dibromo-3-chloropropane ND ug/L 10/02/18 14:40 96-12-82.0 1.7 1
Dibromochloromethane ND ug/L 10/02/18 14:40 124-48-15.0 1.8 1
1,2-Dibromoethane (EDB)ND ug/L 10/02/18 14:40 106-93-45.0 1.7 1
Dibromomethane ND ug/L 10/02/18 14:40 74-95-35.0 2.0 1
1,2-Dichlorobenzene ND ug/L 10/02/18 14:40 95-50-15.0 1.5 1
1,3-Dichlorobenzene ND ug/L 10/02/18 14:40 541-73-15.0 1.5 1
1,4-Dichlorobenzene ND ug/L 10/02/18 14:40 106-46-75.0 1.5 1
Dichlorodifluoromethane ND ug/L 10/02/18 14:40 75-71-85.0 1.6 1
1,1-Dichloroethane ND ug/L 10/02/18 14:40 75-34-35.0 1.8 1
1,2-Dichloroethane ND ug/L 10/02/18 14:40 107-06-25.0 1.8 1
1,2-Dichloroethene (Total)ND ug/L 10/02/18 14:40 540-59-05.0 4.4 1
1,1-Dichloroethene ND ug/L 10/02/18 14:40 75-35-45.0 1.9 1
cis-1,2-Dichloroethene ND ug/L 10/02/18 14:40 156-59-25.0 1.8 1
trans-1,2-Dichloroethene ND ug/L 10/02/18 14:40 156-60-55.0 1.8 1
1,2-Dichloropropane ND ug/L 10/02/18 14:40 78-87-55.0 1.7 1
1,3-Dichloropropane ND ug/L 10/02/18 14:40 142-28-95.0 1.7 1
2,2-Dichloropropane ND ug/L 10/02/18 14:40 594-20-75.0 1.6 1
1,1-Dichloropropene ND ug/L 10/02/18 14:40 563-58-65.0 1.7 1
cis-1,3-Dichloropropene ND ug/L 10/02/18 14:40 10061-01-55.0 1.6 1
trans-1,3-Dichloropropene ND ug/L 10/02/18 14:40 10061-02-65.0 1.6 1
Diisopropyl ether ND ug/L 10/02/18 14:40 108-20-35.0 1.7 1
Ethylbenzene ND ug/L 10/02/18 14:40 100-41-45.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 10/02/18 14:40 87-68-35.0 1.8 1
2-Hexanone ND ug/L 10/02/18 14:40 591-78-610.0 3.8 1
Isopropylbenzene (Cumene)ND ug/L 10/02/18 14:40 98-82-85.0 1.6 1
p-Isopropyltoluene ND ug/L 10/02/18 14:40 99-87-65.0 1.6 1
Methylene Chloride ND ug/L 10/02/18 14:40 75-09-25.0 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Sample:ESW-TB001 Lab ID:92400643004 Collected:09/24/18 00:00 Received:09/25/18 07:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B8260 MSV
4-Methyl-2-pentanone (MIBK)ND ug/L 10/02/18 14:40 108-10-110.0 3.6 1
Methyl-tert-butyl ether ND ug/L 10/02/18 14:40 1634-04-45.0 1.7 1
Naphthalene ND ug/L 10/02/18 14:40 91-20-35.0 2.0 1
n-Propylbenzene ND ug/L 10/02/18 14:40 103-65-15.0 1.5 1
Styrene ND ug/L 10/02/18 14:40 100-42-55.0 1.6 1
1,1,1,2-Tetrachloroethane ND ug/L 10/02/18 14:40 630-20-65.0 1.7 1
1,1,2,2-Tetrachloroethane ND ug/L 10/02/18 14:40 79-34-55.0 1.5 1
Tetrachloroethene ND ug/L 10/02/18 14:40 127-18-45.0 1.8 1
Toluene ND ug/L 10/02/18 14:40 108-88-35.0 1.6 1
1,2,3-Trichlorobenzene ND ug/L 10/02/18 14:40 87-61-65.0 2.0 1
1,2,4-Trichlorobenzene ND ug/L 10/02/18 14:40 120-82-15.0 1.7 1
1,1,1-Trichloroethane ND ug/L 10/02/18 14:40 71-55-65.0 1.9 1
1,1,2-Trichloroethane ND ug/L 10/02/18 14:40 79-00-55.0 1.7 1
Trichloroethene ND ug/L 10/02/18 14:40 79-01-65.0 1.8 1
Trichlorofluoromethane ND ug/L 10/02/18 14:40 75-69-410.0 1.7 1
1,2,3-Trichloropropane ND ug/L 10/02/18 14:40 96-18-45.0 1.5 1
1,2,4-Trimethylbenzene ND ug/L 10/02/18 14:40 95-63-65.0 1.5 1
1,3,5-Trimethylbenzene ND ug/L 10/02/18 14:40 108-67-85.0 1.3 1
Vinyl acetate ND ug/L 10/02/18 14:40 108-05-410.0 2.3 1
Vinyl chloride ND ug/L 10/02/18 14:40 75-01-45.0 1.5 1
m&p-Xylene ND ug/L 10/02/18 14:40 179601-23-110.0 3.1 1
o-Xylene ND ug/L 10/02/18 14:40 95-47-65.0 1.6 1
Surrogates
4-Bromofluorobenzene (S)97 %10/02/18 14:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %10/02/18 14:40 17060-07-070-130 1
Toluene-d8 (S)104 %10/02/18 14:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
433825
EPA 8260B
EPA 8260B
8260 MSV
Associated Lab Samples:92400643004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2389677
Associated Lab Samples:92400643004
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 10/02/18 06:161.7
1,1,1-Trichloroethane ug/L ND 5.0 10/02/18 06:161.9
1,1,2,2-Tetrachloroethane ug/L ND 5.0 10/02/18 06:161.5
1,1,2-Trichloroethane ug/L ND 5.0 10/02/18 06:161.7
1,1-Dichloroethane ug/L ND 5.0 10/02/18 06:161.8
1,1-Dichloroethene ug/L ND 5.0 10/02/18 06:161.9
1,1-Dichloropropene ug/L ND 5.0 10/02/18 06:161.7
1,2,3-Trichlorobenzene ug/L ND 5.0 10/02/18 06:162.0
1,2,3-Trichloropropane ug/L ND 5.0 10/02/18 06:161.5
1,2,4-Trichlorobenzene ug/L ND 5.0 10/02/18 06:161.7
1,2,4-Trimethylbenzene ug/L ND 5.0 10/02/18 06:161.5
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/02/18 06:161.7
1,2-Dibromoethane (EDB)ug/L ND 5.0 10/02/18 06:161.7
1,2-Dichlorobenzene ug/L ND 5.0 10/02/18 06:161.5
1,2-Dichloroethane ug/L ND 5.0 10/02/18 06:161.8
1,2-Dichloroethene (Total)ug/L ND 5.0 10/02/18 06:164.4
1,2-Dichloropropane ug/L ND 5.0 10/02/18 06:161.7
1,3,5-Trimethylbenzene ug/L ND 5.0 10/02/18 06:161.3
1,3-Dichlorobenzene ug/L ND 5.0 10/02/18 06:161.5
1,3-Dichloropropane ug/L ND 5.0 10/02/18 06:161.7
1,4-Dichlorobenzene ug/L ND 5.0 10/02/18 06:161.5
2,2-Dichloropropane ug/L ND 5.0 10/02/18 06:161.6
2-Butanone (MEK)ug/L ND 10.0 10/02/18 06:164.9
2-Chlorotoluene ug/L ND 5.0 10/02/18 06:161.5
2-Hexanone ug/L ND 10.0 10/02/18 06:163.8
4-Chlorotoluene ug/L ND 5.0 10/02/18 06:161.6
4-Methyl-2-pentanone (MIBK)ug/L ND 10.0 10/02/18 06:163.6
Acetone ug/L ND 25.0 10/02/18 06:1610.0
Benzene ug/L ND 5.0 10/02/18 06:161.7
Bromobenzene ug/L ND 5.0 10/02/18 06:161.5
Bromochloromethane ug/L ND 5.0 10/02/18 06:162.2
Bromodichloromethane ug/L ND 5.0 10/02/18 06:161.7
Bromoform ug/L ND 5.0 10/02/18 06:161.5
Bromomethane ug/L ND 10.0 10/02/18 06:162.5
Carbon tetrachloride ug/L ND 5.0 10/02/18 06:161.9
Chlorobenzene ug/L ND 5.0 10/02/18 06:161.7
Chloroethane ug/L ND 10.0 10/02/18 06:161.6
Chloroform ug/L ND 5.0 10/02/18 06:161.9
Chloromethane ug/L ND 5.0 10/02/18 06:161.5
cis-1,2-Dichloroethene ug/L ND 5.0 10/02/18 06:161.8
cis-1,3-Dichloropropene ug/L ND 5.0 10/02/18 06:161.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2389677
Associated Lab Samples:92400643004
Matrix:Water
AnalyzedMDL
Dibromochloromethane ug/L ND 5.0 10/02/18 06:161.8
Dibromomethane ug/L ND 5.0 10/02/18 06:162.0
Dichlorodifluoromethane ug/L ND 5.0 10/02/18 06:161.6
Diisopropyl ether ug/L ND 5.0 10/02/18 06:161.7
Ethylbenzene ug/L ND 5.0 10/02/18 06:161.6
Hexachloro-1,3-butadiene ug/L 3.8J 5.0 10/02/18 06:161.8
Isopropylbenzene (Cumene)ug/L ND 5.0 10/02/18 06:161.6
m&p-Xylene ug/L ND 10.0 10/02/18 06:163.1
Methyl-tert-butyl ether ug/L ND 5.0 10/02/18 06:161.7
Methylene Chloride ug/L ND 5.0 10/02/18 06:161.9
n-Butylbenzene ug/L ND 5.0 10/02/18 06:161.9
n-Propylbenzene ug/L ND 5.0 10/02/18 06:161.5
Naphthalene ug/L ND 5.0 10/02/18 06:162.0
o-Xylene ug/L ND 5.0 10/02/18 06:161.6
p-Isopropyltoluene ug/L ND 5.0 10/02/18 06:161.6
sec-Butylbenzene ug/L ND 5.0 10/02/18 06:161.7
Styrene ug/L ND 5.0 10/02/18 06:161.6
tert-Butyl Alcohol ug/L ND 100 10/02/18 06:1657.7
tert-Butylbenzene ug/L ND 5.0 10/02/18 06:161.6
Tetrachloroethene ug/L ND 5.0 10/02/18 06:161.8
Toluene ug/L ND 5.0 10/02/18 06:161.6
trans-1,2-Dichloroethene ug/L ND 5.0 10/02/18 06:161.8
trans-1,3-Dichloropropene ug/L ND 5.0 10/02/18 06:161.6
Trichloroethene ug/L ND 5.0 10/02/18 06:161.8
Trichlorofluoromethane ug/L ND 10.0 10/02/18 06:161.7
Vinyl acetate ug/L ND 10.0 10/02/18 06:162.3
Vinyl chloride ug/L ND 5.0 10/02/18 06:161.5
1,2-Dichloroethane-d4 (S)%99 70-130 10/02/18 06:16
4-Bromofluorobenzene (S)%97 70-130 10/02/18 06:16
Toluene-d8 (S)%104 70-130 10/02/18 06:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2389678LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.050 96 80-125
1,1,1-Trichloroethane ug/L 47.450 95 71-129
1,1,2,2-Tetrachloroethane ug/L 49.050 98 79-124
1,1,2-Trichloroethane ug/L 48.550 97 85-125
1,1-Dichloroethane ug/L 50.050 100 73-126
1,1-Dichloroethene ug/L 48.750 97 66-135
1,1-Dichloropropene ug/L 49.050 98 74-135
1,2,3-Trichlorobenzene ug/L 54.150 108 73-135
1,2,3-Trichloropropane ug/L 52.150 104 75-130
1,2,4-Trichlorobenzene ug/L 48.750 97 75-134
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2389678LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/L 49.150 98 79-125
1,2-Dibromo-3-chloropropane ug/L 45.750 91 71-133
1,2-Dibromoethane (EDB)ug/L 49.550 99 83-124
1,2-Dichlorobenzene ug/L 53.850 108 80-133
1,2-Dichloroethane ug/L 48.350 97 67-128
1,2-Dichloroethene (Total)ug/L 98.6
1,2-Dichloropropane ug/L 54.550 109 75-132
1,3,5-Trimethylbenzene ug/L 48.150 96 79-123
1,3-Dichlorobenzene ug/L 52.150 104 77-130
1,3-Dichloropropane ug/L 51.050 102 76-131
1,4-Dichlorobenzene ug/L 52.150 104 78-130
2,2-Dichloropropane ug/L 44.550 89 40-160
2-Butanone (MEK)ug/L 92.5100 93 61-144
2-Chlorotoluene ug/L 49.150 98 74-132
2-Hexanone ug/L 96.9100 97 68-143
4-Chlorotoluene ug/L 54.150 108 76-133
4-Methyl-2-pentanone (MIBK)ug/L 93.0100 93 72-135
Acetone ug/L 93.1100 93 48-146
Benzene ug/L 53.650 107 80-125
Bromobenzene ug/L 53.150 106 75-125
Bromochloromethane ug/L 47.750 95 71-125
Bromodichloromethane ug/L 51.250 102 78-124
Bromoform ug/L 41.350 83 71-128
Bromomethane ug/L 32.950 66 40-160
Carbon tetrachloride ug/L 46.850 94 69-131
Chlorobenzene ug/L 53.750 107 81-122
Chloroethane ug/L 38.550 77 39-148
Chloroform ug/L 45.250 90 73-127
Chloromethane ug/L 35.150 70 44-146
cis-1,2-Dichloroethene ug/L 50.750 101 74-124
cis-1,3-Dichloropropene ug/L 47.450 95 72-132
Dibromochloromethane ug/L 46.350 93 78-125
Dibromomethane ug/L 52.950 106 82-120
Dichlorodifluoromethane ug/L 34.650 69 34-157
Diisopropyl ether ug/L 44.850 90 69-135
Ethylbenzene ug/L 52.250 104 79-121
Hexachloro-1,3-butadiene ug/L 49.250 98 72-131
Isopropylbenzene (Cumene)ug/L 51.250 102 81-132
m&p-Xylene ug/L 110100 110 81-124
Methyl-tert-butyl ether ug/L 49.350 99 74-131
Methylene Chloride ug/L 46.450 93 64-133
n-Butylbenzene ug/L 47.750 95 78-127
n-Propylbenzene ug/L 50.450 101 78-130
Naphthalene ug/L 47.950 96 73-133
o-Xylene ug/L 56.450 113 79-131
p-Isopropyltoluene ug/L 47.850 96 80-131
sec-Butylbenzene ug/L 50.150 100 80-133
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2389678LABORATORY CONTROL SAMPLE:
LCSSpike
Styrene ug/L 48.850 98 84-126
tert-Butyl Alcohol ug/L 434500 87 36-136
tert-Butylbenzene ug/L 48.550 97 77-133
Tetrachloroethene ug/L 51.250 102 78-122
Toluene ug/L 50.050 100 80-121
trans-1,2-Dichloroethene ug/L 47.950 96 71-127
trans-1,3-Dichloropropene ug/L 47.350 95 69-141
Trichloroethene ug/L 49.850 100 78-122
Trichlorofluoromethane ug/L 37.250 74 53-137
Vinyl acetate ug/L 99.7100 100 40-160
Vinyl chloride ug/L 44.250 88 58-137
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2389679MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92400992001
2389680
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 200 97 70-130103 6 30200ND194205
1,1,1-Trichloroethane ug/L 200 105 70-130111 5 30200ND210222
1,1,2,2-Tetrachloroethane ug/L 200 101 70-130105 3 30200ND203209
1,1,2-Trichloroethane ug/L 200 99 70-130109 10 30200ND197217
1,1-Dichloroethane ug/L 200 104 70-130113 8 30200ND208225
1,1-Dichloroethene ug/L 200 99 65-160110 11 30200ND198221
1,1-Dichloropropene ug/L 200 106 70-130112 5 30200ND212223
1,2,3-Trichlorobenzene ug/L 200 101 70-130115 13 30200ND203231
1,2,3-Trichloropropane ug/L 200 107 70-130105 1 30200ND213211
1,2,4-Trichlorobenzene ug/L 200 99 70-130113 13 30200ND199227
1,2,4-Trimethylbenzene ug/L 200 103 70-130113 9 30200ND206225
1,2-Dibromo-3-
chloropropane ug/L 200 92 70-13098 6 30200ND185196
1,2-Dibromoethane (EDB)ug/L 200 98 60-139104 6 30200ND196208
1,2-Dichlorobenzene ug/L 200 104 70-130114 9 30200ND208228
1,2-Dichloroethane ug/L 200 97 70-130105 9 30200ND193211
1,2-Dichloroethene (Total)ug/L 7 30ND402432
1,2-Dichloropropane ug/L 200 107 70-130119 11 30200ND213239
1,3,5-Trimethylbenzene ug/L 200 104 70-130114 9 30200ND208227
1,3-Dichlorobenzene ug/L 200 102 70-130112 9 30200ND204224
1,3-Dichloropropane ug/L 200 103 70-130109 6 30200ND206218
1,4-Dichlorobenzene ug/L 200 102 70-130112 9 30200ND204224
2,2-Dichloropropane ug/L 200 96 70-130101 6 30200ND191203
2-Butanone (MEK)ug/L 400 86 70-13093 6 30400102445474
2-Chlorotoluene ug/L 200 104 70-130114 9 30200ND208228
2-Hexanone ug/L 400 102 70-130109 6 30400ND409437
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2389679MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92400992001
2389680
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
4-Chlorotoluene ug/L 200 106 70-130117 10 30200ND212234
4-Methyl-2-pentanone
(MIBK)ug/L 400 83 70-13088 5 30400ND410432
Acetone ug/L M1400-30 70-130-18 6 30400982860911
Benzene ug/L 200 108 58-162118 10 30200ND215237
Bromobenzene ug/L 200 102 70-130113 10 30200ND204226
Bromochloromethane ug/L 200 95 70-130103 8 30200ND190205
Bromodichloromethane ug/L 200 98 70-130109 10 30200ND197217
Bromoform ug/L 200 84 70-13088 5 30200ND168177
Bromomethane ug/L 200 85 70-13093 9 30200ND169186
Carbon tetrachloride ug/L 200 103 70-130111 8 30200ND206222
Chlorobenzene ug/L 200 106 70-138113 7 30200ND211226
Chloroethane ug/L 200 80 70-13092 14 30200ND159184
Chloroform ug/L 200 97 70-130104 6 30200ND195208
Chloromethane ug/L 200 77 70-13084 8 30200ND154168
cis-1,2-Dichloroethene ug/L 200 102 70-130108 7 30200ND203217
cis-1,3-Dichloropropene ug/L 200 95 70-130103 8 30200ND191206
Dibromochloromethane ug/L 200 93 70-13099 7 30200ND186199
Dibromomethane ug/L 200 103 70-130113 9 30200ND206226
Dichlorodifluoromethane ug/L 200 73 70-13078 7 30200ND146156
Diisopropyl ether ug/L 200 95 70-13097 2 30200ND189193
Ethylbenzene ug/L 200 106 22-189115 9 30200ND212231
Hexachloro-1,3-butadiene ug/L 200 107 70-130119 11 30200ND215239
Isopropylbenzene (Cumene)ug/L 200 109 70-130120 10 30200ND217240
m&p-Xylene ug/L 400 109 32-193119 9 30400ND438477
Methyl-tert-butyl ether ug/L 200 95 37-169104 9 30200ND189208
Methylene Chloride ug/L 200 106 70-130110 4 30200ND211220
n-Butylbenzene ug/L 200 103 70-130114 10 30200ND207229
n-Propylbenzene ug/L 200 107 70-130117 9 30200ND213234
Naphthalene ug/L 200 96 19-212104 9 30200ND191209
o-Xylene ug/L 200 109 70-135119 9 30200ND217238
p-Isopropyltoluene ug/L 200 104 70-130114 9 30200ND208228
sec-Butylbenzene ug/L 200 108 70-130120 11 30200ND216240
Styrene ug/L 200 102 70-130109 7 30200ND204219
tert-Butyl Alcohol ug/L 2000 116 70-130124 7 302000ND23102480
tert-Butylbenzene ug/L 200 91 70-13099 8 30200ND183198
Tetrachloroethene ug/L 200 103 70-130112 8 30200ND207224
Toluene ug/L 200 100 65-152108 7 30200ND232248
trans-1,2-Dichloroethene ug/L 200 99 70-130108 8 30200ND199215
trans-1,3-Dichloropropene ug/L 200 96 70-130102 6 30200ND193205
Trichloroethene ug/L 200 106 70-142116 9 30200ND212231
Trichlorofluoromethane ug/L 200 89 70-13095 6 30200ND179190
Vinyl acetate ug/L 400 106 70-130112 6 30400ND423450
Vinyl chloride ug/L 200 91 70-130100 9 30200ND182200
1,2-Dichloroethane-d4 (S)%92 70-13092
4-Bromofluorobenzene (S)%100 70-130102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2389679MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92400992001
2389680
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Toluene-d8 (S)%97 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
432572
EPA 5035A
EPA 8260B
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92400643001, 92400643002, 92400643003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2384169
Associated Lab Samples:92400643001, 92400643002, 92400643003
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.5 09/25/18 15:322.3
1,1,1-Trichloroethane ug/kg ND 5.5 09/25/18 15:322.0
1,1,2,2-Tetrachloroethane ug/kg ND 5.5 09/25/18 15:322.1
1,1,2-Trichloroethane ug/kg ND 5.5 09/25/18 15:322.3
1,1-Dichloroethane ug/kg ND 5.5 09/25/18 15:321.6
1,1-Dichloroethene ug/kg ND 5.5 09/25/18 15:322.0
1,1-Dichloropropene ug/kg ND 5.5 09/25/18 15:321.6
1,2,3-Trichlorobenzene ug/kg ND 5.5 09/25/18 15:322.4
1,2,3-Trichloropropane ug/kg ND 5.5 09/25/18 15:321.8
1,2,4-Trichlorobenzene ug/kg ND 5.5 09/25/18 15:321.8
1,2,4-Trimethylbenzene ug/kg ND 5.5 09/25/18 15:322.2
1,2-Dibromo-3-chloropropane ug/kg ND 5.5 09/25/18 15:324.0
1,2-Dibromoethane (EDB)ug/kg ND 5.5 09/25/18 15:322.0
1,2-Dichlorobenzene ug/kg ND 5.5 09/25/18 15:322.1
1,2-Dichloroethane ug/kg ND 5.5 09/25/18 15:322.4
1,2-Dichloropropane ug/kg ND 5.5 09/25/18 15:321.9
1,3,5-Trimethylbenzene ug/kg ND 5.5 09/25/18 15:322.0
1,3-Dichlorobenzene ug/kg ND 5.5 09/25/18 15:322.2
1,3-Dichloropropane ug/kg ND 5.5 09/25/18 15:322.1
1,4-Dichlorobenzene ug/kg ND 5.5 09/25/18 15:321.9
2,2-Dichloropropane ug/kg ND 5.5 09/25/18 15:321.9
2-Butanone (MEK)ug/kg ND 110 09/25/18 15:323.2
2-Chlorotoluene ug/kg ND 5.5 09/25/18 15:321.9
2-Hexanone ug/kg ND 54.9 09/25/18 15:324.3
4-Chlorotoluene ug/kg ND 5.5 09/25/18 15:322.0
4-Methyl-2-pentanone (MIBK)ug/kg ND 54.9 09/25/18 15:324.1
Acetone ug/kg ND 110 09/25/18 15:3211.0
Benzene ug/kg ND 5.5 09/25/18 15:321.8
Bromobenzene ug/kg ND 5.5 09/25/18 15:322.2
Bromochloromethane ug/kg ND 5.5 09/25/18 15:321.9
Bromodichloromethane ug/kg ND 5.5 09/25/18 15:322.1
Bromoform ug/kg ND 5.5 09/25/18 15:322.5
Bromomethane ug/kg ND 11.0 09/25/18 15:322.7
Carbon tetrachloride ug/kg ND 5.5 09/25/18 15:322.9
Chlorobenzene ug/kg ND 5.5 09/25/18 15:322.1
Chloroethane ug/kg ND 11.0 09/25/18 15:322.6
Chloroform ug/kg ND 5.5 09/25/18 15:321.8
Chloromethane ug/kg ND 11.0 09/25/18 15:322.6
cis-1,2-Dichloroethene ug/kg ND 5.5 09/25/18 15:321.5
cis-1,3-Dichloropropene ug/kg ND 5.5 09/25/18 15:322.0
Dibromochloromethane ug/kg ND 5.5 09/25/18 15:322.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2384169
Associated Lab Samples:92400643001, 92400643002, 92400643003
Matrix:Solid
AnalyzedMDL
Dibromomethane ug/kg ND 5.5 09/25/18 15:322.7
Dichlorodifluoromethane ug/kg ND 11.0 09/25/18 15:324.0
Diisopropyl ether ug/kg ND 5.5 09/25/18 15:321.9
Ethylbenzene ug/kg ND 5.5 09/25/18 15:322.0
Hexachloro-1,3-butadiene ug/kg ND 5.5 09/25/18 15:322.2
Isopropylbenzene (Cumene)ug/kg ND 5.5 09/25/18 15:322.1
m&p-Xylene ug/kg ND 11.0 09/25/18 15:324.0
Methyl-tert-butyl ether ug/kg ND 5.5 09/25/18 15:321.6
Methylene Chloride ug/kg ND 22.0 09/25/18 15:323.3
n-Butylbenzene ug/kg ND 5.5 09/25/18 15:322.0
n-Propylbenzene ug/kg ND 5.5 09/25/18 15:321.9
Naphthalene ug/kg 1.3J 5.5 09/25/18 15:321.3
o-Xylene ug/kg ND 5.5 09/25/18 15:322.1
p-Isopropyltoluene ug/kg ND 5.5 09/25/18 15:321.9
sec-Butylbenzene ug/kg ND 5.5 09/25/18 15:321.8
Styrene ug/kg ND 5.5 09/25/18 15:322.0
tert-Butylbenzene ug/kg ND 5.5 09/25/18 15:322.2
Tetrachloroethene ug/kg ND 5.5 09/25/18 15:321.9
Toluene ug/kg ND 5.5 09/25/18 15:322.0
trans-1,2-Dichloroethene ug/kg ND 5.5 09/25/18 15:322.1
trans-1,3-Dichloropropene ug/kg ND 5.5 09/25/18 15:321.6
Trichloroethene ug/kg ND 5.5 09/25/18 15:322.3
Trichlorofluoromethane ug/kg ND 5.5 09/25/18 15:322.4
Vinyl acetate ug/kg ND 54.9 09/25/18 15:329.7
Vinyl chloride ug/kg ND 11.0 09/25/18 15:322.0
Xylene (Total)ug/kg ND 11.0 09/25/18 15:324.0
1,2-Dichloroethane-d4 (S)%95 70-132 09/25/18 15:32
4-Bromofluorobenzene (S)%97 70-130 09/25/18 15:32
Toluene-d8 (S)%99 70-130 09/25/18 15:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2384170LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 57.456.3 102 74-137
1,1,1-Trichloroethane ug/kg 55.456.3 98 67-140
1,1,2,2-Tetrachloroethane ug/kg 49.056.3 87 72-141
1,1,2-Trichloroethane ug/kg 55.856.3 99 78-138
1,1-Dichloroethane ug/kg 57.256.3 102 69-134
1,1-Dichloroethene ug/kg 65.256.3 116 67-138
1,1-Dichloropropene ug/kg 56.956.3 101 69-139
1,2,3-Trichlorobenzene ug/kg 52.756.3 94 70-146
1,2,3-Trichloropropane ug/kg 56.156.3 100 69-144
1,2,4-Trichlorobenzene ug/kg 52.756.3 94 68-148
1,2,4-Trimethylbenzene ug/kg 56.856.3 101 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2384170LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 49.756.3 88 65-140
1,2-Dibromoethane (EDB)ug/kg 56.056.3 99 77-135
1,2-Dichlorobenzene ug/kg 54.956.3 97 77-141
1,2-Dichloroethane ug/kg 56.956.3 101 65-137
1,2-Dichloropropane ug/kg 58.856.3 104 72-136
1,3,5-Trimethylbenzene ug/kg 56.756.3 101 76-133
1,3-Dichlorobenzene ug/kg 53.956.3 96 74-138
1,3-Dichloropropane ug/kg 59.056.3 105 71-139
1,4-Dichlorobenzene ug/kg 53.556.3 95 76-138
2,2-Dichloropropane ug/kg 52.856.3 94 68-137
2-Butanone (MEK)ug/kg 103J113 92 58-147
2-Chlorotoluene ug/kg 56.456.3 100 73-139
2-Hexanone ug/kg 104113 92 62-145
4-Chlorotoluene ug/kg 55.556.3 99 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 107113 95 64-149
Acetone ug/kg 140113 124 53-153
Benzene ug/kg 59.456.3 106 73-135
Bromobenzene ug/kg 55.156.3 98 75-133
Bromochloromethane ug/kg 55.556.3 99 73-134
Bromodichloromethane ug/kg 57.656.3 102 71-135
Bromoform ug/kg 54.056.3 96 66-141
Bromomethane ug/kg 66.056.3 117 53-160
Carbon tetrachloride ug/kg 56.756.3 101 60-145
Chlorobenzene ug/kg 56.856.3 101 78-130
Chloroethane ug/kg 60.556.3 107 64-149
Chloroform ug/kg 54.356.3 96 70-134
Chloromethane ug/kg 53.656.3 95 52-150
cis-1,2-Dichloroethene ug/kg 61.056.3 108 70-133
cis-1,3-Dichloropropene ug/kg 56.456.3 100 68-134
Dibromochloromethane ug/kg 55.856.3 99 71-138
Dibromomethane ug/kg 56.456.3 100 74-130
Dichlorodifluoromethane ug/kg 56.256.3 100 40-160
Diisopropyl ether ug/kg 58.856.3 104 69-141
Ethylbenzene ug/kg 57.956.3 103 75-133
Hexachloro-1,3-butadiene ug/kg 54.456.3 97 68-143
Isopropylbenzene (Cumene)ug/kg 59.056.3 105 76-143
m&p-Xylene ug/kg 116113 103 75-136
Methyl-tert-butyl ether ug/kg 53.456.3 95 68-144
Methylene Chloride ug/kg 58.156.3 103 45-154
n-Butylbenzene ug/kg 57.956.3 103 72-137
n-Propylbenzene ug/kg 58.456.3 104 76-136
Naphthalene ug/kg 60.556.3 107 68-151
o-Xylene ug/kg 57.856.3 103 76-141
p-Isopropyltoluene ug/kg 57.356.3 102 76-140
sec-Butylbenzene ug/kg 58.956.3 105 79-139
Styrene ug/kg 54.956.3 98 79-137
tert-Butylbenzene ug/kg 52.656.3 93 74-143
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2384170LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 51.856.3 92 71-138
Toluene ug/kg 56.156.3 100 74-131
trans-1,2-Dichloroethene ug/kg 61.156.3 108 67-135
trans-1,3-Dichloropropene ug/kg 55.556.3 99 65-146
Trichloroethene ug/kg 63.356.3 112 67-135
Trichlorofluoromethane ug/kg 56.756.3 101 59-144
Vinyl acetate ug/kg 50.5J113 45 40-160
Vinyl chloride ug/kg 64.056.3 114 56-141
Xylene (Total)ug/kg 174169 103 76-137
1,2-Dichloroethane-d4 (S)%96 70-132
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2384172MATRIX SPIKE SAMPLE:
MSSpike
Result
92400643002
1,1,1,2-Tetrachloroethane ug/kg 16.317.3 94 70-130ND
1,1,1-Trichloroethane ug/kg 16.817.3 97 70-130ND
1,1,2,2-Tetrachloroethane ug/kg ND M117.3 0 70-130ND
1,1,2-Trichloroethane ug/kg 15.417.3 89 70-130ND
1,1-Dichloroethane ug/kg 17.117.3 99 70-130ND
1,1-Dichloroethene ug/kg 19.717.3 114 49-180ND
1,1-Dichloropropene ug/kg 15.917.3 92 70-130ND
1,2,3-Trichlorobenzene ug/kg 10.1 M117.3 58 70-130ND
1,2,3-Trichloropropane ug/kg 16.317.3 94 70-130ND
1,2,4-Trichlorobenzene ug/kg 10.0 M117.3 58 70-130ND
1,2,4-Trimethylbenzene ug/kg 16.117.3 93 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 14.317.3 82 70-130ND
1,2-Dibromoethane (EDB)ug/kg 15.017.3 87 70-130ND
1,2-Dichlorobenzene ug/kg 13.717.3 79 70-130ND
1,2-Dichloroethane ug/kg 16.617.3 96 70-130ND
1,2-Dichloropropane ug/kg 17.017.3 98 70-130ND
1,3,5-Trimethylbenzene ug/kg 16.317.3 94 70-130ND
1,3-Dichlorobenzene ug/kg 12.517.3 72 70-130ND
1,3-Dichloropropane ug/kg 16.717.3 96 70-130ND
1,4-Dichlorobenzene ug/kg 12.717.3 73 70-130ND
2,2-Dichloropropane ug/kg 15.917.3 92 70-130ND
2-Butanone (MEK)ug/kg 34.9J34.7 101 70-130ND
2-Chlorotoluene ug/kg 15.617.3 90 70-130ND
2-Hexanone ug/kg 30.7J34.7 89 70-130ND
4-Chlorotoluene ug/kg 14.117.3 82 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 32.7J34.7 94 70-130ND
Acetone ug/kg 49.9J34.7 107 70-13012.8J
Benzene ug/kg 17.117.3 99 50-166ND
Bromobenzene ug/kg 14.617.3 84 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2384172MATRIX SPIKE SAMPLE:
MSSpike
Result
92400643002
Bromochloromethane ug/kg 15.317.3 88 70-130ND
Bromodichloromethane ug/kg 16.017.3 92 70-130ND
Bromoform ug/kg 13.717.3 79 70-130ND
Bromomethane ug/kg 18.317.3 106 70-130ND
Carbon tetrachloride ug/kg 15.917.3 92 70-130ND
Chlorobenzene ug/kg 14.917.3 86 43-169ND
Chloroethane ug/kg 19.617.3 113 70-130ND
Chloroform ug/kg 16.817.3 97 70-130ND
Chloromethane ug/kg 15.117.3 87 70-130ND
cis-1,2-Dichloroethene ug/kg 16.117.3 93 70-130ND
cis-1,3-Dichloropropene ug/kg 14.217.3 82 70-130ND
Dibromochloromethane ug/kg 14.617.3 85 70-130ND
Dibromomethane ug/kg 16.017.3 92 70-130ND
Dichlorodifluoromethane ug/kg 17.717.3 102 70-130ND
Diisopropyl ether ug/kg 18.317.3 106 70-130ND
Ethylbenzene ug/kg 15.717.3 91 70-130ND
Hexachloro-1,3-butadiene ug/kg 11.9 M117.3 69 70-130ND
Isopropylbenzene (Cumene)ug/kg 16.117.3 93 70-130ND
m&p-Xylene ug/kg 31.134.7 90 70-130ND
Methyl-tert-butyl ether ug/kg 16.917.3 98 70-130ND
Methylene Chloride ug/kg 19.117.3 110 70-130ND
n-Butylbenzene ug/kg 13.917.3 80 70-130ND
n-Propylbenzene ug/kg 16.317.3 94 70-130ND
Naphthalene ug/kg 12.717.3 74 70-130ND
o-Xylene ug/kg 15.917.3 92 70-130ND
p-Isopropyltoluene ug/kg 15.717.3 90 70-130ND
sec-Butylbenzene ug/kg 16.217.3 93 70-130ND
Styrene ug/kg 13.117.3 76 70-130ND
tert-Butylbenzene ug/kg 15.617.3 90 70-130ND
Tetrachloroethene ug/kg 14.217.3 82 70-130ND
Toluene ug/kg 15.317.3 89 52-163ND
trans-1,2-Dichloroethene ug/kg 17.217.3 99 70-130ND
trans-1,3-Dichloropropene ug/kg 13.417.3 77 70-130ND
Trichloroethene ug/kg 28.217.3 163 49-167ND
Trichlorofluoromethane ug/kg 17.817.3 103 70-130ND
Vinyl acetate ug/kg ND M134.7 21 70-130ND
Vinyl chloride ug/kg 19.917.3 115 70-130ND
Xylene (Total)ug/kg 47.052 91 70-130ND
1,2-Dichloroethane-d4 (S)%94 70-132
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400643001
2384171SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg 13.9J 3012.1J
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400643001
2384171SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg 3.5J 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%92 693
4-Bromofluorobenzene (S)%90 389
Toluene-d8 (S)%98 498
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
432588
EPA 3546
EPA 8082A
8082 GCS PCB
Associated Lab Samples:92400643001, 92400643002, 92400643003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2384274
Associated Lab Samples:92400643001, 92400643002, 92400643003
Matrix:Solid
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/kg ND 33.6 09/26/18 17:3615.3
PCB-1221 (Aroclor 1221)ug/kg ND 33.6 09/26/18 17:3615.3
PCB-1232 (Aroclor 1232)ug/kg ND 33.6 09/26/18 17:3615.3
PCB-1242 (Aroclor 1242)ug/kg ND 33.6 09/26/18 17:3615.3
PCB-1248 (Aroclor 1248)ug/kg ND 33.6 09/26/18 17:3615.3
PCB-1254 (Aroclor 1254)ug/kg ND 33.6 09/26/18 17:3615.3
PCB-1260 (Aroclor 1260)ug/kg ND 33.6 09/26/18 17:3615.3
Decachlorobiphenyl (S)%104 21-132 09/26/18 17:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2384275LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2384276
PCB-1016 (Aroclor 1016)ug/kg 173169 103 31-12082136 24 30
PCB-1260 (Aroclor 1260)ug/kg 195169 116 32-120107178 9 30
Decachlorobiphenyl (S)%108 21-13298
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
432500
EPA 3546
EPA 8270D by SIM
8270 MSSV PAH by SIM
Associated Lab Samples:92400643001, 92400643002, 92400643003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2383771
Associated Lab Samples:92400643001, 92400643002, 92400643003
Matrix:Solid
AnalyzedMDL
1-Methylnaphthalene ug/kg ND 10.1 09/27/18 13:281.2
2-Methylnaphthalene ug/kg ND 10.1 09/27/18 13:281.1
Acenaphthene ug/kg ND 10.1 09/27/18 13:281.5
Acenaphthylene ug/kg ND 10.1 09/27/18 13:281.3
Anthracene ug/kg ND 10.1 09/27/18 13:281.4
Benzo(a)anthracene ug/kg 0.82J 10.1 09/27/18 13:280.72
Benzo(a)pyrene ug/kg ND 10.1 09/27/18 13:281.1
Benzo(b)fluoranthene ug/kg 0.92J 10.1 09/27/18 13:280.68
Benzo(g,h,i)perylene ug/kg ND 10.1 09/27/18 13:282.6
Benzo(k)fluoranthene ug/kg ND 10.1 09/27/18 13:281.5
Chrysene ug/kg ND 10.1 09/27/18 13:281.8
Dibenz(a,h)anthracene ug/kg ND 10.1 09/27/18 13:281.8
Fluoranthene ug/kg ND 10.1 09/27/18 13:280.84
Fluorene ug/kg ND 10.1 09/27/18 13:281.6
Indeno(1,2,3-cd)pyrene ug/kg ND 10.1 09/27/18 13:282.8
Naphthalene ug/kg ND 10.1 09/27/18 13:282.3
Phenanthrene ug/kg ND 10.1 09/27/18 13:281.5
Pyrene ug/kg ND 10.1 09/27/18 13:281.8
2-Fluorobiphenyl (S)%63 10-110 09/27/18 13:28
Nitrobenzene-d5 (S)%68 10-128 09/27/18 13:28
Terphenyl-d14 (S)%68 39-119 09/27/18 13:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2383772LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/kg 25.933.8 77 44-130
2-Methylnaphthalene ug/kg 26.433.8 78 41-134
Acenaphthene ug/kg 29.233.8 86 52-123
Acenaphthylene ug/kg 25.833.8 76 49-116
Anthracene ug/kg 29.933.8 89 41-133
Benzo(a)anthracene ug/kg 29.233.8 86 56-130
Benzo(a)pyrene ug/kg 29.133.8 86 51-136
Benzo(b)fluoranthene ug/kg 30.733.8 91 37-149
Benzo(g,h,i)perylene ug/kg 26.633.8 79 39-127
Benzo(k)fluoranthene ug/kg 31.933.8 94 45-139
Chrysene ug/kg 31.833.8 94 59-127
Dibenz(a,h)anthracene ug/kg 30.033.8 89 37-139
Fluoranthene ug/kg 31.433.8 93 53-132
Fluorene ug/kg 27.033.8 80 45-127
Indeno(1,2,3-cd)pyrene ug/kg 30.533.8 90 35-145
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2383772LABORATORY CONTROL SAMPLE:
LCSSpike
Naphthalene ug/kg 26.733.8 79 45-123
Phenanthrene ug/kg 30.633.8 91 50-125
Pyrene ug/kg 30.733.8 91 52-132
2-Fluorobiphenyl (S)%81 10-110
Nitrobenzene-d5 (S)%87 10-128
Terphenyl-d14 (S)%81 39-119
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2383773MATRIX SPIKE SAMPLE:
MSSpike
Result
92400518002
1-Methylnaphthalene ug/kg 25.638.7 51 50-150ND
2-Methylnaphthalene ug/kg 26.138.7 52 50-150ND
Acenaphthene ug/kg 21.238.7 55 50-150ND
Acenaphthylene ug/kg 18.9 M138.7 49 50-150ND
Anthracene ug/kg 18.7 M138.7 46 50-150ND
Benzo(a)anthracene ug/kg 21.8 M138.7 38 50-150ND
Benzo(a)pyrene ug/kg 19.2 M138.7 30 50-150ND
Benzo(b)fluoranthene ug/kg 24.2 M138.7 35 50-150ND
Benzo(g,h,i)perylene ug/kg 14.7 M138.7 21 50-150ND
Benzo(k)fluoranthene ug/kg 17.5 M138.7 34 50-150ND
Chrysene ug/kg 23.7 M138.7 41 50-150ND
Dibenz(a,h)anthracene ug/kg 13.7 M138.7 30 50-150ND
Fluoranthene ug/kg 29.0 M138.7 47 50-150ND
Fluorene ug/kg 18.6 M138.7 48 50-150ND
Indeno(1,2,3-cd)pyrene ug/kg 16.0 M138.7 27 50-150ND
Naphthalene ug/kg 25.938.7 55 50-150ND
Phenanthrene ug/kg 28.438.7 55 50-150ND
Pyrene ug/kg 29.7 M138.7 48 50-150ND
2-Fluorobiphenyl (S)%65 10-110
Nitrobenzene-d5 (S)%76 10-128
Terphenyl-d14 (S)%55 39-119
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400518003
2383774SAMPLE DUPLICATE:
1-Methylnaphthalene ug/kg 42.1 D6523024.8
2-Methylnaphthalene ug/kg 46.8 D6493028.3
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg 13.3 17 3015.8
Anthracene ug/kg 23.4 13 3026.6
Benzo(a)anthracene ug/kg 69.6 D64130106
Benzo(a)pyrene ug/kg 65.4 D6373094.6
Benzo(b)fluoranthene ug/kg 120 23 30151
Benzo(g,h,i)perylene ug/kg 43.6 D6343061.5
REPORT OF LABORATORY ANALYSIS
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Page 31 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400518003
2383774SAMPLE DUPLICATE:
Benzo(k)fluoranthene ug/kg 37.9 D6313051.9
Chrysene ug/kg 85.4 23 30107
Dibenz(a,h)anthracene ug/kg 14.9 29 3020.0
Fluoranthene ug/kg 127 D64330197
Fluorene ug/kg 3.2J 30ND
Indeno(1,2,3-cd)pyrene ug/kg 42.2 D6353059.9
Naphthalene ug/kg 55.7 24 3043.9
Phenanthrene ug/kg 93.6 18 30112
Pyrene ug/kg 111 D63630159
2-Fluorobiphenyl (S)%42 2454
Nitrobenzene-d5 (S)%53 758
Terphenyl-d14 (S)%45 2860
REPORT OF LABORATORY ANALYSIS
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Page 32 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
432585
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92400643001, 92400643002, 92400643003
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400332003
2384246SAMPLE DUPLICATE:
Percent Moisture %11.8 2 2511.6
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400643003
2384247SAMPLE DUPLICATE:
Percent Moisture %21.5 1 2521.4
REPORT OF LABORATORY ANALYSIS
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Page 33 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
481710
EPA 9012
EPA 9012
9012 Cyanide
Associated Lab Samples:92400643001, 92400643002, 92400643003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2607788
Associated Lab Samples:92400643001, 92400643002, 92400643003
Matrix:Solid
AnalyzedMDL
Cyanide mg/kg ND 0.24 10/02/18 16:100.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2607789LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide mg/kg 1.31.2 106 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2607790MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92400643001
2607791
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/kg M1.764 136 80-120122 8 20.776ND 1.2 1.1
REPORT OF LABORATORY ANALYSIS
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Page 34 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
481867
EPA 9056
EPA 9056
9056 IC Anions
Associated Lab Samples:92400643001, 92400643002, 92400643003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2608290
Associated Lab Samples:92400643001, 92400643002, 92400643003
Matrix:Solid
AnalyzedMDL
Fluoride mg/kg ND 5.0 10/01/18 10:292.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2608291LABORATORY CONTROL SAMPLE:
LCSSpike
Fluoride mg/kg 49.249.6 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2608293MATRIX SPIKE SAMPLE:
MSSpike
Result
92400799001
Fluoride mg/kg 54.3 M156.3 68 80-12015.8
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400799001
2608292SAMPLE DUPLICATE:
Fluoride mg/kg 16.0 2 2015.8
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
REPORT OF LABORATORY ANALYSIS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92400643
Frmr Electrical Shop/Warehouse
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92400643001 432588 432974ESW-SB001 (0'-1')EPA 3546 EPA 8082A
92400643002 432588 432974ESW-SB001 (0'-1') DUP EPA 3546 EPA 8082A
92400643003 432588 432974ESW-SB001 (4'-5')EPA 3546 EPA 8082A
92400643001 432500 432996ESW-SB001 (0'-1')EPA 3546 EPA 8270D by SIM
92400643002 432500 432996ESW-SB001 (0'-1') DUP EPA 3546 EPA 8270D by SIM
92400643003 432500 432996ESW-SB001 (4'-5')EPA 3546 EPA 8270D by SIM
92400643004 433825ESW-TB001 EPA 8260B
92400643001 432572 432586ESW-SB001 (0'-1')EPA 5035A EPA 8260B
92400643002 432572 432586ESW-SB001 (0'-1') DUP EPA 5035A EPA 8260B
92400643003 432572 432586ESW-SB001 (4'-5')EPA 5035A EPA 8260B
92400643001 432585ESW-SB001 (0'-1')ASTM D2974-87
92400643002 432585ESW-SB001 (0'-1') DUP ASTM D2974-87
92400643003 432585ESW-SB001 (4'-5')ASTM D2974-87
92400643001 481710 482312ESW-SB001 (0'-1')EPA 9012 EPA 9012
92400643002 481710 482312ESW-SB001 (0'-1') DUP EPA 9012 EPA 9012
92400643003 481710 482312ESW-SB001 (4'-5')EPA 9012 EPA 9012
92400643001 481867 481884ESW-SB001 (0'-1')EPA 9056 EPA 9056
92400643002 481867 481884ESW-SB001 (0'-1') DUP EPA 9056 EPA 9056
92400643003 481867 481884ESW-SB001 (4'-5')EPA 9056 EPA 9056
REPORT OF LABORATORY ANALYSIS
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Page 37 of 40
Page 38 of 40
Page 39 of 40
Page 40 of 40
#=CL#
November 12, 2018
LIMS USE: FR - MICHAEL WORDEN
LIMS OBJECT ID: 92400796
92400796
Project:
Pace Project No.:
RE:
Michael W. Worden
Environeering, Inc.
16100 Cairnway
Suite 320
Houston, TX 77084
Former Maintenance Shop Area
Dear Michael Worden:
Enclosed are the analytical results for sample(s) received by the laboratory on September 25, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
This revision was issued on 11/12/18 to report J-flagged results to the MDL, per client request.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 1 of 52
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 2 of 52
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Lab ID Sample ID Matrix Date Collected Date Received
92400796001 MSA-SB001 (0'-1')Solid 09/24/18 14:25 09/25/18 07:30
92400796002 MSA-SB001 (4'-5')Solid 09/24/18 14:30 09/25/18 07:30
92400796003 MSA-SB002 (0'-1')Solid 09/24/18 14:40 09/25/18 07:30
92400796004 MSA-SB002 (4'-5')Solid 09/24/18 14:45 09/25/18 07:30
92400796005 MSA-SB003 (0'-1')Solid 09/24/18 15:00 09/25/18 07:30
92400796006 MSA-SB003 (4'-5')Solid 09/24/18 15:05 09/25/18 07:30
92400796007 MSA-SB004 (0'-1')Solid 09/24/18 15:30 09/25/18 07:30
92400796008 MSA-SB004 (4'-5')Solid 09/24/18 15:35 09/25/18 07:30
REPORT OF LABORATORY ANALYSIS
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92400796001 MSA-SB001 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92400796002 MSA-SB001 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92400796003 MSA-SB002 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92400796004 MSA-SB002 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92400796005 MSA-SB003 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92400796006 MSA-SB003 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92400796007 MSA-SB004 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92400796008 MSA-SB004 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
EPA 8260B 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
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Page 4 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB001 (0'-1')Lab ID:92400796001 Collected:09/24/18 14:25 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 166 ug/kg 09/27/18 22:18 83-32-909/26/18 14:1712.0 1.8 1
Acenaphthylene 49.2 ug/kg 09/27/18 22:18 208-96-809/26/18 14:1712.0 1.6 1
Anthracene 345 ug/kg 09/27/18 22:18 120-12-709/26/18 14:1712.0 1.7 1
Benzo(a)anthracene 892 ug/kg 09/28/18 14:46 56-55-309/26/18 14:1747.8 3.4 4
Benzo(a)pyrene 929 ug/kg 09/27/18 22:18 50-32-809/26/18 14:1712.0 1.3 1
Benzo(b)fluoranthene 1190 ug/kg 09/28/18 14:46 205-99-209/26/18 14:1747.8 3.2 4
Benzo(g,h,i)perylene 539 ug/kg 09/27/18 22:18 191-24-209/26/18 14:1712.0 3.1 1
Benzo(k)fluoranthene 395 ug/kg 09/27/18 22:18 207-08-909/26/18 14:1712.0 1.8 1
Chrysene 857 ug/kg 09/28/18 14:46 218-01-909/26/18 14:1747.8 8.6 4
Dibenz(a,h)anthracene 163 ug/kg 09/27/18 22:18 53-70-309/26/18 14:1712.0 2.2 1
Fluoranthene 1670 ug/kg 09/28/18 14:46 206-44-009/26/18 14:1747.8 4.0 4
Fluorene 118 ug/kg 09/27/18 22:18 86-73-709/26/18 14:1712.0 1.9 1
Indeno(1,2,3-cd)pyrene 510 ug/kg 09/27/18 22:18 193-39-509/26/18 14:1712.0 3.3 1
1-Methylnaphthalene 118 ug/kg 09/27/18 22:18 90-12-009/26/18 14:1712.0 1.4 1
2-Methylnaphthalene 107 ug/kg 09/27/18 22:18 91-57-609/26/18 14:1712.0 1.3 1
Naphthalene 85.5 ug/kg 09/27/18 22:18 91-20-309/26/18 14:1712.0 2.8 1
Phenanthrene 1270 ug/kg 09/28/18 14:46 85-01-809/26/18 14:1747.8 7.2 4
Pyrene 1370 ug/kg 09/28/18 14:46 129-00-009/26/18 14:1747.8 8.6 4
Surrogates
Nitrobenzene-d5 (S)62 %09/27/18 22:18 4165-60-009/26/18 14:1710-128 1
2-Fluorobiphenyl (S)61 %09/27/18 22:18 321-60-809/26/18 14:1710-110 1
Terphenyl-d14 (S)80 %09/27/18 22:18 1718-51-009/26/18 14:1739-119 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone ND ug/kg 09/26/18 20:34 67-64-109/26/18 10:3813013.0 1
Benzene ND ug/kg 09/26/18 20:34 71-43-209/26/18 10:386.5 2.1 1
Bromobenzene ND ug/kg 09/26/18 20:34 108-86-109/26/18 10:386.5 2.6 1
Bromochloromethane ND ug/kg 09/26/18 20:34 74-97-509/26/18 10:386.5 2.2 1
Bromodichloromethane ND ug/kg 09/26/18 20:34 75-27-409/26/18 10:386.5 2.5 1
Bromoform ND ug/kg 09/26/18 20:34 75-25-209/26/18 10:386.5 3.0 1
Bromomethane ND ug/kg 09/26/18 20:34 74-83-909/26/18 10:3813.0 3.2 1
2-Butanone (MEK)ND ug/kg 09/26/18 20:34 78-93-309/26/18 10:381303.8 1
n-Butylbenzene ND ug/kg 09/26/18 20:34 104-51-8 M109/26/18 10:386.5 2.3 1
sec-Butylbenzene ND ug/kg 09/26/18 20:34 135-98-809/26/18 10:386.5 2.1 1
tert-Butylbenzene ND ug/kg 09/26/18 20:34 98-06-609/26/18 10:386.5 2.6 1
Carbon tetrachloride ND ug/kg 09/26/18 20:34 56-23-509/26/18 10:386.5 3.4 1
Chlorobenzene ND ug/kg 09/26/18 20:34 108-90-709/26/18 10:386.5 2.5 1
Chloroethane ND ug/kg 09/26/18 20:34 75-00-309/26/18 10:3813.0 3.1 1
Chloroform ND ug/kg 09/26/18 20:34 67-66-309/26/18 10:386.5 2.1 1
Chloromethane ND ug/kg 09/26/18 20:34 74-87-309/26/18 10:3813.0 3.1 1
2-Chlorotoluene ND ug/kg 09/26/18 20:34 95-49-809/26/18 10:386.5 2.2 1
4-Chlorotoluene ND ug/kg 09/26/18 20:34 106-43-409/26/18 10:386.5 2.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/26/18 20:34 96-12-809/26/18 10:386.5 4.7 1
Dibromochloromethane ND ug/kg 09/26/18 20:34 124-48-109/26/18 10:386.5 2.3 1
1,2-Dibromoethane (EDB)ND ug/kg 09/26/18 20:34 106-93-409/26/18 10:386.5 2.3 1
REPORT OF LABORATORY ANALYSIS
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Page 5 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB001 (0'-1')Lab ID:92400796001 Collected:09/24/18 14:25 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Dibromomethane ND ug/kg 09/26/18 20:34 74-95-309/26/18 10:386.5 3.2 1
1,2-Dichlorobenzene ND ug/kg 09/26/18 20:34 95-50-109/26/18 10:386.5 2.5 1
1,3-Dichlorobenzene ND ug/kg 09/26/18 20:34 541-73-109/26/18 10:386.5 2.6 1
1,4-Dichlorobenzene ND ug/kg 09/26/18 20:34 106-46-709/26/18 10:386.5 2.2 1
Dichlorodifluoromethane ND ug/kg 09/26/18 20:34 75-71-809/26/18 10:3813.0 4.7 1
1,1-Dichloroethane ND ug/kg 09/26/18 20:34 75-34-309/26/18 10:386.5 1.9 1
1,2-Dichloroethane ND ug/kg 09/26/18 20:34 107-06-209/26/18 10:386.5 2.9 1
1,1-Dichloroethene ND ug/kg 09/26/18 20:34 75-35-409/26/18 10:386.5 2.3 1
cis-1,2-Dichloroethene ND ug/kg 09/26/18 20:34 156-59-209/26/18 10:386.5 1.8 1
trans-1,2-Dichloroethene ND ug/kg 09/26/18 20:34 156-60-509/26/18 10:386.5 2.5 1
1,2-Dichloropropane ND ug/kg 09/26/18 20:34 78-87-509/26/18 10:386.5 2.2 1
1,3-Dichloropropane ND ug/kg 09/26/18 20:34 142-28-909/26/18 10:386.5 2.5 1
2,2-Dichloropropane ND ug/kg 09/26/18 20:34 594-20-709/26/18 10:386.5 2.2 1
1,1-Dichloropropene ND ug/kg 09/26/18 20:34 563-58-609/26/18 10:386.5 1.9 1
cis-1,3-Dichloropropene ND ug/kg 09/26/18 20:34 10061-01-509/26/18 10:386.5 2.3 1
trans-1,3-Dichloropropene ND ug/kg 09/26/18 20:34 10061-02-609/26/18 10:386.5 1.9 1
Diisopropyl ether ND ug/kg 09/26/18 20:34 108-20-309/26/18 10:386.5 2.2 1
Ethylbenzene ND ug/kg 09/26/18 20:34 100-41-409/26/18 10:386.5 2.3 1
Hexachloro-1,3-butadiene ND ug/kg 09/26/18 20:34 87-68-3 M109/26/18 10:386.5 2.6 1
2-Hexanone ND ug/kg 09/26/18 20:34 591-78-609/26/18 10:3865.0 5.1 1
Isopropylbenzene (Cumene)ND ug/kg 09/26/18 20:34 98-82-809/26/18 10:386.5 2.5 1
p-Isopropyltoluene ND ug/kg 09/26/18 20:34 99-87-609/26/18 10:386.5 2.2 1
Methylene Chloride ND ug/kg 09/26/18 20:34 75-09-2 M109/26/18 10:3826.0 3.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/26/18 20:34 108-10-109/26/18 10:3865.0 4.8 1
Methyl-tert-butyl ether ND ug/kg 09/26/18 20:34 1634-04-409/26/18 10:386.5 1.9 1
Naphthalene ND ug/kg 09/26/18 20:34 91-20-309/26/18 10:386.5 1.6 1
n-Propylbenzene ND ug/kg 09/26/18 20:34 103-65-109/26/18 10:386.5 2.2 1
Styrene ND ug/kg 09/26/18 20:34 100-42-509/26/18 10:386.5 2.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/26/18 20:34 630-20-609/26/18 10:386.5 2.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/26/18 20:34 79-34-5 M109/26/18 10:386.5 2.5 1
Tetrachloroethene ND ug/kg 09/26/18 20:34 127-18-409/26/18 10:386.5 2.2 1
Toluene ND ug/kg 09/26/18 20:34 108-88-309/26/18 10:386.5 2.3 1
1,2,3-Trichlorobenzene ND ug/kg 09/26/18 20:34 87-61-609/26/18 10:386.5 2.9 1
1,2,4-Trichlorobenzene ND ug/kg 09/26/18 20:34 120-82-1 M109/26/18 10:386.5 2.1 1
1,1,1-Trichloroethane ND ug/kg 09/26/18 20:34 71-55-609/26/18 10:386.5 2.3 1
1,1,2-Trichloroethane ND ug/kg 09/26/18 20:34 79-00-509/26/18 10:386.5 2.7 1
Trichloroethene ND ug/kg 09/26/18 20:34 79-01-6 M109/26/18 10:386.5 2.7 1
Trichlorofluoromethane ND ug/kg 09/26/18 20:34 75-69-409/26/18 10:386.5 2.9 1
1,2,3-Trichloropropane ND ug/kg 09/26/18 20:34 96-18-409/26/18 10:386.5 2.1 1
1,2,4-Trimethylbenzene ND ug/kg 09/26/18 20:34 95-63-609/26/18 10:386.5 2.6 1
1,3,5-Trimethylbenzene ND ug/kg 09/26/18 20:34 108-67-809/26/18 10:386.5 2.3 1
Vinyl acetate ND ug/kg 09/26/18 20:34 108-05-4 M109/26/18 10:3865.0 11.4 1
Vinyl chloride ND ug/kg 09/26/18 20:34 75-01-409/26/18 10:3813.0 2.3 1
Xylene (Total)ND ug/kg 09/26/18 20:34 1330-20-709/26/18 10:3813.0 4.7 1
m&p-Xylene ND ug/kg 09/26/18 20:34 179601-23-109/26/18 10:3813.0 4.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB001 (0'-1')Lab ID:92400796001 Collected:09/24/18 14:25 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
o-Xylene ND ug/kg 09/26/18 20:34 95-47-609/26/18 10:386.5 2.5 1
Surrogates
Toluene-d8 (S)104 %09/26/18 20:34 2037-26-509/26/18 10:3870-130 1
4-Bromofluorobenzene (S)93 %09/26/18 20:34 460-00-409/26/18 10:3870-130 1
1,2-Dichloroethane-d4 (S)85 %09/26/18 20:34 17060-07-009/26/18 10:3870-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.8 %09/25/18 18:040.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB001 (4'-5')Lab ID:92400796002 Collected:09/24/18 14:30 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 09/27/18 22:39 83-32-909/26/18 14:1712.1 1.8 1
Acenaphthylene ND ug/kg 09/27/18 22:39 208-96-809/26/18 14:1712.1 1.6 1
Anthracene ND ug/kg 09/27/18 22:39 120-12-709/26/18 14:1712.1 1.7 1
Benzo(a)anthracene 2.2J ug/kg 09/27/18 22:39 56-55-309/26/18 14:1712.1 0.86 1
Benzo(a)pyrene 2.0J ug/kg 09/27/18 22:39 50-32-809/26/18 14:1712.1 1.3 1
Benzo(b)fluoranthene 2.7J ug/kg 09/27/18 22:39 205-99-209/26/18 14:1712.1 0.81 1
Benzo(g,h,i)perylene ND ug/kg 09/27/18 22:39 191-24-209/26/18 14:1712.1 3.2 1
Benzo(k)fluoranthene ND ug/kg 09/27/18 22:39 207-08-909/26/18 14:1712.1 1.8 1
Chrysene ND ug/kg 09/27/18 22:39 218-01-909/26/18 14:1712.1 2.2 1
Dibenz(a,h)anthracene ND ug/kg 09/27/18 22:39 53-70-309/26/18 14:1712.1 2.2 1
Fluoranthene 4.0J ug/kg 09/27/18 22:39 206-44-009/26/18 14:1712.1 1.0 1
Fluorene ND ug/kg 09/27/18 22:39 86-73-709/26/18 14:1712.1 1.9 1
Indeno(1,2,3-cd)pyrene ND ug/kg 09/27/18 22:39 193-39-509/26/18 14:1712.1 3.4 1
1-Methylnaphthalene ND ug/kg 09/27/18 22:39 90-12-009/26/18 14:1712.1 1.5 1
2-Methylnaphthalene ND ug/kg 09/27/18 22:39 91-57-609/26/18 14:1712.1 1.3 1
Naphthalene ND ug/kg 09/27/18 22:39 91-20-309/26/18 14:1712.1 2.8 1
Phenanthrene 3.1J ug/kg 09/27/18 22:39 85-01-809/26/18 14:1712.1 1.8 1
Pyrene 3.7J ug/kg 09/27/18 22:39 129-00-009/26/18 14:1712.1 2.2 1
Surrogates
Nitrobenzene-d5 (S)68 %09/27/18 22:39 4165-60-009/26/18 14:1710-128 1
2-Fluorobiphenyl (S)67 %09/27/18 22:39 321-60-809/26/18 14:1710-110 1
Terphenyl-d14 (S)76 %09/27/18 22:39 1718-51-009/26/18 14:1739-119 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone ND ug/kg 09/26/18 21:14 67-64-109/26/18 10:3890.3 9.0 1
Benzene ND ug/kg 09/26/18 21:14 71-43-209/26/18 10:384.5 1.4 1
Bromobenzene ND ug/kg 09/26/18 21:14 108-86-109/26/18 10:384.5 1.8 1
Bromochloromethane ND ug/kg 09/26/18 21:14 74-97-509/26/18 10:384.5 1.5 1
Bromodichloromethane ND ug/kg 09/26/18 21:14 75-27-409/26/18 10:384.5 1.7 1
Bromoform ND ug/kg 09/26/18 21:14 75-25-209/26/18 10:384.5 2.1 1
Bromomethane ND ug/kg 09/26/18 21:14 74-83-909/26/18 10:389.0 2.3 1
2-Butanone (MEK)ND ug/kg 09/26/18 21:14 78-93-309/26/18 10:3890.3 2.6 1
n-Butylbenzene ND ug/kg 09/26/18 21:14 104-51-809/26/18 10:384.5 1.6 1
sec-Butylbenzene ND ug/kg 09/26/18 21:14 135-98-809/26/18 10:384.5 1.4 1
tert-Butylbenzene ND ug/kg 09/26/18 21:14 98-06-609/26/18 10:384.5 1.8 1
Carbon tetrachloride ND ug/kg 09/26/18 21:14 56-23-509/26/18 10:384.5 2.3 1
Chlorobenzene ND ug/kg 09/26/18 21:14 108-90-709/26/18 10:384.5 1.7 1
Chloroethane ND ug/kg 09/26/18 21:14 75-00-309/26/18 10:389.0 2.2 1
Chloroform ND ug/kg 09/26/18 21:14 67-66-309/26/18 10:384.5 1.4 1
Chloromethane ND ug/kg 09/26/18 21:14 74-87-309/26/18 10:389.0 2.2 1
2-Chlorotoluene ND ug/kg 09/26/18 21:14 95-49-809/26/18 10:384.5 1.5 1
4-Chlorotoluene ND ug/kg 09/26/18 21:14 106-43-409/26/18 10:384.5 1.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/26/18 21:14 96-12-809/26/18 10:384.5 3.3 1
Dibromochloromethane ND ug/kg 09/26/18 21:14 124-48-109/26/18 10:384.5 1.6 1
1,2-Dibromoethane (EDB)ND ug/kg 09/26/18 21:14 106-93-409/26/18 10:384.5 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB001 (4'-5')Lab ID:92400796002 Collected:09/24/18 14:30 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Dibromomethane ND ug/kg 09/26/18 21:14 74-95-309/26/18 10:384.5 2.3 1
1,2-Dichlorobenzene ND ug/kg 09/26/18 21:14 95-50-109/26/18 10:384.5 1.7 1
1,3-Dichlorobenzene ND ug/kg 09/26/18 21:14 541-73-109/26/18 10:384.5 1.8 1
1,4-Dichlorobenzene ND ug/kg 09/26/18 21:14 106-46-709/26/18 10:384.5 1.5 1
Dichlorodifluoromethane ND ug/kg 09/26/18 21:14 75-71-809/26/18 10:389.0 3.3 1
1,1-Dichloroethane ND ug/kg 09/26/18 21:14 75-34-309/26/18 10:384.5 1.4 1
1,2-Dichloroethane ND ug/kg 09/26/18 21:14 107-06-209/26/18 10:384.5 2.0 1
1,1-Dichloroethene ND ug/kg 09/26/18 21:14 75-35-409/26/18 10:384.5 1.6 1
cis-1,2-Dichloroethene ND ug/kg 09/26/18 21:14 156-59-209/26/18 10:384.5 1.3 1
trans-1,2-Dichloroethene ND ug/kg 09/26/18 21:14 156-60-509/26/18 10:384.5 1.7 1
1,2-Dichloropropane ND ug/kg 09/26/18 21:14 78-87-509/26/18 10:384.5 1.5 1
1,3-Dichloropropane ND ug/kg 09/26/18 21:14 142-28-909/26/18 10:384.5 1.7 1
2,2-Dichloropropane ND ug/kg 09/26/18 21:14 594-20-709/26/18 10:384.5 1.5 1
1,1-Dichloropropene ND ug/kg 09/26/18 21:14 563-58-609/26/18 10:384.5 1.4 1
cis-1,3-Dichloropropene ND ug/kg 09/26/18 21:14 10061-01-509/26/18 10:384.5 1.6 1
trans-1,3-Dichloropropene ND ug/kg 09/26/18 21:14 10061-02-609/26/18 10:384.5 1.4 1
Diisopropyl ether ND ug/kg 09/26/18 21:14 108-20-309/26/18 10:384.5 1.5 1
Ethylbenzene ND ug/kg 09/26/18 21:14 100-41-409/26/18 10:384.5 1.6 1
Hexachloro-1,3-butadiene ND ug/kg 09/26/18 21:14 87-68-309/26/18 10:384.5 1.8 1
2-Hexanone ND ug/kg 09/26/18 21:14 591-78-609/26/18 10:3845.1 3.5 1
Isopropylbenzene (Cumene)ND ug/kg 09/26/18 21:14 98-82-809/26/18 10:384.5 1.7 1
p-Isopropyltoluene ND ug/kg 09/26/18 21:14 99-87-609/26/18 10:384.5 1.5 1
Methylene Chloride ND ug/kg 09/26/18 21:14 75-09-209/26/18 10:3818.1 2.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/26/18 21:14 108-10-109/26/18 10:3845.1 3.3 1
Methyl-tert-butyl ether ND ug/kg 09/26/18 21:14 1634-04-409/26/18 10:384.5 1.4 1
Naphthalene ND ug/kg 09/26/18 21:14 91-20-309/26/18 10:384.5 1.1 1
n-Propylbenzene ND ug/kg 09/26/18 21:14 103-65-109/26/18 10:384.5 1.5 1
Styrene ND ug/kg 09/26/18 21:14 100-42-509/26/18 10:384.5 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/26/18 21:14 630-20-609/26/18 10:384.5 1.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/26/18 21:14 79-34-509/26/18 10:384.5 1.7 1
Tetrachloroethene ND ug/kg 09/26/18 21:14 127-18-409/26/18 10:384.5 1.5 1
Toluene ND ug/kg 09/26/18 21:14 108-88-309/26/18 10:384.5 1.6 1
1,2,3-Trichlorobenzene ND ug/kg 09/26/18 21:14 87-61-609/26/18 10:384.5 2.0 1
1,2,4-Trichlorobenzene ND ug/kg 09/26/18 21:14 120-82-109/26/18 10:384.5 1.4 1
1,1,1-Trichloroethane ND ug/kg 09/26/18 21:14 71-55-609/26/18 10:384.5 1.6 1
1,1,2-Trichloroethane ND ug/kg 09/26/18 21:14 79-00-509/26/18 10:384.5 1.9 1
Trichloroethene ND ug/kg 09/26/18 21:14 79-01-609/26/18 10:384.5 1.9 1
Trichlorofluoromethane ND ug/kg 09/26/18 21:14 75-69-409/26/18 10:384.5 2.0 1
1,2,3-Trichloropropane ND ug/kg 09/26/18 21:14 96-18-409/26/18 10:384.5 1.4 1
1,2,4-Trimethylbenzene ND ug/kg 09/26/18 21:14 95-63-609/26/18 10:384.5 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 09/26/18 21:14 108-67-809/26/18 10:384.5 1.6 1
Vinyl acetate ND ug/kg 09/26/18 21:14 108-05-409/26/18 10:3845.1 7.9 1
Vinyl chloride ND ug/kg 09/26/18 21:14 75-01-409/26/18 10:389.0 1.6 1
Xylene (Total)ND ug/kg 09/26/18 21:14 1330-20-709/26/18 10:389.0 3.3 1
m&p-Xylene ND ug/kg 09/26/18 21:14 179601-23-109/26/18 10:389.0 3.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB001 (4'-5')Lab ID:92400796002 Collected:09/24/18 14:30 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
o-Xylene ND ug/kg 09/26/18 21:14 95-47-609/26/18 10:384.5 1.7 1
Surrogates
Toluene-d8 (S)103 %09/26/18 21:14 2037-26-509/26/18 10:3870-130 1
4-Bromofluorobenzene (S)93 %09/26/18 21:14 460-00-409/26/18 10:3870-130 1
1,2-Dichloroethane-d4 (S)85 %09/26/18 21:14 17060-07-009/26/18 10:3870-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.1 %09/25/18 18:050.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB002 (0'-1')Lab ID:92400796003 Collected:09/24/18 14:40 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 10.4J ug/kg 09/27/18 23:00 83-32-909/26/18 14:1711.9 1.8 1
Acenaphthylene 8.4J ug/kg 09/27/18 23:00 208-96-809/26/18 14:1711.9 1.6 1
Anthracene 36.6 ug/kg 09/27/18 23:00 120-12-709/26/18 14:1711.9 1.7 1
Benzo(a)anthracene 235 ug/kg 09/27/18 23:00 56-55-309/26/18 14:1711.9 0.85 1
Benzo(a)pyrene 290 ug/kg 09/27/18 23:00 50-32-809/26/18 14:1711.9 1.3 1
Benzo(b)fluoranthene 537 ug/kg 09/27/18 23:00 205-99-2 2g09/26/18 14:1711.9 0.80 1
Benzo(g,h,i)perylene 266 ug/kg 09/27/18 23:00 191-24-209/26/18 14:1711.9 3.1 1
Benzo(k)fluoranthene ND ug/kg 09/27/18 23:00 207-08-909/26/18 14:1711.9 1.8 1
Chrysene 349 ug/kg 09/27/18 23:00 218-01-909/26/18 14:1711.9 2.1 1
Dibenz(a,h)anthracene 66.1 ug/kg 09/27/18 23:00 53-70-309/26/18 14:1711.9 2.1 1
Fluoranthene 300 ug/kg 09/27/18 23:00 206-44-009/26/18 14:1711.9 0.99 1
Fluorene 6.0J ug/kg 09/27/18 23:00 86-73-709/26/18 14:1711.9 1.9 1
Indeno(1,2,3-cd)pyrene 228 ug/kg 09/27/18 23:00 193-39-509/26/18 14:1711.9 3.3 1
1-Methylnaphthalene 17.4 ug/kg 09/27/18 23:00 90-12-009/26/18 14:1711.9 1.4 1
2-Methylnaphthalene 28.7 ug/kg 09/27/18 23:00 91-57-609/26/18 14:1711.9 1.3 1
Naphthalene 21.0 ug/kg 09/27/18 23:00 91-20-309/26/18 14:1711.9 2.7 1
Phenanthrene 158 ug/kg 09/27/18 23:00 85-01-809/26/18 14:1711.9 1.8 1
Pyrene 267 ug/kg 09/27/18 23:00 129-00-009/26/18 14:1711.9 2.1 1
Surrogates
Nitrobenzene-d5 (S)53 %09/27/18 23:00 4165-60-009/26/18 14:1710-128 1
2-Fluorobiphenyl (S)52 %09/27/18 23:00 321-60-809/26/18 14:1710-110 1
Terphenyl-d14 (S)90 %09/27/18 23:00 1718-51-009/26/18 14:1739-119 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone ND ug/kg 09/26/18 21:35 67-64-109/26/18 10:3898.0 9.8 1
Benzene ND ug/kg 09/26/18 21:35 71-43-209/26/18 10:384.9 1.6 1
Bromobenzene ND ug/kg 09/26/18 21:35 108-86-109/26/18 10:384.9 2.0 1
Bromochloromethane ND ug/kg 09/26/18 21:35 74-97-509/26/18 10:384.9 1.7 1
Bromodichloromethane ND ug/kg 09/26/18 21:35 75-27-409/26/18 10:384.9 1.9 1
Bromoform ND ug/kg 09/26/18 21:35 75-25-209/26/18 10:384.9 2.3 1
Bromomethane ND ug/kg 09/26/18 21:35 74-83-909/26/18 10:389.8 2.4 1
2-Butanone (MEK)ND ug/kg 09/26/18 21:35 78-93-309/26/18 10:3898.0 2.8 1
n-Butylbenzene ND ug/kg 09/26/18 21:35 104-51-809/26/18 10:384.9 1.8 1
sec-Butylbenzene ND ug/kg 09/26/18 21:35 135-98-809/26/18 10:384.9 1.6 1
tert-Butylbenzene ND ug/kg 09/26/18 21:35 98-06-609/26/18 10:384.9 2.0 1
Carbon tetrachloride ND ug/kg 09/26/18 21:35 56-23-509/26/18 10:384.9 2.5 1
Chlorobenzene ND ug/kg 09/26/18 21:35 108-90-709/26/18 10:384.9 1.9 1
Chloroethane ND ug/kg 09/26/18 21:35 75-00-309/26/18 10:389.8 2.4 1
Chloroform ND ug/kg 09/26/18 21:35 67-66-309/26/18 10:384.9 1.6 1
Chloromethane ND ug/kg 09/26/18 21:35 74-87-309/26/18 10:389.8 2.4 1
2-Chlorotoluene ND ug/kg 09/26/18 21:35 95-49-809/26/18 10:384.9 1.7 1
4-Chlorotoluene ND ug/kg 09/26/18 21:35 106-43-409/26/18 10:384.9 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/26/18 21:35 96-12-809/26/18 10:384.9 3.5 1
Dibromochloromethane ND ug/kg 09/26/18 21:35 124-48-109/26/18 10:384.9 1.8 1
1,2-Dibromoethane (EDB)ND ug/kg 09/26/18 21:35 106-93-409/26/18 10:384.9 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB002 (0'-1')Lab ID:92400796003 Collected:09/24/18 14:40 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Dibromomethane ND ug/kg 09/26/18 21:35 74-95-309/26/18 10:384.9 2.4 1
1,2-Dichlorobenzene ND ug/kg 09/26/18 21:35 95-50-109/26/18 10:384.9 1.9 1
1,3-Dichlorobenzene ND ug/kg 09/26/18 21:35 541-73-109/26/18 10:384.9 2.0 1
1,4-Dichlorobenzene ND ug/kg 09/26/18 21:35 106-46-709/26/18 10:384.9 1.7 1
Dichlorodifluoromethane ND ug/kg 09/26/18 21:35 75-71-809/26/18 10:389.8 3.5 1
1,1-Dichloroethane ND ug/kg 09/26/18 21:35 75-34-309/26/18 10:384.9 1.5 1
1,2-Dichloroethane ND ug/kg 09/26/18 21:35 107-06-209/26/18 10:384.9 2.2 1
1,1-Dichloroethene ND ug/kg 09/26/18 21:35 75-35-409/26/18 10:384.9 1.8 1
cis-1,2-Dichloroethene ND ug/kg 09/26/18 21:35 156-59-209/26/18 10:384.9 1.4 1
trans-1,2-Dichloroethene ND ug/kg 09/26/18 21:35 156-60-509/26/18 10:384.9 1.9 1
1,2-Dichloropropane ND ug/kg 09/26/18 21:35 78-87-509/26/18 10:384.9 1.7 1
1,3-Dichloropropane ND ug/kg 09/26/18 21:35 142-28-909/26/18 10:384.9 1.9 1
2,2-Dichloropropane ND ug/kg 09/26/18 21:35 594-20-709/26/18 10:384.9 1.7 1
1,1-Dichloropropene ND ug/kg 09/26/18 21:35 563-58-609/26/18 10:384.9 1.5 1
cis-1,3-Dichloropropene ND ug/kg 09/26/18 21:35 10061-01-509/26/18 10:384.9 1.8 1
trans-1,3-Dichloropropene ND ug/kg 09/26/18 21:35 10061-02-609/26/18 10:384.9 1.5 1
Diisopropyl ether ND ug/kg 09/26/18 21:35 108-20-309/26/18 10:384.9 1.7 1
Ethylbenzene ND ug/kg 09/26/18 21:35 100-41-409/26/18 10:384.9 1.8 1
Hexachloro-1,3-butadiene ND ug/kg 09/26/18 21:35 87-68-309/26/18 10:384.9 2.0 1
2-Hexanone ND ug/kg 09/26/18 21:35 591-78-609/26/18 10:3849.0 3.8 1
Isopropylbenzene (Cumene)ND ug/kg 09/26/18 21:35 98-82-809/26/18 10:384.9 1.9 1
p-Isopropyltoluene ND ug/kg 09/26/18 21:35 99-87-609/26/18 10:384.9 1.7 1
Methylene Chloride ND ug/kg 09/26/18 21:35 75-09-209/26/18 10:3819.6 2.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/26/18 21:35 108-10-109/26/18 10:3849.0 3.6 1
Methyl-tert-butyl ether ND ug/kg 09/26/18 21:35 1634-04-409/26/18 10:384.9 1.5 1
Naphthalene ND ug/kg 09/26/18 21:35 91-20-309/26/18 10:384.9 1.2 1
n-Propylbenzene ND ug/kg 09/26/18 21:35 103-65-109/26/18 10:384.9 1.7 1
Styrene ND ug/kg 09/26/18 21:35 100-42-509/26/18 10:384.9 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/26/18 21:35 630-20-609/26/18 10:384.9 2.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/26/18 21:35 79-34-509/26/18 10:384.9 1.9 1
Tetrachloroethene ND ug/kg 09/26/18 21:35 127-18-409/26/18 10:384.9 1.7 1
Toluene ND ug/kg 09/26/18 21:35 108-88-309/26/18 10:384.9 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 09/26/18 21:35 87-61-609/26/18 10:384.9 2.2 1
1,2,4-Trichlorobenzene ND ug/kg 09/26/18 21:35 120-82-109/26/18 10:384.9 1.6 1
1,1,1-Trichloroethane ND ug/kg 09/26/18 21:35 71-55-609/26/18 10:384.9 1.8 1
1,1,2-Trichloroethane ND ug/kg 09/26/18 21:35 79-00-509/26/18 10:384.9 2.1 1
Trichloroethene ND ug/kg 09/26/18 21:35 79-01-609/26/18 10:384.9 2.1 1
Trichlorofluoromethane ND ug/kg 09/26/18 21:35 75-69-409/26/18 10:384.9 2.2 1
1,2,3-Trichloropropane ND ug/kg 09/26/18 21:35 96-18-409/26/18 10:384.9 1.6 1
1,2,4-Trimethylbenzene ND ug/kg 09/26/18 21:35 95-63-609/26/18 10:384.9 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 09/26/18 21:35 108-67-809/26/18 10:384.9 1.8 1
Vinyl acetate ND ug/kg 09/26/18 21:35 108-05-409/26/18 10:3849.0 8.6 1
Vinyl chloride ND ug/kg 09/26/18 21:35 75-01-409/26/18 10:389.8 1.8 1
Xylene (Total)ND ug/kg 09/26/18 21:35 1330-20-709/26/18 10:389.8 3.5 1
m&p-Xylene ND ug/kg 09/26/18 21:35 179601-23-109/26/18 10:389.8 3.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 12 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB002 (0'-1')Lab ID:92400796003 Collected:09/24/18 14:40 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
o-Xylene ND ug/kg 09/26/18 21:35 95-47-609/26/18 10:384.9 1.9 1
Surrogates
Toluene-d8 (S)103 %09/26/18 21:35 2037-26-509/26/18 10:3870-130 1
4-Bromofluorobenzene (S)96 %09/26/18 21:35 460-00-409/26/18 10:3870-130 1
1,2-Dichloroethane-d4 (S)81 %09/26/18 21:35 17060-07-009/26/18 10:3870-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.8 %09/25/18 18:050.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB002 (4'-5')Lab ID:92400796004 Collected:09/24/18 14:45 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 4.4J ug/kg 09/27/18 23:21 83-32-909/26/18 14:1712.3 1.8 1
Acenaphthylene 8.0J ug/kg 09/27/18 23:21 208-96-809/26/18 14:1712.3 1.6 1
Anthracene 6.5J ug/kg 09/27/18 23:21 120-12-709/26/18 14:1712.3 1.7 1
Benzo(a)anthracene 63.5 ug/kg 09/27/18 23:21 56-55-3 1g09/26/18 14:1712.3 0.87 1
Benzo(a)pyrene ND ug/kg 09/27/18 23:21 50-32-809/26/18 14:1712.3 1.3 1
Benzo(b)fluoranthene 12.3 ug/kg 09/27/18 23:21 205-99-209/26/18 14:1712.3 0.82 1
Benzo(g,h,i)perylene ND ug/kg 09/27/18 23:21 191-24-209/26/18 14:1712.3 3.2 1
Benzo(k)fluoranthene ND ug/kg 09/27/18 23:21 207-08-909/26/18 14:1712.3 1.8 1
Chrysene ND ug/kg 09/27/18 23:21 218-01-909/26/18 14:1712.3 2.2 1
Dibenz(a,h)anthracene ND ug/kg 09/27/18 23:21 53-70-309/26/18 14:1712.3 2.2 1
Fluoranthene ND ug/kg 09/27/18 23:21 206-44-009/26/18 14:1712.3 1.0 1
Fluorene ND ug/kg 09/27/18 23:21 86-73-709/26/18 14:1712.3 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/kg 09/27/18 23:21 193-39-509/26/18 14:1712.3 3.4 1
1-Methylnaphthalene 4.6J ug/kg 09/27/18 23:21 90-12-009/26/18 14:1712.3 1.5 1
2-Methylnaphthalene 6.1J ug/kg 09/27/18 23:21 91-57-609/26/18 14:1712.3 1.3 1
Naphthalene ND ug/kg 09/27/18 23:21 91-20-309/26/18 14:1712.3 2.8 1
Phenanthrene 5.3J ug/kg 09/27/18 23:21 85-01-809/26/18 14:1712.3 1.8 1
Pyrene 31.0 ug/kg 09/27/18 23:21 129-00-009/26/18 14:1712.3 2.2 1
Surrogates
Nitrobenzene-d5 (S)76 %09/27/18 23:21 4165-60-009/26/18 14:1710-128 1
2-Fluorobiphenyl (S)68 %09/27/18 23:21 321-60-809/26/18 14:1710-110 1
Terphenyl-d14 (S)93 %09/27/18 23:21 1718-51-009/26/18 14:1739-119 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone 33.2J ug/kg 09/26/18 21:55 67-64-109/26/18 10:3813913.9 1
Benzene ND ug/kg 09/26/18 21:55 71-43-209/26/18 10:386.9 2.2 1
Bromobenzene ND ug/kg 09/26/18 21:55 108-86-109/26/18 10:386.9 2.8 1
Bromochloromethane ND ug/kg 09/26/18 21:55 74-97-509/26/18 10:386.9 2.4 1
Bromodichloromethane ND ug/kg 09/26/18 21:55 75-27-409/26/18 10:386.9 2.6 1
Bromoform ND ug/kg 09/26/18 21:55 75-25-209/26/18 10:386.9 3.2 1
Bromomethane ND ug/kg 09/26/18 21:55 74-83-909/26/18 10:3813.9 3.5 1
2-Butanone (MEK)ND ug/kg 09/26/18 21:55 78-93-309/26/18 10:381394.0 1
n-Butylbenzene ND ug/kg 09/26/18 21:55 104-51-809/26/18 10:386.9 2.5 1
sec-Butylbenzene ND ug/kg 09/26/18 21:55 135-98-809/26/18 10:386.9 2.2 1
tert-Butylbenzene ND ug/kg 09/26/18 21:55 98-06-609/26/18 10:386.9 2.8 1
Carbon tetrachloride ND ug/kg 09/26/18 21:55 56-23-509/26/18 10:386.9 3.6 1
Chlorobenzene ND ug/kg 09/26/18 21:55 108-90-709/26/18 10:386.9 2.6 1
Chloroethane ND ug/kg 09/26/18 21:55 75-00-309/26/18 10:3813.9 3.3 1
Chloroform ND ug/kg 09/26/18 21:55 67-66-309/26/18 10:386.9 2.2 1
Chloromethane ND ug/kg 09/26/18 21:55 74-87-309/26/18 10:3813.9 3.3 1
2-Chlorotoluene ND ug/kg 09/26/18 21:55 95-49-809/26/18 10:386.9 2.4 1
4-Chlorotoluene ND ug/kg 09/26/18 21:55 106-43-409/26/18 10:386.9 2.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/26/18 21:55 96-12-809/26/18 10:386.9 5.0 1
Dibromochloromethane ND ug/kg 09/26/18 21:55 124-48-109/26/18 10:386.9 2.5 1
1,2-Dibromoethane (EDB)ND ug/kg 09/26/18 21:55 106-93-409/26/18 10:386.9 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB002 (4'-5')Lab ID:92400796004 Collected:09/24/18 14:45 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Dibromomethane ND ug/kg 09/26/18 21:55 74-95-309/26/18 10:386.9 3.5 1
1,2-Dichlorobenzene ND ug/kg 09/26/18 21:55 95-50-109/26/18 10:386.9 2.6 1
1,3-Dichlorobenzene ND ug/kg 09/26/18 21:55 541-73-109/26/18 10:386.9 2.8 1
1,4-Dichlorobenzene ND ug/kg 09/26/18 21:55 106-46-709/26/18 10:386.9 2.4 1
Dichlorodifluoromethane ND ug/kg 09/26/18 21:55 75-71-809/26/18 10:3813.9 5.0 1
1,1-Dichloroethane ND ug/kg 09/26/18 21:55 75-34-309/26/18 10:386.9 2.1 1
1,2-Dichloroethane ND ug/kg 09/26/18 21:55 107-06-209/26/18 10:386.9 3.1 1
1,1-Dichloroethene ND ug/kg 09/26/18 21:55 75-35-409/26/18 10:386.9 2.5 1
cis-1,2-Dichloroethene ND ug/kg 09/26/18 21:55 156-59-209/26/18 10:386.9 1.9 1
trans-1,2-Dichloroethene ND ug/kg 09/26/18 21:55 156-60-509/26/18 10:386.9 2.6 1
1,2-Dichloropropane ND ug/kg 09/26/18 21:55 78-87-509/26/18 10:386.9 2.4 1
1,3-Dichloropropane ND ug/kg 09/26/18 21:55 142-28-909/26/18 10:386.9 2.6 1
2,2-Dichloropropane ND ug/kg 09/26/18 21:55 594-20-709/26/18 10:386.9 2.4 1
1,1-Dichloropropene ND ug/kg 09/26/18 21:55 563-58-609/26/18 10:386.9 2.1 1
cis-1,3-Dichloropropene ND ug/kg 09/26/18 21:55 10061-01-509/26/18 10:386.9 2.5 1
trans-1,3-Dichloropropene ND ug/kg 09/26/18 21:55 10061-02-609/26/18 10:386.9 2.1 1
Diisopropyl ether ND ug/kg 09/26/18 21:55 108-20-309/26/18 10:386.9 2.4 1
Ethylbenzene ND ug/kg 09/26/18 21:55 100-41-409/26/18 10:386.9 2.5 1
Hexachloro-1,3-butadiene ND ug/kg 09/26/18 21:55 87-68-309/26/18 10:386.9 2.8 1
2-Hexanone ND ug/kg 09/26/18 21:55 591-78-609/26/18 10:3869.4 5.4 1
Isopropylbenzene (Cumene)ND ug/kg 09/26/18 21:55 98-82-809/26/18 10:386.9 2.6 1
p-Isopropyltoluene ND ug/kg 09/26/18 21:55 99-87-609/26/18 10:386.9 2.4 1
Methylene Chloride ND ug/kg 09/26/18 21:55 75-09-209/26/18 10:3827.8 4.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/26/18 21:55 108-10-109/26/18 10:3869.4 5.1 1
Methyl-tert-butyl ether ND ug/kg 09/26/18 21:55 1634-04-409/26/18 10:386.9 2.1 1
Naphthalene ND ug/kg 09/26/18 21:55 91-20-309/26/18 10:386.9 1.7 1
n-Propylbenzene ND ug/kg 09/26/18 21:55 103-65-109/26/18 10:386.9 2.4 1
Styrene ND ug/kg 09/26/18 21:55 100-42-509/26/18 10:386.9 2.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/26/18 21:55 630-20-609/26/18 10:386.9 2.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/26/18 21:55 79-34-509/26/18 10:386.9 2.6 1
Tetrachloroethene ND ug/kg 09/26/18 21:55 127-18-409/26/18 10:386.9 2.4 1
Toluene ND ug/kg 09/26/18 21:55 108-88-309/26/18 10:386.9 2.5 1
1,2,3-Trichlorobenzene ND ug/kg 09/26/18 21:55 87-61-609/26/18 10:386.9 3.1 1
1,2,4-Trichlorobenzene ND ug/kg 09/26/18 21:55 120-82-109/26/18 10:386.9 2.2 1
1,1,1-Trichloroethane ND ug/kg 09/26/18 21:55 71-55-609/26/18 10:386.9 2.5 1
1,1,2-Trichloroethane ND ug/kg 09/26/18 21:55 79-00-509/26/18 10:386.9 2.9 1
Trichloroethene ND ug/kg 09/26/18 21:55 79-01-609/26/18 10:386.9 2.9 1
Trichlorofluoromethane ND ug/kg 09/26/18 21:55 75-69-409/26/18 10:386.9 3.1 1
1,2,3-Trichloropropane ND ug/kg 09/26/18 21:55 96-18-409/26/18 10:386.9 2.2 1
1,2,4-Trimethylbenzene ND ug/kg 09/26/18 21:55 95-63-609/26/18 10:386.9 2.8 1
1,3,5-Trimethylbenzene ND ug/kg 09/26/18 21:55 108-67-809/26/18 10:386.9 2.5 1
Vinyl acetate ND ug/kg 09/26/18 21:55 108-05-409/26/18 10:3869.4 12.2 1
Vinyl chloride ND ug/kg 09/26/18 21:55 75-01-409/26/18 10:3813.9 2.5 1
Xylene (Total)ND ug/kg 09/26/18 21:55 1330-20-709/26/18 10:3813.9 5.0 1
m&p-Xylene ND ug/kg 09/26/18 21:55 179601-23-109/26/18 10:3813.9 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB002 (4'-5')Lab ID:92400796004 Collected:09/24/18 14:45 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
o-Xylene ND ug/kg 09/26/18 21:55 95-47-609/26/18 10:386.9 2.6 1
Surrogates
Toluene-d8 (S)107 %09/26/18 21:55 2037-26-509/26/18 10:3870-130 1
4-Bromofluorobenzene (S)101 %09/26/18 21:55 460-00-409/26/18 10:3870-130 1
1,2-Dichloroethane-d4 (S)87 %09/26/18 21:55 17060-07-009/26/18 10:3870-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.4 %09/25/18 18:050.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB003 (0'-1')Lab ID:92400796005 Collected:09/24/18 15:00 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 765 ug/kg 09/27/18 23:42 83-32-909/26/18 14:1711.7 1.8 1
Acenaphthylene 99.9 ug/kg 09/27/18 23:42 208-96-809/26/18 14:1711.7 1.5 1
Anthracene 1320 ug/kg 09/28/18 15:07 120-12-709/26/18 14:1711716.4 10
Benzo(a)anthracene 2970 ug/kg 09/28/18 15:07 56-55-309/26/18 14:171178.3 10
Benzo(a)pyrene 2540 ug/kg 09/28/18 15:07 50-32-809/26/18 14:1711712.9 10
Benzo(b)fluoranthene 4070 ug/kg 09/28/18 15:07 205-99-209/26/18 14:171177.8 10
Benzo(g,h,i)perylene 1740 ug/kg 09/28/18 15:07 191-24-209/26/18 14:1711730.4 10
Benzo(k)fluoranthene ND ug/kg 09/27/18 23:42 207-08-909/26/18 14:1711.7 1.8 1
Chrysene 2850 ug/kg 09/28/18 15:07 218-01-909/26/18 14:1711721.0 10
Dibenz(a,h)anthracene 560 ug/kg 09/27/18 23:42 53-70-309/26/18 14:1711.7 2.1 1
Fluoranthene 5900 ug/kg 09/28/18 15:07 206-44-009/26/18 14:171179.7 10
Fluorene 660 ug/kg 09/27/18 23:42 86-73-709/26/18 14:1711.7 1.9 1
Indeno(1,2,3-cd)pyrene 1610 ug/kg 09/28/18 15:07 193-39-509/26/18 14:1711732.7 10
1-Methylnaphthalene 243 ug/kg 09/27/18 23:42 90-12-009/26/18 14:1711.7 1.4 1
2-Methylnaphthalene 420 ug/kg 09/27/18 23:42 91-57-609/26/18 14:1711.7 1.3 1
Naphthalene 1240 ug/kg 09/28/18 15:07 91-20-309/26/18 14:1711726.9 10
Phenanthrene 5170 ug/kg 09/28/18 15:07 85-01-809/26/18 14:1711717.5 10
Pyrene 5120 ug/kg 09/28/18 15:07 129-00-009/26/18 14:1711721.0 10
Surrogates
Nitrobenzene-d5 (S)58 %09/27/18 23:42 4165-60-009/26/18 14:1710-128 1
2-Fluorobiphenyl (S)54 %09/27/18 23:42 321-60-809/26/18 14:1710-110 1
Terphenyl-d14 (S)103 %09/27/18 23:42 1718-51-009/26/18 14:1739-119 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone 15.7J ug/kg 09/26/18 18:53 67-64-109/26/18 12:5810010.0 1
Benzene ND ug/kg 09/26/18 18:53 71-43-209/26/18 12:585.0 1.6 1
Bromobenzene ND ug/kg 09/26/18 18:53 108-86-109/26/18 12:585.0 2.0 1
Bromochloromethane ND ug/kg 09/26/18 18:53 74-97-509/26/18 12:585.0 1.7 1
Bromodichloromethane ND ug/kg 09/26/18 18:53 75-27-409/26/18 12:585.0 1.9 1
Bromoform ND ug/kg 09/26/18 18:53 75-25-209/26/18 12:585.0 2.3 1
Bromomethane ND ug/kg 09/26/18 18:53 74-83-909/26/18 12:5810.0 2.5 1
2-Butanone (MEK)ND ug/kg 09/26/18 18:53 78-93-309/26/18 12:581002.9 1
n-Butylbenzene ND ug/kg 09/26/18 18:53 104-51-809/26/18 12:585.0 1.8 1
sec-Butylbenzene ND ug/kg 09/26/18 18:53 135-98-809/26/18 12:585.0 1.6 1
tert-Butylbenzene ND ug/kg 09/26/18 18:53 98-06-609/26/18 12:585.0 2.0 1
Carbon tetrachloride ND ug/kg 09/26/18 18:53 56-23-509/26/18 12:585.0 2.6 1
Chlorobenzene ND ug/kg 09/26/18 18:53 108-90-709/26/18 12:585.0 1.9 1
Chloroethane ND ug/kg 09/26/18 18:53 75-00-309/26/18 12:5810.0 2.4 1
Chloroform ND ug/kg 09/26/18 18:53 67-66-309/26/18 12:585.0 1.6 1
Chloromethane ND ug/kg 09/26/18 18:53 74-87-309/26/18 12:5810.0 2.4 1
2-Chlorotoluene ND ug/kg 09/26/18 18:53 95-49-809/26/18 12:585.0 1.7 1
4-Chlorotoluene ND ug/kg 09/26/18 18:53 106-43-409/26/18 12:585.0 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/26/18 18:53 96-12-809/26/18 12:585.0 3.6 1
Dibromochloromethane ND ug/kg 09/26/18 18:53 124-48-109/26/18 12:585.0 1.8 1
1,2-Dibromoethane (EDB)ND ug/kg 09/26/18 18:53 106-93-409/26/18 12:585.0 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB003 (0'-1')Lab ID:92400796005 Collected:09/24/18 15:00 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Dibromomethane ND ug/kg 09/26/18 18:53 74-95-309/26/18 12:585.0 2.5 1
1,2-Dichlorobenzene ND ug/kg 09/26/18 18:53 95-50-109/26/18 12:585.0 1.9 1
1,3-Dichlorobenzene ND ug/kg 09/26/18 18:53 541-73-109/26/18 12:585.0 2.0 1
1,4-Dichlorobenzene ND ug/kg 09/26/18 18:53 106-46-709/26/18 12:585.0 1.7 1
Dichlorodifluoromethane ND ug/kg 09/26/18 18:53 75-71-809/26/18 12:5810.0 3.6 1
1,1-Dichloroethane ND ug/kg 09/26/18 18:53 75-34-309/26/18 12:585.0 1.5 1
1,2-Dichloroethane ND ug/kg 09/26/18 18:53 107-06-209/26/18 12:585.0 2.2 1
1,1-Dichloroethene ND ug/kg 09/26/18 18:53 75-35-409/26/18 12:585.0 1.8 1
cis-1,2-Dichloroethene ND ug/kg 09/26/18 18:53 156-59-209/26/18 12:585.0 1.4 1
trans-1,2-Dichloroethene ND ug/kg 09/26/18 18:53 156-60-509/26/18 12:585.0 1.9 1
1,2-Dichloropropane ND ug/kg 09/26/18 18:53 78-87-509/26/18 12:585.0 1.7 1
1,3-Dichloropropane ND ug/kg 09/26/18 18:53 142-28-909/26/18 12:585.0 1.9 1
2,2-Dichloropropane ND ug/kg 09/26/18 18:53 594-20-709/26/18 12:585.0 1.7 1
1,1-Dichloropropene ND ug/kg 09/26/18 18:53 563-58-609/26/18 12:585.0 1.5 1
cis-1,3-Dichloropropene ND ug/kg 09/26/18 18:53 10061-01-509/26/18 12:585.0 1.8 1
trans-1,3-Dichloropropene ND ug/kg 09/26/18 18:53 10061-02-609/26/18 12:585.0 1.5 1
Diisopropyl ether ND ug/kg 09/26/18 18:53 108-20-309/26/18 12:585.0 1.7 1
Ethylbenzene ND ug/kg 09/26/18 18:53 100-41-409/26/18 12:585.0 1.8 1
Hexachloro-1,3-butadiene ND ug/kg 09/26/18 18:53 87-68-309/26/18 12:585.0 2.0 1
2-Hexanone ND ug/kg 09/26/18 18:53 591-78-609/26/18 12:5850.1 3.9 1
Isopropylbenzene (Cumene)ND ug/kg 09/26/18 18:53 98-82-809/26/18 12:585.0 1.9 1
p-Isopropyltoluene ND ug/kg 09/26/18 18:53 99-87-609/26/18 12:585.0 1.7 1
Methylene Chloride ND ug/kg 09/26/18 18:53 75-09-209/26/18 12:5820.0 3.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/26/18 18:53 108-10-109/26/18 12:5850.1 3.7 1
Methyl-tert-butyl ether ND ug/kg 09/26/18 18:53 1634-04-409/26/18 12:585.0 1.5 1
Naphthalene 7.3 ug/kg 09/26/18 18:53 91-20-309/26/18 12:585.0 1.2 1
n-Propylbenzene ND ug/kg 09/26/18 18:53 103-65-109/26/18 12:585.0 1.7 1
Styrene ND ug/kg 09/26/18 18:53 100-42-509/26/18 12:585.0 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/26/18 18:53 630-20-609/26/18 12:585.0 2.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/26/18 18:53 79-34-509/26/18 12:585.0 1.9 1
Tetrachloroethene ND ug/kg 09/26/18 18:53 127-18-409/26/18 12:585.0 1.7 1
Toluene ND ug/kg 09/26/18 18:53 108-88-309/26/18 12:585.0 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 09/26/18 18:53 87-61-609/26/18 12:585.0 2.2 1
1,2,4-Trichlorobenzene ND ug/kg 09/26/18 18:53 120-82-109/26/18 12:585.0 1.6 1
1,1,1-Trichloroethane ND ug/kg 09/26/18 18:53 71-55-609/26/18 12:585.0 1.8 1
1,1,2-Trichloroethane ND ug/kg 09/26/18 18:53 79-00-509/26/18 12:585.0 2.1 1
Trichloroethene ND ug/kg 09/26/18 18:53 79-01-609/26/18 12:585.0 2.1 1
Trichlorofluoromethane ND ug/kg 09/26/18 18:53 75-69-409/26/18 12:585.0 2.2 1
1,2,3-Trichloropropane ND ug/kg 09/26/18 18:53 96-18-409/26/18 12:585.0 1.6 1
1,2,4-Trimethylbenzene ND ug/kg 09/26/18 18:53 95-63-609/26/18 12:585.0 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 09/26/18 18:53 108-67-809/26/18 12:585.0 1.8 1
Vinyl acetate ND ug/kg 09/26/18 18:53 108-05-409/26/18 12:5850.1 8.8 1
Vinyl chloride ND ug/kg 09/26/18 18:53 75-01-409/26/18 12:5810.0 1.8 1
Xylene (Total)ND ug/kg 09/26/18 18:53 1330-20-709/26/18 12:5810.0 3.6 1
m&p-Xylene ND ug/kg 09/26/18 18:53 179601-23-109/26/18 12:5810.0 3.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB003 (0'-1')Lab ID:92400796005 Collected:09/24/18 15:00 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
o-Xylene ND ug/kg 09/26/18 18:53 95-47-609/26/18 12:585.0 1.9 1
Surrogates
Toluene-d8 (S)97 %09/26/18 18:53 2037-26-509/26/18 12:5870-130 1
4-Bromofluorobenzene (S)94 %09/26/18 18:53 460-00-409/26/18 12:5870-130 1
1,2-Dichloroethane-d4 (S)89 %09/26/18 18:53 17060-07-009/26/18 12:5870-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.7 %09/25/18 18:050.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB003 (4'-5')Lab ID:92400796006 Collected:09/24/18 15:05 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 09/28/18 00:03 83-32-909/26/18 14:1712.4 1.9 1
Acenaphthylene ND ug/kg 09/28/18 00:03 208-96-809/26/18 14:1712.4 1.6 1
Anthracene ND ug/kg 09/28/18 00:03 120-12-709/26/18 14:1712.4 1.7 1
Benzo(a)anthracene 2.3J ug/kg 09/28/18 00:03 56-55-309/26/18 14:1712.4 0.88 1
Benzo(a)pyrene 2.3J ug/kg 09/28/18 00:03 50-32-809/26/18 14:1712.4 1.4 1
Benzo(b)fluoranthene 2.5J ug/kg 09/28/18 00:03 205-99-209/26/18 14:1712.4 0.83 1
Benzo(g,h,i)perylene 3.3J ug/kg 09/28/18 00:03 191-24-209/26/18 14:1712.4 3.2 1
Benzo(k)fluoranthene ND ug/kg 09/28/18 00:03 207-08-909/26/18 14:1712.4 1.9 1
Chrysene ND ug/kg 09/28/18 00:03 218-01-909/26/18 14:1712.4 2.2 1
Dibenz(a,h)anthracene ND ug/kg 09/28/18 00:03 53-70-309/26/18 14:1712.4 2.2 1
Fluoranthene 5.3J ug/kg 09/28/18 00:03 206-44-009/26/18 14:1712.4 1.0 1
Fluorene ND ug/kg 09/28/18 00:03 86-73-709/26/18 14:1712.4 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/kg 09/28/18 00:03 193-39-509/26/18 14:1712.4 3.5 1
1-Methylnaphthalene ND ug/kg 09/28/18 00:03 90-12-009/26/18 14:1712.4 1.5 1
2-Methylnaphthalene ND ug/kg 09/28/18 00:03 91-57-609/26/18 14:1712.4 1.4 1
Naphthalene ND ug/kg 09/28/18 00:03 91-20-309/26/18 14:1712.4 2.9 1
Phenanthrene 5.6J ug/kg 09/28/18 00:03 85-01-809/26/18 14:1712.4 1.9 1
Pyrene 4.7J ug/kg 09/28/18 00:03 129-00-009/26/18 14:1712.4 2.2 1
Surrogates
Nitrobenzene-d5 (S)14 %09/28/18 00:03 4165-60-009/26/18 14:1710-128 1
2-Fluorobiphenyl (S)14 %09/28/18 00:03 321-60-809/26/18 14:1710-110 1
Terphenyl-d14 (S)57 %09/28/18 00:03 1718-51-009/26/18 14:1739-119 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone 28.6J ug/kg 09/26/18 19:13 67-64-109/26/18 12:5810710.7 1
Benzene ND ug/kg 09/26/18 19:13 71-43-209/26/18 12:585.3 1.7 1
Bromobenzene ND ug/kg 09/26/18 19:13 108-86-109/26/18 12:585.3 2.1 1
Bromochloromethane ND ug/kg 09/26/18 19:13 74-97-509/26/18 12:585.3 1.8 1
Bromodichloromethane ND ug/kg 09/26/18 19:13 75-27-409/26/18 12:585.3 2.0 1
Bromoform ND ug/kg 09/26/18 19:13 75-25-209/26/18 12:585.3 2.5 1
Bromomethane ND ug/kg 09/26/18 19:13 74-83-909/26/18 12:5810.7 2.7 1
2-Butanone (MEK)ND ug/kg 09/26/18 19:13 78-93-309/26/18 12:581073.1 1
n-Butylbenzene ND ug/kg 09/26/18 19:13 104-51-809/26/18 12:585.3 1.9 1
sec-Butylbenzene ND ug/kg 09/26/18 19:13 135-98-809/26/18 12:585.3 1.7 1
tert-Butylbenzene ND ug/kg 09/26/18 19:13 98-06-609/26/18 12:585.3 2.1 1
Carbon tetrachloride ND ug/kg 09/26/18 19:13 56-23-509/26/18 12:585.3 2.8 1
Chlorobenzene ND ug/kg 09/26/18 19:13 108-90-709/26/18 12:585.3 2.0 1
Chloroethane ND ug/kg 09/26/18 19:13 75-00-309/26/18 12:5810.7 2.6 1
Chloroform ND ug/kg 09/26/18 19:13 67-66-309/26/18 12:585.3 1.7 1
Chloromethane ND ug/kg 09/26/18 19:13 74-87-309/26/18 12:5810.7 2.6 1
2-Chlorotoluene ND ug/kg 09/26/18 19:13 95-49-809/26/18 12:585.3 1.8 1
4-Chlorotoluene ND ug/kg 09/26/18 19:13 106-43-409/26/18 12:585.3 1.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/26/18 19:13 96-12-809/26/18 12:585.3 3.8 1
Dibromochloromethane ND ug/kg 09/26/18 19:13 124-48-109/26/18 12:585.3 1.9 1
1,2-Dibromoethane (EDB)ND ug/kg 09/26/18 19:13 106-93-409/26/18 12:585.3 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB003 (4'-5')Lab ID:92400796006 Collected:09/24/18 15:05 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Dibromomethane ND ug/kg 09/26/18 19:13 74-95-309/26/18 12:585.3 2.7 1
1,2-Dichlorobenzene ND ug/kg 09/26/18 19:13 95-50-109/26/18 12:585.3 2.0 1
1,3-Dichlorobenzene ND ug/kg 09/26/18 19:13 541-73-109/26/18 12:585.3 2.1 1
1,4-Dichlorobenzene ND ug/kg 09/26/18 19:13 106-46-709/26/18 12:585.3 1.8 1
Dichlorodifluoromethane ND ug/kg 09/26/18 19:13 75-71-809/26/18 12:5810.7 3.8 1
1,1-Dichloroethane ND ug/kg 09/26/18 19:13 75-34-309/26/18 12:585.3 1.6 1
1,2-Dichloroethane ND ug/kg 09/26/18 19:13 107-06-209/26/18 12:585.3 2.4 1
1,1-Dichloroethene ND ug/kg 09/26/18 19:13 75-35-409/26/18 12:585.3 1.9 1
cis-1,2-Dichloroethene ND ug/kg 09/26/18 19:13 156-59-209/26/18 12:585.3 1.5 1
trans-1,2-Dichloroethene ND ug/kg 09/26/18 19:13 156-60-509/26/18 12:585.3 2.0 1
1,2-Dichloropropane ND ug/kg 09/26/18 19:13 78-87-509/26/18 12:585.3 1.8 1
1,3-Dichloropropane ND ug/kg 09/26/18 19:13 142-28-909/26/18 12:585.3 2.0 1
2,2-Dichloropropane ND ug/kg 09/26/18 19:13 594-20-709/26/18 12:585.3 1.8 1
1,1-Dichloropropene ND ug/kg 09/26/18 19:13 563-58-609/26/18 12:585.3 1.6 1
cis-1,3-Dichloropropene ND ug/kg 09/26/18 19:13 10061-01-509/26/18 12:585.3 1.9 1
trans-1,3-Dichloropropene ND ug/kg 09/26/18 19:13 10061-02-609/26/18 12:585.3 1.6 1
Diisopropyl ether ND ug/kg 09/26/18 19:13 108-20-309/26/18 12:585.3 1.8 1
Ethylbenzene ND ug/kg 09/26/18 19:13 100-41-409/26/18 12:585.3 1.9 1
Hexachloro-1,3-butadiene ND ug/kg 09/26/18 19:13 87-68-309/26/18 12:585.3 2.1 1
2-Hexanone ND ug/kg 09/26/18 19:13 591-78-609/26/18 12:5853.5 4.2 1
Isopropylbenzene (Cumene)ND ug/kg 09/26/18 19:13 98-82-809/26/18 12:585.3 2.0 1
p-Isopropyltoluene ND ug/kg 09/26/18 19:13 99-87-609/26/18 12:585.3 1.8 1
Methylene Chloride 5.0J ug/kg 09/26/18 19:13 75-09-209/26/18 12:5821.4 3.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/26/18 19:13 108-10-109/26/18 12:5853.5 4.0 1
Methyl-tert-butyl ether ND ug/kg 09/26/18 19:13 1634-04-409/26/18 12:585.3 1.6 1
Naphthalene ND ug/kg 09/26/18 19:13 91-20-309/26/18 12:585.3 1.3 1
n-Propylbenzene ND ug/kg 09/26/18 19:13 103-65-109/26/18 12:585.3 1.8 1
Styrene ND ug/kg 09/26/18 19:13 100-42-509/26/18 12:585.3 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/26/18 19:13 630-20-609/26/18 12:585.3 2.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/26/18 19:13 79-34-509/26/18 12:585.3 2.0 1
Tetrachloroethene ND ug/kg 09/26/18 19:13 127-18-409/26/18 12:585.3 1.8 1
Toluene ND ug/kg 09/26/18 19:13 108-88-309/26/18 12:585.3 1.9 1
1,2,3-Trichlorobenzene ND ug/kg 09/26/18 19:13 87-61-609/26/18 12:585.3 2.4 1
1,2,4-Trichlorobenzene ND ug/kg 09/26/18 19:13 120-82-109/26/18 12:585.3 1.7 1
1,1,1-Trichloroethane ND ug/kg 09/26/18 19:13 71-55-609/26/18 12:585.3 1.9 1
1,1,2-Trichloroethane ND ug/kg 09/26/18 19:13 79-00-509/26/18 12:585.3 2.2 1
Trichloroethene ND ug/kg 09/26/18 19:13 79-01-609/26/18 12:585.3 2.2 1
Trichlorofluoromethane ND ug/kg 09/26/18 19:13 75-69-409/26/18 12:585.3 2.4 1
1,2,3-Trichloropropane ND ug/kg 09/26/18 19:13 96-18-409/26/18 12:585.3 1.7 1
1,2,4-Trimethylbenzene ND ug/kg 09/26/18 19:13 95-63-609/26/18 12:585.3 2.1 1
1,3,5-Trimethylbenzene ND ug/kg 09/26/18 19:13 108-67-809/26/18 12:585.3 1.9 1
Vinyl acetate ND ug/kg 09/26/18 19:13 108-05-409/26/18 12:5853.5 9.4 1
Vinyl chloride ND ug/kg 09/26/18 19:13 75-01-409/26/18 12:5810.7 1.9 1
Xylene (Total)ND ug/kg 09/26/18 19:13 1330-20-709/26/18 12:5810.7 3.8 1
m&p-Xylene ND ug/kg 09/26/18 19:13 179601-23-109/26/18 12:5810.7 3.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB003 (4'-5')Lab ID:92400796006 Collected:09/24/18 15:05 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
o-Xylene ND ug/kg 09/26/18 19:13 95-47-609/26/18 12:585.3 2.0 1
Surrogates
Toluene-d8 (S)99 %09/26/18 19:13 2037-26-509/26/18 12:5870-130 1
4-Bromofluorobenzene (S)98 %09/26/18 19:13 460-00-409/26/18 12:5870-130 1
1,2-Dichloroethane-d4 (S)92 %09/26/18 19:13 17060-07-009/26/18 12:5870-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 18.4 %09/25/18 18:050.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB004 (0'-1')Lab ID:92400796007 Collected:09/24/18 15:30 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 12.6 ug/kg 09/28/18 00:24 83-32-909/26/18 14:1712.2 1.8 1
Acenaphthylene 5.9J ug/kg 09/28/18 00:24 208-96-809/26/18 14:1712.2 1.6 1
Anthracene 34.5 ug/kg 09/28/18 00:24 120-12-709/26/18 14:1712.2 1.7 1
Benzo(a)anthracene 153 ug/kg 09/28/18 00:24 56-55-309/26/18 14:1712.2 0.86 1
Benzo(a)pyrene 134 ug/kg 09/28/18 00:24 50-32-809/26/18 14:1712.2 1.3 1
Benzo(b)fluoranthene 298 ug/kg 09/28/18 00:24 205-99-209/26/18 14:1712.2 0.82 1
Benzo(g,h,i)perylene 94.9 ug/kg 09/28/18 00:24 191-24-209/26/18 14:1712.2 3.2 1
Benzo(k)fluoranthene 92.5 ug/kg 09/28/18 00:24 207-08-909/26/18 14:1712.2 1.8 1
Chrysene 194 ug/kg 09/28/18 00:24 218-01-909/26/18 14:1712.2 2.2 1
Dibenz(a,h)anthracene 7.8J ug/kg 09/28/18 00:24 53-70-309/26/18 14:1712.2 2.2 1
Fluoranthene 198 ug/kg 09/28/18 00:24 206-44-009/26/18 14:1712.2 1.0 1
Fluorene 8.4J ug/kg 09/28/18 00:24 86-73-709/26/18 14:1712.2 1.9 1
Indeno(1,2,3-cd)pyrene 90.4 ug/kg 09/28/18 00:24 193-39-509/26/18 14:1712.2 3.4 1
1-Methylnaphthalene 7.4J ug/kg 09/28/18 00:24 90-12-009/26/18 14:1712.2 1.5 1
2-Methylnaphthalene 9.2J ug/kg 09/28/18 00:24 91-57-609/26/18 14:1712.2 1.3 1
Naphthalene 10.6J ug/kg 09/28/18 00:24 91-20-309/26/18 14:1712.2 2.8 1
Phenanthrene 110 ug/kg 09/28/18 00:24 85-01-809/26/18 14:1712.2 1.8 1
Pyrene 166 ug/kg 09/28/18 00:24 129-00-009/26/18 14:1712.2 2.2 1
Surrogates
Nitrobenzene-d5 (S)57 %09/28/18 00:24 4165-60-009/26/18 14:1710-128 1
2-Fluorobiphenyl (S)51 %09/28/18 00:24 321-60-809/26/18 14:1710-110 1
Terphenyl-d14 (S)72 %09/28/18 00:24 1718-51-009/26/18 14:1739-119 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone 231 ug/kg 09/26/18 19:32 67-64-109/26/18 12:5888.1 8.8 1
Benzene ND ug/kg 09/26/18 19:32 71-43-209/26/18 12:584.4 1.4 1
Bromobenzene ND ug/kg 09/26/18 19:32 108-86-109/26/18 12:584.4 1.8 1
Bromochloromethane ND ug/kg 09/26/18 19:32 74-97-509/26/18 12:584.4 1.5 1
Bromodichloromethane ND ug/kg 09/26/18 19:32 75-27-409/26/18 12:584.4 1.7 1
Bromoform ND ug/kg 09/26/18 19:32 75-25-209/26/18 12:584.4 2.0 1
Bromomethane ND ug/kg 09/26/18 19:32 74-83-909/26/18 12:588.8 2.2 1
2-Butanone (MEK)ND ug/kg 09/26/18 19:32 78-93-309/26/18 12:5888.1 2.6 1
n-Butylbenzene ND ug/kg 09/26/18 19:32 104-51-809/26/18 12:584.4 1.6 1
sec-Butylbenzene ND ug/kg 09/26/18 19:32 135-98-809/26/18 12:584.4 1.4 1
tert-Butylbenzene ND ug/kg 09/26/18 19:32 98-06-609/26/18 12:584.4 1.8 1
Carbon tetrachloride ND ug/kg 09/26/18 19:32 56-23-509/26/18 12:584.4 2.3 1
Chlorobenzene ND ug/kg 09/26/18 19:32 108-90-709/26/18 12:584.4 1.7 1
Chloroethane ND ug/kg 09/26/18 19:32 75-00-309/26/18 12:588.8 2.1 1
Chloroform ND ug/kg 09/26/18 19:32 67-66-309/26/18 12:584.4 1.4 1
Chloromethane ND ug/kg 09/26/18 19:32 74-87-309/26/18 12:588.8 2.1 1
2-Chlorotoluene ND ug/kg 09/26/18 19:32 95-49-809/26/18 12:584.4 1.5 1
4-Chlorotoluene ND ug/kg 09/26/18 19:32 106-43-409/26/18 12:584.4 1.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/26/18 19:32 96-12-809/26/18 12:584.4 3.2 1
Dibromochloromethane ND ug/kg 09/26/18 19:32 124-48-109/26/18 12:584.4 1.6 1
1,2-Dibromoethane (EDB)ND ug/kg 09/26/18 19:32 106-93-409/26/18 12:584.4 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB004 (0'-1')Lab ID:92400796007 Collected:09/24/18 15:30 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Dibromomethane ND ug/kg 09/26/18 19:32 74-95-309/26/18 12:584.4 2.2 1
1,2-Dichlorobenzene ND ug/kg 09/26/18 19:32 95-50-109/26/18 12:584.4 1.7 1
1,3-Dichlorobenzene ND ug/kg 09/26/18 19:32 541-73-109/26/18 12:584.4 1.8 1
1,4-Dichlorobenzene ND ug/kg 09/26/18 19:32 106-46-709/26/18 12:584.4 1.5 1
Dichlorodifluoromethane ND ug/kg 09/26/18 19:32 75-71-809/26/18 12:588.8 3.2 1
1,1-Dichloroethane ND ug/kg 09/26/18 19:32 75-34-309/26/18 12:584.4 1.3 1
1,2-Dichloroethane ND ug/kg 09/26/18 19:32 107-06-209/26/18 12:584.4 1.9 1
1,1-Dichloroethene ND ug/kg 09/26/18 19:32 75-35-409/26/18 12:584.4 1.6 1
cis-1,2-Dichloroethene ND ug/kg 09/26/18 19:32 156-59-209/26/18 12:584.4 1.2 1
trans-1,2-Dichloroethene ND ug/kg 09/26/18 19:32 156-60-509/26/18 12:584.4 1.7 1
1,2-Dichloropropane ND ug/kg 09/26/18 19:32 78-87-509/26/18 12:584.4 1.5 1
1,3-Dichloropropane ND ug/kg 09/26/18 19:32 142-28-909/26/18 12:584.4 1.7 1
2,2-Dichloropropane ND ug/kg 09/26/18 19:32 594-20-709/26/18 12:584.4 1.5 1
1,1-Dichloropropene ND ug/kg 09/26/18 19:32 563-58-609/26/18 12:584.4 1.3 1
cis-1,3-Dichloropropene ND ug/kg 09/26/18 19:32 10061-01-509/26/18 12:584.4 1.6 1
trans-1,3-Dichloropropene ND ug/kg 09/26/18 19:32 10061-02-609/26/18 12:584.4 1.3 1
Diisopropyl ether ND ug/kg 09/26/18 19:32 108-20-309/26/18 12:584.4 1.5 1
Ethylbenzene ND ug/kg 09/26/18 19:32 100-41-409/26/18 12:584.4 1.6 1
Hexachloro-1,3-butadiene ND ug/kg 09/26/18 19:32 87-68-309/26/18 12:584.4 1.8 1
2-Hexanone ND ug/kg 09/26/18 19:32 591-78-609/26/18 12:5844.1 3.4 1
Isopropylbenzene (Cumene)ND ug/kg 09/26/18 19:32 98-82-809/26/18 12:584.4 1.7 1
p-Isopropyltoluene ND ug/kg 09/26/18 19:32 99-87-609/26/18 12:584.4 1.5 1
Methylene Chloride 4.0J ug/kg 09/26/18 19:32 75-09-209/26/18 12:5817.6 2.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/26/18 19:32 108-10-109/26/18 12:5844.1 3.3 1
Methyl-tert-butyl ether ND ug/kg 09/26/18 19:32 1634-04-409/26/18 12:584.4 1.3 1
Naphthalene ND ug/kg 09/26/18 19:32 91-20-309/26/18 12:584.4 1.1 1
n-Propylbenzene ND ug/kg 09/26/18 19:32 103-65-109/26/18 12:584.4 1.5 1
Styrene ND ug/kg 09/26/18 19:32 100-42-509/26/18 12:584.4 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/26/18 19:32 630-20-609/26/18 12:584.4 1.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/26/18 19:32 79-34-509/26/18 12:584.4 1.7 1
Tetrachloroethene ND ug/kg 09/26/18 19:32 127-18-409/26/18 12:584.4 1.5 1
Toluene ND ug/kg 09/26/18 19:32 108-88-309/26/18 12:584.4 1.6 1
1,2,3-Trichlorobenzene ND ug/kg 09/26/18 19:32 87-61-609/26/18 12:584.4 1.9 1
1,2,4-Trichlorobenzene ND ug/kg 09/26/18 19:32 120-82-109/26/18 12:584.4 1.4 1
1,1,1-Trichloroethane ND ug/kg 09/26/18 19:32 71-55-609/26/18 12:584.4 1.6 1
1,1,2-Trichloroethane ND ug/kg 09/26/18 19:32 79-00-509/26/18 12:584.4 1.9 1
Trichloroethene ND ug/kg 09/26/18 19:32 79-01-609/26/18 12:584.4 1.9 1
Trichlorofluoromethane ND ug/kg 09/26/18 19:32 75-69-409/26/18 12:584.4 1.9 1
1,2,3-Trichloropropane ND ug/kg 09/26/18 19:32 96-18-409/26/18 12:584.4 1.4 1
1,2,4-Trimethylbenzene ND ug/kg 09/26/18 19:32 95-63-609/26/18 12:584.4 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 09/26/18 19:32 108-67-809/26/18 12:584.4 1.6 1
Vinyl acetate ND ug/kg 09/26/18 19:32 108-05-409/26/18 12:5844.1 7.8 1
Vinyl chloride ND ug/kg 09/26/18 19:32 75-01-409/26/18 12:588.8 1.6 1
Xylene (Total)ND ug/kg 09/26/18 19:32 1330-20-709/26/18 12:588.8 3.2 1
m&p-Xylene ND ug/kg 09/26/18 19:32 179601-23-109/26/18 12:588.8 3.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB004 (0'-1')Lab ID:92400796007 Collected:09/24/18 15:30 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
o-Xylene ND ug/kg 09/26/18 19:32 95-47-609/26/18 12:584.4 1.7 1
Surrogates
Toluene-d8 (S)97 %09/26/18 19:32 2037-26-509/26/18 12:5870-130 1
4-Bromofluorobenzene (S)97 %09/26/18 19:32 460-00-409/26/18 12:5870-130 1
1,2-Dichloroethane-d4 (S)94 %09/26/18 19:32 17060-07-009/26/18 12:5870-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.9 %09/25/18 18:050.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB004 (4'-5')Lab ID:92400796008 Collected:09/24/18 15:35 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 09/28/18 00:45 83-32-909/26/18 14:1712.1 1.8 1
Acenaphthylene ND ug/kg 09/28/18 00:45 208-96-809/26/18 14:1712.1 1.6 1
Anthracene ND ug/kg 09/28/18 00:45 120-12-709/26/18 14:1712.1 1.7 1
Benzo(a)anthracene 1.6J ug/kg 09/28/18 00:45 56-55-309/26/18 14:1712.1 0.86 1
Benzo(a)pyrene ND ug/kg 09/28/18 00:45 50-32-809/26/18 14:1712.1 1.3 1
Benzo(b)fluoranthene 2.0J ug/kg 09/28/18 00:45 205-99-209/26/18 14:1712.1 0.81 1
Benzo(g,h,i)perylene ND ug/kg 09/28/18 00:45 191-24-209/26/18 14:1712.1 3.1 1
Benzo(k)fluoranthene ND ug/kg 09/28/18 00:45 207-08-909/26/18 14:1712.1 1.8 1
Chrysene ND ug/kg 09/28/18 00:45 218-01-909/26/18 14:1712.1 2.2 1
Dibenz(a,h)anthracene ND ug/kg 09/28/18 00:45 53-70-309/26/18 14:1712.1 2.2 1
Fluoranthene 2.5J ug/kg 09/28/18 00:45 206-44-009/26/18 14:1712.1 1.0 1
Fluorene ND ug/kg 09/28/18 00:45 86-73-709/26/18 14:1712.1 1.9 1
Indeno(1,2,3-cd)pyrene ND ug/kg 09/28/18 00:45 193-39-509/26/18 14:1712.1 3.4 1
1-Methylnaphthalene ND ug/kg 09/28/18 00:45 90-12-009/26/18 14:1712.1 1.4 1
2-Methylnaphthalene ND ug/kg 09/28/18 00:45 91-57-609/26/18 14:1712.1 1.3 1
Naphthalene ND ug/kg 09/28/18 00:45 91-20-309/26/18 14:1712.1 2.8 1
Phenanthrene ND ug/kg 09/28/18 00:45 85-01-809/26/18 14:1712.1 1.8 1
Pyrene 2.2J ug/kg 09/28/18 00:45 129-00-009/26/18 14:1712.1 2.2 1
Surrogates
Nitrobenzene-d5 (S)65 %09/28/18 00:45 4165-60-009/26/18 14:1710-128 1
2-Fluorobiphenyl (S)59 %09/28/18 00:45 321-60-809/26/18 14:1710-110 1
Terphenyl-d14 (S)72 %09/28/18 00:45 1718-51-009/26/18 14:1739-119 1
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Acetone 77.2J ug/kg 09/26/18 19:52 67-64-109/26/18 12:5882.4 8.2 1
Benzene ND ug/kg 09/26/18 19:52 71-43-209/26/18 12:584.1 1.3 1
Bromobenzene ND ug/kg 09/26/18 19:52 108-86-109/26/18 12:584.1 1.6 1
Bromochloromethane ND ug/kg 09/26/18 19:52 74-97-509/26/18 12:584.1 1.4 1
Bromodichloromethane ND ug/kg 09/26/18 19:52 75-27-409/26/18 12:584.1 1.6 1
Bromoform ND ug/kg 09/26/18 19:52 75-25-209/26/18 12:584.1 1.9 1
Bromomethane ND ug/kg 09/26/18 19:52 74-83-909/26/18 12:588.2 2.1 1
2-Butanone (MEK)ND ug/kg 09/26/18 19:52 78-93-309/26/18 12:5882.4 2.4 1
n-Butylbenzene ND ug/kg 09/26/18 19:52 104-51-809/26/18 12:584.1 1.5 1
sec-Butylbenzene ND ug/kg 09/26/18 19:52 135-98-809/26/18 12:584.1 1.3 1
tert-Butylbenzene ND ug/kg 09/26/18 19:52 98-06-609/26/18 12:584.1 1.6 1
Carbon tetrachloride ND ug/kg 09/26/18 19:52 56-23-509/26/18 12:584.1 2.1 1
Chlorobenzene ND ug/kg 09/26/18 19:52 108-90-709/26/18 12:584.1 1.6 1
Chloroethane ND ug/kg 09/26/18 19:52 75-00-309/26/18 12:588.2 2.0 1
Chloroform ND ug/kg 09/26/18 19:52 67-66-309/26/18 12:584.1 1.3 1
Chloromethane ND ug/kg 09/26/18 19:52 74-87-309/26/18 12:588.2 2.0 1
2-Chlorotoluene ND ug/kg 09/26/18 19:52 95-49-809/26/18 12:584.1 1.4 1
4-Chlorotoluene ND ug/kg 09/26/18 19:52 106-43-409/26/18 12:584.1 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/26/18 19:52 96-12-809/26/18 12:584.1 3.0 1
Dibromochloromethane ND ug/kg 09/26/18 19:52 124-48-109/26/18 12:584.1 1.5 1
1,2-Dibromoethane (EDB)ND ug/kg 09/26/18 19:52 106-93-409/26/18 12:584.1 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB004 (4'-5')Lab ID:92400796008 Collected:09/24/18 15:35 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
Dibromomethane ND ug/kg 09/26/18 19:52 74-95-309/26/18 12:584.1 2.1 1
1,2-Dichlorobenzene ND ug/kg 09/26/18 19:52 95-50-109/26/18 12:584.1 1.6 1
1,3-Dichlorobenzene ND ug/kg 09/26/18 19:52 541-73-109/26/18 12:584.1 1.6 1
1,4-Dichlorobenzene ND ug/kg 09/26/18 19:52 106-46-709/26/18 12:584.1 1.4 1
Dichlorodifluoromethane ND ug/kg 09/26/18 19:52 75-71-809/26/18 12:588.2 3.0 1
1,1-Dichloroethane ND ug/kg 09/26/18 19:52 75-34-309/26/18 12:584.1 1.2 1
1,2-Dichloroethane ND ug/kg 09/26/18 19:52 107-06-209/26/18 12:584.1 1.8 1
1,1-Dichloroethene ND ug/kg 09/26/18 19:52 75-35-409/26/18 12:584.1 1.5 1
cis-1,2-Dichloroethene ND ug/kg 09/26/18 19:52 156-59-209/26/18 12:584.1 1.2 1
trans-1,2-Dichloroethene ND ug/kg 09/26/18 19:52 156-60-509/26/18 12:584.1 1.6 1
1,2-Dichloropropane ND ug/kg 09/26/18 19:52 78-87-509/26/18 12:584.1 1.4 1
1,3-Dichloropropane ND ug/kg 09/26/18 19:52 142-28-909/26/18 12:584.1 1.6 1
2,2-Dichloropropane ND ug/kg 09/26/18 19:52 594-20-709/26/18 12:584.1 1.4 1
1,1-Dichloropropene ND ug/kg 09/26/18 19:52 563-58-609/26/18 12:584.1 1.2 1
cis-1,3-Dichloropropene ND ug/kg 09/26/18 19:52 10061-01-509/26/18 12:584.1 1.5 1
trans-1,3-Dichloropropene ND ug/kg 09/26/18 19:52 10061-02-609/26/18 12:584.1 1.2 1
Diisopropyl ether ND ug/kg 09/26/18 19:52 108-20-309/26/18 12:584.1 1.4 1
Ethylbenzene ND ug/kg 09/26/18 19:52 100-41-409/26/18 12:584.1 1.5 1
Hexachloro-1,3-butadiene ND ug/kg 09/26/18 19:52 87-68-309/26/18 12:584.1 1.6 1
2-Hexanone ND ug/kg 09/26/18 19:52 591-78-609/26/18 12:5841.2 3.2 1
Isopropylbenzene (Cumene)ND ug/kg 09/26/18 19:52 98-82-809/26/18 12:584.1 1.6 1
p-Isopropyltoluene ND ug/kg 09/26/18 19:52 99-87-609/26/18 12:584.1 1.4 1
Methylene Chloride ND ug/kg 09/26/18 19:52 75-09-209/26/18 12:5816.5 2.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/26/18 19:52 108-10-109/26/18 12:5841.2 3.0 1
Methyl-tert-butyl ether ND ug/kg 09/26/18 19:52 1634-04-409/26/18 12:584.1 1.2 1
Naphthalene ND ug/kg 09/26/18 19:52 91-20-309/26/18 12:584.1 0.99 1
n-Propylbenzene ND ug/kg 09/26/18 19:52 103-65-109/26/18 12:584.1 1.4 1
Styrene ND ug/kg 09/26/18 19:52 100-42-509/26/18 12:584.1 1.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/26/18 19:52 630-20-609/26/18 12:584.1 1.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/26/18 19:52 79-34-509/26/18 12:584.1 1.6 1
Tetrachloroethene ND ug/kg 09/26/18 19:52 127-18-409/26/18 12:584.1 1.4 1
Toluene ND ug/kg 09/26/18 19:52 108-88-309/26/18 12:584.1 1.5 1
1,2,3-Trichlorobenzene ND ug/kg 09/26/18 19:52 87-61-609/26/18 12:584.1 1.8 1
1,2,4-Trichlorobenzene ND ug/kg 09/26/18 19:52 120-82-109/26/18 12:584.1 1.3 1
1,1,1-Trichloroethane ND ug/kg 09/26/18 19:52 71-55-609/26/18 12:584.1 1.5 1
1,1,2-Trichloroethane ND ug/kg 09/26/18 19:52 79-00-509/26/18 12:584.1 1.7 1
Trichloroethene ND ug/kg 09/26/18 19:52 79-01-609/26/18 12:584.1 1.7 1
Trichlorofluoromethane ND ug/kg 09/26/18 19:52 75-69-409/26/18 12:584.1 1.8 1
1,2,3-Trichloropropane ND ug/kg 09/26/18 19:52 96-18-409/26/18 12:584.1 1.3 1
1,2,4-Trimethylbenzene ND ug/kg 09/26/18 19:52 95-63-609/26/18 12:584.1 1.6 1
1,3,5-Trimethylbenzene ND ug/kg 09/26/18 19:52 108-67-809/26/18 12:584.1 1.5 1
Vinyl acetate ND ug/kg 09/26/18 19:52 108-05-409/26/18 12:5841.2 7.2 1
Vinyl chloride ND ug/kg 09/26/18 19:52 75-01-409/26/18 12:588.2 1.5 1
Xylene (Total)ND ug/kg 09/26/18 19:52 1330-20-709/26/18 12:588.2 3.0 1
m&p-Xylene ND ug/kg 09/26/18 19:52 179601-23-109/26/18 12:588.2 3.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 52
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Sample:MSA-SB004 (4'-5')Lab ID:92400796008 Collected:09/24/18 15:35 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B Preparation Method: EPA 5035A8260/5035A Volatile Organics
o-Xylene ND ug/kg 09/26/18 19:52 95-47-609/26/18 12:584.1 1.6 1
Surrogates
Toluene-d8 (S)98 %09/26/18 19:52 2037-26-509/26/18 12:5870-130 1
4-Bromofluorobenzene (S)96 %09/26/18 19:52 460-00-409/26/18 12:5870-130 1
1,2-Dichloroethane-d4 (S)91 %09/26/18 19:52 17060-07-009/26/18 12:5870-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.6 %09/25/18 18:290.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
432748
EPA 5035A
EPA 8260B
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92400796001, 92400796002, 92400796003, 92400796004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2384933
Associated Lab Samples:92400796001, 92400796002, 92400796003, 92400796004
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 4.8 09/26/18 13:042.0
1,1,1-Trichloroethane ug/kg ND 4.8 09/26/18 13:041.7
1,1,2,2-Tetrachloroethane ug/kg ND 4.8 09/26/18 13:041.8
1,1,2-Trichloroethane ug/kg ND 4.8 09/26/18 13:042.0
1,1-Dichloroethane ug/kg ND 4.8 09/26/18 13:041.4
1,1-Dichloroethene ug/kg ND 4.8 09/26/18 13:041.7
1,1-Dichloropropene ug/kg ND 4.8 09/26/18 13:041.4
1,2,3-Trichlorobenzene ug/kg ND 4.8 09/26/18 13:042.1
1,2,3-Trichloropropane ug/kg ND 4.8 09/26/18 13:041.5
1,2,4-Trichlorobenzene ug/kg ND 4.8 09/26/18 13:041.5
1,2,4-Trimethylbenzene ug/kg ND 4.8 09/26/18 13:041.9
1,2-Dibromo-3-chloropropane ug/kg ND 4.8 09/26/18 13:043.4
1,2-Dibromoethane (EDB)ug/kg ND 4.8 09/26/18 13:041.7
1,2-Dichlorobenzene ug/kg ND 4.8 09/26/18 13:041.8
1,2-Dichloroethane ug/kg ND 4.8 09/26/18 13:042.1
1,2-Dichloropropane ug/kg ND 4.8 09/26/18 13:041.6
1,3,5-Trimethylbenzene ug/kg ND 4.8 09/26/18 13:041.7
1,3-Dichlorobenzene ug/kg ND 4.8 09/26/18 13:041.9
1,3-Dichloropropane ug/kg ND 4.8 09/26/18 13:041.8
1,4-Dichlorobenzene ug/kg ND 4.8 09/26/18 13:041.6
2,2-Dichloropropane ug/kg ND 4.8 09/26/18 13:041.6
2-Butanone (MEK)ug/kg ND 95.1 09/26/18 13:042.8
2-Chlorotoluene ug/kg ND 4.8 09/26/18 13:041.6
2-Hexanone ug/kg ND 47.5 09/26/18 13:043.7
4-Chlorotoluene ug/kg ND 4.8 09/26/18 13:041.7
4-Methyl-2-pentanone (MIBK)ug/kg ND 47.5 09/26/18 13:043.5
Acetone ug/kg ND 95.1 09/26/18 13:049.5
Benzene ug/kg ND 4.8 09/26/18 13:041.5
Bromobenzene ug/kg ND 4.8 09/26/18 13:041.9
Bromochloromethane ug/kg ND 4.8 09/26/18 13:041.6
Bromodichloromethane ug/kg ND 4.8 09/26/18 13:041.8
Bromoform ug/kg ND 4.8 09/26/18 13:042.2
Bromomethane ug/kg ND 9.5 09/26/18 13:042.4
Carbon tetrachloride ug/kg ND 4.8 09/26/18 13:042.5
Chlorobenzene ug/kg ND 4.8 09/26/18 13:041.8
Chloroethane ug/kg ND 9.5 09/26/18 13:042.3
Chloroform ug/kg ND 4.8 09/26/18 13:041.5
Chloromethane ug/kg ND 9.5 09/26/18 13:042.3
cis-1,2-Dichloroethene ug/kg ND 4.8 09/26/18 13:041.3
cis-1,3-Dichloropropene ug/kg ND 4.8 09/26/18 13:041.7
Dibromochloromethane ug/kg ND 4.8 09/26/18 13:041.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2384933
Associated Lab Samples:92400796001, 92400796002, 92400796003, 92400796004
Matrix:Solid
AnalyzedMDL
Dibromomethane ug/kg ND 4.8 09/26/18 13:042.4
Dichlorodifluoromethane ug/kg ND 9.5 09/26/18 13:043.4
Diisopropyl ether ug/kg ND 4.8 09/26/18 13:041.6
Ethylbenzene ug/kg ND 4.8 09/26/18 13:041.7
Hexachloro-1,3-butadiene ug/kg ND 4.8 09/26/18 13:041.9
Isopropylbenzene (Cumene)ug/kg ND 4.8 09/26/18 13:041.8
m&p-Xylene ug/kg ND 9.5 09/26/18 13:043.4
Methyl-tert-butyl ether ug/kg ND 4.8 09/26/18 13:041.4
Methylene Chloride ug/kg ND 19.0 09/26/18 13:042.9
n-Butylbenzene ug/kg ND 4.8 09/26/18 13:041.7
n-Propylbenzene ug/kg ND 4.8 09/26/18 13:041.6
Naphthalene ug/kg ND 4.8 09/26/18 13:041.1
o-Xylene ug/kg ND 4.8 09/26/18 13:041.8
p-Isopropyltoluene ug/kg ND 4.8 09/26/18 13:041.6
sec-Butylbenzene ug/kg ND 4.8 09/26/18 13:041.5
Styrene ug/kg ND 4.8 09/26/18 13:041.7
tert-Butylbenzene ug/kg ND 4.8 09/26/18 13:041.9
Tetrachloroethene ug/kg ND 4.8 09/26/18 13:041.6
Toluene ug/kg ND 4.8 09/26/18 13:041.7
trans-1,2-Dichloroethene ug/kg ND 4.8 09/26/18 13:041.8
trans-1,3-Dichloropropene ug/kg ND 4.8 09/26/18 13:041.4
Trichloroethene ug/kg ND 4.8 09/26/18 13:042.0
Trichlorofluoromethane ug/kg ND 4.8 09/26/18 13:042.1
Vinyl acetate ug/kg ND 47.5 09/26/18 13:048.4
Vinyl chloride ug/kg ND 9.5 09/26/18 13:041.7
Xylene (Total)ug/kg ND 9.5 09/26/18 13:043.4
1,2-Dichloroethane-d4 (S)%90 70-132 09/26/18 13:04
4-Bromofluorobenzene (S)%93 70-130 09/26/18 13:04
Toluene-d8 (S)%106 70-130 09/26/18 13:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2384934LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 48.448.7 99 74-137
1,1,1-Trichloroethane ug/kg 51.648.7 106 67-140
1,1,2,2-Tetrachloroethane ug/kg 46.848.7 96 72-141
1,1,2-Trichloroethane ug/kg 49.748.7 102 78-138
1,1-Dichloroethane ug/kg 49.648.7 102 69-134
1,1-Dichloroethene ug/kg 58.448.7 120 67-138
1,1-Dichloropropene ug/kg 51.248.7 105 69-139
1,2,3-Trichlorobenzene ug/kg 50.548.7 104 70-146
1,2,3-Trichloropropane ug/kg 50.748.7 104 69-144
1,2,4-Trichlorobenzene ug/kg 50.648.7 104 68-148
1,2,4-Trimethylbenzene ug/kg 50.448.7 103 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2384934LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 47.548.7 98 65-140
1,2-Dibromoethane (EDB)ug/kg 51.848.7 106 77-135
1,2-Dichlorobenzene ug/kg 49.448.7 101 77-141
1,2-Dichloroethane ug/kg 47.948.7 98 65-137
1,2-Dichloropropane ug/kg 50.248.7 103 72-136
1,3,5-Trimethylbenzene ug/kg 49.848.7 102 76-133
1,3-Dichlorobenzene ug/kg 49.248.7 101 74-138
1,3-Dichloropropane ug/kg 52.448.7 108 71-139
1,4-Dichlorobenzene ug/kg 48.848.7 100 76-138
2,2-Dichloropropane ug/kg 48.048.7 99 68-137
2-Butanone (MEK)ug/kg 10397.5 105 58-147
2-Chlorotoluene ug/kg 48.048.7 98 73-139
2-Hexanone ug/kg 85.897.5 88 62-145
4-Chlorotoluene ug/kg 47.948.7 98 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 94.497.5 97 64-149
Acetone ug/kg 10297.5 105 53-153
Benzene ug/kg 53.648.7 110 73-135
Bromobenzene ug/kg 49.548.7 102 75-133
Bromochloromethane ug/kg 48.348.7 99 73-134
Bromodichloromethane ug/kg 53.648.7 110 71-135
Bromoform ug/kg 50.648.7 104 66-141
Bromomethane ug/kg 54.148.7 111 53-160
Carbon tetrachloride ug/kg 50.748.7 104 60-145
Chlorobenzene ug/kg 50.348.7 103 78-130
Chloroethane ug/kg 47.348.7 97 64-149
Chloroform ug/kg 49.148.7 101 70-134
Chloromethane ug/kg 46.248.7 95 52-150
cis-1,2-Dichloroethene ug/kg 50.348.7 103 70-133
cis-1,3-Dichloropropene ug/kg 52.748.7 108 68-134
Dibromochloromethane ug/kg 53.048.7 109 71-138
Dibromomethane ug/kg 51.148.7 105 74-130
Dichlorodifluoromethane ug/kg 53.148.7 109 40-160
Diisopropyl ether ug/kg 51.348.7 105 69-141
Ethylbenzene ug/kg 51.048.7 105 75-133
Hexachloro-1,3-butadiene ug/kg 53.548.7 110 68-143
Isopropylbenzene (Cumene)ug/kg 52.448.7 108 76-143
m&p-Xylene ug/kg 10197.5 103 75-136
Methyl-tert-butyl ether ug/kg 53.548.7 110 68-144
Methylene Chloride ug/kg 56.348.7 115 45-154
n-Butylbenzene ug/kg 49.848.7 102 72-137
n-Propylbenzene ug/kg 50.248.7 103 76-136
Naphthalene ug/kg 47.048.7 96 68-151
o-Xylene ug/kg 51.948.7 106 76-141
p-Isopropyltoluene ug/kg 49.748.7 102 76-140
sec-Butylbenzene ug/kg 51.048.7 105 79-139
Styrene ug/kg 50.348.7 103 79-137
tert-Butylbenzene ug/kg 46.848.7 96 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2384934LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 47.348.7 97 71-138
Toluene ug/kg 48.948.7 100 74-131
trans-1,2-Dichloroethene ug/kg 56.048.7 115 67-135
trans-1,3-Dichloropropene ug/kg 53.448.7 110 65-146
Trichloroethene ug/kg 56.448.7 116 67-135
Trichlorofluoromethane ug/kg 46.948.7 96 59-144
Vinyl acetate ug/kg 63.397.5 65 40-160
Vinyl chloride ug/kg 52.448.7 108 56-141
Xylene (Total)ug/kg 153146 104 76-137
1,2-Dichloroethane-d4 (S)%96 70-132
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2384936MATRIX SPIKE SAMPLE:
MSSpike
Result
92400796001
1,1,1,2-Tetrachloroethane ug/kg 18.820.4 92 70-130ND
1,1,1-Trichloroethane ug/kg 19.120.4 94 70-130ND
1,1,2,2-Tetrachloroethane ug/kg ND M120.4 0 70-130ND
1,1,2-Trichloroethane ug/kg 16.620.4 81 70-130ND
1,1-Dichloroethane ug/kg 20.420.4 100 70-130ND
1,1-Dichloroethene ug/kg 23.220.4 114 49-180ND
1,1-Dichloropropene ug/kg 18.820.4 92 70-130ND
1,2,3-Trichlorobenzene ug/kg 14.520.4 71 70-130ND
1,2,3-Trichloropropane ug/kg 16.520.4 81 70-130ND
1,2,4-Trichlorobenzene ug/kg 14.0 M120.4 69 70-130ND
1,2,4-Trimethylbenzene ug/kg 16.120.4 79 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 16.620.4 82 70-130ND
1,2-Dibromoethane (EDB)ug/kg 17.620.4 87 70-130ND
1,2-Dichlorobenzene ug/kg 16.920.4 83 70-130ND
1,2-Dichloroethane ug/kg 18.120.4 89 70-130ND
1,2-Dichloropropane ug/kg 17.820.4 88 70-130ND
1,3,5-Trimethylbenzene ug/kg 16.320.4 80 70-130ND
1,3-Dichlorobenzene ug/kg 16.920.4 83 70-130ND
1,3-Dichloropropane ug/kg 18.920.4 93 70-130ND
1,4-Dichlorobenzene ug/kg 17.120.4 84 70-130ND
2,2-Dichloropropane ug/kg 18.220.4 89 70-130ND
2-Butanone (MEK)ug/kg 34.9J40.7 86 70-130ND
2-Chlorotoluene ug/kg 17.220.4 84 70-130ND
2-Hexanone ug/kg 34.2J40.7 84 70-130ND
4-Chlorotoluene ug/kg 17.020.4 84 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 32.2J40.7 79 70-130ND
Acetone ug/kg 45.9J40.7 113 70-130ND
Benzene ug/kg 19.720.4 97 50-166ND
Bromobenzene ug/kg 17.820.4 87 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2384936MATRIX SPIKE SAMPLE:
MSSpike
Result
92400796001
Bromochloromethane ug/kg 19.220.4 94 70-130ND
Bromodichloromethane ug/kg 19.220.4 94 70-130ND
Bromoform ug/kg 18.120.4 89 70-130ND
Bromomethane ug/kg 21.620.4 106 70-130ND
Carbon tetrachloride ug/kg 19.720.4 97 70-130ND
Chlorobenzene ug/kg 18.520.4 91 43-169ND
Chloroethane ug/kg 16.920.4 83 70-130ND
Chloroform ug/kg 19.520.4 96 70-130ND
Chloromethane ug/kg 15.520.4 76 70-130ND
cis-1,2-Dichloroethene ug/kg 19.520.4 96 70-130ND
cis-1,3-Dichloropropene ug/kg 16.820.4 83 70-130ND
Dibromochloromethane ug/kg 18.320.4 90 70-130ND
Dibromomethane ug/kg 18.320.4 90 70-130ND
Dichlorodifluoromethane ug/kg 15.020.4 74 70-130ND
Diisopropyl ether ug/kg 18.320.4 90 70-130ND
Ethylbenzene ug/kg 19.120.4 94 70-130ND
Hexachloro-1,3-butadiene ug/kg 10.1 M120.4 50 70-130ND
Isopropylbenzene (Cumene)ug/kg 18.520.4 91 70-130ND
m&p-Xylene ug/kg 38.240.7 94 70-130ND
Methyl-tert-butyl ether ug/kg 17.420.4 85 70-130ND
Methylene Chloride ug/kg 29.4 M120.4 144 70-130ND
n-Butylbenzene ug/kg 13.7 M120.4 67 70-130ND
n-Propylbenzene ug/kg 17.520.4 86 70-130ND
Naphthalene ug/kg 14.520.4 71 70-130ND
o-Xylene ug/kg 19.320.4 95 70-130ND
p-Isopropyltoluene ug/kg 15.520.4 76 70-130ND
sec-Butylbenzene ug/kg 15.920.4 78 70-130ND
Styrene ug/kg 18.020.4 88 70-130ND
tert-Butylbenzene ug/kg 15.320.4 75 70-130ND
Tetrachloroethene ug/kg 17.620.4 86 70-130ND
Toluene ug/kg 19.320.4 95 52-163ND
trans-1,2-Dichloroethene ug/kg 20.720.4 102 70-130ND
trans-1,3-Dichloropropene ug/kg 16.520.4 81 70-130ND
Trichloroethene ug/kg 35.1 M120.4 172 49-167ND
Trichlorofluoromethane ug/kg 18.620.4 91 70-130ND
Vinyl acetate ug/kg 12.5J M140.7 31 70-130ND
Vinyl chloride ug/kg 20.820.4 102 70-130ND
Xylene (Total)ug/kg 57.561.2 94 70-130ND
1,2-Dichloroethane-d4 (S)%88 70-132
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400708002
2384935SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400708002
2384935SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg 6.7J 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%91 486
4-Bromofluorobenzene (S)%97 399
Toluene-d8 (S)%100 8107
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
432778
EPA 5035A
EPA 8260B
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92400796005, 92400796006, 92400796007, 92400796008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2385166
Associated Lab Samples:92400796005, 92400796006, 92400796007, 92400796008
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.8 09/26/18 14:112.4
1,1,1-Trichloroethane ug/kg ND 5.8 09/26/18 14:112.1
1,1,2,2-Tetrachloroethane ug/kg ND 5.8 09/26/18 14:112.2
1,1,2-Trichloroethane ug/kg ND 5.8 09/26/18 14:112.4
1,1-Dichloroethane ug/kg ND 5.8 09/26/18 14:111.7
1,1-Dichloroethene ug/kg ND 5.8 09/26/18 14:112.1
1,1-Dichloropropene ug/kg ND 5.8 09/26/18 14:111.7
1,2,3-Trichlorobenzene ug/kg ND 5.8 09/26/18 14:112.6
1,2,3-Trichloropropane ug/kg ND 5.8 09/26/18 14:111.9
1,2,4-Trichlorobenzene ug/kg ND 5.8 09/26/18 14:111.9
1,2,4-Trimethylbenzene ug/kg ND 5.8 09/26/18 14:112.3
1,2-Dibromo-3-chloropropane ug/kg ND 5.8 09/26/18 14:114.2
1,2-Dibromoethane (EDB)ug/kg ND 5.8 09/26/18 14:112.1
1,2-Dichlorobenzene ug/kg ND 5.8 09/26/18 14:112.2
1,2-Dichloroethane ug/kg ND 5.8 09/26/18 14:112.6
1,2-Dichloropropane ug/kg ND 5.8 09/26/18 14:112.0
1,3,5-Trimethylbenzene ug/kg ND 5.8 09/26/18 14:112.1
1,3-Dichlorobenzene ug/kg ND 5.8 09/26/18 14:112.3
1,3-Dichloropropane ug/kg ND 5.8 09/26/18 14:112.2
1,4-Dichlorobenzene ug/kg ND 5.8 09/26/18 14:112.0
2,2-Dichloropropane ug/kg ND 5.8 09/26/18 14:112.0
2-Butanone (MEK)ug/kg ND 116 09/26/18 14:113.4
2-Chlorotoluene ug/kg ND 5.8 09/26/18 14:112.0
2-Hexanone ug/kg ND 58.0 09/26/18 14:114.5
4-Chlorotoluene ug/kg ND 5.8 09/26/18 14:112.1
4-Methyl-2-pentanone (MIBK)ug/kg ND 58.0 09/26/18 14:114.3
Acetone ug/kg ND 116 09/26/18 14:1111.6
Benzene ug/kg ND 5.8 09/26/18 14:111.9
Bromobenzene ug/kg ND 5.8 09/26/18 14:112.3
Bromochloromethane ug/kg ND 5.8 09/26/18 14:112.0
Bromodichloromethane ug/kg ND 5.8 09/26/18 14:112.2
Bromoform ug/kg ND 5.8 09/26/18 14:112.7
Bromomethane ug/kg ND 11.6 09/26/18 14:112.9
Carbon tetrachloride ug/kg ND 5.8 09/26/18 14:113.0
Chlorobenzene ug/kg ND 5.8 09/26/18 14:112.2
Chloroethane ug/kg ND 11.6 09/26/18 14:112.8
Chloroform ug/kg ND 5.8 09/26/18 14:111.9
Chloromethane ug/kg ND 11.6 09/26/18 14:112.8
cis-1,2-Dichloroethene ug/kg ND 5.8 09/26/18 14:111.6
cis-1,3-Dichloropropene ug/kg ND 5.8 09/26/18 14:112.1
Dibromochloromethane ug/kg ND 5.8 09/26/18 14:112.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 36 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2385166
Associated Lab Samples:92400796005, 92400796006, 92400796007, 92400796008
Matrix:Solid
AnalyzedMDL
Dibromomethane ug/kg ND 5.8 09/26/18 14:112.9
Dichlorodifluoromethane ug/kg ND 11.6 09/26/18 14:114.2
Diisopropyl ether ug/kg ND 5.8 09/26/18 14:112.0
Ethylbenzene ug/kg ND 5.8 09/26/18 14:112.1
Hexachloro-1,3-butadiene ug/kg ND 5.8 09/26/18 14:112.3
Isopropylbenzene (Cumene)ug/kg ND 5.8 09/26/18 14:112.2
m&p-Xylene ug/kg ND 11.6 09/26/18 14:114.2
Methyl-tert-butyl ether ug/kg ND 5.8 09/26/18 14:111.7
Methylene Chloride ug/kg ND 23.2 09/26/18 14:113.5
n-Butylbenzene ug/kg ND 5.8 09/26/18 14:112.1
n-Propylbenzene ug/kg ND 5.8 09/26/18 14:112.0
Naphthalene ug/kg ND 5.8 09/26/18 14:111.4
o-Xylene ug/kg ND 5.8 09/26/18 14:112.2
p-Isopropyltoluene ug/kg ND 5.8 09/26/18 14:112.0
sec-Butylbenzene ug/kg ND 5.8 09/26/18 14:111.9
Styrene ug/kg ND 5.8 09/26/18 14:112.1
tert-Butylbenzene ug/kg ND 5.8 09/26/18 14:112.3
Tetrachloroethene ug/kg ND 5.8 09/26/18 14:112.0
Toluene ug/kg ND 5.8 09/26/18 14:112.1
trans-1,2-Dichloroethene ug/kg ND 5.8 09/26/18 14:112.2
trans-1,3-Dichloropropene ug/kg ND 5.8 09/26/18 14:111.7
Trichloroethene ug/kg ND 5.8 09/26/18 14:112.4
Trichlorofluoromethane ug/kg ND 5.8 09/26/18 14:112.6
Vinyl acetate ug/kg ND 58.0 09/26/18 14:1110.2
Vinyl chloride ug/kg ND 11.6 09/26/18 14:112.1
Xylene (Total)ug/kg ND 11.6 09/26/18 14:114.2
1,2-Dichloroethane-d4 (S)%94 70-132 09/26/18 14:11
4-Bromofluorobenzene (S)%96 70-130 09/26/18 14:11
Toluene-d8 (S)%100 70-130 09/26/18 14:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2385167LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 62.462.3 100 74-137
1,1,1-Trichloroethane ug/kg 62.062.3 99 67-140
1,1,2,2-Tetrachloroethane ug/kg 61.062.3 98 72-141
1,1,2-Trichloroethane ug/kg 61.962.3 99 78-138
1,1-Dichloroethane ug/kg 64.162.3 103 69-134
1,1-Dichloroethene ug/kg 72.462.3 116 67-138
1,1-Dichloropropene ug/kg 63.662.3 102 69-139
1,2,3-Trichlorobenzene ug/kg 61.962.3 99 70-146
1,2,3-Trichloropropane ug/kg 62.762.3 101 69-144
1,2,4-Trichlorobenzene ug/kg 64.762.3 104 68-148
1,2,4-Trimethylbenzene ug/kg 65.962.3 106 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2385167LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 53.762.3 86 65-140
1,2-Dibromoethane (EDB)ug/kg 61.662.3 99 77-135
1,2-Dichlorobenzene ug/kg 62.162.3 100 77-141
1,2-Dichloroethane ug/kg 64.162.3 103 65-137
1,2-Dichloropropane ug/kg 65.062.3 104 72-136
1,3,5-Trimethylbenzene ug/kg 63.662.3 102 76-133
1,3-Dichlorobenzene ug/kg 62.962.3 101 74-138
1,3-Dichloropropane ug/kg 64.162.3 103 71-139
1,4-Dichlorobenzene ug/kg 61.662.3 99 76-138
2,2-Dichloropropane ug/kg 64.262.3 103 68-137
2-Butanone (MEK)ug/kg 122J125 98 58-147
2-Chlorotoluene ug/kg 62.762.3 101 73-139
2-Hexanone ug/kg 121125 97 62-145
4-Chlorotoluene ug/kg 64.462.3 103 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 123125 99 64-149
Acetone ug/kg 178125 143 53-153
Benzene ug/kg 65.362.3 105 73-135
Bromobenzene ug/kg 61.362.3 98 75-133
Bromochloromethane ug/kg 57.462.3 92 73-134
Bromodichloromethane ug/kg 64.262.3 103 71-135
Bromoform ug/kg 58.562.3 94 66-141
Bromomethane ug/kg 77.462.3 124 53-160
Carbon tetrachloride ug/kg 62.362.3 100 60-145
Chlorobenzene ug/kg 64.262.3 103 78-130
Chloroethane ug/kg 68.062.3 109 64-149
Chloroform ug/kg 59.962.3 96 70-134
Chloromethane ug/kg 57.462.3 92 52-150
cis-1,2-Dichloroethene ug/kg 66.962.3 107 70-133
cis-1,3-Dichloropropene ug/kg 63.462.3 102 68-134
Dibromochloromethane ug/kg 61.362.3 98 71-138
Dibromomethane ug/kg 63.762.3 102 74-130
Dichlorodifluoromethane ug/kg 63.062.3 101 40-160
Diisopropyl ether ug/kg 64.462.3 103 69-141
Ethylbenzene ug/kg 65.362.3 105 75-133
Hexachloro-1,3-butadiene ug/kg 62.162.3 100 68-143
Isopropylbenzene (Cumene)ug/kg 66.762.3 107 76-143
m&p-Xylene ug/kg 133125 107 75-136
Methyl-tert-butyl ether ug/kg 60.362.3 97 68-144
Methylene Chloride ug/kg 67.862.3 109 45-154
n-Butylbenzene ug/kg 67.462.3 108 72-137
n-Propylbenzene ug/kg 66.062.3 106 76-136
Naphthalene ug/kg 67.862.3 109 68-151
o-Xylene ug/kg 66.062.3 106 76-141
p-Isopropyltoluene ug/kg 64.762.3 104 76-140
sec-Butylbenzene ug/kg 65.362.3 105 79-139
Styrene ug/kg 62.762.3 101 79-137
tert-Butylbenzene ug/kg 57.262.3 92 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2385167LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 57.662.3 92 71-138
Toluene ug/kg 62.462.3 100 74-131
trans-1,2-Dichloroethene ug/kg 69.562.3 112 67-135
trans-1,3-Dichloropropene ug/kg 62.462.3 100 65-146
Trichloroethene ug/kg 66.362.3 106 67-135
Trichlorofluoromethane ug/kg 63.962.3 102 59-144
Vinyl acetate ug/kg 98.5125 79 40-160
Vinyl chloride ug/kg 72.462.3 116 56-141
Xylene (Total)ug/kg 199187 106 76-137
1,2-Dichloroethane-d4 (S)%92 70-132
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2385169MATRIX SPIKE SAMPLE:
MSSpike
Result
92400486007
1,1,1,2-Tetrachloroethane ug/kg 21.622.5 96 70-130ND
1,1,1-Trichloroethane ug/kg 27.622.5 123 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 22.622.5 101 70-130ND
1,1,2-Trichloroethane ug/kg 23.822.5 106 70-130ND
1,1-Dichloroethane ug/kg 28.922.5 129 70-130ND
1,1-Dichloroethene ug/kg 33.222.5 148 49-180ND
1,1-Dichloropropene ug/kg 28.922.5 129 70-130ND
1,2,3-Trichlorobenzene ug/kg 20.022.5 89 70-130ND
1,2,3-Trichloropropane ug/kg 22.322.5 99 70-130ND
1,2,4-Trichlorobenzene ug/kg 20.522.5 91 70-130ND
1,2,4-Trimethylbenzene ug/kg 24.422.5 109 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 22.322.5 99 70-130ND
1,2-Dibromoethane (EDB)ug/kg 21.922.5 98 70-130ND
1,2-Dichlorobenzene ug/kg 23.122.5 103 70-130ND
1,2-Dichloroethane ug/kg 29.322.5 130 70-130ND
1,2-Dichloropropane ug/kg 24.222.5 108 70-130ND
1,3,5-Trimethylbenzene ug/kg 23.322.5 104 70-130ND
1,3-Dichlorobenzene ug/kg 22.322.5 99 70-130ND
1,3-Dichloropropane ug/kg 23.822.5 106 70-130ND
1,4-Dichlorobenzene ug/kg 22.522.5 100 70-130ND
2,2-Dichloropropane ug/kg 25.822.5 115 70-130ND
2-Butanone (MEK)ug/kg 66.7J44.9 121 70-130ND
2-Chlorotoluene ug/kg 23.922.5 106 70-130ND
2-Hexanone ug/kg 52.3J44.9 116 70-130ND
4-Chlorotoluene ug/kg 23.622.5 105 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 53.6J44.9 108 70-130ND
Acetone ug/kg 14344.9 98 70-130ND
Benzene ug/kg 24.822.5 111 50-166ND
Bromobenzene ug/kg 24.022.5 107 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2385169MATRIX SPIKE SAMPLE:
MSSpike
Result
92400486007
Bromochloromethane ug/kg 28.122.5 125 70-130ND
Bromodichloromethane ug/kg 23.122.5 103 70-130ND
Bromoform ug/kg 20.322.5 91 70-130ND
Bromomethane ug/kg 31.0 M122.5 138 70-130ND
Carbon tetrachloride ug/kg 22.622.5 101 70-130ND
Chlorobenzene ug/kg 22.622.5 101 43-169ND
Chloroethane ug/kg 32.2 M122.5 143 70-130ND
Chloroform ug/kg 28.422.5 126 70-130ND
Chloromethane ug/kg 27.822.5 124 70-130ND
cis-1,2-Dichloroethene ug/kg 28.122.5 125 70-130ND
cis-1,3-Dichloropropene ug/kg 22.722.5 101 70-130ND
Dibromochloromethane ug/kg 20.922.5 93 70-130ND
Dibromomethane ug/kg 23.722.5 105 70-130ND
Dichlorodifluoromethane ug/kg 28.522.5 127 70-130ND
Diisopropyl ether ug/kg 31.7 M122.5 141 70-130ND
Ethylbenzene ug/kg 22.522.5 100 70-130ND
Hexachloro-1,3-butadiene ug/kg 15.622.5 70 70-130ND
Isopropylbenzene (Cumene)ug/kg 22.322.5 99 70-130ND
m&p-Xylene ug/kg 45.344.9 101 70-130ND
Methyl-tert-butyl ether ug/kg 28.222.5 126 70-130ND
Methylene Chloride ug/kg 56.9 M122.5 169 70-130ND
n-Butylbenzene ug/kg 22.222.5 99 70-130ND
n-Propylbenzene ug/kg 24.222.5 108 70-130ND
Naphthalene ug/kg 27.322.5 110 70-130ND
o-Xylene ug/kg 22.622.5 101 70-130ND
p-Isopropyltoluene ug/kg 22.622.5 101 70-130ND
sec-Butylbenzene ug/kg 22.622.5 100 70-130ND
Styrene ug/kg 21.522.5 96 70-130ND
tert-Butylbenzene ug/kg 20.722.5 92 70-130ND
Tetrachloroethene ug/kg 19.922.5 88 70-130ND
Toluene ug/kg 24.122.5 103 52-163ND
trans-1,2-Dichloroethene ug/kg 32.1 M122.5 143 70-130ND
trans-1,3-Dichloropropene ug/kg 22.522.5 100 70-130ND
Trichloroethene ug/kg 24.122.5 107 49-167ND
Trichlorofluoromethane ug/kg 28.522.5 127 70-130ND
Vinyl acetate ug/kg 23.8J M144.9 53 70-130ND
Vinyl chloride ug/kg 34.7 M122.5 155 70-130ND
Xylene (Total)ug/kg 67.967.4 101 70-130ND
1,2-Dichloroethane-d4 (S)%115 70-132
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400486006
2385168SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg 3.6J 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg 18.8J 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400486006
2385168SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg 16.0J 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg 1.5J 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%103 2105
4-Bromofluorobenzene (S)%96 197
Toluene-d8 (S)%99 099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 42 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
432770
EPA 3546
EPA 8270D by SIM
8270 MSSV PAH by SIM
Associated Lab Samples:92400796001, 92400796002, 92400796003, 92400796004, 92400796005, 92400796006, 92400796007,
92400796008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2385110
Associated Lab Samples:92400796001, 92400796002, 92400796003, 92400796004, 92400796005, 92400796006, 92400796007,
92400796008
Matrix:Solid
AnalyzedMDL
1-Methylnaphthalene ug/kg ND 10.1 09/27/18 14:111.2
2-Methylnaphthalene ug/kg ND 10.1 09/27/18 14:111.1
Acenaphthene ug/kg ND 10.1 09/27/18 14:111.5
Acenaphthylene ug/kg ND 10.1 09/27/18 14:111.3
Anthracene ug/kg ND 10.1 09/27/18 14:111.4
Benzo(a)anthracene ug/kg ND 10.1 09/27/18 14:110.71
Benzo(a)pyrene ug/kg ND 10.1 09/27/18 14:111.1
Benzo(b)fluoranthene ug/kg 0.96J 10.1 09/27/18 14:110.67
Benzo(g,h,i)perylene ug/kg ND 10.1 09/27/18 14:112.6
Benzo(k)fluoranthene ug/kg ND 10.1 09/27/18 14:111.5
Chrysene ug/kg ND 10.1 09/27/18 14:111.8
Dibenz(a,h)anthracene ug/kg ND 10.1 09/27/18 14:111.8
Fluoranthene ug/kg ND 10.1 09/27/18 14:110.84
Fluorene ug/kg ND 10.1 09/27/18 14:111.6
Indeno(1,2,3-cd)pyrene ug/kg ND 10.1 09/27/18 14:112.8
Naphthalene ug/kg ND 10.1 09/27/18 14:112.3
Phenanthrene ug/kg ND 10.1 09/27/18 14:111.5
Pyrene ug/kg ND 10.1 09/27/18 14:111.8
2-Fluorobiphenyl (S)%51 10-110 09/27/18 14:11
Nitrobenzene-d5 (S)%54 10-128 09/27/18 14:11
Terphenyl-d14 (S)%60 39-119 09/27/18 14:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2385111LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/kg 26.333.3 79 44-130
2-Methylnaphthalene ug/kg 27.833.3 83 41-134
Acenaphthene ug/kg 29.433.3 88 52-123
Acenaphthylene ug/kg 26.533.3 79 49-116
Anthracene ug/kg 29.333.3 88 41-133
Benzo(a)anthracene ug/kg 29.233.3 88 56-130
Benzo(a)pyrene ug/kg 28.233.3 85 51-136
Benzo(b)fluoranthene ug/kg 28.733.3 86 37-149
Benzo(g,h,i)perylene ug/kg 26.333.3 79 39-127
Benzo(k)fluoranthene ug/kg 29.333.3 88 45-139
Chrysene ug/kg 30.133.3 90 59-127
Dibenz(a,h)anthracene ug/kg 28.833.3 86 37-139
Fluoranthene ug/kg 31.033.3 93 53-132
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2385111LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 26.033.3 78 45-127
Indeno(1,2,3-cd)pyrene ug/kg 29.433.3 88 35-145
Naphthalene ug/kg 27.933.3 84 45-123
Phenanthrene ug/kg 30.433.3 91 50-125
Pyrene ug/kg 31.033.3 93 52-132
2-Fluorobiphenyl (S)%87 10-110
Nitrobenzene-d5 (S)%92 10-128
Terphenyl-d14 (S)%81 39-119
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2385112MATRIX SPIKE SAMPLE:
MSSpike
Result
92400789001
1-Methylnaphthalene ug/kg 25.240.4 55 50-1503.0J
2-Methylnaphthalene ug/kg 26.140.4 59 50-1502.2J
Acenaphthene ug/kg 31.140.4 65 50-1504.6J
Acenaphthylene ug/kg 24.840.4 56 50-1502.1J
Anthracene ug/kg 45.840.4 75 50-15015.6
Benzo(a)anthracene ug/kg 192 M140.4 156 50-150129
Benzo(a)pyrene ug/kg 206 M140.4 194 50-150128
Benzo(b)fluoranthene ug/kg 324 M140.4 280 50-150211
Benzo(g,h,i)perylene ug/kg 10640.4 67 50-15079.1
Benzo(k)fluoranthene ug/kg 102 M140.4 28 50-15090.3
Chrysene ug/kg 220 M140.4 173 50-150150
Dibenz(a,h)anthracene ug/kg 47.240.4 55 50-15025.1
Fluoranthene ug/kg 25040.4 88 50-150214
Fluorene ug/kg 26.040.4 57 50-1502.9J
Indeno(1,2,3-cd)pyrene ug/kg 11040.4 81 50-15077.6
Naphthalene ug/kg 25.340.4 56 50-1502.8J
Phenanthrene ug/kg 92.240.4 69 50-15064.2
Pyrene ug/kg 24840.4 144 50-150190
2-Fluorobiphenyl (S)%62 10-110
Nitrobenzene-d5 (S)%62 10-128
Terphenyl-d14 (S)%61 39-119
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400789002
2385113SAMPLE DUPLICATE:
1-Methylnaphthalene ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg 1.3J 301.5J
Benzo(a)pyrene ug/kg ND 301.5J
REPORT OF LABORATORY ANALYSIS
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Page 44 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400789002
2385113SAMPLE DUPLICATE:
Benzo(b)fluoranthene ug/kg 1.9J 302.1J
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Chrysene ug/kg 2.2J 302.6J
Dibenz(a,h)anthracene ug/kg ND 30ND
Fluoranthene ug/kg 1.2J 301.4J
Fluorene ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2-Fluorobiphenyl (S)%69 370
Nitrobenzene-d5 (S)%70 069
Terphenyl-d14 (S)%70 372
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
432644
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92400796001, 92400796002, 92400796003, 92400796004, 92400796005, 92400796006, 92400796007
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400798001
2384677SAMPLE DUPLICATE:
Percent Moisture %17.0 1 2516.8
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400796007
2384678SAMPLE DUPLICATE:
Percent Moisture %18.2 2 2517.9
REPORT OF LABORATORY ANALYSIS
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Page 46 of 52
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
432650
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92400796008
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400787001
2384692SAMPLE DUPLICATE:
Percent Moisture %28.3 0 2528.2
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400799004
2384693SAMPLE DUPLICATE:
Percent Moisture %13.8 1 2514.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 09:04 AM
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Could not achieve adequate chromatographic separation of benzo(a)anthracene and chrysene. Result should be
considered a sum of the isomers.1g
Could not achieve adequate chromatographic separation of benzo(b)fluoranthene and benzo(k)fluoranthene. Result
should be considered a sum of the isomers.2g
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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Page 48 of 52
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92400796
Former Maintenance Shop Area
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92400796001 432770 432998MSA-SB001 (0'-1')EPA 3546 EPA 8270D by SIM
92400796002 432770 432998MSA-SB001 (4'-5')EPA 3546 EPA 8270D by SIM
92400796003 432770 432998MSA-SB002 (0'-1')EPA 3546 EPA 8270D by SIM
92400796004 432770 432998MSA-SB002 (4'-5')EPA 3546 EPA 8270D by SIM
92400796005 432770 432998MSA-SB003 (0'-1')EPA 3546 EPA 8270D by SIM
92400796006 432770 432998MSA-SB003 (4'-5')EPA 3546 EPA 8270D by SIM
92400796007 432770 432998MSA-SB004 (0'-1')EPA 3546 EPA 8270D by SIM
92400796008 432770 432998MSA-SB004 (4'-5')EPA 3546 EPA 8270D by SIM
92400796001 432748 432762MSA-SB001 (0'-1')EPA 5035A EPA 8260B
92400796002 432748 432762MSA-SB001 (4'-5')EPA 5035A EPA 8260B
92400796003 432748 432762MSA-SB002 (0'-1')EPA 5035A EPA 8260B
92400796004 432748 432762MSA-SB002 (4'-5')EPA 5035A EPA 8260B
92400796005 432778 432796MSA-SB003 (0'-1')EPA 5035A EPA 8260B
92400796006 432778 432796MSA-SB003 (4'-5')EPA 5035A EPA 8260B
92400796007 432778 432796MSA-SB004 (0'-1')EPA 5035A EPA 8260B
92400796008 432778 432796MSA-SB004 (4'-5')EPA 5035A EPA 8260B
92400796001 432644MSA-SB001 (0'-1')ASTM D2974-87
92400796002 432644MSA-SB001 (4'-5')ASTM D2974-87
92400796003 432644MSA-SB002 (0'-1')ASTM D2974-87
92400796004 432644MSA-SB002 (4'-5')ASTM D2974-87
92400796005 432644MSA-SB003 (0'-1')ASTM D2974-87
92400796006 432644MSA-SB003 (4'-5')ASTM D2974-87
92400796007 432644MSA-SB004 (0'-1')ASTM D2974-87
92400796008 432650MSA-SB004 (4'-5')ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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Page 49 of 52
Page 50 of 52
Page 51 of 52
Page 52 of 52
#=CL#
November 12, 2018
LIMS USE: FR - MICHAEL WORDEN
LIMS OBJECT ID: 92401224
92401224
Project:
Pace Project No.:
RE:
Michael W. Worden
Environeering, Inc.
16100 Cairnway
Suite 320
Houston, TX 77084
Frmr Potline/Bath Crushing
Dear Michael Worden:
Enclosed are the analytical results for sample(s) received by the laboratory on September 26, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
This revision was issued on 11/12/18 to report J-flagged results to the MDL, per client request.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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Page 1 of 83
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Lab ID Sample ID Matrix Date Collected Date Received
92401224001 PBC-SB001 (0'-1')Solid 09/25/18 09:05 09/26/18 15:25
92401224002 PBC-SB001 (4'-5')Solid 09/25/18 09:10 09/26/18 15:25
92401224003 PBC-SB002 (0'-1')Solid 09/25/18 09:20 09/26/18 15:25
92401224004 PBC-SB002 (4'-5')Solid 09/25/18 09:25 09/26/18 15:25
92401224005 PBC-SB003 (0'-1')Solid 09/25/18 09:40 09/26/18 15:25
92401224006 PBC-SB003 (4'-5')Solid 09/25/18 09:45 09/26/18 15:25
92401224007 PBC-SB004 (0'-1')Solid 09/25/18 10:40 09/26/18 15:25
92401224008 PBC-SB004 (4'-5')Solid 09/25/18 10:45 09/26/18 15:25
92401224009 PBC-SB005 (0'-1')Solid 09/25/18 11:45 09/26/18 15:25
92401224010 PBC-SB005 (4'-5')Solid 09/25/18 11:50 09/26/18 15:25
92401224011 PBC-SB006 (0'-1')Solid 09/25/18 12:05 09/26/18 15:25
92401224012 PBC-SB006 (4'-5')Solid 09/25/18 12:10 09/26/18 15:25
92401224013 PBC-SB007 (0'-1')Solid 09/25/18 12:55 09/26/18 15:25
92401224014 PBC-SB007 (4'-5')Solid 09/25/18 13:00 09/26/18 15:25
92401224015 PBC-SB008 (0'-1')Solid 09/25/18 14:25 09/26/18 15:25
92401224016 PBC-SB008 (4'-5')Solid 09/25/18 14:30 09/26/18 15:25
92401224017 PBC-SB009 (0'-1')Solid 09/25/18 14:45 09/26/18 15:25
92401224018 PBC-SB009 (4'-5')Solid 09/25/18 14:50 09/26/18 15:25
92401224019 PBC-SB010 (0'-1')Solid 09/25/18 15:00 09/26/18 15:25
92401224020 PBC-SB010 (4'-5')Solid 09/25/18 15:05 09/26/18 15:25
92401224021 PBC-SB011 (0'-1')Solid 09/25/18 15:30 09/26/18 15:25
92401224022 PBC-SB011 (2'-3')Solid 09/25/18 15:35 09/26/18 15:25
92401224023 PBC-SB012 (0'-1')Solid 09/25/18 16:10 09/26/18 15:25
92401224024 PBC-SB012 (4'-5')Solid 09/25/18 16:15 09/26/18 15:25
92401224025 PBC-SB013 (0'-1')Solid 09/25/18 16:30 09/26/18 15:25
92401224026 PBC-SB013 (4'-5')Solid 09/25/18 16:35 09/26/18 15:25
92401224027 PBC-SB014 (0'-1')Solid 09/26/18 08:15 09/26/18 15:25
92401224028 PBC-SB014 (4'-5')Solid 09/26/18 08:20 09/26/18 15:25
92401224029 PBC-SB015 (0'-1')Solid 09/26/18 08:50 09/26/18 15:25
92401224030 PBC-SB015 (4'-5')Solid 09/26/18 08:55 09/26/18 15:25
92401224031 PBC-SB016 (0'-1')Solid 09/26/18 09:40 09/26/18 15:25
92401224032 PBC-SB016 (4'-5')Solid 09/26/18 09:45 09/26/18 15:25
92401224033 PBC-SB017 (0'-1')Solid 09/26/18 10:35 09/26/18 15:25
92401224034 PBC-SB017 (4'-5')Solid 09/26/18 10:40 09/26/18 15:25
92401224035 ESW-EB001 Water 09/25/18 17:00 09/26/18 15:25
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 3 of 83
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92401224001 PBC-SB001 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224002 PBC-SB001 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224003 PBC-SB002 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224004 PBC-SB002 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224005 PBC-SB003 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224006 PBC-SB003 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224007 PBC-SB004 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224008 PBC-SB004 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224009 PBC-SB005 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224010 PBC-SB005 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 4 of 83
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224011 PBC-SB006 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224012 PBC-SB006 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224013 PBC-SB007 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224014 PBC-SB007 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224015 PBC-SB008 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224016 PBC-SB008 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224017 PBC-SB009 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224018 PBC-SB009 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224019 PBC-SB010 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 5 of 83
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224020 PBC-SB010 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224021 PBC-SB011 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224022 PBC-SB011 (2'-3')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224023 PBC-SB012 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224024 PBC-SB012 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224025 PBC-SB013 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224026 PBC-SB013 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224027 PBC-SB014 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224028 PBC-SB014 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 83
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 9056 1 PASI-OSEW
92401224029 PBC-SB015 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224030 PBC-SB015 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224031 PBC-SB016 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224032 PBC-SB016 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224033 PBC-SB017 (0'-1')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224034 PBC-SB017 (4'-5')EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92401224035 ESW-EB001 EPA 8082A 8 PASI-CSEM
EPA 8270D by SIM 21 PASI-CPKS
EPA 8260B 71 PASI-CSAS
EPA 9012B 1 PASI-ADMN
EPA 9056A 1 PASI-ACDC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB001 (0'-1')Lab ID:92401224001 Collected:09/25/18 09:05 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/02/18 19:49 83-32-909/28/18 16:1912.1 1.8 1
Acenaphthylene ND ug/kg 10/02/18 19:49 208-96-809/28/18 16:1912.1 1.6 1
Anthracene 2.5J ug/kg 10/02/18 19:49 120-12-709/28/18 16:1912.1 1.7 1
Benzo(a)anthracene 32.8 ug/kg 10/02/18 19:49 56-55-309/28/18 16:1912.1 0.86 1
Benzo(a)pyrene 50.1 ug/kg 10/02/18 19:49 50-32-809/28/18 16:1912.1 1.3 1
Benzo(b)fluoranthene 94.8 ug/kg 10/02/18 19:49 205-99-209/28/18 16:1912.1 0.81 1
Benzo(g,h,i)perylene 59.4 ug/kg 10/02/18 19:49 191-24-2 M109/28/18 16:1912.1 3.1 1
Benzo(k)fluoranthene 31.9 ug/kg 10/02/18 19:49 207-08-909/28/18 16:1912.1 1.8 1
Chrysene 37.5 ug/kg 10/02/18 19:49 218-01-909/28/18 16:1912.1 2.2 1
Dibenz(a,h)anthracene 4.7J ug/kg 10/02/18 19:49 53-70-309/28/18 16:1912.1 2.2 1
Fluoranthene 38.2 ug/kg 10/02/18 19:49 206-44-0 M109/28/18 16:1912.1 1.0 1
Fluorene ND ug/kg 10/02/18 19:49 86-73-709/28/18 16:1912.1 1.9 1
Indeno(1,2,3-cd)pyrene 52.6 ug/kg 10/02/18 19:49 193-39-509/28/18 16:1912.1 3.4 1
1-Methylnaphthalene 2.0J ug/kg 10/02/18 19:49 90-12-009/28/18 16:1912.1 1.4 1
2-Methylnaphthalene 3.1J ug/kg 10/02/18 19:49 91-57-609/28/18 16:1912.1 1.3 1
Naphthalene 2.8J ug/kg 10/02/18 19:49 91-20-309/28/18 16:1912.1 2.8 1
Phenanthrene 12.7 ug/kg 10/02/18 19:49 85-01-809/28/18 16:1912.1 1.8 1
Pyrene 35.5 ug/kg 10/02/18 19:49 129-00-009/28/18 16:1912.1 2.2 1
Surrogates
Nitrobenzene-d5 (S)75 %10/02/18 19:49 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)68 %10/02/18 19:49 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)81 %10/02/18 19:49 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.5 %09/27/18 18:210.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 15:47 57-12-5 M1,R110/04/18 15:150.30 0.17 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 218 mg/kg 10/03/18 13:41 16984-48-8 M610/02/18 09:0059.6 29.8 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB001 (4'-5')Lab ID:92401224002 Collected:09/25/18 09:10 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/02/18 20:31 83-32-909/28/18 16:1912.2 1.8 1
Acenaphthylene ND ug/kg 10/02/18 20:31 208-96-809/28/18 16:1912.2 1.6 1
Anthracene ND ug/kg 10/02/18 20:31 120-12-709/28/18 16:1912.2 1.7 1
Benzo(a)anthracene ND ug/kg 10/02/18 20:31 56-55-309/28/18 16:1912.2 0.87 1
Benzo(a)pyrene ND ug/kg 10/02/18 20:31 50-32-809/28/18 16:1912.2 1.3 1
Benzo(b)fluoranthene ND ug/kg 10/02/18 20:31 205-99-209/28/18 16:1912.2 0.82 1
Benzo(g,h,i)perylene ND ug/kg 10/02/18 20:31 191-24-209/28/18 16:1912.2 3.2 1
Benzo(k)fluoranthene ND ug/kg 10/02/18 20:31 207-08-909/28/18 16:1912.2 1.8 1
Chrysene ND ug/kg 10/02/18 20:31 218-01-909/28/18 16:1912.2 2.2 1
Dibenz(a,h)anthracene ND ug/kg 10/02/18 20:31 53-70-309/28/18 16:1912.2 2.2 1
Fluoranthene ND ug/kg 10/02/18 20:31 206-44-009/28/18 16:1912.2 1.0 1
Fluorene ND ug/kg 10/02/18 20:31 86-73-709/28/18 16:1912.2 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/02/18 20:31 193-39-509/28/18 16:1912.2 3.4 1
1-Methylnaphthalene ND ug/kg 10/02/18 20:31 90-12-009/28/18 16:1912.2 1.5 1
2-Methylnaphthalene ND ug/kg 10/02/18 20:31 91-57-609/28/18 16:1912.2 1.3 1
Naphthalene ND ug/kg 10/02/18 20:31 91-20-309/28/18 16:1912.2 2.8 1
Phenanthrene ND ug/kg 10/02/18 20:31 85-01-809/28/18 16:1912.2 1.8 1
Pyrene ND ug/kg 10/02/18 20:31 129-00-009/28/18 16:1912.2 2.2 1
Surrogates
Nitrobenzene-d5 (S)84 %10/02/18 20:31 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)77 %10/02/18 20:31 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)84 %10/02/18 20:31 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 18.3 %09/27/18 17:230.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 15:50 57-12-510/04/18 15:150.31 0.18 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride ND mg/kg 10/03/18 14:47 16984-48-810/02/18 09:006.1 3.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB002 (0'-1')Lab ID:92401224003 Collected:09/25/18 09:20 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 3.1J ug/kg 10/02/18 21:13 83-32-909/28/18 16:1912.5 1.9 1
Acenaphthylene 2.2J ug/kg 10/02/18 21:13 208-96-809/28/18 16:1912.5 1.6 1
Anthracene 10.3J ug/kg 10/02/18 21:13 120-12-709/28/18 16:1912.5 1.8 1
Benzo(a)anthracene 64.9 ug/kg 10/02/18 21:13 56-55-309/28/18 16:1912.5 0.89 1
Benzo(a)pyrene 54.9 ug/kg 10/02/18 21:13 50-32-809/28/18 16:1912.5 1.4 1
Benzo(b)fluoranthene 121 ug/kg 10/02/18 21:13 205-99-209/28/18 16:1912.5 0.84 1
Benzo(g,h,i)perylene 47.4 ug/kg 10/02/18 21:13 191-24-209/28/18 16:1912.5 3.3 1
Benzo(k)fluoranthene 37.6 ug/kg 10/02/18 21:13 207-08-909/28/18 16:1912.5 1.9 1
Chrysene 77.4 ug/kg 10/02/18 21:13 218-01-909/28/18 16:1912.5 2.3 1
Dibenz(a,h)anthracene 3.7J ug/kg 10/02/18 21:13 53-70-309/28/18 16:1912.5 2.3 1
Fluoranthene 92.3 ug/kg 10/02/18 21:13 206-44-009/28/18 16:1912.5 1.0 1
Fluorene 3.0J ug/kg 10/02/18 21:13 86-73-709/28/18 16:1912.5 2.0 1
Indeno(1,2,3-cd)pyrene 43.0 ug/kg 10/02/18 21:13 193-39-509/28/18 16:1912.5 3.5 1
1-Methylnaphthalene 11.4J ug/kg 10/02/18 21:13 90-12-009/28/18 16:1912.5 1.5 1
2-Methylnaphthalene 10.5J ug/kg 10/02/18 21:13 91-57-609/28/18 16:1912.5 1.4 1
Naphthalene 9.0J ug/kg 10/02/18 21:13 91-20-309/28/18 16:1912.5 2.9 1
Phenanthrene 52.4 ug/kg 10/02/18 21:13 85-01-809/28/18 16:1912.5 1.9 1
Pyrene 76.1 ug/kg 10/02/18 21:13 129-00-009/28/18 16:1912.5 2.3 1
Surrogates
Nitrobenzene-d5 (S)85 %10/02/18 21:13 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)80 %10/02/18 21:13 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)90 %10/02/18 21:13 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.8 %09/27/18 17:230.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 15:51 57-12-510/04/18 15:150.33 0.18 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride ND mg/kg 10/03/18 15:09 16984-48-810/02/18 09:0063.1 31.6 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB002 (4'-5')Lab ID:92401224004 Collected:09/25/18 09:25 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/02/18 21:34 83-32-909/28/18 16:1912.5 1.9 1
Acenaphthylene ND ug/kg 10/02/18 21:34 208-96-809/28/18 16:1912.5 1.6 1
Anthracene ND ug/kg 10/02/18 21:34 120-12-709/28/18 16:1912.5 1.8 1
Benzo(a)anthracene 2.9J ug/kg 10/02/18 21:34 56-55-309/28/18 16:1912.5 0.89 1
Benzo(a)pyrene ND ug/kg 10/02/18 21:34 50-32-809/28/18 16:1912.5 1.4 1
Benzo(b)fluoranthene 1.0J ug/kg 10/02/18 21:34 205-99-209/28/18 16:1912.5 0.84 1
Benzo(g,h,i)perylene ND ug/kg 10/02/18 21:34 191-24-209/28/18 16:1912.5 3.3 1
Benzo(k)fluoranthene ND ug/kg 10/02/18 21:34 207-08-909/28/18 16:1912.5 1.9 1
Chrysene 3.4J ug/kg 10/02/18 21:34 218-01-909/28/18 16:1912.5 2.3 1
Dibenz(a,h)anthracene ND ug/kg 10/02/18 21:34 53-70-309/28/18 16:1912.5 2.3 1
Fluoranthene ND ug/kg 10/02/18 21:34 206-44-009/28/18 16:1912.5 1.0 1
Fluorene ND ug/kg 10/02/18 21:34 86-73-709/28/18 16:1912.5 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/02/18 21:34 193-39-509/28/18 16:1912.5 3.5 1
1-Methylnaphthalene ND ug/kg 10/02/18 21:34 90-12-009/28/18 16:1912.5 1.5 1
2-Methylnaphthalene ND ug/kg 10/02/18 21:34 91-57-609/28/18 16:1912.5 1.4 1
Naphthalene ND ug/kg 10/02/18 21:34 91-20-309/28/18 16:1912.5 2.9 1
Phenanthrene ND ug/kg 10/02/18 21:34 85-01-809/28/18 16:1912.5 1.9 1
Pyrene ND ug/kg 10/02/18 21:34 129-00-009/28/18 16:1912.5 2.3 1
Surrogates
Nitrobenzene-d5 (S)81 %10/02/18 21:34 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)73 %10/02/18 21:34 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)80 %10/02/18 21:34 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.2 %09/27/18 17:230.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 15:52 57-12-510/04/18 15:150.30 0.17 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride ND mg/kg 10/03/18 15:31 16984-48-810/02/18 09:006.2 3.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB003 (0'-1')Lab ID:92401224005 Collected:09/25/18 09:40 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/02/18 21:55 83-32-909/28/18 16:1912.5 1.9 1
Acenaphthylene ND ug/kg 10/02/18 21:55 208-96-809/28/18 16:1912.5 1.6 1
Anthracene ND ug/kg 10/02/18 21:55 120-12-709/28/18 16:1912.5 1.8 1
Benzo(a)anthracene 1.7J ug/kg 10/02/18 21:55 56-55-309/28/18 16:1912.5 0.89 1
Benzo(a)pyrene 1.6J ug/kg 10/02/18 21:55 50-32-809/28/18 16:1912.5 1.4 1
Benzo(b)fluoranthene 2.9J ug/kg 10/02/18 21:55 205-99-209/28/18 16:1912.5 0.84 1
Benzo(g,h,i)perylene ND ug/kg 10/02/18 21:55 191-24-209/28/18 16:1912.5 3.3 1
Benzo(k)fluoranthene ND ug/kg 10/02/18 21:55 207-08-909/28/18 16:1912.5 1.9 1
Chrysene ND ug/kg 10/02/18 21:55 218-01-909/28/18 16:1912.5 2.3 1
Dibenz(a,h)anthracene ND ug/kg 10/02/18 21:55 53-70-309/28/18 16:1912.5 2.3 1
Fluoranthene 3.1J ug/kg 10/02/18 21:55 206-44-009/28/18 16:1912.5 1.0 1
Fluorene ND ug/kg 10/02/18 21:55 86-73-709/28/18 16:1912.5 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/02/18 21:55 193-39-509/28/18 16:1912.5 3.5 1
1-Methylnaphthalene ND ug/kg 10/02/18 21:55 90-12-009/28/18 16:1912.5 1.5 1
2-Methylnaphthalene ND ug/kg 10/02/18 21:55 91-57-609/28/18 16:1912.5 1.4 1
Naphthalene ND ug/kg 10/02/18 21:55 91-20-309/28/18 16:1912.5 2.9 1
Phenanthrene ND ug/kg 10/02/18 21:55 85-01-809/28/18 16:1912.5 1.9 1
Pyrene 2.9J ug/kg 10/02/18 21:55 129-00-009/28/18 16:1912.5 2.3 1
Surrogates
Nitrobenzene-d5 (S)73 %10/02/18 21:55 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)70 %10/02/18 21:55 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)75 %10/02/18 21:55 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.8 %09/27/18 17:230.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide 0.31J mg/kg 10/05/18 15:53 57-12-510/04/18 15:150.32 0.18 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 33.1 mg/kg 10/03/18 15:53 16984-48-810/02/18 09:006.2 3.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB003 (4'-5')Lab ID:92401224006 Collected:09/25/18 09:45 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 9.6J ug/kg 10/03/18 01:05 83-32-909/28/18 16:1912.3 1.8 1
Acenaphthylene 8.2J ug/kg 10/03/18 01:05 208-96-809/28/18 16:1912.3 1.6 1
Anthracene 14.6 ug/kg 10/03/18 01:05 120-12-709/28/18 16:1912.3 1.7 1
Benzo(a)anthracene 49.2 ug/kg 10/03/18 01:05 56-55-309/28/18 16:1912.3 0.87 1
Benzo(a)pyrene 50.2 ug/kg 10/03/18 01:05 50-32-809/28/18 16:1912.3 1.4 1
Benzo(b)fluoranthene 73.9 ug/kg 10/03/18 01:05 205-99-209/28/18 16:1912.3 0.82 1
Benzo(g,h,i)perylene 27.5 ug/kg 10/03/18 01:05 191-24-209/28/18 16:1912.3 3.2 1
Benzo(k)fluoranthene 23.7 ug/kg 10/03/18 01:05 207-08-909/28/18 16:1912.3 1.8 1
Chrysene 54.1 ug/kg 10/03/18 01:05 218-01-909/28/18 16:1912.3 2.2 1
Dibenz(a,h)anthracene 8.7J ug/kg 10/03/18 01:05 53-70-309/28/18 16:1912.3 2.2 1
Fluoranthene 84.0 ug/kg 10/03/18 01:05 206-44-009/28/18 16:1912.3 1.0 1
Fluorene 11.1J ug/kg 10/03/18 01:05 86-73-709/28/18 16:1912.3 2.0 1
Indeno(1,2,3-cd)pyrene 24.5 ug/kg 10/03/18 01:05 193-39-509/28/18 16:1912.3 3.4 1
1-Methylnaphthalene 19.7 ug/kg 10/03/18 01:05 90-12-009/28/18 16:1912.3 1.5 1
2-Methylnaphthalene 33.2 ug/kg 10/03/18 01:05 91-57-609/28/18 16:1912.3 1.4 1
Naphthalene 48.6 ug/kg 10/03/18 01:05 91-20-309/28/18 16:1912.3 2.8 1
Phenanthrene 72.0 ug/kg 10/03/18 01:05 85-01-809/28/18 16:1912.3 1.8 1
Pyrene 78.9 ug/kg 10/03/18 01:05 129-00-009/28/18 16:1912.3 2.2 1
Surrogates
Nitrobenzene-d5 (S)69 %10/03/18 01:05 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)67 %10/03/18 01:05 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)102 %10/03/18 01:05 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.8 %09/27/18 17:230.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 15:54 57-12-510/04/18 15:150.31 0.18 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 24.0 mg/kg 10/03/18 16:15 16984-48-810/02/18 09:006.0 3.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 13 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB004 (0'-1')Lab ID:92401224007 Collected:09/25/18 10:40 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 247 ug/kg 10/03/18 01:26 83-32-909/28/18 16:1911.9 1.8 1
Acenaphthylene ND ug/kg 10/03/18 01:26 208-96-809/28/18 16:1911.9 1.5 1
Anthracene 760 ug/kg 10/03/18 01:26 120-12-709/28/18 16:1911.9 1.7 1
Benzo(a)anthracene 1750 ug/kg 10/03/18 10:17 56-55-309/28/18 16:1959.5 4.2 5
Benzo(a)pyrene 1240 ug/kg 10/03/18 10:17 50-32-809/28/18 16:1959.5 6.5 5
Benzo(b)fluoranthene 2280 ug/kg 10/03/18 10:17 205-99-209/28/18 16:1959.5 4.0 5
Benzo(g,h,i)perylene 640 ug/kg 10/03/18 01:26 191-24-209/28/18 16:1911.9 3.1 1
Benzo(k)fluoranthene 884 ug/kg 10/03/18 01:26 207-08-909/28/18 16:1911.9 1.8 1
Chrysene 1570 ug/kg 10/03/18 10:17 218-01-909/28/18 16:1959.5 10.7 5
Dibenz(a,h)anthracene 85.3 ug/kg 10/03/18 01:26 53-70-309/28/18 16:1911.9 2.1 1
Fluoranthene 3370 ug/kg 10/03/18 10:17 206-44-009/28/18 16:1959.5 4.9 5
Fluorene 224 ug/kg 10/03/18 01:26 86-73-709/28/18 16:1911.9 1.9 1
Indeno(1,2,3-cd)pyrene 683 ug/kg 10/03/18 01:26 193-39-509/28/18 16:1911.9 3.3 1
1-Methylnaphthalene 256 ug/kg 10/03/18 01:26 90-12-009/28/18 16:1911.9 1.4 1
2-Methylnaphthalene 326 ug/kg 10/03/18 01:26 91-57-609/28/18 16:1911.9 1.3 1
Naphthalene 158 ug/kg 10/03/18 01:26 91-20-309/28/18 16:1911.9 2.7 1
Phenanthrene 3030 ug/kg 10/03/18 10:17 85-01-809/28/18 16:1959.5 8.9 5
Pyrene 2350 ug/kg 10/03/18 10:17 129-00-009/28/18 16:1959.5 10.7 5
Surrogates
Nitrobenzene-d5 (S)73 %10/03/18 01:26 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)70 %10/03/18 01:26 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)90 %10/03/18 01:26 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.8 %09/27/18 17:230.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 15:55 57-12-510/04/18 15:150.30 0.17 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 24.6J mg/kg 10/03/18 16:37 16984-48-810/02/18 09:0029.9 15.0 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB004 (4'-5')Lab ID:92401224008 Collected:09/25/18 10:45 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/02/18 22:17 83-32-909/28/18 16:1913.5 2.0 1
Acenaphthylene ND ug/kg 10/02/18 22:17 208-96-809/28/18 16:1913.5 1.8 1
Anthracene ND ug/kg 10/02/18 22:17 120-12-709/28/18 16:1913.5 1.9 1
Benzo(a)anthracene ND ug/kg 10/02/18 22:17 56-55-309/28/18 16:1913.5 0.96 1
Benzo(a)pyrene ND ug/kg 10/02/18 22:17 50-32-809/28/18 16:1913.5 1.5 1
Benzo(b)fluoranthene ND ug/kg 10/02/18 22:17 205-99-209/28/18 16:1913.5 0.90 1
Benzo(g,h,i)perylene ND ug/kg 10/02/18 22:17 191-24-209/28/18 16:1913.5 3.5 1
Benzo(k)fluoranthene ND ug/kg 10/02/18 22:17 207-08-909/28/18 16:1913.5 2.0 1
Chrysene ND ug/kg 10/02/18 22:17 218-01-909/28/18 16:1913.5 2.4 1
Dibenz(a,h)anthracene ND ug/kg 10/02/18 22:17 53-70-309/28/18 16:1913.5 2.4 1
Fluoranthene ND ug/kg 10/02/18 22:17 206-44-009/28/18 16:1913.5 1.1 1
Fluorene ND ug/kg 10/02/18 22:17 86-73-709/28/18 16:1913.5 2.2 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/02/18 22:17 193-39-509/28/18 16:1913.5 3.8 1
1-Methylnaphthalene ND ug/kg 10/02/18 22:17 90-12-009/28/18 16:1913.5 1.6 1
2-Methylnaphthalene ND ug/kg 10/02/18 22:17 91-57-609/28/18 16:1913.5 1.5 1
Naphthalene ND ug/kg 10/02/18 22:17 91-20-309/28/18 16:1913.5 3.1 1
Phenanthrene ND ug/kg 10/02/18 22:17 85-01-809/28/18 16:1913.5 2.0 1
Pyrene ND ug/kg 10/02/18 22:17 129-00-009/28/18 16:1913.5 2.4 1
Surrogates
Nitrobenzene-d5 (S)77 %10/02/18 22:17 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)76 %10/02/18 22:17 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)78 %10/02/18 22:17 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 25.4 %09/27/18 17:230.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 15:56 57-12-510/04/18 15:150.33 0.19 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride ND mg/kg 10/03/18 16:59 16984-48-810/02/18 09:006.7 3.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB005 (0'-1')Lab ID:92401224009 Collected:09/25/18 11:45 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/02/18 22:38 83-32-909/28/18 16:1912.4 1.9 1
Acenaphthylene 2.2J ug/kg 10/02/18 22:38 208-96-809/28/18 16:1912.4 1.6 1
Anthracene 2.2J ug/kg 10/02/18 22:38 120-12-709/28/18 16:1912.4 1.7 1
Benzo(a)anthracene 17.5 ug/kg 10/02/18 22:38 56-55-309/28/18 16:1912.4 0.88 1
Benzo(a)pyrene 18.1 ug/kg 10/02/18 22:38 50-32-809/28/18 16:1912.4 1.4 1
Benzo(b)fluoranthene 33.2 ug/kg 10/02/18 22:38 205-99-209/28/18 16:1912.4 0.83 1
Benzo(g,h,i)perylene 13.6 ug/kg 10/02/18 22:38 191-24-209/28/18 16:1912.4 3.2 1
Benzo(k)fluoranthene 9.1J ug/kg 10/02/18 22:38 207-08-909/28/18 16:1912.4 1.9 1
Chrysene 19.6 ug/kg 10/02/18 22:38 218-01-909/28/18 16:1912.4 2.2 1
Dibenz(a,h)anthracene ND ug/kg 10/02/18 22:38 53-70-309/28/18 16:1912.4 2.2 1
Fluoranthene 28.8 ug/kg 10/02/18 22:38 206-44-009/28/18 16:1912.4 1.0 1
Fluorene ND ug/kg 10/02/18 22:38 86-73-709/28/18 16:1912.4 2.0 1
Indeno(1,2,3-cd)pyrene 12.6 ug/kg 10/02/18 22:38 193-39-509/28/18 16:1912.4 3.5 1
1-Methylnaphthalene ND ug/kg 10/02/18 22:38 90-12-009/28/18 16:1912.4 1.5 1
2-Methylnaphthalene 1.9J ug/kg 10/02/18 22:38 91-57-609/28/18 16:1912.4 1.4 1
Naphthalene ND ug/kg 10/02/18 22:38 91-20-309/28/18 16:1912.4 2.8 1
Phenanthrene 8.0J ug/kg 10/02/18 22:38 85-01-809/28/18 16:1912.4 1.9 1
Pyrene 24.5 ug/kg 10/02/18 22:38 129-00-009/28/18 16:1912.4 2.2 1
Surrogates
Nitrobenzene-d5 (S)75 %10/02/18 22:38 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)71 %10/02/18 22:38 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)77 %10/02/18 22:38 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.8 %09/27/18 17:240.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:00 57-12-510/04/18 15:150.31 0.18 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 161 mg/kg 10/04/18 10:36 16984-48-810/02/18 09:0060.7 30.3 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB005 (4'-5')Lab ID:92401224010 Collected:09/25/18 11:50 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/02/18 22:59 83-32-909/28/18 16:1911.9 1.8 1
Acenaphthylene ND ug/kg 10/02/18 22:59 208-96-809/28/18 16:1911.9 1.5 1
Anthracene ND ug/kg 10/02/18 22:59 120-12-709/28/18 16:1911.9 1.7 1
Benzo(a)anthracene 2.5J ug/kg 10/02/18 22:59 56-55-309/28/18 16:1911.9 0.84 1
Benzo(a)pyrene 4.9J ug/kg 10/02/18 22:59 50-32-809/28/18 16:1911.9 1.3 1
Benzo(b)fluoranthene 12.0 ug/kg 10/02/18 22:59 205-99-209/28/18 16:1911.9 0.79 1
Benzo(g,h,i)perylene 4.6J ug/kg 10/02/18 22:59 191-24-209/28/18 16:1911.9 3.1 1
Benzo(k)fluoranthene 4.8J ug/kg 10/02/18 22:59 207-08-909/28/18 16:1911.9 1.8 1
Chrysene 12.1 ug/kg 10/02/18 22:59 218-01-909/28/18 16:1911.9 2.1 1
Dibenz(a,h)anthracene ND ug/kg 10/02/18 22:59 53-70-309/28/18 16:1911.9 2.1 1
Fluoranthene 29.6 ug/kg 10/02/18 22:59 206-44-009/28/18 16:1911.9 0.98 1
Fluorene ND ug/kg 10/02/18 22:59 86-73-709/28/18 16:1911.9 1.9 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/02/18 22:59 193-39-509/28/18 16:1911.9 3.3 1
1-Methylnaphthalene ND ug/kg 10/02/18 22:59 90-12-009/28/18 16:1911.9 1.4 1
2-Methylnaphthalene ND ug/kg 10/02/18 22:59 91-57-609/28/18 16:1911.9 1.3 1
Naphthalene ND ug/kg 10/02/18 22:59 91-20-309/28/18 16:1911.9 2.7 1
Phenanthrene 6.4J ug/kg 10/02/18 22:59 85-01-809/28/18 16:1911.9 1.8 1
Pyrene 23.2 ug/kg 10/02/18 22:59 129-00-009/28/18 16:1911.9 2.1 1
Surrogates
Nitrobenzene-d5 (S)61 %10/02/18 22:59 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)57 %10/02/18 22:59 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)62 %10/02/18 22:59 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.7 %09/27/18 17:240.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:01 57-12-510/04/18 15:150.30 0.17 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride ND mg/kg 10/03/18 17:43 16984-48-810/02/18 09:005.9 3.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB006 (0'-1')Lab ID:92401224011 Collected:09/25/18 12:05 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/02/18 23:20 83-32-909/28/18 16:1911.9 1.8 1
Acenaphthylene 2.4J ug/kg 10/02/18 23:20 208-96-809/28/18 16:1911.9 1.5 1
Anthracene 2.0J ug/kg 10/02/18 23:20 120-12-709/28/18 16:1911.9 1.7 1
Benzo(a)anthracene 15.1 ug/kg 10/02/18 23:20 56-55-309/28/18 16:1911.9 0.84 1
Benzo(a)pyrene 17.4 ug/kg 10/02/18 23:20 50-32-809/28/18 16:1911.9 1.3 1
Benzo(b)fluoranthene 31.3 ug/kg 10/02/18 23:20 205-99-209/28/18 16:1911.9 0.80 1
Benzo(g,h,i)perylene 13.7 ug/kg 10/02/18 23:20 191-24-209/28/18 16:1911.9 3.1 1
Benzo(k)fluoranthene 11.6J ug/kg 10/02/18 23:20 207-08-909/28/18 16:1911.9 1.8 1
Chrysene 19.6 ug/kg 10/02/18 23:20 218-01-909/28/18 16:1911.9 2.1 1
Dibenz(a,h)anthracene ND ug/kg 10/02/18 23:20 53-70-309/28/18 16:1911.9 2.1 1
Fluoranthene 27.6 ug/kg 10/02/18 23:20 206-44-009/28/18 16:1911.9 0.98 1
Fluorene ND ug/kg 10/02/18 23:20 86-73-709/28/18 16:1911.9 1.9 1
Indeno(1,2,3-cd)pyrene 12.7 ug/kg 10/02/18 23:20 193-39-509/28/18 16:1911.9 3.3 1
1-Methylnaphthalene 1.6J ug/kg 10/02/18 23:20 90-12-009/28/18 16:1911.9 1.4 1
2-Methylnaphthalene 2.4J ug/kg 10/02/18 23:20 91-57-609/28/18 16:1911.9 1.3 1
Naphthalene ND ug/kg 10/02/18 23:20 91-20-309/28/18 16:1911.9 2.7 1
Phenanthrene 14.9 ug/kg 10/02/18 23:20 85-01-809/28/18 16:1911.9 1.8 1
Pyrene 23.0 ug/kg 10/02/18 23:20 129-00-009/28/18 16:1911.9 2.1 1
Surrogates
Nitrobenzene-d5 (S)68 %10/02/18 23:20 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)63 %10/02/18 23:20 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)83 %10/02/18 23:20 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.9 %09/27/18 17:240.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:02 57-12-510/04/18 15:150.30 0.17 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 47.2 mg/kg 10/03/18 18:49 16984-48-8 D6,M110/02/18 09:005.9 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB006 (4'-5')Lab ID:92401224012 Collected:09/25/18 12:10 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/02/18 23:41 83-32-909/28/18 16:1913.0 1.9 1
Acenaphthylene ND ug/kg 10/02/18 23:41 208-96-809/28/18 16:1913.0 1.7 1
Anthracene ND ug/kg 10/02/18 23:41 120-12-709/28/18 16:1913.0 1.8 1
Benzo(a)anthracene 2.4J ug/kg 10/02/18 23:41 56-55-309/28/18 16:1913.0 0.92 1
Benzo(a)pyrene 2.2J ug/kg 10/02/18 23:41 50-32-809/28/18 16:1913.0 1.4 1
Benzo(b)fluoranthene 3.7J ug/kg 10/02/18 23:41 205-99-209/28/18 16:1913.0 0.87 1
Benzo(g,h,i)perylene ND ug/kg 10/02/18 23:41 191-24-209/28/18 16:1913.0 3.4 1
Benzo(k)fluoranthene ND ug/kg 10/02/18 23:41 207-08-909/28/18 16:1913.0 1.9 1
Chrysene 2.7J ug/kg 10/02/18 23:41 218-01-909/28/18 16:1913.0 2.3 1
Dibenz(a,h)anthracene ND ug/kg 10/02/18 23:41 53-70-309/28/18 16:1913.0 2.3 1
Fluoranthene 4.1J ug/kg 10/02/18 23:41 206-44-009/28/18 16:1913.0 1.1 1
Fluorene ND ug/kg 10/02/18 23:41 86-73-709/28/18 16:1913.0 2.1 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/02/18 23:41 193-39-509/28/18 16:1913.0 3.6 1
1-Methylnaphthalene 8.4J ug/kg 10/02/18 23:41 90-12-009/28/18 16:1913.0 1.6 1
2-Methylnaphthalene 11.5J ug/kg 10/02/18 23:41 91-57-609/28/18 16:1913.0 1.4 1
Naphthalene 6.5J ug/kg 10/02/18 23:41 91-20-309/28/18 16:1913.0 3.0 1
Phenanthrene 5.0J ug/kg 10/02/18 23:41 85-01-809/28/18 16:1913.0 1.9 1
Pyrene 3.6J ug/kg 10/02/18 23:41 129-00-009/28/18 16:1913.0 2.3 1
Surrogates
Nitrobenzene-d5 (S)83 %10/02/18 23:41 4165-60-009/28/18 16:1910-128 1
2-Fluorobiphenyl (S)75 %10/02/18 23:41 321-60-809/28/18 16:1910-110 1
Terphenyl-d14 (S)87 %10/02/18 23:41 1718-51-009/28/18 16:1939-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 21.5 %09/27/18 17:240.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:03 57-12-510/04/18 15:150.33 0.18 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride ND mg/kg 10/03/18 19:55 16984-48-810/02/18 09:006.4 3.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB007 (0'-1')Lab ID:92401224013 Collected:09/25/18 12:55 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/01/18 15:34 83-32-909/28/18 17:0712.5 1.9 1
Acenaphthylene ND ug/kg 10/01/18 15:34 208-96-809/28/18 17:0712.5 1.6 1
Anthracene 2.4J ug/kg 10/01/18 15:34 120-12-709/28/18 17:0712.5 1.8 1
Benzo(a)anthracene 14.1 ug/kg 10/01/18 15:34 56-55-3 M109/28/18 17:0712.5 0.89 1
Benzo(a)pyrene 14.2 ug/kg 10/01/18 15:34 50-32-8 M109/28/18 17:0712.5 1.4 1
Benzo(b)fluoranthene 24.6 ug/kg 10/01/18 15:34 205-99-2 M109/28/18 17:0712.5 0.84 1
Benzo(g,h,i)perylene 12.5J ug/kg 10/01/18 15:34 191-24-2 M109/28/18 17:0712.5 3.3 1
Benzo(k)fluoranthene 9.3J ug/kg 10/01/18 15:34 207-08-9 M109/28/18 17:0712.5 1.9 1
Chrysene 15.0 ug/kg 10/01/18 15:34 218-01-9 M109/28/18 17:0712.5 2.3 1
Dibenz(a,h)anthracene 3.8J ug/kg 10/01/18 15:34 53-70-3 M109/28/18 17:0712.5 2.3 1
Fluoranthene 22.7 ug/kg 10/01/18 15:34 206-44-0 M109/28/18 17:0712.5 1.0 1
Fluorene ND ug/kg 10/01/18 15:34 86-73-709/28/18 17:0712.5 2.0 1
Indeno(1,2,3-cd)pyrene 10.5J ug/kg 10/01/18 15:34 193-39-5 M109/28/18 17:0712.5 3.5 1
1-Methylnaphthalene 12.0J ug/kg 10/01/18 15:34 90-12-0 M109/28/18 17:0712.5 1.5 1
2-Methylnaphthalene 17.6 ug/kg 10/01/18 15:34 91-57-6 M109/28/18 17:0712.5 1.4 1
Naphthalene 14.5 ug/kg 10/01/18 15:34 91-20-3 M109/28/18 17:0712.5 2.9 1
Phenanthrene 16.8 ug/kg 10/01/18 15:34 85-01-8 M109/28/18 17:0712.5 1.9 1
Pyrene 19.4 ug/kg 10/01/18 15:34 129-00-0 M109/28/18 17:0712.5 2.3 1
Surrogates
Nitrobenzene-d5 (S)65 %10/01/18 15:34 4165-60-009/28/18 17:0710-128 1
2-Fluorobiphenyl (S)60 %10/01/18 15:34 321-60-809/28/18 17:0710-110 1
Terphenyl-d14 (S)66 %10/01/18 15:34 1718-51-009/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 21.1 %09/27/18 17:240.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:06 57-12-510/04/18 15:150.32 0.18 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 21.3 mg/kg 10/03/18 20:17 16984-48-810/02/18 09:006.3 3.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB007 (4'-5')Lab ID:92401224014 Collected:09/25/18 13:00 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/01/18 16:16 83-32-909/28/18 17:0710.8 1.6 1
Acenaphthylene ND ug/kg 10/01/18 16:16 208-96-809/28/18 17:0710.8 1.4 1
Anthracene ND ug/kg 10/01/18 16:16 120-12-709/28/18 17:0710.8 1.5 1
Benzo(a)anthracene ND ug/kg 10/01/18 16:16 56-55-309/28/18 17:0710.8 0.77 1
Benzo(a)pyrene ND ug/kg 10/01/18 16:16 50-32-809/28/18 17:0710.8 1.2 1
Benzo(b)fluoranthene ND ug/kg 10/01/18 16:16 205-99-209/28/18 17:0710.8 0.72 1
Benzo(g,h,i)perylene ND ug/kg 10/01/18 16:16 191-24-209/28/18 17:0710.8 2.8 1
Benzo(k)fluoranthene ND ug/kg 10/01/18 16:16 207-08-909/28/18 17:0710.8 1.6 1
Chrysene ND ug/kg 10/01/18 16:16 218-01-909/28/18 17:0710.8 1.9 1
Dibenz(a,h)anthracene ND ug/kg 10/01/18 16:16 53-70-309/28/18 17:0710.8 1.9 1
Fluoranthene ND ug/kg 10/01/18 16:16 206-44-009/28/18 17:0710.8 0.90 1
Fluorene ND ug/kg 10/01/18 16:16 86-73-709/28/18 17:0710.8 1.7 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/01/18 16:16 193-39-509/28/18 17:0710.8 3.0 1
1-Methylnaphthalene ND ug/kg 10/01/18 16:16 90-12-009/28/18 17:0710.8 1.3 1
2-Methylnaphthalene ND ug/kg 10/01/18 16:16 91-57-609/28/18 17:0710.8 1.2 1
Naphthalene ND ug/kg 10/01/18 16:16 91-20-309/28/18 17:0710.8 2.5 1
Phenanthrene ND ug/kg 10/01/18 16:16 85-01-809/28/18 17:0710.8 1.6 1
Pyrene ND ug/kg 10/01/18 16:16 129-00-009/28/18 17:0710.8 1.9 1
Surrogates
Nitrobenzene-d5 (S)47 %10/01/18 16:16 4165-60-009/28/18 17:0710-128 1
2-Fluorobiphenyl (S)47 %10/01/18 16:16 321-60-809/28/18 17:0710-110 1
Terphenyl-d14 (S)48 %10/01/18 16:16 1718-51-009/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 6.3 %09/27/18 17:240.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:07 57-12-510/04/18 15:150.27 0.15 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride ND mg/kg 10/03/18 20:39 16984-48-810/02/18 09:005.3 2.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB008 (0'-1')Lab ID:92401224015 Collected:09/25/18 14:25 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 173 ug/kg 10/01/18 16:58 83-32-909/28/18 17:0711.7 1.8 1
Acenaphthylene ND ug/kg 10/01/18 16:58 208-96-809/28/18 17:0711.7 1.5 1
Anthracene 212 ug/kg 10/01/18 16:58 120-12-709/28/18 17:0711.7 1.6 1
Benzo(a)anthracene 620 ug/kg 10/01/18 16:58 56-55-309/28/18 17:0711.7 0.83 1
Benzo(a)pyrene 509 ug/kg 10/01/18 16:58 50-32-809/28/18 17:0711.7 1.3 1
Benzo(b)fluoranthene 916 ug/kg 10/01/18 16:58 205-99-209/28/18 17:0711.7 0.79 1
Benzo(g,h,i)perylene 356 ug/kg 10/01/18 16:58 191-24-209/28/18 17:0711.7 3.1 1
Benzo(k)fluoranthene 264 ug/kg 10/01/18 16:58 207-08-909/28/18 17:0711.7 1.8 1
Chrysene 590 ug/kg 10/01/18 16:58 218-01-909/28/18 17:0711.7 2.1 1
Dibenz(a,h)anthracene 110 ug/kg 10/01/18 16:58 53-70-309/28/18 17:0711.7 2.1 1
Fluoranthene 958 ug/kg 10/02/18 16:00 206-44-009/28/18 17:0723.5 2.0 2
Fluorene 120 ug/kg 10/01/18 16:58 86-73-709/28/18 17:0711.7 1.9 1
Indeno(1,2,3-cd)pyrene 336 ug/kg 10/01/18 16:58 193-39-509/28/18 17:0711.7 3.3 1
1-Methylnaphthalene 31.5 ug/kg 10/01/18 16:58 90-12-009/28/18 17:0711.7 1.4 1
2-Methylnaphthalene 50.4 ug/kg 10/01/18 16:58 91-57-609/28/18 17:0711.7 1.3 1
Naphthalene 148 ug/kg 10/01/18 16:58 91-20-309/28/18 17:0711.7 2.7 1
Phenanthrene 843 ug/kg 10/01/18 16:58 85-01-809/28/18 17:0711.7 1.8 1
Pyrene 864 ug/kg 10/01/18 16:58 129-00-009/28/18 17:0711.7 2.1 1
Surrogates
Nitrobenzene-d5 (S)69 %10/01/18 16:58 4165-60-009/28/18 17:0710-128 1
2-Fluorobiphenyl (S)61 %10/01/18 16:58 321-60-809/28/18 17:0710-110 1
Terphenyl-d14 (S)75 %10/01/18 16:58 1718-51-009/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.7 %09/27/18 17:240.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:08 57-12-510/04/18 15:150.30 0.17 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 72.9 mg/kg 10/03/18 21:01 16984-48-810/02/18 09:005.9 3.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB008 (4'-5')Lab ID:92401224016 Collected:09/25/18 14:30 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/01/18 17:19 83-32-909/28/18 17:0711.5 1.7 1
Acenaphthylene ND ug/kg 10/01/18 17:19 208-96-809/28/18 17:0711.5 1.5 1
Anthracene ND ug/kg 10/01/18 17:19 120-12-709/28/18 17:0711.5 1.6 1
Benzo(a)anthracene ND ug/kg 10/01/18 17:19 56-55-309/28/18 17:0711.5 0.82 1
Benzo(a)pyrene ND ug/kg 10/01/18 17:19 50-32-809/28/18 17:0711.5 1.3 1
Benzo(b)fluoranthene ND ug/kg 10/01/18 17:19 205-99-209/28/18 17:0711.5 0.77 1
Benzo(g,h,i)perylene ND ug/kg 10/01/18 17:19 191-24-209/28/18 17:0711.5 3.0 1
Benzo(k)fluoranthene ND ug/kg 10/01/18 17:19 207-08-909/28/18 17:0711.5 1.7 1
Chrysene ND ug/kg 10/01/18 17:19 218-01-909/28/18 17:0711.5 2.1 1
Dibenz(a,h)anthracene ND ug/kg 10/01/18 17:19 53-70-309/28/18 17:0711.5 2.1 1
Fluoranthene ND ug/kg 10/01/18 17:19 206-44-009/28/18 17:0711.5 0.96 1
Fluorene ND ug/kg 10/01/18 17:19 86-73-709/28/18 17:0711.5 1.8 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/01/18 17:19 193-39-509/28/18 17:0711.5 3.2 1
1-Methylnaphthalene ND ug/kg 10/01/18 17:19 90-12-009/28/18 17:0711.5 1.4 1
2-Methylnaphthalene ND ug/kg 10/01/18 17:19 91-57-609/28/18 17:0711.5 1.3 1
Naphthalene ND ug/kg 10/01/18 17:19 91-20-309/28/18 17:0711.5 2.7 1
Phenanthrene ND ug/kg 10/01/18 17:19 85-01-809/28/18 17:0711.5 1.7 1
Pyrene ND ug/kg 10/01/18 17:19 129-00-009/28/18 17:0711.5 2.1 1
Surrogates
Nitrobenzene-d5 (S)63 %10/01/18 17:19 4165-60-009/28/18 17:0710-128 1
2-Fluorobiphenyl (S)55 %10/01/18 17:19 321-60-809/28/18 17:0710-110 1
Terphenyl-d14 (S)69 %10/01/18 17:19 1718-51-009/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.2 %09/27/18 17:240.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide 0.23J mg/kg 10/05/18 16:09 57-12-510/04/18 15:150.27 0.16 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 35.3 mg/kg 10/03/18 21:23 16984-48-810/02/18 09:005.7 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB009 (0'-1')Lab ID:92401224017 Collected:09/25/18 14:45 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/01/18 17:40 83-32-909/28/18 17:0712.0 1.8 1
Acenaphthylene ND ug/kg 10/01/18 17:40 208-96-809/28/18 17:0712.0 1.6 1
Anthracene ND ug/kg 10/01/18 17:40 120-12-709/28/18 17:0712.0 1.7 1
Benzo(a)anthracene 18.9 ug/kg 10/01/18 17:40 56-55-309/28/18 17:0712.0 0.85 1
Benzo(a)pyrene 21.7 ug/kg 10/01/18 17:40 50-32-809/28/18 17:0712.0 1.3 1
Benzo(b)fluoranthene 47.5 ug/kg 10/01/18 17:40 205-99-209/28/18 17:0712.0 0.80 1
Benzo(g,h,i)perylene 23.4 ug/kg 10/01/18 17:40 191-24-209/28/18 17:0712.0 3.1 1
Benzo(k)fluoranthene 18.4 ug/kg 10/01/18 17:40 207-08-909/28/18 17:0712.0 1.8 1
Chrysene 35.5 ug/kg 10/01/18 17:40 218-01-909/28/18 17:0712.0 2.2 1
Dibenz(a,h)anthracene 6.4J ug/kg 10/01/18 17:40 53-70-309/28/18 17:0712.0 2.2 1
Fluoranthene 64.7 ug/kg 10/01/18 17:40 206-44-009/28/18 17:0712.0 1.0 1
Fluorene ND ug/kg 10/01/18 17:40 86-73-709/28/18 17:0712.0 1.9 1
Indeno(1,2,3-cd)pyrene 17.8 ug/kg 10/01/18 17:40 193-39-509/28/18 17:0712.0 3.4 1
1-Methylnaphthalene ND ug/kg 10/01/18 17:40 90-12-009/28/18 17:0712.0 1.4 1
2-Methylnaphthalene ND ug/kg 10/01/18 17:40 91-57-609/28/18 17:0712.0 1.3 1
Naphthalene ND ug/kg 10/01/18 17:40 91-20-309/28/18 17:0712.0 2.8 1
Phenanthrene 12.0J ug/kg 10/01/18 17:40 85-01-809/28/18 17:0712.0 1.8 1
Pyrene 54.2 ug/kg 10/01/18 17:40 129-00-009/28/18 17:0712.0 2.2 1
Surrogates
Nitrobenzene-d5 (S)52 %10/01/18 17:40 4165-60-009/28/18 17:0710-128 1
2-Fluorobiphenyl (S)48 %10/01/18 17:40 321-60-809/28/18 17:0710-110 1
Terphenyl-d14 (S)57 %10/01/18 17:40 1718-51-009/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.7 %09/27/18 17:240.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:14 57-12-510/04/18 18:100.30 0.17 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 41.3 mg/kg 10/03/18 21:45 16984-48-810/02/18 09:006.0 3.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB009 (4'-5')Lab ID:92401224018 Collected:09/25/18 14:50 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/01/18 18:01 83-32-909/28/18 17:0711.8 1.8 1
Acenaphthylene ND ug/kg 10/01/18 18:01 208-96-809/28/18 17:0711.8 1.5 1
Anthracene ND ug/kg 10/01/18 18:01 120-12-709/28/18 17:0711.8 1.7 1
Benzo(a)anthracene ND ug/kg 10/01/18 18:01 56-55-309/28/18 17:0711.8 0.84 1
Benzo(a)pyrene ND ug/kg 10/01/18 18:01 50-32-809/28/18 17:0711.8 1.3 1
Benzo(b)fluoranthene ND ug/kg 10/01/18 18:01 205-99-209/28/18 17:0711.8 0.79 1
Benzo(g,h,i)perylene ND ug/kg 10/01/18 18:01 191-24-209/28/18 17:0711.8 3.1 1
Benzo(k)fluoranthene ND ug/kg 10/01/18 18:01 207-08-909/28/18 17:0711.8 1.8 1
Chrysene ND ug/kg 10/01/18 18:01 218-01-909/28/18 17:0711.8 2.1 1
Dibenz(a,h)anthracene ND ug/kg 10/01/18 18:01 53-70-309/28/18 17:0711.8 2.1 1
Fluoranthene ND ug/kg 10/01/18 18:01 206-44-009/28/18 17:0711.8 0.98 1
Fluorene ND ug/kg 10/01/18 18:01 86-73-709/28/18 17:0711.8 1.9 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/01/18 18:01 193-39-509/28/18 17:0711.8 3.3 1
1-Methylnaphthalene ND ug/kg 10/01/18 18:01 90-12-009/28/18 17:0711.8 1.4 1
2-Methylnaphthalene ND ug/kg 10/01/18 18:01 91-57-609/28/18 17:0711.8 1.3 1
Naphthalene ND ug/kg 10/01/18 18:01 91-20-309/28/18 17:0711.8 2.7 1
Phenanthrene ND ug/kg 10/01/18 18:01 85-01-809/28/18 17:0711.8 1.8 1
Pyrene ND ug/kg 10/01/18 18:01 129-00-009/28/18 17:0711.8 2.1 1
Surrogates
Nitrobenzene-d5 (S)55 %10/01/18 18:01 4165-60-009/28/18 17:0710-128 1
2-Fluorobiphenyl (S)46 %10/01/18 18:01 321-60-809/28/18 17:0710-110 1
Terphenyl-d14 (S)56 %10/01/18 18:01 1718-51-009/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.5 %09/27/18 17:240.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:17 57-12-510/04/18 18:100.31 0.18 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 15.9 mg/kg 10/03/18 22:07 16984-48-810/02/18 09:005.9 3.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB010 (0'-1')Lab ID:92401224019 Collected:09/25/18 15:00 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/01/18 18:22 83-32-909/28/18 17:0712.5 1.9 1
Acenaphthylene 4.0J ug/kg 10/01/18 18:22 208-96-809/28/18 17:0712.5 1.6 1
Anthracene 3.9J ug/kg 10/01/18 18:22 120-12-709/28/18 17:0712.5 1.7 1
Benzo(a)anthracene 23.4 ug/kg 10/01/18 18:22 56-55-309/28/18 17:0712.5 0.89 1
Benzo(a)pyrene 31.1 ug/kg 10/01/18 18:22 50-32-809/28/18 17:0712.5 1.4 1
Benzo(b)fluoranthene 69.2 ug/kg 10/01/18 18:22 205-99-209/28/18 17:0712.5 0.84 1
Benzo(g,h,i)perylene 41.3 ug/kg 10/01/18 18:22 191-24-209/28/18 17:0712.5 3.2 1
Benzo(k)fluoranthene 24.9 ug/kg 10/01/18 18:22 207-08-909/28/18 17:0712.5 1.9 1
Chrysene 28.6 ug/kg 10/01/18 18:22 218-01-909/28/18 17:0712.5 2.2 1
Dibenz(a,h)anthracene 2.8J ug/kg 10/01/18 18:22 53-70-309/28/18 17:0712.5 2.2 1
Fluoranthene 19.7 ug/kg 10/01/18 18:22 206-44-009/28/18 17:0712.5 1.0 1
Fluorene ND ug/kg 10/01/18 18:22 86-73-709/28/18 17:0712.5 2.0 1
Indeno(1,2,3-cd)pyrene 36.5 ug/kg 10/01/18 18:22 193-39-509/28/18 17:0712.5 3.5 1
1-Methylnaphthalene ND ug/kg 10/01/18 18:22 90-12-009/28/18 17:0712.5 1.5 1
2-Methylnaphthalene ND ug/kg 10/01/18 18:22 91-57-609/28/18 17:0712.5 1.4 1
Naphthalene ND ug/kg 10/01/18 18:22 91-20-309/28/18 17:0712.5 2.9 1
Phenanthrene 4.5J ug/kg 10/01/18 18:22 85-01-809/28/18 17:0712.5 1.9 1
Pyrene 19.1 ug/kg 10/01/18 18:22 129-00-009/28/18 17:0712.5 2.2 1
Surrogates
Nitrobenzene-d5 (S)60 %10/01/18 18:22 4165-60-009/28/18 17:0710-128 1
2-Fluorobiphenyl (S)57 %10/01/18 18:22 321-60-809/28/18 17:0710-110 1
Terphenyl-d14 (S)66 %10/01/18 18:22 1718-51-009/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.1 %09/27/18 17:530.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:18 57-12-510/04/18 18:100.32 0.18 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 57.2 mg/kg 10/03/18 22:29 16984-48-810/02/18 09:006.2 3.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB010 (4'-5')Lab ID:92401224020 Collected:09/25/18 15:05 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/01/18 18:43 83-32-909/28/18 17:0711.6 1.7 1
Acenaphthylene ND ug/kg 10/01/18 18:43 208-96-809/28/18 17:0711.6 1.5 1
Anthracene ND ug/kg 10/01/18 18:43 120-12-709/28/18 17:0711.6 1.6 1
Benzo(a)anthracene ND ug/kg 10/01/18 18:43 56-55-309/28/18 17:0711.6 0.83 1
Benzo(a)pyrene ND ug/kg 10/01/18 18:43 50-32-809/28/18 17:0711.6 1.3 1
Benzo(b)fluoranthene ND ug/kg 10/01/18 18:43 205-99-209/28/18 17:0711.6 0.78 1
Benzo(g,h,i)perylene ND ug/kg 10/01/18 18:43 191-24-209/28/18 17:0711.6 3.0 1
Benzo(k)fluoranthene ND ug/kg 10/01/18 18:43 207-08-909/28/18 17:0711.6 1.7 1
Chrysene ND ug/kg 10/01/18 18:43 218-01-909/28/18 17:0711.6 2.1 1
Dibenz(a,h)anthracene ND ug/kg 10/01/18 18:43 53-70-309/28/18 17:0711.6 2.1 1
Fluoranthene ND ug/kg 10/01/18 18:43 206-44-009/28/18 17:0711.6 0.97 1
Fluorene ND ug/kg 10/01/18 18:43 86-73-709/28/18 17:0711.6 1.9 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/01/18 18:43 193-39-509/28/18 17:0711.6 3.3 1
1-Methylnaphthalene ND ug/kg 10/01/18 18:43 90-12-009/28/18 17:0711.6 1.4 1
2-Methylnaphthalene ND ug/kg 10/01/18 18:43 91-57-609/28/18 17:0711.6 1.3 1
Naphthalene ND ug/kg 10/01/18 18:43 91-20-309/28/18 17:0711.6 2.7 1
Phenanthrene ND ug/kg 10/01/18 18:43 85-01-809/28/18 17:0711.6 1.7 1
Pyrene ND ug/kg 10/01/18 18:43 129-00-009/28/18 17:0711.6 2.1 1
Surrogates
Nitrobenzene-d5 (S)140 %10/01/18 18:43 4165-60-0 S309/28/18 17:0710-128 1
2-Fluorobiphenyl (S)124 %10/01/18 18:43 321-60-8 S309/28/18 17:0710-110 1
Terphenyl-d14 (S)132 %10/01/18 18:43 1718-51-0 S309/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.6 %09/27/18 17:530.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide 0.21J mg/kg 10/05/18 16:19 57-12-510/04/18 18:100.30 0.17 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 11.2 mg/kg 10/03/18 22:51 16984-48-810/02/18 09:005.8 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB011 (0'-1')Lab ID:92401224021 Collected:09/25/18 15:30 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/01/18 19:04 83-32-909/28/18 17:0712.1 1.8 1
Acenaphthylene ND ug/kg 10/01/18 19:04 208-96-809/28/18 17:0712.1 1.6 1
Anthracene ND ug/kg 10/01/18 19:04 120-12-709/28/18 17:0712.1 1.7 1
Benzo(a)anthracene 5.8J ug/kg 10/01/18 19:04 56-55-309/28/18 17:0712.1 0.86 1
Benzo(a)pyrene 6.3J ug/kg 10/01/18 19:04 50-32-809/28/18 17:0712.1 1.3 1
Benzo(b)fluoranthene 16.4 ug/kg 10/01/18 19:04 205-99-209/28/18 17:0712.1 0.81 1
Benzo(g,h,i)perylene 6.1J ug/kg 10/01/18 19:04 191-24-209/28/18 17:0712.1 3.1 1
Benzo(k)fluoranthene 5.0J ug/kg 10/01/18 19:04 207-08-909/28/18 17:0712.1 1.8 1
Chrysene 8.0J ug/kg 10/01/18 19:04 218-01-909/28/18 17:0712.1 2.2 1
Dibenz(a,h)anthracene ND ug/kg 10/01/18 19:04 53-70-309/28/18 17:0712.1 2.2 1
Fluoranthene 9.3J ug/kg 10/01/18 19:04 206-44-009/28/18 17:0712.1 1.0 1
Fluorene ND ug/kg 10/01/18 19:04 86-73-709/28/18 17:0712.1 1.9 1
Indeno(1,2,3-cd)pyrene 6.0J ug/kg 10/01/18 19:04 193-39-509/28/18 17:0712.1 3.4 1
1-Methylnaphthalene ND ug/kg 10/01/18 19:04 90-12-009/28/18 17:0712.1 1.5 1
2-Methylnaphthalene ND ug/kg 10/01/18 19:04 91-57-609/28/18 17:0712.1 1.3 1
Naphthalene ND ug/kg 10/01/18 19:04 91-20-309/28/18 17:0712.1 2.8 1
Phenanthrene 3.1J ug/kg 10/01/18 19:04 85-01-809/28/18 17:0712.1 1.8 1
Pyrene 8.5J ug/kg 10/01/18 19:04 129-00-009/28/18 17:0712.1 2.2 1
Surrogates
Nitrobenzene-d5 (S)34 %10/01/18 19:04 4165-60-009/28/18 17:0710-128 1
2-Fluorobiphenyl (S)33 %10/01/18 19:04 321-60-809/28/18 17:0710-110 1
Terphenyl-d14 (S)39 %10/01/18 19:04 1718-51-009/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.4 %09/27/18 17:530.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:20 57-12-510/04/18 18:100.31 0.18 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 92.3 mg/kg 10/04/18 00:41 16984-48-8 M110/02/18 09:006.0 3.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB011 (2'-3')Lab ID:92401224022 Collected:09/25/18 15:35 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/01/18 19:25 83-32-909/28/18 17:0711.1 1.7 1
Acenaphthylene ND ug/kg 10/01/18 19:25 208-96-809/28/18 17:0711.1 1.4 1
Anthracene ND ug/kg 10/01/18 19:25 120-12-709/28/18 17:0711.1 1.6 1
Benzo(a)anthracene ND ug/kg 10/01/18 19:25 56-55-309/28/18 17:0711.1 0.79 1
Benzo(a)pyrene ND ug/kg 10/01/18 19:25 50-32-809/28/18 17:0711.1 1.2 1
Benzo(b)fluoranthene ND ug/kg 10/01/18 19:25 205-99-209/28/18 17:0711.1 0.74 1
Benzo(g,h,i)perylene ND ug/kg 10/01/18 19:25 191-24-209/28/18 17:0711.1 2.9 1
Benzo(k)fluoranthene ND ug/kg 10/01/18 19:25 207-08-909/28/18 17:0711.1 1.7 1
Chrysene ND ug/kg 10/01/18 19:25 218-01-909/28/18 17:0711.1 2.0 1
Dibenz(a,h)anthracene ND ug/kg 10/01/18 19:25 53-70-309/28/18 17:0711.1 2.0 1
Fluoranthene ND ug/kg 10/01/18 19:25 206-44-009/28/18 17:0711.1 0.92 1
Fluorene ND ug/kg 10/01/18 19:25 86-73-709/28/18 17:0711.1 1.8 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/01/18 19:25 193-39-509/28/18 17:0711.1 3.1 1
1-Methylnaphthalene 1.7J ug/kg 10/01/18 19:25 90-12-009/28/18 17:0711.1 1.3 1
2-Methylnaphthalene 4.6J ug/kg 10/01/18 19:25 91-57-609/28/18 17:0711.1 1.2 1
Naphthalene 2.7J ug/kg 10/01/18 19:25 91-20-309/28/18 17:0711.1 2.5 1
Phenanthrene ND ug/kg 10/01/18 19:25 85-01-809/28/18 17:0711.1 1.7 1
Pyrene ND ug/kg 10/01/18 19:25 129-00-009/28/18 17:0711.1 2.0 1
Surrogates
Nitrobenzene-d5 (S)71 %10/01/18 19:25 4165-60-009/28/18 17:0710-128 1
2-Fluorobiphenyl (S)64 %10/01/18 19:25 321-60-809/28/18 17:0710-110 1
Terphenyl-d14 (S)71 %10/01/18 19:25 1718-51-009/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 11.3 %09/27/18 17:530.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide 0.18J mg/kg 10/05/18 16:21 57-12-510/04/18 18:100.27 0.16 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 48.3 mg/kg 10/04/18 01:47 16984-48-810/02/18 09:005.6 2.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB012 (0'-1')Lab ID:92401224023 Collected:09/25/18 16:10 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/01/18 19:46 83-32-909/28/18 17:0711.6 1.7 1
Acenaphthylene ND ug/kg 10/01/18 19:46 208-96-809/28/18 17:0711.6 1.5 1
Anthracene ND ug/kg 10/01/18 19:46 120-12-709/28/18 17:0711.6 1.6 1
Benzo(a)anthracene ND ug/kg 10/01/18 19:46 56-55-309/28/18 17:0711.6 0.83 1
Benzo(a)pyrene ND ug/kg 10/01/18 19:46 50-32-809/28/18 17:0711.6 1.3 1
Benzo(b)fluoranthene ND ug/kg 10/01/18 19:46 205-99-209/28/18 17:0711.6 0.78 1
Benzo(g,h,i)perylene ND ug/kg 10/01/18 19:46 191-24-209/28/18 17:0711.6 3.0 1
Benzo(k)fluoranthene ND ug/kg 10/01/18 19:46 207-08-909/28/18 17:0711.6 1.7 1
Chrysene ND ug/kg 10/01/18 19:46 218-01-909/28/18 17:0711.6 2.1 1
Dibenz(a,h)anthracene ND ug/kg 10/01/18 19:46 53-70-309/28/18 17:0711.6 2.1 1
Fluoranthene ND ug/kg 10/01/18 19:46 206-44-009/28/18 17:0711.6 0.96 1
Fluorene ND ug/kg 10/01/18 19:46 86-73-709/28/18 17:0711.6 1.9 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/01/18 19:46 193-39-509/28/18 17:0711.6 3.3 1
1-Methylnaphthalene ND ug/kg 10/01/18 19:46 90-12-009/28/18 17:0711.6 1.4 1
2-Methylnaphthalene ND ug/kg 10/01/18 19:46 91-57-609/28/18 17:0711.6 1.3 1
Naphthalene ND ug/kg 10/01/18 19:46 91-20-309/28/18 17:0711.6 2.7 1
Phenanthrene ND ug/kg 10/01/18 19:46 85-01-809/28/18 17:0711.6 1.7 1
Pyrene ND ug/kg 10/01/18 19:46 129-00-009/28/18 17:0711.6 2.1 1
Surrogates
Nitrobenzene-d5 (S)50 %10/01/18 19:46 4165-60-009/28/18 17:0710-128 1
2-Fluorobiphenyl (S)48 %10/01/18 19:46 321-60-809/28/18 17:0710-110 1
Terphenyl-d14 (S)51 %10/01/18 19:46 1718-51-009/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.5 %09/27/18 17:530.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:24 57-12-510/04/18 18:100.31 0.17 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 3.7J mg/kg 10/04/18 02:10 16984-48-810/02/18 09:005.8 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB012 (4'-5')Lab ID:92401224024 Collected:09/25/18 16:15 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/01/18 20:07 83-32-909/28/18 17:0711.4 1.7 1
Acenaphthylene ND ug/kg 10/01/18 20:07 208-96-809/28/18 17:0711.4 1.5 1
Anthracene ND ug/kg 10/01/18 20:07 120-12-709/28/18 17:0711.4 1.6 1
Benzo(a)anthracene ND ug/kg 10/01/18 20:07 56-55-309/28/18 17:0711.4 0.81 1
Benzo(a)pyrene ND ug/kg 10/01/18 20:07 50-32-809/28/18 17:0711.4 1.3 1
Benzo(b)fluoranthene ND ug/kg 10/01/18 20:07 205-99-209/28/18 17:0711.4 0.76 1
Benzo(g,h,i)perylene ND ug/kg 10/01/18 20:07 191-24-209/28/18 17:0711.4 3.0 1
Benzo(k)fluoranthene ND ug/kg 10/01/18 20:07 207-08-909/28/18 17:0711.4 1.7 1
Chrysene ND ug/kg 10/01/18 20:07 218-01-909/28/18 17:0711.4 2.0 1
Dibenz(a,h)anthracene ND ug/kg 10/01/18 20:07 53-70-309/28/18 17:0711.4 2.0 1
Fluoranthene ND ug/kg 10/01/18 20:07 206-44-009/28/18 17:0711.4 0.94 1
Fluorene ND ug/kg 10/01/18 20:07 86-73-709/28/18 17:0711.4 1.8 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/01/18 20:07 193-39-509/28/18 17:0711.4 3.2 1
1-Methylnaphthalene ND ug/kg 10/01/18 20:07 90-12-009/28/18 17:0711.4 1.4 1
2-Methylnaphthalene ND ug/kg 10/01/18 20:07 91-57-609/28/18 17:0711.4 1.3 1
Naphthalene ND ug/kg 10/01/18 20:07 91-20-309/28/18 17:0711.4 2.6 1
Phenanthrene ND ug/kg 10/01/18 20:07 85-01-809/28/18 17:0711.4 1.7 1
Pyrene ND ug/kg 10/01/18 20:07 129-00-009/28/18 17:0711.4 2.0 1
Surrogates
Nitrobenzene-d5 (S)56 %10/01/18 20:07 4165-60-009/28/18 17:0710-128 1
2-Fluorobiphenyl (S)53 %10/01/18 20:07 321-60-809/28/18 17:0710-110 1
Terphenyl-d14 (S)57 %10/01/18 20:07 1718-51-009/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.2 %09/27/18 17:530.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:25 57-12-510/04/18 18:100.29 0.16 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride ND mg/kg 10/04/18 02:32 16984-48-810/02/18 09:005.7 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB013 (0'-1')Lab ID:92401224025 Collected:09/25/18 16:30 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/01/18 20:28 83-32-909/28/18 17:0712.5 1.9 1
Acenaphthylene ND ug/kg 10/01/18 20:28 208-96-809/28/18 17:0712.5 1.6 1
Anthracene ND ug/kg 10/01/18 20:28 120-12-709/28/18 17:0712.5 1.7 1
Benzo(a)anthracene ND ug/kg 10/01/18 20:28 56-55-309/28/18 17:0712.5 0.88 1
Benzo(a)pyrene ND ug/kg 10/01/18 20:28 50-32-809/28/18 17:0712.5 1.4 1
Benzo(b)fluoranthene ND ug/kg 10/01/18 20:28 205-99-209/28/18 17:0712.5 0.83 1
Benzo(g,h,i)perylene ND ug/kg 10/01/18 20:28 191-24-209/28/18 17:0712.5 3.2 1
Benzo(k)fluoranthene ND ug/kg 10/01/18 20:28 207-08-909/28/18 17:0712.5 1.9 1
Chrysene ND ug/kg 10/01/18 20:28 218-01-909/28/18 17:0712.5 2.2 1
Dibenz(a,h)anthracene ND ug/kg 10/01/18 20:28 53-70-309/28/18 17:0712.5 2.2 1
Fluoranthene ND ug/kg 10/01/18 20:28 206-44-009/28/18 17:0712.5 1.0 1
Fluorene ND ug/kg 10/01/18 20:28 86-73-709/28/18 17:0712.5 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/01/18 20:28 193-39-509/28/18 17:0712.5 3.5 1
1-Methylnaphthalene ND ug/kg 10/01/18 20:28 90-12-009/28/18 17:0712.5 1.5 1
2-Methylnaphthalene ND ug/kg 10/01/18 20:28 91-57-609/28/18 17:0712.5 1.4 1
Naphthalene ND ug/kg 10/01/18 20:28 91-20-309/28/18 17:0712.5 2.9 1
Phenanthrene ND ug/kg 10/01/18 20:28 85-01-809/28/18 17:0712.5 1.9 1
Pyrene ND ug/kg 10/01/18 20:28 129-00-009/28/18 17:0712.5 2.2 1
Surrogates
Nitrobenzene-d5 (S)69 %10/01/18 20:28 4165-60-009/28/18 17:0710-128 1
2-Fluorobiphenyl (S)63 %10/01/18 20:28 321-60-809/28/18 17:0710-110 1
Terphenyl-d14 (S)66 %10/01/18 20:28 1718-51-009/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 18.4 %09/27/18 17:530.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:26 57-12-510/04/18 18:100.32 0.18 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 8.2 mg/kg 10/04/18 02:54 16984-48-810/02/18 09:006.1 3.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 32 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB013 (4'-5')Lab ID:92401224026 Collected:09/25/18 16:35 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/01/18 20:49 83-32-909/28/18 17:0712.7 1.9 1
Acenaphthylene ND ug/kg 10/01/18 20:49 208-96-809/28/18 17:0712.7 1.7 1
Anthracene ND ug/kg 10/01/18 20:49 120-12-709/28/18 17:0712.7 1.8 1
Benzo(a)anthracene 0.95J ug/kg 10/01/18 20:49 56-55-309/28/18 17:0712.7 0.90 1
Benzo(a)pyrene ND ug/kg 10/01/18 20:49 50-32-809/28/18 17:0712.7 1.4 1
Benzo(b)fluoranthene 1.7J ug/kg 10/01/18 20:49 205-99-209/28/18 17:0712.7 0.85 1
Benzo(g,h,i)perylene ND ug/kg 10/01/18 20:49 191-24-209/28/18 17:0712.7 3.3 1
Benzo(k)fluoranthene ND ug/kg 10/01/18 20:49 207-08-909/28/18 17:0712.7 1.9 1
Chrysene ND ug/kg 10/01/18 20:49 218-01-909/28/18 17:0712.7 2.3 1
Dibenz(a,h)anthracene ND ug/kg 10/01/18 20:49 53-70-309/28/18 17:0712.7 2.3 1
Fluoranthene ND ug/kg 10/01/18 20:49 206-44-009/28/18 17:0712.7 1.1 1
Fluorene ND ug/kg 10/01/18 20:49 86-73-709/28/18 17:0712.7 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/01/18 20:49 193-39-509/28/18 17:0712.7 3.6 1
1-Methylnaphthalene ND ug/kg 10/01/18 20:49 90-12-009/28/18 17:0712.7 1.5 1
2-Methylnaphthalene ND ug/kg 10/01/18 20:49 91-57-609/28/18 17:0712.7 1.4 1
Naphthalene ND ug/kg 10/01/18 20:49 91-20-309/28/18 17:0712.7 2.9 1
Phenanthrene ND ug/kg 10/01/18 20:49 85-01-809/28/18 17:0712.7 1.9 1
Pyrene ND ug/kg 10/01/18 20:49 129-00-009/28/18 17:0712.7 2.3 1
Surrogates
Nitrobenzene-d5 (S)61 %10/01/18 20:49 4165-60-009/28/18 17:0710-128 1
2-Fluorobiphenyl (S)58 %10/01/18 20:49 321-60-809/28/18 17:0710-110 1
Terphenyl-d14 (S)62 %10/01/18 20:49 1718-51-009/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.7 %09/27/18 17:530.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:27 57-12-510/04/18 18:100.32 0.18 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride ND mg/kg 10/04/18 03:16 16984-48-810/02/18 09:006.3 3.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB014 (0'-1')Lab ID:92401224027 Collected:09/26/18 08:15 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/01/18 21:10 83-32-909/28/18 17:0712.4 1.9 1
Acenaphthylene 4.7J ug/kg 10/01/18 21:10 208-96-809/28/18 17:0712.4 1.6 1
Anthracene 5.5J ug/kg 10/01/18 21:10 120-12-709/28/18 17:0712.4 1.7 1
Benzo(a)anthracene 38.1 ug/kg 10/01/18 21:10 56-55-309/28/18 17:0712.4 0.88 1
Benzo(a)pyrene 43.0 ug/kg 10/01/18 21:10 50-32-809/28/18 17:0712.4 1.4 1
Benzo(b)fluoranthene 72.3 ug/kg 10/01/18 21:10 205-99-209/28/18 17:0712.4 0.83 1
Benzo(g,h,i)perylene 29.3 ug/kg 10/01/18 21:10 191-24-209/28/18 17:0712.4 3.2 1
Benzo(k)fluoranthene 20.7 ug/kg 10/01/18 21:10 207-08-909/28/18 17:0712.4 1.9 1
Chrysene 44.6 ug/kg 10/01/18 21:10 218-01-909/28/18 17:0712.4 2.2 1
Dibenz(a,h)anthracene 2.8J ug/kg 10/01/18 21:10 53-70-309/28/18 17:0712.4 2.2 1
Fluoranthene 70.9 ug/kg 10/01/18 21:10 206-44-009/28/18 17:0712.4 1.0 1
Fluorene ND ug/kg 10/01/18 21:10 86-73-709/28/18 17:0712.4 2.0 1
Indeno(1,2,3-cd)pyrene 28.7 ug/kg 10/01/18 21:10 193-39-509/28/18 17:0712.4 3.5 1
1-Methylnaphthalene 10.1J ug/kg 10/01/18 21:10 90-12-009/28/18 17:0712.4 1.5 1
2-Methylnaphthalene 11.9J ug/kg 10/01/18 21:10 91-57-609/28/18 17:0712.4 1.4 1
Naphthalene 8.8J ug/kg 10/01/18 21:10 91-20-309/28/18 17:0712.4 2.9 1
Phenanthrene 27.0 ug/kg 10/01/18 21:10 85-01-809/28/18 17:0712.4 1.9 1
Pyrene 59.2 ug/kg 10/01/18 21:10 129-00-009/28/18 17:0712.4 2.2 1
Surrogates
Nitrobenzene-d5 (S)75 %10/01/18 21:10 4165-60-009/28/18 17:0710-128 1
2-Fluorobiphenyl (S)67 %10/01/18 21:10 321-60-809/28/18 17:0710-110 1
Terphenyl-d14 (S)76 %10/01/18 21:10 1718-51-009/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 18.5 %09/27/18 17:540.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:28 57-12-510/04/18 18:100.32 0.18 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 57.3 mg/kg 10/04/18 03:38 16984-48-810/02/18 09:006.1 3.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB014 (4'-5')Lab ID:92401224028 Collected:09/26/18 08:20 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/01/18 21:31 83-32-909/28/18 17:0713.5 2.0 1
Acenaphthylene ND ug/kg 10/01/18 21:31 208-96-809/28/18 17:0713.5 1.8 1
Anthracene ND ug/kg 10/01/18 21:31 120-12-709/28/18 17:0713.5 1.9 1
Benzo(a)anthracene ND ug/kg 10/01/18 21:31 56-55-309/28/18 17:0713.5 0.96 1
Benzo(a)pyrene ND ug/kg 10/01/18 21:31 50-32-809/28/18 17:0713.5 1.5 1
Benzo(b)fluoranthene ND ug/kg 10/01/18 21:31 205-99-209/28/18 17:0713.5 0.91 1
Benzo(g,h,i)perylene ND ug/kg 10/01/18 21:31 191-24-209/28/18 17:0713.5 3.5 1
Benzo(k)fluoranthene ND ug/kg 10/01/18 21:31 207-08-909/28/18 17:0713.5 2.0 1
Chrysene ND ug/kg 10/01/18 21:31 218-01-909/28/18 17:0713.5 2.4 1
Dibenz(a,h)anthracene ND ug/kg 10/01/18 21:31 53-70-309/28/18 17:0713.5 2.4 1
Fluoranthene ND ug/kg 10/01/18 21:31 206-44-009/28/18 17:0713.5 1.1 1
Fluorene ND ug/kg 10/01/18 21:31 86-73-709/28/18 17:0713.5 2.2 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/01/18 21:31 193-39-509/28/18 17:0713.5 3.8 1
1-Methylnaphthalene ND ug/kg 10/01/18 21:31 90-12-009/28/18 17:0713.5 1.6 1
2-Methylnaphthalene ND ug/kg 10/01/18 21:31 91-57-609/28/18 17:0713.5 1.5 1
Naphthalene ND ug/kg 10/01/18 21:31 91-20-309/28/18 17:0713.5 3.1 1
Phenanthrene ND ug/kg 10/01/18 21:31 85-01-809/28/18 17:0713.5 2.0 1
Pyrene ND ug/kg 10/01/18 21:31 129-00-009/28/18 17:0713.5 2.4 1
Surrogates
Nitrobenzene-d5 (S)62 %10/01/18 21:31 4165-60-009/28/18 17:0710-128 1
2-Fluorobiphenyl (S)54 %10/01/18 21:31 321-60-809/28/18 17:0710-110 1
Terphenyl-d14 (S)65 %10/01/18 21:31 1718-51-009/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 25.8 %09/27/18 17:540.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:29 57-12-510/04/18 18:100.35 0.20 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 33.3 mg/kg 10/04/18 04:00 16984-48-810/02/18 09:006.7 3.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB015 (0'-1')Lab ID:92401224029 Collected:09/26/18 08:50 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/01/18 21:52 83-32-909/28/18 17:0712.3 1.8 1
Acenaphthylene ND ug/kg 10/01/18 21:52 208-96-809/28/18 17:0712.3 1.6 1
Anthracene ND ug/kg 10/01/18 21:52 120-12-709/28/18 17:0712.3 1.7 1
Benzo(a)anthracene 2.8J ug/kg 10/01/18 21:52 56-55-309/28/18 17:0712.3 0.87 1
Benzo(a)pyrene 2.9J ug/kg 10/01/18 21:52 50-32-809/28/18 17:0712.3 1.4 1
Benzo(b)fluoranthene 4.7J ug/kg 10/01/18 21:52 205-99-209/28/18 17:0712.3 0.82 1
Benzo(g,h,i)perylene ND ug/kg 10/01/18 21:52 191-24-209/28/18 17:0712.3 3.2 1
Benzo(k)fluoranthene ND ug/kg 10/01/18 21:52 207-08-909/28/18 17:0712.3 1.8 1
Chrysene 3.7J ug/kg 10/01/18 21:52 218-01-909/28/18 17:0712.3 2.2 1
Dibenz(a,h)anthracene ND ug/kg 10/01/18 21:52 53-70-309/28/18 17:0712.3 2.2 1
Fluoranthene 4.3J ug/kg 10/01/18 21:52 206-44-009/28/18 17:0712.3 1.0 1
Fluorene ND ug/kg 10/01/18 21:52 86-73-709/28/18 17:0712.3 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/01/18 21:52 193-39-509/28/18 17:0712.3 3.4 1
1-Methylnaphthalene 8.7J ug/kg 10/01/18 21:52 90-12-009/28/18 17:0712.3 1.5 1
2-Methylnaphthalene 12.4 ug/kg 10/01/18 21:52 91-57-609/28/18 17:0712.3 1.4 1
Naphthalene 8.8J ug/kg 10/01/18 21:52 91-20-309/28/18 17:0712.3 2.8 1
Phenanthrene 6.4J ug/kg 10/01/18 21:52 85-01-809/28/18 17:0712.3 1.8 1
Pyrene 3.8J ug/kg 10/01/18 21:52 129-00-009/28/18 17:0712.3 2.2 1
Surrogates
Nitrobenzene-d5 (S)64 %10/01/18 21:52 4165-60-009/28/18 17:0710-128 1
2-Fluorobiphenyl (S)59 %10/01/18 21:52 321-60-809/28/18 17:0710-110 1
Terphenyl-d14 (S)66 %10/01/18 21:52 1718-51-009/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.5 %09/27/18 17:540.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:32 57-12-510/04/18 18:100.32 0.18 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 149 mg/kg 10/04/18 11:39 16984-48-810/02/18 09:0062.1 31.1 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB015 (4'-5')Lab ID:92401224030 Collected:09/26/18 08:55 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/01/18 22:13 83-32-909/28/18 17:0711.6 1.7 1
Acenaphthylene ND ug/kg 10/01/18 22:13 208-96-809/28/18 17:0711.6 1.5 1
Anthracene ND ug/kg 10/01/18 22:13 120-12-709/28/18 17:0711.6 1.6 1
Benzo(a)anthracene ND ug/kg 10/01/18 22:13 56-55-309/28/18 17:0711.6 0.83 1
Benzo(a)pyrene ND ug/kg 10/01/18 22:13 50-32-809/28/18 17:0711.6 1.3 1
Benzo(b)fluoranthene ND ug/kg 10/01/18 22:13 205-99-209/28/18 17:0711.6 0.78 1
Benzo(g,h,i)perylene ND ug/kg 10/01/18 22:13 191-24-209/28/18 17:0711.6 3.0 1
Benzo(k)fluoranthene ND ug/kg 10/01/18 22:13 207-08-909/28/18 17:0711.6 1.7 1
Chrysene ND ug/kg 10/01/18 22:13 218-01-909/28/18 17:0711.6 2.1 1
Dibenz(a,h)anthracene ND ug/kg 10/01/18 22:13 53-70-309/28/18 17:0711.6 2.1 1
Fluoranthene ND ug/kg 10/01/18 22:13 206-44-009/28/18 17:0711.6 0.97 1
Fluorene ND ug/kg 10/01/18 22:13 86-73-709/28/18 17:0711.6 1.9 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/01/18 22:13 193-39-509/28/18 17:0711.6 3.3 1
1-Methylnaphthalene ND ug/kg 10/01/18 22:13 90-12-009/28/18 17:0711.6 1.4 1
2-Methylnaphthalene ND ug/kg 10/01/18 22:13 91-57-609/28/18 17:0711.6 1.3 1
Naphthalene ND ug/kg 10/01/18 22:13 91-20-309/28/18 17:0711.6 2.7 1
Phenanthrene ND ug/kg 10/01/18 22:13 85-01-809/28/18 17:0711.6 1.7 1
Pyrene ND ug/kg 10/01/18 22:13 129-00-009/28/18 17:0711.6 2.1 1
Surrogates
Nitrobenzene-d5 (S)56 %10/01/18 22:13 4165-60-009/28/18 17:0710-128 1
2-Fluorobiphenyl (S)53 %10/01/18 22:13 321-60-809/28/18 17:0710-110 1
Terphenyl-d14 (S)58 %10/01/18 22:13 1718-51-009/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.4 %09/27/18 17:540.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:33 57-12-510/04/18 18:100.29 0.17 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride ND mg/kg 10/04/18 04:44 16984-48-810/02/18 09:005.9 3.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB016 (0'-1')Lab ID:92401224031 Collected:09/26/18 09:40 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/01/18 22:34 83-32-909/28/18 17:0711.6 1.7 1
Acenaphthylene ND ug/kg 10/01/18 22:34 208-96-809/28/18 17:0711.6 1.5 1
Anthracene ND ug/kg 10/01/18 22:34 120-12-709/28/18 17:0711.6 1.6 1
Benzo(a)anthracene ND ug/kg 10/01/18 22:34 56-55-309/28/18 17:0711.6 0.83 1
Benzo(a)pyrene ND ug/kg 10/01/18 22:34 50-32-809/28/18 17:0711.6 1.3 1
Benzo(b)fluoranthene ND ug/kg 10/01/18 22:34 205-99-209/28/18 17:0711.6 0.78 1
Benzo(g,h,i)perylene ND ug/kg 10/01/18 22:34 191-24-209/28/18 17:0711.6 3.0 1
Benzo(k)fluoranthene ND ug/kg 10/01/18 22:34 207-08-909/28/18 17:0711.6 1.7 1
Chrysene ND ug/kg 10/01/18 22:34 218-01-909/28/18 17:0711.6 2.1 1
Dibenz(a,h)anthracene ND ug/kg 10/01/18 22:34 53-70-309/28/18 17:0711.6 2.1 1
Fluoranthene ND ug/kg 10/01/18 22:34 206-44-009/28/18 17:0711.6 0.97 1
Fluorene ND ug/kg 10/01/18 22:34 86-73-709/28/18 17:0711.6 1.9 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/01/18 22:34 193-39-509/28/18 17:0711.6 3.3 1
1-Methylnaphthalene ND ug/kg 10/01/18 22:34 90-12-009/28/18 17:0711.6 1.4 1
2-Methylnaphthalene ND ug/kg 10/01/18 22:34 91-57-609/28/18 17:0711.6 1.3 1
Naphthalene ND ug/kg 10/01/18 22:34 91-20-309/28/18 17:0711.6 2.7 1
Phenanthrene ND ug/kg 10/01/18 22:34 85-01-809/28/18 17:0711.6 1.7 1
Pyrene ND ug/kg 10/01/18 22:34 129-00-009/28/18 17:0711.6 2.1 1
Surrogates
Nitrobenzene-d5 (S)49 %10/01/18 22:34 4165-60-009/28/18 17:0710-128 1
2-Fluorobiphenyl (S)47 %10/01/18 22:34 321-60-809/28/18 17:0710-110 1
Terphenyl-d14 (S)50 %10/01/18 22:34 1718-51-009/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.3 %09/27/18 17:540.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:36 57-12-510/04/18 18:100.29 0.17 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 39.0 mg/kg 10/04/18 05:50 16984-48-8 M110/02/18 09:005.8 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB016 (4'-5')Lab ID:92401224032 Collected:09/26/18 09:45 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/01/18 22:55 83-32-909/28/18 17:0711.6 1.7 1
Acenaphthylene ND ug/kg 10/01/18 22:55 208-96-809/28/18 17:0711.6 1.5 1
Anthracene ND ug/kg 10/01/18 22:55 120-12-709/28/18 17:0711.6 1.6 1
Benzo(a)anthracene ND ug/kg 10/01/18 22:55 56-55-309/28/18 17:0711.6 0.82 1
Benzo(a)pyrene ND ug/kg 10/01/18 22:55 50-32-809/28/18 17:0711.6 1.3 1
Benzo(b)fluoranthene ND ug/kg 10/01/18 22:55 205-99-209/28/18 17:0711.6 0.78 1
Benzo(g,h,i)perylene ND ug/kg 10/01/18 22:55 191-24-209/28/18 17:0711.6 3.0 1
Benzo(k)fluoranthene ND ug/kg 10/01/18 22:55 207-08-909/28/18 17:0711.6 1.7 1
Chrysene ND ug/kg 10/01/18 22:55 218-01-909/28/18 17:0711.6 2.1 1
Dibenz(a,h)anthracene ND ug/kg 10/01/18 22:55 53-70-309/28/18 17:0711.6 2.1 1
Fluoranthene ND ug/kg 10/01/18 22:55 206-44-009/28/18 17:0711.6 0.96 1
Fluorene ND ug/kg 10/01/18 22:55 86-73-709/28/18 17:0711.6 1.9 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/01/18 22:55 193-39-509/28/18 17:0711.6 3.2 1
1-Methylnaphthalene ND ug/kg 10/01/18 22:55 90-12-009/28/18 17:0711.6 1.4 1
2-Methylnaphthalene ND ug/kg 10/01/18 22:55 91-57-609/28/18 17:0711.6 1.3 1
Naphthalene ND ug/kg 10/01/18 22:55 91-20-309/28/18 17:0711.6 2.7 1
Phenanthrene ND ug/kg 10/01/18 22:55 85-01-809/28/18 17:0711.6 1.7 1
Pyrene ND ug/kg 10/01/18 22:55 129-00-009/28/18 17:0711.6 2.1 1
Surrogates
Nitrobenzene-d5 (S)60 %10/01/18 22:55 4165-60-009/28/18 17:0710-128 1
2-Fluorobiphenyl (S)55 %10/01/18 22:55 321-60-809/28/18 17:0710-110 1
Terphenyl-d14 (S)59 %10/01/18 22:55 1718-51-009/28/18 17:0739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.0 %09/27/18 17:540.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:37 57-12-510/04/18 18:100.29 0.17 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 8.5 mg/kg 10/04/18 06:56 16984-48-810/02/18 09:005.8 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
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Page 39 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB017 (0'-1')Lab ID:92401224033 Collected:09/26/18 10:35 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/02/18 16:21 83-32-909/28/18 18:2412.1 1.8 1
Acenaphthylene ND ug/kg 10/02/18 16:21 208-96-809/28/18 18:2412.1 1.6 1
Anthracene ND ug/kg 10/02/18 16:21 120-12-709/28/18 18:2412.1 1.7 1
Benzo(a)anthracene 9.3J ug/kg 10/02/18 16:21 56-55-309/28/18 18:2412.1 0.86 1
Benzo(a)pyrene 2.2J ug/kg 10/02/18 16:21 50-32-809/28/18 18:2412.1 1.3 1
Benzo(b)fluoranthene 17.2 ug/kg 10/02/18 16:21 205-99-209/28/18 18:2412.1 0.81 1
Benzo(g,h,i)perylene 6.7J ug/kg 10/02/18 16:21 191-24-209/28/18 18:2412.1 3.1 1
Benzo(k)fluoranthene 6.3J ug/kg 10/02/18 16:21 207-08-909/28/18 18:2412.1 1.8 1
Chrysene 13.0 ug/kg 10/02/18 16:21 218-01-909/28/18 18:2412.1 2.2 1
Dibenz(a,h)anthracene ND ug/kg 10/02/18 16:21 53-70-309/28/18 18:2412.1 2.2 1
Fluoranthene 15.9 ug/kg 10/02/18 16:21 206-44-009/28/18 18:2412.1 1.0 1
Fluorene ND ug/kg 10/02/18 16:21 86-73-709/28/18 18:2412.1 1.9 1
Indeno(1,2,3-cd)pyrene 6.0J ug/kg 10/02/18 16:21 193-39-509/28/18 18:2412.1 3.4 1
1-Methylnaphthalene ND ug/kg 10/02/18 16:21 90-12-009/28/18 18:2412.1 1.4 1
2-Methylnaphthalene ND ug/kg 10/02/18 16:21 91-57-609/28/18 18:2412.1 1.3 1
Naphthalene ND ug/kg 10/02/18 16:21 91-20-309/28/18 18:2412.1 2.8 1
Phenanthrene 4.9J ug/kg 10/02/18 16:21 85-01-809/28/18 18:2412.1 1.8 1
Pyrene 21.4 ug/kg 10/02/18 16:21 129-00-009/28/18 18:2412.1 2.2 1
Surrogates
Nitrobenzene-d5 (S)71 %10/02/18 16:21 4165-60-009/28/18 18:2410-128 1
2-Fluorobiphenyl (S)67 %10/02/18 16:21 321-60-809/28/18 18:2410-110 1
Terphenyl-d14 (S)78 %10/02/18 16:21 1718-51-009/28/18 18:2439-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.4 %09/27/18 17:540.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:41 57-12-510/04/18 20:150.32 0.18 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 42.5J mg/kg 10/04/18 07:18 16984-48-810/02/18 09:0060.4 30.2 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
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Page 40 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:PBC-SB017 (4'-5')Lab ID:92401224034 Collected:09/26/18 10:40 Received:09/26/18 15:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 10/02/18 16:42 83-32-909/28/18 18:2412.3 1.8 1
Acenaphthylene ND ug/kg 10/02/18 16:42 208-96-809/28/18 18:2412.3 1.6 1
Anthracene ND ug/kg 10/02/18 16:42 120-12-709/28/18 18:2412.3 1.7 1
Benzo(a)anthracene ND ug/kg 10/02/18 16:42 56-55-309/28/18 18:2412.3 0.87 1
Benzo(a)pyrene ND ug/kg 10/02/18 16:42 50-32-809/28/18 18:2412.3 1.3 1
Benzo(b)fluoranthene ND ug/kg 10/02/18 16:42 205-99-209/28/18 18:2412.3 0.82 1
Benzo(g,h,i)perylene ND ug/kg 10/02/18 16:42 191-24-209/28/18 18:2412.3 3.2 1
Benzo(k)fluoranthene ND ug/kg 10/02/18 16:42 207-08-909/28/18 18:2412.3 1.8 1
Chrysene ND ug/kg 10/02/18 16:42 218-01-909/28/18 18:2412.3 2.2 1
Dibenz(a,h)anthracene ND ug/kg 10/02/18 16:42 53-70-309/28/18 18:2412.3 2.2 1
Fluoranthene ND ug/kg 10/02/18 16:42 206-44-009/28/18 18:2412.3 1.0 1
Fluorene ND ug/kg 10/02/18 16:42 86-73-709/28/18 18:2412.3 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/02/18 16:42 193-39-509/28/18 18:2412.3 3.4 1
1-Methylnaphthalene ND ug/kg 10/02/18 16:42 90-12-009/28/18 18:2412.3 1.5 1
2-Methylnaphthalene ND ug/kg 10/02/18 16:42 91-57-609/28/18 18:2412.3 1.3 1
Naphthalene ND ug/kg 10/02/18 16:42 91-20-309/28/18 18:2412.3 2.8 1
Phenanthrene ND ug/kg 10/02/18 16:42 85-01-809/28/18 18:2412.3 1.8 1
Pyrene ND ug/kg 10/02/18 16:42 129-00-009/28/18 18:2412.3 2.2 1
Surrogates
Nitrobenzene-d5 (S)71 %10/02/18 16:42 4165-60-009/28/18 18:2410-128 1
2-Fluorobiphenyl (S)65 %10/02/18 16:42 321-60-809/28/18 18:2410-110 1
Terphenyl-d14 (S)80 %10/02/18 16:42 1718-51-009/28/18 18:2439-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 18.2 %09/27/18 17:540.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/05/18 16:44 57-12-510/04/18 20:150.32 0.18 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 66.0 mg/kg 10/04/18 09:30 16984-48-810/02/18 09:006.1 3.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 41 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:ESW-EB001 Lab ID:92401224035 Collected:09/25/18 17:00 Received:09/26/18 15:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8082A Preparation Method: EPA 3510C8082 GCS PCB RVE
PCB-1016 (Aroclor 1016)ND ug/L 10/01/18 11:23 12674-11-209/28/18 15:160.42 0.42 1
PCB-1221 (Aroclor 1221)ND ug/L 10/01/18 11:23 11104-28-209/28/18 15:160.42 0.42 1
PCB-1232 (Aroclor 1232)ND ug/L 10/01/18 11:23 11141-16-509/28/18 15:160.42 0.42 1
PCB-1242 (Aroclor 1242)ND ug/L 10/01/18 11:23 53469-21-909/28/18 15:160.42 0.42 1
PCB-1248 (Aroclor 1248)ND ug/L 10/01/18 11:23 12672-29-609/28/18 15:160.42 0.42 1
PCB-1254 (Aroclor 1254)ND ug/L 10/01/18 11:23 11097-69-109/28/18 15:160.42 0.42 1
PCB-1260 (Aroclor 1260)ND ug/L 10/01/18 11:23 11096-82-509/28/18 15:160.42 0.42 1
Surrogates
Decachlorobiphenyl (S)58 %10/01/18 11:23 2051-24-309/28/18 15:1610-132 1
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35118270 Low Volume PAH SIM
Acenaphthene ND ug/L 10/03/18 14:23 83-32-9 L110/01/18 12:160.50 0.50 1
Acenaphthylene ND ug/L 10/03/18 14:23 208-96-8 L110/01/18 12:160.50 0.50 1
Anthracene ND ug/L 10/03/18 14:23 120-12-7 L110/01/18 12:160.050 0.050 1
Benzo(a)anthracene ND ug/L 10/03/18 14:23 56-55-3 L110/01/18 12:160.050 0.050 1
Benzo(a)pyrene ND ug/L 10/03/18 14:23 50-32-8 L110/01/18 12:160.10 0.10 1
Benzo(b)fluoranthene ND ug/L 10/03/18 14:23 205-99-2 L110/01/18 12:160.050 0.050 1
Benzo(g,h,i)perylene ND ug/L 10/03/18 14:23 191-24-2 L110/01/18 12:160.20 0.20 1
Benzo(k)fluoranthene ND ug/L 10/03/18 14:23 207-08-9 L110/01/18 12:160.20 0.20 1
Chrysene ND ug/L 10/03/18 14:23 218-01-9 L110/01/18 12:160.10 0.10 1
Dibenz(a,h)anthracene ND ug/L 10/03/18 14:23 53-70-3 L110/01/18 12:160.15 0.15 1
Fluoranthene ND ug/L 10/03/18 14:23 206-44-0 L110/01/18 12:160.30 0.30 1
Fluorene ND ug/L 10/03/18 14:23 86-73-7 L110/01/18 12:160.31 0.31 1
Indeno(1,2,3-cd)pyrene ND ug/L 10/03/18 14:23 193-39-5 L110/01/18 12:160.050 0.050 1
1-Methylnaphthalene ND ug/L 10/03/18 14:23 90-12-010/01/18 12:160.80 0.80 1
2-Methylnaphthalene ND ug/L 10/03/18 14:23 91-57-610/01/18 12:160.80 0.80 1
Naphthalene ND ug/L 10/03/18 14:23 91-20-310/01/18 12:161.5 1.5 1
Phenanthrene ND ug/L 10/03/18 14:23 85-01-8 L110/01/18 12:160.20 0.20 1
Pyrene ND ug/L 10/03/18 14:23 129-00-0 L110/01/18 12:160.10 0.10 1
Surrogates
Nitrobenzene-d5 (S)121 %10/03/18 14:23 4165-60-010/01/18 12:1670-130 1
2-Fluorobiphenyl (S)118 %10/03/18 14:23 321-60-810/01/18 12:1670-130 1
Terphenyl-d14 (S)115 %10/03/18 14:23 1718-51-010/01/18 12:1670-130 1
Analytical Method: EPA 8260B8260 MSV
Acetone ND ug/L 10/02/18 14:58 67-64-125.0 10.0 1
Benzene ND ug/L 10/02/18 14:58 71-43-25.0 1.7 1
Bromobenzene ND ug/L 10/02/18 14:58 108-86-15.0 1.5 1
Bromochloromethane ND ug/L 10/02/18 14:58 74-97-55.0 2.2 1
Bromodichloromethane ND ug/L 10/02/18 14:58 75-27-45.0 1.7 1
Bromoform ND ug/L 10/02/18 14:58 75-25-25.0 1.5 1
Bromomethane ND ug/L 10/02/18 14:58 74-83-910.0 2.5 1
2-Butanone (MEK)ND ug/L 10/02/18 14:58 78-93-310.0 4.9 1
tert-Butyl Alcohol ND ug/L 10/02/18 14:58 75-65-010057.7 1
n-Butylbenzene ND ug/L 10/02/18 14:58 104-51-85.0 1.9 1
sec-Butylbenzene ND ug/L 10/02/18 14:58 135-98-85.0 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:ESW-EB001 Lab ID:92401224035 Collected:09/25/18 17:00 Received:09/26/18 15:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B8260 MSV
tert-Butylbenzene ND ug/L 10/02/18 14:58 98-06-65.0 1.6 1
Carbon tetrachloride ND ug/L 10/02/18 14:58 56-23-55.0 1.9 1
Chlorobenzene ND ug/L 10/02/18 14:58 108-90-75.0 1.7 1
Chloroethane ND ug/L 10/02/18 14:58 75-00-310.0 1.6 1
Chloroform ND ug/L 10/02/18 14:58 67-66-35.0 1.9 1
Chloromethane ND ug/L 10/02/18 14:58 74-87-35.0 1.5 1
2-Chlorotoluene ND ug/L 10/02/18 14:58 95-49-85.0 1.5 1
4-Chlorotoluene ND ug/L 10/02/18 14:58 106-43-45.0 1.6 1
1,2-Dibromo-3-chloropropane ND ug/L 10/02/18 14:58 96-12-82.0 1.7 1
Dibromochloromethane ND ug/L 10/02/18 14:58 124-48-15.0 1.8 1
1,2-Dibromoethane (EDB)ND ug/L 10/02/18 14:58 106-93-45.0 1.7 1
Dibromomethane ND ug/L 10/02/18 14:58 74-95-35.0 2.0 1
1,2-Dichlorobenzene ND ug/L 10/02/18 14:58 95-50-15.0 1.5 1
1,3-Dichlorobenzene ND ug/L 10/02/18 14:58 541-73-15.0 1.5 1
1,4-Dichlorobenzene ND ug/L 10/02/18 14:58 106-46-75.0 1.5 1
Dichlorodifluoromethane ND ug/L 10/02/18 14:58 75-71-85.0 1.6 1
1,1-Dichloroethane ND ug/L 10/02/18 14:58 75-34-35.0 1.8 1
1,2-Dichloroethane ND ug/L 10/02/18 14:58 107-06-25.0 1.8 1
1,2-Dichloroethene (Total)ND ug/L 10/02/18 14:58 540-59-05.0 4.4 1
1,1-Dichloroethene ND ug/L 10/02/18 14:58 75-35-45.0 1.9 1
cis-1,2-Dichloroethene ND ug/L 10/02/18 14:58 156-59-25.0 1.8 1
trans-1,2-Dichloroethene ND ug/L 10/02/18 14:58 156-60-55.0 1.8 1
1,2-Dichloropropane ND ug/L 10/02/18 14:58 78-87-55.0 1.7 1
1,3-Dichloropropane ND ug/L 10/02/18 14:58 142-28-95.0 1.7 1
2,2-Dichloropropane ND ug/L 10/02/18 14:58 594-20-75.0 1.6 1
1,1-Dichloropropene ND ug/L 10/02/18 14:58 563-58-65.0 1.7 1
cis-1,3-Dichloropropene ND ug/L 10/02/18 14:58 10061-01-55.0 1.6 1
trans-1,3-Dichloropropene ND ug/L 10/02/18 14:58 10061-02-65.0 1.6 1
Diisopropyl ether ND ug/L 10/02/18 14:58 108-20-35.0 1.7 1
Ethylbenzene ND ug/L 10/02/18 14:58 100-41-45.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 10/02/18 14:58 87-68-35.0 1.8 1
2-Hexanone ND ug/L 10/02/18 14:58 591-78-610.0 3.8 1
Isopropylbenzene (Cumene)ND ug/L 10/02/18 14:58 98-82-85.0 1.6 1
p-Isopropyltoluene ND ug/L 10/02/18 14:58 99-87-65.0 1.6 1
Methylene Chloride ND ug/L 10/02/18 14:58 75-09-25.0 1.9 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/02/18 14:58 108-10-110.0 3.6 1
Methyl-tert-butyl ether ND ug/L 10/02/18 14:58 1634-04-45.0 1.7 1
Naphthalene ND ug/L 10/02/18 14:58 91-20-35.0 2.0 1
n-Propylbenzene ND ug/L 10/02/18 14:58 103-65-15.0 1.5 1
Styrene ND ug/L 10/02/18 14:58 100-42-55.0 1.6 1
1,1,1,2-Tetrachloroethane ND ug/L 10/02/18 14:58 630-20-65.0 1.7 1
1,1,2,2-Tetrachloroethane ND ug/L 10/02/18 14:58 79-34-55.0 1.5 1
Tetrachloroethene ND ug/L 10/02/18 14:58 127-18-45.0 1.8 1
Toluene ND ug/L 10/02/18 14:58 108-88-35.0 1.6 1
1,2,3-Trichlorobenzene ND ug/L 10/02/18 14:58 87-61-65.0 2.0 1
1,2,4-Trichlorobenzene ND ug/L 10/02/18 14:58 120-82-15.0 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 83
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Sample:ESW-EB001 Lab ID:92401224035 Collected:09/25/18 17:00 Received:09/26/18 15:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260B8260 MSV
1,1,1-Trichloroethane ND ug/L 10/02/18 14:58 71-55-65.0 1.9 1
1,1,2-Trichloroethane ND ug/L 10/02/18 14:58 79-00-55.0 1.7 1
Trichloroethene ND ug/L 10/02/18 14:58 79-01-65.0 1.8 1
Trichlorofluoromethane ND ug/L 10/02/18 14:58 75-69-410.0 1.7 1
1,2,3-Trichloropropane ND ug/L 10/02/18 14:58 96-18-45.0 1.5 1
1,2,4-Trimethylbenzene ND ug/L 10/02/18 14:58 95-63-65.0 1.5 1
1,3,5-Trimethylbenzene ND ug/L 10/02/18 14:58 108-67-85.0 1.3 1
Vinyl acetate ND ug/L 10/02/18 14:58 108-05-410.0 2.3 1
Vinyl chloride ND ug/L 10/02/18 14:58 75-01-45.0 1.5 1
m&p-Xylene ND ug/L 10/02/18 14:58 179601-23-110.0 3.1 1
o-Xylene ND ug/L 10/02/18 14:58 95-47-65.0 1.6 1
Surrogates
4-Bromofluorobenzene (S)95 %10/02/18 14:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %10/02/18 14:58 17060-07-070-130 1
Toluene-d8 (S)103 %10/02/18 14:58 2037-26-570-130 1
Analytical Method: EPA 9012B Preparation Method: EPA 9012B9012B Cyanide, Total
Cyanide ND mg/L 10/03/18 01:50 57-12-510/02/18 06:370.0080 0.0040 1
Analytical Method: EPA 9056A9056 IC anions 28 Days
Fluoride ND mg/L 09/29/18 08:32 16984-48-80.10 0.050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
433825
EPA 8260B
EPA 8260B
8260 MSV
Associated Lab Samples:92401224035
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2389677
Associated Lab Samples:92401224035
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 10/02/18 06:161.7
1,1,1-Trichloroethane ug/L ND 5.0 10/02/18 06:161.9
1,1,2,2-Tetrachloroethane ug/L ND 5.0 10/02/18 06:161.5
1,1,2-Trichloroethane ug/L ND 5.0 10/02/18 06:161.7
1,1-Dichloroethane ug/L ND 5.0 10/02/18 06:161.8
1,1-Dichloroethene ug/L ND 5.0 10/02/18 06:161.9
1,1-Dichloropropene ug/L ND 5.0 10/02/18 06:161.7
1,2,3-Trichlorobenzene ug/L ND 5.0 10/02/18 06:162.0
1,2,3-Trichloropropane ug/L ND 5.0 10/02/18 06:161.5
1,2,4-Trichlorobenzene ug/L ND 5.0 10/02/18 06:161.7
1,2,4-Trimethylbenzene ug/L ND 5.0 10/02/18 06:161.5
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/02/18 06:161.7
1,2-Dibromoethane (EDB)ug/L ND 5.0 10/02/18 06:161.7
1,2-Dichlorobenzene ug/L ND 5.0 10/02/18 06:161.5
1,2-Dichloroethane ug/L ND 5.0 10/02/18 06:161.8
1,2-Dichloroethene (Total)ug/L ND 5.0 10/02/18 06:164.4
1,2-Dichloropropane ug/L ND 5.0 10/02/18 06:161.7
1,3,5-Trimethylbenzene ug/L ND 5.0 10/02/18 06:161.3
1,3-Dichlorobenzene ug/L ND 5.0 10/02/18 06:161.5
1,3-Dichloropropane ug/L ND 5.0 10/02/18 06:161.7
1,4-Dichlorobenzene ug/L ND 5.0 10/02/18 06:161.5
2,2-Dichloropropane ug/L ND 5.0 10/02/18 06:161.6
2-Butanone (MEK)ug/L ND 10.0 10/02/18 06:164.9
2-Chlorotoluene ug/L ND 5.0 10/02/18 06:161.5
2-Hexanone ug/L ND 10.0 10/02/18 06:163.8
4-Chlorotoluene ug/L ND 5.0 10/02/18 06:161.6
4-Methyl-2-pentanone (MIBK)ug/L ND 10.0 10/02/18 06:163.6
Acetone ug/L ND 25.0 10/02/18 06:1610.0
Benzene ug/L ND 5.0 10/02/18 06:161.7
Bromobenzene ug/L ND 5.0 10/02/18 06:161.5
Bromochloromethane ug/L ND 5.0 10/02/18 06:162.2
Bromodichloromethane ug/L ND 5.0 10/02/18 06:161.7
Bromoform ug/L ND 5.0 10/02/18 06:161.5
Bromomethane ug/L ND 10.0 10/02/18 06:162.5
Carbon tetrachloride ug/L ND 5.0 10/02/18 06:161.9
Chlorobenzene ug/L ND 5.0 10/02/18 06:161.7
Chloroethane ug/L ND 10.0 10/02/18 06:161.6
Chloroform ug/L ND 5.0 10/02/18 06:161.9
Chloromethane ug/L ND 5.0 10/02/18 06:161.5
cis-1,2-Dichloroethene ug/L ND 5.0 10/02/18 06:161.8
cis-1,3-Dichloropropene ug/L ND 5.0 10/02/18 06:161.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
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Huntersville, NC 28078
[phone]
Page 45 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2389677
Associated Lab Samples:92401224035
Matrix:Water
AnalyzedMDL
Dibromochloromethane ug/L ND 5.0 10/02/18 06:161.8
Dibromomethane ug/L ND 5.0 10/02/18 06:162.0
Dichlorodifluoromethane ug/L ND 5.0 10/02/18 06:161.6
Diisopropyl ether ug/L ND 5.0 10/02/18 06:161.7
Ethylbenzene ug/L ND 5.0 10/02/18 06:161.6
Hexachloro-1,3-butadiene ug/L 3.8J 5.0 10/02/18 06:161.8
Isopropylbenzene (Cumene)ug/L ND 5.0 10/02/18 06:161.6
m&p-Xylene ug/L ND 10.0 10/02/18 06:163.1
Methyl-tert-butyl ether ug/L ND 5.0 10/02/18 06:161.7
Methylene Chloride ug/L ND 5.0 10/02/18 06:161.9
n-Butylbenzene ug/L ND 5.0 10/02/18 06:161.9
n-Propylbenzene ug/L ND 5.0 10/02/18 06:161.5
Naphthalene ug/L ND 5.0 10/02/18 06:162.0
o-Xylene ug/L ND 5.0 10/02/18 06:161.6
p-Isopropyltoluene ug/L ND 5.0 10/02/18 06:161.6
sec-Butylbenzene ug/L ND 5.0 10/02/18 06:161.7
Styrene ug/L ND 5.0 10/02/18 06:161.6
tert-Butyl Alcohol ug/L ND 100 10/02/18 06:1657.7
tert-Butylbenzene ug/L ND 5.0 10/02/18 06:161.6
Tetrachloroethene ug/L ND 5.0 10/02/18 06:161.8
Toluene ug/L ND 5.0 10/02/18 06:161.6
trans-1,2-Dichloroethene ug/L ND 5.0 10/02/18 06:161.8
trans-1,3-Dichloropropene ug/L ND 5.0 10/02/18 06:161.6
Trichloroethene ug/L ND 5.0 10/02/18 06:161.8
Trichlorofluoromethane ug/L ND 10.0 10/02/18 06:161.7
Vinyl acetate ug/L ND 10.0 10/02/18 06:162.3
Vinyl chloride ug/L ND 5.0 10/02/18 06:161.5
1,2-Dichloroethane-d4 (S)%99 70-130 10/02/18 06:16
4-Bromofluorobenzene (S)%97 70-130 10/02/18 06:16
Toluene-d8 (S)%104 70-130 10/02/18 06:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2389678LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.050 96 80-125
1,1,1-Trichloroethane ug/L 47.450 95 71-129
1,1,2,2-Tetrachloroethane ug/L 49.050 98 79-124
1,1,2-Trichloroethane ug/L 48.550 97 85-125
1,1-Dichloroethane ug/L 50.050 100 73-126
1,1-Dichloroethene ug/L 48.750 97 66-135
1,1-Dichloropropene ug/L 49.050 98 74-135
1,2,3-Trichlorobenzene ug/L 54.150 108 73-135
1,2,3-Trichloropropane ug/L 52.150 104 75-130
1,2,4-Trichlorobenzene ug/L 48.750 97 75-134
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
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Huntersville, NC 28078
[phone]
Page 46 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2389678LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/L 49.150 98 79-125
1,2-Dibromo-3-chloropropane ug/L 45.750 91 71-133
1,2-Dibromoethane (EDB)ug/L 49.550 99 83-124
1,2-Dichlorobenzene ug/L 53.850 108 80-133
1,2-Dichloroethane ug/L 48.350 97 67-128
1,2-Dichloroethene (Total)ug/L 98.6
1,2-Dichloropropane ug/L 54.550 109 75-132
1,3,5-Trimethylbenzene ug/L 48.150 96 79-123
1,3-Dichlorobenzene ug/L 52.150 104 77-130
1,3-Dichloropropane ug/L 51.050 102 76-131
1,4-Dichlorobenzene ug/L 52.150 104 78-130
2,2-Dichloropropane ug/L 44.550 89 40-160
2-Butanone (MEK)ug/L 92.5100 93 61-144
2-Chlorotoluene ug/L 49.150 98 74-132
2-Hexanone ug/L 96.9100 97 68-143
4-Chlorotoluene ug/L 54.150 108 76-133
4-Methyl-2-pentanone (MIBK)ug/L 93.0100 93 72-135
Acetone ug/L 93.1100 93 48-146
Benzene ug/L 53.650 107 80-125
Bromobenzene ug/L 53.150 106 75-125
Bromochloromethane ug/L 47.750 95 71-125
Bromodichloromethane ug/L 51.250 102 78-124
Bromoform ug/L 41.350 83 71-128
Bromomethane ug/L 32.950 66 40-160
Carbon tetrachloride ug/L 46.850 94 69-131
Chlorobenzene ug/L 53.750 107 81-122
Chloroethane ug/L 38.550 77 39-148
Chloroform ug/L 45.250 90 73-127
Chloromethane ug/L 35.150 70 44-146
cis-1,2-Dichloroethene ug/L 50.750 101 74-124
cis-1,3-Dichloropropene ug/L 47.450 95 72-132
Dibromochloromethane ug/L 46.350 93 78-125
Dibromomethane ug/L 52.950 106 82-120
Dichlorodifluoromethane ug/L 34.650 69 34-157
Diisopropyl ether ug/L 44.850 90 69-135
Ethylbenzene ug/L 52.250 104 79-121
Hexachloro-1,3-butadiene ug/L 49.250 98 72-131
Isopropylbenzene (Cumene)ug/L 51.250 102 81-132
m&p-Xylene ug/L 110100 110 81-124
Methyl-tert-butyl ether ug/L 49.350 99 74-131
Methylene Chloride ug/L 46.450 93 64-133
n-Butylbenzene ug/L 47.750 95 78-127
n-Propylbenzene ug/L 50.450 101 78-130
Naphthalene ug/L 47.950 96 73-133
o-Xylene ug/L 56.450 113 79-131
p-Isopropyltoluene ug/L 47.850 96 80-131
sec-Butylbenzene ug/L 50.150 100 80-133
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
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Huntersville, NC 28078
[phone]
Page 47 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2389678LABORATORY CONTROL SAMPLE:
LCSSpike
Styrene ug/L 48.850 98 84-126
tert-Butyl Alcohol ug/L 434500 87 36-136
tert-Butylbenzene ug/L 48.550 97 77-133
Tetrachloroethene ug/L 51.250 102 78-122
Toluene ug/L 50.050 100 80-121
trans-1,2-Dichloroethene ug/L 47.950 96 71-127
trans-1,3-Dichloropropene ug/L 47.350 95 69-141
Trichloroethene ug/L 49.850 100 78-122
Trichlorofluoromethane ug/L 37.250 74 53-137
Vinyl acetate ug/L 99.7100 100 40-160
Vinyl chloride ug/L 44.250 88 58-137
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2389679MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92400992001
2389680
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 200 97 70-130103 6 30200ND194205
1,1,1-Trichloroethane ug/L 200 105 70-130111 5 30200ND210222
1,1,2,2-Tetrachloroethane ug/L 200 101 70-130105 3 30200ND203209
1,1,2-Trichloroethane ug/L 200 99 70-130109 10 30200ND197217
1,1-Dichloroethane ug/L 200 104 70-130113 8 30200ND208225
1,1-Dichloroethene ug/L 200 99 65-160110 11 30200ND198221
1,1-Dichloropropene ug/L 200 106 70-130112 5 30200ND212223
1,2,3-Trichlorobenzene ug/L 200 101 70-130115 13 30200ND203231
1,2,3-Trichloropropane ug/L 200 107 70-130105 1 30200ND213211
1,2,4-Trichlorobenzene ug/L 200 99 70-130113 13 30200ND199227
1,2,4-Trimethylbenzene ug/L 200 103 70-130113 9 30200ND206225
1,2-Dibromo-3-
chloropropane ug/L 200 92 70-13098 6 30200ND185196
1,2-Dibromoethane (EDB)ug/L 200 98 60-139104 6 30200ND196208
1,2-Dichlorobenzene ug/L 200 104 70-130114 9 30200ND208228
1,2-Dichloroethane ug/L 200 97 70-130105 9 30200ND193211
1,2-Dichloroethene (Total)ug/L 7 30ND402432
1,2-Dichloropropane ug/L 200 107 70-130119 11 30200ND213239
1,3,5-Trimethylbenzene ug/L 200 104 70-130114 9 30200ND208227
1,3-Dichlorobenzene ug/L 200 102 70-130112 9 30200ND204224
1,3-Dichloropropane ug/L 200 103 70-130109 6 30200ND206218
1,4-Dichlorobenzene ug/L 200 102 70-130112 9 30200ND204224
2,2-Dichloropropane ug/L 200 96 70-130101 6 30200ND191203
2-Butanone (MEK)ug/L 400 86 70-13093 6 30400102445474
2-Chlorotoluene ug/L 200 104 70-130114 9 30200ND208228
2-Hexanone ug/L 400 102 70-130109 6 30400ND409437
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2389679MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92400992001
2389680
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
4-Chlorotoluene ug/L 200 106 70-130117 10 30200ND212234
4-Methyl-2-pentanone
(MIBK)ug/L 400 83 70-13088 5 30400ND410432
Acetone ug/L M1400-30 70-130-18 6 30400982860911
Benzene ug/L 200 108 58-162118 10 30200ND215237
Bromobenzene ug/L 200 102 70-130113 10 30200ND204226
Bromochloromethane ug/L 200 95 70-130103 8 30200ND190205
Bromodichloromethane ug/L 200 98 70-130109 10 30200ND197217
Bromoform ug/L 200 84 70-13088 5 30200ND168177
Bromomethane ug/L 200 85 70-13093 9 30200ND169186
Carbon tetrachloride ug/L 200 103 70-130111 8 30200ND206222
Chlorobenzene ug/L 200 106 70-138113 7 30200ND211226
Chloroethane ug/L 200 80 70-13092 14 30200ND159184
Chloroform ug/L 200 97 70-130104 6 30200ND195208
Chloromethane ug/L 200 77 70-13084 8 30200ND154168
cis-1,2-Dichloroethene ug/L 200 102 70-130108 7 30200ND203217
cis-1,3-Dichloropropene ug/L 200 95 70-130103 8 30200ND191206
Dibromochloromethane ug/L 200 93 70-13099 7 30200ND186199
Dibromomethane ug/L 200 103 70-130113 9 30200ND206226
Dichlorodifluoromethane ug/L 200 73 70-13078 7 30200ND146156
Diisopropyl ether ug/L 200 95 70-13097 2 30200ND189193
Ethylbenzene ug/L 200 106 22-189115 9 30200ND212231
Hexachloro-1,3-butadiene ug/L 200 107 70-130119 11 30200ND215239
Isopropylbenzene (Cumene)ug/L 200 109 70-130120 10 30200ND217240
m&p-Xylene ug/L 400 109 32-193119 9 30400ND438477
Methyl-tert-butyl ether ug/L 200 95 37-169104 9 30200ND189208
Methylene Chloride ug/L 200 106 70-130110 4 30200ND211220
n-Butylbenzene ug/L 200 103 70-130114 10 30200ND207229
n-Propylbenzene ug/L 200 107 70-130117 9 30200ND213234
Naphthalene ug/L 200 96 19-212104 9 30200ND191209
o-Xylene ug/L 200 109 70-135119 9 30200ND217238
p-Isopropyltoluene ug/L 200 104 70-130114 9 30200ND208228
sec-Butylbenzene ug/L 200 108 70-130120 11 30200ND216240
Styrene ug/L 200 102 70-130109 7 30200ND204219
tert-Butyl Alcohol ug/L 2000 116 70-130124 7 302000ND23102480
tert-Butylbenzene ug/L 200 91 70-13099 8 30200ND183198
Tetrachloroethene ug/L 200 103 70-130112 8 30200ND207224
Toluene ug/L 200 100 65-152108 7 30200ND232248
trans-1,2-Dichloroethene ug/L 200 99 70-130108 8 30200ND199215
trans-1,3-Dichloropropene ug/L 200 96 70-130102 6 30200ND193205
Trichloroethene ug/L 200 106 70-142116 9 30200ND212231
Trichlorofluoromethane ug/L 200 89 70-13095 6 30200ND179190
Vinyl acetate ug/L 400 106 70-130112 6 30400ND423450
Vinyl chloride ug/L 200 91 70-130100 9 30200ND182200
1,2-Dichloroethane-d4 (S)%92 70-13092
4-Bromofluorobenzene (S)%100 70-130102
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2389679MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92400992001
2389680
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Toluene-d8 (S)%97 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
433423
EPA 3510C
EPA 8082A
8082 GCS PCB
Associated Lab Samples:92401224035
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2388086
Associated Lab Samples:92401224035
Matrix:Water
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/L ND 0.50 10/01/18 14:460.50
PCB-1221 (Aroclor 1221)ug/L ND 0.50 10/01/18 14:460.50
PCB-1232 (Aroclor 1232)ug/L ND 0.50 10/01/18 14:460.50
PCB-1242 (Aroclor 1242)ug/L ND 0.50 10/01/18 14:460.50
PCB-1248 (Aroclor 1248)ug/L ND 0.50 10/01/18 14:460.50
PCB-1254 (Aroclor 1254)ug/L ND 0.50 10/01/18 14:460.50
PCB-1260 (Aroclor 1260)ug/L ND 0.50 10/01/18 14:460.50
Decachlorobiphenyl (S)%96 10-132 10/01/18 14:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2388087LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2388088
PCB-1016 (Aroclor 1016)ug/L 4.05 79 50-1501075.4 30 30
PCB-1260 (Aroclor 1260)ug/L 4.05 80 50-1501025.1 24 30
Decachlorobiphenyl (S)%S07710-132182
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
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[phone]
Page 51 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
433443
EPA 3546
EPA 8270D by SIM
8270 MSSV PAH by SIM
Associated Lab Samples:92401224001, 92401224002, 92401224003, 92401224004, 92401224005, 92401224006, 92401224007,
92401224008, 92401224009, 92401224010, 92401224011, 92401224012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2388169
Associated Lab Samples:92401224001, 92401224002, 92401224003, 92401224004, 92401224005, 92401224006, 92401224007,
92401224008, 92401224009, 92401224010, 92401224011, 92401224012
Matrix:Solid
AnalyzedMDL
1-Methylnaphthalene ug/kg ND 10 10/02/18 10:571.2
2-Methylnaphthalene ug/kg ND 10 10/02/18 10:571.1
Acenaphthene ug/kg ND 10 10/02/18 10:571.5
Acenaphthylene ug/kg ND 10 10/02/18 10:571.3
Anthracene ug/kg ND 10 10/02/18 10:571.4
Benzo(a)anthracene ug/kg ND 10 10/02/18 10:570.71
Benzo(a)pyrene ug/kg ND 10 10/02/18 10:571.1
Benzo(b)fluoranthene ug/kg ND 10 10/02/18 10:570.67
Benzo(g,h,i)perylene ug/kg ND 10 10/02/18 10:572.6
Benzo(k)fluoranthene ug/kg ND 10 10/02/18 10:571.5
Chrysene ug/kg ND 10 10/02/18 10:571.8
Dibenz(a,h)anthracene ug/kg ND 10 10/02/18 10:571.8
Fluoranthene ug/kg ND 10 10/02/18 10:570.83
Fluorene ug/kg ND 10 10/02/18 10:571.6
Indeno(1,2,3-cd)pyrene ug/kg ND 10 10/02/18 10:572.8
Naphthalene ug/kg ND 10 10/02/18 10:572.3
Phenanthrene ug/kg ND 10 10/02/18 10:571.5
Pyrene ug/kg ND 10 10/02/18 10:571.8
2-Fluorobiphenyl (S)%88 10-110 10/02/18 10:57
Nitrobenzene-d5 (S)%98 10-128 10/02/18 10:57
Terphenyl-d14 (S)%101 39-119 10/02/18 10:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2388171LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/kg 30.133.8 89 44-130
2-Methylnaphthalene ug/kg 31.133.8 92 41-134
Acenaphthene ug/kg 31.833.8 94 52-123
Acenaphthylene ug/kg 30.633.8 90 49-116
Anthracene ug/kg 31.833.8 94 41-133
Benzo(a)anthracene ug/kg 31.933.8 94 56-130
Benzo(a)pyrene ug/kg 31.033.8 92 51-136
Benzo(b)fluoranthene ug/kg 34.633.8 102 37-149
Benzo(g,h,i)perylene ug/kg 29.333.8 87 39-127
Benzo(k)fluoranthene ug/kg 31.933.8 94 45-139
Chrysene ug/kg 32.433.8 96 59-127
Dibenz(a,h)anthracene ug/kg 32.933.8 97 37-139
Fluoranthene ug/kg 32.333.8 96 53-132
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 52 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2388171LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 32.133.8 95 45-127
Indeno(1,2,3-cd)pyrene ug/kg 33.633.8 99 35-145
Naphthalene ug/kg 29.533.8 87 45-123
Phenanthrene ug/kg 31.633.8 93 50-125
Pyrene ug/kg 32.233.8 95 52-132
2-Fluorobiphenyl (S)%93 10-110
Nitrobenzene-d5 (S)%99 10-128
Terphenyl-d14 (S)%99 39-119
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2388172MATRIX SPIKE SAMPLE:
MSSpike
Result
92401224001
1-Methylnaphthalene ug/kg 33.540.6 78 50-1502.0J
2-Methylnaphthalene ug/kg 37.240.6 84 50-1503.1J
Acenaphthene ug/kg 30.840.6 74 50-150ND
Acenaphthylene ug/kg 27.740.6 67 50-150ND
Anthracene ug/kg 33.640.6 77 50-1502.5J
Benzo(a)anthracene ug/kg 80.440.6 117 50-15032.8
Benzo(a)pyrene ug/kg 83.340.6 82 50-15050.1
Benzo(b)fluoranthene ug/kg 12740.6 79 50-15094.8
Benzo(g,h,i)perylene ug/kg 76.5 M140.6 42 50-15059.4
Benzo(k)fluoranthene ug/kg 59.240.6 67 50-15031.9
Chrysene ug/kg 82.240.6 110 50-15037.5
Dibenz(a,h)anthracene ug/kg 39.340.6 85 50-1504.7J
Fluoranthene ug/kg 101 M140.6 154 50-15038.2
Fluorene ug/kg 30.540.6 74 50-150ND
Indeno(1,2,3-cd)pyrene ug/kg 74.340.6 53 50-15052.6
Naphthalene ug/kg 36.840.6 84 50-1502.8J
Phenanthrene ug/kg 55.340.6 105 50-15012.7
Pyrene ug/kg 89.340.6 132 50-15035.5
2-Fluorobiphenyl (S)%72 10-110
Nitrobenzene-d5 (S)%78 10-128
Terphenyl-d14 (S)%74 39-119
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92401224002
2388173SAMPLE DUPLICATE:
1-Methylnaphthalene ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92401224002
2388173SAMPLE DUPLICATE:
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2-Fluorobiphenyl (S)%70 977
Nitrobenzene-d5 (S)%77 984
Terphenyl-d14 (S)%80 584
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
433445
EPA 3546
EPA 8270D by SIM
8270 MSSV PAH by SIM
Associated Lab Samples:92401224013, 92401224014, 92401224015, 92401224016, 92401224017, 92401224018, 92401224019,
92401224020, 92401224021, 92401224022, 92401224023, 92401224024, 92401224025, 92401224026,
92401224027, 92401224028, 92401224029, 92401224030, 92401224031, 92401224032
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2388178
Associated Lab Samples:92401224013, 92401224014, 92401224015, 92401224016, 92401224017, 92401224018, 92401224019,
92401224020, 92401224021, 92401224022, 92401224023, 92401224024, 92401224025, 92401224026,
92401224027, 92401224028, 92401224029, 92401224030, 92401224031, 92401224032
Matrix:Solid
AnalyzedMDL
1-Methylnaphthalene ug/kg ND 10.0 10/01/18 14:521.2
2-Methylnaphthalene ug/kg ND 10.0 10/01/18 14:521.1
Acenaphthene ug/kg ND 10.0 10/01/18 14:521.5
Acenaphthylene ug/kg ND 10.0 10/01/18 14:521.3
Anthracene ug/kg ND 10.0 10/01/18 14:521.4
Benzo(a)anthracene ug/kg ND 10.0 10/01/18 14:520.71
Benzo(a)pyrene ug/kg ND 10.0 10/01/18 14:521.1
Benzo(b)fluoranthene ug/kg ND 10.0 10/01/18 14:520.67
Benzo(g,h,i)perylene ug/kg ND 10.0 10/01/18 14:522.6
Benzo(k)fluoranthene ug/kg ND 10.0 10/01/18 14:521.5
Chrysene ug/kg ND 10.0 10/01/18 14:521.8
Dibenz(a,h)anthracene ug/kg ND 10.0 10/01/18 14:521.8
Fluoranthene ug/kg ND 10.0 10/01/18 14:520.83
Fluorene ug/kg ND 10.0 10/01/18 14:521.6
Indeno(1,2,3-cd)pyrene ug/kg ND 10.0 10/01/18 14:522.8
Naphthalene ug/kg ND 10.0 10/01/18 14:522.3
Phenanthrene ug/kg ND 10.0 10/01/18 14:521.5
Pyrene ug/kg ND 10.0 10/01/18 14:521.8
2-Fluorobiphenyl (S)%78 10-110 10/01/18 14:52
Nitrobenzene-d5 (S)%83 10-128 10/01/18 14:52
Terphenyl-d14 (S)%83 39-119 10/01/18 14:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2388179LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/kg 19.533.6 58 44-130
2-Methylnaphthalene ug/kg 20.133.6 60 41-134
Acenaphthene ug/kg 20.733.6 62 52-123
Acenaphthylene ug/kg 19.033.6 57 49-116
Anthracene ug/kg 20.733.6 62 41-133
Benzo(a)anthracene ug/kg 20.833.6 62 56-130
Benzo(a)pyrene ug/kg 20.533.6 61 51-136
Benzo(b)fluoranthene ug/kg 22.433.6 67 37-149
Benzo(g,h,i)perylene ug/kg 19.033.6 57 39-127
Benzo(k)fluoranthene ug/kg 19.933.6 59 45-139
Chrysene ug/kg 21.133.6 63 59-127
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2388179LABORATORY CONTROL SAMPLE:
LCSSpike
Dibenz(a,h)anthracene ug/kg 21.033.6 63 37-139
Fluoranthene ug/kg 20.933.6 62 53-132
Fluorene ug/kg 20.233.6 60 45-127
Indeno(1,2,3-cd)pyrene ug/kg 21.633.6 64 35-145
Naphthalene ug/kg 19.333.6 58 45-123
Phenanthrene ug/kg 20.833.6 62 50-125
Pyrene ug/kg 21.033.6 63 52-132
2-Fluorobiphenyl (S)%58 10-110
Nitrobenzene-d5 (S)%61 10-128
Terphenyl-d14 (S)%60 39-119
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2388180MATRIX SPIKE SAMPLE:
MSSpike
Result
92401224013
1-Methylnaphthalene ug/kg 28.4 M141.7 39 50-15012.0J
2-Methylnaphthalene ug/kg 30.1 M141.7 30 50-15017.6
Acenaphthene ug/kg 27.941.7 65 50-150ND
Acenaphthylene ug/kg 25.741.7 62 50-150ND
Anthracene ug/kg 27.641.7 60 50-1502.4J
Benzo(a)anthracene ug/kg 25.8 M141.7 28 50-15014.1
Benzo(a)pyrene ug/kg 23.5 M141.7 22 50-15014.2
Benzo(b)fluoranthene ug/kg 28.8 M141.7 10 50-15024.6
Benzo(g,h,i)perylene ug/kg 20.5 M141.7 19 50-15012.5J
Benzo(k)fluoranthene ug/kg 22.8 M141.7 32 50-1509.3J
Chrysene ug/kg 27.1 M141.7 29 50-15015.0
Dibenz(a,h)anthracene ug/kg 20.7 M141.7 41 50-1503.8J
Fluoranthene ug/kg 31.4 M141.7 21 50-15022.7
Fluorene ug/kg 27.441.7 64 50-150ND
Indeno(1,2,3-cd)pyrene ug/kg 22.4 M141.7 29 50-15010.5J
Naphthalene ug/kg 28.5 M141.7 34 50-15014.5
Phenanthrene ug/kg 30.2 M141.7 32 50-15016.8
Pyrene ug/kg 30.5 M141.7 27 50-15019.4
2-Fluorobiphenyl (S)%62 10-110
Nitrobenzene-d5 (S)%70 10-128
Terphenyl-d14 (S)%51 39-119
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92401224014
2388181SAMPLE DUPLICATE:
1-Methylnaphthalene ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Anthracene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92401224014
2388181SAMPLE DUPLICATE:
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg 2.2J 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2-Fluorobiphenyl (S)%58 2147
Nitrobenzene-d5 (S)%61 2547
Terphenyl-d14 (S)%62 2548
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
433447
EPA 3546
EPA 8270D by SIM
8270 MSSV PAH by SIM
Associated Lab Samples:92401224033, 92401224034
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2388190
Associated Lab Samples:92401224033, 92401224034
Matrix:Solid
AnalyzedMDL
1-Methylnaphthalene ug/kg ND 9.8 10/02/18 10:361.2
2-Methylnaphthalene ug/kg ND 9.8 10/02/18 10:361.1
Acenaphthene ug/kg ND 9.8 10/02/18 10:361.5
Acenaphthylene ug/kg ND 9.8 10/02/18 10:361.3
Anthracene ug/kg ND 9.8 10/02/18 10:361.4
Benzo(a)anthracene ug/kg ND 9.8 10/02/18 10:360.70
Benzo(a)pyrene ug/kg ND 9.8 10/02/18 10:361.1
Benzo(b)fluoranthene ug/kg ND 9.8 10/02/18 10:360.66
Benzo(g,h,i)perylene ug/kg ND 9.8 10/02/18 10:362.6
Benzo(k)fluoranthene ug/kg ND 9.8 10/02/18 10:361.5
Chrysene ug/kg ND 9.8 10/02/18 10:361.8
Dibenz(a,h)anthracene ug/kg ND 9.8 10/02/18 10:361.8
Fluoranthene ug/kg ND 9.8 10/02/18 10:360.82
Fluorene ug/kg ND 9.8 10/02/18 10:361.6
Indeno(1,2,3-cd)pyrene ug/kg ND 9.8 10/02/18 10:362.8
Naphthalene ug/kg ND 9.8 10/02/18 10:362.3
Phenanthrene ug/kg ND 9.8 10/02/18 10:361.5
Pyrene ug/kg ND 9.8 10/02/18 10:361.8
2-Fluorobiphenyl (S)%72 10-110 10/02/18 10:36
Nitrobenzene-d5 (S)%79 10-128 10/02/18 10:36
Terphenyl-d14 (S)%86 39-119 10/02/18 10:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2388191LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2388192
1-Methylnaphthalene ug/kg 25.833.1 78 44-1308227.4 6 30
2-Methylnaphthalene ug/kg 27.033.1 82 41-1348528.7 6 30
Acenaphthene ug/kg 27.333.1 82 52-1238829.5 8 30
Acenaphthylene ug/kg 26.633.1 80 49-1168528.6 7 30
Anthracene ug/kg 27.833.1 84 41-1338729.4 5 30
Benzo(a)anthracene ug/kg 28.333.1 85 56-1308729.2 3 30
Benzo(a)pyrene ug/kg 27.833.1 84 51-1368628.9 4 30
Benzo(b)fluoranthene ug/kg 31.433.1 95 37-1499431.6 1 30
Benzo(g,h,i)perylene ug/kg 25.433.1 77 39-1277826.3 3 30
Benzo(k)fluoranthene ug/kg 28.733.1 87 45-1398829.7 4 30
Chrysene ug/kg 28.833.1 87 59-1278829.7 3 30
Dibenz(a,h)anthracene ug/kg 28.633.1 86 37-1398729.2 2 30
Fluoranthene ug/kg 28.833.1 87 53-1328929.8 3 30
Fluorene ug/kg 27.833.1 84 45-1278629.1 5 30
Indeno(1,2,3-cd)pyrene ug/kg 29.333.1 89 35-1458930.0 2 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2388191LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2388192
Naphthalene ug/kg 25.333.1 76 45-1238127.2 7 30
Phenanthrene ug/kg 27.333.1 82 50-1258628.9 6 30
Pyrene ug/kg 28.533.1 86 52-1328930.1 5 30
2-Fluorobiphenyl (S)%77 10-11082
Nitrobenzene-d5 (S)%85 10-12890
Terphenyl-d14 (S)%85 39-11991
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
433661
EPA 3511
EPA 8270D by SIM
8270 3511 Low Volume PAH SIM
Associated Lab Samples:92401224035
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2389133
Associated Lab Samples:92401224035
Matrix:Water
AnalyzedMDL
1-Methylnaphthalene ug/L ND 0.80 10/03/18 12:370.80
2-Methylnaphthalene ug/L ND 0.80 10/03/18 12:370.80
Acenaphthene ug/L ND 0.50 10/03/18 12:370.50
Acenaphthylene ug/L ND 0.50 10/03/18 12:370.50
Anthracene ug/L ND 0.050 10/03/18 12:370.050
Benzo(a)anthracene ug/L ND 0.050 10/03/18 12:370.050
Benzo(a)pyrene ug/L ND 0.10 10/03/18 12:370.10
Benzo(b)fluoranthene ug/L ND 0.050 10/03/18 12:370.050
Benzo(g,h,i)perylene ug/L ND 0.20 10/03/18 12:370.20
Benzo(k)fluoranthene ug/L ND 0.20 10/03/18 12:370.20
Chrysene ug/L ND 0.10 10/03/18 12:370.10
Dibenz(a,h)anthracene ug/L ND 0.15 10/03/18 12:370.15
Fluoranthene ug/L ND 0.30 10/03/18 12:370.30
Fluorene ug/L ND 0.31 10/03/18 12:370.31
Indeno(1,2,3-cd)pyrene ug/L ND 0.050 10/03/18 12:370.050
Naphthalene ug/L ND 1.5 10/03/18 12:371.5
Phenanthrene ug/L ND 0.20 10/03/18 12:370.20
Pyrene ug/L ND 0.10 10/03/18 12:370.10
2-Fluorobiphenyl (S)%132 70-130 S310/03/18 12:37
Nitrobenzene-d5 (S)%135 70-130 S310/03/18 12:37
Terphenyl-d14 (S)%124 70-130 10/03/18 12:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2389134LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/L 3.12.5 124 70-130
2-Methylnaphthalene ug/L 3.22.5 127 70-130
Acenaphthene ug/L 3.5 L12.5 142 70-130
Acenaphthylene ug/L 3.5 L12.5 141 70-130
Anthracene ug/L 3.9 L12.5 157 70-130
Benzo(a)anthracene ug/L 3.8 L12.5 151 70-130
Benzo(a)pyrene ug/L 3.7 L12.5 149 70-130
Benzo(b)fluoranthene ug/L 4.1 L12.5 165 70-130
Benzo(g,h,i)perylene ug/L 3.3 L12.5 134 70-130
Benzo(k)fluoranthene ug/L 4.0 L12.5 160 70-130
Chrysene ug/L 3.9 L12.5 156 70-130
Dibenz(a,h)anthracene ug/L 3.7 L12.5 147 70-130
Fluoranthene ug/L 4.0 L12.5 159 70-130
Fluorene ug/L 3.5 L12.5 140 70-130
Indeno(1,2,3-cd)pyrene ug/L 3.9 L12.5 154 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2389134LABORATORY CONTROL SAMPLE:
LCSSpike
Naphthalene ug/L 3.32.5 130 70-130
Phenanthrene ug/L 3.9 L12.5 156 70-130
Pyrene ug/L 3.9 L12.5 156 70-130
2-Fluorobiphenyl (S)%128 70-130
Nitrobenzene-d5 (S)%S013670-130
Terphenyl-d14 (S)%118 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2389135MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92400858001
2389136
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1-Methylnaphthalene ug/L M12.5 -1 70-13053 302.5ND ND 1.3
2-Methylnaphthalene ug/L M12.5 -1 70-13053 302.5ND ND 1.4
Acenaphthene ug/L M02.5 0 70-13063 302.5ND ND 1.6
Acenaphthylene ug/L M02.5 0 70-13061 302.5ND ND 1.5
Anthracene ug/L M02.5 -7 70-13062 302.50.086 ND 1.7
Benzo(a)anthracene ug/L M02.5 0 70-13062 302.5ND ND 1.6
Benzo(a)pyrene ug/L M02.5 0 70-13067 302.5ND ND 1.7
Benzo(b)fluoranthene ug/L M02.5 0 70-13071 302.5ND ND 1.8
Benzo(g,h,i)perylene ug/L M02.5 0 70-13052 302.5ND ND 1.3
Benzo(k)fluoranthene ug/L M02.5 0 70-13080 302.5ND ND 2.0
Chrysene ug/L M02.5 0 70-13072 302.5ND ND 1.8
Dibenz(a,h)anthracene ug/L M02.5 0 70-13050 302.5ND ND 1.2
Fluoranthene ug/L M02.5 0 70-13064 302.5ND ND 1.6
Fluorene ug/L M02.5 0 70-13062 302.5ND ND 1.6
Indeno(1,2,3-cd)pyrene ug/L M02.5 0 70-13055 302.5ND ND 1.4
Naphthalene ug/L M12.5 -8 70-13050 302.5ND ND ND
Phenanthrene ug/L M02.5 0 70-13067 302.5ND ND 1.7
Pyrene ug/L M02.5 -1 70-13061 302.5ND ND 1.5
2-Fluorobiphenyl (S)%S0070-13053
Nitrobenzene-d5 (S)%S0070-13070
Terphenyl-d14 (S)%S0070-13047
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
433173
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92401224002, 92401224003, 92401224004, 92401224005, 92401224006, 92401224007, 92401224008,
92401224009, 92401224010, 92401224011, 92401224012, 92401224013, 92401224014, 92401224015,
92401224016, 92401224017, 92401224018
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92401023029
2387221SAMPLE DUPLICATE:
Percent Moisture %19.5 D6432512.6
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92401224018
2387222SAMPLE DUPLICATE:
Percent Moisture %15.1 3 2515.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
433175
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92401224019, 92401224020, 92401224021, 92401224022, 92401224023, 92401224024, 92401224025,
92401224026, 92401224027, 92401224028, 92401224029, 92401224030, 92401224031, 92401224032,
92401224033, 92401224034
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400988001
2387265SAMPLE DUPLICATE:
Percent Moisture %6.4 9 257.0
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92401224034
2387266SAMPLE DUPLICATE:
Percent Moisture %16.7 8 2518.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
433178
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92401224001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92401183013
2387274SAMPLE DUPLICATE:
Percent Moisture %17.2 8 2518.7
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400899002
2387275SAMPLE DUPLICATE:
Percent Moisture %13.8 5 2514.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
483046
EPA 9012
EPA 9012
9012 Cyanide
Associated Lab Samples:92401224001, 92401224002, 92401224003, 92401224004, 92401224005, 92401224006, 92401224007,
92401224008, 92401224009, 92401224010, 92401224011, 92401224012, 92401224013, 92401224014,
92401224015, 92401224016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2613729
Associated Lab Samples:92401224001, 92401224002, 92401224003, 92401224004, 92401224005, 92401224006, 92401224007,
92401224008, 92401224009, 92401224010, 92401224011, 92401224012, 92401224013, 92401224014,
92401224015, 92401224016
Matrix:Solid
AnalyzedMDL
Cyanide mg/kg ND 0.24 10/05/18 15:430.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2613730LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide mg/kg 1.31.2 105 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2613731MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92401224001
2613732
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/kg M1,R1.754 110 80-12078 28 20.754ND 0.96 0.72
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2613733MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92401224012
2613734
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/kg .815 117 80-120110 7 20.803ND 0.95 0.88
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
483047
EPA 9012
EPA 9012
9012 Cyanide
Associated Lab Samples:92401224017, 92401224018, 92401224019, 92401224020, 92401224021, 92401224022, 92401224023,
92401224024, 92401224025, 92401224026, 92401224027, 92401224028, 92401224029, 92401224030,
92401224031, 92401224032
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2613735
Associated Lab Samples:92401224017, 92401224018, 92401224019, 92401224020, 92401224021, 92401224022, 92401224023,
92401224024, 92401224025, 92401224026, 92401224027, 92401224028, 92401224029, 92401224030,
92401224031, 92401224032
Matrix:Solid
AnalyzedMDL
Cyanide mg/kg ND 0.25 10/05/18 16:120.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2613736LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide mg/kg 1.31.2 108 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2613737MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92401224017
2613738
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/kg .756 119 80-120109 8 20.756ND 0.98 0.91
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2613739MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92401224028
2613740
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/kg .89 96 80-120102 6 20.89ND 0.88 0.93
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
483049
EPA 9012
EPA 9012
9012 Cyanide
Associated Lab Samples:92401224033, 92401224034
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2613741
Associated Lab Samples:92401224033, 92401224034
Matrix:Solid
AnalyzedMDL
Cyanide mg/kg ND 0.25 10/05/18 16:380.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2613742LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide mg/kg 1.21.2 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2613743MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92401224033
2613744
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/kg .787 116 80-120111 4 20.787ND 0.91 0.88
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
433737
EPA 9012B
EPA 9012B
EPA 9012B Cyanide
Associated Lab Samples:92401224035
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2389445
Associated Lab Samples:92401224035
Matrix:Water
AnalyzedMDL
Cyanide mg/L ND 0.0080 10/03/18 01:490.0040
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2389446LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide mg/L 0.10.1 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2389447MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92401224035
2389448
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/L .1 94 75-12585 9 20.1ND 0.094 0.085
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
482157
EPA 9056
EPA 9056
9056 IC Anions
Associated Lab Samples:92401224001, 92401224002, 92401224003, 92401224004, 92401224005, 92401224006, 92401224007,
92401224008, 92401224009, 92401224010, 92401224011, 92401224012, 92401224013, 92401224014,
92401224015, 92401224016, 92401224017, 92401224018, 92401224019, 92401224020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2609514
Associated Lab Samples:92401224001, 92401224002, 92401224003, 92401224004, 92401224005, 92401224006, 92401224007,
92401224008, 92401224009, 92401224010, 92401224011, 92401224012, 92401224013, 92401224014,
92401224015, 92401224016, 92401224017, 92401224018, 92401224019, 92401224020
Matrix:Solid
AnalyzedMDL
Fluoride mg/kg ND 5.0 10/03/18 12:572.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2609515LABORATORY CONTROL SAMPLE:
LCSSpike
Fluoride mg/kg 52.349.9 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2609517MATRIX SPIKE SAMPLE:
MSSpike
Result
92401224001
Fluoride mg/kg 221 M659.6 5 80-120218
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2609519MATRIX SPIKE SAMPLE:
MSSpike
Result
92401224011
Fluoride mg/kg 60.6 M158.5 23 80-12047.2
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92401224001
2609516SAMPLE DUPLICATE:
Fluoride mg/kg 223 2 20218
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92401224011
2609518SAMPLE DUPLICATE:
Fluoride mg/kg 59.1 D6222047.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
482158
EPA 9056
EPA 9056
9056 IC Anions
Associated Lab Samples:92401224021, 92401224022, 92401224023, 92401224024, 92401224025, 92401224026, 92401224027,
92401224028, 92401224029, 92401224030, 92401224031, 92401224032, 92401224033, 92401224034
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2609520
Associated Lab Samples:92401224021, 92401224022, 92401224023, 92401224024, 92401224025, 92401224026, 92401224027,
92401224028, 92401224029, 92401224030, 92401224031, 92401224032, 92401224033, 92401224034
Matrix:Solid
AnalyzedMDL
Fluoride mg/kg ND 5.0 10/03/18 23:572.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2609521LABORATORY CONTROL SAMPLE:
LCSSpike
Fluoride mg/kg 52.150 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2609523MATRIX SPIKE SAMPLE:
MSSpike
Result
92401224021
Fluoride mg/kg 103 M160.2 17 80-12092.3
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2609525MATRIX SPIKE SAMPLE:
MSSpike
Result
92401224031
Fluoride mg/kg 81.7 M1587480-12039.0
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92401224021
2609522SAMPLE DUPLICATE:
Fluoride mg/kg 105 13 2092.3
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92401224031
2609524SAMPLE DUPLICATE:
Fluoride mg/kg 40.0 3 2039.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 83
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
433307
EPA 9056A
EPA 9056A
9056 IC anions 28 Days
Associated Lab Samples:92401224035
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2387661
Associated Lab Samples:92401224035
Matrix:Water
AnalyzedMDL
Fluoride mg/L ND 0.10 09/29/18 05:510.050
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2387662LABORATORY CONTROL SAMPLE:
LCSSpike
Fluoride mg/L 2.62.5 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2387663MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92400889001
2387664
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Fluoride mg/L M12.5 82 90-11074 4 102.52.8 4.8 4.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 83
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
ANALYTE QUALIFIERS
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 83
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92401224035 433423 433611ESW-EB001 EPA 3510C EPA 8082A
92401224001 433443 433807PBC-SB001 (0'-1')EPA 3546 EPA 8270D by SIM
92401224002 433443 433807PBC-SB001 (4'-5')EPA 3546 EPA 8270D by SIM
92401224003 433443 433807PBC-SB002 (0'-1')EPA 3546 EPA 8270D by SIM
92401224004 433443 433807PBC-SB002 (4'-5')EPA 3546 EPA 8270D by SIM
92401224005 433443 433807PBC-SB003 (0'-1')EPA 3546 EPA 8270D by SIM
92401224006 433443 433807PBC-SB003 (4'-5')EPA 3546 EPA 8270D by SIM
92401224007 433443 433807PBC-SB004 (0'-1')EPA 3546 EPA 8270D by SIM
92401224008 433443 433807PBC-SB004 (4'-5')EPA 3546 EPA 8270D by SIM
92401224009 433443 433807PBC-SB005 (0'-1')EPA 3546 EPA 8270D by SIM
92401224010 433443 433807PBC-SB005 (4'-5')EPA 3546 EPA 8270D by SIM
92401224011 433443 433807PBC-SB006 (0'-1')EPA 3546 EPA 8270D by SIM
92401224012 433443 433807PBC-SB006 (4'-5')EPA 3546 EPA 8270D by SIM
92401224013 433445 433674PBC-SB007 (0'-1')EPA 3546 EPA 8270D by SIM
92401224014 433445 433674PBC-SB007 (4'-5')EPA 3546 EPA 8270D by SIM
92401224015 433445 433674PBC-SB008 (0'-1')EPA 3546 EPA 8270D by SIM
92401224016 433445 433674PBC-SB008 (4'-5')EPA 3546 EPA 8270D by SIM
92401224017 433445 433674PBC-SB009 (0'-1')EPA 3546 EPA 8270D by SIM
92401224018 433445 433674PBC-SB009 (4'-5')EPA 3546 EPA 8270D by SIM
92401224019 433445 433674PBC-SB010 (0'-1')EPA 3546 EPA 8270D by SIM
92401224020 433445 433674PBC-SB010 (4'-5')EPA 3546 EPA 8270D by SIM
92401224021 433445 433674PBC-SB011 (0'-1')EPA 3546 EPA 8270D by SIM
92401224022 433445 433674PBC-SB011 (2'-3')EPA 3546 EPA 8270D by SIM
92401224023 433445 433674PBC-SB012 (0'-1')EPA 3546 EPA 8270D by SIM
92401224024 433445 433674PBC-SB012 (4'-5')EPA 3546 EPA 8270D by SIM
92401224025 433445 433674PBC-SB013 (0'-1')EPA 3546 EPA 8270D by SIM
92401224026 433445 433674PBC-SB013 (4'-5')EPA 3546 EPA 8270D by SIM
92401224027 433445 433674PBC-SB014 (0'-1')EPA 3546 EPA 8270D by SIM
92401224028 433445 433674PBC-SB014 (4'-5')EPA 3546 EPA 8270D by SIM
92401224029 433445 433674PBC-SB015 (0'-1')EPA 3546 EPA 8270D by SIM
92401224030 433445 433674PBC-SB015 (4'-5')EPA 3546 EPA 8270D by SIM
92401224031 433445 433674PBC-SB016 (0'-1')EPA 3546 EPA 8270D by SIM
92401224032 433445 433674PBC-SB016 (4'-5')EPA 3546 EPA 8270D by SIM
92401224033 433447 433679PBC-SB017 (0'-1')EPA 3546 EPA 8270D by SIM
92401224034 433447 433679PBC-SB017 (4'-5')EPA 3546 EPA 8270D by SIM
92401224035 433661 434049ESW-EB001 EPA 3511 EPA 8270D by SIM
92401224035 433825ESW-EB001 EPA 8260B
92401224001 433178PBC-SB001 (0'-1')ASTM D2974-87
92401224002 433173PBC-SB001 (4'-5')ASTM D2974-87
92401224003 433173PBC-SB002 (0'-1')ASTM D2974-87
92401224004 433173PBC-SB002 (4'-5')ASTM D2974-87
92401224005 433173PBC-SB003 (0'-1')ASTM D2974-87
92401224006 433173PBC-SB003 (4'-5')ASTM D2974-87
92401224007 433173PBC-SB004 (0'-1')ASTM D2974-87
92401224008 433173PBC-SB004 (4'-5')ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 83
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92401224009 433173PBC-SB005 (0'-1')ASTM D2974-87
92401224010 433173PBC-SB005 (4'-5')ASTM D2974-87
92401224011 433173PBC-SB006 (0'-1')ASTM D2974-87
92401224012 433173PBC-SB006 (4'-5')ASTM D2974-87
92401224013 433173PBC-SB007 (0'-1')ASTM D2974-87
92401224014 433173PBC-SB007 (4'-5')ASTM D2974-87
92401224015 433173PBC-SB008 (0'-1')ASTM D2974-87
92401224016 433173PBC-SB008 (4'-5')ASTM D2974-87
92401224017 433173PBC-SB009 (0'-1')ASTM D2974-87
92401224018 433173PBC-SB009 (4'-5')ASTM D2974-87
92401224019 433175PBC-SB010 (0'-1')ASTM D2974-87
92401224020 433175PBC-SB010 (4'-5')ASTM D2974-87
92401224021 433175PBC-SB011 (0'-1')ASTM D2974-87
92401224022 433175PBC-SB011 (2'-3')ASTM D2974-87
92401224023 433175PBC-SB012 (0'-1')ASTM D2974-87
92401224024 433175PBC-SB012 (4'-5')ASTM D2974-87
92401224025 433175PBC-SB013 (0'-1')ASTM D2974-87
92401224026 433175PBC-SB013 (4'-5')ASTM D2974-87
92401224027 433175PBC-SB014 (0'-1')ASTM D2974-87
92401224028 433175PBC-SB014 (4'-5')ASTM D2974-87
92401224029 433175PBC-SB015 (0'-1')ASTM D2974-87
92401224030 433175PBC-SB015 (4'-5')ASTM D2974-87
92401224031 433175PBC-SB016 (0'-1')ASTM D2974-87
92401224032 433175PBC-SB016 (4'-5')ASTM D2974-87
92401224033 433175PBC-SB017 (0'-1')ASTM D2974-87
92401224034 433175PBC-SB017 (4'-5')ASTM D2974-87
92401224001 483046 483132PBC-SB001 (0'-1')EPA 9012 EPA 9012
92401224002 483046 483132PBC-SB001 (4'-5')EPA 9012 EPA 9012
92401224003 483046 483132PBC-SB002 (0'-1')EPA 9012 EPA 9012
92401224004 483046 483132PBC-SB002 (4'-5')EPA 9012 EPA 9012
92401224005 483046 483132PBC-SB003 (0'-1')EPA 9012 EPA 9012
92401224006 483046 483132PBC-SB003 (4'-5')EPA 9012 EPA 9012
92401224007 483046 483132PBC-SB004 (0'-1')EPA 9012 EPA 9012
92401224008 483046 483132PBC-SB004 (4'-5')EPA 9012 EPA 9012
92401224009 483046 483132PBC-SB005 (0'-1')EPA 9012 EPA 9012
92401224010 483046 483132PBC-SB005 (4'-5')EPA 9012 EPA 9012
92401224011 483046 483132PBC-SB006 (0'-1')EPA 9012 EPA 9012
92401224012 483046 483132PBC-SB006 (4'-5')EPA 9012 EPA 9012
92401224013 483046 483132PBC-SB007 (0'-1')EPA 9012 EPA 9012
92401224014 483046 483132PBC-SB007 (4'-5')EPA 9012 EPA 9012
92401224015 483046 483132PBC-SB008 (0'-1')EPA 9012 EPA 9012
92401224016 483046 483132PBC-SB008 (4'-5')EPA 9012 EPA 9012
92401224017 483047 483172PBC-SB009 (0'-1')EPA 9012 EPA 9012
92401224018 483047 483172PBC-SB009 (4'-5')EPA 9012 EPA 9012
92401224019 483047 483172PBC-SB010 (0'-1')EPA 9012 EPA 9012
92401224020 483047 483172PBC-SB010 (4'-5')EPA 9012 EPA 9012
92401224021 483047 483172PBC-SB011 (0'-1')EPA 9012 EPA 9012
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
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Page 74 of 83
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92401224022 483047 483172PBC-SB011 (2'-3')EPA 9012 EPA 9012
92401224023 483047 483172PBC-SB012 (0'-1')EPA 9012 EPA 9012
92401224024 483047 483172PBC-SB012 (4'-5')EPA 9012 EPA 9012
92401224025 483047 483172PBC-SB013 (0'-1')EPA 9012 EPA 9012
92401224026 483047 483172PBC-SB013 (4'-5')EPA 9012 EPA 9012
92401224027 483047 483172PBC-SB014 (0'-1')EPA 9012 EPA 9012
92401224028 483047 483172PBC-SB014 (4'-5')EPA 9012 EPA 9012
92401224029 483047 483172PBC-SB015 (0'-1')EPA 9012 EPA 9012
92401224030 483047 483172PBC-SB015 (4'-5')EPA 9012 EPA 9012
92401224031 483047 483172PBC-SB016 (0'-1')EPA 9012 EPA 9012
92401224032 483047 483172PBC-SB016 (4'-5')EPA 9012 EPA 9012
92401224033 483049 483397PBC-SB017 (0'-1')EPA 9012 EPA 9012
92401224034 483049 483397PBC-SB017 (4'-5')EPA 9012 EPA 9012
92401224035 433737 433778ESW-EB001 EPA 9012B EPA 9012B
92401224001 482157 482751PBC-SB001 (0'-1')EPA 9056 EPA 9056
92401224002 482157 482751PBC-SB001 (4'-5')EPA 9056 EPA 9056
92401224003 482157 482751PBC-SB002 (0'-1')EPA 9056 EPA 9056
92401224004 482157 482751PBC-SB002 (4'-5')EPA 9056 EPA 9056
92401224005 482157 482751PBC-SB003 (0'-1')EPA 9056 EPA 9056
92401224006 482157 482751PBC-SB003 (4'-5')EPA 9056 EPA 9056
92401224007 482157 482751PBC-SB004 (0'-1')EPA 9056 EPA 9056
92401224008 482157 482751PBC-SB004 (4'-5')EPA 9056 EPA 9056
92401224009 482157 482751PBC-SB005 (0'-1')EPA 9056 EPA 9056
92401224010 482157 482751PBC-SB005 (4'-5')EPA 9056 EPA 9056
92401224011 482157 482751PBC-SB006 (0'-1')EPA 9056 EPA 9056
92401224012 482157 482751PBC-SB006 (4'-5')EPA 9056 EPA 9056
92401224013 482157 482751PBC-SB007 (0'-1')EPA 9056 EPA 9056
92401224014 482157 482751PBC-SB007 (4'-5')EPA 9056 EPA 9056
92401224015 482157 482751PBC-SB008 (0'-1')EPA 9056 EPA 9056
92401224016 482157 482751PBC-SB008 (4'-5')EPA 9056 EPA 9056
92401224017 482157 482751PBC-SB009 (0'-1')EPA 9056 EPA 9056
92401224018 482157 482751PBC-SB009 (4'-5')EPA 9056 EPA 9056
92401224019 482157 482751PBC-SB010 (0'-1')EPA 9056 EPA 9056
92401224020 482157 482751PBC-SB010 (4'-5')EPA 9056 EPA 9056
92401224021 482158 482752PBC-SB011 (0'-1')EPA 9056 EPA 9056
92401224022 482158 482752PBC-SB011 (2'-3')EPA 9056 EPA 9056
92401224023 482158 482752PBC-SB012 (0'-1')EPA 9056 EPA 9056
92401224024 482158 482752PBC-SB012 (4'-5')EPA 9056 EPA 9056
92401224025 482158 482752PBC-SB013 (0'-1')EPA 9056 EPA 9056
92401224026 482158 482752PBC-SB013 (4'-5')EPA 9056 EPA 9056
92401224027 482158 482752PBC-SB014 (0'-1')EPA 9056 EPA 9056
92401224028 482158 482752PBC-SB014 (4'-5')EPA 9056 EPA 9056
92401224029 482158 482752PBC-SB015 (0'-1')EPA 9056 EPA 9056
92401224030 482158 482752PBC-SB015 (4'-5')EPA 9056 EPA 9056
92401224031 482158 482752PBC-SB016 (0'-1')EPA 9056 EPA 9056
92401224032 482158 482752PBC-SB016 (4'-5')EPA 9056 EPA 9056
92401224033 482158 482752PBC-SB017 (0'-1')EPA 9056 EPA 9056
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
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9800 Kincey Ave. Suite 100
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[phone]
Page 75 of 83
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92401224
Frmr Potline/Bath Crushing
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92401224034 482158 482752PBC-SB017 (4'-5')EPA 9056 EPA 9056
92401224035 433307ESW-EB001 EPA 9056A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 10:09 AM
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[phone]
Page 76 of 83
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Page 78 of 83
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Page 83 of 83
#=CL#
November 12, 2018
LIMS USE: FR - MICHAEL WORDEN
LIMS OBJECT ID: 92400799
92400799
Project:
Pace Project No.:
RE:
Michael W. Worden
Environeering, Inc.
16100 Cairnway
Suite 320
Houston, TX 77084
Former Rectifier Station
Dear Michael Worden:
Enclosed are the analytical results for sample(s) received by the laboratory on September 25, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
This revision was issued on 11/12/18 to report J-flagged results to the MDL, per client request.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
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[phone]
Page 1 of 20
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92400799
Former Rectifier Station
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 2 of 20
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92400799
Former Rectifier Station
Lab ID Sample ID Matrix Date Collected Date Received
92400799001 REC-SB001 (0'-1')Solid 09/24/18 18:15 09/25/18 07:30
92400799002 REC-SB001 (4'-5')Solid 09/24/18 18:20 09/25/18 07:30
92400799003 REC-SB002 (0'-1')Solid 09/24/18 18:40 09/25/18 07:30
92400799004 REC-SB002 (4'-5')Solid 09/24/18 18:45 09/25/18 07:30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 3 of 20
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92400799
Former Rectifier Station
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92400799001 REC-SB001 (0'-1')EPA 8082A 8 PASI-CSEM
EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92400799002 REC-SB001 (4'-5')EPA 8082A 8 PASI-CSEM
EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92400799003 REC-SB002 (0'-1')EPA 8082A 8 PASI-CSEM
EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
92400799004 REC-SB002 (4'-5')EPA 8082A 8 PASI-CSEM
EPA 8270D by SIM 21 PASI-CPKS
ASTM D2974-87 1 PASI-CKDF
EPA 9012 1 PASI-OJDW
EPA 9056 1 PASI-OSEW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400799
Former Rectifier Station
Sample:REC-SB001 (0'-1')Lab ID:92400799001 Collected:09/24/18 18:15 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8082A Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 09/28/18 15:12 12674-11-209/26/18 15:3837.8 17.2 1
PCB-1221 (Aroclor 1221)ND ug/kg 09/28/18 15:12 11104-28-209/26/18 15:3837.8 17.2 1
PCB-1232 (Aroclor 1232)ND ug/kg 09/28/18 15:12 11141-16-509/26/18 15:3837.8 17.2 1
PCB-1242 (Aroclor 1242)ND ug/kg 09/28/18 15:12 53469-21-909/26/18 15:3837.8 17.2 1
PCB-1248 (Aroclor 1248)ND ug/kg 09/28/18 15:12 12672-29-609/26/18 15:3837.8 17.2 1
PCB-1254 (Aroclor 1254)ND ug/kg 09/28/18 15:12 11097-69-109/26/18 15:3837.8 17.2 1
PCB-1260 (Aroclor 1260)ND ug/kg 09/28/18 15:12 11096-82-509/26/18 15:3837.8 17.2 1
Surrogates
Decachlorobiphenyl (S)134 %09/28/18 15:12 2051-24-3 S3,S509/26/18 15:3821-132 1
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene 310 ug/kg 09/28/18 01:06 83-32-909/26/18 14:1711.3 1.7 1
Acenaphthylene 14.9 ug/kg 09/28/18 01:06 208-96-809/26/18 14:1711.3 1.5 1
Anthracene 605 ug/kg 09/28/18 01:06 120-12-709/26/18 14:1711.3 1.6 1
Benzo(a)anthracene 1140 ug/kg 09/28/18 15:28 56-55-309/26/18 14:1745.4 3.2 4
Benzo(a)pyrene 827 ug/kg 09/28/18 15:28 50-32-809/26/18 14:1745.4 5.0 4
Benzo(b)fluoranthene 1280 ug/kg 09/28/18 15:28 205-99-209/26/18 14:1745.4 3.0 4
Benzo(g,h,i)perylene 383 ug/kg 09/28/18 01:06 191-24-209/26/18 14:1711.3 2.9 1
Benzo(k)fluoranthene 462 ug/kg 09/28/18 01:06 207-08-909/26/18 14:1711.3 1.7 1
Chrysene 1060 ug/kg 09/28/18 15:28 218-01-909/26/18 14:1745.4 8.2 4
Dibenz(a,h)anthracene 177 ug/kg 09/28/18 01:06 53-70-309/26/18 14:1711.3 2.0 1
Fluoranthene 1820 ug/kg 09/28/18 15:28 206-44-009/26/18 14:1745.4 3.8 4
Fluorene 243 ug/kg 09/28/18 01:06 86-73-709/26/18 14:1711.3 1.8 1
Indeno(1,2,3-cd)pyrene 407 ug/kg 09/28/18 01:06 193-39-509/26/18 14:1711.3 3.2 1
1-Methylnaphthalene 57.8 ug/kg 09/28/18 01:06 90-12-009/26/18 14:1711.3 1.4 1
2-Methylnaphthalene 76.2 ug/kg 09/28/18 01:06 91-57-609/26/18 14:1711.3 1.2 1
Naphthalene 37.8 ug/kg 09/28/18 01:06 91-20-309/26/18 14:1711.3 2.6 1
Phenanthrene 1580 ug/kg 09/28/18 15:28 85-01-809/26/18 14:1745.4 6.8 4
Pyrene 1460 ug/kg 09/28/18 15:28 129-00-009/26/18 14:1745.4 8.2 4
Surrogates
Nitrobenzene-d5 (S)49 %09/28/18 01:06 4165-60-009/26/18 14:1710-128 1
2-Fluorobiphenyl (S)52 %09/28/18 01:06 321-60-809/26/18 14:1710-110 1
Terphenyl-d14 (S)81 %09/28/18 01:06 1718-51-009/26/18 14:1739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 12.1 %09/25/18 18:290.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/02/18 16:20 57-12-509/29/18 18:450.30 0.17 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 15.8 mg/kg 10/01/18 13:59 16984-48-8 M110/01/18 09:305.7 2.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 11:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 5 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400799
Former Rectifier Station
Sample:REC-SB001 (4'-5')Lab ID:92400799002 Collected:09/24/18 18:20 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8082A Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 09/28/18 15:32 12674-11-209/26/18 15:3837.8 17.2 1
PCB-1221 (Aroclor 1221)ND ug/kg 09/28/18 15:32 11104-28-209/26/18 15:3837.8 17.2 1
PCB-1232 (Aroclor 1232)ND ug/kg 09/28/18 15:32 11141-16-509/26/18 15:3837.8 17.2 1
PCB-1242 (Aroclor 1242)ND ug/kg 09/28/18 15:32 53469-21-909/26/18 15:3837.8 17.2 1
PCB-1248 (Aroclor 1248)ND ug/kg 09/28/18 15:32 12672-29-609/26/18 15:3837.8 17.2 1
PCB-1254 (Aroclor 1254)ND ug/kg 09/28/18 15:32 11097-69-109/26/18 15:3837.8 17.2 1
PCB-1260 (Aroclor 1260)ND ug/kg 09/28/18 15:32 11096-82-509/26/18 15:3837.8 17.2 1
Surrogates
Decachlorobiphenyl (S)82 %09/28/18 15:32 2051-24-309/26/18 15:3821-132 1
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 09/28/18 12:18 83-32-909/26/18 14:1711.6 1.7 1
Acenaphthylene ND ug/kg 09/28/18 12:18 208-96-809/26/18 14:1711.6 1.5 1
Anthracene ND ug/kg 09/28/18 12:18 120-12-709/26/18 14:1711.6 1.6 1
Benzo(a)anthracene 2.3J ug/kg 09/28/18 12:18 56-55-309/26/18 14:1711.6 0.82 1
Benzo(a)pyrene 2.2J ug/kg 09/28/18 12:18 50-32-809/26/18 14:1711.6 1.3 1
Benzo(b)fluoranthene 3.2J ug/kg 09/28/18 12:18 205-99-209/26/18 14:1711.6 0.78 1
Benzo(g,h,i)perylene ND ug/kg 09/28/18 12:18 191-24-209/26/18 14:1711.6 3.0 1
Benzo(k)fluoranthene ND ug/kg 09/28/18 12:18 207-08-909/26/18 14:1711.6 1.7 1
Chrysene 2.4J ug/kg 09/28/18 12:18 218-01-909/26/18 14:1711.6 2.1 1
Dibenz(a,h)anthracene ND ug/kg 09/28/18 12:18 53-70-309/26/18 14:1711.6 2.1 1
Fluoranthene 3.3J ug/kg 09/28/18 12:18 206-44-009/26/18 14:1711.6 0.96 1
Fluorene ND ug/kg 09/28/18 12:18 86-73-709/26/18 14:1711.6 1.9 1
Indeno(1,2,3-cd)pyrene ND ug/kg 09/28/18 12:18 193-39-509/26/18 14:1711.6 3.2 1
1-Methylnaphthalene ND ug/kg 09/28/18 12:18 90-12-009/26/18 14:1711.6 1.4 1
2-Methylnaphthalene ND ug/kg 09/28/18 12:18 91-57-609/26/18 14:1711.6 1.3 1
Naphthalene ND ug/kg 09/28/18 12:18 91-20-309/26/18 14:1711.6 2.7 1
Phenanthrene 2.3J ug/kg 09/28/18 12:18 85-01-809/26/18 14:1711.6 1.7 1
Pyrene 3.2J ug/kg 09/28/18 12:18 129-00-009/26/18 14:1711.6 2.1 1
Surrogates
Nitrobenzene-d5 (S)57 %09/28/18 12:18 4165-60-009/26/18 14:1710-128 1
2-Fluorobiphenyl (S)55 %09/28/18 12:18 321-60-809/26/18 14:1710-110 1
Terphenyl-d14 (S)66 %09/28/18 12:18 1718-51-009/26/18 14:1739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.1 %09/25/18 18:290.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/02/18 16:21 57-12-509/29/18 18:450.31 0.17 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 3.6J mg/kg 10/01/18 15:10 16984-48-810/01/18 09:305.8 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 11:20 AM
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Page 6 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400799
Former Rectifier Station
Sample:REC-SB002 (0'-1')Lab ID:92400799003 Collected:09/24/18 18:40 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8082A Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 09/28/18 16:12 12674-11-209/26/18 15:3836.7 16.7 1
PCB-1221 (Aroclor 1221)ND ug/kg 09/28/18 16:12 11104-28-209/26/18 15:3836.7 16.7 1
PCB-1232 (Aroclor 1232)ND ug/kg 09/28/18 16:12 11141-16-509/26/18 15:3836.7 16.7 1
PCB-1242 (Aroclor 1242)ND ug/kg 09/28/18 16:12 53469-21-909/26/18 15:3836.7 16.7 1
PCB-1248 (Aroclor 1248)ND ug/kg 09/28/18 16:12 12672-29-609/26/18 15:3836.7 16.7 1
PCB-1254 (Aroclor 1254)ND ug/kg 09/28/18 16:12 11097-69-109/26/18 15:3836.7 16.7 1
PCB-1260 (Aroclor 1260)ND ug/kg 09/28/18 16:12 11096-82-509/26/18 15:3836.7 16.7 1
Surrogates
Decachlorobiphenyl (S)87 %09/28/18 16:12 2051-24-309/26/18 15:3821-132 1
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 09/28/18 12:39 83-32-909/26/18 14:1711.2 1.7 1
Acenaphthylene ND ug/kg 09/28/18 12:39 208-96-809/26/18 14:1711.2 1.5 1
Anthracene 3.2J ug/kg 09/28/18 12:39 120-12-709/26/18 14:1711.2 1.6 1
Benzo(a)anthracene 43.8 ug/kg 09/28/18 12:39 56-55-309/26/18 14:1711.2 0.80 1
Benzo(a)pyrene 51.3 ug/kg 09/28/18 12:39 50-32-809/26/18 14:1711.2 1.2 1
Benzo(b)fluoranthene 82.3 ug/kg 09/28/18 12:39 205-99-209/26/18 14:1711.2 0.75 1
Benzo(g,h,i)perylene 35.6 ug/kg 09/28/18 12:39 191-24-209/26/18 14:1711.2 2.9 1
Benzo(k)fluoranthene 32.5 ug/kg 09/28/18 12:39 207-08-909/26/18 14:1711.2 1.7 1
Chrysene 75.3 ug/kg 09/28/18 12:39 218-01-909/26/18 14:1711.2 2.0 1
Dibenz(a,h)anthracene 12.2 ug/kg 09/28/18 12:39 53-70-309/26/18 14:1711.2 2.0 1
Fluoranthene 34.1 ug/kg 09/28/18 12:39 206-44-009/26/18 14:1711.2 0.93 1
Fluorene ND ug/kg 09/28/18 12:39 86-73-709/26/18 14:1711.2 1.8 1
Indeno(1,2,3-cd)pyrene 30.6 ug/kg 09/28/18 12:39 193-39-509/26/18 14:1711.2 3.1 1
1-Methylnaphthalene ND ug/kg 09/28/18 12:39 90-12-009/26/18 14:1711.2 1.3 1
2-Methylnaphthalene ND ug/kg 09/28/18 12:39 91-57-609/26/18 14:1711.2 1.2 1
Naphthalene ND ug/kg 09/28/18 12:39 91-20-309/26/18 14:1711.2 2.6 1
Phenanthrene 10.3J ug/kg 09/28/18 12:39 85-01-809/26/18 14:1711.2 1.7 1
Pyrene 32.9 ug/kg 09/28/18 12:39 129-00-009/26/18 14:1711.2 2.0 1
Surrogates
Nitrobenzene-d5 (S)70 %09/28/18 12:39 4165-60-009/26/18 14:1710-128 1
2-Fluorobiphenyl (S)64 %09/28/18 12:39 321-60-809/26/18 14:1710-110 1
Terphenyl-d14 (S)73 %09/28/18 12:39 1718-51-009/26/18 14:1739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 11.2 %09/25/18 18:290.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/02/18 16:22 57-12-509/29/18 18:450.27 0.15 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride ND mg/kg 10/01/18 15:33 16984-48-810/01/18 09:305.6 2.8 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 11:20 AM
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92400799
Former Rectifier Station
Sample:REC-SB002 (4'-5')Lab ID:92400799004 Collected:09/24/18 18:45 Received:09/25/18 07:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8082A Preparation Method: EPA 35468082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 09/28/18 16:32 12674-11-209/26/18 15:3838.9 17.7 1
PCB-1221 (Aroclor 1221)ND ug/kg 09/28/18 16:32 11104-28-209/26/18 15:3838.9 17.7 1
PCB-1232 (Aroclor 1232)ND ug/kg 09/28/18 16:32 11141-16-509/26/18 15:3838.9 17.7 1
PCB-1242 (Aroclor 1242)ND ug/kg 09/28/18 16:32 53469-21-909/26/18 15:3838.9 17.7 1
PCB-1248 (Aroclor 1248)ND ug/kg 09/28/18 16:32 12672-29-609/26/18 15:3838.9 17.7 1
PCB-1254 (Aroclor 1254)ND ug/kg 09/28/18 16:32 11097-69-109/26/18 15:3838.9 17.7 1
PCB-1260 (Aroclor 1260)ND ug/kg 09/28/18 16:32 11096-82-509/26/18 15:3838.9 17.7 1
Surrogates
Decachlorobiphenyl (S)86 %09/28/18 16:32 2051-24-309/26/18 15:3821-132 1
Analytical Method: EPA 8270D by SIM Preparation Method: EPA 35468270 MSSV MW PAH by SIM
Acenaphthene ND ug/kg 09/28/18 13:00 83-32-909/26/18 14:1711.7 1.8 1
Acenaphthylene ND ug/kg 09/28/18 13:00 208-96-809/26/18 14:1711.7 1.5 1
Anthracene ND ug/kg 09/28/18 13:00 120-12-709/26/18 14:1711.7 1.6 1
Benzo(a)anthracene ND ug/kg 09/28/18 13:00 56-55-309/26/18 14:1711.7 0.83 1
Benzo(a)pyrene ND ug/kg 09/28/18 13:00 50-32-809/26/18 14:1711.7 1.3 1
Benzo(b)fluoranthene 0.86J ug/kg 09/28/18 13:00 205-99-209/26/18 14:1711.7 0.78 1
Benzo(g,h,i)perylene ND ug/kg 09/28/18 13:00 191-24-209/26/18 14:1711.7 3.0 1
Benzo(k)fluoranthene ND ug/kg 09/28/18 13:00 207-08-909/26/18 14:1711.7 1.8 1
Chrysene ND ug/kg 09/28/18 13:00 218-01-909/26/18 14:1711.7 2.1 1
Dibenz(a,h)anthracene ND ug/kg 09/28/18 13:00 53-70-309/26/18 14:1711.7 2.1 1
Fluoranthene ND ug/kg 09/28/18 13:00 206-44-009/26/18 14:1711.7 0.97 1
Fluorene ND ug/kg 09/28/18 13:00 86-73-709/26/18 14:1711.7 1.9 1
Indeno(1,2,3-cd)pyrene ND ug/kg 09/28/18 13:00 193-39-509/26/18 14:1711.7 3.3 1
1-Methylnaphthalene ND ug/kg 09/28/18 13:00 90-12-009/26/18 14:1711.7 1.4 1
2-Methylnaphthalene 1.4J ug/kg 09/28/18 13:00 91-57-609/26/18 14:1711.7 1.3 1
Naphthalene ND ug/kg 09/28/18 13:00 91-20-309/26/18 14:1711.7 2.7 1
Phenanthrene ND ug/kg 09/28/18 13:00 85-01-809/26/18 14:1711.7 1.8 1
Pyrene ND ug/kg 09/28/18 13:00 129-00-009/26/18 14:1711.7 2.1 1
Surrogates
Nitrobenzene-d5 (S)61 %09/28/18 13:00 4165-60-009/26/18 14:1710-128 1
2-Fluorobiphenyl (S)57 %09/28/18 13:00 321-60-809/26/18 14:1710-110 1
Terphenyl-d14 (S)64 %09/28/18 13:00 1718-51-009/26/18 14:1739-119 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.0 %09/25/18 18:290.10 0.10 1
Analytical Method: EPA 9012 Preparation Method: EPA 90129012 Cyanide, Total
Cyanide ND mg/kg 10/02/18 16:23 57-12-509/29/18 18:450.31 0.17 1
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions
Fluoride 16.4 mg/kg 10/01/18 16:43 16984-48-810/01/18 09:305.8 2.9 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 11:20 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 8 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400799
Former Rectifier Station
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
432840
EPA 3546
EPA 8082A
8082 GCS PCB
Associated Lab Samples:92400799001, 92400799002, 92400799003, 92400799004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2385452
Associated Lab Samples:92400799001, 92400799002, 92400799003, 92400799004
Matrix:Solid
AnalyzedMDL
PCB-1016 (Aroclor 1016)ug/kg ND 33.1 09/28/18 18:1215.1
PCB-1221 (Aroclor 1221)ug/kg ND 33.1 09/28/18 18:1215.1
PCB-1232 (Aroclor 1232)ug/kg ND 33.1 09/28/18 18:1215.1
PCB-1242 (Aroclor 1242)ug/kg ND 33.1 09/28/18 18:1215.1
PCB-1248 (Aroclor 1248)ug/kg ND 33.1 09/28/18 18:1215.1
PCB-1254 (Aroclor 1254)ug/kg ND 33.1 09/28/18 18:1215.1
PCB-1260 (Aroclor 1260)ug/kg ND 33.1 09/28/18 18:1215.1
Decachlorobiphenyl (S)%100 21-132 09/28/18 18:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2385453LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/kg 159164 96 31-120
PCB-1260 (Aroclor 1260)ug/kg 176164 107 32-120
Decachlorobiphenyl (S)%105 21-132
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2385454MATRIX SPIKE SAMPLE:
MSSpike
Result
92398025033
PCB-1016 (Aroclor 1016)ug/kg 64.0 M11643449-150ND
PCB-1260 (Aroclor 1260)ug/kg 154 M11644950-15073.1
Decachlorobiphenyl (S)%52 21-132
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400799002
2385455SAMPLE DUPLICATE:
PCB-1016 (Aroclor 1016)ug/kg ND 30ND
PCB-1221 (Aroclor 1221)ug/kg ND 30ND
PCB-1232 (Aroclor 1232)ug/kg ND 30ND
PCB-1242 (Aroclor 1242)ug/kg ND 30ND
PCB-1248 (Aroclor 1248)ug/kg ND 30ND
PCB-1254 (Aroclor 1254)ug/kg ND 30ND
PCB-1260 (Aroclor 1260)ug/kg ND 30ND
Decachlorobiphenyl (S)%71 1382
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 11:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400799
Former Rectifier Station
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
432770
EPA 3546
EPA 8270D by SIM
8270 MSSV PAH by SIM
Associated Lab Samples:92400799001, 92400799002, 92400799003, 92400799004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2385110
Associated Lab Samples:92400799001, 92400799002, 92400799003, 92400799004
Matrix:Solid
AnalyzedMDL
1-Methylnaphthalene ug/kg ND 10.1 09/27/18 14:111.2
2-Methylnaphthalene ug/kg ND 10.1 09/27/18 14:111.1
Acenaphthene ug/kg ND 10.1 09/27/18 14:111.5
Acenaphthylene ug/kg ND 10.1 09/27/18 14:111.3
Anthracene ug/kg ND 10.1 09/27/18 14:111.4
Benzo(a)anthracene ug/kg ND 10.1 09/27/18 14:110.71
Benzo(a)pyrene ug/kg ND 10.1 09/27/18 14:111.1
Benzo(b)fluoranthene ug/kg 0.96J 10.1 09/27/18 14:110.67
Benzo(g,h,i)perylene ug/kg ND 10.1 09/27/18 14:112.6
Benzo(k)fluoranthene ug/kg ND 10.1 09/27/18 14:111.5
Chrysene ug/kg ND 10.1 09/27/18 14:111.8
Dibenz(a,h)anthracene ug/kg ND 10.1 09/27/18 14:111.8
Fluoranthene ug/kg ND 10.1 09/27/18 14:110.84
Fluorene ug/kg ND 10.1 09/27/18 14:111.6
Indeno(1,2,3-cd)pyrene ug/kg ND 10.1 09/27/18 14:112.8
Naphthalene ug/kg ND 10.1 09/27/18 14:112.3
Phenanthrene ug/kg ND 10.1 09/27/18 14:111.5
Pyrene ug/kg ND 10.1 09/27/18 14:111.8
2-Fluorobiphenyl (S)%51 10-110 09/27/18 14:11
Nitrobenzene-d5 (S)%54 10-128 09/27/18 14:11
Terphenyl-d14 (S)%60 39-119 09/27/18 14:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2385111LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/kg 26.333.3 79 44-130
2-Methylnaphthalene ug/kg 27.833.3 83 41-134
Acenaphthene ug/kg 29.433.3 88 52-123
Acenaphthylene ug/kg 26.533.3 79 49-116
Anthracene ug/kg 29.333.3 88 41-133
Benzo(a)anthracene ug/kg 29.233.3 88 56-130
Benzo(a)pyrene ug/kg 28.233.3 85 51-136
Benzo(b)fluoranthene ug/kg 28.733.3 86 37-149
Benzo(g,h,i)perylene ug/kg 26.333.3 79 39-127
Benzo(k)fluoranthene ug/kg 29.333.3 88 45-139
Chrysene ug/kg 30.133.3 90 59-127
Dibenz(a,h)anthracene ug/kg 28.833.3 86 37-139
Fluoranthene ug/kg 31.033.3 93 53-132
Fluorene ug/kg 26.033.3 78 45-127
Indeno(1,2,3-cd)pyrene ug/kg 29.433.3 88 35-145
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 11:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400799
Former Rectifier Station
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2385111LABORATORY CONTROL SAMPLE:
LCSSpike
Naphthalene ug/kg 27.933.3 84 45-123
Phenanthrene ug/kg 30.433.3 91 50-125
Pyrene ug/kg 31.033.3 93 52-132
2-Fluorobiphenyl (S)%87 10-110
Nitrobenzene-d5 (S)%92 10-128
Terphenyl-d14 (S)%81 39-119
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2385112MATRIX SPIKE SAMPLE:
MSSpike
Result
92400789001
1-Methylnaphthalene ug/kg 25.240.4 55 50-1503.0J
2-Methylnaphthalene ug/kg 26.140.4 59 50-1502.2J
Acenaphthene ug/kg 31.140.4 65 50-1504.6J
Acenaphthylene ug/kg 24.840.4 56 50-1502.1J
Anthracene ug/kg 45.840.4 75 50-15015.6
Benzo(a)anthracene ug/kg 192 M140.4 156 50-150129
Benzo(a)pyrene ug/kg 206 M140.4 194 50-150128
Benzo(b)fluoranthene ug/kg 324 M140.4 280 50-150211
Benzo(g,h,i)perylene ug/kg 10640.4 67 50-15079.1
Benzo(k)fluoranthene ug/kg 102 M140.4 28 50-15090.3
Chrysene ug/kg 220 M140.4 173 50-150150
Dibenz(a,h)anthracene ug/kg 47.240.4 55 50-15025.1
Fluoranthene ug/kg 25040.4 88 50-150214
Fluorene ug/kg 26.040.4 57 50-1502.9J
Indeno(1,2,3-cd)pyrene ug/kg 11040.4 81 50-15077.6
Naphthalene ug/kg 25.340.4 56 50-1502.8J
Phenanthrene ug/kg 92.240.4 69 50-15064.2
Pyrene ug/kg 24840.4 144 50-150190
2-Fluorobiphenyl (S)%62 10-110
Nitrobenzene-d5 (S)%62 10-128
Terphenyl-d14 (S)%61 39-119
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400789002
2385113SAMPLE DUPLICATE:
1-Methylnaphthalene ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg 1.3J 301.5J
Benzo(a)pyrene ug/kg ND 301.5J
Benzo(b)fluoranthene ug/kg 1.9J 302.1J
Benzo(g,h,i)perylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 11:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400799
Former Rectifier Station
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400789002
2385113SAMPLE DUPLICATE:
Benzo(k)fluoranthene ug/kg ND 30ND
Chrysene ug/kg 2.2J 302.6J
Dibenz(a,h)anthracene ug/kg ND 30ND
Fluoranthene ug/kg 1.2J 301.4J
Fluorene ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2-Fluorobiphenyl (S)%69 370
Nitrobenzene-d5 (S)%70 069
Terphenyl-d14 (S)%70 372
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 11:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400799
Former Rectifier Station
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
432650
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92400799001, 92400799002, 92400799003, 92400799004
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400787001
2384692SAMPLE DUPLICATE:
Percent Moisture %28.3 0 2528.2
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400799004
2384693SAMPLE DUPLICATE:
Percent Moisture %13.8 1 2514.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 11:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400799
Former Rectifier Station
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
481710
EPA 9012
EPA 9012
9012 Cyanide
Associated Lab Samples:92400799001, 92400799002, 92400799003, 92400799004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2607788
Associated Lab Samples:92400799001, 92400799002, 92400799003, 92400799004
Matrix:Solid
AnalyzedMDL
Cyanide mg/kg ND 0.24 10/02/18 16:100.14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2607789LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide mg/kg 1.31.2 106 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2607790MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92400643001
2607791
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/kg M1.764 136 80-120122 8 20.776ND 1.2 1.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 11:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92400799
Former Rectifier Station
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
481867
EPA 9056
EPA 9056
9056 IC Anions
Associated Lab Samples:92400799001, 92400799002, 92400799003, 92400799004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2608290
Associated Lab Samples:92400799001, 92400799002, 92400799003, 92400799004
Matrix:Solid
AnalyzedMDL
Fluoride mg/kg ND 5.0 10/01/18 10:292.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2608291LABORATORY CONTROL SAMPLE:
LCSSpike
Fluoride mg/kg 49.249.6 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2608293MATRIX SPIKE SAMPLE:
MSSpike
Result
92400799001
Fluoride mg/kg 54.3 M156.3 68 80-12015.8
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92400799001
2608292SAMPLE DUPLICATE:
Fluoride mg/kg 16.0 2 2015.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 11:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 15 of 20
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92400799
Former Rectifier Station
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 11:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 20
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92400799
Former Rectifier Station
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92400799001 432840 433354REC-SB001 (0'-1')EPA 3546 EPA 8082A
92400799002 432840 433354REC-SB001 (4'-5')EPA 3546 EPA 8082A
92400799003 432840 433354REC-SB002 (0'-1')EPA 3546 EPA 8082A
92400799004 432840 433354REC-SB002 (4'-5')EPA 3546 EPA 8082A
92400799001 432770 432998REC-SB001 (0'-1')EPA 3546 EPA 8270D by SIM
92400799002 432770 432998REC-SB001 (4'-5')EPA 3546 EPA 8270D by SIM
92400799003 432770 432998REC-SB002 (0'-1')EPA 3546 EPA 8270D by SIM
92400799004 432770 432998REC-SB002 (4'-5')EPA 3546 EPA 8270D by SIM
92400799001 432650REC-SB001 (0'-1')ASTM D2974-87
92400799002 432650REC-SB001 (4'-5')ASTM D2974-87
92400799003 432650REC-SB002 (0'-1')ASTM D2974-87
92400799004 432650REC-SB002 (4'-5')ASTM D2974-87
92400799001 481710 482312REC-SB001 (0'-1')EPA 9012 EPA 9012
92400799002 481710 482312REC-SB001 (4'-5')EPA 9012 EPA 9012
92400799003 481710 482312REC-SB002 (0'-1')EPA 9012 EPA 9012
92400799004 481710 482312REC-SB002 (4'-5')EPA 9012 EPA 9012
92400799001 481867 481884REC-SB001 (0'-1')EPA 9056 EPA 9056
92400799002 481867 481884REC-SB001 (4'-5')EPA 9056 EPA 9056
92400799003 481867 481884REC-SB002 (0'-1')EPA 9056 EPA 9056
92400799004 481867 481884REC-SB002 (4'-5')EPA 9056 EPA 9056
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/12/2018 11:20 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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