9209_CDLFNorthWakeclosed_April2017GWMR_20170601

North Wake C&D Landfill
Facility Permit No. 9209-CDLF
Semi-Annual Sampling Report
(April 2017 Sampling Event)
Wake County
Report
Prepared June 2017

5400 Glenwood Avenue, Suite 400
Raleigh, North Carolina 27612
tel: [phone]
fax: [phone]

June 1, 2017

Ms. Jaclynne Drummond
North Carolina Department of Environmental Quality
Division of Waste Management
Solid Waste Section
2090 U.S. 70 Highway
Swannanoa, North Carolina 28778

Subject: April 2017 Semi-Annual Groundwater Monitoring Report
North Wake C&D Landfill
Facility Permit No. 9209-CDLF

Dear Ms. Drummond:
CDM Smith Inc. (CDM Smith), on behalf of Wake County, is submitting an electronic copy of the April
2017 semi-annual sampling event report. This letter report presents the results of the most recent
semi-annual sampling event at the North Wake C&D Landfill and constitutes the first sampling event
for 2017. The approved groundwater monitoring network consists of the background well (i.e. MW-1)
and three downgradient compliance wells (i.e. CD-1, -2, and -3). Field activities and results of the April
2017 sampling event are discussed below.
Field Activities
Groundwater samples from the North Wake C&D Landfill were collected on April 11, 2017, by use of
disposable, laboratory decontaminated bailers. Monitoring well locations for the North Wake C&D
Landfill are shown on Figure 1. Well construction details are provided in Table 1.
Groundwater elevations were measured at each well prior to sampling and are presented in Table 2.
These groundwater elevations were used to construct a potentiometric surface map for this sampling
event. The potentiometric contours are shown on Figure 1.
After depth to groundwater was measured, three well volumes of water were removed from each
well prior to sampling to provide fresh formation water within the well water column. Each well
volume was measured for pH, conductivity, temperature, turbidity, dissolved oxygen, and oxidation-
reduction potential using a YSI-556 multi-parameter water quality meter and a HANNA HI 98703
turbidity meter. Monitoring wells with elevated turbidity were allowed to stabilize prior to sample
collection. The water quality parameters at the time of sampling are presented in Table 2.

Ms. Jaclynne Drummond
June 1, 2017
Page 2

Sampling Results
Shealy Environmental Services, Inc. located in West Columbia, South Carolina, analyzed the
groundwater samples for North Carolina Appendix I volatile organic compounds (VOCs) and Resource
and Conservation Recovery Act metals (i.e. arsenic, barium, cadmium, chromium, lead, mercury,
selenium, and silver). In accordance with Solid Waste Section (SWS) guidelines the analytical results
were reported to the laboratory specific method detection limit (MDL) and are quantifiable at or
below SWS Limits (SWSLs). All monitoring wells for the C&D Landfill had detections of analytes above
the MDL but below SWSLs. These detections were qualified as estimated or “J” flags. All mercury
detections had “B” flags, indicating that the analyte was detected in the associated method blank.
No VOCs or metals were detected above the 15A NCAC 02L .0202 (NC 2L) Groundwater Standard in
samples collected from MW-1, CD-1, or -2. Mercury was the only constituent detected above the NC
2L Groundwater Standard in samples collected from CD-3. Mercury has historically been detected
below the NC 2L Standard in the background monitoring well MW-1 and CD-3. Future analytical
results will be evaluated to determine if a trend appears.
Equipment and trip blanks were analyzed for quality control. The equipment blank had estimated
detections of acetone, barium, and mercury below their respective NC 2L Standard. There were no
VOC detections in the trip blank. A complete summary of all detected and estimated concentrations
for the March 2011 through April 2017 sampling events is presented in Table 3. The laboratory
analytical data report is provided in Appendix A.
The next semi-annual sampling event will be completed in the fall of 2017. If you have any questions
or require further explanation, do not hesitate to call me at [phone].
Very truly yours,

Mathew F. Colone, P.G.
CDM Smith Inc.

cc: John Roberson, WCSWM
Elliott Cornell, WCSWM
Table 1
Well Construction Summary
North Wake C&D Landfill - Permit Number 9209-CDLF
Facility
Permit
Number
Monitoring
Well Code
Installation
Date Latitude Longitude
Geology of
Screened
Interval
Total
Depth
(feet bgs)
Top of Casing
Elevation
(feet AMSL)
Screened
Interval
(feet bgs)
Filter Pack
Interval
(feet bgs)
Seal
Interval
(feet bgs)
Monitoring
Well Diameter
(inches)
9209-CDLF MW-1 1994 35.90984 78.58489 Regolith 58 333.80 48.0 - 58.0 46.0 - 58.0 44.0 - 46.0 2.0
9209-CDLF CD-1 May 2001 35.90907 78.58318 Regolith 25 296.26 10.0 - 25.0 8.0 - 25.0 8.0 - 10.0 2.0
9209-CDLF CD-2 May 2001 35.91032 78.58207 Regolith 25 282.64 10.0 - 25.0 8.0 - 25.0 8.0 - 10.0 2.0
9209-CDLF CD-3 May 2001 35.91016 78.58340 Regolith 33 301.49 10.0 - 25.0 8.0 - 25.0 8.0 - 10.0 2.0
Notes:
1. bgs - Below Ground Surface
2. AMSL - Above Mean Sea Level
3. Latitude and longitude coordinate system - World Geodetic System 1984
Page 1 of 1 June 2017
Table 2
Water Quality Parameters
North Wake C&D Landfill - Permit Number 9209-CDLF
pH Conductivity Temperature Turbidity DO ORP TOC
Elevation
Depth to
Groundwater
Groundwater
Elevation
(S.U.)(µS/cm)(degrees Celsius)(NTUs)(mg/L)(mV)(feet AMSL)(feet)(feet AMSL)
MW-1 5.56 71 16.6 19 4.98 55.1 333.80 46.98 286.82
CD-1 6.12 83 16.0 68 6.78 69.6 296.26 14.83 281.43
CD-2 5.81 81 15.4 25 6.39 79.1 282.64 11.59 271.05
CD-3 5.49 77 18.0 16 3.08 68.7 301.49 21.87 279.62
Notes:
1. AMSL - Above Mean Sea Level
2. TOC - Top of Casing
3. µS/cm - Microsiemens per centimeter
4. mg/L - Milligrams per liter
5. ORP - Oxidation-Reduction Potential
6. NTUs - Nephelometric Turbidity Units
7. mV - Millivolts
8. S.U. - Standard Units
9. DO - Dissolved Oxygen
10. Monitoring wells with high turbidity were allowed to settle prior to sampling; turbidity shown in table was recorded at the time of sampling.
April 2017 Semi-Annual Sampling Event
Monitoring
Well Code
Groundwater Elevations (Measured 4/10/2017)Water Quality Parameters
Page 1 of 1 June 2017
Table 3
Detected Groundwater Constituents - Metals and Volatile Organic Compounds
April 2017 Semi-Annual Sampling Event
North Wake C&D Landfill - Permit Number 9209-CDLF ArsenicBariumCadmiumChromiumLeadMercurySeleniumSilverAcetone1,1-DichloroetheneChloroformMethylene ChlorideVinyl ChlorideTetrahydrofuranTrichlorofluoromethane0.01 0.7 0.002 0.01 0.015 0.001 0.02 0.02 6,000 7 70 5 0.03 NS 2,000
0.01 0.1 0.001 0.01 0.01 0.0002 0.01 0.01 100 5 5 1 1 NS 1
MW-1 14-Mar-11 0.0421J
MW-1 20-Oct-11 0.0444J 0.00619J
MW-1 11-Apr-12 0.0384J
MW-1 26-Oct-12 0.0431J 0.00387J
MW-1 11-Apr-13 0.040J
MW-1 2-Oct-13 0.050J 0.001J
MW-1 3-Apr-14 0.040J 0.016 8.1J
MW-1 12-Nov-14 0.040J 0.00006J
MW-1 8-Apr-15 0.040J 0.001J 0.00021
MW-1 7-Oct-15 0.060J 0.001J 0.003J 0.00009J
MW-1 24-Mar-16 0.002J 0.040J 0.00013J 8.6J 0.27JB
MW-1 1-Sep-16 0.053J 0.000061J 0.0012J 0.0023J 0.00014J 2.3J
MW-1 11-Apr-17 0.044J 0.00042J 0.00071B
CD-1 14-Mar-11 0.00312J 0.174 0.00978J 0.00434J
CD-1 20-Oct-11 0.0629J 0.00306J
CD-1 11-Apr-12 0.0731J 0.00372J
CD-1 26-Oct-12 0.227 0.00793J 0.00669J
CD-1 11-Apr-13 0.130 0.007J
CD-1 2-Oct-13 0.220 0.013
CD-1 3-Apr-14 0.130 0.009J
CD-1 12-Nov-14 0.120 0.006J
CD-1 8-Apr-15 0.090J 0.006J
CD-1 7-Oct-15 0.070J 0.004J 6.1J
CD-1 25-Mar-16 0.002J 0.060J 0.003J 0.27JB
CD-1 1-Sep-16 0.068J 0.000065J 0.0031J 0.00059J
CD-1 11-Apr-17 0.075J 0.0034J 0.00065J 0.000062JB
CD-2 14-Mar-11 0.0569J 0.00174J 0.00274J 0.97J
CD-2 20-Oct-11 0.0532J 0.00378J 5.9J 1.8J
CD-2 11-Apr-12 0.340 0.0156 0.0142 0.00247J 0.80J
CD-2 26-Oct-12 0.102 0.00481J 0.00389J
CD-2 11-Apr-13 0.120 0.004J
CD-2 2-Oct-13 0.080J 0.005J
CD-2 3-Apr-14 0.060J 0.006J 0.61J
CD-2 12-Nov-14 0.040J 0.003J
CD-2 8-Apr-15 0.060J 0.002J 0.36J
CD-2 7-Oct-15 0.050J 0.0010J 0.003J
CD-2 25-Mar-16 0.002J 0.040J 0.001J
CD-2 1-Sep-16 0.066J 0.00023J 0.0032J 0.00094J
CD-2 11-Apr-17 0.051J 0.0023J 0.00045J 0.000038JB
CD-3 14-Mar-11 0.0507J
CD-3 20-Oct-11 0.0453J
CD-3 11-Apr-12 0.0675J 0.00226J
CD-3 26-Oct-12 0.0731J 0.00361J
CD-3 11-Apr-13 0.050J
CD-3 1-Oct-13 0.030J 0.00003J
CD-3 3-Apr-14 0.040J 0.001J
CD-3 12-Nov-14 0.040J 0.00008J
CD-3 8-Apr-15 0.040J 0.0001J
CD-3 7-Oct-15 0.050J 0.00026 0.28J
CD-3 24-Mar-16 0.003J 0.050J 0.00060 0.28JB 0.24J
CD-3 1-Sep-16 0.082J 0.000078J 0.0026J 0.0014 0.51J 1.2
CD-3 11-Apr-17 0.049J 0.00055J 0.00033J 0.0029B 0.40J 2.6

Notes:
1. Metal detections are in milligrams per liter (parts per million).
2. Volatile organic compound detections are in micrograms per liter (parts per billion).
4. B - Indicates the analyte was detected in the associated method blank.
5. NS - No Standard
- Concentration exceeds the 15A NCAC 02L .0202 (2L) Groundwater Standard.
- Indicates the result is below the detection limit.
North Carolina 2L Standard
Solid Waste Section Limit
Metals
3. J - Indicates the analytical result is an estimated concentration between the method detection limit and the Solid Waste Section Reporting Limit.Monitoring Well CodeSample DateVolatile Organic Compounds
Page 1 of 1 June 2017

Appendix A
Analytical Data
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
CDM Smith
5400 Glenwood Avenue
Suite 400
Raleigh, NC 27612
Attention: Mathew Colone
SD12009Lot Number:
North Wake C&D LandfillProject Name:
04/25/2017
04/25/2017
Date Completed:
Date Revised:
Catherine S. Dover
Project Manager

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Page: 1 of 34
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Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
CDM Smith
Lot Number: SD12009
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
Project Name: North Wake C&D Landfill
Project Number:
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
VOA 8260B
Sample SD12009-004 (C-3) was re-analyzed within holding times to confirm the vinyl chloride hit in the first analysis. Vinyl chloride was non-detect
in the re-analysis. The vinyl chloride hit reported in the first analysis is attributed to the presence of freon-151 in the sample that degraded to vinyl
chloride in the instrument trap during the heated desorb process.
Page: 2 of 34
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
CDM Smith
Lot Number: SD12009

Project Name: North Wake C&D Landfill
Project Number:
Sample Number Sample ID Matrix Date Sampled Date Received
001 04/11/2017 0925MW-1 Aqueous 04/12/2017
002 04/11/2017 1000CD-1 Aqueous 04/12/2017
003 04/11/2017 0950CD-2 Aqueous 04/12/2017
004 04/11/2017 0945CD-3 Aqueous 04/12/2017
005 04/11/2017 1530EQ BLANK Aqueous 04/12/2017
006 04/11/2017TRIP BLANK Aqueous 04/12/2017
(6 samples)
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Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-1
SD12009-001
04/11/2017 0925
04/12/2017
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/12/2017 2317 ECP 39496
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Tetrahydrofuran 109-99-9 8260B 5.0 U 1ug/L1.05.0
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 4 of 34
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-1
SD12009-001
04/11/2017 0925
04/12/2017
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/12/2017 2317 ECP 39496
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 111 70-130
1,2-Dichloroethane-d4 105 70-130
Toluene-d8 103 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
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Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
MW-1
SD12009-001
04/11/2017 0925
04/12/2017
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 04/14/2017 1704 COH 04/14/2017 1246 39621
1 3005A 6020B 1 04/13/2017 1457 BNW 04/13/2017 0905 39507
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6020B 2.0 U 1ug/L1.32.0
Barium 7440-39-3 6020B 44 1ug/L0.635.0
Cadmium 7440-43-9 6020B 0.50 U 1ug/L0.130.50
Chromium 7440-47-3 6020B 5.0 U 1ug/L1.35.0
Lead 7439-92-1 6020B 0.42 J 1ug/L0.251.0
Mercury 7439-97-6 7470A 0.00071 B 1mg/L0.0000280.00010
Selenium 7782-49-2 6020B 5.0 U 1ug/L1.35.0
Silver 7440-22-4 6020B 1.0 U 1ug/L0.251.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 6 of 34
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Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
CD-1
SD12009-002
04/11/2017 1000
04/12/2017
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/12/2017 2338 ECP 39496
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Tetrahydrofuran 109-99-9 8260B 5.0 U 1ug/L1.05.0
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 7 of 34
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
CD-1
SD12009-002
04/11/2017 1000
04/12/2017
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/12/2017 2338 ECP 39496
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 106 70-130
1,2-Dichloroethane-d4 103 70-130
Toluene-d8 98 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 8 of 34
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
CD-1
SD12009-002
04/11/2017 1000
04/12/2017
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 04/14/2017 1707 COH 04/14/2017 1246 39621
1 3005A 6020B 1 04/13/2017 1503 BNW 04/13/2017 0905 39507
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6020B 2.0 U 1ug/L1.32.0
Barium 7440-39-3 6020B 75 1ug/L0.635.0
Cadmium 7440-43-9 6020B 0.50 U 1ug/L0.130.50
Chromium 7440-47-3 6020B 3.4 J 1ug/L1.35.0
Lead 7439-92-1 6020B 0.65 J 1ug/L0.251.0
Mercury 7439-97-6 7470A 0.000062 BJ 1mg/L0.0000280.00010
Selenium 7782-49-2 6020B 5.0 U 1ug/L1.35.0
Silver 7440-22-4 6020B 1.0 U 1ug/L0.251.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 9 of 34
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
CD-2
SD12009-003
04/11/2017 0950
04/12/2017
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/13/2017 0000 ECP 39496
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Tetrahydrofuran 109-99-9 8260B 5.0 U 1ug/L1.05.0
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 10 of 34
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
CD-2
SD12009-003
04/11/2017 0950
04/12/2017
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/13/2017 0000 ECP 39496
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 107 70-130
1,2-Dichloroethane-d4 108 70-130
Toluene-d8 100 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 11 of 34
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
CD-2
SD12009-003
04/11/2017 0950
04/12/2017
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 04/14/2017 1714 COH 04/14/2017 1246 39621
1 3005A 6020B 1 04/13/2017 1509 BNW 04/13/2017 0905 39507
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6020B 2.0 U 1ug/L1.32.0
Barium 7440-39-3 6020B 51 1ug/L0.635.0
Cadmium 7440-43-9 6020B 0.50 U 1ug/L0.130.50
Chromium 7440-47-3 6020B 2.3 J 1ug/L1.35.0
Lead 7439-92-1 6020B 0.45 J 1ug/L0.251.0
Mercury 7439-97-6 7470A 0.000038 BJ 1mg/L0.0000280.00010
Selenium 7782-49-2 6020B 5.0 U 1ug/L1.35.0
Silver 7440-22-4 6020B 1.0 U 1ug/L0.251.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 12 of 34
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
CD-3
SD12009-004
04/11/2017 0945
04/12/2017
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/13/2017 0022 ECP 39496
2 5030B 8260B 1 04/24/2017 2117 ECP 40382
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.40 J 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Tetrahydrofuran 109-99-9 8260B 2.6 J 1ug/L1.05.0
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 13 of 34
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
CD-3
SD12009-004
04/11/2017 0945
04/12/2017
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/13/2017 0022 ECP 39496
2 5030B 8260B 1 04/24/2017 2117 ECP 40382
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 2ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
Bromofluorobenzene 111 70-130 H 103 70-130
1,2-Dichloroethane-d4 110 70-130 H 96 70-130
Toluene-d8 105 70-130 H 102 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 14 of 34
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
CD-3
SD12009-004
04/11/2017 0945
04/12/2017
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 04/14/2017 1723 COH 04/14/2017 1246 39621
1 3005A 6020B 1 04/13/2017 1515 BNW 04/13/2017 0905 39507
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6020B 2.0 U 1ug/L1.32.0
Barium 7440-39-3 6020B 49 1ug/L0.635.0
Cadmium 7440-43-9 6020B 0.55 1ug/L0.130.50
Chromium 7440-47-3 6020B 5.0 U 1ug/L1.35.0
Lead 7439-92-1 6020B 0.33 J 1ug/L0.251.0
Mercury 7439-97-6 7470A 0.0029 B 1mg/L0.0000280.00010
Selenium 7782-49-2 6020B 5.0 U 1ug/L1.35.0
Silver 7440-22-4 6020B 1.0 U 1ug/L0.251.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 15 of 34
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
EQ BLANK
SD12009-005
04/11/2017 1530
04/12/2017
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/12/2017 2233 ECP 39496
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 2.4 J 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Tetrahydrofuran 109-99-9 8260B 5.0 U 1ug/L1.05.0
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 16 of 34
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
EQ BLANK
SD12009-005
04/11/2017 1530
04/12/2017
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/12/2017 2233 ECP 39496
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 104 70-130
1,2-Dichloroethane-d4 103 70-130
Toluene-d8 100 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 17 of 34
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ICP-MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
EQ BLANK
SD12009-005
04/11/2017 1530
04/12/2017
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 04/14/2017 1728 COH 04/14/2017 1246 39621
1 3005A 6020B 1 04/13/2017 1539 BNW 04/13/2017 0905 39507
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6020B 2.0 U 1ug/L1.32.0
Barium 7440-39-3 6020B 0.73 J 1ug/L0.635.0
Cadmium 7440-43-9 6020B 0.50 U 1ug/L0.130.50
Chromium 7440-47-3 6020B 5.0 U 1ug/L1.35.0
Lead 7439-92-1 6020B 1.0 U 1ug/L0.251.0
Mercury 7439-97-6 7470A 0.000034 BJ 1mg/L0.0000280.00010
Selenium 7782-49-2 6020B 5.0 U 1ug/L1.35.0
Silver 7440-22-4 6020B 1.0 U 1ug/L0.251.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 18 of 34
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Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
TRIP BLANK
SD12009-006
04/11/2017
04/12/2017
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/12/2017 2255 ECP 39496
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 10 U 1ug/L2.010
Acrylonitrile 107-13-1 8260B 5.0 U 1ug/L0.805.0
Benzene 71-43-2 8260B 0.50 U 1ug/L0.400.50
Bromochloromethane 74-97-5 8260B 0.50 U 1ug/L0.400.50
Bromodichloromethane 75-27-4 8260B 0.50 U 1ug/L0.400.50
Bromoform 75-25-2 8260B 0.50 U 1ug/L0.400.50
Bromomethane (Methyl bromide)74-83-9 8260B 0.50 U 1ug/L0.400.50
2-Butanone (MEK)78-93-3 8260B 10 U 1ug/L2.010
Carbon disulfide 75-15-0 8260B 0.50 U 1ug/L0.400.50
Carbon tetrachloride 56-23-5 8260B 0.50 U 1ug/L0.400.50
Chlorobenzene 108-90-7 8260B 0.50 U 1ug/L0.400.50
Chloroethane 75-00-3 8260B 0.50 U 1ug/L0.400.50
Chloroform 67-66-3 8260B 0.50 U 1ug/L0.400.50
Chloromethane (Methyl chloride)74-87-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B 0.50 U 1ug/L0.400.50
Dibromochloromethane 124-48-1 8260B 0.50 U 1ug/L0.400.50
1,2-Dibromoethane (EDB)106-93-4 8260B 0.50 U 1ug/L0.400.50
Dibromomethane (Methylene bromide)74-95-3 8260B 0.50 U 1ug/L0.400.50
trans-1,4-Dichloro-2-butene 110-57-6 8260B 2.0 U 1ug/L0.402.0
1,2-Dichlorobenzene 95-50-1 8260B 0.50 U 1ug/L0.400.50
1,4-Dichlorobenzene 106-46-7 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethane 75-34-3 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloroethane 107-06-2 8260B 0.50 U 1ug/L0.400.50
1,1-Dichloroethene 75-35-4 8260B 0.50 U 1ug/L0.400.50
cis-1,2-Dichloroethene 156-59-2 8260B 0.50 U 1ug/L0.400.50
trans-1,2-Dichloroethene 156-60-5 8260B 0.50 U 1ug/L0.400.50
1,2-Dichloropropane 78-87-5 8260B 0.50 U 1ug/L0.400.50
cis-1,3-Dichloropropene 10061-01-5 8260B 0.50 U 1ug/L0.400.50
trans-1,3-Dichloropropene 10061-02-6 8260B 0.50 U 1ug/L0.400.50
Ethylbenzene 100-41-4 8260B 0.50 U 1ug/L0.400.50
2-Hexanone 591-78-6 8260B 10 U 1ug/L2.010
Methyl iodide (Iodomethane)74-88-4 8260B 5.0 U 1ug/L0.405.0
4-Methyl-2-pentanone 108-10-1 8260B 10 U 1ug/L2.010
Methylene chloride 75-09-2 8260B 0.50 U 1ug/L0.400.50
Styrene 100-42-5 8260B 0.50 U 1ug/L0.400.50
1,1,1,2-Tetrachloroethane 630-20-6 8260B 0.50 U 1ug/L0.400.50
1,1,2,2-Tetrachloroethane 79-34-5 8260B 0.50 U 1ug/L0.400.50
Tetrachloroethene 127-18-4 8260B 0.50 U 1ug/L0.400.50
Tetrahydrofuran 109-99-9 8260B 5.0 U 1ug/L1.05.0
Toluene 108-88-3 8260B 0.50 U 1ug/L0.400.50
1,1,1-Trichloroethane 71-55-6 8260B 0.50 U 1ug/L0.400.50
1,1,2-Trichloroethane 79-00-5 8260B 0.50 U 1ug/L0.400.50
Trichloroethene 79-01-6 8260B 0.50 U 1ug/L0.400.50
Trichlorofluoromethane 75-69-4 8260B 0.50 U 1ug/L0.400.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 19 of 34
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
CDM Smith
TRIP BLANK
SD12009-006
04/11/2017
04/12/2017
Aqueous
Project Name: North Wake C&D Landfill
Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/12/2017 2255 ECP 39496
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,2,3-Trichloropropane 96-18-4 8260B 0.50 U 1ug/L0.400.50
Vinyl acetate 108-05-4 8260B 5.0 U 1ug/L1.25.0
Vinyl chloride 75-01-4 8260B 0.50 U 1ug/L0.400.50
Xylenes (total)1330-20-7 8260B 1.0 U 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
Bromofluorobenzene 108 70-130
1,2-Dichloroethane-d4 104 70-130
Toluene-d8 102 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
D = Dilution > 1
Page: 20 of 34
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QC Summary
Page: 21 of 34
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Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ39496-001
39496 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone 10 04/12/2017 2118U102.0 ug/L1
Acrylonitrile 5.0 04/12/2017 2118U5.0 0.80 ug/L1
Benzene 0.50 04/12/2017 2118U0.50 0.40 ug/L1
Bromochloromethane 0.50 04/12/2017 2118U0.50 0.40 ug/L1
Bromodichloromethane 0.50 04/12/2017 2118U0.50 0.40 ug/L1
Bromoform 0.50 04/12/2017 2118U0.50 0.40 ug/L1
Bromomethane (Methyl bromide)0.50 04/12/2017 2118U0.50 0.40 ug/L1
2-Butanone (MEK)10 04/12/2017 2118U102.0 ug/L1
Carbon disulfide 0.50 04/12/2017 2118U0.50 0.40 ug/L1
Carbon tetrachloride 0.50 04/12/2017 2118U0.50 0.40 ug/L1
Chlorobenzene 0.50 04/12/2017 2118U0.50 0.40 ug/L1
Chloroethane 0.50 04/12/2017 2118U0.50 0.40 ug/L1
Chloroform 0.50 04/12/2017 2118U0.50 0.40 ug/L1
Chloromethane (Methyl chloride)0.50 04/12/2017 2118U0.50 0.40 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)0.50 04/12/2017 2118U0.50 0.40 ug/L1
Dibromochloromethane 0.50 04/12/2017 2118U0.50 0.40 ug/L1
1,2-Dibromoethane (EDB)0.50 04/12/2017 2118U0.50 0.40 ug/L1
Dibromomethane (Methylene bromide)0.50 04/12/2017 2118U0.50 0.40 ug/L1
trans-1,4-Dichloro-2-butene 2.0 04/12/2017 2118U2.0 0.40 ug/L1
1,4-Dichlorobenzene 0.50 04/12/2017 2118U0.50 0.40 ug/L1
1,2-Dichlorobenzene 0.50 04/12/2017 2118U0.50 0.40 ug/L1
1,2-Dichloroethane 0.50 04/12/2017 2118U0.50 0.40 ug/L1
1,1-Dichloroethane 0.50 04/12/2017 2118U0.50 0.40 ug/L1
trans-1,2-Dichloroethene 0.50 04/12/2017 2118U0.50 0.40 ug/L1
cis-1,2-Dichloroethene 0.50 04/12/2017 2118U0.50 0.40 ug/L1
1,1-Dichloroethene 0.50 04/12/2017 2118U0.50 0.40 ug/L1
1,2-Dichloropropane 0.50 04/12/2017 2118U0.50 0.40 ug/L1
trans-1,3-Dichloropropene 0.50 04/12/2017 2118U0.50 0.40 ug/L1
cis-1,3-Dichloropropene 0.50 04/12/2017 2118U0.50 0.40 ug/L1
Ethylbenzene 0.50 04/12/2017 2118U0.50 0.40 ug/L1
2-Hexanone 10 04/12/2017 2118U102.0 ug/L1
Methyl iodide (Iodomethane)5.0 04/12/2017 2118U5.0 0.40 ug/L1
4-Methyl-2-pentanone 10 04/12/2017 2118U102.0 ug/L1
Methylene chloride 0.50 04/12/2017 2118U0.50 0.40 ug/L1
Styrene 0.50 04/12/2017 2118U0.50 0.40 ug/L1
1,1,2,2-Tetrachloroethane 0.50 04/12/2017 2118U0.50 0.40 ug/L1
1,1,1,2-Tetrachloroethane 0.50 04/12/2017 2118U0.50 0.40 ug/L1
Tetrachloroethene 0.50 04/12/2017 2118U0.50 0.40 ug/L1
Tetrahydrofuran 5.0 04/12/2017 2118U5.0 1.0 ug/L1
Toluene 0.50 04/12/2017 2118U0.50 0.40 ug/L1
1,1,2-Trichloroethane 0.50 04/12/2017 2118U0.50 0.40 ug/L1
1,1,1-Trichloroethane 0.50 04/12/2017 2118U0.50 0.40 ug/L1
Trichloroethene 0.50 04/12/2017 2118U0.50 0.40 ug/L1
Trichlorofluoromethane 0.50 04/12/2017 2118U0.50 0.40 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 22 of 34
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ39496-001
39496 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
1,2,3-Trichloropropane 0.50 04/12/2017 2118U0.50 0.40 ug/L1
Vinyl acetate 5.0 04/12/2017 2118U5.0 1.2 ug/L1
Vinyl chloride 0.50 04/12/2017 2118U0.50 0.40 ug/L1
Xylenes (total)1.0 04/12/2017 2118U1.0 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 107 70-130
1,2-Dichloroethane-d4 100 70-130
Toluene-d8 102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 23 of 34
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ39496-002
39496 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Acetone 97 04/12/2017 20209710060-1401
Acrylonitrile 92 04/12/2017 20209210060-1401
Benzene 47 04/12/2017 2020945070-1301
Bromochloromethane 48 04/12/2017 2020965070-1301
Bromodichloromethane 50 04/12/2017 20201005070-1301
Bromoform 49 04/12/2017 2020995070-1301
Bromomethane (Methyl bromide)51 04/12/2017 20201025060-1401
2-Butanone (MEK)97 04/12/2017 20209710060-1401
Carbon disulfide 49 04/12/2017 2020995060-1401
Carbon tetrachloride 50 04/12/2017 2020995070-1301
Chlorobenzene 48 04/12/2017 2020975070-1301
Chloroethane 51 04/12/2017 20201035060-1401
Chloroform 49 04/12/2017 2020985070-1301
Chloromethane (Methyl chloride)48 04/12/2017 2020955050-1301
1,2-Dibromo-3-chloropropane (DBCP)46 04/12/2017 2020915070-1301
Dibromochloromethane 51 04/12/2017 20201015070-1301
1,2-Dibromoethane (EDB)47 04/12/2017 2020955070-1301
Dibromomethane (Methylene bromide)47 04/12/2017 2020945070-1301
trans-1,4-Dichloro-2-butene 45 04/12/2017 2020905034-1421
1,4-Dichlorobenzene 47 04/12/2017 2020945070-1301
1,2-Dichlorobenzene 48 04/12/2017 2020965070-1301
1,2-Dichloroethane 49 04/12/2017 2020975070-1301
1,1-Dichloroethane 48 04/12/2017 2020975070-1301
trans-1,2-Dichloroethene 51 04/12/2017 20201025070-1301
cis-1,2-Dichloroethene 49 04/12/2017 2020975070-1301
1,1-Dichloroethene 52 04/12/2017 20201035070-1301
1,2-Dichloropropane 48 04/12/2017 2020975070-1301
trans-1,3-Dichloropropene 47 04/12/2017 2020945070-1301
cis-1,3-Dichloropropene 51 04/12/2017 20201025070-1301
Ethylbenzene 48 04/12/2017 2020965070-1301
2-Hexanone 85 04/12/2017 20208510060-1401
Methyl iodide (Iodomethane)51 04/12/2017 20201015070-1301
4-Methyl-2-pentanone 90 04/12/2017 20209010060-1401
Methylene chloride 46 04/12/2017 2020915070-1301
Styrene 49 04/12/2017 2020985070-1301
1,1,2,2-Tetrachloroethane 48 04/12/2017 2020965070-1301
1,1,1,2-Tetrachloroethane 48 04/12/2017 2020965070-1301
Tetrachloroethene 51 04/12/2017 20201025070-1301
Tetrahydrofuran 46 04/12/2017 2020915070-1301
Toluene 49 04/12/2017 2020985070-1301
1,1,2-Trichloroethane 47 04/12/2017 2020935070-1301
1,1,1-Trichloroethane 49 04/12/2017 2020985070-1301
Trichloroethene 48 04/12/2017 2020965070-1301
Trichlorofluoromethane 48 04/12/2017 2020965060-1401
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 24 of 34
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ39496-002
39496 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
1,2,3-Trichloropropane 49 04/12/2017 2020995070-1301
Vinyl acetate 56 04/12/2017 20201125060-1401
Vinyl chloride 50 04/12/2017 20201005060-1401
Xylenes (total)97 04/12/2017 20209710070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 102 70-130
1,2-Dichloroethane-d4 99 70-130
Toluene-d8 98 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 25 of 34
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Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ40382-001
40382 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Vinyl chloride 0.50 04/24/2017 2039U0.50 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 103 70-130
1,2-Dichloroethane-d4 93 70-130
Toluene-d8 98 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 26 of 34
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ40382-002
40382 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Vinyl chloride 55 04/24/2017 19251115060-1401
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 100 70-130
1,2-Dichloroethane-d4 93 70-130
Toluene-d8 99 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 27 of 34
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ICP-MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ39507-001
39507 3005A
04/13/2017 905Analytical Method:6020B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Arsenic 2.0 04/13/2017 1318U2.0 1.3 ug/L1
Barium 5.0 04/13/2017 1318U5.0 0.63 ug/L1
Cadmium 0.50 04/13/2017 1318U0.50 0.13 ug/L1
Chromium 5.0 04/13/2017 1318U5.0 1.3 ug/L1
Lead 1.0 04/13/2017 1318U1.0 0.25 ug/L1
Selenium 5.0 04/13/2017 1318U5.0 1.3 ug/L1
Silver 1.0 04/13/2017 1318U1.0 0.25 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 28 of 34
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Shealy Environmental Services, Inc.

ICP-MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ39507-002
39507 3005A
04/13/2017 905Analytical Method:6020B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Arsenic 100 04/13/2017 132410210080-1201
Barium 100 04/13/2017 132410010080-1201
Cadmium 100 04/13/2017 132410010080-1201
Chromium 100 04/13/2017 132410010080-1201
Lead 96 04/13/2017 13249610080-1201
Selenium 110 04/13/2017 132410610080-1201
Silver 100 04/13/2017 132410310080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 29 of 34
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ39621-001
39621 7470A
04/14/2017 1246Analytical Method:7470A
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Mercury 0.000050 04/14/2017 1620J0.00010 0.000028 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 30 of 34
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ39621-002
39621 7470A
04/14/2017 1246Analytical Method:7470A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Mercury 0.0019 04/14/2017 1623960.0020 80-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 31 of 34
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS - MS
Batch:Prep Method:
Prep Date:
Sample ID:SD12009-003MS
39621 7470A
04/14/2017 1246Analytical Method:7470A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Mercury 0.0020 04/14/2017 1717960.0020 85-1150.000038 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 32 of 34
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS - MSD
Batch:Prep Method:
Prep Date:
Sample ID:SD12009-003MD
39621 7470A
04/14/2017 1246Analytical Method:7470A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Mercury 0.0020 04/14/2017 17201000.0020 85-1154.0 200.000038 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 33 of 34
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

ICP-MS - MS
Batch:Prep Method:
Prep Date:
Sample ID:SD12009-004MS
39621 7470A
04/14/2017 1246Analytical Method:7470A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Mercury 0.0047 04/14/2017 1725900.0020 85-1150.0029 1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
U = Not detected at or above the detection limit
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 34 of 34
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

cdmsmith.com