4104_CityHighPointKerseyValleyMSWLF_May2018GWMR_20170601

July 10, 2017

Ms. Jackie Drummond, Hydrogeologist
NC Division of Waste Management
Solid Waste Section
Mail Service Center 1646
Raleigh, NC 27699-1646

Re: 2017 First Semi-Annual Water Quality Monitoring Results
Kersey Valley MSWLF
Permit #41-04
High Point, North Carolina

Dear Jackie:

Babb & Associates, P.A. has completed the 2017 first semi-annual sampling event at the Kersey Valley
MSWLF. On May 2-3, 2017, fourteen groundwater monitoring wells, eight surface water monitoring
stations, and two landfill leachate collection points were sampled and analyzed for volatile organic
compounds (VOCs) by EPA Method 8260 and Appendix I inorganic compounds. In addition, the two
leachate samples were analyzed for BOD, COD, nitrate, phosphate, and sulfate.

A site map is provided with this report which shows the groundwater and surface water sample locations
and shallow potentiometric surface (Figure 1). Additional attachments to this report include tables
summarizing the groundwater and surface water analytical results (Tables 1 & 2), field parameters
collected during the monitoring event (Table 3), landfill leachate analytical results (Table 4), well
construction information (Table 5), and groundwater flow rates (Table 6). The laboratory analytical report
is included as Appendix A and attached as an Excel EDD file.

If there are any questions regarding the attached information, please contact me at [phone].

Respectfully,
Babb & Associates, P.A.

Gary D. Babb, P.G.
President

Enclosures

cc: Mr. Robby Stone (pdf copy)
Mr. Mike Spencer (paper copy)

Water Quality Monitoring Report

Kersey Valley Municipal Solid Waste Landfill
3940 East Kivett Drive
High Point, North Carolina
Permit No. 41-04

Prepared for:

City of High Point
Department of Public Services
High Point, NC

Prepared by:

Babb & Associates, P.A.
P.O. Box 37697
Raleigh, North Carolina 27627

May 2017

__________________________________
Gary D. Babb, Licensed Geologist

Table of Contents

1.0 Introduction 1
1.1 Site Information
1.2 Site Geology
1.3 Site Hydrogeology

2.0 Water Quality Monitoring Program 3
2.1 Groundwater Monitoring Network
2.2 Surface Water Monitoring Network
2.3 Landfill Leachate Monitoring

3.0 Water Quality Sample Collection 5
3.1 Field Sample Procedures
3.2 Field Quality Assurance
3.3 Sample Delivery/Chain-of-Custody

4.0 Laboratory Analysis 7

5.0 Hydrogeological Conditions 8

6.0 Laboratory Analytical Results 9
6.1 Groundwater Analytical Results
6.2 Surface Water Analytical Results
6.3 Landfill Leachate Analytical Results
6.4 Quality Control Sample

7.0 Historical Data Comparison 11

8.0 Conclusions 12

Figure 1 Water Quality Monitoring Sample Locations/Potentiometric Map

Table 1 Groundwater Analytical Results
Table 2 Surface Water Analytical Results
Table 3 Field Parameter Measurements
Table 4 Landfill Leachate Analytical Results
Table 5 Well Construction Information/Elevations
Table 6 Hydrologic Test Results

Appendix A ENCO Laboratory Analytical Report

Kersey Valley MSWLF Water Quality Monitoring Report
May 2017 Page 1

1.0 Introduction

1.1 Site Information

The Kersey Valley Municipal Solid Waste Landfill (MSWLF) is located approximately
five miles east of downtown High Point and one-half mile east of the intersection of US
70/US 29/I-85 Business on Kivett Drive. The surrounding area is mixed residential,
commercial, and industrial land uses.

The MSWLF facility is located on approximately 164 acres owned by the City of High
Point. The permitted facility is bounded on the north by Kivett Drive, on the west by
Jackson Lake Road, and to the south by private property. Kersey Valley Road runs
through the center of the site and separates the Area 1 and Area 2 landfill units. Two
unnamed tributaries of Richland Creek (“South” and “East” tributaries) run along much
of the southern portion of the site between the landfill units and neighboring properties.
Also, a pond exists on the site just to the west of the Area 1 landfill unit.

Ground surface elevations range from approximately El. 740 msl along the unnamed
tributary on the south end of the site to El. 900 msl at the top of the Area 1 landfill unit.
The facility location and existing site conditions are shown on Figure 1.

1.2 Site Geology1

The Kersey Valley MSWLF is located in the central Piedmont Physiographic Province,
in the northern portion of the Carolina Slate Belt. Granite is the predominant rock type in
the area and outcrops are observed along the creeks and within the site. Rock core

____________________
1 Water Quality Monitoring Plan – Kersey Valley Landfill Facility, Smith Gardner, Inc., November 2014
Kersey Valley MSWLF Water Quality Monitoring Report
May 2017 Page 2

borings indicated a light tan to pinkish white, medium to coarse grained porphyritic
granite with abundant quartz, potassium feldspar and mica. Granite exposures at the
surface are generally highly weathered but become less weathered with depth.

Site stratigraphy includes three main layers: 1) near surface soils which include moderate
to high plasticity silt and clay, low plasticity sandy silt and clayey silt; 2) weathered rock
(saprolite); and 3) bedrock. Near surface soils generally have standard Penetration Test
(SPT) values ranging from 20-50 blows per foot (bpf). The saprolite generally has SPT
values of >50 bpf. No unusual geologic features or conditions were identified during
prior site studies.

1.3 Site Hydrogeology1

Groundwater in the upper-most aquifer generally flows through unconsolidated
sediments and secondary fractures in the underlying bedrock. Recharge occurs primarily
in the northern portion of the site and is limited on slopes. Groundwater flows generally
south where it discharges into two unnamed tributaries of Richland Creek. The
groundwater potentiometric surface generally reflects a subdued expression of the surface
topography. Local conditions are considered typical for the central Piedmont Region. A
composite potentiometric surface map for the site is provided as Figure 1.

____________________
1 Water Quality Monitoring Plan – Kersey Valley Landfill Facility, Smith Gardner, Inc., November 2014

Kersey Valley MSWLF Water Quality Monitoring Report
May 2017 Page 3

2.0 Water Quality Monitoring Program

The water quality monitoring network at the Kersey Valley MSWLF is evaluated on a semi-
annual basis. The location of the groundwater, surface water, and landfill leachate samples
collected during the semi-annual monitoring events is shown on the attached Figure 1.

2.1 Groundwater Monitoring Network

The existing groundwater monitoring network consists of fourteen shallow aquifer wells
which are screened across the water table in the partially weathered rock, just above the
depths of auger refusal. The fourteen monitoring wells sampled for subsequent
laboratory analysis include:

MW-1 (background) MW-3A
MW-4 MW-6A
MW-8A MW-9
MW-10 MW-11
MW-12 MW-13S
MW-14 MW-15
MW-16 MW-17

In addition to the fourteen monitoring wells sampled for laboratory analysis, four deeper
aquifer monitoring wells are gauged for water levels. This provides information on the
vertical component of groundwater flow at the site. The four deeper aquifer monitoring
wells include:

MW-7D MW-8B
MW-9D MW-13D

Kersey Valley MSWLF Water Quality Monitoring Report
May 2017 Page 4

The shallow wells have been constructed in boreholes advanced to the top of rock
(defined by refusal) using 6-inch diameter hollow stem augers. The deeper aquifer
monitoring wells are screened within the bedrock having been advanced below auger
refusal depths using air-rotary or rock coring techniques. All monitoring wells are
constructed of 2-inch diameter Schedule 40 PVC, with an isolated well screen interval, in
accordance with applicable NC Well Construction Standards. Monitoring well
construction information is provided on Table 5.

2.2 Surface Water Monitoring Network

The current surface water monitoring network consists of eight monitoring stations as
shown on Figure 1. The surface water monitoring stations are located along the south
side of Area 1 and the south/southeast side of Area 2 of the landfill. The eight surface
water stations sampled for the water quality monitoring program include:

SW-1 (background) SW-3
SW-5 SW-6
SW-7 SW-8
SW-9 SW-10

2.3 Landfill Leachate Monitoring

Landfill leachate samples are collected from Area 1 (Leachate Phase 1-3) and Area 2
(Leachate Phase 4-5). The leachate sample collected from the leachate storage lagoon in
the south central portion of the site represents Area 1. The leachate sample collected
from the leachate storage tank facility in the northeast corner of the site represents Area
2. The location of these two leachate collection points is shown on the attached Figure 1.

Kersey Valley MSWLF Water Quality Monitoring Report
May 2017 Page 5

3.0 Water Quality Sample Collection

Samples of groundwater, surface water, and leachate were collected in accordance with the
approved Water Quality Monitoring Plan, November 2014 and the NC Solid Waste Section
Guidelines for Groundwater, Soil, and Surface Water Sampling Guidance Document, 2008. A
description of the sample collection procedure is provided below.

3.1 Field Sample Procedures

Prior to groundwater sampling, water levels were obtained from each well using an
electric water level meter capable of measuring the depth to water to the nearest 0.01 feet.
This information was later used to determine the elevation of the water table in each
monitoring well relative to surveyed datum (Table 5). The depth to water in each well
was also used to determine the volume of standing water in the well casing. This
information allowed for the purging of a minimum of three casing volumes from each
well prior to sample collection to assure a fresh groundwater sample was collected. New
nitrile gloves were worn by sampling personnel and each well was purged and sampled
with a new disposable bailer which was discarded after use.

After the monitoring wells had been allowed to recover from purging, normally 12-14
hours, samples are collected in the following order:

 Volatile organics
 Total metals
 Inorganics (nitrate, phosphorus, sulfate)
 Biological (BOD, COD)
 Field Parameters (pH, Conductivity, Temperature)

Kersey Valley MSWLF Water Quality Monitoring Report
May 2017 Page 6

The groundwater samples are collected directly in the laboratory-supplied containers
which are pre-filled with the appropriate preservative. The samples are not filtered in the
field or the laboratory. After collection, the samples are placed in a cooler on ice for
shipment to the analytical laboratory.

Surface water and landfill leachate samples are collected directly into the laboratory-
supplied containers as grab samples. Sampling personnel wear new disposable nitrile
gloves for each surface water and leachate sample collected. As with the groundwater
samples, these samples are stored in a cooler on ice prior to delivery to the analytical
laboratory.

3.2 Field Quality Assurance

One trip blank sample was prepared by the analytical laboratory and accompanied the
sample shipment until receipt back at the laboratory. The trip blank sample was analyzed
for volatile organic compounds. Temperature blanks are also provided with the sample
shipments to assure the proper temperature is maintained until delivery to the analytical
laboratory.

3.3 Sample Delivery/Chain of Custody

All groundwater, surface water, and landfill leachate samples are stored in coolers on ice
immediately after collection. Individual sample containers for each monitoring well or
surface water sample are placed in zip lock plastic bags to reduce the potential for cross
contamination between sample locations. Chain-of-Custody control documents are
prepared and shipped with each cooler. Custody seals are also used for each cooler to
maintain sample integrity until delivery to the analytical laboratory. The sample coolers
are shipped via Federal Express for next morning delivery to the analytical laboratory.

Kersey Valley MSWLF Water Quality Monitoring Report
May 2017 Page 7

4.0 Laboratory Analysis

The samples were analyzed for parameters specified by the NC Solid Waste Section for detection
monitoring at permitted solid waste facilities. The standard detection monitoring program for
groundwater and surface water samples consists of the Appendix I parameters. The Appendix I
analysis consists of volatile organic compounds (VOCs) by EPA Method 8260B and inorganic
compounds by EPA Methods 6010C/6020A.

In addition to the Appendix I parameters, the two leachate samples are analyzed for biological
oxygen demand (SM 5210B-2001), chemical oxygen demand (SM5220D-1997), phosphorus
(EPA Method 365.4), sulfate (EPA Method 300.0), and nitrate/nitrite (EPA Method 353.2).

The laboratory performing the water quality analysis is Environmental Conservation
Laboratories, Inc. (ENCO) of Cary, North Carolina, which is a NC Certified Laboratory.
Internal quality control samples, including matrix spikes/matrix spike duplicates, are performed
by ENCO for each set of samples. The ENCO laboratory report, including internal quality
control samples, is provided with this report in Appendix A.

Kersey Valley MSWLF Water Quality Monitoring Report
May 2017 Page 8

5.0 Hydrogeological Conditions

The depth to groundwater was measured in the fourteen compliance monitoring wells and the
four deeper aquifer monitoring wells during the May 2-3, 2017 monitoring event. The
groundwater elevations were calculated relative to the surveyed measuring point (top of casing)
for each monitoring well. The groundwater elevations are summarized on Table 5 and the
potentiometric surface of the shallow water table is shown on Figure 1.

The general direction of groundwater flow, based on the water level information collected during
this monitoring event, is also shown on Figure 1. Groundwater flow direction is generally to the
south, toward an unnamed tributary of Richland Creek.

Based on the results of prior hydrological tests conducted in Area 1 of the site, groundwater flow
rates in the shallow saprolite range from 1.24 ft/day to 2.38 ft/day. The hydrologic tests
conducted in Area 2 in the fractured bedrock indicated groundwater flow rates in the range of
0.124 ft/day to 0.690 ft/day. The average hydraulic conductivity and transmissivity values for
Areas 1 and 2 of the MSWLF are provided on Table 6.

The vertical component of groundwater flow is determined from an evaluation of groundwater
elevations observed in nested well pairs. Three nested pairs of monitoring wells were evaluated
for vertical groundwater flow at the site. The following vertical groundwater gradients were
determined from the elevations determined during the May 2017 monitoring event:

Monitoring Wells MW-8A/8B 0.092 ft/ft downward
Monitoring Wells MW-9/9D 0.078 ft/ft downward
Monitoring Wells MW-13S/13D 0.004 ft/ft downward

Kersey Valley MSWLF Water Quality Monitoring Report
May 2017 Page 9

6.0 Laboratory Analytical Results

Final laboratory analytical results for the samples collected on May 3, 2017 were received from
the analytical laboratory on May 23, 2017. A summary of the analytical results are provided on
Table 1 (groundwater), Table 2 (surface water), Table 3 (field parameters), and Table 4 (landfill
leachate).

6.1 Groundwater Analytical Results

One volatile organic compound (VOCs) was detected at a concentration equaling or
exceeding the laboratory method reporting limit at the site. The compound toluene was
reported at a concentration of 1.1 ug/l in monitoring well MW-1 and MW-12. Note that
monitoring well MW-1 is the upgradient background monitoring location for the site.
The reported toluene concentration in the two monitoring wells is below the established
NC 2L Groundwater Standard of 600 ug/l. No other VOCs were reported above the
laboratory reporting limits or Solid Waste Section Limits (SWSL) in any of the
remaining twelve monitoring wells.

Four inorganic compounds were detected above the laboratory reporting limits and
SWSLs, including barium, chromium, cobalt, and zinc. The reported concentration of
barium in monitoring wells MW-6A, MW-9, MW-11, MW-12, MW-13S, MW-14, MW-
15, and MW-17 were all above the SWSL but well below the established NC 2L
Groundwater Standard of 600 ug/l. The compound cobalt was reported above the SWSL
in monitoring wells MW-6A, MW-9, and MW-13S. The compound cobalt does not have
an established NC 2L Groundwater Standard. The compound zinc was reported above
the SWSL in MW-1, MW-4, MW-6A, MW-9, MW-10, MW-11 MW-12, and MW-13S,
however, the reported concentrations of zinc in these monitoring wells were all well
below the established NC 2L Groundwater Standard of 1,000 ug/l. The inorganic
compound chromium was reported above the SWSL and NC 2L Groundwater Standard

Kersey Valley MSWLF Water Quality Monitoring Report
May 2017 Page 10

in monitoring well MW-9. The reported concentration of chromium in monitoring well
MW-9 (16.8 ug/l) slightly exceeded the established NC 2L Groundwater Standard of 10
ug/l. No other inorganic compounds were reported at a concentration which exceeded the
laboratory reporting limits, SWSLs, or NC 2L Groundwater Standards.

6.2 Surface Water Analytical Results

No VOCs were detected at a concentration equaling or exceeding the laboratory method
reporting limit in any of the eight surface water samples. Only one inorganic compound
was detected at concentrations that exceeded the laboratory method reporting limit. The
reported concentration of zinc (12.4 ug/l) in SW-6 was reported above the laboratory
reporting limit and SWSL but well below the established 2B Surface Water Standard of
50 ug/l. No other inorganic compounds were detected in the eight surface water samples
above the laboratory reporting limits, SWSLs, or NC 2B Surface Water Standards.
Please note that surface water monitoring station SW-9 was dry at the time of this water
quality monitoring event.

Kersey Valley MSWLF Water Quality Monitoring Report
May 2017 Page 11

6.3 Landfill Leachate Analytical Results

No volatile organic compounds were identified above the laboratory limits or SWSLs in
either of the two landfill leachate samples. Several inorganic compounds were detected
at a concentration equaling or exceeding the laboratory method reporting limits in the two
leachate samples, including: barium, chromium, cobalt, and zinc. Additional parameters
evaluated in the two leachate samples include: BOD (42,000 ug/l), COD (270,000 ug/l),
phosphorus (790 ug/l), nitrite/nitrate (2,800 ug/l), and sulfate (14,000 ug/l-estimated).
Please refer to Table 4 for a full summary of the reported VOCs, inorganics, and other
indicator compounds in the two leachate samples.

6.4 Quality Control Sample

One trip blank was submitted and analyzed for quality assurance purposes. No VOCs
were detected at a concentration equaling or exceeding laboratory quantitation limits in
the trip blank.

Kersey Valley MSWLF Water Quality Monitoring Report
May 2017 Page 12

7.0 Historical Data Comparison

A review of the laboratory analytical data for the groundwater samples collected over past
monitoring events indicate the presence of low concentrations of naturally occurring inorganic
compounds (i.e. barium, zinc). No volatile organic compounds have been reported in any of the
groundwater monitoring wells above the NC 2L Groundwater Standards. The reported
concentration of naturally occurring inorganic compounds vary slightly between monitoring
events, likely due to fluctuating amounts of silt/sediment in the samples. Filtering of the
groundwater samples prior to laboratory analysis is not allowed.

Kersey Valley MSWLF Water Quality Monitoring Report
May 2017 Page 13

8.0 Conclusions

Based on the results of this water quality monitoring event, the Kersey Valley MSWLF will
remain in Detection Monitoring in accordance with Title 15A NACA 13B .1633. The 2017 fall
semi-annual water quality monitoring event is tentatively scheduled for October 2017.

Attachments to this report include tables summarizing the groundwater and surface water
analytical results (Tables 1 & 2), field parameters collected during the monitoring event (Table
3), landfill leachate analytical results (Table 4), well construction information (Table 5), and
hydrologic test results (Table 6). A copy of the laboratory analytical report in pdf and EDD
formats is also included with this report in Appendix A.

FIGURES
MW-3A**TOC=749.50DTW=17.01GWE=732.49TOC=784.62DTW=13.58GWE=771.04MW-7DTOC=783.97DTW=22.78GWE=761.19MW-8ATOC=760.69DTW=5.91GWE=754.78MW-8BTOC=760.91DTW=7.47GWE=753.44MW-15TOC=775.93DTW=15.03GWE=760.90MW-9TOC=786.48DTW=21.73GWE=764.75MW-9DTOC=785.91DTW=23.16GWE=762.75MW-10TOC=814.84DTW=22.19GWE=792.65MW-1TOC=833.37DTW=30.50GWE=802.87MW-4TOC=830.32DTW=19.71GWE=810.61MW-6ATOC=784.62MW-11TOC=813.06DTW=10.26GWE=802.80MW-12TOC=782.18DTW=9.19GWE=772.99MW-13STOC=819.19DTW=25.74GWE=793.45MW-13DTOC=818.78DTW=25.44GWE=793.34MW-14TOC=805.21DTW=16.41GWE=788.80MW-9TOC=786.48DTW=21.73GWE=764.75MW-9DTOC=785.91DTW=23.16GWE=762.75MW-10TOC=814.84DTW=22.19GWE=792.65MW-1TOC=833.37DTW=30.50GWE=802.87MW-4TOC=830.32DTW=19.71GWE=810.61MW-6ATOC=784.62MW-11TOC=813.06DTW=10.26GWE=802.80MW-12TOC=782.18DTW=9.19GWE=772.99MW-13STOC=819.19DTW=25.74GWE=793.45MW-13DTOC=818.78DTW=25.44GWE=793.34MW-14TOC=805.21DTW=16.41GWE=788.80PROJECT TITLE:DRAWING TITLE:REV.DATEDESCRIPTIONDESIGNED:DRAWN:APPROVED:PROJECT NO:SCALE:FILENAME:PREPARED BY:PREPARED FOR:SHEET NUMBER:DRAWING NUMBER:DATE:G:\CAD\High Point\Hpoint 16-2\sheets\HP-D0529.dwg - 6/6/2017 11:51 AM
SEALSEALSMITHGARDNERENGINEERS+14 N. Boylan Avenue, Raleigh NC 27603NC LIC. NO. F-1370 (ENGINEERING)919.828.0577Electronic files are instruments of service provided by SmithGardner, Inc. for the convenience of the intended recipient(s), andno warranty is either expressed or implied.  Any reuse orredistribution of this document in whole or part without thewritten authorization of Smith Gardner, Inc., will be at the solerisk of the recipient.  If there is a discrepancy between theelectronic files and the signed and sealed hard copies, the hardcopies shall govern.  Use of  any electronic files generated orprovided by Smith Gardner, Inc., constitutes an acceptance ofthese terms and conditions.© 2017 Smith Gardner, Inc.CITY OF HIGH POINTDEPARTMENT OFPUBLIC SERVICESHIGH POINT, NCKERSEY VALLEY MSW LANDFILLPHASES 5A & 5BGROUNDWATERPOTENTIOMETRICSURFACE MAPMAY 2017 M.M.G.J.A.L.HPOINT 16-2AS SHOWNJun 17HP-D0529FIG.1MW-1TOC=DTW=GWE=

TABLES
TABLE 12017 First Semi-Annual Groundwater Monitoring Well Laboratory Analytical ResultsKersey Valley MSWLFHigh Point, North CarolinaPermit #41-04Parameter MW-1 MW-3A MW-4 MW-6A MW-8A MW-9 MW-10 2L Std.Inorganics (ug/l) Antimony BQL BQL BQL BQL BQL BQL BQL NEBarium 88.6 J 62.3 J 64.0 J 271 51.5 J 181 99.1 J 700Beryllium 0.561 J BQL 0.316 J BQL BQL BQL BQL NECadmium BQL BQL BQL BQL BQL BQL BQL 2Chromium 2.73 J BQL 3.51 J 1.99 J BQL16.82.34 J 10Cobalt 4.75 J BQL 1.35 J 13.1 1.80 J 15.1 5.36 J NECopper 3.99 J BQL 3.06 J 2.78 J 1.64 J 22.8 3.91 J 1000Lead BQL BQL BQL BQL BQL 3.86 J BQL 15Nickel 10.9 J 3.48 J BQL 2.45 J BQL 11.0 J 5.75 J 100Selenium BQL BQL BQL BQL BQL 0.965 J BQL 20Thallium 0.119 J 0.122 J BQL 0.141 J BQL 0.160 J 0.113 J NEVanadium BQL 5.76 J 2.68 J 5.56 J 2.14 J 43.2 17.8 J NEZinc 44.9 5.33 J 10.3 11.0 5.91 J 52.2 24.4 1000Method 8260B (ug/l)Toluene 1.1 BQL BQL BQL BQL BQL 0.78 J 600Notes:Samples collected on May 3, 2017BQL - Below laboratory quantitation limit.J - Detected below the quantitation limit.Bold concentrations equal or exceed established or interim standards.NE - not established.
TABLE 1 (continued)2017 First Semi-Annual Groundwater Monitoring Well Laboratory Analytical ResultsKersey Valley MSWLFHigh Point, North CarolinaPermit #41-04Parameter MW-11 MW-12 MW-13S MW-14 MW-15 MW-16 MW-17 2L Std.Inorganics (ug/l) Barium 129 189 251 41.2 23.1 79.2 J 87.7 700Beryllium BQL BQL 0.293 J BQL BQL BQL BQL NEChromium 1.54 J 3.72 J 4.86 J BQL BQL BQL BQL 10Cobalt 3.22 J 2.68 J 15.7 BQL BQL BQL BQL NECopper 3.69 J 4.94 J 19.6 BQL BQL 1.89 J 1.86 J 1000Lead BQL BQL BQL BQL BQL BQL BQL 15Nickel 2.82 J 16.7 J 7.96 J BQL BQL BQL 14.8 J 100Selenium BQL BQL BQL BQL 1.20 J BQL BQL 20Thallium BQL BQL 0.136 J BQL BQL BQL BQL NEVanadium 11.0 J 7.70 J 24.9 J 1.67 J BQL 2.21 J 3.51 J NEZinc 36.9 10.3 131.0 8.43 J BQL BQL 5.43 J 1000Method 8260B (ug/l)Toluene BQL 1.1 BQL 0.44 J BQL BQL BQL 600Notes:Samples collected on May 3, 2017BQL - Below laboratory quantitation limit.J - Detected below the quantitation limit.B - Amount in Prep Blank > MDLBold concentrations equal or exceed established or interim standards.NE - not established.
TABLE 22017 First Semi-Annual Surface Water Laboratory Analytical ResultsKersey Valley MSWLFHigh Point, North CarolinaPermit #41-04Parameter SW-1 SW-3 SW-5 SW-6 SW-7 SW-8 SW-9 SW-10 2B Std.App. I Metals (ug/l)DryAntimony BQL 0.443 J BQL BQL BQL 0.370 J BQL 640Barium 68.3 J 88.8 J 66.4 J 55.7 J 53.5 J 83.5 J 219 1000Beryllium BQL BQL BQL BQL BQL BQL BQL 6.5Chromium BQL BQL BQL BQL BQL BQL BQL 50Cobalt BQL BQL BQL 1.29 J 1.63 J 1.26 J 7.31 J 3Copper 3.32 J 2.52 J 3.03 J 2.82 J 1.79 J 3.01 J BQL 7Lead BQL BQL BQL BQL BQL BQL BQL 25Nickel BQL BQL BQL BQL BQL 2.39 J BQL 88Silver BQL BQL BQL BQL BQL BQL BQL 0.06Vanadium 3.39 J 1.62 J 4.21 J 1.49 J BQL 2.56 J 2.63 J NEZinc 7.93 J BQL 6.35 J 12.4 6.65 J BQL BQL 50Method 8260B (ug/l)BQL BQL BQL BQL BQL BQL Dry BQL 140Notes:Samples collected on May 3, 2017BQL - Below laboratory quantitation limit.J - Detected below the quantitation limit.B - Amount in Prep Blank > MDLBold concentrations equal or exceed established or interim standards.NE - Not Established
TABLE 32017 First Semi-Annual Field ParametersKersey Valley MSWLFHigh Point, North CarolinaPermit #41-04Monitoring StationSample Date Sample Time Conductivity Temperature - C pHMW-1 5/3/2017 1015 107 19.5 5.0MW-3A 5/3/2017 800 262 16.6 6.4MW-4 5/3/2017 1005 60 15.0 5.5MW-6A 5/3/2017 840 467 16.4 5.8MW-8A 5/3/2017 815 192 14.8 6.0MW-9 5/3/2017 850 317 19.3 5.7MW-10 5/3/2017 1030 230 20.8 5.5MW-11 5/3/2017 930 137 16 6.5MW-12 5/3/2017 905 275 15.7 6.1MW-13S 5/3/2017 1105 214 17.9 5.7MW-14 5/3/2017 1130 241 16.9 6.3MW-15 5/3/2017 1145 650 13.4 6.3MW-16 5/3/2017 1220 515 15.5 6.9MW-17 5/3/2017 1245 265 19.4 6.0SW-1 5/3/2017 945 163 16.2 6.9SW-3 5/3/2017 830 339 15.8 7.0SW-5 5/3/2017 920 170 15.4 6.8SW-6 5/3/2017 1200 320 11.5 6.9SW-7 5/3/2017 1235 306 19.2 7.3SW-8 5/3/2017 1300 312 20.1 7.5SW-9 Dry Dry Dry Dry DrySW-10 5/3/2017 1315 945 22.2 6.2Leachate Phase 1-3 5/3/2017 1345 1405 26.1 7.9Leachate Phase 4-5 5/3/2017 1325 2084 25.9 7.1
TABLE 42017 First Semi-Annual Landfill Leachate Laboratory Analytical ResultsKersey Valley MSWLFHigh Point, North CarolinaPermit #41-04Parameter Leachate Phase 1-3 (Area 1) Leachate Phase 4-5 (Area 2)Inorganics (ug/l)Antimony BQL BQLArsenic BQL 9.66 JBarium 482 169Beryllium BQL BQLChromium 7.74 J 11.7Cobalt 9.56 J 11.4Copper 9.10 J 3.60 JLead BQL BQLNickel 30.6 J 30.8 JThallium BQL BQLVanadium 12.9 J 16.8 JZinc 41.3 9.55 JBiochemical Oxygen Demand 42000 20000Chemical Oxygen Demand 270000 190000Nitrate/Nitrite 2800 120Phosphorus 790 680Sulfate 7200 J 14000 JMethod 8260B (ug/l)Acetone BQL 140 J2-Butanone BQL 98 JNotes:Samples collected on May 3, 2017BQL - Below laboratory quantitation limit.J - Detected below the quantitation limit.B - Amount in Prep Blank > MDL
Table 5Groundwater Monitoring Well ConstructionKersey Valley MSWLFHigh Point, North CaroliinaPermit #41-04Well IDDate DrilledWell DiameterTotal DepthTOS DepthScreened IntervalGround ElevationTOC ElevationGroundwater DepthGroundwater ElevationLat/Long GeologyMW-1 NA 2" 44.5' NA NA 831.87 833.37 30.50 802.87804526.7486N 1724007.1470EGranitic GneissMW-3A 3/25/97 2" 32.2' 20' 20'-35' 748.23 749.50 17.01 732.49802574.4351N 1724329.0288EGranitic GneissMW-4 8/10/93 2" 20.5' 15' 15'-25' 827.82 830.32 19.71 810.61804359.1321N 1723459.1855ESandy SiltMW-6A 3/25/97 2" 23.5' 6' 6'-21' NA 784.62 13.58 771.04802708.7456N 1723640.4105EGranitic GneissMW-7D 3/25/97 2" 56.6' 49' 49'-54' NA 783.97 22.78 761.19802574.5846N 1723984.6854EGranitic GneissMW-8A 8/11/93 2" 18.0' 10' 10'-15' 758.19 760.69 5.91 754.78802446.5231N 1723791.7164EGranitic GneissMW-8B 8/12/93 2" 32.5' 20' 20'-30' 758.41 760.91 7.47 753.44802458.1560N 1723806.1747EDioriteMW-9 8/11/93 2" 25.3' 10' 10'-25' 782.64 786.48 21.73 764.75802980.7000N 1723357.8400EDioriteMW-9D 3/25/97 2" 51.0' 46' 46'-51' 783.75 785.91 23.16 762.75802988.9400N 1723359.4500EGranitic GneissMW-10 NA 2" 36.6' 18' 18'-33' 812.60 814.84 22.19 792.65803471.2000N 1724362.3600ESilty Sand PWRMW-11 NA 2" 25.5' 13.5' 13.5'-23.5' 808.99 813.06 10.26 802.80903926.9554N 1722574.9937EGranitic GneissMW-12 NA 2" 31.3' 15' 15'-30' 779.61 782.18 9.19 772.99803352.1500N 1722735.7100EGranitic GneissMW-13S NA 2" 30.0' 15' 15'-30' 816.36 819.19 25.74 793.45803950.7711N 1725197.5538ESilty Sand MW-13D NA 2" 59.4' 44' 44'-54' 816.45 818.78 25.44 793.34803954.1375N 1725200.9852ESilty Sand PWRMW-14 9/3/10 2" 47.0' 32' 32'-47' 801.79 805.21 16.41 788.80803278.6700N 1726081.5500EGraniteMW-15 9/2/10 2" 40.0' 30' 30'-40' 772.57 775.93 15.03 760.90802675.4000N 1725908.0900EGraniteMW-16 4/7/15 2" 47.0' 37' 37'-47' TBD TBD 20.68 TBD802262.729N 1725515.373EDioriteMW-17 4/7/15 2" 41.0' 31' 31'-41' TBD TBD 17.76 TBD802370.766N 1724784.691EDioriteTOS - Top of Screen TBD - To Be DeterminedTOC - Top of Casing NA - Not AvailableGroundwater depths collected on May 3, 2017
Table 6Groundwater Flow RatesKersey Valley MSWLFHigh Point, North CarolinaPermit #41-04Area A Shallow Saprolite Average Hydraulic Conductivity = 2.38 ft/dayAverage Transmissivity ‐ 107.4 ft2/dayArea B Shallow Saprolite Average Hydraulic Conductivity = 1.24 ft/dayAverage Transmissivity = 55.9 ft2/dayArea C Fractured Bedrock Average Hydraulic Conductivity = 0.690 ft/dayAverage Transmissivity = 51.75 ft2/dayArea D Fractured Bedrock Average Hydraulic Conductivity = 0.124 ft/dayAverage Transmissivity = 9.29 ft2/dayArea AArea BArea CArea D

APPENDIX A
102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:www.encolabs.com
Environmental Conservation Laboratories, Inc.
ENCO Workorder(s): CA05956
Raleigh, NC 27606
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: [none], Project Name/Desc: Kersey Valley Landfill
Attn: Gary Babb
Babb & Associates (BA024)
3605 Country Cove Lane
Bill Scott
Project Manager
Tuesday, May 23, 2017
RE: Laboratory Results for
Dear Gary Babb,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, May 4, 2017.
The total number of pages in this report, including this page is 87.
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SAMPLE SUMMARY/LABORATORY CHRONICLE
4104-MW1 CA05956-01 Sampled:05/03/17 10:15 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 10:51
EPA 6020B 10/30/17 05/09/17 13:41 5/22/2017 10:47
EPA 8260B 05/17/17 05/12/17 12:23 5/12/2017 20:09
4104-MW3A CA05956-02 Sampled:05/03/17 08:00 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 11:03
EPA 6020B 10/30/17 05/09/17 13:41 5/22/2017 10:51
EPA 8260B 05/17/17 05/12/17 12:23 5/12/2017 20:40
4104-MW4 CA05956-03 Sampled:05/03/17 10:05 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 11:06
EPA 6020B 10/30/17 05/09/17 13:41 5/22/2017 10:54
EPA 8260B 05/17/17 05/12/17 12:23 5/12/2017 21:10
4104-MW6A CA05956-04 Sampled:05/03/17 08:40 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 11:09
EPA 6020B 10/30/17 05/09/17 13:41 5/22/2017 10:58
EPA 8260B 05/17/17 05/12/17 12:23 5/12/2017 21:40
4104-MW8A CA05956-05 Sampled:05/03/17 08:15 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 11:19
EPA 6020B 10/30/17 05/09/17 13:41 5/22/2017 11:02
EPA 8260B 05/17/17 05/12/17 12:23 5/12/2017 22:11
4104-MW9 CA05956-06 Sampled:05/03/17 08:50 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 11:21
EPA 6020B 10/30/17 05/09/17 13:41 5/22/2017 11:05
EPA 8260B 05/17/17 05/12/17 12:23 5/12/2017 22:41
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4104-MW10 CA05956-07 Sampled:05/03/17 10:30 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 11:24
EPA 6020B 10/30/17 05/09/17 13:41 5/22/2017 11:09
EPA 8260B 05/17/17 05/12/17 12:23 5/12/2017 23:11
4104-MW11 CA05956-08 Sampled:05/03/17 09:30 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 11:26
EPA 6020B 10/30/17 05/09/17 13:41 5/22/2017 11:13
EPA 8260B 05/17/17 05/12/17 12:23 5/12/2017 23:42
4104-MW12 CA05956-09 Sampled:05/03/17 09:05 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 11:29
EPA 6020B 10/30/17 05/09/17 13:41 5/22/2017 11:16
EPA 8260B 05/17/17 05/12/17 12:23 5/13/2017 00:12
4104-MW13S CA05956-10 Sampled:05/03/17 11:05 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 11:31
EPA 6020B 10/30/17 05/09/17 13:41 5/22/2017 11:27
EPA 8260B 05/17/17 05/12/17 12:23 5/13/2017 00:42
4104-MW14 CA05956-11 Sampled:05/03/17 11:30 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 11:37
EPA 6020B 10/30/17 05/12/17 12:27 5/22/2017 12:20
EPA 8260B 05/17/17 05/12/17 12:21 5/12/2017 17:02
4104-MW15 CA05956-12 Sampled:05/03/17 11:45 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 11:40
EPA 6020B 10/30/17 05/12/17 12:27 5/22/2017 12:42
EPA 8260B 05/17/17 05/12/17 12:21 5/12/2017 17:31
4104-MW16 CA05956-13 Sampled:05/03/17 12:20 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 11:42
EPA 6020B 10/30/17 05/12/17 12:27 5/22/2017 12:46
EPA 8260B 05/17/17 05/12/17 12:21 5/12/2017 18:01
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4104-MW17 CA05956-14 Sampled:05/03/17 12:45 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 11:45
EPA 6020B 10/30/17 05/12/17 12:27 5/22/2017 12:50
EPA 8260B 05/17/17 05/12/17 12:21 5/12/2017 18:31
4104-SW1 CA05956-15 Sampled:05/03/17 09:45 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 11:59
EPA 6020B 10/30/17 05/12/17 12:27 5/22/2017 13:06
EPA 8260B 05/17/17 05/12/17 12:21 5/12/2017 19:01
4104-SW3 CA05956-16 Sampled:05/03/17 08:30 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 12:02
EPA 6020B 10/30/17 05/12/17 12:27 5/22/2017 13:09
EPA 8260B 05/17/17 05/12/17 12:21 5/12/2017 19:30
4104-SW5 CA05956-17 Sampled:05/03/17 09:20 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 12:04
EPA 6020B 10/30/17 05/12/17 12:27 5/22/2017 13:13
EPA 8260B 05/17/17 05/12/17 12:21 5/12/2017 20:00
4104-SW6 CA05956-18 Sampled:05/03/17 12:00 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 12:07
EPA 6020B 10/30/17 05/12/17 12:27 5/22/2017 13:17
EPA 8260B 05/17/17 05/12/17 12:21 5/12/2017 20:30
4104-SW7 CA05956-19 Sampled:05/03/17 12:35 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 12:09
EPA 6020B 10/30/17 05/12/17 12:27 5/22/2017 13:20
EPA 8260B 05/17/17 05/12/17 12:21 5/12/2017 21:00
4104-SW8 CA05956-20 Sampled:05/03/17 13:00 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:33 5/11/2017 12:12
EPA 6020B 10/30/17 05/12/17 12:27 5/22/2017 13:24
EPA 8260B 05/17/17 05/12/17 12:21 5/12/2017 21:29
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4104-SW10 CA05956-21 Sampled:05/03/17 13:15 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 6010D 10/30/17 05/09/17 13:37 5/12/2017 10:59
EPA 6020B 10/30/17 05/12/17 12:27 5/22/2017 13:27
EPA 8260B 05/17/17 05/12/17 12:21 5/12/2017 21:59
4104-Tripblank CA05956-22 Sampled:05/03/17 08:00 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 8260B 05/17/17 05/11/17 14:59 5/11/2017 19:36
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NORTH CAROLINA SWS SAMPLE DETECTION SUMMARY
Analyte MethodUnitsResults
Lab ID:Client ID:4104-MW1 CA05956-01
Flag NotesMDLNC SWSLMRLDF
88.6 ug/L EPA 6010DJ 10010.01.001Barium - Total
0.561 ug/L EPA 6010DJ 11.000.1301Beryllium - Total
2.73 ug/L EPA 6010DJ 1010.01.401Chromium - Total
4.75 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
3.99 ug/L EPA 6010DJ 1010.01.601Copper - Total
10.9 ug/L EPA 6010DJ 5010.02.201Nickel - Total
0.119 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
1.1 ug/L EPA 8260B 11.00.141Toluene
44.9 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-MW3A CA05956-02
Flag NotesMDLNC SWSLMRLDF
62.3 ug/L EPA 6010DJ 10010.01.001Barium - Total
3.48 ug/L EPA 6010DJ 5010.02.201Nickel - Total
0.122 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
5.76 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
5.33 ug/L EPA 6010DJ 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-MW4 CA05956-03
Flag NotesMDLNC SWSLMRLDF
64.0 ug/L EPA 6010DJ 10010.01.001Barium - Total
0.316 ug/L EPA 6010DJ 11.000.1301Beryllium - Total
3.51 ug/L EPA 6010DJ 1010.01.401Chromium - Total
1.35 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
3.06 ug/L EPA 6010DJ 1010.01.601Copper - Total
2.68 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
10.3 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-MW6A CA05956-04
Flag NotesMDLNC SWSLMRLDF
271 ug/L EPA 6010D 10010.01.001Barium - Total
1.99 ug/L EPA 6010DJ 1010.01.401Chromium - Total
13.1 ug/L EPA 6010D 1010.01.101Cobalt - Total
2.78 ug/L EPA 6010DJ 1010.01.601Copper - Total
2.45 ug/L EPA 6010DJ 5010.02.201Nickel - Total
0.141 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
5.56 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
11.0 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-MW8A CA05956-05
Flag NotesMDLNC SWSLMRLDF
51.5 ug/L EPA 6010DJ 10010.01.001Barium - Total
1.80 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
1.64 ug/L EPA 6010DJ 1010.01.601Copper - Total
2.14 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
5.91 ug/L EPA 6010DJ 1010.04.401Zinc - Total
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Analyte MethodUnitsResults
Lab ID:Client ID:4104-MW9 CA05956-06
Flag NotesMDLNC SWSLMRLDF
181 ug/L EPA 6010D 10010.01.001Barium - Total
16.8 ug/L EPA 6010D 1010.01.401Chromium - Total
15.1 ug/L EPA 6010D 1010.01.101Cobalt - Total
22.8 ug/L EPA 6010D 1010.01.601Copper - Total
3.86 ug/L EPA 6010DJ 1010.03.101Lead - Total
11.0 ug/L EPA 6010DJ 5010.02.201Nickel - Total
0.965 ug/L EPA 6020BJ 103.000.9101Selenium - Total
0.160 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
43.2 ug/L EPA 6010D 2510.01.401Vanadium - Total
52.2 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-MW10 CA05956-07
Flag NotesMDLNC SWSLMRLDF
99.1 ug/L EPA 6010DJ 10010.01.001Barium - Total
2.34 ug/L EPA 6010DJ 1010.01.401Chromium - Total
5.36 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
3.91 ug/L EPA 6010DJ 1010.01.601Copper - Total
5.75 ug/L EPA 6010DJ 5010.02.201Nickel - Total
0.113 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
0.78 ug/L EPA 8260BJ 11.00.141Toluene
17.8 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
24.4 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-MW11 CA05956-08
Flag NotesMDLNC SWSLMRLDF
129 ug/L EPA 6010D 10010.01.001Barium - Total
1.54 ug/L EPA 6010DJ 1010.01.401Chromium - Total
3.22 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
3.69 ug/L EPA 6010DJ 1010.01.601Copper - Total
2.82 ug/L EPA 6010DJ 5010.02.201Nickel - Total
11.0 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
36.9 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-MW12 CA05956-09
Flag NotesMDLNC SWSLMRLDF
189 ug/L EPA 6010D 10010.01.001Barium - Total
3.72 ug/L EPA 6010DJ 1010.01.401Chromium - Total
2.68 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
4.94 ug/L EPA 6010DJ 1010.01.601Copper - Total
16.7 ug/L EPA 6010DJ 5010.02.201Nickel - Total
1.1 ug/L EPA 8260B 11.00.141Toluene
7.70 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
10.3 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-MW13S CA05956-10
Flag NotesMDLNC SWSLMRLDF
251 ug/L EPA 6010D 10010.01.001Barium - Total
0.293 ug/L EPA 6010DJ 11.000.1301Beryllium - Total
4.86 ug/L EPA 6010DJ 1010.01.401Chromium - Total
15.7 ug/L EPA 6010D 1010.01.101Cobalt - Total
19.6 ug/L EPA 6010D 1010.01.601Copper - Total
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Analyte MethodUnitsResults
Lab ID:Client ID:4104-MW13S CA05956-10
Flag NotesMDLNC SWSLMRLDF
7.96 ug/L EPA 6010DJ 5010.02.201Nickel - Total
0.136 ug/L EPA 6020BJ 5.51.000.1101Thallium - Total
24.9 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
131 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-MW14 CA05956-11
Flag NotesMDLNC SWSLMRLDF
41.2 ug/L EPA 6010DJ 10010.01.001Barium - Total
0.44 ug/L EPA 8260BJ 11.00.141Toluene
1.67 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
8.43 ug/L EPA 6010DJ 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-MW15 CA05956-12
Flag NotesMDLNC SWSLMRLDF
23.1 ug/L EPA 6010DJ 10010.01.001Barium - Total
1.20 ug/L EPA 6020BJ 103.000.9101Selenium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-MW16 CA05956-13
Flag NotesMDLNC SWSLMRLDF
79.2 ug/L EPA 6010DJ 10010.01.001Barium - Total
1.89 ug/L EPA 6010DJ 1010.01.601Copper - Total
2.21 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-MW17 CA05956-14
Flag NotesMDLNC SWSLMRLDF
87.7 ug/L EPA 6010DJ 10010.01.001Barium - Total
1.86 ug/L EPA 6010DJ 1010.01.601Copper - Total
14.8 ug/L EPA 6010DJ 5010.02.201Nickel - Total
3.51 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
5.43 ug/L EPA 6010DJ 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-SW1 CA05956-15
Flag NotesMDLNC SWSLMRLDF
68.3 ug/L EPA 6010DJ 10010.01.001Barium - Total
3.32 ug/L EPA 6010DJ 1010.01.601Copper - Total
3.39 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
7.93 ug/L EPA 6010DJ 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-SW3 CA05956-16
Flag NotesMDLNC SWSLMRLDF
0.443 ug/L EPA 6020BJ 62.000.3701Antimony - Total
88.8 ug/L EPA 6010DJ 10010.01.001Barium - Total
2.52 ug/L EPA 6010DJ 1010.01.601Copper - Total
1.62 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-SW5 CA05956-17
Flag NotesMDLNC SWSLMRLDF
66.4 ug/L EPA 6010DJ 10010.01.001Barium - Total
3.03 ug/L EPA 6010DJ 1010.01.601Copper - Total
4.21 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
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Analyte MethodUnitsResults
Lab ID:Client ID:4104-SW5 CA05956-17
Flag NotesMDLNC SWSLMRLDF
6.35 ug/L EPA 6010DJ 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-SW6 CA05956-18
Flag NotesMDLNC SWSLMRLDF
55.7 ug/L EPA 6010DJ 10010.01.001Barium - Total
1.29 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
2.82 ug/L EPA 6010DJ 1010.01.601Copper - Total
1.49 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
12.4 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-SW7 CA05956-19
Flag NotesMDLNC SWSLMRLDF
53.5 ug/L EPA 6010DJ 10010.01.001Barium - Total
1.63 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
1.79 ug/L EPA 6010DJ 1010.01.601Copper - Total
6.65 ug/L EPA 6010DJ 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-SW8 CA05956-20
Flag NotesMDLNC SWSLMRLDF
0.370 ug/L EPA 6020BJ 62.000.3701Antimony - Total
83.5 ug/L EPA 6010DJ 10010.01.001Barium - Total
1.26 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
3.01 ug/L EPA 6010DJ 1010.01.601Copper - Total
2.39 ug/L EPA 6010DJ 5010.02.201Nickel - Total
2.56 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-SW10 CA05956-21
Flag NotesMDLNC SWSLMRLDF
219 ug/L EPA 6010D 10010.01.001Barium - Total
7.31 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
2.63 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
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ANALYTICAL RESULTS
4104-MW1Description:Lab Sample ID:CA05956-01 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 10:15 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 20:091,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/12/17 20:091,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/12/17 20:091,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/12/17 20:091,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 20:091,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/12/17 20:091,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 20:091,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 20:091,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/12/17 20:091,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/12/17 20:091,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/12/17 20:091,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/12/17 20:091,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/12/17 20:091,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/12/17 20:092-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/12/17 20:092-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/12/17 20:094-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/12/17 20:09Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/12/17 20:09Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/12/17 20:09Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 20:09Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/12/17 20:09Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 20:09Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/12/17 20:09Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/12/17 20:09Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/12/17 20:09Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 20:09Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 20:09Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/12/17 20:09Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/12/17 20:09Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 20:09cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/12/17 20:09cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/12/17 20:09Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 20:09Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/12/17 20:09Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 20:09Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/12/17 20:09m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/12/17 20:09Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 20:09o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/12/17 20:09Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/12/17 20:09Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 20:09Toluene [108-88-3] ^0.14 MRK1.01.1 11
ug/L EPA 8260B 05/12/17 20:09trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 20:09trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 20:09trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/12/17 20:09Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 20:09Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/12/17 20:09Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/12/17 20:09Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
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4104-MW1Description:Lab Sample ID:CA05956-01 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 10:15 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 20:09Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13691 %MRKEPA 8260B 05/12/17 20:097E120224650.0 1
Dibromofluoromethane 67-12989 %MRKEPA 8260B 05/12/17 20:097E120224450.0 1
Toluene-d8 59-13493 %MRKEPA 8260B 05/12/17 20:097E120224650.0 1
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4104-MW1Description:Lab Sample ID:CA05956-01 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 10:15 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 10:47Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/11/17 10:51Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 10:51Barium [7440-39-3] ^1.00 JMV10.088.6 J 1001
ug/L EPA 6010D 05/11/17 10:51Beryllium [7440-41-7] ^0.130 JMV1.000.561 J 11
ug/L EPA 6010D 05/11/17 10:51Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 10:51Chromium [7440-47-3] ^1.40 JMV10.02.73 J 101
ug/L EPA 6010D 05/11/17 10:51Cobalt [7440-48-4] ^1.10 JMV10.04.75 J 101
ug/L EPA 6010D 05/11/17 10:51Copper [7440-50-8] ^1.60 JMV10.03.99 J 101
ug/L EPA 6010D 05/11/17 10:51Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/11/17 10:51Nickel [7440-02-0] ^2.20 JMV10.010.9 J 501
ug/L EPA 6020B 05/22/17 10:47Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/11/17 10:51Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 10:47Thallium [7440-28-0] ^0.110 JDH1.000.119 J 5.51
ug/L EPA 6010D 05/11/17 10:51Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 05/11/17 10:51Zinc [7440-66-6] ^4.40 JMV10.044.9 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-MW3ADescription:Lab Sample ID:CA05956-02 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 08:00 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 20:401,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/12/17 20:401,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/12/17 20:401,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/12/17 20:401,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 20:401,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/12/17 20:401,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 20:401,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 20:401,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/12/17 20:401,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/12/17 20:401,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/12/17 20:401,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/12/17 20:401,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/12/17 20:401,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/12/17 20:402-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/12/17 20:402-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/12/17 20:404-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/12/17 20:40Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/12/17 20:40Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/12/17 20:40Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 20:40Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/12/17 20:40Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 20:40Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/12/17 20:40Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/12/17 20:40Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/12/17 20:40Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 20:40Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 20:40Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/12/17 20:40Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/12/17 20:40Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 20:40cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/12/17 20:40cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/12/17 20:40Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 20:40Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/12/17 20:40Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 20:40Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/12/17 20:40m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/12/17 20:40Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 20:40o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/12/17 20:40Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/12/17 20:40Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 20:40Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 20:40trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 20:40trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 20:40trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/12/17 20:40Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 20:40Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/12/17 20:40Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/12/17 20:40Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/12/17 20:40Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-MW3ADescription:Lab Sample ID:CA05956-02 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 08:00 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13691 %MRKEPA 8260B 05/12/17 20:407E120224550.0 1
Dibromofluoromethane 67-12987 %MRKEPA 8260B 05/12/17 20:407E120224450.0 1
Toluene-d8 59-13492 %MRKEPA 8260B 05/12/17 20:407E120224650.0 1
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4104-MW3ADescription:Lab Sample ID:CA05956-02 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 08:00 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 10:51Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/11/17 11:03Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 11:03Barium [7440-39-3] ^1.00 JMV10.062.3 J 1001
ug/L EPA 6010D 05/11/17 11:03Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/11/17 11:03Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 11:03Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/11/17 11:03Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 05/11/17 11:03Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 05/11/17 11:03Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/11/17 11:03Nickel [7440-02-0] ^2.20 JMV10.03.48 J 501
ug/L EPA 6020B 05/22/17 10:51Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/11/17 11:03Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 10:51Thallium [7440-28-0] ^0.110 JDH1.000.122 J 5.51
ug/L EPA 6010D 05/11/17 11:03Vanadium [7440-62-2] ^1.40 JMV10.05.76 J 251
ug/L EPA 6010D 05/11/17 11:03Zinc [7440-66-6] ^4.40 JMV10.05.33 J 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-MW4Description:Lab Sample ID:CA05956-03 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 10:05 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 21:101,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/12/17 21:101,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/12/17 21:101,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/12/17 21:101,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 21:101,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/12/17 21:101,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 21:101,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 21:101,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/12/17 21:101,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/12/17 21:101,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/12/17 21:101,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/12/17 21:101,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/12/17 21:101,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/12/17 21:102-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/12/17 21:102-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/12/17 21:104-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/12/17 21:10Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/12/17 21:10Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/12/17 21:10Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 21:10Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/12/17 21:10Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 21:10Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/12/17 21:10Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/12/17 21:10Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/12/17 21:10Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 21:10Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 21:10Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/12/17 21:10Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/12/17 21:10Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 21:10cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/12/17 21:10cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/12/17 21:10Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 21:10Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/12/17 21:10Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 21:10Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/12/17 21:10m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/12/17 21:10Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 21:10o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/12/17 21:10Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/12/17 21:10Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 21:10Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 21:10trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 21:10trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 21:10trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/12/17 21:10Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 21:10Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/12/17 21:10Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/12/17 21:10Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/12/17 21:10Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-MW4Description:Lab Sample ID:CA05956-03 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 10:05 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13697 %MRKEPA 8260B 05/12/17 21:107E120224950.0 1
Dibromofluoromethane 67-12994 %MRKEPA 8260B 05/12/17 21:107E120224750.0 1
Toluene-d8 59-13498 %MRKEPA 8260B 05/12/17 21:107E120224950.0 1
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4104-MW4Description:Lab Sample ID:CA05956-03 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 10:05 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 10:54Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/11/17 11:06Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 11:06Barium [7440-39-3] ^1.00 JMV10.064.0 J 1001
ug/L EPA 6010D 05/11/17 11:06Beryllium [7440-41-7] ^0.130 JMV1.000.316 J 11
ug/L EPA 6010D 05/11/17 11:06Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 11:06Chromium [7440-47-3] ^1.40 JMV10.03.51 J 101
ug/L EPA 6010D 05/11/17 11:06Cobalt [7440-48-4] ^1.10 JMV10.01.35 J 101
ug/L EPA 6010D 05/11/17 11:06Copper [7440-50-8] ^1.60 JMV10.03.06 J 101
ug/L EPA 6010D 05/11/17 11:06Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/11/17 11:06Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/22/17 10:54Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/11/17 11:06Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 10:54Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/11/17 11:06Vanadium [7440-62-2] ^1.40 JMV10.02.68 J 251
ug/L EPA 6010D 05/11/17 11:06Zinc [7440-66-6] ^4.40 JMV10.010.3 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-MW6ADescription:Lab Sample ID:CA05956-04 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 08:40 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 21:401,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/12/17 21:401,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/12/17 21:401,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/12/17 21:401,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 21:401,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/12/17 21:401,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 21:401,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 21:401,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/12/17 21:401,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/12/17 21:401,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/12/17 21:401,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/12/17 21:401,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/12/17 21:401,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/12/17 21:402-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/12/17 21:402-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/12/17 21:404-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/12/17 21:40Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/12/17 21:40Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/12/17 21:40Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 21:40Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/12/17 21:40Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 21:40Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/12/17 21:40Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/12/17 21:40Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/12/17 21:40Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 21:40Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 21:40Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/12/17 21:40Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/12/17 21:40Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 21:40cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/12/17 21:40cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/12/17 21:40Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 21:40Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/12/17 21:40Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 21:40Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/12/17 21:40m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/12/17 21:40Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 21:40o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/12/17 21:40Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/12/17 21:40Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 21:40Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 21:40trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 21:40trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 21:40trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/12/17 21:40Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 21:40Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/12/17 21:40Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/12/17 21:40Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/12/17 21:40Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-MW6ADescription:Lab Sample ID:CA05956-04 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 08:40 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13691 %MRKEPA 8260B 05/12/17 21:407E120224650.0 1
Dibromofluoromethane 67-12990 %MRKEPA 8260B 05/12/17 21:407E120224550.0 1
Toluene-d8 59-13495 %MRKEPA 8260B 05/12/17 21:407E120224850.0 1
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4104-MW6ADescription:Lab Sample ID:CA05956-04 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 08:40 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 10:58Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/11/17 11:09Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 11:09Barium [7440-39-3] ^1.00 JMV10.0271 1001
ug/L EPA 6010D 05/11/17 11:09Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/11/17 11:09Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 11:09Chromium [7440-47-3] ^1.40 JMV10.01.99 J 101
ug/L EPA 6010D 05/11/17 11:09Cobalt [7440-48-4] ^1.10 JMV10.013.1 101
ug/L EPA 6010D 05/11/17 11:09Copper [7440-50-8] ^1.60 JMV10.02.78 J 101
ug/L EPA 6010D 05/11/17 11:09Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/11/17 11:09Nickel [7440-02-0] ^2.20 JMV10.02.45 J 501
ug/L EPA 6020B 05/22/17 10:58Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/11/17 11:09Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 10:58Thallium [7440-28-0] ^0.110 JDH1.000.141 J 5.51
ug/L EPA 6010D 05/11/17 11:09Vanadium [7440-62-2] ^1.40 JMV10.05.56 J 251
ug/L EPA 6010D 05/11/17 11:09Zinc [7440-66-6] ^4.40 JMV10.011.0 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-MW8ADescription:Lab Sample ID:CA05956-05 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 08:15 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 22:111,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/12/17 22:111,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/12/17 22:111,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/12/17 22:111,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 22:111,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/12/17 22:111,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 22:111,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 22:111,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/12/17 22:111,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/12/17 22:111,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/12/17 22:111,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/12/17 22:111,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/12/17 22:111,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/12/17 22:112-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/12/17 22:112-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/12/17 22:114-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/12/17 22:11Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/12/17 22:11Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/12/17 22:11Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 22:11Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/12/17 22:11Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 22:11Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/12/17 22:11Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/12/17 22:11Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/12/17 22:11Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 22:11Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 22:11Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/12/17 22:11Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/12/17 22:11Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 22:11cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/12/17 22:11cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/12/17 22:11Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 22:11Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/12/17 22:11Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 22:11Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/12/17 22:11m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/12/17 22:11Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 22:11o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/12/17 22:11Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/12/17 22:11Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 22:11Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 22:11trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 22:11trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 22:11trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/12/17 22:11Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 22:11Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/12/17 22:11Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/12/17 22:11Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/12/17 22:11Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-MW8ADescription:Lab Sample ID:CA05956-05 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 08:15 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13689 %MRKEPA 8260B 05/12/17 22:117E120224550.0 1
Dibromofluoromethane 67-12989 %MRKEPA 8260B 05/12/17 22:117E120224550.0 1
Toluene-d8 59-13493 %MRKEPA 8260B 05/12/17 22:117E120224750.0 1
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4104-MW8ADescription:Lab Sample ID:CA05956-05 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 08:15 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 11:02Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/11/17 11:19Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 11:19Barium [7440-39-3] ^1.00 JMV10.051.5 J 1001
ug/L EPA 6010D 05/11/17 11:19Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/11/17 11:19Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 11:19Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/11/17 11:19Cobalt [7440-48-4] ^1.10 JMV10.01.80 J 101
ug/L EPA 6010D 05/11/17 11:19Copper [7440-50-8] ^1.60 JMV10.01.64 J 101
ug/L EPA 6010D 05/11/17 11:19Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/11/17 11:19Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/22/17 11:02Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/11/17 11:19Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 11:02Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/11/17 11:19Vanadium [7440-62-2] ^1.40 JMV10.02.14 J 251
ug/L EPA 6010D 05/11/17 11:19Zinc [7440-66-6] ^4.40 JMV10.05.91 J 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-MW9Description:Lab Sample ID:CA05956-06 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 08:50 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 22:411,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/12/17 22:411,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/12/17 22:411,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/12/17 22:411,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 22:411,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/12/17 22:411,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 22:411,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 22:411,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/12/17 22:411,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/12/17 22:411,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/12/17 22:411,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/12/17 22:411,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/12/17 22:411,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/12/17 22:412-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/12/17 22:412-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/12/17 22:414-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/12/17 22:41Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/12/17 22:41Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/12/17 22:41Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 22:41Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/12/17 22:41Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 22:41Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/12/17 22:41Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/12/17 22:41Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/12/17 22:41Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 22:41Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 22:41Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/12/17 22:41Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/12/17 22:41Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 22:41cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/12/17 22:41cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/12/17 22:41Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 22:41Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/12/17 22:41Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 22:41Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/12/17 22:41m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/12/17 22:41Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 22:41o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/12/17 22:41Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/12/17 22:41Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 22:41Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 22:41trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 22:41trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 22:41trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/12/17 22:41Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 22:41Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/12/17 22:41Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/12/17 22:41Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/12/17 22:41Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-MW9Description:Lab Sample ID:CA05956-06 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 08:50 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13691 %MRKEPA 8260B 05/12/17 22:417E120224650.0 1
Dibromofluoromethane 67-12988 %MRKEPA 8260B 05/12/17 22:417E120224450.0 1
Toluene-d8 59-13493 %MRKEPA 8260B 05/12/17 22:417E120224650.0 1
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4104-MW9Description:Lab Sample ID:CA05956-06 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 08:50 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 11:05Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/11/17 11:21Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 11:21Barium [7440-39-3] ^1.00 JMV10.0181 1001
ug/L EPA 6010D 05/11/17 11:21Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/11/17 11:21Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 11:21Chromium [7440-47-3] ^1.40 JMV10.016.8 101
ug/L EPA 6010D 05/11/17 11:21Cobalt [7440-48-4] ^1.10 JMV10.015.1 101
ug/L EPA 6010D 05/11/17 11:21Copper [7440-50-8] ^1.60 JMV10.022.8 101
ug/L EPA 6010D 05/11/17 11:21Lead [7439-92-1] ^3.10 JMV10.03.86 J 101
ug/L EPA 6010D 05/11/17 11:21Nickel [7440-02-0] ^2.20 JMV10.011.0 J 501
ug/L EPA 6020B 05/22/17 11:05Selenium [7782-49-2] ^0.910 JDH3.000.965 J 101
ug/L EPA 6010D 05/11/17 11:21Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 11:05Thallium [7440-28-0] ^0.110 JDH1.000.160 J 5.51
ug/L EPA 6010D 05/11/17 11:21Vanadium [7440-62-2] ^1.40 JMV10.043.2 251
ug/L EPA 6010D 05/11/17 11:21Zinc [7440-66-6] ^4.40 JMV10.052.2 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-MW10Description:Lab Sample ID:CA05956-07 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 10:30 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 23:111,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/12/17 23:111,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/12/17 23:111,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/12/17 23:111,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 23:111,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/12/17 23:111,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 23:111,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 23:111,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/12/17 23:111,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/12/17 23:111,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/12/17 23:111,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/12/17 23:111,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/12/17 23:111,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/12/17 23:112-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/12/17 23:112-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/12/17 23:114-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/12/17 23:11Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/12/17 23:11Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/12/17 23:11Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 23:11Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/12/17 23:11Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 23:11Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/12/17 23:11Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/12/17 23:11Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/12/17 23:11Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 23:11Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 23:11Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/12/17 23:11Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/12/17 23:11Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 23:11cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/12/17 23:11cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/12/17 23:11Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 23:11Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/12/17 23:11Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 23:11Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/12/17 23:11m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/12/17 23:11Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 23:11o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/12/17 23:11Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/12/17 23:11Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 23:11Toluene [108-88-3] ^0.14 MRK1.00.78 J 11
ug/L EPA 8260B 05/12/17 23:11trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 23:11trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 23:11trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/12/17 23:11Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 23:11Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/12/17 23:11Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/12/17 23:11Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/12/17 23:11Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-MW10Description:Lab Sample ID:CA05956-07 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 10:30 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13689 %MRKEPA 8260B 05/12/17 23:117E120224550.0 1
Dibromofluoromethane 67-12990 %MRKEPA 8260B 05/12/17 23:117E120224550.0 1
Toluene-d8 59-13494 %MRKEPA 8260B 05/12/17 23:117E120224750.0 1
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4104-MW10Description:Lab Sample ID:CA05956-07 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 10:30 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 11:09Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/11/17 11:24Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 11:24Barium [7440-39-3] ^1.00 JMV10.099.1 J 1001
ug/L EPA 6010D 05/11/17 11:24Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/11/17 11:24Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 11:24Chromium [7440-47-3] ^1.40 JMV10.02.34 J 101
ug/L EPA 6010D 05/11/17 11:24Cobalt [7440-48-4] ^1.10 JMV10.05.36 J 101
ug/L EPA 6010D 05/11/17 11:24Copper [7440-50-8] ^1.60 JMV10.03.91 J 101
ug/L EPA 6010D 05/11/17 11:24Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/11/17 11:24Nickel [7440-02-0] ^2.20 JMV10.05.75 J 501
ug/L EPA 6020B 05/22/17 11:09Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/11/17 11:24Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 11:09Thallium [7440-28-0] ^0.110 JDH1.000.113 J 5.51
ug/L EPA 6010D 05/11/17 11:24Vanadium [7440-62-2] ^1.40 JMV10.017.8 J 251
ug/L EPA 6010D 05/11/17 11:24Zinc [7440-66-6] ^4.40 JMV10.024.4 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-MW11Description:Lab Sample ID:CA05956-08 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 09:30 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 23:421,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/12/17 23:421,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/12/17 23:421,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/12/17 23:421,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 23:421,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/12/17 23:421,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 23:421,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 23:421,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/12/17 23:421,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/12/17 23:421,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/12/17 23:421,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/12/17 23:421,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/12/17 23:421,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/12/17 23:422-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/12/17 23:422-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/12/17 23:424-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/12/17 23:42Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/12/17 23:42Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/12/17 23:42Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 23:42Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/12/17 23:42Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 23:42Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/12/17 23:42Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/12/17 23:42Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/12/17 23:42Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 23:42Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 23:42Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/12/17 23:42Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/12/17 23:42Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 23:42cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/12/17 23:42cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/12/17 23:42Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 23:42Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/12/17 23:42Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 23:42Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/12/17 23:42m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/12/17 23:42Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 23:42o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/12/17 23:42Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/12/17 23:42Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 23:42Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 23:42trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 23:42trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 23:42trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/12/17 23:42Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 23:42Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/12/17 23:42Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/12/17 23:42Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/12/17 23:42Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-MW11Description:Lab Sample ID:CA05956-08 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 09:30 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13692 %MRKEPA 8260B 05/12/17 23:427E120224650.0 1
Dibromofluoromethane 67-12989 %MRKEPA 8260B 05/12/17 23:427E120224450.0 1
Toluene-d8 59-13492 %MRKEPA 8260B 05/12/17 23:427E120224650.0 1
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4104-MW11Description:Lab Sample ID:CA05956-08 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 09:30 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 11:13Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/11/17 11:26Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 11:26Barium [7440-39-3] ^1.00 JMV10.0129 1001
ug/L EPA 6010D 05/11/17 11:26Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/11/17 11:26Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 11:26Chromium [7440-47-3] ^1.40 JMV10.01.54 J 101
ug/L EPA 6010D 05/11/17 11:26Cobalt [7440-48-4] ^1.10 JMV10.03.22 J 101
ug/L EPA 6010D 05/11/17 11:26Copper [7440-50-8] ^1.60 JMV10.03.69 J 101
ug/L EPA 6010D 05/11/17 11:26Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/11/17 11:26Nickel [7440-02-0] ^2.20 JMV10.02.82 J 501
ug/L EPA 6020B 05/22/17 11:13Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/11/17 11:26Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 11:13Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/11/17 11:26Vanadium [7440-62-2] ^1.40 JMV10.011.0 J 251
ug/L EPA 6010D 05/11/17 11:26Zinc [7440-66-6] ^4.40 JMV10.036.9 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-MW12Description:Lab Sample ID:CA05956-09 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 09:05 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/13/17 00:121,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/13/17 00:121,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/13/17 00:121,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/13/17 00:121,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/13/17 00:121,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/13/17 00:121,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/13/17 00:121,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/13/17 00:121,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/13/17 00:121,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/13/17 00:121,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/13/17 00:121,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/13/17 00:121,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/13/17 00:121,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/13/17 00:122-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/13/17 00:122-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/13/17 00:124-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/13/17 00:12Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/13/17 00:12Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/13/17 00:12Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/13/17 00:12Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/13/17 00:12Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/13/17 00:12Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/13/17 00:12Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/13/17 00:12Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/13/17 00:12Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/13/17 00:12Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/13/17 00:12Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/13/17 00:12Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/13/17 00:12Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/13/17 00:12cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/13/17 00:12cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/13/17 00:12Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/13/17 00:12Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/13/17 00:12Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/13/17 00:12Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/13/17 00:12m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/13/17 00:12Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/13/17 00:12o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/13/17 00:12Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/13/17 00:12Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/13/17 00:12Toluene [108-88-3] ^0.14 MRK1.01.1 11
ug/L EPA 8260B 05/13/17 00:12trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/13/17 00:12trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/13/17 00:12trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/13/17 00:12Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/13/17 00:12Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/13/17 00:12Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/13/17 00:12Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/13/17 00:12Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-MW12Description:Lab Sample ID:CA05956-09 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 09:05 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13691 %MRKEPA 8260B 05/13/17 00:127E120224650.0 1
Dibromofluoromethane 67-12989 %MRKEPA 8260B 05/13/17 00:127E120224550.0 1
Toluene-d8 59-13492 %MRKEPA 8260B 05/13/17 00:127E120224650.0 1
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4104-MW12Description:Lab Sample ID:CA05956-09 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 09:05 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 11:16Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/11/17 11:29Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 11:29Barium [7440-39-3] ^1.00 JMV10.0189 1001
ug/L EPA 6010D 05/11/17 11:29Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/11/17 11:29Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 11:29Chromium [7440-47-3] ^1.40 JMV10.03.72 J 101
ug/L EPA 6010D 05/11/17 11:29Cobalt [7440-48-4] ^1.10 JMV10.02.68 J 101
ug/L EPA 6010D 05/11/17 11:29Copper [7440-50-8] ^1.60 JMV10.04.94 J 101
ug/L EPA 6010D 05/11/17 11:29Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/11/17 11:29Nickel [7440-02-0] ^2.20 JMV10.016.7 J 501
ug/L EPA 6020B 05/22/17 11:16Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/11/17 11:29Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 11:16Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/11/17 11:29Vanadium [7440-62-2] ^1.40 JMV10.07.70 J 251
ug/L EPA 6010D 05/11/17 11:29Zinc [7440-66-6] ^4.40 JMV10.010.3 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-MW13SDescription:Lab Sample ID:CA05956-10 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 11:05 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/13/17 00:421,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/13/17 00:421,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/13/17 00:421,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/13/17 00:421,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/13/17 00:421,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/13/17 00:421,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/13/17 00:421,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/13/17 00:421,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/13/17 00:421,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/13/17 00:421,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/13/17 00:421,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/13/17 00:421,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/13/17 00:421,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/13/17 00:422-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/13/17 00:422-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/13/17 00:424-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/13/17 00:42Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/13/17 00:42Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/13/17 00:42Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/13/17 00:42Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/13/17 00:42Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/13/17 00:42Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/13/17 00:42Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/13/17 00:42Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/13/17 00:42Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/13/17 00:42Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/13/17 00:42Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/13/17 00:42Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/13/17 00:42Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/13/17 00:42cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/13/17 00:42cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/13/17 00:42Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/13/17 00:42Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/13/17 00:42Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/13/17 00:42Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/13/17 00:42m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/13/17 00:42Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/13/17 00:42o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/13/17 00:42Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/13/17 00:42Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/13/17 00:42Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/13/17 00:42trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/13/17 00:42trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/13/17 00:42trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/13/17 00:42Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/13/17 00:42Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/13/17 00:42Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/13/17 00:42Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/13/17 00:42Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-MW13SDescription:Lab Sample ID:CA05956-10 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 11:05 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13689 %MRKEPA 8260B 05/13/17 00:427E120224450.0 1
Dibromofluoromethane 67-12988 %MRKEPA 8260B 05/13/17 00:427E120224450.0 1
Toluene-d8 59-13492 %MRKEPA 8260B 05/13/17 00:427E120224650.0 1
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4104-MW13SDescription:Lab Sample ID:CA05956-10 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 11:05 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 11:27Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/11/17 11:31Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 11:31Barium [7440-39-3] ^1.00 JMV10.0251 1001
ug/L EPA 6010D 05/11/17 11:31Beryllium [7440-41-7] ^0.130 JMV1.000.293 J 11
ug/L EPA 6010D 05/11/17 11:31Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 11:31Chromium [7440-47-3] ^1.40 JMV10.04.86 J 101
ug/L EPA 6010D 05/11/17 11:31Cobalt [7440-48-4] ^1.10 JMV10.015.7 101
ug/L EPA 6010D 05/11/17 11:31Copper [7440-50-8] ^1.60 JMV10.019.6 101
ug/L EPA 6010D 05/11/17 11:31Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/11/17 11:31Nickel [7440-02-0] ^2.20 JMV10.07.96 J 501
ug/L EPA 6020B 05/22/17 11:27Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/11/17 11:31Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 11:27Thallium [7440-28-0] ^0.110 JDH1.000.136 J 5.51
ug/L EPA 6010D 05/11/17 11:31Vanadium [7440-62-2] ^1.40 JMV10.024.9 J 251
ug/L EPA 6010D 05/11/17 11:31Zinc [7440-66-6] ^4.40 JMV10.0131 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-MW14Description:Lab Sample ID:CA05956-11 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 11:30 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 17:021,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/12/17 17:021,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/12/17 17:021,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/12/17 17:021,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 17:021,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/12/17 17:021,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 17:021,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 17:021,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/12/17 17:021,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/12/17 17:021,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/12/17 17:021,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/12/17 17:021,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/12/17 17:021,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/12/17 17:022-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/12/17 17:022-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/12/17 17:024-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/12/17 17:02Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/12/17 17:02Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/12/17 17:02Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 17:02Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/12/17 17:02Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 17:02Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/12/17 17:02Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/12/17 17:02Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/12/17 17:02Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 17:02Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 17:02Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/12/17 17:02Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/12/17 17:02Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 17:02cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/12/17 17:02cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/12/17 17:02Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 17:02Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/12/17 17:02Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 17:02Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/12/17 17:02m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/12/17 17:02Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 17:02o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/12/17 17:02Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/12/17 17:02Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 17:02Toluene [108-88-3] ^0.14 MRK1.00.44 J 11
ug/L EPA 8260B 05/12/17 17:02trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 17:02trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 17:02trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/12/17 17:02Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 17:02Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/12/17 17:02Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/12/17 17:02Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/12/17 17:02Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-MW14Description:Lab Sample ID:CA05956-11 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 11:30 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136101 %MRKEPA 8260B 05/12/17 17:027E120215150.0 1
Dibromofluoromethane 67-129105 %MRKEPA 8260B 05/12/17 17:027E120215350.0 1
Toluene-d8 59-134106 %MRKEPA 8260B 05/12/17 17:027E120215350.0 1
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4104-MW14Description:Lab Sample ID:CA05956-11 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 11:30 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 12:20Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/11/17 11:37Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 11:37Barium [7440-39-3] ^1.00 JMV10.041.2 J 1001
ug/L EPA 6010D 05/11/17 11:37Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/11/17 11:37Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 11:37Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/11/17 11:37Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 05/11/17 11:37Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 05/11/17 11:37Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/11/17 11:37Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/22/17 12:20Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/11/17 11:37Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 12:20Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/11/17 11:37Vanadium [7440-62-2] ^1.40 JMV10.01.67 J 251
ug/L EPA 6010D 05/11/17 11:37Zinc [7440-66-6] ^4.40 JMV10.08.43 J 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-MW15Description:Lab Sample ID:CA05956-12 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 11:45 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 17:311,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/12/17 17:311,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/12/17 17:311,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/12/17 17:311,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 17:311,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/12/17 17:311,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 17:311,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 17:311,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/12/17 17:311,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/12/17 17:311,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/12/17 17:311,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/12/17 17:311,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/12/17 17:311,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/12/17 17:312-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/12/17 17:312-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/12/17 17:314-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/12/17 17:31Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/12/17 17:31Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/12/17 17:31Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 17:31Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/12/17 17:31Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 17:31Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/12/17 17:31Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/12/17 17:31Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/12/17 17:31Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 17:31Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 17:31Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/12/17 17:31Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/12/17 17:31Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 17:31cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/12/17 17:31cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/12/17 17:31Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 17:31Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/12/17 17:31Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 17:31Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/12/17 17:31m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/12/17 17:31Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 17:31o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/12/17 17:31Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/12/17 17:31Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 17:31Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 17:31trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 17:31trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 17:31trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/12/17 17:31Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 17:31Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/12/17 17:31Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/12/17 17:31Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/12/17 17:31Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-MW15Description:Lab Sample ID:CA05956-12 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 11:45 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136105 %MRKEPA 8260B 05/12/17 17:317E120215350.0 1
Dibromofluoromethane 67-129110 %MRKEPA 8260B 05/12/17 17:317E120215550.0 1
Toluene-d8 59-134108 %MRKEPA 8260B 05/12/17 17:317E120215450.0 1
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4104-MW15Description:Lab Sample ID:CA05956-12 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 11:45 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 12:42Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/11/17 11:40Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 11:40Barium [7440-39-3] ^1.00 JMV10.023.1 J 1001
ug/L EPA 6010D 05/11/17 11:40Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/11/17 11:40Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 11:40Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/11/17 11:40Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 05/11/17 11:40Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 05/11/17 11:40Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/11/17 11:40Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/22/17 12:42Selenium [7782-49-2] ^0.910 JDH3.001.20 J 101
ug/L EPA 6010D 05/11/17 11:40Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 12:42Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/11/17 11:40Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 05/11/17 11:40Zinc [7440-66-6] ^4.40 JMV10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-MW16Description:Lab Sample ID:CA05956-13 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 12:20 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 18:011,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/12/17 18:011,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/12/17 18:011,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/12/17 18:011,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 18:011,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/12/17 18:011,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 18:011,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 18:011,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/12/17 18:011,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/12/17 18:011,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/12/17 18:011,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/12/17 18:011,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/12/17 18:011,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/12/17 18:012-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/12/17 18:012-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/12/17 18:014-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/12/17 18:01Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/12/17 18:01Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/12/17 18:01Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 18:01Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/12/17 18:01Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 18:01Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/12/17 18:01Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/12/17 18:01Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/12/17 18:01Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 18:01Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 18:01Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/12/17 18:01Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/12/17 18:01Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 18:01cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/12/17 18:01cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/12/17 18:01Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 18:01Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/12/17 18:01Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 18:01Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/12/17 18:01m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/12/17 18:01Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 18:01o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/12/17 18:01Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/12/17 18:01Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 18:01Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 18:01trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 18:01trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 18:01trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/12/17 18:01Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 18:01Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/12/17 18:01Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/12/17 18:01Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/12/17 18:01Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-MW16Description:Lab Sample ID:CA05956-13 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 12:20 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136103 %MRKEPA 8260B 05/12/17 18:017E120215250.0 1
Dibromofluoromethane 67-129106 %MRKEPA 8260B 05/12/17 18:017E120215350.0 1
Toluene-d8 59-134107 %MRKEPA 8260B 05/12/17 18:017E120215450.0 1
Page 47 of 87
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www.encolabs.com
4104-MW16Description:Lab Sample ID:CA05956-13 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 12:20 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 12:46Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/11/17 11:42Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 11:42Barium [7440-39-3] ^1.00 JMV10.079.2 J 1001
ug/L EPA 6010D 05/11/17 11:42Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/11/17 11:42Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 11:42Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/11/17 11:42Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 05/11/17 11:42Copper [7440-50-8] ^1.60 JMV10.01.89 J 101
ug/L EPA 6010D 05/11/17 11:42Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/11/17 11:42Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/22/17 12:46Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/11/17 11:42Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 12:46Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/11/17 11:42Vanadium [7440-62-2] ^1.40 JMV10.02.21 J 251
ug/L EPA 6010D 05/11/17 11:42Zinc [7440-66-6] ^4.40 JMV10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-MW17Description:Lab Sample ID:CA05956-14 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 12:45 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 18:311,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/12/17 18:311,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/12/17 18:311,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/12/17 18:311,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 18:311,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/12/17 18:311,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 18:311,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 18:311,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/12/17 18:311,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/12/17 18:311,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/12/17 18:311,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/12/17 18:311,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/12/17 18:311,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/12/17 18:312-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/12/17 18:312-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/12/17 18:314-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/12/17 18:31Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/12/17 18:31Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/12/17 18:31Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 18:31Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/12/17 18:31Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 18:31Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/12/17 18:31Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/12/17 18:31Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/12/17 18:31Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 18:31Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 18:31Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/12/17 18:31Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/12/17 18:31Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 18:31cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/12/17 18:31cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/12/17 18:31Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 18:31Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/12/17 18:31Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 18:31Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/12/17 18:31m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/12/17 18:31Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 18:31o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/12/17 18:31Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/12/17 18:31Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 18:31Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 18:31trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 18:31trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 18:31trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/12/17 18:31Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 18:31Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/12/17 18:31Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/12/17 18:31Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/12/17 18:31Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-MW17Description:Lab Sample ID:CA05956-14 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 12:45 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136100 %MRKEPA 8260B 05/12/17 18:317E120215050.0 1
Dibromofluoromethane 67-129111 %MRKEPA 8260B 05/12/17 18:317E120215650.0 1
Toluene-d8 59-134106 %MRKEPA 8260B 05/12/17 18:317E120215350.0 1
Page 50 of 87
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4104-MW17Description:Lab Sample ID:CA05956-14 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 12:45 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 12:50Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/11/17 11:45Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 11:45Barium [7440-39-3] ^1.00 JMV10.087.7 J 1001
ug/L EPA 6010D 05/11/17 11:45Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/11/17 11:45Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 11:45Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/11/17 11:45Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 05/11/17 11:45Copper [7440-50-8] ^1.60 JMV10.01.86 J 101
ug/L EPA 6010D 05/11/17 11:45Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/11/17 11:45Nickel [7440-02-0] ^2.20 JMV10.014.8 J 501
ug/L EPA 6020B 05/22/17 12:50Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/11/17 11:45Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 12:50Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/11/17 11:45Vanadium [7440-62-2] ^1.40 JMV10.03.51 J 251
ug/L EPA 6010D 05/11/17 11:45Zinc [7440-66-6] ^4.40 JMV10.05.43 J 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-SW1Description:Lab Sample ID:CA05956-15 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 09:45 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 19:011,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/12/17 19:011,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/12/17 19:011,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/12/17 19:011,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 19:011,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/12/17 19:011,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 19:011,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 19:011,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/12/17 19:011,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/12/17 19:011,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/12/17 19:011,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/12/17 19:011,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/12/17 19:011,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/12/17 19:012-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/12/17 19:012-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/12/17 19:014-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/12/17 19:01Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/12/17 19:01Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/12/17 19:01Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 19:01Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/12/17 19:01Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 19:01Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/12/17 19:01Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/12/17 19:01Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/12/17 19:01Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 19:01Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 19:01Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/12/17 19:01Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/12/17 19:01Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 19:01cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/12/17 19:01cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/12/17 19:01Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 19:01Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/12/17 19:01Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 19:01Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/12/17 19:01m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/12/17 19:01Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 19:01o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/12/17 19:01Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/12/17 19:01Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 19:01Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 19:01trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 19:01trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 19:01trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/12/17 19:01Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 19:01Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/12/17 19:01Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/12/17 19:01Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/12/17 19:01Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-SW1Description:Lab Sample ID:CA05956-15 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 09:45 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136103 %MRKEPA 8260B 05/12/17 19:017E120215250.0 1
Dibromofluoromethane 67-129108 %MRKEPA 8260B 05/12/17 19:017E120215450.0 1
Toluene-d8 59-134108 %MRKEPA 8260B 05/12/17 19:017E120215450.0 1
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4104-SW1Description:Lab Sample ID:CA05956-15 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 09:45 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 13:06Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/11/17 11:59Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 11:59Barium [7440-39-3] ^1.00 JMV10.068.3 J 1001
ug/L EPA 6010D 05/11/17 11:59Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/11/17 11:59Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 11:59Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/11/17 11:59Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 05/11/17 11:59Copper [7440-50-8] ^1.60 JMV10.03.32 J 101
ug/L EPA 6010D 05/11/17 11:59Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/11/17 11:59Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/22/17 13:06Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/11/17 11:59Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 13:06Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/11/17 11:59Vanadium [7440-62-2] ^1.40 JMV10.03.39 J 251
ug/L EPA 6010D 05/11/17 11:59Zinc [7440-66-6] ^4.40 JMV10.07.93 J 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-SW3Description:Lab Sample ID:CA05956-16 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 08:30 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 19:301,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/12/17 19:301,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/12/17 19:301,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/12/17 19:301,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 19:301,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/12/17 19:301,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 19:301,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 19:301,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/12/17 19:301,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/12/17 19:301,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/12/17 19:301,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/12/17 19:301,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/12/17 19:301,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/12/17 19:302-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/12/17 19:302-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/12/17 19:304-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/12/17 19:30Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/12/17 19:30Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/12/17 19:30Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 19:30Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/12/17 19:30Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 19:30Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/12/17 19:30Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/12/17 19:30Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/12/17 19:30Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 19:30Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 19:30Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/12/17 19:30Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/12/17 19:30Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 19:30cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/12/17 19:30cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/12/17 19:30Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 19:30Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/12/17 19:30Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 19:30Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/12/17 19:30m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/12/17 19:30Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 19:30o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/12/17 19:30Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/12/17 19:30Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 19:30Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 19:30trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 19:30trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 19:30trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/12/17 19:30Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 19:30Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/12/17 19:30Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/12/17 19:30Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/12/17 19:30Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-SW3Description:Lab Sample ID:CA05956-16 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 08:30 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136100 %MRKEPA 8260B 05/12/17 19:307E120215050.0 1
Dibromofluoromethane 67-129112 %MRKEPA 8260B 05/12/17 19:307E120215650.0 1
Toluene-d8 59-134109 %MRKEPA 8260B 05/12/17 19:307E120215450.0 1
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4104-SW3Description:Lab Sample ID:CA05956-16 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 08:30 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 13:09Antimony [7440-36-0] ^0.370 JDH2.000.443 J 61
ug/L EPA 6010D 05/11/17 12:02Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 12:02Barium [7440-39-3] ^1.00 JMV10.088.8 J 1001
ug/L EPA 6010D 05/11/17 12:02Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/11/17 12:02Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 12:02Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/11/17 12:02Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 05/11/17 12:02Copper [7440-50-8] ^1.60 JMV10.02.52 J 101
ug/L EPA 6010D 05/11/17 12:02Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/11/17 12:02Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/22/17 13:09Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/11/17 12:02Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 13:09Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/11/17 12:02Vanadium [7440-62-2] ^1.40 JMV10.01.62 J 251
ug/L EPA 6010D 05/11/17 12:02Zinc [7440-66-6] ^4.40 JMV10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-SW5Description:Lab Sample ID:CA05956-17 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 09:20 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 20:001,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/12/17 20:001,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/12/17 20:001,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/12/17 20:001,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 20:001,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/12/17 20:001,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 20:001,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 20:001,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/12/17 20:001,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/12/17 20:001,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/12/17 20:001,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/12/17 20:001,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/12/17 20:001,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/12/17 20:002-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/12/17 20:002-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/12/17 20:004-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/12/17 20:00Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/12/17 20:00Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/12/17 20:00Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 20:00Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/12/17 20:00Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 20:00Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/12/17 20:00Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/12/17 20:00Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/12/17 20:00Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 20:00Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 20:00Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/12/17 20:00Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/12/17 20:00Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 20:00cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/12/17 20:00cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/12/17 20:00Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 20:00Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/12/17 20:00Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 20:00Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/12/17 20:00m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/12/17 20:00Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 20:00o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/12/17 20:00Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/12/17 20:00Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 20:00Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 20:00trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 20:00trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 20:00trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/12/17 20:00Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 20:00Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/12/17 20:00Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/12/17 20:00Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/12/17 20:00Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-SW5Description:Lab Sample ID:CA05956-17 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 09:20 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136101 %MRKEPA 8260B 05/12/17 20:007E120215050.0 1
Dibromofluoromethane 67-129111 %MRKEPA 8260B 05/12/17 20:007E120215550.0 1
Toluene-d8 59-134103 %MRKEPA 8260B 05/12/17 20:007E120215150.0 1
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4104-SW5Description:Lab Sample ID:CA05956-17 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 09:20 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 13:13Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/11/17 12:04Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 12:04Barium [7440-39-3] ^1.00 JMV10.066.4 J 1001
ug/L EPA 6010D 05/11/17 12:04Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/11/17 12:04Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 12:04Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/11/17 12:04Cobalt [7440-48-4] ^1.10 JMV10.01.10 U 101
ug/L EPA 6010D 05/11/17 12:04Copper [7440-50-8] ^1.60 JMV10.03.03 J 101
ug/L EPA 6010D 05/11/17 12:04Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/11/17 12:04Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/22/17 13:13Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/11/17 12:04Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 13:13Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/11/17 12:04Vanadium [7440-62-2] ^1.40 JMV10.04.21 J 251
ug/L EPA 6010D 05/11/17 12:04Zinc [7440-66-6] ^4.40 JMV10.06.35 J 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-SW6Description:Lab Sample ID:CA05956-18 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 12:00 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 20:301,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/12/17 20:301,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/12/17 20:301,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/12/17 20:301,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 20:301,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/12/17 20:301,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 20:301,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 20:301,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/12/17 20:301,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/12/17 20:301,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/12/17 20:301,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/12/17 20:301,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/12/17 20:301,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/12/17 20:302-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/12/17 20:302-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/12/17 20:304-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/12/17 20:30Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/12/17 20:30Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/12/17 20:30Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 20:30Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/12/17 20:30Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 20:30Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/12/17 20:30Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/12/17 20:30Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/12/17 20:30Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 20:30Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 20:30Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/12/17 20:30Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/12/17 20:30Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 20:30cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/12/17 20:30cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/12/17 20:30Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 20:30Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/12/17 20:30Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 20:30Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/12/17 20:30m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/12/17 20:30Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 20:30o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/12/17 20:30Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/12/17 20:30Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 20:30Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 20:30trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 20:30trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 20:30trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/12/17 20:30Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 20:30Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/12/17 20:30Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/12/17 20:30Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/12/17 20:30Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-SW6Description:Lab Sample ID:CA05956-18 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 12:00 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136102 %MRKEPA 8260B 05/12/17 20:307E120215150.0 1
Dibromofluoromethane 67-129109 %MRKEPA 8260B 05/12/17 20:307E120215450.0 1
Toluene-d8 59-134109 %MRKEPA 8260B 05/12/17 20:307E120215550.0 1
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4104-SW6Description:Lab Sample ID:CA05956-18 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 12:00 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 13:17Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/11/17 12:07Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 12:07Barium [7440-39-3] ^1.00 JMV10.055.7 J 1001
ug/L EPA 6010D 05/11/17 12:07Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/11/17 12:07Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 12:07Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/11/17 12:07Cobalt [7440-48-4] ^1.10 JMV10.01.29 J 101
ug/L EPA 6010D 05/11/17 12:07Copper [7440-50-8] ^1.60 JMV10.02.82 J 101
ug/L EPA 6010D 05/11/17 12:07Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/11/17 12:07Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/22/17 13:17Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/11/17 12:07Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 13:17Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/11/17 12:07Vanadium [7440-62-2] ^1.40 JMV10.01.49 J 251
ug/L EPA 6010D 05/11/17 12:07Zinc [7440-66-6] ^4.40 JMV10.012.4 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-SW7Description:Lab Sample ID:CA05956-19 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 12:35 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 21:001,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/12/17 21:001,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/12/17 21:001,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/12/17 21:001,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 21:001,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/12/17 21:001,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 21:001,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 21:001,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/12/17 21:001,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/12/17 21:001,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/12/17 21:001,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/12/17 21:001,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/12/17 21:001,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/12/17 21:002-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/12/17 21:002-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/12/17 21:004-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/12/17 21:00Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/12/17 21:00Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/12/17 21:00Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 21:00Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/12/17 21:00Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 21:00Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/12/17 21:00Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/12/17 21:00Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/12/17 21:00Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 21:00Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 21:00Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/12/17 21:00Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/12/17 21:00Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 21:00cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/12/17 21:00cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/12/17 21:00Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 21:00Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/12/17 21:00Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 21:00Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/12/17 21:00m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/12/17 21:00Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 21:00o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/12/17 21:00Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/12/17 21:00Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 21:00Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 21:00trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 21:00trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 21:00trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/12/17 21:00Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 21:00Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/12/17 21:00Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/12/17 21:00Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/12/17 21:00Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-SW7Description:Lab Sample ID:CA05956-19 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 12:35 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136102 %MRKEPA 8260B 05/12/17 21:007E120215150.0 1
Dibromofluoromethane 67-129111 %MRKEPA 8260B 05/12/17 21:007E120215550.0 1
Toluene-d8 59-134107 %MRKEPA 8260B 05/12/17 21:007E120215450.0 1
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4104-SW7Description:Lab Sample ID:CA05956-19 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 12:35 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 13:20Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/11/17 12:09Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 12:09Barium [7440-39-3] ^1.00 JMV10.053.5 J 1001
ug/L EPA 6010D 05/11/17 12:09Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/11/17 12:09Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 12:09Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/11/17 12:09Cobalt [7440-48-4] ^1.10 JMV10.01.63 J 101
ug/L EPA 6010D 05/11/17 12:09Copper [7440-50-8] ^1.60 JMV10.01.79 J 101
ug/L EPA 6010D 05/11/17 12:09Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/11/17 12:09Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/22/17 13:20Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/11/17 12:09Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 13:20Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/11/17 12:09Vanadium [7440-62-2] ^1.40 JMV10.01.40 U 251
ug/L EPA 6010D 05/11/17 12:09Zinc [7440-66-6] ^4.40 JMV10.06.65 J 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-SW8Description:Lab Sample ID:CA05956-20 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 13:00 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 21:291,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/12/17 21:291,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/12/17 21:291,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/12/17 21:291,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 21:291,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/12/17 21:291,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 21:291,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 21:291,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/12/17 21:291,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/12/17 21:291,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/12/17 21:291,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/12/17 21:291,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/12/17 21:291,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/12/17 21:292-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/12/17 21:292-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/12/17 21:294-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/12/17 21:29Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/12/17 21:29Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/12/17 21:29Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 21:29Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/12/17 21:29Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 21:29Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/12/17 21:29Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/12/17 21:29Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/12/17 21:29Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 21:29Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 21:29Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/12/17 21:29Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/12/17 21:29Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 21:29cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/12/17 21:29cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/12/17 21:29Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 21:29Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/12/17 21:29Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 21:29Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/12/17 21:29m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/12/17 21:29Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 21:29o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/12/17 21:29Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/12/17 21:29Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 21:29Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 21:29trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 21:29trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 21:29trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/12/17 21:29Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 21:29Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/12/17 21:29Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/12/17 21:29Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/12/17 21:29Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-SW8Description:Lab Sample ID:CA05956-20 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 13:00 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136102 %MRKEPA 8260B 05/12/17 21:297E120215150.0 1
Dibromofluoromethane 67-129104 %MRKEPA 8260B 05/12/17 21:297E120215250.0 1
Toluene-d8 59-134107 %MRKEPA 8260B 05/12/17 21:297E120215450.0 1
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4104-SW8Description:Lab Sample ID:CA05956-20 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 13:00 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 13:24Antimony [7440-36-0] ^0.370 JDH2.000.370 J 61
ug/L EPA 6010D 05/11/17 12:12Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/11/17 12:12Barium [7440-39-3] ^1.00 JMV10.083.5 J 1001
ug/L EPA 6010D 05/11/17 12:12Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/11/17 12:12Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/11/17 12:12Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/11/17 12:12Cobalt [7440-48-4] ^1.10 JMV10.01.26 J 101
ug/L EPA 6010D 05/11/17 12:12Copper [7440-50-8] ^1.60 JMV10.03.01 J 101
ug/L EPA 6010D 05/11/17 12:12Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/11/17 12:12Nickel [7440-02-0] ^2.20 JMV10.02.39 J 501
ug/L EPA 6020B 05/22/17 13:24Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/11/17 12:12Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 13:24Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/11/17 12:12Vanadium [7440-62-2] ^1.40 JMV10.02.56 J 251
ug/L EPA 6010D 05/11/17 12:12Zinc [7440-66-6] ^4.40 JMV10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-SW10Description:Lab Sample ID:CA05956-21 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 13:15 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/12/17 21:591,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/12/17 21:591,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/12/17 21:591,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/12/17 21:591,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 21:591,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/12/17 21:591,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 21:591,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 21:591,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/12/17 21:591,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/12/17 21:591,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/12/17 21:591,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/12/17 21:591,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/12/17 21:591,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/12/17 21:592-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/12/17 21:592-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/12/17 21:594-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/12/17 21:59Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/12/17 21:59Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/12/17 21:59Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 21:59Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/12/17 21:59Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 21:59Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/12/17 21:59Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/12/17 21:59Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/12/17 21:59Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 21:59Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 21:59Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/12/17 21:59Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/12/17 21:59Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 21:59cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/12/17 21:59cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/12/17 21:59Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/12/17 21:59Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/12/17 21:59Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/12/17 21:59Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/12/17 21:59m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/12/17 21:59Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/12/17 21:59o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/12/17 21:59Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/12/17 21:59Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/12/17 21:59Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/12/17 21:59trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/12/17 21:59trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 21:59trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/12/17 21:59Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/12/17 21:59Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/12/17 21:59Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/12/17 21:59Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/12/17 21:59Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-SW10Description:Lab Sample ID:CA05956-21 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 13:15 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-136102 %MRKEPA 8260B 05/12/17 21:597E120215150.0 1
Dibromofluoromethane 67-129110 %MRKEPA 8260B 05/12/17 21:597E120215550.0 1
Toluene-d8 59-134108 %MRKEPA 8260B 05/12/17 21:597E120215450.0 1
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4104-SW10Description:Lab Sample ID:CA05956-21 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 13:15 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 13:27Antimony [7440-36-0] ^0.370 JDH2.000.370 U 61
ug/L EPA 6010D 05/12/17 10:59Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/12/17 10:59Barium [7440-39-3] ^1.00 JMV10.0219 1001
ug/L EPA 6010D 05/12/17 10:59Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/12/17 10:59Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/12/17 10:59Chromium [7440-47-3] ^1.40 JMV10.01.40 U 101
ug/L EPA 6010D 05/12/17 10:59Cobalt [7440-48-4] ^1.10 JMV10.07.31 J 101
ug/L EPA 6010D 05/12/17 10:59Copper [7440-50-8] ^1.60 JMV10.01.60 U 101
ug/L EPA 6010D 05/12/17 10:59Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/12/17 10:59Nickel [7440-02-0] ^2.20 JMV10.02.20 U 501
ug/L EPA 6020B 05/22/17 13:27Selenium [7782-49-2] ^0.910 JDH3.000.910 U 101
ug/L EPA 6010D 05/12/17 10:59Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 13:27Thallium [7440-28-0] ^0.110 JDH1.000.110 U 5.51
ug/L EPA 6010D 05/12/17 10:59Vanadium [7440-62-2] ^1.40 JMV10.02.63 J 251
ug/L EPA 6010D 05/12/17 10:59Zinc [7440-66-6] ^4.40 JMV10.04.40 U 101
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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4104-TripblankDescription:Lab Sample ID:CA05956-22 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 08:00 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/11/17 19:361,1,1,2-Tetrachloroethane [630-20-6] ^0.17 MRK1.00.17 U 51
ug/L EPA 8260B 05/11/17 19:361,1,1-Trichloroethane [71-55-6] ^0.12 MRK1.00.12 U 11
ug/L EPA 8260B 05/11/17 19:361,1,2,2-Tetrachloroethane [79-34-5] ^0.28 MRK1.00.28 U 31
ug/L EPA 8260B 05/11/17 19:361,1,2-Trichloroethane [79-00-5] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/11/17 19:361,1-Dichloroethane [75-34-3] ^0.13 MRK1.00.13 U 51
ug/L EPA 8260B 05/11/17 19:361,1-Dichloroethene [75-35-4] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/11/17 19:361,2,3-Trichloropropane [96-18-4] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/11/17 19:361,2-Dibromo-3-chloropropane [96-12-8] ^0.48 MRK1.00.48 U 131
ug/L EPA 8260B 05/11/17 19:361,2-Dibromoethane [106-93-4] ^0.66 MRK1.00.66 U 11
ug/L EPA 8260B 05/11/17 19:361,2-Dichlorobenzene [95-50-1] ^0.19 MRK1.00.19 U 51
ug/L EPA 8260B 05/11/17 19:361,2-Dichloroethane [107-06-2] ^0.21 MRK1.00.21 U 11
ug/L EPA 8260B 05/11/17 19:361,2-Dichloropropane [78-87-5] ^0.10 MRK1.00.10 U 11
ug/L EPA 8260B 05/11/17 19:361,4-Dichlorobenzene [106-46-7] ^0.19 MRK1.00.19 U 11
ug/L EPA 8260B 05/11/17 19:362-Butanone [78-93-3] ^1.3 MRK5.01.3 U 1001
ug/L EPA 8260B 05/11/17 19:362-Hexanone [591-78-6] ^0.88 MRK5.00.88 U 501
ug/L EPA 8260B 05/11/17 19:364-Methyl-2-pentanone [108-10-1] ^1.1 MRK5.01.1 U 1001
ug/L EPA 8260B 05/11/17 19:36Acetone [67-64-1] ^10 MRK2010U 1001
ug/L EPA 8260B 05/11/17 19:36Acrylonitrile [107-13-1] ^3.5 MRK103.5 U 2001
ug/L EPA 8260B 05/11/17 19:36Benzene [71-43-2] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/11/17 19:36Bromochloromethane [74-97-5] ^0.48 MRK1.00.48 U 31
ug/L EPA 8260B 05/11/17 19:36Bromodichloromethane [75-27-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/11/17 19:36Bromoform [75-25-2] ^0.22 MRK1.00.22 U 31
ug/L EPA 8260B 05/11/17 19:36Bromomethane [74-83-9] ^0.14 MRK1.00.14 U 101
ug/L EPA 8260B 05/11/17 19:36Carbon disulfide [75-15-0] ^1.5 MRK5.01.5 U 1001
ug/L EPA 8260B 05/11/17 19:36Carbon tetrachloride [56-23-5] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/11/17 19:36Chlorobenzene [108-90-7] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/11/17 19:36Chloroethane [75-00-3] ^0.23 MRK1.00.23 U 101
ug/L EPA 8260B 05/11/17 19:36Chloroform [67-66-3] ^0.18 MRK1.00.18 U 51
ug/L EPA 8260B 05/11/17 19:36Chloromethane [74-87-3] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/11/17 19:36cis-1,2-Dichloroethene [156-59-2] ^0.15 MRK1.00.15 U 51
ug/L EPA 8260B 05/11/17 19:36cis-1,3-Dichloropropene [10061-01-5] ^0.20 MRK1.00.20 U 11
ug/L EPA 8260B 05/11/17 19:36Dibromochloromethane [124-48-1] ^0.17 MRK1.00.17 U 31
ug/L EPA 8260B 05/11/17 19:36Dibromomethane [74-95-3] ^0.27 MRK1.00.27 U 101
ug/L EPA 8260B 05/11/17 19:36Ethylbenzene [100-41-4] ^0.13 MRK1.00.13 U 11
ug/L EPA 8260B 05/11/17 19:36Iodomethane [74-88-4] ^1.7 MRK5.01.7 U 101
ug/L EPA 8260B 05/11/17 19:36m,p-Xylenes [108-38-3/106-42-3] ^0.17 MRK2.00.17 U NE1
ug/L EPA 8260B 05/11/17 19:36Methylene chloride [75-09-2] ^0.23 MRK1.00.23 U 11
ug/L EPA 8260B 05/11/17 19:36o-Xylene [95-47-6] ^0.065 MRK1.00.065 U NE1
ug/L EPA 8260B 05/11/17 19:36Styrene [100-42-5] ^0.11 MRK1.00.11 U 11
ug/L EPA 8260B 05/11/17 19:36Tetrachloroethene [127-18-4] ^0.17 MRK1.00.17 U 11
ug/L EPA 8260B 05/11/17 19:36Toluene [108-88-3] ^0.14 MRK1.00.14 U 11
ug/L EPA 8260B 05/11/17 19:36trans-1,2-Dichloroethene [156-60-5] ^0.21 MRK1.00.21 U 51
ug/L EPA 8260B 05/11/17 19:36trans-1,3-Dichloropropene [10061-02-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/11/17 19:36trans-1,4-Dichloro-2-butene [110-57-6] ^0.70 MRK1.00.70 U 1001
ug/L EPA 8260B 05/11/17 19:36Trichloroethene [79-01-6] ^0.15 MRK1.00.15 U 11
ug/L EPA 8260B 05/11/17 19:36Trichlorofluoromethane [75-69-4] ^0.24 MRK1.00.24 U 11
ug/L EPA 8260B 05/11/17 19:36Vinyl acetate [108-05-4] ^0.95 MRK5.00.95 U 501
ug/L EPA 8260B 05/11/17 19:36Vinyl chloride [75-01-4] ^0.32 MRK1.00.32 U 11
ug/L EPA 8260B 05/11/17 19:36Xylenes (Total) [1330-20-7] ^0.45 MRK3.00.45 U 51
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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4104-TripblankDescription:Lab Sample ID:CA05956-22 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 08:00 Work Order:CA05956
Kersey Valley LandfillProject:Sampled By:ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13692 %MRKEPA 8260B 05/11/17 19:367E110254650.0 1
Dibromofluoromethane 67-12988 %MRKEPA 8260B 05/11/17 19:367E110254450.0 1
Toluene-d8 59-13494 %MRKEPA 8260B 05/11/17 19:367E110254750.0 1
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E11025 - EPA 5030B_MS
Prepared: 05/11/2017 14:59 Analyzed: 05/11/2017 19:06Blank (7E11025-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L2010U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.065 U o-Xylene
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E11025 - EPA 5030B_MS
Prepared: 05/11/2017 14:59 Analyzed: 05/11/2017 19:06Blank (7E11025-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9346
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 8643
ug/L 50.0 59-134Surrogate: Toluene-d8 9447
Prepared: 05/11/2017 14:59 Analyzed: 05/11/2017 17:05LCS (7E11025-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1338818 1,1-Dichloroethene
ug/L1.0 20.0 81-13410621 Benzene
ug/L1.0 20.0 83-11710421 Chlorobenzene
ug/L1.0 20.0 71-11811423 Toluene
ug/L1.0 20.0 74-11910220 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9447
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 8744
ug/L 50.0 59-134Surrogate: Toluene-d8 9548
Prepared: 05/11/2017 14:59 Analyzed: 05/11/2017 17:36Matrix Spike (7E11025-MS1)
Source: CA07191-03
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-133960.21 U19 1,1-Dichloroethene
ug/L1.0 20.0 81-1341120.15 U22 Benzene
ug/L1.0 20.0 83-1171060.17 U21 Chlorobenzene
ug/L1.0 20.0 71-1181200.14 U24 QM-07Toluene
ug/L1.0 20.0 74-1191060.15 U21 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9447
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 8643
ug/L 50.0 59-134Surrogate: Toluene-d8 9648
Prepared: 05/11/2017 14:59 Analyzed: 05/11/2017 18:06Matrix Spike Dup (7E11025-MSD1)
Source: CA07191-03
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-13390 70.21 U18 1,1-Dichloroethene
ug/L1.0 20.0 1781-134106 60.15 U21 Benzene
ug/L1.0 20.0 1683-117102 40.17 U20 Chlorobenzene
ug/L1.0 20.0 1771-118113 60.14 U23 Toluene
ug/L1.0 20.0 2274-11999 70.15 U20 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9447
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 8744
ug/L 50.0 59-134Surrogate: Toluene-d8 9548
Batch 7E12021 - EPA 5030B_MS
Prepared: 05/12/2017 12:21 Analyzed: 05/12/2017 16:03Blank (7E12021-BLK1)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E12021 - EPA 5030B_MS
Prepared: 05/12/2017 12:21 Analyzed: 05/12/2017 16:03Blank (7E12021-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L2010U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.065 U o-Xylene
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E12021 - EPA 5030B_MS
Prepared: 05/12/2017 12:21 Analyzed: 05/12/2017 16:03Blank (7E12021-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 10151
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 10854
ug/L 50.0 59-134Surrogate: Toluene-d8 10653
Prepared: 05/12/2017 12:21 Analyzed: 05/12/2017 14:01LCS (7E12021-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-13311122 1,1-Dichloroethene
ug/L1.0 20.0 81-13411723 Benzene
ug/L1.0 20.0 83-11710120 Chlorobenzene
ug/L1.0 20.0 71-11810822 Toluene
ug/L1.0 20.0 74-11910220 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 10050
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 11155
ug/L 50.0 59-134Surrogate: Toluene-d8 10653
Prepared: 05/12/2017 12:21 Analyzed: 05/12/2017 14:32Matrix Spike (7E12021-MS1)
Source: CA07191-06
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1331160.21 U23 1,1-Dichloroethene
ug/L1.0 20.0 81-1341220.15 U24 Benzene
ug/L1.0 20.0 83-1171020.17 U20 Chlorobenzene
ug/L1.0 20.0 71-1181130.14 U23 Toluene
ug/L1.0 20.0 74-1191080.15 U22 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 10151
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 11256
ug/L 50.0 59-134Surrogate: Toluene-d8 10653
Prepared: 05/12/2017 12:21 Analyzed: 05/12/2017 15:02Matrix Spike Dup (7E12021-MSD1)
Source: CA07191-06
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-133108 70.21 U22 1,1-Dichloroethene
ug/L1.0 20.0 1781-134116 60.15 U23 Benzene
ug/L1.0 20.0 1683-11798 40.17 U20 Chlorobenzene
ug/L1.0 20.0 1771-118108 50.14 U22 Toluene
ug/L1.0 20.0 2274-119102 60.15 U20 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 10151
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 11256
ug/L 50.0 59-134Surrogate: Toluene-d8 10753
Batch 7E12022 - EPA 5030B_MS
Prepared: 05/12/2017 12:23 Analyzed: 05/12/2017 16:37Blank (7E12022-BLK1)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E12022 - EPA 5030B_MS
Prepared: 05/12/2017 12:23 Analyzed: 05/12/2017 16:37Blank (7E12022-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L2010U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.065 U o-Xylene
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E12022 - EPA 5030B_MS
Prepared: 05/12/2017 12:23 Analyzed: 05/12/2017 16:37Blank (7E12022-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9146
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 8543
ug/L 50.0 59-134Surrogate: Toluene-d8 9246
Prepared: 05/12/2017 12:23 Analyzed: 05/12/2017 14:06LCS (7E12022-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1338317 1,1-Dichloroethene
ug/L1.0 20.0 81-1349820 Benzene
ug/L1.0 20.0 83-1179519 Chlorobenzene
ug/L1.0 20.0 71-11810521 Toluene
ug/L1.0 20.0 74-1199319 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9347
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 8442
ug/L 50.0 59-134Surrogate: Toluene-d8 9447
Prepared: 05/12/2017 12:23 Analyzed: 05/12/2017 14:37Matrix Spike (7E12022-MS1)
Source: CA07191-09
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-133940.21 U19 1,1-Dichloroethene
ug/L1.0 20.0 81-1341050.15 U21 Benzene
ug/L1.0 20.0 83-1171010.17 U20 Chlorobenzene
ug/L1.0 20.0 71-1181140.14 U23 Toluene
ug/L1.0 20.0 74-1191010.15 U20 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9246
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 8543
ug/L 50.0 59-134Surrogate: Toluene-d8 9246
Prepared: 05/12/2017 12:23 Analyzed: 05/12/2017 15:37Matrix Spike Dup (7E12022-MSD1)
Source: CA07191-09
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-13384 120.21 U17 1,1-Dichloroethene
ug/L1.0 20.0 1781-13497 80.15 U19 Benzene
ug/L1.0 20.0 1683-11797 50.17 U19 Chlorobenzene
ug/L1.0 20.0 1771-118105 80.14 U21 Toluene
ug/L1.0 20.0 2274-11994 70.15 U19 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9347
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 8542
ug/L 50.0 59-134Surrogate: Toluene-d8 9246
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7E09019 - EPA 3005A
Prepared: 05/09/2017 13:33 Analyzed: 05/11/2017 10:46Blank (7E09019-BLK1)
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7E09019 - EPA 3005A
Prepared: 05/09/2017 13:33 Analyzed: 05/11/2017 10:46Blank (7E09019-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.06.80 U Arsenic
ug/L10.01.00 U Barium
ug/L1.000.130 U Beryllium
ug/L1.000.360 U Cadmium
ug/L10.01.40 U Chromium
ug/L10.01.10 U Cobalt
ug/L10.01.60 U Copper
ug/L10.03.10 U Lead
ug/L10.02.21 J Nickel
ug/L10.01.90 U Silver
ug/L10.01.40 U Vanadium
ug/L10.04.40 U Zinc
Prepared: 05/09/2017 13:33 Analyzed: 05/11/2017 10:49LCS (7E09019-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 80-12096192 Arsenic
ug/L10.0 200 80-12099198 Barium
ug/L1.00 20.0 80-1209919.8 Beryllium
ug/L1.00 20.0 80-12010220.4 Cadmium
ug/L10.0 200 80-12098195 Chromium
ug/L10.0 200 80-120102204 Cobalt
ug/L10.0 200 80-12096193 Copper
ug/L10.0 200 80-120101201 Lead
ug/L10.0 200 80-12099199 Nickel
ug/L10.0 200 80-12098195 Silver
ug/L10.0 200 80-12095191 Vanadium
ug/L10.0 200 80-120101203 Zinc
Prepared: 05/09/2017 13:33 Analyzed: 05/11/2017 10:54Matrix Spike (7E09019-MS1)
Source: CA05956-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 75-125966.80 U192 Arsenic
ug/L10.0 200 75-1259988.6287 Barium
ug/L1.00 20.0 75-1251010.56120.8 Beryllium
ug/L1.00 20.0 75-1251050.360 U20.9 Cadmium
ug/L10.0 200 75-125992.73201 Chromium
ug/L10.0 200 75-1251044.75212 Cobalt
ug/L10.0 200 75-125973.99198 Copper
ug/L10.0 200 75-1251043.10 U208 Lead
ug/L10.0 200 75-1259910.9209 Nickel
ug/L10.0 200 75-125971.90 U195 Silver
ug/L10.0 200 75-125971.40 U195 Vanadium
ug/L10.0 200 75-12510444.9252 Zinc
Prepared: 05/09/2017 13:33 Analyzed: 05/11/2017 10:56Matrix Spike Dup (7E09019-MSD1)
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7E09019 - EPA 3005A
Prepared: 05/09/2017 13:33 Analyzed: 05/11/2017 10:56Matrix Spike Dup (7E09019-MSD1) Continued
Source: CA05956-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 2075-12594 26.80 U189 Arsenic
ug/L10.0 200 2075-12595 388.6279 Barium
ug/L1.00 20.0 2075-12596 50.56119.8 Beryllium
ug/L1.00 20.0 2075-125101 30.360 U20.2 Cadmium
ug/L10.0 200 2075-12594 52.73192 Chromium
ug/L10.0 200 2075-125101 34.75206 Cobalt
ug/L10.0 200 2075-12594 43.99191 Copper
ug/L10.0 200 2075-12599 53.10 U198 Lead
ug/L10.0 200 2075-12594 510.9199 Nickel
ug/L10.0 200 2075-12593 41.90 U186 Silver
ug/L10.0 200 2075-12593 41.40 U186 Vanadium
ug/L10.0 200 2075-125100 244.9246 Zinc
Prepared: 05/09/2017 13:33 Analyzed: 05/11/2017 10:58Post Spike (7E09019-PS1)
Source: CA05956-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.0100 0.200 80-120940.0002030.188 Arsenic
mg/L0.0100 0.200 80-120970.08860.283 Barium
mg/L0.00100 0.0200 80-120990.0005610.0203 Beryllium
mg/L0.00100 0.0200 80-1201015.59E-50.0203 Cadmium
mg/L0.0100 0.200 80-120970.002730.197 Chromium
mg/L0.0100 0.200 80-1201010.004750.206 Cobalt
mg/L0.0100 0.200 80-120950.003990.194 Copper
mg/L0.0100 0.200 80-120990.0007190.199 Lead
mg/L0.0100 0.200 80-120980.01090.207 Nickel
mg/L0.0100 0.200 80-12095-0.001100.190 Silver
mg/L0.0100 0.200 80-120950.001310.192 Vanadium
mg/L0.0100 0.200 80-120970.04490.239 Zinc
Batch 7E09020 - EPA 3005A
Prepared: 05/09/2017 13:37 Analyzed: 05/12/2017 10:53Blank (7E09020-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.06.80 U Arsenic
ug/L10.01.00 U Barium
ug/L1.000.130 U Beryllium
ug/L1.000.360 U Cadmium
ug/L10.01.40 U Chromium
ug/L10.01.10 U Cobalt
ug/L10.01.60 U Copper
ug/L10.03.10 U Lead
ug/L10.02.20 U Nickel
ug/L10.01.90 U Silver
ug/L10.01.40 U Vanadium
ug/L10.04.40 U Zinc
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7E09020 - EPA 3005A
Prepared: 05/09/2017 13:37 Analyzed: 05/12/2017 10:56LCS (7E09020-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 80-12096192 Arsenic
ug/L10.0 200 80-12097194 Barium
ug/L1.00 20.0 80-1209619.1 Beryllium
ug/L1.00 20.0 80-12010020.1 Cadmium
ug/L10.0 200 80-12094189 Chromium
ug/L10.0 200 80-12099197 Cobalt
ug/L10.0 200 80-12094188 Copper
ug/L10.0 200 80-12099197 Lead
ug/L10.0 200 80-12096192 Nickel
ug/L10.0 200 80-12094188 Silver
ug/L10.0 200 80-12092184 Vanadium
ug/L10.0 200 80-120101203 Zinc
Prepared: 05/09/2017 13:37 Analyzed: 05/12/2017 11:01Matrix Spike (7E09020-MS1)
Source: CA05956-21
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 75-125946.80 U187 Arsenic
ug/L10.0 200 75-12588219395 Barium
ug/L1.00 20.0 75-125950.130 U19.0 Beryllium
ug/L1.00 20.0 75-125890.360 U17.8 Cadmium
ug/L10.0 200 75-125921.40 U185 Chromium
ug/L10.0 200 75-125927.31191 Cobalt
ug/L10.0 200 75-125941.60 U189 Copper
ug/L10.0 200 75-125923.10 U185 Lead
ug/L10.0 200 75-125912.20 U183 Nickel
ug/L10.0 200 75-125941.90 U188 Silver
ug/L10.0 200 75-125922.63187 Vanadium
ug/L10.0 200 75-125954.40 U189 Zinc
Prepared: 05/09/2017 13:37 Analyzed: 05/12/2017 11:06Matrix Spike Dup (7E09020-MSD1)
Source: CA05956-21
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 2075-125102 86.80 U203 Arsenic
ug/L10.0 200 2075-125105 8219429 Barium
ug/L1.00 20.0 2075-125104 90.130 U20.9 Beryllium
ug/L1.00 20.0 2075-12596 80.360 U19.1 Cadmium
ug/L10.0 200 2075-125101 91.40 U203 Chromium
ug/L10.0 200 2075-125101 97.31209 Cobalt
ug/L10.0 200 2075-125104 91.60 U207 Copper
ug/L10.0 200 2075-125102 103.10 U204 Lead
ug/L10.0 200 2075-125101 92.20 U201 Nickel
ug/L10.0 200 2075-125102 91.90 U205 Silver
ug/L10.0 200 2075-125101 102.63206 Vanadium
ug/L10.0 200 2075-125104 94.40 U208 Zinc
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7E09020 - EPA 3005A
Prepared: 05/09/2017 13:37 Analyzed: 05/12/2017 11:09Post Spike (7E09020-PS1)
Source: CA05956-21
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.0100 0.200 80-120990.001340.198 Arsenic
mg/L0.0100 0.200 80-120990.2190.416 Barium
mg/L0.00100 0.0200 80-120102-7.01E-50.0203 Beryllium
mg/L0.00100 0.0200 80-12095-0.0005380.0191 Cadmium
mg/L0.0100 0.200 80-12099-0.0002000.198 Chromium
mg/L0.0100 0.200 80-120990.007310.205 Cobalt
mg/L0.0100 0.200 80-120101-0.0009990.201 Copper
mg/L0.0100 0.200 80-120990.0007740.198 Lead
mg/L0.0100 0.200 80-12098-0.0004390.196 Nickel
mg/L0.0100 0.200 80-120100-0.0005070.199 Silver
mg/L0.0100 0.200 80-120980.002630.199 Vanadium
mg/L0.0100 0.200 80-1201010.0008490.204 Zinc
Batch 7E09021 - EPA 3005A
Prepared: 05/09/2017 13:41 Analyzed: 05/17/2017 14:11Blank (7E09021-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.000.370 U Antimony
ug/L3.000.910 U Selenium
ug/L1.000.110 U Thallium
Prepared: 05/09/2017 13:41 Analyzed: 05/17/2017 14:15LCS (7E09021-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-12094187 Antimony
ug/L3.00 200 80-120101201 Selenium
ug/L1.00 200 80-12089178 Thallium
Prepared: 05/09/2017 13:41 Analyzed: 05/17/2017 14:22Matrix Spike (7E09021-MS1)
Source: CA06110-08
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 75-125940.370 U187 Antimony
ug/L3.00 200 75-1251100.910 U220 Selenium
ug/L1.00 200 75-125870.110 U174 Thallium
Prepared: 05/09/2017 13:41 Analyzed: 05/17/2017 14:26Matrix Spike Dup (7E09021-MSD1)
Source: CA06110-08
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 2075-12595 10.370 U190 Antimony
ug/L3.00 200 2075-125109 0.60.910 U218 Selenium
ug/L1.00 200 2075-12588 0.60.110 U175 Thallium
Prepared: 05/09/2017 13:41 Analyzed: 05/17/2017 14:30Post Spike (7E09021-PS1)
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7E09021 - EPA 3005A
Prepared: 05/09/2017 13:41 Analyzed: 05/17/2017 14:30Post Spike (7E09021-PS1) Continued
Source: CA06110-08
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-120980.301196 Antimony
ug/L3.00 200 80-1201130.383227 Selenium
ug/L1.00 200 75-125910.0948182 Thallium
Batch 7E12023 - EPA 3005A
Prepared: 05/12/2017 12:27 Analyzed: 05/22/2017 12:16Blank (7E12023-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.000.370 U Antimony
ug/L3.000.910 U Selenium
ug/L1.000.110 U Thallium
Prepared: 05/12/2017 12:27 Analyzed: 05/22/2017 12:24LCS (7E12023-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-120102205 Antimony
ug/L3.00 200 80-120110220 Selenium
ug/L1.00 200 80-120103205 Thallium
Prepared: 05/12/2017 12:27 Analyzed: 05/22/2017 12:28Matrix Spike (7E12023-MS1)
Source: CA05956-11
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 75-1251040.370 U208 Antimony
ug/L3.00 200 75-1251140.910 U228 Selenium
ug/L1.00 200 75-1251020.110 U205 Thallium
Prepared: 05/12/2017 12:27 Analyzed: 05/22/2017 12:32Matrix Spike Dup (7E12023-MSD1)
Source: CA05956-11
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 2075-125105 10.370 U210 Antimony
ug/L3.00 200 2075-125115 10.910 U231 Selenium
ug/L1.00 200 2075-125104 10.110 U207 Thallium
Prepared: 05/12/2017 12:27 Analyzed: 05/22/2017 12:35Post Spike (7E12023-PS1)
Source: CA05956-11
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-1201040.134209 Antimony
ug/L3.00 200 80-1201090.291218 Selenium
ug/L1.00 200 75-125990.0712199 Thallium
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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was
accepted based on acceptable LCS recovery.
QM-07
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102-A Woodwinds Industrial Court
Cary NC, 27511
919.467.3090 919.467.3515Phone:FAX:www.encolabs.com
Environmental Conservation Laboratories, Inc.
ENCO Workorder(s): CA05957
Raleigh, NC 27606
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Enclosure(s)
Project Number: [none], Project Name/Desc: Kersey Valley Landfill-Leachate
Attn: Gary Babb
Babb & Associates (BA024)
3605 Country Cove Lane
Bill Scott
Project Manager
Tuesday, May 23, 2017
RE: Laboratory Results for
Dear Gary Babb,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Thursday, May 4, 2017.
The total number of pages in this report, including this page is 21.
Page 1 of 22
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SAMPLE SUMMARY/LABORATORY CHRONICLE
4104-LeachateP1-3 CA05957-01 Sampled:05/03/17 13:45 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 300.0 05/31/17 05/16/17 11:06 5/16/2017 16:27
EPA 353.2 05/05/17 13:45 05/05/17 09:35 5/5/2017 09:35
EPA 353.2 05/31/17 05/04/17 14:13 5/4/2017 14:13
EPA 353.2 01/27/20 05/10/17 10:17 5/10/2017 10:27
EPA 365.4 05/31/17 05/05/17 12:30 5/8/2017 13:21
EPA 6010D 10/30/17 05/09/17 13:37 5/12/2017 11:14
EPA 6020B 10/30/17 05/12/17 12:27 5/22/2017 13:31
EPA 8260B 05/17/17 05/15/17 00:59 5/15/2017 21:16
SM 5210B-2001 05/05/17 13:45 05/04/17 14:23 5/4/2017 14:23
SM 5220D-1997 05/31/17 05/04/17 17:30 5/5/2017 09:52
4104-LeachateP4-5 CA05957-02 Sampled:05/03/17 13:25 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 300.0 05/31/17 05/16/17 11:06 5/16/2017 16:41
EPA 353.2 05/05/17 13:25 05/05/17 09:36 5/5/2017 09:36
EPA 353.2 05/31/17 05/04/17 14:16 5/4/2017 14:16
EPA 353.2 01/27/20 05/10/17 10:17 5/10/2017 10:27
EPA 6010D 10/30/17 05/09/17 13:37 5/12/2017 11:25
EPA 6020B 10/30/17 05/12/17 12:27 5/22/2017 13:35
EPA 8260B 05/17/17 05/15/17 00:59 5/15/2017 21:46
SM 5210B-2001 05/05/17 13:25 05/04/17 14:23 5/4/2017 14:23
SM 5220D-1997 05/31/17 05/04/17 17:30 5/5/2017 09:52
4104-LeachateP4-5 CA05957-02RE1 Sampled:05/03/17 13:25 Received:05/04/17 09:30Client ID:Lab ID:
Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)
EPA 365.4 05/31/17 05/05/17 12:30 5/8/2017 14:17
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NORTH CAROLINA SWS SAMPLE DETECTION SUMMARY
Analyte MethodUnitsResults
Lab ID:Client ID:4104-LeachateP1-3 CA05957-01
Flag NotesMDLNC SWSLMRLDF
482 ug/L EPA 6010D 10010.01.001Barium - Total
42000 ug/L SM 5210B-2001 NE200020001Biochemical Oxygen Demand
270000 ug/L SM 5220D-1997 NE10000100001Chemical Oxygen Demand
7.74 ug/L EPA 6010DJ 1010.01.401Chromium - Total
9.56 ug/L EPA 6010DJ 1010.01.101Cobalt - Total
9.10 ug/L EPA 6010DJ 1010.01.601Copper - Total
30.6 ug/L EPA 6010DJ 5010.02.201Nickel - Total
1400 ug/L EPA 353.2J 10000100251Nitrate as N
2800 ug/L EPA 353.2D NE200822Nitrate/Nitrite as N
1400 ug/L EPA 353.2 1000100171Nitrite as N
790 ug/L EPA 365.4 NE100251Phosphorus
7200 ug/L EPA 300.0J 250000500029001Sulfate as SO4
12.9 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
41.3 ug/L EPA 6010D 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-LeachateP4-5 CA05957-02
Flag NotesMDLNC SWSLMRLDF
98 ug/L EPA 8260BJD R-041005013102-Butanone
140 ug/L EPA 8260BJD R-0410020010010Acetone
9.66 ug/L EPA 6010DJ 1010.06.801Arsenic - Total
169 ug/L EPA 6010D 10010.01.001Barium - Total
20000 ug/L SM 5210B-2001 NE200020001Biochemical Oxygen Demand
190000 ug/L SM 5220D-1997 NE10000100001Chemical Oxygen Demand
11.7 ug/L EPA 6010D 1010.01.401Chromium - Total
11.4 ug/L EPA 6010D 1010.01.101Cobalt - Total
3.60 ug/L EPA 6010DJ 1010.01.601Copper - Total
30.8 ug/L EPA 6010DJ 5010.02.201Nickel - Total
100 ug/L EPA 353.2J 10000100251Nitrate as N
120 ug/L EPA 353.2 NE100411Nitrate/Nitrite as N
20 ug/L EPA 353.2J 1000100171Nitrite as N
14000 ug/L EPA 300.0J 250000500029001Sulfate as SO4
16.8 ug/L EPA 6010DJ 2510.01.401Vanadium - Total
9.55 ug/L EPA 6010DJ 1010.04.401Zinc - Total
Analyte MethodUnitsResults
Lab ID:Client ID:4104-LeachateP4-5 CA05957-02RE1
Flag NotesMDLNC SWSLMRLDF
680 ug/L EPA 365.4 NE100251Phosphorus
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ANALYTICAL RESULTS
4104-LeachateP1-3Description:Lab Sample ID:CA05957-01 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 13:45 Work Order:CA05957
Kersey Valley Landfill-LeachateProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/15/17 21:161,1,1,2-Tetrachloroethane [630-20-6] ^1.7 MRK101.7 UD R-04510
ug/L EPA 8260B 05/15/17 21:161,1,1-Trichloroethane [71-55-6] ^1.2 MRK101.2 UD R-04110
ug/L EPA 8260B 05/15/17 21:161,1,2,2-Tetrachloroethane [79-34-5] ^2.8 MRK102.8 UD R-04310
ug/L EPA 8260B 05/15/17 21:161,1,2-Trichloroethane [79-00-5] ^1.4 MRK101.4 UD R-04110
ug/L EPA 8260B 05/15/17 21:161,1-Dichloroethane [75-34-3] ^1.3 MRK101.3 UD R-04510
ug/L EPA 8260B 05/15/17 21:161,1-Dichloroethene [75-35-4] ^2.1 MRK102.1 UD R-04510
ug/L EPA 8260B 05/15/17 21:161,2,3-Trichloropropane [96-18-4] ^2.3 MRK102.3 UD R-04110
ug/L EPA 8260B 05/15/17 21:161,2-Dibromo-3-chloropropane [96-12-8] ^4.8 MRK104.8 UD R-041310
ug/L EPA 8260B 05/15/17 21:161,2-Dibromoethane [106-93-4] ^6.6 MRK106.6 UD R-04110
ug/L EPA 8260B 05/15/17 21:161,2-Dichlorobenzene [95-50-1] ^1.9 MRK101.9 UD R-04510
ug/L EPA 8260B 05/15/17 21:161,2-Dichloroethane [107-06-2] ^2.1 MRK102.1 UD R-04110
ug/L EPA 8260B 05/15/17 21:161,2-Dichloropropane [78-87-5] ^1.0 MRK101.0 UD R-04110
ug/L EPA 8260B 05/15/17 21:161,4-Dichlorobenzene [106-46-7] ^1.9 MRK101.9 UD R-04110
ug/L EPA 8260B 05/15/17 21:162-Butanone [78-93-3] ^13 MRK5013UD R-0410010
ug/L EPA 8260B 05/15/17 21:162-Hexanone [591-78-6] ^8.8 MRK508.8 UD R-045010
ug/L EPA 8260B 05/15/17 21:164-Methyl-2-pentanone [108-10-1] ^11 MRK5011UD R-0410010
ug/L EPA 8260B 05/15/17 21:16Acetone [67-64-1] ^100 MRK200100UD R-0410010
ug/L EPA 8260B 05/15/17 21:16Acrylonitrile [107-13-1] ^35 MRK10035UD R-0420010
ug/L EPA 8260B 05/15/17 21:16Benzene [71-43-2] ^1.5 MRK101.5 UD R-04110
ug/L EPA 8260B 05/15/17 21:16Bromochloromethane [74-97-5] ^4.8 MRK104.8 UD R-04310
ug/L EPA 8260B 05/15/17 21:16Bromodichloromethane [75-27-4] ^1.7 MRK101.7 UD R-04110
ug/L EPA 8260B 05/15/17 21:16Bromoform [75-25-2] ^2.2 MRK102.2 UD R-04310
ug/L EPA 8260B 05/15/17 21:16Bromomethane [74-83-9] ^1.4 MRK101.4 UD R-041010
ug/L EPA 8260B 05/15/17 21:16Carbon disulfide [75-15-0] ^15 MRK5015UD R-0410010
ug/L EPA 8260B 05/15/17 21:16Carbon tetrachloride [56-23-5] ^1.7 MRK101.7 UD R-04110
ug/L EPA 8260B 05/15/17 21:16Chlorobenzene [108-90-7] ^1.7 MRK101.7 UD R-04310
ug/L EPA 8260B 05/15/17 21:16Chloroethane [75-00-3] ^2.3 MRK102.3 UD R-041010
ug/L EPA 8260B 05/15/17 21:16Chloroform [67-66-3] ^1.8 MRK101.8 UD R-04510
ug/L EPA 8260B 05/15/17 21:16Chloromethane [74-87-3] ^1.3 MRK101.3 UD R-04110
ug/L EPA 8260B 05/15/17 21:16cis-1,2-Dichloroethene [156-59-2] ^1.5 MRK101.5 UD R-04510
ug/L EPA 8260B 05/15/17 21:16cis-1,3-Dichloropropene [10061-01-5] ^2.0 MRK102.0 UD R-04110
ug/L EPA 8260B 05/15/17 21:16Dibromochloromethane [124-48-1] ^1.7 MRK101.7 UD R-04310
ug/L EPA 8260B 05/15/17 21:16Dibromomethane [74-95-3] ^2.7 MRK102.7 UD R-041010
ug/L EPA 8260B 05/15/17 21:16Ethylbenzene [100-41-4] ^1.3 MRK101.3 UD R-04110
ug/L EPA 8260B 05/15/17 21:16Iodomethane [74-88-4] ^17 MRK5017UD R-041010
ug/L EPA 8260B 05/15/17 21:16m,p-Xylenes [108-38-3/106-42-3] ^1.7 MRK201.7 UD R-04NE10
ug/L EPA 8260B 05/15/17 21:16Methylene chloride [75-09-2] ^2.3 MRK102.3 UD R-04110
ug/L EPA 8260B 05/15/17 21:16o-Xylene [95-47-6] ^0.65 MRK100.65 UD R-04NE10
ug/L EPA 8260B 05/15/17 21:16Styrene [100-42-5] ^1.1 MRK101.1 UD R-04110
ug/L EPA 8260B 05/15/17 21:16Tetrachloroethene [127-18-4] ^1.7 MRK101.7 UD R-04110
ug/L EPA 8260B 05/15/17 21:16Toluene [108-88-3] ^1.4 MRK101.4 UD R-04110
ug/L EPA 8260B 05/15/17 21:16trans-1,2-Dichloroethene [156-60-5] ^2.1 MRK102.1 UD R-04510
ug/L EPA 8260B 05/15/17 21:16trans-1,3-Dichloropropene [10061-02-6] ^1.5 MRK101.5 UD R-04110
ug/L EPA 8260B 05/15/17 21:16trans-1,4-Dichloro-2-butene [110-57-6] ^7.0 MRK107.0 UD R-0410010
ug/L EPA 8260B 05/15/17 21:16Trichloroethene [79-01-6] ^1.5 MRK101.5 UD R-04110
ug/L EPA 8260B 05/15/17 21:16Trichlorofluoromethane [75-69-4] ^2.4 MRK102.4 UD R-04110
ug/L EPA 8260B 05/15/17 21:16Vinyl acetate [108-05-4] ^9.5 MRK509.5 UD R-045010
ug/L EPA 8260B 05/15/17 21:16Vinyl chloride [75-01-4] ^3.2 MRK103.2 UD R-04110
Page 4 of 21
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www.encolabs.com
4104-LeachateP1-3Description:Lab Sample ID:CA05957-01 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 13:45 Work Order:CA05957
Kersey Valley Landfill-LeachateProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/15/17 21:16Xylenes (Total) [1330-20-7] ^4.5 MRK304.5 UD R-04510
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13691 %MRKEPA 8260B 05/15/17 21:167E120244650.0 R-041
Dibromofluoromethane 67-12998 %MRKEPA 8260B 05/15/17 21:167E120244950.0 R-041
Toluene-d8 59-13497 %MRKEPA 8260B 05/15/17 21:167E120244850.0 R-041
Page 5 of 21
Page 5 of 22
www.encolabs.com
4104-LeachateP1-3Description:Lab Sample ID:CA05957-01 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 13:45 Work Order:CA05957
Kersey Valley Landfill-LeachateProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 13:31Antimony [7440-36-0] ^3.70 JDH20.03.70 UD 610
ug/L EPA 6010D 05/12/17 11:14Arsenic [7440-38-2] ^6.80 JMV10.06.80 U 101
ug/L EPA 6010D 05/12/17 11:14Barium [7440-39-3] ^1.00 JMV10.0482 1001
ug/L EPA 6010D 05/12/17 11:14Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/12/17 11:14Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/12/17 11:14Chromium [7440-47-3] ^1.40 JMV10.07.74 J 101
ug/L EPA 6010D 05/12/17 11:14Cobalt [7440-48-4] ^1.10 JMV10.09.56 J 101
ug/L EPA 6010D 05/12/17 11:14Copper [7440-50-8] ^1.60 JMV10.09.10 J 101
ug/L EPA 6010D 05/12/17 11:14Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/12/17 11:14Nickel [7440-02-0] ^2.20 JMV10.030.6 J 501
ug/L EPA 6020B 05/22/17 13:31Selenium [7782-49-2] ^9.10 JDH30.09.10 UD 1010
ug/L EPA 6010D 05/12/17 11:14Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 13:31Thallium [7440-28-0] ^1.10 JDH10.01.10 UD 5.510
ug/L EPA 6010D 05/12/17 11:14Vanadium [7440-62-2] ^1.40 JMV10.012.9 J 251
ug/L EPA 6010D 05/12/17 11:14Zinc [7440-66-6] ^4.40 JMV10.041.3 101
Page 6 of 21
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www.encolabs.com
4104-LeachateP1-3Description:Lab Sample ID:CA05957-01 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 13:45 Work Order:CA05957
Kersey Valley Landfill-LeachateProject:Sampled By:Travis Queen
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L SM 5210B-2001 05/04/17 14:23Biochemical Oxygen Demand^2000 JOC200042000 NE1
ug/L SM 5220D-1997 05/05/17 09:52Chemical Oxygen Demand^10000 JOC10000270000 NE1
ug/L EPA 353.2 05/10/17 10:27Nitrate as N [14797-55-8] ^25 JLJ1001400J 100001
ug/L EPA 353.2 05/04/17 14:13Nitrate/Nitrite as N^82 JLJ2002800D NE2
ug/L EPA 353.2 05/05/17 09:35Nitrite as N [14797-65-0] ^17 JLJ1001400 10001
ug/L EPA 365.4 05/08/17 13:21Phosphorus [7723-14-0] ^25 JLJ100790 NE1
ug/L EPA 300.0 05/16/17 16:27Sulfate as SO4 [14808-79-8] ^2900 MKS50007200J 2500001
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 7 of 21
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4104-LeachateP4-5Description:Lab Sample ID:CA05957-02 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 13:25 Work Order:CA05957
Kersey Valley Landfill-LeachateProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 8260B 05/15/17 21:461,1,1,2-Tetrachloroethane [630-20-6] ^1.7 MRK101.7 UD R-04510
ug/L EPA 8260B 05/15/17 21:461,1,1-Trichloroethane [71-55-6] ^1.2 MRK101.2 UD R-04110
ug/L EPA 8260B 05/15/17 21:461,1,2,2-Tetrachloroethane [79-34-5] ^2.8 MRK102.8 UD R-04310
ug/L EPA 8260B 05/15/17 21:461,1,2-Trichloroethane [79-00-5] ^1.4 MRK101.4 UD R-04110
ug/L EPA 8260B 05/15/17 21:461,1-Dichloroethane [75-34-3] ^1.3 MRK101.3 UD R-04510
ug/L EPA 8260B 05/15/17 21:461,1-Dichloroethene [75-35-4] ^2.1 MRK102.1 UD R-04510
ug/L EPA 8260B 05/15/17 21:461,2,3-Trichloropropane [96-18-4] ^2.3 MRK102.3 UD R-04110
ug/L EPA 8260B 05/15/17 21:461,2-Dibromo-3-chloropropane [96-12-8] ^4.8 MRK104.8 UD R-041310
ug/L EPA 8260B 05/15/17 21:461,2-Dibromoethane [106-93-4] ^6.6 MRK106.6 UD R-04110
ug/L EPA 8260B 05/15/17 21:461,2-Dichlorobenzene [95-50-1] ^1.9 MRK101.9 UD R-04510
ug/L EPA 8260B 05/15/17 21:461,2-Dichloroethane [107-06-2] ^2.1 MRK102.1 UD R-04110
ug/L EPA 8260B 05/15/17 21:461,2-Dichloropropane [78-87-5] ^1.0 MRK101.0 UD R-04110
ug/L EPA 8260B 05/15/17 21:461,4-Dichlorobenzene [106-46-7] ^1.9 MRK101.9 UD R-04110
ug/L EPA 8260B 05/15/17 21:462-Butanone [78-93-3] ^13 MRK5098JD R-0410010
ug/L EPA 8260B 05/15/17 21:462-Hexanone [591-78-6] ^8.8 MRK508.8 UD R-045010
ug/L EPA 8260B 05/15/17 21:464-Methyl-2-pentanone [108-10-1] ^11 MRK5011UD R-0410010
ug/L EPA 8260B 05/15/17 21:46Acetone [67-64-1] ^100 MRK200140JD R-0410010
ug/L EPA 8260B 05/15/17 21:46Acrylonitrile [107-13-1] ^35 MRK10035UD R-0420010
ug/L EPA 8260B 05/15/17 21:46Benzene [71-43-2] ^1.5 MRK101.5 UD R-04110
ug/L EPA 8260B 05/15/17 21:46Bromochloromethane [74-97-5] ^4.8 MRK104.8 UD R-04310
ug/L EPA 8260B 05/15/17 21:46Bromodichloromethane [75-27-4] ^1.7 MRK101.7 UD R-04110
ug/L EPA 8260B 05/15/17 21:46Bromoform [75-25-2] ^2.2 MRK102.2 UD R-04310
ug/L EPA 8260B 05/15/17 21:46Bromomethane [74-83-9] ^1.4 MRK101.4 UD R-041010
ug/L EPA 8260B 05/15/17 21:46Carbon disulfide [75-15-0] ^15 MRK5015UD R-0410010
ug/L EPA 8260B 05/15/17 21:46Carbon tetrachloride [56-23-5] ^1.7 MRK101.7 UD R-04110
ug/L EPA 8260B 05/15/17 21:46Chlorobenzene [108-90-7] ^1.7 MRK101.7 UD R-04310
ug/L EPA 8260B 05/15/17 21:46Chloroethane [75-00-3] ^2.3 MRK102.3 UD R-041010
ug/L EPA 8260B 05/15/17 21:46Chloroform [67-66-3] ^1.8 MRK101.8 UD R-04510
ug/L EPA 8260B 05/15/17 21:46Chloromethane [74-87-3] ^1.3 MRK101.3 UD R-04110
ug/L EPA 8260B 05/15/17 21:46cis-1,2-Dichloroethene [156-59-2] ^1.5 MRK101.5 UD R-04510
ug/L EPA 8260B 05/15/17 21:46cis-1,3-Dichloropropene [10061-01-5] ^2.0 MRK102.0 UD R-04110
ug/L EPA 8260B 05/15/17 21:46Dibromochloromethane [124-48-1] ^1.7 MRK101.7 UD R-04310
ug/L EPA 8260B 05/15/17 21:46Dibromomethane [74-95-3] ^2.7 MRK102.7 UD R-041010
ug/L EPA 8260B 05/15/17 21:46Ethylbenzene [100-41-4] ^1.3 MRK101.3 UD R-04110
ug/L EPA 8260B 05/15/17 21:46Iodomethane [74-88-4] ^17 MRK5017UD R-041010
ug/L EPA 8260B 05/15/17 21:46m,p-Xylenes [108-38-3/106-42-3] ^1.7 MRK201.7 UD R-04NE10
ug/L EPA 8260B 05/15/17 21:46Methylene chloride [75-09-2] ^2.3 MRK102.3 UD R-04110
ug/L EPA 8260B 05/15/17 21:46o-Xylene [95-47-6] ^0.65 MRK100.65 UD R-04NE10
ug/L EPA 8260B 05/15/17 21:46Styrene [100-42-5] ^1.1 MRK101.1 UD R-04110
ug/L EPA 8260B 05/15/17 21:46Tetrachloroethene [127-18-4] ^1.7 MRK101.7 UD R-04110
ug/L EPA 8260B 05/15/17 21:46Toluene [108-88-3] ^1.4 MRK101.4 UD R-04110
ug/L EPA 8260B 05/15/17 21:46trans-1,2-Dichloroethene [156-60-5] ^2.1 MRK102.1 UD R-04510
ug/L EPA 8260B 05/15/17 21:46trans-1,3-Dichloropropene [10061-02-6] ^1.5 MRK101.5 UD R-04110
ug/L EPA 8260B 05/15/17 21:46trans-1,4-Dichloro-2-butene [110-57-6] ^7.0 MRK107.0 UD R-0410010
ug/L EPA 8260B 05/15/17 21:46Trichloroethene [79-01-6] ^1.5 MRK101.5 UD R-04110
ug/L EPA 8260B 05/15/17 21:46Trichlorofluoromethane [75-69-4] ^2.4 MRK102.4 UD R-04110
ug/L EPA 8260B 05/15/17 21:46Vinyl acetate [108-05-4] ^9.5 MRK509.5 UD R-045010
ug/L EPA 8260B 05/15/17 21:46Vinyl chloride [75-01-4] ^3.2 MRK103.2 UD R-04110
ug/L EPA 8260B 05/15/17 21:46Xylenes (Total) [1330-20-7] ^4.5 MRK304.5 UD R-04510
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
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www.encolabs.com
4104-LeachateP4-5Description:Lab Sample ID:CA05957-02 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 13:25 Work Order:CA05957
Kersey Valley Landfill-LeachateProject:Sampled By:Travis Queen
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF
4-Bromofluorobenzene 53-13689 %MRKEPA 8260B 05/15/17 21:467E120244450.0 R-041
Dibromofluoromethane 67-12995 %MRKEPA 8260B 05/15/17 21:467E120244850.0 R-041
Toluene-d8 59-13493 %MRKEPA 8260B 05/15/17 21:467E120244650.0 R-041
Page 9 of 21
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www.encolabs.com
4104-LeachateP4-5Description:Lab Sample ID:CA05957-02 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 13:25 Work Order:CA05957
Kersey Valley Landfill-LeachateProject:Sampled By:Travis Queen
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L EPA 6020B 05/22/17 13:35Antimony [7440-36-0] ^3.70 JDH20.03.70 UD 610
ug/L EPA 6010D 05/12/17 11:25Arsenic [7440-38-2] ^6.80 JMV10.09.66 J 101
ug/L EPA 6010D 05/12/17 11:25Barium [7440-39-3] ^1.00 JMV10.0169 1001
ug/L EPA 6010D 05/12/17 11:25Beryllium [7440-41-7] ^0.130 JMV1.000.130 U 11
ug/L EPA 6010D 05/12/17 11:25Cadmium [7440-43-9] ^0.360 JMV1.000.360 U 11
ug/L EPA 6010D 05/12/17 11:25Chromium [7440-47-3] ^1.40 JMV10.011.7 101
ug/L EPA 6010D 05/12/17 11:25Cobalt [7440-48-4] ^1.10 JMV10.011.4 101
ug/L EPA 6010D 05/12/17 11:25Copper [7440-50-8] ^1.60 JMV10.03.60 J 101
ug/L EPA 6010D 05/12/17 11:25Lead [7439-92-1] ^3.10 JMV10.03.10 U 101
ug/L EPA 6010D 05/12/17 11:25Nickel [7440-02-0] ^2.20 JMV10.030.8 J 501
ug/L EPA 6020B 05/22/17 13:35Selenium [7782-49-2] ^9.10 JDH30.09.10 UD 1010
ug/L EPA 6010D 05/12/17 11:25Silver [7440-22-4] ^1.90 JMV10.01.90 U 101
ug/L EPA 6020B 05/22/17 13:35Thallium [7440-28-0] ^1.10 JDH10.01.10 UD 5.510
ug/L EPA 6010D 05/12/17 11:25Vanadium [7440-62-2] ^1.40 JMV10.016.8 J 251
ug/L EPA 6010D 05/12/17 11:25Zinc [7440-66-6] ^4.40 JMV10.09.55 J 101
Page 10 of 21
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www.encolabs.com
4104-LeachateP4-5Description:Lab Sample ID:CA05957-02 05/04/17 09:30Received:
Matrix:Water Sampled:05/03/17 13:25 Work Order:CA05957
Kersey Valley Landfill-LeachateProject:Sampled By:Travis Queen
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 591]
Analyte [CAS Number]DFUnitsResults MDL Method Analyzed ByMRLFlag NotesNC SWSL
ug/L SM 5210B-2001 05/04/17 14:23Biochemical Oxygen Demand^2000 JOC200020000 NE1
ug/L SM 5220D-1997 05/05/17 09:52Chemical Oxygen Demand^10000 JOC10000190000 NE1
ug/L EPA 353.2 05/10/17 10:27Nitrate as N [14797-55-8] ^25 JLJ100100J 100001
ug/L EPA 353.2 05/04/17 14:16Nitrate/Nitrite as N^41 JLJ100120 NE1
ug/L EPA 353.2 05/05/17 09:36Nitrite as N [14797-65-0] ^17 JLJ10020J 10001
ug/L EPA 365.4 05/08/17 14:17Phosphorus [7723-14-0] ^25 JLJ100680 NE1
ug/L EPA 300.0 05/16/17 16:41Sulfate as SO4 [14808-79-8] ^2900 MKS500014000J 2500001
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 11 of 21
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www.encolabs.com
QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E12024 - EPA 5030B_MS
Prepared: 05/12/2017 13:06 Analyzed: 05/15/2017 15:14Blank (7E12024-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.00.17 U 1,1,1,2-Tetrachloroethane
ug/L1.00.12 U 1,1,1-Trichloroethane
ug/L1.00.28 U 1,1,2,2-Tetrachloroethane
ug/L1.00.14 U 1,1,2-Trichloroethane
ug/L1.00.13 U 1,1-Dichloroethane
ug/L1.00.21 U 1,1-Dichloroethene
ug/L1.00.23 U 1,2,3-Trichloropropane
ug/L1.00.48 U 1,2-Dibromo-3-chloropropane
ug/L1.00.66 U 1,2-Dibromoethane
ug/L1.00.19 U 1,2-Dichlorobenzene
ug/L1.00.21 U 1,2-Dichloroethane
ug/L1.00.10 U 1,2-Dichloropropane
ug/L1.00.19 U 1,4-Dichlorobenzene
ug/L5.01.3 U 2-Butanone
ug/L5.00.88 U 2-Hexanone
ug/L5.01.1 U 4-Methyl-2-pentanone
ug/L2010U Acetone
ug/L103.5 U Acrylonitrile
ug/L1.00.15 U Benzene
ug/L1.00.48 U Bromochloromethane
ug/L1.00.17 U Bromodichloromethane
ug/L1.00.22 U Bromoform
ug/L1.00.14 U Bromomethane
ug/L5.01.5 U Carbon disulfide
ug/L1.00.17 U Carbon tetrachloride
ug/L1.00.17 U Chlorobenzene
ug/L1.00.23 U Chloroethane
ug/L1.00.18 U Chloroform
ug/L1.00.13 U Chloromethane
ug/L1.00.15 U cis-1,2-Dichloroethene
ug/L1.00.20 U cis-1,3-Dichloropropene
ug/L1.00.17 U Dibromochloromethane
ug/L1.00.27 U Dibromomethane
ug/L1.00.13 U Ethylbenzene
ug/L5.01.7 U Iodomethane
ug/L2.00.17 U m,p-Xylenes
ug/L1.00.23 U Methylene chloride
ug/L1.00.065 U o-Xylene
ug/L1.00.11 U Styrene
ug/L1.00.17 U Tetrachloroethene
ug/L1.00.14 U Toluene
ug/L1.00.21 U trans-1,2-Dichloroethene
ug/L1.00.15 U trans-1,3-Dichloropropene
ug/L1.00.70 U trans-1,4-Dichloro-2-butene
ug/L1.00.15 U Trichloroethene
ug/L1.00.24 U Trichlorofluoromethane
ug/L5.00.95 U Vinyl acetate
ug/L1.00.32 U Vinyl chloride
ug/L3.00.45 U Xylenes (Total)
Page 12 of 21
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QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 7E12024 - EPA 5030B_MS
Prepared: 05/12/2017 13:06 Analyzed: 05/15/2017 15:14Blank (7E12024-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9145
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9347
ug/L 50.0 59-134Surrogate: Toluene-d8 9347
Prepared: 05/12/2017 13:06 Analyzed: 05/15/2017 13:13LCS (7E12024-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-13310120 1,1-Dichloroethene
ug/L1.0 20.0 81-13411022 Benzene
ug/L1.0 20.0 83-11710020 Chlorobenzene
ug/L1.0 20.0 71-11811523 Toluene
ug/L1.0 20.0 74-1199820 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9447
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9146
ug/L 50.0 59-134Surrogate: Toluene-d8 9447
Prepared: 05/12/2017 13:06 Analyzed: 05/15/2017 13:43Matrix Spike (7E12024-MS1)
Source: CA07386-03
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 75-1331050.21 U21 1,1-Dichloroethene
ug/L1.0 20.0 81-1341100.15 U22 Benzene
ug/L1.0 20.0 83-1171010.17 U20 Chlorobenzene
ug/L1.0 20.0 71-1181160.14 U23 Toluene
ug/L1.0 20.0 74-1191010.15 U20 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 9547
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9045
ug/L 50.0 59-134Surrogate: Toluene-d8 9447
Prepared: 05/12/2017 13:06 Analyzed: 05/15/2017 14:13Matrix Spike Dup (7E12024-MSD1)
Source: CA07386-03
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1.0 20.0 2075-13398 70.21 U20 1,1-Dichloroethene
ug/L1.0 20.0 1781-134106 40.15 U21 Benzene
ug/L1.0 20.0 1683-11791 110.17 U18 Chlorobenzene
ug/L1.0 20.0 1771-118102 130.14 U20 Toluene
ug/L1.0 20.0 2274-11994 80.15 U19 Trichloroethene
ug/L 50.0 53-136Surrogate: 4-Bromofluorobenzene 8844
ug/L 50.0 67-129Surrogate: Dibromofluoromethane 9347
ug/L 50.0 59-134Surrogate: Toluene-d8 9749
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7E09020 - EPA 3005A
Prepared: 05/09/2017 13:37 Analyzed: 05/12/2017 10:53Blank (7E09020-BLK1)
Page 13 of 21
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7E09020 - EPA 3005A
Prepared: 05/09/2017 13:37 Analyzed: 05/12/2017 10:53Blank (7E09020-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.06.80 U Arsenic
ug/L10.01.00 U Barium
ug/L1.000.130 U Beryllium
ug/L1.000.360 U Cadmium
ug/L10.01.40 U Chromium
ug/L10.01.10 U Cobalt
ug/L10.01.60 U Copper
ug/L10.03.10 U Lead
ug/L10.02.20 U Nickel
ug/L10.01.90 U Silver
ug/L10.01.40 U Vanadium
ug/L10.04.40 U Zinc
Prepared: 05/09/2017 13:37 Analyzed: 05/12/2017 10:56LCS (7E09020-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 80-12096192 Arsenic
ug/L10.0 200 80-12097194 Barium
ug/L1.00 20.0 80-1209619.1 Beryllium
ug/L1.00 20.0 80-12010020.1 Cadmium
ug/L10.0 200 80-12094189 Chromium
ug/L10.0 200 80-12099197 Cobalt
ug/L10.0 200 80-12094188 Copper
ug/L10.0 200 80-12099197 Lead
ug/L10.0 200 80-12096192 Nickel
ug/L10.0 200 80-12094188 Silver
ug/L10.0 200 80-12092184 Vanadium
ug/L10.0 200 80-120101203 Zinc
Prepared: 05/09/2017 13:37 Analyzed: 05/12/2017 11:01Matrix Spike (7E09020-MS1)
Source: CA05956-21
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 75-125946.80 U187 Arsenic
ug/L10.0 200 75-12588219395 Barium
ug/L1.00 20.0 75-125950.130 U19.0 Beryllium
ug/L1.00 20.0 75-125890.360 U17.8 Cadmium
ug/L10.0 200 75-125921.40 U185 Chromium
ug/L10.0 200 75-125927.31191 Cobalt
ug/L10.0 200 75-125941.60 U189 Copper
ug/L10.0 200 75-125923.10 U185 Lead
ug/L10.0 200 75-125912.20 U183 Nickel
ug/L10.0 200 75-125941.90 U188 Silver
ug/L10.0 200 75-125922.63187 Vanadium
ug/L10.0 200 75-125954.40 U189 Zinc
Prepared: 05/09/2017 13:37 Analyzed: 05/12/2017 11:06Matrix Spike Dup (7E09020-MSD1)
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7E09020 - EPA 3005A
Prepared: 05/09/2017 13:37 Analyzed: 05/12/2017 11:06Matrix Spike Dup (7E09020-MSD1) Continued
Source: CA05956-21
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10.0 200 2075-125102 86.80 U203 Arsenic
ug/L10.0 200 2075-125105 8219429 Barium
ug/L1.00 20.0 2075-125104 90.130 U20.9 Beryllium
ug/L1.00 20.0 2075-12596 80.360 U19.1 Cadmium
ug/L10.0 200 2075-125101 91.40 U203 Chromium
ug/L10.0 200 2075-125101 97.31209 Cobalt
ug/L10.0 200 2075-125104 91.60 U207 Copper
ug/L10.0 200 2075-125102 103.10 U204 Lead
ug/L10.0 200 2075-125101 92.20 U201 Nickel
ug/L10.0 200 2075-125102 91.90 U205 Silver
ug/L10.0 200 2075-125101 102.63206 Vanadium
ug/L10.0 200 2075-125104 94.40 U208 Zinc
Prepared: 05/09/2017 13:37 Analyzed: 05/12/2017 11:09Post Spike (7E09020-PS1)
Source: CA05956-21
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.0100 0.200 80-120990.001340.198 Arsenic
mg/L0.0100 0.200 80-120990.2190.416 Barium
mg/L0.00100 0.0200 80-120102-7.01E-50.0203 Beryllium
mg/L0.00100 0.0200 80-12095-0.0005380.0191 Cadmium
mg/L0.0100 0.200 80-12099-0.0002000.198 Chromium
mg/L0.0100 0.200 80-120990.007310.205 Cobalt
mg/L0.0100 0.200 80-120101-0.0009990.201 Copper
mg/L0.0100 0.200 80-120990.0007740.198 Lead
mg/L0.0100 0.200 80-12098-0.0004390.196 Nickel
mg/L0.0100 0.200 80-120100-0.0005070.199 Silver
mg/L0.0100 0.200 80-120980.002630.199 Vanadium
mg/L0.0100 0.200 80-1201010.0008490.204 Zinc
Batch 7E12023 - EPA 3005A
Prepared: 05/12/2017 12:27 Analyzed: 05/22/2017 12:16Blank (7E12023-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.000.370 U Antimony
ug/L3.000.910 U Selenium
ug/L1.000.110 U Thallium
Prepared: 05/12/2017 12:27 Analyzed: 05/22/2017 12:24LCS (7E12023-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-120102205 Antimony
ug/L3.00 200 80-120110220 Selenium
ug/L1.00 200 80-120103205 Thallium
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QUALITY CONTROL
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 7E12023 - EPA 3005A
Prepared: 05/12/2017 12:27 Analyzed: 05/22/2017 12:28Matrix Spike (7E12023-MS1)
Source: CA05956-11
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 75-1251040.370 U208 Antimony
ug/L3.00 200 75-1251140.910 U228 Selenium
ug/L1.00 200 75-1251020.110 U205 Thallium
Prepared: 05/12/2017 12:27 Analyzed: 05/22/2017 12:32Matrix Spike Dup (7E12023-MSD1)
Source: CA05956-11
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 2075-125105 10.370 U210 Antimony
ug/L3.00 200 2075-125115 10.910 U231 Selenium
ug/L1.00 200 2075-125104 10.110 U207 Thallium
Prepared: 05/12/2017 12:27 Analyzed: 05/22/2017 12:35Post Spike (7E12023-PS1)
Source: CA05956-11
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2.00 200 80-1201040.134209 Antimony
ug/L3.00 200 80-1201090.291218 Selenium
ug/L1.00 200 75-125990.0712199 Thallium
Classical Chemistry Parameters - Quality Control
Batch 7E04027 - NO PREP
Prepared: 05/04/2017 13:47 Analyzed: 05/04/2017 13:47Blank (7E04027-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10041U Nitrate/Nitrite as N
Prepared: 05/04/2017 13:49 Analyzed: 05/04/2017 13:49LCS (7E04027-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.10 1.25 90-110941.2 Nitrate/Nitrite as N
Prepared: 05/04/2017 14:02 Analyzed: 05/04/2017 14:02Matrix Spike (7E04027-MS1)
Source: CA01939-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L100 513 90-11010041 U510 Nitrate/Nitrite as N
Prepared: 05/04/2017 13:58 Analyzed: 05/04/2017 13:58Matrix Spike (7E04027-MS2)
Source: CA04526-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10000 50000 90-1109875000120000 Nitrate/Nitrite as N
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QUALITY CONTROL
Classical Chemistry Parameters - Quality Control
Batch 7E04027 - NO PREP
Prepared: 05/04/2017 14:07 Analyzed: 05/04/2017 14:07Matrix Spike Dup (7E04027-MSD1)
Source: CA01939-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L100 513 1090-11096 441 U490 Nitrate/Nitrite as N
Batch 7E04028 - NO PREP
Prepared & Analyzed: 05/04/2017 14:23Blank (7E04028-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L20002000U Biochemical Oxygen Demand
Prepared & Analyzed: 05/04/2017 14:23LCS (7E04028-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2000 198000 85-11594190000 Biochemical Oxygen Demand
Prepared & Analyzed: 05/04/2017 14:23Duplicate (7E04028-DUP1)
Source: CA01318-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L2000 3013340000290000 Biochemical Oxygen Demand
Batch 7E04033 - Same
Prepared: 05/04/2017 17:30 Analyzed: 05/05/2017 09:52Blank (7E04033-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L1000010000U Chemical Oxygen Demand
Prepared: 05/04/2017 17:30 Analyzed: 05/05/2017 09:52LCS (7E04033-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10000 500000 90-11099490000 Chemical Oxygen Demand
Prepared: 05/04/2017 17:30 Analyzed: 05/05/2017 09:52Matrix Spike (7E04033-MS1)
Source: CA03400-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L80000 4000000 90-1109042000007800000 Chemical Oxygen Demand
Prepared: 05/04/2017 17:30 Analyzed: 05/05/2017 09:52Matrix Spike Dup (7E04033-MSD1)
Source: CA03400-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L80000 4000000 1090-11088 142000007700000 QM-07Chemical Oxygen Demand
Batch 7E05003 - NO PREP
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QUALITY CONTROL
Classical Chemistry Parameters - Quality Control
Prepared: 05/05/2017 09:32 Analyzed: 05/05/2017 09:32Blank (7E05003-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10017U Nitrite as N
Prepared: 05/05/2017 09:34 Analyzed: 05/05/2017 09:34LCS (7E05003-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
mg/L0.10 1.00 90-1101011.0 Nitrite as N
Prepared: 05/05/2017 09:33 Analyzed: 05/05/2017 09:33Matrix Spike (7E05003-MS1)
Source: CA05957-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L100 1000 90-1109514002400E QM-02Nitrite as N
Prepared: 05/05/2017 09:36 Analyzed: 05/05/2017 09:36Matrix Spike Dup (7E05003-MSD1)
Source: CA05957-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L100 1000 1090-11097 0.714002400E QM-02Nitrite as N
Batch 7E05009 - Same
Prepared: 05/05/2017 12:30 Analyzed: 05/08/2017 13:11Blank (7E05009-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L10025U Phosphorus
Prepared: 05/05/2017 12:30 Analyzed: 05/08/2017 13:13LCS (7E05009-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L100 1600 80-1201031700 Phosphorus
Prepared: 05/05/2017 12:30 Analyzed: 05/08/2017 13:14Matrix Spike (7E05009-MS1)
Source: CA01318-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L100 640 80-1202973002200 QM-07Phosphorus
Prepared: 05/05/2017 12:30 Analyzed: 05/08/2017 13:18Matrix Spike Dup (7E05009-MSD1)
Source: CA01318-02
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L100 640 2580-120110 743001000 QM-11Phosphorus
Batch 7E16015 - NO PREP
Prepared: 05/16/2017 11:06 Analyzed: 05/16/2017 12:37Blank (7E16015-BLK1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
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QUALITY CONTROL
Classical Chemistry Parameters - Quality Control
Batch 7E16015 - NO PREP
Prepared: 05/16/2017 11:06 Analyzed: 05/16/2017 12:37Blank (7E16015-BLK1) Continued
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L50002900U Sulfate as SO4
Prepared: 05/16/2017 11:06 Analyzed: 05/16/2017 12:52LCS (7E16015-BS1)
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L5000 50000 90-1109949000 Sulfate as SO4
Prepared: 05/16/2017 11:06 Analyzed: 05/16/2017 13:06Matrix Spike (7E16015-MS1)
Source: CA01939-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L5000 20000 90-11092590024000 Sulfate as SO4
Prepared: 05/16/2017 11:06 Analyzed: 05/16/2017 13:35Matrix Spike (7E16015-MS2)
Source: CA05496-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L5000 20000 90-11091460023000 Sulfate as SO4
Prepared: 05/16/2017 11:06 Analyzed: 05/16/2017 13:20Matrix Spike Dup (7E16015-MSD1)
Source: CA01939-01
RPD%RECSourceSpike
MRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResultFlag
ug/L5000 20000 1090-11095 2590025000 Sulfate as SO4
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FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
The RPD and/or percent recovery for this QC spike sample cannot be accurately calculated due
to the high concentration of analyte present in the sample.
QM-02
The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was
accepted based on acceptable LCS recovery.
QM-07
Precision between duplicate matrix spikes of the same sample was outside acceptance limits.QM-11
The Reporting Limits for this analysis are elevated due to sample foaming.R-04
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